data_new _audit_creation_method 'SHELXL-2016/6' _shelx_SHELXL_version_number '2016/6' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C23 H28 Br2 N4 Pd, C3 H7 N O' _chemical_formula_sum 'C26 H35 Br2 N5 O Pd' _chemical_formula_weight 699.81 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_H-M_alt 'P n m a' _space_group_name_Hall '-P 2ac 2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' _cell_length_a 16.2158(6) _cell_length_b 18.1879(7) _cell_length_c 9.2992(4) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2742.63(19) _cell_formula_units_Z 4 _cell_measurement_temperature 298(2) _cell_measurement_reflns_used 9730 _cell_measurement_theta_min 2.46 _cell_measurement_theta_max 28.245 _exptl_crystal_description block _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.695 _exptl_crystal_F_000 1400 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.230 _exptl_crystal_size_mid 0.190 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 3.619 _shelx_estimated_absorpt_T_min 0.490 _shelx_estimated_absorpt_T_max 0.714 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.549 _exptl_absorpt_correction_T_max 0.714 _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 298(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'Microfocus sealed tube' _diffrn_measurement_device_type 'Bruker AXS D8 Quest diffractometer' _diffrn_measurement_method 'omega and phi scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 76298 _diffrn_reflns_av_unetI/netI 0.0138 _diffrn_reflns_av_R_equivalents 0.0387 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_theta_min 2.512 _diffrn_reflns_theta_max 28.371 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 3528 _reflns_number_gt 2954 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Apex3 v2017.3-0 (Bruker, 2017)' _computing_cell_refinement 'SAINT V8.38A (Bruker, 2017)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2015)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0910P)^2^+3.9596P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_extinction_coef 0.0048(6) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 3528 _refine_ls_number_parameters 173 _refine_ls_number_restraints 18 _refine_ls_R_factor_all 0.0473 _refine_ls_R_factor_gt 0.0342 _refine_ls_wR_factor_ref 0.1299 _refine_ls_wR_factor_gt 0.1080 _refine_ls_goodness_of_fit_ref 0.989 _refine_ls_restrained_S_all 1.007 _refine_ls_shift/su_max 0.007 _refine_ls_shift/su_mean 0.001 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.14080(2) 0.250000 -0.18251(4) 0.02824(14) Uani 1 2 d S T P . . Br1 Br 0.19181(3) 0.34930(2) -0.34406(5) 0.05203(17) Uani 1 1 d . . . . . C1 C 0.09583(18) 0.32672(17) -0.0504(3) 0.0297(6) Uani 1 1 d . . . . . C2 C 0.0827(2) 0.41353(18) 0.1196(4) 0.0373(7) Uani 1 1 d . . . . . C3 C 0.0926(3) 0.4657(2) 0.2273(5) 0.0533(10) Uani 1 1 d . . . . . H3 H 0.144250 0.476187 0.265789 0.064 Uiso 1 1 calc R U . . . C4 C 0.0230(4) 0.5010(2) 0.2743(5) 0.0632(13) Uani 1 1 d . . . . . H4 H 0.027981 0.536115 0.346535 0.076 Uiso 1 1 calc R U . . . C5 C -0.0541(3) 0.4867(2) 0.2188(5) 0.0593(12) Uani 1 1 d . . . . . H5 H -0.099523 0.511919 0.254602 0.071 Uiso 1 1 calc R U . . . C6 C -0.0651(2) 0.4351(2) 0.1104(5) 0.0476(9) Uani 1 1 d . . . . . H6 H -0.116776 0.425500 0.071217 0.057 Uiso 1 1 calc R U . . . C7 C 0.0051(2) 0.39883(16) 0.0638(4) 0.0337(7) Uani 1 1 d . . . . . C8 C 0.2281(2) 0.3682(2) 0.0602(4) 0.0414(8) Uani 1 1 d . . . . . H8 H 0.249903 0.328704 -0.000531 0.050 Uiso 1 1 calc R U . . . C9 C 0.2621(3) 0.4406(3) 0.0031(6) 0.0614(12) Uani 1 1 d . . . . . H9A H 0.245577 0.446831 -0.095306 0.092 Uiso 1 1 calc R U . . . H9B H 0.321247 0.440055 0.008775 0.092 Uiso 1 1 calc R U . . . H9C H 0.241031 0.480521 0.059662 0.092 Uiso 1 1 calc R U . . . C10 C 0.2555(3) 0.3529(3) 0.2146(6) 0.0646(13) Uani 1 1 d . . . . . H10A H 0.244710 0.395261 0.273135 0.097 Uiso 1 1 calc R U . . . H10B H 0.313423 0.342151 0.215929 0.097 Uiso 1 1 calc R U . . . H10C H 0.225406 0.311523 0.251624 0.097 Uiso 1 1 calc R U . . . C11 C -0.0507(2) 0.3199(2) -0.1356(4) 0.0412(8) Uani 1 1 d . . . . . H11A H -0.027875 0.312200 -0.230853 0.049 Uiso 1 1 calc R U . . . H11B H -0.091408 0.358839 -0.143140 0.049 Uiso 1 1 calc R U . . . C12 C -0.0943(3) 0.250000 -0.0893(7) 0.0448(12) Uani 1 2 d S T P . . H12A H -0.149555 0.250001 -0.129056 0.054 Uiso 1 2 calc R U P . . H12B H -0.099215 0.250001 0.014667 0.054 Uiso 1 2 calc R U P . . C13 C 0.5704(6) 0.250000 0.1527(10) 0.092(3) Uani 1 2 d S T P . . H13A H 0.590667 0.299423 0.160731 0.139 Uiso 0.5 1 calc R U P . . H13B H 0.610451 0.220252 0.103704 0.139 Uiso 0.5 1 calc R U P . . H13C H 0.560753 0.230326 0.246957 0.139 Uiso 0.5 1 calc R U P . . C14 C 0.4593(6) 0.3123(6) 0.0311(8) 0.171(5) Uani 1 1 d D U . . . N1 N 0.13754(16) 0.36745(15) 0.0467(3) 0.0328(6) Uani 1 1 d . . . . . N2 N 0.01576(16) 0.34505(14) -0.0403(3) 0.0313(6) Uani 1 1 d . . . . . N3 N 0.4951(3) 0.250000 0.0732(6) 0.0595(13) Uani 1 2 d DS TU P . . O1 O 0.3946(6) 0.3013(10) -0.0417(11) 0.271(12) Uani 0.5 1 d D U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.0289(2) 0.0264(2) 0.0295(2) 0.000 0.00358(11) 0.000 Br1 0.0685(3) 0.0368(2) 0.0508(3) 0.00753(15) 0.02164(19) 0.00047(17) C1 0.0293(13) 0.0272(14) 0.0326(15) 0.0039(12) 0.0007(12) -0.0051(11) C2 0.0458(17) 0.0291(15) 0.0370(16) -0.0034(13) 0.0076(14) -0.0026(14) C3 0.070(3) 0.0382(19) 0.051(2) -0.0107(17) 0.007(2) -0.0077(19) C4 0.095(4) 0.038(2) 0.056(2) -0.0161(19) 0.026(3) -0.001(2) C5 0.072(3) 0.039(2) 0.068(3) 0.0032(19) 0.035(2) 0.013(2) C6 0.047(2) 0.0350(17) 0.061(2) 0.0058(17) 0.0188(18) 0.0040(16) C7 0.0377(15) 0.0232(13) 0.0402(17) 0.0010(12) 0.0121(13) -0.0001(12) C8 0.0313(15) 0.0421(18) 0.051(2) -0.0067(16) -0.0040(15) -0.0099(14) C9 0.048(2) 0.058(3) 0.078(3) 0.005(2) 0.002(2) -0.019(2) C10 0.050(2) 0.083(4) 0.061(3) 0.002(2) -0.016(2) -0.010(2) C11 0.0339(16) 0.0363(17) 0.053(2) 0.0013(15) -0.0133(15) 0.0040(14) C12 0.027(2) 0.036(2) 0.071(4) 0.000 -0.009(2) 0.000 C13 0.087(6) 0.121(8) 0.069(5) 0.000 -0.017(4) 0.000 C14 0.203(9) 0.233(10) 0.077(5) 0.053(6) 0.051(5) 0.167(8) N1 0.0305(12) 0.0312(13) 0.0366(14) -0.0068(11) 0.0020(10) -0.0045(10) N2 0.0288(12) 0.0262(12) 0.0389(14) -0.0007(10) -0.0004(11) 0.0005(10) N3 0.060(3) 0.072(3) 0.046(3) 0.000 0.000(2) 0.000 O1 0.147(8) 0.58(3) 0.083(7) 0.086(11) 0.037(6) 0.241(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 C1 1.997(3) 8_565 ? Pd1 C1 1.997(3) . ? Pd1 Br1 2.4906(4) . ? Pd1 Br1 2.4906(4) 8_565 ? C1 N2 1.344(4) . ? C1 N1 1.350(4) . ? C2 C7 1.387(5) . ? C2 C3 1.389(5) . ? C2 N1 1.397(4) . ? C3 C4 1.371(7) . ? C3 H3 0.9300 . ? C4 C5 1.377(8) . ? C4 H4 0.9300 . ? C5 C6 1.388(7) . ? C5 H5 0.9300 . ? C6 C7 1.385(5) . ? C6 H6 0.9300 . ? C7 N2 1.388(4) . ? C8 N1 1.475(4) . ? C8 C9 1.523(6) . ? C8 C10 1.528(6) . ? C8 H8 0.9800 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C11 N2 1.469(4) . ? C11 C12 1.517(5) . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C13 N3 1.428(10) . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C13 H13A 0.960(18) 8_565 ? C13 H13B 0.96(7) 8_565 ? C13 H13C 0.96(6) 8_565 ? C14 O1 1.264(9) . ? C14 N3 1.332(8) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Pd1 C1 88.66(17) 8_565 . ? C1 Pd1 Br1 177.48(8) 8_565 . ? C1 Pd1 Br1 89.17(8) . . ? C1 Pd1 Br1 89.17(8) 8_565 8_565 ? C1 Pd1 Br1 177.48(8) . 8_565 ? Br1 Pd1 Br1 92.97(2) . 8_565 ? N2 C1 N1 107.5(3) . . ? N2 C1 Pd1 124.7(2) . . ? N1 C1 Pd1 127.7(2) . . ? C7 C2 C3 120.4(4) . . ? C7 C2 N1 106.3(3) . . ? C3 C2 N1 133.2(4) . . ? C4 C3 C2 117.0(5) . . ? C4 C3 H3 121.5 . . ? C2 C3 H3 121.5 . . ? C3 C4 C5 122.6(4) . . ? C3 C4 H4 118.7 . . ? C5 C4 H4 118.7 . . ? C4 C5 C6 121.2(4) . . ? C4 C5 H5 119.4 . . ? C6 C5 H5 119.4 . . ? C7 C6 C5 116.3(4) . . ? C7 C6 H6 121.9 . . ? C5 C6 H6 121.9 . . ? C6 C7 C2 122.5(3) . . ? C6 C7 N2 131.1(3) . . ? C2 C7 N2 106.5(3) . . ? N1 C8 C9 109.8(3) . . ? N1 C8 C10 111.5(3) . . ? C9 C8 C10 112.4(4) . . ? N1 C8 H8 107.6 . . ? C9 C8 H8 107.6 . . ? C10 C8 H8 107.6 . . ? C8 C9 H9A 109.5 . . ? C8 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C8 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C8 C10 H10A 109.5 . . ? C8 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C8 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? N2 C11 C12 115.5(3) . . ? N2 C11 H11A 108.4 . . ? C12 C11 H11A 108.4 . . ? N2 C11 H11B 108.4 . . ? C12 C11 H11B 108.4 . . ? H11A C11 H11B 107.5 . . ? C11 C12 C11 113.9(5) . 8_565 ? C11 C12 H12A 108.8 . . ? C11 C12 H12A 108.8 8_565 . ? C11 C12 H12B 108.8 . . ? C11 C12 H12B 108.8 8_565 . ? H12A C12 H12B 107.7 . . ? N3 C13 H13A 109.5 . . ? N3 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? N3 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? N3 C13 H13A 109.5(4) . 8_565 ? H13A C13 H13A 138.9 . 8_565 ? H13B C13 H13A 43.8 . 8_565 ? H13C C13 H13A 68.6 . 8_565 ? N3 C13 H13B 109.5(16) . 8_565 ? H13A C13 H13B 43.8 . 8_565 ? H13B C13 H13B 68.6 . 8_565 ? H13C C13 H13B 138.9 . 8_565 ? H13A C13 H13B 109.5 8_565 8_565 ? N3 C13 H13C 109.5(13) . 8_565 ? H13A C13 H13C 68.6 . 8_565 ? H13B C13 H13C 138.9 . 8_565 ? H13C C13 H13C 43.8 . 8_565 ? H13A C13 H13C 109.5 8_565 8_565 ? H13B C13 H13C 109.5 8_565 8_565 ? O1 C14 N3 112.6(10) . . ? C1 N1 C2 109.5(3) . . ? C1 N1 C8 124.2(3) . . ? C2 N1 C8 126.0(3) . . ? C1 N2 C7 110.2(3) . . ? C1 N2 C11 126.1(3) . . ? C7 N2 C11 123.3(3) . . ? C14 N3 C14 116.6(11) . 8_565 ? C14 N3 C13 121.7(5) . . ? C14 N3 C13 121.7(5) 8_565 . ? _refine_diff_density_max 1.039 _refine_diff_density_min -0.978 _refine_diff_density_rms 0.111 _shelx_res_file ; TITL waseem2_0ma_c.res in Pna2(1) new.res created by SHELXL-2016/6 at 16:06:12 on 21-Jul-2020 CELL 0.71073 16.2158 18.1879 9.2992 90.000 90.000 90.000 ZERR 4 0.0006 0.0007 0.0004 0.000 0.000 0.000 LATT 1 SYMM 1/2-X,-Y,1/2+Z SYMM 1/2+X,1/2-Y,1/2-Z SYMM -X,1/2+Y,-Z SFAC C H Br N Pd O UNIT 104 140 8 20 4 4 OMIT 2 1 0 OMIT 0 1 1 OMIT 0 2 0 L.S. 2 ACTA BOND $H FMAP 2 PLAN 10 SIZE 0.10 0.19 0.23 DFIX 1.20 0.01 C14 O1 DFIX 2.22 0.01 N3 O1 FLAT C13 N3 C14 O1 DELU N3 C14 O1 SIMU N3 C14 O1 WGHT 0.091000 3.959600 EXTI 0.004767 FVAR 0.33794 MOLE 1 PD1 5 0.140797 0.250000 -0.182510 10.50000 0.02887 0.02638 = 0.02948 0.00000 0.00358 0.00000 BR1 3 0.191808 0.349302 -0.344056 11.00000 0.06853 0.03676 = 0.05079 0.00753 0.02164 0.00047 C1 1 0.095826 0.326716 -0.050441 11.00000 0.02928 0.02718 = 0.03263 0.00388 0.00074 -0.00515 C2 1 0.082676 0.413527 0.119550 11.00000 0.04577 0.02906 = 0.03702 -0.00338 0.00765 -0.00256 C3 1 0.092644 0.465700 0.227284 11.00000 0.07044 0.03824 = 0.05131 -0.01068 0.00711 -0.00768 AFIX 43 H3 2 0.144250 0.476187 0.265789 11.00000 -1.20000 AFIX 0 C4 1 0.022982 0.501037 0.274295 11.00000 0.09510 0.03819 = 0.05618 -0.01615 0.02595 -0.00117 AFIX 43 H4 2 0.027981 0.536115 0.346535 11.00000 -1.20000 AFIX 0 C5 1 -0.054078 0.486659 0.218813 11.00000 0.07175 0.03855 = 0.06768 0.00324 0.03529 0.01266 AFIX 43 H5 2 -0.099523 0.511919 0.254602 11.00000 -1.20000 AFIX 0 C6 1 -0.065126 0.435124 0.110405 11.00000 0.04716 0.03502 = 0.06064 0.00575 0.01878 0.00401 AFIX 43 H6 2 -0.116776 0.425500 0.071217 11.00000 -1.20000 AFIX 0 C7 1 0.005069 0.398833 0.063850 11.00000 0.03772 0.02320 = 0.04016 0.00104 0.01212 -0.00006 C8 1 0.228140 0.368237 0.060194 11.00000 0.03132 0.04207 = 0.05068 -0.00671 -0.00399 -0.00993 AFIX 13 H8 2 0.249903 0.328704 -0.000531 11.00000 -1.20000 AFIX 0 C9 1 0.262139 0.440595 0.003053 11.00000 0.04810 0.05797 = 0.07820 0.00507 0.00186 -0.01864 AFIX 137 H9A 2 0.245577 0.446831 -0.095306 11.00000 -1.50000 H9B 2 0.321247 0.440055 0.008775 11.00000 -1.50000 H9C 2 0.241031 0.480521 0.059662 11.00000 -1.50000 AFIX 0 C10 1 0.255459 0.352864 0.214570 11.00000 0.04959 0.08293 = 0.06134 0.00246 -0.01601 -0.01022 AFIX 137 H10A 2 0.244710 0.395261 0.273135 11.00000 -1.50000 H10B 2 0.313423 0.342151 0.215929 11.00000 -1.50000 H10C 2 0.225406 0.311523 0.251624 11.00000 -1.50000 AFIX 0 C11 1 -0.050725 0.319929 -0.135647 11.00000 0.03393 0.03635 = 0.05335 0.00134 -0.01330 0.00400 AFIX 23 H11A 2 -0.027875 0.312200 -0.230853 11.00000 -1.20000 H11B 2 -0.091408 0.358839 -0.143140 11.00000 -1.20000 AFIX 0 C12 1 -0.094256 0.250000 -0.089284 10.50000 0.02701 0.03642 = 0.07085 0.00000 -0.00944 0.00000 AFIX 23 H12A 2 -0.149555 0.250001 -0.129056 10.50000 -1.20000 H12B 2 -0.099215 0.250001 0.014667 10.50000 -1.20000 AFIX 0 C13 1 0.570406 0.250000 0.152652 10.50000 0.08741 0.12085 = 0.06909 0.00000 -0.01651 0.00000 AFIX 137 H13A 2 0.590667 0.299423 0.160731 10.50000 -1.50000 H13B 2 0.610451 0.220252 0.103704 10.50000 -1.50000 H13C 2 0.560753 0.230326 0.246957 10.50000 -1.50000 AFIX 0 C14 1 0.459286 0.312295 0.031096 11.00000 0.20268 0.23303 = 0.07701 0.05292 0.05079 0.16694 N1 4 0.137537 0.367448 0.046719 11.00000 0.03048 0.03119 = 0.03664 -0.00677 0.00197 -0.00447 N2 4 0.015758 0.345052 -0.040318 11.00000 0.02883 0.02620 = 0.03888 -0.00074 -0.00040 0.00046 N3 4 0.495065 0.250000 0.073173 10.50000 0.05998 0.07222 = 0.04636 0.00000 -0.00040 0.00000 O1 6 0.394587 0.301287 -0.041675 10.50000 0.14666 0.58282 = 0.08331 0.08557 0.03693 0.24073 HKLF 4 REM waseem2_0ma_c.res in Pna2(1) REM R1 = 0.0342 for 2954 Fo > 4sig(Fo) and 0.0473 for all 3528 data REM 173 parameters refined using 18 restraints END WGHT 0.0539 4.2919 REM Highest difference peak 1.039, deepest hole -0.978, 1-sigma level 0.111 Q1 1 0.1446 0.3524 -0.3565 11.00000 0.05 1.04 Q2 1 0.4900 0.3347 0.0492 11.00000 0.05 0.98 Q3 1 0.3727 0.2500 -0.0544 10.50000 0.05 0.83 Q4 1 0.0866 0.3499 -0.3433 11.00000 0.05 0.58 Q5 1 -0.2622 0.2500 0.0097 10.50000 0.05 0.57 Q6 1 0.6399 0.2500 -0.0031 10.50000 0.05 0.52 Q7 1 -0.1407 0.5501 0.1764 11.00000 0.05 0.50 Q8 1 0.1097 0.3945 0.0839 11.00000 0.05 0.46 Q9 1 0.1915 0.3483 -0.0139 11.00000 0.05 0.44 Q10 1 0.0435 0.4186 0.0852 11.00000 0.05 0.43 ; _shelx_res_checksum 24874 _shelx_hkl_file ; 0 0 -1 0.90 0.60 0 0 -1 0.00 0.20 0 0 2 565.04 16.20 0 0 2 531.85 15.70 0 0 -2 524.65 16.10 0 0 -2 542.85 16.20 0 0 -2 550.44 16.10 0 0 -2 548.35 16.10 0 0 2 566.84 16.10 0 0 2 552.14 16.10 0 0 -2 541.45 15.80 0 0 2 543.35 16.10 0 0 3 -2.10 2.10 0 0 3 -0.40 1.50 0 0 -3 -0.80 2.10 0 0 -3 -1.60 1.50 0 0 -3 2.10 2.00 0 0 -3 1.20 1.50 0 0 3 -1.00 1.60 0 0 -3 -1.30 2.10 0 0 3 -1.70 1.90 0 0 4 543.25 16.90 0 0 -4 559.64 17.00 0 0 -4 561.14 18.20 0 0 -4 575.84 18.00 0 0 4 577.54 17.80 0 0 4 565.44 17.80 0 0 -4 557.04 17.60 0 0 4 592.74 18.10 0 0 5 3.80 3.50 0 0 -5 -6.80 3.40 0 0 -5 -1.70 3.50 0 0 5 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79.59 2.60 -2 4 -1 80.89 3.50 -2 -4 1 76.99 4.00 -2 -4 -2 1969.70 56.39 -2 -4 -2 2005.20 56.39 2 -4 2 2011.40 56.39 -2 4 2 1937.01 55.79 2 4 -2 1983.20 56.59 2 4 -2 1911.51 55.89 -2 -4 -2 2017.90 56.49 2 4 -2 2075.19 56.69 2 -4 2 2003.60 56.39 2 4 -2 2093.29 56.59 2 4 -2 1991.80 56.69 -2 -4 -2 2069.29 56.39 -2 4 2 1958.90 55.79 2 -4 2 1997.90 56.39 -2 4 2 1938.61 55.99 -2 -4 -2 2009.00 56.59 2 -4 2 1947.11 56.19 2 -4 2 2057.69 56.59 -2 4 2 1925.11 55.89 -2 4 2 1913.71 55.79 -2 4 -2 1942.11 55.99 2 4 2 1952.90 56.39 2 -4 -2 1961.60 55.99 -2 4 -2 1937.71 56.59 2 -4 -2 1974.90 55.79 -2 -4 2 2088.99 56.59 -2 -4 2 2056.69 56.69 -2 -4 2 1955.20 56.49 -2 -4 2 1983.90 56.49 2 -4 -2 1914.31 55.89 2 4 2 2020.70 56.59 2 4 2 2050.49 56.49 -2 4 -2 2031.90 56.49 -2 4 -2 2010.50 56.49 -2 4 -2 1971.70 56.49 -2 -4 2 1988.90 55.89 2 -4 -2 1958.10 55.99 -2 4 -2 2007.70 56.29 2 4 2 2029.20 56.49 -2 -4 -3 156.38 6.90 2 -4 3 151.58 6.30 2 4 -3 166.38 7.00 -2 -4 -3 152.88 7.20 -2 -4 -3 154.88 6.60 2 -4 3 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295.77 14.60 -11 4 -5 297.47 15.20 11 4 5 319.17 16.50 11 -4 -5 302.17 12.20 -11 4 -5 298.17 16.10 11 -4 -5 293.37 11.80 -11 4 -5 276.67 14.30 -11 -4 5 283.87 8.90 11 -4 6 15.60 8.10 -11 -4 -6 19.70 9.20 11 -4 6 14.20 6.70 -11 4 6 18.20 4.90 -11 4 6 18.20 5.60 -11 4 6 9.10 2.40 -11 -4 -6 22.00 8.00 -11 -4 -6 4.60 8.80 -11 4 6 14.50 5.30 11 -4 6 13.00 7.00 11 4 -6 9.60 6.20 11 4 6 18.10 6.40 -11 -4 6 18.70 6.20 -11 -4 6 13.40 7.30 11 -4 -6 25.10 5.50 -11 4 -6 9.70 7.90 -11 4 -6 10.50 8.00 -11 -4 6 24.60 7.70 11 -4 -6 21.10 5.70 11 4 6 14.80 8.40 -11 4 -6 19.80 8.70 11 -4 -6 11.20 5.50 11 4 6 23.40 7.60 11 -4 7 160.48 11.50 -11 -4 -7 142.49 13.60 -11 -4 -7 172.08 15.10 -11 4 7 138.59 10.10 -11 4 7 154.68 11.40 11 4 -7 132.19 12.50 -11 4 7 157.68 11.30 11 -4 7 136.99 14.60 11 -4 7 165.58 12.40 11 4 7 154.68 15.90 11 4 7 148.59 13.80 -11 4 -7 158.18 15.50 11 4 7 148.39 14.10 -11 -4 7 150.68 14.70 -11 -4 7 163.88 15.20 -11 4 -7 167.98 16.00 11 -4 -7 154.28 11.50 -11 4 -7 154.08 14.60 11 -4 -7 154.98 13.10 11 -4 -7 159.48 11.50 11 -4 8 15.00 8.50 11 4 -8 3.10 7.70 -11 -4 -8 -5.20 9.80 11 -4 8 6.30 9.70 -11 4 8 14.10 6.90 11 -4 8 11.50 8.00 -11 -4 -8 -10.70 13.40 -11 4 -8 13.10 10.20 11 4 8 25.60 9.40 11 4 8 -7.40 9.90 11 -4 -8 25.90 7.50 11 -4 -8 -1.90 7.50 -11 -4 8 2.60 9.30 -11 4 -8 6.40 10.20 11 -4 9 -19.20 8.80 -11 -4 -9 7.50 9.50 -11 -4 -9 16.20 12.60 11 -4 9 -0.40 9.70 -11 4 9 5.30 8.10 11 -4 9 -9.40 9.90 -11 -4 -9 7.50 10.90 11 4 9 1.10 10.10 -11 4 -9 -19.90 10.60 11 4 9 -5.60 9.80 11 -4 -9 0.40 8.40 -11 -4 9 -0.80 9.60 11 4 9 -3.90 9.90 -11 4 -9 10.10 11.20 11 -4 -9 -2.50 8.90 -11 4 -9 2.80 11.80 11 -4 10 9.50 10.70 11 -4 10 -7.10 11.60 -11 4 10 3.00 8.40 -11 -4 -10 2.10 14.50 -11 -4 -10 3.80 11.30 -11 -4 -10 -5.80 11.60 11 4 -10 0.70 11.30 11 4 -10 6.90 12.00 11 -4 10 7.30 11.80 -11 4 -10 11.70 12.70 -11 4 -10 -8.40 12.80 -11 4 -10 21.30 23.00 11 -4 -10 3.10 9.90 11 -4 -10 -0.90 10.10 11 4 10 9.30 12.20 11 4 10 8.20 11.70 11 4 10 2.10 10.70 12 -4 0 38.10 3.10 12 -4 0 33.40 3.90 -12 -4 0 34.20 5.00 12 4 0 47.70 6.00 12 4 0 32.80 6.10 -12 -4 0 40.30 6.50 -12 4 0 38.40 3.60 -12 4 0 37.90 4.30 -12 4 0 47.10 5.30 -12 4 0 38.30 4.30 12 -4 0 40.70 5.70 -12 -4 0 37.70 6.50 12 4 0 36.40 5.40 12 4 0 36.50 5.50 12 4 0 35.30 5.80 12 -4 0 34.40 4.30 -12 4 0 45.40 4.80 -12 4 0 43.60 6.10 -12 -4 0 38.80 5.40 -12 -4 0 43.10 6.00 -12 -4 0 49.00 6.40 12 4 0 36.30 5.60 -12 4 1 1935.91 54.69 12 4 -1 1884.41 55.99 12 4 -1 1943.91 55.89 12 -4 1 1866.81 55.69 12 4 -1 1777.72 55.99 -12 -4 -1 1917.01 56.39 -12 4 1 1879.31 53.89 -12 4 1 1927.91 55.29 12 4 -1 1810.82 56.29 12 -4 1 1900.61 54.09 12 -4 1 1930.51 55.19 12 -4 1 1886.71 55.19 -12 4 1 1891.11 54.79 -12 -4 -1 1941.61 56.59 12 4 -1 1917.51 56.09 12 -4 1 1930.21 54.39 -12 4 1 1836.42 54.39 -12 -4 -1 1937.21 56.79 -12 -4 -1 1925.71 55.79 12 4 -1 1921.61 55.19 -12 4 1 1903.41 55.39 12 -4 -1 1893.41 53.89 12 -4 -1 1880.41 55.09 12 -4 -1 1917.41 53.79 -12 -4 1 1940.81 55.09 -12 4 -1 1922.81 55.09 -12 -4 1 1977.20 56.49 12 4 1 1932.61 56.09 12 4 1 1935.01 55.89 -12 -4 1 1942.01 56.69 -12 4 -1 1979.60 56.29 12 4 1 1798.92 56.69 -12 4 -1 1916.71 55.59 -12 4 -1 1932.81 54.59 -12 -4 1 1905.11 55.79 12 4 1 1937.71 56.59 -12 4 -1 1925.81 54.99 -12 4 -1 1901.11 55.29 12 -4 -1 1875.01 53.99 12 4 1 1836.02 55.79 -12 -4 1 1946.01 56.59 -12 -4 -2 1.30 6.30 12 -4 2 9.90 5.50 12 -4 2 12.20 4.70 12 -4 2 10.70 3.80 12 -4 2 2.70 4.70 -12 4 2 12.40 4.10 12 4 -2 12.10 5.10 12 -4 2 11.10 3.80 -12 4 2 7.70 3.20 12 4 -2 6.20 5.00 -12 4 2 15.20 4.30 -12 -4 -2 3.40 6.20 12 4 -2 1.50 5.30 -12 -4 -2 11.30 5.80 -12 4 2 4.40 3.30 -12 -4 -2 -1.50 5.40 -12 -4 2 8.80 3.50 -12 4 -2 13.70 4.40 -12 4 -2 11.90 4.80 -12 4 -2 10.60 3.70 -12 -4 2 6.40 6.00 12 4 2 2.00 5.10 -12 4 -2 9.30 5.00 -12 -4 2 11.10 4.40 12 -4 -2 14.30 3.00 12 -4 -2 10.80 3.40 -12 4 -2 9.70 5.70 12 -4 -2 11.70 1.80 -12 -4 2 8.60 5.80 12 -4 -2 6.70 3.60 -12 -4 2 8.00 3.70 -12 4 -2 8.20 5.20 12 -4 -2 14.30 2.70 -12 -4 2 11.50 5.10 -12 4 -2 7.50 4.20 12 4 2 2.40 5.50 -12 -4 2 3.20 5.60 12 4 2 16.40 5.50 12 4 2 10.50 5.50 12 -4 3 14.40 4.10 -12 4 3 13.30 3.70 -12 4 3 8.30 3.30 -12 4 3 8.60 4.00 12 -4 3 6.50 5.50 -12 4 3 9.00 4.00 -12 -4 -3 9.90 6.00 -12 -4 -3 8.60 7.10 12 4 -3 11.70 5.30 12 -4 3 4.30 4.40 12 4 -3 1.60 6.00 -12 -4 -3 7.30 6.70 12 -4 3 10.30 6.10 12 4 -3 11.40 5.30 12 -4 -3 17.80 3.10 -12 4 -3 2.50 6.40 -12 4 -3 3.50 5.70 12 4 3 5.00 6.20 12 -4 -3 9.10 2.90 -12 -4 3 8.10 2.80 -12 4 -3 7.60 4.90 12 4 3 15.60 6.40 12 -4 -3 11.50 3.70 -12 4 -3 12.40 4.40 -12 -4 3 11.90 4.60 -12 -4 3 11.80 3.30 -12 4 -3 5.00 5.00 12 4 3 18.80 6.00 12 -4 -3 9.10 3.10 -12 4 -3 3.50 4.30 12 -4 -3 15.10 3.60 -12 -4 3 8.20 6.40 -12 -4 3 2.90 5.90 -12 -4 3 7.50 6.00 12 4 -4 2.00 6.20 -12 -4 -4 7.80 6.80 -12 4 4 5.10 3.90 -12 4 4 4.90 3.50 12 -4 4 8.80 4.80 12 4 -4 -3.10 5.00 -12 -4 -4 -1.50 7.20 12 -4 4 11.70 5.10 -12 4 4 7.70 4.10 12 -4 4 2.60 6.40 -12 -4 -4 1.20 7.10 -12 -4 4 2.90 6.20 -12 -4 4 2.40 1.40 12 -4 -4 6.30 4.30 12 -4 -4 2.40 3.90 12 4 4 3.70 7.00 12 4 4 3.30 6.50 -12 4 -4 0.00 5.20 -12 -4 4 5.50 6.10 -12 -4 4 1.90 6.40 12 4 4 7.90 5.90 -12 4 -4 -5.40 7.00 -12 4 -4 6.20 6.00 -12 -4 4 5.70 1.30 -12 4 -4 -0.60 5.80 -12 4 -4 1.70 5.30 -12 -4 4 3.30 4.90 12 -4 -4 -0.30 3.60 12 -4 5 208.88 10.80 -12 4 5 198.08 9.60 12 4 -5 204.08 13.00 12 4 -5 192.88 11.80 12 -4 5 221.28 13.20 -12 -4 -5 194.28 14.80 -12 4 5 187.88 10.20 -12 -4 -5 193.78 15.00 -12 -4 -5 214.28 14.00 -12 4 5 198.68 10.50 12 4 5 221.58 13.00 12 -4 -5 202.08 10.10 -12 -4 5 212.18 13.50 -12 -4 5 188.38 11.80 12 -4 -5 208.28 10.10 -12 4 -5 199.58 12.80 12 4 5 211.48 14.00 -12 4 -5 174.48 12.00 12 -4 -5 186.28 9.60 -12 -4 5 193.28 12.90 -12 4 -5 207.68 13.60 -12 4 -5 207.28 12.70 -12 -4 5 209.78 14.80 12 -4 -5 233.18 10.50 -12 -4 5 193.68 6.10 12 4 5 194.28 15.20 12 -4 6 4.20 6.70 12 -4 6 13.80 7.90 -12 4 6 7.30 5.50 12 4 -6 -0.90 5.90 -12 4 6 1.00 5.40 12 4 -6 10.80 8.10 -12 -4 -6 12.90 9.80 -12 4 6 17.30 5.10 -12 -4 -6 10.50 8.40 12 -4 6 -3.40 8.00 -12 -4 -6 -1.90 9.30 -12 4 -6 -1.10 8.00 12 4 6 -7.90 8.70 12 -4 -6 10.30 6.00 12 4 6 7.10 7.90 -12 -4 6 18.60 8.30 -12 4 -6 -4.00 8.80 -12 -4 6 8.70 7.60 12 4 6 13.70 8.50 12 -4 -6 2.30 5.50 12 -4 -6 -1.00 5.50 -12 4 -6 20.50 9.20 12 -4 -6 6.40 5.30 12 -4 7 519.05 22.00 -12 -4 -7 483.15 24.50 -12 4 7 487.75 19.30 -12 4 7 515.25 20.20 -12 -4 -7 518.45 24.70 12 -4 7 588.54 21.50 12 -4 7 481.95 23.00 12 4 -7 506.25 20.40 12 -4 -7 518.25 19.60 -12 -4 7 532.55 23.10 12 -4 -7 522.45 19.70 -12 4 -7 560.14 23.60 12 4 7 533.45 21.90 12 4 7 521.75 22.60 -12 4 -7 525.75 22.90 -12 -4 7 508.55 21.70 12 4 7 537.15 24.30 12 4 -8 -15.70 7.00 -12 -4 -8 -3.90 9.40 -12 -4 -8 -15.30 11.60 12 -4 8 11.30 9.20 -12 -4 -8 -2.70 9.50 -12 4 8 -5.40 7.00 12 -4 8 4.60 8.40 12 4 8 3.60 10.00 -12 4 -8 -3.20 10.50 12 4 8 -1.00 9.40 12 -4 -8 2.90 7.80 -12 -4 8 5.30 9.00 12 4 8 -1.30 8.20 -12 -4 8 -13.30 9.90 -12 4 -8 -4.40 10.10 -12 4 -8 -5.60 11.00 -12 -4 -9 -22.50 10.60 -12 -4 -9 -5.70 20.40 12 -4 9 2.10 10.20 12 -4 9 -8.50 11.00 -12 4 9 15.40 8.40 12 -4 9 7.70 13.70 -12 -4 -9 3.60 11.00 -12 4 -9 6.10 12.30 -12 4 -9 -12.80 11.30 12 4 9 3.00 10.30 12 4 9 -5.30 12.00 -12 -4 9 -12.00 10.70 -12 4 -9 -3.20 11.50 -12 -4 9 -8.10 9.70 12 -4 -9 1.80 8.80 12 -4 10 -14.60 10.30 12 4 -10 -7.70 14.00 -12 -4 -10 18.60 13.10 12 -4 10 7.50 12.30 -12 4 10 20.70 9.30 -12 -4 -10 1.40 15.10 -12 -4 -10 -2.60 12.10 12 -4 10 -9.50 12.90 12 4 10 4.10 12.50 -12 -4 10 10.20 11.20 12 4 10 7.50 13.50 -12 4 -10 15.40 14.00 12 4 10 13.80 10.80 -12 4 -10 11.00 13.40 -12 4 -10 9.60 12.80 12 -4 -10 3.00 10.10 -13 -4 0 -0.80 6.00 -13 4 0 6.30 4.50 -13 4 0 5.10 4.40 -13 -4 0 -5.60 6.30 -13 4 0 2.30 3.30 -13 4 0 4.50 3.80 -13 -4 0 9.50 5.80 13 4 0 2.50 5.30 -13 4 0 -1.40 4.90 13 -4 0 -1.20 5.00 -13 4 0 -1.50 3.80 13 4 0 -0.20 5.30 -13 -4 0 -7.00 4.40 13 4 0 -7.50 4.90 13 -4 0 3.50 4.00 13 -4 0 -2.70 3.80 -13 -4 0 -0.60 4.40 -13 -4 0 8.10 5.40 13 -4 0 0.20 2.90 13 4 0 -1.50 5.10 13 -4 0 5.30 2.70 13 4 -1 152.28 10.30 -13 4 1 146.99 9.00 13 4 -1 142.59 10.80 13 4 -1 162.48 9.00 -13 -4 -1 138.89 11.50 13 -4 1 142.49 9.20 -13 -4 -1 139.29 9.40 -13 4 1 147.49 8.20 -13 4 1 145.99 6.70 13 4 -1 142.89 10.60 -13 -4 -1 162.58 10.00 -13 4 1 153.58 7.80 13 -4 1 149.39 10.50 13 -4 1 152.98 7.30 13 -4 1 144.59 9.10 -13 -4 -1 124.69 11.00 -13 -4 -1 162.48 11.10 -13 4 1 149.88 8.50 13 -4 1 151.68 6.90 -13 4 1 155.28 8.10 13 -4 -1 151.18 6.90 -13 -4 1 160.98 10.90 -13 4 -1 148.19 8.10 -13 4 -1 152.08 7.20 -13 4 -1 143.89 10.50 -13 -4 1 161.08 11.30 -13 -4 1 145.59 10.60 13 -4 -1 148.99 6.30 13 -4 -1 136.49 9.10 -13 4 -1 141.59 8.70 13 -4 -1 138.09 8.60 -13 4 -1 151.18 8.70 13 4 1 161.48 10.20 13 4 1 146.09 11.00 -13 4 -1 151.08 9.40 13 4 1 133.89 10.00 -13 4 -1 134.79 9.80 -13 -4 1 154.28 8.70 13 4 1 146.99 10.30 -13 -4 1 134.89 9.20 13 -4 2 343.47 12.40 13 4 -2 377.46 15.40 13 4 -2 341.37 14.70 -13 4 2 355.46 13.50 -13 -4 -2 360.06 15.50 13 -4 2 359.46 14.40 -13 -4 -2 332.27 15.60 -13 -4 -2 335.67 16.20 -13 4 2 355.46 12.20 13 4 -2 328.77 14.20 13 -4 2 370.26 15.50 13 -4 2 294.17 12.80 -13 4 2 354.36 12.90 13 -4 2 321.77 14.30 -13 4 -2 331.57 12.40 -13 4 -2 333.67 14.20 13 -4 -2 347.27 10.70 13 4 2 338.97 14.40 -13 -4 2 360.06 16.30 13 4 2 332.77 15.90 -13 4 -2 326.57 15.50 -13 4 -2 351.46 13.50 13 4 2 354.76 15.20 -13 4 -2 337.37 13.30 13 -4 -2 328.77 12.30 -13 -4 2 336.57 14.90 13 -4 -2 348.77 11.60 -13 -4 2 354.36 15.20 -13 4 -2 344.97 13.40 -13 -4 2 328.57 14.20 -13 -4 2 334.77 12.50 -13 -4 2 340.47 12.50 13 -4 3 3.90 4.20 -13 4 3 2.80 4.70 -13 4 3 6.90 3.60 13 -4 3 1.20 4.40 -13 -4 -3 7.30 6.50 13 -4 3 -3.30 5.80 -13 -4 -3 -6.80 7.00 13 4 -3 3.70 5.40 -13 4 3 2.50 4.20 13 4 -3 7.10 6.10 -13 4 3 2.50 4.20 -13 -4 -3 -5.30 6.80 13 -4 3 -1.80 6.30 -13 4 -3 5.50 5.50 -13 -4 3 1.40 3.50 13 -4 -3 9.30 3.70 13 4 3 -3.40 5.70 13 -4 -3 0.70 3.00 -13 4 -3 11.00 5.80 -13 -4 3 2.90 3.20 13 4 3 -2.50 6.60 -13 -4 3 9.60 6.30 -13 -4 3 4.70 5.30 -13 4 -3 -0.80 5.70 13 -4 -3 2.70 3.10 13 4 3 11.50 6.60 -13 4 -3 -6.80 6.80 -13 4 -3 -2.80 4.60 -13 -4 3 3.50 6.90 13 -4 -3 8.00 3.20 13 -4 -3 6.90 3.90 -13 -4 3 5.30 6.60 -13 4 -3 -2.80 5.00 13 -4 4 166.08 12.40 -13 4 4 158.48 9.50 -13 -4 -4 163.38 12.90 -13 -4 -4 155.98 13.50 -13 4 4 164.98 9.00 13 4 -4 159.08 11.00 13 4 -4 172.68 11.90 -13 -4 -4 171.98 13.90 13 -4 4 171.88 9.60 13 -4 4 184.38 10.00 13 -4 -4 165.08 8.80 -13 -4 4 152.48 12.20 -13 -4 4 163.78 12.70 -13 4 -4 162.78 13.70 13 -4 -4 167.48 9.40 -13 4 -4 168.88 12.20 -13 -4 4 185.78 11.70 13 4 4 154.28 13.50 13 -4 -4 165.78 8.50 13 4 4 175.18 11.70 -13 -4 4 171.68 11.00 -13 4 -4 146.79 10.60 13 -4 -4 162.68 8.10 -13 4 -4 163.58 11.80 -13 4 -4 171.38 11.70 -13 -4 4 170.38 5.80 13 4 4 160.08 12.90 -13 4 5 57.69 6.20 -13 4 5 69.69 7.60 -13 4 5 52.79 6.00 13 -4 5 68.09 7.40 -13 -4 -5 66.49 10.30 13 4 -5 52.99 8.30 13 -4 5 50.59 8.70 13 4 -5 55.19 7.10 -13 -4 -5 45.30 9.90 -13 -4 -5 46.90 8.80 13 -4 -5 50.99 6.20 -13 4 -5 48.50 9.00 -13 4 -5 53.29 10.00 -13 4 -5 44.10 7.50 -13 4 -5 55.99 8.90 13 4 5 61.69 9.30 13 -4 -5 51.29 5.70 13 4 5 59.89 9.70 13 -4 -5 63.69 6.50 13 -4 -5 55.39 5.70 13 4 5 71.59 8.70 -13 -4 5 59.89 8.10 -13 -4 5 50.79 7.00 13 -4 -5 55.89 5.90 -13 -4 5 54.89 8.40 -13 -4 5 58.29 8.70 -13 4 6 325.67 14.50 -13 4 6 316.87 14.40 13 4 -6 291.97 15.30 -13 -4 -6 297.17 19.20 -13 4 6 315.57 13.90 13 4 -6 305.77 16.90 -13 -4 -6 331.07 19.80 13 -4 6 322.87 15.40 13 -4 6 345.67 15.80 -13 -4 -6 333.67 18.20 13 4 6 331.87 17.50 13 -4 -6 304.17 14.00 -13 4 -6 321.57 19.40 -13 -4 6 341.67 18.10 -13 4 -6 318.67 17.90 13 4 6 328.47 19.30 13 -4 -6 322.87 14.20 -13 -4 6 306.67 17.50 -13 4 -6 306.37 17.20 13 4 6 330.27 16.80 13 -4 -6 289.77 13.80 -13 -4 -7 16.00 11.50 -13 -4 -7 33.50 10.50 -13 -4 -7 36.60 13.50 -13 4 7 29.80 7.20 13 4 -7 43.40 7.80 13 -4 7 36.80 9.80 -13 4 7 29.40 6.80 13 4 -7 37.00 10.00 13 -4 7 45.20 8.30 13 -4 7 19.60 9.90 13 4 7 29.20 11.10 -13 4 -7 33.90 11.20 -13 -4 7 47.40 9.80 -13 4 -7 45.70 10.50 -13 -4 7 16.90 10.00 13 4 7 41.60 9.30 13 -4 -7 31.80 7.30 13 4 7 47.50 10.40 -13 4 -7 29.80 10.20 -13 -4 -8 4.40 10.80 13 4 -8 27.10 8.20 -13 4 8 20.10 7.90 -13 -4 -8 0.70 12.00 13 -4 8 19.40 10.40 -13 -4 -8 25.10 11.20 -13 4 8 17.30 7.40 -13 -4 -8 5.80 13.00 13 -4 8 6.00 11.40 13 -4 8 20.80 9.70 -13 -4 8 8.10 11.80 -13 4 -8 14.90 10.80 -13 4 -8 18.50 11.50 -13 4 -8 3.30 11.40 13 4 8 17.80 9.90 -13 -4 8 18.10 10.20 13 4 8 39.50 10.50 13 -4 -8 18.50 8.30 13 4 8 14.30 11.50 -13 4 9 4.90 8.20 -13 -4 -9 -1.30 11.80 13 -4 9 4.70 11.30 -13 4 9 7.90 9.40 13 -4 9 4.00 9.80 -13 -4 -9 20.40 14.20 -13 -4 -9 11.80 12.10 -13 4 -9 10.30 12.10 13 4 9 10.20 11.90 13 -4 -9 2.70 9.10 -13 -4 9 2.10 12.50 -13 4 -9 20.10 13.30 13 4 9 -5.40 11.20 13 4 9 6.90 10.50 -13 -4 9 10.70 10.40 -13 4 -9 7.40 12.00 14 -4 0 426.16 16.40 -14 4 0 449.66 15.50 -14 4 0 443.26 16.90 14 -4 0 438.76 14.30 14 -4 0 428.66 15.70 -14 -4 0 423.76 16.20 -14 -4 0 423.16 19.00 -14 -4 0 427.96 17.60 14 4 0 460.25 17.50 -14 4 0 432.36 15.30 -14 4 0 434.56 16.10 -14 4 0 442.76 16.00 14 4 0 430.36 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3.90 5.20 -15 4 -2 5.90 5.10 -15 -4 2 -3.90 4.60 -15 -4 2 4.50 7.30 15 -4 -2 2.00 3.30 15 -4 -2 7.80 2.60 -15 -4 2 0.90 7.50 -15 -4 2 10.90 7.60 -15 4 -2 5.10 7.70 -15 -4 2 -3.50 4.80 -15 4 -2 2.80 6.10 -15 4 -2 2.40 5.40 15 4 2 -0.90 7.00 15 -4 -2 4.00 4.50 15 -4 3 544.35 18.90 -15 -4 -3 555.74 21.70 -15 4 3 509.95 18.70 -15 4 3 563.84 18.90 -15 -4 -3 575.14 23.20 -15 -4 -3 506.55 22.10 -15 -4 -3 553.94 21.60 15 4 -3 541.65 20.50 -15 4 3 536.25 18.30 15 -4 3 529.05 21.30 15 -4 3 511.85 21.00 15 4 -3 535.55 20.30 -15 4 3 527.35 18.10 15 -4 3 558.84 18.20 15 -4 -3 530.15 17.30 15 4 3 552.04 20.50 -15 4 -3 530.05 18.90 -15 4 -3 582.64 21.50 -15 -4 3 556.84 22.30 -15 -4 3 539.55 21.60 15 -4 -3 519.85 18.60 15 4 3 545.05 21.80 15 4 3 514.15 22.20 -15 4 -3 538.95 20.20 -15 -4 3 535.25 17.50 -15 -4 3 529.65 17.70 -15 -4 3 561.14 21.80 15 -4 -3 537.95 17.10 -15 4 -3 564.84 22.30 15 -4 -3 503.15 17.00 -15 4 -3 531.45 20.10 -15 -4 -4 42.20 9.20 -15 4 4 29.10 5.40 -15 4 4 30.20 6.00 -15 -4 -4 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5.70 -11 -5 -4 23.30 7.60 11 5 -4 1.20 5.30 11 -5 4 16.00 6.10 -11 -5 -4 24.40 6.60 -11 -5 -4 12.10 7.30 -11 5 4 13.90 3.60 11 -5 4 9.90 4.70 -11 5 4 16.40 3.10 11 5 -4 9.80 6.50 -11 -5 4 8.70 6.60 -11 -5 4 13.40 1.90 -11 -5 4 9.40 5.50 11 5 4 20.30 6.00 11 -5 -4 13.00 3.40 11 5 4 20.60 7.20 -11 5 -4 12.90 5.00 -11 5 -4 13.70 6.00 -11 -5 4 10.70 3.00 -11 5 -4 8.40 4.90 11 -5 -4 15.40 2.00 11 -5 -4 19.40 3.50 -11 5 -4 9.90 6.80 11 5 4 36.10 7.30 -11 5 -4 2.10 6.00 -11 -5 4 9.70 6.30 11 -5 -4 10.40 3.70 -11 -5 4 14.00 1.80 11 -5 -4 18.90 3.60 11 -5 -4 16.90 3.70 -11 -5 4 13.80 6.20 11 5 -5 -2.80 6.60 -11 -5 -5 8.10 6.90 -11 -5 -5 -3.90 7.80 11 -5 5 -7.00 6.30 11 5 -5 -0.30 5.80 -11 5 5 2.20 4.10 11 -5 5 0.00 6.60 -11 5 5 7.00 4.30 -11 5 5 5.60 3.60 11 -5 5 2.30 5.00 -11 -5 -5 -10.20 7.50 -11 -5 5 4.20 7.00 -11 -5 5 5.60 5.70 11 -5 -5 -2.10 4.20 11 5 5 0.00 6.80 -11 -5 5 1.40 2.40 -11 5 -5 -4.90 6.80 -11 5 -5 -14.60 5.50 11 -5 -5 -0.90 4.30 -11 5 -5 2.60 7.50 11 -5 -5 -3.10 3.30 11 5 5 9.70 6.80 -11 5 -5 1.60 6.60 11 5 5 -1.40 7.50 11 -5 -5 4.80 3.90 11 -5 -5 2.40 4.00 -11 -5 5 9.50 6.90 -11 -5 5 -2.10 6.90 -11 -5 -6 736.83 27.70 -11 -5 -6 739.03 28.00 -11 5 6 715.53 23.00 11 -5 6 709.93 26.40 -11 -5 -6 747.83 26.70 11 -5 6 729.63 25.80 -11 5 6 725.33 23.50 -11 5 6 697.93 23.30 11 5 -6 705.73 25.20 11 -5 6 757.02 24.50 -11 -5 6 715.73 26.80 11 -5 -6 653.53 23.90 -11 5 -6 783.52 27.10 11 -5 -6 718.33 23.60 -11 5 -6 725.83 26.70 11 -5 -6 695.23 23.40 11 -5 -6 671.83 23.50 -11 -5 6 697.63 25.90 -11 5 -6 740.73 27.30 11 5 6 736.93 27.70 11 5 6 746.33 25.60 11 -5 -6 715.33 23.70 11 5 6 700.13 26.20 -11 5 7 18.30 5.90 -11 -5 -7 1.20 8.60 -11 5 7 10.80 5.70 11 5 -7 13.10 7.10 11 -5 7 17.00 7.30 11 -5 7 10.50 8.50 -11 5 7 9.60 2.50 11 -5 7 27.50 8.70 -11 -5 -7 5.30 9.90 11 5 7 19.20 8.50 -11 5 -7 12.70 9.00 11 -5 -7 2.30 6.00 -11 5 -7 15.00 8.80 11 -5 -7 10.30 6.30 -11 -5 7 10.50 8.90 11 5 7 14.80 8.40 11 5 7 13.20 9.60 -11 -5 7 14.20 8.10 -11 5 -7 24.90 9.80 11 -5 8 11.80 8.20 -11 5 8 12.60 6.60 -11 -5 -8 28.80 12.20 11 -5 8 20.80 7.60 11 5 -8 22.60 8.30 11 -5 8 12.70 9.70 -11 -5 -8 13.20 8.10 11 5 8 28.50 9.20 11 5 8 6.20 10.40 11 5 8 8.80 9.70 -11 -5 8 25.80 9.30 11 -5 -8 30.70 7.30 -11 5 -8 10.20 10.50 11 -5 -8 5.90 7.70 -11 5 -8 -5.30 9.80 11 -5 9 -19.90 10.70 11 -5 9 -8.50 10.00 -11 -5 -9 0.20 10.00 -11 5 9 18.20 7.90 -11 -5 -9 -4.70 13.30 11 5 -9 6.80 8.10 11 -5 -9 -4.70 8.30 -11 5 -9 -11.10 10.90 11 5 9 -6.30 10.70 -11 5 -9 1.60 11.00 -11 5 -9 -0.30 11.70 11 5 9 14.50 9.80 11 5 9 -8.70 11.90 -11 -5 9 -2.10 10.00 11 -5 -9 -4.60 7.90 11 5 -10 37.90 14.00 -11 5 10 46.00 9.40 -11 -5 -10 72.59 14.00 -11 -5 -10 61.69 15.60 11 -5 10 64.99 13.10 11 -5 10 48.80 13.20 -11 -5 -10 77.49 13.40 -11 5 -10 43.90 14.20 -11 -5 10 66.89 12.10 -11 5 -10 51.59 13.70 11 5 10 68.49 13.50 11 5 10 57.29 12.50 -11 5 -10 82.69 17.20 11 5 10 64.49 13.50 11 -5 -10 71.49 11.50 11 -5 -10 76.99 10.90 12 -5 0 1894.71 54.59 -12 5 0 1929.01 54.89 12 -5 0 1902.91 55.69 12 -5 0 1881.41 53.89 12 -5 0 1875.01 53.49 12 -5 0 1892.81 54.79 12 5 0 1915.11 55.79 -12 -5 0 1907.31 56.99 12 5 0 1949.80 56.29 -12 -5 0 1891.01 56.19 -12 5 0 1947.71 54.69 -12 5 0 1931.11 55.39 -12 -5 0 1864.71 56.29 -12 5 0 1841.22 54.69 -12 5 0 1858.21 53.89 12 5 0 1861.61 56.19 -12 -5 0 1963.20 56.79 -12 -5 0 1914.81 56.89 -12 -5 0 1935.41 55.69 -12 5 0 1970.40 56.09 12 5 0 1998.90 56.99 -12 5 1 -1.10 1.80 12 -5 1 -0.10 3.90 -12 5 1 6.50 2.90 12 -5 1 1.50 2.40 12 5 -1 7.10 5.00 -12 5 1 -0.40 3.20 -12 -5 -1 5.10 6.20 12 -5 1 3.90 5.50 -12 -5 -1 -2.80 5.80 -12 -5 -1 10.10 4.60 -12 -5 -1 -4.40 5.30 12 5 -1 2.90 4.20 12 5 -1 17.20 5.80 -12 5 1 3.20 3.10 -12 5 1 7.80 4.90 -12 -5 -1 4.30 4.80 12 5 -1 3.70 5.10 12 -5 1 1.90 3.00 12 -5 -1 -4.40 4.30 -12 5 -1 1.80 4.10 -12 -5 1 -0.10 6.10 12 -5 -1 4.10 4.80 12 5 1 3.60 5.10 -12 5 -1 -2.20 3.40 12 -5 -1 1.80 2.20 -12 5 -1 5.90 5.50 -12 -5 1 3.20 4.20 12 -5 -1 5.90 1.60 -12 -5 1 8.90 5.60 -12 5 -1 0.80 3.80 12 5 1 2.30 5.40 12 5 1 5.90 5.50 -12 5 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25.70 6.80 12 -5 3 35.80 4.80 -12 -5 -3 24.50 7.60 12 5 -3 19.80 6.60 12 -5 3 30.50 6.10 -12 -5 -3 20.20 7.50 12 -5 -3 34.40 3.10 12 5 3 20.00 7.10 -12 -5 3 37.00 4.20 -12 5 -3 23.70 5.90 -12 -5 3 28.50 3.50 -12 -5 3 21.80 5.10 -12 5 -3 29.70 4.90 12 5 3 35.30 7.20 -12 5 -3 28.80 5.50 -12 -5 3 34.30 7.30 12 -5 -3 28.10 4.60 12 -5 -3 28.40 3.50 12 5 3 28.60 6.20 -12 5 -3 27.20 5.50 12 -5 -3 33.10 3.80 -12 -5 3 24.90 6.80 -12 5 -3 41.20 7.30 -12 -5 3 30.70 7.00 12 -5 -3 30.70 3.50 12 -5 -3 36.90 3.10 -12 5 4 364.46 13.10 12 -5 4 372.66 16.10 -12 5 4 356.66 12.30 12 -5 4 376.26 14.20 12 -5 4 342.37 15.40 12 5 -4 348.67 15.60 12 -5 4 393.46 14.10 -12 5 4 361.56 12.80 -12 -5 -4 376.86 16.50 12 5 -4 363.76 16.10 -12 -5 -4 368.66 17.50 -12 -5 -4 335.97 17.60 12 -5 -4 369.86 13.30 -12 -5 4 369.26 16.70 12 5 4 363.16 15.80 12 5 4 340.67 16.50 -12 -5 4 369.66 15.60 -12 -5 4 355.26 11.00 12 -5 -4 368.56 12.50 12 -5 -4 367.76 12.60 -12 -5 4 367.96 11.00 -12 5 -4 403.66 16.70 12 -5 -4 372.16 12.50 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877.91 26.10 10 -6 -6 905.61 27.90 10 -6 -6 829.62 28.20 10 -6 -6 874.11 27.00 -10 6 7 46.10 4.50 -10 6 7 41.00 4.30 -10 -6 -7 37.60 11.00 10 -6 7 31.50 8.80 10 -6 7 47.20 7.90 -10 6 7 38.90 5.70 10 -6 7 62.99 9.10 -10 6 7 48.10 6.20 10 6 -7 33.80 7.80 -10 -6 -7 52.79 9.30 -10 -6 7 35.50 3.10 -10 6 -7 50.09 10.10 10 -6 -7 52.99 7.20 -10 -6 7 53.29 8.80 -10 6 -7 35.50 9.90 10 6 7 51.19 9.30 10 6 7 36.10 9.50 10 6 7 39.70 10.00 10 -6 -7 54.79 6.50 -10 6 -7 39.10 9.70 -10 -6 7 48.00 4.00 10 -6 -7 53.89 6.80 10 -6 -7 54.49 6.40 10 -6 -7 40.30 4.50 -10 -6 -8 192.18 17.00 -10 6 8 178.98 8.70 10 6 -8 192.58 14.20 -10 -6 -8 176.98 18.60 10 -6 8 152.08 15.10 10 -6 8 154.58 15.40 -10 6 8 192.98 11.90 10 -6 -8 194.28 13.40 -10 -6 8 192.48 15.50 10 6 8 205.38 17.60 10 -6 -8 182.58 12.50 -10 6 -8 139.09 16.90 -10 6 -8 216.98 18.10 -10 6 -8 204.08 17.50 10 6 8 200.88 12.90 -10 -6 -9 -35.70 11.60 -10 -6 -9 10.20 10.90 10 -6 9 3.10 9.80 10 6 -9 -8.40 9.20 -10 6 9 0.60 7.20 10 6 -9 -3.00 10.60 10 -6 9 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11.60 -20 -7 3 10.20 12.40 20 7 3 -0.30 11.70 -20 7 -3 31.20 13.50 20 7 3 28.30 12.70 -20 -7 3 -0.50 11.80 0 -8 0 4510.05 125.59 0 -8 0 4414.86 125.59 0 -8 0 4628.64 125.69 0 -8 0 4551.74 126.19 0 8 0 4537.85 125.69 0 8 0 4354.56 125.59 0 -8 0 4539.05 125.89 0 -8 0 4412.76 125.49 0 -8 0 4518.75 125.79 0 8 0 4429.76 125.59 0 8 0 4456.75 125.89 0 8 -1 2.90 2.50 0 -8 1 -2.10 2.50 0 -8 -1 -0.20 3.10 0 -8 1 -1.90 2.40 0 8 -1 -0.40 2.80 0 -8 -1 -3.60 2.50 0 -8 -1 2.00 2.20 0 8 -1 -0.60 2.30 0 8 1 -2.30 2.40 0 -8 -1 -2.20 2.20 0 8 1 -4.00 2.60 0 -8 1 -1.20 2.50 0 8 -1 -0.20 2.10 0 -8 1 -4.70 2.50 0 8 1 1.10 2.30 0 -8 -1 -3.00 2.20 0 -8 -1 -4.10 2.20 0 -8 1 -0.60 2.10 0 -8 1 2.70 2.70 0 -8 -2 1888.81 55.49 0 8 2 1964.60 55.69 0 8 2 1960.40 55.69 0 8 2 1967.20 55.89 0 -8 -2 1940.91 55.59 0 8 -2 1990.70 56.39 0 -8 -2 1914.91 55.69 0 -8 -2 1946.51 55.99 0 8 -2 1987.10 55.99 0 -8 2 2031.60 56.09 0 8 -2 2004.90 56.09 0 -8 -2 1984.20 55.49 0 -8 2 1754.32 56.69 0 8 -2 1948.31 56.09 0 -8 2 2001.70 56.79 0 8 -2 1940.61 56.19 0 -8 2 2076.29 56.49 0 -8 2 1814.12 55.89 0 -8 -2 2006.70 55.89 0 8 3 -1.50 3.10 0 -8 3 -1.90 3.40 0 8 -3 -4.10 3.10 0 8 3 -1.80 2.70 0 -8 3 -4.10 3.30 0 8 3 -1.60 3.80 0 -8 -3 -3.40 2.90 0 8 3 0.30 2.80 0 -8 -3 -4.40 2.60 0 8 -3 -2.30 3.50 0 -8 -3 5.20 2.60 0 -8 3 0.80 3.50 0 -8 -3 -1.60 2.90 0 -8 -3 -0.60 3.30 0 -8 3 -3.00 3.10 0 -8 -3 -0.20 2.90 0 8 -3 -6.10 3.10 0 8 -3 -3.20 3.60 0 -8 3 -3.70 2.80 0 -8 3 -5.70 3.00 0 8 -3 1.00 3.00 0 -8 -4 1.20 2.90 0 8 4 6.40 3.70 0 -8 4 7.00 3.90 0 8 -4 4.80 3.80 0 -8 -4 2.10 3.50 0 8 -4 8.50 3.60 0 -8 -4 6.70 4.00 0 8 4 -0.90 3.30 0 -8 4 4.50 3.00 0 -8 4 7.60 3.90 0 -8 -4 6.20 3.10 0 8 -4 3.30 3.80 0 -8 -4 2.10 4.10 0 8 4 3.00 3.60 0 8 -4 3.90 4.40 0 8 4 6.90 3.70 0 8 -4 3.60 3.40 0 -8 4 4.20 4.00 0 8 5 1.70 4.40 0 8 -5 3.80 5.20 0 -8 -5 -0.10 4.60 0 -8 5 1.30 4.40 0 8 -5 -3.50 4.30 0 -8 -5 -0.30 3.50 0 -8 5 1.00 4.40 0 8 -5 -0.20 4.80 0 -8 5 2.10 4.30 0 -8 -5 0.20 5.20 0 8 5 -4.20 4.10 0 8 -5 -3.80 4.30 0 -8 -5 -0.20 3.90 0 8 5 1.50 4.00 0 -8 5 -0.80 4.70 0 -8 -5 0.90 3.80 0 8 5 7.20 4.50 0 8 5 5.60 4.20 0 8 -5 3.10 4.50 0 -8 5 0.50 3.70 0 8 -6 496.95 17.40 0 8 -6 515.95 19.30 0 8 6 462.15 17.40 0 -8 -6 404.56 17.50 0 8 -6 459.55 17.70 0 8 6 481.75 17.80 0 -8 -6 483.45 17.30 0 8 6 469.15 17.10 0 -8 -6 482.55 16.50 0 -8 -6 478.55 17.50 0 -8 6 455.15 16.00 0 8 6 458.75 17.60 0 -8 6 498.75 17.20 0 -8 -6 478.45 18.20 0 8 6 480.75 17.50 0 -8 6 483.25 17.70 0 8 -7 -5.90 6.50 0 -8 -7 -4.00 7.00 0 -8 -7 -3.90 4.70 0 8 7 -8.90 6.40 0 8 7 -5.30 6.10 0 -8 7 -6.70 5.50 0 -8 7 6.70 4.90 0 8 7 -5.30 6.50 0 -8 -7 -6.50 5.90 0 8 -7 2.10 7.60 0 8 -7 -2.60 5.00 0 8 7 -4.00 5.40 0 8 8 753.52 27.40 0 8 -8 825.92 26.90 0 -8 8 764.82 25.80 0 8 8 800.42 27.30 0 -8 -8 768.22 28.60 0 8 -8 747.13 27.80 0 8 8 793.12 27.20 0 8 -8 809.52 30.00 0 -8 8 766.72 27.50 0 -8 -8 843.82 28.70 0 8 9 -8.80 7.70 0 8 -9 -8.10 8.50 0 -8 9 15.30 8.50 0 8 9 -12.00 8.60 0 8 9 -8.40 8.20 0 8 -9 -13.30 7.00 0 -8 9 3.60 6.60 0 -8 -9 -8.70 9.00 0 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18.90 9.40 -5 -8 9 23.90 9.10 -5 8 -9 17.90 13.30 5 -8 -9 22.30 9.20 5 8 9 18.60 9.50 5 8 9 1.90 10.20 -5 -8 9 27.30 6.30 -5 8 -9 12.80 9.20 5 -8 10 159.58 14.80 -5 8 10 177.78 15.10 -5 -8 -10 132.69 14.20 -5 8 10 164.68 13.90 5 8 -10 200.88 17.50 5 8 -10 159.28 16.50 -5 -8 -10 186.38 19.70 5 -8 10 171.28 16.20 -5 8 -10 145.69 15.60 5 8 10 163.08 14.00 5 8 10 172.68 18.30 -5 -8 10 162.38 17.00 -5 8 -10 189.18 16.60 5 -8 -10 151.18 14.20 -5 -8 10 166.48 11.70 5 8 10 136.39 14.80 5 -8 -10 149.59 16.80 -5 8 -10 196.08 17.90 -5 -8 -11 11.90 14.50 5 8 -11 -12.30 13.80 5 8 -11 33.30 13.70 -5 8 11 11.80 9.20 5 -8 11 32.80 11.70 5 -8 11 35.50 12.30 -5 8 11 2.10 10.50 -5 -8 -11 27.00 12.20 5 8 11 5.10 8.90 5 8 11 21.70 12.50 5 8 11 30.40 12.20 -5 -8 11 12.20 11.90 -5 8 -11 21.80 12.50 5 -8 -11 18.00 12.30 -5 8 -11 48.90 14.40 5 -8 -11 1.30 13.10 -5 8 -11 19.00 14.70 5 8 11 30.90 11.60 6 -8 0 2015.00 57.29 6 8 0 2038.10 57.99 -6 -8 0 1965.70 57.89 -6 -8 0 1971.50 58.09 -6 -8 0 2077.79 57.89 -6 8 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34.20 9.20 9 -9 -7 22.80 6.40 -9 -9 7 29.60 8.90 -9 9 -7 1.80 9.40 -9 -9 -8 14.10 10.70 -9 -9 -8 19.40 11.70 9 9 -8 -4.40 8.20 -9 -9 -8 4.00 9.50 9 -9 8 12.00 8.70 9 -9 8 9.30 8.60 -9 9 8 -1.40 6.20 9 9 8 6.00 10.20 -9 9 -8 -5.80 10.40 9 -9 -8 -4.10 7.40 -9 -9 8 7.70 4.90 9 -9 -8 3.50 5.70 -9 9 -8 2.90 10.20 -9 -9 8 8.10 9.80 9 9 8 0.40 9.40 -9 9 -8 -12.80 10.10 9 9 8 -9.70 10.20 -9 -9 -9 249.48 21.60 -9 -9 -9 271.67 19.60 9 9 -9 260.57 18.70 9 -9 9 295.67 18.40 9 -9 9 291.77 18.50 -9 9 9 275.37 15.70 9 9 -9 280.17 22.60 -9 9 -9 305.77 21.90 9 9 9 290.97 19.10 -9 9 -9 312.57 21.20 9 -9 -9 273.17 15.30 -9 -9 9 306.87 19.60 9 9 9 308.17 22.40 9 9 9 284.27 20.10 9 -9 -9 266.77 17.10 -9 -9 -10 15.60 15.80 9 -9 10 16.90 11.60 -9 9 10 10.00 9.00 -9 -9 -10 14.10 14.10 9 9 -10 16.10 12.20 -9 -9 -10 31.00 12.10 9 9 -10 7.80 13.30 9 -9 10 31.00 11.30 -9 9 -10 20.60 13.90 -9 -9 10 12.30 12.00 -9 9 -10 4.60 25.00 9 9 10 14.40 12.40 9 9 10 33.00 12.50 9 -9 -10 17.40 10.50 -9 9 -10 5.00 12.60 9 9 10 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6.80 6.50 10 9 2 1.60 6.00 -10 -9 2 -5.80 6.60 -10 -9 2 8.80 6.70 -10 9 -2 2.60 3.00 10 9 -3 116.39 11.50 -10 -9 -3 99.39 9.90 10 -9 3 79.49 6.60 10 -9 3 95.49 8.30 10 -9 3 103.39 9.80 -10 -9 -3 102.59 10.70 10 -9 3 120.09 8.90 10 9 -3 109.19 11.40 -10 -9 -3 75.79 9.10 -10 9 -3 98.29 8.70 10 -9 -3 102.59 8.80 -10 9 -3 97.09 9.20 -10 -9 3 94.69 8.00 -10 9 -3 91.39 7.00 -10 -9 3 98.19 9.20 -10 -9 3 102.99 9.40 -10 -9 3 107.69 11.20 -10 9 -3 103.29 11.20 -10 9 -3 91.19 6.30 10 9 3 84.39 9.00 10 -9 -3 101.39 7.40 10 9 3 105.19 8.50 -10 -9 3 104.59 7.10 -10 9 -3 97.69 7.50 10 9 3 94.59 9.10 -10 -9 -4 84.49 9.30 10 9 -4 78.19 8.20 10 9 -4 73.09 8.00 10 -9 4 73.49 8.40 10 -9 4 64.19 7.90 10 -9 4 69.19 7.20 -10 -9 -4 80.69 8.50 -10 -9 -4 87.19 10.00 -10 9 -4 77.89 9.40 -10 -9 4 65.59 8.70 10 9 4 70.49 9.10 -10 -9 4 79.79 7.60 -10 -9 4 85.79 9.30 -10 9 -4 75.09 7.00 10 -9 -4 62.99 5.00 -10 9 -4 78.19 7.80 10 9 4 80.09 9.30 -10 9 -4 74.69 6.10 10 9 4 89.09 8.70 -10 -9 4 72.09 9.20 10 -9 -4 64.49 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310.17 16.10 11 -9 -2 309.67 12.90 11 -9 -2 295.87 13.20 -11 9 -2 322.57 11.00 -11 -9 2 339.47 16.30 -11 9 -2 318.07 11.70 -11 -9 2 307.37 15.70 11 9 2 312.97 16.10 -11 -9 2 306.37 14.50 -11 9 -2 330.97 12.40 -11 -9 2 305.57 13.10 -11 9 -2 321.17 15.30 11 9 2 327.27 15.10 11 9 2 320.97 15.20 -11 9 -2 312.27 9.70 -11 -9 -3 325.97 16.70 11 -9 3 315.87 12.90 -11 -9 -3 259.27 16.20 -11 9 3 317.47 13.30 11 9 -3 294.67 15.20 11 -9 3 307.57 13.60 11 -9 3 299.97 13.30 11 9 -3 318.17 15.90 -11 -9 -3 324.07 15.60 11 -9 3 293.37 14.70 -11 9 -3 341.57 16.30 -11 9 -3 348.57 13.90 11 -9 -3 293.77 14.30 -11 9 -3 300.27 11.00 11 -9 -3 320.27 12.50 -11 9 -3 316.97 12.60 -11 9 -3 292.07 11.80 11 9 3 320.07 14.40 -11 -9 3 300.97 16.60 -11 9 -3 304.17 13.60 11 9 3 343.27 15.50 -11 -9 3 303.07 12.70 -11 -9 3 300.17 15.70 -11 -9 3 305.67 15.90 11 9 3 316.97 17.00 11 -9 4 1206.88 38.10 -11 -9 -4 1174.88 39.80 11 9 -4 1240.98 39.10 -11 -9 -4 1235.88 38.70 -11 -9 -4 1192.18 39.80 11 -9 4 1217.78 37.30 11 9 -4 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67.29 12.50 -10 10 -8 54.89 12.70 -10 10 -8 52.29 11.80 10 -10 9 174.98 17.60 -10 -10 -9 92.69 15.60 -10 -10 -9 123.49 14.40 -10 -10 -9 101.49 16.80 10 10 -9 91.49 12.40 10 -10 9 125.89 13.50 -10 -10 9 95.09 14.80 -10 10 -9 126.59 14.70 10 -10 -9 99.19 10.80 10 10 9 111.49 14.70 10 10 9 135.69 14.40 10 10 9 82.69 14.70 -10 -10 9 111.69 14.20 -10 10 -9 146.89 14.90 -10 10 -9 101.29 14.60 -11 -10 0 -4.60 7.30 -11 -10 0 -5.70 6.70 -11 -10 0 -13.80 6.70 11 -10 0 -3.20 3.30 11 10 0 -9.90 6.70 11 -10 0 0.30 5.70 -11 10 0 -5.10 6.00 11 10 0 -15.20 6.50 -11 -10 -1 469.45 19.10 11 -10 1 456.25 14.60 -11 -10 -1 450.45 19.60 11 10 -1 453.25 19.40 11 10 -1 485.35 18.00 11 -10 1 481.65 15.90 -11 -10 -1 449.95 19.60 -11 10 1 462.95 18.00 11 -10 1 480.65 18.30 11 -10 -1 446.86 17.20 -11 -10 1 471.95 19.70 -11 -10 1 471.55 19.60 -11 10 -1 467.05 18.70 -11 -10 1 495.05 19.60 11 10 1 431.16 19.50 -11 10 -1 447.66 14.40 -11 10 -1 468.25 14.20 -11 10 -1 458.85 14.70 11 10 1 479.25 18.80 -11 10 2 339.87 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110.79 6.60 -11 -10 5 73.69 10.30 -11 10 -5 85.39 9.30 11 10 5 72.09 9.30 -11 10 -5 96.59 8.70 -11 10 -5 80.59 8.00 -11 -10 -6 2.30 10.50 11 10 -6 1.80 7.40 -11 -10 -6 -23.30 15.70 -11 10 6 3.20 3.20 11 10 -6 -14.60 10.80 11 -10 6 9.50 8.20 11 -10 6 1.20 9.20 -11 -10 6 -7.40 8.90 -11 -10 6 5.30 5.30 -11 10 -6 11.10 8.10 11 -10 -6 2.90 4.00 11 -10 -6 4.40 3.70 -11 -10 6 -11.70 8.40 -11 -10 6 7.80 10.10 -11 10 -6 -3.10 7.50 11 10 -7 53.39 11.60 -11 -10 -7 37.90 10.30 11 -10 7 33.60 9.80 -11 -10 -7 31.60 11.80 11 10 -7 34.50 9.10 -11 -10 -7 35.20 10.10 -11 10 7 28.50 5.30 11 -10 7 38.40 10.30 11 10 7 49.99 10.60 -11 10 -7 38.60 10.90 -11 -10 7 32.00 5.70 -11 10 -7 25.90 11.50 -11 10 -7 41.50 10.10 11 10 7 35.50 11.40 -11 -10 7 29.20 11.80 11 -10 -7 38.50 6.20 -11 -10 7 21.00 10.30 11 10 7 24.70 10.60 -11 -10 -8 13.70 16.70 11 10 -8 39.20 13.10 -11 -10 -8 48.40 11.60 11 10 -8 54.09 10.90 -11 10 -8 46.00 10.70 -11 -10 8 52.49 13.40 11 10 8 54.39 22.00 11 10 8 50.39 11.30 -11 10 -8 45.60 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5.40 6.10 10 11 7 -5.60 10.10 -10 11 -7 8.60 10.20 10 -11 -7 17.60 6.10 -10 -11 -8 92.79 24.00 -10 -11 -8 65.09 11.90 10 -11 8 75.69 13.50 10 11 -8 61.09 10.60 10 11 -8 73.59 13.80 -10 -11 -8 65.39 14.10 -10 11 -8 62.39 12.40 -10 -11 8 77.19 14.40 -10 11 -8 62.39 12.90 10 11 8 75.89 12.50 -10 -11 8 75.39 12.60 -10 11 -8 75.09 12.10 10 -11 -8 57.79 8.40 10 11 8 83.59 13.80 -10 -11 8 67.69 7.60 10 11 8 52.69 12.80 -10 -11 -9 105.39 13.60 10 -11 9 84.79 12.40 10 11 -9 77.79 14.50 10 -11 9 97.89 13.40 -10 -11 -9 68.29 15.50 -10 -11 -9 77.89 16.80 -10 11 -9 75.19 13.40 10 11 9 61.49 13.90 -10 11 -9 68.79 14.40 -10 -11 9 91.29 15.60 10 11 9 63.39 13.10 -10 -11 9 82.59 13.50 -10 11 -9 56.29 13.80 10 11 9 74.09 14.70 -11 -11 0 -12.80 7.70 11 11 0 1.90 7.00 11 -11 0 1.50 6.10 11 11 0 -6.70 6.90 -11 -11 0 -8.80 5.60 11 -11 0 0.30 3.00 -11 -11 0 -0.40 7.30 -11 11 0 -1.00 6.50 11 -11 1 29.00 6.60 -11 -11 -1 27.50 7.50 -11 11 1 33.10 7.20 11 -11 1 29.00 4.50 11 -11 1 28.70 3.10 11 11 -1 23.00 8.40 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8.80 12 -12 3 59.59 8.70 -12 -12 -3 64.19 9.40 -12 -12 3 40.00 10.00 -12 12 -3 47.00 5.60 12 12 3 59.29 9.80 -12 12 -3 54.49 4.40 -12 -12 3 44.00 8.30 -12 12 -3 58.99 5.20 -12 12 -3 45.00 5.20 -12 -12 3 54.19 10.50 -12 12 -3 52.29 9.60 -12 12 -3 42.00 4.40 -12 12 -3 53.89 6.40 12 -12 -3 53.79 7.10 12 12 3 47.50 10.30 12 -12 4 -0.60 8.20 12 -12 4 5.80 6.10 -12 -12 -4 1.30 9.10 12 -12 4 -2.60 8.00 12 12 -4 1.80 11.00 -12 -12 -4 -17.30 10.70 12 12 -4 1.50 7.90 12 -12 -4 -1.50 5.70 -12 -12 4 1.40 9.00 12 12 4 -4.10 7.30 -12 12 -4 -1.90 6.50 -12 -12 4 1.90 9.60 -12 -12 4 -0.20 16.90 -12 12 -4 0.70 5.70 -12 -12 -5 -11.00 10.00 12 12 -5 3.20 8.60 12 -12 5 5.00 9.30 12 -12 5 15.50 7.50 12 12 -5 5.30 9.90 -12 -12 -5 18.70 9.30 -12 -12 -5 -22.40 9.70 12 -12 -5 -0.90 5.70 -12 -12 5 16.40 10.00 12 12 5 5.30 9.40 12 12 5 -13.20 9.50 -12 12 -5 1.60 7.60 -12 -12 5 2.30 9.70 -12 -12 5 23.40 11.00 -12 12 -5 -7.70 10.20 -12 12 -5 4.60 7.20 -12 -12 -6 48.30 13.10 12 12 -6 55.19 12.00 -12 -12 -6 57.59 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13 12 6 -16.10 19.10 -13 -12 6 5.90 13.00 -13 -12 -7 16.40 11.40 13 12 -7 -7.30 10.50 13 12 -7 0.40 12.50 -13 -12 -7 17.90 13.80 13 -12 7 -4.40 9.60 -13 -12 -7 34.00 15.30 13 -12 7 8.40 11.40 -13 12 -7 -11.00 11.80 -13 -12 7 2.10 12.60 13 12 7 17.80 11.20 -13 12 -7 19.80 10.30 -13 -12 7 -0.10 11.80 13 12 7 4.10 12.90 13 12 7 13.90 13.20 -14 -12 0 159.98 16.40 14 12 0 155.28 15.50 14 -12 0 136.99 13.20 -14 12 0 156.18 14.60 14 12 0 165.48 12.10 14 -12 0 138.39 6.70 -14 -12 0 127.29 19.80 14 -12 1 34.80 9.00 14 12 -1 24.00 9.60 -14 -12 -1 28.80 10.50 14 12 -1 32.20 11.30 -14 -12 -1 26.70 9.80 -14 12 1 29.70 8.60 14 -12 -1 32.40 8.10 14 12 1 33.00 10.00 -14 -12 1 35.20 11.00 -14 -12 1 38.20 12.70 14 12 1 48.00 11.10 -14 12 -1 26.40 9.80 -14 -12 -2 125.69 12.20 14 12 -2 116.49 12.00 -14 -12 -2 118.09 12.90 -14 12 2 123.39 12.90 14 -12 2 135.59 13.30 -14 -12 2 112.89 12.30 14 12 2 114.39 14.30 -14 -12 2 119.99 14.80 -14 -12 2 115.19 13.80 -14 12 -2 119.29 7.30 -14 12 -2 126.79 11.40 14 -12 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35.70 12.40 -10 -13 8 10.70 12.20 -10 13 -8 16.30 11.70 -10 13 -8 41.80 10.90 -10 13 -8 8.00 12.30 -10 -13 8 3.90 13.50 10 13 8 1.30 12.60 -11 -13 0 -1.50 8.70 -11 -13 0 3.60 8.20 11 13 0 9.10 6.60 -11 -13 0 1.20 8.30 -11 13 0 -11.30 7.30 11 -13 0 -1.10 6.30 11 13 0 0.40 8.10 11 -13 0 -2.30 3.30 -11 13 1 5.40 7.30 11 -13 1 5.40 4.50 11 13 -1 5.00 8.10 11 13 -1 0.50 8.10 -11 -13 -1 1.50 8.90 -11 -13 -1 -10.60 8.40 11 -13 1 -8.00 6.80 11 -13 1 -2.70 2.20 -11 -13 -1 3.50 7.90 -11 -13 1 6.90 8.70 11 13 1 1.60 6.50 11 -13 -1 2.80 6.70 -11 -13 1 8.20 8.30 11 13 1 17.00 8.20 -11 -13 1 3.10 8.40 11 -13 -1 5.00 1.90 -11 13 -1 -11.90 8.00 11 13 -2 194.58 15.10 -11 -13 -2 180.78 15.50 -11 13 2 216.18 13.70 -11 -13 -2 187.68 16.00 11 -13 2 186.08 9.10 -11 -13 -2 201.78 14.60 11 13 -2 194.18 12.80 11 -13 2 198.48 12.00 11 -13 2 214.98 13.60 11 13 2 164.98 16.00 -11 13 -2 199.58 12.60 -11 -13 2 193.78 15.30 -11 13 -2 185.98 10.50 -11 13 -2 207.48 15.60 -11 13 -2 201.68 7.40 11 13 2 192.68 14.80 -11 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32.90 13.80 15 13 -5 28.40 10.90 15 -13 5 23.30 11.80 15 13 5 36.20 14.10 -15 13 -5 31.60 13.00 -15 -13 5 31.70 13.20 -15 -13 5 42.30 14.00 15 13 5 47.90 12.30 -15 13 -5 32.00 9.40 -15 -13 5 50.89 13.20 15 -13 6 6.80 12.30 -15 -13 -6 -18.00 14.30 16 13 0 112.19 13.50 16 13 0 119.49 13.40 -16 -13 0 133.79 14.30 -16 -13 0 144.79 14.60 -16 13 0 140.29 13.20 16 -13 0 161.98 14.10 -16 -13 0 158.28 17.40 -16 -13 -1 17.90 11.20 -16 13 1 0.90 9.30 -16 -13 -1 -0.50 19.00 16 13 -1 -0.30 10.70 16 13 -1 16.80 11.40 16 -13 1 10.10 10.10 -16 -13 -1 -0.20 11.90 16 13 1 19.20 11.60 16 13 1 14.40 10.50 -16 -13 1 -4.10 13.00 -16 -13 1 9.70 12.00 -16 -13 1 -1.60 11.00 16 -13 -1 5.10 8.70 -16 13 -1 -1.60 10.80 16 -13 2 87.39 11.20 -16 -13 -2 56.89 15.20 -16 13 2 87.99 14.00 -16 -13 -2 78.29 13.80 -16 -13 -2 80.99 12.40 16 13 -2 93.79 13.30 16 13 -2 80.69 12.20 -16 -13 2 83.89 13.00 -16 -13 2 68.89 16.20 -16 13 -2 72.49 12.60 16 13 2 84.99 12.90 -16 -13 2 63.19 14.30 16 13 2 80.79 14.90 16 -13 -2 64.79 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39.10 14.40 8 14 9 44.40 13.10 -8 14 -9 57.79 15.10 -8 14 -9 48.30 14.00 -8 -14 9 32.60 15.60 -8 -14 9 57.39 13.70 9 14 0 1.90 7.80 9 -14 0 -2.70 6.60 9 -14 0 2.60 3.90 -9 14 0 7.70 7.60 -9 -14 0 -2.50 7.80 9 14 0 1.10 8.10 -9 -14 0 6.50 7.80 -9 -14 0 -1.30 8.30 -9 -14 -1 0.10 7.90 -9 -14 -1 -4.80 5.70 9 14 -1 10.10 8.20 9 14 -1 6.50 7.80 9 -14 1 -3.50 2.90 9 -14 1 -1.80 2.80 9 -14 1 -1.70 6.80 -9 14 1 14.40 7.40 -9 -14 -1 5.80 8.40 9 -14 1 -0.70 4.60 9 14 1 -9.60 7.60 9 -14 -1 4.90 3.20 -9 -14 1 10.70 7.90 -9 -14 1 9.40 8.30 -9 -14 1 -9.40 7.40 -9 14 -1 -3.10 2.30 9 14 1 11.70 7.90 9 -14 -1 4.50 6.20 -9 14 -1 1.10 2.20 -9 14 -1 -3.10 7.60 9 14 -2 1.00 8.30 9 -14 2 -1.00 6.60 9 -14 2 -0.50 5.50 -9 -14 -2 -12.20 8.30 -9 -14 -2 4.10 7.60 -9 -14 -2 -0.70 8.20 9 -14 2 -1.20 3.20 9 14 -2 -7.70 7.40 -9 14 -2 -1.30 3.70 -9 14 -2 -1.10 2.90 -9 14 -2 -1.70 4.20 9 14 2 -5.00 7.80 -9 -14 2 2.20 8.00 9 14 2 -6.60 8.20 -9 14 -2 2.00 8.30 -9 14 -2 2.80 3.30 9 -14 -2 3.70 6.00 -9 14 -2 -1.90 3.50 -9 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11.10 6.60 -9 -14 5 11.10 10.30 -9 14 -5 -0.50 7.30 9 14 5 16.10 10.40 -9 14 -5 13.80 11.60 -9 -14 5 6.50 15.50 9 14 5 -2.50 9.40 -9 14 -5 5.80 7.10 9 -14 -5 3.70 6.70 9 -14 -5 4.30 2.90 9 -14 6 66.39 8.80 9 14 -6 71.99 11.00 -9 -14 -6 85.19 13.20 9 14 -6 56.69 11.60 -9 -14 -6 89.79 11.40 9 -14 6 98.69 11.00 -9 -14 -6 92.19 12.90 -9 -14 6 58.99 12.60 -9 14 -6 87.39 10.90 9 14 6 94.49 11.50 -9 -14 6 77.99 11.80 -9 14 -6 86.09 12.20 -9 -14 6 81.59 12.00 -9 -14 6 122.39 12.40 9 14 6 77.49 12.20 -9 14 -6 87.39 9.60 9 -14 7 36.60 9.00 -9 -14 -7 42.50 10.80 9 -14 7 38.70 11.00 9 14 -7 48.10 13.30 -9 -14 -7 33.50 11.70 -9 -14 -7 27.50 13.00 9 14 -7 24.20 10.70 9 14 7 56.69 12.80 -9 14 -7 19.00 11.20 -9 -14 7 49.90 13.20 -9 14 -7 48.80 10.20 -9 -14 7 42.50 8.60 9 14 7 57.69 11.80 -9 14 -7 26.10 12.00 -9 -14 7 39.20 11.40 -9 -14 -8 27.20 13.10 9 -14 8 36.50 12.00 9 14 -8 20.40 10.80 -9 -14 -8 27.10 14.00 9 14 -8 37.50 14.20 -9 -14 -8 50.89 11.80 9 -14 8 34.00 10.10 -9 -14 8 35.00 8.60 9 14 8 36.20 13.40 -9 -14 8 27.70 12.30 -9 -14 8 14.00 13.70 9 14 8 41.50 12.00 -9 14 -8 32.10 12.80 -9 14 -8 31.90 13.10 -10 14 0 409.86 18.60 10 -14 0 382.66 14.00 -10 -14 0 354.96 19.10 10 14 0 362.86 19.50 10 -14 0 373.96 16.90 10 14 0 414.26 18.90 -10 -14 0 410.86 19.40 -10 -14 0 421.66 19.40 -10 14 1 345.97 16.50 10 14 -1 288.47 17.50 10 -14 1 279.67 9.90 10 14 -1 324.97 17.30 10 -14 1 298.27 15.30 -10 -14 -1 319.77 17.00 -10 -14 -1 330.87 17.70 10 -14 1 290.97 10.10 -10 -14 -1 303.47 17.40 10 -14 1 316.17 13.20 10 14 1 303.07 16.70 -10 -14 1 301.97 17.30 -10 14 -1 311.17 17.10 -10 -14 1 302.07 17.50 -10 -14 1 327.67 17.80 10 -14 -1 306.87 14.70 10 14 1 279.17 17.70 -10 -14 -2 350.86 17.80 10 14 -2 363.36 18.30 10 -14 2 336.77 16.60 -10 -14 -2 327.77 18.40 10 -14 2 319.87 12.50 -10 -14 -2 340.07 19.10 10 -14 2 347.87 11.60 10 -14 2 320.97 15.00 10 14 -2 323.37 18.30 -10 -14 2 336.97 18.60 -10 14 -2 338.37 11.70 10 14 2 369.66 17.80 10 14 2 314.67 19.00 -10 14 -2 353.26 13.10 -10 14 -2 325.57 18.20 10 -14 -2 356.36 15.40 -10 -14 2 345.27 18.10 -10 14 -2 322.97 10.00 -10 -14 2 366.96 18.70 -10 14 -2 343.27 12.90 10 -14 3 -3.50 4.50 -10 -14 -3 4.70 8.20 10 14 -3 -1.80 9.10 10 -14 3 5.60 8.20 -10 -14 -3 -7.10 8.90 10 14 -3 0.80 8.50 -10 -14 -3 -15.30 8.80 10 -14 3 -3.60 5.30 10 14 3 -1.40 8.60 10 -14 -3 -9.70 5.70 -10 14 -3 3.00 6.80 -10 14 -3 -1.50 5.20 -10 -14 3 -2.10 6.90 -10 -14 3 -0.10 8.10 -10 14 -3 -2.90 4.40 -10 14 -3 0.60 4.50 -10 14 -3 4.10 3.90 -10 -14 3 -9.10 8.70 -10 14 -3 -6.70 4.70 10 14 3 -8.30 9.10 -10 14 -3 -6.40 3.70 10 14 -4 114.19 11.20 -10 -14 -4 100.69 11.80 -10 -14 -4 82.59 12.30 10 -14 4 122.79 13.30 10 -14 4 95.79 10.20 10 -14 4 76.99 8.20 -10 -14 -4 97.19 10.20 -10 -14 4 103.89 11.80 10 14 4 97.69 11.70 -10 -14 4 139.39 14.30 -10 14 -4 98.09 11.00 10 -14 -4 125.39 11.10 -10 -14 4 98.09 11.20 -10 14 -4 159.38 14.90 -10 14 -4 111.89 10.70 -10 -14 -5 66.49 10.20 10 14 -5 67.59 12.00 10 -14 5 76.49 10.20 -10 -14 -5 74.59 12.00 10 -14 5 71.39 8.30 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12.20 -10 14 -8 38.90 13.50 -10 -14 8 20.10 14.00 10 14 8 35.50 14.50 10 14 8 44.60 13.00 -10 -14 8 25.70 13.10 -10 14 -8 33.40 13.70 -11 -14 0 6.70 9.00 -11 -14 0 6.50 6.70 11 -14 0 1.70 3.70 11 14 0 2.40 8.80 11 14 0 -2.40 8.40 -11 -14 0 8.60 9.50 -11 14 0 -3.00 8.20 11 -14 0 2.10 7.60 11 -14 1 7.30 4.80 -11 14 1 7.60 8.00 11 -14 1 4.80 1.80 -11 -14 -1 8.70 9.70 11 14 -1 14.50 9.40 11 -14 1 -1.80 7.20 11 -14 1 5.10 1.70 -11 -14 -1 27.10 8.60 11 14 -1 16.60 8.40 -11 -14 -1 3.70 9.00 11 -14 -1 10.20 7.50 -11 14 -1 13.10 8.60 11 -14 -1 13.30 2.30 -11 -14 1 13.70 8.90 11 14 1 7.50 8.90 -11 -14 1 -2.40 8.80 11 14 1 10.90 9.30 -11 -14 1 5.80 9.50 11 -14 2 -4.90 5.50 11 -14 2 -2.50 3.80 11 14 -2 2.50 8.00 -11 -14 -2 3.50 9.20 -11 -14 -2 3.70 6.60 11 -14 2 -11.00 7.70 11 14 -2 3.30 8.50 -11 -14 -2 7.70 9.20 11 14 2 -10.70 9.20 -11 -14 2 11.20 9.20 -11 -14 2 5.20 9.10 11 14 2 15.90 9.10 -11 14 -2 2.60 2.50 -11 14 -2 1.60 2.50 11 -14 -2 0.90 6.80 -11 14 -2 2.60 8.80 -11 -14 2 9.40 9.60 -11 -14 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459.85 21.70 12 -14 -1 447.76 18.50 12 14 1 411.46 29.10 -12 14 -1 446.76 21.00 12 14 -2 22.40 12.80 12 14 -2 6.80 9.20 -12 -14 -2 2.50 10.80 -12 -14 -2 10.50 10.70 -12 14 2 12.00 8.30 12 -14 2 11.10 8.20 -12 14 -2 15.30 3.10 -12 14 -2 -7.40 14.40 12 14 2 -4.70 15.60 -12 -14 2 1.70 10.00 12 14 2 11.50 11.70 -12 14 -2 6.60 6.90 12 -14 -2 10.60 7.30 -12 -14 -3 -8.10 9.30 -12 -14 -3 2.70 9.20 -12 -14 -3 -11.40 10.00 12 -14 3 7.20 9.00 12 14 -3 4.70 15.40 12 14 -3 -11.90 9.90 -12 -14 3 -8.60 9.20 -12 14 -3 1.40 4.00 -12 14 -3 -8.30 9.60 12 -14 -3 -6.50 6.80 -12 -14 3 -3.80 10.10 -12 -14 3 6.80 10.20 12 14 3 17.10 9.40 -12 14 -3 -2.90 5.30 12 14 3 -9.50 9.50 12 -14 4 -6.20 8.90 12 14 -4 -0.60 10.20 -12 -14 -4 12.10 9.60 12 -14 4 4.80 5.90 12 14 -4 -9.50 9.20 -12 -14 -4 -4.70 10.50 -12 -14 -4 -0.30 11.10 -12 14 -4 4.90 9.90 12 14 4 2.60 9.80 -12 -14 4 -1.60 10.50 12 14 4 -7.60 9.80 -12 14 -4 -6.50 5.80 12 -14 -4 -2.50 7.00 -12 14 -4 2.30 6.60 -12 -14 4 -8.60 9.40 -12 -14 4 -6.70 10.30 -12 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162.78 17.80 -14 14 0 179.18 19.40 -14 -14 0 195.68 18.10 14 14 0 183.88 18.40 -14 -14 -1 36.50 10.70 14 -14 1 35.60 9.60 14 14 -1 55.19 11.30 -14 -14 -1 33.20 11.40 -14 -14 -1 37.70 12.00 14 14 -1 22.80 10.00 -14 14 1 40.60 10.00 -14 -14 1 40.30 11.40 14 14 1 37.60 10.70 -14 -14 1 38.10 11.10 -14 -14 1 22.50 11.50 14 14 1 30.40 11.00 14 -14 -1 36.90 8.80 -14 14 -1 17.90 10.30 -14 14 2 109.29 11.20 14 14 -2 121.29 13.30 -14 -14 -2 93.89 13.00 -14 -14 -2 110.69 12.50 -14 -14 -2 122.99 14.40 14 14 -2 116.99 12.90 14 14 2 125.29 13.00 14 14 2 100.29 13.30 -14 14 -2 116.79 13.40 -14 -14 2 112.89 13.80 14 -14 -2 113.09 10.50 -14 -14 2 131.89 13.80 -14 -14 2 107.09 13.40 14 14 -3 -5.10 11.10 -14 -14 -3 1.00 11.40 14 -14 3 4.70 9.50 -14 -14 -3 24.10 10.50 -14 -14 -3 -8.90 11.20 14 14 -3 3.80 10.10 14 14 3 14.30 10.50 14 14 3 -1.80 10.90 -14 -14 3 9.20 11.10 -14 -14 3 -10.00 10.70 -14 -14 3 -7.60 10.30 14 -14 -3 6.60 7.90 -14 14 -3 25.90 11.40 -14 -14 -4 22.20 15.60 14 14 -4 33.30 9.70 -14 -14 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32.40 12.20 -15 14 -4 43.60 13.20 -15 -14 4 36.00 12.80 -15 -14 -5 59.59 16.10 -15 -14 -5 95.29 13.30 15 14 -5 75.39 14.60 15 14 -5 71.09 12.70 15 -14 5 86.99 13.80 -15 -14 -5 62.39 15.30 -15 -14 5 87.79 14.50 -15 -14 5 57.99 14.20 -15 -14 5 69.29 14.40 15 14 5 62.39 12.50 -15 14 -5 76.49 13.80 15 14 5 69.19 15.30 -16 14 0 51.89 11.50 -16 -14 0 43.70 12.60 16 14 0 61.89 12.00 16 -14 0 49.99 10.80 16 14 0 47.00 19.30 -16 -14 0 51.69 13.40 -16 -14 0 28.10 16.20 16 -14 1 80.19 12.00 -16 -14 -1 69.79 12.90 16 14 -1 63.49 14.50 -16 -14 -1 43.30 13.50 16 14 -1 68.29 12.10 -16 14 1 74.59 11.20 -16 -14 -1 44.30 14.10 16 14 1 73.09 12.80 -16 -14 1 70.89 13.10 16 -14 -1 61.69 10.50 16 14 1 58.39 16.50 -16 -14 1 85.29 13.90 -16 -14 1 55.29 16.30 -16 14 -1 93.09 12.60 -16 -14 -2 -19.80 12.30 -16 -14 -2 18.60 11.70 16 14 -2 6.20 11.60 16 -14 2 3.90 10.70 -16 -14 -2 11.80 11.70 -16 14 2 14.60 9.90 16 -14 -2 -0.30 8.90 16 14 2 -10.30 12.00 -16 14 -2 7.00 11.70 -16 -14 2 -2.20 12.10 -16 -14 2 7.20 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10.90 -7 15 -6 52.99 11.20 7 -15 7 94.29 11.70 -7 -15 -7 59.19 10.70 7 15 -7 75.39 11.40 -7 -15 -7 58.69 12.20 7 15 -7 80.99 13.30 -7 15 7 80.89 8.90 7 -15 7 99.49 10.60 -7 -15 -7 71.69 13.10 -7 15 -7 70.59 12.90 -7 15 -7 73.89 10.90 -7 -15 7 76.09 9.70 -7 -15 7 70.09 13.50 -7 -15 7 95.69 12.20 7 15 7 44.90 11.90 -7 15 -7 68.39 12.50 7 -15 -7 75.29 8.50 7 15 7 92.29 12.00 7 -15 8 8.50 9.20 -7 15 8 11.50 8.50 -7 -15 -8 -1.60 11.90 7 15 -8 -1.20 13.20 -7 -15 -8 -11.20 12.20 7 -15 8 7.00 11.40 7 15 -8 4.20 11.20 -7 -15 -8 2.70 10.00 7 15 8 7.60 12.50 7 15 8 20.20 11.70 7 -15 -8 -0.60 8.60 -7 -15 8 13.40 9.20 -7 -15 8 11.30 11.80 -7 15 -8 10.50 10.40 -7 -15 8 -6.60 13.50 -7 15 -8 0.40 11.40 -7 15 -8 18.60 13.00 -8 -15 0 257.27 15.80 -8 15 0 229.68 7.60 -8 15 0 241.38 8.00 8 -15 0 229.18 7.30 -8 15 0 271.07 15.30 -8 15 0 250.37 12.00 -8 15 0 237.18 8.00 8 15 0 255.47 15.30 -8 -15 0 237.38 15.50 -8 -15 0 262.17 15.40 8 -15 0 229.68 7.30 8 -15 0 258.57 11.30 8 15 0 246.08 16.20 -8 15 0 231.58 7.60 8 -15 0 233.98 13.80 8 15 -1 732.73 26.20 -8 -15 -1 701.93 25.90 -8 -15 -1 719.23 26.40 -8 -15 -1 710.13 26.70 -8 15 1 705.03 22.40 8 15 -1 699.23 26.60 8 -15 1 694.13 21.40 8 -15 1 686.23 20.20 8 -15 1 656.83 21.20 8 -15 1 710.93 25.10 8 -15 1 734.63 23.50 -8 15 -1 681.23 20.20 -8 15 -1 680.73 21.00 -8 15 -1 661.73 20.50 8 15 1 696.03 26.70 -8 15 -1 729.13 26.00 8 15 1 713.93 25.80 -8 -15 1 670.63 26.00 -8 -15 1 720.33 26.50 8 -15 -1 709.63 24.60 -8 -15 1 679.03 26.30 8 -15 -1 731.03 22.00 -8 15 -1 692.93 20.70 -8 15 -1 658.83 23.50 -8 15 -1 684.83 24.00 -8 -15 -2 248.18 14.60 8 -15 2 219.58 14.00 8 -15 2 220.88 9.30 8 15 -2 209.08 15.50 -8 -15 -2 175.78 15.40 -8 -15 -2 212.78 15.00 8 -15 2 222.28 10.10 8 -15 2 213.38 12.50 -8 15 2 223.48 9.50 8 15 -2 215.58 15.40 -8 15 2 195.88 7.00 8 15 2 224.78 14.70 8 15 2 226.48 16.20 -8 15 -2 218.98 9.30 -8 -15 2 197.88 14.80 -8 -15 2 191.98 15.30 -8 15 -2 210.58 9.30 -8 -15 2 199.08 15.70 8 -15 -2 213.08 13.70 -8 15 -2 215.18 8.70 -8 15 -2 226.48 10.00 -8 15 -2 214.28 15.10 8 -15 -2 210.78 8.70 -8 -15 -3 4.50 8.50 8 -15 3 6.00 4.80 8 15 -3 6.20 8.30 8 -15 3 1.20 5.40 -8 -15 -3 2.50 7.10 -8 15 3 -0.10 2.90 8 -15 3 6.60 7.90 8 15 -3 3.40 8.40 -8 15 3 9.40 3.00 -8 -15 -3 -9.50 9.00 -8 15 -3 2.10 5.40 -8 15 -3 7.40 4.70 -8 15 -3 14.70 8.50 -8 -15 3 1.60 7.00 -8 15 -3 7.20 4.80 -8 -15 3 13.30 9.00 -8 -15 3 4.40 7.90 8 15 3 7.20 8.90 8 15 3 -3.90 8.00 -8 15 -3 11.50 5.20 -8 15 -3 6.70 4.40 -8 15 -3 2.40 5.10 8 -15 4 18.70 8.60 -8 -15 -4 9.70 8.00 -8 -15 -4 5.00 9.90 8 -15 4 18.40 5.90 -8 15 4 15.90 2.30 8 15 -4 18.00 9.70 8 15 -4 13.40 8.80 -8 -15 -4 8.90 8.80 8 15 4 6.20 8.80 -8 15 -4 14.90 5.70 -8 15 -4 21.50 7.50 8 -15 -4 15.50 4.70 -8 -15 4 20.40 9.80 -8 15 -4 9.50 6.50 -8 -15 4 3.30 8.40 8 -15 -4 14.50 2.80 8 15 4 1.00 7.10 -8 15 -4 12.90 5.70 -8 -15 4 10.50 9.10 -8 15 -4 24.50 6.40 -8 15 -4 13.10 5.70 -8 15 -4 16.80 6.30 8 -15 5 457.75 20.30 -8 -15 -5 480.95 33.30 -8 15 5 479.15 16.80 -8 -15 -5 484.15 21.30 -8 -15 -5 501.55 23.00 8 -15 5 477.75 19.40 8 15 -5 501.15 23.10 8 15 5 472.25 21.70 -8 15 -5 523.15 24.00 -8 15 -5 477.35 19.50 8 -15 -5 496.25 16.10 8 15 5 447.46 22.90 -8 15 -5 503.25 21.10 -8 -15 5 499.95 24.20 -8 -15 5 470.75 25.70 -8 -15 -6 118.29 11.80 8 -15 6 148.29 15.30 8 -15 6 137.19 13.50 -8 15 6 118.49 10.00 8 15 -6 111.99 12.30 8 15 -6 109.39 11.60 -8 -15 -6 115.89 14.10 8 -15 -6 141.49 9.70 -8 -15 6 115.69 13.70 8 15 6 117.89 12.10 -8 -15 6 94.29 11.90 -8 -15 6 98.29 10.10 8 15 6 95.29 13.10 -8 -15 6 105.79 12.50 -8 15 -6 114.39 11.70 -8 15 -6 104.59 10.50 -8 15 -6 126.09 13.20 8 15 -7 196.88 17.80 8 -15 7 190.38 15.70 8 -15 7 246.98 20.20 -8 -15 -7 197.08 17.40 -8 -15 -7 217.08 19.20 -8 -15 -7 164.58 16.80 8 15 -7 180.38 16.70 8 15 7 171.28 16.10 8 15 7 242.08 18.30 -8 15 -7 202.18 19.90 -8 15 -7 200.58 19.40 -8 -15 7 192.68 20.30 -8 -15 7 171.08 16.40 -8 -15 7 204.48 14.40 -8 15 -7 176.18 15.20 8 15 -8 76.99 14.50 -8 -15 -8 50.69 16.80 8 -15 8 46.40 10.30 -8 -15 -8 71.69 12.00 8 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58.89 12.10 -9 15 -5 53.59 8.30 9 15 5 46.10 10.80 -9 15 -5 49.99 11.50 9 15 5 61.69 10.80 -9 -15 5 39.50 8.70 -9 -15 5 29.60 10.50 9 -15 -5 40.60 7.90 -9 15 -5 43.10 9.00 9 -15 6 24.20 10.00 -9 -15 -6 10.30 11.10 -9 -15 -6 -4.50 11.50 9 -15 6 1.00 8.00 9 15 -6 6.90 10.00 9 15 -6 8.10 11.70 -9 -15 -6 25.00 9.70 -9 15 -6 13.70 11.30 -9 15 -6 17.40 8.70 -9 -15 6 26.00 10.80 9 15 6 25.70 10.80 -9 -15 6 11.10 8.50 9 15 6 20.90 11.70 -9 15 -6 -0.10 9.50 -9 -15 6 15.60 10.90 -9 -15 6 15.30 11.40 -9 -15 -7 65.89 11.40 9 -15 7 70.19 12.20 -9 -15 -7 58.99 13.10 -9 -15 -7 66.69 17.80 9 -15 7 55.39 9.90 9 15 -7 67.29 13.80 -9 -15 7 67.29 9.60 -9 -15 7 48.60 13.90 -9 15 -7 65.69 20.70 -9 -15 7 71.89 12.00 -9 15 -7 62.19 13.80 -9 15 -7 75.69 11.10 9 15 7 58.49 12.30 9 15 7 61.19 23.00 9 15 -8 3.20 14.00 9 15 -8 -1.50 11.40 9 -15 8 20.80 12.30 9 -15 8 15.70 10.60 -9 -15 -8 -17.00 13.40 -9 -15 -8 4.00 13.40 -9 -15 -8 -1.10 10.80 -9 15 -8 4.50 11.10 9 15 8 24.90 13.30 -9 15 -8 -11.50 11.20 9 15 8 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6.30 10 15 2 79.19 11.10 10 -15 3 22.90 8.90 -10 -15 -3 17.40 8.90 10 15 -3 13.30 9.30 -10 -15 -3 12.60 9.50 -10 -15 -3 -5.50 10.10 10 -15 3 18.90 4.90 -10 15 -3 13.10 4.10 -10 -15 3 15.40 11.10 -10 -15 3 6.60 9.40 10 15 3 9.90 10.20 10 -15 -3 10.40 7.70 -10 15 -3 18.80 5.30 -10 15 -3 14.00 5.50 -10 -15 -4 100.79 12.80 -10 -15 -4 92.79 20.30 -10 -15 -4 117.99 11.60 10 -15 4 97.29 10.40 10 15 -4 90.79 11.50 10 15 -4 112.79 11.20 10 -15 4 102.99 11.30 -10 15 -4 107.09 12.50 -10 15 -4 130.19 9.10 -10 -15 4 108.49 13.30 -10 -15 4 103.49 12.20 -10 15 -4 109.69 11.30 -10 -15 4 122.99 12.60 10 -15 -4 101.09 9.40 -10 15 -4 107.39 10.90 10 15 4 101.59 12.40 10 15 4 107.59 11.90 10 15 -5 252.47 18.30 10 15 -5 290.17 19.60 -10 -15 -5 251.47 17.00 -10 -15 -5 252.37 20.40 -10 -15 -5 276.97 19.70 10 -15 5 240.18 15.00 10 -15 5 277.97 17.60 10 -15 -5 252.17 15.30 10 15 5 271.77 18.30 -10 15 -5 278.67 19.90 10 15 5 240.58 20.30 -10 15 -5 275.07 15.30 -10 -15 5 249.48 18.60 -10 -15 5 273.77 18.90 -10 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22.80 8.10 11 15 1 33.00 13.40 -11 -15 1 12.60 9.80 11 15 1 7.30 9.50 -11 -15 1 8.10 10.90 -11 -15 1 15.40 9.80 -11 15 -1 4.70 8.50 11 -15 2 -18.00 10.10 11 15 -2 -0.10 7.70 -11 -15 -2 -10.30 9.30 11 15 -2 -0.40 9.10 11 -15 2 11.80 8.30 11 15 2 4.60 7.30 -11 15 -2 -0.10 2.30 -11 -15 2 -4.40 14.30 11 -15 -2 -3.60 7.00 -11 -15 2 1.70 11.90 -11 -15 -3 45.80 9.80 11 15 -3 37.60 12.80 -11 -15 -3 49.50 11.90 11 -15 3 47.70 5.50 11 15 -3 51.19 9.20 -11 -15 3 40.50 11.30 -11 15 -3 45.50 10.90 -11 -15 3 56.99 11.40 -11 -15 3 54.19 10.80 11 15 3 38.20 9.80 11 15 3 54.89 11.40 11 -15 -3 53.59 8.50 -11 15 -3 44.10 6.30 11 -15 4 71.29 7.40 -11 -15 -4 86.09 11.00 -11 -15 -4 60.19 12.30 11 15 -4 112.59 13.20 11 15 -4 78.59 11.40 11 -15 4 90.69 11.40 -11 -15 -4 76.89 12.00 11 15 4 78.79 12.70 11 15 4 74.69 11.60 -11 15 -4 79.29 12.20 -11 -15 4 64.09 11.60 -11 15 -4 89.59 8.30 -11 15 -4 86.49 8.40 11 -15 -4 81.39 9.40 -11 15 -4 81.89 7.60 -11 -15 4 94.39 12.80 -11 -15 4 86.59 12.10 -11 -15 -5 -12.20 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