data_LP18005_XPREP_a _audit_creation_method 'SHELXL-2018/1' _shelx_SHELXL_version_number '2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C44 H32 O2' _chemical_formula_sum 'C44 H32 O2' _chemical_formula_weight 592.69 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 14.1264(3) _cell_length_b 11.2302(3) _cell_length_c 20.1932(5) _cell_angle_alpha 90 _cell_angle_beta 108.1510(10) _cell_angle_gamma 90 _cell_volume 3044.08(13) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9896 _cell_measurement_theta_min 3.29 _cell_measurement_theta_max 78.64 _exptl_crystal_description 'plate' _exptl_crystal_colour 'clear_pale_red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.293 _exptl_crystal_F_000 1248 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 0.602 _shelx_estimated_absorpt_T_min 0.889 _shelx_estimated_absorpt_T_max 0.942 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.6929 _exptl_absorpt_correction_T_max 0.7542 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type 'CuK\a' _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 31122 _diffrn_reflns_av_unetI/netI 0.0240 _diffrn_reflns_av_R_equivalents 0.0320 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_theta_min 3.292 _diffrn_reflns_theta_max 79.075 _diffrn_reflns_theta_full 67.679 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 6492 _reflns_number_gt 5658 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX3 V2016.1-0' _computing_cell_refinement 'Bruker SAINT 8.37A' _computing_data_reduction 'Bruker SAINT 8.37A' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0511P)^2^+1.4735P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 6492 _refine_ls_number_parameters 438 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0479 _refine_ls_R_factor_gt 0.0407 _refine_ls_wR_factor_ref 0.1059 _refine_ls_wR_factor_gt 0.1006 _refine_ls_goodness_of_fit_ref 1.027 _refine_ls_restrained_S_all 1.027 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.36654(7) 1.09966(9) 0.65552(5) 0.0243(2) Uani 1 1 d . . . . . C1 C 0.52656(8) 0.66470(11) 0.61176(6) 0.0148(2) Uani 1 1 d . . . . . C2 C 0.58893(9) 0.56167(12) 0.64213(6) 0.0174(3) Uani 1 1 d . . . . . C3 C 0.56777(10) 0.45432(12) 0.66905(7) 0.0211(3) Uani 1 1 d . . . . . H3 H 0.501062 0.435128 0.666058 0.025 Uiso 1 1 calc R U . . . C4 C 0.64424(10) 0.37546(13) 0.70025(7) 0.0254(3) Uani 1 1 d . . . . . H4 H 0.629130 0.301931 0.717940 0.031 Uiso 1 1 calc R U . . . C5 C 0.74313(10) 0.40228(13) 0.70610(7) 0.0254(3) Uani 1 1 d . . . . . H5 H 0.794445 0.346628 0.726871 0.031 Uiso 1 1 calc R U . . . C6 C 0.76623(9) 0.51005(13) 0.68158(7) 0.0220(3) Uani 1 1 d . . . . . H6 H 0.833393 0.529796 0.686249 0.026 Uiso 1 1 calc R U . . . C7 C 0.68971(9) 0.58881(12) 0.65008(6) 0.0176(3) Uani 1 1 d . . . . . C8 C 0.69393(9) 0.70618(12) 0.62021(6) 0.0175(3) Uani 1 1 d . . . . . C9 C 0.77395(9) 0.76376(13) 0.60771(6) 0.0198(3) Uani 1 1 d . . . . . H9 H 0.838894 0.730288 0.623567 0.024 Uiso 1 1 calc R U . . . C10 C 0.75723(10) 0.87071(13) 0.57176(7) 0.0221(3) Uani 1 1 d . . . . . H10 H 0.811140 0.911694 0.563278 0.026 Uiso 1 1 calc R U . . . C11 C 0.66102(10) 0.91848(13) 0.54791(7) 0.0225(3) Uani 1 1 d . . . . . H11 H 0.650320 0.991734 0.523152 0.027 Uiso 1 1 calc R U . . . C12 C 0.58074(9) 0.86054(13) 0.55982(7) 0.0203(3) Uani 1 1 d . . . . . H12 H 0.515571 0.892981 0.542323 0.024 Uiso 1 1 calc R U . . . C13 C 0.59672(9) 0.75438(12) 0.59768(6) 0.0168(2) Uani 1 1 d . . . . . C14 C 0.42489(9) 0.68085(11) 0.59367(6) 0.0153(2) Uani 1 1 d . . . . . C15 C 0.34131(8) 0.58401(11) 0.57143(6) 0.0147(2) Uani 1 1 d . . . . . C16 C 0.25216(9) 0.66074(12) 0.52723(6) 0.0154(2) Uani 1 1 d . . . . . C17 C 0.27405(9) 0.78312(12) 0.55015(6) 0.0157(2) Uani 1 1 d . . . . . C18 C 0.20652(9) 0.87535(12) 0.54895(7) 0.0193(3) Uani 1 1 d . . . . . H18 H 0.137998 0.866299 0.523389 0.023 Uiso 1 1 calc R U . A 1 C19 C 0.24004(9) 0.97884(12) 0.58494(7) 0.0211(3) Uani 0.468(5) 1 d . . P B 1 O2 O 0.1763(5) 1.0727(6) 0.5734(2) 0.0207(8) Uani 0.468(5) 1 d . . P B 1 C31 C 0.1411(2) 1.0888(3) 0.63216(17) 0.0294(9) Uani 0.468(5) 1 d . . P B 1 H31A H 0.099008 1.159976 0.625109 0.044 Uiso 0.468(5) 1 calc R U P B 1 H31B H 0.198031 1.098323 0.674475 0.044 Uiso 0.468(5) 1 calc R U P B 1 H31C H 0.102175 1.018971 0.637064 0.044 Uiso 0.468(5) 1 calc R U P B 1 C19' C 0.24004(9) 0.97884(12) 0.58494(7) 0.0211(3) Uani 0.532(5) 1 d . . P B 2 O2' O 0.1802(4) 1.0695(5) 0.5976(2) 0.0245(9) Uani 0.532(5) 1 d . . P B 2 C31' C 0.0765(2) 1.0451(3) 0.57950(18) 0.0337(8) Uani 0.532(5) 1 d . . P B 2 H31D H 0.048933 1.035484 0.528875 0.050 Uiso 0.532(5) 1 calc R U P B 2 H31E H 0.042967 1.111394 0.594528 0.050 Uiso 0.532(5) 1 calc R U P B 2 H31F H 0.066230 0.971734 0.602584 0.050 Uiso 0.532(5) 1 calc R U P B 2 C20 C 0.34312(9) 0.99342(12) 0.62272(6) 0.0181(3) Uani 1 1 d . . . . . C21 C 0.40957(9) 0.90169(12) 0.62521(6) 0.0166(2) Uani 1 1 d . . . . . H21 H 0.477933 0.910203 0.651325 0.020 Uiso 1 1 calc R U . . . C22 C 0.37469(9) 0.79572(11) 0.58861(6) 0.0154(2) Uani 1 1 d . . . . . C23 C 0.36751(9) 0.48939(12) 0.52507(6) 0.0183(3) Uani 1 1 d . . . . . H23A H 0.311745 0.433708 0.508187 0.027 Uiso 1 1 calc R U . . . H23B H 0.427101 0.445824 0.552168 0.027 Uiso 1 1 calc R U . . . H23C H 0.380398 0.528242 0.485281 0.027 Uiso 1 1 calc R U . . . C24 C 0.31939(8) 0.53346(12) 0.63643(6) 0.0152(2) Uani 1 1 d . . . . . C25 C 0.32009(9) 0.41156(12) 0.64974(7) 0.0192(3) Uani 1 1 d . . . . . H25 H 0.332917 0.357032 0.617595 0.023 Uiso 1 1 calc R U . . . C26 C 0.30220(10) 0.36835(13) 0.70972(7) 0.0223(3) Uani 1 1 d . . . . . H26 H 0.302451 0.284992 0.717793 0.027 Uiso 1 1 calc R U . . . C27 C 0.28411(9) 0.44670(13) 0.75736(6) 0.0212(3) Uani 1 1 d . . . . . H27 H 0.273089 0.417608 0.798519 0.025 Uiso 1 1 calc R U . . . C28 C 0.28225(9) 0.56820(13) 0.74433(6) 0.0197(3) Uani 1 1 d . . . . . H28 H 0.269199 0.622373 0.776569 0.024 Uiso 1 1 calc R U . . . C29 C 0.29933(9) 0.61126(12) 0.68450(6) 0.0172(2) Uani 1 1 d . . . . . H29 H 0.297346 0.694617 0.676148 0.021 Uiso 1 1 calc R U . . . C30 C 0.46966(10) 1.12068(14) 0.69105(8) 0.0282(3) Uani 1 1 d . . . . . H30A H 0.507145 1.117567 0.657611 0.042 Uiso 1 1 calc R U . . . H30B H 0.494819 1.059518 0.726837 0.042 Uiso 1 1 calc R U . . . H30C H 0.477738 1.199390 0.713073 0.042 Uiso 1 1 calc R U . . . C32 C 0.17021(9) 0.62616(12) 0.47323(6) 0.0158(2) Uani 1 1 d . . . . . C33 C 0.11560(9) 0.51263(12) 0.45949(6) 0.0168(2) Uani 1 1 d . . . . . C34 C 0.12132(9) 0.41057(12) 0.49971(6) 0.0195(3) Uani 1 1 d . . . . . H34 H 0.171999 0.403241 0.543342 0.023 Uiso 1 1 calc R U . . . C35 C 0.05246(10) 0.31934(13) 0.47570(7) 0.0218(3) Uani 1 1 d . . . . . H35 H 0.057396 0.249085 0.502774 0.026 Uiso 1 1 calc R U . . . C36 C -0.02355(10) 0.32956(13) 0.41257(7) 0.0224(3) Uani 1 1 d . . . . . H36 H -0.069229 0.265862 0.396576 0.027 Uiso 1 1 calc R U . . . C37 C -0.03291(9) 0.43225(13) 0.37292(7) 0.0217(3) Uani 1 1 d . . . . . H37 H -0.085630 0.440357 0.330365 0.026 Uiso 1 1 calc R U . . . C38 C 0.03595(9) 0.52281(12) 0.39645(6) 0.0178(3) Uani 1 1 d . . . . . C39 C 0.04072(9) 0.64020(12) 0.36650(6) 0.0181(3) Uani 1 1 d . . . . . C40 C -0.01393(10) 0.68643(14) 0.30195(7) 0.0237(3) Uani 1 1 d . . . . . H40 H -0.067326 0.642380 0.271520 0.028 Uiso 1 1 calc R U . . . C41 C 0.01081(10) 0.79751(14) 0.28287(7) 0.0253(3) Uani 1 1 d . . . . . H41 H -0.026560 0.830780 0.239317 0.030 Uiso 1 1 calc R U . . . C42 C 0.09017(10) 0.86093(13) 0.32712(7) 0.0232(3) Uani 1 1 d . . . . . H42 H 0.106920 0.936751 0.313123 0.028 Uiso 1 1 calc R U . . . C43 C 0.14539(9) 0.81477(13) 0.39165(7) 0.0213(3) Uani 1 1 d . . . . . H43 H 0.200362 0.857955 0.420980 0.026 Uiso 1 1 calc R U . . . C44 C 0.11931(9) 0.70462(12) 0.41285(6) 0.0173(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0200(5) 0.0161(5) 0.0356(5) -0.0069(4) 0.0071(4) -0.0016(4) C1 0.0138(5) 0.0120(6) 0.0197(5) -0.0029(4) 0.0066(4) -0.0017(4) C2 0.0185(6) 0.0176(7) 0.0164(5) -0.0018(5) 0.0058(4) 0.0020(5) C3 0.0179(6) 0.0201(7) 0.0246(6) 0.0005(5) 0.0056(5) -0.0007(5) C4 0.0251(7) 0.0176(7) 0.0315(7) 0.0038(5) 0.0058(5) -0.0001(5) C5 0.0204(6) 0.0210(7) 0.0321(7) 0.0028(6) 0.0042(5) 0.0052(5) C6 0.0159(6) 0.0215(7) 0.0270(6) -0.0032(5) 0.0045(5) 0.0004(5) C7 0.0184(6) 0.0176(7) 0.0169(5) -0.0033(5) 0.0058(4) -0.0001(5) C8 0.0184(6) 0.0183(7) 0.0153(5) -0.0034(5) 0.0048(4) 0.0000(5) C9 0.0161(6) 0.0236(7) 0.0210(6) -0.0036(5) 0.0074(5) -0.0004(5) C10 0.0210(6) 0.0245(7) 0.0229(6) 0.0006(5) 0.0100(5) -0.0040(5) C11 0.0231(6) 0.0232(7) 0.0224(6) 0.0051(5) 0.0088(5) -0.0011(5) C12 0.0185(6) 0.0220(7) 0.0208(6) 0.0025(5) 0.0067(5) 0.0012(5) C13 0.0174(6) 0.0178(7) 0.0157(5) -0.0018(5) 0.0059(4) -0.0017(5) C14 0.0175(6) 0.0148(6) 0.0134(5) 0.0001(4) 0.0047(4) -0.0016(5) C15 0.0135(5) 0.0150(6) 0.0146(5) 0.0001(4) 0.0030(4) -0.0003(4) C16 0.0152(5) 0.0163(6) 0.0154(5) 0.0023(5) 0.0061(4) -0.0003(5) C17 0.0155(5) 0.0161(6) 0.0152(5) 0.0022(4) 0.0043(4) -0.0016(5) C18 0.0141(5) 0.0189(7) 0.0232(6) 0.0033(5) 0.0032(5) 0.0005(5) C19 0.0180(6) 0.0154(7) 0.0301(7) 0.0030(5) 0.0077(5) 0.0035(5) O2 0.0218(13) 0.0206(14) 0.023(2) 0.0018(18) 0.0120(19) 0.0075(9) C31 0.0315(17) 0.0323(19) 0.0298(17) 0.0037(13) 0.0176(14) 0.0096(14) C19' 0.0180(6) 0.0154(7) 0.0301(7) 0.0030(5) 0.0077(5) 0.0035(5) O2' 0.0214(12) 0.0195(13) 0.036(2) -0.003(2) 0.014(2) 0.0032(9) C31' 0.0207(14) 0.0259(16) 0.0563(19) -0.0002(13) 0.0149(13) 0.0049(11) C20 0.0205(6) 0.0139(6) 0.0207(6) 0.0003(5) 0.0074(5) -0.0019(5) C21 0.0151(5) 0.0160(6) 0.0185(5) 0.0008(5) 0.0053(4) -0.0021(5) C22 0.0152(5) 0.0157(6) 0.0154(5) 0.0025(4) 0.0051(4) -0.0005(4) C23 0.0189(6) 0.0178(7) 0.0181(6) -0.0031(5) 0.0056(5) -0.0001(5) C24 0.0117(5) 0.0171(6) 0.0148(5) 0.0014(4) 0.0013(4) -0.0016(4) C25 0.0187(6) 0.0169(7) 0.0220(6) 0.0003(5) 0.0063(5) 0.0007(5) C26 0.0215(6) 0.0179(7) 0.0274(7) 0.0061(5) 0.0075(5) 0.0003(5) C27 0.0172(6) 0.0273(8) 0.0188(6) 0.0059(5) 0.0051(5) -0.0015(5) C28 0.0170(6) 0.0237(7) 0.0181(6) -0.0020(5) 0.0050(5) -0.0020(5) C29 0.0159(5) 0.0159(6) 0.0186(6) -0.0001(5) 0.0036(4) -0.0015(5) C30 0.0209(6) 0.0228(8) 0.0395(8) -0.0091(6) 0.0072(6) -0.0051(5) C32 0.0147(5) 0.0183(6) 0.0145(5) 0.0010(5) 0.0047(4) -0.0001(5) C33 0.0154(5) 0.0189(7) 0.0170(5) -0.0023(5) 0.0064(4) -0.0015(5) C34 0.0189(6) 0.0204(7) 0.0192(6) -0.0003(5) 0.0058(5) -0.0020(5) C35 0.0239(6) 0.0194(7) 0.0246(6) 0.0004(5) 0.0114(5) -0.0037(5) C36 0.0205(6) 0.0221(7) 0.0265(6) -0.0061(5) 0.0102(5) -0.0078(5) C37 0.0162(6) 0.0287(8) 0.0197(6) -0.0042(5) 0.0048(5) -0.0045(5) C38 0.0148(5) 0.0222(7) 0.0175(6) -0.0020(5) 0.0068(4) -0.0004(5) C39 0.0141(5) 0.0226(7) 0.0181(6) -0.0015(5) 0.0058(4) -0.0003(5) C40 0.0176(6) 0.0317(8) 0.0192(6) 0.0003(5) 0.0020(5) -0.0003(5) C41 0.0215(6) 0.0339(8) 0.0185(6) 0.0068(6) 0.0036(5) 0.0046(6) C42 0.0229(6) 0.0244(7) 0.0232(6) 0.0067(5) 0.0086(5) 0.0021(5) C43 0.0195(6) 0.0225(7) 0.0208(6) 0.0023(5) 0.0047(5) -0.0021(5) C44 0.0149(5) 0.0208(7) 0.0163(5) 0.0012(5) 0.0049(4) 0.0009(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C20 1.3547(16) . ? O1 C30 1.4288(16) . ? C1 C14 1.3793(16) . ? C1 C2 1.4678(17) . ? C1 C13 1.5010(17) . ? C2 C3 1.3927(19) . ? C2 C7 1.4153(17) . ? C3 C4 1.3871(19) . ? C3 H3 0.9500 . ? C4 C5 1.3977(19) . ? C4 H4 0.9500 . ? C5 C6 1.385(2) . ? C5 H5 0.9500 . ? C6 C7 1.3882(18) . ? C6 H6 0.9500 . ? C7 C8 1.4585(18) . ? C8 C9 1.3919(18) . ? C8 C13 1.4129(17) . ? C9 C10 1.3852(19) . ? C9 H9 0.9500 . ? C10 C11 1.3997(19) . ? C10 H10 0.9500 . ? C11 C12 1.3918(18) . ? C11 H11 0.9500 . ? C12 C13 1.3961(18) . ? C12 H12 0.9500 . ? C14 C22 1.4601(17) . ? C14 C15 1.5646(16) . ? C15 C23 1.5358(17) . ? C15 C24 1.5473(16) . ? C15 C16 1.5571(16) . ? C16 C32 1.3760(16) . ? C16 C17 1.4524(18) . ? C17 C22 1.3988(16) . ? C17 C18 1.4032(18) . ? C18 C19' 1.3743(19) . ? C18 C19 1.3743(19) . ? C18 H18 0.9500 . ? C19 O2 1.359(7) . ? C19 C20 1.4273(18) . ? O2 C31 1.433(4) . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C19' O2' 1.397(6) . ? C19' C20 1.4273(18) . ? O2' C31' 1.420(6) . ? C31' H31D 0.9800 . ? C31' H31E 0.9800 . ? C31' H31F 0.9800 . ? C20 C21 1.3840(18) . ? C21 C22 1.4066(17) . ? C21 H21 0.9500 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 C25 1.3946(18) . ? C24 C29 1.3990(17) . ? C25 C26 1.3988(18) . ? C25 H25 0.9500 . ? C26 C27 1.385(2) . ? C26 H26 0.9500 . ? C27 C28 1.388(2) . ? C27 H27 0.9500 . ? C28 C29 1.3906(17) . ? C28 H28 0.9500 . ? C29 H29 0.9500 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C32 C33 1.4712(17) . ? C32 C44 1.4946(17) . ? C33 C34 1.3924(18) . ? C33 C38 1.4168(17) . ? C34 C35 1.3918(18) . ? C34 H34 0.9500 . ? C35 C36 1.3923(19) . ? C35 H35 0.9500 . ? C36 C37 1.387(2) . ? C36 H36 0.9500 . ? C37 C38 1.3851(18) . ? C37 H37 0.9500 . ? C38 C39 1.4607(19) . ? C39 C40 1.3920(18) . ? C39 C44 1.4087(17) . ? C40 C41 1.382(2) . ? C40 H40 0.9500 . ? C41 C42 1.392(2) . ? C41 H41 0.9500 . ? C42 C43 1.3934(18) . ? C42 H42 0.9500 . ? C43 C44 1.3955(19) . ? C43 H43 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C20 O1 C30 116.52(11) . . ? C14 C1 C2 130.87(11) . . ? C14 C1 C13 123.79(11) . . ? C2 C1 C13 105.20(10) . . ? C3 C2 C7 118.21(12) . . ? C3 C2 C1 132.19(11) . . ? C7 C2 C1 109.23(11) . . ? C4 C3 C2 119.90(12) . . ? C4 C3 H3 120.1 . . ? C2 C3 H3 120.1 . . ? C3 C4 C5 121.15(13) . . ? C3 C4 H4 119.4 . . ? C5 C4 H4 119.4 . . ? C6 C5 C4 119.92(13) . . ? C6 C5 H5 120.0 . . ? C4 C5 H5 120.0 . . ? C5 C6 C7 118.96(12) . . ? C5 C6 H6 120.5 . . ? C7 C6 H6 120.5 . . ? C6 C7 C2 121.80(12) . . ? C6 C7 C8 129.72(12) . . ? C2 C7 C8 108.48(11) . . ? C9 C8 C13 121.76(12) . . ? C9 C8 C7 129.41(12) . . ? C13 C8 C7 108.58(11) . . ? C10 C9 C8 118.84(12) . . ? C10 C9 H9 120.6 . . ? C8 C9 H9 120.6 . . ? C9 C10 C11 120.10(12) . . ? C9 C10 H10 120.0 . . ? C11 C10 H10 120.0 . . ? C12 C11 C10 121.16(13) . . ? C12 C11 H11 119.4 . . ? C10 C11 H11 119.4 . . ? C13 C12 C11 119.50(12) . . ? C13 C12 H12 120.3 . . ? C11 C12 H12 120.3 . . ? C12 C13 C8 118.59(11) . . ? C12 C13 C1 132.30(11) . . ? C8 C13 C1 108.35(11) . . ? C1 C14 C22 125.28(11) . . ? C1 C14 C15 127.96(11) . . ? C22 C14 C15 106.70(10) . . ? C23 C15 C24 114.40(11) . . ? C23 C15 C16 109.81(9) . . ? C24 C15 C16 110.45(9) . . ? C23 C15 C14 110.63(9) . . ? C24 C15 C14 110.13(9) . . ? C16 C15 C14 100.55(10) . . ? C32 C16 C17 124.23(11) . . ? C32 C16 C15 128.95(12) . . ? C17 C16 C15 106.69(10) . . ? C22 C17 C18 120.19(12) . . ? C22 C17 C16 110.57(11) . . ? C18 C17 C16 128.09(11) . . ? C19' C18 C17 119.66(11) . . ? C19 C18 C17 119.66(11) . . ? C19 C18 H18 120.2 . . ? C17 C18 H18 120.2 . . ? O2 C19 C18 117.7(3) . . ? O2 C19 C20 120.9(3) . . ? C18 C19 C20 120.38(12) . . ? C19 O2 C31 109.8(3) . . ? O2 C31 H31A 109.5 . . ? O2 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? O2 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C18 C19' O2' 125.8(2) . . ? C18 C19' C20 120.38(12) . . ? O2' C19' C20 113.2(2) . . ? C19' O2' C31' 116.5(4) . . ? O2' C31' H31D 109.5 . . ? O2' C31' H31E 109.5 . . ? H31D C31' H31E 109.5 . . ? O2' C31' H31F 109.5 . . ? H31D C31' H31F 109.5 . . ? H31E C31' H31F 109.5 . . ? O1 C20 C21 125.32(11) . . ? O1 C20 C19 114.55(11) . . ? C21 C20 C19 120.10(12) . . ? O1 C20 C19' 114.55(11) . . ? C21 C20 C19' 120.10(12) . . ? C20 C21 C22 119.21(11) . . ? C20 C21 H21 120.4 . . ? C22 C21 H21 120.4 . . ? C17 C22 C21 120.43(11) . . ? C17 C22 C14 109.69(11) . . ? C21 C22 C14 128.88(11) . . ? C15 C23 H23A 109.5 . . ? C15 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C15 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C25 C24 C29 118.05(11) . . ? C25 C24 C15 122.17(11) . . ? C29 C24 C15 119.78(11) . . ? C24 C25 C26 121.00(12) . . ? C24 C25 H25 119.5 . . ? C26 C25 H25 119.5 . . ? C27 C26 C25 120.21(13) . . ? C27 C26 H26 119.9 . . ? C25 C26 H26 119.9 . . ? C26 C27 C28 119.31(12) . . ? C26 C27 H27 120.3 . . ? C28 C27 H27 120.3 . . ? C29 C28 C27 120.55(12) . . ? C29 C28 H28 119.7 . . ? C27 C28 H28 119.7 . . ? C28 C29 C24 120.87(12) . . ? C28 C29 H29 119.6 . . ? C24 C29 H29 119.6 . . ? O1 C30 H30A 109.5 . . ? O1 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? O1 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C16 C32 C33 131.01(11) . . ? C16 C32 C44 123.53(12) . . ? C33 C32 C44 105.45(10) . . ? C34 C33 C38 118.43(12) . . ? C34 C33 C32 132.20(11) . . ? C38 C33 C32 108.81(11) . . ? C33 C34 C35 119.70(12) . . ? C33 C34 H34 120.1 . . ? C35 C34 H34 120.2 . . ? C36 C35 C34 120.95(13) . . ? C36 C35 H35 119.5 . . ? C34 C35 H35 119.5 . . ? C37 C36 C35 120.32(12) . . ? C37 C36 H36 119.8 . . ? C35 C36 H36 119.8 . . ? C38 C37 C36 118.83(12) . . ? C38 C37 H37 120.6 . . ? C36 C37 H37 120.6 . . ? C37 C38 C33 121.69(12) . . ? C37 C38 C39 129.69(12) . . ? C33 C38 C39 108.58(11) . . ? C40 C39 C44 121.53(13) . . ? C40 C39 C38 129.84(12) . . ? C44 C39 C38 108.47(11) . . ? C41 C40 C39 118.88(12) . . ? C41 C40 H40 120.6 . . ? C39 C40 H40 120.6 . . ? C40 C41 C42 120.38(12) . . ? C40 C41 H41 119.8 . . ? C42 C41 H41 119.8 . . ? C41 C42 C43 120.94(13) . . ? C41 C42 H42 119.5 . . ? C43 C42 H42 119.5 . . ? C42 C43 C44 119.49(12) . . ? C42 C43 H43 120.3 . . ? C44 C43 H43 120.3 . . ? C43 C44 C39 118.69(11) . . ? C43 C44 C32 131.83(11) . . ? C39 C44 C32 108.57(11) . . ? _refine_diff_density_max 0.353 _refine_diff_density_min -0.239 _refine_diff_density_rms 0.048 _shelx_res_file ; TITL LP18005_XPREP_a.res in P2(1)/c LP18005_XPREP_a.res created by SHELXL-2018/1 at 16:46:32 on 16-Apr-2018 REM Old TITL LP18005_XPREP in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.135, Rweak 0.004, Alpha 0.028, Orientation as input REM Formula found by SHELXT: C46 O CELL 1.54178 14.1264 11.2302 20.1932 90.000 108.151 90.000 ZERR 4.000 0.0003 0.0003 0.0005 0.000 0.001 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H O UNIT 176 128 8 TEMP -173.140 SIZE 0.10 0.20 0.20 L.S. 20 BOND $H htab acta LIST 6 FMAP 2 PLAN 10 WGHT 0.051100 1.473500 FVAR 0.35019 0.46792 O1 3 0.366537 1.099662 0.655517 11.00000 0.01999 0.01613 = 0.03556 -0.00693 0.00709 -0.00164 C1 1 0.526563 0.664704 0.611762 11.00000 0.01380 0.01196 = 0.01967 -0.00293 0.00660 -0.00172 C2 1 0.588928 0.561673 0.642131 11.00000 0.01852 0.01761 = 0.01643 -0.00175 0.00579 0.00196 C3 1 0.567766 0.454317 0.669052 11.00000 0.01785 0.02006 = 0.02457 0.00055 0.00564 -0.00068 AFIX 43 H3 2 0.501062 0.435128 0.666058 11.00000 -1.20000 AFIX 0 C4 1 0.644239 0.375455 0.700246 11.00000 0.02507 0.01762 = 0.03154 0.00380 0.00584 -0.00011 AFIX 43 H4 2 0.629130 0.301931 0.717940 11.00000 -1.20000 AFIX 0 C5 1 0.743134 0.402279 0.706097 11.00000 0.02043 0.02102 = 0.03208 0.00280 0.00416 0.00516 AFIX 43 H5 2 0.794445 0.346628 0.726871 11.00000 -1.20000 AFIX 0 C6 1 0.766230 0.510053 0.681582 11.00000 0.01591 0.02153 = 0.02700 -0.00319 0.00449 0.00043 AFIX 43 H6 2 0.833393 0.529796 0.686249 11.00000 -1.20000 AFIX 0 C7 1 0.689706 0.588806 0.650078 11.00000 0.01838 0.01765 = 0.01694 -0.00334 0.00582 -0.00014 C8 1 0.693925 0.706180 0.620212 11.00000 0.01844 0.01829 = 0.01533 -0.00343 0.00480 0.00002 C9 1 0.773947 0.763756 0.607715 11.00000 0.01607 0.02359 = 0.02099 -0.00362 0.00739 -0.00042 AFIX 43 H9 2 0.838894 0.730288 0.623567 11.00000 -1.20000 AFIX 0 C10 1 0.757228 0.870706 0.571760 11.00000 0.02102 0.02448 = 0.02292 0.00064 0.01004 -0.00402 AFIX 43 H10 2 0.811140 0.911694 0.563278 11.00000 -1.20000 AFIX 0 C11 1 0.661016 0.918477 0.547908 11.00000 0.02311 0.02320 = 0.02243 0.00509 0.00877 -0.00114 AFIX 43 H11 2 0.650320 0.991734 0.523152 11.00000 -1.20000 AFIX 0 C12 1 0.580743 0.860540 0.559822 11.00000 0.01847 0.02203 = 0.02081 0.00252 0.00675 0.00120 AFIX 43 H12 2 0.515571 0.892981 0.542323 11.00000 -1.20000 AFIX 0 C13 1 0.596723 0.754383 0.597685 11.00000 0.01743 0.01777 = 0.01574 -0.00184 0.00586 -0.00171 C14 1 0.424885 0.680853 0.593671 11.00000 0.01752 0.01483 = 0.01343 0.00010 0.00473 -0.00161 C15 1 0.341305 0.584013 0.571434 11.00000 0.01354 0.01498 = 0.01460 0.00011 0.00304 -0.00031 C16 1 0.252160 0.660739 0.527233 11.00000 0.01523 0.01633 = 0.01542 0.00228 0.00608 -0.00032 C17 1 0.274047 0.783117 0.550148 11.00000 0.01553 0.01613 = 0.01523 0.00218 0.00431 -0.00155 C18 1 0.206525 0.875348 0.548947 11.00000 0.01409 0.01889 = 0.02320 0.00334 0.00322 0.00050 AFIX 43 H18 2 0.137998 0.866299 0.523389 11.00000 -1.20000 AFIX 0 exyz C19 C19' eadp C19 C19' part 1 21.00 C19 1 0.240037 0.978843 0.584938 21.00000 0.01804 0.01535 = 0.03014 0.00303 0.00769 0.00348 O2 3 0.176270 1.072749 0.573431 21.00000 0.02179 0.02058 = 0.02321 0.00181 0.01200 0.00747 C31 1 0.141092 1.088771 0.632159 21.00000 0.03151 0.03234 = 0.02976 0.00367 0.01757 0.00958 AFIX 137 H31A 2 0.099008 1.159976 0.625109 21.00000 -1.50000 H31B 2 0.198031 1.098323 0.674475 21.00000 -1.50000 H31C 2 0.102175 1.018971 0.637064 21.00000 -1.50000 AFIX 0 part 2 -21.00 C19' 1 0.240037 0.978843 0.584938 -21.00000 0.01804 0.01535 = 0.03014 0.00303 0.00769 0.00348 O2' 3 0.180151 1.069486 0.597618 -21.00000 0.02135 0.01950 = 0.03648 -0.00329 0.01437 0.00319 C31' 1 0.076540 1.045137 0.579497 -21.00000 0.02072 0.02594 = 0.05631 -0.00023 0.01491 0.00490 AFIX 137 H31D 2 0.048933 1.035484 0.528875 -21.00000 -1.50000 H31E 2 0.042967 1.111394 0.594528 -21.00000 -1.50000 H31F 2 0.066230 0.971734 0.602584 -21.00000 -1.50000 AFIX 0 part 0 C20 1 0.343118 0.993419 0.622719 11.00000 0.02054 0.01385 = 0.02070 0.00031 0.00739 -0.00194 C21 1 0.409573 0.901691 0.625209 11.00000 0.01511 0.01604 = 0.01851 0.00085 0.00526 -0.00206 AFIX 43 H21 2 0.477933 0.910203 0.651325 11.00000 -1.20000 AFIX 0 C22 1 0.374691 0.795718 0.588612 11.00000 0.01521 0.01567 = 0.01541 0.00246 0.00510 -0.00052 C23 1 0.367508 0.489386 0.525073 11.00000 0.01889 0.01782 = 0.01808 -0.00306 0.00563 -0.00008 AFIX 137 H23A 2 0.311745 0.433708 0.508187 11.00000 -1.50000 H23B 2 0.427101 0.445824 0.552168 11.00000 -1.50000 H23C 2 0.380398 0.528242 0.485281 11.00000 -1.50000 AFIX 0 C24 1 0.319386 0.533457 0.636430 11.00000 0.01169 0.01709 = 0.01477 0.00143 0.00130 -0.00155 C25 1 0.320090 0.411556 0.649743 11.00000 0.01872 0.01686 = 0.02197 0.00029 0.00630 0.00069 AFIX 43 H25 2 0.332917 0.357032 0.617595 11.00000 -1.20000 AFIX 0 C26 1 0.302196 0.368346 0.709715 11.00000 0.02150 0.01789 = 0.02738 0.00612 0.00753 0.00029 AFIX 43 H26 2 0.302451 0.284992 0.717793 11.00000 -1.20000 AFIX 0 C27 1 0.284108 0.446703 0.757357 11.00000 0.01719 0.02727 = 0.01878 0.00585 0.00510 -0.00154 AFIX 43 H27 2 0.273089 0.417608 0.798519 11.00000 -1.20000 AFIX 0 C28 1 0.282247 0.568202 0.744335 11.00000 0.01698 0.02374 = 0.01813 -0.00201 0.00499 -0.00202 AFIX 43 H28 2 0.269199 0.622373 0.776569 11.00000 -1.20000 AFIX 0 C29 1 0.299326 0.611264 0.684497 11.00000 0.01591 0.01594 = 0.01864 -0.00014 0.00361 -0.00146 AFIX 43 H29 2 0.297346 0.694617 0.676148 11.00000 -1.20000 AFIX 0 C30 1 0.469657 1.120685 0.691050 11.00000 0.02087 0.02280 = 0.03946 -0.00909 0.00725 -0.00513 AFIX 137 H30A 2 0.507145 1.117567 0.657611 11.00000 -1.50000 H30B 2 0.494819 1.059518 0.726837 11.00000 -1.50000 H30C 2 0.477738 1.199390 0.713073 11.00000 -1.50000 AFIX 0 C32 1 0.170212 0.626165 0.473233 11.00000 0.01471 0.01828 = 0.01455 0.00103 0.00466 -0.00012 C33 1 0.115605 0.512632 0.459495 11.00000 0.01537 0.01889 = 0.01698 -0.00233 0.00638 -0.00147 C34 1 0.121324 0.410571 0.499712 11.00000 0.01888 0.02043 = 0.01918 -0.00034 0.00583 -0.00201 AFIX 43 H34 2 0.171999 0.403241 0.543342 11.00000 -1.20000 AFIX 0 C35 1 0.052462 0.319339 0.475699 11.00000 0.02389 0.01942 = 0.02460 0.00042 0.01137 -0.00368 AFIX 43 H35 2 0.057396 0.249085 0.502774 11.00000 -1.20000 AFIX 0 C36 1 -0.023553 0.329561 0.412566 11.00000 0.02050 0.02212 = 0.02646 -0.00608 0.01022 -0.00785 AFIX 43 H36 2 -0.069229 0.265862 0.396576 11.00000 -1.20000 AFIX 0 C37 1 -0.032915 0.432252 0.372918 11.00000 0.01620 0.02865 = 0.01975 -0.00420 0.00485 -0.00452 AFIX 43 H37 2 -0.085630 0.440357 0.330365 11.00000 -1.20000 AFIX 0 C38 1 0.035952 0.522811 0.396451 11.00000 0.01483 0.02223 = 0.01750 -0.00201 0.00681 -0.00041 C39 1 0.040722 0.640197 0.366500 11.00000 0.01414 0.02260 = 0.01815 -0.00149 0.00580 -0.00034 C40 1 -0.013928 0.686430 0.301949 11.00000 0.01755 0.03169 = 0.01924 0.00027 0.00204 -0.00028 AFIX 43 H40 2 -0.067326 0.642380 0.271520 11.00000 -1.20000 AFIX 0 C41 1 0.010808 0.797515 0.282872 11.00000 0.02151 0.03394 = 0.01852 0.00679 0.00358 0.00463 AFIX 43 H41 2 -0.026560 0.830780 0.239317 11.00000 -1.20000 AFIX 0 C42 1 0.090172 0.860933 0.327121 11.00000 0.02293 0.02437 = 0.02321 0.00671 0.00862 0.00208 AFIX 43 H42 2 0.106920 0.936751 0.313123 11.00000 -1.20000 AFIX 0 C43 1 0.145387 0.814774 0.391648 11.00000 0.01948 0.02246 = 0.02084 0.00233 0.00473 -0.00206 AFIX 43 H43 2 0.200362 0.857955 0.420980 11.00000 -1.20000 AFIX 0 C44 1 0.119306 0.704625 0.412852 11.00000 0.01488 0.02081 = 0.01627 0.00121 0.00490 0.00091 HKLF 4 REM LP18005_XPREP_a.res in P2(1)/c REM R1 = 0.0407 for 5658 Fo > 4sig(Fo) and 0.0479 for all 6492 data REM 438 parameters refined using 0 restraints END WGHT 0.0444 1.4715 REM Instructions for potential hydrogen bonds HTAB C31 O1 REM Highest difference peak 0.353, deepest hole -0.239, 1-sigma level 0.048 Q1 1 0.5401 0.6409 0.6445 11.00000 0.05 0.35 Q2 1 0.5512 0.7101 0.6084 11.00000 0.05 0.29 Q3 1 0.4832 0.6764 0.6095 11.00000 0.05 0.29 Q4 1 0.5790 0.2627 0.5933 11.00000 0.05 0.28 Q5 1 0.1539 0.5656 0.4728 11.00000 0.05 0.27 Q6 1 0.4959 0.8245 0.4670 11.00000 0.05 0.26 Q7 1 0.1495 0.6633 0.4473 11.00000 0.05 0.23 Q8 1 0.3288 0.5565 0.6048 11.00000 0.05 0.23 Q9 1 0.8222 0.4001 0.7623 11.00000 0.05 0.22 Q10 1 0.1947 0.6474 0.5050 11.00000 0.05 0.21 ; _shelx_res_checksum 67869 _shelx_hkl_file ; 1 0 0 161.98 4.50 -1 0 0 154.98 4.50 -2 0 0 1120.29 33.10 2 0 0 1219.38 33.40 3 0 0 3787.72 102.39 -3 0 0 3478.35 101.79 -3 0 0 3618.54 101.99 -4 0 0 5.10 0.50 4 0 0 5.10 0.60 -4 0 0 5.50 0.60 5 0 0 0.90 0.40 -5 0 0 0.60 0.40 -6 0 0 41.70 2.00 -7 0 0 141.59 4.90 7 0 0 131.69 4.90 7 0 0 140.59 5.00 -8 0 0 19.40 1.80 8 0 0 18.20 1.80 8 0 0 18.40 1.90 8 0 0 18.20 2.70 -9 0 0 9.00 1.30 9 0 0 7.50 1.20 9 0 0 5.00 2.40 9 0 0 7.80 1.20 10 0 0 4.00 1.20 -10 0 0 3.60 0.80 -10 0 0 3.10 0.90 10 0 0 3.00 0.90 11 0 0 95.19 3.80 -11 0 0 97.29 3.80 -11 0 0 97.19 3.50 11 0 0 95.49 3.90 12 0 0 -0.30 1.30 -12 0 0 -1.20 0.80 12 0 0 0.40 0.90 -13 0 0 39.10 2.30 13 0 0 39.60 2.50 -13 0 0 41.30 2.00 -14 0 0 29.20 1.60 14 0 0 26.20 1.90 -14 0 0 28.30 1.80 -15 0 0 82.49 3.10 -15 0 0 77.09 2.80 15 0 0 80.19 3.20 16 0 0 7.40 1.10 -16 0 0 8.20 1.00 -17 0 0 100.59 3.20 0 -1 0 -0.80 0.10 0 -1 0 -0.90 0.10 0 -1 0 -0.80 0.10 0 1 0 -1.00 0.10 1 -1 0 79.69 2.30 -1 -1 0 77.99 2.30 1 -1 0 74.59 2.30 -1 1 0 81.39 2.30 1 1 0 77.49 2.30 -1 1 0 78.79 2.30 -2 -1 0 437.66 12.40 2 -1 0 446.66 12.40 -2 1 0 449.16 12.50 -2 1 0 442.56 12.40 2 1 0 431.46 12.40 3 -1 0 6.50 0.60 -3 -1 0 8.30 0.50 3 1 0 8.40 0.50 -3 1 0 7.50 0.60 -3 1 0 6.30 0.60 -4 -1 0 16.90 0.90 4 -1 0 19.40 1.00 -4 1 0 18.90 1.00 -4 1 0 17.30 0.90 4 1 0 16.90 0.90 5 -1 0 0.50 0.40 -5 -1 0 1.40 0.50 -5 1 0 0.30 0.40 -5 1 0 1.40 0.40 5 1 0 0.70 0.40 6 -1 0 19.50 1.40 -6 -1 0 19.00 1.30 -6 -1 0 19.70 1.40 -6 1 0 21.40 1.50 6 1 0 21.50 1.40 -7 -1 0 155.88 5.50 7 -1 0 174.58 5.80 7 -1 0 166.48 5.80 -7 1 0 166.98 5.60 7 1 0 165.98 5.60 7 1 0 154.08 5.60 8 -1 0 127.79 4.60 -8 -1 0 121.99 4.20 -8 -1 0 120.69 4.40 8 -1 0 125.29 5.40 8 -1 0 131.29 4.30 8 -1 0 128.49 4.10 8 1 0 124.89 4.40 8 1 0 122.39 5.30 -8 1 0 125.39 4.30 -8 1 0 130.89 4.20 -9 -1 0 84.09 3.30 9 -1 0 80.29 3.50 -9 -1 0 83.59 3.10 9 -1 0 80.99 3.00 9 -1 0 79.39 3.20 9 1 0 82.79 3.70 9 1 0 83.89 3.30 -9 1 0 81.39 3.20 10 -1 0 -0.70 0.90 -10 -1 0 1.50 1.00 -10 -1 0 1.20 0.80 10 -1 0 1.00 1.00 -10 1 0 0.00 0.90 10 1 0 -0.20 0.80 -10 1 0 0.30 0.70 10 1 0 -1.10 1.50 11 -1 0 9.70 1.20 11 -1 0 7.90 1.30 -11 -1 0 8.50 1.20 -11 1 0 7.80 1.00 -11 1 0 9.00 1.20 11 1 0 8.70 1.20 -12 -1 0 290.17 9.10 12 -1 0 296.57 9.00 -12 -1 0 291.37 8.90 12 -1 0 298.77 9.40 -12 1 0 292.57 8.90 12 1 0 284.97 9.30 -12 1 0 297.27 9.20 13 -1 0 6.30 1.20 13 -1 0 6.90 1.20 -13 -1 0 3.10 1.00 -13 -1 0 5.00 0.90 13 1 0 6.00 1.20 -13 1 0 6.00 1.10 -13 1 0 4.90 0.90 14 -1 0 1.30 0.80 -14 -1 0 0.90 0.80 -14 -1 0 0.50 0.60 -14 1 0 0.90 0.80 14 1 0 -0.60 0.70 -14 1 0 -0.30 0.70 -15 -1 0 4.60 0.70 15 -1 0 5.10 0.90 -15 -1 0 6.30 0.90 15 1 0 3.10 0.80 -15 1 0 5.80 0.90 -16 -1 0 23.40 1.40 -16 -1 0 24.50 1.40 16 -1 0 23.10 1.50 -16 1 0 20.30 1.40 16 1 0 22.60 1.40 17 -1 0 0.20 0.70 -17 -1 0 0.40 0.70 0 -2 0 1049.99 32.90 0 -2 0 1265.57 32.90 0 -2 0 1236.68 33.20 0 2 0 1138.79 33.10 1 -2 0 295.77 8.30 1 -2 0 277.87 8.30 -1 2 0 302.87 8.30 2 -2 0 757.92 22.40 -2 -2 0 853.11 22.40 2 -2 0 789.42 22.30 -2 2 0 780.92 22.40 -2 2 0 786.52 22.40 2 2 0 824.52 22.60 3 -2 0 131.39 3.80 3 -2 0 127.29 3.90 -3 -2 0 125.49 3.70 -3 2 0 122.59 3.90 -3 2 0 122.79 3.80 3 2 0 118.79 3.70 -4 -2 0 236.58 6.90 4 -2 0 229.48 7.10 4 2 0 242.78 6.90 -4 2 0 229.08 7.10 -4 2 0 236.68 7.00 -5 -2 0 161.58 4.90 5 -2 0 149.59 5.10 -5 2 0 167.48 5.10 5 2 0 151.38 4.90 5 2 0 151.28 4.90 -5 2 0 161.48 5.10 6 -2 0 31.20 2.00 6 -2 0 30.20 1.90 6 2 0 37.80 1.80 6 2 0 35.90 1.70 -6 2 0 33.70 1.90 -7 -2 0 127.79 4.60 7 -2 0 135.69 4.40 7 -2 0 133.19 4.90 7 -2 0 131.09 5.10 7 -2 0 131.19 4.20 -7 2 0 131.89 4.60 7 2 0 130.89 4.80 -7 2 0 121.29 4.80 7 2 0 128.69 4.70 -8 -2 0 56.59 2.90 -8 -2 0 54.19 2.70 8 -2 0 54.79 2.40 8 -2 0 52.29 3.90 8 -2 0 55.39 2.20 8 -2 0 56.99 3.00 -8 2 0 57.89 2.40 8 2 0 51.99 2.50 -8 2 0 54.09 2.50 -9 -2 0 24.10 1.80 9 -2 0 23.50 1.80 9 -2 0 26.00 1.60 9 -2 0 22.70 2.30 -9 2 0 25.40 1.80 -9 2 0 26.10 1.60 9 2 0 26.90 1.90 10 -2 0 54.89 2.50 10 -2 0 55.99 2.90 -10 -2 0 57.39 2.50 -10 -2 0 55.09 2.70 10 -2 0 53.39 2.30 10 2 0 52.59 2.60 -10 2 0 57.69 2.40 -10 2 0 55.19 2.70 11 -2 0 0.50 0.80 -11 -2 0 0.80 0.70 11 -2 0 0.00 1.00 11 -2 0 0.80 1.00 -11 -2 0 0.70 0.90 11 2 0 1.60 0.90 -11 2 0 1.00 0.80 -11 2 0 2.70 0.80 12 -2 0 7.70 1.30 12 -2 0 7.50 1.10 -12 -2 0 7.60 1.10 -12 -2 0 10.10 1.30 -12 2 0 5.60 1.10 12 2 0 11.50 1.70 -12 2 0 4.80 0.90 13 -2 0 66.79 2.80 13 -2 0 65.09 3.20 -13 -2 0 60.89 2.90 -13 2 0 61.59 2.60 -13 2 0 67.09 2.90 13 2 0 63.69 2.90 14 -2 0 14.00 1.60 -14 -2 0 16.70 1.30 14 -2 0 13.80 1.70 -14 -2 0 17.90 1.50 -14 2 0 16.40 1.50 14 2 0 14.00 1.50 -15 -2 0 31.50 1.80 15 -2 0 30.30 1.90 -15 -2 0 30.20 1.50 -15 2 0 31.40 1.80 15 2 0 30.40 1.70 -16 -2 0 -0.10 0.60 16 -2 0 -0.20 0.60 -16 -2 0 1.20 0.80 -16 2 0 0.10 1.20 16 2 0 1.40 0.70 0 -3 0 0.30 0.10 0 -3 0 0.20 0.20 0 -3 0 0.30 0.10 1 -3 0 66.39 2.10 1 -3 0 69.09 2.20 -1 -3 0 68.59 2.20 1 -3 0 69.99 2.20 -1 3 0 68.79 2.20 2 -3 0 14.80 0.80 2 -3 0 13.50 0.70 2 -3 0 13.00 0.70 -2 3 0 14.30 0.80 3 -3 0 58.09 2.10 3 -3 0 60.29 2.00 3 -3 0 56.59 2.10 3 3 0 60.09 1.80 3 3 0 57.89 1.80 -3 3 0 57.19 2.10 4 -3 0 18.60 1.20 4 -3 0 16.40 1.10 4 3 0 16.00 0.80 -4 3 0 18.20 1.10 4 3 0 15.70 0.80 5 -3 0 622.14 18.10 5 -3 0 619.44 18.10 -5 3 0 636.34 18.10 5 3 0 624.14 17.80 5 3 0 611.64 17.70 6 -3 0 218.48 7.20 6 -3 0 205.68 7.00 6 3 0 213.98 6.70 6 3 0 212.78 6.70 -6 3 0 223.68 7.10 7 -3 0 0.30 1.20 7 -3 0 1.20 0.70 7 -3 0 1.40 0.80 -7 -3 0 -0.60 1.00 7 -3 0 1.70 1.30 7 3 0 1.30 1.00 7 3 0 -0.60 0.90 -7 3 0 2.00 1.00 7 3 0 0.10 0.80 -7 3 0 2.30 1.30 8 -3 0 12.30 1.50 8 -3 0 9.40 1.20 8 -3 0 10.90 1.90 -8 -3 0 12.00 1.70 -8 -3 0 12.80 1.60 -8 3 0 11.10 1.20 -8 3 0 10.80 1.30 8 3 0 12.40 1.60 9 -3 0 5.10 1.60 9 -3 0 5.60 1.10 -9 -3 0 6.40 1.20 9 -3 0 5.90 0.80 -9 3 0 5.60 1.00 9 3 0 5.00 1.10 -9 3 0 4.70 1.10 -10 -3 0 73.79 3.20 10 -3 0 70.19 2.90 -10 -3 0 73.49 3.00 10 -3 0 68.59 3.50 10 -3 0 70.69 2.70 -10 3 0 68.49 2.90 10 3 0 71.79 3.10 -10 3 0 71.49 3.00 11 -3 0 3.70 0.80 -11 -3 0 3.00 1.00 11 -3 0 3.40 1.30 -11 -3 0 2.90 1.10 11 -3 0 2.70 0.90 -11 3 0 2.20 1.00 -11 3 0 2.80 1.00 11 3 0 3.00 1.00 -12 -3 0 0.70 0.80 12 -3 0 -1.10 1.10 12 -3 0 -0.10 0.80 -12 -3 0 -1.20 0.90 12 3 0 0.60 0.90 -12 3 0 -0.10 0.90 -13 -3 0 6.20 0.90 -13 -3 0 6.50 1.30 13 -3 0 8.60 1.10 13 -3 0 6.80 1.20 13 3 0 10.90 1.60 -13 3 0 5.70 1.10 -14 -3 0 -0.20 0.60 14 -3 0 0.60 0.80 14 -3 0 -0.10 0.80 -14 -3 0 0.10 0.80 14 3 0 0.40 0.70 -14 3 0 0.90 0.80 -15 -3 0 12.10 1.10 -15 -3 0 16.30 1.40 15 -3 0 12.80 1.50 15 3 0 13.40 1.30 -15 3 0 13.10 1.40 -16 -3 0 0.80 0.50 -16 -3 0 0.60 0.70 16 -3 0 0.90 0.80 0 -4 0 1420.66 39.70 0 -4 0 1409.06 39.80 0 -4 0 1445.86 39.60 -1 -4 0 93.59 2.90 1 -4 0 89.49 2.80 1 -4 0 87.99 2.80 1 -4 0 87.69 2.80 -1 4 0 88.69 2.90 -2 -4 0 8.30 0.70 2 -4 0 7.50 0.60 2 -4 0 7.40 0.60 2 -4 0 7.50 0.70 -2 4 0 7.00 0.80 3 -4 0 22.70 1.10 3 -4 0 22.90 1.20 3 -4 0 23.00 1.30 -3 4 0 25.10 1.30 4 -4 0 17.10 1.20 4 -4 0 18.40 1.40 4 4 0 17.10 0.70 4 4 0 18.20 0.80 -4 4 0 18.60 1.40 5 -4 0 38.00 2.00 5 -4 0 38.00 2.20 5 4 0 34.90 1.50 5 4 0 37.90 1.50 -5 4 0 36.70 2.20 6 -4 0 129.49 4.30 6 -4 0 132.39 5.10 6 -4 0 133.59 5.00 6 -4 0 122.89 4.40 -6 4 0 127.89 4.60 6 4 0 126.39 4.30 -6 4 0 135.29 5.20 7 -4 0 3.10 0.90 7 -4 0 1.70 1.70 7 -4 0 2.40 0.70 -7 4 0 2.60 1.30 -7 4 0 2.80 1.10 7 4 0 2.70 1.10 7 4 0 2.30 1.30 8 -4 0 114.99 3.80 8 -4 0 110.09 5.20 8 -4 0 119.39 4.10 -8 4 0 113.09 4.20 8 4 0 112.99 4.10 -9 -4 0 34.90 2.80 9 -4 0 37.60 3.10 9 -4 0 36.90 2.10 -9 -4 0 34.50 2.50 9 -4 0 32.80 1.80 -9 4 0 38.30 2.30 9 4 0 35.30 2.40 10 -4 0 0.10 0.80 10 -4 0 -0.10 0.60 -10 -4 0 -0.30 1.20 -10 -4 0 2.00 1.00 10 -4 0 1.50 1.50 -10 4 0 0.70 1.00 10 4 0 0.20 0.90 -11 -4 0 13.30 1.60 -11 -4 0 11.90 1.60 11 -4 0 9.40 1.60 11 -4 0 10.70 1.50 11 -4 0 11.50 1.20 11 4 0 12.70 1.70 -11 4 0 15.70 1.90 -12 -4 0 1.90 0.90 12 -4 0 1.30 0.80 -12 -4 0 1.50 1.10 12 -4 0 1.90 0.90 12 -4 0 4.60 1.40 12 4 0 1.80 1.00 -12 4 0 1.80 1.00 13 -4 0 3.30 1.10 -13 -4 0 4.50 0.90 -13 -4 0 2.10 0.70 13 -4 0 2.90 0.80 -13 4 0 4.20 0.90 13 4 0 2.80 0.90 14 -4 0 7.20 0.90 -14 -4 0 7.40 1.10 14 -4 0 7.90 1.20 -14 -4 0 6.00 0.80 -14 4 0 7.60 1.10 14 4 0 8.10 1.00 -15 -4 0 0.90 0.50 -15 -4 0 0.10 0.80 15 -4 0 -1.00 0.90 -16 -4 0 1.60 1.30 -16 -4 0 2.60 0.60 16 -4 0 1.30 0.90 0 -5 0 -0.30 0.30 -1 -5 0 363.96 10.80 1 -5 0 369.06 10.60 1 -5 0 374.76 10.70 1 -5 0 379.76 10.60 -2 -5 0 164.58 5.30 2 -5 0 167.28 5.20 2 -5 0 170.48 5.20 2 -5 0 171.88 5.30 -2 5 0 177.18 5.40 -3 -5 0 1.70 0.60 3 -5 0 2.30 0.70 3 -5 0 2.60 0.60 3 -5 0 2.60 0.60 -3 5 0 3.00 0.80 4 -5 0 106.49 3.90 -4 -5 0 99.09 3.80 4 -5 0 105.59 3.90 5 -5 0 162.38 5.80 5 -5 0 163.78 5.70 -5 5 0 151.48 5.30 -5 5 0 163.08 5.90 6 -5 0 148.19 4.90 6 -5 0 145.19 4.70 6 -5 0 137.19 5.70 -6 5 0 145.89 5.00 -6 5 0 150.28 6.20 7 -5 0 29.30 1.60 7 -5 0 26.40 1.80 -7 5 0 22.70 2.20 -7 5 0 29.60 4.40 7 5 0 29.30 2.40 8 -5 0 14.80 1.60 8 -5 0 16.50 1.40 -8 5 0 18.30 2.50 8 5 0 18.80 2.10 9 -5 0 64.79 2.50 9 -5 0 63.59 4.30 9 -5 0 63.09 2.80 9 5 0 60.89 2.90 -9 5 0 57.49 3.20 -10 -5 0 11.20 1.50 -10 -5 0 12.60 1.80 10 -5 0 5.50 1.90 10 -5 0 10.80 1.50 10 -5 0 8.90 1.20 10 5 0 11.90 1.40 -10 5 0 12.10 1.60 11 -5 0 3.40 1.80 -11 -5 0 6.60 1.50 11 -5 0 3.90 0.70 11 -5 0 3.50 0.90 -11 -5 0 4.50 1.00 -11 5 0 3.70 1.30 11 5 0 5.00 1.20 12 -5 0 0.40 0.60 -12 -5 0 0.70 0.90 12 -5 0 -1.60 1.40 -12 -5 0 -0.80 1.10 12 -5 0 1.20 0.80 12 5 0 0.30 0.90 13 -5 0 1.40 1.30 13 -5 0 2.20 0.70 -13 -5 0 0.80 1.10 -13 -5 0 0.80 0.70 -13 5 0 0.00 1.20 14 -5 0 3.10 1.30 14 -5 0 2.10 0.70 -14 -5 0 1.70 0.70 -14 -5 0 1.50 1.10 15 -5 0 11.10 1.20 -15 -5 0 10.20 1.30 15 -5 0 9.30 1.40 -15 -5 0 12.00 1.00 -16 -5 0 0.00 0.70 0 -6 0 50.29 2.00 1 -6 0 347.87 9.80 1 -6 0 352.66 9.80 -1 -6 0 339.97 10.20 1 -6 0 347.37 10.20 2 -6 0 471.25 13.60 -2 -6 0 477.05 13.70 2 -6 0 477.35 13.60 2 -6 0 478.35 13.60 -2 6 0 464.85 13.90 -2 6 0 452.85 14.50 3 -6 0 16.70 1.50 3 -6 0 15.60 1.60 3 -6 0 14.40 1.40 -3 -6 0 13.50 1.70 -3 6 0 12.70 2.00 -4 -6 0 163.28 5.70 4 -6 0 159.58 5.80 -4 6 0 162.68 6.10 -4 6 0 165.98 6.30 5 -6 0 17.90 2.10 5 -6 0 20.00 2.00 -5 -6 0 24.00 2.80 -5 6 0 21.40 3.00 -5 6 0 13.80 2.40 6 -6 0 30.80 1.80 6 -6 0 29.30 2.00 -6 6 0 24.10 3.40 -7 6 0 29.10 3.40 8 -6 0 78.39 3.20 8 -6 0 77.69 2.90 -8 6 0 68.89 4.80 9 -6 0 44.20 2.10 9 -6 0 44.00 2.40 10 -6 0 98.59 3.80 -10 -6 0 92.09 3.90 10 -6 0 100.89 3.50 11 -6 0 0.90 0.80 11 -6 0 0.20 0.60 -12 -6 0 1.50 0.80 12 -6 0 0.90 1.80 12 -6 0 1.70 0.70 12 -6 0 1.70 0.60 13 -6 0 4.70 1.80 13 -6 0 5.60 0.80 -13 -6 0 5.50 0.90 13 -6 0 4.20 0.80 -13 -6 0 7.20 2.10 14 -6 0 -1.40 1.80 14 -6 0 0.00 0.60 -14 -6 0 0.00 0.60 -15 -6 0 34.00 1.50 15 -6 0 31.30 1.60 0 -7 0 0.10 0.80 0 7 0 0.50 1.70 1 -7 0 169.38 5.60 -1 -7 0 171.78 5.60 1 7 0 182.98 6.70 -1 7 0 175.68 6.60 2 -7 0 20.00 1.50 2 -7 0 21.50 1.80 -2 7 0 20.90 2.70 2 7 0 21.10 3.30 3 -7 0 52.49 3.00 -3 7 0 54.29 3.40 3 7 0 46.00 4.20 -4 7 0 1.80 1.50 4 7 0 0.80 2.60 5 -7 0 14.60 1.50 5 -7 0 18.50 2.10 -5 7 0 18.90 2.80 -6 7 0 7.60 1.80 7 -7 0 9.90 1.30 7 -7 0 11.60 1.40 -7 7 0 7.80 1.80 8 -7 0 1.80 0.70 8 -7 0 2.50 1.00 -8 7 0 2.60 2.00 9 -7 0 52.49 2.30 9 -7 0 52.49 2.50 -9 7 0 41.20 4.10 10 -7 0 213.78 6.90 10 -7 0 210.88 6.60 11 -7 0 0.00 0.70 -11 -7 0 -2.80 1.10 11 -7 0 1.00 0.50 12 -7 0 4.10 0.70 -12 -7 0 6.20 1.00 12 -7 0 4.30 0.70 -13 -7 0 3.00 0.80 13 -7 0 2.00 0.60 -14 -7 0 18.70 1.30 0 8 0 -0.20 1.50 -1 8 0 45.90 3.40 1 8 0 56.09 3.60 2 8 0 165.38 6.50 3 8 0 15.50 2.30 -3 8 0 20.20 2.80 4 8 0 4.80 2.30 -4 8 0 1.50 1.60 5 -8 0 2.80 1.20 5 -8 0 4.90 1.50 -5 8 0 2.70 1.50 6 -8 0 44.40 2.30 6 -8 0 49.50 2.70 -6 8 0 53.69 3.50 7 -8 0 284.47 8.80 7 -8 0 289.17 8.60 -7 8 0 275.17 9.60 8 -8 0 16.70 1.80 8 -8 0 18.10 1.50 -8 8 0 19.20 2.90 9 -8 0 15.90 1.70 9 -8 0 15.20 1.40 -9 8 0 16.10 2.20 10 -8 0 5.00 0.90 10 -8 0 4.90 0.70 11 -8 0 2.10 0.50 11 -8 0 0.70 0.70 12 -8 0 2.40 0.60 12 -8 0 1.60 0.50 13 -8 0 14.20 1.10 -13 -8 0 16.60 1.50 14 -8 0 7.80 0.90 0 9 0 0.00 1.30 1 9 0 37.00 3.20 -1 9 0 29.70 2.90 2 9 0 75.39 4.30 -2 9 0 76.29 4.10 -3 9 0 -0.20 1.40 3 9 0 0.20 1.80 4 9 0 114.49 5.40 -4 9 0 107.19 5.00 5 -9 0 63.39 2.90 5 -9 0 61.29 3.40 -5 9 0 71.89 3.90 6 -9 0 7.30 1.40 6 -9 0 6.30 1.10 -6 9 0 6.10 1.60 7 -9 0 205.58 6.60 7 -9 0 205.98 6.40 -7 9 0 198.28 7.40 8 -9 0 25.60 1.60 9 -9 0 12.40 1.10 9 -9 0 10.10 1.40 -9 9 0 10.80 1.80 10 -9 0 7.30 0.90 10 -9 0 9.90 1.30 11 -9 0 0.10 0.60 11 -9 0 -0.90 0.50 12 -9 0 1.60 0.60 12 -9 0 3.00 0.60 13 -9 0 2.70 0.70 0 10 0 159.68 6.40 -1 10 0 1.90 1.40 1 10 0 2.40 1.60 2 10 0 55.99 3.80 -2 10 0 54.69 3.60 -3 10 0 117.79 5.20 3 10 0 101.29 5.00 -4 10 0 87.49 4.40 4 10 0 84.59 4.80 5 -10 0 16.30 1.90 -5 10 0 20.30 2.60 6 -10 0 128.79 4.70 -6 10 0 131.09 5.40 7 -10 0 2.50 0.70 7 -10 0 3.00 1.10 -7 10 0 1.50 1.20 8 -10 0 116.39 3.80 8 -10 0 115.19 4.00 -8 10 0 105.49 4.50 9 -10 0 40.40 1.70 9 -10 0 33.50 2.00 -9 10 0 42.50 3.00 10 -10 0 3.20 0.80 10 -10 0 2.50 0.50 11 -10 0 1.20 0.70 11 -10 0 1.60 0.50 12 -10 0 18.70 1.80 0 11 0 -2.40 1.30 1 11 0 129.69 5.40 -1 11 0 121.99 5.40 2 11 0 -1.40 1.30 -2 11 0 0.00 1.30 -3 11 0 16.60 2.30 3 11 0 11.80 2.30 4 11 0 21.60 3.10 5 -11 0 24.10 1.80 -5 11 0 21.00 2.30 6 -11 0 0.40 0.80 -6 11 0 -0.80 1.00 7 -11 0 1.60 0.70 -7 11 0 0.70 1.10 8 -11 0 3.40 1.30 8 -11 0 3.10 0.60 -8 11 0 1.40 1.20 9 -11 0 16.50 1.80 9 -11 0 21.10 1.10 10 -11 0 3.40 0.50 0 12 0 8.70 1.50 -1 12 0 1.00 1.10 1 12 0 1.90 1.20 -2 12 0 -0.50 0.90 2 12 0 1.00 1.30 -3 12 0 3.80 1.00 3 12 0 4.50 1.60 -4 12 0 5.40 1.10 5 -12 0 4.90 1.00 -5 12 0 3.40 1.10 6 -12 0 5.30 0.80 -6 12 0 4.80 1.10 -7 12 0 12.70 1.60 8 -12 0 27.30 1.30 -8 12 0 26.70 2.50 9 -12 0 11.70 0.90 0 13 0 -0.80 1.00 1 13 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95.89 3.40 -16 -1 1 95.79 3.30 -16 -1 1 92.29 3.10 -16 1 1 93.89 3.30 16 1 -1 96.39 3.30 -15 -1 1 6.50 0.90 -15 -1 1 7.60 1.00 15 -1 -1 6.70 1.00 15 1 -1 6.90 1.00 -15 1 1 6.80 1.00 -15 1 1 8.10 0.90 -14 -1 1 18.60 1.60 14 -1 -1 23.10 1.70 -14 -1 1 18.30 1.30 -14 1 1 17.20 1.50 14 1 -1 16.10 1.50 -14 1 1 16.00 1.30 -13 -1 1 35.40 2.10 -13 -1 1 33.40 1.90 13 -1 -1 34.20 2.40 13 -1 -1 32.10 2.30 13 1 -1 34.00 2.20 -13 1 1 31.80 1.80 -13 1 1 34.70 2.10 12 -1 -1 55.09 2.60 -12 -1 1 47.20 2.60 12 -1 -1 53.09 2.80 -12 1 1 51.79 2.60 12 1 -1 48.60 2.70 -12 1 1 53.99 2.30 -11 -1 1 2.30 0.80 11 -1 -1 3.80 1.00 11 -1 -1 5.50 1.20 -11 -1 1 2.40 1.00 -11 1 1 2.70 0.80 -11 1 1 2.40 0.90 11 1 -1 2.10 0.90 10 -1 -1 1.90 0.90 10 1 -1 3.00 1.00 10 1 -1 3.20 1.60 9 -1 -1 84.39 3.20 9 -1 -1 81.29 3.00 -9 -1 1 82.49 3.30 9 -1 -1 83.79 3.50 -9 1 1 86.99 3.30 9 1 -1 82.29 3.30 9 1 -1 76.49 3.70 -8 -1 1 51.89 2.60 8 -1 -1 49.80 2.20 -8 -1 1 56.49 2.50 8 -1 -1 50.09 2.70 8 -1 -1 53.79 3.40 8 -1 -1 47.40 2.30 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5 -4 4 34.80 3.00 -5 4 -4 44.00 3.00 5 4 4 35.90 2.60 5 4 4 35.90 2.40 -6 -4 -4 52.79 4.30 6 -4 4 48.90 2.40 6 -4 4 48.50 2.10 6 -4 4 40.70 4.50 -6 4 -4 48.90 4.20 6 4 4 45.70 2.60 -6 4 -4 46.90 2.90 7 -4 4 5.00 1.00 7 -4 4 6.40 2.50 7 -4 4 5.90 0.90 -7 -4 -4 7.70 1.60 -7 -4 -4 7.10 1.80 7 4 4 7.90 1.30 -7 4 -4 8.80 1.50 8 -4 4 0.60 0.60 8 -4 4 0.20 0.90 -8 -4 -4 1.60 1.40 8 4 4 -0.10 1.00 -8 4 -4 0.70 1.20 -9 -4 -4 32.40 2.10 -9 -4 -4 31.30 2.50 9 -4 4 34.60 3.20 9 -4 4 35.40 2.10 9 -4 4 33.80 1.80 -9 4 -4 33.00 2.40 9 4 4 33.50 2.30 10 -4 4 49.99 2.20 10 -4 4 48.00 3.30 -10 -4 -4 51.79 2.90 -10 -4 -4 49.40 2.50 10 -4 4 51.19 2.60 10 4 4 54.19 2.70 -10 4 -4 49.10 2.80 11 -4 4 52.19 2.20 -11 -4 -4 51.59 2.50 11 -4 4 51.09 3.20 -11 -4 -4 51.69 2.80 11 -4 4 50.69 2.50 11 4 4 51.69 2.60 -11 4 -4 50.39 2.80 12 -4 4 3.10 1.20 12 -4 4 4.60 0.80 -12 -4 -4 7.20 0.90 -12 -4 -4 4.40 1.00 -12 4 -4 3.80 1.00 12 4 4 5.60 0.90 -13 -4 -4 -0.20 0.80 -13 -4 -4 1.20 0.60 13 -4 4 2.40 1.10 13 -4 4 0.30 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2.50 -8 5 4 45.90 2.60 -8 5 4 45.10 2.60 -8 5 4 48.90 4.20 7 -5 -4 32.80 1.90 7 -5 -4 31.20 1.80 -7 5 4 38.10 3.80 -7 5 4 26.50 2.20 6 -5 -4 0.50 0.90 6 -5 -4 0.00 1.40 -6 -5 4 -0.20 1.30 6 -5 -4 0.50 1.00 -6 5 4 -1.90 1.50 -6 5 4 1.30 1.00 -5 -5 4 8.00 1.50 5 -5 -4 7.70 1.20 5 -5 -4 7.60 1.30 -5 5 4 5.40 1.20 -5 5 4 9.10 1.60 -4 -5 4 3.70 1.00 4 -5 -4 3.00 0.90 4 -5 -4 4.80 0.90 -4 5 4 4.40 0.70 -3 -5 4 54.49 2.60 3 -5 -4 53.89 2.50 3 -5 -4 57.39 2.30 -3 5 4 53.09 1.80 -2 -5 4 102.19 3.70 2 -5 -4 95.99 3.30 2 -5 -4 94.89 3.40 1 -5 -4 96.09 3.20 -1 -5 4 92.89 2.90 1 -5 -4 92.49 3.10 -1 -5 4 95.69 3.50 0 -5 4 672.93 19.50 0 -5 -4 668.83 19.10 0 -5 4 657.93 19.40 0 5 4 713.13 19.10 0 5 -4 666.23 19.00 -1 -5 -4 81.29 2.70 1 -5 4 83.89 3.20 1 -5 4 84.29 3.00 -1 5 -4 83.29 2.90 -1 5 -4 82.59 3.50 1 5 4 83.99 2.70 2 -5 4 8.60 1.30 2 -5 4 7.60 1.40 -2 -5 -4 9.30 0.80 -2 5 -4 11.10 1.90 -2 5 -4 8.90 1.20 3 -5 4 42.20 2.40 3 -5 4 44.40 2.50 -3 -5 -4 43.50 1.80 -3 -5 -4 45.70 1.70 -3 -5 -4 42.40 1.80 -3 5 -4 42.80 3.00 3 5 4 42.90 1.80 -4 -5 -4 49.10 2.10 -4 -5 -4 46.70 2.10 4 -5 4 49.80 2.80 4 -5 4 44.10 2.70 4 -5 4 50.69 3.20 -4 5 -4 51.59 3.70 4 5 4 45.50 2.20 -5 -5 -4 1.20 1.00 5 -5 4 1.30 1.00 5 -5 4 -0.30 0.80 5 5 4 -0.20 1.40 -5 5 -4 0.50 2.10 6 -5 4 44.90 2.10 6 -5 4 43.10 2.40 -6 5 -4 39.70 4.30 -6 5 -4 45.20 3.70 6 5 4 43.20 2.60 7 -5 4 6.10 1.10 7 -5 4 5.60 0.80 -7 5 -4 6.20 1.80 -8 -5 -4 81.09 3.60 -8 -5 -4 85.79 4.10 8 -5 4 87.49 3.40 8 -5 4 85.79 3.10 -8 5 -4 80.99 3.80 8 5 4 81.09 3.50 9 -5 4 66.99 2.60 -9 -5 -4 60.29 3.40 9 -5 4 64.69 4.20 -9 -5 -4 59.99 2.90 9 -5 4 63.69 2.90 -9 5 -4 62.49 3.30 9 5 4 63.89 3.00 -10 -5 -4 0.90 0.90 -10 -5 -4 0.40 1.30 10 -5 4 -1.20 0.80 10 -5 4 0.10 0.70 10 -5 4 -0.60 1.70 -10 5 -4 -2.00 1.40 10 5 4 -0.30 1.00 -11 -5 -4 0.50 1.10 11 -5 4 1.60 1.60 11 -5 4 -0.20 0.70 11 5 4 -0.80 0.90 -11 5 -4 -2.40 1.20 12 -5 4 3.70 1.50 -12 -5 -4 3.70 0.80 12 -5 4 4.50 0.90 -12 -5 -4 4.40 1.10 13 -5 4 0.20 0.60 -13 -5 -4 -1.50 0.90 13 -5 4 2.40 1.30 -13 -5 -4 1.00 0.60 -14 -5 -4 4.80 1.10 14 -5 4 3.90 1.50 -14 -5 -4 5.10 0.70 14 -5 4 5.50 0.80 -16 -6 4 10.70 1.00 -15 -6 4 -0.10 0.50 15 -6 -4 0.80 0.60 15 -6 -4 2.90 1.80 14 -6 -4 19.80 2.10 14 -6 -4 16.00 1.30 -14 -6 4 16.60 1.30 13 -6 -4 12.00 1.90 -13 -6 4 11.10 1.30 13 -6 -4 11.40 1.10 13 -6 -4 10.90 1.20 12 -6 -4 -3.00 1.70 12 -6 -4 0.80 0.70 12 -6 -4 0.70 0.60 -12 -6 4 1.70 0.90 -11 -6 4 16.20 2.20 11 -6 -4 21.60 1.50 11 -6 -4 25.10 3.30 11 -6 -4 22.40 1.80 10 -6 -4 50.79 2.20 10 -6 -4 50.29 2.40 -10 6 4 55.39 4.50 9 -6 -4 0.00 0.80 9 -6 -4 1.30 0.70 -9 6 4 2.20 2.00 -9 6 4 0.80 1.00 8 -6 -4 53.09 2.50 8 -6 -4 55.79 2.30 -8 6 4 54.39 3.80 -8 6 4 54.09 2.70 7 -6 -4 112.79 3.90 7 -6 -4 113.99 4.00 -7 6 4 112.09 5.30 6 -6 -4 20.10 1.80 6 -6 -4 15.30 1.90 -6 6 4 20.60 3.10 -6 6 4 21.50 1.90 -5 -6 4 290.87 10.00 5 -6 -4 292.87 8.90 5 -6 -4 287.67 8.90 5 6 -4 280.37 10.00 -5 6 4 297.57 8.90 -5 6 4 303.17 9.90 -4 -6 4 56.99 3.50 4 -6 -4 53.69 3.20 -4 6 4 57.19 2.70 -4 6 4 59.59 3.80 4 6 -4 53.59 4.00 -3 -6 4 10.60 1.50 3 -6 -4 7.30 1.20 3 -6 -4 8.50 1.40 -3 6 4 7.50 1.50 3 6 -4 9.90 2.10 2 -6 -4 171.78 5.40 -2 -6 4 174.38 6.00 2 -6 -4 172.08 5.60 2 6 -4 165.68 6.40 1 -6 -4 1.10 0.50 -1 -6 4 1.20 0.90 1 -6 -4 1.10 0.60 1 6 -4 1.30 1.50 -1 6 4 -0.30 1.90 0 -6 4 37.40 2.40 0 -6 4 38.50 1.50 0 -6 -4 37.80 1.50 0 -6 4 40.60 1.50 0 -6 -4 38.60 1.50 0 6 4 40.30 4.70 0 6 -4 39.50 3.00 1 -6 4 50.49 2.20 1 -6 4 48.10 2.70 1 -6 4 47.20 2.90 -1 6 -4 47.40 3.20 2 -6 4 68.79 3.10 2 -6 4 71.99 3.40 -2 6 -4 73.09 3.80 -2 6 -4 71.89 4.90 3 -6 4 44.30 3.00 3 -6 4 43.80 2.90 -3 6 -4 47.70 3.30 4 -6 4 63.39 3.10 4 -6 4 59.99 2.90 -4 6 -4 69.19 3.80 5 -6 4 124.59 4.20 5 -6 4 121.29 4.40 -5 6 -4 115.29 5.20 6 -6 4 100.49 3.60 6 -6 4 106.59 3.90 -6 6 -4 92.59 5.20 7 -6 4 2.10 1.00 7 -6 4 1.50 0.70 -7 6 -4 4.50 2.40 8 -6 4 6.90 1.10 -8 -6 -4 8.30 1.60 8 -6 4 6.90 0.90 9 -6 4 29.50 1.70 -9 -6 -4 26.80 2.30 9 -6 4 29.90 2.00 10 -6 4 8.90 1.10 -10 -6 -4 10.60 1.30 10 -6 4 8.40 1.20 -10 -6 -4 12.50 1.70 -11 -6 -4 10.30 1.60 11 -6 4 10.60 1.10 11 -6 4 11.90 1.30 -11 -6 -4 10.00 1.20 12 -6 4 31.00 1.70 -12 -6 -4 29.60 1.60 12 -6 4 25.70 1.50 -12 -6 -4 27.60 2.50 -13 -6 -4 12.40 1.70 13 -6 4 13.30 1.10 -13 -6 -4 15.20 1.10 14 -6 4 61.59 2.30 -14 -6 -4 62.69 2.20 15 -7 -4 39.20 1.60 -15 -7 4 39.20 1.70 14 -7 -4 37.30 1.70 13 -7 -4 3.90 0.70 13 -7 -4 2.70 0.60 12 -7 -4 4.50 0.60 12 -7 -4 4.20 0.80 -12 -7 4 2.60 1.00 11 -7 -4 6.90 0.80 11 -7 -4 8.60 1.10 10 -7 -4 51.69 2.50 10 -7 -4 50.29 2.20 -10 7 4 50.99 4.00 9 -7 -4 5.50 0.90 9 -7 -4 7.50 1.10 -9 7 4 7.00 1.90 8 -7 -4 0.90 0.80 8 -7 -4 1.60 0.70 -8 7 4 2.30 0.90 -8 7 4 0.30 1.60 7 -7 -4 282.67 8.60 7 -7 -4 275.17 8.50 -7 7 4 281.27 8.80 -7 7 4 284.17 9.70 6 -7 -4 76.99 3.20 6 -7 -4 79.09 3.20 -6 7 4 79.19 3.20 -6 7 4 80.09 4.40 5 -7 -4 5.30 1.40 5 -7 -4 2.90 1.20 -5 7 4 3.00 1.60 -5 7 4 5.30 1.10 5 7 -4 3.70 2.10 4 7 -4 253.87 8.60 -4 7 4 238.48 8.60 -4 7 4 242.38 7.60 3 -7 -4 4.10 1.50 -3 -7 4 1.20 1.80 -3 7 4 1.70 1.20 3 7 -4 3.50 1.70 -3 7 4 3.90 1.80 -2 -7 4 31.90 3.30 2 -7 -4 30.90 2.10 -2 7 4 29.90 3.10 2 7 -4 35.80 3.00 -2 7 4 30.30 2.50 -1 -7 4 460.55 14.70 -1 7 4 497.85 15.10 1 7 -4 483.35 14.90 0 -7 4 88.79 4.50 0 7 4 94.59 4.80 0 7 -4 97.59 4.40 1 -7 4 93.69 4.60 1 7 4 101.19 4.90 -1 7 -4 88.79 4.40 -2 7 -4 177.48 6.60 2 7 4 172.48 7.00 -3 7 -4 3.10 1.50 4 -7 4 16.20 2.00 4 -7 4 25.50 2.50 -4 7 -4 23.40 3.30 5 -7 4 53.29 2.80 5 -7 4 51.29 2.40 -5 7 -4 45.70 3.50 6 -7 4 47.30 2.60 6 -7 4 45.60 2.20 -6 7 -4 43.60 3.50 7 -7 4 20.30 1.50 7 -7 4 19.40 1.90 -7 7 -4 20.30 3.30 8 -7 4 76.19 3.20 8 -7 4 70.49 2.90 9 -7 4 12.20 1.60 9 -7 4 12.70 1.30 10 -7 4 2.60 0.60 10 -7 4 3.80 0.80 -10 -7 -4 4.20 1.20 11 -7 4 16.80 1.40 -11 -7 -4 15.30 1.60 11 -7 4 13.80 1.10 -12 -7 -4 3.20 0.80 12 -7 4 3.10 0.70 13 -7 4 24.50 1.40 -13 -7 -4 24.90 1.40 14 -8 -4 10.60 1.00 -14 -8 4 11.70 1.70 -13 -8 4 14.90 1.60 13 -8 -4 10.80 1.00 13 -8 -4 12.10 1.10 12 -8 -4 0.20 0.60 12 -8 -4 0.20 0.50 11 -8 -4 1.30 0.70 11 -8 -4 -0.80 0.50 10 -8 -4 6.70 1.00 10 -8 -4 7.90 1.10 -10 8 4 9.10 1.80 9 -8 -4 42.60 2.30 9 -8 -4 47.80 2.10 -9 8 4 40.50 3.40 8 -8 -4 150.48 4.90 8 -8 -4 147.59 5.10 -8 8 4 155.98 6.30 7 -8 -4 4.90 1.10 7 -8 -4 5.20 0.90 -7 8 4 5.90 1.80 6 -8 -4 163.88 5.40 6 -8 -4 157.78 5.50 6 8 -4 157.98 6.80 -6 8 4 163.48 6.60 -6 8 4 168.18 5.50 5 -8 -4 0.90 1.20 5 -8 -4 0.80 1.30 -5 8 4 0.20 1.00 -5 8 4 2.70 1.60 5 8 -4 2.30 1.90 -4 8 4 5.60 1.80 4 8 -4 6.40 1.80 -3 8 4 195.48 7.30 3 8 -4 177.38 7.00 -3 8 4 186.48 6.00 -2 8 4 81.09 4.30 2 8 -4 72.59 4.70 1 8 -4 70.19 3.90 -1 8 4 63.69 6.00 0 8 -4 19.60 2.60 1 8 4 12.60 3.60 -1 8 -4 14.20 2.50 -2 8 -4 32.60 2.90 -3 8 -4 16.90 2.50 4 -8 4 266.57 8.20 4 -8 4 263.77 8.50 -4 8 -4 268.67 9.20 5 -8 4 25.40 2.00 5 -8 4 28.30 2.50 -5 8 -4 33.20 3.10 6 -8 4 -0.20 0.70 6 -8 4 -0.30 1.00 -6 8 -4 1.60 1.50 7 -8 4 36.80 2.00 7 -8 4 37.10 2.30 -7 8 -4 35.40 3.30 8 -8 4 28.60 2.00 8 -8 4 25.80 1.60 -8 8 -4 30.30 3.20 9 -8 4 31.60 1.60 9 -8 4 33.90 1.90 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5.50 1.20 -6 8 -6 5.60 1.70 7 -8 6 37.40 2.30 7 -8 6 40.30 2.00 8 -8 6 0.00 0.60 -8 -8 -6 0.20 1.40 8 -8 6 0.10 0.80 9 -8 6 1.90 0.70 -9 -8 -6 1.40 1.20 9 -8 6 2.20 0.60 10 -8 6 -0.10 0.60 10 -8 6 -0.20 0.50 -10 -8 -6 -0.90 0.90 11 -8 6 5.00 0.70 11 -8 6 4.90 0.70 -11 -8 -6 4.50 0.80 12 -8 6 2.30 0.60 13 -9 -6 2.40 0.60 13 -9 -6 3.40 0.60 12 -9 -6 0.40 0.60 12 -9 -6 1.00 0.50 11 -9 -6 7.00 0.90 11 -9 -6 7.50 1.10 -11 9 6 6.10 1.70 10 -9 -6 0.50 0.70 10 -9 -6 0.90 0.60 -10 9 6 3.40 1.40 9 -9 -6 0.70 0.70 9 -9 -6 0.10 0.50 -9 9 6 -0.80 1.20 8 -9 -6 1.30 0.90 8 -9 -6 0.70 0.60 -8 9 6 0.40 1.30 7 -9 -6 114.79 4.30 7 -9 -6 120.89 4.10 -7 9 6 118.89 5.30 6 -9 -6 11.60 1.40 6 -9 -6 10.20 1.20 6 9 -6 13.60 2.20 -6 9 6 7.70 1.80 5 -9 -6 208.58 7.00 5 -9 -6 218.88 7.00 5 9 -6 220.98 7.90 -5 9 6 230.38 8.30 4 -9 -6 49.70 2.90 -4 9 6 48.00 3.60 4 9 -6 44.50 3.30 -3 9 6 112.69 5.30 3 9 -6 113.79 5.10 2 9 -6 233.28 8.10 -2 9 6 213.48 8.30 -1 9 6 84.19 4.50 1 9 -6 76.19 4.10 0 9 6 9.90 1.90 0 9 -6 6.60 1.60 -1 9 -6 353.56 11.40 1 9 6 331.07 11.40 2 9 6 4.50 2.10 -2 9 -6 2.30 1.40 3 -9 6 140.19 5.00 -3 9 -6 145.19 5.90 4 -9 6 296.87 9.10 4 -9 6 287.27 9.30 -4 9 -6 306.57 10.00 5 -9 6 33.30 2.50 5 -9 6 35.40 2.00 -5 9 -6 35.00 2.90 6 -9 6 117.59 4.20 6 -9 6 102.79 4.60 -6 9 -6 117.39 4.70 7 -9 6 3.50 0.90 7 -9 6 2.70 0.70 -7 9 -6 0.10 1.60 8 -9 6 6.70 1.00 8 -9 6 8.70 1.10 9 -9 6 15.90 1.10 9 -9 6 18.80 1.40 -9 -9 -6 15.40 2.10 10 -9 6 74.09 2.70 -10 -9 -6 75.69 3.00 10 -9 6 76.69 2.50 11 -9 6 5.90 0.80 12 -10 -6 6.80 0.80 12 -10 -6 6.10 0.70 11 -10 -6 2.30 0.70 11 -10 -6 1.30 0.50 10 -10 -6 -0.10 0.70 10 -10 -6 -0.30 0.50 -10 10 6 1.20 1.20 9 -10 -6 68.39 2.50 9 -10 -6 70.79 2.80 -9 10 6 67.89 3.40 8 -10 -6 2.60 0.60 8 -10 -6 3.60 0.90 -8 10 6 2.60 1.20 7 -10 -6 26.90 1.50 7 -10 -6 27.80 2.00 -7 10 6 26.80 2.40 6 -10 -6 10.60 1.50 6 -10 -6 13.00 1.40 6 10 -6 11.60 1.90 -6 10 6 13.40 2.40 5 -10 -6 27.00 1.90 5 10 -6 26.80 2.80 -5 10 6 29.80 2.90 4 -10 -6 27.40 2.30 -4 10 6 26.70 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10 206.78 6.60 -7 -5 -10 216.18 6.90 7 5 10 218.48 6.90 8 -5 10 132.39 5.70 8 -5 10 132.79 4.30 -8 -5 -10 125.99 4.80 8 -5 10 134.29 4.70 -8 -5 -10 123.09 4.70 9 -5 10 0.90 0.70 -9 -5 -10 1.40 1.00 9 -5 10 -1.60 1.70 -9 -5 -10 0.90 0.70 9 -5 10 0.20 0.70 9 5 10 0.50 0.80 -10 -5 -10 -0.30 0.90 10 -5 10 -0.40 0.70 -10 -5 -10 0.30 0.60 10 -5 10 1.30 1.60 10 5 10 1.30 0.90 -11 -5 -10 1.00 0.60 11 -5 10 -1.00 1.70 11 -5 10 0.70 0.60 -12 -5 -10 7.40 0.90 -16 -6 10 16.50 1.00 15 -6 -10 5.90 0.80 15 -6 -10 3.70 1.90 14 -6 -10 41.00 1.80 -14 -6 10 42.10 1.80 14 -6 -10 35.20 3.20 -13 -6 10 10.50 1.20 13 -6 -10 8.40 1.10 13 -6 -10 8.60 1.00 13 -6 -10 9.90 1.80 -13 6 10 10.60 1.40 -12 -6 10 12.30 1.40 12 -6 -10 12.30 1.00 12 -6 -10 14.10 1.90 12 -6 -10 11.20 1.20 -12 6 10 11.20 1.50 -12 6 10 9.60 2.10 11 -6 -10 75.99 2.70 -11 -6 10 67.69 3.10 11 -6 -10 76.09 3.00 -11 6 10 71.79 4.10 -11 6 10 75.99 3.30 -10 -6 10 44.90 2.60 10 -6 -10 43.90 2.00 10 -6 -10 42.30 2.20 -10 6 10 46.30 3.40 -10 6 10 46.20 2.60 9 -6 -10 2.10 0.70 9 -6 -10 0.40 0.70 -9 6 10 1.10 1.10 8 -6 -10 279.87 8.30 8 -6 -10 263.17 8.10 8 6 -10 247.88 9.30 -8 6 10 275.77 8.60 7 -6 -10 11.70 1.50 7 -6 -10 10.50 1.40 7 6 -10 11.60 2.10 -7 6 10 11.40 1.70 6 -6 -10 194.18 6.10 6 -6 -10 189.68 6.10 6 6 -10 179.68 6.90 -6 6 10 187.18 6.30 5 -6 -10 133.19 4.70 5 -6 -10 130.59 5.10 5 6 -10 127.79 5.40 -5 6 10 141.89 4.80 5 6 -10 133.49 4.40 4 -6 -10 19.20 2.00 4 -6 -10 23.50 2.10 -4 6 10 21.70 2.20 4 6 -10 22.90 1.90 4 6 -10 20.70 2.80 3 -6 -10 19.90 2.10 3 -6 -10 15.50 2.20 -3 6 10 13.90 1.80 3 6 -10 15.70 1.80 2 -6 -10 53.99 3.10 2 -6 -10 52.79 3.10 -2 6 10 55.79 2.70 2 6 -10 55.09 2.60 1 -6 -10 10.80 1.70 1 -6 -10 11.50 1.80 -1 -6 10 10.00 1.90 1 6 -10 9.20 1.80 -1 6 10 11.90 1.70 1 6 -10 10.50 1.30 0 -6 10 204.88 7.00 0 -6 -10 209.78 6.90 0 -6 10 186.68 6.60 0 -6 -10 201.48 6.90 0 6 -10 206.48 7.30 1 -6 10 219.38 8.20 -1 -6 -10 242.18 7.90 -1 -6 -10 246.48 8.00 1 -6 10 229.68 8.20 -1 6 -10 249.08 8.30 1 6 10 244.98 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2.80 0.90 8 -7 10 2.10 0.80 8 -7 10 1.50 0.60 -8 -7 -10 3.10 1.40 -8 -7 -10 1.10 0.80 -9 -7 -10 7.00 1.50 -9 -7 -10 7.50 0.90 9 -7 10 6.40 0.90 9 -7 10 6.40 0.70 10 -7 10 1.90 0.60 -11 -7 -10 2.80 0.60 11 -7 10 2.70 0.60 14 -8 -10 1.30 0.50 13 -8 -10 12.40 1.00 13 -8 -10 9.80 1.00 -13 -8 10 11.20 1.40 12 -8 -10 1.50 0.60 12 -8 -10 1.00 0.50 11 -8 -10 50.09 2.10 11 -8 -10 50.69 1.90 -11 8 10 49.30 3.00 10 -8 -10 2.10 0.50 10 -8 -10 0.90 0.60 -10 8 10 3.20 1.30 -10 8 10 2.40 0.80 9 -8 -10 31.80 1.60 9 -8 -10 29.70 1.80 -9 8 10 31.30 1.90 -9 8 10 26.60 2.70 8 -8 -10 36.00 2.00 8 -8 -10 35.50 1.80 -8 8 10 33.60 2.10 8 8 -10 34.20 4.00 -8 8 10 36.30 3.10 7 -8 -10 7.20 1.00 7 -8 -10 5.10 1.00 -7 8 10 7.20 1.20 -7 8 10 5.40 1.70 7 8 -10 10.00 2.00 6 -8 -10 4.60 1.00 6 -8 -10 4.60 0.90 6 8 -10 5.00 1.60 -6 8 10 3.20 1.60 -6 8 10 2.90 1.00 5 -8 -10 76.49 3.10 5 -8 -10 74.49 3.20 -5 8 10 77.19 3.20 5 8 -10 73.09 4.00 -5 8 10 80.49 4.40 4 -8 -10 51.39 2.70 4 -8 -10 53.69 2.90 4 8 -10 52.79 3.40 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5 -2 14 1.70 1.00 5 -2 14 3.30 0.90 -5 -2 -14 2.80 2.10 -5 2 -14 2.80 1.10 5 2 14 1.30 1.10 6 -2 14 1.50 1.30 -6 -2 -14 2.20 0.80 6 -2 14 2.50 1.00 -6 -2 -14 1.40 1.00 -6 2 -14 2.40 1.00 6 2 14 3.10 1.10 -7 -2 -14 34.10 1.70 7 -2 14 32.40 1.90 -7 -2 -14 33.50 2.10 7 -2 14 32.70 2.40 7 2 14 29.00 2.10 -7 2 -14 33.40 2.00 -8 -2 -14 3.80 0.70 -8 -2 -14 0.70 0.70 8 -2 14 2.60 1.00 8 -2 14 2.40 0.80 8 2 14 1.70 0.80 -8 2 -14 2.80 0.90 9 -2 14 8.20 1.20 -9 -2 -14 13.50 1.30 -9 -2 -14 10.50 1.10 9 -2 14 12.50 1.40 -9 2 -14 12.40 1.40 9 2 14 11.00 1.30 -10 -2 -14 7.20 1.00 10 -2 14 8.50 1.00 -10 2 -14 6.80 1.10 10 2 14 6.50 0.80 -11 -2 -14 35.80 1.50 16 -3 -14 14.40 1.20 -16 -3 14 15.30 1.10 -16 -3 14 15.20 1.10 -16 3 14 11.90 1.50 -15 -3 14 0.40 0.50 -15 -3 14 -0.20 0.60 15 -3 -14 -0.50 0.70 15 3 -14 0.70 0.60 -15 3 14 -0.10 0.70 14 -3 -14 43.00 2.20 14 -3 -14 43.20 1.90 -14 -3 14 42.60 2.00 -14 -3 14 42.40 1.80 -14 3 14 44.50 2.00 14 3 -14 42.50 1.90 -14 3 14 43.60 2.50 -13 -3 14 5.90 0.90 13 -3 -14 5.60 1.00 -13 -3 14 5.10 0.80 13 -3 -14 6.10 0.80 -13 3 14 4.80 0.80 -13 3 14 4.70 1.10 13 3 -14 5.60 0.80 12 -3 -14 122.49 4.10 -12 -3 14 122.29 4.20 -12 -3 14 121.19 4.10 12 -3 -14 118.69 4.50 12 3 -14 122.49 4.20 -12 3 14 118.59 4.20 -12 3 14 112.09 4.60 11 -3 -14 96.49 3.50 -11 -3 14 95.89 3.50 -11 -3 14 88.99 3.60 11 -3 -14 99.69 4.00 11 3 -14 91.19 3.50 -11 3 14 94.89 3.60 -11 3 14 94.49 4.10 -10 -3 14 11.70 1.60 10 -3 -14 13.60 1.60 10 -3 -14 13.20 1.40 10 -3 -14 14.80 1.20 -10 -3 14 14.30 1.50 -10 3 14 14.30 1.60 10 3 -14 13.80 1.50 -10 3 14 10.50 1.50 9 -3 -14 83.29 3.60 9 -3 -14 79.99 3.20 9 -3 -14 81.89 2.90 -9 -3 14 79.59 3.20 -9 -3 14 77.99 3.30 -9 3 14 81.99 3.70 -9 3 14 83.39 3.30 9 3 -14 79.09 3.20 8 -3 -14 134.69 5.20 8 -3 -14 137.39 4.50 -8 -3 14 143.59 5.00 8 -3 -14 140.89 4.80 -8 -3 14 145.29 4.80 8 3 -14 141.89 4.90 -8 3 14 147.99 4.90 -8 3 14 137.19 5.30 7 -3 -14 4.70 1.30 7 -3 -14 7.60 1.10 -7 -3 14 7.10 1.10 7 -3 -14 6.20 0.90 -7 -3 14 8.20 1.20 -7 3 14 6.50 1.10 7 3 -14 9.00 1.20 -7 3 14 5.60 1.20 7 3 -14 3.60 1.50 6 -3 -14 32.10 2.80 -6 -3 14 37.50 2.30 6 -3 -14 34.50 1.80 -6 -3 14 37.10 2.10 6 -3 -14 36.80 2.10 6 3 -14 34.00 3.20 6 3 -14 35.00 2.10 -6 3 14 37.00 2.10 -6 3 14 34.70 2.50 -5 -3 14 250.77 7.90 5 -3 -14 248.38 8.40 5 -3 -14 254.17 7.90 5 -3 -14 259.67 7.70 -5 -3 14 260.77 8.10 -5 3 14 258.77 7.90 5 3 -14 244.08 8.00 -5 3 14 240.08 8.20 5 3 -14 253.57 8.90 -4 -3 14 67.19 3.30 4 -3 -14 66.39 3.90 4 -3 -14 70.69 3.10 4 -3 -14 70.29 2.90 4 3 -14 74.79 4.10 -4 3 14 68.09 3.40 4 3 -14 75.29 3.10 -4 3 14 71.19 3.20 3 -3 -14 0.30 2.00 3 -3 -14 -0.30 0.80 -3 -3 14 0.80 0.90 3 -3 -14 0.30 0.70 -3 3 14 0.50 1.00 -3 3 14 1.20 1.00 3 3 -14 0.50 0.90 3 3 -14 -0.40 1.30 2 -3 -14 38.20 3.80 -2 -3 14 39.90 2.40 -2 -3 14 39.50 2.20 2 -3 -14 36.50 2.40 2 -3 -14 41.50 2.20 2 3 -14 33.10 3.00 -2 3 14 39.80 2.50 2 3 -14 38.80 2.50 2 3 -14 44.00 3.00 -2 3 14 39.10 2.60 -1 -3 14 286.07 8.50 -1 -3 14 283.87 8.70 1 -3 -14 273.97 8.70 1 -3 -14 278.87 8.50 1 -3 -14 264.07 9.60 1 3 -14 269.17 8.60 -1 3 14 273.47 8.90 1 3 -14 275.27 9.30 1 3 -14 274.67 8.80 -1 3 14 270.77 8.50 0 -3 -14 95.19 3.60 0 -3 14 90.29 3.50 0 -3 -14 92.79 3.90 0 -3 14 98.59 3.80 0 3 14 102.49 4.10 0 3 -14 88.19 4.50 0 3 -14 90.79 3.90 1 -3 14 41.10 4.20 -1 -3 -14 42.90 2.30 1 -3 14 41.10 2.10 1 -3 14 40.80 2.50 -1 -3 -14 43.70 2.60 -1 3 -14 35.90 2.60 1 3 14 42.50 2.60 -1 3 -14 31.00 3.10 1 3 14 35.90 2.60 2 -3 14 67.09 3.10 2 -3 14 60.69 2.70 -2 -3 -14 64.79 2.90 -2 -3 -14 62.59 3.10 2 -3 14 63.89 4.40 -2 3 -14 63.89 3.90 2 3 14 68.29 4.20 2 3 14 59.69 3.20 -2 3 -14 63.89 3.10 3 -3 14 46.80 2.20 -3 -3 -14 47.30 2.70 3 -3 14 43.50 2.60 3 -3 14 50.29 3.90 -3 -3 -14 46.00 2.50 3 3 14 42.40 2.80 -3 3 -14 53.09 3.70 -3 3 -14 44.30 2.70 4 -3 14 91.79 3.80 4 -3 14 93.19 3.40 4 -3 14 87.79 4.70 -4 -3 -14 96.19 3.70 -4 -3 -14 90.39 3.90 4 3 14 97.39 4.10 -4 3 -14 93.09 3.80 5 -3 14 212.58 7.10 5 -3 14 220.38 6.70 -5 -3 -14 204.88 6.90 -5 -3 -14 213.58 7.20 5 -3 14 215.38 7.70 -5 3 -14 216.88 7.00 5 3 14 213.38 7.30 6 -3 14 3.60 1.50 6 -3 14 2.30 0.90 -6 -3 -14 1.20 0.90 -6 -3 -14 0.70 0.80 6 3 14 1.60 1.00 -7 -3 -14 38.40 2.20 7 -3 14 40.40 2.10 -7 -3 -14 41.10 1.90 7 -3 14 35.90 2.70 -7 3 -14 34.80 2.20 7 3 14 37.40 2.20 -8 -3 -14 0.40 0.70 -8 -3 -14 -0.30 0.60 8 -3 14 -1.00 1.00 8 -3 14 -0.20 0.70 -8 3 -14 0.80 1.00 8 3 14 -1.20 0.70 -9 -3 -14 48.40 2.10 9 -3 14 48.00 2.10 9 -3 14 50.79 2.60 -9 -3 -14 50.39 1.90 9 3 14 50.79 2.10 -10 -3 -14 35.00 1.60 10 -3 14 32.00 2.10 10 3 14 29.70 1.50 -10 3 -14 32.30 1.80 16 -4 -14 9.10 1.40 -16 -4 14 8.60 0.80 -16 -4 14 6.80 0.90 15 -4 -14 10.30 1.40 -15 -4 14 11.40 0.90 15 -4 -14 10.30 1.40 -14 -4 14 83.99 3.00 14 -4 -14 84.19 3.00 14 -4 -14 88.89 3.40 -14 -4 14 87.79 2.90 -14 4 14 85.79 3.00 -14 4 14 83.09 3.40 -13 -4 14 7.10 1.00 13 -4 -14 9.50 1.10 -13 -4 14 9.00 1.00 13 -4 -14 8.20 1.10 -13 4 14 11.50 1.60 -13 4 14 7.90 1.00 13 4 -14 8.10 1.20 -12 -4 14 13.10 1.40 12 -4 -14 17.00 1.50 -12 -4 14 14.00 1.30 12 -4 -14 17.50 1.90 -12 4 14 15.00 1.70 -12 4 14 16.20 1.50 12 4 -14 14.00 1.30 -11 -4 14 221.28 7.20 11 -4 -14 226.98 6.80 11 -4 -14 237.48 7.20 -11 -4 14 222.98 7.10 11 -4 -14 222.48 7.50 -11 4 14 236.58 7.10 -11 4 14 231.48 7.60 11 4 -14 225.18 7.10 10 -4 -14 0.70 0.70 -10 -4 14 0.00 0.80 10 -4 -14 1.50 0.60 10 -4 -14 0.10 1.20 -10 -4 14 1.80 0.90 10 4 -14 0.80 0.70 -10 4 14 1.50 1.10 -10 4 14 -0.60 0.90 -9 -4 14 100.29 3.80 9 -4 -14 101.99 4.30 -9 -4 14 101.29 3.90 9 -4 -14 101.29 3.80 9 -4 -14 103.39 3.50 -9 4 14 100.79 4.20 -9 4 14 105.99 3.80 9 4 -14 96.99 3.70 8 -4 -14 81.19 3.20 8 -4 -14 83.79 3.00 -8 -4 14 79.79 3.40 -8 -4 14 82.89 3.30 8 -4 -14 76.69 3.90 -8 4 14 81.99 3.30 8 4 -14 85.19 3.20 -8 4 14 78.29 3.60 7 -4 -14 0.70 0.70 -7 -4 14 0.20 1.00 7 -4 -14 0.10 1.30 -7 -4 14 0.60 0.90 7 -4 -14 -0.60 0.70 7 4 -14 0.30 0.70 -7 4 14 1.00 1.00 7 4 -14 -0.70 1.60 -7 4 14 0.20 1.00 6 -4 -14 8.80 1.30 6 -4 -14 8.90 1.80 6 -4 -14 11.70 1.50 -6 -4 14 13.10 1.90 -6 -4 14 13.10 1.70 -6 4 14 12.60 1.80 6 4 -14 12.20 1.60 6 4 -14 13.20 2.20 -6 4 14 7.80 1.30 5 -4 -14 12.70 1.40 5 -4 -14 12.30 1.60 -5 -4 14 12.90 1.80 -5 -4 14 13.70 1.60 5 4 -14 20.90 3.10 5 4 -14 11.50 1.50 -5 4 14 15.10 1.90 -5 4 14 14.70 1.90 -4 -4 14 17.40 2.10 4 -4 -14 21.10 1.80 -4 -4 14 16.30 1.80 4 -4 -14 16.00 1.60 -4 4 14 15.50 2.00 4 4 -14 17.70 1.70 -4 4 14 18.70 2.20 -3 -4 14 133.89 4.70 3 -4 -14 137.59 4.90 -3 -4 14 135.59 4.90 3 -4 -14 138.29 4.70 -3 4 14 128.49 5.10 3 4 -14 133.49 5.60 3 4 -14 136.29 4.80 -3 4 14 139.39 5.10 2 -4 -14 217.38 7.00 -2 -4 14 221.98 7.00 -2 -4 14 230.38 7.20 2 -4 -14 217.78 7.20 2 4 -14 218.48 7.20 2 4 -14 223.68 7.80 -2 4 14 218.98 7.30 -2 4 14 199.48 7.00 1 -4 -14 0.70 0.90 -1 -4 14 2.00 0.90 -1 -4 14 1.70 1.10 1 -4 -14 -0.30 0.90 1 4 -14 -0.40 0.90 1 4 -14 2.00 1.40 -1 4 14 0.10 1.10 0 -4 -14 188.58 6.10 0 -4 14 185.08 6.30 0 -4 -14 189.18 6.30 0 -4 14 183.38 6.00 0 4 -14 178.88 6.30 0 4 -14 176.78 6.80 0 4 14 191.78 6.50 -1 -4 -14 4.10 1.20 1 -4 14 4.50 1.10 1 -4 14 3.80 0.90 -1 -4 -14 2.50 1.00 1 4 14 3.60 1.10 2 -4 14 6.10 1.00 -2 -4 -14 7.60 1.40 -2 -4 -14 6.50 1.10 2 -4 14 4.30 1.10 2 4 14 8.80 1.40 -3 -4 -14 4.30 1.20 3 -4 14 3.30 1.00 -3 -4 -14 4.50 1.00 3 -4 14 5.20 1.00 3 4 14 3.60 1.10 -3 4 -14 5.90 1.90 -4 -4 -14 45.20 2.40 -4 -4 -14 45.00 2.70 4 -4 14 50.09 4.00 4 -4 14 46.20 2.20 4 -4 14 46.70 2.60 4 4 14 44.70 2.60 5 -4 14 3.80 0.80 -5 -4 -14 5.80 1.00 5 -4 14 4.30 1.00 -5 -4 -14 4.90 1.20 5 4 14 7.40 1.20 6 -4 14 30.30 1.60 -6 -4 -14 33.70 1.80 6 -4 14 27.30 1.90 -6 -4 -14 35.20 2.10 6 -4 14 32.40 3.10 6 4 14 29.70 2.00 7 -4 14 0.00 0.80 -7 -4 -14 0.00 0.60 7 -4 14 0.70 0.70 7 -4 14 -1.50 1.50 -7 -4 -14 0.60 0.80 7 4 14 0.70 0.70 8 -4 14 3.00 0.80 -8 -4 -14 1.90 0.80 -8 -4 -14 3.20 0.70 8 -4 14 4.50 1.50 8 4 14 2.10 0.80 9 -4 14 5.80 1.50 -9 -4 -14 1.70 0.70 9 -4 14 1.80 0.70 -9 -4 -14 2.80 0.60 -10 -4 -14 28.60 1.40 -10 4 -14 26.20 1.50 -15 -5 14 4.80 0.80 -15 -5 14 6.40 1.10 15 -5 -14 4.80 0.80 15 -5 -14 7.50 1.20 14 -5 -14 13.70 1.90 14 -5 -14 15.10 1.10 -14 -5 14 15.40 1.00 -14 5 14 11.80 1.30 13 -5 -14 5.50 0.80 -13 -5 14 5.30 0.80 13 -5 -14 4.70 1.10 -13 -5 14 6.50 0.90 -13 5 14 5.80 0.90 12 -5 -14 13.10 1.20 -12 -5 14 15.50 1.30 12 -5 -14 12.60 1.10 12 -5 -14 16.10 2.20 -12 -5 14 13.50 1.60 -12 5 14 17.20 2.70 -12 5 14 12.80 1.50 -11 -5 14 28.90 1.90 -11 -5 14 28.80 1.70 11 -5 -14 27.00 1.80 11 -5 -14 34.10 1.80 11 -5 -14 31.70 2.60 -11 5 14 34.20 2.10 -11 5 14 34.70 2.50 11 5 -14 28.30 1.60 10 -5 -14 37.90 2.00 10 -5 -14 39.60 3.10 10 -5 -14 38.30 1.80 -10 -5 14 39.00 2.10 -10 -5 14 36.70 2.30 10 5 -14 39.70 2.00 -10 5 14 41.50 2.40 -10 5 14 39.50 2.50 9 -5 -14 -0.10 1.50 -9 -5 14 1.50 0.90 9 -5 -14 0.50 0.60 9 -5 -14 0.40 0.70 -9 -5 14 0.60 1.00 -9 5 14 0.60 1.20 -9 5 14 1.20 1.10 9 5 -14 0.70 0.70 8 -5 -14 23.20 1.50 -8 -5 14 19.80 1.90 8 -5 -14 21.30 2.30 8 -5 -14 18.10 1.60 -8 -5 14 19.10 2.10 8 5 -14 20.10 1.60 -8 5 14 18.60 2.30 -8 5 14 16.30 2.00 8 5 -14 12.90 2.20 -7 -5 14 49.90 2.60 7 -5 -14 49.60 2.20 7 -5 -14 51.19 2.40 -7 -5 14 51.19 2.70 7 5 -14 48.70 4.00 -7 5 14 49.20 2.70 7 5 -14 44.20 2.30 -7 5 14 50.69 2.90 6 -5 -14 60.89 2.60 -6 -5 14 57.09 2.90 6 -5 -14 58.89 2.70 -6 -5 14 61.39 3.00 -6 5 14 60.39 3.00 6 5 -14 61.79 2.60 5 -5 -14 3.10 0.90 -5 -5 14 2.80 1.10 5 -5 -14 2.10 0.80 -5 -5 14 1.60 1.20 -5 5 14 2.70 1.10 5 5 -14 2.50 0.90 -4 -5 14 8.00 1.20 4 -5 -14 8.30 1.10 -4 -5 14 8.00 1.40 4 -5 -14 6.60 1.10 4 5 -14 6.60 1.10 -4 5 14 5.50 1.10 -3 -5 14 -0.80 1.00 3 -5 -14 0.50 1.00 3 -5 -14 0.00 0.80 -3 -5 14 1.40 0.90 -3 5 14 0.50 1.00 3 5 -14 -1.50 0.90 -2 -5 14 13.80 1.60 2 -5 -14 18.40 1.80 -2 -5 14 14.10 1.80 2 -5 -14 17.50 2.00 2 5 -14 17.20 2.60 -2 5 14 16.10 1.90 2 5 -14 16.10 1.80 -1 -5 14 161.28 5.50 1 -5 -14 164.18 5.60 -1 -5 14 154.48 5.70 1 -5 -14 158.78 5.70 -1 5 14 170.58 5.80 1 5 -14 163.98 5.70 1 5 -14 171.28 6.40 0 -5 -14 76.59 3.20 0 -5 -14 76.19 3.40 0 -5 14 73.69 3.40 0 -5 14 72.29 3.10 0 5 14 75.19 3.40 0 5 -14 75.59 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