data_Ag1D-PIm _audit_creation_date 2021-05-12 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2016/4' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '0.25(C96 H80 Ag32 N48 O48)' _chemical_formula_sum 'C24 H20 Ag8 N12 O12' _chemical_formula_weight 1531.48 _chemical_melting_point ? _chemical_oxdiff_usercomment ' ' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ag' 'Ag' 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'tetragonal' _space_group_IT_number 130 _space_group_name_H-M_alt 'P 4/n c c' _space_group_name_Hall '-P 4a 2ac' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-y+1/2, x, z' 'y, -x+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' 'y+1/2, x+1/2, -z+1/2' '-y, -x, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'y-1/2, -x, -z' '-y, x-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' '-y-1/2, -x-1/2, z-1/2' 'y, x, z-1/2' _cell_length_a 16.38990(10) _cell_length_b 16.38990(10) _cell_length_c 14.3453(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3853.56(7) _cell_formula_units_Z 4 _cell_measurement_reflns_used 4475 _cell_measurement_temperature 200.00(10) _cell_measurement_theta_max 73.1690 _cell_measurement_theta_min 3.7920 _shelx_estimated_absorpt_T_max 0.737 _shelx_estimated_absorpt_T_min 0.442 _exptl_absorpt_coefficient_mu 32.541 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.25143 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.27b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.640 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 2880 _exptl_crystal_size_max 0.03 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.01 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0450 _diffrn_reflns_av_unetI/netI 0.0327 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.980 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 10460 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.980 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.071 _diffrn_reflns_theta_min 5.398 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 200.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.980 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 15.00 41.00 0.50 0.50 -- 0.00 57.00 30.00 52 2 \w -10.00 89.00 0.50 0.50 -- 0.00 38.00 60.00 198 3 \w 65.00 96.00 0.50 1.00 -- 95.20 -30.00 120.00 62 4 \w 30.00 113.00 0.50 1.00 -- 95.20 -61.00 -60.00 166 5 \w 160.00 185.00 0.50 1.00 -- 95.20 61.00-150.00 50 6 \w 6.00 54.00 0.50 1.00 -- 95.20 -30.00 120.00 96 7 \w 28.00 122.00 0.50 1.00 -- 95.20 -77.00 -60.00 188 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC12 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0163964000 _diffrn_orient_matrix_UB_12 0.0185190000 _diffrn_orient_matrix_UB_13 -0.1035619000 _diffrn_orient_matrix_UB_21 -0.0453444000 _diffrn_orient_matrix_UB_22 0.0818746000 _diffrn_orient_matrix_UB_23 0.0097736000 _diffrn_orient_matrix_UB_31 0.0807296000 _diffrn_orient_matrix_UB_32 0.0422356000 _diffrn_orient_matrix_UB_33 0.0266279000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1661 _reflns_number_total 1925 _reflns_odcompleteness_completeness 99.95 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXD (Sheldrick, 2008)' _refine_diff_density_max 0.564 _refine_diff_density_min -1.663 _refine_diff_density_rms 0.217 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.127 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 128 _refine_ls_number_reflns 1925 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0354 _refine_ls_R_factor_gt 0.0316 _refine_ls_restrained_S_all 1.127 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0492P)^2^+1.7572P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0864 _refine_ls_wR_factor_ref 0.0895 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2.a Secondary CH2 refined with riding coordinates: C3(H3A,H3B) 2.b Aromatic/amide H refined with riding coordinates: C6(H6), C5(H5), C4(H4) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ag1 Ag 0.750000 0.250000 0.60473(3) 0.02850(15) Uani 1 2 d S T P . . Ag3 Ag 0.38412(2) -0.13451(2) 0.49669(2) 0.03639(14) Uani 1 1 d . . . . . Ag2 Ag 0.66029(2) 0.16029(2) 0.750000 0.03725(16) Uani 1 2 d S T P . . N3 N 0.49719(19) -0.10409(19) 0.5663(2) 0.0276(6) Uani 1 1 d . . . . . N2 N 0.62065(19) -0.06681(19) 0.6055(2) 0.0278(7) Uani 1 1 d . . . . . O3 O 0.6830(2) 0.0236(2) 0.8332(2) 0.0489(8) Uani 1 1 d . . . . . O1 O 0.7995(2) 0.0850(2) 0.8400(3) 0.0555(9) Uani 1 1 d . . . . . C1 C 0.7213(2) 0.1254(2) 0.6053(2) 0.0254(8) Uani 1 1 d . . . . . C6 C 0.5695(2) -0.0822(2) 0.5344(3) 0.0285(8) Uani 1 1 d . . . . . H6 H 0.583153 -0.077931 0.471693 0.034 Uiso 1 1 calc R . . . . C5 C 0.5029(3) -0.1026(3) 0.6621(3) 0.0349(9) Uani 1 1 d . . . . . H5 H 0.460841 -0.115372 0.703092 0.042 Uiso 1 1 calc R . . . . N1 N 0.7581(2) 0.0210(3) 0.8498(2) 0.0421(9) Uani 1 1 d . . . . . C4 C 0.5788(3) -0.0796(3) 0.6871(3) 0.0363(9) Uani 1 1 d . . . . . H4 H 0.598687 -0.073704 0.747426 0.044 Uiso 1 1 calc R . . . . C3 C 0.7039(2) -0.0373(2) 0.5977(3) 0.0366(10) Uani 1 1 d . . . . . H3A H 0.727580 -0.057388 0.540152 0.044 Uiso 1 1 calc R . . . . H3B H 0.735895 -0.058763 0.649052 0.044 Uiso 1 1 calc R . . . . C2 C 0.7083(2) 0.0532(2) 0.5988(3) 0.0280(8) Uani 1 1 d . . . . . O2 O 0.7910(3) -0.0436(3) 0.8743(3) 0.0894(16) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ag1 0.0343(3) 0.0195(2) 0.0317(3) 0.000 0.000 -0.00511(14) Ag3 0.0257(2) 0.0393(2) 0.0442(2) -0.00509(12) -0.01003(11) 0.00208(14) Ag2 0.0409(2) 0.0409(2) 0.0299(2) -0.00314(11) 0.00314(11) -0.00287(19) N3 0.0219(16) 0.0230(16) 0.0380(17) 0.0016(13) -0.0015(13) -0.0014(13) N2 0.0222(16) 0.0232(16) 0.0382(16) -0.0008(12) -0.0002(12) -0.0033(13) O3 0.0432(19) 0.051(2) 0.0527(19) 0.0003(15) -0.0082(15) -0.0089(15) O1 0.0387(19) 0.057(2) 0.071(2) -0.0241(18) 0.0010(16) -0.0006(17) C1 0.0217(18) 0.0216(18) 0.0328(19) -0.0002(14) -0.0050(14) -0.0008(14) C6 0.0282(19) 0.0239(19) 0.0336(19) 0.0034(15) -0.0001(15) -0.0041(15) C5 0.035(2) 0.036(2) 0.0339(19) -0.0064(16) 0.0072(16) -0.0071(17) N1 0.044(2) 0.051(2) 0.0319(19) -0.0093(16) -0.0056(15) 0.017(2) C4 0.037(2) 0.036(2) 0.036(2) -0.0073(17) -0.0020(17) -0.0046(18) C3 0.022(2) 0.022(2) 0.066(3) -0.0004(18) -0.0030(18) -0.0032(16) C2 0.0188(17) 0.026(2) 0.0394(19) 0.0016(15) -0.0057(14) -0.0050(15) O2 0.105(4) 0.079(3) 0.084(3) 0.016(2) -0.008(3) 0.049(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ag1 Ag1 3.0046(9) 11_666 ? Ag1 Ag3 3.2889(4) 4_655 ? Ag1 Ag3 3.2889(4) 3 ? Ag1 Ag3 3.2453(4) 9_656 ? Ag1 Ag3 3.2453(4) 10_666 ? Ag1 Ag2 2.9440(5) . ? Ag1 Ag2 2.9439(5) 2_655 ? Ag1 C1 2.095(4) 2_655 ? Ag1 C1 2.095(4) . ? Ag3 Ag1 3.2453(4) 9_656 ? Ag3 Ag1 3.2889(4) 3_545 ? Ag3 N3 2.163(3) . ? Ag3 C1 2.269(4) 9_656 ? Ag3 C2 2.439(4) 9_656 ? Ag2 Ag1 2.9440(5) 7_546 ? Ag2 O3 2.565(3) . ? Ag2 O3 2.565(3) 7_546 ? Ag2 C1 2.374(4) 7_546 ? Ag2 C1 2.375(4) . ? N3 C6 1.321(5) . ? N3 C5 1.377(5) . ? N2 C6 1.344(5) . ? N2 C4 1.373(5) . ? N2 C3 1.452(5) . ? O3 N1 1.255(5) . ? O1 N1 1.257(5) . ? C1 Ag3 2.269(4) 9_656 ? C1 C2 1.207(5) . ? C6 H6 0.9300 . ? C5 H5 0.9300 . ? C5 C4 1.348(6) . ? N1 O2 1.238(6) . ? C4 H4 0.9300 . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C2 1.485(6) . ? C2 Ag3 2.439(4) 9_656 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Ag1 Ag1 Ag3 63.366(9) 11_666 9_656 ? Ag1 Ag1 Ag3 61.887(8) 11_666 3 ? Ag1 Ag1 Ag3 61.887(8) 11_666 4_655 ? Ag1 Ag1 Ag3 63.366(9) 11_666 10_666 ? Ag3 Ag1 Ag3 123.774(17) 4_655 3 ? Ag3 Ag1 Ag3 77.805(6) 10_666 4_655 ? Ag3 Ag1 Ag3 77.805(6) 9_656 4_655 ? Ag3 Ag1 Ag3 126.731(18) 9_656 10_666 ? Ag3 Ag1 Ag3 77.805(6) 9_656 3 ? Ag3 Ag1 Ag3 77.805(6) 10_666 3 ? Ag2 Ag1 Ag1 135.064(9) . 11_666 ? Ag2 Ag1 Ag1 135.065(9) 2_655 11_666 ? Ag2 Ag1 Ag3 71.805(9) 2_655 10_666 ? Ag2 Ag1 Ag3 71.804(9) . 9_656 ? Ag2 Ag1 Ag3 112.329(7) . 3 ? Ag2 Ag1 Ag3 161.256(15) . 10_666 ? Ag2 Ag1 Ag3 106.691(7) 2_655 3 ? Ag2 Ag1 Ag3 161.255(15) 2_655 9_656 ? Ag2 Ag1 Ag3 112.330(7) 2_655 4_655 ? Ag2 Ag1 Ag3 106.690(7) . 4_655 ? Ag2 Ag1 Ag2 89.872(17) 2_655 . ? C1 Ag1 Ag1 90.21(10) . 11_666 ? C1 Ag1 Ag1 90.21(10) 2_655 11_666 ? C1 Ag1 Ag3 58.63(10) 2_655 3 ? C1 Ag1 Ag3 44.05(10) 2_655 10_666 ? C1 Ag1 Ag3 58.63(10) . 4_655 ? C1 Ag1 Ag3 136.22(10) 2_655 9_656 ? C1 Ag1 Ag3 44.05(10) . 9_656 ? C1 Ag1 Ag3 136.22(10) . 10_666 ? C1 Ag1 Ag3 121.60(10) 2_655 4_655 ? C1 Ag1 Ag3 121.60(10) . 3 ? C1 Ag1 Ag2 53.03(10) 2_655 2_655 ? C1 Ag1 Ag2 53.04(10) . . ? C1 Ag1 Ag2 126.59(10) . 2_655 ? C1 Ag1 Ag2 126.59(10) 2_655 . ? C1 Ag1 C1 179.6(2) 2_655 . ? Ag1 Ag3 Ag1 54.748(14) 9_656 3_545 ? N3 Ag3 Ag1 119.18(8) . 3_545 ? N3 Ag3 Ag1 157.17(8) . 9_656 ? N3 Ag3 C1 159.22(13) . 9_656 ? N3 Ag3 C2 131.71(12) . 9_656 ? C1 Ag3 Ag1 80.34(9) 9_656 3_545 ? C1 Ag3 Ag1 39.94(9) 9_656 9_656 ? C1 Ag3 C2 29.43(13) 9_656 9_656 ? C2 Ag3 Ag1 69.28(9) 9_656 9_656 ? C2 Ag3 Ag1 99.43(9) 9_656 3_545 ? Ag1 Ag2 Ag1 90.127(17) 7_546 . ? O3 Ag2 Ag1 133.86(8) . . ? O3 Ag2 Ag1 91.95(7) 7_546 . ? O3 Ag2 Ag1 133.86(8) 7_546 7_546 ? O3 Ag2 Ag1 91.95(7) . 7_546 ? O3 Ag2 O3 118.05(14) . 7_546 ? C1 Ag2 Ag1 44.82(9) . . ? C1 Ag2 Ag1 121.92(9) . 7_546 ? C1 Ag2 Ag1 44.82(9) 7_546 7_546 ? C1 Ag2 Ag1 121.92(9) 7_546 . ? C1 Ag2 O3 89.77(11) . 7_546 ? C1 Ag2 O3 97.80(12) 7_546 7_546 ? C1 Ag2 O3 97.80(12) . . ? C1 Ag2 O3 89.77(11) 7_546 . ? C1 Ag2 C1 165.31(18) 7_546 . ? C6 N3 Ag3 132.2(3) . . ? C6 N3 C5 106.3(3) . . ? C5 N3 Ag3 121.5(3) . . ? C6 N2 C4 107.8(3) . . ? C6 N2 C3 126.1(3) . . ? C4 N2 C3 125.9(3) . . ? N1 O3 Ag2 105.1(3) . . ? Ag1 C1 Ag3 96.01(14) . 9_656 ? Ag1 C1 Ag2 82.14(12) . . ? Ag3 C1 Ag2 103.12(14) 9_656 . ? C2 C1 Ag1 174.6(3) . . ? C2 C1 Ag3 83.1(3) . 9_656 ? C2 C1 Ag2 103.2(3) . . ? N3 C6 N2 110.4(3) . . ? N3 C6 H6 124.8 . . ? N2 C6 H6 124.8 . . ? N3 C5 H5 125.3 . . ? C4 C5 N3 109.5(4) . . ? C4 C5 H5 125.3 . . ? O3 N1 O1 118.6(4) . . ? O2 N1 O3 120.7(5) . . ? O2 N1 O1 120.7(4) . . ? N2 C4 H4 127.0 . . ? C5 C4 N2 106.1(4) . . ? C5 C4 H4 127.0 . . ? N2 C3 H3A 109.2 . . ? N2 C3 H3B 109.2 . . ? N2 C3 C2 112.2(3) . . ? H3A C3 H3B 107.9 . . ? C2 C3 H3A 109.2 . . ? C2 C3 H3B 109.2 . . ? C1 C2 Ag3 67.5(2) . 9_656 ? C1 C2 C3 171.7(4) . . ? C3 C2 Ag3 120.7(3) . 9_656 ? _smtbx_masks_special_details ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.250 0.250 -0.291 239.6 143.7 ? 2 0.750 0.750 -0.770 239.6 145.0 ? _shelx_res_file ; TITL hy_a.res in P4/ncc hy.res created by SHELXL-2016/4 at 17:49:38 on 12-May-2021 REM Old TITL HY in P4/ncc #130 REM SHELXT solution in P4/ncc REM R1 0.126, Rweak 0.001, Alpha 0.023, Orientation as input REM Formula found by SHELXT: C7 N2 Ag2 F3 CELL 1.54184 16.3899 16.3899 14.3453 90 90 90 ZERR 4 0.0001 0.0001 0.0002 0 0 0 LATT 1 SYMM 0.5-X,0.5-Y,+Z SYMM 0.5-Y,+X,+Z SYMM +Y,0.5-X,+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,-Y,0.5-Z SYMM 0.5+Y,0.5+X,0.5-Z SYMM -Y,-X,0.5-Z SFAC C H Ag N O UNIT 96 80 32 48 48 L.S. 20 0 0 PLAN 20 SIZE 0.01 0.03 0.03 BOND $H list 4 ABIN fmap 2 53 acta OMIT 1 3 0 OMIT 1 1 0 REM REM REM WGHT 0.049200 1.757200 FVAR 0.10188 AG1 3 0.750000 0.250000 0.604725 10.50000 0.03429 0.01951 = 0.03170 0.00000 0.00000 -0.00511 AG3 3 0.384125 -0.134512 0.496692 11.00000 0.02569 0.03926 = 0.04423 -0.00509 -0.01003 0.00208 AG2 3 0.660289 0.160289 0.750000 10.50000 0.04090 0.04090 = 0.02994 -0.00314 0.00314 -0.00287 N3 4 0.497190 -0.104087 0.566318 11.00000 0.02187 0.02305 = 0.03796 0.00159 -0.00150 -0.00145 N2 4 0.620653 -0.066812 0.605531 11.00000 0.02216 0.02321 = 0.03818 -0.00079 -0.00023 -0.00332 O3 5 0.683033 0.023626 0.833218 11.00000 0.04316 0.05091 = 0.05265 0.00026 -0.00824 -0.00894 O1 5 0.799527 0.085005 0.840003 11.00000 0.03871 0.05721 = 0.07071 -0.02411 0.00098 -0.00063 C1 1 0.721333 0.125444 0.605259 11.00000 0.02166 0.02162 = 0.03279 -0.00015 -0.00503 -0.00085 C6 1 0.569529 -0.082156 0.534441 11.00000 0.02817 0.02386 = 0.03360 0.00337 -0.00013 -0.00415 AFIX 43 H6 2 0.583153 -0.077931 0.471693 11.00000 -1.20000 AFIX 0 C5 1 0.502859 -0.102565 0.662055 11.00000 0.03463 0.03630 = 0.03388 -0.00645 0.00723 -0.00711 AFIX 43 H5 2 0.460841 -0.115372 0.703092 11.00000 -1.20000 AFIX 0 N1 4 0.758133 0.020983 0.849849 11.00000 0.04374 0.05060 = 0.03189 -0.00927 -0.00565 0.01677 C4 1 0.578753 -0.079635 0.687108 11.00000 0.03663 0.03643 = 0.03580 -0.00729 -0.00197 -0.00461 AFIX 43 H4 2 0.598687 -0.073704 0.747426 11.00000 -1.20000 AFIX 0 C3 1 0.703914 -0.037290 0.597718 11.00000 0.02182 0.02197 = 0.06609 -0.00039 -0.00300 -0.00324 AFIX 23 H3A 2 0.727580 -0.057388 0.540152 11.00000 -1.20000 H3B 2 0.735895 -0.058763 0.649052 11.00000 -1.20000 AFIX 0 C2 1 0.708332 0.053176 0.598770 11.00000 0.01876 0.02585 = 0.03945 0.00157 -0.00573 -0.00503 O2 5 0.791029 -0.043580 0.874336 11.00000 0.10486 0.07939 = 0.08403 0.01584 -0.00819 0.04896 HKLF 4 REM hy_a.res in P4/ncc REM R1 = 0.0316 for 1661 Fo > 4sig(Fo) and 0.0354 for all 1925 data REM 128 parameters refined using 0 restraints END WGHT 0.0492 1.7572 REM Highest difference peak 0.564, deepest hole -1.663, 1-sigma level 0.217 Q1 1 0.4615 -0.1224 0.5555 11.00000 0.05 0.56 Q2 1 0.7220 0.1581 0.7551 11.00000 0.05 0.55 Q3 1 0.7553 0.0909 0.7205 11.00000 0.05 0.49 Q4 1 0.8022 0.1586 0.8826 11.00000 0.05 0.47 Q5 1 0.7483 0.1235 0.9417 11.00000 0.05 0.46 Q6 1 0.7375 0.1498 0.6793 11.00000 0.05 0.45 Q7 1 0.7409 0.1513 0.8237 11.00000 0.05 0.44 Q8 1 0.4043 -0.1394 0.4371 11.00000 0.05 0.43 Q9 1 0.7347 0.1222 0.5710 11.00000 0.05 0.43 Q10 1 0.7993 0.1572 0.6274 11.00000 0.05 0.43 Q11 1 0.7211 -0.0412 0.5070 11.00000 0.05 0.42 Q12 1 0.7789 0.1006 0.8523 11.00000 0.05 0.42 Q13 1 0.7274 0.1051 0.5843 11.00000 0.05 0.41 Q14 1 0.7819 -0.1155 0.8802 11.00000 0.05 0.41 Q15 1 0.7434 -0.0763 0.8412 11.00000 0.05 0.40 Q16 1 0.6602 -0.0622 0.6024 11.00000 0.05 0.40 Q17 1 0.6631 -0.0102 0.8660 11.00000 0.05 0.40 Q18 1 0.5588 0.0003 0.7387 11.00000 0.05 0.40 Q19 1 0.7716 0.1222 0.6131 11.00000 0.05 0.40 Q20 1 0.6749 -0.0225 0.7934 11.00000 0.05 0.39 ; _shelx_res_checksum 12704 _shelx_hkl_file ; 0 0 1 -0.06 0.39 0 0 1 0.27 0.38 0 0 -1 0.21 0.30 0 0 -1 0.06 0.30 0 0 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13.08 7 2 9 216.83 13.39 7 2 10 9.45 1.70 7 2 -10 12.81 1.85 2 7 10 13.18 1.86 2 7 11 66.74 5.37 -7 2 11 79.37 5.66 7 2 -11 72.15 5.38 7 -2 -11 69.70 5.34 7 2 11 65.86 5.40 7 2 -12 1.39 0.87 -7 2 12 0.46 0.90 7 2 12 -0.21 0.84 2 7 12 0.45 0.95 7 -2 -12 -0.39 0.70 2 7 13 57.71 4.52 -2 7 13 60.20 4.79 -7 2 13 55.38 4.47 7 2 13 58.65 4.41 2 7 14 1.27 0.89 -7 2 14 0.17 0.67 -2 7 14 -0.20 0.86 -2 -7 14 -0.11 0.49 2 -7 14 -0.30 0.68 2 7 15 14.34 1.53 -7 2 15 13.13 1.39 -2 7 15 10.93 1.47 7 -2 15 10.27 1.35 2 -7 15 12.77 1.34 2 7 16 2.42 0.63 -2 7 16 1.03 0.53 7 -2 16 2.76 0.58 2 -7 16 0.52 0.37 -3 -7 0 191.99 11.73 -3 7 0 186.83 12.05 3 7 0 190.53 12.73 -7 -3 0 184.05 12.53 3 7 0 187.32 11.84 -3 7 1 1.78 0.76 -3 -7 1 3.41 0.83 -7 -3 -1 3.05 0.74 -3 -7 -1 2.35 0.59 -7 3 -1 3.13 0.82 7 3 -1 3.55 1.22 3 7 1 2.82 1.22 3 7 -1 4.36 0.86 3 7 -1 2.37 1.19 -3 7 -1 4.34 1.08 -7 -3 1 4.18 1.64 -7 3 -2 271.31 15.74 -3 7 2 251.78 15.93 -3 -7 2 278.98 16.13 3 7 -2 262.45 16.08 -7 -3 2 258.91 16.39 3 7 -2 273.17 17.04 -7 -3 -2 252.44 15.16 7 3 -2 221.40 16.17 3 -7 2 258.25 15.29 -7 -3 2 266.66 17.42 7 3 -2 248.74 15.95 3 7 2 223.37 16.03 -3 7 3 119.44 8.24 -7 3 -3 122.28 7.85 -3 -7 3 125.73 8.58 3 -7 3 120.02 7.54 -3 7 -3 119.85 8.28 3 7 -3 107.78 8.19 -7 -3 3 137.76 9.75 3 7 3 131.78 7.89 3 7 -3 113.25 9.14 7 3 -3 102.29 8.17 7 -3 3 113.66 7.48 7 3 -3 127.33 8.65 3 7 -3 114.83 8.06 3 7 3 149.22 8.29 -3 7 -3 123.82 7.94 -7 -3 3 112.47 8.59 -3 7 4 1519.92 90.76 7 3 -4 1624.50 90.95 -3 -7 4 1514.58 91.35 3 7 4 1618.97 90.32 3 -7 4 1534.20 89.92 3 7 -4 1547.49 92.12 -3 7 -4 1505.98 90.27 3 7 -4 1450.14 90.53 3 7 -4 1574.21 90.70 -7 -3 4 1467.56 91.34 -7 3 -4 1473.09 90.10 -3 7 -4 1600.84 90.91 -7 -3 4 1816.89 92.48 3 -7 4 1588.53 91.12 -3 -7 5 39.67 4.54 3 7 5 51.23 3.97 3 -7 5 45.32 3.52 7 3 -5 45.68 4.08 -7 3 -5 50.10 3.68 -3 7 -5 49.37 3.74 3 7 -5 58.20 5.44 7 3 -5 44.39 4.04 3 7 -5 57.25 4.18 -3 7 5 52.82 3.71 3 7 -5 40.57 3.96 -3 7 -5 55.81 4.47 -7 -3 5 57.27 5.18 3 -7 5 50.43 4.64 -3 7 5 49.88 4.32 -3 7 6 1053.46 60.35 3 7 -6 1070.66 60.48 3 7 -6 1062.58 60.74 7 3 -6 1017.37 60.64 7 3 -6 1050.89 60.74 -3 7 6 857.72 60.96 7 3 7 7.60 1.26 7 3 -7 7.53 1.47 3 7 -7 8.39 1.39 7 3 -7 7.37 1.41 3 7 -7 5.30 1.10 3 7 -8 4.32 1.09 7 3 8 3.88 1.11 7 3 -8 3.43 1.06 7 3 -8 4.47 1.21 7 3 -9 7.21 1.29 7 3 -9 7.07 1.41 3 7 9 7.37 1.31 7 -3 -9 5.16 1.28 7 3 9 10.23 1.57 3 7 -9 8.20 1.32 7 3 10 23.20 2.49 3 7 10 22.00 2.39 7 3 -10 18.70 2.36 3 7 -10 25.39 2.29 7 3 11 4.13 1.15 7 3 -11 3.54 1.14 3 7 11 4.50 1.12 -7 3 12 51.45 4.62 3 7 12 52.39 4.41 7 3 -12 55.40 4.38 7 3 13 -0.69 0.71 3 7 13 -0.58 0.92 3 -7 13 -0.19 0.76 -7 3 13 -0.21 0.79 3 7 14 317.56 18.40 -7 3 14 302.00 18.38 3 -7 14 315.92 18.34 7 3 14 272.11 18.14 3 7 15 5.91 0.96 3 -7 15 3.55 0.78 -7 3 15 5.06 0.91 7 -3 15 3.46 0.84 7 -3 16 41.46 2.73 3 -7 16 40.82 2.66 3 7 16 36.16 2.64 7 3 16 34.20 2.53 -4 -7 0 -0.28 0.46 -4 7 0 -0.21 0.52 -7 -4 0 -0.19 0.55 4 7 0 0.17 0.79 -7 -4 0 0.33 0.99 4 7 0 -0.46 1.29 7 4 0 -0.22 0.90 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0.93 1.00 7 -4 4 1.35 0.55 -4 -7 4 0.74 0.82 -7 4 -4 0.86 0.58 4 7 4 0.88 0.78 4 7 -4 0.98 0.93 4 -7 4 1.37 0.59 7 4 -4 1.09 1.07 -7 -4 4 0.46 1.35 -4 7 -4 1.98 0.91 -4 7 4 0.27 0.69 -7 -4 4 0.45 1.14 4 7 5 59.61 4.48 -4 7 5 57.94 4.08 -7 4 -5 47.78 4.08 4 -7 5 53.32 3.99 -4 7 -5 58.39 4.72 7 4 -5 61.47 4.75 4 7 -5 59.85 4.61 7 4 -5 60.53 4.77 4 7 -5 52.62 4.55 -4 7 5 53.32 4.80 4 7 -6 0.25 0.97 7 4 -6 0.51 1.01 -4 7 6 -0.18 0.72 4 -7 6 0.66 0.64 4 7 -6 -0.21 0.73 7 4 -6 0.24 0.96 4 7 -7 165.14 10.68 7 4 -7 160.06 10.99 7 4 -7 160.10 10.81 4 7 -7 173.27 11.03 4 7 -8 -0.23 0.73 7 4 8 -0.21 0.70 7 4 -8 0.49 0.83 4 7 8 0.59 0.68 7 4 -8 0.22 0.73 4 7 -8 -0.35 0.67 4 7 9 47.58 3.89 7 4 -9 45.87 3.88 7 4 -9 46.57 4.07 4 7 -9 51.86 4.00 7 4 9 48.07 3.98 7 4 10 15.90 1.96 7 4 -10 17.19 2.10 4 7 10 16.99 1.95 4 7 -10 15.72 1.89 4 7 11 69.99 5.01 7 4 -11 63.40 5.03 4 7 -11 64.81 4.77 7 4 11 65.50 4.98 7 4 -12 4.40 1.06 7 4 12 3.94 1.02 4 7 12 2.49 0.86 -7 4 12 3.29 1.20 4 7 13 22.82 2.25 7 4 13 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7 2 923.26 53.82 -7 -5 2 930.95 54.93 5 7 2 980.93 53.64 5 -7 2 796.28 53.51 7 -5 2 944.05 53.58 -7 -5 2 997.61 56.68 -7 -5 -2 1087.06 55.43 5 7 -2 1012.69 56.69 7 5 2 934.13 53.90 -5 7 3 101.92 8.05 7 5 -3 109.80 8.40 7 5 -3 124.79 8.28 5 7 -3 107.26 8.22 -7 5 -3 115.13 7.89 -5 7 -3 118.96 8.15 5 7 3 114.28 7.63 5 -7 3 118.52 7.39 7 5 3 114.99 7.49 -7 -5 3 106.98 8.79 7 -5 3 119.77 7.37 5 7 3 112.62 7.44 -7 -5 3 122.49 9.76 -5 -7 3 123.77 8.56 5 7 -3 136.12 10.05 -7 5 -4 621.99 37.06 7 5 -4 686.91 37.78 5 7 4 623.36 36.97 -7 -5 4 687.83 39.26 -7 -5 4 660.19 38.67 5 7 -4 658.39 39.29 5 -7 4 593.12 36.53 -5 -7 4 566.49 38.01 -5 7 -4 627.09 37.36 5 7 -4 607.71 37.34 5 7 -4 667.70 37.60 7 -5 4 608.31 36.56 -5 7 4 562.38 37.49 5 7 -5 296.44 17.33 5 7 5 268.05 17.02 -7 5 -5 248.20 16.78 7 5 -5 264.39 17.31 7 -5 5 268.56 16.55 5 -7 5 273.55 16.54 5 7 -5 260.61 17.20 7 5 -5 299.12 17.45 7 5 -6 1915.19 115.21 5 7 -6 1992.22 115.16 7 -5 6 2015.52 114.88 7 5 -6 1977.30 115.47 5 -7 6 1951.54 114.79 5 7 -6 1944.86 115.37 5 7 -7 160.07 10.69 5 -7 7 169.22 10.78 7 5 -7 146.01 10.67 7 5 -7 165.05 11.04 5 7 -7 180.42 11.10 5 7 8 26.70 2.38 5 7 -8 22.94 2.53 7 5 -8 18.25 2.44 7 5 -8 22.89 2.37 5 7 -8 21.43 2.27 5 7 9 52.60 4.13 5 7 -9 53.93 4.38 5 7 -9 52.39 4.06 7 5 -9 49.01 4.38 7 5 -9 51.34 4.22 7 5 9 59.10 4.33 7 5 -10 51.95 4.20 5 7 -10 44.95 3.94 5 7 10 48.46 3.91 7 5 10 54.59 4.11 5 7 11 34.62 3.10 5 -7 11 38.89 3.65 5 7 -11 37.51 3.15 7 5 11 40.56 3.28 7 5 -11 33.74 3.22 7 5 -12 8.71 1.36 7 5 12 9.09 1.32 5 7 12 7.42 1.25 5 -7 12 11.40 1.71 7 -5 12 5.05 1.38 5 -7 13 27.83 2.56 -7 5 13 23.20 2.55 -5 7 13 20.18 2.50 7 -5 13 23.49 2.47 7 5 13 25.51 2.25 5 7 13 28.10 2.36 -7 5 14 450.10 24.73 -5 7 14 396.75 24.69 5 -7 14 428.69 24.62 7 -5 14 411.40 24.61 7 5 14 392.97 24.33 5 7 14 391.90 24.40 -7 5 15 8.93 1.07 -5 7 15 8.69 1.10 5 -7 15 6.33 0.96 7 -5 15 7.40 1.01 5 7 15 5.88 0.83 -5 7 16 7.94 0.88 5 -7 16 8.17 0.86 7 -5 16 9.81 0.93 -6 7 0 0.50 0.76 6 7 0 0.30 0.59 7 6 0 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0.94 -9 4 -3 200.34 12.51 4 9 3 195.38 12.37 4 9 3 197.66 11.97 4 -9 3 197.26 11.97 9 4 3 200.57 12.21 9 -4 3 191.90 11.90 4 9 3 181.22 12.05 4 9 -3 178.09 12.80 9 4 -3 187.40 12.95 9 -4 4 1.45 0.67 9 4 -4 2.28 1.29 4 9 4 0.22 0.84 4 -9 4 -0.14 0.53 4 9 4 1.18 0.68 4 9 -4 0.58 1.13 9 4 -4 1.39 1.17 4 9 4 1.00 0.54 4 9 -4 0.54 1.05 4 9 5 243.20 15.00 -4 9 5 232.87 14.42 9 -4 5 220.23 14.27 4 -9 5 229.45 14.31 9 4 -5 243.30 15.38 4 9 -5 212.53 14.96 4 9 -5 247.02 15.12 9 4 -6 15.41 2.47 4 9 6 21.73 2.62 -4 9 6 17.52 2.02 4 9 -6 18.43 2.23 4 -9 6 15.82 1.89 9 4 -6 18.07 2.43 9 -4 6 15.69 1.89 4 9 -6 18.69 2.41 -4 9 7 136.97 9.51 4 9 -7 143.67 9.48 4 -9 7 141.74 9.44 9 4 -7 139.42 9.92 9 -4 7 141.19 9.44 4 9 -7 153.09 9.82 9 4 -7 127.28 9.61 9 4 -8 12.34 2.02 4 9 8 15.96 1.84 9 4 -8 11.92 1.91 9 -4 8 9.38 1.80 4 -9 8 13.41 1.98 4 9 -8 15.53 1.82 4 9 -8 12.04 1.94 4 9 9 67.47 5.26 4 9 -9 67.50 5.14 9 4 -9 79.69 5.87 4 -9 9 72.75 5.74 4 9 -9 75.30 5.49 9 -4 9 78.32 5.85 9 -4 -9 73.56 5.80 9 4 -9 74.62 5.59 9 4 -10 9.89 1.73 4 9 10 10.00 1.44 9 -4 10 5.40 1.46 9 4 -10 6.98 1.39 4 9 -10 8.49 1.38 9 -4 -10 10.14 1.67 4 -9 10 7.17 1.52 4 9 11 34.60 2.84 9 4 -11 28.45 3.03 4 9 -11 28.70 2.65 4 -9 11 32.87 3.19 9 -4 11 34.66 3.24 9 4 -12 10.60 1.52 4 9 12 9.01 1.33 -9 4 12 11.38 1.63 4 -9 12 12.07 1.68 9 -4 -12 6.86 1.31 9 -4 12 12.52 1.68 -9 4 13 59.88 4.08 -4 9 13 44.47 4.10 4 -9 13 55.33 3.98 9 -4 13 50.96 3.96 9 4 -13 51.30 3.80 4 9 13 51.33 3.80 4 9 14 0.49 0.46 -9 4 14 1.27 0.56 -4 9 14 1.35 0.86 4 -9 14 0.11 0.52 9 -4 14 0.36 0.60 9 -4 15 24.15 1.83 4 -9 15 22.32 1.77 9 5 0 4.52 1.06 -9 -5 0 3.14 1.62 5 9 0 8.31 1.46 9 5 0 6.79 1.59 5 9 0 5.71 1.08 -5 -9 1 74.87 5.81 5 9 -1 87.38 5.82 -9 -5 1 80.03 7.73 9 5 1 74.47 5.47 5 9 1 85.00 5.85 9 5 1 79.16 5.98 5 9 -1 75.44 7.77 5 9 -1 84.79 6.22 9 5 -1 72.99 5.78 9 5 -1 86.54 6.61 5 9 1 82.17 5.54 9 -5 2 1.58 0.62 9 5 -2 6.36 1.44 5 9 2 3.12 0.89 5 -9 2 3.19 0.76 5 9 2 3.56 0.97 -9 -5 2 1.99 1.17 9 5 2 2.57 0.88 9 5 -2 4.45 1.80 5 9 2 2.00 0.73 5 9 -2 1.57 0.92 5 9 -3 16.80 2.14 9 5 -3 12.89 2.20 9 -5 3 11.32 1.38 5 9 3 13.67 1.42 5 9 3 12.10 1.65 5 -9 3 12.49 1.46 9 5 3 11.41 1.49 5 9 3 9.96 1.45 5 9 -3 12.40 2.21 5 9 4 1153.97 66.51 5 9 -4 1180.30 67.08 5 9 4 1098.90 65.96 5 -9 4 1119.18 65.97 9 -5 4 1122.93 65.92 9 5 -4 1017.17 66.93 9 5 -4 1247.03 67.54 5 9 -5 4.23 1.44 5 9 5 6.74 1.57 -5 9 5 8.51 1.28 5 -9 5 7.44 1.16 9 5 -5 5.35 1.63 9 -5 5 5.76 1.09 5 9 -5 5.50 1.60 9 5 -6 283.07 18.29 9 -5 6 287.38 17.70 5 9 -6 292.12 18.09 -5 9 6 294.49 17.76 5 9 -6 292.81 18.32 5 -9 6 281.48 17.66 9 5 -6 255.06 18.29 9 5 -7 2.80 1.37 5 -9 7 3.45 1.11 5 9 -7 3.06 1.21 9 -5 7 3.66 1.18 9 5 -7 0.28 1.00 5 9 -7 1.97 1.31 9 -5 8 40.39 3.76 9 5 -8 36.30 3.66 5 9 -8 42.16 3.78 9 5 -8 39.52 3.86 5 -9 8 50.80 4.03 5 9 -8 38.18 3.44 9 5 -9 1.08 0.95 9 5 -9 1.20 0.93 5 9 -9 2.06 0.81 5 -9 9 2.79 1.20 9 -5 9 1.96 1.16 5 9 -9 2.79 1.04 9 -5 10 46.64 4.16 9 5 -10 44.54 4.09 5 9 -10 49.29 3.90 9 5 -10 48.12 3.88 9 -5 -10 39.67 3.81 5 -9 10 50.34 4.28 9 5 -11 8.46 1.54 5 -9 11 9.22 1.71 9 -5 11 9.96 1.70 5 9 -11 6.16 1.18 -9 5 12 139.57 8.66 5 -9 12 142.44 8.59 9 5 -12 119.13 8.29 9 -5 12 123.17 8.42 9 -5 -12 110.32 8.11 -9 5 13 9.63 1.42 5 -9 13 10.96 1.44 9 -5 13 10.20 1.45 -9 5 14 119.64 7.33 5 -9 14 109.33 7.28 9 -5 14 114.75 7.34 9 -5 15 1.68 0.48 5 -9 15 1.83 0.45 9 6 0 0.19 0.69 6 9 0 0.25 0.84 9 6 0 1.13 1.14 6 9 0 0.72 0.74 9 6 1 9.81 1.34 9 6 -1 7.74 1.47 9 6 1 10.92 1.72 6 9 1 9.02 1.38 6 9 -1 10.74 1.93 6 9 1 8.85 1.48 9 6 -1 11.28 2.03 6 9 1 11.64 1.46 6 9 -1 9.69 1.52 6 9 -2 1.43 0.88 9 6 -2 0.26 0.92 6 9 2 0.95 0.75 9 -6 2 -0.13 0.52 6 -9 2 0.14 0.59 6 9 2 2.30 0.98 9 6 2 1.65 0.85 9 6 -2 -0.37 1.44 6 9 2 1.65 0.70 9 6 -3 36.91 3.77 6 9 3 39.36 3.38 6 9 3 37.01 3.15 6 -9 3 35.90 3.00 9 -6 3 40.46 3.07 9 6 3 38.96 3.20 6 9 -3 38.16 3.98 6 9 3 39.59 3.00 6 9 -3 35.18 3.62 9 6 -4 3.72 1.63 9 6 -4 -0.34 1.40 6 9 4 0.49 0.83 -6 9 4 0.65 0.65 6 -9 4 0.98 0.68 6 9 -4 2.69 1.47 6 9 4 1.13 0.68 9 -6 4 1.42 0.71 6 9 -5 0.65 1.13 6 9 5 1.14 1.22 6 9 -5 0.31 1.11 9 -6 5 1.07 0.78 6 -9 5 -0.18 0.72 9 6 -5 1.71 1.41 6 9 -6 27.98 3.31 6 9 -6 32.57 3.27 6 -9 6 25.82 2.74 9 6 -6 25.69 3.17 6 9 -7 34.71 3.51 9 6 -7 34.34 3.57 9 -6 7 28.39 3.03 6 9 -7 34.67 3.28 9 6 -7 27.64 3.18 6 -9 7 32.10 3.17 9 6 -8 0.30 1.11 6 -9 8 0.55 1.13 9 -6 8 1.89 1.14 6 9 -8 1.57 1.04 9 6 -8 -0.26 1.07 6 9 -8 -0.81 1.18 9 6 -9 -0.55 0.92 6 9 -9 -0.20 0.71 9 6 -9 0.24 0.89 6 -9 9 -0.29 1.11 9 -6 9 -0.28 1.04 6 9 -9 0.48 0.91 9 6 -10 3.43 1.28 9 6 -10 2.87 1.03 6 -9 10 3.84 1.52 9 -6 10 0.82 1.20 9 -6 -10 2.27 1.09 6 9 -10 4.00 1.06 9 6 -11 46.72 3.76 6 -9 11 47.48 3.93 6 9 -11 35.64 3.36 9 -6 11 48.49 4.01 9 6 -12 20.34 2.01 -9 6 12 20.52 2.31 9 -6 -12 14.58 1.79 6 -9 12 20.02 2.19 9 -6 12 22.74 2.29 -9 6 13 5.46 1.13 -6 9 13 7.30 1.32 6 -9 13 8.55 1.25 9 -6 13 8.76 1.30 -9 6 14 -0.32 0.50 -6 9 14 0.63 0.64 6 -9 14 -0.42 0.52 9 -6 14 -0.11 0.52 -6 9 15 15.54 1.35 6 -9 15 15.70 1.27 9 -6 15 15.98 1.29 7 9 0 1103.24 63.92 9 7 0 1129.39 64.11 7 9 0 1008.55 63.26 7 9 0 1079.24 63.40 9 7 0 1101.55 63.45 7 9 -1 135.52 8.88 7 9 1 110.49 7.86 7 9 1 120.00 8.22 9 7 -1 122.84 8.21 7 9 1 106.41 7.73 9 7 1 114.06 8.24 9 7 -1 127.98 8.89 9 7 1 122.18 7.86 7 9 -1 119.14 8.11 9 7 2 672.51 41.41 7 9 2 638.78 41.33 7 9 2 712.76 41.14 7 9 -2 696.67 42.37 9 7 -2 708.32 42.52 7 9 -2 736.64 41.79 9 7 -2 714.25 41.85 7 9 2 697.03 41.40 7 9 3 272.56 17.39 7 9 3 283.50 17.14 9 -7 3 267.39 16.94 7 9 -3 290.13 17.87 9 7 3 275.06 17.14 9 7 -3 277.47 17.94 7 9 -4 20.13 2.72 9 -7 4 15.71 1.87 9 7 -4 17.07 2.60 7 9 4 15.64 2.26 7 9 4 18.54 1.88 7 9 -4 14.86 2.54 9 7 -4 19.54 3.05 9 -7 5 260.91 15.87 7 9 -5 274.55 16.80 9 7 -5 270.69 16.88 7 9 -6 26.33 3.32 9 -7 6 32.54 2.92 7 -9 6 24.66 2.75 7 9 -6 25.82 3.06 9 7 -6 32.95 3.53 9 7 -7 128.66 9.00 9 7 -7 113.80 8.57 7 -9 7 118.75 8.46 9 -7 7 115.57 8.38 7 9 -7 127.61 8.85 7 9 -7 118.64 8.49 9 7 -8 239.08 14.99 9 -7 8 209.67 14.73 9 7 -8 231.71 14.63 7 -9 8 207.16 14.72 7 9 -8 222.26 14.47 7 9 -8 250.39 14.91 9 -7 9 77.53 6.78 7 -9 9 91.81 6.96 7 9 -9 97.53 6.56 9 7 -9 95.87 6.68 7 9 -9 85.83 6.66 9 7 -9 96.25 6.92 9 7 -10 566.47 33.54 9 -7 10 582.23 33.83 7 -9 10 561.84 33.78 7 9 -10 561.09 33.09 9 7 -10 562.15 33.26 7 9 -10 568.48 33.41 9 -7 -10 494.78 33.22 7 -9 11 38.85 3.62 9 -7 11 43.19 3.69 7 9 -11 38.82 3.27 9 7 -11 39.27 3.41 7 9 -12 20.81 1.91 7 -9 12 19.75 2.16 9 -7 -12 18.70 1.88 9 -7 12 22.21 2.25 9 7 -12 19.65 1.94 -9 7 13 18.96 1.97 -7 9 13 19.66 2.07 9 -7 13 17.74 1.89 -9 7 14 1.05 0.48 -7 9 14 0.11 0.56 7 -9 14 -0.37 0.45 9 -7 14 0.57 0.51 9 8 0 -0.41 0.70 9 8 0 0.60 1.07 8 9 0 -0.29 1.01 8 9 0 -0.20 0.70 9 8 -1 163.03 10.91 8 9 1 145.88 10.19 8 9 1 141.44 9.99 8 9 1 155.90 9.85 8 9 -1 163.96 10.87 9 8 1 142.77 10.21 9 8 1 146.16 9.80 8 9 -1 157.17 10.17 9 8 -1 154.76 10.19 8 9 -2 1.62 1.18 9 8 -2 1.94 1.12 8 9 2 2.18 0.98 8 9 -2 0.38 1.53 8 9 2 1.75 0.89 9 8 2 -0.22 0.75 8 9 2 1.31 0.68 9 8 -2 -0.78 1.36 9 8 2 1.42 0.68 8 9 -3 259.83 15.98 8 -9 3 212.04 14.84 9 -8 3 244.63 14.98 8 9 3 244.46 15.13 9 8 3 245.43 15.13 9 8 -3 260.23 15.96 8 9 -4 3.83 1.66 9 8 -4 6.39 1.84 8 9 4 4.27 0.99 9 -8 4 5.86 1.24 8 9 -4 8.51 2.13 9 8 -4 4.77 1.77 9 8 -5 142.20 11.36 9 -8 5 159.32 10.68 8 9 -5 172.44 11.60 9 8 -5 185.84 11.85 8 9 -6 2.12 1.54 9 8 -6 0.33 1.23 9 -8 6 1.88 1.21 8 9 -6 0.94 1.18 9 8 -7 92.86 7.03 8 9 -7 88.15 6.91 9 -8 7 90.40 6.60 9 8 -7 83.61 6.65 8 9 -7 81.06 6.52 8 9 -8 0.86 1.18 9 8 -8 -0.60 1.21 9 8 -8 -0.51 1.07 8 9 -8 0.48 0.95 9 -8 8 1.42 1.37 9 -8 9 131.62 9.47 9 8 -9 130.25 9.05 8 9 -9 138.87 9.28 8 9 -9 129.20 9.00 9 8 -9 145.39 9.42 9 8 -10 2.65 1.20 9 8 -10 1.81 0.86 8 9 -10 1.89 0.84 9 -8 10 2.62 1.37 8 9 -10 4.45 1.23 9 -8 11 57.98 4.45 8 9 -11 55.25 4.09 9 8 -11 47.18 4.03 9 -8 12 -0.17 0.77 8 9 -12 -0.38 0.59 8 -9 12 0.34 0.85 9 8 -12 0.67 0.60 -9 8 13 42.98 3.18 -8 9 13 43.30 3.25 8 -9 13 40.15 3.06 9 -8 13 37.40 3.05 -9 8 14 2.75 0.57 -8 9 14 2.43 0.56 8 -9 14 2.46 0.55 9 -8 14 1.99 0.54 9 9 0 731.13 45.32 9 9 0 765.32 44.76 9 9 -1 0.24 0.84 9 9 -1 0.36 1.32 9 9 1 1.84 1.13 9 9 1 0.19 0.69 9 9 -2 110.94 9.06 9 9 2 126.12 7.93 9 9 2 124.31 8.26 9 9 -2 106.56 8.40 9 9 -3 1.31 1.33 9 9 3 1.04 0.78 9 -9 4 111.99 7.83 9 9 -4 118.65 9.13 9 9 -4 119.50 8.79 9 9 -5 0.75 1.30 9 -9 5 -0.43 0.90 9 9 -5 -0.37 1.54 9 -9 6 31.61 3.11 9 9 -6 29.17 3.40 9 9 -7 -0.28 0.98 9 -9 7 -0.54 1.04 9 -9 8 282.51 18.19 9 9 -8 276.24 17.90 9 9 -8 293.02 18.24 9 -9 9 -0.56 1.19 9 9 -9 0.41 0.85 9 9 -9 -0.49 1.05 9 9 -10 190.96 12.10 9 9 -10 192.67 12.34 9 9 -11 0.16 0.68 9 9 -12 29.51 2.35 -9 9 13 -0.71 0.66 0 10 0 636.30 40.97 0 10 0 669.00 40.43 0 10 0 664.74 43.85 0 10 0 682.76 40.10 -10 0 0 775.58 43.20 0 10 -1 0.84 1.72 -10 0 1 1.21 1.44 0 10 1 1.27 0.84 0 10 1 -0.19 0.76 0 10 -1 0.76 1.05 0 10 1 -0.16 0.63 0 10 -2 105.25 7.45 10 0 2 94.27 7.16 0 10 2 91.09 6.66 0 10 2 94.95 7.39 0 10 -2 102.63 6.94 0 10 -3 0.30 1.16 0 -10 3 0.22 0.39 0 10 -3 1.63 1.02 0 10 -4 1.42 1.05 0 10 4 1.05 0.79 0 -10 4 1.30 0.55 0 10 -4 3.62 1.25 0 10 5 -0.67 0.90 0 -10 5 -0.13 0.54 0 10 -5 0.74 0.91 0 10 -5 0.81 1.01 10 0 -5 -0.33 1.26 0 10 6 764.31 46.03 10 0 -6 735.11 46.37 0 10 -6 777.24 45.80 0 -10 6 790.51 45.48 0 10 -6 755.78 46.19 10 0 6 774.93 45.41 0 10 7 -0.28 1.09 0 10 -7 0.23 0.89 0 -10 7 0.69 0.68 0 10 -7 0.84 0.74 10 0 -7 -0.30 1.09 10 0 7 0.35 0.63 0 10 -8 559.23 31.76 0 -10 8 507.88 31.66 10 0 -8 513.24 32.24 10 0 -9 -0.28 1.02 0 -10 9 -0.42 0.80 10 0 -9 -0.27 0.85 10 0 -10 25.42 2.89 0 -10 10 28.26 2.58 10 0 -10 22.42 2.60 10 0 -11 -0.50 1.01 0 -10 11 0.36 0.66 10 0 -12 23.99 2.55 0 10 12 25.19 2.67 0 -10 12 25.10 2.29 10 0 12 29.30 2.52 10 0 -13 0.71 0.59 0 10 13 -0.37 0.87 10 0 13 -0.26 0.54 0 10 14 223.02 13.08 10 0 14 203.48 12.72 0 10 15 -0.27 0.45 1 10 0 0.36 0.74 -1 10 0 0.30 0.62 1 10 0 0.65 0.86 1 10 0 0.16 0.66 1 10 0 -0.58 1.30 10 1 0 2.22 1.53 -10 -1 0 0.71 1.78 1 10 -1 18.77 2.69 1 10 1 18.75 2.57 -1 10 1 13.92 2.18 -1 10 -1 23.79 2.63 1 10 1 19.19 2.11 -1 10 -1 22.98 2.20 1 10 1 20.00 1.99 1 10 -1 25.22 4.04 10 1 1 25.15 2.85 10 1 -1 20.17 3.18 -10 -1 1 21.12 3.86 1 10 -2 12.05 2.84 -1 10 2 5.76 1.40 -1 10 -2 11.54 1.94 -10 -1 2 4.31 2.23 1 10 -2 9.93 1.85 1 10 2 8.70 1.30 1 10 2 8.54 1.21 -1 10 -2 7.61 1.39 1 10 -2 6.59 1.39 10 1 2 8.97 1.56 10 1 -2 15.06 2.73 -1 10 3 108.52 8.57 1 10 -3 119.37 8.58 1 -10 3 117.00 7.54 -1 10 -3 125.78 8.70 -1 10 -3 129.12 8.33 1 10 3 113.39 7.80 1 10 -3 118.73 8.24 10 -1 4 13.90 1.41 1 10 4 18.20 2.11 10 1 -4 16.97 2.62 -1 10 -4 15.61 2.22 1 -10 4 15.44 1.54 -1 10 -4 16.42 2.19 1 10 -4 14.47 2.24 1 10 -4 15.38 2.15 1 10 5 9.44 1.63 -1 10 5 7.43 1.40 -1 10 -5 9.83 1.61 1 10 -5 10.65 1.74 1 -10 5 9.91 1.25 -1 10 -5 4.97 1.43 10 -1 5 9.28 1.13 1 10 -5 8.75 1.64 10 1 -5 9.72 1.98 1 10 -6 0.45 0.88 1 10 6 -0.26 0.99 -1 10 6 0.69 0.87 -1 10 -6 -0.38 0.74 1 -10 6 -0.16 0.56 -1 10 -6 1.22 1.03 1 10 -6 -0.27 0.98 10 -1 6 0.46 0.65 10 1 -6 0.31 1.20 10 -1 -6 -0.31 1.09 1 10 7 8.57 1.75 -1 10 7 9.94 1.77 10 1 -7 6.44 1.68 10 -1 7 9.15 1.37 1 10 -7 11.37 1.48 1 -10 7 8.52 1.31 -1 10 -7 9.72 1.52 1 10 -7 7.55 1.47 10 -1 -7 8.77 1.87 10 1 -8 0.85 1.19 -1 10 -8 0.69 0.73 1 -10 8 0.84 0.87 1 10 -8 0.85 0.80 10 1 -8 0.56 1.09 10 -1 -8 0.58 1.04 10 -1 8 0.66 0.74 1 -10 9 2.91 1.08 10 1 -9 5.65 1.56 1 10 -9 9.16 1.31 10 1 -9 6.95 1.46 10 -1 -9 3.57 1.33 10 -1 9 8.66 1.50 10 1 -10 6.81 1.50 10 -1 -10 10.39 1.74 1 -10 10 5.48 1.34 10 -1 -10 7.12 1.43 10 1 -10 6.75 1.40 10 -1 10 6.43 1.42 1 10 11 72.77 5.56 10 1 -11 73.08 5.58 1 -10 11 69.70 5.24 10 -1 11 74.97 5.43 10 -1 -11 67.17 5.51 10 1 -12 19.72 2.24 1 10 12 19.36 2.27 10 -1 -12 20.37 2.25 -1 10 12 24.61 2.64 1 -10 12 23.52 2.14 10 1 12 20.49 2.08 10 -1 12 20.99 2.19 10 1 -13 0.57 0.68 10 -1 -13 -0.28 0.56 1 10 13 0.34 0.71 -1 10 13 0.97 0.86 1 -10 13 0.12 0.54 10 -1 13 0.41 0.58 10 1 13 0.97 0.59 1 10 14 6.97 1.05 -1 10 14 5.91 1.06 10 1 14 3.83 0.69 10 -1 14 4.18 0.71 1 10 15 10.71 1.09 -1 10 15 12.47 1.23 2 10 0 1560.17 92.14 10 2 0 1459.56 90.66 2 10 0 1618.55 90.86 2 10 0 1521.70 90.46 10 2 0 1649.47 91.71 10 2 -1 9.15 2.19 10 2 1 9.21 1.32 -2 -10 1 9.11 1.51 2 10 1 6.06 1.68 2 10 -1 9.27 2.01 2 10 1 8.92 1.42 2 10 1 10.53 1.33 -10 -2 1 12.59 3.22 -2 10 -1 14.91 1.72 2 10 -1 5.25 1.90 2 10 -1 7.76 1.29 10 2 1 10.08 1.85 -10 2 -1 12.42 1.60 10 -2 2 5.17 0.71 2 10 2 2.70 0.76 2 10 2 1.05 0.73 -2 10 -2 0.66 0.74 -10 -2 2 2.11 1.68 2 10 -2 0.29 1.09 2 10 -2 1.82 1.45 10 2 2 0.91 0.93 10 2 -2 1.68 1.70 10 -2 3 0.32 0.41 2 -10 3 2.03 0.65 2 10 -3 0.30 1.31 2 10 3 0.33 0.63 2 10 3 0.46 0.61 -2 10 -3 1.46 0.94 2 10 -3 0.24 0.93 2 -10 4 380.31 22.21 2 10 -4 387.20 23.21 -2 10 -4 341.52 22.88 10 -2 4 366.21 22.05 2 10 -4 356.35 22.96 10 2 -4 387.35 23.75 2 10 -5 12.13 2.07 -2 10 5 14.31 1.80 2 10 -5 13.23 2.02 10 2 -5 16.61 2.50 2 -10 5 12.69 1.50 -2 10 -5 16.78 2.13 10 -2 5 13.43 1.48 2 10 6 432.62 30.44 -2 10 6 500.36 30.16 2 10 -6 542.63 30.40 -2 10 -6 531.98 30.32 2 -10 6 480.33 29.84 2 10 -6 499.75 30.54 10 -2 6 497.12 29.82 10 2 -6 511.59 30.76 10 2 -7 7.95 1.64 2 10 7 5.41 1.77 10 2 -7 5.40 1.47 -2 10 7 5.57 1.45 -2 10 -7 2.14 0.87 2 10 -7 3.05 1.07 2 -10 7 3.36 0.99 2 10 -7 6.40 1.45 10 -2 7 4.75 1.08 10 2 -8 109.48 7.74 10 -2 -8 99.32 7.69 10 2 -8 108.56 7.80 10 -2 8 111.50 7.45 2 -10 8 93.83 7.21 2 10 -8 105.45 7.07 2 10 -8 102.50 7.34 10 2 -9 0.85 0.99 2 -10 9 0.24 0.92 10 2 -9 -0.27 0.92 2 10 -9 -0.20 0.72 10 -2 -9 1.97 1.14 10 -2 9 0.75 1.05 2 10 10 75.88 5.57 -10 2 10 81.48 5.52 10 2 -10 66.21 5.60 10 -2 -10 67.45 5.51 2 -10 10 68.89 5.48 10 -2 10 67.60 5.54 2 10 -10 74.58 5.12 10 2 -10 72.69 5.49 10 2 -11 0.73 0.93 2 10 11 1.46 0.90 10 -2 -11 0.98 1.00 2 -10 11 1.66 0.98 10 -2 11 0.66 0.91 10 2 -12 12.72 1.63 2 10 12 9.59 1.44 -2 10 12 7.74 1.66 10 -2 -12 9.85 1.54 2 -10 12 10.22 1.41 10 -2 12 10.42 1.51 10 2 12 8.65 1.25 10 2 -13 5.83 1.02 2 10 13 7.24 1.15 -2 10 13 7.48 1.35 2 -10 13 7.05 1.05 10 -2 13 4.63 1.06 -2 10 14 168.53 9.69 2 -10 14 139.58 9.21 10 -2 14 147.36 9.32 2 10 14 158.82 9.44 -2 10 15 0.48 0.46 10 -2 15 -0.12 0.28 3 10 0 -0.57 1.08 10 3 0 -0.61 0.91 3 10 0 -0.46 0.92 10 3 0 0.33 1.28 3 10 0 0.69 0.68 10 3 -1 26.14 2.69 10 3 1 22.97 2.19 3 10 -1 19.18 3.41 3 10 1 22.14 2.36 10 3 1 27.42 2.79 3 10 1 25.86 2.27 3 10 -1 23.46 2.35 10 3 -1 26.55 3.38 3 10 -1 22.38 2.70 -3 -10 1 20.76 2.41 -10 3 -1 21.89 2.46 10 3 -2 29.63 3.09 3 10 2 26.60 2.37 3 10 2 30.06 2.32 10 -3 2 28.65 2.05 3 10 -2 27.32 3.03 10 3 2 23.39 2.47 10 3 -2 27.06 3.45 3 10 3 172.89 10.51 3 -10 3 157.03 9.88 3 10 3 142.94 10.01 10 -3 3 157.16 9.78 3 10 3 164.22 10.01 3 10 -3 157.52 10.92 10 3 3 157.66 10.19 10 3 -3 143.48 10.89 10 3 -4 8.01 1.83 3 10 4 7.62 1.50 3 -10 4 6.82 1.05 3 10 -4 7.99 1.76 10 -3 4 5.57 0.95 10 3 -4 5.31 1.87 3 10 -4 6.14 1.59 3 10 4 7.44 1.18 3 10 5 179.07 11.87 -3 10 5 170.79 11.40 10 -3 5 183.14 11.17 3 -10 5 169.47 11.16 3 10 -5 165.08 11.89 10 3 -5 183.00 12.37 10 3 -5 193.02 12.42 3 10 -5 178.65 11.93 -3 10 6 0.65 0.71 3 -10 6 1.83 0.77 3 10 -6 2.99 1.15 10 -3 6 0.88 0.66 10 3 -6 1.59 1.40 3 10 -6 0.29 1.08 -3 10 7 123.83 9.15 10 -3 7 133.52 9.00 3 -10 7 140.09 9.10 10 3 -7 116.10 9.56 10 3 -7 132.13 9.46 3 10 -7 150.45 9.49 3 10 -7 141.77 9.13 10 3 -8 2.40 1.32 3 10 -8 0.72 0.89 3 10 -8 2.65 0.95 3 -10 8 1.19 1.03 10 3 -8 2.53 1.21 10 -3 8 3.37 1.17 10 -3 -8 1.23 1.28 3 10 9 26.60 2.56 10 3 -9 22.51 2.81 3 -10 9 22.98 2.63 10 3 -9 21.96 2.60 3 10 -9 25.43 2.52 10 -3 9 21.18 2.61 10 -3 -9 25.29 2.84 3 10 10 25.96 2.53 10 3 -10 25.87 2.89 3 10 -10 27.05 2.48 3 -10 10 27.45 2.83 10 3 -10 23.37 2.60 10 -3 -10 23.78 2.66 10 -3 10 26.51 2.87 3 10 11 42.00 3.28 -10 3 11 40.60 3.42 3 -10 11 38.65 3.42 10 -3 11 37.97 3.46 10 3 -11 37.39 3.48 10 -3 -11 33.21 3.43 10 3 -12 4.65 1.13 3 10 12 4.77 1.00 -10 3 12 4.77 1.05 10 -3 -12 5.65 1.15 3 -10 12 2.12 0.86 10 -3 12 4.42 1.06 10 3 -13 6.96 1.07 3 10 13 7.02 1.07 -3 10 13 8.75 1.44 3 -10 13 7.34 1.07 10 -3 13 10.90 1.31 -3 10 14 1.39 0.78 3 -10 14 0.64 0.48 10 -3 14 0.80 0.49 -3 10 15 27.95 2.03 10 -3 15 23.74 1.81 4 10 0 187.86 11.93 4 10 0 189.02 12.29 10 4 0 194.06 12.77 10 4 0 182.10 12.02 10 4 -1 138.89 9.07 4 10 1 116.18 8.46 4 10 -1 146.45 9.34 10 4 -1 141.65 9.87 10 4 1 139.67 9.21 4 10 1 120.70 8.70 4 10 -1 126.11 8.72 10 4 1 134.88 8.56 4 10 2 171.82 12.09 4 10 2 186.68 11.97 10 -4 2 200.44 11.81 4 10 -2 198.49 12.50 10 4 2 192.46 12.40 10 4 -2 189.65 13.40 10 4 -2 199.81 12.86 10 4 -3 18.61 2.58 10 -4 3 17.25 1.70 4 10 3 17.26 2.15 4 -10 3 15.66 1.71 4 10 -3 22.30 2.84 4 10 3 17.49 1.92 4 10 3 17.37 1.80 10 4 3 19.40 2.01 4 10 4 598.33 35.77 4 -10 4 589.73 35.19 10 -4 4 579.65 35.12 4 10 4 598.45 35.29 4 10 -4 635.44 36.36 4 10 -4 570.27 36.03 10 4 -4 581.81 36.65 10 4 -4 603.61 36.49 10 4 -5 25.19 3.23 4 10 5 27.61 3.00 -4 10 5 19.31 2.31 4 -10 5 29.36 2.51 10 -4 5 26.59 2.38 4 10 5 33.01 2.51 4 10 -5 25.42 2.95 4 10 -5 18.17 2.76 10 4 -5 25.39 3.21 10 4 -6 7.85 1.80 4 10 -6 11.76 2.04 4 10 6 8.39 1.88 -4 10 6 10.95 1.60 10 -4 6 9.99 1.49 4 10 -6 11.04 1.74 4 -10 6 11.35 1.55 10 4 -7 36.10 3.80 -4 10 7 37.77 3.44 4 -10 7 30.15 3.12 10 -4 7 32.59 3.12 4 10 -7 33.86 3.26 4 10 -7 42.54 3.73 10 4 -7 34.29 3.56 4 -10 8 3.27 1.23 10 4 -8 3.35 1.53 10 4 -8 0.83 1.10 10 -4 8 2.49 1.12 4 10 -8 0.25 1.17 10 4 -9 27.90 2.97 4 -10 9 22.72 2.77 4 10 -9 24.36 2.38 10 4 -9 25.61 2.76 10 -4 9 28.83 2.98 4 10 -9 25.23 2.62 10 -4 -9 24.81 2.87 4 10 10 247.26 15.30 10 -4 10 266.00 15.93 4 10 -10 244.53 15.38 10 4 -10 238.04 15.57 4 -10 10 249.65 15.86 10 -4 -10 221.94 15.59 10 4 -10 266.29 15.95 10 4 -11 10.02 1.73 4 10 11 10.55 1.45 4 -10 11 16.05 2.02 10 -4 11 13.05 1.88 4 10 -11 15.57 1.58 -10 4 12 30.48 2.66 10 -4 -12 27.92 2.60 10 -4 12 24.22 2.53 4 -10 12 27.27 2.60 10 4 -12 29.24 2.66 10 4 -13 6.44 0.97 -10 4 13 7.54 1.07 -4 10 13 6.57 1.24 10 -4 13 6.68 1.11 4 -10 13 7.01 1.08 -4 10 14 19.21 1.78 4 -10 14 16.40 1.49 10 -4 14 16.46 1.53 -4 10 15 1.52 0.48 10 5 0 0.20 0.75 5 10 0 -0.26 0.86 10 5 0 -0.63 1.09 5 10 0 -0.19 0.72 5 10 1 26.39 2.38 10 5 -1 25.46 2.67 10 5 1 27.19 2.37 5 10 -1 24.46 2.95 10 5 1 21.70 2.64 10 5 -1 33.36 3.61 5 10 1 23.55 2.53 5 10 -1 20.86 2.42 10 5 -2 -0.87 1.07 5 10 2 0.20 0.73 5 10 2 0.84 0.81 10 -5 2 0.27 0.49 10 5 -2 -1.24 1.59 10 5 2 -0.22 0.79 5 10 2 0.49 0.68 5 10 -2 0.73 0.98 10 5 -3 1.68 1.50 5 10 3 3.19 1.06 10 5 -3 2.54 1.89 5 -10 3 2.75 0.86 10 -5 3 1.13 0.71 5 10 3 1.83 0.81 5 10 -3 2.42 1.52 5 10 3 2.73 0.76 10 5 3 1.34 0.83 5 10 -3 2.80 1.38 10 5 -4 0.73 1.30 5 10 4 -0.26 1.01 10 -5 4 0.16 0.60 5 -10 4 0.66 0.65 5 10 4 1.21 0.71 10 5 -4 -1.61 1.98 5 10 -4 -0.67 1.48 5 10 4 0.72 0.54 10 5 -5 29.18 3.54 -5 10 5 28.44 2.70 5 10 5 29.19 3.28 5 -10 5 26.90 2.60 10 -5 5 32.29 2.71 5 10 -5 33.22 3.44 10 5 -5 37.95 3.86 5 10 -5 19.78 3.02 5 -10 6 6.30 1.29 -5 10 6 6.25 1.29 10 5 -6 2.99 1.59 5 10 -6 5.27 1.51 10 -5 6 5.64 1.17 5 10 -6 7.29 1.80 10 5 -7 4.64 1.62 5 -10 7 4.77 1.31 5 10 -7 4.17 1.26 10 -5 7 4.18 1.23 10 5 -7 4.78 1.48 5 10 -7 2.64 1.23 10 5 -8 5.18 1.68 5 10 -8 9.07 1.46 5 -10 8 7.94 1.67 10 -5 8 7.54 1.60 10 5 -8 7.06 1.60 5 10 -8 9.43 1.72 10 5 -9 11.40 1.96 5 10 -9 9.92 1.52 5 -10 9 13.72 2.13 10 5 -9 10.87 1.78 10 -5 9 13.02 2.08 5 10 -9 12.81 1.86 10 -5 -9 15.56 2.14 10 5 -10 1.26 1.19 5 -10 10 2.34 1.28 10 5 -10 2.14 1.01 10 -5 10 2.06 1.28 5 10 -10 3.53 0.99 10 -5 -10 2.86 1.09 10 5 -11 3.69 1.18 5 -10 11 2.24 1.13 10 -5 11 2.46 1.11 5 10 -11 2.22 0.80 10 5 -12 5.71 1.15 -10 5 12 10.56 1.43 10 -5 -12 6.33 1.17 5 -10 12 8.76 1.43 10 -5 12 6.45 1.23 -10 5 13 28.04 2.20 -5 10 13 20.24 2.28 5 -10 13 27.91 2.26 10 -5 13 25.76 2.24 10 5 -13 22.96 2.04 10 -5 14 1.12 0.52 5 -10 14 1.23 0.50 10 6 0 128.18 9.05 6 10 0 145.30 9.59 6 10 0 133.38 9.07 10 6 0 148.02 9.85 10 6 1 0.35 0.64 10 6 -1 -0.24 0.91 6 10 1 -0.41 0.76 6 10 1 1.08 0.71 6 10 -1 0.31 1.21 6 10 1 -0.24 0.84 10 6 -1 -0.73 1.47 10 6 1 1.83 1.01 6 10 -1 0.44 0.88 6 10 2 519.18 34.67 10 6 -2 602.52 36.06 6 10 2 607.21 34.52 6 10 2 564.96 34.69 6 10 -2 577.67 35.01 10 6 2 580.03 34.81 10 6 -2 617.19 35.30 10 6 -3 20.61 2.76 6 10 3 19.65 1.94 6 10 3 20.96 2.36 6 -10 3 18.11 1.94 10 -6 3 19.13 1.90 6 10 3 16.33 1.96 6 10 -3 14.58 2.74 10 6 3 19.61 2.10 10 6 -3 19.06 3.28 6 10 -3 22.45 2.67 6 10 4 398.69 24.99 -6 10 4 415.42 24.56 6 -10 4 418.19 24.47 10 -6 4 385.22 24.38 6 10 4 399.99 24.46 6 10 -4 451.92 25.78 10 6 -4 372.16 25.42 10 6 -5 2.61 1.60 6 10 5 -0.31 1.37 -6 10 5 -0.20 0.67 10 -6 5 0.19 0.66 6 -10 5 1.57 0.98 6 10 -5 0.65 1.29 10 6 -5 0.37 1.50 6 10 -5 -0.34 1.43 6 10 -6 12.23 2.01 6 -10 6 17.52 2.08 10 -6 6 11.83 1.72 10 6 -6 10.99 2.26 6 10 -6 12.24 2.21 10 6 -7 -0.67 1.26 6 -10 7 0.76 0.98 6 10 -7 -0.26 0.89 10 -6 7 1.71 1.09 10 6 -7 0.90 1.15 6 10 -7 3.05 1.38 10 6 -8 2.76 1.40 6 10 -8 2.93 1.07 6 -10 8 3.31 1.38 10 -6 8 0.81 1.02 10 6 -8 5.68 1.41 6 10 -8 3.80 1.40 10 6 -9 9.38 1.89 6 10 -9 7.40 1.34 10 -6 9 11.83 1.97 6 -10 9 7.58 1.69 10 6 -9 9.84 1.61 6 10 -9 10.10 1.67 6 -10 10 527.83 30.17 10 -6 10 508.24 30.11 10 6 -10 480.55 29.66 10 6 -10 498.60 29.95 10 -6 -10 459.79 29.79 6 10 -10 490.81 29.67 10 6 -11 1.03 0.88 6 10 -11 -0.16 0.64 6 -10 11 0.67 1.09 10 -6 11 0.22 0.92 -10 6 12 23.01 2.21 10 -6 -12 14.61 1.79 10 6 -12 21.88 2.04 6 -10 12 20.49 2.13 10 -6 12 20.10 2.11 10 -6 13 -0.38 0.63 -10 6 13 0.25 0.62 6 -10 13 0.50 0.62 6 -10 14 0.08 0.37 10 -6 14 0.84 0.44 10 7 0 -0.42 0.79 7 10 0 0.41 0.72 7 10 0 0.57 1.05 10 7 0 1.57 1.35 7 10 0 0.82 0.81 7 10 1 61.72 5.06 7 10 -1 61.21 5.01 7 10 -1 73.37 5.91 7 10 -1 73.05 5.37 7 10 1 69.89 5.09 7 10 1 67.65 5.37 10 7 1 71.61 5.56 10 7 -1 68.37 5.98 10 7 -1 74.83 5.47 10 7 1 71.80 5.05 10 7 -2 6.08 1.57 7 10 2 4.88 1.17 7 10 2 4.20 1.23 7 10 -2 2.58 1.64 10 7 2 5.34 1.28 10 7 -2 5.32 1.91 7 10 2 5.01 1.03 7 10 -2 5.93 1.53 7 10 3 46.47 3.48 7 10 3 42.42 3.89 10 -7 3 40.15 3.46 7 10 3 44.27 3.65 10 7 3 44.63 3.69 7 10 -3 53.31 4.46 10 7 -3 47.74 4.43 10 7 -3 37.61 4.63 10 7 -4 4.82 1.80 7 10 4 3.15 1.24 10 -7 4 3.42 0.98 7 10 -4 2.25 1.49 7 10 4 2.77 0.85 7 -10 4 2.80 0.96 7 10 -4 2.72 1.52 10 7 -5 18.71 2.94 7 -10 5 23.87 2.45 10 -7 5 22.72 2.39 10 7 -5 23.46 3.16 7 10 -5 28.45 3.30 7 -10 6 1.64 1.16 10 -7 6 1.61 0.97 7 10 -6 1.52 1.33 10 7 -6 3.39 1.46 7 10 -6 2.05 1.44 10 7 -7 21.07 2.96 7 -10 7 21.72 2.55 10 7 -7 17.99 2.60 10 -7 7 19.51 2.53 7 10 -7 21.82 2.60 7 10 -7 21.36 2.79 10 7 -8 -0.30 1.12 10 -7 8 0.55 1.16 7 -10 8 -0.57 1.02 7 10 -8 0.46 0.89 10 7 -8 0.27 1.02 7 10 -8 0.83 1.02 10 7 -9 20.06 2.53 10 7 -9 17.50 2.25 7 -10 9 18.47 2.52 7 10 -9 22.21 2.22 10 -7 9 19.06 2.59 7 10 -9 18.57 2.29 10 7 -10 11.53 1.81 7 10 -10 14.05 1.83 10 -7 10 16.65 2.13 10 7 -10 12.42 1.68 10 -7 -10 11.45 1.78 10 7 -11 22.84 2.52 7 -10 11 30.79 2.86 7 10 -11 29.02 2.52 10 -7 11 28.21 2.81 -10 7 12 5.65 1.15 10 -7 -12 4.69 0.93 7 -10 12 7.29 1.23 10 -7 12 6.66 1.21 7 10 -12 5.35 0.87 10 7 -12 6.33 1.04 -10 7 13 8.84 1.14 -7 10 13 6.63 1.19 7 -10 13 7.84 1.08 10 -7 13 10.07 1.15 -7 10 14 2.27 0.56 7 -10 14 1.14 0.41 10 -7 14 1.81 0.47 8 10 0 214.89 14.10 8 10 0 215.06 13.56 10 8 0 216.54 14.24 10 8 0 204.79 13.50 8 10 1 153.68 10.81 8 10 1 159.79 10.57 8 10 -1 174.29 11.61 10 8 1 166.93 11.08 8 10 -1 165.33 10.93 10 8 -1 172.94 11.72 10 8 -1 166.27 10.99 10 8 1 152.33 10.47 8 10 1 171.55 11.07 8 10 2 42.47 3.14 8 10 2 27.93 3.17 10 8 2 33.54 3.21 10 8 -2 38.34 3.66 8 10 -2 35.69 4.05 10 8 -2 32.88 4.04 8 10 2 33.39 3.21 8 10 -2 34.50 3.48 8 10 3 71.37 5.87 10 8 -3 63.65 6.47 8 10 -3 79.92 6.35 10 8 -3 79.10 6.35 8 10 3 82.37 5.64 10 8 3 73.07 5.54 8 10 4 271.32 16.18 10 -8 4 250.97 16.12 8 10 -4 276.73 17.50 8 10 -4 258.84 17.08 10 8 -4 237.61 17.04 10 -8 5 103.30 7.59 8 10 -5 114.47 8.57 10 8 -5 124.12 8.86 10 8 -5 109.52 8.60 10 -8 6 42.33 3.75 8 10 -6 47.02 4.28 10 8 -6 42.81 4.25 8 10 -6 38.18 4.17 10 -8 7 102.40 7.22 10 8 -7 91.76 7.24 8 10 -7 104.07 7.54 8 10 -7 94.65 7.13 10 8 -7 92.25 7.49 8 -10 8 34.83 4.06 10 -8 8 40.66 4.05 8 10 -8 40.21 3.74 10 8 -8 44.26 3.94 8 10 -8 47.42 4.16 10 8 -9 43.79 3.89 8 -10 9 44.20 4.27 10 -8 9 44.23 4.27 8 10 -9 48.42 3.88 10 8 -9 53.36 4.32 8 10 -9 52.80 4.21 10 8 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5.59 10 9 -5 64.31 5.73 9 10 -5 66.07 5.65 9 10 -6 1.92 1.40 10 -9 6 -0.25 1.02 10 9 -6 3.01 1.64 10 9 -7 26.70 3.15 10 -9 7 22.78 2.72 9 10 -7 20.75 2.67 10 9 -7 20.46 2.67 9 10 -7 23.58 2.96 10 9 -8 11.60 2.05 10 -9 8 7.18 1.78 10 9 -8 10.55 1.76 9 10 -8 7.63 1.59 9 10 -8 11.83 1.92 10 -9 9 52.35 4.72 9 10 -9 58.74 4.41 10 9 -9 60.51 4.48 9 10 -9 56.49 4.57 10 9 -9 53.65 4.55 10 -9 10 4.72 1.36 9 10 -10 3.80 0.91 10 9 -10 3.85 0.94 9 10 -10 3.47 1.03 10 9 -10 4.43 1.21 10 -9 11 1.05 0.92 10 9 -11 1.03 0.72 9 10 -11 2.67 0.78 -10 9 12 -0.29 0.69 10 -9 12 0.13 0.59 9 10 -12 0.46 0.43 10 9 -12 0.10 0.45 -10 9 13 32.16 2.31 -9 10 13 30.71 2.37 10 10 0 255.09 16.41 10 10 0 245.92 15.75 10 10 1 -0.55 1.07 10 10 -1 2.97 1.68 10 10 1 -0.20 0.72 10 10 -1 0.76 0.97 10 10 -2 155.62 10.71 10 10 2 150.66 10.34 10 10 -2 156.63 11.41 10 10 3 -0.22 0.77 10 10 -3 0.43 1.71 10 10 -3 1.32 1.42 10 10 -4 87.73 7.16 10 10 -5 -0.37 1.20 10 10 -5 0.75 1.54 10 10 -6 326.39 20.86 10 -10 7 -0.53 1.06 10 10 -7 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12 -0.26 0.53 11 -1 12 0.15 0.64 11 1 -13 12.11 1.36 11 -1 -13 9.45 1.25 1 11 13 12.03 1.39 -1 11 13 13.56 1.59 11 -1 13 10.97 1.20 1 11 14 289.35 18.37 -1 11 14 335.75 18.61 11 2 0 0.70 0.90 2 11 0 0.76 0.86 2 11 0 -0.57 0.80 11 2 0 1.94 1.42 11 2 -1 4.85 1.40 2 11 1 5.55 1.22 2 11 1 4.07 1.00 2 11 -1 4.02 1.22 11 2 1 4.09 1.52 11 2 -1 3.61 1.80 11 2 -2 0.35 1.17 2 11 -2 -0.32 1.28 2 11 2 0.20 0.72 2 11 2 0.17 0.66 11 2 2 0.77 1.04 11 2 -2 0.48 1.66 2 11 -3 18.37 2.70 11 2 -3 18.33 2.89 11 -2 3 24.27 1.92 2 11 3 20.20 2.18 -2 11 -3 23.76 2.74 2 11 -3 19.52 2.55 11 2 3 22.64 2.34 11 2 -3 18.54 3.27 11 2 -4 10.81 2.31 -2 11 -4 10.77 1.88 2 -11 4 5.38 1.03 2 11 -4 9.83 2.11 11 -2 4 7.15 1.03 2 11 -4 8.61 1.77 11 2 -5 2.94 1.64 -2 11 5 0.69 0.94 2 -11 5 3.93 0.88 2 11 -5 2.36 1.37 11 -2 5 1.28 0.65 -2 11 -5 2.04 1.26 2 11 -5 2.15 1.32 11 2 -5 2.66 1.50 11 -2 6 1.49 0.70 -2 11 6 0.74 0.96 2 -11 6 1.29 0.82 -2 11 -6 3.11 1.22 2 11 -6 1.28 1.06 2 11 -6 0.59 1.14 11 2 -6 2.08 1.34 11 2 -7 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138.74 9.20 3 11 -8 150.17 9.58 11 3 -8 153.00 10.12 11 -3 -8 143.05 9.98 11 -3 8 137.31 9.41 11 3 -9 4.37 1.54 3 11 9 5.85 1.19 11 -3 -9 6.82 1.66 3 -11 9 6.36 1.39 11 -3 9 3.16 1.17 11 3 -9 3.17 1.23 3 11 -9 5.22 1.21 3 11 10 407.32 23.63 3 11 -10 398.46 23.54 3 -11 10 340.21 23.72 11 3 -10 391.71 23.86 11 -3 -10 368.55 23.88 11 3 -10 408.36 24.16 11 -3 10 405.95 23.92 11 3 -11 20.93 2.29 3 11 11 17.03 1.82 11 -3 -11 15.41 2.09 3 -11 11 19.84 2.07 11 -3 11 17.93 2.04 11 3 -12 8.98 1.42 11 -3 12 10.04 1.37 11 -3 -12 9.13 1.39 3 -11 12 11.56 1.39 11 3 -13 4.13 0.85 -3 11 13 7.09 1.27 3 -11 13 7.24 0.94 11 -3 13 5.21 0.88 -3 11 14 23.78 1.93 11 -3 14 19.79 1.61 11 4 0 0.22 0.78 4 11 0 -0.27 1.15 4 11 0 -0.20 0.76 11 4 0 0.35 1.19 11 4 1 2.33 0.82 11 4 -1 1.88 1.14 4 11 1 1.41 0.96 4 11 -1 0.92 1.22 11 4 -1 2.91 1.65 4 11 1 1.67 0.82 11 4 1 2.06 1.22 4 11 -1 2.46 1.09 4 11 2 52.84 4.27 4 11 2 48.84 3.95 4 11 2 53.47 4.16 4 11 -2 54.53 4.43 11 4 2 49.68 4.24 11 4 -2 44.28 4.48 11 4 -2 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8.62 1.34 11 -4 -10 5.81 1.40 11 4 -11 0.43 1.00 -11 4 11 -0.74 0.81 11 -4 -11 -0.45 0.87 4 11 -11 0.69 0.59 4 -11 11 1.20 0.91 11 -4 11 0.40 0.89 11 4 -12 1.69 0.79 11 -4 -12 1.90 0.85 11 -4 12 3.74 0.90 4 -11 12 0.76 0.67 11 4 -13 0.11 0.44 -4 11 13 0.49 0.78 4 -11 13 -0.63 0.53 11 -4 13 0.45 0.53 -4 11 14 0.54 0.50 11 -4 14 0.07 0.33 5 11 0 347.50 20.94 11 5 0 341.65 21.29 11 5 0 322.60 20.42 5 11 0 321.10 20.37 11 5 -1 172.39 11.88 5 11 1 173.10 11.54 5 11 1 188.75 11.96 5 11 -1 178.29 11.80 11 5 1 180.14 12.12 11 5 -1 172.45 12.72 11 5 1 185.87 11.53 5 11 -1 189.08 12.41 5 11 2 1157.48 68.82 5 11 2 1190.12 68.50 5 11 2 1129.22 68.70 5 11 -2 1218.40 69.08 11 5 2 1141.00 68.82 11 5 -2 1169.79 69.33 11 5 -2 1150.90 70.16 11 5 -3 88.42 7.65 5 11 3 110.11 7.37 11 -5 3 97.51 6.62 5 11 3 106.72 6.81 5 11 3 89.62 6.85 5 11 -3 89.35 7.78 5 11 -3 96.37 7.48 11 5 3 109.17 7.07 11 5 -3 101.90 8.39 5 11 4 255.25 15.70 -5 11 4 246.59 15.18 11 5 -4 222.45 16.08 5 -11 4 231.96 14.94 11 -5 4 224.56 14.88 5 11 4 251.27 15.06 5 11 -4 255.81 16.19 5 11 5 248.27 15.62 -5 11 5 228.96 14.83 11 5 -5 231.40 15.94 5 -11 5 229.20 14.69 11 -5 5 237.48 14.66 5 11 -5 263.63 15.74 5 11 -5 201.13 15.33 11 5 -5 240.76 16.01 -5 11 6 141.03 9.96 5 -11 6 152.20 9.94 11 -5 6 141.41 9.78 5 11 -6 152.55 10.35 5 11 -6 152.34 10.53 11 5 -6 156.77 10.77 5 11 -7 95.69 7.11 5 -11 7 100.29 7.12 11 -5 7 92.29 6.98 11 5 -7 95.53 7.44 5 11 -7 110.81 7.58 11 5 -8 78.69 6.23 5 -11 8 80.67 5.99 11 -5 8 72.06 5.78 5 11 -8 72.50 5.58 5 11 -8 79.55 5.92 11 5 -8 71.89 5.91 11 5 -9 3.62 1.42 5 11 -9 1.84 0.88 5 -11 9 2.67 1.26 11 -5 9 4.10 1.31 11 5 -9 3.72 1.27 5 11 -9 6.23 1.32 11 -5 -9 2.67 1.26 5 -11 10 898.97 52.33 11 -5 10 892.45 52.26 5 11 -10 888.29 51.95 11 5 -10 873.43 52.05 11 -5 -10 832.87 52.16 11 5 -10 889.13 52.32 -11 5 11 29.29 2.62 11 5 -11 22.48 2.48 5 -11 11 26.36 2.58 11 -5 11 26.75 2.61 5 11 -11 24.00 2.22 11 5 -12 0.94 0.67 -11 5 12 -0.41 0.63 11 -5 -12 0.79 0.68 5 -11 12 0.30 0.69 11 -5 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7 4.34 1.46 6 11 -7 5.16 1.38 11 6 -7 7.75 1.77 11 -6 7 4.19 1.20 6 11 -7 1.52 1.37 11 6 -8 18.66 2.68 6 11 -8 20.97 2.28 6 -11 8 15.55 2.24 11 -6 8 16.79 2.33 11 6 -8 15.92 2.30 6 11 -8 17.22 2.33 11 6 -9 -0.27 1.12 6 11 -9 1.67 0.83 11 -6 9 1.30 1.20 11 6 -9 -0.24 0.83 6 11 -9 1.12 1.00 6 -11 9 1.61 1.28 11 -6 -9 0.58 1.06 11 6 -10 2.09 1.25 11 -6 10 2.59 1.21 6 -11 10 0.72 1.02 11 6 -10 0.97 0.82 6 11 -10 2.57 0.97 11 -6 -10 1.11 0.98 11 6 -11 -0.19 0.82 6 -11 11 1.36 0.92 11 -6 11 0.19 0.80 6 11 -11 0.57 0.67 11 6 -12 0.84 0.61 -11 6 12 0.14 0.59 11 -6 -12 -0.28 0.56 6 -11 12 0.43 0.67 11 -6 12 -0.58 0.72 6 -11 13 -0.10 0.43 11 -6 13 0.79 0.50 7 11 0 58.66 5.29 7 11 0 71.91 5.83 7 11 0 79.42 5.49 11 7 0 72.30 6.04 11 7 0 77.29 5.46 11 7 1 0.56 0.70 11 7 -1 0.26 0.87 7 11 1 1.45 0.95 7 11 -1 0.23 0.88 7 11 1 0.53 1.14 7 11 -1 1.40 1.47 11 7 1 0.28 0.96 11 7 -1 0.78 1.51 7 11 1 1.60 0.89 7 11 -1 -0.25 1.02 11 7 -2 26.22 3.13 7 11 2 28.41 3.00 7 11 2 26.60 2.58 7 11 -2 26.03 3.57 7 11 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0.37 0.82 11 -7 11 -0.36 0.91 7 11 -11 0.55 0.58 -11 7 12 73.17 4.59 7 -11 12 67.81 4.55 11 -7 12 67.51 4.56 11 7 -12 63.05 4.45 11 -7 -12 54.15 4.33 -7 11 13 0.48 0.57 11 -7 13 -0.44 0.41 11 8 0 -0.44 0.73 8 11 0 0.26 0.93 8 11 0 -0.31 1.03 11 8 0 -0.67 1.26 8 11 0 0.45 0.90 11 8 -1 19.39 2.49 8 11 1 23.98 2.75 11 8 1 26.07 2.42 8 11 1 24.60 2.77 8 11 -1 19.84 2.93 11 8 1 22.10 2.73 11 8 -1 28.45 3.55 8 11 1 24.13 2.45 8 11 -1 24.39 2.70 11 8 -2 0.30 1.26 8 11 2 1.72 1.21 8 11 2 2.17 1.10 8 11 -2 2.80 1.82 11 8 2 1.23 0.91 11 8 -2 3.49 2.11 8 11 2 2.05 0.85 8 11 -2 2.29 1.28 11 8 -3 2.44 1.39 8 11 3 2.74 1.22 8 11 3 3.27 1.09 11 8 3 4.07 1.11 11 8 -3 4.11 2.15 8 11 -3 3.91 1.54 11 8 -4 1.14 1.58 8 11 4 1.78 0.90 8 11 -4 0.40 1.85 8 11 -4 1.78 1.59 11 8 -5 1.95 1.72 11 -8 5 3.28 1.07 8 11 -5 2.52 1.58 11 8 -5 2.38 1.64 11 8 -6 13.05 2.38 8 -11 6 11.97 1.89 11 -8 6 6.21 1.55 8 11 -6 10.26 2.06 11 8 -6 13.50 2.37 8 11 -6 10.74 2.44 8 -11 7 9.38 1.93 8 11 -7 3.68 1.47 11 -8 7 6.71 1.54 11 8 -7 6.53 1.66 8 11 -7 9.26 1.96 11 8 -8 32.35 3.32 8 -11 8 32.63 3.30 11 8 -8 26.22 2.93 8 11 -8 33.03 2.96 11 -8 8 25.69 2.96 8 11 -8 25.66 2.93 11 8 -9 6.82 1.54 8 -11 9 6.97 1.58 11 -8 9 4.74 1.50 8 11 -9 7.71 1.31 11 8 -9 7.16 1.30 8 11 -9 4.54 1.22 11 8 -10 2.54 1.00 8 -11 10 1.31 0.97 11 -8 10 1.49 1.08 11 8 -10 3.65 0.91 8 11 -10 1.38 0.88 11 -8 -10 1.65 0.88 11 -8 11 0.66 0.78 8 -11 11 0.67 0.80 8 11 -11 1.03 0.63 11 8 -11 1.22 0.73 -11 8 12 2.62 0.73 11 -8 12 2.21 0.70 11 8 -12 1.64 0.57 -8 11 13 10.36 1.13 9 11 0 50.93 4.33 11 9 0 64.84 5.24 11 9 0 53.54 4.36 9 11 0 54.12 4.91 9 11 1 263.00 16.34 9 11 -1 259.67 16.86 9 11 -1 252.43 16.15 11 9 1 263.80 15.77 11 9 1 228.92 16.15 11 9 -1 243.74 16.92 11 9 -1 259.14 16.16 9 11 1 244.35 15.79 9 11 2 184.63 11.86 9 11 2 190.76 12.25 9 11 -2 192.10 13.26 11 9 2 173.55 12.10 9 11 -2 185.01 12.49 11 9 -2 178.60 13.28 11 9 -2 200.50 12.62 9 11 3 136.27 8.73 11 9 3 129.46 8.64 9 11 -3 115.79 9.15 11 9 -3 118.70 9.80 11 9 -3 129.46 9.37 9 11 4 346.06 20.67 9 11 -4 298.23 21.75 9 11 -4 343.82 21.65 11 9 -4 345.18 21.75 9 11 -5 94.84 6.96 11 9 -5 85.33 6.92 9 11 -5 77.30 6.66 11 9 -5 68.46 6.56 9 11 -6 389.12 24.53 11 9 -6 385.22 24.70 11 9 -6 399.23 24.91 11 -9 7 61.53 5.16 9 11 -7 67.19 5.24 11 9 -7 57.39 5.18 9 11 -7 72.03 5.60 11 9 -8 8.59 1.81 9 11 -8 5.74 1.28 11 9 -8 8.27 1.58 11 -9 8 6.46 1.65 9 11 -8 7.07 1.56 9 -11 9 69.31 5.88 11 -9 9 82.25 6.04 9 11 -9 80.40 5.62 9 11 -9 84.44 5.90 11 9 -9 82.83 5.93 11 9 -9 78.69 5.70 11 9 -10 9.07 1.18 9 11 -10 6.02 0.96 9 11 -10 5.44 1.17 11 -9 10 6.44 1.38 11 9 -10 6.12 1.20 9 11 -11 39.06 2.90 11 9 -11 37.42 2.96 -9 11 12 15.17 1.56 11 9 -12 12.80 1.26 10 11 0 0.32 1.14 11 10 0 1.29 1.44 10 11 0 0.22 0.85 11 10 0 0.65 0.82 11 10 1 -0.28 1.05 10 11 1 2.22 1.09 10 11 -1 -0.74 1.28 11 10 -1 1.49 1.50 10 11 1 0.39 0.68 11 10 1 0.19 0.64 10 11 -1 0.50 0.92 11 10 -1 -0.75 0.99 10 11 2 5.55 1.30 11 10 2 1.69 0.98 10 11 -2 2.44 1.69 11 10 -2 4.99 1.93 10 11 -2 4.85 1.37 11 10 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13.74 11 11 -8 219.46 14.00 11 11 -9 -0.27 0.53 11 11 -9 0.17 0.78 11 11 -10 18.77 1.79 11 11 -11 -0.16 0.36 0 12 0 28.97 2.88 0 12 0 24.19 3.09 12 0 1 1.23 1.59 12 0 -1 1.73 2.28 0 12 -2 1368.08 78.63 12 0 2 1279.98 78.90 12 0 -2 1378.92 80.68 0 12 -2 1313.75 79.25 0 12 -3 0.59 1.17 0 12 -3 3.04 1.66 12 0 3 -0.51 0.91 12 0 -3 -0.54 1.93 0 12 4 393.65 23.09 0 12 -4 330.06 23.05 0 12 -4 386.69 23.58 0 12 5 1.14 1.17 0 12 -5 1.59 1.31 0 12 -5 0.30 1.01 12 0 -5 -0.42 1.66 0 12 6 1300.71 74.49 0 12 -6 1256.32 74.38 12 0 -6 1200.52 74.79 0 12 7 -0.32 1.12 0 12 -7 -0.25 1.02 12 0 -7 -0.69 1.51 12 0 -8 28.92 3.28 0 12 -8 35.46 3.00 12 0 -8 25.65 3.16 12 0 -9 0.59 1.09 12 0 -9 1.43 1.30 12 0 -10 326.26 20.23 12 0 -10 321.38 20.38 12 0 -11 0.69 1.11 0 12 11 0.21 0.90 0 12 12 25.33 2.30 12 0 -12 22.55 2.32 12 0 -13 0.22 0.45 0 12 13 -0.12 0.52 12 1 0 0.27 1.05 1 12 0 -0.58 1.14 1 12 0 0.21 0.72 12 1 0 -0.93 1.88 1 12 1 5.75 1.26 1 12 1 11.09 1.76 1 12 -1 9.88 1.75 12 1 1 13.14 2.25 12 1 -1 11.33 2.81 12 -1 1 9.94 2.40 1 12 -2 0.36 1.37 -1 12 -2 1.11 1.15 12 1 2 1.19 1.04 12 1 -2 -0.56 2.06 12 -1 2 3.85 1.70 1 12 -3 11.59 2.35 -1 12 -3 12.87 2.21 1 12 -3 10.07 1.98 12 1 3 9.78 1.64 12 1 -3 9.55 2.75 12 -1 3 9.56 1.82 -1 12 4 0.53 1.00 1 12 -4 -0.35 1.39 -1 12 -4 -0.97 1.28 1 12 -4 2.24 1.35 1 12 5 32.75 3.30 -1 12 5 25.81 2.91 1 12 -5 25.83 3.08 -1 12 -5 25.15 3.09 1 12 -5 18.44 2.77 12 1 -5 31.91 3.81 12 -1 -5 24.12 3.55 12 1 -6 1.85 1.43 1 12 6 0.64 1.33 -1 12 6 -0.29 1.16 1 -12 6 1.27 0.67 1 12 -6 1.04 1.09 -1 12 -6 1.15 1.26 1 12 -6 0.91 1.19 12 1 -6 -0.37 1.58 12 -1 -6 1.15 1.51 1 12 7 13.44 2.32 -1 12 7 13.16 2.18 1 -12 7 6.87 1.31 1 12 -7 7.90 1.46 -1 12 -7 11.40 1.75 1 12 -7 13.73 1.99 12 1 -7 9.56 2.03 12 -1 -7 10.19 2.19 12 1 -8 0.97 1.41 1 -12 8 -0.61 0.75 12 -1 8 1.14 0.86 1 12 -8 1.10 0.89 12 1 -8 0.31 1.02 12 -1 -8 -0.64 1.21 12 1 -9 -0.60 1.18 12 -1 -9 1.74 1.24 1 -12 9 0.20 0.71 12 -1 9 1.17 0.87 1 12 -9 0.36 0.64 12 1 -9 1.97 1.23 12 -1 -9 1.16 1.20 12 1 -10 0.53 1.08 1 12 10 1.31 0.90 12 -1 -10 0.27 1.14 12 -1 -10 0.48 0.91 1 -12 10 0.17 0.62 12 -1 10 0.18 0.75 12 1 -10 -0.23 1.10 12 1 -11 13.53 2.06 1 12 11 17.96 1.92 12 -1 11 17.19 1.78 12 1 -11 15.88 1.81 12 1 -12 1.20 0.82 1 12 12 2.11 0.72 12 -1 -12 1.58 0.83 -1 12 12 1.45 0.93 12 1 -13 0.75 0.51 12 -1 -13 -0.11 0.45 1 12 13 0.40 0.51 -1 12 13 -0.39 0.62 2 12 0 467.33 28.87 2 12 0 506.22 29.45 12 2 0 487.67 30.27 12 2 0 460.68 29.09 2 12 1 447.52 27.78 12 2 -1 458.44 28.46 12 2 1 462.50 28.69 12 2 -1 478.23 29.68 2 12 -1 453.01 27.99 2 12 1 470.24 28.12 12 2 -2 5.27 1.77 2 12 -2 11.65 2.26 12 2 2 6.84 1.59 2 12 2 4.11 1.23 12 2 -2 5.36 2.58 2 12 3 511.31 28.90 2 12 -3 441.79 28.75 2 12 -3 443.48 29.19 12 2 3 464.41 28.41 12 2 -3 506.59 30.48 12 -2 3 472.92 28.79 12 2 -3 437.00 29.37 -2 12 4 105.37 7.45 2 12 -4 107.58 8.05 2 12 -4 95.39 7.72 12 2 -4 100.15 8.21 -2 12 5 415.95 26.28 12 -2 5 404.93 25.55 2 12 -5 499.86 26.95 2 12 -5 404.05 26.62 12 2 -5 453.99 27.45 12 2 -5 443.55 27.26 2 -12 6 268.37 17.15 2 12 -6 289.06 17.73 12 -2 6 270.73 17.00 2 12 -6 276.98 17.96 12 -2 -6 283.71 18.43 12 2 -6 286.50 18.37 12 2 -6 277.75 18.32 2 12 7 282.13 17.33 -2 12 7 268.03 16.77 2 -12 7 242.87 16.15 12 -2 7 254.51 16.07 2 12 -7 264.72 16.36 12 2 -7 263.25 17.06 12 -2 -7 227.29 16.85 2 12 -7 279.22 16.75 2 12 -8 139.02 9.08 2 -12 8 136.63 8.95 12 -2 8 122.35 8.74 2 12 -8 123.74 8.67 12 2 -8 138.36 9.48 12 -2 -8 132.78 9.54 12 2 -8 134.55 9.56 2 12 9 115.82 7.47 12 -2 9 111.88 7.42 2 12 -9 119.17 7.39 12 2 -9 105.40 7.74 12 -2 -9 97.63 7.72 12 2 -9 117.07 8.03 2 12 10 52.09 3.90 2 -12 10 46.66 3.87 2 12 -10 47.06 3.62 12 -2 10 49.23 3.95 12 2 -10 44.78 4.03 12 -2 -10 43.01 4.06 12 -2 -10 52.76 4.37 12 2 -10 57.04 4.43 2 12 11 95.50 6.45 2 -12 11 101.57 6.50 12 -2 11 101.81 6.57 12 2 -11 87.93 6.45 12 -2 -11 99.81 6.97 12 2 -11 92.07 6.83 12 2 -12 7.73 1.27 12 -2 -12 7.90 1.26 -2 12 12 9.55 1.53 12 -2 12 6.06 1.01 2 -12 12 8.69 1.05 12 2 -13 51.06 3.82 12 -2 -13 54.42 3.83 -2 12 14 87.50 5.57 12 3 0 0.24 0.79 3 12 0 0.29 0.99 3 12 0 1.52 1.09 12 3 0 -0.41 1.37 12 3 -1 35.50 3.58 3 12 1 38.41 3.23 3 12 -1 34.64 3.31 3 12 1 36.33 3.42 3 12 -1 34.26 3.81 12 3 1 30.97 3.58 12 3 -1 29.19 4.18 12 3 -2 19.70 2.85 3 12 2 20.47 2.41 3 12 2 24.47 2.35 3 12 -2 22.95 2.68 12 3 2 17.64 2.43 12 3 -2 22.90 3.71 3 12 3 78.75 6.15 3 12 -3 76.57 6.53 12 3 3 81.87 5.80 3 12 3 70.70 5.59 12 3 -3 85.51 7.42 12 3 -3 69.26 6.55 12 3 -4 -1.30 1.63 3 12 4 0.30 1.10 -3 12 4 0.25 0.95 3 12 -4 0.72 1.36 12 -3 4 -0.14 0.58 3 12 -4 1.66 1.42 12 3 -5 16.39 2.79 3 12 5 17.35 2.60 -3 12 5 13.62 2.02 12 -3 5 13.72 1.61 3 -12 5 12.66 1.65 3 12 -5 19.76 2.63 3 12 -5 13.46 2.42 12 3 -5 11.00 2.45 12 3 -6 3.12 1.54 -3 12 6 -0.27 1.14 3 -12 6 1.02 0.88 3 12 -6 2.24 1.25 12 -3 6 1.98 0.86 3 12 -6 1.91 1.34 12 3 -6 0.75 1.42 -3 12 7 63.41 5.57 3 -12 7 69.09 5.31 12 -3 7 72.31 5.29 3 12 -7 73.29 5.47 3 12 -7 73.58 5.76 12 3 -7 77.69 6.12 12 -3 -7 65.84 6.03 12 3 -8 -0.32 1.25 3 -12 8 -0.93 0.98 12 -3 8 0.88 0.87 3 12 -8 0.20 0.68 3 12 -8 0.24 0.94 12 3 -8 0.30 1.27 12 -3 -8 0.67 1.31 12 3 -9 6.06 1.62 12 -3 9 5.97 1.27 3 12 -9 3.99 1.11 12 3 -9 6.27 1.44 3 -12 9 5.00 1.23 12 -3 -9 7.05 1.72 12 3 -10 5.76 1.48 12 -3 -10 6.56 1.62 3 -12 10 3.82 1.11 12 -3 10 3.84 1.08 3 12 -10 4.88 1.05 12 3 -10 3.03 1.12 12 -3 -10 5.71 1.41 12 3 -11 22.04 2.52 3 -12 11 24.78 2.35 12 -3 11 26.12 2.42 12 3 -11 26.03 2.34 12 -3 -11 30.37 2.86 12 3 -12 -0.16 0.71 12 -3 12 -0.12 0.55 12 -3 -12 -0.49 0.65 -3 12 12 0.98 0.84 3 -12 12 -0.11 0.54 12 3 -13 2.78 0.65 12 -3 13 2.32 0.53 -3 12 14 0.25 0.43 4 12 0 826.27 50.83 12 4 0 888.12 51.99 12 4 0 828.34 50.85 4 12 0 915.40 51.46 4 12 1 2.89 1.31 12 4 -1 5.46 1.42 4 12 -1 4.06 1.62 4 12 1 3.69 1.07 4 12 -1 1.98 1.12 12 4 1 5.79 1.57 4 12 2 1092.01 64.03 4 12 2 1094.52 63.55 4 12 2 1039.05 63.72 4 12 -2 1084.14 64.08 12 4 2 1058.70 63.89 12 4 -2 1075.71 65.44 12 4 -2 1109.55 64.51 12 4 -3 2.00 1.45 4 12 -3 7.73 2.12 4 12 3 4.51 1.46 4 12 3 3.06 1.11 12 4 3 5.58 1.28 12 4 -3 4.07 2.40 12 4 -4 0.43 1.48 4 12 4 2.44 1.36 -4 12 4 0.72 1.15 12 -4 4 3.25 0.81 4 12 -4 -0.37 1.32 4 12 -4 1.69 1.51 12 4 -5 2.52 1.78 4 12 5 4.41 1.52 -4 12 5 3.68 1.22 12 -4 5 4.96 1.00 4 12 -5 0.99 1.26 12 4 -5 0.85 1.54 4 12 -5 2.75 1.52 4 12 6 346.78 22.80 -4 12 6 353.68 22.06 4 -12 6 346.59 21.81 12 -4 6 340.70 21.61 4 12 -6 359.80 22.56 12 4 -6 368.97 22.91 12 4 -6 385.12 23.13 4 12 -6 358.76 22.27 4 -12 7 0.23 0.94 -4 12 7 0.28 1.00 4 12 -7 0.98 0.99 12 -4 7 0.87 0.86 12 4 -7 0.66 1.40 4 12 -7 1.45 1.15 4 -12 8 302.98 19.19 12 -4 8 302.04 19.13 4 12 -8 295.90 18.96 4 12 -8 323.84 19.35 12 4 -8 304.94 19.52 12 4 -8 334.05 19.82 12 -4 -8 289.27 19.71 12 4 -9 0.28 1.15 4 -12 9 -1.19 1.11 12 -4 9 0.46 0.93 4 12 -9 1.18 0.84 12 4 -9 0.25 0.97 4 12 -9 -0.82 1.01 12 -4 -9 -0.29 1.02 4 -12 10 691.24 40.83 12 -4 10 691.42 40.85 12 4 -10 688.18 40.82 12 -4 -10 657.14 40.91 12 4 -10 708.11 41.10 4 12 -10 673.87 40.51 12 4 -11 3.78 1.09 12 -4 -11 3.36 1.08 4 -12 11 3.13 0.91 12 -4 11 3.72 0.99 -4 12 12 40.68 3.19 4 -12 12 33.07 2.63 12 -4 12 32.12 2.63 12 4 -12 32.01 2.77 12 -4 -12 34.25 2.82 12 -4 13 0.61 0.41 12 4 -13 0.26 0.35 12 5 0 1.60 1.00 5 12 0 0.30 1.18 5 12 0 0.68 0.92 12 5 0 -0.37 1.09 12 5 -1 10.17 1.69 5 12 1 4.84 1.40 5 12 1 4.81 1.43 5 12 -1 7.30 2.02 5 12 1 7.50 1.42 12 5 1 5.55 1.53 12 5 -1 5.29 2.19 5 12 -1 4.54 1.32 12 5 -2 0.33 1.25 5 12 2 -0.27 0.98 5 12 2 0.24 0.89 5 12 2 0.59 0.77 12 5 2 0.52 0.84 12 5 -2 0.98 2.07 5 12 -2 0.57 0.99 12 5 -3 0.77 1.45 5 12 3 -0.28 0.98 5 12 3 0.88 0.87 5 12 -3 -0.40 1.73 5 12 3 0.19 0.58 12 5 3 0.22 0.70 5 12 -3 0.96 1.35 12 5 -4 -0.41 1.56 5 12 4 2.50 1.47 -5 12 4 0.70 0.86 5 12 4 0.41 0.80 5 12 -4 1.89 1.93 12 5 -5 15.78 2.91 5 12 5 17.29 2.62 -5 12 5 19.54 2.25 12 -5 5 15.08 1.84 5 12 -5 13.87 2.46 12 5 -5 13.54 2.85 5 12 -5 17.21 2.63 12 5 -6 1.95 1.59 -5 12 6 2.05 1.14 5 -12 6 4.96 1.22 12 -5 6 2.87 0.98 5 12 -6 4.39 1.41 12 5 -6 4.80 1.90 5 12 -6 5.64 1.76 5 -12 7 7.32 1.57 12 -5 7 9.30 1.54 5 12 -7 11.17 1.68 12 5 -7 9.95 2.07 5 12 -7 6.80 1.82 12 5 -8 4.04 1.58 5 -12 8 5.57 1.44 5 12 -8 3.58 1.11 12 -5 8 3.12 1.21 12 5 -8 0.28 1.04 5 12 -8 3.52 1.25 12 -5 -8 5.66 1.69 12 5 -9 3.26 1.40 5 -12 9 0.49 1.05 5 12 -9 2.39 0.84 12 -5 9 1.41 1.01 12 5 -9 3.36 1.24 5 12 -9 0.83 0.88 12 -5 -9 2.29 1.23 12 5 -10 1.61 1.25 5 -12 10 0.63 1.06 12 -5 10 0.41 0.87 12 5 -10 0.58 0.90 5 12 -10 0.50 0.74 12 -5 -10 -0.22 0.92 12 -5 -11 1.55 0.88 5 -12 11 0.50 0.82 12 -5 11 0.66 0.72 5 12 -11 0.84 0.57 12 5 -12 0.14 0.59 12 -5 -12 0.42 0.61 12 -5 12 -0.12 0.54 -5 12 13 2.92 0.76 12 -5 13 2.19 0.49 6 12 0 54.42 5.07 6 12 0 57.82 4.86 6 12 0 59.80 4.79 12 6 0 63.07 5.48 12 6 0 64.54 4.80 6 12 1 259.06 17.49 6 12 1 273.84 17.67 6 12 -1 304.86 18.40 12 6 1 262.81 17.73 6 12 1 289.89 17.34 12 6 -1 299.90 18.72 12 6 -1 260.34 17.59 6 12 -1 279.08 17.60 6 12 2 250.31 16.68 6 12 2 275.03 16.33 6 12 2 266.26 16.58 6 12 -2 274.53 16.93 12 6 2 256.77 16.63 12 6 -2 266.58 18.04 12 6 -2 274.95 17.09 6 12 -2 212.14 17.11 6 12 3 277.56 18.82 6 12 3 280.73 18.47 6 12 3 321.23 18.39 6 12 -3 296.97 19.14 12 6 3 304.45 18.53 12 6 -3 293.60 20.02 12 6 -3 291.16 19.37 6 12 4 382.12 24.04 -6 12 4 407.04 23.57 6 12 -4 391.15 24.50 12 6 -4 343.80 24.37 6 12 4 376.19 23.34 6 12 -5 358.24 20.95 6 12 5 311.73 20.72 -6 12 5 347.66 20.12 12 -6 5 309.09 19.80 12 6 -5 339.09 21.27 12 6 -5 359.61 21.45 12 6 -6 2.70 1.80 -6 12 6 7.62 1.44 6 -12 6 2.36 1.16 12 -6 6 5.41 1.26 6 12 -6 3.86 1.46 12 6 -6 4.34 1.66 6 12 -6 7.41 1.75 6 -12 7 189.28 12.99 12 -6 7 195.46 12.92 6 12 -7 207.16 13.08 6 12 -7 204.22 13.35 12 6 -7 200.98 13.39 12 6 -8 20.70 2.77 6 -12 8 18.93 2.45 12 -6 8 19.05 2.42 6 12 -8 17.83 2.12 12 6 -8 20.76 2.52 6 12 -8 18.92 2.42 6 -12 9 66.99 5.43 12 -6 9 72.97 5.43 6 12 -9 69.08 5.05 6 12 -9 66.41 5.18 12 6 -9 69.17 5.33 12 6 -9 75.50 5.65 12 -6 -9 69.56 5.62 12 -6 -10 295.66 18.26 6 -12 10 294.49 18.29 12 -6 10 307.36 18.30 6 12 -10 289.02 17.98 12 6 -10 283.44 18.04 12 6 -10 299.04 18.35 6 -12 11 53.81 4.15 12 -6 11 61.54 4.24 6 12 -11 58.55 3.96 12 6 -11 50.69 4.16 12 -6 -11 54.36 4.26 12 -6 12 39.50 2.84 12 6 -12 39.33 2.89 12 -6 -12 33.82 2.79 -6 12 13 60.49 4.15 12 7 0 0.45 0.78 7 12 0 -0.79 0.97 7 12 0 -0.32 1.26 12 7 0 1.41 1.36 7 12 0 2.32 1.09 12 7 -1 14.34 2.02 7 12 1 9.69 1.76 7 12 -1 9.77 1.80 7 12 1 14.76 2.15 7 12 -1 9.10 2.22 12 7 1 13.40 2.12 12 7 -1 12.36 2.53 7 12 1 12.70 1.76 7 12 -1 14.20 2.00 12 7 -2 4.71 1.53 7 12 2 4.00 1.33 7 12 -2 2.12 1.15 7 12 -2 0.40 1.63 7 12 2 2.23 1.17 12 7 2 2.56 1.07 7 12 2 3.51 1.05 12 7 -2 4.60 2.20 7 12 -2 2.63 1.29 12 7 -3 13.05 2.51 7 12 3 14.62 2.36 7 12 3 16.91 2.13 7 12 3 21.53 2.03 12 7 3 16.33 1.99 12 7 -3 19.57 3.34 7 12 -3 16.73 2.57 12 7 -4 0.79 1.70 7 12 4 1.96 1.38 -7 12 4 1.06 0.82 7 12 4 1.02 0.98 7 12 -4 1.97 1.63 7 12 -4 0.71 1.55 12 7 -5 2.01 1.90 7 12 -5 4.91 1.84 12 7 -5 7.79 2.23 12 7 -6 2.66 1.60 12 -7 6 0.23 0.85 7 12 -6 0.90 1.13 12 7 -6 0.36 1.50 7 12 -6 0.67 1.39 12 -7 7 44.91 3.90 7 12 -7 40.09 3.79 7 12 -7 52.19 4.38 12 7 -7 37.24 3.94 12 7 -8 10.48 2.02 7 -12 8 8.10 1.75 12 -7 8 7.11 1.53 7 12 -8 8.67 1.49 12 7 -8 9.20 1.66 7 12 -8 6.71 1.52 12 7 -9 0.24 1.09 7 -12 9 1.20 1.09 12 -7 9 0.46 0.92 7 12 -9 0.17 0.66 12 7 -9 -0.42 0.95 7 12 -9 0.60 1.00 12 -7 -9 -0.78 1.07 12 7 -10 6.93 1.35 7 -12 10 5.42 1.26 12 -7 10 7.11 1.25 12 7 -10 4.60 1.03 7 12 -10 4.40 1.04 12 -7 -10 4.06 1.06 -12 7 11 26.44 2.19 7 12 -11 24.26 2.04 12 -7 -11 20.03 2.19 12 -7 11 25.57 2.27 12 7 -11 24.54 2.23 12 -7 -12 0.20 0.38 12 7 -12 0.91 0.49 8 12 0 3.77 1.31 8 12 0 2.56 1.50 12 8 0 6.56 1.85 8 12 0 5.76 1.32 12 8 0 3.06 1.00 12 8 -1 4.14 1.35 8 12 1 4.50 1.41 8 12 1 5.03 1.48 8 12 -1 4.77 2.02 12 8 1 5.86 1.58 12 8 -1 2.01 1.68 8 12 1 5.24 1.20 8 12 -1 5.16 1.46 8 12 2 127.88 8.85 8 12 2 120.24 8.11 8 12 2 111.42 8.40 8 12 -2 121.69 9.34 8 12 -2 123.44 8.75 12 8 2 111.50 8.33 12 8 -2 122.44 9.59 12 8 -2 134.10 8.90 12 8 -3 0.35 1.26 8 12 3 1.34 0.93 12 8 3 1.06 0.84 12 8 -3 -0.47 1.71 8 12 -3 2.29 1.56 8 12 4 1146.89 65.86 8 12 -4 1115.95 67.14 8 12 -4 1097.74 66.80 12 8 -4 1084.89 66.92 12 8 -5 -0.39 1.50 8 12 -5 0.35 1.54 12 8 -5 -0.40 1.75 8 12 -6 565.28 35.20 12 8 -6 580.68 35.54 12 8 -6 589.51 35.69 8 12 -7 2.46 1.17 12 8 -7 -0.29 1.22 8 12 -7 2.03 1.52 12 -8 8 39.06 3.64 8 12 -8 38.63 3.39 8 12 -8 44.75 3.78 12 8 -8 41.88 3.65 12 8 -8 35.44 3.69 12 8 -9 0.45 0.94 8 12 -9 0.16 0.65 12 -8 9 0.22 0.99 12 8 -9 -0.19 0.80 8 12 -9 0.19 0.81 12 -8 -9 0.71 0.93 12 8 -10 0.69 0.62 8 12 -10 0.44 0.70 12 -8 -10 0.16 0.60 12 8 -10 1.93 0.86 -12 8 11 0.12 0.56 12 -8 -11 0.28 0.57 8 12 -11 0.41 0.47 12 8 -11 0.65 0.60 -8 12 12 89.68 5.24 12 8 -12 68.98 4.83 9 12 0 0.64 1.20 12 9 0 -0.66 1.31 9 12 0 -0.23 0.91 12 9 0 0.43 0.80 9 12 1 10.23 1.92 9 12 -1 12.05 2.42 12 9 1 10.96 1.98 12 9 -1 10.45 2.36 9 12 1 12.84 1.64 9 12 -1 10.89 1.85 12 9 -1 13.27 1.86 12 9 -2 7.26 1.67 9 12 2 6.32 1.47 9 12 -2 4.84 1.91 12 9 2 5.07 1.31 12 9 -2 4.78 2.06 9 12 2 5.09 1.07 9 12 -2 4.30 1.54 12 9 -3 32.00 3.51 12 9 3 33.97 2.97 12 9 -3 25.71 3.84 9 12 3 30.31 2.94 9 12 -3 31.12 3.43 12 9 -4 0.73 1.50 9 12 4 -0.19 0.76 9 12 -4 0.79 1.93 9 12 -4 -0.69 1.33 12 9 -5 15.47 2.67 9 12 -5 25.30 3.04 12 9 -5 21.36 3.16 9 12 -5 20.00 3.07 12 9 -6 8.24 2.21 9 12 -6 14.25 2.25 12 9 -6 12.54 2.20 9 12 -7 25.31 2.69 12 9 -7 22.37 2.78 9 12 -7 28.30 3.09 12 9 -8 0.74 1.22 9 12 -8 2.27 0.97 12 9 -8 1.27 0.97 9 12 -8 1.82 1.12 9 12 -9 12.89 1.52 12 9 -9 13.58 1.68 9 12 -9 13.03 1.70 12 -9 -9 14.08 1.91 12 9 -9 15.32 1.89 12 9 -10 1.04 0.57 9 12 -10 0.27 0.59 12 9 -10 1.52 0.80 -12 9 11 1.16 0.56 12 -9 -11 0.33 0.52 9 12 -11 -0.09 0.40 -9 12 12 0.09 0.41 10 12 0 280.90 17.66 10 12 0 256.70 18.06 12 10 0 284.22 17.54 12 10 0 306.78 18.37 10 12 1 88.42 6.07 10 12 1 82.20 6.43 10 12 -1 85.00 6.37 10 12 -1 91.48 7.07 12 10 1 82.99 6.44 12 10 -1 90.72 7.20 12 10 -1 76.59 6.18 10 12 2 19.64 2.35 12 10 2 20.37 2.36 10 12 -2 24.75 3.25 12 10 -2 19.12 3.23 10 12 -2 20.99 2.62 12 10 -2 19.69 2.50 10 12 3 213.90 13.97 12 10 3 226.15 13.93 10 12 -3 203.83 15.00 10 12 -3 219.62 14.60 12 10 -3 222.90 15.30 12 10 -3 230.14 14.70 10 12 -4 10.21 2.14 12 10 -4 8.50 2.06 10 12 -5 147.43 9.81 10 12 -5 117.69 9.38 12 10 -5 141.33 9.80 12 10 -5 121.84 9.48 10 12 -6 224.71 14.37 12 10 -6 210.85 14.38 12 10 -6 219.70 14.54 10 12 -7 62.93 4.80 12 10 -7 57.17 4.80 10 12 -8 106.31 7.43 12 10 -8 112.88 7.57 10 12 -8 114.49 7.70 10 12 -9 78.83 5.33 12 10 -9 70.78 5.12 12 10 -9 78.96 5.40 12 -10 -9 75.16 5.34 10 12 -9 71.82 5.07 12 10 -10 6.52 0.87 10 12 -10 8.40 1.09 12 10 -10 7.62 1.10 12 10 -11 30.98 2.29 11 12 0 0.59 1.32 12 11 0 0.89 1.12 11 12 0 0.80 0.84 12 11 0 0.77 0.74 11 12 1 7.36 1.49 12 11 1 4.57 1.39 11 12 -1 7.12 1.88 12 11 -1 5.50 1.84 11 12 1 7.77 1.18 11 12 -1 5.69 1.34 12 11 -1 3.36 1.15 11 12 2 -0.22 0.84 12 11 2 1.30 0.98 11 12 -2 -0.37 1.41 12 11 -2 2.28 1.81 11 12 -2 1.04 1.07 12 11 -2 0.26 0.90 12 11 3 9.75 1.44 11 12 3 7.87 1.32 11 12 -3 5.78 2.18 12 11 -3 10.19 2.49 11 12 -3 6.65 1.82 12 11 -3 7.51 1.75 11 12 -4 -0.31 1.27 12 11 -4 0.31 1.25 11 12 -5 10.62 2.09 12 11 -5 18.02 2.61 11 12 -5 12.79 2.23 12 11 -5 12.33 2.19 11 12 -6 5.89 1.54 12 11 -6 8.19 1.75 11 12 -6 8.04 1.76 12 11 -6 5.08 1.48 11 12 -7 1.61 0.99 12 11 -7 3.14 1.11 12 11 -7 0.71 1.19 11 12 -8 0.15 0.64 12 11 -8 -0.16 0.68 11 12 -8 0.37 0.85 11 12 -9 4.96 0.83 12 11 -9 5.53 0.91 11 12 -9 4.56 1.00 12 11 -9 5.74 1.05 12 -11 -9 5.55 0.97 11 12 -10 0.86 0.50 12 11 -10 1.10 0.54 12 12 0 1146.94 67.34 12 12 0 1145.52 67.94 12 12 1 0.23 0.96 12 12 -1 0.31 1.37 12 12 -1 0.20 0.93 12 12 2 76.03 5.45 12 12 -2 70.60 5.69 12 12 -2 79.05 6.43 12 12 -3 -0.35 1.52 12 12 -3 -0.52 1.15 12 12 -4 27.49 3.05 12 12 -5 -0.57 1.37 12 12 -5 0.27 1.15 12 12 -6 26.04 2.73 12 12 -6 22.54 2.67 12 12 -7 0.35 0.77 12 12 -7 -0.41 1.03 12 12 -8 312.24 18.85 12 12 -9 -0.33 0.37 12 12 -9 -0.23 0.52 13 0 0 0.91 0.99 13 0 0 2.17 2.15 13 0 1 1.30 1.72 13 0 -1 0.63 2.31 0 13 -2 1.51 1.28 13 0 2 4.39 1.73 13 0 -2 1.29 2.24 0 13 -3 0.33 1.31 13 0 3 2.14 0.90 13 0 -3 0.60 1.88 0 13 4 3.38 1.50 0 13 -4 3.81 1.61 0 13 5 1.25 1.37 0 13 -5 0.67 1.33 13 0 -5 2.27 1.63 0 13 6 26.47 3.12 13 0 -6 14.40 2.76 0 13 -6 21.84 2.74 13 0 -6 24.71 3.41 0 13 7 -0.69 1.30 0 13 -7 1.02 1.12 13 0 -7 -1.42 1.58 13 0 -8 60.22 5.26 13 0 -8 58.56 5.26 13 0 -9 -0.29 1.23 13 0 -9 0.28 1.14 13 0 -10 1.77 1.12 0 13 10 -0.21 0.86 13 0 -10 0.89 0.92 13 0 -11 0.21 0.87 0 13 11 0.33 0.68 13 0 -12 1.94 0.79 0 13 12 1.29 0.63 1 13 0 176.59 12.24 1 13 0 194.19 12.87 13 1 0 207.77 14.02 13 -1 0 216.90 14.69 13 1 0 174.70 12.44 1 13 -1 79.37 6.84 13 1 1 93.08 7.69 13 1 -1 90.24 8.59 13 -1 1 111.90 8.38 13 -1 -1 102.73 9.20 13 1 -1 105.96 7.66 1 13 -2 145.67 11.14 13 1 2 144.31 10.68 13 1 -2 159.81 12.53 13 -1 2 168.57 11.19 13 -1 -2 166.15 13.01 13 1 -2 150.69 11.26 1 13 -3 106.78 9.21 1 13 -3 129.55 9.06 13 -1 3 119.88 8.66 13 1 -3 136.68 10.68 13 -1 -3 131.42 10.68 13 1 -3 117.42 9.63 -1 13 4 327.78 19.87 -1 13 -4 297.05 20.02 1 13 -4 286.29 19.90 13 1 -4 330.56 20.90 1 13 -4 318.72 20.39 1 13 5 67.21 5.82 -1 13 5 72.81 5.77 1 13 -5 63.46 5.86 1 13 -5 77.52 6.03 13 1 -5 61.31 6.29 13 -1 -5 72.50 6.65 13 1 -5 71.46 6.41 1 13 6 410.55 25.32 -1 13 6 415.95 25.08 1 13 -6 394.30 24.99 1 13 -6 383.88 24.65 13 1 -6 404.97 25.54 13 -1 -6 400.14 25.53 13 1 -6 387.99 25.44 1 13 7 92.99 6.97 -1 13 7 82.94 6.61 1 13 -7 75.19 6.12 13 1 -7 78.72 6.72 13 -1 -7 77.95 6.69 13 1 -8 8.77 2.16 13 -1 -8 7.20 1.85 1 13 -8 9.27 1.53 13 1 -8 9.69 1.89 13 -1 -8 7.70 1.80 1 13 -9 90.09 6.29 13 1 -9 90.15 6.83 13 -1 -9 88.17 6.87 13 1 -9 101.67 7.12 13 -1 -9 88.73 6.91 13 1 -10 2.98 1.21 1 13 10 5.21 1.09 13 -1 -10 4.32 1.27 13 1 -10 2.58 1.08 13 -1 -10 5.65 1.32 1 13 11 35.88 2.83 -1 13 11 38.37 3.19 13 1 -11 31.28 2.79 13 1 -11 37.02 3.20 13 -1 -11 36.18 3.22 13 1 -12 2.81 0.81 13 -1 -12 1.49 0.71 -1 13 12 2.16 0.76 -1 13 13 8.45 0.94 13 2 0 0.26 0.92 2 13 0 -0.32 1.11 2 13 0 0.48 0.93 13 2 0 -1.39 1.66 2 13 1 103.02 7.09 2 13 -1 96.25 7.23 2 13 1 97.31 7.35 13 2 1 85.89 7.57 13 2 -1 92.51 8.71 13 -2 1 106.19 8.68 13 2 -1 107.59 7.73 13 2 -2 15.05 2.65 2 13 -2 16.23 2.75 13 2 2 8.81 1.89 13 2 -2 15.28 3.37 13 -2 2 14.79 2.46 2 13 3 140.39 9.65 2 13 -3 141.04 9.75 2 13 -3 126.18 9.95 13 2 -3 147.54 11.25 13 -2 3 131.45 9.45 13 2 -3 120.67 10.09 13 2 -4 1.39 1.99 -2 13 4 1.71 1.30 2 13 -4 0.75 1.49 2 13 -4 4.83 1.82 -2 13 5 46.16 4.30 13 2 -5 50.02 5.13 2 13 -5 43.49 4.49 2 13 -5 50.07 4.65 13 2 -5 52.48 5.32 13 -2 -5 53.94 5.29 13 2 -6 8.52 2.32 -2 13 6 5.68 1.60 2 13 -6 5.23 1.44 2 13 -6 7.23 1.73 13 2 -6 7.11 2.16 13 -2 -6 6.08 2.02 -2 13 7 203.07 12.59 2 13 -7 195.95 12.26 13 2 -7 164.88 12.46 13 -2 -7 170.06 12.60 2 13 -7 177.74 11.85 2 13 -8 1.56 1.03 13 2 -8 -0.31 1.13 13 -2 -8 0.32 1.28 13 2 -9 18.39 2.67 13 -2 -9 18.39 2.45 2 13 -9 19.57 2.09 13 2 -9 21.14 2.52 13 -2 -9 27.26 2.86 13 2 -10 -0.72 1.13 13 -2 -10 -0.25 0.97 13 2 -10 -0.21 0.82 13 -2 -10 -0.22 0.94 -2 13 11 62.69 4.32 13 2 -11 53.01 4.13 13 -2 -11 53.71 4.19 13 2 -12 0.43 0.59 -2 13 12 0.29 0.69 -2 13 13 7.73 0.94 3 13 0 680.96 41.46 3 13 0 713.58 42.06 13 3 0 693.62 42.70 13 3 0 686.99 41.58 13 3 -1 160.12 10.52 3 13 1 145.57 9.90 3 13 -1 150.99 10.19 3 13 1 145.26 10.21 3 13 -1 140.44 10.65 13 3 1 143.34 10.59 13 3 -1 155.58 11.65 3 13 2 183.77 12.73 3 13 2 187.48 12.43 3 13 -2 193.72 12.74 13 3 2 182.77 12.60 13 3 -2 208.33 14.49 13 3 -2 184.82 13.25 3 13 3 150.12 9.91 3 13 -3 143.63 10.38 13 3 -3 155.86 11.44 13 -3 3 118.10 9.53 13 3 -3 132.78 10.38 13 3 -4 11.85 2.68 3 13 4 7.51 2.08 -3 13 4 10.97 1.97 3 13 -4 9.79 2.14 3 13 5 201.38 14.49 -3 13 5 227.72 14.18 3 13 -5 228.18 14.54 3 13 -5 192.62 14.32 13 3 -5 207.96 15.07 13 3 -5 232.95 15.20 13 3 -6 14.14 2.64 -3 13 6 12.64 2.15 13 -3 6 17.42 1.84 3 13 -6 20.68 2.52 3 13 -6 16.06 2.44 13 3 -6 14.53 2.63 13 -3 -6 12.98 2.53 -3 13 7 133.46 9.11 13 -3 7 119.46 8.36 3 13 -7 129.83 8.69 3 13 -7 128.04 8.95 13 3 -7 124.02 9.27 13 -3 -7 123.75 9.44 13 -3 8 151.56 10.05 3 13 -8 148.83 10.04 3 13 -8 161.57 10.35 13 3 -8 161.45 10.78 13 -3 -8 150.27 10.85 13 3 -9 25.70 2.96 3 13 -9 26.85 2.50 13 -3 9 20.87 2.34 13 3 -9 28.55 2.86 13 -3 -9 26.67 2.95 13 -3 10 225.94 14.08 3 13 -10 219.04 13.94 13 3 -10 230.68 14.37 13 -3 -10 228.03 14.44 13 3 -10 234.99 14.57 13 -3 -10 227.12 14.62 13 -3 11 47.90 3.46 13 3 -11 47.60 3.84 13 -3 -11 45.97 3.85 -3 13 12 26.97 2.42 13 3 -12 29.75 2.36 13 -3 -12 24.25 2.26 -3 13 13 37.29 2.72 13 4 0 0.24 0.80 4 13 0 0.32 1.28 4 13 0 -0.24 1.03 13 4 0 1.66 1.60 4 13 1 45.96 4.16 4 13 -1 49.25 4.46 4 13 1 53.23 4.58 13 4 1 55.02 4.86 13 4 -1 65.51 5.97 13 4 -1 50.56 4.53 4 13 -1 51.92 4.97 13 4 -2 1.08 1.33 4 13 2 2.95 1.34 4 13 2 0.77 0.99 4 13 2 1.95 0.97 13 4 2 0.83 1.00 4 13 -2 2.69 1.40 13 4 -2 2.18 2.43 4 13 3 119.84 8.75 4 13 3 114.39 8.24 4 13 -3 126.58 9.40 13 4 -3 133.58 10.31 13 4 -3 111.70 9.21 13 4 -4 -0.44 1.71 4 13 4 -0.66 1.31 -4 13 4 1.06 1.00 4 13 -4 -0.77 1.52 4 13 -4 -0.35 1.71 4 13 -5 69.37 5.84 4 13 5 60.57 5.74 -4 13 5 60.37 5.21 4 13 -5 66.86 5.72 13 4 -5 70.22 6.45 13 4 -5 69.69 6.27 13 4 -6 10.84 2.50 4 13 6 10.93 2.43 -4 13 6 13.30 1.97 13 -4 6 6.84 1.27 4 13 -6 9.70 1.86 4 13 -6 12.05 2.26 13 4 -6 8.10 2.13 13 4 -7 17.41 2.90 13 -4 7 20.19 2.19 4 13 -7 22.17 2.51 13 4 -7 20.80 2.88 4 13 -7 22.90 2.73 13 -4 -7 16.72 2.90 13 -4 8 15.46 1.95 4 13 -8 17.54 1.96 4 13 -8 14.02 2.02 13 4 -8 15.19 2.22 13 -4 -8 14.21 2.46 13 -4 9 42.80 3.72 4 13 -9 47.40 3.78 13 4 -9 47.58 4.08 13 -4 -9 45.37 4.15 13 4 -9 51.61 4.29 13 4 -10 8.41 1.56 13 -4 -10 7.16 1.53 13 -4 10 6.13 1.17 4 13 -10 9.20 1.21 13 4 -10 6.16 1.25 13 -4 -10 7.32 1.37 13 -4 11 41.82 3.23 13 4 -11 49.83 3.64 13 -4 -11 41.20 3.55 13 4 -12 11.35 1.37 13 -4 -12 12.76 1.42 -4 13 13 8.87 1.00 5 13 0 287.43 18.03 13 5 0 293.18 18.98 13 5 0 275.59 17.93 5 13 0 297.37 18.63 5 13 1 79.42 6.36 5 13 1 80.03 6.03 5 13 -1 85.57 6.34 5 13 1 79.75 6.39 5 13 -1 87.20 6.98 13 5 1 80.82 6.57 13 5 -1 88.46 7.47 13 5 -1 83.90 6.43 5 13 2 235.40 16.23 5 13 2 264.33 16.14 5 13 2 255.71 15.84 13 5 2 240.48 16.09 13 5 -2 253.52 17.63 13 5 -2 238.29 16.56 5 13 -2 270.60 16.54 13 5 -3 17.74 2.91 5 13 3 14.52 2.34 5 13 3 19.70 2.31 5 13 -3 18.90 3.07 13 5 -3 17.93 3.42 5 13 -3 19.35 2.80 5 13 4 155.96 11.26 -5 13 4 158.96 10.80 5 13 -4 183.60 11.86 13 5 -4 147.45 11.62 13 5 -5 18.57 2.98 5 13 5 22.28 2.95 -5 13 5 15.96 2.12 5 13 -5 20.03 2.81 13 5 -5 11.30 2.88 5 13 -5 14.15 2.59 13 5 -6 12.12 2.55 -5 13 6 8.21 1.70 5 13 -6 9.81 1.82 13 5 -6 7.45 2.08 5 13 -6 11.77 2.27 13 5 -7 32.20 3.51 13 -5 7 25.91 2.63 5 13 -7 27.74 2.83 13 5 -7 24.12 3.03 5 13 -7 25.81 2.96 13 -5 -7 23.66 3.28 13 -5 8 56.01 4.23 5 13 -8 48.21 3.99 5 13 -8 47.12 4.16 13 5 -8 50.95 4.46 13 -5 -8 51.63 4.73 13 -5 9 33.18 3.15 5 13 -9 39.58 3.26 5 13 -9 38.01 3.02 13 5 -9 37.94 3.39 13 5 -9 41.27 3.63 13 -5 -9 31.94 3.43 13 -5 10 253.62 15.64 5 13 -10 261.50 15.53 13 5 -10 237.34 15.64 13 -5 -10 267.48 15.87 13 5 -10 253.67 15.91 13 -5 -10 242.99 15.96 13 5 -11 16.45 1.82 13 -5 -11 17.22 1.88 13 -5 11 16.15 1.62 13 5 -12 -0.11 0.46 13 -5 -12 0.11 0.49 -5 13 12 0.29 0.67 13 6 0 -0.45 0.85 6 13 0 -0.28 1.07 6 13 0 -0.33 1.40 13 6 0 0.74 1.47 6 13 0 -0.24 0.97 13 6 -1 16.12 2.26 6 13 1 15.98 2.31 6 13 -1 22.92 2.51 6 13 1 16.49 2.38 6 13 -1 21.87 3.06 6 13 1 16.27 2.08 13 6 1 13.76 2.28 13 6 -1 15.34 2.96 6 13 -1 19.00 2.45 13 6 -2 1.96 1.35 6 13 2 0.89 1.17 6 13 2 1.28 1.22 6 13 -2 -1.22 2.00 6 13 2 0.42 0.89 13 6 2 1.31 1.15 13 6 -2 0.98 1.65 6 13 -2 0.30 1.27 13 6 -3 5.31 1.90 6 13 3 2.84 1.36 6 13 3 2.79 1.03 13 6 3 1.99 1.01 13 6 -3 3.53 2.48 6 13 -3 1.00 1.52 13 6 -4 9.03 2.24 6 13 4 6.44 1.76 -6 13 4 9.95 1.55 6 13 -4 8.17 2.30 13 6 -5 4.11 1.97 -6 13 5 8.63 1.59 6 13 -5 7.16 2.13 13 6 -6 0.38 1.48 -6 13 6 -0.25 0.90 6 13 -6 0.29 1.16 13 6 -6 -0.36 1.58 6 13 -6 1.30 1.34 13 6 -7 41.85 4.25 6 13 -7 37.82 3.62 6 13 -7 40.70 3.90 13 6 -7 44.08 4.12 13 -6 8 3.49 1.17 6 13 -8 2.11 0.92 13 6 -8 3.31 1.24 6 13 -8 3.69 1.24 13 -6 -8 3.35 1.34 13 6 -9 3.32 1.28 13 -6 9 3.76 1.08 6 13 -9 3.28 0.91 13 6 -9 3.11 1.06 6 13 -9 4.20 1.10 13 -6 -9 2.49 1.18 13 6 -10 1.34 0.88 13 6 -10 2.77 0.86 6 13 -10 3.42 0.85 13 -6 -10 3.52 1.06 13 6 -11 7.14 1.16 13 -6 -11 6.37 1.14 6 13 -11 7.24 0.90 13 -6 -12 0.18 0.42 -6 13 12 0.39 0.59 13 6 -12 0.83 0.47 13 7 0 10.01 1.58 7 13 0 12.78 2.09 7 13 0 14.33 2.37 13 7 0 9.69 2.24 7 13 0 12.07 1.84 7 13 1 161.49 10.77 7 13 -1 158.50 10.72 7 13 1 139.48 10.17 7 13 1 147.31 10.62 7 13 -1 160.47 10.64 7 13 -1 178.72 11.44 13 7 1 151.97 10.76 13 7 -1 150.65 11.40 13 7 -1 162.47 10.62 13 7 -2 4.37 1.52 7 13 2 5.90 1.62 7 13 -2 5.87 1.47 7 13 2 7.34 1.59 7 13 -2 9.74 2.36 13 7 2 3.31 1.13 7 13 2 3.42 1.09 13 7 -2 10.38 2.68 7 13 -2 5.64 1.55 7 13 3 182.12 12.19 -7 13 3 173.60 11.47 7 13 3 177.32 11.52 7 13 -3 174.76 12.12 13 7 -3 177.71 13.01 13 7 -3 167.23 12.25 -7 13 4 565.60 33.07 7 13 4 537.37 32.95 7 13 -4 557.36 34.20 7 13 -4 550.62 33.84 13 7 -4 498.70 34.33 13 7 -4 573.40 34.20 7 13 -5 96.28 7.45 13 7 -5 91.01 7.67 7 13 -6 272.10 17.43 7 13 -6 262.41 17.52 13 7 -6 273.90 17.79 13 7 -6 273.69 17.88 7 13 -7 81.43 6.38 7 13 -7 84.24 6.65 13 7 -7 103.50 7.00 13 7 -7 88.22 6.99 7 13 -8 19.48 2.04 13 7 -8 14.47 2.05 7 13 -8 15.19 2.04 13 -7 -8 15.48 2.29 7 13 -9 94.99 6.41 7 13 -9 98.59 6.65 13 7 -9 93.07 6.65 13 7 -9 95.99 6.92 13 -7 -9 101.67 6.97 7 13 -10 24.71 2.14 13 7 -10 25.11 2.19 13 7 -10 26.78 2.43 13 -7 -10 22.48 2.22 7 13 -11 38.70 2.84 13 7 -11 41.19 3.11 13 -7 -11 45.12 3.21 -7 13 12 78.37 5.19 8 13 0 0.32 1.14 8 13 0 1.28 1.35 13 8 0 0.69 1.16 8 13 0 0.23 0.99 13 8 0 1.67 0.92 8 13 1 93.07 7.00 8 13 1 85.27 6.26 8 13 1 93.83 6.81 8 13 -1 94.05 6.68 8 13 -1 82.54 7.02 13 8 1 88.53 6.75 13 8 -1 77.61 7.16 13 8 -1 86.92 6.51 13 8 -2 1.78 1.17 8 13 2 0.33 1.09 8 13 2 0.50 0.93 8 13 -2 2.00 1.61 13 8 2 0.24 0.84 8 13 2 0.38 0.76 13 8 -2 1.80 1.85 8 13 -2 0.87 1.29 13 8 -3 26.39 3.31 8 13 3 27.56 2.73 13 8 -3 23.22 3.68 8 13 -3 28.16 3.28 13 8 -4 7.08 1.98 8 13 4 5.03 1.20 8 13 -4 6.49 2.05 13 8 -4 2.20 2.02 8 13 -4 5.79 1.90 8 13 -5 111.45 7.80 13 8 -5 83.88 7.52 13 8 -6 9.73 2.34 8 13 -6 9.36 1.89 13 8 -6 8.52 2.09 8 13 -7 87.55 6.10 8 13 -7 76.91 6.19 13 8 -7 77.70 6.19 13 8 -7 82.18 6.41 8 13 -8 5.62 1.15 13 8 -8 3.61 1.22 8 13 -8 6.14 1.36 8 13 -9 19.64 1.91 13 8 -9 22.54 2.15 13 8 -9 28.62 2.54 8 13 -9 21.42 2.17 13 -8 -9 20.57 2.29 13 8 -10 1.70 0.64 8 13 -10 2.36 0.71 13 8 -10 2.08 0.89 8 13 -11 16.62 1.37 13 8 -11 16.67 1.54 13 -8 -11 16.04 1.52 9 13 0 175.37 11.52 9 13 0 178.47 12.07 13 9 0 179.61 12.13 13 9 0 172.20 11.32 9 13 1 4.84 1.37 9 13 -1 4.95 1.76 13 9 1 7.31 1.54 13 9 -1 6.41 1.95 9 13 1 5.29 1.18 9 13 -1 4.93 1.45 13 9 -1 3.06 1.18 9 13 2 7.35 1.42 9 13 -2 8.90 2.26 13 9 2 5.71 1.36 9 13 2 5.85 1.15 13 9 -2 4.63 2.04 9 13 -2 6.92 1.62 13 9 -2 7.19 1.61 13 9 -3 14.48 2.33 9 13 3 15.04 1.89 13 9 -3 12.23 2.75 9 13 -3 13.78 2.25 9 13 -4 196.45 12.22 13 9 -4 177.79 12.13 13 9 -5 24.88 3.10 9 13 -5 26.21 3.08 9 13 -5 22.72 3.01 9 13 -6 152.29 10.20 13 9 -6 148.28 10.40 13 9 -6 144.15 10.41 13 9 -7 9.71 1.81 9 13 -7 5.61 1.40 13 9 -7 9.09 1.68 9 13 -7 7.83 1.66 9 13 -8 15.52 1.80 13 9 -8 17.29 1.93 9 13 -8 18.19 2.03 13 -9 -8 12.82 1.97 9 13 -9 5.62 0.90 13 9 -9 5.61 1.02 9 13 -9 5.93 1.03 13 -9 -9 5.28 1.12 13 9 -9 5.64 1.14 13 9 -10 9.88 1.14 9 13 -10 13.47 1.30 13 9 -10 14.28 1.45 13 9 -11 0.48 0.38 10 13 0 -0.29 1.28 13 10 0 0.60 1.15 10 13 0 -0.81 0.98 13 10 0 1.10 0.77 10 13 1 52.17 4.03 10 13 -1 50.31 4.28 10 13 1 48.67 4.36 10 13 -1 55.65 4.96 13 10 1 50.59 4.40 13 10 -1 54.46 4.93 13 10 -1 55.45 4.29 10 13 2 13.45 1.91 10 13 -2 17.98 2.77 13 10 2 13.33 1.84 13 10 -2 15.04 2.75 10 13 -2 14.28 2.09 13 10 -2 15.54 2.08 10 13 3 6.96 1.29 10 13 -3 5.98 2.03 13 10 -3 7.95 2.16 10 13 -3 7.15 1.72 13 10 -3 7.55 1.66 13 10 -4 0.37 1.45 10 13 -4 1.51 1.40 13 10 -4 1.25 1.26 10 13 -5 25.19 3.05 10 13 -5 23.78 2.94 13 10 -5 22.75 2.95 10 13 -6 1.71 1.18 13 10 -6 -0.53 1.17 10 13 -6 0.27 1.21 13 10 -6 -0.57 1.24 10 13 -7 3.98 1.13 13 10 -7 8.04 1.43 13 10 -7 5.76 1.42 10 13 -8 1.44 0.69 13 10 -8 1.29 0.78 10 13 -8 0.17 0.75 13 -10 -8 -0.59 0.80 10 13 -9 34.83 2.57 13 10 -9 27.74 2.33 13 10 -9 31.68 2.58 10 13 -9 30.28 2.29 13 -10 -9 26.70 2.42 10 13 -10 0.09 0.39 13 10 -10 0.40 0.48 11 13 0 503.93 30.67 13 11 0 494.79 30.54 11 13 0 535.08 31.33 13 11 0 528.97 31.30 11 13 1 136.94 9.22 11 13 -1 141.29 9.12 11 13 -1 129.49 9.61 13 11 1 136.62 9.19 13 11 -1 130.61 8.97 13 11 -1 135.45 9.71 11 13 2 53.97 4.45 11 13 -2 57.98 4.72 13 11 2 62.29 4.52 11 13 -2 59.49 5.30 13 11 -2 46.71 5.02 13 11 -2 68.16 4.85 11 13 3 107.07 7.30 11 13 -3 113.03 7.92 11 13 -3 104.04 8.33 13 11 -3 103.36 8.35 13 11 -3 120.89 8.01 13 11 -4 9.77 2.19 11 13 -4 10.13 1.87 13 11 -4 10.78 1.98 11 13 -5 89.13 6.42 11 13 -5 77.21 6.14 13 11 -5 76.44 6.16 11 13 -6 14.90 2.00 13 11 -6 14.25 2.04 11 13 -6 9.99 1.84 13 11 -6 13.99 2.05 11 13 -7 52.47 3.93 13 11 -7 45.61 3.87 13 11 -7 52.99 4.11 11 13 -8 193.99 12.17 11 13 -8 210.31 12.42 13 11 -8 205.28 12.27 13 -11 -8 182.78 12.34 11 13 -9 41.08 2.89 13 11 -9 37.27 2.71 13 11 -9 37.69 2.89 12 13 0 -0.97 1.13 13 12 0 -0.24 0.95 12 13 0 -0.30 0.63 12 13 1 18.88 2.13 13 12 1 19.32 2.10 12 13 -1 17.30 2.39 13 12 -1 19.07 2.53 12 13 -1 18.23 1.95 13 12 -1 15.00 1.83 12 13 2 2.86 0.84 13 12 2 1.64 0.79 12 13 -2 1.53 1.29 13 12 -2 5.59 1.87 12 13 -2 3.10 1.05 13 12 -2 1.41 0.92 12 13 -3 4.96 1.74 13 12 -3 6.33 1.75 12 13 -3 3.44 1.25 13 12 -3 6.11 1.36 13 12 -4 0.29 1.39 12 13 -4 0.72 1.11 13 12 -4 0.24 0.90 12 13 -5 4.33 1.38 12 13 -5 0.69 0.92 13 12 -5 3.97 1.36 12 13 -6 0.76 0.93 13 12 -6 2.73 1.04 12 13 -6 1.22 1.05 13 12 -6 1.24 0.97 12 13 -7 1.55 0.78 13 12 -7 0.15 0.69 12 13 -7 -0.49 0.86 13 12 -7 0.17 0.79 12 13 -8 0.85 0.49 13 12 -8 1.00 0.52 13 -12 -8 0.68 0.54 13 13 0 200.24 12.84 13 13 1 0.34 0.78 13 13 -1 1.68 1.18 13 13 -1 0.42 0.62 13 13 -2 7.96 1.76 13 13 -2 7.39 1.27 13 13 -3 -0.54 1.15 13 13 -3 0.76 0.84 13 13 -4 54.04 4.42 13 13 -4 61.46 4.79 13 13 -5 0.38 0.90 13 13 -6 55.30 4.22 13 13 -6 57.90 4.21 13 13 -7 0.33 0.48 13 13 -7 -0.38 0.63 13 -13 -7 -0.12 0.55 14 0 0 190.16 13.95 14 0 0 179.14 12.29 14 0 -1 0.37 1.36 14 0 1 -0.44 1.52 14 0 -1 0.65 2.47 14 0 -2 15.55 2.96 14 0 2 17.27 2.57 14 0 -2 15.71 3.80 14 0 -3 -0.50 1.92 0 14 3 -0.32 1.26 14 0 -3 0.63 2.20 0 14 4 150.53 9.90 0 14 -4 120.18 9.73 14 0 -4 133.00 10.99 14 0 -4 133.44 10.56 14 0 -5 0.44 1.57 0 14 5 -0.34 1.30 0 14 -5 3.47 1.52 14 0 -6 28.30 3.75 0 14 6 39.56 3.94 14 0 -6 31.06 3.86 14 0 -7 -0.70 1.48 0 14 7 2.49 1.64 14 0 -7 -0.35 1.39 14 0 -8 40.37 3.99 14 0 -9 -0.53 1.10 14 0 -9 -1.02 1.16 0 14 10 64.65 4.59 14 0 -10 61.65 4.76 14 0 -10 63.19 4.97 14 0 -11 -0.17 0.77 14 0 -12 0.35 0.56 14 1 0 0.28 1.02 14 -1 0 0.32 1.16 14 1 0 -0.52 1.74 14 -1 0 -1.20 2.31 14 1 -1 22.90 3.00 14 1 1 20.99 3.16 14 1 -1 14.65 3.69 14 -1 1 31.98 3.94 14 -1 -1 26.40 4.68 14 1 -2 1.30 1.51 14 1 2 0.65 1.15 14 1 -2 3.25 2.79 14 -1 2 -0.36 1.16 14 -1 -2 -0.71 2.86 -1 14 3 105.31 7.45 1 14 -3 90.64 7.46 14 1 -3 92.11 8.79 14 1 -3 75.70 7.78 14 1 -4 -0.48 1.73 -1 14 4 -0.95 1.34 1 14 -4 1.44 1.66 14 1 -4 -0.55 2.39 14 -1 -4 -0.55 2.56 14 1 -5 22.64 3.40 1 14 5 15.09 2.58 -1 14 5 15.38 2.41 1 14 -5 16.21 2.64 14 1 -6 19.12 2.93 1 14 6 18.75 2.82 -1 14 6 15.96 2.58 14 -1 -6 19.91 2.98 1 14 -6 18.62 2.60 14 1 -6 17.76 2.89 14 -1 -6 16.22 2.86 14 1 -7 34.94 3.90 -1 14 7 33.67 3.74 14 -1 -7 30.02 3.66 1 14 -7 35.84 3.37 14 1 -7 35.42 3.87 14 -1 -7 31.62 3.74 14 1 -8 34.10 3.43 14 -1 -8 23.94 3.08 14 1 -9 14.31 2.13 14 -1 -9 15.04 2.16 14 1 -9 13.61 1.98 14 -1 -9 10.54 1.87 14 1 -10 -0.22 1.03 14 -1 -10 1.12 0.98 -1 14 10 -0.18 0.72 14 1 -10 0.37 0.71 14 -1 -10 -0.20 0.76 -1 14 11 35.17 2.81 14 1 -11 36.19 3.10 14 -1 -11 36.22 3.09 14 1 -12 2.08 0.69 14 -1 -12 1.16 0.58 2 14 0 370.64 24.23 2 14 0 382.03 24.76 14 2 0 422.32 25.78 14 -2 0 436.39 26.86 14 2 0 389.32 24.24 14 2 -1 -1.33 1.35 2 14 -1 0.87 1.11 14 2 1 -0.39 1.42 14 2 -1 -0.58 2.17 14 -2 1 -0.50 1.93 14 -2 -1 1.46 2.53 14 2 -2 46.65 5.12 2 14 2 62.30 5.20 2 14 -2 60.59 5.67 14 2 2 55.76 4.94 14 -2 2 59.07 5.30 14 2 -2 49.93 6.20 14 -2 -2 63.06 7.08 14 2 -3 1.86 1.71 2 14 3 3.31 1.65 2 14 -3 -0.42 1.63 2 14 -3 1.71 1.35 14 2 -3 -1.21 2.34 14 -2 -3 2.59 2.89 -2 14 4 117.04 8.66 2 14 -4 113.25 8.87 2 14 -4 134.90 9.42 14 2 -4 126.75 10.11 14 2 -4 108.56 9.43 14 2 -5 11.74 2.80 -2 14 5 11.61 2.16 2 14 -5 19.67 2.67 2 14 -5 13.35 2.40 -2 14 6 61.85 5.55 2 14 -6 66.89 5.55 14 2 -6 70.57 6.16 14 -2 -6 57.30 5.83 14 2 -6 67.28 6.10 14 2 -7 8.51 2.05 -2 14 7 7.97 1.97 2 14 -7 7.96 1.68 14 2 -7 5.82 1.92 14 -2 -7 8.82 1.98 2 14 -8 58.12 4.47 14 2 -8 48.94 4.71 14 -2 -8 61.65 5.10 14 2 -9 0.77 1.13 14 -2 -9 0.79 1.19 14 2 -9 1.89 1.13 14 -2 -9 0.51 1.03 14 2 -10 145.85 9.98 14 -2 -10 152.74 10.10 14 2 -10 164.24 10.28 14 -2 -10 157.65 10.30 14 2 -11 1.32 0.72 14 -2 -11 2.24 0.86 -2 14 11 2.24 0.82 14 2 -12 1.88 0.62 14 -2 -12 1.11 0.56 -2 14 12 0.37 0.40 14 3 0 -0.24 0.87 3 14 0 1.03 1.16 3 14 0 0.26 0.98 14 3 0 -0.91 1.75 14 -3 0 -0.67 2.38 3 14 -1 162.20 11.84 3 14 -1 163.33 11.31 3 14 1 167.54 11.47 14 3 1 150.02 11.61 14 3 -1 168.02 12.79 14 -3 1 199.01 13.08 14 3 -1 168.83 11.50 14 3 -2 19.55 2.95 3 14 2 20.00 2.77 3 14 -2 20.60 2.74 14 3 2 16.40 2.30 14 3 -2 15.99 3.34 14 -3 2 22.43 3.03 3 14 3 117.23 8.83 3 14 -3 133.31 9.59 14 3 -3 138.28 10.62 14 -3 3 101.09 8.37 14 -3 -3 135.81 10.86 14 3 -3 127.87 9.60 14 3 -4 9.25 2.37 3 14 4 6.25 1.92 -3 14 4 6.43 1.67 3 14 -4 10.37 2.28 3 14 -4 7.81 2.01 14 3 -4 5.86 2.80 3 14 5 104.78 7.90 -3 14 5 94.56 7.26 3 14 -5 91.78 7.56 3 14 -5 110.67 7.74 14 -3 -5 80.23 7.97 14 3 -5 101.85 8.26 14 3 -6 19.67 3.03 -3 14 6 12.88 2.19 3 14 -6 14.44 2.13 3 14 -6 14.47 2.29 14 3 -6 18.84 2.91 14 -3 -6 12.09 2.59 3 14 -7 88.02 6.25 3 14 -7 83.00 5.97 14 3 -7 84.39 6.60 14 -3 -7 63.29 6.37 14 3 -7 82.58 6.74 3 14 -8 5.40 1.24 14 3 -8 7.99 1.79 14 -3 -8 5.74 1.70 3 14 -9 54.37 4.13 14 3 -9 62.29 4.63 14 -3 -9 55.38 4.68 14 3 -9 54.08 4.58 14 -3 -9 51.80 4.55 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1 -2 318.98 23.27 15 -1 2 315.40 21.39 15 -1 -2 361.47 24.06 15 1 -2 350.60 22.09 15 -1 -2 333.64 22.21 -1 15 3 92.50 7.34 15 1 -3 96.75 8.97 15 1 -3 83.53 7.79 15 -1 -3 91.74 8.15 15 1 -4 35.80 4.47 15 -1 -4 27.14 4.14 -1 15 4 37.19 3.84 15 1 -4 29.21 4.50 15 -1 -4 35.51 4.83 1 15 5 78.63 6.48 -1 15 5 71.45 6.21 15 1 -5 77.41 6.85 15 -1 -5 75.49 6.73 15 1 -6 13.58 2.59 15 -1 -6 8.99 2.14 1 15 6 15.14 2.66 -1 15 6 11.73 2.21 15 1 -6 15.14 2.69 15 -1 -6 12.05 2.53 15 1 -7 66.32 5.36 15 -1 -7 59.03 5.24 15 1 -7 61.10 5.36 15 -1 -7 50.83 5.06 15 1 -8 54.17 4.57 15 -1 -8 50.34 4.56 15 1 -9 43.88 3.61 15 -1 -9 45.80 3.73 15 1 -9 34.15 3.52 15 -1 -9 41.61 3.76 15 1 -10 333.73 20.00 15 -1 -10 302.82 19.95 15 1 -10 343.14 20.25 15 -1 -10 348.77 20.29 15 1 -11 17.48 1.77 15 -1 -11 19.77 1.84 15 -2 0 1.18 1.08 15 2 0 -0.47 2.00 15 -2 0 2.99 2.57 15 2 1 84.49 7.40 15 2 -1 105.58 8.80 15 -2 1 96.32 8.05 15 -2 -1 99.87 9.28 15 2 -1 93.87 7.18 15 2 -2 7.34 1.91 2 15 2 11.83 2.17 15 2 2 8.16 1.76 15 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3 -2 4.74 2.75 15 -3 2 3.50 1.64 15 -3 -2 7.95 3.45 15 3 -3 35.41 4.21 3 15 3 43.35 4.15 -3 15 3 39.94 3.91 3 15 -3 27.85 4.08 15 3 -3 38.74 5.23 3 15 4 363.13 22.26 -3 15 4 356.61 21.83 3 15 -4 326.36 22.02 3 15 -4 334.00 22.21 15 3 -4 391.59 23.55 15 -3 -4 390.07 23.59 15 3 -4 291.66 22.24 15 3 -5 18.13 2.95 3 15 5 13.82 2.60 -3 15 5 14.17 2.29 3 15 -5 16.80 2.41 3 15 -5 12.84 2.35 -3 15 6 326.41 21.90 3 15 -6 353.94 22.00 15 3 -6 351.30 22.45 15 -3 -6 356.53 22.56 15 3 -6 364.27 22.57 15 3 -7 20.68 2.78 15 -3 -7 22.49 2.93 3 15 -7 24.36 2.59 15 3 -7 22.63 2.89 15 -3 -7 20.41 2.76 15 3 -8 7.89 1.79 3 15 -8 7.68 1.36 15 3 -8 6.60 1.51 15 -3 -8 5.87 1.62 15 -3 -9 18.41 2.35 15 3 -9 18.68 2.17 15 3 -10 35.08 3.03 15 -3 -10 42.55 3.20 15 3 -10 40.32 3.32 15 -3 -10 45.84 3.45 -3 15 11 15.98 1.45 15 -3 -11 17.10 1.66 15 3 -11 16.08 1.59 4 15 0 -0.32 1.16 4 15 0 0.35 1.51 15 4 0 -1.22 1.57 15 -4 0 0.63 2.24 15 4 -1 29.94 3.11 4 15 1 31.60 3.40 4 15 -1 34.34 3.86 4 15 -1 26.70 3.11 15 4 1 23.83 3.12 15 4 -1 30.46 4.21 15 -4 1 31.03 4.04 15 -4 -1 31.69 5.10 15 4 -2 10.27 2.04 4 15 2 10.02 2.02 4 15 -2 11.59 2.19 15 4 2 10.39 1.80 15 4 -2 9.89 3.06 15 -4 2 8.13 2.06 15 -4 -2 17.79 4.11 4 15 3 49.86 4.83 -4 15 3 46.73 4.42 4 15 -3 56.21 5.36 15 4 -3 53.30 5.18 15 4 -3 51.83 5.91 15 -4 -3 52.81 6.29 15 4 -4 -0.41 1.48 4 15 4 1.07 1.37 -4 15 4 1.65 1.18 4 15 -4 -0.74 1.76 15 4 -4 1.50 2.19 15 -4 -4 -0.53 1.88 15 4 -5 39.30 4.51 4 15 5 50.36 4.78 -4 15 5 42.25 4.02 4 15 -5 45.66 4.30 4 15 -5 41.92 4.24 15 4 -6 5.03 1.85 -4 15 6 7.41 1.61 4 15 -6 5.93 1.54 4 15 -6 7.59 1.71 15 4 -6 3.16 1.71 15 -4 -6 7.00 2.06 15 4 -7 22.37 2.90 4 15 -7 22.10 2.54 15 4 -7 22.65 2.84 15 -4 -7 24.51 3.02 15 4 -8 -1.27 1.21 4 15 -8 1.26 0.74 15 4 -8 2.08 1.09 15 -4 -8 0.51 1.05 15 4 -9 29.32 2.71 15 -4 -9 32.65 2.90 15 -4 -9 28.84 2.90 15 4 -10 0.15 0.65 15 -4 -10 0.99 0.75 15 4 -10 0.49 0.56 15 -4 -10 -0.26 0.64 15 4 -11 9.96 1.15 15 -4 -11 11.42 1.22 -4 15 11 9.39 1.07 5 15 0 84.36 6.77 5 15 0 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56.19 4.19 15 5 -10 1.40 0.72 15 -5 -10 2.87 0.85 15 5 -10 2.00 0.59 15 -5 -10 1.49 0.63 15 5 -11 27.11 2.06 15 -5 -11 25.94 2.07 6 15 0 -0.95 1.31 6 15 0 -1.62 1.39 6 15 0 -0.48 1.13 15 6 0 2.12 1.57 15 6 -1 10.73 1.71 6 15 1 12.86 2.32 6 15 -1 11.51 2.16 6 15 1 13.89 2.17 6 15 -1 14.91 2.68 6 15 -1 13.09 2.03 15 6 1 14.07 2.11 15 6 -1 12.24 2.59 15 6 -2 2.58 1.23 6 15 2 4.62 1.57 6 15 -2 2.26 1.33 -6 15 2 1.69 0.98 6 15 -2 1.17 1.71 15 6 2 0.23 0.85 6 15 -2 2.88 1.46 15 6 -2 0.47 1.87 15 -6 2 0.34 1.23 15 6 -3 -0.67 1.46 6 15 3 0.34 1.28 -6 15 3 0.47 0.95 6 15 -3 -0.32 1.16 6 15 -3 -0.62 1.48 15 6 -3 -0.48 1.99 15 6 -4 3.25 1.80 -6 15 4 1.14 0.96 6 15 -4 2.66 1.32 6 15 -4 1.39 1.38 6 15 -4 0.32 1.55 15 6 -4 0.45 1.68 15 6 -5 2.50 1.65 -6 15 5 1.11 1.00 6 15 -5 3.50 1.48 15 6 -6 0.97 1.46 6 15 -6 0.47 1.01 15 6 -6 1.88 1.42 6 15 -6 1.85 1.35 15 -6 -6 0.33 1.49 15 6 -7 0.27 1.07 6 15 -7 0.18 0.73 15 6 -7 0.25 1.12 6 15 -7 -0.43 0.96 15 -6 -7 1.39 1.38 15 6 -8 -0.88 1.10 15 6 -8 1.77 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0.61 0.63 -3 20 0 -0.15 0.66 -3 20 1 33.02 2.65 -3 20 -1 30.39 2.66 -3 20 -2 3.93 0.90 0 0 0 0.00 0.00 TITL HY in P4/ncc REM P4/ncc (#130 in standard setting) CELL 1.54184 16.389873 16.389873 14.345279 90.0000 90.0000 90.0000 ZERR 17.00 0.000125 0.000125 0.000179 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y+1/2, z SYMM -y+1/2, x, z SYMM y,-x+1/2, z SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y,-z+1/2 SYMM y+1/2, x+1/2,-z+1/2 SYMM -y,-x,-z+1/2 SFAC C H N O UNIT 187.00 170.00 17.00 17.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 55889 _shelx_fab_file ; 0 0 2 -11.1182 7.7266 0 0 4 6.9050 10.4948 0 0 6 10.2190 6.2998 0 0 8 -0.4133 8.3069 0 0 10 -3.1577 3.5894 0 0 12 1.5912 6.2724 0 0 14 0.7548 3.4651 0 0 16 -2.0418 3.8831 1 0 2 -15.5679 -0.9144 1 0 4 5.1377 -0.2963 1 0 6 1.8211 0.3583 1 0 8 -2.2242 0.8920 1 0 10 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0.5714 20 1 1 -0.0255 -1.4605 20 1 2 0.2557 -0.0894 20 1 3 0.2243 0.5587 20 2 0 -1.7898 2.1290 20 2 1 -0.5812 -0.7953 20 2 2 0.7035 -2.2482 20 3 1 0.0953 0.6135 20 3 2 -0.4312 0.4487 0 0 0 0.0 0.0 ; _shelx_fab_checksum 52441 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.605 _oxdiff_exptl_absorpt_empirical_full_min 0.564