# Electronic Supplementary Material (ESI) for Chemical Science. # This journal is © The Royal Society of Chemistry 2021 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_glo9476 _database_code_depnum_ccdc_archive 'CCDC 2006231' loop_ _audit_author_name _audit_author_address 'Constantin G. Daniliuc' ;Organisch Chemisches Institut WWU University of Muenster Germany ; _audit_update_record ; 2020-05-27 deposited with the CCDC. 2021-03-04 downloaded from the CCDC. ; _audit_creation_method 'APEX3 v2016.1-0' _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_sum 'C10 H18 N2 O' _chemical_formula_iupac ? _chemical_formula_weight 182.26 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.8352(5) _cell_length_b 9.3209(4) _cell_length_c 11.4836(6) _cell_angle_alpha 90 _cell_angle_beta 108.743(3) _cell_angle_gamma 90 _cell_volume 996.91(9) _cell_formula_units_Z 4 _cell_measurement_reflns_used 3813 _cell_measurement_theta_min 5.1655 _cell_measurement_theta_max 66.3913 _cell_measurement_temperature 100.(2) _exptl_crystal_description prism _exptl_crystal_colour colourless _exptl_crystal_size_max 0.180 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.080 _exptl_crystal_density_diffrn 1.214 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 400 _exptl_absorpt_coefficient_mu 0.626 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Bruker AXS (2014). SADABS, Version 2014/5, Bruker AXS Inc., Madison, Wisconsin, USA. ; _exptl_absorpt_correction_T_min 0.80 _exptl_absorpt_correction_T_max 0.95 _exptl_special_details ; ; _diffrn_ambient_temperature 100.(2) _diffrn_source 'fine-focus sealed tube' _diffrn_source_type 'fine-focus sealed tube' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Kappa CCD APEXII' _diffrn_measurement_method 'phi / omega scans' _diffrn_detector_area_resol_mean 8.3333 _diffrn_reflns_number 14466 _diffrn_reflns_av_R_equivalents 0.0643 _diffrn_reflns_av_unetI/netI 0.0335 _diffrn_reflns_theta_min 5.17 _diffrn_reflns_theta_max 66.72 _diffrn_reflns_theta_full 66.72 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measured_fraction_theta_full 0.993 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 13 _refine_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. The hydrogen at N1 atom was refined freely. ; _reflns_number_total 1752 _reflns_number_gt 1334 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0591 _refine_ls_R_factor_gt 0.0410 _refine_ls_wR_factor_gt 0.0930 _refine_ls_wR_factor_ref 0.1017 _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_restrained_S_all 1.054 _refine_ls_number_reflns 1752 _refine_ls_number_parameters 124 _refine_ls_number_restraints 0 _refine_ls_number_constraints ? _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0420P)^2^+0.3186P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.171 _refine_diff_density_min -0.195 _refine_ls_extinction_method none _refine_ls_extinction_coef ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection 'APEX3 v2016.1-0 (Bruker AXS Inc., 2016)' _computing_cell_refinement 'SAINT V8.37A (Bruker AXS Inc., 2015)' _computing_data_reduction 'SAINT V8.37A (Bruker AXS Inc., 2015)' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'APEX3 v2016.1-0 (Bruker AXS Inc., 2016)' _computing_publication_material 'APEX3 v2016.1-0 (Bruker AXS Inc., 2016)' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.65297(12) 0.26082(12) 0.16985(10) 0.0267(3) Uani d . . . 1 . . N N1 0.62143(15) 0.57753(15) 0.40879(13) 0.0238(3) Uani d . . . 1 . . H H1 0.6605(19) 0.644(2) 0.3777(16) 0.023(5) Uiso d . . . 1 . . C C2 0.72191(17) 0.45950(18) 0.45671(14) 0.0231(4) Uani d . . . 1 . . H H2 0.6716 0.3834 0.4887 0.028 Uiso calc U . R 1 . . C C3 0.76696(17) 0.39591(18) 0.35198(14) 0.0232(4) Uani d . . . 1 . . H H3A 0.8284 0.4661 0.3277 0.028 Uiso calc U . R 1 . . H H3B 0.8252 0.3088 0.3822 0.028 Uiso calc U . R 1 . . C C4 0.64227(18) 0.35721(17) 0.24053(15) 0.0230(4) Uani d . . . 1 . . N N5 0.52015(14) 0.43501(15) 0.22081(12) 0.0227(3) Uani d . . . 1 . . C C6 0.39109(17) 0.39286(18) 0.12023(15) 0.0258(4) Uani d . . . 1 . . H H6A 0.3295 0.3325 0.1536 0.031 Uiso calc U . R 1 . . H H6B 0.4197 0.3347 0.0598 0.031 Uiso calc U . R 1 . . C C7 0.30577(18) 0.52228(19) 0.05565(14) 0.0261(4) Uani d . . . 1 . . H H7 0.3677 0.5789 0.0183 0.031 Uiso calc U . R 1 . . C C8 0.26969(18) 0.61702(19) 0.14992(15) 0.0266(4) Uani d . . . 1 . . H H8A 0.2194 0.7045 0.109 0.032 Uiso calc U . R 1 . . H H8B 0.2045 0.5646 0.1852 0.032 Uiso calc U . R 1 . . C C9 0.40569(18) 0.65943(18) 0.25258(15) 0.0267(4) Uani d . . . 1 . . H H9A 0.4658 0.7203 0.218 0.032 Uiso calc U . R 1 . . H H9B 0.3791 0.717 0.3144 0.032 Uiso calc U . R 1 . . C C10 0.49279(17) 0.53046(17) 0.31553(14) 0.0230(4) Uani d . . . 1 . . H H10 0.4339 0.4755 0.3569 0.028 Uiso calc U . R 1 . . C C11 0.84928(18) 0.51222(19) 0.56178(14) 0.0260(4) Uani d . . . 1 . . H H11A 0.8958 0.5915 0.5332 0.039 Uiso calc U . R 1 . . H H11B 0.918 0.4336 0.591 0.039 Uiso calc U . R 1 . . H H11C 0.8164 0.5456 0.6291 0.039 Uiso calc U . R 1 . . C C12 0.17147(19) 0.4752(2) -0.04780(16) 0.0306(4) Uani d . . . 1 . . H H12A 0.1119 0.4147 -0.0138 0.046 Uiso calc U . R 1 . . H H12B 0.1998 0.4208 -0.1093 0.046 Uiso calc U . R 1 . . H H12C 0.1166 0.5601 -0.0866 0.046 Uiso calc U . R 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0296(7) 0.0236(6) 0.0263(6) 0.0026(5) 0.0082(5) -0.0032(5) N1 0.0223(8) 0.0220(8) 0.0247(7) -0.0001(6) 0.0043(6) -0.0006(6) C2 0.0241(9) 0.0219(9) 0.0238(8) 0.0003(7) 0.0083(7) 0.0001(7) C3 0.0232(9) 0.0210(9) 0.0240(9) 0.0018(7) 0.0057(7) 0.0004(7) C4 0.0262(9) 0.0202(9) 0.0240(8) -0.0010(7) 0.0098(7) 0.0019(7) N5 0.0217(7) 0.0231(7) 0.0219(7) 0.0007(6) 0.0053(6) -0.0034(6) C6 0.0233(9) 0.0261(9) 0.0260(9) -0.0023(7) 0.0048(7) -0.0015(7) C7 0.0250(9) 0.0283(10) 0.0232(8) -0.0007(7) 0.0051(8) 0.0017(7) C8 0.0241(9) 0.0266(9) 0.0281(9) 0.0026(7) 0.0069(8) 0.0024(7) C9 0.0276(9) 0.0245(9) 0.0279(9) 0.0025(7) 0.0087(8) -0.0016(7) C10 0.0236(9) 0.0229(9) 0.0230(8) 0.0004(7) 0.0080(7) -0.0017(7) C11 0.0272(9) 0.0261(9) 0.0232(8) -0.0002(7) 0.0062(7) 0.0005(7) C12 0.0294(10) 0.0309(10) 0.0278(9) 0.0026(8) 0.0041(8) 0.0002(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C4 . 1.2377(19) ? N1 C10 . 1.439(2) ? N1 C2 . 1.463(2) ? N1 H1 . 0.864(19) ? C2 C11 . 1.515(2) ? C2 C3 . 1.529(2) ? C2 H2 . 1.0 ? C3 C4 . 1.504(2) ? C3 H3A . 0.99 ? C3 H3B . 0.99 ? C4 N5 . 1.358(2) ? N5 C6 . 1.469(2) ? N5 C10 . 1.495(2) ? C6 C7 . 1.520(2) ? C6 H6A . 0.99 ? C6 H6B . 0.99 ? C7 C8 . 1.525(2) ? C7 C12 . 1.530(2) ? C7 H7 . 1.0 ? C8 C9 . 1.524(2) ? C8 H8A . 0.99 ? C8 H8B . 0.99 ? C9 C10 . 1.518(2) ? C9 H9A . 0.99 ? C9 H9B . 0.99 ? C10 H10 . 1.0 ? C11 H11A . 0.98 ? C11 H11B . 0.98 ? C11 H11C . 0.98 ? C12 H12A . 0.98 ? C12 H12B . 0.98 ? C12 H12C . 0.98 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C10 N1 C2 . . 112.14(13) ? C10 N1 H1 . . 108.2(11) ? C2 N1 H1 . . 111.0(12) ? N1 C2 C11 . . 109.96(13) ? N1 C2 C3 . . 109.10(13) ? C11 C2 C3 . . 112.20(14) ? N1 C2 H2 . . 108.5 ? C11 C2 H2 . . 108.5 ? C3 C2 H2 . . 108.5 ? C4 C3 C2 . . 113.53(14) ? C4 C3 H3A . . 108.9 ? C2 C3 H3A . . 108.9 ? C4 C3 H3B . . 108.9 ? C2 C3 H3B . . 108.9 ? H3A C3 H3B . . 107.7 ? O1 C4 N5 . . 122.35(15) ? O1 C4 C3 . . 120.94(15) ? N5 C4 C3 . . 116.69(14) ? C4 N5 C6 . . 118.87(14) ? C4 N5 C10 . . 123.55(13) ? C6 N5 C10 . . 114.79(13) ? N5 C6 C7 . . 111.94(14) ? N5 C6 H6A . . 109.2 ? C7 C6 H6A . . 109.2 ? N5 C6 H6B . . 109.2 ? C7 C6 H6B . . 109.2 ? H6A C6 H6B . . 107.9 ? C6 C7 C8 . . 109.34(13) ? C6 C7 C12 . . 110.79(14) ? C8 C7 C12 . . 112.18(14) ? C6 C7 H7 . . 108.1 ? C8 C7 H7 . . 108.1 ? C12 C7 H7 . . 108.1 ? C9 C8 C7 . . 110.66(14) ? C9 C8 H8A . . 109.5 ? C7 C8 H8A . . 109.5 ? C9 C8 H8B . . 109.5 ? C7 C8 H8B . . 109.5 ? H8A C8 H8B . . 108.1 ? C10 C9 C8 . . 112.57(14) ? C10 C9 H9A . . 109.1 ? C8 C9 H9A . . 109.1 ? C10 C9 H9B . . 109.1 ? C8 C9 H9B . . 109.1 ? H9A C9 H9B . . 107.8 ? N1 C10 N5 . . 113.72(13) ? N1 C10 C9 . . 109.87(13) ? N5 C10 C9 . . 109.32(13) ? N1 C10 H10 . . 107.9 ? N5 C10 H10 . . 107.9 ? C9 C10 H10 . . 107.9 ? C2 C11 H11A . . 109.5 ? C2 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C2 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C7 C12 H12A . . 109.5 ? C7 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C7 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C10 N1 C2 C11 . . . . -175.18(13) ? C10 N1 C2 C3 . . . . 61.37(17) ? N1 C2 C3 C4 . . . . -51.64(18) ? C11 C2 C3 C4 . . . . -173.74(14) ? C2 C3 C4 O1 . . . . -152.79(15) ? C2 C3 C4 N5 . . . . 28.6(2) ? O1 C4 N5 C6 . . . . 7.1(2) ? C3 C4 N5 C6 . . . . -174.24(14) ? O1 C4 N5 C10 . . . . 167.16(15) ? C3 C4 N5 C10 . . . . -14.2(2) ? C4 N5 C6 C7 . . . . -142.53(15) ? C10 N5 C6 C7 . . . . 55.74(18) ? N5 C6 C7 C8 . . . . -55.37(18) ? N5 C6 C7 C12 . . . . -179.51(14) ? C6 C7 C8 C9 . . . . 55.64(18) ? C12 C7 C8 C9 . . . . 178.97(14) ? C7 C8 C9 C10 . . . . -56.21(19) ? C2 N1 C10 N5 . . . . -46.55(19) ? C2 N1 C10 C9 . . . . -169.44(14) ? C4 N5 C10 N1 . . . . 22.9(2) ? C6 N5 C10 N1 . . . . -176.30(13) ? C4 N5 C10 C9 . . . . 146.12(15) ? C6 N5 C10 C9 . . . . -53.11(18) ? C8 C9 C10 N1 . . . . 178.34(14) ? C8 C9 C10 N5 . . . . 52.89(18) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 O1 2_655 0.864(19) 2.344(19) 3.1536(19) 156.1(16) ? _shelx_res_file ; glo9476.res created by SHELXL-2014/7 TITL glo9476.res in P2(1)/n CELL 1.54178 9.8352 9.3209 11.4836 90.000 108.743 90.000 ZERR 4.000 0.0005 0.0004 0.0006 0.000 0.003 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 40 72 8 4 SIZE 0.08 0.12 0.18 TEMP -173.150 ACTA CONF L.S. 30 BOND $H FMAP 2 PLAN 10 EQIV $1 -x+3/2, y+1/2, -z+1/2 HTAB N1 O1_$1 WGHT 0.042000 0.318600 FVAR 0.89886 O1 4 0.652966 0.260818 0.169848 11.00000 0.02958 0.02359 = 0.02632 -0.00319 0.00818 0.00259 N1 3 0.621432 0.577534 0.408791 11.00000 0.02225 0.02203 = 0.02472 -0.00062 0.00435 -0.00013 H1 2 0.660488 0.644015 0.377738 11.00000 0.02288 C2 1 0.721913 0.459498 0.456712 11.00000 0.02414 0.02186 = 0.02383 0.00015 0.00827 0.00027 AFIX 13 H2 2 0.671599 0.383424 0.488747 11.00000 -1.20000 AFIX 0 C3 1 0.766955 0.395913 0.351978 11.00000 0.02324 0.02099 = 0.02399 0.00039 0.00569 0.00176 AFIX 23 H3A 2 0.828425 0.466115 0.327666 11.00000 -1.20000 H3B 2 0.825185 0.308798 0.382218 11.00000 -1.20000 AFIX 0 C4 1 0.642271 0.357210 0.240526 11.00000 0.02615 0.02022 = 0.02396 0.00191 0.00981 -0.00096 N5 3 0.520145 0.435007 0.220809 11.00000 0.02173 0.02314 = 0.02195 -0.00340 0.00526 0.00071 C6 1 0.391088 0.392859 0.120235 11.00000 0.02326 0.02605 = 0.02597 -0.00152 0.00480 -0.00233 AFIX 23 H6A 2 0.329464 0.332518 0.153630 11.00000 -1.20000 H6B 2 0.419686 0.334690 0.059804 11.00000 -1.20000 AFIX 0 C7 1 0.305773 0.522284 0.055646 11.00000 0.02495 0.02831 = 0.02321 0.00168 0.00510 -0.00068 AFIX 13 H7 2 0.367667 0.578888 0.018344 11.00000 -1.20000 AFIX 0 C8 1 0.269686 0.617020 0.149922 11.00000 0.02410 0.02660 = 0.02810 0.00244 0.00695 0.00262 AFIX 23 H8A 2 0.219440 0.704451 0.108975 11.00000 -1.20000 H8B 2 0.204527 0.564645 0.185208 11.00000 -1.20000 AFIX 0 C9 1 0.405693 0.659432 0.252583 11.00000 0.02759 0.02454 = 0.02791 -0.00156 0.00870 0.00253 AFIX 23 H9A 2 0.465770 0.720320 0.217972 11.00000 -1.20000 H9B 2 0.379091 0.717048 0.314397 11.00000 -1.20000 AFIX 0 C10 1 0.492794 0.530465 0.315529 11.00000 0.02359 0.02290 = 0.02298 -0.00166 0.00801 0.00042 AFIX 13 H10 2 0.433921 0.475500 0.356885 11.00000 -1.20000 AFIX 0 C11 1 0.849280 0.512218 0.561776 11.00000 0.02721 0.02612 = 0.02321 0.00054 0.00621 -0.00020 AFIX 137 H11A 2 0.895832 0.591494 0.533153 11.00000 -1.50000 H11B 2 0.918015 0.433635 0.591024 11.00000 -1.50000 H11C 2 0.816384 0.545627 0.629114 11.00000 -1.50000 AFIX 0 C12 1 0.171467 0.475224 -0.047802 11.00000 0.02941 0.03091 = 0.02784 0.00023 0.00409 0.00263 AFIX 137 H12A 2 0.111914 0.414697 -0.013828 11.00000 -1.50000 H12B 2 0.199825 0.420752 -0.109272 11.00000 -1.50000 H12C 2 0.116619 0.560074 -0.086577 11.00000 -1.50000 AFIX 0 HKLF 4 REM glo9476.res in P2(1)/n REM R1 = 0.0410 for 1334 Fo > 4sig(Fo) and 0.0591 for all 1752 data REM 124 parameters refined using 0 restraints END WGHT 0.0420 0.3190 REM Highest difference peak 0.171, deepest hole -0.195, 1-sigma level 0.041 Q1 1 0.5327 0.4991 0.1617 11.00000 0.05 0.17 Q2 1 0.3895 0.5649 0.2913 11.00000 0.05 0.16 Q3 1 0.7443 0.4423 0.3993 11.00000 0.05 0.15 Q4 1 0.2959 0.5774 0.1057 11.00000 0.05 0.14 Q5 1 0.4194 0.4613 0.0421 11.00000 0.05 0.13 Q6 1 0.8810 0.4923 0.2982 11.00000 0.05 0.12 Q7 1 0.6334 0.2738 0.0881 11.00000 0.05 0.12 Q8 1 0.4335 0.2035 0.2527 11.00000 0.05 0.12 Q9 1 0.6421 0.4223 0.5558 11.00000 0.05 0.12 Q10 1 0.2751 0.4376 0.0882 11.00000 0.05 0.11 ; _shelx_res_checksum 47545 _shelx_hkl_file ; 1 0 0 8.60 2.30 1 0 0 2.50 2.20 -1 0 0 1.10 2.00 -1 0 0 2.30 2.00 -2 0 0 2524.85 80.59 -2 0 0 2370.26 77.99 2 0 0 2433.36 79.29 2 0 0 2348.76 80.39 -2 0 0 2436.26 79.39 -3 0 0 -2.40 3.60 -3 0 0 -3.90 4.30 -3 0 0 0.90 4.60 3 0 0 6.60 6.00 -4 0 0 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12.90 7 2 -10 135.79 15.90 6 -2 -10 26.30 7.90 -6 -2 10 33.20 8.90 -6 -2 10 35.00 9.40 6 -2 -10 39.40 8.00 6 -2 -10 44.30 9.00 6 2 -10 24.30 8.00 -6 2 10 10.40 8.00 6 2 -10 31.80 12.20 -5 -2 10 -7.40 9.60 5 -2 -10 -3.60 5.70 -5 -2 10 -3.00 7.80 -5 -2 10 -3.70 9.40 -5 2 10 4.50 10.70 -5 2 10 2.40 8.30 5 2 -10 10.70 6.20 -5 2 10 -8.00 7.00 5 2 -10 9.90 7.40 -4 -2 10 48.00 9.00 -4 -2 10 53.19 9.00 -4 -2 10 46.20 8.80 -4 -2 10 41.00 11.90 -4 -2 10 52.99 13.10 4 -2 -10 50.39 8.20 4 -2 -10 44.40 8.40 4 2 -10 69.49 9.60 -4 2 10 48.20 11.10 -4 2 10 32.60 12.10 -4 2 10 33.30 10.30 4 2 -10 35.40 8.70 -4 2 10 66.69 12.20 4 2 -10 57.79 8.50 -3 -2 10 8.90 8.90 -3 -2 10 13.00 5.80 3 -2 -10 3.40 5.20 3 -2 -10 -7.30 4.70 -3 -2 10 -5.50 7.20 -3 -2 10 10.00 8.80 -3 -2 10 -10.10 9.30 -3 -2 10 6.10 6.30 3 2 -10 -0.40 5.80 -3 2 10 4.80 6.90 3 2 -10 16.40 7.00 -3 2 10 11.80 8.60 3 2 -10 -2.10 5.70 -3 2 10 13.60 9.30 -3 2 10 -3.60 8.70 -2 -2 10 512.05 24.70 -2 -2 10 465.25 27.10 2 -2 -10 480.75 22.40 -2 -2 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-3 10 19.00 9.00 3 -3 -10 18.80 6.00 -3 -3 10 13.00 10.00 -3 -3 10 21.70 9.10 -3 -3 10 15.70 11.40 -3 -3 10 23.90 6.60 3 3 -10 24.60 9.90 -3 3 10 21.50 9.40 3 3 -10 18.80 6.60 -3 3 10 38.70 8.70 -3 3 10 36.80 11.50 -3 3 10 12.50 9.20 2 -3 -10 133.29 11.20 -2 -3 10 151.68 15.60 -2 -3 10 134.79 13.00 -2 -3 10 146.59 14.90 -2 -3 10 106.39 12.30 -2 -3 10 117.09 14.90 -2 -3 10 126.79 16.50 -2 3 10 146.99 19.90 -2 3 10 152.28 15.50 -2 3 10 137.59 19.00 2 3 -10 122.69 11.20 -2 3 10 142.99 13.60 -1 -3 10 61.89 12.20 -1 -3 10 53.99 9.40 -1 -3 10 68.49 13.50 1 -3 -10 92.39 8.90 -1 -3 10 81.19 12.00 -1 -3 10 71.39 11.70 -1 3 10 93.09 14.00 -1 3 10 53.69 10.90 -1 3 10 107.69 15.60 -1 3 10 76.89 10.20 1 3 -10 80.89 9.30 0 -3 10 74.89 11.10 0 -3 10 76.29 9.70 0 -3 10 56.59 10.90 0 -3 10 86.89 12.70 0 -3 10 85.09 11.10 0 3 10 85.19 15.60 0 3 10 103.89 13.30 0 3 -10 85.19 8.80 0 3 10 69.89 11.00 1 -3 10 51.59 9.30 1 -3 10 106.79 15.80 1 -3 10 92.79 11.40 1 3 10 108.09 17.20 -1 3 -10 88.09 8.60 1 3 10 80.59 13.50 1 3 10 111.09 12.80 2 -3 10 26.80 6.20 2 -3 10 21.60 9.00 2 -3 10 48.30 8.30 2 -3 10 16.30 8.20 2 3 10 46.50 9.70 2 3 10 37.90 8.10 -2 3 -10 29.60 5.70 3 -3 10 1.40 5.00 3 -3 10 -6.80 7.90 3 -3 10 -2.60 6.80 3 -3 10 4.90 4.40 -3 3 -10 7.90 4.10 4 -3 10 3.00 3.80 4 -3 10 -0.10 4.00 4 -3 10 -2.30 3.80 9 -4 -10 -0.70 4.30 -9 4 10 6.90 5.30 9 4 -10 4.60 4.60 -8 -4 10 12.80 5.90 8 -4 -10 -0.30 7.70 8 4 -10 11.30 5.50 8 4 -10 9.70 5.00 -8 4 10 11.70 4.40 -7 -4 10 25.00 9.50 7 -4 -10 10.90 8.60 7 -4 -10 22.80 7.80 -7 -4 10 24.40 9.50 7 4 -10 31.00 7.80 -7 4 10 37.80 7.40 7 4 -10 15.10 5.70 -6 -4 10 100.59 14.40 -6 -4 10 99.99 11.60 6 -4 -10 77.19 10.20 6 -4 -10 92.79 11.10 -6 4 10 106.59 13.90 6 4 -10 109.59 15.30 6 4 -10 88.29 10.40 5 -4 -10 27.20 7.20 5 -4 -10 32.60 7.70 -5 -4 10 35.30 8.90 -5 -4 10 12.50 10.40 5 4 -10 24.90 7.10 -5 4 10 21.70 9.30 5 4 -10 20.40 8.70 -5 4 10 16.10 8.40 -4 -4 10 110.29 14.70 -4 -4 10 129.09 13.90 -4 -4 10 99.49 13.70 4 -4 -10 116.99 11.30 4 4 -10 107.89 11.10 -4 4 10 120.99 14.20 -4 4 10 92.89 13.70 -4 4 10 133.39 15.10 4 4 -10 111.89 14.50 -3 -4 10 22.20 7.40 3 -4 -10 26.90 7.00 -3 -4 10 34.10 10.40 -3 -4 10 19.10 11.20 -3 -4 10 26.70 9.00 -3 4 10 25.30 9.10 -3 4 10 26.00 12.50 3 4 -10 21.30 6.90 -3 4 10 10.90 7.00 3 4 -10 30.00 10.10 -2 -4 10 6.50 6.40 -2 -4 10 8.50 10.60 -2 -4 10 -4.10 5.80 2 -4 -10 4.40 4.90 -2 -4 10 2.10 4.90 -2 -4 10 -1.40 8.50 -2 -4 10 1.90 7.80 -2 4 10 -21.00 10.60 -2 4 10 -9.20 11.30 -2 4 10 1.30 6.10 2 4 -10 -8.40 5.30 -1 -4 10 13.20 9.50 -1 -4 10 43.60 10.20 -1 -4 10 31.00 7.70 -1 -4 10 32.90 7.80 -1 -4 10 39.70 9.60 1 -4 -10 34.20 5.80 -1 4 10 25.80 10.40 -1 4 10 37.50 7.90 -1 4 10 20.40 12.50 1 4 -10 27.70 6.90 0 -4 10 0.20 7.80 0 -4 10 10.00 10.10 0 -4 10 2.70 6.50 0 -4 10 17.20 9.60 0 -4 10 -6.90 7.90 0 4 10 2.80 8.40 0 4 10 2.90 5.50 0 4 10 0.00 10.30 1 -4 10 6.00 7.40 1 -4 10 3.80 4.80 1 -4 10 0.40 5.60 1 -4 10 8.20 6.90 -1 4 -10 12.90 4.90 1 4 10 10.00 7.40 1 4 10 11.90 8.20 -1 4 -10 7.40 8.70 2 -4 10 7.70 5.80 2 -4 10 16.30 5.80 2 -4 10 12.10 5.50 2 -4 10 7.40 4.80 -2 4 -10 7.40 3.40 -2 4 -10 6.30 5.80 2 4 10 7.60 9.00 3 -4 10 40.20 9.30 3 -4 10 82.69 8.80 3 -4 10 96.09 9.10 -3 4 -10 74.29 8.30 8 -5 -10 15.90 5.10 -8 -5 10 14.80 5.20 8 -5 -10 25.70 5.70 8 5 -10 17.90 5.10 -7 -5 10 -1.70 5.40 -7 -5 10 2.30 7.60 7 -5 -10 9.20 7.60 7 5 -10 3.40 4.60 7 5 -10 -4.30 4.30 6 -5 -10 1.90 7.70 6 -5 -10 1.80 5.90 -6 -5 10 -1.30 8.50 -6 -5 10 -6.90 8.00 6 5 -10 -0.60 5.00 6 5 -10 4.20 5.80 5 -5 -10 8.80 6.40 5 -5 -10 15.80 10.40 -5 -5 10 6.60 8.90 -5 -5 10 14.10 10.00 5 -5 -10 17.60 8.60 -5 5 10 21.10 7.30 5 5 -10 22.60 8.20 5 5 -10 -3.00 6.40 -4 -5 10 5.90 7.30 -4 -5 10 6.70 5.50 4 -5 -10 6.30 6.10 -4 -5 10 2.50 6.30 -4 5 10 6.60 7.80 4 5 -10 -5.20 5.70 -4 5 10 5.90 7.50 -3 -5 10 1.00 7.70 3 -5 -10 2.70 5.50 -3 -5 10 -4.90 5.50 -3 -5 10 -3.30 6.30 -3 5 10 3.80 6.30 -3 5 10 -5.30 7.80 3 5 -10 5.40 5.60 -3 5 10 13.00 8.30 3 5 -10 -0.40 6.00 -2 -5 10 22.70 10.60 2 -5 -10 23.50 6.20 -2 -5 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7.10 0 0 12 -1.60 7.00 0 0 12 -6.10 5.00 0 0 12 4.90 10.30 0 0 12 4.10 5.80 0 0 12 4.30 4.90 1 0 12 5.30 7.20 1 0 12 -9.20 5.50 1 0 12 3.70 4.30 1 0 12 -6.50 4.10 8 -1 -12 3.30 4.30 8 -1 -12 -3.10 7.40 8 1 -12 0.10 4.20 8 1 -12 -2.90 4.50 7 -1 -12 24.90 6.70 7 -1 -12 26.20 6.80 7 1 -12 20.00 6.70 7 1 -12 13.80 5.50 6 -1 -12 28.60 9.20 6 -1 -12 12.10 6.00 -6 -1 12 8.90 6.90 -6 -1 12 -0.90 9.30 -6 1 12 13.60 5.80 6 1 -12 15.00 8.40 -6 1 12 13.20 8.00 6 1 -12 11.30 5.80 -5 -1 12 19.20 10.20 -5 -1 12 13.20 7.90 -5 -1 12 16.80 9.60 5 -1 -12 18.80 5.00 -5 -1 12 14.80 7.70 5 1 -12 18.60 10.00 -5 1 12 14.60 7.90 -5 1 12 22.50 8.10 5 1 -12 19.90 6.20 -5 1 12 21.40 8.70 -4 -1 12 0.70 10.10 4 -1 -12 5.90 5.00 -4 -1 12 17.20 6.30 -4 -1 12 22.10 9.50 -4 -1 12 17.40 10.30 -4 1 12 7.00 8.40 4 1 -12 6.50 5.70 -4 1 12 16.30 8.50 -4 1 12 20.80 11.70 -4 1 12 15.20 7.00 -3 -1 12 271.87 18.30 -3 -1 12 242.78 19.70 3 -1 -12 212.58 13.90 -3 -1 12 244.98 16.60 -3 -1 12 238.28 16.10 3 1 -12 246.18 14.50 -3 1 12 230.58 16.40 -3 1 12 249.48 20.70 -3 1 12 261.17 17.80 -3 1 12 265.77 15.60 -2 -1 12 193.28 15.70 -2 -1 12 184.08 14.60 -2 -1 12 173.58 18.20 -2 -1 12 201.78 13.40 -2 -1 12 180.18 13.40 2 -1 -12 187.18 11.80 -2 1 12 192.58 17.00 -2 1 12 197.98 13.80 -2 1 12 189.98 16.50 -2 1 12 213.88 19.40 2 1 -12 173.18 12.00 1 -1 -12 1.70 4.00 -1 -1 12 7.70 7.60 -1 -1 12 -8.00 7.40 -1 -1 12 2.90 5.40 -1 -1 12 5.10 7.80 -1 -1 12 -2.30 5.90 1 1 -12 7.70 5.10 -1 1 12 -2.70 10.30 -1 1 12 11.90 8.70 -1 1 12 2.70 5.50 -1 1 12 -2.10 7.80 0 -1 12 20.80 8.20 0 -1 12 23.00 8.40 0 -1 12 9.50 5.60 0 -1 12 17.20 8.60 0 -1 12 25.20 6.50 0 1 12 6.40 7.20 0 1 -12 31.70 6.60 0 1 12 3.80 9.80 0 1 12 25.50 7.80 0 1 12 15.60 7.80 1 -1 12 -12.00 8.20 1 -1 12 -6.00 4.50 1 -1 12 -1.00 4.80 1 -1 12 -1.10 5.10 1 1 12 -5.30 6.00 1 1 12 4.20 5.50 1 1 12 2.50 9.00 1 1 12 8.70 9.00 8 -2 -12 20.10 5.50 8 2 -12 -0.80 4.70 -7 -2 12 6.80 6.00 7 -2 -12 7.30 7.70 7 2 -12 9.90 5.80 7 2 -12 5.40 6.20 -6 -2 12 5.90 6.50 -6 -2 12 7.20 6.40 6 -2 -12 10.00 5.50 6 -2 -12 2.10 5.50 6 2 -12 14.40 6.40 -5 -2 12 8.40 5.50 -5 -2 12 -7.00 8.40 -5 -2 12 6.00 7.10 5 -2 -12 -4.30 4.90 5 2 -12 10.70 4.50 -5 2 12 0.50 9.80 -5 2 12 2.40 6.90 -5 2 12 8.40 5.60 5 2 -12 7.90 9.80 -4 -2 12 15.00 8.00 -4 -2 12 24.00 8.70 -4 -2 12 13.80 5.80 4 -2 -12 20.20 6.20 -4 -2 12 21.60 7.80 -4 -2 12 21.70 10.10 -4 2 12 24.40 8.40 -4 2 12 8.50 11.10 -4 2 12 25.30 8.80 4 2 -12 5.20 5.40 -3 -2 12 8.00 7.10 3 -2 -12 26.60 6.10 -3 -2 12 6.70 10.80 -3 -2 12 27.80 7.30 -3 -2 12 30.20 8.30 3 2 -12 15.40 6.10 -3 2 12 42.10 10.10 -3 2 12 24.80 7.20 -3 2 12 12.90 6.60 -3 2 12 24.10 9.10 -2 -2 12 85.89 10.40 -2 -2 12 95.29 15.30 -2 -2 12 94.19 11.00 2 -2 -12 84.19 8.00 -2 -2 12 104.49 12.60 -2 -2 12 104.09 12.10 -2 2 12 83.89 14.00 -2 2 12 51.79 10.10 -2 2 12 103.99 13.00 2 2 -12 103.19 9.60 -2 2 12 84.49 11.30 -1 -2 12 31.80 6.80 -1 -2 12 29.60 9.00 1 -2 -12 25.50 4.70 -1 -2 12 17.10 10.30 -1 -2 12 24.60 8.20 -1 -2 12 40.00 9.00 -1 2 12 22.40 11.30 -1 2 12 20.70 8.40 1 2 -12 21.80 5.70 -1 2 12 28.70 8.80 -1 2 12 43.00 7.90 0 -2 12 154.88 12.50 0 -2 12 151.08 11.40 0 -2 12 165.18 12.20 0 -2 12 194.48 16.70 0 2 12 176.88 13.80 0 2 12 130.39 11.30 0 2 12 150.78 13.90 1 -2 12 1.80 6.80 1 -2 12 1.10 4.40 1 -2 12 9.40 6.70 1 -2 12 8.80 5.00 1 2 12 5.40 6.00 1 2 12 9.50 4.90 1 2 12 6.60 5.60 7 -3 -12 23.10 7.60 7 -3 -12 13.20 5.50 -7 -3 12 6.00 5.20 7 3 -12 19.70 5.80 -6 -3 12 6.40 6.30 6 -3 -12 -0.20 7.00 -6 -3 12 3.90 5.70 6 3 -12 13.40 6.10 -5 -3 12 0.30 5.80 -5 -3 12 -2.00 6.40 5 -3 -12 1.70 3.80 5 -3 -12 -2.60 4.60 -5 3 12 7.80 5.70 5 3 -12 10.40 6.80 -5 3 12 7.70 6.70 -5 3 12 7.30 7.20 -4 -3 12 2.00 8.90 -4 -3 12 15.80 5.70 4 -3 -12 -0.60 7.10 4 -3 -12 3.50 5.30 -4 -3 12 11.10 7.60 -4 -3 12 13.50 7.10 -4 3 12 -2.70 7.20 4 3 -12 13.50 5.60 -4 3 12 2.30 6.10 4 3 -12 7.30 6.60 -4 3 12 -2.80 9.40 3 -3 -12 25.40 6.40 -3 -3 12 13.30 8.90 3 -3 -12 21.40 5.80 -3 -3 12 37.40 7.20 -3 -3 12 33.20 8.50 -3 -3 12 23.90 9.80 -3 -3 12 22.30 6.90 3 3 -12 28.20 5.60 3 3 -12 42.10 7.70 -3 3 12 19.50 6.60 -3 3 12 11.30 10.70 -3 3 12 7.60 10.80 -2 -3 12 2.20 4.80 -2 -3 12 -1.50 9.40 2 -3 -12 2.30 4.30 -2 -3 12 12.00 9.80 -2 -3 12 10.20 5.50 2 3 -12 2.10 3.70 2 3 -12 7.50 7.40 -2 3 12 7.50 7.90 -2 3 12 -0.90 7.20 -2 3 12 1.50 5.00 -2 3 12 -3.70 7.30 -1 -3 12 34.10 7.10 -1 -3 12 17.70 9.70 -1 -3 12 17.20 7.00 -1 -3 12 5.40 7.30 -1 -3 12 14.40 6.90 -1 3 12 17.70 5.60 -1 3 12 23.50 8.70 1 3 -12 25.30 6.10 -1 3 12 26.20 8.30 1 3 -12 37.20 6.90 0 -3 12 26.40 7.10 0 -3 12 19.90 7.30 0 -3 12 75.19 10.10 0 -3 12 48.30 6.90 0 3 12 29.50 7.00 0 3 12 19.20 7.00 0 3 -12 49.70 7.50 0 3 12 55.89 9.30 1 -3 12 3.50 4.20 1 -3 12 10.20 15.20 1 -3 12 7.20 4.90 1 -3 12 0.40 4.10 6 -4 -12 3.00 6.30 6 -4 -12 1.10 4.60 -6 -4 12 0.40 5.00 -6 -4 12 7.40 5.70 6 4 -12 -0.70 4.00 6 4 -12 -2.60 4.60 5 -4 -12 1.80 4.70 -5 -4 12 -0.40 5.10 -5 -4 12 -0.10 5.90 -5 4 12 4.20 5.40 5 4 -12 -4.90 5.30 5 4 -12 -1.90 6.10 -4 -4 12 34.80 8.10 -4 -4 12 17.90 8.10 -4 -4 12 40.00 7.60 4 4 -12 68.49 9.80 -4 4 12 35.30 7.70 4 4 -12 57.79 7.50 -4 4 12 58.09 7.90 -4 4 12 50.79 8.80 -3 -4 12 -6.90 5.80 -3 -4 12 4.60 8.30 3 4 -12 1.80 7.80 -3 4 12 -10.40 5.10 -3 4 12 5.50 9.70 -3 4 12 3.40 7.40 -2 -4 12 251.77 16.60 -2 -4 12 259.27 15.90 -2 -4 12 239.88 14.10 -2 -4 12 231.18 12.80 -2 4 12 263.27 19.20 -2 4 12 272.57 17.40 -2 4 12 243.28 13.80 -1 -4 12 36.00 5.70 -1 -4 12 24.10 6.70 -1 -4 12 27.50 7.20 -1 4 12 37.40 5.70 -1 4 12 44.40 8.40 -1 4 12 69.29 9.60 1 4 -12 37.70 6.50 0 -4 12 16.60 4.60 0 -4 12 19.60 6.30 0 -4 12 13.60 4.80 0 4 12 26.00 6.80 0 4 12 10.80 5.90 5 -5 -12 9.80 7.00 -5 -5 12 -1.40 4.90 4 -5 -12 44.30 9.10 -4 -5 12 19.30 6.30 4 5 -12 39.20 5.80 4 5 -12 22.80 6.00 -4 5 12 44.10 7.30 -3 -5 12 33.20 7.10 3 -5 -12 38.80 8.90 -3 5 12 10.40 6.60 3 5 -12 16.80 6.20 -3 5 12 28.20 7.30 -2 -5 12 27.50 8.90 -2 -5 12 58.99 8.50 -2 5 12 75.59 9.70 2 5 -12 52.59 7.60 6 0 -13 3.90 5.00 6 0 -13 -3.80 4.80 5 0 -13 2.00 5.10 -5 0 13 -2.60 8.40 -5 0 13 -3.30 4.40 -4 0 13 0.80 8.90 -4 0 13 0.70 4.70 -4 0 13 -7.50 4.70 -4 0 13 -2.70 6.40 4 0 -13 -3.20 5.60 -3 0 13 4.20 5.50 -3 0 13 -3.20 5.90 -3 0 13 -15.30 9.80 -3 0 13 5.00 7.60 -2 0 13 -4.40 6.60 -2 0 13 5.10 6.80 -2 0 13 -3.00 5.10 -2 0 13 1.90 5.40 -1 0 13 194.38 13.50 -1 0 13 176.68 12.10 -1 0 13 159.98 12.70 6 -1 -13 -4.70 4.00 -6 -1 13 -4.00 5.50 6 1 -13 4.50 4.60 -5 -1 13 24.00 7.00 -5 1 13 27.00 7.10 -5 1 13 27.20 7.40 5 1 -13 36.90 6.90 -5 1 13 29.50 7.90 -4 -1 13 20.60 6.70 -4 -1 13 26.30 8.30 -4 -1 13 9.70 4.80 -4 -1 13 12.10 7.30 -4 1 13 19.80 5.90 -4 1 13 20.50 6.90 -4 1 13 9.20 9.80 4 1 -13 4.30 8.20 -3 -1 13 34.40 8.40 -3 -1 13 74.69 9.50 -3 -1 13 49.30 8.20 -3 -1 13 64.69 9.90 -3 1 13 72.59 10.50 -3 1 13 44.40 8.50 -3 1 13 30.70 8.50 -3 1 13 76.19 10.40 3 1 -13 45.80 7.90 -2 -1 13 40.90 8.40 -2 -1 13 32.40 7.60 -2 -1 13 32.80 8.10 -2 -1 13 46.00 7.60 -2 1 13 36.20 8.00 -2 1 13 63.49 11.40 -2 1 13 57.69 7.50 -2 1 13 6.80 9.60 -1 -1 13 8.50 4.90 -1 -1 13 40.90 7.60 -1 -1 13 30.20 5.60 -1 -1 13 36.00 8.10 -1 1 13 30.60 8.00 -1 1 13 23.30 5.90 -1 1 13 22.20 5.80 -1 1 13 37.40 8.10 6 -2 -13 0.60 4.20 6 2 -13 6.40 4.90 -5 -2 13 46.40 7.70 5 -2 -13 30.20 5.80 -5 2 13 39.80 6.10 5 2 -13 46.50 7.50 -5 2 13 15.50 6.40 -5 2 13 33.90 10.90 -4 -2 13 1.30 4.50 -4 -2 13 -4.60 5.50 -4 -2 13 10.80 6.20 4 -2 -13 4.90 6.40 4 2 -13 -0.50 8.00 -4 2 13 3.80 4.90 -4 2 13 -1.40 8.40 -4 2 13 0.20 5.90 -3 -2 13 2.90 5.90 -3 -2 13 6.90 4.80 -3 -2 13 -1.10 6.10 -3 -2 13 12.60 5.10 -3 2 13 14.10 7.60 -3 2 13 14.80 6.70 -3 2 13 9.70 6.80 -2 -2 13 127.79 10.70 -2 -2 13 126.49 11.50 -2 -2 13 129.89 11.70 -2 2 13 127.49 10.00 -2 2 13 135.09 10.10 -2 2 13 122.99 12.20 -2 2 13 139.59 12.40 -1 -2 13 19.90 4.70 -1 -2 13 23.60 6.50 -1 -2 13 -0.70 6.40 -1 2 13 5.10 6.10 -1 2 13 25.20 5.20 -1 2 13 26.70 7.10 -5 -3 13 4.20 5.50 5 3 -13 2.20 5.10 -4 -3 13 31.80 7.00 -4 3 13 20.00 8.90 -4 3 13 46.80 6.70 -4 3 13 29.20 6.60 4 3 -13 33.10 6.90 -3 -3 13 5.90 6.10 -3 -3 13 3.20 4.50 -3 -3 13 0.30 5.40 -3 3 13 9.60 6.80 -3 3 13 6.30 6.40 -3 3 13 -3.80 4.50 3 3 -13 -1.70 5.40 -2 -3 13 7.70 5.80 -2 3 13 5.40 6.30 -2 3 13 5.80 5.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 76552 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_glo9508 _database_code_depnum_ccdc_archive 'CCDC 2006232' loop_ _audit_author_name _audit_author_address 'Constantin G. Daniliuc' ;Organisch Chemisches Institut WWU University of Muenster Germany ; _audit_update_record ; 2020-05-27 deposited with the CCDC. 2021-03-04 downloaded from the CCDC. ; _audit_creation_method 'APEX3 v2016.1-0' _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_sum 'C10 H20 Cl2 N2 O' _chemical_formula_iupac ? _chemical_formula_weight 255.18 _chemical_absolute_configuration ad _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 1 21 1' _space_group_name_Hall 'P 2yb' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 8.3482(5) _cell_length_b 6.0629(3) _cell_length_c 13.2849(9) _cell_angle_alpha 90 _cell_angle_beta 106.642(2) _cell_angle_gamma 90 _cell_volume 644.24(7) _cell_formula_units_Z 2 _cell_measurement_reflns_used 1130 _cell_measurement_theta_min 4.08 _cell_measurement_theta_max 28.28 _cell_measurement_temperature 173.(2) _exptl_crystal_description needle _exptl_crystal_colour colourless _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.020 _exptl_crystal_size_min 0.020 _exptl_crystal_density_diffrn 1.315 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 272 _exptl_absorpt_coefficient_mu 0.483 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Denzo (Otwinowski, Borek, Majewski & Minor, 2003)' _exptl_absorpt_correction_T_min 0.89 _exptl_absorpt_correction_T_max 0.99 _exptl_special_details ; ; _diffrn_ambient_temperature 173.(2) _diffrn_source 'Mo rotating anode' _diffrn_source_type 'Mo rotating anode' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Montel mirror' _diffrn_measurement_device_type 'rotating anode Nonius FR591' _diffrn_measurement_method 'omega and phi scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 4170 _diffrn_reflns_av_R_equivalents 0.0540 _diffrn_reflns_av_unetI/netI 0.0396 _diffrn_reflns_theta_min 4.22 _diffrn_reflns_theta_max 24.99 _diffrn_reflns_theta_full 24.99 _diffrn_measured_fraction_theta_max 0.968 _diffrn_measured_fraction_theta_full 0.968 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _refine_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. The hydrogens at O1 and N1 atoms were refined freely. ; _reflns_number_total 1959 _reflns_number_gt 1802 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0644 _refine_ls_R_factor_gt 0.0577 _refine_ls_wR_factor_gt 0.1439 _refine_ls_wR_factor_ref 0.1517 _refine_ls_goodness_of_fit_ref 1.077 _refine_ls_restrained_S_all 1.077 _refine_ls_number_reflns 1959 _refine_ls_number_parameters 150 _refine_ls_number_restraints 2 _refine_ls_number_constraints ? _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0782P)^2^+0.9832P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.324 _refine_diff_density_min -0.271 _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details ; Flack x determined using 645 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.12(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; Collect (Nonius B.V., 1998) ; _computing_cell_refinement 'Collect (Nonius B.V., 1998)' _computing_data_reduction 'Denzo-SMN (Otwinowski & Minor, 1997)' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'XP (Sheldrick, 2014)' _computing_publication_material 'SHELXL-2014/7 (Sheldrick, 2014)' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N N1 0.3077(6) -0.0168(12) 0.8767(4) 0.0273(10) Uani d . . D 1 . . H H1A 0.371(8) 0.098(13) 0.912(5) 0.022(17) Uiso d . . . 1 . . H H1B 0.344(9) -0.153(7) 0.899(6) 0.05(2) Uiso d . . D 1 . . O O1 -0.0501(6) -0.2946(9) 0.6404(3) 0.0385(12) Uani d . . . 1 . . C C2 0.1345(7) 0.0058(13) 0.8883(4) 0.0288(13) Uani d . . . 1 . . H H2 0.0881 0.1536 0.8617 0.035 Uiso calc U . R 1 . . C C3 0.0307(8) -0.1734(13) 0.8197(5) 0.0328(15) Uani d . . . 1 . . H H3A 0.0606 -0.3174 0.8552 0.039 Uiso calc U . R 1 . . H H3B -0.0888 -0.1457 0.8126 0.039 Uiso calc U . R 1 . . C C4 0.0538(8) -0.1871(12) 0.7130(4) 0.0298(14) Uani d . . . 1 . . N N5 0.1792(6) -0.0867(9) 0.6909(4) 0.0252(11) Uani d . . . 1 . . C C6 0.1906(8) -0.0709(12) 0.5820(4) 0.0335(16) Uani d . . . 1 . . H H6A 0.1877 0.0861 0.561 0.04 Uiso calc U . R 1 . . H H6B 0.0935 -0.1462 0.5336 0.04 Uiso calc U . R 1 . . C C7 0.3513(8) -0.1763(13) 0.5736(5) 0.0346(16) Uani d . . . 1 . . H H7 0.3582 -0.1507 0.5006 0.042 Uiso calc U . R 1 . . C C8 0.4985(8) -0.0565(13) 0.6490(5) 0.0381(17) Uani d . . . 1 . . H H8A 0.6041 -0.1282 0.647 0.046 Uiso calc U . R 1 . . H H8B 0.5011 0.0981 0.6255 0.046 Uiso calc U . R 1 . . C C9 0.4868(7) -0.0586(14) 0.7614(5) 0.0379(19) Uani d . . . 1 . . H H9A 0.5769 0.0348 0.8059 0.046 Uiso calc U . R 1 . . H H9B 0.5041 -0.211 0.7891 0.046 Uiso calc U . R 1 . . C C10 0.3175(7) 0.0259(11) 0.7687(4) 0.0281(14) Uani d . . . 1 . . H H10 0.3098 0.1883 0.7549 0.034 Uiso calc U . R 1 . . C C11 0.1429(8) -0.0151(17) 1.0030(5) 0.0424(16) Uani d . . . 1 . . H H11A 0.0306 0.0026 1.0111 0.064 Uiso calc U . R 1 . . H H11B 0.2167 0.0994 1.0434 0.064 Uiso calc U . R 1 . . H H11C 0.1868 -0.1608 1.0288 0.064 Uiso calc U . R 1 . . C C12 0.3514(10) -0.4248(14) 0.5911(6) 0.048(2) Uani d . . . 1 . . H H12A 0.3371 -0.4551 0.6605 0.073 Uiso calc U . R 1 . . H H12B 0.4579 -0.487 0.5873 0.073 Uiso calc U . R 1 . . H H12C 0.2594 -0.4922 0.5368 0.073 Uiso calc U . R 1 . . Cl Cl1 0.37162(19) 0.4865(3) 0.92481(12) 0.0380(4) Uani d . . . 1 . . Cl Cl2 -0.1832(3) -0.6540(4) 0.71840(14) 0.0569(6) Uani d . . . 1 . . H H2A -0.104(11) -0.422(17) 0.669(7) 0.06(3) Uiso d . . . 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.029(2) 0.024(3) 0.024(2) -0.004(3) -0.0005(19) -0.001(2) O1 0.037(3) 0.049(3) 0.024(2) -0.014(2) -0.0003(19) -0.002(2) C2 0.028(3) 0.026(4) 0.029(3) 0.002(3) 0.004(2) -0.005(3) C3 0.030(3) 0.041(4) 0.027(3) -0.006(3) 0.007(2) -0.003(3) C4 0.030(3) 0.030(4) 0.024(3) -0.005(3) -0.001(2) -0.002(3) N5 0.023(2) 0.027(3) 0.023(2) -0.003(2) 0.0012(18) -0.0013(19) C6 0.039(3) 0.038(5) 0.020(3) -0.005(3) 0.003(2) 0.000(2) C7 0.038(3) 0.046(4) 0.022(3) -0.003(3) 0.012(2) 0.001(3) C8 0.037(3) 0.042(5) 0.039(3) -0.009(3) 0.016(3) -0.002(3) C9 0.026(3) 0.058(6) 0.028(3) -0.013(3) 0.004(2) -0.002(3) C10 0.031(3) 0.027(4) 0.023(3) -0.006(3) 0.002(2) 0.000(2) C11 0.044(3) 0.052(4) 0.033(3) 0.004(4) 0.014(3) -0.008(4) C12 0.054(4) 0.044(5) 0.050(4) -0.001(4) 0.020(4) -0.012(4) Cl1 0.0418(8) 0.0205(8) 0.0395(8) 0.0011(8) -0.0078(6) -0.0001(7) Cl2 0.0565(11) 0.0539(14) 0.0435(10) -0.0245(10) -0.0124(8) 0.0128(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag N1 C10 . 1.484(7) ? N1 C2 . 1.504(7) ? N1 H1A . 0.92(7) ? N1 H1B . 0.90(3) ? O1 C4 . 1.275(8) ? O1 H2A . 1.02(10) ? C2 C11 . 1.510(8) ? C2 C3 . 1.520(9) ? C2 H2 . 1.0 ? C3 C4 . 1.486(8) ? C3 H3A . 0.99 ? C3 H3B . 0.99 ? C4 N5 . 1.315(8) ? N5 C10 . 1.478(7) ? N5 C6 . 1.480(7) ? C6 C7 . 1.519(9) ? C6 H6A . 0.99 ? C6 H6B . 0.99 ? C7 C12 . 1.525(12) ? C7 C8 . 1.528(9) ? C7 H7 . 1.0 ? C8 C9 . 1.525(8) ? C8 H8A . 0.99 ? C8 H8B . 0.99 ? C9 C10 . 1.531(9) ? C9 H9A . 0.99 ? C9 H9B . 0.99 ? C10 H10 . 1.0 ? C11 H11A . 0.98 ? C11 H11B . 0.98 ? C11 H11C . 0.98 ? C12 H12A . 0.98 ? C12 H12B . 0.98 ? C12 H12C . 0.98 ? Cl2 H2A . 1.76(10) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C10 N1 C2 . . 113.9(4) ? C10 N1 H1A . . 100.(4) ? C2 N1 H1A . . 108.(4) ? C10 N1 H1B . . 112.(5) ? C2 N1 H1B . . 107.(5) ? H1A N1 H1B . . 116.(6) ? C4 O1 H2A . . 113.(5) ? N1 C2 C11 . . 109.1(5) ? N1 C2 C3 . . 105.8(5) ? C11 C2 C3 . . 113.5(6) ? N1 C2 H2 . . 109.4 ? C11 C2 H2 . . 109.4 ? C3 C2 H2 . . 109.4 ? C4 C3 C2 . . 113.9(5) ? C4 C3 H3A . . 108.8 ? C2 C3 H3A . . 108.8 ? C4 C3 H3B . . 108.8 ? C2 C3 H3B . . 108.8 ? H3A C3 H3B . . 107.7 ? O1 C4 N5 . . 118.7(5) ? O1 C4 C3 . . 120.2(6) ? N5 C4 C3 . . 121.0(5) ? C4 N5 C10 . . 124.8(5) ? C4 N5 C6 . . 121.8(5) ? C10 N5 C6 . . 113.4(4) ? N5 C6 C7 . . 110.5(5) ? N5 C6 H6A . . 109.6 ? C7 C6 H6A . . 109.6 ? N5 C6 H6B . . 109.6 ? C7 C6 H6B . . 109.6 ? H6A C6 H6B . . 108.1 ? C6 C7 C12 . . 111.5(6) ? C6 C7 C8 . . 108.3(6) ? C12 C7 C8 . . 113.9(6) ? C6 C7 H7 . . 107.6 ? C12 C7 H7 . . 107.6 ? C8 C7 H7 . . 107.6 ? C9 C8 C7 . . 111.9(5) ? C9 C8 H8A . . 109.2 ? C7 C8 H8A . . 109.2 ? C9 C8 H8B . . 109.2 ? C7 C8 H8B . . 109.2 ? H8A C8 H8B . . 107.9 ? C8 C9 C10 . . 112.2(5) ? C8 C9 H9A . . 109.2 ? C10 C9 H9A . . 109.2 ? C8 C9 H9B . . 109.2 ? C10 C9 H9B . . 109.2 ? H9A C9 H9B . . 107.9 ? N5 C10 N1 . . 110.3(5) ? N5 C10 C9 . . 110.6(5) ? N1 C10 C9 . . 108.0(5) ? N5 C10 H10 . . 109.3 ? N1 C10 H10 . . 109.3 ? C9 C10 H10 . . 109.3 ? C2 C11 H11A . . 109.5 ? C2 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C2 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C7 C12 H12A . . 109.5 ? C7 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C7 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C10 N1 C2 C11 . . . . -173.5(6) ? C10 N1 C2 C3 . . . . 64.0(7) ? N1 C2 C3 C4 . . . . -46.6(8) ? C11 C2 C3 C4 . . . . -166.3(6) ? C2 C3 C4 O1 . . . . -164.7(6) ? C2 C3 C4 N5 . . . . 14.2(10) ? O1 C4 N5 C10 . . . . -174.0(6) ? C3 C4 N5 C10 . . . . 7.1(10) ? O1 C4 N5 C6 . . . . 8.0(10) ? C3 C4 N5 C6 . . . . -170.9(6) ? C4 N5 C6 C7 . . . . -121.3(7) ? C10 N5 C6 C7 . . . . 60.5(7) ? N5 C6 C7 C12 . . . . 66.8(7) ? N5 C6 C7 C8 . . . . -59.3(7) ? C6 C7 C8 C9 . . . . 56.1(8) ? C12 C7 C8 C9 . . . . -68.5(8) ? C7 C8 C9 C10 . . . . -52.4(9) ? C4 N5 C10 N1 . . . . 7.8(9) ? C6 N5 C10 N1 . . . . -174.0(5) ? C4 N5 C10 C9 . . . . 127.3(6) ? C6 N5 C10 C9 . . . . -54.5(7) ? C2 N1 C10 N5 . . . . -44.8(8) ? C2 N1 C10 C9 . . . . -165.8(6) ? C8 C9 C10 N5 . . . . 50.0(8) ? C8 C9 C10 N1 . . . . 170.8(6) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1A Cl1 . 0.92(7) 2.36(8) 3.132(7) 142.(5) ? N1 H1B Cl1 1_545 0.90(3) 2.22(3) 3.093(7) 166.(7) ? C2 H2 Cl2 1_565 1.0 2.77 3.600(7) 141.2 ? C7 H7 Cl2 2_556 1.0 2.86 3.731(6) 146.3 ? O1 H2A Cl2 . 1.02(10) 1.76(10) 2.778(5) 176.(8) ? _shelx_res_file ; glo9508.res created by SHELXL-2014/7 TITL glo9508 in P2(1) CELL 0.71073 8.3482 6.0629 13.2849 90.000 106.642 90.000 ZERR 2.00 0.0005 0.0003 0.0009 0.000 0.002 0.000 LATT -1 SYMM -X, 0.5+Y, -Z SFAC C H N O CL UNIT 20 40 4 2 4 SIZE 0.24 0.02 0.02 TEMP -100 ACTA CONF OMIT -3 50 L.S. 15 BOND $H FMAP 2 PLAN 10 DFIX 0.88 N1 H1B HTAB N1 Cl1 EQIV $1 -x+1, y-1/2, -z+2 EQIV $2 x, y-1, z HTAB N1 Cl1_$2 EQIV $3 x, y+1, z HTAB C2 Cl2_$3 EQIV $4 -x, y+1/2, -z+1 HTAB C7 Cl2_$4 HTAB O1 Cl2 WGHT 0.078200 0.983200 FVAR 0.84527 N1 3 0.307721 -0.016845 0.876686 11.00000 0.02934 0.02379 = 0.02360 -0.00109 -0.00052 -0.00414 H1A 2 0.371034 0.098203 0.911606 11.00000 0.02215 H1B 2 0.343561 -0.152740 0.898518 11.00000 0.04824 O1 4 -0.050113 -0.294607 0.640422 11.00000 0.03701 0.04858 = 0.02418 -0.00189 -0.00025 -0.01368 C2 1 0.134550 0.005786 0.888312 11.00000 0.02794 0.02647 = 0.02916 -0.00496 0.00362 0.00213 AFIX 13 H2 2 0.088140 0.153648 0.861749 11.00000 -1.20000 AFIX 0 C3 1 0.030749 -0.173385 0.819670 11.00000 0.02961 0.04061 = 0.02735 -0.00290 0.00699 -0.00562 AFIX 23 H3A 2 0.060583 -0.317404 0.855217 11.00000 -1.20000 H3B 2 -0.088838 -0.145748 0.812645 11.00000 -1.20000 AFIX 0 C4 1 0.053761 -0.187135 0.712974 11.00000 0.03014 0.02984 = 0.02385 -0.00208 -0.00117 -0.00470 N5 3 0.179165 -0.086661 0.690875 11.00000 0.02288 0.02686 = 0.02251 -0.00127 0.00118 -0.00300 C6 1 0.190576 -0.070852 0.582000 11.00000 0.03898 0.03821 = 0.01975 -0.00031 0.00260 -0.00527 AFIX 23 H6A 2 0.187651 0.086093 0.560981 11.00000 -1.20000 H6B 2 0.093481 -0.146161 0.533628 11.00000 -1.20000 AFIX 0 C7 1 0.351303 -0.176251 0.573631 11.00000 0.03808 0.04565 = 0.02232 0.00088 0.01211 -0.00266 AFIX 13 H7 2 0.358163 -0.150699 0.500615 11.00000 -1.20000 AFIX 0 C8 1 0.498520 -0.056490 0.648978 11.00000 0.03662 0.04230 = 0.03854 -0.00169 0.01574 -0.00912 AFIX 23 H8A 2 0.604140 -0.128187 0.647039 11.00000 -1.20000 H8B 2 0.501094 0.098114 0.625512 11.00000 -1.20000 AFIX 0 C9 1 0.486770 -0.058555 0.761435 11.00000 0.02552 0.05830 = 0.02764 -0.00197 0.00385 -0.01254 AFIX 23 H9A 2 0.576851 0.034818 0.805859 11.00000 -1.20000 H9B 2 0.504107 -0.210996 0.789140 11.00000 -1.20000 AFIX 0 C10 1 0.317547 0.025934 0.768652 11.00000 0.03088 0.02670 = 0.02330 -0.00026 0.00215 -0.00567 AFIX 13 H10 2 0.309814 0.188312 0.754896 11.00000 -1.20000 AFIX 0 C11 1 0.142897 -0.015063 1.002961 11.00000 0.04448 0.05207 = 0.03253 -0.00805 0.01383 0.00413 AFIX 137 H11A 2 0.030605 0.002635 1.011134 11.00000 -1.50000 H11B 2 0.216735 0.099423 1.043369 11.00000 -1.50000 H11C 2 0.186769 -0.160778 1.028791 11.00000 -1.50000 AFIX 0 C12 1 0.351441 -0.424847 0.591109 11.00000 0.05393 0.04445 = 0.04992 -0.01214 0.01985 -0.00134 AFIX 137 H12A 2 0.337140 -0.455121 0.660484 11.00000 -1.50000 H12B 2 0.457902 -0.487006 0.587280 11.00000 -1.50000 H12C 2 0.259369 -0.492172 0.536793 11.00000 -1.50000 AFIX 0 CL1 5 0.371619 0.486503 0.924809 11.00000 0.04175 0.02051 = 0.03953 -0.00011 -0.00780 0.00110 CL2 5 -0.183200 -0.654003 0.718402 11.00000 0.05651 0.05395 = 0.04351 0.01282 -0.01237 -0.02455 H2A 2 -0.104013 -0.421808 0.668585 11.00000 0.06132 HKLF 4 REM glo9508 in P2(1) REM R1 = 0.0577 for 1802 Fo > 4sig(Fo) and 0.0644 for all 1959 data REM 150 parameters refined using 2 restraints END WGHT 0.0779 0.9813 REM Highest difference peak 0.324, deepest hole -0.271, 1-sigma level 0.072 Q1 1 0.3686 -0.3159 0.9240 11.00000 0.05 0.32 Q2 1 -0.1225 -0.0129 0.8362 11.00000 0.05 0.28 Q3 1 0.3774 -0.2415 0.8539 11.00000 0.05 0.27 Q4 1 0.3638 0.3145 0.9200 11.00000 0.05 0.26 Q5 1 0.1894 0.0072 0.9567 11.00000 0.05 0.25 Q6 1 -0.1387 -0.7032 0.6656 11.00000 0.05 0.24 Q7 1 0.1374 -0.2027 0.5586 11.00000 0.05 0.24 Q8 1 0.3074 -0.2382 0.8997 11.00000 0.05 0.23 Q9 1 0.4058 0.5021 1.0161 11.00000 0.05 0.22 Q10 1 0.0408 0.1549 0.9977 11.00000 0.05 0.22 ; _shelx_res_checksum 20681 _shelx_hkl_file ; 0 0 3 1070.50 19.50 1 0 0 4 90.60 2.00 1 0 0 5 270.20 5.70 1 0 0 7 58.50 3.20 1 0 0 8 17.20 1.60 1 0 0 9 4.90 1.40 1 0 0 10 57.00 3.50 1 0 0 11 68.60 4.30 1 0 0 12 10.00 1.90 1 0 0 13 -0.30 1.40 1 0 0 14 147.70 9.00 1 0 0 15 4.70 1.50 1 0 0 16 -1.00 2.10 1 0 1 2 360.70 7.30 1 0 -1 -2 331.10 11.30 1 0 1 3 741.70 14.60 1 0 -1 -3 743.10 18.10 1 0 1 4 1128.40 36.30 1 0 -1 -4 1098.00 25.80 1 0 1 5 509.50 13.70 1 0 -1 -5 533.20 13.40 1 0 -1 -6 223.50 6.40 1 0 1 7 47.60 1.70 1 0 -1 -7 41.70 1.70 1 0 1 8 71.60 3.90 1 0 -1 -8 58.30 2.40 1 0 1 9 88.30 3.00 1 0 -1 -9 76.60 2.90 1 0 1 10 592.80 15.30 1 0 -1 -10 532.00 13.50 1 0 1 11 50.90 1.90 1 0 -1 -11 50.80 2.60 1 0 1 12 7.80 1.80 1 0 -1 -12 0.90 1.00 1 0 1 13 7.60 1.70 1 0 -1 -13 6.90 1.80 1 0 1 14 -4.60 1.50 1 0 -1 -14 2.60 2.10 1 0 1 15 58.30 4.40 1 0 -1 -15 49.30 4.20 1 0 1 16 123.00 8.00 1 0 -1 -16 127.40 8.30 1 0 2 0 4026.60 92.30 1 0 2 1 1043.20 21.50 1 0 -2 -1 1092.90 37.30 1 0 2 2 991.00 24.00 1 0 -2 -2 930.00 31.20 1 0 2 3 114.80 3.80 1 0 -2 -3 91.40 2.70 1 0 2 4 344.00 7.70 1 0 -2 -4 306.40 11.40 1 0 2 6 377.40 9.70 1 0 -2 -6 315.10 8.70 1 0 2 7 379.90 14.10 1 0 -2 -7 379.20 18.10 1 0 2 8 103.50 5.50 1 0 -2 -8 81.00 3.40 1 0 2 9 156.40 7.60 1 0 -2 -9 135.70 7.40 1 0 -2 -10 38.50 1.90 1 0 2 11 53.90 3.70 1 0 -2 -11 56.90 3.70 1 0 -2 -12 70.40 5.00 1 0 2 13 64.90 4.30 1 0 -2 -13 61.60 3.50 1 0 2 14 23.10 2.80 1 0 -2 -14 20.90 2.40 1 0 2 15 25.50 2.40 1 0 -2 -15 21.10 2.70 1 0 2 16 7.00 2.00 1 0 -2 -16 10.70 2.00 1 0 3 0 0.50 1.60 1 0 3 1 151.10 6.90 1 0 -3 -1 121.50 5.40 1 0 3 3 391.50 15.30 1 0 -3 -3 388.00 14.10 1 0 3 4 25.00 1.90 1 0 -3 -4 14.40 1.60 1 0 3 5 92.50 5.30 1 0 -3 -5 119.80 4.00 1 0 3 6 109.10 6.30 1 0 -3 -6 108.20 3.80 1 0 3 7 106.30 5.40 1 0 -3 -7 96.70 6.40 1 0 3 8 11.80 1.80 1 0 -3 -8 12.60 1.40 1 0 3 9 227.80 9.90 1 0 -3 -9 238.40 7.00 1 0 3 10 144.70 6.60 1 0 -3 -10 131.60 4.40 1 0 3 11 76.30 4.70 1 0 -3 -11 85.60 4.60 1 0 3 12 51.50 3.20 1 0 -3 -12 40.50 2.80 1 0 3 13 26.40 2.90 1 0 -3 -13 27.90 2.70 1 0 3 14 8.40 2.10 1 0 -3 -14 14.30 2.20 1 0 3 15 11.80 2.00 1 0 -3 -15 5.70 1.90 1 0 4 0 159.20 7.10 1 0 4 1 525.20 14.70 1 0 4 2 251.30 10.30 1 0 -4 -2 210.70 9.80 1 0 4 3 37.60 2.40 1 0 -4 -3 33.60 3.10 1 0 4 4 208.30 8.70 1 0 4 5 12.00 2.00 1 0 -4 -5 11.80 1.70 1 0 4 6 54.00 3.50 1 0 -4 -6 48.30 3.60 1 0 4 7 376.70 15.10 1 0 -4 -7 315.00 11.40 1 0 4 8 32.60 3.20 1 0 -4 -8 27.30 2.40 1 0 4 9 93.70 5.50 1 0 -4 -9 83.30 4.20 1 0 4 10 26.00 2.80 1 0 -4 -10 25.80 2.60 1 0 4 11 -0.30 1.60 1 0 -4 -11 0.60 1.70 1 0 4 12 27.30 3.10 1 0 -4 -12 20.70 2.20 1 0 4 14 3.90 1.90 1 0 -4 -14 5.10 1.70 1 0 5 0 5.20 2.30 1 0 5 1 55.10 3.00 1 0 5 2 105.60 5.30 1 0 5 3 103.00 5.30 1 0 -5 -4 213.40 9.50 1 0 5 5 16.00 2.10 1 0 5 6 61.20 3.70 1 0 -5 -6 72.30 4.40 1 0 5 7 41.60 3.30 1 0 -5 -7 24.10 2.90 1 0 5 8 69.40 3.90 1 0 -5 -8 62.20 3.90 1 0 5 9 35.70 3.80 1 0 -5 -9 41.70 3.70 1 0 5 10 44.80 3.80 1 0 -5 -10 49.30 3.40 1 0 5 11 26.60 3.10 1 0 -5 -11 37.70 3.30 1 0 5 12 20.70 2.70 1 0 -5 -12 15.80 2.50 1 0 5 13 -5.60 1.50 1 0 -5 -13 -1.50 1.70 1 0 6 0 232.10 11.50 1 0 6 1 148.90 7.80 1 0 6 2 17.80 3.10 1 0 6 3 2.30 1.50 1 0 6 4 6.30 1.70 1 0 6 5 86.70 5.50 1 0 -6 -5 64.10 4.40 1 0 6 6 59.80 3.80 1 0 -6 -6 35.90 3.40 1 0 6 7 5.00 2.20 1 0 -6 -7 1.60 2.00 1 0 6 8 11.00 2.60 1 0 -6 -8 10.30 2.10 1 0 6 9 3.90 2.40 1 0 -6 -9 12.40 2.70 1 0 6 10 11.10 2.30 1 0 -6 -10 0.20 1.90 1 0 6 11 16.40 3.20 1 0 7 0 9.30 2.40 1 0 7 2 11.70 2.00 1 0 7 3 -1.30 2.40 1 0 7 4 103.40 4.80 1 0 7 5 55.80 3.50 1 0 7 6 3.10 1.70 1 0 7 7 1.10 1.90 1 0 -7 -7 0.70 2.30 1 0 7 8 10.30 2.20 1 0 -7 -8 0.10 2.50 1 0 8 0 36.20 4.40 1 0 8 1 41.90 3.80 1 0 8 2 15.50 2.10 1 0 8 3 5.60 1.90 1 1 0 -17 13.50 2.30 1 1 0 -16 13.10 2.40 1 1 0 -15 -4.60 1.40 1 1 0 -14 4.10 1.20 1 1 0 -13 69.40 4.10 1 1 0 -12 -0.90 1.30 1 1 0 -11 243.30 10.00 1 1 0 -10 33.30 2.40 1 1 0 -9 64.50 3.90 1 1 0 -8 170.50 8.20 1 1 0 -7 1076.00 34.90 1 1 0 -6 1050.80 37.20 1 1 0 -5 160.80 4.00 1 1 0 -4 370.90 9.20 1 1 0 -3 1548.90 34.80 1 1 0 2 2.50 0.30 1 1 0 3 3896.00 69.90 1 1 0 4 5.40 0.40 1 1 0 5 18.40 0.80 1 1 0 6 597.00 15.00 1 1 0 7 147.80 4.50 1 1 0 8 85.50 2.90 1 1 0 9 302.40 13.20 1 1 0 10 385.00 17.50 1 1 0 12 252.50 12.70 1 1 0 13 -3.00 1.50 1 1 0 14 1.50 1.90 1 1 0 15 20.00 2.50 1 1 0 16 17.80 2.80 1 1 1 -17 34.00 3.30 1 -1 -1 17 25.00 2.90 1 1 1 -16 19.80 2.60 1 -1 -1 16 28.80 2.70 1 1 1 -15 16.10 2.60 1 -1 -1 15 12.00 2.00 1 1 1 -14 29.10 3.00 1 -1 -1 14 31.10 2.70 1 1 1 -13 45.50 3.50 1 -1 -1 13 30.00 2.00 1 1 1 -12 86.60 4.40 1 -1 -1 12 94.40 6.00 1 1 1 -11 12.50 1.90 1 -1 -1 11 16.90 1.40 1 1 1 -10 7.90 1.20 1 -1 -1 10 3.70 1.60 1 1 1 -9 89.50 3.90 1 -1 -1 9 94.10 4.80 1 1 1 -8 319.50 12.40 1 -1 -1 8 312.10 8.90 1 -1 -1 7 1523.30 36.00 1 1 1 -6 1.10 0.90 1 -1 -1 6 2.50 1.10 1 1 1 -5 549.40 13.80 1 -1 -1 5 466.80 11.40 1 1 1 -4 476.40 11.80 1 -1 -1 4 486.90 12.40 1 1 1 -3 994.40 24.50 1 -1 -1 3 1000.90 24.20 1 1 1 -2 135.20 4.00 1 -1 -1 2 144.70 3.10 1 1 1 -1 103.40 3.20 1 -1 -1 1 128.40 6.10 1 1 1 0 2915.10 53.30 1 -1 -1 0 2981.20 68.30 1 1 1 1 462.40 11.30 1 -1 -1 -1 448.70 10.80 1 1 1 2 1551.00 51.10 1 -1 -1 -2 1428.10 32.40 1 1 1 3 462.40 8.20 1 -1 -1 -3 414.20 14.10 1 1 1 4 80.50 2.10 1 -1 -1 -4 71.10 2.20 1 1 1 5 123.40 3.10 1 -1 -1 -5 121.30 4.40 1 1 1 6 211.50 6.50 1 -1 -1 -6 240.30 8.90 1 1 1 7 610.90 16.80 1 -1 -1 -7 583.30 14.90 1 1 1 8 99.80 5.90 1 -1 -1 -8 91.70 3.20 1 1 1 9 645.20 17.30 1 -1 -1 -9 556.80 14.60 1 1 1 10 294.40 8.60 1 -1 -1 -10 294.90 13.20 1 1 1 11 3.40 0.90 1 -1 -1 -11 10.60 1.70 1 1 1 12 21.60 2.10 1 -1 -1 -12 26.30 2.40 1 1 1 13 64.30 4.90 1 -1 -1 -13 63.40 5.20 1 1 1 14 4.30 1.70 1 -1 -1 -14 8.90 1.80 1 1 1 15 11.40 2.10 1 -1 -1 -15 16.70 2.70 1 1 1 16 1.90 1.90 1 -1 -1 -16 3.90 1.70 1 1 2 -16 7.00 2.00 1 -1 -2 16 3.70 2.10 1 1 2 -15 7.90 1.80 1 -1 -2 15 4.90 2.00 1 1 2 -14 16.20 2.30 1 -1 -2 14 20.70 2.50 1 1 2 -13 11.60 1.80 1 -1 -2 13 5.80 2.20 1 1 2 -12 10.10 1.80 1 -1 -2 12 10.20 1.40 1 1 2 -11 47.80 2.90 1 -1 -2 11 46.50 2.20 1 1 2 -10 28.30 1.80 1 -1 -2 10 32.50 1.90 1 1 2 -9 134.20 7.50 1 -1 -2 9 133.00 4.50 1 1 2 -8 69.00 3.90 1 -1 -2 8 58.10 2.70 1 -1 -2 7 649.80 16.50 1 1 2 -6 145.10 7.90 1 -1 -2 6 131.60 4.20 1 1 2 -5 8.90 1.10 1 -1 -2 5 15.50 1.50 1 1 2 -4 265.40 7.30 1 -1 -2 4 270.00 7.40 1 1 2 -3 899.80 18.40 1 -1 -2 3 825.70 27.20 1 1 2 -2 109.30 2.90 1 -1 -2 2 136.40 6.00 1 1 2 -1 832.80 31.50 1 -1 -2 1 858.90 21.50 1 1 2 0 1355.00 22.90 1 -1 -2 0 1212.60 42.60 1 1 2 1 882.20 18.30 1 -1 -2 -1 971.10 32.60 1 1 2 2 735.90 26.30 1 -1 -2 -2 689.10 23.40 1 1 2 3 382.20 9.90 1 -1 -2 -3 346.90 12.10 1 1 2 4 536.40 11.20 1 -1 -2 -4 557.10 18.70 1 1 2 5 222.00 6.30 1 -1 -2 -5 211.00 7.90 1 1 2 6 22.60 1.10 1 -1 -2 -6 23.50 1.90 1 1 2 7 250.70 8.60 1 -1 -2 -7 301.10 11.00 1 1 2 8 196.00 9.30 1 -1 -2 -8 147.80 5.90 1 1 2 9 131.90 4.40 1 -1 -2 -9 123.90 5.10 1 1 2 10 243.60 11.60 1 -1 -2 -10 188.70 7.80 1 1 2 11 39.70 2.80 1 -1 -2 -11 30.00 2.10 1 1 2 12 56.30 4.00 1 -1 -2 -12 52.60 3.70 1 1 2 13 34.50 2.50 1 -1 -2 -13 26.10 2.60 1 1 2 14 26.70 2.90 1 -1 -2 -14 22.60 2.60 1 1 2 15 8.10 2.30 1 -1 -2 -15 8.30 1.80 1 1 3 -16 28.50 2.90 1 -1 -3 16 17.90 2.60 1 1 3 -15 6.20 2.00 1 -1 -3 15 3.10 1.70 1 1 3 -14 47.40 4.10 1 -1 -3 14 40.70 3.40 1 1 3 -12 7.60 1.60 1 -1 -3 12 8.90 1.60 1 1 3 -11 149.50 6.70 1 -1 -3 11 117.70 4.10 1 1 3 -10 45.90 3.80 1 -1 -3 10 41.10 2.40 1 1 3 -9 174.70 9.60 1 -1 -3 9 164.40 7.00 1 1 3 -8 94.30 4.20 1 -1 -3 8 104.30 3.80 1 1 3 -7 205.30 9.10 1 -1 -3 7 173.20 6.80 1 1 3 -6 123.10 5.20 1 -1 -3 6 109.40 4.70 1 -1 -3 5 327.20 9.40 1 1 3 -4 71.70 3.80 1 -1 -3 4 67.80 2.90 1 1 3 -3 99.30 4.80 1 -1 -3 3 103.20 4.10 1 1 3 -2 20.80 1.80 1 -1 -3 2 27.60 1.90 1 1 3 -1 367.10 13.30 1 -1 -3 1 452.70 16.60 1 1 3 0 396.70 10.70 1 1 3 1 11.80 1.70 1 1 3 2 145.40 6.50 1 -1 -3 -2 148.80 5.90 1 1 3 3 806.20 22.60 1 1 3 4 291.50 14.60 1 -1 -3 -4 307.00 11.00 1 1 3 5 59.80 2.90 1 -1 -3 -5 59.40 3.20 1 1 3 6 101.00 3.50 1 -1 -3 -6 83.50 4.40 1 1 3 7 51.10 2.50 1 -1 -3 -7 50.00 3.00 1 1 3 8 246.80 12.70 1 -1 -3 -8 225.90 8.60 1 1 3 9 429.80 19.40 1 -1 -3 -9 389.00 15.10 1 1 3 10 37.80 3.00 1 -1 -3 -10 22.30 2.30 1 1 3 11 13.50 2.10 1 -1 -3 -11 19.60 2.10 1 -1 -3 -12 14.20 2.20 1 1 3 13 8.00 2.10 1 -1 -3 -13 15.90 2.20 1 1 3 14 51.90 4.60 1 -1 -3 -14 34.60 3.30 1 1 3 15 13.20 2.30 1 -1 -3 -15 13.60 2.10 1 1 4 -15 11.70 2.20 1 -1 -4 15 8.10 1.70 1 1 4 -14 1.90 2.10 1 -1 -4 14 -0.90 1.70 1 1 4 -13 -1.00 1.30 1 -1 -4 13 1.90 1.70 1 1 4 -12 9.40 1.90 1 -1 -4 12 10.40 2.00 1 1 4 -11 34.20 2.90 1 -1 -4 11 22.00 2.80 1 -1 -4 10 36.00 2.60 1 1 4 -9 101.50 4.80 1 -1 -4 9 90.60 4.80 1 1 4 -8 70.80 5.00 1 -1 -4 8 78.60 4.30 1 1 4 -7 134.40 6.80 1 -1 -4 7 112.40 4.30 1 1 4 -6 194.70 9.10 1 -1 -4 6 144.80 6.30 1 -1 -4 5 46.90 4.60 1 -1 -4 4 441.70 16.40 1 1 4 -3 14.40 2.00 1 -1 -4 3 28.00 2.60 1 1 4 -2 180.40 8.80 1 -1 -4 2 204.40 9.50 1 1 4 -1 607.10 16.00 1 1 4 0 149.20 5.20 1 1 4 1 55.50 2.40 1 1 4 2 395.20 14.80 1 -1 -4 -2 362.60 14.40 1 1 4 3 10.80 2.40 1 -1 -4 -3 19.40 1.90 1 1 4 4 114.30 6.80 1 -1 -4 -4 111.70 5.40 1 1 4 5 292.30 13.00 1 -1 -4 -5 289.90 11.70 1 1 4 6 46.60 3.60 1 -1 -4 -6 28.00 2.70 1 1 4 7 11.30 2.20 1 -1 -4 -7 18.60 2.10 1 1 4 8 37.00 3.00 1 -1 -4 -8 44.60 2.90 1 1 4 9 18.80 2.70 1 -1 -4 -9 13.80 1.90 1 1 4 10 30.00 3.10 1 -1 -4 -10 40.40 3.00 1 1 4 11 5.10 1.90 1 -1 -4 -11 11.30 1.80 1 1 4 12 -3.20 1.70 1 -1 -4 -12 0.20 1.90 1 1 4 13 28.60 3.00 1 -1 -4 -13 29.10 2.50 1 1 4 14 9.80 2.60 1 -1 -4 -14 11.70 2.50 1 1 5 -13 15.20 2.60 1 -1 -5 13 17.00 3.00 1 1 5 -12 11.80 2.20 1 -1 -5 12 21.40 3.30 1 1 5 -11 30.30 2.90 1 -1 -5 11 31.50 2.50 1 1 5 -10 30.50 2.60 1 -1 -5 10 20.60 2.70 1 1 5 -9 -0.20 1.40 1 -1 -5 9 4.60 2.30 1 1 5 -8 39.30 2.50 1 -1 -5 8 42.00 3.70 1 1 5 -7 39.40 3.20 1 -1 -5 7 23.50 3.00 1 1 5 -6 27.20 2.90 1 -1 -5 6 22.60 2.60 1 1 5 -4 44.90 3.30 1 -1 -5 4 50.50 3.40 1 1 5 -3 7.10 1.90 1 -1 -5 3 5.40 2.00 1 1 5 -2 75.40 3.70 1 1 5 -1 8.60 1.50 1 1 5 0 46.20 2.20 1 1 5 1 25.70 3.00 1 1 5 2 200.70 6.60 1 -1 -5 -3 58.90 4.20 1 1 5 4 119.30 6.60 1 -1 -5 -4 122.80 6.30 1 1 5 6 56.00 3.50 1 -1 -5 -6 53.30 3.70 1 1 5 8 110.00 6.30 1 -1 -5 -8 85.10 4.60 1 1 5 9 145.20 8.80 1 -1 -5 -9 138.20 6.40 1 1 5 10 39.70 4.40 1 -1 -5 -10 45.10 3.20 1 1 5 11 2.40 2.40 1 -1 -5 -11 12.80 2.00 1 1 5 12 16.80 2.60 1 -1 -5 -12 10.50 2.40 1 1 6 -11 14.40 2.30 1 -1 -6 11 19.70 2.50 1 1 6 -10 37.80 3.50 1 -1 -6 10 41.60 3.30 1 1 6 -9 4.90 2.00 1 -1 -6 9 4.50 2.00 1 1 6 -8 104.20 7.10 1 -1 -6 8 89.00 5.20 1 1 6 -7 97.60 6.00 1 -1 -6 7 94.20 5.40 1 1 6 -6 23.20 2.90 1 -1 -6 6 22.90 2.80 1 1 6 -5 -3.30 1.70 1 -1 -6 5 -0.80 1.80 1 1 6 -4 6.30 1.60 1 1 6 -3 86.20 3.60 1 1 6 -2 331.20 11.10 1 1 6 -1 31.80 2.50 1 1 6 0 18.00 1.80 1 1 6 1 29.10 3.10 1 1 6 2 24.40 2.10 1 1 6 3 81.90 5.40 1 1 6 4 54.40 3.70 1 -1 -6 -5 19.20 2.70 1 1 6 6 52.90 4.60 1 -1 -6 -6 50.40 3.60 1 1 6 7 15.20 2.70 1 -1 -6 -7 9.40 2.00 1 1 6 8 15.30 2.50 1 -1 -6 -8 6.20 2.00 1 1 6 9 11.20 2.60 1 -1 -6 -9 5.30 2.10 1 1 6 10 -2.70 1.80 1 -1 -6 -10 2.80 2.00 1 1 7 -8 -1.10 2.30 1 -1 -7 8 3.50 2.30 1 1 7 -7 55.90 4.40 1 -1 -7 7 62.70 5.00 1 1 7 -6 34.70 3.40 1 1 7 -5 3.00 2.00 1 1 7 -4 34.30 2.50 1 1 7 -3 13.00 3.10 1 1 7 -2 4.60 2.40 1 1 7 -1 4.30 1.80 1 1 7 0 3.00 1.60 1 1 7 1 21.90 2.20 1 1 7 2 72.40 3.70 1 1 7 3 59.10 3.50 1 1 7 4 11.10 1.80 1 1 7 5 2.00 1.60 1 1 7 6 2.30 1.70 1 1 7 7 52.30 5.20 1 -1 -7 -8 81.10 6.10 1 1 8 -3 33.80 3.10 1 1 8 -2 69.80 5.90 1 1 8 -1 11.50 2.00 1 1 8 0 14.90 2.40 1 1 8 1 16.40 3.50 1 1 8 2 24.70 3.40 1 2 0 -17 17.40 2.60 1 2 0 -16 17.20 2.40 1 2 0 -15 16.90 1.80 1 2 0 -14 -1.70 1.40 1 2 0 -13 14.50 1.90 1 2 0 -12 3.80 1.40 1 2 0 -11 -3.30 1.40 1 2 0 -10 344.90 14.60 1 2 0 -9 10.00 1.40 1 2 0 -8 4.30 0.90 1 2 0 -7 1152.60 40.60 1 2 0 -6 705.90 16.90 1 2 0 -5 1604.30 29.50 1 2 0 -4 37.30 1.30 1 2 0 -3 380.40 7.50 1 2 0 -2 31.20 1.00 1 2 0 -1 915.70 17.30 1 2 0 0 62.30 1.50 1 2 0 1 1141.50 21.40 1 2 0 2 127.80 2.80 1 2 0 3 293.20 6.00 1 2 0 4 626.60 12.30 1 2 0 5 32.10 0.90 1 2 0 6 70.30 2.40 1 2 0 7 88.20 3.20 1 2 0 8 30.00 1.50 1 2 0 9 20.70 1.40 1 2 0 10 11.10 1.50 1 2 0 11 165.60 8.50 1 2 0 12 15.90 1.80 1 2 0 13 36.00 3.20 1 2 0 14 6.90 2.10 1 2 0 15 78.50 5.50 1 2 1 -17 3.50 2.00 1 -2 -1 17 0.60 2.10 1 2 1 -16 19.50 2.30 1 -2 -1 16 9.60 2.60 1 2 1 -15 39.90 3.20 1 -2 -1 15 51.50 3.50 1 2 1 -14 29.90 2.60 1 -2 -1 14 24.10 2.30 1 2 1 -13 15.70 1.80 1 -2 -1 13 13.10 1.50 1 2 1 -12 104.30 6.20 1 -2 -1 12 91.10 3.50 1 2 1 -11 60.30 3.90 1 -2 -1 11 71.90 2.90 1 2 1 -10 22.10 1.70 1 -2 -1 10 17.80 1.60 1 2 1 -9 31.70 1.10 1 -2 -1 9 32.60 1.70 1 2 1 -8 113.70 2.50 1 -2 -1 8 106.90 5.00 1 2 1 -7 130.60 3.80 1 -2 -1 7 129.90 5.70 1 2 1 -6 15.60 1.20 1 -2 -1 6 13.20 0.80 1 2 1 -5 424.20 10.90 1 -2 -1 5 386.20 9.30 1 2 1 -4 589.60 21.00 1 -2 -1 4 575.30 11.30 1 2 1 -3 179.60 4.60 1 -2 -1 3 170.10 3.70 1 2 1 -2 693.80 17.20 1 -2 -1 2 652.90 12.40 1 2 1 -1 1640.90 36.60 1 -2 -1 1 1799.00 41.40 1 2 1 0 2939.90 42.70 1 -2 -1 0 3374.10 107.70 1 2 1 1 510.00 10.50 1 -2 -1 -1 475.20 11.50 1 2 1 2 514.80 9.40 1 -2 -1 -2 483.30 15.90 1 2 1 3 1890.50 37.70 1 -2 -1 -3 1747.60 54.50 1 2 1 4 160.70 3.90 1 -2 -1 -4 180.50 6.60 1 2 1 5 486.90 10.20 1 -2 -1 -5 545.30 19.10 1 2 1 6 149.40 4.20 1 -2 -1 -6 161.60 6.10 1 2 1 7 73.30 2.20 1 -2 -1 -7 85.60 3.60 1 2 1 8 212.80 5.70 1 -2 -1 -8 214.50 9.10 1 2 1 9 202.70 6.50 1 -2 -1 -9 219.10 8.90 1 2 1 10 441.80 13.50 1 -2 -1 -10 460.30 17.00 1 2 1 11 87.80 3.50 1 -2 -1 -11 89.10 4.80 1 2 1 12 71.30 4.50 1 -2 -1 -12 64.70 4.40 1 2 1 13 47.30 3.40 1 -2 -1 -13 41.80 3.60 1 2 1 15 4.80 2.20 1 -2 -1 -15 7.90 2.20 1 2 2 -17 -2.70 1.30 1 -2 -2 17 2.50 2.00 1 2 2 -16 14.20 2.40 1 -2 -2 16 17.40 2.60 1 2 2 -14 27.80 2.40 1 -2 -2 14 19.60 2.60 1 2 2 -13 3.80 1.30 1 -2 -2 13 7.80 1.40 1 2 2 -12 65.90 3.70 1 -2 -2 12 76.10 2.90 1 2 2 -11 37.70 2.80 1 -2 -2 11 28.60 1.80 1 2 2 -10 131.50 7.60 1 -2 -2 10 128.20 4.70 1 2 2 -9 38.80 3.00 1 -2 -2 9 39.70 2.10 1 2 2 -8 88.20 4.30 1 -2 -2 8 68.60 2.70 1 2 2 -7 193.20 7.60 1 -2 -2 7 172.50 5.10 1 2 2 -6 58.20 3.40 1 -2 -2 6 63.30 2.50 1 -2 -2 5 388.40 8.40 1 2 2 -4 264.80 7.50 1 -2 -2 4 253.90 5.70 1 2 2 -3 450.00 9.30 1 -2 -2 3 386.20 16.80 1 2 2 -2 597.30 12.40 1 -2 -2 2 544.60 13.10 1 2 2 -1 62.70 2.10 1 -2 -2 1 59.20 2.70 1 2 2 0 318.30 5.40 1 -2 -2 0 324.80 14.60 1 2 2 1 73.80 2.50 1 -2 -2 -1 52.30 4.70 1 2 2 2 550.50 11.80 1 -2 -2 -2 532.80 18.90 1 2 2 3 94.70 3.40 1 -2 -2 -3 118.20 4.80 1 2 2 4 11.00 0.80 1 -2 -2 -4 11.20 1.30 1 2 2 5 109.80 3.10 1 -2 -2 -5 110.30 4.40 1 2 2 6 135.00 6.80 1 -2 -2 -6 145.80 5.50 1 2 2 7 33.80 3.00 1 -2 -2 -7 38.70 2.30 1 2 2 8 64.40 3.80 1 -2 -2 -8 46.60 2.60 1 2 2 9 25.00 2.10 1 -2 -2 -9 17.00 1.90 1 2 2 10 22.10 2.10 1 -2 -2 -10 27.00 2.20 1 2 2 11 56.10 2.60 1 -2 -2 -11 47.10 3.20 1 2 2 12 72.70 4.80 1 -2 -2 -12 57.50 3.80 1 2 2 13 29.30 3.10 1 -2 -2 -13 22.60 2.50 1 2 2 14 12.50 2.10 1 -2 -2 -14 15.40 2.30 1 2 2 15 3.30 1.90 1 -2 -2 -15 7.20 2.50 1 2 3 -16 15.50 2.50 1 -2 -3 16 14.60 2.40 1 2 3 -15 15.60 2.30 1 -2 -3 15 8.30 2.20 1 2 3 -14 16.90 2.10 1 -2 -3 14 18.30 2.40 1 2 3 -13 42.20 3.20 1 -2 -3 13 28.10 2.80 1 -2 -3 12 79.00 3.50 1 2 3 -11 24.00 2.30 1 -2 -3 11 26.60 2.00 1 2 3 -10 25.20 2.30 1 -2 -3 10 27.70 1.90 1 2 3 -9 112.10 5.80 1 -2 -3 9 126.20 6.70 1 2 3 -8 279.20 13.20 1 -2 -3 8 244.40 10.00 1 2 3 -7 110.70 4.80 1 -2 -3 7 92.70 3.80 1 2 3 -6 1.60 1.00 1 -2 -3 6 -1.60 1.40 1 -2 -3 5 15.90 2.90 1 2 3 -4 125.10 4.90 1 -2 -3 3 63.90 2.90 1 2 3 -2 399.80 10.60 1 -2 -3 2 440.70 17.50 1 2 3 -1 13.20 1.70 1 -2 -3 1 21.00 3.70 1 2 3 0 103.90 2.80 1 2 3 1 654.70 17.00 1 2 3 2 1114.00 29.00 1 -2 -3 -2 1135.90 40.50 1 2 3 3 295.00 11.30 1 -2 -3 -3 287.70 11.60 1 2 3 4 65.90 2.70 1 -2 -3 -4 71.80 3.70 1 2 3 5 76.20 4.60 1 -2 -3 -5 86.60 4.00 1 2 3 6 352.60 10.30 1 -2 -3 -6 324.50 12.30 1 2 3 7 139.70 4.70 1 -2 -3 -7 149.10 6.40 1 2 3 8 4.40 1.90 1 -2 -3 -8 0.00 1.50 1 2 3 9 20.40 2.20 1 -2 -3 -9 20.50 2.40 1 2 3 10 -2.70 1.90 1 -2 -3 -10 6.40 1.80 1 2 3 11 41.20 3.20 1 -2 -3 -11 42.10 3.00 1 2 3 12 111.50 6.60 1 -2 -3 -12 129.00 6.20 1 2 3 13 14.70 2.30 1 -2 -3 -13 15.60 2.80 1 2 3 14 -2.20 1.90 1 -2 -3 -14 2.10 2.30 1 2 4 -15 5.10 1.80 1 -2 -4 15 7.60 1.90 1 2 4 -14 31.70 2.90 1 -2 -4 14 42.40 3.30 1 2 4 -13 -1.80 1.90 1 -2 -4 13 4.60 1.50 1 2 4 -12 46.10 3.70 1 -2 -4 12 30.70 3.10 1 2 4 -11 8.50 1.70 1 -2 -4 11 10.00 1.70 1 2 4 -10 104.80 5.70 1 -2 -4 10 110.50 4.80 1 2 4 -9 133.30 6.70 1 -2 -4 9 102.10 4.90 1 2 4 -8 81.60 5.00 1 -2 -4 8 87.80 4.80 1 2 4 -7 46.00 2.70 1 -2 -4 7 46.00 2.90 1 2 4 -6 42.10 2.80 1 -2 -4 6 46.50 2.50 1 -2 -4 5 9.70 1.70 1 2 4 -4 117.60 4.90 1 -2 -4 4 129.70 7.30 1 2 4 -3 408.30 15.60 1 -2 -4 3 349.20 13.90 1 2 4 -2 89.70 3.30 1 2 4 -1 85.70 4.90 1 2 4 0 26.70 1.70 1 2 4 1 97.80 5.50 1 2 4 2 326.00 14.10 1 2 4 3 13.70 2.30 1 -2 -4 -3 14.30 2.10 1 2 4 4 15.50 2.30 1 -2 -4 -4 20.50 2.20 1 2 4 5 41.60 3.10 1 2 4 6 98.60 5.50 1 -2 -4 -6 98.50 4.80 1 2 4 7 31.40 2.70 1 -2 -4 -7 22.10 2.30 1 2 4 8 140.30 8.10 1 -2 -4 -8 135.60 6.80 1 2 4 9 6.50 2.20 1 2 4 10 9.40 2.20 1 -2 -4 -10 14.40 2.30 1 2 4 11 73.80 4.50 1 -2 -4 -11 67.10 4.10 1 2 4 12 36.50 3.40 1 -2 -4 -12 36.50 3.10 1 -2 -4 -13 1.80 1.80 1 2 5 -13 16.90 2.60 1 -2 -5 13 29.10 3.20 1 2 5 -12 7.60 2.00 1 -2 -5 12 5.20 2.10 1 2 5 -11 93.30 6.30 1 -2 -5 11 106.20 4.50 1 2 5 -10 2.60 1.50 1 -2 -5 10 1.90 1.60 1 2 5 -8 97.70 5.30 1 -2 -5 8 100.20 4.60 1 2 5 -7 36.00 2.90 1 -2 -5 7 47.50 2.90 1 2 5 -6 54.60 3.50 1 -2 -5 6 35.20 2.50 1 2 5 -5 42.10 3.50 1 -2 -5 5 32.90 3.10 1 2 5 -4 8.80 2.00 1 -2 -5 4 2.10 2.30 1 2 5 -3 1.60 1.50 1 2 5 -2 73.50 3.90 1 2 5 -1 120.70 5.50 1 2 5 0 94.10 3.60 1 2 5 1 201.40 6.50 1 2 5 2 103.20 5.40 1 2 5 4 2.00 1.70 1 -2 -5 -4 9.10 2.00 1 2 5 5 88.30 5.40 1 -2 -5 -5 69.00 4.30 1 2 5 6 94.40 5.60 1 -2 -5 -6 79.10 4.60 1 2 5 7 149.80 9.30 1 -2 -5 -7 124.10 6.40 1 2 5 9 -1.30 1.70 1 2 5 10 25.70 3.10 1 -2 -5 -10 42.90 3.70 1 2 5 11 29.90 3.60 1 -2 -5 -11 31.50 3.00 1 2 6 -11 9.80 2.10 1 -2 -6 11 6.90 2.30 1 2 6 -10 0.00 1.60 1 -2 -6 10 -1.90 2.10 1 2 6 -9 47.70 3.90 1 -2 -6 9 51.80 4.20 1 2 6 -8 22.70 2.50 1 -2 -6 8 23.70 2.90 1 2 6 -7 4.20 1.80 1 -2 -6 7 6.60 2.30 1 2 6 -6 2.30 1.60 1 -2 -6 6 9.50 2.00 1 -2 -6 5 72.90 4.50 1 2 6 -4 112.10 4.30 1 2 6 -3 71.90 3.40 1 2 6 -2 9.90 1.50 1 2 6 -1 40.00 2.30 1 2 6 0 13.30 1.70 1 2 6 1 87.90 3.60 1 2 6 2 114.50 5.30 1 2 6 3 34.50 2.60 1 2 6 4 92.50 4.00 1 2 6 5 22.40 2.90 1 -2 -6 -5 12.20 2.70 1 -2 -6 -6 13.10 2.10 1 2 6 7 5.40 2.10 1 -2 -6 -7 -3.70 1.90 1 2 6 8 0.00 1.90 1 -2 -6 -8 12.50 2.30 1 2 6 9 10.40 2.20 1 -2 -6 -9 7.30 2.60 1 2 6 10 3.50 2.50 1 -2 -6 -10 19.70 2.90 1 2 7 -9 23.40 3.10 1 -2 -7 9 30.00 3.30 1 2 7 -8 2.00 2.10 1 -2 -7 8 11.00 2.70 1 2 7 -7 12.00 2.40 1 -2 -7 7 7.60 2.60 1 2 7 -6 20.80 2.70 1 2 7 -5 18.50 2.60 1 2 7 -4 20.60 2.20 1 2 7 -3 0.00 1.40 1 2 7 -2 2.30 3.10 1 2 7 -1 140.00 5.60 1 2 7 0 38.70 2.70 1 2 7 1 47.90 3.20 1 2 7 2 29.60 2.50 1 2 7 3 32.20 3.70 1 2 7 4 4.30 2.40 1 2 7 5 39.90 3.00 1 2 7 6 22.80 2.20 1 -2 -7 -7 29.90 4.00 1 3 0 -17 -3.00 2.00 1 3 0 -16 0.80 1.30 1 3 0 -15 0.00 2.00 1 3 0 -14 1.70 1.70 1 3 0 -13 -0.10 1.70 1 3 0 -12 35.50 2.70 1 3 0 -11 -0.30 1.10 1 3 0 -10 21.10 1.80 1 3 0 -9 92.00 4.40 1 3 0 -8 117.80 4.70 1 3 0 -6 9.70 0.80 1 3 0 -5 71.40 2.20 1 3 0 -4 1022.10 19.30 1 3 0 -3 1011.20 23.30 1 3 0 -2 14.20 0.60 1 3 0 -1 3.10 0.50 1 3 0 0 -0.40 0.70 1 3 0 1 572.60 11.50 1 3 0 2 1336.20 25.80 1 3 0 3 296.20 5.60 1 3 0 4 80.80 2.80 1 3 0 5 471.50 12.40 1 3 0 6 231.10 6.60 1 3 0 7 445.60 12.60 1 3 0 8 2.80 1.00 1 3 0 9 77.50 3.50 1 3 0 11 12.00 1.90 1 3 0 12 20.50 2.00 1 3 0 13 5.00 1.90 1 3 0 14 1.40 1.90 1 3 0 15 13.10 2.50 1 3 1 -17 0.10 1.90 1 -3 -1 17 4.60 1.60 1 3 1 -16 2.20 1.80 1 3 1 -15 14.60 2.00 1 -3 -1 15 23.90 2.00 1 3 1 -14 25.00 2.20 1 -3 -1 14 30.90 2.20 1 3 1 -13 28.70 2.50 1 -3 -1 13 33.80 2.30 1 3 1 -12 77.70 5.40 1 -3 -1 12 79.00 3.70 1 3 1 -11 96.50 4.50 1 -3 -1 11 73.40 3.00 1 3 1 -10 22.80 1.60 1 -3 -1 10 18.90 2.50 1 3 1 -9 201.80 5.10 1 -3 -1 9 207.60 6.20 1 3 1 -8 375.00 9.30 1 -3 -1 8 336.10 9.20 1 3 1 -7 62.20 2.80 1 -3 -1 7 60.90 3.90 1 3 1 -6 105.90 4.00 1 -3 -1 6 106.30 3.30 1 3 1 -5 47.00 1.70 1 -3 -1 5 59.00 2.40 1 3 1 -4 112.90 2.70 1 -3 -1 4 122.40 6.00 1 3 1 -3 781.10 18.40 1 -3 -1 3 737.40 14.80 1 3 1 -2 116.30 2.80 1 -3 -1 2 120.20 3.50 1 3 1 -1 659.90 15.30 1 -3 -1 1 637.00 23.10 1 3 1 0 179.30 3.50 1 -3 -1 0 177.30 5.20 1 3 1 1 207.80 4.20 1 -3 -1 -1 217.90 5.70 1 3 1 2 119.10 2.80 1 -3 -1 -2 115.00 3.40 1 3 1 3 469.20 10.60 1 -3 -1 -3 519.40 10.40 1 3 1 4 185.60 4.60 1 -3 -1 -4 201.90 5.50 1 3 1 5 47.10 2.20 1 -3 -1 -5 62.60 2.90 1 3 1 6 428.80 10.50 1 -3 -1 -6 399.50 14.30 1 3 1 7 38.00 1.60 1 -3 -1 -7 36.10 2.30 1 3 1 8 173.40 6.10 1 -3 -1 -8 178.20 8.30 1 3 1 9 11.70 1.30 1 -3 -1 -9 15.00 1.80 1 3 1 10 93.00 3.30 1 -3 -1 -10 105.10 6.10 1 3 1 11 70.70 2.80 1 -3 -1 -11 64.80 4.40 1 3 1 12 99.10 6.20 1 -3 -1 -12 88.40 5.40 1 3 1 13 19.00 2.70 1 -3 -1 -13 16.80 2.60 1 3 1 14 2.40 1.80 1 -3 -1 -14 3.40 2.10 1 3 2 -17 8.60 2.10 1 -3 -2 17 13.70 2.30 1 3 2 -16 16.40 2.60 1 -3 -2 16 17.00 2.60 1 3 2 -15 8.70 1.70 1 -3 -2 15 6.50 1.40 1 3 2 -14 5.90 1.40 1 -3 -2 14 13.60 1.60 1 3 2 -13 31.50 2.30 1 -3 -2 13 25.60 1.70 1 3 2 -12 8.80 1.60 1 -3 -2 12 5.00 1.50 1 3 2 -11 4.00 1.10 1 -3 -2 11 10.80 1.70 1 3 2 -10 61.10 2.50 1 -3 -2 10 67.10 4.70 1 3 2 -9 36.70 2.20 1 -3 -2 9 34.50 2.10 1 -3 -2 8 36.00 1.90 1 3 2 -7 39.80 2.00 1 -3 -2 7 46.00 3.00 1 -3 -2 6 389.30 10.70 1 3 2 -5 208.50 7.90 1 -3 -2 5 182.60 6.00 1 3 2 -4 208.00 7.90 1 -3 -2 4 211.50 6.30 1 -3 -2 3 488.00 10.40 1 3 2 -2 366.00 9.20 1 -3 -2 2 361.40 10.10 1 3 2 -1 135.10 3.90 1 -3 -2 1 144.10 7.40 1 3 2 0 420.80 7.40 1 -3 -2 0 457.50 18.70 1 3 2 1 597.80 15.50 1 -3 -2 -1 663.20 17.80 1 3 2 2 222.30 5.50 1 3 2 3 492.10 11.10 1 -3 -2 -3 548.00 19.90 1 3 2 4 148.50 4.90 1 -3 -2 -4 133.20 5.30 1 3 2 5 151.00 4.30 1 -3 -2 -5 150.10 6.00 1 3 2 6 28.40 2.30 1 -3 -2 -6 17.10 1.70 1 3 2 7 130.30 7.90 1 -3 -2 -7 121.10 5.40 1 3 2 8 158.50 7.30 1 -3 -2 -8 135.40 5.80 1 3 2 9 70.80 4.50 1 -3 -2 -9 68.80 3.90 1 3 2 10 86.30 3.70 1 -3 -2 -10 72.00 3.70 1 3 2 11 33.60 2.00 1 -3 -2 -11 32.10 2.60 1 3 2 12 21.70 2.70 1 -3 -2 -12 21.20 2.40 1 3 2 13 31.90 3.20 1 -3 -2 -13 25.90 2.60 1 3 2 14 20.50 2.40 1 -3 -2 -14 22.90 3.20 1 3 3 -16 18.20 2.10 1 -3 -3 16 10.10 2.10 1 3 3 -15 8.00 2.10 1 -3 -3 15 14.20 2.40 1 3 3 -14 29.40 2.60 1 -3 -3 14 21.10 2.20 1 3 3 -13 -1.50 1.10 1 -3 -3 13 1.40 1.50 1 3 3 -12 37.20 3.20 1 -3 -3 12 43.80 2.60 1 3 3 -11 10.60 1.70 1 -3 -3 11 10.20 1.60 1 3 3 -10 135.60 6.90 1 -3 -3 10 155.20 7.00 1 3 3 -9 229.00 9.80 1 -3 -3 9 197.00 10.90 1 3 3 -8 66.40 4.00 1 -3 -3 8 73.80 3.00 1 3 3 -7 114.40 4.60 1 -3 -3 7 97.00 6.00 1 -3 -3 6 109.00 4.20 1 3 3 -5 125.20 5.70 1 -3 -3 5 117.50 3.70 1 3 3 -4 71.10 3.30 1 -3 -3 4 91.70 3.70 1 3 3 -3 10.10 1.20 1 -3 -3 3 8.20 1.10 1 3 3 -2 60.30 2.40 1 -3 -3 2 65.00 3.30 1 3 3 -1 664.90 17.30 1 -3 -3 1 628.20 24.10 1 3 3 0 202.30 5.60 1 -3 -3 0 206.80 9.60 1 3 3 1 174.70 8.50 1 -3 -3 -1 184.60 9.30 1 3 3 2 7.70 0.90 1 -3 -3 -2 14.50 1.60 1 3 3 4 336.90 10.60 1 -3 -3 -4 379.10 14.30 1 3 3 5 262.90 12.80 1 -3 -3 -5 265.10 11.40 1 3 3 6 28.40 2.20 1 -3 -3 -6 37.00 2.50 1 3 3 7 60.70 3.90 1 -3 -3 -7 51.70 2.80 1 3 3 8 115.10 6.20 1 -3 -3 -8 98.30 5.20 1 3 3 9 65.20 4.50 1 -3 -3 -9 56.10 3.60 1 3 3 10 113.10 6.80 1 -3 -3 -10 90.40 4.40 1 3 3 11 21.90 2.30 1 -3 -3 -11 20.60 2.50 1 3 3 12 14.50 2.30 1 -3 -3 -12 19.10 2.90 1 3 3 13 14.70 2.40 1 -3 -3 -13 9.80 2.10 1 3 4 -15 16.30 2.10 1 -3 -4 15 8.90 2.10 1 3 4 -14 7.60 1.50 1 -3 -4 14 1.60 2.20 1 3 4 -13 4.10 1.40 1 -3 -4 13 8.70 2.00 1 3 4 -12 11.70 1.80 1 -3 -4 12 9.30 1.90 1 3 4 -11 42.70 3.10 1 -3 -4 11 57.40 3.10 1 3 4 -10 -0.70 1.30 1 -3 -4 10 -1.40 1.30 1 3 4 -9 35.30 2.30 1 -3 -4 9 28.60 2.00 1 3 4 -8 53.90 3.30 1 -3 -4 8 41.50 2.50 1 -3 -4 7 2.50 1.40 1 3 4 -5 314.20 13.30 1 -3 -4 5 270.20 13.70 1 3 4 -4 15.70 1.40 1 -3 -4 4 20.60 2.00 1 3 4 -3 24.50 1.90 1 -3 -4 3 14.10 4.50 1 3 4 -2 150.90 7.10 1 -3 -4 2 159.30 8.70 1 3 4 -1 194.50 8.50 1 3 4 0 234.00 6.80 1 3 4 1 25.40 2.80 1 3 4 2 41.90 3.40 1 -3 -4 -2 42.20 2.70 1 3 4 3 105.40 7.50 1 -3 -4 -3 125.00 5.80 1 -3 -4 -4 44.40 2.80 1 3 4 5 100.10 6.80 1 -3 -4 -5 65.00 3.80 1 3 4 6 32.60 3.60 1 -3 -4 -6 50.80 2.90 1 3 4 7 24.30 2.20 1 3 4 8 55.80 4.30 1 -3 -4 -8 68.30 4.30 1 3 4 9 127.40 6.90 1 -3 -4 -9 120.50 6.30 1 3 4 10 0.90 2.00 1 -3 -4 -10 10.90 2.20 1 3 4 11 20.20 2.50 1 -3 -4 -11 15.30 2.00 1 3 4 12 51.30 4.60 1 -3 -4 -12 67.50 4.90 1 3 5 -13 13.40 2.00 1 -3 -5 13 10.10 2.00 1 3 5 -12 8.30 1.70 1 -3 -5 12 10.00 1.70 1 3 5 -11 25.30 2.70 1 -3 -5 11 20.90 2.10 1 3 5 -10 78.70 4.40 1 -3 -5 10 61.30 3.20 1 3 5 -9 18.50 2.10 1 -3 -5 9 7.10 2.30 1 3 5 -8 80.00 4.40 1 -3 -5 8 68.70 4.60 1 3 5 -7 67.20 3.90 1 -3 -5 7 60.50 3.20 1 3 5 -6 6.40 1.60 1 -3 -5 6 7.60 3.80 1 3 5 -5 28.20 2.10 1 -3 -5 5 32.60 2.30 1 3 5 -3 43.90 4.10 1 3 5 -2 213.00 10.30 1 3 5 -1 212.90 6.50 1 3 5 1 235.40 7.70 1 3 5 2 45.80 2.60 1 3 5 3 123.30 6.90 1 -3 -5 -3 121.00 6.90 1 3 5 4 138.90 7.80 1 -3 -5 -4 149.80 7.40 1 3 5 5 91.30 6.40 1 -3 -5 -5 88.90 5.00 1 3 5 6 64.60 4.50 1 -3 -5 -6 85.00 5.30 1 3 5 7 20.50 2.40 1 3 5 8 32.30 3.40 1 -3 -5 -8 35.80 3.30 1 3 5 9 -0.20 1.70 1 -3 -5 -9 10.50 2.20 1 3 5 10 43.80 3.90 1 -3 -5 -10 34.90 3.50 1 3 5 11 12.50 2.60 1 -3 -5 -11 5.90 2.20 1 3 6 -11 12.10 2.30 1 -3 -6 11 17.20 2.60 1 3 6 -10 4.10 1.80 1 -3 -6 10 12.90 2.10 1 3 6 -9 34.40 3.20 1 -3 -6 9 38.80 3.50 1 -3 -6 8 9.90 2.30 1 3 6 -6 27.10 2.60 1 -3 -6 6 38.00 3.20 1 3 6 -5 50.70 2.70 1 3 6 -3 46.90 2.80 1 3 6 -2 2.50 1.60 1 3 6 -1 7.10 1.50 1 3 6 0 51.00 3.90 1 3 6 1 75.90 5.90 1 3 6 2 21.50 2.10 1 3 6 3 8.00 1.70 1 3 6 4 3.90 1.50 1 3 6 5 35.20 3.40 1 -3 -6 -5 35.30 3.30 1 3 6 6 4.70 2.40 1 -3 -6 -6 8.80 2.60 1 3 6 7 39.00 4.40 1 -3 -6 -7 17.50 2.90 1 3 6 8 60.10 4.80 1 -3 -6 -8 49.60 3.60 1 3 7 -8 39.00 3.40 1 -3 -7 8 50.90 4.00 1 3 7 -7 22.50 2.20 1 3 7 -6 14.00 1.80 1 3 7 -5 3.30 1.50 1 3 7 -4 10.10 1.90 1 3 7 -3 42.40 3.00 1 3 7 -2 79.30 6.60 1 3 7 -1 6.50 1.80 1 3 7 0 26.00 2.20 1 3 7 1 80.90 4.10 1 3 7 2 51.80 2.90 1 3 7 3 26.30 2.40 1 3 7 4 19.20 2.20 1 3 7 5 31.20 2.70 1 4 0 -17 15.10 1.80 1 4 0 -16 9.00 1.50 1 4 0 -15 29.40 2.20 1 4 0 -14 8.90 1.80 1 4 0 -13 1.30 1.30 1 4 0 -12 77.70 4.20 1 4 0 -11 21.00 2.10 1 4 0 -10 25.20 1.90 1 4 0 -9 -2.30 1.00 1 4 0 -8 10.50 1.30 1 4 0 -7 1.30 1.20 1 4 0 -6 876.00 20.80 1 4 0 -5 1.40 0.50 1 4 0 -4 22.20 0.80 1 4 0 -3 131.70 3.80 1 4 0 -2 1613.30 37.00 1 4 0 -1 1329.30 22.00 1 4 0 0 365.20 6.70 1 4 0 1 8.80 0.70 1 4 0 2 53.20 1.30 1 4 0 3 218.90 6.60 1 4 0 4 55.30 2.20 1 4 0 5 497.30 13.90 1 4 0 6 2.00 0.80 1 4 0 7 9.60 1.10 1 4 0 8 322.20 10.50 1 4 0 9 1.40 1.30 1 4 0 10 133.00 5.10 1 4 0 11 9.80 1.70 1 4 0 12 -1.70 1.50 1 4 0 13 81.10 6.20 1 4 0 14 36.70 3.80 1 4 1 -17 5.10 1.70 1 -4 -1 17 8.60 2.30 1 4 1 -16 13.10 2.40 1 -4 -1 16 7.00 1.50 1 4 1 -15 2.90 1.60 1 -4 -1 15 8.80 1.50 1 4 1 -14 1.70 1.60 1 -4 -1 14 5.40 1.40 1 4 1 -13 2.10 1.60 1 -4 -1 13 -0.50 1.20 1 4 1 -12 50.40 3.50 1 -4 -1 12 45.80 2.20 1 4 1 -11 70.30 3.80 1 -4 -1 11 92.20 3.90 1 4 1 -10 122.60 3.60 1 -4 -1 10 133.10 6.10 1 4 1 -9 20.00 0.90 1 -4 -1 9 20.60 1.40 1 4 1 -8 38.10 1.20 1 -4 -1 8 45.80 2.10 1 4 1 -7 107.80 2.70 1 -4 -1 7 106.30 5.90 1 4 1 -6 158.00 6.50 1 -4 -1 6 146.70 4.40 1 4 1 -5 122.70 2.90 1 -4 -1 5 134.80 4.00 1 4 1 -4 19.30 1.00 1 -4 -1 4 21.40 2.50 1 4 1 -3 519.60 12.40 1 -4 -1 3 456.80 9.40 1 4 1 -2 269.10 9.80 1 -4 -1 2 270.00 6.20 1 4 1 -1 404.10 10.50 1 -4 -1 1 431.60 15.90 1 4 1 0 225.10 11.90 1 -4 -1 0 198.60 6.00 1 4 1 1 22.60 1.40 1 -4 -1 -1 18.70 0.90 1 4 1 2 55.30 1.70 1 -4 -1 -2 58.00 1.90 1 4 1 3 448.80 7.70 1 -4 -1 -3 446.00 11.40 1 4 1 4 271.50 6.80 1 -4 -1 -4 270.00 7.00 1 4 1 5 71.50 2.40 1 -4 -1 -5 74.90 2.70 1 4 1 6 19.70 1.20 1 -4 -1 -6 29.30 2.10 1 4 1 7 43.10 2.40 1 -4 -1 -7 47.50 2.90 1 4 1 8 105.20 4.20 1 -4 -1 -8 85.70 4.40 1 4 1 9 120.10 4.50 1 -4 -1 -9 98.60 5.40 1 4 1 10 27.50 1.80 1 -4 -1 -10 24.90 2.50 1 4 1 11 41.30 2.40 1 -4 -1 -11 50.40 3.40 1 4 1 12 18.00 1.80 1 -4 -1 -12 9.40 1.90 1 4 1 13 4.50 1.80 1 -4 -1 -13 6.30 2.10 1 4 2 -17 17.00 2.20 1 -4 -2 17 13.30 2.50 1 4 2 -16 7.40 2.10 1 -4 -2 16 13.60 1.80 1 4 2 -15 14.90 2.00 1 -4 -2 15 8.50 1.70 1 4 2 -14 1.20 1.60 1 -4 -2 14 -1.00 1.10 1 -4 -2 13 26.60 1.80 1 4 2 -12 66.60 3.70 1 -4 -2 12 57.50 2.60 1 4 2 -11 19.00 1.10 1 -4 -2 11 17.20 1.40 1 4 2 -10 148.70 4.20 1 -4 -2 10 116.00 4.60 1 4 2 -9 76.10 3.40 1 -4 -2 9 62.70 3.40 1 4 2 -8 146.60 5.90 1 -4 -2 8 131.60 5.40 1 4 2 -7 157.20 6.10 1 -4 -2 7 134.00 7.00 1 4 2 -6 49.30 2.60 1 -4 -2 6 54.80 2.10 1 -4 -2 5 149.10 4.80 1 4 2 -4 88.00 3.60 1 -4 -2 4 82.40 3.00 1 4 2 -3 68.70 2.80 1 -4 -2 3 72.60 2.80 1 4 2 -2 309.30 6.40 1 -4 -2 2 328.60 14.80 1 4 2 -1 362.00 9.20 1 -4 -2 1 348.80 15.70 1 4 2 0 217.00 6.00 1 -4 -2 0 195.50 9.50 1 4 2 1 528.70 12.80 1 -4 -2 -1 541.70 21.70 1 4 2 2 73.10 2.50 1 -4 -2 -2 73.70 2.90 1 4 2 3 103.60 3.10 1 -4 -2 -3 98.50 4.40 1 4 2 4 55.00 2.10 1 -4 -2 -4 62.40 3.20 1 4 2 5 25.00 2.30 1 -4 -2 -5 36.80 2.50 1 4 2 6 249.70 13.00 1 -4 -2 -6 217.30 8.90 1 4 2 8 89.10 3.70 1 -4 -2 -8 67.20 4.10 1 4 2 9 83.70 3.70 1 -4 -2 -9 82.60 4.80 1 4 2 10 93.90 4.00 1 -4 -2 -10 97.60 5.60 1 4 2 11 34.20 3.20 1 -4 -2 -11 39.00 3.10 1 4 2 12 80.50 6.10 1 -4 -2 -12 86.80 6.00 1 4 2 13 53.60 4.70 1 -4 -2 -13 46.30 3.90 1 4 3 -16 7.80 1.90 1 -4 -3 16 5.40 2.20 1 4 3 -15 29.50 2.80 1 -4 -3 15 32.30 2.40 1 4 3 -14 -1.40 1.30 1 -4 -3 14 0.50 1.40 1 4 3 -13 2.60 1.50 1 -4 -3 13 1.30 1.40 1 4 3 -12 60.30 3.20 1 -4 -3 12 56.40 2.80 1 4 3 -11 98.00 4.80 1 -4 -3 11 81.30 3.50 1 -4 -3 10 10.80 1.80 1 4 3 -9 34.80 2.30 1 -4 -3 9 22.20 2.00 1 4 3 -8 8.70 1.00 1 -4 -3 8 7.10 1.50 1 4 3 -7 57.30 2.60 1 -4 -3 7 47.10 2.50 1 4 3 -6 37.60 2.20 1 -4 -3 6 39.30 2.20 1 4 3 -5 23.80 1.50 1 -4 -3 5 16.00 1.70 1 4 3 -4 181.00 7.00 1 -4 -3 4 166.10 5.00 1 4 3 -3 124.70 4.70 1 -4 -3 3 135.00 7.50 1 4 3 -2 192.20 8.00 1 -4 -3 2 160.50 8.40 1 4 3 -1 45.20 1.40 1 -4 -3 1 60.50 4.50 1 4 3 0 55.80 1.80 1 4 3 1 0.60 0.40 1 -4 -3 -1 -0.30 2.90 1 4 3 2 121.20 3.80 1 4 3 3 194.20 7.80 1 -4 -3 -3 212.30 9.10 1 -4 -3 -4 68.50 3.90 1 4 3 5 244.30 10.10 1 -4 -3 -5 195.80 7.90 1 -4 -3 -6 67.50 3.90 1 4 3 7 66.10 3.50 1 -4 -3 -7 55.40 3.20 1 4 3 8 118.70 7.90 1 -4 -3 -8 112.80 6.00 1 4 3 9 2.80 1.50 1 -4 -3 -9 0.60 1.60 1 4 3 10 38.40 3.50 1 -4 -3 -10 34.30 3.00 1 4 3 11 52.90 4.50 1 -4 -3 -11 55.40 4.50 1 4 3 12 1.10 1.60 1 -4 -3 -12 3.00 2.00 1 4 4 -15 0.00 1.60 1 -4 -4 15 3.90 1.80 1 4 4 -14 15.00 2.10 1 -4 -4 14 5.30 1.60 1 4 4 -13 37.00 3.10 1 -4 -4 13 25.70 2.30 1 4 4 -12 8.60 1.40 1 -4 -4 12 4.70 2.00 1 4 4 -11 24.00 2.10 1 -4 -4 11 21.10 3.00 1 4 4 -10 59.70 3.10 1 -4 -4 10 56.60 3.00 1 4 4 -9 10.10 1.70 1 -4 -4 9 6.70 2.20 1 4 4 -8 108.00 4.50 1 -4 -4 8 120.30 4.50 1 4 4 -7 21.60 2.00 1 -4 -4 7 23.90 2.20 1 4 4 -6 38.70 1.90 1 -4 -4 6 36.50 4.80 1 4 4 -5 66.80 3.10 1 -4 -4 5 66.10 3.00 1 4 4 -4 18.50 1.80 1 -4 -4 4 16.70 1.90 1 4 4 -3 25.70 1.60 1 -4 -4 3 18.00 4.00 1 4 4 -2 235.20 11.20 1 -4 -4 2 228.50 10.80 1 4 4 -1 110.70 4.20 1 -4 -4 1 120.70 7.90 1 4 4 0 149.20 8.60 1 -4 -4 0 158.80 8.90 1 4 4 1 581.60 16.40 1 4 4 2 34.40 1.90 1 4 4 3 48.40 3.80 1 -4 -4 -3 66.10 4.00 1 4 4 4 12.50 2.30 1 -4 -4 -4 9.50 1.80 1 4 4 5 14.00 2.50 1 4 4 6 61.90 4.80 1 -4 -4 -6 65.60 3.80 1 -4 -4 -7 32.10 2.70 1 4 4 8 3.30 2.20 1 -4 -4 -8 7.40 2.10 1 4 4 9 34.20 3.50 1 -4 -4 -9 32.20 3.00 1 4 4 10 17.60 2.50 1 -4 -4 -10 12.80 2.10 1 4 4 11 21.20 2.60 1 -4 -4 -11 15.40 2.10 1 4 5 -13 12.20 1.80 1 -4 -5 13 14.30 2.90 1 4 5 -12 18.10 2.00 1 -4 -5 12 11.20 1.90 1 4 5 -11 11.80 1.90 1 -4 -5 11 6.60 1.60 1 4 5 -10 38.80 2.40 1 -4 -5 10 50.10 3.10 1 4 5 -9 28.00 2.00 1 -4 -5 9 25.20 2.20 1 4 5 -8 -1.00 1.30 1 -4 -5 8 -0.50 1.50 1 -4 -5 7 20.60 2.20 1 4 5 -6 3.00 1.10 1 -4 -5 6 4.50 1.90 1 4 5 -5 26.90 2.40 1 -4 -5 5 33.10 2.40 1 4 5 -4 71.30 3.60 1 -4 -5 4 50.90 5.70 1 4 5 -3 26.50 1.90 1 -4 -5 3 30.30 4.50 1 4 5 -2 4.00 2.50 1 4 5 -1 7.30 1.40 1 4 5 0 87.00 5.20 1 4 5 1 37.40 2.80 1 4 5 2 132.30 6.00 1 4 5 3 8.40 1.40 1 4 5 4 99.20 6.80 1 -4 -5 -4 104.10 5.50 1 4 5 5 94.00 6.80 1 -4 -5 -5 79.10 5.40 1 4 5 6 6.10 2.50 1 -4 -5 -6 8.50 1.90 1 4 5 7 21.40 2.70 1 -4 -5 -7 23.40 2.60 1 4 5 8 31.90 3.40 1 4 5 9 37.90 4.50 1 4 5 10 23.60 3.40 1 4 6 -11 13.60 2.30 1 -4 -6 11 20.50 2.20 1 4 6 -10 -1.70 1.20 1 -4 -6 10 1.70 1.80 1 -4 -6 9 4.80 1.80 1 4 6 -8 15.20 2.00 1 -4 -6 8 12.10 3.70 1 4 6 -7 13.60 1.60 1 -4 -6 7 6.20 3.90 1 -4 -6 6 89.30 5.20 1 4 6 -4 8.50 2.00 1 4 6 -3 27.50 3.90 1 4 6 -2 24.10 3.30 1 4 6 -1 164.60 7.40 1 4 6 0 77.00 3.20 1 4 6 1 16.20 1.80 1 4 6 2 27.90 2.10 1 4 6 3 22.40 3.90 1 4 6 4 9.50 2.90 1 4 6 5 37.30 4.20 1 4 6 6 14.60 2.90 1 4 6 7 14.20 2.70 1 4 7 -7 7.70 1.50 1 4 7 -6 0.60 1.30 1 4 7 -5 11.50 1.90 1 4 7 -4 2.70 1.40 1 4 7 -3 0.10 1.20 1 4 7 -2 39.10 4.80 1 4 7 -1 29.50 3.60 1 4 7 0 -6.60 2.50 1 4 7 1 17.30 3.40 1 4 7 2 11.60 2.90 1 4 7 3 26.20 3.30 1 4 7 4 67.90 5.20 1 5 0 -17 -0.70 1.50 1 5 0 -16 8.10 1.50 1 5 0 -15 10.20 1.40 1 5 0 -14 7.20 1.70 1 5 0 -11 3.20 1.00 1 5 0 -10 142.20 6.50 1 5 0 -9 395.40 14.20 1 5 0 -8 692.60 17.00 1 5 0 -7 -0.70 1.20 1 5 0 -6 0.40 0.40 1 5 0 -5 60.50 2.20 1 5 0 -4 83.60 2.60 1 5 0 -3 1603.00 30.80 1 5 0 -2 6.70 0.60 1 5 0 -1 25.40 1.00 1 5 0 0 65.40 1.60 1 5 0 1 40.80 1.10 1 5 0 2 0.50 0.60 1 5 0 3 195.50 4.60 1 5 0 4 0.60 0.50 1 5 0 5 93.10 3.30 1 5 0 7 94.20 3.90 1 5 0 8 7.30 1.20 1 5 0 9 65.60 3.00 1 5 0 10 8.80 1.40 1 5 0 11 111.50 7.30 1 5 0 12 29.10 3.10 1 5 1 -17 4.00 1.70 1 -5 -1 17 3.90 1.50 1 -5 -1 16 1.00 1.40 1 5 1 -15 5.20 2.00 1 -5 -1 15 3.60 1.40 1 -5 -1 14 11.10 1.50 1 5 1 -13 57.30 3.70 1 -5 -1 13 49.30 2.90 1 5 1 -12 15.90 1.70 1 -5 -1 12 8.70 1.30 1 5 1 -11 14.00 1.00 1 -5 -1 11 9.40 2.50 1 5 1 -10 19.00 1.10 1 -5 -1 10 20.60 1.60 1 5 1 -9 262.10 10.30 1 -5 -1 9 259.60 7.70 1 5 1 -8 8.10 0.80 1 -5 -1 8 6.00 1.20 1 5 1 -7 6.00 0.70 1 -5 -1 7 1.20 2.30 1 5 1 -6 64.40 2.40 1 -5 -1 6 60.10 1.80 1 5 1 -5 54.80 2.10 1 -5 -1 5 47.20 1.50 1 5 1 -4 213.70 5.10 1 -5 -1 4 203.40 9.10 1 5 1 -3 10.20 0.80 1 -5 -1 3 7.70 1.50 1 5 1 -2 76.60 2.00 1 -5 -1 2 77.70 2.90 1 5 1 -1 188.70 5.80 1 -5 -1 1 171.50 5.40 1 5 1 0 71.10 2.20 1 -5 -1 0 71.50 2.60 1 5 1 1 507.10 9.20 1 -5 -1 -1 503.00 10.40 1 5 1 2 206.80 5.00 1 -5 -1 -2 186.50 5.20 1 5 1 3 155.50 4.00 1 -5 -1 -3 151.10 4.70 1 5 1 4 95.40 2.80 1 -5 -1 -4 92.90 3.30 1 5 1 5 37.80 2.00 1 -5 -1 -5 38.90 1.90 1 5 1 6 85.30 3.40 1 5 1 7 404.30 12.90 1 -5 -1 -7 349.20 14.70 1 5 1 8 121.70 4.30 1 -5 -1 -8 120.50 5.70 1 5 1 9 9.10 1.30 1 -5 -1 -9 10.60 1.50 1 5 1 10 64.60 3.40 1 -5 -1 -10 44.00 3.30 1 5 1 11 0.30 1.20 1 -5 -1 -11 -2.30 1.50 1 5 1 12 21.10 2.80 1 -5 -1 -12 21.50 3.00 1 5 2 -16 3.80 1.80 1 -5 -2 16 -1.70 1.50 1 5 2 -15 3.60 1.80 1 -5 -2 15 3.90 1.20 1 5 2 -14 3.30 1.30 1 -5 -2 14 1.40 1.20 1 -5 -2 13 11.70 1.70 1 5 2 -12 8.90 1.40 1 -5 -2 12 9.80 1.80 1 5 2 -11 13.30 0.90 1 -5 -2 11 14.80 1.70 1 5 2 -10 74.20 2.50 1 -5 -2 10 66.10 3.10 1 5 2 -9 241.50 8.80 1 -5 -2 9 221.70 7.00 1 5 2 -8 155.80 6.50 1 -5 -2 8 130.60 4.30 1 5 2 -7 100.20 4.20 1 -5 -2 7 100.60 3.40 1 5 2 -6 105.00 5.20 1 -5 -2 6 117.10 4.00 1 5 2 -5 43.90 2.50 1 -5 -2 5 39.00 1.90 1 5 2 -4 78.50 3.50 1 -5 -2 4 90.50 3.30 1 5 2 -3 144.60 5.20 1 -5 -2 3 131.50 4.30 1 5 2 -2 450.50 16.30 1 -5 -2 2 420.40 17.50 1 5 2 -1 206.50 9.20 1 -5 -2 1 196.00 10.40 1 5 2 0 112.90 5.60 1 5 2 1 117.60 5.30 1 -5 -2 -1 112.50 5.90 1 5 2 2 90.40 4.50 1 5 2 3 3.20 0.50 1 -5 -2 -3 4.70 0.80 1 5 2 4 128.20 3.40 1 -5 -2 -4 147.90 6.30 1 5 2 5 115.40 5.60 1 -5 -2 -5 105.70 5.30 1 5 2 6 9.80 1.30 1 -5 -2 -6 11.70 1.40 1 5 2 7 49.50 2.50 1 -5 -2 -7 43.60 2.80 1 5 2 8 89.50 3.90 1 5 2 9 26.00 2.00 1 -5 -2 -9 27.70 2.30 1 5 2 10 34.20 2.40 1 -5 -2 -10 21.50 2.40 1 5 2 11 13.80 2.00 1 -5 -2 -11 17.30 2.40 1 5 2 12 39.20 3.80 1 5 3 -16 -3.80 1.50 1 -5 -3 16 0.50 1.30 1 5 3 -15 7.70 1.80 1 -5 -3 15 8.80 1.90 1 5 3 -14 14.30 1.80 1 -5 -3 14 13.00 3.00 1 5 3 -13 2.20 1.40 1 -5 -3 13 5.90 1.60 1 5 3 -12 31.40 2.00 1 -5 -3 12 30.40 3.50 1 5 3 -11 23.40 1.60 1 -5 -3 11 23.30 2.20 1 5 3 -10 22.50 1.90 1 -5 -3 10 29.80 2.00 1 5 3 -9 31.50 2.30 1 -5 -3 9 32.90 2.20 1 5 3 -8 16.30 1.40 1 -5 -3 8 19.40 1.90 1 5 3 -7 13.40 1.30 1 -5 -3 7 15.60 1.60 1 5 3 -6 195.10 7.20 1 -5 -3 6 186.50 11.00 1 5 3 -5 28.20 1.80 1 -5 -3 5 22.50 1.80 1 5 3 -4 9.50 0.90 1 -5 -3 4 17.10 3.30 1 5 3 -3 75.10 2.10 1 -5 -3 3 73.50 5.10 1 5 3 -2 73.30 2.60 1 5 3 -1 3.50 0.50 1 -5 -3 1 1.90 2.30 1 5 3 0 7.40 0.60 1 -5 -3 0 8.80 3.00 1 5 3 1 29.90 1.40 1 -5 -3 -1 35.60 3.30 1 5 3 2 205.00 9.20 1 -5 -3 -2 237.20 12.10 1 5 3 3 110.30 7.10 1 -5 -3 -3 152.70 6.70 1 5 3 4 9.70 1.50 1 -5 -3 -4 6.20 1.30 1 5 3 5 61.50 4.00 1 -5 -3 -5 48.80 2.80 1 5 3 6 23.30 2.30 1 -5 -3 -6 20.40 2.10 1 5 3 7 60.60 4.50 1 -5 -3 -7 52.00 3.40 1 5 3 8 208.40 11.00 1 -5 -3 -8 223.40 9.30 1 5 3 9 46.40 2.70 1 5 3 10 35.70 2.50 1 5 3 11 10.30 2.50 1 5 4 -14 3.10 1.60 1 -5 -4 14 -0.70 1.40 1 5 4 -13 8.40 1.70 1 -5 -4 13 8.50 1.70 1 5 4 -12 20.20 1.90 1 -5 -4 12 12.60 1.90 1 5 4 -11 1.70 1.30 1 -5 -4 11 2.90 1.60 1 5 4 -10 44.80 3.30 1 -5 -4 10 33.90 2.60 1 5 4 -9 7.40 1.20 1 -5 -4 9 7.80 1.60 1 5 4 -8 74.40 3.70 1 -5 -4 8 57.60 3.10 1 5 4 -7 99.80 4.80 1 -5 -4 7 97.90 4.20 1 5 4 -6 27.20 1.70 1 -5 -4 6 25.90 2.20 1 5 4 -5 21.10 1.40 1 -5 -4 5 22.50 3.50 1 5 4 -4 68.50 2.70 1 -5 -4 4 62.80 4.90 1 5 4 -3 30.40 4.10 1 -5 -4 3 39.10 5.30 1 5 4 -2 235.20 8.60 1 -5 -4 2 227.90 11.00 1 5 4 -1 107.70 4.10 1 5 4 0 46.90 2.10 1 5 4 1 57.10 3.50 1 5 4 2 17.90 1.40 1 5 4 3 46.30 4.10 1 -5 -4 -3 51.40 3.10 1 5 4 4 149.20 7.40 1 -5 -4 -4 166.30 7.80 1 5 4 5 8.00 2.10 1 -5 -4 -5 6.90 1.60 1 5 4 7 33.80 3.10 1 5 4 8 34.00 3.10 1 5 4 9 3.10 2.00 1 5 4 10 48.10 4.40 1 5 5 -13 9.10 1.80 1 -5 -5 13 4.20 1.90 1 5 5 -12 8.70 1.60 1 -5 -5 12 3.90 2.10 1 -5 -5 11 17.70 2.10 1 5 5 -10 11.00 1.50 1 -5 -5 10 8.90 3.40 1 5 5 -9 6.00 1.30 1 -5 -5 9 0.70 1.50 1 5 5 -8 23.00 1.80 1 -5 -5 8 24.90 2.30 1 5 5 -7 28.60 2.30 1 -5 -5 7 28.90 2.50 1 -5 -5 6 82.10 3.70 1 5 5 -5 21.70 1.40 1 -5 -5 5 18.60 4.70 1 5 5 -4 55.20 4.60 1 -5 -5 4 67.10 5.60 1 5 5 -3 53.70 4.10 1 -5 -5 3 30.20 4.50 1 5 5 -2 29.00 1.80 1 5 5 -1 12.60 1.20 1 5 5 0 9.00 1.20 1 5 5 2 25.10 3.10 1 5 5 3 76.30 5.70 1 5 5 4 6.40 2.20 1 5 5 5 28.00 3.20 1 5 5 6 1.40 2.20 1 5 5 7 67.00 5.30 1 5 5 8 66.80 5.60 1 -5 -6 10 8.40 2.60 1 -5 -6 9 8.40 2.10 1 -5 -6 8 86.60 4.40 1 -5 -6 7 40.20 2.90 1 5 6 -6 10.80 3.20 1 -5 -6 6 0.70 4.50 1 5 6 -5 14.10 3.10 1 -5 -6 5 8.80 4.20 1 5 6 -4 19.60 3.60 1 5 6 -3 89.80 5.70 1 5 6 -2 58.30 5.10 1 5 6 -1 0.00 2.90 1 5 6 0 21.30 3.60 1 5 6 1 30.30 3.50 1 5 6 2 42.80 4.30 1 5 6 3 64.00 4.90 1 5 6 4 2.40 2.50 1 5 7 -4 30.30 3.80 1 5 7 -3 10.50 3.20 1 5 7 -1 10.50 2.90 1 5 7 0 -3.80 3.00 1 6 0 -17 0.00 1.60 1 6 0 -16 -1.20 1.30 1 6 0 -15 15.50 1.80 1 6 0 -14 4.80 1.50 1 6 0 -13 11.50 1.40 1 6 0 -12 41.40 2.80 1 6 0 -11 7.90 1.40 1 6 0 -10 43.10 3.00 1 6 0 -8 13.10 1.20 1 6 0 -7 2.10 0.80 1 6 0 -6 80.40 2.20 1 6 0 -5 77.80 2.30 1 6 0 -4 4.50 0.70 1 6 0 -3 35.90 1.00 1 6 0 -2 114.50 3.00 1 6 0 -1 1.60 0.50 1 6 0 0 650.10 12.10 1 6 0 1 5.50 0.60 1 6 0 2 14.40 0.70 1 6 0 3 260.80 7.90 1 6 0 4 32.30 1.80 1 6 0 5 13.40 1.30 1 6 0 6 7.90 2.00 1 6 0 7 112.90 4.40 1 6 0 8 4.30 2.30 1 6 0 9 108.70 4.70 1 6 0 10 3.90 2.20 1 6 1 -16 54.50 3.60 1 -6 -1 16 41.40 2.90 1 6 1 -15 20.60 2.40 1 -6 -1 15 28.50 2.10 1 6 1 -14 4.70 1.60 1 -6 -1 14 5.20 1.60 1 6 1 -13 13.30 1.60 1 -6 -1 13 17.10 1.80 1 6 1 -12 12.90 1.70 1 -6 -1 12 12.30 1.60 1 6 1 -11 12.30 1.50 1 -6 -1 11 21.60 2.80 1 6 1 -10 89.90 3.00 1 6 1 -9 49.70 2.00 1 -6 -1 9 62.70 2.80 1 6 1 -8 148.50 4.50 1 -6 -1 8 153.10 5.30 1 6 1 -7 152.10 4.80 1 -6 -1 7 152.10 3.60 1 6 1 -6 65.10 2.30 1 -6 -1 6 48.30 1.70 1 6 1 -5 11.80 0.90 1 -6 -1 5 11.50 0.80 1 6 1 -4 16.20 1.10 1 -6 -1 4 12.00 1.50 1 6 1 -3 28.00 1.20 1 -6 -1 3 25.00 2.10 1 6 1 -2 115.90 3.00 1 -6 -1 2 104.60 3.90 1 6 1 -1 85.40 5.10 1 -6 -1 1 85.30 3.30 1 6 1 0 121.00 3.40 1 -6 -1 0 122.30 4.20 1 6 1 1 428.80 9.60 1 -6 -1 -1 430.50 11.30 1 6 1 2 115.40 3.20 1 -6 -1 -2 91.40 2.70 1 6 1 3 46.40 1.80 1 -6 -1 -3 54.00 2.10 1 6 1 4 169.70 8.80 1 -6 -1 -4 155.00 4.10 1 6 1 5 51.60 2.70 1 -6 -1 -5 46.40 2.30 1 6 1 6 59.80 3.10 1 -6 -1 -6 72.80 3.90 1 6 1 7 137.50 5.40 1 -6 -1 -7 139.10 6.80 1 6 1 8 16.40 1.60 1 6 1 9 39.60 2.40 1 6 1 10 33.70 2.20 1 6 1 11 10.40 1.70 1 6 2 -16 17.10 2.20 1 -6 -2 16 25.30 2.30 1 6 2 -15 20.40 2.40 1 -6 -2 15 21.90 2.10 1 6 2 -14 -1.30 1.40 1 -6 -2 14 -1.90 1.40 1 6 2 -13 6.80 1.40 1 -6 -2 13 6.70 1.50 1 6 2 -12 12.10 1.60 1 -6 -2 12 14.90 1.70 1 6 2 -11 13.80 0.90 1 -6 -2 11 15.60 1.60 1 6 2 -10 33.80 1.80 1 -6 -2 10 33.30 2.20 1 6 2 -9 91.30 3.20 1 -6 -2 9 110.60 4.00 1 6 2 -8 48.70 2.20 1 -6 -2 8 58.70 2.50 1 6 2 -7 30.50 1.90 1 -6 -2 7 31.90 1.90 1 6 2 -6 64.80 3.00 1 -6 -2 6 61.40 2.80 1 6 2 -5 6.40 0.70 1 -6 -2 5 6.60 3.60 1 -6 -2 4 102.80 5.50 1 6 2 -3 52.90 3.20 1 -6 -2 3 52.50 4.00 1 -6 -2 2 47.40 3.80 1 6 2 0 208.20 8.40 1 -6 -2 0 211.90 10.10 1 6 2 1 0.30 1.70 1 -6 -2 -1 2.40 2.60 1 6 2 2 51.20 3.30 1 6 2 3 167.50 4.80 1 -6 -2 -3 173.00 8.00 1 6 2 4 36.10 2.20 1 -6 -2 -4 25.60 1.70 1 6 2 5 68.70 3.10 1 6 2 6 35.90 2.30 1 6 2 7 55.80 2.70 1 6 2 8 12.50 1.50 1 6 2 9 16.10 1.70 1 6 2 10 50.80 3.20 1 6 3 -15 -1.00 1.50 1 -6 -3 15 3.90 1.50 1 6 3 -14 9.40 1.80 1 -6 -3 14 14.60 1.70 1 6 3 -13 8.20 1.50 1 -6 -3 13 4.70 1.60 1 6 3 -12 3.70 1.20 1 -6 -3 12 2.70 1.30 1 6 3 -11 6.20 1.20 1 -6 -3 11 2.10 1.50 1 6 3 -10 10.90 1.30 1 -6 -3 10 11.20 1.70 1 6 3 -9 11.70 1.30 1 -6 -3 9 21.20 2.00 1 6 3 -8 4.10 0.90 1 -6 -3 8 3.30 1.50 1 6 3 -7 11.60 1.00 1 -6 -3 7 9.20 1.90 1 6 3 -6 1.00 0.60 1 -6 -3 6 5.80 1.50 1 6 3 -5 60.30 3.10 1 -6 -3 5 64.40 2.80 1 6 3 -4 42.20 1.80 1 -6 -3 4 40.00 4.30 1 6 3 -3 112.00 6.60 1 6 3 -2 76.30 4.60 1 -6 -3 2 84.30 5.20 1 6 3 -1 4.80 2.40 1 -6 -3 1 6.50 3.30 1 -6 -3 0 502.80 21.40 1 6 3 1 347.40 15.00 1 -6 -3 -1 326.70 13.60 1 6 3 2 7.30 1.80 1 -6 -3 -2 1.20 2.70 1 6 3 3 25.10 2.60 1 6 3 4 6.90 2.00 1 6 3 5 30.90 2.70 1 6 3 6 127.70 7.10 1 6 3 7 30.00 2.10 1 6 3 8 0.40 1.10 1 6 3 9 -0.10 1.80 1 6 3 10 1.00 1.30 1 6 4 -14 4.50 1.30 1 -6 -4 14 1.60 1.50 1 6 4 -13 6.80 1.30 1 -6 -4 13 6.80 1.70 1 6 4 -12 15.90 1.60 1 -6 -4 12 8.40 1.70 1 6 4 -11 3.30 1.00 1 -6 -4 11 6.20 1.50 1 6 4 -10 45.00 2.80 1 -6 -4 10 55.40 3.80 1 6 4 -9 52.40 3.00 1 -6 -4 9 54.70 3.00 1 6 4 -8 4.10 0.80 1 -6 -4 8 4.20 1.50 1 6 4 -7 17.60 1.50 1 -6 -4 7 22.30 2.70 1 -6 -4 6 6.90 1.60 1 6 4 -5 61.90 5.40 1 -6 -4 5 54.60 4.80 1 6 4 -4 90.70 5.40 1 -6 -4 4 92.50 6.90 1 6 4 -3 18.40 3.30 1 -6 -4 3 11.30 3.70 1 6 4 -2 12.40 2.10 1 -6 -4 1 13.20 3.70 1 -6 -4 0 0.10 3.00 1 6 4 1 43.40 3.80 1 -6 -4 -1 18.80 3.60 1 6 4 2 53.10 3.80 1 6 4 3 7.30 1.90 1 6 4 4 33.30 2.80 1 6 4 5 57.30 5.00 1 6 4 6 2.90 2.30 1 6 4 7 3.60 1.80 1 6 4 8 0.30 1.90 1 -6 -5 12 0.60 1.60 1 -6 -5 11 8.10 1.70 1 -6 -5 10 2.10 1.70 1 -6 -5 9 4.70 1.90 1 -6 -5 8 13.30 2.00 1 -6 -5 7 -0.10 1.50 1 6 5 -6 56.30 5.70 1 -6 -5 6 49.90 5.40 1 6 5 -5 53.50 4.60 1 6 5 -4 16.40 3.50 1 6 5 -3 15.00 2.70 1 -6 -5 3 15.60 4.30 1 6 5 -2 0.10 2.10 1 -6 -5 2 5.10 3.80 1 -6 -5 1 84.10 7.30 1 6 5 0 88.00 5.50 1 6 5 1 61.50 5.80 1 6 5 2 55.30 4.00 1 6 5 3 12.80 2.80 1 6 5 4 67.30 5.00 1 6 5 5 47.60 4.20 1 6 5 7 21.90 3.10 1 -6 -6 9 4.30 1.70 1 -6 -6 8 4.80 4.00 1 -6 -6 7 -0.20 3.20 1 6 6 -6 12.10 3.60 1 6 6 -5 35.80 4.40 1 -6 -6 5 20.90 5.30 1 6 6 -4 28.70 3.90 1 -6 -6 4 22.50 4.70 1 6 6 0 14.50 3.30 1 6 6 1 19.90 3.30 1 6 6 2 6.40 2.90 1 6 6 3 2.90 2.60 1 6 6 4 6.70 2.60 1 7 0 -16 53.10 3.20 1 7 0 -15 16.30 1.80 1 7 0 -14 30.70 2.30 1 7 0 -13 4.10 1.10 1 7 0 -12 -2.40 2.00 1 7 0 -11 2.20 1.10 1 7 0 -10 16.90 2.80 1 7 0 -9 46.70 1.80 1 7 0 -8 17.00 1.10 1 7 0 -7 13.90 1.10 1 7 0 -6 101.10 2.70 1 7 0 -5 8.50 0.90 1 7 0 -4 155.80 3.20 1 7 0 -3 8.40 0.50 1 7 0 -2 3.30 0.30 1 7 0 -1 6.30 1.50 1 7 0 0 177.10 4.20 1 7 0 1 36.60 1.40 1 7 0 2 2.00 1.30 1 7 0 3 64.00 4.00 1 7 0 4 67.80 4.90 1 7 0 6 58.60 5.10 1 7 0 7 40.80 3.40 1 7 0 8 20.70 3.40 1 7 0 9 17.00 3.40 1 7 1 -16 8.60 2.00 1 -7 -1 16 12.90 1.80 1 7 1 -15 10.30 1.90 1 -7 -1 15 18.80 1.80 1 -7 -1 14 -1.20 1.20 1 7 1 -13 2.50 1.40 1 -7 -1 13 0.80 1.20 1 7 1 -12 5.20 1.30 1 -7 -1 12 3.10 1.30 1 7 1 -11 4.00 0.90 1 -7 -1 11 4.90 1.30 1 7 1 -10 9.40 1.00 1 -7 -1 10 8.60 1.20 1 7 1 -9 22.90 1.50 1 -7 -1 9 32.60 3.60 1 7 1 -8 28.00 1.40 1 -7 -1 8 30.80 1.90 1 7 1 -7 75.90 2.60 1 -7 -1 7 76.80 3.00 1 7 1 -6 50.30 2.10 1 -7 -1 6 49.30 2.30 1 7 1 -5 34.20 2.80 1 -7 -1 5 26.30 1.70 1 7 1 -4 74.10 3.40 1 -7 -1 4 64.80 3.40 1 7 1 -3 107.60 6.50 1 -7 -1 3 87.20 3.10 1 7 1 -2 17.00 2.00 1 -7 -1 2 18.30 1.90 1 7 1 -1 49.80 2.00 1 -7 -1 1 43.00 4.10 1 7 1 0 432.00 12.00 1 -7 -1 0 355.10 10.40 1 7 1 1 16.10 1.00 1 -7 -1 -1 11.60 1.90 1 7 1 2 291.20 7.80 1 -7 -1 -2 273.70 13.90 1 7 1 3 29.20 1.80 1 -7 -1 -3 20.00 1.70 1 7 1 4 35.20 2.00 1 -7 -1 -4 25.90 2.60 1 7 1 5 62.90 3.10 1 -7 -1 -5 51.80 4.80 1 7 1 6 18.80 1.50 1 7 1 7 43.60 4.00 1 7 1 8 7.90 2.60 1 7 1 9 15.30 2.70 1 7 2 -15 6.00 1.50 1 -7 -2 15 3.70 1.60 1 7 2 -14 6.70 1.60 1 -7 -2 14 8.30 1.50 1 7 2 -13 6.50 1.40 1 -7 -2 13 2.00 1.30 1 7 2 -12 2.80 1.30 1 -7 -2 12 1.30 1.30 1 7 2 -11 1.00 0.80 1 -7 -2 11 -1.30 1.10 1 7 2 -10 6.40 1.00 1 -7 -2 10 4.10 1.30 1 7 2 -9 1.80 0.70 1 -7 -2 9 1.50 1.40 1 7 2 -8 27.30 1.50 1 -7 -2 8 20.50 1.70 1 7 2 -7 104.70 5.50 1 -7 -2 7 84.30 6.80 1 7 2 -6 38.70 2.80 1 -7 -2 6 44.80 2.30 1 7 2 -5 58.30 3.50 1 -7 -2 5 51.00 3.70 1 7 2 -4 3.10 1.50 1 -7 -2 4 1.30 2.30 1 7 2 -3 22.80 1.50 1 -7 -2 3 28.00 3.70 1 7 2 -2 52.50 2.20 1 -7 -2 2 44.20 3.90 1 7 2 -1 36.50 2.00 1 7 2 0 29.80 2.00 1 7 2 1 11.40 1.40 1 7 2 2 41.60 1.80 1 7 2 3 40.30 2.20 1 7 2 4 33.50 2.40 1 7 2 5 2.80 1.10 1 7 2 6 44.40 2.60 1 7 2 7 14.00 1.60 1 7 2 8 43.20 4.30 1 7 2 9 46.20 5.20 1 -7 -3 14 -3.50 2.70 1 -7 -3 13 10.30 1.70 1 -7 -3 12 5.30 1.50 1 -7 -3 11 19.80 2.00 1 7 3 -10 9.10 1.80 1 -7 -3 10 17.80 1.80 1 -7 -3 9 1.10 1.50 1 -7 -3 8 5.30 3.10 1 -7 -3 7 77.20 3.50 1 -7 -3 6 69.20 3.00 1 -7 -3 5 12.40 3.80 1 -7 -3 4 -4.20 3.10 1 7 3 -3 19.80 2.60 1 -7 -3 3 17.80 3.60 1 7 3 -2 151.40 7.00 1 -7 -3 2 136.60 6.60 1 7 3 -1 79.80 5.50 1 -7 -3 1 70.90 6.20 1 7 3 0 39.80 2.90 1 -7 -3 0 24.70 3.60 1 7 3 1 8.00 1.60 1 7 3 2 2.30 1.60 1 -7 -3 -2 1.50 3.70 1 7 3 3 99.40 5.70 1 7 3 4 66.20 3.50 1 7 3 5 1.00 1.80 1 7 3 6 5.50 1.50 1 7 3 7 20.40 2.00 1 7 3 8 3.10 1.40 1 -7 -4 13 3.50 1.70 1 -7 -4 12 2.30 1.60 1 -7 -4 11 12.60 2.00 1 -7 -4 10 2.90 1.70 1 -7 -4 9 0.30 1.50 1 -7 -4 8 13.00 1.60 1 -7 -4 7 98.50 4.40 1 7 4 -6 37.30 3.40 1 -7 -4 6 18.70 3.90 1 7 4 -5 4.70 2.60 1 -7 -4 5 6.80 3.10 1 -7 -4 4 14.40 3.80 1 7 4 -3 34.60 3.00 1 -7 -4 3 18.80 3.60 1 7 4 -2 20.70 2.70 1 -7 -4 2 19.40 4.00 1 -7 -4 1 15.70 3.50 1 7 4 0 7.40 1.90 1 -7 -4 0 22.60 3.30 1 7 4 1 -0.10 1.70 1 7 4 2 11.30 2.00 1 7 4 3 54.70 3.80 1 7 4 4 9.10 1.90 1 7 4 5 3.50 2.00 1 7 4 6 10.70 2.30 1 7 4 7 22.90 2.90 1 -7 -5 11 6.60 1.70 1 -7 -5 10 -1.30 1.60 1 -7 -5 9 2.20 1.60 1 -7 -5 8 23.00 2.30 1 -7 -5 6 3.10 3.70 1 7 5 -5 4.20 2.80 1 -7 -5 5 1.30 3.60 1 7 5 -4 14.30 2.70 1 -7 -5 4 4.20 3.40 1 7 5 -3 43.80 4.10 1 -7 -5 3 35.90 4.00 1 7 5 -2 78.30 5.30 1 7 5 -1 18.50 2.80 1 -7 -5 1 21.70 4.20 1 7 5 1 8.20 2.70 1 7 5 3 50.80 4.20 1 7 5 4 33.30 3.80 1 7 6 -7 18.30 3.00 1 7 6 -5 12.90 3.10 1 -7 -6 5 18.50 4.30 1 7 6 -4 25.30 4.00 1 -7 -6 4 6.10 3.60 1 7 6 -3 1.20 3.20 1 7 6 -2 19.70 3.60 1 7 6 -1 11.50 3.10 1 7 6 0 10.80 3.20 1 7 6 1 13.10 3.30 1 8 0 -15 19.70 4.10 1 8 0 -14 -1.30 1.20 1 8 0 -13 2.10 1.30 1 8 0 -12 24.80 1.80 1 8 0 -11 2.20 1.10 1 8 0 -10 -1.00 0.80 1 8 0 -9 8.70 1.70 1 8 0 -8 1.70 1.50 1 8 0 -7 141.40 5.60 1 8 0 -6 0.80 1.50 1 8 0 -5 38.30 2.10 1 8 0 -4 19.60 2.00 1 8 0 -3 0.50 1.40 1 8 0 -2 35.00 2.20 1 8 0 -1 75.20 3.50 1 8 0 0 4.40 1.50 1 8 0 1 40.80 2.60 1 8 0 2 192.60 9.50 1 8 0 3 20.30 2.70 1 8 0 4 18.30 2.80 1 8 0 5 3.90 2.40 1 8 0 6 13.50 2.90 1 8 0 7 60.30 5.40 1 8 0 8 -3.70 2.40 1 -8 -1 15 -2.00 1.30 1 -8 -1 14 7.60 1.40 1 -8 -1 13 1.20 1.40 1 -8 -1 12 30.10 1.70 1 8 1 -11 5.00 1.50 1 -8 -1 11 4.70 0.90 1 8 1 -10 11.70 1.60 1 -8 -1 10 10.30 1.40 1 8 1 -9 22.10 2.80 1 -8 -1 9 32.90 2.10 1 8 1 -8 2.00 1.80 1 -8 -1 8 0.90 3.00 1 -8 -1 7 4.70 3.20 1 8 1 -6 8.50 2.00 1 -8 -1 6 6.60 2.20 1 8 1 -5 16.50 2.20 1 -8 -1 5 17.80 3.30 1 8 1 -4 19.80 1.20 1 -8 -1 4 21.00 1.90 1 8 1 -3 35.70 2.50 1 -8 -1 3 28.20 2.10 1 8 1 -2 16.10 1.70 1 -8 -1 2 15.50 1.90 1 8 1 -1 10.20 1.40 1 -8 -1 1 11.30 1.60 1 8 1 0 14.60 1.80 1 -8 -1 0 13.80 1.70 1 8 1 1 18.50 1.60 1 -8 -1 -1 17.40 1.90 1 8 1 2 46.00 3.80 1 -8 -1 -2 37.80 2.90 1 8 1 3 79.50 5.40 1 -8 -1 -3 65.00 4.60 1 8 1 4 4.40 2.30 1 8 1 5 30.80 3.60 1 8 1 6 15.30 2.80 1 8 1 7 1.20 2.30 1 -8 -2 14 13.60 1.60 1 -8 -2 13 5.90 1.50 1 -8 -2 12 2.90 1.30 1 -8 -2 11 20.80 2.10 1 8 2 -10 9.20 1.50 1 -8 -2 10 4.80 1.20 1 8 2 -9 26.80 2.80 1 -8 -2 9 24.10 2.00 1 8 2 -8 3.60 2.00 1 -8 -2 8 1.80 3.40 1 8 2 -7 92.70 5.30 1 -8 -2 7 77.30 5.80 1 8 2 -6 2.30 1.40 1 -8 -2 6 -2.20 3.20 1 8 2 -5 64.30 2.90 1 8 2 -4 16.00 2.20 1 -8 -2 4 9.00 2.40 1 8 2 -3 21.80 2.40 1 -8 -2 3 11.40 3.20 1 8 2 -2 31.90 2.80 1 -8 -2 2 28.70 3.20 1 8 2 -1 21.70 1.60 1 -8 -2 1 8.90 3.40 1 8 2 0 63.90 3.30 1 -8 -2 0 58.90 4.10 1 8 2 1 31.50 3.80 1 -8 -2 -1 31.70 3.70 1 8 2 2 9.20 2.40 1 -8 -2 -2 11.00 2.90 1 8 2 3 38.90 4.30 1 8 2 4 6.70 2.30 1 8 2 5 35.50 3.90 1 8 2 6 23.70 3.70 1 8 2 7 60.50 5.30 1 -8 -3 13 0.20 1.40 1 -8 -3 12 12.10 1.70 1 -8 -3 11 2.60 1.30 1 8 3 -10 13.60 1.90 1 -8 -3 10 10.90 1.60 1 8 3 -9 39.80 3.00 1 -8 -3 9 47.50 2.60 1 8 3 -8 8.50 1.70 1 -8 -3 8 8.80 1.50 1 8 3 -7 19.10 2.10 1 -8 -3 7 22.70 2.20 1 8 3 -6 32.90 2.20 1 -8 -3 6 11.30 3.90 1 8 3 -5 22.00 1.80 1 -8 -3 5 20.00 4.20 1 8 3 -4 35.30 3.40 1 -8 -3 4 16.00 3.00 1 8 3 -3 22.70 3.00 1 8 3 -2 11.80 1.20 1 8 3 -1 21.00 1.70 1 -8 -3 1 20.50 3.20 1 8 3 0 2.10 1.90 1 -8 -3 0 -1.60 2.60 1 8 3 1 49.70 2.70 1 -8 -3 -1 39.10 4.20 1 8 3 2 65.60 3.30 1 -8 -3 -2 55.80 5.00 1 8 3 3 23.80 1.90 1 8 3 4 9.10 2.50 1 8 3 5 22.10 3.20 1 8 3 6 2.20 1.90 1 -8 -4 12 2.00 1.70 1 -8 -4 11 8.50 1.90 1 -8 -4 10 7.90 1.50 1 -8 -4 9 5.10 1.70 1 -8 -4 8 12.80 2.10 1 8 4 -7 15.90 3.40 1 8 4 -6 2.80 2.10 1 -8 -4 6 0.90 3.20 1 8 4 -5 51.00 4.60 1 -8 -4 5 32.50 4.30 1 8 4 -3 10.40 2.60 1 -8 -4 3 -0.40 3.00 1 8 4 -1 23.20 2.80 1 8 4 1 9.40 2.40 1 -8 -4 -1 10.70 3.40 1 8 4 2 13.50 2.30 1 8 4 3 18.90 2.40 1 8 4 4 15.00 1.90 1 8 5 -9 27.00 3.90 1 8 5 -8 8.70 3.30 1 -8 -5 8 16.20 3.70 1 8 5 -7 8.70 3.70 1 -8 -5 7 -2.00 3.40 1 8 5 -6 7.20 2.50 1 -8 -5 6 4.40 3.40 1 8 5 -5 20.70 4.00 1 -8 -5 5 19.60 4.80 1 8 5 -4 17.60 2.80 1 -8 -5 4 10.70 3.90 1 -8 -5 3 8.50 3.90 1 8 5 -2 44.20 5.00 1 8 5 -1 10.20 3.40 1 -8 -5 1 -3.40 2.80 1 8 5 0 7.70 2.90 1 8 5 1 13.90 3.60 1 9 0 -13 -1.90 2.80 1 9 0 -12 15.30 3.20 1 9 0 -11 7.20 3.30 1 9 0 -10 38.80 4.80 1 9 0 -9 19.10 2.20 1 9 0 -8 1.10 1.50 1 9 0 -7 7.00 1.70 1 9 0 -6 6.50 1.60 1 9 0 -5 -1.50 1.80 1 9 0 -4 3.40 1.50 1 9 0 -3 60.30 3.40 1 9 0 -2 -1.10 1.20 1 9 0 -1 12.10 1.60 1 9 0 0 56.50 3.10 1 9 0 1 7.90 2.60 1 9 0 2 41.50 4.30 1 9 0 3 9.10 2.70 1 9 0 4 8.40 2.80 1 9 0 5 51.20 4.90 1 9 1 -13 -0.20 2.60 1 -9 -1 13 3.30 2.70 1 -9 -1 12 -1.30 3.00 1 -9 -1 11 8.10 3.00 1 9 1 -10 0.20 1.60 1 -9 -1 10 7.90 3.60 1 9 1 -9 1.60 1.60 1 -9 -1 9 3.60 2.80 1 9 1 -8 3.60 1.40 1 -9 -1 8 3.50 2.60 1 9 1 -7 0.50 1.70 1 -9 -1 7 -1.70 2.90 1 9 1 -6 26.20 2.20 1 -9 -1 6 19.00 2.90 1 9 1 -5 60.80 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34.30 3.50 1 -10 -3 6 18.00 3.80 1 10 3 -5 5.50 2.10 1 -10 -3 5 11.30 3.30 1 10 3 -4 0.20 1.90 1 -10 -3 4 2.30 3.30 1 10 3 -3 5.20 1.90 1 -10 -3 3 0.10 3.20 1 10 3 -2 0.10 2.00 1 -10 -3 2 -0.60 2.80 1 11 0 -7 5.80 2.00 1 11 0 -6 6.00 2.00 1 11 0 -5 2.10 1.70 1 11 0 -4 2.50 1.40 1 11 1 -6 0.50 1.60 1 -11 -1 6 3.10 2.50 1 11 1 -5 4.10 1.60 1 11 1 -4 6.20 1.80 1 -11 -1 4 2.50 2.20 1 0 0 0 ; _shelx_hkl_checksum 40840 #============================================================================= # end of cif data for "glo9508" (compound all-cis-4a) #============================================================================= #============================================================================= # end of cif file #=============================================================================