data_cu_lp18017_0m_c_pl_sq _audit_creation_method 'SHELXL-2018/1' _shelx_SHELXL_version_number '2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C48 H24 N6 O8 Pd Zn2' _chemical_formula_weight 1049.87 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' 0.1215 3.9337 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Zn' 'Zn' -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system tetragonal _space_group_IT_number 123 _space_group_name_H-M_alt 'P 4/m m m' _space_group_name_Hall '-P 4 2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x, z' '-x, -y, z' 'y, -x, z' 'x, -y, -z' 'y, x, -z' '-x, y, -z' '-y, -x, -z' '-x, -y, -z' 'y, -x, -z' 'x, y, -z' '-y, x, -z' '-x, y, z' '-y, -x, z' 'x, -y, z' 'y, x, z' _cell_length_a 16.6421(8) _cell_length_b 16.6421(8) _cell_length_c 16.1146(15) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4463.1(6) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9966 _cell_measurement_theta_min 2.66 _cell_measurement_theta_max 64.97 _exptl_crystal_description 'plate' _exptl_crystal_colour 'clear_dark_red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 0.391 _exptl_crystal_F_000 524 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.20 _exptl_crystal_size_min 0.08 _exptl_absorpt_coefficient_mu 1.245 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.4869 _exptl_absorpt_correction_T_max 0.7526 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type Cu K\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 33559 _diffrn_reflns_av_unetI/netI 0.0463 _diffrn_reflns_av_R_equivalents 0.1790 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.756 _diffrn_reflns_theta_max 53.386 _diffrn_reflns_theta_full 53.386 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 1588 _reflns_number_gt 1288 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX3 V2016.1-0' _computing_cell_refinement 'Bruker SAINT 8.37A' _computing_data_reduction 'Bruker SAINT 8.37A' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1040P)^2^+7.8451P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 1588 _refine_ls_number_parameters 59 _refine_ls_number_restraints 12 _refine_ls_R_factor_all 0.0747 _refine_ls_R_factor_gt 0.0625 _refine_ls_wR_factor_ref 0.1850 _refine_ls_wR_factor_gt 0.1752 _refine_ls_goodness_of_fit_ref 1.060 _refine_ls_restrained_S_all 1.079 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.500000 0.500000 0.500000 0.0386(5) Uani 1 16 d S T P . . N1 N 0.3788(4) 0.500000 0.500000 0.0371(19) Uani 1 4 d S T P . . C1 C 0.2470(3) 0.4592(4) 0.500000 0.063(2) Uani 1 2 d S T P . . H1 H 0.201426 0.424914 0.500000 0.076 Uiso 1 2 calc R U P . . C2 C 0.3301(3) 0.4353(3) 0.500000 0.0426(17) Uani 1 2 d S T P . . Zn1 Zn 0.000000 0.000000 0.40980(11) 0.0329(6) Uani 1 8 d S T P . . O1 O 0.0843(2) 0.0843(2) 0.4334(4) 0.0754(17) Uani 1 2 d S T P . . N2 N 0.000000 0.000000 0.2873(12) 0.094(5) Uani 1 8 d S T P . . C4 C 0.2904(3) 0.2904(3) 0.500000 0.044(3) Uani 1 4 d S T P . . C3 C 0.3547(3) 0.3547(3) 0.500000 0.046(3) Uani 1 4 d S T P . . C5 C 0.2612(3) 0.2612(3) 0.4252(6) 0.085(3) Uani 1 2 d S TU P . . H5 H 0.281397 0.281397 0.374222 0.102 Uiso 1 2 calc R U P . . C6 C 0.2015(3) 0.2015(3) 0.4254(6) 0.077(3) Uani 1 2 d S TU P . . H6 H 0.181032 0.181032 0.374583 0.093 Uiso 1 2 calc R U P . . C7 C 0.1728(3) 0.1728(3) 0.500000 0.047(3) Uani 1 4 d S T P . . C8 C 0.1077(4) 0.1077(4) 0.500000 0.045(3) Uani 1 4 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.0085(5) 0.0085(5) 0.0989(13) 0.000 0.000 0.000 N1 0.024(4) 0.011(4) 0.076(5) 0.000 0.000 0.000 C1 0.011(3) 0.024(3) 0.154(7) 0.000 0.000 0.003(3) C2 0.020(3) 0.016(3) 0.091(5) 0.000 0.000 -0.003(3) Zn1 0.0136(6) 0.0136(6) 0.0714(13) 0.000 0.000 0.000 O1 0.056(2) 0.056(2) 0.114(5) -0.006(2) -0.006(2) -0.036(3) N2 0.071(6) 0.071(6) 0.141(15) 0.000 0.000 0.000 C4 0.012(3) 0.012(3) 0.108(9) 0.000 0.000 0.003(3) C3 0.020(3) 0.020(3) 0.098(8) 0.000 0.000 -0.007(4) C5 0.080(4) 0.080(4) 0.096(6) 0.004(3) 0.004(3) -0.065(5) C6 0.074(4) 0.074(4) 0.083(5) -0.002(3) -0.002(3) -0.053(5) C7 0.014(3) 0.014(3) 0.113(9) 0.000 0.000 -0.004(3) C8 0.017(3) 0.017(3) 0.100(9) 0.000 0.000 -0.004(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 N1 2.017(6) 10_566 ? Pd1 N1 2.017(6) . ? Pd1 N1 2.017(6) 9_666 ? Pd1 N1 2.017(6) 2_655 ? N1 C2 1.347(7) 5_566 ? N1 C2 1.347(7) . ? C1 C1 1.357(13) 5_566 ? C1 C2 1.439(8) . ? C1 H1 0.9500 . ? C2 C3 1.403(7) . ? Zn1 N2 1.975(19) . ? Zn1 O1 2.021(5) . ? Zn1 O1 2.021(5) 3 ? Zn1 O1 2.021(5) 4 ? Zn1 O1 2.021(5) 2 ? Zn1 Zn1 2.907(3) 9_556 ? O1 C8 1.205(6) . ? C4 C5 1.387(9) 11_556 ? C4 C5 1.387(9) . ? C4 C3 1.514(11) . ? C5 C6 1.405(10) . ? C5 H5 0.9500 . ? C6 C7 1.378(9) . ? C6 H6 0.9500 . ? C7 C8 1.533(12) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Pd1 N1 90.0 10_566 . ? N1 Pd1 N1 90.000(1) 10_566 9_666 ? N1 Pd1 N1 180.0 . 9_666 ? N1 Pd1 N1 180.0 10_566 2_655 ? N1 Pd1 N1 90.000(1) . 2_655 ? N1 Pd1 N1 90.0 9_666 2_655 ? C2 N1 C2 106.1(7) 5_566 . ? C2 N1 Pd1 127.0(3) 5_566 . ? C2 N1 Pd1 127.0(3) . . ? C1 C1 C2 106.1(3) 5_566 . ? C1 C1 H1 127.0 5_566 . ? C2 C1 H1 127.0 . . ? N1 C2 C3 126.1(6) . . ? N1 C2 C1 110.9(5) . . ? C3 C2 C1 123.0(5) . . ? N2 Zn1 O1 100.87(19) . . ? N2 Zn1 O1 100.87(19) . 3 ? O1 Zn1 O1 158.3(4) . 3 ? N2 Zn1 O1 100.87(19) . 4 ? O1 Zn1 O1 87.96(7) . 4 ? O1 Zn1 O1 87.96(7) 3 4 ? N2 Zn1 O1 100.87(19) . 2 ? O1 Zn1 O1 87.96(7) . 2 ? O1 Zn1 O1 87.96(7) 3 2 ? O1 Zn1 O1 158.3(4) 4 2 ? N2 Zn1 Zn1 180.0 . 9_556 ? O1 Zn1 Zn1 79.13(19) . 9_556 ? O1 Zn1 Zn1 79.13(19) 3 9_556 ? O1 Zn1 Zn1 79.13(19) 4 9_556 ? O1 Zn1 Zn1 79.13(19) 2 9_556 ? C8 O1 Zn1 128.0(6) . . ? C5 C4 C5 120.6(9) 11_556 . ? C5 C4 C3 119.7(4) 11_556 . ? C5 C4 C3 119.7(4) . . ? C2 C3 C2 123.9(7) 6_556 . ? C2 C3 C4 118.0(4) 6_556 . ? C2 C3 C4 118.0(4) . . ? C4 C5 C6 119.6(8) . . ? C4 C5 H5 120.2 . . ? C6 C5 H5 120.2 . . ? C7 C6 C5 119.4(8) . . ? C7 C6 H6 120.3 . . ? C5 C6 H6 120.3 . . ? C6 C7 C6 121.4(9) . 11_556 ? C6 C7 C8 119.3(4) . . ? C6 C7 C8 119.3(4) 11_556 . ? O1 C8 O1 125.7(9) . 11_556 ? O1 C8 C7 117.1(5) . . ? O1 C8 C7 117.1(5) 11_556 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 N1 C2 C3 180.0 5_566 . . . ? Pd1 N1 C2 C3 0.0 . . . . ? C2 N1 C2 C1 0.0 5_566 . . . ? Pd1 N1 C2 C1 180.0 . . . . ? C1 C1 C2 N1 0.0 5_566 . . . ? C1 C1 C2 C3 180.0 5_566 . . . ? N1 C2 C3 C2 0.0 . . . 6_556 ? C1 C2 C3 C2 180.0 . . . 6_556 ? N1 C2 C3 C4 180.0 . . . . ? C1 C2 C3 C4 0.0 . . . . ? C5 C4 C3 C2 90.000(0) 11_556 . . 6_556 ? C5 C4 C3 C2 -90.000(0) . . . 6_556 ? C5 C4 C3 C2 -90.000(0) 11_556 . . . ? C5 C4 C3 C2 90.000(0) . . . . ? C5 C4 C5 C6 0.000(1) 11_556 . . . ? C3 C4 C5 C6 180.000(1) . . . . ? C4 C5 C6 C7 0.000(1) . . . . ? C5 C6 C7 C6 0.000(0) . . . 11_556 ? C5 C6 C7 C8 180.000(0) . . . . ? Zn1 O1 C8 O1 0.000(0) . . . 11_556 ? Zn1 O1 C8 C7 180.000(0) . . . . ? C6 C7 C8 O1 0.000(0) . . . . ? C6 C7 C8 O1 180.000(0) 11_556 . . . ? C6 C7 C8 O1 180.000(0) . . . 11_556 ? C6 C7 C8 O1 0.000(0) 11_556 . . 11_556 ? _refine_diff_density_max 1.601 _refine_diff_density_min -0.669 _refine_diff_density_rms 0.073 _shelx_res_file ; TITL cu_LP18017P -4c R = 0.26 New: P4/mmm cu_lp18017_0m_c_pl_sq.res created by SHELXL-2018/1 at 01:27:29 on 21-Dec-2019 CELL 1.54178 16.6421 16.6421 16.1146 90.000 90.000 90.000 ZERR 1 0.0008 0.0008 0.0015 0.000 0.000 0.000 LATT 1 SYMM - Y , X , Z SYMM - X , - Y , Z SYMM Y , - X , Z SYMM X , - Y , - Z SYMM Y , X , - Z SYMM - X , Y , - Z SYMM - Y , - X , - Z SFAC C N O Pd Zn H UNIT 48 6 8 1 2 24 LIST 4 TEMP -173 L.S. 20 0 80 FMAP 2 PLAN -20 ACTA BOND $H shel 15 0.96 isor 0.01 0.02 C5 C6 CONF ABIN WGHT 0.104000 7.845100 FVAR 0.38405 RESI 0 PD1 4 0.500000 0.500000 0.500000 10.06250 0.00846 0.00846 = 0.09889 0.00000 0.00000 0.00000 N1 2 0.378792 0.500000 0.500000 10.25000 0.02365 0.01127 = 0.07638 0.00000 0.00000 0.00000 C1 1 0.247035 0.459242 0.500000 10.50000 0.01102 0.02433 = 0.15417 0.00000 0.00000 0.00290 AFIX 43 H1 6 0.201426 0.424914 0.500000 10.50000 -1.20000 AFIX 0 C2 1 0.330107 0.435318 0.500000 10.50000 0.02048 0.01589 = 0.09142 0.00000 0.00000 -0.00330 ZN1 5 0.000000 0.000000 0.409797 10.12500 0.01364 0.01364 = 0.07145 0.00000 0.00000 0.00000 O1 3 0.084341 0.084341 0.433443 10.50000 0.05594 0.05594 = 0.11435 -0.00624 -0.00624 -0.03567 N2 2 0.000000 0.000000 0.287256 10.12500 0.07096 0.07096 = 0.14051 0.00000 0.00000 0.00000 C4 1 0.290395 0.290395 0.500000 10.25000 0.01245 0.01245 = 0.10776 0.00000 0.00000 0.00250 C3 1 0.354711 0.354711 0.500000 10.25000 0.01966 0.01966 = 0.09780 0.00000 0.00000 -0.00672 C5 1 0.261168 0.261168 0.425237 10.50000 0.07977 0.07977 = 0.09576 0.00399 0.00399 -0.06483 AFIX 43 H5 6 0.281397 0.281397 0.374222 10.50000 -1.20000 AFIX 0 C6 1 0.201470 0.201470 0.425419 10.50000 0.07435 0.07435 = 0.08300 -0.00174 -0.00174 -0.05333 AFIX 43 H6 6 0.181032 0.181032 0.374583 10.50000 -1.20000 AFIX 0 C7 1 0.172839 0.172839 0.500000 10.25000 0.01403 0.01403 = 0.11262 0.00000 0.00000 -0.00353 C8 1 0.107689 0.107689 0.500000 10.25000 0.01709 0.01709 = 0.09970 0.00000 0.00000 -0.00402 HKLF 4 REM cu_LP18017P -4c R = 0.26 New: P4/mmm REM R1 = 0.0625 for 1288 Fo > 4sig(Fo) and 0.0747 for all 1588 data REM 59 parameters refined using 12 restraints END WGHT 0.1025 7.5624 REM Highest difference peak 1.601, deepest hole -0.669, 1-sigma level 0.073 Q1 1 0.5000 0.5000 0.4243 10.12500 0.05 1.60 Q2 1 0.0000 0.0000 0.5000 10.06250 0.05 1.50 Q3 1 0.0000 0.0000 0.3294 10.12500 0.05 0.62 Q4 1 0.5000 0.4442 0.5000 10.25000 0.05 0.54 Q5 1 0.0473 0.0473 0.2400 10.50000 0.05 0.44 Q6 1 0.2490 0.5480 0.5712 11.00000 0.05 0.31 Q7 1 0.2096 0.5000 0.4484 10.50000 0.05 0.26 Q8 1 0.2281 0.2281 0.3515 10.50000 0.05 0.25 Q9 1 0.3461 0.5000 0.5000 10.25000 0.05 0.23 Q10 1 0.0698 0.1136 0.5000 10.50000 0.05 0.22 Q11 1 0.0931 0.0931 0.3712 10.50000 0.05 0.21 Q12 1 0.2441 0.5000 0.5000 10.25000 0.05 0.20 Q13 1 0.2097 0.1563 0.3691 11.00000 0.05 0.19 Q14 1 0.1089 0.1089 0.4280 10.50000 0.05 0.18 Q15 1 0.5000 0.3737 0.4355 10.50000 0.05 0.17 Q16 1 0.3268 0.5614 0.5753 11.00000 0.05 0.17 Q17 1 0.1672 0.2244 0.4528 11.00000 0.05 0.17 Q18 1 0.1366 0.1366 0.3954 10.50000 0.05 0.16 Q19 1 0.1579 0.5000 0.5000 10.25000 0.05 0.15 Q20 1 0.1985 0.1985 0.5000 10.25000 0.05 0.15 ; _shelx_res_checksum 35365 _shelx_hkl_file ; -3 0 0 459.84 36.90 -4 0 0 5900.82 469.16 -5 0 0 43.54 7.11 -6 0 0 352.05 29.45 -7 0 0 107.57 12.94 -8 0 0 759.17 62.57 -8 0 0 760.48 62.61 -9 0 0 99.57 23.19 9 0 0 58.03 13.34 10 0 0 780.45 64.21 10 0 0 760.38 64.52 10 0 0 746.45 63.73 10 0 0 815.96 64.19 -11 0 0 394.87 36.99 11 0 0 370.90 35.40 11 0 0 350.10 34.52 11 0 0 394.06 34.90 11 0 0 406.44 33.94 11 0 0 385.37 35.11 -12 0 0 1379.63 103.13 12 0 0 1262.90 102.39 12 0 0 1153.00 102.00 -13 0 0 -4.82 12.54 13 0 0 7.00 11.08 13 0 0 -7.64 9.38 13 0 0 3.49 8.89 13 0 0 4.72 9.57 13 0 0 -11.39 8.93 -14 0 0 467.90 40.70 14 0 0 409.60 40.04 14 0 0 430.47 40.54 14 0 0 454.45 39.41 14 0 0 484.09 40.76 -15 0 0 3.90 12.34 15 0 0 8.57 13.61 15 0 0 32.37 10.08 15 0 0 5.64 11.37 15 0 0 -2.57 9.40 15 0 0 7.79 11.93 -16 0 0 450.02 41.77 16 0 0 471.16 41.72 16 0 0 527.02 42.38 16 0 0 422.52 42.55 16 0 0 499.40 41.24 -17 0 0 -9.61 10.59 17 0 0 -11.22 10.59 17 0 0 -5.54 10.51 17 0 0 -12.81 8.46 17 0 0 -2.54 8.30 -18 0 0 361.23 30.99 18 0 0 301.41 32.86 18 0 0 326.34 31.87 18 0 0 320.80 31.55 18 0 0 376.18 30.63 -19 0 0 11.20 9.12 19 0 0 -37.03 22.84 19 0 0 9.33 7.96 19 0 0 -3.78 13.97 19 -1 0 323.40 27.49 19 -1 0 268.54 27.64 -19 1 0 287.95 26.95 18 -1 0 -2.57 9.99 18 -1 0 -13.84 8.88 18 -1 0 29.33 12.97 18 -1 0 -2.77 8.60 -18 1 0 3.21 10.09 17 -1 0 337.55 30.51 17 -1 0 320.59 28.93 17 -1 0 269.09 31.80 17 -1 0 330.49 30.25 -17 1 0 317.75 30.56 16 -1 0 26.85 9.66 16 -1 0 10.86 11.85 16 -1 0 14.12 11.01 16 -1 0 30.99 9.49 -16 1 0 7.33 11.93 15 -1 0 423.16 39.72 15 -1 0 491.82 39.92 15 -1 0 442.53 38.65 15 -1 0 402.58 40.96 15 -1 0 475.52 50.01 -15 1 0 398.56 40.00 14 -1 0 -2.84 9.37 14 -1 0 19.48 13.86 14 -1 0 8.02 9.83 14 -1 0 -6.16 11.03 14 -1 0 -4.42 10.77 -14 1 0 -3.71 13.46 13 -1 0 641.28 59.25 13 -1 0 769.28 59.67 13 -1 0 669.29 58.89 13 -1 0 741.54 58.64 -13 1 0 697.30 60.54 12 -1 0 -9.31 9.49 12 -1 0 -11.58 9.50 12 -1 0 5.72 11.38 -12 1 0 11.40 14.98 11 -1 0 1266.79 106.75 11 -1 0 1397.68 106.65 11 -1 0 1308.82 106.55 11 -1 0 1440.33 107.29 -11 1 0 1176.31 107.99 10 -1 0 222.97 20.36 10 -1 0 153.43 21.18 10 -1 0 181.55 21.71 10 -1 0 220.27 21.69 10 -1 0 190.81 23.18 9 -1 0 876.27 71.76 9 -1 0 931.49 71.70 -9 1 0 792.02 75.75 -8 1 0 75.26 15.71 3 -1 0 638.59 50.91 2 -1 0 61.08 5.89 -2 1 0 76.68 5.86 1 -1 0 2660.24 216.08 -1 1 0 2771.16 216.08 0 -1 0 2.88 1.18 0 1 0 3.04 0.90 -1 -1 0 3403.02 271.10 1 1 0 3410.96 271.10 -2 -1 0 91.52 8.08 2 1 0 93.93 8.16 -3 -1 0 825.62 66.01 -4 -1 0 114.79 11.22 -5 -1 0 728.48 58.68 -6 -1 0 105.83 11.80 -8 -1 0 69.50 15.62 -8 -1 0 69.01 15.17 -9 -1 0 966.80 76.15 -9 -1 0 896.74 77.11 9 1 0 865.88 74.47 -10 -1 0 256.16 26.47 -10 -1 0 296.60 36.36 10 1 0 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136.46 28.52 7 -9 2 181.88 30.91 7 -9 2 183.91 23.02 8 -9 2 149.77 23.55 8 -9 2 178.95 28.02 8 -9 2 163.53 24.82 8 -9 2 154.33 26.84 8 -9 2 164.43 26.34 9 -9 2 607.82 53.55 9 -9 2 615.28 53.48 9 -9 2 543.91 52.98 9 -9 2 604.23 52.22 10 -9 2 124.21 23.98 10 -9 2 101.61 18.31 10 -9 2 74.83 15.17 10 -9 2 87.21 17.12 11 -9 2 132.00 23.31 11 -9 2 130.38 26.42 11 -9 2 94.04 16.47 11 -9 2 86.60 18.46 12 -9 2 19.62 14.75 12 -9 2 -1.19 13.80 12 -9 2 20.90 13.76 13 -9 2 49.98 13.27 13 -9 2 68.11 15.55 13 -9 2 51.81 14.37 14 -9 2 37.03 13.02 14 -9 2 29.62 12.61 14 -9 2 40.79 13.24 15 -9 2 182.85 23.09 15 -9 2 181.33 23.61 15 -9 2 244.98 26.60 16 -9 2 12.34 10.99 16 -9 2 -3.97 13.40 16 -9 2 -6.43 11.63 17 -9 2 66.31 15.30 17 -9 2 71.80 12.72 17 -9 2 90.28 20.39 17 8 -2 31.84 13.56 17 8 -2 26.89 11.10 16 8 -2 148.50 18.60 16 8 -2 142.36 18.09 16 8 -2 155.64 21.16 15 8 -2 -0.85 7.79 15 8 -2 -9.49 9.15 15 8 -2 22.36 9.72 -15 -8 2 -1.78 24.65 14 8 -2 105.82 16.56 -14 -8 2 70.68 29.35 13 8 -2 34.52 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19.07 16 -8 2 174.50 22.71 17 -8 2 9.13 10.39 17 -8 2 6.53 10.93 17 -8 2 -4.98 11.25 18 7 -2 -3.03 10.87 18 7 -2 1.74 18.22 18 7 -2 19.78 7.58 17 7 -2 164.56 18.92 17 7 -2 110.96 21.78 17 7 -2 160.59 18.29 16 7 -2 42.90 10.97 16 7 -2 20.02 9.76 16 7 -2 32.08 8.72 -16 -7 2 44.09 13.07 15 7 -2 178.26 20.57 15 7 -2 147.76 22.51 15 7 -2 227.00 20.06 -15 -7 2 184.19 20.55 14 7 -2 97.28 16.55 14 7 -2 96.77 16.77 -14 -7 2 118.86 15.05 -14 -7 2 29.63 27.05 13 7 -2 232.76 22.86 13 7 -2 202.25 22.72 -13 -7 2 144.91 28.14 12 7 -2 33.74 9.33 12 7 -2 33.25 11.91 -12 -7 2 23.54 12.79 -12 -7 2 39.05 20.39 11 7 -2 49.65 13.45 11 7 -2 46.23 9.93 -11 -7 2 24.07 19.13 -11 -7 2 36.27 12.72 10 7 -2 71.45 11.52 10 7 -2 86.81 14.68 9 7 -2 198.56 21.39 9 7 -2 131.40 25.53 9 7 -2 214.72 23.04 -9 -7 2 172.88 23.05 -9 -7 2 162.97 25.24 8 7 -2 64.81 10.18 8 7 -2 68.87 14.48 8 7 -2 69.89 12.42 -8 -7 2 79.37 15.55 7 7 -2 575.63 46.91 7 7 -2 555.76 48.11 7 7 -2 513.40 45.42 7 7 -2 526.43 53.74 -7 -7 2 527.76 47.51 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188.67 23.03 -6 -15 3 211.71 24.33 -6 -15 3 227.13 23.02 -6 -15 3 201.16 25.33 -5 -15 3 93.15 14.52 -5 -15 3 75.23 12.95 -5 -15 3 128.12 25.48 4 15 -3 34.81 9.59 4 15 -3 32.22 9.79 -4 -15 3 39.16 12.20 -4 -15 3 30.90 10.09 -4 -15 3 41.25 12.17 3 15 -3 22.28 10.76 3 15 -3 35.69 10.27 -3 -15 3 30.76 13.76 -3 -15 3 17.97 9.80 -3 -15 3 14.17 11.86 2 15 -3 30.24 12.74 2 15 -3 22.64 15.83 -2 -15 3 32.58 11.73 -2 -15 3 57.18 18.77 -2 -15 3 45.82 10.22 1 15 -3 28.05 14.71 -1 -15 3 53.66 10.43 -1 -15 3 45.47 11.98 0 15 -3 307.02 34.09 0 -15 3 258.94 27.46 0 -15 3 279.60 27.26 -1 15 -3 39.39 20.63 1 -15 3 39.26 11.26 1 -15 3 64.52 10.50 2 -15 3 38.04 11.18 2 -15 3 46.83 10.53 3 -15 3 12.13 11.17 3 -15 3 12.07 10.25 4 -15 3 23.51 10.27 5 -15 3 122.87 16.74 5 -15 3 102.37 20.63 6 -15 3 213.29 33.11 7 -15 3 104.91 18.60 7 -15 3 78.49 15.53 8 -15 3 50.94 11.69 8 -15 3 80.04 15.07 9 -15 3 68.89 12.21 9 -15 3 85.31 16.37 10 -15 3 112.99 18.64 11 -15 3 -2.27 16.17 13 14 -3 79.25 14.20 13 14 -3 22.12 17.01 -13 -14 3 55.40 12.50 12 14 -3 -1.72 8.06 12 14 -3 42.35 27.47 -12 -14 3 17.96 9.95 11 14 -3 29.75 21.48 11 14 -3 77.36 15.04 -11 -14 3 82.25 13.28 10 14 -3 75.65 15.38 -10 -14 3 65.38 13.34 9 14 -3 124.85 17.60 9 14 -3 110.93 17.67 -9 -14 3 125.44 15.38 8 14 -3 33.03 9.39 -8 -14 3 34.25 12.72 -8 -14 3 38.06 16.54 7 14 -3 190.14 19.09 7 14 -3 137.31 20.36 -7 -14 3 169.59 18.66 -7 -14 3 172.15 30.03 -7 -14 3 133.46 22.27 6 14 -3 111.71 16.41 -6 -14 3 85.77 17.77 -6 -14 3 138.35 19.50 -6 -14 3 101.71 14.98 5 14 -3 106.80 15.21 5 14 -3 83.74 16.89 -5 -14 3 66.28 12.47 -5 -14 3 109.39 16.48 -5 -14 3 78.42 15.99 4 14 -3 0.85 10.10 4 14 -3 4.95 9.56 -4 -14 3 10.58 9.77 -4 -14 3 4.75 11.88 -4 -14 3 11.03 12.47 3 14 -3 3.28 10.05 3 14 -3 -5.01 11.13 -3 -14 3 11.51 11.19 -3 -14 3 8.41 12.77 -3 -14 3 6.11 9.07 2 14 -3 22.63 10.55 2 14 -3 -20.03 12.87 -2 -14 3 13.73 9.15 -2 -14 3 -24.27 13.95 -2 -14 3 18.09 11.21 1 14 -3 118.85 19.61 -1 -14 3 144.57 18.70 -1 -14 3 120.45 17.66 0 14 -3 36.13 17.17 0 -14 3 28.59 10.63 0 -14 3 30.59 10.21 -1 14 -3 132.92 21.46 1 -14 3 142.28 18.76 1 -14 3 126.05 18.45 2 -14 3 6.08 10.36 2 -14 3 17.57 9.65 3 -14 3 -1.76 10.31 3 -14 3 11.50 10.62 4 -14 3 4.80 10.65 4 -14 3 17.29 11.37 5 -14 3 85.98 17.08 5 -14 3 82.27 14.08 6 -14 3 135.94 21.82 6 -14 3 115.67 19.10 7 -14 3 167.30 22.72 7 -14 3 171.13 20.83 8 -14 3 27.71 14.20 8 -14 3 16.51 13.64 9 -14 3 105.29 18.10 9 -14 3 104.59 18.88 10 -14 3 41.13 12.21 11 -14 3 103.09 21.49 14 13 -3 46.97 13.53 14 13 -3 53.36 12.52 13 13 -3 36.12 8.51 13 13 -3 41.47 13.94 -13 -13 3 56.48 11.53 12 13 -3 29.65 8.35 12 13 -3 30.67 15.32 -12 -13 3 26.08 11.45 11 13 -3 19.37 8.12 11 13 -3 33.31 17.90 -11 -13 3 13.13 10.98 10 13 -3 44.23 9.19 10 13 -3 42.07 20.31 -10 -13 3 73.58 12.98 9 13 -3 1.46 8.69 9 13 -3 4.70 12.49 9 13 -3 -30.48 32.26 -9 -13 3 10.14 10.17 8 13 -3 63.29 10.97 8 13 -3 94.20 16.21 -8 -13 3 99.48 21.61 -8 -13 3 57.12 14.31 -8 -13 3 80.74 15.10 7 13 -3 55.53 10.63 7 13 -3 77.41 12.54 -7 -13 3 52.55 18.46 -7 -13 3 76.75 12.73 -7 -13 3 60.86 13.08 6 13 -3 118.11 16.21 6 13 -3 86.01 17.05 -6 -13 3 116.45 16.70 -6 -13 3 152.66 25.71 -6 -13 3 78.96 13.93 5 13 -3 15.31 8.83 5 13 -3 19.81 9.41 -5 -13 3 39.35 10.60 -5 -13 3 17.55 13.65 -5 -13 3 22.61 11.37 4 13 -3 0.78 10.04 4 13 -3 -4.46 8.99 -4 -13 3 5.17 9.91 -4 -13 3 -2.33 11.31 -4 -13 3 4.79 12.06 3 13 -3 9.33 11.46 3 13 -3 28.96 9.51 -3 -13 3 32.34 10.16 -3 -13 3 23.24 11.28 2 13 -3 92.02 15.95 -2 -13 3 91.45 17.35 -2 -13 3 88.43 15.67 -2 -13 3 65.32 14.86 1 13 -3 48.78 15.82 1 13 -3 42.76 14.26 -1 -13 3 55.68 11.19 -1 -13 3 64.74 10.21 0 13 -3 159.58 27.27 0 -13 3 173.94 20.57 0 -13 3 171.42 20.56 1 -13 3 55.30 10.81 1 -13 3 59.52 11.71 2 -13 3 94.24 16.34 2 -13 3 67.59 11.55 3 -13 3 26.36 9.59 3 -13 3 14.63 10.66 4 -13 3 22.62 11.18 4 -13 3 4.79 10.63 5 -13 3 25.36 11.65 5 -13 3 39.24 11.78 6 -13 3 76.86 17.45 6 -13 3 107.01 20.45 7 -13 3 56.31 13.71 7 -13 3 58.52 15.30 7 -13 3 82.46 13.85 8 -13 3 70.82 15.50 8 -13 3 35.33 14.94 8 -13 3 64.66 13.47 9 -13 3 11.25 12.89 10 -13 3 37.76 10.98 10 -13 3 51.38 12.06 10 -13 3 23.96 12.76 11 -13 3 6.31 12.20 11 -13 3 38.97 14.64 12 -13 3 5.49 11.91 15 12 -3 36.41 12.29 15 12 -3 33.82 11.63 -15 -12 3 17.12 16.08 14 12 -3 13.68 7.49 14 12 -3 18.55 11.74 -14 -12 3 7.55 11.96 13 12 -3 18.59 13.41 13 12 -3 28.97 7.90 -13 -12 3 27.69 11.93 12 12 -3 16.08 8.12 12 12 -3 28.34 14.36 -12 -12 3 8.76 11.81 11 12 -3 29.58 15.51 11 12 -3 12.39 7.94 -11 -12 3 33.54 11.82 10 12 -3 -17.84 14.10 10 12 -3 13.68 8.51 10 12 -3 9.88 18.60 -10 -12 3 6.64 11.26 9 12 -3 35.30 10.04 9 12 -3 71.20 13.14 9 12 -3 59.26 22.71 -9 -12 3 41.13 12.15 8 12 -3 2.97 9.04 8 12 -3 13.52 24.74 8 12 -3 5.23 11.03 -8 -12 3 5.65 13.16 -8 -12 3 -8.22 20.65 -8 -12 3 6.10 10.89 7 12 -3 88.69 17.00 7 12 -3 135.06 16.72 -7 -12 3 68.25 15.13 -7 -12 3 107.26 16.51 -7 -12 3 119.94 20.36 6 12 -3 58.02 10.67 6 12 -3 36.63 9.23 -6 -12 3 60.96 11.96 -6 -12 3 84.04 17.07 -6 -12 3 51.33 12.04 5 12 -3 44.19 10.00 5 12 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18.89 11 -12 3 30.48 13.98 11 -12 3 13.43 16.80 11 -12 3 8.75 11.96 12 -12 3 17.43 16.35 12 -12 3 16.11 12.65 13 -12 3 15.68 12.01 13 -12 3 8.82 16.14 14 -12 3 18.50 22.70 14 -12 3 17.93 21.54 15 -12 3 -13.52 15.42 15 -12 3 34.12 14.96 15 11 -3 26.27 7.89 -15 -11 3 18.65 15.08 14 11 -3 90.30 13.98 14 11 -3 80.59 13.33 -14 -11 3 59.39 14.88 13 11 -3 15.34 12.57 13 11 -3 19.71 8.16 -13 -11 3 10.40 13.49 12 11 -3 24.75 12.65 12 11 -3 9.22 7.88 -12 -11 3 30.86 12.21 11 11 -3 70.38 16.38 11 11 -3 56.66 10.14 -11 -11 3 46.42 13.81 10 11 -3 149.10 26.27 10 11 -3 152.91 19.29 10 11 -3 118.00 22.07 -10 -11 3 126.42 19.48 9 11 -3 38.76 20.95 9 11 -3 16.04 12.76 9 11 -3 41.11 9.68 -9 -11 3 35.95 12.28 8 11 -3 83.73 24.07 8 11 -3 88.72 16.74 8 11 -3 93.77 13.38 -8 -11 3 95.84 22.82 -8 -11 3 115.95 17.15 -8 -11 3 61.80 17.96 7 11 -3 16.84 8.54 7 11 -3 60.48 29.06 7 11 -3 15.57 10.25 -7 -11 3 21.61 17.72 -7 -11 3 24.25 11.40 -7 -11 3 7.59 12.89 6 11 -3 99.55 15.95 -6 -11 3 89.82 14.44 -6 -11 3 135.18 25.08 5 11 -3 -7.58 9.62 -5 -11 3 -10.76 11.31 -5 -11 3 0.37 13.97 4 11 -3 55.63 10.42 -4 -11 3 88.06 16.72 -4 -11 3 79.26 17.07 -4 -11 3 103.57 17.69 3 11 -3 40.70 12.93 3 11 -3 38.24 9.29 -3 -11 3 61.74 12.55 -3 -11 3 15.99 12.69 2 11 -3 315.23 29.74 -2 -11 3 262.22 28.07 -2 -11 3 305.86 28.86 1 11 -3 144.11 18.47 1 11 -3 130.03 24.77 -1 -11 3 161.00 20.34 -1 -11 3 172.55 19.45 0 -11 3 16.33 16.25 0 -11 3 28.76 9.04 0 -11 3 26.01 10.51 1 -11 3 168.74 20.81 1 -11 3 157.47 19.51 2 -11 3 307.91 30.15 2 -11 3 347.14 30.91 3 -11 3 65.34 11.65 3 -11 3 83.20 16.79 4 -11 3 160.36 34.87 5 -11 3 -13.89 13.98 5 -11 3 32.29 12.35 5 -11 3 52.64 26.04 5 -11 3 10.70 10.87 6 -11 3 101.35 19.62 6 -11 3 95.80 18.79 6 -11 3 5.51 37.65 7 -11 3 28.52 13.18 7 -11 3 -17.19 22.82 7 -11 3 16.19 11.84 7 -11 3 23.18 13.82 8 -11 3 97.31 22.51 8 -11 3 69.23 13.44 8 -11 3 63.15 21.53 8 -11 3 79.06 15.76 8 -11 3 49.49 15.96 9 -11 3 39.00 13.11 9 -11 3 39.68 18.99 9 -11 3 31.02 15.87 9 -11 3 15.95 15.20 9 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10 -3 91.80 15.98 7 10 -3 130.29 26.50 7 10 -3 98.80 13.37 -7 -10 3 111.94 17.36 -7 -10 3 92.52 15.28 6 10 -3 27.68 8.34 -6 -10 3 23.76 11.86 -6 -10 3 30.73 16.03 -6 -10 3 -5.89 13.92 5 10 -3 170.60 20.84 5 10 -3 211.67 20.83 -5 -10 3 227.83 26.18 -5 -10 3 161.50 22.48 -5 -10 3 170.45 21.80 4 10 -3 5.70 9.97 4 10 -3 16.25 8.45 -4 -10 3 22.50 9.87 -4 -10 3 17.06 11.84 3 10 -3 146.20 20.28 3 10 -3 110.22 17.34 -3 -10 3 122.76 17.77 -3 -10 3 126.90 20.44 2 10 -3 29.48 10.29 1 10 -3 21.42 13.15 -1 -10 3 42.08 9.02 -1 -10 3 33.70 11.08 0 -10 3 10.35 14.50 0 -10 3 30.79 10.73 0 -10 3 30.51 8.79 1 -10 3 31.64 8.71 1 -10 3 26.32 20.26 1 -10 3 24.97 10.37 1 -10 3 83.14 42.14 2 -10 3 77.73 29.33 2 -10 3 61.97 9.95 3 -10 3 162.58 20.53 3 -10 3 134.98 18.44 3 -10 3 219.14 38.13 4 -10 3 30.58 9.10 4 -10 3 40.21 25.91 4 -10 3 26.17 11.30 4 -10 3 -13.54 18.92 5 -10 3 195.05 23.55 5 -10 3 203.54 23.26 5 -10 3 149.92 31.03 5 -10 3 253.69 34.78 6 -10 3 33.04 11.27 6 -10 3 25.13 13.27 6 -10 3 11.35 14.09 6 -10 3 48.74 22.71 7 -10 3 120.91 24.96 7 -10 3 100.17 16.78 7 -10 3 127.71 22.25 7 -10 3 80.39 24.03 8 -10 3 81.09 20.56 8 -10 3 65.07 13.17 8 -10 3 61.84 20.72 8 -10 3 72.71 15.58 8 -10 3 49.88 15.83 9 -10 3 127.59 23.73 9 -10 3 170.12 25.24 9 -10 3 233.06 26.42 9 -10 3 196.65 31.13 9 -10 3 177.68 28.68 10 -10 3 267.02 29.91 10 -10 3 279.25 32.07 10 -10 3 193.08 31.36 10 -10 3 255.97 32.08 10 -10 3 302.22 35.00 11 -10 3 92.00 18.98 11 -10 3 85.87 18.13 11 -10 3 115.77 23.52 11 -10 3 106.05 22.48 12 -10 3 -22.00 15.17 12 -10 3 -10.98 14.72 12 -10 3 32.59 13.39 13 -10 3 63.36 14.10 13 -10 3 36.35 12.55 13 -10 3 60.78 14.91 14 -10 3 50.16 14.84 14 -10 3 56.65 14.13 14 -10 3 58.05 14.14 15 -10 3 103.21 17.35 15 -10 3 87.00 14.06 15 -10 3 75.79 15.86 16 -10 3 49.31 15.00 16 -10 3 35.06 12.23 16 -10 3 32.17 13.06 17 9 -3 31.36 8.75 16 9 -3 45.06 11.37 -16 -9 3 -32.54 35.13 15 9 -3 72.59 12.48 15 9 -3 63.32 10.07 15 9 -3 48.80 15.39 -15 -9 3 28.20 19.67 14 9 -3 89.29 15.36 14 9 -3 130.89 16.32 -14 -9 3 95.00 19.46 13 9 -3 19.22 10.98 13 9 -3 19.70 8.54 -13 -9 3 -15.02 16.92 12 9 -3 84.48 16.54 12 9 -3 95.29 18.31 -12 -9 3 55.08 17.14 11 9 -3 43.36 14.67 11 9 -3 41.69 10.03 -11 -9 3 34.39 15.09 10 9 -3 288.22 28.48 10 9 -3 193.99 28.45 10 9 -3 231.82 24.80 -10 -9 3 243.41 27.02 9 9 -3 441.58 39.90 9 9 -3 331.24 34.94 -9 -9 3 414.82 36.25 8 9 -3 194.40 32.43 8 9 -3 218.31 23.90 8 9 -3 193.29 22.95 -8 -9 3 270.22 24.73 -8 -9 3 231.15 35.48 7 9 -3 59.49 22.17 7 9 -3 48.01 12.08 7 9 -3 83.80 14.90 -7 -9 3 60.01 15.04 -7 -9 3 56.91 19.18 6 9 -3 344.17 28.24 6 9 -3 294.93 41.02 6 9 -3 247.43 27.30 -6 -9 3 306.58 29.49 5 9 -3 18.79 9.67 5 9 -3 26.19 8.34 -5 -9 3 20.49 11.39 -5 -9 3 22.76 13.67 -5 -9 3 2.89 12.13 4 9 -3 252.93 22.76 4 9 -3 184.68 22.32 -4 -9 3 184.78 23.54 -4 -9 3 225.43 23.69 3 9 -3 98.73 13.68 -3 -9 3 88.00 16.07 -3 -9 3 73.95 14.35 -2 -9 3 73.91 14.36 -1 -9 3 63.79 12.55 -1 -9 3 74.19 13.83 0 -9 3 74.16 12.14 0 -9 3 56.04 9.64 -1 9 -3 60.24 21.40 1 -9 3 71.29 13.53 1 -9 3 51.76 11.18 -2 9 -3 70.75 20.87 2 -9 3 101.20 17.21 2 -9 3 100.24 14.78 -3 9 -3 42.73 21.74 3 -9 3 65.30 11.91 3 -9 3 79.29 14.32 4 -9 3 265.37 24.52 4 -9 3 247.75 37.36 4 -9 3 224.35 26.06 5 -9 3 27.00 13.72 5 -9 3 57.75 21.67 5 -9 3 17.60 10.54 5 -9 3 16.69 12.10 6 -9 3 294.93 28.58 6 -9 3 304.08 29.66 6 -9 3 256.22 35.73 6 -9 3 206.80 35.65 6 -9 3 338.73 39.03 7 -9 3 85.58 23.69 7 -9 3 46.62 14.78 7 -9 3 85.48 20.65 7 -9 3 73.62 12.98 7 -9 3 59.11 15.18 8 -9 3 200.34 32.71 8 -9 3 190.63 27.17 8 -9 3 175.59 32.77 8 -9 3 179.52 29.88 8 -9 3 216.27 30.82 9 -9 3 335.72 35.62 9 -9 3 269.20 33.19 9 -9 3 303.72 32.83 9 -9 3 261.79 31.27 9 -9 3 264.17 33.70 10 -9 3 245.99 31.54 10 -9 3 189.83 28.07 10 -9 3 146.45 26.65 10 -9 3 205.30 30.18 10 -9 3 236.85 27.62 11 -9 3 28.11 16.48 11 -9 3 18.29 15.82 11 -9 3 36.40 15.36 12 -9 3 59.19 14.91 12 -9 3 41.73 15.94 12 -9 3 49.01 15.84 13 -9 3 9.61 13.01 13 -9 3 -1.19 12.07 13 -9 3 20.41 14.84 14 -9 3 85.10 15.25 14 -9 3 86.27 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12.61 15.45 -12 -10 5 26.04 17.29 11 10 -5 249.79 28.94 11 10 -5 252.02 25.87 -11 -10 5 243.67 25.68 10 10 -5 38.52 10.70 10 10 -5 37.98 19.62 10 10 -5 24.67 15.01 -10 -10 5 26.67 14.19 9 10 -5 583.04 46.83 9 10 -5 516.94 51.65 9 10 -5 442.34 46.18 -9 -10 5 590.37 46.08 8 10 -5 12.63 24.59 8 10 -5 15.66 12.39 -8 -10 5 18.82 13.16 7 10 -5 119.03 20.39 7 10 -5 103.57 18.68 7 10 -5 97.11 30.43 -7 -10 5 151.56 27.86 -7 -10 5 123.02 17.86 6 10 -5 0.17 11.35 -6 -10 5 20.77 18.07 -6 -10 5 -0.53 16.07 -6 -10 5 14.45 12.52 5 10 -5 645.66 53.13 -5 -10 5 616.56 52.99 -5 -10 5 621.95 56.06 4 10 -5 4.60 14.63 4 10 -5 -15.40 17.17 -4 -10 5 -3.40 19.82 -4 -10 5 -7.50 12.98 3 10 -5 255.03 26.21 -3 -10 5 223.56 27.18 -3 -10 5 230.10 26.57 2 10 -5 0.22 15.08 -2 -10 5 -3.44 11.77 -2 -10 5 2.10 10.86 -2 -10 5 -14.10 13.26 1 10 -5 282.43 32.18 -1 -10 5 293.25 27.83 -1 -10 5 234.55 26.97 0 -10 5 26.80 11.22 0 -10 5 23.32 16.48 0 -10 5 17.09 9.46 1 -10 5 316.35 28.17 1 -10 5 303.44 29.82 1 -10 5 268.27 39.92 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36.59 2 -7 7 343.81 39.74 3 -7 7 -12.53 28.91 3 -7 7 -33.60 19.09 3 -7 7 4.53 18.53 3 -7 7 50.24 31.72 3 -7 7 0.97 10.59 4 -7 7 281.24 38.67 4 -7 7 401.70 35.61 4 -7 7 313.35 44.90 4 -7 7 332.95 31.70 5 -7 7 27.12 18.43 5 -7 7 7.37 23.21 5 -7 7 -13.72 25.73 5 -7 7 15.07 10.81 6 -7 7 326.28 30.40 6 -7 7 329.56 33.56 6 -7 7 265.93 39.16 7 -7 7 -2.75 32.67 7 -7 7 -18.46 14.37 7 -7 7 -18.45 16.20 8 -7 7 563.75 57.57 8 -7 7 638.93 54.17 8 -7 7 639.01 52.31 9 -7 7 0.88 10.94 9 -7 7 -3.31 19.26 9 -7 7 -19.94 15.42 10 -7 7 22.72 12.37 10 -7 7 17.49 15.11 10 -7 7 17.72 18.85 11 -7 7 -13.01 14.14 11 -7 7 -18.76 13.18 11 -7 7 11.57 18.04 12 -7 7 73.14 18.92 12 -7 7 94.03 15.44 12 -7 7 104.44 17.96 13 -7 7 32.95 12.47 13 -7 7 -5.78 17.14 14 -7 7 60.61 11.67 14 -7 7 60.20 13.25 15 -7 7 16.52 9.30 15 -7 7 6.65 10.31 16 -7 7 36.23 9.72 17 6 -7 87.48 16.14 17 6 -7 118.83 20.32 16 6 -7 0.40 9.86 16 6 -7 -7.07 13.95 15 6 -7 210.67 22.05 15 6 -7 183.58 23.25 -15 -6 7 138.01 37.38 14 6 -7 26.23 10.15 14 6 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12.69 12.49 2 -2 17 15.50 15.16 -3 2 -17 -0.54 11.75 3 -2 17 -5.01 16.74 -4 2 -17 4.43 11.49 4 -2 17 6.35 13.65 4 -2 17 13.00 19.01 -5 2 -17 15.71 11.44 5 -2 17 -3.90 12.42 -6 2 -17 5.99 10.34 6 -2 17 6.72 11.55 -7 2 -17 32.79 10.12 7 -2 17 4.16 10.61 -8 2 -17 26.40 9.59 8 -2 17 2.49 12.63 8 1 -17 13.49 19.44 -8 -1 17 17.34 22.55 7 1 -17 22.18 21.62 -7 -1 17 9.45 15.40 6 1 -17 18.96 23.51 -6 -1 17 6.84 15.28 5 1 -17 -5.61 25.29 -5 -1 17 2.04 14.74 4 1 -17 -15.94 27.19 -4 -1 17 20.42 14.73 3 1 -17 4.97 29.76 -3 -1 17 28.29 14.91 2 1 -17 2.57 33.11 -2 -1 17 11.43 14.26 1 1 -17 5.73 37.21 -1 -1 17 15.09 14.72 0 1 -17 23.91 16.44 0 -1 17 9.33 15.02 -1 1 -17 -6.93 14.47 1 -1 17 12.95 15.18 -2 1 -17 1.55 13.75 2 -1 17 15.79 15.87 2 -1 17 29.47 14.89 -3 1 -17 4.29 12.74 3 -1 17 2.49 16.11 3 -1 17 -17.15 15.23 -4 1 -17 19.14 12.36 4 -1 17 31.06 14.07 4 -1 17 36.78 18.44 -5 1 -17 -3.71 11.02 5 -1 17 23.66 13.42 -6 1 -17 38.01 10.92 6 -1 17 21.12 11.98 6 -1 17 -0.40 11.35 -7 1 -17 1.70 10.32 7 -1 17 14.28 11.37 -8 1 -17 32.80 10.23 8 -1 17 21.49 13.83 8 0 -17 -1.83 18.01 -8 0 17 13.05 22.37 7 0 -17 13.30 19.85 -7 0 17 51.61 18.23 6 0 -17 -30.62 21.09 -6 0 17 30.06 17.31 5 0 -17 14.98 23.12 -5 0 17 38.52 17.14 4 0 -17 16.60 24.88 -4 0 17 12.63 15.97 3 0 -17 7.23 26.72 -3 0 17 6.29 15.66 2 0 -17 27.07 28.53 -2 0 17 14.86 15.62 1 0 -17 11.35 31.31 -1 0 17 26.65 15.55 0 0 -17 -24.95 36.31 0 0 17 7.52 15.68 -1 0 -17 44.94 16.93 1 0 17 39.65 16.10 -2 0 -17 15.71 14.70 2 0 17 2.38 16.27 -3 0 -17 8.50 13.62 3 0 17 -2.79 14.64 3 0 17 36.60 16.62 -4 0 -17 -14.74 12.36 4 0 17 8.03 13.34 4 0 17 -10.08 17.20 -5 0 -17 19.36 11.76 5 0 17 11.52 12.99 -6 0 -17 15.03 11.16 6 0 17 -8.52 12.23 -7 0 -17 -4.38 10.33 7 0 17 -5.37 11.60 7 0 17 23.47 10.93 -8 0 -17 6.55 9.81 8 0 17 4.23 14.85 8 -1 -17 28.51 17.21 -8 1 17 11.07 24.55 7 -1 -17 17.98 18.76 -7 1 17 1.65 21.21 6 -1 -17 36.79 20.13 -6 1 17 -8.76 19.38 5 -1 -17 13.35 21.05 -5 1 17 0.83 18.64 4 -1 -17 -5.55 22.85 -4 1 17 41.36 17.95 3 -1 -17 -31.28 23.92 -3 1 17 13.14 16.97 2 -1 -17 -14.47 26.21 -2 1 17 -15.69 16.40 1 -1 -17 21.38 27.67 -1 1 17 6.62 16.71 0 -1 -17 1.14 30.43 0 1 17 1.95 16.50 -1 -1 -17 58.85 36.63 1 1 17 18.85 16.62 -2 -1 -17 -0.22 16.82 2 1 17 7.06 16.61 -3 -1 -17 18.32 15.21 3 1 17 2.84 15.16 3 1 17 28.55 16.86 -4 -1 -17 15.58 13.80 4 1 17 12.53 13.99 4 1 17 27.16 16.98 -5 -1 -17 0.77 12.74 5 1 17 2.93 13.84 -6 -1 -17 25.32 12.02 6 1 17 12.29 12.90 -7 -1 -17 5.79 10.81 7 1 17 -12.14 12.06 7 1 17 11.46 10.19 8 1 17 12.06 12.77 8 -2 -17 13.16 15.27 8 -2 -17 32.64 16.01 -8 2 17 -42.65 27.36 7 -2 -17 14.56 17.20 7 -2 -17 50.16 26.15 -7 2 17 -13.87 30.81 6 -2 -17 -0.69 18.69 -6 2 17 -19.32 21.92 5 -2 -17 11.93 19.31 -5 2 17 7.48 20.54 4 -2 -17 -22.77 21.10 -4 2 17 5.26 19.47 3 -2 -17 -29.52 21.79 -3 2 17 17.86 18.70 2 -2 -17 26.18 23.46 -2 2 17 -15.43 17.78 1 -2 -17 10.20 25.25 -1 2 17 -0.70 17.41 0 -2 -17 -0.02 27.55 0 2 17 24.86 17.44 -1 -2 -17 27.96 31.23 1 2 17 5.08 17.12 -2 -2 -17 -15.89 34.94 2 2 17 8.89 16.90 3 2 17 -15.48 17.06 3 2 17 14.56 15.70 -4 -2 -17 -17.76 15.53 4 2 17 -7.53 17.49 4 2 17 -1.74 15.11 -5 -2 -17 -1.37 13.81 5 2 17 -14.77 14.32 -6 -2 -17 -4.49 12.76 6 2 17 3.07 10.57 6 2 17 44.21 14.23 7 2 17 27.93 18.64 7 2 17 14.09 9.87 -8 -2 -17 14.21 12.91 8 2 17 -13.84 14.25 8 2 17 -2.72 14.92 8 -3 -17 9.95 16.95 -8 3 17 23.81 34.46 7 -3 -17 11.90 18.46 7 -3 -17 -14.19 17.88 -7 3 17 63.80 31.52 6 -3 -17 6.75 18.63 6 -3 -17 38.89 35.79 -6 3 17 -32.62 26.38 5 -3 -17 -17.26 33.02 5 -3 -17 8.59 19.17 -5 3 17 22.62 23.42 4 -3 -17 21.91 19.33 -4 3 17 39.41 21.97 3 -3 -17 -23.09 20.20 -3 3 17 3.05 20.43 2 -3 -17 -11.80 21.47 -2 3 17 28.18 19.54 1 -3 -17 26.70 23.35 -1 3 17 40.25 19.21 0 -3 -17 23.19 24.84 0 3 17 19.25 18.05 -1 -3 -17 25.42 26.98 1 3 17 -16.83 17.97 -2 -3 -17 -41.80 28.59 2 3 17 27.46 16.13 2 3 17 15.59 17.64 -3 -3 -17 15.54 32.17 3 3 17 -2.04 16.70 3 3 17 -33.72 17.67 4 3 17 36.35 18.20 4 3 17 21.50 16.65 5 3 17 -7.94 15.73 6 3 17 28.88 10.90 6 3 17 28.82 20.66 7 3 17 -5.96 17.96 7 3 17 7.32 9.32 8 3 17 1.98 10.82 8 -4 -17 36.15 17.96 7 -4 -17 32.36 17.03 7 -4 -17 32.14 17.40 -7 4 17 20.31 35.49 6 -4 -17 1.48 17.48 6 -4 -17 10.38 19.85 -6 4 17 24.31 34.20 5 -4 -17 66.93 25.53 -5 4 17 50.77 27.56 4 -4 -17 21.20 18.41 -4 4 17 10.20 24.00 3 -4 -17 31.60 19.03 -3 4 17 45.21 22.66 2 -4 -17 20.51 19.96 -2 4 17 21.55 21.08 1 -4 -17 19.52 21.01 -1 4 17 37.28 20.06 0 -4 -17 7.99 21.47 0 4 17 7.96 19.31 -1 -4 -17 22.44 23.51 1 4 17 5.00 18.41 -2 -4 -17 77.57 24.86 2 4 17 -12.26 18.50 2 4 17 -1.97 18.19 -3 -4 -17 8.01 26.50 3 4 17 3.72 18.06 3 4 17 -3.22 17.77 4 4 17 -15.31 18.77 5 4 17 45.56 23.35 6 4 17 20.00 25.12 6 4 17 8.47 10.42 7 4 17 -8.74 9.00 8 4 17 8.06 14.98 7 -5 -17 -4.95 15.78 6 -5 -17 16.71 20.85 6 -5 -17 13.56 16.29 -6 5 17 -42.69 36.63 5 -5 -17 8.12 16.85 -5 5 17 -45.72 35.95 4 -5 -17 17.30 17.17 -4 5 17 23.25 27.73 3 -5 -17 14.47 17.82 -3 5 17 -10.49 24.24 2 -5 -17 4.37 17.78 -2 5 17 7.74 22.90 1 -5 -17 20.71 18.72 -1 5 17 -5.85 21.34 0 -5 -17 0.90 19.68 0 5 17 22.84 20.42 -1 -5 -17 0.33 20.40 1 5 17 -2.81 19.85 1 5 17 -0.88 20.11 -2 -5 -17 -3.85 21.30 2 5 17 30.14 20.93 2 5 17 48.24 19.52 -3 -5 -17 14.64 23.49 3 5 17 15.11 31.46 3 5 17 -19.37 17.91 -4 -5 -17 -23.42 24.88 -5 -5 -17 -9.58 37.52 5 5 17 -5.67 10.43 6 5 17 -5.61 9.83 7 5 17 0.32 8.77 6 -6 -17 -22.48 15.12 5 -6 -17 -6.45 15.30 -5 6 17 47.43 37.61 4 -6 -17 0.38 15.88 -4 6 17 58.28 35.51 3 -6 -17 29.14 16.32 -3 6 17 -15.17 30.40 2 -6 -17 -14.86 16.53 -2 6 17 6.74 24.72 1 -6 -17 -8.72 16.38 -1 6 17 11.59 22.99 0 -6 -17 -16.98 16.91 0 6 17 26.70 22.04 -1 -6 -17 19.63 17.59 1 6 17 50.05 21.00 1 6 17 13.51 39.83 -2 -6 -17 13.85 18.26 2 6 17 17.04 19.32 -3 -6 -17 18.75 19.67 -4 -6 -17 48.18 21.56 -5 -6 -17 24.27 23.64 5 6 17 -0.23 10.16 -6 -6 -17 2.39 26.02 6 6 17 14.52 9.33 5 -7 -17 -2.89 14.42 -4 7 17 133.86 42.09 3 -7 -17 -9.78 14.39 -3 7 17 25.01 35.51 -2 7 17 92.59 33.53 1 -7 -17 6.46 15.22 -1 7 17 84.91 29.36 0 -7 -17 49.18 15.46 0 7 17 51.92 23.65 -1 -7 -17 0.40 15.17 -2 -7 -17 25.78 16.40 -3 -7 -17 7.71 16.49 4 7 17 10.46 10.54 -5 -7 -17 -5.56 18.60 5 7 17 2.97 9.82 4 -8 -17 -6.40 13.92 3 -8 -17 27.92 13.61 -3 8 17 77.69 48.68 2 -8 -17 14.46 13.68 -2 8 17 -4.04 33.09 1 -8 -17 28.75 13.98 0 -8 -17 10.72 13.61 -1 -8 -17 24.09 13.26 -2 -8 -17 12.36 13.51 2 8 17 -14.28 11.27 -3 -8 -17 4.10 21.25 3 8 17 13.24 10.95 -4 -8 -17 2.37 14.55 4 8 17 13.72 12.37 1 -9 -17 -0.03 15.41 0 -9 -17 1.97 15.18 0 9 17 -6.31 14.55 1 9 17 -12.27 12.82 -2 -6 18 0.26 14.13 1 6 -18 10.01 12.87 -1 -6 18 12.31 13.62 0 6 -18 -20.69 13.42 -1 6 -18 22.45 18.03 1 -6 18 17.52 13.57 2 -6 18 -5.57 12.98 -3 -5 18 -2.50 13.38 -3 -5 18 -4.80 18.61 -3 -5 18 15.99 14.42 -2 -5 18 -0.86 17.28 -2 -5 18 9.57 16.00 -2 -5 18 1.38 16.33 1 5 -18 30.57 15.49 -1 -5 18 -2.25 17.78 -1 -5 18 15.57 16.42 -1 -5 18 9.24 13.81 0 -5 18 -6.83 16.35 0 -5 18 21.24 20.05 0 -5 18 -8.95 11.41 -1 5 -18 -6.73 12.88 1 -5 18 -2.85 11.46 1 -5 18 12.47 16.44 2 -5 18 7.76 16.03 2 -5 18 -10.65 11.46 -3 5 -18 -17.88 15.41 3 -5 18 36.94 15.19 -5 -4 18 9.56 16.22 -4 -4 18 10.00 12.15 -3 -4 18 14.70 12.22 -2 -4 18 -10.98 12.41 -1 -4 18 11.84 13.10 -1 -4 18 2.67 12.91 0 4 -18 11.10 18.79 0 -4 18 -5.09 12.84 0 -4 18 4.46 14.27 -1 4 -18 2.16 12.05 1 -4 18 34.43 17.46 1 -4 18 11.11 11.67 -2 4 -18 2.78 10.92 2 -4 18 12.87 11.53 -3 4 -18 -21.60 10.17 3 -4 18 -2.47 11.05 -4 4 -18 -19.26 11.85 4 -4 18 -11.69 10.16 6 3 -18 9.28 28.17 5 3 -18 89.13 33.20 -5 -3 18 13.64 12.82 -5 -3 18 16.92 12.82 4 3 -18 78.43 49.50 -3 -3 18 18.83 12.51 -2 -3 18 27.12 12.95 -1 -3 18 5.75 13.01 0 3 -18 -5.10 22.14 0 -3 18 -0.09 12.84 0 -3 18 27.59 13.48 -1 3 -18 -15.33 13.15 1 -3 18 -1.73 14.46 1 -3 18 11.23 13.13 -2 3 -18 -10.54 11.99 2 -3 18 15.57 11.47 2 -3 18 21.63 16.83 3 -3 18 12.30 10.91 -4 3 -18 7.71 10.38 4 -3 18 -0.19 10.09 5 -3 18 0.30 10.81 6 2 -18 11.51 24.10 -6 -2 18 -5.07 17.76 5 2 -18 15.05 27.22 -5 -2 18 29.73 13.24 4 2 -18 -42.75 30.77 -4 -2 18 2.62 12.71 3 2 -18 -42.30 36.72 -3 -2 18 -10.68 12.58 -2 -2 18 -11.06 13.19 -1 -2 18 4.10 13.53 0 -2 18 10.20 13.59 -1 2 -18 25.02 15.35 1 -2 18 12.42 14.24 1 -2 18 -5.42 12.20 -2 2 -18 27.64 13.39 2 -2 18 -12.35 11.12 2 -2 18 7.32 14.88 -3 2 -18 9.36 12.03 3 -2 18 2.71 16.55 3 -2 18 3.30 10.86 -4 2 -18 -7.28 11.02 4 -2 18 -10.99 10.28 -5 2 -18 -0.20 13.45 5 -2 18 13.43 10.16 6 1 -18 6.23 21.55 -6 -1 18 21.49 18.13 5 1 -18 17.72 37.80 -5 -1 18 23.41 13.92 4 1 -18 16.95 36.15 -4 -1 18 26.76 13.98 3 1 -18 3.12 34.79 -3 -1 18 -0.97 13.28 2 1 -18 11.93 51.33 -2 -1 18 24.01 13.86 -1 -1 18 13.81 13.69 0 -1 18 42.18 14.40 1 -1 18 2.59 14.20 1 -1 18 11.92 12.73 -2 1 -18 18.72 16.68 2 -1 18 44.09 14.99 -3 1 -18 32.59 13.50 3 -1 18 -11.89 15.24 3 -1 18 -6.18 11.03 -4 1 -18 -6.62 12.75 4 -1 18 -1.65 10.61 5 -1 18 13.64 9.95 -6 1 -18 15.80 14.95 6 0 -18 0.84 33.39 -6 0 18 11.43 19.16 5 0 -18 -17.56 22.53 -5 0 18 54.96 15.84 4 0 -18 -17.71 22.80 3 0 -18 -24.14 25.14 -3 0 18 3.23 14.60 2 0 -18 -21.72 27.41 -2 0 18 -18.57 14.17 1 0 -18 -34.55 32.44 0 0 18 26.09 14.46 1 0 18 32.34 12.86 1 0 18 36.56 15.11 2 0 18 -1.19 12.46 2 0 18 -10.35 14.60 3 0 18 12.31 11.54 3 0 18 -19.88 15.13 4 0 18 -4.72 11.13 5 0 18 -4.94 11.19 -6 0 -18 -18.46 11.88 6 0 18 -0.25 12.80 6 -1 -18 17.73 27.25 -6 1 18 37.68 19.98 5 -1 -18 2.20 19.10 -5 1 18 56.82 19.23 4 -1 -18 54.91 21.26 -4 1 18 36.41 16.93 3 -1 -18 -4.94 22.14 -3 1 18 15.82 15.73 2 -1 -18 12.70 24.23 -2 1 18 19.76 15.42 1 -1 -18 54.96 27.39 -1 1 18 36.29 15.43 0 -1 -18 15.97 32.00 0 1 18 39.05 14.99 1 1 18 -6.06 12.15 1 1 18 -14.61 14.60 2 1 18 23.70 15.17 2 1 18 1.79 12.97 3 1 18 8.71 14.89 3 1 18 6.68 11.95 4 1 18 -5.36 11.70 5 1 18 6.16 13.32 6 -2 -18 10.44 21.26 5 -2 -18 -28.59 17.49 -5 2 18 5.55 22.86 4 -2 -18 -14.60 18.77 -4 2 18 17.74 18.68 3 -2 -18 28.30 20.25 -3 2 18 14.60 17.23 2 -2 -18 10.41 21.69 -2 2 18 -6.72 16.25 1 -2 -18 28.47 24.13 -1 2 18 3.84 15.89 0 -2 -18 10.77 26.26 0 2 18 15.80 15.36 -1 -2 -18 6.07 32.91 1 2 18 -12.72 12.80 1 2 18 28.43 14.74 2 2 18 -1.19 13.63 2 2 18 -2.84 15.27 3 2 18 0.23 12.63 3 2 18 -4.24 15.27 4 2 18 -32.08 16.56 5 2 18 8.59 9.24 5 2 18 39.84 12.75 6 2 18 6.08 10.68 5 -3 -18 1.45 16.59 -5 3 18 -18.33 22.64 4 -3 -18 -14.83 17.25 -4 3 18 -29.20 24.03 3 -3 -18 36.47 18.64 -3 3 18 -10.41 18.78 2 -3 -18 6.75 19.81 -2 3 18 18.29 17.78 1 -3 -18 -27.33 21.03 -1 3 18 23.19 17.05 0 -3 -18 -0.43 22.84 0 3 18 32.77 16.32 -1 -3 -18 -25.55 24.36 1 3 18 19.00 15.51 1 3 18 -25.24 13.70 -2 -3 -18 90.16 41.49 2 3 18 -0.97 15.66 2 3 18 11.42 14.17 -3 -3 -18 31.62 44.91 3 3 18 2.58 14.59 3 3 18 11.57 18.50 4 3 18 -7.12 14.59 5 3 18 -27.58 15.03 6 3 18 16.27 13.66 5 -4 -18 4.51 17.04 4 -4 -18 -16.79 15.93 -4 4 18 7.10 24.01 3 -4 -18 18.20 16.77 -3 4 18 -13.65 26.40 2 -4 -18 -3.18 17.74 -2 4 18 2.78 19.72 1 -4 -18 -3.97 18.63 -1 4 18 27.41 18.24 0 -4 -18 -33.88 19.58 0 4 18 1.80 17.16 0 4 18 -15.27 19.22 -1 -4 -18 -10.25 21.17 1 4 18 -17.65 16.23 1 4 18 -6.23 17.37 2 4 18 -18.03 15.69 2 4 18 -6.81 16.86 3 4 18 0.13 17.38 4 4 18 12.44 18.80 5 4 18 12.01 8.84 3 -5 -18 -3.06 15.23 -3 5 18 4.43 24.01 2 -5 -18 -8.40 15.95 -2 5 18 17.56 24.86 1 -5 -18 -10.61 16.49 -1 5 18 -31.82 23.34 0 -5 -18 10.36 16.85 0 5 18 0.29 19.53 0 5 18 -27.88 19.09 -1 -5 -18 2.32 22.30 1 5 18 4.39 17.58 1 5 18 16.02 20.80 -3 -5 -18 -7.20 21.02 -4 -5 -18 23.18 24.66 4 5 18 -13.01 8.94 3 -6 -18 4.96 18.76 2 -6 -18 -27.86 14.86 1 -6 -18 -6.76 15.72 -1 6 18 59.93 26.56 0 -6 -18 -22.55 21.44 0 6 18 47.15 22.54 -1 -6 -18 13.29 20.00 -2 -6 -18 -20.77 16.10 -3 -6 -18 8.88 18.14 3 6 18 3.45 9.85 3 0 -19 79.50 26.55 2 0 -19 65.33 29.91 0 0 19 4.19 18.17 2 -1 -19 12.38 24.40 1 -1 -19 58.92 28.79 2 -2 -19 -20.27 20.88 1 -2 -19 39.89 22.86 0 -2 -19 -19.45 25.27 -1 -2 -19 -19.99 41.51 0 -3 -19 1.38 21.53 0 0 0 0.00 0.00 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7526 _exptl_absorpt_correction_T_min 0.4869 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54184 16.630 16.631 16.195 89.913 90.059 90.049 ) _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 12591 _shelx_fab_file ; 0 1 0 -10.26 0.00 1 1 0 -60.31 0.00 0 2 0 87.95 0.00 1 2 0 -38.78 0.00 2 2 0 -35.13 0.00 0 3 0 -18.13 0.00 1 3 0 16.47 0.00 2 3 0 22.41 0.00 3 3 0 40.22 0.00 0 4 0 79.88 0.00 1 4 0 3.54 0.00 2 4 0 -1.79 0.00 3 4 0 18.24 0.00 4 4 0 34.48 0.00 0 5 0 10.48 0.00 1 5 0 0.30 0.00 2 5 0 -13.09 0.00 3 5 0 -13.71 0.00 4 5 0 -0.95 0.00 5 5 0 -25.85 0.00 0 6 0 4.36 0.00 1 6 0 -3.20 0.00 2 6 0 -13.87 0.00 3 6 0 8.08 0.00 4 6 0 -6.99 0.00 5 6 0 -7.38 0.00 6 6 0 -22.59 0.00 0 7 0 -0.52 0.00 1 7 0 -2.10 0.00 2 7 0 -4.81 0.00 3 7 0 -0.66 0.00 4 7 0 12.72 0.00 5 7 0 -8.37 0.00 6 7 0 3.53 0.00 7 7 0 -3.90 0.00 0 8 0 5.76 0.00 1 8 0 -2.23 0.00 2 8 0 -16.94 0.00 3 8 0 -3.03 0.00 4 8 0 1.05 0.00 5 8 0 -6.97 0.00 6 8 0 -13.00 0.00 7 8 0 -1.08 0.00 8 8 0 -1.73 0.00 0 9 0 3.19 0.00 1 9 0 1.51 0.00 2 9 0 -1.53 0.00 3 9 0 -5.15 0.00 4 9 0 0.41 0.00 5 9 0 -10.39 0.00 6 9 0 0.04 0.00 7 9 0 -5.84 0.00 8 9 0 0.04 0.00 9 9 0 -11.14 0.00 0 10 0 -2.73 0.00 1 10 0 -1.67 0.00 2 10 0 -3.88 0.00 3 10 0 3.57 0.00 4 10 0 -2.07 0.00 5 10 0 0.58 0.00 6 10 0 -5.55 0.00 7 10 0 -0.30 0.00 8 10 0 -3.90 0.00 9 10 0 -1.86 0.00 10 10 0 -4.18 0.00 0 11 0 0.09 0.00 1 11 0 9.45 0.00 2 11 0 0.35 0.00 3 11 0 5.71 0.00 4 11 0 2.37 0.00 5 11 0 -0.23 0.00 6 11 0 -2.29 0.00 7 11 0 1.21 0.00 8 11 0 2.89 0.00 9 11 0 -1.81 0.00 10 11 0 -1.68 0.00 11 11 0 2.98 0.00 0 12 0 13.90 0.00 1 12 0 0.08 0.00 2 12 0 0.05 0.00 3 12 0 0.21 0.00 4 12 0 3.78 0.00 5 12 0 -0.29 0.00 6 12 0 -0.95 0.00 7 12 0 -0.13 0.00 8 12 0 1.85 0.00 9 12 0 -0.65 0.00 10 12 0 -1.81 0.00 11 12 0 -1.80 0.00 12 12 0 2.12 0.00 0 13 0 -3.02 0.00 1 13 0 4.51 0.00 2 13 0 -3.84 0.00 3 13 0 1.02 0.00 4 13 0 0.23 0.00 5 13 0 -0.68 0.00 6 13 0 -0.95 0.00 7 13 0 0.08 0.00 8 13 0 -0.01 0.00 9 13 0 -1.56 0.00 10 13 0 -1.55 0.00 11 13 0 0.70 0.00 12 13 0 -1.17 0.00 13 13 0 -0.66 0.00 0 14 0 4.95 0.00 1 14 0 -1.15 0.00 2 14 0 2.68 0.00 3 14 0 -2.43 0.00 4 14 0 1.79 0.00 5 14 0 -1.72 0.00 6 14 0 -0.08 0.00 7 14 0 -0.85 0.00 8 14 0 1.31 0.00 9 14 0 1.23 0.00 10 14 0 1.30 0.00 11 14 0 0.35 0.00 12 14 0 1.58 0.00 13 14 0 1.43 0.00 0 15 0 0.72 0.00 1 15 0 5.73 0.00 2 15 0 1.29 0.00 3 15 0 4.52 0.00 4 15 0 -0.09 0.00 5 15 0 4.10 0.00 6 15 0 -1.28 0.00 7 15 0 5.98 0.00 8 15 0 -0.31 0.00 9 15 0 1.23 0.00 10 15 0 -1.81 0.00 11 15 0 3.32 0.00 12 15 0 -2.05 0.00 0 16 0 7.40 0.00 1 16 0 0.46 0.00 2 16 0 1.98 0.00 3 16 0 1.04 0.00 4 16 0 4.44 0.00 5 16 0 2.24 0.00 6 16 0 -0.88 0.00 7 16 0 0.15 0.00 8 16 0 1.02 0.00 9 16 0 2.10 0.00 10 16 0 0.12 0.00 11 16 0 0.32 0.00 0 17 0 1.66 0.00 1 17 0 -0.10 0.00 2 17 0 0.24 0.00 3 17 0 0.32 0.00 4 17 0 -2.42 0.00 5 17 0 -0.87 0.00 6 17 0 -2.23 0.00 7 17 0 0.37 0.00 8 17 0 -1.49 0.00 9 17 0 -0.71 0.00 0 18 0 3.63 0.00 1 18 0 -1.07 0.00 2 18 0 -0.52 0.00 3 18 0 -1.92 0.00 4 18 0 0.29 0.00 5 18 0 1.57 0.00 6 18 0 1.20 0.00 7 18 0 0.05 0.00 0 19 0 1.57 0.00 1 19 0 1.26 0.00 2 19 0 -1.44 0.00 3 19 0 1.54 0.00 4 19 0 0.73 0.00 0 0 1 313.67 0.00 0 1 1 0.82 0.00 1 1 1 97.81 0.00 0 2 1 -34.79 0.00 1 2 1 29.46 0.00 2 2 1 55.66 0.00 0 3 1 -73.50 0.00 1 3 1 16.16 0.00 2 3 1 1.75 0.00 3 3 1 12.49 0.00 0 4 1 16.96 0.00 1 4 1 19.61 0.00 2 4 1 10.65 0.00 3 4 1 -8.85 0.00 4 4 1 -1.24 0.00 0 5 1 -7.17 0.00 1 5 1 8.79 0.00 2 5 1 7.28 0.00 3 5 1 -1.40 0.00 4 5 1 0.85 0.00 5 5 1 -7.05 0.00 0 6 1 -8.43 0.00 1 6 1 2.08 0.00 2 6 1 3.86 0.00 3 6 1 -0.48 0.00 4 6 1 -9.12 0.00 5 6 1 9.45 0.00 6 6 1 -7.12 0.00 0 7 1 -6.17 0.00 1 7 1 -1.07 0.00 2 7 1 1.20 0.00 3 7 1 -7.89 0.00 4 7 1 1.78 0.00 5 7 1 -6.72 0.00 6 7 1 -1.85 0.00 7 7 1 -11.12 0.00 0 8 1 1.74 0.00 1 8 1 -2.11 0.00 2 8 1 -3.48 0.00 3 8 1 -2.06 0.00 4 8 1 -4.94 0.00 5 8 1 2.11 0.00 6 8 1 -8.26 0.00 7 8 1 -3.23 0.00 8 8 1 -6.97 0.00 0 9 1 -1.69 0.00 1 9 1 -3.73 0.00 2 9 1 2.64 0.00 3 9 1 -6.75 0.00 4 9 1 -2.06 0.00 5 9 1 -6.31 0.00 6 9 1 2.44 0.00 7 9 1 -8.66 0.00 8 9 1 -0.14 0.00 9 9 1 -6.32 0.00 0 10 1 1.39 0.00 1 10 1 1.34 0.00 2 10 1 4.33 0.00 3 10 1 0.14 0.00 4 10 1 -3.77 0.00 5 10 1 0.14 0.00 6 10 1 -0.33 0.00 7 10 1 -1.10 0.00 8 10 1 -4.17 0.00 9 10 1 0.88 0.00 10 10 1 -3.08 0.00 0 11 1 1.02 0.00 1 11 1 1.97 0.00 2 11 1 2.22 0.00 3 11 1 0.72 0.00 4 11 1 0.62 0.00 5 11 1 0.00 0.00 6 11 1 1.24 0.00 7 11 1 -1.37 0.00 8 11 1 -0.67 0.00 9 11 1 -0.74 0.00 10 11 1 0.12 0.00 11 11 1 1.98 0.00 0 12 1 6.69 0.00 1 12 1 -3.38 0.00 2 12 1 1.09 0.00 3 12 1 -2.37 0.00 4 12 1 0.88 0.00 5 12 1 -2.05 0.00 6 12 1 -1.09 0.00 7 12 1 -2.81 0.00 8 12 1 -0.76 0.00 9 12 1 -0.23 0.00 10 12 1 -1.53 0.00 11 12 1 -0.30 0.00 12 12 1 -0.14 0.00 0 13 1 -0.09 0.00 1 13 1 2.88 0.00 2 13 1 -1.46 0.00 3 13 1 1.32 0.00 4 13 1 -0.44 0.00 5 13 1 1.03 0.00 6 13 1 1.38 0.00 7 13 1 -0.65 0.00 8 13 1 0.71 0.00 9 13 1 0.53 0.00 10 13 1 -0.75 0.00 11 13 1 0.16 0.00 12 13 1 -0.90 0.00 13 13 1 1.69 0.00 0 14 1 4.78 0.00 1 14 1 1.51 0.00 2 14 1 5.04 0.00 3 14 1 -1.48 0.00 4 14 1 1.87 0.00 5 14 1 -1.37 0.00 6 14 1 1.92 0.00 7 14 1 -0.05 0.00 8 14 1 -0.42 0.00 9 14 1 1.17 0.00 10 14 1 1.18 0.00 11 14 1 0.79 0.00 12 14 1 0.09 0.00 13 14 1 2.16 0.00 0 15 1 -0.90 0.00 1 15 1 3.47 0.00 2 15 1 1.32 0.00 3 15 1 2.44 0.00 4 15 1 0.99 0.00 5 15 1 1.61 0.00 6 15 1 0.34 0.00 7 15 1 1.45 0.00 8 15 1 0.42 0.00 9 15 1 1.01 0.00 10 15 1 -1.00 0.00 11 15 1 1.61 0.00 12 15 1 -1.36 0.00 0 16 1 1.39 0.00 1 16 1 0.96 0.00 2 16 1 0.91 0.00 3 16 1 -1.08 0.00 4 16 1 2.01 0.00 5 16 1 0.35 0.00 6 16 1 -0.23 0.00 7 16 1 0.20 0.00 8 16 1 0.98 0.00 9 16 1 1.12 0.00 10 16 1 -0.10 0.00 11 16 1 0.32 0.00 0 17 1 -0.56 0.00 1 17 1 2.80 0.00 2 17 1 0.99 0.00 3 17 1 1.04 0.00 4 17 1 -0.88 0.00 5 17 1 0.84 0.00 6 17 1 -0.89 0.00 7 17 1 0.32 0.00 8 17 1 1.70 0.00 9 17 1 0.31 0.00 0 18 1 0.86 0.00 1 18 1 1.33 0.00 2 18 1 1.86 0.00 3 18 1 0.04 0.00 4 18 1 0.44 0.00 5 18 1 0.62 0.00 6 18 1 0.02 0.00 7 18 1 -2.56 0.00 0 19 1 0.04 0.00 1 19 1 0.26 0.00 2 19 1 -1.74 0.00 3 19 1 0.03 0.00 4 19 1 0.47 0.00 0 0 2 -164.10 0.00 0 1 2 37.76 0.00 1 1 2 -19.91 0.00 0 2 2 12.57 0.00 1 2 2 8.31 0.00 2 2 2 93.81 0.00 0 3 2 20.18 0.00 1 3 2 5.98 0.00 2 3 2 4.77 0.00 3 3 2 19.33 0.00 0 4 2 -0.06 0.00 1 4 2 -11.95 0.00 2 4 2 0.50 0.00 3 4 2 -9.61 0.00 4 4 2 -15.53 0.00 0 5 2 6.58 0.00 1 5 2 -11.45 0.00 2 5 2 -0.79 0.00 3 5 2 7.16 0.00 4 5 2 -5.82 0.00 5 5 2 -2.65 0.00 0 6 2 10.19 0.00 1 6 2 0.20 0.00 2 6 2 11.65 0.00 3 6 2 4.87 0.00 4 6 2 -1.53 0.00 5 6 2 16.14 0.00 6 6 2 6.80 0.00 0 7 2 10.24 0.00 1 7 2 -0.84 0.00 2 7 2 -0.54 0.00 3 7 2 -0.20 0.00 4 7 2 4.81 0.00 5 7 2 -2.54 0.00 6 7 2 -0.79 0.00 7 7 2 -8.23 0.00 0 8 2 1.83 0.00 1 8 2 -4.13 0.00 2 8 2 -3.73 0.00 3 8 2 1.44 0.00 4 8 2 -5.88 0.00 5 8 2 -1.42 0.00 6 8 2 -4.69 0.00 7 8 2 -0.22 0.00 8 8 2 -9.77 0.00 0 9 2 0.78 0.00 1 9 2 0.69 0.00 2 9 2 -1.16 0.00 3 9 2 0.74 0.00 4 9 2 0.79 0.00 5 9 2 -1.57 0.00 6 9 2 -1.27 0.00 7 9 2 -2.79 0.00 8 9 2 -2.57 0.00 9 9 2 -1.30 0.00 0 10 2 -2.57 0.00 1 10 2 2.90 0.00 2 10 2 1.76 0.00 3 10 2 -1.22 0.00 4 10 2 -2.00 0.00 5 10 2 -2.13 0.00 6 10 2 0.50 0.00 7 10 2 1.44 0.00 8 10 2 -2.69 0.00 9 10 2 -0.49 0.00 10 10 2 2.79 0.00 0 11 2 -0.40 0.00 1 11 2 0.00 0.00 2 11 2 -2.20 0.00 3 11 2 -2.52 0.00 4 11 2 0.88 0.00 5 11 2 -1.52 0.00 6 11 2 -0.47 0.00 7 11 2 -1.82 0.00 8 11 2 -2.56 0.00 9 11 2 -2.27 0.00 10 11 2 1.58 0.00 11 11 2 -0.43 0.00 0 12 2 -3.33 0.00 1 12 2 -0.92 0.00 2 12 2 -0.39 0.00 3 12 2 -1.31 0.00 4 12 2 -0.49 0.00 5 12 2 -0.80 0.00 6 12 2 -0.60 0.00 7 12 2 -0.42 0.00 8 12 2 -1.82 0.00 9 12 2 -0.09 0.00 10 12 2 0.70 0.00 11 12 2 2.55 0.00 12 12 2 -0.94 0.00 0 13 2 -0.81 0.00 1 13 2 4.26 0.00 2 13 2 -2.46 0.00 3 13 2 2.40 0.00 4 13 2 -0.75 0.00 5 13 2 1.40 0.00 6 13 2 -1.06 0.00 7 13 2 0.78 0.00 8 13 2 -1.46 0.00 9 13 2 2.08 0.00 10 13 2 -1.96 0.00 11 13 2 0.53 0.00 12 13 2 -2.11 0.00 13 13 2 1.64 0.00 0 14 2 0.63 0.00 1 14 2 0.51 0.00 2 14 2 2.13 0.00 3 14 2 -1.84 0.00 4 14 2 0.05 0.00 5 14 2 -2.14 0.00 6 14 2 2.32 0.00 7 14 2 0.55 0.00 8 14 2 -1.37 0.00 9 14 2 -1.03 0.00 10 14 2 2.19 0.00 11 14 2 0.52 0.00 12 14 2 2.07 0.00 13 14 2 -0.13 0.00 0 15 2 0.21 0.00 1 15 2 -0.03 0.00 2 15 2 -0.55 0.00 3 15 2 1.36 0.00 4 15 2 2.18 0.00 5 15 2 -0.32 0.00 6 15 2 1.52 0.00 7 15 2 -0.78 0.00 8 15 2 1.18 0.00 9 15 2 -0.03 0.00 10 15 2 1.08 0.00 11 15 2 -1.33 0.00 12 15 2 1.30 0.00 0 16 2 2.49 0.00 1 16 2 -0.51 0.00 2 16 2 3.56 0.00 3 16 2 -1.00 0.00 4 16 2 0.72 0.00 5 16 2 -2.41 0.00 6 16 2 1.08 0.00 7 16 2 1.00 0.00 8 16 2 0.19 0.00 9 16 2 0.51 0.00 10 16 2 1.01 0.00 11 16 2 -0.91 0.00 0 17 2 0.76 0.00 1 17 2 2.48 0.00 2 17 2 0.09 0.00 3 17 2 2.58 0.00 4 17 2 0.45 0.00 5 17 2 2.18 0.00 6 17 2 -1.17 0.00 7 17 2 0.13 0.00 8 17 2 0.22 0.00 9 17 2 2.19 0.00 0 18 2 -0.95 0.00 1 18 2 -0.92 0.00 2 18 2 1.95 0.00 3 18 2 0.12 0.00 4 18 2 0.34 0.00 5 18 2 -0.70 0.00 6 18 2 0.61 0.00 7 18 2 -0.83 0.00 0 19 2 1.64 0.00 1 19 2 -0.17 0.00 2 19 2 -0.83 0.00 3 19 2 0.70 0.00 4 19 2 0.15 0.00 0 0 3 -22.54 0.00 0 1 3 -22.18 0.00 1 1 3 -8.34 0.00 0 2 3 -5.45 0.00 1 2 3 -3.38 0.00 2 2 3 -39.17 0.00 0 3 3 5.92 0.00 1 3 3 27.20 0.00 2 3 3 -6.26 0.00 3 3 3 -1.77 0.00 0 4 3 -1.54 0.00 1 4 3 12.13 0.00 2 4 3 -8.39 0.00 3 4 3 7.24 0.00 4 4 3 13.93 0.00 0 5 3 -5.29 0.00 1 5 3 1.66 0.00 2 5 3 -7.61 0.00 3 5 3 -2.18 0.00 4 5 3 1.17 0.00 5 5 3 0.53 0.00 0 6 3 -10.05 0.00 1 6 3 -3.14 0.00 2 6 3 -3.53 0.00 3 6 3 -7.11 0.00 4 6 3 3.29 0.00 5 6 3 7.74 0.00 6 6 3 0.69 0.00 0 7 3 4.89 0.00 1 7 3 5.03 0.00 2 7 3 0.45 0.00 3 7 3 -2.25 0.00 4 7 3 8.65 0.00 5 7 3 0.52 0.00 6 7 3 1.13 0.00 7 7 3 -3.78 0.00 0 8 3 0.50 0.00 1 8 3 8.15 0.00 2 8 3 -1.98 0.00 3 8 3 5.84 0.00 4 8 3 2.80 0.00 5 8 3 1.86 0.00 6 8 3 -0.44 0.00 7 8 3 5.28 0.00 8 8 3 2.26 0.00 0 9 3 -3.50 0.00 1 9 3 0.90 0.00 2 9 3 -3.86 0.00 3 9 3 1.42 0.00 4 9 3 -0.10 0.00 5 9 3 1.74 0.00 6 9 3 -2.01 0.00 7 9 3 0.15 0.00 8 9 3 0.93 0.00 9 9 3 2.46 0.00 0 10 3 -0.95 0.00 1 10 3 -1.03 0.00 2 10 3 1.53 0.00 3 10 3 0.04 0.00 4 10 3 -0.58 0.00 5 10 3 -0.86 0.00 6 10 3 -0.88 0.00 7 10 3 -1.75 0.00 8 10 3 -0.98 0.00 9 10 3 -1.98 0.00 10 10 3 -0.13 0.00 0 11 3 1.15 0.00 1 11 3 -1.43 0.00 2 11 3 -0.14 0.00 3 11 3 -1.43 0.00 4 11 3 2.66 0.00 5 11 3 0.21 0.00 6 11 3 0.24 0.00 7 11 3 -2.12 0.00 8 11 3 3.15 0.00 9 11 3 -0.03 0.00 10 11 3 0.43 0.00 11 11 3 -2.74 0.00 0 12 3 -0.02 0.00 1 12 3 -1.44 0.00 2 12 3 0.83 0.00 3 12 3 0.55 0.00 4 12 3 -1.63 0.00 5 12 3 0.18 0.00 6 12 3 -0.57 0.00 7 12 3 -0.37 0.00 8 12 3 -0.50 0.00 9 12 3 -0.39 0.00 10 12 3 -0.51 0.00 11 12 3 1.77 0.00 12 12 3 2.09 0.00 0 13 3 -2.28 0.00 1 13 3 0.28 0.00 2 13 3 -2.75 0.00 3 13 3 -2.81 0.00 4 13 3 -0.35 0.00 5 13 3 -0.24 0.00 6 13 3 -1.86 0.00 7 13 3 0.25 0.00 8 13 3 -1.60 0.00 9 13 3 2.43 0.00 10 13 3 -1.76 0.00 11 13 3 0.77 0.00 12 13 3 -1.42 0.00 13 13 3 2.79 0.00 0 14 3 -0.16 0.00 1 14 3 -3.42 0.00 2 14 3 -0.57 0.00 3 14 3 -2.26 0.00 4 14 3 0.15 0.00 5 14 3 -1.01 0.00 6 14 3 1.54 0.00 7 14 3 0.46 0.00 8 14 3 2.01 0.00 9 14 3 -1.09 0.00 10 14 3 -0.79 0.00 11 14 3 -0.78 0.00 12 14 3 1.38 0.00 13 14 3 -1.68 0.00 0 15 3 2.07 0.00 1 15 3 0.41 0.00 2 15 3 -0.94 0.00 3 15 3 0.39 0.00 4 15 3 1.53 0.00 5 15 3 -0.27 0.00 6 15 3 -0.99 0.00 7 15 3 -0.58 0.00 8 15 3 0.24 0.00 9 15 3 0.16 0.00 10 15 3 -0.48 0.00 11 15 3 0.90 0.00 12 15 3 -0.94 0.00 0 16 3 3.61 0.00 1 16 3 -2.21 0.00 2 16 3 2.57 0.00 3 16 3 -1.00 0.00 4 16 3 1.14 0.00 5 16 3 -1.26 0.00 6 16 3 1.02 0.00 7 16 3 0.22 0.00 8 16 3 -0.50 0.00 9 16 3 0.68 0.00 10 16 3 0.79 0.00 0 17 3 0.21 0.00 1 17 3 0.43 0.00 2 17 3 -2.51 0.00 3 17 3 1.09 0.00 4 17 3 -1.38 0.00 5 17 3 1.33 0.00 6 17 3 -0.35 0.00 7 17 3 0.14 0.00 8 17 3 0.36 0.00 9 17 3 1.67 0.00 0 18 3 -0.52 0.00 1 18 3 -1.24 0.00 2 18 3 -0.92 0.00 3 18 3 -0.56 0.00 4 18 3 -0.39 0.00 5 18 3 -0.53 0.00 6 18 3 1.22 0.00 7 18 3 0.58 0.00 0 19 3 1.74 0.00 1 19 3 0.34 0.00 2 19 3 -0.21 0.00 3 19 3 0.62 0.00 0 0 4 67.36 0.00 0 1 4 -53.33 0.00 1 1 4 12.81 0.00 0 2 4 -12.39 0.00 1 2 4 6.31 0.00 2 2 4 -14.84 0.00 0 3 4 -22.03 0.00 1 3 4 -8.44 0.00 2 3 4 -7.39 0.00 3 3 4 -13.28 0.00 0 4 4 -3.30 0.00 1 4 4 -2.02 0.00 2 4 4 -1.28 0.00 3 4 4 -6.03 0.00 4 4 4 -2.14 0.00 0 5 4 -0.01 0.00 1 5 4 -1.88 0.00 2 5 4 5.50 0.00 3 5 4 2.95 0.00 4 5 4 1.54 0.00 5 5 4 2.90 0.00 0 6 4 0.03 0.00 1 6 4 -4.18 0.00 2 6 4 2.41 0.00 3 6 4 -1.39 0.00 4 6 4 -3.12 0.00 5 6 4 7.73 0.00 6 6 4 4.25 0.00 0 7 4 -2.02 0.00 1 7 4 -7.64 0.00 2 7 4 0.50 0.00 3 7 4 -4.32 0.00 4 7 4 -1.01 0.00 5 7 4 -3.54 0.00 6 7 4 4.53 0.00 7 7 4 1.11 0.00 0 8 4 2.96 0.00 1 8 4 0.76 0.00 2 8 4 0.57 0.00 3 8 4 4.61 0.00 4 8 4 -1.94 0.00 5 8 4 5.13 0.00 6 8 4 0.01 0.00 7 8 4 6.06 0.00 8 8 4 3.31 0.00 0 9 4 0.85 0.00 1 9 4 1.06 0.00 2 9 4 5.63 0.00 3 9 4 1.84 0.00 4 9 4 4.67 0.00 5 9 4 1.94 0.00 6 9 4 7.74 0.00 7 9 4 0.91 0.00 8 9 4 3.61 0.00 9 9 4 2.58 0.00 0 10 4 1.29 0.00 1 10 4 -1.29 0.00 2 10 4 1.11 0.00 3 10 4 -0.31 0.00 4 10 4 2.17 0.00 5 10 4 2.68 0.00 6 10 4 -1.35 0.00 7 10 4 1.53 0.00 8 10 4 -1.44 0.00 9 10 4 5.60 0.00 10 10 4 -0.91 0.00 0 11 4 -1.42 0.00 1 11 4 0.75 0.00 2 11 4 0.73 0.00 3 11 4 -2.14 0.00 4 11 4 0.30 0.00 5 11 4 -1.30 0.00 6 11 4 -0.36 0.00 7 11 4 0.22 0.00 8 11 4 0.07 0.00 9 11 4 0.40 0.00 10 11 4 -0.27 0.00 11 11 4 -3.68 0.00 0 12 4 -0.51 0.00 1 12 4 -1.92 0.00 2 12 4 -1.72 0.00 3 12 4 0.18 0.00 4 12 4 0.54 0.00 5 12 4 -0.08 0.00 6 12 4 -0.07 0.00 7 12 4 0.51 0.00 8 12 4 1.29 0.00 9 12 4 1.95 0.00 10 12 4 -0.10 0.00 11 12 4 -0.21 0.00 12 12 4 0.42 0.00 0 13 4 -3.17 0.00 1 13 4 -1.07 0.00 2 13 4 -0.65 0.00 3 13 4 -2.55 0.00 4 13 4 0.62 0.00 5 13 4 -2.38 0.00 6 13 4 1.80 0.00 7 13 4 -0.65 0.00 8 13 4 0.93 0.00 9 13 4 0.48 0.00 10 13 4 1.12 0.00 11 13 4 -2.07 0.00 12 13 4 1.00 0.00 13 13 4 0.16 0.00 0 14 4 3.35 0.00 1 14 4 -3.47 0.00 2 14 4 -1.47 0.00 3 14 4 0.16 0.00 4 14 4 -1.25 0.00 5 14 4 -0.85 0.00 6 14 4 0.28 0.00 7 14 4 0.27 0.00 8 14 4 0.91 0.00 9 14 4 -0.49 0.00 10 14 4 -2.29 0.00 11 14 4 -1.21 0.00 12 14 4 -1.39 0.00 13 14 4 3.12 0.00 0 15 4 -1.24 0.00 1 15 4 -0.34 0.00 2 15 4 -2.21 0.00 3 15 4 -0.19 0.00 4 15 4 -0.45 0.00 5 15 4 0.21 0.00 6 15 4 -1.06 0.00 7 15 4 -0.16 0.00 8 15 4 0.31 0.00 9 15 4 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1 7 15 4.67 0.00 2 7 15 -1.23 0.00 3 7 15 -0.86 0.00 4 7 15 -3.22 0.00 5 7 15 0.48 0.00 6 7 15 2.29 0.00 7 7 15 -2.38 0.00 0 8 15 2.70 0.00 1 8 15 0.72 0.00 2 8 15 -0.74 0.00 3 8 15 -1.65 0.00 4 8 15 -1.44 0.00 5 8 15 1.52 0.00 6 8 15 3.01 0.00 7 8 15 0.65 0.00 8 8 15 1.42 0.00 0 9 15 2.36 0.00 1 9 15 -5.00 0.00 2 9 15 4.03 0.00 3 9 15 -1.31 0.00 4 9 15 -1.81 0.00 5 9 15 1.66 0.00 6 9 15 4.54 0.00 7 9 15 -4.28 0.00 8 9 15 -0.97 0.00 0 10 15 0.86 0.00 1 10 15 0.47 0.00 2 10 15 -0.10 0.00 3 10 15 0.86 0.00 4 10 15 -0.70 0.00 5 10 15 1.35 0.00 6 10 15 3.45 0.00 7 10 15 -0.03 0.00 0 11 15 -0.13 0.00 1 11 15 -0.44 0.00 2 11 15 -0.32 0.00 3 11 15 2.80 0.00 4 11 15 -0.86 0.00 5 11 15 1.50 0.00 0 12 15 -0.33 0.00 1 12 15 0.38 0.00 2 12 15 -7.21 0.00 0 0 16 -0.29 0.00 0 1 16 0.06 0.00 1 1 16 7.90 0.00 0 2 16 -5.39 0.00 1 2 16 -1.71 0.00 2 2 16 -7.78 0.00 0 3 16 -5.47 0.00 1 3 16 1.47 0.00 2 3 16 -2.22 0.00 3 3 16 -2.47 0.00 0 4 16 8.64 0.00 1 4 16 -1.54 0.00 2 4 16 2.10 0.00 3 4 16 3.51 0.00 4 4 16 3.23 0.00 0 5 16 0.82 0.00 1 5 16 -2.69 0.00 2 5 16 -0.66 0.00 3 5 16 -1.14 0.00 4 5 16 1.64 0.00 5 5 16 -2.60 0.00 0 6 16 -3.74 0.00 1 6 16 1.92 0.00 2 6 16 -1.79 0.00 3 6 16 0.38 0.00 4 6 16 4.54 0.00 5 6 16 0.24 0.00 6 6 16 -0.22 0.00 0 7 16 0.75 0.00 1 7 16 -2.26 0.00 2 7 16 2.78 0.00 3 7 16 -1.62 0.00 4 7 16 0.49 0.00 5 7 16 2.99 0.00 6 7 16 -1.50 0.00 7 7 16 -1.25 0.00 0 8 16 -1.89 0.00 1 8 16 0.56 0.00 2 8 16 -0.61 0.00 3 8 16 -0.18 0.00 4 8 16 0.82 0.00 5 8 16 0.32 0.00 6 8 16 -2.33 0.00 7 8 16 1.29 0.00 0 9 16 1.94 0.00 1 9 16 -3.20 0.00 2 9 16 0.67 0.00 3 9 16 -4.15 0.00 4 9 16 1.05 0.00 5 9 16 1.32 0.00 6 9 16 7.11 0.00 0 10 16 -4.09 0.00 1 10 16 0.82 0.00 2 10 16 -2.05 0.00 3 10 16 -0.04 0.00 4 10 16 0.69 0.00 0 0 17 14.87 0.00 0 1 17 -0.16 0.00 1 1 17 -4.34 0.00 0 2 17 4.54 0.00 1 2 17 -5.94 0.00 2 2 17 5.52 0.00 0 3 17 -3.85 0.00 1 3 17 0.58 0.00 2 3 17 -1.80 0.00 3 3 17 -5.18 0.00 0 4 17 0.71 0.00 1 4 17 -0.35 0.00 2 4 17 -0.95 0.00 3 4 17 3.24 0.00 4 4 17 -3.93 0.00 0 5 17 -0.60 0.00 1 5 17 -0.72 0.00 2 5 17 -2.28 0.00 3 5 17 -0.74 0.00 4 5 17 3.05 0.00 5 5 17 2.86 0.00 0 6 17 0.54 0.00 1 6 17 -0.85 0.00 2 6 17 0.64 0.00 3 6 17 -0.60 0.00 4 6 17 0.05 0.00 5 6 17 1.70 0.00 6 6 17 0.73 0.00 0 7 17 2.17 0.00 1 7 17 1.92 0.00 2 7 17 1.23 0.00 3 7 17 0.33 0.00 4 7 17 2.55 0.00 5 7 17 0.50 0.00 0 8 17 2.33 0.00 1 8 17 3.33 0.00 2 8 17 2.23 0.00 3 8 17 2.85 0.00 4 8 17 4.22 0.00 0 9 17 -6.67 0.00 1 9 17 -3.56 0.00 0 0 18 3.04 0.00 0 1 18 -7.09 0.00 1 1 18 1.43 0.00 0 2 18 -2.66 0.00 1 2 18 -1.16 0.00 2 2 18 -1.14 0.00 0 3 18 3.80 0.00 1 3 18 0.19 0.00 2 3 18 -1.87 0.00 3 3 18 -7.45 0.00 0 4 18 4.01 0.00 1 4 18 -0.19 0.00 2 4 18 3.01 0.00 3 4 18 3.70 0.00 4 4 18 0.23 0.00 0 5 18 1.28 0.00 1 5 18 -5.78 0.00 2 5 18 -1.24 0.00 3 5 18 -4.80 0.00 4 5 18 0.07 0.00 0 6 18 1.11 0.00 1 6 18 -5.37 0.00 2 6 18 2.72 0.00 3 6 18 -1.32 0.00 0 0 19 11.45 0.00 1 1 19 -12.94 0.00 0 2 19 -4.18 0.00 1 2 19 5.21 0.00 2 2 19 -1.03 0.00 0 3 19 10.23 0.00 14 14 0 -0.29 0.00 13 15 0 -1.38 0.00 12 16 0 1.68 0.00 10 17 0 0.39 0.00 8 18 0 -0.44 0.00 5 19 0 -0.35 0.00 6 19 0 -2.06 0.00 0 20 0 0.20 0.00 14 14 1 -2.65 0.00 13 15 1 0.60 0.00 10 17 1 1.41 0.00 8 18 1 -0.30 0.00 5 19 1 -0.25 0.00 6 19 1 0.28 0.00 14 14 2 0.17 0.00 13 15 2 -0.42 0.00 10 17 2 0.45 0.00 8 18 2 1.28 0.00 5 19 2 -0.89 0.00 11 16 3 -0.61 0.00 10 17 3 -0.27 0.00 8 18 3 1.19 0.00 4 19 3 -1.93 0.00 5 19 3 -0.89 0.00 12 15 4 -5.65 0.00 11 16 4 -1.14 0.00 9 17 4 -1.73 0.00 7 18 4 1.36 0.00 3 19 4 -2.62 0.00 4 19 4 -1.57 0.00 13 14 5 3.92 0.00 12 15 5 -4.14 0.00 9 17 5 -3.15 0.00 6 18 5 -1.04 0.00 7 18 5 0.03 0.00 0 19 5 -0.03 0.00 1 19 5 -2.26 0.00 2 19 5 3.95 0.00 3 19 5 -2.42 0.00 11 15 6 1.21 0.00 10 16 6 -0.49 0.00 8 17 6 -2.59 0.00 5 18 6 0.21 0.00 6 18 6 -0.39 0.00 0 19 6 1.04 0.00 1 19 6 -1.41 0.00 13 13 7 -5.36 0.00 12 14 7 5.87 0.00 11 15 7 0.77 0.00 9 16 7 0.01 0.00 7 17 7 -4.06 0.00 4 18 7 0.11 0.00 10 15 8 -4.60 0.00 8 16 8 4.11 0.00 6 17 8 -7.26 0.00 0 18 8 5.46 0.00 1 18 8 -4.28 0.00 2 18 8 3.81 0.00 12 13 9 0.76 0.00 9 15 9 -4.96 0.00 7 16 9 1.11 0.00 4 17 9 5.07 0.00 5 17 9 -1.80 0.00 12 12 10 1.36 0.00 11 13 10 4.59 0.00 8 15 10 1.95 0.00 5 16 10 2.02 0.00 6 16 10 3.71 0.00 0 17 10 3.12 0.00 1 17 10 5.34 0.00 2 17 10 1.79 0.00 11 12 11 2.88 0.00 10 13 11 1.66 0.00 8 14 11 -1.74 0.00 6 15 11 4.73 0.00 1 16 11 -1.86 0.00 2 16 11 -5.41 0.00 3 16 11 5.41 0.00 11 11 12 -0.92 0.00 10 12 12 1.84 0.00 8 13 12 -3.64 0.00 7 14 12 1.61 0.00 3 15 12 -0.23 0.00 4 15 12 1.00 0.00 8 12 13 -3.30 0.00 7 13 13 -4.07 0.00 4 14 13 -4.39 0.00 0 0 14 -19.65 0.00 9 10 14 2.08 0.00 8 11 14 1.84 0.00 6 12 14 -3.33 0.00 4 13 14 -7.01 0.00 6 11 15 -0.61 0.00 3 12 15 -2.13 0.00 4 12 15 -3.49 0.00 5 10 16 -2.17 0.00 0 11 16 0.41 0.00 1 11 16 0.19 0.00 2 11 16 1.77 0.00 6 7 17 -3.46 0.00 5 8 17 0.60 0.00 2 9 17 -7.10 0.00 3 9 17 -4.63 0.00 5 5 18 2.33 0.00 4 6 18 -0.42 0.00 0 7 18 6.49 0.00 1 7 18 8.75 0.00 2 7 18 3.44 0.00 0 1 19 -4.04 0.00 1 3 19 -0.98 0.00 2 3 19 -1.38 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 30118) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 -0.007 -0.007 -0.005 3698 1145 ' ' _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL cu_lp18017P 4/m m m R = 0.15 CELL 16.6421 16.6421 16.1146 90.00 90.00 90.00 SPGR P4/mmm # Solvent Accessible Volume = 3696 # Electrons Found in S.A.V. = 1126 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.500 0.438-0.003 ! 3.98 eA-3 C102 1.000 0.935 0.093 ! 2.91 eA-3 Q103 0.500 0.496 0.438 ! 2.49 eA-3 Q104 1.000 1.007 0.469 ! 2.30 eA-3 C105 0.500 0.766 0.796 ! 2.06 eA-3 C106 1.000 0.271 0.279 ! 1.82 eA-3 Q107 1.000 1.004 0.656 ! 1.62 eA-3 C108 1.000 1.001 0.109 ! 1.59 eA-3 C109 0.739 0.266-0.004 ! 1.55 eA-3 C110 0.500 0.578 0.166 ! 1.49 eA-3 Q111 0.500 0.453 0.508 ! 1.36 eA-3 C112 1.000 0.267 0.114 ! 1.26 eA-3 C113 1.000 0.733 0.352 ! 1.23 eA-3 C114 0.713 0.504 0.266 ! 1.11 eA-3 C115 0.500 0.507 0.031 ! 1.06 eA-3 C116 1.000 1.000 0.000 ! 1.02 eA-3 C117 1.000 0.341 0.463 ! 1.01 eA-3 C118 0.500 1.000 0.500 ! 0.95 eA-3 C119 0.500 0.670 0.249 ! 0.94 eA-3 C120 0.500 0.505 0.125 ! 0.90 eA-3 C121 1.000 0.621 0.589 ! 0.89 eA-3 C122 0.780 0.543 0.261 ! 0.88 eA-3 C123 0.797 0.150 0.112 ! 0.87 eA-3 C124 0.441 1.000 0.500 ! 0.86 eA-3 C125 1.000 0.415 0.473 ! 0.86 eA-3 C126 0.500 1.000 0.000 ! 0.84 eA-3 C127 1.000 0.561 0.552 ! 0.84 eA-3 C128 0.762 0.759 0.106 ! 0.83 eA-3 C129 1.000 0.676 0.677 ! 0.82 eA-3 C130 0.782 0.146 0.080 ! 0.82 eA-3 C131 0.663 0.452 0.736 ! 0.82 eA-3 Q132 0.500 0.250 0.492 ! 0.81 eA-3 C133 0.564 0.156 0.003 ! 0.81 eA-3 C134 0.780 0.172 0.004 ! 0.80 eA-3 C135 0.453 0.502 0.078 ! 0.79 eA-3 C136 0.592 0.436 0.764 ! 0.78 eA-3 C137 0.463 0.510 0.781 ! 0.77 eA-3 C138 0.951 0.336 0.354 ! 0.77 eA-3 Q139 1.000 0.031 0.408 ! 0.75 eA-3 C140 0.109 0.844 0.807 ! 0.75 eA-3 C141 0.610 0.507 0.719 ! 0.75 eA-3 Q142 0.500 0.509 0.344 ! 0.75 eA-3 C143 0.809 0.813 0.028 ! 0.75 eA-3 C144 0.790 0.500 0.000 ! 0.75 eA-3 C145 0.950 0.803 0.730 ! 0.75 eA-3 Q146 1.000 0.921 0.828 ! 0.74 eA-3 C147 1.000 0.906 0.004 ! 0.73 eA-3 C148 0.500 0.834 0.267 ! 0.72 eA-3 Q149 0.939 0.038 0.251 ! 0.72 eA-3 C150 0.532 0.521 0.939 ! 0.72 eA-3 C151 0.965 0.298 0.328 ! 0.71 eA-3 C152 0.967 0.783 0.206 ! 0.71 eA-3 C153 0.198 0.241 0.148 ! 0.71 eA-3 C154 0.947 0.536 0.406 ! 0.71 eA-3 C155 0.761 0.241 0.202 ! 0.71 eA-3 C156 1.000 0.439 0.156 ! 0.70 eA-3 C157 0.048 0.174 0.774 ! 0.70 eA-3 C158 0.468 0.953-0.003 ! 0.69 eA-3 C159 0.189 0.179 0.189 ! 0.68 eA-3 C160 1.000 0.185 0.074 ! 0.67 eA-3 C161 0.921 0.649 0.299 ! 0.67 eA-3 C162 0.500 0.098 0.813 ! 0.66 eA-3 C163 0.199 0.391 0.003 ! 0.66 eA-3 C164 1.000 0.504 0.172 ! 0.66 eA-3 C165 0.500 0.035 0.108 ! 0.66 eA-3 C166 0.831 0.495 0.031 ! 0.66 eA-3 C167 0.261 0.140 0.003 ! 0.64 eA-3 C168 0.703 0.657 0.218 ! 0.64 eA-3 C169 0.708 0.698 0.208 ! 0.64 eA-3 C170 0.893 0.203 0.140 ! 0.64 eA-3 C171 0.879 0.337 0.300 ! 0.63 eA-3 C172 0.936 0.610 0.359 ! 0.63 eA-3 C173 0.500 0.794 0.869 ! 0.63 eA-3 Q174 1.000 0.105 0.218 ! 0.62 eA-3 C175 0.421 0.423 0.312 ! 0.62 eA-3 C176 0.440 0.803 0.324 ! 0.62 eA-3 C177 0.834 0.840 0.928 ! 0.61 eA-3 C178 0.576 0.801 0.216 ! 0.61 eA-3 C179 0.500 0.110 0.252 ! 0.61 eA-3 C180 0.339 0.506 0.109 ! 0.61 eA-3 C181 1.000 0.732 0.187 ! 0.61 eA-3 C182 0.921 0.928 0.077 ! 0.61 eA-3 Q183 1.000 0.998 0.219 ! 0.61 eA-3 C184 0.583 0.158 0.187 ! 0.60 eA-3 C185 0.405 0.640 0.012 ! 0.60 eA-3 C186 0.471 0.086 0.097 ! 0.60 eA-3 C187 0.796 0.495 0.078 ! 0.60 eA-3 C188 0.132 0.464 0.287 ! 0.60 eA-3 C189 0.407 0.179 0.269 ! 0.60 eA-3 C190 0.476 0.139 0.078 ! 0.60 eA-3 C191 0.051 0.421 0.410 ! 0.59 eA-3 C192 0.081 0.338 0.161 ! 0.59 eA-3 C193 0.449 0.448 0.324 ! 0.59 eA-3 C194 0.550 0.560 0.128 ! 0.58 eA-3 C195 0.858 0.224 0.177 ! 0.58 eA-3 C196 0.839 0.870 0.139 ! 0.58 eA-3 C197 0.636 0.688-0.006 ! 0.58 eA-3 C198 0.500 0.245 0.929 ! 0.58 eA-3 C199 0.875 0.375 0.009 ! 0.57 eA-3 ) ; _shelx_fab_checksum 54054