data_13189sadabs _publ_requested_journal 'J. Am. Chem. Soc.' _publ_section_title ; Dialkyl Ether Formation at High Valent Nickel ; loop_ _publ_author_name _publ_author_address 'Franck Le Vaillant' ; Max-Planck-Institut f\"ur Kohlenforschung Kaiser-Wilhelm-Platz 1 45470 M\"ulheim an der Ruhr Germany ; 'Edward J. Reijerse' ; Max-Planck-Institut f\"ur Chemische Energiekonversion Stiftstrasse 34-36 45470 M\"ulheim an der Ruhr Germany ; 'Markus Leutszch' ; Max-Planck-Institut f\"ur Kohlenforschung Kaiser-Wilhelm-Platz 1 45470 M\"ulheim an der Ruhr Germany ; 'Josep Cornella' ; Max-Planck-Institut f\"ur Kohlenforschung Kaiser-Wilhelm-Platz 1 45470 M\"ulheim an der Ruhr Germany ; _audit_block_code LEF-LA-357-01 _audit_creation_date 2020-07-06 _audit_creation_method ; Olex2 1.3 (compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003) ; _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ; Title ; _chemical_formula_moiety 'C22 H16 F6 N4 Ni O6 S2' _chemical_formula_sum 'C22 H16 F6 N4 Ni O6 S2' _chemical_formula_weight 669.22 _chemical_properties_physical 'Air- and Moisture-sensitive' _chemical_absolute_configuration rmad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 1 2/c 1' _space_group_name_Hall '-C 2yc' _symmetry_cell_setting MONOCLINIC _symmetry_space_group_name_H-M 'C2/c' _symmetry_space_group_name_Hall '-C 2yc' _symmetry_Int_Tables_number 15 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 9.8858(3) _cell_length_b 14.1256(5) _cell_length_c 18.5755(7) _cell_angle_alpha 90 _cell_angle_beta 102.0660(10) _cell_angle_gamma 90 _cell_volume 2536.63(15) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9885 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.7610 _cell_measurement_theta_min 2.2423 _shelx_estimated_absorpt_T_max 0.978 _shelx_estimated_absorpt_T_min 0.960 _exptl_absorpt_coefficient_mu 1.022 _exptl_absorpt_correction_T_max 0.98626 _exptl_absorpt_correction_T_min 0.97866 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details 'SADABS (Bruker AXS, 2012)' _exptl_special_details ; Crystal mounted on a MiTeGen loop using Perfluoropolyether PFO-XR75 ; _exptl_crystal_colour 'light violet' _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.752 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description prism _exptl_crystal_F_000 1352 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: dichlormethane ' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0.00 -1.00 0.00 0.0150 0.00 1.00 0.00 0.0050 -1.00 0.00 1.00 0.0100 1.00 0.00 -1.00 0.0100 0.00 0.00 -1.00 0.0150 0.00 0.00 1.00 0.0100 _exptl_crystal_size_max 0.040 _exptl_crystal_size_mid 0.032 _exptl_crystal_size_min 0.022 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0368 _diffrn_reflns_av_unetI/netI 0.0202 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 39008 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.566 _diffrn_reflns_theta_min 2.242 _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 66.67 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker-AXS Kappa Mach3 APEX-II' _diffrn_measurement_method 'CCD \f- and \w-scans' _diffrn_radiation_type Mo-K\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_source 1\mS _diffrn_radiation_monochromator 'Incoatec Helios mirrors' _diffrn_source_current 0.0 _diffrn_source_power 0.0 _diffrn_source_voltage 0.0 _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3073 _reflns_number_total 3550 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT software (Bruker AXS, 2004)' _computing_data_collection 'APEX3 (Bruker AXS, 2005-2017)' _computing_data_reduction 'SAINT software (Bruker AXS, 2004)' _computing_molecular_graphics 'DIAMOND (Crystal Impact GbR, 1997-2014)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL (G. M. Sheldrick, 2015)' _computing_structure_solution 'SHELXT (G. M. Sheldrick, 2015)' _refine_diff_density_max 0.505 _refine_diff_density_min -0.408 _refine_diff_density_rms 0.062 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 186 _refine_ls_number_reflns 3550 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0351 _refine_ls_R_factor_gt 0.0268 _refine_ls_restrained_S_all 1.046 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0288P)^2^+3.3744P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0626 _refine_ls_wR_factor_ref 0.0660 _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The minimum and maximum estimated transmissions from the multi-scan scaling are 0.9511 and 1.0000 (SADABS). Highest peak ? Deepest hole ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4), C7(H7), C8(H8), C9(H9), C10(H10) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.500000 0.16418(2) 0.750000 0.01005(7) Uani 1 2 d S T P . . S1 S 0.29828(4) 0.00548(2) 0.64063(2) 0.01323(8) Uani 1 1 d . . . . . F1 F 0.07255(11) -0.01113(9) 0.69269(6) 0.0383(3) Uani 1 1 d . . . . . F2 F 0.03888(11) -0.01399(9) 0.57517(6) 0.0401(3) Uani 1 1 d . . . . . F3 F 0.08535(12) 0.11783(9) 0.63233(8) 0.0473(3) Uani 1 1 d . . . . . O1 O 0.35990(11) 0.05258(8) 0.70956(5) 0.0167(2) Uani 1 1 d . . . . . O2 O 0.31141(12) -0.09562(8) 0.64384(6) 0.0222(2) Uani 1 1 d . . . . . O3 O 0.32426(12) 0.05016(8) 0.57534(6) 0.0238(3) Uani 1 1 d . . . . . N1 N 0.36499(12) 0.26129(8) 0.69261(6) 0.0131(2) Uani 1 1 d . . . . . N2 N 0.57131(12) 0.17046(8) 0.65398(6) 0.0129(2) Uani 1 1 d . . . . . C1 C 0.26116(15) 0.30339(11) 0.71647(8) 0.0176(3) Uani 1 1 d . . . . . H1 H 0.250945 0.291655 0.765407 0.021 Uiso 1 1 calc R U . . . C2 C 0.16790(16) 0.36355(11) 0.67236(9) 0.0214(3) Uani 1 1 d . . . . . H2 H 0.094836 0.392268 0.690552 0.026 Uiso 1 1 calc R U . . . C3 C 0.18391(16) 0.38068(11) 0.60126(9) 0.0217(3) Uani 1 1 d . . . . . H3 H 0.121130 0.421067 0.569679 0.026 Uiso 1 1 calc R U . . . C4 C 0.29224(16) 0.33846(11) 0.57651(8) 0.0187(3) Uani 1 1 d . . . . . H4 H 0.305419 0.350331 0.528104 0.022 Uiso 1 1 calc R U . . . C5 C 0.38131(14) 0.27853(10) 0.62339(7) 0.0137(3) Uani 1 1 d . . . . . C6 C 0.49780(14) 0.22774(10) 0.60181(7) 0.0136(3) Uani 1 1 d . . . . . C7 C 0.52848(16) 0.23471(11) 0.53230(8) 0.0182(3) Uani 1 1 d . . . . . H7 H 0.478355 0.277283 0.496939 0.022 Uiso 1 1 calc R U . . . C8 C 0.63245(16) 0.17925(11) 0.51498(8) 0.0206(3) Uani 1 1 d . . . . . H8 H 0.651715 0.181050 0.466990 0.025 Uiso 1 1 calc R U . . . C9 C 0.70810(16) 0.12100(11) 0.56871(8) 0.0198(3) Uani 1 1 d . . . . . H9 H 0.781021 0.082896 0.558496 0.024 Uiso 1 1 calc R U . . . C10 C 0.67513(15) 0.11949(10) 0.63775(8) 0.0166(3) Uani 1 1 d . . . . . H10 H 0.728367 0.080747 0.674977 0.020 Uiso 1 1 calc R U . . . C11 C 0.11411(16) 0.02536(13) 0.63549(9) 0.0243(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.01190(12) 0.01107(12) 0.00710(11) 0.000 0.00180(8) 0.000 S1 0.01558(16) 0.01441(17) 0.00954(15) -0.00009(12) 0.00229(12) -0.00314(12) F1 0.0214(5) 0.0653(8) 0.0315(6) 0.0048(5) 0.0133(4) -0.0018(5) F2 0.0257(5) 0.0598(8) 0.0282(6) 0.0005(5) -0.0093(4) -0.0167(5) F3 0.0299(6) 0.0347(7) 0.0723(9) 0.0022(6) -0.0006(6) 0.0143(5) O1 0.0187(5) 0.0192(5) 0.0111(5) -0.0015(4) 0.0009(4) -0.0060(4) O2 0.0312(6) 0.0161(5) 0.0213(5) -0.0022(4) 0.0103(5) -0.0005(4) O3 0.0310(6) 0.0281(6) 0.0118(5) 0.0031(4) 0.0034(4) -0.0127(5) N1 0.0157(5) 0.0116(5) 0.0115(5) -0.0007(4) 0.0014(4) -0.0004(4) N2 0.0146(5) 0.0138(5) 0.0105(5) -0.0009(4) 0.0027(4) -0.0028(4) C1 0.0191(7) 0.0167(7) 0.0165(7) -0.0031(5) 0.0026(5) 0.0030(6) C2 0.0197(7) 0.0176(7) 0.0246(8) -0.0049(6) -0.0003(6) 0.0050(6) C3 0.0238(8) 0.0127(7) 0.0232(8) 0.0005(6) -0.0074(6) 0.0022(6) C4 0.0235(7) 0.0151(7) 0.0147(6) 0.0018(5) -0.0026(5) -0.0027(6) C5 0.0155(6) 0.0117(6) 0.0123(6) -0.0005(5) -0.0010(5) -0.0038(5) C6 0.0160(6) 0.0132(6) 0.0107(6) 0.0000(5) 0.0009(5) -0.0055(5) C7 0.0225(7) 0.0194(7) 0.0123(6) 0.0016(5) 0.0028(5) -0.0073(6) C8 0.0257(8) 0.0254(8) 0.0130(6) -0.0037(6) 0.0091(6) -0.0118(6) C9 0.0202(7) 0.0219(8) 0.0202(7) -0.0058(6) 0.0111(6) -0.0045(6) C10 0.0172(7) 0.0171(7) 0.0161(7) -0.0015(5) 0.0052(5) -0.0014(5) C11 0.0175(7) 0.0297(8) 0.0232(8) 0.0016(7) -0.0012(6) -0.0009(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 O1 2.1290(10) . ? Ni1 O1 2.1290(10) 2_656 ? Ni1 N1 2.0505(12) 2_656 ? Ni1 N1 2.0505(12) . ? Ni1 N2 2.0522(12) . ? Ni1 N2 2.0523(12) 2_656 ? S1 O1 1.4586(10) . ? S1 O2 1.4342(12) . ? S1 O3 1.4371(11) . ? S1 C11 1.8249(17) . ? F1 C11 1.321(2) . ? F2 C11 1.3301(19) . ? F3 C11 1.335(2) . ? N1 C1 1.3394(19) . ? N1 C5 1.3510(18) . ? N2 C6 1.3519(18) . ? N2 C10 1.3387(19) . ? C1 H1 0.9500 . ? C1 C2 1.388(2) . ? C2 H2 0.9500 . ? C2 C3 1.384(2) . ? C3 H3 0.9500 . ? C3 C4 1.386(2) . ? C4 H4 0.9500 . ? C4 C5 1.389(2) . ? C5 C6 1.481(2) . ? C6 C7 1.3902(19) . ? C7 H7 0.9500 . ? C7 C8 1.383(2) . ? C8 H8 0.9500 . ? C8 C9 1.386(2) . ? C9 H9 0.9500 . ? C9 C10 1.388(2) . ? C10 H10 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Ni1 O1 84.46(6) 2_656 . ? N1 Ni1 O1 90.41(4) . . ? N1 Ni1 O1 90.41(4) 2_656 2_656 ? N1 Ni1 O1 169.58(4) 2_656 . ? N1 Ni1 O1 169.58(4) . 2_656 ? N1 Ni1 N1 96.03(7) 2_656 . ? N1 Ni1 N2 96.80(5) . 2_656 ? N1 Ni1 N2 79.85(5) 2_656 2_656 ? N1 Ni1 N2 96.80(5) 2_656 . ? N1 Ni1 N2 79.85(5) . . ? N2 Ni1 O1 92.39(4) . . ? N2 Ni1 O1 92.39(4) 2_656 2_656 ? N2 Ni1 O1 91.28(4) 2_656 . ? N2 Ni1 O1 91.28(4) . 2_656 ? N2 Ni1 N2 175.04(7) . 2_656 ? O1 S1 C11 101.82(7) . . ? O2 S1 O1 113.58(7) . . ? O2 S1 O3 116.22(7) . . ? O2 S1 C11 103.65(8) . . ? O3 S1 O1 115.15(7) . . ? O3 S1 C11 103.93(7) . . ? S1 O1 Ni1 140.27(6) . . ? C1 N1 Ni1 125.84(10) . . ? C1 N1 C5 119.15(12) . . ? C5 N1 Ni1 114.91(9) . . ? C6 N2 Ni1 114.71(9) . . ? C10 N2 Ni1 126.25(10) . . ? C10 N2 C6 118.88(12) . . ? N1 C1 H1 118.8 . . ? N1 C1 C2 122.46(14) . . ? C2 C1 H1 118.8 . . ? C1 C2 H2 120.8 . . ? C3 C2 C1 118.42(15) . . ? C3 C2 H2 120.8 . . ? C2 C3 H3 120.3 . . ? C2 C3 C4 119.47(14) . . ? C4 C3 H3 120.3 . . ? C3 C4 H4 120.4 . . ? C3 C4 C5 119.14(14) . . ? C5 C4 H4 120.4 . . ? N1 C5 C4 121.35(14) . . ? N1 C5 C6 115.11(12) . . ? C4 C5 C6 123.52(13) . . ? N2 C6 C5 115.32(12) . . ? N2 C6 C7 121.29(14) . . ? C7 C6 C5 123.36(13) . . ? C6 C7 H7 120.2 . . ? C8 C7 C6 119.54(14) . . ? C8 C7 H7 120.2 . . ? C7 C8 H8 120.5 . . ? C7 C8 C9 118.97(14) . . ? C9 C8 H8 120.5 . . ? C8 C9 H9 120.7 . . ? C8 C9 C10 118.62(14) . . ? C10 C9 H9 120.7 . . ? N2 C10 C9 122.62(14) . . ? N2 C10 H10 118.7 . . ? C9 C10 H10 118.7 . . ? F1 C11 S1 111.87(11) . . ? F1 C11 F2 107.54(14) . . ? F1 C11 F3 108.53(15) . . ? F2 C11 S1 110.84(12) . . ? F2 C11 F3 107.17(14) . . ? F3 C11 S1 110.71(12) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ni1 N1 C1 C2 -175.36(11) . . . . ? Ni1 N1 C5 C4 176.20(11) . . . . ? Ni1 N1 C5 C6 -2.63(15) . . . . ? Ni1 N2 C6 C5 1.86(15) . . . . ? Ni1 N2 C6 C7 -176.01(11) . . . . ? Ni1 N2 C10 C9 173.37(11) . . . . ? O1 S1 C11 F1 -59.48(14) . . . . ? O1 S1 C11 F2 -179.49(12) . . . . ? O1 S1 C11 F3 61.71(13) . . . . ? O2 S1 O1 Ni1 128.97(10) . . . . ? O2 S1 C11 F1 58.65(14) . . . . ? O2 S1 C11 F2 -61.37(13) . . . . ? O2 S1 C11 F3 179.84(12) . . . . ? O3 S1 O1 Ni1 -8.56(14) . . . . ? O3 S1 C11 F1 -179.43(12) . . . . ? O3 S1 C11 F2 60.55(14) . . . . ? O3 S1 C11 F3 -58.25(13) . . . . ? N1 C1 C2 C3 -0.3(2) . . . . ? N1 C5 C6 N2 0.51(18) . . . . ? N1 C5 C6 C7 178.33(13) . . . . ? N2 C6 C7 C8 2.7(2) . . . . ? C1 N1 C5 C4 -0.4(2) . . . . ? C1 N1 C5 C6 -179.22(12) . . . . ? C1 C2 C3 C4 -0.6(2) . . . . ? C2 C3 C4 C5 1.0(2) . . . . ? C3 C4 C5 N1 -0.5(2) . . . . ? C3 C4 C5 C6 178.21(13) . . . . ? C4 C5 C6 N2 -178.29(13) . . . . ? C4 C5 C6 C7 -0.5(2) . . . . ? C5 N1 C1 C2 0.8(2) . . . . ? C5 C6 C7 C8 -175.03(13) . . . . ? C6 N2 C10 C9 -1.9(2) . . . . ? C6 C7 C8 C9 -3.0(2) . . . . ? C7 C8 C9 C10 1.0(2) . . . . ? C8 C9 C10 N2 1.5(2) . . . . ? C10 N2 C6 C5 177.62(12) . . . . ? C10 N2 C6 C7 -0.3(2) . . . . ? C11 S1 O1 Ni1 -120.27(11) . . . . ? _shelx_res_file ; TITL 13189sadabs in C2/c #15 13189sadabs.res created by SHELXL-2018/3 at 09:46:40 on 06-Jul-2020 REM reset to C2/c #15 CELL 0.71073 9.8858 14.1256 18.5755 90 102.066 90 ZERR 4 0.0003 0.0005 0.0007 0 0.001 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H F N Ni O S UNIT 88 64 24 16 4 24 8 L.S. 10 PLAN 10 SIZE 0.022 0.032 0.04 TEMP -173 CONF BOND MORE -1 BOND $H fmap 2 acta OMIT -1 1 11 REM REM REM WGHT 0.028800 3.374400 FVAR 0.25387 NI1 5 0.500000 0.164182 0.750000 10.50000 0.01190 0.01107 = 0.00710 0.00000 0.00180 0.00000 S1 7 0.298279 0.005480 0.640626 11.00000 0.01558 0.01441 = 0.00954 -0.00009 0.00229 -0.00314 F1 3 0.072554 -0.011128 0.692688 11.00000 0.02139 0.06533 = 0.03155 0.00481 0.01334 -0.00181 F2 3 0.038884 -0.013991 0.575168 11.00000 0.02573 0.05977 = 0.02823 0.00046 -0.00931 -0.01671 F3 3 0.085346 0.117826 0.632327 11.00000 0.02985 0.03468 = 0.07235 0.00217 -0.00059 0.01430 O1 6 0.359904 0.052580 0.709563 11.00000 0.01871 0.01919 = 0.01108 -0.00147 0.00086 -0.00601 O2 6 0.311409 -0.095624 0.643842 11.00000 0.03116 0.01609 = 0.02135 -0.00215 0.01025 -0.00049 O3 6 0.324257 0.050157 0.575337 11.00000 0.03096 0.02810 = 0.01178 0.00305 0.00345 -0.01271 N1 4 0.364993 0.261290 0.692606 11.00000 0.01575 0.01156 = 0.01148 -0.00074 0.00137 -0.00037 N2 4 0.571309 0.170461 0.653983 11.00000 0.01457 0.01378 = 0.01046 -0.00087 0.00267 -0.00277 C1 1 0.261158 0.303394 0.716467 11.00000 0.01906 0.01669 = 0.01652 -0.00307 0.00264 0.00301 AFIX 43 H1 2 0.250945 0.291655 0.765407 11.00000 -1.20000 AFIX 0 C2 1 0.167899 0.363550 0.672360 11.00000 0.01970 0.01764 = 0.02464 -0.00487 -0.00031 0.00496 AFIX 43 H2 2 0.094836 0.392268 0.690552 11.00000 -1.20000 AFIX 0 C3 1 0.183908 0.380681 0.601260 11.00000 0.02381 0.01273 = 0.02325 0.00049 -0.00742 0.00221 AFIX 43 H3 2 0.121130 0.421067 0.569679 11.00000 -1.20000 AFIX 0 C4 1 0.292236 0.338456 0.576507 11.00000 0.02350 0.01510 = 0.01470 0.00179 -0.00265 -0.00274 AFIX 43 H4 2 0.305419 0.350331 0.528104 11.00000 -1.20000 AFIX 0 C5 1 0.381314 0.278533 0.623389 11.00000 0.01550 0.01166 = 0.01229 -0.00048 -0.00097 -0.00381 C6 1 0.497799 0.227737 0.601809 11.00000 0.01599 0.01324 = 0.01067 -0.00003 0.00092 -0.00554 C7 1 0.528477 0.234709 0.532297 11.00000 0.02247 0.01942 = 0.01231 0.00164 0.00283 -0.00732 AFIX 43 H7 2 0.478355 0.277283 0.496939 11.00000 -1.20000 AFIX 0 C8 1 0.632446 0.179251 0.514978 11.00000 0.02565 0.02540 = 0.01302 -0.00368 0.00911 -0.01178 AFIX 43 H8 2 0.651715 0.181050 0.466990 11.00000 -1.20000 AFIX 0 C9 1 0.708105 0.121002 0.568709 11.00000 0.02018 0.02193 = 0.02023 -0.00582 0.01106 -0.00449 AFIX 43 H9 2 0.781021 0.082896 0.558496 11.00000 -1.20000 AFIX 0 C10 1 0.675134 0.119493 0.637752 11.00000 0.01720 0.01714 = 0.01608 -0.00148 0.00525 -0.00139 AFIX 43 H10 2 0.728367 0.080747 0.674977 11.00000 -1.20000 AFIX 0 C11 1 0.114107 0.025357 0.635490 11.00000 0.01751 0.02971 = 0.02320 0.00161 -0.00121 -0.00090 HKLF 4 REM 13189sadabs in C2/c #15 REM wR2 = 0.0660, GooF = S = 1.046, Restrained GooF = 1.046 for all data REM R1 = 0.0268 for 3073 Fo > 4sig(Fo) and 0.0351 for all 3550 data REM 186 parameters refined using 0 restraints END WGHT 0.0288 3.3744 REM Highest difference peak 0.505, deepest hole -0.408, 1-sigma level 0.062 Q1 1 0.2021 0.0182 0.6345 11.00000 0.05 0.51 Q2 1 0.4383 0.2480 0.6125 11.00000 0.05 0.47 Q3 1 0.3385 0.0272 0.6780 11.00000 0.05 0.40 Q4 1 0.2367 0.3533 0.5919 11.00000 0.05 0.37 Q5 1 0.3049 0.2757 0.7007 11.00000 0.05 0.37 Q6 1 0.6664 0.1451 0.5435 11.00000 0.05 0.36 Q7 1 0.5192 0.2381 0.5687 11.00000 0.05 0.36 Q8 1 0.3077 0.0397 0.6093 11.00000 0.05 0.36 Q9 1 0.0942 0.1025 0.6725 11.00000 0.05 0.35 Q10 1 0.3424 0.3142 0.6008 11.00000 0.05 0.34 ; _shelx_res_checksum 43339 _shelx_hkl_file ; -2 0 2 4.50 1.50 -2 0 2 1.40 1.50 -2 0 2 4.40 1.50 -2 0 2 6.50 1.60 2 0 -2 4.80 2.10 2 0 -2 3.20 1.90 2 0 -2 2.40 2.00 2 0 -2 8.40 2.00 2 0 -2 2.70 1.50 2 0 -2 2.50 1.60 -4 0 4 157.88 6.50 -4 0 4 162.18 6.70 4 0 -4 172.98 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207.38 10.80 -2 6 3 229.38 9.20 2 6 -3 252.47 10.30 -2 6 3 210.68 9.30 -2 6 3 236.78 9.30 -2 -6 3 238.58 9.40 2 -6 -3 288.17 11.50 2 -6 -3 233.18 9.80 2 -6 -3 231.68 8.60 -2 -6 3 239.48 7.30 2 -6 -3 255.97 9.60 -2 -6 3 230.18 9.60 -2 -6 3 237.68 9.40 4 6 -5 96.29 5.90 -4 6 5 97.29 6.30 -4 6 5 108.19 6.60 4 6 -5 107.59 6.90 4 6 -5 98.59 8.00 -4 6 5 105.79 6.30 4 6 -5 101.59 6.80 -4 6 5 102.69 6.70 4 6 -5 104.69 6.50 -4 6 5 99.49 6.90 4 6 -5 111.09 7.40 -4 -6 5 110.79 6.90 4 -6 -5 106.99 6.50 -4 -6 5 103.19 6.50 4 -6 -5 102.79 7.80 4 -6 -5 111.89 7.10 -4 -6 5 104.89 7.00 4 -6 -5 98.29 7.10 4 -6 -5 105.19 6.50 4 -6 -5 111.29 6.90 6 6 -7 28.00 3.30 6 6 -7 28.60 4.60 6 6 -7 20.10 4.40 -6 6 7 20.30 4.80 6 6 -7 26.60 5.50 -6 6 7 30.90 4.70 6 6 -7 19.40 4.30 -6 6 7 13.80 3.60 -6 6 7 27.60 3.60 6 6 -7 16.30 5.40 6 -6 -7 13.90 5.50 6 -6 -7 22.50 4.20 6 -6 -7 23.60 4.80 -6 -6 7 28.70 2.50 6 -6 -7 14.80 4.40 6 -6 -7 25.50 5.50 -6 -6 7 27.00 4.60 6 -6 -7 19.90 4.50 -6 -6 7 24.60 4.40 8 6 -9 14.50 5.00 -8 6 9 14.10 5.80 8 6 -9 21.40 7.20 8 -6 -9 5.10 6.00 8 -6 -9 16.00 6.10 8 -6 -9 19.70 6.50 8 -6 -9 9.40 5.10 10 6 -11 48.00 9.60 10 6 -11 43.00 7.80 10 6 -11 58.09 10.00 -10 6 11 39.90 8.60 10 -6 -11 48.70 8.90 10 -6 -11 53.69 8.80 10 -6 -11 43.80 8.90 12 6 -13 64.59 12.20 -12 6 13 81.79 12.30 12 6 -13 77.59 10.60 12 -6 -13 72.99 12.20 12 -6 -13 70.79 10.50 12 -6 -13 58.69 10.70 11 7 -10 239.38 15.20 -11 7 10 237.48 15.60 11 7 -10 241.28 17.40 11 -7 -10 227.18 15.60 11 -7 -10 225.08 15.90 11 -7 -10 223.08 16.50 9 7 -8 139.09 10.80 9 7 -8 109.19 11.00 -9 7 8 130.69 12.10 9 -7 -8 126.39 11.10 9 -7 -8 100.29 10.60 9 -7 -8 127.79 10.70 7 7 -6 61.29 4.90 7 7 -6 51.19 6.40 -7 7 6 58.39 5.40 -7 7 6 54.79 5.80 7 7 -6 55.69 6.50 7 7 -6 51.99 7.50 -7 7 6 63.49 6.50 7 7 -6 55.19 5.90 -7 7 6 46.20 7.00 7 -7 -6 57.49 7.20 7 -7 -6 52.69 6.50 7 -7 -6 56.79 5.90 7 -7 -6 64.49 7.30 7 -7 -6 62.09 7.00 -7 -7 6 60.29 6.50 7 -7 -6 63.39 8.20 -5 7 4 26.90 4.20 5 7 -4 29.40 4.20 5 7 -4 20.60 4.30 -5 7 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17.60 3.60 -1 -7 0 21.10 3.80 1 -7 0 22.40 3.30 1 -7 0 18.40 3.70 1 -7 0 20.70 3.10 -1 7 2 574.44 17.00 1 7 -2 566.84 15.70 1 7 -2 569.14 17.50 -1 7 2 578.04 17.60 1 7 -2 593.24 18.60 -1 7 2 589.84 18.10 1 7 -2 574.24 17.50 -1 7 2 582.74 17.70 -1 7 2 572.54 17.80 1 7 -2 577.84 18.30 -1 -7 2 553.34 17.40 1 -7 -2 560.24 17.40 -1 -7 2 579.94 18.20 1 -7 -2 579.24 18.40 1 -7 -2 556.44 17.70 -1 -7 2 575.44 16.30 1 -7 -2 560.64 17.30 1 -7 -2 560.34 16.10 3 7 -4 363.56 13.80 -3 7 4 358.46 13.10 3 7 -4 376.46 12.50 -3 7 4 359.66 12.90 -3 7 4 352.26 12.70 -3 7 4 368.76 13.60 3 7 -4 360.66 12.70 -3 7 4 368.96 13.30 3 7 -4 374.96 13.10 3 7 -4 376.16 14.90 3 7 -4 349.77 13.00 3 -7 -4 367.96 12.70 3 -7 -4 346.57 13.20 3 -7 -4 358.56 13.00 -3 -7 4 356.86 13.70 3 -7 -4 357.36 13.60 -3 -7 4 381.66 13.20 3 -7 -4 375.46 14.00 -3 -7 4 381.86 13.20 -3 -7 4 360.56 10.20 3 -7 -4 372.46 12.40 5 7 -6 32.60 5.20 -5 7 6 22.50 3.90 -5 7 6 21.90 4.40 -5 7 6 21.30 3.80 5 7 -6 10.60 5.00 5 7 -6 20.80 3.90 -5 7 6 18.40 5.00 5 7 -6 20.30 4.50 -5 7 6 25.90 4.30 5 7 -6 21.10 4.60 5 7 -6 24.70 3.60 5 -7 -6 31.40 5.00 -5 -7 6 21.60 4.10 5 -7 -6 24.60 4.30 -5 -7 6 25.00 2.30 -5 -7 6 17.20 4.00 5 -7 -6 19.40 4.60 5 -7 -6 17.40 4.10 5 -7 -6 24.60 5.60 5 -7 -6 23.70 4.30 -5 -7 6 21.20 4.00 -7 7 8 37.50 5.20 7 7 -8 27.60 5.40 -7 7 8 50.19 5.00 7 7 -8 46.20 8.50 7 7 -8 36.00 6.00 7 7 -8 42.20 4.10 7 7 -8 51.69 7.40 -7 7 8 55.79 7.90 7 -7 -8 40.50 6.70 7 -7 -8 35.80 6.40 7 -7 -8 41.40 5.60 7 -7 -8 42.00 7.50 -7 -7 8 49.80 6.60 7 -7 -8 32.00 6.10 -9 7 10 4.30 5.30 9 7 -10 2.20 6.50 9 7 -10 6.50 5.10 9 7 -10 -0.40 5.90 9 -7 -10 1.30 5.20 9 -7 -10 0.60 5.40 9 -7 -10 -0.10 6.00 9 -7 -10 4.20 6.10 11 7 -12 98.19 12.90 -11 7 12 129.29 13.90 11 7 -12 116.89 11.60 11 -7 -12 119.29 12.30 11 -7 -12 102.99 13.00 11 -7 -12 141.19 14.00 12 8 -11 176.98 15.00 12 8 -11 223.38 18.90 -12 8 11 193.68 17.10 12 -8 -11 203.88 16.80 12 -8 -11 189.98 17.70 12 -8 -11 227.68 17.10 -10 8 9 293.17 17.40 10 8 -9 307.77 18.30 10 8 -9 298.57 16.20 10 -8 -9 285.77 17.40 10 -8 -9 273.87 16.40 10 -8 -9 263.77 15.90 -8 8 7 155.18 11.40 8 8 -7 142.99 12.30 8 8 -7 173.28 11.30 -8 8 7 159.18 8.80 8 -8 -7 166.98 11.40 8 -8 -7 175.28 11.40 8 -8 -7 177.78 12.80 8 -8 -7 168.58 11.70 6 8 -5 168.98 10.50 -6 8 5 157.48 9.00 -6 8 5 160.88 9.50 6 8 -5 169.98 9.20 -6 8 5 164.58 8.90 6 8 -5 154.18 10.40 6 8 -5 169.48 8.30 6 8 -5 163.98 9.90 -6 8 5 159.88 10.30 6 -8 -5 166.88 10.60 6 -8 -5 161.38 9.60 6 -8 -5 154.08 10.30 6 -8 -5 169.18 9.20 6 -8 -5 168.18 10.40 -6 -8 5 150.08 9.50 -6 -8 5 184.28 9.50 6 -8 -5 151.18 9.30 6 -8 -5 187.58 10.20 4 8 -3 151.88 8.00 -4 8 3 136.19 8.60 4 8 -3 129.69 8.10 -4 8 3 159.48 8.10 4 8 -3 142.39 8.70 -4 8 3 152.68 8.60 -4 8 3 120.79 8.00 4 8 -3 148.39 8.90 4 8 -3 142.19 7.80 -4 8 3 143.59 7.90 4 8 -3 140.79 10.40 4 -8 -3 150.18 8.40 -4 -8 3 142.89 8.00 4 -8 -3 141.39 8.70 4 -8 -3 140.99 8.60 -4 -8 3 157.18 8.80 4 -8 -3 143.79 8.00 4 -8 -3 147.29 8.80 4 -8 -3 145.79 8.00 -4 -8 3 160.28 8.30 -2 8 1 211.88 9.40 2 8 -1 214.88 9.70 -2 8 1 221.18 9.40 2 8 -1 219.38 9.60 -2 8 1 220.78 10.00 2 8 -1 218.88 10.30 2 8 -1 218.18 7.10 -2 8 1 202.58 9.20 2 8 -1 211.18 9.00 -2 8 1 217.18 9.70 2 -8 -1 199.08 9.00 2 -8 -1 208.98 9.90 2 -8 -1 211.68 10.20 -2 -8 1 219.68 10.30 -2 -8 1 231.18 9.70 2 -8 -1 201.08 9.10 -2 -8 1 213.98 9.50 0 8 1 1094.79 30.60 0 8 -1 1097.19 29.00 0 8 -1 1096.49 30.50 0 8 -1 1084.99 30.30 0 8 -1 1075.19 31.20 0 8 -1 1116.49 30.60 0 8 -1 1091.29 30.80 0 8 1 1084.89 30.40 0 8 1 1119.99 30.80 0 8 1 1106.99 29.10 0 8 1 1085.39 31.00 0 -8 -1 1160.78 30.80 0 -8 -1 1101.09 28.50 0 -8 -1 1067.09 29.70 0 -8 1 1112.69 31.50 0 -8 -1 1103.59 30.60 0 -8 1 1115.19 29.00 0 -8 1 1120.19 30.60 0 -8 -1 1110.39 31.50 0 -8 1 1119.19 29.10 0 -8 1 1089.99 30.60 2 8 -3 1544.85 41.50 -2 8 3 1534.65 42.10 2 8 -3 1581.94 41.30 -2 8 3 1589.94 41.60 2 8 -3 1516.35 40.50 -2 8 3 1544.05 41.50 -2 8 3 1569.64 41.50 -2 8 3 1579.34 41.70 2 8 -3 1558.24 42.70 2 8 -3 1587.44 38.90 2 8 -3 1597.04 43.40 2 8 -3 1537.95 41.60 2 -8 -3 1579.94 41.80 2 -8 -3 1557.94 40.20 2 -8 -3 1521.05 41.80 2 -8 -3 1590.74 41.70 2 -8 -3 1553.24 42.40 -2 -8 3 1586.94 41.90 -2 -8 3 1629.84 42.70 -4 8 5 120.39 7.90 -4 8 5 127.49 7.70 4 8 -5 139.79 8.10 -4 8 5 124.79 8.20 4 8 -5 119.39 8.10 4 8 -5 160.58 9.40 -4 8 5 127.39 8.30 4 8 -5 133.99 10.30 -4 8 5 134.89 7.70 4 8 -5 126.49 7.40 4 8 -5 128.39 8.10 4 -8 -5 147.89 9.00 4 -8 -5 125.39 8.00 -4 -8 5 132.59 4.80 -4 -8 5 129.89 8.20 -4 -8 5 137.99 8.20 4 -8 -5 120.59 9.60 4 -8 -5 112.39 7.40 4 -8 -5 135.99 7.60 -4 -8 5 130.69 7.90 4 -8 -5 124.99 7.80 6 8 -7 0.10 3.40 6 8 -7 -1.40 3.00 -6 8 7 2.10 3.50 -6 8 7 -3.00 3.00 6 8 -7 7.70 4.40 6 8 -7 -1.50 5.10 -6 8 7 -0.90 3.10 6 8 -7 1.00 4.00 -6 8 7 2.70 4.60 6 8 -7 -0.20 3.90 6 -8 -7 7.80 4.80 6 -8 -7 -1.10 3.50 6 -8 -7 1.40 4.80 6 -8 -7 5.50 4.00 -6 -8 7 1.90 3.60 6 -8 -7 3.10 4.00 6 -8 -7 2.10 4.40 -8 8 9 -4.20 5.10 8 8 -9 -2.90 5.10 8 8 -9 12.40 7.00 8 8 -9 6.30 4.90 8 -8 -9 3.80 4.90 8 -8 -9 2.80 5.20 8 -8 -9 5.40 5.90 8 -8 -9 7.10 4.90 10 8 -11 164.68 13.40 -10 8 11 148.29 13.60 10 8 -11 142.79 13.80 10 -8 -11 128.89 12.60 10 -8 -11 122.39 12.60 10 -8 -11 147.09 13.00 11 9 -10 57.19 9.20 -11 9 10 53.49 10.80 11 9 -10 78.09 12.10 11 -9 -10 74.59 10.50 11 -9 -10 56.79 10.50 11 -9 -10 69.09 10.60 9 9 -8 44.30 7.90 -9 9 8 30.40 8.10 9 9 -8 36.40 8.50 9 -9 -8 30.80 7.20 9 -9 -8 38.10 7.50 9 -9 -8 33.20 7.70 7 9 -6 246.48 10.80 -7 9 6 233.58 11.30 7 9 -6 274.37 13.40 -7 9 6 230.48 13.30 7 9 -6 250.67 13.90 7 -9 -6 249.08 13.70 7 -9 -6 243.18 13.20 7 -9 -6 240.98 14.20 7 -9 -6 248.08 13.10 7 -9 -6 241.68 13.20 -5 9 4 1000.60 29.70 5 9 -4 1036.30 30.10 5 9 -4 1035.80 31.30 -5 9 4 1013.60 31.20 -5 9 4 1030.90 29.80 5 9 -4 994.60 30.70 -5 9 4 1060.19 30.60 5 9 -4 1038.50 29.20 5 9 -4 988.70 30.10 5 -9 -4 1004.20 30.50 5 -9 -4 984.30 29.90 5 -9 -4 991.90 29.80 -5 -9 4 1078.99 30.40 -5 -9 4 1022.10 30.80 5 -9 -4 1010.50 30.70 5 -9 -4 1002.50 29.90 5 -9 -4 1003.90 30.60 -3 9 2 239.68 10.60 3 9 -2 239.98 7.30 -3 9 2 230.38 10.80 3 9 -2 237.08 10.60 3 9 -2 248.48 10.80 3 9 -2 234.98 11.00 -3 9 2 251.67 11.00 -3 9 2 230.08 11.00 3 9 -2 252.17 10.70 -3 9 2 252.27 10.60 3 9 -2 233.18 11.50 3 -9 -2 240.38 11.40 -3 -9 2 240.18 10.70 3 -9 -2 225.58 10.70 3 -9 -2 242.68 10.30 3 -9 -2 230.48 10.50 3 -9 -2 239.08 10.70 3 -9 -2 239.58 11.40 -3 -9 2 215.58 10.40 -3 -9 2 259.17 11.70 -1 9 0 1066.99 28.60 1 9 0 1010.90 30.10 -1 9 0 1080.29 29.70 1 9 0 1021.80 29.50 1 9 0 1047.90 27.30 -1 9 0 1046.10 30.30 -1 9 0 1046.60 29.30 1 9 0 1026.40 29.60 1 9 0 1042.00 29.60 -1 9 0 1046.40 29.70 1 -9 0 1070.59 29.60 1 -9 0 1032.00 30.40 -1 -9 0 1025.50 28.70 1 -9 0 1035.60 29.90 1 -9 0 1008.50 27.90 1 -9 0 1016.00 28.20 -1 -9 0 1016.40 29.60 -1 -9 0 1016.20 29.40 -1 -9 0 1034.50 27.40 -1 -9 0 1029.90 30.50 1 9 -2 281.17 12.10 1 9 -2 284.97 9.60 -1 9 2 278.97 12.10 -1 9 2 273.37 11.50 1 9 -2 255.07 12.20 -1 9 2 302.77 12.10 -1 9 2 285.87 10.90 1 9 -2 269.47 11.50 -1 9 2 278.07 11.80 1 9 -2 288.77 11.80 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452.35 13.00 -2 4 0 457.65 13.20 2 4 0 440.06 12.90 2 4 0 440.26 12.90 2 4 0 460.75 13.50 2 4 0 446.46 13.50 -2 4 0 448.76 11.50 -2 4 0 436.26 13.20 -2 4 0 420.16 12.70 -2 4 0 425.16 13.10 2 -4 0 434.66 12.90 2 -4 0 442.76 12.80 -2 -4 0 457.95 13.50 2 -4 0 431.86 12.90 2 -4 0 454.25 12.60 2 -4 0 442.06 13.00 -2 -4 0 449.95 12.70 -2 -4 0 465.35 13.10 0 4 2 11.40 2.20 0 4 -2 11.90 2.50 0 4 2 8.50 2.70 0 4 2 8.50 2.60 0 4 2 11.70 2.50 0 4 -2 12.90 2.50 0 4 -2 9.00 2.90 0 4 -2 8.40 2.60 0 4 2 9.50 2.30 0 -4 2 9.20 2.10 0 -4 -2 11.90 1.60 0 -4 -2 11.00 2.60 0 -4 -2 11.00 2.40 0 -4 -2 12.00 2.30 0 -4 2 10.30 2.80 0 -4 -2 4.30 2.40 0 -4 2 10.50 2.60 0 -4 2 6.70 2.00 0 -4 2 10.40 2.20 -2 4 4 16.00 2.90 2 4 -4 12.60 3.00 2 4 -4 14.50 2.50 2 4 -4 13.90 2.60 -2 4 4 20.90 3.00 2 4 -4 8.00 2.50 -2 4 4 19.10 3.20 -2 4 4 13.00 2.80 2 4 -4 19.40 3.70 -2 4 4 21.90 3.40 2 4 -4 21.50 3.00 2 -4 -4 15.90 3.60 2 -4 -4 19.60 3.00 -2 -4 4 14.10 2.50 2 -4 -4 14.50 3.00 2 -4 -4 15.20 2.60 -2 -4 4 12.70 3.00 -2 -4 4 15.10 1.80 -2 -4 4 16.80 3.10 2 -4 -4 16.10 2.00 2 -4 -4 20.80 2.70 2 -4 -4 15.00 2.90 4 4 -6 358.46 13.00 4 4 -6 365.36 12.50 -4 4 6 347.27 12.90 4 4 -6 370.96 12.50 4 4 -6 345.37 10.60 4 4 -6 350.96 14.60 -4 4 6 347.17 12.00 -4 4 6 348.27 12.30 4 4 -6 350.86 12.20 -4 4 6 368.06 12.60 -4 4 6 340.67 11.00 -4 -4 6 374.06 10.20 4 -4 -6 359.86 12.30 -4 -4 6 361.96 12.80 -4 -4 6 382.56 11.60 4 -4 -6 366.56 12.70 4 -4 -6 367.76 12.50 4 -4 -6 335.57 11.40 4 -4 -6 363.56 14.30 4 -4 -6 341.27 12.60 -4 -4 6 353.86 12.30 -4 -4 6 360.36 12.40 6 4 -8 211.78 9.70 -6 4 8 185.78 9.50 -6 4 8 184.98 7.10 6 4 -8 179.08 11.80 6 4 -8 196.58 9.90 -6 4 8 189.98 9.30 -6 4 8 168.48 9.20 6 4 -8 202.98 9.90 6 4 -8 201.38 10.10 -6 4 8 187.28 10.10 6 4 -8 193.08 6.30 6 -4 -8 188.08 10.00 6 -4 -8 203.38 10.80 6 -4 -8 197.98 9.80 -6 -4 8 206.18 9.40 -6 -4 8 181.88 9.40 -6 -4 8 218.68 9.40 6 -4 -8 179.18 11.50 6 -4 -8 190.28 8.10 6 -4 -8 179.58 9.30 6 -4 -8 190.48 9.40 -6 -4 8 188.98 8.70 8 4 -10 285.47 16.40 8 4 -10 283.57 13.80 8 4 -10 304.77 14.30 8 4 -10 302.67 13.80 -8 4 10 258.07 15.20 -8 4 10 290.37 14.80 8 -4 -10 270.67 13.60 8 -4 -10 297.37 13.30 -8 -4 10 296.77 12.30 8 -4 -10 270.17 11.50 8 -4 -10 279.27 14.80 8 -4 -10 289.37 16.50 -8 -4 10 278.67 13.10 8 -4 -10 259.37 13.70 10 4 -12 202.78 13.30 -10 4 12 190.18 13.90 10 4 -12 190.28 15.80 10 -4 -12 172.08 13.10 10 -4 -12 168.68 13.20 10 -4 -12 178.88 13.90 12 4 -14 10.40 8.10 -12 4 14 0.60 7.70 12 4 -14 -3.40 6.80 12 -4 -14 -0.30 7.30 12 -4 -14 1.40 6.80 12 -4 -14 -3.30 6.70 11 5 -9 62.59 10.50 11 5 -9 37.20 7.40 -11 5 9 37.00 8.00 11 -5 -9 39.70 7.60 11 -5 -9 49.70 9.30 11 -5 -9 50.89 9.70 -9 5 7 10.70 5.50 9 5 -7 2.60 5.50 9 5 -7 6.40 4.60 9 -5 -7 11.30 5.00 9 -5 -7 15.10 5.90 9 -5 -7 3.70 5.60 -7 5 5 179.58 8.90 -7 5 5 173.98 7.60 7 5 -5 170.88 9.30 -7 5 5 170.08 8.40 -7 5 5 172.68 10.40 7 5 -5 190.88 8.90 7 5 -5 180.38 9.40 7 5 -5 171.58 10.40 7 -5 -5 177.58 9.60 7 -5 -5 172.18 9.00 7 -5 -5 173.98 9.90 -7 -5 5 166.78 6.70 -7 -5 5 180.18 9.10 7 -5 -5 174.08 10.10 7 -5 -5 175.08 10.10 7 -5 -5 172.58 8.50 -7 -5 5 182.58 8.80 5 5 -3 606.34 17.80 -5 5 3 546.65 17.30 -5 5 3 606.84 17.10 5 5 -3 564.04 18.90 5 5 -3 594.64 16.70 -5 5 3 588.14 18.90 -5 5 3 592.44 17.90 5 5 -3 586.44 18.40 5 -5 -3 616.44 18.20 5 -5 -3 575.14 18.00 -5 -5 3 604.04 18.20 5 -5 -3 596.24 18.00 5 -5 -3 583.54 19.30 5 -5 -3 582.04 17.50 5 -5 -3 604.64 18.30 5 -5 -3 585.14 18.40 3 5 -1 1014.90 28.10 3 5 -1 984.30 27.10 -3 5 1 982.40 26.30 3 5 -1 1004.60 27.20 3 5 -1 970.30 26.30 -3 5 1 989.00 26.30 -3 5 1 939.71 26.60 -3 5 1 995.30 27.10 3 5 -1 1001.90 26.20 -3 -5 1 996.30 26.50 -3 -5 1 1012.00 26.10 3 -5 -1 943.21 26.60 -3 -5 1 999.70 27.00 3 -5 -1 998.80 26.70 3 -5 -1 995.30 26.60 3 -5 -1 1014.00 26.70 3 -5 -1 1006.40 26.40 -1 5 -1 60.39 4.50 1 5 1 75.29 5.20 -1 5 -1 72.19 4.30 -1 5 -1 61.99 4.60 1 5 1 58.39 4.50 1 5 1 58.39 4.60 -1 5 -1 62.79 4.40 -1 5 -1 65.79 4.50 1 5 1 70.59 3.50 1 5 1 67.09 5.10 1 -5 1 66.39 4.50 1 -5 1 70.09 4.40 -1 -5 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25.10 5 5 -7 838.42 24.40 -5 5 7 783.32 23.60 5 5 -7 852.91 24.60 -5 5 7 806.62 24.30 -5 5 7 792.72 23.90 5 5 -7 802.32 24.90 5 5 -7 829.92 24.30 5 -5 -7 796.82 24.10 5 -5 -7 799.32 24.60 -5 -5 7 854.51 21.30 -5 -5 7 845.02 24.00 5 -5 -7 871.81 26.60 5 -5 -7 819.62 23.90 5 -5 -7 815.52 24.60 -5 -5 7 833.52 24.80 -5 -5 7 820.72 24.10 5 -5 -7 814.32 21.70 7 5 -9 478.25 20.60 7 5 -9 507.55 18.40 7 5 -9 486.85 17.60 7 5 -9 503.55 18.70 -7 5 9 478.85 17.50 7 5 -9 483.45 18.10 -7 5 9 481.45 19.00 -7 5 9 480.35 17.40 -7 5 9 468.75 14.40 -7 -5 9 488.75 16.00 7 -5 -9 503.95 19.10 7 -5 -9 500.55 17.70 7 -5 -9 510.85 20.80 7 -5 -9 491.55 18.40 -7 -5 9 508.25 17.60 -7 -5 9 503.95 14.40 7 -5 -9 487.75 14.90 -7 -5 9 464.35 17.60 7 -5 -9 480.75 17.80 9 5 -11 357.36 19.50 -9 5 11 367.06 18.30 9 5 -11 397.56 17.50 9 5 -11 382.86 18.10 9 -5 -11 348.97 17.30 9 -5 -11 384.16 18.40 9 -5 -11 395.06 17.80 11 5 -13 13.20 6.70 -11 5 13 15.60 7.60 11 5 -13 16.90 7.20 11 -5 -13 22.20 7.50 11 -5 -13 12.20 7.90 11 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355.56 16.20 5 7 -7 367.86 14.80 -5 7 7 350.86 14.00 -5 7 7 352.66 13.60 5 7 -7 350.96 14.00 -5 7 7 346.27 14.60 -5 7 7 351.56 12.50 5 7 -7 353.86 14.00 -5 7 7 359.36 13.50 5 7 -7 351.56 13.80 5 -7 -7 363.26 13.80 5 -7 -7 354.26 13.70 -5 -7 7 358.96 13.70 -5 -7 7 363.16 13.80 5 -7 -7 351.56 15.40 -5 -7 7 364.56 14.40 5 -7 -7 331.77 13.00 -5 -7 7 352.66 10.20 5 -7 -7 342.17 14.30 5 -7 -7 345.17 14.20 -7 7 9 1.90 3.00 7 7 -9 4.20 2.60 7 7 -9 8.10 4.70 7 7 -9 -4.70 4.80 -7 7 9 -3.50 3.30 7 7 -9 10.60 5.30 -7 7 9 4.10 4.90 7 7 -9 5.90 4.20 7 -7 -9 -5.30 5.50 7 -7 -9 11.40 5.00 7 -7 -9 -3.10 5.10 7 -7 -9 4.40 4.50 -7 -7 9 0.50 3.80 7 -7 -9 2.20 3.70 -9 7 11 62.19 9.40 9 7 -11 56.09 9.10 9 7 -11 52.19 10.40 9 7 -11 48.10 7.50 9 -7 -11 50.29 8.80 9 -7 -11 42.90 7.70 9 -7 -11 41.20 8.70 9 -7 -11 40.50 7.60 -11 7 13 92.49 12.20 11 7 -13 82.99 12.10 11 7 -13 78.09 10.40 11 -7 -13 98.49 11.60 11 -7 -13 75.39 11.10 11 -7 -13 92.09 12.20 12 8 -10 17.50 7.60 12 8 -10 58.69 11.70 -12 8 10 41.90 10.30 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24.90 7.10 -9 9 11 16.70 7.10 9 9 -11 25.60 7.90 9 9 -11 19.80 8.80 9 -9 -11 17.40 7.30 9 -9 -11 19.90 6.40 9 -9 -11 15.90 6.90 9 -9 -11 9.90 7.40 11 9 -13 -5.70 7.60 -11 9 13 -8.60 7.80 11 9 -13 5.20 7.20 11 -9 -13 -5.20 7.00 11 -9 -13 -5.80 6.90 11 -9 -13 -5.50 7.40 10 10 -8 2.90 7.30 -10 10 8 -5.70 6.60 10 10 -8 2.30 6.30 10 -10 -8 -2.70 6.10 10 -10 -8 0.60 6.10 -8 10 6 37.20 8.00 8 10 -6 36.40 7.40 8 10 -6 31.20 7.60 8 10 -6 43.90 7.20 -8 10 6 35.40 5.80 8 -10 -6 36.90 6.80 8 -10 -6 35.40 6.80 8 -10 -6 46.90 7.70 8 -10 -6 36.90 7.40 8 -10 -6 34.70 7.30 6 10 -4 -5.90 3.30 -6 10 4 4.50 4.30 -6 10 4 5.80 4.90 6 10 -4 1.70 4.60 6 10 -4 0.00 4.50 6 10 -4 -1.80 4.20 -6 -10 4 -0.70 3.80 6 -10 -4 -7.60 4.10 6 -10 -4 6.40 4.10 6 -10 -4 3.50 5.00 6 -10 -4 0.20 4.50 6 -10 -4 1.50 4.40 6 -10 -4 -4.10 3.80 4 10 -2 115.39 8.80 4 10 -2 115.79 8.40 -4 10 2 119.69 8.70 4 10 -2 115.39 9.30 -4 10 2 122.89 8.80 -4 10 2 120.09 8.00 4 10 -2 119.89 8.10 4 10 -2 122.09 8.70 -4 10 2 114.09 8.70 4 -10 -2 119.99 8.80 -4 -10 2 122.49 9.00 4 -10 -2 122.99 8.20 4 -10 -2 133.59 9.80 4 -10 -2 117.39 8.20 4 -10 -2 118.69 8.70 4 -10 -2 107.39 8.00 -4 -10 2 120.49 8.30 2 10 0 382.26 14.80 -2 10 0 353.46 14.10 -2 10 0 377.56 14.10 2 10 0 356.86 14.70 -2 10 0 363.06 14.00 -2 10 0 374.76 14.70 2 10 0 377.16 11.50 2 10 0 371.76 14.70 -2 10 0 393.96 14.00 2 10 0 364.16 14.00 -2 -10 0 375.56 12.10 2 -10 0 362.06 14.70 2 -10 0 356.06 14.00 -2 -10 0 356.36 14.20 -2 -10 0 346.07 13.80 2 -10 0 355.26 13.10 2 -10 0 403.06 15.40 -2 -10 0 375.26 15.20 -2 -10 0 363.06 14.30 2 -10 0 350.46 13.10 0 10 -2 33.70 5.60 0 10 -2 27.30 4.90 0 10 -2 24.10 4.30 0 10 -2 28.80 3.80 0 10 -2 21.70 4.80 0 10 2 35.70 5.30 0 10 2 30.80 5.50 0 10 -2 28.10 4.80 0 10 2 21.60 3.80 0 10 2 28.30 5.20 0 10 2 30.30 5.10 0 -10 2 31.70 4.20 0 -10 -2 23.90 4.50 0 -10 2 26.30 4.70 0 -10 -2 33.60 5.60 0 -10 2 28.60 3.70 0 -10 2 26.60 4.80 0 -10 2 19.30 4.80 0 -10 -2 28.10 4.90 0 -10 -2 26.90 3.50 0 -10 -2 34.70 5.20 2 10 -4 6.60 3.90 -2 10 4 9.20 3.90 -2 10 4 10.30 4.00 -2 10 4 8.10 4.40 2 10 -4 6.00 4.30 2 10 -4 8.30 3.30 -2 10 4 4.70 3.70 2 10 -4 15.10 4.50 -2 10 4 11.20 4.50 2 10 -4 8.70 2.40 2 10 -4 6.90 3.10 2 10 -4 5.30 4.40 -2 -10 4 7.20 3.90 2 -10 -4 14.50 4.70 2 -10 -4 5.00 3.70 -2 -10 4 3.40 2.90 2 -10 -4 9.10 3.20 -2 -10 4 0.20 3.20 -2 -10 4 7.00 3.80 2 -10 -4 10.20 4.70 2 -10 -4 11.80 4.10 -4 10 6 22.50 4.90 -4 10 6 25.80 5.20 -4 10 6 23.20 5.60 4 10 -6 33.00 6.30 -4 10 6 17.60 4.80 4 10 -6 19.50 4.70 4 10 -6 19.90 4.70 4 10 -6 22.40 6.60 4 10 -6 17.30 4.30 4 10 -6 21.40 5.30 4 -10 -6 14.30 4.50 -4 -10 6 17.50 2.70 4 -10 -6 17.80 4.30 -4 -10 6 15.70 4.70 4 -10 -6 14.40 4.50 -4 -10 6 17.80 5.20 4 -10 -6 18.80 4.90 4 -10 -6 13.80 5.80 4 -10 -6 17.50 5.20 -6 10 8 58.49 8.40 -6 10 8 53.59 6.40 -6 10 8 66.19 7.20 6 10 -8 50.99 7.50 6 10 -8 57.19 8.00 6 10 -8 42.10 6.90 6 10 -8 62.29 10.10 6 10 -8 66.49 6.50 6 -10 -8 54.19 8.40 6 -10 -8 53.89 7.50 -6 -10 8 54.79 7.10 6 -10 -8 61.59 8.10 6 -10 -8 51.59 6.70 6 -10 -8 50.59 6.90 8 10 -10 210.28 16.20 -8 10 10 203.48 14.90 8 10 -10 214.78 13.90 8 10 -10 178.38 13.40 8 -10 -10 195.88 14.30 8 -10 -10 213.98 13.80 8 -10 -10 202.18 15.10 8 -10 -10 178.98 13.20 10 10 -12 79.49 11.90 -10 10 12 41.90 9.50 10 10 -12 61.99 10.00 10 -10 -12 82.49 11.40 10 -10 -12 47.80 10.00 10 -10 -12 66.99 11.80 10 -10 -12 49.70 9.50 -11 11 9 12.20 8.20 11 11 -9 37.90 10.30 11 11 -9 24.80 8.10 11 -11 -9 34.40 8.60 11 -11 -9 16.70 8.10 11 -11 -9 33.60 10.20 9 11 -7 2.50 6.00 -9 11 7 7.30 7.10 9 11 -7 4.60 7.20 9 -11 -7 15.30 6.50 9 -11 -7 3.80 6.10 9 -11 -7 16.10 6.30 9 -11 -7 1.40 6.10 -7 11 5 69.89 7.40 7 11 -5 61.39 8.60 7 11 -5 63.99 8.20 -7 11 5 74.89 9.60 7 11 -5 69.89 7.20 7 -11 -5 75.19 7.90 7 -11 -5 71.59 8.50 7 -11 -5 73.99 9.10 7 -11 -5 70.89 8.70 7 -11 -5 70.99 8.40 -5 11 3 29.70 6.00 5 11 -3 19.20 4.90 5 11 -3 24.50 6.10 -5 11 3 14.20 4.60 5 11 -3 15.90 5.70 5 11 -3 15.00 5.60 -5 11 3 22.10 5.80 -5 -11 3 20.10 5.10 5 -11 -3 23.90 5.50 5 -11 -3 6.40 5.40 5 -11 -3 18.60 5.70 5 -11 -3 11.50 5.30 5 -11 -3 28.70 5.40 -3 11 1 9.80 4.70 3 11 -1 21.20 5.30 3 11 -1 25.00 4.90 -3 11 1 12.20 4.80 -3 11 1 20.20 4.80 -3 11 1 18.10 4.60 3 11 -1 23.60 2.60 3 11 -1 12.10 4.60 3 11 -1 26.40 5.50 -3 -11 1 22.50 5.20 3 -11 -1 21.60 5.00 3 -11 -1 21.90 4.50 3 -11 -1 16.40 4.70 3 -11 -1 24.60 5.60 3 -11 -1 25.20 4.90 -3 -11 1 19.40 4.40 -3 -11 1 21.40 4.70 3 -11 -1 26.00 5.60 -3 -11 1 24.00 3.90 -1 11 -1 368.86 15.40 1 11 1 342.87 14.30 -1 11 -1 359.96 14.20 1 11 1 367.26 15.00 -1 11 -1 375.36 14.60 -1 11 -1 331.47 13.20 -1 11 -1 353.46 14.80 1 11 1 335.77 14.80 1 11 1 349.27 15.00 1 11 1 362.86 12.30 1 -11 1 356.46 12.80 -1 -11 -1 338.97 15.30 1 -11 1 371.56 13.20 -1 -11 -1 369.36 14.10 -1 -11 -1 351.26 14.20 -1 -11 -1 375.76 15.00 1 -11 1 352.66 14.50 -1 -11 -1 367.56 12.20 1 -11 1 349.96 15.10 1 -11 1 350.06 15.50 1 11 -3 39.20 6.50 1 11 -3 46.50 5.90 -1 11 3 54.29 6.80 1 11 -3 32.30 5.60 1 11 -3 33.90 4.20 -1 11 3 39.60 6.10 1 11 -3 38.00 5.20 -1 11 3 42.90 6.10 -1 11 3 36.10 5.10 -1 11 3 35.40 5.60 1 11 -3 35.60 6.00 -1 -11 3 39.50 5.80 1 -11 -3 36.20 5.80 1 -11 -3 43.90 6.20 -1 -11 3 38.40 4.70 -1 -11 3 44.50 4.60 1 -11 -3 42.50 5.90 1 -11 -3 36.40 5.60 -1 -11 3 42.30 5.80 -1 -11 3 30.80 5.50 3 11 -5 276.27 13.30 3 11 -5 260.17 15.10 -3 11 5 250.57 12.80 3 11 -5 263.17 9.20 3 11 -5 247.78 11.10 -3 11 5 268.37 13.00 3 11 -5 247.68 13.70 3 11 -5 270.27 12.70 3 11 -5 272.17 12.60 -3 11 5 270.77 12.40 -3 11 5 265.67 13.20 -3 11 5 262.57 13.10 3 -11 -5 265.77 12.30 -3 -11 5 253.27 13.00 3 -11 -5 255.27 13.40 -3 -11 5 266.17 13.20 -3 -11 5 275.97 12.90 3 -11 -5 274.67 11.30 3 -11 -5 259.87 14.50 3 -11 -5 269.97 12.80 3 -11 -5 281.07 13.90 5 11 -7 214.18 13.20 -5 11 7 184.68 11.30 5 11 -7 156.98 14.40 -5 11 7 182.18 11.40 5 11 -7 186.18 12.00 5 11 -7 198.38 10.80 -5 11 7 187.88 12.00 5 11 -7 196.88 11.30 5 -11 -7 193.38 13.70 5 -11 -7 191.58 11.50 5 -11 -7 181.38 12.40 -5 -11 7 188.58 12.00 5 -11 -7 194.58 10.80 5 -11 -7 176.98 11.70 -7 11 9 57.89 9.10 7 11 -9 50.19 6.20 7 11 -9 58.79 8.30 -7 11 9 61.89 7.20 7 11 -9 64.49 10.30 7 11 -9 59.79 8.50 7 -11 -9 59.99 8.80 7 -11 -9 33.90 8.20 7 -11 -9 47.20 8.20 9 11 -11 65.69 10.50 -9 11 11 55.09 10.40 9 11 -11 49.20 8.80 9 -11 -11 42.60 8.80 9 -11 -11 60.69 10.00 9 -11 -11 74.09 10.40 9 -11 -11 49.60 10.70 10 12 -8 120.39 13.80 -10 12 8 112.99 14.10 10 12 -8 140.89 13.70 10 -12 -8 112.39 12.30 10 -12 -8 104.39 12.50 10 -12 -8 119.69 11.60 8 12 -6 230.88 15.10 8 12 -6 245.08 15.20 -8 12 6 223.18 12.90 -8 12 6 218.38 15.40 8 -12 -6 213.08 14.30 8 -12 -6 237.18 14.60 8 -12 -6 235.68 13.30 8 -12 -6 227.68 14.00 8 -12 -6 223.68 15.30 -6 12 4 99.49 10.40 -6 12 4 111.49 9.60 6 12 -4 124.59 11.00 6 12 -4 122.99 9.70 6 12 -4 121.19 10.90 6 -12 -4 100.99 9.50 6 -12 -4 117.69 9.10 6 -12 -4 100.19 9.90 6 -12 -4 128.89 10.00 6 -12 -4 104.79 10.10 4 12 -2 141.69 11.00 -4 12 2 103.89 9.50 4 12 -2 104.69 9.00 4 12 -2 114.89 9.70 -4 12 2 123.69 10.20 -4 12 2 118.19 9.00 4 -12 -2 107.29 8.90 -4 -12 2 101.49 8.80 4 -12 -2 97.09 8.90 4 -12 -2 99.29 8.90 4 -12 -2 117.39 9.10 4 -12 -2 97.29 9.20 -4 -12 2 121.09 10.10 -2 12 0 162.18 10.90 2 12 0 174.98 11.20 2 12 0 156.48 10.10 2 12 0 165.78 7.60 2 12 0 161.28 11.10 -2 12 0 145.09 9.90 -2 12 0 171.78 10.90 -2 12 0 152.68 9.40 2 12 0 159.58 10.40 -2 -12 0 167.18 10.00 2 -12 0 149.39 9.80 -2 -12 0 162.28 8.20 -2 -12 0 169.48 10.30 2 -12 0 139.89 10.80 -2 -12 0 167.08 11.20 2 -12 0 162.88 9.50 -2 -12 0 148.99 10.50 2 -12 0 179.48 11.50 2 -12 0 160.58 10.10 0 12 2 167.18 10.50 0 12 2 172.38 11.00 0 12 -2 179.68 10.80 0 12 -2 158.98 10.70 0 12 2 174.08 10.80 0 12 -2 155.28 11.10 0 12 2 153.18 8.60 0 12 -2 155.98 8.50 0 -12 2 171.28 10.30 0 -12 -2 162.28 9.90 0 -12 2 169.88 8.90 0 -12 -2 166.38 10.70 0 -12 -2 176.18 11.50 0 -12 -2 164.88 8.00 0 -12 2 171.58 11.30 0 -12 2 168.78 11.30 0 -12 2 154.18 8.20 0 -12 -2 159.48 9.80 -2 12 4 528.85 20.00 2 12 -4 541.55 21.90 2 12 -4 580.34 20.30 -2 12 4 504.15 19.10 -2 12 4 549.74 21.00 2 12 -4 562.74 20.50 -2 12 4 574.84 20.90 2 12 -4 564.94 20.30 2 12 -4 539.35 16.80 -2 12 4 577.74 20.50 2 12 -4 596.64 21.80 2 -12 -4 544.75 20.70 -2 -12 4 558.74 20.40 -2 -12 4 547.95 21.20 -2 -12 4 527.65 18.30 2 -12 -4 540.65 21.40 2 -12 -4 580.54 20.50 -2 -12 4 599.64 21.00 -2 -12 4 526.35 18.00 2 -12 -4 555.44 18.00 2 -12 -4 552.64 20.70 4 12 -6 473.65 17.50 4 12 -6 477.85 22.10 -4 12 6 486.95 19.10 4 12 -6 459.45 19.10 -4 12 6 477.55 18.80 -4 12 6 471.05 19.40 4 12 -6 469.15 18.30 4 12 -6 481.05 20.10 4 -12 -6 429.96 17.90 4 -12 -6 472.75 20.00 -4 -12 6 478.45 19.90 4 -12 -6 496.65 19.90 4 -12 -6 493.75 17.30 4 -12 -6 482.15 18.80 6 12 -8 132.29 9.90 6 12 -8 139.79 10.70 6 12 -8 130.79 13.50 6 12 -8 145.99 12.10 -6 12 8 124.09 10.00 -6 12 8 126.19 11.80 6 -12 -8 157.28 12.90 6 -12 -8 118.69 11.70 6 -12 -8 126.59 10.10 6 -12 -8 120.59 10.30 -8 12 10 -5.20 6.40 8 12 -10 1.80 6.20 8 12 -10 2.50 6.20 8 -12 -10 -4.10 6.50 8 -12 -10 2.40 6.60 8 -12 -10 10.40 7.10 8 -12 -10 3.30 6.40 9 13 -7 20.20 8.40 9 13 -7 16.60 7.80 -9 13 7 20.90 7.70 9 -13 -7 20.40 7.50 9 -13 -7 28.10 8.40 9 -13 -7 18.90 6.80 9 -13 -7 29.10 8.00 -7 13 5 157.18 12.10 7 13 -5 147.69 12.50 7 13 -5 178.08 13.80 -7 13 5 126.99 12.10 7 13 -5 165.88 11.20 7 -13 -5 151.08 10.80 7 -13 -5 166.48 12.00 7 -13 -5 180.98 13.80 7 -13 -5 156.88 13.00 7 -13 -5 147.59 11.90 5 13 -3 34.00 6.90 -5 13 3 32.10 7.20 5 13 -3 37.10 6.40 -5 13 3 33.00 7.00 5 13 -3 31.70 6.70 5 -13 -3 30.60 5.70 5 -13 -3 32.50 6.30 5 -13 -3 26.90 6.10 5 -13 -3 38.20 7.80 3 13 -1 14.60 5.80 3 13 -1 20.00 6.00 3 13 -1 11.00 5.60 -3 13 1 15.20 5.30 -3 13 1 20.90 5.10 -3 13 1 16.20 4.80 3 -13 -1 23.70 5.80 3 -13 -1 4.70 5.30 3 -13 -1 15.40 5.20 -3 -13 1 17.00 4.90 -3 -13 1 15.10 4.00 3 -13 -1 23.20 5.60 -3 -13 1 7.50 5.10 3 -13 -1 7.10 4.70 -1 13 -1 243.08 11.40 -1 13 -1 223.58 13.20 1 13 1 246.38 13.70 -1 13 -1 246.68 13.60 1 13 1 254.17 13.40 1 13 1 234.98 12.70 -1 13 -1 238.08 12.60 1 13 1 235.98 10.40 1 13 1 233.38 13.50 1 -13 1 227.88 13.70 1 -13 1 240.68 13.60 1 -13 1 224.88 12.30 1 -13 1 234.78 11.60 -1 -13 -1 257.67 14.20 -1 -13 -1 250.47 13.40 -1 -13 -1 206.38 12.10 -1 -13 -1 226.18 10.20 -1 -13 -1 240.58 12.10 1 -13 1 238.38 11.10 -1 13 3 44.20 6.00 -1 13 3 37.10 6.60 1 13 -3 42.30 5.10 1 13 -3 38.20 7.10 -1 13 3 34.90 6.10 1 13 -3 37.60 6.80 -1 13 3 31.40 6.50 -1 13 3 29.70 6.20 1 13 -3 39.50 5.80 1 13 -3 50.19 7.70 1 -13 -3 44.70 6.60 1 -13 -3 34.90 7.00 -1 -13 3 37.70 5.50 1 -13 -3 35.10 6.40 -1 -13 3 42.50 5.10 -1 -13 3 38.70 6.80 1 -13 -3 45.00 7.10 -1 -13 3 46.30 7.40 -1 -13 3 58.09 7.30 1 -13 -3 32.70 5.00 3 13 -5 138.39 10.50 3 13 -5 118.99 11.10 -3 13 5 137.29 11.30 3 13 -5 145.49 11.50 -3 13 5 131.99 10.30 3 13 -5 117.99 11.80 -3 13 5 130.59 10.30 3 -13 -5 131.89 12.40 -3 -13 5 137.09 11.20 3 -13 -5 108.49 8.60 3 -13 -5 143.89 10.60 -3 -13 5 124.69 8.80 3 -13 -5 138.39 11.50 3 -13 -5 148.29 10.90 -3 -13 5 132.39 8.90 5 13 -7 78.19 8.40 5 13 -7 66.59 11.20 -5 13 7 108.19 11.00 5 13 -7 87.09 9.70 5 13 -7 86.79 8.70 5 13 -7 57.59 10.10 -5 13 7 52.99 7.80 5 -13 -7 80.39 8.10 5 -13 -7 80.39 9.70 5 -13 -7 73.49 9.50 5 -13 -7 97.59 10.00 -7 13 9 72.19 8.60 7 13 -9 65.69 7.70 7 13 -9 93.09 10.70 7 13 -9 81.89 9.80 -7 13 9 70.39 9.90 7 -13 -9 98.29 11.00 7 -13 -9 83.99 11.00 7 -13 -9 80.29 9.10 7 -13 -9 79.39 10.90 -9 13 11 3.50 7.90 9 13 -11 7.90 7.40 9 13 -11 1.80 7.60 9 -13 -11 6.80 7.70 9 -13 -11 25.10 8.20 9 -13 -11 9.10 7.90 9 -13 -11 10.00 7.10 -8 14 6 63.89 10.70 -8 14 6 52.19 8.30 8 14 -6 58.69 10.30 8 14 -6 56.69 9.70 8 -14 -6 52.29 9.20 8 -14 -6 45.90 9.10 8 -14 -6 48.00 9.30 -6 14 4 1.30 5.20 6 14 -4 15.60 6.00 -6 14 4 10.50 5.80 6 14 -4 9.90 6.30 6 14 -4 18.60 7.30 6 -14 -4 17.80 6.20 6 -14 -4 3.90 5.90 6 -14 -4 1.40 6.40 -4 14 2 40.50 7.70 -4 14 2 44.50 7.30 4 14 -2 47.30 7.50 4 14 -2 45.00 7.90 -4 -14 2 47.40 7.10 -4 -14 2 55.49 6.20 4 -14 -2 49.20 8.30 4 -14 -2 50.69 7.20 4 -14 -2 43.10 7.00 -2 14 0 66.79 7.30 -2 14 0 65.39 8.80 2 14 0 78.79 9.00 2 14 0 69.59 8.90 2 14 0 80.99 9.20 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4 -3 82.89 5.00 2 4 3 88.59 4.60 2 4 3 81.59 3.40 2 4 3 86.49 4.30 2 4 3 87.19 5.60 2 -4 3 80.29 4.80 2 -4 3 79.89 4.30 2 -4 3 77.29 5.40 -2 -4 -3 75.39 4.90 -2 -4 -3 72.19 5.70 -2 -4 -3 82.09 4.40 2 -4 3 92.99 5.30 2 -4 3 95.89 4.70 2 -4 3 80.69 3.10 2 -4 3 82.69 4.50 2 -4 3 83.69 4.30 0 4 -5 22.40 3.10 0 4 5 18.50 3.10 0 4 5 16.00 3.00 0 4 -5 21.20 2.90 0 4 -5 17.10 3.70 0 4 -5 23.90 2.90 0 4 -5 22.10 1.70 0 4 5 16.70 3.10 0 4 -5 25.30 3.40 0 4 5 20.50 3.00 0 4 5 19.90 3.00 0 -4 -5 15.70 3.20 0 -4 5 23.90 3.30 0 -4 5 13.30 2.70 0 -4 5 11.60 2.40 0 -4 5 23.40 3.00 0 -4 5 20.60 3.00 0 -4 -5 23.00 3.00 0 -4 -5 16.20 2.70 0 -4 -5 19.50 3.20 -2 4 7 35.00 4.20 2 4 -7 35.90 4.20 -2 4 7 33.70 3.90 2 4 -7 10.40 6.20 -2 4 7 40.90 4.00 2 4 -7 44.10 4.40 2 4 -7 32.50 3.40 2 4 -7 35.20 3.40 -2 4 7 31.30 4.40 2 4 -7 34.60 3.80 -2 4 7 28.60 3.90 2 -4 -7 43.60 4.00 2 -4 -7 36.80 6.10 2 -4 -7 38.80 4.00 2 -4 -7 41.10 4.50 2 -4 -7 30.40 4.10 -2 -4 7 41.90 3.40 2 -4 -7 36.70 3.50 -2 -4 7 25.30 3.80 -2 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16.60 -8 -4 13 378.76 13.30 -8 -4 13 382.06 16.00 8 -4 -13 361.56 17.30 8 -4 -13 374.46 17.10 8 -4 -13 385.66 15.20 10 4 -15 66.79 9.30 10 4 -15 60.09 10.30 -10 4 15 60.59 9.70 10 4 -15 43.80 8.50 10 -4 -15 68.39 9.80 10 -4 -15 57.79 9.10 10 -4 -15 78.69 11.20 13 5 -8 17.60 10.00 -13 5 8 24.80 8.50 13 5 -8 35.00 7.70 13 -5 -8 23.60 8.90 13 -5 -8 25.70 8.60 13 -5 -8 30.90 8.10 -11 5 6 -8.90 4.70 11 5 -6 8.60 6.70 11 5 -6 -2.40 4.30 11 -5 -6 8.40 5.90 11 -5 -6 1.40 5.80 11 -5 -6 -1.90 4.60 9 5 -4 44.10 5.90 9 5 -4 57.59 8.70 -9 5 4 47.30 7.20 9 -5 -4 45.30 5.80 9 -5 -4 49.40 7.60 9 -5 -4 59.69 7.50 -7 5 2 291.87 10.60 -7 5 2 286.67 12.70 -7 5 2 276.37 10.20 7 5 -2 273.47 11.00 -7 5 2 283.67 10.30 7 5 -2 280.97 11.30 7 5 -2 279.87 13.80 7 5 -2 292.07 10.70 7 5 -2 264.37 11.10 7 -5 -2 283.97 11.10 7 -5 -2 285.77 10.90 -7 -5 2 282.87 8.10 7 -5 -2 257.47 12.20 7 -5 -2 279.07 11.80 -7 -5 2 289.77 10.90 -7 -5 2 270.57 10.50 7 -5 -2 254.47 10.60 7 -5 -2 266.27 10.00 -5 5 0 40.50 3.60 -5 5 0 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198.18 8.90 -1 -5 -4 194.38 8.20 1 -5 4 195.38 8.00 1 5 -6 137.79 6.80 -1 5 6 133.79 6.80 1 5 -6 138.49 6.60 -1 5 6 141.29 7.40 -1 5 6 133.19 7.10 1 5 -6 144.99 11.30 -1 5 6 141.29 7.30 1 5 -6 130.09 7.00 1 5 -6 138.09 5.20 1 5 -6 143.29 6.90 -1 5 6 128.89 7.00 -1 -5 6 132.99 7.30 1 -5 -6 131.09 7.30 -1 -5 6 138.29 6.80 1 -5 -6 156.88 8.80 -1 -5 6 128.89 6.20 1 -5 -6 128.99 6.90 -1 -5 6 133.99 7.20 -3 5 8 805.62 24.80 3 5 -8 814.82 22.90 3 5 -8 843.92 26.50 3 5 -8 862.51 24.90 -3 5 8 816.92 24.00 -3 5 8 799.82 24.00 3 5 -8 822.32 23.80 3 5 -8 822.32 22.50 -3 5 8 828.32 24.30 3 5 -8 863.41 24.20 -3 5 8 799.72 23.10 -3 -5 8 834.22 24.00 3 -5 -8 827.22 24.10 3 -5 -8 818.42 24.50 3 -5 -8 796.52 24.10 3 -5 -8 811.82 26.00 3 -5 -8 817.62 22.90 3 -5 -8 816.82 23.00 -3 -5 8 833.22 24.50 -3 -5 8 801.52 21.80 -3 -5 8 838.62 24.40 -5 5 10 3.30 3.40 5 5 -10 0.60 2.20 5 5 -10 4.70 3.60 5 5 -10 1.90 3.20 -5 5 10 0.70 3.80 5 5 -10 0.80 3.30 -5 5 10 -1.10 2.80 5 5 -10 -1.30 3.50 5 5 -10 -1.60 4.50 -5 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-15 11.40 8.70 10 -6 -15 9.40 7.00 10 -6 -15 17.90 8.50 -11 7 6 44.00 8.80 11 7 -6 55.49 10.40 11 7 -6 62.99 8.40 11 -7 -6 38.50 9.30 11 -7 -6 61.39 8.00 11 -7 -6 56.99 8.80 -9 7 4 22.70 6.20 9 7 -4 15.60 5.00 9 7 -4 10.40 6.50 9 -7 -4 17.80 5.30 9 -7 -4 13.50 5.70 9 -7 -4 13.70 5.90 9 -7 -4 15.60 5.50 -7 7 2 -1.90 3.60 7 7 -2 8.90 3.80 -7 7 2 6.50 3.00 7 7 -2 -2.30 3.20 -7 7 2 4.80 3.20 -7 7 2 7.00 3.60 7 7 -2 4.20 4.70 7 7 -2 7.80 3.10 -7 -7 2 4.70 3.10 7 -7 -2 4.90 2.80 7 -7 -2 2.30 4.40 7 -7 -2 -5.70 4.00 7 -7 -2 4.00 3.30 7 -7 -2 3.70 3.60 -7 -7 2 10.00 3.50 7 -7 -2 11.60 4.00 -5 7 0 408.66 14.40 5 7 0 463.95 16.70 5 7 0 434.56 14.80 5 7 0 430.86 15.40 5 7 0 448.86 14.50 5 7 0 430.86 15.00 -5 7 0 428.26 15.80 -5 7 0 420.86 14.80 -5 7 0 419.76 14.10 -5 -7 0 437.26 15.10 5 -7 0 425.66 15.30 -5 -7 0 450.85 14.70 5 -7 0 430.76 14.10 5 -7 0 440.76 15.30 5 -7 0 425.66 14.90 5 -7 0 425.66 13.70 5 -7 0 424.26 14.90 3 7 2 1.90 1.10 3 7 2 0.90 2.90 -3 7 -2 1.40 2.70 -3 7 -2 -1.10 2.20 3 7 2 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16.60 2.40 -3 5 -4 17.30 2.90 3 5 4 23.30 2.20 -3 5 -4 21.30 3.10 3 5 4 20.90 3.20 -3 5 -4 9.30 3.10 3 -5 4 17.10 3.10 3 -5 4 18.30 2.90 3 -5 4 15.50 2.50 3 -5 4 14.50 3.30 3 -5 4 20.10 2.70 -3 -5 -4 16.60 3.10 3 -5 4 23.80 4.00 3 -5 4 23.50 3.10 -3 -5 -4 19.00 4.20 -3 -5 -4 17.70 2.80 3 -5 4 17.10 2.00 -1 5 -6 113.19 5.80 -1 5 -6 108.29 6.40 1 5 6 111.09 6.60 1 5 6 112.89 6.40 1 5 6 110.29 7.30 -1 5 -6 128.49 7.90 -1 5 -6 110.99 6.30 1 5 6 100.99 6.20 1 -5 6 96.19 6.20 1 -5 6 118.89 6.40 1 -5 6 112.49 6.30 -1 -5 -6 110.29 5.90 -1 -5 -6 117.29 6.60 -1 -5 -6 115.09 7.50 -1 -5 -6 116.89 5.90 1 -5 6 115.09 6.00 1 5 -8 501.95 16.60 -1 5 8 499.45 16.40 1 5 -8 498.65 15.60 1 5 -8 521.75 16.00 -1 5 8 501.55 16.30 1 5 -8 479.25 13.80 1 5 -8 605.74 19.70 -1 5 8 515.05 16.90 1 5 -8 494.25 15.40 -1 5 8 501.65 16.10 -1 -5 8 494.75 15.80 1 -5 -8 499.25 16.50 -1 -5 8 486.15 16.10 1 -5 -8 488.05 15.80 1 -5 -8 509.85 17.80 -1 -5 8 481.85 14.90 1 -5 -8 489.05 16.00 -1 -5 8 470.65 16.10 -3 5 10 113.89 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13 8 98.49 9.20 -1 13 8 92.49 10.20 1 13 -8 76.49 8.90 -1 -13 8 88.59 9.50 -1 -13 8 97.09 8.00 1 -13 -8 82.49 9.90 1 -13 -8 84.49 10.40 -1 -13 8 75.59 8.10 -1 -13 8 88.99 9.10 3 13 -10 148.39 11.30 -3 13 10 154.78 12.00 3 13 -10 148.79 14.30 -3 13 10 149.59 12.20 -3 -13 10 149.39 11.00 3 -13 -10 140.39 13.50 3 -13 -10 172.58 11.70 -5 13 12 -1.50 5.50 -5 13 12 1.60 5.70 5 13 -12 -1.40 7.50 5 13 -12 5.90 5.00 5 -13 -12 2.20 5.60 5 -13 -12 1.90 7.30 -7 13 14 73.79 12.00 7 13 -14 79.09 13.40 7 -13 -14 85.89 13.00 7 -13 -14 80.39 10.80 8 14 -1 7.10 6.80 -8 14 1 -0.90 6.40 -8 14 1 6.50 6.50 8 -14 -1 -0.70 6.20 8 -14 -1 11.40 7.00 -8 -14 1 18.80 7.50 8 -14 -1 3.90 6.70 -6 14 -1 11.10 6.20 -6 14 -1 3.80 5.50 6 14 1 7.40 5.70 6 14 1 17.30 7.10 6 -14 1 4.30 6.10 6 -14 1 16.40 6.70 6 -14 1 0.40 5.90 -6 -14 -1 13.30 6.20 4 14 3 114.79 11.30 4 14 3 124.49 11.20 -4 14 -3 117.19 10.60 -4 14 -3 118.39 11.50 4 -14 3 129.89 11.20 4 -14 3 133.69 11.10 -4 -14 -3 105.89 10.80 4 -14 3 136.39 12.10 2 14 5 318.37 16.40 -2 14 -5 293.17 14.60 2 14 5 311.67 16.50 -2 14 -5 295.67 14.10 -2 14 -5 297.07 15.20 2 -14 5 306.57 16.50 -2 -14 -5 303.37 16.00 2 -14 5 271.77 14.10 0 14 7 95.59 10.20 0 14 7 126.49 9.70 0 14 -7 114.29 8.90 0 14 -7 119.79 10.50 0 14 7 122.19 11.10 0 14 -7 122.89 11.90 0 14 7 141.69 12.10 0 -14 7 126.29 11.90 0 -14 7 131.29 11.60 0 -14 -7 142.29 12.60 0 -14 -7 110.39 11.30 0 -14 7 148.19 10.30 2 14 -9 46.90 9.00 -2 14 9 55.09 9.00 -2 14 9 46.00 7.70 2 14 -9 51.69 7.90 2 -14 -9 39.80 9.40 -2 -14 9 52.49 7.40 -2 -14 9 43.10 5.90 -4 14 11 111.09 11.50 4 14 -11 113.29 10.60 4 14 -11 147.69 15.20 -4 14 11 115.19 11.30 4 -14 -11 122.99 11.20 4 -14 -11 116.59 13.30 -4 -14 11 115.09 10.70 6 14 -13 217.98 19.20 6 14 -13 199.18 13.30 -6 14 13 207.48 16.80 -6 14 13 173.08 13.90 6 -14 -13 190.38 14.20 6 -14 -13 194.48 17.40 -7 15 0 108.29 12.00 7 15 0 139.79 13.50 -7 15 0 110.89 11.60 7 15 0 122.09 11.40 7 -15 0 137.89 13.00 -7 -15 0 132.59 13.50 7 -15 0 145.69 13.90 7 -15 0 102.99 11.50 -5 15 -2 86.99 10.40 -5 15 -2 94.99 10.50 5 15 2 116.99 12.10 5 15 2 104.99 11.00 5 -15 2 112.29 11.00 -5 -15 -2 104.59 11.40 5 -15 2 88.19 10.90 5 -15 2 99.79 10.60 -3 15 -4 15.50 5.40 3 15 4 20.60 7.30 -3 15 -4 21.20 6.60 3 15 4 19.80 7.30 3 -15 4 15.00 5.90 3 -15 4 13.50 6.00 -3 -15 -4 15.80 6.40 3 -15 4 8.70 6.50 -1 15 -6 36.70 6.50 -1 15 -6 37.60 8.20 1 15 6 35.30 8.10 1 15 6 45.90 8.60 -1 15 -6 33.40 7.40 1 -15 6 41.40 8.50 -1 -15 -6 27.20 7.30 1 -15 6 38.00 7.00 -1 15 8 155.98 11.70 1 15 -8 181.78 10.30 1 15 -8 181.58 14.70 1 15 -8 175.48 13.20 -1 15 8 162.98 13.80 1 -15 -8 150.18 14.20 -1 -15 8 170.28 11.70 -1 -15 8 186.88 14.80 3 15 -10 75.09 11.40 -3 15 10 76.29 9.70 3 15 -10 85.99 9.90 -3 15 10 87.49 10.80 3 -15 -10 79.49 11.80 -3 -15 10 71.29 8.70 3 -15 -10 72.79 9.50 -5 15 12 19.50 7.30 5 15 -12 2.10 8.40 5 15 -12 9.20 5.90 -5 15 12 1.80 6.70 -5 -15 12 3.40 6.10 5 -15 -12 0.40 6.70 5 -15 -12 15.00 8.50 -6 16 -1 77.29 10.50 6 16 1 75.29 10.90 -6 16 -1 93.59 11.50 6 16 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7.70 6 -4 -14 47.70 8.80 6 -4 -14 90.69 10.40 6 -4 -14 68.49 7.20 -6 -4 14 66.69 5.90 6 -4 -14 65.79 7.30 8 4 -16 1.50 4.90 -8 4 16 4.30 6.60 8 4 -16 -2.10 6.30 8 4 -16 -4.00 5.40 8 -4 -16 -1.00 5.00 8 -4 -16 0.00 6.40 8 -4 -16 -3.50 5.70 -8 -4 16 -8.90 3.30 -8 -4 16 10.00 6.10 8 -4 -16 -3.90 6.40 8 -4 -16 4.70 5.10 -10 4 18 -8.50 8.10 10 4 -18 -2.50 6.40 10 4 -18 -1.20 7.20 10 4 -18 -0.30 7.10 10 -4 -18 8.20 7.00 10 -4 -18 0.90 7.50 10 -4 -18 -1.80 6.40 13 5 -5 152.98 16.60 13 5 -5 140.59 11.50 -13 5 5 155.58 13.90 13 -5 -5 119.49 14.30 13 -5 -5 136.69 14.20 13 -5 -5 130.79 11.40 -11 5 3 70.69 8.80 11 5 -3 82.19 10.80 11 5 -3 64.19 7.30 11 -5 -3 75.89 10.60 11 -5 -3 85.79 7.90 9 5 -1 100.69 7.50 -9 5 1 107.69 7.00 9 5 -1 93.39 10.50 -9 5 1 98.29 7.10 -9 5 1 98.99 9.00 9 -5 -1 111.29 7.70 9 -5 -1 107.89 10.30 9 -5 -1 113.69 9.20 9 -5 -1 112.89 9.80 9 -5 -1 100.39 6.50 -7 5 -1 1.00 1.90 -7 5 -1 1.40 2.60 -7 5 -1 5.00 2.50 -7 5 -1 5.20 2.20 7 5 1 7.30 2.80 7 5 1 3.60 2.70 7 5 1 4.20 2.30 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12 -6 -4 331.87 16.50 10 6 -2 224.18 15.10 -10 6 2 237.18 13.70 10 6 -2 212.88 11.50 10 -6 -2 234.08 13.90 10 -6 -2 204.08 11.60 10 -6 -2 183.88 13.20 10 -6 -2 246.58 13.60 8 6 0 3.60 3.30 -8 6 0 8.00 4.60 8 6 0 4.40 2.80 -8 6 0 8.00 3.00 -8 6 0 7.80 3.80 8 6 0 2.50 4.70 8 -6 0 2.80 4.70 8 -6 0 6.40 5.40 8 -6 0 5.90 3.40 8 -6 0 8.30 3.00 -8 -6 0 8.50 3.00 8 -6 0 12.10 4.30 6 6 2 34.40 4.20 -6 6 -2 40.20 4.70 -6 6 -2 36.60 3.90 6 6 2 39.80 6.50 -6 6 -2 34.70 3.40 6 6 2 41.50 4.00 6 6 2 27.30 3.80 -6 6 -2 33.30 3.50 -6 6 -2 38.70 5.60 6 6 2 31.30 3.90 -6 -6 -2 38.70 2.20 6 -6 2 38.90 4.30 -6 -6 -2 33.80 3.80 6 -6 2 38.10 3.70 6 -6 2 31.20 5.30 6 -6 2 38.70 5.40 6 -6 2 35.50 3.90 6 -6 2 35.90 4.10 -6 -6 -2 29.50 3.80 6 -6 2 37.10 4.10 4 6 4 193.68 6.20 4 6 4 193.78 8.00 -4 6 -4 190.68 8.90 -4 6 -4 185.38 8.00 -4 6 -4 187.58 7.40 4 6 4 198.78 8.20 4 6 4 191.78 8.20 4 6 4 169.88 9.60 -4 6 -4 189.18 8.10 4 6 4 195.28 8.50 -4 -6 -4 199.08 8.00 4 -6 4 189.38 8.10 4 -6 4 188.88 9.50 4 -6 4 200.38 9.70 4 -6 4 197.28 8.70 4 -6 4 197.78 8.30 4 -6 4 193.98 7.60 4 -6 4 191.18 7.80 -4 -6 -4 201.98 8.60 4 -6 4 189.78 6.80 2 6 6 1116.19 30.00 -2 6 -6 1059.39 29.00 -2 6 -6 1090.69 30.50 -2 6 -6 1089.59 30.10 2 6 6 1102.29 29.50 2 6 6 1083.59 29.70 2 6 6 1119.39 28.00 -2 6 -6 1082.49 29.90 -2 -6 -6 1123.09 30.20 2 -6 6 1116.89 28.70 2 -6 6 1084.49 29.30 -2 -6 -6 1114.39 29.50 2 -6 6 1082.19 29.80 2 -6 6 1080.29 30.20 -2 -6 -6 1083.79 31.30 2 -6 6 1098.59 29.90 2 -6 6 1025.70 29.40 0 6 -8 371.96 12.90 0 6 8 383.86 13.10 0 6 -8 375.56 9.90 0 6 8 373.36 13.80 0 6 -8 355.46 15.00 0 6 -8 373.26 13.70 0 6 8 371.36 13.50 0 6 -8 359.36 13.00 0 6 8 374.46 13.60 0 6 -8 369.36 12.40 0 -6 -8 374.96 12.80 0 -6 8 362.96 13.40 0 -6 8 380.16 13.50 0 -6 -8 361.06 13.50 0 -6 -8 363.96 14.30 0 -6 8 386.16 13.00 0 -6 8 373.86 12.90 0 -6 8 357.36 12.60 0 -6 -8 372.96 13.10 2 6 -10 280.17 10.90 2 6 -10 268.27 14.30 2 6 -10 301.67 11.50 2 6 -10 278.57 11.70 2 6 -10 270.47 12.40 -2 6 10 274.17 11.60 -2 6 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311.57 19.50 8 6 -16 285.17 16.00 8 -6 -16 281.27 16.40 -8 -6 16 254.87 11.60 8 -6 -16 276.77 17.20 8 -6 -16 275.37 18.90 8 -6 -16 271.47 14.90 10 6 -18 133.59 15.70 10 6 -18 101.29 12.20 -10 6 18 93.99 14.40 10 -6 -18 133.99 14.60 10 -6 -18 130.39 12.70 10 -6 -18 117.49 13.10 10 -6 -18 133.39 16.20 -11 7 3 93.89 10.80 11 7 -3 106.09 12.70 11 7 -3 74.39 8.10 11 -7 -3 74.89 8.40 11 -7 -3 84.59 9.80 11 -7 -3 90.89 11.60 -9 7 1 0.20 3.50 -9 7 1 0.60 5.00 9 7 -1 3.00 6.10 9 7 -1 0.90 3.60 9 -7 -1 6.10 4.80 9 -7 -1 4.30 5.70 9 -7 -1 6.20 5.50 9 -7 -1 0.10 3.90 -7 7 -1 84.89 8.50 7 7 1 93.39 9.70 7 7 1 89.09 7.10 7 7 1 89.99 6.30 -7 7 -1 71.79 6.80 7 7 1 92.89 7.00 -7 7 -1 89.49 6.20 7 -7 1 84.59 6.90 7 -7 1 93.79 8.80 7 -7 1 94.89 7.10 -7 -7 -1 93.79 6.40 7 -7 1 81.39 6.50 7 -7 1 73.69 5.60 7 -7 1 90.79 8.30 5 7 3 357.96 13.10 -5 7 -3 352.76 12.20 -5 7 -3 319.37 11.70 -5 7 -3 346.37 14.30 5 7 3 398.46 12.90 5 7 3 394.06 15.70 5 7 3 390.46 13.30 5 7 3 389.76 13.50 -5 7 -3 368.26 13.70 -5 7 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3.90 5.90 -7 7 15 1.90 6.80 7 7 -15 -2.40 5.30 7 -7 -15 -4.30 6.10 -7 -7 15 7.70 3.60 -7 -7 15 10.50 6.10 7 -7 -15 9.10 6.10 9 7 -17 20.30 7.80 -9 7 17 10.20 8.60 9 7 -17 33.00 8.10 9 7 -17 3.00 8.90 9 -7 -17 20.10 8.90 9 -7 -17 19.20 9.40 9 -7 -17 26.90 8.30 9 -7 -17 15.40 7.50 12 8 -4 31.70 7.30 -12 8 4 39.10 9.10 12 8 -4 35.40 10.30 12 -8 -4 20.60 6.60 12 -8 -4 40.10 9.90 12 -8 -4 31.50 8.00 -10 8 2 24.00 6.80 10 8 -2 14.60 7.90 10 8 -2 26.90 6.00 10 -8 -2 17.70 7.40 10 -8 -2 20.00 5.70 10 -8 -2 19.60 6.00 10 -8 -2 8.90 6.00 8 8 0 360.96 14.90 -8 8 0 370.96 15.00 -8 8 0 377.76 17.00 8 8 0 348.87 17.10 8 -8 0 352.06 16.50 8 -8 0 365.36 16.20 8 -8 0 384.06 14.60 8 -8 0 390.36 15.10 -6 8 -2 32.10 5.40 6 8 2 27.50 6.20 -6 8 -2 54.99 6.10 6 8 2 43.80 5.50 -6 8 -2 39.80 4.50 6 8 2 40.60 4.60 -6 8 -2 40.40 4.80 6 8 2 39.60 5.30 6 -8 2 47.20 6.80 6 -8 2 37.00 5.20 6 -8 2 32.90 4.80 6 -8 2 37.50 4.30 6 -8 2 37.10 4.30 -6 -8 -2 38.70 5.00 -6 -8 -2 39.60 4.70 6 -8 2 36.40 5.90 -4 8 -4 43.50 5.00 4 8 4 32.10 4.20 4 8 4 35.50 2.70 4 8 4 31.70 4.70 4 8 4 28.70 4.60 -4 8 -4 30.10 5.10 -4 8 -4 37.40 4.50 4 -8 4 36.90 4.90 4 -8 4 39.50 6.00 4 -8 4 37.00 4.70 4 -8 4 30.90 4.00 -4 -8 -4 37.20 4.60 -4 -8 -4 36.80 5.00 4 -8 4 33.30 2.80 4 -8 4 30.50 4.50 -4 -8 -4 33.00 5.60 -2 8 -6 185.48 9.50 -2 8 -6 176.38 10.10 2 8 6 184.28 9.30 2 8 6 177.68 8.80 2 8 6 190.38 10.30 -2 8 -6 182.08 8.50 -2 8 -6 181.88 9.60 2 8 6 183.18 8.40 2 8 6 176.68 9.40 2 -8 6 164.28 8.70 2 -8 6 161.58 8.90 2 -8 6 194.28 8.70 2 -8 6 192.38 8.30 -2 -8 -6 174.48 9.40 -2 -8 -6 193.48 9.00 -2 -8 -6 186.18 10.40 2 -8 6 175.68 9.30 0 8 8 9.30 4.00 0 8 -8 7.20 3.40 0 8 -8 12.10 3.80 0 8 8 12.00 3.30 0 8 -8 6.40 3.20 0 8 8 6.20 3.50 0 8 8 9.60 3.90 0 8 8 10.00 3.90 0 8 -8 15.40 3.70 0 -8 8 7.50 3.30 0 -8 8 10.30 4.10 0 -8 -8 7.40 3.00 0 -8 8 10.90 3.60 0 -8 -8 9.60 3.50 0 -8 -8 15.00 4.70 0 -8 8 11.60 3.60 0 -8 8 11.00 3.30 0 -8 -8 9.50 3.80 2 8 -10 275.37 11.80 -2 8 10 262.77 12.20 2 8 -10 254.17 11.70 2 8 -10 274.07 15.40 -2 8 10 270.97 13.20 -2 8 10 269.37 13.30 -2 8 10 261.17 12.00 2 8 -10 273.57 13.10 2 8 -10 267.47 9.70 -2 8 10 267.57 12.30 2 8 -10 262.57 12.00 -2 -8 10 260.57 10.50 -2 -8 10 289.87 13.20 2 -8 -10 270.27 11.00 -2 -8 10 268.27 12.70 2 -8 -10 260.97 12.40 2 -8 -10 282.77 15.60 2 -8 -10 270.67 11.60 2 -8 -10 259.47 11.90 -2 -8 10 283.97 11.90 2 -8 -10 259.47 12.90 4 8 -12 27.40 4.80 -4 8 12 20.60 5.10 4 8 -12 24.20 5.40 4 8 -12 28.90 5.50 4 8 -12 29.90 6.30 4 8 -12 32.30 4.80 -4 8 12 19.20 5.70 4 8 -12 22.10 7.40 -4 8 12 27.10 5.30 -4 8 12 18.70 6.30 -4 -8 12 27.70 4.00 -4 -8 12 32.10 5.80 4 -8 -12 27.70 6.00 4 -8 -12 22.50 4.90 4 -8 -12 31.00 5.00 4 -8 -12 30.00 6.10 -4 -8 12 27.30 6.10 -4 -8 12 22.50 5.50 4 -8 -12 24.70 7.80 4 -8 -12 19.80 4.80 6 8 -14 23.50 7.60 -6 8 14 42.00 7.10 6 8 -14 44.60 6.70 -6 8 14 26.50 7.30 6 8 -14 42.80 7.30 6 8 -14 41.80 5.20 6 8 -14 45.30 7.70 6 -8 -14 31.40 7.20 6 -8 -14 30.60 6.60 6 -8 -14 34.20 8.00 6 -8 -14 40.40 6.40 -6 -8 14 27.30 6.50 -6 -8 14 36.40 4.80 -8 8 16 12.50 7.40 8 8 -16 -5.30 7.90 8 8 -16 13.10 6.40 8 8 -16 6.80 6.10 8 -8 -16 19.10 7.40 8 -8 -16 -3.70 6.60 8 -8 -16 2.70 6.20 8 -8 -16 -1.40 6.10 11 9 -3 55.99 7.90 11 9 -3 57.59 11.00 -11 9 3 44.10 9.00 11 -9 -3 58.09 8.20 11 -9 -3 36.60 8.00 11 -9 -3 49.10 9.20 11 -9 -3 42.40 9.80 -9 9 1 4.60 4.60 9 9 -1 8.00 4.90 9 9 -1 8.00 6.20 -9 9 1 12.30 6.10 9 -9 -1 2.30 4.20 9 -9 -1 -0.40 5.40 9 -9 -1 6.90 5.40 9 -9 -1 8.20 4.90 -7 9 -1 9.30 5.10 7 9 1 7.10 4.10 -7 9 -1 5.20 4.50 7 9 1 -1.40 5.40 7 -9 1 9.70 5.30 7 -9 1 8.70 4.90 7 -9 1 3.60 3.30 7 -9 1 -1.60 3.70 5 9 3 44.90 5.80 -5 9 -3 31.10 4.80 -5 9 -3 38.10 6.00 -5 9 -3 42.00 4.00 5 9 3 23.20 5.80 -5 9 -3 29.30 5.60 -5 9 -3 41.20 4.90 5 9 3 36.20 5.50 5 9 3 35.30 4.60 5 -9 3 40.00 3.50 -5 -9 -3 38.30 5.50 5 -9 3 34.60 4.60 5 -9 3 32.10 5.20 -5 -9 -3 41.70 4.90 5 -9 3 36.20 6.20 5 -9 3 38.50 5.40 5 -9 3 48.00 6.20 3 9 5 0.90 3.60 3 9 5 6.70 2.70 3 9 5 -0.70 3.40 -3 9 -5 -0.50 3.00 3 9 5 9.50 3.80 -3 9 -5 2.50 2.70 3 9 5 3.20 1.80 -3 9 -5 4.10 4.10 3 9 5 -0.70 2.90 -3 9 -5 1.30 3.70 -3 -9 -5 0.40 1.50 3 -9 5 0.30 4.00 3 -9 5 4.60 3.00 -3 -9 -5 2.10 4.00 3 -9 5 -2.60 3.10 -3 -9 -5 1.70 3.10 3 -9 5 8.00 3.60 -3 -9 -5 2.60 3.20 3 -9 5 3.30 3.10 3 -9 5 7.30 3.40 -1 9 -7 141.59 9.30 1 9 7 141.49 9.50 1 9 7 145.99 8.50 -1 9 -7 157.88 10.50 1 9 7 146.89 8.70 1 9 7 143.89 9.20 -1 9 -7 141.39 8.20 -1 9 -7 150.68 9.30 -1 -9 -7 144.49 9.20 -1 -9 -7 144.49 8.30 1 -9 7 153.88 9.30 1 -9 7 139.19 8.50 -1 -9 -7 157.08 8.40 -1 -9 -7 152.48 10.20 1 -9 7 138.59 8.40 1 -9 7 145.29 8.60 1 -9 7 158.98 9.30 -1 9 9 79.19 7.70 1 9 -9 91.79 7.00 1 9 -9 84.59 9.80 -1 9 9 87.19 8.00 -1 9 9 88.49 7.70 -1 9 9 85.89 7.90 -1 9 9 91.59 8.40 1 9 -9 100.19 8.20 1 9 -9 94.89 7.60 1 9 -9 80.59 4.40 1 9 -9 95.79 8.60 1 -9 -9 100.39 7.80 -1 -9 9 91.69 7.60 -1 -9 9 90.09 6.90 1 -9 -9 82.49 9.00 -1 -9 9 82.19 7.60 1 -9 -9 100.29 8.10 1 -9 -9 103.99 8.80 -1 -9 9 73.89 6.70 -1 -9 9 78.99 7.50 -3 9 11 3.30 4.10 3 9 -11 -0.30 3.70 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14.50 -8 10 0 298.97 14.20 8 10 0 288.87 16.90 -8 10 0 290.07 15.80 8 -10 0 276.17 14.30 8 -10 0 281.77 15.10 8 -10 0 294.57 15.60 -6 10 -2 377.46 16.40 6 10 2 355.96 16.70 -6 10 -2 352.96 15.60 6 10 2 364.76 15.50 6 -10 2 344.27 16.20 6 -10 2 375.46 15.60 6 -10 2 380.66 15.80 4 10 4 15.90 5.00 4 10 4 18.30 4.90 -4 10 -4 22.80 4.10 -4 10 -4 24.80 4.80 -4 10 -4 26.80 4.80 -4 10 -4 29.00 5.90 4 10 4 33.30 6.30 -4 -10 -4 18.70 2.60 -4 -10 -4 18.60 4.20 4 -10 4 21.40 4.80 4 -10 4 22.80 4.90 4 -10 4 17.90 4.50 4 -10 4 25.30 4.50 -4 -10 -4 24.70 5.60 -4 -10 -4 13.40 4.60 -2 10 -6 341.17 13.20 -2 10 -6 307.67 13.80 2 10 6 317.67 14.10 2 10 6 310.27 13.30 2 10 6 367.06 15.30 -2 10 -6 335.77 14.40 -2 10 -6 331.17 14.30 2 10 6 338.87 14.50 2 10 6 330.77 12.60 2 -10 6 340.27 13.90 2 -10 6 318.57 13.90 2 -10 6 359.06 14.50 -2 -10 -6 333.77 14.50 -2 -10 -6 321.97 13.50 2 -10 6 321.87 13.80 2 -10 6 341.37 13.60 -2 -10 -6 323.37 15.10 2 -10 6 317.17 13.00 0 10 8 186.38 10.80 0 10 -8 161.08 9.40 0 10 8 158.08 9.70 0 10 -8 164.88 10.20 0 10 8 167.78 10.80 0 10 8 165.58 10.70 0 10 -8 150.58 10.20 0 10 -8 167.38 12.00 0 10 8 174.38 9.80 0 -10 8 149.49 10.30 0 -10 -8 185.78 10.80 0 -10 -8 131.59 5.80 0 -10 8 152.08 8.90 0 -10 -8 170.28 9.60 0 -10 -8 185.68 11.70 0 -10 8 159.38 9.60 0 -10 8 148.59 10.00 0 -10 8 140.89 9.10 0 -10 -8 161.68 15.30 -2 10 10 191.78 11.70 2 10 -10 158.68 10.30 -2 10 10 170.98 11.30 2 10 -10 175.88 7.80 2 10 -10 183.88 13.70 2 10 -10 171.88 11.70 -2 10 10 175.08 11.10 2 10 -10 187.58 10.70 -2 10 10 173.08 11.90 -2 10 10 177.98 10.60 2 -10 -10 163.38 9.90 -2 -10 10 172.08 10.20 2 -10 -10 163.78 10.60 -2 -10 10 171.68 11.30 2 -10 -10 168.98 13.80 -2 -10 10 206.08 12.20 2 -10 -10 160.98 10.60 -2 -10 10 192.88 11.00 -2 -10 10 177.78 9.20 2 -10 -10 174.98 11.60 -4 10 12 342.77 15.90 -4 10 12 375.46 16.70 4 10 -12 332.07 19.70 4 10 -12 380.16 16.80 -4 10 12 389.86 18.30 4 10 -12 350.56 17.70 -4 10 12 385.56 18.20 4 10 -12 392.96 14.70 4 10 -12 342.97 15.00 4 10 -12 391.46 20.20 4 -10 -12 389.06 17.10 -4 -10 12 397.46 17.60 4 -10 -12 366.66 14.30 4 -10 -12 368.66 19.80 4 -10 -12 370.76 17.60 -4 -10 12 397.26 14.00 4 -10 -12 385.06 16.10 4 -10 -12 374.16 17.30 -4 -10 12 369.86 17.30 6 10 -14 136.09 9.50 -6 10 14 151.88 14.30 6 10 -14 121.19 13.30 6 10 -14 142.99 10.60 6 -10 -14 127.29 10.70 6 -10 -14 117.39 11.30 6 -10 -14 143.39 14.30 8 10 -16 4.60 8.80 -8 10 16 9.10 8.60 8 10 -16 3.50 6.50 8 -10 -16 2.80 5.70 8 -10 -16 16.40 9.30 11 11 -3 2.90 7.50 11 11 -3 -5.70 6.20 -11 11 3 -0.10 7.50 11 -11 -3 0.40 6.50 11 -11 -3 11.40 8.30 11 -11 -3 1.10 6.50 9 11 -1 58.49 10.00 -9 11 1 53.59 8.50 -9 11 1 65.59 8.20 9 11 -1 63.49 8.60 9 -11 -1 58.69 9.10 9 -11 -1 46.00 8.60 9 -11 -1 66.49 8.70 7 11 1 55.39 8.80 7 11 1 69.99 8.30 -7 11 -1 61.39 7.60 -7 11 -1 58.39 8.40 7 -11 1 62.29 8.20 7 -11 1 67.29 8.40 7 -11 1 69.39 8.10 -5 11 -3 313.67 15.00 5 11 3 336.57 15.00 -5 11 -3 298.37 14.70 5 11 3 318.97 15.00 5 -11 3 299.07 14.20 -5 -11 -3 302.57 15.70 5 -11 3 296.77 14.60 5 -11 3 322.87 15.00 -3 11 -5 1.50 4.90 3 11 5 -0.40 4.00 3 11 5 1.70 4.70 3 11 5 2.60 4.00 3 11 5 5.00 3.00 -3 11 -5 6.80 3.60 3 11 5 8.50 4.70 -3 11 -5 1.60 3.20 -3 11 -5 6.90 4.10 3 -11 5 5.40 4.10 3 -11 5 5.80 4.60 -3 -11 -5 3.60 4.10 -3 -11 -5 4.00 4.90 3 -11 5 6.10 3.70 -1 11 -7 4.90 4.70 1 11 7 1.80 3.90 1 11 7 1.90 4.90 1 11 7 6.90 4.10 -1 11 -7 3.90 5.00 1 11 7 4.10 4.30 1 11 7 12.00 5.10 -1 11 -7 1.80 4.30 -1 11 -7 10.20 3.80 1 -11 7 6.30 4.50 1 -11 7 5.80 4.50 1 -11 7 2.10 4.00 1 -11 7 8.10 4.10 1 -11 7 6.80 4.50 -1 -11 -7 18.80 5.50 -1 -11 -7 6.60 3.80 -1 -11 -7 9.10 5.30 -1 11 9 88.29 8.50 1 11 -9 82.99 9.70 -1 11 9 73.89 8.20 1 11 -9 89.69 8.30 1 11 -9 92.49 8.60 -1 11 9 93.69 9.30 -1 11 9 69.29 8.20 -1 11 9 85.89 8.40 1 11 -9 87.69 8.90 1 -11 -9 86.49 8.40 -1 -11 9 88.39 7.90 1 -11 -9 96.29 9.20 -1 -11 9 70.59 7.30 1 -11 -9 95.69 10.30 -1 -11 9 93.69 8.80 -1 -11 9 79.99 8.50 -1 -11 9 83.79 7.40 3 11 -11 85.19 8.60 -3 11 11 76.59 8.50 3 11 -11 84.19 8.20 -3 11 11 70.69 8.60 -3 11 11 89.79 9.60 -3 11 11 76.49 8.40 3 11 -11 68.39 10.20 -3 11 11 75.99 9.40 3 -11 -11 71.09 6.90 3 -11 -11 99.69 9.80 3 -11 -11 83.39 9.40 3 -11 -11 92.69 10.60 3 -11 -11 86.29 8.10 -3 -11 11 70.59 8.70 3 -11 -11 94.09 11.80 -3 -11 11 85.39 8.40 -3 -11 11 91.79 7.30 5 11 -13 346.67 14.90 -5 11 13 361.96 19.00 5 11 -13 350.16 15.30 5 11 -13 374.16 21.30 5 -11 -13 352.76 16.30 5 -11 -13 320.97 25.50 5 -11 -13 358.36 20.20 -7 11 15 -14.30 6.10 7 11 -15 0.10 5.80 7 11 -15 -0.90 8.00 7 -11 -15 -2.10 8.40 7 -11 -15 4.50 5.80 10 12 -2 73.09 11.80 10 12 -2 75.09 9.90 -10 12 2 65.49 11.30 10 -12 -2 51.99 9.10 10 -12 -2 84.09 10.60 10 -12 -2 64.29 10.20 8 12 0 -0.40 5.40 -8 12 0 -1.90 4.90 8 12 0 -3.70 6.50 -8 12 0 1.80 5.20 8 -12 0 4.90 6.10 8 -12 0 9.70 5.90 8 -12 0 2.10 5.60 6 12 2 7.90 5.00 -6 12 -2 7.00 5.00 -6 12 -2 8.70 5.40 6 12 2 16.70 5.70 6 -12 2 5.50 6.00 -6 -12 -2 16.00 6.40 6 -12 2 6.70 5.30 6 -12 2 5.60 5.30 -4 12 -4 43.20 6.70 4 12 4 43.90 7.10 4 12 4 39.30 6.90 -4 12 -4 41.60 6.20 -4 -12 -4 43.80 7.10 4 -12 4 32.50 6.50 4 -12 4 37.40 6.10 -2 12 -6 859.91 28.10 2 12 6 870.01 26.60 2 12 6 920.11 29.50 2 12 6 878.71 29.10 2 12 6 942.31 30.00 -2 12 -6 839.52 27.60 -2 12 -6 892.11 27.80 -2 12 -6 894.11 29.20 -2 -12 -6 905.41 29.90 -2 -12 -6 926.51 30.30 2 -12 6 905.71 28.30 2 -12 6 921.71 28.20 0 12 -8 179.68 11.90 0 12 8 189.68 12.90 0 12 8 200.28 12.80 0 12 -8 196.38 11.30 0 12 8 187.08 11.60 0 12 -8 185.18 13.20 0 12 8 160.48 10.60 0 -12 8 188.58 11.30 0 -12 -8 199.18 12.80 0 -12 8 185.48 10.50 0 -12 8 183.58 11.10 0 -12 8 190.58 12.40 0 -12 -8 213.88 13.40 -2 12 10 35.30 7.20 -2 12 10 46.00 7.70 2 12 -10 38.10 6.90 -2 12 10 34.50 7.10 -2 12 10 43.10 7.10 2 12 -10 47.00 8.90 2 12 -10 42.10 6.70 2 -12 -10 39.60 7.30 2 -12 -10 39.60 6.70 -2 -12 10 52.19 6.00 -2 -12 10 49.60 6.50 -2 -12 10 33.40 6.60 2 -12 -10 53.69 9.70 -2 -12 10 37.70 6.80 -4 12 12 28.00 6.70 -4 12 12 24.20 7.40 4 12 -12 17.70 8.10 4 12 -12 25.30 5.80 4 -12 -12 20.10 6.00 4 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13.10 11 -7 -2 216.28 14.90 9 7 0 71.59 7.10 -9 7 0 80.79 7.40 -9 7 0 73.29 8.70 9 7 0 71.39 9.60 9 -7 0 65.89 8.40 9 -7 0 61.59 8.50 9 -7 0 78.79 7.20 7 7 2 184.48 12.30 -7 7 -2 150.88 7.50 7 7 2 148.09 7.50 -7 7 -2 137.89 9.60 7 7 2 147.39 8.60 7 7 2 169.88 11.70 -7 7 -2 136.89 8.80 -7 -7 -2 138.29 7.60 7 -7 2 152.58 10.00 7 -7 2 143.79 10.20 7 -7 2 159.38 8.10 7 -7 2 153.38 8.60 7 -7 2 156.88 7.70 -5 7 -4 2.10 3.30 5 7 4 -3.10 4.10 5 7 4 1.90 2.80 5 7 4 2.10 2.80 -5 7 -4 1.80 2.60 5 7 4 6.60 3.10 5 7 4 5.70 1.80 -5 7 -4 7.60 2.80 5 -7 4 3.30 2.50 -5 -7 -4 6.30 3.00 -5 -7 -4 6.30 2.70 5 -7 4 10.40 4.40 5 -7 4 8.30 2.60 5 -7 4 6.00 3.60 5 -7 4 6.80 4.50 5 -7 4 5.60 2.50 5 -7 4 6.50 3.00 5 -7 4 4.90 3.10 3 7 6 103.79 7.00 3 7 6 102.29 4.90 -3 7 -6 108.59 7.00 3 7 6 111.69 6.40 -3 7 -6 104.49 5.90 3 7 6 99.89 7.00 3 7 6 107.99 6.30 3 7 6 105.89 7.30 -3 7 -6 108.89 7.50 -3 7 -6 120.19 7.00 3 -7 6 90.19 8.30 3 -7 6 129.29 8.10 3 -7 6 129.39 7.80 -3 -7 -6 110.69 7.20 3 -7 6 104.89 6.40 3 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79.49 7.10 -2 -8 -7 65.39 6.30 2 -8 7 58.59 5.30 2 -8 7 53.09 5.50 2 -8 7 54.39 5.40 2 -8 7 53.79 5.70 -2 -8 -7 72.49 7.70 0 8 -9 893.01 26.60 0 8 9 906.51 27.50 0 8 -9 899.41 26.70 0 8 9 898.31 27.60 0 8 9 903.61 26.90 0 8 -9 924.51 26.10 0 8 -9 913.71 28.00 0 8 9 882.11 27.30 0 8 -9 922.61 29.20 0 -8 -9 924.21 26.50 0 -8 9 901.21 26.30 0 -8 9 907.71 27.50 0 -8 -9 889.61 28.70 0 -8 -9 896.81 27.60 0 -8 9 915.81 27.50 0 -8 9 896.91 26.90 0 -8 9 903.51 26.40 0 -8 -9 928.01 27.10 -2 8 11 398.06 15.80 -2 8 11 412.36 16.60 -2 8 11 406.26 17.30 2 8 -11 423.86 16.00 2 8 -11 418.06 15.20 2 8 -11 412.36 18.60 -2 8 11 412.86 16.40 2 8 -11 404.76 16.80 2 8 -11 391.16 15.20 -2 -8 11 408.26 14.50 2 -8 -11 414.16 16.10 -2 -8 11 403.56 16.40 2 -8 -11 405.46 15.50 2 -8 -11 402.16 15.90 -2 -8 11 407.96 16.50 2 -8 -11 411.96 14.60 2 -8 -11 408.96 16.70 2 -8 -11 379.36 18.80 -2 -8 11 408.66 15.50 -4 8 13 6.50 4.50 4 8 -13 6.50 4.70 -4 8 13 16.90 4.60 4 8 -13 14.50 4.80 4 8 -13 9.00 3.80 -4 8 13 8.90 5.20 -4 8 13 6.80 5.20 4 8 -13 10.50 5.50 4 8 -13 14.50 4.20 4 8 -13 -9.50 7.70 4 -8 -13 10.70 5.20 4 -8 -13 1.40 4.00 4 -8 -13 9.50 4.20 4 -8 -13 25.40 9.20 4 -8 -13 16.20 4.40 4 -8 -13 8.40 4.60 -4 -8 13 8.30 5.40 -4 -8 13 9.10 3.50 -4 -8 13 5.30 4.90 -4 -8 13 11.90 4.80 -6 8 15 49.50 9.30 6 8 -15 44.90 6.80 -6 8 15 43.90 7.60 6 8 -15 46.50 9.80 6 8 -15 46.00 5.60 6 8 -15 48.10 8.30 6 -8 -15 52.89 10.20 6 -8 -15 42.30 6.50 -6 -8 15 49.99 5.50 6 -8 -15 38.10 7.20 6 -8 -15 41.30 7.20 8 8 -17 155.08 16.80 -8 8 17 131.29 15.20 8 8 -17 130.09 11.80 8 -8 -17 152.48 16.30 8 -8 -17 139.59 12.60 8 -8 -17 143.89 13.90 -11 9 2 -2.50 6.40 11 9 -2 5.30 8.00 11 9 -2 1.10 5.10 11 -9 -2 -5.30 7.00 11 -9 -2 -1.10 6.00 11 -9 -2 -5.70 4.80 -9 9 0 -2.80 4.50 9 9 0 8.60 4.80 9 9 0 15.30 7.30 -9 9 0 16.20 5.30 9 -9 0 13.50 5.00 9 -9 0 14.40 6.40 9 -9 0 8.40 4.40 -7 9 -2 168.48 11.20 7 9 2 167.38 12.70 7 9 2 175.08 10.40 -7 9 -2 171.78 11.10 7 -9 2 162.78 11.40 7 -9 2 180.88 10.60 7 -9 2 175.88 11.00 -5 9 -4 1864.71 49.60 -5 9 -4 1852.81 51.19 5 9 4 1855.81 50.09 -5 9 -4 1820.62 48.00 -5 9 -4 1839.12 50.69 5 9 4 1910.41 50.39 5 -9 4 1913.21 49.10 -5 -9 -4 1925.31 49.70 -5 -9 -4 1842.62 50.29 5 -9 4 1850.61 49.99 5 -9 4 1961.00 50.29 -5 -9 -4 1913.51 53.09 5 -9 4 1837.82 50.99 3 9 6 138.59 5.90 3 9 6 149.29 7.50 -3 9 -6 117.59 8.30 -3 9 -6 125.49 9.30 3 9 6 147.89 9.30 3 9 6 147.89 9.00 -3 9 -6 130.89 7.80 3 9 6 149.19 9.20 -3 9 -6 136.29 9.40 3 -9 6 150.58 9.20 -3 -9 -6 145.29 8.20 3 -9 6 140.69 8.00 3 -9 6 133.49 9.60 3 -9 6 141.69 8.40 -3 -9 -6 157.28 10.50 -3 -9 -6 145.39 9.10 3 -9 6 141.09 9.10 3 -9 6 126.19 7.70 1 9 8 156.78 9.60 -1 9 -8 138.79 11.70 -1 9 -8 163.78 9.70 1 9 8 166.38 9.00 1 9 8 153.28 9.30 1 9 8 153.18 9.90 -1 9 -8 146.99 9.70 1 9 8 149.79 10.10 -1 9 -8 139.29 8.30 1 -9 8 167.78 9.10 1 -9 8 156.88 9.30 -1 -9 -8 144.89 9.40 1 -9 8 143.29 9.00 1 -9 8 173.58 9.20 -1 -9 -8 150.68 11.00 -1 -9 -8 150.08 8.80 1 -9 8 144.89 9.60 -1 9 10 4.00 4.30 1 9 -10 4.30 4.20 1 9 -10 2.60 3.70 1 9 -10 6.20 3.70 -1 9 10 2.80 4.30 -1 9 10 1.30 3.10 -1 9 10 8.00 4.50 1 9 -10 3.00 5.90 -1 9 10 1.80 4.00 1 9 -10 5.50 2.10 -1 -9 10 5.20 3.60 -1 -9 10 2.90 4.30 1 -9 -10 -3.10 3.80 -1 -9 10 6.70 3.80 1 -9 -10 4.40 4.20 -1 -9 10 2.50 3.70 1 -9 -10 8.70 6.10 1 -9 -10 3.60 3.80 -1 -9 10 1.90 3.90 -3 9 12 372.36 16.10 3 9 -12 335.27 19.00 3 9 -12 362.96 16.70 3 9 -12 378.86 15.40 3 9 -12 351.76 12.90 -3 9 12 344.97 17.00 -3 9 12 348.67 16.30 -3 9 12 322.97 14.70 3 9 -12 368.26 14.40 3 -9 -12 347.37 15.60 -3 -9 12 350.06 15.60 -3 -9 12 343.87 13.30 3 -9 -12 334.47 14.10 3 -9 -12 355.06 15.60 -3 -9 12 362.36 15.30 3 -9 -12 359.56 16.20 -3 -9 12 362.86 16.30 3 -9 -12 343.57 13.80 3 -9 -12 347.27 19.50 -5 9 14 715.03 25.40 5 9 -14 690.13 29.10 -5 9 14 701.03 27.80 5 9 -14 712.73 22.80 5 -9 -14 722.83 25.80 5 -9 -14 747.03 24.10 5 -9 -14 685.13 25.70 5 -9 -14 743.83 29.10 -7 9 16 258.27 18.30 7 9 -16 276.97 19.90 7 -9 -16 252.77 14.20 7 -9 -16 276.17 19.50 9 9 -18 8.70 7.60 -9 9 18 1.80 8.90 9 9 -18 3.10 8.70 9 -9 -18 1.60 8.40 9 -9 -18 3.60 7.50 9 -9 -18 -1.40 7.30 -10 10 1 6.80 6.60 10 10 -1 10.90 7.60 10 10 -1 5.60 5.60 10 -10 -1 3.10 5.20 10 -10 -1 1.50 6.30 10 -10 -1 11.80 7.50 -8 10 -1 71.39 9.10 -8 10 -1 63.19 7.80 8 10 1 68.99 9.90 8 10 1 62.39 7.60 8 -10 1 62.99 9.00 8 -10 1 62.19 8.10 8 -10 1 62.79 7.60 6 10 3 719.83 25.40 -6 10 -3 636.44 23.50 6 10 3 688.03 23.00 -6 10 -3 696.33 23.50 -6 -10 -3 659.23 25.20 6 -10 3 691.43 23.10 6 -10 3 668.83 24.10 6 -10 3 650.93 23.00 -4 10 -5 138.09 10.20 4 10 5 131.29 9.80 -4 10 -5 145.29 11.10 4 10 5 146.99 9.40 -4 10 -5 140.69 8.70 4 10 5 135.79 10.20 -4 10 -5 150.68 8.20 4 -10 5 156.98 9.40 4 -10 5 153.48 9.70 4 -10 5 146.19 10.20 4 -10 5 137.99 9.10 -4 -10 -5 145.29 11.00 -4 -10 -5 130.89 9.60 4 -10 5 139.09 8.20 -2 10 -7 86.69 7.00 2 10 7 93.39 7.60 2 10 7 102.69 8.60 2 10 7 94.19 7.20 -2 10 -7 92.69 8.20 -2 10 -7 116.99 9.50 2 10 7 117.09 10.00 -2 10 -7 91.49 8.60 2 10 7 107.79 8.70 -2 -10 -7 98.59 9.10 2 -10 7 101.89 8.00 2 -10 7 109.29 9.00 -2 -10 -7 107.29 8.00 2 -10 7 109.69 7.70 2 -10 7 102.39 8.00 -2 -10 -7 106.59 9.70 2 -10 7 93.99 8.10 2 -10 7 107.99 8.10 0 10 9 17.40 4.70 0 10 9 20.50 5.20 0 10 -9 12.60 4.00 0 10 9 12.00 4.50 0 10 9 17.70 5.60 0 10 9 14.20 5.20 0 10 -9 15.20 4.90 0 10 -9 16.40 4.80 0 10 -9 16.80 6.60 0 -10 9 10.00 4.50 0 -10 9 11.80 5.00 0 -10 9 16.50 4.50 0 -10 9 6.90 4.10 0 -10 -9 10.70 4.10 0 -10 9 8.00 4.30 0 -10 -9 21.50 5.20 0 -10 -9 10.20 5.00 2 10 -11 925.81 30.60 2 10 -11 891.31 28.30 -2 10 11 899.51 29.90 -2 10 11 866.31 28.80 2 10 -11 903.91 28.80 -2 10 11 902.11 30.20 -2 10 11 920.61 29.70 -2 10 11 919.11 29.40 2 10 -11 964.20 32.90 -2 -10 11 944.91 29.40 2 -10 -11 916.31 29.40 -2 -10 11 979.60 27.40 -2 -10 11 940.51 30.10 -2 -10 11 913.61 29.80 -2 -10 11 921.11 28.20 2 -10 -11 893.31 31.70 2 -10 -11 922.41 30.30 2 -10 -11 921.11 27.60 -4 10 13 7.50 6.10 4 10 -13 4.70 4.00 4 10 -13 -2.50 4.50 -4 10 13 -5.40 4.10 4 10 -13 2.50 6.20 4 10 -13 1.00 4.00 4 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6 21.80 3.30 -4 -4 -6 23.00 4.50 4 -4 6 22.70 2.70 4 -4 6 23.10 2.60 4 -4 6 28.80 3.10 4 -4 6 20.20 4.40 4 -4 6 24.40 2.50 -4 -4 -6 20.90 2.60 -4 -4 -6 21.10 2.90 -2 4 -8 627.34 17.90 -2 4 -8 638.24 19.30 2 4 8 645.94 18.30 2 4 8 646.24 17.90 2 4 8 634.84 18.50 -2 4 -8 604.44 18.50 -2 4 -8 647.94 20.20 2 4 8 644.94 18.50 2 4 8 652.43 18.30 -2 4 -8 630.94 16.90 -2 -4 -8 658.83 18.40 2 -4 8 635.54 18.80 -2 -4 -8 636.14 20.80 2 -4 8 628.64 17.90 -2 -4 -8 645.64 18.70 2 -4 8 619.14 17.90 2 -4 8 627.04 17.10 2 -4 8 635.14 19.30 2 -4 8 634.44 18.30 2 -4 8 660.13 18.50 0 4 10 402.86 15.60 0 4 -10 411.86 14.30 0 4 -10 417.06 13.80 0 4 10 416.16 14.50 0 4 -10 430.46 14.10 0 4 10 401.16 13.80 0 4 -10 414.06 12.70 0 4 10 417.16 14.00 0 4 -10 416.66 15.90 0 -4 10 415.36 13.80 0 -4 -10 417.66 14.00 0 -4 -10 425.76 13.40 0 -4 -10 412.46 15.50 0 -4 -10 418.46 14.30 0 -4 10 417.76 13.70 0 -4 10 407.56 13.60 0 -4 10 406.16 14.10 0 -4 -10 401.66 15.50 0 -4 10 415.86 14.40 2 4 -12 51.19 5.30 2 4 -12 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423.46 16.20 -4 10 -6 428.06 17.60 4 10 6 433.76 13.20 4 -10 6 447.26 18.00 4 -10 6 442.76 17.00 -4 -10 -6 457.45 19.20 4 -10 6 441.96 17.40 4 -10 6 446.76 16.40 2 10 8 43.50 5.50 -2 10 -8 33.80 5.60 -2 10 -8 37.80 6.90 2 10 8 39.60 5.60 2 10 8 49.50 6.50 -2 10 -8 54.99 6.10 -2 10 -8 38.50 6.00 2 10 8 51.29 6.70 2 -10 8 39.60 6.10 2 -10 8 47.00 6.60 -2 -10 -8 40.30 7.00 -2 -10 -8 41.50 5.40 2 -10 8 39.00 6.00 -2 -10 -8 46.20 6.40 2 -10 8 41.90 5.50 2 -10 8 46.70 6.60 2 -10 8 38.70 5.30 0 10 -10 44.10 6.00 0 10 -10 38.90 6.30 0 10 10 41.30 5.90 0 10 -10 33.50 6.40 0 10 10 38.90 7.00 0 10 10 36.70 5.90 0 10 -10 37.30 7.50 0 10 10 32.10 6.10 0 -10 10 43.70 6.40 0 -10 10 45.40 6.30 0 -10 -10 49.80 7.10 0 -10 10 38.40 5.80 0 -10 10 40.20 5.80 0 -10 -10 41.20 7.60 0 -10 10 46.70 7.20 0 -10 -10 39.60 5.90 -2 10 12 144.29 11.60 2 10 -12 133.29 13.10 2 10 -12 123.09 9.60 2 10 -12 144.69 9.90 -2 10 12 121.09 9.60 -2 10 12 141.49 11.60 -2 10 12 135.39 10.30 -2 -10 12 117.09 8.80 -2 -10 12 119.59 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101.69 8.50 2 -8 -13 95.99 11.20 2 -8 -13 101.49 9.60 -2 -8 13 127.49 10.40 2 -8 -13 106.09 7.50 -2 -8 13 80.49 8.10 2 -8 -13 117.19 9.20 2 -8 -13 109.59 8.90 -2 -8 13 95.89 7.90 -4 8 15 180.68 12.30 4 8 -15 192.08 10.00 -4 8 15 189.58 13.30 -4 8 15 204.68 15.10 4 8 -15 212.38 11.10 4 8 -15 206.18 12.50 4 8 -15 184.58 16.60 4 -8 -15 203.48 11.70 4 -8 -15 166.98 14.20 -4 -8 15 208.88 12.40 -4 -8 15 200.88 10.30 -4 -8 15 217.38 13.40 4 -8 -15 198.78 13.20 4 -8 -15 202.68 10.70 6 8 -17 114.09 14.40 6 8 -17 116.59 9.70 -6 8 17 105.79 12.80 -6 -8 17 108.19 8.20 6 -8 -17 94.69 11.90 6 -8 -17 103.49 9.30 8 8 -19 9.90 6.60 -8 8 19 28.20 9.90 8 8 -19 19.90 8.90 8 -8 -19 15.80 7.30 8 -8 -19 27.20 10.40 11 9 0 -4.10 7.10 -11 9 0 8.00 6.70 11 9 0 3.00 5.20 11 -9 0 4.90 6.90 11 -9 0 2.40 5.00 11 -9 0 2.70 6.60 9 9 2 11.80 5.00 -9 9 -2 5.90 5.80 9 9 2 -2.90 6.40 -9 9 -2 6.20 5.30 9 -9 2 6.90 4.40 9 -9 2 4.80 6.00 9 -9 2 11.30 6.70 7 9 4 159.78 13.00 -7 9 -4 182.58 11.50 -7 9 -4 174.98 11.90 7 9 4 181.08 10.60 7 -9 4 190.18 10.60 7 -9 4 185.68 12.00 7 -9 4 205.78 11.60 -5 9 -6 394.86 16.00 5 9 6 377.86 15.40 -5 9 -6 373.46 15.00 5 -9 6 395.46 15.20 5 -9 6 362.26 14.70 5 -9 6 405.56 15.30 -5 -9 -6 393.86 17.60 5 -9 6 364.76 16.10 5 -9 6 414.96 16.70 3 9 8 500.75 17.60 -3 9 -8 503.95 19.40 3 9 8 502.85 18.60 -3 9 -8 493.65 16.90 -3 9 -8 549.95 19.00 3 9 8 531.25 18.40 -3 9 -8 502.65 18.00 3 9 8 496.25 17.40 3 9 8 518.65 15.20 3 -9 8 508.05 16.90 3 -9 8 514.65 18.20 -3 -9 -8 493.75 18.40 3 -9 8 497.45 18.30 3 -9 8 524.65 17.50 3 -9 8 502.35 18.70 3 -9 8 517.35 18.20 -3 -9 -8 521.85 17.60 -3 -9 -8 507.85 20.40 -1 9 -10 223.98 10.70 1 9 10 221.78 12.20 -1 9 -10 206.88 14.00 1 9 10 224.58 11.00 1 9 10 227.78 11.80 1 9 10 233.38 11.50 -1 9 -10 214.28 11.80 -1 -9 -10 210.48 11.60 1 -9 10 245.58 11.20 1 -9 10 210.88 11.10 -1 -9 -10 221.48 13.40 1 -9 10 209.08 11.10 1 -9 10 199.08 11.80 -1 -9 -10 229.98 11.10 1 -9 10 224.48 11.40 1 9 -12 1.20 6.60 1 9 -12 0.00 4.40 -1 9 12 -0.80 4.70 -1 9 12 6.10 4.20 1 9 -12 -0.30 3.40 1 9 -12 -1.80 3.90 -1 9 12 4.20 5.10 -1 9 12 0.90 4.10 -1 -9 12 3.30 3.70 1 -9 -12 1.90 3.80 -1 -9 12 -3.90 3.80 1 -9 -12 -1.30 4.50 -1 -9 12 -4.10 4.30 1 -9 -12 2.80 6.40 -1 -9 12 2.70 3.90 -1 -9 12 -0.70 3.90 -3 9 14 44.30 8.00 -3 9 14 62.49 8.10 -3 9 14 49.80 8.20 3 9 -14 53.49 7.10 3 9 -14 44.10 6.50 3 9 -14 45.80 9.80 3 -9 -14 73.39 9.00 -3 -9 14 49.50 6.20 3 -9 -14 50.59 9.60 -3 -9 14 68.79 8.70 3 -9 -14 51.49 6.40 3 -9 -14 49.40 6.70 -3 -9 14 57.79 7.60 5 9 -16 251.77 12.60 5 9 -16 255.57 12.50 5 9 -16 252.07 19.30 -5 9 16 244.78 17.60 5 -9 -16 253.37 18.30 5 -9 -16 261.07 13.20 7 9 -18 285.87 21.20 7 9 -18 264.97 14.90 -7 9 18 253.37 20.20 7 -9 -18 306.47 14.90 7 -9 -18 287.57 20.80 -10 10 -1 20.00 7.50 10 10 1 19.70 8.50 10 10 1 22.90 6.20 -10 10 -1 13.40 6.00 10 -10 1 18.00 7.30 10 -10 1 18.60 5.90 10 -10 1 5.00 7.30 -8 10 -3 38.50 7.70 8 10 3 41.50 8.70 -8 10 -3 28.60 7.00 8 10 3 39.40 6.40 8 -10 3 34.40 6.10 8 -10 3 37.50 7.60 8 -10 3 44.90 7.20 -6 10 -5 11.30 5.60 6 10 5 7.10 4.90 -6 10 -5 7.60 4.50 6 -10 5 6.10 4.50 -6 -10 -5 3.20 5.50 6 -10 5 11.30 4.90 6 -10 5 1.30 5.30 -4 10 -7 365.46 15.40 4 10 7 371.16 15.90 4 10 7 372.46 11.50 -4 10 -7 368.86 15.80 4 -10 7 388.76 16.80 -4 -10 -7 346.37 16.90 4 -10 7 394.56 14.90 4 -10 7 387.96 16.30 4 -10 7 362.66 15.40 -2 10 -9 25.00 5.40 2 10 9 51.79 6.70 -2 10 -9 27.40 4.80 -2 10 -9 45.50 7.40 2 10 9 34.60 5.50 2 10 9 30.80 6.30 -2 -10 -9 39.10 7.30 2 -10 9 36.10 5.30 2 -10 9 42.00 5.40 2 -10 9 47.00 6.70 2 -10 9 35.60 6.10 -2 -10 -9 34.80 6.10 2 -10 9 43.60 6.50 0 10 -11 28.80 8.60 0 10 -11 22.00 5.70 0 10 -11 32.00 5.50 0 10 11 38.90 6.60 0 10 11 35.50 6.10 0 10 11 42.60 6.70 0 -10 -11 19.60 6.20 0 -10 11 40.30 6.20 0 -10 11 37.40 6.40 0 -10 11 38.50 5.90 0 -10 11 32.20 5.60 0 -10 -11 43.60 6.50 -2 10 13 130.89 10.50 -2 10 13 125.99 10.80 2 10 -13 107.69 9.10 2 10 -13 109.99 12.50 2 10 -13 102.79 9.30 -2 10 13 101.89 10.90 -2 -10 13 122.19 9.10 -2 -10 13 120.19 10.80 2 -10 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7.80 4.30 0 8 15 19.70 6.50 0 -8 15 23.50 6.30 0 -8 -15 17.10 7.90 0 -8 -15 24.70 6.60 0 -8 15 10.10 4.80 0 -8 15 15.20 5.20 -2 8 17 95.29 10.20 -2 8 17 85.29 10.60 2 8 -17 86.99 8.40 2 8 -17 101.69 13.40 2 -8 -17 84.49 7.00 -2 -8 17 85.59 8.80 2 -8 -17 81.89 9.70 -2 -8 17 92.59 10.40 2 -8 -17 86.89 12.60 -2 -8 17 106.19 9.90 4 8 -19 133.69 15.70 4 8 -19 116.29 9.60 -4 8 19 117.09 13.10 4 -8 -19 139.59 15.10 4 -8 -19 106.59 10.90 -4 -8 19 112.79 9.80 -4 -8 19 118.39 12.40 6 8 -21 131.89 16.90 -6 8 21 123.49 14.80 -6 -8 21 114.39 9.90 6 -8 -21 134.39 15.30 11 9 4 103.39 9.60 11 9 4 81.29 12.80 -11 9 -4 97.49 11.70 11 -9 4 100.59 9.50 11 -9 4 99.69 12.00 11 -9 4 73.89 11.30 -9 9 -6 91.99 10.90 9 9 6 94.99 8.70 -9 9 -6 92.79 9.70 9 -9 6 74.89 10.00 9 -9 6 88.19 8.10 9 -9 6 90.69 11.00 -9 -9 -6 96.89 12.10 7 9 8 61.29 7.20 -7 9 -8 61.59 8.00 7 -9 8 59.59 6.80 7 -9 8 48.60 8.80 7 -9 8 63.09 9.10 -7 -9 -8 67.79 10.00 5 9 10 9.50 4.80 -5 9 -10 -9.10 5.40 -5 9 -10 -1.30 4.50 5 -9 10 -4.50 4.40 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67.89 10.50 10 -10 5 72.59 7.90 -8 10 -7 38.90 8.40 8 10 7 34.40 6.50 -8 10 -7 40.50 7.80 8 -10 7 29.70 7.60 -8 -10 -7 38.40 9.10 8 -10 7 38.50 6.30 6 10 9 32.10 6.40 -6 10 -9 38.70 7.20 -6 -10 -9 51.29 9.00 6 -10 9 39.80 6.40 6 -10 9 53.29 6.70 6 -10 9 39.90 7.50 6 -10 9 36.70 7.30 -4 10 -11 131.59 11.00 4 10 11 128.29 7.50 -4 10 -11 112.69 11.60 4 10 11 133.99 11.10 4 -10 11 117.09 10.80 4 -10 11 155.38 11.20 4 -10 11 127.59 10.40 -4 -10 -11 131.89 12.90 4 -10 11 133.99 8.90 -2 10 -13 36.00 6.80 2 10 13 25.50 6.30 -2 10 -13 14.20 8.20 2 10 13 27.90 4.60 2 10 13 30.10 7.00 2 -10 13 19.20 6.30 2 -10 13 23.50 4.50 2 -10 13 11.30 5.40 2 -10 13 29.40 6.90 -2 -10 -13 22.60 7.20 0 10 -15 168.38 11.50 0 10 -15 155.78 14.80 0 10 15 131.29 12.40 0 10 15 138.39 12.00 0 -10 15 152.38 11.10 0 -10 -15 153.88 12.70 0 -10 15 156.38 11.40 0 -10 -15 150.08 14.30 0 -10 15 134.49 11.70 -2 10 17 366.46 19.10 2 10 -17 321.67 15.90 2 10 -17 304.07 21.30 -2 10 17 313.47 18.80 -2 -10 17 359.46 18.90 -2 -10 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11.70 0 14 15 40.40 9.50 0 14 -15 50.89 9.30 0 -14 15 35.90 9.50 0 -14 -15 50.89 11.80 0 -14 15 47.00 8.10 0 -14 15 68.29 9.30 2 14 -17 119.09 14.80 -2 14 17 131.79 13.90 2 14 -17 113.89 12.10 2 -14 -17 104.79 15.50 2 -14 -17 108.49 10.70 -2 -14 17 113.79 11.30 -2 -14 17 115.59 12.10 -5 15 -10 10.60 6.90 5 15 10 -0.10 7.40 -5 15 -10 3.10 6.40 5 -15 10 17.90 8.10 -5 -15 -10 2.80 7.50 5 -15 10 13.20 7.80 5 -15 10 7.70 5.80 3 15 12 9.50 8.00 -3 15 -12 -6.20 6.90 3 -15 12 3.60 6.90 3 -15 12 -0.40 5.40 3 -15 12 7.80 6.80 3 -15 12 9.70 7.10 -3 -15 -12 -1.10 7.50 -1 15 -14 61.89 10.60 -1 15 -14 64.39 10.70 1 15 14 56.79 10.30 1 -15 14 71.99 10.00 1 -15 14 63.69 10.50 1 -15 14 63.19 9.90 -1 -15 -14 51.09 12.10 1 15 -16 72.99 10.90 -1 15 16 79.79 10.90 1 15 -16 107.19 13.80 1 -15 -16 73.19 14.60 -1 -15 16 59.59 9.60 -1 -15 16 69.79 9.90 1 -15 -16 84.59 10.00 -1 -15 16 76.79 12.10 -4 16 -11 -6.00 5.90 4 16 11 6.10 7.90 -4 16 -11 -3.20 7.00 4 -16 11 -0.60 7.70 -4 -16 -11 1.60 8.10 4 -16 11 7.60 5.60 4 -16 11 2.10 6.50 -2 16 -13 21.80 9.10 2 16 13 20.40 9.00 -2 -16 -13 20.30 9.70 2 -16 13 43.50 9.10 2 -16 13 39.30 9.50 2 -16 13 42.20 8.80 12 0 4 93.19 11.50 12 0 4 81.99 5.90 12 0 4 116.49 12.40 10 0 6 115.59 11.10 10 0 6 129.19 11.80 -10 0 -6 124.19 9.30 8 0 8 23.40 5.20 8 0 8 33.80 5.90 8 0 8 17.90 5.60 8 0 8 25.60 5.40 6 0 10 2.70 3.90 -6 0 -10 2.70 3.70 6 0 10 -1.00 3.30 6 0 10 -0.70 1.70 6 0 10 0.40 1.60 -4 0 -12 1997.70 48.90 4 0 12 1910.31 49.10 4 0 12 1925.21 48.40 4 0 12 1957.50 49.40 4 0 12 1883.81 52.09 4 0 12 2028.50 48.70 -4 0 -12 1962.50 52.39 -4 0 -12 1883.61 48.60 4 0 12 1997.90 49.99 -4 0 -12 1973.00 55.09 2 0 14 1978.60 51.09 2 0 14 2048.20 51.89 -2 0 -14 1912.61 51.79 -2 0 -14 1959.40 54.19 -2 0 -14 2019.50 52.19 2 0 14 2024.70 53.09 2 0 14 2014.80 51.89 -2 0 -14 2109.29 57.19 2 0 14 2108.39 52.99 0 0 -16 270.77 14.60 0 0 -16 238.58 14.50 0 0 16 235.78 11.40 0 0 16 261.87 10.10 0 0 -16 243.58 11.40 0 0 16 251.97 11.30 0 0 -16 242.98 11.60 0 0 16 248.68 12.60 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18.70 7 3 18 212.88 12.60 7 3 18 245.58 15.10 7 -3 18 213.48 12.20 -7 -3 -18 220.38 19.60 7 -3 18 211.78 15.60 -7 -3 -18 232.88 17.00 -5 3 -20 48.90 10.70 5 3 20 40.10 8.30 5 3 20 27.10 6.90 -5 -3 -20 36.80 10.30 5 -3 20 40.60 7.20 5 -3 20 28.10 8.20 -5 -3 -20 51.29 9.90 3 3 22 69.79 9.40 3 3 22 75.59 10.10 -3 3 -22 58.89 12.20 3 -3 22 70.69 9.80 3 -3 22 75.19 10.30 -3 -3 -22 52.79 12.10 -3 -3 -22 64.49 12.30 1 3 24 -2.60 5.40 1 3 24 6.60 7.00 -1 3 -24 -9.60 8.90 -1 -3 -24 -2.40 7.90 -1 -3 -24 -3.60 8.80 1 -3 24 -2.90 5.80 1 -3 24 3.90 7.00 6 4 19 84.79 9.20 -6 4 -19 92.79 11.40 6 4 19 83.79 9.90 -6 4 -19 94.59 12.80 -6 -4 -19 82.79 11.80 6 -4 19 79.59 10.90 -6 -4 -19 107.49 14.40 6 -4 19 88.39 9.50 6 -4 19 92.09 9.10 -4 4 -21 73.19 10.40 -4 4 -21 98.69 13.80 4 4 21 69.69 9.30 4 4 21 88.19 10.20 4 -4 21 76.69 9.50 -4 -4 -21 55.69 12.00 -4 -4 -21 66.09 11.60 4 -4 21 70.99 8.30 4 -4 21 79.49 10.60 2 4 23 153.98 14.00 -2 4 -23 147.39 17.40 -2 4 -23 149.49 13.30 2 4 23 155.98 12.50 -2 -4 -23 119.79 14.90 -2 -4 -23 152.78 16.20 2 -4 23 131.49 13.00 2 -4 23 145.39 11.50 2 -4 23 172.18 14.40 -5 5 -20 37.70 10.50 -5 5 -20 27.30 8.30 5 5 20 44.70 7.90 -5 -5 -20 44.60 10.90 5 -5 20 33.40 7.20 5 -5 20 43.70 7.80 -5 -5 -20 37.30 10.30 5 -5 20 48.90 9.30 -3 5 -22 128.69 12.80 3 5 22 137.29 13.00 3 5 22 110.39 11.10 -3 5 -22 114.39 15.70 3 -5 22 113.99 12.60 -3 -5 -22 121.39 15.70 3 -5 22 120.89 11.00 -3 -5 -22 146.49 16.30 3 -5 22 131.49 12.50 -4 6 -21 1.70 9.10 4 6 21 16.70 7.20 -4 6 -21 -10.50 5.90 4 6 21 12.10 6.20 -4 -6 -21 -8.90 8.50 -4 -6 -21 18.90 9.30 4 -6 21 1.40 5.80 4 -6 21 5.80 6.30 4 -6 21 14.90 7.50 6 0 20 7.70 7.00 -6 0 -20 5.20 8.50 6 0 20 3.00 5.20 4 0 22 48.60 8.30 4 0 22 51.59 9.40 -4 0 -22 64.39 11.90 -2 0 -24 95.29 14.60 2 0 24 97.49 11.70 2 0 24 59.69 9.60 5 1 21 6.20 6.50 -5 1 -21 13.40 9.20 5 1 21 14.90 5.90 5 -1 21 7.40 5.70 5 -1 21 8.40 6.90 -5 -1 -21 12.60 9.00 -5 -1 -21 -6.00 8.60 3 1 23 38.50 8.10 -3 1 -23 31.80 10.30 3 1 23 25.20 7.40 -3 -1 -23 19.20 9.50 -3 -1 -23 -12.70 8.70 3 -1 23 25.30 8.10 3 -1 23 25.30 7.60 -6 2 -20 390.76 23.40 6 2 20 350.06 16.80 6 2 20 365.46 18.60 -6 -2 -20 335.27 20.40 -6 -2 -20 394.26 23.80 6 -2 20 386.86 17.00 6 -2 20 336.37 19.40 4 2 22 7.90 6.20 -4 2 -22 7.90 8.30 4 -2 22 -3.50 6.30 -4 -2 -22 -14.20 8.10 -4 -2 -22 0.00 8.10 4 -2 22 7.40 6.10 -2 2 -24 40.70 11.80 2 2 24 55.09 8.60 2 2 24 43.20 9.40 -2 -2 -24 25.80 10.80 -2 -2 -24 59.59 12.40 2 -2 24 50.89 9.70 -5 3 -21 84.99 13.40 5 3 21 68.99 10.30 5 3 21 87.79 9.70 5 -3 21 88.09 9.60 -5 -3 -21 68.39 11.90 5 -3 21 93.89 12.10 -5 -3 -21 97.79 14.40 -3 3 -23 -7.00 8.10 3 3 23 4.90 6.60 3 3 23 2.50 5.90 3 -3 23 -0.60 6.20 -3 -3 -23 9.00 8.50 3 -3 23 11.60 6.80 -3 -3 -23 2.10 9.70 -4 4 -22 6.70 9.00 -4 4 -22 6.30 6.60 4 4 22 8.70 6.50 4 4 22 11.00 6.80 -4 -4 -22 -13.10 8.30 4 -4 22 4.60 7.00 -4 -4 -22 2.50 7.70 4 -4 22 6.70 6.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 98387 _olex2_submission_special_instructions 'No special instructions were received' _shelx_SHELXL_version_number 2018/3