data_cu_molan506b_0m_a_sq _audit_creation_method 'SHELXL-2018/1' _shelx_SHELXL_version_number '2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C40 H30 F4 Fe N8' _chemical_formula_weight 754.57 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.7043(4) _cell_length_b 13.6484(6) _cell_length_c 14.3016(6) _cell_angle_alpha 81.388(3) _cell_angle_beta 78.691(2) _cell_angle_gamma 81.445(2) _cell_volume 2010.33(15) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9985 _cell_measurement_theta_min 3.18 _cell_measurement_theta_max 65.34 _exptl_crystal_description plate _exptl_crystal_colour red _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.247 _exptl_crystal_F_000 776 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.07 _exptl_absorpt_coefficient_mu 3.481 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.5371 _exptl_absorpt_correction_T_max 0.7526 _exptl_absorpt_process_details 'SADABS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 25255 _diffrn_reflns_av_unetI/netI 0.0506 _diffrn_reflns_av_R_equivalents 0.0594 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.176 _diffrn_reflns_theta_max 65.370 _diffrn_reflns_theta_full 65.370 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measured_fraction_theta_full 0.982 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_Laue_measured_fraction_full 0.982 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_point_group_measured_fraction_full 0.982 _reflns_number_total 6777 _reflns_number_gt 5820 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0215P)^2^+3.4680P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 6777 _refine_ls_number_parameters 480 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0604 _refine_ls_R_factor_gt 0.0497 _refine_ls_wR_factor_ref 0.1132 _refine_ls_wR_factor_gt 0.1081 _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_restrained_S_all 1.051 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.22358(4) 0.24011(3) 0.41466(3) 0.01840(13) Uani 1 1 d . . . . . F1 F -0.23679(18) 0.06007(14) 0.72581(12) 0.0343(4) Uani 1 1 d . . . . . C1 C 0.0053(3) 0.1461(2) 0.4769(2) 0.0187(6) Uani 1 1 d . . . . . N1 N 0.0906(2) 0.18318(17) 0.39309(16) 0.0186(5) Uani 1 1 d . . . . . C2 C 0.0545(3) 0.0968(2) 0.5560(2) 0.0211(6) Uani 1 1 d . . . . . H2 H 0.144835 0.082767 0.552017 0.025 Uiso 1 1 calc R U . . . N2 N 0.0596(2) 0.16657(17) 0.31164(16) 0.0202(5) Uani 1 1 d . . . . . F2 F 0.7576(2) 0.40261(17) 0.20246(15) 0.0501(6) Uani 1 1 d . . . . . F3 F -0.35471(17) 0.47447(14) 0.50915(14) 0.0349(4) Uani 1 1 d . . . . . C3 C -0.0254(3) 0.0675(2) 0.6406(2) 0.0238(7) Uani 1 1 d . . . . . H3 H 0.008250 0.034092 0.695230 0.029 Uiso 1 1 calc R U . . . N3 N 0.2399(2) 0.24250(18) 0.21168(16) 0.0209(5) Uani 1 1 d . . . . . F4 F 0.73563(17) -0.05784(14) 0.26872(13) 0.0362(5) Uani 1 1 d . . . . . C4 C -0.1565(3) 0.0887(2) 0.6429(2) 0.0243(7) Uani 1 1 d . . . . . N4 N 0.2865(2) 0.25976(18) 0.28645(17) 0.0217(5) Uani 1 1 d . . . . . N6 N 0.1955(2) 0.32817(17) 0.58855(16) 0.0200(5) Uani 1 1 d . . . . . C6 C -0.1269(3) 0.1659(2) 0.4820(2) 0.0220(6) Uani 1 1 d . . . . . H6 H -0.161107 0.199769 0.427776 0.026 Uiso 1 1 calc R U . . . N5 N 0.1495(2) 0.31131(18) 0.51397(17) 0.0197(5) Uani 1 1 d . . . . . C5 C -0.2087(3) 0.1366(2) 0.5658(2) 0.0250(7) Uani 1 1 d . . . . . H5 H -0.299136 0.149424 0.569781 0.030 Uiso 1 1 calc R U . . . N7 N 0.3974(2) 0.22300(18) 0.54709(17) 0.0212(5) Uani 1 1 d . . . . . C7 C 0.1329(3) 0.1973(2) 0.2281(2) 0.0211(6) Uani 1 1 d . . . . . N8 N 0.3664(2) 0.20189(17) 0.46731(17) 0.0210(5) Uani 1 1 d . . . . . C8 C 0.0895(3) 0.1785(2) 0.1400(2) 0.0225(6) Uani 1 1 d . . . . . C9 C -0.0349(3) 0.1619(3) 0.1426(2) 0.0422(9) Uani 1 1 d . . . . . H9 H -0.094523 0.163519 0.201228 0.051 Uiso 1 1 calc R U . . . C11 C 0.0100(4) 0.1414(3) -0.0266(2) 0.0445(10) Uani 1 1 d . . . . . C10 C -0.0747(4) 0.1430(4) 0.0613(3) 0.0578(13) Uani 1 1 d . . . . . H10 H -0.160833 0.130890 0.065264 0.069 Uiso 1 1 calc R U . . . C12 C 0.1346(3) 0.1580(3) -0.0284(2) 0.0339(8) Uani 1 1 d . . . . . H12 H 0.194535 0.156522 -0.086931 0.041 Uiso 1 1 calc R U . . . C13 C 0.1741(3) 0.1767(2) 0.0529(2) 0.0303(7) Uani 1 1 d . . . . . H13 H 0.260311 0.188431 0.049200 0.036 Uiso 1 1 calc R U . . . C15 C 0.4049(3) 0.3033(2) 0.2574(2) 0.0230(6) Uani 1 1 d . . . . . C14 C -0.0341(5) 0.1217(4) -0.1154(3) 0.0694(15) Uani 1 1 d . . . . . H14A H 0.019019 0.152764 -0.172748 0.104 Uiso 1 1 calc R U . . . H14B H -0.124074 0.150109 -0.113672 0.104 Uiso 1 1 calc R U . . . H14C H -0.025916 0.049558 -0.117353 0.104 Uiso 1 1 calc R U . . . C16 C 0.5005(3) 0.2659(2) 0.1861(2) 0.0287(7) Uani 1 1 d . . . . . H16 H 0.484451 0.216789 0.150841 0.034 Uiso 1 1 calc R U . . . C17 C 0.6186(3) 0.3006(3) 0.1671(2) 0.0336(8) Uani 1 1 d . . . . . H17 H 0.684492 0.275857 0.118509 0.040 Uiso 1 1 calc R U . . . C19 C 0.5461(3) 0.4119(2) 0.2890(2) 0.0335(8) Uani 1 1 d . . . . . H19 H 0.562241 0.462144 0.322852 0.040 Uiso 1 1 calc R U . . . C18 C 0.6400(3) 0.3714(3) 0.2193(2) 0.0353(8) Uani 1 1 d . . . . . C20 C 0.4276(3) 0.3766(2) 0.3079(2) 0.0258(7) Uani 1 1 d . . . . . H20 H 0.361432 0.402582 0.355665 0.031 Uiso 1 1 calc R U . . . C21 C 0.0204(3) 0.3597(2) 0.5145(2) 0.0198(6) Uani 1 1 d . . . . . C22 C -0.0679(3) 0.3623(2) 0.6002(2) 0.0233(6) Uani 1 1 d . . . . . H22 H -0.041239 0.337202 0.659796 0.028 Uiso 1 1 calc R U . . . C23 C -0.1943(3) 0.4015(2) 0.5982(2) 0.0263(7) Uani 1 1 d . . . . . H23 H -0.255264 0.403988 0.656069 0.032 Uiso 1 1 calc R U . . . C24 C -0.2303(3) 0.4366(2) 0.5112(2) 0.0254(7) Uani 1 1 d . . . . . C25 C -0.1450(3) 0.4369(2) 0.4250(2) 0.0247(7) Uani 1 1 d . . . . . H25 H -0.172387 0.462695 0.365887 0.030 Uiso 1 1 calc R U . . . C26 C -0.0181(3) 0.3983(2) 0.4277(2) 0.0216(6) Uani 1 1 d . . . . . H26 H 0.042966 0.398273 0.369741 0.026 Uiso 1 1 calc R U . . . C27 C 0.3133(3) 0.2848(2) 0.6008(2) 0.0216(6) Uani 1 1 d . . . . . C29 C 0.2639(3) 0.3419(2) 0.7636(2) 0.0299(7) Uani 1 1 d . . . . . H29 H 0.175590 0.353851 0.758658 0.036 Uiso 1 1 calc R U . . . C30 C 0.3028(3) 0.3598(3) 0.8456(2) 0.0364(8) Uani 1 1 d . . . . . H30 H 0.239938 0.383326 0.896632 0.044 Uiso 1 1 calc R U . . . C31 C 0.4307(4) 0.3444(3) 0.8553(2) 0.0367(9) Uani 1 1 d . . . . . C32 C 0.5204(3) 0.3100(3) 0.7796(2) 0.0349(8) Uani 1 1 d . . . . . H32 H 0.608715 0.298866 0.784518 0.042 Uiso 1 1 calc R U . . . C33 C 0.4832(3) 0.2916(2) 0.6970(2) 0.0296(7) Uani 1 1 d . . . . . H33 H 0.546406 0.268720 0.645872 0.036 Uiso 1 1 calc R U . . . C34 C 0.4721(4) 0.3664(3) 0.9443(3) 0.0546(12) Uani 1 1 d . . . . . H34A H 0.553933 0.325938 0.952036 0.082 Uiso 1 1 calc R U . . . H34B H 0.406712 0.350203 1.000696 0.082 Uiso 1 1 calc R U . . . H34C H 0.482512 0.437377 0.937951 0.082 Uiso 1 1 calc R U . . . C35 C 0.4644(3) 0.1326(2) 0.41930(19) 0.0192(6) Uani 1 1 d . . . . . C36 C 0.4276(3) 0.0539(2) 0.3836(2) 0.0225(6) Uani 1 1 d . . . . . H36 H 0.339444 0.044692 0.394184 0.027 Uiso 1 1 calc R U . . . C37 C 0.5189(3) -0.0113(2) 0.3326(2) 0.0258(7) Uani 1 1 d . . . . . H37 H 0.494677 -0.065375 0.308312 0.031 Uiso 1 1 calc R U . . . C38 C 0.6446(3) 0.0051(2) 0.3187(2) 0.0263(7) Uani 1 1 d . . . . . C39 C 0.6843(3) 0.0822(2) 0.3527(2) 0.0271(7) Uani 1 1 d . . . . . H39 H 0.772645 0.091072 0.341680 0.032 Uiso 1 1 calc R U . . . C40 C 0.5924(3) 0.1469(2) 0.4037(2) 0.0227(6) Uani 1 1 d . . . . . H40 H 0.617417 0.200842 0.427685 0.027 Uiso 1 1 calc R U . . . C28 C 0.3545(3) 0.3063(2) 0.6880(2) 0.0230(7) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0207(2) 0.0215(3) 0.0160(2) -0.00145(18) -0.00825(17) -0.00672(18) F1 0.0373(11) 0.0432(12) 0.0218(9) -0.0002(8) 0.0010(8) -0.0149(9) C1 0.0255(16) 0.0170(14) 0.0168(14) -0.0034(11) -0.0048(11) -0.0101(11) N1 0.0208(13) 0.0217(13) 0.0158(12) -0.0007(10) -0.0098(9) -0.0034(10) C2 0.0249(16) 0.0199(15) 0.0202(15) -0.0019(12) -0.0074(12) -0.0043(12) N2 0.0283(14) 0.0194(13) 0.0152(12) 0.0003(10) -0.0085(10) -0.0067(10) F2 0.0450(13) 0.0685(15) 0.0434(12) -0.0052(11) 0.0000(10) -0.0404(11) F3 0.0231(10) 0.0405(11) 0.0429(11) -0.0080(9) -0.0119(8) 0.0006(8) C3 0.0349(18) 0.0232(16) 0.0167(15) -0.0008(12) -0.0094(13) -0.0098(13) N3 0.0285(14) 0.0227(13) 0.0141(12) 0.0001(10) -0.0092(10) -0.0065(10) F4 0.0301(10) 0.0386(11) 0.0385(11) -0.0109(9) -0.0013(8) -0.0005(8) C4 0.0318(17) 0.0245(16) 0.0188(15) -0.0019(12) -0.0028(12) -0.0140(13) N4 0.0227(13) 0.0222(13) 0.0227(13) -0.0009(10) -0.0089(10) -0.0067(10) N6 0.0246(13) 0.0218(13) 0.0175(12) 0.0007(10) -0.0112(10) -0.0090(10) C6 0.0261(16) 0.0194(15) 0.0241(16) -0.0008(12) -0.0108(12) -0.0084(12) N5 0.0193(13) 0.0222(13) 0.0200(12) -0.0008(10) -0.0074(10) -0.0073(10) C5 0.0261(16) 0.0235(17) 0.0275(17) -0.0033(13) -0.0052(13) -0.0091(13) N7 0.0286(14) 0.0205(13) 0.0188(13) -0.0002(10) -0.0117(10) -0.0097(10) C7 0.0292(16) 0.0183(15) 0.0178(15) -0.0007(12) -0.0079(12) -0.0062(12) N8 0.0268(14) 0.0196(13) 0.0191(13) -0.0023(10) -0.0045(10) -0.0099(10) C8 0.0319(17) 0.0236(16) 0.0156(15) -0.0010(12) -0.0091(12) -0.0102(13) C9 0.040(2) 0.074(3) 0.0189(17) -0.0107(17) -0.0019(14) -0.0254(19) C11 0.054(2) 0.067(3) 0.0201(18) -0.0114(17) -0.0136(16) -0.016(2) C10 0.047(2) 0.111(4) 0.029(2) -0.021(2) -0.0090(17) -0.038(2) C12 0.041(2) 0.044(2) 0.0195(17) -0.0062(14) -0.0065(14) -0.0111(16) C13 0.0335(18) 0.0376(19) 0.0224(16) -0.0045(14) -0.0072(13) -0.0086(14) C15 0.0274(17) 0.0236(16) 0.0195(15) 0.0054(12) -0.0085(12) -0.0109(12) C14 0.066(3) 0.126(5) 0.029(2) -0.027(2) -0.016(2) -0.025(3) C16 0.0377(19) 0.0337(19) 0.0168(15) 0.0004(13) -0.0043(13) -0.0158(14) C17 0.0372(19) 0.047(2) 0.0187(16) -0.0006(14) -0.0004(13) -0.0212(16) C19 0.046(2) 0.0300(19) 0.0304(18) -0.0003(14) -0.0103(15) -0.0222(15) C18 0.040(2) 0.044(2) 0.0264(18) 0.0042(15) -0.0066(15) -0.0259(16) C20 0.0324(18) 0.0255(17) 0.0221(16) -0.0006(13) -0.0077(13) -0.0109(13) C21 0.0262(16) 0.0141(14) 0.0216(15) -0.0035(11) -0.0060(12) -0.0073(11) C22 0.0314(17) 0.0204(16) 0.0213(15) -0.0051(12) -0.0085(13) -0.0065(12) C23 0.0293(17) 0.0268(17) 0.0245(16) -0.0062(13) -0.0052(13) -0.0054(13) C24 0.0220(16) 0.0233(16) 0.0341(18) -0.0054(13) -0.0106(13) -0.0042(12) C25 0.0264(17) 0.0250(17) 0.0260(16) -0.0018(13) -0.0120(13) -0.0049(12) C26 0.0254(16) 0.0213(16) 0.0208(15) -0.0018(12) -0.0073(12) -0.0086(12) C27 0.0261(16) 0.0188(15) 0.0225(15) 0.0002(12) -0.0076(12) -0.0091(12) C29 0.0313(18) 0.040(2) 0.0217(16) 0.0008(14) -0.0092(13) -0.0155(15) C30 0.044(2) 0.050(2) 0.0210(17) 0.0003(15) -0.0119(15) -0.0211(17) C31 0.055(2) 0.043(2) 0.0195(17) 0.0052(15) -0.0188(16) -0.0248(17) C32 0.039(2) 0.039(2) 0.0348(19) 0.0034(15) -0.0249(16) -0.0132(15) C33 0.0319(18) 0.0308(18) 0.0306(18) -0.0043(14) -0.0141(14) -0.0061(14) C34 0.069(3) 0.077(3) 0.030(2) -0.002(2) -0.027(2) -0.030(2) C35 0.0237(16) 0.0187(15) 0.0160(14) 0.0028(11) -0.0082(11) -0.0043(11) C36 0.0230(16) 0.0216(16) 0.0249(16) -0.0008(12) -0.0079(12) -0.0062(12) C37 0.0313(18) 0.0218(16) 0.0274(17) -0.0012(13) -0.0108(13) -0.0073(13) C38 0.0280(17) 0.0268(17) 0.0232(16) -0.0005(13) -0.0059(13) -0.0014(13) C39 0.0250(17) 0.0338(18) 0.0234(16) 0.0029(13) -0.0067(13) -0.0104(13) C40 0.0242(16) 0.0244(16) 0.0219(15) 0.0004(12) -0.0096(12) -0.0064(12) C28 0.0332(17) 0.0192(16) 0.0210(15) 0.0040(12) -0.0152(13) -0.0104(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N8 1.809(2) . ? Fe1 N1 1.816(2) . ? Fe1 N4 1.819(2) . ? Fe1 N5 1.826(2) . ? F1 C4 1.363(3) . ? C1 C2 1.382(4) . ? C1 C6 1.389(4) . ? C1 N1 1.433(4) . ? N1 N2 1.331(3) . ? C2 C3 1.381(4) . ? C2 H2 0.9500 . ? N2 C7 1.341(4) . ? F2 C18 1.353(4) . ? F3 C24 1.359(3) . ? C3 C4 1.384(4) . ? C3 H3 0.9500 . ? N3 N4 1.330(3) . ? N3 C7 1.345(4) . ? F4 C38 1.363(4) . ? C4 C5 1.368(4) . ? N4 C15 1.440(4) . ? N6 N5 1.322(3) . ? N6 C27 1.343(4) . ? C6 C5 1.383(4) . ? C6 H6 0.9500 . ? N5 C21 1.440(4) . ? C5 H5 0.9500 . ? N7 N8 1.331(3) . ? N7 C27 1.345(4) . ? C7 C8 1.494(4) . ? N8 C35 1.443(4) . ? C8 C9 1.376(4) . ? C8 C13 1.391(4) . ? C9 C10 1.385(5) . ? C9 H9 0.9500 . ? C11 C12 1.380(5) . ? C11 C10 1.399(5) . ? C11 C14 1.512(5) . ? C10 H10 0.9500 . ? C12 C13 1.382(4) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C15 C16 1.392(4) . ? C15 C20 1.393(4) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C16 C17 1.379(4) . ? C16 H16 0.9500 . ? C17 C18 1.376(5) . ? C17 H17 0.9500 . ? C19 C18 1.384(5) . ? C19 C20 1.386(4) . ? C19 H19 0.9500 . ? C20 H20 0.9500 . ? C21 C26 1.388(4) . ? C21 C22 1.395(4) . ? C22 C23 1.384(4) . ? C22 H22 0.9500 . ? C23 C24 1.371(4) . ? C23 H23 0.9500 . ? C24 C25 1.382(4) . ? C25 C26 1.388(4) . ? C25 H25 0.9500 . ? C26 H26 0.9500 . ? C27 C28 1.484(4) . ? C29 C30 1.384(4) . ? C29 C28 1.396(4) . ? C29 H29 0.9500 . ? C30 C31 1.385(5) . ? C30 H30 0.9500 . ? C31 C32 1.387(5) . ? C31 C34 1.511(4) . ? C32 C33 1.386(4) . ? C32 H32 0.9500 . ? C33 C28 1.391(4) . ? C33 H33 0.9500 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 C40 1.383(4) . ? C35 C36 1.392(4) . ? C36 C37 1.391(4) . ? C36 H36 0.9500 . ? C37 C38 1.368(4) . ? C37 H37 0.9500 . ? C38 C39 1.377(4) . ? C39 C40 1.390(4) . ? C39 H39 0.9500 . ? C40 H40 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N8 Fe1 N1 137.84(10) . . ? N8 Fe1 N4 103.33(11) . . ? N1 Fe1 N4 91.11(10) . . ? N8 Fe1 N5 91.05(11) . . ? N1 Fe1 N5 102.84(10) . . ? N4 Fe1 N5 140.13(11) . . ? C2 C1 C6 119.6(3) . . ? C2 C1 N1 119.7(3) . . ? C6 C1 N1 120.5(2) . . ? N2 N1 C1 112.9(2) . . ? N2 N1 Fe1 131.00(18) . . ? C1 N1 Fe1 116.04(17) . . ? C3 C2 C1 121.2(3) . . ? C3 C2 H2 119.4 . . ? C1 C2 H2 119.4 . . ? N1 N2 C7 118.6(2) . . ? C2 C3 C4 117.5(3) . . ? C2 C3 H3 121.3 . . ? C4 C3 H3 121.3 . . ? N4 N3 C7 118.7(2) . . ? F1 C4 C5 118.7(3) . . ? F1 C4 C3 118.3(3) . . ? C5 C4 C3 123.0(3) . . ? N3 N4 C15 112.1(2) . . ? N3 N4 Fe1 130.71(19) . . ? C15 N4 Fe1 117.13(19) . . ? N5 N6 C27 119.1(2) . . ? C5 C6 C1 120.2(3) . . ? C5 C6 H6 119.9 . . ? C1 C6 H6 119.9 . . ? N6 N5 C21 111.7(2) . . ? N6 N5 Fe1 130.51(19) . . ? C21 N5 Fe1 117.80(18) . . ? C4 C5 C6 118.6(3) . . ? C4 C5 H5 120.7 . . ? C6 C5 H5 120.7 . . ? N8 N7 C27 118.3(2) . . ? N2 C7 N3 129.7(3) . . ? N2 C7 C8 115.3(2) . . ? N3 C7 C8 115.0(2) . . ? N7 N8 C35 111.7(2) . . ? N7 N8 Fe1 131.3(2) . . ? C35 N8 Fe1 116.86(18) . . ? C9 C8 C13 118.0(3) . . ? C9 C8 C7 121.2(3) . . ? C13 C8 C7 120.9(3) . . ? C8 C9 C10 121.2(3) . . ? C8 C9 H9 119.4 . . ? C10 C9 H9 119.4 . . ? C12 C11 C10 117.4(3) . . ? C12 C11 C14 121.7(3) . . ? C10 C11 C14 120.8(4) . . ? C9 C10 C11 121.0(3) . . ? C9 C10 H10 119.5 . . ? C11 C10 H10 119.5 . . ? C11 C12 C13 121.5(3) . . ? C11 C12 H12 119.3 . . ? C13 C12 H12 119.3 . . ? C12 C13 C8 121.0(3) . . ? C12 C13 H13 119.5 . . ? C8 C13 H13 119.5 . . ? C16 C15 C20 120.2(3) . . ? C16 C15 N4 120.5(3) . . ? C20 C15 N4 119.1(3) . . ? C11 C14 H14A 109.5 . . ? C11 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C11 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C17 C16 C15 119.5(3) . . ? C17 C16 H16 120.2 . . ? C15 C16 H16 120.2 . . ? C18 C17 C16 119.3(3) . . ? C18 C17 H17 120.3 . . ? C16 C17 H17 120.3 . . ? C18 C19 C20 117.8(3) . . ? C18 C19 H19 121.1 . . ? C20 C19 H19 121.1 . . ? F2 C18 C17 118.9(3) . . ? F2 C18 C19 118.5(3) . . ? C17 C18 C19 122.5(3) . . ? C19 C20 C15 120.5(3) . . ? C19 C20 H20 119.7 . . ? C15 C20 H20 119.7 . . ? C26 C21 C22 120.1(3) . . ? C26 C21 N5 119.1(3) . . ? C22 C21 N5 120.7(3) . . ? C23 C22 C21 119.7(3) . . ? C23 C22 H22 120.2 . . ? C21 C22 H22 120.2 . . ? C24 C23 C22 118.9(3) . . ? C24 C23 H23 120.5 . . ? C22 C23 H23 120.5 . . ? F3 C24 C23 118.9(3) . . ? F3 C24 C25 118.2(3) . . ? C23 C24 C25 122.9(3) . . ? C24 C25 C26 117.8(3) . . ? C24 C25 H25 121.1 . . ? C26 C25 H25 121.1 . . ? C21 C26 C25 120.5(3) . . ? C21 C26 H26 119.7 . . ? C25 C26 H26 119.7 . . ? N6 C27 N7 129.5(3) . . ? N6 C27 C28 114.8(3) . . ? N7 C27 C28 115.6(3) . . ? C30 C29 C28 120.0(3) . . ? C30 C29 H29 120.0 . . ? C28 C29 H29 120.0 . . ? C29 C30 C31 121.9(3) . . ? C29 C30 H30 119.1 . . ? C31 C30 H30 119.1 . . ? C30 C31 C32 117.8(3) . . ? C30 C31 C34 121.3(4) . . ? C32 C31 C34 120.8(3) . . ? C33 C32 C31 121.1(3) . . ? C33 C32 H32 119.5 . . ? C31 C32 H32 119.5 . . ? C32 C33 C28 120.8(3) . . ? C32 C33 H33 119.6 . . ? C28 C33 H33 119.6 . . ? C31 C34 H34A 109.5 . . ? C31 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? C31 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C40 C35 C36 120.1(3) . . ? C40 C35 N8 120.9(3) . . ? C36 C35 N8 118.9(2) . . ? C37 C36 C35 120.5(3) . . ? C37 C36 H36 119.8 . . ? C35 C36 H36 119.8 . . ? C38 C37 C36 117.8(3) . . ? C38 C37 H37 121.1 . . ? C36 C37 H37 121.1 . . ? F4 C38 C37 118.8(3) . . ? F4 C38 C39 118.0(3) . . ? C37 C38 C39 123.2(3) . . ? C38 C39 C40 118.5(3) . . ? C38 C39 H39 120.7 . . ? C40 C39 H39 120.7 . . ? C35 C40 C39 119.9(3) . . ? C35 C40 H40 120.1 . . ? C39 C40 H40 120.1 . . ? C33 C28 C29 118.3(3) . . ? C33 C28 C27 121.3(3) . . ? C29 C28 C27 120.4(3) . . ? _refine_diff_density_max 0.366 _refine_diff_density_min -0.506 _refine_diff_density_rms 0.060 _shelx_res_file ; TITL cu_molan506b_0m_a.res in P-1 cu_molan506b_0m_a_sq.res created by SHELXL-2018/1 at 17:37:52 on 26-Apr-2018 REM Old TITL cu_molan506b_0m in P-1 REM SHELXT solution in P-1 REM R1 0.155, Rweak 0.022, Alpha 0.080, Orientation as input REM Formula found by SHELXT: C48 N8 O F3 Fe CELL 1.54178 10.7043 13.6484 14.3016 81.388 78.691 81.445 ZERR 2.000 0.0004 0.0006 0.0006 0.003 0.002 0.002 LATT 1 SFAC C H N F Fe UNIT 80 60 16 8 2 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -173.160 L.S. 5 0 68 BOND $H ACTA FMAP 2 PLAN 20 ABIN WGHT 0.021500 3.468000 FVAR 0.32489 FE1 5 0.223579 0.240111 0.414665 11.00000 0.02074 0.02154 = 0.01600 -0.00145 -0.00825 -0.00672 F1 4 -0.236794 0.060072 0.725809 11.00000 0.03728 0.04321 = 0.02183 -0.00022 0.00103 -0.01492 C1 1 0.005266 0.146057 0.476870 11.00000 0.02547 0.01702 = 0.01679 -0.00343 -0.00478 -0.01013 N1 3 0.090618 0.183182 0.393095 11.00000 0.02083 0.02173 = 0.01578 -0.00070 -0.00980 -0.00337 C2 1 0.054456 0.096769 0.555951 11.00000 0.02487 0.01992 = 0.02022 -0.00189 -0.00740 -0.00434 AFIX 43 H2 2 0.144835 0.082767 0.552017 11.00000 -1.20000 AFIX 0 N2 3 0.059575 0.166570 0.311643 11.00000 0.02828 0.01937 = 0.01524 0.00028 -0.00845 -0.00668 F2 4 0.757554 0.402615 0.202455 11.00000 0.04498 0.06847 = 0.04336 -0.00519 0.00002 -0.04040 F3 4 -0.354708 0.474469 0.509151 11.00000 0.02313 0.04053 = 0.04288 -0.00800 -0.01192 0.00059 C3 1 -0.025443 0.067489 0.640632 11.00000 0.03490 0.02316 = 0.01670 -0.00079 -0.00943 -0.00984 AFIX 43 H3 2 0.008250 0.034092 0.695230 11.00000 -1.20000 AFIX 0 N3 3 0.239884 0.242502 0.211682 11.00000 0.02851 0.02269 = 0.01406 0.00011 -0.00923 -0.00646 F4 4 0.735630 -0.057842 0.268720 11.00000 0.03014 0.03865 = 0.03850 -0.01093 -0.00129 -0.00048 C4 1 -0.156488 0.088671 0.642894 11.00000 0.03185 0.02448 = 0.01879 -0.00185 -0.00280 -0.01402 N4 3 0.286512 0.259762 0.286445 11.00000 0.02273 0.02224 = 0.02271 -0.00092 -0.00891 -0.00670 N6 3 0.195523 0.328173 0.588548 11.00000 0.02460 0.02176 = 0.01754 0.00074 -0.01121 -0.00902 C6 1 -0.126866 0.165936 0.481985 11.00000 0.02610 0.01943 = 0.02414 -0.00080 -0.01084 -0.00838 AFIX 43 H6 2 -0.161107 0.199769 0.427776 11.00000 -1.20000 AFIX 0 N5 3 0.149484 0.311308 0.513971 11.00000 0.01929 0.02216 = 0.02005 -0.00081 -0.00738 -0.00733 C5 1 -0.208676 0.136587 0.565815 11.00000 0.02611 0.02354 = 0.02751 -0.00329 -0.00519 -0.00911 AFIX 43 H5 2 -0.299136 0.149424 0.569781 11.00000 -1.20000 AFIX 0 N7 3 0.397402 0.223004 0.547088 11.00000 0.02859 0.02051 = 0.01881 -0.00016 -0.01166 -0.00969 C7 1 0.132933 0.197275 0.228146 11.00000 0.02922 0.01833 = 0.01783 -0.00065 -0.00794 -0.00625 N8 3 0.366402 0.201890 0.467311 11.00000 0.02675 0.01956 = 0.01911 -0.00229 -0.00452 -0.00995 C8 1 0.089503 0.178539 0.140033 11.00000 0.03193 0.02358 = 0.01557 -0.00096 -0.00913 -0.01022 C9 1 -0.034873 0.161947 0.142602 11.00000 0.03985 0.07370 = 0.01886 -0.01073 -0.00190 -0.02540 AFIX 43 H9 2 -0.094523 0.163519 0.201228 11.00000 -1.20000 AFIX 0 C11 1 0.010022 0.141422 -0.026552 11.00000 0.05351 0.06723 = 0.02011 -0.01140 -0.01361 -0.01575 C10 1 -0.074708 0.142997 0.061312 11.00000 0.04738 0.11101 = 0.02868 -0.02107 -0.00898 -0.03797 AFIX 43 H10 2 -0.160833 0.130890 0.065264 11.00000 -1.20000 AFIX 0 C12 1 0.134593 0.157991 -0.028443 11.00000 0.04120 0.04386 = 0.01953 -0.00616 -0.00646 -0.01106 AFIX 43 H12 2 0.194535 0.156522 -0.086931 11.00000 -1.20000 AFIX 0 C13 1 0.174100 0.176682 0.052889 11.00000 0.03348 0.03760 = 0.02239 -0.00450 -0.00724 -0.00855 AFIX 43 H13 2 0.260311 0.188431 0.049200 11.00000 -1.20000 AFIX 0 C15 1 0.404852 0.303264 0.257386 11.00000 0.02744 0.02357 = 0.01952 0.00537 -0.00846 -0.01087 C14 1 -0.034119 0.121732 -0.115393 11.00000 0.06610 0.12594 = 0.02906 -0.02748 -0.01608 -0.02541 AFIX 137 H14A 2 0.019019 0.152764 -0.172748 11.00000 -1.50000 H14B 2 -0.124074 0.150109 -0.113672 11.00000 -1.50000 H14C 2 -0.025916 0.049558 -0.117353 11.00000 -1.50000 AFIX 0 C16 1 0.500454 0.265881 0.186140 11.00000 0.03765 0.03374 = 0.01681 0.00037 -0.00431 -0.01583 AFIX 43 H16 2 0.484451 0.216789 0.150841 11.00000 -1.20000 AFIX 0 C17 1 0.618584 0.300598 0.167140 11.00000 0.03716 0.04689 = 0.01872 -0.00055 -0.00041 -0.02123 AFIX 43 H17 2 0.684492 0.275857 0.118509 11.00000 -1.20000 AFIX 0 C19 1 0.546065 0.411855 0.289041 11.00000 0.04578 0.03004 = 0.03036 -0.00032 -0.01025 -0.02217 AFIX 43 H19 2 0.562241 0.462144 0.322852 11.00000 -1.20000 AFIX 0 C18 1 0.640030 0.371442 0.219334 11.00000 0.03951 0.04406 = 0.02637 0.00419 -0.00658 -0.02591 C20 1 0.427617 0.376570 0.307906 11.00000 0.03239 0.02555 = 0.02205 -0.00057 -0.00769 -0.01090 AFIX 43 H20 2 0.361432 0.402582 0.355665 11.00000 -1.20000 AFIX 0 C21 1 0.020350 0.359685 0.514470 11.00000 0.02619 0.01410 = 0.02161 -0.00352 -0.00596 -0.00726 C22 1 -0.067856 0.362252 0.600241 11.00000 0.03144 0.02039 = 0.02133 -0.00515 -0.00848 -0.00649 AFIX 43 H22 2 -0.041239 0.337202 0.659796 11.00000 -1.20000 AFIX 0 C23 1 -0.194339 0.401471 0.598156 11.00000 0.02927 0.02684 = 0.02446 -0.00616 -0.00523 -0.00543 AFIX 43 H23 2 -0.255264 0.403988 0.656069 11.00000 -1.20000 AFIX 0 C24 1 -0.230294 0.436624 0.511186 11.00000 0.02199 0.02333 = 0.03410 -0.00536 -0.01064 -0.00417 C25 1 -0.145027 0.436908 0.425033 11.00000 0.02641 0.02497 = 0.02596 -0.00183 -0.01205 -0.00492 AFIX 43 H25 2 -0.172387 0.462695 0.365887 11.00000 -1.20000 AFIX 0 C26 1 -0.018083 0.398281 0.427740 11.00000 0.02544 0.02134 = 0.02080 -0.00183 -0.00726 -0.00861 AFIX 43 H26 2 0.042966 0.398273 0.369741 11.00000 -1.20000 AFIX 0 C27 1 0.313304 0.284807 0.600770 11.00000 0.02613 0.01879 = 0.02246 0.00025 -0.00762 -0.00910 C29 1 0.263939 0.341907 0.763550 11.00000 0.03132 0.04042 = 0.02170 0.00078 -0.00922 -0.01550 AFIX 43 H29 2 0.175590 0.353851 0.758658 11.00000 -1.20000 AFIX 0 C30 1 0.302801 0.359810 0.845560 11.00000 0.04397 0.05021 = 0.02096 0.00032 -0.01186 -0.02109 AFIX 43 H30 2 0.239938 0.383326 0.896632 11.00000 -1.20000 AFIX 0 C31 1 0.430714 0.344427 0.855312 11.00000 0.05526 0.04337 = 0.01947 0.00517 -0.01883 -0.02477 C32 1 0.520356 0.310019 0.779636 11.00000 0.03853 0.03926 = 0.03476 0.00344 -0.02493 -0.01319 AFIX 43 H32 2 0.608715 0.298866 0.784518 11.00000 -1.20000 AFIX 0 C33 1 0.483176 0.291640 0.697025 11.00000 0.03192 0.03075 = 0.03060 -0.00427 -0.01413 -0.00609 AFIX 43 H33 2 0.546406 0.268720 0.645872 11.00000 -1.20000 AFIX 0 C34 1 0.472102 0.366417 0.944313 11.00000 0.06916 0.07726 = 0.03013 -0.00221 -0.02695 -0.02989 AFIX 137 H34A 2 0.553933 0.325938 0.952036 11.00000 -1.50000 H34B 2 0.406712 0.350203 1.000696 11.00000 -1.50000 H34C 2 0.482512 0.437377 0.937951 11.00000 -1.50000 AFIX 0 C35 1 0.464395 0.132582 0.419301 11.00000 0.02375 0.01875 = 0.01596 0.00276 -0.00825 -0.00427 C36 1 0.427578 0.053924 0.383628 11.00000 0.02301 0.02155 = 0.02491 -0.00080 -0.00790 -0.00616 AFIX 43 H36 2 0.339444 0.044692 0.394184 11.00000 -1.20000 AFIX 0 C37 1 0.518857 -0.011268 0.332638 11.00000 0.03128 0.02183 = 0.02738 -0.00123 -0.01077 -0.00733 AFIX 43 H37 2 0.494677 -0.065375 0.308312 11.00000 -1.20000 AFIX 0 C38 1 0.644624 0.005065 0.318651 11.00000 0.02803 0.02684 = 0.02323 -0.00048 -0.00588 -0.00142 C39 1 0.684347 0.082233 0.352732 11.00000 0.02502 0.03381 = 0.02341 0.00293 -0.00666 -0.01039 AFIX 43 H39 2 0.772645 0.091072 0.341680 11.00000 -1.20000 AFIX 0 C40 1 0.592383 0.146897 0.403660 11.00000 0.02415 0.02436 = 0.02194 0.00038 -0.00958 -0.00642 AFIX 43 H40 2 0.617417 0.200842 0.427685 11.00000 -1.20000 AFIX 0 C28 1 0.354468 0.306319 0.688041 11.00000 0.03316 0.01923 = 0.02100 0.00396 -0.01519 -0.01038 HKLF 4 REM cu_molan506b_0m_a.res in P-1 REM R1 = 0.0497 for 5820 Fo > 4sig(Fo) and 0.0604 for all 6777 data REM 480 parameters refined using 0 restraints END WGHT 0.0215 3.4679 REM Highest difference peak 0.366, deepest hole -0.506, 1-sigma level 0.060 Q1 1 -0.2047 0.4011 0.8316 11.00000 0.05 0.37 Q2 1 0.0268 0.4725 0.1657 11.00000 0.05 0.34 Q3 1 0.1692 0.3180 0.4272 11.00000 0.05 0.30 Q4 1 0.2003 0.2150 0.4912 11.00000 0.05 0.30 Q5 1 -0.1167 0.1052 -0.0969 11.00000 0.05 0.28 Q6 1 0.2481 0.2865 0.3458 11.00000 0.05 0.27 Q7 1 0.2013 0.2340 0.3398 11.00000 0.05 0.27 Q8 1 0.0824 0.5234 0.2141 11.00000 0.05 0.27 Q9 1 0.2772 0.1610 0.4218 11.00000 0.05 0.26 Q10 1 0.5407 0.0852 0.0413 11.00000 0.05 0.26 Q11 1 0.0612 0.1823 -0.0364 11.00000 0.05 0.26 Q12 1 0.1079 0.2170 0.0813 11.00000 0.05 0.25 Q13 1 0.1295 0.4476 1.0716 11.00000 0.05 0.25 Q14 1 0.6069 0.3743 0.1594 11.00000 0.05 0.24 Q15 1 -0.0894 0.4286 0.9472 11.00000 0.05 0.24 Q16 1 0.8000 0.4663 0.1446 11.00000 0.05 0.24 Q17 1 0.1731 0.1725 0.4411 11.00000 0.05 0.24 Q18 1 -0.0281 0.3199 0.5416 11.00000 0.05 0.23 Q19 1 0.4864 0.0060 0.0843 11.00000 0.05 0.23 Q20 1 0.1048 0.2361 0.4871 11.00000 0.05 0.23 ; _shelx_res_checksum 20848 _shelx_hkl_file ; -1 0 0 36.90 2.00 -2 0 0 31.20 1.80 -3 0 0 204.78 11.10 -3 0 0 207.38 11.20 -4 0 0 379.16 21.50 -4 0 0 408.66 21.50 -4 0 0 401.46 21.40 -5 0 0 206.78 11.40 -5 0 0 200.48 11.60 -5 0 0 221.08 11.50 -6 0 0 10.30 1.50 -6 0 0 13.20 2.20 -6 0 0 13.10 1.80 6 0 0 12.00 2.90 6 0 0 10.50 2.50 -7 0 0 125.29 8.10 -7 0 0 115.09 7.60 7 0 0 96.49 10.00 7 0 0 122.99 7.80 7 0 0 128.69 8.30 7 0 0 121.09 9.50 7 0 0 108.29 7.10 7 0 0 94.29 7.30 8 0 0 76.99 10.00 8 0 0 68.09 5.90 8 0 0 66.89 6.60 9 0 0 28.90 5.80 9 0 0 30.10 4.90 9 0 0 30.80 4.70 9 0 0 29.50 3.60 10 0 0 6.20 3.70 10 0 0 -0.60 2.80 10 0 0 1.60 2.20 10 0 0 2.30 2.40 11 0 0 25.50 4.70 11 0 0 21.90 4.10 12 0 0 3.40 2.20 12 0 0 0.10 1.90 12 -1 0 2.70 1.70 12 -1 0 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2.30 -8 5 0 3.10 2.20 7 -5 0 118.99 8.20 7 -5 0 118.79 8.60 7 -5 0 126.29 8.50 -7 5 0 121.99 7.90 6 -5 0 2.00 2.70 6 -5 0 2.10 2.20 6 -5 0 2.60 2.70 -6 5 0 2.60 1.90 5 -5 0 105.99 6.70 5 -5 0 105.89 7.70 5 -5 0 94.89 6.80 -5 5 0 101.99 6.60 4 -5 0 -1.50 2.60 4 -5 0 2.30 2.20 4 -5 0 -1.00 1.70 -4 5 0 0.90 0.90 -4 5 0 1.30 2.00 -4 5 0 1.50 1.40 -4 5 0 0.70 1.30 3 -5 0 258.17 13.60 -3 5 0 244.88 13.70 -3 5 0 246.98 13.50 -3 5 0 262.87 13.40 -3 5 0 236.58 20.40 -3 5 0 237.68 13.70 -3 5 0 219.28 18.50 -2 5 0 26.40 2.50 -2 5 0 27.80 5.20 -2 5 0 34.30 7.40 -2 5 0 24.00 1.90 -2 5 0 24.30 2.10 -2 5 0 27.10 1.70 1 -5 0 106.29 5.50 -1 5 0 101.09 5.50 -1 5 0 99.09 5.60 -1 5 0 84.19 10.90 -1 5 0 98.69 5.50 -1 5 0 84.49 9.50 0 -5 0 41.10 2.40 0 -5 0 41.10 2.40 0 5 0 40.10 2.40 0 5 0 40.80 6.40 0 5 0 39.20 2.40 -1 -5 0 41.40 2.50 -1 -5 0 43.40 2.60 1 5 0 36.50 5.90 1 5 0 46.40 2.50 1 5 0 39.60 2.50 -2 -5 0 5.70 0.80 -2 -5 0 5.00 0.70 2 5 0 4.70 4.80 -3 -5 0 19.80 1.60 3 5 0 26.80 5.60 3 5 0 16.60 5.10 -4 -5 0 3.30 0.90 4 5 0 3.70 5.40 4 5 0 -2.20 6.20 -5 -5 0 4.70 1.20 5 5 0 7.00 1.40 5 5 0 11.20 6.70 5 5 0 7.30 1.50 -6 -5 0 208.68 12.60 6 5 0 212.98 12.50 6 5 0 219.78 12.60 6 5 0 214.08 12.50 6 5 0 256.07 16.50 6 5 0 240.58 14.40 7 5 0 22.10 4.20 7 5 0 27.10 3.40 8 5 0 40.80 4.30 8 5 0 39.50 3.40 8 5 0 40.30 7.10 8 5 0 39.50 3.50 9 5 0 49.40 4.00 9 5 0 50.59 4.00 9 5 0 53.69 5.20 10 5 0 21.70 3.20 10 5 0 24.70 2.90 10 5 0 22.90 2.90 12 5 0 13.90 2.80 12 5 0 19.50 2.20 10 -6 0 1.40 2.00 10 -6 0 2.50 1.70 9 -6 0 14.00 3.10 -9 6 0 19.70 3.60 8 -6 0 5.30 2.20 8 -6 0 4.10 2.80 8 -6 0 4.50 2.70 -8 6 0 3.90 2.00 7 -6 0 16.20 3.10 7 -6 0 15.70 2.60 7 -6 0 14.90 3.10 7 -6 0 15.10 2.60 -7 6 0 14.90 2.40 6 -6 0 84.39 6.70 6 -6 0 82.19 6.70 6 -6 0 83.29 5.60 6 -6 0 76.49 6.00 -6 6 0 81.19 5.70 5 -6 0 23.20 3.90 5 -6 0 33.00 4.70 5 -6 0 30.10 3.70 -5 6 0 26.90 3.20 4 -6 0 478.95 28.10 4 -6 0 513.15 27.90 4 -6 0 468.95 28.20 -4 6 0 565.14 27.90 -4 6 0 520.15 27.80 3 -6 0 43.30 4.30 3 -6 0 39.60 5.10 -3 6 0 55.99 3.60 -3 6 0 56.19 3.30 -3 6 0 54.39 3.60 -3 6 0 46.00 13.10 -3 6 0 51.49 3.90 2 -6 0 335.87 18.90 -2 6 0 360.96 18.80 -2 6 0 359.66 18.90 -2 6 0 280.17 26.40 -2 6 0 306.97 24.20 -2 6 0 356.16 18.90 -2 6 0 370.66 18.80 1 -6 0 267.77 15.10 1 -6 0 289.07 14.90 -1 6 0 257.17 21.70 -1 6 0 272.87 14.90 -1 6 0 257.47 19.60 -1 6 0 275.97 14.90 0 -6 0 3.60 0.70 0 6 0 7.10 6.30 0 6 0 -8.60 11.50 0 6 0 3.40 0.70 0 6 0 4.60 1.20 0 6 0 4.90 0.80 -1 -6 0 39.40 2.70 -1 -6 0 42.50 2.80 1 6 0 45.80 2.50 1 6 0 34.60 6.90 1 6 0 39.50 2.60 -2 -6 0 868.61 46.40 -2 -6 0 808.42 46.40 -2 -6 0 870.31 46.40 2 6 0 891.11 50.39 2 6 0 856.61 49.30 -3 -6 0 7.50 1.10 -3 -6 0 6.30 1.10 -3 -6 0 6.10 1.20 3 6 0 5.80 0.90 3 6 0 3.60 6.30 3 6 0 5.20 5.40 -4 -6 0 316.77 16.60 -4 -6 0 294.07 16.60 4 6 0 296.37 16.60 -5 -6 0 106.49 6.40 -5 -6 0 118.19 6.50 5 6 0 91.39 8.10 5 6 0 110.69 6.50 5 6 0 108.89 6.60 5 6 0 109.59 6.40 -6 -6 0 41.60 3.80 6 6 0 47.80 3.60 6 6 0 58.39 6.30 6 6 0 53.49 5.00 6 6 0 44.70 3.50 6 6 0 52.29 3.90 7 6 0 69.59 4.60 7 6 0 55.89 8.30 7 6 0 74.19 4.60 7 6 0 68.69 4.90 8 6 0 2.50 1.60 8 6 0 1.70 1.60 8 6 0 -0.70 2.00 11 6 0 55.89 3.80 11 6 0 54.09 3.80 11 6 0 50.59 5.30 10 -7 0 4.00 1.90 10 -7 0 7.30 1.70 -10 7 0 4.10 1.70 9 -7 0 12.70 2.90 9 -7 0 12.20 2.20 9 -7 0 12.40 2.60 -9 7 0 12.70 2.10 8 -7 0 26.80 4.10 8 -7 0 24.90 4.90 8 -7 0 23.80 4.50 -8 7 0 23.80 3.50 7 -7 0 13.00 2.60 7 -7 0 13.80 3.10 7 -7 0 15.90 2.60 7 -7 0 16.00 3.20 -7 7 0 13.10 2.20 6 -7 0 10.90 2.40 6 -7 0 12.80 3.00 6 -7 0 8.60 2.60 6 -7 0 10.40 2.30 -6 7 0 10.00 2.20 5 -7 0 80.69 6.40 5 -7 0 71.89 5.50 -5 7 0 76.39 5.30 4 -7 0 4.10 2.40 4 -7 0 0.70 2.40 4 -7 0 1.30 1.90 -4 7 0 1.60 1.50 3 -7 0 17.80 2.30 3 -7 0 15.10 2.60 3 -7 0 12.40 2.90 -3 7 0 16.10 2.60 -3 7 0 19.80 2.30 -3 7 0 13.50 2.40 -3 7 0 15.50 2.00 2 -7 0 259.27 15.20 -2 7 0 257.87 14.80 -2 7 0 281.57 14.60 -2 7 0 253.97 29.90 1 -7 0 4.40 2.50 1 -7 0 2.50 1.40 1 -7 0 2.50 1.10 -1 7 0 3.00 1.30 -1 7 0 3.80 1.20 -1 7 0 3.20 1.00 -1 7 0 16.20 13.50 -1 7 0 1.90 9.30 0 -7 0 8.10 1.10 0 -7 0 5.90 1.40 0 -7 0 6.40 1.00 0 7 0 7.00 1.10 0 7 0 14.40 10.10 0 7 0 10.10 1.50 0 7 0 9.30 1.30 -1 -7 0 11.80 2.00 -1 -7 0 13.30 1.70 -1 -7 0 14.40 1.50 1 7 0 19.80 9.80 1 7 0 17.30 2.50 1 7 0 12.50 9.60 1 7 0 11.90 1.60 1 7 0 12.40 1.40 -2 -7 0 14.40 1.90 -2 -7 0 11.50 1.40 -2 -7 0 13.80 1.80 2 7 0 11.30 8.80 2 7 0 29.10 9.30 2 7 0 10.10 1.30 -3 -7 0 243.98 13.40 -3 -7 0 233.08 13.40 -3 -7 0 254.67 13.40 3 7 0 233.28 13.60 -4 -7 0 6.40 1.30 -4 -7 0 6.00 1.50 4 7 0 8.00 1.80 4 7 0 9.00 1.60 4 7 0 7.30 1.60 -5 -7 0 2.70 1.40 5 7 0 1.20 1.50 5 7 0 3.60 1.60 5 7 0 3.40 1.40 -6 -7 0 200.48 11.60 6 7 0 194.48 13.80 6 7 0 193.88 11.50 6 7 0 233.88 14.80 -7 -7 0 12.50 2.30 7 7 0 15.30 2.10 7 7 0 14.20 2.00 7 7 0 12.90 1.80 -8 -7 0 18.50 2.70 8 7 0 25.00 2.90 8 7 0 28.30 3.00 8 7 0 22.90 3.40 9 7 0 4.90 1.80 9 7 0 -8.30 5.50 9 7 0 2.50 2.40 9 7 0 2.50 1.60 10 7 0 54.69 8.70 10 7 0 67.09 4.40 10 7 0 67.89 5.00 10 7 0 65.89 4.40 11 7 0 6.60 1.50 11 7 0 10.20 2.60 11 7 0 6.80 1.50 9 -8 0 20.50 3.30 9 -8 0 15.10 2.50 -9 8 0 15.30 2.10 8 -8 0 3.40 2.30 8 -8 0 0.20 1.90 8 -8 0 2.40 1.80 -8 8 0 -1.20 1.80 7 -8 0 6.50 2.40 7 -8 0 1.70 2.40 7 -8 0 3.30 2.20 7 -8 0 5.80 2.70 -7 8 0 2.70 1.90 6 -8 0 43.00 5.50 6 -8 0 40.30 5.10 6 -8 0 42.30 4.20 6 -8 0 46.30 5.00 -6 8 0 40.20 4.00 5 -8 0 4.00 2.60 5 -8 0 1.50 2.00 5 -8 0 3.90 2.40 -5 8 0 1.80 1.80 4 -8 0 372.96 20.70 4 -8 0 319.57 20.70 4 -8 0 374.36 20.40 -4 8 0 392.16 20.20 3 -8 0 37.50 6.00 3 -8 0 42.40 4.30 3 -8 0 52.69 5.00 -3 8 0 48.40 3.70 2 -8 0 10.00 2.40 -2 8 0 9.00 1.60 -2 8 0 11.20 2.40 1 -8 0 134.49 8.20 -1 8 0 132.89 7.60 -1 8 0 131.99 8.60 -1 8 0 124.59 7.70 -1 8 0 130.29 24.20 0 -8 0 3.90 1.30 0 -8 0 6.10 1.60 0 8 0 -13.90 13.80 0 8 0 5.40 1.30 0 8 0 8.10 2.30 0 8 0 6.60 1.50 -1 -8 0 19.30 2.60 -1 -8 0 24.70 2.40 1 8 0 24.00 4.00 1 8 0 25.40 3.50 1 8 0 -6.20 14.20 1 8 0 20.70 2.10 -2 -8 0 7.50 1.40 -2 -8 0 6.80 1.60 2 8 0 8.60 1.90 -3 -8 0 6.40 1.40 -3 -8 0 7.60 1.70 3 8 0 4.10 1.80 3 8 0 6.80 1.70 3 8 0 5.90 1.80 -4 -8 0 40.00 3.10 4 8 0 39.10 3.30 4 8 0 36.20 3.20 4 8 0 36.80 3.50 -5 -8 0 212.18 11.80 5 8 0 205.28 11.70 5 8 0 208.98 11.70 5 8 0 212.88 14.10 5 8 0 205.28 11.80 -6 -8 0 71.09 4.60 6 8 0 60.89 4.40 6 8 0 70.49 4.50 6 8 0 64.29 4.30 6 8 0 61.19 4.40 6 8 0 44.40 8.60 -7 -8 0 166.78 9.60 7 8 0 167.68 9.50 7 8 0 159.88 9.30 7 8 0 145.39 12.50 7 8 0 166.28 9.40 8 8 0 3.70 1.60 8 8 0 4.20 1.90 8 8 0 -0.90 5.00 8 8 0 4.70 1.90 -9 -8 0 46.70 5.20 9 8 0 56.89 4.00 9 8 0 52.59 4.40 9 8 0 58.59 4.10 -10 -8 0 69.29 6.70 10 8 0 68.29 4.50 10 8 0 66.39 4.50 10 8 0 66.79 5.00 11 8 0 1.20 1.20 11 8 0 2.20 2.20 11 8 0 4.70 1.40 9 -9 0 6.70 1.90 9 -9 0 7.30 1.70 -9 9 0 8.90 1.70 8 -9 0 3.40 1.90 8 -9 0 1.20 2.00 -8 9 0 2.60 1.70 7 -9 0 11.80 3.00 7 -9 0 8.60 2.40 -7 9 0 7.60 2.10 6 -9 0 -0.30 2.60 6 -9 0 3.30 2.30 6 -9 0 0.90 2.20 6 -9 0 4.20 2.50 -6 9 0 -1.60 1.70 5 -9 0 213.78 12.40 5 -9 0 211.28 11.90 5 -9 0 188.88 12.40 -5 9 0 201.58 11.70 4 -9 0 54.29 4.90 4 -9 0 70.19 5.70 4 -9 0 44.60 6.50 -4 9 0 55.39 4.50 3 -9 0 291.27 16.60 -3 9 0 293.07 16.30 2 -9 0 9.50 2.50 -2 9 0 15.10 2.90 -2 9 0 10.50 1.80 1 -9 0 9.10 3.80 -1 9 0 7.10 3.00 -1 9 0 13.00 2.90 -1 9 0 5.70 1.50 0 -9 0 50.49 3.90 0 9 0 43.20 3.70 0 9 0 44.80 4.60 -1 -9 0 114.29 6.80 1 9 0 109.49 7.20 -2 -9 0 25.30 2.60 -2 -9 0 33.60 4.80 2 9 0 20.90 3.20 2 9 0 25.30 3.40 -3 -9 0 72.39 4.50 3 9 0 61.79 4.80 3 9 0 68.59 4.80 3 9 0 67.99 5.00 -4 -9 0 68.99 4.40 4 9 0 63.19 4.40 4 9 0 59.89 4.40 -5 -9 0 102.29 6.20 5 9 0 97.09 6.10 5 9 0 93.79 6.00 5 9 0 100.89 6.10 -6 -9 0 20.20 3.00 6 9 0 20.70 2.80 6 9 0 20.50 2.80 6 9 0 17.70 2.50 6 9 0 18.20 2.60 -7 -9 0 49.90 4.20 7 9 0 44.30 3.90 7 9 0 49.10 3.80 7 9 0 49.60 4.00 7 9 0 56.29 4.10 -8 -9 0 7.50 2.20 8 9 0 9.30 1.80 8 9 0 10.80 2.00 8 9 0 6.10 1.90 -9 -9 0 15.70 2.60 9 9 0 10.30 2.00 9 9 0 22.70 3.20 9 9 0 21.40 2.90 -10 -9 0 67.19 6.30 10 9 0 73.69 4.50 10 9 0 70.79 4.90 10 9 0 69.09 4.60 8 -10 0 6.60 1.70 8 -10 0 8.90 2.10 -8 10 0 12.90 2.30 7 -10 0 4.20 2.10 7 -10 0 6.10 2.20 7 -10 0 4.90 2.10 -7 10 0 2.10 1.70 6 -10 0 119.89 8.80 6 -10 0 144.29 8.20 6 -10 0 147.29 9.00 -6 10 0 124.99 8.00 5 -10 0 27.40 5.10 5 -10 0 27.70 5.20 5 -10 0 32.40 4.10 -5 10 0 27.90 3.30 -4 10 0 199.58 11.50 3 -10 0 8.40 2.30 -3 10 0 3.90 1.80 2 -10 0 15.00 2.60 -2 10 0 18.80 2.30 -2 10 0 23.20 3.80 1 -10 0 3.40 2.50 -1 10 0 1.90 1.70 -1 10 0 2.50 2.50 0 -10 0 63.59 8.10 0 -10 0 53.89 4.80 0 10 0 53.29 4.30 -1 -10 0 125.29 9.10 -1 -10 0 117.99 7.70 1 10 0 137.69 8.30 -2 -10 0 115.99 6.90 -2 -10 0 108.69 9.20 2 10 0 112.39 7.10 -3 -10 0 15.30 2.60 3 10 0 17.60 2.20 3 10 0 14.60 2.30 3 10 0 15.80 2.80 -4 -10 0 66.49 4.50 4 10 0 60.79 4.50 4 10 0 64.59 4.60 4 10 0 59.09 4.50 -5 -10 0 6.80 1.90 5 10 0 8.50 1.80 5 10 0 7.90 1.80 5 10 0 11.80 1.80 -6 -10 0 2.10 1.70 6 10 0 3.10 1.60 6 10 0 6.00 1.80 6 10 0 4.90 1.60 6 10 0 3.20 1.80 -7 -10 0 3.50 1.80 7 10 0 7.30 1.70 7 10 0 5.90 1.80 7 10 0 6.60 2.00 7 10 0 7.50 1.70 -8 -10 0 11.80 2.20 8 10 0 11.60 1.90 8 10 0 11.70 1.70 8 10 0 13.30 2.00 -9 -10 0 100.49 6.70 9 10 0 103.19 6.00 9 10 0 98.39 6.30 9 10 0 101.39 6.20 -10 -10 0 23.40 4.00 10 10 0 19.80 2.10 10 10 0 14.00 2.10 10 10 0 15.60 2.30 7 -11 0 4.00 1.90 -7 11 0 2.80 1.50 6 -11 0 2.10 2.10 6 -11 0 2.80 2.20 -6 11 0 0.70 1.70 5 -11 0 206.38 11.50 5 -11 0 193.28 12.00 -5 11 0 193.68 11.30 4 -11 0 25.20 3.90 -4 11 0 20.60 3.00 3 -11 0 129.09 7.90 -3 11 0 120.29 7.50 -3 11 0 113.49 9.00 2 -11 0 28.50 4.20 -2 11 0 26.00 3.30 -2 11 0 30.80 5.40 1 -11 0 3.30 2.40 -1 11 0 6.50 2.00 -1 11 0 5.20 2.60 0 -11 0 9.90 3.10 0 -11 0 12.40 3.30 0 11 0 7.20 2.40 -1 -11 0 58.09 4.80 -1 -11 0 54.89 5.90 1 11 0 55.99 4.80 -2 -11 0 53.49 6.80 -2 -11 0 55.09 4.50 2 11 0 60.89 4.70 -3 -11 0 30.10 3.30 3 11 0 29.80 3.60 3 11 0 29.10 3.60 -4 -11 0 78.09 5.30 4 11 0 72.49 5.30 4 11 0 81.59 5.60 4 11 0 81.49 5.40 -5 -11 0 69.89 4.90 5 11 0 68.69 5.00 5 11 0 68.69 4.80 5 11 0 73.49 4.80 -6 -11 0 116.09 7.20 6 11 0 95.29 11.60 6 11 0 113.99 6.90 6 11 0 118.69 7.10 6 11 0 116.99 6.90 6 11 0 124.19 7.10 -7 -11 0 3.60 1.80 7 11 0 3.70 1.70 7 11 0 2.60 1.40 7 11 0 3.00 1.60 -8 -11 0 53.29 4.50 8 11 0 58.49 4.10 8 11 0 58.59 3.80 8 11 0 52.39 4.00 -9 -11 0 53.69 4.30 9 11 0 50.99 3.70 9 11 0 53.19 3.60 9 11 0 52.39 3.80 6 -12 0 4.80 2.00 6 -12 0 4.70 1.90 -6 12 0 4.10 1.50 5 -12 0 0.60 2.10 5 -12 0 -1.90 2.10 -5 12 0 1.70 1.60 4 -12 0 83.09 8.40 4 -12 0 82.79 5.70 -4 12 0 76.89 5.30 3 -12 0 -0.20 2.40 -3 12 0 3.30 1.80 -3 12 0 1.30 3.80 2 -12 0 47.60 4.70 -2 12 0 49.60 5.40 -2 12 0 36.40 3.70 1 -12 0 23.90 4.40 -1 12 0 29.60 3.50 0 -12 0 36.50 5.00 0 12 0 44.10 4.50 -1 -12 0 66.59 5.80 -1 -12 0 75.39 6.40 1 12 0 68.39 5.40 -2 -12 0 20.80 3.30 -2 -12 0 27.40 4.50 2 12 0 24.40 3.60 -3 -12 0 84.29 6.80 3 12 0 93.29 6.00 -4 -12 0 -0.80 1.60 4 12 0 -1.00 2.70 4 12 0 -1.10 1.70 4 12 0 -2.00 1.90 -5 -12 0 6.80 2.00 5 12 0 9.80 2.30 5 12 0 9.20 1.90 5 12 0 5.50 1.70 -6 -12 0 -0.90 1.70 6 12 0 1.40 1.30 6 12 0 1.20 1.60 6 12 0 3.00 1.40 -7 -12 0 24.40 3.20 7 12 0 29.50 2.60 7 12 0 28.50 2.90 7 12 0 27.70 2.90 -8 -12 0 0.30 1.60 8 12 0 2.90 1.60 8 12 0 4.50 1.30 8 12 0 1.30 1.50 -9 -12 0 10.60 2.10 9 12 0 9.10 1.50 9 12 0 14.00 1.70 9 12 0 8.50 1.50 5 -13 0 76.79 5.60 5 -13 0 90.79 5.30 -5 13 0 70.09 5.10 4 -13 0 -0.40 2.10 4 -13 0 -0.40 2.00 -4 13 0 2.50 1.70 3 -13 0 10.40 2.40 -3 13 0 14.70 2.20 -3 13 0 8.00 3.40 2 -13 0 39.30 4.20 -2 13 0 46.00 4.60 1 -13 0 7.40 2.30 -1 13 0 9.30 2.50 0 -13 0 75.39 6.20 0 13 0 85.69 6.00 -1 -13 0 22.00 3.30 1 13 0 26.80 3.80 -2 -13 0 88.99 6.70 -2 -13 0 97.59 7.80 2 13 0 98.69 6.40 -3 -13 0 23.70 3.70 3 13 0 27.70 3.40 -4 -13 0 2.10 1.90 4 13 0 3.50 1.70 -5 -13 0 14.70 2.20 5 13 0 14.40 2.40 5 13 0 17.60 2.70 5 13 0 18.30 2.30 -6 -13 0 44.90 3.90 6 13 0 52.79 3.60 6 13 0 47.90 3.60 6 13 0 53.49 4.00 6 13 0 46.20 3.60 7 13 0 1.10 1.70 7 13 0 1.00 1.30 7 13 0 1.30 1.30 -8 -13 0 58.69 4.20 8 13 0 53.39 3.70 8 13 0 55.29 3.50 8 13 0 52.69 3.70 4 -14 0 4.00 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7 -3 10.40 3.50 6 7 -3 7.80 1.90 -6 -7 3 9.40 2.20 5 7 -3 59.59 4.20 5 7 -3 56.89 4.00 5 7 -3 54.79 4.30 5 7 -3 61.39 4.30 -5 -7 3 58.29 4.40 4 7 -3 239.78 13.90 4 7 -3 255.17 14.00 4 7 -3 247.88 13.90 4 7 -3 254.97 14.00 -4 -7 3 257.17 14.10 3 7 -3 8.90 1.60 3 7 -3 10.20 1.70 3 7 -3 8.60 1.70 -3 -7 3 7.90 1.50 2 7 -3 43.10 3.60 2 7 -3 41.40 3.50 -2 -7 3 42.30 3.50 -2 -7 3 43.60 3.30 -2 -7 3 43.50 4.20 1 7 -3 141.29 8.80 1 7 -3 147.29 8.90 1 7 -3 142.79 21.40 -1 -7 3 155.28 8.70 -1 -7 3 169.88 9.20 -1 -7 3 152.88 8.80 0 7 -3 98.99 16.10 0 7 -3 92.29 6.30 0 7 -3 98.49 5.90 0 7 -3 102.99 5.80 0 -7 3 101.89 6.00 -1 7 -3 8.80 20.20 -1 7 -3 1.30 2.10 -1 7 -3 5.20 1.80 -1 7 -3 3.50 1.30 -1 7 -3 -17.20 15.10 1 -7 3 5.00 2.50 1 -7 3 4.20 1.70 -2 7 -3 27.40 3.60 -2 7 -3 38.00 5.20 -2 7 -3 29.70 3.80 -2 7 -3 -20.10 24.80 -2 7 -3 35.80 2.90 2 -7 3 39.30 4.20 2 -7 3 33.60 4.30 2 -7 3 30.00 3.30 -3 7 -3 114.19 9.20 -3 7 -3 126.29 7.10 3 -7 3 117.09 7.70 -4 7 -3 4.20 1.50 4 -7 3 4.40 2.20 4 -7 3 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7.50 1.40 9 11 3 6.00 1.60 9 11 3 7.00 1.70 -10 -11 -3 14.30 2.10 10 11 3 22.50 3.00 10 11 3 18.50 1.90 10 11 3 14.80 2.10 6 -12 -3 -0.30 1.80 6 -12 -3 3.20 1.80 -6 12 3 -1.40 1.60 5 -12 -3 2.40 2.30 5 -12 -3 5.90 2.30 -5 12 3 1.80 1.80 4 -12 -3 -2.50 1.80 -4 12 3 -1.20 1.80 3 -12 -3 -1.00 2.30 -3 12 3 0.50 1.90 2 -12 -3 1.40 2.40 -2 12 3 3.20 1.90 -2 12 3 4.00 3.60 -1 12 3 1.30 2.90 0 12 3 77.59 6.20 -1 -12 -3 8.70 3.60 1 12 3 0.80 2.30 -2 -12 -3 21.90 3.10 2 12 3 21.80 3.70 -3 -12 -3 97.29 6.30 3 12 3 91.49 6.40 4 12 3 90.19 5.90 4 12 3 94.89 6.20 -5 -12 -3 11.20 2.10 5 12 3 11.90 1.90 5 12 3 10.50 2.00 -6 -12 -3 10.10 2.00 6 12 3 10.90 1.70 6 12 3 9.30 1.80 -7 -12 -3 1.70 1.70 7 12 3 2.80 1.40 7 12 3 2.30 1.90 7 12 3 3.70 1.40 7 12 3 2.20 1.30 -8 -12 -3 3.20 1.70 8 12 3 2.80 1.30 8 12 3 1.90 1.60 8 12 3 1.60 1.60 -9 -12 -3 6.00 1.60 9 12 3 4.40 1.50 9 12 3 6.80 1.60 9 12 3 7.50 1.30 5 -13 -3 2.60 1.80 5 -13 -3 2.50 1.80 -5 13 3 3.40 1.70 4 -13 -3 1.80 2.00 -4 13 3 2.30 1.80 3 -13 -3 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4.10 2.40 0 12 -4 2.30 2.20 0 -12 4 5.40 3.00 -1 12 -4 33.00 4.10 1 -12 4 30.20 4.30 -2 12 -4 15.10 3.90 2 -12 4 17.40 3.00 -3 12 -4 -0.60 2.90 3 -12 4 2.60 2.10 -4 12 -4 5.20 4.40 4 -12 4 6.00 2.30 -5 12 -4 2.60 3.00 5 -12 4 -0.40 2.00 -6 12 -4 7.40 2.80 6 -12 4 -1.50 1.60 8 11 -4 1.60 1.20 8 11 -4 2.80 1.20 8 11 -4 0.00 1.50 8 11 -4 7.00 3.40 -8 -11 4 1.30 1.80 7 11 -4 20.80 2.30 7 11 -4 17.30 2.80 7 11 -4 19.40 2.80 7 11 -4 16.10 2.40 -7 -11 4 21.80 3.10 6 11 -4 24.80 3.00 6 11 -4 20.50 4.00 6 11 -4 29.00 2.70 6 11 -4 26.30 2.70 -6 -11 4 23.50 3.40 5 11 -4 98.59 5.80 5 11 -4 90.59 5.80 5 11 -4 89.59 5.90 5 11 -4 97.89 6.00 -5 -11 4 96.49 6.30 4 11 -4 46.70 3.80 4 11 -4 43.60 3.90 4 11 -4 45.30 3.70 4 11 -4 45.60 3.80 -4 -11 4 41.90 4.00 3 11 -4 56.29 4.40 3 11 -4 59.09 4.40 3 11 -4 54.49 4.20 -3 -11 4 52.29 4.30 2 11 -4 25.30 3.40 2 11 -4 22.30 3.40 2 11 -4 27.00 3.50 1 11 -4 21.80 3.40 1 11 -4 14.70 2.50 -1 -11 4 18.40 3.30 -1 -11 4 11.80 3.70 0 11 -4 4.30 3.90 0 11 -4 6.70 2.30 0 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205.18 11.70 3 10 -4 214.18 11.80 3 10 -4 183.68 11.80 3 10 -4 207.98 11.70 -3 -10 4 220.98 12.00 2 10 -4 95.59 6.20 2 10 -4 96.39 6.20 2 10 -4 101.09 6.30 -2 -10 4 97.19 6.30 1 10 -4 23.60 3.30 1 10 -4 21.50 3.40 1 10 -4 20.20 3.40 -1 -10 4 20.70 4.00 -1 -10 4 17.10 3.20 0 10 -4 5.80 2.20 0 10 -4 7.70 4.50 0 -10 4 4.80 2.90 0 -10 4 3.60 2.30 -1 10 -4 52.69 4.80 1 -10 4 44.50 5.30 1 -10 4 52.29 5.10 -2 10 -4 1.30 2.50 -2 10 -4 0.70 2.10 2 -10 4 -0.60 2.50 -3 10 -4 29.40 3.90 -3 10 -4 23.60 3.10 3 -10 4 28.70 4.20 3 -10 4 19.80 3.70 -4 10 -4 3.00 1.70 -4 10 -4 -3.00 3.80 4 -10 4 -0.40 2.80 4 -10 4 2.50 2.60 -5 10 -4 37.30 3.60 5 -10 4 33.90 5.00 5 -10 4 47.40 4.30 -6 10 -4 26.30 3.00 6 -10 4 22.70 3.40 6 -10 4 25.50 4.40 -7 10 -4 2.40 1.60 7 -10 4 2.90 2.00 7 -10 4 -0.40 2.00 -8 10 -4 2.30 1.60 8 -10 4 1.70 1.80 9 9 -4 43.70 6.40 9 9 -4 34.30 3.10 9 9 -4 34.90 3.00 9 9 -4 36.50 3.00 -9 -9 4 39.00 4.60 8 9 -4 0.10 1.50 8 9 -4 -0.70 1.60 8 9 -4 -0.50 1.70 8 9 -4 0.50 2.80 -8 -9 4 -0.30 2.40 7 9 -4 14.00 2.30 7 9 -4 17.90 2.70 7 9 -4 18.90 2.40 7 9 -4 25.30 4.20 -7 -9 4 18.30 2.70 6 9 -4 14.60 2.00 6 9 -4 17.40 2.20 6 9 -4 15.10 2.30 6 9 -4 26.40 4.60 6 9 -4 18.60 2.50 -6 -9 4 16.40 2.40 5 9 -4 206.58 11.70 5 9 -4 210.28 11.70 5 9 -4 198.38 11.60 5 9 -4 192.88 11.50 -5 -9 4 212.58 11.80 4 9 -4 239.88 13.40 4 9 -4 234.88 13.40 4 9 -4 242.58 13.50 4 9 -4 236.48 13.50 -4 -9 4 240.78 13.60 3 9 -4 197.28 11.30 3 9 -4 204.28 11.30 3 9 -4 188.78 11.30 3 9 -4 194.78 11.30 -3 -9 4 208.88 11.50 2 9 -4 33.80 3.20 2 9 -4 31.50 3.40 2 9 -4 31.10 3.40 -2 -9 4 30.10 3.40 1 9 -4 25.10 3.00 1 9 -4 21.80 3.20 -1 -9 4 15.00 2.90 -1 -9 4 21.40 4.00 0 9 -4 28.30 3.70 0 -9 4 25.90 3.30 -1 9 -4 -0.20 2.10 -1 9 -4 -0.80 2.00 1 -9 4 -2.60 2.40 1 -9 4 -0.30 2.30 -2 9 -4 19.90 3.10 -2 9 -4 21.50 2.90 2 -9 4 17.40 2.90 -3 9 -4 56.89 6.20 -3 9 -4 56.99 4.30 3 -9 4 56.09 5.00 3 -9 4 55.69 7.00 -4 9 -4 36.40 3.50 4 -9 4 34.40 4.20 -5 9 -4 22.40 3.50 5 -9 4 15.40 2.90 5 -9 4 26.70 3.90 -6 9 -4 -0.10 1.80 6 -9 4 2.60 2.30 6 -9 4 2.20 2.40 -7 9 -4 4.70 1.80 7 -9 4 3.00 2.10 7 -9 4 3.10 2.30 7 -9 4 2.30 2.00 -8 9 -4 10.90 1.70 8 -9 4 6.70 2.00 8 -9 4 8.20 2.10 9 -9 4 8.30 1.80 10 8 -4 6.00 1.40 10 8 -4 5.30 1.50 10 8 -4 4.80 1.30 9 8 -4 2.90 1.60 9 8 -4 3.40 3.20 9 8 -4 1.50 1.70 9 8 -4 3.70 1.70 -9 -8 4 14.40 6.20 8 8 -4 3.40 2.80 8 8 -4 1.20 2.70 8 8 -4 4.00 2.80 8 8 -4 -1.90 2.20 -8 -8 4 1.30 2.70 7 8 -4 1.50 1.70 7 8 -4 2.10 2.90 7 8 -4 -0.20 2.00 7 8 -4 3.60 2.10 -7 -8 4 -2.20 2.20 6 8 -4 67.49 6.00 6 8 -4 62.49 4.30 6 8 -4 49.20 4.50 6 8 -4 56.89 4.70 6 8 -4 63.59 4.50 -6 -8 4 58.99 4.80 5 8 -4 7.40 1.90 5 8 -4 8.60 1.80 5 8 -4 6.40 1.60 5 8 -4 8.60 2.00 -5 -8 4 8.30 2.10 4 8 -4 38.20 3.40 4 8 -4 32.60 3.30 4 8 -4 36.50 3.30 4 8 -4 28.00 3.10 -4 -8 4 32.00 3.40 3 8 -4 138.49 7.90 3 8 -4 128.79 7.90 3 8 -4 143.09 7.90 3 8 -4 114.59 8.40 -3 -8 4 141.59 8.00 2 8 -4 66.89 4.50 2 8 -4 55.69 4.90 2 8 -4 66.09 4.50 -2 -8 4 68.09 4.50 1 8 -4 25.50 3.10 1 8 -4 26.10 3.20 -1 -8 4 24.40 2.90 -1 -8 4 25.40 4.10 0 8 -4 119.49 7.70 0 8 -4 129.79 7.70 0 -8 4 128.99 7.50 0 -8 4 125.19 8.60 -1 8 -4 202.78 11.30 -1 8 -4 189.18 10.80 1 -8 4 177.18 11.30 1 -8 4 195.38 11.00 -2 8 -4 33.70 3.00 -2 8 -4 28.50 4.80 2 -8 4 24.40 4.20 -3 8 -4 6.00 1.70 -3 8 -4 5.50 3.60 3 -8 4 8.60 2.30 3 -8 4 7.10 3.00 -4 8 -4 172.38 9.50 4 -8 4 171.88 9.80 4 -8 4 141.39 10.60 -5 8 -4 16.90 2.20 5 -8 4 13.90 2.80 5 -8 4 9.40 3.40 5 -8 4 20.50 2.90 -6 8 -4 109.59 7.80 6 -8 4 110.29 8.20 6 -8 4 127.69 7.70 6 -8 4 126.59 8.40 -7 8 -4 1.40 1.80 7 -8 4 -2.50 2.20 7 -8 4 0.80 2.10 7 -8 4 -0.10 2.00 -8 8 -4 108.59 6.50 8 -8 4 100.09 6.50 8 -8 4 100.09 6.90 8 -8 4 109.79 7.40 -9 8 -4 5.80 1.60 9 -8 4 6.70 1.80 9 -8 4 5.50 1.90 10 7 -4 0.70 1.50 10 7 -4 1.00 1.60 10 7 -4 1.50 1.40 9 7 -4 5.90 1.90 9 7 -4 8.70 3.30 9 7 -4 4.10 2.00 9 7 -4 6.50 1.70 8 7 -4 1.70 2.20 8 7 -4 2.10 3.10 8 7 -4 2.90 1.70 8 7 -4 2.20 2.00 -8 -7 4 4.80 3.10 7 7 -4 14.50 3.40 7 7 -4 24.50 3.00 7 7 -4 24.00 3.20 7 7 -4 15.40 2.40 6 7 -4 14.10 1.90 6 7 -4 10.60 2.20 6 7 -4 19.50 3.30 6 7 -4 11.50 2.00 -6 -7 4 11.00 2.40 5 7 -4 20.30 2.50 5 7 -4 20.90 2.40 5 7 -4 19.00 3.10 5 7 -4 18.30 3.10 -5 -7 4 18.40 3.20 4 7 -4 253.17 13.80 4 7 -4 255.07 13.90 4 7 -4 221.68 14.50 -4 -7 4 260.87 14.00 3 7 -4 49.00 3.80 3 7 -4 49.30 3.70 3 7 -4 49.80 3.70 3 7 -4 48.00 3.80 -3 -7 4 48.40 3.70 2 7 -4 4.10 1.90 2 7 -4 6.50 1.80 2 7 -4 5.90 1.50 -2 -7 4 5.10 1.40 1 7 -4 107.69 6.80 1 7 -4 108.89 6.80 -1 -7 4 114.09 6.70 -1 -7 4 116.59 7.00 0 7 -4 35.10 14.00 0 7 -4 22.30 2.60 0 7 -4 25.60 3.40 0 7 -4 29.50 3.20 0 -7 4 26.30 3.60 0 -7 4 22.30 2.60 0 -7 4 20.90 3.20 -1 7 -4 31.90 3.20 -1 7 -4 31.90 3.80 -1 7 -4 34.10 4.00 1 -7 4 34.90 3.20 1 -7 4 28.80 3.60 1 -7 4 30.60 4.40 -2 7 -4 82.49 6.40 -2 7 -4 81.59 4.90 -2 7 -4 78.29 6.30 2 -7 4 77.19 5.70 2 -7 4 72.59 5.80 -3 7 -4 91.49 5.40 -3 7 -4 75.09 7.50 3 -7 4 78.29 7.40 3 -7 4 92.09 6.10 -4 7 -4 6.90 1.60 4 -7 4 6.80 2.20 4 -7 4 7.70 2.70 -5 7 -4 37.90 3.60 5 -7 4 35.80 5.40 5 -7 4 39.00 4.00 5 -7 4 31.60 4.90 -6 7 -4 0.10 1.70 6 -7 4 0.00 2.10 6 -7 4 0.70 2.20 6 -7 4 0.20 2.30 -7 7 -4 3.40 1.80 7 -7 4 5.40 2.30 7 -7 4 2.30 2.20 7 -7 4 4.00 2.40 -8 7 -4 -1.90 1.70 8 -7 4 2.00 2.50 8 -7 4 0.30 2.00 -9 7 -4 83.89 5.40 9 -7 4 86.49 5.90 9 -7 4 84.79 6.30 -10 7 -4 0.60 1.50 10 -7 4 1.50 1.40 10 -7 4 0.70 1.70 10 6 -4 39.00 3.20 10 6 -4 37.70 3.40 10 6 -4 31.60 6.20 10 6 -4 41.20 3.40 9 6 -4 35.60 3.30 9 6 -4 35.70 5.70 9 6 -4 42.40 3.90 9 6 -4 33.70 3.50 8 6 -4 3.60 2.10 8 6 -4 3.40 1.90 8 6 -4 4.50 3.60 8 6 -4 4.10 2.00 7 6 -4 34.70 3.40 7 6 -4 34.60 5.50 7 6 -4 26.30 3.80 7 6 -4 26.80 3.40 -7 -6 4 33.00 4.80 6 6 -4 285.97 15.60 6 6 -4 275.17 15.70 6 6 -4 299.07 16.40 6 6 -4 271.27 15.50 -6 -6 4 260.37 15.80 5 6 -4 161.18 9.30 5 6 -4 179.78 9.30 5 6 -4 146.49 9.30 5 6 -4 162.38 9.40 -5 -6 4 152.78 9.40 4 6 -4 430.76 23.60 4 6 -4 423.46 23.50 4 6 -4 452.35 23.60 4 6 -4 414.26 23.50 -4 -6 4 430.56 23.60 3 6 -4 42.50 3.60 3 6 -4 45.00 3.60 3 6 -4 47.00 3.60 3 6 -4 46.60 3.60 -3 -6 4 52.29 3.50 -3 -6 4 43.80 4.00 -3 -6 4 47.30 3.80 2 6 -4 41.80 3.90 2 6 -4 49.20 3.70 2 6 -4 49.40 3.70 -2 -6 4 51.89 3.50 -2 -6 4 55.69 3.70 1 6 -4 23.90 3.10 1 6 -4 23.00 3.00 1 6 -4 35.90 11.90 -1 -6 4 27.10 2.40 -1 -6 4 26.10 2.50 -1 -6 4 25.50 2.40 0 6 -4 3.00 14.90 0 6 -4 5.40 1.80 0 6 -4 6.80 1.30 0 6 -4 11.40 9.50 0 -6 4 4.10 1.30 0 -6 4 4.10 1.30 0 -6 4 3.00 1.20 -1 6 -4 22.40 2.30 -1 6 -4 19.20 16.80 -1 6 -4 61.09 17.60 -1 6 -4 25.50 2.60 -1 6 -4 21.50 2.50 1 -6 4 23.20 2.70 1 -6 4 18.50 2.00 1 -6 4 22.10 2.30 -2 6 -4 6.10 20.30 -2 6 -4 13.70 2.30 -2 6 -4 11.30 2.80 -2 6 -4 16.00 2.00 2 -6 4 12.10 2.20 2 -6 4 12.30 2.50 2 -6 4 13.60 1.60 -3 6 -4 73.99 4.40 -3 6 -4 58.99 5.60 -3 6 -4 57.79 5.00 3 -6 4 67.49 5.20 3 -6 4 78.99 7.90 -4 6 -4 54.09 3.70 4 -6 4 47.70 5.50 4 -6 4 51.39 4.40 4 -6 4 49.70 6.10 -5 6 -4 0.60 1.40 5 -6 4 0.90 2.20 5 -6 4 4.60 2.20 5 -6 4 4.30 2.40 -6 6 -4 49.40 4.10 6 -6 4 52.99 4.50 6 -6 4 48.30 5.00 6 -6 4 53.39 5.40 -7 6 -4 73.19 4.90 7 -6 4 66.99 5.70 7 -6 4 65.59 5.20 7 -6 4 59.09 6.00 -8 6 -4 10.30 2.00 8 -6 4 6.80 2.50 8 -6 4 7.60 2.30 8 -6 4 11.40 2.50 -9 6 -4 31.40 3.30 9 -6 4 32.60 3.70 9 -6 4 30.30 4.30 -10 6 -4 36.70 3.20 10 -6 4 37.90 3.60 10 -6 4 30.10 4.10 11 5 -4 5.80 1.30 11 5 -4 5.00 1.70 11 5 -4 6.70 2.10 10 5 -4 24.60 3.20 10 5 -4 17.50 3.90 10 5 -4 23.80 3.00 10 5 -4 21.60 2.80 9 5 -4 13.30 2.10 9 5 -4 10.30 2.00 9 5 -4 10.00 2.20 8 5 -4 5.00 2.00 8 5 -4 2.30 2.00 8 5 -4 -0.80 2.20 8 5 -4 -1.80 3.40 7 5 -4 128.29 9.10 7 5 -4 119.59 7.70 7 5 -4 120.89 7.50 7 5 -4 125.69 7.50 6 5 -4 161.88 9.90 6 5 -4 185.88 11.20 6 5 -4 160.68 10.10 6 5 -4 163.88 9.80 -6 -5 4 194.48 11.80 5 5 -4 17.60 3.40 5 5 -4 8.30 1.70 5 5 -4 8.20 1.80 5 5 -4 10.60 1.60 5 5 -4 10.30 2.30 -5 -5 4 15.20 3.40 4 5 -4 302.67 16.90 4 5 -4 323.07 17.00 4 5 -4 309.57 17.00 4 5 -4 291.87 16.90 -4 -5 4 306.27 17.10 -4 -5 4 308.57 17.00 3 5 -4 183.68 10.90 3 5 -4 202.28 10.90 3 5 -4 187.58 10.80 3 5 -4 182.08 10.80 -3 -5 4 193.58 10.90 -3 -5 4 197.18 10.60 -3 -5 4 198.18 10.90 2 5 -4 79.99 13.20 -2 -5 4 83.59 4.90 -2 -5 4 84.59 5.20 -2 -5 4 88.09 5.10 1 5 -4 5.10 10.30 1 5 -4 4.30 6.60 -1 -5 4 1.00 1.10 -1 -5 4 1.50 0.70 -1 -5 4 -0.60 1.00 0 5 -4 338.37 27.30 0 5 -4 327.97 18.60 0 5 -4 370.46 23.30 0 -5 4 332.87 18.50 -1 5 -4 63.59 3.80 -1 5 -4 60.99 3.80 -1 5 -4 40.50 12.40 1 -5 4 55.39 3.80 1 -5 4 63.89 3.70 1 -5 4 60.09 4.00 -2 5 -4 154.18 8.20 -2 5 -4 146.29 8.00 -2 5 -4 124.49 18.50 -2 5 -4 119.39 16.60 2 -5 4 135.09 8.10 2 -5 4 144.39 7.90 -3 5 -4 127.99 20.60 -3 5 -4 138.19 7.50 -3 5 -4 125.69 7.70 3 -5 4 124.09 8.00 -4 5 -4 128.79 8.30 -4 5 -4 130.69 8.70 -4 5 -4 144.09 7.80 4 -5 4 135.29 9.10 4 -5 4 132.59 8.10 -5 5 -4 113.59 6.50 5 -5 4 106.49 7.50 5 -5 4 107.69 6.90 5 -5 4 103.29 7.30 -6 5 -4 3.40 1.60 6 -5 4 2.20 2.00 6 -5 4 4.90 2.30 6 -5 4 4.80 2.20 -7 5 -4 125.79 7.20 7 -5 4 115.29 8.00 7 -5 4 118.79 7.30 7 -5 4 100.89 7.50 8 -5 4 0.90 2.30 8 -5 4 2.10 2.00 8 -5 4 0.20 2.30 -9 5 -4 17.30 2.90 9 -5 4 15.40 2.80 9 -5 4 18.60 3.60 -10 5 -4 27.10 3.10 10 -5 4 23.70 4.20 10 -5 4 29.50 3.80 -11 5 -4 7.70 1.90 11 -5 4 13.80 2.60 11 -5 4 7.00 1.80 11 4 -4 4.70 1.40 11 4 -4 5.50 3.30 11 4 -4 5.10 1.90 10 4 -4 15.10 2.30 10 4 -4 15.00 2.50 10 4 -4 14.20 3.80 10 4 -4 18.50 2.80 9 4 -4 49.90 4.70 9 4 -4 61.69 4.40 9 4 -4 58.39 4.40 9 4 -4 50.29 6.70 8 4 -4 4.50 2.00 8 4 -4 5.20 2.10 8 4 -4 5.70 3.80 8 4 -4 2.30 2.20 7 4 -4 134.19 8.00 7 4 -4 132.69 8.20 7 4 -4 134.09 9.70 7 4 -4 134.59 7.90 6 4 -4 58.29 4.40 6 4 -4 53.89 4.20 5 4 -4 84.39 5.40 5 4 -4 80.89 5.50 5 4 -4 100.29 7.20 5 4 -4 83.79 5.60 4 4 -4 211.68 11.60 4 4 -4 207.28 11.70 4 4 -4 200.78 11.60 -4 -4 4 215.38 11.30 -4 -4 4 198.88 11.80 3 4 -4 81.69 14.40 3 4 -4 56.89 8.50 -3 -4 4 54.09 4.10 -3 -4 4 59.29 3.40 -3 -4 4 59.49 3.80 2 4 -4 127.59 14.60 2 4 -4 157.78 12.40 -2 -4 4 152.08 8.10 -2 -4 4 141.29 7.90 -2 -4 4 134.39 8.20 1 4 -4 201.68 14.40 1 4 -4 201.98 10.50 -1 -4 4 206.48 10.70 -1 -4 4 189.38 10.60 -1 -4 4 174.28 10.80 0 4 -4 23.60 1.70 0 4 -4 24.80 5.40 0 -4 4 22.00 1.80 0 -4 4 23.90 1.80 -1 4 -4 849.32 43.90 -1 4 -4 815.42 46.50 -1 4 -4 794.82 43.80 1 -4 4 818.92 43.70 1 -4 4 772.22 43.80 -2 4 -4 20.70 5.20 -2 4 -4 23.10 2.00 2 -4 4 20.80 2.00 2 -4 4 24.70 2.70 2 -4 4 21.70 1.60 -3 4 -4 2.20 1.10 -3 4 -4 4.80 1.10 -3 4 -4 12.90 8.40 3 -4 4 1.70 1.00 -4 4 -4 7.70 1.30 -4 4 -4 7.30 1.70 4 -4 4 8.50 2.10 -5 4 -4 12.50 2.10 5 -4 4 11.60 2.00 5 -4 4 8.40 2.20 5 -4 4 7.40 3.20 5 -4 4 10.40 2.40 -6 4 -4 91.89 5.40 6 -4 4 69.39 7.50 6 -4 4 81.49 6.40 6 -4 4 85.49 6.10 6 -4 4 88.89 5.90 -7 4 -4 8.10 1.80 7 -4 4 6.50 2.00 7 -4 4 10.00 2.50 7 -4 4 13.10 2.40 -8 4 -4 50.69 4.30 8 -4 4 53.19 5.60 8 -4 4 51.89 5.30 8 -4 4 51.59 4.70 8 -4 4 60.39 5.10 -9 4 -4 12.90 2.00 9 -4 4 9.60 2.30 9 -4 4 8.90 2.50 -10 4 -4 24.70 3.30 10 -4 4 31.50 4.00 10 -4 4 27.90 4.40 -11 4 -4 5.30 2.10 11 -4 4 8.30 1.80 11 -4 4 6.30 2.00 11 3 -4 10.10 2.00 11 3 -4 10.90 2.20 10 3 -4 0.70 1.80 10 3 -4 0.40 3.40 10 3 -4 3.00 2.20 10 3 -4 -1.00 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5.30 4 12 -5 0.30 1.60 4 12 -5 1.00 1.80 4 12 -5 1.90 1.60 -4 -12 5 0.00 1.90 3 12 -5 98.89 6.30 3 12 -5 98.29 6.10 -3 -12 5 98.69 6.40 2 12 -5 100.19 6.40 2 12 -5 109.99 6.60 -2 -12 5 93.89 6.60 1 12 -5 8.70 2.20 -1 -12 5 5.00 2.40 -1 -12 5 12.10 3.30 0 12 -5 14.40 2.50 0 -12 5 14.10 3.00 -1 12 -5 4.60 3.20 -1 12 -5 3.50 2.80 1 -12 5 10.70 3.00 -2 12 -5 11.10 3.20 -2 12 -5 15.30 2.70 2 -12 5 21.80 3.80 -3 12 -5 -0.10 2.90 -3 12 -5 3.30 2.90 3 -12 5 2.00 2.40 -4 12 -5 1.60 2.90 -4 12 -5 8.10 3.60 4 -12 5 -2.20 2.10 -5 12 -5 -3.80 2.50 5 -12 5 0.60 1.80 7 11 -5 2.60 1.20 7 11 -5 2.70 1.70 7 11 -5 5.10 2.20 7 11 -5 3.00 1.30 -7 -11 5 4.80 1.70 6 11 -5 10.00 2.00 6 11 -5 16.30 2.30 6 11 -5 14.90 1.80 6 11 -5 17.80 2.60 -6 -11 5 17.50 2.30 5 11 -5 49.20 3.90 5 11 -5 56.29 4.60 5 11 -5 46.50 3.70 5 11 -5 44.40 3.80 5 11 -5 47.40 3.60 -5 -11 5 50.29 4.20 4 11 -5 142.09 8.20 4 11 -5 125.79 8.20 4 11 -5 146.09 8.40 4 11 -5 139.39 8.10 -4 -11 5 145.29 8.50 3 11 -5 2.20 1.80 3 11 -5 0.10 1.70 3 11 -5 0.40 1.90 -3 -11 5 -1.20 2.00 2 11 -5 7.60 2.30 2 11 -5 7.40 2.10 -2 -11 5 7.40 2.20 1 11 -5 41.90 4.70 1 11 -5 43.10 4.10 -1 -11 5 33.80 3.90 -1 -11 5 35.50 6.30 0 11 -5 35.10 4.20 0 11 -5 42.10 8.80 0 -11 5 40.60 5.30 0 -11 5 35.70 4.10 -1 11 -5 40.80 4.50 -1 11 -5 38.20 6.50 1 -11 5 40.50 5.00 -2 11 -5 13.60 2.70 -2 11 -5 8.60 3.80 2 -11 5 11.80 2.80 -3 11 -5 70.19 5.70 3 -11 5 57.69 5.30 -4 11 -5 0.40 3.60 -4 11 -5 1.20 2.60 4 -11 5 4.10 2.70 -5 11 -5 42.40 4.20 5 -11 5 52.39 4.30 -6 11 -5 -0.60 2.40 6 -11 5 -0.30 1.90 -7 11 -5 11.20 2.40 7 -11 5 15.50 2.40 8 10 -5 15.00 1.90 8 10 -5 20.20 4.10 8 10 -5 11.50 1.50 8 10 -5 12.20 2.00 -8 -10 5 18.10 3.00 7 10 -5 1.80 1.80 7 10 -5 1.10 2.30 7 10 -5 4.80 1.50 7 10 -5 0.70 1.50 -7 -10 5 1.00 2.00 6 10 -5 55.49 4.90 6 10 -5 52.49 4.20 6 10 -5 51.39 3.80 6 10 -5 57.79 4.00 -6 -10 5 53.99 4.50 5 10 -5 262.37 14.40 5 10 -5 247.88 14.20 5 10 -5 243.78 14.20 5 10 -5 256.57 14.30 -5 -10 5 263.37 14.50 4 10 -5 54.69 4.40 4 10 -5 58.09 4.40 4 10 -5 54.99 4.20 4 10 -5 55.59 4.40 -4 -10 5 55.99 4.40 3 10 -5 97.79 6.10 3 10 -5 94.49 6.20 3 10 -5 100.19 6.00 3 10 -5 91.19 6.30 -3 -10 5 84.89 6.90 2 10 -5 11.60 2.10 2 10 -5 9.70 2.00 2 10 -5 10.40 2.30 -2 -10 5 5.90 2.00 1 10 -5 1.80 2.00 1 10 -5 4.10 2.40 -1 -10 5 2.50 2.00 -1 -10 5 2.50 3.70 0 10 -5 1.40 3.60 0 10 -5 2.30 2.00 0 -10 5 -3.60 3.00 0 -10 5 0.30 2.10 -1 10 -5 86.19 8.70 -1 10 -5 106.49 6.80 1 -10 5 102.89 7.00 1 -10 5 98.09 7.10 -2 10 -5 58.19 5.40 2 -10 5 54.49 5.30 -3 10 -5 10.20 2.20 -3 10 -5 7.50 3.20 3 -10 5 12.40 2.90 -4 10 -5 4.50 2.10 -4 10 -5 6.10 3.70 4 -10 5 3.60 2.60 -5 10 -5 41.90 3.70 5 -10 5 37.10 4.10 5 -10 5 29.40 5.20 -6 10 -5 27.70 3.20 6 -10 5 24.90 3.60 6 -10 5 23.20 3.20 -7 10 -5 11.50 1.90 7 -10 5 9.90 2.10 7 -10 5 12.20 2.70 9 9 -5 4.30 1.30 9 9 -5 5.20 1.30 9 9 -5 4.20 1.30 9 9 -5 7.50 3.30 8 9 -5 3.70 1.50 8 9 -5 2.30 1.80 8 9 -5 2.90 1.40 8 9 -5 3.10 2.50 -8 -9 5 2.00 2.30 7 9 -5 5.40 1.70 7 9 -5 7.50 1.60 7 9 -5 4.30 1.80 7 9 -5 4.80 2.50 -7 -9 5 7.80 2.30 6 9 -5 180.98 10.60 6 9 -5 164.38 9.80 6 9 -5 168.98 9.80 6 9 -5 169.18 10.00 -6 -9 5 165.48 10.10 5 9 -5 -1.50 1.90 5 9 -5 0.70 1.60 5 9 -5 1.40 1.80 5 9 -5 -1.60 1.90 -5 -9 5 -2.70 1.70 4 9 -5 126.29 7.70 4 9 -5 125.49 7.70 4 9 -5 129.89 7.90 4 9 -5 134.09 7.90 -4 -9 5 136.09 8.00 3 9 -5 30.30 3.40 3 9 -5 31.60 3.50 3 9 -5 30.40 3.10 3 9 -5 30.00 3.60 -3 -9 5 25.90 3.50 2 9 -5 36.70 3.90 2 9 -5 40.60 3.70 2 9 -5 37.00 3.50 -2 -9 5 39.00 3.70 1 9 -5 11.10 2.10 1 9 -5 9.30 2.00 1 9 -5 8.30 2.30 -1 -9 5 8.40 2.00 -1 -9 5 4.80 3.80 0 9 -5 8.10 3.90 0 9 -5 6.50 2.10 0 -9 5 8.30 2.10 0 -9 5 7.50 3.10 -1 9 -5 45.00 4.40 1 -9 5 35.60 4.20 1 -9 5 36.00 4.60 -2 9 -5 66.79 5.10 -2 9 -5 67.99 5.80 2 -9 5 71.49 5.70 -3 9 -5 88.99 6.00 -3 9 -5 71.89 6.80 3 -9 5 88.59 6.20 -4 9 -5 8.30 4.10 -4 9 -5 10.10 1.90 4 -9 5 4.80 3.20 4 -9 5 8.10 2.80 -5 9 -5 36.90 3.50 5 -9 5 41.40 4.40 5 -9 5 29.70 5.80 -6 9 -5 4.50 1.90 6 -9 5 2.30 2.30 -7 9 -5 9.90 1.90 7 -9 5 5.70 2.30 7 -9 5 9.40 2.20 -8 9 -5 4.20 1.70 8 -9 5 3.60 1.80 8 -9 5 1.80 2.10 9 8 -5 4.10 1.50 9 8 -5 5.10 1.70 9 8 -5 8.50 3.00 9 8 -5 5.00 1.40 -9 -8 5 13.50 3.30 8 8 -5 -1.70 1.70 8 8 -5 -0.70 2.60 8 8 -5 0.50 1.60 8 8 -5 0.50 1.50 -8 -8 5 3.60 2.70 7 8 -5 62.69 5.70 7 8 -5 61.99 4.60 7 8 -5 60.99 4.80 7 8 -5 64.79 4.50 -7 -8 5 62.69 5.20 6 8 -5 1.20 1.70 6 8 -5 3.10 1.90 6 8 -5 0.60 2.00 6 8 -5 2.70 2.80 -6 -8 5 -1.10 1.80 5 8 -5 135.39 8.20 5 8 -5 136.89 8.10 5 8 -5 139.79 8.30 5 8 -5 141.19 8.30 -5 -8 5 137.29 8.40 4 8 -5 21.40 2.90 4 8 -5 15.60 2.10 4 8 -5 16.00 3.00 4 8 -5 16.40 2.10 -4 -8 5 17.60 3.10 3 8 -5 181.78 10.10 3 8 -5 170.48 10.10 3 8 -5 175.78 10.10 3 8 -5 168.08 10.10 -3 -8 5 177.88 10.20 2 8 -5 8.50 1.70 2 8 -5 7.00 1.80 2 8 -5 9.30 2.40 -2 -8 5 7.40 1.90 1 8 -5 114.69 9.30 1 8 -5 119.69 7.00 1 8 -5 99.69 7.10 -1 -8 5 122.49 6.90 -1 -8 5 104.09 8.60 0 8 -5 74.49 5.10 0 8 -5 67.59 7.70 0 -8 5 73.39 4.90 0 -8 5 66.39 6.30 -1 8 -5 69.19 5.40 1 -8 5 76.39 5.20 1 -8 5 75.09 6.10 -2 8 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4 7 -5 110.29 6.60 4 7 -5 105.09 6.50 4 7 -5 107.99 6.70 -4 -7 5 100.99 6.70 3 7 -5 24.70 2.90 3 7 -5 20.40 3.40 3 7 -5 24.10 3.10 -3 -7 5 22.90 2.90 2 7 -5 11.30 2.10 2 7 -5 11.00 2.20 2 7 -5 12.60 1.90 2 7 -5 17.00 2.10 -2 -7 5 11.50 1.80 1 7 -5 23.40 2.70 1 7 -5 30.40 3.00 1 7 -5 31.00 6.50 1 7 -5 32.70 3.20 -1 -7 5 27.20 2.80 0 7 -5 161.48 9.10 0 7 -5 156.88 9.20 0 7 -5 152.88 11.00 0 -7 5 166.08 9.10 0 -7 5 145.29 10.00 0 -7 5 152.58 9.70 -1 7 -5 61.99 4.40 -1 7 -5 63.19 5.00 1 -7 5 56.99 5.30 1 -7 5 60.89 4.30 1 -7 5 54.69 5.50 -2 7 -5 46.60 4.90 -2 7 -5 46.30 3.40 2 -7 5 45.00 4.40 2 -7 5 41.50 4.20 -3 7 -5 9.90 1.60 -3 7 -5 8.20 3.50 -4 7 -5 19.20 2.70 4 -7 5 15.00 3.30 4 -7 5 23.20 2.90 -5 7 -5 77.49 4.80 5 -7 5 62.49 6.50 5 -7 5 75.79 5.40 5 -7 5 54.29 6.40 -6 7 -5 1.10 1.70 6 -7 5 2.30 2.40 6 -7 5 0.60 2.40 6 -7 5 -1.40 2.40 -7 7 -5 45.00 3.60 7 -7 5 37.10 5.30 7 -7 5 34.90 4.70 7 -7 5 33.20 4.20 -8 7 -5 4.00 1.80 8 -7 5 2.00 1.90 8 -7 5 1.80 2.00 8 -7 5 1.20 1.70 -9 7 -5 50.49 3.70 9 -7 5 48.20 4.70 9 -7 5 42.70 4.20 -10 7 -5 6.80 1.80 10 -7 5 6.20 1.70 10 -7 5 8.70 1.80 10 6 -5 2.90 1.40 10 6 -5 0.90 3.30 10 6 -5 1.30 1.80 10 6 -5 4.80 1.60 9 6 -5 3.90 3.00 9 6 -5 1.70 1.70 9 6 -5 -0.40 1.80 9 6 -5 3.00 1.90 8 6 -5 3.10 1.80 8 6 -5 0.90 3.00 8 6 -5 4.90 2.00 8 6 -5 2.70 2.10 -8 -6 5 12.20 3.40 7 6 -5 152.58 10.30 7 6 -5 151.88 9.10 7 6 -5 152.98 9.10 7 6 -5 160.28 9.40 6 6 -5 34.60 5.20 6 6 -5 30.30 3.80 6 6 -5 30.70 3.20 6 6 -5 28.90 3.40 -6 -6 5 31.00 4.40 5 6 -5 15.30 2.00 5 6 -5 17.20 2.40 5 6 -5 15.50 2.20 5 6 -5 28.70 4.90 5 6 -5 20.10 2.70 -5 -6 5 17.00 2.30 4 6 -5 9.00 1.90 4 6 -5 7.60 1.60 4 6 -5 10.30 1.90 -4 -6 5 11.20 1.80 3 6 -5 129.79 7.70 3 6 -5 140.29 7.70 3 6 -5 126.09 7.70 3 6 -5 131.09 7.80 -3 -6 5 126.99 7.70 2 6 -5 84.99 5.60 2 6 -5 84.19 5.30 2 6 -5 78.99 5.50 2 6 -5 82.59 5.30 -2 -6 5 83.99 5.20 1 6 -5 16.00 2.70 1 6 -5 20.50 5.00 1 6 -5 17.60 3.50 1 6 -5 21.90 2.70 -1 -6 5 13.60 1.90 -1 -6 5 15.40 2.30 -1 -6 5 10.30 1.80 0 6 -5 114.79 7.00 0 6 -5 117.19 9.00 0 6 -5 125.39 7.20 0 6 -5 120.99 7.30 0 -6 5 125.49 7.00 0 -6 5 125.69 7.30 0 -6 5 107.89 7.10 -1 6 -5 20.20 3.60 -1 6 -5 16.70 2.00 -1 6 -5 20.10 2.50 -1 6 -5 25.70 3.40 -1 6 -5 10.20 14.00 1 -6 5 20.40 3.00 1 -6 5 23.40 4.10 1 -6 5 20.50 2.60 -2 6 -5 115.99 7.40 -2 6 -5 108.59 7.90 -2 6 -5 130.19 6.90 -2 6 -5 124.69 7.90 2 -6 5 106.49 7.10 2 -6 5 120.99 7.60 2 -6 5 120.49 7.20 -3 6 -5 58.09 3.80 -3 6 -5 45.50 6.00 -3 6 -5 47.10 6.10 3 -6 5 59.49 4.70 -4 6 -5 43.10 3.30 4 -6 5 36.60 4.10 4 -6 5 42.90 5.80 4 -6 5 28.20 5.30 -5 6 -5 6.50 1.70 5 -6 5 7.10 2.40 -6 6 -5 4.50 1.70 6 -6 5 3.00 2.40 6 -6 5 3.50 2.20 6 -6 5 2.00 2.40 -7 6 -5 49.20 3.90 7 -6 5 44.50 4.60 7 -6 5 44.40 4.40 7 -6 5 40.60 5.20 -8 6 -5 73.69 4.90 8 -6 5 68.09 5.70 8 -6 5 68.89 5.20 8 -6 5 66.69 6.20 -9 6 -5 37.40 3.50 9 -6 5 35.20 4.60 9 -6 5 39.40 4.10 -10 6 -5 34.20 3.00 10 -6 5 32.50 3.90 10 -6 5 28.10 3.30 10 5 -5 68.49 4.60 10 5 -5 64.69 4.60 10 5 -5 70.89 4.40 10 5 -5 64.99 6.30 9 5 -5 32.90 3.30 9 5 -5 30.80 3.50 9 5 -5 33.00 5.30 9 5 -5 34.70 3.40 8 5 -5 145.79 10.10 8 5 -5 135.79 8.60 8 5 -5 154.78 8.90 7 5 -5 4.40 2.00 7 5 -5 4.40 1.90 7 5 -5 7.00 3.30 7 5 -5 5.80 2.10 6 5 -5 171.28 10.00 6 5 -5 174.48 10.00 6 5 -5 182.78 11.10 6 5 -5 166.78 10.20 -6 -5 5 169.18 10.60 5 5 -5 19.40 2.50 5 5 -5 15.30 2.20 5 5 -5 15.30 2.40 5 5 -5 16.10 2.30 5 5 -5 27.00 4.80 -5 -5 5 21.10 3.60 4 5 -5 109.89 6.60 4 5 -5 113.59 6.60 4 5 -5 106.59 6.50 4 5 -5 101.99 6.60 -4 -5 5 107.69 6.70 3 5 -5 11.70 1.70 3 5 -5 14.40 2.00 3 5 -5 12.20 1.80 3 5 -5 15.20 1.90 -3 -5 5 16.50 2.50 -3 -5 5 15.50 2.30 2 5 -5 16.00 2.00 2 5 -5 11.20 2.00 2 5 -5 13.10 1.80 2 5 -5 10.40 1.90 -2 -5 5 12.80 1.40 -2 -5 5 9.20 1.80 -2 -5 5 12.60 2.20 1 5 -5 32.20 9.60 1 5 -5 35.10 3.40 1 5 -5 40.70 3.40 -1 -5 5 40.00 3.20 -1 -5 5 39.80 3.00 -1 -5 5 41.50 2.80 0 5 -5 13.50 2.40 0 5 -5 10.20 9.90 0 5 -5 14.00 1.60 0 -5 5 15.70 1.90 0 -5 5 18.40 2.20 0 -5 5 15.20 2.10 -1 5 -5 801.52 41.50 -1 5 -5 770.52 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63.79 5.00 2 -9 -5 4.60 2.80 2 -9 -5 3.90 3.20 2 -9 -5 5.00 2.50 -2 9 5 2.20 1.80 1 -9 -5 193.68 12.70 1 -9 -5 194.28 11.70 -1 9 5 201.38 11.30 -1 9 5 191.38 12.70 0 -9 -5 4.00 3.60 0 -9 -5 8.90 2.60 0 9 5 3.40 1.60 0 9 5 6.20 3.10 -1 -9 -5 50.29 5.40 -1 -9 -5 49.50 4.60 1 9 5 52.19 5.10 1 9 5 52.29 4.10 -2 -9 -5 3.00 2.80 -2 -9 -5 2.20 1.80 2 9 5 5.50 2.10 -3 -9 -5 8.70 4.10 -3 -9 -5 4.70 1.60 3 9 5 4.00 1.80 -4 -9 -5 47.20 3.80 4 9 5 48.50 4.10 -5 -9 -5 14.70 2.60 5 9 5 7.40 3.30 5 9 5 15.90 2.60 -6 -9 -5 13.50 2.00 6 9 5 13.30 2.00 6 9 5 14.60 2.20 -7 -9 -5 20.80 3.10 7 9 5 25.40 2.90 7 9 5 22.70 2.90 7 9 5 18.30 3.00 -8 -9 -5 153.18 9.10 8 9 5 158.88 9.00 8 9 5 153.88 9.00 8 9 5 158.58 9.30 8 9 5 145.29 8.90 -9 -9 -5 95.09 6.40 9 9 5 90.89 6.50 9 9 5 96.29 6.00 9 9 5 117.09 6.30 -10 -9 -5 43.60 4.10 10 9 5 47.40 3.30 10 9 5 42.20 4.50 10 9 5 46.80 3.50 -11 -9 -5 3.40 2.20 11 9 5 3.50 1.40 11 9 5 3.10 1.20 7 -10 -5 29.20 3.60 7 -10 -5 22.80 4.20 7 -10 -5 24.90 3.70 -7 10 5 19.20 3.30 6 -10 -5 20.90 4.20 6 -10 -5 14.70 3.10 6 -10 -5 15.00 2.50 6 -10 -5 13.70 2.20 -6 10 5 12.30 2.50 5 -10 -5 4.90 2.30 5 -10 -5 7.20 3.00 5 -10 -5 7.20 2.60 -5 10 5 5.10 2.20 4 -10 -5 4.50 3.20 4 -10 -5 5.00 2.60 -4 10 5 1.10 2.10 3 -10 -5 18.70 3.20 3 -10 -5 18.10 3.60 -3 10 5 14.80 2.30 2 -10 -5 15.70 3.40 2 -10 -5 14.20 2.90 2 -10 -5 13.50 3.40 -2 10 5 11.10 2.20 1 -10 -5 69.09 5.70 1 -10 -5 68.19 7.00 1 -10 -5 75.79 7.40 -1 10 5 68.59 7.00 -1 10 5 64.49 5.00 0 -10 -5 66.99 5.80 0 10 5 69.09 5.10 0 10 5 71.49 6.30 -1 -10 -5 20.20 3.10 -1 -10 -5 26.40 3.30 1 10 5 24.00 3.40 1 10 5 23.00 3.20 -2 -10 -5 2.30 2.10 -2 -10 -5 1.80 3.10 2 10 5 2.90 2.20 -3 -10 -5 4.50 4.80 -3 -10 -5 5.60 1.90 3 10 5 6.70 2.10 -4 -10 -5 6.20 2.00 4 10 5 5.80 1.90 -5 -10 -5 28.80 3.30 5 10 5 27.10 3.20 5 10 5 27.30 3.30 -6 -10 -5 4.90 1.90 6 10 5 5.00 2.20 6 10 5 5.90 1.80 6 10 5 5.60 1.70 -7 -10 -5 101.79 6.40 7 10 5 77.79 8.80 7 10 5 105.89 6.30 7 10 5 104.29 6.30 7 10 5 102.09 6.20 -8 -10 -5 1.70 1.80 8 10 5 4.80 1.90 8 10 5 2.70 1.70 8 10 5 4.00 1.40 8 10 5 6.20 1.60 -9 -10 -5 48.00 4.00 9 10 5 45.80 3.50 9 10 5 39.60 4.10 9 10 5 45.30 3.40 -10 -10 -5 45.30 4.10 10 10 5 51.49 3.50 10 10 5 45.30 3.30 6 -11 -5 7.60 2.30 6 -11 -5 7.90 2.10 -6 11 5 5.60 1.90 5 -11 -5 76.29 6.30 5 -11 -5 68.29 5.40 5 -11 -5 72.99 6.30 5 -11 -5 77.29 6.10 -5 11 5 70.69 5.40 4 -11 -5 2.00 2.20 4 -11 -5 9.00 3.00 4 -11 -5 6.50 3.10 -4 11 5 3.00 2.10 3 -11 -5 35.30 5.60 3 -11 -5 34.80 5.40 -3 11 5 24.80 3.70 2 -11 -5 4.50 3.50 2 -11 -5 6.20 2.60 1 -11 -5 7.10 2.60 1 -11 -5 10.30 3.90 -1 11 5 7.30 2.10 -1 11 5 10.10 3.90 0 -11 -5 52.39 5.20 0 11 5 56.79 5.80 0 11 5 53.79 4.60 -1 -11 -5 113.49 7.90 1 11 5 116.59 7.80 -2 -11 -5 96.29 7.20 -2 -11 -5 91.99 6.70 2 11 5 92.79 6.50 -3 -11 -5 7.50 3.70 -3 -11 -5 5.00 2.10 3 11 5 5.10 2.10 -4 -11 -5 293.47 16.50 4 11 5 290.77 16.50 4 11 5 290.67 16.30 -5 -11 -5 3.90 1.90 5 11 5 4.40 2.00 5 11 5 2.10 1.80 -6 -11 -5 82.39 5.60 6 11 5 75.19 5.80 6 11 5 85.09 5.40 6 11 5 85.89 5.50 -7 -11 -5 5.70 1.90 7 11 5 6.30 2.00 7 11 5 6.90 1.70 7 11 5 8.00 1.70 -8 -11 -5 209.08 12.00 8 11 5 216.98 11.90 8 11 5 207.28 11.70 8 11 5 199.98 11.60 8 11 5 211.28 11.80 -9 -11 -5 4.10 1.80 9 11 5 7.60 1.40 9 11 5 6.10 1.90 9 11 5 8.90 1.70 -10 -11 -5 9.40 2.00 10 11 5 12.70 1.60 10 11 5 15.20 1.80 -6 12 5 5.00 2.00 5 -12 -5 31.10 4.10 5 -12 -5 29.00 4.90 5 -12 -5 26.70 3.50 4 -12 -5 42.30 5.80 4 -12 -5 41.50 4.30 -4 12 5 42.20 4.10 3 -12 -5 6.70 3.20 3 -12 -5 -4.00 2.10 -3 12 5 -1.30 1.90 -2 12 5 24.10 3.50 1 -12 -5 9.10 2.70 -1 12 5 9.10 2.20 -1 12 5 7.40 3.80 0 -12 -5 4.00 2.80 0 12 5 0.00 2.90 0 12 5 7.20 2.60 -1 -12 -5 51.69 5.30 1 12 5 39.60 4.90 -2 -12 -5 5.40 3.10 -2 -12 -5 5.60 2.80 2 12 5 3.50 2.30 -3 -12 -5 0.60 3.60 3 12 5 -0.90 2.00 3 12 5 -0.40 2.30 -4 -12 -5 57.19 4.70 4 12 5 57.39 4.60 4 12 5 57.69 4.60 -5 -12 -5 44.70 4.20 5 12 5 49.40 3.80 5 12 5 47.90 4.00 -6 -12 -5 8.00 2.10 6 12 5 7.20 1.60 6 12 5 8.10 1.80 -7 -12 -5 52.89 4.40 7 12 5 55.79 3.90 7 12 5 59.99 3.80 7 12 5 49.99 4.50 -8 -12 -5 0.80 1.70 8 12 5 4.00 1.60 8 12 5 4.20 1.30 8 12 5 2.00 2.00 8 12 5 2.60 1.20 -9 -12 -5 49.50 4.00 9 12 5 57.79 3.50 9 12 5 47.60 3.80 9 12 5 56.19 3.90 4 -13 -5 0.70 2.00 4 -13 -5 -2.40 1.90 -4 13 5 0.00 2.40 3 -13 -5 0.10 2.10 -3 13 5 3.00 2.00 -2 13 5 1.00 2.20 -1 13 5 65.79 5.90 -1 13 5 48.20 5.30 0 13 5 6.40 2.90 1 13 5 7.00 2.70 2 13 5 0.40 2.20 -3 -13 -5 34.10 4.90 3 13 5 34.80 3.90 -4 -13 -5 9.80 2.60 4 13 5 9.70 1.90 4 13 5 8.90 2.00 -5 -13 -5 4.60 2.20 5 13 5 7.00 1.60 5 13 5 4.70 2.40 -6 -13 -5 66.39 5.00 6 13 5 67.39 4.40 6 13 5 67.99 4.60 -7 -13 -5 0.80 1.60 7 13 5 3.70 1.50 7 13 5 0.80 1.40 7 13 5 2.60 1.30 -8 -13 -5 21.40 2.80 8 13 5 26.70 2.30 8 13 5 25.40 2.60 2 -14 -5 48.40 4.30 1 -14 -5 -2.60 2.10 -1 14 5 1.90 3.10 0 -14 -5 29.80 4.00 0 14 5 28.30 4.40 -1 -14 -5 3.00 2.40 1 14 5 7.00 2.50 -2 -14 -5 10.30 2.80 2 14 5 7.80 2.10 -3 -14 -5 147.89 10.00 3 14 5 146.89 8.80 -4 -14 -5 117.99 8.60 4 14 5 131.19 7.60 -5 -14 -5 41.90 4.50 5 14 5 47.50 3.70 -6 -14 -5 -0.90 1.90 6 14 5 -0.70 1.40 6 14 5 0.40 1.60 -7 -14 -5 95.19 6.40 7 14 5 102.79 5.90 7 14 5 100.79 5.90 7 14 5 102.09 5.90 1 -15 -5 -0.10 1.60 -1 15 5 4.40 4.90 0 -15 -5 -4.20 2.00 0 15 5 2.00 2.40 -1 -15 -5 8.80 2.40 1 15 5 13.00 2.40 -2 -15 -5 12.80 2.90 2 15 5 10.40 2.10 -3 -15 -5 34.30 5.70 3 15 5 22.90 3.20 4 15 5 9.40 1.80 5 15 5 85.39 5.30 -6 -15 -5 81.99 6.90 6 15 5 76.79 4.70 6 15 5 79.39 4.70 4 13 -6 17.60 2.20 4 13 -6 26.90 3.30 4 13 -6 17.20 2.70 -4 -13 6 16.10 2.80 3 13 -6 1.90 1.50 -3 -13 6 -0.90 2.00 2 13 -6 17.90 2.80 -2 -13 6 5.10 3.10 1 13 -6 67.79 4.80 0 13 -6 0.50 2.00 0 -13 6 4.40 3.10 -1 13 -6 16.60 2.40 1 -13 6 10.80 2.70 -2 13 -6 0.00 1.90 2 -13 6 0.10 2.40 -3 13 -6 36.10 4.80 -3 13 -6 42.30 4.30 3 -13 6 43.00 3.70 6 12 -6 31.20 3.30 6 12 -6 29.20 2.70 -6 -12 6 32.20 3.20 5 12 -6 59.19 4.60 5 12 -6 66.19 4.30 -5 -12 6 56.09 4.30 4 12 -6 11.90 2.10 4 12 -6 9.70 1.70 4 12 -6 10.00 2.30 -4 -12 6 7.80 1.90 3 12 -6 8.50 2.30 3 12 -6 3.20 1.80 -3 -12 6 5.40 2.00 2 12 -6 97.99 6.40 -2 -12 6 103.99 6.50 1 12 -6 6.10 2.00 -1 -12 6 6.60 2.60 -1 -12 6 9.60 3.70 0 12 -6 1.90 2.10 0 -12 6 -1.30 3.10 -1 12 -6 12.40 3.50 -1 12 -6 11.10 2.50 1 -12 6 8.70 2.90 -2 12 -6 66.69 5.40 -2 12 -6 75.69 6.10 2 -12 6 62.89 5.50 -3 12 -6 1.70 2.70 -3 12 -6 0.00 2.60 3 -12 6 -0.90 2.10 -4 12 -6 1.00 3.30 -4 12 -6 -0.60 2.40 4 -12 6 0.40 2.10 -5 12 -6 -1.20 2.00 5 -12 6 -1.00 1.70 7 11 -6 7.10 1.40 7 11 -6 6.80 2.00 7 11 -6 7.00 1.30 7 11 -6 6.30 1.40 -7 -11 6 4.60 1.80 6 11 -6 2.10 1.40 6 11 -6 1.10 1.40 6 11 -6 1.40 1.70 6 11 -6 0.20 2.00 -6 -11 6 3.40 1.70 5 11 -6 5.80 1.80 5 11 -6 5.60 1.70 5 11 -6 9.00 2.30 5 11 -6 7.60 1.50 5 11 -6 7.90 1.70 -5 -11 6 8.40 2.00 4 11 -6 51.99 4.00 4 11 -6 54.99 4.10 4 11 -6 53.59 3.80 -4 -11 6 50.69 4.40 3 11 -6 12.70 3.10 3 11 -6 17.70 2.90 3 11 -6 16.10 2.30 -3 -11 6 12.50 2.30 2 11 -6 11.30 3.40 2 11 -6 9.00 2.10 -2 -11 6 6.00 2.20 1 11 -6 12.70 2.40 -1 -11 6 13.10 2.40 -1 -11 6 20.00 4.20 0 11 -6 64.49 5.00 0 11 -6 62.19 7.40 0 -11 6 52.89 5.10 0 -11 6 66.59 6.00 -1 11 -6 39.50 4.30 -1 11 -6 35.80 5.60 1 -11 6 37.70 4.80 -2 11 -6 5.60 3.10 -2 11 -6 4.90 2.60 2 -11 6 4.40 2.50 -3 11 -6 46.10 4.90 -3 11 -6 48.60 5.60 -4 11 -6 3.70 3.40 4 -11 6 1.40 2.40 -5 11 -6 24.90 4.70 -5 11 -6 23.40 3.30 -6 11 -6 -5.80 2.90 6 -11 6 1.60 1.70 7 10 -6 18.80 2.60 7 10 -6 21.50 3.50 7 10 -6 17.80 2.30 7 10 -6 18.90 2.20 -7 -10 6 18.10 3.10 6 10 -6 8.50 1.90 6 10 -6 10.90 1.70 6 10 -6 10.20 1.60 6 10 -6 8.30 2.40 -6 -10 6 10.30 2.10 5 10 -6 54.59 3.90 5 10 -6 52.99 5.70 5 10 -6 57.99 3.80 5 10 -6 53.09 4.30 -5 -10 6 52.99 4.50 4 10 -6 9.30 1.90 4 10 -6 16.70 2.20 4 10 -6 15.30 2.20 4 10 -6 12.80 2.10 -4 -10 6 12.60 2.30 3 10 -6 30.40 3.60 3 10 -6 35.60 3.30 3 10 -6 30.40 3.70 3 10 -6 26.60 4.10 -3 -10 6 32.00 3.60 2 10 -6 36.30 3.80 2 10 -6 36.90 3.40 2 10 -6 33.00 4.20 -2 -10 6 30.70 3.60 1 10 -6 6.70 3.50 1 10 -6 7.60 2.30 -1 -10 6 5.00 4.10 0 10 -6 75.39 5.50 0 10 -6 78.79 7.50 0 -10 6 71.59 6.70 0 -10 6 74.49 5.70 -1 10 -6 14.20 3.50 -1 10 -6 14.50 2.60 1 -10 6 11.70 3.10 -2 10 -6 136.29 10.40 -2 10 -6 155.48 9.40 2 -10 6 158.18 9.60 -3 10 -6 -3.40 2.80 -3 10 -6 1.30 3.10 3 -10 6 1.30 2.60 -4 10 -6 5.10 3.80 -4 10 -6 6.10 2.50 4 -10 6 7.50 2.60 -5 10 -6 1.60 2.20 5 -10 6 0.20 2.00 -6 10 -6 62.69 5.00 6 -10 6 77.19 5.10 -7 10 -6 9.60 2.80 7 -10 6 15.10 2.70 8 9 -6 50.29 3.60 8 9 -6 50.69 3.50 8 9 -6 53.29 3.70 8 9 -6 51.89 4.80 -8 -9 6 54.29 4.30 7 9 -6 11.90 1.80 7 9 -6 9.80 1.70 7 9 -6 7.20 2.00 7 9 -6 6.80 2.40 -7 -9 6 8.90 2.30 6 9 -6 11.10 2.20 6 9 -6 7.20 1.70 6 9 -6 6.20 2.90 -6 -9 6 8.50 2.20 5 9 -6 12.30 2.20 5 9 -6 8.40 1.80 5 9 -6 15.00 2.10 5 9 -6 11.40 2.00 -5 -9 6 10.60 2.20 4 9 -6 25.70 3.40 4 9 -6 27.90 3.60 4 9 -6 31.50 3.50 4 9 -6 30.80 3.20 -4 -9 6 25.10 3.20 3 9 -6 3.00 2.00 3 9 -6 2.70 1.90 3 9 -6 2.60 1.80 3 9 -6 4.40 2.10 -3 -9 6 0.30 1.80 2 9 -6 2.80 1.80 2 9 -6 3.50 1.80 2 9 -6 1.20 2.20 -2 -9 6 0.60 1.90 1 9 -6 4.80 1.90 1 9 -6 4.60 2.00 1 9 -6 5.80 2.60 1 9 -6 4.10 3.90 -1 -9 6 4.60 2.00 -1 -9 6 7.10 4.10 0 9 -6 22.00 3.60 0 9 -6 16.20 3.70 0 -9 6 17.70 3.60 0 -9 6 18.60 3.30 -1 9 -6 148.99 9.00 -1 9 -6 149.99 10.20 1 -9 6 143.59 8.90 1 -9 6 144.09 9.30 -2 9 -6 0.20 2.40 -2 9 -6 1.40 3.20 2 -9 6 1.30 2.60 -3 9 -6 69.39 5.20 -3 9 -6 80.29 6.50 3 -9 6 71.29 5.80 -4 9 -6 0.90 1.80 -4 9 -6 -0.10 3.80 4 -9 6 -0.50 2.50 -5 9 -6 10.90 2.20 5 -9 6 5.60 2.50 -6 9 -6 2.30 2.00 6 -9 6 8.20 3.00 6 -9 6 -2.40 3.70 -7 9 -6 10.10 2.00 7 -9 6 8.00 2.20 7 -9 6 12.40 3.00 8 -9 6 19.50 3.50 8 -9 6 28.60 2.80 9 8 -6 40.20 4.30 9 8 -6 36.70 2.70 9 8 -6 32.20 2.90 9 8 -6 34.00 2.70 -9 -8 6 34.40 4.30 8 8 -6 2.30 1.60 8 8 -6 2.90 1.70 8 8 -6 3.20 2.50 8 8 -6 3.40 1.50 -8 -8 6 4.50 2.50 7 8 -6 1.90 1.40 7 8 -6 -0.60 2.40 7 8 -6 3.90 1.60 7 8 -6 0.70 1.80 -7 -8 6 2.30 2.40 6 8 -6 6.80 2.70 6 8 -6 2.60 1.90 6 8 -6 3.60 2.20 6 8 -6 5.40 1.90 -6 -8 6 0.30 2.10 5 8 -6 16.90 2.20 5 8 -6 20.40 2.30 5 8 -6 20.50 3.00 5 8 -6 16.60 2.50 -5 -8 6 15.50 2.70 4 8 -6 8.40 1.90 4 8 -6 8.80 2.10 4 8 -6 10.20 2.10 4 8 -6 7.00 2.00 -4 -8 6 8.50 2.10 3 8 -6 27.40 3.10 3 8 -6 25.60 3.40 3 8 -6 28.70 3.30 3 8 -6 25.40 3.30 -3 -8 6 25.40 3.30 2 8 -6 11.80 1.90 2 8 -6 9.60 2.30 2 8 -6 10.40 2.00 2 8 -6 10.40 2.20 -2 -8 6 7.80 1.90 1 8 -6 126.89 10.90 1 8 -6 125.79 7.80 1 8 -6 126.29 7.60 -1 -8 6 134.59 7.80 0 8 -6 80.29 7.50 0 8 -6 88.99 6.00 0 -8 6 88.69 5.80 0 -8 6 88.39 9.00 -1 8 -6 15.50 2.50 -1 8 -6 16.30 3.50 1 -8 6 16.80 2.90 1 -8 6 15.90 2.30 -2 8 -6 15.50 2.50 -2 8 -6 13.50 2.60 2 -8 6 19.10 2.90 -3 8 -6 0.50 3.10 -3 8 -6 -0.80 1.80 3 -8 6 -1.50 2.10 -4 8 -6 54.99 4.20 -4 8 -6 50.89 6.80 4 -8 6 46.80 4.90 5 -8 6 8.30 2.60 5 -8 6 5.70 3.30 -6 8 -6 5.30 2.00 6 -8 6 0.10 2.50 6 -8 6 1.20 2.70 7 -8 6 21.40 3.20 7 -8 6 17.90 2.90 -8 8 -6 0.70 1.80 8 -8 6 0.20 1.80 8 -8 6 0.70 2.40 -9 8 -6 3.70 2.30 -9 8 -6 6.30 1.80 9 7 -6 6.30 2.60 9 7 -6 6.20 1.50 9 7 -6 6.10 1.70 9 7 -6 3.20 1.50 -9 -7 6 8.60 3.50 8 7 -6 5.40 1.80 8 7 -6 4.20 2.60 8 7 -6 6.10 2.00 8 7 -6 7.20 1.80 -8 -7 6 7.10 3.00 7 7 -6 5.20 2.70 7 7 -6 2.30 1.70 7 7 -6 2.40 1.80 7 7 -6 -1.60 1.90 -7 -7 6 2.90 2.50 6 7 -6 16.70 2.20 6 7 -6 24.40 4.70 6 7 -6 12.20 2.50 6 7 -6 14.30 2.30 -6 -7 6 14.50 2.40 5 7 -6 51.49 4.50 5 7 -6 52.59 4.10 5 7 -6 55.59 4.10 5 7 -6 48.90 4.10 -5 -7 6 51.29 4.50 4 7 -6 13.70 2.00 4 7 -6 13.80 2.20 4 7 -6 13.40 2.10 4 7 -6 16.80 2.30 -4 -7 6 14.70 2.30 3 7 -6 1.50 1.70 3 7 -6 4.60 1.90 3 7 -6 1.60 1.50 3 7 -6 1.40 1.70 -3 -7 6 1.50 1.60 2 7 -6 155.58 9.60 2 7 -6 174.68 11.90 2 7 -6 162.48 9.60 2 7 -6 164.88 9.50 2 7 -6 163.28 9.70 -2 -7 6 164.88 9.60 1 7 -6 33.50 6.20 1 7 -6 29.30 4.30 1 7 -6 26.10 3.80 1 7 -6 31.40 3.90 -1 -7 6 32.60 3.10 0 7 -6 6.00 1.90 0 7 -6 7.90 1.80 0 7 -6 4.50 3.00 0 -7 6 6.80 1.80 0 -7 6 4.90 3.10 -1 7 -6 54.29 6.40 -1 7 -6 56.99 4.50 -1 7 -6 42.40 4.50 1 -7 6 45.50 5.00 1 -7 6 52.59 4.00 -2 7 -6 -0.70 2.10 -2 7 -6 0.30 1.70 2 -7 6 -1.50 4.20 2 -7 6 -2.00 2.20 -3 7 -6 84.39 5.30 3 -7 6 79.29 6.00 -4 7 -6 1.10 1.60 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5.00 -4 3 -6 84.79 5.60 4 -3 6 79.69 5.70 4 -3 6 69.99 6.20 -5 3 -6 2.30 1.20 5 -3 6 1.80 1.90 5 -3 6 -2.90 2.90 5 -3 6 2.20 1.90 -6 3 -6 8.10 1.50 6 -3 6 5.90 2.40 6 -3 6 6.40 2.40 -7 3 -6 35.90 3.20 7 -3 6 28.80 4.00 7 -3 6 32.60 3.70 7 -3 6 25.50 5.00 -8 3 -6 15.80 2.80 8 -3 6 9.70 2.60 8 -3 6 12.80 2.50 8 -3 6 11.70 2.30 -9 3 -6 16.50 2.90 9 -3 6 14.40 2.60 9 -3 6 12.10 2.70 9 -3 6 11.60 2.70 -10 3 -6 34.70 3.60 10 -3 6 37.40 4.10 10 -3 6 34.00 4.40 10 -3 6 33.20 4.10 11 -3 6 1.90 1.60 11 -3 6 2.40 1.70 10 2 -6 5.80 1.80 10 2 -6 4.60 1.90 10 2 -6 3.90 2.70 9 2 -6 15.10 3.30 9 2 -6 22.60 3.20 9 2 -6 28.10 3.10 8 2 -6 5.10 2.50 8 2 -6 1.10 3.70 8 2 -6 4.80 2.20 8 2 -6 3.90 2.20 7 2 -6 -2.50 3.30 7 2 -6 0.90 2.20 7 2 -6 3.70 2.10 7 2 -6 0.10 2.40 6 2 -6 219.78 12.90 6 2 -6 198.48 11.70 6 2 -6 195.58 11.80 6 2 -6 206.18 11.90 5 2 -6 13.60 5.80 5 2 -6 12.80 2.00 5 2 -6 10.70 2.50 5 2 -6 13.20 3.30 5 2 -6 8.60 2.20 4 2 -6 191.88 11.80 4 2 -6 192.38 11.70 4 2 -6 198.78 11.80 4 2 -6 208.88 11.60 4 2 -6 222.68 12.50 4 2 -6 212.78 14.60 -4 -2 6 206.28 11.90 3 2 -6 5.50 2.10 3 2 -6 2.60 2.20 3 2 -6 6.50 1.80 3 2 -6 2.50 1.40 3 2 -6 4.90 3.10 3 2 -6 4.10 1.70 -3 -2 6 2.00 1.30 -3 -2 6 5.10 1.90 2 2 -6 144.79 15.40 2 2 -6 138.79 8.10 -2 -2 6 151.48 8.30 -2 -2 6 147.89 8.40 -2 -2 6 134.99 19.10 1 2 -6 58.89 8.10 1 2 -6 60.09 3.40 -1 -2 6 41.30 9.90 -1 -2 6 54.89 3.80 0 2 -6 374.76 24.20 0 2 -6 378.26 20.30 0 2 -6 375.46 20.40 0 -2 6 372.16 26.50 -1 2 -6 54.29 3.10 -1 2 -6 47.50 3.10 -1 2 -6 48.40 3.40 1 -2 6 53.29 3.10 1 -2 6 51.09 3.40 -2 2 -6 275.27 16.70 -2 2 -6 323.17 16.70 -2 2 -6 316.57 21.80 2 -2 6 300.17 24.20 2 -2 6 314.27 16.60 -3 2 -6 355.86 19.20 -3 2 -6 319.87 25.40 -3 2 -6 375.26 19.20 3 -2 6 334.97 28.40 -4 2 -6 2.90 1.00 -4 2 -6 4.30 1.60 4 -2 6 4.90 2.00 -5 2 -6 49.60 4.80 -5 2 -6 61.69 3.70 5 -2 6 54.59 4.70 5 -2 6 53.39 4.40 5 -2 6 56.49 6.10 -6 2 -6 1.40 1.30 6 -2 6 2.90 2.00 6 -2 6 1.40 1.70 6 -2 6 2.80 2.20 -7 2 -6 365.36 20.00 7 -2 6 343.57 20.30 7 -2 6 376.66 20.20 7 -2 6 370.46 20.70 -8 2 -6 210.78 11.50 8 -2 6 207.78 12.00 8 -2 6 196.88 11.60 8 -2 6 186.18 12.30 -9 2 -6 32.90 3.30 9 -2 6 37.80 4.70 9 -2 6 24.60 5.10 9 -2 6 36.50 3.90 -10 2 -6 8.70 2.20 10 -2 6 9.30 2.50 10 -2 6 13.80 2.20 -11 2 -6 16.10 2.70 11 -2 6 10.60 2.10 11 -2 6 17.10 3.10 11 -2 6 15.80 2.40 10 1 -6 6.90 2.10 10 1 -6 5.10 2.70 9 1 -6 -1.20 2.00 9 1 -6 -2.80 2.90 9 1 -6 3.00 1.90 8 1 -6 3.00 2.20 8 1 -6 4.80 3.50 8 1 -6 2.20 2.10 8 1 -6 2.90 3.70 7 1 -6 45.80 5.10 7 1 -6 55.89 4.80 7 1 -6 63.39 4.50 7 1 -6 54.69 7.40 7 1 -6 43.40 6.90 6 1 -6 50.89 7.40 6 1 -6 40.40 4.00 6 1 -6 39.60 6.40 6 1 -6 40.80 4.20 5 1 -6 14.40 3.60 5 1 -6 17.30 3.00 5 1 -6 17.40 2.30 5 1 -6 13.00 2.30 5 1 -6 23.80 5.70 5 1 -6 17.40 4.20 4 1 -6 104.79 6.60 4 1 -6 109.29 6.90 4 1 -6 112.39 10.30 4 1 -6 95.49 7.20 4 1 -6 117.59 8.10 4 1 -6 105.29 7.20 -4 -1 6 111.59 6.90 -4 -1 6 96.39 6.70 3 1 -6 455.35 23.50 3 1 -6 405.06 22.90 3 1 -6 423.86 22.80 3 1 -6 386.76 22.80 -3 -1 6 415.16 22.90 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7.80 3.00 0 -7 7 10.60 3.50 0 -7 7 10.20 2.00 -1 7 -7 9.50 2.30 -1 7 -7 12.00 3.30 1 -7 7 6.00 2.90 1 -7 7 10.20 2.00 -2 7 -7 36.90 5.90 -2 7 -7 40.80 4.20 -2 7 -7 41.00 4.50 2 -7 7 41.70 4.30 2 -7 7 42.10 4.80 -3 7 -7 102.49 6.70 -3 7 -7 107.99 7.60 3 -7 7 107.49 7.30 -4 7 -7 8.40 3.90 -4 7 -7 8.20 2.10 4 -7 7 8.90 2.60 -5 7 -7 2.40 1.80 5 -7 7 1.20 2.70 -6 7 -7 10.70 2.10 6 -7 7 12.10 2.80 6 -7 7 8.90 3.60 -7 7 -7 5.30 2.10 7 -7 7 1.30 2.70 7 -7 7 4.60 2.30 -8 7 -7 3.80 2.00 8 -7 7 5.40 2.00 8 -7 7 5.40 2.70 -9 7 -7 10.70 1.90 -9 7 -7 8.40 2.60 9 -7 7 11.00 2.60 9 6 -7 7.70 1.50 9 6 -7 5.80 1.70 9 6 -7 8.60 2.70 9 6 -7 9.80 1.80 8 6 -7 18.30 2.40 8 6 -7 15.80 3.00 8 6 -7 18.50 2.70 8 6 -7 19.90 2.70 -8 -6 7 26.50 4.30 7 6 -7 14.90 2.90 7 6 -7 17.80 2.40 7 6 -7 16.60 2.60 7 6 -7 14.00 2.10 -7 -6 7 20.90 3.00 6 6 -7 12.40 2.20 6 6 -7 7.80 2.30 6 6 -7 7.30 2.10 6 6 -7 8.50 2.90 -6 -6 7 12.30 2.40 5 6 -7 59.89 4.80 5 6 -7 79.79 6.30 5 6 -7 64.09 4.80 5 6 -7 63.69 5.10 5 6 -7 62.49 4.70 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19.40 3.10 0 5 -7 17.90 3.00 0 -5 7 28.80 4.20 0 -5 7 14.10 3.10 0 -5 7 18.80 2.50 -1 5 -7 63.59 5.10 -1 5 -7 66.29 4.90 -1 5 -7 69.19 6.60 -1 5 -7 67.99 5.00 1 -5 7 64.79 5.70 1 -5 7 75.09 4.60 1 -5 7 73.39 5.90 -2 5 -7 64.99 5.30 -2 5 -7 61.89 4.50 -2 5 -7 56.09 5.10 2 -5 7 68.99 4.50 2 -5 7 65.59 5.30 -3 5 -7 69.99 6.70 -3 5 -7 82.29 5.00 3 -5 7 72.49 5.70 -4 5 -7 -0.40 3.80 -4 5 -7 3.70 1.60 4 -5 7 4.10 2.30 -5 5 -7 1.20 1.60 5 -5 7 -1.00 2.20 -6 5 -7 140.89 7.80 6 -5 7 132.49 8.10 6 -5 7 122.99 9.50 6 -5 7 117.69 8.30 7 -5 7 32.90 4.10 7 -5 7 23.50 3.60 7 -5 7 25.30 4.30 -8 5 -7 6.30 2.10 8 -5 7 10.80 2.20 8 -5 7 4.80 2.60 8 -5 7 3.60 2.10 -9 5 -7 1.50 1.90 9 -5 7 3.90 2.00 9 -5 7 9.20 2.80 9 -5 7 1.40 2.20 -10 5 -7 12.10 2.00 -10 5 -7 15.40 3.20 10 -5 7 20.60 3.70 9 4 -7 14.50 2.00 9 4 -7 15.00 2.40 9 4 -7 9.40 2.80 9 4 -7 8.20 1.90 8 4 -7 0.80 1.90 8 4 -7 0.00 2.70 8 4 -7 7.20 2.00 8 4 -7 7.40 1.90 7 4 -7 32.40 5.50 7 4 -7 33.50 4.00 7 4 -7 31.60 3.70 7 4 -7 34.10 3.70 -7 -4 7 36.80 4.90 6 4 -7 29.70 3.90 6 4 -7 30.50 3.70 6 4 -7 29.10 3.50 6 4 -7 37.60 5.40 -6 -4 7 34.90 4.70 5 4 -7 -1.00 1.80 5 4 -7 2.00 1.90 5 4 -7 6.30 2.80 5 4 -7 0.90 2.00 5 4 -7 1.90 2.30 -5 -4 7 2.40 2.40 4 4 -7 223.18 12.20 4 4 -7 214.38 14.50 4 4 -7 185.88 11.50 4 4 -7 191.48 11.50 4 4 -7 189.38 11.30 4 4 -7 196.58 11.40 -4 -4 7 197.58 11.50 3 4 -7 2.60 1.90 3 4 -7 4.30 1.80 3 4 -7 4.90 1.70 3 4 -7 2.70 1.70 3 4 -7 7.60 4.00 -3 -4 7 2.80 1.70 2 4 -7 130.69 8.10 2 4 -7 141.49 8.20 2 4 -7 135.19 8.50 2 4 -7 146.29 9.90 2 4 -7 138.59 8.20 -2 -4 7 139.39 8.10 1 4 -7 -0.10 1.80 1 4 -7 -2.00 2.60 1 4 -7 -2.20 2.80 1 4 -7 -0.80 1.60 1 4 -7 1.10 1.60 -1 -4 7 1.20 1.40 -1 -4 7 -1.30 2.20 0 4 -7 31.70 4.90 0 4 -7 33.90 3.50 0 4 -7 35.50 4.10 0 4 -7 37.10 3.30 0 -4 7 33.80 2.90 0 -4 7 33.80 3.60 -1 4 -7 107.29 6.20 -1 4 -7 102.79 7.80 -1 4 -7 99.19 6.30 -1 4 -7 71.59 17.60 -1 4 -7 99.99 6.70 -1 4 -7 107.79 6.40 1 -4 7 109.89 26.30 1 -4 7 102.79 7.50 1 -4 7 107.79 6.60 1 -4 7 115.19 6.30 -2 4 -7 564.14 29.70 -2 4 -7 475.15 30.10 -2 4 -7 536.15 29.90 -2 4 -7 539.35 29.60 2 -4 7 573.84 29.70 2 -4 7 535.65 30.00 2 -4 7 588.94 30.10 -3 4 -7 2.70 2.00 -3 4 -7 3.90 1.40 -3 4 -7 3.20 3.00 3 -4 7 5.50 2.30 -4 4 -7 9.90 1.60 -4 4 -7 11.80 4.00 4 -4 7 7.20 2.30 4 -4 7 5.70 2.80 -5 4 -7 2.10 1.50 5 -4 7 5.20 2.20 5 -4 7 -2.80 3.20 5 -4 7 1.30 2.10 -6 4 -7 27.40 3.20 6 -4 7 24.80 3.70 6 -4 7 17.80 3.40 6 -4 7 22.60 4.00 -7 4 -7 6.20 1.90 7 -4 7 3.40 2.10 7 -4 7 1.70 2.30 7 -4 7 0.70 2.70 -8 4 -7 50.29 4.10 8 -4 7 45.40 5.00 8 -4 7 53.99 4.40 8 -4 7 45.20 5.90 -9 4 -7 7.40 2.10 9 -4 7 11.40 2.50 9 -4 7 2.20 3.50 9 -4 7 6.90 2.10 9 -4 7 10.30 2.10 -10 4 -7 15.40 2.80 -10 4 -7 17.10 3.60 10 -4 7 11.80 2.20 10 -4 7 18.20 3.20 10 3 -7 20.90 2.50 10 3 -7 22.50 2.30 10 3 -7 23.10 3.60 9 3 -7 -2.60 1.80 9 3 -7 0.10 2.70 9 3 -7 0.80 1.80 8 3 -7 8.10 2.20 8 3 -7 4.80 2.90 8 3 -7 11.70 2.30 8 3 -7 10.10 2.30 7 3 -7 3.10 2.30 7 3 -7 6.70 2.20 7 3 -7 3.40 3.20 7 3 -7 5.50 2.10 -7 -3 7 10.00 2.80 6 3 -7 74.29 5.60 6 3 -7 84.59 5.80 6 3 -7 79.49 5.60 6 3 -7 75.69 6.80 -6 -3 7 82.59 6.40 5 3 -7 109.69 7.70 5 3 -7 97.69 6.60 5 3 -7 92.69 6.50 5 3 -7 121.39 16.70 5 3 -7 95.69 6.40 -5 -3 7 103.69 7.00 4 3 -7 40.60 3.70 4 3 -7 39.70 4.00 4 3 -7 53.39 8.90 4 3 -7 42.50 4.60 -4 -3 7 45.10 4.00 3 3 -7 89.19 8.50 3 3 -7 83.69 6.70 3 3 -7 70.79 5.20 3 3 -7 82.99 5.30 3 3 -7 80.19 5.50 3 3 -7 80.59 5.50 -3 -3 7 80.69 5.30 2 3 -7 21.00 2.70 2 3 -7 21.50 3.50 2 3 -7 24.80 2.70 2 3 -7 21.80 3.20 2 3 -7 23.20 3.10 -2 -3 7 16.60 2.30 -2 -3 7 24.40 2.60 1 3 -7 5.80 2.80 1 3 -7 9.50 1.70 1 3 -7 6.40 1.90 1 3 -7 8.50 1.90 1 3 -7 7.70 1.40 -1 -3 7 3.60 1.50 -1 -3 7 6.10 1.50 0 3 -7 41.20 12.50 0 3 -7 20.50 4.70 0 3 -7 29.80 3.10 0 3 -7 27.40 3.20 0 -3 7 26.90 2.70 0 -3 7 19.20 16.50 0 -3 7 28.90 3.10 -1 3 -7 30.10 12.10 -1 3 -7 10.50 1.30 -1 3 -7 10.60 2.60 -1 3 -7 8.10 1.60 -1 3 -7 8.40 1.50 -1 3 -7 9.60 2.20 1 -3 7 15.10 17.30 1 -3 7 8.40 1.60 1 -3 7 10.10 1.50 -2 3 -7 612.24 31.90 -2 3 -7 610.34 31.90 -2 3 -7 523.45 32.30 -2 3 -7 567.84 32.10 -2 3 -7 524.15 40.60 2 -3 7 620.74 31.90 2 -3 7 565.44 32.20 2 -3 7 643.54 31.90 2 -3 7 590.34 46.70 -3 3 -7 81.99 5.10 -3 3 -7 87.19 5.40 -3 3 -7 87.99 7.30 3 -3 7 88.69 5.80 3 -3 7 74.19 5.70 -4 3 -7 29.00 2.70 4 -3 7 27.90 3.60 4 -3 7 38.70 4.70 -5 3 -7 6.20 1.50 5 -3 7 6.30 2.10 5 -3 7 7.10 2.10 5 -3 7 4.30 3.40 6 -3 7 10.50 2.20 6 -3 7 11.40 2.30 -7 3 -7 14.90 2.10 7 -3 7 9.90 2.30 7 -3 7 14.70 2.40 7 -3 7 11.20 2.90 8 -3 7 29.70 4.50 8 -3 7 17.50 3.10 8 -3 7 25.80 3.70 -9 3 -7 51.99 4.20 9 -3 7 43.40 4.80 9 -3 7 51.49 5.30 9 -3 7 46.10 4.40 -10 3 -7 30.50 3.60 -10 3 -7 36.60 6.90 10 -3 7 38.60 4.70 10 -3 7 49.60 4.40 10 -3 7 42.90 4.10 10 2 -7 1.40 1.50 10 2 -7 3.50 2.00 10 2 -7 -0.50 2.10 9 2 -7 15.30 2.30 9 2 -7 11.10 3.30 9 2 -7 12.40 2.10 8 2 -7 -1.50 1.90 8 2 -7 -2.60 2.90 8 2 -7 -0.40 2.30 8 2 -7 0.80 1.90 7 2 -7 4.90 2.10 7 2 -7 3.00 2.60 7 2 -7 -0.20 3.40 7 2 -7 4.00 2.30 6 2 -7 128.89 8.60 6 2 -7 145.99 8.50 6 2 -7 143.79 8.50 6 2 -7 138.69 9.80 6 2 -7 148.29 13.80 -6 -2 7 134.89 8.90 5 2 -7 13.60 3.30 5 2 -7 10.40 2.10 5 2 -7 15.40 2.70 5 2 -7 11.80 2.20 -5 -2 7 12.50 2.70 4 2 -7 51.89 4.50 4 2 -7 53.79 4.60 4 2 -7 54.49 4.80 4 2 -7 63.39 8.80 4 2 -7 62.19 5.70 4 2 -7 53.09 4.30 -4 -2 7 52.39 4.60 3 2 -7 37.40 6.70 3 2 -7 25.40 3.30 3 2 -7 22.80 3.50 3 2 -7 30.70 4.70 3 2 -7 23.70 3.60 3 2 -7 24.10 3.10 -3 -2 7 27.20 3.10 2 2 -7 5.90 2.90 2 2 -7 5.50 1.90 2 2 -7 6.10 2.10 2 2 -7 6.90 2.20 2 2 -7 4.80 1.70 2 2 -7 8.70 1.70 -2 -2 7 5.90 1.50 -2 -2 7 2.40 1.40 1 2 -7 200.88 11.10 1 2 -7 214.88 12.20 1 2 -7 204.08 11.40 1 2 -7 181.08 11.20 1 2 -7 201.88 11.40 -1 -2 7 198.78 25.00 -1 -2 7 203.68 11.10 -1 -2 7 187.78 11.10 0 2 -7 168.28 9.80 0 2 -7 178.38 17.60 0 -2 7 180.88 23.00 0 -2 7 183.38 10.10 0 -2 7 188.58 10.10 -1 2 -7 -6.70 7.90 1 -2 7 -6.30 12.00 -2 2 -7 78.29 5.30 -2 2 -7 91.39 5.20 -2 2 -7 80.69 6.70 -2 2 -7 96.39 5.30 -2 2 -7 93.29 16.20 2 -2 7 86.99 5.40 2 -2 7 88.29 5.20 2 -2 7 96.29 16.30 -3 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2.50 7 -8 -7 4.90 2.20 7 -8 -7 4.30 1.90 7 -8 -7 3.60 2.50 -7 8 7 2.30 2.60 6 -8 -7 61.19 5.80 6 -8 -7 73.59 5.70 6 -8 -7 60.99 5.90 -6 8 7 59.89 5.50 5 -8 -7 -1.40 3.30 5 -8 -7 2.30 2.60 5 -8 -7 1.70 2.50 5 -8 -7 -0.10 2.90 -5 8 7 1.20 2.50 4 -8 -7 1.30 2.90 4 -8 -7 6.50 2.60 4 -8 -7 8.20 2.80 4 -8 -7 6.40 3.40 -4 8 7 6.40 2.30 3 -8 -7 2.10 2.50 3 -8 -7 6.20 2.40 3 -8 -7 6.00 3.40 -3 8 7 2.90 2.30 2 -8 -7 1.50 3.70 2 -8 -7 2.80 2.30 2 -8 -7 2.20 2.50 -2 8 7 1.10 2.00 1 -8 -7 88.69 6.80 1 -8 -7 88.89 9.00 -1 8 7 96.99 6.20 0 8 7 -0.60 1.60 0 8 7 2.20 3.60 -1 -8 -7 85.99 6.30 -1 -8 -7 91.09 6.80 1 8 7 93.79 5.90 1 8 7 88.29 7.20 -2 -8 -7 1.70 1.70 -2 -8 -7 0.90 2.70 2 8 7 4.10 2.30 2 8 7 2.80 1.90 -3 -8 -7 81.49 5.40 -3 -8 -7 71.59 7.50 3 8 7 94.69 6.20 -4 -8 -7 7.10 1.60 -4 -8 -7 8.70 4.20 4 8 7 7.30 2.00 4 8 7 5.90 3.00 -5 -8 -7 55.39 4.30 5 8 7 63.99 6.50 5 8 7 61.09 4.60 -6 -8 -7 170.08 10.00 6 8 7 166.78 10.00 6 8 7 172.88 9.90 6 8 7 169.48 11.60 -7 -8 -7 191.88 11.20 7 8 7 197.58 12.80 7 8 7 188.08 11.20 7 8 7 198.38 11.10 -8 -8 -7 38.00 3.40 8 8 7 31.10 3.60 8 8 7 32.10 3.30 8 8 7 31.40 4.40 8 8 7 36.60 3.40 -9 -8 -7 9.40 2.00 9 8 7 9.90 1.80 9 8 7 10.30 1.80 -10 -8 -7 15.40 2.30 10 8 7 20.60 2.50 10 8 7 21.60 2.50 -11 -8 -7 -2.20 1.70 11 8 7 -0.10 1.20 11 8 7 1.00 1.30 7 -9 -7 22.80 3.50 7 -9 -7 23.50 3.70 7 -9 -7 21.20 3.00 6 -9 -7 -1.80 2.60 6 -9 -7 -1.20 2.10 6 -9 -7 -2.00 2.20 -6 9 7 -4.40 2.20 5 -9 -7 16.20 4.20 5 -9 -7 20.00 3.80 -5 9 7 13.00 2.80 4 -9 -7 2.20 2.90 4 -9 -7 7.90 3.60 4 -9 -7 10.50 2.90 -4 9 7 5.50 2.30 3 -9 -7 11.40 3.60 3 -9 -7 12.90 2.80 3 -9 -7 3.70 3.10 -3 9 7 10.10 2.30 2 -9 -7 8.60 2.90 2 -9 -7 11.70 3.90 -2 9 7 8.40 2.40 1 -9 -7 -6.20 4.00 1 -9 -7 1.70 2.70 -1 9 7 6.50 4.60 -1 9 7 1.00 2.00 0 -9 -7 7.80 2.70 0 9 7 8.70 3.70 0 9 7 7.60 2.00 -1 -9 -7 63.99 5.80 1 9 7 64.29 6.20 1 9 7 65.29 4.80 -2 -9 -7 113.79 8.30 -2 -9 -7 118.69 7.50 2 9 7 109.89 8.00 2 9 7 125.39 7.80 -3 -9 -7 3.30 3.80 -3 -9 -7 1.90 1.80 3 9 7 3.30 2.10 -4 -9 -7 28.00 3.40 -4 -9 -7 39.00 6.30 4 9 7 27.10 3.60 -5 -9 -7 240.58 14.20 5 9 7 252.17 14.20 5 9 7 237.58 14.40 5 9 7 267.47 15.40 -6 -9 -7 25.90 3.20 6 9 7 23.60 3.90 6 9 7 23.60 3.20 6 9 7 24.70 2.90 -7 -9 -7 2.60 1.70 7 9 7 0.00 1.70 7 9 7 2.50 2.00 -8 -9 -7 11.50 2.00 8 9 7 14.00 2.10 8 9 7 9.90 1.90 8 9 7 8.80 2.30 8 9 7 11.40 1.90 -9 -9 -7 36.80 3.70 9 9 7 42.30 3.30 9 9 7 38.20 3.20 -10 -9 -7 0.50 1.70 10 9 7 2.10 1.50 10 9 7 0.20 1.30 -11 -9 -7 4.10 2.00 11 9 7 4.80 1.30 11 9 7 5.70 1.20 6 -10 -7 11.80 2.70 6 -10 -7 11.40 2.10 6 -10 -7 8.90 2.20 -6 10 7 6.40 2.20 5 -10 -7 16.50 2.80 5 -10 -7 12.70 3.20 5 -10 -7 19.20 3.40 5 -10 -7 14.60 2.60 -5 10 7 16.60 2.70 4 -10 -7 13.30 3.00 4 -10 -7 16.00 3.30 -4 10 7 12.80 2.60 3 -10 -7 11.50 3.20 3 -10 -7 14.40 3.10 3 -10 -7 12.20 3.60 -3 10 7 7.20 2.40 2 -10 -7 71.69 7.50 2 -10 -7 81.19 7.80 2 -10 -7 77.19 6.30 1 -10 -7 14.10 4.20 1 -10 -7 7.60 2.80 -1 10 7 7.60 2.20 0 -10 -7 0.00 2.50 0 10 7 -1.50 2.00 0 10 7 1.60 3.60 -1 -10 -7 14.70 3.30 1 10 7 20.90 3.50 1 10 7 19.00 2.70 -2 -10 -7 26.10 4.40 -2 -10 -7 31.40 5.10 2 10 7 29.70 4.60 -3 -10 -7 149.49 10.40 -3 -10 -7 150.18 9.30 3 10 7 156.78 9.50 -4 -10 -7 31.40 5.10 -4 -10 -7 25.40 3.50 4 10 7 27.80 3.70 -5 -10 -7 17.00 3.00 5 10 7 12.30 2.20 -6 -10 -7 22.70 3.80 6 10 7 24.00 3.20 6 10 7 24.30 3.10 -7 -10 -7 1.10 1.80 7 10 7 1.80 1.80 7 10 7 0.90 1.90 7 10 7 2.10 2.10 -8 -10 -7 29.30 3.40 8 10 7 30.10 2.90 8 10 7 26.10 3.20 8 10 7 21.30 3.50 8 10 7 29.90 3.20 -9 -10 -7 0.80 1.70 9 10 7 0.90 1.40 9 10 7 0.70 1.60 -10 -10 -7 28.50 3.10 10 10 7 31.30 2.60 10 10 7 32.30 2.80 6 -11 -7 1.90 1.70 6 -11 -7 0.80 1.80 -6 11 7 -1.30 2.10 5 -11 -7 78.69 5.60 5 -11 -7 69.89 5.80 5 -11 -7 73.99 6.10 5 -11 -7 71.49 5.10 4 -11 -7 20.90 2.70 4 -11 -7 20.00 2.90 4 -11 -7 20.80 3.40 -4 11 7 15.80 2.70 3 -11 -7 13.20 3.10 3 -11 -7 22.60 3.70 3 -11 -7 23.40 4.60 -3 11 7 13.20 2.60 2 -11 -7 2.00 2.90 2 -11 -7 1.20 3.00 -2 11 7 0.40 2.20 1 -11 -7 6.60 3.10 1 -11 -7 2.70 3.60 -1 11 7 2.30 2.10 -1 11 7 11.90 4.60 0 -11 -7 55.59 5.70 0 11 7 67.69 6.90 -1 -11 -7 18.20 3.50 1 11 7 16.90 3.40 -2 -11 -7 120.09 8.50 2 11 7 122.59 8.20 -3 -11 -7 14.80 3.80 -3 -11 -7 7.10 2.50 3 11 7 8.30 2.40 -4 -11 -7 4.60 4.20 -4 -11 -7 0.10 2.40 4 11 7 0.60 2.00 -5 -11 -7 73.19 5.20 5 11 7 73.69 5.40 -6 -11 -7 18.20 2.50 6 11 7 20.10 2.30 6 11 7 13.00 2.20 -7 -11 -7 15.90 3.00 7 11 7 14.30 2.50 7 11 7 14.50 2.40 -8 -11 -7 3.10 1.80 8 11 7 4.80 1.50 8 11 7 3.60 2.00 8 11 7 5.10 1.50 8 11 7 3.40 1.80 -9 -11 -7 94.39 6.00 9 11 7 104.79 5.70 9 11 7 86.49 5.90 -10 -11 -7 2.80 1.90 10 11 7 0.50 1.00 5 -12 -7 2.40 3.00 5 -12 -7 4.20 1.70 -5 12 7 1.10 2.00 4 -12 -7 10.90 2.20 4 -12 -7 12.10 2.80 3 -12 -7 7.80 2.90 -3 12 7 0.40 2.20 2 -12 -7 -2.00 3.00 2 -12 -7 0.10 3.10 -2 12 7 -0.50 2.20 1 -12 -7 11.00 2.90 1 -12 -7 3.20 3.20 -1 12 7 5.70 2.30 -1 12 7 8.90 3.80 0 -12 -7 4.80 2.90 0 12 7 3.80 3.50 0 12 7 7.30 2.60 -1 -12 -7 144.09 9.70 1 12 7 154.08 9.80 -2 -12 -7 2.30 2.80 2 12 7 -0.60 2.40 -3 -12 -7 7.80 3.60 -3 -12 -7 8.00 2.90 3 12 7 6.20 2.50 3 12 7 5.90 2.40 -4 -12 -7 2.60 2.30 -4 -12 -7 6.60 3.80 4 12 7 4.20 2.10 4 12 7 6.90 2.10 -5 -12 -7 4.20 2.20 5 12 7 2.70 1.90 5 12 7 5.40 1.70 -6 -12 -7 0.20 1.90 6 12 7 1.90 1.50 -7 -12 -7 15.20 2.40 7 12 7 16.50 2.60 7 12 7 19.30 2.40 -8 -12 -7 77.29 5.30 8 12 7 79.19 4.80 8 12 7 71.09 5.00 8 12 7 81.09 4.80 -9 -12 -7 66.19 4.70 9 12 7 64.89 4.10 4 -13 -7 15.20 2.70 -4 13 7 21.30 3.60 3 -13 -7 6.70 2.00 -3 13 7 11.30 2.20 2 -13 -7 -1.00 2.00 -2 13 7 5.30 2.50 -1 13 7 2.10 3.70 0 -13 -7 2.60 2.20 0 13 7 3.00 3.20 -1 -13 -7 7.60 2.40 1 13 7 4.00 2.40 -2 -13 -7 111.59 7.50 -3 -13 -7 -3.70 2.70 -4 -13 -7 3.60 2.90 -4 -13 -7 3.90 3.80 4 13 7 0.10 1.90 4 13 7 1.90 1.90 -5 -13 -7 2.10 2.30 5 13 7 0.30 1.70 5 13 7 2.40 1.60 -6 -13 -7 33.30 3.70 6 13 7 38.20 3.30 6 13 7 35.20 3.00 -7 -13 -7 23.10 3.10 7 13 7 28.90 2.50 7 13 7 27.00 2.70 -8 -13 -7 8.60 1.90 8 13 7 13.20 1.80 8 13 7 7.80 2.10 2 -14 -7 5.20 1.90 1 -14 -7 -2.30 2.00 -1 14 7 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9 -8 18.70 2.10 7 9 -8 17.10 2.00 7 9 -8 18.20 2.40 -7 -9 8 18.30 2.80 6 9 -8 1.70 1.50 6 9 -8 -1.60 1.30 6 9 -8 0.80 1.50 6 9 -8 1.00 2.10 -6 -9 8 0.60 1.70 5 9 -8 26.00 2.80 5 9 -8 24.50 3.00 5 9 -8 26.70 4.00 5 9 -8 25.50 2.70 -5 -9 8 19.60 3.20 4 9 -8 22.60 2.70 4 9 -8 20.70 3.00 -4 -9 8 18.60 3.30 3 9 -8 7.30 2.00 3 9 -8 7.00 1.90 3 9 -8 2.80 3.90 -3 -9 8 2.00 2.00 2 9 -8 64.99 5.70 2 9 -8 68.09 5.20 -2 -9 8 70.89 5.10 1 9 -8 2.60 2.20 1 9 -8 3.30 3.80 -1 -9 8 1.50 2.00 0 9 -8 4.30 3.30 0 9 -8 -1.30 2.30 0 -9 8 1.10 3.40 0 -9 8 1.30 2.00 -1 9 -8 19.50 3.00 -1 9 -8 21.40 3.50 1 -9 8 20.40 3.70 1 -9 8 23.20 3.60 -2 9 -8 6.60 3.10 -2 9 -8 12.30 2.90 2 -9 8 6.80 2.60 -3 9 -8 2.60 2.90 -3 9 -8 6.70 3.00 3 -9 8 1.40 2.50 -4 9 -8 29.70 5.00 -4 9 -8 34.50 4.50 4 -9 8 29.30 4.20 -5 9 -8 0.00 3.90 -5 9 -8 -1.00 2.40 -5 9 -8 -2.50 2.60 5 -9 8 2.50 2.30 -6 9 -8 1.70 2.50 -6 9 -8 -2.80 2.20 6 -9 8 2.70 2.20 -7 9 -8 -3.60 2.00 -7 9 -8 0.30 2.10 7 -9 8 -0.40 1.60 7 8 -8 10.10 2.20 7 8 -8 14.50 1.90 7 8 -8 16.10 2.20 7 8 -8 16.10 2.10 -7 -8 8 14.70 2.20 6 8 -8 17.30 2.50 6 8 -8 14.60 2.70 6 8 -8 18.30 2.20 6 8 -8 16.80 2.50 -6 -8 8 17.30 3.20 5 8 -8 -0.60 1.70 5 8 -8 1.20 1.70 5 8 -8 4.20 2.60 5 8 -8 0.90 1.60 5 8 -8 0.20 1.90 -5 -8 8 -1.00 1.90 4 8 -8 104.09 6.90 4 8 -8 96.69 5.80 4 8 -8 87.09 5.80 4 8 -8 84.79 5.70 4 8 -8 87.39 6.00 -4 -8 8 79.99 6.00 3 8 -8 9.10 2.10 3 8 -8 5.10 2.40 3 8 -8 5.80 1.90 3 8 -8 7.00 2.00 -3 -8 8 2.50 1.90 2 8 -8 35.00 5.00 2 8 -8 33.30 3.90 2 8 -8 33.00 3.40 2 8 -8 34.80 3.60 2 8 -8 29.10 3.70 -2 -8 8 30.60 4.80 1 8 -8 0.20 2.20 1 8 -8 1.00 3.40 -1 -8 8 1.90 1.90 0 8 -8 137.89 9.10 0 8 -8 161.38 10.10 0 -8 8 142.39 10.10 0 -8 8 153.38 8.90 -1 8 -8 22.30 3.00 -1 8 -8 26.10 5.20 1 -8 8 23.40 3.50 1 -8 8 20.60 2.70 -2 8 -8 26.10 5.40 -2 8 -8 26.00 4.40 -3 8 -8 57.79 6.30 -3 8 -8 55.69 5.50 3 -8 8 51.39 5.30 -4 8 -8 14.20 3.60 -4 8 -8 16.70 2.50 -4 8 -8 15.50 3.60 4 -8 8 12.70 3.00 -5 8 -8 33.40 3.80 -5 8 -8 40.50 5.40 -5 8 -8 24.70 4.10 5 -8 8 38.00 4.20 -6 8 -8 1.20 2.10 -6 8 -8 -1.70 2.80 6 -8 8 2.60 2.30 -7 8 -8 1.40 1.90 -7 8 -8 -1.90 2.50 7 -8 8 2.70 1.90 -8 8 -8 0.50 2.30 -8 8 -8 -2.80 1.80 8 -8 8 1.60 1.60 8 7 -8 1.80 1.30 8 7 -8 0.30 1.40 8 7 -8 3.20 1.40 8 7 -8 0.40 2.00 -8 -7 8 4.10 2.20 7 7 -8 22.40 2.70 7 7 -8 28.80 2.70 7 7 -8 19.00 3.80 7 7 -8 26.90 3.00 -7 -7 8 30.40 3.40 6 7 -8 8.90 1.90 6 7 -8 8.60 1.80 6 7 -8 9.10 1.90 6 7 -8 7.90 2.80 -6 -7 8 8.90 2.30 5 7 -8 20.50 3.00 5 7 -8 23.60 3.10 5 7 -8 29.00 3.10 5 7 -8 30.10 4.70 5 7 -8 20.30 2.60 -5 -7 8 23.50 3.50 4 7 -8 8.80 2.00 4 7 -8 14.70 3.10 4 7 -8 8.00 2.00 4 7 -8 7.80 2.00 4 7 -8 5.80 2.10 -4 -7 8 6.70 2.00 3 7 -8 4.40 1.90 3 7 -8 4.20 1.80 3 7 -8 3.90 2.20 3 7 -8 8.00 2.00 -3 -7 8 1.60 1.90 2 7 -8 20.70 4.10 2 7 -8 21.80 3.10 2 7 -8 22.60 3.30 2 7 -8 23.90 3.00 2 7 -8 20.50 2.40 -2 -7 8 18.90 3.30 1 7 -8 29.50 6.20 1 7 -8 25.10 3.60 1 7 -8 24.90 2.90 -1 -7 8 27.80 3.40 0 7 -8 95.79 6.80 0 7 -8 110.09 7.90 0 -7 8 100.89 6.50 0 -7 8 108.29 8.30 -1 7 -8 33.10 4.40 -1 7 -8 42.30 5.70 1 -7 8 38.10 5.20 1 -7 8 38.40 3.70 -2 7 -8 7.20 2.60 -2 7 -8 8.50 3.00 2 -7 8 8.20 2.70 -3 7 -8 12.30 2.50 -3 7 -8 12.80 3.20 3 -7 8 15.70 3.00 -4 7 -8 40.50 4.00 -4 7 -8 51.89 5.90 4 -7 8 48.70 5.00 -5 7 -8 36.00 5.50 -5 7 -8 31.00 3.60 -5 7 -8 25.40 4.10 5 -7 8 38.80 4.40 -6 7 -8 -5.00 3.20 -6 7 -8 -3.20 2.20 6 -7 8 5.10 2.70 -7 7 -8 4.60 2.20 -7 7 -8 1.30 3.00 7 -7 8 9.20 2.20 -8 7 -8 4.60 1.90 -8 7 -8 2.70 2.70 8 -7 8 5.50 1.90 -9 7 -8 31.60 4.10 -9 7 -8 27.00 3.00 8 6 -8 19.30 2.40 8 6 -8 22.10 3.80 8 6 -8 22.50 2.80 8 6 -8 23.20 2.70 -8 -6 8 20.00 2.80 7 6 -8 8.00 2.10 7 6 -8 6.40 2.70 7 6 -8 10.50 1.90 7 6 -8 10.00 1.90 -7 -6 8 7.30 2.40 6 6 -8 35.60 3.80 6 6 -8 39.40 3.40 6 6 -8 36.70 3.50 6 6 -8 35.30 4.70 -6 -6 8 38.30 4.00 5 6 -8 1.40 1.90 5 6 -8 3.70 2.80 5 6 -8 -1.40 2.00 5 6 -8 1.40 2.10 5 6 -8 2.30 1.90 -5 -6 8 0.20 1.90 4 6 -8 40.90 4.90 4 6 -8 32.70 3.40 4 6 -8 32.80 3.30 4 6 -8 31.40 3.50 4 6 -8 29.00 3.80 -4 -6 8 26.90 3.60 3 6 -8 18.40 3.10 3 6 -8 27.90 4.80 3 6 -8 18.70 2.60 3 6 -8 19.30 2.30 3 6 -8 22.30 3.10 -3 -6 8 18.20 2.50 2 6 -8 37.00 3.60 2 6 -8 32.10 3.50 2 6 -8 37.30 3.40 2 6 -8 35.00 3.50 2 6 -8 33.10 6.20 -2 -6 8 29.20 3.50 1 6 -8 8.10 2.00 1 6 -8 10.80 2.10 1 6 -8 6.50 3.20 1 6 -8 10.20 2.20 -1 -6 8 6.30 1.90 0 6 -8 4.50 2.90 0 6 -8 -1.40 3.20 0 6 -8 0.20 1.80 0 -6 8 7.20 4.00 0 -6 8 2.20 1.80 -1 6 -8 230.78 13.60 -1 6 -8 215.58 12.90 1 -6 8 228.88 12.60 1 -6 8 217.88 13.40 -2 6 -8 3.00 2.50 -2 6 -8 1.70 2.90 -2 6 -8 0.00 2.10 2 -6 8 2.20 2.20 2 -6 8 1.90 2.70 -3 6 -8 53.49 4.30 -3 6 -8 54.59 5.40 -3 6 -8 46.50 6.00 3 -6 8 45.80 4.90 -4 6 -8 7.00 2.20 -4 6 -8 6.50 3.70 4 -6 8 8.20 2.60 -5 6 -8 13.00 2.30 5 -6 8 23.90 4.00 -6 6 -8 4.90 2.10 6 -6 8 11.10 2.80 -7 6 -8 1.60 2.20 7 -6 8 3.10 4.20 7 -6 8 8.30 2.40 -8 6 -8 0.60 2.00 8 -6 8 8.50 2.90 8 -6 8 5.20 2.90 8 -6 8 5.20 2.00 -9 6 -8 22.30 2.80 -9 6 -8 20.70 4.30 9 -6 8 28.90 5.40 9 5 -8 0.20 2.30 9 5 -8 4.20 1.70 9 5 -8 4.20 1.40 8 5 -8 33.90 4.30 8 5 -8 38.60 3.30 8 5 -8 38.80 3.20 8 5 -8 36.50 3.40 -8 -5 8 29.80 5.20 7 5 -8 82.59 5.30 7 5 -8 70.19 6.20 7 5 -8 64.29 4.90 7 5 -8 81.49 5.60 -7 -5 8 74.99 5.60 6 5 -8 68.59 5.00 6 5 -8 69.69 5.00 6 5 -8 73.09 5.40 6 5 -8 72.99 6.40 -6 -5 8 80.09 5.50 5 5 -8 4.50 2.20 5 5 -8 5.60 2.10 5 5 -8 10.30 2.10 5 5 -8 12.80 3.10 5 5 -8 7.40 2.10 -5 -5 8 8.60 2.20 4 5 -8 7.20 2.90 4 5 -8 0.80 2.00 4 5 -8 3.40 1.80 4 5 -8 13.20 5.10 4 5 -8 2.60 1.80 4 5 -8 3.00 1.80 -4 -5 8 1.80 2.10 3 5 -8 65.19 7.90 3 5 -8 60.39 4.40 3 5 -8 62.59 4.50 3 5 -8 59.59 4.80 3 5 -8 57.19 4.50 -3 -5 8 58.09 4.60 2 5 -8 22.50 3.10 2 5 -8 22.80 3.10 2 5 -8 27.40 4.80 2 5 -8 22.80 3.10 -2 -5 8 20.50 3.00 1 5 -8 217.78 13.30 1 5 -8 248.08 13.70 1 5 -8 201.08 12.60 1 5 -8 225.58 12.80 1 5 -8 232.78 12.60 -1 -5 8 217.08 12.60 0 5 -8 3.20 2.70 0 5 -8 2.70 2.00 0 5 -8 1.00 2.00 0 -5 8 1.20 1.50 0 -5 8 0.60 3.80 -1 5 -8 41.20 4.00 -1 5 -8 42.00 5.40 1 -5 8 37.40 5.20 1 -5 8 42.80 3.50 -2 5 -8 8.50 2.00 -2 5 -8 6.80 2.40 -2 5 -8 8.60 5.00 2 -5 8 10.90 2.10 2 -5 8 9.30 2.70 -3 5 -8 11.70 3.10 -3 5 -8 15.00 2.10 3 -5 8 15.70 2.80 -4 5 -8 7.70 2.00 -4 5 -8 4.20 3.70 4 -5 8 10.50 2.50 -5 5 -8 2.30 2.00 5 -5 8 9.00 2.40 -6 5 -8 47.20 4.10 -7 5 -8 3.00 2.10 7 -5 8 4.20 3.30 7 -5 8 -1.30 2.80 7 -5 8 8.70 2.50 -8 5 -8 36.00 3.90 8 -5 8 47.40 5.20 8 -5 8 36.80 5.70 -9 5 -8 21.30 3.00 9 -5 8 20.00 3.10 9 -5 8 18.40 3.10 9 -5 8 27.70 5.00 9 -5 8 16.00 2.80 -10 5 -8 -1.10 1.60 -10 5 -8 1.80 2.60 10 -5 8 2.80 3.00 9 4 -8 4.20 1.50 9 4 -8 -0.70 2.20 9 4 -8 2.60 1.50 8 4 -8 2.90 2.10 8 4 -8 4.80 2.90 8 4 -8 8.00 1.90 8 4 -8 3.70 1.80 -8 -4 8 3.30 2.90 7 4 -8 35.10 3.80 7 4 -8 39.00 3.50 7 4 -8 29.40 4.80 -7 -4 8 39.30 4.20 6 4 -8 13.20 2.30 6 4 -8 12.70 3.40 6 4 -8 11.40 2.20 6 4 -8 12.10 2.40 -6 -4 8 16.20 2.50 5 4 -8 23.40 6.00 5 4 -8 15.80 2.40 5 4 -8 7.80 2.50 5 4 -8 11.30 2.20 5 4 -8 12.50 3.00 5 4 -8 17.40 2.30 -5 -4 8 14.20 2.50 4 4 -8 71.89 5.20 4 4 -8 74.99 5.60 4 4 -8 89.79 6.60 4 4 -8 79.19 5.40 4 4 -8 78.59 5.40 4 4 -8 87.39 9.50 -4 -4 8 79.99 5.60 3 4 -8 24.30 3.30 3 4 -8 25.80 3.70 3 4 -8 27.60 2.90 3 4 -8 22.40 3.30 -3 -4 8 22.70 3.30 2 4 -8 126.99 8.00 2 4 -8 129.79 9.10 2 4 -8 127.99 8.10 2 4 -8 117.69 7.60 2 4 -8 120.59 7.50 -2 -4 8 120.89 7.40 1 4 -8 9.40 2.00 1 4 -8 12.00 3.00 1 4 -8 8.60 2.00 1 4 -8 9.60 1.90 1 4 -8 9.30 3.00 -1 -4 8 10.20 1.80 0 4 -8 44.10 5.30 0 4 -8 39.50 3.80 0 4 -8 39.10 4.10 0 -4 8 44.90 3.40 0 -4 8 42.60 6.60 -1 4 -8 2.50 2.60 -1 4 -8 4.00 2.50 -1 4 -8 4.80 2.10 1 -4 8 3.30 2.90 1 -4 8 0.80 3.00 1 -4 8 3.30 1.40 -2 4 -8 4.60 1.60 -2 4 -8 4.80 2.70 -2 4 -8 1.00 2.20 -2 4 -8 0.80 2.40 2 -4 8 3.40 2.60 2 -4 8 4.60 1.80 -3 4 -8 4.90 1.60 -3 4 -8 4.90 2.70 -3 4 -8 5.60 2.90 3 -4 8 6.20 2.30 -4 4 -8 26.60 3.20 -4 4 -8 27.10 3.80 4 -4 8 33.70 4.00 -5 4 -8 17.40 3.10 5 -4 8 22.50 3.80 -6 4 -8 11.50 2.20 6 -4 8 10.70 3.60 6 -4 8 5.30 2.70 6 -4 8 12.00 2.60 7 -4 8 10.10 3.30 7 -4 8 11.90 2.50 -8 4 -8 1.00 2.20 -8 4 -8 0.90 3.40 8 -4 8 3.20 2.70 8 -4 8 7.60 2.20 -10 4 -8 41.60 5.70 -10 4 -8 35.30 3.20 10 -4 8 34.70 4.50 10 -4 8 37.20 4.50 9 3 -8 -0.30 2.30 9 3 -8 2.50 1.60 9 3 -8 -1.20 1.60 8 3 -8 -0.10 1.90 8 3 -8 -1.40 2.30 8 3 -8 1.00 1.90 8 3 -8 -0.40 2.80 7 3 -8 70.89 4.80 7 3 -8 64.29 6.30 7 3 -8 66.79 5.00 7 3 -8 58.39 4.70 -7 -3 8 66.39 5.40 6 3 -8 0.10 2.10 6 3 -8 4.70 2.10 6 3 -8 0.80 2.90 6 3 -8 3.20 2.30 5 3 -8 48.70 5.30 5 3 -8 58.49 4.50 5 3 -8 53.49 4.60 5 3 -8 55.99 10.10 5 3 -8 56.39 5.90 5 3 -8 56.89 4.60 -5 -3 8 58.69 4.80 4 3 -8 0.80 2.00 4 3 -8 1.60 4.40 4 3 -8 6.40 2.70 4 3 -8 2.90 1.90 4 3 -8 0.90 2.00 4 3 -8 0.60 1.90 -4 -3 8 0.30 1.90 3 3 -8 60.09 4.40 3 3 -8 56.39 5.30 3 3 -8 54.89 7.90 3 3 -8 56.79 4.80 3 3 -8 67.89 7.50 3 3 -8 65.29 5.20 -3 -3 8 62.09 4.50 2 3 -8 125.89 7.60 2 3 -8 129.09 9.00 2 3 -8 121.09 8.00 2 3 -8 123.49 7.40 2 3 -8 121.79 7.30 -2 -3 8 120.89 7.30 1 3 -8 9.50 2.90 1 3 -8 5.70 1.80 1 3 -8 5.60 2.70 1 3 -8 2.50 1.90 1 3 -8 5.20 1.90 -1 -3 8 4.40 1.40 0 3 -8 115.39 7.40 0 3 -8 118.49 7.60 0 3 -8 137.59 8.50 0 -3 8 117.99 7.70 0 -3 8 131.29 7.30 -1 3 -8 26.40 27.60 -1 3 -8 56.39 5.90 -1 3 -8 55.29 3.90 -1 3 -8 62.49 5.60 -1 3 -8 57.79 4.40 -1 3 -8 58.19 5.00 -1 3 -8 47.50 4.10 1 -3 8 65.29 3.90 1 -3 8 -16.30 33.60 1 -3 8 63.19 5.80 1 -3 8 61.09 4.80 -2 3 -8 129.99 8.60 -2 3 -8 135.69 7.50 -2 3 -8 126.29 7.60 -2 3 -8 126.19 8.10 2 -3 8 126.19 7.90 2 -3 8 133.59 7.60 2 -3 8 125.39 8.20 -3 3 -8 82.19 6.50 -3 3 -8 90.09 6.90 -3 3 -8 92.69 5.30 -3 3 -8 73.59 5.80 3 -3 8 82.99 5.90 3 -3 8 72.19 5.60 -4 3 -8 96.09 7.90 -4 3 -8 117.09 8.20 -4 3 -8 106.59 6.60 4 -3 8 117.69 7.10 -5 3 -8 34.80 3.40 5 -3 8 36.70 3.90 -6 3 -8 3.00 2.00 6 -3 8 4.90 3.40 6 -3 8 5.30 2.10 6 -3 8 4.60 2.30 -7 3 -8 81.99 6.20 7 -3 8 111.89 6.40 7 -3 8 98.29 7.00 7 -3 8 85.79 8.10 -8 3 -8 102.59 7.10 -8 3 -8 101.79 8.80 8 -3 8 105.29 8.50 8 -3 8 125.99 7.80 8 -3 8 124.49 7.20 -9 3 -8 88.29 6.20 -9 3 -8 100.49 7.70 9 -3 8 86.29 6.60 9 -3 8 98.29 6.00 9 -3 8 93.99 6.80 -10 3 -8 29.50 6.00 -10 3 -8 18.70 2.80 10 -3 8 19.50 3.90 10 -3 8 15.90 2.60 9 2 -8 5.30 1.80 9 2 -8 8.60 1.70 9 2 -8 3.90 2.50 8 2 -8 -2.00 2.70 8 2 -8 -0.20 1.90 8 2 -8 4.50 1.90 7 2 -8 7.90 3.20 7 2 -8 12.60 2.30 7 2 -8 12.00 2.50 7 2 -8 8.90 2.30 -7 -2 8 14.80 2.90 6 2 -8 -0.80 3.00 6 2 -8 4.70 2.20 6 2 -8 6.70 2.40 6 2 -8 5.90 2.70 6 2 -8 8.30 5.90 -6 -2 8 8.90 2.30 5 2 -8 11.10 5.00 5 2 -8 8.20 2.00 5 2 -8 7.20 3.00 5 2 -8 7.10 2.00 5 2 -8 8.50 2.60 -5 -2 8 8.30 2.40 4 2 -8 27.70 4.10 4 2 -8 31.10 5.30 4 2 -8 26.20 3.80 4 2 -8 32.70 4.90 4 2 -8 26.10 3.50 -4 -2 8 35.40 3.60 3 2 -8 0.90 1.70 3 2 -8 -0.10 1.90 3 2 -8 2.40 2.20 3 2 -8 -1.20 3.40 3 2 -8 0.00 1.70 3 2 -8 5.20 2.60 -3 -2 8 -0.10 1.60 2 2 -8 51.19 4.70 2 2 -8 51.79 4.10 2 2 -8 48.90 5.50 2 2 -8 55.29 6.20 2 2 -8 50.39 4.40 2 2 -8 45.20 3.80 -2 -2 8 50.29 3.80 1 2 -8 49.60 3.90 1 2 -8 56.69 4.30 1 2 -8 47.20 5.40 1 2 -8 55.19 5.50 1 2 -8 57.19 4.40 -1 -2 8 52.59 4.30 -1 -2 8 57.79 3.80 0 2 -8 97.29 6.10 0 2 -8 84.49 5.70 0 2 -8 85.99 5.80 0 2 -8 95.09 6.90 0 -2 8 95.99 5.80 0 -2 8 99.79 5.60 -1 2 -8 48.20 5.00 -1 2 -8 48.70 4.30 -1 2 -8 44.20 3.50 -1 2 -8 48.90 3.10 -1 2 -8 45.10 4.00 -1 2 -8 41.80 14.20 -1 2 -8 43.20 3.60 1 -2 8 43.00 5.30 1 -2 8 51.29 3.70 1 -2 8 51.79 19.30 1 -2 8 53.79 3.40 -2 2 -8 13.20 1.70 -2 2 -8 15.10 2.80 -2 2 -8 13.80 2.10 -2 2 -8 15.00 2.50 2 -2 8 17.50 2.70 2 -2 8 14.50 1.90 -3 2 -8 62.79 4.80 -3 2 -8 68.79 6.10 -3 2 -8 73.99 4.40 -3 2 -8 68.79 5.70 3 -2 8 57.49 4.90 3 -2 8 70.79 5.00 -4 2 -8 4.20 1.50 -4 2 -8 2.80 3.50 -4 2 -8 5.60 2.70 4 -2 8 7.50 2.20 -5 2 -8 40.20 5.50 -5 2 -8 44.50 3.60 5 -2 8 37.70 5.40 5 -2 8 54.89 5.30 -6 2 -8 25.80 3.20 6 -2 8 24.50 5.10 -7 2 -8 363.36 23.70 -7 2 -8 404.56 23.00 7 -2 8 428.06 23.80 7 -2 8 466.75 23.10 7 -2 8 421.56 23.30 -8 2 -8 253.67 16.10 8 -2 8 281.47 15.40 8 -2 8 282.47 15.00 8 -2 8 235.18 15.70 -9 2 -8 27.60 3.40 -9 2 -8 26.40 6.10 9 -2 8 20.60 3.60 9 -2 8 19.50 2.90 9 -2 8 17.50 2.70 9 1 -8 6.40 1.80 9 1 -8 0.20 2.40 9 1 -8 4.70 1.80 8 1 -8 31.40 3.20 8 1 -8 25.80 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16.20 3.00 2 7 -9 12.40 3.90 1 7 -9 16.90 2.50 1 7 -9 13.90 2.50 1 7 -9 16.50 3.70 -1 -7 9 16.50 3.00 0 7 -9 113.09 8.00 0 7 -9 91.59 6.70 0 -7 9 97.69 6.30 0 -7 9 95.49 8.00 -1 7 -9 40.60 5.60 -1 7 -9 25.70 4.10 1 -7 9 33.70 3.70 1 -7 9 30.60 5.00 -2 7 -9 6.70 3.10 -2 7 -9 5.60 2.70 2 -7 9 6.40 2.90 -3 7 -9 17.20 3.20 -3 7 -9 15.20 3.40 3 -7 9 16.00 3.10 -4 7 -9 169.38 10.20 -4 7 -9 176.88 11.00 -4 7 -9 178.28 11.30 4 -7 9 178.18 10.70 -5 7 -9 -7.20 4.00 -5 7 -9 0.40 2.10 -5 7 -9 1.40 3.00 5 -7 9 5.30 2.80 -6 7 -9 -0.20 4.10 -6 7 -9 6.30 2.20 6 -7 9 18.50 5.30 -7 7 -9 18.80 3.10 -7 7 -9 26.40 4.60 7 -7 9 30.70 3.40 -8 7 -9 7.50 2.00 -8 7 -9 6.10 2.40 8 -7 9 5.40 1.70 8 6 -9 31.40 2.70 8 6 -9 31.80 3.50 8 6 -9 29.50 2.50 7 6 -9 15.60 2.80 7 6 -9 17.50 2.30 7 6 -9 20.50 2.60 7 6 -9 11.70 2.00 -7 -6 9 21.90 3.00 6 6 -9 76.39 5.80 6 6 -9 69.09 5.10 6 6 -9 73.59 4.90 6 6 -9 75.09 4.90 -6 -6 9 76.39 5.20 5 6 -9 35.80 3.30 5 6 -9 37.40 3.70 5 6 -9 30.10 3.30 5 6 -9 30.00 4.80 -5 -6 9 32.70 3.70 4 6 -9 3.40 1.90 4 6 -9 3.30 2.10 4 6 -9 5.40 1.90 4 6 -9 8.50 2.00 4 6 -9 7.50 2.90 -4 -6 9 5.30 2.00 3 6 -9 137.29 7.90 3 6 -9 129.09 7.90 3 6 -9 149.69 8.90 3 6 -9 134.39 10.70 3 6 -9 115.39 7.90 3 6 -9 126.59 8.20 -3 -6 9 130.29 8.00 2 6 -9 67.19 5.80 2 6 -9 72.59 5.00 2 6 -9 66.59 7.30 2 6 -9 65.69 4.80 2 6 -9 68.39 4.90 -2 -6 9 65.79 5.00 1 6 -9 0.40 3.10 1 6 -9 5.40 2.00 1 6 -9 -1.50 1.90 -1 -6 9 3.00 1.90 0 6 -9 24.60 5.30 0 6 -9 18.10 2.50 0 6 -9 15.10 2.70 0 -6 9 22.70 3.00 0 -6 9 18.60 4.00 -1 6 -9 73.39 6.60 -1 6 -9 72.49 5.30 1 -6 9 63.79 6.30 1 -6 9 68.69 4.90 -2 6 -9 46.30 4.60 -2 6 -9 49.30 6.00 2 -6 9 51.69 5.20 -3 6 -9 4.00 2.60 -3 6 -9 0.70 2.10 -3 6 -9 2.40 2.90 3 -6 9 1.30 2.50 -4 6 -9 -3.10 3.10 -4 6 -9 2.30 3.00 -4 6 -9 2.70 2.00 4 -6 9 1.00 2.60 -5 6 -9 32.30 6.00 -5 6 -9 40.70 5.80 -5 6 -9 41.80 3.70 5 -6 9 38.70 4.80 -6 6 -9 36.70 3.90 -6 6 -9 41.40 5.70 6 -6 9 48.20 4.50 -7 6 -9 6.80 2.10 -7 6 -9 6.70 2.80 7 -6 9 9.20 2.40 -8 6 -9 84.89 6.40 -8 6 -9 73.79 5.20 8 -6 9 77.59 5.20 -9 6 -9 0.40 2.20 -9 6 -9 0.00 1.80 8 5 -9 6.70 1.50 8 5 -9 6.60 2.30 8 5 -9 6.80 1.70 7 5 -9 32.00 3.10 7 5 -9 32.40 4.40 7 5 -9 33.60 3.40 7 5 -9 33.20 3.10 -7 -5 9 33.10 3.70 6 5 -9 19.30 3.10 6 5 -9 10.70 3.70 6 5 -9 13.90 2.50 6 5 -9 8.40 2.30 -6 -5 9 17.70 3.30 5 5 -9 6.60 2.90 5 5 -9 10.40 2.00 5 5 -9 7.50 2.20 5 5 -9 7.50 1.90 -5 -5 9 7.60 2.20 4 5 -9 8.50 2.00 4 5 -9 14.30 4.80 4 5 -9 8.40 2.30 4 5 -9 6.00 2.80 4 5 -9 11.20 2.00 4 5 -9 12.10 2.20 -4 -5 9 3.40 3.00 3 5 -9 75.69 5.80 3 5 -9 81.49 5.30 3 5 -9 80.29 5.40 3 5 -9 86.99 6.40 3 5 -9 75.89 8.50 3 5 -9 76.59 5.40 -3 -5 9 78.99 5.50 2 5 -9 54.99 6.60 2 5 -9 56.29 4.30 2 5 -9 56.59 5.20 2 5 -9 57.29 4.30 2 5 -9 52.29 4.30 -2 -5 9 57.19 4.40 1 5 -9 175.38 10.20 1 5 -9 161.58 10.20 1 5 -9 184.28 11.30 -1 -5 9 181.58 10.20 0 5 -9 46.30 4.00 0 5 -9 45.50 5.70 0 5 -9 33.80 4.10 0 -5 9 44.70 3.70 -1 5 -9 46.80 4.20 -1 5 -9 46.50 5.60 1 -5 9 43.60 3.70 1 -5 9 46.90 5.50 -2 5 -9 76.29 5.80 -2 5 -9 81.79 6.90 2 -5 9 77.39 6.10 -3 5 -9 59.19 4.60 -3 5 -9 64.69 5.40 -3 5 -9 63.89 6.30 3 -5 9 56.59 5.30 -4 5 -9 208.58 12.80 -4 5 -9 205.08 12.60 -4 5 -9 201.38 11.80 4 -5 9 209.88 12.20 -5 5 -9 10.30 2.10 -5 5 -9 7.80 3.20 -5 5 -9 7.20 3.90 5 -5 9 11.40 2.80 -6 5 -9 96.99 6.50 -6 5 -9 94.09 8.00 6 -5 9 117.89 7.10 -7 5 -9 95.09 6.50 -7 5 -9 100.69 7.80 7 -5 9 103.69 6.60 -8 5 -9 17.90 3.20 -8 5 -9 17.30 3.20 8 -5 9 22.50 3.20 -9 5 -9 26.80 2.90 -9 5 -9 28.60 4.50 9 -5 9 26.10 4.10 9 -5 9 29.00 3.20 8 4 -9 4.70 1.80 8 4 -9 6.40 1.60 8 4 -9 0.90 2.30 7 4 -9 21.20 2.90 7 4 -9 19.50 2.80 -7 -4 9 16.40 2.70 6 4 -9 97.79 6.00 6 4 -9 94.49 6.30 6 4 -9 88.09 6.00 -6 -4 9 99.09 6.30 5 4 -9 21.80 3.10 5 4 -9 12.90 3.00 5 4 -9 22.50 5.60 5 4 -9 21.70 3.20 5 4 -9 13.80 2.40 -5 -4 9 19.70 3.00 4 4 -9 7.50 2.00 4 4 -9 2.90 2.00 4 4 -9 5.40 2.20 4 4 -9 7.30 2.90 4 4 -9 6.40 2.00 4 4 -9 4.70 4.30 -4 -4 9 6.10 2.10 3 4 -9 29.40 3.90 3 4 -9 28.40 3.40 3 4 -9 33.60 4.80 3 4 -9 32.00 3.20 3 4 -9 29.30 4.50 3 4 -9 27.30 3.30 -3 -4 9 32.60 3.60 2 4 -9 31.30 3.50 2 4 -9 34.90 3.40 2 4 -9 35.50 3.60 2 4 -9 32.50 4.60 2 4 -9 38.70 5.80 2 4 -9 38.00 5.10 -2 -4 9 33.40 3.50 1 4 -9 41.00 5.60 1 4 -9 35.30 3.60 1 4 -9 40.60 5.70 1 4 -9 38.40 3.60 -1 -4 9 39.80 3.50 0 4 -9 24.60 3.20 0 4 -9 21.70 3.30 0 4 -9 20.70 4.90 0 -4 9 22.60 4.00 0 -4 9 25.80 2.90 -1 4 -9 29.10 3.90 -1 4 -9 24.70 5.00 -1 4 -9 27.40 3.60 1 -4 9 21.70 2.80 1 -4 9 18.70 3.40 -2 4 -9 109.29 7.20 -2 4 -9 122.39 8.50 -2 4 -9 128.89 8.00 -3 4 -9 334.07 18.60 -3 4 -9 341.37 19.50 -3 4 -9 331.47 19.00 3 -4 9 342.97 19.00 -4 4 -9 18.00 3.00 -4 4 -9 14.20 3.20 -4 4 -9 10.90 3.20 4 -4 9 14.30 2.50 -5 4 -9 54.09 4.40 -5 4 -9 43.90 5.90 5 -4 9 54.09 4.80 -6 4 -9 45.70 6.00 -6 4 -9 38.10 3.90 6 -4 9 52.79 4.70 -7 4 -9 112.19 7.40 -7 4 -9 118.39 8.80 7 -4 9 125.09 7.60 -8 4 -9 40.70 3.90 8 -4 9 53.09 5.60 8 -4 9 33.60 6.00 -9 4 -9 0.60 2.80 -9 4 -9 2.30 1.90 9 -4 9 1.50 1.90 9 -4 9 1.20 2.40 9 -4 9 -0.30 2.70 -10 4 -9 21.60 5.10 8 3 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34.90 3.80 -2 3 -9 28.40 3.00 -2 3 -9 36.00 4.90 2 -3 9 33.00 4.20 -3 3 -9 32.50 3.00 -3 3 -9 41.90 6.10 -3 3 -9 34.10 4.30 3 -3 9 26.20 4.00 -4 3 -9 25.40 3.10 -4 3 -9 18.60 3.40 -4 3 -9 27.40 5.20 4 -3 9 13.20 5.70 4 -3 9 29.20 3.60 -5 3 -9 4.60 3.00 -5 3 -9 6.60 1.90 5 -3 9 3.10 2.20 -6 3 -9 22.10 3.30 -6 3 -9 15.10 3.40 -7 3 -9 121.69 8.90 -7 3 -9 101.89 7.60 7 -3 9 107.79 9.10 7 -3 9 115.89 9.40 7 -3 9 135.29 7.60 -8 3 -9 3.80 2.20 -8 3 -9 0.50 3.20 8 -3 9 0.60 2.10 8 -3 9 9.50 3.40 8 -3 9 0.40 2.70 -9 3 -9 4.20 3.00 -9 3 -9 3.00 2.00 9 -3 9 2.10 2.40 9 -3 9 1.10 2.20 9 -3 9 10.10 3.30 9 -3 9 1.80 2.00 -10 3 -9 -0.40 1.50 10 -3 9 0.20 2.90 10 -3 9 -1.00 2.10 10 -3 9 2.40 2.20 9 2 -9 -1.20 1.80 9 2 -9 -1.80 1.30 9 2 -9 1.70 1.40 8 2 -9 9.60 2.70 8 2 -9 9.10 1.80 -8 -2 9 7.50 3.20 7 2 -9 -0.40 3.40 7 2 -9 3.70 2.00 6 2 -9 72.39 6.80 6 2 -9 67.69 10.40 6 2 -9 76.09 5.60 6 2 -9 86.19 5.40 6 2 -9 71.99 5.50 -6 -2 9 78.09 5.40 5 2 -9 2.30 2.50 5 2 -9 3.40 2.10 5 2 -9 -1.30 2.90 5 2 -9 -1.30 4.60 5 2 -9 -0.10 2.10 -5 -2 9 3.60 1.90 4 2 -9 26.70 4.80 4 2 -9 32.50 3.80 4 2 -9 27.20 3.90 4 2 -9 34.70 4.00 4 2 -9 32.00 4.90 4 2 -9 38.10 3.70 -4 -2 9 40.40 3.60 3 2 -9 58.69 5.60 3 2 -9 60.19 4.40 3 2 -9 57.19 7.00 3 2 -9 57.39 4.80 3 2 -9 59.89 4.60 3 2 -9 55.39 4.80 -3 -2 9 63.79 4.40 2 2 -9 82.39 6.30 2 2 -9 91.59 6.10 2 2 -9 84.19 7.40 2 2 -9 106.89 6.70 -2 -2 9 91.09 5.70 1 2 -9 129.09 7.80 1 2 -9 128.39 8.60 1 2 -9 140.89 9.00 1 2 -9 124.49 9.00 1 2 -9 127.19 7.70 -1 -2 9 132.39 7.70 0 2 -9 1.80 1.80 0 2 -9 5.60 1.70 0 2 -9 4.30 2.40 0 -2 9 5.00 1.50 0 -2 9 3.50 4.00 -1 2 -9 83.79 5.60 -1 2 -9 91.39 6.70 -1 2 -9 87.09 5.80 1 -2 9 88.19 5.40 1 -2 9 84.29 6.00 1 -2 9 79.09 6.30 -2 2 -9 14.00 2.20 -2 2 -9 14.30 2.30 -2 2 -9 16.20 2.80 2 -2 9 14.70 2.50 -3 2 -9 168.48 10.00 -3 2 -9 180.58 10.70 -3 2 -9 175.88 9.60 3 -2 9 165.48 9.90 3 -2 9 151.88 10.00 -4 2 -9 33.60 3.10 -4 2 -9 21.50 3.60 4 -2 9 34.70 5.90 -5 2 -9 169.38 11.40 -5 2 -9 190.48 10.40 5 -2 9 178.88 10.50 -6 2 -9 26.70 3.50 -6 2 -9 29.10 5.50 6 -2 9 28.70 3.60 6 -2 9 17.20 5.50 -7 2 -9 93.89 6.10 -7 2 -9 83.89 7.80 7 -2 9 89.29 6.40 7 -2 9 88.29 8.40 7 -2 9 109.79 8.20 -8 2 -9 22.40 3.90 -8 2 -9 30.10 3.40 8 -2 9 18.40 3.40 8 -2 9 24.70 3.70 -9 2 -9 6.00 3.20 -9 2 -9 3.80 2.10 9 -2 9 5.30 2.30 9 -2 9 0.40 2.10 9 -2 9 2.20 1.90 9 1 -9 19.00 3.20 9 1 -9 21.20 2.90 9 1 -9 22.70 2.50 8 1 -9 1.80 2.00 8 1 -9 2.90 1.80 8 1 -9 0.80 2.40 -8 -1 9 -2.20 3.30 7 1 -9 0.80 2.50 7 1 -9 -4.00 4.00 7 1 -9 2.10 2.30 -7 -1 9 3.20 2.50 6 1 -9 55.49 4.70 6 1 -9 47.60 6.10 6 1 -9 60.89 9.50 6 1 -9 66.69 4.50 -6 -1 9 46.70 4.60 5 1 -9 28.60 3.50 5 1 -9 30.40 3.50 5 1 -9 26.40 5.20 5 1 -9 25.60 3.50 5 1 -9 25.70 5.00 -5 -1 9 30.50 3.60 4 1 -9 65.39 5.30 4 1 -9 60.19 4.90 4 1 -9 62.09 5.00 4 1 -9 64.09 4.80 4 1 -9 56.49 7.90 4 1 -9 65.39 6.00 -4 -1 9 65.09 4.70 3 1 -9 34.40 3.60 3 1 -9 26.20 6.30 3 1 -9 33.00 3.80 3 1 -9 32.00 4.80 3 1 -9 34.60 4.90 3 1 -9 29.10 3.30 -3 -1 9 34.70 3.20 2 1 -9 103.29 8.10 2 1 -9 98.59 7.30 2 1 -9 93.39 6.30 2 1 -9 105.39 6.70 2 1 -9 101.29 6.70 -2 -1 9 103.29 6.10 1 1 -9 17.60 2.60 1 1 -9 18.30 2.20 1 1 -9 16.90 3.40 1 1 -9 17.60 3.10 1 1 -9 17.10 3.00 -1 -1 9 18.60 2.40 0 1 -9 81.79 6.40 0 1 -9 86.69 5.50 0 1 -9 78.69 5.30 0 -1 9 80.59 5.10 -1 1 -9 1.20 1.60 -1 1 -9 0.60 2.30 -1 1 -9 3.50 2.00 1 -1 9 0.20 2.50 -2 1 -9 71.49 5.40 -2 1 -9 82.19 4.90 -2 1 -9 84.49 6.40 2 -1 9 80.89 5.60 2 -1 9 84.29 5.10 -3 1 -9 22.00 3.90 -3 1 -9 27.40 2.40 -3 1 -9 19.50 2.70 -3 1 -9 30.80 4.60 3 -1 9 23.90 3.70 3 -1 9 22.60 3.20 -4 1 -9 161.08 8.70 -4 1 -9 154.38 9.90 -4 1 -9 136.09 9.70 4 -1 9 155.28 9.00 4 -1 9 147.39 9.80 -5 1 -9 7.20 1.70 -5 1 -9 8.50 3.70 5 -1 9 5.00 1.90 -6 1 -9 339.97 20.10 -6 1 -9 377.76 19.40 6 -1 9 319.37 20.50 6 -1 9 370.56 19.50 6 -1 9 337.17 20.10 -7 1 -9 103.29 8.60 -7 1 -9 114.39 6.90 7 -1 9 110.29 7.00 7 -1 9 106.99 8.90 -8 1 -9 89.29 5.80 -8 1 -9 82.29 8.00 8 -1 9 84.29 7.50 8 -1 9 85.99 6.00 9 0 -9 0.80 2.10 9 0 -9 7.60 2.10 9 0 -9 -1.40 1.40 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170.68 9.40 -3 0 -9 26.80 3.10 -3 0 -9 24.80 4.70 -3 0 -9 30.90 3.60 -3 0 -9 28.30 2.30 3 0 9 24.50 3.30 3 0 9 21.20 3.40 -4 0 -9 27.50 2.40 -4 0 -9 27.60 4.90 -4 0 -9 20.00 3.60 4 0 9 24.70 3.10 4 0 9 16.70 3.10 -5 0 -9 103.39 7.80 -5 0 -9 107.39 6.30 5 0 9 100.29 7.40 -6 0 -9 5.90 1.80 -6 0 -9 6.60 3.20 6 0 9 4.90 3.80 6 0 9 5.30 2.00 -7 0 -9 3.40 3.60 -7 0 -9 6.60 1.90 7 0 9 1.70 2.10 7 0 9 2.60 3.00 -8 0 -9 10.40 4.00 -8 0 -9 5.20 2.30 8 0 9 8.00 2.30 8 0 9 9.30 2.80 -9 0 -9 10.30 2.00 9 0 9 4.70 2.50 9 0 9 5.50 2.40 9 0 9 7.00 2.10 9 -1 -9 3.20 1.40 9 -1 -9 2.00 2.10 8 -1 -9 -0.40 2.20 8 -1 -9 0.60 2.00 8 -1 -9 0.90 2.60 8 -1 -9 3.50 2.00 -8 1 9 3.70 3.90 7 -1 -9 32.00 5.40 7 -1 -9 47.10 5.10 7 -1 -9 35.30 4.30 7 -1 -9 49.60 3.80 -7 1 9 48.60 4.70 6 -1 -9 21.40 2.60 6 -1 -9 15.50 3.90 6 -1 -9 17.50 3.40 6 -1 -9 18.10 2.90 -6 1 9 23.10 3.50 5 -1 -9 12.10 3.30 5 -1 -9 7.50 4.20 5 -1 -9 12.10 3.60 5 -1 -9 17.50 2.40 -5 1 9 15.00 2.30 4 -1 -9 29.00 4.10 4 -1 -9 32.00 3.60 4 -1 -9 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2 9 9 92.39 7.00 -3 -9 -9 9.40 3.30 -3 -9 -9 14.30 2.50 3 9 9 13.20 2.90 -4 -9 -9 1.00 1.80 -4 -9 -9 0.90 4.20 4 9 9 1.10 2.30 -5 -9 -9 79.79 5.30 5 9 9 80.59 5.90 -6 -9 -9 2.60 1.60 6 9 9 5.70 2.70 6 9 9 3.80 2.10 -7 -9 -9 44.30 3.80 7 9 9 45.50 3.80 7 9 9 37.40 5.50 7 9 9 36.30 4.00 -8 -9 -9 4.00 1.70 8 9 9 2.60 1.50 8 9 9 1.00 1.80 8 9 9 2.00 2.00 8 9 9 -1.70 3.20 -9 -9 -9 8.20 1.70 9 9 9 3.40 2.10 9 9 9 8.60 1.80 9 9 9 7.40 1.80 9 9 9 14.10 2.40 -10 -9 -9 63.69 4.40 10 9 9 59.99 4.10 10 9 9 61.19 4.10 5 -10 -9 2.80 2.30 5 -10 -9 4.30 2.20 5 -10 -9 5.80 2.50 4 -10 -9 9.40 2.90 4 -10 -9 8.70 2.60 4 -10 -9 11.30 2.40 -4 10 9 5.40 2.40 3 -10 -9 4.00 2.50 3 -10 -9 7.40 3.10 3 -10 -9 7.80 2.40 -3 10 9 0.80 2.30 2 -10 -9 4.70 2.60 2 -10 -9 6.00 3.10 -2 10 9 1.40 2.30 1 -10 -9 117.29 8.00 -1 10 9 100.29 7.20 0 -10 -9 119.19 8.40 0 10 9 122.39 10.00 0 10 9 107.09 7.40 -1 -10 -9 118.39 8.30 1 10 9 123.59 9.10 1 10 9 103.29 8.20 -2 -10 -9 3.60 3.20 2 10 9 2.30 2.90 -3 -10 -9 0.20 2.20 -3 -10 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1.70 9 11 9 3.30 1.20 3 -12 -9 21.60 2.50 3 -12 -9 27.30 4.40 -3 12 9 20.50 3.70 2 -12 -9 17.70 2.70 2 -12 -9 17.70 3.10 -2 12 9 11.30 2.70 1 -12 -9 38.30 4.80 1 -12 -9 33.70 4.10 -1 12 9 35.80 4.70 0 -12 -9 8.50 3.60 0 -12 -9 11.60 2.80 0 12 9 8.00 4.00 -1 -12 -9 29.90 3.90 1 12 9 19.60 3.40 -2 -12 -9 3.80 2.90 2 12 9 -0.40 2.20 -3 -12 -9 4.80 2.50 -4 -12 -9 6.80 3.70 4 12 9 4.20 2.80 -5 -12 -9 16.50 2.70 5 12 9 20.20 2.60 5 12 9 18.10 2.30 -6 -12 -9 43.60 4.10 6 12 9 45.40 3.50 6 12 9 41.90 3.70 -7 -12 -9 -0.10 1.70 7 12 9 0.10 1.50 7 12 9 1.10 1.40 -8 -12 -9 17.50 3.20 8 12 9 19.70 2.40 8 12 9 23.70 2.20 2 -13 -9 19.00 3.00 0 -13 -9 13.90 2.90 0 13 9 14.00 3.90 -1 -13 -9 2.50 2.60 1 13 9 1.60 2.80 -2 -13 -9 11.70 2.90 2 13 9 10.30 2.70 -3 -13 -9 5.30 3.00 3 13 9 1.00 2.10 -4 -13 -9 2.10 3.90 4 13 9 4.20 2.10 4 13 9 -2.10 1.90 5 13 9 -0.60 1.70 5 13 9 3.70 1.70 -6 -13 -9 4.10 2.60 6 13 9 -0.20 1.50 6 13 9 1.30 1.40 -7 -13 -9 110.19 7.20 7 13 9 119.39 6.60 7 13 9 105.69 7.00 7 13 9 118.99 6.70 0 14 9 11.20 3.80 1 14 9 -1.10 2.70 2 14 9 44.00 4.70 3 14 9 24.50 3.30 4 14 9 19.00 2.90 5 14 9 0.60 1.50 1 11 -10 2.90 1.50 1 11 -10 1.10 1.70 0 11 -10 34.30 3.10 -1 11 -10 2.60 4.70 -1 11 -10 2.50 1.50 1 -11 10 -3.00 3.30 -2 11 -10 17.80 2.70 -2 11 -10 12.00 3.70 2 -11 10 11.20 2.20 3 10 -10 5.10 1.40 3 10 -10 2.70 1.90 -3 -10 10 4.30 1.80 2 10 -10 29.30 3.00 2 10 -10 26.20 3.40 -2 -10 10 23.10 4.00 1 10 -10 30.60 3.20 0 10 -10 14.00 3.40 0 10 -10 11.40 2.10 0 -10 10 11.10 3.70 -1 10 -10 7.80 2.90 -1 10 -10 10.40 2.00 1 -10 10 4.70 2.60 -2 10 -10 4.10 2.50 -2 10 -10 2.20 1.90 2 -10 10 -1.20 2.20 -3 10 -10 62.99 5.40 -3 10 -10 63.79 4.70 3 -10 10 61.59 4.70 -4 10 -10 1.40 2.50 -4 10 -10 3.20 2.00 4 -10 10 3.30 1.90 5 9 -10 2.30 1.90 5 9 -10 4.10 1.90 -5 -9 10 3.90 1.60 4 9 -10 11.70 1.70 4 9 -10 12.80 1.90 4 9 -10 14.40 2.40 -4 -9 10 18.00 2.50 3 9 -10 5.10 2.20 3 9 -10 6.80 1.60 -3 -9 10 6.20 1.80 2 9 -10 44.20 4.30 2 9 -10 45.60 3.70 -2 -9 10 36.10 3.60 1 9 -10 8.80 2.00 1 9 -10 6.50 3.40 -1 -9 10 6.00 2.10 0 9 -10 5.70 1.90 0 9 -10 3.10 2.90 -1 9 -10 6.70 2.80 -1 9 -10 5.10 2.00 1 -9 10 2.40 2.50 -2 9 -10 14.80 3.00 -2 9 -10 15.30 2.50 -3 9 -10 5.60 2.10 -3 9 -10 5.70 2.60 3 -9 10 5.00 2.40 -4 9 -10 3.60 2.50 -4 9 -10 1.80 2.40 4 -9 10 2.60 2.20 -5 9 -10 40.80 4.60 5 -9 10 47.30 3.90 -6 9 -10 1.50 2.00 6 -9 10 2.00 1.50 6 8 -10 0.30 1.80 6 8 -10 0.90 1.10 6 8 -10 4.80 1.50 -6 -8 10 -0.90 1.60 5 8 -10 46.70 3.60 5 8 -10 42.20 3.20 5 8 -10 42.50 4.10 -5 -8 10 44.00 3.40 4 8 -10 61.39 4.40 4 8 -10 68.19 5.50 4 8 -10 65.59 5.00 4 8 -10 68.09 4.40 -4 -8 10 73.89 4.70 3 8 -10 28.10 4.40 3 8 -10 27.20 3.00 3 8 -10 25.10 3.90 3 8 -10 18.70 2.90 -3 -8 10 26.00 3.20 2 8 -10 7.50 3.70 2 8 -10 9.90 2.70 2 8 -10 3.70 2.00 2 8 -10 8.50 4.10 -2 -8 10 5.50 1.90 1 8 -10 50.09 4.20 1 8 -10 46.50 8.00 -1 -8 10 43.40 4.00 0 8 -10 5.00 2.10 0 8 -10 5.60 3.00 0 -8 10 5.60 2.10 0 -8 10 0.80 3.40 -1 8 -10 23.70 3.60 -1 8 -10 15.10 3.30 1 -8 10 9.90 3.80 -2 8 -10 44.00 5.20 -2 8 -10 43.20 4.20 2 -8 10 38.60 4.50 -3 8 -10 120.99 7.70 -4 8 -10 113.19 7.60 -4 8 -10 117.59 8.10 4 -8 10 121.99 7.60 -5 8 -10 4.50 2.60 -5 8 -10 -3.00 3.20 5 -8 10 2.90 2.20 -6 8 -10 60.89 5.40 6 -8 10 68.49 4.70 -7 8 -10 3.10 2.00 7 -8 10 2.70 1.50 6 7 -10 12.00 1.70 6 7 -10 7.40 2.20 6 7 -10 8.00 1.50 -6 -7 10 7.70 2.00 5 7 -10 42.10 3.70 5 7 -10 38.90 4.30 5 7 -10 44.10 3.40 -5 -7 10 46.70 3.60 4 7 -10 13.70 1.90 4 7 -10 15.10 2.60 4 7 -10 18.20 2.30 4 7 -10 17.20 2.90 -4 -7 10 18.40 3.00 3 7 -10 7.50 2.70 3 7 -10 7.80 1.90 3 7 -10 10.10 2.20 -3 -7 10 9.30 2.00 2 7 -10 5.60 3.40 2 7 -10 2.70 1.90 2 7 -10 7.40 2.80 2 7 -10 4.10 2.10 -2 -7 10 5.60 2.00 1 7 -10 -0.30 3.20 1 7 -10 2.10 2.10 1 7 -10 6.30 2.20 -1 -7 10 3.00 1.90 0 7 -10 5.70 2.20 0 7 -10 1.50 3.10 0 -7 10 6.50 2.00 0 -7 10 -1.20 3.40 -1 7 -10 41.90 4.40 -1 7 -10 52.09 6.00 1 -7 10 31.30 5.00 -2 7 -10 42.60 4.50 -2 7 -10 43.50 5.80 2 -7 10 32.40 4.70 -3 7 -10 41.20 5.70 -3 7 -10 43.80 4.70 3 -7 10 39.20 4.80 -4 7 -10 1.50 2.90 -4 7 -10 3.50 2.90 4 -7 10 5.60 2.60 -5 7 -10 51.59 4.80 -5 7 -10 69.29 6.00 5 -7 10 68.89 5.60 -6 7 -10 7.20 2.70 -6 7 -10 9.40 2.20 -7 7 -10 39.20 4.60 -7 7 -10 31.00 4.60 7 -7 10 44.50 3.60 -8 7 -10 0.80 1.90 8 -7 10 -0.10 1.40 7 6 -10 5.60 1.40 7 6 -10 5.80 2.00 7 6 -10 7.30 1.60 -7 -6 10 5.60 1.90 6 6 -10 4.80 1.60 6 6 -10 4.00 2.10 6 6 -10 6.70 1.80 -6 -6 10 5.60 1.90 5 6 -10 6.50 2.10 5 6 -10 5.90 2.40 5 6 -10 6.50 1.80 -5 -6 10 6.80 1.90 4 6 -10 -0.30 2.40 4 6 -10 1.70 1.70 4 6 -10 3.30 2.50 -4 -6 10 6.10 2.00 3 6 -10 82.79 8.30 3 6 -10 79.89 6.10 3 6 -10 86.29 5.60 3 6 -10 81.59 5.50 3 6 -10 88.29 6.80 -3 -6 10 84.19 5.60 2 6 -10 46.40 5.10 2 6 -10 45.50 6.90 2 6 -10 58.39 4.40 2 6 -10 42.50 4.10 2 6 -10 62.39 5.50 -2 -6 10 52.89 4.10 1 6 -10 34.40 3.80 1 6 -10 46.30 4.10 1 6 -10 31.70 6.00 -1 -6 10 39.00 4.20 0 6 -10 54.09 4.80 0 6 -10 55.19 4.70 0 6 -10 60.99 6.40 0 -6 10 45.10 5.90 0 -6 10 52.69 4.20 -1 6 -10 66.99 6.60 -1 6 -10 60.29 4.90 1 -6 10 56.49 4.50 1 -6 10 42.60 5.40 -2 6 -10 5.50 3.10 -2 6 -10 7.10 2.40 2 -6 10 5.20 2.70 2 -6 10 4.70 3.20 -3 6 -10 3.00 3.00 -3 6 -10 1.30 2.50 3 -6 10 3.50 2.70 -4 6 -10 40.70 5.00 -4 6 -10 32.90 3.80 -4 6 -10 51.19 5.80 4 -6 10 49.00 4.90 -5 6 -10 20.30 3.50 -5 6 -10 20.10 3.20 -5 6 -10 12.90 3.50 -6 6 -10 92.09 6.00 -7 6 -10 14.70 2.30 -7 6 -10 19.10 3.10 7 -6 10 23.10 3.40 -8 6 -10 5.40 1.90 -8 6 -10 7.30 2.40 8 -6 10 6.20 1.80 8 -6 10 4.30 2.40 7 5 -10 5.30 1.70 7 5 -10 2.60 2.10 7 5 -10 6.80 1.70 6 5 -10 42.40 4.40 6 5 -10 39.50 3.70 6 5 -10 43.50 3.50 -6 -5 10 46.40 3.90 5 5 -10 63.79 6.10 5 5 -10 68.09 7.20 5 5 -10 67.49 5.00 -5 -5 10 76.79 5.00 4 5 -10 64.59 8.30 4 5 -10 61.99 5.10 4 5 -10 72.59 6.20 4 5 -10 67.79 4.70 4 5 -10 67.59 4.90 -4 -5 10 72.89 4.90 3 5 -10 2.70 2.80 3 5 -10 -0.40 1.90 3 5 -10 2.50 2.30 3 5 -10 1.40 3.50 3 5 -10 4.30 1.90 -3 -5 10 2.20 1.80 2 5 -10 81.89 5.90 2 5 -10 86.59 8.10 2 5 -10 98.39 7.10 2 5 -10 101.49 6.10 2 5 -10 85.59 6.80 -2 -5 10 95.69 6.00 1 5 -10 7.80 3.30 1 5 -10 9.30 2.20 1 5 -10 15.40 2.30 -1 -5 10 9.80 2.10 0 5 -10 143.09 9.50 0 5 -10 140.49 8.10 0 5 -10 120.19 8.00 0 -5 10 130.59 7.90 0 -5 10 122.29 9.20 -1 5 -10 223.48 12.60 -1 5 -10 202.78 11.60 1 -5 10 186.38 11.40 1 -5 10 187.18 12.00 -2 5 -10 187.98 10.90 -2 5 -10 210.88 11.90 2 -5 10 165.48 10.80 2 -5 10 177.08 11.10 -3 5 -10 26.30 5.30 -3 5 -10 13.60 2.50 -3 5 -10 19.30 2.90 3 -5 10 24.00 4.10 -4 5 -10 38.10 5.80 -4 5 -10 38.70 5.00 -4 5 -10 34.90 3.50 4 -5 10 48.60 4.60 -5 5 -10 68.19 6.80 -5 5 -10 71.49 5.10 -5 5 -10 74.49 6.90 5 -5 10 90.49 6.00 -6 5 -10 90.29 6.20 -6 5 -10 87.19 7.50 6 -5 10 111.49 6.70 -7 5 -10 9.60 2.80 -7 5 -10 9.90 2.10 7 -5 10 11.90 2.30 -8 5 -10 1.50 1.80 -8 5 -10 2.90 2.60 8 -5 10 7.00 2.00 -9 5 -10 55.99 4.90 9 -5 10 41.40 4.40 9 -5 10 49.70 4.90 7 4 -10 22.50 3.90 7 4 -10 25.90 3.00 7 4 -10 29.60 2.90 6 4 -10 34.90 4.60 6 4 -10 41.80 3.50 6 4 -10 41.90 3.80 -6 -4 10 49.30 3.90 5 4 -10 5.60 1.90 5 4 -10 3.50 2.70 5 4 -10 8.50 2.10 -5 -4 10 7.50 2.10 4 4 -10 15.40 2.30 4 4 -10 17.60 3.00 4 4 -10 12.20 2.90 4 4 -10 11.90 4.30 4 4 -10 16.40 2.50 -4 -4 10 18.30 3.00 3 4 -10 47.50 4.10 3 4 -10 44.20 6.70 3 4 -10 47.00 4.60 3 4 -10 45.30 5.40 3 4 -10 50.99 4.10 -3 -4 10 48.60 4.00 2 4 -10 5.60 2.00 2 4 -10 2.70 1.90 2 4 -10 1.60 3.10 2 4 -10 7.70 2.70 2 4 -10 1.90 2.70 -2 -4 10 1.90 1.90 1 4 -10 13.80 3.10 1 4 -10 20.80 3.40 1 4 -10 19.00 3.00 1 4 -10 10.30 2.10 -1 -4 10 15.10 2.20 0 4 -10 20.40 3.10 0 4 -10 15.00 2.20 0 4 -10 23.00 5.20 0 -4 10 16.70 3.40 0 -4 10 15.60 2.90 -1 4 -10 27.30 3.30 -1 4 -10 22.80 5.20 1 -4 10 21.50 3.10 1 -4 10 25.80 4.40 -2 4 -10 277.77 15.10 -2 4 -10 248.58 14.20 2 -4 10 240.98 14.30 2 -4 10 234.08 14.10 -3 4 -10 64.29 6.30 -3 4 -10 57.29 4.90 -3 4 -10 51.59 4.40 3 -4 10 55.89 5.00 -4 4 -10 34.90 3.60 -4 4 -10 34.10 4.70 -4 4 -10 41.60 5.70 4 -4 10 44.10 4.30 -5 4 -10 140.19 9.50 -5 4 -10 131.59 8.10 -5 4 -10 123.19 9.50 5 -4 10 150.78 8.70 -6 4 -10 11.50 3.30 -6 4 -10 12.30 2.10 6 -4 10 6.70 2.90 -7 4 -10 37.70 5.30 -7 4 -10 38.60 3.80 7 -4 10 49.30 4.20 7 -4 10 31.60 3.90 -8 4 -10 18.70 3.20 -8 4 -10 25.40 3.20 9 -4 10 10.30 2.60 9 -4 10 16.20 2.60 8 3 -10 -1.00 1.50 8 3 -10 0.10 1.40 8 3 -10 -1.60 1.90 -8 -3 10 -4.30 3.00 7 3 -10 -0.80 1.80 7 3 -10 -1.30 2.40 7 3 -10 1.30 1.80 6 3 -10 51.39 5.30 6 3 -10 46.20 4.10 6 3 -10 61.39 4.20 -6 -3 10 51.39 4.40 5 3 -10 -0.80 2.60 5 3 -10 -2.10 2.00 5 3 -10 -0.70 4.30 5 3 -10 2.00 2.10 -5 -3 10 1.00 2.00 4 3 -10 0.90 2.00 4 3 -10 0.20 2.60 4 3 -10 4.00 2.20 4 3 -10 4.70 2.10 4 3 -10 0.70 4.00 -4 -3 10 5.60 3.00 3 3 -10 28.60 3.80 3 3 -10 24.60 3.20 3 3 -10 21.80 4.50 3 3 -10 18.50 2.40 -3 -3 10 21.70 3.30 2 3 -10 9.60 2.80 2 3 -10 6.50 3.20 2 3 -10 7.10 2.00 2 3 -10 15.00 2.60 2 3 -10 10.60 1.90 -2 -3 10 10.60 2.10 1 3 -10 8.70 3.80 1 3 -10 8.60 1.90 1 3 -10 5.70 3.00 1 3 -10 5.90 3.00 1 3 -10 8.70 2.00 -1 -3 10 7.90 1.80 0 3 -10 22.10 5.00 0 3 -10 22.80 3.00 0 3 -10 20.60 2.50 0 -3 10 21.00 2.90 -1 3 -10 30.20 5.20 -1 3 -10 32.50 3.30 -1 3 -10 28.10 3.70 -2 3 -10 5.40 2.70 -2 3 -10 5.30 2.00 2 -3 10 7.40 2.40 2 -3 10 6.60 1.90 -3 3 -10 64.09 4.60 -3 3 -10 66.49 5.20 -3 3 -10 75.69 6.50 3 -3 10 66.99 5.30 -4 3 -10 7.90 2.90 -4 3 -10 10.60 2.80 -4 3 -10 9.70 1.80 4 -3 10 12.70 2.40 -5 3 -10 30.20 3.40 -5 3 -10 27.20 5.20 -5 3 -10 20.70 4.00 5 -3 10 32.20 4.00 -6 3 -10 64.89 5.60 -6 3 -10 57.49 6.40 6 -3 10 59.39 5.00 -7 3 -10 2.60 3.10 -7 3 -10 3.80 2.00 7 -3 10 5.90 2.30 -8 3 -10 6.50 2.60 -8 3 -10 5.40 2.10 9 -3 10 72.79 5.60 9 -3 10 88.49 5.30 -10 3 -10 0.40 1.70 10 -3 10 -0.60 1.90 8 2 -10 23.40 3.30 8 2 -10 24.50 2.40 8 2 -10 21.10 2.60 -8 -2 10 18.50 3.70 7 2 -10 -1.80 2.40 7 2 -10 -0.20 1.80 7 2 -10 -0.10 1.80 -7 -2 10 2.10 2.40 6 2 -10 58.19 5.80 6 2 -10 54.69 5.00 6 2 -10 68.69 4.80 5 2 -10 53.49 8.50 5 2 -10 64.49 4.60 5 2 -10 58.29 5.90 5 2 -10 52.19 4.70 -5 -2 10 57.19 4.40 4 2 -10 0.30 2.00 4 2 -10 -0.40 2.00 4 2 -10 -1.40 3.70 4 2 -10 -1.90 2.10 4 2 -10 0.30 2.80 -4 -2 10 -0.30 1.70 3 2 -10 11.20 3.60 3 2 -10 16.00 2.80 3 2 -10 8.30 2.30 3 2 -10 13.30 2.30 3 2 -10 9.10 2.70 -3 -2 10 13.00 2.10 2 2 -10 3.30 3.00 2 2 -10 6.50 2.00 2 2 -10 2.40 2.50 2 2 -10 5.10 2.40 2 2 -10 5.50 2.00 -2 -2 10 5.20 1.70 1 2 -10 450.45 27.00 1 2 -10 480.35 26.70 1 2 -10 475.95 27.20 1 2 -10 495.55 26.70 1 2 -10 521.35 27.50 -1 -2 10 502.65 26.70 0 2 -10 64.59 5.90 0 2 -10 64.29 4.50 0 2 -10 62.29 4.50 0 2 -10 48.10 6.60 0 -2 10 52.29 6.40 0 -2 10 61.49 4.30 -1 2 -10 8.20 2.80 -1 2 -10 9.50 2.70 -1 2 -10 7.40 2.00 1 -2 10 8.00 2.80 -2 2 -10 36.20 3.60 -2 2 -10 38.20 5.10 -2 2 -10 30.50 3.50 2 -2 10 29.20 4.00 2 -2 10 36.80 3.40 -3 2 -10 12.90 2.40 -3 2 -10 11.20 2.50 -3 2 -10 12.70 2.80 3 -2 10 11.90 2.90 3 -2 10 13.70 2.30 -4 2 -10 100.89 7.60 -4 2 -10 92.79 6.90 -4 2 -10 103.19 6.10 4 -2 10 94.89 6.40 -5 2 -10 55.99 6.70 -5 2 -10 81.99 6.70 -5 2 -10 75.59 5.00 5 -2 10 79.69 5.40 5 -2 10 63.69 6.10 -6 2 -10 8.10 2.00 -6 2 -10 4.50 3.00 6 -2 10 9.60 2.40 -7 2 -10 1.00 3.00 -7 2 -10 0.10 1.90 7 -2 10 1.20 2.30 -8 2 -10 96.19 6.40 -8 2 -10 115.29 8.60 8 -2 10 104.39 6.50 8 -2 10 85.99 7.90 -9 2 -10 -1.10 3.40 -9 2 -10 2.60 1.70 9 -2 10 2.20 1.90 9 -2 10 0.30 2.20 10 -2 10 13.60 2.20 8 1 -10 3.10 1.90 8 1 -10 7.80 1.60 8 1 -10 8.20 1.60 -8 -1 10 6.00 3.60 7 1 -10 10.00 2.00 7 1 -10 4.50 2.70 7 1 -10 5.60 2.00 6 1 -10 29.10 3.50 6 1 -10 23.30 4.60 6 1 -10 29.20 3.30 -6 -1 10 37.80 3.80 5 1 -10 4.10 2.30 5 1 -10 -3.60 2.90 5 1 -10 -2.10 2.10 5 1 -10 -1.90 4.20 4 1 -10 19.10 4.30 4 1 -10 27.20 3.90 4 1 -10 28.70 3.80 4 1 -10 31.20 3.50 4 1 -10 26.00 5.00 -4 -1 10 31.40 3.40 3 1 -10 3.40 2.70 3 1 -10 5.00 2.10 3 1 -10 6.30 2.10 3 1 -10 5.50 2.10 3 1 -10 1.20 3.40 -3 -1 10 2.60 1.90 2 1 -10 42.80 6.10 2 1 -10 55.69 4.10 2 1 -10 52.89 4.80 2 1 -10 50.09 5.40 2 1 -10 52.19 4.40 -2 -1 10 53.89 4.00 1 1 -10 1.00 2.90 1 1 -10 1.80 1.80 1 1 -10 2.40 2.60 1 1 -10 2.60 1.80 1 1 -10 3.50 2.80 -1 -1 10 2.20 1.60 0 1 -10 34.00 5.30 0 1 -10 31.00 4.00 0 1 -10 20.00 3.70 -1 1 -10 9.00 2.00 -1 1 -10 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10.60 0 8 10 172.28 12.60 -1 -8 -10 15.90 3.10 1 8 10 28.70 4.00 1 8 10 23.10 4.30 -2 -8 -10 7.60 3.00 2 8 10 8.80 3.40 2 8 10 11.20 2.80 -3 -8 -10 20.30 3.60 -3 -8 -10 14.80 3.50 3 8 10 20.80 3.50 -4 -8 -10 4.90 1.80 -4 -8 -10 4.80 3.70 4 8 10 4.30 2.50 -5 -8 -10 3.20 4.80 -5 -8 -10 4.30 1.50 5 8 10 0.40 2.20 -6 -8 -10 60.79 4.20 6 8 10 56.89 4.80 6 8 10 51.69 5.00 -7 -8 -10 5.10 1.70 7 8 10 -1.10 2.60 7 8 10 2.80 1.90 7 8 10 2.80 2.00 -8 -8 -10 76.89 4.90 8 8 10 67.39 4.80 8 8 10 73.19 4.90 8 8 10 63.69 5.90 -9 -8 -10 30.80 3.00 9 8 10 25.40 4.40 9 8 10 30.60 3.00 9 8 10 30.20 3.10 9 8 10 31.00 3.00 -10 -8 -10 1.80 1.40 10 8 10 3.40 1.50 10 8 10 5.00 1.50 10 8 10 -0.70 1.80 5 -9 -10 18.60 2.90 5 -9 -10 23.80 3.60 -5 9 10 15.10 2.50 4 -9 -10 11.30 3.10 4 -9 -10 9.20 2.30 4 -9 -10 9.00 2.90 4 -9 -10 8.00 2.50 -4 9 10 4.30 2.30 3 -9 -10 66.99 5.80 3 -9 -10 57.89 6.40 3 -9 -10 62.79 5.00 -3 9 10 58.79 5.20 2 -9 -10 5.50 2.70 -2 9 10 3.20 2.50 1 -9 -10 129.19 8.70 -1 9 10 122.89 8.10 0 -9 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11.10 1.70 8 11 10 12.90 2.30 3 -12 -10 4.80 1.60 -3 12 10 8.40 2.30 2 -12 -10 72.59 6.00 2 -12 -10 81.19 5.60 1 -12 -10 1.60 2.70 1 -12 -10 0.70 2.40 0 -12 -10 6.80 3.20 0 -12 -10 14.40 2.90 0 12 10 15.90 4.20 -1 -12 -10 3.70 2.60 1 12 10 -3.40 3.00 -2 -12 -10 41.60 4.70 2 12 10 37.30 4.60 -3 -12 -10 6.10 3.00 3 12 10 6.80 2.40 -4 -12 -10 35.40 5.70 4 12 10 32.10 3.70 -5 -12 -10 31.60 6.10 5 12 10 26.30 3.20 -6 -12 -10 60.69 6.50 6 12 10 55.39 4.20 6 12 10 57.29 4.10 -7 -12 -10 6.80 2.10 7 12 10 5.20 1.50 7 12 10 4.00 1.40 -8 -12 -10 22.10 3.10 8 12 10 20.30 2.40 0 -13 -10 -2.50 2.20 0 13 10 3.40 4.20 -1 -13 -10 44.20 4.70 1 13 10 37.10 5.20 2 13 10 14.40 2.80 -3 -13 -10 9.30 3.00 3 13 10 6.60 2.30 -4 -13 -10 1.70 3.60 4 13 10 3.10 1.80 4 13 10 5.60 2.10 5 13 10 43.60 3.40 5 13 10 35.10 3.40 6 13 10 10.90 1.50 6 13 10 8.80 1.60 1 14 10 -0.40 3.80 2 14 10 41.20 4.10 3 14 10 6.80 1.80 4 14 10 9.40 1.80 1 10 -11 2.80 2.10 1 10 -11 2.80 1.40 0 10 -11 5.40 1.50 0 10 -11 4.30 1.90 -1 10 -11 3.10 2.70 -1 10 -11 0.10 2.00 -1 10 -11 1.90 1.60 -2 10 -11 8.70 1.80 -2 10 -11 5.80 2.30 2 -10 11 6.90 2.00 -3 10 -11 16.10 3.50 3 -10 11 11.90 1.90 3 9 -11 1.20 1.30 3 9 -11 1.60 1.90 2 9 -11 18.00 3.20 2 9 -11 21.60 2.50 1 9 -11 4.60 1.70 1 9 -11 5.60 3.50 1 9 -11 3.30 2.10 0 9 -11 2.40 2.90 0 9 -11 4.70 2.20 0 9 -11 5.10 1.80 -1 9 -11 13.20 2.90 1 -9 11 14.70 3.00 -2 9 -11 17.40 3.10 -2 9 -11 19.20 4.40 -3 9 -11 47.10 4.80 -3 9 -11 47.60 4.00 3 -9 11 41.40 4.00 -4 9 -11 1.00 2.10 -4 9 -11 0.40 2.10 4 -9 11 -0.30 1.70 -5 9 -11 46.70 4.30 5 -9 11 44.60 3.50 4 8 -11 5.00 1.50 4 8 -11 2.30 2.10 -4 -8 11 5.70 1.60 3 8 -11 7.90 1.60 3 8 -11 6.60 2.50 3 8 -11 8.70 1.90 -3 -8 11 6.90 1.70 2 8 -11 7.10 1.90 2 8 -11 7.50 2.40 2 8 -11 8.30 3.70 1 8 -11 2.30 3.00 1 8 -11 5.10 2.30 1 8 -11 5.90 1.90 0 8 -11 11.40 3.00 0 -8 11 13.70 5.10 -1 8 -11 47.00 5.50 -1 8 -11 51.79 4.10 1 -8 11 34.90 4.70 -2 8 -11 23.60 3.30 -2 8 -11 15.40 3.00 2 -8 11 17.60 2.80 -3 8 -11 77.49 5.60 -3 8 -11 87.29 6.40 3 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2.50 1.30 6 6 -11 -0.70 1.90 5 6 -11 81.99 5.20 5 6 -11 80.29 5.90 5 6 -11 83.49 5.40 -5 -6 11 89.39 5.30 4 6 -11 5.80 1.70 4 6 -11 4.60 2.50 4 6 -11 5.60 1.70 4 6 -11 6.30 2.10 -4 -6 11 6.40 1.80 3 6 -11 15.70 3.00 3 6 -11 18.60 2.60 3 6 -11 19.80 3.70 3 6 -11 29.30 3.80 -3 -6 11 20.20 3.00 2 6 -11 6.60 2.60 2 6 -11 1.30 3.00 2 6 -11 2.50 1.90 2 6 -11 2.20 1.80 -2 -6 11 3.40 1.90 1 6 -11 12.90 2.20 1 6 -11 16.40 2.40 1 6 -11 12.90 3.00 1 6 -11 10.10 3.20 -1 -6 11 13.50 2.20 0 6 -11 4.90 2.20 0 6 -11 1.00 2.90 0 -6 11 -0.80 2.90 -1 6 -11 79.19 5.50 -1 6 -11 81.19 6.80 1 -6 11 64.79 5.90 1 -6 11 59.99 5.20 -2 6 -11 57.29 6.40 -2 6 -11 63.99 5.00 2 -6 11 50.79 5.10 -3 6 -11 3.40 3.00 -3 6 -11 5.90 2.40 3 -6 11 5.20 2.50 -4 6 -11 28.90 4.40 -4 6 -11 23.90 4.80 4 -6 11 16.30 2.80 -5 6 -11 12.90 2.80 -5 6 -11 8.50 3.10 5 -6 11 13.90 2.40 -6 6 -11 19.30 4.40 6 -6 11 23.30 3.50 -7 6 -11 0.70 2.30 -7 6 -11 -0.70 2.50 7 -6 11 3.80 1.80 -8 6 -11 64.69 4.80 8 -6 11 52.69 3.90 8 -6 11 59.09 6.20 6 5 -11 28.30 2.60 6 5 -11 27.80 3.00 6 5 -11 29.90 3.80 5 5 -11 -1.30 1.70 5 5 -11 -1.70 2.20 5 5 -11 0.00 1.60 -5 -5 11 -0.80 1.80 4 5 -11 1.70 1.80 4 5 -11 3.40 1.70 4 5 -11 3.60 3.90 4 5 -11 4.40 2.30 4 5 -11 3.50 1.90 -4 -5 11 4.20 1.90 3 5 -11 2.20 2.60 3 5 -11 3.40 3.20 3 5 -11 4.40 1.80 3 5 -11 2.50 1.80 -3 -5 11 2.80 1.90 2 5 -11 41.30 5.10 2 5 -11 43.70 3.90 2 5 -11 36.30 6.10 2 5 -11 34.40 3.70 -2 -5 11 39.60 3.70 1 5 -11 26.70 5.80 1 5 -11 36.00 3.70 1 5 -11 27.40 3.50 1 5 -11 33.00 5.10 -1 -5 11 30.30 3.30 0 5 -11 64.39 6.30 0 5 -11 68.99 6.90 0 5 -11 71.99 5.10 0 5 -11 61.49 5.10 0 -5 11 56.59 6.20 -1 5 -11 52.89 4.50 -1 5 -11 52.59 6.20 1 -5 11 40.90 5.10 -2 5 -11 30.70 3.80 -2 5 -11 23.90 5.70 2 -5 11 28.40 4.20 -3 5 -11 27.70 4.00 -3 5 -11 30.50 5.50 3 -5 11 31.80 4.30 -4 5 -11 5.10 2.90 -4 5 -11 4.20 2.70 4 -5 11 4.20 2.60 -5 5 -11 23.60 4.90 5 -5 11 24.50 3.90 -6 5 -11 3.00 2.00 -6 5 -11 5.40 2.60 6 -5 11 6.00 2.50 -7 5 -11 7.70 2.00 -7 5 -11 9.60 2.70 -8 5 -11 7.40 2.50 -8 5 -11 7.00 2.50 8 -5 11 8.30 1.80 7 4 -11 22.10 2.40 7 4 -11 23.30 2.20 7 4 -11 18.10 3.10 -7 -4 11 17.90 3.40 6 4 -11 0.40 2.30 6 4 -11 -1.20 1.60 6 4 -11 0.80 1.60 5 4 -11 32.30 4.40 5 4 -11 51.99 8.00 5 4 -11 35.70 3.50 5 4 -11 34.50 3.30 -5 -4 11 39.10 3.60 4 4 -11 6.60 2.40 4 4 -11 5.40 1.90 4 4 -11 5.20 2.90 -4 -4 11 8.10 2.10 3 4 -11 0.40 3.30 3 4 -11 3.30 2.00 3 4 -11 5.50 2.80 3 4 -11 5.00 1.90 3 4 -11 -0.10 2.30 -3 -4 11 3.10 1.90 2 4 -11 15.70 3.10 2 4 -11 23.00 3.30 2 4 -11 30.40 3.50 2 4 -11 23.30 4.80 2 4 -11 17.40 3.70 -2 -4 11 26.20 3.00 1 4 -11 17.40 2.30 1 4 -11 23.60 3.70 1 4 -11 20.70 3.30 -1 -4 11 22.10 2.90 0 4 -11 0.80 2.00 0 4 -11 3.80 2.00 0 4 -11 2.10 3.20 0 4 -11 2.80 2.90 0 -4 11 3.90 2.00 -1 4 -11 34.30 5.90 -1 4 -11 34.40 3.80 -2 4 -11 207.68 11.90 -2 4 -11 185.08 10.80 2 -4 11 161.68 10.70 2 -4 11 180.38 10.90 -3 4 -11 3.40 2.30 -3 4 -11 3.50 3.00 3 -4 11 3.10 2.40 -4 4 -11 8.70 2.80 -4 4 -11 13.40 3.20 4 -4 11 13.60 2.60 -5 4 -11 21.40 3.10 -5 4 -11 31.40 5.20 -5 4 -11 22.20 3.60 -6 4 -11 5.90 2.80 -6 4 -11 1.00 1.80 6 -4 11 10.90 2.60 -7 4 -11 51.49 4.40 -7 4 -11 64.49 5.80 7 -4 11 70.49 4.80 -8 4 -11 15.60 2.70 -8 4 -11 19.40 4.50 8 -4 11 23.10 3.00 9 -4 11 61.79 4.20 9 -4 11 70.89 4.80 7 3 -11 1.30 1.50 7 3 -11 2.30 1.60 7 3 -11 0.50 2.20 -7 -3 11 -0.30 2.20 6 3 -11 128.29 8.70 6 3 -11 143.89 8.10 6 3 -11 130.39 7.90 -6 -3 11 141.89 8.30 5 3 -11 0.60 1.90 5 3 -11 0.50 2.60 5 3 -11 2.90 1.80 5 3 -11 9.10 4.00 4 3 -11 3.10 3.60 4 3 -11 3.20 1.90 4 3 -11 2.60 2.00 4 3 -11 0.70 2.80 4 3 -11 2.00 2.00 -4 -3 11 3.70 1.90 3 3 -11 8.30 3.50 3 3 -11 13.60 2.20 3 3 -11 10.00 2.20 3 3 -11 10.40 3.00 3 3 -11 11.00 2.50 -3 -3 11 15.30 2.80 2 3 -11 34.90 3.80 2 3 -11 41.90 3.70 2 3 -11 33.90 4.70 2 3 -11 34.90 4.90 2 3 -11 28.50 5.90 -2 -3 11 39.00 3.40 1 3 -11 25.70 3.50 1 3 -11 31.60 4.80 1 3 -11 25.40 3.80 1 3 -11 35.10 3.50 -1 -3 11 30.20 3.30 0 3 -11 39.60 3.60 0 3 -11 32.30 3.70 0 3 -11 27.80 5.50 0 3 -11 35.00 5.60 0 -3 11 34.40 5.80 -1 3 -11 56.69 6.30 -1 3 -11 59.49 4.60 1 -3 11 49.90 5.30 1 -3 11 59.89 4.50 -2 3 -11 24.80 5.40 -2 3 -11 25.60 3.50 2 -3 11 22.20 3.80 2 -3 11 19.80 3.50 -3 3 -11 77.29 5.80 -3 3 -11 86.79 7.10 3 -3 11 78.79 5.80 -4 3 -11 19.90 3.10 -4 3 -11 21.60 3.10 -4 3 -11 26.50 5.40 4 -3 11 32.20 3.80 -5 3 -11 4.40 3.00 -5 3 -11 5.30 2.00 -5 3 -11 2.70 3.20 5 -3 11 9.00 2.50 -6 3 -11 15.90 2.90 -6 3 -11 12.70 3.10 -7 3 -11 28.80 3.40 7 -3 11 38.00 3.80 -8 3 -11 45.40 3.90 -8 3 -11 52.99 5.60 8 -3 11 49.80 4.00 -9 3 -11 11.10 3.20 -9 3 -11 6.10 1.70 9 -3 11 6.90 2.00 9 -3 11 7.20 1.70 7 2 -11 -0.20 2.20 7 2 -11 2.50 1.60 7 2 -11 0.30 1.50 -7 -2 11 -1.10 2.20 6 2 -11 0.30 2.60 6 2 -11 3.50 2.00 6 2 -11 2.90 1.90 -6 -2 11 4.50 2.20 5 2 -11 -1.90 3.10 5 2 -11 3.70 2.00 5 2 -11 0.10 3.50 4 2 -11 2.30 2.10 4 2 -11 5.70 2.20 4 2 -11 4.20 2.60 4 2 -11 6.30 5.50 4 2 -11 4.40 2.10 3 2 -11 11.30 2.90 3 2 -11 18.80 2.60 3 2 -11 21.20 2.60 3 2 -11 11.60 3.50 2 2 -11 6.70 2.60 2 2 -11 17.20 3.00 2 2 -11 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0.00 0 3 16 -0.26 0.00 1 3 16 -0.40 0.00 2 3 16 1.46 0.00 3 3 16 1.70 0.00 4 3 16 0.18 0.00 5 3 16 -0.39 0.00 6 3 16 -0.39 0.00 -1 4 16 -0.39 0.00 0 4 16 0.65 0.00 1 4 16 -0.18 0.00 2 4 16 -0.59 0.00 3 4 16 -1.98 0.00 4 4 16 -0.59 0.00 5 4 16 0.60 0.00 6 4 16 0.16 0.00 0 5 16 0.03 0.00 1 5 16 0.03 0.00 2 5 16 1.17 0.00 3 5 16 0.97 0.00 4 5 16 0.99 0.00 5 5 16 0.04 0.00 1 6 16 -0.38 0.00 2 6 16 -0.29 0.00 3 6 16 -1.35 0.00 4 6 16 -0.99 0.00 5 6 16 0.66 0.00 2 7 16 0.10 0.00 3 7 16 0.72 0.00 4 7 16 -0.18 0.00 -12 2 0 -0.47 0.00 11 5 0 -0.60 0.00 9 6 0 2.74 0.00 10 6 0 2.68 0.00 12 6 0 0.07 0.00 11 9 0 -0.51 0.00 10 11 0 -0.17 0.00 -7 12 0 -1.03 0.00 -6 13 0 0.33 0.00 1 16 0 -0.10 0.00 2 16 0 -0.32 0.00 -5 -15 1 1.10 0.00 -7 -14 1 0.38 0.00 -8 -13 1 -0.25 0.00 -9 -12 1 0.05 0.00 7 -12 1 -0.99 0.00 10 -8 1 -0.98 0.00 -12 -5 1 -0.52 0.00 -12 -3 1 -0.39 0.00 -12 -2 1 -0.10 0.00 -2 0 1 38.40 0.00 -12 1 1 0.13 0.00 12 3 1 1.38 0.00 12 4 1 -0.57 0.00 11 5 1 0.13 0.00 -7 12 1 -0.52 0.00 -3 15 1 0.34 0.00 6 15 1 -0.86 0.00 0 16 1 -0.20 0.00 1 16 1 -0.08 0.00 2 16 1 -0.01 0.00 3 16 1 0.31 0.00 2 -15 2 0.26 0.00 -10 -10 2 -0.39 0.00 -11 -8 2 -0.09 0.00 10 -8 2 -0.55 0.00 -12 -3 2 -0.65 0.00 -4 -3 2 -8.79 0.00 12 -3 2 0.47 0.00 -12 -2 2 0.41 0.00 -12 -1 2 -0.15 0.00 -12 0 2 0.04 0.00 12 4 2 -1.04 0.00 -11 5 2 -0.43 0.00 10 6 2 -0.26 0.00 11 6 2 -2.54 0.00 8 7 2 1.79 0.00 9 7 2 -2.06 0.00 12 7 2 0.55 0.00 -3 15 2 0.17 0.00 0 16 2 0.10 0.00 3 16 2 0.82 0.00 -3 -15 3 -0.23 0.00 1 -15 3 -0.12 0.00 4 -14 3 0.38 0.00 -9 -11 3 0.55 0.00 -11 -7 3 0.64 0.00 12 -3 3 -0.22 0.00 -11 4 3 -0.05 0.00 12 4 3 -3.33 0.00 12 5 3 2.40 0.00 10 6 3 -1.48 0.00 11 6 3 -2.71 0.00 -10 7 3 -0.56 0.00 9 7 3 -0.87 0.00 11 10 3 0.28 0.00 9 13 3 -0.07 0.00 0 16 3 0.15 0.00 3 16 3 0.26 0.00 -1 -15 4 -0.12 0.00 -5 -14 4 0.53 0.00 -4 1 4 -0.80 0.00 12 1 4 0.59 0.00 12 2 4 -2.96 0.00 -11 3 4 0.51 0.00 12 3 4 3.16 0.00 12 4 4 -7.44 0.00 11 5 4 4.22 0.00 12 5 4 3.27 0.00 10 6 4 -0.98 0.00 11 6 4 -2.56 0.00 9 7 4 -1.29 0.00 10 7 4 2.36 0.00 -8 10 4 0.58 0.00 11 10 4 -0.04 0.00 9 13 4 -0.33 0.00 -4 14 4 1.04 0.00 1 16 4 -0.43 0.00 3 16 4 -0.57 0.00 -4 -14 5 -0.13 0.00 -7 -12 5 0.00 0.00 6 -12 5 0.02 0.00 -8 -11 5 -0.22 0.00 8 -10 5 -0.40 0.00 -11 -3 5 0.30 0.00 12 -2 5 0.31 0.00 12 -1 5 -0.75 0.00 12 0 5 0.05 0.00 -11 1 5 0.50 0.00 12 1 5 2.32 0.00 12 2 5 -5.14 0.00 12 3 5 5.68 0.00 11 4 5 -5.54 0.00 11 5 5 6.57 0.00 11 6 5 -2.94 0.00 9 7 5 -2.52 0.00 12 7 5 0.13 0.00 11 10 5 -0.60 0.00 -7 11 5 -0.34 0.00 -5 13 5 -0.67 0.00 -3 14 5 0.80 0.00 -2 15 5 -0.70 0.00 2 16 5 0.45 0.00 3 16 5 -0.65 0.00 -2 -14 6 -0.53 0.00 -1 -14 6 -0.70 0.00 0 -14 6 0.50 0.00 1 -14 6 0.73 0.00 4 -13 6 -0.54 0.00 -8 -10 6 -0.23 0.00 10 -7 6 -0.53 0.00 -10 -6 6 -0.73 0.00 12 -1 6 -0.13 0.00 12 0 6 -0.18 0.00 11 2 6 -5.20 0.00 12 2 6 -3.08 0.00 11 3 6 6.84 0.00 -10 4 6 0.06 0.00 10 4 6 -2.34 0.00 12 4 6 -6.59 0.00 11 5 6 6.70 0.00 10 6 6 -0.73 0.00 11 6 6 -3.34 0.00 -9 7 6 0.06 0.00 12 7 6 -0.04 0.00 -8 9 6 -0.20 0.00 6 15 6 -0.53 0.00 -8 -9 7 0.10 0.00 9 -8 7 0.44 0.00 -10 -4 7 -0.64 0.00 11 -4 7 0.70 0.00 11 -3 7 -0.03 0.00 11 -2 7 0.92 0.00 12 -1 7 -0.35 0.00 11 0 7 0.06 0.00 12 0 7 1.10 0.00 11 1 7 1.06 0.00 12 1 7 -0.99 0.00 10 2 7 -3.81 0.00 11 2 7 -3.35 0.00 10 3 7 5.02 0.00 10 4 7 -4.14 0.00 12 4 7 -0.98 0.00 10 5 7 5.93 0.00 11 5 7 3.76 0.00 -9 6 7 0.32 0.00 12 6 7 0.58 0.00 -7 10 7 -0.13 0.00 0 -13 8 -0.19 0.00 -4 -12 8 -0.01 0.00 -8 -8 8 0.27 0.00 9 -4 8 1.64 0.00 11 -3 8 0.20 0.00 10 -2 8 -0.03 0.00 11 -2 8 0.50 0.00 10 -1 8 -1.75 0.00 11 -1 8 -0.34 0.00 10 0 8 -1.38 0.00 11 0 8 1.96 0.00 10 1 8 -0.22 0.00 11 1 8 -1.80 0.00 12 1 8 -2.46 0.00 10 2 8 -2.87 0.00 11 2 8 1.42 0.00 10 3 8 2.21 0.00 11 3 8 -0.96 0.00 12 5 8 -0.79 0.00 11 9 8 0.29 0.00 -2 14 8 -0.78 0.00 1 15 8 0.12 0.00 4 15 8 0.31 0.00 -2 -12 9 0.34 0.00 2 -12 9 -0.49 0.00 -4 -11 9 0.19 0.00 6 -10 9 -0.45 0.00 8 -8 9 1.01 0.00 10 -5 9 -0.44 0.00 -9 -3 9 0.65 0.00 10 -2 9 -0.06 0.00 11 -2 9 0.45 0.00 9 -1 9 -0.54 0.00 10 -1 9 -1.58 0.00 11 -1 9 -1.26 0.00 10 0 9 -0.21 0.00 11 0 9 2.96 0.00 10 1 9 -2.40 0.00 -9 2 9 0.37 0.00 11 2 9 3.95 0.00 -8 6 9 0.52 0.00 11 8 9 0.23 0.00 -5 11 9 -0.47 0.00 -4 12 9 1.34 0.00 -1 13 9 -0.18 0.00 -1 14 9 1.14 0.00 6 14 9 -0.22 0.00 -2 -11 10 0.11 0.00 3 -11 10 -0.51 0.00 -4 -10 10 0.62 0.00 5 -10 10 0.19 0.00 -8 -4 10 0.12 0.00 10 -4 10 0.39 0.00 11 -1 10 -1.24 0.00 -8 4 10 0.06 0.00 5 4 10 -2.47 0.00 4 5 10 5.65 0.00 -7 7 10 0.22 0.00 11 7 10 -0.31 0.00 9 11 10 0.23 0.00 -1 13 10 -0.78 0.00 7 13 10 0.03 0.00 5 14 10 -0.16 0.00 -2 -10 11 0.14 0.00 -4 -9 11 -0.55 0.00 -5 -8 11 0.65 0.00 11 2 11 1.02 0.00 11 3 11 0.68 0.00 11 4 11 0.74 0.00 -7 5 11 -0.09 0.00 11 5 11 -0.14 0.00 -5 9 11 -1.65 0.00 -2 12 11 0.28 0.00 6 13 11 0.24 0.00 -2 -9 12 -0.47 0.00 -7 -1 12 -0.47 0.00 10 -1 12 -0.13 0.00 -7 0 12 0.14 0.00 -7 1 12 -0.28 0.00 10 7 12 0.32 0.00 2 13 12 0.69 0.00 3 13 12 0.39 0.00 -1 -8 13 0.77 0.00 3 -8 13 0.37 0.00 -3 -7 13 -0.95 0.00 5 -7 13 -0.06 0.00 -4 -6 13 0.32 0.00 -5 -4 13 -0.12 0.00 -6 -1 13 -0.08 0.00 -6 0 13 0.86 0.00 -6 1 13 -0.22 0.00 -6 2 13 1.14 0.00 -5 6 13 -0.45 0.00 -3 9 13 -0.56 0.00 -2 10 13 0.13 0.00 2 12 13 -0.58 0.00 3 12 13 0.86 0.00 4 12 13 -0.02 0.00 1 -7 14 0.47 0.00 2 -7 14 -0.35 0.00 -2 -6 14 0.20 0.00 -3 -5 14 -0.42 0.00 -5 1 14 -0.24 0.00 7 1 14 -0.16 0.00 9 2 14 -0.01 0.00 9 3 14 -0.69 0.00 9 4 14 0.37 0.00 7 9 14 0.00 0.00 0 10 14 -0.55 0.00 6 10 14 -0.52 0.00 2 11 14 -0.69 0.00 3 11 14 -0.25 0.00 4 11 14 -0.75 0.00 0 -5 15 0.10 0.00 3 -5 15 0.43 0.00 5 -4 15 -0.60 0.00 -3 -2 15 0.51 0.00 7 -1 15 -0.83 0.00 8 2 15 0.82 0.00 8 3 15 0.08 0.00 8 4 15 0.44 0.00 7 7 15 0.22 0.00 1 9 15 0.81 0.00 5 9 15 0.17 0.00 1 -3 16 0.83 0.00 2 -3 16 0.55 0.00 4 -2 16 -0.80 0.00 -1 -1 16 1.19 0.00 5 -1 16 0.34 0.00 6 1 16 -0.27 0.00 -1 5 16 -0.63 0.00 6 5 16 -0.04 0.00 0 6 16 -0.14 0.00 1 7 16 0.48 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 100616) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.500 0.000 237 80 ' ' 2 0.500 1.000 0.000 152 40 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta -2 0 1 9.614 -4 -3 2 21.436 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL cu_molan50P -1m_a R = 0.15 CELL 10.7043 13.6484 14.3016 81.39 78.69 81.44 SPGR P-1 # Solvent Accessible Volume = 391 # Note: Atoms in Void as Cxxx and Qxxx all others C101 0.486 1.008 0.076 ! 5.41 eA-3 C102 0.203 0.602 0.153 ! 5.36 eA-3 C103 0.093 0.540 0.198 ! 5.10 eA-3 C104 0.531 0.098 0.029 ! 4.35 eA-3 C105 0.121 0.449 0.079 ! 4.27 eA-3 C106 0.044 0.468 0.161 ! 4.16 eA-3 C107 0.185 0.550 0.048 ! 4.04 eA-3 C108 0.409 0.935 0.044 ! 3.77 eA-3 C109 0.205 0.507 0.176 ! 3.20 eA-3 C110 0.107 0.577 0.044 ! 3.10 eA-3 C111 0.141 0.645 0.098 ! 2.37 eA-3 C112 0.211 0.610 0.064 ! 1.62 eA-3 Q113 0.109 0.858 0.114 ! 0.83 eA-3 C114 0.330 0.973 0.010 ! 0.66 eA-3 C115 0.055 0.441 0.031 ! 0.63 eA-3 C116 1.000 0.589 0.032 ! 0.59 eA-3 Q117 0.203 0.709 0.047 ! 0.57 eA-3 Q118 0.284 0.429 0.130 ! 0.57 eA-3 Q119 0.082 0.175 0.271 ! 0.55 eA-3 C120 1.007 0.519 0.093 ! 0.54 eA-3 Q121 0.011 0.827 0.150 ! 0.51 eA-3 ) ; _shelx_fab_checksum 812 #===END data_twin5_100K _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C42 H38 Fe N8 O4' _chemical_formula_weight 774.65 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 2/c' _space_group_name_Hall '-C 2yc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 18.8670(8) _cell_length_b 9.9736(4) _cell_length_c 21.0794(8) _cell_angle_alpha 90 _cell_angle_beta 112.918(2) _cell_angle_gamma 90 _cell_volume 3653.4(3) _cell_formula_units_Z 4 _cell_measurement_temperature 101(2) _cell_measurement_reflns_used 4635 _cell_measurement_theta_min 4.55 _cell_measurement_theta_max 65.11 _exptl_crystal_description 'needle' _exptl_crystal_colour 'red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.408 _exptl_crystal_F_000 1616 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 3.766 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.490688 _exptl_absorpt_correction_T_max 0.752592 _exptl_absorpt_process_details 'SADABS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 101(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 3060 _diffrn_reflns_av_unetI/netI 0.0477 _diffrn_reflns_av_R_equivalents ? _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min 0 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_theta_min 4.555 _diffrn_reflns_theta_max 65.196 _diffrn_reflns_theta_full 65.196 _diffrn_measured_fraction_theta_max 0.967 _diffrn_measured_fraction_theta_full 0.967 _diffrn_reflns_Laue_measured_fraction_max 0.967 _diffrn_reflns_Laue_measured_fraction_full 0.967 _diffrn_reflns_point_group_measured_fraction_max 0.967 _diffrn_reflns_point_group_measured_fraction_full 0.967 _reflns_number_total 3060 _reflns_number_gt 2786 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refined as a 2-component twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0837P)^2^+16.6108P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3060 _refine_ls_number_parameters 252 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0727 _refine_ls_R_factor_gt 0.0633 _refine_ls_wR_factor_ref 0.1729 _refine_ls_wR_factor_gt 0.1647 _refine_ls_goodness_of_fit_ref 1.133 _refine_ls_restrained_S_all 1.133 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.5000 0.45198(13) 0.7500 0.0191(3) Uani 1 2 d S T P . . O1 O 0.6368(2) 0.8054(4) 1.04105(19) 0.0312(10) Uani 1 1 d . . . . . O2 O 0.3045(2) 0.1862(4) 0.44828(19) 0.0268(9) Uani 1 1 d . . . . . N1 N 0.5937(3) 0.5245(5) 0.8002(2) 0.0215(10) Uani 1 1 d . . . . . N2 N 0.6572(2) 0.5296(4) 0.7880(2) 0.0194(10) Uani 1 1 d . . . . . N3 N 0.6028(2) 0.4032(5) 0.6813(2) 0.0190(10) Uani 1 1 d . . . . . N4 N 0.5336(2) 0.3965(5) 0.6838(2) 0.0177(9) Uani 1 1 d . . . . . C1 C 0.6029(3) 0.5966(6) 0.8623(3) 0.0216(12) Uani 1 1 d . . . . . C2 C 0.5467(3) 0.6862(6) 0.8621(3) 0.0236(12) Uani 1 1 d . . . . . H2 H 0.5018 0.6983 0.8215 0.028 Uiso 1 1 calc R U . . . C3 C 0.5559(3) 0.7580(6) 0.9209(3) 0.0255(12) Uani 1 1 d . . . . . H3 H 0.5176 0.8204 0.9203 0.031 Uiso 1 1 calc R U . . . C4 C 0.6206(3) 0.7395(6) 0.9805(3) 0.0256(13) Uani 1 1 d . . . . . C5 C 0.6760(4) 0.6451(6) 0.9805(3) 0.0275(13) Uani 1 1 d . . . . . H5 H 0.7198 0.6290 1.0217 0.033 Uiso 1 1 calc R U . . . C6 C 0.6675(3) 0.5762(6) 0.9219(3) 0.0239(12) Uani 1 1 d . . . . . H6 H 0.7059 0.5145 0.9221 0.029 Uiso 1 1 calc R U . . . C7 C 0.6593(3) 0.4686(5) 0.7322(2) 0.0179(11) Uani 1 1 d . . . . . C8 C 0.7349(3) 0.4740(6) 0.7261(3) 0.0203(12) Uani 1 1 d . . . . . C9 C 0.7940(3) 0.5529(6) 0.7690(3) 0.0245(12) Uani 1 1 d . . . . . H9 H 0.7857 0.6078 0.8022 0.029 Uiso 1 1 calc R U . . . C10 C 0.8649(3) 0.5539(6) 0.7647(3) 0.0273(13) Uani 1 1 d . . . . . H10 H 0.9050 0.6090 0.7947 0.033 Uiso 1 1 calc R U . . . C11 C 0.8776(3) 0.4733(6) 0.7159(3) 0.0265(13) Uani 1 1 d . . . . . H11 H 0.9266 0.4727 0.7128 0.032 Uiso 1 1 calc R U . . . C12 C 0.8189(3) 0.3948(6) 0.6723(3) 0.0247(13) Uani 1 1 d . . . . . H12 H 0.8274 0.3398 0.6391 0.030 Uiso 1 1 calc R U . . . C13 C 0.7481(3) 0.3953(6) 0.6764(3) 0.0227(11) Uani 1 1 d . . . . . H13 H 0.7076 0.3421 0.6454 0.027 Uiso 1 1 calc R U . . . C14 C 0.5854(4) 0.9111(6) 1.0411(3) 0.0342(15) Uani 1 1 d . . . . . H00A H 0.5826 0.9774 1.0059 0.051 Uiso 1 1 calc R U . . . H00B H 0.6044 0.9542 1.0864 0.051 Uiso 1 1 calc R U . . . H00D H 0.5341 0.8739 1.0310 0.051 Uiso 1 1 calc R U . . . C15 C 0.4795(3) 0.3380(5) 0.6222(3) 0.0201(12) Uani 1 1 d . . . . . C16 C 0.4749(3) 0.3756(6) 0.5581(3) 0.0221(12) Uani 1 1 d . . . . . H16 H 0.5122 0.4360 0.5546 0.027 Uiso 1 1 calc R U . . . C17 C 0.4180(3) 0.3285(6) 0.4986(3) 0.0246(13) Uani 1 1 d . . . . . H17 H 0.4158 0.3563 0.4547 0.030 Uiso 1 1 calc R U . . . C18 C 0.3630(3) 0.2384(6) 0.5038(3) 0.0188(12) Uani 1 1 d . . . . . C19 C 0.3687(3) 0.1978(6) 0.5677(3) 0.0254(12) Uani 1 1 d . . . . . H19 H 0.3327 0.1345 0.5711 0.031 Uiso 1 1 calc R U . . . C20 C 0.4249(3) 0.2460(6) 0.6269(3) 0.0214(12) Uani 1 1 d . . . . . H20 H 0.4270 0.2177 0.6706 0.026 Uiso 1 1 calc R U . . . C21 C 0.2919(4) 0.2366(7) 0.3818(3) 0.0327(14) Uani 1 1 d . . . . . H21A H 0.3351 0.2113 0.3695 0.049 Uiso 1 1 calc R U . . . H21B H 0.2878 0.3346 0.3819 0.049 Uiso 1 1 calc R U . . . H21C H 0.2442 0.1988 0.3481 0.049 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0136(6) 0.0248(6) 0.0185(6) 0.000 0.0058(5) 0.000 O1 0.032(2) 0.034(2) 0.026(2) -0.0053(18) 0.0095(18) 0.003(2) O2 0.021(2) 0.029(2) 0.027(2) -0.0045(17) 0.0053(17) -0.0013(18) N1 0.020(2) 0.025(3) 0.022(2) -0.004(2) 0.010(2) 0.0015(19) N2 0.019(2) 0.020(2) 0.021(2) -0.0006(19) 0.0101(19) -0.003(2) N3 0.012(2) 0.024(2) 0.023(2) -0.0002(19) 0.0095(18) 0.0044(19) N4 0.013(2) 0.019(2) 0.020(2) 0.0004(18) 0.0050(18) 0.0019(18) C1 0.020(3) 0.025(3) 0.022(3) -0.004(2) 0.010(2) -0.009(2) C2 0.015(3) 0.030(3) 0.024(3) -0.001(2) 0.006(2) -0.004(3) C3 0.026(3) 0.021(3) 0.033(3) 0.000(3) 0.015(3) -0.001(2) C4 0.030(3) 0.028(3) 0.021(3) 0.000(2) 0.011(2) -0.002(2) C5 0.027(3) 0.032(3) 0.021(3) -0.001(2) 0.007(2) -0.004(3) C6 0.021(3) 0.025(3) 0.025(3) 0.000(2) 0.008(2) -0.001(2) C7 0.012(2) 0.019(3) 0.021(3) -0.001(2) 0.005(2) 0.002(2) C8 0.014(3) 0.026(3) 0.020(3) 0.003(2) 0.006(2) 0.003(2) C9 0.018(3) 0.033(3) 0.022(3) -0.003(2) 0.008(2) -0.003(2) C10 0.019(3) 0.033(3) 0.028(3) -0.006(3) 0.008(2) -0.012(2) C11 0.015(3) 0.035(4) 0.032(3) 0.004(3) 0.011(2) 0.001(2) C12 0.015(3) 0.032(3) 0.029(3) -0.004(3) 0.012(2) 0.002(2) C13 0.016(3) 0.025(3) 0.026(3) 0.001(2) 0.007(2) 0.003(2) C14 0.041(4) 0.030(3) 0.034(3) -0.008(3) 0.017(3) 0.004(3) C15 0.017(3) 0.022(3) 0.021(3) -0.007(2) 0.007(2) 0.007(2) C16 0.015(3) 0.026(3) 0.025(3) -0.003(2) 0.007(2) -0.003(2) C17 0.026(3) 0.028(3) 0.021(3) 0.005(2) 0.011(2) 0.008(2) C18 0.009(3) 0.021(3) 0.023(3) -0.005(2) 0.003(2) 0.004(2) C19 0.022(3) 0.019(3) 0.033(3) 0.000(3) 0.009(2) 0.000(2) C20 0.018(3) 0.023(3) 0.026(3) -0.001(2) 0.012(2) 0.002(2) C21 0.032(3) 0.036(3) 0.025(3) -0.008(3) 0.006(3) -0.004(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.819(4) . ? Fe1 N1 1.819(4) 2_656 ? Fe1 N4 1.830(4) 2_656 ? Fe1 N4 1.830(4) . ? O1 C4 1.360(7) . ? O1 C14 1.432(7) . ? O2 C18 1.361(6) . ? O2 C21 1.419(7) . ? N1 N2 1.321(6) . ? N1 C1 1.444(7) . ? N2 C7 1.338(6) . ? N3 N4 1.328(6) . ? N3 C7 1.349(7) . ? N4 C15 1.427(7) . ? C1 C6 1.382(8) . ? C1 C2 1.385(8) . ? C2 C3 1.382(8) . ? C2 H2 0.9500 . ? C3 C4 1.382(8) . ? C3 H3 0.9500 . ? C4 C5 1.406(8) . ? C5 C6 1.369(8) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 C8 1.482(7) . ? C8 C9 1.377(8) . ? C8 C13 1.406(8) . ? C9 C10 1.376(8) . ? C9 H9 0.9500 . ? C10 C11 1.397(8) . ? C10 H10 0.9500 . ? C11 C12 1.376(8) . ? C11 H11 0.9500 . ? C12 C13 1.371(7) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C14 H00A 0.9800 . ? C14 H00B 0.9800 . ? C14 H00D 0.9800 . ? C15 C16 1.373(7) . ? C15 C20 1.411(8) . ? C16 C17 1.379(8) . ? C16 H16 0.9500 . ? C17 C18 1.409(8) . ? C17 H17 0.9500 . ? C18 C19 1.370(8) . ? C19 C20 1.372(8) . ? C19 H19 0.9500 . ? C20 H20 0.9500 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N1 133.2(3) . 2_656 ? N1 Fe1 N4 102.91(19) . 2_656 ? N1 Fe1 N4 90.97(18) 2_656 2_656 ? N1 Fe1 N4 90.97(18) . . ? N1 Fe1 N4 102.91(19) 2_656 . ? N4 Fe1 N4 144.8(3) 2_656 . ? C4 O1 C14 116.8(4) . . ? C18 O2 C21 118.8(4) . . ? N2 N1 C1 111.0(4) . . ? N2 N1 Fe1 130.7(3) . . ? C1 N1 Fe1 118.2(3) . . ? N1 N2 C7 119.5(4) . . ? N4 N3 C7 118.5(4) . . ? N3 N4 C15 110.6(4) . . ? N3 N4 Fe1 130.7(3) . . ? C15 N4 Fe1 118.7(3) . . ? C6 C1 C2 120.1(5) . . ? C6 C1 N1 120.2(5) . . ? C2 C1 N1 119.8(5) . . ? C3 C2 C1 120.2(5) . . ? C3 C2 H2 119.9 . . ? C1 C2 H2 119.9 . . ? C4 C3 C2 120.3(6) . . ? C4 C3 H3 119.9 . . ? C2 C3 H3 119.9 . . ? O1 C4 C3 125.8(5) . . ? O1 C4 C5 115.4(5) . . ? C3 C4 C5 118.8(5) . . ? C6 C5 C4 120.7(5) . . ? C6 C5 H5 119.6 . . ? C4 C5 H5 119.6 . . ? C5 C6 C1 119.9(6) . . ? C5 C6 H6 120.1 . . ? C1 C6 H6 120.1 . . ? N2 C7 N3 129.3(5) . . ? N2 C7 C8 114.8(4) . . ? N3 C7 C8 115.9(4) . . ? C9 C8 C13 118.3(5) . . ? C9 C8 C7 121.7(5) . . ? C13 C8 C7 120.0(5) . . ? C10 C9 C8 121.4(5) . . ? C10 C9 H9 119.3 . . ? C8 C9 H9 119.3 . . ? C9 C10 C11 119.6(5) . . ? C9 C10 H10 120.2 . . ? C11 C10 H10 120.2 . . ? C12 C11 C10 119.6(5) . . ? C12 C11 H11 120.2 . . ? C10 C11 H11 120.2 . . ? C13 C12 C11 120.5(5) . . ? C13 C12 H12 119.8 . . ? C11 C12 H12 119.8 . . ? C12 C13 C8 120.5(5) . . ? C12 C13 H13 119.7 . . ? C8 C13 H13 119.7 . . ? O1 C14 H00A 109.5 . . ? O1 C14 H00B 109.5 . . ? H00A C14 H00B 109.5 . . ? O1 C14 H00D 109.5 . . ? H00A C14 H00D 109.5 . . ? H00B C14 H00D 109.5 . . ? C16 C15 C20 118.6(5) . . ? C16 C15 N4 122.1(5) . . ? C20 C15 N4 119.1(5) . . ? C15 C16 C17 122.0(5) . . ? C15 C16 H16 119.0 . . ? C17 C16 H16 119.0 . . ? C16 C17 C18 118.9(5) . . ? C16 C17 H17 120.6 . . ? C18 C17 H17 120.6 . . ? O2 C18 C19 117.3(5) . . ? O2 C18 C17 123.5(5) . . ? C19 C18 C17 119.1(5) . . ? C18 C19 C20 121.9(5) . . ? C18 C19 H19 119.1 . . ? C20 C19 H19 119.1 . . ? C19 C20 C15 119.4(5) . . ? C19 C20 H20 120.3 . . ? C15 C20 H20 120.3 . . ? O2 C21 H21A 109.5 . . ? O2 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? O2 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? _refine_diff_density_max 1.148 _refine_diff_density_min -0.390 _refine_diff_density_rms 0.100 _shelx_res_file ; twin5_100K.res created by SHELXL-2014/7 TITL twin4_a.res in C2/c REM Old TITL twin4 in C2/c REM SHELXT solution in C2/c REM R1 0.189, Rweak 0.040, Alpha 0.089, Orientation as input REM Formula found by SHELXT: C42 N8 O4 Fe CELL 1.54178 18.8670 9.9736 21.0794 90.000 112.918 90.000 ZERR 4.000 0.0008 0.0004 0.0008 0.000 0.002 0.000 LATT 7 SYMM -X, Y, 1/2-Z SFAC C H N O FE UNIT 168 152 32 16 4 TEMP -172.350 L.S. 10 BOND $H LIST 4 FMAP 2 acta rem shel 10 0.87 PLAN 5 WGHT 0.083700 16.610800 BASF 0.46962 FVAR 0.42284 FE1 5 0.500000 0.451979 0.750000 10.50000 0.01362 0.02477 = 0.01854 0.00000 0.00581 0.00000 O1 4 0.636790 0.805361 1.041052 11.00000 0.03216 0.03394 = 0.02584 -0.00531 0.00947 0.00339 O2 4 0.304519 0.186193 0.448283 11.00000 0.02078 0.02898 = 0.02702 -0.00448 0.00527 -0.00132 N1 3 0.593664 0.524457 0.800189 11.00000 0.02001 0.02468 = 0.02179 -0.00366 0.01021 0.00152 N2 3 0.657196 0.529617 0.787971 11.00000 0.01871 0.02044 = 0.02120 -0.00063 0.01014 -0.00329 N3 3 0.602822 0.403223 0.681328 11.00000 0.01240 0.02433 = 0.02261 -0.00019 0.00951 0.00437 N4 3 0.533622 0.396513 0.683766 11.00000 0.01325 0.01875 = 0.01980 0.00042 0.00497 0.00187 C1 1 0.602917 0.596620 0.862327 11.00000 0.01962 0.02507 = 0.02230 -0.00352 0.01044 -0.00858 C2 1 0.546733 0.686198 0.862102 11.00000 0.01468 0.03032 = 0.02450 -0.00118 0.00615 -0.00362 AFIX 43 H2 2 0.501757 0.698302 0.821456 11.00000 -1.20000 AFIX 0 C3 1 0.555937 0.758046 0.920877 11.00000 0.02614 0.02129 = 0.03270 -0.00041 0.01534 -0.00115 AFIX 43 H3 2 0.517618 0.820423 0.920256 11.00000 -1.20000 AFIX 0 C4 1 0.620633 0.739535 0.980534 11.00000 0.02968 0.02796 = 0.02066 -0.00028 0.01144 -0.00156 C5 1 0.676000 0.645132 0.980529 11.00000 0.02712 0.03180 = 0.02135 -0.00096 0.00699 -0.00362 AFIX 43 H5 2 0.719766 0.629017 1.021690 11.00000 -1.20000 AFIX 0 C6 1 0.667503 0.576229 0.921856 11.00000 0.02103 0.02514 = 0.02475 -0.00017 0.00818 -0.00092 AFIX 43 H6 2 0.705933 0.514496 0.922051 11.00000 -1.20000 AFIX 0 C7 1 0.659295 0.468602 0.732176 11.00000 0.01217 0.01881 = 0.02108 -0.00098 0.00458 0.00221 C8 1 0.734872 0.473954 0.726074 11.00000 0.01430 0.02609 = 0.02002 0.00349 0.00605 0.00305 C9 1 0.794035 0.552855 0.768970 11.00000 0.01793 0.03310 = 0.02227 -0.00294 0.00756 -0.00295 AFIX 43 H9 2 0.785708 0.607760 0.802250 11.00000 -1.20000 AFIX 0 C10 1 0.864938 0.553850 0.764652 11.00000 0.01931 0.03305 = 0.02834 -0.00564 0.00787 -0.01187 AFIX 43 H10 2 0.905039 0.609009 0.794664 11.00000 -1.20000 AFIX 0 C11 1 0.877632 0.473277 0.715875 11.00000 0.01469 0.03476 = 0.03188 0.00403 0.01108 0.00094 AFIX 43 H11 2 0.926552 0.472695 0.712811 11.00000 -1.20000 AFIX 0 C12 1 0.818854 0.394782 0.672306 11.00000 0.01545 0.03189 = 0.02940 -0.00375 0.01165 0.00225 AFIX 43 H12 2 0.827367 0.339821 0.639140 11.00000 -1.20000 AFIX 0 C13 1 0.748073 0.395288 0.676398 11.00000 0.01642 0.02466 = 0.02571 0.00094 0.00681 0.00300 AFIX 43 H13 2 0.707628 0.342056 0.645419 11.00000 -1.20000 AFIX 0 C14 1 0.585430 0.911062 1.041106 11.00000 0.04103 0.03047 = 0.03372 -0.00817 0.01729 0.00383 AFIX 137 H00A 2 0.582617 0.977378 1.005898 11.00000 -1.50000 H00B 2 0.604442 0.954230 1.086444 11.00000 -1.50000 H00D 2 0.534089 0.873905 1.031012 11.00000 -1.50000 AFIX 0 C15 1 0.479502 0.337961 0.622196 11.00000 0.01699 0.02210 = 0.02087 -0.00657 0.00698 0.00733 C16 1 0.474947 0.375600 0.558091 11.00000 0.01458 0.02619 = 0.02512 -0.00278 0.00726 -0.00327 AFIX 43 H16 2 0.512219 0.435992 0.554637 11.00000 -1.20000 AFIX 0 C17 1 0.417966 0.328493 0.498562 11.00000 0.02574 0.02842 = 0.02107 0.00531 0.01073 0.00833 AFIX 43 H17 2 0.415812 0.356327 0.454747 11.00000 -1.20000 AFIX 0 C18 1 0.362992 0.238405 0.503781 11.00000 0.00948 0.02051 = 0.02298 -0.00471 0.00271 0.00422 C19 1 0.368700 0.197826 0.567660 11.00000 0.02234 0.01927 = 0.03336 0.00003 0.00943 0.00039 AFIX 43 H19 2 0.332720 0.134519 0.571059 11.00000 -1.20000 AFIX 0 C20 1 0.424894 0.245984 0.626888 11.00000 0.01763 0.02341 = 0.02607 -0.00055 0.01164 0.00162 AFIX 43 H20 2 0.427025 0.217697 0.670629 11.00000 -1.20000 AFIX 0 C21 1 0.291927 0.236620 0.381817 11.00000 0.03160 0.03633 = 0.02540 -0.00829 0.00581 -0.00413 AFIX 137 H21A 2 0.335140 0.211301 0.369514 11.00000 -1.50000 H21B 2 0.287768 0.334554 0.381947 11.00000 -1.50000 H21C 2 0.244176 0.198833 0.348082 11.00000 -1.50000 AFIX 0 HKLF 5 REM twin4_a.res in C2/c REM R1 = 0.0633 for 2786 Fo > 4sig(Fo) and 0.0727 for all 3060 data REM 252 parameters refined using 0 restraints END WGHT 0.0837 16.6113 REM Highest difference peak 1.148, deepest hole -0.390, 1-sigma level 0.100 Q1 1 0.4756 0.4535 0.6964 11.00000 0.05 1.15 Q2 1 0.6317 0.5381 0.8603 11.00000 0.05 0.44 Q3 1 0.6408 0.6236 0.9304 11.00000 0.05 0.41 Q4 1 0.5621 0.5049 0.7518 11.00000 0.05 0.41 Q5 1 0.3393 0.1768 0.5138 11.00000 0.05 0.40 ; _shelx_res_checksum 68627 _shelx_hkl_file ; -1 0 1 -0.9706 0.96654 -2 1 0 0 -0.9706 0.96654 1 -2 0 2 3002.90 94.4453 -2 2 0 0 3002.90 94.4453 1 -3 0 3 -0.9089 3.38678 -2 3 0 0 -0.9089 3.38678 1 4 0 0 2605.14 56.2488 1 -5 0 4 -0.5435 3.77142 -2 5 0 0 -0.5435 3.77142 1 -6 0 5 801.653 20.7644 -2 6 0 0 801.653 20.7644 1 -7 0 6 -4.6781 4.64445 -2 7 0 0 -4.6781 4.64445 1 -8 0 7 660.112 21.5374 -2 8 0 0 660.112 21.5374 1 -9 0 8 1.89616 5.46273 -2 9 0 0 1.89616 5.46273 1 -10 0 9 362.672 15.3082 -2 10 0 0 362.672 15.3082 1 11 0 0 1.50934 6.69971 1 12 0 0 163.361 16.3522 1 -14 0 12 70.4901 24.2493 -2 14 0 0 70.4901 24.2493 1 -15 0 13 -25.867 19.6388 -2 15 0 0 -25.867 19.6388 1 -16 0 14 74.5033 21.4944 -2 16 0 0 74.5033 21.4944 1 -18 0 16 80.0989 26.6255 -2 18 0 0 80.0989 26.6255 1 -20 0 17 31.8031 22.2548 -2 20 0 0 31.8031 22.2548 1 0 1 0 -0.0536 0.25142 -2 0 1 0 -0.0536 0.25142 1 -2 1 2 -0.4817 1.54764 -2 2 1 0 -0.4817 1.54764 1 -3 1 3 3465.72 75.8939 -2 3 1 0 3465.72 75.8939 1 4 1 0 -0.5240 0.65390 1 -5 1 4 1808.59 35.5163 -2 5 1 0 1808.59 35.5163 1 -6 1 5 0.66862 2.76925 -2 6 1 0 0.66862 2.76925 1 -7 1 6 2693.41 67.4643 -2 7 1 0 2693.41 67.4643 1 -8 1 7 -2.6101 3.08324 -2 8 1 0 -2.6101 3.08324 1 -9 1 8 124.073 4.12960 -2 9 1 0 124.073 4.12960 1 -10 1 9 2.13089 9.44506 -2 10 1 0 2.13089 9.44506 1 -11 1 10 949.952 55.1787 -2 11 1 0 949.952 55.1787 1 -12 1 11 -3.2722 24.5078 -2 12 1 0 -3.2722 24.5078 1 -13 1 11 960.564 31.6629 -2 13 1 0 960.564 31.6629 1 -15 1 13 709.087 31.4804 -2 15 1 0 709.087 31.4804 1 -16 1 14 4.81579 14.2721 -2 16 1 0 4.81579 14.2721 1 -17 1 15 186.817 17.7608 -2 17 1 0 186.817 17.7608 1 -18 1 16 18.1694 26.2586 -2 18 1 0 18.1694 26.2586 1 -19 1 17 315.470 23.2459 -2 19 1 0 315.470 23.2459 1 -20 1 17 19.5746 15.6142 -2 20 1 0 19.5746 15.6142 1 0 2 0 465.769 9.77590 -2 0 2 0 465.769 9.77590 1 -1 2 1 1.00332 1.27181 -2 1 2 0 1.00332 1.27181 1 -2 2 2 186.468 3.41673 -2 2 2 0 186.468 3.41673 1 -3 2 3 3.43534 2.97799 -2 3 2 0 3.43534 2.97799 1 4 2 0 336.310 7.86047 1 -5 2 4 -2.3703 2.82464 -2 5 2 0 -2.3703 2.82464 1 -6 2 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1 -12 5 13 -7.6772 37.1456 -2 12 5 3 -7.6772 37.1456 1 -14 5 15 19.1481 10.5766 -2 14 5 3 19.1481 10.5766 1 -15 5 16 102.133 13.8947 -2 15 5 3 102.133 13.8947 1 -16 5 17 -3.9814 12.3474 -2 16 5 3 -3.9814 12.3474 1 -17 5 18 101.529 23.2253 -2 17 5 3 101.529 23.2253 1 -18 6 13 111.011 10.7528 -2 -18 6 3 111.011 10.7528 1 -17 6 12 12.2753 9.22525 -2 -17 6 3 12.2753 9.22525 1 -16 6 11 213.102 12.8694 -2 -16 6 3 213.102 12.8694 1 -15 6 10 9.35338 8.76660 -2 -15 6 3 9.35338 8.76660 1 -13 6 8 22.1919 21.0406 -2 -13 6 3 22.1919 21.0406 1 -11 6 7 -2.6809 20.1853 -2 -11 6 3 -2.6809 20.1853 1 -10 6 6 337.451 15.0962 -2 -10 6 3 337.451 15.0962 1 -9 6 5 1.53811 8.87282 -2 -9 6 3 1.53811 8.87282 1 -8 6 4 729.114 20.7250 -2 -8 6 3 729.114 20.7250 1 -7 6 3 -11.654 9.67884 -2 -7 6 3 -11.654 9.67884 1 -6 6 2 198.100 11.4397 -2 -6 6 3 198.100 11.4397 1 -5 6 1 23.3842 18.2716 -2 -5 6 3 23.3842 18.2716 1 -4 6 1 948.944 35.9466 -2 -4 6 3 948.944 35.9466 1 3 6 0 -7.8056 7.51376 -2 -3 6 3 -7.8056 7.51376 1 2 6 1 503.324 9.70191 -2 -2 6 3 503.324 9.70191 1 1 6 2 -2.1943 4.44172 -2 -1 6 3 -2.1943 4.44172 1 0 6 3 417.277 7.67963 -2 0 6 3 417.277 7.67963 1 -1 6 4 10.6801 4.83454 -2 1 6 3 10.6801 4.83454 1 -2 6 5 680.290 14.9035 -2 2 6 3 680.290 14.9035 1 -3 6 6 -21.448 24.9679 -2 3 6 3 -21.448 24.9679 1 4 6 3 9.85138 4.70870 1 -5 6 7 -11.346 10.4713 -2 5 6 3 -11.346 10.4713 1 -6 6 8 478.574 18.0980 -2 6 6 3 478.574 18.0980 1 -7 6 9 -8.8483 9.08715 -2 7 6 3 -8.8483 9.08715 1 -8 6 10 860.342 27.5201 -2 8 6 3 860.342 27.5201 1 -9 6 11 -4.9530 10.9279 -2 9 6 3 -4.9530 10.9279 1 -10 6 12 337.881 14.8328 -2 10 6 3 337.881 14.8328 1 -11 6 13 -15.448 21.6009 -2 11 6 3 -15.448 21.6009 1 12 6 3 11.4363 5.63974 1 -13 6 14 15.6679 19.8992 -2 13 6 3 15.6679 19.8992 1 -14 6 15 271.145 20.1848 -2 14 6 3 271.145 20.1848 1 -16 6 17 87.5184 15.3349 -2 16 6 3 87.5184 15.3349 1 -17 7 12 64.2076 11.2749 -2 -17 7 3 64.2076 11.2749 1 -16 7 11 0.06134 7.65108 -2 -16 7 3 0.06134 7.65108 1 -15 7 10 32.2413 7.80542 -2 -15 7 3 32.2413 7.80542 1 -14 7 9 -3.6655 10.8172 -2 -14 7 3 -3.6655 10.8172 1 -13 7 8 579.109 25.6578 -2 -13 7 3 579.109 25.6578 1 -12 7 7 11.4315 21.8886 -2 -12 7 3 11.4315 21.8886 1 -11 7 7 438.656 23.7631 -2 -11 7 3 438.656 23.7631 1 -10 7 6 -11.528 12.7042 -2 -10 7 3 -11.528 12.7042 1 -9 7 5 521.593 15.5130 -2 -9 7 3 521.593 15.5130 1 -8 7 4 0.55093 7.21840 -2 -8 7 3 0.55093 7.21840 1 -7 7 3 14.9181 7.93090 -2 -7 7 3 14.9181 7.93090 1 -6 7 2 -4.6442 8.19499 -2 -6 7 3 -4.6442 8.19499 1 -5 7 1 1613.86 48.3672 -2 -5 7 3 1613.86 48.3672 1 3 7 0 340.491 13.8674 -2 -3 7 3 340.491 13.8674 1 2 7 1 0.08886 6.41907 -2 -2 7 3 0.08886 6.41907 1 1 7 2 92.2199 6.56064 -2 -1 7 3 92.2199 6.56064 1 0 7 3 -0.0556 4.52032 -2 0 7 3 -0.0556 4.52032 1 -1 7 4 107.979 7.29117 -2 1 7 3 107.979 7.29117 1 -2 7 5 -5.0956 8.27529 -2 2 7 3 -5.0956 8.27529 1 -3 7 6 269.320 14.3033 -2 3 7 3 269.320 14.3033 1 -5 7 7 1109.99 30.1479 -2 5 7 3 1109.99 30.1479 1 -6 7 8 -12.750 13.0191 -2 6 7 3 -12.750 13.0191 1 -7 7 9 363.584 13.7711 -2 7 7 3 363.584 13.7711 1 -8 7 10 -4.5452 9.76794 -2 8 7 3 -4.5452 9.76794 1 -9 7 11 209.528 13.5778 -2 9 7 3 209.528 13.5778 1 -11 7 13 84.4836 33.1862 -2 11 7 3 84.4836 33.1862 1 -12 7 13 9.42514 33.7145 -2 12 7 3 9.42514 33.7145 1 -13 7 14 69.0352 18.5567 -2 13 7 3 69.0352 18.5567 1 -14 7 15 -1.4259 14.0203 -2 14 7 3 -1.4259 14.0203 1 -15 7 16 152.484 17.6875 -2 15 7 3 152.484 17.6875 1 -15 8 10 -3.3314 6.41570 -2 -15 8 3 -3.3314 6.41570 1 -14 8 9 137.705 10.3354 -2 -14 8 3 137.705 10.3354 1 -13 8 8 10.5229 16.2757 -2 -13 8 3 10.5229 16.2757 1 -12 8 8 345.920 32.1178 -2 -12 8 3 345.920 32.1178 1 -12 8 7 503.239 32.0015 -2 -12 8 3 503.239 32.0015 1 -11 8 7 0.03489 15.1763 -2 -11 8 3 0.03489 15.1763 1 -9 8 5 -7.2126 10.3537 -2 -9 8 3 -7.2126 10.3537 1 -8 8 4 34.7568 7.75816 -2 -8 8 3 34.7568 7.75816 1 -7 8 3 -17.323 8.16668 -2 -7 8 3 -17.323 8.16668 1 -6 8 2 233.419 10.9066 -2 -6 8 3 233.419 10.9066 1 -5 8 1 -8.8160 10.6287 -2 -5 8 3 -8.8160 10.6287 1 4 8 0 519.068 32.6556 -2 -4 8 3 519.068 32.6556 1 3 8 0 -16.746 17.7922 -2 -3 8 3 -16.746 17.7922 1 2 8 1 23.8558 7.76659 -2 -2 8 3 23.8558 7.76659 1 1 8 2 3.72462 15.4887 -2 -1 8 3 3.72462 15.4887 1 0 8 3 9.11242 5.69952 -2 0 8 3 9.11242 5.69952 1 -1 8 4 -10.785 10.8112 -2 1 8 3 -10.785 10.8112 1 -2 8 5 18.9958 16.2771 -2 2 8 3 18.9958 16.2771 1 -3 8 6 7.10216 14.5708 -2 3 8 3 7.10216 14.5708 1 -4 8 6 58.1272 17.9099 -2 4 8 3 58.1272 17.9099 1 -4 8 7 97.9910 30.4778 -2 4 8 3 97.9910 30.4778 1 -5 8 7 8.27872 19.7656 -2 5 8 3 8.27872 19.7656 1 -6 8 8 -10.656 10.9278 -2 6 8 3 -10.656 10.9278 1 -7 8 9 -20.605 9.82940 -2 7 8 3 -20.605 9.82940 1 -8 8 10 79.9044 21.3102 -2 8 8 3 79.9044 21.3102 1 -9 8 11 -25.267 14.3480 -2 9 8 3 -25.267 14.3480 1 -10 8 12 67.9583 11.2932 -2 10 8 3 67.9583 11.2932 1 -12 8 13 24.7671 27.2307 -2 12 8 3 24.7671 27.2307 1 -13 9 8 122.228 11.5089 -2 -13 9 3 122.228 11.5089 1 -12 9 8 12.0133 23.9355 -2 -12 9 3 12.0133 23.9355 1 -12 9 7 21.2232 15.6566 -2 -12 9 3 21.2232 15.6566 1 -11 9 7 9.34245 22.1446 -2 -11 9 3 9.34245 22.1446 1 -10 9 6 5.29087 11.1040 -2 -10 9 3 5.29087 11.1040 1 -9 9 5 89.7753 8.88682 -2 -9 9 3 89.7753 8.88682 1 -8 9 4 -9.4642 10.7328 -2 -8 9 3 -9.4642 10.7328 1 -7 9 3 130.784 20.3174 -2 -7 9 3 130.784 20.3174 1 -6 9 2 2.23899 14.1296 -2 -6 9 3 2.23899 14.1296 1 -5 9 1 408.473 16.0837 -2 -5 9 3 408.473 16.0837 1 3 9 0 78.4178 12.9384 -2 -3 9 3 78.4178 12.9384 1 2 9 1 -1.7290 11.7696 -2 -2 9 3 -1.7290 11.7696 1 1 9 2 34.3898 8.70353 -2 -1 9 3 34.3898 8.70353 1 0 9 3 1.62476 7.56248 -2 0 9 3 1.62476 7.56248 1 -1 9 4 105.939 9.88408 -2 1 9 3 105.939 9.88408 1 -2 9 5 -18.953 16.3554 -2 2 9 3 -18.953 16.3554 1 -3 9 6 22.9140 19.7501 -2 3 9 3 22.9140 19.7501 1 -5 9 7 126.730 26.3116 -2 5 9 3 126.730 26.3116 1 -6 9 8 -17.371 16.7965 -2 6 9 3 -17.371 16.7965 1 -7 9 9 -10.707 9.07911 -2 7 9 3 -10.707 9.07911 1 -8 9 10 6.93574 8.58323 -2 8 9 3 6.93574 8.58323 1 -9 9 11 109.896 10.0814 -2 9 9 3 109.896 10.0814 1 -10 9 12 -0.9482 20.0870 -2 10 9 3 -0.9482 20.0870 1 -11 9 13 128.693 21.5861 -2 11 9 3 128.693 21.5861 1 -11 10 7 3.87716 13.1039 -2 -11 10 3 3.87716 13.1039 1 -10 10 6 44.1509 9.04032 -2 -10 10 3 44.1509 9.04032 1 -9 10 5 -4.6562 8.67745 -2 -9 10 3 -4.6562 8.67745 1 -8 10 4 138.352 8.30505 -2 -8 10 3 138.352 8.30505 1 -7 10 3 -3.8842 7.90371 -2 -7 10 3 -3.8842 7.90371 1 -6 10 2 219.658 10.3537 -2 -6 10 3 219.658 10.3537 1 -5 10 1 -4.5263 13.0556 -2 -5 10 3 -4.5263 13.0556 1 4 10 0 82.7855 19.6425 -2 -4 10 3 82.7855 19.6425 1 -4 10 1 170.965 33.7747 -2 -4 10 3 170.965 33.7747 1 2 10 1 -19.353 18.7973 -2 -2 10 3 -19.353 18.7973 1 1 10 2 68.6246 15.4964 -2 -1 10 3 68.6246 15.4964 1 0 10 3 -0.0721 8.06948 -2 0 10 3 -0.0721 8.06948 1 -1 10 4 0.65706 12.2950 -2 1 10 3 0.65706 12.2950 1 -2 10 5 109.688 12.0702 -2 2 10 3 109.688 12.0702 1 -3 10 6 -15.640 22.5085 -2 3 10 3 -15.640 22.5085 1 -4 10 6 105.447 19.4271 -2 4 10 3 105.447 19.4271 1 -4 10 7 -6.8629 25.4191 -2 4 10 3 -6.8629 25.4191 1 -5 10 7 -4.4197 13.5118 -2 5 10 3 -4.4197 13.5118 1 -6 10 8 201.355 10.9760 -2 6 10 3 201.355 10.9760 1 -7 10 9 -5.6601 8.31114 -2 7 10 3 -5.6601 8.31114 1 -8 10 10 139.537 8.51482 -2 8 10 3 139.537 8.51482 1 -9 10 11 -5.3029 17.2605 -2 9 10 3 -5.3029 17.2605 1 -7 11 3 109.647 8.73364 -2 -7 11 3 109.647 8.73364 1 -6 11 2 13.4942 17.1122 -2 -6 11 3 13.4942 17.1122 1 -5 11 1 18.0931 21.1376 -2 -5 11 3 18.0931 21.1376 1 4 11 0 17.0946 24.8287 -2 -4 11 3 17.0946 24.8287 1 3 11 0 38.7908 13.0329 -2 -3 11 3 38.7908 13.0329 1 2 11 1 6.37988 12.0246 -2 -2 11 3 6.37988 12.0246 1 1 11 2 321.150 13.1582 -2 -1 11 3 321.150 13.1582 1 0 11 3 -2.2776 17.8467 -2 0 11 3 -2.2776 17.8467 1 -1 11 4 356.043 13.8242 -2 1 11 3 356.043 13.8242 1 -2 11 5 -21.513 16.6006 -2 2 11 3 -21.513 16.6006 1 -2 11 5 169.422 29.7947 -2 -2 11 4 169.422 29.7947 -2 2 11 3 169.422 29.7947 1 -3 11 6 278.452 21.3052 -2 3 11 3 278.452 21.3052 1 4 11 3 -10.059 10.1827 1 -5 11 7 49.1561 9.64147 -2 5 11 3 49.1561 9.64147 1 -21 0 4 -0.7684 8.10860 1 -17 0 11 -1.6408 23.2404 -2 -17 0 4 -1.6408 23.2404 1 -16 0 10 706.028 30.9348 -2 -16 0 4 706.028 30.9348 1 -15 0 9 -13.063 14.3040 -2 -15 0 4 -13.063 14.3040 1 -14 0 8 2010.20 59.6273 -2 -14 0 4 2010.20 59.6273 1 -13 0 7 -7.0156 18.1600 -2 -13 0 4 -7.0156 18.1600 1 -12 0 4 309.238 13.6184 1 -11 0 6 -9.5753 21.2824 -2 -11 0 4 -9.5753 21.2824 1 -10 0 5 353.666 13.7426 -2 -10 0 4 353.666 13.7426 1 -9 0 4 -1.5386 8.79572 -2 -9 0 4 -1.5386 8.79572 1 -8 0 3 546.524 14.9131 -2 -8 0 4 546.524 14.9131 1 -7 0 2 -1.7455 4.23808 -2 -7 0 4 -1.7455 4.23808 1 -6 0 1 472.909 12.9409 -2 -6 0 4 472.909 12.9409 1 5 0 0 -1.6380 5.61860 -2 -5 0 4 -1.6380 5.61860 1 -4 0 4 3303.12 86.2004 1 3 0 1 -3.8603 5.64800 -2 -3 0 4 -3.8603 5.64800 1 2 0 2 1660.82 84.5422 -2 -2 0 4 1660.82 84.5422 1 1 0 3 -0.5661 1.43543 -2 -1 0 4 -0.5661 1.43543 1 -2 0 6 512.772 22.6551 -2 2 0 4 512.772 22.6551 1 3 0 4 -0.0195 0.95419 1 4 0 4 253.024 6.78340 1 -5 0 8 14.3062 6.48828 -2 5 0 4 14.3062 6.48828 1 -6 0 9 1775.70 54.8717 -2 6 0 4 1775.70 54.8717 1 -7 0 10 -2.9679 3.67148 -2 7 0 4 -2.9679 3.67148 1 -8 0 11 2872.40 63.1797 -2 8 0 4 2872.40 63.1797 1 -9 0 12 2.72754 12.5325 -2 9 0 4 2.72754 12.5325 1 -10 0 13 747.551 31.5089 -2 10 0 4 747.551 31.5089 1 -11 0 14 -18.205 18.3923 -2 11 0 4 -18.205 18.3923 1 -12 0 14 431.316 25.0535 -2 12 0 4 431.316 25.0535 1 -13 0 15 13.3214 20.2440 -2 13 0 4 13.3214 20.2440 1 -14 0 16 1405.71 68.9206 -2 14 0 4 1405.71 68.9206 1 -16 0 18 190.247 25.8324 -2 16 0 4 190.247 25.8324 1 -17 0 19 27.5944 27.1191 -2 17 0 4 27.5944 27.1191 1 -21 1 14 195.243 20.8607 -2 -21 1 4 195.243 20.8607 1 -17 1 11 138.818 14.5197 -2 -17 1 4 138.818 14.5197 1 -16 1 10 -0.9896 10.9735 -2 -16 1 4 -0.9896 10.9735 1 -15 1 9 612.028 15.8934 -2 -15 1 4 612.028 15.8934 1 -14 1 8 1.26240 14.2783 -2 -14 1 4 1.26240 14.2783 1 -13 1 7 425.155 17.7896 -2 -13 1 4 425.155 17.7896 1 -12 1 6 -9.9904 19.7335 -2 -12 1 4 -9.9904 19.7335 1 -11 1 6 573.289 12.4295 -2 -11 1 4 573.289 12.4295 1 -10 1 5 -0.8734 6.95439 -2 -10 1 4 -0.8734 6.95439 1 -9 1 4 422.239 12.7956 -2 -9 1 4 422.239 12.7956 1 -8 1 3 0.29630 1.87947 -2 -8 1 4 0.29630 1.87947 1 -7 1 2 989.359 18.6170 -2 -7 1 4 989.359 18.6170 1 -6 1 1 4.39026 4.55203 -2 -6 1 4 4.39026 4.55203 1 5 1 0 1765.52 38.9863 -2 -5 1 4 1765.52 38.9863 1 -4 1 4 0.38293 0.97132 1 3 1 1 2478.87 54.3463 -2 -3 1 4 2478.87 54.3463 1 2 1 2 -0.7707 2.29319 -2 -2 1 4 -0.7707 2.29319 1 1 1 3 2252.39 46.2716 -2 -1 1 4 2252.39 46.2716 1 0 1 4 2.63658 1.06437 -2 0 1 4 2.63658 1.06437 1 -1 1 5 2255.56 50.7802 -2 1 1 4 2255.56 50.7802 1 -2 1 6 0.36396 2.14986 -2 2 1 4 0.36396 2.14986 1 3 1 4 196.995 4.76271 1 4 1 4 0.69224 0.86661 1 -5 1 8 1958.28 84.7301 -2 5 1 4 1958.28 84.7301 1 -6 1 9 -2.4809 4.76248 -2 6 1 4 -2.4809 4.76248 1 -7 1 10 1315.71 22.3894 -2 7 1 4 1315.71 22.3894 1 -8 1 11 2.93448 4.09814 -2 8 1 4 2.93448 4.09814 1 -9 1 12 352.488 13.5226 -2 9 1 4 352.488 13.5226 1 -10 1 13 -1.5294 9.92439 -2 10 1 4 -1.5294 9.92439 1 -11 1 14 570.529 19.9303 -2 11 1 4 570.529 19.9303 1 -12 1 14 -23.934 39.8730 -2 12 1 4 -23.934 39.8730 1 -13 1 15 1369.56 44.0152 -2 13 1 4 1369.56 44.0152 1 -14 1 16 39.9944 18.6864 -2 14 1 4 39.9944 18.6864 1 -16 1 18 6.56189 15.8014 -2 16 1 4 6.56189 15.8014 1 -17 1 19 284.603 22.2383 -2 17 1 4 284.603 22.2383 1 -21 2 15 8.06720 19.3280 -2 -21 2 4 8.06720 19.3280 1 -21 2 14 23.4877 15.6933 -2 -21 2 4 23.4877 15.6933 1 -18 2 12 300.899 20.1825 -2 -18 2 4 300.899 20.1825 1 -17 2 11 3.53318 15.8501 -2 -17 2 4 3.53318 15.8501 1 -16 2 10 118.261 10.1495 -2 -16 2 4 118.261 10.1495 1 -15 2 9 -0.6249 10.2123 -2 -15 2 4 -0.6249 10.2123 1 -14 2 8 826.026 25.0145 -2 -14 2 4 826.026 25.0145 1 -13 2 7 32.6212 17.7932 -2 -13 2 4 32.6212 17.7932 1 -12 2 6 537.916 28.5381 -2 -12 2 4 537.916 28.5381 1 -11 2 6 2.51994 9.52455 -2 -11 2 4 2.51994 9.52455 1 -10 2 5 36.4829 6.53262 -2 -10 2 4 36.4829 6.53262 1 -9 2 4 5.63266 5.45247 -2 -9 2 4 5.63266 5.45247 1 -8 2 3 764.534 13.5693 -2 -8 2 4 764.534 13.5693 1 -7 2 2 -4.9520 3.47591 -2 -7 2 4 -4.9520 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11.1393 1 10 6 12 158.806 11.6123 -2 -10 6 21 158.806 11.6123 1 9 6 13 32.7062 7.89183 -2 -9 6 21 32.7062 7.89183 1 8 6 14 113.346 25.2379 -2 -8 6 21 113.346 25.2379 1 7 6 15 2.36655 11.5070 -2 -7 6 21 2.36655 11.5070 1 6 6 16 44.5776 14.0848 -2 -6 6 21 44.5776 14.0848 1 -5 6 21 0.57838 3.33444 1 15 0 9 -7.9747 17.4520 -2 -15 0 22 -7.9747 17.4520 1 14 0 10 241.068 15.5063 -2 -14 0 22 241.068 15.5063 1 13 0 11 -27.921 14.6518 -2 -13 0 22 -27.921 14.6518 1 -12 0 22 100.695 10.3793 1 -11 0 22 -0.0814 6.73648 1 10 0 13 334.838 23.2646 -2 -10 0 22 334.838 23.2646 1 9 0 14 -19.830 14.0379 -2 -9 0 22 -19.830 14.0379 1 8 0 15 0.19282 12.2087 -2 -8 0 22 0.19282 12.2087 1 7 0 16 -12.083 14.2292 -2 -7 0 22 -12.083 14.2292 1 6 0 17 163.969 19.4765 -2 -6 0 22 163.969 19.4765 1 -5 0 22 -8.9802 6.01691 1 -4 0 22 172.840 11.4002 1 -3 0 22 2.10345 5.47395 1 2 0 20 1013.23 45.4120 -2 -2 0 22 1013.23 45.4120 1 0 0 22 167.774 13.5278 -2 0 0 22 167.774 13.5278 1 15 1 9 91.5832 12.3983 -2 -15 1 22 91.5832 12.3983 1 14 1 10 -8.4382 8.93394 -2 -14 1 22 -8.4382 8.93394 1 13 1 11 121.804 31.6944 -2 -13 1 22 121.804 31.6944 1 -12 1 22 -2.6991 4.05825 1 -11 1 22 461.564 13.2735 1 10 1 13 -6.8992 10.2641 -2 -10 1 22 -6.8992 10.2641 1 9 1 14 216.579 10.9140 -2 -9 1 22 216.579 10.9140 1 8 1 15 -0.7560 7.93665 -2 -8 1 22 -0.7560 7.93665 1 7 1 16 67.1128 8.98814 -2 -7 1 22 67.1128 8.98814 1 6 1 17 12.6638 9.95626 -2 -6 1 22 12.6638 9.95626 1 -5 1 22 242.356 9.92101 1 -4 1 22 -1.6695 4.15142 1 -3 1 22 10.2445 4.23906 1 2 1 20 -8.1694 11.0039 -2 -2 1 22 -8.1694 11.0039 1 1 1 21 113.510 9.04578 -2 -1 1 22 113.510 9.04578 1 0 1 22 0.16655 10.3546 -2 0 1 22 0.16655 10.3546 1 -1 1 23 19.9591 10.4571 -2 1 1 22 19.9591 10.4571 1 16 2 8 245.409 12.6381 -2 -16 2 22 245.409 12.6381 1 14 2 10 406.749 15.0793 -2 -14 2 22 406.749 15.0793 1 13 2 11 44.0877 30.5963 -2 -13 2 22 44.0877 30.5963 1 -12 2 22 176.579 7.65419 1 11 2 12 10.7871 37.0058 -2 -11 2 22 10.7871 37.0058 1 10 2 13 1.40992 9.92818 -2 -10 2 22 1.40992 9.92818 1 9 2 14 -17.816 14.3208 -2 -9 2 22 -17.816 14.3208 1 8 2 15 45.5448 8.02689 -2 -8 2 22 45.5448 8.02689 1 7 2 16 -1.1723 10.4353 -2 -7 2 22 -1.1723 10.4353 1 6 2 17 281.029 12.8433 -2 -6 2 22 281.029 12.8433 1 -5 2 22 1.54853 4.16233 1 -4 2 22 251.962 9.76428 1 -3 2 22 -2.5336 4.14558 1 2 2 20 547.208 20.0869 -2 -2 2 22 547.208 20.0869 1 1 2 21 -1.6467 8.09174 -2 -1 2 22 -1.6467 8.09174 1 0 2 22 16.8740 6.27771 -2 0 2 22 16.8740 6.27771 1 1 2 22 8.33901 4.53389 1 15 3 9 285.322 24.0972 -2 -15 3 22 285.322 24.0972 1 14 3 10 6.78573 16.3333 -2 -14 3 22 6.78573 16.3333 1 13 3 11 -6.6250 14.2047 -2 -13 3 22 -6.6250 14.2047 1 -12 3 22 -3.9895 3.60186 1 -11 3 22 138.010 7.47191 1 10 3 13 14.6357 9.72530 -2 -10 3 22 14.6357 9.72530 1 9 3 14 116.059 9.25796 -2 -9 3 22 116.059 9.25796 1 8 3 15 2.28719 6.97225 -2 -8 3 22 2.28719 6.97225 1 7 3 16 72.5738 8.50169 -2 -7 3 22 72.5738 8.50169 1 6 3 17 16.6159 17.7518 -2 -6 3 22 16.6159 17.7518 1 -5 3 22 6.41180 4.00841 1 -4 3 22 -1.2370 4.92298 1 -3 3 22 205.446 8.65691 1 2 3 20 -5.3831 10.7248 -2 -2 3 22 -5.3831 10.7248 1 1 3 21 71.9716 9.51539 -2 -1 3 22 71.9716 9.51539 1 -14 4 22 35.3937 6.87293 1 -13 4 22 2.76599 7.25620 1 -12 4 22 48.2211 4.27630 1 -11 4 22 4.39585 3.69561 1 10 4 13 165.722 10.4397 -2 -10 4 22 165.722 10.4397 1 9 4 14 10.3463 7.92758 -2 -9 4 22 10.3463 7.92758 1 8 4 15 276.879 10.1087 -2 -8 4 22 276.879 10.1087 1 7 4 16 11.7747 7.35808 -2 -7 4 22 11.7747 7.35808 1 6 4 17 141.629 9.59288 -2 -6 4 22 141.629 9.59288 1 -5 4 22 -2.0762 3.77130 1 -4 4 22 32.1865 4.07523 1 -3 4 22 -4.3725 3.85123 1 2 4 20 29.4756 13.3309 -2 -2 4 22 29.4756 13.3309 1 -11 5 22 19.3334 3.74213 1 10 5 13 30.7929 9.52433 -2 -10 5 22 30.7929 9.52433 1 9 5 14 8.19608 8.59991 -2 -9 5 22 8.19608 8.59991 1 8 5 15 6.59392 6.98748 -2 -8 5 22 6.59392 6.98748 1 7 5 16 7.38910 7.61708 -2 -7 5 22 7.38910 7.61708 1 6 5 17 21.2302 9.11531 -2 -6 5 22 21.2302 9.11531 1 -5 5 22 6.27731 3.48162 1 -4 5 22 1.65889 3.20784 1 15 0 10 11.2618 11.8157 -2 -15 0 23 11.2618 11.8157 1 14 0 11 -5.6970 28.2669 -2 -14 0 23 -5.6970 28.2669 1 13 0 12 -11.656 14.7161 -2 -13 0 23 -11.656 14.7161 1 -12 0 23 1.43190 6.44713 1 -11 0 23 -7.8138 6.68137 1 10 0 14 338.726 21.4644 -2 -10 0 23 338.726 21.4644 1 9 0 15 1.76488 13.8160 -2 -9 0 23 1.76488 13.8160 1 8 0 16 44.2950 11.9263 -2 -8 0 23 44.2950 11.9263 1 7 0 17 -3.5989 12.9721 -2 -7 0 23 -3.5989 12.9721 1 6 0 18 12.3903 15.2372 -2 -6 0 23 12.3903 15.2372 1 -5 0 23 1.63256 6.40913 1 -4 0 23 -5.9940 6.46459 1 -3 0 23 5.03502 5.76340 1 2 0 21 1.12682 13.8838 -2 -2 0 23 1.12682 13.8838 1 15 1 10 43.0516 9.30258 -2 -15 1 23 43.0516 9.30258 1 14 1 11 26.8027 13.8919 -2 -14 1 23 26.8027 13.8919 1 -13 1 23 0.08993 4.20800 1 -12 1 23 -1.3925 4.23674 1 -11 1 23 33.4200 5.25204 1 10 1 14 -13.699 10.8965 -2 -10 1 23 -13.699 10.8965 1 9 1 15 100.937 9.40725 -2 -9 1 23 100.937 9.40725 1 8 1 16 -2.7206 7.09495 -2 -8 1 23 -2.7206 7.09495 1 7 1 17 3.67714 8.04437 -2 -7 1 23 3.67714 8.04437 1 6 1 18 -6.1942 9.49121 -2 -6 1 23 -6.1942 9.49121 1 -5 1 23 4.64243 3.92540 1 -4 1 23 -4.8960 3.71348 1 -3 1 23 -0.4901 3.94932 1 2 1 21 -5.5353 14.4051 -2 -2 1 23 -5.5353 14.4051 1 1 1 22 24.5608 19.1890 -2 -1 1 23 24.5608 19.1890 1 14 2 11 -3.7508 14.7751 -2 -14 2 23 -3.7508 14.7751 1 13 2 12 21.8447 34.5963 -2 -13 2 23 21.8447 34.5963 1 -12 2 23 8.20733 3.76918 1 -11 2 23 -3.2332 3.81061 1 10 2 14 249.491 13.8317 -2 -10 2 23 249.491 13.8317 1 9 2 15 22.6296 10.6800 -2 -9 2 23 22.6296 10.6800 1 8 2 16 35.8624 7.03407 -2 -8 2 23 35.8624 7.03407 1 7 2 17 -10.094 7.46696 -2 -7 2 23 -10.094 7.46696 1 6 2 18 12.5097 8.75217 -2 -6 2 23 12.5097 8.75217 1 -5 2 23 3.61948 3.77978 1 -4 2 23 33.6903 4.15907 1 -3 2 23 -2.7273 4.39933 1 2 2 21 25.8419 13.4411 -2 -2 2 23 25.8419 13.4411 1 -13 3 23 198.919 8.33322 1 -12 3 23 -2.4692 3.56043 1 -11 3 23 33.8856 3.90472 1 10 3 14 -12.510 9.80570 -2 -10 3 23 -12.510 9.80570 1 9 3 15 108.440 8.41200 -2 -9 3 23 108.440 8.41200 1 8 3 16 -3.2721 6.28165 -2 -8 3 23 -3.2721 6.28165 1 7 3 17 101.530 7.61223 -2 -7 3 23 101.530 7.61223 1 6 3 18 20.8260 8.11311 -2 -6 3 23 20.8260 8.11311 1 -5 3 23 26.2390 3.91346 1 -4 3 23 -0.4418 4.36844 1 -3 3 23 201.635 8.63536 1 -11 4 23 -2.1423 5.11623 1 10 4 14 350.701 20.2487 -2 -10 4 23 350.701 20.2487 1 9 4 15 18.2806 8.69627 -2 -9 4 23 18.2806 8.69627 1 8 4 16 108.334 6.69929 -2 -8 4 23 108.334 6.69929 1 7 4 17 9.92601 6.36787 -2 -7 4 23 9.92601 6.36787 1 -6 4 23 11.9214 3.43157 1 -5 4 23 -0.2551 3.11512 1 -13 0 24 1.56267 5.40505 1 -12 0 24 411.011 20.2596 1 -11 0 24 -2.1485 5.58970 1 10 0 15 30.1611 13.7676 -2 -10 0 24 30.1611 13.7676 1 9 0 16 10.6975 11.9446 -2 -9 0 24 10.6975 11.9446 1 8 0 17 22.7182 10.3649 -2 -8 0 24 22.7182 10.3649 1 7 0 18 -13.803 11.5508 -2 -7 0 24 -13.803 11.5508 1 6 0 19 65.8623 14.4955 -2 -6 0 24 65.8623 14.4955 1 -5 0 24 6.61828 5.76354 1 -4 0 24 26.6960 5.77222 1 -13 1 24 166.204 8.60629 1 -12 1 24 -0.8960 4.17982 1 -11 1 24 77.6593 7.50065 1 10 1 15 -17.575 9.65873 -2 -10 1 24 -17.575 9.65873 1 9 1 16 197.543 10.9579 -2 -9 1 24 197.543 10.9579 1 8 1 17 -6.0006 7.20685 -2 -8 1 24 -6.0006 7.20685 1 7 1 18 19.3091 8.21188 -2 -7 1 24 19.3091 8.21188 1 6 1 19 12.6596 9.29588 -2 -6 1 24 12.6596 9.29588 1 -5 1 24 112.958 7.84458 1 -4 1 24 4.46606 3.93771 1 -12 2 24 80.2555 5.85455 1 -11 2 24 8.25154 4.61763 1 10 2 15 102.880 10.1706 -2 -10 2 24 102.880 10.1706 1 9 2 16 3.69187 8.17916 -2 -9 2 24 3.69187 8.17916 1 8 2 17 25.1424 6.27224 -2 -8 2 24 25.1424 6.27224 1 7 2 18 3.03129 6.91117 -2 -7 2 24 3.03129 6.91117 1 6 2 19 232.714 16.9215 -2 -6 2 24 232.714 16.9215 1 -5 2 24 -0.4067 3.56821 1 8 3 17 -12.611 11.4322 -2 -8 3 24 -12.611 11.4322 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 41288 #===END data_twin5 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C38 H28 F2 Fe N8' _chemical_formula_weight 690.53 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.783(3) _cell_length_b 11.110(4) _cell_length_c 17.438(5) _cell_angle_alpha 87.54(2) _cell_angle_beta 83.79(2) _cell_angle_gamma 71.55(2) _cell_volume 1604.6(9) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9252 _cell_measurement_theta_min 3.026 _cell_measurement_theta_max 27.104 _exptl_crystal_description 'block' _exptl_crystal_colour 'dark red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.429 _exptl_crystal_F_000 712 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.160 _exptl_crystal_size_min 0.150 _exptl_absorpt_coefficient_mu 0.524 _shelx_estimated_absorpt_T_min 0.902 _shelx_estimated_absorpt_T_max 0.926 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.688857 _exptl_absorpt_correction_T_max 0.745491 _exptl_absorpt_process_details 'TWINABS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 13912 _diffrn_reflns_av_unetI/netI 0.0178 _diffrn_reflns_av_R_equivalents ? _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_theta_min 3.029 _diffrn_reflns_theta_max 27.232 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 13912 _reflns_number_gt 12051 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refined as a 2-component twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0395P)^2^+1.1355P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 13912 _refine_ls_number_parameters 443 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0507 _refine_ls_R_factor_gt 0.0394 _refine_ls_wR_factor_ref 0.1070 _refine_ls_wR_factor_gt 0.0974 _refine_ls_goodness_of_fit_ref 1.086 _refine_ls_restrained_S_all 1.086 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.60987(4) 0.26318(3) 0.25428(2) 0.01901(9) Uani 1 1 d . . . . . F1 F 1.04693(18) -0.56171(12) 0.24164(9) 0.0320(3) Uani 1 1 d . . . . . C1 C 0.4930(3) 0.17635(19) 0.13245(12) 0.0182(4) Uani 1 1 d . . . . . N1 N 0.5941(2) 0.13841(16) 0.19473(10) 0.0185(3) Uani 1 1 d . . . . . C2 C 0.5452(3) 0.1239(2) 0.05980(12) 0.0214(4) Uani 1 1 d . . . . . H2 H 0.6433 0.0598 0.0513 0.026 Uiso 1 1 calc R U . . . N2 N 0.6577(2) 0.01427(16) 0.19893(10) 0.0186(3) Uani 1 1 d . . . . . F2 F 0.1878(2) 1.09034(13) 0.25389(11) 0.0505(5) Uani 1 1 d . . . . . N3 N 0.8132(2) 0.02405(16) 0.30452(10) 0.0191(4) Uani 1 1 d . . . . . C3 C 0.4490(3) 0.1684(2) 0.00001(13) 0.0246(5) Uani 1 1 d . . . . . H3 H 0.4833 0.1340 -0.0489 0.030 Uiso 1 1 calc R U . . . N4 N 0.7503(2) 0.14840(16) 0.31132(10) 0.0182(3) Uani 1 1 d . . . . . C4 C 0.3033(3) 0.2628(2) 0.01234(13) 0.0259(5) Uani 1 1 d . . . . . H4 H 0.2404 0.2928 -0.0283 0.031 Uiso 1 1 calc R U . . . N7 N 0.4180(2) 0.50294(16) 0.31790(10) 0.0192(4) Uani 1 1 d . . . . . C7 C 0.7631(3) -0.03513(19) 0.25143(12) 0.0188(4) Uani 1 1 d . . . . . N6 N 0.5595(2) 0.51305(16) 0.19136(10) 0.0197(4) Uani 1 1 d . . . . . C6 C 0.3457(3) 0.2706(2) 0.14577(12) 0.0224(4) Uani 1 1 d . . . . . H6 H 0.3108 0.3048 0.1947 0.027 Uiso 1 1 calc R U . . . N5 N 0.6228(2) 0.38807(16) 0.18518(10) 0.0191(4) Uani 1 1 d . . . . . C5 C 0.2506(3) 0.3133(2) 0.08545(13) 0.0263(5) Uani 1 1 d . . . . . H5 H 0.1513 0.3759 0.0941 0.032 Uiso 1 1 calc R U . . . N8 N 0.4791(2) 0.37788(16) 0.32372(10) 0.0187(3) Uani 1 1 d . . . . . C8 C 0.8360(3) -0.17468(19) 0.24951(12) 0.0182(4) Uani 1 1 d . . . . . C9 C 0.7842(3) -0.2486(2) 0.20176(13) 0.0237(4) Uani 1 1 d . . . . . H9 H 0.7005 -0.2096 0.1717 0.028 Uiso 1 1 calc R U . . . C10 C 0.8552(3) -0.3785(2) 0.19848(14) 0.0264(5) Uani 1 1 d . . . . . H10 H 0.8215 -0.4273 0.1660 0.032 Uiso 1 1 calc R U . . . C11 C 0.9769(3) -0.43404(19) 0.24432(14) 0.0235(4) Uani 1 1 d . . . . . C12 C 1.0315(3) -0.3656(2) 0.29271(14) 0.0269(5) Uani 1 1 d . . . . . H12 H 1.1137 -0.4060 0.3233 0.032 Uiso 1 1 calc R U . . . C13 C 0.9612(3) -0.2356(2) 0.29466(13) 0.0246(4) Uani 1 1 d . . . . . H13 H 0.9977 -0.1877 0.3265 0.030 Uiso 1 1 calc R U . . . C14 C 0.8175(3) 0.19506(19) 0.37093(12) 0.0196(4) Uani 1 1 d . . . . . C16 C 0.9035(3) 0.1794(2) 0.49772(14) 0.0303(5) Uani 1 1 d . . . . . H16 H 0.9191 0.1370 0.5448 0.036 Uiso 1 1 calc R U . . . C15 C 0.8418(3) 0.1305(2) 0.44090(13) 0.0244(4) Uani 1 1 d . . . . . H15 H 0.8170 0.0553 0.4495 0.029 Uiso 1 1 calc R U . . . C17 C 0.9421(3) 0.2904(2) 0.48540(14) 0.0300(5) Uani 1 1 d . . . . . H17 H 0.9830 0.3225 0.5241 0.036 Uiso 1 1 calc R U . . . C19 C 0.8568(3) 0.3059(2) 0.35825(13) 0.0266(5) Uani 1 1 d . . . . . H19 H 0.8409 0.3487 0.3113 0.032 Uiso 1 1 calc R U . . . C18 C 0.9198(3) 0.3537(2) 0.41534(15) 0.0309(5) Uani 1 1 d . . . . . H18 H 0.9469 0.4279 0.4065 0.037 Uiso 1 1 calc R U . . . C20 C 0.7206(3) 0.3516(2) 0.11353(12) 0.0207(4) Uani 1 1 d . . . . . C21 C 0.6797(3) 0.4204(2) 0.04604(13) 0.0247(4) Uani 1 1 d . . . . . H21 H 0.5944 0.4959 0.0478 0.030 Uiso 1 1 calc R U . . . C22 C 0.7667(3) 0.3761(2) -0.02352(14) 0.0316(5) Uani 1 1 d . . . . . H22 H 0.7389 0.4218 -0.0686 0.038 Uiso 1 1 calc R U . . . C23 C 0.8944(3) 0.2648(2) -0.02679(14) 0.0329(5) Uani 1 1 d . . . . . H23 H 0.9504 0.2345 -0.0740 0.039 Uiso 1 1 calc R U . . . C24 C 0.9390(3) 0.1983(2) 0.04078(15) 0.0314(5) Uani 1 1 d . . . . . H24 H 1.0263 0.1242 0.0388 0.038 Uiso 1 1 calc R U . . . C25 C 0.8540(3) 0.2420(2) 0.11102(14) 0.0251(4) Uani 1 1 d . . . . . H25 H 0.8857 0.1985 0.1563 0.030 Uiso 1 1 calc R U . . . C26 C 0.4624(3) 0.56131(19) 0.25462(13) 0.0202(4) Uani 1 1 d . . . . . C27 C 0.3922(3) 0.70158(19) 0.25453(13) 0.0211(4) Uani 1 1 d . . . . . C28 C 0.3581(3) 0.7689(2) 0.18549(13) 0.0268(5) Uani 1 1 d . . . . . H28 H 0.3826 0.7251 0.1392 0.032 Uiso 1 1 calc R U . . . C29 C 0.2888(3) 0.8993(2) 0.18488(15) 0.0342(6) Uani 1 1 d . . . . . H29 H 0.2649 0.9432 0.1388 0.041 Uiso 1 1 calc R U . . . C30 C 0.2559(3) 0.9627(2) 0.25367(17) 0.0339(6) Uani 1 1 d . . . . . C31 C 0.2904(3) 0.9007(2) 0.32279(15) 0.0335(6) Uani 1 1 d . . . . . H31 H 0.2695 0.9458 0.3685 0.040 Uiso 1 1 calc R U . . . C32 C 0.3571(3) 0.7695(2) 0.32289(14) 0.0271(5) Uani 1 1 d . . . . . H32 H 0.3787 0.7263 0.3694 0.033 Uiso 1 1 calc R U . . . C33 C 0.4243(2) 0.32945(19) 0.39546(12) 0.0198(4) Uani 1 1 d . . . . . C34 C 0.4068(3) 0.2087(2) 0.39789(13) 0.0235(4) Uani 1 1 d . . . . . H34 H 0.4195 0.1641 0.3525 0.028 Uiso 1 1 calc R U . . . C35 C 0.3705(3) 0.1553(2) 0.46808(14) 0.0286(5) Uani 1 1 d . . . . . H35 H 0.3612 0.0741 0.4697 0.034 Uiso 1 1 calc R U . . . C36 C 0.3479(3) 0.2226(2) 0.53578(14) 0.0315(5) Uani 1 1 d . . . . . H36 H 0.3257 0.1862 0.5830 0.038 Uiso 1 1 calc R U . . . C37 C 0.3588(3) 0.3442(2) 0.53263(14) 0.0310(5) Uani 1 1 d . . . . . H37 H 0.3412 0.3902 0.5779 0.037 Uiso 1 1 calc R U . . . C38 C 0.3956(3) 0.3987(2) 0.46300(13) 0.0250(5) Uani 1 1 d . . . . . H38 H 0.4010 0.4810 0.4615 0.030 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.02275(16) 0.01810(15) 0.01496(15) 0.00065(10) -0.00454(11) -0.00395(11) F1 0.0324(8) 0.0207(6) 0.0385(8) -0.0026(5) 0.0001(6) -0.0032(5) C1 0.0194(10) 0.0215(10) 0.0160(10) 0.0033(7) -0.0045(8) -0.0092(8) N1 0.0178(8) 0.0223(9) 0.0144(8) 0.0018(6) -0.0018(7) -0.0050(7) C2 0.0239(11) 0.0229(10) 0.0182(10) 0.0005(7) -0.0029(8) -0.0085(8) N2 0.0178(8) 0.0214(9) 0.0159(9) 0.0011(6) -0.0006(7) -0.0057(7) F2 0.0709(12) 0.0157(7) 0.0536(10) 0.0011(6) 0.0180(9) -0.0058(7) N3 0.0184(8) 0.0215(9) 0.0165(9) 0.0002(6) -0.0010(7) -0.0051(7) C3 0.0338(13) 0.0283(11) 0.0145(10) 0.0004(8) -0.0026(9) -0.0136(9) N4 0.0202(9) 0.0204(9) 0.0141(8) -0.0002(6) -0.0010(7) -0.0065(7) C4 0.0301(12) 0.0313(12) 0.0198(11) 0.0060(8) -0.0105(9) -0.0125(9) N7 0.0194(8) 0.0197(9) 0.0184(9) 0.0008(6) -0.0051(7) -0.0049(7) C7 0.0172(9) 0.0240(10) 0.0156(9) 0.0005(7) -0.0012(7) -0.0073(8) N6 0.0201(9) 0.0195(9) 0.0208(9) 0.0015(6) -0.0057(7) -0.0068(7) C6 0.0225(10) 0.0252(11) 0.0187(10) -0.0005(8) -0.0024(8) -0.0065(8) N5 0.0184(8) 0.0226(9) 0.0171(9) 0.0004(6) -0.0053(7) -0.0063(7) C5 0.0232(11) 0.0281(11) 0.0265(12) 0.0024(8) -0.0077(9) -0.0053(9) N8 0.0215(9) 0.0199(9) 0.0159(9) 0.0016(6) -0.0061(7) -0.0071(7) C8 0.0151(9) 0.0226(10) 0.0160(9) -0.0002(7) 0.0013(7) -0.0055(7) C9 0.0240(11) 0.0256(11) 0.0234(11) 0.0012(8) -0.0075(9) -0.0089(9) C10 0.0286(12) 0.0262(12) 0.0272(12) -0.0026(8) -0.0038(9) -0.0120(9) C11 0.0217(10) 0.0180(10) 0.0269(11) -0.0017(8) 0.0046(8) -0.0030(8) C12 0.0224(11) 0.0271(12) 0.0273(12) 0.0006(8) -0.0043(9) -0.0021(9) C13 0.0227(11) 0.0265(11) 0.0232(11) -0.0034(8) -0.0045(9) -0.0046(9) C14 0.0180(10) 0.0219(10) 0.0164(10) -0.0021(7) -0.0029(8) -0.0023(8) C16 0.0350(13) 0.0375(13) 0.0164(11) 0.0009(8) -0.0077(9) -0.0069(10) C15 0.0295(12) 0.0239(11) 0.0197(11) 0.0012(8) -0.0047(9) -0.0077(9) C17 0.0303(12) 0.0348(13) 0.0243(12) -0.0087(9) -0.0104(10) -0.0057(10) C19 0.0306(12) 0.0277(12) 0.0236(11) 0.0035(8) -0.0093(9) -0.0107(9) C18 0.0352(13) 0.0280(12) 0.0331(13) -0.0013(9) -0.0107(10) -0.0126(10) C20 0.0212(10) 0.0248(11) 0.0192(10) -0.0013(7) -0.0018(8) -0.0116(8) C21 0.0297(12) 0.0252(11) 0.0212(11) 0.0006(8) -0.0036(9) -0.0112(9) C22 0.0405(14) 0.0356(13) 0.0222(12) 0.0013(9) -0.0014(10) -0.0177(11) C23 0.0317(13) 0.0444(15) 0.0256(12) -0.0068(10) 0.0081(10) -0.0189(11) C24 0.0250(12) 0.0341(13) 0.0339(13) -0.0048(9) 0.0038(10) -0.0091(10) C25 0.0218(11) 0.0275(11) 0.0265(12) 0.0013(8) -0.0035(9) -0.0085(9) C26 0.0196(10) 0.0237(10) 0.0182(10) 0.0003(7) -0.0046(8) -0.0073(8) C27 0.0207(10) 0.0234(10) 0.0201(10) 0.0007(8) -0.0005(8) -0.0088(8) C28 0.0306(12) 0.0255(11) 0.0218(11) 0.0016(8) 0.0013(9) -0.0068(9) C29 0.0411(15) 0.0251(12) 0.0298(13) 0.0076(9) 0.0063(11) -0.0053(10) C30 0.0390(14) 0.0150(10) 0.0430(15) 0.0006(9) 0.0096(11) -0.0063(9) C31 0.0443(15) 0.0261(12) 0.0320(14) -0.0076(9) 0.0017(11) -0.0145(10) C32 0.0349(13) 0.0264(12) 0.0229(11) -0.0005(8) -0.0049(10) -0.0128(9) C33 0.0177(10) 0.0220(10) 0.0168(10) 0.0025(7) -0.0045(8) -0.0017(8) C34 0.0233(11) 0.0234(11) 0.0219(11) -0.0002(8) -0.0020(9) -0.0049(8) C35 0.0278(12) 0.0278(12) 0.0290(13) 0.0072(9) -0.0019(10) -0.0083(9) C36 0.0285(12) 0.0421(14) 0.0204(11) 0.0092(9) -0.0004(9) -0.0078(10) C37 0.0328(13) 0.0391(14) 0.0181(11) -0.0015(9) -0.0025(9) -0.0069(10) C38 0.0281(11) 0.0238(11) 0.0210(11) -0.0007(8) -0.0051(9) -0.0043(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.8154(19) . ? Fe1 N4 1.8159(19) . ? Fe1 N8 1.8205(19) . ? Fe1 N5 1.8211(19) . ? F1 C11 1.356(2) . ? C1 C6 1.387(3) . ? C1 C2 1.387(3) . ? C1 N1 1.441(3) . ? N1 N2 1.316(2) . ? C2 C3 1.388(3) . ? C2 H2 0.9300 . ? N2 C7 1.347(3) . ? F2 C30 1.354(3) . ? N3 N4 1.321(2) . ? N3 C7 1.344(3) . ? C3 C4 1.376(3) . ? C3 H3 0.9300 . ? N4 C14 1.439(3) . ? C4 C5 1.387(3) . ? C4 H4 0.9300 . ? N7 N8 1.325(2) . ? N7 C26 1.340(3) . ? C7 C8 1.479(3) . ? N6 N5 1.327(2) . ? N6 C26 1.338(3) . ? C6 C5 1.387(3) . ? C6 H6 0.9300 . ? N5 C20 1.433(3) . ? C5 H5 0.9300 . ? N8 C33 1.436(3) . ? C8 C9 1.397(3) . ? C8 C13 1.399(3) . ? C9 C10 1.380(3) . ? C9 H9 0.9300 . ? C10 C11 1.374(3) . ? C10 H10 0.9300 . ? C11 C12 1.376(3) . ? C12 C13 1.380(3) . ? C12 H12 0.9300 . ? C13 H13 0.9300 . ? C14 C19 1.384(3) . ? C14 C15 1.390(3) . ? C16 C17 1.381(4) . ? C16 C15 1.385(3) . ? C16 H16 0.9300 . ? C15 H15 0.9300 . ? C17 C18 1.384(3) . ? C17 H17 0.9300 . ? C19 C18 1.389(3) . ? C19 H19 0.9300 . ? C18 H18 0.9300 . ? C20 C21 1.393(3) . ? C20 C25 1.396(3) . ? C21 C22 1.382(3) . ? C21 H21 0.9300 . ? C22 C23 1.380(4) . ? C22 H22 0.9300 . ? C23 C24 1.389(4) . ? C23 H23 0.9300 . ? C24 C25 1.384(3) . ? C24 H24 0.9300 . ? C25 H25 0.9300 . ? C26 C27 1.483(3) . ? C27 C32 1.391(3) . ? C27 C28 1.399(3) . ? C28 C29 1.382(3) . ? C28 H28 0.9300 . ? C29 C30 1.374(4) . ? C29 H29 0.9300 . ? C30 C31 1.376(4) . ? C31 C32 1.389(3) . ? C31 H31 0.9300 . ? C32 H32 0.9300 . ? C33 C38 1.390(3) . ? C33 C34 1.396(3) . ? C34 C35 1.387(3) . ? C34 H34 0.9300 . ? C35 C36 1.387(4) . ? C35 H35 0.9300 . ? C36 C37 1.383(4) . ? C36 H36 0.9300 . ? C37 C38 1.386(3) . ? C37 H37 0.9300 . ? C38 H38 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N4 91.34(8) . . ? N1 Fe1 N8 137.45(8) . . ? N4 Fe1 N8 104.90(8) . . ? N1 Fe1 N5 103.70(8) . . ? N4 Fe1 N5 135.40(8) . . ? N8 Fe1 N5 91.89(8) . . ? C6 C1 C2 120.68(19) . . ? C6 C1 N1 118.59(19) . . ? C2 C1 N1 120.67(19) . . ? N2 N1 C1 111.70(16) . . ? N2 N1 Fe1 130.99(14) . . ? C1 N1 Fe1 117.29(13) . . ? C1 C2 C3 119.1(2) . . ? C1 C2 H2 120.5 . . ? C3 C2 H2 120.5 . . ? N1 N2 C7 118.52(17) . . ? N4 N3 C7 119.01(17) . . ? C4 C3 C2 120.8(2) . . ? C4 C3 H3 119.6 . . ? C2 C3 H3 119.6 . . ? N3 N4 C14 111.31(16) . . ? N3 N4 Fe1 130.38(14) . . ? C14 N4 Fe1 118.14(13) . . ? C3 C4 C5 119.8(2) . . ? C3 C4 H4 120.1 . . ? C5 C4 H4 120.1 . . ? N8 N7 C26 118.81(17) . . ? N3 C7 N2 129.46(19) . . ? N3 C7 C8 115.35(18) . . ? N2 C7 C8 115.19(18) . . ? N5 N6 C26 119.01(17) . . ? C1 C6 C5 119.4(2) . . ? C1 C6 H6 120.3 . . ? C5 C6 H6 120.3 . . ? N6 N5 C20 112.19(16) . . ? N6 N5 Fe1 129.82(14) . . ? C20 N5 Fe1 117.93(14) . . ? C4 C5 C6 120.2(2) . . ? C4 C5 H5 119.9 . . ? C6 C5 H5 119.9 . . ? N7 N8 C33 112.44(16) . . ? N7 N8 Fe1 130.02(14) . . ? C33 N8 Fe1 117.46(13) . . ? C9 C8 C13 118.41(19) . . ? C9 C8 C7 121.09(19) . . ? C13 C8 C7 120.49(19) . . ? C10 C9 C8 121.1(2) . . ? C10 C9 H9 119.5 . . ? C8 C9 H9 119.5 . . ? C11 C10 C9 118.3(2) . . ? C11 C10 H10 120.8 . . ? C9 C10 H10 120.8 . . ? F1 C11 C10 118.7(2) . . ? F1 C11 C12 118.4(2) . . ? C10 C11 C12 122.8(2) . . ? C11 C12 C13 118.3(2) . . ? C11 C12 H12 120.9 . . ? C13 C12 H12 120.9 . . ? C12 C13 C8 121.0(2) . . ? C12 C13 H13 119.5 . . ? C8 C13 H13 119.5 . . ? C19 C14 C15 120.1(2) . . ? C19 C14 N4 119.28(19) . . ? C15 C14 N4 120.66(19) . . ? C17 C16 C15 120.9(2) . . ? C17 C16 H16 119.6 . . ? C15 C16 H16 119.6 . . ? C16 C15 C14 119.2(2) . . ? C16 C15 H15 120.4 . . ? C14 C15 H15 120.4 . . ? C16 C17 C18 119.8(2) . . ? C16 C17 H17 120.1 . . ? C18 C17 H17 120.1 . . ? C14 C19 C18 120.3(2) . . ? C14 C19 H19 119.9 . . ? C18 C19 H19 119.9 . . ? C17 C18 C19 119.7(2) . . ? C17 C18 H18 120.1 . . ? C19 C18 H18 120.1 . . ? C21 C20 C25 119.8(2) . . ? C21 C20 N5 120.9(2) . . ? C25 C20 N5 119.24(19) . . ? C22 C21 C20 119.7(2) . . ? C22 C21 H21 120.2 . . ? C20 C21 H21 120.2 . . ? C23 C22 C21 120.7(2) . . ? C23 C22 H22 119.6 . . ? C21 C22 H22 119.6 . . ? C22 C23 C24 119.7(2) . . ? C22 C23 H23 120.2 . . ? C24 C23 H23 120.2 . . ? C25 C24 C23 120.3(2) . . ? C25 C24 H24 119.9 . . ? C23 C24 H24 119.9 . . ? C24 C25 C20 119.7(2) . . ? C24 C25 H25 120.2 . . ? C20 C25 H25 120.2 . . ? N6 C26 N7 130.21(19) . . ? N6 C26 C27 114.89(18) . . ? N7 C26 C27 114.90(18) . . ? C32 C27 C28 118.3(2) . . ? C32 C27 C26 121.06(19) . . ? C28 C27 C26 120.64(19) . . ? C29 C28 C27 121.2(2) . . ? C29 C28 H28 119.4 . . ? C27 C28 H28 119.4 . . ? C30 C29 C28 118.7(2) . . ? C30 C29 H29 120.7 . . ? C28 C29 H29 120.7 . . ? F2 C30 C29 119.3(2) . . ? F2 C30 C31 118.6(2) . . ? C29 C30 C31 122.2(2) . . ? C30 C31 C32 118.6(2) . . ? C30 C31 H31 120.7 . . ? C32 C31 H31 120.7 . . ? C31 C32 C27 121.0(2) . . ? C31 C32 H32 119.5 . . ? C27 C32 H32 119.5 . . ? C38 C33 C34 119.7(2) . . ? C38 C33 N8 120.90(19) . . ? C34 C33 N8 119.36(19) . . ? C35 C34 C33 120.0(2) . . ? C35 C34 H34 120.0 . . ? C33 C34 H34 120.0 . . ? C36 C35 C34 120.2(2) . . ? C36 C35 H35 119.9 . . ? C34 C35 H35 119.9 . . ? C37 C36 C35 119.5(2) . . ? C37 C36 H36 120.2 . . ? C35 C36 H36 120.2 . . ? C36 C37 C38 120.9(2) . . ? C36 C37 H37 119.5 . . ? C38 C37 H37 119.5 . . ? C37 C38 C33 119.6(2) . . ? C37 C38 H38 120.2 . . ? C33 C38 H38 120.2 . . ? _refine_diff_density_max 0.585 _refine_diff_density_min -0.517 _refine_diff_density_rms 0.062 _shelx_res_file ; twin5.res created by SHELXL-2014/7 TITL twin4_a.res in P-1 REM Old TITL twin4 in P-1 REM SHELXT solution in P-1 REM R1 0.136, Rweak 0.010, Alpha 0.045, Orientation as input REM Formula found by SHELXT: C38 N9 F Fe CELL 0.71073 8.7833 11.1096 17.4380 87.536 83.792 71.550 ZERR 2.000 0.0030 0.0039 0.0051 0.022 0.021 0.023 LATT 1 SFAC C H N F FE UNIT 76 56 16 4 2 TEMP 0 SIZE 0.150 0.160 0.200 L.S. 10 BOND $H LIST 4 acta FMAP 2 PLAN 5 WGHT 0.039500 1.135500 BASF 0.48460 FVAR 0.34984 FE1 5 0.609866 0.263183 0.254285 11.00000 0.02275 0.01810 = 0.01496 0.00065 -0.00454 -0.00395 F1 4 1.046931 -0.561715 0.241637 11.00000 0.03245 0.02070 = 0.03845 -0.00262 0.00009 -0.00319 C1 1 0.492991 0.176351 0.132455 11.00000 0.01941 0.02148 = 0.01599 0.00333 -0.00450 -0.00916 N1 3 0.594080 0.138415 0.194727 11.00000 0.01781 0.02227 = 0.01435 0.00184 -0.00184 -0.00503 C2 1 0.545218 0.123890 0.059800 11.00000 0.02394 0.02292 = 0.01824 0.00045 -0.00286 -0.00854 AFIX 43 H2 2 0.643338 0.059795 0.051251 11.00000 -1.20000 AFIX 0 N2 3 0.657662 0.014272 0.198927 11.00000 0.01775 0.02143 = 0.01589 0.00109 -0.00064 -0.00568 F2 4 0.187780 1.090343 0.253892 11.00000 0.07092 0.01575 = 0.05361 0.00109 0.01801 -0.00584 N3 3 0.813197 0.024051 0.304520 11.00000 0.01840 0.02147 = 0.01649 0.00022 -0.00096 -0.00509 C3 1 0.448975 0.168396 0.000012 11.00000 0.03375 0.02833 = 0.01455 0.00044 -0.00260 -0.01363 AFIX 43 H3 2 0.483328 0.133988 -0.048930 11.00000 -1.20000 AFIX 0 N4 3 0.750312 0.148397 0.311317 11.00000 0.02021 0.02040 = 0.01407 -0.00023 -0.00102 -0.00652 C4 1 0.303342 0.262834 0.012339 11.00000 0.03005 0.03127 = 0.01975 0.00595 -0.01046 -0.01255 AFIX 43 H4 2 0.240431 0.292752 -0.028251 11.00000 -1.20000 AFIX 0 N7 3 0.417973 0.502937 0.317896 11.00000 0.01940 0.01966 = 0.01838 0.00080 -0.00514 -0.00489 C7 1 0.763057 -0.035130 0.251434 11.00000 0.01721 0.02401 = 0.01558 0.00051 -0.00119 -0.00733 N6 3 0.559454 0.513055 0.191362 11.00000 0.02008 0.01946 = 0.02076 0.00146 -0.00574 -0.00682 C6 1 0.345656 0.270550 0.145771 11.00000 0.02251 0.02522 = 0.01874 -0.00047 -0.00237 -0.00648 AFIX 43 H6 2 0.310829 0.304801 0.194726 11.00000 -1.20000 AFIX 0 N5 3 0.622820 0.388068 0.185184 11.00000 0.01838 0.02261 = 0.01712 0.00044 -0.00526 -0.00634 C5 1 0.250632 0.313276 0.085445 11.00000 0.02316 0.02813 = 0.02651 0.00236 -0.00772 -0.00533 AFIX 43 H5 2 0.151275 0.375941 0.094060 11.00000 -1.20000 AFIX 0 N8 3 0.479114 0.377878 0.323721 11.00000 0.02149 0.01991 = 0.01594 0.00160 -0.00612 -0.00713 C8 1 0.836030 -0.174680 0.249507 11.00000 0.01508 0.02260 = 0.01597 -0.00024 0.00129 -0.00546 C9 1 0.784218 -0.248588 0.201761 11.00000 0.02399 0.02564 = 0.02343 0.00116 -0.00745 -0.00895 AFIX 43 H9 2 0.700544 -0.209606 0.171696 11.00000 -1.20000 AFIX 0 C10 1 0.855178 -0.378523 0.198476 11.00000 0.02862 0.02617 = 0.02718 -0.00263 -0.00383 -0.01204 AFIX 43 H10 2 0.821451 -0.427256 0.166038 11.00000 -1.20000 AFIX 0 C11 1 0.976856 -0.434038 0.244320 11.00000 0.02172 0.01799 = 0.02691 -0.00166 0.00461 -0.00300 C12 1 1.031521 -0.365631 0.292712 11.00000 0.02245 0.02711 = 0.02734 0.00063 -0.00428 -0.00208 AFIX 43 H12 2 1.113713 -0.405997 0.323316 11.00000 -1.20000 AFIX 0 C13 1 0.961233 -0.235587 0.294658 11.00000 0.02270 0.02650 = 0.02321 -0.00345 -0.00449 -0.00464 AFIX 43 H13 2 0.997659 -0.187692 0.326478 11.00000 -1.20000 AFIX 0 C14 1 0.817514 0.195063 0.370934 11.00000 0.01804 0.02190 = 0.01640 -0.00210 -0.00291 -0.00229 C16 1 0.903480 0.179405 0.497718 11.00000 0.03500 0.03751 = 0.01640 0.00090 -0.00767 -0.00690 AFIX 43 H16 2 0.919068 0.136964 0.544787 11.00000 -1.20000 AFIX 0 C15 1 0.841833 0.130459 0.440903 11.00000 0.02953 0.02394 = 0.01975 0.00124 -0.00473 -0.00767 AFIX 43 H15 2 0.817008 0.055280 0.449457 11.00000 -1.20000 AFIX 0 C17 1 0.942099 0.290383 0.485399 11.00000 0.03030 0.03479 = 0.02429 -0.00867 -0.01044 -0.00568 AFIX 43 H17 2 0.982986 0.322493 0.524061 11.00000 -1.20000 AFIX 0 C19 1 0.856768 0.305943 0.358246 11.00000 0.03064 0.02771 = 0.02357 0.00353 -0.00930 -0.01066 AFIX 43 H19 2 0.840899 0.348695 0.311288 11.00000 -1.20000 AFIX 0 C18 1 0.919774 0.353681 0.415341 11.00000 0.03524 0.02797 = 0.03306 -0.00134 -0.01073 -0.01262 AFIX 43 H18 2 0.946855 0.427876 0.406537 11.00000 -1.20000 AFIX 0 C20 1 0.720576 0.351567 0.113526 11.00000 0.02121 0.02477 = 0.01921 -0.00131 -0.00183 -0.01158 C21 1 0.679739 0.420447 0.046036 11.00000 0.02968 0.02516 = 0.02123 0.00063 -0.00355 -0.01121 AFIX 43 H21 2 0.594371 0.495874 0.047760 11.00000 -1.20000 AFIX 0 C22 1 0.766735 0.376131 -0.023520 11.00000 0.04054 0.03561 = 0.02217 0.00126 -0.00142 -0.01771 AFIX 43 H22 2 0.738907 0.421825 -0.068628 11.00000 -1.20000 AFIX 0 C23 1 0.894428 0.264841 -0.026787 11.00000 0.03171 0.04444 = 0.02555 -0.00676 0.00813 -0.01890 AFIX 43 H23 2 0.950378 0.234498 -0.074016 11.00000 -1.20000 AFIX 0 C24 1 0.939008 0.198350 0.040784 11.00000 0.02498 0.03408 = 0.03392 -0.00483 0.00376 -0.00914 AFIX 43 H24 2 1.026329 0.124197 0.038833 11.00000 -1.20000 AFIX 0 C25 1 0.854036 0.241970 0.111021 11.00000 0.02184 0.02751 = 0.02651 0.00131 -0.00352 -0.00852 AFIX 43 H25 2 0.885719 0.198458 0.156328 11.00000 -1.20000 AFIX 0 C26 1 0.462386 0.561310 0.254616 11.00000 0.01959 0.02369 = 0.01824 0.00032 -0.00465 -0.00726 C27 1 0.392164 0.701578 0.254535 11.00000 0.02065 0.02341 = 0.02008 0.00074 -0.00054 -0.00881 C28 1 0.358117 0.768895 0.185495 11.00000 0.03059 0.02551 = 0.02178 0.00159 0.00130 -0.00676 AFIX 43 H28 2 0.382552 0.725142 0.139178 11.00000 -1.20000 AFIX 0 C29 1 0.288814 0.899262 0.184883 11.00000 0.04112 0.02510 = 0.02979 0.00762 0.00633 -0.00526 AFIX 43 H29 2 0.264931 0.943175 0.138831 11.00000 -1.20000 AFIX 0 C30 1 0.255915 0.962681 0.253673 11.00000 0.03904 0.01500 = 0.04296 0.00059 0.00961 -0.00631 C31 1 0.290407 0.900733 0.322794 11.00000 0.04431 0.02610 = 0.03197 -0.00758 0.00167 -0.01449 AFIX 43 H31 2 0.269483 0.945845 0.368512 11.00000 -1.20000 AFIX 0 C32 1 0.357109 0.769458 0.322886 11.00000 0.03493 0.02635 = 0.02291 -0.00051 -0.00495 -0.01284 AFIX 43 H32 2 0.378664 0.726282 0.369358 11.00000 -1.20000 AFIX 0 C33 1 0.424299 0.329452 0.395463 11.00000 0.01770 0.02197 = 0.01684 0.00253 -0.00445 -0.00171 C34 1 0.406790 0.208729 0.397888 11.00000 0.02328 0.02341 = 0.02193 -0.00018 -0.00201 -0.00487 AFIX 43 H34 2 0.419471 0.164123 0.352473 11.00000 -1.20000 AFIX 0 C35 1 0.370462 0.155304 0.468075 11.00000 0.02777 0.02781 = 0.02902 0.00720 -0.00188 -0.00827 AFIX 43 H35 2 0.361190 0.074108 0.469731 11.00000 -1.20000 AFIX 0 C36 1 0.347928 0.222617 0.535785 11.00000 0.02849 0.04207 = 0.02036 0.00916 -0.00042 -0.00785 AFIX 43 H36 2 0.325672 0.186218 0.582951 11.00000 -1.20000 AFIX 0 C37 1 0.358805 0.344244 0.532626 11.00000 0.03283 0.03911 = 0.01810 -0.00150 -0.00251 -0.00694 AFIX 43 H37 2 0.341188 0.390152 0.577875 11.00000 -1.20000 AFIX 0 C38 1 0.395581 0.398693 0.463000 11.00000 0.02813 0.02378 = 0.02101 -0.00067 -0.00511 -0.00434 AFIX 43 H38 2 0.401019 0.481025 0.461454 11.00000 -1.20000 AFIX 0 HKLF 5 REM twin4_a.res in P-1 REM R1 = 0.0394 for 12051 Fo > 4sig(Fo) and 0.0507 for all 13912 data REM 443 parameters refined using 0 restraints END WGHT 0.0395 1.1356 REM Highest difference peak 0.585, deepest hole -0.517, 1-sigma level 0.062 Q1 1 0.5683 0.3609 0.2515 11.00000 0.05 0.58 Q2 1 0.6495 0.1845 0.2527 11.00000 0.05 0.54 Q3 1 0.8143 0.3223 0.1096 11.00000 0.05 0.39 Q4 1 0.3809 0.2876 0.3977 11.00000 0.05 0.36 Q5 1 0.1751 1.2067 0.2344 11.00000 0.05 0.34 ; _shelx_res_checksum 8377 _shelx_hkl_file ; 2 2 0 6.03205 0.11048 -2 2 0 0 6.03205 0.11048 1 3 3 0 293.989 1.45249 -2 3 0 0 293.989 1.45249 1 4 4 0 284.479 1.40634 -2 4 0 0 284.479 1.40634 1 4 0 0 170.247 2.27281 2 4 0 0 183.277 3.52885 1 5 0 0 164.376 1.12783 1 5 0 0 150.227 0.94769 2 5 5 0 326.471 2.45361 -2 5 0 0 326.471 2.45361 1 6 0 0 12.5693 0.23604 2 6 0 0 13.0665 0.22245 1 7 0 0 2.14159 0.14314 1 7 0 0 1.77436 0.15899 2 8 0 0 6.88177 0.26506 1 8 0 0 6.25265 0.25106 2 9 0 0 33.3269 0.44039 1 9 0 0 32.0045 0.46972 2 10 0 0 0.43216 0.23017 2 10 0 0 0.96677 0.22608 1 -10 1 0 10.9266 0.69209 2 -10 1 0 11.6402 0.49457 1 -9 1 0 0.76304 0.20432 1 -9 1 0 0.49028 0.23171 2 -8 1 0 12.7401 0.34477 1 -8 1 0 11.7487 0.37945 2 -7 1 0 33.3155 0.36930 1 -7 1 0 30.2025 0.33434 2 -6 1 0 0.38953 0.10422 1 -6 1 0 0.25101 0.09573 2 -5 1 0 0.78811 0.08648 2 -5 1 0 1.11474 0.09477 1 -4 1 0 -0.0401 0.06166 1 -4 1 0 -0.0657 0.06818 2 -3 1 0 362.932 1.62787 1 -3 1 0 337.183 1.61439 2 3 4 0 731.980 13.5759 -2 -3 1 0 731.980 13.5759 1 -2 1 0 429.169 2.07237 2 -2 1 0 460.325 2.22348 1 2 3 0 821.946 11.7461 -2 -2 1 0 821.946 11.7461 1 -1 1 0 158.070 0.75073 2 -1 1 0 170.386 0.83893 1 1 2 0 233.695 3.96861 -2 -1 1 0 233.695 3.96861 1 2 1 0 730.254 4.11271 -2 2 1 0 730.254 4.11271 1 3 2 0 120.070 0.67242 -2 3 1 0 120.070 0.67242 1 4 3 0 49.3879 0.34802 -2 4 1 0 49.3879 0.34802 1 5 4 0 88.3605 0.56130 -2 5 1 0 88.3605 0.56130 1 6 5 0 85.2301 0.58466 -2 6 1 0 85.2301 0.58466 1 7 1 0 104.859 1.19069 1 7 6 0 148.222 1.15629 -2 7 1 0 148.222 1.15629 1 8 1 0 13.0330 0.37460 2 8 1 0 13.9819 0.31896 1 8 7 0 17.6829 1.61049 -2 8 1 0 17.6829 1.61049 1 9 1 0 0.32042 0.18810 2 9 1 0 0.30278 0.17283 1 10 1 0 13.2888 0.45212 1 10 1 0 12.5612 0.40394 2 -10 2 0 3.35279 0.55923 1 -10 2 0 1.86553 0.83350 2 -9 2 0 22.2955 0.50693 1 -9 2 0 20.9339 1.00933 2 -8 2 0 27.7942 0.45768 1 -8 2 0 25.1040 0.37715 2 7 10 0 99.8109 2.98377 -2 -8 2 0 99.8109 2.98377 1 -7 2 0 3.46725 0.18332 1 -7 2 0 3.65846 0.17692 2 -6 2 0 19.7447 0.26286 2 -6 2 0 21.7022 0.29711 1 -5 2 0 42.4107 0.32523 2 -5 2 0 46.0044 0.34136 1 -4 2 0 187.826 0.94603 2 -4 2 0 202.228 0.98054 1 -3 2 0 34.8635 0.25423 2 -3 2 0 37.0925 0.27973 1 -2 2 0 6.20678 0.10554 2 -2 2 0 6.83918 0.10514 1 -1 2 0 0.06456 0.03559 1 -1 2 0 0.15024 0.04311 2 0 2 0 897.649 4.70264 2 0 2 0 964.593 5.06912 1 1 2 0 74.6256 0.38253 2 1 2 0 76.9502 0.37635 1 -1 1 0 194.935 5.06182 -2 1 2 0 194.935 5.06182 1 2 0 0 5.73435 0.11860 -2 2 2 0 5.73435 0.11860 1 3 1 0 123.243 0.73043 -2 3 2 0 123.243 0.73043 1 4 2 0 640.730 3.13865 -2 4 2 0 640.730 3.13865 1 5 3 0 31.3226 0.28995 -2 5 2 0 31.3226 0.28995 1 6 4 0 0.14677 0.25517 -2 6 2 0 0.14677 0.25517 1 7 5 0 117.002 0.85974 -2 7 2 0 117.002 0.85974 1 8 6 0 48.0569 0.79955 -2 8 2 0 48.0569 0.79955 1 9 7 0 40.6541 0.80604 -2 9 2 0 40.6541 0.80604 1 9 2 0 30.0399 1.78116 1 10 2 0 1.24317 0.26084 2 10 8 0 7.47233 1.22181 -2 10 2 0 7.47233 1.22181 1 10 2 0 1.14312 0.30476 1 11 2 0 0.04965 0.30899 2 11 2 0 0.63470 0.32847 1 -9 3 0 0.55095 0.30698 1 -9 3 0 0.03324 0.29959 2 8 11 0 -0.0990 1.28478 -2 -9 3 0 -0.0990 1.28478 1 -8 3 0 31.6352 0.51023 2 -8 3 0 35.1120 0.51838 1 7 10 0 104.861 2.23431 -2 -8 3 0 104.861 2.23431 1 -7 3 0 40.7293 0.48315 1 -7 3 0 37.6879 0.45420 2 -6 3 0 42.3557 0.44077 1 -6 3 0 39.7209 0.40104 2 -5 3 0 16.3414 0.24414 2 -5 3 0 17.6362 0.24347 1 -4 3 0 29.7811 0.27239 1 -4 3 0 27.8170 0.27401 2 -3 3 0 442.857 2.05322 2 -3 3 0 472.921 2.18475 1 -2 3 0 49.1725 0.30159 1 -2 3 0 45.3636 0.29135 2 -1 3 0 12.4453 0.13811 1 -1 3 0 11.7974 0.13282 2 0 3 0 1.19302 0.04808 2 0 3 0 1.21418 0.05951 1 1 3 0 45.7874 0.26169 1 1 3 0 44.0992 0.24803 2 2 3 0 355.037 1.73030 1 2 3 0 339.342 1.55025 2 -2 1 0 814.318 11.7609 -2 2 3 0 814.318 11.7609 1 3 0 0 296.598 1.61222 -2 3 3 0 296.598 1.61222 1 4 1 0 49.1643 0.35903 -2 4 3 0 49.1643 0.35903 1 5 2 0 33.4717 0.30147 -2 5 3 0 33.4717 0.30147 1 6 3 0 166.659 0.92271 -2 6 3 0 166.659 0.92271 1 7 4 0 18.4652 0.32132 -2 7 3 0 18.4652 0.32132 1 8 5 0 0.45537 0.48654 -2 8 3 0 0.45537 0.48654 1 9 6 0 6.36483 0.55580 -2 9 3 0 6.36483 0.55580 1 10 7 0 7.37622 0.65531 -2 10 3 0 7.37622 0.65531 1 11 3 0 5.86940 0.31440 1 11 3 0 5.15521 0.30694 2 -9 4 0 0.55110 0.51855 2 -9 4 0 -0.4541 0.40639 1 8 12 0 1.23756 1.13225 -2 -9 4 0 1.23756 1.13225 1 -8 4 0 13.2140 0.41067 1 7 11 0 20.8992 1.69334 -2 -8 4 0 20.8992 1.69334 1 -8 4 0 12.3652 0.66712 2 -7 4 0 6.09761 0.24109 1 -7 4 0 5.23837 0.23250 2 6 10 0 34.2834 2.25884 -2 -7 4 0 34.2834 2.25884 1 -6 4 0 15.7940 0.28750 1 -6 4 0 14.8349 0.33584 2 -5 4 0 29.5570 0.32058 1 -5 4 0 28.4568 0.31391 2 -4 4 0 108.375 0.63446 1 -4 4 0 100.833 0.59978 2 -3 4 0 0.04186 0.08543 1 -3 4 0 0.05222 0.08377 2 -2 4 0 3.13821 0.10943 2 -2 4 0 3.47810 0.12258 1 -1 4 0 58.6276 0.34064 1 -1 4 0 55.3023 0.42252 2 0 4 0 17.9783 0.15783 2 0 4 0 19.0057 0.19251 1 1 4 0 6.93858 0.11359 1 1 4 0 6.72849 0.10566 2 2 4 0 7.52886 0.11349 1 2 4 0 7.37071 0.12204 2 3 4 0 349.053 1.57449 2 3 4 0 367.958 1.76010 1 -3 1 0 737.977 13.2670 -2 3 4 0 737.977 13.2670 1 4 0 0 277.469 1.51456 -2 4 4 0 277.469 1.51456 1 4 4 0 101.649 1.48465 1 4 4 0 95.9138 2.09840 2 5 1 0 94.6861 0.64172 -2 5 4 0 94.6861 0.64172 1 6 2 0 0.34276 0.39612 -2 6 4 0 0.34276 0.39612 1 7 3 0 19.0716 0.30123 -2 7 4 0 19.0716 0.30123 1 8 4 0 72.8953 0.72191 -2 8 4 0 72.8953 0.72191 1 9 5 0 2.27704 0.41548 -2 9 4 0 2.27704 0.41548 1 10 6 0 6.68608 0.50818 -2 10 4 0 6.68608 0.50818 1 11 7 0 4.16499 1.16818 -2 11 4 0 4.16499 1.16818 1 11 4 0 1.87157 0.40178 2 11 4 0 0.65100 0.36062 1 -8 5 0 0.03041 0.30640 1 -8 5 0 -0.1486 0.33127 2 7 12 0 -2.5027 1.75739 -2 -8 5 0 -2.5027 1.75739 1 -7 5 0 0.63865 0.25523 2 6 11 0 18.5569 1.18280 -2 -7 5 0 18.5569 1.18280 1 -7 5 0 0.59527 0.19436 1 -6 5 0 18.5351 0.31940 1 -6 5 0 17.4646 0.35125 2 -5 5 0 31.6800 0.36690 1 -5 5 0 29.2117 0.33762 2 -4 5 0 42.0553 0.36772 2 -4 5 0 43.8182 0.37195 1 -3 5 0 41.2916 0.33451 2 -3 5 0 44.3849 0.40563 1 -2 5 0 156.943 0.92371 2 -2 5 0 168.742 1.04561 1 -1 5 0 5.56320 0.15974 2 -1 5 0 6.27891 0.14447 1 0 5 0 13.2867 0.16149 2 0 5 0 14.0857 0.16344 1 1 5 0 68.1854 0.41156 1 1 5 0 64.2459 0.38103 2 2 5 0 123.088 0.64063 2 2 5 0 128.588 0.66182 1 3 5 0 97.6810 0.53512 1 3 5 0 92.6760 0.49810 2 4 5 0 38.1098 0.27612 1 4 5 0 36.4883 0.26284 2 5 5 0 167.035 1.15818 1 5 5 0 158.700 1.10681 2 5 0 0 327.839 2.93476 -2 5 5 0 327.839 2.93476 1 6 1 0 85.3205 0.64411 -2 6 5 0 85.3205 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11.6422 0.55486 -2 1 3 19 11.6422 0.55486 1 2 -1 19 1.08027 0.47809 -2 2 3 19 1.08027 0.47809 1 3 0 19 9.14268 0.45159 -2 3 3 19 9.14268 0.45159 1 4 1 19 36.0839 0.52871 -2 4 3 19 36.0839 0.52871 1 5 2 19 14.0249 0.90119 -2 5 3 19 14.0249 0.90119 1 6 3 19 0.44042 0.29943 -2 6 3 19 0.44042 0.29943 1 -3 4 19 -0.3504 0.24024 2 -3 4 19 -0.0373 0.34245 1 -2 4 19 5.16968 0.29951 1 -2 4 19 4.42168 0.27652 2 -1 4 19 2.68694 0.23399 2 -1 4 19 2.98646 0.24551 1 0 4 19 6.26993 0.25261 2 0 4 19 6.03287 0.24848 1 1 4 19 12.0337 0.36101 1 1 4 19 11.2800 0.36006 2 2 4 19 1.91944 0.16023 2 2 4 19 1.61306 0.19661 1 2 -2 19 6.37737 1.10563 -2 2 4 19 6.37737 1.10563 1 3 -1 19 6.73485 1.20975 -2 3 4 19 6.73485 1.20975 1 3 4 19 4.91094 0.29483 1 3 4 19 4.60484 0.32988 2 4 0 19 7.17453 0.74245 -2 4 4 19 7.17453 0.74245 1 4 4 19 6.13119 0.53940 2 5 1 19 54.8369 1.49113 -2 5 4 19 54.8369 1.49113 1 6 2 19 10.5666 0.63554 -2 6 4 19 10.5666 0.63554 1 -2 5 19 4.20179 0.33185 1 -2 5 19 4.29695 0.27129 2 -1 5 19 2.00823 0.25800 1 -1 5 19 1.78475 0.24503 2 0 5 19 0.60737 0.20509 2 0 5 19 0.84641 0.21891 1 1 5 19 1.69469 0.20286 2 1 5 19 1.65975 0.20192 1 2 5 19 21.6288 0.36471 2 2 5 19 23.9062 0.39116 1 3 5 19 16.5665 0.34168 2 3 5 19 18.1074 0.31008 1 4 -1 19 67.3053 3.36135 -2 4 5 19 67.3053 3.36135 1 4 5 19 25.6308 0.35469 2 4 5 19 27.4944 0.63538 1 5 5 19 0.59001 0.52175 2 5 0 19 11.4841 1.15048 -2 5 5 19 11.4841 1.15048 1 5 5 19 0.25961 0.37280 1 6 1 19 33.8984 0.92157 -2 6 5 19 33.8984 0.92157 1 -1 6 19 5.41356 0.26710 2 -1 6 19 5.62439 0.27714 1 0 6 19 4.81965 0.25203 1 0 6 19 4.95030 0.23529 2 1 6 19 6.21518 0.25668 1 1 6 19 6.07673 0.25100 2 2 6 19 -0.0212 0.19177 1 2 6 19 0.23951 0.18656 2 3 6 19 0.14277 0.19344 1 3 6 19 0.16919 0.16571 2 4 6 19 7.21658 0.41094 1 4 6 19 7.24718 0.29106 2 5 6 19 4.56376 0.29745 1 5 6 19 4.70208 0.22369 2 6 6 19 1.38344 0.25224 2 6 6 19 1.13677 0.35874 1 6 0 19 7.52446 1.71631 -2 6 6 19 7.52446 1.71631 1 0 7 19 0.94355 0.23939 1 0 7 19 0.83943 0.24264 2 1 7 19 0.71993 0.20360 2 1 7 19 0.89540 0.20488 1 2 7 19 3.60594 0.20566 2 2 7 19 3.79644 0.21634 1 3 7 19 1.34391 0.18809 1 3 7 19 1.38704 0.20290 2 4 7 19 4.54480 0.19294 2 4 7 19 4.53430 0.22853 1 5 7 19 0.07316 0.18870 2 5 7 19 -0.1841 0.26790 1 2 8 19 16.6777 1.94412 1 2 8 19 14.9627 1.50965 2 3 8 19 2.39327 0.29126 2 3 8 19 2.87247 0.25350 1 -2 -5 20 8.21618 0.34158 1 -2 -5 20 7.13564 0.34588 2 -1 -5 20 4.49202 0.29160 2 -1 -5 20 4.64359 0.26943 1 0 -5 20 0.78572 0.26725 2 0 -5 20 1.26029 0.24170 1 1 -5 20 0.34849 0.25580 1 1 -5 20 0.12003 0.26029 2 2 -5 20 8.48666 0.34062 1 2 -5 20 6.79874 0.32498 2 -3 1 20 20.8956 0.90703 -2 -3 -4 20 20.8956 0.90703 1 -3 -4 20 0.54612 0.66543 2 -2 -4 20 0.49378 0.24573 1 -2 -4 20 0.42195 0.26943 2 -1 -4 20 12.3735 0.40354 1 -1 -4 20 11.3661 0.38934 2 0 -4 20 24.1379 0.52102 2 0 -4 20 25.2522 0.47601 1 1 -4 20 6.86464 0.27301 2 1 -4 20 6.56691 0.26045 1 2 -4 20 0.18124 0.19185 1 2 -4 20 0.53598 0.22782 2 3 -4 20 3.87146 0.24452 2 3 -4 20 4.35382 0.23318 1 -3 0 20 2.56369 0.67792 -2 -3 -3 20 2.56369 0.67792 1 -2 1 20 19.5633 0.72098 -2 -2 -3 20 19.5633 0.72098 1 -1 2 20 56.3949 0.96263 -2 -1 -3 20 56.3949 0.96263 1 -1 -3 20 4.67919 0.46752 1 0 -3 20 0.39181 0.20934 1 0 -3 20 0.93364 0.25584 2 1 -3 20 4.08970 0.22103 1 1 -3 20 3.73412 0.23048 2 2 -3 20 8.54320 0.28963 1 2 -3 20 7.29583 0.28551 2 3 -3 20 12.6878 0.41140 2 3 -3 20 12.8516 0.35574 1 4 -3 20 -0.4266 0.28409 2 4 -3 20 -0.1651 0.20264 1 -3 -1 20 3.77459 0.55503 -2 -3 -2 20 3.77459 0.55503 1 -2 0 20 29.6120 0.62788 -2 -2 -2 20 29.6120 0.62788 1 -1 1 20 16.4388 0.57867 -2 -1 -2 20 16.4388 0.57867 1 0 2 20 9.41965 0.56459 -2 0 -2 20 9.41965 0.56459 1 1 3 20 2.03046 0.58526 -2 1 -2 20 2.03046 0.58526 1 1 -2 20 0.84853 0.67445 2 1 -2 20 1.70942 0.34203 1 2 -2 20 0.38953 0.18657 2 2 -2 20 0.62956 0.19145 1 3 -2 20 10.5477 0.30914 1 3 -2 20 9.13286 0.34792 2 4 -2 20 31.6117 0.45617 2 4 -2 20 35.0642 0.46772 1 -3 -2 20 1.54576 0.52068 -2 -3 -1 20 1.54576 0.52068 1 -2 -1 20 31.4104 0.51914 -2 -2 -1 20 31.4104 0.51914 1 -1 0 20 18.1857 0.47246 -2 -1 -1 20 18.1857 0.47246 1 0 1 20 11.9263 0.47921 -2 0 -1 20 11.9263 0.47921 1 1 2 20 0.77821 0.47102 -2 1 -1 20 0.77821 0.47102 1 2 3 20 -0.0090 0.47845 -2 2 -1 20 -0.0090 0.47845 1 3 4 20 44.4580 0.76917 -2 3 -1 20 44.4580 0.76917 1 3 -1 20 13.9272 0.59080 2 3 -1 20 13.5769 0.50215 1 4 -1 20 5.13016 0.19332 1 4 -1 20 4.99810 0.30713 2 5 -1 20 10.2806 0.32074 1 5 -1 20 10.7027 0.59355 2 -3 -3 20 4.30136 0.68571 -2 -3 0 20 4.30136 0.68571 1 -2 -2 20 27.6604 0.64125 -2 -2 0 20 27.6604 0.64125 1 -1 -1 20 18.4539 0.47873 -2 -1 0 20 18.4539 0.47873 1 0 0 20 133.881 0.87823 -2 0 0 20 133.881 0.87823 1 1 1 20 2.82345 0.32432 -2 1 0 20 2.82345 0.32432 1 2 2 20 18.9527 0.44249 -2 2 0 20 18.9527 0.44249 1 3 3 20 2.77327 0.59467 -2 3 0 20 2.77327 0.59467 1 4 4 20 35.2663 1.07844 -2 4 0 20 35.2663 1.07844 1 4 0 20 18.5527 1.07604 1 5 5 20 45.7483 1.27992 -2 5 0 20 45.7483 1.27992 1 5 0 20 19.6590 0.57944 1 -3 1 20 19.4373 1.08309 1 -3 -4 20 24.4438 1.08951 -2 -3 1 20 24.4438 1.08951 1 -2 -3 20 19.2424 0.73241 -2 -2 1 20 19.2424 0.73241 1 -1 -2 20 15.6184 0.61787 -2 -1 1 20 15.6184 0.61787 1 0 -1 20 13.2753 0.49675 -2 0 1 20 13.2753 0.49675 1 1 0 20 2.63964 0.37537 -2 1 1 20 2.63964 0.37537 1 2 1 20 73.4142 0.59025 -2 2 1 20 73.4142 0.59025 1 3 2 20 19.8850 0.44444 -2 3 1 20 19.8850 0.44444 1 4 3 20 14.1125 0.59028 -2 4 1 20 14.1125 0.59028 1 5 4 20 4.63844 1.00838 -2 5 1 20 4.63844 1.00838 1 -3 2 20 -0.4446 0.34122 1 -3 2 20 -0.4766 0.28274 2 -2 2 20 22.7053 0.55487 1 -2 2 20 22.0954 0.49525 2 -2 -4 20 22.6513 2.80539 -2 -2 2 20 22.6513 2.80539 1 -1 -3 20 60.1105 0.85326 -2 -1 2 20 60.1105 0.85326 1 -1 2 20 46.8698 0.89607 2 0 -2 20 9.40899 0.62793 -2 0 2 20 9.40899 0.62793 1 1 -1 20 0.10007 0.50739 -2 1 2 20 0.10007 0.50739 1 2 0 20 21.3192 0.45440 -2 2 2 20 21.3192 0.45440 1 3 1 20 20.3711 0.38784 -2 3 2 20 20.3711 0.38784 1 4 2 20 80.2139 0.87364 -2 4 2 20 80.2139 0.87364 1 5 3 20 17.7699 1.00630 -2 5 2 20 17.7699 1.00630 1 6 2 20 18.3860 0.72614 1 6 2 20 17.6690 1.12686 2 -2 3 20 6.21942 0.30799 1 -2 3 20 6.44467 0.30385 2 -1 3 20 4.38772 0.24769 2 -1 3 20 4.34778 0.28232 1 0 3 20 3.44801 0.29386 1 0 -3 20 2.18919 1.40127 -2 0 3 20 2.18919 1.40127 1 0 3 20 2.95586 0.21671 2 1 -2 20 2.34371 0.57936 -2 1 3 20 2.34371 0.57936 1 1 3 20 1.06815 0.33325 2 1 3 20 1.63247 0.61401 1 2 -1 20 0.91772 0.49859 -2 2 3 20 0.91772 0.49859 1 3 0 20 4.73338 0.44198 -2 3 3 20 4.73338 0.44198 1 4 1 20 17.1587 0.46156 -2 4 3 20 17.1587 0.46156 1 5 2 20 18.1476 0.84418 -2 5 3 20 18.1476 0.84418 1 6 3 20 0.23198 0.39763 -2 6 3 20 0.23198 0.39763 1 -2 4 20 -0.1264 0.30238 1 -2 4 20 0.27254 0.30455 2 -1 4 20 22.5606 0.57176 1 -1 4 20 20.3494 0.47255 2 0 4 20 10.1203 0.40753 1 0 4 20 9.52032 0.32585 2 1 4 20 0.00848 0.19962 1 1 4 20 0.41132 0.18565 2 2 4 20 13.5646 0.35704 1 2 4 20 13.2509 0.35719 2 2 -2 20 6.33159 1.91039 -2 2 4 20 6.33159 1.91039 1 3 4 20 30.2720 0.54603 1 3 4 20 27.4992 0.82178 2 3 -1 20 45.0702 0.98105 -2 3 4 20 45.0702 0.98105 1 4 0 20 29.8248 0.76227 -2 4 4 20 29.8248 0.76227 1 4 4 20 19.4356 1.00728 2 5 1 20 8.14441 1.17247 -2 5 4 20 8.14441 1.17247 1 -1 5 20 9.12995 0.36956 2 -1 5 20 8.85009 0.39244 1 0 5 20 1.83448 0.26252 1 0 5 20 1.06534 0.23526 2 1 5 20 17.8075 0.44707 1 1 5 20 15.7625 0.46224 2 2 5 20 5.10688 0.22540 1 2 5 20 4.77019 0.20851 2 3 5 20 1.35563 0.17546 1 3 5 20 1.72723 0.17187 2 4 5 20 1.08459 0.19965 2 4 5 20 1.37793 0.32411 1 4 -1 20 7.22820 2.90221 -2 4 5 20 7.22820 2.90221 1 5 0 20 45.1498 1.42916 -2 5 5 20 45.1498 1.42916 1 5 5 20 29.2416 2.08146 2 0 6 20 0.61031 0.30540 1 0 6 20 1.02869 0.27010 2 1 6 20 4.32642 0.23575 2 1 6 20 4.68477 0.26567 1 2 6 20 3.79218 0.21324 2 2 6 20 3.53677 0.22673 1 3 6 20 22.6638 0.39086 2 3 6 20 22.9083 0.45681 1 4 6 20 14.7235 0.38888 2 4 6 20 17.1489 0.61489 1 -1 -4 21 4.12496 0.31657 2 -1 -4 21 3.77579 0.30548 1 0 -4 21 1.27728 0.26063 1 0 -4 21 1.25178 0.27619 2 1 -4 21 8.62747 0.31193 1 1 -4 21 7.24883 0.32187 2 -2 1 21 20.0646 1.10799 -2 -2 -3 21 20.0646 1.10799 1 -1 -3 21 33.4231 0.97989 1 -1 2 21 34.7550 1.01548 -2 -1 -3 21 34.7550 1.01548 1 0 -3 21 38.7822 0.67770 2 0 -3 21 40.0084 0.56527 1 1 -3 21 7.42926 0.34085 2 1 -3 21 7.28363 0.27919 1 2 -3 21 1.01527 0.22600 1 2 -3 21 1.19838 0.23117 2 -2 0 21 12.5334 0.65847 -2 -2 -2 21 12.5334 0.65847 1 -1 1 21 9.17484 0.65282 -2 -1 -2 21 9.17484 0.65282 1 0 2 21 17.1989 0.65838 -2 0 -2 21 17.1989 0.65838 1 1 3 21 7.35245 0.70115 -2 1 -2 21 7.35245 0.70115 1 1 -2 21 6.51918 0.77127 2 1 -2 21 6.82372 0.49943 1 2 -2 21 3.72391 0.24695 2 2 -2 21 4.56594 0.23159 1 2 4 21 14.5634 2.40515 -2 2 -2 21 14.5634 2.40515 1 3 -2 21 2.60833 0.19245 1 3 -2 21 2.84539 0.20087 2 -2 -1 21 0.41764 0.28980 -2 -2 -1 21 0.41764 0.28980 1 -1 0 21 96.5187 0.81851 -2 -1 -1 21 96.5187 0.81851 1 0 1 21 19.3967 0.51654 -2 0 -1 21 19.3967 0.51654 1 1 2 21 0.90319 0.49638 -2 1 -1 21 0.90319 0.49638 1 2 3 21 0.58527 0.50034 -2 2 -1 21 0.58527 0.50034 1 3 4 21 40.8713 0.73304 -2 3 -1 21 40.8713 0.73304 1 3 -1 21 25.9263 0.92317 1 3 -1 21 26.0697 0.60512 2 4 -1 21 34.3187 0.41851 1 4 -1 21 33.0054 0.56507 2 -2 -2 21 14.2097 0.69231 -2 -2 0 21 14.2097 0.69231 1 -1 -1 21 94.2449 0.87493 -2 -1 0 21 94.2449 0.87493 1 0 0 21 1.48621 0.22619 -2 0 0 21 1.48621 0.22619 1 1 1 21 16.7293 0.44139 -2 1 0 21 16.7293 0.44139 1 2 2 21 0.52807 0.47600 -2 2 0 21 0.52807 0.47600 1 3 3 21 33.0308 0.65342 -2 3 0 21 33.0308 0.65342 1 4 4 21 12.6792 0.70123 -2 4 0 21 12.6792 0.70123 1 4 0 21 1.94514 0.34844 1 -2 -3 21 23.2034 1.03062 -2 -2 1 21 23.2034 1.03062 1 -1 -2 21 9.55823 0.67422 -2 -1 1 21 9.55823 0.67422 1 0 -1 21 20.5107 0.56649 -2 0 1 21 20.5107 0.56649 1 1 0 21 16.6398 0.42912 -2 1 1 21 16.6398 0.42912 1 2 1 21 0.54394 0.18202 -2 2 1 21 0.54394 0.18202 1 3 2 21 26.3655 0.53169 -2 3 1 21 26.3655 0.53169 1 4 3 21 42.5379 0.73885 -2 4 1 21 42.5379 0.73885 1 -2 2 21 0.31037 0.33729 1 -2 2 21 0.02594 0.28854 2 -1 -3 21 35.7490 0.87193 -2 -1 2 21 35.7490 0.87193 1 -1 2 21 0.50612 0.40238 2 0 -2 21 16.0340 0.67661 -2 0 2 21 16.0340 0.67661 1 1 -1 21 0.42854 0.53267 -2 1 2 21 0.42854 0.53267 1 2 0 21 0.96406 0.40405 -2 2 2 21 0.96406 0.40405 1 3 1 21 24.3931 0.50949 -2 3 2 21 24.3931 0.50949 1 4 2 21 6.32183 0.34013 -2 4 2 21 6.32183 0.34013 1 5 2 21 1.76539 0.51984 1 5 2 21 2.07746 0.54513 2 -1 3 21 13.5062 0.50017 2 -1 3 21 14.3672 0.50764 1 0 3 21 4.61748 0.30902 1 0 3 21 4.34171 0.24192 2 0 -3 21 47.5706 1.45741 -2 0 3 21 47.5706 1.45741 1 1 -2 21 6.71597 0.70019 -2 1 3 21 6.71597 0.70019 1 1 3 21 1.22083 0.37746 2 1 3 21 -0.4221 0.62438 1 2 -1 21 1.03350 0.58678 -2 2 3 21 1.03350 0.58678 1 3 0 21 32.6109 0.62603 -2 3 3 21 32.6109 0.62603 1 4 1 21 42.3380 0.71398 -2 4 3 21 42.3380 0.71398 1 0 4 21 29.2816 0.57844 1 0 4 21 27.2906 0.54903 2 1 4 21 7.45514 0.26828 2 1 4 21 8.27232 0.33747 1 2 4 21 7.08479 0.26842 2 2 -2 21 10.2435 1.47911 -2 2 4 21 10.2435 1.47911 1 2 4 21 7.60976 0.33693 1 3 -1 21 37.1909 1.01800 -2 3 4 21 37.1909 1.01800 1 3 4 21 12.7469 0.53543 1 3 4 21 11.6564 0.76215 2 4 0 21 14.8076 0.83285 -2 4 4 21 14.8076 0.83285 1 1 5 21 -0.1461 0.25237 1 1 5 21 0.20453 0.23941 2 2 5 21 3.34908 0.22283 2 2 5 21 3.59956 0.22853 1 3 5 21 19.8739 0.39302 2 3 5 21 21.6392 0.39556 1 0 2 22 6.32950 1.14421 -2 0 -2 22 6.32950 1.14421 1 1 3 22 55.7307 1.34836 -2 1 -2 22 55.7307 1.34836 1 1 -2 22 10.6774 0.89181 1 0 1 22 14.5766 0.72937 -2 0 -1 22 14.5766 0.72937 1 1 2 22 2.73978 0.60149 -2 1 -1 22 2.73978 0.60149 1 2 3 22 30.1917 0.84153 -2 2 -1 22 30.1917 0.84153 1 0 0 22 13.3589 0.44966 -2 0 0 22 13.3589 0.44966 1 1 1 22 4.69604 0.44210 -2 1 0 22 4.69604 0.44210 1 2 2 22 2.42586 0.44483 -2 2 0 22 2.42586 0.44483 1 3 0 22 0.25694 0.33278 1 3 0 22 0.27251 0.58594 2 0 -1 22 11.8705 0.74594 -2 0 1 22 11.8705 0.74594 1 1 0 22 4.11166 0.45767 -2 1 1 22 4.11166 0.45767 1 2 1 22 24.8724 0.43989 -2 2 1 22 24.8724 0.43989 1 3 2 22 2.05790 0.42904 -2 3 1 22 2.05790 0.42904 1 0 2 22 3.77274 0.36071 2 0 2 22 3.72313 0.32585 1 0 -2 22 14.4992 2.91500 -2 0 2 22 14.4992 2.91500 1 1 -1 22 0.91781 0.70241 -2 1 2 22 0.91781 0.70241 1 2 0 22 3.09737 0.47017 -2 2 2 22 3.09737 0.47017 1 3 1 22 1.97079 0.45123 -2 3 2 22 1.97079 0.45123 1 1 3 22 45.5539 0.92183 1 1 -2 22 57.0569 1.83444 -2 1 3 22 57.0569 1.83444 1 1 3 22 39.0443 1.53560 2 2 -1 22 33.8353 0.77450 -2 2 3 22 33.8353 0.77450 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 50240 #===END data_mo_molan508_0m_a_sq _audit_creation_method 'SHELXL-2018/1' _shelx_SHELXL_version_number '2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C40 H34 Fe N8 O2' _chemical_formula_weight 714.61 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.0505(4) _cell_length_b 16.0146(5) _cell_length_c 17.4162(5) _cell_angle_alpha 90 _cell_angle_beta 101.7610(10) _cell_angle_gamma 90 _cell_volume 3563.54(19) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9634 _cell_measurement_theta_min 3.00 _cell_measurement_theta_max 28.71 _exptl_crystal_description 'block' _exptl_crystal_colour 'red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.269 _exptl_crystal_F_000 1353 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.26 _exptl_crystal_size_mid 0.23 _exptl_crystal_size_min 0.13 _exptl_absorpt_coefficient_mu 0.468 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.7178 _exptl_absorpt_correction_T_max 0.7458 _exptl_absorpt_process_details 'SADABS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 113018 _diffrn_reflns_av_unetI/netI 0.0200 _diffrn_reflns_av_R_equivalents 0.0485 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_theta_min 3.002 _diffrn_reflns_theta_max 28.737 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 9224 _reflns_number_gt 7643 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0353P)^2^+2.2701P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 9224 _refine_ls_number_parameters 537 _refine_ls_number_restraints 136 _refine_ls_R_factor_all 0.0446 _refine_ls_R_factor_gt 0.0326 _refine_ls_wR_factor_ref 0.0840 _refine_ls_wR_factor_gt 0.0776 _refine_ls_goodness_of_fit_ref 1.022 _refine_ls_restrained_S_all 1.019 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.66297(2) 0.27549(2) 0.44911(2) 0.01404(5) Uani 1 1 d . . . . . O1 O 1.22890(8) 0.25411(8) 0.24745(6) 0.0269(2) Uani 1 1 d . . . . . O2 O 0.09853(8) 0.25199(7) 0.65542(6) 0.0249(2) Uani 1 1 d . . . . . N1 N 0.71201(8) 0.33525(7) 0.37334(6) 0.0147(2) Uani 1 1 d . . . . . N2 N 0.79484(8) 0.31807(7) 0.34238(6) 0.0148(2) Uani 1 1 d . . . . . N3 N 0.86228(8) 0.20800(7) 0.43507(6) 0.0150(2) Uani 1 1 d . . . . . N4 N 0.77577(8) 0.20451(7) 0.46389(6) 0.0146(2) Uani 1 1 d . . . . . N5 N 0.55277(8) 0.20413(7) 0.43993(6) 0.0139(2) Uani 1 1 d . . . . . N6 N 0.46772(8) 0.20665(7) 0.47085(6) 0.0142(2) Uani 1 1 d . . . . . N7 N 0.52597(8) 0.32957(7) 0.54900(6) 0.0152(2) Uani 1 1 d . . . . . N8 N 0.60803(8) 0.34172(7) 0.51583(6) 0.0152(2) Uani 1 1 d D . . . . C1 C 0.65045(10) 0.40145(8) 0.33008(8) 0.0161(2) Uani 1 1 d . . . . . C2 C 0.54583(11) 0.41187(9) 0.33507(8) 0.0207(3) Uani 1 1 d . . . . . H2 H 0.514546 0.374140 0.365581 0.025 Uiso 1 1 calc R U . . . C3 C 0.48699(11) 0.47708(9) 0.29572(9) 0.0240(3) Uani 1 1 d . . . . . H3 H 0.416216 0.484184 0.300291 0.029 Uiso 1 1 calc R U . . . C4 C 0.53110(11) 0.53187(9) 0.24978(9) 0.0246(3) Uani 1 1 d . . . . . H4 H 0.490888 0.576358 0.222862 0.030 Uiso 1 1 calc R U . . . C5 C 0.63473(12) 0.52085(9) 0.24364(9) 0.0241(3) Uani 1 1 d . . . . . H5 H 0.665082 0.557796 0.211869 0.029 Uiso 1 1 calc R U . . . C6 C 0.69460(11) 0.45639(9) 0.28344(8) 0.0202(3) Uani 1 1 d . . . . . H6 H 0.765467 0.449693 0.278945 0.024 Uiso 1 1 calc R U . . . C7 C 0.86517(10) 0.26157(8) 0.37612(7) 0.0137(2) Uani 1 1 d . . . . . C8 C 0.96164(10) 0.25692(8) 0.34343(7) 0.0135(2) Uani 1 1 d . . . . . C9 C 0.95875(10) 0.27625(8) 0.26479(7) 0.0147(2) Uani 1 1 d . . . . . H9 H 0.894256 0.291454 0.231681 0.018 Uiso 1 1 calc R U . . . C10 C 1.04897(10) 0.27345(8) 0.23470(7) 0.0159(2) Uani 1 1 d . . . . . H10 H 1.045863 0.286042 0.180967 0.019 Uiso 1 1 calc R U . . . C11 C 1.14454(10) 0.25221(8) 0.28288(8) 0.0162(2) Uani 1 1 d . . . . . C12 C 1.14892(10) 0.23204(8) 0.36114(8) 0.0168(2) Uani 1 1 d . . . . . H12 H 1.213540 0.216940 0.394144 0.020 Uiso 1 1 calc R U . . . C13 C 1.05731(10) 0.23425(8) 0.39053(7) 0.0161(2) Uani 1 1 d . . . . . H13 H 1.060081 0.220002 0.443863 0.019 Uiso 1 1 calc R U . . . C14 C 1.32868(12) 0.23513(14) 0.29504(11) 0.0435(5) Uani 1 1 d . . . . . H14A H 1.382414 0.238504 0.263217 0.065 Uiso 1 1 calc R U . . . H14B H 1.327458 0.178565 0.316307 0.065 Uiso 1 1 calc R U . . . H14C H 1.344705 0.275279 0.338295 0.065 Uiso 1 1 calc R U . . . C15 C 0.77951(10) 0.13557(8) 0.51738(7) 0.0152(2) Uani 1 1 d . . . . . C16 C 0.82551(11) 0.05998(9) 0.50286(8) 0.0201(3) Uani 1 1 d . . . . . H16 H 0.855083 0.053789 0.457650 0.024 Uiso 1 1 calc R U . . . C17 C 0.82778(12) -0.00590(9) 0.55473(8) 0.0236(3) Uani 1 1 d . . . . . H17 H 0.859361 -0.057248 0.545082 0.028 Uiso 1 1 calc R U . . . C18 C 0.78410(11) 0.00256(9) 0.62096(8) 0.0225(3) Uani 1 1 d . . . . . H18 H 0.785104 -0.043041 0.655984 0.027 Uiso 1 1 calc R U . . . C19 C 0.73916(11) 0.07784(9) 0.63549(8) 0.0205(3) Uani 1 1 d . . . . . H19 H 0.710018 0.083952 0.680908 0.025 Uiso 1 1 calc R U . . . C20 C 0.73654(10) 0.14447(9) 0.58388(8) 0.0177(3) Uani 1 1 d . . . . . H20 H 0.705525 0.195921 0.593953 0.021 Uiso 1 1 calc R U . . . C21 C 0.55121(9) 0.13304(8) 0.38936(7) 0.0138(2) Uani 1 1 d . . . . . C22 C 0.51750(11) 0.05607(9) 0.41161(8) 0.0198(3) Uani 1 1 d . . . . . H22 H 0.492789 0.050980 0.459066 0.024 Uiso 1 1 calc R U . . . C23 C 0.52004(11) -0.01327(9) 0.36434(9) 0.0220(3) Uani 1 1 d . . . . . H23 H 0.498946 -0.066234 0.380194 0.026 Uiso 1 1 calc R U . . . C24 C 0.55339(11) -0.00543(9) 0.29386(9) 0.0219(3) Uani 1 1 d . . . . . H24 H 0.555075 -0.052902 0.261437 0.026 Uiso 1 1 calc R U . . . C25 C 0.58417(11) 0.07196(9) 0.27107(8) 0.0220(3) Uani 1 1 d . . . . . H25 H 0.605279 0.077493 0.222239 0.026 Uiso 1 1 calc R U . . . C26 C 0.58455(10) 0.14145(8) 0.31866(8) 0.0172(3) Uani 1 1 d . . . . . H26 H 0.607249 0.194085 0.303260 0.021 Uiso 1 1 calc R U . . . C27 C 0.46016(10) 0.26611(8) 0.52368(7) 0.0134(2) Uani 1 1 d . . . . . C28 C 0.36610(10) 0.26008(8) 0.55931(7) 0.0139(2) Uani 1 1 d . . . . . C29 C 0.33343(11) 0.32811(9) 0.59827(8) 0.0201(3) Uani 1 1 d . . . . . H29 H 0.372871 0.378386 0.603426 0.024 Uiso 1 1 calc R U . . . C30 C 0.24413(11) 0.32317(9) 0.62951(9) 0.0231(3) Uani 1 1 d . . . . . H30 H 0.222408 0.370349 0.655167 0.028 Uiso 1 1 calc R U . . . C31 C 0.18590(10) 0.24976(9) 0.62368(8) 0.0180(3) Uani 1 1 d . . . . . C32 C 0.21932(10) 0.18039(9) 0.58744(7) 0.0167(2) Uani 1 1 d . . . . . H32 H 0.181595 0.129376 0.584677 0.020 Uiso 1 1 calc R U . . . C33 C 0.30833(10) 0.18611(8) 0.55526(7) 0.0157(2) Uani 1 1 d . . . . . H33 H 0.330293 0.138743 0.529998 0.019 Uiso 1 1 calc R U . . . C34 C 0.02570(11) 0.18469(10) 0.63651(9) 0.0247(3) Uani 1 1 d . . . . . H34A H 0.006273 0.178408 0.579418 0.037 Uiso 1 1 calc R U . . . H34B H -0.037036 0.196671 0.657372 0.037 Uiso 1 1 calc R U . . . H34C H 0.057966 0.132886 0.659791 0.037 Uiso 1 1 calc R U . . . C35 C 0.6713(9) 0.4096(7) 0.5556(8) 0.018(5) Uani 0.203(19) 1 d DG U P A 1 C36 C 0.6593(14) 0.4912(9) 0.5280(7) 0.032(5) Uani 0.203(19) 1 d G . P A 1 H36 H 0.608161 0.503880 0.482366 0.039 Uiso 0.203(19) 1 calc R U P A 1 C37 C 0.7221(14) 0.5543(6) 0.5673(7) 0.019(4) Uani 0.203(19) 1 d G . P A 1 H37 H 0.713942 0.610114 0.548399 0.022 Uiso 0.203(19) 1 calc R U P A 1 C38 C 0.7970(8) 0.5359(7) 0.6341(8) 0.020(4) Uani 0.203(19) 1 d G U P A 1 H38 H 0.839924 0.578989 0.660868 0.024 Uiso 0.203(19) 1 calc R U P A 1 C39 C 0.8090(14) 0.4543(8) 0.6616(12) 0.024(5) Uani 0.203(19) 1 d G . P A 1 H39 H 0.860127 0.441629 0.707303 0.029 Uiso 0.203(19) 1 calc R U P A 1 C40 C 0.7461(15) 0.3912(6) 0.6224(12) 0.026(5) Uani 0.203(19) 1 d G . P A 1 H40 H 0.754346 0.335394 0.641271 0.032 Uiso 0.203(19) 1 calc R U P A 1 C35' C 0.6747(5) 0.4101(3) 0.5574(4) 0.015(2) Uani 0.383(16) 1 d DG U P A 2 C36' C 0.6896(9) 0.4845(4) 0.5201(4) 0.029(2) Uani 0.383(16) 1 d G . P A 2 H36' H 0.655465 0.493451 0.467122 0.034 Uiso 0.383(16) 1 calc R U P A 2 C37' C 0.7545(9) 0.5459(4) 0.5603(4) 0.031(2) Uani 0.383(16) 1 d G . P A 2 H37' H 0.764766 0.596728 0.534845 0.038 Uiso 0.383(16) 1 calc R U P A 2 C38' C 0.8045(6) 0.5328(4) 0.6378(4) 0.030(2) Uani 0.383(16) 1 d G . P A 2 H38' H 0.848896 0.574692 0.665305 0.036 Uiso 0.383(16) 1 calc R U P A 2 C39' C 0.7896(6) 0.4583(4) 0.6751(3) 0.0203(13) Uani 0.383(16) 1 d G . P A 2 H39' H 0.823727 0.449378 0.728042 0.024 Uiso 0.383(16) 1 calc R U P A 2 C40' C 0.7246(7) 0.3970(4) 0.6348(4) 0.0187(14) Uani 0.383(16) 1 d G . P A 2 H40' H 0.714426 0.346099 0.660320 0.022 Uiso 0.383(16) 1 calc R U P A 2 C35" C 0.6711(3) 0.4069(3) 0.5509(3) 0.0173(16) Uani 0.425(12) 1 d DG U P A 3 C36" C 0.6329(4) 0.4881(3) 0.5408(3) 0.0234(12) Uani 0.425(12) 1 d G . P A 3 H36" H 0.565759 0.498341 0.509097 0.028 Uiso 0.425(12) 1 calc R U P A 3 C37" C 0.6931(5) 0.5541(3) 0.5770(3) 0.0255(14) Uani 0.425(12) 1 d G . P A 3 H37" H 0.666994 0.609614 0.570028 0.031 Uiso 0.425(12) 1 calc R U P A 3 C38" C 0.7913(4) 0.5391(3) 0.6233(3) 0.0302(16) Uani 0.425(12) 1 d G . P A 3 H38" H 0.832431 0.584271 0.648016 0.036 Uiso 0.425(12) 1 calc R U P A 3 C39" C 0.8295(3) 0.4579(3) 0.6334(5) 0.0359(16) Uani 0.425(12) 1 d G . P A 3 H39" H 0.896635 0.447655 0.665075 0.043 Uiso 0.425(12) 1 calc R U P A 3 C40" C 0.7693(4) 0.3918(2) 0.5972(4) 0.0277(14) Uani 0.425(12) 1 d G . P A 3 H40" H 0.795401 0.336380 0.604144 0.033 Uiso 0.425(12) 1 calc R U P A 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.01095(9) 0.01785(10) 0.01425(9) -0.00131(7) 0.00478(6) -0.00090(7) O1 0.0117(5) 0.0460(7) 0.0242(5) 0.0153(5) 0.0064(4) 0.0043(4) O2 0.0150(5) 0.0334(6) 0.0300(5) -0.0085(4) 0.0129(4) -0.0040(4) N1 0.0104(5) 0.0153(5) 0.0185(5) -0.0021(4) 0.0030(4) -0.0011(4) N2 0.0123(5) 0.0158(5) 0.0167(5) -0.0012(4) 0.0039(4) -0.0003(4) N3 0.0132(5) 0.0177(5) 0.0147(5) -0.0007(4) 0.0043(4) -0.0009(4) N4 0.0141(5) 0.0171(5) 0.0132(5) -0.0006(4) 0.0044(4) -0.0014(4) N5 0.0135(5) 0.0163(5) 0.0129(5) 0.0006(4) 0.0051(4) 0.0004(4) N6 0.0118(5) 0.0188(5) 0.0124(5) 0.0003(4) 0.0037(4) 0.0002(4) N7 0.0136(5) 0.0173(5) 0.0156(5) 0.0010(4) 0.0048(4) 0.0004(4) N8 0.0127(5) 0.0174(5) 0.0158(5) 0.0007(4) 0.0033(4) -0.0009(4) C1 0.0135(6) 0.0149(6) 0.0187(6) -0.0033(5) 0.0004(5) -0.0006(5) C2 0.0155(6) 0.0225(7) 0.0242(7) -0.0007(5) 0.0043(5) -0.0007(5) C3 0.0149(6) 0.0266(7) 0.0296(7) -0.0034(6) 0.0020(5) 0.0039(5) C4 0.0212(7) 0.0179(6) 0.0314(8) -0.0013(6) -0.0025(6) 0.0042(5) C5 0.0228(7) 0.0170(6) 0.0314(8) 0.0020(6) 0.0030(6) -0.0018(5) C6 0.0144(6) 0.0183(6) 0.0276(7) 0.0002(5) 0.0035(5) -0.0013(5) C7 0.0122(6) 0.0158(6) 0.0130(5) -0.0020(4) 0.0022(4) -0.0011(4) C8 0.0138(6) 0.0120(5) 0.0151(6) -0.0006(4) 0.0039(4) -0.0003(4) C9 0.0130(6) 0.0163(6) 0.0139(6) 0.0002(5) 0.0004(4) 0.0010(5) C10 0.0165(6) 0.0186(6) 0.0124(5) 0.0023(5) 0.0023(4) 0.0007(5) C11 0.0128(6) 0.0174(6) 0.0190(6) 0.0037(5) 0.0047(5) -0.0010(5) C12 0.0120(6) 0.0195(6) 0.0174(6) 0.0050(5) -0.0001(5) -0.0004(5) C13 0.0165(6) 0.0181(6) 0.0135(6) 0.0028(5) 0.0024(5) 0.0004(5) C14 0.0114(7) 0.0791(14) 0.0409(10) 0.0319(10) 0.0073(6) 0.0052(8) C15 0.0135(6) 0.0175(6) 0.0140(6) -0.0003(5) 0.0016(4) -0.0030(5) C16 0.0251(7) 0.0192(6) 0.0171(6) -0.0021(5) 0.0067(5) -0.0004(5) C17 0.0308(8) 0.0162(6) 0.0240(7) -0.0011(5) 0.0059(6) 0.0004(6) C18 0.0249(7) 0.0204(7) 0.0213(7) 0.0043(5) 0.0029(5) -0.0038(5) C19 0.0202(7) 0.0262(7) 0.0160(6) 0.0020(5) 0.0055(5) -0.0022(5) C20 0.0159(6) 0.0212(6) 0.0165(6) 0.0007(5) 0.0043(5) 0.0013(5) C21 0.0107(5) 0.0168(6) 0.0137(6) -0.0008(5) 0.0018(4) 0.0008(4) C22 0.0244(7) 0.0190(6) 0.0175(6) 0.0032(5) 0.0078(5) -0.0002(5) C23 0.0232(7) 0.0160(6) 0.0272(7) 0.0029(5) 0.0060(5) -0.0007(5) C24 0.0203(7) 0.0185(6) 0.0290(7) -0.0077(5) 0.0099(5) -0.0018(5) C25 0.0224(7) 0.0243(7) 0.0233(7) -0.0068(5) 0.0143(5) -0.0050(5) C26 0.0169(6) 0.0177(6) 0.0193(6) -0.0013(5) 0.0089(5) -0.0034(5) C27 0.0123(5) 0.0169(6) 0.0110(5) 0.0013(4) 0.0023(4) 0.0014(4) C28 0.0113(5) 0.0191(6) 0.0111(5) -0.0004(4) 0.0017(4) 0.0004(5) C29 0.0180(6) 0.0200(6) 0.0236(7) -0.0051(5) 0.0076(5) -0.0022(5) C30 0.0200(7) 0.0233(7) 0.0285(7) -0.0093(6) 0.0111(6) -0.0004(5) C31 0.0127(6) 0.0267(7) 0.0156(6) -0.0019(5) 0.0047(5) -0.0011(5) C32 0.0143(6) 0.0205(6) 0.0155(6) -0.0011(5) 0.0035(5) -0.0027(5) C33 0.0154(6) 0.0179(6) 0.0142(6) -0.0008(5) 0.0042(5) 0.0016(5) C34 0.0149(6) 0.0376(8) 0.0226(7) -0.0018(6) 0.0064(5) -0.0058(6) C35 0.013(6) 0.019(5) 0.022(6) -0.002(4) 0.005(4) -0.001(4) C36 0.044(10) 0.021(4) 0.029(7) 0.000(4) 0.001(6) 0.003(5) C37 0.025(7) 0.016(4) 0.019(4) -0.002(3) 0.013(5) 0.007(4) C38 0.022(5) 0.020(4) 0.022(5) -0.002(4) 0.010(4) -0.001(3) C39 0.011(6) 0.024(4) 0.034(8) 0.006(5) -0.006(6) -0.004(4) C40 0.017(8) 0.020(5) 0.038(8) 0.011(5) -0.004(7) -0.010(4) C35' 0.015(3) 0.008(2) 0.021(3) -0.006(2) 0.004(2) -0.008(2) C36' 0.040(4) 0.020(2) 0.020(2) 0.0047(18) -0.007(2) -0.009(2) C37' 0.043(5) 0.016(2) 0.031(3) 0.001(2) -0.004(3) -0.008(2) C38' 0.030(4) 0.027(3) 0.028(3) -0.005(2) -0.004(2) -0.010(3) C39' 0.018(3) 0.026(2) 0.019(2) -0.0056(16) 0.0074(19) -0.0014(18) C40' 0.016(3) 0.021(2) 0.021(2) -0.0013(16) 0.0068(18) -0.0011(17) C35" 0.018(3) 0.023(2) 0.014(2) 0.0034(19) 0.0085(18) 0.003(2) C36" 0.026(2) 0.0208(18) 0.022(2) 0.0001(15) 0.0035(19) 0.0020(16) C37" 0.036(3) 0.0187(18) 0.026(2) -0.0030(15) 0.017(2) -0.0004(18) C38" 0.037(3) 0.017(2) 0.039(3) -0.007(2) 0.013(2) -0.015(2) C39" 0.024(2) 0.027(2) 0.050(4) -0.001(2) -0.007(2) -0.0081(17) C40" 0.021(2) 0.0191(18) 0.039(3) 0.0005(17) -0.003(2) -0.0030(15) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N5 1.8183(11) . ? Fe1 N8 1.8246(11) . ? Fe1 N4 1.8360(11) . ? Fe1 N1 1.8470(11) . ? O1 C11 1.3677(16) . ? O1 C14 1.4265(18) . ? O2 C31 1.3653(16) . ? O2 C34 1.4303(18) . ? N1 N2 1.3313(14) . ? N1 C1 1.4459(16) . ? N2 C7 1.3366(16) . ? N3 N4 1.3270(15) . ? N3 C7 1.3443(16) . ? N4 C15 1.4389(16) . ? N5 N6 1.3294(14) . ? N5 C21 1.4370(16) . ? N6 C27 1.3417(16) . ? N7 N8 1.3306(15) . ? N7 C27 1.3456(16) . ? N8 C35" 1.391(4) . ? N8 C35 1.453(8) . ? N8 C35' 1.490(4) . ? C1 C2 1.3958(18) . ? C1 C6 1.3988(19) . ? C2 C3 1.391(2) . ? C2 H2 0.9500 . ? C3 C4 1.389(2) . ? C3 H3 0.9500 . ? C4 C5 1.389(2) . ? C4 H4 0.9500 . ? C5 C6 1.391(2) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 C8 1.4857(17) . ? C8 C13 1.3950(17) . ? C8 C9 1.3970(17) . ? C9 C10 1.3837(17) . ? C9 H9 0.9500 . ? C10 C11 1.3960(18) . ? C10 H10 0.9500 . ? C11 C12 1.3904(18) . ? C12 C13 1.3936(18) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C20 1.3931(17) . ? C15 C16 1.3971(18) . ? C16 C17 1.3855(19) . ? C16 H16 0.9500 . ? C17 C18 1.393(2) . ? C17 H17 0.9500 . ? C18 C19 1.386(2) . ? C18 H18 0.9500 . ? C19 C20 1.3912(19) . ? C19 H19 0.9500 . ? C20 H20 0.9500 . ? C21 C22 1.3902(18) . ? C21 C26 1.3937(17) . ? C22 C23 1.3866(19) . ? C22 H22 0.9500 . ? C23 C24 1.389(2) . ? C23 H23 0.9500 . ? C24 C25 1.386(2) . ? C24 H24 0.9500 . ? C25 C26 1.3869(18) . ? C25 H25 0.9500 . ? C26 H26 0.9500 . ? C27 C28 1.4872(17) . ? C28 C29 1.3953(18) . ? C28 C33 1.3983(18) . ? C29 C30 1.3852(19) . ? C29 H29 0.9500 . ? C30 C31 1.392(2) . ? C30 H30 0.9500 . ? C31 C32 1.3911(19) . ? C32 C33 1.3918(17) . ? C32 H32 0.9500 . ? C33 H33 0.9500 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 C36 1.3900 . ? C35 C40 1.3900 . ? C36 C37 1.3900 . ? C36 H36 0.9500 . ? C37 C38 1.3900 . ? C37 H37 0.9500 . ? C38 C39 1.3900 . ? C38 H38 0.9500 . ? C39 C40 1.3900 . ? C39 H39 0.9500 . ? C40 H40 0.9500 . ? C35' C36' 1.3900 . ? C35' C40' 1.3900 . ? C36' C37' 1.3900 . ? C36' H36' 0.9500 . ? C37' C38' 1.3900 . ? C37' H37' 0.9500 . ? C38' C39' 1.3900 . ? C38' H38' 0.9500 . ? C39' C40' 1.3900 . ? C39' H39' 0.9500 . ? C40' H40' 0.9500 . ? C35" C36" 1.3900 . ? C35" C40" 1.3900 . ? C36" C37" 1.3900 . ? C36" H36" 0.9500 . ? C37" C38" 1.3900 . ? C37" H37" 0.9500 . ? C38" C39" 1.3900 . ? C38" H38" 0.9500 . ? C39" C40" 1.3900 . ? C39" H39" 0.9500 . ? C40" H40" 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N5 Fe1 N8 90.85(5) . . ? N5 Fe1 N4 102.73(5) . . ? N8 Fe1 N4 132.73(5) . . ? N5 Fe1 N1 130.23(5) . . ? N8 Fe1 N1 113.09(5) . . ? N4 Fe1 N1 92.08(5) . . ? C11 O1 C14 117.16(11) . . ? C31 O2 C34 117.24(11) . . ? N2 N1 C1 110.57(10) . . ? N2 N1 Fe1 127.63(9) . . ? C1 N1 Fe1 121.04(8) . . ? N1 N2 C7 120.22(11) . . ? N4 N3 C7 118.31(11) . . ? N3 N4 C15 110.98(10) . . ? N3 N4 Fe1 129.83(9) . . ? C15 N4 Fe1 119.09(8) . . ? N6 N5 C21 111.31(10) . . ? N6 N5 Fe1 131.01(9) . . ? C21 N5 Fe1 117.65(8) . . ? N5 N6 C27 118.91(11) . . ? N8 N7 C27 118.99(11) . . ? N7 N8 C35" 112.1(2) . . ? N7 N8 C35 109.4(5) . . ? N7 N8 C35' 109.8(3) . . ? N7 N8 Fe1 130.32(9) . . ? C35" N8 Fe1 116.2(2) . . ? C35 N8 Fe1 118.7(5) . . ? C35' N8 Fe1 118.0(3) . . ? C2 C1 C6 119.01(12) . . ? C2 C1 N1 120.13(12) . . ? C6 C1 N1 120.86(11) . . ? C3 C2 C1 120.51(13) . . ? C3 C2 H2 119.7 . . ? C1 C2 H2 119.7 . . ? C4 C3 C2 120.41(13) . . ? C4 C3 H3 119.8 . . ? C2 C3 H3 119.8 . . ? C3 C4 C5 119.23(13) . . ? C3 C4 H4 120.4 . . ? C5 C4 H4 120.4 . . ? C4 C5 C6 120.83(14) . . ? C4 C5 H5 119.6 . . ? C6 C5 H5 119.6 . . ? C5 C6 C1 120.00(13) . . ? C5 C6 H6 120.0 . . ? C1 C6 H6 120.0 . . ? N2 C7 N3 130.10(12) . . ? N2 C7 C8 115.16(11) . . ? N3 C7 C8 114.74(11) . . ? C13 C8 C9 118.44(11) . . ? C13 C8 C7 120.96(11) . . ? C9 C8 C7 120.60(11) . . ? C10 C9 C8 120.61(11) . . ? C10 C9 H9 119.7 . . ? C8 C9 H9 119.7 . . ? C9 C10 C11 120.34(12) . . ? C9 C10 H10 119.8 . . ? C11 C10 H10 119.8 . . ? O1 C11 C12 124.84(12) . . ? O1 C11 C10 115.22(11) . . ? C12 C11 C10 119.94(12) . . ? C11 C12 C13 119.16(12) . . ? C11 C12 H12 120.4 . . ? C13 C12 H12 120.4 . . ? C12 C13 C8 121.51(12) . . ? C12 C13 H13 119.2 . . ? C8 C13 H13 119.2 . . ? O1 C14 H14A 109.5 . . ? O1 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? O1 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C20 C15 C16 119.99(12) . . ? C20 C15 N4 119.57(12) . . ? C16 C15 N4 120.44(11) . . ? C17 C16 C15 119.65(12) . . ? C17 C16 H16 120.2 . . ? C15 C16 H16 120.2 . . ? C16 C17 C18 120.51(13) . . ? C16 C17 H17 119.7 . . ? C18 C17 H17 119.7 . . ? C19 C18 C17 119.70(13) . . ? C19 C18 H18 120.1 . . ? C17 C18 H18 120.1 . . ? C18 C19 C20 120.30(13) . . ? C18 C19 H19 119.8 . . ? C20 C19 H19 119.8 . . ? C19 C20 C15 119.85(13) . . ? C19 C20 H20 120.1 . . ? C15 C20 H20 120.1 . . ? C22 C21 C26 120.36(12) . . ? C22 C21 N5 119.84(11) . . ? C26 C21 N5 119.80(11) . . ? C23 C22 C21 119.83(12) . . ? C23 C22 H22 120.1 . . ? C21 C22 H22 120.1 . . ? C22 C23 C24 120.13(13) . . ? C22 C23 H23 119.9 . . ? C24 C23 H23 119.9 . . ? C25 C24 C23 119.69(13) . . ? C25 C24 H24 120.2 . . ? C23 C24 H24 120.2 . . ? C24 C25 C26 120.82(13) . . ? C24 C25 H25 119.6 . . ? C26 C25 H25 119.6 . . ? C25 C26 C21 119.12(12) . . ? C25 C26 H26 120.4 . . ? C21 C26 H26 120.4 . . ? N6 C27 N7 129.01(11) . . ? N6 C27 C28 114.99(11) . . ? N7 C27 C28 115.99(11) . . ? C29 C28 C33 118.10(12) . . ? C29 C28 C27 120.82(12) . . ? C33 C28 C27 121.08(11) . . ? C30 C29 C28 120.76(13) . . ? C30 C29 H29 119.6 . . ? C28 C29 H29 119.6 . . ? C29 C30 C31 120.66(13) . . ? C29 C30 H30 119.7 . . ? C31 C30 H30 119.7 . . ? O2 C31 C32 124.71(12) . . ? O2 C31 C30 115.91(12) . . ? C32 C31 C30 119.38(12) . . ? C31 C32 C33 119.65(12) . . ? C31 C32 H32 120.2 . . ? C33 C32 H32 120.2 . . ? C32 C33 C28 121.40(12) . . ? C32 C33 H33 119.3 . . ? C28 C33 H33 119.3 . . ? O2 C34 H34A 109.5 . . ? O2 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? O2 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C36 C35 C40 120.0 . . ? C36 C35 N8 121.7(10) . . ? C40 C35 N8 118.3(10) . . ? C37 C36 C35 120.0 . . ? C37 C36 H36 120.0 . . ? C35 C36 H36 120.0 . . ? C36 C37 C38 120.0 . . ? C36 C37 H37 120.0 . . ? C38 C37 H37 120.0 . . ? C39 C38 C37 120.0 . . ? C39 C38 H38 120.0 . . ? C37 C38 H38 120.0 . . ? C40 C39 C38 120.0 . . ? C40 C39 H39 120.0 . . ? C38 C39 H39 120.0 . . ? C39 C40 C35 120.0 . . ? C39 C40 H40 120.0 . . ? C35 C40 H40 120.0 . . ? C36' C35' C40' 120.0 . . ? C36' C35' N8 121.8(4) . . ? C40' C35' N8 118.2(4) . . ? C37' C36' C35' 120.0 . . ? C37' C36' H36' 120.0 . . ? C35' C36' H36' 120.0 . . ? C36' C37' C38' 120.0 . . ? C36' C37' H37' 120.0 . . ? C38' C37' H37' 120.0 . . ? C39' C38' C37' 120.0 . . ? C39' C38' H38' 120.0 . . ? C37' C38' H38' 120.0 . . ? C38' C39' C40' 120.0 . . ? C38' C39' H39' 120.0 . . ? C40' C39' H39' 120.0 . . ? C39' C40' C35' 120.0 . . ? C39' C40' H40' 120.0 . . ? C35' C40' H40' 120.0 . . ? C36" C35" C40" 120.0 . . ? C36" C35" N8 118.8(3) . . ? C40" C35" N8 121.2(3) . . ? C37" C36" C35" 120.0 . . ? C37" C36" H36" 120.0 . . ? C35" C36" H36" 120.0 . . ? C36" C37" C38" 120.0 . . ? C36" C37" H37" 120.0 . . ? C38" C37" H37" 120.0 . . ? C39" C38" C37" 120.0 . . ? C39" C38" H38" 120.0 . . ? C37" C38" H38" 120.0 . . ? C38" C39" C40" 120.0 . . ? C38" C39" H39" 120.0 . . ? C40" C39" H39" 120.0 . . ? C39" C40" C35" 120.0 . . ? C39" C40" H40" 120.0 . . ? C35" C40" H40" 120.0 . . ? _refine_diff_density_max 0.454 _refine_diff_density_min -0.366 _refine_diff_density_rms 0.052 _shelx_res_file ; TITL mo_molan508_0m_a.res in P2(1)/n mo_molan508_0m_a_sq.res created by SHELXL-2018/1 at 14:16:26 on 16-Apr-2018 REM Old TITL mo_molan508_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.135, Rweak 0.004, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C43 N10 Fe CELL 0.71073 13.0505 16.0146 17.4162 90.000 101.761 90.000 ZERR 4.000 0.0004 0.0005 0.0005 0.000 0.001 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C N O FE H UNIT 160 32 8 4 1 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -173.170 L.S. 10 0 22 BOND $H dfix 1.44 0.01 N8 C35 N8 C35' N8 C35" rigu 0.002 C35 > C40 rigu 0.002 C35' > C40' rigu 0.002 C35" > C40" sump 1 0.01 1 2 1 3 1 4 isor 0.005 C38 c35 C35' C35" FMAP 2 PLAN 20 ABIN ACTA WGHT 0.035300 2.270100 FVAR 0.19452 0.20335 0.38337 0.42457 FE1 4 0.662974 0.275490 0.449111 11.00000 0.01095 0.01785 = 0.01425 -0.00131 0.00478 -0.00090 O1 3 1.228902 0.254111 0.247454 11.00000 0.01168 0.04598 = 0.02423 0.01535 0.00635 0.00432 O2 3 0.098530 0.251987 0.655419 11.00000 0.01499 0.03337 = 0.02998 -0.00851 0.01290 -0.00404 N1 2 0.712014 0.335248 0.373339 11.00000 0.01036 0.01534 = 0.01855 -0.00208 0.00304 -0.00111 N2 2 0.794839 0.318069 0.342381 11.00000 0.01233 0.01580 = 0.01675 -0.00116 0.00387 -0.00027 N3 2 0.862285 0.208003 0.435072 11.00000 0.01322 0.01771 = 0.01470 -0.00072 0.00430 -0.00094 N4 2 0.775772 0.204508 0.463893 11.00000 0.01408 0.01710 = 0.01320 -0.00060 0.00445 -0.00141 N5 2 0.552774 0.204133 0.439934 11.00000 0.01348 0.01633 = 0.01292 0.00056 0.00508 0.00036 N6 2 0.467720 0.206647 0.470847 11.00000 0.01176 0.01880 = 0.01241 0.00031 0.00368 0.00019 N7 2 0.525970 0.329573 0.548999 11.00000 0.01363 0.01729 = 0.01558 0.00098 0.00476 0.00040 N8 2 0.608027 0.341723 0.515830 11.00000 0.01265 0.01743 = 0.01580 0.00066 0.00332 -0.00094 C1 1 0.650452 0.401454 0.330081 11.00000 0.01346 0.01494 = 0.01875 -0.00332 0.00044 -0.00064 C2 1 0.545825 0.411872 0.335073 11.00000 0.01545 0.02252 = 0.02419 -0.00068 0.00429 -0.00070 AFIX 43 H2 5 0.514546 0.374140 0.365581 11.00000 -1.20000 AFIX 0 C3 1 0.486994 0.477083 0.295716 11.00000 0.01488 0.02661 = 0.02955 -0.00340 0.00201 0.00388 AFIX 43 H3 5 0.416216 0.484184 0.300291 11.00000 -1.20000 AFIX 0 C4 1 0.531105 0.531870 0.249776 11.00000 0.02117 0.01787 = 0.03144 -0.00132 -0.00245 0.00424 AFIX 43 H4 5 0.490888 0.576358 0.222862 11.00000 -1.20000 AFIX 0 C5 1 0.634726 0.520853 0.243640 11.00000 0.02279 0.01702 = 0.03138 0.00195 0.00304 -0.00184 AFIX 43 H5 5 0.665082 0.557796 0.211869 11.00000 -1.20000 AFIX 0 C6 1 0.694601 0.456392 0.283443 11.00000 0.01436 0.01831 = 0.02756 0.00021 0.00351 -0.00127 AFIX 43 H6 5 0.765467 0.449693 0.278945 11.00000 -1.20000 AFIX 0 C7 1 0.865166 0.261574 0.376122 11.00000 0.01219 0.01585 = 0.01300 -0.00195 0.00216 -0.00107 C8 1 0.961641 0.256920 0.343427 11.00000 0.01383 0.01204 = 0.01514 -0.00064 0.00392 -0.00035 C9 1 0.958754 0.276248 0.264794 11.00000 0.01295 0.01627 = 0.01389 0.00024 0.00040 0.00104 AFIX 43 H9 5 0.894256 0.291454 0.231681 11.00000 -1.20000 AFIX 0 C10 1 1.048973 0.273446 0.234696 11.00000 0.01650 0.01863 = 0.01240 0.00226 0.00229 0.00074 AFIX 43 H10 5 1.045863 0.286042 0.180967 11.00000 -1.20000 AFIX 0 C11 1 1.144540 0.252205 0.282883 11.00000 0.01279 0.01742 = 0.01895 0.00373 0.00466 -0.00098 C12 1 1.148921 0.232038 0.361135 11.00000 0.01204 0.01954 = 0.01740 0.00504 -0.00011 -0.00042 AFIX 43 H12 5 1.213540 0.216940 0.394144 11.00000 -1.20000 AFIX 0 C13 1 1.057314 0.234253 0.390530 11.00000 0.01649 0.01810 = 0.01349 0.00282 0.00238 0.00035 AFIX 43 H13 5 1.060081 0.220002 0.443863 11.00000 -1.20000 AFIX 0 C14 1 1.328677 0.235130 0.295042 11.00000 0.01137 0.07909 = 0.04091 0.03186 0.00732 0.00521 AFIX 137 H14A 5 1.382414 0.238504 0.263217 11.00000 -1.50000 H14B 5 1.327458 0.178565 0.316307 11.00000 -1.50000 H14C 5 1.344705 0.275279 0.338295 11.00000 -1.50000 AFIX 0 C15 1 0.779506 0.135571 0.517381 11.00000 0.01354 0.01751 = 0.01404 -0.00034 0.00161 -0.00301 C16 1 0.825512 0.059981 0.502856 11.00000 0.02509 0.01920 = 0.01712 -0.00213 0.00672 -0.00042 AFIX 43 H16 5 0.855083 0.053789 0.457650 11.00000 -1.20000 AFIX 0 C17 1 0.827780 -0.005903 0.554734 11.00000 0.03083 0.01618 = 0.02398 -0.00110 0.00589 0.00042 AFIX 43 H17 5 0.859361 -0.057248 0.545082 11.00000 -1.20000 AFIX 0 C18 1 0.784096 0.002564 0.620955 11.00000 0.02493 0.02040 = 0.02134 0.00430 0.00293 -0.00375 AFIX 43 H18 5 0.785104 -0.043041 0.655984 11.00000 -1.20000 AFIX 0 C19 1 0.739159 0.077840 0.635491 11.00000 0.02016 0.02617 = 0.01601 0.00204 0.00551 -0.00219 AFIX 43 H19 5 0.710018 0.083952 0.680908 11.00000 -1.20000 AFIX 0 C20 1 0.736541 0.144471 0.583876 11.00000 0.01592 0.02119 = 0.01650 0.00073 0.00428 0.00125 AFIX 43 H20 5 0.705525 0.195921 0.593953 11.00000 -1.20000 AFIX 0 C21 1 0.551205 0.133041 0.389363 11.00000 0.01072 0.01675 = 0.01370 -0.00078 0.00181 0.00083 C22 1 0.517500 0.056066 0.411607 11.00000 0.02442 0.01902 = 0.01753 0.00319 0.00781 -0.00018 AFIX 43 H22 5 0.492789 0.050980 0.459066 11.00000 -1.20000 AFIX 0 C23 1 0.520045 -0.013268 0.364344 11.00000 0.02324 0.01596 = 0.02716 0.00290 0.00604 -0.00071 AFIX 43 H23 5 0.498946 -0.066234 0.380194 11.00000 -1.20000 AFIX 0 C24 1 0.553387 -0.005427 0.293862 11.00000 0.02030 0.01848 = 0.02897 -0.00766 0.00993 -0.00177 AFIX 43 H24 5 0.555075 -0.052902 0.261437 11.00000 -1.20000 AFIX 0 C25 1 0.584172 0.071962 0.271070 11.00000 0.02242 0.02434 = 0.02333 -0.00683 0.01426 -0.00496 AFIX 43 H25 5 0.605279 0.077493 0.222239 11.00000 -1.20000 AFIX 0 C26 1 0.584555 0.141451 0.318657 11.00000 0.01687 0.01768 = 0.01929 -0.00130 0.00890 -0.00342 AFIX 43 H26 5 0.607249 0.194085 0.303260 11.00000 -1.20000 AFIX 0 C27 1 0.460157 0.266108 0.523680 11.00000 0.01225 0.01687 = 0.01101 0.00128 0.00231 0.00136 C28 1 0.366099 0.260083 0.559314 11.00000 0.01134 0.01908 = 0.01115 -0.00037 0.00172 0.00041 C29 1 0.333425 0.328110 0.598269 11.00000 0.01802 0.02001 = 0.02359 -0.00512 0.00758 -0.00220 AFIX 43 H29 5 0.372871 0.378386 0.603426 11.00000 -1.20000 AFIX 0 C30 1 0.244133 0.323174 0.629508 11.00000 0.01999 0.02331 = 0.02851 -0.00927 0.01106 -0.00037 AFIX 43 H30 5 0.222408 0.370349 0.655167 11.00000 -1.20000 AFIX 0 C31 1 0.185904 0.249764 0.623678 11.00000 0.01266 0.02667 = 0.01558 -0.00191 0.00469 -0.00107 C32 1 0.219323 0.180389 0.587442 11.00000 0.01432 0.02045 = 0.01545 -0.00106 0.00347 -0.00270 AFIX 43 H32 5 0.181595 0.129376 0.584677 11.00000 -1.20000 AFIX 0 C33 1 0.308326 0.186107 0.555258 11.00000 0.01538 0.01793 = 0.01422 -0.00081 0.00416 0.00158 AFIX 43 H33 5 0.330293 0.138743 0.529998 11.00000 -1.20000 AFIX 0 C34 1 0.025701 0.184691 0.636512 11.00000 0.01488 0.03759 = 0.02265 -0.00176 0.00637 -0.00578 AFIX 137 H34A 5 0.006273 0.178408 0.579418 11.00000 -1.50000 H34B 5 -0.037036 0.196671 0.657372 11.00000 -1.50000 H34C 5 0.057966 0.132886 0.659791 11.00000 -1.50000 AFIX 66 PART 1 21.00 C35 1 0.671307 0.409649 0.555609 21.00000 0.01348 0.01912 = 0.02189 -0.00245 0.00533 -0.00063 C36 1 0.659308 0.491243 0.528026 21.00000 0.04367 0.02102 = 0.02904 -0.00042 0.00100 0.00310 AFIX 43 H36 5 0.608161 0.503880 0.482366 21.00000 -1.20000 AFIX 65 C37 1 0.722144 0.554348 0.567251 21.00000 0.02470 0.01566 = 0.01916 -0.00183 0.01346 0.00744 AFIX 43 H37 5 0.713942 0.610114 0.548399 21.00000 -1.20000 AFIX 65 C38 1 0.796979 0.535859 0.634059 21.00000 0.02163 0.01981 = 0.02176 -0.00191 0.01035 -0.00070 AFIX 43 H38 5 0.839924 0.578989 0.660868 21.00000 -1.20000 AFIX 65 C39 1 0.808980 0.454265 0.661643 21.00000 0.01109 0.02365 = 0.03367 0.00639 -0.00558 -0.00423 AFIX 43 H39 5 0.860127 0.441629 0.707303 21.00000 -1.20000 AFIX 65 C40 1 0.746145 0.391160 0.622419 21.00000 0.01701 0.01984 = 0.03823 0.01120 -0.00417 -0.00995 AFIX 43 H40 5 0.754346 0.335394 0.641271 21.00000 -1.20000 AFIX 66 PART 2 31.000 C35' 1 0.674669 0.410065 0.557352 31.00000 0.01504 0.00815 = 0.02061 -0.00633 0.00387 -0.00817 C36' 1 0.689621 0.484504 0.520086 31.00000 0.03977 0.02021 = 0.02001 0.00475 -0.00692 -0.00913 AFIX 43 H36' 5 0.655465 0.493451 0.467122 31.00000 -1.20000 AFIX 65 C37' 1 0.754547 0.545853 0.560315 31.00000 0.04304 0.01586 = 0.03059 0.00144 -0.00370 -0.00805 AFIX 43 H37' 5 0.764766 0.596728 0.534845 31.00000 -1.20000 AFIX 65 C38' 1 0.804522 0.532762 0.637810 31.00000 0.02999 0.02652 = 0.02808 -0.00503 -0.00420 -0.00996 AFIX 43 H38' 5 0.848896 0.574692 0.665305 31.00000 -1.20000 AFIX 65 C39' 1 0.789571 0.458324 0.675078 31.00000 0.01751 0.02612 = 0.01890 -0.00557 0.00741 -0.00144 AFIX 43 H39' 5 0.823727 0.449378 0.728042 31.00000 -1.20000 AFIX 65 C40' 1 0.724645 0.396974 0.634850 31.00000 0.01591 0.02073 = 0.02062 -0.00128 0.00677 -0.00109 AFIX 43 H40' 5 0.714426 0.346099 0.660320 31.00000 -1.20000 AFIX 66 PART 3 41.000 C35" 1 0.671061 0.406899 0.550891 41.00000 0.01751 0.02306 = 0.01356 0.00337 0.00847 0.00331 C36" 1 0.632924 0.488052 0.540759 41.00000 0.02619 0.02078 = 0.02248 0.00007 0.00354 0.00204 AFIX 43 H36" 5 0.565759 0.498341 0.509097 41.00000 -1.20000 AFIX 65 C37" 1 0.693059 0.554150 0.576953 41.00000 0.03634 0.01870 = 0.02589 -0.00304 0.01702 -0.00042 AFIX 43 H37" 5 0.666994 0.609614 0.570028 41.00000 -1.20000 AFIX 65 C38" 1 0.791332 0.539096 0.623280 41.00000 0.03746 0.01655 = 0.03861 -0.00657 0.01257 -0.01504 AFIX 43 H38" 5 0.832431 0.584271 0.648016 41.00000 -1.20000 AFIX 65 C39" 1 0.829470 0.457943 0.633412 41.00000 0.02418 0.02711 = 0.05013 -0.00134 -0.00740 -0.00809 AFIX 43 H39" 5 0.896635 0.447655 0.665075 41.00000 -1.20000 AFIX 65 C40" 1 0.769336 0.391844 0.597219 41.00000 0.02077 0.01913 = 0.03947 0.00049 -0.00265 -0.00295 AFIX 43 H40" 5 0.795401 0.336380 0.604144 41.00000 -1.20000 AFIX 0 HKLF 4 REM mo_molan508_0m_a.res in P2(1)/n REM R1 = 0.0326 for 7643 Fo > 4sig(Fo) and 0.0446 for all 9224 data REM 537 parameters refined using 136 restraints END WGHT 0.0353 2.2701 REM Highest difference peak 0.454, deepest hole -0.366, 1-sigma level 0.052 Q1 1 0.9147 0.2601 0.3618 11.00000 0.05 0.45 Q2 1 0.7691 0.1387 0.5504 11.00000 0.05 0.33 Q3 1 1.0085 0.2714 0.2520 11.00000 0.05 0.32 Q4 1 1.1401 0.2353 0.3180 11.00000 0.05 0.31 Q5 1 0.4193 0.2591 0.5445 11.00000 0.05 0.31 Q6 1 0.9684 0.2721 0.3088 11.00000 0.05 0.31 Q7 1 0.5592 0.1388 0.3512 11.00000 0.05 0.31 Q8 1 0.1980 0.2174 0.5965 11.00000 0.05 0.31 Q9 1 0.5178 0.5045 0.2760 11.00000 0.05 0.31 Q10 1 1.0973 0.2696 0.2604 11.00000 0.05 0.31 Q11 1 0.5171 0.0996 0.3923 11.00000 0.05 0.30 Q12 1 0.8175 0.1031 0.5202 11.00000 0.05 0.30 Q13 1 1.0062 0.2449 0.3612 11.00000 0.05 0.29 Q14 1 1.1025 0.2287 0.3712 11.00000 0.05 0.28 Q15 1 0.5214 0.4564 0.3246 11.00000 0.05 0.27 Q16 1 0.6677 0.4204 0.2957 11.00000 0.05 0.27 Q17 1 0.5334 -0.0042 0.3298 11.00000 0.05 0.27 Q18 1 0.6834 0.3745 0.3572 11.00000 0.05 0.26 Q19 1 0.7456 0.0379 0.6132 11.00000 0.05 0.26 Q20 1 0.2750 0.1747 0.5868 11.00000 0.05 0.25 ; _shelx_res_checksum 142 _shelx_hkl_file ; 2 0 0 221.58 5.90 2 0 0 221.78 5.90 2 0 0 240.08 6.00 2 0 0 229.98 5.90 -2 0 0 228.18 5.90 -2 0 0 233.98 5.90 -2 0 0 229.68 5.90 -2 0 0 229.48 5.90 3 0 0 -0.40 0.30 -3 0 0 -0.70 0.40 -3 0 0 -0.50 0.40 -3 0 0 -0.30 0.30 -3 0 0 -0.40 0.30 3 0 0 -0.80 0.30 3 0 0 -0.50 0.40 3 0 0 -0.80 0.30 -4 0 0 333.67 8.70 -4 0 0 340.17 8.80 4 0 0 325.47 8.70 -4 0 0 334.27 8.70 4 0 0 329.07 8.70 4 0 0 328.97 8.70 -4 0 0 333.47 8.70 4 0 0 337.27 8.70 -5 0 0 0.00 0.40 5 0 0 -0.20 0.40 5 0 0 -0.30 0.40 -5 0 0 -0.20 0.40 -5 0 0 -0.10 0.40 5 0 0 -0.40 0.30 5 0 0 -0.10 0.40 -5 0 0 -0.50 0.40 6 0 0 547.25 14.30 6 0 0 571.84 14.40 6 0 0 541.05 14.40 -6 0 0 555.34 14.40 -6 0 0 557.04 14.30 -6 0 0 548.25 14.30 6 0 0 546.15 14.30 7 0 0 0.00 0.70 -7 0 0 0.30 0.50 7 0 0 0.20 0.60 -7 0 0 0.50 0.50 7 0 0 -0.60 0.50 -7 0 0 -0.20 0.60 7 0 0 0.20 0.50 -7 0 0 0.10 0.60 -8 0 0 111.99 3.90 -8 0 0 107.19 3.90 8 0 0 112.69 3.90 8 0 0 112.79 3.70 8 0 0 113.69 3.90 8 0 0 117.49 3.80 -8 0 0 112.49 3.70 -8 0 0 116.19 3.80 -9 0 0 -0.40 0.60 -9 0 0 0.90 0.70 9 0 0 0.00 0.70 9 0 0 -0.20 0.60 -9 0 0 0.10 0.70 -9 0 0 0.00 0.80 9 0 0 -0.10 0.80 9 0 0 0.30 0.80 10 0 0 277.37 8.10 -10 0 0 275.57 8.10 -10 0 0 254.27 8.00 10 0 0 270.37 8.10 10 0 0 263.87 7.80 10 0 0 258.87 7.80 -10 0 0 272.27 7.80 -10 0 0 267.37 7.80 -11 0 0 0.40 0.90 11 0 0 -0.30 1.00 -11 0 0 0.30 1.20 11 0 0 0.90 0.80 11 0 0 1.40 1.70 -11 0 0 1.00 0.90 11 0 0 0.80 0.80 -11 0 0 -1.00 0.90 -12 0 0 1.70 1.20 12 0 0 4.80 1.60 -12 0 0 6.80 1.50 -12 0 0 6.90 1.40 12 0 0 6.40 1.50 13 0 0 1.90 1.10 -13 0 0 0.70 1.50 13 0 0 0.10 1.50 13 0 0 0.20 1.10 -13 0 0 -0.10 1.20 -14 0 0 10.80 1.70 14 0 0 13.90 1.90 -14 0 0 11.20 1.90 -14 0 0 9.90 1.80 14 0 0 10.70 2.00 14 0 0 11.80 2.10 -14 0 0 9.80 2.00 14 0 0 9.50 1.90 15 0 0 1.80 2.20 -15 0 0 0.90 1.60 -15 0 0 -1.00 1.80 15 0 0 0.00 1.90 15 0 0 0.60 1.50 -15 0 0 -0.10 1.90 15 0 0 -0.40 1.50 -15 0 0 -1.70 1.90 16 0 0 90.49 5.30 16 0 0 98.49 5.80 -16 0 0 84.99 5.20 -16 0 0 93.49 4.90 -16 0 0 96.99 5.50 16 0 0 88.19 4.80 -16 0 0 95.19 6.10 17 0 0 1.60 2.40 17 0 0 -3.70 2.50 -17 0 0 -2.20 2.50 -17 0 0 -4.00 2.30 -2 -1 0 748.63 18.00 2 -1 0 715.73 18.00 2 -1 0 702.83 17.90 -2 -1 0 729.53 17.90 -2 -1 0 706.13 17.90 2 -1 0 724.73 17.90 -2 -1 0 737.93 18.00 2 -1 0 720.73 18.00 2 1 0 721.13 17.90 2 1 0 713.83 17.90 -2 1 0 709.53 18.00 -2 1 0 716.23 17.90 -2 1 0 703.83 17.90 -2 1 0 718.73 18.00 -3 -1 0 1063.49 26.10 3 -1 0 1027.80 26.00 -3 -1 0 1032.30 26.10 -3 -1 0 1065.59 26.00 -3 -1 0 1056.89 26.00 3 -1 0 1055.79 26.00 3 -1 0 1029.50 26.00 3 -1 0 1029.70 26.00 -3 1 0 1076.29 26.10 3 1 0 1041.30 26.00 -3 1 0 1038.10 26.00 3 1 0 1035.60 26.10 -3 1 0 1049.20 26.00 3 1 0 1010.50 26.10 -3 1 0 1022.60 26.00 -4 -1 0 2.30 0.40 4 -1 0 3.10 0.40 4 -1 0 3.00 0.50 4 -1 0 2.70 0.40 -4 -1 0 3.50 0.50 -4 -1 0 2.80 0.40 -4 -1 0 3.60 0.50 4 -1 0 4.10 0.60 -4 1 0 3.40 0.50 4 1 0 1.90 0.40 4 1 0 3.40 0.50 -4 1 0 3.10 0.40 -4 1 0 2.50 0.50 4 1 0 3.00 0.50 -4 1 0 3.10 0.50 4 1 0 3.50 0.50 -5 -1 0 97.89 3.10 5 -1 0 96.89 3.10 5 -1 0 93.69 3.00 -5 -1 0 97.89 3.00 5 -1 0 97.29 3.00 5 -1 0 96.69 3.10 -5 -1 0 97.79 3.10 -5 1 0 97.49 3.00 5 1 0 98.19 3.10 -5 1 0 97.09 3.00 -5 1 0 102.09 3.10 -5 1 0 100.79 3.10 5 1 0 99.59 3.10 5 1 0 94.59 3.00 5 1 0 97.59 3.00 6 -1 0 27.60 1.40 6 -1 0 28.40 1.60 -6 -1 0 29.50 1.60 -6 -1 0 31.40 1.50 6 -1 0 30.00 1.50 6 -1 0 28.80 1.50 -6 -1 0 29.60 1.50 6 1 0 29.70 1.60 6 1 0 29.10 1.50 -6 1 0 30.10 1.50 6 1 0 29.40 1.50 -6 1 0 28.50 1.60 6 1 0 28.30 1.60 -6 1 0 30.90 1.60 -6 1 0 29.90 1.50 -7 -1 0 141.19 4.30 7 -1 0 135.69 4.30 7 -1 0 138.69 4.30 7 -1 0 136.39 4.40 -7 -1 0 141.49 4.40 7 -1 0 145.39 4.40 -7 -1 0 140.19 4.40 7 1 0 138.19 4.40 -7 1 0 140.29 4.30 7 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-0.40 1.00 -11 -1 0 -0.80 0.90 -11 -1 0 0.70 0.90 11 -1 0 -0.40 0.70 -11 1 0 -0.50 0.90 11 1 0 -0.20 0.70 11 1 0 -0.50 1.10 11 1 0 -0.10 1.10 -11 1 0 0.20 1.00 -11 1 0 -0.20 1.10 -11 1 0 0.40 0.80 11 1 0 -0.40 0.80 -12 -1 0 19.80 2.60 -12 -1 0 23.50 2.30 12 -1 0 18.90 1.90 12 -1 0 23.40 2.60 -12 -1 0 17.40 2.00 -12 1 0 14.50 2.40 -12 1 0 24.50 2.60 -12 1 0 25.60 2.40 12 1 0 21.70 2.10 12 1 0 20.10 2.40 -12 1 0 17.60 1.90 12 1 0 22.40 2.70 -13 -1 0 0.40 1.10 13 -1 0 -0.50 1.00 -13 -1 0 0.80 1.60 13 -1 0 0.60 1.20 -13 -1 0 1.70 1.50 -13 -1 0 0.10 1.20 13 -1 0 2.20 1.40 -13 1 0 0.70 1.30 13 1 0 -0.40 1.40 13 1 0 0.90 1.00 13 1 0 0.70 1.20 -13 1 0 0.60 1.10 -14 -1 0 99.09 5.10 -14 -1 0 104.99 4.60 -14 -1 0 106.89 4.90 14 -1 0 101.39 4.80 14 -1 0 102.99 5.10 -14 -1 0 95.19 4.60 14 -1 0 100.59 4.80 -14 1 0 102.89 4.80 -14 1 0 96.79 5.00 14 1 0 99.39 4.50 14 1 0 100.19 5.10 14 1 0 97.79 4.80 -14 1 0 101.89 4.70 -14 1 0 101.29 4.50 14 1 0 97.99 4.70 -15 -1 0 7.00 2.10 -15 -1 0 5.90 1.80 15 -1 0 0.90 1.60 15 -1 0 6.20 2.10 15 -1 0 4.70 1.90 -15 -1 0 6.00 2.20 -15 -1 0 6.40 1.90 15 -1 0 6.50 2.20 15 1 0 4.00 1.60 15 1 0 4.00 2.00 -15 1 0 2.80 2.00 -15 1 0 3.80 1.70 -15 1 0 6.20 2.00 15 1 0 5.70 2.10 -15 1 0 6.70 2.10 15 1 0 3.20 1.90 -16 -1 0 23.30 2.60 16 -1 0 30.70 3.80 -16 -1 0 26.80 3.20 -16 -1 0 22.20 2.70 16 -1 0 32.90 3.70 16 -1 0 22.30 2.50 -16 -1 0 27.00 3.60 16 1 0 27.40 3.10 16 1 0 23.80 3.20 -16 1 0 21.80 2.80 -16 1 0 27.30 2.90 -16 1 0 24.10 3.00 16 1 0 30.50 3.40 -17 -1 0 4.80 2.40 17 -1 0 0.00 2.60 17 -1 0 0.30 2.50 -17 -1 0 0.40 2.60 17 1 0 0.50 2.40 -17 1 0 1.20 2.50 17 1 0 1.60 2.60 -17 1 0 1.70 2.40 -1 -2 0 23.40 0.90 -1 -2 0 22.90 1.00 1 -2 0 21.60 0.90 -1 2 0 23.10 0.90 1 2 0 22.10 0.90 -1 2 0 22.50 0.90 -1 2 0 23.20 0.90 -1 2 0 23.50 0.80 2 -2 0 114.59 3.10 2 -2 0 116.49 3.10 -2 -2 0 118.59 3.20 -2 -2 0 115.39 3.10 2 -2 0 113.59 3.10 2 -2 0 112.99 3.10 -2 -2 0 114.99 3.10 2 2 0 108.69 3.20 -2 2 0 116.69 3.10 2 2 0 113.69 3.20 -2 2 0 115.19 3.10 -2 2 0 115.29 3.10 2 2 0 114.29 3.10 -2 2 0 110.49 3.10 2 2 0 113.99 3.10 3 -2 0 1.90 0.40 3 -2 0 2.20 0.50 -3 -2 0 1.90 0.50 3 -2 0 2.00 0.40 3 -2 0 2.60 0.50 -3 -2 0 2.50 0.50 -3 -2 0 1.10 0.40 -3 -2 0 2.40 0.50 3 2 0 1.90 0.50 3 2 0 1.30 0.40 3 2 0 2.80 0.50 -3 2 0 2.80 0.50 3 2 0 1.90 0.40 -3 2 0 2.00 0.40 -3 2 0 1.30 0.40 -3 2 0 2.30 0.40 -4 -2 0 270.37 7.10 4 -2 0 262.47 7.10 -4 -2 0 278.87 7.20 4 -2 0 265.17 7.20 -4 -2 0 275.87 7.20 4 -2 0 268.87 7.10 -4 -2 0 265.87 7.10 4 -2 0 269.57 7.20 4 2 0 267.77 7.10 -4 2 0 266.27 7.10 4 2 0 270.47 7.20 4 2 0 270.57 7.10 4 2 0 256.87 7.20 -4 2 0 270.47 7.20 -4 2 0 274.97 7.20 -4 2 0 268.17 7.10 -5 -2 0 152.08 4.40 5 -2 0 145.09 4.30 -5 -2 0 149.69 4.40 -5 -2 0 147.09 4.30 5 -2 0 155.08 4.40 -5 -2 0 150.78 4.30 5 -2 0 146.09 4.30 5 -2 0 151.78 4.40 -5 2 0 151.68 4.30 -5 2 0 150.48 4.40 -5 2 0 148.09 4.40 -5 2 0 155.68 4.30 5 2 0 152.18 4.50 5 2 0 147.69 4.30 5 2 0 147.89 4.40 5 2 0 150.78 4.30 6 -2 0 23.00 1.30 -6 -2 0 23.20 1.30 6 -2 0 21.70 1.30 6 -2 0 23.30 1.40 6 -2 0 20.10 1.30 -6 -2 0 23.50 1.40 -6 -2 0 21.70 1.40 -6 -2 0 23.20 1.30 6 2 0 24.00 1.40 6 2 0 22.10 1.30 6 2 0 23.60 1.40 6 2 0 21.50 1.50 -6 2 0 21.60 1.30 -6 2 0 23.20 1.30 -6 2 0 23.30 1.40 -6 2 0 23.80 1.40 7 -2 0 191.68 5.50 -7 -2 0 192.88 5.60 7 -2 0 194.38 5.60 -7 -2 0 188.08 5.60 7 -2 0 190.68 5.70 -7 -2 0 194.38 5.70 7 -2 0 191.78 5.70 -7 -2 0 185.38 5.70 7 2 0 196.18 5.70 -7 2 0 179.48 5.60 7 2 0 189.98 5.60 7 2 0 185.78 5.50 -7 2 0 198.58 5.70 -7 2 0 192.88 5.50 -7 2 0 189.68 5.50 7 2 0 188.28 5.70 -8 -2 0 2.80 0.90 -8 -2 0 2.40 0.80 8 -2 0 3.00 0.80 -8 -2 0 1.70 0.80 8 -2 0 1.00 0.60 8 -2 0 0.90 0.70 -8 -2 0 2.50 0.70 8 -2 0 2.00 0.80 -8 2 0 2.50 0.90 8 2 0 1.00 0.70 8 2 0 1.70 0.70 -8 2 0 0.90 0.60 -8 2 0 1.60 0.80 8 2 0 1.40 0.70 8 2 0 1.00 0.70 -8 2 0 2.50 0.70 9 -2 0 1.20 0.90 -9 -2 0 1.70 0.90 -9 -2 0 3.00 0.90 -9 -2 0 0.80 0.70 -9 -2 0 3.30 1.00 9 -2 0 1.50 0.80 9 -2 0 1.90 0.70 9 -2 0 1.80 0.80 9 2 0 0.90 0.80 9 2 0 2.10 0.80 9 2 0 1.90 1.00 -9 2 0 0.90 0.70 -9 2 0 3.60 1.00 -9 2 0 0.70 0.80 9 2 0 2.00 0.80 -9 2 0 2.90 0.90 -10 -2 0 202.78 6.30 10 -2 0 211.38 6.60 -10 -2 0 209.78 6.60 10 -2 0 201.58 6.30 -10 -2 0 204.28 6.50 10 -2 0 201.38 6.50 10 -2 0 201.58 6.40 -10 -2 0 219.98 6.40 -10 2 0 198.78 6.50 -10 2 0 204.28 6.30 -10 2 0 207.78 6.30 10 2 0 197.18 6.50 10 2 0 206.68 6.30 -10 2 0 209.38 6.50 10 2 0 206.48 6.40 10 2 0 201.08 6.50 -11 -2 0 28.70 2.50 11 -2 0 29.20 2.00 -11 -2 0 26.90 2.30 11 -2 0 27.60 2.50 -11 -2 0 27.40 2.10 -11 -2 0 26.40 2.20 11 -2 0 25.80 2.20 11 2 0 27.80 2.30 -11 2 0 25.80 2.20 11 2 0 25.00 2.30 11 2 0 29.50 2.10 -11 2 0 24.50 2.30 -11 2 0 28.10 2.10 11 2 0 31.10 3.10 -11 2 0 23.80 2.50 -12 -2 0 2.70 1.20 -12 -2 0 -0.70 1.00 12 -2 0 -0.20 1.10 -12 -2 0 1.20 1.10 12 -2 0 -0.80 0.80 12 -2 0 0.00 1.30 -12 -2 0 1.70 1.20 -12 2 0 1.50 1.10 12 2 0 -1.30 1.10 12 2 0 1.00 1.00 -12 2 0 -1.00 1.20 -12 2 0 1.70 1.10 12 2 0 0.70 1.30 13 -2 0 1.10 1.30 13 -2 0 0.00 1.30 -13 -2 0 1.60 1.30 -13 -2 0 -0.90 1.50 13 -2 0 0.40 1.00 -13 -2 0 -0.30 1.30 -13 -2 0 0.90 1.20 13 2 0 1.00 1.10 -13 2 0 -0.60 1.00 13 2 0 -0.10 1.10 13 2 0 -0.10 2.00 13 2 0 1.70 1.50 -13 2 0 -0.80 1.30 -13 2 0 1.00 1.60 14 -2 0 4.70 1.60 -14 -2 0 7.30 1.70 14 -2 0 5.10 1.80 14 -2 0 5.40 1.50 -14 -2 0 10.00 1.80 -14 -2 0 5.40 1.70 -14 -2 0 3.90 1.90 14 -2 0 8.00 2.20 14 2 0 6.60 1.80 14 2 0 7.00 2.00 14 2 0 9.90 2.20 -14 2 0 8.30 1.80 14 2 0 4.50 1.40 -14 2 0 5.90 2.00 -14 2 0 5.80 1.80 -14 2 0 4.40 1.60 -15 -2 0 3.80 2.10 15 -2 0 1.00 1.40 -15 -2 0 -0.70 1.70 -15 -2 0 0.90 1.60 15 -2 0 3.10 1.70 15 -2 0 0.50 1.80 -15 -2 0 2.80 2.00 15 -2 0 1.40 1.90 -15 2 0 3.30 1.80 -15 2 0 2.50 1.70 15 2 0 1.00 1.50 15 2 0 1.10 1.80 -15 2 0 1.40 2.00 15 2 0 3.20 1.80 15 2 0 2.40 2.10 -15 2 0 1.20 1.80 16 -2 0 62.09 4.50 16 -2 0 62.59 5.20 -16 -2 0 67.19 4.90 -16 -2 0 57.19 5.60 -16 -2 0 65.99 4.90 -16 -2 0 54.79 4.10 16 2 0 60.99 5.40 16 2 0 55.69 4.10 -16 2 0 62.59 4.70 -16 2 0 63.29 4.70 -16 2 0 59.39 4.20 16 2 0 66.69 4.80 -17 -2 0 8.20 2.80 17 -2 0 7.10 2.60 -17 -2 0 12.00 2.60 17 -2 0 3.90 5.00 17 2 0 11.50 4.20 17 2 0 9.90 2.90 -17 2 0 9.70 2.70 -17 2 0 9.70 2.90 0 -3 0 -0.10 0.30 0 -3 0 -0.20 0.20 0 -3 0 -0.10 0.20 0 -3 0 -0.20 0.20 0 3 0 0.10 0.30 0 3 0 -0.20 0.20 0 3 0 0.00 0.30 0 3 0 -0.20 0.20 1 -3 0 86.59 2.40 -1 -3 0 86.49 2.50 1 -3 0 86.29 2.40 -1 -3 0 86.39 2.40 1 -3 0 86.09 2.40 -1 -3 0 84.09 2.40 -1 3 0 85.79 2.40 1 3 0 88.59 2.50 -1 3 0 82.19 2.40 1 3 0 84.59 2.40 -1 3 0 82.99 2.40 -1 3 0 86.59 2.40 1 3 0 87.59 2.40 2 -3 0 12.70 0.70 -2 -3 0 13.80 0.80 2 -3 0 12.80 0.80 2 -3 0 12.70 0.80 2 -3 0 14.50 0.80 -2 -3 0 14.40 0.80 -2 -3 0 12.60 0.80 -2 3 0 14.30 0.80 -2 3 0 13.70 0.70 2 3 0 13.90 0.80 2 3 0 13.20 0.80 -2 3 0 13.60 0.70 -2 3 0 13.30 0.80 2 3 0 12.80 0.80 -3 -3 0 0.30 0.30 3 -3 0 0.00 0.30 -3 -3 0 0.40 0.40 -3 -3 0 0.20 0.40 3 -3 0 -0.10 0.30 3 -3 0 0.40 0.40 -3 -3 0 0.40 0.30 3 -3 0 0.80 0.40 -3 3 0 0.10 0.40 -3 3 0 0.30 0.30 3 3 0 0.20 0.30 3 3 0 0.00 0.40 3 3 0 0.20 0.30 -3 3 0 0.40 0.30 -3 3 0 0.50 0.40 3 3 0 0.10 0.30 4 -3 0 161.88 4.50 -4 -3 0 167.88 4.60 -4 -3 0 164.08 4.60 4 -3 0 165.98 4.60 4 -3 0 157.78 4.50 -4 -3 0 163.58 4.50 4 -3 0 158.58 4.60 -4 -3 0 159.08 4.50 4 3 0 158.48 4.60 4 3 0 164.68 4.60 -4 3 0 163.48 4.50 4 3 0 161.18 4.50 -4 3 0 161.08 4.60 -4 3 0 161.48 4.50 -4 3 0 164.48 4.60 5 -3 0 9.20 0.90 -5 -3 0 9.00 1.00 5 -3 0 8.30 0.90 5 -3 0 9.20 1.00 -5 -3 0 8.60 1.10 5 -3 0 8.50 0.90 -5 -3 0 8.00 0.90 -5 -3 0 9.80 1.00 -5 3 0 8.50 1.00 -5 3 0 8.70 1.00 -5 3 0 9.40 0.90 5 3 0 8.40 1.00 5 3 0 8.20 0.90 -5 3 0 9.80 0.90 5 3 0 8.50 1.00 -6 -3 0 15.20 1.20 6 -3 0 16.30 1.20 6 -3 0 14.90 1.20 -6 -3 0 16.70 1.20 -6 -3 0 16.40 1.30 -6 -3 0 16.00 1.30 6 -3 0 15.90 1.20 6 -3 0 15.80 1.10 6 3 0 15.10 1.20 6 3 0 15.20 1.30 -6 3 0 15.70 1.20 -6 3 0 16.70 1.20 6 3 0 16.60 1.20 6 3 0 15.30 1.30 -6 3 0 16.10 1.30 -6 3 0 18.30 1.30 7 -3 0 37.50 1.90 -7 -3 0 38.90 2.00 -7 -3 0 37.20 1.80 -7 -3 0 35.70 1.80 7 -3 0 37.70 1.80 7 -3 0 37.40 2.00 7 -3 0 37.80 1.90 -7 -3 0 37.70 2.00 -7 3 0 38.50 1.80 -7 3 0 38.00 1.90 7 3 0 37.90 2.00 7 3 0 38.90 1.80 -7 3 0 39.70 1.80 7 3 0 33.80 1.80 7 3 0 38.70 2.00 -7 3 0 35.90 1.90 8 -3 0 5.20 0.90 8 -3 0 5.20 0.90 -8 -3 0 6.00 0.90 -8 -3 0 5.60 1.00 -8 -3 0 4.60 1.00 8 -3 0 4.30 0.90 -8 -3 0 5.10 0.90 8 -3 0 4.40 0.90 -8 3 0 4.20 0.80 8 3 0 5.30 1.00 8 3 0 4.90 0.90 -8 3 0 5.20 0.80 8 3 0 2.90 0.80 -8 3 0 5.10 1.00 8 3 0 3.60 0.70 -8 3 0 4.70 0.90 9 -3 0 0.40 0.70 -9 -3 0 2.20 0.90 9 -3 0 -1.60 0.50 9 -3 0 0.50 0.80 9 -3 0 0.70 0.80 -9 -3 0 1.80 1.00 -9 -3 0 0.40 0.70 -9 -3 0 1.80 0.90 -9 3 0 0.30 0.80 9 3 0 0.40 0.70 9 3 0 0.10 0.80 9 3 0 1.40 0.80 -9 3 0 0.20 0.70 -9 3 0 0.50 0.90 -9 3 0 1.10 0.80 9 3 0 1.10 0.90 -10 -3 0 93.89 3.80 -10 -3 0 86.89 3.60 10 -3 0 90.69 3.70 10 -3 0 89.49 3.70 -10 -3 0 91.79 3.80 -10 -3 0 92.09 3.60 10 -3 0 91.39 3.50 10 -3 0 91.49 3.80 -10 3 0 88.79 3.50 10 3 0 88.89 3.70 -10 3 0 92.59 3.50 -10 3 0 92.59 3.80 10 3 0 96.39 3.80 -10 3 0 89.19 3.70 10 3 0 91.69 3.50 10 3 0 85.49 3.80 11 -3 0 -0.30 1.00 11 -3 0 -1.10 1.00 -11 -3 0 2.40 1.20 -11 -3 0 3.00 1.00 -11 -3 0 3.30 1.30 11 -3 0 2.90 1.30 11 -3 0 2.70 1.00 -11 -3 0 2.40 1.30 -11 3 0 1.30 1.00 -11 3 0 0.70 1.20 11 3 0 1.30 1.10 11 3 0 2.50 1.20 -11 3 0 2.80 1.00 11 3 0 1.50 0.90 -11 3 0 2.50 1.10 11 3 0 3.90 1.60 -12 -3 0 7.20 1.60 12 -3 0 8.00 1.50 12 -3 0 7.20 1.40 12 -3 0 7.90 1.40 -12 -3 0 7.60 1.40 -12 -3 0 7.30 1.30 12 3 0 7.80 1.40 -12 3 0 7.30 1.40 -12 3 0 9.00 1.60 -12 3 0 7.70 1.40 12 3 0 9.30 1.80 12 3 0 9.20 1.60 -13 -3 0 24.20 2.80 13 -3 0 21.60 2.70 -13 -3 0 26.60 2.50 13 -3 0 28.40 2.50 13 -3 0 26.50 3.00 -13 -3 0 25.00 2.70 -13 -3 0 28.50 3.10 -13 3 0 19.00 2.20 13 3 0 24.50 2.80 -13 3 0 24.00 2.90 13 3 0 23.50 3.00 13 3 0 27.20 2.80 -13 3 0 28.80 2.50 13 3 0 26.10 2.60 -14 -3 0 44.60 3.60 -14 -3 0 44.80 3.30 14 -3 0 44.60 3.50 -14 -3 0 41.10 3.80 -14 -3 0 43.20 3.40 14 -3 0 43.20 3.60 14 -3 0 39.30 3.80 14 -3 0 43.10 3.10 -14 3 0 53.39 3.50 14 3 0 40.10 4.00 -14 3 0 39.60 3.50 14 3 0 45.70 3.60 14 3 0 42.60 3.20 14 3 0 38.80 3.50 -14 3 0 43.00 3.20 -14 3 0 50.79 3.80 -15 -3 0 21.50 2.70 -15 -3 0 18.70 2.30 15 -3 0 12.00 1.90 15 -3 0 14.10 2.40 15 -3 0 18.60 2.40 15 -3 0 19.40 2.70 -15 -3 0 18.00 2.50 -15 -3 0 22.50 2.70 -15 3 0 21.90 2.80 -15 3 0 13.50 2.20 15 3 0 17.10 2.20 15 3 0 16.70 2.50 -15 3 0 20.60 2.70 15 3 0 13.30 2.30 -15 3 0 16.30 2.20 15 3 0 17.00 2.70 -16 -3 0 9.20 3.00 16 -3 0 9.40 1.90 16 -3 0 13.50 2.90 -16 -3 0 9.40 2.40 16 -3 0 7.70 2.10 -16 -3 0 12.30 2.20 -16 3 0 10.90 2.30 16 3 0 9.20 2.10 -16 3 0 8.60 2.40 16 3 0 12.80 2.70 -16 3 0 5.30 2.20 16 3 0 9.60 2.70 -17 -3 0 -2.60 2.20 17 -3 0 -2.20 3.00 -17 -3 0 4.20 2.70 -17 3 0 -0.40 2.60 -17 3 0 -1.50 2.40 17 3 0 -1.00 2.70 0 -4 0 4338.57 106.09 0 -4 0 4226.68 105.89 0 -4 0 4270.47 106.09 0 -4 0 4230.98 106.19 0 4 0 4116.29 106.29 0 4 0 4233.18 105.89 0 4 0 4198.18 106.29 0 4 0 4311.27 105.99 1 -4 0 207.78 5.50 1 -4 0 216.28 5.50 1 -4 0 213.18 5.60 -1 -4 0 204.18 5.60 1 -4 0 201.68 5.50 -1 -4 0 206.38 5.50 -1 -4 0 209.78 5.60 -1 -4 0 209.88 5.50 1 4 0 208.98 5.50 1 4 0 215.58 5.60 -1 4 0 208.08 5.50 1 4 0 211.18 5.50 -1 4 0 207.98 5.50 -1 4 0 205.28 5.50 -1 4 0 214.58 5.50 1 4 0 206.58 5.60 -2 -4 0 66.59 2.20 2 -4 0 64.89 2.10 2 -4 0 68.69 2.10 2 -4 0 67.29 2.10 -2 -4 0 68.19 2.10 2 -4 0 65.99 2.10 -2 -4 0 66.69 2.10 -2 -4 0 67.69 2.10 -2 4 0 65.19 2.10 2 4 0 64.59 2.10 2 4 0 66.89 2.20 2 4 0 67.69 2.10 2 4 0 68.49 2.20 -2 4 0 65.69 2.00 -2 4 0 65.39 2.00 -2 4 0 66.39 2.10 -3 -4 0 0.90 0.40 -3 -4 0 1.50 0.50 -3 -4 0 1.20 0.40 -3 -4 0 1.20 0.40 3 -4 0 1.80 0.50 3 -4 0 1.50 0.40 3 -4 0 1.30 0.40 3 -4 0 0.70 0.40 3 4 0 1.40 0.40 -3 4 0 1.00 0.40 -3 4 0 1.60 0.40 3 4 0 2.10 0.50 3 4 0 1.30 0.40 3 4 0 0.80 0.40 -3 4 0 1.30 0.40 -3 4 0 1.50 0.50 -4 -4 0 180.68 5.30 -4 -4 0 181.08 5.20 4 -4 0 181.88 5.10 4 -4 0 181.18 5.10 -4 -4 0 187.88 5.20 4 -4 0 187.18 5.20 4 -4 0 188.28 5.20 -4 4 0 181.48 5.10 -4 4 0 189.28 5.10 4 4 0 183.78 5.20 4 4 0 192.38 5.30 -4 4 0 188.98 5.20 4 4 0 185.68 5.20 4 4 0 196.18 5.30 -4 4 0 185.28 5.20 5 -4 0 6.20 0.80 5 -4 0 6.70 0.80 -5 -4 0 5.90 0.80 -5 -4 0 5.60 0.70 -5 -4 0 6.00 0.80 5 -4 0 5.60 0.70 5 -4 0 3.80 0.60 -5 -4 0 4.70 0.70 5 4 0 4.60 0.70 5 4 0 5.40 0.80 -5 4 0 6.10 0.70 5 4 0 5.40 0.70 -5 4 0 5.10 0.70 5 4 0 6.40 0.80 -5 4 0 4.10 0.70 -5 4 0 5.60 0.70 -6 -4 0 484.15 12.70 -6 -4 0 537.45 13.00 6 -4 0 481.65 12.70 6 -4 0 469.85 12.80 -6 -4 0 481.75 12.70 6 -4 0 496.65 12.70 6 -4 0 483.45 12.80 -6 -4 0 505.85 12.90 6 4 0 453.85 12.80 6 4 0 466.25 12.80 -6 4 0 473.85 12.80 -6 4 0 485.35 12.70 -6 4 0 486.65 12.70 6 4 0 478.35 12.70 -6 4 0 482.35 12.80 6 4 0 490.05 12.70 -7 -4 0 125.49 4.00 -7 -4 0 122.49 4.10 7 -4 0 119.49 4.00 -7 -4 0 123.19 3.90 -7 -4 0 125.29 4.10 7 -4 0 117.89 4.00 7 -4 0 125.69 3.90 7 -4 0 124.19 4.00 7 4 0 125.39 4.10 -7 4 0 123.99 3.90 -7 4 0 115.89 4.00 -7 4 0 122.29 3.90 7 4 0 121.49 4.00 -7 4 0 121.99 4.10 7 4 0 122.69 4.10 7 4 0 122.29 3.90 -8 -4 0 31.30 1.80 -8 -4 0 30.90 2.00 8 -4 0 28.40 1.70 8 -4 0 27.40 1.90 -8 -4 0 28.20 1.80 -8 -4 0 30.00 1.90 8 -4 0 29.50 1.90 8 -4 0 28.50 1.80 8 4 0 27.50 1.90 8 4 0 29.50 1.80 -8 4 0 29.20 1.80 8 4 0 29.10 1.80 8 4 0 31.00 2.00 -8 4 0 31.00 1.80 -8 4 0 28.10 1.90 -8 4 0 28.20 1.90 9 -4 0 -0.80 0.70 -9 -4 0 0.00 0.80 -9 -4 0 1.10 0.90 9 -4 0 0.20 0.80 -9 -4 0 0.80 0.90 -9 -4 0 -0.60 0.60 9 -4 0 -0.10 0.70 9 -4 0 0.20 0.90 9 4 0 0.80 0.80 -9 4 0 1.40 0.90 9 4 0 -0.10 0.80 9 4 0 0.40 0.80 9 4 0 -0.20 0.70 -9 4 0 -0.20 0.70 -9 4 0 0.70 0.70 -9 4 0 0.20 0.80 -10 -4 0 119.69 4.20 10 -4 0 117.29 4.40 -10 -4 0 122.99 4.60 10 -4 0 120.19 4.20 -10 -4 0 120.09 4.50 10 -4 0 115.59 4.30 -10 4 0 120.69 4.20 10 4 0 117.09 4.20 10 4 0 117.29 4.50 10 4 0 112.99 4.50 -10 4 0 119.19 4.20 -10 4 0 116.99 4.40 10 4 0 99.69 5.60 -11 -4 0 41.40 2.70 11 -4 0 45.50 2.90 -11 -4 0 40.50 2.70 11 -4 0 39.90 2.60 -11 -4 0 42.70 3.00 -11 -4 0 40.20 2.50 11 -4 0 42.80 2.50 11 4 0 43.00 2.80 -11 4 0 43.90 2.90 -11 4 0 40.50 2.60 -11 4 0 42.60 2.70 11 4 0 38.80 2.50 -11 4 0 40.60 2.40 11 4 0 43.10 3.00 11 4 0 44.70 2.80 -12 -4 0 1.50 1.30 -12 -4 0 0.90 1.00 12 -4 0 0.40 1.30 12 -4 0 0.10 1.00 12 -4 0 -0.90 0.90 -12 4 0 0.30 1.10 -12 4 0 0.00 1.20 12 4 0 1.10 1.40 -12 4 0 0.40 1.10 12 4 0 0.50 1.00 -12 4 0 -0.80 1.90 12 4 0 2.20 1.90 13 -4 0 36.80 2.80 -13 -4 0 43.40 3.50 -13 -4 0 41.40 2.90 13 -4 0 43.00 3.50 13 -4 0 44.70 3.20 -13 -4 0 39.00 3.10 -13 -4 0 41.10 3.20 13 4 0 34.20 3.10 -13 4 0 41.70 2.90 13 4 0 38.90 3.20 -13 4 0 36.50 3.70 -13 4 0 40.30 3.40 13 4 0 43.00 3.60 13 4 0 39.40 2.90 -14 -4 0 -1.50 1.40 -14 -4 0 -0.60 1.50 14 -4 0 1.60 1.90 14 -4 0 0.80 1.60 -14 -4 0 2.20 1.60 14 -4 0 0.20 1.70 14 -4 0 1.20 1.30 -14 -4 0 1.00 1.90 -14 4 0 -1.20 1.30 14 4 0 1.20 1.60 -14 4 0 0.20 1.60 14 4 0 3.20 1.40 14 4 0 3.20 1.80 -14 4 0 -0.10 1.70 14 4 0 2.10 1.80 -14 4 0 -0.60 1.70 -15 -4 0 37.70 3.70 -15 -4 0 32.10 3.80 15 -4 0 34.10 4.20 -15 -4 0 31.20 3.40 -15 -4 0 26.20 2.90 15 -4 0 31.30 3.10 15 -4 0 31.20 3.60 15 -4 0 24.80 2.80 -15 4 0 27.60 3.10 -15 4 0 30.50 3.20 -15 4 0 30.70 3.70 15 4 0 23.00 2.50 -15 4 0 23.20 2.70 15 4 0 23.90 2.90 15 4 0 26.40 2.90 15 4 0 33.10 4.00 -16 -4 0 3.60 4.20 16 -4 0 1.10 2.00 16 -4 0 1.60 1.70 -16 -4 0 3.50 2.20 -16 -4 0 2.60 1.90 16 -4 0 7.30 2.90 -16 4 0 2.60 2.30 16 4 0 -1.00 2.50 16 4 0 5.50 2.30 -16 4 0 -0.10 2.40 -16 4 0 4.50 2.10 16 4 0 6.70 2.00 0 -5 0 0.10 0.30 0 -5 0 -0.40 0.30 0 -5 0 0.10 0.30 0 -5 0 -0.30 0.40 0 5 0 -0.40 0.30 0 5 0 -0.10 0.30 0 5 0 0.20 0.30 0 5 0 -0.20 0.30 1 -5 0 48.00 1.60 -1 -5 0 46.10 1.70 -1 -5 0 51.99 1.80 -1 -5 0 47.00 1.60 -1 -5 0 46.80 1.60 1 -5 0 48.70 1.60 1 -5 0 46.60 1.70 1 -5 0 46.20 1.70 1 5 0 49.20 1.70 -1 5 0 49.00 1.60 -1 5 0 47.50 1.60 1 5 0 46.30 1.70 1 5 0 48.10 1.60 -1 5 0 47.10 1.70 -1 5 0 45.30 1.70 1 5 0 47.50 1.70 -2 -5 0 24.70 1.20 -2 -5 0 23.90 1.10 -2 -5 0 24.20 1.10 2 -5 0 23.50 1.10 2 -5 0 22.70 1.10 2 -5 0 23.30 1.10 -2 5 0 24.70 1.20 -2 5 0 23.10 1.10 2 5 0 22.70 1.20 2 5 0 24.00 1.10 -2 5 0 24.80 1.10 -2 5 0 22.90 1.10 2 5 0 23.90 1.20 2 5 0 24.10 1.10 -3 -5 0 320.87 8.10 3 -5 0 302.57 8.00 3 -5 0 299.57 8.00 3 -5 0 299.87 8.00 -3 -5 0 291.87 8.10 3 -5 0 294.47 8.00 -3 -5 0 303.67 8.00 -3 -5 0 308.87 8.00 -3 5 0 296.07 8.00 3 5 0 302.57 8.10 -3 5 0 302.47 7.90 -3 5 0 299.17 8.00 3 5 0 305.37 8.00 -3 5 0 300.27 7.90 3 5 0 308.67 8.10 3 5 0 302.17 8.00 -4 -5 0 438.06 11.40 -4 -5 0 435.26 11.50 4 -5 0 454.05 11.50 4 -5 0 441.66 11.40 4 -5 0 430.46 11.40 -4 -5 0 436.66 11.40 4 -5 0 426.26 11.30 -4 -5 0 421.56 11.50 -4 5 0 433.06 11.30 -4 5 0 436.56 11.40 4 5 0 432.56 11.40 -4 5 0 436.46 11.40 -4 5 0 435.66 11.30 4 5 0 449.36 11.50 4 5 0 431.96 11.30 4 5 0 436.76 11.50 5 -5 0 10.20 1.10 -5 -5 0 11.00 1.20 5 -5 0 11.10 1.10 -5 -5 0 12.10 1.10 5 -5 0 12.60 1.00 5 -5 0 11.90 1.10 -5 -5 0 11.40 1.10 -5 -5 0 10.30 1.20 5 5 0 10.20 1.10 -5 5 0 12.30 1.10 5 5 0 11.20 1.00 -5 5 0 11.10 1.10 -5 5 0 9.70 1.10 -5 5 0 11.30 1.00 5 5 0 10.70 1.20 5 5 0 11.70 1.20 6 -5 0 2.80 0.70 6 -5 0 2.60 0.60 6 -5 0 2.40 0.60 -6 -5 0 3.60 0.70 -6 -5 0 2.90 0.80 -6 -5 0 2.80 0.70 -6 -5 0 4.50 0.90 6 -5 0 3.30 0.70 -6 5 0 3.10 0.60 6 5 0 4.40 0.80 -6 5 0 3.20 0.70 -6 5 0 4.10 0.80 6 5 0 3.10 0.70 -6 5 0 4.00 0.70 6 5 0 3.70 0.80 6 5 0 2.70 0.70 -7 -5 0 101.89 3.70 7 -5 0 103.49 3.60 -7 -5 0 106.49 3.60 -7 -5 0 106.09 3.60 7 -5 0 98.59 3.60 -7 -5 0 103.29 3.70 7 -5 0 104.69 3.50 7 -5 0 100.49 3.50 7 5 0 111.79 3.80 -7 5 0 102.89 3.40 7 5 0 109.89 3.70 -7 5 0 99.19 3.60 -7 5 0 104.29 3.60 7 5 0 104.59 3.50 -7 5 0 102.89 3.40 7 5 0 99.19 3.50 8 -5 0 0.20 0.60 -8 -5 0 0.90 0.70 -8 -5 0 1.10 0.80 8 -5 0 1.00 0.60 8 -5 0 0.50 0.70 8 -5 0 1.90 0.90 -8 -5 0 1.20 0.60 -8 -5 0 0.90 0.80 8 5 0 0.50 0.90 -8 5 0 0.50 0.70 -8 5 0 0.90 0.80 8 5 0 0.30 0.60 8 5 0 0.50 0.80 -8 5 0 0.30 0.80 8 5 0 2.30 0.80 -8 5 0 -0.20 0.70 -9 -5 0 9.30 1.20 9 -5 0 8.80 1.20 -9 -5 0 8.10 1.10 9 -5 0 8.50 1.00 -9 -5 0 13.20 1.70 9 -5 0 11.70 1.40 -9 -5 0 7.10 1.20 9 -5 0 7.90 1.10 9 5 0 9.40 1.20 9 5 0 7.50 1.20 9 5 0 9.60 1.30 9 5 0 9.50 1.20 -9 5 0 12.30 1.40 -9 5 0 10.00 1.20 -9 5 0 12.10 1.30 -9 5 0 10.00 1.20 -10 -5 0 137.89 4.90 -10 -5 0 135.69 4.70 10 -5 0 128.99 4.90 -10 -5 0 137.99 5.00 10 -5 0 134.39 4.70 10 -5 0 134.89 4.60 -10 -5 0 136.49 4.80 10 -5 0 131.39 4.80 -10 5 0 130.89 4.90 10 5 0 136.19 4.90 10 5 0 141.29 5.00 10 5 0 130.59 4.60 -10 5 0 133.39 4.60 10 5 0 119.49 5.40 -10 5 0 134.89 4.60 -10 5 0 130.39 4.80 -11 -5 0 2.50 1.10 -11 -5 0 0.20 1.20 11 -5 0 0.50 1.00 11 -5 0 -0.10 1.00 11 -5 0 0.50 1.00 11 -5 0 -0.40 1.10 -11 5 0 1.50 1.10 -11 5 0 -0.20 1.10 11 5 0 0.20 1.00 11 5 0 1.10 1.30 11 5 0 -0.30 1.20 -11 5 0 -0.10 0.80 -11 5 0 -1.50 1.20 11 5 0 1.40 1.00 12 -5 0 5.20 1.30 -12 -5 0 9.50 1.80 -12 -5 0 6.60 1.40 -12 -5 0 5.90 1.40 12 -5 0 7.00 1.40 12 -5 0 6.90 1.70 12 5 0 6.40 1.40 -12 5 0 8.30 1.80 -12 5 0 7.90 1.60 12 5 0 7.60 1.80 -12 5 0 7.70 1.50 13 -5 0 90.19 4.60 -13 -5 0 88.19 4.60 -13 -5 0 90.19 4.40 13 -5 0 77.09 4.10 -13 -5 0 83.29 4.10 13 -5 0 78.29 4.20 13 -5 0 82.79 4.00 -13 -5 0 82.79 4.00 13 5 0 86.49 4.30 -13 5 0 84.09 3.90 13 5 0 82.69 4.40 -13 5 0 83.69 4.50 13 5 0 86.29 4.00 13 5 0 80.39 4.60 -14 -5 0 16.50 2.30 -14 -5 0 19.30 2.20 14 -5 0 20.20 2.40 14 -5 0 17.70 2.50 -14 -5 0 23.10 2.90 -14 -5 0 15.50 2.10 14 -5 0 16.00 1.90 14 -5 0 16.80 2.40 14 5 0 20.20 2.60 -14 5 0 19.30 2.10 -14 5 0 16.60 2.20 14 5 0 20.20 2.30 14 5 0 16.80 2.30 -14 5 0 18.50 2.30 14 5 0 21.90 2.80 -14 5 0 19.00 2.60 15 -5 0 10.40 2.40 -15 -5 0 17.80 2.90 -15 -5 0 15.20 2.40 15 -5 0 11.50 2.60 -15 -5 0 12.50 2.20 15 -5 0 9.00 1.80 15 -5 0 12.70 2.10 -15 -5 0 12.70 2.30 15 5 0 13.10 2.00 15 5 0 13.60 2.80 15 5 0 11.80 2.40 -15 5 0 8.70 2.20 -15 5 0 9.30 2.30 15 5 0 11.10 2.40 -15 5 0 15.00 2.60 -15 5 0 13.30 2.00 16 -5 0 2.30 2.00 16 -5 0 3.70 2.10 -16 -5 0 4.10 2.40 -16 -5 0 4.20 2.10 16 -5 0 4.40 2.70 16 5 0 2.90 2.40 -16 5 0 -1.90 2.20 16 5 0 0.70 1.90 -16 5 0 4.40 2.10 -16 5 0 -2.10 2.40 0 -6 0 237.88 6.40 0 -6 0 239.28 6.40 0 -6 0 243.58 6.50 0 -6 0 235.28 6.50 0 6 0 237.48 6.40 0 6 0 243.68 6.50 0 6 0 234.58 6.50 0 6 0 244.18 6.40 -1 -6 0 77.29 2.50 -1 -6 0 80.29 2.60 -1 -6 0 85.59 2.60 1 -6 0 87.19 2.60 1 -6 0 82.19 2.60 1 -6 0 79.39 2.50 -1 -6 0 82.99 2.70 1 -6 0 83.79 2.70 -1 6 0 84.59 2.50 1 6 0 80.69 2.60 1 6 0 84.99 2.60 1 6 0 83.29 2.60 1 6 0 82.69 2.50 -1 6 0 81.59 2.60 -1 6 0 81.19 2.50 -2 -6 0 8.00 0.90 -2 -6 0 8.20 1.00 -2 -6 0 7.70 0.80 2 -6 0 6.60 0.80 2 -6 0 6.80 0.80 2 -6 0 7.60 0.80 -2 -6 0 8.60 0.90 2 -6 0 8.10 0.80 -2 6 0 7.10 0.80 2 6 0 9.80 0.90 -2 6 0 7.90 0.90 -2 6 0 7.60 0.80 -2 6 0 5.80 0.70 2 6 0 7.90 0.90 2 6 0 8.80 0.90 2 6 0 7.60 0.80 -3 -6 0 0.80 0.50 3 -6 0 0.30 0.50 3 -6 0 -0.10 0.40 -3 -6 0 0.50 0.50 3 -6 0 -0.20 0.40 3 -6 0 -0.50 0.40 -3 -6 0 -0.10 0.40 -3 -6 0 -0.10 0.50 3 6 0 0.10 0.40 3 6 0 -0.30 0.40 3 6 0 0.20 0.40 -3 6 0 -0.10 0.40 -3 6 0 0.30 0.50 -3 6 0 0.30 0.50 3 6 0 0.40 0.50 -3 6 0 -0.50 0.40 -4 -6 0 279.27 7.60 4 -6 0 273.27 7.60 -4 -6 0 292.27 7.70 4 -6 0 269.77 7.60 -4 -6 0 278.67 7.70 4 -6 0 280.57 7.60 -4 -6 0 281.37 7.60 4 -6 0 276.47 7.70 -4 6 0 278.07 7.50 4 6 0 271.97 7.60 4 6 0 284.57 7.70 -4 6 0 279.37 7.50 4 6 0 295.47 7.80 -4 6 0 272.97 7.60 -4 6 0 283.17 7.70 4 6 0 276.47 7.60 -5 -6 0 61.89 2.40 5 -6 0 60.09 2.40 -5 -6 0 59.09 2.40 -5 -6 0 59.99 2.30 5 -6 0 58.79 2.30 5 -6 0 58.39 2.30 5 -6 0 58.49 2.20 -5 -6 0 60.99 2.30 5 6 0 56.89 2.40 -5 6 0 63.09 2.30 5 6 0 57.99 2.20 -5 6 0 61.19 2.40 -5 6 0 58.69 2.20 5 6 0 58.09 2.40 -5 6 0 59.49 2.40 5 6 0 61.79 2.30 -6 -6 0 59.59 2.40 6 -6 0 56.19 2.40 -6 -6 0 56.29 2.40 6 -6 0 57.39 2.30 6 -6 0 56.19 2.30 -6 -6 0 58.29 2.30 -6 -6 0 59.29 2.50 6 -6 0 57.59 2.40 6 6 0 57.49 2.40 -6 6 0 58.29 2.40 -6 6 0 55.99 2.40 6 6 0 56.09 2.50 6 6 0 58.39 2.50 -6 6 0 60.99 2.30 6 6 0 57.39 2.30 -6 6 0 57.99 2.20 -7 -6 0 132.39 4.30 -7 -6 0 121.89 4.20 7 -6 0 122.19 4.20 7 -6 0 123.89 4.10 7 -6 0 125.69 4.00 -7 -6 0 125.99 4.10 7 -6 0 121.29 4.20 -7 6 0 125.59 4.20 7 6 0 127.49 4.30 7 6 0 123.79 4.10 -7 6 0 125.69 4.00 7 6 0 123.19 4.30 -7 6 0 121.69 4.00 -7 6 0 121.89 4.20 7 6 0 126.59 4.10 -8 -6 0 1.40 0.80 8 -6 0 1.20 0.70 -8 -6 0 0.50 0.70 -8 -6 0 2.10 1.00 -8 -6 0 2.10 1.00 8 -6 0 1.80 0.70 8 -6 0 1.00 0.70 8 -6 0 1.30 0.90 8 6 0 0.70 0.80 -8 6 0 1.00 0.90 -8 6 0 1.50 0.70 8 6 0 2.40 0.90 -8 6 0 2.10 0.90 8 6 0 0.90 0.70 -8 6 0 0.60 0.70 8 6 0 1.30 0.80 9 -6 0 21.20 2.00 -9 -6 0 16.10 1.70 9 -6 0 18.90 1.70 -9 -6 0 18.20 2.10 9 -6 0 17.60 1.80 -9 -6 0 18.40 1.90 9 -6 0 15.70 1.70 -9 -6 0 14.90 1.80 9 6 0 19.40 1.80 -9 6 0 20.40 1.80 9 6 0 20.10 1.90 -9 6 0 15.10 1.90 -9 6 0 14.80 1.70 9 6 0 18.90 2.00 -9 6 0 17.20 1.90 9 6 0 18.90 2.10 -10 -6 0 163.78 5.60 10 -6 0 156.88 5.40 -10 -6 0 155.38 5.30 10 -6 0 157.18 5.30 10 -6 0 163.08 5.60 -10 -6 0 155.68 5.50 10 -6 0 162.28 5.40 10 6 0 156.28 5.60 -10 6 0 157.78 5.20 -10 6 0 160.38 5.30 10 6 0 152.28 5.20 -10 6 0 152.58 5.50 10 6 0 161.48 5.60 -10 6 0 155.08 5.50 10 6 0 153.58 5.40 -11 -6 0 24.70 2.70 11 -6 0 24.20 2.40 11 -6 0 26.30 2.60 -11 -6 0 25.60 2.20 11 -6 0 22.50 2.30 -11 -6 0 21.60 2.40 11 -6 0 18.80 2.10 11 6 0 26.40 2.80 -11 6 0 23.00 2.10 -11 6 0 22.50 2.30 -11 6 0 23.50 2.40 11 6 0 25.30 2.40 -12 -6 0 39.00 2.70 12 -6 0 33.80 2.60 12 -6 0 39.30 2.90 -12 -6 0 35.60 2.90 12 -6 0 33.50 3.10 12 -6 0 24.30 2.60 -12 -6 0 32.10 3.30 -12 6 0 32.90 3.00 12 6 0 39.20 3.30 12 6 0 36.20 2.70 12 6 0 35.30 2.90 -12 6 0 37.90 2.90 -12 6 0 33.80 2.50 -13 -6 0 6.80 1.80 -13 -6 0 8.50 1.90 13 -6 0 5.60 1.60 -13 -6 0 7.00 1.70 -13 -6 0 7.10 1.60 13 -6 0 7.10 1.80 13 -6 0 8.00 1.80 13 -6 0 6.60 1.50 -13 6 0 7.60 1.60 13 6 0 8.20 1.60 -13 6 0 11.60 1.90 13 6 0 10.10 2.10 -13 6 0 9.50 2.10 13 6 0 8.30 1.90 13 6 0 7.80 1.90 14 -6 0 5.20 1.70 -14 -6 0 6.50 2.00 14 -6 0 7.50 1.90 14 -6 0 9.70 2.10 -14 -6 0 5.50 1.80 -14 -6 0 7.50 2.00 -14 -6 0 6.80 2.10 14 -6 0 1.00 1.60 -14 6 0 6.40 1.90 -14 6 0 5.90 2.20 -14 6 0 7.40 2.00 14 6 0 6.80 1.60 -14 6 0 8.60 1.80 14 6 0 4.60 2.10 14 6 0 7.60 2.10 14 6 0 4.60 1.90 -15 -6 0 2.50 2.40 15 -6 0 -1.30 1.60 -15 -6 0 -1.50 2.00 15 -6 0 2.10 2.30 -15 -6 0 -0.70 1.80 -15 -6 0 -0.70 2.00 15 -6 0 3.50 2.00 15 -6 0 1.90 2.10 15 6 0 -0.90 2.10 15 6 0 -2.30 2.10 15 6 0 4.40 1.80 -15 6 0 0.40 1.90 15 6 0 -1.50 2.00 -15 6 0 0.00 1.60 -15 6 0 2.30 2.30 -15 6 0 1.70 2.00 -16 -6 0 1.10 2.30 16 -6 0 3.80 2.30 16 -6 0 5.80 3.00 -16 -6 0 -1.10 2.20 16 -6 0 4.40 2.20 16 6 0 2.60 2.50 -16 6 0 1.00 2.00 -16 6 0 -1.80 2.30 -16 6 0 3.50 2.60 16 6 0 6.20 2.50 0 -7 0 0.20 0.40 0 -7 0 0.10 0.50 0 -7 0 -0.10 0.40 0 -7 0 0.90 0.40 0 7 0 -0.10 0.40 0 7 0 -0.10 0.40 0 7 0 0.10 0.40 0 7 0 -0.20 0.40 1 -7 0 10.40 0.90 -1 -7 0 10.30 1.00 1 -7 0 11.20 1.00 -1 -7 0 10.70 1.00 -1 -7 0 10.20 1.00 -1 -7 0 11.20 0.90 1 -7 0 12.40 1.00 1 -7 0 9.40 1.00 1 7 0 11.30 0.90 -1 7 0 10.90 0.90 -1 7 0 10.60 1.00 1 7 0 12.50 1.00 -1 7 0 10.10 0.90 2 -7 0 323.67 8.60 2 -7 0 321.87 8.70 2 -7 0 331.47 8.70 -2 -7 0 333.37 8.70 -2 -7 0 325.27 8.70 -2 -7 0 318.67 8.80 -2 -7 0 308.07 8.70 2 -7 0 328.77 8.80 2 7 0 321.67 8.60 -2 7 0 324.17 8.70 2 7 0 323.87 8.80 -2 7 0 327.67 8.60 -2 7 0 325.97 8.60 2 7 0 327.87 8.60 2 7 0 340.57 8.80 -2 7 0 331.37 8.80 -3 -7 0 252.37 7.00 3 -7 0 255.77 6.90 3 -7 0 246.58 6.80 3 -7 0 253.07 6.90 -3 -7 0 257.27 6.90 -3 -7 0 253.67 6.90 3 -7 0 241.98 6.90 -3 -7 0 257.57 7.00 3 7 0 246.18 6.80 3 7 0 253.37 6.90 -3 7 0 249.78 6.90 -3 7 0 248.78 6.90 -3 7 0 245.08 6.80 3 7 0 243.68 7.00 -3 7 0 254.17 6.80 3 7 0 240.48 7.00 4 -7 0 102.59 3.30 4 -7 0 104.69 3.40 4 -7 0 103.69 3.40 4 -7 0 99.99 3.30 -4 -7 0 102.99 3.40 -4 -7 0 105.19 3.50 -4 -7 0 105.49 3.40 -4 -7 0 103.99 3.50 4 7 0 103.39 3.50 -4 7 0 104.89 3.30 -4 7 0 99.89 3.40 4 7 0 106.69 3.30 4 7 0 104.79 3.40 4 7 0 102.19 3.50 -4 7 0 103.29 3.40 -4 7 0 101.29 3.20 5 -7 0 0.80 0.60 -5 -7 0 -0.20 0.50 5 -7 0 0.10 0.50 -5 -7 0 -0.20 0.60 -5 -7 0 -0.10 0.60 5 -7 0 -0.30 0.60 -5 -7 0 -0.70 0.60 5 -7 0 -0.10 0.50 -5 7 0 0.10 0.50 -5 7 0 0.30 0.50 5 7 0 -0.10 0.70 5 7 0 -0.10 0.50 5 7 0 -0.20 0.50 5 7 0 0.00 0.60 -5 7 0 -0.30 0.50 -5 7 0 0.20 0.60 6 -7 0 0.30 0.50 -6 -7 0 0.80 0.70 6 -7 0 -0.20 0.60 -6 -7 0 0.20 0.60 -6 -7 0 0.30 0.70 6 -7 0 0.00 0.60 -6 -7 0 0.00 0.60 6 -7 0 0.20 0.60 6 7 0 -0.20 0.50 -6 7 0 0.80 0.70 6 7 0 -0.40 0.60 6 7 0 -0.40 0.70 6 7 0 -0.30 0.70 -6 7 0 0.10 0.60 -6 7 0 -0.40 0.60 -6 7 0 0.60 0.50 -7 -7 0 52.99 2.50 7 -7 0 51.29 2.50 7 -7 0 50.99 2.40 7 -7 0 49.10 2.30 -7 -7 0 49.20 2.40 -7 -7 0 49.10 2.40 7 -7 0 52.49 2.40 -7 -7 0 51.49 2.60 7 7 0 50.69 2.30 -7 7 0 54.69 2.50 -7 7 0 51.39 2.50 7 7 0 49.80 2.60 7 7 0 49.10 2.40 7 7 0 54.89 2.60 -7 7 0 52.39 2.30 -7 7 0 51.49 2.30 -8 -7 0 25.90 2.00 8 -7 0 25.00 2.00 8 -7 0 25.40 1.90 8 -7 0 23.80 1.80 -8 -7 0 21.80 2.10 8 -7 0 25.20 1.70 -8 -7 0 24.40 1.80 8 7 0 24.30 2.10 -8 7 0 24.00 1.70 -8 7 0 24.30 1.80 8 7 0 22.80 1.90 8 7 0 23.90 1.80 -8 7 0 22.10 1.90 8 7 0 19.80 1.90 -8 7 0 24.50 2.00 -9 -7 0 153.88 5.30 -9 -7 0 155.88 5.40 -9 -7 0 153.38 5.50 9 -7 0 158.68 5.30 -9 -7 0 159.08 5.20 9 -7 0 162.58 5.50 9 -7 0 151.98 5.10 9 7 0 160.18 5.50 -9 7 0 158.58 5.10 -9 7 0 156.48 5.10 9 7 0 154.68 6.40 9 7 0 154.38 5.30 -9 7 0 161.98 5.40 -9 7 0 154.88 5.50 9 7 0 156.08 5.20 10 -7 0 79.09 3.70 10 -7 0 78.69 3.50 10 -7 0 78.59 3.50 10 -7 0 80.09 3.40 -10 -7 0 81.59 3.60 -10 -7 0 85.19 3.60 10 7 0 84.49 3.60 -10 7 0 77.09 4.00 10 7 0 79.79 3.90 -10 7 0 79.99 3.60 10 7 0 74.09 3.60 -10 7 0 73.99 3.30 10 7 0 79.29 3.40 11 -7 0 0.70 1.20 11 -7 0 0.60 1.00 -11 -7 0 0.00 1.20 11 -7 0 0.20 1.00 -11 -7 0 1.10 1.40 -11 -7 0 3.10 1.10 11 -7 0 0.20 1.30 -11 7 0 0.10 1.10 -11 7 0 -0.50 0.90 11 7 0 1.50 1.10 -11 7 0 0.90 1.20 11 7 0 0.20 1.30 11 7 0 1.50 1.10 -12 -7 0 12.50 2.10 12 -7 0 9.50 1.50 -12 -7 0 9.10 1.60 12 -7 0 10.00 1.80 12 -7 0 10.30 1.60 12 -7 0 15.10 2.10 -12 -7 0 9.40 1.70 12 7 0 11.40 2.10 12 7 0 14.50 2.00 -12 7 0 11.60 1.80 12 7 0 12.20 1.70 12 7 0 14.30 2.00 -12 7 0 9.50 1.70 -12 7 0 10.60 1.50 13 -7 0 45.00 3.10 13 -7 0 44.40 3.50 -13 -7 0 48.60 4.00 13 -7 0 51.19 3.90 -13 -7 0 46.20 3.70 -13 -7 0 50.39 3.80 -13 -7 0 44.80 3.30 13 -7 0 45.50 3.40 13 7 0 48.10 3.60 -13 7 0 51.89 3.90 13 7 0 44.30 4.10 -13 7 0 49.30 4.20 13 7 0 47.70 3.70 -13 7 0 48.00 3.10 -13 7 0 52.99 3.50 13 7 0 45.00 3.30 -14 -7 0 20.80 2.90 14 -7 0 16.50 2.30 -14 -7 0 13.60 2.30 -14 -7 0 14.30 2.50 14 -7 0 19.60 2.30 14 -7 0 16.60 2.30 -14 -7 0 15.10 2.20 14 -7 0 19.10 2.80 -14 7 0 14.50 2.20 14 7 0 15.10 2.70 -14 7 0 15.70 2.30 14 7 0 17.00 2.30 14 7 0 15.50 2.40 -14 7 0 19.30 2.20 14 7 0 14.20 2.30 -14 7 0 16.00 2.50 15 -7 0 7.30 2.70 15 -7 0 4.30 2.10 15 -7 0 5.50 1.90 -15 -7 0 12.40 2.80 -15 -7 0 9.30 2.10 -15 -7 0 8.20 2.40 15 7 0 4.30 2.40 -15 7 0 7.20 2.20 15 7 0 4.20 2.60 -15 7 0 9.30 2.10 -15 7 0 9.20 2.20 15 7 0 6.60 1.90 15 7 0 5.20 2.40 -16 -7 0 7.80 2.80 16 -7 0 4.80 3.00 16 -7 0 2.50 1.90 16 -7 0 2.00 2.50 -16 -7 0 4.40 2.50 16 7 0 1.50 2.50 -16 7 0 4.20 2.00 -16 7 0 6.50 2.70 16 7 0 2.90 2.50 -16 7 0 6.90 2.50 0 -8 0 52.39 2.10 0 -8 0 52.59 2.00 0 -8 0 53.89 2.10 0 -8 0 54.09 2.20 0 8 0 53.59 2.00 0 8 0 54.19 2.10 0 8 0 53.49 2.00 0 8 0 56.29 2.20 1 -8 0 114.39 3.70 -1 -8 0 108.19 3.70 1 -8 0 117.79 3.60 -1 -8 0 122.39 3.60 -1 -8 0 114.29 3.70 1 -8 0 120.39 3.60 1 -8 0 116.69 3.70 -1 -8 0 118.69 3.60 -1 8 0 119.49 3.50 -1 8 0 120.79 3.60 1 8 0 118.39 3.70 1 8 0 119.89 3.60 -1 8 0 114.89 3.70 1 8 0 120.29 3.60 -2 -8 0 3.40 0.60 2 -8 0 4.00 0.60 2 -8 0 2.60 0.60 -2 -8 0 4.00 0.70 2 -8 0 3.00 0.60 -2 -8 0 3.70 0.70 -2 -8 0 4.20 0.80 2 -8 0 3.60 0.60 2 8 0 3.60 0.70 2 8 0 3.60 0.60 2 8 0 4.60 0.80 -2 8 0 3.80 0.60 -2 8 0 3.40 0.70 2 8 0 3.80 0.60 -2 8 0 3.60 0.70 -2 8 0 3.80 0.60 -3 -8 0 3.20 0.60 3 -8 0 2.50 0.70 -3 -8 0 3.30 0.80 -3 -8 0 2.60 0.70 3 -8 0 2.70 0.70 -3 -8 0 2.50 0.60 3 -8 0 3.20 0.70 3 -8 0 3.30 0.60 3 8 0 3.70 0.80 3 8 0 2.30 0.70 -3 8 0 2.80 0.70 -3 8 0 2.40 0.60 -3 8 0 2.60 0.60 -3 8 0 3.30 0.70 3 8 0 3.30 0.60 3 8 0 2.60 0.70 4 -8 0 196.68 5.60 4 -8 0 190.48 5.50 -4 -8 0 191.68 5.60 4 -8 0 195.08 5.60 -4 -8 0 189.48 5.70 -4 -8 0 187.78 5.60 -4 -8 0 187.58 5.70 4 8 0 186.68 5.50 -4 8 0 191.28 5.60 -4 8 0 193.28 5.50 4 8 0 181.28 5.70 4 8 0 189.58 5.50 -4 8 0 188.08 5.60 -4 8 0 189.48 5.40 4 8 0 196.38 5.70 5 -8 0 111.39 3.60 5 -8 0 107.69 3.60 5 -8 0 112.19 3.80 -5 -8 0 106.49 3.70 -5 -8 0 106.89 3.80 -5 -8 0 111.79 3.70 5 -8 0 109.59 3.70 -5 -8 0 102.89 3.80 5 8 0 111.39 3.60 5 8 0 114.09 3.70 5 8 0 108.89 3.80 -5 8 0 110.39 3.80 -5 8 0 111.99 3.60 5 8 0 113.09 3.90 -5 8 0 109.19 3.70 -5 8 0 106.89 3.50 -6 -8 0 0.20 0.70 6 -8 0 0.80 0.70 6 -8 0 -0.40 0.60 6 -8 0 -0.30 0.60 6 -8 0 0.40 0.60 -6 -8 0 -0.30 0.70 -6 -8 0 0.50 0.80 -6 -8 0 0.00 0.60 -6 8 0 0.10 0.60 -6 8 0 0.30 0.60 6 8 0 0.00 0.60 6 8 0 0.40 0.70 -6 8 0 0.70 0.70 6 8 0 0.60 0.70 6 8 0 0.10 0.80 -6 8 0 -0.70 0.60 -7 -8 0 149.29 4.90 -7 -8 0 145.99 4.70 7 -8 0 143.99 4.70 7 -8 0 141.79 4.70 7 -8 0 150.58 4.80 7 -8 0 144.09 4.60 -7 -8 0 140.59 4.80 -7 -8 0 138.29 4.70 7 8 0 139.69 4.60 -7 8 0 139.09 4.50 -7 8 0 142.89 4.80 7 8 0 147.09 4.90 -7 8 0 143.89 4.80 -7 8 0 140.19 4.50 7 8 0 137.29 4.80 7 8 0 141.99 4.70 8 -8 0 1.10 0.90 -8 -8 0 2.10 0.80 -8 -8 0 0.30 1.00 8 -8 0 0.20 0.70 8 -8 0 0.50 0.70 -8 -8 0 0.80 0.90 -8 -8 0 -0.50 0.70 8 -8 0 0.20 0.90 8 8 0 1.30 0.90 8 8 0 1.30 0.80 -8 8 0 2.10 0.80 -8 8 0 0.30 0.80 -8 8 0 0.60 1.00 8 8 0 0.50 0.70 -8 8 0 0.70 0.80 8 8 0 0.00 0.90 -9 -8 0 51.39 2.60 9 -8 0 50.39 2.80 9 -8 0 47.50 2.70 -9 -8 0 43.40 2.90 -9 -8 0 50.89 2.80 9 -8 0 50.39 2.60 9 -8 0 50.59 2.90 9 8 0 54.49 2.90 9 8 0 50.69 2.80 9 8 0 52.29 2.60 -9 8 0 52.09 2.50 9 8 0 54.09 3.10 -9 8 0 57.39 2.70 -9 8 0 56.29 2.90 -10 -8 0 66.89 3.50 -10 -8 0 61.59 3.50 10 -8 0 69.69 3.50 -10 -8 0 63.69 3.40 10 -8 0 66.59 3.30 10 -8 0 48.10 3.50 10 -8 0 54.99 3.70 10 8 0 69.29 3.30 10 8 0 63.09 3.40 -10 8 0 65.39 3.20 -10 8 0 65.89 3.30 10 8 0 67.99 3.60 10 8 0 63.19 3.00 -10 8 0 63.99 3.00 -11 -8 0 119.99 5.10 11 -8 0 122.09 4.60 11 -8 0 120.89 4.80 -11 -8 0 119.19 4.90 11 -8 0 121.79 4.80 -11 -8 0 122.49 4.70 11 8 0 121.59 5.00 11 8 0 115.29 4.50 11 8 0 115.69 5.10 -11 8 0 113.99 4.80 -11 8 0 120.49 4.50 -11 8 0 116.89 4.60 -12 -8 0 1.00 1.30 -12 -8 0 -0.40 1.50 -12 -8 0 1.60 1.50 12 -8 0 -0.20 1.60 -12 -8 0 0.50 1.40 12 -8 0 -0.60 1.30 12 -8 0 -1.30 1.10 12 -8 0 1.60 1.30 12 8 0 0.80 1.60 12 8 0 -0.40 1.50 -12 8 0 0.60 1.20 12 8 0 1.30 1.30 -12 8 0 1.20 1.60 -12 8 0 -0.10 1.30 12 8 0 2.70 1.60 13 -8 0 54.89 4.20 -13 -8 0 55.69 3.90 13 -8 0 54.79 3.80 13 -8 0 57.59 3.60 -13 -8 0 46.40 4.20 13 -8 0 56.49 3.90 -13 -8 0 56.29 3.60 -13 -8 0 48.00 3.80 -13 8 0 50.99 3.70 -13 8 0 59.69 4.20 -13 8 0 55.79 3.50 13 8 0 57.39 4.00 13 8 0 52.69 4.40 13 8 0 50.59 3.50 -13 8 0 57.09 3.90 13 8 0 59.39 4.10 14 -8 0 1.50 2.30 -14 -8 0 3.00 1.70 -14 -8 0 0.50 2.20 14 -8 0 -0.90 1.60 14 -8 0 -1.70 1.70 14 -8 0 1.00 1.90 -14 -8 0 2.50 2.10 -14 -8 0 -1.60 1.90 -14 8 0 1.00 1.60 14 8 0 0.90 1.50 -14 8 0 2.00 2.00 -14 8 0 0.70 1.90 14 8 0 4.80 2.00 14 8 0 3.80 2.10 -14 8 0 2.30 2.10 14 8 0 2.40 2.20 -15 -8 0 3.80 2.30 15 -8 0 1.10 1.80 -15 -8 0 3.10 2.70 15 -8 0 4.80 2.10 15 -8 0 5.20 2.70 -15 -8 0 3.70 1.90 -15 8 0 6.70 2.50 15 8 0 4.70 1.90 15 8 0 6.10 2.50 -15 8 0 5.30 2.10 -15 8 0 0.50 2.30 -16 -8 0 -2.10 2.60 16 -8 0 -3.30 3.10 16 8 0 -1.20 2.70 -16 8 0 3.30 2.70 16 8 0 -2.60 2.30 -16 8 0 3.20 2.00 0 -9 0 -0.10 0.50 0 -9 0 -0.50 0.60 0 -9 0 0.40 0.50 0 -9 0 -0.40 0.40 0 9 0 0.20 0.50 0 9 0 -0.20 0.50 0 9 0 -0.10 0.50 0 9 0 0.00 0.50 -1 -9 0 14.50 1.20 1 -9 0 12.10 1.20 -1 -9 0 12.70 1.30 -1 -9 0 13.90 1.20 1 -9 0 12.80 1.20 -1 -9 0 10.80 1.10 1 -9 0 13.50 1.10 1 -9 0 12.40 1.20 -1 9 0 12.50 1.10 1 9 0 12.50 1.10 1 9 0 11.80 1.20 1 9 0 11.20 1.20 1 9 0 13.50 1.30 -1 9 0 12.80 1.10 -1 9 0 12.30 1.20 -2 -9 0 11.40 1.20 -2 -9 0 11.70 1.10 -2 -9 0 11.60 1.30 2 -9 0 12.10 1.10 -2 -9 0 11.50 1.20 2 -9 0 11.20 1.30 2 -9 0 10.60 1.20 2 -9 0 12.00 1.20 2 9 0 10.80 1.20 2 9 0 12.60 1.30 -2 9 0 12.40 1.30 2 9 0 10.50 1.10 -2 9 0 9.40 1.10 -2 9 0 9.70 1.20 -2 9 0 10.50 1.10 2 9 0 10.50 1.20 -3 -9 0 392.36 10.50 3 -9 0 391.46 10.40 -3 -9 0 379.56 10.50 -3 -9 0 385.96 10.40 3 -9 0 389.06 10.40 3 -9 0 384.96 10.50 3 -9 0 385.06 10.50 -3 -9 0 395.16 10.60 -3 9 0 385.76 10.50 3 9 0 392.46 10.40 3 9 0 401.16 10.40 -3 9 0 387.66 10.30 -3 9 0 385.26 10.50 3 9 0 391.26 10.60 3 9 0 367.56 10.50 -3 9 0 392.46 10.30 4 -9 0 107.69 3.60 -4 -9 0 108.79 3.60 -4 -9 0 107.29 3.60 4 -9 0 108.59 3.70 4 -9 0 105.99 3.50 4 -9 0 104.59 3.60 -4 -9 0 98.89 3.70 -4 -9 0 100.59 3.70 -4 9 0 108.19 3.50 4 9 0 104.99 3.70 4 9 0 107.49 3.60 -4 9 0 106.79 3.70 -4 9 0 107.99 3.70 4 9 0 111.49 3.80 -4 9 0 105.99 3.40 4 9 0 106.69 3.50 -5 -9 0 13.50 1.50 5 -9 0 14.30 1.50 5 -9 0 14.20 1.40 -5 -9 0 13.60 1.40 -5 -9 0 13.20 1.50 -5 -9 0 12.70 1.60 5 -9 0 12.00 1.30 5 -9 0 10.80 1.30 5 9 0 14.40 1.50 5 9 0 12.70 1.50 -5 9 0 12.30 1.30 -5 9 0 12.20 1.40 -5 9 0 14.50 1.40 5 9 0 14.40 1.30 -5 9 0 12.30 1.50 5 9 0 13.90 1.60 6 -9 0 3.00 0.80 6 -9 0 1.20 0.70 -6 -9 0 2.30 0.90 6 -9 0 1.30 0.70 -6 -9 0 0.80 0.70 -6 -9 0 1.80 0.90 -6 -9 0 2.00 0.80 6 -9 0 2.80 0.90 -6 9 0 1.10 0.80 6 9 0 1.60 0.90 -6 9 0 2.20 0.70 -6 9 0 1.80 0.80 6 9 0 1.50 0.80 6 9 0 2.40 0.80 -6 9 0 1.30 0.90 6 9 0 -0.10 0.80 7 -9 0 66.39 3.00 -7 -9 0 67.99 3.00 -7 -9 0 69.39 3.20 7 -9 0 68.49 2.80 7 -9 0 69.19 3.10 7 -9 0 68.29 2.90 -7 -9 0 67.49 3.10 -7 -9 0 67.89 2.90 -7 9 0 64.69 2.80 -7 9 0 68.09 3.00 7 9 0 68.29 3.00 -7 9 0 68.29 3.10 7 9 0 71.59 3.20 7 9 0 68.59 2.90 7 9 0 66.59 3.20 -7 9 0 69.39 2.80 8 -9 0 64.79 2.80 8 -9 0 64.19 2.90 -8 -9 0 60.59 2.90 -8 -9 0 56.19 3.00 -8 -9 0 63.59 3.20 8 -9 0 63.39 3.10 -8 -9 0 62.09 3.00 8 9 0 61.99 3.00 -8 9 0 66.19 2.80 -8 9 0 62.99 2.70 8 9 0 60.99 3.30 8 9 0 58.89 3.00 8 9 0 63.69 2.80 -8 9 0 63.09 3.10 -9 -9 0 31.60 2.40 9 -9 0 31.00 2.40 -9 -9 0 32.60 2.30 9 -9 0 27.30 2.50 9 -9 0 32.10 2.30 -9 -9 0 34.80 2.70 9 -9 0 28.80 2.10 -9 9 0 29.70 2.40 -9 9 0 28.60 2.20 9 9 0 35.10 2.50 9 9 0 31.20 2.60 -9 9 0 30.40 2.10 9 9 0 35.20 2.50 9 9 0 29.20 2.10 -10 -9 0 25.70 2.40 -10 -9 0 26.70 2.90 10 -9 0 25.20 2.30 -10 -9 0 26.30 2.50 10 -9 0 25.00 2.20 10 -9 0 24.80 2.70 10 -9 0 23.80 2.40 -10 9 0 26.80 2.40 -10 9 0 24.20 2.10 10 9 0 28.90 2.80 10 9 0 23.80 2.40 10 9 0 21.40 2.60 -10 9 0 28.60 2.60 -11 -9 0 1.60 1.50 11 -9 0 2.30 1.20 -11 -9 0 2.60 1.50 -11 -9 0 4.80 1.30 11 -9 0 2.70 1.50 11 -9 0 3.00 1.40 11 -9 0 2.60 1.20 11 9 0 3.00 1.50 -11 9 0 3.30 1.40 -11 9 0 1.60 1.30 11 9 0 4.20 1.30 -11 9 0 4.60 1.30 -12 -9 0 3.20 1.70 12 -9 0 2.20 1.30 12 -9 0 3.10 1.80 12 -9 0 1.60 1.50 12 -9 0 1.60 1.60 -12 -9 0 -0.10 1.30 -12 -9 0 1.80 1.80 -12 -9 0 1.70 1.70 12 9 0 1.90 1.80 12 9 0 0.10 1.60 -12 9 0 0.20 1.50 -12 9 0 -1.30 1.60 -12 9 0 1.10 1.20 12 9 0 2.90 1.50 12 9 0 -1.50 1.20 -13 -9 0 103.39 5.50 13 -9 0 93.39 4.80 -13 -9 0 90.19 4.70 13 -9 0 104.59 4.90 13 -9 0 97.49 4.60 -13 -9 0 95.79 4.80 -13 -9 0 95.49 5.00 13 -9 0 99.29 5.30 13 9 0 94.59 4.50 -13 9 0 94.59 5.20 -13 9 0 91.19 4.90 13 9 0 98.49 5.00 13 9 0 95.59 5.40 -13 9 0 98.09 4.40 13 9 0 92.59 5.00 -13 9 0 90.09 4.70 14 -9 0 -0.90 1.60 14 -9 0 0.40 1.70 -14 -9 0 3.70 2.30 -14 -9 0 -1.30 2.10 14 -9 0 -2.50 2.20 14 -9 0 3.40 2.20 -14 -9 0 1.20 1.80 -14 -9 0 -2.00 2.00 14 9 0 0.30 2.40 -14 9 0 -1.20 2.00 -14 9 0 -0.20 2.40 14 9 0 1.90 2.10 14 9 0 -3.40 1.60 -14 9 0 1.80 2.00 14 9 0 4.60 2.20 -14 9 0 2.10 1.70 15 -9 0 0.30 2.30 -15 -9 0 0.00 2.20 15 -9 0 -2.40 2.60 15 -9 0 -1.30 2.10 -15 -9 0 3.80 2.30 -15 -9 0 -0.90 2.50 -15 9 0 2.30 2.30 15 9 0 -0.40 1.90 15 9 0 0.20 2.50 -15 9 0 1.90 2.30 -15 9 0 3.40 2.20 0 -10 0 100.99 3.40 0 -10 0 98.19 3.40 0 -10 0 100.19 3.50 0 -10 0 100.49 3.50 0 10 0 98.99 3.50 0 10 0 101.69 3.30 0 10 0 103.49 3.30 0 10 0 101.19 3.50 -1 -10 0 33.00 1.70 1 -10 0 32.90 1.80 1 -10 0 31.80 1.90 1 -10 0 30.80 1.70 -1 -10 0 33.40 1.80 -1 -10 0 31.60 1.80 -1 -10 0 31.20 1.80 1 -10 0 35.20 1.70 1 10 0 31.30 1.70 -1 10 0 33.20 1.60 -1 10 0 31.50 1.60 1 10 0 31.80 1.70 1 10 0 34.80 1.90 -1 10 0 34.70 1.90 1 10 0 32.00 1.90 2 -10 0 0.90 0.60 -2 -10 0 0.60 0.60 2 -10 0 0.20 0.60 -2 -10 0 0.10 0.60 2 -10 0 -0.10 0.60 -2 -10 0 -0.10 0.60 2 -10 0 0.20 0.60 -2 -10 0 1.10 0.70 -2 10 0 0.20 0.60 2 10 0 0.90 0.70 -2 10 0 0.00 0.70 2 10 0 0.40 0.60 -2 10 0 0.30 0.60 -2 10 0 0.80 0.60 2 10 0 1.10 0.60 2 10 0 0.10 0.60 3 -10 0 0.10 0.60 3 -10 0 0.50 0.60 3 -10 0 0.80 0.70 -3 -10 0 1.10 0.70 3 -10 0 -0.30 0.60 -3 -10 0 0.40 0.60 -3 -10 0 -0.40 0.70 -3 -10 0 0.40 0.70 3 10 0 0.70 0.60 3 10 0 0.20 0.70 -3 10 0 0.40 0.70 -3 10 0 0.70 0.70 -3 10 0 0.30 0.60 -3 10 0 0.20 0.50 3 10 0 0.30 0.70 3 10 0 1.10 0.60 -4 -10 0 5.50 0.90 -4 -10 0 6.20 1.00 4 -10 0 6.10 1.00 4 -10 0 6.30 1.00 -4 -10 0 3.80 0.80 4 -10 0 6.10 1.00 4 -10 0 5.70 0.90 -4 -10 0 5.30 1.10 4 10 0 5.20 1.00 4 10 0 6.10 1.10 -4 10 0 6.10 1.00 -4 10 0 5.40 0.90 4 10 0 6.30 0.80 -4 10 0 4.20 0.80 4 10 0 5.50 0.90 -4 10 0 6.30 1.00 -5 -10 0 196.58 6.10 5 -10 0 201.28 6.20 5 -10 0 203.18 6.20 -5 -10 0 201.88 6.10 5 -10 0 210.88 6.20 5 -10 0 200.38 6.00 -5 -10 0 199.98 6.20 -5 -10 0 200.78 6.30 5 10 0 202.98 6.00 -5 10 0 199.88 6.20 5 10 0 204.98 6.30 -5 10 0 200.78 5.90 -5 10 0 206.48 6.20 5 10 0 212.38 6.30 -5 10 0 202.28 6.00 5 10 0 202.08 6.10 6 -10 0 8.70 1.20 6 -10 0 14.20 1.70 -6 -10 0 8.70 1.20 -6 -10 0 7.80 1.10 6 -10 0 8.10 1.00 -6 -10 0 7.40 1.00 6 -10 0 7.80 1.20 -6 -10 0 9.60 1.40 6 10 0 11.40 1.40 6 10 0 11.50 1.30 -6 10 0 11.20 1.30 6 10 0 12.00 1.30 6 10 0 8.40 1.20 -6 10 0 9.30 1.10 -6 10 0 9.20 1.10 -6 10 0 11.30 1.40 7 -10 0 30.10 2.40 7 -10 0 27.70 1.90 7 -10 0 31.90 2.10 -7 -10 0 26.30 2.30 7 -10 0 30.30 2.30 -7 -10 0 33.20 2.50 -7 -10 0 32.30 2.30 -7 -10 0 32.70 2.10 7 10 0 34.30 2.80 -7 10 0 29.00 2.00 7 10 0 34.00 2.30 7 10 0 31.40 2.20 -7 10 0 31.70 2.30 -7 10 0 31.10 2.20 -7 10 0 30.70 1.90 7 10 0 31.40 2.10 -8 -10 0 -0.60 0.90 -8 -10 0 0.50 0.90 -8 -10 0 0.50 1.00 8 -10 0 1.50 1.00 8 -10 0 0.70 0.80 -8 -10 0 1.40 1.10 8 -10 0 0.20 0.80 8 -10 0 -0.60 1.00 -8 10 0 0.70 0.80 8 10 0 1.00 0.90 8 10 0 -0.40 1.00 8 10 0 1.30 1.20 -8 10 0 1.80 1.00 8 10 0 0.00 1.00 -8 10 0 0.20 0.90 -9 -10 0 0.80 1.30 -9 -10 0 -0.40 0.90 9 -10 0 -0.70 1.10 9 -10 0 1.80 1.30 9 -10 0 0.40 1.00 9 10 0 0.30 1.20 9 10 0 1.60 1.20 9 10 0 0.10 0.90 -9 10 0 0.80 0.90 -9 10 0 -0.30 1.10 9 10 0 2.00 1.20 -10 -10 0 10.30 1.60 10 -10 0 13.20 1.60 -10 -10 0 12.50 1.90 10 -10 0 11.20 1.60 -10 -10 0 11.10 1.80 10 -10 0 10.40 1.60 10 -10 0 11.40 1.80 -10 10 0 10.00 1.60 -10 10 0 11.20 1.60 10 10 0 10.80 1.70 10 10 0 10.30 1.40 -10 10 0 9.90 1.40 10 10 0 10.70 1.70 11 -10 0 215.38 7.20 11 -10 0 216.28 7.50 -11 -10 0 214.38 7.30 11 -10 0 219.78 7.40 11 -10 0 215.68 7.10 -11 -10 0 217.88 7.50 -11 -10 0 211.18 7.60 11 10 0 212.98 7.10 11 10 0 211.48 7.60 -11 10 0 222.88 7.00 11 10 0 214.88 7.20 11 10 0 213.48 7.50 -11 10 0 225.18 7.40 -12 -10 0 -0.40 1.70 12 -10 0 -0.10 1.40 -12 -10 0 0.20 1.60 12 -10 0 0.20 1.50 -12 -10 0 -2.60 1.60 12 -10 0 0.70 1.40 12 -10 0 -0.90 1.80 -12 -10 0 -1.80 1.40 12 10 0 -0.40 1.90 12 10 0 0.80 1.30 12 10 0 0.40 1.70 -12 10 0 -0.80 1.50 12 10 0 1.40 1.40 -12 10 0 0.90 2.10 -12 10 0 1.30 1.90 -12 10 0 1.90 1.30 -13 -10 0 71.79 4.20 -13 -10 0 65.79 4.50 13 -10 0 66.69 4.20 13 -10 0 67.39 4.30 -13 -10 0 71.99 4.50 13 -10 0 64.69 4.80 13 -10 0 60.09 3.90 -13 -10 0 71.79 4.90 13 10 0 68.39 4.00 -13 10 0 70.99 4.90 -13 10 0 68.09 4.50 13 10 0 67.59 4.60 -13 10 0 66.49 4.20 13 10 0 59.79 4.50 -13 10 0 70.59 3.90 13 10 0 62.79 4.90 -14 -10 0 -1.20 1.80 14 -10 0 2.30 2.50 -14 -10 0 -0.20 2.50 -14 -10 0 3.80 2.20 14 -10 0 1.90 1.70 14 -10 0 6.10 2.00 14 10 0 1.50 1.80 -14 10 0 -0.10 2.10 -14 10 0 -0.50 2.00 14 10 0 3.10 2.30 14 10 0 -1.80 2.30 -14 10 0 4.00 1.90 15 -10 0 -5.00 2.60 15 -10 0 4.90 3.00 -15 -10 0 1.40 2.70 15 -10 0 1.00 2.10 -15 -10 0 3.20 3.00 15 10 0 0.00 2.60 15 10 0 -2.40 2.40 -15 10 0 4.50 2.10 -15 10 0 -1.10 2.40 -15 10 0 0.20 2.60 0 -11 0 0.40 0.60 0 -11 0 0.90 0.70 0 -11 0 0.50 0.70 0 -11 0 0.50 0.60 0 11 0 0.20 0.60 0 11 0 -0.30 0.70 0 11 0 -0.30 0.60 0 11 0 0.20 0.80 1 -11 0 10.40 1.30 -1 -11 0 12.60 1.50 1 -11 0 12.10 1.40 1 -11 0 13.40 1.60 -1 -11 0 11.20 1.40 -1 -11 0 10.80 1.30 -1 -11 0 12.00 1.50 1 -11 0 11.40 1.30 -1 11 0 11.70 1.40 1 11 0 13.60 1.50 1 11 0 9.90 1.20 -1 11 0 12.20 1.50 1 11 0 13.70 1.40 -1 11 0 11.10 1.20 1 11 0 8.60 1.10 -1 11 0 13.30 1.30 -2 -11 0 44.10 2.20 2 -11 0 39.70 2.10 2 -11 0 43.40 2.10 -2 -11 0 41.90 2.10 -2 -11 0 42.00 2.10 -2 -11 0 38.10 2.30 2 -11 0 45.60 2.30 2 -11 0 40.80 2.10 -2 11 0 40.60 1.90 2 11 0 41.30 2.30 2 11 0 42.30 2.10 2 11 0 40.10 2.00 -2 11 0 42.70 2.20 -2 11 0 40.40 2.10 2 11 0 44.20 2.20 -2 11 0 42.30 2.10 3 -11 0 127.39 4.30 -3 -11 0 121.19 4.20 3 -11 0 122.89 4.20 3 -11 0 127.39 4.20 -3 -11 0 123.59 4.30 -3 -11 0 127.89 4.10 -3 -11 0 120.19 4.20 3 -11 0 126.49 4.10 3 11 0 125.39 4.10 -3 11 0 124.09 4.20 -3 11 0 125.79 4.30 3 11 0 119.19 4.20 -3 11 0 121.49 4.00 3 11 0 120.99 4.30 3 11 0 120.49 4.00 -3 11 0 121.69 4.00 -4 -11 0 26.10 2.10 -4 -11 0 25.30 2.00 -4 -11 0 24.10 1.80 4 -11 0 28.80 2.00 -4 -11 0 26.40 1.90 4 -11 0 27.30 1.90 4 -11 0 28.30 1.80 4 -11 0 27.40 1.90 4 11 0 27.80 2.00 4 11 0 28.10 1.80 4 11 0 29.50 1.90 -4 11 0 30.30 2.00 -4 11 0 28.50 1.70 -4 11 0 27.40 1.80 -4 11 0 29.10 2.00 4 11 0 30.70 2.10 5 -11 0 1.10 0.90 5 -11 0 1.20 0.70 5 -11 0 1.60 0.80 -5 -11 0 1.00 1.00 -5 -11 0 -0.30 0.70 -5 -11 0 1.70 0.80 5 -11 0 1.10 0.90 -5 -11 0 1.90 0.90 5 11 0 1.20 1.00 5 11 0 0.20 0.80 5 11 0 0.10 0.80 5 11 0 0.00 0.80 -5 11 0 0.90 0.90 -5 11 0 0.50 0.80 -5 11 0 1.50 0.70 -5 11 0 -0.20 0.80 -6 -11 0 14.30 1.60 -6 -11 0 12.80 1.80 6 -11 0 12.80 1.50 -6 -11 0 10.90 1.30 6 -11 0 9.90 1.30 -6 -11 0 12.90 1.50 6 -11 0 9.50 1.30 6 -11 0 11.40 1.30 -6 11 0 12.80 1.50 -6 11 0 12.20 1.50 6 11 0 15.20 1.80 -6 11 0 11.60 1.20 6 11 0 11.60 1.30 -6 11 0 13.70 1.60 6 11 0 10.20 1.40 6 11 0 11.70 1.60 -7 -11 0 18.80 1.90 7 -11 0 23.10 2.10 -7 -11 0 21.00 2.10 -7 -11 0 19.20 2.30 7 -11 0 18.70 1.90 7 -11 0 19.50 1.80 -7 -11 0 17.30 2.10 -7 11 0 18.60 2.00 7 11 0 18.10 2.30 7 11 0 19.20 1.80 -7 11 0 22.50 1.80 7 11 0 19.10 2.40 -7 11 0 22.70 1.90 7 11 0 19.10 2.10 8 -11 0 33.00 2.70 8 -11 0 34.00 2.20 8 -11 0 35.00 2.60 -8 -11 0 34.80 2.80 8 -11 0 32.20 2.50 -8 -11 0 36.10 3.60 -8 -11 0 23.40 3.20 8 11 0 36.70 2.30 8 11 0 35.70 2.70 -8 11 0 35.20 2.20 8 11 0 32.60 2.50 8 11 0 30.90 2.60 -8 11 0 36.30 2.40 -8 11 0 30.50 2.50 9 -11 0 13.20 1.60 9 -11 0 16.30 2.00 9 -11 0 19.20 2.40 -9 -11 0 14.40 1.80 -9 -11 0 15.40 1.80 -9 -11 0 15.10 1.70 9 -11 0 19.60 2.10 9 11 0 14.80 1.80 -9 11 0 14.00 1.50 -9 11 0 17.00 1.80 9 11 0 13.50 1.80 9 11 0 13.00 1.70 -9 11 0 14.60 1.70 10 -11 0 70.49 3.50 -10 -11 0 77.19 3.80 -10 -11 0 70.29 3.90 10 -11 0 68.09 3.70 10 -11 0 74.79 3.70 -10 -11 0 71.99 4.10 10 11 0 76.69 4.30 10 11 0 72.09 3.50 10 11 0 69.39 4.10 -10 11 0 75.09 3.60 -10 11 0 76.19 3.90 11 -11 0 10.30 1.90 11 -11 0 16.40 2.00 -11 -11 0 15.60 2.50 -11 -11 0 11.40 1.90 -11 -11 0 14.60 2.10 11 -11 0 17.50 2.40 -11 -11 0 8.30 1.70 11 -11 0 11.80 1.70 -11 11 0 11.60 1.60 -11 11 0 8.40 1.70 -11 11 0 11.70 2.00 11 11 0 15.60 2.40 11 11 0 11.70 2.00 11 11 0 11.40 2.00 11 11 0 10.40 1.60 12 -11 0 1.30 1.50 12 -11 0 0.60 2.00 -12 -11 0 -1.50 1.70 -12 -11 0 3.00 2.10 12 -11 0 2.80 1.60 -12 -11 0 1.60 1.90 -12 -11 0 3.40 1.60 12 -11 0 4.00 1.90 12 11 0 3.90 1.90 12 11 0 2.40 1.60 12 11 0 1.40 1.80 12 11 0 3.40 2.10 -12 11 0 2.80 1.40 -12 11 0 1.30 1.70 -12 11 0 2.30 2.00 -12 11 0 2.70 1.70 13 -11 0 2.60 1.70 -13 -11 0 10.20 2.30 -13 -11 0 8.90 2.70 13 -11 0 8.10 2.30 -13 -11 0 4.30 1.90 13 -11 0 6.40 2.30 -13 -11 0 9.30 2.40 13 -11 0 7.00 2.00 -13 11 0 6.20 2.40 -13 11 0 9.20 2.30 -13 11 0 7.60 2.10 13 11 0 5.50 2.50 13 11 0 9.00 2.30 13 11 0 5.30 2.20 -13 11 0 6.30 1.80 13 11 0 5.80 1.80 -14 -11 0 11.50 2.80 14 -11 0 20.30 2.60 14 -11 0 18.90 3.20 14 -11 0 15.90 2.80 -14 -11 0 17.00 3.00 -14 -11 0 15.20 3.10 -14 11 0 19.80 2.70 -14 11 0 16.30 2.40 -14 11 0 25.90 3.20 14 11 0 19.80 2.50 14 11 0 18.60 3.00 0 -12 0 42.50 2.30 0 -12 0 48.30 2.50 0 -12 0 41.90 2.10 0 -12 0 43.70 2.30 0 12 0 42.80 2.20 0 12 0 42.80 2.30 0 12 0 45.00 2.40 0 12 0 44.70 2.10 1 -12 0 -0.10 0.60 -1 -12 0 0.20 0.80 -1 -12 0 0.40 0.70 1 -12 0 1.10 0.80 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1.70 -1 13 0 21.50 1.90 1 13 0 18.20 1.60 1 13 0 20.30 1.90 -1 13 0 19.00 1.60 1 13 0 18.80 1.80 -2 -13 0 -1.60 0.70 2 -13 0 0.00 0.80 -2 -13 0 0.00 0.80 2 -13 0 -0.20 1.00 2 -13 0 -0.20 0.90 -2 -13 0 -0.30 1.00 2 -13 0 0.10 0.70 -2 -13 0 0.20 0.90 2 13 0 0.60 1.00 -2 13 0 0.50 0.80 -2 13 0 0.10 0.70 2 13 0 1.20 0.90 -2 13 0 -0.60 0.90 2 13 0 1.10 0.80 -2 13 0 -0.10 0.90 2 13 0 -1.10 0.80 -3 -13 0 163.08 5.50 3 -13 0 165.68 5.60 -3 -13 0 157.78 6.20 3 -13 0 169.58 5.40 -3 -13 0 162.08 5.60 3 -13 0 173.18 6.30 -3 -13 0 167.48 5.40 3 -13 0 164.58 5.50 -3 13 0 157.08 5.50 3 13 0 166.78 5.60 3 13 0 167.88 5.30 3 13 0 168.08 5.40 -3 13 0 171.48 5.50 -3 13 0 164.28 5.20 -3 13 0 174.18 5.30 -4 -13 0 36.30 2.60 -4 -13 0 41.10 2.60 4 -13 0 39.90 2.30 -4 -13 0 44.00 2.50 4 -13 0 43.70 2.70 4 -13 0 36.90 2.40 -4 -13 0 42.00 2.40 4 -13 0 38.20 2.50 4 13 0 37.70 2.20 4 13 0 37.00 2.50 -4 13 0 43.40 2.60 -4 13 0 43.80 2.40 4 13 0 41.50 2.40 -4 13 0 41.20 2.20 5 -13 0 22.20 2.10 -5 -13 0 16.00 1.80 5 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3.50 -9 -13 0 46.60 3.10 -9 -13 0 37.70 3.30 9 -13 0 53.59 3.10 -9 -13 0 46.20 3.70 -9 13 0 50.39 3.30 -9 13 0 54.49 3.60 9 13 0 52.39 3.00 -9 13 0 42.40 3.00 -9 13 0 33.90 4.30 9 13 0 42.90 4.20 9 13 0 52.19 3.70 -10 -13 0 13.20 2.20 -10 -13 0 9.90 2.10 -10 -13 0 13.50 2.10 10 -13 0 12.20 1.80 -10 -13 0 8.50 1.70 10 -13 0 13.70 1.90 10 -13 0 14.60 2.30 10 13 0 12.00 2.30 10 13 0 15.20 2.00 -10 13 0 14.70 2.30 -10 13 0 11.10 1.60 10 13 0 9.50 1.90 -10 13 0 15.90 2.30 10 13 0 12.20 1.70 -11 -13 0 6.50 1.90 -11 -13 0 5.40 2.10 11 -13 0 5.20 1.90 11 -13 0 5.70 1.70 -11 -13 0 3.30 2.40 11 -13 0 6.90 2.10 -11 -13 0 2.30 1.80 11 -13 0 6.10 1.80 -11 13 0 5.70 1.60 11 13 0 3.30 1.60 -11 13 0 5.00 2.30 -11 13 0 3.90 1.80 -11 13 0 4.30 2.00 11 13 0 5.30 2.00 11 13 0 4.80 2.20 11 13 0 4.70 2.00 12 -13 0 0.60 1.60 12 -13 0 -2.50 2.20 -12 -13 0 -2.80 1.60 -12 -13 0 1.60 2.30 12 -13 0 1.50 1.70 -12 -13 0 -1.00 1.80 12 -13 0 1.30 2.00 -12 13 0 0.40 1.90 12 13 0 -2.20 2.10 12 13 0 -0.70 1.60 12 13 0 0.70 2.10 -12 13 0 1.70 2.00 12 13 0 -0.40 1.90 -12 13 0 -0.90 1.60 13 -13 0 -1.50 2.70 -13 -13 0 -1.40 2.20 13 -13 0 0.80 2.10 -13 -13 0 -1.40 2.60 -13 -13 0 -4.80 2.60 13 -13 0 5.10 2.20 13 13 0 -1.70 2.90 -13 13 0 -0.40 2.20 13 13 0 5.80 2.70 13 13 0 2.50 2.00 -13 13 0 -1.00 1.90 -13 13 0 -0.80 2.30 0 -14 0 0.90 1.00 0 -14 0 1.10 1.00 0 -14 0 1.40 1.00 0 -14 0 0.20 0.80 0 14 0 0.30 0.90 0 14 0 0.80 0.80 0 14 0 -0.20 0.90 -1 -14 0 137.89 5.00 -1 -14 0 142.89 5.00 1 -14 0 142.99 5.00 1 -14 0 140.99 4.90 1 -14 0 143.39 4.80 -1 -14 0 135.39 4.80 -1 -14 0 138.69 5.10 1 -14 0 150.18 5.10 -1 14 0 148.19 5.10 1 14 0 137.69 4.80 1 14 0 147.09 4.70 -1 14 0 143.09 4.70 1 14 0 146.79 5.10 -1 14 0 143.19 4.70 2 -14 0 10.50 1.40 -2 -14 0 9.70 1.40 2 -14 0 9.90 1.20 -2 -14 0 11.10 1.30 -2 -14 0 9.30 1.50 -2 -14 0 9.90 1.40 2 -14 0 10.50 1.60 2 -14 0 9.10 1.30 2 14 0 11.00 1.40 -2 14 0 12.20 1.40 2 14 0 11.20 1.30 -2 14 0 10.90 1.20 2 14 0 10.40 1.50 -2 14 0 11.00 1.50 -3 -14 0 19.30 1.90 3 -14 0 20.60 1.80 -3 -14 0 24.00 2.30 3 -14 0 19.60 2.00 3 -14 0 20.50 2.20 -3 -14 0 21.70 2.40 -3 -14 0 25.40 2.40 3 -14 0 22.70 2.30 -3 14 0 24.90 2.20 3 14 0 18.30 2.10 -3 14 0 20.90 1.80 3 14 0 19.40 1.90 -3 14 0 19.80 1.90 3 14 0 23.50 2.20 4 -14 0 10.20 1.50 4 -14 0 9.10 1.40 -4 -14 0 8.10 1.40 -4 -14 0 10.70 1.40 4 -14 0 9.30 1.20 -4 -14 0 11.30 1.70 -4 -14 0 10.20 1.60 4 -14 0 8.50 1.60 4 14 0 10.90 1.70 4 14 0 11.70 1.30 -4 14 0 9.80 1.20 -4 14 0 10.00 1.30 4 14 0 10.10 1.60 -4 14 0 11.40 1.50 -5 -14 0 11.30 1.50 5 -14 0 11.80 1.50 -5 -14 0 12.00 1.60 -5 -14 0 14.00 2.00 5 -14 0 13.80 1.80 -5 -14 0 10.30 1.40 5 -14 0 10.60 1.60 5 14 0 11.60 1.60 5 14 0 10.40 1.60 5 14 0 9.80 1.20 -5 14 0 13.20 1.50 -5 14 0 11.50 1.50 -5 14 0 15.50 1.70 -6 -14 0 -0.40 1.00 6 -14 0 -0.10 1.20 6 -14 0 0.60 1.00 6 -14 0 0.90 1.00 -6 -14 0 -0.10 1.20 -6 -14 0 1.10 1.40 6 -14 0 -1.60 1.10 -6 -14 0 -0.10 1.10 6 14 0 -0.30 0.90 -6 14 0 0.60 0.90 6 14 0 0.10 1.20 -6 14 0 0.50 1.20 6 14 0 -0.90 1.10 -7 -14 0 64.39 3.90 7 -14 0 60.59 3.50 -7 -14 0 58.29 3.50 -7 -14 0 59.39 3.70 -7 -14 0 63.19 3.40 7 -14 0 62.99 3.50 7 -14 0 64.19 3.70 7 -14 0 64.49 3.30 7 14 0 64.79 3.70 7 14 0 59.99 3.10 -7 14 0 63.49 3.00 -7 14 0 64.29 3.40 -7 14 0 66.39 3.30 8 -14 0 3.70 1.40 8 -14 0 4.40 1.60 8 -14 0 4.10 3.00 -8 -14 0 2.20 1.70 -8 -14 0 2.60 1.50 -8 -14 0 2.50 1.40 8 -14 0 2.80 1.40 -8 -14 0 1.10 1.40 -8 14 0 4.60 1.40 -8 14 0 2.60 1.60 -8 14 0 2.30 1.40 8 14 0 0.00 1.70 8 14 0 4.00 1.70 -8 14 0 0.60 1.30 8 14 0 3.20 1.30 9 -14 0 5.50 1.90 -9 -14 0 6.00 1.60 -9 -14 0 7.20 1.80 9 -14 0 6.40 1.50 9 -14 0 3.40 1.50 9 -14 0 5.90 1.80 -9 -14 0 5.00 1.90 -9 -14 0 6.40 2.10 9 14 0 4.70 1.80 -9 14 0 6.70 1.60 -9 14 0 5.70 1.90 9 14 0 4.30 1.40 -9 14 0 0.40 1.40 9 14 0 5.40 1.80 -9 14 0 3.90 1.40 9 14 0 7.00 1.90 -10 -14 0 17.70 2.40 10 -14 0 24.50 2.90 10 -14 0 18.20 2.20 -10 -14 0 31.10 4.00 10 -14 0 21.40 2.40 -10 -14 0 22.90 2.70 10 -14 0 23.90 2.70 -10 -14 0 23.60 2.50 10 14 0 23.50 2.80 10 14 0 20.70 2.30 10 14 0 24.70 3.00 -10 14 0 25.70 3.00 -10 14 0 23.10 2.60 10 14 0 22.60 2.60 -10 14 0 28.10 2.70 11 -14 0 18.00 2.50 -11 -14 0 23.70 3.10 11 -14 0 20.90 2.40 -11 -14 0 26.60 3.30 -11 -14 0 22.70 2.70 11 -14 0 22.60 2.40 11 14 0 26.00 3.00 -11 14 0 21.20 2.50 -11 14 0 21.80 2.70 -11 14 0 24.40 2.80 11 14 0 16.50 2.60 11 14 0 22.30 2.80 11 14 0 19.20 2.30 -11 14 0 27.20 3.10 12 -14 0 16.60 2.50 -12 -14 0 19.30 2.70 -12 -14 0 17.90 2.60 -12 -14 0 18.40 3.00 12 -14 0 22.60 2.70 12 14 0 24.00 2.60 -12 14 0 19.60 3.00 -12 14 0 27.50 2.80 12 14 0 24.10 3.10 12 14 0 19.80 3.00 -12 14 0 22.10 2.50 -13 -14 0 -1.30 2.90 13 -14 0 -0.20 2.60 13 -14 0 3.90 3.00 -13 -14 0 -3.70 2.80 13 14 0 0.10 2.10 -13 14 0 0.10 2.40 -13 14 0 4.60 2.60 -13 14 0 4.30 2.10 13 14 0 3.20 2.80 0 -15 0 -0.40 1.00 0 -15 0 1.30 1.00 0 -15 0 0.30 1.10 0 -15 0 0.10 1.10 0 15 0 1.00 1.10 0 15 0 1.10 0.90 -1 -15 0 115.99 4.70 -1 -15 0 115.39 4.50 -1 -15 0 118.99 4.60 1 -15 0 120.49 4.60 1 -15 0 115.89 4.70 1 -15 0 113.69 4.40 -1 -15 0 119.59 4.60 1 -15 0 126.19 4.60 -1 15 0 120.59 4.60 1 15 0 118.29 4.20 1 15 0 120.99 4.40 1 15 0 118.29 4.60 -1 15 0 123.69 4.30 -1 15 0 120.19 4.20 2 -15 0 42.70 2.80 2 -15 0 39.90 2.70 -2 -15 0 41.20 2.80 2 -15 0 42.80 2.60 -2 -15 0 37.60 2.60 2 -15 0 40.50 2.80 -2 -15 0 42.70 3.00 2 15 0 34.50 2.50 -2 15 0 43.10 2.30 2 15 0 36.60 2.30 2 15 0 39.10 2.80 -2 15 0 40.40 2.70 -2 15 0 42.10 2.50 3 -15 0 -0.40 1.20 3 -15 0 0.60 1.00 -3 -15 0 1.10 1.10 3 -15 0 0.20 1.20 -3 -15 0 -0.50 1.20 -3 -15 0 0.00 1.30 -3 -15 0 1.10 1.10 -3 15 0 2.10 1.10 3 15 0 1.90 1.20 -3 15 0 1.10 0.90 -3 15 0 -0.50 1.00 3 15 0 0.20 1.00 -4 -15 0 52.19 3.10 4 -15 0 54.59 3.30 4 -15 0 51.09 3.10 -4 -15 0 51.59 3.00 -4 -15 0 54.29 3.20 -4 -15 0 49.30 3.40 4 -15 0 50.79 2.80 4 -15 0 51.69 3.00 -4 15 0 55.99 2.90 -4 15 0 53.79 2.70 4 15 0 51.19 3.10 4 15 0 53.89 3.00 4 15 0 47.70 2.70 -4 15 0 51.79 3.10 5 -15 0 1.10 1.00 -5 -15 0 2.70 1.70 5 -15 0 1.50 1.30 5 -15 0 0.60 1.40 -5 -15 0 0.40 1.00 -5 -15 0 0.60 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5 4 33.60 3.00 -13 5 4 28.50 2.70 -13 5 4 30.70 3.30 -13 5 4 33.50 3.00 13 5 -4 33.70 2.60 13 5 -4 36.10 3.10 -12 -5 4 -0.60 1.10 12 -5 -4 0.30 1.00 -12 -5 4 0.10 1.00 -12 -5 4 0.60 1.70 -12 -5 4 -0.10 1.10 12 -5 -4 0.70 1.40 -12 5 4 -1.90 1.00 12 5 -4 0.70 1.20 12 5 -4 -0.20 0.90 12 5 -4 -1.10 1.10 -12 5 4 -0.10 1.20 -12 5 4 1.10 1.30 12 5 -4 0.60 1.10 11 -5 -4 139.39 4.90 11 -5 -4 129.39 5.20 11 -5 -4 141.69 5.20 -11 -5 4 147.19 5.20 -11 -5 4 148.19 5.10 -11 -5 4 143.69 5.20 -11 -5 4 137.69 5.00 11 -5 -4 144.39 5.10 -11 5 4 134.99 4.90 11 5 -4 138.89 4.80 -11 5 4 144.99 5.40 -11 5 4 144.39 5.20 -11 5 4 148.09 5.10 11 5 -4 153.18 5.30 10 -5 -4 9.80 1.40 10 -5 -4 10.60 1.30 10 -5 -4 8.20 1.50 -10 -5 4 9.60 1.40 10 -5 -4 9.90 1.40 -10 -5 4 7.50 1.20 -10 -5 4 10.50 1.50 10 5 -4 8.50 1.20 -10 5 4 8.90 1.30 10 5 -4 10.60 1.40 -10 5 4 8.30 1.10 10 5 -4 9.60 1.10 -10 5 4 9.20 1.50 -10 5 4 11.60 1.50 10 5 -4 6.10 1.30 -9 -5 4 6.70 1.00 9 -5 -4 8.00 1.20 -9 -5 4 8.00 1.20 9 -5 -4 8.00 1.30 -9 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6 4 35.00 2.90 13 6 -4 36.60 2.70 12 -6 -4 7.20 1.80 -12 -6 4 4.70 1.50 12 -6 -4 6.60 1.40 -12 -6 4 3.00 1.20 -12 -6 4 6.90 1.60 -12 -6 4 4.70 1.50 12 -6 -4 4.00 1.20 12 6 -4 4.90 1.40 12 6 -4 4.10 1.40 -12 6 4 6.60 1.40 -12 6 4 6.40 1.50 -11 -6 4 -0.50 1.40 11 -6 -4 0.20 1.00 -11 -6 4 -1.40 1.00 -11 -6 4 0.30 1.10 11 -6 -4 0.10 1.20 -11 6 4 1.50 1.20 11 6 -4 2.00 1.10 11 6 -4 0.10 1.00 11 6 -4 0.20 0.90 -11 6 4 -0.70 1.00 -11 6 4 0.80 0.90 10 -6 -4 5.30 1.00 -10 -6 4 7.70 1.20 10 -6 -4 6.40 1.30 -10 -6 4 6.30 1.20 -10 -6 4 7.10 1.30 10 -6 -4 5.40 1.20 10 -6 -4 4.60 1.30 -10 -6 4 6.30 1.20 -10 6 4 4.80 1.10 10 6 -4 6.80 1.10 -10 6 4 7.50 1.20 10 6 -4 5.00 1.10 -10 6 4 4.60 1.00 10 6 -4 2.30 1.10 10 6 -4 6.40 1.30 -9 -6 4 85.49 3.50 -9 -6 4 93.79 3.50 -9 -6 4 87.59 3.50 9 -6 -4 92.09 3.50 9 -6 -4 89.19 3.40 -9 -6 4 90.99 3.60 9 -6 -4 86.19 3.60 9 -6 -4 84.29 3.70 9 6 -4 83.39 3.60 9 6 -4 87.89 3.30 -9 6 4 86.69 3.70 -9 6 4 90.59 3.70 9 6 -4 93.89 3.70 9 6 -4 94.19 3.40 -9 6 4 92.29 3.50 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0.90 -2 11 4 1.00 0.80 2 11 -4 1.30 0.80 -2 11 4 -0.40 0.60 2 11 -4 -0.60 0.60 -2 11 4 0.00 0.70 -1 -11 4 72.39 2.80 1 -11 -4 73.59 3.00 1 -11 -4 75.59 3.20 -1 -11 4 75.89 2.80 1 -11 -4 75.79 2.90 1 -11 -4 72.99 3.10 -1 -11 4 74.99 2.70 -1 -11 4 73.29 2.90 -1 11 4 71.89 3.10 1 11 -4 72.99 2.80 1 11 -4 75.19 2.40 -1 11 4 76.99 3.00 -1 11 4 77.19 3.00 -1 11 4 76.69 3.20 1 11 -4 75.39 2.50 1 11 -4 75.79 2.90 0 -11 -4 144.99 4.80 0 -11 4 140.49 4.40 0 -11 4 142.89 4.40 0 -11 -4 140.29 4.60 0 -11 4 145.09 4.50 0 -11 -4 142.29 4.60 0 -11 4 140.39 4.40 0 -11 -4 148.09 4.90 0 11 4 138.39 4.80 0 11 -4 141.49 4.50 0 11 -4 142.49 4.00 0 11 4 144.29 4.90 0 11 -4 136.99 4.10 0 11 4 143.49 4.60 0 11 -4 132.39 4.40 0 11 4 146.09 4.70 1 -11 4 325.77 9.00 -1 -11 -4 330.97 9.40 -1 -11 -4 329.07 9.20 -1 -11 -4 329.27 9.40 1 -11 4 325.27 8.90 1 -11 4 324.07 8.90 -1 -11 -4 317.07 9.10 1 -11 4 320.07 8.80 1 11 4 320.07 9.30 -1 11 -4 321.17 8.50 -1 11 -4 325.07 8.90 1 11 4 328.17 9.40 1 11 4 325.57 9.10 -1 11 -4 332.77 9.00 -1 11 -4 317.97 8.50 1 11 4 329.57 9.20 -2 -11 -4 25.30 2.00 -2 -11 -4 21.90 2.10 -2 -11 -4 22.60 1.80 2 -11 4 22.60 1.50 -2 -11 -4 22.80 1.90 2 -11 4 24.10 1.60 2 -11 4 23.10 1.70 2 -11 4 23.80 1.60 -2 11 -4 24.20 1.60 2 11 4 24.40 2.10 2 11 4 21.60 1.90 -2 11 -4 22.50 1.30 -2 11 -4 24.60 1.30 -2 11 -4 21.90 1.70 2 11 4 21.10 1.90 2 11 4 20.30 1.80 -3 -11 -4 16.40 1.70 3 -11 4 16.80 1.50 -3 -11 -4 18.20 1.90 3 -11 4 16.80 1.40 3 -11 4 16.80 1.40 -3 -11 -4 21.80 1.90 -3 -11 -4 18.90 2.10 3 -11 4 18.00 1.60 -3 11 -4 17.30 1.20 3 11 4 16.50 1.80 3 11 4 15.00 1.80 3 11 4 12.90 1.60 -3 11 -4 18.90 1.70 3 11 4 16.10 2.00 -3 11 -4 17.30 1.20 -3 11 -4 19.70 1.50 4 -11 4 4.50 1.00 -4 -11 -4 6.00 1.10 4 -11 4 4.30 0.90 -4 -11 -4 3.40 1.50 4 -11 4 4.60 0.80 -4 -11 -4 4.50 1.30 -4 -11 -4 3.80 1.10 4 -11 4 3.00 0.80 4 11 4 3.80 1.00 -4 11 -4 4.70 0.90 4 11 4 4.40 1.10 -4 11 -4 5.60 0.70 4 11 4 5.60 1.20 -4 11 -4 5.50 1.00 4 11 4 3.60 1.00 -4 11 -4 6.20 0.80 -5 -11 -4 0.40 1.10 5 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6.80 2.40 12 -11 4 6.40 1.70 -12 -11 -4 3.80 2.00 12 -11 4 5.80 1.70 12 -11 4 4.70 2.20 -12 -11 -4 8.40 2.40 12 11 4 3.30 1.70 12 11 4 3.00 2.10 12 11 4 9.00 2.40 -12 11 -4 2.30 2.00 -12 11 -4 5.70 1.80 12 11 4 5.10 2.40 -12 11 -4 7.30 2.20 -13 -11 -4 6.30 2.00 -13 -11 -4 4.70 2.40 13 -11 4 2.40 1.70 13 -11 4 1.80 2.40 13 -11 4 2.20 2.00 13 11 4 3.00 1.90 13 11 4 -2.30 2.80 -13 11 -4 1.40 1.70 13 11 4 2.10 2.20 14 -12 -4 5.80 2.70 -14 -12 4 3.00 2.30 14 -12 -4 0.50 2.10 14 -12 -4 1.40 2.70 -14 -12 4 3.90 2.80 -14 -12 4 1.90 2.30 -14 12 4 8.20 2.70 14 12 -4 -5.10 2.30 -14 12 4 6.10 2.20 14 12 -4 7.20 2.50 14 12 -4 4.40 2.00 13 -12 -4 80.49 5.50 -13 -12 4 79.49 5.40 -13 -12 4 66.99 4.40 13 -12 -4 78.09 4.90 -13 -12 4 80.49 4.80 13 -12 -4 79.39 4.50 -13 -12 4 87.59 7.30 13 12 -4 80.49 4.80 -13 12 4 78.39 4.50 13 12 -4 77.59 5.10 13 12 -4 72.99 4.20 -13 12 4 81.39 6.90 -13 12 4 81.19 5.10 -13 12 4 86.59 5.10 12 -12 -4 3.10 2.20 -12 -12 4 0.00 1.50 -12 -12 4 3.10 1.80 12 -12 -4 -2.10 1.80 -12 -12 4 -0.80 1.70 12 -12 -4 -0.90 1.70 -12 -12 4 2.50 2.10 12 -12 -4 -0.40 1.50 12 12 -4 0.10 1.70 -12 12 4 1.50 1.90 -12 12 4 1.80 1.90 12 12 -4 2.30 2.10 -12 12 4 -0.90 1.50 12 12 -4 -0.80 1.30 -12 12 4 1.60 2.00 12 12 -4 1.10 1.80 11 -12 -4 11.60 2.10 11 -12 -4 11.20 2.30 -11 -12 4 12.00 2.10 -11 -12 4 11.40 1.90 -11 -12 4 15.10 2.30 11 -12 -4 14.00 2.00 -11 -12 4 16.80 2.10 11 -12 -4 13.60 2.00 11 12 -4 7.90 2.00 11 12 -4 11.90 1.70 11 12 -4 16.90 2.20 -11 12 4 11.40 2.40 -11 12 4 14.30 2.10 -11 12 4 14.40 2.00 -11 12 4 10.50 1.90 -10 -12 4 0.30 1.40 -10 -12 4 1.70 1.30 10 -12 -4 0.10 1.30 10 -12 -4 1.40 1.40 -10 -12 4 4.60 2.10 10 -12 -4 -0.40 1.20 -10 -12 4 4.10 1.40 10 12 -4 0.90 1.40 10 12 -4 2.10 1.10 -10 12 4 0.70 1.50 -10 12 4 2.60 1.50 10 12 -4 2.30 1.50 10 12 -4 2.20 1.40 -10 12 4 0.90 1.20 -10 12 4 0.00 1.60 9 -12 -4 28.80 2.60 -9 -12 4 30.10 2.70 -9 -12 4 31.90 2.90 -9 -12 4 32.10 2.50 9 -12 -4 31.50 2.80 -9 -12 4 31.10 2.70 -9 12 4 29.60 2.50 -9 12 4 25.00 3.10 -9 12 4 31.50 2.80 9 12 -4 30.30 2.70 9 12 -4 32.70 2.30 -8 -12 4 38.40 2.80 8 -12 -4 37.30 2.80 8 -12 -4 39.50 3.20 -8 -12 4 37.60 2.70 -8 -12 4 37.30 2.60 8 -12 -4 39.00 2.60 -8 12 4 35.90 3.00 8 12 -4 35.30 2.70 -8 12 4 37.80 2.70 8 12 -4 40.40 2.50 -8 12 4 32.40 2.40 8 12 -4 39.90 2.20 -7 -12 4 17.50 2.10 -7 -12 4 16.40 1.80 -7 -12 4 19.10 2.30 7 -12 -4 15.50 3.00 -7 -12 4 15.70 2.40 7 -12 -4 14.90 2.00 7 12 -4 17.30 2.10 -7 12 4 13.10 1.60 -7 12 4 16.30 1.90 -7 12 4 18.00 2.20 7 12 -4 16.90 1.60 -7 12 4 15.10 1.60 7 12 -4 16.40 1.80 6 -12 -4 1.80 1.20 -6 -12 4 -0.10 0.80 -6 -12 4 1.80 1.10 -6 -12 4 1.70 1.80 -6 -12 4 1.20 0.90 6 -12 -4 -0.70 0.80 6 -12 -4 0.90 0.90 -6 12 4 0.80 1.10 -6 12 4 1.20 1.10 6 12 -4 0.50 0.90 6 12 -4 2.00 0.90 -6 12 4 0.90 0.90 6 12 -4 0.20 0.70 6 12 -4 0.70 1.10 -6 12 4 -0.60 0.80 -5 -12 4 4.70 1.10 -5 -12 4 5.20 1.00 -5 -12 4 5.50 1.00 -5 -12 4 7.00 1.20 5 -12 -4 6.30 1.10 5 -12 -4 5.50 1.10 5 -12 -4 2.40 1.00 5 -12 -4 5.40 1.30 -5 12 4 3.10 1.80 5 12 -4 5.90 1.10 -5 12 4 3.00 0.90 5 12 -4 5.40 0.90 -5 12 4 6.40 1.40 5 12 -4 4.80 1.00 -5 12 4 3.40 1.10 5 12 -4 5.00 1.10 -4 -12 4 2.70 0.80 4 -12 -4 3.60 1.00 -4 -12 4 3.20 0.80 4 -12 -4 3.40 0.90 -4 -12 4 2.70 1.00 -4 -12 4 3.80 1.10 4 -12 -4 2.70 1.10 4 -12 -4 2.10 1.20 4 12 -4 3.10 0.90 4 12 -4 3.10 0.80 -4 12 4 3.90 1.00 4 12 -4 3.30 0.80 4 12 -4 2.80 1.10 -4 12 4 2.70 0.90 -4 12 4 4.10 1.10 -3 -12 4 41.00 2.20 3 -12 -4 42.80 2.30 -3 -12 4 41.80 2.20 3 -12 -4 39.00 2.80 -3 -12 4 38.10 2.10 3 -12 -4 44.00 2.50 3 -12 -4 46.20 2.70 -3 -12 4 43.90 2.30 -3 12 4 45.90 2.30 3 12 -4 41.40 2.20 3 12 -4 45.10 2.30 -3 12 4 37.10 2.40 -3 12 4 41.80 2.40 3 12 -4 42.90 1.90 -3 12 4 42.30 2.60 3 12 -4 42.50 1.90 2 -12 -4 12.40 1.50 -2 -12 4 10.50 1.20 2 -12 -4 11.10 1.40 -2 -12 4 10.70 1.30 -2 -12 4 12.00 1.40 -2 -12 4 10.90 1.40 2 -12 -4 10.70 1.30 2 -12 -4 9.30 1.30 2 12 -4 11.40 1.10 2 12 -4 10.10 1.20 -2 12 4 9.90 1.40 2 12 -4 10.60 1.00 -2 12 4 12.80 1.60 -2 12 4 10.00 1.30 -2 12 4 9.70 1.20 2 12 -4 11.40 1.30 -1 -12 4 83.49 3.10 -1 -12 4 82.69 3.20 1 -12 -4 83.09 3.50 -1 -12 4 83.99 3.10 1 -12 -4 78.59 3.60 1 -12 -4 81.39 3.40 -1 -12 4 85.79 3.20 1 -12 -4 80.89 3.30 -1 12 4 84.89 3.40 1 12 -4 84.99 2.80 1 12 -4 86.39 2.80 -1 12 4 85.69 3.60 -1 12 4 86.29 3.30 1 12 -4 83.59 3.20 1 12 -4 83.99 3.20 0 -12 -4 71.69 3.30 0 -12 -4 68.39 2.90 0 -12 4 65.99 2.70 0 -12 4 70.49 2.70 0 -12 -4 65.29 3.10 0 -12 4 69.29 2.80 0 -12 4 65.69 2.70 0 -12 -4 64.89 3.00 0 12 4 65.99 3.10 0 12 -4 66.89 2.30 0 12 4 67.99 3.00 0 12 -4 63.29 2.70 0 12 4 72.09 2.90 0 12 -4 64.49 2.80 0 12 -4 63.99 2.40 0 12 4 66.89 3.20 1 -12 4 48.50 2.30 1 -12 4 51.19 2.40 1 -12 4 52.09 2.30 -1 -12 -4 48.30 2.60 1 -12 4 50.99 2.30 -1 -12 -4 51.69 2.70 -1 -12 -4 47.40 2.50 1 12 4 51.99 2.70 1 12 4 48.50 2.50 1 12 4 47.90 2.80 -1 12 -4 50.99 2.00 1 12 4 49.60 2.60 -1 12 -4 45.60 2.30 -1 12 -4 48.80 1.90 -1 12 -4 49.80 2.40 2 -12 4 14.00 1.60 -2 -12 -4 15.50 1.80 2 -12 4 13.50 1.40 -2 -12 -4 11.40 1.30 2 -12 4 13.50 1.60 -2 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12 12 4 13.30 2.60 -12 12 -4 9.70 2.00 12 12 4 10.90 2.10 13 -12 4 7.30 2.20 -13 -12 -4 9.50 2.80 -13 -12 -4 7.90 2.60 13 -12 4 8.50 2.60 13 -12 4 8.50 2.30 -13 12 -4 4.80 1.80 13 12 4 11.40 2.80 -13 12 -4 6.50 2.60 13 12 4 6.40 2.60 14 -13 -4 -2.90 3.00 -14 -13 4 2.20 3.00 14 13 -4 1.40 2.00 14 13 -4 -3.20 2.50 -14 13 4 5.30 2.50 14 13 -4 2.20 2.80 -14 13 4 0.80 2.60 13 -13 -4 -1.50 2.00 -13 -13 4 0.50 2.60 13 -13 -4 0.30 2.00 -13 -13 4 1.20 1.90 13 -13 -4 3.50 2.90 -13 -13 4 0.50 2.10 -13 13 4 4.30 1.90 13 13 -4 1.70 2.40 13 13 -4 2.20 1.80 -13 13 4 3.50 2.50 -13 13 4 3.20 2.30 13 13 -4 -3.20 2.20 12 -13 -4 3.10 1.70 -12 -13 4 1.70 1.70 12 -13 -4 -0.90 1.90 -12 -13 4 2.10 2.10 -12 -13 4 2.40 1.70 12 -13 -4 -4.20 1.70 -12 -13 4 -0.80 2.00 12 13 -4 -3.90 1.80 -12 13 4 -0.40 1.60 12 13 -4 1.30 2.10 -12 13 4 5.00 2.20 -12 13 4 2.50 2.10 12 13 -4 0.30 1.90 -12 13 4 0.40 2.00 12 13 -4 1.30 1.50 11 -13 -4 47.20 3.80 -11 -13 4 46.50 3.60 -11 -13 4 53.09 3.80 -11 -13 4 44.90 4.10 11 -13 -4 51.09 3.90 11 -13 -4 49.30 3.50 -11 13 4 44.90 3.90 11 13 -4 46.50 3.10 11 13 -4 44.50 4.00 -11 13 4 55.09 3.50 -11 13 4 49.99 4.20 11 13 -4 48.20 3.80 -11 13 4 48.10 4.00 -10 -13 4 65.69 3.70 10 -13 -4 69.59 4.40 -10 -13 4 76.79 4.30 -10 -13 4 64.79 4.00 10 -13 -4 59.89 3.90 10 -13 -4 65.29 4.00 -10 -13 4 69.39 3.90 10 -13 -4 69.89 3.80 10 13 -4 65.59 4.00 -10 13 4 68.99 3.60 -10 13 4 65.79 4.00 10 13 -4 65.09 3.60 10 13 -4 64.19 3.80 -10 13 4 61.99 4.00 -10 13 4 66.49 4.30 10 13 -4 58.39 4.00 9 -13 -4 2.60 1.70 9 -13 -4 -0.20 1.40 -9 -13 4 4.40 1.60 -9 -13 4 -0.30 1.10 -9 -13 4 3.30 1.40 9 -13 -4 2.80 1.50 -9 -13 4 2.70 1.50 9 -13 -4 1.50 1.30 -9 13 4 0.00 1.60 9 13 -4 0.00 1.00 9 13 -4 1.20 1.30 9 13 -4 1.60 1.50 -9 13 4 0.60 1.20 9 13 -4 1.00 1.30 -9 13 4 3.80 1.50 -9 13 4 -0.90 1.40 8 -13 -4 1.50 1.10 8 -13 -4 -1.20 1.50 8 -13 -4 0.80 1.40 -8 -13 4 3.90 1.10 -8 -13 4 0.40 1.20 -8 -13 4 0.10 1.30 -8 -13 4 2.00 1.20 8 13 -4 4.30 1.40 8 13 -4 1.00 0.90 8 13 -4 1.90 1.20 -8 13 4 2.80 1.20 8 13 -4 2.30 1.30 -8 13 4 3.50 1.40 -8 13 4 3.10 1.70 7 -13 -4 7.80 1.40 -7 -13 4 6.90 1.50 7 -13 -4 8.30 1.40 7 -13 -4 7.60 1.60 -7 -13 4 6.50 1.30 -7 -13 4 7.60 1.80 -7 -13 4 9.00 1.60 -7 13 4 7.70 1.60 7 13 -4 8.60 1.30 -7 13 4 7.30 1.30 7 13 -4 7.10 1.10 7 13 -4 7.70 1.40 -7 13 4 6.50 1.20 -6 -13 4 57.49 3.00 6 -13 -4 56.99 4.00 6 -13 -4 58.19 3.00 -6 -13 4 60.49 2.90 -6 -13 4 64.19 3.20 6 -13 -4 60.99 3.60 -6 -13 4 62.29 3.10 -6 13 4 59.09 3.00 6 13 -4 58.59 3.10 -6 13 4 61.89 3.50 6 13 -4 60.39 2.60 -6 13 4 57.09 3.10 -6 13 4 54.29 3.10 6 13 -4 62.39 2.70 5 -13 -4 5.80 1.30 -5 -13 4 4.50 1.00 5 -13 -4 7.00 1.50 -5 -13 4 6.50 1.20 -5 -13 4 7.30 1.20 -5 -13 4 6.10 1.30 5 -13 -4 3.80 1.10 -5 13 4 5.10 1.50 5 13 -4 5.20 1.20 5 13 -4 6.20 1.20 -5 13 4 6.80 1.40 5 13 -4 5.90 1.00 5 13 -4 4.50 0.90 -5 13 4 3.00 1.00 -5 13 4 3.00 1.20 -4 -13 4 2.60 1.10 4 -13 -4 0.30 0.90 -4 -13 4 2.10 0.90 -4 -13 4 0.50 0.80 4 -13 -4 1.30 1.20 -4 -13 4 0.80 0.90 4 -13 -4 2.60 1.00 4 13 -4 1.60 0.90 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150.98 5.40 0 -13 4 256.57 7.40 0 -13 -4 257.87 7.80 0 -13 -4 272.27 8.00 0 -13 -4 250.47 7.60 0 -13 4 252.97 7.50 0 -13 4 258.57 7.40 0 -13 4 253.97 7.30 0 13 -4 234.58 7.80 0 13 -4 256.57 6.90 0 13 4 252.97 7.80 0 13 4 251.37 8.00 0 13 4 257.07 7.50 0 13 -4 258.17 7.00 0 13 4 212.48 8.70 0 13 -4 258.77 7.40 -1 -13 -4 91.19 3.90 -1 -13 -4 89.49 3.60 1 -13 4 94.29 3.50 1 -13 4 88.89 3.40 -1 -13 -4 86.29 3.80 1 -13 4 92.99 3.50 1 -13 4 94.59 3.40 1 13 4 94.19 3.60 1 13 4 77.89 4.10 1 13 4 92.59 3.80 1 13 4 91.09 3.90 -1 13 -4 87.49 2.90 -1 13 -4 86.99 3.40 -1 13 -4 91.19 3.00 -1 13 -4 82.79 4.80 -2 -13 -4 -0.30 0.90 2 -13 4 1.30 0.70 2 -13 4 1.30 0.80 -2 -13 -4 0.80 0.90 2 -13 4 1.20 0.90 -2 -13 -4 0.70 1.20 2 -13 4 1.00 0.90 -2 13 -4 0.40 0.60 2 13 4 0.40 1.10 -2 13 -4 1.30 1.00 2 13 4 0.90 1.10 2 13 4 0.30 0.90 2 13 4 -0.30 0.90 -2 13 -4 0.90 0.60 -2 13 -4 0.70 0.80 -3 -13 -4 7.20 1.30 3 -13 4 8.10 1.20 -3 -13 -4 6.10 1.60 3 -13 4 6.80 1.00 3 -13 4 5.80 1.10 -3 -13 -4 7.10 1.40 3 -13 4 7.20 1.10 3 13 4 7.50 1.50 -3 13 -4 7.70 1.30 3 13 4 7.10 1.20 3 13 4 5.90 1.50 3 13 4 6.70 1.20 -3 13 -4 7.40 1.10 -3 13 -4 6.80 0.90 -3 13 -4 6.70 0.90 -4 -13 -4 2.00 1.40 -4 -13 -4 -0.10 1.00 4 -13 4 0.90 0.80 4 -13 4 1.10 0.80 4 -13 4 0.50 0.90 4 -13 4 0.90 0.90 4 13 4 1.00 1.20 -4 13 -4 0.10 0.60 -4 13 -4 2.40 1.10 4 13 4 -0.40 0.90 -4 13 -4 1.70 0.70 4 13 4 0.50 0.90 -4 13 -4 0.00 0.80 4 13 4 2.00 1.20 5 -13 4 59.09 2.80 5 -13 4 63.19 3.10 -5 -13 -4 62.79 3.60 -5 -13 -4 65.89 3.20 5 -13 4 59.49 3.00 -5 13 -4 58.29 2.50 -5 13 -4 60.09 2.90 -5 13 -4 58.79 2.40 5 13 4 59.69 3.20 5 13 4 60.89 3.30 5 13 4 65.49 3.60 6 -13 4 156.38 5.20 6 -13 4 156.48 5.40 -6 -13 -4 166.48 6.10 6 -13 4 146.29 5.20 -6 -13 -4 159.58 5.60 -6 -13 -4 152.78 5.80 6 -13 4 152.18 5.40 -6 13 -4 156.58 4.80 6 13 4 155.68 6.10 -6 13 -4 155.48 5.40 6 13 4 156.98 5.90 6 13 4 151.28 5.50 -6 13 -4 152.78 4.80 -7 -13 -4 75.19 3.80 7 -13 4 77.99 3.80 -7 -13 -4 87.89 4.20 -7 -13 -4 87.29 4.40 7 -13 4 78.79 3.70 7 -13 4 77.19 3.50 7 -13 4 69.89 4.90 -7 13 -4 80.89 3.80 -7 13 -4 77.39 3.10 -7 13 -4 79.69 3.70 7 13 4 80.49 4.40 7 13 4 80.39 4.10 7 13 4 83.89 4.10 -7 13 -4 79.09 3.20 7 13 4 80.49 3.80 -8 -13 -4 0.70 1.50 8 -13 4 0.20 1.30 -8 -13 -4 2.00 1.60 8 -13 4 0.40 1.40 8 -13 4 1.50 1.20 8 -13 4 0.30 1.10 -8 -13 -4 3.00 1.90 -8 -13 -4 0.90 1.40 -8 13 -4 -0.10 1.40 -8 13 -4 -1.20 0.90 -8 13 -4 -0.30 1.00 8 13 4 1.40 1.50 8 13 4 -2.10 1.50 8 13 4 2.20 1.80 -8 13 -4 1.40 1.40 8 13 4 1.30 1.30 -9 -13 -4 -2.70 1.80 9 -13 4 1.10 1.20 9 -13 4 1.60 1.40 -9 -13 -4 1.60 1.50 9 -13 4 1.20 1.60 -9 -13 -4 0.20 1.70 -9 -13 -4 0.60 1.60 9 13 4 0.00 1.80 -9 13 -4 1.80 1.60 -9 13 -4 0.10 1.20 9 13 4 0.80 1.50 9 13 4 1.50 1.60 9 13 4 -0.10 1.60 -9 13 -4 -1.40 1.00 -9 13 -4 1.70 1.50 10 -13 4 8.00 2.00 -10 -13 -4 9.10 2.60 -10 -13 -4 3.00 1.70 10 -13 4 7.30 1.70 10 -13 4 6.40 1.60 10 -13 4 7.70 2.00 -10 -13 -4 7.40 2.00 -10 13 -4 7.60 1.40 10 13 4 5.70 1.90 -10 13 -4 9.00 2.10 -10 13 -4 10.70 2.00 10 13 4 4.90 2.30 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10 19.30 1.70 2 6 10 17.70 1.60 3 -6 10 0.40 0.50 -3 -6 -10 1.50 0.70 3 -6 10 -0.20 0.40 3 -6 10 0.50 0.40 3 -6 10 0.20 0.40 -3 -6 -10 0.70 0.80 -3 -6 -10 1.30 0.90 -3 -6 -10 0.20 0.70 3 6 10 -0.20 0.70 3 6 10 0.60 0.70 3 6 10 1.50 0.90 -3 6 -10 1.10 0.40 3 6 10 0.60 0.70 -3 6 -10 1.10 0.50 4 -6 10 93.79 3.00 -4 -6 -10 93.49 3.70 -4 -6 -10 98.09 3.30 4 -6 10 94.59 3.00 4 -6 10 91.99 3.00 4 -6 10 100.69 3.00 -4 -6 -10 97.99 4.00 4 6 10 96.29 3.50 4 6 10 91.69 3.60 4 6 10 98.99 3.70 4 6 10 96.39 3.60 -4 6 -10 96.29 3.00 -4 6 -10 85.69 2.90 5 -6 10 64.09 2.40 -5 -6 -10 62.69 2.70 5 -6 10 65.39 2.50 -5 -6 -10 65.19 2.70 -5 -6 -10 63.59 3.10 5 -6 10 62.79 2.40 -5 -6 -10 69.79 3.10 5 -6 10 64.79 2.40 -5 6 -10 56.89 2.60 5 6 10 63.49 3.10 5 6 10 66.99 3.00 5 6 10 64.59 2.80 5 6 10 65.09 3.10 -5 6 -10 64.99 2.40 -6 -6 -10 15.80 1.60 6 -6 10 15.30 1.50 6 -6 10 17.50 1.40 -6 -6 -10 15.70 2.00 6 -6 10 16.00 1.40 6 -6 10 16.80 1.50 -6 -6 -10 15.10 1.80 -6 -6 -10 9.30 1.80 -6 6 -10 15.90 1.50 -6 6 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14 28.80 3.40 -11 -5 -14 30.90 3.40 11 5 14 20.80 2.60 11 5 14 21.50 3.20 11 5 14 27.10 3.30 15 -6 -14 58.39 4.10 -15 -6 14 50.89 4.40 15 -6 -14 50.79 5.20 -15 -6 14 51.09 4.20 15 -6 -14 47.90 4.80 -15 -6 14 55.09 6.40 -15 6 14 74.39 6.50 -15 6 14 41.40 5.40 15 6 -14 61.59 4.80 -14 -6 14 22.00 2.70 -14 -6 14 26.40 2.90 -14 -6 14 22.20 2.40 -14 -6 14 30.50 3.30 14 -6 -14 32.10 4.10 14 -6 -14 27.90 3.30 14 -6 -14 32.20 3.90 14 6 -14 24.60 1.90 -14 6 14 25.40 2.90 -14 6 14 24.50 3.10 -14 6 14 24.70 2.70 14 6 -14 22.80 2.60 13 -6 -14 12.60 2.20 13 -6 -14 15.20 2.30 -13 -6 14 12.10 1.90 13 -6 -14 9.70 2.50 -13 -6 14 17.60 2.00 -13 -6 14 13.70 2.10 -13 -6 14 14.40 2.20 13 -6 -14 13.40 1.80 13 6 -14 12.30 2.10 13 6 -14 14.40 1.30 -13 6 14 11.90 2.20 13 6 -14 13.80 2.10 -13 6 14 8.70 2.20 -13 6 14 19.50 2.80 -13 6 14 15.40 2.30 -12 -6 14 0.70 1.30 -12 -6 14 1.10 1.20 12 -6 -14 0.80 1.20 -12 -6 14 0.00 1.50 12 -6 -14 1.20 1.60 -12 -6 14 1.90 1.50 12 -6 -14 0.00 1.80 -12 6 14 0.00 1.40 -12 6 14 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0.00 -5 0 23 -0.63 0.00 -3 0 23 -1.04 0.00 -1 0 23 -0.67 0.00 -7 1 23 0.25 0.00 -6 1 23 0.32 0.00 -5 1 23 0.06 0.00 -4 1 23 0.67 0.00 -3 1 23 -0.27 0.00 -2 1 23 0.88 0.00 -1 1 23 -0.23 0.00 0 1 23 0.20 0.00 -6 2 23 -0.28 0.00 -5 2 23 -0.11 0.00 -4 2 23 0.17 0.00 -3 2 23 -0.53 0.00 -2 2 23 0.46 0.00 -1 2 23 -0.43 0.00 -6 3 23 -0.17 0.00 -5 3 23 0.12 0.00 -4 3 23 -0.03 0.00 -3 3 23 -0.32 0.00 -2 3 23 0.43 0.00 -1 3 23 -0.38 0.00 -5 4 23 0.21 0.00 -4 4 23 -0.03 0.00 -3 4 23 -0.22 0.00 -2 4 23 0.33 0.00 1 1 0 -66.15 0.00 0 2 0 54.15 0.00 17 4 0 0.01 0.00 15 11 0 0.32 0.00 -1 0 1 -74.51 0.00 1 0 1 -60.90 0.00 -1 1 1 2.16 0.00 0 1 1 67.22 0.00 1 1 1 -0.05 0.00 0 2 1 -1.41 0.00 17 3 1 -0.14 0.00 -17 5 1 -0.13 0.00 16 8 1 -0.06 0.00 -16 9 1 0.09 0.00 -14 13 1 -0.60 0.00 -11 17 1 0.17 0.00 -7 20 1 -0.57 0.00 0 0 2 58.91 0.00 -1 1 2 -60.16 0.00 0 1 2 -1.91 0.00 17 1 2 -0.22 0.00 16 7 2 0.21 0.00 -16 9 2 0.37 0.00 15 10 2 -0.28 0.00 -12 16 2 -0.01 0.00 -11 17 2 -0.01 0.00 -10 18 2 0.25 0.00 8 19 2 -0.24 0.00 -7 20 2 -0.83 0.00 4 21 2 -0.54 0.00 -17 6 3 -0.08 0.00 -12 16 3 -0.35 0.00 11 16 3 0.67 0.00 -11 17 3 0.22 0.00 -10 18 3 0.21 0.00 9 18 3 0.12 0.00 -7 20 3 -0.29 0.00 6 20 3 -0.39 0.00 16 5 4 0.26 0.00 -17 6 4 -0.27 0.00 14 11 4 0.69 0.00 13 13 4 0.46 0.00 -12 16 4 0.39 0.00 -11 17 4 -0.47 0.00 -10 18 4 0.51 0.00 -4 21 4 -0.01 0.00 3 21 4 -0.23 0.00 16 3 5 0.27 0.00 -17 6 5 0.07 0.00 15 8 5 0.25 0.00 12 14 5 0.18 0.00 -12 16 5 -0.24 0.00 -11 17 5 0.17 0.00 5 20 5 -0.23 0.00 -3 21 5 0.32 0.00 2 21 5 -0.09 0.00 -17 6 6 -0.25 0.00 10 16 6 -1.14 0.00 9 17 6 0.80 0.00 -8 19 6 0.42 0.00 -6 20 6 -0.07 0.00 -2 21 6 -0.60 0.00 -1 21 6 0.49 0.00 0 21 6 -0.64 0.00 15 5 7 -0.40 0.00 -17 6 7 0.00 0.00 -16 9 7 0.29 0.00 13 11 7 -0.66 0.00 -14 13 7 0.12 0.00 15 2 8 -0.11 0.00 -17 5 8 -0.07 0.00 13 10 8 -0.71 0.00 -15 11 8 -0.22 0.00 12 12 8 -0.44 0.00 9 16 8 -0.68 0.00 -9 18 8 -0.31 0.00 5 19 8 0.34 0.00 2 20 8 -0.45 0.00 14 6 9 0.28 0.00 13 9 9 -0.52 0.00 12 11 9 -0.05 0.00 -12 15 9 0.10 0.00 -11 16 9 -0.14 0.00 -10 17 9 0.37 0.00 4 19 9 -0.45 0.00 -3 20 9 0.43 0.00 0 20 9 -0.14 0.00 -17 3 10 -0.15 0.00 14 3 10 0.23 0.00 -15 10 10 0.73 0.00 12 10 10 0.38 0.00 -14 12 10 0.12 0.00 11 12 10 -0.56 0.00 -8 18 10 0.17 0.00 5 18 10 -0.14 0.00 -17 0 11 -0.49 0.00 -17 1 11 -0.08 0.00 -17 2 11 -0.33 0.00 -16 7 11 -1.25 0.00 11 11 11 -0.94 0.00 -13 13 11 -0.07 0.00 8 15 11 -0.94 0.00 -9 17 11 -0.30 0.00 -7 18 11 0.03 0.00 -4 19 11 0.21 0.00 1 19 11 0.32 0.00 13 2 12 -0.08 0.00 -16 6 12 -1.25 0.00 12 7 12 0.45 0.00 -15 9 12 0.58 0.00 -14 11 12 -0.68 0.00 9 13 12 -0.10 0.00 8 14 12 -0.27 0.00 6 16 12 -0.93 0.00 -8 17 12 -0.09 0.00 -6 18 12 0.07 0.00 12 5 13 -0.74 0.00 -15 8 13 0.68 0.00 11 8 13 -0.58 0.00 -14 10 13 -0.96 0.00 -12 13 13 -0.68 0.00 -9 16 13 0.45 0.00 5 16 13 0.74 0.00 -7 17 13 0.27 0.00 3 17 13 -0.59 0.00 -4 18 13 0.06 0.00 0 18 13 0.11 0.00 -16 2 14 -0.06 0.00 11 6 14 -0.61 0.00 -15 7 14 0.66 0.00 -13 11 14 0.44 0.00 8 12 14 0.46 0.00 5 15 14 0.10 0.00 -8 16 14 -0.07 0.00 1 17 14 0.80 0.00 11 2 15 1.97 0.00 -14 8 15 -0.61 0.00 9 9 15 -1.32 0.00 -13 10 15 0.60 0.00 7 12 15 -0.44 0.00 5 14 15 -0.34 0.00 2 16 15 0.36 0.00 -15 3 16 0.20 0.00 10 4 16 -1.47 0.00 -14 7 16 -0.21 0.00 9 7 16 0.04 0.00 -13 9 16 0.69 0.00 -11 12 16 -0.37 0.00 6 12 16 0.51 0.00 -10 13 16 0.30 0.00 5 13 16 -0.48 0.00 -7 15 16 -0.33 0.00 2 15 16 0.15 0.00 -4 16 16 0.13 0.00 -3 16 16 -0.26 0.00 -2 16 16 -0.22 0.00 -1 16 16 -0.11 0.00 9 4 17 1.58 0.00 -14 5 17 0.19 0.00 8 7 17 -0.18 0.00 7 9 17 -1.72 0.00 -11 11 17 -0.18 0.00 -10 12 17 0.20 0.00 -7 14 17 -0.22 0.00 2 14 17 0.03 0.00 -4 15 17 0.22 0.00 -3 15 17 -0.42 0.00 -2 15 17 -0.03 0.00 -1 15 17 -0.17 0.00 -14 0 18 1.25 0.00 -14 1 18 -0.18 0.00 8 4 18 -1.61 0.00 -13 6 18 -0.71 0.00 7 7 18 0.29 0.00 -12 8 18 -0.44 0.00 6 9 18 1.62 0.00 3 12 18 -0.26 0.00 -7 13 18 0.03 0.00 -4 14 18 0.21 0.00 -3 14 18 -0.44 0.00 -2 14 18 0.05 0.00 -1 14 18 -0.26 0.00 -13 3 19 -0.10 0.00 7 4 19 1.52 0.00 -12 6 19 0.84 0.00 -11 8 19 0.26 0.00 -7 12 19 0.18 0.00 1 12 19 -0.24 0.00 -4 13 19 0.05 0.00 -3 13 19 -0.16 0.00 -2 13 19 -0.03 0.00 6 2 20 -1.52 0.00 -12 3 20 0.05 0.00 6 3 20 0.50 0.00 -11 6 20 -0.39 0.00 5 6 20 -0.86 0.00 -9 9 20 -0.26 0.00 -6 11 20 -0.38 0.00 0 11 20 0.63 0.00 -11 2 21 0.00 0.00 4 4 21 0.24 0.00 -10 5 21 -0.36 0.00 3 6 21 0.42 0.00 -9 7 21 0.51 0.00 -8 8 21 -0.55 0.00 0 9 21 -0.30 0.00 -4 10 21 -0.92 0.00 -3 10 21 -0.11 0.00 -2 10 21 -0.19 0.00 3 1 22 0.40 0.00 -9 4 22 -0.01 0.00 2 4 22 -0.23 0.00 1 6 22 -0.84 0.00 0 7 22 1.04 0.00 -4 8 22 0.37 0.00 -3 8 22 0.22 0.00 -2 8 22 0.47 0.00 -7 2 23 0.04 0.00 0 2 23 0.17 0.00 -7 3 23 0.25 0.00 0 3 23 0.13 0.00 -6 4 23 -0.23 0.00 -1 4 23 -0.36 0.00 -5 5 23 0.23 0.00 -4 5 23 0.10 0.00 -3 5 23 -0.06 0.00 -2 5 23 0.49 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 230318) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.500 0.500 115 39 ' ' 2 0.500 0.000 1.000 115 39 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 1 0 2.039 0 2 0 2.544 -1 0 1 1.786 1 0 1 2.178 -1 1 1 2.193 0 1 1 1.745 1 1 1 2.522 0 2 1 2.810 0 0 2 2.389 -1 1 2 2.884 0 1 2 2.707 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL mo_molan50P 21/n R = 0.10 CELL 13.0505 16.0146 17.4162 90.00 101.76 90.00 SPGR P21/n # Solvent Accessible Volume = 230 # Electrons Found in S.A.V. = 77 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.938 0.461 0.453 ! 8.54 eA-3 C102 0.954 0.552 0.420 ! 6.19 eA-3 C103 0.987 0.561 0.489 ! 5.30 eA-3 Q104 0.264 0.123 0.085 ! 1.35 eA-3 Q105 0.625 0.493 0.518 ! 1.11 eA-3 Q106 0.841 0.897 0.969 ! 1.11 eA-3 Q107 0.327 0.980 0.136 ! 1.06 eA-3 Q108 0.737 0.546 0.595 ! 1.01 eA-3 Q109 0.717 0.483 0.511 ! 0.96 eA-3 Q110 0.158 0.546 0.390 ! 0.94 eA-3 Q111 0.779 0.552 0.541 ! 0.92 eA-3 Q112 0.317 0.060 0.139 ! 0.87 eA-3 Q113 0.877 0.460 0.408 ! 0.80 eA-3 Q114 0.924 0.446 0.396 ! 0.78 eA-3 Q115 0.299 0.968 0.092 ! 0.76 eA-3 Q116 0.171 0.969 0.060 ! 0.76 eA-3 Q117 0.593 0.762 0.137 ! 0.72 eA-3 Q118 0.472 0.484 0.296 ! 0.71 eA-3 C119 0.892 0.506 0.406 ! 0.70 eA-3 Q120 0.856 0.788 0.030 ! 0.69 eA-3 Q121 0.269 0.750 0.237 ! 0.68 eA-3 Q122 0.800 0.784 0.390 ! 0.67 eA-3 Q123 0.216 0.100 0.138 ! 0.64 eA-3 Q124 0.768 0.140 0.543 ! 0.64 eA-3 Q125 0.342 0.756 0.562 ! 0.60 eA-3 Q126 0.676 0.664 0.390 ! 0.59 eA-3 Q127 0.803 0.780 0.060 ! 0.58 eA-3 Q128 0.670 0.379 0.347 ! 0.57 eA-3 Q129 0.907 0.907 0.174 ! 0.55 eA-3 Q130 0.332 0.506 0.080 ! 0.54 eA-3 Q131 0.487 0.778 0.250 ! 0.53 eA-3 Q132 0.987 0.716 0.750 ! 0.53 eA-3 Q133 0.483 0.208 0.776 ! 0.52 eA-3 Q134 0.688 0.835 0.141 ! 0.52 eA-3 Q135 0.564 0.145 0.340 ! 0.52 eA-3 Q136 0.967 0.283 0.956 ! 0.51 eA-3 Q137 0.437 0.986 0.720 ! 0.51 eA-3 Q138 0.515 0.205 0.458 ! 0.51 eA-3 Q139 0.889 0.173 0.444 ! 0.51 eA-3 Q140 0.672 0.479 0.284 ! 0.51 eA-3 ) ; _shelx_fab_checksum 71998 #===END data_cu_molan529_0m_a _audit_creation_method 'SHELXL-2018/1' _shelx_SHELXL_version_number '2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C38 H30 Fe N8' _chemical_formula_weight 654.55 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 15.1516(5) _cell_length_b 12.1817(4) _cell_length_c 16.9830(6) _cell_angle_alpha 90 _cell_angle_beta 92.7330(10) _cell_angle_gamma 90 _cell_volume 3131.03(18) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9855 _cell_measurement_theta_min 2.92 _cell_measurement_theta_max 70.17 _exptl_crystal_description 'plate' _exptl_crystal_colour 'red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.389 _exptl_crystal_F_000 1360 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.02 _exptl_absorpt_coefficient_mu 4.193 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.4301 _exptl_absorpt_correction_T_max 0.7533 _exptl_absorpt_process_details 'SADABS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 25816 _diffrn_reflns_av_unetI/netI 0.0352 _diffrn_reflns_av_R_equivalents 0.0421 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 2.920 _diffrn_reflns_theta_max 70.221 _diffrn_reflns_theta_full 67.679 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 5886 _reflns_number_gt 5463 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0331P)^2^+2.4692P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 5886 _refine_ls_number_parameters 424 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0378 _refine_ls_R_factor_gt 0.0343 _refine_ls_wR_factor_ref 0.0874 _refine_ls_wR_factor_gt 0.0849 _refine_ls_goodness_of_fit_ref 1.044 _refine_ls_restrained_S_all 1.044 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.23192(2) 0.63224(2) 0.61932(2) 0.01527(9) Uani 1 1 d . . . . . C1 C 0.34123(12) 0.62136(14) 0.48188(10) 0.0171(4) Uani 1 1 d . . . . . N1 N 0.29548(10) 0.55736(12) 0.53757(8) 0.0159(3) Uani 1 1 d . . . . . N3 N 0.25243(10) 0.39717(12) 0.65915(9) 0.0171(3) Uani 1 1 d . . . . . C3 C 0.35683(13) 0.79466(15) 0.41546(11) 0.0222(4) Uani 1 1 d . . . . . H3 H 0.335930 0.866701 0.403990 0.027 Uiso 1 1 calc R U . . . N2 N 0.31380(10) 0.45209(12) 0.53378(8) 0.0171(3) Uani 1 1 d . . . . . C2 C 0.31101(13) 0.72760(15) 0.46552(10) 0.0204(4) Uani 1 1 d . . . . . H2 H 0.259195 0.753961 0.488600 0.024 Uiso 1 1 calc R U . . . N4 N 0.22451(10) 0.49431(12) 0.68009(8) 0.0159(3) Uani 1 1 d . . . . . C4 C 0.43259(13) 0.75717(16) 0.38227(10) 0.0223(4) Uani 1 1 d . . . . . H4 H 0.464883 0.803926 0.349350 0.027 Uiso 1 1 calc R U . . . N5 N 0.13477(10) 0.73971(12) 0.60208(8) 0.0161(3) Uani 1 1 d . . . . . C5 C 0.46137(13) 0.65028(16) 0.39741(11) 0.0227(4) Uani 1 1 d . . . . . H5 H 0.512608 0.623789 0.373458 0.027 Uiso 1 1 calc R U . . . N7 N 0.27238(10) 0.83288(12) 0.70965(8) 0.0162(3) Uani 1 1 d . . . . . C7 C 0.28832(12) 0.38077(14) 0.58877(10) 0.0162(4) Uani 1 1 d . . . . . N6 N 0.12382(10) 0.82752(12) 0.64558(8) 0.0167(3) Uani 1 1 d . . . . . C6 C 0.41639(12) 0.58232(15) 0.44679(10) 0.0199(4) Uani 1 1 d . . . . . H6 H 0.436514 0.509547 0.456752 0.024 Uiso 1 1 calc R U . . . N8 N 0.30338(10) 0.74438(12) 0.67775(8) 0.0159(3) Uani 1 1 d . . . . . C8 C 0.31195(12) 0.26417(15) 0.57260(10) 0.0172(4) Uani 1 1 d . . . . . C9 C 0.36552(13) 0.23726(15) 0.51029(11) 0.0206(4) Uani 1 1 d . . . . . H9 H 0.383780 0.293294 0.475725 0.025 Uiso 1 1 calc R U . . . C20 C 0.06891(12) 0.72884(15) 0.53923(10) 0.0165(4) Uani 1 1 d . . . . . C21 C 0.00431(12) 0.80811(16) 0.52230(10) 0.0193(4) Uani 1 1 d . . . . . H21 H 0.001223 0.871960 0.554163 0.023 Uiso 1 1 calc R U . . . C22 C -0.05536(12) 0.79325(17) 0.45875(11) 0.0228(4) Uani 1 1 d . . . . . H22 H -0.099645 0.846978 0.447561 0.027 Uiso 1 1 calc R U . . . C23 C -0.05119(13) 0.70062(17) 0.41118(11) 0.0243(4) Uani 1 1 d . . . . . H23 H -0.091942 0.691521 0.367403 0.029 Uiso 1 1 calc R U . . . C24 C 0.01276(14) 0.62178(16) 0.42805(12) 0.0250(4) Uani 1 1 d . . . . . H24 H 0.015623 0.558118 0.395954 0.030 Uiso 1 1 calc R U . . . C25 C 0.07274(13) 0.63541(15) 0.49172(11) 0.0219(4) Uani 1 1 d . . . . . H25 H 0.116506 0.581079 0.503013 0.026 Uiso 1 1 calc R U . . . C26 C 0.18585(12) 0.86170(14) 0.69912(10) 0.0160(4) Uani 1 1 d . . . . . C27 C 0.16139(12) 0.95802(15) 0.74743(10) 0.0169(4) Uani 1 1 d . . . . . C28 C 0.08659(13) 1.02142(16) 0.72788(11) 0.0231(4) Uani 1 1 d . . . . . H28 H 0.048790 1.001467 0.683977 0.028 Uiso 1 1 calc R U . . . C29 C 0.06729(14) 1.11288(17) 0.77199(12) 0.0273(4) Uani 1 1 d . . . . . H29 H 0.016770 1.155906 0.757611 0.033 Uiso 1 1 calc R U . . . C30 C 0.12095(14) 1.14264(16) 0.83714(12) 0.0255(4) Uani 1 1 d . . . . . H30 H 0.107233 1.205429 0.867401 0.031 Uiso 1 1 calc R U . . . C31 C 0.19460(13) 1.07971(16) 0.85743(11) 0.0232(4) Uani 1 1 d . . . . . H31 H 0.231546 1.099322 0.901972 0.028 Uiso 1 1 calc R U . . . C32 C 0.21485(13) 0.98815(16) 0.81314(10) 0.0211(4) Uani 1 1 d . . . . . H32 H 0.265573 0.945562 0.827674 0.025 Uiso 1 1 calc R U . . . C33 C 0.39790(12) 0.73733(15) 0.68535(10) 0.0167(4) Uani 1 1 d . . . . . C34 C 0.43660(13) 0.63332(15) 0.68544(10) 0.0196(4) Uani 1 1 d . . . . . H34 H 0.400695 0.569693 0.679164 0.024 Uiso 1 1 calc R U . . . C35 C 0.52775(13) 0.62326(16) 0.69474(11) 0.0230(4) Uani 1 1 d . . . . . H35 H 0.554148 0.552507 0.695821 0.028 Uiso 1 1 calc R U . . . C36 C 0.58039(13) 0.71601(17) 0.70245(11) 0.0246(4) Uani 1 1 d . . . . . H36 H 0.642782 0.708892 0.708554 0.030 Uiso 1 1 calc R U . . . C37 C 0.54168(13) 0.81950(17) 0.70122(11) 0.0232(4) Uani 1 1 d . . . . . H37 H 0.577891 0.883025 0.706217 0.028 Uiso 1 1 calc R U . . . C38 C 0.45037(12) 0.83081(15) 0.69273(10) 0.0194(4) Uani 1 1 d . . . . . H38 H 0.424113 0.901639 0.691989 0.023 Uiso 1 1 calc R U . . . C18 C 0.13884(13) 0.60730(16) 0.86359(11) 0.0217(4) Uani 1 1 d . . . . . H18 H 0.112120 0.673349 0.880292 0.026 Uiso 1 1 calc R U . . . C10 C 0.39215(14) 0.12970(16) 0.49854(11) 0.0241(4) Uani 1 1 d . . . . . H10 H 0.428800 0.112810 0.456333 0.029 Uiso 1 1 calc R U . . . C11 C 0.36567(14) 0.04712(16) 0.54786(11) 0.0248(4) Uani 1 1 d . . . . . H11 H 0.384799 -0.026252 0.540405 0.030 Uiso 1 1 calc R U . . . C13 C 0.28441(13) 0.17950(15) 0.62069(11) 0.0213(4) Uani 1 1 d . . . . . H13 H 0.246971 0.195362 0.662529 0.026 Uiso 1 1 calc R U . . . C14 C 0.20008(11) 0.49898(15) 0.76048(10) 0.0166(4) Uani 1 1 d . . . . . C15 C 0.21638(13) 0.41366(15) 0.81423(11) 0.0212(4) Uani 1 1 d . . . . . H15 H 0.242585 0.347244 0.797625 0.025 Uiso 1 1 calc R U . . . C16 C 0.19409(13) 0.42649(16) 0.89190(11) 0.0235(4) Uani 1 1 d . . . . . H16 H 0.205366 0.368553 0.928449 0.028 Uiso 1 1 calc R U . . . C17 C 0.15553(12) 0.52283(16) 0.91693(11) 0.0213(4) Uani 1 1 d . . . . . H17 H 0.140638 0.530890 0.970327 0.026 Uiso 1 1 calc R U . . . C12 C 0.31100(14) 0.07237(16) 0.60821(11) 0.0246(4) Uani 1 1 d . . . . . H12 H 0.291455 0.015561 0.641514 0.029 Uiso 1 1 calc R U . . . C19 C 0.16119(12) 0.59527(15) 0.78583(11) 0.0191(4) Uani 1 1 d . . . . . H19 H 0.149801 0.653440 0.749494 0.023 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.02032(15) 0.00992(15) 0.01559(14) -0.00057(10) 0.00123(11) 0.00310(11) C1 0.0235(9) 0.0145(9) 0.0131(8) -0.0016(6) -0.0012(7) -0.0002(7) N1 0.0206(8) 0.0113(7) 0.0158(7) -0.0013(6) 0.0010(6) 0.0024(6) N3 0.0194(7) 0.0122(7) 0.0197(7) -0.0019(6) 0.0002(6) 0.0006(6) C3 0.0318(10) 0.0148(9) 0.0200(9) 0.0014(7) 0.0013(8) 0.0020(8) N2 0.0214(8) 0.0122(7) 0.0175(7) -0.0011(6) -0.0013(6) 0.0018(6) C2 0.0256(10) 0.0164(9) 0.0194(9) -0.0005(7) 0.0040(7) 0.0031(8) N4 0.0177(7) 0.0124(7) 0.0179(7) -0.0016(6) 0.0017(6) 0.0010(6) C4 0.0286(10) 0.0220(10) 0.0163(8) 0.0020(7) 0.0011(7) -0.0042(8) N5 0.0201(8) 0.0125(7) 0.0158(7) -0.0004(6) 0.0006(6) 0.0005(6) C5 0.0243(10) 0.0243(10) 0.0194(9) 0.0000(7) 0.0017(8) 0.0024(8) N7 0.0209(8) 0.0125(7) 0.0152(7) 0.0008(6) 0.0019(6) 0.0028(6) C7 0.0173(8) 0.0135(9) 0.0175(8) -0.0006(7) -0.0005(7) 0.0002(7) N6 0.0213(8) 0.0142(7) 0.0148(7) 0.0007(6) 0.0019(6) 0.0022(6) C6 0.0237(9) 0.0166(9) 0.0192(9) 0.0004(7) -0.0014(7) 0.0022(8) N8 0.0191(7) 0.0128(7) 0.0158(7) 0.0012(6) 0.0012(6) 0.0022(6) C8 0.0195(9) 0.0143(9) 0.0174(8) -0.0014(7) -0.0024(7) 0.0016(7) C9 0.0285(10) 0.0154(9) 0.0182(8) 0.0001(7) 0.0027(7) -0.0009(8) C20 0.0176(9) 0.0171(9) 0.0150(8) 0.0019(7) 0.0025(7) -0.0027(7) C21 0.0218(9) 0.0188(9) 0.0176(8) 0.0007(7) 0.0042(7) -0.0001(8) C22 0.0188(9) 0.0277(10) 0.0218(9) 0.0035(8) 0.0012(7) 0.0023(8) C23 0.0222(9) 0.0285(11) 0.0219(9) 0.0007(8) -0.0025(8) -0.0068(8) C24 0.0292(10) 0.0200(10) 0.0255(10) -0.0047(8) -0.0012(8) -0.0051(8) C25 0.0240(10) 0.0167(9) 0.0250(9) -0.0017(7) 0.0002(8) 0.0014(8) C26 0.0195(9) 0.0122(8) 0.0162(8) 0.0016(6) 0.0013(7) 0.0013(7) C27 0.0204(9) 0.0143(9) 0.0163(8) 0.0007(7) 0.0031(7) 0.0002(7) C28 0.0247(10) 0.0212(10) 0.0231(9) -0.0043(7) -0.0028(8) 0.0040(8) C29 0.0261(10) 0.0226(10) 0.0330(11) -0.0054(8) -0.0008(9) 0.0077(9) C30 0.0317(11) 0.0189(10) 0.0265(10) -0.0073(8) 0.0066(8) -0.0007(8) C31 0.0275(10) 0.0236(10) 0.0187(9) -0.0042(7) 0.0020(8) -0.0019(8) C32 0.0246(10) 0.0193(9) 0.0193(9) 0.0001(7) -0.0003(7) 0.0029(8) C33 0.0190(9) 0.0191(9) 0.0121(8) 0.0002(7) 0.0016(7) 0.0030(7) C34 0.0232(10) 0.0172(9) 0.0184(9) -0.0026(7) 0.0009(7) 0.0033(8) C35 0.0266(10) 0.0210(10) 0.0212(9) -0.0029(7) 0.0002(8) 0.0091(8) C36 0.0195(9) 0.0321(11) 0.0224(9) -0.0009(8) 0.0037(7) 0.0029(8) C37 0.0232(10) 0.0249(10) 0.0218(9) 0.0003(8) 0.0051(8) -0.0029(8) C38 0.0237(9) 0.0169(9) 0.0179(8) 0.0017(7) 0.0050(7) 0.0021(8) C18 0.0251(10) 0.0174(9) 0.0231(9) -0.0026(7) 0.0055(8) 0.0003(8) C10 0.0334(11) 0.0199(10) 0.0192(9) -0.0049(7) 0.0025(8) 0.0044(8) C11 0.0351(11) 0.0126(9) 0.0262(10) -0.0039(7) -0.0029(8) 0.0065(8) C13 0.0255(10) 0.0169(9) 0.0215(9) -0.0006(7) 0.0022(7) 0.0010(8) C14 0.0162(8) 0.0158(9) 0.0180(8) -0.0003(7) 0.0013(7) -0.0028(7) C15 0.0246(10) 0.0143(9) 0.0249(9) 0.0006(7) 0.0032(8) 0.0030(8) C16 0.0277(10) 0.0208(10) 0.0223(9) 0.0056(7) 0.0028(8) 0.0009(8) C17 0.0230(9) 0.0235(10) 0.0178(8) -0.0005(7) 0.0055(7) -0.0021(8) C12 0.0324(11) 0.0141(9) 0.0274(10) 0.0025(7) 0.0036(8) 0.0014(8) C19 0.0218(9) 0.0148(9) 0.0210(9) 0.0022(7) 0.0034(7) 0.0014(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.9532(15) . ? Fe1 N4 1.9780(15) . ? Fe1 N8 1.9801(15) . ? Fe1 N5 1.9812(15) . ? C1 C6 1.394(3) . ? C1 C2 1.396(3) . ? C1 N1 1.430(2) . ? N1 N2 1.314(2) . ? N3 N4 1.311(2) . ? N3 C7 1.351(2) . ? C3 C4 1.380(3) . ? C3 C2 1.389(3) . ? C3 H3 0.9500 . ? N2 C7 1.346(2) . ? C2 H2 0.9500 . ? N4 C14 1.433(2) . ? C4 C5 1.393(3) . ? C4 H4 0.9500 . ? N5 N6 1.315(2) . ? N5 C20 1.432(2) . ? C5 C6 1.381(3) . ? C5 H5 0.9500 . ? N7 N8 1.304(2) . ? N7 C26 1.361(2) . ? C7 C8 1.493(2) . ? N6 C26 1.342(2) . ? C6 H6 0.9500 . ? N8 C33 1.434(2) . ? C8 C13 1.392(3) . ? C8 C9 1.403(3) . ? C9 C10 1.388(3) . ? C9 H9 0.9500 . ? C20 C21 1.395(3) . ? C20 C25 1.398(3) . ? C21 C22 1.386(3) . ? C21 H21 0.9500 . ? C22 C23 1.391(3) . ? C22 H22 0.9500 . ? C23 C24 1.385(3) . ? C23 H23 0.9500 . ? C24 C25 1.389(3) . ? C24 H24 0.9500 . ? C25 H25 0.9500 . ? C26 C27 1.489(2) . ? C27 C32 1.397(2) . ? C27 C28 1.398(3) . ? C28 C29 1.382(3) . ? C28 H28 0.9500 . ? C29 C30 1.390(3) . ? C29 H29 0.9500 . ? C30 C31 1.384(3) . ? C30 H30 0.9500 . ? C31 C32 1.388(3) . ? C31 H31 0.9500 . ? C32 H32 0.9500 . ? C33 C38 1.391(3) . ? C33 C34 1.396(3) . ? C34 C35 1.388(3) . ? C34 H34 0.9500 . ? C35 C36 1.386(3) . ? C35 H35 0.9500 . ? C36 C37 1.390(3) . ? C36 H36 0.9500 . ? C37 C38 1.391(3) . ? C37 H37 0.9500 . ? C38 H38 0.9500 . ? C18 C17 1.386(3) . ? C18 C19 1.387(3) . ? C18 H18 0.9500 . ? C10 C11 1.381(3) . ? C10 H10 0.9500 . ? C11 C12 1.383(3) . ? C11 H11 0.9500 . ? C13 C12 1.385(3) . ? C13 H13 0.9500 . ? C14 C19 1.390(3) . ? C14 C15 1.397(2) . ? C15 C16 1.386(3) . ? C15 H15 0.9500 . ? C16 C17 1.387(3) . ? C16 H16 0.9500 . ? C17 H17 0.9500 . ? C12 H12 0.9500 . ? C19 H19 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N4 90.93(6) . . ? N1 Fe1 N8 113.71(6) . . ? N4 Fe1 N8 111.58(6) . . ? N1 Fe1 N5 126.27(6) . . ? N4 Fe1 N5 125.33(6) . . ? N8 Fe1 N5 90.17(6) . . ? C6 C1 C2 119.87(17) . . ? C6 C1 N1 121.89(16) . . ? C2 C1 N1 118.17(17) . . ? N2 N1 C1 112.91(14) . . ? N2 N1 Fe1 127.08(12) . . ? C1 N1 Fe1 119.11(11) . . ? N4 N3 C7 121.46(15) . . ? C4 C3 C2 120.34(18) . . ? C4 C3 H3 119.8 . . ? C2 C3 H3 119.8 . . ? N1 N2 C7 121.85(15) . . ? C3 C2 C1 119.89(18) . . ? C3 C2 H2 120.1 . . ? C1 C2 H2 120.1 . . ? N3 N4 C14 113.31(14) . . ? N3 N4 Fe1 126.72(12) . . ? C14 N4 Fe1 119.16(11) . . ? C3 C4 C5 119.53(18) . . ? C3 C4 H4 120.2 . . ? C5 C4 H4 120.2 . . ? N6 N5 C20 113.07(14) . . ? N6 N5 Fe1 124.55(11) . . ? C20 N5 Fe1 122.37(11) . . ? C6 C5 C4 120.87(19) . . ? C6 C5 H5 119.6 . . ? C4 C5 H5 119.6 . . ? N8 N7 C26 121.50(15) . . ? N2 C7 N3 131.25(16) . . ? N2 C7 C8 114.03(15) . . ? N3 C7 C8 114.42(15) . . ? N5 N6 C26 121.99(15) . . ? C5 C6 C1 119.47(17) . . ? C5 C6 H6 120.3 . . ? C1 C6 H6 120.3 . . ? N7 N8 C33 112.95(14) . . ? N7 N8 Fe1 125.41(12) . . ? C33 N8 Fe1 121.57(11) . . ? C13 C8 C9 118.02(17) . . ? C13 C8 C7 121.04(17) . . ? C9 C8 C7 120.89(16) . . ? C10 C9 C8 120.77(18) . . ? C10 C9 H9 119.6 . . ? C8 C9 H9 119.6 . . ? C21 C20 C25 119.51(16) . . ? C21 C20 N5 123.14(16) . . ? C25 C20 N5 117.31(16) . . ? C22 C21 C20 119.68(17) . . ? C22 C21 H21 120.2 . . ? C20 C21 H21 120.2 . . ? C21 C22 C23 120.80(18) . . ? C21 C22 H22 119.6 . . ? C23 C22 H22 119.6 . . ? C24 C23 C22 119.56(17) . . ? C24 C23 H23 120.2 . . ? C22 C23 H23 120.2 . . ? C23 C24 C25 120.24(18) . . ? C23 C24 H24 119.9 . . ? C25 C24 H24 119.9 . . ? C24 C25 C20 120.21(18) . . ? C24 C25 H25 119.9 . . ? C20 C25 H25 119.9 . . ? N6 C26 N7 130.40(16) . . ? N6 C26 C27 115.66(15) . . ? N7 C26 C27 113.24(15) . . ? C32 C27 C28 118.50(17) . . ? C32 C27 C26 119.83(16) . . ? C28 C27 C26 121.65(16) . . ? C29 C28 C27 120.45(17) . . ? C29 C28 H28 119.8 . . ? C27 C28 H28 119.8 . . ? C28 C29 C30 120.74(18) . . ? C28 C29 H29 119.6 . . ? C30 C29 H29 119.6 . . ? C31 C30 C29 119.20(18) . . ? C31 C30 H30 120.4 . . ? C29 C30 H30 120.4 . . ? C30 C31 C32 120.46(17) . . ? C30 C31 H31 119.8 . . ? C32 C31 H31 119.8 . . ? C31 C32 C27 120.63(17) . . ? C31 C32 H32 119.7 . . ? C27 C32 H32 119.7 . . ? C38 C33 C34 120.30(17) . . ? C38 C33 N8 121.53(16) . . ? C34 C33 N8 118.16(16) . . ? C35 C34 C33 119.73(17) . . ? C35 C34 H34 120.1 . . ? C33 C34 H34 120.1 . . ? C36 C35 C34 120.26(17) . . ? C36 C35 H35 119.9 . . ? C34 C35 H35 119.9 . . ? C35 C36 C37 119.83(18) . . ? C35 C36 H36 120.1 . . ? C37 C36 H36 120.1 . . ? C36 C37 C38 120.54(18) . . ? C36 C37 H37 119.7 . . ? C38 C37 H37 119.7 . . ? C37 C38 C33 119.32(17) . . ? C37 C38 H38 120.3 . . ? C33 C38 H38 120.3 . . ? C17 C18 C19 119.91(18) . . ? C17 C18 H18 120.0 . . ? C19 C18 H18 120.0 . . ? C11 C10 C9 120.37(19) . . ? C11 C10 H10 119.8 . . ? C9 C10 H10 119.8 . . ? C10 C11 C12 119.29(18) . . ? C10 C11 H11 120.4 . . ? C12 C11 H11 120.4 . . ? C12 C13 C8 120.72(18) . . ? C12 C13 H13 119.6 . . ? C8 C13 H13 119.6 . . ? C19 C14 C15 119.31(16) . . ? C19 C14 N4 117.46(16) . . ? C15 C14 N4 123.18(16) . . ? C16 C15 C14 119.63(17) . . ? C16 C15 H15 120.2 . . ? C14 C15 H15 120.2 . . ? C15 C16 C17 120.83(17) . . ? C15 C16 H16 119.6 . . ? C17 C16 H16 119.6 . . ? C18 C17 C16 119.63(17) . . ? C18 C17 H17 120.2 . . ? C16 C17 H17 120.2 . . ? C11 C12 C13 120.79(18) . . ? C11 C12 H12 119.6 . . ? C13 C12 H12 119.6 . . ? C18 C19 C14 120.69(17) . . ? C18 C19 H19 119.7 . . ? C14 C19 H19 119.7 . . ? _refine_diff_density_max 0.315 _refine_diff_density_min -0.426 _refine_diff_density_rms 0.050 _shelx_res_file ; TITL cu_molan529_0m_a.res in P2(1)/c cu_molan529_0m_a.res created by SHELXL-2018/1 at 14:37:32 on 02-Oct-2018 REM Old TITL cu_molan529_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.101, Rweak 0.008, Alpha 0.022, Orientation as input REM Formula found by SHELXT: C38 N8 Fe CELL 1.54178 15.1516 12.1817 16.9830 90.000 92.733 90.000 ZERR 4.000 0.0005 0.0004 0.0006 0.000 0.001 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N FE UNIT 152 120 32 4 TEMP -173.150 L.S. 10 acta BOND $H LIST 4 FMAP 2 PLAN 20 WGHT 0.033100 2.469200 FVAR 0.39642 FE1 4 0.231916 0.632245 0.619319 11.00000 0.02032 0.00992 = 0.01559 -0.00057 0.00123 0.00310 C1 1 0.341231 0.621358 0.481877 11.00000 0.02348 0.01454 = 0.01312 -0.00157 -0.00116 -0.00021 N1 3 0.295483 0.557359 0.537565 11.00000 0.02064 0.01130 = 0.01580 -0.00132 0.00101 0.00238 N3 3 0.252430 0.397170 0.659145 11.00000 0.01939 0.01222 = 0.01973 -0.00193 0.00017 0.00057 C3 1 0.356831 0.794659 0.415459 11.00000 0.03178 0.01478 = 0.01996 0.00143 0.00126 0.00197 AFIX 43 H3 2 0.335930 0.866701 0.403990 11.00000 -1.20000 AFIX 0 N2 3 0.313804 0.452092 0.533777 11.00000 0.02145 0.01224 = 0.01752 -0.00110 -0.00126 0.00185 C2 1 0.311012 0.727599 0.465521 11.00000 0.02560 0.01636 = 0.01943 -0.00051 0.00400 0.00312 AFIX 43 H2 2 0.259195 0.753961 0.488600 11.00000 -1.20000 AFIX 0 N4 3 0.224513 0.494306 0.680094 11.00000 0.01770 0.01235 = 0.01787 -0.00165 0.00170 0.00104 C4 1 0.432594 0.757171 0.382275 11.00000 0.02864 0.02200 = 0.01631 0.00197 0.00108 -0.00423 AFIX 43 H4 2 0.464883 0.803926 0.349350 11.00000 -1.20000 AFIX 0 N5 3 0.134765 0.739712 0.602077 11.00000 0.02007 0.01248 = 0.01576 -0.00038 0.00057 0.00051 C5 1 0.461369 0.650279 0.397414 11.00000 0.02435 0.02434 = 0.01943 -0.00001 0.00169 0.00242 AFIX 43 H5 2 0.512608 0.623789 0.373458 11.00000 -1.20000 AFIX 0 N7 3 0.272384 0.832879 0.709654 11.00000 0.02091 0.01254 = 0.01516 0.00084 0.00185 0.00284 C7 1 0.288323 0.380768 0.588771 11.00000 0.01729 0.01349 = 0.01754 -0.00064 -0.00052 0.00023 N6 3 0.123818 0.827523 0.645582 11.00000 0.02130 0.01417 = 0.01483 0.00072 0.00189 0.00219 C6 1 0.416390 0.582317 0.446787 11.00000 0.02371 0.01664 = 0.01924 0.00037 -0.00139 0.00218 AFIX 43 H6 2 0.436514 0.509547 0.456752 11.00000 -1.20000 AFIX 0 N8 3 0.303380 0.744384 0.677754 11.00000 0.01905 0.01279 = 0.01582 0.00116 0.00122 0.00222 C8 1 0.311953 0.264173 0.572600 11.00000 0.01953 0.01434 = 0.01738 -0.00143 -0.00236 0.00157 C9 1 0.365518 0.237260 0.510287 11.00000 0.02851 0.01535 = 0.01820 0.00007 0.00267 -0.00090 AFIX 43 H9 2 0.383780 0.293294 0.475725 11.00000 -1.20000 AFIX 0 C20 1 0.068910 0.728840 0.539227 11.00000 0.01759 0.01713 = 0.01502 0.00189 0.00245 -0.00274 C21 1 0.004307 0.808107 0.522297 11.00000 0.02185 0.01880 = 0.01759 0.00073 0.00423 -0.00007 AFIX 43 H21 2 0.001223 0.871960 0.554163 11.00000 -1.20000 AFIX 0 C22 1 -0.055364 0.793248 0.458752 11.00000 0.01883 0.02769 = 0.02180 0.00355 0.00118 0.00230 AFIX 43 H22 2 -0.099645 0.846978 0.447561 11.00000 -1.20000 AFIX 0 C23 1 -0.051187 0.700621 0.411177 11.00000 0.02216 0.02848 = 0.02189 0.00071 -0.00249 -0.00683 AFIX 43 H23 2 -0.091942 0.691521 0.367403 11.00000 -1.20000 AFIX 0 C24 1 0.012761 0.621775 0.428046 11.00000 0.02917 0.01997 = 0.02555 -0.00471 -0.00124 -0.00506 AFIX 43 H24 2 0.015623 0.558118 0.395954 11.00000 -1.20000 AFIX 0 C25 1 0.072740 0.635413 0.491716 11.00000 0.02400 0.01669 = 0.02499 -0.00170 0.00016 0.00144 AFIX 43 H25 2 0.116506 0.581079 0.503013 11.00000 -1.20000 AFIX 0 C26 1 0.185855 0.861702 0.699122 11.00000 0.01945 0.01225 = 0.01620 0.00164 0.00130 0.00131 C27 1 0.161391 0.958017 0.747430 11.00000 0.02042 0.01432 = 0.01626 0.00066 0.00307 0.00022 C28 1 0.086595 1.021418 0.727885 11.00000 0.02474 0.02125 = 0.02309 -0.00425 -0.00279 0.00397 AFIX 43 H28 2 0.048790 1.001467 0.683977 11.00000 -1.20000 AFIX 0 C29 1 0.067292 1.112878 0.771989 11.00000 0.02605 0.02257 = 0.03296 -0.00535 -0.00078 0.00771 AFIX 43 H29 2 0.016770 1.155906 0.757611 11.00000 -1.20000 AFIX 0 C30 1 0.120947 1.142636 0.837144 11.00000 0.03167 0.01893 = 0.02649 -0.00733 0.00658 -0.00074 AFIX 43 H30 2 0.107233 1.205429 0.867401 11.00000 -1.20000 AFIX 0 C31 1 0.194595 1.079708 0.857425 11.00000 0.02749 0.02363 = 0.01868 -0.00419 0.00196 -0.00194 AFIX 43 H31 2 0.231546 1.099322 0.901972 11.00000 -1.20000 AFIX 0 C32 1 0.214854 0.988149 0.813145 11.00000 0.02462 0.01932 = 0.01927 0.00008 -0.00026 0.00286 AFIX 43 H32 2 0.265573 0.945562 0.827674 11.00000 -1.20000 AFIX 0 C33 1 0.397896 0.737327 0.685353 11.00000 0.01902 0.01907 = 0.01207 0.00024 0.00161 0.00304 C34 1 0.436598 0.633320 0.685441 11.00000 0.02323 0.01722 = 0.01838 -0.00263 0.00094 0.00329 AFIX 43 H34 2 0.400695 0.569693 0.679164 11.00000 -1.20000 AFIX 0 C35 1 0.527750 0.623261 0.694738 11.00000 0.02660 0.02101 = 0.02121 -0.00287 0.00019 0.00911 AFIX 43 H35 2 0.554148 0.552507 0.695821 11.00000 -1.20000 AFIX 0 C36 1 0.580393 0.716007 0.702446 11.00000 0.01950 0.03212 = 0.02242 -0.00094 0.00367 0.00286 AFIX 43 H36 2 0.642782 0.708892 0.708554 11.00000 -1.20000 AFIX 0 C37 1 0.541683 0.819503 0.701220 11.00000 0.02324 0.02494 = 0.02182 0.00032 0.00511 -0.00293 AFIX 43 H37 2 0.577891 0.883025 0.706217 11.00000 -1.20000 AFIX 0 C38 1 0.450370 0.830806 0.692735 11.00000 0.02373 0.01688 = 0.01792 0.00169 0.00496 0.00210 AFIX 43 H38 2 0.424113 0.901639 0.691989 11.00000 -1.20000 AFIX 0 C18 1 0.138836 0.607304 0.863593 11.00000 0.02506 0.01735 = 0.02305 -0.00262 0.00555 0.00028 AFIX 43 H18 2 0.112120 0.673349 0.880292 11.00000 -1.20000 AFIX 0 C10 1 0.392149 0.129697 0.498541 11.00000 0.03340 0.01986 = 0.01924 -0.00493 0.00248 0.00445 AFIX 43 H10 2 0.428800 0.112810 0.456333 11.00000 -1.20000 AFIX 0 C11 1 0.365669 0.047124 0.547857 11.00000 0.03512 0.01264 = 0.02623 -0.00393 -0.00292 0.00652 AFIX 43 H11 2 0.384799 -0.026252 0.540405 11.00000 -1.20000 AFIX 0 C13 1 0.284414 0.179499 0.620691 11.00000 0.02551 0.01692 = 0.02154 -0.00056 0.00219 0.00105 AFIX 43 H13 2 0.246971 0.195362 0.662529 11.00000 -1.20000 AFIX 0 C14 1 0.200084 0.498977 0.760484 11.00000 0.01616 0.01577 = 0.01796 -0.00035 0.00132 -0.00281 C15 1 0.216377 0.413662 0.814231 11.00000 0.02461 0.01430 = 0.02494 0.00061 0.00319 0.00298 AFIX 43 H15 2 0.242585 0.347244 0.797625 11.00000 -1.20000 AFIX 0 C16 1 0.194088 0.426489 0.891898 11.00000 0.02770 0.02081 = 0.02228 0.00559 0.00283 0.00085 AFIX 43 H16 2 0.205366 0.368553 0.928449 11.00000 -1.20000 AFIX 0 C17 1 0.155529 0.522829 0.916928 11.00000 0.02297 0.02347 = 0.01777 -0.00049 0.00552 -0.00205 AFIX 43 H17 2 0.140638 0.530890 0.970327 11.00000 -1.20000 AFIX 0 C12 1 0.311004 0.072371 0.608213 11.00000 0.03238 0.01413 = 0.02741 0.00248 0.00362 0.00142 AFIX 43 H12 2 0.291455 0.015561 0.641514 11.00000 -1.20000 AFIX 0 C19 1 0.161187 0.595272 0.785830 11.00000 0.02179 0.01478 = 0.02104 0.00224 0.00341 0.00138 AFIX 43 H19 2 0.149801 0.653440 0.749494 11.00000 -1.20000 REM ##### AFIX 0 HKLF 4 REM cu_molan529_0m_a.res in P2(1)/c REM R1 = 0.0343 for 5463 Fo > 4sig(Fo) and 0.0378 for all 5886 data REM 424 parameters refined using 0 restraints END WGHT 0.0331 2.4692 REM Highest difference peak 0.315, deepest hole -0.426, 1-sigma level 0.050 Q1 1 0.2566 0.5772 0.5749 11.00000 0.05 0.31 Q2 1 0.1744 0.6864 0.5958 11.00000 0.05 0.29 Q3 1 0.2215 0.5542 0.6651 11.00000 0.05 0.26 Q4 1 0.2552 0.6954 0.5936 11.00000 0.05 0.24 Q5 1 0.2433 0.3405 0.7000 11.00000 0.05 0.24 Q6 1 0.2429 0.6891 0.5735 11.00000 0.05 0.23 Q7 1 0.3142 0.3159 0.5873 11.00000 0.05 0.23 Q8 1 0.1831 0.9662 0.7808 11.00000 0.05 0.23 Q9 1 0.1737 0.9050 0.7295 11.00000 0.05 0.22 Q10 1 0.1389 0.5878 0.8180 11.00000 0.05 0.22 Q11 1 0.3064 0.2221 0.5957 11.00000 0.05 0.22 Q12 1 0.3413 0.2472 0.5423 11.00000 0.05 0.21 Q13 1 0.4188 0.6858 0.6614 11.00000 0.05 0.21 Q14 1 0.2168 0.4634 0.7860 11.00000 0.05 0.20 Q15 1 0.2046 0.4889 0.7251 11.00000 0.05 0.20 Q16 1 0.0356 0.7630 0.5270 11.00000 0.05 0.20 Q17 1 0.1404 0.5547 0.8838 11.00000 0.05 0.19 Q18 1 0.1837 0.5468 0.7747 11.00000 0.05 0.18 Q19 1 0.3371 0.6860 0.4941 11.00000 0.05 0.18 Q20 1 0.0837 0.6901 0.5119 11.00000 0.05 0.18 ; _shelx_res_checksum 8009 _shelx_hkl_file ; 1 0 0 -6.50 0.70 -1 0 0 -6.00 0.70 1 0 0 -7.00 0.20 -2 0 0 5450.45 283.87 2 0 0 5629.24 283.87 3 0 0 59.99 3.30 -3 0 0 60.99 3.30 3 0 0 63.19 5.40 -3 0 0 60.99 5.20 4 0 0 238.08 14.90 -4 0 0 235.48 14.70 4 0 0 244.98 12.40 -4 0 0 232.18 12.40 5 0 0 119.99 6.40 5 0 0 117.69 10.40 -5 0 0 118.59 10.00 -5 0 0 119.49 6.40 6 0 0 582.24 29.00 -6 0 0 497.25 29.20 6 0 0 600.14 33.40 -6 0 0 573.94 33.00 -7 0 0 83.39 13.50 7 0 0 93.39 5.30 7 0 0 104.89 14.60 7 0 0 87.99 5.30 8 0 0 442.26 23.50 8 0 0 460.55 23.50 -8 0 0 446.76 23.50 9 0 0 505.35 27.70 9 0 0 529.95 27.60 -9 0 0 552.14 27.90 10 0 0 10.20 1.70 -10 0 0 12.50 2.20 10 0 0 12.70 2.50 11 0 0 360.76 19.30 -11 0 0 352.16 19.50 11 0 0 370.36 19.80 12 0 0 145.29 9.30 -12 0 0 142.39 8.70 12 0 0 147.49 8.60 13 0 0 888.01 46.00 -13 0 0 849.52 45.50 13 0 0 887.41 45.60 14 0 0 253.97 14.50 -14 0 0 248.48 13.90 14 0 0 248.48 14.00 15 0 0 16.40 2.60 -15 0 0 20.70 3.30 15 0 0 18.70 3.00 16 0 0 36.10 4.10 16 0 0 37.40 4.20 -16 0 0 31.70 3.50 17 0 0 268.77 14.40 -17 0 0 267.57 14.00 17 0 0 251.87 14.50 18 0 0 1.40 1.90 18 0 0 2.20 1.80 0 -1 0 1.80 0.70 1 -1 0 1781.32 88.49 -1 1 0 1647.64 88.29 2 -1 0 177.78 9.90 2 -1 0 173.88 9.00 -2 -1 0 179.08 10.60 -2 1 0 168.18 9.00 2 1 0 174.28 10.60 -2 1 0 174.18 9.80 3 -1 0 12.30 2.50 -3 -1 0 13.60 1.10 3 -1 0 15.40 1.00 -3 -1 0 18.20 4.40 -3 1 0 10.80 2.20 -3 1 0 11.50 0.90 3 1 0 14.20 1.10 3 1 0 15.90 3.50 -4 -1 0 763.82 41.90 4 -1 0 775.02 39.20 -4 -1 0 742.03 39.30 4 -1 0 792.62 41.30 4 1 0 809.32 42.00 4 1 0 748.83 39.30 -4 1 0 764.82 41.00 -4 1 0 726.93 39.20 -5 -1 0 32.50 2.00 5 -1 0 27.50 1.90 -5 -1 0 42.80 7.60 5 -1 0 32.60 5.40 5 1 0 21.50 4.90 -5 1 0 19.10 4.30 -5 1 0 29.50 1.80 5 1 0 29.00 2.00 6 -1 0 342.07 22.80 6 -1 0 318.57 19.00 -6 -1 0 371.86 18.80 -6 -1 0 360.36 24.00 -6 1 0 365.96 22.40 6 1 0 393.66 24.40 6 1 0 377.16 18.80 7 -1 0 61.29 3.90 -7 -1 0 63.19 11.10 -7 -1 0 61.89 3.80 7 -1 0 61.39 3.70 7 -1 0 61.39 9.90 7 1 0 62.29 3.80 -7 1 0 51.39 9.20 7 1 0 57.79 3.90 7 1 0 61.19 10.70 8 -1 0 9.60 1.40 8 -1 0 11.80 2.10 -8 -1 0 13.10 1.90 8 1 0 12.10 1.60 -8 1 0 11.30 1.40 8 1 0 10.60 1.60 9 -1 0 138.19 7.60 -9 -1 0 137.09 8.10 9 1 0 132.99 7.60 -9 1 0 129.99 7.80 9 1 0 123.29 7.80 9 1 0 135.59 8.40 10 -1 0 474.85 25.80 -10 -1 0 483.55 25.50 10 -1 0 474.45 25.20 10 1 0 486.65 25.30 -10 1 0 494.95 25.40 10 1 0 471.75 25.80 11 -1 0 170.78 9.70 11 -1 0 182.98 10.60 -11 1 0 168.78 9.80 11 1 0 168.18 9.80 11 1 0 167.48 10.40 -12 -1 0 49.99 4.70 12 -1 0 54.99 4.40 12 -1 0 54.79 5.40 12 1 0 53.89 4.60 -12 1 0 55.19 4.50 12 1 0 57.49 5.30 13 -1 0 0.80 1.90 -13 -1 0 0.40 2.00 13 -1 0 0.80 2.30 13 1 0 -2.10 2.00 -13 1 0 1.30 1.80 13 1 0 1.90 2.30 -14 -1 0 198.48 11.90 14 -1 0 203.68 11.80 14 -1 0 221.18 12.30 14 1 0 203.48 12.40 -14 1 0 209.88 11.70 14 1 0 212.78 12.00 15 -1 0 48.70 4.50 15 -1 0 49.60 5.60 -15 -1 0 45.20 4.50 -15 1 0 50.49 4.10 15 1 0 49.10 5.10 15 1 0 45.30 4.60 16 -1 0 7.10 2.20 -16 -1 0 6.70 1.90 16 -1 0 8.40 2.10 16 1 0 8.30 2.30 -16 1 0 6.40 1.70 16 1 0 4.10 2.30 17 -1 0 2.30 1.80 -17 -1 0 3.80 1.60 17 -1 0 4.20 1.80 17 1 0 3.30 2.00 17 1 0 3.50 2.10 18 -1 0 144.29 8.40 18 -1 0 148.99 8.40 18 1 0 145.89 8.40 18 1 0 130.09 8.70 -1 -2 0 584.14 31.00 -1 -2 0 651.73 32.60 -1 2 0 653.73 33.00 -1 2 0 556.04 31.00 1 2 0 629.34 32.50 1 2 0 568.54 31.00 -2 -2 0 3339.27 168.48 2 -2 0 3310.67 167.68 2 -2 0 2981.80 168.18 2 2 0 3399.56 168.58 -3 -2 0 2143.79 115.39 3 -2 0 2128.89 114.29 3 -2 0 2210.78 114.49 3 2 0 2359.46 115.69 4 -2 0 179.78 12.00 4 -2 0 174.38 11.80 4 -2 0 185.28 9.60 -4 -2 0 182.98 13.50 -4 -2 0 185.78 9.70 -4 2 0 187.38 9.60 4 2 0 176.08 9.70 4 2 0 193.18 13.70 5 -2 0 838.92 46.10 -5 -2 0 874.81 43.70 5 -2 0 841.22 43.60 -5 2 0 877.51 43.50 5 2 0 815.42 48.60 5 2 0 834.82 43.70 6 -2 0 254.87 13.40 -6 -2 0 233.08 20.00 6 -2 0 253.57 18.00 6 2 0 260.77 20.60 6 2 0 251.57 13.60 -6 2 0 275.97 13.40 -7 -2 0 487.15 33.90 -7 -2 0 502.35 25.70 7 -2 0 502.15 25.50 -7 2 0 512.55 25.50 7 2 0 462.95 33.70 7 2 0 460.95 26.00 7 2 0 502.25 25.70 -8 -2 0 22.90 2.60 8 -2 0 18.20 2.50 -8 -2 0 18.30 3.20 8 -2 0 21.10 2.20 8 2 0 20.10 2.50 -8 2 0 24.10 2.00 8 2 0 17.50 2.60 9 -2 0 3.10 1.30 -9 -2 0 3.60 1.80 9 2 0 1.60 1.40 -9 2 0 4.20 1.60 9 2 0 4.20 2.10 -10 -2 0 144.19 8.70 10 -2 0 149.99 9.40 10 -2 0 141.99 8.10 10 2 0 141.69 8.30 10 2 0 139.49 9.00 -10 2 0 139.99 8.30 11 -2 0 1.20 1.40 11 -2 0 7.60 2.60 -11 -2 0 2.60 2.00 -11 2 0 2.30 2.00 11 2 0 -2.30 2.10 11 2 0 0.30 1.70 -12 -2 0 28.80 4.00 12 -2 0 37.70 4.80 12 -2 0 27.50 3.50 12 2 0 24.60 4.40 12 2 0 29.10 3.90 -12 2 0 26.30 3.40 13 -2 0 4.70 1.90 13 -2 0 3.70 2.50 -13 -2 0 8.10 2.50 13 2 0 5.80 2.60 13 2 0 4.90 2.40 -13 2 0 5.80 1.90 -14 -2 0 2.00 2.20 14 -2 0 0.90 1.80 14 -2 0 0.70 2.30 14 2 0 -1.70 2.00 -14 2 0 0.20 1.80 14 2 0 -0.50 2.40 15 -2 0 35.90 3.90 -15 -2 0 29.90 3.90 15 -2 0 32.70 4.30 15 2 0 29.10 4.20 -15 2 0 28.40 3.50 15 2 0 31.20 4.90 16 -2 0 163.88 9.30 -16 -2 0 152.18 9.20 16 -2 0 154.88 9.50 16 2 0 160.68 9.80 16 2 0 161.48 9.60 -17 -2 0 99.29 6.10 17 -2 0 94.69 6.60 17 -2 0 102.69 6.20 17 2 0 102.39 6.70 18 -2 0 -6.20 3.10 18 -2 0 2.30 1.80 18 2 0 -1.70 1.50 0 -3 0 0.90 0.40 0 -3 0 0.20 0.30 0 -3 0 2.20 2.20 0 3 0 -3.10 2.30 -1 -3 0 193.28 12.60 -1 -3 0 191.78 10.40 1 -3 0 209.98 10.40 1 -3 0 220.38 10.40 1 -3 0 212.18 12.70 1 3 0 177.18 12.60 1 3 0 196.08 10.40 -1 3 0 179.48 13.50 -2 -3 0 184.88 12.60 -2 -3 0 175.58 9.50 2 -3 0 203.18 12.70 2 -3 0 154.08 9.40 2 3 0 191.88 9.50 -2 3 0 182.98 11.80 2 3 0 182.88 12.50 3 -3 0 38.20 5.40 3 -3 0 42.50 2.30 -3 -3 0 36.80 2.40 -3 -3 0 30.60 5.20 3 -3 0 33.60 6.40 3 3 0 38.40 2.40 3 3 0 29.70 5.10 -3 3 0 41.20 2.20 4 -3 0 341.77 17.80 4 -3 0 321.07 21.40 -4 -3 0 335.97 22.10 4 -3 0 349.96 20.10 -4 -3 0 357.56 18.00 4 3 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4 -4 0 1872.91 93.69 4 -4 0 1761.32 90.99 -4 -4 0 1724.03 91.19 -4 -4 0 1715.83 95.79 4 -4 0 1893.21 95.29 -4 4 0 1606.04 90.99 4 4 0 1870.21 96.09 4 4 0 1791.62 91.19 -5 -4 0 111.39 6.30 5 -4 0 115.69 6.00 5 -4 0 103.09 16.70 5 -4 0 99.99 11.30 -5 -4 0 120.29 16.90 5 4 0 98.29 16.60 5 4 0 112.59 6.40 -6 -4 0 442.76 33.10 -6 -4 0 450.45 22.60 -6 -4 0 416.86 22.70 6 -4 0 379.36 31.80 6 -4 0 442.86 22.40 -6 4 0 440.46 22.30 6 4 0 442.76 22.80 6 4 0 384.26 32.60 6 4 0 444.66 22.70 -7 -4 0 29.60 2.90 7 -4 0 25.10 3.10 -7 -4 0 23.40 3.70 7 -4 0 25.90 2.20 -7 -4 0 18.30 17.10 7 4 0 25.50 3.80 -7 4 0 26.40 2.00 7 4 0 24.10 3.10 7 4 0 22.70 3.00 -8 -4 0 561.54 29.40 -8 -4 0 502.95 29.30 8 -4 0 556.34 28.80 -8 -4 0 584.04 29.00 -8 4 0 538.25 28.90 8 4 0 537.45 29.30 8 4 0 558.04 29.40 8 4 0 589.74 29.20 9 -4 0 244.38 13.40 -9 -4 0 236.48 13.80 9 4 0 250.17 13.60 -9 4 0 241.28 13.30 9 4 0 250.07 13.90 10 -4 0 220.38 12.20 -10 -4 0 221.18 12.90 -10 4 0 225.58 12.30 10 4 0 234.18 13.20 10 4 0 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32.10 3 -5 0 684.93 36.80 -3 -5 0 584.14 38.20 -3 -5 0 575.64 32.20 3 -5 0 644.74 31.90 3 5 0 582.04 38.30 3 5 0 629.24 32.10 4 -5 0 55.09 9.50 4 -5 0 56.09 3.20 -4 -5 0 51.49 3.50 -4 -5 0 33.10 8.90 4 5 0 48.10 3.50 4 5 0 50.79 12.30 5 -5 0 347.07 24.60 -5 -5 0 308.57 17.30 5 -5 0 334.57 17.00 -5 -5 0 327.67 17.20 5 5 0 316.77 17.30 -6 -5 0 842.02 42.60 6 -5 0 810.52 42.30 -6 -5 0 804.52 42.70 6 5 0 817.72 43.10 6 5 0 802.82 42.70 6 5 0 850.61 43.20 -7 -5 0 3.40 2.10 7 -5 0 9.00 1.40 7 -5 0 11.30 1.90 -7 -5 0 5.70 2.20 7 5 0 7.70 2.40 7 5 0 4.80 1.90 7 5 0 7.80 1.90 8 -5 0 1433.66 73.69 -8 -5 0 1487.65 74.29 -8 -5 0 1572.74 73.89 8 5 0 1532.75 74.49 -8 5 0 1363.46 73.59 8 5 0 1207.08 73.89 9 -5 0 66.19 4.70 -9 -5 0 70.29 5.70 -9 -5 0 62.89 5.60 -9 5 0 65.69 4.70 9 5 0 57.69 8.20 10 -5 0 194.18 10.80 -10 -5 0 190.38 11.60 -10 5 0 186.58 10.70 10 5 0 203.78 12.00 -11 -5 0 56.09 5.50 11 -5 0 60.39 4.50 11 5 0 56.69 6.00 -11 5 0 57.59 5.60 12 -5 0 26.40 3.40 -12 -5 0 18.50 3.10 12 5 0 9.40 2.60 12 5 0 15.70 3.50 -13 -5 0 -1.20 2.50 13 -5 0 3.30 1.80 13 5 0 -1.10 2.80 13 5 0 -3.50 2.00 -14 -5 0 80.29 6.30 14 -5 0 85.29 5.70 14 5 0 75.49 7.30 -15 -5 0 29.60 4.10 15 5 0 23.90 3.50 15 5 0 21.30 3.30 16 -5 0 11.60 2.40 -16 -5 0 11.60 2.30 16 5 0 7.50 2.40 17 -5 0 16.20 2.70 -17 -5 0 19.90 2.90 0 -6 0 65.59 4.00 0 -6 0 62.79 3.90 0 -6 0 62.99 4.30 -1 -6 0 226.08 12.70 1 -6 0 250.37 12.80 1 -6 0 240.68 12.70 -1 -6 0 245.78 12.80 1 -6 0 287.37 26.10 -1 -6 0 235.68 12.80 1 -6 0 219.18 12.90 2 -6 0 127.29 7.50 -2 -6 0 134.99 7.50 2 -6 0 139.09 7.50 -2 -6 0 132.59 7.60 -2 -6 0 138.29 7.60 -3 -6 0 646.24 33.90 -3 -6 0 642.64 33.90 3 -6 0 653.23 33.80 -3 -6 0 665.43 34.00 -4 -6 0 596.94 31.00 -4 -6 0 581.64 31.00 4 -6 0 563.44 30.80 4 -6 0 612.94 30.80 -4 -6 0 614.54 31.20 -4 -6 0 602.24 31.60 4 6 0 585.94 31.60 5 -6 0 3.60 1.20 5 -6 0 2.80 1.20 -5 -6 0 2.40 1.50 -5 -6 0 5.50 1.90 -5 -6 0 5.10 1.40 5 6 0 2.00 2.30 5 6 0 3.10 2.60 -6 -6 0 174.68 11.10 -6 -6 0 178.98 10.60 -6 -6 0 175.48 9.90 6 6 0 190.28 11.10 6 6 0 160.58 10.40 6 6 0 180.78 10.90 -7 -6 0 100.59 7.10 7 -6 0 103.29 6.20 -7 -6 0 104.09 6.20 -7 6 0 93.89 6.40 7 6 0 102.49 7.10 7 6 0 78.99 6.50 8 -6 0 244.28 13.60 -8 -6 0 252.77 14.50 -8 -6 0 259.27 13.90 8 6 0 247.68 14.50 9 -6 0 190.88 11.00 -9 -6 0 195.28 11.40 -9 -6 0 204.58 12.10 9 6 0 206.18 12.40 10 -6 0 105.89 6.50 -10 -6 0 110.59 7.60 10 6 0 82.59 6.70 10 6 0 107.39 8.00 -11 -6 0 202.68 11.60 11 -6 0 189.58 10.50 11 6 0 191.38 12.10 11 6 0 160.48 10.80 12 -6 0 50.59 4.20 -12 -6 0 44.90 5.60 12 6 0 40.70 6.10 12 6 0 54.29 4.80 -13 -6 0 -0.20 2.60 13 -6 0 1.40 1.80 13 6 0 -3.60 2.60 13 6 0 8.20 2.70 -14 -6 0 0.30 2.30 14 -6 0 2.50 1.90 14 6 0 -3.20 2.50 15 -6 0 11.70 2.30 -15 -6 0 10.40 2.50 16 -6 0 95.29 6.60 -16 -6 0 93.69 6.10 0 -7 0 1.20 1.20 0 -7 0 0.60 1.20 0 -7 0 1.00 1.30 0 7 0 -1.20 2.50 1 -7 0 93.99 5.70 -1 -7 0 87.89 5.70 -1 -7 0 102.89 5.90 1 -7 0 99.39 5.80 1 -7 0 93.69 5.70 -1 -7 0 94.79 5.80 1 7 0 83.79 6.80 -2 -7 0 8.40 2.80 2 -7 0 7.60 1.50 -2 -7 0 9.00 1.60 -2 -7 0 9.60 1.90 2 -7 0 10.10 1.80 2 -7 0 8.60 1.60 -2 -7 0 10.40 2.20 -2 7 0 7.00 2.70 2 7 0 5.10 2.40 -3 -7 0 85.99 6.80 -3 -7 0 83.49 5.40 3 -7 0 82.79 6.20 -3 -7 0 84.89 6.00 -3 -7 0 82.79 5.80 3 7 0 85.89 6.70 4 -7 0 38.30 4.80 -4 -7 0 34.20 3.30 -4 -7 0 25.70 3.00 4 7 0 25.30 3.70 -4 7 0 18.20 3.50 4 7 0 26.90 4.40 -5 -7 0 11.40 4.00 -5 -7 0 8.20 1.70 5 -7 0 10.80 2.60 5 7 0 10.20 2.90 -5 7 0 7.90 2.90 5 7 0 10.70 2.90 -6 -7 0 32.50 3.40 -6 -7 0 39.90 5.70 -6 7 0 26.60 3.60 6 7 0 26.00 4.70 6 7 0 41.80 5.20 7 -7 0 5.90 2.20 -7 -7 0 3.70 2.90 -7 -7 0 2.50 1.90 7 7 0 1.20 4.10 -8 -7 0 26.00 4.00 -8 -7 0 16.60 2.70 8 -7 0 22.10 3.80 8 7 0 16.10 3.50 -9 -7 0 33.60 4.10 9 -7 0 27.40 4.00 -9 -7 0 31.80 5.20 9 7 0 23.60 3.90 10 -7 0 276.87 15.20 -10 -7 0 301.77 16.30 10 7 0 253.37 16.30 11 -7 0 26.40 3.80 -11 -7 0 27.30 3.90 11 7 0 15.80 3.70 -12 -7 0 85.29 6.80 12 -7 0 83.09 5.80 12 7 0 59.19 6.80 -13 -7 0 -1.20 2.50 13 -7 0 2.10 2.20 -14 -7 0 42.80 4.70 14 -7 0 40.20 4.70 14 7 0 27.90 3.80 15 -7 0 4.50 2.60 -15 -7 0 1.00 2.10 15 7 0 -2.60 1.90 16 -7 0 12.50 2.90 -16 -7 0 6.90 1.80 16 7 0 6.40 1.80 0 -8 0 1824.62 91.59 0 -8 0 1816.82 90.99 0 8 0 1665.93 91.49 1 -8 0 8.20 1.60 -1 -8 0 7.20 2.40 -1 -8 0 8.90 1.70 -1 8 0 4.00 2.60 1 8 0 7.50 2.80 2 -8 0 360.76 19.50 -2 -8 0 382.16 20.20 -2 -8 0 374.96 19.70 2 8 0 354.76 20.40 -3 -8 0 219.78 11.60 -3 -8 0 216.78 11.90 3 -8 0 189.68 11.30 3 8 0 191.58 12.30 4 -8 0 113.99 7.50 -4 -8 0 119.79 7.30 4 8 0 115.19 8.30 -5 -8 0 230.78 14.90 -5 -8 0 201.68 11.90 5 -8 0 190.88 12.30 5 8 0 218.18 13.00 -6 -8 0 360.46 20.10 6 -8 0 370.56 20.60 6 8 0 381.96 21.00 -7 -8 0 368.96 19.90 -7 -8 0 367.76 20.80 7 -8 0 356.46 20.20 8 -8 0 81.79 6.80 -8 -8 0 70.69 7.40 -8 -8 0 72.79 5.90 9 -8 0 262.87 15.00 -9 -8 0 269.17 15.70 -9 -8 0 250.47 14.60 10 -8 0 20.50 3.20 -10 -8 0 27.90 4.40 -11 -8 0 348.47 19.60 11 -8 0 336.77 19.00 12 -8 0 30.50 5.20 -12 -8 0 22.30 3.50 12 8 0 14.40 3.20 13 -8 0 268.57 15.70 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4 117.09 8.20 -16 -6 -4 47.80 3.70 16 -6 4 41.70 4.50 16 6 4 43.50 5.80 16 7 -4 14.00 3.30 -15 -7 4 57.09 4.70 15 7 -4 58.49 4.90 -14 -7 4 4.00 2.40 14 7 -4 0.70 2.20 13 7 -4 62.89 5.70 -12 -7 4 49.50 6.10 12 7 -4 67.69 5.10 -11 -7 4 21.80 4.10 -10 -7 4 378.36 22.20 10 7 -4 411.26 21.20 -9 -7 4 4.00 2.90 9 7 -4 -0.60 2.70 -8 -7 4 285.27 15.90 8 7 -4 286.57 14.70 8 7 -4 222.68 16.40 -7 -7 4 34.20 4.40 7 7 -4 22.70 3.50 7 7 -4 24.10 4.10 -6 -7 4 8.50 2.10 -6 -7 4 10.70 3.10 6 7 -4 2.30 3.10 -5 -7 4 16.60 3.60 -5 -7 4 14.50 2.30 -5 -7 4 16.80 2.40 5 7 -4 10.10 3.40 5 7 -4 12.30 2.80 5 7 -4 17.00 2.30 -4 -7 4 263.97 14.40 -4 -7 4 254.07 13.90 4 7 -4 259.27 14.10 4 7 -4 231.78 14.50 -3 -7 4 442.16 21.70 -3 -7 4 386.86 22.30 -3 -7 4 404.16 21.10 3 7 -4 348.37 21.90 3 7 -4 399.06 21.70 -2 -7 4 5.70 1.80 -2 -7 4 4.70 1.50 -2 -7 4 4.90 3.90 -2 -7 4 9.50 5.60 2 7 -4 2.40 2.40 2 7 -4 1.20 2.50 -1 -7 4 225.78 13.60 1 -7 -4 233.08 13.30 -1 -7 4 282.07 15.20 -1 -7 4 241.48 13.30 1 7 -4 249.78 14.10 1 7 -4 244.38 14.10 0 -7 4 1.50 1.20 0 -7 4 1.30 1.60 0 -7 -4 1.30 1.50 0 7 -4 2.50 2.10 0 7 -4 -4.60 2.60 1 -7 4 17.50 2.40 -1 -7 -4 15.00 2.50 1 -7 4 18.00 2.50 -1 7 -4 20.10 3.40 2 -7 4 2.20 1.80 2 -7 4 2.30 1.40 -2 -7 -4 1.60 1.30 -2 7 -4 0.70 1.70 3 -7 4 132.89 7.80 -3 -7 -4 132.39 7.70 3 -7 4 127.19 8.20 -3 7 -4 135.19 7.90 -4 -7 -4 9.10 1.70 4 -7 4 12.80 2.70 4 -7 4 6.70 2.20 -4 7 -4 11.20 2.10 -5 -7 -4 129.79 8.10 5 -7 4 135.99 8.90 5 -7 4 146.29 9.20 -5 7 -4 137.99 8.10 -6 -7 -4 27.30 3.30 6 -7 4 40.40 5.60 6 -7 4 22.00 3.60 6 7 4 29.20 4.00 -7 -7 -4 77.69 7.60 7 -7 4 68.79 6.50 -7 -7 -4 70.89 5.30 7 -7 4 91.09 7.60 7 7 4 67.99 6.60 -7 7 -4 72.69 5.20 8 -7 4 8.70 2.90 -8 -7 -4 14.10 3.40 -8 -7 -4 14.00 2.40 8 -7 4 6.20 3.80 8 7 4 11.30 3.00 -8 7 -4 10.30 2.10 9 -7 4 75.79 6.70 -9 -7 -4 77.29 5.80 9 -7 4 97.69 8.50 -9 -7 -4 75.99 7.10 9 7 4 76.99 6.90 -9 7 -4 82.39 5.50 10 -7 4 715.53 38.30 10 -7 4 604.04 37.80 -10 -7 -4 736.93 37.80 10 7 4 756.42 38.00 -10 7 -4 729.53 36.90 11 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8 -4 743.73 38.80 -3 -8 4 89.79 8.40 -3 -8 4 93.89 6.60 -3 -8 4 89.49 6.00 3 8 -4 103.59 7.10 3 8 -4 85.59 7.30 -2 -8 4 647.04 35.20 -2 -8 4 683.83 35.80 -2 -8 4 617.94 36.40 2 8 -4 706.23 36.00 2 8 -4 716.23 35.80 1 -8 -4 46.10 4.20 -1 -8 4 52.49 4.10 -1 -8 4 46.80 4.50 1 8 -4 63.09 5.80 1 8 -4 62.39 5.20 0 -8 4 171.18 9.60 0 -8 -4 167.38 9.60 0 -8 4 156.58 9.90 0 8 -4 183.58 10.30 0 8 -4 169.98 10.80 1 -8 4 73.19 5.40 1 -8 4 74.29 5.10 -1 -8 -4 81.89 5.30 -1 8 -4 87.29 6.00 2 -8 4 32.80 3.30 2 -8 4 31.90 3.70 -2 -8 -4 37.60 3.50 -2 8 -4 40.90 4.10 -3 -8 -4 73.99 5.10 3 -8 4 69.19 5.00 3 -8 4 66.59 5.30 -3 8 -4 73.29 5.60 4 -8 4 323.97 17.30 4 -8 4 310.47 17.50 -4 -8 -4 325.77 17.30 -4 8 -4 313.27 17.20 5 -8 4 16.00 2.70 -5 -8 -4 8.70 2.20 5 -8 4 9.70 2.40 -5 8 -4 10.80 2.20 -6 -8 -4 152.18 9.50 6 -8 4 161.48 10.00 6 -8 4 165.38 9.90 -6 8 -4 153.98 9.20 7 -8 4 12.00 3.10 7 -8 4 13.30 2.80 -7 -8 -4 11.30 2.50 7 8 4 8.30 3.50 -7 8 -4 13.10 2.20 -8 -8 -4 141.79 10.50 -8 -8 -4 134.59 8.60 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-5 3 -9 8.20 2.20 -5 3 -9 3.80 2.00 5 3 9 5.40 2.90 6 -3 9 212.08 14.60 -6 -3 -9 239.78 14.30 -6 -3 -9 242.48 13.20 6 -3 9 235.68 15.10 6 -3 9 246.38 13.80 -6 3 -9 250.97 13.60 6 3 9 246.18 13.80 -6 3 -9 246.48 13.60 7 -3 9 238.58 14.00 7 -3 9 227.48 14.60 -7 -3 -9 249.97 13.30 -7 -3 -9 235.88 14.10 7 -3 9 240.08 15.20 -7 3 -9 237.18 13.60 -7 3 -9 251.67 13.70 7 3 9 243.98 14.00 -8 -3 -9 14.20 2.30 8 -3 9 9.90 3.30 8 -3 9 13.50 3.70 8 -3 9 12.10 4.30 -8 -3 -9 18.50 3.20 8 3 9 18.00 2.90 -8 3 -9 16.70 2.80 -8 3 -9 15.40 2.90 9 -3 9 29.30 4.20 -9 -3 -9 37.40 3.80 9 -3 9 46.80 6.60 9 -3 9 35.00 5.90 -9 -3 -9 39.00 5.00 -9 3 -9 43.10 4.50 9 3 9 40.10 4.90 -9 3 -9 36.40 4.70 9 3 9 37.80 5.00 -10 -3 -9 5.30 2.40 10 -3 9 9.00 3.30 10 -3 9 20.60 6.00 10 -3 9 1.20 3.10 -10 -3 -9 8.10 2.30 -10 3 -9 4.90 2.50 10 3 9 6.40 2.70 10 3 9 4.00 2.90 -10 3 -9 7.70 2.50 11 -3 9 26.90 4.10 11 -3 9 40.40 6.20 -11 -3 -9 32.60 4.70 11 3 9 37.40 4.90 -11 3 -9 39.20 4.90 11 3 9 37.00 5.40 12 -3 9 25.30 3.70 12 -3 9 22.50 4.20 -12 -3 -9 25.10 3.80 12 3 9 24.00 3.50 12 3 9 20.70 5.20 -12 3 -9 22.70 3.10 -13 -3 -9 4.40 2.10 -13 -3 -9 6.20 2.30 13 -3 9 8.70 2.80 13 -3 9 5.90 3.10 13 3 9 6.20 2.50 -13 3 -9 8.70 2.50 13 3 9 13.00 3.00 -14 -3 -9 31.90 3.50 14 -3 9 23.10 3.80 -14 -3 -9 33.30 3.90 14 3 9 35.80 4.50 14 3 9 28.10 4.40 -14 3 -9 35.00 3.70 15 -3 9 59.99 5.50 -15 -3 -9 72.49 4.80 15 3 9 72.99 5.80 -15 3 -9 75.09 4.50 15 3 9 59.19 6.20 16 4 -9 2.20 1.90 -14 -4 9 180.38 10.40 -13 -4 9 104.09 7.10 -12 -4 9 32.50 4.50 12 4 -9 24.30 3.90 -11 -4 9 -0.30 2.40 11 4 -9 -4.50 2.60 -10 -4 9 295.67 18.00 10 4 -9 343.97 17.70 -9 -4 9 345.87 19.60 9 4 -9 388.76 19.10 9 4 -9 315.77 19.80 -8 -4 9 94.19 7.40 8 4 -9 108.59 6.50 8 4 -9 95.09 7.70 -7 -4 9 32.30 4.60 7 4 -9 40.00 5.00 7 4 -9 29.10 3.40 6 4 -9 9.20 2.60 -5 -4 9 31.30 4.40 -5 -4 9 24.50 4.30 5 4 -9 26.20 2.90 5 4 -9 33.40 4.20 -4 -4 9 277.57 16.20 -4 -4 9 289.67 16.20 4 4 -9 302.37 16.10 4 4 -9 295.07 15.60 -3 -4 9 73.69 5.70 -3 -4 9 77.19 5.70 3 4 -9 73.39 8.20 3 4 -9 76.69 5.40 3 4 -9 74.69 4.80 -2 -4 9 53.19 4.60 -2 -4 9 51.49 4.90 2 4 -9 50.79 4.50 2 4 -9 55.59 3.80 2 4 -9 59.59 6.80 -1 -4 9 50.89 5.80 1 -4 -9 55.39 4.40 -1 -4 9 55.79 4.40 -1 -4 9 47.70 4.60 -1 -4 9 49.20 4.90 1 4 -9 51.39 3.70 1 4 -9 57.69 4.80 1 4 -9 39.40 5.60 1 4 -9 48.80 4.30 0 -4 9 16.70 2.30 0 -4 -9 21.10 3.00 0 -4 9 16.90 2.30 0 -4 9 16.20 2.90 0 -4 9 22.10 3.50 0 4 -9 18.10 2.50 0 4 -9 17.90 3.20 0 4 -9 17.80 2.70 0 4 9 18.40 2.50 0 4 -9 24.30 3.30 1 -4 9 0.30 1.70 1 -4 9 2.60 3.10 1 -4 9 3.10 1.50 1 -4 9 0.80 2.40 -1 -4 -9 1.10 1.40 -1 4 -9 -0.60 1.30 -1 4 -9 2.90 1.60 -1 4 -9 0.30 2.00 1 4 9 1.80 1.80 -1 4 -9 2.90 2.10 -2 -4 -9 1.50 1.40 2 -4 9 3.30 3.50 2 -4 9 2.30 1.50 2 -4 9 1.50 3.60 2 -4 9 0.40 1.90 -2 4 -9 2.80 1.70 -2 4 -9 1.50 2.00 -2 4 -9 2.30 1.40 -2 4 -9 2.50 2.20 2 4 9 1.30 1.80 3 -4 9 -1.50 3.70 -3 -4 -9 0.80 1.40 3 -4 9 1.40 4.40 3 -4 9 2.10 2.10 3 -4 9 -0.20 1.40 -3 4 -9 -0.40 1.80 -3 4 -9 -0.80 1.80 4 -4 9 6.50 4.30 4 -4 9 0.90 2.80 -4 -4 -9 -0.10 1.40 4 -4 9 0.60 1.70 -4 4 -9 0.90 1.80 -4 4 -9 1.80 1.80 -4 4 -9 2.10 1.90 5 -4 9 143.89 11.60 -5 -4 -9 137.79 7.80 5 -4 9 130.09 8.00 5 -4 9 116.79 9.50 5 4 9 126.19 9.60 -5 4 -9 121.69 8.10 -5 4 -9 129.69 8.00 -6 -4 -9 35.50 3.60 6 -4 9 39.80 6.50 6 -4 9 31.50 4.80 6 -4 9 28.10 4.50 6 4 9 36.00 5.40 -6 4 -9 34.00 4.20 -6 4 -9 36.20 6.40 -7 -4 -9 7.10 2.00 7 -4 9 5.90 2.80 7 -4 9 19.60 5.80 7 -4 9 6.50 3.30 -7 -4 -9 15.90 4.50 -7 4 -9 10.90 2.40 -7 4 -9 7.50 2.20 7 4 9 8.50 2.70 -8 -4 -9 96.89 6.50 8 -4 9 86.09 8.50 8 -4 9 87.39 7.60 8 -4 9 111.39 11.70 -8 -4 -9 106.79 7.80 8 4 9 105.49 7.50 -8 4 -9 107.09 7.10 -8 4 -9 109.49 7.00 9 -4 9 2.10 6.20 9 -4 9 -0.90 3.30 9 -4 9 -2.10 2.80 -9 -4 -9 0.20 1.70 -9 -4 -9 0.00 2.40 -9 4 -9 2.90 2.40 9 4 9 2.20 2.50 -9 4 -9 0.70 2.40 10 -4 9 161.68 11.00 -10 -4 -9 175.38 10.00 -10 -4 -9 179.08 10.80 10 -4 9 149.29 11.90 -10 4 -9 180.38 10.70 10 4 9 189.88 11.20 10 4 9 194.38 11.00 11 -4 9 0.30 2.80 -11 -4 -9 1.60 2.20 11 -4 9 2.00 3.40 -11 4 -9 6.30 2.60 11 4 9 5.10 2.50 11 4 9 5.70 2.90 12 -4 9 -1.80 3.20 12 -4 9 -1.80 2.60 -12 -4 -9 0.30 2.00 12 4 9 1.70 2.50 -12 4 -9 0.90 2.50 12 4 9 1.70 2.20 -13 -4 -9 1.10 2.00 13 -4 9 -1.60 2.20 13 -4 9 -0.80 2.80 -13 -4 -9 2.60 2.00 13 4 9 0.70 2.40 -13 4 -9 4.40 2.00 13 4 9 2.80 2.40 -14 -4 -9 23.00 3.30 14 -4 9 13.60 3.00 -14 -4 -9 17.70 3.10 14 -4 9 17.70 2.60 14 4 9 21.60 3.00 14 4 9 26.60 4.30 -14 4 -9 18.90 2.90 15 -4 9 8.40 2.00 -15 -4 -9 7.30 1.80 15 4 9 12.10 2.60 -15 4 -9 10.40 1.50 15 4 9 9.70 3.10 15 5 -9 55.29 4.70 15 5 -9 67.99 5.10 -14 -5 9 203.08 12.20 14 5 -9 201.88 12.60 14 5 -9 245.98 12.20 -13 -5 9 181.38 11.00 13 5 -9 211.38 10.70 13 5 -9 160.38 11.20 12 5 -9 221.18 12.60 -11 -5 9 4.00 2.70 11 5 -9 11.10 2.40 11 5 -9 5.20 2.70 10 5 -9 34.10 5.80 10 5 -9 39.90 4.40 -9 -5 9 794.12 43.60 9 5 -9 835.72 43.80 9 5 -9 834.32 42.90 -8 -5 9 5.50 2.70 8 5 -9 21.80 3.50 8 5 -9 12.00 2.80 -7 -5 9 362.46 20.50 7 5 -9 391.76 20.60 7 5 -9 350.06 19.60 -6 -5 9 182.78 11.90 6 5 -9 211.08 12.00 -5 -5 9 17.30 3.10 -5 -5 9 16.90 2.50 5 5 -9 24.60 4.00 5 5 -9 12.10 5.40 5 5 -9 15.20 2.10 -4 -5 9 522.75 27.80 -4 -5 9 519.85 27.90 4 5 -9 528.55 28.80 4 5 -9 517.75 27.60 4 5 -9 508.25 27.20 -3 -5 9 35.70 4.50 -3 -5 9 40.40 4.00 3 5 -9 37.90 3.90 3 5 -9 30.20 3.10 3 5 -9 35.10 6.30 -2 -5 9 82.09 6.20 -2 -5 9 79.19 6.10 -2 -5 9 88.59 6.00 2 5 -9 83.89 7.10 2 5 -9 88.49 5.30 2 5 -9 84.59 5.90 -1 -5 9 149.39 8.90 -1 -5 9 155.48 9.40 1 -5 -9 144.29 8.70 -1 -5 9 136.59 8.90 1 5 -9 147.89 8.80 1 5 -9 152.78 9.40 1 5 -9 158.88 8.40 0 -5 9 102.39 6.50 0 -5 9 104.69 7.40 0 -5 9 103.29 6.80 0 -5 -9 101.99 7.00 0 5 -9 101.99 6.80 0 5 -9 99.99 7.10 0 5 -9 108.59 7.60 0 5 -9 113.49 6.30 0 5 9 111.69 6.80 1 -5 9 35.50 3.80 -1 -5 -9 36.60 3.40 1 -5 9 36.80 5.10 1 -5 9 33.70 3.20 1 5 9 37.00 3.90 -1 5 -9 36.00 4.00 -1 5 -9 37.90 4.30 -1 5 -9 32.70 3.20 2 -5 9 258.67 14.70 2 -5 9 266.47 15.30 -2 -5 -9 274.07 14.20 2 -5 9 258.77 14.10 -2 5 -9 260.47 14.00 -2 5 -9 247.78 14.40 -2 5 -9 262.57 14.40 3 -5 9 8.10 3.60 3 -5 9 4.60 1.60 -3 -5 -9 1.40 1.50 3 -5 9 4.50 2.20 -3 5 -9 2.50 1.90 -3 5 -9 3.50 2.00 4 -5 9 45.70 4.20 -4 -5 -9 50.29 4.10 4 -5 9 57.79 7.30 -4 5 -9 51.39 4.60 5 -5 9 -0.70 1.90 -5 -5 -9 -1.50 1.60 5 -5 9 3.20 2.70 5 -5 9 4.60 4.50 -5 5 -9 2.00 2.00 -5 5 -9 1.90 2.00 6 -5 9 41.00 6.30 6 -5 9 56.29 8.90 -6 -5 -9 32.20 3.80 6 -5 9 38.10 4.60 -6 5 -9 34.10 4.30 -6 5 -9 39.30 4.40 7 -5 9 211.18 12.60 7 -5 9 232.98 15.50 -7 -5 -9 219.88 12.10 7 -5 9 197.98 13.70 -7 5 -9 217.88 12.40 -7 5 -9 215.98 12.30 7 5 9 214.18 13.20 8 -5 9 4.20 3.50 8 -5 9 3.10 2.70 -8 -5 -9 7.00 2.10 -8 -5 -9 8.50 3.20 8 5 9 7.00 2.90 -8 5 -9 4.00 2.40 -8 5 -9 6.20 2.60 -9 -5 -9 52.79 6.00 -9 5 -9 47.50 5.20 9 5 9 49.50 5.70 -10 -5 -9 4.00 1.90 -10 -5 -9 3.90 2.50 10 -5 9 -1.10 2.60 10 -5 9 -4.20 3.30 10 5 9 3.60 2.60 -10 5 -9 1.10 2.30 -11 -5 -9 6.50 2.60 11 -5 9 4.20 2.60 11 -5 9 -0.10 3.20 -11 5 -9 5.90 2.40 11 5 9 7.00 2.80 11 5 9 3.10 2.80 12 -5 9 33.10 5.30 -12 -5 -9 44.90 4.60 12 -5 9 43.50 4.70 12 5 9 47.60 5.10 12 5 9 49.99 5.20 -12 5 -9 48.30 4.30 -13 -5 -9 45.80 4.40 13 -5 9 51.19 4.50 13 -5 9 43.10 5.10 -13 5 -9 52.79 4.10 13 5 9 56.09 5.70 13 5 9 53.89 5.10 -14 -5 -9 3.80 1.90 -14 -5 -9 4.80 1.70 14 -5 9 3.60 1.90 14 -5 9 4.10 2.00 14 5 9 3.30 2.30 14 5 9 3.10 4.00 -14 5 -9 5.30 1.40 -15 -5 -9 3.50 1.70 15 -5 9 5.00 1.30 15 5 9 0.30 2.30 -15 -6 9 20.70 2.70 15 6 -9 25.80 3.00 14 6 -9 36.10 4.50 14 6 -9 32.10 3.80 -13 -6 9 40.60 4.60 13 6 -9 57.39 5.20 13 6 -9 52.79 4.50 -12 -6 9 334.07 19.80 12 6 -9 365.26 19.30 12 6 -9 379.66 20.20 -11 -6 9 4.70 2.90 11 6 -9 10.20 3.00 11 6 -9 6.90 2.10 10 6 -9 35.00 4.10 10 6 -9 44.10 5.80 -9 -6 9 10.00 3.20 9 6 -9 12.40 2.30 9 6 -9 16.70 3.40 -8 -6 9 373.56 21.10 8 6 -9 419.16 21.20 8 6 -9 328.87 22.70 8 6 -9 375.16 20.10 -7 -6 9 753.22 40.40 7 6 -9 735.33 39.50 7 6 -9 727.73 41.40 7 6 -9 815.12 40.30 -6 -6 9 60.89 6.10 6 6 -9 79.69 6.10 6 6 -9 58.19 4.80 6 6 -9 71.59 8.70 -5 -6 9 34.70 3.70 -5 -6 9 26.60 4.60 5 6 -9 34.20 4.50 5 6 -9 25.60 4.40 5 6 -9 30.50 3.30 -4 -6 9 30.00 3.70 -4 -6 9 26.40 4.60 4 6 -9 24.50 3.10 4 6 -9 35.20 4.20 -3 -6 9 41.60 4.40 -3 -6 9 34.00 5.00 3 6 -9 41.40 4.30 3 6 -9 47.30 5.70 -2 -6 9 166.58 9.60 -2 -6 9 155.58 10.20 2 6 -9 173.38 10.50 -1 -6 9 179.98 11.00 -1 -6 9 193.28 10.50 1 -6 -9 186.88 10.40 -1 -6 9 177.08 10.90 1 6 -9 172.78 10.80 1 6 -9 192.28 11.10 1 6 -9 187.58 10.20 0 -6 9 141.59 10.10 0 -6 9 169.98 10.20 0 -6 9 169.78 9.30 0 -6 -9 166.68 9.30 0 6 -9 161.38 9.90 0 6 -9 161.38 9.50 0 6 9 165.68 9.60 -1 -6 -9 702.43 36.20 1 -6 9 705.03 36.10 1 -6 9 712.73 36.80 1 6 9 728.63 36.30 -1 6 -9 641.64 36.40 -1 6 -9 670.63 36.30 2 -6 9 332.07 17.60 2 -6 9 331.17 18.70 2 -6 9 326.17 18.10 -2 -6 -9 333.37 17.70 -2 6 -9 326.77 18.10 3 -6 9 149.79 8.80 -3 -6 -9 151.08 8.90 3 -6 9 157.38 9.50 3 -6 9 155.88 10.30 -3 6 -9 149.49 9.10 -3 6 -9 147.59 9.20 -4 -6 -9 28.70 3.50 4 -6 9 32.30 3.60 4 -6 9 32.40 4.60 -4 6 -9 26.80 4.00 -4 6 -9 30.70 4.00 5 -6 9 677.43 34.90 5 -6 9 644.84 34.30 5 -6 9 649.93 33.70 -5 -6 -9 624.54 33.70 -5 6 -9 635.94 33.60 -5 6 -9 616.84 33.80 6 -6 9 426.66 23.60 6 -6 9 452.35 24.30 -6 -6 -9 419.96 22.70 6 -6 9 417.86 22.80 -6 6 -9 422.86 22.90 -6 6 -9 411.46 22.70 7 -6 9 31.70 5.60 -7 -6 -9 26.80 3.60 7 -6 9 28.50 4.20 -7 6 -9 31.40 4.50 8 -6 9 0.00 3.00 -8 6 -9 3.80 2.40 -9 -6 -9 224.28 12.20 9 -6 9 213.88 12.50 9 -6 9 204.38 13.40 -9 -6 -9 219.88 13.30 9 6 9 203.08 15.40 -9 6 -9 236.98 12.60 -10 -6 -9 175.08 9.70 10 -6 9 160.88 11.00 10 -6 9 168.78 10.10 -10 -6 -9 172.98 10.60 -10 6 -9 180.18 10.10 10 6 9 151.48 11.10 11 -6 9 111.39 7.50 -11 -6 -9 114.99 8.00 11 -6 9 112.69 8.00 11 6 9 117.89 8.10 -11 6 -9 122.59 7.30 -12 -6 -9 44.20 4.60 12 -6 9 42.30 4.10 12 -6 9 41.90 4.80 12 6 9 50.39 5.00 -12 6 -9 47.20 4.00 13 -6 9 43.80 3.80 -13 -6 -9 43.50 4.30 13 -6 9 40.80 4.10 -13 6 -9 45.00 3.50 13 6 9 46.70 4.70 14 -6 9 14.60 2.30 -14 -6 -9 22.70 3.30 14 -6 9 21.50 2.40 14 6 9 23.50 3.50 -14 6 -9 19.90 2.10 14 7 -9 16.00 2.70 -13 -7 9 164.08 10.30 13 7 -9 190.68 10.50 12 7 -9 31.70 4.20 12 7 -9 45.00 4.80 -11 -7 9 13.80 2.90 11 7 -9 22.90 3.50 -10 -7 9 11.80 3.30 10 7 -9 12.90 2.20 -9 -7 9 135.29 9.50 9 7 -9 126.99 11.50 9 7 -9 137.89 8.10 -8 -7 9 141.69 10.20 8 7 -9 142.49 9.00 8 7 -9 159.98 12.10 8 7 -9 181.98 10.50 -7 -7 9 14.60 3.30 7 7 -9 16.10 4.40 7 7 -9 12.10 2.10 -6 -7 9 169.38 11.20 6 7 -9 184.88 11.10 6 7 -9 194.68 12.20 6 7 -9 168.88 10.10 -5 -7 9 17.30 3.10 -5 -7 9 18.50 3.60 5 7 -9 23.80 4.30 5 7 -9 15.30 2.30 5 7 -9 19.00 3.80 -4 -7 9 6.60 2.70 -4 -7 9 8.30 2.00 4 7 -9 7.70 2.40 4 7 -9 12.90 3.50 4 7 -9 6.20 1.80 -3 -7 9 39.50 4.90 -3 -7 9 46.60 4.50 -3 -7 9 49.99 5.30 3 7 -9 46.90 4.00 3 7 -9 54.49 5.90 3 7 -9 52.39 4.80 -2 -7 9 104.09 7.60 -2 -7 9 106.49 7.10 -2 -7 9 107.39 6.90 2 7 -9 106.79 7.10 2 7 -9 104.89 6.60 2 7 -9 111.79 7.70 1 -7 -9 89.39 6.30 -1 -7 9 100.49 6.30 -1 -7 9 101.39 7.40 -1 -7 9 102.79 6.80 1 7 -9 101.29 6.60 1 7 -9 99.89 7.20 0 -7 9 327.97 18.00 0 -7 -9 329.07 17.70 0 -7 9 324.27 17.60 0 -7 9 335.77 18.40 0 7 -9 331.67 18.10 0 7 -9 318.87 17.80 1 -7 9 367.86 20.30 1 -7 9 372.56 20.00 1 -7 9 366.26 19.50 -1 -7 -9 349.47 19.60 1 7 9 381.96 19.80 -1 7 -9 360.56 19.70 -1 7 -9 364.26 20.00 2 -7 9 374.76 20.00 2 -7 9 365.16 19.50 -2 -7 -9 356.16 19.50 2 -7 9 375.06 20.40 -2 7 -9 352.76 19.60 -2 7 -9 362.26 19.80 -3 -7 -9 105.79 7.00 3 -7 9 118.69 7.70 3 -7 9 110.29 6.90 3 -7 9 101.19 8.40 -3 7 -9 114.39 7.40 -3 7 -9 108.89 7.20 4 -7 9 556.54 29.40 -4 -7 -9 531.45 28.90 4 -7 9 556.44 28.80 4 -7 9 553.44 29.90 -4 7 -9 532.05 28.90 -4 7 -9 553.64 29.10 -5 -7 -9 7.80 2.10 5 -7 9 14.00 3.00 5 -7 9 14.80 2.40 -5 7 -9 11.50 2.60 -5 7 -9 11.80 2.80 6 -7 9 411.06 21.70 6 -7 9 385.36 21.10 -6 -7 -9 376.66 21.10 -6 7 -9 398.26 21.30 7 -7 9 86.49 6.30 7 -7 9 88.59 7.00 -7 -7 -9 79.39 6.00 -7 7 -9 94.79 6.50 8 -7 9 26.00 4.80 8 -7 9 30.40 4.10 -8 -7 -9 25.90 3.80 -8 7 -9 32.50 4.30 -9 -7 -9 2.90 2.10 9 -7 9 4.60 2.20 9 -7 9 0.10 2.40 -9 7 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3 8 -9 52.19 5.10 3 8 -9 55.39 5.90 -2 -8 9 105.79 6.90 -2 -8 9 104.49 7.80 -2 -8 9 114.29 7.40 2 8 -9 104.09 7.20 2 8 -9 104.19 7.80 1 -8 -9 390.36 20.90 -1 -8 9 379.26 20.80 -1 -8 9 384.16 21.60 -1 -8 9 397.76 21.30 1 8 -9 395.86 21.40 1 8 -9 392.56 21.10 0 -8 9 13.80 3.10 0 -8 9 11.50 2.10 0 -8 9 10.50 2.30 0 -8 -9 10.90 2.20 0 8 -9 10.70 2.30 0 8 -9 11.70 2.60 1 -8 9 33.90 3.60 1 -8 9 31.50 4.30 -1 -8 -9 29.60 3.70 1 -8 9 43.50 5.60 -1 8 -9 28.20 3.90 -1 8 -9 32.70 4.50 1 8 9 30.80 4.20 -2 -8 -9 7.20 2.10 2 -8 9 9.90 2.40 2 -8 9 6.70 3.30 2 -8 9 5.90 1.90 -2 8 -9 5.80 2.30 -2 8 -9 6.10 2.10 -3 -8 -9 171.38 9.80 3 -8 9 162.18 11.10 3 -8 9 173.58 10.40 3 -8 9 164.48 9.60 -3 8 -9 160.38 10.10 -3 8 -9 156.68 9.80 4 -8 9 31.00 4.70 -4 -8 -9 24.50 3.60 4 -8 9 26.10 3.60 -4 8 -9 26.40 4.40 5 -8 9 209.58 11.40 5 -8 9 170.08 11.40 -5 -8 -9 155.08 10.90 -5 8 -9 196.58 10.90 -6 -8 -9 10.60 2.30 6 -8 9 14.40 2.90 6 -8 9 10.30 2.20 -6 8 -9 13.60 2.70 -7 -8 -9 0.60 2.00 7 -8 9 1.20 1.90 7 -8 9 3.30 2.30 -7 8 -9 5.30 2.40 8 -8 9 9.60 2.70 -8 -8 -9 11.40 2.40 8 -8 9 9.50 2.10 -8 8 -9 10.30 2.50 9 -8 9 2.40 1.90 -9 -8 -9 1.10 2.10 9 -8 9 0.60 1.80 -9 8 -9 3.70 2.00 10 -8 9 24.20 3.20 -10 -8 -9 30.00 4.10 10 -8 9 23.90 3.50 -10 8 -9 27.60 3.40 10 8 9 24.70 3.50 11 -8 9 2.80 1.50 11 -8 9 4.30 1.70 11 8 9 4.00 2.30 -11 8 -9 3.50 1.60 12 -8 9 67.29 4.60 12 -8 9 70.59 4.50 12 8 9 69.09 5.30 -12 -9 9 -0.10 1.60 12 9 -9 3.30 1.50 -11 -9 9 15.40 2.50 11 9 -9 21.70 3.10 -10 -9 9 5.90 2.30 10 9 -9 9.40 2.30 -9 -9 9 39.90 4.90 9 9 -9 47.90 4.60 -8 -9 9 44.30 5.00 8 9 -9 45.70 5.90 8 9 -9 53.09 4.90 -7 -9 9 20.00 3.60 7 9 -9 28.70 4.90 -6 -9 9 13.30 2.90 6 9 -9 26.50 4.40 6 9 -9 18.30 3.50 -5 -9 9 13.60 2.30 -5 -9 9 20.70 3.60 5 9 -9 22.30 3.90 5 9 -9 16.70 2.80 -4 -9 9 84.69 6.20 -4 -9 9 85.09 6.90 4 9 -9 88.69 7.40 4 9 -9 88.79 6.50 -3 -9 9 11.70 2.70 -3 -9 9 17.80 3.40 -3 -9 9 13.70 2.50 3 9 -9 11.00 2.60 3 9 -9 18.80 3.50 2 -9 -9 72.39 6.80 -2 -9 9 87.79 6.50 -2 -9 9 84.19 7.10 2 9 -9 84.19 6.90 2 9 -9 87.69 6.20 -1 -9 9 9.70 3.30 -1 -9 9 8.50 2.40 1 9 -9 11.20 2.50 1 9 -9 8.10 2.60 0 -9 9 -0.40 3.20 0 -9 9 4.80 2.20 0 9 -9 0.80 2.10 0 9 -9 3.00 2.50 1 -9 9 74.99 5.90 1 -9 9 65.89 7.40 -1 9 -9 72.29 6.10 -1 9 -9 63.69 5.50 2 -9 9 415.56 22.60 2 -9 9 433.36 23.80 2 -9 9 461.25 23.20 -2 -9 -9 415.06 22.80 -2 9 -9 418.96 23.00 -2 9 -9 407.66 22.70 3 -9 9 5.40 2.40 -3 -9 -9 3.60 2.00 3 -9 9 4.10 1.90 3 9 9 6.10 2.30 -3 9 -9 3.20 2.40 4 -9 9 455.45 24.40 4 -9 9 487.05 25.00 -4 -9 -9 437.46 24.60 -4 9 -9 462.95 24.70 5 -9 9 83.69 5.80 5 -9 9 90.29 6.50 -5 -9 -9 78.29 6.00 -5 9 -9 83.09 6.30 -6 -9 -9 92.69 6.50 6 -9 9 92.39 6.90 6 -9 9 95.09 6.20 -6 9 -9 93.59 6.60 -7 -9 -9 62.69 5.40 7 -9 9 74.59 5.60 7 -9 9 68.39 5.00 -7 9 -9 76.39 5.50 -8 -9 -9 0.90 2.00 8 -9 9 1.10 1.70 8 -9 9 2.30 1.80 -8 9 -9 0.60 1.80 -9 -9 -9 67.79 5.20 9 -9 9 64.99 4.60 9 -9 9 67.19 4.90 9 9 9 61.59 5.80 -9 9 -9 71.29 4.80 10 -9 9 5.90 1.70 10 -9 9 6.20 1.60 10 9 9 3.10 2.30 -10 9 -9 5.40 1.50 11 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4.30 2.10 2 -10 9 4.20 1.90 -2 10 -9 3.00 2.40 -3 -10 -9 40.00 4.40 3 -10 9 50.59 4.80 3 -10 9 39.00 3.90 -3 10 -9 42.10 4.60 -4 -10 -9 -2.70 2.00 4 -10 9 -0.20 1.80 4 10 9 0.20 1.70 -4 10 -9 3.40 3.40 5 -10 9 66.99 5.10 5 -10 9 63.49 4.80 -5 -10 -9 63.59 5.30 -5 10 -9 62.99 5.20 6 -10 9 12.10 2.10 -6 -10 -9 8.40 2.30 6 -10 9 6.30 1.90 6 10 9 2.70 2.20 -6 10 -9 8.10 2.10 7 -10 9 424.46 22.50 -7 -10 -9 437.36 22.90 7 -10 9 457.95 22.90 7 10 9 394.46 23.00 -7 10 -9 424.16 22.60 -8 -10 -9 3.00 2.00 8 -10 9 3.00 1.50 8 -10 9 1.10 1.40 8 10 9 -2.40 2.00 -8 10 -9 1.30 1.60 -9 -10 -9 143.99 8.80 9 -10 9 151.28 8.30 9 -10 9 140.29 8.10 -9 10 -9 143.39 8.00 10 -10 9 94.99 5.90 10 -10 9 105.09 6.10 -9 -11 9 43.80 4.10 9 11 -9 58.69 4.50 -8 -11 9 1.10 1.90 8 11 -9 4.20 3.20 -7 -11 9 81.99 5.90 7 11 -9 81.39 5.50 7 11 -9 71.79 5.80 -6 -11 9 19.00 2.90 6 11 -9 20.00 3.60 6 11 -9 21.60 3.90 -5 -11 9 304.77 16.60 5 11 -9 299.57 16.50 5 11 -9 286.27 16.00 -4 -11 9 97.09 7.20 4 11 -9 95.79 6.40 4 11 -9 98.39 7.10 -3 -11 9 218.08 12.50 -3 -11 9 189.08 11.50 3 -11 -9 206.28 12.30 3 11 -9 200.58 11.90 -2 -11 9 89.39 7.20 2 -11 -9 87.39 6.60 -2 -11 9 75.69 5.60 2 11 -9 76.79 6.30 -1 -11 9 59.69 5.10 -1 -11 9 60.19 4.70 -1 -11 9 57.89 6.90 1 -11 -9 56.59 5.30 1 11 -9 52.79 5.20 0 -11 9 238.38 13.30 0 -11 -9 253.27 13.70 0 -11 9 232.58 13.60 0 11 -9 234.08 13.70 -1 -11 -9 2.20 2.20 1 -11 9 6.40 2.00 1 -11 9 4.60 2.00 -1 11 -9 5.20 2.20 -2 -11 -9 397.16 20.90 2 -11 9 370.66 20.40 2 -11 9 401.16 20.90 -2 11 -9 366.96 20.70 -3 -11 -9 5.60 2.30 3 -11 9 6.20 2.00 3 -11 9 4.50 1.90 -3 11 -9 7.20 2.30 -4 -11 -9 321.37 18.10 4 -11 9 331.37 17.70 4 -11 9 346.07 18.10 -4 11 -9 325.97 17.90 5 -11 9 1.20 1.60 -5 -11 -9 0.70 2.00 5 -11 9 3.00 1.70 -5 11 -9 1.00 1.80 6 -11 9 155.38 8.70 -6 -11 -9 155.98 9.10 6 -11 9 171.38 9.00 -6 11 -9 153.38 8.80 6 11 9 132.99 8.60 -7 -11 -9 53.59 4.60 7 -11 9 53.59 4.00 7 -11 9 55.09 4.00 7 11 9 57.59 4.20 -7 11 -9 55.09 3.90 8 -11 9 132.89 7.60 8 -11 9 143.59 7.60 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7 -10 57.69 4.80 6 7 -10 70.69 6.00 -5 -7 10 13.10 2.90 -5 -7 10 10.30 2.10 5 7 -10 11.20 2.10 -4 -7 10 297.37 16.90 -4 -7 10 300.47 17.30 4 7 -10 308.27 17.00 4 7 -10 309.57 17.60 4 7 -10 304.57 16.30 -3 -7 10 7.70 2.10 -3 -7 10 10.20 2.90 3 7 -10 9.10 2.00 3 7 -10 6.10 2.20 3 7 -10 14.00 3.40 -2 -7 10 238.38 13.90 -2 -7 10 234.38 13.60 2 7 -10 240.08 13.90 2 7 -10 237.38 13.50 2 7 -10 241.38 13.10 1 -7 -10 4.00 2.10 -1 -7 10 5.20 1.90 -1 -7 10 5.30 2.20 -1 -7 10 5.40 2.60 1 7 -10 5.80 2.20 1 7 -10 5.00 2.40 0 -7 10 7.30 2.10 0 -7 10 8.30 2.20 0 -7 10 6.30 2.40 0 -7 -10 10.20 2.10 0 7 -10 8.30 2.20 0 7 -10 7.30 2.30 1 -7 10 103.09 6.30 -1 -7 -10 101.49 6.40 1 -7 10 94.29 7.40 1 -7 10 100.69 6.90 -1 7 -10 96.79 7.10 1 7 10 98.79 6.80 -1 7 -10 95.29 6.80 2 -7 10 75.79 6.10 2 -7 10 72.99 5.30 2 -7 10 78.69 6.70 -2 -7 -10 72.19 5.40 2 7 10 80.29 5.70 -2 7 -10 74.39 6.00 -2 7 -10 72.19 5.70 3 -7 10 4.80 3.40 3 -7 10 3.30 2.30 3 -7 10 2.40 1.80 -3 -7 -10 0.80 1.80 -3 7 -10 1.70 2.50 -3 7 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8 3 14 9.50 3.20 9 -3 14 211.38 12.20 -9 -3 -14 225.38 12.40 -9 -3 -14 198.48 12.70 9 -3 14 206.18 13.00 -9 3 -14 217.28 11.90 -9 3 -14 213.68 12.20 9 3 14 224.88 13.00 10 -3 14 39.00 5.10 10 -3 14 40.20 4.00 -10 -3 -14 37.20 4.20 -10 -3 -14 34.60 4.90 10 3 14 42.80 5.20 -10 3 -14 39.70 4.10 -10 3 -14 33.00 3.50 -11 -3 -14 19.00 3.40 -11 -3 -14 17.10 3.00 11 -3 14 16.00 2.80 11 -3 14 14.00 2.90 -11 3 -14 17.60 3.10 11 3 14 19.80 3.30 12 -3 14 54.19 3.70 -12 -3 -14 46.10 4.40 12 -3 14 42.50 4.90 -12 3 -14 59.99 3.90 12 3 14 51.89 5.10 13 4 -14 27.30 3.40 13 4 -14 19.40 3.60 12 4 -14 8.10 1.90 12 4 -14 9.50 2.20 -11 -4 14 22.60 3.30 11 4 -14 30.70 3.20 -10 -4 14 21.30 3.70 10 4 -14 29.90 3.50 10 4 -14 37.50 4.20 -9 -4 14 103.99 7.30 9 4 -14 120.49 7.60 9 4 -14 109.39 7.00 -8 -4 14 88.39 7.60 8 4 -14 93.39 6.20 -7 -4 14 147.99 9.30 7 4 -14 134.39 8.60 7 4 -14 156.58 9.30 -6 -4 14 10.20 2.80 6 -4 -14 11.60 2.70 6 4 -14 8.90 2.50 6 4 -14 8.50 2.10 5 -4 -14 125.49 8.00 -5 -4 14 139.99 8.80 5 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6.00 11 4 14 97.19 6.90 -11 4 -14 104.49 6.10 12 -4 14 32.10 2.60 -12 -4 -14 30.10 2.70 -12 4 -14 32.50 4.40 12 5 -14 18.60 2.90 12 5 -14 13.30 2.10 -11 -5 14 8.00 1.90 11 5 -14 8.20 1.90 11 5 -14 10.90 2.20 -10 -5 14 184.98 10.90 10 5 -14 185.78 10.60 10 5 -14 205.08 11.20 -9 -5 14 19.70 3.00 9 5 -14 32.80 4.10 9 5 -14 25.30 3.30 -8 -5 14 122.89 8.20 8 5 -14 135.99 8.30 8 5 -14 125.59 7.70 -7 -5 14 16.90 2.90 7 5 -14 16.30 3.30 7 5 -14 19.60 3.30 -6 -5 14 275.97 15.60 6 5 -14 271.27 15.40 5 -5 -14 7.70 2.40 -5 -5 14 1.60 2.40 5 5 -14 1.30 1.80 5 5 -14 -0.30 2.20 -4 -5 14 651.53 35.50 4 -5 -14 684.03 35.10 4 5 -14 674.23 35.40 4 5 -14 673.23 35.00 -3 -5 14 2.80 2.40 3 -5 -14 1.60 1.90 3 5 -14 3.30 2.40 3 5 -14 2.60 1.80 -2 -5 14 25.80 4.60 -2 -5 14 30.30 4.00 2 -5 -14 21.80 3.40 2 5 -14 26.20 4.20 2 5 -14 22.60 4.20 2 5 -14 20.20 3.30 -1 -5 14 5.00 2.00 -1 -5 14 3.30 2.30 1 -5 -14 1.60 1.80 1 5 -14 6.00 3.40 1 5 -14 3.60 2.50 1 5 -14 1.90 1.80 0 -5 14 292.47 15.70 0 -5 14 297.37 16.20 0 -5 -14 282.77 15.50 0 -5 -14 274.27 16.10 0 5 -14 257.87 16.10 0 5 -14 290.17 15.90 0 5 -14 282.47 15.30 -1 -5 -14 183.08 11.40 -1 -5 -14 181.88 10.80 1 -5 14 204.58 11.70 1 -5 14 193.98 11.00 1 5 14 179.68 12.00 -1 5 -14 183.28 10.50 -1 5 -14 192.58 11.30 -1 5 -14 187.18 11.50 2 -5 14 148.29 8.90 -2 -5 -14 143.89 8.80 2 -5 14 157.38 9.80 -2 5 -14 150.48 9.20 2 5 14 134.19 10.30 -2 5 -14 138.29 9.30 -3 -5 -14 163.08 9.90 3 -5 14 156.68 10.80 3 -5 14 171.98 10.20 -3 5 -14 171.38 10.50 3 5 14 177.68 11.10 -3 5 -14 173.78 10.20 4 -5 14 14.40 3.20 -4 -5 -14 4.50 2.10 4 -5 14 11.10 2.40 4 5 14 10.40 3.00 -4 5 -14 7.70 2.30 -4 5 -14 9.90 2.80 5 -5 14 202.28 12.50 5 -5 14 212.88 12.10 -5 -5 -14 194.78 11.70 -5 5 -14 213.78 11.90 -5 5 -14 206.18 12.20 5 5 14 219.88 12.50 -6 -5 -14 9.30 2.20 6 -5 14 7.80 2.90 -6 5 -14 8.40 2.60 -6 5 -14 11.60 2.20 -7 -5 -14 33.40 3.90 7 -5 14 44.40 4.20 7 -5 14 38.60 5.00 7 5 14 44.40 5.10 -7 5 -14 40.40 3.80 -7 5 -14 40.20 4.30 8 -5 14 152.28 9.80 8 -5 14 167.28 9.60 -8 -5 -14 163.98 9.80 -8 -5 -14 158.28 9.30 8 5 14 180.48 10.30 -8 5 -14 153.68 9.20 -8 5 -14 164.88 9.60 9 -5 14 224.58 12.80 -9 -5 -14 186.08 12.20 9 -5 14 233.28 12.40 -9 -5 -14 216.38 12.50 -9 5 -14 233.98 12.40 9 5 14 242.28 13.10 -10 -5 -14 13.00 2.20 10 -5 14 19.00 3.00 10 -5 14 19.20 2.80 -10 5 -14 16.30 3.00 10 5 14 17.30 2.90 -11 -5 -14 25.00 2.90 11 -5 14 29.30 2.70 -11 5 -14 29.30 2.90 11 5 14 28.70 4.00 -11 -6 14 2.70 1.50 11 6 -14 2.20 1.90 11 6 -14 1.10 1.60 -10 -6 14 6.60 2.00 10 6 -14 9.20 1.90 10 6 -14 10.00 2.10 -9 -6 14 53.69 4.70 9 6 -14 61.69 5.00 9 6 -14 52.89 4.40 -8 -6 14 22.70 3.80 8 6 -14 30.00 3.90 8 6 -14 21.30 3.30 -7 -6 14 103.89 7.20 7 6 -14 101.89 6.60 7 6 -14 109.39 7.20 6 6 -14 0.90 1.80 -5 -6 14 207.48 12.40 5 6 -14 215.78 12.30 5 6 -14 204.38 11.60 -4 -6 14 8.10 2.60 4 -6 -14 12.50 2.50 4 6 -14 10.60 4.40 4 6 -14 9.30 2.50 4 6 -14 10.10 2.10 3 -6 -14 126.69 7.60 -3 -6 14 113.49 7.50 -3 -6 14 120.59 8.10 3 6 -14 118.59 7.20 3 6 -14 126.59 8.00 3 6 -14 109.39 8.80 -2 -6 14 1.70 1.80 -2 -6 14 1.90 2.40 2 -6 -14 2.70 1.90 2 6 -14 -2.20 2.90 2 6 -14 1.90 2.30 1 -6 -14 220.18 12.40 -1 -6 14 226.18 12.60 -1 -6 14 235.28 13.10 1 6 -14 206.08 13.20 1 6 -14 218.98 12.80 0 -6 14 26.60 3.60 0 -6 -14 21.40 3.40 0 -6 14 26.90 4.80 0 6 -14 25.00 4.30 0 6 -14 20.50 3.50 1 -6 14 198.98 11.30 1 -6 14 183.68 10.70 -1 -6 -14 171.68 11.20 -1 -6 -14 178.18 10.50 -1 6 -14 187.78 10.90 -1 6 -14 178.48 11.20 2 -6 14 6.90 2.00 2 -6 14 5.60 2.90 -2 -6 -14 2.60 1.90 -2 6 -14 5.00 2.60 -2 6 -14 4.60 2.30 2 6 14 7.70 3.40 3 -6 14 8.80 2.10 -3 -6 -14 3.30 2.10 3 -6 14 9.00 2.90 3 6 14 8.30 3.40 -3 6 -14 7.40 2.50 -3 6 -14 6.10 2.20 4 -6 14 234.28 12.90 -4 -6 -14 228.98 12.70 4 6 14 206.38 15.90 -4 6 -14 230.08 12.90 -4 6 -14 221.68 13.20 5 -6 14 56.59 4.90 -5 -6 -14 49.60 4.50 5 -6 14 48.70 5.10 -5 6 -14 47.10 5.00 5 6 14 58.39 5.60 -5 6 -14 50.99 4.40 -6 -6 -14 23.40 3.40 6 -6 14 22.80 3.50 6 -6 14 15.70 2.90 -6 6 -14 16.00 2.60 -6 6 -14 17.40 3.20 6 6 14 26.90 4.50 -7 -6 -14 29.70 3.50 7 -6 14 35.40 3.80 7 -6 14 26.40 4.20 7 6 14 39.10 4.80 -7 6 -14 31.40 4.00 -7 6 -14 25.10 3.40 -8 -6 -14 1.60 1.70 8 -6 14 3.20 1.70 8 -6 14 0.60 2.50 -8 -6 -14 0.30 1.90 -8 6 -14 1.40 1.90 8 6 14 1.60 2.50 -9 -6 -14 10.40 2.10 9 -6 14 14.40 2.70 9 -6 14 9.70 2.90 9 6 14 11.20 2.70 -9 6 -14 13.30 2.10 -10 -6 -14 51.89 4.20 10 -6 14 61.59 4.00 -10 6 -14 58.79 4.00 10 6 14 52.59 5.10 -11 -7 14 20.80 2.40 -10 -7 14 1.40 1.60 10 7 -14 5.50 1.70 -9 -7 14 35.30 3.70 9 7 -14 37.00 3.80 -8 -7 14 81.39 6.00 8 7 -14 85.89 6.10 8 7 -14 88.29 6.20 -7 -7 14 4.00 2.10 7 7 -14 4.70 2.10 7 7 -14 0.00 2.60 -6 -7 14 4.50 2.30 6 7 -14 4.90 2.20 6 7 -14 4.20 2.10 -5 -7 14 27.50 4.10 5 7 -14 20.20 4.40 5 7 -14 23.40 3.70 5 7 -14 27.00 4.10 -4 -7 14 6.70 2.40 4 7 -14 0.90 3.20 4 7 -14 2.10 2.30 4 7 -14 2.10 2.40 -3 -7 14 42.10 6.70 3 -7 -14 50.59 4.60 -3 -7 14 32.50 3.80 3 7 -14 43.60 5.40 3 7 -14 42.90 5.20 -2 -7 14 29.40 4.60 -2 -7 14 27.80 3.40 2 -7 -14 24.10 3.80 2 7 -14 21.10 3.40 2 7 -14 30.30 4.40 1 -7 -14 174.28 10.20 -1 -7 14 175.48 10.90 1 7 -14 186.68 10.60 1 7 -14 168.18 11.50 0 -7 -14 75.29 5.60 0 -7 14 78.49 6.70 0 -7 14 84.79 6.70 0 7 -14 80.39 6.00 1 -7 14 102.89 9.80 -1 -7 -14 124.59 7.40 1 -7 14 109.19 8.90 -1 7 -14 110.89 9.60 -1 7 -14 127.29 7.90 -2 -7 -14 428.26 23.00 2 -7 14 456.65 23.50 -2 7 -14 436.66 23.30 -2 7 -14 405.16 23.70 -3 -7 -14 31.00 3.70 3 -7 14 32.40 4.40 3 -7 14 40.30 3.90 -3 7 -14 36.00 4.50 3 7 14 35.30 5.20 -3 7 -14 37.10 3.80 -4 -7 -14 247.48 13.60 4 -7 14 255.67 13.70 4 -7 14 253.27 14.00 4 7 14 208.98 14.20 -4 7 -14 256.17 13.90 -4 7 -14 250.57 13.50 5 -7 14 23.50 4.20 5 -7 14 24.80 3.40 -5 -7 -14 24.60 3.40 -5 7 -14 21.00 3.20 -5 7 -14 29.20 3.90 5 7 14 30.30 3.80 6 -7 14 8.00 2.40 -6 -7 -14 2.10 1.70 6 -7 14 6.00 1.90 6 7 14 2.70 2.70 -6 7 -14 4.80 2.10 7 -7 14 117.39 8.10 7 -7 14 125.69 7.60 -7 -7 -14 124.39 7.50 -7 7 -14 132.29 7.80 7 7 14 142.19 8.50 -8 -7 -14 81.29 5.60 8 -7 14 71.79 6.40 8 -7 14 84.09 5.30 -8 -7 -14 85.09 5.40 -8 7 -14 85.19 5.50 8 7 14 87.69 6.30 -9 -7 -14 1.90 1.60 9 -7 14 4.30 1.30 9 7 14 4.70 2.50 -9 7 -14 3.40 1.50 -9 -8 14 81.49 5.30 9 8 -14 85.59 5.40 -8 -8 14 20.50 3.10 8 8 -14 20.30 3.10 -7 -8 14 58.69 4.90 7 8 -14 65.69 4.90 -6 -8 14 4.20 2.10 6 8 -14 9.10 3.50 6 8 -14 3.10 2.00 -5 -8 14 135.69 8.70 5 8 -14 137.49 8.50 5 8 -14 139.19 9.30 -4 -8 14 5.10 2.30 4 8 -14 4.60 2.00 4 8 -14 0.20 2.70 3 -8 -14 230.88 13.00 -3 -8 14 243.08 13.30 3 8 -14 217.58 13.20 3 8 -14 224.88 12.90 2 -8 -14 11.40 2.40 -2 -8 14 11.60 2.70 -2 -8 14 10.90 1.60 2 8 -14 10.80 2.40 2 8 -14 6.70 2.50 1 -8 -14 54.39 4.50 -1 -8 14 53.79 4.00 -1 -8 14 55.29 5.20 1 8 -14 48.80 5.00 1 8 -14 46.80 4.60 0 -8 14 21.90 2.80 0 -8 14 15.60 2.90 0 -8 -14 20.70 3.30 0 8 -14 16.60 2.60 0 8 -14 20.10 3.00 1 -8 14 152.98 9.20 -1 -8 -14 136.19 8.60 1 -8 14 154.58 8.70 -1 8 -14 139.69 8.60 -1 8 -14 141.99 9.00 -2 -8 -14 183.88 11.50 -2 -8 -14 184.38 10.90 2 -8 14 207.78 11.10 2 -8 14 200.18 11.60 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