data_007b-19018 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C23 H29 N2, C6 H2 N3 O9 S' _chemical_formula_sum 'C29 H31 N5 O9 S' _chemical_formula_weight 625.65 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.2796(3) _cell_length_b 32.4638(7) _cell_length_c 24.8002(7) _cell_angle_alpha 90 _cell_angle_beta 98.611(3) _cell_angle_gamma 90 _cell_volume 6590.8(3) _cell_formula_units_Z 8 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 25924 _cell_measurement_theta_min 5.5830 _cell_measurement_theta_max 66.6090 _exptl_crystal_description Block _exptl_crystal_colour Colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.261 _exptl_crystal_F_000 2624 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 1.359 _shelx_estimated_absorpt_T_min 0.773 _shelx_estimated_absorpt_T_max 0.876 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.92914 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.16b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 22919 _diffrn_reflns_av_unetI/netI 0.0621 _diffrn_reflns_av_R_equivalents 0.1726 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -38 _diffrn_reflns_limit_k_max 38 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_theta_min 2.258 _diffrn_reflns_theta_max 67.132 _diffrn_reflns_theta_full 67.132 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 0.995 _reflns_number_total 22919 _reflns_number_gt 16141 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; This data was refined as a 2-component twin. The fractional volume contribution of the minor twin component was freely refined to a converged value of 0.3543(10). Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were first found in the difference map, then generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. The program SQUEEZE was used to compensate for the contribution of disordered solvents contained in voids within the crystal lattice from the diffraction intensities. This procedure was applied to the data file and the submitted model is based on the solvent removed data. Based on the total electron density found in the voids (201 e/A^3^), it is likely that ~4 ethyl acetate molecules are present in the unit cell. See "_platon_squeeze_details" in this .cif for more information. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0980P)^2^+3.6432P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 22919 _refine_ls_number_parameters 808 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1007 _refine_ls_R_factor_gt 0.0659 _refine_ls_wR_factor_ref 0.1839 _refine_ls_wR_factor_gt 0.1666 _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_restrained_S_all 1.032 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.79263(12) 0.97158(3) 0.59771(4) 0.0310(2) Uani 1 1 d . . . . . O1 O 0.6879(3) 0.99969(9) 0.62163(11) 0.0325(6) Uani 1 1 d . . . . . O2 O 0.9619(3) 0.97352(10) 0.62083(12) 0.0384(7) Uani 1 1 d . . . . . O3 O 0.7253(3) 0.93043(9) 0.58955(12) 0.0359(7) Uani 1 1 d . . . . . O4 O 0.9806(4) 0.91693(10) 0.52376(13) 0.0408(7) Uani 1 1 d . . . . . O5 O 0.7757(4) 0.89415(10) 0.46715(13) 0.0477(8) Uani 1 1 d . . . . . O6 O 0.6372(4) 1.00049(10) 0.32665(12) 0.0396(7) Uani 1 1 d . . . . . O7 O 0.6054(4) 1.06356(10) 0.35306(13) 0.0413(7) Uani 1 1 d . . . . . O8 O 0.5927(4) 1.07910(10) 0.55787(13) 0.0441(8) Uani 1 1 d . . . . . O9 O 0.8533(4) 1.07001(10) 0.58250(12) 0.0417(7) Uani 1 1 d . . . . . N5 N 0.8535(5) 0.92180(11) 0.49294(15) 0.0362(8) Uani 1 1 d . . . . . N6 N 0.6406(4) 1.02733(11) 0.36179(14) 0.0343(8) Uani 1 1 d . . . . . N7 N 0.7225(5) 1.06161(11) 0.55510(15) 0.0360(8) Uani 1 1 d . . . . . C47 C 0.7780(5) 0.98994(12) 0.52750(17) 0.0297(9) Uani 1 1 d . . . . . C48 C 0.7906(5) 0.96397(13) 0.48357(17) 0.0305(9) Uani 1 1 d . . . . . C49 C 0.7475(5) 0.97550(13) 0.42969(17) 0.0320(9) Uani 1 1 d . . . . . H49 H 0.7576 0.9568 0.4009 0.038 Uiso 1 1 calc R U . . . C50 C 0.6902(5) 1.01451(13) 0.41919(16) 0.0312(9) Uani 1 1 d . . . . . C51 C 0.6759(5) 1.04260(13) 0.45992(17) 0.0326(9) Uani 1 1 d . . . . . H51 H 0.6349 1.0696 0.4519 0.039 Uiso 1 1 calc R U . . . C52 C 0.7240(5) 1.02957(13) 0.51283(17) 0.0324(9) Uani 1 1 d . . . . . S2 S 1.13015(12) 0.81161(3) 1.14619(4) 0.0326(2) Uani 1 1 d . . . . . O10 O 1.2086(3) 0.77455(9) 1.13090(12) 0.0363(7) Uani 1 1 d . . . . . O11 O 1.0291(4) 0.80608(10) 1.18828(11) 0.0397(7) Uani 1 1 d . . . . . O12 O 1.2388(3) 0.84686(9) 1.15513(12) 0.0361(7) Uani 1 1 d . . . . . O13 O 0.7619(4) 0.76326(12) 1.12669(15) 0.0553(9) Uani 1 1 d . . . . . O14 O 0.6670(5) 0.82077(14) 1.15503(16) 0.0689(12) Uani 1 1 d . . . . . O15 O 0.7155(4) 0.88798(11) 0.91491(13) 0.0490(8) Uani 1 1 d . . . . . O16 O 0.5103(4) 0.87332(13) 0.95746(15) 0.0564(9) Uani 1 1 d . . . . . O17 O 1.2975(4) 0.82105(11) 1.03814(15) 0.0488(8) Uani 1 1 d . . . . . O18 O 1.2661(4) 0.88714(11) 1.03965(15) 0.0555(9) Uani 1 1 d . . . . . N8 N 0.7448(5) 0.80053(14) 1.12625(17) 0.0455(10) Uani 1 1 d . . . . . N9 N 0.6552(5) 0.87422(12) 0.95414(15) 0.0417(9) Uani 1 1 d . . . . . N10 N 1.2152(5) 0.85178(12) 1.04027(15) 0.0396(9) Uani 1 1 d . . . . . C53 C 0.9879(5) 0.82716(13) 1.08685(17) 0.0319(9) Uani 1 1 d . . . . . C54 C 0.8193(5) 0.82339(13) 1.08432(17) 0.0329(9) Uani 1 1 d . . . . . C55 C 0.7083(5) 0.83890(14) 1.04232(18) 0.0355(9) Uani 1 1 d . . . . . H55 H 0.5940 0.8365 1.0423 0.043 Uiso 1 1 calc R U . . . C56 C 0.7708(5) 0.85812(13) 1.00008(17) 0.0339(9) Uani 1 1 d . . . . . C57 C 0.9349(5) 0.86257(14) 0.99908(17) 0.0358(10) Uani 1 1 d . . . . . H57 H 0.9748 0.8759 0.9696 0.043 Uiso 1 1 calc R U . . . C58 C 1.0393(5) 0.84683(13) 1.04263(17) 0.0336(9) Uani 1 1 d . . . . . N1 N 0.7525(4) 0.59352(12) 0.74932(14) 0.0319(8) Uani 1 1 d . . . . . N2 N 0.8638(7) 0.46047(16) 0.5083(2) 0.0714(14) Uani 1 1 d . . . . . C1 C 0.7524(5) 0.61688(14) 0.80351(17) 0.0340(9) Uani 1 1 d . . . . . H1A H 0.7507 0.5958 0.8328 0.041 Uiso 1 1 calc R U . . . C2 C 0.9097(5) 0.64151(14) 0.81771(17) 0.0334(9) Uani 1 1 d . . . . . H2 H 0.9092 0.6524 0.8554 0.040 Uiso 1 1 calc R U . . . C3 C 1.0545(5) 0.61197(15) 0.82142(18) 0.0391(10) Uani 1 1 d . . . . . H3 H 1.0381 0.5905 0.8490 0.047 Uiso 1 1 calc R U . . . C4 C 1.0568(5) 0.58988(15) 0.76772(18) 0.0403(10) Uani 1 1 d . . . . . H4A H 1.0681 0.6104 0.7389 0.048 Uiso 1 1 calc R U . . . H4B H 1.1526 0.5713 0.7710 0.048 Uiso 1 1 calc R U . . . C5 C 0.9028(5) 0.56509(14) 0.75132(17) 0.0352(9) Uani 1 1 d . . . . . H5 H 0.8965 0.5442 0.7805 0.042 Uiso 1 1 calc R U . . . C6 C 0.8974(5) 0.54203(14) 0.69790(18) 0.0359(9) Uani 1 1 d . . . . . C7 C 0.8741(6) 0.49993(16) 0.6970(2) 0.0472(11) Uani 1 1 d . . . . . H7 H 0.8591 0.4860 0.7296 0.057 Uiso 1 1 calc R U . . . C8 C 0.8725(7) 0.47775(17) 0.6489(2) 0.0561(14) Uani 1 1 d . . . . . H8 H 0.8582 0.4487 0.6486 0.067 Uiso 1 1 calc R U . . . C9 C 0.8921(6) 0.49875(16) 0.6010(2) 0.0466(11) Uani 1 1 d . . . . . C10 C 0.9199(5) 0.54082(14) 0.60203(18) 0.0399(10) Uani 1 1 d . . . . . H10 H 0.9378 0.5548 0.5698 0.048 Uiso 1 1 calc R U . . . C11 C 0.9215(5) 0.56238(14) 0.65029(18) 0.0385(10) Uani 1 1 d . . . . . H11 H 0.9392 0.5913 0.6509 0.046 Uiso 1 1 calc R U . . . C12 C 0.8794(7) 0.47704(17) 0.5497(2) 0.0560(13) Uani 1 1 d . . . . . C13 C 0.5973(5) 0.64202(14) 0.80081(18) 0.0375(10) Uani 1 1 d . . . . . H13A H 0.5024 0.6231 0.7968 0.045 Uiso 1 1 calc R U . . . H13B H 0.5862 0.6599 0.7681 0.045 Uiso 1 1 calc R U . . . C14 C 0.5939(6) 0.66893(15) 0.85120(19) 0.0424(11) Uani 1 1 d . . . . . H14A H 0.6067 0.6515 0.8839 0.064 Uiso 1 1 calc R U . . . H14B H 0.4893 0.6836 0.8479 0.064 Uiso 1 1 calc R U . . . H14C H 0.6834 0.6889 0.8541 0.064 Uiso 1 1 calc R U . . . C15 C 0.9230(6) 0.67954(14) 0.78105(17) 0.0376(10) Uani 1 1 d . . . . . H15A H 0.9955 0.6726 0.7540 0.045 Uiso 1 1 calc R U . . . H15B H 0.8135 0.6858 0.7607 0.045 Uiso 1 1 calc R U . . . C16 C 0.9894(6) 0.71825(16) 0.8125(2) 0.0484(12) Uani 1 1 d . . . . . H16A H 0.9208 0.7248 0.8403 0.073 Uiso 1 1 calc R U . . . H16B H 0.9879 0.7414 0.7871 0.073 Uiso 1 1 calc R U . . . H16C H 1.1017 0.7132 0.8301 0.073 Uiso 1 1 calc R U . . . C17 C 1.2181(5) 0.63276(17) 0.8412(2) 0.0471(12) Uani 1 1 d . . . . . H17A H 1.2094 0.6491 0.8739 0.071 Uiso 1 1 calc R U . . . H17B H 1.2472 0.6508 0.8125 0.071 Uiso 1 1 calc R U . . . H17C H 1.3028 0.6117 0.8500 0.071 Uiso 1 1 calc R U . . . C18 C 0.6009(5) 0.56845(14) 0.73373(17) 0.0339(9) Uani 1 1 d . . . . . C19 C 0.5103(5) 0.57524(15) 0.68309(18) 0.0393(10) Uani 1 1 d . . . . . H19 H 0.5397 0.5963 0.6598 0.047 Uiso 1 1 calc R U . . . C20 C 0.3745(6) 0.55033(16) 0.6671(2) 0.0456(11) Uani 1 1 d . . . . . H20 H 0.3101 0.5543 0.6325 0.055 Uiso 1 1 calc R U . . . C21 C 0.3334(6) 0.51996(16) 0.7016(2) 0.0454(11) Uani 1 1 d . . . . . H21 H 0.2404 0.5032 0.6905 0.054 Uiso 1 1 calc R U . . . C22 C 0.4260(5) 0.51377(14) 0.7519(2) 0.0405(10) Uani 1 1 d . . . . . H22 H 0.3974 0.4926 0.7751 0.049 Uiso 1 1 calc R U . . . C23 C 0.5615(5) 0.53853(14) 0.76869(19) 0.0384(10) Uani 1 1 d . . . . . H23 H 0.6252 0.5348 0.8035 0.046 Uiso 1 1 calc R U . . . N3 N 0.7573(4) 0.81362(11) 0.61847(13) 0.0285(7) Uani 1 1 d . . . . . N4 N 0.6028(5) 0.79006(14) 0.90710(17) 0.0543(11) Uani 1 1 d . . . . . C24 C 0.7659(5) 0.81928(13) 0.55706(16) 0.0322(9) Uani 1 1 d . . . . . H24 H 0.7992 0.8484 0.5514 0.039 Uiso 1 1 calc R U . . . C25 C 0.5954(5) 0.81251(13) 0.52319(16) 0.0301(9) Uani 1 1 d . . . . . H25 H 0.6049 0.8213 0.4851 0.036 Uiso 1 1 calc R U . . . C26 C 0.4736(5) 0.84267(13) 0.54366(17) 0.0326(9) Uani 1 1 d . . . . . H26 H 0.5164 0.8712 0.5405 0.039 Uiso 1 1 calc R U . . . C27 C 0.4621(5) 0.83483(13) 0.60322(17) 0.0319(9) Uani 1 1 d . . . . . H27A H 0.4226 0.8064 0.6075 0.038 Uiso 1 1 calc R U . . . H27B H 0.3817 0.8541 0.6152 0.038 Uiso 1 1 calc R U . . . C28 C 0.6261(5) 0.84046(13) 0.63901(16) 0.0305(9) Uani 1 1 d . . . . . H28 H 0.6592 0.8700 0.6368 0.037 Uiso 1 1 calc R U . . . C29 C 0.6217(5) 0.83013(13) 0.69833(17) 0.0310(9) Uani 1 1 d . . . . . C30 C 0.5746(5) 0.79099(13) 0.71276(18) 0.0351(9) Uani 1 1 d . . . . . H30 H 0.5428 0.7711 0.6851 0.042 Uiso 1 1 calc R U . . . C31 C 0.5731(5) 0.78052(14) 0.76658(17) 0.0355(9) Uani 1 1 d . . . . . H31 H 0.5443 0.7535 0.7762 0.043 Uiso 1 1 calc R U . . . C32 C 0.6145(5) 0.81022(14) 0.80630(18) 0.0385(10) Uani 1 1 d . . . . . C33 C 0.6589(6) 0.84987(15) 0.79233(19) 0.0457(11) Uani 1 1 d . . . . . H33 H 0.6856 0.8701 0.8199 0.055 Uiso 1 1 calc R U . . . C34 C 0.6639(5) 0.85954(14) 0.73864(18) 0.0391(10) Uani 1 1 d . . . . . H34 H 0.6961 0.8863 0.7291 0.047 Uiso 1 1 calc R U . . . C35 C 0.6092(6) 0.79953(15) 0.86291(19) 0.0434(11) Uani 1 1 d . . . . . C36 C 0.9007(5) 0.79102(14) 0.54221(17) 0.0355(9) Uani 1 1 d . . . . . H36A H 1.0070 0.8003 0.5622 0.043 Uiso 1 1 calc R U . . . H36B H 0.8809 0.7627 0.5544 0.043 Uiso 1 1 calc R U . . . C37 C 0.9107(6) 0.79023(15) 0.48152(18) 0.0414(11) Uani 1 1 d . . . . . H37A H 0.8093 0.7788 0.4617 0.062 Uiso 1 1 calc R U . . . H37B H 1.0032 0.7731 0.4750 0.062 Uiso 1 1 calc R U . . . H37C H 0.9259 0.8183 0.4687 0.062 Uiso 1 1 calc R U . . . C38 C 0.5376(5) 0.76764(13) 0.51916(17) 0.0329(9) Uani 1 1 d . . . . . H38A H 0.6324 0.7494 0.5307 0.040 Uiso 1 1 calc R U . . . H38B H 0.4582 0.7633 0.5448 0.040 Uiso 1 1 calc R U . . . C39 C 0.4581(6) 0.75514(16) 0.46208(19) 0.0460(11) Uani 1 1 d . . . . . H39A H 0.5387 0.7570 0.4370 0.069 Uiso 1 1 calc R U . . . H39B H 0.3664 0.7736 0.4498 0.069 Uiso 1 1 calc R U . . . H39C H 0.4181 0.7268 0.4628 0.069 Uiso 1 1 calc R U . . . C40 C 0.3034(5) 0.84059(15) 0.50950(19) 0.0394(10) Uani 1 1 d . . . . . H40A H 0.3120 0.8460 0.4712 0.059 Uiso 1 1 calc R U . . . H40B H 0.2324 0.8613 0.5226 0.059 Uiso 1 1 calc R U . . . H40C H 0.2568 0.8131 0.5129 0.059 Uiso 1 1 calc R U . . . C41 C 0.9170(5) 0.82235(13) 0.65223(16) 0.0313(9) Uani 1 1 d . . . . . C42 C 0.9802(5) 0.86181(14) 0.65377(18) 0.0345(9) Uani 1 1 d . . . . . H42 H 0.9261 0.8829 0.6314 0.041 Uiso 1 1 calc R U . . . C43 C 1.1232(5) 0.86999(15) 0.68832(18) 0.0393(10) Uani 1 1 d . . . . . H43 H 1.1671 0.8971 0.6904 0.047 Uiso 1 1 calc R U . . . C44 C 1.2031(5) 0.83881(15) 0.72006(18) 0.0392(10) Uani 1 1 d . . . . . H44 H 1.3009 0.8447 0.7441 0.047 Uiso 1 1 calc R U . . . C45 C 1.1414(5) 0.79951(15) 0.71693(18) 0.0402(10) Uani 1 1 d . . . . . H45 H 1.1983 0.7782 0.7381 0.048 Uiso 1 1 calc R U . . . C46 C 0.9957(5) 0.79060(14) 0.68282(17) 0.0335(9) Uani 1 1 d . . . . . H46 H 0.9519 0.7635 0.6807 0.040 Uiso 1 1 calc R U . . . H3A H 0.735(5) 0.7836(15) 0.6252(18) 0.032(11) Uiso 1 1 d . . . . . H1 H 0.763(6) 0.6143(18) 0.724(2) 0.052(15) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0297(5) 0.0298(5) 0.0350(5) 0.0025(4) 0.0100(4) -0.0012(4) O1 0.0313(15) 0.0322(16) 0.0364(15) -0.0013(12) 0.0130(11) 0.0012(11) O2 0.0289(16) 0.0438(18) 0.0435(17) 0.0020(14) 0.0086(12) -0.0008(13) O3 0.0394(17) 0.0283(16) 0.0411(16) 0.0051(12) 0.0090(12) -0.0021(12) O4 0.0340(18) 0.0408(18) 0.0492(18) 0.0034(14) 0.0115(14) 0.0066(13) O5 0.070(2) 0.0273(17) 0.0449(18) -0.0023(14) 0.0047(15) -0.0016(15) O6 0.0420(18) 0.0416(18) 0.0363(16) -0.0025(14) 0.0096(12) -0.0015(13) O7 0.0464(19) 0.0363(18) 0.0430(17) 0.0073(14) 0.0123(13) -0.0017(13) O8 0.054(2) 0.0362(18) 0.0453(18) 0.0011(14) 0.0193(15) 0.0094(15) O9 0.051(2) 0.0374(18) 0.0383(16) -0.0049(13) 0.0103(14) -0.0108(14) N5 0.042(2) 0.028(2) 0.041(2) -0.0003(16) 0.0119(17) 0.0021(15) N6 0.031(2) 0.036(2) 0.0382(19) 0.0006(16) 0.0113(14) -0.0042(15) N7 0.046(2) 0.0297(19) 0.0352(19) 0.0006(15) 0.0148(17) -0.0021(17) C47 0.024(2) 0.028(2) 0.039(2) 0.0028(17) 0.0101(16) -0.0034(16) C48 0.026(2) 0.028(2) 0.039(2) -0.0002(17) 0.0092(16) -0.0001(16) C49 0.028(2) 0.031(2) 0.038(2) -0.0038(17) 0.0107(16) -0.0039(17) C50 0.029(2) 0.033(2) 0.034(2) 0.0034(17) 0.0099(16) -0.0006(16) C51 0.032(2) 0.028(2) 0.040(2) 0.0009(17) 0.0123(17) -0.0013(16) C52 0.034(2) 0.028(2) 0.037(2) -0.0049(17) 0.0114(17) -0.0039(17) S2 0.0356(6) 0.0282(5) 0.0334(5) -0.0008(4) 0.0028(4) 0.0000(4) O10 0.0398(17) 0.0294(16) 0.0388(16) -0.0029(12) 0.0030(12) 0.0035(12) O11 0.0436(18) 0.0454(19) 0.0307(15) 0.0019(13) 0.0073(12) -0.0021(14) O12 0.0368(17) 0.0268(16) 0.0436(17) -0.0017(12) 0.0023(12) -0.0047(12) O13 0.055(2) 0.049(2) 0.061(2) 0.0146(17) 0.0050(16) -0.0138(16) O14 0.058(2) 0.094(3) 0.061(2) 0.021(2) 0.0295(19) 0.029(2) O15 0.062(2) 0.046(2) 0.0379(18) 0.0071(15) 0.0046(15) 0.0063(16) O16 0.040(2) 0.069(3) 0.057(2) 0.0080(18) -0.0019(16) 0.0090(17) O17 0.040(2) 0.042(2) 0.065(2) 0.0053(16) 0.0120(15) -0.0021(15) O18 0.056(2) 0.047(2) 0.066(2) -0.0058(17) 0.0177(17) -0.0185(17) N8 0.038(2) 0.053(3) 0.046(2) 0.0099(19) 0.0085(17) 0.0019(18) N9 0.045(3) 0.039(2) 0.039(2) 0.0040(17) 0.0000(17) 0.0060(17) N10 0.048(2) 0.035(2) 0.036(2) 0.0027(16) 0.0075(16) -0.0031(18) C53 0.037(2) 0.023(2) 0.036(2) -0.0030(16) 0.0051(17) -0.0001(16) C54 0.034(2) 0.034(2) 0.032(2) 0.0018(17) 0.0105(17) -0.0009(17) C55 0.032(2) 0.037(2) 0.038(2) 0.0021(18) 0.0057(17) -0.0011(18) C56 0.038(3) 0.029(2) 0.033(2) 0.0008(17) -0.0001(17) 0.0062(17) C57 0.045(3) 0.031(2) 0.031(2) 0.0031(17) 0.0060(18) -0.0003(18) C58 0.035(2) 0.027(2) 0.039(2) -0.0021(17) 0.0055(17) -0.0013(17) N1 0.0262(19) 0.035(2) 0.0354(18) -0.0009(16) 0.0072(14) 0.0012(14) N2 0.117(4) 0.049(3) 0.054(3) -0.003(2) 0.031(3) -0.010(3) C1 0.037(2) 0.035(2) 0.032(2) 0.0000(18) 0.0097(17) -0.0010(18) C2 0.029(2) 0.039(3) 0.032(2) -0.0003(18) 0.0051(16) -0.0062(18) C3 0.035(3) 0.045(3) 0.038(2) 0.0028(19) 0.0076(18) -0.0016(19) C4 0.036(3) 0.043(3) 0.042(2) 0.001(2) 0.0100(19) -0.001(2) C5 0.030(2) 0.040(3) 0.036(2) 0.0040(18) 0.0069(17) 0.0058(18) C6 0.034(2) 0.038(2) 0.037(2) 0.0000(18) 0.0105(17) 0.0026(18) C7 0.062(3) 0.043(3) 0.040(2) -0.001(2) 0.016(2) -0.008(2) C8 0.085(4) 0.038(3) 0.049(3) -0.008(2) 0.019(3) -0.017(3) C9 0.056(3) 0.041(3) 0.046(3) -0.004(2) 0.017(2) 0.002(2) C10 0.042(3) 0.039(3) 0.040(2) 0.0023(19) 0.0109(19) 0.0040(19) C11 0.041(3) 0.033(2) 0.042(2) 0.0004(19) 0.0082(19) 0.0088(18) C12 0.080(4) 0.042(3) 0.049(3) -0.006(2) 0.021(3) -0.010(3) C13 0.035(3) 0.038(3) 0.041(2) -0.0013(19) 0.0103(18) -0.0010(19) C14 0.042(3) 0.041(3) 0.046(3) -0.005(2) 0.012(2) -0.001(2) C15 0.040(3) 0.040(3) 0.033(2) -0.0013(18) 0.0065(18) -0.0062(19) C16 0.060(3) 0.042(3) 0.043(3) -0.003(2) 0.009(2) -0.018(2) C17 0.034(3) 0.064(3) 0.043(3) 0.000(2) 0.0055(19) -0.005(2) C18 0.028(2) 0.035(2) 0.039(2) -0.0041(18) 0.0070(17) -0.0025(17) C19 0.034(3) 0.042(3) 0.042(2) -0.003(2) 0.0042(18) -0.0031(19) C20 0.035(3) 0.049(3) 0.052(3) -0.010(2) 0.001(2) -0.003(2) C21 0.034(3) 0.045(3) 0.059(3) -0.015(2) 0.011(2) -0.005(2) C22 0.035(3) 0.036(2) 0.055(3) -0.005(2) 0.020(2) -0.0022(19) C23 0.033(2) 0.041(3) 0.043(2) 0.0014(19) 0.0104(18) -0.0010(19) N3 0.0244(18) 0.031(2) 0.0307(17) -0.0004(14) 0.0052(13) 0.0008(13) N4 0.068(3) 0.054(3) 0.041(2) 0.007(2) 0.0078(19) -0.004(2) C24 0.031(2) 0.034(2) 0.033(2) 0.0006(17) 0.0085(16) 0.0002(17) C25 0.030(2) 0.029(2) 0.031(2) 0.0044(16) 0.0043(16) -0.0010(16) C26 0.030(2) 0.029(2) 0.038(2) 0.0029(17) 0.0051(17) 0.0010(17) C27 0.027(2) 0.032(2) 0.037(2) 0.0007(17) 0.0064(16) 0.0023(16) C28 0.029(2) 0.027(2) 0.037(2) 0.0010(17) 0.0090(16) 0.0038(16) C29 0.026(2) 0.031(2) 0.037(2) 0.0014(17) 0.0058(16) -0.0019(16) C30 0.037(3) 0.030(2) 0.039(2) -0.0021(18) 0.0079(18) 0.0013(17) C31 0.036(2) 0.032(2) 0.040(2) 0.0051(18) 0.0091(18) 0.0008(18) C32 0.038(3) 0.039(3) 0.039(2) 0.0044(19) 0.0084(18) 0.0008(19) C33 0.059(3) 0.042(3) 0.037(2) -0.002(2) 0.007(2) -0.010(2) C34 0.047(3) 0.032(2) 0.039(2) 0.0004(19) 0.0086(19) -0.0104(19) C35 0.049(3) 0.043(3) 0.037(3) 0.001(2) 0.0059(19) -0.003(2) C36 0.030(2) 0.038(2) 0.040(2) 0.0007(19) 0.0087(17) 0.0037(17) C37 0.040(3) 0.045(3) 0.041(2) -0.003(2) 0.0112(19) 0.001(2) C38 0.034(2) 0.030(2) 0.035(2) 0.0005(17) 0.0031(17) -0.0006(17) C39 0.055(3) 0.041(3) 0.039(2) -0.003(2) -0.002(2) -0.006(2) C40 0.033(2) 0.041(3) 0.043(2) 0.004(2) 0.0010(18) 0.0006(19) C41 0.025(2) 0.036(2) 0.033(2) -0.0018(17) 0.0041(16) -0.0005(17) C42 0.028(2) 0.036(2) 0.040(2) 0.0000(18) 0.0076(17) -0.0035(17) C43 0.031(2) 0.044(3) 0.044(2) -0.003(2) 0.0104(18) -0.0068(19) C44 0.028(2) 0.047(3) 0.042(2) -0.001(2) 0.0052(18) -0.0055(19) C45 0.030(2) 0.049(3) 0.041(2) 0.006(2) 0.0044(18) 0.003(2) C46 0.028(2) 0.035(2) 0.038(2) 0.0020(18) 0.0071(17) -0.0023(17) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O2 1.434(3) . ? S1 O1 1.446(3) . ? S1 O3 1.450(3) . ? S1 C47 1.827(4) . ? O4 N5 1.215(5) . ? O5 N5 1.228(5) . ? O6 N6 1.230(5) . ? O7 N6 1.223(5) . ? O8 N7 1.226(5) . ? O9 N7 1.221(5) . ? N5 C48 1.471(5) . ? N6 C50 1.481(5) . ? N7 C52 1.478(5) . ? C47 C52 1.393(6) . ? C47 C48 1.394(6) . ? C48 C49 1.382(6) . ? C49 C50 1.364(6) . ? C49 H49 0.9500 . ? C50 C51 1.379(6) . ? C51 C52 1.380(6) . ? C51 H51 0.9500 . ? S2 O11 1.443(3) . ? S2 O10 1.445(3) . ? S2 O12 1.452(3) . ? S2 C53 1.814(4) . ? O13 N8 1.218(6) . ? O14 N8 1.222(6) . ? O15 N9 1.241(5) . ? O16 N9 1.215(5) . ? O17 N10 1.214(5) . ? O18 N10 1.224(5) . ? N8 C54 1.485(6) . ? N9 C56 1.470(6) . ? N10 C58 1.475(6) . ? C53 C58 1.390(6) . ? C53 C54 1.393(6) . ? C54 C55 1.377(6) . ? C55 C56 1.384(6) . ? C55 H55 0.9500 . ? C56 C57 1.370(6) . ? C57 C58 1.377(6) . ? C57 H57 0.9500 . ? N1 C18 1.497(5) . ? N1 C1 1.543(5) . ? N1 C5 1.544(5) . ? N1 H1 0.93(6) . ? N2 C12 1.148(7) . ? C1 C13 1.515(6) . ? C1 C2 1.524(6) . ? C1 H1A 1.0000 . ? C2 C3 1.527(6) . ? C2 C15 1.547(6) . ? C2 H2 1.0000 . ? C3 C4 1.515(6) . ? C3 C17 1.527(7) . ? C3 H3 1.0000 . ? C4 C5 1.511(6) . ? C4 H4A 0.9900 . ? C4 H4B 0.9900 . ? C5 C6 1.516(6) . ? C5 H5 1.0000 . ? C6 C7 1.380(7) . ? C6 C11 1.393(6) . ? C7 C8 1.392(7) . ? C7 H7 0.9500 . ? C8 C9 1.399(7) . ? C8 H8 0.9500 . ? C9 C10 1.385(7) . ? C9 C12 1.446(7) . ? C10 C11 1.385(6) . ? C10 H10 0.9500 . ? C11 H11 0.9500 . ? C13 C14 1.529(6) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C16 1.536(6) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 C23 1.374(6) . ? C18 C19 1.381(6) . ? C19 C20 1.393(6) . ? C19 H19 0.9500 . ? C20 C21 1.380(7) . ? C20 H20 0.9500 . ? C21 C22 1.377(7) . ? C21 H21 0.9500 . ? C22 C23 1.392(6) . ? C22 H22 0.9500 . ? C23 H23 0.9500 . ? N3 C41 1.483(5) . ? N3 C28 1.538(5) . ? N3 C24 1.546(5) . ? N3 H3A 1.01(5) . ? N4 C35 1.147(6) . ? C24 C36 1.532(6) . ? C24 C25 1.547(6) . ? C24 H24 1.0000 . ? C25 C38 1.532(6) . ? C25 C26 1.545(6) . ? C25 H25 1.0000 . ? C26 C27 1.516(6) . ? C26 C40 1.533(6) . ? C26 H26 1.0000 . ? C27 C28 1.518(6) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 C29 1.515(6) . ? C28 H28 1.0000 . ? C29 C34 1.389(6) . ? C29 C30 1.392(6) . ? C30 C31 1.379(6) . ? C30 H30 0.9500 . ? C31 C32 1.384(6) . ? C31 H31 0.9500 . ? C32 C33 1.397(7) . ? C32 C35 1.453(6) . ? C33 C34 1.375(6) . ? C33 H33 0.9500 . ? C34 H34 0.9500 . ? C36 C37 1.520(6) . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 C39 1.524(6) . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C41 C42 1.382(6) . ? C41 C46 1.384(6) . ? C42 C43 1.379(6) . ? C42 H42 0.9500 . ? C43 C44 1.388(7) . ? C43 H43 0.9500 . ? C44 C45 1.372(7) . ? C44 H44 0.9500 . ? C45 C46 1.396(6) . ? C45 H45 0.9500 . ? C46 H46 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 S1 O1 114.75(18) . . ? O2 S1 O3 115.37(18) . . ? O1 S1 O3 113.39(17) . . ? O2 S1 C47 106.75(18) . . ? O1 S1 C47 103.11(17) . . ? O3 S1 C47 101.43(18) . . ? O4 N5 O5 124.8(4) . . ? O4 N5 C48 118.3(3) . . ? O5 N5 C48 116.9(4) . . ? O7 N6 O6 125.2(4) . . ? O7 N6 C50 117.7(3) . . ? O6 N6 C50 117.1(4) . . ? O9 N7 O8 125.3(4) . . ? O9 N7 C52 116.8(4) . . ? O8 N7 C52 117.8(4) . . ? C52 C47 C48 114.4(4) . . ? C52 C47 S1 121.6(3) . . ? C48 C47 S1 123.1(3) . . ? C49 C48 C47 123.6(4) . . ? C49 C48 N5 116.0(4) . . ? C47 C48 N5 120.4(4) . . ? C50 C49 C48 117.9(4) . . ? C50 C49 H49 121.0 . . ? C48 C49 H49 121.0 . . ? C49 C50 C51 122.7(4) . . ? C49 C50 N6 118.9(4) . . ? C51 C50 N6 118.4(4) . . ? C50 C51 C52 116.7(4) . . ? C50 C51 H51 121.6 . . ? C52 C51 H51 121.6 . . ? C51 C52 C47 124.6(4) . . ? C51 C52 N7 115.3(4) . . ? C47 C52 N7 120.1(4) . . ? O11 S2 O10 114.72(19) . . ? O11 S2 O12 113.61(18) . . ? O10 S2 O12 113.82(18) . . ? O11 S2 C53 104.19(19) . . ? O10 S2 C53 106.36(18) . . ? O12 S2 C53 102.53(18) . . ? O13 N8 O14 126.8(4) . . ? O13 N8 C54 116.3(4) . . ? O14 N8 C54 116.8(4) . . ? O16 N9 O15 125.3(4) . . ? O16 N9 C56 118.3(4) . . ? O15 N9 C56 116.4(4) . . ? O17 N10 O18 125.0(4) . . ? O17 N10 C58 118.4(4) . . ? O18 N10 C58 116.5(4) . . ? C58 C53 C54 115.3(4) . . ? C58 C53 S2 122.0(3) . . ? C54 C53 S2 122.5(3) . . ? C55 C54 C53 123.5(4) . . ? C55 C54 N8 114.4(4) . . ? C53 C54 N8 122.1(4) . . ? C54 C55 C56 117.0(4) . . ? C54 C55 H55 121.5 . . ? C56 C55 H55 121.5 . . ? C57 C56 C55 123.0(4) . . ? C57 C56 N9 118.7(4) . . ? C55 C56 N9 118.2(4) . . ? C56 C57 C58 117.0(4) . . ? C56 C57 H57 121.5 . . ? C58 C57 H57 121.5 . . ? C57 C58 C53 124.0(4) . . ? C57 C58 N10 115.9(4) . . ? C53 C58 N10 120.2(4) . . ? C18 N1 C1 112.5(3) . . ? C18 N1 C5 108.9(3) . . ? C1 N1 C5 111.8(3) . . ? C18 N1 H1 112(3) . . ? C1 N1 H1 104(3) . . ? C5 N1 H1 107(3) . . ? C13 C1 C2 114.7(4) . . ? C13 C1 N1 109.7(3) . . ? C2 C1 N1 110.3(3) . . ? C13 C1 H1A 107.3 . . ? C2 C1 H1A 107.3 . . ? N1 C1 H1A 107.3 . . ? C1 C2 C3 108.7(4) . . ? C1 C2 C15 114.6(3) . . ? C3 C2 C15 114.3(4) . . ? C1 C2 H2 106.2 . . ? C3 C2 H2 106.2 . . ? C15 C2 H2 106.2 . . ? C4 C3 C2 110.9(4) . . ? C4 C3 C17 111.3(4) . . ? C2 C3 C17 113.1(4) . . ? C4 C3 H3 107.0 . . ? C2 C3 H3 107.0 . . ? C17 C3 H3 107.0 . . ? C5 C4 C3 111.5(4) . . ? C5 C4 H4A 109.3 . . ? C3 C4 H4A 109.3 . . ? C5 C4 H4B 109.3 . . ? C3 C4 H4B 109.3 . . ? H4A C4 H4B 108.0 . . ? C4 C5 C6 114.3(4) . . ? C4 C5 N1 109.5(4) . . ? C6 C5 N1 110.4(3) . . ? C4 C5 H5 107.5 . . ? C6 C5 H5 107.5 . . ? N1 C5 H5 107.5 . . ? C7 C6 C11 119.6(4) . . ? C7 C6 C5 119.2(4) . . ? C11 C6 C5 121.1(4) . . ? C6 C7 C8 120.6(5) . . ? C6 C7 H7 119.7 . . ? C8 C7 H7 119.7 . . ? C7 C8 C9 119.2(5) . . ? C7 C8 H8 120.4 . . ? C9 C8 H8 120.4 . . ? C10 C9 C8 120.4(4) . . ? C10 C9 C12 119.1(4) . . ? C8 C9 C12 120.5(5) . . ? C11 C10 C9 119.6(4) . . ? C11 C10 H10 120.2 . . ? C9 C10 H10 120.2 . . ? C10 C11 C6 120.6(4) . . ? C10 C11 H11 119.7 . . ? C6 C11 H11 119.7 . . ? N2 C12 C9 177.5(7) . . ? C1 C13 C14 113.0(4) . . ? C1 C13 H13A 109.0 . . ? C14 C13 H13A 109.0 . . ? C1 C13 H13B 109.0 . . ? C14 C13 H13B 109.0 . . ? H13A C13 H13B 107.8 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C16 C15 C2 114.0(4) . . ? C16 C15 H15A 108.8 . . ? C2 C15 H15A 108.8 . . ? C16 C15 H15B 108.8 . . ? C2 C15 H15B 108.8 . . ? H15A C15 H15B 107.7 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C3 C17 H17A 109.5 . . ? C3 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C3 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C23 C18 C19 122.6(4) . . ? C23 C18 N1 119.4(4) . . ? C19 C18 N1 117.9(4) . . ? C18 C19 C20 118.1(4) . . ? C18 C19 H19 121.0 . . ? C20 C19 H19 121.0 . . ? C21 C20 C19 120.1(5) . . ? C21 C20 H20 119.9 . . ? C19 C20 H20 119.9 . . ? C22 C21 C20 120.6(4) . . ? C22 C21 H21 119.7 . . ? C20 C21 H21 119.7 . . ? C21 C22 C23 120.1(4) . . ? C21 C22 H22 120.0 . . ? C23 C22 H22 120.0 . . ? C18 C23 C22 118.4(4) . . ? C18 C23 H23 120.8 . . ? C22 C23 H23 120.8 . . ? C41 N3 C28 108.6(3) . . ? C41 N3 C24 111.4(3) . . ? C28 N3 C24 113.5(3) . . ? C41 N3 H3A 105(2) . . ? C28 N3 H3A 110(2) . . ? C24 N3 H3A 108(2) . . ? C36 C24 N3 108.0(3) . . ? C36 C24 C25 115.0(4) . . ? N3 C24 C25 110.2(3) . . ? C36 C24 H24 107.8 . . ? N3 C24 H24 107.8 . . ? C25 C24 H24 107.8 . . ? C38 C25 C26 114.3(3) . . ? C38 C25 C24 114.9(3) . . ? C26 C25 C24 108.6(3) . . ? C38 C25 H25 106.1 . . ? C26 C25 H25 106.1 . . ? C24 C25 H25 106.1 . . ? C27 C26 C40 110.1(3) . . ? C27 C26 C25 110.7(3) . . ? C40 C26 C25 112.5(4) . . ? C27 C26 H26 107.8 . . ? C40 C26 H26 107.8 . . ? C25 C26 H26 107.8 . . ? C26 C27 C28 111.6(3) . . ? C26 C27 H27A 109.3 . . ? C28 C27 H27A 109.3 . . ? C26 C27 H27B 109.3 . . ? C28 C27 H27B 109.3 . . ? H27A C27 H27B 108.0 . . ? C29 C28 C27 113.0(3) . . ? C29 C28 N3 108.5(3) . . ? C27 C28 N3 110.6(3) . . ? C29 C28 H28 108.2 . . ? C27 C28 H28 108.2 . . ? N3 C28 H28 108.2 . . ? C34 C29 C30 119.5(4) . . ? C34 C29 C28 120.4(4) . . ? C30 C29 C28 120.0(4) . . ? C31 C30 C29 121.2(4) . . ? C31 C30 H30 119.4 . . ? C29 C30 H30 119.4 . . ? C30 C31 C32 118.7(4) . . ? C30 C31 H31 120.7 . . ? C32 C31 H31 120.7 . . ? C31 C32 C33 120.8(4) . . ? C31 C32 C35 118.8(4) . . ? C33 C32 C35 120.5(4) . . ? C34 C33 C32 119.9(4) . . ? C34 C33 H33 120.1 . . ? C32 C33 H33 120.1 . . ? C33 C34 C29 120.0(4) . . ? C33 C34 H34 120.0 . . ? C29 C34 H34 120.0 . . ? N4 C35 C32 178.0(5) . . ? C37 C36 C24 113.4(4) . . ? C37 C36 H36A 108.9 . . ? C24 C36 H36A 108.9 . . ? C37 C36 H36B 108.9 . . ? C24 C36 H36B 108.9 . . ? H36A C36 H36B 107.7 . . ? C36 C37 H37A 109.5 . . ? C36 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C36 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C39 C38 C25 113.6(4) . . ? C39 C38 H38A 108.8 . . ? C25 C38 H38A 108.8 . . ? C39 C38 H38B 108.8 . . ? C25 C38 H38B 108.8 . . ? H38A C38 H38B 107.7 . . ? C38 C39 H39A 109.5 . . ? C38 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C38 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C26 C40 H40A 109.5 . . ? C26 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C26 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C42 C41 C46 122.0(4) . . ? C42 C41 N3 119.7(4) . . ? C46 C41 N3 118.3(4) . . ? C43 C42 C41 118.8(4) . . ? C43 C42 H42 120.6 . . ? C41 C42 H42 120.6 . . ? C42 C43 C44 120.2(4) . . ? C42 C43 H43 119.9 . . ? C44 C43 H43 119.9 . . ? C45 C44 C43 120.3(4) . . ? C45 C44 H44 119.9 . . ? C43 C44 H44 119.9 . . ? C44 C45 C46 120.5(4) . . ? C44 C45 H45 119.8 . . ? C46 C45 H45 119.8 . . ? C41 C46 C45 118.1(4) . . ? C41 C46 H46 120.9 . . ? C45 C46 H46 120.9 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O2 S1 C47 C52 -102.0(3) . . . . ? O1 S1 C47 C52 19.3(4) . . . . ? O3 S1 C47 C52 136.9(3) . . . . ? O2 S1 C47 C48 89.9(4) . . . . ? O1 S1 C47 C48 -148.8(3) . . . . ? O3 S1 C47 C48 -31.3(4) . . . . ? C52 C47 C48 C49 -2.5(6) . . . . ? S1 C47 C48 C49 166.4(3) . . . . ? C52 C47 C48 N5 177.1(4) . . . . ? S1 C47 C48 N5 -14.0(5) . . . . ? O4 N5 C48 C49 130.1(4) . . . . ? O5 N5 C48 C49 -47.3(5) . . . . ? O4 N5 C48 C47 -49.5(5) . . . . ? O5 N5 C48 C47 133.1(4) . . . . ? C47 C48 C49 C50 0.2(6) . . . . ? N5 C48 C49 C50 -179.4(4) . . . . ? C48 C49 C50 C51 0.8(6) . . . . ? C48 C49 C50 N6 -179.0(3) . . . . ? O7 N6 C50 C49 -172.7(4) . . . . ? O6 N6 C50 C49 7.7(5) . . . . ? O7 N6 C50 C51 7.4(5) . . . . ? O6 N6 C50 C51 -172.1(4) . . . . ? C49 C50 C51 C52 0.5(6) . . . . ? N6 C50 C51 C52 -179.7(3) . . . . ? C50 C51 C52 C47 -3.1(6) . . . . ? C50 C51 C52 N7 174.2(4) . . . . ? C48 C47 C52 C51 4.0(6) . . . . ? S1 C47 C52 C51 -165.1(3) . . . . ? C48 C47 C52 N7 -173.2(4) . . . . ? S1 C47 C52 N7 17.7(5) . . . . ? O9 N7 C52 C51 -117.6(4) . . . . ? O8 N7 C52 C51 58.5(5) . . . . ? O9 N7 C52 C47 59.8(5) . . . . ? O8 N7 C52 C47 -124.1(4) . . . . ? O11 S2 C53 C58 160.9(3) . . . . ? O10 S2 C53 C58 -77.5(4) . . . . ? O12 S2 C53 C58 42.3(4) . . . . ? O11 S2 C53 C54 -13.6(4) . . . . ? O10 S2 C53 C54 108.0(4) . . . . ? O12 S2 C53 C54 -132.2(3) . . . . ? C58 C53 C54 C55 -2.0(6) . . . . ? S2 C53 C54 C55 172.8(4) . . . . ? C58 C53 C54 N8 175.5(4) . . . . ? S2 C53 C54 N8 -9.7(6) . . . . ? O13 N8 C54 C55 107.9(5) . . . . ? O14 N8 C54 C55 -69.0(6) . . . . ? O13 N8 C54 C53 -69.8(6) . . . . ? O14 N8 C54 C53 113.3(5) . . . . ? C53 C54 C55 C56 1.9(7) . . . . ? N8 C54 C55 C56 -175.8(4) . . . . ? C54 C55 C56 C57 -0.9(7) . . . . ? C54 C55 C56 N9 178.7(4) . . . . ? O16 N9 C56 C57 -173.8(4) . . . . ? O15 N9 C56 C57 5.7(6) . . . . ? O16 N9 C56 C55 6.5(6) . . . . ? O15 N9 C56 C55 -173.9(4) . . . . ? C55 C56 C57 C58 0.1(6) . . . . ? N9 C56 C57 C58 -179.5(4) . . . . ? C56 C57 C58 C53 -0.3(6) . . . . ? C56 C57 C58 N10 179.6(4) . . . . ? C54 C53 C58 C57 1.1(6) . . . . ? S2 C53 C58 C57 -173.7(3) . . . . ? C54 C53 C58 N10 -178.7(4) . . . . ? S2 C53 C58 N10 6.5(6) . . . . ? O17 N10 C58 C57 -116.6(5) . . . . ? O18 N10 C58 C57 62.2(5) . . . . ? O17 N10 C58 C53 63.3(5) . . . . ? O18 N10 C58 C53 -118.0(5) . . . . ? C18 N1 C1 C13 -53.3(5) . . . . ? C5 N1 C1 C13 -176.2(4) . . . . ? C18 N1 C1 C2 179.5(3) . . . . ? C5 N1 C1 C2 56.6(4) . . . . ? C13 C1 C2 C3 177.5(4) . . . . ? N1 C1 C2 C3 -58.1(4) . . . . ? C13 C1 C2 C15 -53.2(5) . . . . ? N1 C1 C2 C15 71.3(5) . . . . ? C1 C2 C3 C4 60.0(5) . . . . ? C15 C2 C3 C4 -69.5(5) . . . . ? C1 C2 C3 C17 -174.1(4) . . . . ? C15 C2 C3 C17 56.4(5) . . . . ? C2 C3 C4 C5 -59.9(5) . . . . ? C17 C3 C4 C5 173.2(4) . . . . ? C3 C4 C5 C6 -179.8(4) . . . . ? C3 C4 C5 N1 55.8(5) . . . . ? C18 N1 C5 C4 -179.3(3) . . . . ? C1 N1 C5 C4 -54.4(4) . . . . ? C18 N1 C5 C6 54.0(4) . . . . ? C1 N1 C5 C6 178.9(3) . . . . ? C4 C5 C6 C7 123.7(5) . . . . ? N1 C5 C6 C7 -112.4(5) . . . . ? C4 C5 C6 C11 -53.9(6) . . . . ? N1 C5 C6 C11 70.0(5) . . . . ? C11 C6 C7 C8 -0.8(7) . . . . ? C5 C6 C7 C8 -178.4(5) . . . . ? C6 C7 C8 C9 -1.0(8) . . . . ? C7 C8 C9 C10 2.8(8) . . . . ? C7 C8 C9 C12 -175.6(5) . . . . ? C8 C9 C10 C11 -2.7(7) . . . . ? C12 C9 C10 C11 175.7(5) . . . . ? C9 C10 C11 C6 0.8(7) . . . . ? C7 C6 C11 C10 0.9(7) . . . . ? C5 C6 C11 C10 178.5(4) . . . . ? C2 C1 C13 C14 -50.5(5) . . . . ? N1 C1 C13 C14 -175.2(4) . . . . ? C1 C2 C15 C16 136.8(4) . . . . ? C3 C2 C15 C16 -96.7(5) . . . . ? C1 N1 C18 C23 -58.5(5) . . . . ? C5 N1 C18 C23 66.0(5) . . . . ? C1 N1 C18 C19 124.6(4) . . . . ? C5 N1 C18 C19 -110.9(4) . . . . ? C23 C18 C19 C20 -0.5(7) . . . . ? N1 C18 C19 C20 176.3(4) . . . . ? C18 C19 C20 C21 0.1(7) . . . . ? C19 C20 C21 C22 -0.3(7) . . . . ? C20 C21 C22 C23 0.7(7) . . . . ? C19 C18 C23 C22 0.9(7) . . . . ? N1 C18 C23 C22 -175.8(4) . . . . ? C21 C22 C23 C18 -1.0(7) . . . . ? C41 N3 C24 C36 57.0(4) . . . . ? C28 N3 C24 C36 179.9(3) . . . . ? C41 N3 C24 C25 -176.6(3) . . . . ? C28 N3 C24 C25 -53.7(4) . . . . ? C36 C24 C25 C38 49.7(5) . . . . ? N3 C24 C25 C38 -72.6(4) . . . . ? C36 C24 C25 C26 179.1(3) . . . . ? N3 C24 C25 C26 56.8(4) . . . . ? C38 C25 C26 C27 69.0(4) . . . . ? C24 C25 C26 C27 -60.8(4) . . . . ? C38 C25 C26 C40 -54.7(5) . . . . ? C24 C25 C26 C40 175.5(3) . . . . ? C40 C26 C27 C28 -174.8(4) . . . . ? C25 C26 C27 C28 60.2(5) . . . . ? C26 C27 C28 C29 -176.2(3) . . . . ? C26 C27 C28 N3 -54.3(5) . . . . ? C41 N3 C28 C29 -59.4(4) . . . . ? C24 N3 C28 C29 176.2(3) . . . . ? C41 N3 C28 C27 176.1(3) . . . . ? C24 N3 C28 C27 51.7(4) . . . . ? C27 C28 C29 C34 -121.3(4) . . . . ? N3 C28 C29 C34 115.6(4) . . . . ? C27 C28 C29 C30 58.5(5) . . . . ? N3 C28 C29 C30 -64.6(5) . . . . ? C34 C29 C30 C31 -1.7(6) . . . . ? C28 C29 C30 C31 178.5(4) . . . . ? C29 C30 C31 C32 2.1(6) . . . . ? C30 C31 C32 C33 -0.8(7) . . . . ? C30 C31 C32 C35 178.6(4) . . . . ? C31 C32 C33 C34 -0.9(7) . . . . ? C35 C32 C33 C34 179.8(5) . . . . ? C32 C33 C34 C29 1.3(7) . . . . ? C30 C29 C34 C33 0.0(7) . . . . ? C28 C29 C34 C33 179.8(4) . . . . ? N3 C24 C36 C37 174.1(4) . . . . ? C25 C24 C36 C37 50.6(5) . . . . ? C26 C25 C38 C39 96.6(4) . . . . ? C24 C25 C38 C39 -136.8(4) . . . . ? C28 N3 C41 C42 -60.2(5) . . . . ? C24 N3 C41 C42 65.4(5) . . . . ? C28 N3 C41 C46 117.7(4) . . . . ? C24 N3 C41 C46 -116.7(4) . . . . ? C46 C41 C42 C43 -2.3(6) . . . . ? N3 C41 C42 C43 175.5(4) . . . . ? C41 C42 C43 C44 1.2(6) . . . . ? C42 C43 C44 C45 0.7(7) . . . . ? C43 C44 C45 C46 -1.5(7) . . . . ? C42 C41 C46 C45 1.4(6) . . . . ? N3 C41 C46 C45 -176.4(4) . . . . ? C44 C45 C46 C41 0.5(6) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N3 H3A O10 1.01(5) 1.91(5) 2.913(5) 173(4) 4_575 N1 H1 O12 0.93(6) 2.11(6) 3.023(5) 166(5) 4_575 _refine_diff_density_max 0.398 _refine_diff_density_min -0.537 _refine_diff_density_rms 0.058 _shelx_res_file ; 007b-19018.res created by SHELXL-2014/7 TITL 007b-19018 CELL 1.54184 8.2796 32.4638 24.8002 90 98.611 90 ZERR 8 0.0003 0.0007 0.0007 0 0.003 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O S UNIT 232 248 40 72 8 L.S. 10 TEMP -180 SIZE 0.20 0.20 0.10 CONF MORE -1 BOND $H ABIN EQIV $4 x-1/2, -y+3/2, z-1/2 HTAB N3 O10_$4 HTAB N1 O12_$4 ACTA MERG 0 WGHT 0.098000 3.643200 BASF 0.35430 FVAR 2.45247 S1 5 0.792633 0.971579 0.597707 11.00000 0.02968 0.02983 = 0.03497 0.00251 0.00996 -0.00117 O1 4 0.687864 0.999686 0.621630 11.00000 0.03126 0.03220 = 0.03635 -0.00132 0.01303 0.00124 O2 4 0.961928 0.973519 0.620827 11.00000 0.02890 0.04377 = 0.04347 0.00202 0.00856 -0.00082 O3 4 0.725330 0.930432 0.589546 11.00000 0.03940 0.02828 = 0.04106 0.00506 0.00897 -0.00207 O4 4 0.980649 0.916931 0.523758 11.00000 0.03398 0.04077 = 0.04917 0.00345 0.01153 0.00664 O5 4 0.775669 0.894145 0.467147 11.00000 0.06965 0.02733 = 0.04490 -0.00226 0.00470 -0.00162 O6 4 0.637239 1.000486 0.326655 11.00000 0.04201 0.04165 = 0.03626 -0.00251 0.00958 -0.00150 O7 4 0.605362 1.063561 0.353065 11.00000 0.04637 0.03628 = 0.04300 0.00734 0.01234 -0.00167 O8 4 0.592695 1.079104 0.557867 11.00000 0.05444 0.03620 = 0.04527 0.00106 0.01935 0.00939 O9 4 0.853345 1.070014 0.582502 11.00000 0.05061 0.03738 = 0.03832 -0.00489 0.01033 -0.01081 N5 3 0.853542 0.921804 0.492937 11.00000 0.04199 0.02781 = 0.04067 -0.00031 0.01191 0.00212 N6 3 0.640601 1.027326 0.361789 11.00000 0.03094 0.03568 = 0.03822 0.00061 0.01127 -0.00425 N7 3 0.722479 1.061615 0.555099 11.00000 0.04585 0.02973 = 0.03517 0.00060 0.01485 -0.00208 C47 1 0.777981 0.989937 0.527505 11.00000 0.02406 0.02769 = 0.03892 0.00279 0.01013 -0.00344 C48 1 0.790628 0.963975 0.483573 11.00000 0.02587 0.02828 = 0.03868 -0.00021 0.00917 -0.00009 C49 1 0.747549 0.975503 0.429693 11.00000 0.02834 0.03133 = 0.03820 -0.00379 0.01072 -0.00393 AFIX 43 H49 2 0.757597 0.956842 0.400876 11.00000 -1.20000 AFIX 0 C50 1 0.690166 1.014506 0.419193 11.00000 0.02885 0.03278 = 0.03367 0.00342 0.00994 -0.00061 C51 1 0.675853 1.042599 0.459916 11.00000 0.03187 0.02760 = 0.04031 0.00088 0.01230 -0.00131 AFIX 43 H51 2 0.634873 1.069598 0.451924 11.00000 -1.20000 AFIX 0 C52 1 0.723970 1.029570 0.512835 11.00000 0.03448 0.02764 = 0.03691 -0.00490 0.01143 -0.00393 S2 5 1.130154 0.811613 1.146192 11.00000 0.03557 0.02817 = 0.03343 -0.00078 0.00277 -0.00001 O10 4 1.208586 0.774548 1.130900 11.00000 0.03982 0.02939 = 0.03880 -0.00289 0.00299 0.00349 O11 4 1.029146 0.806084 1.188281 11.00000 0.04360 0.04539 = 0.03075 0.00194 0.00725 -0.00210 O12 4 1.238829 0.846859 1.155132 11.00000 0.03682 0.02679 = 0.04357 -0.00168 0.00225 -0.00466 O13 4 0.761941 0.763263 1.126691 11.00000 0.05506 0.04901 = 0.06076 0.01461 0.00499 -0.01381 O14 4 0.667008 0.820768 1.155027 11.00000 0.05807 0.09371 = 0.06135 0.02055 0.02950 0.02885 O15 4 0.715472 0.887978 0.914911 11.00000 0.06221 0.04605 = 0.03792 0.00705 0.00459 0.00633 O16 4 0.510328 0.873320 0.957463 11.00000 0.04005 0.06912 = 0.05727 0.00795 -0.00194 0.00899 O17 4 1.297454 0.821048 1.038139 11.00000 0.04044 0.04250 = 0.06482 0.00527 0.01200 -0.00208 O18 4 1.266079 0.887135 1.039650 11.00000 0.05611 0.04654 = 0.06637 -0.00579 0.01774 -0.01853 N8 3 0.744825 0.800532 1.126250 11.00000 0.03789 0.05274 = 0.04644 0.00990 0.00852 0.00194 N9 3 0.655247 0.874216 0.954145 11.00000 0.04509 0.03913 = 0.03882 0.00396 0.00005 0.00597 N10 3 1.215159 0.851780 1.040272 11.00000 0.04837 0.03522 = 0.03567 0.00273 0.00751 -0.00311 C53 1 0.987853 0.827160 1.086847 11.00000 0.03668 0.02303 = 0.03600 -0.00304 0.00513 -0.00010 C54 1 0.819288 0.823387 1.084317 11.00000 0.03448 0.03431 = 0.03154 0.00182 0.01051 -0.00089 C55 1 0.708318 0.838902 1.042324 11.00000 0.03157 0.03712 = 0.03782 0.00212 0.00572 -0.00110 AFIX 43 H55 2 0.593962 0.836526 1.042336 11.00000 -1.20000 AFIX 0 C56 1 0.770811 0.858121 1.000081 11.00000 0.03753 0.02928 = 0.03313 0.00076 -0.00009 0.00624 C57 1 0.934854 0.862571 0.999076 11.00000 0.04517 0.03141 = 0.03083 0.00313 0.00598 -0.00035 AFIX 43 H57 2 0.974796 0.875925 0.969640 11.00000 -1.20000 AFIX 0 C58 1 1.039279 0.846827 1.042633 11.00000 0.03454 0.02744 = 0.03869 -0.00206 0.00547 -0.00131 N1 3 0.752538 0.593518 0.749315 11.00000 0.02624 0.03485 = 0.03535 -0.00091 0.00719 0.00122 N2 3 0.863821 0.460473 0.508337 11.00000 0.11712 0.04870 = 0.05400 -0.00306 0.03081 -0.00960 C1 1 0.752422 0.616880 0.803515 11.00000 0.03692 0.03504 = 0.03158 0.00002 0.00971 -0.00104 AFIX 13 H1A 2 0.750654 0.595761 0.832775 11.00000 -1.20000 AFIX 0 C2 1 0.909681 0.641512 0.817707 11.00000 0.02873 0.03921 = 0.03246 -0.00031 0.00512 -0.00621 AFIX 13 H2 2 0.909191 0.652387 0.855407 11.00000 -1.20000 AFIX 0 C3 1 1.054470 0.611969 0.821423 11.00000 0.03499 0.04499 = 0.03785 0.00275 0.00763 -0.00157 AFIX 13 H3 2 1.038066 0.590512 0.849021 11.00000 -1.20000 AFIX 0 C4 1 1.056834 0.589883 0.767718 11.00000 0.03640 0.04347 = 0.04221 0.00062 0.00999 -0.00094 AFIX 23 H4A 2 1.068134 0.610365 0.738945 11.00000 -1.20000 H4B 2 1.152609 0.571296 0.771043 11.00000 -1.20000 AFIX 0 C5 1 0.902835 0.565086 0.751319 11.00000 0.03021 0.03969 = 0.03624 0.00403 0.00686 0.00577 AFIX 13 H5 2 0.896547 0.544172 0.780536 11.00000 -1.20000 AFIX 0 C6 1 0.897416 0.542035 0.697904 11.00000 0.03446 0.03779 = 0.03700 0.00005 0.01045 0.00256 C7 1 0.874121 0.499933 0.697040 11.00000 0.06165 0.04256 = 0.03987 -0.00142 0.01557 -0.00770 AFIX 43 H7 2 0.859055 0.485961 0.729575 11.00000 -1.20000 AFIX 0 C8 1 0.872501 0.477752 0.648916 11.00000 0.08469 0.03785 = 0.04867 -0.00839 0.01942 -0.01747 AFIX 43 H8 2 0.858250 0.448712 0.648581 11.00000 -1.20000 AFIX 0 C9 1 0.892116 0.498748 0.601048 11.00000 0.05612 0.04088 = 0.04592 -0.00388 0.01740 0.00157 C10 1 0.919947 0.540820 0.602030 11.00000 0.04215 0.03874 = 0.04025 0.00228 0.01085 0.00400 AFIX 43 H10 2 0.937835 0.554806 0.569799 11.00000 -1.20000 AFIX 0 C11 1 0.921543 0.562381 0.650293 11.00000 0.04138 0.03277 = 0.04207 0.00037 0.00819 0.00877 AFIX 43 H11 2 0.939246 0.591302 0.650940 11.00000 -1.20000 AFIX 0 C12 1 0.879362 0.477039 0.549693 11.00000 0.08046 0.04164 = 0.04929 -0.00552 0.02104 -0.00967 C13 1 0.597284 0.642018 0.800811 11.00000 0.03502 0.03841 = 0.04059 -0.00129 0.01034 -0.00097 AFIX 23 H13A 2 0.502417 0.623113 0.796792 11.00000 -1.20000 H13B 2 0.586205 0.659851 0.768081 11.00000 -1.20000 AFIX 0 C14 1 0.593877 0.668934 0.851197 11.00000 0.04204 0.04103 = 0.04561 -0.00472 0.01164 -0.00102 AFIX 137 H14A 2 0.606726 0.651542 0.883858 11.00000 -1.50000 H14B 2 0.489342 0.683571 0.847910 11.00000 -1.50000 H14C 2 0.683380 0.688947 0.854129 11.00000 -1.50000 AFIX 0 C15 1 0.923017 0.679541 0.781051 11.00000 0.03994 0.04016 = 0.03316 -0.00133 0.00651 -0.00617 AFIX 23 H15A 2 0.995458 0.672649 0.754007 11.00000 -1.20000 H15B 2 0.813497 0.685774 0.760743 11.00000 -1.20000 AFIX 0 C16 1 0.989364 0.718248 0.812467 11.00000 0.06034 0.04219 = 0.04283 -0.00271 0.00850 -0.01767 AFIX 137 H16A 2 0.920811 0.724784 0.840285 11.00000 -1.50000 H16B 2 0.987929 0.741428 0.787085 11.00000 -1.50000 H16C 2 1.101680 0.713227 0.830072 11.00000 -1.50000 AFIX 0 C17 1 1.218119 0.632759 0.841196 11.00000 0.03356 0.06426 = 0.04327 -0.00021 0.00552 -0.00537 AFIX 137 H17A 2 1.209435 0.649108 0.873857 11.00000 -1.50000 H17B 2 1.247163 0.650816 0.812466 11.00000 -1.50000 H17C 2 1.302760 0.611693 0.849951 11.00000 -1.50000 AFIX 0 C18 1 0.600927 0.568455 0.733728 11.00000 0.02838 0.03516 = 0.03882 -0.00409 0.00695 -0.00249 C19 1 0.510322 0.575245 0.683086 11.00000 0.03359 0.04176 = 0.04209 -0.00250 0.00423 -0.00306 AFIX 43 H19 2 0.539729 0.596297 0.659783 11.00000 -1.20000 AFIX 0 C20 1 0.374521 0.550332 0.667142 11.00000 0.03463 0.04852 = 0.05208 -0.01028 0.00132 -0.00257 AFIX 43 H20 2 0.310066 0.554263 0.632484 11.00000 -1.20000 AFIX 0 C21 1 0.333442 0.519958 0.701588 11.00000 0.03397 0.04475 = 0.05858 -0.01464 0.01056 -0.00536 AFIX 43 H21 2 0.240435 0.503160 0.690511 11.00000 -1.20000 AFIX 0 C22 1 0.426033 0.513774 0.751871 11.00000 0.03502 0.03585 = 0.05489 -0.00529 0.02045 -0.00218 AFIX 43 H22 2 0.397401 0.492585 0.775112 11.00000 -1.20000 AFIX 0 C23 1 0.561531 0.538530 0.768692 11.00000 0.03259 0.04052 = 0.04345 0.00144 0.01040 -0.00097 AFIX 43 H23 2 0.625228 0.534814 0.803524 11.00000 -1.20000 AFIX 0 N3 3 0.757286 0.813616 0.618469 11.00000 0.02440 0.03079 = 0.03066 -0.00038 0.00520 0.00079 N4 3 0.602784 0.790059 0.907105 11.00000 0.06804 0.05395 = 0.04087 0.00681 0.00777 -0.00431 C24 1 0.765924 0.819283 0.557062 11.00000 0.03098 0.03360 = 0.03331 0.00055 0.00854 0.00020 AFIX 13 H24 2 0.799207 0.848383 0.551363 11.00000 -1.20000 AFIX 0 C25 1 0.595387 0.812512 0.523193 11.00000 0.03026 0.02916 = 0.03069 0.00437 0.00426 -0.00101 AFIX 13 H25 2 0.604934 0.821284 0.485147 11.00000 -1.20000 AFIX 0 C26 1 0.473563 0.842666 0.543656 11.00000 0.03013 0.02931 = 0.03822 0.00294 0.00505 0.00098 AFIX 13 H26 2 0.516427 0.871231 0.540547 11.00000 -1.20000 AFIX 0 C27 1 0.462077 0.834826 0.603224 11.00000 0.02664 0.03247 = 0.03719 0.00073 0.00640 0.00230 AFIX 23 H27A 2 0.422624 0.806396 0.607492 11.00000 -1.20000 H27B 2 0.381748 0.854052 0.615242 11.00000 -1.20000 AFIX 0 C28 1 0.626118 0.840465 0.639012 11.00000 0.02872 0.02742 = 0.03656 0.00105 0.00904 0.00383 AFIX 13 H28 2 0.659208 0.869970 0.636807 11.00000 -1.20000 AFIX 0 C29 1 0.621693 0.830130 0.698329 11.00000 0.02560 0.03118 = 0.03664 0.00144 0.00579 -0.00190 C30 1 0.574552 0.790989 0.712761 11.00000 0.03740 0.02986 = 0.03874 -0.00214 0.00792 0.00131 AFIX 43 H30 2 0.542828 0.771135 0.685056 11.00000 -1.20000 AFIX 0 C31 1 0.573085 0.780522 0.766582 11.00000 0.03561 0.03152 = 0.04034 0.00515 0.00909 0.00080 AFIX 43 H31 2 0.544252 0.753465 0.776204 11.00000 -1.20000 AFIX 0 C32 1 0.614454 0.810216 0.806305 11.00000 0.03785 0.03913 = 0.03923 0.00444 0.00836 0.00078 C33 1 0.658864 0.849867 0.792328 11.00000 0.05862 0.04158 = 0.03673 -0.00246 0.00705 -0.00954 AFIX 43 H33 2 0.685576 0.870116 0.819875 11.00000 -1.20000 AFIX 0 C34 1 0.663857 0.859544 0.738635 11.00000 0.04714 0.03183 = 0.03908 0.00043 0.00864 -0.01037 AFIX 43 H34 2 0.696128 0.886335 0.729113 11.00000 -1.20000 AFIX 0 C35 1 0.609219 0.799532 0.862906 11.00000 0.04940 0.04328 = 0.03727 0.00074 0.00587 -0.00266 C36 1 0.900672 0.791016 0.542211 11.00000 0.02991 0.03795 = 0.03968 0.00070 0.00869 0.00371 AFIX 23 H36A 2 1.007043 0.800269 0.562156 11.00000 -1.20000 H36B 2 0.880926 0.762672 0.554434 11.00000 -1.20000 AFIX 0 C37 1 0.910660 0.790232 0.481518 11.00000 0.04036 0.04462 = 0.04087 -0.00274 0.01123 0.00126 AFIX 137 H37A 2 0.809304 0.778778 0.461707 11.00000 -1.50000 H37B 2 1.003183 0.773082 0.474971 11.00000 -1.50000 H37C 2 0.925931 0.818329 0.468743 11.00000 -1.50000 AFIX 0 C38 1 0.537583 0.767637 0.519158 11.00000 0.03364 0.02999 = 0.03454 0.00052 0.00313 -0.00063 AFIX 23 H38A 2 0.632351 0.749420 0.530698 11.00000 -1.20000 H38B 2 0.458205 0.763344 0.544777 11.00000 -1.20000 AFIX 0 C39 1 0.458102 0.755144 0.462077 11.00000 0.05494 0.04097 = 0.03940 -0.00286 -0.00201 -0.00553 AFIX 137 H39A 2 0.538670 0.756997 0.436978 11.00000 -1.50000 H39B 2 0.366426 0.773633 0.449750 11.00000 -1.50000 H39C 2 0.418099 0.726768 0.462798 11.00000 -1.50000 AFIX 0 C40 1 0.303360 0.840593 0.509504 11.00000 0.03276 0.04094 = 0.04293 0.00416 0.00101 0.00060 AFIX 137 H40A 2 0.312020 0.846023 0.471170 11.00000 -1.50000 H40B 2 0.232431 0.861309 0.522631 11.00000 -1.50000 H40C 2 0.256831 0.813123 0.512878 11.00000 -1.50000 AFIX 0 C41 1 0.917025 0.822349 0.652230 11.00000 0.02499 0.03618 = 0.03258 -0.00175 0.00413 -0.00054 C42 1 0.980211 0.861811 0.653773 11.00000 0.02799 0.03646 = 0.03984 0.00001 0.00759 -0.00347 AFIX 43 H42 2 0.926136 0.882918 0.631441 11.00000 -1.20000 AFIX 0 C43 1 1.123183 0.869991 0.688319 11.00000 0.03147 0.04418 = 0.04365 -0.00284 0.01036 -0.00676 AFIX 43 H43 2 1.167140 0.897073 0.690397 11.00000 -1.20000 AFIX 0 C44 1 1.203081 0.838807 0.720059 11.00000 0.02831 0.04736 = 0.04190 -0.00119 0.00524 -0.00551 AFIX 43 H44 2 1.300901 0.844699 0.744061 11.00000 -1.20000 AFIX 0 C45 1 1.141431 0.799511 0.716928 11.00000 0.03034 0.04939 = 0.04057 0.00625 0.00445 0.00264 AFIX 43 H45 2 1.198314 0.778204 0.738125 11.00000 -1.20000 AFIX 0 C46 1 0.995735 0.790605 0.682824 11.00000 0.02844 0.03473 = 0.03794 0.00204 0.00712 -0.00233 AFIX 43 H46 2 0.951866 0.763513 0.680681 11.00000 -1.20000 AFIX 0 H3A 2 0.735151 0.783636 0.625246 11.00000 0.03217 H1 2 0.762865 0.614267 0.723934 11.00000 0.05211 HKLF 5 REM 007b-19018 REM R1 = 0.0659 for 16141 Fo > 4sig(Fo) and 0.1007 for all 22919 data REM 808 parameters refined using 0 restraints END WGHT 0.0975 3.6233 REM Highest difference peak 0.398, deepest hole -0.537, 1-sigma level 0.058 Q1 1 1.2289 0.8263 1.1178 11.00000 0.05 0.40 Q2 1 1.3631 0.8103 1.1412 11.00000 0.05 0.28 Q3 1 1.1356 0.8944 0.9021 11.00000 0.05 0.28 Q4 1 1.2289 0.8125 0.9972 11.00000 0.05 0.24 Q5 1 0.8536 0.9155 0.4206 11.00000 0.05 0.22 Q6 1 0.7447 0.8354 0.8822 11.00000 0.05 0.22 Q7 1 0.8987 0.8356 0.7400 11.00000 0.05 0.22 Q8 1 0.4560 0.8595 1.0003 11.00000 0.05 0.20 Q9 1 0.7167 0.6866 0.7450 11.00000 0.05 0.20 Q10 1 0.4987 0.6322 0.6390 11.00000 0.05 0.19 Q11 1 0.7810 0.8419 1.1779 11.00000 0.05 0.19 Q12 1 0.5852 0.8705 0.8211 11.00000 0.05 0.19 Q13 1 0.5898 0.8983 0.7180 11.00000 0.05 0.19 Q14 1 0.9548 0.7208 0.6377 11.00000 0.05 0.19 Q15 1 0.3070 0.8101 0.5609 11.00000 0.05 0.19 Q16 1 1.4034 0.8426 1.1812 11.00000 0.05 0.19 Q17 1 0.5346 0.8859 0.6793 11.00000 0.05 0.19 Q18 1 0.8598 1.0591 0.4994 11.00000 0.05 0.19 Q19 1 0.6647 0.6784 0.3783 11.00000 0.05 0.19 Q20 1 0.9105 0.7689 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106.804 1 4 3 7 1226.25 97.8116 1 4 3 8 168.099 113.223 1 4 -3 9 19327.0 151.110 1 4 3 10 2707.86 131.714 1 4 3 11 2795.88 124.514 1 4 3 12 551.984 129.031 1 4 3 13 8233.94 148.726 1 4 3 14 408.586 143.490 1 4 3 15 398.356 154.343 1 4 3 16 249.138 173.323 1 4 3 17 1434.77 167.256 1 4 -3 18 1459.62 157.066 1 4 3 19 6628.77 167.404 1 4 3 20 34.7734 153.554 1 4 3 21 86.2893 154.576 1 4 3 22 643.331 137.767 1 4 3 23 105.919 136.517 1 4 3 24 159.930 125.825 1 -4 4 28 840.968 131.446 1 4 4 -27 209.043 134.748 1 -4 -4 26 2780.83 150.200 1 -4 -4 25 3830.66 140.957 1 -4 4 24 4135.95 152.721 1 -4 -4 23 3621.65 147.517 1 -4 -4 22 268.377 151.296 1 4 4 -21 16682.1 178.820 1 -4 -4 20 6951.56 149.943 1 -4 -4 19 1106.53 137.367 1 -4 -4 18 8221.90 133.208 1 4 4 -17 558.892 123.760 1 -4 -4 16 11316.7 127.473 1 -4 -4 15 11557.8 112.403 1 4 4 -14 18275.1 119.610 1 -4 4 13 5371.48 108.436 1 4 -4 -12 374.300 95.2408 1 4 4 -11 3544.42 93.4546 1 4 4 -10 10265.3 104.396 1 4 -4 -9 35672.2 116.188 1 4 4 -8 11378.0 111.906 1 -4 4 -4 12101.7 1195.62 -2 4 -4 -8 12101.7 1195.62 1 4 -4 -7 1210.31 126.122 1 -4 -4 -3 1177.58 228.422 -2 4 4 -7 1177.58 228.422 1 4 -4 -6 1153.69 118.163 1 4 4 2 2092.80 287.664 -2 -4 -4 6 2092.80 287.664 1 4 -4 -5 2593.33 134.692 1 4 4 1 19263.8 486.904 -2 -4 -4 5 19263.8 486.904 1 4 4 -4 13805.3 158.432 1 4 4 0 29936.6 526.684 -2 -4 -4 4 29936.6 526.684 1 4 4 -3 410.847 142.596 1 4 4 -1 455.898 436.586 -2 -4 -4 3 455.898 436.586 1 4 4 -2 469.931 158.078 1 -4 -4 2 533.321 295.174 -2 4 4 -2 533.321 295.174 1 -4 4 1 237.262 185.406 1 -4 -4 3 341.210 264.555 -2 4 4 -1 341.210 264.555 1 4 -4 0 28569.1 424.562 1 -4 -4 4 36651.8 334.657 -2 4 4 0 36651.8 334.657 1 4 4 1 36435.8 275.024 1 -4 -4 5 36776.2 296.798 -2 4 4 1 36776.2 296.798 1 4 4 2 1233.35 218.316 1 -4 -4 6 1783.75 266.434 -2 4 4 2 1783.75 266.434 1 4 4 3 68.7437 217.418 1 4 4 -7 1535.32 269.052 -2 -4 -4 -3 1535.32 269.052 1 4 -4 4 1408.03 125.765 1 -4 4 8 7044.30 342.377 -2 4 -4 4 7044.30 342.377 1 4 -4 5 6645.01 111.606 1 4 -4 6 18286.0 111.610 1 -4 -4 10 23730.9 2357.86 -2 4 4 6 23730.9 2357.86 1 4 4 7 17075.0 107.412 1 4 -4 8-42.8314 101.112 1 4 4 9 3856.93 115.483 1 4 4 10 13764.5 129.107 1 4 4 11 14006.7 137.461 1 4 4 12 1727.45 134.254 1 4 4 13 2063.06 142.614 1 4 -4 14 1427.04 153.272 1 4 4 15 7558.01 165.364 1 4 -4 16 4680.28 178.048 1 4 4 17 118.951 188.369 1 4 -4 18 1646.20 157.432 1 4 -4 19 340.140 155.112 1 4 -4 20 723.361 157.646 1 4 -4 21-42.5338 157.911 1 4 -4 22 164.078 139.112 1 4 4 23 917.423 120.422 1 4 4 24 428.363 119.062 1 -4 5 28 165.143 127.790 1 -4 5 27 66.6985 130.070 1 -4 -5 26 64.0955 132.734 1 -4 -5 25 36.5055 144.975 1 4 5 -24 1939.09 147.636 1 -4 5 23 19.1733 152.769 1 -4 -5 22 976.365 149.072 1 -4 -5 21 3024.81 153.308 1 -4 5 20 1408.55 136.098 1 4 5 -19 309.226 123.080 1 -4 -5 18 126.089 124.343 1 -4 -5 17 63.6312 113.920 1 4 -5 -16 16568.7 122.811 1 4 5 -15 19707.4 113.283 1 4 -5 -14 882.836 99.3639 1 4 5 -13 16583.8 110.610 1 4 -5 -12 3474.16 99.8903 1 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152.410 1 4 5 -7 6239.95 236.211 -2 -4 -5 -3 6239.95 236.211 1 4 5 4 3136.47 121.581 1 -4 -5 8 8509.57 311.725 -2 4 5 4 8509.57 311.725 1 4 -5 5 18223.7 118.404 1 -4 -5 9 17888.8 382.723 -2 4 5 5 17888.8 382.723 1 4 5 6 12318.2 109.293 1 -4 -5 10 13017.5 639.922 -2 4 5 6 13017.5 639.922 1 4 5 7 1369.06 107.698 1 4 5 8 1979.77 107.923 1 4 -5 9 850.905 144.622 1 4 5 10 75.1817 117.987 1 4 5 11 150.746 130.586 1 4 5 12 2321.48 138.981 1 4 5 13 2001.01 147.567 1 4 5 14 1197.82 154.805 1 4 -5 15 228.865 156.797 1 4 -5 16 168.644 148.860 1 4 5 17-86.0683 174.284 1 4 5 18 6096.41 169.925 1 4 -5 19 860.029 159.339 1 4 5 20 218.692 159.117 1 4 5 21 5439.63 160.535 1 4 -5 22 675.331 132.177 1 4 -5 23 3811.82 124.564 1 4 5 24 33.5236 114.691 1 4 -6 -28 741.761 134.781 1 -4 -6 27 34.0897 136.344 1 -4 6 26 270.128 127.328 1 4 6 -25-73.9268 142.658 1 -4 -6 24 3583.13 156.608 1 -4 -6 23 56.1034 160.584 1 -4 -6 22-35.4256 134.933 1 -4 6 21 949.646 137.083 1 -4 6 20 1463.59 129.237 1 -4 -6 19 9330.61 142.034 1 -4 -6 18 15837.0 139.363 1 4 6 -17 878.538 114.678 1 -4 6 16 1554.88 113.773 1 4 6 -15 1620.19 110.128 1 -4 -6 14 1101.88 100.035 1 4 6 -13 2477.43 103.582 1 -4 -6 12 10060.5 106.130 1 4 -6 -11 495.758 102.273 1 4 6 -10 246.393 102.511 1 -4 -6 9 2632.74 102.139 1 -4 -6 -5 2901.45 277.073 -2 4 6 -9 2901.45 277.073 1 4 -6 -8 135.457 101.564 1 4 6 4 1535.73 378.226 -2 -4 -6 8 1535.73 378.226 1 4 6 -7 9235.98 120.283 1 4 6 3 9199.15 273.626 -2 -4 -6 7 9199.15 273.626 1 4 -6 -6 3295.70 130.063 1 4 6 2 20510.1 314.035 -2 -4 -6 6 20510.1 314.035 1 4 -6 -5 989.084 137.219 1 4 6 1 6538.62 332.444 -2 -4 -6 5 6538.62 332.444 1 4 6 -4 1105.06 139.513 1 4 -6 0 8829.95 342.598 -2 -4 6 4 8829.95 342.598 1 -4 6 3 2222.66 141.499 1 -4 -6 1 3846.95 368.430 -2 4 6 -3 3846.95 368.430 1 4 -6 -2 38496.6 175.171 1 -4 -6 2 57228.0 329.396 -2 4 6 -2 57228.0 329.396 1 -4 6 1 574.062 165.982 1 4 6 -3 2914.02 350.989 -2 -4 -6 1 2914.02 350.989 1 4 6 0 12060.3 166.184 1 -4 -6 4 12700.5 268.110 -2 4 6 0 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137.878 1 4 -7 -24-143.903 151.546 1 -4 -7 23 611.990 150.421 1 4 -7 -22 6954.51 161.341 1 -4 7 21 4758.61 146.830 1 -4 7 20 1102.78 134.158 1 4 -7 -19 1116.05 138.074 1 -4 -7 18 3241.19 132.821 1 -4 7 17 1593.00 130.119 1 -4 -7 16 7913.16 125.121 1 4 7 -15 1547.57 114.919 1 4 -7 -14 551.741 104.892 1 -4 -7 13 11492.8 115.056 1 4 7 -12 7346.14 111.803 1 4 7 -11 8698.23 108.214 1 -4 7 10 9702.24 102.394 1 4 7 -9 260.875 98.7604 1 4 7 5 2984.39 293.271 -2 -4 -7 9 2984.39 293.271 1 4 -7 -8 1756.30 124.024 1 4 7 4 5988.02 323.717 -2 -4 -7 8 5988.02 323.717 1 4 -7 -7 349.871 109.761 1 -4 -7 -3 2252.30 227.559 -2 4 7 -7 2252.30 227.559 1 4 -7 -6 13630.7 133.624 1 -4 7 -2 30155.2 388.441 -2 4 -7 -6 30155.2 388.441 1 4 -7 -5 424.336 141.366 1 -4 -7 -1 2572.44 209.898 -2 4 7 -5 2572.44 209.898 1 4 -7 -4 1068.12 136.261 1 -4 -7 0 5241.42 285.337 -2 4 7 -4 5241.42 285.337 1 4 7 -3 4378.35 157.977 1 -4 -7 1 8661.60 367.933 -2 4 7 -3 8661.60 367.933 1 4 -7 -2 19500.9 166.188 1 -4 -7 2 31302.3 318.693 -2 4 7 -2 31302.3 318.693 1 -4 7 1 7796.98 174.271 1 -4 -7 3 9405.97 335.156 -2 4 7 -1 9405.97 335.156 1 4 -7 0 6029.19 176.400 1 -4 -7 4 7032.56 254.890 -2 4 7 0 7032.56 254.890 1 4 7 1 2638.53 170.918 1 4 -7 -5 3482.09 197.740 -2 -4 7 -1 3482.09 197.740 1 4 7 2 33699.5 184.752 1 -4 -7 6 40414.3 247.369 -2 4 7 2 40414.3 247.369 1 4 -7 3 2955.88 130.649 1 4 7 -7 3279.73 243.825 -2 -4 -7 -3 3279.73 243.825 1 4 -7 4 8463.70 123.791 1 4 7 -8 8892.82 315.405 -2 -4 -7 -4 8892.82 315.405 1 4 7 5 5039.24 109.434 1 -4 -7 9 4346.17 351.863 -2 4 7 5 4346.17 351.863 1 -4 -7 -6 195.716 104.620 1 -4 -7 10 5385.81 607.255 -2 4 7 6 5385.81 607.255 1 4 7 7 4836.92 117.780 1 -4 -7 11 13369.8 682.979 -2 4 7 7 13369.8 682.979 1 4 -7 8 13060.1 149.376 1 4 -7 9 9638.99 134.363 1 4 -7 10 799.938 130.413 1 4 7 11 822.929 140.509 1 4 7 12 8608.33 141.852 1 4 7 13 9717.73 151.286 1 4 7 14 2183.45 154.032 1 4 7 15 1176.86 158.385 1 4 7 16 6083.61 167.062 1 4 -7 17 476.197 161.445 1 4 -7 18 1879.58 182.109 1 4 -7 19 988.524 166.463 1 4 7 20-44.3857 151.758 1 4 -7 21 1067.77 144.394 1 4 -7 22 296.232 135.538 1 4 -7 23 356.333 116.569 1 4 -7 24-48.5444 121.504 1 -4 8 27 88.5520 137.094 1 -4 8 26 1085.34 141.594 1 4 8 -25 198.069 136.316 1 -4 8 24 117.454 147.039 1 -4 -8 23 107.504 140.643 1 -4 8 22 359.563 150.184 1 -4 8 21 6266.34 145.585 1 -4 -8 20 1235.24 143.628 1 -4 -8 19 4743.88 140.287 1 -4 8 18 19693.5 144.893 1 -4 8 17 12.4992 124.013 1 4 8 -16 5104.36 120.310 1 4 8 -15 3288.40 133.079 1 4 8 -14 47478.0 142.724 1 -4 8 13 70.2583 106.525 1 4 -8 -12 1522.95 104.141 1 4 8 -11 138.046 100.836 1 -4 -8 10 38827.7 127.269 1 4 -8 -9 7076.34 110.051 1 4 8 5 6591.65 355.649 -2 -4 -8 9 6591.65 355.649 1 -4 8 8 25933.9 136.941 1 4 8 4 24490.1 253.699 -2 -4 -8 8 24490.1 253.699 1 4 -8 -7 11761.2 126.027 1 4 8 3 11392.2 231.544 -2 -4 -8 7 11392.2 231.544 1 4 8 -6 5752.99 117.755 1 4 8 2 6352.78 213.514 -2 -4 -8 6 6352.78 213.514 1 -4 8 5 1276.56 136.465 1 4 8 1 21726.5 244.933 -2 -4 -8 5 21726.5 244.933 1 4 8 -4 181.618 142.038 1 -4 8 0 27977.7 344.756 -2 4 -8 -4 27977.7 344.756 1 4 -8 -3 15188.3 166.784 1 4 8 -1 17661.7 344.982 -2 -4 -8 3 17661.7 344.982 1 4 -8 -2 8501.93 155.955 1 -4 8 2 12155.8 251.737 -2 4 -8 -2 12155.8 251.737 1 4 8 -1 1388.94 164.388 1 -4 -8 3 8830.43 741.459 -2 4 8 -1 8830.43 741.459 1 4 8 0 41170.3 209.149 1 -4 -8 4 41659.7 244.568 -2 4 8 0 41659.7 244.568 1 4 -8 1 39284.2 182.677 1 -4 -8 5 38843.8 205.972 -2 4 8 1 38843.8 205.972 1 4 8 2 652.703 139.628 1 -4 8 6 3983.66 196.654 -2 4 -8 2 3983.66 196.654 1 4 -8 3 417.205 143.466 1 4 8 -7 7106.43 261.454 -2 -4 -8 -3 7106.43 261.454 1 4 -8 4 360.793 125.691 1 4 8 -8 14521.5 334.506 -2 -4 -8 -4 14521.5 334.506 1 4 8 5 215.443 122.383 1 -4 8 9 4156.16 483.995 -2 4 -8 5 4156.16 483.995 1 4 -8 6 18045.7 130.196 1 -4 -8 10 36595.1 715.409 -2 4 8 6 36595.1 715.409 1 4 8 7 8715.02 118.105 1 -4 -8 -8 2566.04 124.036 1 4 8 9 1269.85 122.303 1 4 -8 10 8470.12 136.766 1 4 8 11 12877.0 135.242 1 4 8 12 987.984 138.830 1 4 8 13 774.359 145.069 1 4 8 14 3019.97 157.170 1 4 8 15 10955.9 170.732 1 -4 -8 -16 13674.8 162.866 1 4 8 17 4414.71 166.129 1 4 -8 18-15.7259 165.904 1 4 -8 19 116.385 155.569 1 4 -8 20 2217.23 149.868 1 4 -8 21 657.037 141.248 1 4 8 22 1697.39 134.181 1 4 -8 23 475.408 115.694 1 4 -8 24 169.738 133.581 1 -4 -9 27 138.202 130.623 1 4 -9 -26 153.335 134.175 1 -4 -9 25 32.6621 148.175 1 -4 -9 24 346.745 129.930 1 -4 -9 23 135.168 137.108 1 -4 9 22 1006.17 158.776 1 4 -9 -21 2168.46 139.082 1 -4 9 20 192.293 133.803 1 -4 -9 19 133.627 133.101 1 -4 -9 18 16816.7 152.793 1 -4 9 17 7376.85 138.653 1 4 9 -16 2975.61 128.547 1 -4 -9 15 4180.63 144.211 1 -4 9 14 464.176 124.105 1 4 9 -13-9.04526 115.798 1 4 9 -12 27239.1 115.405 1 4 9 -11 1789.13 102.375 1 -4 -9 10-14.7663 113.075 1 4 9 6 6017.69 494.404 -2 -4 -9 10 6017.69 494.404 1 4 9 -9 87.9476 105.692 1 4 9 5 811.418 239.200 -2 -4 -9 9 811.418 239.200 1 4 9 -8 9946.55 124.601 1 -4 -9 -4 13178.9 227.152 -2 4 9 -8 13178.9 227.152 1 4 9 -7 2660.55 119.953 1 4 9 3 2665.97 237.724 -2 -4 -9 7 2665.97 237.724 1 4 9 -6 321.467 133.625 1 4 9 2 3688.39 186.345 -2 -4 -9 6 3688.39 186.345 1 4 -9 -5 3951.93 135.388 1 4 9 1 3623.72 184.854 -2 -4 -9 5 3623.72 184.854 1 4 9 -4 129.019 132.703 1 -4 -9 0 1404.76 209.911 -2 4 9 -4 1404.76 209.911 1 4 -9 -3 3093.23 151.815 1 4 9 -1 4884.19 250.257 -2 -4 -9 3 4884.19 250.257 1 4 -9 -2 12440.3 162.617 1 4 9 -2 19003.0 267.630 -2 -4 -9 2 19003.0 267.630 1 4 -9 -1 2669.76 146.682 1 -4 -9 3 4247.98 300.802 -2 4 9 -1 4247.98 300.802 1 4 9 0 619.796 176.923 1 -4 -9 4 797.285 168.874 -2 4 9 0 797.285 168.874 1 4 9 1 294.492 141.102 1 4 9 -5 2985.89 193.648 -2 -4 -9 -1 2985.89 193.648 1 4 -9 2 5524.34 152.975 1 -4 9 6 5721.36 237.465 -2 4 -9 2 5721.36 237.465 1 4 -9 3 21.9772 141.067 1 4 9 -7 1442.98 210.363 -2 -4 -9 -3 1442.98 210.363 1 4 9 4 7142.97 146.778 1 4 9 -8 11956.2 320.020 -2 -4 -9 -4 11956.2 320.020 1 4 9 5 485.436 126.184 1 -4 -9 9 777.424 268.858 -2 4 9 5 777.424 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767.183 176.216 1 4 14 -5 4058.75 208.115 -2 -4 -14 -1 4058.75 208.115 1 -4 -14 -2 1103.91 232.605 1 4 14 -6 20903.7 309.728 -2 -4 -14 -2 20903.7 309.728 1 4 14 3 463.116 214.998 1 4 14 -7 1365.49 191.458 -2 -4 -14 -3 1365.49 191.458 1 4 14 4 2239.39 171.195 1 -4 14 8 3771.83 245.391 -2 4 -14 4 3771.83 245.391 1 4 14 5 5544.10 170.278 1 -4 -14 9 10599.6 295.095 -2 4 14 5 10599.6 295.095 1 4 14 6 10042.1 158.818 1 -4 -14 10 15514.2 403.678 -2 4 14 6 15514.2 403.678 1 4 14 7 5868.89 139.847 1 -4 -14 11 8985.88 695.831 -2 4 14 7 8985.88 695.831 1 4 14 8 1452.54 136.779 1 -4 -14 12 1822.45 711.251 -2 4 14 8 1822.45 711.251 1 4 14 9 2222.66 143.039 1 -4 -14 13 3274.24 726.795 -2 4 14 9 3274.24 726.795 1 4 -14 10 272.118 142.678 1 -4 -14 -11 16328.5 158.835 1 4 14 12-34.6410 147.468 1 4 14 13 4205.97 169.441 1 4 14 14 1354.49 162.637 1 4 14 15 862.164 168.182 1 4 14 16 831.051 177.193 1 4 14 17 1103.29 166.674 1 4 14 18 2671.87 161.849 1 4 -14 19 97.9966 153.784 1 4 -14 20 252.183 134.915 1 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185.922 1 5 25 4-54.1202 357.000 1 5 25 -8 771.936 218.208 -2 -5 -25 -4 771.936 218.208 1 5 25 5 757.968 306.413 1 -5 -25 9 196.056 235.430 -2 5 25 5 196.056 235.430 1 5 25 6 1567.36 270.304 1 -5 -25 10 1917.51 234.734 -2 5 25 6 1917.51 234.734 1 5 25 7 69.0309 208.323 1 -5 25 11 975.628 271.502 -2 5 -25 7 975.628 271.502 1 5 25 8 788.339 176.317 1 -5 25 12 1884.62 339.767 -2 5 -25 8 1884.62 339.767 1 5 25 9 206.901 188.570 1 -5 25 13 1883.05 329.557 -2 5 -25 9 1883.05 329.557 1 5 25 10 1095.44 188.835 1 -5 25 14 1874.43 415.755 -2 5 -25 10 1874.43 415.755 1 5 25 11 150.788 161.250 1 -5 25 15 238.193 410.500 -2 5 -25 11 238.193 410.500 1 5 25 12 240.180 140.393 1 -5 25 16 205.107 801.943 -2 5 -25 12 205.107 801.943 1 5 25 13 656.141 129.850 1 5 25 14 354.667 144.494 1 -5 -26 17 367.599 156.743 1 5 26 -16 1.29314 131.184 1 -5 -26 15 200.897 137.894 1 5 26 11 245.432 826.342 -2 -5 -26 15 245.432 826.342 1 5 -26 -14 85.8688 146.452 1 5 26 10 546.591 714.376 -2 -5 -26 14 546.591 714.376 1 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1 4 606.058 1429.40 1 6 -1 -9 5150.03 213.472 -2 -6 1 -4 5150.03 213.472 1 -6 -1 10 1355.68 173.158 -2 6 1 5 1355.68 173.158 1 -6 1 -6 57.1094 1714.64 1 6 -1 -11 2258.70 184.554 -2 -6 1 -6 2258.70 184.554 1 -6 1 -7 1531.61 1580.56 1 -6 1 12 4392.04 255.641 -2 6 -1 7 4392.04 255.641 1 -6 -1 -8-251.562 1503.84 1 -6 1 13 3225.20 196.199 -2 6 -1 8 3225.20 196.199 1 -6 1 -9 1126.09 1540.55 1 -6 1 14 4987.37 193.652 -2 6 -1 9 4987.37 193.652 1 -6 1 -10 1963.75 1605.75 1 -6 1 15 3069.68 205.335 -2 6 -1 10 3069.68 205.335 1 -6 1 -11 240.175 1503.89 1 -6 1 16 1999.57 211.397 -2 6 -1 11 1999.57 211.397 1 -6 1 17 2463.70 210.079 -2 6 -1 12 2463.70 210.079 1 -6 -1 18 3174.75 213.470 -2 6 1 13 3174.75 213.470 1 -6 1 19 652.093 218.502 -2 6 -1 14 652.093 218.502 1 6 -1 15 1890.05 300.255 1 -6 1 20 2521.73 242.533 -2 6 -1 15 2521.73 242.533 1 6 1 16 1039.19 270.410 1 -6 1 21 1964.31 281.718 -2 6 -1 16 1964.31 281.718 1 6 -1 17 503.365 223.647 1 -6 1 22 1005.57 314.440 -2 6 -1 17 1005.57 314.440 1 6 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6 11740.9 230.440 1 -6 5 -7 4605.70 1927.71 1 6 5 -12 6270.00 217.694 -2 -6 -5 -7 6270.00 217.694 1 -6 5 -8 1940.81 1966.84 1 6 5 -13 6801.40 211.130 -2 -6 -5 -8 6801.40 211.130 1 -6 -5 -9 5734.87 1524.73 1 -6 5 14 15097.9 288.632 -2 6 -5 9 15097.9 288.632 1 -6 -5 -10 126.076 1599.65 1 -6 5 15 830.408 208.424 -2 6 -5 10 830.408 208.424 1 6 5 11 5797.92 591.838 1 -6 5 16 9225.10 234.571 -2 6 -5 11 9225.10 234.571 1 6 5 12-17.7277 529.216 1 -6 5 17 2241.93 218.840 -2 6 -5 12 2241.93 218.840 1 6 5 13 2260.39 492.563 1 -6 5 18 3720.89 229.667 -2 6 -5 13 3720.89 229.667 1 6 5 14 512.249 400.223 1 -6 5 19 920.229 251.190 -2 6 -5 14 920.229 251.190 1 6 -5 15 1066.26 317.830 1 -6 5 20 722.694 257.512 -2 6 -5 15 722.694 257.512 1 6 5 16 301.674 242.023 1 -6 5 21 1259.17 289.893 -2 6 -5 16 1259.17 289.893 1 6 -5 17 1209.76 176.384 1 -6 5 22 2786.63 367.374 -2 6 -5 17 2786.63 367.374 1 6 -5 18 151.335 151.327 1 -6 5 23 1133.64 446.284 -2 6 -5 18 1133.64 446.284 1 6 -5 19 1241.44 129.463 1 6 -5 20 1067.92 149.738 1 -6 -6 25 169.873 128.183 1 -6 -6 24 296.153 125.417 1 -6 6 -19 2224.45 630.423 -2 6 -6 -24 2224.45 630.423 1 -6 -6 23 175.865 126.544 1 -6 6 -18 543.156 692.770 -2 6 -6 -23 543.156 692.770 1 -6 -6 22-21.5515 129.125 1 -6 6 -17 356.562 763.011 -2 6 -6 -22 356.562 763.011 1 -6 -6 21 1636.85 146.811 1 6 6 16 2378.64 465.302 -2 -6 -6 21 2378.64 465.302 1 -6 6 20 1234.58 139.959 1 -6 6 -15 2011.64 384.044 -2 6 -6 -20 2011.64 384.044 1 -6 6 19 9490.13 268.884 1 6 -6 14 7555.17 398.892 -2 -6 6 19 7555.17 398.892 1 6 6 -18 1510.67 184.015 1 -6 6 -13 2419.07 305.083 -2 6 -6 -18 2419.07 305.083 1 6 6 -17 11543.6 318.305 1 -6 -6 -12 10183.9 291.747 -2 6 6 -17 10183.9 291.747 1 -6 -6 16 4343.99 633.136 1 -6 -6 -11 7649.47 217.997 -2 6 6 -16 7649.47 217.997 1 -6 -6 15 1163.98 517.218 1 6 -6 10 2645.48 193.249 -2 -6 6 15 2645.48 193.249 1 6 6 -14 1606.53 958.417 1 -6 -6 -9 3255.89 193.256 -2 6 6 -14 3255.89 193.256 1 6 6 -13 361.093 980.818 1 -6 6 -8 1878.26 185.350 -2 6 -6 -13 1878.26 185.350 1 6 6 -12 327.266 967.161 1 -6 6 -7 1254.60 189.373 -2 6 -6 -12 1254.60 189.373 1 6 6 -11 15141.5 1299.63 1 6 6 6 21698.7 204.539 -2 -6 -6 11 21698.7 204.539 1 6 6 -10 2107.11 1589.33 1 6 6 5 1560.76 188.753 -2 -6 -6 10 1560.76 188.753 1 6 6 -9 2890.75 1425.04 1 -6 -6 -4 6032.26 208.742 -2 6 6 -9 6032.26 208.742 1 6 6 -8-913.197 1342.54 1 6 6 3 1022.06 182.563 -2 -6 -6 8 1022.06 182.563 1 6 6 -7 18145.0 1345.23 1 -6 6 -2 17893.6 205.716 -2 6 -6 -7 17893.6 205.716 1 6 -6 -6 474.762 1299.29 1 -6 6 -1 4665.95 184.252 -2 6 -6 -6 4665.95 184.252 1 6 6 -5 948.536 1280.45 1 -6 -6 0 1357.90 172.307 -2 6 6 -5 1357.90 172.307 1 6 6 -4 11900.7 1285.40 1 -6 6 1 11720.6 183.795 -2 6 -6 -4 11720.6 183.795 1 6 6 -3 940.387 1023.13 1 -6 6 2 10396.1 189.108 -2 6 -6 -3 10396.1 189.108 1 6 6 -2 14616.9 1597.28 1 -6 6 3 17701.9 198.383 -2 6 -6 -2 17701.9 198.383 1 6 6 -1 5001.48 1610.15 1 -6 6 4 9517.50 192.625 -2 6 -6 -1 9517.50 192.625 1 6 6 0 2138.96 2194.27 1 -6 -6 5 1628.25 158.169 -2 6 6 0 1628.25 158.169 1 6 6 1 7782.83 1557.09 1 -6 -6 6 8110.33 181.728 -2 6 6 1 8110.33 181.728 1 6 -6 2 782.924 1261.59 1 -6 6 7 10913.9 191.455 -2 6 -6 2 10913.9 191.455 1 6 6 3 788.901 1494.07 1 -6 -6 8 1264.17 188.461 -2 6 6 3 1264.17 188.461 1 6 6 4 1906.78 2243.94 1 -6 -6 9 4727.83 269.596 -2 6 6 4 4727.83 269.596 1 -6 -6 10 1232.96 209.255 -2 6 6 5 1232.96 209.255 1 -6 6 -6 4717.22 2494.97 1 -6 -6 11 21487.2 222.826 -2 6 6 6 21487.2 222.826 1 -6 6 -7-1078.84 2580.77 1 -6 -6 12 2108.81 198.106 -2 6 6 7 2108.81 198.106 1 -6 6 -8 221.083 2003.14 1 -6 -6 13 1362.74 202.021 -2 6 6 8 1362.74 202.021 1 -6 6 -9 2066.59 1523.29 1 -6 -6 14 4045.37 218.440 -2 6 6 9 4045.37 218.440 1 -6 -6 -10 2687.81 1653.14 1 -6 6 15 2596.51 217.621 -2 6 -6 10 2596.51 217.621 1 6 6 11 9844.00 597.745 1 -6 6 16 8912.48 285.068 -2 6 -6 11 8912.48 285.068 1 6 6 12 344.853 580.529 1 -6 6 17 5760.52 243.869 -2 6 -6 12 5760.52 243.869 1 6 6 13 947.314 386.594 1 -6 6 18 2139.50 241.305 -2 6 -6 13 2139.50 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6 -7 13 2132.31 321.038 -2 -6 7 18 2132.31 321.038 1 6 7 -17 9152.70 229.259 1 -6 7 -12 9356.67 273.124 -2 6 -7 -17 9356.67 273.124 1 -6 -7 16-104.313 428.748 1 -6 -7 -11 825.375 203.022 -2 6 7 -16 825.375 203.022 1 6 7 -15 2089.62 510.705 1 6 -7 10 2709.03 197.402 -2 -6 7 15 2709.03 197.402 1 6 7 -14 2778.13 986.985 1 -6 7 -9 2756.75 178.626 -2 6 -7 -14 2756.75 178.626 1 6 7 -13 347.773 993.159 1 -6 -7 -8 3335.82 176.792 -2 6 7 -13 3335.82 176.792 1 6 7 -12 166.241 1090.81 1 -6 -7 -7 2429.33 191.808 -2 6 7 -12 2429.33 191.808 1 6 7 -11 1156.77 1801.65 1 -6 -7 -6 1940.63 187.931 -2 6 7 -11 1940.63 187.931 1 6 7 -10 727.734 1791.43 1 6 7 5 1588.37 199.841 -2 -6 -7 10 1588.37 199.841 1 6 7 -9 1504.71 1705.82 1 6 7 4 6671.93 218.164 -2 -6 -7 9 6671.93 218.164 1 6 7 -8 3806.91 1631.71 1 -6 7 -3 9580.08 222.895 -2 6 -7 -8 9580.08 222.895 1 6 7 -7-1084.34 2093.08 1 -6 -7 -2 1548.67 181.098 -2 6 7 -7 1548.67 181.098 1 6 7 -6 1594.45 1571.95 1 6 7 1 1842.74 182.629 -2 -6 -7 6 1842.74 182.629 1 6 7 -5 7949.84 1624.04 1 6 7 0 24935.8 204.639 -2 -6 -7 5 24935.8 204.639 1 6 7 -4 958.453 1801.63 1 6 7 -1 2192.73 165.316 -2 -6 -7 4 2192.73 165.316 1 6 7 -3 4107.08 2047.50 1 6 7 -2 10562.6 187.731 -2 -6 -7 3 10562.6 187.731 1 6 7 -2 12792.3 2249.69 1 -6 7 3 12744.6 186.719 -2 6 -7 -2 12744.6 186.719 1 6 7 -1 1659.91 2056.52 1 -6 7 4 2327.06 169.790 -2 6 -7 -1 2327.06 169.790 1 6 7 0 23741.9 1865.14 1 -6 -7 5 36401.6 212.863 -2 6 7 0 36401.6 212.863 1 6 -7 1 2916.85 1310.07 1 -6 -7 6 2910.13 182.136 -2 6 7 1 2910.13 182.136 1 6 7 2-283.525 1564.59 1 -6 7 7 1826.09 199.214 -2 6 -7 2 1826.09 199.214 1 6 7 3 6783.50 1290.39 1 -6 -7 8 13606.9 242.517 -2 6 7 3 13606.9 242.517 1 6 7 4 7763.59 1628.63 1 6 7 -9 9965.38 233.288 -2 -6 -7 -4 9965.38 233.288 1 -6 -7 10 1067.48 196.267 -2 6 7 5 1067.48 196.267 1 -6 7 -6-831.145 2417.07 1 -6 -7 11 2188.73 206.731 -2 6 7 6 2188.73 206.731 1 -6 7 -7 3033.69 2671.43 1 -6 -7 12 4434.97 198.897 -2 6 7 7 4434.97 198.897 1 -6 7 -8 1506.02 2855.18 1 6 7 -13 4032.21 205.252 -2 -6 -7 -8 4032.21 205.252 1 -6 7 -9 1228.10 1587.30 1 -6 -7 14 1803.63 204.011 -2 6 7 9 1803.63 204.011 1 -6 -7 -10 1665.06 1899.98 1 -6 -7 15 2499.21 220.111 -2 6 7 10 2499.21 220.111 1 6 7 11 291.553 595.007 1 -6 7 16 1725.72 247.350 -2 6 -7 11 1725.72 247.350 1 6 7 12 2971.83 585.980 1 -6 7 17 6680.74 252.612 -2 6 -7 12 6680.74 252.612 1 6 7 13 1383.07 569.608 1 -6 7 18 2701.29 226.094 -2 6 -7 13 2701.29 226.094 1 6 7 14 520.371 362.765 1 -6 7 19 10394.3 310.235 -2 6 -7 14 10394.3 310.235 1 6 7 15 114.594 235.955 1 -6 7 20 414.133 298.126 -2 6 -7 15 414.133 298.126 1 6 7 16 790.101 196.851 1 -6 7 21 2010.92 349.150 -2 6 -7 16 2010.92 349.150 1 6 -7 17 770.627 162.772 1 -6 7 22 2058.15 468.325 -2 6 -7 17 2058.15 468.325 1 6 7 18 21.2732 148.974 1 -6 7 23 1172.98 776.826 -2 6 -7 18 1172.98 776.826 1 6 -7 19 557.803 123.688 1 -6 -8 25-9.63647 222.607 1 -6 -8 24 241.456 129.991 1 -6 8 -19 1175.73 590.861 -2 6 -8 -24 1175.73 590.861 1 -6 -8 23 25.1541 134.298 1 -6 8 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2305.21 181.891 1 6 8 -10-573.518 1789.19 1 6 8 5 1030.09 199.019 -2 -6 -8 10 1030.09 199.019 1 6 8 -9-1219.96 1689.25 1 -6 -8 -4 773.838 195.610 -2 6 8 -9 773.838 195.610 1 6 8 -8 6435.17 2299.34 1 -6 -8 -3 6214.92 214.874 -2 6 8 -8 6214.92 214.874 1 6 8 -7 648.228 2111.15 1 -6 -8 -2 219.857 183.542 -2 6 8 -7 219.857 183.542 1 6 8 -6 3313.18 2147.30 1 -6 -8 -1 5472.96 212.639 -2 6 8 -6 5472.96 212.639 1 6 8 -5 3735.55 1924.05 1 -6 -8 0 3773.65 192.235 -2 6 8 -5 3773.65 192.235 1 -6 8 1 22041.3 231.741 -2 6 -8 -4 22041.3 231.741 1 6 8 -3-538.742 2185.53 1 -6 -8 2 446.920 169.818 -2 6 8 -3 446.920 169.818 1 6 8 -2-743.110 2120.42 1 -6 8 3 253.711 177.309 -2 6 -8 -2 253.711 177.309 1 -6 8 1 11632.0 2652.16 1 -6 -8 4 38724.1 239.806 -2 6 8 -1 38724.1 239.806 1 6 8 0 1759.42 1670.64 1 -6 -8 5 4627.38 198.689 -2 6 8 0 4627.38 198.689 1 6 8 1 2745.31 1693.87 1 -6 8 6 6423.27 215.284 -2 6 -8 1 6423.27 215.284 1 6 8 2-153.934 1604.17 1 -6 -8 7 271.810 185.477 -2 6 8 2 271.810 185.477 1 6 8 3-382.372 1609.58 1 -6 -8 8 3901.42 189.023 -2 6 8 3 3901.42 189.023 1 6 8 4-485.713 1575.07 1 -6 8 9 842.205 181.670 -2 6 -8 4 842.205 181.670 1 -6 -8 10 520.471 187.518 -2 6 8 5 520.471 187.518 1 -6 8 -6 182.244 2456.90 1 -6 -8 11 1709.07 195.843 -2 6 8 6 1709.07 195.843 1 -6 8 -7-829.448 2743.42 1 -6 -8 12 3540.04 212.507 -2 6 8 7 3540.04 212.507 1 -6 8 -8 307.033 2924.58 1 -6 -8 13 2036.76 203.405 -2 6 8 8 2036.76 203.405 1 6 8 9 689.826 1567.60 1 -6 -8 14 806.440 205.072 -2 6 8 9 806.440 205.072 1 6 8 10 15941.8 691.903 1 -6 -8 15 16597.6 250.289 -2 6 8 10 16597.6 250.289 1 6 8 11 673.796 597.047 1 -6 -8 16 1026.77 213.034 -2 6 8 11 1026.77 213.034 1 6 8 12-275.929 574.481 1 -6 8 17 1834.55 211.039 -2 6 -8 12 1834.55 211.039 1 6 8 13 163.916 335.630 1 -6 8 18 924.602 241.852 -2 6 -8 13 924.602 241.852 1 6 8 14-208.761 259.847 1 -6 8 19 460.902 266.071 -2 6 -8 14 460.902 266.071 1 6 8 15 3347.91 222.310 1 -6 8 20 3896.83 335.297 -2 6 -8 15 3896.83 335.297 1 6 8 16 270.919 202.617 1 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898.332 127.368 2 2 3 27 568.903 134.316 2 -2 -4 29 486.158 134.800 2 -2 -4 28 113.727 118.210 2 -2 4 27 551.497 126.680 2 -2 4 26 1533.96 130.447 2 -2 4 25 43.9000 142.824 2 -2 4 24 234.510 155.708 2 -2 -4 23 33.0434 165.625 2 -2 4 22 2193.29 178.359 2 -2 -4 21 402.967 173.820 2 -2 -4 20 2948.26 178.784 2 -2 4 19 6869.94 195.136 2 -2 4 18 13.7347 165.337 2 -2 4 17 14655.4 215.641 2 -2 4 16 265.028 218.940 2 -2 4 15-200.952 253.192 2 -2 -4 14 821.290 535.881 2 -2 4 13 1180.03 352.795 2 -2 4 12 246.225 569.442 2 -2 -4 11 3824.73 623.609 2 -2 -4 10-163.283 755.868 2 -2 -4 9 3846.35 435.689 2 -2 -4 8 3078.60 564.151 2 2 -4 -7 2030.51 784.820 2 2 -4 -5 17930.9 241.055 2 -2 -4 4 32146.2 348.712 2 2 4 -3 14437.2 254.747 2 2 -4 -2 44379.0 244.393 2 -2 -4 1 8458.04 373.895 2 -2 4 0 9238.13 460.686 2 -2 -4 -1 22825.8 453.129 2 -2 -4 -2 6337.36 302.630 2 -2 -4 -6 2732.53 1356.53 2 -2 -4 -7 9792.44 1550.83 2 -2 -4 -8 1273.52 865.038 2 -2 -4 -9 4609.41 697.799 2 -2 -4 -10 8116.31 910.915 2 -2 -4 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158.780 2 -2 -6 22-41.9084 168.282 2 -2 -6 21 3185.75 186.830 2 -2 -6 20 300.251 184.310 2 -2 -6 19 6293.56 229.958 2 -2 -6 18 1352.79 205.774 2 -2 6 17 9661.41 257.866 2 -2 6 16 1279.99 239.231 2 -2 6 15 2839.66 311.277 2 -2 6 14 525.862 371.735 2 -2 6 13 89.0093 349.468 2 -2 -6 11 3462.74 910.940 2 -2 -6 10 2913.19 977.770 2 2 -6 -9 1628.42 591.285 2 2 -6 -8 2366.21 803.382 2 2 6 -6 39752.1 731.327 2 2 6 -4 26777.6 441.397 2 -2 -6 3 2817.19 175.847 2 -2 -6 2 15125.5 461.315 2 -2 -6 1 28847.3 743.849 2 -2 6 0 28038.9 345.843 2 -2 -6 -1 48722.5 797.551 2 -2 -6 -2 39.4071 385.711 2 -2 -6 -3 1953.98 658.872 2 -2 -6 -4 1116.01 779.784 2 2 -6 6 1121.50 295.174 2 -2 -6 -7 39022.7 1492.52 2 -2 -6 -8-451.720 1221.80 2 -2 -6 -9 24.2057 905.877 2 -2 -6 -10 317.485 757.771 2 -2 -6 -11 2194.39 812.892 2 -2 -6 -12 5493.49 418.811 2 -2 -6 -13 12809.5 370.710 2 -2 -6 -14 1096.98 366.507 2 -2 -6 -15 248.103 374.054 2 -2 -6 -16-86.1904 243.110 2 2 -6 17 4529.22 289.068 2 -2 -6 -18 347.727 263.711 2 2 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5653.53 370.727 2 -2 -7 -3 85.9896 508.545 2 -2 -7 -4-80.1741 751.318 2 -2 -7 -9 6773.41 826.736 2 -2 -7 -10 6420.97 837.215 2 -2 -7 -11 982.726 805.172 2 -2 -7 -12 1045.51 1018.36 2 -2 -7 -13 8517.29 482.399 2 -2 -7 -14 328.334 442.690 2 -2 -7 -15 50.3663 369.454 2 -2 -7 -16 225.938 309.678 2 -2 -7 -17 844.585 225.413 2 2 7 18 1789.11 256.387 2 -2 -7 -19 7267.38 204.213 2 2 -7 20 153.755 172.051 2 2 -7 21 3169.89 177.622 2 2 7 22 89.0988 150.354 2 2 7 23 200.117 150.923 2 2 7 24 656.891 152.011 2 2 7 25 2020.04 147.438 2 2 7 26 601.700 136.678 2 2 -7 27 150.623 134.854 2 -2 -8 28 286.805 132.551 2 -2 8 27 2716.42 132.310 2 -2 8 26-55.5827 142.732 2 -2 8 25 1417.96 146.650 2 -2 8 24 35.1606 147.099 2 -2 -8 23 116.450 155.027 2 -2 -8 22 359.321 148.181 2 -2 8 21 177.759 162.076 2 -2 -8 20 293.379 246.687 2 -2 8 19 3847.70 263.799 2 -2 8 18 5877.90 450.103 2 -2 8 17 542.676 311.596 2 -2 8 16-215.182 301.455 2 -2 8 15 865.231 652.529 2 -2 8 14-160.478 449.942 2 -2 8 13 286.601 418.453 2 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133.988 2 -2 -9 25 3359.71 146.297 2 -2 9 24 1446.31 154.457 2 -2 -9 23 2888.47 156.604 2 -2 -9 22 168.408 155.359 2 -2 -9 21 604.602 195.246 2 -2 9 20 3253.39 254.646 2 -2 9 19 4905.06 319.892 2 -2 9 18 134.716 320.641 2 -2 9 17-127.053 353.515 2 -2 9 16-217.320 334.431 2 -2 9 15 6630.03 525.564 2 -2 9 14 349.974 367.178 2 -2 9 13 195.666 415.861 2 -2 -9 12 477.873 389.328 2 -2 -9 11 5322.30 388.663 2 2 -9 -10 15951.8 980.989 2 2 -9 -9 5974.12 1018.74 2 2 9 -8 2900.46 556.307 2 2 9 -7 10848.1 562.500 2 2 -9 -6 16858.6 521.923 2 2 9 -5 1207.77 676.911 2 -2 -9 4 17691.2 418.569 2 2 9 -3 1687.71 157.057 2 -2 -9 2 12777.7 413.934 2 -2 -9 1 13894.2 676.441 2 -2 -9 0 10519.7 175.952 2 -2 -9 -1 6.73181 455.228 2 -2 -9 -2 3366.69 368.288 2 -2 -9 -3 6994.65 660.918 2 -2 -9 -4 27001.2 1120.06 2 -2 -9 -7-404.878 1308.12 2 -2 -9 -8 4525.45 1357.33 2 -2 -9 -9 1707.55 1018.55 2 -2 -9 -10 5059.37 1061.96 2 -2 -9 -11 1918.61 880.645 2 -2 -9 -12 6990.98 1275.07 2 -2 -9 -13-113.011 1284.83 2 -2 -9 -14 1863.79 504.673 2 -2 -9 -15 65.3655 336.941 2 2 -9 16 3111.89 332.043 2 2 -9 17 3549.20 318.224 2 2 -9 18 7864.42 316.238 2 2 -9 19 346.941 220.383 2 2 -9 20 2349.54 192.360 2 2 9 21 544.884 184.062 2 2 -9 22 888.071 156.440 2 2 9 23 215.929 159.145 2 2 9 24 253.085 148.295 2 2 9 25 705.912 140.245 2 2 -9 26 570.928 131.000 2 -2 -10 28 59.6229 122.936 2 -2 10 27 174.677 131.208 2 -2 10 26 796.327 134.345 2 -2 10 25 199.986 150.203 2 -2 -10 24 1931.93 148.208 2 -2 -10 23 1214.67 140.376 2 -2 10 22 1791.54 168.523 2 -2 10 21 151.372 206.859 2 -2 -10 20 4177.50 236.291 2 -2 -10 19 502.776 300.577 2 -2 10 18 404.205 294.876 2 -2 10 17 28.6197 356.881 2 -2 10 16 4312.38 346.135 2 -2 10 15 3239.69 398.290 2 -2 10 14 1037.86 362.870 2 -2 10 13 10039.2 435.939 2 -2 -10 12-4.19397 389.103 2 -2 -10 11 1796.95 369.235 2 2 -10 -10 12011.9 1050.65 2 2 -10 -9 1778.73 1072.96 2 2 10 -8 418.265 645.377 2 2 10 -7 189.759 428.642 2 -2 10 6 878.242 396.681 2 -2 -10 5 24454.3 389.806 2 -2 -10 4 413.972 615.836 2 -2 -10 3 7363.72 288.943 2 2 -10 -2-63.1331 198.297 2 -2 -10 1 38922.1 613.462 2 -2 10 0 202.853 203.958 2 -2 -10 -1 262.467 456.145 2 -2 -10 -2 4940.65 401.184 2 -2 -10 -7 5001.33 1425.46 2 -2 -10 -8 1629.32 1328.06 2 -2 -10 -9 677.263 1376.64 2 -2 -10 -10 587.978 870.617 2 -2 -10 -11 186.980 870.528 2 -2 -10 -12 6181.67 1343.09 2 -2 -10 -13 1717.43 1418.15 2 -2 -10 -14 747.396 532.084 2 -2 -10 -15 223.761 470.320 2 2 -10 16 1908.16 337.416 2 2 -10 17 5284.23 292.343 2 2 -10 18 1899.07 296.546 2 -2 -10 -19 9095.39 284.450 2 2 10 20 1809.22 187.469 2 2 -10 21-34.4826 181.161 2 2 -10 22 349.686 163.012 2 2 10 23 1908.30 170.479 2 2 10 24 154.826 143.857 2 2 -10 25-75.0439 141.343 2 2 -10 26 165.108 126.767 2 -2 -11 28 193.313 124.690 2 -2 11 27 40.8826 125.487 2 -2 11 26 243.908 138.391 2 -2 11 25 246.955 155.164 2 -2 -11 24 47.5463 147.430 2 -2 -11 23 2945.32 150.602 2 -2 -11 22 1146.57 171.293 2 -2 -11 21-139.196 183.981 2 -2 -11 20-68.5869 253.231 2 -2 -11 19 781.559 336.702 2 -2 11 18-80.4843 337.854 2 -2 11 17 1677.40 364.389 2 -2 11 16 90.2576 300.634 2 -2 11 14 975.857 464.451 2 -2 11 13 1666.16 410.874 2 -2 11 12 2618.11 364.437 2 -2 11 11 7542.18 363.278 2 2 -11 -10 1048.71 1067.41 2 2 -11 -9 2871.21 1176.26 2 2 -11 -8 1850.98 1223.62 2 2 -11 -6 535.829 395.188 2 -2 -11 5 10010.5 428.260 2 -2 -11 4 1607.37 696.694 2 -2 -11 3 19696.7 387.856 2 -2 -11 2 39.2498 376.364 2 -2 -11 1 7861.30 701.948 2 2 -11 0 3886.69 219.664 2 2 -11 1 1924.21 234.515 2 -2 -11 -2-102.136 762.795 2 -2 -11 -8 123.161 1358.49 2 -2 -11 -9 1002.42 1029.76 2 -2 -11 -10 4615.70 899.393 2 -2 -11 -11 10917.2 974.256 2 -2 -11 -12-765.686 1282.94 2 -2 -11 -13 4465.59 1368.05 2 -2 -11 -14 554.999 501.837 2 2 -11 15 656.636 358.236 2 2 -11 16 1891.23 391.129 2 2 -11 17 554.360 324.534 2 2 -11 18 2057.24 253.939 2 2 -11 19 1054.18 205.609 2 2 -11 20 1612.33 200.287 2 2 11 21 1130.10 196.811 2 2 -11 22 61.6802 172.096 2 2 -11 23 141.779 167.088 2 2 -11 24 1233.93 150.338 2 2 -11 25 530.669 133.279 2 2 -11 26 149.316 121.701 2 -2 -12 28-134.033 272.463 2 -2 12 27 270.196 120.192 2 -2 12 26 111.032 132.762 2 -2 -12 25 341.673 146.858 2 -2 -12 24 121.814 152.005 2 -2 12 23 1861.64 153.680 2 -2 12 22 100.917 166.631 2 -2 -12 21 1851.71 187.588 2 -2 -12 20 234.888 252.131 2 -2 12 19-169.567 306.526 2 -2 12 18 1092.33 372.909 2 -2 12 17 316.793 290.739 2 -2 12 16 5823.95 326.418 2 -2 12 15 243.402 448.854 2 -2 12 14 1326.84 460.788 2 -2 -12 12 978.271 374.509 2 -2 -12 11 3598.19 1354.79 2 2 -12 -10 1498.76 1126.08 2 2 -12 -9 1459.37 1240.38 2 2 -12 -8 2620.82 1326.14 2 -2 -12 5 950.873 383.339 2 -2 -12 4 8082.81 788.859 2 -2 -12 3 44049.0 1152.84 2 -2 -12 2 23681.7 515.362 2 -2 -12 1 5455.74 545.874 2 -2 12 0 69.5686 259.770 2 -2 -12 -1 20546.9 710.668 2 2 -12 2 220.675 574.275 2 -2 -12 -7-295.004 1408.92 2 -2 -12 -9-186.782 1079.69 2 -2 -12 -10 593.830 1106.37 2 -2 -12 -11 127.458 989.755 2 -2 -12 -12 1444.71 1411.23 2 -2 -12 -13 3285.65 1471.85 2 -2 -12 -14 1611.87 501.516 2 2 -12 15 362.888 477.736 2 -2 -12 -16 61.6325 319.663 2 2 -12 17 6334.83 362.749 2 2 -12 18 89.7307 256.280 2 2 -12 19 63.0836 248.992 2 2 -12 20 996.924 194.771 2 2 -12 21 954.723 196.280 2 2 -12 22-43.8154 161.809 2 2 -12 23-23.8563 151.398 2 2 -12 24 545.382 147.441 2 2 -12 25-113.650 129.997 2 2 -12 26 639.884 124.158 2 -2 13 27 532.360 119.999 2 -2 13 26 203.903 128.693 2 -2 13 25 675.445 133.730 2 -2 -13 24 230.753 145.461 2 -2 13 23 89.9831 149.001 2 -2 13 22-40.9000 168.477 2 -2 13 21 3546.52 212.812 2 -2 13 20 988.565 270.521 2 -2 13 19 85.4078 252.374 2 -2 13 18 781.699 386.614 2 -2 13 17 476.588 299.790 2 -2 13 16-40.0137 287.385 2 -2 13 15-146.333 395.211 2 -2 13 14 254.898 350.877 2 -2 13 13 11107.3 433.287 2 -2 -13 12 470.860 1501.34 2 -2 -13 11 2730.81 1494.26 2 2 -13 -10 8037.66 1282.72 2 2 -13 -5 1985.49 636.082 2 -2 -13 4 3361.63 589.818 2 -2 -13 3 384.874 924.549 2 -2 -13 2 5818.74 525.374 2 -2 -13 1 14290.8 801.976 2 -2 13 0 2703.29 293.679 2 2 -13 1 5091.73 391.392 2 2 -13 2 2039.32 824.602 2 2 -13 3 1333.31 960.484 2 2 -13 4 476.593 1102.47 2 -2 -13 -8-272.176 1792.71 2 -2 -13 -9 3320.46 1162.85 2 -2 -13 -10 4404.31 1122.03 2 -2 -13 -11 842.021 1004.00 2 -2 -13 -12 2009.18 1387.31 2 -2 -13 -13 206.745 1412.10 2 2 -13 14 557.391 1543.03 2 -2 -13 -15 136.325 361.678 2 2 -13 16 1598.84 356.166 2 2 -13 17 956.578 390.350 2 2 -13 18 1930.03 252.491 2 2 13 19 1827.46 260.125 2 2 -13 20 408.150 226.469 2 2 -13 21 291.399 182.914 2 2 -13 22 668.780 177.960 2 2 -13 23 2842.29 157.243 2 2 -13 24 678.153 142.503 2 2 -13 25 41.3341 127.567 2 2 -13 26 210.935 226.325 2 -2 -14 27 64.2679 137.769 2 -2 14 26 276.472 124.232 2 -2 -14 25 113.485 128.297 2 -2 -14 24-64.2694 146.107 2 -2 14 23 92.3744 149.217 2 -2 14 22 126.555 161.006 2 -2 14 21 802.021 240.860 2 -2 14 20 251.431 294.618 2 -2 14 19 1190.48 334.177 2 -2 14 18 225.852 297.162 2 -2 14 17 6475.31 396.155 2 -2 14 16 3291.23 307.458 2 -2 14 15 1360.74 377.872 2 -2 14 14 3682.49 455.706 2 -2 -14 12 909.543 1572.19 2 2 -14 -10 1403.20 1290.18 2 2 -14 -9 2783.70 1433.92 2 -2 -14 4 22840.0 1004.50 2 -2 -14 3 4793.80 706.935 2 -2 -14 1 6607.61 613.041 2 -2 -14 0 14352.6 965.285 2 -2 -14 -1 850.848 661.496 2 2 -14 3 817.840 916.813 2 2 -14 4-181.058 1085.26 2 2 -14 5 448.377 1186.71 2 -2 -14 -9 350.995 1489.52 2 -2 -14 -10 109.240 1483.48 2 -2 -14 -11 1278.09 1597.08 2 -2 -14 -12-110.542 1490.48 2 2 -14 13 347.078 1215.54 2 2 -14 14 1334.61 534.713 2 -2 -14 -15 90.5738 520.074 2 2 -14 16 1624.48 354.495 2 2 -14 17 771.757 390.634 2 2 -14 18 1998.54 239.658 2 2 -14 19-60.7973 245.618 2 2 -14 20 516.806 236.910 2 2 -14 21 601.208 198.943 2 2 -14 22 312.070 168.109 2 2 -14 23 998.303 149.276 2 2 -14 24 1153.91 136.859 2 2 -14 25 236.851 119.632 2 -2 -15 27 449.517 133.977 2 -2 15 26 208.571 140.225 2 -2 -15 25 405.305 129.451 2 -2 15 24 817.513 145.004 2 -2 15 23-51.9712 147.360 2 -2 -15 22 1694.00 160.243 2 -2 15 21 62.7248 243.446 2 -2 15 20 1237.74 247.786 2 -2 15 19 285.183 324.064 2 -2 15 18-28.7140 304.116 2 -2 15 17 979.207 313.740 2 -2 15 16 314.256 398.550 2 -2 15 15 1359.29 757.184 2 -2 15 14 439.338 709.818 2 -2 -15 12 2066.97 1620.05 2 2 -15 -10 4076.98 1462.98 2 2 -15 -9 2733.48 1504.78 2 -2 -15 4 712.201 869.539 2 -2 -15 3 3404.51 718.639 2 -2 15 1 177.885 600.588 2 -2 -15 0 884.429 904.797 2 -2 -15 -1 6479.91 1062.58 2 2 -15 5-225.147 1163.26 2 2 -15 6 294.440 1257.15 2 2 -15 7 1001.38 1419.35 2 -2 -15 -9-179.522 1531.78 2 -2 -15 -10 835.605 1621.57 2 -2 -15 -11 11.9216 936.052 2 2 -15 12 984.901 1209.40 2 2 -15 13-243.264 1307.41 2 -2 -15 -14 5056.34 2521.23 2 2 -15 15 1375.63 528.707 2 2 -15 16 5141.10 544.163 2 2 -15 17 204.912 315.098 2 2 -15 18 400.526 610.173 2 2 -15 19 804.799 262.530 2 2 -15 20-54.7797 220.451 2 2 -15 21-42.8262 194.523 2 2 -15 22 932.595 172.941 2 2 -15 23 254.185 144.524 2 2 -15 24 935.986 138.740 2 2 -15 25 1423.06 127.871 2 -2 16 26 733.436 133.067 2 -2 -16 25 46.9776 138.244 2 -2 16 24 63.3141 139.824 2 -2 16 23 385.732 149.045 2 -2 16 22 1605.90 186.364 2 -2 16 21 516.952 214.235 2 -2 16 20 570.902 247.595 2 -2 16 19 108.649 253.627 2 -2 16 18 574.643 378.147 2 -2 16 17 324.078 385.150 2 -2 16 16 1453.26 797.208 2 -2 16 15 1170.29 765.899 2 -2 -16 12 1663.04 1829.39 2 2 -16 -10 3919.08 1430.19 2 -2 -16 3 1716.59 733.669 2 -2 -16 2 901.885 1174.74 2 -2 -16 0 32.6018 939.929 2 -2 -16 -1 5576.37 1097.61 2 2 -16 6 1697.96 1292.27 2 2 -16 7 449.631 1380.43 2 -2 -16 -8 1885.64 1107.90 2 -2 -16 -9 164.535 1136.37 2 -2 -16 -10 2376.48 1157.68 2 -2 -16 -11 1386.63 992.198 2 2 -16 12 4665.79 1306.56 2 2 -16 13 151.072 1366.18 2 2 -16 14-546.555 1722.97 2 2 -16 15 804.576 504.900 2 2 -16 16 905.484 357.885 2 2 -16 17 429.231 337.044 2 2 -16 18 3.85780 426.904 2 2 -16 19 790.753 265.883 2 2 -16 20 1544.66 234.160 2 2 -16 21 171.907 188.618 2 2 -16 22 1473.73 158.732 2 2 -16 23 50.0555 139.396 2 2 -16 24 62.3870 131.483 2 2 16 25 477.718 237.722 2 -2 -17 26 641.452 130.786 2 -2 -17 25 556.966 129.685 2 -2 17 24 739.610 147.687 2 -2 17 23 77.2361 149.217 2 -2 -17 22 484.784 172.718 2 -2 -17 21-278.945 216.152 2 -2 17 20-78.6043 289.572 2 2 -17 -19 829.659 339.168 2 -2 17 18 3538.05 392.580 2 -2 17 17 2766.49 395.859 2 -2 17 16 461.369 782.275 2 -2 -17 12 773.472 1996.17 2 -2 -17 3 4871.49 788.211 2 -2 -17 0-202.713 984.077 2 -2 -17 -9 1917.57 1685.76 2 -2 -17 -10 1071.61 1235.26 2 2 -17 11 896.262 1458.67 2 2 -17 12 2345.95 1350.73 2 2 -17 13-522.057 1399.92 2 2 -17 14 887.802 1792.49 2 -2 -17 -15 657.241 500.551 2 -2 -17 -16 895.438 540.683 2 2 -17 17 168.324 381.826 2 2 -17 18 225.830 334.553 2 2 -17 19 418.286 251.529 2 2 -17 20 370.307 184.556 2 2 -17 21 588.190 202.415 2 2 -17 22 93.0978 164.628 2 2 -17 23 497.251 142.762 2 2 -17 24 334.951 131.097 2 -2 -18 26 143.345 175.275 2 -2 -18 25 580.969 129.690 2 -2 18 24 473.862 135.642 2 -2 18 23 344.301 143.798 2 -2 -18 22 346.101 171.031 2 2 18 -21 509.468 218.927 2 -2 18 20 856.172 287.251 2 -2 18 19 849.878 345.268 2 -2 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3974.03 800.482 2 -2 -19 12 2845.82 2206.03 2 -2 -19 -9 393.850 1893.14 2 -2 -19 -10 2836.80 1996.42 2 2 -19 11 5087.25 1859.97 2 2 -19 12-850.533 1894.28 2 2 -19 13-13.8830 2003.13 2 -2 -19 -14 3828.78 2924.49 2 2 -19 15 2621.28 464.094 2 2 -19 16 208.124 384.172 2 2 -19 17-152.249 312.781 2 2 -19 18-547.884 359.594 2 2 -19 19 1548.82 238.423 2 2 19 20 107.616 212.499 2 2 -19 21 232.940 172.677 2 2 -19 22 448.851 147.952 2 2 -19 23-0.45823 135.707 2 -2 -20 25 145.268 135.836 2 -2 20 24 140.520 118.679 2 -2 20 23 124.081 134.446 2 -2 -20 22 272.797 155.806 2 2 20 -21 518.236 233.083 2 -2 20 20-152.668 267.439 2 -2 20 19 1867.15 380.098 2 -2 20 18 3302.14 405.069 2 -2 20 17 474.482 535.706 2 -2 20 16 237.357 797.327 2 -2 20 15 14829.5 840.565 2 2 -20 -9-837.982 1800.32 2 2 -20 -1 125.914 1255.55 2 -2 -20 -8 348.315 2047.70 2 -2 -20 -9 5999.73 2046.29 2 -2 -20 -10 1539.26 2083.04 2 2 -20 11 2714.50 2719.28 2 2 -20 12 523.811 1961.36 2 -2 -20 -13 1181.69 2939.26 2 -2 -20 -14-2236.67 2977.30 2 2 -20 16-592.360 510.335 2 2 -20 17 5276.34 389.872 2 2 -20 18 408.146 398.079 2 -2 -20 -19-45.2460 278.461 2 2 20 20 1088.98 208.405 2 2 20 21 183.003 186.759 2 2 -20 22 550.525 152.845 2 2 -20 23 281.791 143.522 2 -2 -21 24 55.3521 140.246 2 -2 21 23 147.906 128.561 2 -2 -21 22 211.678 142.934 2 2 21 -21 168.793 172.537 2 -2 21 20 900.072 233.954 2 -2 21 19 200.964 327.653 2 -2 21 18 1584.02 348.032 2 -2 21 17 853.887 538.341 2 -2 21 16-0.30347 798.385 2 2 -21 -15 541.347 420.497 2 -2 -21 -8 3670.28 2193.24 2 -2 -21 -9 3614.00 2159.75 2 -2 -21 -11-714.666 2716.39 2 2 -21 12-171.498 3037.52 2 -2 -21 -13 331.204 2929.01 2 2 -21 16 1974.54 386.801 2 2 -21 17 598.161 378.201 2 2 -21 18-217.293 501.941 2 2 21 19 278.697 229.214 2 2 21 20 444.845 201.992 2 2 21 21 629.266 185.679 2 2 -21 22 648.761 140.574 2 -2 -22 24-114.045 171.146 2 -2 22 23 18.9264 134.991 2 -2 22 22 213.848 142.705 2 2 22 -21 243.810 152.089 2 -2 22 20-149.088 264.315 2 -2 22 19 882.676 320.319 2 -2 22 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586.351 2 -3 0 -5 34880.7 522.312 2 -3 0 -7 74193.0 240.863 2 -3 0 -9 4116.86 130.728 2 -3 0 -11 5137.05 149.076 2 -3 0 -13 1004.29 145.212 2 -3 0 -15 10168.9 218.989 2 -3 0 -17 3211.65 196.626 2 3 0 19 2902.23 182.601 2 3 0 21 626.989 244.880 2 3 0 23 2077.62 241.043 2 3 0 25 348.465 182.635 2 -3 1 29-55.4296 130.685 2 -3 -1 28 607.347 121.584 2 -3 -1 27 90.4321 126.753 2 -3 1 26 389.226 125.515 2 -3 1 25 745.571 140.637 2 -3 -1 24 3326.25 141.260 2 -3 1 23 140.464 147.877 2 -3 -1 22 4511.09 153.069 2 -3 1 21 144.136 147.760 2 -3 -1 20 1552.27 152.384 2 -3 -1 19 2683.34 143.467 2 -3 1 18 1411.84 141.393 2 -3 1 17 3760.14 136.148 2 -3 1 16 2088.21 127.090 2 -3 -1 15 12833.7 134.846 2 -3 -1 14-51.6428 108.345 2 -3 -1 13 349.801 105.149 2 -3 -1 12 768.619 97.4290 2 -3 -1 11 116.355 106.540 2 -3 -1 10 8264.72 128.604 2 -3 1 9 6511.75 215.204 2 -3 1 8 1759.07 351.086 2 -3 -1 7 3232.17 234.257 2 -3 1 6 339.950 417.263 2 -3 -1 5 1555.46 454.780 2 -3 -1 4 4900.66 252.538 2 -3 -1 3 1741.03 269.936 2 -3 -1 2 14103.9 319.028 2 -3 -1 1 1013.52 265.409 2 -3 -1 0 27145.2 337.937 2 -3 -1 -1 8400.12 183.628 2 -3 -1 -2 26805.7 445.319 2 -3 -1 -3 1662.83 326.088 2 -3 -1 -4 2355.49 337.415 2 -3 -1 -5 30731.9 395.528 2 -3 -1 -6 29440.8 402.574 2 -3 -1 -7 5766.57 124.987 2 -3 -1 -8 1762.36 97.8205 2 -3 -1 -9 139.848 90.3117 2 3 1 10 8504.51 95.7755 2 3 1 11 3243.37 87.5737 2 3 1 12 5876.85 101.976 2 3 1 13 1443.08 100.924 2 3 -1 14-32.4079 110.441 2 3 -1 15 297.614 113.057 2 3 1 16 3486.34 129.388 2 3 1 17 5930.73 135.795 2 3 1 18 91.4663 130.700 2 3 1 19 136.592 140.011 2 3 1 20 88.2368 139.614 2 3 1 21 268.717 159.418 2 3 1 22 2788.81 183.301 2 3 1 23 846.290 155.157 2 3 1 24 92.7770 141.558 2 3 1 25 160.899 126.483 2 3 1 26 236.520 110.883 2 -3 2 29 189.170 136.994 2 -3 -2 28 134.461 120.479 2 -3 2 27 395.133 124.294 2 -3 2 26 140.810 136.414 2 -3 2 25 1997.71 137.005 2 -3 2 24 425.271 149.831 2 -3 2 23 2782.05 166.147 2 -3 2 22 910.673 146.695 2 -3 2 21 4975.33 155.399 2 -3 -2 20 3097.07 152.359 2 -3 2 19 4415.32 148.480 2 -3 -2 18 2017.95 136.219 2 -3 2 17 393.206 128.546 2 -3 -2 16 200.374 124.514 2 -3 2 15 1305.42 131.384 2 -3 -2 14 57.3910 109.015 2 -3 -2 13 1435.58 102.836 2 -3 -2 12 2670.92 102.604 2 -3 2 11 3670.48 108.223 2 -3 2 10 436.444 127.068 2 -3 2 9 293.612 232.171 2 -3 2 8 14877.5 413.320 2 -3 2 7 1748.18 344.128 2 -3 -2 6 21132.0 505.170 2 -3 -2 5 313.859 401.155 2 -3 -2 4 48226.5 571.842 2 -3 -2 3 2486.58 419.251 2 -3 -2 2 8027.21 338.977 2 -3 -2 1 41056.6 334.532 2 -3 -2 0 2263.43 273.881 2 -3 -2 -1 4334.43 267.318 2 -3 -2 -2 2279.93 358.376 2 -3 -2 -3 422.235 325.326 2 -3 -2 -4 12590.1 380.487 2 -3 -2 -5 5079.21 359.744 2 -3 -2 -6 7202.17 235.308 2 -3 -2 -7 9067.32 131.534 2 -3 -2 -8 132.891 92.6315 2 -3 -2 -9 5458.63 96.2782 2 3 2 10 3849.78 88.1679 2 3 2 11 3184.08 88.2320 2 3 2 12 4987.60 108.226 2 3 -2 13 7245.86 107.082 2 3 -2 14 713.801 113.004 2 3 -2 15 2365.35 125.262 2 3 2 16 121.237 133.705 2 3 2 17 912.377 132.048 2 3 2 18 1227.49 143.841 2 3 2 19 962.595 143.024 2 3 2 20 253.722 146.657 2 3 2 21 397.102 153.741 2 3 2 22 133.506 152.397 2 3 2 23 229.535 159.227 2 3 2 24 383.185 142.580 2 3 2 25 181.783 127.512 2 3 2 26 116.238 123.415 2 -3 3 29-102.753 179.309 2 -3 -3 28 148.800 119.577 2 -3 3 27 686.033 125.260 2 -3 3 26 65.1835 134.398 2 -3 3 25 371.703 139.563 2 -3 3 24 187.611 155.325 2 -3 3 23 1213.76 150.077 2 -3 3 22 1608.79 152.651 2 -3 -3 21 93.8729 156.123 2 -3 3 20 1048.39 154.312 2 -3 3 19 147.009 145.314 2 -3 -3 18 5714.78 139.564 2 -3 -3 17 3453.24 124.428 2 -3 -3 16 3841.40 118.547 2 -3 -3 15 10122.8 123.871 2 -3 -3 14 14863.7 116.849 2 -3 3 13 976.197 103.552 2 -3 -3 12 1112.03 102.062 2 -3 -3 11 216.102 102.365 2 -3 3 10 590.788 125.412 2 -3 -3 9 23884.8 286.747 2 -3 3 8 17466.9 340.638 2 -3 3 7 365.828 390.979 2 -3 3 6 2108.77 367.241 2 -3 3 5 2655.42 309.249 2 -3 -3 4 25478.0 445.743 2 -3 -3 3 175.459 308.633 2 -3 -3 2 13847.8 344.206 2 -3 -3 1 8513.16 270.917 2 -3 -3 0 6309.92 244.704 2 -3 -3 -1 19305.9 237.398 2 -3 -3 -2 10520.8 247.188 2 -3 -3 -3 855.231 325.278 2 -3 -3 -4 386.526 347.672 2 -3 -3 -5 2739.94 370.666 2 -3 3 -6 4991.45 148.967 2 -3 3 -7 7253.26 119.118 2 -3 -3 -8 313.556 97.1550 2 -3 -3 -9 28.1446 85.5764 2 -3 -3 -10 6221.16 90.9319 2 3 3 11 493.900 93.9432 2 3 3 12 9457.38 103.155 2 3 3 13 226.472 110.209 2 3 3 14 2410.39 110.877 2 3 3 15 2885.09 141.811 2 3 3 16 373.810 125.842 2 3 -3 17 1033.35 134.061 2 3 3 18 6809.85 160.983 2 3 3 19 969.099 137.040 2 3 3 20 586.220 149.289 2 3 3 21 33.9432 144.373 2 3 3 22-58.5187 151.841 2 3 3 23 707.196 152.811 2 3 3 24 262.062 140.482 2 3 3 25 20.6088 124.661 2 3 3 26 324.227 119.406 2 -3 -4 28 654.001 119.036 2 -3 4 27 203.404 124.581 2 -3 4 26-21.6985 139.588 2 -3 4 25 1603.03 155.623 2 -3 4 24 633.133 146.707 2 -3 4 23 2989.10 150.562 2 -3 4 22 1003.42 149.746 2 -3 -4 21 581.988 153.283 2 -3 4 20 751.705 160.553 2 -3 4 19 107.104 144.700 2 -3 4 18 3374.49 147.758 2 -3 -4 17 2202.63 120.337 2 -3 -4 16 26840.7 134.731 2 -3 -4 15 3722.63 109.741 2 -3 -4 14 323.079 107.573 2 -3 4 13 841.661 102.155 2 -3 4 12 5110.57 105.271 2 -3 -4 11 1681.18 108.633 2 -3 4 10 701.015 125.166 2 -3 -4 9 710.255 183.733 2 -3 -4 8 184.480 386.703 2 -3 4 7 559.686 357.630 2 -3 -4 6 838.827 274.758 2 -3 4 5 7076.20 306.055 2 -3 4 4 1819.04 250.362 2 -3 4 3 11394.0 264.534 2 -3 -4 2 268.007 194.251 2 -3 -4 1 3453.87 334.353 2 -3 -4 0 23454.4 240.524 2 -3 -4 -1 6559.35 225.754 2 -3 -4 -2 10019.7 291.764 2 3 -4 3 2725.63 242.334 2 3 -4 4 8789.19 362.087 2 3 -4 5 5580.10 392.532 2 3 -4 6 6364.97 141.559 2 3 -4 7 4165.79 112.735 2 -3 -4 -8 1128.73 101.601 2 -3 -4 -9 8258.71 89.6886 2 -3 4 -10 7345.03 91.9705 2 -3 -4 -11 210.545 100.386 2 3 4 12 645.017 103.298 2 3 4 13 985.423 104.504 2 3 4 14 965.943 111.262 2 3 4 15-27.2106 131.316 2 3 4 16 498.113 132.110 2 3 4 17 1877.41 135.283 2 3 -4 18 4363.81 139.768 2 -3 4 -19 1282.25 143.210 2 3 4 20 37.2474 154.123 2 3 4 21 1038.41 139.288 2 3 4 22 56.3866 134.499 2 3 4 23 710.852 141.206 2 3 4 24 135.649 138.808 2 3 4 25 132.541 120.161 2 3 4 26 451.447 124.763 2 -3 5 28 781.680 106.918 2 -3 5 27 945.069 123.719 2 -3 5 26 512.204 138.473 2 -3 5 25 923.982 160.744 2 -3 5 24 1584.36 165.029 2 -3 5 23 990.632 157.247 2 -3 5 22 2636.93 153.166 2 -3 -5 21 6618.36 165.152 2 -3 5 20 2018.80 140.973 2 -3 5 19 558.283 145.219 2 -3 -5 18 176.560 135.915 2 -3 -5 17 1969.63 142.922 2 -3 5 16 3500.52 127.876 2 -3 -5 15 96.4093 127.865 2 -3 5 14 3016.24 114.627 2 -3 5 13 14976.8 124.252 2 -3 5 12 8864.93 111.310 2 -3 -5 11 30.4157 106.704 2 -3 5 10 6052.30 130.551 2 -3 -5 9 2919.89 186.431 2 -3 -5 8 1158.89 351.804 2 3 5 -7 5030.75 243.551 2 -3 5 6 89.7633 325.879 2 -3 5 5 4585.83 240.051 2 -3 -5 4 6328.98 326.362 2 -3 5 3 15137.7 365.317 2 -3 5 2 21058.8 280.808 2 -3 5 1 3880.02 281.497 2 -3 5 0 8613.00 301.688 2 3 -5 1 1770.91 165.560 2 -3 -5 -2 16643.4 225.298 2 -3 -5 -3 27706.3 331.627 2 -3 -5 -4 17039.4 317.077 2 3 -5 5 3242.90 361.747 2 3 -5 6 7309.95 157.834 2 3 5 7 3584.93 103.024 2 -3 -5 -8 461.284 94.3700 2 -3 -5 -9 5295.65 94.5231 2 -3 -5 -10 235.511 92.5541 2 3 5 11 3101.03 109.567 2 -3 -5 -12 2282.89 106.195 2 3 5 13 2262.01 105.151 2 3 5 14 1240.43 111.275 2 3 5 15 1250.18 121.240 2 3 5 16 3561.93 132.591 2 3 5 17 1821.06 136.950 2 3 5 18 186.551 141.268 2 3 5 19 184.244 146.365 2 3 5 20 32.2601 142.673 2 3 5 21 571.975 138.938 2 3 5 22-50.1713 135.406 2 3 5 23-88.7653 136.254 2 3 5 24 146.703 135.392 2 3 5 25 132.282 135.138 2 3 5 26 465.006 123.298 2 -3 6 28 23.5483 114.008 2 -3 6 27-177.154 121.229 2 -3 6 26 78.9970 136.144 2 -3 -6 25 767.291 153.581 2 -3 6 24 378.779 162.929 2 -3 6 23 314.149 169.098 2 -3 -6 22 1730.75 169.182 2 -3 6 21 221.509 151.417 2 -3 -6 20 1996.69 147.767 2 -3 -6 19-100.674 143.538 2 -3 -6 18 976.059 147.405 2 -3 -6 17-2.64747 141.963 2 -3 -6 16 215.867 129.414 2 -3 -6 15 7.00392 122.556 2 -3 6 14 4817.56 118.291 2 -3 6 13 13445.2 125.595 2 -3 6 12 3631.81 109.647 2 -3 -6 11 3082.93 109.133 2 -3 6 10 3362.45 137.045 2 -3 -6 9 5832.20 186.081 2 -3 -6 8 521.214 283.335 2 3 6 -7 10755.5 316.410 2 3 6 -6 15341.3 337.474 2 -3 6 5 10973.2 327.723 2 -3 6 4 3435.98 240.919 2 -3 6 3 77.0495 315.581 2 -3 6 2 2779.84 232.940 2 -3 6 1 7586.32 203.161 2 3 -6 0 6177.27 272.446 2 -3 -6 -1 7667.89 266.983 2 -3 -6 -2 8755.44 223.629 2 -3 -6 -3 11864.0 266.478 2 -3 -6 -4 13270.3 395.551 2 -3 6 -5 3630.16 157.252 2 -3 6 -6 182.528 132.966 2 -3 6 -7 9780.81 110.213 2 -3 -6 -8 1458.91 94.9912 2 -3 -6 -9 4159.26 96.3584 2 3 6 10 11253.9 109.199 2 3 6 11 291.051 97.3214 2 -3 -6 -12 1983.17 98.0934 2 3 6 13 354.960 107.648 2 3 6 14 724.189 111.571 2 3 6 15 12442.5 148.431 2 3 6 16 152.500 128.377 2 3 6 17 2806.90 135.517 2 3 6 18 842.125 143.354 2 3 6 19 5109.99 149.153 2 3 6 20 737.305 144.224 2 3 6 21 65.7806 135.200 2 3 6 22 534.376 129.543 2 3 6 23 298.877 133.050 2 3 6 24 995.629 138.416 2 3 6 25 60.3742 129.297 2 3 -6 26-77.9385 134.703 2 -3 7 28 874.617 111.899 2 -3 7 27 352.847 119.259 2 -3 7 26 355.395 140.432 2 -3 7 25 517.413 151.811 2 -3 7 24 2026.09 157.141 2 -3 7 23 334.062 169.203 2 -3 7 22 1560.15 166.027 2 -3 7 21 431.929 159.616 2 -3 -7 20-58.8243 156.065 2 -3 -7 19 5.65744 157.788 2 -3 -7 18 192.821 152.772 2 -3 -7 17 2170.13 149.658 2 -3 -7 16 1883.24 132.550 2 -3 -7 15 3112.53 131.342 2 -3 -7 14 444.170 130.792 2 -3 7 13 10710.8 133.513 2 -3 7 12 16645.9 121.332 2 -3 7 11 7880.94 115.173 2 -3 7 10 747.595 138.285 2 -3 -7 9 1288.76 149.759 2 3 7 -8 8644.05 310.224 2 3 7 -7 6652.69 540.984 2 3 7 -6 9749.31 405.405 2 3 7 -5 180.860 370.603 2 -3 -7 4 2846.52 448.349 2 -3 7 3 2640.12 288.223 2 -3 7 2 28194.0 324.955 2 -3 7 1 84.3427 441.615 2 3 -7 0 18320.6 265.785 2 -3 -7 -1 807.985 336.094 2 -3 7 -2 9983.64 390.693 2 -3 -7 -3 7359.08 280.964 2 -3 -7 -4 23047.6 259.679 2 -3 7 -5 31906.8 168.259 2 -3 -7 -6 8389.78 133.873 2 -3 -7 -7 2182.21 97.1338 2 -3 7 -8 5731.35 104.918 2 -3 -7 -9 7126.84 96.5655 2 -3 -7 -10 224.665 100.429 2 -3 -7 -11 2262.81 108.023 2 3 7 12 2561.08 102.064 2 3 7 13 289.091 107.144 2 3 7 14 11091.6 136.959 2 3 7 15-95.7408 122.599 2 3 7 16 1340.20 129.957 2 -3 -7 -17 4893.44 143.841 2 3 7 18 72.2247 144.748 2 3 7 19 22.9954 143.311 2 3 7 20 465.762 150.449 2 3 7 21 58.1181 137.510 2 3 7 22 379.605 129.170 2 3 7 23 138.608 129.440 2 3 7 24 88.9232 135.701 2 3 7 25 570.733 129.397 2 3 -7 26 1.15426 194.414 2 -3 8 28-17.5428 111.636 2 -3 8 27 189.498 120.676 2 -3 8 26 2114.84 138.923 2 -3 8 25 549.195 153.813 2 -3 -8 24 301.594 159.664 2 -3 8 23 2052.49 154.619 2 -3 8 22 1876.62 163.951 2 -3 8 21 712.038 164.824 2 -3 -8 20 440.313 155.006 2 -3 -8 19 3166.21 155.244 2 -3 -8 18 873.517 152.194 2 -3 -8 17 8108.98 154.918 2 -3 -8 16 3356.41 136.108 2 -3 -8 15 2485.06 130.005 2 -3 -8 14-214.297 124.266 2 -3 -8 13 514.134 109.797 2 -3 -8 12 11884.6 113.977 2 -3 -8 11 243.935 121.929 2 -3 -8 10-6.33810 128.607 2 -3 -8 9 3991.71 160.892 2 -3 -8 8 5105.39 230.699 2 -3 8 7 338.089 385.551 2 -3 -8 6 1244.44 335.202 2 -3 8 5 426.668 367.547 2 -3 8 4 3474.11 476.548 2 -3 8 3 22281.1 229.096 2 -3 8 2 1077.75 354.908 2 3 -8 -1 17989.0 408.961 2 -3 8 0 23472.3 526.897 2 -3 8 -1 16174.9 406.247 2 -3 -8 -2 3847.86 423.800 2 -3 -8 -3 270.521 287.310 2 -3 8 -4 5466.58 145.452 2 -3 8 -5 331.802 147.482 2 -3 8 -6 21681.7 147.561 2 -3 -8 -7 55.3238 100.770 2 -3 -8 -8 2628.03 102.884 2 -3 -8 -9 558.893 92.1143 2 -3 -8 -10 9262.74 106.719 2 3 8 11 2227.75 131.755 2 3 8 12 6725.66 115.969 2 3 8 13 101.404 114.549 2 3 8 14 7897.59 140.603 2 3 8 15 322.449 129.087 2 3 8 16 481.187 127.525 2 3 8 17 151.067 138.387 2 3 8 18 97.7114 141.086 2 3 8 19 685.213 145.540 2 3 8 20-56.9486 140.526 2 3 8 21 240.324 143.342 2 3 8 22 18.7906 134.278 2 3 8 23 147.299 126.174 2 3 8 24 967.212 135.196 2 3 8 25 858.230 133.676 2 -3 9 28 194.566 116.259 2 -3 9 27-71.0170 115.485 2 -3 -9 26 77.6338 137.734 2 -3 9 25 881.797 142.921 2 -3 9 24 218.029 151.088 2 -3 9 23 168.679 145.764 2 -3 9 22 130.355 155.918 2 -3 -9 21 1205.09 160.152 2 -3 -9 20-89.0042 158.638 2 -3 -9 19 866.796 164.689 2 -3 -9 18 6050.05 194.086 2 -3 -9 17 1355.35 150.851 2 -3 -9 16 34.3457 136.405 2 -3 -9 15 3.65015 122.877 2 -3 -9 14 1103.72 115.430 2 -3 -9 13 11135.3 126.865 2 -3 -9 12 7361.70 122.167 2 -3 -9 11 13.7418 114.062 2 3 -9 -10 1351.84 136.916 2 -3 -9 9 2840.02 149.994 2 -3 -9 8-0.92781 199.027 2 -3 -9 7 1204.25 343.260 2 -3 9 6 4184.01 521.474 2 -3 9 5 19467.0 434.699 2 3 -9 -4 78531.5 496.903 2 -3 9 3 255.164 393.383 2 -3 -9 2 430.439 324.722 2 -3 -9 1 686.752 429.163 2 -3 -9 0 798.568 488.879 2 -3 9 -1 14251.3 349.780 2 -3 9 -2 980.421 445.156 2 -3 -9 -3 9016.94 211.723 2 -3 -9 -4 2593.65 186.811 2 -3 9 -5 7261.07 165.001 2 -3 9 -6 3809.39 134.668 2 -3 -9 -7 4330.95 99.6545 2 -3 -9 -8 14.7044 101.810 2 3 9 9 634.100 109.254 2 3 9 10-72.1907 103.045 2 3 9 11-31.5988 106.722 2 3 9 12 2410.35 111.539 2 3 9 13 577.959 117.714 2 3 9 14 32.8889 129.622 2 3 9 15 8106.03 155.256 2 3 9 16 123.448 143.648 2 3 9 17 1161.79 143.524 2 3 9 18 94.0138 147.106 2 3 9 19 613.883 147.384 2 3 9 20 732.350 147.189 2 3 9 21 472.298 146.800 2 3 -9 22 251.419 140.575 2 3 9 23 2116.20 128.181 2 3 9 24 214.678 118.050 2 3 -9 25 123.655 134.341 2 -3 10 28 135.683 124.874 2 -3 10 27 66.2253 114.677 2 -3 10 26 282.603 133.468 2 -3 10 25-29.9100 141.133 2 -3 10 24 85.0201 142.228 2 -3 10 23 143.256 144.283 2 -3 10 22-190.620 155.210 2 -3 -10 21 618.374 153.183 2 -3 -10 20 53.0688 159.763 2 -3 -10 19 1764.62 157.615 2 -3 -10 18 1341.61 165.720 2 -3 10 17 1199.21 149.928 2 -3 -10 16 135.041 136.827 2 -3 -10 15 1262.19 130.493 2 -3 -10 14 941.190 116.466 2 -3 -10 13 1307.49 119.152 2 -3 -10 12 12473.0 146.609 2 -3 -10 11 4184.03 131.981 2 -3 -10 10 10277.2 172.048 2 -3 -10 9 2278.83 152.449 2 -3 10 8 1991.83 201.541 2 -3 -10 7 3589.23 255.353 2 3 -10 -6 5893.48 360.423 2 -3 -10 5 1052.24 548.758 2 -3 -10 4 2828.89 507.079 2 -3 10 3 3697.50 528.608 2 -3 10 2 7499.45 319.291 2 -3 -10 1 4612.77 448.472 2 -3 -10 0 12201.9 331.044 2 -3 -10 -1 5944.01 258.554 2 -3 -10 -2 3910.03 303.370 2 -3 10 -3 15715.9 185.867 2 -3 10 -4 1142.03 176.018 2 -3 10 -5 13566.9 156.883 2 -3 -10 -6 374.605 108.917 2 -3 -10 -7 1074.55 107.910 2 -3 -10 -8 903.589 112.229 2 -3 -10 -9-64.7568 114.978 2 3 10 10 9007.26 112.754 2 3 10 11 21.3797 108.808 2 3 10 12 2629.50 111.772 2 3 10 13 3023.64 118.900 2 3 10 14 5806.43 157.000 2 3 10 15 1994.34 135.739 2 3 10 16 1039.83 138.775 2 3 10 17 1726.52 142.544 2 3 10 18 77.1332 146.638 2 3 10 19 69.1806 147.832 2 3 10 20-48.4511 148.204 2 3 10 21 9.76882 143.547 2 3 10 22 186.819 134.366 2 3 10 23 418.785 123.781 2 3 10 24 573.850 120.349 2 3 -10 25 288.351 146.023 2 -3 11 27 217.150 121.182 2 -3 11 26 212.206 125.852 2 -3 11 25 87.4879 141.323 2 -3 11 24 6.49536 133.117 2 -3 11 23-58.4481 143.133 2 -3 11 22 374.419 153.526 2 -3 -11 21 1375.43 157.945 2 -3 -11 20 1288.65 153.199 2 3 11 -19 157.038 156.332 2 3 11 -18 300.379 161.635 2 3 11 -17 141.822 151.113 2 3 11 -16 275.999 137.205 2 3 11 -15 641.457 135.173 2 3 11 -14 8807.64 122.348 2 3 11 -13 3461.77 122.045 2 3 11 -12 310.596 143.905 2 -3 11 11 646.534 144.988 2 -3 -11 10 2017.27 153.621 2 -3 11 9-77.2318 163.613 2 -3 -11 8 1385.68 197.531 2 -3 -11 7 4268.97 227.384 2 3 -11 -6 29.7943 297.333 2 -3 -11 5 3170.12 322.996 2 -3 -11 4 14912.8 522.123 2 -3 11 3 1214.17 457.575 2 -3 11 2 7525.87 469.441 2 -3 -11 1 219.346 437.453 2 -3 -11 0 4966.78 318.295 2 -3 -11 -1 777.016 358.735 2 -3 -11 -2 3815.36 265.215 2 -3 11 -3 9395.43 181.272 2 -3 11 -4 5077.01 163.372 2 -3 -11 -5 209.239 127.627 2 -3 -11 -6 3288.84 118.045 2 3 -11 7 1955.54 117.493 2 3 -11 8 7967.71 126.110 2 3 11 9 3312.60 115.167 2 3 11 10 4338.39 113.139 2 3 11 11 5062.51 111.072 2 3 11 12 58.6416 111.340 2 3 11 13 1169.34 119.000 2 3 11 14 2150.93 124.124 2 3 11 15 3551.98 141.425 2 3 11 16 1513.88 144.095 2 3 11 17 576.375 143.649 2 3 11 18 1442.94 152.455 2 3 11 19-172.444 156.351 2 3 11 20 771.282 153.388 2 3 11 21-23.6008 141.419 2 3 11 22 112.126 134.215 2 3 11 23 41.9644 127.863 2 3 -11 24 129.320 125.008 2 3 -11 25 70.9692 141.770 2 -3 12 27 346.244 117.750 2 -3 12 26 821.606 125.408 2 -3 12 25 139.948 129.862 2 -3 12 24 455.523 133.640 2 -3 12 23 379.923 142.741 2 -3 -12 22 3060.01 163.080 2 -3 12 21 514.724 152.236 2 -3 -12 20 988.381 155.842 2 3 12 -19 123.003 155.149 2 -3 -12 18 4.73712 155.047 2 -3 -12 17 142.818 132.398 2 3 12 -16 219.303 130.987 2 -3 -12 15-63.5628 121.419 2 3 12 -14 10763.9 135.171 2 -3 -12 13 58.7048 130.864 2 -3 -12 12 1574.97 145.647 2 -3 12 11 3907.41 163.975 2 -3 12 10 196.775 155.672 2 -3 12 9 8500.97 180.199 2 -3 -12 8 1152.14 236.217 2 -3 -12 7 1899.44 280.721 2 -3 -12 6 3421.70 314.075 2 -3 -12 5 261.942 320.834 2 -3 -12 4 6436.53 533.991 2 -3 -12 3 925.961 517.158 2 -3 -12 2 10318.4 372.482 2 -3 -12 1 1199.77 260.412 2 -3 -12 0 1118.78 240.201 2 3 -12 1 1000.67 346.042 2 -3 12 -2 2532.03 194.554 2 -3 12 -3-53.5445 190.179 2 -3 12 -4 4583.37 183.481 2 -3 -12 -5 727.979 146.686 2 -3 -12 -6 73.5125 124.420 2 -3 -12 -7 3236.27 136.318 2 -3 -12 -8 2529.88 137.656 2 3 -12 9 382.352 130.185 2 3 12 10 2820.96 118.438 2 3 12 11 4742.88 111.551 2 3 12 12 57.3857 116.374 2 3 12 13 555.481 127.221 2 3 12 14-4.41306 124.098 2 3 12 15 2008.01 132.205 2 3 12 16 4275.89 146.777 2 3 12 17 124.427 144.340 2 3 12 18 3514.84 157.421 2 3 12 19 543.623 157.708 2 3 12 20 160.454 149.933 2 3 12 21 66.3877 141.237 2 3 12 22 958.056 129.736 2 3 -12 23 17.1204 129.230 2 3 -12 24 519.546 127.408 2 3 -12 25 245.186 224.035 2 -3 13 27 87.1780 121.471 2 -3 13 26 487.981 136.946 2 -3 13 25 220.113 125.947 2 -3 13 24 1173.29 131.665 2 -3 13 23 78.3789 145.737 2 -3 -13 22 3297.61 158.030 2 -3 -13 21-24.1658 150.427 2 -3 -13 20 52.0941 149.905 2 -3 -13 19 643.704 155.088 2 -3 -13 18-102.565 161.182 2 -3 -13 17 1443.28 126.735 2 3 13 -16 7761.47 146.682 2 -3 -13 15 982.652 130.327 2 -3 -13 14 1824.42 128.420 2 -3 -13 13 551.767 148.378 2 -3 -13 12 120.290 143.400 2 -3 13 11 5731.39 156.375 2 -3 -13 10 3547.81 159.171 2 -3 13 9 2733.86 198.481 2 -3 -13 8 669.810 243.104 2 -3 13 7 8224.84 303.046 2 -3 -13 6 2197.77 341.453 2 -3 -13 5 319.263 330.501 2 -3 -13 4 975.952 255.158 2 -3 -13 3 22798.5 388.395 2 -3 -13 2 12958.8 274.183 2 -3 -13 1 1536.44 263.524 2 -3 -13 0 855.738 260.103 2 -3 13 -1 6.00107 182.161 2 -3 -13 -2 1149.97 253.073 2 -3 -13 -3 3507.70 202.298 2 -3 -13 -4 23686.2 207.707 2 -3 -13 -5 92.2324 148.362 2 -3 -13 -6 2820.84 139.800 2 -3 -13 -7 1.13454 144.472 2 3 -13 8 96.8165 140.270 2 3 -13 9 43.5698 121.979 2 3 13 10 837.647 120.371 2 3 13 11 976.421 112.294 2 3 -13 12 553.158 121.879 2 3 13 13 7690.67 175.362 2 3 13 14 2605.48 138.452 2 3 13 15 276.784 143.556 2 3 13 16 836.576 140.368 2 3 13 17 1013.67 146.262 2 3 13 18-10.5686 151.459 2 3 13 19 1246.49 155.083 2 3 13 20 356.091 148.837 2 3 -13 21 280.326 148.544 2 3 -13 22 1170.42 144.818 2 3 -13 23 435.821 138.084 2 3 -13 24-6.19867 122.147 2 -3 14 27 215.429 139.155 2 -3 14 26 596.066 129.460 2 -3 14 25 586.557 129.467 2 -3 14 24 107.405 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825.807 151.279 2 3 14 14 407.133 146.585 2 3 14 15 13101.2 189.279 2 3 14 16 108.155 139.568 2 3 14 17 33.9892 146.967 2 3 14 18 795.770 150.173 2 3 14 19 117.525 143.904 2 3 -14 20 0.96702 151.723 2 3 -14 21 401.812 161.401 2 3 -14 22 165.102 149.863 2 3 -14 23 245.761 132.262 2 3 -14 24 52.5795 121.805 2 -3 15 26 1180.26 125.674 2 -3 15 25 640.542 122.930 2 -3 15 24 1194.36 132.595 2 -3 15 23 771.299 142.049 2 -3 -15 22 112.207 148.832 2 -3 -15 21 1145.77 154.595 2 -3 -15 20 699.600 159.387 2 -3 -15 19 196.605 164.714 2 -3 -15 18 877.432 136.498 2 3 15 -17 6277.92 143.018 2 -3 -15 16 2496.52 137.279 2 3 15 -15 451.750 139.317 2 3 15 -14 5194.93 153.985 2 -3 -15 13 729.146 161.061 2 -3 15 12 384.980 176.716 2 -3 15 11 220.868 170.123 2 -3 15 10 10317.2 195.380 2 3 -15 -9 1779.33 269.075 2 -3 -15 8 942.156 309.374 2 -3 -15 7 97.5110 300.812 2 3 -15 -6 651.255 371.450 2 -3 15 5 4216.78 277.660 2 -3 -15 4 10044.0 256.463 2 -3 -15 3 11233.8 274.373 2 -3 -15 2 7565.68 281.056 2 -3 -15 1 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3776.95 326.450 2 -3 -18 3 2424.42 338.285 2 -3 -18 2 2076.90 433.668 2 -3 -18 1 1535.22 403.098 2 -3 -18 0 5039.99 357.774 2 -3 -18 -1 2057.92 367.558 2 -3 -18 -2 1462.33 302.413 2 -3 -18 -3 6345.19 329.078 2 -3 -18 -4 142.710 284.919 2 -3 -18 -5 820.722 214.948 2 -3 18 -6 250.517 218.431 2 -3 18 -7 9566.06 206.477 2 -3 18 -8 10.7089 189.613 2 -3 18 -9 523.481 176.927 2 -3 18 -10 4146.86 185.000 2 3 -18 11 3963.35 174.788 2 3 -18 12 1311.32 171.106 2 3 18 13 91.1452 152.480 2 3 18 14 2673.28 162.630 2 3 18 15 867.704 153.259 2 3 18 16 466.525 151.553 2 3 18 17 216.626 146.932 2 3 18 18 223.837 154.494 2 3 18 19-153.766 153.042 2 3 18 20-80.2011 159.828 2 3 18 21 210.669 146.922 2 3 18 22 797.275 131.981 2 -3 19 25 307.098 140.768 2 -3 19 24 263.206 130.307 2 -3 19 23-76.1421 154.391 2 -3 -19 22-64.5859 154.607 2 -3 -19 21 558.305 159.088 2 -3 -19 20 2281.97 141.850 2 -3 -19 19 79.5014 128.226 2 -3 -19 18 583.935 136.636 2 -3 -19 17 1211.41 145.237 2 -3 -19 16-12.0829 159.700 2 -3 -19 15 504.023 181.576 2 -3 -19 14 72.8735 211.075 2 -3 19 13 349.678 207.024 2 -3 19 12 515.542 249.541 2 -3 -19 11 298.288 309.316 2 -3 -19 10 850.353 319.645 2 3 -19 -9 10784.8 326.336 2 3 -19 -8 1111.10 312.128 2 3 -19 -7 4815.59 450.910 2 3 -19 -6 1329.21 309.315 2 -3 -19 5 356.355 416.972 2 -3 -19 4 513.113 445.255 2 -3 -19 3 254.604 333.806 2 -3 -19 2 649.453 346.825 2 -3 -19 1 1140.00 453.039 2 -3 -19 0 2229.98 262.306 2 -3 -19 -1 2688.90 276.404 2 -3 -19 -2 2021.85 253.953 2 -3 -19 -3 535.490 294.338 2 -3 -19 -4 2331.10 316.014 2 -3 -19 -5 4687.15 213.061 2 -3 -19 -6 3280.99 258.522 2 -3 19 -7-157.780 224.458 2 -3 19 -8-23.9671 196.584 2 -3 19 -9 4874.82 200.040 2 -3 19 -10 2334.36 177.366 2 3 -19 11 1431.96 184.699 2 3 -19 12 403.656 186.045 2 -3 19 -13 137.686 155.935 2 3 19 14 282.420 161.816 2 3 19 15-12.1387 151.379 2 3 19 16 234.972 155.525 2 3 19 17 33.5812 160.559 2 3 19 18 1449.33 160.394 2 3 19 19-70.9860 160.606 2 3 19 20-11.3894 154.624 2 3 19 21 103.232 140.421 2 3 19 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258.400 2 3 -20 12 1743.04 204.572 2 3 20 13 804.134 174.053 2 3 20 14 308.607 163.845 2 3 20 15 2081.58 156.721 2 3 20 16 127.867 153.203 2 3 20 17 644.740 155.524 2 3 20 18 203.888 152.458 2 3 20 19 351.854 151.182 2 3 20 20 670.130 145.837 2 3 20 21 178.664 131.287 2 3 20 22 23.3286 155.598 2 -3 21 24 122.293 118.963 2 -3 21 23 90.5166 130.460 2 -3 -21 22 488.057 150.593 2 -3 -21 21 6.12085 148.181 2 -3 -21 20 46.3653 149.881 2 -3 -21 19 201.745 141.370 2 -3 -21 18 1166.78 151.653 2 -3 -21 17 3094.22 167.477 2 -3 -21 16 833.457 167.313 2 -3 -21 15 1617.67 184.682 2 -3 21 14 13510.1 253.572 2 -3 21 13 162.112 260.450 2 -3 21 12 1317.16 268.674 2 -3 -21 11 394.824 283.132 2 -3 -21 10 6579.89 455.425 2 -3 -21 9 457.367 444.969 2 3 -21 -8 527.884 374.199 2 3 -21 -7 2669.97 1295.42 2 3 -21 -6 4479.11 284.645 2 3 -21 -5 1793.86 346.354 2 3 -21 -4-60.7085 482.880 2 3 -21 -3 145.663 288.776 2 -3 -21 2 263.200 356.310 2 -3 -21 1 2071.97 370.335 2 -3 -21 0 717.443 523.075 2 -3 -21 -1 390.623 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1053.45 497.958 2 3 -22 -6 6745.10 298.965 2 3 -22 -5 83.8055 498.427 2 3 -22 -4 1697.77 497.475 2 3 -22 -3 846.279 369.768 2 3 -22 -2 1617.50 322.071 2 3 -22 -1 1982.12 550.249 2 3 -22 0 1706.59 544.638 2 3 -22 1 5610.30 467.527 2 3 -22 2 725.621 360.255 2 3 -22 3 441.799 302.393 2 3 -22 4 1124.80 279.694 2 3 -22 5 3539.70 271.378 2 3 -22 6 547.339 271.309 2 3 -22 7 647.028 240.220 2 3 -22 8 270.764 214.750 2 3 -22 9 4453.46 219.223 2 3 -22 10 545.735 226.345 2 3 22 11 231.600 237.999 2 3 22 12 698.141 216.384 2 3 22 13 1926.49 207.445 2 3 22 14 640.636 183.690 2 3 22 15 112.160 159.182 2 3 22 16 588.379 167.522 2 3 22 17 591.836 153.298 2 3 22 18 586.270 152.371 2 3 22 19 364.677 147.013 2 3 22 20 24.6833 139.564 2 3 -22 21 677.008 289.132 2 -3 23 23 89.6091 166.383 2 -3 -23 22 451.321 139.260 2 -3 -23 21 921.870 146.678 2 -3 -23 20 250.420 143.097 2 -3 -23 19 234.180 131.089 2 -3 -23 18 1151.30 159.847 2 -3 -23 17 5595.49 165.583 2 -3 23 16 2862.08 172.200 2 3 23 -15 456.555 187.986 2 -3 23 14-16.7236 239.784 2 -3 23 13 2435.19 296.437 2 -3 23 12 1787.98 296.515 2 -3 -23 11-67.0899 323.790 2 -3 -23 10-75.9766 370.472 2 -3 -23 9 1497.82 453.434 2 -3 -23 8 779.300 546.840 2 3 -23 -7 513.524 382.422 2 3 -23 -6 1100.43 505.260 2 3 -23 -5 8952.34 509.582 2 3 -23 -4 1009.25 507.468 2 3 -23 -3-18.3619 365.551 2 3 -23 -2 669.869 388.757 2 3 -23 -1 1381.12 552.350 2 3 -23 0 2076.39 574.247 2 3 -23 1 903.006 358.589 2 3 -23 2 3826.31 490.441 2 3 -23 3 404.962 392.398 2 3 -23 4 836.011 334.771 2 3 -23 5 2664.73 390.649 2 3 -23 6 555.655 270.649 2 3 -23 7 1517.64 238.301 2 3 -23 8 367.688 223.700 2 3 -23 9 48.0895 208.052 2 -3 -23 -10 295.051 217.026 2 -3 -23 -11 103.951 247.977 2 3 23 12 1526.71 218.932 2 -3 23 -13 4675.30 213.963 2 3 23 14 770.889 193.276 2 3 23 15 574.468 154.537 2 3 23 16 873.261 148.335 2 3 23 17-9.59068 148.156 2 3 23 18 86.7278 144.561 2 3 23 19 881.281 142.210 2 3 23 20 31.3267 129.341 2 -3 24 22 576.960 132.904 2 -3 -24 21 625.439 144.041 2 -3 -24 20 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13196.4 148.656 2 -4 -1 -2 14243.5 142.896 2 -4 -1 -3 293.973 112.825 2 -4 -1 -4 32115.1 127.514 2 -4 -1 -5 1037.82 107.753 2 -4 -1 -6 227.964 87.0035 2 -4 -1 -7 674.027 89.6451 2 -4 -1 -8 2897.83 99.5105 2 -4 1 -9 8454.79 128.216 2 -4 -1 -10 3186.80 108.948 2 -4 -1 -11 6257.15 107.260 2 4 -1 12 6235.16 124.562 2 -4 -1 -13 1505.82 126.043 2 4 1 14 1704.37 134.650 2 4 1 15 1621.33 132.019 2 4 1 16 224.962 153.419 2 4 1 17-25.8640 145.413 2 4 1 18 577.868 147.413 2 4 1 19 3950.47 161.661 2 4 1 20 356.497 150.775 2 4 1 21 141.151 147.824 2 4 1 22 279.140 143.820 2 4 1 23 984.910 135.441 2 4 1 24 188.948 117.199 2 -4 1 -25 340.653 390.451 2 -4 2 28 250.955 122.206 2 -4 2 27 544.221 129.348 2 -4 2 26 750.712 151.101 2 -4 2 25 32.4682 132.468 2 -4 2 24 643.712 162.565 2 -4 -2 23 94.4617 160.932 2 -4 2 22 42.9221 153.192 2 -4 2 21-106.525 162.318 2 -4 2 20 2242.20 156.787 2 -4 -2 19 759.121 165.515 2 -4 2 18 10415.2 165.195 2 -4 2 17 143.445 141.484 2 -4 -2 16 11001.3 139.104 2 -4 -2 15 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155.082 95.5558 2 -4 -3 -9 12055.3 106.398 2 -4 -3 -10 1727.64 100.267 2 -4 3 -11 1616.34 108.913 2 -4 -3 -12 306.463 104.943 2 4 3 13 5336.85 119.562 2 4 3 14 215.235 130.192 2 4 -3 15 47.5795 140.947 2 4 3 16 117.024 138.951 2 4 3 17 658.270 146.623 2 4 3 18 652.938 162.602 2 4 3 19 3142.21 149.551 2 4 3 20 155.873 142.480 2 4 3 21 78.0439 141.305 2 4 3 22 466.719 136.230 2 4 3 23 8.78539 130.115 2 4 3 24 38.8006 121.823 2 -4 -4 28 461.806 111.188 2 -4 4 27 183.366 128.444 2 -4 4 26 1495.08 125.896 2 -4 4 25 2248.20 152.523 2 -4 4 24 2196.86 156.118 2 -4 4 23 1872.38 157.327 2 -4 4 22 1020.29 154.665 2 -4 -4 21 8400.89 183.260 2 -4 4 20 3554.16 168.295 2 -4 -4 19 624.947 168.744 2 -4 -4 18 4021.38 157.871 2 -4 -4 17 420.699 142.714 2 -4 -4 16 5593.80 140.357 2 -4 -4 15 5966.45 132.931 2 -4 -4 14 9570.97 129.067 2 -4 -4 13 2639.82 116.415 2 -4 -4 12 157.983 106.740 2 -4 4 11 1864.54 96.9401 2 -4 4 10 5588.36 106.258 2 -4 4 9 19419.1 120.053 2 -4 4 8 6397.56 125.948 2 -4 -4 7 517.154 165.550 2 -4 4 6 617.028 225.293 2 -4 -4 5 1360.79 245.877 2 -4 -4 4 8965.87 375.219 2 4 -4 -3 234.992 210.957 2 -4 -4 2 322.316 159.413 2 -4 -4 1-114.600 142.174 2 -4 4 0 15612.6 152.799 2 -4 4 -1 20521.5 144.706 2 -4 -4 -2 767.017 122.116 2 -4 -4 -3 27.9124 128.495 2 -4 -4 -4 857.130 102.902 2 -4 -4 -5 3790.95 107.381 2 -4 -4 -6 10816.0 99.1169 2 -4 -4 -7 10164.2 100.825 2 -4 -4 -8 20.3266 92.9010 2 -4 -4 -9 2070.87 108.652 2 -4 -4 -10 8420.30 108.096 2 4 4 11 8959.78 111.808 2 4 4 12 978.057 113.312 2 -4 -4 -13 1204.41 124.786 2 4 4 14 1020.39 126.989 2 4 4 15 4476.08 137.015 2 4 4 16 2542.83 140.565 2 4 -4 17 96.4897 160.684 2 4 4 18 763.464 149.509 2 4 4 19 254.083 146.175 2 4 4 20 161.904 147.618 2 4 4 21 196.833 140.283 2 4 4 22 314.584 133.146 2 4 4 23 329.545 135.716 2 4 4 24 132.780 122.106 2 -4 -5 28-24.2598 121.200 2 -4 5 27 69.7908 117.468 2 -4 5 26 42.5205 125.485 2 -4 -5 25 102.429 141.659 2 -4 5 24 928.517 154.633 2 -4 5 23-9.53045 155.384 2 -4 -5 22 584.783 164.896 2 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17-85.9111 142.640 2 4 5 18 3001.42 151.690 2 4 5 19 506.941 142.727 2 4 5 20 27.6234 145.477 2 4 -5 21 2158.22 147.882 2 4 5 22 465.557 136.097 2 4 5 23 1494.58 133.638 2 4 5 24 244.197 124.140 2 -4 6 28 533.575 128.490 2 -4 6 27 8.67015 108.267 2 -4 6 26 198.042 126.071 2 -4 6 25 132.979 141.172 2 -4 6 24 2009.60 155.124 2 -4 6 23 222.706 159.463 2 -4 -6 22-241.161 161.999 2 -4 6 21 227.337 174.705 2 -4 6 20 735.461 159.557 2 -4 -6 19 4549.69 161.155 2 -4 -6 18 7968.79 165.515 2 -4 -6 17 596.745 151.597 2 -4 -6 16 891.854 150.385 2 -4 -6 15 889.340 136.589 2 -4 -6 14 746.797 132.691 2 -4 -6 13 1427.91 120.096 2 -4 -6 12 4753.12 129.103 2 -4 -6 11 136.502 110.695 2 -4 6 10 112.099 104.506 2 4 6 -9 1502.63 108.406 2 4 6 -8 132.485 105.321 2 -4 6 7 5577.40 128.940 2 -4 -6 6 1827.00 150.392 2 -4 6 5 647.501 184.502 2 -4 -6 4 637.437 163.882 2 4 -6 -3 1249.47 174.748 2 -4 -6 2 21948.4 167.046 2 -4 -6 1 279.909 137.690 2 -4 6 0 7541.55 157.757 2 -4 6 -1 5514.08 133.199 2 -4 6 -2 17366.9 142.977 2 -4 -6 -3 384.812 120.445 2 -4 -6 -4 903.609 100.323 2 -4 -6 -5 1340.55 107.282 2 -4 -6 -6 20388.3 109.487 2 -4 -6 -7 135.163 99.0544 2 4 6 8 114.637 97.0864 2 -4 -6 -9 9.43224 101.213 2 -4 -6 -10 44.4309 98.9837 2 -4 -6 -11 293.901 101.367 2 -4 -6 -12 165.811 111.222 2 4 6 13 5053.23 114.032 2 4 6 14 507.986 121.413 2 4 6 15 630.041 131.810 2 4 6 16 680.700 131.850 2 4 6 17 1485.84 137.458 2 4 6 18 2001.12 135.962 2 4 6 19-96.4036 156.209 2 4 6 20 13.0076 150.478 2 4 6 21 457.173 143.338 2 4 6 22 36.3857 132.358 2 4 6 23 479.902 132.048 2 4 6 24 99.7423 132.866 2 -4 7 27 74.5876 110.069 2 -4 7 26 1512.06 127.651 2 -4 7 25-87.2814 139.266 2 -4 7 24-108.515 147.837 2 -4 7 23 221.790 161.776 2 -4 7 22 3611.38 175.566 2 -4 7 21 2095.15 165.005 2 -4 -7 20 512.934 156.619 2 -4 -7 19 552.085 156.746 2 -4 -7 18 1780.71 156.732 2 -4 -7 17 786.101 148.192 2 -4 -7 16 3736.74 140.634 2 -4 -7 15 981.681 131.237 2 -4 -7 14 477.671 134.229 2 -4 7 13 6085.03 134.595 2 -4 7 12 3809.44 144.795 2 -4 7 11 4815.13 119.469 2 4 7 -10 5051.03 110.183 2 -4 -7 9 163.001 108.994 2 -4 -7 8 981.003 112.927 2 -4 -7 7 186.616 120.894 2 -4 -7 6 8028.19 156.953 2 -4 -7 5 380.874 188.981 2 -4 -7 4 713.949 165.428 2 4 -7 -3 2267.58 167.504 2 -4 7 2 11211.1 149.933 2 -4 7 1 4318.82 152.924 2 -4 -7 0 3607.08 143.984 2 -4 -7 -1 1385.51 135.960 2 -4 7 -2 20440.5 142.689 2 -4 -7 -3 1620.71 112.866 2 -4 7 -4 4840.11 116.607 2 -4 -7 -5 2797.04 109.474 2 -4 -7 -6 232.600 94.5901 2 -4 -7 -7 2868.70 103.132 2 -4 -7 -8 7922.05 111.022 2 4 7 9 5758.58 108.476 2 -4 -7 -10 633.564 105.436 2 -4 -7 -11 394.984 110.752 2 4 7 12 5090.67 119.859 2 4 7 13 5978.92 129.163 2 4 7 14 1506.58 124.691 2 4 7 15 758.568 134.471 2 4 7 16 3081.94 137.023 2 4 7 17 345.075 137.723 2 4 7 18 949.482 145.677 2 4 7 19 492.585 142.158 2 4 7 20-53.0083 149.267 2 4 7 21 690.841 141.597 2 4 7 22-43.7685 131.116 2 4 7 23 131.459 131.437 2 4 7 24 90.9881 126.466 2 -4 8 27-72.5495 105.730 2 -4 8 26 516.934 124.680 2 -4 8 25 180.661 137.945 2 -4 8 24-22.3311 143.834 2 -4 8 23 26.9906 150.387 2 -4 8 22 4.61856 175.242 2 -4 -8 21 2923.79 166.445 2 -4 -8 20 609.297 163.624 2 -4 -8 19 2164.66 159.527 2 -4 -8 18 9485.15 169.082 2 -4 -8 17 74.6553 144.006 2 -4 -8 16 2707.98 142.595 2 -4 -8 15 1516.10 133.670 2 -4 8 14 24697.7 142.651 2 -4 -8 13 206.552 124.443 2 4 8 -12 705.457 123.060 2 -4 -8 11-31.6657 112.053 2 -4 8 10 21795.4 134.303 2 -4 -8 9 4047.61 126.889 2 -4 -8 8 14876.1 122.475 2 -4 8 7 6381.28 146.101 2 -4 -8 6 3366.31 156.081 2 -4 8 5 679.950 157.836 2 -4 8 4 48.7286 162.912 2 -4 -8 3 8553.74 164.014 2 -4 8 2 4633.72 152.754 2 -4 8 1 832.353 149.079 2 -4 -8 0 22997.1 159.010 2 -4 8 -1 23113.8 147.967 2 -4 -8 -2 396.651 117.856 2 -4 -8 -3 270.263 113.429 2 -4 -8 -4 232.242 115.605 2 -4 8 -5 127.071 109.093 2 -4 -8 -6 10649.4 113.516 2 -4 -8 -7 5287.85 102.359 2 -4 -8 -8 1275.53 103.257 2 -4 -8 -9 782.003 105.430 2 -4 -8 -10 4848.58 111.252 2 -4 -8 -11 8004.96 134.081 2 4 8 12 645.288 119.546 2 4 8 13 530.205 120.126 2 4 8 14 1777.67 133.582 2 4 8 15 6448.96 138.449 2 4 8 16 7867.10 147.036 2 4 8 17 2185.80 139.119 2 4 8 18-2.66236 150.948 2 4 8 19 23.4386 140.760 2 4 8 20 843.513 133.073 2 4 8 21 143.268 138.262 2 4 8 22 717.527 136.247 2 4 8 23 206.363 124.321 2 4 -8 24-17.4658 141.003 2 -4 9 27 48.7748 117.594 2 -4 9 26 102.046 123.513 2 -4 9 25 64.7922 131.500 2 -4 9 24 28.3315 142.579 2 -4 9 23 213.446 160.806 2 -4 9 22 410.373 160.446 2 -4 9 21 1409.33 163.675 2 -4 -9 20 51.6261 152.705 2 4 9 -19 251.737 161.061 2 4 9 -18 7838.40 177.798 2 4 9 -17 3705.11 148.369 2 4 9 -16 1146.63 142.794 2 4 9 -15 2306.05 131.413 2 4 9 -14 309.403 131.697 2 4 9 -13 14.3604 120.318 2 -4 -9 12 14855.1 132.553 2 -4 -9 11 1134.02 123.347 2 4 9 -10-78.0657 124.443 2 -4 -9 9 51.7979 120.587 2 -4 -9 8 5646.33 146.029 2 -4 -9 7 1481.21 141.053 2 -4 9 6 263.547 163.354 2 -4 -9 5 2139.19 134.922 2 -4 9 4-45.7086 170.742 2 -4 9 3 1747.01 155.776 2 -4 9 2 7455.00 155.794 2 -4 9 1 1491.46 165.336 2 -4 -9 0 227.213 136.523 2 -4 9 -1 113.461 126.572 2 -4 -9 -2 3164.71 133.157 2 -4 -9 -3-44.5572 115.338 2 -4 -9 -4 3938.65 118.621 2 -4 -9 -5 252.486 112.511 2 4 9 6 6287.82 111.626 2 -4 -9 -7 137.130 99.5332 2 -4 -9 -8 3002.14 100.337 2 -4 9 -9 220.808 108.107 2 4 9 10 4882.77 135.633 2 -4 -9 -11 1007.74 138.963 2 4 9 12 2074.89 123.920 2 4 9 13 282.191 132.494 2 4 9 14 2673.20 137.839 2 4 9 15 803.858 135.904 2 4 9 16 2274.45 133.497 2 4 9 17 1686.64 131.073 2 4 9 18 7837.69 166.355 2 4 9 19 251.156 140.409 2 4 9 20 310.547 132.790 2 4 9 21 90.4131 136.087 2 4 9 22 66.3105 138.404 2 4 9 23 539.292 124.508 2 4 -9 24 419.124 178.246 2 -4 10 27 101.804 113.540 2 -4 10 26 50.3573 126.068 2 -4 10 25 1119.15 130.677 2 -4 10 24 53.2438 137.035 2 -4 -10 23 2818.86 142.795 2 -4 10 22 128.934 154.958 2 -4 10 21 802.917 148.564 2 -4 -10 20 818.228 152.258 2 -4 -10 19 97.2172 160.043 2 4 10 -18 3340.20 154.592 2 -4 -10 17 1823.43 151.190 2 4 10 -16 8364.20 159.647 2 4 10 -15-189.770 144.233 2 -4 -10 14 415.943 130.013 2 -4 -10 13 2513.22 137.023 2 -4 -10 12 294.815 127.850 2 4 10 -11 260.631 134.152 2 4 10 -10-37.2090 118.723 2 -4 10 9 15579.3 141.297 2 -4 -10 8 957.038 130.307 2 -4 -10 7 5231.88 146.420 2 -4 10 6 1811.30 187.111 2 -4 10 5 196.146 142.390 2 -4 10 4 2766.90 179.471 2 -4 10 3 10314.9 166.984 2 -4 10 2 3594.40 164.474 2 -4 10 1 31907.2 172.719 2 -4 10 0 1249.95 145.505 2 -4 -10 -1 2134.17 144.961 2 -4 10 -2 6064.45 142.371 2 -4 -10 -3 1823.58 133.011 2 -4 -10 -4 1165.63 112.751 2 -4 -10 -5 4201.65 115.612 2 4 10 6 3374.03 102.820 2 4 10 7 2851.41 97.3999 2 -4 -10 -8 124.483 104.938 2 -4 -10 -9 511.834 113.279 2 -4 -10 -10 1612.61 121.940 2 4 10 11 5806.86 141.932 2 4 10 12 92.5133 134.936 2 4 10 13 1005.40 128.690 2 4 10 14 2608.95 152.026 2 4 10 15 2459.51 142.890 2 4 10 16 1861.66 140.193 2 4 10 17 1826.15 131.004 2 4 10 18 181.567 138.333 2 4 10 19 356.705 144.747 2 4 10 20 1124.89 138.235 2 4 10 21-27.5231 132.738 2 4 10 22 659.227 134.735 2 4 10 23 165.923 118.432 2 -4 11 27 205.634 127.348 2 -4 11 26 49.6171 127.502 2 -4 11 25 142.577 132.419 2 -4 11 24 451.609 145.747 2 -4 11 23 320.446 143.931 2 -4 11 22 121.461 145.073 2 -4 11 21 2243.01 147.124 2 -4 -11 20 579.915 148.823 2 -4 -11 19 85.3555 154.389 2 -4 -11 18 680.727 147.391 2 -4 -11 17 303.001 146.303 2 -4 -11 16 639.991 165.516 2 -4 -11 15 1803.25 154.896 2 -4 -11 14-209.013 143.079 2 -4 -11 13 2881.94 139.813 2 4 11 -12 51.2453 138.042 2 -4 11 11 19064.4 154.253 2 -4 11 10-17.3172 122.853 2 4 11 -9 51.1998 133.621 2 -4 -11 8 2254.18 152.941 2 -4 -11 7 3375.76 157.163 2 -4 -11 6 3247.19 213.116 2 -4 11 5 1244.05 160.750 2 4 11 -4 28.8123 163.857 2 -4 11 3 5211.77 186.141 2 -4 11 2 463.562 165.594 2 -4 11 1 667.171 141.328 2 -4 11 0 25396.6 171.642 2 -4 -11 -1 4108.45 152.382 2 4 -11 2 2024.72 151.322 2 -4 -11 -3 518.945 136.937 2 -4 -11 -4 1182.22 127.097 2 -4 11 -5 4945.11 132.021 2 4 11 6 9940.44 117.036 2 -4 -11 -7 1501.65 98.2644 2 -4 -11 -8 3923.98 105.368 2 -4 -11 -9 397.952 109.257 2 4 11 10 1125.08 126.557 2 4 11 11 1609.50 133.857 2 4 11 12 85.8505 131.186 2 4 11 13 54.3653 128.341 2 4 11 14 2722.19 148.935 2 4 11 15 195.090 138.330 2 4 11 16 10435.6 178.570 2 4 11 17 794.719 143.718 2 4 11 18 44.2461 150.149 2 4 11 19 613.769 149.038 2 4 11 20 158.727 139.651 2 4 11 21 148.681 128.836 2 4 11 22 443.922 133.383 2 4 -11 23 117.960 129.670 2 -4 12 26-10.4468 122.897 2 -4 12 25 277.425 136.226 2 -4 12 24 52.3872 139.609 2 -4 12 23 650.955 154.442 2 -4 12 22 22.1441 153.419 2 -4 -12 21 170.737 150.053 2 -4 -12 20 17.7538 158.632 2 -4 -12 19 415.553 161.981 2 -4 -12 18 1212.97 152.809 2 -4 -12 17 831.341 162.754 2 -4 -12 16 1420.62 153.162 2 4 12 -15 6143.51 145.253 2 -4 -12 14 1240.95 138.288 2 4 12 -13 14517.3 145.049 2 -4 -12 12 977.931 131.754 2 4 12 -11 4277.54 127.554 2 4 12 -10 1004.88 128.307 2 -4 12 9 418.504 135.918 2 -4 -12 8 235.873 148.852 2 -4 -12 7 1130.70 164.737 2 -4 -12 6 105.773 196.226 2 -4 12 5 2084.10 170.411 2 -4 12 4 3121.59 169.314 2 -4 12 3 2022.57 184.251 2 -4 12 2-27.3468 159.793 2 -4 12 1 2013.81 154.220 2 -4 -12 0 141.688 148.370 2 -4 -12 -1 867.698 151.284 2 -4 -12 -2 1947.08 152.239 2 -4 -12 -3 1070.33 136.771 2 -4 -12 -4 1286.71 128.904 2 -4 -12 -5 22591.0 147.958 2 -4 -12 -6 4330.42 109.136 2 -4 -12 -7 2971.74 102.975 2 -4 -12 -8 315.866 104.732 2 4 12 9 2282.15 115.983 2 4 12 10 765.417 124.956 2 4 12 11 266.560 134.535 2 4 12 12-54.5334 134.028 2 4 12 13 266.741 142.499 2 4 12 14 86.4832 139.429 2 4 12 15 2235.64 145.569 2 4 12 16 796.946 138.287 2 4 12 17 846.156 142.566 2 4 12 18 1323.88 149.985 2 4 12 19 549.222 148.076 2 4 12 20 135.854 139.462 2 4 12 21 676.320 127.953 2 4 -12 22 49.0047 126.026 2 4 -12 23 131.745 132.006 2 -4 13 26-60.4669 126.131 2 -4 13 25-26.5137 130.125 2 -4 13 24 92.1032 141.260 2 -4 13 23 87.7445 151.720 2 -4 13 22 203.217 143.651 2 -4 -13 21 3729.05 153.790 2 -4 -13 20-43.4321 157.166 2 -4 -13 19-14.1279 175.388 2 -4 -13 18 165.695 166.719 2 -4 -13 17 1110.46 157.085 2 -4 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128.772 2 4 -13 22 156.405 119.447 2 -4 13 -23 83.0268 191.843 2 -4 14 26 53.3964 128.376 2 -4 14 25 5.45802 124.014 2 -4 14 24 723.729 133.432 2 -4 14 23 102.797 144.481 2 -4 14 22 225.302 154.163 2 -4 -14 21 19.4345 162.217 2 -4 -14 20 3784.80 169.904 2 -4 -14 19 2001.31 173.539 2 -4 -14 18 1076.06 170.441 2 -4 -14 17 123.727 161.198 2 -4 -14 16 140.211 155.066 2 4 14 -15 56.7703 149.220 2 -4 -14 14 3081.62 145.225 2 -4 -14 13-60.1553 143.530 2 -4 -14 12 256.730 137.334 2 4 14 -11 3477.07 138.326 2 4 14 -10 6494.92 156.170 2 -4 -14 9 5692.82 177.017 2 -4 -14 8 1625.68 156.247 2 -4 -14 7 188.847 207.273 2 4 14 -6 21004.7 288.767 2 -4 -14 5 3357.28 180.237 2 4 14 -4 20474.4 194.216 2 -4 14 3-192.919 190.083 2 -4 14 2 3276.89 217.493 2 -4 -14 1 4651.53 168.304 2 -4 14 0 3693.17 165.102 2 -4 -14 -1 441.347 156.795 2 -4 14 -2 714.943 172.033 2 -4 -14 -3 224.453 165.575 2 -4 -14 -4 1282.54 164.146 2 -4 -14 -5 3352.79 143.896 2 -4 -14 -6 5895.03 131.595 2 -4 -14 -7 3388.63 114.616 2 4 14 8 983.677 114.600 2 4 14 9 1233.21 127.618 2 4 14 10 155.652 137.072 2 4 14 11 9733.18 145.147 2 4 14 12 35.7261 137.197 2 4 14 13 2242.09 131.583 2 4 14 14 706.856 139.857 2 4 14 15 537.121 157.862 2 4 14 16 334.720 146.771 2 4 14 17 295.159 143.895 2 4 14 18 887.827 145.787 2 4 14 19 72.1964 139.365 2 4 -14 20 122.054 135.470 2 4 -14 21 41.9323 122.915 2 4 -14 22 72.2648 121.612 2 -4 -15 26 89.0082 380.134 2 -4 15 25 14.2265 118.431 2 -4 15 24-30.8105 127.894 2 -4 15 23 851.579 140.597 2 -4 15 22 402.899 145.944 2 -4 -15 21 360.164 158.380 2 -4 -15 20 1361.76 163.834 2 -4 -15 19 365.339 175.009 2 -4 -15 18 3069.66 161.922 2 -4 -15 17 908.009 153.101 2 -4 -15 16 4879.72 162.792 2 -4 -15 15 2189.17 150.517 2 -4 -15 14-52.6180 146.330 2 -4 -15 13 1220.15 149.946 2 4 15 -12 2231.38 149.863 2 4 15 -11 9178.28 157.745 2 4 15 -10 3647.52 157.621 2 -4 -15 9 34.3696 163.011 2 -4 -15 8 4955.08 166.416 2 -4 -15 7 4234.97 221.299 2 -4 -15 6 2746.15 238.264 2 -4 -15 5 1815.18 175.226 2 -4 -15 4-136.212 181.198 2 -4 -15 3 11505.3 206.160 2 4 15 -2 26901.2 232.059 2 -4 -15 1 2408.02 205.665 2 -4 -15 0 492.434 171.218 2 -4 15 -1 2531.06 178.185 2 -4 15 -2 6836.33 183.135 2 -4 15 -3 884.717 180.720 2 -4 15 -4 2335.37 169.573 2 -4 -15 -5 4166.61 154.718 2 -4 -15 -6 137.700 115.859 2 4 -15 7 182.671 118.765 2 4 15 8 10316.3 129.052 2 4 15 9 3130.98 129.695 2 4 15 10 2654.93 138.907 2 4 15 11 1372.30 130.692 2 4 15 12 869.668 131.495 2 4 15 13 376.452 140.928 2 4 15 14 5941.65 157.616 2 4 15 15-6.08297 149.812 2 4 15 16 166.815 147.638 2 4 15 17 1655.12 141.883 2 4 15 18 1123.21 139.114 2 4 -15 19 219.739 135.763 2 4 -15 20 44.5536 130.385 2 4 -15 21 354.934 123.680 2 -4 15 -22 277.974 132.354 2 -4 16 25 71.6137 126.109 2 -4 16 24 51.7393 121.083 2 -4 16 23 332.566 135.189 2 -4 16 22 377.288 141.341 2 -4 -16 21 72.8675 149.311 2 -4 -16 20 1685.26 158.515 2 -4 -16 19 1653.88 169.043 2 -4 -16 18 4606.49 167.709 2 -4 -16 17 1408.53 161.242 2 -4 -16 16 42.5140 158.612 2 -4 -16 15 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286.857 142.060 2 -5 -1 26 2108.17 135.704 2 -5 1 25 685.266 144.942 2 -5 1 24 7537.38 172.784 2 -5 1 23 218.820 140.883 2 -5 1 22 330.527 167.774 2 -5 1 21 490.524 166.054 2 -5 1 20 400.565 159.495 2 -5 -1 19 35.3474 153.774 2 -5 1 18 792.302 151.823 2 -5 1 17 166.601 149.003 2 -5 1 16 1621.89 158.540 2 -5 1 15 174.804 136.057 2 -5 -1 14-75.1730 132.248 2 -5 -1 13 1465.46 120.907 2 -5 1 12 433.331 128.169 2 -5 -1 11 550.998 148.636 2 -5 -1 10 562.964 142.681 2 -5 -1 9 538.282 188.112 2 5 1 -8 742.578 206.565 2 5 -1 -7 85.0630 178.235 2 -5 1 6 323.710 189.281 2 -5 -1 5 22.2467 170.819 2 -5 -1 4 833.149 203.121 2 -5 -1 3 2384.33 208.718 2 5 -1 -2 1880.64 242.108 2 -5 -1 1 7578.90 267.731 2 -5 -1 0 9159.11 282.367 2 -5 -1 -1 214.630 224.783 2 -5 -1 -2 506.566 206.753 2 -5 -1 -3 17.9442 210.462 2 5 -1 4 2947.45 186.219 2 5 -1 5 6072.08 193.637 2 5 -1 6 225.226 125.708 2 5 -1 7 1395.59 110.826 2 5 -1 8 732.062 108.293 2 -5 -1 -9 6353.62 124.802 2 -5 -1 -10 11156.0 128.854 2 -5 -1 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262.746 2 -5 -2 1 133.850 336.854 2 -5 2 0 410.610 254.456 2 -5 -2 -1 5852.47 348.878 2 -5 -2 -2 4.29637 267.294 2 -5 -2 -3 4273.72 245.733 2 5 -2 4 1540.51 200.671 2 5 -2 5 6933.88 225.558 2 -5 -2 -6 113.294 135.345 2 -5 -2 -7 305.844 116.316 2 -5 -2 -8 2886.22 118.974 2 -5 -2 -9 2727.15 114.504 2 -5 2 -10 1988.67 121.968 2 -5 -2 -11 586.240 116.971 2 -5 -2 -12 107.331 118.716 2 5 2 13 84.9865 123.712 2 5 2 14 606.077 132.882 2 5 2 15 793.711 129.723 2 5 2 16 1400.92 159.341 2 5 2 17-186.542 140.087 2 5 -2 18 248.750 165.219 2 5 -2 19 1551.70 146.516 2 5 2 20 942.979 128.938 2 5 2 21 263.322 128.863 2 5 2 22 111.278 126.590 2 -5 -2 -23 296.562 294.847 2 -5 3 27 258.589 124.913 2 -5 3 26 342.779 121.874 2 -5 3 25 452.596 143.791 2 -5 3 24 1256.37 146.256 2 -5 3 23 130.257 158.033 2 -5 3 22 591.699 162.745 2 -5 3 21 138.673 154.073 2 -5 -3 20 17815.5 213.378 2 -5 -3 19 4.71237 169.184 2 -5 3 18 63.8202 166.947 2 -5 3 17 2732.35 149.903 2 -5 3 16 192.861 133.425 2 -5 -3 15 517.498 130.298 2 -5 3 14 8177.65 207.705 2 -5 -3 13 820.068 146.022 2 -5 -3 12 699.834 133.773 2 -5 -3 11 1646.64 160.623 2 5 3 -10 581.162 147.339 2 5 3 -9 368.666 185.976 2 5 3 -8 1620.87 195.077 2 -5 3 7 746.387 228.361 2 5 -3 -6 900.979 194.974 2 -5 -3 5 6589.21 220.216 2 5 -3 -4 2623.15 241.538 2 5 -3 -3 1812.09 296.212 2 5 -3 -2 170.414 223.754 2 -5 -3 1 1571.72 327.636 2 -5 -3 0 3314.89 289.351 2 -5 -3 -1 13521.8 294.144 2 -5 -3 -2 7422.18 244.078 2 -5 -3 -3 3448.47 197.511 2 -5 -3 -4 626.024 195.366 2 5 3 5 12.3993 204.854 2 -5 3 -6 3029.93 138.976 2 -5 3 -7 3421.65 128.495 2 -5 -3 -8 1929.96 112.560 2 -5 -3 -9 5648.99 124.697 2 -5 -3 -10 99.4116 124.179 2 -5 -3 -11 2778.75 121.391 2 -5 -3 -12 1502.26 120.114 2 -5 -3 -13 51.5739 122.093 2 5 3 14 129.916 137.299 2 5 3 15 1828.05 129.980 2 -5 3 -16 7783.81 184.577 2 5 3 17-29.7203 139.628 2 5 3 18 128.685 148.918 2 5 3 19 2063.36 145.956 2 5 3 20 1226.12 126.388 2 5 3 21 103.949 126.032 2 5 3 22 36.3844 126.578 2 -5 4 27 135.465 132.677 2 -5 4 26 153.819 129.965 2 -5 4 25 422.720 127.604 2 -5 4 24 492.776 152.596 2 -5 4 23 422.111 164.356 2 -5 4 22 2288.38 160.531 2 -5 4 21 1555.34 164.513 2 -5 4 20 1101.79 173.578 2 -5 4 19 52.1752 155.169 2 -5 -4 18 13220.0 177.609 2 -5 4 17 393.501 149.386 2 -5 4 16 1664.15 150.781 2 -5 -4 15 649.884 161.666 2 -5 -4 14 1204.07 148.722 2 -5 -4 13 161.783 130.741 2 5 4 -12 30.6839 141.224 2 5 4 -11 909.490 146.204 2 5 4 -10 4188.14 168.700 2 5 4 -9-250.971 165.230 2 5 4 -8 1042.45 168.734 2 -5 4 7 288.627 174.571 2 5 -4 -6 13422.3 335.032 2 -5 4 5 127.201 247.064 2 5 -4 -4 1794.80 268.745 2 5 -4 -3 943.345 242.943 2 5 -4 -2 4600.09 224.502 2 -5 -4 1 7859.75 338.867 2 -5 -4 0 54.4218 282.271 2 -5 -4 -1 1913.63 223.145 2 -5 -4 -2 1255.51 205.872 2 -5 -4 -3 567.200 217.667 2 -5 -4 -4 518.429 200.529 2 -5 -4 -5 123.631 157.009 2 -5 -4 -6-67.7438 142.791 2 -5 -4 -7 958.394 135.136 2 -5 -4 -8 10104.1 145.900 2 -5 -4 -9 246.328 113.865 2 -5 -4 -10 521.227 122.525 2 -5 -4 -11 5742.93 134.944 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287.302 2 -5 -5 -1 3706.05 279.592 2 -5 -5 -2 6285.64 354.763 2 -5 -5 -3 1621.95 194.142 2 -5 -5 -4 1871.51 204.523 2 -5 5 -5 5857.80 165.613 2 -5 5 -6 7127.44 152.708 2 -5 5 -7 587.255 142.509 2 5 5 8 333.665 119.061 2 -5 -5 -9 5744.80 121.614 2 5 5 10 18972.2 133.374 2 -5 -5 -11 1760.41 127.508 2 -5 -5 -12 600.359 131.103 2 -5 -5 -13 1486.56 139.825 2 5 5 14-99.3404 139.315 2 5 5 15 208.772 132.281 2 5 5 16-66.6355 140.827 2 5 5 17 68.4234 146.293 2 5 5 18 221.452 149.656 2 5 5 19-5.43969 140.972 2 5 5 20 172.993 139.062 2 5 5 21 440.641 125.276 2 5 5 22 86.3092 115.363 2 -5 6 26 980.236 120.550 2 -5 6 25 859.122 143.052 2 -5 6 24 898.680 156.840 2 -5 -6 23 1232.84 141.161 2 -5 -6 22 95.5563 160.716 2 -5 6 21 916.643 165.519 2 -5 6 20 489.841 165.184 2 -5 6 19 2059.09 155.110 2 -5 6 18 188.522 161.818 2 5 6 -17 467.690 161.403 2 -5 -6 16 68.7695 161.812 2 5 6 -15 137.113 174.408 2 5 6 -14 943.213 141.993 2 5 6 -13 191.888 145.203 2 -5 -6 12 360.725 130.488 2 5 6 -11-163.621 165.440 2 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13.7538 188.481 2 -5 7 20 475.937 167.334 2 -5 7 19 40.8508 168.714 2 -5 7 18 82.3346 161.623 2 5 7 -17 313.768 162.260 2 5 7 -16 1818.30 158.154 2 5 7 -15 583.341 161.837 2 5 7 -14 333.111 141.015 2 5 7 -13 444.822 130.012 2 -5 -7 12 508.260 141.850 2 -5 -7 11 1072.26 183.586 2 5 7 -10 6337.20 205.491 2 -5 -7 9 4336.80 175.476 2 -5 -7 8 30.6892 176.281 2 -5 -7 7 507.485 258.054 2 -5 7 6-44.9208 223.637 2 -5 7 5 4172.52 376.315 2 -5 7 4 2195.26 269.323 2 -5 -7 3 2202.67 381.026 2 -5 -7 2 2686.39 274.560 2 -5 -7 1 26693.7 394.556 2 -5 -7 0 4329.08 286.903 2 -5 -7 -1 433.949 347.519 2 -5 -7 -2 6.12151 292.519 2 -5 -7 -3 9533.88 320.861 2 -5 -7 -4 1286.12 207.234 2 -5 7 -5 235.419 160.426 2 -5 7 -6 44.5247 160.185 2 -5 7 -7 578.152 144.770 2 -5 -7 -8 1469.76 120.348 2 -5 -7 -9 1116.47 121.753 2 -5 -7 -10 1602.67 121.908 2 -5 -7 -11 848.797 133.200 2 -5 -7 -12 926.566 136.871 2 -5 -7 -13 185.296 130.505 2 5 7 14 269.758 137.869 2 5 7 15 220.017 147.647 2 5 7 16 1443.70 153.940 2 5 7 17 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0.00 -8 16 16 0.82 0.00 6 19 16 0.10 0.00 -7 22 16 0.47 0.00 4 27 16 0.05 0.00 3 29 16 0.02 0.00 2 31 16 -0.56 0.00 1 32 16 -0.02 0.00 -1 33 16 0.34 0.00 7 7 17 -2.00 0.00 7 8 17 0.14 0.00 -8 15 17 -0.17 0.00 6 17 17 -0.43 0.00 5 22 17 -0.59 0.00 3 28 17 -0.65 0.00 2 30 17 -0.16 0.00 -3 31 17 -0.39 0.00 1 31 17 0.22 0.00 -1 32 17 0.14 0.00 0 32 17 -0.03 0.00 -8 13 18 1.03 0.00 6 15 18 0.55 0.00 -7 19 18 -0.54 0.00 4 24 18 -0.38 0.00 3 27 18 -0.04 0.00 2 29 18 -0.04 0.00 -3 30 18 -0.66 0.00 1 30 18 0.24 0.00 -1 31 18 0.38 0.00 0 31 18 0.17 0.00 -8 10 19 -0.31 0.00 -8 11 19 1.72 0.00 6 12 19 -0.94 0.00 -7 18 19 0.92 0.00 -6 22 19 0.47 0.00 -5 25 19 -1.42 0.00 -3 29 19 0.00 0.00 1 29 19 -0.10 0.00 -1 30 19 1.49 0.00 -8 7 20 1.70 0.00 -8 8 20 0.03 0.00 6 8 20 -0.29 0.00 -7 16 20 0.36 0.00 5 16 20 -0.04 0.00 -6 21 20 0.34 0.00 4 21 20 -1.24 0.00 -5 24 20 -0.55 0.00 3 24 20 -0.03 0.00 -4 26 20 -0.61 0.00 2 26 20 1.05 0.00 -1 29 20 1.00 0.00 -8 1 21 0.48 0.00 -8 2 21 -1.22 0.00 -8 3 21 0.23 0.00 -7 14 21 -0.19 0.00 5 14 21 0.35 0.00 -6 19 21 0.76 0.00 4 19 21 -0.84 0.00 -5 23 21 -0.15 0.00 -4 25 21 -0.32 0.00 2 25 21 1.52 0.00 0 27 21 0.60 0.00 5 10 22 0.73 0.00 -7 11 22 0.93 0.00 -7 12 22 -0.21 0.00 4 17 22 -0.61 0.00 -5 21 22 -0.06 0.00 2 23 22 0.83 0.00 -3 25 22 0.60 0.00 1 25 22 -0.36 0.00 -2 26 22 0.55 0.00 0 26 22 -0.53 0.00 5 3 23 0.71 0.00 5 4 23 0.33 0.00 5 5 23 -0.32 0.00 -7 7 23 -0.20 0.00 -7 8 23 0.57 0.00 -7 9 23 -0.05 0.00 4 14 23 0.12 0.00 -6 15 23 -1.12 0.00 2 21 23 0.64 0.00 -4 22 23 0.46 0.00 1 23 23 0.66 0.00 0 24 23 1.38 0.00 -7 1 24 -0.30 0.00 -7 2 24 -1.29 0.00 -7 3 24 0.85 0.00 4 10 24 -0.02 0.00 -6 13 24 0.06 0.00 3 16 24 0.45 0.00 -5 17 24 1.07 0.00 2 19 24 0.41 0.00 -4 20 24 0.45 0.00 1 21 24 -0.56 0.00 -3 22 24 1.11 0.00 -2 23 24 1.12 0.00 -1 23 24 1.00 0.00 4 2 25 0.64 0.00 4 3 25 -0.21 0.00 4 4 25 0.74 0.00 4 5 25 -0.11 0.00 -6 9 25 -0.63 0.00 -6 10 25 -0.08 0.00 3 13 25 -1.05 0.00 -5 15 25 1.17 0.00 2 17 25 -0.59 0.00 -4 18 25 -0.49 0.00 1 19 25 0.28 0.00 -3 20 25 0.48 0.00 -2 21 25 0.25 0.00 -1 21 25 0.70 0.00 -6 0 26 -0.07 0.00 -6 1 26 0.50 0.00 -6 2 26 0.98 0.00 -6 3 26 -0.74 0.00 -6 4 26 0.65 0.00 -6 5 26 -0.76 0.00 3 8 26 -0.15 0.00 3 9 26 1.26 0.00 -5 12 26 -0.29 0.00 2 14 26 0.08 0.00 -4 16 26 -0.13 0.00 1 17 26 0.31 0.00 -3 18 26 -1.22 0.00 0 18 26 -0.20 0.00 -2 19 26 0.25 0.00 -1 19 26 -0.68 0.00 -5 7 27 0.18 0.00 -5 8 27 -1.32 0.00 2 9 27 -1.46 0.00 2 10 27 -0.63 0.00 -4 12 27 -0.73 0.00 -4 13 27 0.74 0.00 1 13 27 0.57 0.00 -3 15 27 0.89 0.00 -2 16 27 -1.60 0.00 -1 16 27 0.17 0.00 2 0 28 -0.91 0.00 2 1 28 0.00 0.00 2 2 28 -0.14 0.00 -4 7 28 0.88 0.00 -4 8 28 -0.80 0.00 -4 9 28 0.40 0.00 1 9 28 -1.20 0.00 -3 11 28 0.54 0.00 -3 12 28 -1.09 0.00 0 12 28 -0.26 0.00 -2 13 28 0.04 0.00 -1 13 28 -0.81 0.00 -3 5 29 0.37 0.00 -3 6 29 0.30 0.00 0 6 29 -1.13 0.00 -3 7 29 1.20 0.00 0 7 29 0.42 0.00 -2 8 29 0.14 0.00 -1 8 29 1.98 0.00 -2 9 29 0.20 0.00 -1 9 29 -0.16 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 200618) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.000 453 100 ' ' 2 0.500 0.500 0.500 453 100 ' ' 3 0.194 0.208 0.742 7 0 ' ' 4 0.305 0.708 0.758 7 0 ' ' 5 0.694 0.292 0.242 7 0 ' ' 6 0.805 0.792 0.258 7 0 ' ' _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL 007b-1901_twin1_hP 21/n R = 0.12 CELL 8.2796 32.4638 24.8002 90.00 98.61 90.00 SPGR P21/n # Solvent Accessible Volume = 944 # Electrons Found in S.A.V. = 201 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.861 0.103 0.097 ! 7.52 eA-3 C102 0.704 0.627 0.370 ! 4.10 eA-3 C103 0.707 0.106 0.165 ! 4.08 eA-3 C104 0.672 0.673 0.376 ! 3.83 eA-3 C105 0.314 0.439 0.594 ! 3.78 eA-3 C106 0.909 0.042 0.054 ! 3.41 eA-3 C107 0.287 0.939 0.855 ! 2.36 eA-3 Q108 0.273 0.885 0.221 ! 0.53 eA-3 Q109 0.265 0.218 0.380 ! 0.51 eA-3 ) ; _shelx_fab_checksum 87755