############################################################################## # # # This CIF contains the data in a paper accepted for publication in # # Acta Crystallographica Section C. It conforms to the requirements of # # Notes for Authors for Acta Crystallographica Section C, and has been # # peer reviewed under the auspices of the IUCr Commission on Journals. # # # # Full details of the Crystallographic Information File format # # are given in the paper "The Crystallographic Information File (CIF): # # a New Standard Archive File for Crystallography" by S. R. Hall, F. H. # # Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # # # The current version of the core CIF dictionary is obtainable from # # ftp://ftp.iucr.org/pub/cif_core.dic. # # # # Software is freely available for graphical display of the structure(s) # # in this CIF. For information consult the CIF software page # # http://www.iucr.org/resources/cif/software. # # # # This file may be used for bona fide research purposes within the # # scientific community so long as proper attribution is given to the journal # # article from which it was obtained. # # # ############################################################################## data_I _audit_creation_method ; Olex2 1.3 (compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003) ; _chemical_name_systematic ; Sodium-serinol hexatungstoanitimonate ; _chemical_name_common ? _chemical_formula_moiety 'C6 H56.001 N2 Na5 O22 7+, O24 Sb W6 7-' _chemical_formula_sum 'C6 H56 N2 Na5 O46 Sb W6' _chemical_formula_iupac '[Na5 (H2 O)18 (C3 H10 N1 O2)2] [Sb W6 O24]' _chemical_formula_weight 2232.32 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'C 1 2/c 1' _space_group_name_Hall '-C 2yc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 21.9761(14) _cell_length_b 13.9179(9) _cell_length_c 16.2090(10) _cell_angle_alpha 90 _cell_angle_beta 111.189(2) _cell_angle_gamma 90 _cell_volume 4622.5(5) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9051 _cell_measurement_theta_min 2.43 _cell_measurement_theta_max 33.17 _cell_measurement_temperature 200(2) _exptl_crystal_description block _exptl_crystal_colour 'clear colourless' _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.05 _exptl_crystal_density_diffrn 3.208 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 4096 _exptl_absorpt_coefficient_mu 15.614 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_absorpt_correction_T_min 0.5423 _exptl_absorpt_correction_T_max 0.7465 _diffrn_ambient_temperature 200.15 _diffrn_source ? _diffrn_source_power 0.03 _diffrn_source_voltage 50.0 _diffrn_source_current 0.6 _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 100214 _diffrn_reflns_av_R_equivalents 0.0295 _diffrn_reflns_av_unetI/netI 0.0140 _diffrn_reflns_theta_min 1.988 _diffrn_reflns_theta_max 33.203 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_limit_h_min -33 _diffrn_reflns_limit_h_max 33 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_limit_l_max 24 _diffrn_standards_number 0 _refine_special_details ; Olex2_refinement_description 1. Fixed U~iso~ At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All N(H,H,H) groups, All O(H,H) groups 2. Restrained distances O24---H24B = O24---H24A = O23---H23A = O23---H23B = O22---H22A = O22---H22B = O21---H21A = O21---H21B = O20---H20A = O20---H20B = O19---H19A = O19---H19B = O18---H18B = O18---H18A = O16---H16B = O16---H16A = O17---H17B = O17---H17A = O15---H15B = O15---H15A = O14---H14 = O13---H13 0.95 with \s of 0.03 Na1---H24A \\sim Na1---H24B with \s of 0.02 3. Others Sof(O24)=Sof(H24A)=Sof(H24B)=FVAR(1) Sof(O23)=Sof(H23A)=Sof(H23B)=FVAR(2) 4.a Free rotating group: O24(H24A,H24B) 4.b Rotating group: O23(H23A,H23B) 4.c Ternary CH refined with riding coordinates: C2(H2) 4.d Secondary CH2 refined with riding coordinates: C1(H1D,H1E), C3(H3A,H3B) 4.e Idealized Me refined as rotating group: N1(H1A,H1B,H1C) ; _reflns_number_total 8841 _reflns_number_gt 8213 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0156 _refine_ls_R_factor_gt 0.0131 _refine_ls_wR_factor_gt 0.0243 _refine_ls_wR_factor_ref 0.0246 _refine_ls_goodness_of_fit_ref 1.151 _refine_ls_restrained_S_all 1.155 _refine_ls_number_reflns 8841 _refine_ls_number_parameters 390 _refine_ls_number_restraints 23 _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0049P)^2^+8.8181P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.601 _refine_diff_density_min -0.689 _refine_ls_extinction_method ; SHELXL2018 (Sheldrick, 2015b) ; _refine_ls_extinction_coef 0.000087(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX3 (Bruker, 2015) ; _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_structure_solution ; SHELXT2018 (Sheldrick, 2015a) and shelXle (H\"ubschle et al., 2011) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) and DIAMOND (Brandenburg, 2006) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) and PLATON (Spek, 2020) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W W1 0.23646(2) 0.98310(2) 0.50967(2) 0.00915(2) Uani d 1 . . W W2 0.33638(2) 0.89214(2) 0.42377(2) 0.00926(2) Uani d 1 . . W W3 0.34950(2) 0.65895(2) 0.41500(2) 0.00910(2) Uani d 1 . . Sb Sb1 0.250000 0.750000 0.500000 0.00687(3) Uani d 1 . . O O1 0.19305(6) 0.63497(9) 0.46152(8) 0.0092(2) Uani d 1 . . O O2 0.32045(6) 0.65301(9) 0.53084(8) 0.0093(2) Uani d 1 . . O O3 0.26877(6) 0.76387(9) 0.38977(8) 0.0088(2) Uani d 1 . . O O4 0.29370(7) 1.06930(10) 0.56698(9) 0.0160(3) Uani d 1 . . O O5 0.16585(7) 1.05002(10) 0.45722(9) 0.0164(3) Uani d 1 . . O O6 0.21773(6) 0.93907(9) 0.61149(8) 0.0116(2) Uani d 1 . . O O7 0.39611(7) 0.97551(10) 0.48078(9) 0.0174(3) Uani d 1 . . O O8 0.25818(6) 0.96747(9) 0.40414(8) 0.0115(2) Uani d 1 . . O O9 0.33570(7) 0.89690(10) 0.31671(9) 0.0160(3) Uani d 1 . . O O10 0.39142(6) 0.77917(9) 0.46445(8) 0.0122(2) Uani d 1 . . O O11 0.34480(7) 0.67242(10) 0.30582(9) 0.0143(3) Uani d 1 . . O O12 0.41832(7) 0.58827(10) 0.46496(9) 0.0168(3) Uani d 1 . . Na Na1 0.500000 0.99629(9) 0.250000 0.0197(2) Uani d 1 A . Na Na2 0.500000 0.74736(9) 0.250000 0.0239(3) Uani d 1 A . Na Na3 0.500000 0.49315(9) 0.250000 0.0192(2) Uani d 1 A . Na Na4 0.41110(4) 0.34118(6) 0.32760(5) 0.01762(16) Uani d 1 . . O O13 0.33515(7) 0.21655(10) 0.26482(9) 0.0161(3) Uani d 1 . . H H13 0.3018(12) 0.232(2) 0.2144(16) 0.039(8) Uiso d 1 . . O O14 0.37746(8) 0.31336(12) 0.45147(10) 0.0228(3) Uani d 1 . . H H14 0.370(2) 0.366(2) 0.479(3) 0.086(14) Uiso d 1 . . O O15 0.31493(7) 0.43482(11) 0.27597(10) 0.0175(3) Uani d 1 . . H H15A 0.2958(12) 0.4493(19) 0.2199(14) 0.026(7) Uiso d 1 . . H H15B 0.3004(14) 0.4779(19) 0.3006(19) 0.041(9) Uiso d 1 . . O O16 0.49851(9) 0.23264(14) 0.37966(13) 0.0348(4) Uani d 1 . . H H16A 0.504(3) 0.179(3) 0.352(3) 0.13(2) Uiso d 1 . . H H16B 0.5299(14) 0.230(2) 0.4319(17) 0.051(10) Uiso d 1 . . O O17 0.42545(8) 0.35821(12) 0.19100(10) 0.0222(3) Uani d 1 . . H H17A 0.3901(13) 0.364(2) 0.1394(17) 0.044(9) Uiso d 1 . . H H17B 0.4492(15) 0.316(2) 0.175(2) 0.053(10) Uiso d 1 . . O O18 0.48239(7) 0.47272(12) 0.38301(10) 0.0198(3) Uani d 1 . . H H18A 0.5179(12) 0.455(2) 0.4319(15) 0.031(7) Uiso d 1 . . H H18B 0.4610(15) 0.513(2) 0.407(2) 0.053(10) Uiso d 1 . . O O19 0.57928(7) 0.61738(12) 0.29274(10) 0.0206(3) Uani d 1 . . H H19A 0.6093(13) 0.603(2) 0.3462(16) 0.043(9) Uiso d 1 . . H H19B 0.6047(14) 0.629(2) 0.262(2) 0.046(9) Uiso d 1 . . O O20 0.50365(10) 0.76172(17) 0.39592(13) 0.0405(5) Uani d 1 . . H H20A 0.471(2) 0.777(4) 0.416(4) 0.15(2) Uiso d 1 . . H H20B 0.5370(18) 0.742(3) 0.445(2) 0.103(17) Uiso d 1 . . O O21 0.58506(8) 0.87360(12) 0.28898(11) 0.0218(3) Uani d 1 . . H H21A 0.6135(13) 0.893(2) 0.3411(16) 0.042(9) Uiso d 1 . . H H21B 0.601(2) 0.878(3) 0.246(2) 0.094(15) Uiso d 1 . . O O22 0.58231(8) 1.11103(13) 0.30761(11) 0.0274(4) Uani d 1 . . H H22A 0.6160(12) 1.114(2) 0.3604(16) 0.036(8) Uiso d 1 . . H H22B 0.6034(15) 1.141(2) 0.277(2) 0.053(10) Uiso d 1 . . O O23 0.4836(2) 1.0261(7) 0.3845(3) 0.0214(16) Uani d 0.49(3) A 2 H H23A 0.520517 1.019846 0.429088 0.032 Uiso d 0.49(3) A 2 H H23B 0.458680 0.981153 0.392879 0.032 Uiso d 0.49(3) A 2 N N1 0.24448(8) 0.28660(12) 0.33045(11) 0.0151(3) Uani d 1 . . H H1A 0.209963 0.263685 0.284205 0.023 Uiso calc 1 . . H H1B 0.268602 0.326406 0.309808 0.023 Uiso calc 1 . . H H1C 0.229658 0.319666 0.367847 0.023 Uiso calc 1 . . C C1 0.31201(10) 0.15213(14) 0.31546(13) 0.0170(4) Uani d 1 . . H H1D 0.348055 0.108998 0.349921 0.020 Uiso calc 1 . . H H1E 0.276807 0.111847 0.274682 0.020 Uiso calc 1 . . C C2 0.28596(10) 0.20445(14) 0.37896(13) 0.0151(3) Uani d 1 . . H H2 0.256858 0.158600 0.394736 0.018 Uiso calc 1 . . C C3 0.33729(10) 0.23864(15) 0.46485(13) 0.0192(4) Uani d 1 . . H H3A 0.315385 0.262462 0.504576 0.023 Uiso calc 1 . . H H3B 0.365219 0.183629 0.494426 0.023 Uiso calc 1 . . O O24 0.4901(3) 0.9763(14) 0.3884(4) 0.041(3) Uani d 0.51(3) A 1 H H24A 0.525636 0.986172 0.433912 0.061 Uiso d 0.51(3) A 1 H H24B 0.460889 1.011938 0.398180 0.061 Uiso d 0.51(3) A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 W1 0.01187(3) 0.00678(3) 0.00937(3) 0.00066(2) 0.00455(2) -0.00038(2) W2 0.00935(3) 0.00934(3) 0.00992(3) -0.00122(2) 0.00449(2) 0.00009(2) W3 0.00888(3) 0.01020(3) 0.00925(3) 0.00212(2) 0.00452(2) 0.00001(2) Sb1 0.00750(6) 0.00630(6) 0.00766(6) 0.00040(5) 0.00376(5) -0.00023(5) O1 0.0100(5) 0.0090(6) 0.0085(5) -0.0005(4) 0.0033(4) -0.0006(4) O2 0.0098(5) 0.0092(6) 0.0092(5) 0.0025(4) 0.0038(4) 0.0000(4) O3 0.0092(5) 0.0098(6) 0.0083(5) 0.0002(4) 0.0041(4) 0.0001(4) O4 0.0205(7) 0.0128(6) 0.0155(6) -0.0032(5) 0.0075(5) -0.0029(5) O5 0.0191(7) 0.0136(6) 0.0168(6) 0.0060(5) 0.0066(5) 0.0035(5) O6 0.0136(6) 0.0114(6) 0.0101(6) -0.0010(5) 0.0047(5) -0.0021(5) O7 0.0144(6) 0.0168(7) 0.0200(7) -0.0046(5) 0.0050(5) -0.0026(5) O8 0.0140(6) 0.0103(6) 0.0104(6) 0.0010(5) 0.0046(5) 0.0010(5) O9 0.0189(7) 0.0175(7) 0.0141(6) -0.0001(5) 0.0090(5) 0.0018(5) O10 0.0096(5) 0.0134(6) 0.0129(6) -0.0002(5) 0.0031(5) -0.0002(5) O11 0.0165(6) 0.0163(7) 0.0125(6) 0.0016(5) 0.0080(5) 0.0002(5) O12 0.0140(6) 0.0187(7) 0.0173(7) 0.0064(5) 0.0052(5) 0.0008(5) Na1 0.0167(5) 0.0227(6) 0.0192(6) 0.000 0.0059(5) 0.000 Na2 0.0221(6) 0.0230(6) 0.0256(6) 0.000 0.0073(5) 0.000 Na3 0.0205(6) 0.0199(6) 0.0193(6) 0.000 0.0095(5) 0.000 Na4 0.0149(4) 0.0206(4) 0.0174(4) -0.0004(3) 0.0060(3) 0.0009(3) O13 0.0179(7) 0.0170(7) 0.0126(6) 0.0008(5) 0.0045(5) -0.0001(5) O14 0.0220(7) 0.0267(8) 0.0204(7) -0.0071(6) 0.0086(6) -0.0050(6) O15 0.0201(7) 0.0148(7) 0.0157(7) 0.0036(5) 0.0043(6) -0.0012(5) O16 0.0290(9) 0.0278(10) 0.0314(10) 0.0090(7) -0.0085(7) -0.0045(8) O17 0.0177(7) 0.0324(9) 0.0142(7) -0.0026(6) 0.0031(6) -0.0011(6) O18 0.0187(7) 0.0248(8) 0.0148(7) 0.0074(6) 0.0047(6) -0.0018(6) O19 0.0177(7) 0.0266(8) 0.0182(7) 0.0008(6) 0.0075(6) 0.0056(6) O20 0.0266(9) 0.0643(14) 0.0300(10) 0.0032(9) 0.0094(8) 0.0026(10) O21 0.0191(7) 0.0265(8) 0.0214(8) -0.0021(6) 0.0091(6) 0.0001(6) O22 0.0201(8) 0.0370(10) 0.0200(8) -0.0105(7) 0.0010(6) 0.0034(7) O23 0.0177(17) 0.027(4) 0.0190(17) -0.0030(17) 0.0059(13) 0.0033(17) N1 0.0150(7) 0.0143(7) 0.0156(7) 0.0007(6) 0.0052(6) -0.0007(6) C1 0.0209(9) 0.0105(8) 0.0184(9) 0.0016(7) 0.0055(7) 0.0002(7) C2 0.0184(9) 0.0110(8) 0.0150(8) -0.0004(7) 0.0049(7) 0.0025(6) C3 0.0209(9) 0.0211(10) 0.0135(8) -0.0014(8) 0.0038(7) 0.0009(7) O24 0.023(2) 0.080(9) 0.022(2) -0.016(3) 0.0111(17) -0.017(3) _geom_special_details ; All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag W1 Sb1 . 3.2668(2) ? W1 O1 7_566 2.1899(12) ? W1 O2 7_566 2.2339(13) ? W1 O4 . 1.7435(14) ? W1 O5 . 1.7449(13) ? W1 O6 . 1.9391(13) ? W1 O8 . 1.9471(13) ? W2 Sb1 . 3.27720(15) ? W2 O1 7_566 2.2106(12) ? W2 O3 . 2.2599(12) ? W2 O7 . 1.7455(14) ? W2 O8 . 1.9387(13) ? W2 O9 . 1.7312(13) ? W2 O10 . 1.9477(13) ? W3 Sb1 . 3.23479(15) ? W3 O2 . 2.1925(12) ? W3 O3 . 2.2189(12) ? W3 O6 7_566 1.9416(13) ? W3 O10 . 1.9383(13) ? W3 O11 . 1.7452(13) ? W3 O12 . 1.7394(13) ? Sb1 O1 . 1.9885(12) ? Sb1 O1 7_566 1.9885(12) ? Sb1 O2 7_566 1.9773(12) ? Sb1 O2 . 1.9773(12) ? Sb1 O3 . 1.9830(12) ? Sb1 O3 7_566 1.9830(12) ? Na1 Na2 . 3.4647(18) ? Na1 O21 . 2.4404(18) ? Na1 O21 2_655 2.4405(18) ? Na1 O22 2_655 2.3394(18) ? Na1 O22 . 2.3394(18) ? Na1 O23 2_655 2.371(6) ? Na1 O23 . 2.371(6) ? Na1 O24 . 2.346(6) ? Na1 O24 2_655 2.346(6) ? Na2 Na3 . 3.5381(18) ? Na2 O19 . 2.4322(19) ? Na2 O19 2_655 2.4322(19) ? Na2 O20 . 2.346(2) ? Na2 O20 2_655 2.346(2) ? Na2 O21 2_655 2.4752(19) ? Na2 O21 . 2.4752(19) ? Na3 Na4 . 3.4130(11) ? Na3 Na4 2_655 3.4130(11) ? Na3 O17 2_655 2.4480(19) ? Na3 O17 . 2.4480(19) ? Na3 O18 . 2.3414(15) ? Na3 O18 2_655 2.3414(15) ? Na3 O19 . 2.3733(18) ? Na3 O19 2_655 2.3733(18) ? Na4 O13 . 2.3669(17) ? Na4 O14 . 2.4085(17) ? Na4 O15 . 2.3636(17) ? Na4 O16 . 2.3479(19) ? Na4 O17 . 2.3585(17) ? Na4 O18 . 2.3655(18) ? O13 H13 . 0.90(2) ? O13 C1 . 1.428(2) ? O14 H14 . 0.91(2) ? O14 C3 . 1.431(3) ? O15 H15A . 0.88(2) ? O15 H15B . 0.84(2) ? O16 H16A . 0.90(3) ? O16 H16B . 0.88(2) ? O17 H17A . 0.92(2) ? O17 H17B . 0.88(2) ? O18 H18A . 0.92(2) ? O18 H18B . 0.91(2) ? O19 H19A . 0.90(2) ? O19 H19B . 0.88(2) ? O20 H20A . 0.92(3) ? O20 H20B . 0.91(3) ? O21 H21A . 0.89(2) ? O21 H21B . 0.89(3) ? O22 H22A . 0.91(2) ? O22 H22B . 0.89(2) ? O23 H23A . 0.8740 ? O23 H23B . 0.8741 ? N1 H1A . 0.9100 ? N1 H1B . 0.9100 ? N1 H1C . 0.9100 ? N1 C2 . 1.496(2) ? C1 H1D . 0.9900 ? C1 H1E . 0.9900 ? C1 C2 . 1.531(3) ? C2 H2 . 1.0000 ? C2 C3 . 1.517(3) ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? O24 H24A . 0.8699 ? O24 H24B . 0.8705 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 W1 Sb1 7_566 . 36.42(3) ? O1 W1 O2 7_566 7_566 72.79(4) ? O2 W1 Sb1 7_566 . 36.37(3) ? O4 W1 Sb1 . . 130.41(5) ? O4 W1 O1 . 7_566 94.83(6) ? O4 W1 O2 . 7_566 163.66(6) ? O4 W1 O5 . . 103.63(7) ? O4 W1 O6 . . 95.64(6) ? O4 W1 O8 . . 100.73(6) ? O5 W1 Sb1 . . 125.95(5) ? O5 W1 O1 . 7_566 160.13(6) ? O5 W1 O2 . 7_566 90.26(6) ? O5 W1 O6 . . 99.11(6) ? O5 W1 O8 . . 95.10(6) ? O6 W1 Sb1 . . 77.17(4) ? O6 W1 O1 . 7_566 86.15(5) ? O6 W1 O2 . 7_566 73.36(5) ? O6 W1 O8 . . 155.13(5) ? O8 W1 Sb1 . . 77.96(4) ? O8 W1 O1 . 7_566 74.00(5) ? O8 W1 O2 . 7_566 86.33(5) ? O1 W2 Sb1 7_566 . 36.33(3) ? O1 W2 O3 7_566 . 72.77(4) ? O3 W2 Sb1 . . 36.45(3) ? O7 W2 Sb1 . . 128.97(5) ? O7 W2 O1 . 7_566 93.49(6) ? O7 W2 O3 . . 163.07(6) ? O7 W2 O8 . . 100.36(6) ? O7 W2 O10 . . 95.81(6) ? O8 W2 Sb1 . . 77.78(4) ? O8 W2 O1 . 7_566 73.67(5) ? O8 W2 O3 . . 85.49(5) ? O8 W2 O10 . . 153.80(5) ? O9 W2 Sb1 . . 127.21(5) ? O9 W2 O1 . 7_566 161.88(6) ? O9 W2 O3 . . 91.10(6) ? O9 W2 O7 . . 103.75(7) ? O9 W2 O8 . . 97.40(6) ? O9 W2 O10 . . 98.60(6) ? O10 W2 Sb1 . . 76.02(4) ? O10 W2 O1 . 7_566 84.96(5) ? O10 W2 O3 . . 73.62(5) ? O2 W3 Sb1 . . 36.78(3) ? O2 W3 O3 . . 73.84(4) ? O3 W3 Sb1 . . 37.06(3) ? O6 W3 Sb1 7_566 . 77.99(4) ? O6 W3 O2 7_566 . 74.28(5) ? O6 W3 O3 7_566 . 85.85(5) ? O10 W3 Sb1 . . 77.24(4) ? O10 W3 O2 . . 85.43(5) ? O10 W3 O3 . . 74.75(5) ? O10 W3 O6 . 7_566 155.22(5) ? O11 W3 Sb1 . . 126.05(4) ? O11 W3 O2 . . 160.69(5) ? O11 W3 O3 . . 89.55(5) ? O11 W3 O6 . 7_566 95.15(6) ? O11 W3 O10 . . 99.89(6) ? O12 W3 Sb1 . . 129.14(5) ? O12 W3 O2 . . 93.06(6) ? O12 W3 O3 . . 163.91(6) ? O12 W3 O6 . 7_566 99.77(6) ? O12 W3 O10 . . 95.30(6) ? O12 W3 O11 . . 104.81(6) ? W1 Sb1 W1 . 7_566 180.0 ? W1 Sb1 W2 7_566 7_566 59.590(4) ? W1 Sb1 W2 . . 59.590(4) ? W1 Sb1 W2 7_566 . 120.410(3) ? W1 Sb1 W2 . 7_566 120.411(3) ? W2 Sb1 W2 . 7_566 180.0 ? W3 Sb1 W1 7_566 7_566 119.789(2) ? W3 Sb1 W1 . 7_566 60.211(2) ? W3 Sb1 W1 7_566 . 60.211(2) ? W3 Sb1 W1 . . 119.789(2) ? W3 Sb1 W2 . . 60.200(4) ? W3 Sb1 W2 . 7_566 119.800(5) ? W3 Sb1 W2 7_566 7_566 60.200(4) ? W3 Sb1 W2 7_566 . 119.801(5) ? W3 Sb1 W3 . 7_566 180.0 ? O1 Sb1 W1 . . 139.17(4) ? O1 Sb1 W1 . 7_566 40.83(4) ? O1 Sb1 W1 7_566 . 40.83(4) ? O1 Sb1 W1 7_566 7_566 139.17(4) ? O1 Sb1 W2 . . 138.80(4) ? O1 Sb1 W2 7_566 7_566 138.80(3) ? O1 Sb1 W2 . 7_566 41.20(4) ? O1 Sb1 W2 7_566 . 41.19(3) ? O1 Sb1 W3 . 7_566 90.19(4) ? O1 Sb1 W3 7_566 7_566 89.82(4) ? O1 Sb1 W3 7_566 . 90.18(4) ? O1 Sb1 W3 . . 89.81(4) ? O1 Sb1 O1 . 7_566 180.0 ? O2 Sb1 W1 7_566 . 42.06(4) ? O2 Sb1 W1 7_566 7_566 137.94(4) ? O2 Sb1 W1 . . 137.94(4) ? O2 Sb1 W1 . 7_566 42.06(4) ? O2 Sb1 W2 . . 90.01(4) ? O2 Sb1 W2 7_566 . 89.99(4) ? O2 Sb1 W2 . 7_566 89.99(4) ? O2 Sb1 W2 7_566 7_566 90.01(4) ? O2 Sb1 W3 7_566 7_566 41.59(4) ? O2 Sb1 W3 . 7_566 138.40(4) ? O2 Sb1 W3 7_566 . 138.41(4) ? O2 Sb1 W3 . . 41.60(4) ? O2 Sb1 O1 7_566 . 97.11(5) ? O2 Sb1 O1 7_566 7_566 82.89(5) ? O2 Sb1 O1 . . 82.89(5) ? O2 Sb1 O1 . 7_566 97.11(5) ? O2 Sb1 O2 . 7_566 180.0 ? O2 Sb1 O3 7_566 7_566 84.00(5) ? O2 Sb1 O3 7_566 . 96.00(5) ? O2 Sb1 O3 . . 84.00(5) ? O2 Sb1 O3 . 7_566 96.00(5) ? O3 Sb1 W1 . 7_566 90.07(4) ? O3 Sb1 W1 . . 89.93(4) ? O3 Sb1 W1 7_566 7_566 89.93(4) ? O3 Sb1 W1 7_566 . 90.07(4) ? O3 Sb1 W2 7_566 . 137.39(4) ? O3 Sb1 W2 . . 42.61(4) ? O3 Sb1 W2 . 7_566 137.39(4) ? O3 Sb1 W2 7_566 7_566 42.61(4) ? O3 Sb1 W3 . . 42.41(3) ? O3 Sb1 W3 . 7_566 137.59(3) ? O3 Sb1 W3 7_566 7_566 42.41(3) ? O3 Sb1 W3 7_566 . 137.59(4) ? O3 Sb1 O1 7_566 . 83.80(5) ? O3 Sb1 O1 7_566 7_566 96.21(5) ? O3 Sb1 O1 . 7_566 83.79(5) ? O3 Sb1 O1 . . 96.20(5) ? O3 Sb1 O3 . 7_566 180.00(6) ? W1 O1 W2 7_566 7_566 95.28(5) ? Sb1 O1 W1 . 7_566 102.75(5) ? Sb1 O1 W2 . 7_566 102.47(5) ? W3 O2 W1 . 7_566 94.91(5) ? Sb1 O2 W1 . 7_566 101.57(5) ? Sb1 O2 W3 . . 101.63(5) ? W3 O3 W2 . . 93.64(5) ? Sb1 O3 W2 . . 100.94(5) ? Sb1 O3 W3 . . 100.53(5) ? W1 O6 W3 . 7_566 114.36(6) ? W2 O8 W1 . . 113.61(6) ? W3 O10 W2 . . 114.38(6) ? O21 Na1 Na2 . . 45.59(4) ? O21 Na1 Na2 2_655 . 45.59(4) ? O21 Na1 O21 . 2_655 91.19(9) ? O22 Na1 Na2 . . 133.05(5) ? O22 Na1 Na2 2_655 . 133.05(5) ? O22 Na1 O21 . . 87.99(6) ? O22 Na1 O21 2_655 2_655 87.99(6) ? O22 Na1 O21 . 2_655 172.04(6) ? O22 Na1 O21 2_655 . 172.04(6) ? O22 Na1 O22 2_655 . 93.90(10) ? O22 Na1 O23 2_655 . 84.0(2) ? O22 Na1 O23 . . 82.30(18) ? O22 Na1 O23 . 2_655 84.0(2) ? O22 Na1 O23 2_655 2_655 82.30(18) ? O22 Na1 O24 . 2_655 97.9(4) ? O22 Na1 O24 2_655 2_655 91.4(3) ? O22 Na1 O24 . . 91.4(3) ? O22 Na1 O24 2_655 . 97.9(4) ? O23 Na1 Na2 2_655 . 100.1(2) ? O23 Na1 Na2 . . 100.1(2) ? O23 Na1 O21 . . 103.9(2) ? O23 Na1 O21 2_655 . 90.22(18) ? O23 Na1 O23 2_655 . 159.8(5) ? O24 Na1 Na2 2_655 . 83.2(5) ? O24 Na1 Na2 . . 83.2(5) ? O24 Na1 O21 2_655 . 80.7(3) ? O24 Na1 O21 2_655 2_655 89.8(4) ? O24 Na1 O21 . 2_655 80.7(3) ? O24 Na1 O21 . . 89.8(4) ? O24 Na1 O23 2_655 2_655 17.2(3) ? O24 Na1 O23 . 2_655 175.4(5) ? O24 Na1 O24 . 2_655 166.4(9) ? Na1 Na2 Na3 . . 180.0 ? O19 Na2 Na1 . . 138.05(4) ? O19 Na2 Na1 2_655 . 138.06(4) ? O19 Na2 Na3 . . 41.95(4) ? O19 Na2 Na3 2_655 . 41.94(4) ? O19 Na2 O19 2_655 . 83.89(9) ? O19 Na2 O21 2_655 . 176.21(6) ? O19 Na2 O21 . . 93.33(5) ? O19 Na2 O21 . 2_655 176.21(6) ? O19 Na2 O21 2_655 2_655 93.33(5) ? O20 Na2 Na1 2_655 . 85.11(7) ? O20 Na2 Na1 . . 85.11(7) ? O20 Na2 Na3 2_655 . 94.89(7) ? O20 Na2 Na3 . . 94.89(7) ? O20 Na2 O19 . . 90.93(7) ? O20 Na2 O19 . 2_655 96.34(7) ? O20 Na2 O19 2_655 2_655 90.93(7) ? O20 Na2 O19 2_655 . 96.34(7) ? O20 Na2 O20 . 2_655 170.23(13) ? O20 Na2 O21 . . 86.25(7) ? O20 Na2 O21 2_655 2_655 86.26(7) ? O20 Na2 O21 2_655 . 86.81(7) ? O20 Na2 O21 . 2_655 86.81(7) ? O21 Na2 Na1 2_655 . 44.78(4) ? O21 Na2 Na1 . . 44.78(4) ? O21 Na2 Na3 2_655 . 135.22(4) ? O21 Na2 Na3 . . 135.22(4) ? O21 Na2 O21 2_655 . 89.56(9) ? Na4 Na3 Na2 2_655 . 128.30(2) ? Na4 Na3 Na2 . . 128.29(2) ? Na4 Na3 Na4 2_655 . 103.41(4) ? O17 Na3 Na2 . . 140.10(4) ? O17 Na3 Na2 2_655 . 140.10(4) ? O17 Na3 Na4 2_655 2_655 43.71(4) ? O17 Na3 Na4 . . 43.71(4) ? O17 Na3 Na4 2_655 . 76.82(5) ? O17 Na3 Na4 . 2_655 76.82(5) ? O17 Na3 O17 2_655 . 79.80(9) ? O18 Na3 Na2 2_655 . 96.98(5) ? O18 Na3 Na2 . . 96.98(5) ? O18 Na3 Na4 2_655 2_655 43.80(4) ? O18 Na3 Na4 2_655 . 124.83(5) ? O18 Na3 Na4 . 2_655 124.84(5) ? O18 Na3 Na4 . . 43.80(4) ? O18 Na3 O17 . . 87.51(6) ? O18 Na3 O17 2_655 2_655 87.51(6) ? O18 Na3 O17 2_655 . 81.79(6) ? O18 Na3 O17 . 2_655 81.79(6) ? O18 Na3 O18 . 2_655 166.05(10) ? O18 Na3 O19 2_655 . 90.52(6) ? O18 Na3 O19 2_655 2_655 99.67(6) ? O18 Na3 O19 . . 99.67(6) ? O18 Na3 O19 . 2_655 90.52(6) ? O19 Na3 Na2 . . 43.24(4) ? O19 Na3 Na2 2_655 . 43.24(4) ? O19 Na3 Na4 . . 143.27(4) ? O19 Na3 Na4 . 2_655 95.82(4) ? O19 Na3 Na4 2_655 2_655 143.27(4) ? O19 Na3 Na4 2_655 . 95.82(4) ? O19 Na3 O17 2_655 . 97.35(6) ? O19 Na3 O17 2_655 2_655 171.87(6) ? O19 Na3 O17 . . 171.87(6) ? O19 Na3 O17 . 2_655 97.35(6) ? O19 Na3 O19 2_655 . 86.47(9) ? O13 Na4 Na3 . . 134.78(5) ? O13 Na4 O14 . . 81.91(6) ? O14 Na4 Na3 . . 142.74(5) ? O15 Na4 Na3 . . 94.91(5) ? O15 Na4 O13 . . 81.40(6) ? O15 Na4 O14 . . 83.06(6) ? O15 Na4 O18 . . 95.30(6) ? O16 Na4 Na3 . . 91.62(6) ? O16 Na4 O13 . . 92.36(7) ? O16 Na4 O14 . . 93.13(7) ? O16 Na4 O15 . . 173.08(7) ? O16 Na4 O17 . . 91.86(7) ? O16 Na4 O18 . . 91.03(7) ? O17 Na4 Na3 . . 45.83(4) ? O17 Na4 O13 . . 89.02(6) ? O17 Na4 O14 . . 169.82(6) ? O17 Na4 O15 . . 91.04(6) ? O17 Na4 O18 . . 89.07(6) ? O18 Na4 Na3 . . 43.24(4) ? O18 Na4 O13 . . 176.16(6) ? O18 Na4 O14 . . 99.71(6) ? Na4 O13 H13 . . 115.7(19) ? C1 O13 Na4 . . 123.74(12) ? C1 O13 H13 . . 109.0(19) ? Na4 O14 H14 . . 117(3) ? C3 O14 Na4 . . 129.46(12) ? C3 O14 H14 . . 106(3) ? Na4 O15 H15A . . 121.8(17) ? Na4 O15 H15B . . 132(2) ? H15A O15 H15B . . 102(3) ? Na4 O16 H16A . . 126(4) ? Na4 O16 H16B . . 129(2) ? H16A O16 H16B . . 104(4) ? Na3 O17 H17A . . 121(2) ? Na3 O17 H17B . . 104(2) ? Na4 O17 Na3 . . 90.46(6) ? Na4 O17 H17A . . 121(2) ? Na4 O17 H17B . . 120(2) ? H17A O17 H17B . . 101(3) ? Na3 O18 Na4 . . 92.96(6) ? Na3 O18 H18A . . 117.0(17) ? Na3 O18 H18B . . 127(2) ? Na4 O18 H18A . . 111.3(17) ? Na4 O18 H18B . . 106(2) ? H18A O18 H18B . . 101(3) ? Na2 O19 H19A . . 130(2) ? Na2 O19 H19B . . 104(2) ? Na3 O19 Na2 . . 94.82(6) ? Na3 O19 H19A . . 109(2) ? Na3 O19 H19B . . 121(2) ? H19A O19 H19B . . 101(3) ? Na2 O20 H20A . . 130(4) ? Na2 O20 H20B . . 126(3) ? H20A O20 H20B . . 104(4) ? Na1 O21 Na2 . . 89.63(6) ? Na1 O21 H21A . . 104(2) ? Na1 O21 H21B . . 103(3) ? Na2 O21 H21A . . 132(2) ? Na2 O21 H21B . . 109(3) ? H21A O21 H21B . . 113(3) ? Na1 O22 H22A . . 131.2(19) ? Na1 O22 H22B . . 125(2) ? H22A O22 H22B . . 95(3) ? Na1 O23 H23A . . 109.8 ? Na1 O23 H23B . . 109.3 ? H23A O23 H23B . . 104.3 ? H1A N1 H1B . . 109.5 ? H1A N1 H1C . . 109.5 ? H1B N1 H1C . . 109.5 ? C2 N1 H1A . . 109.5 ? C2 N1 H1B . . 109.5 ? C2 N1 H1C . . 109.5 ? O13 C1 H1D . . 109.1 ? O13 C1 H1E . . 109.1 ? O13 C1 C2 . . 112.67(15) ? H1D C1 H1E . . 107.8 ? C2 C1 H1D . . 109.1 ? C2 C1 H1E . . 109.1 ? N1 C2 C1 . . 108.36(15) ? N1 C2 H2 . . 107.3 ? N1 C2 C3 . . 110.62(16) ? C1 C2 H2 . . 107.3 ? C3 C2 C1 . . 115.57(17) ? C3 C2 H2 . . 107.3 ? O14 C3 C2 . . 112.56(16) ? O14 C3 H3A . . 109.1 ? O14 C3 H3B . . 109.1 ? C2 C3 H3A . . 109.1 ? C2 C3 H3B . . 109.1 ? H3A C3 H3B . . 107.8 ? Na1 O24 H24A . . 115.3 ? Na1 O24 H24B . . 115.9 ? H24A O24 H24B . . 104.5 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Na4 O13 C1 C2 . . . . 51.8(2) ? Na4 O14 C3 C2 . . . . -31.5(2) ? O13 C1 C2 N1 . . . . 44.2(2) ? O13 C1 C2 C3 . . . . -80.5(2) ? N1 C2 C3 O14 . . . . -56.4(2) ? C1 C2 C3 O14 . . . . 67.2(2) ? _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min 0.304 _shelx_estimated_absorpt_T_max 0.509 _shelx_hkl_file ; -2 0 0 3235.68 77.59 -2 0 0 3095.79 77.79 -2 0 0 3669.53 78.19 -2 0 0 3705.13 78.09 2 0 0 3708.23 78.39 2 0 0 3393.86 78.69 2 0 0 3325.77 78.39 2 0 0 2960.00 77.69 2 0 0 3783.22 78.59 2 0 0 3577.14 78.89 -2 0 0 3352.86 78.29 2 0 0 3411.56 78.19 -2 0 0 3625.34 78.89 4 0 0 9.50 0.80 -4 0 0 10.80 0.70 4 0 0 10.00 0.80 -4 0 0 8.90 0.70 -4 0 0 9.10 0.80 4 0 0 9.00 0.80 -4 0 0 12.40 0.70 -4 0 0 12.70 0.70 4 0 0 9.60 0.80 4 0 0 9.50 0.70 4 0 0 11.30 1.00 -4 0 0 9.70 0.80 -4 0 0 11.70 0.90 4 0 0 9.60 0.60 6 0 0 557.24 13.70 6 0 0 555.84 13.30 -6 0 0 545.85 12.90 6 0 0 562.84 13.50 6 0 0 555.94 13.30 6 0 0 568.94 13.30 -6 0 0 562.54 13.20 -6 0 0 558.04 13.30 -6 0 0 545.15 13.60 6 0 0 557.74 13.00 8 0 0 912.61 21.20 -8 0 0 904.61 21.30 -8 0 0 897.71 21.60 8 0 0 883.61 21.50 8 0 0 914.31 20.90 -8 0 0 885.11 20.70 8 0 0 891.61 21.20 -8 0 0 891.11 21.30 8 0 0 904.81 21.80 8 0 0 902.91 21.20 10 0 0 2096.49 46.90 10 0 0 2021.30 47.20 10 0 0 2100.59 47.80 -10 0 0 2142.99 47.40 -10 0 0 2090.09 47.50 10 0 0 2092.69 48.10 10 0 0 2003.40 47.30 10 0 0 2054.09 47.30 -10 0 0 1999.80 46.60 -10 0 0 2042.40 47.90 12 0 0 4826.32 106.79 12 0 0 4595.94 107.69 -12 0 0 4857.11 106.49 -12 0 0 4760.02 106.89 -12 0 0 4487.65 107.49 12 0 0 4799.42 107.29 12 0 0 4563.74 106.19 12 0 0 4778.52 106.29 -12 0 0 4764.22 109.49 14 0 0 1.10 1.20 14 0 0 3.80 1.40 -14 0 0 0.60 1.50 -14 0 0 2.10 1.20 -14 0 0 0.70 1.30 14 0 0 1.10 1.40 14 0 0 0.80 0.60 -14 0 0 3.50 0.70 16 0 0 386.86 11.70 16 0 0 394.86 11.60 -16 0 0 388.86 11.50 16 0 0 405.26 12.30 -16 0 0 388.66 12.30 -16 0 0 385.56 11.60 16 0 0 390.86 10.90 18 0 0 65.59 4.30 18 0 0 69.59 4.70 18 0 0 58.29 3.20 18 0 0 63.59 4.50 -18 0 0 67.59 4.10 -18 0 0 58.79 3.90 -18 0 0 61.19 4.90 -20 0 0 320.07 11.80 -20 0 0 303.27 10.80 -20 0 0 323.67 10.60 20 0 0 329.37 11.40 20 0 0 318.97 11.40 20 0 0 318.97 10.10 20 0 0 322.07 10.90 -20 0 0 322.57 10.70 -22 0 0 274.87 10.00 -22 0 0 281.87 11.40 22 0 0 265.07 10.00 -22 0 0 293.67 10.50 22 0 0 267.97 10.80 -22 0 0 281.17 9.70 22 0 0 256.07 10.70 24 0 0 23.80 3.60 24 0 0 26.00 3.70 24 0 0 23.10 3.90 24 0 0 32.20 4.70 -24 0 0 20.40 3.20 -24 0 0 28.10 4.00 -24 0 0 21.50 3.30 -24 0 0 22.20 3.30 -26 0 0 260.47 11.40 -26 0 0 257.57 10.20 26 0 0 242.18 11.50 -26 0 0 250.37 10.70 26 0 0 247.18 10.70 26 0 0 249.97 12.10 26 0 0 217.28 11.10 28 0 0 117.79 8.60 -28 0 0 123.89 8.30 28 0 0 119.79 7.80 28 0 0 114.89 9.40 -28 0 0 125.59 8.40 -28 0 0 111.49 6.60 -30 0 0 6.40 4.10 30 0 0 5.00 4.10 30 0 0 1.80 4.50 -30 0 0 1.10 4.10 -1 -1 0 1.40 0.20 -1 -1 0 0.60 0.20 -1 -1 0 0.60 0.20 1 -1 0 0.70 0.20 1 -1 0 0.60 0.20 1 1 0 1.50 0.20 -1 1 0 2.30 0.30 -3 -1 0 1.30 0.30 -3 -1 0 3.30 0.60 3 -1 0 1.70 0.40 3 -1 0 1.70 0.40 3 -1 0 1.60 0.40 -3 -1 0 1.30 0.30 -3 -1 0 2.20 0.40 3 -1 0 1.10 0.40 -3 -1 0 1.50 0.40 -3 -1 0 0.50 0.30 3 -1 0 0.90 0.20 -3 -1 0 0.90 0.20 -3 -1 0 1.20 0.30 3 -1 0 0.80 0.40 -3 -1 0 1.60 0.40 -3 1 0 1.20 0.40 3 1 0 1.20 0.40 -3 1 0 0.80 0.30 -3 1 0 1.80 0.40 -3 1 0 2.40 0.50 3 1 0 1.20 0.30 3 1 0 1.30 0.40 3 1 0 1.30 0.30 3 1 0 0.70 0.30 3 1 0 2.50 0.40 -3 1 0 0.70 0.20 3 1 0 0.90 0.40 -3 1 0 1.30 0.40 5 -1 0 1.50 0.30 5 -1 0 1.50 0.60 5 -1 0 1.60 0.40 -5 -1 0 1.90 0.70 -5 -1 0 1.40 0.50 -5 -1 0 0.80 0.50 5 -1 0 2.40 0.50 -5 -1 0 2.00 0.40 -5 -1 0 0.60 0.50 5 -1 0 1.00 0.60 -5 1 0 0.80 0.50 -5 1 0 0.80 0.40 5 1 0 1.30 0.50 5 1 0 2.80 0.70 -5 1 0 2.10 0.40 5 1 0 1.70 0.50 -5 1 0 1.80 0.60 5 1 0 0.80 0.50 5 1 0 2.80 0.60 5 1 0 0.90 0.70 -7 -1 0 223.08 5.90 7 -1 0 233.98 6.30 7 -1 0 225.28 5.90 -7 -1 0 230.28 6.30 7 -1 0 226.98 6.70 7 -1 0 225.18 6.40 -7 -1 0 223.48 6.20 7 -1 0 226.58 5.60 -7 -1 0 215.98 6.50 7 1 0 227.48 6.00 7 1 0 235.58 6.40 7 1 0 230.48 6.50 -7 1 0 216.18 6.20 7 1 0 225.38 6.20 7 1 0 229.88 6.50 7 1 0 228.58 6.10 -7 1 0 223.68 6.20 -7 1 0 220.78 6.20 -7 1 0 230.48 6.50 9 -1 0 489.95 11.50 -9 -1 0 473.35 11.80 9 -1 0 476.75 12.00 9 -1 0 491.05 12.40 -9 -1 0 480.85 12.60 -9 -1 0 468.85 12.30 9 -1 0 491.95 13.00 -9 -1 0 483.65 12.30 9 -1 0 461.85 12.40 9 1 0 497.85 12.10 9 1 0 483.75 12.10 -9 1 0 483.85 12.30 9 1 0 475.85 12.20 -9 1 0 477.35 12.20 9 1 0 478.15 12.60 -9 1 0 485.75 12.30 -9 1 0 487.75 12.70 9 1 0 496.45 12.80 9 1 0 484.35 12.40 11 -1 0 940.81 22.80 -11 -1 0 886.21 21.10 -11 -1 0 890.81 22.30 -11 -1 0 890.31 21.90 11 -1 0 899.01 21.90 11 -1 0 900.91 20.90 -11 -1 0 880.81 21.80 11 -1 0 899.11 21.50 11 -1 0 880.71 22.00 11 1 0 915.31 21.50 11 1 0 849.12 21.50 -11 1 0 894.31 21.60 -11 1 0 898.81 21.80 11 1 0 875.11 22.20 11 1 0 880.51 22.00 11 1 0 933.91 21.70 -11 1 0 885.81 21.80 -11 1 0 890.51 22.20 -13 -1 0 433.16 12.50 13 -1 0 453.35 12.50 -13 -1 0 420.56 11.10 13 -1 0 439.86 11.10 13 -1 0 421.56 12.90 -13 -1 0 430.26 12.10 13 -1 0 427.16 12.00 13 -1 0 441.76 11.80 -13 -1 0 431.76 11.90 13 1 0 454.25 11.70 13 1 0 440.56 12.50 13 1 0 439.36 12.20 -13 1 0 435.66 12.50 -13 1 0 433.46 11.90 13 1 0 453.75 11.90 13 1 0 421.26 11.70 -13 1 0 422.16 11.60 15 -1 0 16.00 2.10 15 -1 0 15.20 2.20 15 -1 0 11.70 1.20 -15 -1 0 13.00 1.80 15 -1 0 17.30 1.60 -15 -1 0 13.20 1.50 -15 -1 0 15.70 2.40 15 -1 0 16.10 2.10 -15 -1 0 15.80 2.00 -15 -1 0 14.60 2.00 -15 1 0 14.00 2.00 -15 1 0 13.90 2.10 15 1 0 16.70 2.20 15 1 0 15.80 2.10 15 1 0 15.60 1.90 -15 1 0 13.80 2.30 15 1 0 14.10 2.00 17 -1 0 20.40 1.70 -17 -1 0 22.90 2.80 -17 -1 0 26.20 2.70 -17 -1 0 19.30 2.90 17 -1 0 24.50 2.50 17 -1 0 23.00 2.00 17 -1 0 23.60 2.70 17 -1 0 24.30 3.00 -17 -1 0 22.00 2.40 -17 1 0 21.60 3.00 17 1 0 26.70 2.40 17 1 0 21.40 2.80 17 1 0 22.90 2.60 -17 1 0 15.10 2.20 17 1 0 21.50 2.70 -17 1 0 17.70 2.30 19 -1 0 524.55 15.30 -19 -1 0 528.85 16.00 -19 -1 0 530.95 14.80 -19 -1 0 504.85 14.90 19 -1 0 501.95 15.30 -19 -1 0 494.55 15.20 19 -1 0 515.15 13.90 19 -1 0 504.45 15.70 -19 1 0 514.35 14.90 -19 1 0 520.75 15.80 19 1 0 519.55 15.80 19 1 0 530.55 15.10 -19 1 0 493.85 15.10 19 1 0 533.45 15.90 19 1 0 533.45 14.70 -21 -1 0 737.23 20.00 -21 -1 0 762.32 20.70 21 -1 0 743.13 21.30 -21 -1 0 769.52 21.70 21 -1 0 741.63 20.90 21 -1 0 723.73 20.70 -21 -1 0 733.63 20.80 21 1 0 719.43 21.30 -21 1 0 700.93 21.40 21 1 0 700.83 20.20 21 1 0 748.83 21.40 -21 1 0 724.83 20.80 21 1 0 744.13 20.10 -21 1 0 746.83 20.40 23 -1 0 323.57 12.20 -23 -1 0 340.97 12.10 -23 -1 0 323.27 10.90 -23 -1 0 315.47 11.40 23 -1 0 313.67 13.00 23 -1 0 325.37 12.00 23 -1 0 320.27 11.60 -23 -1 0 317.17 12.30 23 1 0 318.27 12.60 23 1 0 297.07 11.30 -23 1 0 333.57 11.50 -23 1 0 317.07 11.70 23 1 0 333.47 12.60 -23 1 0 325.57 11.40 -23 1 0 341.47 12.90 23 1 0 308.97 12.10 -25 -1 0 1.30 2.10 25 -1 0 -3.10 2.70 -25 -1 0 2.70 2.50 25 -1 0 3.10 2.70 -25 -1 0 2.50 1.70 -25 -1 0 5.90 3.00 25 -1 0 2.60 3.40 -25 1 0 1.40 2.30 -25 1 0 -0.40 1.90 -25 1 0 2.20 2.20 25 1 0 1.70 2.10 25 1 0 5.00 2.50 -25 1 0 3.40 1.90 25 1 0 5.20 2.60 25 1 0 2.80 3.20 27 -1 0 43.70 4.90 27 -1 0 49.30 6.40 -27 -1 0 48.00 5.50 -27 -1 0 54.89 5.90 27 -1 0 47.00 5.80 -27 -1 0 53.69 5.00 -27 1 0 55.29 5.80 27 1 0 47.70 5.30 27 1 0 51.79 6.30 -27 1 0 49.30 5.00 -27 1 0 47.40 5.50 27 1 0 43.10 6.20 29 -1 0 4.50 3.20 -29 -1 0 -0.10 3.50 29 -1 0 0.50 2.60 29 -1 0 1.20 3.20 -29 -1 0 2.10 2.90 -29 1 0 0.60 3.50 -29 1 0 -0.40 2.00 29 1 0 2.00 4.10 -29 1 0 0.00 3.70 29 1 0 -0.80 2.50 -31 -1 0 184.28 10.90 -31 -1 0 190.48 11.90 31 -1 0 175.78 11.30 -31 1 0 186.98 10.30 31 1 0 171.88 12.20 -31 1 0 180.18 10.70 31 1 0 163.18 13.80 0 -2 0 66.19 2.10 0 -2 0 72.89 2.10 0 -2 0 65.39 2.10 0 -2 0 67.39 2.10 0 -2 0 68.89 1.80 0 -2 0 68.89 2.10 0 -2 0 70.39 2.10 0 -2 0 69.49 2.00 0 2 0 69.69 2.10 0 2 0 75.39 2.20 0 2 0 69.39 2.00 0 2 0 68.89 2.10 0 2 0 70.59 2.10 0 2 0 68.69 2.10 0 2 0 68.49 2.10 0 2 0 69.49 1.80 0 2 0 72.19 2.10 -2 -2 0 196.08 5.10 -2 -2 0 186.28 4.90 -2 -2 0 194.98 4.80 2 -2 0 187.08 5.00 2 -2 0 198.38 4.90 2 -2 0 193.58 4.70 -2 -2 0 193.48 4.80 -2 -2 0 195.38 5.20 2 -2 0 200.78 5.10 -2 -2 0 195.98 5.00 2 -2 0 194.88 5.00 -2 2 0 188.98 5.00 -2 2 0 189.18 5.10 2 2 0 189.98 5.00 -2 2 0 199.18 5.20 -2 2 0 191.98 4.80 2 2 0 184.68 4.70 -2 2 0 190.48 4.90 2 2 0 198.28 5.20 -2 2 0 186.08 4.90 2 2 0 195.18 5.10 2 2 0 193.18 4.80 2 2 0 192.38 5.00 2 2 0 189.28 4.90 -4 -2 0 805.62 18.60 -4 -2 0 803.82 18.30 4 -2 0 815.32 18.50 4 -2 0 801.72 18.60 -4 -2 0 824.52 18.50 -4 -2 0 783.22 18.70 4 -2 0 745.13 18.10 -4 -2 0 812.82 18.00 4 -2 0 816.72 18.80 -4 -2 0 770.92 18.10 -4 -2 0 794.02 18.70 -4 2 0 785.42 18.80 -4 2 0 804.42 18.60 4 2 0 817.62 18.60 4 2 0 810.42 18.70 4 2 0 787.22 18.60 4 2 0 797.22 18.70 -4 2 0 760.92 18.60 4 2 0 803.72 18.10 -4 2 0 787.62 18.50 -6 -2 0 331.57 8.60 6 -2 0 327.37 7.70 6 -2 0 347.17 7.70 6 -2 0 336.37 8.60 6 -2 0 334.67 9.00 -6 -2 0 335.77 8.90 6 -2 0 344.57 8.70 -6 -2 0 336.07 8.60 -6 -2 0 325.97 8.30 -6 -2 0 327.67 8.50 6 -2 0 327.57 7.90 -6 2 0 322.97 8.80 6 2 0 329.87 8.20 6 2 0 337.47 8.80 -6 2 0 327.37 8.50 6 2 0 347.07 8.80 6 2 0 345.67 8.70 -6 2 0 329.37 8.90 -6 2 0 318.67 7.80 6 2 0 327.57 8.60 -8 -2 0 8.10 1.20 -8 -2 0 9.20 1.20 8 -2 0 8.80 1.20 8 -2 0 9.70 0.60 -8 -2 0 8.40 1.10 8 -2 0 9.20 1.60 -8 -2 0 8.70 1.10 8 -2 0 9.20 0.60 -8 -2 0 9.70 1.20 8 -2 0 8.80 1.10 8 -2 0 8.20 0.80 8 2 0 8.90 1.00 8 2 0 7.40 1.00 -8 2 0 11.60 1.50 8 2 0 7.80 1.30 -8 2 0 8.30 1.00 -8 2 0 8.10 1.20 8 2 0 10.30 1.10 8 2 0 8.10 1.30 10 -2 0 4.90 0.60 -10 -2 0 4.80 1.20 -10 -2 0 7.70 1.10 10 -2 0 6.90 1.00 10 -2 0 6.60 1.60 10 -2 0 5.90 1.10 -10 -2 0 4.80 1.00 -10 -2 0 6.50 1.20 10 -2 0 6.40 1.10 10 -2 0 6.60 0.60 -10 -2 0 6.50 1.10 -10 2 0 7.50 1.20 -10 2 0 6.50 1.40 10 2 0 5.50 1.20 10 2 0 6.40 1.00 -10 2 0 5.20 1.20 -10 2 0 5.50 1.20 10 2 0 5.50 1.00 10 2 0 8.30 1.20 10 2 0 5.20 1.40 12 -2 0 20.40 2.10 12 -2 0 20.10 2.10 12 -2 0 18.40 1.70 -12 -2 0 20.30 2.10 -12 -2 0 20.70 1.50 12 -2 0 19.70 1.10 -12 -2 0 19.00 1.70 -12 -2 0 22.50 2.20 12 -2 0 18.90 1.20 12 -2 0 21.60 2.40 -12 -2 0 20.40 2.10 12 2 0 15.60 1.70 12 2 0 18.60 1.80 12 2 0 19.80 2.20 12 2 0 19.10 1.80 -12 2 0 16.70 2.00 -12 2 0 19.60 2.00 -12 2 0 19.70 2.00 -12 2 0 17.20 1.80 12 2 0 21.00 2.20 14 -2 0 76.79 2.80 14 -2 0 70.19 4.70 -14 -2 0 77.29 3.50 14 -2 0 77.89 4.00 -14 -2 0 75.79 4.10 14 -2 0 70.89 3.50 14 -2 0 81.39 2.70 -14 -2 0 73.59 4.20 14 -2 0 74.69 3.90 -14 -2 0 74.09 3.20 -14 -2 0 80.69 4.00 -14 2 0 74.99 3.80 -14 2 0 76.49 3.70 -14 2 0 74.39 4.10 14 2 0 74.29 3.60 14 2 0 75.99 3.50 14 2 0 74.79 4.30 -14 2 0 70.99 3.50 14 2 0 79.79 4.20 -16 -2 0 0.90 1.30 16 -2 0 1.40 0.80 16 -2 0 2.80 0.70 -16 -2 0 1.40 1.70 -16 -2 0 3.50 1.50 16 -2 0 1.90 1.30 16 -2 0 1.40 1.30 16 -2 0 0.40 1.60 16 -2 0 -1.10 2.00 -16 -2 0 4.90 1.50 -16 2 0 2.80 1.40 16 2 0 -0.40 1.30 -16 2 0 -0.60 1.60 16 2 0 0.90 1.80 16 2 0 -0.60 1.30 -16 2 0 1.50 1.10 16 2 0 0.30 1.30 -18 -2 0 67.99 4.30 18 -2 0 72.49 4.80 18 -2 0 70.29 3.20 -18 -2 0 71.79 4.80 18 -2 0 62.89 4.20 18 -2 0 73.79 4.30 -18 -2 0 64.49 4.50 -18 -2 0 77.79 4.00 18 2 0 73.09 4.30 -18 2 0 72.59 4.70 -18 2 0 71.69 4.40 -18 2 0 67.59 5.10 18 2 0 66.99 5.00 18 2 0 66.69 3.90 18 2 0 69.19 4.60 -20 -2 0 201.28 8.10 -20 -2 0 215.18 9.20 20 -2 0 213.68 8.70 20 -2 0 198.48 7.80 20 -2 0 199.48 8.40 -20 -2 0 199.08 8.10 -20 -2 0 192.98 7.40 -20 2 0 195.78 8.00 -20 2 0 208.28 8.70 20 2 0 198.08 7.80 -20 2 0 213.48 8.10 20 2 0 207.98 8.00 20 2 0 210.68 9.10 20 2 0 188.38 8.40 -22 -2 0 57.89 4.40 -22 -2 0 54.59 5.40 22 -2 0 69.19 5.00 -22 -2 0 52.39 4.50 22 -2 0 57.89 4.90 -22 -2 0 60.89 4.70 22 -2 0 54.49 5.10 22 2 0 57.29 5.30 -22 2 0 57.39 5.10 -22 2 0 57.49 4.60 22 2 0 56.49 5.10 22 2 0 70.39 4.80 22 2 0 66.29 4.70 22 2 0 60.99 5.60 -22 2 0 62.19 5.60 24 -2 0 11.30 3.40 -24 -2 0 10.20 2.90 -24 -2 0 15.80 3.10 -24 -2 0 11.30 2.70 -24 -2 0 15.20 3.40 24 -2 0 15.40 3.50 24 -2 0 8.70 3.00 24 2 0 9.40 2.80 24 2 0 8.30 3.40 24 2 0 14.90 4.00 -24 2 0 7.40 3.40 -24 2 0 10.60 2.70 24 2 0 15.20 2.60 -24 2 0 10.80 2.80 26 -2 0 11.60 3.00 -26 -2 0 16.00 3.60 -26 -2 0 20.40 3.40 -26 -2 0 13.90 3.80 26 -2 0 13.00 3.10 26 -2 0 18.70 4.00 26 2 0 11.80 3.90 -26 2 0 10.10 3.30 26 2 0 20.80 4.60 -26 2 0 15.90 3.40 26 2 0 16.80 4.40 -26 2 0 13.30 3.40 -28 -2 0 169.48 9.90 -28 -2 0 177.18 9.90 28 -2 0 169.98 10.10 28 -2 0 181.88 10.60 -28 -2 0 174.78 8.10 -28 2 0 183.48 10.30 28 2 0 182.98 10.30 28 2 0 187.38 11.10 -28 2 0 195.18 10.90 28 2 0 172.38 10.60 -28 2 0 183.28 9.20 30 -2 0 243.78 13.90 -30 -2 0 258.87 12.70 -30 -2 0 251.57 12.30 30 -2 0 244.58 12.20 -30 2 0 244.58 10.70 30 2 0 234.78 13.10 30 2 0 237.68 12.80 -30 2 0 243.28 11.80 -30 2 0 256.27 12.40 1 -3 0 125.79 3.40 -1 -3 0 127.79 3.10 -1 -3 0 123.49 3.70 -1 -3 0 125.59 3.60 -1 -3 0 124.59 3.70 -1 -3 0 121.89 3.60 1 -3 0 129.89 3.60 1 -3 0 129.29 3.30 1 -3 0 124.59 3.60 1 -3 0 127.49 3.70 -1 -3 0 124.49 3.80 1 -3 0 134.79 3.80 1 3 0 124.49 3.60 -1 3 0 128.19 3.40 1 3 0 126.09 3.60 1 3 0 120.99 3.70 -1 3 0 128.49 3.70 -1 3 0 125.19 3.80 1 3 0 130.89 3.80 1 3 0 121.99 3.90 -1 3 0 124.99 3.40 -1 3 0 125.39 3.60 -1 3 0 120.59 3.80 1 3 0 129.99 3.80 1 3 0 125.29 3.00 1 3 0 124.39 3.10 -3 -3 0 28.70 1.60 -3 -3 0 26.40 1.10 -3 -3 0 26.10 1.40 -3 -3 0 25.20 1.30 3 -3 0 27.80 1.60 -3 -3 0 26.20 1.70 -3 -3 0 25.50 1.30 3 -3 0 24.00 1.30 -3 -3 0 25.90 1.40 3 -3 0 26.70 1.20 3 -3 0 25.10 1.50 3 -3 0 26.20 1.40 3 3 0 24.50 1.60 3 3 0 24.70 1.60 -3 3 0 24.60 1.60 3 3 0 26.30 1.60 3 3 0 26.60 1.50 -3 3 0 25.00 1.30 -3 3 0 25.90 1.50 3 3 0 24.70 1.10 3 3 0 25.50 1.20 -5 -3 0 898.01 20.20 -5 -3 0 890.71 21.20 -5 -3 0 873.11 21.20 -5 -3 0 887.11 21.00 -5 -3 0 866.11 20.40 5 -3 0 882.81 20.80 5 -3 0 843.42 20.00 -5 -3 0 902.01 20.60 5 -3 0 880.61 20.20 -5 -3 0 877.71 20.90 5 -3 0 897.61 21.20 5 -3 0 906.11 21.10 -5 3 0 904.31 20.10 5 3 0 896.71 21.10 -5 3 0 892.81 21.30 5 3 0 910.41 21.20 -5 3 0 871.81 20.90 5 3 0 914.81 21.20 5 3 0 869.51 21.10 5 3 0 919.61 20.40 -7 -3 0 949.80 22.40 -7 -3 0 934.61 22.30 -7 -3 0 936.91 22.70 7 -3 0 969.40 22.90 7 -3 0 952.10 22.60 7 -3 0 907.31 21.30 -7 -3 0 962.30 22.60 7 -3 0 944.41 22.30 -7 -3 0 942.81 22.00 -7 -3 0 927.11 21.60 7 -3 0 964.40 22.60 -7 3 0 913.61 22.50 7 3 0 957.00 22.50 7 3 0 938.41 22.60 7 3 0 936.31 22.50 7 3 0 959.80 22.70 -7 3 0 907.11 22.30 -7 3 0 927.91 22.80 7 3 0 941.41 21.70 9 -3 0 394.56 9.10 9 -3 0 406.26 11.30 -9 -3 0 378.26 10.20 9 -3 0 388.06 10.50 9 -3 0 405.96 10.80 -9 -3 0 373.86 10.50 -9 -3 0 396.26 10.70 -9 -3 0 387.46 10.90 9 -3 0 389.36 9.50 -9 -3 0 391.36 10.10 -9 3 0 383.96 10.80 9 3 0 378.46 10.50 9 3 0 395.16 9.90 -9 3 0 394.46 10.80 9 3 0 402.86 10.70 9 3 0 396.26 10.80 -9 3 0 392.26 10.50 9 3 0 390.56 10.90 -11 -3 0 4.20 1.50 11 -3 0 6.20 1.40 11 -3 0 5.00 0.60 11 -3 0 2.40 1.30 -11 -3 0 4.20 1.30 11 -3 0 4.80 1.10 -11 -3 0 11.90 1.30 -11 -3 0 4.70 0.90 -11 -3 0 3.70 1.00 11 -3 0 4.10 0.50 11 -3 0 5.20 0.90 11 3 0 9.20 1.80 11 3 0 4.70 1.00 -11 3 0 10.00 1.50 -11 3 0 2.90 1.00 -11 3 0 5.40 1.50 11 3 0 3.40 1.10 -11 3 0 5.00 1.20 11 3 0 2.40 1.30 11 3 0 5.90 1.40 -13 -3 0 10.00 1.70 -13 -3 0 6.90 1.50 13 -3 0 9.00 1.90 -13 -3 0 7.10 1.70 13 -3 0 6.60 0.60 -13 -3 0 7.40 1.40 13 -3 0 10.40 1.70 13 -3 0 7.50 1.20 13 -3 0 6.90 0.70 13 -3 0 7.70 1.50 -13 3 0 6.00 1.30 -13 3 0 4.60 1.40 13 3 0 7.10 1.30 -13 3 0 7.00 1.50 13 3 0 7.10 1.80 13 3 0 6.80 1.90 13 3 0 5.40 1.30 -13 3 0 5.80 1.30 -15 -3 0 607.04 16.50 -15 -3 0 603.44 16.50 15 -3 0 619.74 14.20 15 -3 0 612.94 18.00 -15 -3 0 602.24 17.10 15 -3 0 601.44 16.70 -15 -3 0 605.94 15.80 15 -3 0 610.54 15.70 15 -3 0 619.94 16.90 15 3 0 618.64 17.20 15 3 0 607.34 15.80 -15 3 0 605.74 16.60 -15 3 0 601.64 16.40 -15 3 0 615.84 16.50 -15 3 0 597.94 17.10 15 3 0 595.84 17.10 15 3 0 620.14 16.60 17 -3 0 1281.27 28.70 17 -3 0 1253.37 31.80 17 -3 0 1266.77 30.70 -17 -3 0 1274.97 31.50 17 -3 0 1266.77 33.40 17 -3 0 1237.78 31.80 -17 -3 0 1246.68 30.60 -17 -3 0 1213.78 31.40 -17 -3 0 1264.17 32.20 17 3 0 1226.78 32.00 -17 3 0 1246.68 31.50 -17 3 0 1264.77 32.20 17 3 0 1272.97 32.20 17 3 0 1276.77 30.70 -17 3 0 1241.38 31.20 -17 3 0 1281.07 31.40 17 3 0 1280.97 31.50 -19 -3 0 348.37 10.70 -19 -3 0 330.97 11.10 19 -3 0 322.17 10.60 -19 -3 0 330.57 12.10 -19 -3 0 341.37 11.30 19 -3 0 344.67 11.80 19 -3 0 336.77 11.70 19 3 0 342.77 12.10 -19 3 0 342.97 11.10 19 3 0 337.87 11.80 19 3 0 326.97 11.00 -19 3 0 345.97 10.80 19 3 0 337.87 10.70 -19 3 0 356.86 12.00 19 3 0 350.96 12.30 -19 3 0 329.97 11.10 -21 -3 0 3.20 1.50 21 -3 0 1.30 2.40 -21 -3 0 2.50 2.10 -21 -3 0 3.60 2.10 21 -3 0 4.50 1.90 -21 -3 0 2.10 2.40 21 -3 0 3.70 1.90 21 3 0 5.90 2.80 -21 3 0 1.40 1.90 21 3 0 7.00 2.10 -21 3 0 1.70 1.90 21 3 0 3.10 2.00 21 3 0 3.00 2.00 -21 3 0 6.00 2.10 21 3 0 2.60 2.10 -23 -3 0 3.20 2.10 -23 -3 0 4.20 2.30 -23 -3 0 3.60 3.00 23 -3 0 2.50 2.80 23 -3 0 2.50 2.80 -23 -3 0 3.50 2.10 23 3 0 8.10 2.60 -23 3 0 2.00 2.70 23 3 0 -1.70 2.70 23 3 0 9.70 3.50 23 3 0 5.20 2.30 -23 3 0 2.40 2.90 23 3 0 7.40 3.20 -23 3 0 2.80 1.60 -25 -3 0 164.18 8.70 -25 -3 0 169.18 7.60 -25 -3 0 177.88 9.20 25 -3 0 159.58 9.80 25 -3 0 173.28 9.20 25 -3 0 167.98 9.20 25 3 0 171.48 9.50 -25 3 0 154.38 7.60 25 3 0 162.68 9.70 -25 3 0 170.78 8.90 -25 3 0 161.88 8.30 25 3 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3.20 -2 -4 0 100.19 3.40 -2 4 0 102.89 3.00 -2 4 0 98.39 3.60 2 4 0 104.09 3.80 -2 4 0 97.29 3.40 2 4 0 101.79 3.50 2 4 0 104.99 3.40 -2 4 0 103.89 3.30 2 4 0 102.99 3.60 2 4 0 99.89 3.40 2 4 0 102.49 2.60 -4 -4 0 6376.46 150.08 4 -4 0 6492.45 150.08 4 -4 0 6293.37 147.09 4 -4 0 6294.87 148.39 4 -4 0 6650.63 149.69 4 -4 0 6716.13 148.59 -4 -4 0 6285.47 147.39 -4 -4 0 6244.58 148.79 -4 -4 0 6758.32 148.49 -4 -4 0 6124.39 147.99 -4 -4 0 6881.81 146.79 -4 -4 0 6615.44 149.39 4 4 0 6226.48 149.29 4 4 0 6504.35 146.69 -4 4 0 6369.46 147.89 4 4 0 6077.59 144.99 -4 4 0 6784.82 149.88 -4 4 0 6353.96 148.59 4 4 0 6639.84 149.49 4 4 0 6083.19 149.29 -6 -4 0 2532.15 58.59 6 -4 0 2668.53 58.59 -6 -4 0 2578.74 58.99 -6 -4 0 2587.14 57.59 -6 -4 0 2648.24 58.59 6 -4 0 2573.84 58.79 6 -4 0 2640.34 58.99 6 -4 0 2539.15 59.19 6 -4 0 2404.86 57.59 -6 -4 0 2460.05 57.89 -6 -4 0 2588.04 58.99 -6 -4 0 2628.84 58.19 -6 4 0 2609.34 57.59 6 4 0 2554.04 58.89 6 4 0 2634.64 58.89 6 4 0 2592.54 58.89 6 4 0 2607.64 58.89 -6 4 0 2613.34 58.69 -6 4 0 2542.55 59.09 8 -4 0 2815.62 63.59 8 -4 0 2841.82 63.29 -8 -4 0 2724.23 61.99 8 -4 0 2850.71 63.09 -8 -4 0 2740.33 63.29 -8 -4 0 2784.52 63.29 8 -4 0 2768.02 63.19 -8 -4 0 2664.13 62.79 -8 -4 0 2804.42 62.89 8 -4 0 2866.21 62.89 -8 -4 0 2777.82 62.39 8 -4 0 2596.04 62.69 8 4 0 2767.82 63.29 8 4 0 2798.82 63.19 -8 4 0 2727.43 63.39 -8 4 0 2838.22 62.19 8 4 0 2693.53 63.19 8 4 0 2815.92 61.99 -8 4 0 2643.54 63.09 8 4 0 2706.83 63.09 -8 4 0 2727.43 62.89 10 -4 0 91.69 2.70 10 -4 0 92.99 4.20 -10 -4 0 90.99 4.10 -10 -4 0 84.99 3.10 -10 -4 0 84.89 3.90 10 -4 0 96.69 3.90 -10 -4 0 91.79 3.50 -10 -4 0 90.69 3.70 10 -4 0 88.29 4.50 -10 -4 0 89.29 4.10 10 -4 0 90.49 2.80 10 -4 0 89.79 2.30 10 4 0 88.39 3.90 10 4 0 93.09 3.30 10 4 0 88.09 3.90 -10 4 0 91.79 4.20 -10 4 0 88.39 3.80 -10 4 0 96.39 4.20 10 4 0 86.99 4.00 10 4 0 89.49 4.10 12 -4 0 42.60 1.90 12 -4 0 39.50 1.30 12 -4 0 40.50 2.70 -12 -4 0 35.90 2.00 12 -4 0 42.40 3.20 12 -4 0 38.90 3.30 -12 -4 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0 69.89 3.40 18 -4 0 72.19 4.90 18 -4 0 75.99 4.90 -18 -4 0 69.89 4.40 18 -4 0 67.19 3.80 -18 -4 0 81.19 4.90 -18 -4 0 64.29 4.10 18 4 0 76.59 4.10 -18 4 0 65.59 4.20 18 4 0 73.39 4.60 18 4 0 69.89 4.70 18 4 0 75.89 5.80 -18 4 0 73.89 4.30 18 4 0 75.39 4.90 -18 4 0 71.59 4.80 -18 4 0 77.89 5.40 20 -4 0 2.80 2.50 -20 -4 0 1.30 2.10 -20 -4 0 3.90 1.30 -20 -4 0 3.60 2.70 -20 -4 0 3.50 1.80 20 -4 0 0.90 1.50 -20 -4 0 2.90 2.00 20 4 0 1.00 2.20 20 4 0 2.20 1.60 -20 4 0 3.80 2.00 -20 4 0 5.30 2.20 -20 4 0 3.10 2.60 20 4 0 5.50 2.70 20 4 0 3.80 1.80 20 4 0 5.00 2.80 -22 -4 0 157.38 6.60 -22 -4 0 162.48 8.30 -22 -4 0 167.98 7.80 -22 -4 0 153.98 7.90 22 -4 0 160.38 7.80 22 -4 0 154.98 7.90 -22 4 0 168.18 7.60 -22 4 0 170.88 7.80 22 4 0 166.28 8.00 22 4 0 159.18 8.10 -22 4 0 168.98 8.30 22 4 0 155.28 8.30 22 4 0 175.68 9.30 -24 -4 0 31.70 4.00 24 -4 0 34.40 4.70 -24 -4 0 31.30 4.90 24 -4 0 31.00 4.50 -24 -4 0 27.60 3.50 24 -4 0 26.90 4.70 -24 -4 0 34.10 3.80 24 4 0 29.30 4.50 24 4 0 34.10 4.70 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7.20 1 5 0 276.27 8.00 1 5 0 272.07 7.40 -3 -5 0 1707.03 38.90 3 -5 0 1680.33 39.40 3 -5 0 1728.33 39.40 3 -5 0 1669.83 38.20 3 -5 0 1713.33 38.80 -3 -5 0 1687.43 39.20 -3 -5 0 1716.43 39.90 -3 -5 0 1680.23 39.00 3 -5 0 1706.13 39.10 -3 -5 0 1714.33 39.00 -3 -5 0 1684.93 39.30 3 -5 0 1719.23 39.00 3 5 0 1709.43 39.20 3 5 0 1674.53 39.00 -3 5 0 1715.73 38.50 3 5 0 1727.53 39.30 3 5 0 1706.63 39.40 3 5 0 1684.13 39.40 -3 5 0 1718.93 39.40 3 5 0 1690.73 39.70 -3 5 0 1690.33 39.10 -3 5 0 1703.23 39.60 5 -5 0 316.07 7.80 -5 -5 0 302.07 9.00 -5 -5 0 314.57 8.70 -5 -5 0 312.27 8.90 -5 -5 0 299.17 7.60 -5 -5 0 302.57 8.00 -5 -5 0 298.67 8.40 5 -5 0 306.87 8.40 5 -5 0 312.97 8.70 5 -5 0 310.27 8.90 -5 -5 0 306.17 8.20 5 -5 0 296.37 8.60 5 5 0 302.27 8.70 5 5 0 306.87 8.80 -5 5 0 303.27 8.20 5 5 0 316.87 8.80 5 5 0 307.27 9.00 5 5 0 310.87 7.70 -5 5 0 310.07 9.10 -5 5 0 310.07 8.70 -7 -5 0 144.29 4.70 -7 -5 0 145.79 5.50 -7 -5 0 147.19 5.10 -7 -5 0 142.29 5.50 7 -5 0 147.89 4.00 7 -5 0 148.69 5.20 7 -5 0 148.99 5.50 7 -5 0 151.08 5.00 -7 -5 0 148.29 5.20 -7 -5 0 137.59 4.40 7 5 0 141.09 5.30 -7 5 0 143.99 5.50 7 5 0 149.39 5.40 -7 5 0 151.98 4.10 7 5 0 150.08 4.50 7 5 0 144.49 5.30 7 5 0 150.48 5.30 -7 5 0 147.29 5.20 9 -5 0 300.67 7.10 -9 -5 0 279.97 7.70 9 -5 0 282.17 9.20 9 -5 0 286.17 6.70 -9 -5 0 292.67 8.10 -9 -5 0 295.47 8.60 -9 -5 0 288.67 9.00 -9 -5 0 299.67 9.00 9 -5 0 307.67 8.60 9 -5 0 294.87 9.00 9 -5 0 287.97 8.80 9 5 0 297.47 9.00 9 5 0 294.47 9.10 -9 5 0 299.57 6.80 -9 5 0 282.17 9.10 9 5 0 290.57 9.00 9 5 0 284.57 8.10 9 5 0 277.27 7.60 9 5 0 272.97 8.80 -9 5 0 300.37 8.70 -9 5 0 290.37 8.90 -11 -5 0 167.58 5.80 -11 -5 0 165.68 6.10 -11 -5 0 155.98 4.90 11 -5 0 157.18 4.30 11 -5 0 162.58 6.50 11 -5 0 155.28 6.20 -11 -5 0 153.38 5.30 11 -5 0 152.08 3.70 -11 -5 0 166.08 6.40 11 -5 0 159.58 5.80 11 5 0 164.58 6.20 -11 5 0 165.48 5.80 11 5 0 152.88 5.50 -11 5 0 165.38 6.50 11 5 0 151.08 6.00 -11 5 0 157.98 6.00 11 5 0 161.18 5.00 11 5 0 150.68 6.10 13 -5 0 1017.60 24.00 13 -5 0 1017.80 27.20 -13 -5 0 1014.00 24.40 13 -5 0 1050.09 26.40 -13 -5 0 1053.69 26.60 13 -5 0 1047.70 25.90 -13 -5 0 1018.10 26.10 -13 -5 0 1006.90 25.70 -13 -5 0 1036.80 25.00 -13 5 0 1049.00 26.50 -13 5 0 1070.99 26.50 13 5 0 1044.30 26.60 13 5 0 1033.30 26.20 -13 5 0 1038.20 25.90 13 5 0 1045.00 24.70 13 5 0 1009.40 26.30 13 5 0 1002.00 25.50 15 -5 0 942.41 26.20 15 -5 0 964.30 22.90 -15 -5 0 969.30 25.00 15 -5 0 939.31 24.70 -15 -5 0 980.30 25.60 -15 -5 0 958.00 23.70 15 -5 0 954.80 25.20 -15 -5 0 975.80 24.70 -15 -5 0 934.31 23.00 15 5 0 958.50 25.50 15 5 0 963.90 24.50 15 5 0 957.10 23.40 -15 5 0 943.11 24.60 15 5 0 988.60 25.10 -15 5 0 968.30 24.80 -15 5 0 944.41 25.10 -15 5 0 975.60 25.20 15 5 0 978.80 25.40 -17 -5 0 109.69 6.30 -17 -5 0 105.79 5.60 17 -5 0 104.79 5.40 17 -5 0 107.69 6.60 17 -5 0 105.39 6.20 -17 -5 0 97.59 4.10 -17 -5 0 111.09 5.00 17 -5 0 104.79 4.30 -17 -5 0 108.89 5.50 17 5 0 100.29 4.70 -17 5 0 109.99 5.70 17 5 0 110.29 6.50 -17 5 0 108.59 5.50 -17 5 0 112.19 6.20 17 5 0 103.49 5.70 -17 5 0 101.09 5.70 17 5 0 105.39 5.60 17 5 0 109.49 5.90 19 -5 0 1.70 1.70 -19 -5 0 5.80 2.60 -19 -5 0 0.50 1.30 -19 -5 0 1.70 1.10 -19 -5 0 1.80 2.10 -19 -5 0 -1.30 1.50 19 -5 0 3.90 1.70 19 5 0 2.60 2.20 19 5 0 0.40 1.30 19 5 0 0.90 2.10 19 5 0 1.10 1.80 -19 5 0 0.50 2.30 19 5 0 2.20 2.70 -19 5 0 1.90 2.10 -19 5 0 1.40 1.40 -19 5 0 0.10 1.90 -21 -5 0 0.20 2.80 -21 -5 0 -1.00 1.70 -21 -5 0 1.30 2.40 21 -5 0 2.40 2.60 -21 -5 0 3.10 2.30 21 -5 0 4.00 1.90 21 5 0 1.70 2.00 21 5 0 -1.80 2.90 -21 5 0 2.90 2.30 -21 5 0 2.60 2.70 21 5 0 0.70 1.70 -21 5 0 2.40 2.00 -21 5 0 2.90 2.20 21 5 0 1.00 1.60 -23 -5 0 137.29 7.20 23 -5 0 138.69 7.90 -23 -5 0 149.29 7.30 -23 -5 0 126.99 6.10 -23 -5 0 138.19 8.00 23 -5 0 135.59 8.80 -23 5 0 142.39 7.90 -23 5 0 145.19 7.40 23 5 0 139.69 8.50 -23 5 0 123.39 6.90 -23 5 0 138.89 8.40 23 5 0 144.99 7.60 23 5 0 138.09 7.90 23 5 0 152.88 9.30 25 -5 0 320.37 13.80 25 -5 0 350.86 14.80 -25 -5 0 345.87 14.30 25 -5 0 340.07 13.60 -25 -5 0 328.87 11.50 -25 -5 0 334.37 12.70 25 5 0 333.57 13.00 -25 5 0 336.27 13.80 25 5 0 353.16 15.00 -25 5 0 324.07 13.20 25 5 0 323.27 14.00 -27 -5 0 194.18 10.40 27 -5 0 189.68 10.80 -27 -5 0 189.48 9.60 27 -5 0 188.78 11.70 27 5 0 185.48 9.80 27 5 0 197.98 11.20 27 5 0 195.88 10.60 -27 5 0 189.28 9.80 -27 5 0 210.78 10.40 29 -5 0 -5.00 4.00 29 -5 0 -1.80 3.70 -29 -5 0 2.90 3.60 -29 -5 0 0.40 4.00 29 5 0 -2.50 3.80 29 5 0 -2.50 4.00 29 5 0 -0.80 2.50 -29 5 0 4.10 4.00 -29 5 0 2.60 4.00 0 -6 0 404.06 10.90 0 -6 0 400.36 10.80 0 -6 0 407.96 10.70 0 -6 0 411.76 10.80 0 -6 0 403.16 9.90 0 6 0 400.66 11.00 0 6 0 406.46 10.50 0 6 0 414.26 11.00 0 6 0 420.56 11.40 0 6 0 405.56 11.00 -2 -6 0 56.89 2.70 -2 -6 0 58.19 1.80 2 -6 0 66.79 2.90 2 -6 0 60.19 3.10 2 -6 0 60.79 2.90 -2 -6 0 57.89 3.00 2 -6 0 58.99 2.40 -2 -6 0 59.79 2.80 2 -6 0 58.79 2.60 -2 -6 0 58.69 2.80 -2 -6 0 60.69 2.90 -2 6 0 59.99 2.50 2 6 0 56.89 2.70 -2 6 0 53.29 2.80 2 6 0 60.79 2.90 2 6 0 64.79 3.30 2 6 0 57.09 2.90 2 6 0 61.19 3.00 -2 6 0 60.19 2.80 -2 6 0 62.39 3.20 -4 -6 0 18.20 2.20 -4 -6 0 16.90 1.70 4 -6 0 13.40 0.80 4 -6 0 15.40 1.30 4 -6 0 16.00 1.60 -4 -6 0 15.70 1.50 4 -6 0 16.70 1.90 -4 -6 0 17.50 1.60 4 -6 0 15.40 1.60 -4 -6 0 18.20 1.70 4 -6 0 15.60 1.50 -4 -6 0 15.20 0.70 -4 6 0 15.70 1.20 4 6 0 16.20 1.70 -4 6 0 16.40 1.60 -4 6 0 19.10 1.70 4 6 0 16.70 1.80 4 6 0 16.50 2.00 4 6 0 19.00 1.80 4 6 0 14.60 0.90 -4 6 0 15.90 2.00 4 6 0 15.60 1.60 6 -6 0 26.20 1.50 -6 -6 0 21.80 2.20 -6 -6 0 25.40 2.40 -6 -6 0 26.80 1.90 -6 -6 0 22.70 1.80 6 -6 0 21.50 2.00 6 -6 0 23.00 2.20 -6 -6 0 21.70 2.10 -6 -6 0 24.30 1.70 -6 -6 0 22.50 1.10 6 6 0 22.70 1.40 -6 6 0 23.00 2.50 6 6 0 22.70 2.30 6 6 0 23.70 2.30 6 6 0 24.20 2.20 6 6 0 24.10 2.10 -6 6 0 24.70 2.20 8 -6 0 408.26 11.10 8 -6 0 406.86 11.50 -8 -6 0 380.86 10.30 -8 -6 0 402.36 11.70 -8 -6 0 405.26 11.80 8 -6 0 421.66 11.90 -8 -6 0 396.26 11.20 8 -6 0 416.36 9.90 8 -6 0 404.96 11.60 -8 -6 0 429.86 10.80 8 6 0 409.86 11.70 8 6 0 384.86 11.50 -8 6 0 397.26 10.00 -8 6 0 412.76 11.40 8 6 0 402.06 10.40 8 6 0 404.26 11.60 -8 6 0 388.26 11.90 8 6 0 393.86 12.40 10 -6 0 274.27 8.90 10 -6 0 264.27 8.30 -10 -6 0 263.77 7.40 -10 -6 0 277.37 7.90 10 -6 0 276.17 6.60 -10 -6 0 267.17 8.80 10 -6 0 275.57 8.90 -10 -6 0 267.97 8.80 10 -6 0 267.57 9.20 -10 -6 0 270.97 8.40 10 6 0 263.77 7.80 10 6 0 276.37 8.90 -10 6 0 270.47 8.70 -10 6 0 264.77 9.00 10 6 0 266.57 9.00 -10 6 0 253.37 8.30 -10 6 0 272.27 6.30 10 6 0 261.97 8.70 -12 -6 0 12.50 1.80 12 -6 0 9.30 1.80 12 -6 0 10.30 1.90 -12 -6 0 13.40 2.40 12 -6 0 13.40 2.30 -12 -6 0 8.50 2.00 -12 -6 0 12.30 1.40 -12 -6 0 13.70 1.80 12 -6 0 10.80 2.20 -12 6 0 12.90 2.10 -12 6 0 13.40 2.30 12 6 0 14.10 1.80 -12 6 0 13.30 2.20 12 6 0 12.00 2.20 12 6 0 13.80 2.10 12 6 0 10.40 2.00 14 -6 0 251.87 9.20 14 -6 0 251.97 9.70 -14 -6 0 248.58 9.20 -14 -6 0 244.78 8.90 14 -6 0 243.28 8.40 -14 -6 0 248.08 7.10 14 -6 0 233.58 6.20 -14 -6 0 240.68 7.60 -14 -6 0 246.18 8.40 14 6 0 249.58 9.30 -14 6 0 222.28 8.20 14 6 0 245.48 8.20 -14 6 0 239.68 8.80 14 6 0 242.68 8.90 -14 6 0 249.38 9.00 14 6 0 245.08 8.80 -16 -6 0 56.19 4.80 -16 -6 0 50.79 3.20 -16 -6 0 54.59 3.00 -16 -6 0 56.39 4.00 16 -6 0 48.70 4.00 16 -6 0 54.39 5.30 -16 -6 0 51.69 3.70 16 -6 0 49.90 4.70 -16 6 0 50.79 4.10 16 6 0 61.29 3.20 16 6 0 53.69 4.40 -16 6 0 55.29 4.20 16 6 0 59.79 4.10 -16 6 0 55.09 4.20 -16 6 0 63.29 4.80 16 6 0 58.69 4.30 16 6 0 50.89 4.70 -18 -6 0 121.39 7.00 -18 -6 0 138.29 6.80 18 -6 0 121.59 6.20 18 -6 0 130.69 8.20 -18 -6 0 131.59 6.60 -18 -6 0 109.19 4.60 -18 -6 0 134.79 5.70 18 -6 0 127.49 6.80 -18 6 0 137.09 6.70 -18 6 0 126.09 6.40 -18 6 0 137.89 6.40 -18 6 0 134.29 6.50 18 6 0 134.09 6.50 18 6 0 132.39 6.90 18 6 0 128.29 7.00 18 6 0 124.19 7.00 -20 -6 0 109.49 6.50 20 -6 0 103.29 6.00 -20 -6 0 117.19 5.60 20 -6 0 109.19 7.10 -20 -6 0 107.29 6.40 -20 -6 0 109.39 7.00 20 6 0 112.99 7.10 -20 6 0 115.99 6.60 -20 6 0 99.79 6.30 -20 6 0 119.69 6.40 20 6 0 114.19 6.00 -20 6 0 116.29 6.20 20 6 0 112.29 7.10 20 6 0 112.39 6.80 -22 -6 0 92.69 5.30 22 -6 0 100.19 6.70 -22 -6 0 95.39 6.50 -22 -6 0 89.79 5.80 22 -6 0 95.59 6.60 -22 -6 0 97.09 7.20 22 6 0 94.59 6.60 -22 6 0 85.39 6.00 22 6 0 98.59 6.30 22 6 0 108.39 7.40 -22 6 0 101.19 7.20 22 6 0 96.39 6.60 -22 6 0 94.49 5.80 -22 6 0 99.59 6.70 24 -6 0 656.63 21.70 24 -6 0 621.34 21.30 -24 -6 0 657.93 20.30 -24 -6 0 687.23 21.40 -24 -6 0 662.13 20.20 24 6 0 672.63 21.20 -24 6 0 668.63 21.20 24 6 0 659.13 21.60 24 6 0 680.83 22.60 -24 6 0 642.64 19.70 -24 6 0 616.84 19.60 24 6 0 651.43 20.40 -26 -6 0 303.87 12.50 -26 -6 0 323.07 14.40 26 -6 0 304.57 13.50 26 -6 0 291.37 13.70 -26 6 0 324.97 13.40 26 6 0 322.07 13.70 26 6 0 308.27 13.20 -26 6 0 321.87 13.00 28 -6 0 1.80 3.90 -28 -6 0 -0.20 3.50 -28 -6 0 4.70 3.30 28 -6 0 2.00 4.40 28 6 0 -1.20 3.50 28 6 0 3.60 4.00 -28 6 0 -0.60 3.50 -28 6 0 -1.90 2.40 28 6 0 3.90 4.60 30 -6 0 34.80 5.50 -30 -6 0 33.30 5.60 30 -6 0 33.20 7.00 -30 -6 0 39.50 6.60 -30 6 0 42.00 6.20 30 6 0 22.50 5.60 -30 6 0 36.60 6.00 30 6 0 32.20 5.80 30 6 0 44.60 6.80 1 -7 0 262.57 8.00 -1 -7 0 269.37 8.10 -1 -7 0 264.27 7.90 -1 -7 0 264.67 7.90 1 -7 0 273.47 8.00 1 -7 0 268.37 7.80 1 -7 0 264.27 7.10 -1 -7 0 266.07 6.70 -1 -7 0 262.87 7.80 1 -7 0 261.67 7.70 1 7 0 269.77 7.80 1 7 0 256.67 8.40 1 7 0 262.37 8.10 1 7 0 266.17 8.00 1 7 0 261.37 8.10 -1 7 0 258.37 8.00 -1 7 0 259.57 7.90 -1 7 0 265.47 8.20 -1 7 0 261.37 7.50 -3 -7 0 413.36 11.60 3 -7 0 425.46 11.20 -3 -7 0 430.96 11.30 -3 -7 0 425.96 11.30 3 -7 0 433.86 11.80 3 -7 0 432.96 11.20 3 -7 0 422.76 11.80 -3 -7 0 416.56 11.50 -3 -7 0 428.96 9.90 3 -7 0 422.06 11.50 -3 -7 0 431.46 11.80 3 7 0 435.96 11.60 3 7 0 410.86 12.10 -3 7 0 431.66 12.10 3 7 0 431.76 11.90 3 7 0 425.66 12.00 3 7 0 419.16 11.50 -3 7 0 423.66 11.60 -3 7 0 419.36 11.80 -3 7 0 430.46 10.90 -5 -7 0 52.29 3.60 5 -7 0 52.79 2.40 -5 -7 0 52.19 1.60 5 -7 0 48.70 1.70 5 -7 0 51.49 3.10 -5 -7 0 52.19 2.80 5 -7 0 51.69 3.00 5 -7 0 48.70 2.80 5 -7 0 51.99 3.10 -5 -7 0 50.19 2.50 -5 -7 0 49.80 2.80 -5 7 0 49.20 2.90 5 7 0 52.99 3.00 5 7 0 55.49 2.80 -5 7 0 53.29 2.90 5 7 0 49.00 3.30 5 7 0 50.49 1.90 5 7 0 50.59 3.00 -5 7 0 53.89 3.30 7 -7 0 50.49 3.40 7 -7 0 53.59 2.30 -7 -7 0 51.19 3.40 -7 -7 0 49.80 2.60 -7 -7 0 52.09 3.00 -7 -7 0 52.99 2.90 7 -7 0 53.19 3.10 -7 -7 0 54.99 3.30 7 -7 0 55.59 3.20 -7 -7 0 52.59 1.80 -7 7 0 50.39 3.70 7 7 0 55.19 3.30 7 7 0 53.19 3.30 -7 7 0 49.50 3.20 7 7 0 50.69 3.40 7 7 0 52.19 2.30 9 -7 0 10.70 2.00 -9 -7 0 8.80 2.00 9 -7 0 9.20 1.90 9 -7 0 11.10 1.80 9 -7 0 8.80 1.90 -9 -7 0 8.00 1.50 -9 -7 0 11.20 1.60 -9 -7 0 9.40 1.30 -9 -7 0 7.10 1.90 9 7 0 6.90 1.70 9 7 0 10.40 2.00 9 7 0 8.40 1.70 -9 7 0 9.70 1.60 -9 7 0 6.40 1.70 9 7 0 8.30 1.20 11 -7 0 415.66 12.40 11 -7 0 421.16 13.00 11 -7 0 409.66 11.90 11 -7 0 402.76 9.50 -11 -7 0 397.26 11.90 -11 -7 0 424.46 12.70 -11 -7 0 391.86 10.60 -11 -7 0 415.46 12.50 11 -7 0 399.86 12.30 -11 -7 0 411.16 11.20 -11 7 0 391.66 11.80 -11 7 0 410.86 12.70 -11 7 0 394.96 9.30 11 7 0 389.76 12.30 11 7 0 401.16 12.60 11 7 0 400.06 10.90 -11 7 0 402.36 12.20 11 7 0 397.86 12.30 13 -7 0 830.92 23.20 -13 -7 0 842.22 23.30 -13 -7 0 879.41 22.80 13 -7 0 909.01 24.50 -13 -7 0 854.11 21.20 13 -7 0 885.81 22.80 -13 -7 0 894.01 23.50 13 -7 0 888.11 23.50 -13 -7 0 881.71 21.90 13 7 0 905.41 22.10 13 7 0 874.91 23.50 -13 7 0 889.91 23.40 -13 7 0 870.71 23.70 13 7 0 895.31 23.70 -13 7 0 862.61 22.80 13 7 0 860.91 23.40 -15 -7 0 215.68 8.60 -15 -7 0 204.78 8.40 15 -7 0 190.68 9.30 -15 -7 0 208.88 7.90 15 -7 0 207.28 8.50 -15 -7 0 209.88 6.50 15 -7 0 207.58 7.90 -15 -7 0 208.78 7.20 15 7 0 215.38 9.10 15 7 0 208.98 8.40 15 7 0 197.08 8.30 -15 7 0 205.08 8.10 15 7 0 217.98 7.60 -15 7 0 228.58 8.90 -15 7 0 215.38 8.60 17 -7 0 0.80 1.90 -17 -7 0 0.10 1.40 17 -7 0 -0.50 1.80 17 -7 0 0.30 2.40 -17 -7 0 1.10 1.10 -17 -7 0 4.30 1.70 -17 -7 0 -1.70 1.20 -17 -7 0 1.10 2.40 17 7 0 -3.90 2.00 17 7 0 1.90 2.50 17 7 0 1.40 1.80 -17 7 0 0.10 1.90 -17 7 0 -0.20 2.10 17 7 0 -0.20 1.50 -17 7 0 5.60 2.00 -19 -7 0 4.10 1.90 -19 -7 0 4.60 1.90 -19 -7 0 6.10 2.60 19 -7 0 2.30 1.70 19 -7 0 1.80 2.00 -19 -7 0 5.20 2.70 -19 7 0 5.70 2.50 -19 7 0 0.40 2.60 -19 7 0 3.90 2.60 -19 7 0 5.30 1.90 19 7 0 0.80 2.40 19 7 0 0.00 2.10 19 7 0 5.60 2.80 19 7 0 3.60 1.80 -21 -7 0 193.78 9.40 -21 -7 0 190.98 7.50 -21 -7 0 194.38 9.00 -21 -7 0 199.38 8.80 21 -7 0 188.48 8.70 21 -7 0 204.48 10.10 21 7 0 191.08 8.70 -21 7 0 204.28 9.30 -21 7 0 200.78 8.90 -21 7 0 196.08 9.20 21 7 0 208.88 10.10 21 7 0 189.98 9.50 -21 7 0 205.18 8.90 21 7 0 202.38 10.10 -23 -7 0 287.97 10.20 23 -7 0 301.37 11.90 -23 -7 0 294.47 11.90 23 -7 0 266.17 12.10 23 -7 0 324.27 13.20 -23 -7 0 294.17 11.90 -23 -7 0 301.87 13.10 23 7 0 286.37 11.40 23 7 0 305.37 13.20 -23 7 0 286.37 11.70 23 7 0 295.77 13.10 -23 7 0 321.87 12.50 23 7 0 290.97 12.20 -23 7 0 290.17 11.70 -25 -7 0 70.99 6.00 25 -7 0 60.99 7.00 -25 -7 0 55.59 6.80 25 -7 0 66.59 6.80 25 7 0 65.09 5.90 -25 7 0 73.29 6.50 25 7 0 61.49 6.60 -25 7 0 62.59 7.30 25 7 0 62.99 6.20 -27 -7 0 1.60 2.50 27 -7 0 0.10 3.00 -27 -7 0 0.80 2.80 27 -7 0 -0.80 2.70 27 7 0 -0.60 3.20 -27 7 0 -0.50 2.60 -27 7 0 2.40 2.70 27 7 0 2.90 4.40 27 7 0 0.10 3.90 29 -7 0 0.60 4.30 -29 -7 0 3.00 4.50 -29 -7 0 3.20 3.70 29 -7 0 -1.10 3.30 -29 7 0 3.20 4.00 -29 7 0 3.60 4.10 29 7 0 0.70 4.00 29 7 0 0.50 3.70 0 -8 0 1697.73 40.00 0 -8 0 1730.73 40.40 0 -8 0 1643.64 40.10 0 -8 0 1699.03 38.90 0 -8 0 1716.43 40.10 0 8 0 1690.63 40.50 0 8 0 1752.12 40.50 0 8 0 1748.43 40.40 0 8 0 1663.83 39.70 2 -8 0 274.77 8.50 2 -8 0 269.27 8.00 2 -8 0 285.77 8.40 -2 -8 0 263.17 8.20 -2 -8 0 268.77 8.20 -2 -8 0 271.57 6.80 -2 -8 0 268.37 8.60 2 -8 0 278.37 8.60 2 -8 0 275.97 7.70 -2 8 0 270.37 8.60 2 8 0 257.77 8.60 -2 8 0 273.47 8.70 -2 8 0 274.27 7.90 2 8 0 274.07 8.30 -2 8 0 272.87 8.50 2 8 0 285.57 8.50 2 8 0 266.67 8.80 -4 -8 0 398.36 11.60 4 -8 0 402.76 11.60 -4 -8 0 399.96 9.20 -4 -8 0 387.76 11.20 4 -8 0 393.86 11.10 -4 -8 0 414.06 11.10 -4 -8 0 399.16 11.00 4 -8 0 412.26 11.10 4 -8 0 390.56 11.70 4 -8 0 399.06 10.70 -4 8 0 395.46 11.80 -4 8 0 392.06 11.50 4 8 0 390.06 11.70 -4 8 0 382.96 11.20 4 8 0 399.06 9.20 -4 8 0 400.46 10.40 4 8 0 391.86 11.10 4 8 0 416.46 11.60 4 8 0 398.96 11.60 -6 -8 0 51.89 2.80 6 -8 0 48.20 3.30 -6 -8 0 52.99 3.60 6 -8 0 52.29 3.60 -6 -8 0 55.19 3.00 -6 -8 0 46.00 3.20 6 -8 0 51.99 2.50 6 -8 0 47.30 1.60 6 -8 0 51.59 2.90 -6 -8 0 50.69 1.40 6 8 0 50.29 3.50 -6 8 0 50.29 4.00 -6 8 0 50.69 3.10 6 8 0 52.99 3.60 -6 8 0 47.00 3.00 6 8 0 49.10 2.00 6 8 0 45.90 3.60 6 8 0 48.70 3.10 8 -8 0 224.68 7.40 8 -8 0 223.48 7.90 -8 -8 0 201.38 7.20 8 -8 0 212.48 6.10 -8 -8 0 209.28 6.60 8 -8 0 221.28 7.80 8 -8 0 207.98 7.60 -8 -8 0 219.58 6.90 -8 -8 0 204.88 5.40 -8 -8 0 217.28 8.10 -8 8 0 219.98 7.60 -8 8 0 220.28 8.40 8 8 0 209.58 6.10 8 8 0 207.68 7.60 8 8 0 225.38 8.00 8 8 0 210.68 7.70 -10 -8 0 244.78 7.50 -10 -8 0 249.58 9.20 -10 -8 0 252.37 8.00 10 -8 0 251.27 8.80 10 -8 0 263.17 9.20 -10 -8 0 250.57 8.50 10 -8 0 251.57 6.60 -10 -8 0 246.28 9.00 10 -8 0 247.38 8.40 10 -8 0 247.68 8.70 -10 8 0 253.17 9.50 10 8 0 260.87 9.00 -10 8 0 242.98 8.60 10 8 0 258.97 9.10 10 8 0 259.87 7.50 -10 8 0 251.97 6.90 10 8 0 249.68 9.00 -12 -8 0 1051.09 26.00 12 -8 0 1025.90 26.70 -12 -8 0 1035.10 26.80 12 -8 0 1001.90 26.40 12 -8 0 1022.70 22.90 -12 -8 0 964.20 24.30 -12 -8 0 985.40 26.60 12 -8 0 959.50 25.70 12 -8 0 1012.10 27.20 -12 -8 0 1028.50 25.10 12 8 0 1022.20 26.80 -12 8 0 1046.90 26.60 12 8 0 1014.70 26.90 -12 8 0 1031.80 26.10 12 8 0 1006.90 24.80 12 8 0 1017.20 26.70 -12 8 0 1024.20 27.20 14 -8 0 136.59 6.90 14 -8 0 135.29 7.70 -14 -8 0 148.39 7.10 -14 -8 0 130.69 6.60 -14 -8 0 142.49 5.80 14 -8 0 156.08 7.30 -14 -8 0 146.29 6.30 -14 -8 0 133.09 4.90 14 -8 0 130.69 6.30 14 8 0 144.79 6.80 14 8 0 134.39 5.70 14 8 0 146.29 7.30 -14 8 0 140.99 6.50 14 8 0 139.19 7.00 -14 8 0 144.69 7.00 -14 8 0 139.69 7.40 16 -8 0 15.50 3.40 -16 -8 0 21.10 2.80 16 -8 0 20.80 3.10 -16 -8 0 18.50 3.00 -16 -8 0 19.00 3.20 -16 -8 0 18.20 2.20 16 -8 0 22.10 4.10 16 8 0 18.90 2.60 -16 8 0 16.50 3.20 16 8 0 16.50 3.70 16 8 0 21.70 3.50 -16 8 0 20.20 3.20 -16 8 0 19.40 3.00 16 8 0 20.90 3.20 18 -8 0 26.00 3.20 18 -8 0 23.60 4.80 -18 -8 0 25.90 3.20 -18 -8 0 31.30 3.10 -18 -8 0 26.90 3.70 -18 -8 0 23.40 3.90 18 -8 0 29.10 3.70 18 8 0 28.60 4.10 18 8 0 25.80 3.50 18 8 0 29.50 3.70 -18 8 0 33.10 3.80 -18 8 0 26.40 3.70 -18 8 0 28.20 3.50 18 8 0 34.50 3.60 20 -8 0 6.00 3.30 20 -8 0 4.10 2.00 -20 -8 0 7.00 2.20 -20 -8 0 3.40 2.80 -20 -8 0 7.00 2.20 -20 -8 0 3.90 2.40 20 8 0 1.20 2.50 20 8 0 4.00 2.40 -20 8 0 9.60 3.20 20 8 0 3.50 2.40 20 8 0 7.80 3.10 -20 8 0 8.00 3.10 -20 8 0 3.70 2.80 -20 8 0 5.30 2.10 -22 -8 0 41.90 4.50 22 -8 0 42.80 5.10 -22 -8 0 37.50 3.80 -22 -8 0 37.90 4.60 22 -8 0 31.00 5.00 -22 -8 0 44.80 5.00 22 8 0 48.20 5.20 -22 8 0 53.49 5.20 -22 8 0 40.70 4.60 22 8 0 44.10 5.50 22 8 0 36.40 4.10 -22 8 0 42.60 4.80 -22 8 0 44.90 4.80 22 8 0 33.90 4.50 -24 -8 0 91.09 7.10 24 -8 0 82.99 7.70 24 -8 0 88.59 8.10 -24 -8 0 75.49 6.80 -24 8 0 76.29 6.30 24 8 0 86.89 6.80 24 8 0 65.59 6.00 24 8 0 89.09 7.70 -24 8 0 77.99 6.50 -24 8 0 87.49 6.70 -24 8 0 81.29 6.50 24 8 0 92.09 8.00 26 -8 0 7.00 3.50 -26 -8 0 10.60 4.00 -26 -8 0 19.70 5.10 26 -8 0 6.50 3.50 26 8 0 9.00 3.90 26 8 0 5.00 4.20 -26 8 0 9.90 3.30 26 8 0 12.70 4.00 28 -8 0 49.70 7.20 28 -8 0 59.69 7.00 -28 -8 0 56.09 5.90 -28 -8 0 50.89 6.90 28 8 0 50.49 6.20 28 8 0 51.59 6.20 28 8 0 65.89 8.40 -28 8 0 59.09 6.90 -28 8 0 64.99 6.60 1 -9 0 997.60 23.50 -1 -9 0 957.60 24.50 -1 -9 0 997.80 25.00 1 -9 0 992.50 24.90 -1 -9 0 1003.90 23.00 1 -9 0 981.80 24.80 1 -9 0 927.41 22.00 1 -9 0 994.10 24.50 -1 -9 0 1007.50 24.60 1 9 0 991.20 24.80 -1 9 0 952.90 24.90 1 9 0 997.10 24.40 1 9 0 1008.20 25.10 -1 9 0 991.40 25.00 -1 9 0 987.50 25.00 -1 9 0 1002.10 24.20 1 9 0 993.40 25.10 3 -9 0 1969.50 45.60 3 -9 0 1951.40 46.60 -3 -9 0 1923.01 45.90 3 -9 0 1921.81 46.00 -3 -9 0 1969.80 46.60 -3 -9 0 1992.90 44.00 3 -9 0 1933.81 45.70 -3 -9 0 1999.50 46.20 3 -9 0 1966.30 46.70 -3 9 0 1955.20 46.90 -3 9 0 1970.20 46.50 3 9 0 1996.10 47.00 3 9 0 2009.00 46.40 -3 9 0 1905.71 46.50 3 9 0 1939.91 46.70 3 9 0 1968.90 46.40 -3 9 0 1978.20 45.50 -5 -9 0 39.10 2.80 5 -9 0 33.00 2.50 5 -9 0 34.90 3.20 5 -9 0 39.40 2.50 5 -9 0 37.80 2.70 5 -9 0 37.70 3.20 -5 -9 0 36.90 2.50 -5 -9 0 36.70 3.00 -5 -9 0 37.70 3.20 5 9 0 40.70 3.10 -5 9 0 36.90 3.50 -5 9 0 34.10 3.10 5 9 0 38.70 3.60 5 9 0 34.10 2.90 5 9 0 34.90 1.30 5 9 0 31.10 2.90 -5 9 0 32.00 2.90 7 -9 0 1350.86 33.60 7 -9 0 1362.66 33.70 7 -9 0 1412.36 33.20 -7 -9 0 1353.46 32.50 -7 -9 0 1374.96 32.70 -7 -9 0 1359.86 33.20 7 -9 0 1350.76 31.90 -7 -9 0 1320.97 33.60 -7 9 0 1397.56 34.40 7 9 0 1368.96 34.10 7 9 0 1346.97 33.80 7 9 0 1362.76 32.90 -7 9 0 1383.76 33.60 7 9 0 1347.07 33.80 7 9 0 1328.27 31.20 9 -9 0 1327.77 33.40 -9 -9 0 1323.87 34.00 9 -9 0 1316.57 33.30 -9 -9 0 1347.37 32.90 -9 -9 0 1371.26 32.20 -9 -9 0 1308.57 30.00 9 -9 0 1330.67 32.70 -9 -9 0 1315.07 31.80 9 -9 0 1360.66 33.50 9 -9 0 1314.97 31.00 -9 9 0 1322.37 34.00 9 9 0 1317.67 31.10 9 9 0 1334.37 33.60 9 9 0 1345.07 32.40 9 9 0 1353.26 33.80 9 9 0 1364.46 33.60 -9 9 0 1327.07 33.10 -9 9 0 1342.27 31.30 -9 9 0 1340.57 31.60 11 -9 0 65.59 2.50 -11 -9 0 69.09 4.50 -11 -9 0 68.99 3.40 -11 -9 0 63.69 4.90 11 -9 0 71.29 4.50 -11 -9 0 68.09 3.90 -11 -9 0 63.49 4.40 11 -9 0 72.19 4.90 11 -9 0 64.59 4.60 11 -9 0 75.39 4.40 11 9 0 67.59 4.70 -11 9 0 63.39 5.20 -11 9 0 76.49 4.60 11 9 0 65.99 4.60 11 9 0 65.29 4.40 -11 9 0 58.59 4.50 -11 9 0 61.99 2.60 11 9 0 62.89 3.20 -13 -9 0 474.65 15.20 13 -9 0 517.15 14.70 -13 -9 0 486.85 14.40 -13 -9 0 485.75 15.20 13 -9 0 489.45 15.30 13 -9 0 475.25 15.70 -13 -9 0 468.55 12.80 -13 -9 0 480.35 13.60 13 -9 0 479.75 15.20 13 9 0 483.95 15.40 -13 9 0 470.85 14.40 13 9 0 478.05 13.30 13 9 0 469.45 15.20 -13 9 0 493.55 15.00 13 9 0 511.75 15.90 -13 9 0 496.75 15.70 15 -9 0 125.39 7.10 15 -9 0 143.89 6.80 15 -9 0 145.59 7.30 15 -9 0 126.39 7.40 -15 -9 0 150.88 7.20 -15 -9 0 137.89 7.40 -15 -9 0 142.39 6.80 -15 -9 0 130.29 5.80 15 9 0 132.79 5.80 -15 9 0 135.49 7.80 -15 9 0 140.89 6.90 15 9 0 131.39 6.90 15 9 0 139.19 7.40 -15 9 0 136.29 6.50 15 9 0 135.79 7.50 17 -9 0 297.27 11.90 -17 -9 0 285.77 11.60 -17 -9 0 294.67 9.80 -17 -9 0 289.87 11.40 -17 -9 0 288.77 10.80 17 -9 0 288.27 12.80 17 -9 0 284.07 10.60 -17 9 0 313.37 11.60 -17 9 0 295.47 11.00 17 9 0 298.17 11.50 17 9 0 289.97 12.20 17 9 0 293.97 11.60 -17 9 0 285.87 11.70 17 9 0 291.87 9.80 -19 -9 0 768.22 22.40 19 -9 0 784.92 23.60 -19 -9 0 738.43 22.60 -19 -9 0 774.82 22.00 19 -9 0 740.03 21.80 -19 -9 0 756.42 20.50 19 9 0 744.83 21.00 -19 9 0 809.72 22.50 19 9 0 757.52 22.90 -19 9 0 762.22 22.60 19 9 0 724.43 22.80 -19 9 0 745.03 22.70 19 9 0 744.03 23.50 -21 -9 0 164.88 8.40 -21 -9 0 178.28 8.90 -21 -9 0 159.88 9.30 21 -9 0 160.78 9.00 -21 -9 0 155.58 7.10 21 -9 0 142.79 9.00 -21 9 0 161.38 9.00 -21 9 0 161.88 9.10 -21 9 0 170.18 8.80 21 9 0 155.58 9.40 21 9 0 148.29 8.60 -21 9 0 170.68 8.20 21 9 0 177.68 9.80 -23 -9 0 6.10 3.90 -23 -9 0 5.40 3.20 23 -9 0 6.90 3.80 -23 -9 0 4.50 3.00 23 -9 0 12.10 4.20 23 9 0 -0.60 2.70 23 9 0 7.50 2.80 -23 9 0 8.00 3.00 -23 9 0 6.70 2.70 23 9 0 3.20 3.00 23 9 0 5.60 3.90 -23 9 0 8.30 3.10 -23 9 0 3.10 2.50 25 -9 0 20.00 4.30 25 -9 0 25.20 5.40 -25 -9 0 19.70 4.90 -25 -9 0 25.20 4.60 -25 9 0 28.80 4.50 -25 9 0 31.10 4.50 25 9 0 25.20 4.60 25 9 0 30.40 5.40 25 9 0 24.90 4.30 -25 9 0 17.20 4.10 27 -9 0 12.30 5.20 -27 -9 0 11.30 4.20 -27 -9 0 22.10 4.60 27 -9 0 20.80 4.70 27 9 0 22.00 5.10 -27 9 0 14.00 3.80 27 9 0 16.20 5.10 0 -10 0 2.20 1.30 0 -10 0 5.90 1.80 0 -10 0 3.20 0.90 0 -10 0 3.30 1.40 0 10 0 6.70 2.00 0 10 0 0.90 1.60 0 10 0 2.20 1.40 0 10 0 1.10 1.40 -2 -10 0 16.00 2.00 2 -10 0 12.00 1.60 -2 -10 0 6.20 1.60 -2 -10 0 10.80 2.00 2 -10 0 11.90 1.30 2 -10 0 10.40 2.20 -2 -10 0 8.70 0.90 2 -10 0 12.90 1.80 2 -10 0 13.30 2.20 2 -10 0 8.90 0.70 -2 10 0 7.60 1.80 -2 10 0 8.30 2.10 -2 10 0 12.20 1.80 2 10 0 7.60 1.90 2 10 0 9.90 1.80 2 10 0 10.80 1.90 -2 10 0 9.70 2.10 2 10 0 9.40 2.20 4 -10 0 20.10 2.40 4 -10 0 22.50 2.90 -4 -10 0 27.40 3.00 -4 -10 0 27.60 2.50 -4 -10 0 26.90 2.70 4 -10 0 29.50 3.10 4 -10 0 30.60 2.70 -4 10 0 23.80 2.80 4 10 0 22.70 2.70 -4 10 0 22.20 3.00 4 10 0 24.00 2.90 4 10 0 25.00 2.60 -4 10 0 24.40 2.20 4 10 0 31.40 3.20 -4 10 0 27.20 2.80 -6 -10 0 3.10 1.40 6 -10 0 0.80 1.50 -6 -10 0 2.50 1.10 6 -10 0 0.10 1.80 6 -10 0 0.30 0.90 6 -10 0 1.60 0.80 -6 -10 0 1.10 1.20 -6 -10 0 0.20 1.40 6 10 0 0.30 1.30 -6 10 0 0.80 1.70 6 10 0 1.50 1.80 -6 10 0 1.40 1.50 6 10 0 2.00 1.20 6 10 0 -1.50 1.80 -6 10 0 0.30 1.00 -8 -10 0 29.50 3.20 8 -10 0 31.90 2.90 -8 -10 0 33.80 2.90 8 -10 0 37.20 3.70 8 -10 0 28.80 1.90 8 -10 0 30.30 3.10 -8 -10 0 31.10 2.60 -8 -10 0 34.60 3.30 8 -10 0 29.60 3.00 -8 10 0 33.50 3.60 8 10 0 33.00 2.90 8 10 0 30.80 3.30 8 10 0 27.30 3.50 8 10 0 31.70 1.80 -8 10 0 32.10 3.20 8 10 0 31.40 3.20 10 -10 0 10.20 2.30 10 -10 0 11.90 2.60 -10 -10 0 7.30 2.10 10 -10 0 11.60 2.30 -10 -10 0 10.60 2.00 10 -10 0 10.20 1.90 -10 -10 0 9.50 1.70 -10 -10 0 9.10 1.90 -10 10 0 10.50 1.60 10 10 0 6.30 1.90 10 10 0 8.50 2.20 10 10 0 10.00 2.10 10 10 0 7.80 2.20 -10 10 0 13.40 3.20 -10 10 0 10.70 2.50 10 10 0 8.40 1.30 12 -10 0 51.19 4.60 12 -10 0 58.09 3.90 12 -10 0 57.49 5.00 -12 -10 0 55.99 4.00 -12 -10 0 48.80 3.70 12 -10 0 54.29 4.60 -12 -10 0 59.89 5.10 -12 -10 0 52.19 3.20 -12 10 0 54.19 4.80 -12 10 0 54.19 4.30 12 10 0 53.89 3.80 12 10 0 57.09 3.20 12 10 0 48.80 4.30 12 10 0 58.89 4.60 -12 10 0 52.09 3.90 12 10 0 56.09 4.90 14 -10 0 113.49 5.80 14 -10 0 112.39 6.90 14 -10 0 110.29 6.40 -14 -10 0 112.69 6.80 -14 -10 0 107.59 6.70 -14 -10 0 129.69 6.50 -14 -10 0 118.29 5.50 14 -10 0 134.09 7.30 -14 10 0 111.09 6.30 14 10 0 116.59 5.00 14 10 0 114.99 5.40 14 10 0 116.49 6.70 -14 10 0 119.69 6.80 -14 10 0 126.09 7.60 14 10 0 112.69 6.40 14 10 0 111.99 7.30 -16 -10 0 2.90 1.90 -16 -10 0 7.80 3.00 16 -10 0 5.60 2.90 16 -10 0 3.10 2.60 -16 -10 0 6.10 3.00 16 -10 0 4.20 1.80 -16 -10 0 4.50 2.00 -16 10 0 10.20 2.80 16 10 0 6.10 3.00 16 10 0 5.30 1.80 16 10 0 5.00 2.30 -16 10 0 4.50 2.50 16 10 0 6.40 2.70 -16 10 0 9.50 2.90 18 -10 0 314.27 13.60 -18 -10 0 348.47 12.70 -18 -10 0 355.46 11.50 -18 -10 0 347.67 13.30 -18 -10 0 351.66 13.30 18 -10 0 333.07 13.40 18 10 0 355.36 11.60 18 10 0 373.86 14.10 -18 10 0 350.56 12.60 -18 10 0 362.86 13.10 -18 10 0 360.76 13.90 18 10 0 364.06 14.60 18 10 0 363.86 13.80 -20 -10 0 292.17 12.70 -20 -10 0 292.17 11.70 -20 -10 0 286.17 9.90 -20 -10 0 302.67 11.90 20 -10 0 285.77 11.90 20 -10 0 288.57 13.00 20 10 0 274.47 12.20 20 10 0 292.77 12.90 -20 10 0 295.97 12.30 -20 10 0 276.87 12.50 20 10 0 278.77 12.60 -20 10 0 276.27 11.60 -20 10 0 285.47 11.80 20 10 0 269.37 11.70 22 -10 0 2.50 3.70 -22 -10 0 -0.20 1.90 -22 -10 0 0.10 2.90 -22 -10 0 -3.80 3.20 22 -10 0 -1.40 2.30 22 10 0 1.10 3.20 -22 10 0 1.00 1.90 22 10 0 5.10 2.90 -22 10 0 2.80 2.50 -22 10 0 3.30 2.50 -22 10 0 0.10 3.10 22 10 0 1.90 2.30 24 -10 0 118.39 8.70 24 -10 0 137.79 8.90 -24 -10 0 138.59 8.00 -24 -10 0 133.29 9.70 24 10 0 123.69 9.60 24 10 0 143.89 9.90 -24 10 0 122.89 8.10 -24 10 0 126.29 8.60 -24 10 0 128.39 8.10 -26 -10 0 5.10 4.30 -26 -10 0 5.10 2.90 26 -10 0 1.80 3.20 26 -10 0 0.80 4.40 26 10 0 7.70 4.40 -26 10 0 -1.60 3.70 26 10 0 7.10 4.40 -26 10 0 3.60 2.90 1 -11 0 -1.70 1.10 -1 -11 0 1.90 1.80 -1 -11 0 1.00 1.10 1 -11 0 1.00 0.90 1 -11 0 0.70 1.50 -1 -11 0 3.00 0.80 -1 -11 0 0.70 1.50 1 -11 0 -0.80 1.70 1 11 0 1.90 1.50 1 11 0 0.80 1.30 -1 11 0 1.00 1.80 -1 11 0 1.90 1.40 1 11 0 1.30 1.60 1 11 0 0.70 1.30 -1 11 0 2.50 1.50 -1 11 0 -0.10 1.20 3 -11 0 17.40 2.40 -3 -11 0 20.70 2.40 3 -11 0 14.50 2.40 -3 -11 0 24.90 2.70 3 -11 0 18.70 1.10 -3 -11 0 24.50 3.20 3 -11 0 18.30 2.50 3 -11 0 18.30 2.10 -3 11 0 20.80 2.80 -3 11 0 17.80 2.40 -3 11 0 20.30 2.20 -3 11 0 20.70 3.20 3 11 0 17.00 2.60 3 11 0 21.50 2.60 3 11 0 21.40 3.10 3 11 0 20.20 3.00 5 -11 0 -1.40 1.80 5 -11 0 2.50 1.90 5 -11 0 0.50 1.10 5 -11 0 1.20 1.10 -5 -11 0 -0.20 1.50 -5 -11 0 -1.60 1.10 -5 -11 0 1.20 1.50 5 -11 0 1.60 0.70 5 11 0 3.60 2.10 5 11 0 1.90 1.90 5 11 0 3.10 2.20 5 11 0 2.40 1.40 -5 11 0 1.90 1.70 -5 11 0 -1.80 1.60 -5 11 0 -0.90 1.00 7 -11 0 61.19 4.10 7 -11 0 63.79 3.80 7 -11 0 61.79 4.30 -7 -11 0 62.09 5.00 -7 -11 0 59.89 3.70 7 -11 0 55.69 3.20 7 -11 0 63.09 4.40 -7 -11 0 62.49 3.90 -7 -11 0 60.59 3.90 7 11 0 61.69 4.30 7 11 0 68.99 5.10 7 11 0 54.19 4.10 7 11 0 57.69 4.50 -7 11 0 65.19 5.20 -7 11 0 59.69 4.10 -7 11 0 61.69 4.50 9 -11 0 218.08 9.00 -9 -11 0 239.68 7.70 9 -11 0 225.88 8.90 -9 -11 0 208.68 8.80 -9 -11 0 214.18 8.40 9 -11 0 215.58 8.20 9 -11 0 218.18 9.00 -9 -11 0 224.48 7.90 -9 11 0 210.48 9.10 9 11 0 211.88 9.10 9 11 0 222.48 8.00 9 11 0 215.28 9.00 9 11 0 219.98 9.40 -9 11 0 213.58 8.40 11 -11 0 56.39 3.90 11 -11 0 55.89 5.20 -11 -11 0 56.09 4.00 -11 -11 0 51.09 4.00 11 -11 0 55.69 4.70 11 -11 0 60.29 5.20 -11 -11 0 56.69 3.50 11 11 0 58.69 5.20 11 11 0 53.39 4.10 11 11 0 62.09 4.60 -11 11 0 60.29 5.60 -11 11 0 63.39 4.90 11 11 0 49.90 4.80 -13 -11 0 1.80 2.40 13 -11 0 7.10 2.80 -13 -11 0 4.70 2.00 13 -11 0 3.10 2.10 13 -11 0 0.80 1.40 -13 -11 0 0.90 2.10 13 -11 0 2.80 2.00 -13 11 0 5.10 2.00 13 11 0 4.30 1.90 13 11 0 3.70 2.10 -13 11 0 5.50 2.50 -13 11 0 6.70 2.10 13 11 0 1.70 2.10 13 11 0 3.70 2.60 -15 -11 0 2.90 2.00 -15 -11 0 0.50 1.80 -15 -11 0 4.70 1.90 15 -11 0 2.60 1.60 15 -11 0 2.70 2.80 15 -11 0 -0.20 2.00 15 -11 0 -2.00 1.70 -15 11 0 -0.70 1.70 15 11 0 0.10 2.00 -15 11 0 -1.70 2.90 -15 11 0 2.80 1.90 15 11 0 0.10 2.70 15 11 0 2.40 3.10 15 11 0 0.10 1.30 -17 -11 0 17.90 3.50 -17 -11 0 25.40 4.10 17 -11 0 18.70 3.50 17 -11 0 29.40 4.80 -17 -11 0 22.90 3.10 -17 -11 0 22.40 3.70 -17 11 0 22.30 3.70 -17 11 0 25.40 3.50 17 11 0 23.30 4.40 17 11 0 18.90 3.80 -17 11 0 18.40 3.60 17 11 0 34.40 3.50 17 11 0 26.00 4.50 19 -11 0 75.69 7.20 -19 -11 0 91.79 6.50 -19 -11 0 91.49 5.60 -19 -11 0 101.49 7.70 19 -11 0 96.29 7.10 -19 -11 0 90.99 6.10 -19 11 0 78.89 7.30 19 11 0 95.19 5.50 19 11 0 90.79 7.50 19 11 0 101.59 8.40 -19 11 0 103.39 7.60 -19 11 0 95.19 7.00 19 11 0 95.89 7.00 21 -11 0 123.79 8.60 -21 -11 0 122.19 8.30 21 -11 0 141.39 8.90 -21 -11 0 124.89 8.00 -21 11 0 133.79 9.10 -21 11 0 131.69 8.30 -21 11 0 135.89 8.10 -21 11 0 131.39 7.90 21 11 0 137.59 9.30 21 11 0 150.08 8.90 -23 -11 0 36.90 5.20 23 -11 0 33.20 6.00 -23 -11 0 29.10 4.20 23 -11 0 29.90 4.70 -23 11 0 36.10 5.40 23 11 0 32.70 5.80 -23 11 0 42.40 5.00 -23 11 0 30.70 4.70 23 11 0 34.10 5.70 25 -11 0 2.30 3.10 -25 -11 0 -0.40 2.30 -25 -11 0 2.20 3.10 25 -11 0 3.90 3.30 -25 11 0 -0.50 3.40 25 11 0 5.90 3.80 -25 11 0 -1.00 3.50 25 11 0 5.60 3.30 -25 11 0 -0.50 3.70 -27 -11 0 -0.40 3.10 27 -11 0 5.60 3.80 27 -11 0 3.70 4.90 27 11 0 4.00 4.10 27 11 0 2.90 3.50 -27 11 0 1.30 4.20 -27 11 0 -1.40 4.20 0 -12 0 443.76 11.80 0 -12 0 446.86 13.30 0 -12 0 459.45 14.20 0 -12 0 441.56 13.70 0 12 0 437.06 13.30 0 12 0 441.06 14.00 0 12 0 455.65 14.10 0 12 0 471.45 14.30 2 -12 0 104.69 6.00 -2 -12 0 102.79 5.60 -2 -12 0 101.79 5.50 2 -12 0 100.39 5.00 2 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175.98 9.90 -25 -7 -3 190.78 10.80 -25 -7 -3 162.58 9.50 25 -7 3 158.38 10.70 -25 7 -3 191.78 10.40 25 7 3 180.58 10.40 25 7 3 218.68 11.50 -27 -7 -3 361.46 16.50 -27 -7 -3 321.17 14.40 27 -7 3 356.26 15.50 27 -7 3 368.16 17.00 27 7 3 357.96 15.70 -27 7 -3 378.46 15.20 27 7 3 363.36 14.90 30 -8 -3 23.20 5.20 30 -8 -3 15.60 4.60 -30 -8 3 24.90 5.90 -30 -8 3 26.80 4.60 -30 8 3 35.10 5.10 -30 8 3 28.70 5.10 30 8 -3 33.50 5.40 -28 -8 3 1.80 2.90 28 -8 -3 -2.00 2.80 -28 -8 3 3.70 2.90 28 -8 -3 8.30 4.50 -28 8 3 -1.80 2.80 28 8 -3 -2.00 3.60 -28 8 3 1.50 2.60 28 8 -3 1.00 3.30 26 -8 -3 19.10 4.70 -26 -8 3 10.40 3.60 26 -8 -3 13.10 4.50 -26 -8 3 14.40 4.40 -26 -8 3 8.30 3.60 -26 8 3 13.90 3.60 26 8 -3 14.60 4.20 26 8 -3 15.70 4.50 26 8 -3 13.60 3.90 26 8 -3 11.80 5.40 -24 -8 3 25.00 4.80 24 -8 -3 19.50 3.90 -24 -8 3 22.70 4.00 -24 -8 3 22.30 3.70 24 -8 -3 26.90 5.20 24 8 -3 25.60 3.90 24 8 -3 25.20 4.80 -24 8 3 30.60 4.30 -24 8 3 22.60 3.70 24 8 -3 18.50 4.50 24 8 -3 30.80 5.10 -24 8 3 20.30 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5.80 -16 -8 3 87.79 4.00 -16 8 3 79.29 5.60 16 8 -3 81.89 3.90 -16 8 3 93.89 6.10 16 8 -3 96.79 5.60 16 8 -3 81.59 5.90 -16 8 3 94.89 5.10 16 8 -3 87.49 5.90 16 8 -3 89.49 5.00 -14 -8 3 16.60 2.80 -14 -8 3 12.70 2.50 14 -8 -3 13.40 2.90 -14 -8 3 12.50 1.70 -14 -8 3 12.20 1.90 14 -8 -3 12.90 2.40 14 -8 -3 12.80 2.70 14 -8 -3 13.50 2.00 -14 -8 3 14.80 2.80 14 8 -3 13.10 2.40 14 8 -3 12.80 2.70 -14 8 3 10.70 2.80 14 8 -3 13.40 2.20 -14 8 3 12.60 2.40 -14 8 3 13.40 2.20 14 8 -3 12.10 2.80 14 8 -3 11.00 1.60 12 -8 -3 1040.00 27.00 12 -8 -3 1024.30 25.70 12 -8 -3 1027.60 26.50 -12 -8 3 1021.40 26.90 -12 -8 3 993.60 25.20 12 -8 -3 1021.10 25.10 -12 -8 3 1029.80 26.30 -12 -8 3 1043.60 24.60 -12 -8 3 1058.09 26.20 12 8 -3 1013.50 26.80 -12 8 3 998.60 25.50 -12 8 3 1035.80 26.60 12 8 -3 988.10 24.80 12 8 -3 1054.49 27.60 12 8 -3 1045.10 27.60 -12 8 3 915.71 22.80 -12 8 3 1057.19 23.00 12 8 -3 1004.40 25.10 -10 -8 3 1903.81 44.40 10 -8 -3 1872.91 45.70 10 -8 -3 1910.51 45.20 10 -8 -3 1873.21 43.90 10 -8 -3 1847.62 44.30 -10 -8 3 1870.31 45.10 -10 -8 3 1909.11 43.60 -10 -8 3 1872.21 45.80 -10 -8 3 1888.21 45.00 10 8 -3 1947.71 46.40 10 8 -3 1849.21 43.90 10 8 -3 1860.71 46.40 -10 8 3 1920.71 44.50 10 8 -3 1895.61 44.00 -10 8 3 1854.71 43.00 10 8 -3 1873.21 45.70 -10 8 3 1909.11 45.40 8 -8 -3 134.59 6.00 -8 -8 3 124.59 5.40 -8 -8 3 119.49 5.70 8 -8 -3 122.29 4.40 -8 -8 3 128.79 4.20 -8 -8 3 122.29 5.40 8 -8 -3 123.99 3.90 8 -8 -3 120.79 5.10 8 -8 -3 120.29 4.60 -8 -8 3 127.29 5.00 -8 8 3 120.99 4.80 -8 8 3 119.49 5.70 -8 8 3 120.89 4.20 8 8 -3 127.29 6.10 8 8 -3 124.59 4.50 8 8 -3 128.09 6.40 8 8 -3 118.89 4.80 8 8 -3 131.09 5.90 6 -8 -3 522.25 13.20 6 -8 -3 526.35 14.90 6 -8 -3 528.95 13.10 -6 -8 3 527.15 14.30 -6 -8 3 520.15 13.10 -6 -8 3 517.15 15.10 -6 -8 3 539.75 14.50 6 -8 -3 508.15 13.30 6 -8 -3 539.35 14.20 6 8 -3 527.35 14.10 6 8 -3 532.85 13.30 6 8 -3 517.25 15.20 -6 8 3 523.25 12.50 -6 8 3 528.15 13.40 6 8 -3 528.95 15.00 -6 8 3 527.15 14.00 6 8 -3 520.65 15.60 -6 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55.69 4.10 -8 -8 -3 60.69 3.50 -8 -8 -3 62.79 2.20 8 -8 3 56.49 3.50 -8 -8 -3 63.49 3.70 8 -8 3 63.29 4.30 8 -8 3 64.69 3.50 8 -8 3 59.59 4.60 -8 -8 -3 61.19 4.20 -8 8 -3 66.59 3.90 8 8 3 68.39 4.30 8 8 3 64.19 4.10 8 8 3 67.89 4.00 -8 8 -3 58.89 3.30 -8 8 -3 63.29 3.10 -8 8 -3 68.49 4.70 -8 8 -3 70.59 4.40 10 -8 3 278.67 10.30 10 -8 3 280.17 9.50 10 -8 3 265.17 9.10 -10 -8 -3 268.67 8.80 10 -8 3 277.37 8.50 -10 -8 -3 273.17 10.10 10 -8 3 256.37 6.80 -10 -8 -3 261.37 6.50 -10 -8 -3 254.57 8.70 -10 8 -3 267.67 9.10 -10 8 -3 265.37 7.90 -10 8 -3 268.67 7.60 10 8 3 275.87 9.50 -10 8 -3 280.07 9.50 -10 8 -3 288.57 10.50 10 8 3 273.37 9.50 10 8 3 270.97 9.40 -12 -8 -3 107.39 5.40 12 -8 3 104.29 6.20 12 -8 3 105.29 5.60 12 -8 3 107.59 5.60 -12 -8 -3 106.79 6.00 -12 -8 -3 116.29 6.00 -12 -8 -3 107.79 5.40 12 8 3 119.29 5.80 -12 8 -3 105.99 3.80 -12 8 -3 107.39 5.60 12 8 3 108.09 5.80 -12 8 -3 108.09 5.60 -12 8 -3 107.49 6.70 12 8 3 111.99 6.10 -14 -8 -3 475.25 14.20 14 -8 3 482.45 15.00 -14 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30.00 4.00 17 -9 -3 91.99 6.60 -17 -9 3 91.29 6.40 -17 -9 3 111.69 6.30 -17 -9 3 96.69 5.90 -17 -9 3 89.59 4.40 17 -9 -3 109.89 6.00 -17 -9 3 96.69 4.90 17 9 -3 101.19 7.30 17 9 -3 92.39 6.00 -17 9 3 98.99 6.80 17 9 -3 98.09 5.50 -17 9 3 98.09 6.50 17 9 -3 85.99 7.10 -17 9 3 102.49 5.70 17 9 -3 100.49 4.60 -15 -9 3 66.09 4.50 15 -9 -3 70.99 5.10 -15 -9 3 62.09 3.90 15 -9 -3 61.69 4.80 15 -9 -3 67.19 5.50 -15 -9 3 59.59 4.60 15 -9 -3 68.89 4.10 -15 -9 3 59.69 3.40 -15 -9 3 68.09 4.70 15 9 -3 64.79 4.80 -15 9 3 66.49 4.90 15 9 -3 62.49 3.40 -15 9 3 60.79 5.10 15 9 -3 64.69 4.20 15 9 -3 60.79 5.40 -15 9 3 67.09 4.40 15 9 -3 58.19 5.90 13 -9 -3 27.70 3.50 13 -9 -3 21.50 2.30 -13 -9 3 26.60 2.50 -13 -9 3 22.80 2.20 -13 -9 3 28.80 3.40 13 -9 -3 26.60 3.30 13 -9 -3 27.40 3.00 -13 -9 3 26.20 3.40 -13 -9 3 28.90 3.30 -13 9 3 25.50 3.50 13 9 -3 28.70 3.50 13 9 -3 28.10 2.70 -13 9 3 24.50 2.70 13 9 -3 24.20 2.40 13 9 -3 23.90 3.50 -13 9 3 27.20 3.30 13 9 -3 20.00 3.80 11 -9 -3 4.20 1.40 11 -9 -3 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1 -9 3 666.93 17.40 1 -9 3 698.63 18.10 -1 -9 -3 649.54 16.00 -1 -9 -3 646.44 17.00 1 -9 3 676.13 17.70 -1 -9 -3 661.13 18.20 -1 -9 -3 676.13 17.80 -1 9 -3 655.93 18.40 1 9 3 677.73 17.20 1 9 3 666.13 17.70 1 9 3 689.33 17.80 1 9 3 686.73 17.90 -1 9 -3 674.93 18.60 -1 9 -3 658.93 18.80 3 -9 3 722.63 18.90 3 -9 3 741.73 19.30 -3 -9 -3 723.43 19.30 -3 -9 -3 723.03 18.40 3 -9 3 729.13 18.80 -3 -9 -3 685.53 16.60 -3 -9 -3 704.73 18.80 3 -9 3 691.33 19.40 3 9 3 730.53 19.00 3 9 3 705.43 18.50 -3 9 -3 740.63 20.00 3 9 3 726.03 19.10 -3 9 -3 744.33 19.70 -5 -9 -3 296.57 9.20 5 -9 3 288.47 9.00 -5 -9 -3 284.87 8.80 -5 -9 -3 274.97 7.70 5 -9 3 272.17 9.20 5 -9 3 291.47 9.10 -5 -9 -3 270.77 9.50 5 -9 3 285.37 9.30 5 -9 3 260.77 9.80 5 9 3 285.17 9.10 -5 9 -3 281.17 10.30 -5 9 -3 277.37 8.80 -5 9 -3 282.27 9.70 5 9 3 271.17 6.90 -5 9 -3 277.37 9.20 5 9 3 265.87 9.00 5 9 3 279.47 9.40 7 -9 3 208.68 7.60 7 -9 3 210.28 7.30 -7 -9 -3 201.18 5.80 -7 -9 -3 209.48 7.50 -7 -9 -3 211.28 7.90 -7 -9 -3 195.38 7.20 7 -9 3 200.78 7.70 7 -9 3 207.68 8.30 7 -9 3 207.88 8.00 -7 9 -3 203.88 8.10 7 9 3 200.28 7.80 7 9 3 210.78 8.00 -7 9 -3 202.68 6.90 -7 9 -3 205.28 7.20 7 9 3 201.68 5.80 -7 9 -3 228.28 8.80 7 9 3 215.08 7.90 9 -9 3 248.48 9.10 9 -9 3 242.38 9.80 9 -9 3 240.58 8.50 -9 -9 -3 245.68 8.50 -9 -9 -3 248.08 9.00 9 -9 3 239.88 8.00 9 -9 3 233.68 9.20 -9 -9 -3 239.38 8.30 -9 -9 -3 240.38 6.40 9 9 3 247.58 9.00 -9 9 -3 259.57 8.80 9 9 3 249.38 8.90 -9 9 -3 238.88 7.70 -9 9 -3 240.08 7.50 -9 9 -3 237.78 9.70 9 9 3 253.97 9.00 -9 9 -3 229.38 8.80 11 -9 3 424.56 13.10 11 -9 3 417.26 13.20 -11 -9 -3 433.36 12.80 -11 -9 -3 436.36 12.80 11 -9 3 413.26 14.30 -11 9 -3 416.56 13.50 11 9 3 407.36 13.50 -11 9 -3 425.76 14.60 11 9 3 418.16 13.50 -11 9 -3 417.46 12.90 -11 9 -3 402.06 11.30 11 9 3 424.56 13.50 -13 -9 -3 382.46 12.00 -13 -9 -3 358.26 13.00 13 -9 3 378.46 12.20 -13 -9 -3 396.96 13.10 13 -9 3 382.86 12.70 -13 -9 -3 385.26 12.20 13 -9 3 340.07 13.00 13 -9 3 392.76 14.20 13 9 3 377.46 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53.19 3.30 10 2 -4 54.79 2.90 -10 2 4 51.29 2.20 10 2 -4 50.09 2.80 10 2 -4 54.09 1.40 10 2 -4 57.39 3.10 -8 -2 4 60.29 2.70 -8 -2 4 64.29 2.60 8 -2 -4 62.19 2.90 8 -2 -4 57.89 2.90 8 -2 -4 60.59 2.20 8 -2 -4 61.59 2.20 -8 -2 4 61.39 3.10 -8 -2 4 61.39 1.60 -8 -2 4 58.49 2.90 -8 -2 4 59.29 2.70 -8 2 4 58.79 2.30 -8 2 4 58.39 2.70 8 2 -4 54.59 3.30 8 2 -4 62.79 2.90 8 2 -4 58.39 2.80 8 2 -4 60.49 2.90 -8 2 4 62.99 2.20 -8 2 4 60.89 2.30 8 2 -4 57.29 3.50 -8 2 4 60.39 2.20 -8 2 4 57.99 2.90 8 2 -4 59.89 3.00 8 2 -4 56.99 1.60 -6 -2 4 24.10 0.90 -6 -2 4 20.50 1.40 6 -2 -4 21.30 1.30 -6 -2 4 26.30 2.10 6 -2 -4 22.30 1.60 6 -2 -4 25.90 1.70 6 -2 -4 22.10 1.60 -6 -2 4 21.40 1.50 -6 -2 4 20.20 1.50 -6 -2 4 20.90 1.60 -6 2 4 21.20 1.40 -6 2 4 23.40 1.30 -6 2 4 20.60 1.00 -6 2 4 23.20 1.00 6 2 -4 23.00 1.70 6 2 -4 20.30 1.60 6 2 -4 25.90 1.70 6 2 -4 23.40 1.00 6 2 -4 25.10 2.00 6 2 -4 23.40 2.20 4 -2 -4 443.56 11.20 4 -2 -4 454.85 11.20 4 -2 -4 438.26 11.10 -4 -2 4 475.35 12.10 -4 -2 4 441.86 10.60 -4 -2 4 445.56 11.00 4 -2 -4 441.36 11.30 4 -2 -4 446.26 11.00 -4 -2 4 439.76 11.20 -4 -2 4 471.35 11.00 -4 -2 4 448.06 11.20 4 -2 -4 447.56 10.90 4 2 -4 442.46 11.50 4 2 -4 451.15 12.00 -4 2 4 433.16 10.00 -4 2 4 447.16 11.10 4 2 -4 434.66 11.20 4 2 -4 437.56 11.60 -4 2 4 456.55 10.10 4 2 -4 436.66 11.30 4 2 -4 439.26 10.80 2 -2 -4 445.86 10.90 2 -2 -4 440.46 11.30 -2 -2 4 445.16 11.30 -2 -2 4 450.55 10.30 -2 -2 4 468.75 11.80 -2 -2 4 450.75 11.10 -2 -2 4 434.96 11.20 -2 -2 4 460.75 11.10 2 -2 -4 450.85 11.00 2 -2 -4 452.95 11.00 2 -2 -4 441.16 11.10 2 -2 -4 447.86 11.20 2 2 -4 450.35 11.20 2 2 -4 450.45 11.10 2 2 -4 463.45 11.90 -2 2 4 455.95 11.30 2 2 -4 443.86 11.20 2 2 -4 454.95 11.60 2 2 -4 437.46 10.30 2 2 -4 440.26 11.50 0 -2 4 543.45 12.80 0 -2 4 536.25 13.20 0 -2 4 541.05 13.10 0 -2 4 542.15 12.20 0 -2 -4 538.75 13.00 0 -2 -4 532.95 12.70 0 -2 -4 539.05 13.00 0 -2 4 545.35 13.50 0 -2 4 531.55 13.20 0 2 4 543.85 13.30 0 2 -4 544.55 12.80 0 2 4 535.15 12.30 0 2 -4 486.85 11.90 0 2 -4 538.45 13.10 0 2 4 519.65 12.30 0 2 -4 529.95 13.30 0 2 4 524.35 12.80 0 2 -4 539.55 13.60 0 2 -4 525.65 13.30 2 -2 4 93.99 3.50 2 -2 4 92.29 3.60 -2 -2 -4 96.19 2.90 2 -2 4 100.09 3.60 -2 -2 -4 95.69 3.00 -2 -2 -4 99.09 3.40 2 -2 4 95.79 2.50 2 -2 4 93.49 3.40 -2 -2 -4 96.19 3.30 -2 2 -4 91.49 3.30 2 2 4 94.79 3.30 2 2 4 101.09 3.10 2 2 4 92.89 3.50 -2 2 -4 98.49 3.40 2 2 4 96.09 3.30 -2 2 -4 98.09 3.70 2 2 4 94.19 2.50 -2 2 -4 96.69 2.50 2 2 4 96.79 2.80 2 2 4 91.19 3.10 -2 2 -4 94.09 3.80 -2 2 -4 85.69 2.60 -2 2 -4 98.29 2.90 -4 -2 -4 125.59 4.30 4 -2 4 134.09 4.80 4 -2 4 140.19 4.40 4 -2 4 133.29 4.40 -4 -2 -4 129.79 4.40 4 -2 4 134.39 4.50 -4 -2 -4 133.59 4.30 -4 -2 -4 127.19 4.00 4 2 4 133.09 4.60 -4 2 -4 128.69 4.30 4 2 4 136.29 4.20 -4 2 -4 129.19 4.70 4 2 4 128.59 3.10 4 2 4 127.39 4.20 -4 2 -4 129.09 4.20 -4 2 -4 126.19 3.80 4 2 4 130.79 4.30 4 2 4 127.59 3.50 -4 2 -4 138.59 4.50 4 2 4 127.29 4.30 -4 2 -4 128.79 3.50 -6 -2 -4 377.16 9.30 -6 -2 -4 363.66 8.70 6 -2 4 389.26 10.00 -6 -2 -4 373.36 9.90 -6 -2 -4 372.66 9.80 6 -2 4 378.26 10.60 -6 -2 -4 367.56 10.10 -6 -2 -4 362.46 10.20 6 -2 4 385.56 10.00 6 -2 4 362.06 10.20 -6 2 -4 355.46 10.00 6 2 4 375.26 9.00 -6 2 -4 374.56 10.70 6 2 4 381.16 10.00 6 2 4 371.76 10.10 -6 2 -4 371.06 9.70 -6 2 -4 386.76 10.00 6 2 4 368.36 9.90 -6 2 -4 360.26 9.70 6 2 4 382.36 10.10 8 -2 4 447.66 12.50 -8 -2 -4 440.66 12.20 8 -2 4 442.66 11.50 8 -2 4 438.16 11.70 8 -2 4 431.76 11.30 -8 -2 -4 422.26 11.40 -8 -2 -4 435.96 11.60 -8 -2 -4 427.86 11.80 -8 -2 -4 443.26 11.00 -8 -2 -4 492.25 10.80 8 -2 4 434.06 12.10 8 2 4 420.46 11.60 -8 2 -4 426.26 11.60 8 2 4 430.46 11.90 -8 2 -4 420.06 10.80 8 2 4 435.76 11.80 -8 2 -4 434.06 11.80 -8 2 -4 436.46 11.20 -8 2 -4 428.46 12.30 8 2 4 424.96 10.70 8 2 4 444.16 11.70 10 -2 4 30.40 1.90 -10 -2 -4 30.80 2.50 10 -2 4 33.00 3.10 10 -2 4 31.40 2.20 -10 -2 -4 30.40 2.00 -10 -2 -4 29.20 2.70 10 -2 4 30.40 2.30 -10 -2 -4 29.30 2.40 10 -2 4 27.00 2.70 10 2 4 28.10 1.60 10 2 4 33.90 2.50 10 2 4 30.40 2.60 -10 2 -4 26.30 2.50 -10 2 -4 31.10 2.70 -10 2 -4 32.30 1.90 -10 2 -4 30.60 2.50 10 2 4 30.00 2.20 -10 2 -4 30.30 1.80 10 2 4 30.80 1.90 10 2 4 31.30 2.60 12 -2 4 14.60 1.60 12 -2 4 15.50 2.40 -12 -2 -4 15.90 2.50 -12 -2 -4 18.40 1.80 12 -2 4 15.50 1.70 12 -2 4 14.10 1.90 12 -2 4 15.70 2.10 -12 -2 -4 14.00 1.90 -12 -2 -4 15.30 2.20 -12 2 -4 19.70 2.40 -12 2 -4 17.80 2.60 -12 2 -4 15.90 1.60 12 2 4 14.80 1.50 -12 2 -4 20.10 2.20 -12 2 -4 16.10 1.60 12 2 4 15.90 2.10 12 2 4 15.70 2.00 12 2 4 18.00 1.80 12 2 4 15.50 2.10 12 2 4 15.60 1.90 14 -2 4 0.20 2.00 -14 -2 -4 1.00 1.30 -14 -2 -4 1.70 1.30 14 -2 4 2.40 1.40 -14 -2 -4 -1.00 1.00 -14 -2 -4 2.50 2.00 14 -2 4 -0.30 1.60 14 -2 4 0.00 0.70 14 -2 4 1.10 1.80 14 -2 4 4.00 1.00 -14 2 -4 0.50 1.20 -14 2 -4 1.50 1.00 14 2 4 1.00 1.40 14 2 4 -0.20 1.70 -14 2 -4 0.00 1.60 14 2 4 4.70 2.10 14 2 4 1.60 1.40 14 2 4 1.20 1.20 16 -2 4 25.90 2.30 16 -2 4 23.50 3.80 -16 -2 -4 30.20 2.60 16 -2 4 31.00 3.10 -16 -2 -4 31.40 3.40 -16 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3.40 3.00 -27 -3 4 5.60 2.70 -27 3 4 1.50 2.60 27 3 -4 4.10 3.60 -27 3 4 1.20 2.80 -27 3 4 3.40 3.10 27 3 -4 1.50 2.70 27 3 -4 2.90 2.80 27 3 -4 1.80 3.30 -25 -3 4 595.04 19.00 -25 -3 4 607.04 19.30 25 -3 -4 630.94 20.50 25 -3 -4 600.94 19.70 -25 -3 4 612.34 18.80 25 3 -4 601.44 19.20 25 3 -4 602.34 20.50 25 3 -4 594.54 18.50 25 3 -4 604.04 19.80 -25 3 4 585.64 19.60 -25 3 4 627.84 18.70 -25 3 4 625.24 19.10 -23 -3 4 759.52 21.90 23 -3 -4 762.42 22.80 -23 -3 4 761.22 21.40 -23 -3 4 796.02 22.50 23 -3 -4 747.33 21.40 -23 -3 4 742.13 19.30 23 -3 -4 741.53 22.30 -23 3 4 760.22 21.90 -23 3 4 765.92 22.50 23 3 -4 750.02 22.40 23 3 -4 734.53 21.40 23 3 -4 739.73 23.40 23 3 -4 748.13 22.30 -23 3 4 745.93 21.10 23 3 -4 760.12 22.20 21 -3 -4 128.29 7.20 -21 -3 4 133.39 6.60 21 -3 -4 135.39 7.50 -21 -3 4 148.69 7.40 -21 -3 4 138.69 5.20 21 -3 -4 140.59 6.60 -21 -3 4 133.29 6.30 21 -3 -4 125.99 6.30 21 3 -4 127.39 6.60 -21 3 4 140.09 6.70 -21 3 4 126.39 6.80 -21 3 4 128.69 6.30 -21 3 4 131.79 5.20 21 3 -4 141.89 7.20 21 3 -4 138.79 7.00 21 3 -4 135.09 7.00 21 3 -4 149.39 8.30 -19 -3 4 3.60 1.50 19 -3 -4 6.00 1.90 -19 -3 4 3.50 2.00 19 -3 -4 2.50 2.20 19 -3 -4 3.70 1.70 -19 -3 4 3.00 1.70 19 -3 -4 2.70 1.70 -19 -3 4 2.30 1.00 19 3 -4 3.30 1.70 -19 3 4 2.00 1.30 -19 3 4 3.40 1.50 19 3 -4 3.30 2.00 19 3 -4 2.90 1.90 -19 3 4 2.50 1.10 19 3 -4 2.20 2.00 19 3 -4 4.70 2.10 -19 3 4 4.10 1.80 17 -3 -4 2.40 2.00 17 -3 -4 4.80 1.60 17 -3 -4 1.30 1.40 -17 -3 4 4.70 1.60 -17 -3 4 2.40 0.90 -17 -3 4 2.30 1.30 17 -3 -4 0.20 1.90 -17 -3 4 2.50 1.90 17 3 -4 2.50 1.90 17 3 -4 3.90 1.70 -17 3 4 3.10 1.50 17 3 -4 3.80 2.00 -17 3 4 1.80 1.30 -17 3 4 2.60 1.50 17 3 -4 4.90 2.10 -17 3 4 4.40 1.20 17 3 -4 1.50 1.70 15 -3 -4 747.43 20.50 15 -3 -4 757.42 19.50 -15 -3 4 777.12 18.40 15 -3 -4 790.72 20.50 15 -3 -4 758.12 19.80 15 -3 -4 735.23 17.30 -15 -3 4 790.82 20.50 -15 -3 4 760.82 20.20 -15 -3 4 801.22 20.00 15 3 -4 780.92 20.10 15 3 -4 788.52 20.80 15 3 -4 764.42 20.30 15 3 -4 779.42 20.40 15 3 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-4 11.30 1.50 9 -3 -4 11.50 1.50 -9 -3 4 9.90 1.60 -9 -3 4 12.80 1.40 -9 -3 4 13.10 1.70 -9 -3 4 15.00 1.50 9 -3 -4 11.10 1.60 9 -3 -4 13.80 0.90 -9 -3 4 11.00 1.30 9 3 -4 12.50 1.90 9 3 -4 12.70 2.10 -9 3 4 12.50 1.00 -9 3 4 12.40 1.30 -9 3 4 10.70 1.40 9 3 -4 13.00 1.70 9 3 -4 15.20 1.80 9 3 -4 12.40 0.80 -9 3 4 13.00 1.00 9 3 -4 13.70 1.60 9 3 -4 14.50 1.70 -7 -3 4 98.49 3.60 7 -3 -4 93.79 3.70 -7 -3 4 98.39 3.60 -7 -3 4 101.19 4.10 -7 -3 4 96.79 3.80 7 -3 -4 95.49 2.80 7 -3 -4 101.29 3.90 7 -3 -4 100.49 3.80 7 -3 -4 97.89 3.00 -7 -3 4 99.09 3.50 -7 3 4 101.99 3.40 7 3 -4 97.69 2.90 7 3 -4 95.59 3.90 -7 3 4 97.09 3.00 7 3 -4 97.59 3.90 -7 3 4 96.59 3.00 7 3 -4 106.49 3.90 7 3 -4 95.79 4.40 7 3 -4 100.69 2.50 7 3 -4 103.89 4.80 -7 3 4 94.19 3.10 -5 -3 4 724.73 17.10 -5 -3 4 677.83 16.90 -5 -3 4 698.23 16.50 5 -3 -4 701.63 17.00 5 -3 -4 727.63 16.70 -5 -3 4 687.43 17.10 5 -3 -4 692.43 17.10 5 -3 -4 704.03 17.00 -5 -3 4 714.83 17.90 -5 3 4 704.43 15.90 5 3 -4 680.73 18.00 5 3 -4 689.93 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4 52.69 5.20 -10 -14 -4 58.69 5.70 -10 -14 -4 53.99 5.00 10 -14 4 56.79 5.10 10 14 4 54.89 5.70 10 14 4 49.70 4.60 10 14 4 47.60 5.10 -10 14 -4 50.89 4.60 -10 14 -4 60.79 6.90 -10 14 -4 56.89 5.40 10 14 4 44.70 5.50 -12 -14 -4 6.00 3.00 -12 -14 -4 9.80 3.10 12 -14 4 4.50 2.30 12 -14 4 11.80 3.40 12 -14 4 3.50 2.60 12 -14 4 9.20 3.30 -12 14 -4 1.70 2.60 12 14 4 4.00 3.70 -12 14 -4 4.10 3.40 12 14 4 5.60 2.40 12 14 4 8.40 3.70 12 14 4 8.60 4.00 -12 14 -4 5.30 4.20 14 -14 4 62.89 7.10 -14 -14 -4 65.39 6.10 14 -14 4 71.59 7.50 14 -14 4 60.39 6.00 -14 -14 -4 69.99 5.80 14 14 4 58.49 6.30 -14 14 -4 62.89 7.40 -14 14 -4 64.89 5.80 14 14 4 53.39 5.50 14 14 4 56.29 6.40 -14 14 -4 67.69 6.10 16 -14 4 90.79 8.90 16 -14 4 77.49 7.30 -16 -14 -4 105.79 8.30 -16 -14 -4 94.99 6.40 -16 14 -4 95.09 9.00 16 14 4 112.49 8.80 16 14 4 83.19 8.20 -16 14 -4 86.09 6.30 16 14 4 88.89 6.90 -16 14 -4 109.79 8.60 -18 -14 -4 14.90 4.60 18 -14 4 32.00 6.20 18 -14 4 37.40 6.10 -18 -14 -4 30.10 4.70 18 14 4 27.60 6.20 18 14 4 28.00 4.40 -18 14 -4 22.90 5.00 -18 14 -4 31.80 4.90 18 14 4 25.70 4.80 -20 -14 -4 2.40 3.30 20 -14 4 15.40 6.00 20 -14 4 13.30 4.20 -20 -14 -4 3.20 4.00 20 14 4 14.70 4.50 20 14 4 8.00 3.40 -20 14 -4 12.90 4.40 -20 14 -4 5.90 4.30 23 -15 -4 176.58 11.10 -23 -15 4 171.68 10.60 -23 15 4 157.68 9.10 -23 15 4 179.38 11.30 23 15 -4 167.08 12.50 -23 15 4 182.48 11.90 23 15 -4 173.18 10.90 -21 -15 4 5.60 3.00 21 -15 -4 6.60 3.70 -21 15 4 7.60 4.50 21 15 -4 8.30 4.50 -21 15 4 1.00 3.50 -21 15 4 7.00 3.60 21 15 -4 5.20 4.70 19 -15 -4 121.39 8.80 -19 -15 4 107.69 8.20 -19 -15 4 104.39 7.40 19 -15 -4 102.79 9.10 -19 15 4 117.79 7.20 -19 15 4 123.79 8.60 19 15 -4 102.29 10.20 19 15 -4 118.79 8.90 -19 15 4 129.29 9.90 17 -15 -4 154.48 10.50 -17 -15 4 167.38 9.60 -17 -15 4 144.09 8.20 17 -15 -4 156.48 9.80 -17 15 4 159.08 10.10 -17 15 4 157.38 9.40 17 15 -4 145.49 9.20 -17 15 4 141.79 7.70 17 15 -4 131.29 10.90 -15 -15 4 6.10 3.30 -15 -15 4 5.70 2.80 15 -15 -4 4.80 3.00 15 -15 -4 4.00 2.60 15 15 -4 9.40 2.90 15 15 -4 2.30 2.90 -15 15 4 0.30 2.60 15 15 -4 3.10 3.30 -15 15 4 5.20 3.00 13 -15 -4 88.69 7.80 13 -15 -4 90.39 6.90 -13 -15 4 81.29 5.90 -13 -15 4 83.99 5.90 -13 -15 4 79.89 6.80 13 15 -4 86.79 7.50 13 15 -4 93.59 8.60 13 15 -4 84.39 8.20 13 15 -4 94.29 6.40 -13 15 4 87.29 7.60 -13 15 4 93.49 5.80 -11 -15 4 26.70 3.80 -11 -15 4 34.00 4.50 11 -15 -4 23.70 3.50 11 -15 -4 30.50 4.50 -11 -15 4 18.50 3.70 11 15 -4 18.20 3.70 -11 15 4 19.50 3.50 11 15 -4 20.90 3.60 11 15 -4 23.00 5.10 -11 15 4 25.30 4.70 11 15 -4 27.80 4.70 -9 -15 4 57.99 5.20 -9 -15 4 53.39 4.80 9 -15 -4 49.60 4.60 -9 -15 4 55.89 5.20 9 -15 -4 57.69 5.90 9 15 -4 50.89 4.70 9 15 -4 54.99 6.60 -9 15 4 55.89 5.00 -9 15 4 54.39 5.50 9 15 -4 44.90 5.50 9 15 -4 46.10 5.50 -7 -15 4 64.99 5.50 7 -15 -4 56.89 5.90 7 -15 -4 65.39 4.50 -7 -15 4 63.99 5.40 -7 -15 4 67.69 5.10 -7 15 4 63.89 5.30 7 15 -4 69.99 5.30 7 15 -4 59.69 6.00 -7 15 4 66.19 5.90 7 15 -4 62.49 6.50 7 15 -4 58.59 6.20 -5 -15 4 10.20 3.30 5 -15 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7.30 28 6 -9 47.90 5.90 28 6 -9 39.00 6.70 -28 6 9 48.90 6.30 -28 6 9 51.79 4.80 -26 -6 9 26.80 3.90 -26 -6 9 22.20 3.30 -26 -6 9 20.70 3.60 26 -6 -9 23.50 5.20 26 -6 -9 34.70 5.20 -26 6 9 24.00 4.90 26 6 -9 22.30 4.20 26 6 -9 22.00 6.00 -26 6 9 20.50 3.50 26 6 -9 25.50 4.20 26 6 -9 33.60 5.10 24 -6 -9 68.09 6.30 -24 -6 9 80.39 6.60 -24 -6 9 78.59 5.20 -24 -6 9 79.99 6.20 24 -6 -9 77.99 6.90 -24 -6 9 79.89 6.30 24 6 -9 83.89 8.50 24 6 -9 92.19 7.60 24 6 -9 80.49 6.40 -24 6 9 76.99 6.80 -24 6 9 74.89 5.00 -24 6 9 67.09 6.20 22 -6 -9 7.50 3.30 -22 -6 9 9.70 2.60 -22 -6 9 6.40 2.20 -22 -6 9 5.90 2.00 22 -6 -9 5.80 2.50 -22 -6 9 9.00 2.80 22 6 -9 7.00 4.20 -22 6 9 7.30 2.10 -22 6 9 9.80 3.30 -22 6 9 5.40 2.30 22 6 -9 8.10 2.30 22 6 -9 9.90 3.30 -20 -6 9 168.48 8.00 -20 -6 9 164.38 7.60 -20 -6 9 178.38 7.70 20 -6 -9 159.28 8.60 20 -6 -9 171.38 8.90 -20 -6 9 158.08 7.60 -20 6 9 165.28 8.30 -20 6 9 162.48 6.40 20 6 -9 171.58 8.60 -20 6 9 172.08 8.30 20 6 -9 174.98 10.50 20 6 -9 170.28 7.80 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5.80 -4 2 -10 163.78 6.00 -6 -2 -10 255.17 9.00 6 -2 10 260.77 8.40 -6 -2 -10 256.87 8.80 -6 -2 -10 256.47 8.00 6 -2 10 255.17 8.90 6 -2 10 268.47 9.50 -6 -2 -10 252.97 6.80 6 2 10 256.87 9.00 -6 2 -10 254.07 9.40 -6 2 -10 249.38 8.30 -6 2 -10 276.07 9.50 6 2 10 255.67 8.60 -6 2 -10 251.67 7.30 6 2 10 246.98 7.00 -6 2 -10 256.07 8.90 6 2 10 265.57 8.90 6 2 10 256.17 8.80 -8 -2 -10 82.79 3.10 8 -2 10 82.49 4.80 -8 -2 -10 83.69 4.10 8 -2 10 81.39 4.80 -8 -2 -10 83.79 5.00 -8 -2 -10 90.09 5.40 8 -2 10 80.59 4.30 8 -2 10 90.79 5.90 8 2 10 93.29 5.00 8 2 10 85.09 4.80 8 2 10 85.39 5.00 -8 2 -10 80.89 3.70 8 2 10 86.19 5.20 -8 2 -10 85.89 5.10 -8 2 -10 86.69 4.50 -8 2 -10 96.29 4.80 10 -2 10 82.49 5.50 10 -2 10 91.19 6.30 10 -2 10 84.89 4.30 10 -2 10 90.79 4.90 -10 -2 -10 88.59 4.80 -10 -2 -10 94.29 5.20 -10 -2 -10 90.29 5.40 -10 -2 -10 83.59 5.20 10 -2 10 93.59 5.10 -10 2 -10 89.89 4.90 -10 2 -10 93.39 4.40 10 2 10 89.99 5.40 -10 2 -10 98.19 5.70 -10 2 -10 92.59 4.90 10 2 10 89.09 5.20 10 2 10 101.99 5.40 10 2 10 98.19 5.70 -12 -2 -10 59.19 5.00 12 -2 10 50.99 4.90 -12 -2 -10 61.19 4.60 -12 -2 -10 56.09 4.10 12 -2 10 54.89 4.20 12 -2 10 55.39 4.70 12 -2 10 55.99 4.10 -12 -2 -10 54.19 4.20 12 2 10 56.89 4.40 12 2 10 58.89 4.60 12 2 10 57.89 5.00 -12 2 -10 54.49 4.50 -12 2 -10 59.59 4.40 -12 2 -10 56.09 3.90 -12 2 -10 52.29 4.90 12 2 10 57.19 4.90 -14 -2 -10 133.29 6.90 -14 -2 -10 127.19 7.10 -14 -2 -10 129.79 7.00 14 -2 10 138.19 6.60 -14 -2 -10 138.89 6.40 14 -2 10 137.49 8.30 14 -2 10 144.29 6.70 14 -2 10 140.19 7.50 -14 2 -10 127.89 7.80 -14 2 -10 128.59 6.50 14 2 10 139.29 6.80 14 2 10 128.29 7.50 -14 2 -10 139.59 7.10 14 2 10 133.59 7.50 -14 2 -10 137.39 6.50 14 2 10 131.19 7.00 -16 -2 -10 1.30 2.40 16 -2 10 2.30 2.30 16 -2 10 0.90 1.90 16 -2 10 4.00 2.60 -16 -2 -10 -0.70 3.00 16 -2 10 1.10 2.30 16 2 10 -2.40 1.30 -16 2 -10 1.40 2.20 -16 2 -10 1.30 1.90 16 2 10 3.40 2.20 16 2 10 -1.00 2.00 -16 2 -10 0.50 2.00 16 2 10 1.60 2.10 -18 -2 -10 1.10 2.40 18 -2 10 0.50 1.80 18 -2 10 -0.20 2.30 -18 -2 -10 -1.70 1.60 18 -2 10 -0.20 3.70 18 -2 10 0.90 2.80 18 2 10 2.40 3.00 18 2 10 2.20 3.20 18 2 10 0.70 3.20 18 2 10 1.10 2.40 -18 2 -10 -3.60 2.50 -18 2 -10 0.50 3.30 -20 -2 -10 -0.10 3.50 20 -2 10 2.70 2.80 20 -2 10 1.20 2.00 20 -2 10 6.60 4.70 20 2 10 3.90 2.90 20 2 10 -0.60 3.30 20 2 10 5.40 3.50 -20 2 -10 -2.70 3.60 -20 2 -10 0.20 2.10 22 -2 10 27.80 5.50 22 -2 10 32.60 6.30 -22 -2 -10 17.40 4.10 22 2 10 28.90 5.50 22 2 10 21.20 5.00 22 2 10 28.50 5.70 -22 2 -10 22.90 5.60 -33 -3 10 150.48 9.10 33 -3 -10 124.79 11.10 33 -3 -10 136.89 11.20 -33 -3 10 165.88 11.00 -33 -3 10 159.08 9.10 -33 3 10 161.08 9.60 -33 3 10 154.58 11.00 33 3 -10 128.09 11.30 -31 -3 10 41.50 5.20 -31 -3 10 44.60 5.80 31 -3 -10 50.19 7.20 -31 -3 10 39.00 5.90 31 -3 -10 29.90 6.10 31 3 -10 35.20 5.70 -31 3 10 34.90 5.10 -31 3 10 47.30 5.50 31 3 -10 37.60 5.40 29 -3 -10 291.77 13.60 -29 -3 10 306.67 12.70 -29 -3 10 287.57 12.00 29 -3 -10 308.37 14.80 -29 -3 10 306.97 13.20 -29 3 10 341.87 14.10 29 3 -10 285.47 13.70 -29 3 10 311.97 12.00 29 3 -10 298.07 13.90 27 -3 -10 85.99 8.20 27 -3 -10 91.09 7.90 -27 -3 10 86.39 6.80 -27 -3 10 87.39 6.60 -27 -3 10 85.49 6.40 -27 3 10 88.99 5.50 27 3 -10 82.09 7.30 27 3 -10 87.99 7.70 -27 3 10 87.59 7.20 -25 -3 10 94.19 6.70 -25 -3 10 81.59 6.50 -25 -3 10 86.59 6.10 25 -3 -10 83.99 7.30 25 -3 -10 93.19 7.90 -25 -3 10 98.69 5.80 25 3 -10 96.09 7.60 -25 3 10 88.49 5.50 25 3 -10 104.69 8.30 -25 3 10 88.29 6.10 25 3 -10 77.09 5.60 -25 3 10 79.79 6.00 23 -3 -10 177.28 9.30 -23 -3 10 175.48 7.90 -23 -3 10 185.18 8.10 23 -3 -10 190.18 9.30 -23 -3 10 177.98 8.50 -23 -3 10 193.68 8.40 23 3 -10 182.78 8.90 23 3 -10 185.48 9.30 -23 3 10 182.88 9.10 23 3 -10 182.88 8.80 23 3 -10 207.58 9.50 -23 3 10 174.78 8.50 -23 3 10 195.28 7.60 -21 -3 10 116.79 6.30 21 -3 -10 108.29 7.50 -21 -3 10 118.69 6.10 21 -3 -10 114.39 6.80 -21 -3 10 114.09 6.70 -21 -3 10 103.39 5.70 21 3 -10 109.49 7.00 -21 3 10 112.49 6.70 -21 3 10 114.99 6.70 21 3 -10 100.49 6.40 21 3 -10 105.99 6.80 -21 3 10 105.29 4.90 21 3 -10 106.49 6.50 21 3 -10 104.59 7.20 19 -3 -10 1207.38 29.20 -19 -3 10 1208.38 30.60 -19 -3 10 1205.28 31.60 19 -3 -10 1214.18 32.30 -19 -3 10 1237.58 30.40 19 -3 -10 1206.38 32.60 -19 -3 10 1209.38 30.90 19 3 -10 1153.28 31.60 19 3 -10 1200.78 32.30 19 3 -10 1213.98 32.30 -19 3 10 1213.38 31.30 19 3 -10 1190.98 30.60 19 3 -10 1178.48 32.40 -19 3 10 1211.18 31.50 -19 3 10 1209.98 29.30 -17 -3 10 710.03 18.80 17 -3 -10 707.73 20.50 -17 -3 10 693.13 18.80 -17 -3 10 711.43 19.40 17 -3 -10 716.63 18.20 17 -3 -10 709.43 20.70 -17 -3 10 725.93 20.00 17 3 -10 664.53 20.10 -17 3 10 715.13 19.80 17 3 -10 697.43 21.00 -17 3 10 690.03 19.70 17 3 -10 723.13 20.70 -17 3 10 680.53 17.10 17 3 -10 717.33 20.60 -17 3 10 698.33 17.70 17 3 -10 702.93 19.10 -15 -3 10 2.80 1.10 -15 -3 10 1.30 1.20 -15 -3 10 1.60 1.80 -15 -3 10 1.40 1.00 15 -3 -10 2.80 1.20 15 -3 -10 2.20 1.60 15 -3 -10 3.10 2.30 15 -3 -10 3.00 1.20 15 3 -10 4.10 2.30 15 3 -10 1.20 1.50 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42.10 9 -3 -10 1746.53 42.50 9 -3 -10 1718.53 41.20 -9 -3 10 1782.02 41.30 -9 3 10 1707.23 39.00 9 3 -10 1714.63 42.40 9 3 -10 1625.84 38.70 -9 3 10 1738.53 41.00 9 3 -10 1793.62 42.60 9 3 -10 1738.53 43.10 -9 3 10 1756.62 38.90 9 3 -10 1687.73 40.70 7 -3 -10 1161.78 29.20 7 -3 -10 1171.78 28.10 7 -3 -10 1159.88 29.70 -7 -3 10 1172.58 28.80 -7 -3 10 1158.18 28.70 7 -3 -10 1140.99 28.30 -7 -3 10 1152.98 28.00 -7 -3 10 1204.98 28.40 7 -3 -10 1167.38 28.00 7 -3 -10 1177.28 28.80 7 3 -10 1174.18 28.10 -7 3 10 1172.78 26.20 -7 3 10 1187.28 28.10 7 3 -10 1155.98 30.30 -7 3 10 1149.98 26.30 7 3 -10 1145.09 29.70 7 3 -10 1149.78 29.60 7 3 -10 1109.49 26.70 5 -3 -10 94.99 4.00 5 -3 -10 99.99 4.10 5 -3 -10 105.69 5.40 -5 -3 10 95.19 4.20 -5 -3 10 102.39 4.20 5 -3 -10 89.19 4.40 -5 -3 10 93.19 4.70 -5 -3 10 98.19 4.60 -5 -3 10 96.99 2.60 5 -3 -10 96.09 4.60 5 3 -10 103.59 4.30 5 3 -10 91.99 3.50 5 3 -10 105.19 4.10 5 3 -10 93.09 4.90 -5 3 10 97.29 2.90 5 3 -10 99.99 5.40 -5 3 10 96.29 2.80 -5 3 10 103.19 4.00 3 -3 -10 2.10 1.00 -3 -3 10 2.50 1.30 -3 -3 10 2.40 1.10 3 -3 -10 2.20 1.20 3 -3 -10 0.70 0.80 -3 -3 10 2.20 1.00 -3 -3 10 1.50 1.00 3 -3 -10 3.30 1.40 -3 3 10 1.30 0.80 3 3 -10 2.50 0.90 3 3 -10 4.70 1.80 3 3 -10 2.90 1.40 -3 3 10 1.70 0.50 -3 3 10 2.90 1.30 3 3 -10 4.80 1.20 -3 3 10 5.10 1.20 3 3 -10 2.30 0.90 -3 3 10 1.40 0.60 -1 -3 10 192.78 6.00 -1 -3 10 200.88 4.70 -1 -3 10 213.48 7.50 1 -3 -10 206.98 6.00 -1 -3 10 206.68 7.10 1 -3 -10 207.88 7.10 -1 -3 10 200.48 4.70 -1 -3 10 197.58 7.00 1 -3 -10 211.18 7.10 1 3 -10 198.18 6.60 1 3 -10 191.08 6.50 -1 3 10 198.38 6.10 -1 3 10 194.68 5.70 -1 3 10 203.78 5.70 -1 3 10 202.88 7.00 -1 3 10 191.68 5.60 1 3 -10 199.08 7.70 1 3 -10 192.38 7.90 1 3 -10 192.08 6.00 1 -3 10 612.54 16.80 -1 -3 -10 625.14 16.80 1 -3 10 628.54 17.40 1 -3 10 639.24 16.90 -1 -3 -10 625.14 15.40 -1 -3 -10 634.94 17.00 -1 3 -10 632.24 16.50 1 3 10 621.74 16.90 1 3 10 624.54 16.60 1 3 10 633.54 15.70 -1 3 -10 632.04 17.90 -1 3 -10 620.54 17.30 1 3 10 628.94 14.90 1 3 10 646.54 15.60 -1 3 -10 623.24 15.30 -3 -3 -10 206.58 7.40 3 -3 10 197.78 7.10 3 -3 10 188.48 6.90 -3 -3 -10 183.78 5.70 3 -3 10 200.38 7.90 -3 -3 -10 187.78 7.00 -3 -3 -10 190.48 5.60 -3 3 -10 193.58 6.80 -3 3 -10 208.78 8.10 3 3 10 182.88 4.70 3 3 10 187.38 6.80 3 3 10 184.78 6.90 -3 3 -10 184.28 7.20 3 3 10 193.48 7.00 3 3 10 194.28 6.40 3 3 10 198.48 4.70 -3 3 -10 195.38 5.20 3 3 10 182.08 5.50 -5 -3 -10 12.20 1.40 5 -3 10 12.90 2.10 5 -3 10 7.20 2.00 -5 -3 -10 12.30 2.00 5 -3 10 13.90 2.40 -5 -3 -10 9.90 1.90 -5 -3 -10 11.40 1.30 -5 3 -10 16.30 2.50 -5 3 -10 8.60 1.90 5 3 10 10.70 1.10 5 3 10 11.90 1.90 -5 3 -10 11.20 1.10 5 3 10 9.60 2.30 -5 3 -10 10.50 2.10 5 3 10 11.50 2.00 5 3 10 11.60 2.20 -7 -3 -10 57.39 4.20 -7 -3 -10 50.09 3.80 -7 -3 -10 48.40 3.10 7 -3 10 49.10 4.20 -7 -3 -10 50.59 2.50 7 -3 10 54.19 3.80 7 -3 10 47.00 3.70 -7 3 -10 53.59 4.10 7 3 10 39.60 3.60 7 3 10 49.80 3.60 -7 3 -10 48.90 3.80 7 3 10 50.99 3.70 7 3 10 51.69 3.70 -7 3 -10 56.39 2.60 -7 3 -10 49.30 3.80 9 -3 10 1.70 1.30 -9 -3 -10 0.00 0.80 9 -3 10 0.70 1.40 -9 -3 -10 0.10 2.20 9 -3 10 1.00 1.20 -9 -3 -10 0.10 1.30 9 -3 10 1.00 1.90 -9 -3 -10 4.00 2.10 9 3 10 -0.80 1.20 9 3 10 0.80 1.30 9 3 10 -1.00 1.40 -9 3 -10 1.80 1.10 -9 3 -10 -0.70 1.70 9 3 10 1.80 1.80 -9 3 -10 0.10 1.20 11 -3 10 28.30 4.30 -11 -3 -10 28.40 3.50 -11 -3 -10 29.10 3.40 -11 -3 -10 34.30 3.20 -11 -3 -10 35.10 3.60 11 -3 10 33.50 3.60 11 -3 10 30.20 3.80 11 -3 10 28.20 3.10 11 3 10 28.80 3.70 -11 3 -10 32.40 3.40 11 3 10 24.70 3.40 -11 3 -10 26.40 3.00 -11 3 -10 33.80 4.10 11 3 10 29.70 3.50 11 3 10 28.50 3.20 -11 3 -10 30.30 2.70 13 -3 10 20.10 4.20 13 -3 10 8.70 2.40 -13 -3 -10 16.80 3.20 13 -3 10 14.80 2.80 -13 -3 -10 14.10 3.00 13 -3 10 12.40 3.30 -13 -3 -10 13.90 2.90 13 3 10 13.70 2.70 13 3 10 12.50 3.00 -13 3 -10 7.40 2.60 13 3 10 12.30 3.20 -13 3 -10 19.60 3.70 13 3 10 17.40 2.70 -13 3 -10 13.90 2.60 -15 -3 -10 278.47 11.10 15 -3 10 265.47 11.30 15 -3 10 266.97 12.40 -15 -3 -10 266.57 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12 10 128.09 5.20 10 -12 -10 315.47 12.60 -10 -12 10 322.07 10.90 -10 -12 10 309.97 11.70 -10 -12 10 324.77 12.30 -10 -12 10 320.27 10.50 10 -12 -10 323.67 11.70 -10 -12 10 309.67 12.50 10 12 -10 318.47 11.40 -10 12 10 316.67 9.60 10 12 -10 298.57 13.70 10 12 -10 331.27 13.60 10 12 -10 314.77 12.30 -10 12 10 317.67 12.00 -10 12 10 322.97 10.20 -8 -12 10 4.30 2.80 -8 -12 10 6.10 2.30 -8 -12 10 0.40 2.60 8 -12 -10 4.10 2.40 -8 -12 10 1.40 2.00 -8 -12 10 6.20 2.40 8 -12 -10 4.00 2.00 8 12 -10 6.30 2.60 8 12 -10 0.20 2.20 -8 12 10 1.60 1.70 -8 12 10 3.60 2.00 -8 12 10 4.30 1.50 8 12 -10 5.20 2.40 8 12 -10 -2.50 2.90 -8 12 10 2.80 1.30 -6 -12 10 34.70 4.70 6 -12 -10 30.70 4.40 6 -12 -10 36.70 3.50 -6 -12 10 35.80 4.00 -6 -12 10 31.80 3.30 -6 -12 10 37.70 3.60 6 12 -10 33.50 3.90 6 12 -10 28.80 4.90 6 12 -10 30.40 4.30 -6 12 10 36.80 2.90 -6 12 10 29.90 3.70 6 12 -10 37.00 4.70 -6 12 10 39.00 3.20 -6 12 10 33.50 3.20 -4 -12 10 4.80 2.80 4 -12 -10 10.10 3.20 4 -12 -10 5.70 2.80 -4 -12 10 10.20 3.40 -4 -12 10 6.50 2.10 -4 -12 10 7.20 2.60 -4 12 10 5.10 2.00 4 12 -10 4.70 2.50 -4 12 10 2.60 1.80 4 12 -10 8.70 3.60 4 12 -10 4.90 2.50 -4 12 10 4.80 2.20 -4 12 10 9.60 2.40 4 12 -10 6.10 2.40 2 -12 -10 381.56 13.60 -2 -12 10 404.26 13.40 2 -12 -10 376.56 13.80 -2 -12 10 378.66 13.80 -2 -12 10 404.96 12.10 -2 -12 10 389.86 14.00 2 12 -10 391.16 15.20 2 12 -10 390.86 14.50 -2 12 10 380.76 11.80 2 12 -10 402.36 14.30 -2 12 10 383.06 12.00 -2 12 10 384.76 12.60 2 12 -10 405.46 14.40 0 -12 -10 175.68 8.70 0 -12 -10 162.98 8.40 0 -12 10 177.08 8.80 0 -12 10 165.38 8.70 0 -12 10 171.18 6.90 0 -12 10 173.48 8.00 0 12 -10 164.08 8.70 0 12 -10 171.38 8.50 0 12 -10 174.98 9.60 0 12 10 179.08 7.20 0 12 -10 191.38 9.30 0 12 10 160.98 7.50 0 12 10 161.28 7.50 2 -12 10 39.40 4.50 -2 -12 -10 40.80 4.60 2 -12 10 37.20 4.50 -2 -12 -10 44.60 5.00 2 -12 10 44.00 4.50 2 12 10 36.70 3.70 -2 12 -10 45.10 5.00 -2 12 -10 40.10 4.50 2 12 10 55.39 4.40 -2 12 -10 35.20 4.40 2 12 10 40.90 4.50 -2 12 -10 35.00 4.70 4 -12 10 2.00 3.00 4 -12 10 4.00 2.30 -4 -12 -10 0.20 2.10 4 -12 10 9.30 3.60 -4 -12 -10 -1.90 1.50 -4 12 -10 2.40 2.70 -4 12 -10 1.80 2.70 4 12 10 0.00 1.80 4 12 10 1.00 2.10 -4 12 -10 5.10 3.10 4 12 10 1.80 1.80 -4 12 -10 -1.40 2.40 -6 -12 -10 38.70 4.70 6 -12 10 51.39 6.10 6 -12 10 45.80 5.40 -6 -12 -10 44.40 5.20 6 -12 10 45.50 5.60 6 12 10 37.00 4.70 -6 12 -10 52.49 5.20 6 12 10 54.79 4.90 -6 12 -10 30.30 5.50 6 12 10 45.90 4.60 -6 12 -10 47.50 5.00 -6 12 -10 45.40 4.90 8 -12 10 182.98 10.30 -8 -12 -10 178.58 8.60 8 -12 10 198.68 10.40 -8 -12 -10 185.98 9.60 8 -12 10 188.98 9.40 8 12 10 168.58 8.20 8 12 10 184.18 9.10 -8 12 -10 182.88 11.00 -8 12 -10 186.38 10.00 8 12 10 183.48 8.90 -10 -12 -10 144.59 8.80 10 -12 10 141.39 9.10 10 -12 10 150.68 8.90 10 -12 10 139.59 8.90 -10 -12 -10 135.69 8.00 10 12 10 140.49 8.20 -10 12 -10 146.29 8.40 10 12 10 147.49 7.90 -10 12 -10 157.08 9.80 -12 -12 -10 5.40 3.00 12 -12 10 9.30 3.40 12 -12 10 2.00 2.90 -12 -12 -10 3.90 2.60 -12 12 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20.20 4.70 17 -13 -10 121.39 9.20 -17 -13 10 118.89 8.00 17 -13 -10 108.59 7.40 -17 -13 10 110.29 7.40 -17 13 10 109.79 5.40 17 13 -10 97.09 7.80 -17 13 10 105.09 7.60 -17 13 10 112.79 8.80 -15 -13 10 285.57 11.50 -15 -13 10 282.17 11.10 -15 -13 10 280.27 12.00 15 -13 -10 279.47 12.60 15 -13 -10 281.07 12.00 15 13 -10 319.57 12.60 -15 13 10 261.27 11.30 -15 13 10 275.17 9.20 13 -13 -10 11.70 3.40 13 -13 -10 11.80 2.80 -13 -13 10 12.30 2.20 -13 -13 10 13.70 3.00 -13 -13 10 13.20 3.60 -13 -13 10 8.10 2.70 -13 13 10 10.90 3.50 13 13 -10 4.00 3.40 -13 13 10 9.00 1.80 -11 -13 10 143.89 8.40 11 -13 -10 154.58 8.80 11 -13 -10 147.79 7.50 -11 -13 10 150.88 7.60 -11 -13 10 163.48 7.00 -11 -13 10 161.08 9.00 -11 -13 10 153.18 7.90 11 13 -10 170.48 8.10 -11 13 10 149.99 6.00 -11 13 10 158.08 8.50 11 13 -10 172.98 9.30 11 13 -10 165.28 9.60 -9 -13 10 177.78 8.70 9 -13 -10 174.08 8.20 9 -13 -10 191.48 10.10 -9 -13 10 189.18 8.90 -9 -13 10 192.68 8.00 9 13 -10 198.88 9.10 -9 13 10 187.28 7.00 -9 13 10 194.78 7.40 9 13 -10 206.48 10.00 -9 13 10 199.18 9.40 9 13 -10 203.78 10.20 9 13 -10 199.38 11.20 7 -13 -10 46.10 5.40 -7 -13 10 45.20 4.20 -7 -13 10 41.70 4.80 -7 -13 10 46.50 4.20 7 -13 -10 50.69 4.20 -7 -13 10 42.10 5.10 -7 13 10 39.10 3.80 7 13 -10 40.80 4.80 7 13 -10 46.30 5.60 -7 13 10 45.80 5.00 -7 13 10 47.60 3.40 7 13 -10 48.30 5.00 7 13 -10 44.00 5.40 -5 -13 10 542.35 17.50 -5 -13 10 525.85 17.00 5 -13 -10 525.75 17.90 -5 -13 10 544.45 15.90 -5 -13 10 538.55 16.10 -5 13 10 524.55 15.10 5 13 -10 536.85 17.50 5 13 -10 568.84 18.70 5 13 -10 523.25 19.00 5 13 -10 522.25 17.50 -5 13 10 498.15 15.80 -5 13 10 538.95 17.30 -5 13 10 527.85 15.00 3 -13 -10 233.68 10.30 -3 -13 10 251.67 10.70 3 -13 -10 223.78 10.70 -3 -13 10 241.88 11.10 -3 -13 10 235.08 9.80 -3 -13 10 243.38 9.00 3 13 -10 254.47 11.20 3 13 -10 239.78 11.30 3 13 -10 235.58 10.40 -3 13 10 239.28 8.70 -3 13 10 227.78 8.50 3 13 -10 253.47 11.30 -3 13 10 228.28 9.40 -3 13 10 239.88 10.50 -1 -13 10 153.38 8.60 1 -13 -10 156.78 8.70 -1 -13 10 159.78 8.20 -1 -13 10 166.88 9.20 1 -13 -10 139.89 8.30 -1 13 10 162.58 7.50 -1 13 10 158.78 7.90 1 13 -10 172.38 9.30 1 13 -10 153.38 9.10 -1 13 10 149.59 7.30 1 13 -10 152.58 8.60 -1 13 10 156.58 7.00 1 13 -10 158.18 8.40 1 -13 10 522.65 17.70 1 -13 10 513.75 17.00 1 -13 10 515.35 16.60 -1 -13 -10 493.05 16.80 -1 -13 -10 498.75 16.50 1 13 10 510.35 15.80 -1 13 -10 484.55 17.50 1 13 10 498.55 16.10 -1 13 -10 495.95 17.50 -1 13 -10 530.45 17.40 -1 13 -10 524.55 17.70 1 13 10 493.95 15.20 -3 -13 -10 17.60 4.10 3 -13 10 21.60 4.50 3 -13 10 23.60 4.30 -3 -13 -10 19.70 3.40 3 -13 10 26.20 4.30 3 13 10 17.70 3.60 3 13 10 12.90 3.30 -3 13 -10 16.50 3.80 -3 13 -10 15.40 3.80 -3 13 -10 14.20 3.80 -3 13 -10 22.90 3.80 3 13 10 19.40 3.20 -5 -13 -10 385.06 14.00 5 -13 10 384.16 15.20 -5 -13 -10 365.96 14.10 5 -13 10 403.76 14.90 5 -13 10 374.56 14.60 -5 13 -10 397.66 15.60 -5 13 -10 375.46 13.50 5 13 10 373.16 14.10 5 13 10 376.46 13.20 5 13 10 389.86 13.60 -5 13 -10 394.56 15.10 -7 -13 -10 288.37 12.00 7 -13 10 305.07 12.60 7 -13 10 292.77 13.40 -7 -13 -10 294.07 12.30 7 -13 10 302.37 13.20 7 13 10 284.87 11.80 -7 13 -10 284.87 12.40 -7 13 -10 304.47 14.30 7 13 10 307.57 11.80 9 -13 10 25.90 5.10 9 -13 10 18.10 4.20 -9 -13 -10 24.50 4.00 9 -13 10 31.10 5.60 -9 -13 -10 25.80 4.30 -9 13 -10 23.80 4.90 9 13 10 21.90 4.70 -9 13 -10 20.10 4.70 9 13 10 16.10 3.40 11 -13 10 359.36 14.70 -11 -13 -10 343.47 13.70 -11 -13 -10 356.76 14.10 11 -13 10 376.46 16.10 11 -13 10 366.96 15.50 11 13 10 357.46 14.90 -11 13 -10 392.96 16.40 11 13 10 372.06 14.20 -11 13 -10 398.96 15.60 13 -13 10 131.59 10.30 -13 -13 -10 133.49 8.60 -13 -13 -10 136.19 9.20 13 -13 10 136.79 8.90 13 13 10 114.59 9.10 -13 13 -10 148.79 11.30 -13 13 -10 142.09 8.90 13 13 10 138.99 9.20 -15 -13 -10 50.69 5.70 15 -13 10 51.89 7.70 15 -13 10 56.19 7.10 15 13 10 37.20 6.30 -15 13 -10 48.50 6.60 15 13 10 45.80 5.70 -15 13 -10 44.90 5.80 -24 -14 10 85.99 7.40 24 -14 -10 63.69 8.10 -24 14 10 58.99 5.30 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78.69 6.00 -12 -14 10 76.19 6.40 12 14 -10 77.89 8.90 -12 14 10 80.19 6.20 -12 14 10 78.49 4.50 12 14 -10 87.49 6.20 12 14 -10 83.49 7.20 10 -14 -10 37.10 5.50 -10 -14 10 36.40 4.30 -10 -14 10 29.60 4.00 10 -14 -10 44.20 4.50 -10 -14 10 44.00 4.80 10 14 -10 37.50 5.30 -10 14 10 36.10 3.20 10 14 -10 32.40 5.50 -10 14 10 36.30 4.90 10 14 -10 34.50 4.60 10 14 -10 28.30 4.20 -8 -14 10 36.30 3.80 -8 -14 10 44.90 4.40 -8 -14 10 41.90 4.90 8 -14 -10 34.30 5.20 -8 -14 10 32.90 4.30 8 14 -10 33.30 4.40 8 14 -10 48.80 5.30 -8 14 10 37.80 3.30 8 14 -10 30.80 4.80 -8 14 10 42.50 5.30 8 14 -10 31.10 5.30 -6 -14 10 9.80 3.40 -6 -14 10 6.70 2.60 -6 -14 10 3.80 3.50 -6 -14 10 7.40 2.20 6 -14 -10 4.50 3.50 -6 14 10 6.20 2.50 6 14 -10 9.20 3.20 -6 14 10 10.80 3.60 -6 14 10 9.20 2.10 6 14 -10 12.40 3.60 6 14 -10 11.30 3.80 6 14 -10 11.10 4.30 -4 -14 10 239.88 9.40 -4 -14 10 220.18 10.40 4 -14 -10 233.28 11.30 -4 -14 10 245.48 9.40 -4 -14 10 230.98 10.30 -4 14 10 242.68 10.40 4 14 -10 242.68 10.80 -4 14 10 232.18 9.60 4 14 -10 239.88 11.70 4 14 -10 254.17 11.80 -4 14 10 238.88 8.90 4 14 -10 236.18 11.30 -4 14 10 240.28 8.90 -2 -14 10 231.38 10.60 2 -14 -10 208.98 10.20 -2 -14 10 225.88 9.30 -2 -14 10 236.28 10.70 2 14 -10 225.08 10.40 -2 14 10 213.58 9.10 -2 14 10 212.18 10.30 -2 14 10 208.98 8.70 2 14 -10 236.58 11.80 2 14 -10 223.88 10.40 2 14 -10 224.88 10.50 -2 14 10 220.48 8.70 0 -14 -10 32.80 4.40 0 -14 10 31.90 4.30 0 -14 10 42.70 4.30 0 -14 10 36.10 5.50 0 -14 -10 34.80 4.80 0 14 -10 39.80 5.50 0 14 10 33.80 3.90 0 14 10 33.70 4.40 0 14 10 34.60 3.80 0 14 -10 36.00 5.20 0 14 -10 35.90 5.20 0 14 10 36.50 4.20 0 14 -10 45.00 5.20 2 -14 10 45.00 5.80 -2 -14 -10 61.29 6.00 -2 -14 -10 53.89 5.90 2 -14 10 50.49 5.60 2 -14 10 52.29 5.10 2 14 10 43.20 4.50 -2 14 -10 54.39 5.90 2 14 10 49.70 5.50 2 14 10 47.60 4.60 2 14 10 46.40 4.50 -2 14 -10 46.80 5.60 -2 14 -10 44.70 5.10 -2 14 -10 58.19 5.90 -4 -14 -10 35.40 5.00 4 -14 10 34.70 4.60 4 -14 10 39.10 5.20 4 -14 10 36.80 5.00 -4 -14 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16 -4 -14 10.90 2.40 16 -4 -14 8.70 2.80 16 4 -14 11.00 3.00 16 4 -14 12.90 3.80 -16 4 14 15.20 1.50 16 4 -14 11.90 3.00 -16 4 14 10.10 2.60 -16 4 14 13.00 2.50 14 -4 -14 208.98 8.10 -14 -4 14 221.58 9.00 -14 -4 14 228.48 8.90 14 -4 -14 199.98 9.80 14 -4 -14 211.08 9.80 -14 -4 14 209.68 6.90 14 -4 -14 214.98 8.30 -14 -4 14 216.98 7.90 -14 4 14 211.08 8.60 14 4 -14 217.58 10.70 -14 4 14 214.98 6.00 14 4 -14 196.58 9.50 14 4 -14 207.18 10.00 -14 4 14 214.08 8.10 -12 -4 14 32.50 3.40 12 -4 -14 40.30 3.80 -12 -4 14 32.90 3.60 12 -4 -14 33.90 4.00 -12 -4 14 40.00 3.50 -12 -4 14 34.30 2.20 -12 -4 14 35.20 3.60 12 -4 -14 45.00 3.80 12 -4 -14 42.90 5.00 -12 4 14 34.50 1.60 12 4 -14 31.70 4.20 -12 4 14 33.40 3.40 12 4 -14 36.30 4.20 -12 4 14 34.50 3.30 12 4 -14 33.10 4.70 10 -4 -14 206.58 7.40 -10 -4 14 196.78 8.30 -10 -4 14 191.68 7.40 -10 -4 14 188.18 7.40 10 -4 -14 196.68 7.90 10 -4 -14 199.88 8.00 10 -4 -14 198.18 9.40 -10 -4 14 204.58 8.10 -10 4 14 199.08 7.50 -10 4 14 197.58 7.30 10 4 -14 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12.40 15 5 14 270.27 13.30 17 -5 14 84.19 7.80 -17 -5 -14 84.89 7.60 17 -5 14 89.09 9.20 17 5 14 82.69 7.40 17 5 14 72.79 7.80 -17 5 -14 86.39 8.00 -30 -6 14 18.50 4.60 30 -6 -14 22.00 6.10 -30 -6 14 16.10 3.70 -30 -6 14 16.50 3.50 30 -6 -14 20.60 5.70 30 6 -14 22.60 5.00 -30 6 14 19.10 3.50 -30 6 14 19.20 4.20 -28 -6 14 18.50 3.60 28 -6 -14 25.30 5.90 -28 -6 14 20.40 4.40 28 -6 -14 18.60 4.60 28 6 -14 21.20 4.10 -28 6 14 14.60 3.00 -28 6 14 19.50 4.10 28 6 -14 15.50 5.50 26 -6 -14 69.49 8.00 26 -6 -14 60.29 7.60 -26 -6 14 63.29 5.70 -26 -6 14 71.69 6.00 -26 -6 14 65.59 5.80 26 6 -14 64.69 7.00 -26 6 14 74.79 7.10 26 6 -14 78.29 7.60 -26 6 14 70.49 4.70 26 6 -14 62.79 7.30 -24 -6 14 837.22 24.70 24 -6 -14 808.22 26.40 -24 -6 14 832.82 23.80 24 -6 -14 803.72 26.50 -24 -6 14 804.72 23.00 -24 6 14 862.91 25.30 24 6 -14 834.22 26.00 24 6 -14 819.72 26.30 24 6 -14 795.62 26.70 -24 6 14 812.12 21.50 -22 -6 14 918.11 25.70 22 -6 -14 871.31 27.40 22 -6 -14 869.71 27.50 -22 -6 14 879.51 24.70 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532.15 15.90 14 -6 -14 544.45 17.80 14 -6 -14 525.55 15.30 -14 -6 14 535.85 16.50 -14 -6 14 534.75 16.80 -14 -6 14 531.95 16.50 14 6 -14 546.95 17.80 -14 6 14 567.94 16.70 14 6 -14 524.55 18.10 -14 6 14 527.05 16.50 -14 6 14 545.25 15.00 14 6 -14 548.95 19.20 12 -6 -14 843.62 24.40 12 -6 -14 836.92 22.00 12 -6 -14 827.12 23.80 -12 -6 14 830.72 23.00 -12 -6 14 813.72 23.00 -12 -6 14 809.32 22.20 -12 -6 14 823.22 22.80 -12 6 14 850.51 21.70 -12 6 14 833.72 22.60 12 6 -14 819.12 25.60 12 6 -14 829.62 24.60 12 6 -14 782.32 24.10 -10 -6 14 46.10 3.70 -10 -6 14 46.40 4.20 -10 -6 14 42.30 3.80 10 -6 -14 51.69 5.10 10 -6 -14 50.99 4.90 10 -6 -14 50.19 4.20 10 -6 -14 44.70 3.70 10 -6 -14 50.09 4.30 -10 -6 14 41.50 4.30 -10 6 14 46.90 3.50 10 6 -14 47.90 5.30 -10 6 14 47.10 3.70 10 6 -14 45.00 5.20 -8 -6 14 98.39 6.10 -8 -6 14 95.89 5.50 -8 -6 14 96.89 6.00 -8 -6 14 92.39 5.10 8 -6 -14 93.39 5.30 8 -6 -14 95.29 5.40 8 -6 -14 97.39 5.10 8 6 -14 80.39 4.40 8 6 -14 90.19 7.20 -8 6 14 100.09 5.00 8 6 -14 98.79 6.90 -8 6 14 96.39 5.10 8 6 -14 90.99 5.20 -6 -6 14 126.79 6.40 6 -6 -14 130.69 5.90 6 -6 -14 124.69 6.30 -6 -6 14 133.69 7.00 6 -6 -14 132.09 6.20 -6 -6 14 121.19 5.70 -6 -6 14 125.49 6.30 -6 6 14 119.59 5.30 -6 6 14 128.69 5.50 6 6 -14 125.19 7.70 -6 6 14 123.19 5.80 6 6 -14 140.99 8.10 -6 6 14 127.59 5.90 -6 6 14 125.69 3.50 6 6 -14 124.99 6.00 6 6 -14 127.29 5.10 -4 -6 14 14.20 2.20 -4 -6 14 12.80 2.70 4 -6 -14 10.20 2.60 -4 -6 14 11.20 2.60 4 -6 -14 14.20 2.20 -4 -6 14 9.00 2.30 4 -6 -14 13.60 2.80 4 6 -14 12.70 3.60 -4 6 14 11.60 1.70 -4 6 14 11.20 2.20 -4 6 14 12.60 2.00 4 6 -14 8.90 2.00 4 6 -14 9.50 2.60 -4 6 14 12.90 1.30 4 6 -14 9.60 2.80 4 6 -14 11.20 2.40 -4 6 14 12.10 2.10 -2 -6 14 84.39 5.60 2 -6 -14 71.69 5.20 2 -6 -14 81.79 5.00 -2 -6 14 76.49 5.10 -2 -6 14 80.59 6.00 2 -6 -14 80.29 4.30 -2 6 14 77.49 5.30 2 6 -14 81.99 4.80 -2 6 14 71.79 3.70 2 6 -14 76.19 6.10 2 6 -14 80.89 6.70 -2 6 14 76.99 3.50 2 6 -14 76.79 5.70 2 6 -14 75.99 4.80 -2 6 14 71.09 3.70 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598.44 19.60 -11 -11 21 571.64 20.80 -11 -11 21 559.04 20.30 11 11 -21 618.74 23.90 -9 -11 21 68.79 6.70 9 -11 -21 71.99 7.40 -9 -11 21 81.79 7.80 -9 -11 21 75.49 7.00 9 -11 -21 86.59 7.00 -9 11 21 77.09 6.70 9 11 -21 84.29 9.40 -7 -11 21 29.80 5.50 -7 -11 21 32.60 6.00 7 -11 -21 33.40 5.70 7 -11 -21 35.10 5.50 -7 -11 21 41.30 6.40 -7 11 21 33.70 5.20 7 11 -21 37.30 6.60 -5 -11 21 70.19 7.30 24 0 -22 50.49 7.20 -24 0 22 38.50 6.10 24 0 -22 45.60 6.10 -22 0 22 38.60 5.10 22 0 -22 32.60 5.40 -22 0 22 26.10 5.50 22 0 -22 26.90 6.70 20 0 -22 103.79 10.00 20 0 -22 95.89 8.30 -20 0 22 113.39 7.80 -20 0 22 87.59 8.10 18 0 -22 132.89 8.80 -18 0 22 130.79 8.50 -18 0 22 115.59 7.80 -16 0 22 80.39 6.90 16 0 -22 75.49 7.70 -16 0 22 76.09 7.00 14 0 -22 34.50 6.00 -14 0 22 39.50 5.10 -14 0 22 30.90 5.40 12 0 -22 11.20 3.70 -12 0 22 10.10 3.70 -12 0 22 16.60 4.50 -10 0 22 21.40 4.10 -10 0 22 19.00 4.80 -10 0 22 12.40 2.20 10 0 -22 19.50 4.30 -8 0 22 208.88 11.10 8 0 -22 214.58 11.40 -8 0 22 206.18 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5.20 13 -9 -22 32.30 4.40 13 9 -22 27.50 6.00 -13 9 22 21.00 4.40 11 -9 -22 196.68 10.50 -11 -9 22 180.18 10.90 -11 -9 22 175.18 10.00 11 9 -22 183.38 12.10 9 -9 -22 136.89 9.20 -9 -9 22 138.99 10.00 -9 -9 22 148.79 8.80 -9 -9 22 140.59 8.90 9 -9 -22 144.09 9.50 9 9 -22 121.19 10.50 -7 -9 22 4.40 4.40 -7 -9 22 9.40 3.30 7 -9 -22 1.20 2.90 7 -9 -22 -3.10 3.30 -7 -9 22 3.40 3.00 -7 9 22 1.50 3.70 7 9 -22 2.50 5.30 -5 -9 22 27.80 4.70 -5 -9 22 30.80 5.10 -5 -9 22 29.10 5.30 5 -9 -22 32.10 4.90 5 -9 -22 34.70 5.80 5 9 -22 28.80 5.90 -5 9 22 26.20 5.20 -12 -10 22 282.97 12.90 12 -10 -22 293.07 12.30 -12 -10 22 268.67 12.80 12 10 -22 271.37 15.10 -10 -10 22 319.47 14.50 -10 -10 22 317.27 14.20 -10 -10 22 308.47 14.40 10 -10 -22 285.07 12.80 10 10 -22 340.17 16.50 22 0 -23 0.30 3.80 -22 0 23 3.10 4.20 22 0 -23 1.80 5.10 -22 0 23 -3.20 2.70 20 0 -23 0.70 4.00 -20 0 23 4.00 3.90 -20 0 23 2.50 3.00 -18 0 23 -1.10 3.60 -18 0 23 -1.30 4.00 18 0 -23 0.20 2.60 -16 0 23 4.80 3.70 -16 0 23 4.40 3.10 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2.80 -15 -1 23 1.80 3.90 15 -1 -23 3.40 4.10 -15 -1 23 -2.00 3.40 -15 1 23 0.10 3.30 15 1 -23 -1.20 4.10 -15 1 23 4.90 4.10 -13 -1 23 49.60 5.30 -13 -1 23 45.90 6.10 13 -1 -23 47.30 6.20 -13 1 23 44.90 6.20 13 1 -23 49.30 7.10 -13 1 23 45.70 4.90 -11 -1 23 69.19 5.90 -11 -1 23 57.29 4.40 -11 -1 23 64.49 6.40 11 -1 -23 61.29 7.50 11 1 -23 62.79 7.10 -11 1 23 67.69 7.00 -11 1 23 60.09 5.40 -9 -1 23 5.10 2.30 -9 -1 23 4.50 2.60 9 -1 -23 -1.00 4.20 -9 -1 23 5.60 3.20 9 1 -23 3.60 3.70 -9 1 23 0.30 3.90 7 -1 -23 45.30 7.00 -7 -1 23 57.59 6.60 -7 -1 23 39.40 4.00 -7 1 23 44.30 6.00 7 1 -23 49.60 6.80 -5 -1 23 25.70 3.70 5 -1 -23 19.70 5.50 -5 -1 23 34.10 5.80 5 1 -23 25.80 6.10 -5 1 23 26.40 4.40 -3 -1 23 78.59 7.90 3 -1 -23 78.29 7.60 -3 -1 23 62.09 5.40 -3 1 23 74.99 5.40 3 1 -23 76.09 8.20 -3 1 23 70.89 7.40 1 -1 -23 189.28 12.10 -1 -1 23 178.58 10.40 1 -1 -23 143.59 9.10 -1 -1 23 160.68 8.10 1 1 -23 178.68 10.90 -22 -2 23 189.28 10.90 22 -2 -23 225.48 14.50 22 -2 -23 198.88 10.70 -22 2 23 215.28 11.50 -22 2 23 185.68 11.40 22 2 -23 218.38 13.20 22 2 -23 199.18 12.90 -20 -2 23 4.00 4.40 -20 -2 23 6.50 3.10 -20 -2 23 9.80 4.80 20 -2 -23 16.10 3.80 -20 2 23 15.90 3.80 -20 2 23 10.70 4.90 20 2 -23 10.10 4.30 -18 -2 23 338.57 14.50 -18 -2 23 339.87 14.90 18 -2 -23 334.47 14.90 -18 -2 23 301.97 11.30 18 2 -23 330.67 16.20 -18 2 23 337.77 15.00 -18 2 23 345.67 14.30 -16 -2 23 66.39 7.20 16 -2 -23 108.29 8.70 -16 -2 23 77.99 7.30 -16 -2 23 85.99 5.50 -16 2 23 86.09 8.10 16 2 -23 68.09 7.60 -16 2 23 103.79 7.90 14 -2 -23 175.18 10.00 -14 -2 23 146.19 9.20 -14 -2 23 151.48 8.70 -14 -2 23 138.09 7.00 -14 2 23 159.58 8.50 -14 2 23 159.28 9.40 14 2 -23 176.48 11.80 12 -2 -23 390.06 16.20 -12 -2 23 370.16 14.00 -12 -2 23 365.06 15.30 -12 -2 23 323.27 11.90 -12 2 23 382.56 14.80 -12 2 23 351.16 13.40 12 2 -23 380.26 17.20 -10 -2 23 27.70 4.00 10 -2 -23 36.50 6.20 -10 -2 23 50.39 6.60 -10 -2 23 35.80 4.00 -10 2 23 38.20 5.60 10 2 -23 39.20 6.90 -8 -2 23 137.19 9.60 -8 -2 23 113.79 7.20 -8 -2 23 108.99 6.50 8 -2 -23 142.19 10.60 8 2 -23 119.69 10.40 -8 2 23 111.79 8.70 6 -2 -23 139.29 10.40 -6 -2 23 131.09 9.80 -6 -2 23 132.69 7.30 6 2 -23 141.69 11.30 -6 2 23 129.89 9.40 4 -2 -23 3.40 4.60 -4 -2 23 3.80 2.10 -4 -2 23 5.40 4.50 -4 2 23 10.50 3.40 4 2 -23 9.90 4.00 2 -2 -23 120.09 9.20 -2 -2 23 141.09 9.20 -2 -2 23 125.39 7.70 2 -2 -23 128.69 9.00 -2 2 23 137.59 10.10 2 2 -23 135.39 10.60 -2 2 23 144.39 9.80 0 -2 -23 69.49 7.30 0 -2 23 59.59 7.30 0 -2 -23 53.79 6.60 0 -2 23 51.39 5.60 0 2 23 56.99 6.20 0 2 -23 75.69 8.60 0 2 23 49.20 6.00 0 2 23 52.39 4.90 -21 -3 23 168.18 9.90 21 -3 -23 151.18 12.50 -21 -3 23 161.78 10.90 -21 -3 23 161.98 8.10 21 -3 -23 181.78 10.30 -21 3 23 165.48 11.00 -21 3 23 172.88 10.50 21 3 -23 169.78 12.30 -19 -3 23 139.69 7.40 -19 -3 23 130.69 10.00 19 -3 -23 131.59 9.50 -19 -3 23 134.99 9.00 19 3 -23 127.99 10.30 -19 3 23 156.48 10.40 -19 3 23 145.79 9.40 17 -3 -23 50.49 5.70 -17 -3 23 43.70 6.00 -17 -3 23 40.10 4.00 -17 -3 23 37.70 5.30 17 3 -23 33.20 6.70 -17 3 23 36.70 6.10 -17 3 23 44.20 5.10 15 -3 -23 1.30 3.80 -15 -3 23 0.00 2.20 -15 -3 23 -4.40 3.40 -15 -3 23 0.50 3.80 -15 3 23 -1.70 3.10 -15 3 23 1.90 2.90 15 3 -23 -1.30 3.40 -13 -3 23 -1.20 2.40 -13 -3 23 4.50 2.50 13 -3 -23 0.40 2.70 -13 -3 23 2.20 3.90 -13 3 23 2.70 2.90 13 3 -23 1.70 5.20 -13 3 23 1.00 2.20 -11 -3 23 52.19 5.80 -11 -3 23 59.39 5.10 11 -3 -23 58.39 6.90 -11 -3 23 66.09 6.10 -11 3 23 63.89 6.20 11 3 -23 65.39 7.80 -9 -3 23 147.39 7.90 9 -3 -23 174.28 11.00 -9 -3 23 165.78 8.70 -9 -3 23 169.98 9.70 -9 3 23 154.08 9.20 9 3 -23 156.48 11.80 -7 -3 23 85.69 6.40 -7 -3 23 92.59 7.70 7 -3 -23 101.49 9.10 -7 3 23 92.99 7.90 7 3 -23 87.99 8.50 -5 -3 23 2.80 2.80 -5 -3 23 2.60 3.10 5 -3 -23 5.00 4.70 5 3 -23 -0.20 3.30 -5 3 23 -0.30 2.50 3 -3 -23 38.20 5.20 -3 -3 23 31.50 4.40 3 -3 -23 34.80 6.20 -3 -3 23 41.90 6.40 3 3 -23 34.20 6.80 -3 3 23 41.00 5.90 -3 3 23 36.90 6.30 1 -3 -23 15.30 5.50 -1 -3 23 12.40 3.70 -1 -3 23 16.00 5.30 1 -3 -23 16.90 4.50 1 3 -23 5.50 3.70 -1 3 23 5.30 3.20 -1 3 23 13.30 4.00 -22 -4 23 7.30 4.70 -22 -4 23 8.20 3.10 -22 4 23 5.40 4.50 20 -4 -23 3.00 3.50 -20 -4 23 4.10 3.20 -20 -4 23 7.50 2.90 -20 -4 23 1.40 4.20 20 4 -23 13.10 5.60 -20 4 23 2.90 3.90 -20 4 23 9.60 4.70 -18 -4 23 16.30 3.90 -18 -4 23 17.00 4.00 -18 -4 23 15.30 3.40 18 -4 -23 23.80 4.80 18 4 -23 30.70 5.60 -18 4 23 26.70 5.40 -18 4 23 20.10 4.60 16 -4 -23 3.50 2.80 -16 -4 23 -0.20 2.50 -16 -4 23 -0.80 2.50 -16 -4 23 -1.40 3.90 16 4 -23 2.50 5.00 -16 4 23 1.50 3.30 -16 4 23 -0.90 2.70 -14 -4 23 24.80 5.00 14 -4 -23 23.20 5.00 -14 -4 23 22.30 3.70 -14 -4 23 22.10 4.40 -14 4 23 25.50 4.40 14 4 -23 20.60 6.30 -14 4 23 9.30 4.30 -12 -4 23 4.50 3.10 -12 -4 23 5.90 2.20 12 -4 -23 0.90 2.80 -12 -4 23 2.60 2.80 -12 4 23 5.10 4.10 12 4 -23 8.10 4.20 10 -4 -23 51.69 6.60 -10 -4 23 37.50 4.80 -10 -4 23 48.10 6.40 -10 -4 23 42.90 4.70 -10 4 23 47.30 5.50 10 4 -23 50.49 6.70 -8 -4 23 88.99 6.70 8 -4 -23 105.79 8.90 -8 -4 23 92.99 8.40 -8 -4 23 114.29 7.30 -8 4 23 96.59 8.10 8 4 -23 95.69 8.80 -6 -4 23 -1.90 2.70 6 -4 -23 -1.30 4.30 -6 -4 23 2.70 2.50 -6 -4 23 4.30 4.20 -6 4 23 3.60 3.80 6 4 -23 1.70 5.00 4 -4 -23 29.00 4.90 -4 -4 23 24.40 5.60 4 -4 -23 20.30 5.70 -4 -4 23 23.50 4.20 -4 4 23 26.80 4.70 4 4 -23 24.00 6.30 -4 4 23 30.60 5.20 -2 -4 23 0.50 3.00 2 -4 -23 -2.90 3.30 2 -4 -23 -4.60 4.20 -2 -4 23 -0.20 4.50 2 4 -23 -2.80 4.80 -2 4 23 -1.70 3.70 -2 4 23 0.90 4.20 21 -5 -23 66.89 8.60 -21 -5 23 61.79 6.50 -21 5 23 58.99 6.60 -19 -5 23 24.30 4.50 -19 -5 23 29.00 5.60 -19 -5 23 25.30 4.10 19 -5 -23 29.30 5.10 -19 5 23 19.30 5.30 -19 5 23 20.40 4.00 19 5 -23 26.00 6.70 -17 -5 23 31.30 5.60 -17 -5 23 30.90 5.50 17 -5 -23 27.10 5.10 -17 -5 23 31.40 4.40 17 5 -23 23.30 5.50 -17 5 23 25.10 4.10 -17 5 23 32.70 5.10 15 -5 -23 25.80 5.30 -15 -5 23 17.60 4.20 -15 -5 23 30.80 4.40 -15 -5 23 22.20 4.20 15 5 -23 18.30 5.10 -15 5 23 24.00 5.20 -15 5 23 21.10 4.30 13 -5 -23 7.00 4.40 -13 -5 23 7.40 4.40 -13 -5 23 7.20 4.30 -13 -5 23 9.20 2.60 13 5 -23 8.20 5.60 -13 5 23 13.00 4.60 -11 -5 23 80.99 7.70 -11 -5 23 81.79 6.70 -11 -5 23 80.29 6.40 11 -5 -23 83.89 7.70 -11 5 23 79.59 6.70 11 5 -23 80.59 9.00 -9 -5 23 14.50 4.90 9 -5 -23 19.70 5.20 -9 -5 23 12.50 3.40 -9 -5 23 18.20 3.30 -9 5 23 7.80 4.10 9 5 -23 13.80 5.70 -7 -5 23 73.39 7.00 7 -5 -23 68.79 7.70 -7 -5 23 82.19 6.70 -7 -5 23 68.09 6.30 7 5 -23 87.29 8.70 -7 5 23 84.89 7.40 5 -5 -23 106.09 8.30 -5 -5 23 111.29 8.50 5 -5 -23 126.69 8.90 -5 -5 23 101.19 7.00 -5 -5 23 101.99 7.20 -5 5 23 103.49 8.80 5 5 -23 111.79 9.50 -5 5 23 110.69 10.30 -3 -5 23 -0.20 3.10 -3 -5 23 4.50 3.50 3 -5 -23 -0.10 2.40 3 -5 -23 -0.50 3.00 -3 5 23 -0.50 2.90 3 5 -23 2.00 5.00 -18 -6 23 129.19 8.90 -18 -6 23 121.29 8.00 -18 -6 23 136.09 10.10 18 -6 -23 147.89 9.20 -18 6 23 127.39 8.70 18 6 -23 114.59 10.20 16 -6 -23 83.39 7.60 -16 -6 23 77.09 6.00 -16 -6 23 75.59 7.40 -16 -6 23 61.39 6.50 16 6 -23 76.79 9.40 -16 6 23 72.49 7.50 -16 6 23 58.49 5.70 -14 -6 23 6.60 4.20 -14 -6 23 0.30 4.30 -14 -6 23 3.70 3.20 14 -6 -23 3.20 4.00 -14 6 23 -0.40 3.80 14 6 -23 -1.60 5.30 -12 -6 23 41.30 6.10 -12 -6 23 40.10 5.80 -12 -6 23 34.30 4.80 12 -6 -23 36.50 5.10 -12 6 23 28.00 4.50 12 6 -23 30.80 5.90 -10 -6 23 1.80 2.90 -10 -6 23 2.50 3.00 10 -6 -23 0.50 3.80 -10 -6 23 -0.10 2.70 10 6 -23 -1.40 3.40 -10 6 23 1.30 3.50 -8 -6 23 99.39 8.20 8 -6 -23 120.99 9.20 -8 -6 23 115.59 7.70 -8 -6 23 118.59 8.00 -8 6 23 122.09 8.10 8 6 -23 110.59 10.70 -6 -6 23 166.78 9.10 -6 -6 23 194.88 9.80 6 -6 -23 178.78 10.50 -6 -6 23 174.98 11.40 -6 6 23 193.38 10.30 6 6 -23 197.88 13.20 -4 -6 23 39.40 5.60 -4 -6 23 42.80 5.20 4 -6 -23 49.10 6.20 4 -6 -23 31.30 4.70 -4 -6 23 40.80 6.70 -4 6 23 47.90 6.60 4 6 -23 53.39 7.20 -17 -7 23 159.28 10.70 17 -7 -23 178.58 10.10 -17 -7 23 187.48 9.30 -17 -7 23 185.48 10.40 17 7 -23 161.28 12.80 -17 7 23 178.78 10.20 -15 -7 23 583.64 20.90 -15 -7 23 584.54 19.10 15 -7 -23 615.84 20.30 -15 -7 23 558.64 20.00 15 7 -23 605.24 23.10 -15 7 23 589.34 20.20 13 -7 -23 291.57 13.30 -13 -7 23 272.57 13.60 -13 -7 23 286.47 12.50 -13 -7 23 267.77 13.10 13 7 -23 274.17 14.80 -13 7 23 266.07 12.30 -11 -7 23 3.90 3.00 -11 -7 23 0.30 2.90 11 -7 -23 1.20 2.80 -11 -7 23 1.00 3.30 -11 7 23 -1.00 3.40 11 7 -23 10.00 4.50 -9 -7 23 30.40 5.70 -9 -7 23 29.90 4.40 9 -7 -23 24.40 5.40 -9 -7 23 35.40 5.00 -9 7 23 26.00 5.00 9 7 -23 41.80 6.80 -7 -7 23 16.60 5.00 -7 -7 23 17.60 4.30 -7 -7 23 17.40 4.50 7 -7 -23 16.00 5.00 -7 7 23 12.00 3.60 7 7 -23 19.80 5.20 -5 -7 23 147.59 9.50 -5 -7 23 164.28 11.20 5 -7 -23 168.48 10.10 5 -7 -23 144.19 9.00 -5 -7 23 141.89 8.80 5 7 -23 163.58 12.40 -5 7 23 153.18 9.40 -14 -8 23 50.99 5.40 14 -8 -23 59.99 6.40 -14 -8 23 66.49 7.20 -14 -8 23 44.80 5.70 14 8 -23 48.10 8.00 -14 8 23 51.09 5.20 12 -8 -23 20.40 4.90 -12 -8 23 31.30 5.00 -12 -8 23 27.80 5.00 -12 -8 23 21.70 5.30 -12 8 23 18.60 3.70 12 8 -23 20.50 6.50 -10 -8 23 4.30 4.60 -10 -8 23 6.60 3.40 -10 -8 23 9.60 4.10 10 -8 -23 4.10 3.10 10 8 -23 15.80 6.30 -10 8 23 8.40 3.10 -8 -8 23 3.60 3.80 20 0 -24 52.19 7.10 -20 0 24 51.09 7.00 -20 0 24 68.39 7.40 18 0 -24 75.79 7.50 -18 0 24 89.59 7.70 -18 0 24 69.69 7.20 -16 0 24 107.99 7.50 16 0 -24 106.79 9.60 -16 0 24 101.09 8.80 14 0 -24 22.00 4.80 -14 0 24 17.30 4.40 -14 0 24 6.50 3.60 -12 0 24 30.90 4.80 -12 0 24 29.00 4.90 12 0 -24 19.00 4.70 10 0 -24 12.50 5.40 -10 0 24 8.70 3.60 8 0 -24 32.00 6.60 -8 0 24 43.30 5.50 6 0 -24 152.48 10.30 -6 0 24 146.59 9.30 -4 0 24 19.60 5.30 4 0 -24 8.90 4.20 -4 0 24 9.40 3.20 -19 -1 24 19.60 4.20 -19 -1 24 12.00 5.10 19 -1 -24 12.10 5.10 19 1 -24 21.50 6.10 -19 1 24 9.60 3.50 -19 1 24 11.00 5.10 -17 -1 24 113.89 8.40 -17 -1 24 99.69 8.20 17 -1 -24 116.79 9.60 17 1 -24 91.79 8.60 -17 1 24 94.29 8.50 -17 1 24 96.09 7.80 -15 -1 24 2.50 3.50 15 -1 -24 -3.50 4.20 -15 -1 24 -3.00 3.80 -15 1 24 3.50 3.40 15 1 -24 2.10 4.70 -15 1 24 2.80 3.00 -13 -1 24 192.78 10.30 13 -1 -24 175.58 10.90 -13 -1 24 189.88 11.40 13 1 -24 182.58 12.40 -13 1 24 184.48 10.00 -13 1 24 179.28 11.00 11 -1 -24 326.57 15.50 -11 -1 24 289.57 14.10 -11 -1 24 310.67 12.40 11 1 -24 310.37 15.00 -11 1 24 292.87 13.90 -9 -1 24 82.49 8.00 9 -1 -24 97.89 9.40 -9 1 24 87.09 7.80 9 1 -24 91.99 8.60 -7 -1 24 -2.40 4.10 7 -1 -24 -0.20 4.70 -7 -1 24 -0.60 2.00 7 1 -24 5.10 3.90 -7 1 24 6.10 3.20 5 -1 -24 0.60 4.80 -5 -1 24 2.00 4.30 -5 -1 24 1.90 2.30 -5 1 24 -0.60 2.70 5 1 -24 -3.70 4.40 -18 -2 24 275.67 12.90 18 -2 -24 237.78 12.40 -18 -2 24 251.87 12.90 -18 2 24 264.67 12.80 18 2 -24 264.37 14.90 16 -2 -24 133.19 10.30 -16 -2 24 115.59 8.00 -16 -2 24 110.09 9.40 -16 2 24 118.29 7.80 16 2 -24 110.99 9.50 -16 2 24 111.99 9.00 -14 -2 24 49.99 6.00 14 -2 -24 45.90 6.20 -14 -2 24 50.69 6.10 14 2 -24 64.59 8.00 -14 2 24 47.80 6.60 -14 2 24 47.80 5.60 -12 -2 24 95.39 5.90 -12 -2 24 87.19 7.60 12 -2 -24 97.09 8.90 -12 -2 24 105.39 7.20 12 2 -24 116.29 10.50 -12 2 24 100.19 8.50 10 -2 -24 188.68 12.10 -10 -2 24 171.08 8.10 -10 -2 24 171.58 9.10 -10 -2 24 178.78 11.30 -10 2 24 199.08 11.30 10 2 -24 197.88 13.20 8 -2 -24 163.48 11.70 -8 -2 24 162.58 10.90 8 2 -24 152.48 12.00 -8 2 24 158.68 10.40 6 -2 -24 42.50 7.20 -6 -2 24 41.30 6.30 -6 -2 24 35.30 4.20 6 2 -24 43.20 7.20 -6 2 24 33.00 5.00 -4 -2 24 6.60 4.90 -4 -2 24 1.50 2.60 4 -2 -24 3.60 4.90 -4 2 24 2.40 3.10 4 2 -24 0.40 3.70 -19 -3 24 24.60 4.70 -19 -3 24 24.30 3.70 -19 -3 24 21.90 4.60 19 -3 -24 33.30 5.80 -19 3 24 31.70 5.20 19 3 -24 26.50 5.70 -19 3 24 37.70 5.10 -17 -3 24 240.68 12.60 -17 -3 24 233.68 12.90 17 -3 -24 260.37 13.30 -17 3 24 252.87 12.10 17 3 -24 274.97 15.30 -17 3 24 257.97 13.40 -15 -3 24 73.59 5.60 -15 -3 24 71.79 7.00 15 -3 -24 61.39 7.30 -15 -3 24 66.49 6.70 -15 3 24 61.19 5.80 15 3 -24 74.29 8.00 -15 3 24 77.09 8.00 -13 -3 24 23.60 3.50 13 -3 -24 29.30 5.90 -13 -3 24 26.70 4.90 -13 -3 24 36.90 6.10 13 3 -24 21.00 5.10 -13 3 24 33.60 5.70 -11 -3 24 24.90 5.40 -11 -3 24 21.50 3.90 -11 -3 24 30.50 4.00 11 -3 -24 24.60 5.70 11 3 -24 24.00 6.50 -11 3 24 30.40 5.60 9 -3 -24 87.29 8.00 -9 -3 24 67.79 6.70 -9 -3 24 67.89 6.00 -9 -3 24 79.79 5.50 -9 3 24 85.49 8.00 9 3 -24 85.89 9.20 -7 -3 24 324.77 12.50 -7 -3 24 310.17 14.00 7 -3 -24 349.96 15.40 7 3 -24 327.17 15.80 -7 3 24 340.47 14.70 -5 -3 24 186.58 9.40 -5 -3 24 200.08 11.10 5 -3 -24 207.98 11.70 -5 3 24 189.18 10.30 5 3 -24 217.38 12.70 -18 -4 24 9.80 4.50 -18 -4 24 7.80 3.00 -18 4 24 10.80 4.90 16 -4 -24 2.30 4.10 -16 -4 24 8.40 4.60 -16 -4 24 1.50 1.90 -16 -4 24 4.30 3.20 -16 4 24 3.40 3.50 -16 4 24 4.80 4.30 16 4 -24 0.10 5.20 -14 -4 24 38.70 6.10 14 -4 -24 58.29 6.40 -14 -4 24 34.20 4.40 -14 -4 24 44.60 6.20 14 4 -24 49.60 7.80 -14 4 24 42.20 6.20 -12 -4 24 100.89 8.10 -12 -4 24 102.19 7.40 -12 -4 24 106.39 6.90 12 -4 -24 116.29 9.60 -12 4 24 97.19 8.30 12 4 -24 127.49 11.10 -10 -4 24 33.50 4.40 -10 -4 24 33.00 5.90 10 -4 -24 41.70 6.70 -10 -4 24 38.30 4.80 10 4 -24 37.30 7.10 -10 4 24 39.00 5.80 8 -4 -24 20.50 4.60 -8 -4 24 21.40 5.50 -8 -4 24 8.70 2.70 -8 -4 24 17.00 3.70 8 4 -24 17.00 6.10 -8 4 24 16.00 4.70 6 -4 -24 65.49 7.10 -6 -4 24 66.19 7.70 -6 -4 24 67.09 6.10 -6 4 24 54.69 5.90 6 4 -24 56.79 8.30 -6 4 24 64.59 7.20 15 -5 -24 77.49 7.70 -15 -5 24 63.29 6.60 -15 -5 24 73.49 6.90 -15 5 24 70.89 7.50 15 5 -24 75.29 8.60 -13 -5 24 5.90 3.50 -13 -5 24 12.30 2.90 -13 -5 24 9.20 4.40 13 -5 -24 8.20 3.50 13 5 -24 12.50 4.80 -13 5 24 11.70 4.50 -11 -5 24 0.50 4.10 -11 -5 24 3.80 2.90 11 -5 -24 3.20 4.20 -11 -5 24 0.90 2.80 11 5 -24 -2.20 4.80 -11 5 24 3.10 4.00 -9 -5 24 -0.70 2.70 -9 -5 24 -3.30 4.00 9 -5 -24 0.90 3.20 -9 -5 24 -0.70 2.50 -9 5 24 -0.70 3.60 9 5 -24 -0.30 3.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 73293 _shelx_res_file ; TITL clsi107_0m_b.res in C2/c clsi107_0m_b.res created by SHELXL-2018/3 at 09:53:40 on 15-Jun-2021 REM Old TITL clsi107_0m in C2/c REM SHELXT solution in C2/c: R1 0.174, Rweak 0.004, Alpha 0.034 REM 2.684 for 205 systematic absences, Orientation as input REM Formula found by SHELXT: C8 N8 Na5 O38 Sb W6 REM ##### CELL 0.71073 21.9761 13.9179 16.209 90 111.189 90 ZERR 4 0.0014 0.0009 0.001 0 0.002 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H N Na O Sb W UNIT 24 224 8 20 184 4 24 DFIX 0.95 0.03 O24 H24b O24 H24a O23 H23a O23 H23b O22 H22a O22 H22b O21 = H21A O21 H21B O20 H20A O20 H20B O19 H19A O19 H19B O18 H18B O18 H18A O16 = H16B O16 H16A O17 H17B O17 H17A O15 H15B O15 H15A O14 H14 O13 H13 SADI Na1 H24a Na1 H24b L.S. 20 PLAN 1 SIZE 0.08 0.1 0.05 TEMP -73 CONF BOND $H htab LIST 4 MORE -1 fmap 2 acta OMIT 1 1 0 OMIT 4 0 4 REM REM REM WGHT 0.004900 8.818101 EXTI 0.000087 FVAR 0.05478 0.50865 0.49153 W1 7 0.236461 0.983101 0.509671 11.00000 0.01187 0.00678 = 0.00937 -0.00038 0.00455 0.00066 W2 7 0.336382 0.892142 0.423766 11.00000 0.00935 0.00934 = 0.00992 0.00009 0.00449 -0.00122 W3 7 0.349504 0.658946 0.415000 11.00000 0.00888 0.01020 = 0.00925 0.00001 0.00452 0.00212 SB1 6 0.250000 0.750000 0.500000 10.50000 0.00750 0.00630 = 0.00766 -0.00023 0.00376 0.00040 O1 5 0.193050 0.634973 0.461524 11.00000 0.01004 0.00903 = 0.00848 -0.00063 0.00328 -0.00046 O2 5 0.320450 0.653010 0.530842 11.00000 0.00978 0.00922 = 0.00917 0.00005 0.00381 0.00251 O3 5 0.268765 0.763866 0.389770 11.00000 0.00916 0.00977 = 0.00835 0.00014 0.00413 0.00021 O4 5 0.293699 1.069301 0.566975 11.00000 0.02054 0.01277 = 0.01548 -0.00289 0.00746 -0.00321 O5 5 0.165847 1.050017 0.457225 11.00000 0.01906 0.01364 = 0.01675 0.00351 0.00661 0.00598 O6 5 0.217731 0.939067 0.611493 11.00000 0.01362 0.01136 = 0.01010 -0.00213 0.00472 -0.00096 O7 5 0.396114 0.975514 0.480780 11.00000 0.01438 0.01679 = 0.02000 -0.00257 0.00499 -0.00461 O8 5 0.258179 0.967469 0.404141 11.00000 0.01399 0.01031 = 0.01036 0.00100 0.00461 0.00098 O9 5 0.335702 0.896903 0.316708 11.00000 0.01891 0.01754 = 0.01408 0.00184 0.00896 -0.00011 O10 5 0.391421 0.779171 0.464449 11.00000 0.00959 0.01335 = 0.01286 -0.00016 0.00309 -0.00024 O11 5 0.344805 0.672416 0.305816 11.00000 0.01651 0.01627 = 0.01252 0.00018 0.00797 0.00165 O12 5 0.418325 0.588266 0.464956 11.00000 0.01399 0.01872 = 0.01729 0.00075 0.00518 0.00639 NA1 4 0.500000 0.996294 0.250000 10.50000 0.01671 0.02272 = 0.01920 0.00000 0.00587 0.00000 NA2 4 0.500000 0.747356 0.250000 10.50000 0.02210 0.02301 = 0.02559 0.00000 0.00728 0.00000 NA3 4 0.500000 0.493147 0.250000 10.50000 0.02046 0.01989 = 0.01930 0.00000 0.00951 0.00000 NA4 4 0.411098 0.341180 0.327595 11.00000 0.01495 0.02063 = 0.01742 0.00088 0.00603 -0.00035 O13 5 0.335149 0.216555 0.264821 11.00000 0.01793 0.01697 = 0.01257 -0.00010 0.00446 0.00082 H13 2 0.301838 0.231702 0.214411 11.00000 0.03871 O14 5 0.377459 0.313358 0.451467 11.00000 0.02202 0.02671 = 0.02037 -0.00501 0.00863 -0.00710 H14 2 0.369711 0.366453 0.479079 11.00000 0.08584 O15 5 0.314932 0.434822 0.275972 11.00000 0.02007 0.01485 = 0.01570 -0.00117 0.00434 0.00355 H15A 2 0.295766 0.449338 0.219910 11.00000 0.02596 H15B 2 0.300396 0.477941 0.300585 11.00000 0.04113 O16 5 0.498510 0.232636 0.379661 11.00000 0.02899 0.02779 = 0.03144 -0.00450 -0.00851 0.00900 H16A 2 0.503901 0.179077 0.352247 11.00000 0.13428 H16B 2 0.529939 0.229948 0.431909 11.00000 0.05092 O17 5 0.425454 0.358215 0.191004 11.00000 0.01774 0.03237 = 0.01421 -0.00111 0.00307 -0.00261 H17A 2 0.390104 0.363650 0.139417 11.00000 0.04362 H17B 2 0.449174 0.315598 0.175429 11.00000 0.05321 O18 5 0.482387 0.472715 0.383011 11.00000 0.01870 0.02482 = 0.01481 -0.00178 0.00474 0.00740 H18A 2 0.517853 0.455393 0.431936 11.00000 0.03100 H18B 2 0.460975 0.513196 0.407337 11.00000 0.05304 O19 5 0.579282 0.617379 0.292744 11.00000 0.01773 0.02664 = 0.01824 0.00563 0.00754 0.00081 H19A 2 0.609335 0.602888 0.346160 11.00000 0.04276 H19B 2 0.604654 0.628772 0.262391 11.00000 0.04563 O20 5 0.503651 0.761718 0.395920 11.00000 0.02662 0.06430 = 0.02999 0.00260 0.00939 0.00317 H20A 2 0.471066 0.777093 0.416255 11.00000 0.15121 H20B 2 0.537014 0.741994 0.445411 11.00000 0.10319 O21 5 0.585059 0.873596 0.288983 11.00000 0.01907 0.02652 = 0.02139 0.00007 0.00906 -0.00214 H21A 2 0.613514 0.893176 0.341114 11.00000 0.04220 H21B 2 0.600791 0.878151 0.245655 11.00000 0.09392 O22 5 0.582306 1.111032 0.307611 11.00000 0.02010 0.03696 = 0.01996 0.00344 0.00102 -0.01049 H22A 2 0.615982 1.114179 0.360355 11.00000 0.03602 H22B 2 0.603429 1.140815 0.277075 11.00000 0.05254 PART 2 O23 5 0.483620 1.026104 0.384497 31.00000 0.01766 0.02682 = 0.01905 0.00333 0.00592 -0.00297 AFIX 7 H23A 2 0.520517 1.019846 0.429088 31.00000 -1.50000 H23B 2 0.458680 0.981153 0.392879 31.00000 -1.50000 AFIX 0 PART 0 N1 3 0.244485 0.286597 0.330455 11.00000 0.01501 0.01434 = 0.01557 -0.00066 0.00515 0.00065 AFIX 137 H1A 2 0.209963 0.263685 0.284205 11.00000 -1.50000 H1B 2 0.268602 0.326406 0.309808 11.00000 -1.50000 H1C 2 0.229658 0.319666 0.367847 11.00000 -1.50000 AFIX 0 C1 1 0.312008 0.152134 0.315463 11.00000 0.02091 0.01054 = 0.01835 0.00019 0.00552 0.00164 AFIX 23 H1D 2 0.348055 0.108998 0.349921 11.00000 -1.20000 H1E 2 0.276807 0.111847 0.274682 11.00000 -1.20000 AFIX 0 C2 1 0.285964 0.204452 0.378960 11.00000 0.01839 0.01100 = 0.01498 0.00253 0.00487 -0.00041 AFIX 13 H2 2 0.256858 0.158600 0.394736 11.00000 -1.20000 AFIX 0 C3 1 0.337285 0.238640 0.464855 11.00000 0.02095 0.02106 = 0.01347 0.00091 0.00381 -0.00135 AFIX 23 H3A 2 0.315385 0.262462 0.504576 11.00000 -1.20000 H3B 2 0.365219 0.183629 0.494426 11.00000 -1.20000 AFIX 6 PART 1 O24 5 0.490119 0.976310 0.388357 21.00000 0.02342 0.07998 = 0.02201 -0.01749 0.01113 -0.01583 H24A 2 0.525636 0.986172 0.433912 21.00000 -1.50000 H24B 2 0.460889 1.011938 0.398180 21.00000 -1.50000 AFIX 0 HKLF 4 REM clsi107_0m_b.res in C2/c REM wR2 = 0.0246, GooF = S = 1.151, Restrained GooF = 1.155 for all data REM R1 = 0.0131 for 8213 Fo > 4sig(Fo) and 0.0156 for all 8841 data REM 390 parameters refined using 23 restraints END WGHT 0.0049 8.8073 REM Instructions for potential hydrogen bonds EQIV $3 -x+1/2, y-1/2, -z+1/2 HTAB O13 O3_$3 EQIV $1 -x+1/2, -y+3/2, -z+1 HTAB O14 O5_$1 HTAB O15 O8_$3 HTAB O15 O6_$1 EQIV $4 x, y-1, z HTAB O16 O22_$4 HTAB O16 O23_$4 EQIV $5 -x+1, -y+1, -z+1 HTAB O16 O10_$5 EQIV $6 x, -y+1, z-1/2 HTAB O17 O2_$6 EQIV $2 -x+1, y, -z+1/2 HTAB O17 O16_$2 HTAB O18 O12_$5 HTAB O18 O12 EQIV $7 x+1/2, y-1/2, z HTAB O19 O5_$7 HTAB O19 O11_$2 HTAB O20 O10 HTAB O20 O14_$5 EQIV $8 -x+1, -y+2, -z+1 HTAB O21 O4_$8 HTAB O21 O9_$2 EQIV $9 x+1/2, y+1/2, z HTAB O22 O1_$9 EQIV $10 -x+1, y+1, -z+1/2 HTAB O22 O13_$10 HTAB O23 O7_$8 HTAB O23 O7 HTAB N1 O11_$3 HTAB N1 O15 HTAB N1 O4_$1 HTAB C1 O6_$6 HTAB C1 O11_$3 REM Highest difference peak 0.601, deepest hole -0.689, 1-sigma level 0.119 Q1 1 0.2735 1.0231 0.5520 11.00000 0.05 0.60 ; _shelx_res_checksum 77504 data_global _journal_data_validation_number ? _journal_date_recd_electronic 2021-04-25 _journal_date_accepted 2021-06-16 _journal_name_full 'Acta Crystallographica, Section C' _journal_year 2021 _journal_volume 77 _journal_issue 7 _journal_page_first 420 _journal_page_last 425 _journal_paper_category FA _journal_paper_doi 10.1107/S2053229621006239 _journal_coeditor_code KY3204 _publ_contact_author_name ; Annette Rompel ; _publ_contact_author_address ; Universit\"at Wien, Fakult\"at f\"ur Chemie Institut f\"ur Biophysikalische Chemie Althanstrasse 14 Wien 1090 Austria ; _publ_contact_author_email 'annette.rompel@univie.ac.at' _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_section_title ; Synthesis and characterization of the Anderson--Evans tungstoantimonate [Na~5~(H~2~O)~18~{(HOCH~2~)~2~CHNH~3~}~2~][SbW~6~O~24~] ; _publ_section_title_footnote . loop_ _publ_author_name _publ_author_footnote _publ_author_address 'Kleanthi Sifaki' . ; Universit\"at Wien, Fakult\"at f\"ur Chemie Institut f\"ur Biophysikalische Chemie Althanstrasse 14 Wien 1090 Austria ; 'Nadiia I. Gumerova' . ; Universit\"at Wien, Fakult\"at f\"ur Chemie Institut f\"ur Biophysikalische Chemie Althanstrasse 14 Wien 1090 Austria ; 'Gerald Giester' . ; Universit\"at Wien Fakult\"at f\"ur Geowissenschaften, Geographie und Astronomie Institut f\"ur Mineralogie und Kristallographie Althanstrasse 14 Wien 1090 Austria ; 'Annette Rompel' . ; Universit\"at Wien, Fakult\"at f\"ur Chemie Institut f\"ur Biophysikalische Chemie Althanstrasse 14 Wien 1090 Austria ; _publ_section_synopsis ; The isolation and characterization of the Anderson--Evans-type tungstoantimonate [Sb^V^W^VI^~6~O~24~]^7-^ with a T-shaped sodium--serinol complex [Na~5~(H~2~O)~18~{(HOCH~2~)~2~CHNH~3~}~2~]^7+^ as counter-cation is reported. ;