data_publication_text _publ_contact_author_name 'Jeffrey R. Long' _publ_contact_author_address ;Department of Chemistry University of California, Berkeley USA ; _publ_contact_author_email jrlong@berkeley.edu _publ_contact_author_phone 510-642-0860 loop_ _publ_author_name _publ_author_address 'Siegelman, Rebecca L.' ;Department of Chemistry University of California, Berkeley USA ; 'McDonald, Thomas M.' ;Department of Chemistry University of California, Berkeley USA ; 'Gonzalez, Miguel I.' ;Department of Chemistry University of California, Berkeley USA ; 'Martell, Jeffrey D.' ;Department of Chemistry University of California, Berkeley USA ; 'Milner, Phillip J.' ;Department of Chemistry University of California, Berkeley USA ; 'Berger, Adam H.' ;Department of Chemistry University of California, Berkeley USA ; 'Bhown, Abhoyjit S.' ;Department of Chemistry University of California, Berkeley USA ; 'Long, Jeffrey R.' ;Department of Chemistry University of California, Berkeley USA ; data_gcell107s _audit_creation_date 2016-12-12 _audit_creation_method ; Olex2 1.2 (compiled Nov 22 2016 11:51:51 for OlexSys, GUI svn.r5269) ; _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _publ_section_acknowledgements ; The Advanced Light Source is supported by the Director, Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy under Contract No. DE-AC02-05CH11231. ; _chemical_name_common Zn2(dobpdc)(i-2-CO2)(i-2) _chemical_name_systematic ? _chemical_formula_moiety 'C25 H34 N4 O8 Zn2' _chemical_formula_sum 'C25 H34 N4 O8 Zn2' _chemical_formula_weight 649.33 _chemical_absolute_configuration ? _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0040 0.0020 'ANOMDisVal Program in PLATON Spek, A. L. J. Appl. Crystallogr. 2003, 36, 7-13' 'H' 'H' 0.0000 0.0000 'ANOMDisVal Program in PLATON Spek, A. L. J. Appl. Crystallogr. 2003, 36, 7-13' 'N' 'N' 0.0080 0.0040 'ANOMDisVal Program in PLATON Spek, A. L. J. Appl. Crystallogr. 2003, 36, 7-13' 'O' 'O' 0.0140 0.0070 'ANOMDisVal Program in PLATON Spek, A. L. J. Appl. Crystallogr. 2003, 36, 7-13' 'Zn' 'Zn' 0.2280 1.6720 'ANOMDisVal Program in PLATON Spek, A. L. J. Appl. Crystallogr. 2003, 36, 7-13' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'trigonal' _space_group_IT_number 152 _space_group_name_H-M_alt 'P 31 2 1' _space_group_name_Hall 'P 31 2"' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z+1/3' '-x+y, -x, z+2/3' 'y, x, -z' 'x-y, -y, -z+2/3' '-x, -x+y, -z+1/3' _cell_length_a 21.6521(9) _cell_length_b 21.6521(9) _cell_length_c 6.8387(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 2776.5(3) _cell_formula_units_Z 3 _cell_measurement_reflns_used 9181 _cell_measurement_temperature 195 _cell_measurement_theta_max 26.652 _cell_measurement_theta_min 2.369 _shelx_estimated_absorpt_T_max 0.942 _shelx_estimated_absorpt_T_min 0.796 _exptl_absorpt_coefficient_mu 1.675 _exptl_absorpt_correction_T_max 0.942 _exptl_absorpt_correction_T_min 0.674 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014) was used for absorption correction. wR2(int) was 0.1439 before and 0.0721 after correction. The Ratio of minimum to maximum transmission is 0.715. The \l/2 correction factor is Not present. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'pale yellow' _exptl_crystal_colour_modifier pale _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.007 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 855 _exptl_crystal_size_max 0.143 _exptl_crystal_size_mid 0.036 _exptl_crystal_size_min 0.036 _exptl_special_details ; Data were collected at Beamline 11.3.1 at the Advanced Light Source, Lawrence Berkeley National Laboratory using synchrotron radiation (lamda = 0.7749 angstroms) and a Bruker D8 diffractometer with a PHOTON-100 CMOS detector. The crystal was mounted on a MiTeGen loop using a minimal amount of epoxy to ensure that the crystal pores remained accessible. The sample was then placed in a custom-made gas cell equipped with a borosilicate glass cap, O-ring seal, and gas loading valve. The cell was evacuated under reduced pressure at 323 K for 1 h to remove solvent molecules filling the pores within the crystal. After obtaining the structure of the desolvated crystal to confirm the absence of residual solvent in the pores, the crystal was cooled to 298 K then dosed with 760 torr CO2. The crystal was then cooled to a final temperature of 195 K and the final dataset collected. The crystal was found to be an inversion twin based on the Flack parameter. Refinement of the BASF indicated a twin fraction of 0.41(3). ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0562 _diffrn_reflns_av_unetI/netI 0.0288 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 7 _diffrn_reflns_limit_l_min -7 _diffrn_reflns_number 31599 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 26.781 _diffrn_reflns_theta_max 26.781 _diffrn_reflns_theta_min 2.051 _diffrn_ambient_temperature 195 _diffrn_detector_area_resol_mean 10.42 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 with PHOTON100 CMOS detector' _diffrn_measurement_method '\f and \w shutterless scans' _diffrn_radiation_monochromator 'channel-cut Si(111) crystal' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.7749 _diffrn_source ; Advanced Light Source, station 11.3.1 ; _diffrn_special_details ? _reflns_Friedel_coverage 0.842 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 1.000 _reflns_number_gt 2819 _reflns_number_total 3047 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 0.519 _refine_diff_density_min -0.445 _refine_diff_density_rms 0.096 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.41(3) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.109 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 200 _refine_ls_number_reflns 3047 _refine_ls_number_restraints 102 _refine_ls_R_factor_all 0.0514 _refine_ls_R_factor_gt 0.0457 _refine_ls_restrained_S_all 1.100 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0937P)^2^+1.2629P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1354 _refine_ls_wR_factor_ref 0.1392 _refine_special_details ; Refined as a 2-component inversion twin. Thermal parameters were refined anisotropically for all non-hydrogen atoms. All hydrogen atoms were placed in ideal positions and refined using a riding model. Free refinement of the ammonium carbamate chains indicated an occupancy of 0.62. However, due to overlap of the isopropyl groups of the diamine in the a/b plane, the occupancy of the ammonium carbamate chains was fixed at 0.5 to reflect the hypothesis that a secondary structural transition or secondary conformation (neither of which could be observed in this case) is required to achieve full occupancy at these sites. To account for the remaining unreacted diamine molecules, a nitrogen atom bound to the open Zn coordination sites was refined at 0.5 occupancy. The remaining atoms of the N-isopropylethylenediamine molecule could not be located but were included in the chemical formula and chemical formula weight. The refined Zn-N distance was within error of the Zn-N distance in the structure without CO2. Rigid body and displacement parameter restraints (RIGU and SIMU) were used in the refinement of the ammonium carbamate chains. ; _vrf_CHEMW03_gcell107s ; PROBLEM: ALERT: The ratio of given/expected molecular weight as RESPONSE: The ammonium carbamate chains were modeled at 50% occupancy due to overlap of the atom positions of isopropyl groups in the a/b plane. To account for the remaining unreacted diamine molecules, a nitrogen atom bound to the open Zn coordination sites was refined at 0.5 occupancy. The remaining atoms of the N-isopropylethylenediamine molecule could not be located but were included in the chemical formula and chemical formula weight. ; _vrf_DENSD01_gcell107s ; PROBLEM: The ratio of the submitted crystal density and that RESPONSE: The ammonium carbamate chains were modeled at 50% occupancy due to overlap of the atom positions of isopropyl groups in the a/b plane. To account for the remaining unreacted diamine molecules, a nitrogen atom bound to the open Zn coordination sites was refined at 0.5 occupancy. The remaining atoms of the N-isopropylethylenediamine molecule could not be located but were included in the chemical formula and chemical formula weight. ; _vrf_PLAT043_gcell107s ; PROBLEM: Calculated and Reported Mol. Weight Differ by .. 88.16 Check RESPONSE: The ammonium carbamate chains were modeled at 50% occupancy due to overlap of the atom positions of isopropyl groups in the a/b plane. To account for the remaining unreacted diamine molecules, a nitrogen atom bound to the open Zn coordination sites was refined at 0.5 occupancy. The remaining atoms of the N-isopropylethylenediamine molecule could not be located but were included in the chemical formula and chemical formula weight. ; _vrf_PLAT046_gcell107s ; PROBLEM: Reported Z, MW and D(calc) are Inconsistent .... 1.165 RESPONSE: The ammonium carbamate chains were modeled at 50% occupancy due to overlap of the atom positions of isopropyl groups in the a/b plane. To account for the remaining unreacted diamine molecules, a nitrogen atom bound to the open Zn coordination sites was refined at 0.5 occupancy. The remaining atoms of the N-isopropylethylenediamine molecule could not be located but were included in the chemical formula and chemical formula weight. ; _vrf_PLAT602_gcell107s ; PROBLEM: VERY LARGE Solvent Accessible VOID(S) in Structure ! Info RESPONSE: The structure is a metal-organic framework and retains significant porosity even following insertion of CO2 into the Zn-N bonds to form the observed ammonium carbamate chains. ; _vrf_PLAT220_gcell107s ; PROBLEM: Non-Solvent Resd 1 C Ueq(max)/Ueq(min) Range 10.0 Ratio RESPONSE: Disorder of the isopropyl group within the ammonium carbamate chains results in large displacement parameters. ; _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.59(3) 0.41(3) 2. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H,H,H) groups, All N(H) groups, All N(H,H) groups 3. Uiso/Uaniso restraints and constraints O5 \\sim N2 \\sim N3 \\sim C8 \\sim C9 \\sim C10 \\sim C11 \\sim C12 \\sim C13: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 O4 \\sim N1: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 4. Rigid body (RIGU) restrains O5, N2, N3, C8, C9, C10, C11, C12, C13 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Fixed Sof: O4(0.5) O5(0.5) N2(0.5) H2(0.5) N3(0.5) H3A(0.5) H3B(0.5) C8(0.5) C9(0.5) H9A(0.5) H9B(0.5) C10(0.5) H10A(0.5) H10B(0.5) N1(0.5) C11(0.5) H11(0.5) C12(0.5) H12A(0.25) H12B(0.25) H12C(0.25) H12D(0.25) H12E(0.25) H12F(0.25) C13(0.5) H13A(0.25) H13B(0.25) H13C(0.25) H13D(0.25) H13E(0.25) H13F(0.25) 6.a Ternary CH refined with riding coordinates: C11(H11) 6.b Secondary CH2 refined with riding coordinates: N3(H3A,H3B), C9(H9A,H9B), C10(H10A,H10B) 6.c Aromatic/amide H refined with riding coordinates: C3(H3), C5(H5), C6(H6), N2(H2) 6.d Disordered Me refined with riding coordinates: C12(H12A,H12B,H12C,H12D,H12E,H12F), C13(H13A,H13B,H13C,H13D,H13E,H13F) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary 'intrinsic phasing' _atom_sites_solution_secondary difmap loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.32960(4) 0.72280(4) 0.81472(9) 0.0305(3) Uani 1 1 d . . . . . O1 O 0.4149(3) 0.7610(3) 0.6283(6) 0.0327(12) Uani 1 1 d . . . . . O2 O 0.3542(3) 0.7139(3) 0.2679(6) 0.0281(10) Uani 1 1 d . . . . . O3 O 0.3813(3) 0.7930(2) 0.0339(6) 0.0373(13) Uani 1 1 d . . . . . C1 C 0.4447(4) 0.8242(4) 0.5436(10) 0.0364(18) Uani 1 1 d . . . . . C2 C 0.4361(4) 0.8348(4) 0.3400(9) 0.0370(18) Uani 1 1 d . . . . . C3 C 0.4726(5) 0.9050(4) 0.2660(9) 0.041(2) Uani 1 1 d . . . . . H3 H 0.466704 0.911749 0.131458 0.050 Uiso 1 1 calc R . . . . C4 C 0.5156(5) 0.9636(4) 0.3749(10) 0.050(2) Uani 1 1 d . . . . . C5 C 0.5221(6) 0.9518(4) 0.5731(11) 0.059(3) Uani 1 1 d . . . . . H5 H 0.551162 0.991297 0.654759 0.071 Uiso 1 1 calc R . . . . C6 C 0.4874(5) 0.8844(4) 0.6529(10) 0.048(2) Uani 1 1 d . . . . . H6 H 0.493097 0.879092 0.788487 0.058 Uiso 1 1 calc R . . . . C7 C 0.3881(4) 0.7769(4) 0.2065(9) 0.0251(14) Uani 1 1 d . . . . . O4 O 0.2972(18) 0.788(2) 0.698(5) 0.062(7) Uani 0.5 1 d . U P A 1 O5 O 0.2184(12) 0.8256(12) 0.626(2) 0.103(6) Uani 0.5 1 d . U P A 1 N2 N 0.2562(10) 0.7706(10) 0.421(2) 0.065(4) Uani 0.5 1 d . U P A 1 H2 H 0.287309 0.756183 0.404938 0.079 Uiso 0.5 1 calc R . P A 1 N3 N 0.289(2) 0.8629(17) 0.046(4) 0.139(9) Uani 0.5 1 d . U P A 1 H3A H 0.280657 0.837440 -0.066507 0.167 Uiso 0.5 1 calc R . P A 1 H3B H 0.326611 0.863121 0.107664 0.167 Uiso 0.5 1 calc R . P A 1 C8 C 0.2521(14) 0.7931(13) 0.601(3) 0.065(5) Uani 0.5 1 d . U P A 1 C9 C 0.2174(15) 0.7676(16) 0.262(3) 0.085(6) Uani 0.5 1 d . U P A 1 H9A H 0.166745 0.742721 0.302693 0.102 Uiso 0.5 1 calc R . P A 1 H9B H 0.222576 0.736469 0.165307 0.102 Uiso 0.5 1 calc R . P A 1 C10 C 0.231(2) 0.831(2) 0.162(4) 0.125(9) Uani 0.5 1 d . U P A 1 H10A H 0.188569 0.819084 0.080953 0.150 Uiso 0.5 1 calc R . P A 1 H10B H 0.234802 0.865853 0.261552 0.150 Uiso 0.5 1 calc R . P A 1 N1 N 0.2784(18) 0.782(2) 0.743(5) 0.046(6) Uani 0.5 1 d . U P A 2 C11 C 0.310(4) 0.940(2) -0.005(6) 0.188(16) Uani 0.5 1 d . U P A -1 H11 H 0.271490 0.944731 -0.074653 0.226 Uiso 0.5 1 calc R . P A -1 C12 C 0.348(5) 0.996(3) 0.143(8) 0.30(4) Uani 0.5 1 d . U P A -1 H12A H 0.315189 0.991530 0.247175 0.364 Uiso 0.25 1 calc R . P A -1 H12B H 0.386628 0.989758 0.199191 0.364 Uiso 0.25 1 calc R . P A -1 H12C H 0.368693 1.042927 0.082400 0.364 Uiso 0.25 1 calc R . P A -1 H12D H 0.398484 1.024614 0.105335 0.364 Uiso 0.25 1 calc R . P A -1 H12E H 0.327045 1.026385 0.153319 0.364 Uiso 0.25 1 calc R . P A -1 H12F H 0.344980 0.973217 0.270111 0.364 Uiso 0.25 1 calc R . P A -1 C13 C 0.379(2) 0.9680(18) -0.121(7) 0.161(13) Uani 0.5 1 d . U P A -1 H13A H 0.369584 0.939203 -0.239749 0.193 Uiso 0.25 1 calc R . P A -1 H13B H 0.396563 1.017859 -0.157785 0.193 Uiso 0.25 1 calc R . P A -1 H13C H 0.414498 0.964691 -0.040994 0.193 Uiso 0.25 1 calc R . P A -1 H13D H 0.417512 1.008633 -0.052603 0.193 Uiso 0.25 1 calc R . P A -1 H13E H 0.390534 0.929976 -0.134566 0.193 Uiso 0.25 1 calc R . P A -1 H13F H 0.372599 0.983144 -0.251358 0.193 Uiso 0.25 1 calc R . P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0372(5) 0.0347(5) 0.0143(4) -0.0024(3) -0.0018(3) 0.0139(4) O1 0.043(3) 0.029(3) 0.015(2) 0.0058(19) 0.0009(18) 0.010(2) O2 0.036(3) 0.027(3) 0.0145(18) -0.0030(19) -0.0067(19) 0.010(2) O3 0.057(4) 0.031(2) 0.011(2) 0.0018(18) -0.005(2) 0.012(2) C1 0.047(4) 0.032(4) 0.019(4) 0.004(3) 0.001(3) 0.011(4) C2 0.053(5) 0.038(4) 0.009(3) -0.002(3) -0.001(3) 0.015(4) C3 0.067(6) 0.033(4) 0.008(3) 0.001(3) 0.000(3) 0.013(4) C4 0.087(7) 0.024(4) 0.018(4) -0.002(3) 0.001(4) 0.013(4) C5 0.100(8) 0.031(4) 0.017(4) -0.005(3) -0.011(4) 0.011(5) C6 0.073(6) 0.037(4) 0.010(3) 0.000(3) -0.005(3) 0.009(4) C7 0.034(4) 0.026(4) 0.013(3) -0.001(3) 0.000(3) 0.013(3) O4 0.068(17) 0.089(13) 0.060(16) 0.036(11) 0.035(9) 0.063(14) O5 0.160(16) 0.174(17) 0.061(8) -0.007(11) -0.007(11) 0.148(15) N2 0.091(11) 0.089(11) 0.049(7) -0.009(7) -0.001(7) 0.069(10) N3 0.22(3) 0.140(17) 0.109(18) 0.013(13) 0.009(15) 0.131(19) C8 0.107(15) 0.086(13) 0.040(8) 0.001(9) -0.002(10) 0.077(12) C9 0.103(15) 0.138(17) 0.033(8) -0.029(9) -0.013(9) 0.076(14) C10 0.18(2) 0.16(2) 0.059(14) -0.020(12) -0.033(13) 0.104(18) N1 0.053(18) 0.069(14) 0.036(13) 0.008(11) 0.015(11) 0.044(14) C11 0.31(4) 0.13(2) 0.18(3) -0.005(18) 0.03(3) 0.14(2) C12 0.40(7) 0.18(3) 0.33(5) -0.11(4) 0.03(5) 0.14(4) C13 0.21(4) 0.09(2) 0.19(3) 0.00(2) -0.04(3) 0.08(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 Zn1 3.1533(9) 2_665 ? Zn1 Zn1 3.1532(9) 3_564 ? Zn1 O1 2.038(5) 2_665 ? Zn1 O1 2.048(5) . ? Zn1 O2 2.128(4) 2_665 ? Zn1 O2 2.228(5) 3_565 ? Zn1 O3 2.027(4) 1_556 ? Zn1 O4 2.03(4) . ? Zn1 N1 2.14(4) . ? O1 C1 1.320(9) . ? O2 C7 1.254(8) . ? O3 C7 1.260(7) . ? C1 C2 1.439(10) . ? C1 C6 1.380(10) . ? C2 C3 1.410(10) . ? C2 C7 1.477(10) . ? C3 H3 0.9500 . ? C3 C4 1.361(11) . ? C4 C4 1.480(15) 5_675 ? C4 C5 1.399(11) . ? C5 H5 0.9500 . ? C5 C6 1.376(11) . ? C6 H6 0.9500 . ? O4 C8 1.23(4) . ? O5 C8 1.25(2) . ? N2 H2 0.8800 . ? N2 C8 1.34(2) . ? N2 C9 1.35(2) . ? N3 H3A 0.9100 . ? N3 H3B 0.9100 . ? N3 C10 1.36(4) . ? N3 C11 1.54(5) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.42(4) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 H11 1.0000 . ? C11 C12 1.47(7) . ? C11 C13 1.53(6) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C12 H12D 0.9800 . ? C12 H12E 0.9800 . ? C12 H12F 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C13 H13D 0.9800 . ? C13 H13E 0.9800 . ? C13 H13F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Zn1 Zn1 Zn1 106.50(3) 3_564 2_665 ? O1 Zn1 Zn1 39.61(13) 2_665 2_665 ? O1 Zn1 Zn1 39.39(15) . 3_564 ? O1 Zn1 Zn1 121.78(15) 2_665 3_564 ? O1 Zn1 Zn1 131.63(16) . 2_665 ? O1 Zn1 O1 161.07(18) 2_665 . ? O1 Zn1 O2 82.17(17) 2_665 2_665 ? O1 Zn1 O2 80.98(17) . 2_665 ? O1 Zn1 O2 78.81(18) 2_665 3_565 ? O1 Zn1 O2 89.35(19) . 3_565 ? O1 Zn1 N1 87.4(9) 2_665 . ? O1 Zn1 N1 104.4(8) . . ? O2 Zn1 Zn1 69.69(11) 3_565 3_564 ? O2 Zn1 Zn1 44.88(13) 2_665 3_564 ? O2 Zn1 Zn1 89.71(12) 2_665 2_665 ? O2 Zn1 Zn1 42.39(11) 3_565 2_665 ? O2 Zn1 O2 78.25(5) 2_665 3_565 ? O2 Zn1 N1 101.7(11) 2_665 . ? O3 Zn1 Zn1 84.63(12) 1_556 2_665 ? O3 Zn1 Zn1 128.88(17) 1_556 3_564 ? O3 Zn1 O1 96.3(2) 1_556 . ? O3 Zn1 O1 98.8(2) 1_556 2_665 ? O3 Zn1 O2 91.73(18) 1_556 3_565 ? O3 Zn1 O2 169.6(2) 1_556 2_665 ? O3 Zn1 O4 91.2(12) 1_556 . ? O3 Zn1 N1 88.7(10) 1_556 . ? O4 Zn1 Zn1 109.4(7) . 3_564 ? O4 Zn1 Zn1 136.7(6) . 2_665 ? O4 Zn1 O1 99.4(7) . 2_665 ? O4 Zn1 O1 91.7(6) . . ? O4 Zn1 O2 98.8(11) . 2_665 ? O4 Zn1 O2 176.7(12) . 3_565 ? N1 Zn1 Zn1 124.0(7) . 2_665 ? Zn1 O1 Zn1 101.0(2) 3_564 . ? C1 O1 Zn1 124.5(5) . . ? C1 O1 Zn1 122.7(4) . 3_564 ? Zn1 O2 Zn1 92.73(18) 3_564 2_664 ? C7 O2 Zn1 137.3(4) . 2_664 ? C7 O2 Zn1 124.4(4) . 3_564 ? C7 O3 Zn1 125.6(4) . 1_554 ? O1 C1 C2 123.7(6) . . ? O1 C1 C6 119.4(6) . . ? C6 C1 C2 116.9(7) . . ? C1 C2 C7 123.7(6) . . ? C3 C2 C1 118.1(6) . . ? C3 C2 C7 118.1(6) . . ? C2 C3 H3 117.9 . . ? C4 C3 C2 124.2(6) . . ? C4 C3 H3 117.9 . . ? C3 C4 C4 122.4(8) . 5_675 ? C3 C4 C5 116.4(7) . . ? C5 C4 C4 121.2(8) . 5_675 ? C4 C5 H5 119.1 . . ? C6 C5 C4 121.8(7) . . ? C6 C5 H5 119.1 . . ? C1 C6 H6 118.7 . . ? C5 C6 C1 122.6(6) . . ? C5 C6 H6 118.7 . . ? O2 C7 O3 121.9(6) . . ? O2 C7 C2 119.8(6) . . ? O3 C7 C2 118.3(6) . . ? C8 O4 Zn1 147(3) . . ? C8 N2 H2 116.5 . . ? C8 N2 C9 127.0(17) . . ? C9 N2 H2 116.5 . . ? H3A N3 H3B 107.9 . . ? C10 N3 H3A 109.2 . . ? C10 N3 H3B 109.2 . . ? C10 N3 C11 112(3) . . ? C11 N3 H3A 109.2 . . ? C11 N3 H3B 109.2 . . ? O4 C8 O5 133(2) . . ? O4 C8 N2 105.2(19) . . ? O5 C8 N2 119.4(17) . . ? N2 C9 H9A 107.1 . . ? N2 C9 H9B 107.1 . . ? N2 C9 C10 121(3) . . ? H9A C9 H9B 106.8 . . ? C10 C9 H9A 107.1 . . ? C10 C9 H9B 107.1 . . ? N3 C10 C9 118(3) . . ? N3 C10 H10A 107.9 . . ? N3 C10 H10B 107.9 . . ? C9 C10 H10A 107.9 . . ? C9 C10 H10B 107.9 . . ? H10A C10 H10B 107.2 . . ? N3 C11 H11 114.2 . . ? C12 C11 N3 118(5) . . ? C12 C11 H11 114.2 . . ? C12 C11 C13 90(5) . . ? C13 C11 N3 104(3) . . ? C13 C11 H11 114.2 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? C11 C12 H12D 109.5 . . ? C11 C12 H12E 109.5 . . ? C11 C12 H12F 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12A C12 H12D 141.1 . . ? H12A C12 H12E 56.3 . . ? H12A C12 H12F 56.3 . . ? H12B C12 H12C 109.5 . . ? H12B C12 H12D 56.3 . . ? H12B C12 H12E 141.1 . . ? H12B C12 H12F 56.3 . . ? H12C C12 H12D 56.3 . . ? H12C C12 H12E 56.3 . . ? H12C C12 H12F 141.1 . . ? H12D C12 H12E 109.5 . . ? H12D C12 H12F 109.5 . . ? H12E C12 H12F 109.5 . . ? C11 C13 H13A 109.5 . . ? C11 C13 H13B 109.5 . . ? C11 C13 H13C 109.5 . . ? C11 C13 H13D 109.5 . . ? C11 C13 H13E 109.5 . . ? C11 C13 H13F 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13A C13 H13D 141.1 . . ? H13A C13 H13E 56.3 . . ? H13A C13 H13F 56.3 . . ? H13B C13 H13C 109.5 . . ? H13B C13 H13D 56.3 . . ? H13B C13 H13E 141.1 . . ? H13B C13 H13F 56.3 . . ? H13C C13 H13D 56.3 . . ? H13C C13 H13E 56.3 . . ? H13C C13 H13F 141.1 . . ? H13D C13 H13E 109.5 . . ? H13D C13 H13F 109.5 . . ? H13E C13 H13F 109.5 . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N2 H2 O2 0.88 2.27 3.116(15) 162.3 . N3 H3A O4 0.91 2.06 2.93(4) 159.9 1_554 N3 H3B O3 0.91 2.40 3.05(3) 128.2 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Zn1 O1 C1 C2 -106.1(7) . . . . ? Zn1 O1 C1 C2 29.6(10) 3_564 . . . ? Zn1 O1 C1 C6 -149.7(7) 3_564 . . . ? Zn1 O1 C1 C6 74.6(9) . . . . ? Zn1 O2 C7 O3 2.2(11) 2_664 . . . ? Zn1 O2 C7 O3 148.0(6) 3_564 . . . ? Zn1 O2 C7 C2 -33.9(9) 3_564 . . . ? Zn1 O2 C7 C2 -179.6(5) 2_664 . . . ? Zn1 O3 C7 O2 -10.4(10) 1_554 . . . ? Zn1 O3 C7 C2 171.4(5) 1_554 . . . ? Zn1 O4 C8 O5 131(3) . . . . ? Zn1 O4 C8 N2 -65(4) . . . . ? O1 C1 C2 C3 -178.0(8) . . . . ? O1 C1 C2 C7 5.4(13) . . . . ? O1 C1 C6 C5 177.8(9) . . . . ? C1 C2 C3 C4 0.0(14) . . . . ? C1 C2 C7 O2 -2.7(12) . . . . ? C1 C2 C7 O3 175.6(7) . . . . ? C2 C1 C6 C5 -1.6(14) . . . . ? C2 C3 C4 C4 -179.0(6) . . . 5_675 ? C2 C3 C4 C5 -1.1(15) . . . . ? C3 C2 C7 O2 -179.2(7) . . . . ? C3 C2 C7 O3 -1.0(11) . . . . ? C3 C4 C5 C6 0.8(16) . . . . ? C4 C4 C5 C6 178.8(8) 5_675 . . . ? C4 C5 C6 C1 0.5(18) . . . . ? C6 C1 C2 C3 1.3(12) . . . . ? C6 C1 C2 C7 -175.3(8) . . . . ? C7 C2 C3 C4 176.8(8) . . . . ? N2 C9 C10 N3 76(4) . . . . ? C8 N2 C9 C10 73(4) . . . . ? C9 N2 C8 O4 -179(3) . . . . ? C9 N2 C8 O5 -12(4) . . . . ? C10 N3 C11 C12 79(6) . . . . ? C10 N3 C11 C13 176(4) . . . . ? C11 N3 C10 C9 -164(3) . . . . ? _shelx_res_file ; TITL gcell107s_a.res in P3(1)21 gcell107s.res created by SHELXL-2016/6 at 16:42:34 on 12-Dec-2016 REM Old TITL GCELL107S in P3(2)21 REM SHELXT solution in P3(1)21 REM R1 0.151, Rweak 0.026, Alpha 0.015, Orientation as input REM Flack x = 0.402 ( 0.007 ) from Parsons' quotients REM Formula found by SHELXT: H13d N O3 Zn CELL 0.7749 21.6521 21.6521 6.8387 90 90 120 ZERR 3 0.0009 0.0009 0.0003 0 0 0 LATT -1 SYMM -Y,+X-Y,0.333+Z SYMM +Y-X,-X,0.667+Z SYMM +Y,+X,-Z SYMM -Y+X,-Y,0.667-Z SYMM -X,-X+Y,0.333-Z SFAC C H N O Zn DISP C 0.004 0.002 13.6 DISP H 0 0 0.7 DISP N 0.008 0.004 23.9 DISP O 0.014 0.007 40.889 DISP Zn 0.228 1.672 7409.4 UNIT 60 60 9 24 6 EQIV $1 +X,+Y,-1+Z SIMU O5 > C10 C11 > C13 SIMU O4 N1 RIGU O5 N2 N3 C8 C9 C10 C11 C12 C13 L.S. 100 PLAN 20 SIZE 0.036 0.036 0.143 TEMP -78.15 HTAB N3 O4_$1 HTAB N3 O3 HTAB N2 O2 BIND -1 1 HTAB HTAB BOND $H list 4 MORE -1 CONF fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 REM REM REM WGHT 0.093700 1.262900 BASF 0.41034 FVAR 0.43739 ZN1 5 0.329597 0.722800 0.814719 11.00000 0.03720 0.03468 = 0.01433 -0.00243 -0.00178 0.01391 O1 4 0.414919 0.760991 0.628293 11.00000 0.04291 0.02942 = 0.01514 0.00576 0.00088 0.01008 O2 4 0.354161 0.713901 0.267936 11.00000 0.03564 0.02701 = 0.01449 -0.00302 -0.00667 0.01019 O3 4 0.381288 0.792986 0.033937 11.00000 0.05671 0.03089 = 0.01078 0.00180 -0.00496 0.01165 C1 1 0.444722 0.824248 0.543648 11.00000 0.04697 0.03195 = 0.01892 0.00359 0.00077 0.01110 C2 1 0.436063 0.834809 0.340002 11.00000 0.05284 0.03828 = 0.00923 -0.00225 -0.00113 0.01484 C3 1 0.472566 0.904963 0.265967 11.00000 0.06673 0.03347 = 0.00838 0.00079 0.00001 0.01339 AFIX 43 H3 2 0.466704 0.911749 0.131458 11.00000 -1.20000 AFIX 0 C4 1 0.515648 0.963562 0.374858 11.00000 0.08742 0.02444 = 0.01827 -0.00228 0.00118 0.01273 C5 1 0.522081 0.951751 0.573081 11.00000 0.09979 0.03088 = 0.01736 -0.00465 -0.01120 0.01150 AFIX 43 H5 2 0.551162 0.991297 0.654759 11.00000 -1.20000 AFIX 0 C6 1 0.487418 0.884399 0.652878 11.00000 0.07261 0.03725 = 0.00998 -0.00007 -0.00509 0.00895 AFIX 43 H6 2 0.493097 0.879092 0.788487 11.00000 -1.20000 AFIX 0 C7 1 0.388090 0.776868 0.206534 11.00000 0.03412 0.02575 = 0.01323 -0.00139 -0.00049 0.01325 PART 1 O4 4 0.297231 0.788245 0.697845 10.50000 0.06837 0.08925 = 0.06031 0.03587 0.03475 0.06252 O5 4 0.218373 0.825608 0.626376 10.50000 0.15991 0.17431 = 0.06063 -0.00672 -0.00748 0.14801 N2 3 0.256156 0.770559 0.421345 10.50000 0.09097 0.08907 = 0.04864 -0.00859 -0.00117 0.06920 AFIX 43 H2 2 0.287309 0.756183 0.404938 10.50000 -1.20000 AFIX 0 N3 3 0.289291 0.862948 0.045942 10.50000 0.22217 0.14008 = 0.10944 0.01271 0.00896 0.13068 AFIX 23 H3A 2 0.280657 0.837440 -0.066507 10.50000 -1.20000 H3B 2 0.326611 0.863121 0.107664 10.50000 -1.20000 AFIX 0 C8 1 0.252134 0.793122 0.601459 10.50000 0.10749 0.08576 = 0.04014 0.00073 -0.00191 0.07696 C9 1 0.217442 0.767550 0.262305 10.50000 0.10318 0.13825 = 0.03307 -0.02911 -0.01275 0.07576 AFIX 23 H9A 2 0.166745 0.742721 0.302693 10.50000 -1.20000 H9B 2 0.222576 0.736469 0.165307 10.50000 -1.20000 AFIX 0 C10 1 0.230830 0.830739 0.162370 10.50000 0.17960 0.16154 = 0.05899 -0.02005 -0.03318 0.10369 AFIX 23 H10A 2 0.188569 0.819084 0.080953 10.50000 -1.20000 H10B 2 0.234802 0.865853 0.261552 10.50000 -1.20000 AFIX 0 PART 0 PART 2 N1 3 0.278361 0.782280 0.742643 10.50000 0.05255 0.06869 = 0.03600 0.00809 0.01451 0.04438 PART 0 PART -1 C11 1 0.309718 0.940321 -0.005028 10.50000 0.30804 0.12606 = 0.17782 -0.00493 0.03295 0.14352 AFIX 13 H11 2 0.271490 0.944731 -0.074653 10.50000 -1.20000 AFIX 0 C12 1 0.348276 0.995763 0.143321 10.50000 0.40047 0.17992 = 0.32531 -0.10891 0.02981 0.14201 AFIX 123 H12A 2 0.315189 0.991530 0.247175 10.25000 -1.20000 H12B 2 0.386628 0.989758 0.199191 10.25000 -1.20000 H12C 2 0.368693 1.042927 0.082400 10.25000 -1.20000 H12D 2 0.398484 1.024614 0.105335 10.25000 -1.20000 H12E 2 0.327045 1.026385 0.153319 10.25000 -1.20000 H12F 2 0.344980 0.973217 0.270111 10.25000 -1.20000 AFIX 0 C13 1 0.378773 0.967996 -0.121298 10.50000 0.21320 0.08615 = 0.19441 0.00442 -0.03593 0.08296 AFIX 123 H13A 2 0.369584 0.939203 -0.239749 10.25000 -1.20000 H13B 2 0.396563 1.017859 -0.157785 10.25000 -1.20000 H13C 2 0.414498 0.964691 -0.040994 10.25000 -1.20000 H13D 2 0.417512 1.008633 -0.052603 10.25000 -1.20000 H13E 2 0.390534 0.929976 -0.134566 10.25000 -1.20000 H13F 2 0.372599 0.983144 -0.251358 10.25000 -1.20000 AFIX 0 HKLF 4 REM gcell107s_a.res in P3(1)21 REM R1 = 0.0457 for 2819 Fo > 4sig(Fo) and 0.0514 for all 3047 data REM 200 parameters refined using 102 restraints END WGHT 0.0937 1.2629 REM Instructions for potential hydrogen bonds HTAB N2 O2 HTAB N3 O4_$1 HTAB N3 O5_$1 HTAB N3 O3 EQIV $2 -y+1, x-y+1, z-2/3 HTAB C9 O1_$2 HTAB C10 O5 EQIV $7 x-y+1, -y+2, -z+2/3 HTAB C12 O5_$7 REM Highest difference peak 0.519, deepest hole -0.445, 1-sigma level 0.096 Q1 1 0.2491 0.8090 0.7877 11.00000 0.05 0.52 Q2 1 0.2096 0.8516 -0.1384 11.00000 0.05 0.48 Q3 1 0.0546 0.7412 0.7064 11.00000 0.05 0.34 Q4 1 0.3534 0.6899 0.8187 11.00000 0.05 0.32 Q5 1 0.0632 0.7511 -0.1409 11.00000 0.05 0.31 Q6 1 0.3067 0.7504 0.8196 11.00000 0.05 0.31 Q7 1 0.2182 0.8513 0.0306 11.00000 0.05 0.30 Q8 1 0.0776 0.7756 0.4992 11.00000 0.05 0.30 Q9 1 0.2899 0.6767 0.8502 11.00000 0.05 0.30 Q10 1 0.0408 0.7394 0.5504 11.00000 0.05 0.30 Q11 1 0.0560 0.7140 0.4739 11.00000 0.05 0.29 Q12 1 0.0000 0.7511 0.6667 10.50000 0.05 0.29 Q13 1 0.2095 0.8301 0.7275 11.00000 0.05 0.29 Q14 1 0.1684 0.7697 0.6430 11.00000 0.05 0.29 Q15 1 0.2579 0.8614 0.7356 11.00000 0.05 0.28 Q16 1 0.3605 0.7798 0.7893 11.00000 0.05 0.28 Q17 1 0.2706 0.8461 0.2107 11.00000 0.05 0.27 Q18 1 0.1308 0.7393 0.4015 11.00000 0.05 0.27 Q19 1 0.1732 0.7727 0.4806 11.00000 0.05 0.26 Q20 1 0.1728 0.7648 0.1943 11.00000 0.05 0.24 ; _shelx_res_checksum 47636 _shelx_hkl_file ; 1 1 0 9999.00 351.16 0 -2 0 1734.73 63.89 -2 2 0 1812.82 64.19 2 0 0 1737.43 63.69 -2 0 0 1900.21 63.89 -2 2 0 1739.73 64.39 0 2 0 1702.63 63.79 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61.89 6 -14 0 538.75 28.30 6 8 0 555.74 25.40 8 -14 0 513.75 28.00 8 6 0 568.74 31.30 -14 6 0 582.14 32.60 -14 6 0 556.54 28.90 -14 8 0 576.24 33.80 6 8 0 570.64 31.10 8 6 0 585.44 26.30 8 -14 0 544.55 25.90 6 -14 0 519.45 25.90 -14 8 0 593.14 29.60 -6 -8 0 534.55 26.80 14 -6 0 542.25 24.10 14 -8 0 548.85 23.50 -8 -6 0 547.55 27.90 -8 14 0 527.25 26.60 -8 14 0 513.45 21.40 -6 14 0 544.55 22.50 -8 14 0 562.94 30.90 -6 -8 0 513.85 29.10 14 -6 0 586.34 32.00 -8 -6 0 553.24 30.50 14 -6 0 545.75 26.90 14 -8 0 588.34 27.20 -6 14 0 554.74 29.20 5 -14 0 37.90 11.50 9 5 0 25.90 9.50 5 9 0 19.00 11.20 -14 9 0 39.90 15.90 -14 9 0 22.90 12.30 9 -14 0 24.40 10.40 -14 9 0 21.50 8.10 9 -14 0 29.80 10.90 5 -14 0 23.30 11.40 5 9 0 22.20 4.60 -14 5 0 15.50 11.20 -14 5 0 26.80 14.90 9 5 0 14.10 11.50 5 9 0 29.80 9.80 -9 -5 0 8.70 10.40 14 -5 0 29.90 8.20 14 -9 0 20.50 8.80 -5 -9 0 23.30 11.40 -9 -5 0 16.00 11.20 -9 14 0 17.80 4.20 -5 -9 0 13.20 11.40 -5 14 0 20.30 10.80 -9 14 0 18.00 8.40 -5 14 0 30.20 6.40 -5 14 0 20.60 9.60 14 -5 0 4.70 7.90 -9 14 0 38.40 14.40 14 -9 0 29.30 6.60 14 -5 0 8.60 11.70 10 4 0 317.27 19.30 -14 10 0 364.26 26.80 10 -14 0 355.66 20.40 4 10 0 325.27 15.30 -14 4 0 341.37 26.30 4 10 0 343.97 19.40 10 4 0 346.57 26.20 -14 10 0 359.56 20.50 4 -14 0 309.87 20.40 -14 4 0 347.37 22.60 4 -14 0 341.57 25.20 -14 10 0 359.26 22.60 4 10 0 327.37 24.90 10 -14 0 350.86 23.10 -4 14 0 342.27 21.70 -10 14 0 337.27 21.20 -4 14 0 360.56 22.80 14 -4 0 347.87 25.10 14 -10 0 342.07 20.90 -4 -10 0 310.77 20.50 14 -4 0 358.76 21.70 14 -4 0 350.86 19.10 -10 -4 0 322.47 20.70 -10 -4 0 333.17 24.10 14 -10 0 321.77 15.70 -4 -10 0 318.87 25.10 -10 14 0 337.27 25.00 3 -14 0 89.19 18.50 3 11 0 90.29 19.40 11 3 0 116.09 14.90 11 -14 0 103.39 16.90 3 11 0 85.79 9.40 -14 3 0 89.09 16.90 -14 3 0 99.69 16.70 -14 11 0 87.69 13.90 11 3 0 83.19 20.60 3 -14 0 74.69 13.90 11 -14 0 95.49 14.70 3 11 0 103.79 12.50 -14 11 0 113.29 21.90 -3 14 0 70.99 15.20 -11 14 0 88.29 18.70 -3 -11 0 79.39 14.80 14 -11 0 83.29 7.40 -3 14 0 90.19 17.50 14 -3 0 77.89 12.20 -11 -3 0 63.69 9.20 -11 -3 0 75.79 14.20 -11 -3 0 68.99 15.90 14 -3 0 96.79 13.60 -3 14 0 81.99 11.00 14 -11 0 83.49 14.50 14 -3 0 82.69 15.10 -3 -11 0 76.89 15.20 -11 14 0 67.39 14.30 12 -14 0 58.89 14.20 -14 2 0 63.39 15.00 -14 12 0 52.39 17.20 12 2 0 53.79 13.90 12 2 0 71.89 13.50 2 12 0 66.49 12.80 -14 2 0 65.79 14.40 12 -14 0 80.39 12.90 2 12 0 63.89 13.80 2 12 0 58.39 10.80 -14 12 0 50.99 13.50 2 -14 0 74.19 14.50 2 -14 0 56.99 12.90 -2 -12 0 64.29 14.00 -2 -12 0 40.80 12.10 -12 14 0 42.80 16.60 14 -2 0 60.89 11.40 -2 14 0 59.69 11.70 -12 -2 0 75.59 14.50 14 -12 0 60.29 13.40 14 -2 0 61.09 13.80 -12 14 0 62.49 12.90 14 -12 0 62.39 11.90 -2 14 0 58.39 11.20 -2 14 0 74.69 18.00 14 -12 0 63.49 5.70 -12 -2 0 61.19 13.10 14 -2 0 85.79 14.10 -12 -2 0 50.89 11.30 13 -14 0 204.18 18.80 1 13 0 189.58 20.00 1 13 0 212.58 16.10 -14 13 0 192.88 24.80 1 -14 0 163.48 17.90 13 1 0 195.48 16.30 1 13 0 188.98 15.10 13 1 0 205.98 23.90 -14 1 0 156.28 20.20 -14 1 0 191.58 18.30 13 -14 0 194.08 17.20 -14 13 0 191.28 16.10 1 -14 0 171.78 22.50 -1 14 0 198.28 19.70 14 -13 0 181.48 18.10 -1 14 0 183.98 15.30 -1 -13 0 162.48 22.30 -13 -1 0 160.28 16.40 -13 -1 0 194.98 19.30 -13 14 0 174.48 26.60 -1 14 0 192.38 16.30 -13 -1 0 185.58 21.50 14 -13 0 196.28 16.70 14 -1 0 202.48 17.30 -13 14 0 190.98 17.60 14 -1 0 172.78 22.30 -1 -13 0 199.78 20.00 -14 14 0 57.19 19.40 -14 0 0 54.49 14.50 -14 0 0 63.59 12.90 14 -14 0 52.79 10.90 0 -14 0 45.70 14.30 -14 14 0 60.59 14.50 14 0 0 74.69 15.40 0 14 0 52.69 10.60 14 -14 0 65.29 12.80 -14 0 0 49.40 13.30 0 -14 0 50.89 14.60 0 14 0 71.89 13.10 14 0 0 48.30 14.50 0 14 0 74.29 17.70 -15 8 0 166.08 18.30 8 -15 0 176.18 17.30 7 -15 0 170.58 20.40 -15 8 0 167.88 25.50 -15 7 0 150.88 18.90 8 -15 0 172.28 20.00 7 8 0 177.08 20.80 8 7 0 178.98 22.60 7 8 0 167.48 16.50 8 7 0 168.98 16.30 7 -15 0 151.38 17.20 -15 7 0 149.09 23.80 -7 -8 0 139.49 20.70 15 -8 0 142.79 22.20 -8 15 0 167.38 21.70 15 -7 0 134.09 19.40 -8 15 0 161.98 17.70 -7 15 0 140.49 10.70 -8 -7 0 141.19 18.40 -7 15 0 162.28 17.90 15 -7 0 129.09 16.00 -8 -7 0 128.39 16.20 -8 15 0 142.59 10.00 -7 15 0 169.88 20.70 15 -8 0 137.59 16.00 -7 -8 0 155.38 18.20 15 -8 0 179.78 13.30 15 -7 0 184.38 13.90 6 9 0 521.75 30.40 -15 9 0 538.75 29.00 6 -15 0 479.55 27.90 9 -15 0 515.15 25.20 -15 6 0 496.95 33.10 6 9 0 514.85 24.70 9 -15 0 515.75 29.00 9 6 0 541.95 31.70 -15 6 0 494.75 27.60 -15 9 0 554.84 32.30 9 6 0 504.65 25.10 6 -15 0 494.95 25.70 -6 15 0 524.05 27.70 15 -6 0 479.75 25.60 -6 -9 0 494.15 30.60 -6 15 0 495.75 28.10 -9 15 0 505.65 29.70 -9 -6 0 519.95 27.90 -9 -6 0 496.35 30.10 15 -9 0 521.55 26.40 -6 15 0 499.65 22.00 -9 15 0 454.55 20.00 -9 15 0 515.65 26.30 15 -6 0 510.35 31.30 15 -6 0 498.05 23.40 15 -9 0 505.35 22.50 -15 10 0 302.47 22.50 10 5 0 318.17 20.40 -15 5 0 305.07 22.70 5 -15 0 266.57 19.70 5 -15 0 268.67 24.60 10 -15 0 278.57 18.80 10 -15 0 305.97 23.50 5 10 0 288.27 25.10 -15 10 0 295.67 19.40 -15 10 0 317.77 29.10 10 5 0 304.87 25.70 5 10 0 250.57 13.00 -15 5 0 300.27 27.50 5 10 0 299.67 19.30 -10 -5 0 263.37 22.40 -10 15 0 278.77 20.50 15 -10 0 290.77 15.50 15 -5 0 280.47 20.20 -5 -10 0 242.28 19.90 -5 -10 0 255.37 23.70 15 -5 0 282.67 24.50 -5 15 0 261.47 17.00 -10 15 0 318.87 25.00 15 -10 0 288.97 19.90 -10 -5 0 289.47 20.60 -5 15 0 300.87 21.30 15 -5 0 308.37 17.90 -5 15 0 299.07 22.10 -15 4 0 23.40 13.20 11 -15 0 27.20 11.40 4 -15 0 18.00 13.40 -15 4 0 26.60 16.20 11 4 0 6.50 13.40 4 11 0 29.20 12.80 11 -15 0 37.70 12.40 -15 11 0 16.10 8.80 -15 11 0 39.60 18.20 4 -15 0 14.00 12.50 -15 11 0 28.10 12.60 4 11 0 29.70 10.20 4 11 0 27.20 6.10 -4 15 0 16.10 7.70 15 -11 0 26.70 6.00 15 -11 0 19.60 8.70 -4 -11 0 9.30 12.30 -11 -4 0 14.60 12.30 15 -4 0 62.89 13.70 -4 -11 0 15.90 12.80 -4 15 0 19.60 11.10 15 -4 0 11.20 9.40 -11 15 0 42.10 16.10 15 -4 0 11.50 11.50 -4 15 0 40.40 12.00 -11 -4 0 18.10 12.10 -11 15 0 29.30 9.10 -15 12 0 157.18 26.70 12 -15 0 163.58 17.60 3 -15 0 134.09 18.30 -15 3 0 140.09 22.50 3 12 0 176.58 16.20 12 3 0 159.88 20.80 -15 12 0 141.79 16.20 12 -15 0 170.38 15.70 3 12 0 151.08 11.90 3 12 0 189.08 22.20 12 3 0 155.28 15.90 3 -15 0 143.49 20.40 -15 3 0 149.69 19.30 15 -3 0 135.79 22.00 -3 15 0 165.18 16.80 -3 -12 0 146.59 19.70 -12 15 0 154.78 17.10 15 -3 0 136.89 16.80 -3 15 0 142.99 13.60 -12 -3 0 123.99 10.50 -3 -12 0 106.09 21.00 15 -12 0 152.28 17.00 -12 -3 0 151.18 21.30 15 -12 0 140.49 8.80 -3 15 0 144.59 18.00 -12 15 0 171.18 25.80 15 -3 0 150.18 16.30 -12 -3 0 139.19 17.10 -15 13 0 108.69 13.80 2 13 0 128.59 21.40 2 -15 0 92.99 15.80 13 2 0 105.69 22.40 2 13 0 104.19 13.00 2 -15 0 87.59 18.50 13 2 0 115.79 17.10 13 -15 0 109.79 18.10 13 -15 0 119.99 16.40 2 13 0 124.69 15.40 -15 2 0 104.89 17.00 -15 2 0 105.89 25.40 -15 13 0 125.29 26.90 -13 -2 0 100.19 12.40 -2 15 0 109.79 13.80 15 -2 0 93.99 19.20 -2 15 0 118.79 18.10 -2 -13 0 81.69 18.60 -13 15 0 113.19 16.20 15 -13 0 72.29 15.50 15 -13 0 108.19 16.30 15 -2 0 96.29 16.90 -2 -13 0 92.49 20.70 15 -2 0 128.59 15.70 -2 15 0 96.89 15.90 -13 15 0 114.89 23.70 -13 -2 0 97.29 20.70 -13 -2 0 94.29 19.00 1 14 0 117.99 21.20 14 -15 0 97.39 16.30 1 14 0 98.79 14.80 -15 1 0 71.69 16.70 1 -15 0 76.59 16.00 -15 1 0 97.49 19.30 14 1 0 89.79 17.20 1 14 0 79.29 13.90 -15 14 0 85.69 14.10 -15 14 0 96.99 21.80 14 1 0 113.89 17.30 14 -15 0 87.59 17.90 15 -1 0 91.39 22.80 -1 -14 0 89.89 16.20 15 -1 0 105.19 16.20 -14 -1 0 92.39 17.80 -14 -1 0 73.09 15.00 15 -14 0 93.89 14.10 -1 15 0 103.59 18.20 -14 -1 0 90.89 16.70 -1 -14 0 101.49 19.00 -14 15 0 108.29 23.70 15 -14 0 80.19 15.50 -1 15 0 84.79 14.00 -1 15 0 102.29 15.70 -14 15 0 77.89 14.40 0 15 0 220.48 23.60 -15 0 0 194.58 20.20 15 -15 0 194.58 18.40 -15 15 0 193.78 28.60 15 -15 0 200.08 18.70 15 0 0 199.88 25.30 0 -15 0 182.68 21.10 15 0 0 215.18 19.60 0 15 0 208.38 17.80 -15 0 0 196.08 23.90 0 -15 0 176.78 24.30 0 15 0 202.18 17.20 -15 0 0 174.88 19.50 -15 15 0 182.48 17.10 -16 8 0 639.34 36.90 -16 8 0 561.44 30.60 8 8 0 564.04 32.80 8 -16 0 620.74 29.70 8 -16 0 564.14 32.30 8 8 0 565.74 27.70 16 -8 0 568.14 33.70 16 -8 0 549.95 25.80 -8 -8 0 576.44 30.50 -8 16 0 576.84 32.90 -8 16 0 566.24 23.80 -8 -8 0 551.44 32.20 -8 16 0 592.94 30.10 16 -8 0 550.84 28.00 9 -16 0 138.29 20.20 9 -16 0 151.28 18.60 9 7 0 141.19 21.20 9 7 0 130.49 17.20 -16 9 0 167.58 26.10 7 -16 0 146.49 21.00 -16 7 0 165.98 20.30 -16 9 0 129.89 18.30 -16 7 0 168.38 26.20 7 9 0 142.99 17.00 7 9 0 132.99 20.20 7 -16 0 163.28 18.80 16 -9 0 126.19 14.00 -9 16 0 119.39 20.10 16 -7 0 146.59 14.70 -7 16 0 126.19 19.80 -7 -9 0 105.79 19.00 -7 16 0 146.79 18.10 16 -9 0 117.39 23.10 16 -7 0 135.79 16.60 -9 -7 0 117.99 18.20 -7 -9 0 111.09 20.80 16 -7 0 95.79 21.50 -7 16 0 118.99 11.30 -9 -7 0 113.59 16.90 16 -9 0 140.19 16.50 -9 16 0 157.78 17.80 10 -16 0 32.90 11.40 6 10 0 28.30 11.00 6 10 0 41.60 13.60 6 -16 0 34.70 13.40 10 6 0 51.69 12.50 -16 6 0 45.50 18.70 -16 10 0 51.69 15.40 10 6 0 21.10 12.90 -16 6 0 18.40 14.50 -16 10 0 53.39 19.80 6 -16 0 28.50 12.80 10 -16 0 44.00 12.00 16 -6 0 23.60 10.20 -10 -6 0 17.40 12.70 -6 -10 0 37.90 14.00 16 -10 0 51.69 11.10 -6 -10 0 25.30 12.50 16 -6 0 29.60 14.40 -6 16 0 26.90 7.70 -10 16 0 29.80 15.50 -10 -6 0 14.90 12.70 -6 16 0 42.10 13.80 -6 16 0 21.50 10.10 16 -6 0 38.20 9.40 16 -10 0 28.60 9.70 -10 16 0 23.70 9.80 5 -16 0 103.19 21.80 -16 5 0 137.59 20.20 5 11 0 152.38 23.10 5 11 0 114.79 9.40 5 11 0 115.39 16.50 -16 11 0 123.29 15.80 11 5 0 165.68 17.20 -16 11 0 131.59 24.30 -16 5 0 143.89 25.50 -16 11 0 144.99 19.60 11 -16 0 139.99 20.80 11 -16 0 144.89 15.90 11 5 0 137.99 23.50 5 -16 0 146.49 19.30 -11 -5 0 100.09 18.60 16 -11 0 137.79 11.70 -5 16 0 129.29 19.20 -5 -11 0 88.89 16.80 -11 16 0 130.09 15.60 16 -5 0 100.69 19.90 16 -11 0 120.59 15.30 -5 16 0 127.79 18.60 16 -5 0 113.79 16.80 -11 -5 0 118.59 20.60 -5 -11 0 107.99 18.80 -11 16 0 135.99 21.90 -5 16 0 114.29 12.80 16 -5 0 124.09 15.40 4 -16 0 145.59 19.40 4 12 0 174.98 17.60 -16 4 0 181.68 25.40 -16 4 0 185.38 20.60 12 -16 0 193.58 20.80 12 4 0 174.08 17.60 4 -16 0 155.48 21.90 12 -16 0 206.38 18.70 4 12 0 180.38 12.00 -16 12 0 179.48 17.70 4 12 0 176.98 23.50 12 4 0 185.78 24.60 -16 12 0 173.08 25.60 -4 16 0 194.78 20.70 -12 -4 0 157.68 19.70 -4 16 0 165.68 14.70 16 -4 0 160.28 23.90 16 -12 0 168.68 10.90 -4 16 0 171.38 18.70 16 -4 0 195.98 17.70 -12 16 0 174.88 17.80 -4 -12 0 165.58 20.40 16 -4 0 173.48 18.60 -4 -12 0 143.09 23.10 16 -12 0 190.88 18.40 -12 16 0 211.18 24.50 -12 -4 0 172.68 18.40 3 13 0 166.78 17.50 3 13 0 186.38 23.50 3 -16 0 143.59 21.90 13 -16 0 169.98 20.40 3 -16 0 194.48 19.80 13 -16 0 208.58 19.00 13 3 0 155.28 24.90 3 13 0 157.48 13.50 -16 3 0 162.58 20.80 -16 13 0 159.68 15.80 -16 13 0 166.58 28.20 -16 3 0 160.28 24.90 13 3 0 168.78 19.00 -13 -3 0 142.79 18.50 -13 16 0 177.98 18.20 -3 -13 0 138.09 18.90 16 -3 0 186.48 24.50 -3 16 0 170.38 21.30 -3 -13 0 149.69 23.00 -3 16 0 154.28 15.10 16 -13 0 166.58 9.30 16 -13 0 167.28 18.80 -13 16 0 189.08 27.20 16 -3 0 167.88 18.70 -3 16 0 175.88 18.70 16 -13 0 159.38 16.90 -13 -3 0 180.68 22.30 16 -3 0 160.38 17.70 2 14 0 158.98 14.70 2 -16 0 138.49 23.80 14 2 0 156.58 24.70 -16 2 0 149.29 19.20 2 14 0 150.98 16.90 14 2 0 184.08 17.50 -16 14 0 142.99 16.80 -16 2 0 164.48 22.40 2 14 0 160.08 21.00 2 -16 0 133.49 20.40 14 -16 0 171.58 20.50 -16 14 0 154.18 28.40 14 -16 0 162.08 18.40 -2 16 0 163.28 21.60 -2 16 0 171.88 18.00 -2 16 0 154.08 15.20 16 -14 0 162.78 17.30 -14 16 0 192.18 25.60 -14 -2 0 123.59 14.00 16 -2 0 153.48 23.60 -2 -14 0 150.68 23.30 -14 -2 0 150.78 22.90 -2 -14 0 116.49 18.00 16 -2 0 156.88 17.10 16 -14 0 167.78 18.70 -14 16 0 170.98 18.20 -14 -2 0 144.89 20.50 16 -2 0 161.58 18.10 1 -16 0 8.80 13.40 15 1 0 8.30 14.10 -16 1 0 -9.50 12.90 15 -16 0 14.30 10.70 -16 1 0 3.70 13.40 1 15 0 15.10 11.80 1 15 0 10.90 10.70 -16 15 0 -2.60 17.90 1 15 0 13.50 10.00 15 -16 0 20.80 12.10 -16 15 0 12.50 8.80 1 -16 0 10.50 13.10 -1 16 0 10.00 11.20 -1 16 0 18.50 10.10 -1 16 0 16.80 11.20 16 -1 0 16.60 12.40 16 -15 0 15.90 12.10 -15 -1 0 0.90 9.70 -1 -15 0 3.10 12.50 -1 -15 0 5.50 14.00 16 -15 0 8.30 10.30 16 -1 0 3.60 12.90 -15 -1 0 11.40 14.50 -15 16 0 29.30 18.40 -15 16 0 11.80 9.70 -15 -1 0 0.60 12.30 -16 16 0 238.78 27.20 0 16 0 236.78 23.80 16 0 0 237.38 20.40 16 -16 0 244.68 21.40 0 -16 0 191.38 22.80 -16 0 0 283.67 24.10 16 0 0 254.57 27.10 0 16 0 268.77 19.30 0 16 0 235.68 18.90 16 -16 0 244.28 18.40 -16 16 0 249.28 20.20 -16 0 0 247.58 20.60 0 -16 0 245.08 21.00 8 9 0 106.09 20.80 8 -17 0 89.69 18.50 -17 9 0 105.59 24.30 -17 9 0 72.19 16.10 9 -17 0 74.99 18.10 -17 8 0 77.79 18.10 -17 8 0 97.39 21.50 9 8 0 89.79 23.00 8 -17 0 91.99 20.80 8 9 0 97.59 17.30 9 8 0 133.59 18.00 17 -9 0 83.49 21.80 -9 17 0 96.19 17.00 17 -9 0 75.29 15.40 17 -8 0 80.79 14.70 -8 -9 0 71.79 15.30 17 -9 0 112.59 13.60 -8 -9 0 83.09 18.80 -8 17 0 109.89 18.20 -8 17 0 94.79 17.20 -9 17 0 116.59 20.60 -9 -8 0 92.99 18.50 17 -8 0 108.69 14.40 -9 -8 0 76.39 15.90 17 -8 0 66.99 15.90 -8 17 0 80.79 9.70 -17 10 0 248.08 30.50 10 7 0 226.58 26.50 7 10 0 207.78 19.30 -17 10 0 201.38 20.80 -17 7 0 212.78 21.00 -17 7 0 216.78 28.70 7 -17 0 239.58 19.30 10 -17 0 222.78 23.40 7 -17 0 212.38 24.00 7 10 0 242.68 25.10 10 -17 0 216.98 19.00 10 7 0 260.97 18.50 -10 17 0 231.08 26.00 -7 -10 0 197.58 23.70 -7 17 0 182.88 14.60 17 -10 0 210.28 19.30 -10 -7 0 192.18 21.20 -7 17 0 241.98 23.30 17 -7 0 225.88 17.40 17 -10 0 207.98 23.70 17 -10 0 173.08 23.10 -7 -10 0 183.98 19.70 -10 -7 0 213.68 21.80 17 -7 0 199.78 24.90 -10 17 0 215.68 20.00 17 -7 0 204.78 19.00 -7 17 0 213.58 20.10 -17 11 0 150.68 28.10 11 6 0 191.48 17.90 -17 11 0 191.58 19.90 11 -17 0 210.38 19.40 11 -17 0 183.08 21.80 -17 6 0 159.28 21.60 6 11 0 142.69 16.80 6 -17 0 138.19 18.10 11 6 0 151.88 22.20 6 -17 0 159.28 24.00 6 11 0 198.18 24.50 -17 6 0 180.78 28.40 -6 17 0 180.28 21.50 17 -6 0 175.98 24.20 -11 -6 0 136.69 20.00 -6 -11 0 186.38 21.10 17 -11 0 161.48 18.10 -6 17 0 179.18 20.40 17 -11 0 177.28 13.90 -11 17 0 185.78 19.10 -6 -11 0 162.78 23.50 -6 17 0 164.68 14.00 17 -6 0 161.48 18.20 -11 17 0 166.08 26.00 -11 -6 0 154.08 19.00 17 -6 0 172.48 16.30 12 5 0 133.59 24.30 5 12 0 91.29 9.70 5 -17 0 84.99 17.70 -17 5 0 121.39 21.80 12 -17 0 118.99 21.20 -17 12 0 122.59 28.50 12 5 0 114.99 18.20 5 12 0 144.79 24.00 12 -17 0 125.49 16.20 -17 12 0 120.89 16.30 -17 5 0 131.39 21.20 5 12 0 119.49 17.40 -17 12 0 125.49 20.50 5 -17 0 94.89 19.80 -5 -12 0 86.09 17.50 17 -5 0 119.49 17.40 -12 -5 0 117.29 19.40 -12 17 0 126.29 17.40 17 -5 0 118.39 16.30 17 -5 0 114.29 23.00 -12 -5 0 91.89 17.40 17 -12 0 132.19 11.30 -12 17 0 134.49 25.30 -5 17 0 99.89 13.30 -5 17 0 117.59 19.60 -5 -12 0 110.09 21.20 17 -12 0 138.69 17.60 -5 17 0 131.69 19.60 -17 13 0 28.00 19.60 13 4 0 38.90 13.90 -17 4 0 52.09 18.20 4 13 0 43.40 9.90 -17 13 0 23.00 9.50 -17 4 0 26.70 14.10 4 13 0 37.40 12.40 4 -17 0 24.20 12.20 13 -17 0 39.20 12.80 13 -17 0 27.10 11.80 4 13 0 44.40 14.50 4 -17 0 33.10 13.80 13 4 0 23.80 14.10 -13 17 0 25.90 10.50 -13 -4 0 19.20 12.80 17 -13 0 51.49 7.70 -4 17 0 45.30 13.90 -4 17 0 33.80 12.10 -4 17 0 31.60 9.60 -13 -4 0 22.40 13.60 -4 -13 0 31.00 12.80 17 -13 0 32.40 11.00 17 -4 0 44.70 11.70 -13 17 0 31.90 17.50 -4 -13 0 29.80 14.60 17 -4 0 29.20 10.50 17 -4 0 41.10 15.30 -17 3 0 13.00 14.00 3 14 0 33.50 8.50 14 3 0 33.00 14.20 14 3 0 39.40 13.00 -17 3 0 25.80 16.00 3 -17 0 30.10 15.10 3 14 0 45.40 13.50 -17 14 0 38.10 10.00 -17 14 0 36.00 19.40 14 -17 0 39.90 12.20 3 14 0 26.80 11.20 14 -17 0 47.30 13.10 3 -17 0 28.20 13.70 -14 -3 0 22.20 12.10 -3 -14 0 22.20 14.70 17 -3 0 22.60 9.70 -14 17 0 46.90 19.10 -3 -14 0 21.00 12.40 17 -3 0 44.40 12.80 -3 17 0 18.10 12.00 -14 -3 0 16.30 13.90 -3 17 0 37.20 12.30 17 -3 0 25.80 14.40 -14 17 0 19.10 9.20 -3 17 0 28.20 9.70 17 -14 0 25.00 10.50 17 -14 0 38.50 12.10 15 -17 0 272.47 20.60 15 2 0 263.97 27.40 2 15 0 243.28 17.00 2 15 0 261.47 24.60 -17 2 0 234.78 24.60 2 -17 0 232.78 21.00 15 -17 0 260.17 22.50 -17 15 0 238.28 27.50 -17 15 0 253.57 19.80 2 -17 0 237.98 24.30 2 15 0 258.37 19.40 15 2 0 252.37 21.30 -17 2 0 255.27 22.30 -15 -2 0 238.78 23.60 17 -2 0 235.48 26.30 -15 -2 0 230.68 21.10 -2 -15 0 217.38 23.30 -2 17 0 233.38 23.00 -2 17 0 252.07 17.90 17 -2 0 267.07 20.80 -15 17 0 225.18 18.70 17 -2 0 250.67 19.20 17 -15 0 241.28 21.00 -15 17 0 270.17 28.50 -2 17 0 260.17 20.60 17 -15 0 227.48 17.80 -2 -15 0 251.07 21.30 1 -17 0 447.66 27.60 1 16 0 459.75 24.50 -17 1 0 447.66 27.40 16 1 0 449.46 25.70 1 16 0 439.46 23.90 -17 16 0 456.55 32.50 16 1 0 461.95 31.20 16 -17 0 427.26 26.60 1 16 0 434.36 29.00 -17 16 0 394.36 23.80 1 -17 0 420.76 29.70 16 -17 0 472.35 25.20 -16 17 0 467.65 31.80 17 -1 0 488.15 32.00 -16 -1 0 454.85 27.40 17 -1 0 461.35 25.70 -16 17 0 419.86 25.10 -1 -16 0 419.96 28.90 -1 17 0 480.55 25.20 17 -16 0 469.15 24.80 -1 -16 0 442.46 27.50 17 -16 0 397.76 24.70 -1 17 0 381.76 26.40 17 -1 0 449.56 26.50 -1 17 0 442.16 24.30 -16 -1 0 381.96 28.30 17 0 0 108.39 15.60 0 17 0 80.89 15.60 0 -17 0 103.09 20.50 0 -17 0 109.89 17.30 0 17 0 95.79 15.70 -17 17 0 112.49 22.80 17 0 0 98.49 22.30 17 -17 0 106.69 16.50 0 17 0 64.39 14.20 -17 17 0 96.29 15.40 -17 0 0 110.69 19.90 17 -17 0 104.49 17.50 9 -18 0 337.67 23.30 -18 9 0 296.07 32.10 9 -18 0 302.77 25.40 9 9 0 359.46 28.20 -18 9 0 318.97 25.10 9 9 0 309.47 20.80 -9 -9 0 296.97 23.00 18 -9 0 310.37 22.10 -9 -9 0 301.57 24.60 -9 18 0 329.07 23.40 -9 18 0 309.67 24.70 18 -9 0 299.07 27.10 18 -9 0 309.97 19.40 10 -18 0 149.29 21.90 8 10 0 133.49 18.10 8 -18 0 117.59 17.10 -18 10 0 107.79 19.20 10 8 0 144.29 17.90 -18 8 0 121.39 27.80 -18 10 0 146.79 29.20 10 -18 0 133.39 17.00 10 8 0 151.08 24.20 8 -18 0 119.99 21.60 -18 8 0 116.69 21.30 8 10 0 154.98 23.10 18 -8 0 114.09 17.50 -10 18 0 147.59 23.30 -10 -8 0 126.79 20.70 18 -10 0 108.59 15.30 18 -10 0 136.89 14.70 -8 -10 0 102.79 18.10 18 -8 0 102.89 20.90 18 -10 0 99.99 23.60 -10 -8 0 125.09 21.70 18 -8 0 121.09 15.50 -10 18 0 119.09 18.70 -8 18 0 133.29 22.30 -8 18 0 126.79 19.30 -8 -10 0 104.19 22.00 11 7 0 54.39 13.40 7 11 0 37.10 12.20 -18 7 0 45.60 20.30 -18 7 0 53.29 16.50 11 -18 0 39.20 12.40 7 11 0 58.29 15.40 7 -18 0 50.79 14.40 7 -18 0 26.50 13.00 11 7 0 49.60 15.30 11 -18 0 48.50 13.50 -18 11 0 50.99 15.90 -18 11 0 32.40 20.40 18 -11 0 55.69 12.50 -7 -11 0 33.60 12.50 -7 -11 0 27.90 15.20 18 -7 0 43.20 11.10 18 -11 0 49.30 16.10 -7 18 0 53.99 15.60 18 -11 0 34.00 9.80 -11 -7 0 48.60 14.60 18 -7 0 23.40 10.10 -11 18 0 33.20 10.20 -7 18 0 33.30 10.70 18 -7 0 39.40 14.00 -11 18 0 65.09 18.30 -11 -7 0 49.20 16.20 -18 12 0 23.40 19.60 6 12 0 31.80 13.80 6 -18 0 20.10 14.70 -18 6 0 12.30 18.40 6 12 0 15.00 11.30 12 6 0 10.10 13.10 12 -18 0 35.60 13.20 12 -18 0 11.50 11.50 -18 12 0 28.70 16.00 -18 6 0 7.30 14.30 6 -18 0 13.30 13.20 12 6 0 26.90 14.00 18 -6 0 23.70 11.10 -12 18 0 11.80 9.70 -6 -12 0 23.40 15.00 -6 -12 0 22.10 13.60 -12 -6 0 1.80 13.70 18 -6 0 17.00 13.60 -6 18 0 -0.80 12.70 18 -12 0 12.60 9.60 -12 18 0 14.40 16.40 -12 -6 0 20.50 13.10 18 -6 0 9.80 9.10 -6 18 0 16.40 11.10 13 -18 0 44.50 13.40 -18 5 0 52.29 16.10 -18 5 0 54.49 18.90 -18 13 0 29.70 19.00 13 -18 0 65.39 14.60 5 -18 0 34.40 13.10 -18 13 0 43.10 10.60 13 5 0 50.99 13.70 5 13 0 54.99 14.20 5 13 0 35.90 11.80 13 5 0 48.60 15.00 5 -18 0 26.40 13.40 18 -5 0 28.30 10.80 -13 18 0 46.70 11.10 -5 -13 0 35.30 13.40 -5 18 0 49.80 13.90 18 -13 0 39.20 10.90 -13 -5 0 39.30 14.20 18 -5 0 34.50 14.40 -5 18 0 38.10 12.20 -5 -13 0 38.50 14.10 -13 -5 0 46.40 13.50 -5 18 0 35.20 10.30 18 -5 0 24.20 10.10 -13 18 0 45.90 18.20 4 14 0 178.88 16.80 14 -18 0 212.28 19.50 14 -18 0 170.48 21.30 4 -18 0 174.98 22.00 -18 4 0 150.38 25.30 -18 14 0 178.08 17.50 4 14 0 211.28 23.40 14 4 0 173.58 17.90 -18 14 0 194.88 28.80 14 4 0 201.48 25.30 -18 4 0 184.08 22.40 -4 18 0 183.68 19.80 -14 -4 0 184.58 22.50 -14 18 0 171.88 24.00 18 -4 0 172.48 18.80 -4 -14 0 175.68 23.70 -4 18 0 160.48 20.80 -14 18 0 188.08 18.40 18 -4 0 172.78 25.00 18 -14 0 169.28 19.40 -14 -4 0 167.38 19.30 18 -4 0 162.18 17.40 -4 -14 0 183.38 19.30 18 -14 0 200.58 17.70 15 3 0 204.28 25.20 3 -18 0 172.88 23.80 3 15 0 190.98 18.40 -18 3 0 146.79 24.30 -18 15 0 193.68 28.50 15 -18 0 163.08 18.60 3 15 0 211.58 14.40 15 -18 0 236.18 19.80 -18 15 0 173.88 18.20 3 -18 0 174.78 19.10 15 3 0 198.88 19.90 -18 3 0 190.38 22.10 3 15 0 194.88 21.00 -3 -15 0 167.28 22.20 -3 18 0 187.08 18.00 18 -3 0 198.28 18.20 -15 18 0 172.88 16.80 -3 18 0 153.48 16.50 -15 18 0 208.08 26.40 18 -15 0 185.48 16.20 -15 -3 0 175.48 21.50 18 -3 0 160.48 19.40 -3 18 0 153.58 18.60 18 -3 0 200.18 24.50 18 -15 0 177.98 18.80 -15 -3 0 173.98 19.40 -3 -15 0 185.08 21.50 -18 16 0 62.29 14.20 2 -18 0 29.00 12.00 2 16 0 50.79 13.60 2 -18 0 43.50 14.80 -18 16 0 49.00 19.20 -18 2 0 55.19 15.20 16 2 0 35.90 14.10 16 -18 0 46.00 12.20 16 2 0 40.90 12.50 2 16 0 29.50 12.80 16 -18 0 40.50 12.20 -18 2 0 41.40 15.20 2 16 0 42.00 12.10 18 -16 0 76.59 15.20 -16 18 0 46.30 18.10 18 -2 0 38.80 14.50 -16 -2 0 41.70 14.90 18 -2 0 46.70 12.80 -2 18 0 11.90 10.60 -16 -2 0 40.90 12.00 -2 18 0 35.50 12.30 -2 18 0 35.90 12.30 18 -2 0 32.70 9.50 -16 18 0 35.30 10.50 18 -16 0 30.30 9.70 -2 -16 0 36.30 12.10 -2 -16 0 26.40 13.30 17 -18 0 201.08 16.90 1 -18 0 172.78 22.50 -18 17 0 190.28 17.40 -18 17 0 191.68 27.00 17 1 0 219.48 24.00 17 1 0 227.08 20.10 1 17 0 185.38 21.60 17 -18 0 180.38 18.50 1 -18 0 176.78 18.40 -18 1 0 210.98 22.00 1 17 0 165.08 17.60 -17 -1 0 189.48 23.70 -17 -1 0 216.28 22.30 -1 18 0 210.18 18.60 18 -17 0 144.69 19.70 -1 -17 0 152.18 21.70 -1 18 0 154.68 20.40 -1 -17 0 178.28 20.10 18 -1 0 198.78 18.30 -1 18 0 148.49 16.70 -17 18 0 187.98 18.10 -17 18 0 171.58 26.00 18 -1 0 178.68 19.60 18 -17 0 199.88 18.00 18 -1 0 231.58 24.00 18 -18 0 519.25 30.50 -18 0 0 547.85 30.50 18 0 0 581.74 34.30 18 0 0 533.45 29.00 -18 18 0 571.04 36.30 18 -18 0 605.54 28.90 0 18 0 543.15 28.30 0 18 0 480.15 27.30 0 -18 0 575.24 30.50 -18 18 0 508.05 28.40 -19 10 0 67.09 21.90 9 10 0 69.29 15.40 -19 9 0 69.09 21.70 9 -19 0 54.09 13.70 10 9 0 102.59 23.00 -19 9 0 52.19 17.50 -19 10 0 39.80 15.30 9 -19 0 80.89 18.10 10 9 0 80.29 17.20 10 -19 0 53.49 13.60 10 -19 0 60.09 13.90 19 -10 0 37.80 10.60 -9 19 0 47.60 11.60 19 -9 0 46.50 14.40 -10 -9 0 31.20 12.40 -9 -10 0 53.49 15.30 19 -10 0 54.59 16.10 -9 -10 0 97.69 20.10 19 -10 0 86.79 13.90 -10 19 0 49.30 12.70 19 -9 0 77.59 13.90 -10 19 0 83.49 17.50 -9 19 0 52.29 15.30 19 -9 0 51.69 11.90 -10 -9 0 71.49 16.00 11 -19 0 193.88 21.10 -19 8 0 187.78 20.70 8 -19 0 196.58 21.20 8 11 0 247.48 19.90 11 -19 0 246.78 19.40 -19 11 0 230.08 23.60 8 -19 0 214.18 19.40 8 11 0 251.37 25.40 -19 8 0 277.37 29.80 11 8 0 201.98 19.60 -19 11 0 204.38 29.40 -8 19 0 190.88 19.30 -11 -8 0 250.57 24.10 19 -8 0 205.28 25.60 19 -8 0 217.48 17.80 -11 -8 0 223.48 22.20 -8 -11 0 175.18 21.40 -11 19 0 196.58 23.60 19 -11 0 195.98 18.90 19 -8 0 181.38 17.60 19 -11 0 253.47 16.70 -8 19 0 234.28 23.20 -11 19 0 198.18 18.10 -8 -11 0 188.98 19.90 19 -11 0 216.78 25.30 7 12 0 116.59 17.10 7 -19 0 123.99 22.30 -19 12 0 114.09 20.40 -19 7 0 110.99 21.00 7 12 0 142.09 20.20 7 -19 0 133.39 19.50 12 7 0 142.79 21.20 12 -19 0 104.89 18.40 -19 7 0 99.39 21.00 -19 12 0 87.19 21.20 12 7 0 110.59 16.10 12 -19 0 129.89 18.50 -12 19 0 102.19 20.80 19 -12 0 109.19 24.00 19 -7 0 101.59 22.90 19 -12 0 140.19 14.60 -7 -12 0 85.09 19.40 -12 -7 0 136.49 20.30 -7 19 0 84.59 17.90 19 -7 0 81.59 16.40 -12 19 0 114.49 17.50 -7 19 0 96.59 19.40 -12 -7 0 88.39 17.20 19 -7 0 119.49 15.70 19 -12 0 99.99 16.80 -7 19 0 78.39 10.90 -7 -12 0 115.19 20.70 -19 6 0 64.89 19.30 6 13 0 81.19 14.90 13 6 0 77.89 19.50 13 6 0 50.59 13.10 -19 13 0 58.29 20.70 6 -19 0 45.60 13.00 -19 13 0 53.39 15.10 13 -19 0 34.90 11.80 -19 6 0 60.09 16.10 6 -19 0 52.49 15.40 13 -19 0 95.09 16.80 -6 -13 0 69.19 16.20 19 -13 0 40.90 10.50 -6 19 0 62.49 14.70 -13 19 0 76.59 15.00 -6 19 0 31.90 9.60 -13 -6 0 81.99 18.50 19 -6 0 56.99 15.30 -6 -13 0 51.79 13.80 -6 19 0 72.59 17.10 19 -6 0 61.29 15.20 19 -6 0 58.09 12.60 -13 19 0 61.79 17.60 -13 -6 0 50.19 12.80 14 5 0 49.10 13.10 5 -19 0 38.40 12.10 5 14 0 67.19 17.10 -19 5 0 39.40 15.00 14 5 0 44.30 13.20 -19 14 0 31.40 9.70 14 -19 0 29.80 11.40 -19 5 0 25.10 18.20 5 -19 0 39.20 13.10 14 -19 0 46.00 12.80 5 14 0 47.00 12.20 -19 14 0 37.30 19.10 -14 -5 0 54.59 15.20 -5 -14 0 49.00 12.80 -14 -5 0 57.19 14.10 -5 -14 0 41.10 14.60 19 -5 0 28.10 9.40 19 -5 0 44.70 13.00 19 -5 0 35.70 10.80 19 -14 0 36.50 10.00 -14 19 0 25.70 10.70 -14 19 0 41.30 16.90 -5 19 0 16.00 9.80 -5 19 0 43.40 13.00 -5 19 0 37.20 10.60 15 4 0 12.50 12.70 4 -19 0 0.50 13.30 15 4 0 22.10 13.00 15 -19 0 2.20 10.60 4 15 0 18.40 12.00 -19 4 0 -7.00 12.70 -19 4 0 -18.60 15.90 -19 15 0 11.30 17.30 -19 15 0 17.30 7.80 4 -19 0 14.20 11.50 4 15 0 8.30 11.90 15 -19 0 10.50 11.40 -15 19 0 5.60 14.70 19 -4 0 12.10 8.80 -4 -15 0 2.80 11.40 -15 -4 0 -7.40 12.10 -4 -15 0 10.40 12.80 -15 -4 0 7.60 10.50 19 -15 0 4.50 9.30 -4 19 0 4.40 11.40 -15 19 0 4.10 8.10 -4 19 0 -15.40 8.80 19 -4 0 25.90 12.90 -4 19 0 -7.40 9.60 19 -15 0 3.20 10.90 19 -4 0 10.10 11.10 16 -19 0 145.79 17.90 3 -19 0 113.09 17.30 3 16 0 104.19 21.70 16 -19 0 108.59 19.10 3 -19 0 124.09 17.90 16 3 0 161.28 23.00 -19 16 0 137.19 24.10 -19 3 0 121.79 20.10 16 3 0 140.89 18.10 3 16 0 100.99 16.60 -19 3 0 165.98 21.90 -19 16 0 108.39 16.20 -3 -16 0 112.29 17.20 -3 19 0 86.49 19.40 -16 19 0 147.29 21.90 -16 -3 0 141.49 20.30 -16 19 0 119.19 16.60 -16 -3 0 120.19 19.30 19 -16 0 123.09 14.80 -3 19 0 74.69 15.10 19 -3 0 89.29 18.10 19 -3 0 148.49 23.00 19 -3 0 139.39 17.40 -3 19 0 139.29 18.30 19 -16 0 83.19 15.90 -3 -16 0 128.69 20.20 2 -19 0 342.27 23.30 17 -19 0 357.96 22.10 2 17 0 316.77 22.20 -19 2 0 367.46 26.50 -19 17 0 343.67 22.80 17 2 0 353.66 28.80 17 2 0 360.66 24.00 -19 17 0 367.76 31.30 -19 2 0 341.47 26.50 19 -17 0 345.17 24.50 19 -2 0 352.86 23.60 -2 19 0 309.77 21.70 19 -17 0 369.66 22.60 -17 -2 0 336.27 26.90 -2 19 0 375.36 24.00 19 -2 0 351.26 23.10 -17 19 0 323.17 25.00 19 -2 0 387.96 28.60 -2 -17 0 348.87 23.80 -17 19 0 344.27 29.60 -17 -2 0 389.06 26.40 18 -19 0 104.39 15.40 -19 18 0 79.79 27.00 -19 1 0 139.29 21.30 18 1 0 93.99 16.20 -18 -1 0 88.69 18.10 -1 19 0 102.29 17.10 19 -18 0 121.49 17.20 19 -1 0 93.99 18.40 0 -19 0 70.49 15.40 19 0 0 96.09 18.00 -19 0 0 61.59 22.90 -19 19 0 57.69 18.00 0 19 0 58.19 13.10 19 -19 0 87.99 17.70 10 -20 0 447.06 24.80 -20 10 0 436.96 34.10 -20 10 0 447.86 28.90 10 10 0 387.56 24.70 10 -20 0 355.86 25.70 10 10 0 494.05 30.40 -10 20 0 336.47 24.10 -10 -10 0 412.16 25.50 -10 -10 0 403.16 28.40 -10 20 0 385.16 28.50 20 -10 0 431.06 22.80 20 -10 0 476.35 31.00 20 -10 0 415.86 25.20 -20 9 0 180.28 29.20 9 -20 0 187.98 18.10 -20 9 0 161.88 20.50 11 9 0 186.48 24.30 -20 11 0 158.68 27.10 9 11 0 229.78 24.30 -20 11 0 158.88 20.00 9 -20 0 147.99 21.30 11 -20 0 142.39 19.40 9 11 0 155.48 18.10 11 9 0 165.48 17.30 11 -20 0 187.08 19.40 20 -11 0 162.98 22.50 -9 -11 0 158.18 18.40 -9 20 0 173.38 21.60 -11 20 0 138.99 20.30 20 -9 0 191.88 24.40 20 -11 0 207.68 16.30 -9 -11 0 174.28 19.70 -11 -9 0 206.68 22.30 20 -9 0 160.58 17.40 -11 20 0 171.08 18.50 -9 20 0 167.78 18.90 20 -9 0 185.58 16.70 20 -11 0 128.49 16.70 -11 -9 0 184.08 20.80 12 8 0 22.60 12.70 8 -20 0 -7.10 12.90 8 12 0 13.80 11.50 8 12 0 5.90 11.80 12 -20 0 24.70 12.60 -20 8 0 -1.60 13.20 8 -20 0 8.50 13.00 -20 12 0 10.10 13.80 -20 8 0 13.70 18.90 -20 12 0 -6.50 17.80 12 8 0 25.60 12.70 20 -8 0 20.20 10.00 -12 -8 0 4.40 12.40 20 -12 0 4.00 9.60 20 -12 0 15.90 13.50 -12 20 0 6.40 10.20 -8 20 0 17.10 13.50 20 -8 0 26.90 13.20 -8 20 0 6.80 10.50 -8 20 0 8.80 7.60 20 -8 0 6.30 8.80 -8 -12 0 1.00 13.30 -8 -12 0 6.10 11.50 -12 20 0 -0.10 13.30 -12 -8 0 22.20 11.10 -20 13 0 80.69 17.50 -20 7 0 100.59 20.20 13 -20 0 76.29 17.10 -20 7 0 61.49 20.40 13 7 0 94.69 17.90 7 13 0 101.99 22.40 7 13 0 89.69 16.70 13 -20 0 92.09 17.20 7 -20 0 106.49 19.80 7 -20 0 92.89 18.90 -20 13 0 83.59 22.70 13 7 0 125.79 22.40 -13 -7 0 96.49 18.10 -13 20 0 62.59 16.10 -7 20 0 69.69 15.40 -7 -13 0 88.39 16.60 20 -13 0 84.89 22.60 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4 0 82.59 16.10 16 -20 0 100.39 17.20 -20 16 0 91.99 22.00 -20 16 0 130.09 23.00 4 -20 0 80.69 18.50 -20 4 0 93.69 20.30 4 16 0 97.49 17.30 -20 4 0 104.79 20.40 -4 -16 0 104.29 19.00 20 -16 0 90.39 16.00 20 -4 0 94.39 16.30 20 -4 0 128.59 24.60 -16 -4 0 86.59 17.30 -4 20 0 83.89 14.50 20 -4 0 124.99 24.60 -4 20 0 101.19 18.40 -16 20 0 82.19 18.90 -20 3 0 45.10 15.20 17 -20 0 57.19 18.70 3 -20 0 35.10 16.80 3 17 0 18.40 11.40 -20 3 0 23.80 17.30 -20 17 0 23.10 17.80 20 -17 0 41.50 13.20 -3 -17 0 25.30 17.80 -3 20 0 56.39 15.00 20 -3 0 42.40 13.60 -17 -3 0 44.30 15.90 -3 20 0 31.40 11.00 2 18 0 62.49 13.90 -20 18 0 48.20 18.30 18 -20 0 86.49 17.40 18 2 0 51.89 16.10 2 -20 0 59.39 15.00 20 -18 0 73.49 17.00 -2 -18 0 53.59 14.80 -18 20 0 55.69 17.30 20 -2 0 75.29 14.90 -2 20 0 66.09 13.20 -2 20 0 92.09 18.40 1 19 0 133.49 17.90 19 1 0 111.59 25.70 19 -20 0 153.98 18.20 -20 1 0 159.88 22.40 -20 19 0 121.79 23.40 1 -20 0 140.39 17.90 -19 -1 0 166.38 21.70 -1 20 0 131.79 18.00 -1 20 0 127.39 20.10 20 -19 0 151.08 16.60 -1 -19 0 139.69 18.60 20 -1 0 144.59 19.20 -19 20 0 145.79 23.50 20 -20 0 28.20 13.40 -20 20 0 14.40 16.90 0 -20 0 8.30 12.50 -20 0 0 15.80 15.90 20 0 0 15.50 13.60 0 20 0 13.40 12.40 -21 11 0 28.00 21.60 10 11 0 44.60 13.00 -21 10 0 44.00 15.70 -21 10 0 29.30 22.00 11 -21 0 59.39 15.10 -21 11 0 48.20 15.80 10 -21 0 60.29 15.00 11 10 0 62.89 14.30 21 -10 0 53.09 14.60 -11 21 0 51.69 15.90 -10 21 0 45.80 16.70 21 -11 0 43.00 13.60 -11 -10 0 49.00 14.60 21 -10 0 80.79 15.50 -10 -11 0 61.89 15.70 9 12 0 244.98 20.80 -21 9 0 249.38 24.80 9 -21 0 255.87 21.90 12 9 0 230.18 20.90 -21 12 0 251.97 24.40 12 -21 0 275.27 21.70 -21 9 0 218.38 31.50 -21 12 0 199.58 31.30 -12 21 0 205.38 25.00 -9 -12 0 251.37 22.70 21 -12 0 267.17 26.90 21 -12 0 272.37 18.20 21 -12 0 221.58 21.80 21 -9 0 260.37 19.80 -12 -9 0 244.18 21.40 -9 21 0 228.18 24.00 21 -9 0 293.57 25.80 -21 8 0 117.29 20.60 8 -21 0 106.99 19.20 -21 13 0 100.39 24.80 13 -21 0 129.79 18.60 8 13 0 102.59 18.10 -21 13 0 100.09 20.50 -21 8 0 68.29 22.90 13 8 0 97.49 16.60 21 -13 0 86.19 25.70 -8 21 0 104.09 20.10 -8 -13 0 114.29 19.50 21 -8 0 67.99 19.40 -13 -8 0 119.99 19.30 21 -8 0 112.99 24.50 21 -8 0 114.39 16.00 -13 21 0 102.29 22.10 7 14 0 9.10 12.50 -21 7 0 11.10 15.00 14 -21 0 5.10 12.40 -21 14 0 11.30 18.80 -21 7 0 -6.40 19.30 -7 21 0 13.00 9.00 -14 -7 0 17.50 13.80 -14 21 0 4.00 14.40 21 -7 0 12.80 11.80 -7 21 0 10.80 14.50 -7 -14 0 0.50 13.30 6 15 0 41.40 14.00 -21 6 0 55.29 20.20 -21 6 0 46.90 16.10 -21 15 0 39.10 21.30 15 6 0 33.90 18.60 6 -21 0 31.10 13.30 -15 -6 0 48.20 14.40 -6 21 0 42.70 14.70 -6 21 0 51.29 11.50 21 -6 0 77.69 17.30 -6 -15 0 40.30 20.60 -15 21 0 31.20 20.40 21 -15 0 52.29 13.00 5 16 0 -4.60 11.70 -21 5 0 0.20 18.20 16 5 0 14.20 12.60 -21 5 0 0.70 14.40 5 -21 0 -7.90 12.00 -21 16 0 0.50 19.60 16 -21 0 -1.10 12.10 -16 21 0 7.00 15.30 -5 21 0 20.00 13.20 -5 -16 0 -1.60 12.90 21 -5 0 4.10 12.10 -5 21 0 -6.10 9.90 17 -21 0 44.60 14.00 4 -21 0 5.60 13.00 -21 4 0 22.20 17.80 -21 17 0 21.90 19.00 4 17 0 20.60 11.90 17 4 0 25.40 14.30 -21 4 0 26.90 16.90 -4 21 0 20.20 14.60 -17 -4 0 29.00 14.10 -4 21 0 15.80 11.30 21 -17 0 20.40 11.70 21 -4 0 29.50 13.20 -17 21 0 16.70 16.80 -4 -17 0 20.20 13.20 18 -21 0 53.59 14.50 3 -21 0 38.60 14.50 -21 18 0 39.70 19.70 18 3 0 37.30 14.50 -21 3 0 52.49 16.20 3 18 0 48.00 14.10 -18 21 0 40.80 17.20 -3 -18 0 34.00 14.20 -3 21 0 32.00 12.30 -3 21 0 93.89 19.50 -18 -3 0 53.99 16.20 21 -18 0 58.29 13.80 21 -3 0 57.09 14.10 -21 2 0 11.00 14.00 -21 19 0 27.40 18.20 2 -21 0 18.50 14.30 2 19 0 13.50 12.30 19 -21 0 23.50 13.60 19 2 0 28.00 14.20 21 -19 0 21.50 13.10 -2 -19 0 9.00 13.00 -2 21 0 23.50 14.20 -19 -2 0 23.50 16.10 -19 21 0 2.00 15.90 -2 21 0 16.20 12.50 21 -2 0 23.40 15.00 -21 20 0 -7.60 16.90 -21 1 0 17.40 14.20 1 20 0 -1.00 12.20 1 -21 0 15.90 13.40 20 -21 0 9.50 13.60 20 1 0 5.90 13.20 -20 21 0 -1.50 15.90 21 -20 0 8.20 13.00 21 -1 0 7.40 13.00 -20 -1 0 5.30 14.00 -1 -20 0 5.00 12.70 -1 21 0 21.60 13.00 21 -21 0 39.10 14.20 0 -21 0 35.70 15.00 -21 0 0 34.10 15.60 -21 21 0 16.40 17.20 0 21 0 40.60 14.00 21 0 0 37.60 14.40 11 11 0 208.98 20.70 11 -22 0 192.68 19.30 -22 11 0 156.88 31.90 -22 11 0 198.28 32.80 -11 22 0 207.48 22.50 22 -11 0 238.98 19.90 -11 -11 0 207.58 22.30 12 -22 0 81.89 18.00 -22 10 0 51.19 22.80 12 10 0 43.10 13.60 -22 12 0 62.29 24.20 10 12 0 48.30 13.30 10 -22 0 43.00 14.10 -10 22 0 73.19 18.40 -12 -10 0 61.29 16.70 -10 -12 0 59.29 15.70 22 -10 0 98.09 17.00 -12 22 0 60.59 18.70 -22 9 0 47.70 23.00 9 -22 0 31.60 14.10 13 9 0 34.40 13.80 9 13 0 24.70 12.80 13 -22 0 23.70 14.10 -22 13 0 26.00 22.10 22 -9 0 46.60 12.60 -9 -13 0 25.90 14.80 -9 22 0 36.20 15.60 -13 -9 0 46.90 15.30 -13 22 0 42.40 18.50 14 8 0 125.29 19.30 14 -22 0 135.69 17.80 8 14 0 124.19 18.30 -22 8 0 153.98 31.60 8 -22 0 126.09 17.90 -22 8 0 148.99 27.40 -22 14 0 128.89 27.10 -8 22 0 106.79 21.60 -14 22 0 125.09 25.80 22 -8 0 141.39 18.40 -8 -14 0 136.89 20.50 -14 -8 0 149.39 20.60 15 7 0 19.00 14.40 7 15 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11.40 11.80 22 -4 0 12.20 13.50 3 19 0 -8.60 12.00 3 -22 0 -9.50 12.00 -22 19 0 -12.90 15.70 19 3 0 2.80 13.50 -22 3 0 3.60 14.70 19 -22 0 1.00 12.80 -19 22 0 -3.30 15.60 22 -19 0 5.30 11.60 -19 -3 0 -7.90 13.20 -3 22 0 12.50 12.10 -3 -19 0 -1.60 12.70 -3 22 0 11.40 14.50 22 -3 0 -3.40 15.60 2 -22 0 12.60 12.40 2 20 0 13.10 13.10 20 2 0 23.10 14.30 -22 20 0 2.90 17.80 -22 2 0 19.50 14.50 20 -22 0 22.10 13.90 -20 -2 0 23.80 14.80 -20 22 0 32.20 16.60 22 -2 0 25.30 13.60 22 -20 0 29.90 12.60 -2 22 0 31.90 13.20 -2 -20 0 28.80 13.10 1 -22 0 7.00 12.40 -22 1 0 11.50 14.50 1 21 0 22.00 13.70 21 1 0 10.20 13.90 21 -22 0 28.30 14.10 -22 21 0 3.70 15.80 22 -1 0 13.10 13.50 22 -21 0 18.70 12.50 -21 -1 0 29.30 16.20 -1 22 0 22.70 14.40 -1 -21 0 3.90 13.30 -21 22 0 10.70 16.00 -23 11 0 36.40 22.00 -23 12 0 43.20 17.40 11 12 0 37.50 14.60 -23 11 0 36.60 17.00 -23 12 0 5.50 20.90 12 -23 0 27.60 13.60 12 11 0 28.20 13.20 11 -23 0 31.70 14.80 -12 23 0 44.20 22.10 -11 23 0 26.50 15.80 -12 -11 0 25.20 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176.88 21.90 17 -3 3 169.88 14.90 17 -14 -3 192.58 17.80 -14 -3 -3 186.48 21.50 -3 17 -3 144.19 18.80 17 -14 -3 159.08 19.10 -14 17 3 135.79 21.90 -3 17 -3 128.29 17.60 -3 17 -3 172.48 19.70 -3 -14 3 185.28 20.10 17 -3 3 178.18 18.30 -14 -3 -3 183.48 20.80 -14 17 3 168.98 17.00 17 -3 3 179.78 21.30 -17 13 3 20.90 8.90 13 4 3 33.20 12.60 4 13 -3 24.80 12.40 13 -17 -3 9.40 10.50 4 13 -3 18.20 11.10 -17 4 -3 22.90 14.00 13 4 3 25.40 9.20 4 -17 3 34.80 11.60 4 -17 3 31.30 13.50 -17 4 -3 44.60 12.00 13 -17 -3 39.00 8.90 4 13 -3 4.10 10.70 13 -17 -3 14.70 11.00 -17 13 3 27.40 15.70 17 -4 3 21.20 13.70 17 -4 3 30.30 8.80 -4 17 -3 18.10 11.70 -13 -4 -3 33.40 11.90 -13 17 3 12.20 8.70 17 -13 -3 22.10 9.90 17 -4 3 20.00 10.50 -4 17 -3 26.80 11.70 -4 17 -3 8.90 10.50 -13 17 3 18.50 15.90 -4 -13 3 26.10 11.40 17 -13 -3 39.00 10.50 -4 -13 3 26.70 13.00 -13 -4 -3 30.70 13.50 17 -13 -3 25.90 11.20 12 5 3 19.60 9.40 -17 5 -3 36.60 11.60 5 -17 3 19.90 12.30 -17 12 3 6.00 13.60 5 12 -3 11.90 10.30 12 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218.48 19.80 16 3 -3 190.78 20.10 -19 3 3 166.68 21.60 -19 16 -3 190.98 22.30 16 3 -3 232.48 24.10 -19 3 3 198.08 23.60 3 16 3 208.78 17.40 3 -19 -3 214.18 23.20 19 -3 -3 183.38 19.00 19 -16 3 191.58 17.40 19 -3 -3 161.08 26.70 -16 -3 3 229.38 24.30 -16 -3 3 178.38 19.20 -16 -3 3 241.18 23.40 -16 19 -3 177.08 22.70 19 -3 -3 239.98 26.50 -3 19 3 120.99 28.10 -19 17 -3 302.77 25.70 -19 2 3 304.17 26.90 2 17 3 341.17 20.10 17 2 -3 325.37 28.70 17 -19 3 338.27 23.00 2 -19 -3 361.96 24.70 -19 2 3 287.97 25.30 17 2 -3 294.57 23.20 19 -2 -3 267.27 22.90 19 -17 3 312.57 21.00 -17 -2 3 343.97 26.30 -2 -17 -3 394.56 26.90 -17 19 -3 293.97 24.80 -2 19 3 338.87 31.00 -17 -2 3 257.77 23.70 19 -2 -3 329.57 24.80 1 18 3 44.10 11.70 -19 18 -3 29.90 15.20 -19 1 3 -4.10 14.80 18 -19 3 29.10 13.20 18 1 -3 36.80 10.40 18 1 -3 37.70 13.80 1 -19 -3 41.40 14.80 -19 1 3 34.70 16.10 -18 -1 3 31.10 14.70 -18 19 -3 27.60 15.90 19 -1 -3 31.90 10.10 19 -18 3 23.00 12.60 -18 -1 3 26.50 15.60 -1 19 3 36.70 12.70 19 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17 -3 41.30 14.90 -20 17 3 30.80 18.50 20 -17 -3 31.50 14.60 20 -3 3 31.60 11.70 -17 20 3 26.10 10.80 -17 -3 -3 27.50 15.60 -17 20 3 16.90 18.30 -3 20 -3 54.39 14.90 -3 -17 3 37.90 21.90 16 4 3 65.09 13.40 -20 16 3 52.99 19.10 16 -20 -3 27.00 12.00 4 -20 3 69.39 16.90 -20 4 -3 45.30 16.30 4 16 -3 48.70 15.40 4 16 -3 55.59 17.10 16 -20 -3 39.90 13.20 -16 -4 -3 96.29 19.80 20 -16 -3 80.19 18.40 -4 20 -3 67.69 16.40 -16 20 3 92.29 16.70 -4 20 -3 103.59 20.00 -4 -16 3 63.59 15.80 -16 20 3 28.70 19.00 20 -16 -3 44.60 12.90 20 -4 3 91.49 16.00 5 -20 3 32.90 13.90 15 -20 -3 9.00 12.10 5 15 -3 21.30 18.10 -20 5 -3 27.00 14.30 5 15 -3 11.70 21.90 15 -20 -3 26.50 13.50 -20 15 3 36.30 17.80 15 -20 -3 51.99 13.30 -20 5 -3 46.90 17.20 15 5 3 36.90 11.60 20 -15 -3 37.30 14.60 -15 -5 -3 51.79 16.20 20 -5 3 71.29 15.10 -15 20 3 20.10 19.30 -5 -15 3 85.39 21.50 20 -15 -3 41.70 11.80 -5 -15 3 47.60 14.90 -15 20 3 29.60 10.60 -5 20 -3 39.90 13.70 -20 6 -3 12.70 14.60 -20 14 3 27.80 18.00 14 6 3 6.50 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35.70 14.70 -17 20 -3 1.60 13.90 20 -3 -3 9.70 13.10 20 -3 -3 24.00 9.20 20 -17 3 11.20 12.10 -17 -3 3 19.20 15.50 18 -20 3 111.39 17.70 -20 18 -3 96.39 20.20 2 -20 -3 104.69 18.90 18 2 -3 107.59 18.60 18 2 -3 154.58 24.70 2 18 3 135.49 16.40 -20 2 3 96.29 20.80 -20 2 3 69.39 20.50 -18 -2 3 85.49 19.20 -18 -2 3 114.79 20.20 20 -2 -3 92.99 17.40 20 -2 -3 99.79 19.40 -18 20 -3 101.09 19.80 20 -18 3 114.19 17.30 19 1 -3 186.98 27.80 1 19 3 213.38 17.90 19 -20 3 238.18 20.70 -20 1 3 224.58 25.40 19 1 -3 177.38 19.20 -20 1 3 165.88 28.30 1 -20 -3 204.88 22.60 -20 19 -3 182.48 23.90 20 -19 3 235.98 20.00 -19 20 -3 187.98 24.30 -1 -19 -3 258.87 21.10 20 -1 -3 236.48 29.20 20 -1 -3 181.38 21.20 -1 20 3 235.18 18.50 20 -1 -3 211.88 19.90 -19 -1 3 203.78 23.30 -19 -1 3 150.48 31.90 -20 20 -3 44.70 16.90 -20 0 3 97.99 21.40 0 -20 -3 98.49 18.60 0 20 3 91.49 16.30 20 -20 3 69.99 16.60 -21 2 -3 60.19 17.30 19 2 3 41.30 13.00 2 -21 3 41.60 15.00 2 19 -3 3.20 16.40 19 -21 -3 17.60 13.80 -21 19 3 39.20 20.90 2 19 -3 36.60 16.00 -19 21 3 18.60 20.40 -2 -19 3 51.19 16.80 21 -2 3 42.10 13.90 -2 21 -3 51.69 18.70 -19 -2 -3 58.69 16.80 21 -19 -3 29.90 16.60 -21 3 -3 53.09 17.10 3 18 -3 66.29 16.70 -21 18 3 34.20 19.30 18 3 3 36.90 11.80 3 18 -3 27.40 14.30 3 -21 3 61.69 16.30 18 -21 -3 2.20 14.80 -18 21 3 28.20 19.70 21 -3 3 46.50 14.30 -18 -3 -3 60.29 16.50 -3 21 -3 42.40 16.20 -3 -18 3 90.19 19.30 21 -18 -3 43.60 15.90 -21 4 -3 26.60 15.90 4 -21 3 21.90 15.70 4 17 -3 7.30 15.90 -21 17 3 23.60 20.10 4 17 -3 14.80 13.00 17 4 3 28.30 12.70 21 -17 -3 -1.90 11.30 -17 21 3 11.20 18.40 -4 -17 3 16.10 14.60 -4 21 -3 44.10 14.90 -17 -4 -3 22.20 14.70 21 -4 3 3.50 12.60 21 -17 -3 8.20 14.30 5 -21 3 15.80 14.90 -21 16 3 17.70 18.70 -21 5 -3 6.50 14.30 16 -21 -3 -17.80 12.40 16 5 3 7.80 10.70 5 16 -3 3.20 13.50 21 -16 -3 -2.30 13.10 21 -5 3 14.00 12.00 -16 21 3 -11.50 17.60 21 -16 -3 31.90 12.80 -16 -5 -3 8.30 14.00 -5 -16 3 15.30 14.20 -5 21 -3 4.90 18.90 21 -16 -3 2.90 10.80 -21 6 -3 24.90 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5 -3 3.10 11.00 -21 5 3 32.50 17.60 -16 -5 3 15.80 14.40 -5 21 3 53.19 20.70 21 -16 3 31.20 12.50 -5 -16 -3 50.09 15.20 21 -5 -3 39.10 15.90 21 -5 -3 0.40 9.70 -16 21 -3 21.00 14.30 -21 4 3 69.79 20.00 17 4 -3 22.20 12.20 4 17 3 48.20 12.20 4 -21 -3 13.70 14.80 -21 4 3 15.80 16.30 17 -21 3 54.39 14.40 -21 17 -3 47.50 16.90 -17 21 -3 35.30 14.20 -4 -17 -3 101.99 20.10 21 -17 3 70.89 16.10 -17 -4 3 61.89 16.80 21 -4 -3 57.19 15.10 -4 21 3 45.50 21.20 21 -4 -3 26.40 10.90 18 -21 3 121.49 18.70 -21 3 3 116.79 22.70 3 18 3 108.49 16.60 -21 3 3 134.19 28.40 21 -3 -3 126.19 19.60 -18 -3 3 124.49 21.10 21 -3 -3 112.79 17.40 -3 -18 -3 159.38 21.00 -18 21 -3 66.99 17.30 21 -18 3 116.99 17.70 -3 21 3 106.29 17.10 -21 2 3 40.00 21.00 2 19 3 25.00 11.60 19 2 -3 24.20 12.30 -21 2 3 18.50 18.20 19 -21 3 28.40 13.70 2 -21 -3 -4.40 12.00 -21 19 -3 10.80 15.50 -2 21 3 27.20 13.20 -19 -2 3 24.60 16.50 21 -2 -3 16.70 13.90 -2 -19 -3 55.69 16.00 21 -19 3 31.60 12.70 -19 21 -3 12.00 13.80 -22 17 3 25.10 19.60 5 -22 3 26.20 15.30 -22 5 -3 38.50 16.50 17 5 3 25.30 12.10 5 17 -3 17.70 14.00 17 -22 -3 5.90 13.40 -5 -17 3 28.60 14.60 -17 22 3 6.70 17.40 22 -17 -3 31.40 15.70 -5 22 -3 8.70 14.90 22 -5 3 41.90 13.00 -17 -5 -3 42.90 15.90 -22 6 -3 26.40 15.90 -22 16 3 16.90 20.80 6 16 -3 -0.20 12.10 6 -22 3 32.20 14.30 16 6 3 19.60 12.40 16 -22 -3 -3.60 13.00 -16 22 3 17.30 18.10 -16 -6 -3 42.60 16.00 22 -16 -3 13.30 15.60 -6 22 -3 43.40 15.00 -6 -16 3 19.00 14.90 15 7 3 14.60 10.90 -22 15 3 38.00 20.30 -22 7 -3 25.90 14.90 7 -22 3 33.60 14.60 15 -22 -3 14.00 13.60 7 15 -3 9.80 13.40 -15 -7 -3 43.10 15.10 -7 22 -3 25.70 14.60 -7 -15 3 19.90 15.10 -15 22 3 9.00 17.90 22 -15 -3 51.99 14.70 -22 14 3 114.79 26.30 14 -22 -3 46.30 15.30 8 14 -3 63.69 15.20 14 8 3 82.69 14.00 8 -22 3 92.69 20.00 -22 8 -3 109.99 21.90 -22 8 -3 117.59 21.90 -14 -8 -3 90.69 17.90 22 -14 -3 141.99 19.80 22 -8 3 76.49 14.70 -8 22 -3 84.29 19.40 22 -14 -3 92.39 18.80 -8 -14 3 109.79 20.10 -14 22 3 74.29 21.90 13 -22 -3 41.10 15.10 -22 9 -3 8.20 15.30 9 13 -3 16.00 12.30 13 9 3 19.30 10.90 -22 13 3 65.39 20.90 -22 9 -3 25.40 16.70 9 -22 3 32.00 14.80 -13 -9 -3 28.50 14.60 -13 22 3 18.40 18.30 22 -13 -3 12.00 11.30 22 -13 -3 34.30 15.20 22 -9 3 -19.70 12.40 -9 22 -3 13.30 13.80 -22 12 3 206.18 29.10 10 -22 3 241.98 22.40 12 -22 -3 189.48 21.10 12 10 3 172.88 17.50 10 12 -3 157.48 19.70 -22 10 -3 184.58 24.90 -22 10 -3 222.68 24.40 -10 -12 3 228.38 22.60 -10 22 -3 175.28 22.50 -12 22 3 173.58 29.70 22 -12 -3 243.78 23.40 -12 -10 -3 249.97 23.80 -22 11 3 199.78 28.00 11 11 -3 161.38 19.80 11 -22 3 206.28 21.70 11 11 3 203.88 17.80 -22 11 -3 249.68 24.90 11 -22 -3 177.68 13.90 -22 11 -3 229.18 24.80 11 -22 -3 182.58 21.40 -11 -11 3 262.07 23.30 -11 22 -3 199.08 22.50 -11 22 3 194.18 29.60 -11 -11 -3 247.38 22.50 12 10 -3 -2.60 12.00 12 -22 3 14.10 12.90 -22 10 3 -24.20 15.50 -22 10 3 0.40 19.20 10 12 3 5.60 10.20 10 -22 -3 21.70 14.50 -22 12 -3 11.70 15.90 -22 12 -3 27.00 16.10 -12 -10 3 25.30 15.60 -12 22 -3 7.00 14.20 22 -10 -3 17.60 14.00 -22 13 -3 144.19 21.40 13 -22 3 128.89 19.50 -22 13 -3 139.09 23.20 13 9 -3 92.79 16.60 9 -22 -3 141.69 20.40 -22 9 3 106.19 21.40 9 13 3 106.69 15.80 -22 9 3 79.59 23.70 -9 -13 -3 179.88 21.70 -13 -9 3 147.39 22.50 22 -9 -3 136.49 21.70 -13 22 -3 115.99 18.50 -9 22 3 131.69 26.30 14 8 -3 42.90 13.60 -22 8 3 14.10 28.00 -22 14 -3 41.40 15.80 -22 8 3 38.90 18.70 8 14 3 69.79 15.10 -22 14 -3 68.49 18.80 22 -8 -3 70.89 18.00 -14 22 -3 41.50 14.30 -8 22 3 22.40 22.00 15 -22 3 16.20 12.80 15 7 -3 8.70 11.20 -22 7 3 -1.50 16.70 7 15 3 25.30 11.40 -22 7 3 6.10 22.50 -22 15 -3 24.70 16.40 7 -22 -3 23.20 14.20 -7 22 3 49.10 20.80 22 -7 -3 44.90 15.70 22 -7 -3 8.10 10.10 -15 22 -3 9.20 13.10 -7 -15 -3 51.19 16.00 -22 6 3 -2.40 21.40 6 16 3 18.30 11.20 16 -22 3 16.40 13.60 16 6 -3 -4.30 11.40 -22 16 -3 10.30 16.70 -22 6 3 -9.90 17.40 6 -22 -3 3.70 14.00 -16 -6 3 5.20 14.40 22 -6 -3 23.10 15.60 22 -6 -3 19.60 9.50 -16 22 -3 2.20 13.10 22 -16 3 20.40 12.60 -6 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45.90 9.40 -7 11 -4 59.39 11.30 11 -7 4 22.50 12.30 11 -4 -4 40.70 13.60 11 -7 4 48.40 10.00 -7 -4 4 58.39 11.80 3 -11 -4 149.79 22.00 8 3 -4 79.29 17.80 3 8 4 104.19 12.40 -11 3 4 128.69 15.50 3 -11 -4 150.38 16.60 -11 8 -4 114.89 17.50 -11 8 -4 105.29 10.60 8 -11 4 122.39 16.60 8 -11 4 108.99 14.40 3 -11 -4 101.99 11.90 -11 8 -4 98.19 18.70 8 3 -4 99.39 13.20 3 8 4 91.09 18.20 -8 -3 4 136.59 15.60 -8 11 -4 99.79 15.10 -3 -8 -4 109.09 11.50 11 -3 -4 100.89 10.20 -3 -8 -4 117.89 16.80 -8 -3 4 101.49 14.00 11 -8 4 103.99 15.00 -8 -3 4 114.09 12.10 -3 11 4 97.29 16.70 -3 11 4 126.59 15.80 -8 11 -4 77.79 17.50 11 -3 -4 86.29 18.20 -8 11 -4 104.19 12.00 -3 -8 -4 118.59 21.90 2 -11 -4 30.00 9.50 9 -11 4 35.20 10.00 9 2 -4 46.80 11.40 2 9 4 37.20 9.40 2 9 4 29.00 12.20 -11 2 4 70.49 14.10 -11 9 -4 25.50 14.40 9 2 -4 37.50 14.80 -11 9 -4 37.00 7.50 9 -11 4 30.30 10.30 -11 2 4 31.60 9.20 -9 -2 4 33.10 8.50 -9 11 -4 34.50 8.60 -9 11 -4 28.80 9.10 -2 -9 -4 49.30 14.00 -2 -9 -4 42.10 13.50 -9 -2 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50.89 11.20 -7 12 4 86.39 17.90 12 -7 -4 69.39 13.60 12 -5 4 61.29 14.70 6 -12 4 136.89 15.30 6 -12 -4 132.59 14.10 6 6 -4 113.89 19.90 -12 6 4 152.48 15.50 6 -12 4 120.29 18.10 6 6 4 125.09 21.00 -12 6 -4 139.69 20.70 -12 6 -4 116.49 18.70 -12 6 -4 127.59 10.70 -6 12 -4 104.29 18.20 -6 12 4 141.29 15.80 -6 -6 -4 151.58 20.40 12 -6 -4 154.48 15.30 -6 -6 -4 141.99 17.70 -6 -6 -4 125.69 11.60 -6 -6 4 149.09 14.90 12 -6 -4 97.69 17.40 -6 12 -4 167.28 15.70 12 -6 -4 146.89 11.20 -6 12 -4 142.19 17.10 -6 12 4 150.48 18.30 -6 -6 4 118.69 16.50 12 -6 4 148.29 16.70 12 -6 4 125.09 22.20 12 -6 -4 116.69 12.40 -6 -6 4 132.49 13.70 5 -12 -4 15.60 8.50 -12 7 -4 12.90 12.80 7 5 -4 5.60 13.10 -12 7 -4 4.00 13.40 5 7 4 5.80 10.90 -12 7 -4 13.30 6.40 -12 5 4 44.50 11.90 7 -12 4 12.70 10.60 7 -12 4 13.40 10.30 -5 -7 -4 26.90 12.00 12 -5 -4 0.90 12.50 -7 12 -4 4.40 8.50 -7 -5 4 21.20 9.10 12 -5 -4 25.20 8.40 12 -7 4 18.90 9.40 -5 12 4 16.00 11.90 12 -5 -4 4.50 6.00 -5 -7 -4 8.80 11.10 -7 -5 4 22.70 11.00 -7 -5 4 11.70 9.10 -7 12 -4 17.20 13.30 -5 12 4 11.90 9.30 -7 12 -4 24.00 8.50 12 -7 4 -8.00 13.00 -5 -7 -4 10.90 8.00 -12 8 -4 42.30 9.10 -12 8 -4 31.10 13.10 -12 8 -4 56.39 15.40 8 -12 4 36.90 10.80 4 8 4 34.70 12.30 -12 4 4 59.79 12.50 8 4 -4 66.29 14.10 4 8 4 63.19 10.60 8 -12 4 67.09 14.00 4 -12 -4 44.80 10.30 8 4 -4 18.70 13.30 -4 -8 -4 49.40 11.00 -8 -4 4 29.50 16.00 12 -4 -4 37.20 14.00 12 -8 4 33.80 9.20 -4 12 4 45.20 11.00 -8 12 -4 42.00 14.90 12 -8 4 11.90 13.50 -8 12 -4 44.20 10.10 12 -4 -4 32.70 7.00 -8 -4 4 42.50 10.70 -8 -4 4 42.90 10.00 -4 -8 -4 47.60 13.00 -8 12 -4 57.09 11.10 -4 12 4 58.09 13.40 -4 -8 -4 43.60 13.20 9 -12 4 293.57 19.50 -12 9 -4 301.87 23.40 -12 3 4 301.87 18.50 3 -12 -4 350.06 22.70 3 9 4 283.17 17.50 3 -12 -4 277.07 17.20 3 9 4 276.67 25.00 9 3 -4 309.37 18.80 9 -12 4 298.27 21.70 -12 9 -4 297.07 24.00 3 -12 -4 354.26 26.70 9 3 -4 282.97 23.70 -12 9 -4 288.17 15.30 -12 3 4 244.18 17.80 -3 -9 -4 277.57 16.10 -3 -9 -4 287.27 25.20 -9 12 -4 277.27 22.80 -3 12 4 290.07 21.80 -9 -3 4 249.68 18.60 12 -3 -4 258.27 16.10 -9 -3 4 328.77 19.80 -9 12 -4 301.87 20.80 -3 -9 -4 333.67 22.70 12 -9 4 289.47 20.50 -9 -3 4 280.07 20.20 -3 12 4 292.07 21.20 12 -3 -4 318.17 19.40 12 -3 -4 276.97 22.60 -9 12 -4 283.17 16.40 -12 10 -4 340.47 17.40 -12 10 -4 367.36 26.10 10 -12 4 368.46 21.60 -12 2 4 351.86 21.00 2 -12 -4 363.26 19.60 2 10 4 383.46 28.30 -12 2 4 417.36 22.10 10 2 -4 352.76 23.90 2 10 4 352.56 20.80 10 2 -4 350.06 21.10 10 -12 4 363.06 23.30 2 -12 -4 418.66 24.50 2 -12 -4 419.36 30.00 -2 12 4 381.16 25.80 -10 12 -4 354.86 22.60 -2 -10 -4 347.67 18.90 -10 -2 4 314.47 21.50 -10 12 -4 354.56 18.70 -2 -10 -4 416.96 25.90 12 -2 -4 364.46 23.50 12 -2 -4 378.16 21.00 12 -10 4 363.16 22.60 -2 -10 -4 410.36 28.30 12 -2 -4 338.47 18.70 -10 12 -4 375.26 24.90 -10 -2 4 396.66 21.60 -10 -2 4 357.96 22.80 -2 12 4 382.26 22.90 -12 11 -4 3.70 13.30 -12 11 -4 8.20 6.00 1 -12 -4 15.00 8.50 11 1 -4 8.70 7.50 -12 11 -4 8.60 8.50 11 1 -4 9.80 14.00 11 1 -4 10.70 6.40 11 -12 4 19.40 10.10 1 11 4 11.40 10.10 -12 1 4 17.60 9.80 1 11 4 16.70 11.60 11 -12 4 20.50 9.40 12 -11 4 11.50 8.70 -11 12 -4 19.90 13.50 -1 12 4 17.70 11.40 12 -1 -4 4.50 13.50 -1 12 4 2.90 10.70 12 -1 -4 13.30 6.20 -1 -11 -4 32.50 12.90 -1 -11 -4 15.50 8.30 12 -11 4 9.80 9.80 -11 12 -4 10.50 8.90 0 -12 -4 597.94 30.20 -12 12 -4 507.75 29.80 0 -12 -4 615.74 36.10 -12 0 4 553.34 25.70 12 0 -4 500.05 24.90 12 0 -4 473.45 26.80 -12 12 -4 486.15 27.80 -12 0 4 541.05 26.30 0 12 4 526.35 27.30 12 -12 4 517.55 25.50 0 -12 -4 561.54 24.20 12 0 -4 549.15 29.80 0 12 4 529.05 30.50 12 -12 4 499.55 27.90 0 13 -4 265.57 21.60 -13 0 -4 211.18 17.10 13 0 4 234.98 23.60 -13 13 4 204.58 15.60 13 0 4 184.28 17.60 -13 0 -4 204.68 12.60 -13 13 4 199.28 18.80 -13 0 -4 202.18 21.60 0 -13 4 241.58 20.90 0 13 -4 205.58 20.50 0 -13 4 198.88 22.50 13 -13 -4 212.38 17.30 0 13 -4 159.38 19.50 1 12 -4 34.90 13.10 -13 12 4 20.80 7.30 1 12 -4 25.30 12.70 1 -13 4 20.40 11.00 -13 1 -4 18.30 10.00 12 1 4 6.40 13.60 1 -13 4 23.80 12.80 12 -13 -4 22.00 10.10 -13 1 -4 17.20 13.80 -13 12 4 45.10 12.90 -13 1 -4 37.40 8.30 -12 -1 -4 21.80 9.50 -12 -1 -4 45.90 8.90 -12 13 4 33.20 12.50 -12 -1 -4 20.40 13.00 -1 -12 4 27.00 12.40 -1 -12 4 29.40 12.00 13 -1 4 -2.00 11.50 -12 13 4 19.20 7.40 -1 13 -4 27.00 12.90 13 -1 4 17.50 8.40 -1 13 -4 18.60 9.80 13 -12 -4 21.30 10.10 -13 2 -4 42.80 8.60 -13 11 4 37.60 7.60 2 11 -4 16.90 9.70 -13 2 -4 22.70 13.60 -13 11 4 46.30 13.30 2 -13 4 75.79 17.30 11 -13 -4 39.30 10.30 2 -13 4 41.70 12.20 2 11 -4 23.50 12.40 2 11 -4 56.19 13.90 11 2 4 34.70 12.70 -13 2 -4 40.60 11.80 -11 -2 -4 32.70 13.90 13 -2 4 29.70 10.00 -2 -11 4 34.00 11.60 13 -11 -4 30.80 11.00 -2 -11 4 44.00 12.30 -11 13 4 59.39 14.20 -2 13 -4 29.80 12.80 13 -2 4 28.50 13.00 -11 13 4 31.60 8.30 -11 -2 -4 46.30 9.30 -2 13 -4 14.70 10.50 10 3 4 223.78 24.80 -13 10 4 231.28 20.40 3 -13 4 261.17 20.40 3 10 -4 249.88 21.20 -13 3 -4 213.88 12.90 -13 3 -4 231.68 19.20 10 -13 -4 213.18 16.70 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16.10 4 9 4 55.69 12.50 4 9 4 61.59 13.60 -13 4 4 56.09 11.10 -13 9 -4 64.59 8.80 -13 9 -4 61.69 14.40 9 -13 4 66.59 17.00 9 -13 4 73.19 14.80 4 -13 -4 63.99 11.80 -13 9 -4 94.79 18.60 13 -4 -4 57.09 10.80 -4 -9 -4 109.49 21.50 -4 13 4 95.49 17.30 -9 -4 4 65.59 13.20 -4 13 4 71.59 15.80 -9 13 -4 58.59 15.10 -9 13 -4 64.99 15.20 -9 -4 4 62.59 15.30 -9 13 -4 74.09 11.00 -4 -9 -4 79.39 11.40 13 -9 4 58.09 14.50 13 -4 -4 66.69 14.50 -4 -9 -4 91.59 17.70 3 10 4 37.20 10.10 10 3 -4 62.99 14.20 -13 10 -4 51.49 14.10 3 -13 -4 48.90 9.50 -13 10 -4 53.49 8.20 10 -13 4 48.40 11.70 10 -13 4 40.30 10.40 -13 10 -4 53.49 15.00 10 3 -4 36.10 13.60 -13 3 4 48.20 10.80 3 10 4 42.80 13.00 -3 13 4 56.79 12.90 -3 -10 -4 46.50 9.40 -3 13 4 27.70 10.90 -10 13 -4 54.39 14.60 13 -10 4 37.00 10.20 -10 13 -4 67.89 15.90 13 -3 -4 31.40 12.70 13 -3 -4 34.40 7.20 -10 -3 4 42.10 10.00 -10 -3 4 34.70 9.90 -13 2 4 403.36 30.50 2 11 4 464.65 30.40 2 -13 -4 536.05 28.40 -13 11 -4 421.86 25.30 -13 2 4 475.85 23.80 -13 11 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49.90 9.20 14 -11 -4 34.10 11.20 -11 14 4 20.00 8.60 10 4 4 237.68 23.90 -14 4 -4 259.37 23.40 4 10 -4 250.77 22.40 -14 4 -4 258.67 20.60 4 -14 4 279.67 20.40 10 -14 -4 245.98 17.40 4 10 -4 239.98 20.60 10 -14 -4 204.88 17.90 -14 4 -4 235.58 13.60 -14 10 4 266.87 19.50 4 -14 4 269.07 23.60 14 -4 4 238.18 19.00 -10 -4 -4 248.08 23.60 14 -4 4 264.67 25.30 -4 -10 4 269.87 20.10 -10 -4 -4 256.07 14.30 -10 14 4 267.17 22.50 -4 14 -4 260.27 21.60 14 -10 -4 258.67 19.80 14 -10 -4 256.07 21.40 -4 14 -4 226.08 21.30 14 -10 -4 200.88 18.20 -10 -4 -4 277.27 22.10 -10 14 4 234.68 18.40 -4 -10 4 258.07 23.40 5 9 -4 273.57 22.50 5 9 -4 329.67 24.20 -14 9 4 359.16 21.60 5 -14 4 386.26 23.00 5 -14 4 349.37 24.60 -14 5 -4 318.67 23.80 -14 5 -4 316.27 15.90 -14 5 -4 354.46 23.40 9 5 4 333.87 27.70 9 -14 -4 344.57 19.50 -5 14 -4 315.47 24.10 14 -9 -4 339.37 22.20 14 -9 -4 348.87 23.30 14 -9 -4 289.57 20.20 -9 -5 -4 337.57 23.80 -9 -5 -4 303.27 26.40 -9 14 4 362.56 24.40 -9 14 4 348.57 21.30 -5 -9 4 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156.58 16.00 -3 14 4 191.48 19.40 -11 -3 4 196.38 17.70 -3 -11 -4 182.58 12.20 14 -11 4 172.88 17.10 -3 14 4 161.78 19.20 14 -3 -4 156.78 14.30 -11 14 -4 160.48 18.80 14 -3 -4 168.18 19.70 -14 12 -4 10.20 13.00 -14 12 -4 6.80 8.40 2 -14 -4 16.40 7.30 -14 2 4 16.70 9.80 12 -14 4 18.30 9.10 12 -14 4 12.70 10.00 12 2 -4 4.90 8.50 12 2 -4 9.10 12.80 -14 2 4 10.30 10.40 2 12 4 16.20 11.80 2 -14 -4 16.90 13.30 2 12 4 13.00 10.30 -14 12 -4 1.10 7.10 -2 -12 -4 29.60 13.90 14 -2 -4 13.10 6.60 -2 14 4 11.70 11.60 -2 -12 -4 18.10 7.30 14 -2 -4 15.70 12.60 14 -12 4 -0.40 8.50 -2 -12 -4 33.40 13.40 -2 14 4 7.40 10.30 14 -12 4 5.70 9.90 -12 14 -4 13.90 8.30 -12 14 -4 4.60 11.80 -12 -2 4 4.30 10.10 13 1 -4 225.48 20.80 13 -14 4 178.38 19.30 1 -14 -4 238.18 13.80 -14 13 -4 246.18 21.90 -14 13 -4 221.88 18.00 13 1 -4 175.78 19.10 1 13 4 244.48 22.90 1 13 4 206.68 19.40 -14 1 4 217.18 19.30 13 1 -4 213.38 16.30 13 -14 4 223.08 16.60 -14 1 4 222.98 17.40 14 -13 4 237.78 17.80 14 -13 4 209.28 18.80 -13 14 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361.76 27.80 -15 4 -4 415.86 24.80 11 4 4 427.46 28.50 11 4 4 394.56 22.40 -15 4 -4 405.56 27.20 4 11 -4 414.06 25.80 11 -15 -4 403.56 21.60 4 11 -4 440.66 26.40 -15 4 -4 388.16 18.40 4 -15 4 444.26 25.20 11 -15 -4 421.16 24.60 -15 11 4 392.86 24.70 11 -15 -4 392.36 26.00 15 -11 -4 427.66 26.80 -4 -11 4 431.06 24.10 15 -11 -4 339.67 23.60 -11 15 4 465.15 27.10 15 -11 -4 440.86 24.00 15 -4 4 414.06 24.70 -4 15 -4 409.66 25.00 15 -4 4 441.46 29.90 -11 -4 -4 410.26 19.00 -4 15 -4 381.76 25.90 -11 -4 -4 431.26 26.90 -4 -11 4 409.26 27.60 -11 15 4 416.56 23.40 15 -11 -4 371.26 21.60 -11 -4 -4 422.26 28.10 10 -15 -4 15.90 9.00 5 -15 4 36.90 12.30 -15 5 -4 22.50 15.30 5 10 -4 16.80 12.20 5 10 -4 6.70 9.50 -15 10 4 29.00 12.30 10 5 4 4.10 13.20 -15 5 -4 23.90 11.10 5 -15 4 12.40 10.70 -15 5 -4 15.00 6.20 10 -15 -4 12.40 9.90 15 -10 -4 29.80 12.10 -10 -5 -4 23.30 6.90 15 -10 -4 -0.70 7.80 15 -10 -4 16.60 11.00 -10 15 4 23.90 13.30 -5 -10 4 41.10 11.20 -5 15 -4 4.30 10.20 15 -5 4 5.10 11.10 -10 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345.17 23.70 -7 -8 4 365.16 20.50 -7 -8 4 314.17 23.00 -8 15 4 308.07 21.60 -7 15 -4 310.37 24.10 -8 15 4 342.77 23.90 -7 15 -4 282.97 22.80 15 -8 -4 301.07 18.30 -8 -7 -4 303.17 15.90 15 -7 4 323.17 27.30 15 -8 -4 260.97 19.50 -7 15 -4 371.66 19.90 15 -8 -4 378.26 23.10 -15 8 -4 13.20 5.40 -15 8 -4 20.50 14.40 8 7 -4 5.80 9.30 8 7 -4 1.20 12.90 7 -15 -4 9.00 8.00 7 -15 -4 7.40 10.40 -15 8 -4 20.40 12.00 -15 7 4 17.20 11.30 8 -15 4 26.30 11.30 8 -15 4 22.20 11.30 7 8 4 21.20 12.10 7 -15 -4 2.50 11.20 -7 -8 -4 16.80 7.20 -7 15 4 29.90 13.30 -8 15 -4 8.50 12.00 15 -7 -4 7.90 11.80 15 -7 -4 -2.90 7.10 -8 -7 4 11.00 10.90 -8 15 -4 6.10 8.50 15 -8 4 22.20 11.70 -7 -8 -4 22.10 12.10 -7 -8 -4 14.60 11.30 -8 -7 4 18.00 9.80 15 -8 4 11.60 8.90 -7 15 4 8.40 8.80 -15 9 -4 56.59 14.80 9 -15 4 70.59 15.00 9 -15 4 72.59 13.30 -15 9 -4 51.99 8.00 6 -15 -4 81.19 11.30 -15 6 4 66.39 12.90 6 -15 -4 107.49 17.40 -15 9 -4 74.09 15.50 6 9 4 84.09 19.60 9 6 -4 59.09 14.20 6 9 4 43.80 10.60 -9 -6 4 82.49 14.90 15 -9 4 62.19 11.70 -9 15 -4 75.09 15.60 -6 -9 -4 74.19 9.90 15 -6 -4 46.80 9.10 15 -9 4 44.40 14.90 -6 15 4 67.29 14.10 15 -6 -4 75.09 14.40 -6 15 4 65.79 15.80 -6 -9 -4 80.29 15.90 15 -6 -4 96.89 17.10 -9 15 -4 76.09 10.20 -9 15 -4 61.49 11.80 -15 5 4 60.99 13.00 10 5 -4 59.69 13.80 10 -15 4 58.89 12.00 -15 5 4 60.79 12.30 -15 10 -4 77.09 15.90 -15 10 -4 78.09 18.20 5 10 4 72.39 14.40 5 -15 -4 64.79 10.50 5 10 4 58.09 12.10 10 -15 4 79.09 14.90 -15 10 -4 42.00 7.60 -10 15 -4 81.09 16.80 -5 -10 -4 67.39 8.80 -5 15 4 73.49 15.00 -10 -5 4 60.79 13.70 -10 -5 4 72.39 16.00 15 -5 -4 54.29 11.90 -5 -10 -4 86.49 17.30 15 -5 -4 67.49 14.40 -10 15 -4 70.89 15.60 15 -10 4 38.60 12.60 -5 15 4 59.19 11.80 15 -10 4 58.39 11.50 4 -15 -4 31.70 8.30 -15 11 -4 14.60 5.20 11 -15 4 10.50 10.30 4 11 4 9.60 10.00 4 11 4 36.20 12.50 -15 11 -4 28.80 12.90 -15 4 4 24.60 10.70 11 4 -4 31.60 10.00 -15 4 4 24.90 11.20 11 4 -4 16.20 13.10 -15 11 -4 25.40 14.60 11 -15 4 23.10 11.20 -11 -4 4 24.70 10.00 15 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197.18 18.80 -13 -2 4 162.58 15.00 15 -2 -4 153.98 19.30 -2 15 4 152.78 22.10 -2 -13 -4 168.48 12.40 -13 15 -4 158.08 17.60 -15 14 -4 -0.40 13.10 1 14 4 12.70 11.80 14 1 -4 -13.80 8.80 14 -15 4 0.20 9.80 14 1 -4 20.70 7.30 -15 1 4 4.70 11.90 1 -15 -4 4.10 6.90 -15 14 -4 10.80 7.80 -15 1 4 -3.90 9.70 14 -15 4 -10.00 9.10 14 1 -4 -2.80 12.70 1 14 4 7.00 12.50 -14 -1 4 -6.40 10.20 -1 15 4 3.90 13.60 15 -14 4 -11.90 9.50 -1 15 4 -2.90 11.00 -1 -14 -4 38.40 14.60 15 -14 4 3.50 9.80 -14 15 -4 -1.10 12.40 -14 -1 4 2.80 9.10 -14 15 -4 9.10 8.80 15 -1 -4 -8.80 12.90 -1 -14 -4 3.30 7.10 0 15 4 92.09 21.90 -15 0 4 151.68 18.70 15 0 -4 166.28 18.60 15 -15 4 123.49 16.10 0 15 4 126.79 19.10 -15 15 -4 130.09 20.60 0 -15 -4 152.78 12.10 15 0 -4 119.59 15.40 15 0 -4 152.68 19.50 -15 0 4 138.19 16.70 -15 15 -4 107.09 17.40 15 -15 4 149.59 16.50 -16 0 -4 9.20 16.40 -16 16 4 15.70 8.30 0 -16 4 -4.50 11.70 16 -16 -4 10.80 10.00 -16 16 4 -2.40 15.10 0 16 -4 1.70 13.00 0 -16 4 1.60 14.00 16 0 4 3.70 9.20 15 -16 -4 11.20 10.40 1 -16 4 23.10 14.70 -16 15 4 14.40 14.50 15 -16 -4 5.70 10.30 15 -16 -4 1.10 10.00 -16 15 4 4.00 8.00 15 1 4 11.00 9.50 -16 1 -4 1.60 13.50 1 15 -4 11.40 12.90 16 -1 4 16.40 9.10 16 -15 -4 15.40 10.50 -1 -15 4 29.30 12.30 -15 16 4 25.80 8.40 -1 -15 4 14.00 13.40 16 -15 -4 -7.50 10.10 -1 16 -4 14.90 12.60 -15 -1 -4 15.30 14.20 -15 16 4 3.10 14.70 -16 14 4 104.09 13.50 14 -16 -4 70.19 13.70 -16 2 -4 87.89 19.50 2 14 -4 60.39 12.70 -16 2 -4 72.29 13.70 -16 14 4 54.79 16.80 14 -16 -4 91.39 13.60 2 14 -4 34.40 15.30 14 2 4 88.69 21.60 2 14 -4 57.89 14.80 2 -16 4 99.59 18.30 2 -16 4 84.89 19.60 14 -16 -4 75.39 17.40 -2 16 -4 74.19 15.90 16 -14 -4 78.99 15.40 -2 -14 4 91.99 17.40 -14 16 4 55.39 14.90 -2 -14 4 79.39 19.80 -14 -2 -4 109.19 19.00 16 -2 4 72.59 12.10 -16 3 -4 141.79 18.90 3 13 -4 154.08 20.20 3 13 -4 126.69 18.30 -16 3 -4 133.39 18.10 13 3 4 129.29 22.20 13 -16 -4 134.59 15.00 -16 13 4 147.79 17.50 3 -16 4 128.79 20.90 3 -16 4 169.98 19.70 13 -16 -4 117.49 19.10 13 -16 -4 101.89 17.00 -13 -3 -4 138.79 18.10 -13 16 4 153.48 21.00 16 -3 4 136.09 17.10 -3 -13 4 163.28 20.10 -13 -3 -4 138.79 22.00 -3 16 -4 158.98 19.80 -13 16 4 156.98 16.70 16 -3 4 142.99 13.50 16 -3 4 174.88 22.80 16 -13 -4 168.08 17.40 12 -16 -4 16.00 12.70 -16 4 -4 16.20 13.00 -16 12 4 36.70 13.80 -16 4 -4 46.30 12.40 4 -16 4 33.30 13.30 12 4 4 32.20 12.50 4 -16 4 28.20 11.10 4 12 -4 -2.80 12.30 12 -16 -4 24.70 11.00 12 -16 -4 17.60 8.60 4 12 -4 21.50 12.50 -12 16 4 26.50 15.50 16 -12 -4 38.80 12.60 16 -12 -4 13.10 9.00 -12 -4 -4 23.40 13.50 -12 16 4 6.10 9.20 -4 -12 4 16.60 11.40 16 -12 -4 6.60 10.10 16 -4 4 6.90 13.60 -12 -4 -4 32.00 11.40 -4 16 -4 19.20 10.40 16 -12 -4 23.20 11.60 -4 16 -4 25.20 13.00 -4 -12 4 40.60 13.10 16 -4 4 14.70 9.60 -16 5 -4 266.17 22.70 5 11 -4 239.68 21.80 11 -16 -4 281.87 18.10 5 -16 4 320.17 22.10 5 -16 4 286.57 25.30 -16 11 4 292.87 22.10 11 -16 -4 262.97 24.00 -16 5 -4 282.27 20.90 11 5 4 261.87 26.60 5 11 -4 281.57 22.90 11 -16 -4 332.77 21.70 -5 -11 4 309.17 21.40 -11 16 4 275.77 20.60 16 -5 4 269.17 21.60 -11 -5 -4 279.37 25.70 -11 16 4 292.37 24.70 -5 16 -4 260.87 21.20 -5 -11 4 296.47 22.80 -11 -5 -4 281.37 15.40 -11 -5 -4 310.97 23.50 16 -11 -4 302.67 21.30 16 -5 4 326.67 27.00 -16 10 4 485.35 26.90 6 -16 4 568.64 28.20 10 -16 -4 548.45 25.10 6 10 -4 524.05 28.70 -16 6 -4 520.95 29.00 10 -16 -4 508.15 30.40 6 10 -4 492.45 29.70 -16 6 -4 568.84 31.70 10 6 4 509.65 31.60 10 -16 -4 483.85 28.40 6 -16 4 497.85 29.60 -6 -10 4 490.25 29.90 -10 16 4 520.95 27.70 16 -6 4 551.14 33.10 -10 -6 -4 527.95 29.80 -10 16 4 488.85 30.40 -10 -6 -4 504.95 22.20 16 -10 -4 461.15 25.20 -6 16 -4 496.65 29.70 -6 -10 4 591.84 26.90 16 -10 -4 568.34 30.60 -10 -6 -4 502.35 31.50 -6 16 -4 494.95 29.40 16 -10 -4 564.14 28.10 16 -6 4 510.15 28.50 -6 -10 4 557.84 27.80 16 -10 -4 461.85 26.80 7 -16 4 50.49 12.50 9 -16 -4 31.30 9.00 9 7 4 21.00 12.30 9 -16 -4 26.10 11.30 7 -16 4 68.09 15.70 -16 9 4 57.39 13.50 -16 7 -4 36.30 16.00 -16 7 -4 52.49 13.10 7 9 -4 38.20 13.80 -9 16 4 43.00 14.90 -7 16 -4 31.30 10.60 16 -9 -4 46.10 10.40 16 -7 4 17.60 9.90 -9 -7 -4 46.10 13.30 -9 -7 -4 84.39 20.10 16 -7 4 38.80 12.70 -9 -7 -4 51.49 8.10 -7 16 -4 37.70 13.10 16 -9 -4 51.89 14.00 -7 -9 4 31.80 11.60 -7 -9 4 51.39 12.20 -9 16 4 28.10 9.80 8 -16 4 264.17 19.70 8 8 -4 207.88 20.10 -16 8 4 231.98 18.40 8 -16 -4 175.98 19.00 8 8 4 224.58 23.20 -16 8 -4 200.18 21.20 -16 8 -4 233.18 21.90 8 8 -4 215.58 21.40 8 -16 -4 249.48 15.90 8 -16 4 183.48 21.80 -8 -8 4 251.97 21.10 -8 16 -4 225.08 21.20 -8 -8 4 232.18 18.40 16 -8 4 221.18 25.10 -8 -8 -4 230.08 13.70 -8 -8 -4 253.67 21.80 16 -8 -4 222.88 19.90 -8 16 4 197.58 19.10 -8 16 4 236.58 23.40 16 -8 4 212.18 19.40 -8 16 -4 222.98 20.10 -8 -8 -4 249.78 23.40 -16 9 -4 122.89 20.80 9 7 -4 113.99 18.90 9 -16 4 114.49 20.00 -16 9 -4 121.99 19.50 9 -16 4 144.99 17.20 7 -16 -4 137.69 12.90 -16 7 4 124.19 17.10 9 7 -4 106.59 18.70 7 9 4 111.69 21.80 -7 -9 -4 135.79 11.40 -9 -7 4 158.58 19.00 -9 16 -4 127.99 17.40 -7 -9 -4 166.68 19.30 -9 -7 4 170.28 15.20 -9 16 -4 126.39 19.60 -7 -9 -4 181.98 21.20 -7 16 4 144.39 21.50 -9 -7 4 151.78 17.40 16 -7 -4 134.39 17.70 -7 16 4 82.69 17.60 16 -9 4 125.59 21.50 10 6 -4 4.60 12.00 10 -16 4 5.60 10.70 6 -16 -4 -16.80 11.30 -16 6 4 4.90 11.30 -16 10 -4 12.70 12.30 6 -16 -4 27.20 11.00 10 -16 4 4.20 10.60 10 6 -4 23.70 9.50 6 -16 -4 11.60 7.60 -16 10 -4 -5.90 13.30 6 10 4 16.70 11.40 -10 16 -4 -4.80 10.00 -6 -10 -4 23.50 12.90 16 -10 4 10.00 11.70 16 -10 4 -1.90 8.30 -6 -10 -4 8.20 6.50 -10 -6 4 20.40 10.20 -10 16 -4 9.90 12.60 16 -6 -4 1.40 11.60 -6 16 4 4.00 15.00 -6 16 4 10.70 9.70 -10 -6 4 9.90 10.20 -16 11 -4 75.79 16.00 5 -16 -4 64.59 11.20 11 5 -4 61.09 14.90 -16 5 4 44.10 13.90 -16 5 4 73.39 16.20 11 -16 4 67.09 15.10 11 -16 4 63.59 16.60 11 5 -4 90.39 15.70 5 11 4 97.89 21.10 -16 11 -4 53.09 15.70 -11 -5 4 97.29 16.60 -5 -11 -4 53.39 9.70 16 -5 -4 56.29 13.60 -5 -11 -4 104.49 18.70 -5 16 4 50.49 12.00 -5 16 4 74.89 17.00 16 -11 4 93.79 19.80 -5 -11 -4 102.49 21.60 16 -5 -4 53.69 9.60 -11 16 -4 59.89 14.00 -11 -5 4 85.99 14.30 16 -11 4 53.09 12.00 -11 16 -4 52.19 11.20 -11 -5 4 85.59 15.00 -16 4 4 53.89 12.80 12 4 -4 30.80 12.90 -16 4 4 43.40 13.00 12 -16 4 47.80 13.10 4 12 4 24.90 13.40 12 4 -4 50.49 11.40 4 -16 -4 66.99 10.70 -16 12 -4 51.09 14.80 12 -16 4 34.00 11.60 16 -12 4 42.30 13.70 -4 16 4 30.60 10.70 16 -12 4 57.09 14.60 -12 16 -4 51.89 14.40 -4 -12 -4 54.79 10.00 -12 -4 4 78.09 13.30 -12 -4 4 65.29 16.40 16 -4 -4 57.09 12.40 -12 16 -4 39.30 10.10 -12 -4 4 69.49 15.00 16 -4 -4 50.49 14.20 -4 16 4 46.10 16.30 -16 13 -4 17.60 13.30 13 -16 4 6.60 10.10 13 3 -4 18.00 9.50 -16 3 4 22.20 11.70 3 13 4 17.60 12.00 13 3 -4 -2.10 12.60 -16 3 4 14.40 11.60 13 -16 4 9.90 11.30 3 -16 -4 17.50 7.60 -13 -3 4 4.30 9.30 -3 16 4 2.50 10.60 -13 16 -4 10.80 13.50 -13 -3 4 10.20 10.70 16 -13 4 -8.20 9.60 16 -3 -4 13.80 13.70 -3 -13 -4 11.90 7.30 -13 16 -4 20.70 9.10 -13 -3 4 20.00 11.50 16 -13 4 10.20 11.50 -3 16 4 18.40 14.60 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16 -4 18.50 14.10 0 17 -4 7.10 14.20 0 -17 4 -3.50 13.80 -17 0 -4 14.60 13.60 0 17 -4 -3.30 14.40 17 -17 -4 4.00 11.40 17 0 4 11.90 10.40 0 17 -4 -4.70 9.50 -17 17 4 -0.50 16.20 -17 17 4 12.70 8.80 0 -17 4 7.70 12.00 1 -17 4 28.70 13.60 -17 1 -4 19.40 14.60 -17 16 4 14.00 17.00 16 -17 -4 15.10 11.20 16 -17 -4 14.90 10.20 1 -17 4 23.30 14.70 16 -17 -4 -0.70 10.50 -17 16 4 -2.00 9.20 16 1 4 13.60 12.00 1 16 -4 29.60 14.70 -1 17 -4 -19.70 14.70 -1 -16 4 20.10 14.00 -16 17 4 20.40 8.50 17 -16 -4 -11.70 11.10 -1 17 -4 17.20 14.40 -16 -1 -4 5.70 13.50 -1 -16 4 31.40 11.80 -16 17 4 20.70 16.80 17 -16 -4 10.20 11.10 17 -1 4 9.60 10.80 15 -17 -4 27.50 12.30 2 15 -4 17.10 10.20 2 15 -4 30.10 14.40 2 -17 4 34.30 14.50 2 15 -4 5.30 12.80 -17 15 4 36.40 16.50 15 -17 -4 10.30 10.60 15 -17 -4 25.80 10.90 2 -17 4 13.20 14.20 -17 2 -4 30.40 15.30 -2 -15 4 13.70 13.80 17 -15 -4 28.70 12.10 -15 -2 -4 18.20 13.70 -2 -15 4 37.00 15.30 -15 17 4 21.50 15.70 -2 17 -4 -2.80 14.60 17 -2 4 30.20 10.70 -2 17 -4 35.40 15.00 -15 17 4 29.90 9.90 3 14 -4 10.70 14.70 3 14 -4 4.70 9.70 -17 3 -4 29.70 12.30 3 -17 4 11.50 14.60 3 -17 4 31.80 12.00 14 -17 -4 0.30 11.90 -17 14 4 20.20 13.80 14 -17 -4 15.60 11.00 14 -17 -4 8.60 8.80 17 -14 -4 -12.50 10.30 17 -3 4 11.40 9.50 17 -14 -4 -10.00 9.40 -3 17 -4 3.10 12.00 -3 -14 4 32.90 14.50 -14 17 4 3.70 16.20 -14 -3 -4 16.00 14.60 17 -14 -4 18.60 10.70 -3 17 -4 -16.60 14.30 -14 17 4 4.80 8.60 4 13 -4 148.59 20.60 4 -17 4 141.19 21.30 -17 13 4 161.98 20.30 4 -17 4 195.88 20.20 -17 4 -4 173.68 20.30 13 -17 -4 156.48 15.40 4 13 -4 99.59 18.70 13 -17 -4 147.79 18.90 -17 4 -4 167.68 19.30 -4 17 -4 120.69 19.70 -13 17 4 165.78 17.80 -4 17 -4 142.29 20.40 -13 -4 -4 160.48 18.80 17 -13 -4 170.78 22.50 17 -13 -4 170.68 17.00 17 -4 4 177.78 14.90 -4 -13 4 164.98 20.10 -4 -13 4 140.19 22.50 -17 5 -4 352.06 24.60 12 -17 -4 348.97 26.40 12 -17 -4 339.17 19.80 12 5 4 292.47 28.30 5 12 -4 294.27 24.40 5 -17 4 367.36 24.60 5 12 -4 285.17 23.90 5 -17 4 311.97 27.10 -17 5 -4 342.57 26.70 -5 17 -4 279.67 24.90 17 -5 4 319.07 18.90 -12 -5 -4 338.77 24.70 17 -12 -4 278.17 20.90 -12 -5 -4 354.46 26.90 -5 17 -4 325.57 24.70 17 -12 -4 375.86 23.40 -12 17 4 335.37 26.40 17 -12 -4 372.96 26.50 -5 -12 4 379.36 25.50 -5 -12 4 399.16 24.20 -12 17 4 360.76 23.00 11 -17 -4 76.59 17.10 6 11 -4 20.00 13.00 6 11 -4 29.00 11.40 11 -17 -4 44.30 10.00 -17 11 4 47.20 13.30 11 6 4 79.29 19.90 -17 6 -4 51.49 13.80 11 -17 -4 15.10 12.00 -17 6 -4 45.80 15.80 6 -17 4 55.29 14.20 6 -17 4 49.30 13.40 -11 17 4 29.80 10.70 17 -6 4 44.40 13.90 -11 -6 -4 28.60 12.60 -6 -11 4 40.50 12.40 17 -11 -4 55.99 13.60 -11 -6 -4 51.09 15.00 17 -6 4 36.50 8.60 -11 17 4 44.80 16.50 -6 -11 4 36.20 11.80 -6 17 -4 20.30 10.90 17 -11 -4 12.20 11.20 -6 17 -4 34.10 13.50 17 -6 4 24.20 12.30 10 -17 -4 357.06 26.50 10 -17 -4 336.47 19.10 7 10 -4 315.87 23.00 -17 7 -4 333.07 24.50 7 -17 4 366.86 23.70 -17 7 -4 317.07 24.80 -17 10 4 338.57 23.40 7 -17 4 304.57 25.10 10 7 4 323.87 27.90 10 -17 -4 323.97 24.10 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89.39 19.90 -18 3 -4 101.29 21.10 3 15 -4 90.19 19.60 3 -18 4 99.89 19.50 15 -18 -4 89.29 14.40 15 -18 -4 79.69 18.00 3 15 -4 75.49 17.70 3 -18 4 101.39 20.60 3 15 -4 83.99 18.70 -18 15 4 99.19 22.60 15 3 4 81.69 14.30 -3 -15 4 122.29 19.60 18 -3 4 110.19 15.40 -15 18 4 61.09 12.50 18 -15 -4 55.49 13.80 -15 18 4 62.79 17.70 -3 18 -4 93.09 19.40 -15 -3 -4 112.39 20.40 18 -15 -4 112.89 17.10 14 4 4 75.39 13.90 -18 4 -4 76.79 18.30 14 -18 -4 49.40 14.60 4 14 -4 67.29 15.70 4 -18 4 102.99 19.10 14 -18 -4 70.59 14.10 -18 14 4 90.59 20.10 4 14 -4 51.29 13.90 -18 4 -4 104.79 18.80 4 -18 4 67.59 14.40 14 -18 -4 108.39 18.00 4 14 -4 69.79 15.90 -4 18 -4 62.99 15.20 18 -14 -4 95.99 17.00 18 -14 -4 53.19 12.50 -4 -14 4 52.29 14.20 18 -14 -4 53.69 13.60 -14 18 4 57.29 17.20 -14 -4 -4 98.09 19.80 -14 18 4 77.39 16.20 18 -4 4 63.09 11.90 -4 -14 4 83.39 18.30 5 13 -4 -1.30 10.30 -18 5 -4 9.50 15.20 13 -18 -4 23.70 13.80 -18 13 4 28.60 15.00 5 -18 4 25.10 12.30 13 -18 -4 9.30 8.80 -18 5 -4 7.90 12.20 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49.80 14.10 -5 18 4 29.70 18.00 -13 -5 4 21.00 10.80 18 -5 -4 34.10 14.90 -13 18 -4 15.20 13.10 -5 -13 -4 36.20 8.50 18 -5 -4 17.40 9.70 -5 18 4 28.40 11.60 14 4 -4 -1.60 11.90 4 -18 -4 7.20 7.40 14 -18 4 8.90 20.70 -18 4 4 12.80 12.70 -18 4 4 -10.40 16.20 -18 14 -4 -0.80 13.40 4 -18 -4 -7.00 13.10 -14 18 -4 14.50 13.30 18 -4 -4 4.90 13.20 -4 18 4 3.00 16.70 -14 -4 4 30.80 13.00 -14 -4 4 19.80 9.80 18 -14 4 14.10 12.40 -4 -14 -4 14.90 7.90 -18 15 -4 50.19 16.40 -18 3 4 82.59 17.30 3 -18 -4 57.79 16.30 3 -18 -4 55.49 11.00 15 3 -4 28.00 12.70 15 -18 4 50.79 13.50 15 3 -4 43.50 13.90 -3 18 4 13.30 20.30 18 -15 4 47.70 13.60 -15 18 -4 43.80 15.40 -3 -15 -4 56.69 10.20 -15 -3 4 60.39 22.00 18 -3 -4 47.50 15.10 -15 -3 4 27.00 11.80 -3 18 4 23.90 12.40 -18 2 4 57.09 14.40 -18 16 -4 27.80 14.00 16 2 -4 19.20 13.50 16 -18 4 46.30 13.90 2 -18 -4 34.00 8.60 -2 -16 -4 40.10 8.90 -2 18 4 32.10 19.90 18 -2 -4 27.30 15.00 -16 18 -4 37.60 15.10 18 -16 4 35.20 12.50 -16 -2 4 33.80 12.80 -18 1 4 41.10 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63.19 19.70 16 4 4 45.10 11.70 16 -20 -4 39.10 13.30 -4 20 -4 60.89 17.10 20 -16 -4 35.80 13.90 -4 -16 4 53.69 16.60 -16 -4 -4 40.30 15.40 20 -4 4 68.69 19.90 -16 20 4 31.50 18.40 -4 20 -4 56.49 16.00 5 15 -4 42.20 15.80 -20 5 -4 28.10 15.00 15 -20 -4 38.30 10.20 5 -20 4 20.50 15.00 15 5 4 27.10 11.40 15 -20 -4 31.60 15.90 -20 15 4 28.50 16.80 15 -20 -4 7.80 13.60 20 -15 -4 2.20 12.80 -15 20 4 24.40 10.70 20 -5 4 39.50 11.70 -5 -15 4 31.70 14.80 -15 -5 -4 43.00 14.80 -5 20 -4 24.50 14.40 -15 20 4 20.20 18.20 6 14 -4 9.10 11.30 14 6 4 11.00 10.80 6 -20 4 29.20 15.80 -20 6 -4 5.20 16.30 -20 6 -4 42.50 14.20 14 -20 -4 9.80 9.40 6 14 -4 -2.20 12.60 -20 14 4 28.60 17.50 -6 -14 4 21.40 14.00 -6 -14 4 24.60 11.70 20 -6 4 12.30 10.20 -14 -6 -4 22.20 14.70 -6 20 -4 7.60 13.20 -14 20 4 -9.00 17.70 -6 -14 4 48.80 14.10 20 -14 -4 1.10 13.30 13 7 4 98.19 14.70 -20 7 -4 110.79 19.20 -20 13 4 142.39 24.90 13 -20 -4 92.39 24.20 7 13 -4 86.29 19.20 -20 7 -4 122.29 21.20 7 -20 4 126.59 20.60 13 -20 -4 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46.90 14.30 15 6 -4 64.49 15.00 6 -21 -4 69.99 10.70 6 15 4 80.49 14.20 -21 6 4 42.70 16.30 -21 15 -4 74.59 17.90 21 -15 4 82.49 16.30 -15 -6 4 21.20 16.80 21 -6 -4 75.29 16.00 -15 21 -4 49.00 15.20 -6 21 4 46.30 23.90 0 0 5 -16.60 9.20 0 0 -5 -9.90 10.00 1 0 5 66.49 14.80 0 1 -5 108.39 14.00 -1 0 -5 80.09 14.60 0 -1 5 80.19 15.20 -1 1 5 74.99 15.20 1 -1 -5 67.09 14.40 1 0 5 93.49 8.00 0 1 5 210.48 10.10 1 -1 5 211.28 11.30 1 -1 5 232.78 13.20 0 1 5 208.08 16.70 1 -1 5 212.68 10.60 0 1 5 255.57 11.10 0 -1 -5 208.88 17.70 -1 0 5 238.78 17.30 -1 1 -5 227.08 17.60 1 0 -5 235.48 18.40 -2 0 -5 195.88 13.30 2 0 5 155.08 15.80 2 0 5 191.98 11.70 0 2 -5 161.58 15.60 -2 2 5 173.98 16.80 -2 0 -5 166.38 16.20 2 0 5 218.08 14.50 2 -2 -5 157.18 17.00 1 -2 5 0.70 4.40 1 -2 5 6.50 4.60 1 1 -5 -13.20 10.20 -2 1 5 1.80 9.90 1 1 5 1.90 4.30 1 1 5 -3.60 10.30 1 -2 5 4.50 5.30 1 -2 -5 -5.30 9.30 -2 1 -5 2.70 9.80 2 -1 5 2.50 4.70 -1 2 -5 0.30 9.00 -1 -1 -5 -5.40 9.20 -1 -1 5 -14.70 10.20 2 -1 5 8.70 6.40 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302.37 19.50 6 -8 -7 296.17 21.60 6 2 7 298.97 22.10 2 6 -7 361.56 25.00 -2 -6 7 318.77 22.60 -6 -2 -7 295.77 19.60 -6 8 7 298.67 21.80 -2 8 -7 342.77 24.30 8 -6 -7 323.77 22.60 3 5 -7 22.70 14.50 -8 5 7 27.80 12.30 -8 3 -7 8.30 9.00 5 3 7 8.20 10.40 5 -8 -7 8.30 10.20 8 -5 -7 -1.50 11.60 -5 -3 -7 13.50 9.90 -3 8 -7 6.90 12.70 -3 8 -7 26.60 21.60 -3 -5 7 8.60 11.70 -5 8 7 22.90 12.40 -8 4 -7 84.19 18.80 -8 4 7 128.49 17.50 4 4 7 103.79 16.60 -8 4 -7 96.09 14.60 4 4 -7 143.19 18.20 4 -8 -7 83.19 15.40 -4 -4 7 99.09 17.10 -4 8 7 109.09 15.50 -4 -4 -7 103.49 13.70 -4 8 -7 126.99 22.60 8 -4 -7 99.09 16.30 -4 8 -7 82.49 16.50 -8 3 7 150.18 16.30 3 -8 -7 113.69 15.60 -8 5 -7 115.99 18.00 3 5 7 129.59 17.40 5 3 -7 164.88 20.70 -5 8 -7 149.99 18.50 -3 8 7 135.39 17.60 -5 -3 7 124.69 15.90 -5 8 -7 119.79 19.80 8 -3 -7 123.69 18.30 -3 -5 -7 115.89 14.40 2 -8 -7 19.10 9.90 2 6 7 14.50 11.80 6 2 -7 37.40 14.70 -8 6 -7 16.50 14.00 -8 2 7 35.30 12.20 -2 -6 -7 18.30 9.60 -2 8 7 24.60 11.30 -6 8 -7 14.10 13.30 8 -2 -7 36.50 14.10 -6 8 -7 33.60 12.50 -6 -2 7 24.20 11.30 7 1 -7 142.09 20.20 -8 1 7 170.38 18.20 1 -8 -7 139.59 15.70 -8 7 -7 146.69 21.20 -8 7 -7 153.08 16.70 -7 -1 7 149.69 16.50 -7 8 -7 141.39 18.80 8 -1 -7 145.79 19.70 -1 8 7 165.28 18.10 -7 8 -7 139.39 17.80 -1 -7 -7 157.48 15.50 0 8 7 99.09 16.70 -8 8 -7 73.39 16.20 -8 0 7 110.29 15.40 8 0 -7 99.99 19.00 -8 8 -7 102.29 16.90 0 -8 -7 94.19 13.10 -9 0 -7 169.98 14.60 9 -9 -7 170.28 18.80 -9 9 7 197.08 19.10 0 9 -7 243.88 23.70 8 -9 -7 186.48 18.30 -9 1 -7 158.68 15.20 8 1 7 197.48 18.90 -9 8 7 199.88 18.70 1 8 -7 250.37 22.90 -1 -8 7 185.18 19.40 9 -1 7 162.88 19.00 -8 -1 -7 176.18 15.60 9 -8 -7 184.28 18.40 7 2 7 11.30 11.00 -9 7 7 27.70 11.90 2 7 -7 29.50 15.10 -9 2 -7 19.00 9.20 7 -9 -7 13.70 10.40 9 -7 -7 18.70 12.10 -2 9 -7 38.90 14.60 -2 -7 7 18.80 11.60 -7 -2 -7 27.90 9.50 -7 9 7 23.10 12.00 -2 9 -7 13.20 13.40 -9 3 -7 99.79 14.40 6 3 7 115.19 16.70 -9 6 7 157.38 17.90 6 -9 -7 116.29 16.40 3 6 -7 163.88 21.20 -6 9 7 132.69 18.00 -3 9 -7 106.59 17.60 -6 -3 -7 120.89 14.00 -3 -6 7 115.19 17.60 9 -6 -7 118.19 17.70 5 4 7 100.39 16.80 -9 4 -7 128.89 14.40 5 -9 -7 106.89 15.60 -9 5 7 133.49 15.70 -9 4 -7 111.89 20.00 4 5 -7 124.09 20.50 -5 -4 -7 120.69 14.20 -5 9 7 142.89 16.40 9 -5 -7 130.89 18.50 -4 9 -7 105.09 19.60 -4 -5 7 139.99 17.90 -9 4 7 35.20 12.10 -9 5 -7 25.60 10.90 5 4 -7 42.40 14.90 4 -9 -7 29.10 11.30 4 5 7 38.60 12.80 -9 5 -7 32.10 14.90 -5 9 -7 28.10 14.40 9 -4 -7 22.00 11.80 -4 -5 -7 26.70 9.80 -4 9 7 38.30 13.30 -5 9 -7 50.79 13.70 -5 -4 7 30.80 11.50 3 6 7 63.49 13.30 -9 6 -7 77.09 19.80 -9 3 7 114.19 17.30 6 3 -7 97.39 19.50 -9 6 -7 67.69 16.90 3 -9 -7 73.79 13.70 -3 9 7 90.39 16.10 -6 -3 7 72.49 14.30 -3 -6 -7 73.19 13.50 9 -3 -7 56.89 14.60 -6 9 -7 56.69 14.60 2 7 7 43.40 12.50 -9 7 -7 49.00 14.40 -9 2 7 85.89 16.50 -9 7 -7 70.19 14.10 7 2 -7 76.09 16.60 2 -9 -7 50.79 11.70 -7 -2 7 68.39 14.20 9 -2 -7 50.79 14.70 -7 9 -7 65.79 14.70 -2 9 7 74.49 16.80 -2 -7 -7 57.99 13.00 -7 9 -7 50.09 14.40 -9 8 -7 87.99 14.70 -9 1 7 96.99 15.00 -9 8 -7 61.69 16.10 1 -9 -7 59.19 12.40 8 1 -7 91.59 19.20 -8 -1 7 80.19 14.80 -1 -8 -7 76.09 13.40 -8 9 -7 111.99 16.60 9 -1 -7 80.19 16.30 -8 9 -7 50.39 14.40 -1 9 7 85.89 17.20 9 0 -7 479.85 28.80 0 9 7 435.26 25.90 -9 9 -7 460.05 25.80 -9 0 7 446.26 25.00 0 -9 -7 439.76 23.90 -9 9 -7 400.36 28.20 -10 10 7 98.29 15.90 10 -10 -7 89.29 16.10 -10 0 -7 116.29 21.90 -10 0 -7 61.19 12.30 -10 9 7 36.10 12.80 -10 1 -7 14.50 8.70 9 -10 -7 8.80 11.10 -10 1 -7 -17.10 15.80 1 9 -7 47.80 15.40 9 1 7 6.70 10.10 -9 -1 -7 19.30 8.20 10 -1 7 -1.50 10.70 -9 -1 -7 -31.10 19.00 -1 10 -7 43.40 17.70 10 -9 -7 5.20 11.80 -9 10 7 23.30 12.30 -1 -9 7 6.90 11.80 -10 2 -7 106.69 13.70 -10 8 7 131.59 17.50 2 8 -7 159.38 21.20 8 -10 -7 99.29 16.40 8 2 7 97.69 16.60 -10 2 -7 82.39 18.20 -8 -2 -7 108.89 13.40 -2 -8 7 104.09 17.60 -8 10 7 129.49 18.50 -2 10 -7 108.99 19.10 10 -8 -7 106.69 17.10 -10 7 7 98.59 16.70 7 -10 -7 70.39 14.80 -10 3 -7 85.79 12.40 7 3 7 77.89 15.70 3 7 -7 119.09 21.20 -10 3 -7 45.50 18.90 -7 -3 -7 72.59 12.70 10 -7 -7 56.89 13.80 -3 -7 7 58.79 13.00 -3 10 -7 56.89 14.40 -7 10 7 90.19 17.70 -10 4 -7 16.20 8.90 -10 4 -7 15.20 13.40 6 -10 -7 4.00 9.90 4 6 -7 18.30 14.20 6 4 7 7.00 11.40 -10 6 7 23.60 11.30 -4 10 -7 11.70 16.40 -6 -4 -7 8.10 8.90 -6 10 7 23.30 11.70 10 -6 -7 0.90 11.30 -4 -6 7 9.20 11.80 -4 10 -7 12.00 13.80 5 5 7 24.50 12.20 5 5 -7 32.50 14.70 5 -10 -7 24.50 10.90 -10 5 -7 21.60 10.80 -10 5 -7 28.40 13.60 -10 5 7 39.50 12.10 -5 10 -7 28.60 14.00 -5 -5 -7 20.00 8.70 -5 -5 7 27.40 11.90 -5 10 7 41.10 13.30 -5 10 -7 50.69 18.70 10 -5 -7 28.50 13.30 -10 6 -7 74.49 15.90 4 6 7 74.99 17.00 6 4 -7 96.79 17.30 -10 4 7 104.19 14.80 4 -10 -7 71.69 12.70 -10 6 -7 64.49 16.40 -4 -6 -7 75.89 13.10 -6 10 -7 110.59 18.40 -6 -4 7 84.39 14.70 10 -4 -7 85.29 15.80 -6 10 -7 63.69 15.10 -4 10 7 94.69 16.40 7 3 -7 41.20 14.30 3 -10 -7 50.39 11.30 -10 3 7 84.29 16.80 -10 7 -7 37.10 15.30 3 7 7 44.90 11.90 -10 7 -7 31.60 12.90 -7 -3 7 34.60 11.90 10 -3 -7 38.50 13.20 -3 -7 -7 33.20 9.30 -3 10 7 47.60 12.50 -7 10 -7 39.40 13.50 -10 8 -7 299.87 23.50 2 -10 -7 296.47 19.00 8 2 -7 336.47 24.50 2 8 7 286.07 23.00 -10 2 7 324.37 21.40 -10 8 -7 333.67 20.50 -2 10 7 323.77 22.30 -2 -8 -7 306.77 19.20 -8 -2 7 305.27 20.80 10 -2 -7 317.07 22.80 -8 10 -7 262.87 22.70 -8 10 -7 309.67 22.00 9 1 -7 225.68 20.40 -10 9 -7 195.98 19.00 1 -10 -7 227.28 17.60 1 9 7 177.28 22.90 -10 9 -7 194.48 22.40 -10 1 7 221.18 18.10 -9 10 -7 208.58 19.30 -9 10 -7 199.38 22.20 10 -1 -7 237.88 20.80 -1 10 7 235.68 19.90 -9 -1 7 234.98 18.50 -1 -9 -7 220.58 16.90 -10 10 -7 53.69 12.90 -10 0 7 76.19 16.20 -10 10 -7 41.40 15.90 0 -10 -7 61.09 12.80 10 0 -7 37.90 13.40 0 10 7 42.50 12.10 -11 2 -7 42.70 17.00 -11 2 -7 55.49 12.10 9 2 7 45.90 12.40 9 -11 -7 42.00 12.40 -11 9 7 88.99 17.40 11 -9 -7 60.99 14.50 -2 -9 7 73.69 17.10 -9 -2 -7 47.50 9.90 -2 11 -7 41.30 14.10 -9 11 7 79.79 18.00 3 8 -7 30.50 14.50 8 3 7 3.60 10.20 -11 3 -7 4.40 8.60 8 -11 -7 14.20 10.80 -11 8 7 24.10 12.40 11 -8 -7 6.60 11.50 -3 11 -7 -2.00 13.40 -8 11 7 20.60 13.30 -3 11 -7 32.40 15.50 -3 -8 7 5.00 11.80 -8 -3 -7 7.30 8.20 -11 4 -7 20.00 9.90 -11 7 7 32.60 11.90 4 7 -7 53.49 15.60 7 4 7 17.70 11.80 -11 4 -7 15.30 14.50 7 -11 -7 11.20 11.00 -11 4 -7 23.80 13.90 -4 -7 7 8.00 11.10 11 -7 -7 25.50 12.90 -4 11 -7 5.90 13.00 -7 11 7 23.70 12.20 -7 -4 -7 14.70 8.20 -11 5 -7 -9.10 13.80 6 5 7 21.60 11.40 -11 5 -7 10.10 8.30 -11 6 7 19.20 11.60 5 6 -7 40.90 14.60 6 -11 -7 9.20 9.40 -6 -5 -7 10.20 8.00 -5 -6 7 9.10 12.00 11 -6 -7 -2.00 11.70 -6 11 7 19.20 12.90 -5 11 -7 13.20 14.20 5 6 7 16.50 11.40 -11 6 -7 33.30 10.20 -11 6 -7 26.30 14.90 -11 5 7 43.70 12.40 5 -11 -7 29.20 10.90 6 5 -7 41.90 15.10 -6 -5 7 30.10 12.40 -5 11 7 22.80 12.60 -6 11 -7 41.50 14.70 11 -5 -7 33.10 13.10 -6 11 -7 28.10 14.00 -5 -6 -7 21.50 9.30 7 4 -7 153.78 20.50 -11 7 -7 104.49 18.20 4 7 7 121.59 17.00 4 -11 -7 128.89 15.10 -11 4 7 149.09 17.90 -7 -4 7 142.79 17.50 -4 11 7 118.99 17.70 -4 -7 -7 118.39 13.90 -7 11 -7 107.39 18.10 11 -4 -7 126.09 19.10 -11 3 7 111.19 15.20 3 -11 -7 99.89 14.30 8 3 -7 141.19 19.60 -11 8 -7 110.29 16.60 -11 8 -7 95.09 20.10 3 8 7 116.69 17.10 -3 -8 -7 121.79 14.10 -3 11 7 114.49 18.10 -8 11 -7 90.49 18.10 11 -3 -7 113.59 18.80 -8 11 -7 101.79 18.30 -8 -3 7 108.29 15.40 2 -11 -7 60.09 13.50 -11 9 -7 9.40 13.50 2 9 7 34.40 20.60 -11 2 7 39.00 11.70 -9 11 -7 49.30 13.40 -2 11 7 36.10 13.50 -9 11 -7 31.10 14.60 -2 -9 -7 23.20 9.40 -9 -2 7 30.10 11.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 7025 _shelx_SHELXL_version_number '2016/6' _olex2_submission_special_instructions 'No special instructions were received' loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.59(3) 2 0.41(3)