data_r1 _audit_creation_date 2021-07-21 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _shelx_SHELXL_version_number '2018/3' loop_ _audit_author_name _audit_author_email _audit_author_address 'Berreau, L.M.' lisa.berreau@usu.edu ; Utah State University Chemistry and Biochemistry 0300 Old Main Hill Logan 84322 United States of America ; 'Anderson, S.N.' steve.and29@aggiemail.usu.edu ; Utah State University Chemistry and Biochemistry 0300 Old Main Hill Logan 84322 United States of America ; _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(C23 H21 N O3)' _chemical_formula_sum 'C46 H42 N2 O6' _chemical_formula_weight 718.81 _chemical_melting_point ? _chemical_oxdiff_formula 'C46 N2 O4' _chemical_oxdiff_usercomment 'Flav-1 Diethylamino Derivative' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 61 _space_group_name_H-M_alt 'P b c a' _space_group_name_Hall '-P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 15.8887(3) _cell_length_b 14.1192(2) _cell_length_c 32.2636(5) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 7237.9(2) _cell_formula_units_Z 8 _cell_measurement_reflns_used 26257 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 29.1070 _cell_measurement_theta_min 1.8570 _shelx_estimated_absorpt_T_max 0.974 _shelx_estimated_absorpt_T_min 0.962 _exptl_absorpt_coefficient_mu 0.087 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.826 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.45a (Rigaku Oxford Diffraction, 2019) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear orangish orange' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier orangish _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.319 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description needle _exptl_crystal_F_000 3040 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 1 -2 1 0.2180 1 -1 2 0.2338 0 -1 0 0.1873 0 -2 -1 0.1735 -1 0 -2 0.1307 1 0 2 0.1723 0 1 1 0.2299 1 -2 -1 0.2212 -2 2 -1 0.1871 -2 1 -2 0.1421 2 -1 2 0.2407 1 -2 -2 0.2169 2 -2 -1 0.2432 -2 1 -1 0.1474 0 -1 -2 0.2090 0 1 2 0.1885 -2 1 0 0.1548 -1 0 -1 0.1500 -2 1 2 0.1536 1 0 -1 0.1847 -1 0 1 0.1684 1 0 -2 0.1616 -1 0 2 0.1584 2 1 2 0.2104 2 1 -2 0.1812 0 0 1 0.2114 0 0 -1 0.1680 1 1 -2 0.1707 -1 -1 2 0.2318 -1 -1 0 0.2389 -2 -2 1 0.2366 -1 -1 1 0.2300 0 1 -2 0.1979 0 -1 2 0.2670 -1 1 2 0.1528 _exptl_crystal_preparation 'See liturature' _exptl_crystal_recrystallization_method ? _exptl_crystal_size_max 0.442 _exptl_crystal_size_mid 0.32 _exptl_crystal_size_min 0.303 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 1.0008 -1.9993 0.9992 0.0057 0.1118 -0.0064 1.0006 -0.9993 1.9963 -0.0005 0.0693 -0.0405 0.0003 -1.0000 0.0013 -0.0075 0.0465 0.0174 0.0004 -2.0000 -0.9958 -0.0012 0.0890 0.0515 -1.0004 -0.0007 -1.9950 -0.0069 -0.0228 0.0579 1.0004 0.0007 1.9950 0.0069 0.0228 -0.0579 -0.0002 1.0000 0.9971 -0.0062 -0.0424 -0.0341 1.0006 -1.9994 -0.9975 0.0331 0.1037 0.0270 -2.0009 1.9987 -0.9975 -0.0400 -0.1265 0.0309 -2.0008 0.9987 -1.9946 -0.0337 -0.0840 0.0650 2.0008 -0.9987 1.9946 0.0337 0.0840 -0.0650 1.0005 -1.9995 -1.9959 0.0467 0.0996 0.0437 2.0007 -1.9989 -0.9992 0.0673 0.1184 0.0024 -2.0007 0.9988 -0.9962 -0.0474 -0.0800 0.0483 0.0001 -1.0001 -1.9955 0.0199 0.0384 0.0508 -0.0001 1.0001 1.9955 -0.0199 -0.0384 -0.0508 -2.0006 0.9988 0.0021 -0.0611 -0.0759 0.0317 -1.0003 -0.0006 -0.9967 -0.0206 -0.0188 0.0412 -2.0004 0.9989 1.9989 -0.0885 -0.0678 -0.0017 1.0001 0.0005 -1.0001 0.0480 0.0106 -0.0079 -1.0001 -0.0005 1.0001 -0.0480 -0.0106 0.0079 1.0000 0.0005 -1.9984 0.0616 0.0066 0.0088 -1.0000 -0.0005 1.9984 -0.0616 -0.0066 -0.0088 2.0003 1.0012 1.9920 0.0487 -0.0090 -0.0999 1.9999 1.0010 -2.0014 0.1034 -0.0252 -0.0331 0.0001 0.0001 0.9984 -0.0137 0.0041 -0.0167 -0.0001 -0.0001 -0.9984 0.0137 -0.0041 0.0167 0.9997 1.0004 -1.9997 0.0691 -0.0399 -0.0086 -0.9997 -1.0004 1.9997 -0.0691 0.0399 0.0086 -0.9999 -1.0005 0.0030 -0.0417 0.0318 0.0420 -1.9997 -2.0010 1.0043 -0.0972 0.0677 0.0673 -0.9998 -1.0005 1.0013 -0.0554 0.0359 0.0253 -0.0005 0.9999 -1.9980 0.0348 -0.0546 0.0159 0.0005 -0.9999 1.9980 -0.0348 0.0546 -0.0159 -1.0002 0.9995 1.9972 -0.0542 -0.0531 -0.0262 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0383 _diffrn_reflns_av_unetI/netI 0.0277 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 46 _diffrn_reflns_limit_l_min -45 _diffrn_reflns_number 150211 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.629 _diffrn_reflns_theta_min 1.799 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type 'Rigaku Saturn724+' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -11.00 86.00 0.50 10.75 -- 20.00 54.00-115.31 194 2 \w -73.00 38.00 0.50 10.75 -- 20.00 54.00 115.15 222 3 \w 82.00 108.00 0.50 10.75 -- 20.00 54.00 115.15 52 4 \w -68.00 49.00 0.50 10.75 -- 20.00 54.00 0.00 234 5 \w 58.00 109.00 0.50 10.75 -- 20.00 54.00 0.00 102 6 \w -71.00 104.00 0.50 10.75 -- 20.00 54.00-180.00 350 7 \w -74.00 71.00 0.50 10.75 -- 20.00 54.00 60.00 290 8 \w 75.00 104.00 0.50 10.75 -- 20.00 54.00 60.00 58 9 \w -66.00 37.00 0.50 10.75 -- 20.00 54.00 -30.00 206 10 \w -67.00 6.00 0.50 10.75 -- 20.00 54.00 150.00 146 11 \w 40.00 65.00 0.50 10.75 -- 20.00 54.00 150.00 50 12 \w -74.00 -27.00 0.50 10.75 -- 20.00 54.00 -90.00 94 13 \w -71.00 6.00 0.50 10.75 -- 20.00 54.00-120.00 154 14 \w 65.00 90.00 0.50 10.75 -- 20.00 54.00-120.00 50 15 \w -68.00 -40.00 0.50 10.75 -- 20.00 54.00 -60.00 56 16 \w -69.00 -44.00 0.50 10.75 -- 20.00 54.00-150.00 50 17 \w -39.00 -14.00 0.50 10.75 -- 20.00 54.00-150.00 50 18 \w -66.00 -38.00 0.50 10.75 -- 20.00 54.00 30.00 56 19 \w -66.00 -41.00 0.50 10.75 -- 20.00 54.00-115.31 50 ; _diffrn_measurement_device 'two-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Mini II' _diffrn_measurement_method '\w scans' _diffrn_measurement_specimen_support 'Mitegen 50um' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0342507000 _diffrn_orient_matrix_UB_12 0.0074486000 _diffrn_orient_matrix_UB_13 -0.0137075000 _diffrn_orient_matrix_UB_21 0.0147353000 _diffrn_orient_matrix_UB_22 -0.0465021000 _diffrn_orient_matrix_UB_23 0.0040716000 _diffrn_orient_matrix_UB_31 -0.0245559000 _diffrn_orient_matrix_UB_32 -0.0174520000 _diffrn_orient_matrix_UB_33 -0.0167030000 _diffrn_radiation_collimation 0.3 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_current 24.0 _diffrn_source_power 1.2 _diffrn_source_target Mo _diffrn_source_type 'Rigaku (Mo) X-ray Source' _diffrn_source_voltage 50.0 _diffrn_special_details None _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 7456 _reflns_number_total 11029 _reflns_odcompleteness_completeness 99.93 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.40.45a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.45a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.45a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.867 _refine_diff_density_min -0.407 _refine_diff_density_rms 0.066 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 493 _refine_ls_number_reflns 11029 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1014 _refine_ls_R_factor_gt 0.0651 _refine_ls_restrained_S_all 1.026 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0861P)^2^+6.9315P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1691 _refine_ls_wR_factor_ref 0.1952 _refine_special_details None _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Secondary CH2 refined with riding coordinates: C22B(H22D,H22E), C23A(H23A,H23B), C20B(H20A,H20B), C21A(H21A,H21B) 2.b Aromatic/amide H refined with riding coordinates: C15A(H15A), C15B(H15B), C11A(H11A), C4A(H4A), C11B(H11B), C4B(H4B), C16B(H16B), C9A(H9A), C16A(H16A), C19B(H19B), C9B(H9B), C19A(H19A), C8A(H8A), C18A(H18A), C6B(H6B), C18B(H18B), C8B(H8B), C7B(H7B), C7A(H7A), C6A(H6A) 2.c Idealised Me refined as rotating group: C23B(H23C,H23D,H23E), C24A(H24A,H24B,H24C), C21B(H21C,H21D,H21E), C22A(H22A, H22B,H22C) 2.d Idealised tetrahedral OH refined as rotating group: O2A(H2A), O2B(H2B) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O3A O 0.35495(8) 0.05923(9) 0.42868(4) 0.0229(3) Uani 1 1 d . . . . . O3B O 0.35854(8) 0.71011(9) 0.38673(4) 0.0232(3) Uani 1 1 d . . . . . O1B O 0.46275(9) 0.44969(9) 0.36776(4) 0.0299(3) Uani 1 1 d . . . . . O2A O 0.38728(10) 0.27885(9) 0.37262(4) 0.0303(3) Uani 1 1 d . . . . . H2A H 0.416285 0.324450 0.379230 0.045 Uiso 1 1 calc R U . . . O1A O 0.46296(10) 0.31821(9) 0.44588(5) 0.0323(3) Uani 1 1 d . . . . . O2B O 0.39132(10) 0.49101(10) 0.44292(4) 0.0315(3) Uani 1 1 d . . . . . H2B H 0.418630 0.444324 0.436019 0.047 Uiso 1 1 calc R U . . . N1B N 0.21762(12) 0.80914(13) 0.56310(5) 0.0335(4) Uani 1 1 d . . . . . N1A N 0.20173(13) -0.02794(13) 0.25162(5) 0.0355(4) Uani 1 1 d . . . . . C13B C 0.36043(11) 0.64545(12) 0.41850(5) 0.0210(3) Uani 1 1 d . . . . . C12A C 0.38874(11) 0.08013(12) 0.46671(6) 0.0219(3) Uani 1 1 d . . . . . C12B C 0.39252(11) 0.69033(13) 0.34883(5) 0.0225(3) Uani 1 1 d . . . . . C13A C 0.35590(11) 0.12413(12) 0.39702(6) 0.0216(3) Uani 1 1 d . . . . . C3B C 0.43074(11) 0.60207(12) 0.34068(6) 0.0227(3) Uani 1 1 d . . . . . C14A C 0.31629(11) 0.08613(13) 0.35961(6) 0.0228(3) Uani 1 1 d . . . . . C14B C 0.32304(11) 0.68442(12) 0.45589(6) 0.0228(3) Uani 1 1 d . . . . . C3A C 0.42901(12) 0.16733(12) 0.47430(6) 0.0237(4) Uani 1 1 d . . . . . C2B C 0.43187(12) 0.53002(12) 0.37309(6) 0.0235(3) Uani 1 1 d . . . . . C1B C 0.39406(12) 0.55683(13) 0.41208(6) 0.0237(4) Uani 1 1 d . . . . . C2A C 0.43073(12) 0.23803(13) 0.44146(6) 0.0254(4) Uani 1 1 d . . . . . C15A C 0.27922(12) -0.00445(13) 0.35972(6) 0.0245(4) Uani 1 1 d . . . . . H15A H 0.279930 -0.039792 0.384040 0.029 Uiso 1 1 calc R U . . . C1A C 0.39081(12) 0.21192(12) 0.40308(6) 0.0237(4) Uani 1 1 d . . . . . C15B C 0.27999(12) 0.77179(13) 0.45431(6) 0.0243(4) Uani 1 1 d . . . . . H15B H 0.275433 0.803038 0.429032 0.029 Uiso 1 1 calc R U . . . C11A C 0.38218(11) 0.01143(13) 0.49680(6) 0.0234(3) Uani 1 1 d . . . . . H11A H 0.356318 -0.046097 0.490890 0.028 Uiso 1 1 calc R U . . . C4A C 0.46308(12) 0.18430(13) 0.51307(6) 0.0271(4) Uani 1 1 d . . . . . H4A H 0.490732 0.241193 0.518116 0.033 Uiso 1 1 calc R U . . . C10A C 0.41499(11) 0.02900(13) 0.53666(6) 0.0241(4) Uani 1 1 d . . . . . C11B C 0.38737(12) 0.76036(13) 0.31925(6) 0.0261(4) Uani 1 1 d . . . . . H11B H 0.362885 0.818364 0.325678 0.031 Uiso 1 1 calc R U . . . C4B C 0.46337(12) 0.58551(14) 0.30144(6) 0.0258(4) Uani 1 1 d . . . . . H4B H 0.489144 0.527809 0.295771 0.031 Uiso 1 1 calc R U . . . C16B C 0.24456(12) 0.81222(14) 0.48898(6) 0.0264(4) Uani 1 1 d . . . . . H16B H 0.216093 0.869518 0.486580 0.032 Uiso 1 1 calc R U . . . C10B C 0.41934(12) 0.74370(14) 0.27925(6) 0.0263(4) Uani 1 1 d . . . . . C5B C 0.45813(12) 0.65434(14) 0.27018(6) 0.0268(4) Uani 1 1 d . . . . . C17B C 0.25071(13) 0.76818(14) 0.52809(6) 0.0271(4) Uani 1 1 d . . . . . C5A C 0.45650(12) 0.11684(13) 0.54494(6) 0.0258(4) Uani 1 1 d . . . . . C9A C 0.40904(12) -0.03905(14) 0.56918(6) 0.0283(4) Uani 1 1 d . . . . . H9A H 0.382796 -0.096830 0.564231 0.034 Uiso 1 1 calc R U . . . C16A C 0.24177(13) -0.04251(13) 0.32478(6) 0.0278(4) Uani 1 1 d . . . . . H16A H 0.217597 -0.102401 0.326258 0.033 Uiso 1 1 calc R U . . . C19B C 0.32761(13) 0.63982(13) 0.49459(6) 0.0285(4) Uani 1 1 d . . . . . H19B H 0.354665 0.581605 0.496701 0.034 Uiso 1 1 calc R U . . . C9B C 0.41414(14) 0.81375(15) 0.24739(6) 0.0327(4) Uani 1 1 d . . . . . H9B H 0.389405 0.872058 0.252983 0.039 Uiso 1 1 calc R U . . . C19A C 0.31343(13) 0.13595(14) 0.32197(6) 0.0279(4) Uani 1 1 d . . . . . H19A H 0.336290 0.196521 0.320728 0.034 Uiso 1 1 calc R U . . . C17A C 0.23942(13) 0.00764(14) 0.28686(6) 0.0275(4) Uani 1 1 d . . . . . C8A C 0.44151(13) -0.02027(16) 0.60758(6) 0.0322(4) Uani 1 1 d . . . . . H8A H 0.436695 -0.065277 0.628490 0.039 Uiso 1 1 calc R U . . . C18A C 0.27774(13) 0.09771(14) 0.28683(6) 0.0294(4) Uani 1 1 d . . . . . H18A H 0.278967 0.132390 0.262334 0.035 Uiso 1 1 calc R U . . . C6B C 0.48944(13) 0.63835(16) 0.22936(6) 0.0325(4) Uani 1 1 d . . . . . H6B H 0.514556 0.580713 0.222915 0.039 Uiso 1 1 calc R U . . . C18B C 0.29303(14) 0.67995(14) 0.52970(6) 0.0302(4) Uani 1 1 d . . . . . H18B H 0.297605 0.648430 0.554907 0.036 Uiso 1 1 calc R U . . . C8B C 0.44551(14) 0.79536(17) 0.20858(6) 0.0359(5) Uani 1 1 d . . . . . H8B H 0.442113 0.841439 0.188045 0.043 Uiso 1 1 calc R U . . . C7B C 0.48290(14) 0.70694(17) 0.19959(7) 0.0364(5) Uani 1 1 d . . . . . H7B H 0.503344 0.695195 0.173078 0.044 Uiso 1 1 calc R U . . . C7A C 0.48218(14) 0.06645(16) 0.61586(7) 0.0345(5) Uani 1 1 d . . . . . H7A H 0.503947 0.078185 0.642121 0.041 Uiso 1 1 calc R U . . . C6A C 0.48974(14) 0.13320(15) 0.58552(6) 0.0331(4) Uani 1 1 d . . . . . H6A H 0.516846 0.190072 0.591289 0.040 Uiso 1 1 calc R U . . . C22B C 0.21479(14) 0.75831(17) 0.60233(6) 0.0357(5) Uani 1 1 d . . . . . H22D H 0.203489 0.691951 0.596886 0.043 Uiso 1 1 calc R U . . . H22E H 0.168646 0.782859 0.618832 0.043 Uiso 1 1 calc R U . . . C23A C 0.20842(15) 0.02349(16) 0.21237(6) 0.0355(5) Uani 1 1 d . . . . . H23A H 0.196653 0.089940 0.217327 0.043 Uiso 1 1 calc R U . . . H23B H 0.165940 -0.000249 0.193433 0.043 Uiso 1 1 calc R U . . . C23B C 0.29588(15) 0.76636(18) 0.62717(7) 0.0392(5) Uani 1 1 d . . . . . H23C H 0.341661 0.740646 0.611345 0.059 Uiso 1 1 calc R U . . . H23D H 0.290229 0.731752 0.652628 0.059 Uiso 1 1 calc R U . . . H23E H 0.306914 0.831776 0.633201 0.059 Uiso 1 1 calc R U . . . C20B C 0.18984(15) 0.90958(16) 0.56350(7) 0.0361(5) Uani 1 1 d . . . . . H20A H 0.221502 0.944569 0.542849 0.043 Uiso 1 1 calc R U . . . H20B H 0.202345 0.936872 0.590391 0.043 Uiso 1 1 calc R U . . . C24A C 0.29428(17) 0.01474(19) 0.19192(7) 0.0449(6) Uani 1 1 d . . . . . H24A H 0.294655 0.050205 0.166533 0.067 Uiso 1 1 calc R U . . . H24B H 0.305739 -0.050673 0.186084 0.067 Uiso 1 1 calc R U . . . H24C H 0.336672 0.039171 0.210230 0.067 Uiso 1 1 calc R U . . . C21B C 0.09617(16) 0.92067(19) 0.55469(8) 0.0462(6) Uani 1 1 d . . . . . H21C H 0.084831 0.902988 0.526502 0.069 Uiso 1 1 calc R U . . . H21D H 0.079949 0.985432 0.558960 0.069 Uiso 1 1 calc R U . . . H21E H 0.064686 0.880566 0.573045 0.069 Uiso 1 1 calc R U . . . C21A C 0.14046(19) -0.1054(2) 0.25241(8) 0.0529(7) Uani 1 1 d . . . . . H21A H 0.086539 -0.081205 0.243087 0.064 Uiso 1 1 calc R U . . . H21B H 0.133620 -0.126367 0.280841 0.064 Uiso 1 1 calc R U . . . C22A C 0.1631(2) -0.1872(2) 0.22683(12) 0.0678(9) Uani 1 1 d . . . . . H22A H 0.166228 -0.168261 0.198295 0.102 Uiso 1 1 calc R U . . . H22B H 0.121081 -0.235615 0.229883 0.102 Uiso 1 1 calc R U . . . H22C H 0.216687 -0.211406 0.235537 0.102 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O3A 0.0276(6) 0.0185(6) 0.0225(6) 0.0020(5) 0.0004(5) -0.0006(5) O3B 0.0296(7) 0.0197(6) 0.0203(6) -0.0008(5) 0.0024(5) -0.0013(5) O1B 0.0395(8) 0.0199(6) 0.0302(7) -0.0010(5) 0.0076(6) 0.0024(6) O2A 0.0479(9) 0.0176(6) 0.0255(7) 0.0021(5) 0.0013(6) -0.0035(6) O1A 0.0406(8) 0.0198(6) 0.0367(8) 0.0009(6) -0.0036(6) -0.0040(6) O2B 0.0479(9) 0.0198(6) 0.0267(7) 0.0021(5) 0.0087(6) 0.0043(6) N1B 0.0410(10) 0.0355(9) 0.0241(8) -0.0053(7) 0.0028(7) 0.0047(8) N1A 0.0466(11) 0.0362(9) 0.0236(8) 0.0005(7) -0.0027(7) -0.0102(8) C13B 0.0232(8) 0.0190(7) 0.0207(8) 0.0001(6) 0.0003(6) -0.0036(6) C12A 0.0216(8) 0.0201(8) 0.0241(8) -0.0007(6) 0.0007(7) 0.0026(6) C12B 0.0255(8) 0.0221(8) 0.0200(8) -0.0014(6) 0.0005(7) -0.0029(7) C13A 0.0229(8) 0.0183(7) 0.0236(8) 0.0013(6) 0.0037(7) 0.0034(6) C3B 0.0240(8) 0.0208(8) 0.0234(8) -0.0010(7) 0.0009(7) -0.0031(6) C14A 0.0233(8) 0.0212(8) 0.0240(8) -0.0001(7) 0.0036(7) 0.0033(7) C14B 0.0255(8) 0.0206(8) 0.0223(8) -0.0034(6) 0.0014(7) -0.0035(7) C3A 0.0245(8) 0.0195(8) 0.0273(9) -0.0001(7) -0.0006(7) 0.0020(6) C2B 0.0271(9) 0.0190(7) 0.0242(8) -0.0024(6) 0.0029(7) -0.0024(7) C1B 0.0287(9) 0.0201(8) 0.0223(8) 0.0003(6) 0.0030(7) -0.0026(7) C2A 0.0283(9) 0.0184(8) 0.0294(9) 0.0001(7) 0.0021(7) 0.0009(7) C15A 0.0301(9) 0.0193(8) 0.0242(8) 0.0013(7) 0.0033(7) 0.0024(7) C1A 0.0295(9) 0.0177(7) 0.0239(8) 0.0007(6) 0.0035(7) 0.0030(7) C15B 0.0252(8) 0.0240(8) 0.0236(8) -0.0021(7) -0.0011(7) -0.0019(7) C11A 0.0238(8) 0.0200(8) 0.0265(8) 0.0012(7) 0.0013(7) -0.0003(6) C4A 0.0293(9) 0.0208(8) 0.0312(9) -0.0008(7) -0.0038(8) -0.0008(7) C10A 0.0207(8) 0.0239(8) 0.0276(9) 0.0007(7) 0.0011(7) 0.0016(7) C11B 0.0294(9) 0.0223(8) 0.0266(9) 0.0010(7) 0.0002(7) -0.0015(7) C4B 0.0267(9) 0.0253(9) 0.0253(8) -0.0016(7) 0.0042(7) -0.0031(7) C16B 0.0258(9) 0.0252(9) 0.0282(9) -0.0054(7) -0.0009(7) -0.0004(7) C10B 0.0285(9) 0.0273(9) 0.0230(8) 0.0013(7) 0.0005(7) -0.0061(7) C5B 0.0270(9) 0.0296(9) 0.0238(8) 0.0003(7) 0.0031(7) -0.0065(7) C17B 0.0280(9) 0.0284(9) 0.0250(8) -0.0062(7) 0.0011(7) -0.0022(8) C5A 0.0238(8) 0.0248(8) 0.0287(9) -0.0001(7) -0.0021(7) 0.0008(7) C9A 0.0273(9) 0.0274(9) 0.0302(9) 0.0038(8) -0.0003(7) -0.0015(7) C16A 0.0337(10) 0.0214(8) 0.0282(9) -0.0002(7) 0.0022(8) -0.0022(7) C19B 0.0388(11) 0.0217(8) 0.0251(9) -0.0004(7) 0.0028(8) 0.0012(8) C9B 0.0364(11) 0.0338(10) 0.0278(9) 0.0076(8) 0.0002(8) -0.0039(9) C19A 0.0309(9) 0.0240(9) 0.0289(9) 0.0024(7) 0.0030(8) -0.0022(7) C17A 0.0297(9) 0.0286(9) 0.0243(8) -0.0020(7) 0.0026(7) 0.0004(8) C8A 0.0308(10) 0.0374(11) 0.0285(9) 0.0073(8) -0.0018(8) 0.0007(8) C18A 0.0349(10) 0.0289(9) 0.0242(9) 0.0040(7) 0.0002(8) -0.0035(8) C6B 0.0330(10) 0.0379(11) 0.0265(9) -0.0016(8) 0.0073(8) -0.0052(9) C18B 0.0416(11) 0.0268(9) 0.0222(8) -0.0004(7) 0.0016(8) -0.0004(8) C8B 0.0395(11) 0.0420(12) 0.0263(10) 0.0084(9) -0.0003(8) -0.0087(10) C7B 0.0367(11) 0.0481(13) 0.0244(9) 0.0018(9) 0.0051(8) -0.0102(10) C7A 0.0331(10) 0.0394(11) 0.0309(10) 0.0007(9) -0.0077(8) -0.0007(9) C6A 0.0333(10) 0.0325(10) 0.0334(10) -0.0008(8) -0.0074(8) -0.0036(8) C22B 0.0407(11) 0.0409(11) 0.0255(9) -0.0023(9) 0.0061(9) -0.0021(9) C23A 0.0444(12) 0.0361(11) 0.0259(9) 0.0025(8) -0.0050(9) -0.0006(9) C23B 0.0469(13) 0.0439(12) 0.0270(10) 0.0038(9) 0.0010(9) -0.0041(10) C20B 0.0411(12) 0.0376(11) 0.0295(10) -0.0040(9) 0.0038(9) 0.0009(9) C24A 0.0593(15) 0.0469(13) 0.0285(10) 0.0097(10) 0.0044(10) 0.0102(12) C21B 0.0426(13) 0.0443(13) 0.0518(15) -0.0006(11) 0.0110(11) 0.0039(11) C21A 0.0598(17) 0.0633(17) 0.0358(12) -0.0015(12) 0.0029(12) -0.0212(14) C22A 0.075(2) 0.0403(14) 0.088(2) -0.0043(15) 0.0276(18) -0.0120(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O3A C12A 1.371(2) . ? O3A C13A 1.372(2) . ? O3B C13B 1.373(2) . ? O3B C12B 1.366(2) . ? O1B C2B 1.248(2) . ? O2A H2A 0.8200 . ? O2A C1A 1.365(2) . ? O1A C2A 1.251(2) . ? O2B H2B 0.8200 . ? O2B C1B 1.362(2) . ? N1B C17B 1.374(2) . ? N1B C22B 1.456(3) . ? N1B C20B 1.485(3) . ? N1A C17A 1.380(3) . ? N1A C23A 1.464(3) . ? N1A C21A 1.464(3) . ? C13B C14B 1.453(2) . ? C13B C1B 1.376(2) . ? C12A C3A 1.409(2) . ? C12A C11A 1.376(2) . ? C12B C3B 1.411(2) . ? C12B C11B 1.377(3) . ? C13A C14A 1.463(3) . ? C13A C1A 1.372(2) . ? C3B C2B 1.459(2) . ? C3B C4B 1.388(3) . ? C14A C15A 1.408(3) . ? C14A C19A 1.404(3) . ? C14B C15B 1.411(3) . ? C14B C19B 1.400(3) . ? C3A C2A 1.456(3) . ? C3A C4A 1.384(3) . ? C2B C1B 1.445(2) . ? C2A C1A 1.439(3) . ? C15A H15A 0.9300 . ? C15A C16A 1.383(3) . ? C15B H15B 0.9300 . ? C15B C16B 1.376(3) . ? C11A H11A 0.9300 . ? C11A C10A 1.410(3) . ? C4A H4A 0.9300 . ? C4A C5A 1.405(3) . ? C10A C5A 1.430(3) . ? C10A C9A 1.426(3) . ? C11B H11B 0.9300 . ? C11B C10B 1.407(3) . ? C4B H4B 0.9300 . ? C4B C5B 1.403(3) . ? C16B H16B 0.9300 . ? C16B C17B 1.410(3) . ? C10B C5B 1.434(3) . ? C10B C9B 1.429(3) . ? C5B C6B 1.426(3) . ? C17B C18B 1.417(3) . ? C5A C6A 1.430(3) . ? C9A H9A 0.9300 . ? C9A C8A 1.368(3) . ? C16A H16A 0.9300 . ? C16A C17A 1.414(3) . ? C19B H19B 0.9300 . ? C19B C18B 1.381(3) . ? C9B H9B 0.9300 . ? C9B C8B 1.373(3) . ? C19A H19A 0.9300 . ? C19A C18A 1.378(3) . ? C17A C18A 1.410(3) . ? C8A H8A 0.9300 . ? C8A C7A 1.410(3) . ? C18A H18A 0.9300 . ? C6B H6B 0.9300 . ? C6B C7B 1.368(3) . ? C18B H18B 0.9300 . ? C8B H8B 0.9300 . ? C8B C7B 1.413(3) . ? C7B H7B 0.9300 . ? C7A H7A 0.9300 . ? C7A C6A 1.364(3) . ? C6A H6A 0.9300 . ? C22B H22D 0.9700 . ? C22B H22E 0.9700 . ? C22B C23B 1.522(3) . ? C23A H23A 0.9700 . ? C23A H23B 0.9700 . ? C23A C24A 1.520(3) . ? C23B H23C 0.9600 . ? C23B H23D 0.9600 . ? C23B H23E 0.9600 . ? C20B H20A 0.9700 . ? C20B H20B 0.9700 . ? C20B C21B 1.523(3) . ? C24A H24A 0.9600 . ? C24A H24B 0.9600 . ? C24A H24C 0.9600 . ? C21B H21C 0.9600 . ? C21B H21D 0.9600 . ? C21B H21E 0.9600 . ? C21A H21A 0.9700 . ? C21A H21B 0.9700 . ? C21A C22A 1.465(4) . ? C22A H22A 0.9600 . ? C22A H22B 0.9600 . ? C22A H22C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C12A O3A C13A 121.20(14) . . ? C12B O3B C13B 121.59(14) . . ? C1A O2A H2A 109.5 . . ? C1B O2B H2B 109.5 . . ? C17B N1B C22B 121.28(18) . . ? C17B N1B C20B 121.53(18) . . ? C22B N1B C20B 117.00(17) . . ? C17A N1A C23A 120.06(17) . . ? C17A N1A C21A 123.10(18) . . ? C23A N1A C21A 115.70(18) . . ? O3B C13B C14B 111.04(15) . . ? O3B C13B C1B 120.06(15) . . ? C1B C13B C14B 128.89(16) . . ? O3A C12A C3A 121.41(16) . . ? O3A C12A C11A 116.73(16) . . ? C11A C12A C3A 121.85(17) . . ? O3B C12B C3B 121.16(16) . . ? O3B C12B C11B 116.77(16) . . ? C11B C12B C3B 122.07(17) . . ? O3A C13A C14A 111.38(15) . . ? C1A C13A O3A 120.11(16) . . ? C1A C13A C14A 128.51(16) . . ? C12B C3B C2B 119.19(16) . . ? C4B C3B C12B 118.65(17) . . ? C4B C3B C2B 122.12(17) . . ? C15A C14A C13A 120.72(16) . . ? C19A C14A C13A 122.93(17) . . ? C19A C14A C15A 116.35(17) . . ? C15B C14B C13B 119.93(16) . . ? C19B C14B C13B 123.29(17) . . ? C19B C14B C15B 116.78(16) . . ? C12A C3A C2A 118.77(17) . . ? C4A C3A C12A 119.07(17) . . ? C4A C3A C2A 122.13(17) . . ? O1B C2B C3B 122.69(16) . . ? O1B C2B C1B 121.44(17) . . ? C1B C2B C3B 115.87(16) . . ? O2B C1B C13B 119.87(16) . . ? O2B C1B C2B 118.07(16) . . ? C13B C1B C2B 122.05(16) . . ? O1A C2A C3A 123.04(18) . . ? O1A C2A C1A 120.70(17) . . ? C1A C2A C3A 116.24(16) . . ? C14A C15A H15A 119.0 . . ? C16A C15A C14A 122.05(17) . . ? C16A C15A H15A 119.0 . . ? O2A C1A C13A 120.43(17) . . ? O2A C1A C2A 117.41(16) . . ? C13A C1A C2A 122.15(16) . . ? C14B C15B H15B 119.0 . . ? C16B C15B C14B 122.09(17) . . ? C16B C15B H15B 119.0 . . ? C12A C11A H11A 120.3 . . ? C12A C11A C10A 119.44(17) . . ? C10A C11A H11A 120.3 . . ? C3A C4A H4A 119.5 . . ? C3A C4A C5A 120.99(17) . . ? C5A C4A H4A 119.5 . . ? C11A C10A C5A 119.58(17) . . ? C11A C10A C9A 121.88(17) . . ? C9A C10A C5A 118.53(17) . . ? C12B C11B H11B 120.2 . . ? C12B C11B C10B 119.62(18) . . ? C10B C11B H11B 120.2 . . ? C3B C4B H4B 119.4 . . ? C3B C4B C5B 121.12(18) . . ? C5B C4B H4B 119.4 . . ? C15B C16B H16B 119.5 . . ? C15B C16B C17B 121.07(18) . . ? C17B C16B H16B 119.5 . . ? C11B C10B C5B 119.30(17) . . ? C11B C10B C9B 121.55(19) . . ? C9B C10B C5B 119.15(18) . . ? C4B C5B C10B 119.23(17) . . ? C4B C5B C6B 122.25(19) . . ? C6B C5B C10B 118.52(18) . . ? N1B C17B C16B 121.57(18) . . ? N1B C17B C18B 121.46(18) . . ? C16B C17B C18B 116.97(17) . . ? C4A C5A C10A 119.04(17) . . ? C4A C5A C6A 122.19(18) . . ? C10A C5A C6A 118.77(18) . . ? C10A C9A H9A 119.6 . . ? C8A C9A C10A 120.72(19) . . ? C8A C9A H9A 119.6 . . ? C15A C16A H16A 119.3 . . ? C15A C16A C17A 121.46(18) . . ? C17A C16A H16A 119.3 . . ? C14B C19B H19B 119.1 . . ? C18B C19B C14B 121.75(18) . . ? C18B C19B H19B 119.1 . . ? C10B C9B H9B 119.9 . . ? C8B C9B C10B 120.3(2) . . ? C8B C9B H9B 119.9 . . ? C14A C19A H19A 119.0 . . ? C18A C19A C14A 121.91(18) . . ? C18A C19A H19A 119.0 . . ? N1A C17A C16A 122.83(18) . . ? N1A C17A C18A 121.02(18) . . ? C18A C17A C16A 116.15(17) . . ? C9A C8A H8A 119.6 . . ? C9A C8A C7A 120.85(19) . . ? C7A C8A H8A 119.6 . . ? C19A C18A C17A 122.05(18) . . ? C19A C18A H18A 119.0 . . ? C17A C18A H18A 119.0 . . ? C5B C6B H6B 119.7 . . ? C7B C6B C5B 120.7(2) . . ? C7B C6B H6B 119.7 . . ? C17B C18B H18B 119.3 . . ? C19B C18B C17B 121.32(18) . . ? C19B C18B H18B 119.3 . . ? C9B C8B H8B 119.8 . . ? C9B C8B C7B 120.5(2) . . ? C7B C8B H8B 119.8 . . ? C6B C7B C8B 120.9(2) . . ? C6B C7B H7B 119.5 . . ? C8B C7B H7B 119.5 . . ? C8A C7A H7A 119.9 . . ? C6A C7A C8A 120.28(19) . . ? C6A C7A H7A 119.9 . . ? C5A C6A H6A 119.6 . . ? C7A C6A C5A 120.84(19) . . ? C7A C6A H6A 119.6 . . ? N1B C22B H22D 108.9 . . ? N1B C22B H22E 108.9 . . ? N1B C22B C23B 113.25(18) . . ? H22D C22B H22E 107.7 . . ? C23B C22B H22D 108.9 . . ? C23B C22B H22E 108.9 . . ? N1A C23A H23A 108.8 . . ? N1A C23A H23B 108.8 . . ? N1A C23A C24A 113.59(19) . . ? H23A C23A H23B 107.7 . . ? C24A C23A H23A 108.8 . . ? C24A C23A H23B 108.8 . . ? C22B C23B H23C 109.5 . . ? C22B C23B H23D 109.5 . . ? C22B C23B H23E 109.5 . . ? H23C C23B H23D 109.5 . . ? H23C C23B H23E 109.5 . . ? H23D C23B H23E 109.5 . . ? N1B C20B H20A 109.0 . . ? N1B C20B H20B 109.0 . . ? N1B C20B C21B 112.8(2) . . ? H20A C20B H20B 107.8 . . ? C21B C20B H20A 109.0 . . ? C21B C20B H20B 109.0 . . ? C23A C24A H24A 109.5 . . ? C23A C24A H24B 109.5 . . ? C23A C24A H24C 109.5 . . ? H24A C24A H24B 109.5 . . ? H24A C24A H24C 109.5 . . ? H24B C24A H24C 109.5 . . ? C20B C21B H21C 109.5 . . ? C20B C21B H21D 109.5 . . ? C20B C21B H21E 109.5 . . ? H21C C21B H21D 109.5 . . ? H21C C21B H21E 109.5 . . ? H21D C21B H21E 109.5 . . ? N1A C21A H21A 108.6 . . ? N1A C21A H21B 108.6 . . ? N1A C21A C22A 114.6(2) . . ? H21A C21A H21B 107.6 . . ? C22A C21A H21A 108.6 . . ? C22A C21A H21B 108.6 . . ? C21A C22A H22A 109.5 . . ? C21A C22A H22B 109.5 . . ? C21A C22A H22C 109.5 . . ? H22A C22A H22B 109.5 . . ? H22A C22A H22C 109.5 . . ? H22B C22A H22C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3A C12A C3A C2A 3.1(3) . . . . ? O3A C12A C3A C4A -179.10(17) . . . . ? O3A C12A C11A C10A -179.41(16) . . . . ? O3A C13A C14A C15A 3.3(2) . . . . ? O3A C13A C14A C19A -176.09(16) . . . . ? O3A C13A C1A O2A -175.88(16) . . . . ? O3A C13A C1A C2A 2.9(3) . . . . ? O3B C13B C14B C15B 9.3(2) . . . . ? O3B C13B C14B C19B -170.19(17) . . . . ? O3B C13B C1B O2B -176.12(16) . . . . ? O3B C13B C1B C2B 3.1(3) . . . . ? O3B C12B C3B C2B 1.6(3) . . . . ? O3B C12B C3B C4B 179.27(16) . . . . ? O3B C12B C11B C10B -178.47(17) . . . . ? O1B C2B C1B O2B -1.4(3) . . . . ? O1B C2B C1B C13B 179.42(18) . . . . ? O1A C2A C1A O2A -2.1(3) . . . . ? O1A C2A C1A C13A 179.08(18) . . . . ? N1B C17B C18B C19B -178.8(2) . . . . ? N1A C17A C18A C19A 177.9(2) . . . . ? C13B O3B C12B C3B 0.3(3) . . . . ? C13B O3B C12B C11B -179.82(16) . . . . ? C13B C14B C15B C16B -179.07(17) . . . . ? C13B C14B C19B C18B 178.46(19) . . . . ? C12A O3A C13A C14A -179.88(15) . . . . ? C12A O3A C13A C1A -0.2(2) . . . . ? C12A C3A C2A O1A 177.92(18) . . . . ? C12A C3A C2A C1A -0.5(3) . . . . ? C12A C3A C4A C5A -1.3(3) . . . . ? C12A C11A C10A C5A -1.6(3) . . . . ? C12A C11A C10A C9A 179.19(17) . . . . ? C12B O3B C13B C14B 177.99(15) . . . . ? C12B O3B C13B C1B -2.7(2) . . . . ? C12B C3B C2B O1B 178.26(18) . . . . ? C12B C3B C2B C1B -1.2(3) . . . . ? C12B C3B C4B C5B -0.6(3) . . . . ? C12B C11B C10B C5B -1.1(3) . . . . ? C12B C11B C10B C9B 178.98(18) . . . . ? C13A O3A C12A C3A -2.8(2) . . . . ? C13A O3A C12A C11A 177.91(15) . . . . ? C13A C14A C15A C16A -179.60(18) . . . . ? C13A C14A C19A C18A 178.25(18) . . . . ? C3B C12B C11B C10B 1.4(3) . . . . ? C3B C2B C1B O2B 178.07(16) . . . . ? C3B C2B C1B C13B -1.1(3) . . . . ? C3B C4B C5B C10B 0.8(3) . . . . ? C3B C4B C5B C6B -178.56(18) . . . . ? C14A C13A C1A O2A 3.7(3) . . . . ? C14A C13A C1A C2A -177.49(17) . . . . ? C14A C15A C16A C17A 0.5(3) . . . . ? C14A C19A C18A C17A 2.2(3) . . . . ? C14B C13B C1B O2B 3.1(3) . . . . ? C14B C13B C1B C2B -177.72(18) . . . . ? C14B C15B C16B C17B 0.8(3) . . . . ? C14B C19B C18B C17B 0.4(3) . . . . ? C3A C12A C11A C10A 1.3(3) . . . . ? C3A C2A C1A O2A 176.33(16) . . . . ? C3A C2A C1A C13A -2.5(3) . . . . ? C3A C4A C5A C10A 1.0(3) . . . . ? C3A C4A C5A C6A -178.82(19) . . . . ? C2B C3B C4B C5B 177.05(18) . . . . ? C1B C13B C14B C15B -169.90(18) . . . . ? C1B C13B C14B C19B 10.6(3) . . . . ? C2A C3A C4A C5A 176.46(18) . . . . ? C15A C14A C19A C18A -1.2(3) . . . . ? C15A C16A C17A N1A -179.25(19) . . . . ? C15A C16A C17A C18A 0.4(3) . . . . ? C1A C13A C14A C15A -176.31(18) . . . . ? C1A C13A C14A C19A 4.3(3) . . . . ? C15B C14B C19B C18B -1.1(3) . . . . ? C15B C16B C17B N1B 178.17(19) . . . . ? C15B C16B C17B C18B -1.5(3) . . . . ? C11A C12A C3A C2A -177.69(17) . . . . ? C11A C12A C3A C4A 0.1(3) . . . . ? C11A C10A C5A C4A 0.5(3) . . . . ? C11A C10A C5A C6A -179.71(18) . . . . ? C11A C10A C9A C8A 179.91(19) . . . . ? C4A C3A C2A O1A 0.2(3) . . . . ? C4A C3A C2A C1A -178.22(18) . . . . ? C4A C5A C6A C7A 179.8(2) . . . . ? C10A C5A C6A C7A 0.0(3) . . . . ? C10A C9A C8A C7A -0.5(3) . . . . ? C11B C12B C3B C2B -178.25(17) . . . . ? C11B C12B C3B C4B -0.6(3) . . . . ? C11B C10B C5B C4B 0.0(3) . . . . ? C11B C10B C5B C6B 179.39(18) . . . . ? C11B C10B C9B C8B -179.7(2) . . . . ? C4B C3B C2B O1B 0.7(3) . . . . ? C4B C3B C2B C1B -178.75(17) . . . . ? C4B C5B C6B C7B 179.7(2) . . . . ? C16B C17B C18B C19B 0.9(3) . . . . ? C10B C5B C6B C7B 0.3(3) . . . . ? C10B C9B C8B C7B 0.3(3) . . . . ? C5B C10B C9B C8B 0.4(3) . . . . ? C5B C6B C7B C8B 0.4(3) . . . . ? C17B N1B C22B C23B 85.3(3) . . . . ? C17B N1B C20B C21B 94.5(2) . . . . ? C5A C10A C9A C8A 0.7(3) . . . . ? C9A C10A C5A C4A 179.73(18) . . . . ? C9A C10A C5A C6A -0.5(3) . . . . ? C9A C8A C7A C6A 0.0(3) . . . . ? C16A C17A C18A C19A -1.7(3) . . . . ? C19B C14B C15B C16B 0.5(3) . . . . ? C9B C10B C5B C4B 179.93(18) . . . . ? C9B C10B C5B C6B -0.6(3) . . . . ? C9B C8B C7B C6B -0.7(3) . . . . ? C19A C14A C15A C16A -0.2(3) . . . . ? C17A N1A C23A C24A 75.2(3) . . . . ? C17A N1A C21A C22A -123.3(3) . . . . ? C8A C7A C6A C5A 0.2(3) . . . . ? C22B N1B C17B C16B 172.23(19) . . . . ? C22B N1B C17B C18B -8.1(3) . . . . ? C22B N1B C20B C21B -90.5(2) . . . . ? C23A N1A C17A C16A -174.19(19) . . . . ? C23A N1A C17A C18A 6.2(3) . . . . ? C23A N1A C21A C22A 68.9(3) . . . . ? C20B N1B C17B C16B -13.0(3) . . . . ? C20B N1B C17B C18B 166.7(2) . . . . ? C20B N1B C22B C23B -89.8(2) . . . . ? C21A N1A C17A C16A 18.5(3) . . . . ? C21A N1A C17A C18A -161.1(2) . . . . ? C21A N1A C23A C24A -116.6(2) . . . . ? _shelx_res_file ; TITL r1_a.res in Pbca r1.res created by SHELXL-2018/3 at 10:47:27 on 21-Jul-2021 REM Old TITL R1 in Pbca #61 REM SHELXT solution in Pbca: R1 0.143, Rweak 0.005, Alpha 0.017 REM 1.117 for 748 systematic absences, Orientation as input REM Formula found by SHELXT: C47 N O6 CELL 0.71073 15.8887 14.1192 32.2636 90 90 90 ZERR 8 0.0003 0.0002 0.0005 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 368 336 16 48 L.S. 4 PLAN 5 SIZE 0.303 0.32 0.442 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta OMIT 1 1 1 REM REM REM WGHT 0.086100 6.931500 FVAR 0.21977 O3A 4 0.354954 0.059232 0.428684 11.00000 0.02756 0.01850 = 0.02255 0.00196 0.00043 -0.00060 O3B 4 0.358538 0.710109 0.386734 11.00000 0.02963 0.01969 = 0.02027 -0.00080 0.00244 -0.00126 O1B 4 0.462748 0.449695 0.367764 11.00000 0.03952 0.01986 = 0.03023 -0.00104 0.00756 0.00239 O2A 4 0.387282 0.278849 0.372619 11.00000 0.04786 0.01758 = 0.02545 0.00211 0.00127 -0.00345 AFIX 147 H2A 2 0.416285 0.324450 0.379230 11.00000 -1.50000 AFIX 0 O1A 4 0.462957 0.318208 0.445882 11.00000 0.04058 0.01975 = 0.03667 0.00090 -0.00359 -0.00396 O2B 4 0.391320 0.491014 0.442917 11.00000 0.04789 0.01977 = 0.02669 0.00213 0.00873 0.00431 AFIX 147 H2B 2 0.418630 0.444324 0.436019 11.00000 -1.50000 AFIX 0 N1B 3 0.217621 0.809143 0.563097 11.00000 0.04096 0.03549 = 0.02413 -0.00533 0.00279 0.00468 N1A 3 0.201735 -0.027935 0.251620 11.00000 0.04664 0.03622 = 0.02358 0.00046 -0.00266 -0.01021 C13B 1 0.360432 0.645453 0.418496 11.00000 0.02322 0.01905 = 0.02070 0.00012 0.00031 -0.00361 C12A 1 0.388741 0.080130 0.466711 11.00000 0.02164 0.02011 = 0.02407 -0.00075 0.00067 0.00260 C12B 1 0.392521 0.690335 0.348827 11.00000 0.02554 0.02206 = 0.01996 -0.00138 0.00048 -0.00290 C13A 1 0.355897 0.124134 0.397024 11.00000 0.02288 0.01826 = 0.02361 0.00129 0.00370 0.00342 C3B 1 0.430737 0.602071 0.340681 11.00000 0.02402 0.02078 = 0.02342 -0.00101 0.00087 -0.00309 C14A 1 0.316289 0.086133 0.359606 11.00000 0.02334 0.02117 = 0.02395 -0.00006 0.00362 0.00328 C14B 1 0.323037 0.684420 0.455894 11.00000 0.02551 0.02061 = 0.02227 -0.00336 0.00139 -0.00346 C3A 1 0.429008 0.167329 0.474296 11.00000 0.02445 0.01949 = 0.02731 -0.00009 -0.00058 0.00196 C2B 1 0.431874 0.530024 0.373088 11.00000 0.02715 0.01897 = 0.02424 -0.00238 0.00286 -0.00239 C1B 1 0.394060 0.556834 0.412080 11.00000 0.02867 0.02006 = 0.02231 0.00033 0.00302 -0.00260 C2A 1 0.430730 0.238026 0.441455 11.00000 0.02828 0.01837 = 0.02944 0.00012 0.00206 0.00092 C15A 1 0.279216 -0.004450 0.359719 11.00000 0.03012 0.01929 = 0.02424 0.00126 0.00331 0.00238 AFIX 43 H15A 2 0.279930 -0.039792 0.384040 11.00000 -1.20000 AFIX 0 C1A 1 0.390807 0.211919 0.403083 11.00000 0.02946 0.01769 = 0.02395 0.00068 0.00345 0.00305 C15B 1 0.279994 0.771794 0.454309 11.00000 0.02524 0.02403 = 0.02357 -0.00212 -0.00114 -0.00189 AFIX 43 H15B 2 0.275433 0.803038 0.429032 11.00000 -1.20000 AFIX 0 C11A 1 0.382179 0.011428 0.496804 11.00000 0.02383 0.01999 = 0.02650 0.00119 0.00130 -0.00033 AFIX 43 H11A 2 0.356318 -0.046097 0.490890 11.00000 -1.20000 AFIX 0 C4A 1 0.463075 0.184298 0.513072 11.00000 0.02934 0.02077 = 0.03120 -0.00079 -0.00379 -0.00077 AFIX 43 H4A 2 0.490732 0.241193 0.518116 11.00000 -1.20000 AFIX 0 C10A 1 0.414986 0.028997 0.536661 11.00000 0.02071 0.02391 = 0.02756 0.00069 0.00115 0.00157 C11B 1 0.387365 0.760364 0.319252 11.00000 0.02942 0.02226 = 0.02660 0.00096 0.00015 -0.00151 AFIX 43 H11B 2 0.362885 0.818364 0.325678 11.00000 -1.20000 AFIX 0 C4B 1 0.463368 0.585509 0.301441 11.00000 0.02675 0.02530 = 0.02532 -0.00163 0.00423 -0.00306 AFIX 43 H4B 2 0.489144 0.527809 0.295771 11.00000 -1.20000 AFIX 0 C16B 1 0.244556 0.812225 0.488983 11.00000 0.02581 0.02519 = 0.02820 -0.00539 -0.00090 -0.00037 AFIX 43 H16B 2 0.216093 0.869518 0.486580 11.00000 -1.20000 AFIX 0 C10B 1 0.419342 0.743696 0.279245 11.00000 0.02853 0.02732 = 0.02304 0.00130 0.00051 -0.00606 C5B 1 0.458128 0.654341 0.270183 11.00000 0.02701 0.02963 = 0.02383 0.00032 0.00314 -0.00654 C17B 1 0.250709 0.768182 0.528089 11.00000 0.02797 0.02838 = 0.02503 -0.00621 0.00111 -0.00220 C5A 1 0.456502 0.116839 0.544941 11.00000 0.02375 0.02477 = 0.02874 -0.00011 -0.00209 0.00084 C9A 1 0.409037 -0.039048 0.569179 11.00000 0.02725 0.02740 = 0.03019 0.00377 -0.00025 -0.00146 AFIX 43 H9A 2 0.382796 -0.096830 0.564231 11.00000 -1.20000 AFIX 0 C16A 1 0.241766 -0.042507 0.324776 11.00000 0.03369 0.02138 = 0.02819 -0.00025 0.00223 -0.00220 AFIX 43 H16A 2 0.217597 -0.102401 0.326258 11.00000 -1.20000 AFIX 0 C19B 1 0.327610 0.639816 0.494592 11.00000 0.03879 0.02170 = 0.02505 -0.00044 0.00283 0.00117 AFIX 43 H19B 2 0.354665 0.581605 0.496701 11.00000 -1.20000 AFIX 0 C9B 1 0.414144 0.813746 0.247393 11.00000 0.03639 0.03381 = 0.02784 0.00759 0.00022 -0.00388 AFIX 43 H9B 2 0.389405 0.872058 0.252983 11.00000 -1.20000 AFIX 0 C19A 1 0.313431 0.135951 0.321974 11.00000 0.03090 0.02405 = 0.02887 0.00241 0.00297 -0.00219 AFIX 43 H19A 2 0.336290 0.196521 0.320728 11.00000 -1.20000 AFIX 0 C17A 1 0.239419 0.007643 0.286856 11.00000 0.02970 0.02860 = 0.02429 -0.00203 0.00263 0.00036 C8A 1 0.441508 -0.020268 0.607578 11.00000 0.03082 0.03739 = 0.02854 0.00728 -0.00184 0.00068 AFIX 43 H8A 2 0.436695 -0.065277 0.628490 11.00000 -1.20000 AFIX 0 C18A 1 0.277741 0.097709 0.286832 11.00000 0.03492 0.02891 = 0.02423 0.00402 0.00019 -0.00354 AFIX 43 H18A 2 0.278967 0.132390 0.262334 11.00000 -1.20000 AFIX 0 C6B 1 0.489435 0.638352 0.229365 11.00000 0.03302 0.03791 = 0.02649 -0.00159 0.00728 -0.00525 AFIX 43 H6B 2 0.514556 0.580713 0.222915 11.00000 -1.20000 AFIX 0 C18B 1 0.293027 0.679950 0.529697 11.00000 0.04161 0.02683 = 0.02223 -0.00044 0.00158 -0.00040 AFIX 43 H18B 2 0.297605 0.648430 0.554907 11.00000 -1.20000 AFIX 0 C8B 1 0.445505 0.795361 0.208575 11.00000 0.03950 0.04203 = 0.02630 0.00840 -0.00032 -0.00868 AFIX 43 H8B 2 0.442113 0.841439 0.188045 11.00000 -1.20000 AFIX 0 C7B 1 0.482896 0.706938 0.199593 11.00000 0.03667 0.04805 = 0.02439 0.00182 0.00508 -0.01017 AFIX 43 H7B 2 0.503344 0.695195 0.173078 11.00000 -1.20000 AFIX 0 C7A 1 0.482180 0.066446 0.615861 11.00000 0.03315 0.03945 = 0.03092 0.00068 -0.00768 -0.00068 AFIX 43 H7A 2 0.503947 0.078185 0.642121 11.00000 -1.20000 AFIX 0 C6A 1 0.489739 0.133202 0.585518 11.00000 0.03333 0.03251 = 0.03343 -0.00084 -0.00735 -0.00362 AFIX 43 H6A 2 0.516846 0.190072 0.591289 11.00000 -1.20000 AFIX 0 C22B 1 0.214786 0.758308 0.602334 11.00000 0.04071 0.04088 = 0.02547 -0.00226 0.00612 -0.00212 AFIX 23 H22D 2 0.203489 0.691951 0.596886 11.00000 -1.20000 H22E 2 0.168646 0.782859 0.618832 11.00000 -1.20000 AFIX 0 C23A 1 0.208416 0.023487 0.212365 11.00000 0.04440 0.03605 = 0.02590 0.00247 -0.00505 -0.00056 AFIX 23 H23A 2 0.196653 0.089940 0.217327 11.00000 -1.20000 H23B 2 0.165940 -0.000249 0.193433 11.00000 -1.20000 AFIX 0 C23B 1 0.295879 0.766364 0.627169 11.00000 0.04687 0.04389 = 0.02695 0.00382 0.00096 -0.00409 AFIX 137 H23C 2 0.341661 0.740646 0.611345 11.00000 -1.50000 H23D 2 0.290229 0.731752 0.652628 11.00000 -1.50000 H23E 2 0.306914 0.831776 0.633201 11.00000 -1.50000 AFIX 0 C20B 1 0.189842 0.909579 0.563497 11.00000 0.04108 0.03760 = 0.02950 -0.00395 0.00377 0.00092 AFIX 23 H20A 2 0.221502 0.944569 0.542849 11.00000 -1.20000 H20B 2 0.202345 0.936872 0.590391 11.00000 -1.20000 AFIX 0 C24A 1 0.294283 0.014742 0.191919 11.00000 0.05930 0.04689 = 0.02854 0.00966 0.00444 0.01023 AFIX 137 H24A 2 0.294655 0.050205 0.166533 11.00000 -1.50000 H24B 2 0.305739 -0.050673 0.186084 11.00000 -1.50000 H24C 2 0.336672 0.039171 0.210230 11.00000 -1.50000 AFIX 0 C21B 1 0.096167 0.920666 0.554686 11.00000 0.04264 0.04425 = 0.05181 -0.00056 0.01098 0.00385 AFIX 137 H21C 2 0.084831 0.902988 0.526502 11.00000 -1.50000 H21D 2 0.079949 0.985432 0.558960 11.00000 -1.50000 H21E 2 0.064686 0.880566 0.573045 11.00000 -1.50000 AFIX 0 C21A 1 0.140457 -0.105370 0.252413 11.00000 0.05976 0.06328 = 0.03577 -0.00146 0.00292 -0.02117 AFIX 23 H21A 2 0.086539 -0.081205 0.243087 11.00000 -1.20000 H21B 2 0.133620 -0.126367 0.280841 11.00000 -1.20000 AFIX 0 C22A 1 0.163061 -0.187215 0.226828 11.00000 0.07497 0.04029 = 0.08804 -0.00427 0.02759 -0.01198 AFIX 137 H22A 2 0.166228 -0.168261 0.198295 11.00000 -1.50000 H22B 2 0.121081 -0.235615 0.229883 11.00000 -1.50000 H22C 2 0.216687 -0.211406 0.235537 11.00000 -1.50000 AFIX 0 HKLF 4 REM r1_a.res in Pbca REM wR2 = 0.1952, GooF = S = 1.026, Restrained GooF = 1.026 for all data REM R1 = 0.0651 for 7456 Fo > 4sig(Fo) and 0.1014 for all 11029 data REM 493 parameters refined using 0 restraints END WGHT 0.0862 6.9312 REM Highest difference peak 0.867, deepest hole -0.407, 1-sigma level 0.066 Q1 1 0.1860 -0.1417 0.2574 11.00000 0.05 0.87 Q2 1 0.1359 0.8600 0.5621 11.00000 0.05 0.62 Q3 1 0.1679 0.9588 0.5780 11.00000 0.05 0.48 Q4 1 0.1161 -0.1563 0.2224 11.00000 0.05 0.43 Q5 1 0.1054 -0.1568 0.2553 11.00000 0.05 0.37 ; _shelx_res_checksum 90999 _shelx_hkl_file ; 0 0 -3 0.10 0.19 0 0 -3 0.23 0.20 0 0 3 0.19 0.19 0 0 3 0.90 0.28 0 0 3 0.47 0.31 0 0 4 704.72 3.19 0 0 4 695.49 2.95 0 0 5 0.48 0.51 0 0 5 0.88 0.60 0 0 -5 0.67 0.56 0 0 -5 0.76 0.42 0 0 5 0.53 0.47 0 0 5 1.30 0.61 0 0 5 0.75 0.55 0 0 -5 1.05 0.63 0 0 -5 0.37 0.53 0 0 6 3555.54 95.27 0 0 6 3716.91 95.35 0 0 6 3670.88 95.34 0 0 -6 3765.27 95.27 0 0 -6 3729.37 95.26 0 0 -6 3484.66 95.15 0 0 -6 3764.66 95.34 0 0 6 3767.27 95.30 0 0 6 3728.06 95.24 0 0 -6 3799.52 95.33 0 0 -7 0.33 0.58 0 0 7 0.47 0.76 0 0 -7 2.09 0.89 0 0 7 1.28 0.81 0 0 7 1.84 0.94 0 0 -7 1.84 0.82 0 0 -7 1.87 0.98 0 0 -7 1.24 0.80 0 0 7 1.36 0.72 0 0 7 0.83 0.88 0 0 -8 11.61 0.99 0 0 -8 9.00 0.74 0 0 -8 9.86 0.96 0 0 8 10.41 0.55 0 0 8 9.56 1.15 0 0 8 11.89 1.07 0 0 8 10.84 1.05 0 0 8 9.93 1.14 0 0 8 9.50 0.97 0 0 8 10.95 0.94 0 0 -8 11.08 1.08 0 0 -8 11.29 0.55 0 0 -9 1.38 0.93 0 0 9 0.41 0.40 0 0 9 0.04 0.81 0 0 -9 0.62 0.38 0 0 9 1.06 0.80 0 0 -9 0.06 0.58 0 0 -9 -0.15 0.81 0 0 -9 0.57 0.90 0 0 9 -0.44 1.03 0 0 9 0.17 0.84 0 0 9 -0.27 0.92 0 0 9 -0.15 0.96 0 0 -9 0.37 0.38 0 0 10 225.33 6.62 0 0 10 245.21 6.46 0 0 -10 228.87 6.49 0 0 10 234.78 6.53 0 0 -10 236.19 6.47 0 0 10 229.67 6.52 0 0 -10 227.17 6.07 0 0 -10 226.51 6.28 0 0 10 221.33 6.05 0 0 10 221.15 6.09 0 0 10 243.64 6.69 0 0 10 231.47 6.57 0 0 -10 235.22 6.64 0 0 11 1.23 0.45 0 0 11 2.22 1.14 0 0 11 1.58 0.44 0 0 11 1.00 0.96 0 0 11 1.50 0.85 0 0 11 1.24 1.02 0 0 -11 1.47 0.68 0 0 11 2.54 1.25 0 0 -11 1.55 1.02 0 0 -11 0.49 0.43 0 0 -11 0.51 0.88 0 0 -11 1.41 1.09 0 0 11 1.14 1.00 0 0 12 1984.60 45.23 0 0 -12 2046.75 45.27 0 0 12 2034.79 45.88 0 0 -12 2096.58 45.56 0 0 12 2101.54 45.91 0 0 12 2100.40 45.75 0 0 -12 2105.06 45.79 0 0 -12 2133.16 46.02 0 0 -12 2110.00 45.86 0 0 12 2103.36 46.08 0 0 12 2118.44 46.04 0 0 13 8.52 1.51 0 0 13 6.14 1.32 0 0 13 8.11 1.24 0 0 -13 2.10 0.69 0 0 13 4.43 1.04 0 0 -13 8.10 1.26 0 0 -13 4.94 0.84 0 0 -13 5.42 1.04 0 0 13 7.11 1.43 0 0 -13 9.94 1.43 0 0 13 5.07 1.20 0 0 13 6.66 0.56 0 0 14 40.70 1.99 0 0 14 43.01 2.01 0 0 14 42.08 1.27 0 0 14 44.65 1.88 0 0 -14 43.33 2.01 0 0 -14 43.04 2.13 0 0 14 43.17 2.25 0 0 -14 43.88 1.87 0 0 14 44.48 2.27 0 0 -14 44.91 1.62 0 0 14 42.53 2.21 0 0 15 -0.35 0.97 0 0 -15 0.16 1.27 0 0 15 1.00 1.09 0 0 15 0.46 0.43 0 0 -15 0.25 0.90 0 0 -15 -0.97 1.28 0 0 15 2.27 1.35 0 0 -15 0.97 0.72 0 0 -15 0.42 0.68 0 0 15 1.95 1.36 0 0 15 0.51 1.13 0 0 15 -0.95 1.36 0 0 16 1067.35 26.38 0 0 -16 1091.14 26.16 0 0 16 1083.68 26.40 0 0 -16 1057.36 26.00 0 0 16 1061.10 25.96 0 0 16 997.99 25.31 0 0 16 1063.10 26.42 0 0 -16 1083.68 26.35 0 0 16 1088.59 26.20 0 0 -16 1067.80 25.74 0 0 17 4.12 1.12 0 0 17 4.88 1.50 0 0 17 4.46 1.67 0 0 -17 3.51 1.08 0 0 -17 4.99 1.36 0 0 17 5.49 1.64 0 0 -17 5.28 1.53 0 0 17 5.78 1.57 0 0 -17 5.01 0.87 0 0 18 153.61 4.83 0 0 18 156.30 5.35 0 0 -18 150.59 5.26 0 0 -18 145.81 5.01 0 0 -18 154.03 4.85 0 0 18 157.71 5.32 0 0 18 153.12 5.32 0 0 18 149.73 5.06 0 0 19 1.39 1.30 0 0 19 2.50 1.63 0 0 -19 0.27 1.27 0 0 -19 0.11 1.38 0 0 19 0.22 1.01 0 0 19 0.92 1.40 0 0 -19 0.08 0.98 0 0 19 1.23 1.49 0 0 -20 17.56 1.85 0 0 20 15.89 1.87 0 0 20 13.39 1.86 0 0 20 19.86 2.03 0 0 -20 15.92 1.68 0 0 20 14.04 1.64 0 0 -21 -0.30 1.30 0 0 21 2.56 1.56 0 0 21 0.25 1.62 0 0 -21 1.07 1.44 0 0 21 0.36 1.57 0 0 21 0.72 1.31 0 0 22 5.35 1.81 0 0 22 4.67 1.56 0 0 -22 4.63 1.58 0 0 22 5.66 1.78 0 0 22 8.76 1.85 0 0 -22 6.57 1.52 0 0 -23 1.75 1.43 0 0 23 -1.11 1.71 0 0 23 0.14 1.71 0 0 23 1.02 1.52 0 0 23 1.47 1.79 0 0 -23 1.44 1.61 0 0 24 41.29 2.98 0 0 -24 39.71 2.53 0 0 24 42.45 2.97 0 0 24 37.93 2.62 0 0 24 43.39 2.97 0 0 -24 44.43 2.90 0 0 25 3.19 2.12 0 0 25 2.73 1.81 0 0 -25 2.15 1.72 0 0 25 -1.02 1.98 0 0 25 3.42 2.09 0 0 26 217.22 7.76 0 0 26 221.70 7.75 0 0 -26 225.11 7.35 0 0 26 225.64 7.78 0 0 26 219.84 7.36 0 0 -27 -0.91 2.05 0 0 27 4.57 2.06 0 0 27 4.23 2.38 0 0 27 6.37 2.57 0 0 27 -0.50 2.60 0 0 28 139.43 5.55 0 0 28 140.11 5.95 0 0 28 148.75 6.05 0 0 28 148.29 6.11 0 0 29 0.18 2.32 0 0 29 -5.34 2.91 0 0 29 -1.79 2.59 0 0 29 -1.74 2.14 0 0 -29 5.37 2.38 0 0 -30 4.46 2.44 0 0 30 0.19 2.53 0 0 30 1.90 2.40 0 0 31 3.75 2.49 0 0 31 0.58 2.41 0 0 31 -2.77 2.71 0 0 -31 1.16 2.39 0 0 32 120.38 5.56 0 0 32 118.16 5.53 0 0 32 112.21 5.51 0 0 -32 128.75 5.56 0 0 33 1.18 2.37 0 0 -33 2.27 2.47 0 0 33 3.10 2.61 0 0 33 -1.06 2.38 0 0 34 0.44 2.52 0 0 -34 -1.92 2.58 0 0 34 1.43 2.57 0 0 34 -0.21 2.54 0 0 35 2.25 2.55 0 0 35 -2.21 2.60 0 0 35 0.84 2.52 0 0 -35 -1.98 2.43 0 0 36 12.98 3.05 0 0 -36 16.34 3.00 0 0 36 14.32 3.03 0 0 36 15.09 3.03 0 0 37 -4.30 2.80 0 0 -37 0.93 2.64 0 0 37 2.22 2.73 0 0 37 1.87 2.84 0 0 38 0.46 2.86 0 0 38 1.93 2.80 0 0 -38 1.44 2.61 0 0 -39 -2.47 2.82 0 0 39 -3.75 2.90 0 0 39 0.74 2.95 0 0 40 9.83 3.28 0 0 -40 11.13 3.13 0 0 40 9.89 3.35 0 0 -41 2.33 3.03 0 0 41 1.47 3.16 0 0 41 -0.52 3.15 0 0 42 102.16 5.94 0 0 42 111.88 6.08 0 0 -42 105.38 5.94 0 0 -43 1.09 3.26 0 0 43 -1.28 3.26 0 0 43 7.60 3.46 0 0 -44 1.66 3.18 0 0 44 3.90 3.38 0 0 44 -1.66 3.32 0 0 45 2.91 3.37 0 0 45 -0.56 3.27 0 0 -45 -5.92 3.28 0 0 46 4.57 3.46 1 0 2 2464.14 53.55 1 0 2 2841.00 53.60 1 0 -3 0.25 0.36 1 0 3 0.27 0.22 1 0 3 0.04 0.17 1 0 3 0.30 0.47 -1 0 -3 0.13 0.33 1 0 3 0.22 0.20 1 0 -3 0.21 0.31 -1 0 3 0.39 0.26 1 0 3 0.24 0.21 1 0 -3 0.47 0.40 -1 0 3 0.20 0.40 -1 0 -3 0.02 0.37 -1 0 3 0.12 0.31 -1 0 -3 -0.18 0.32 -1 0 3 0.02 0.30 1 0 4 336.06 6.67 1 0 -4 339.78 6.79 -1 0 -4 194.90 6.62 1 0 4 196.92 6.55 1 0 4 326.18 6.62 1 0 4 337.08 6.77 1 0 -4 324.60 6.71 -1 0 4 339.98 6.76 -1 0 -4 203.79 6.63 1 0 4 338.83 6.77 -1 0 4 262.64 6.68 -1 0 -4 332.37 6.71 1 0 -4 342.85 6.75 1 0 4 244.76 6.55 1 0 -4 202.41 6.62 -1 0 -4 334.47 6.66 -1 0 -4 289.51 6.60 1 0 -5 0.59 0.61 1 0 5 0.34 0.41 1 0 -5 -0.07 0.56 -1 0 5 0.63 0.65 1 0 -5 -0.52 0.61 -1 0 -5 -0.12 0.50 -1 0 5 0.03 0.63 -1 0 -5 0.34 0.43 -1 0 -5 -0.02 0.56 1 0 5 -0.03 0.67 1 0 -5 0.42 0.57 1 0 5 -0.02 0.47 1 0 5 0.18 0.51 1 0 5 0.40 0.44 -1 0 5 0.54 0.62 -1 0 5 -0.52 0.67 1 0 5 0.34 0.74 -1 0 5 -0.02 0.53 1 0 -5 0.31 0.62 -1 0 -5 0.29 0.68 1 0 5 -0.03 0.56 -1 0 -5 0.54 0.50 1 0 6 373.53 10.02 1 0 6 363.95 9.91 -1 0 6 377.12 9.93 1 0 -6 391.02 10.01 -1 0 -6 378.99 10.02 1 0 6 370.82 9.83 -1 0 -6 367.18 9.81 -1 0 6 371.47 10.03 -1 0 6 385.71 10.02 -1 0 -6 363.88 9.86 1 0 6 369.69 9.99 1 0 6 365.15 9.96 1 0 6 377.09 9.91 1 0 -6 387.75 9.98 -1 0 6 378.37 10.02 1 0 6 364.27 9.84 -1 0 -6 358.57 9.93 1 0 -6 381.89 10.01 1 0 6 370.28 9.97 -1 0 -6 371.18 9.89 1 0 -6 376.01 10.03 -1 0 6 383.83 9.97 -1 0 -6 346.17 9.92 1 0 -6 352.62 9.91 -1 0 -7 -0.06 0.67 1 0 7 0.41 0.60 -1 0 -7 -0.13 0.76 1 0 7 0.29 0.48 -1 0 -7 0.04 0.96 -1 0 7 0.51 0.87 1 0 -7 0.55 0.89 1 0 7 -0.22 0.87 1 0 7 -0.04 0.93 1 0 7 0.72 0.78 -1 0 7 0.03 0.79 -1 0 7 0.24 0.93 -1 0 -7 0.55 0.68 -1 0 -7 0.25 0.51 1 0 7 0.65 0.69 -1 0 7 0.49 0.90 1 0 7 0.29 0.54 -1 0 7 0.35 0.40 1 0 -7 0.46 0.73 -1 0 -7 -0.07 0.72 1 0 -7 0.98 0.85 1 0 -7 0.36 0.88 1 0 7 -0.72 0.62 -1 0 7 -0.56 0.74 -1 0 8 363.99 9.74 -1 0 8 360.00 9.63 1 0 8 355.28 9.57 -1 0 8 359.50 9.74 1 0 8 360.57 9.74 1 0 8 354.03 9.52 -1 0 8 344.25 9.30 -1 0 -8 366.62 9.57 1 0 -8 346.87 9.58 1 0 8 328.58 9.35 1 0 8 356.88 9.68 -1 0 -8 361.27 9.65 -1 0 -8 368.57 9.75 -1 0 -8 356.23 9.42 1 0 -8 362.85 9.75 1 0 8 352.74 9.62 -1 0 8 365.88 9.64 -1 0 -8 341.42 9.62 1 0 -8 361.70 9.70 -1 0 8 365.82 9.76 1 0 8 345.68 9.66 1 0 8 360.24 9.44 -1 0 -8 355.43 9.53 1 0 -8 369.19 9.71 1 0 -9 0.31 0.81 1 0 9 0.21 0.53 -1 0 9 0.66 0.84 1 0 9 1.19 0.88 -1 0 -9 0.44 0.79 1 0 9 0.28 0.56 -1 0 -9 1.09 0.55 1 0 -9 0.05 1.04 1 0 9 -0.85 0.70 -1 0 9 0.05 0.98 -1 0 -9 0.61 1.10 1 0 9 -0.18 0.95 -1 0 -9 0.18 0.92 1 0 9 -0.20 0.65 1 0 9 0.23 0.48 -1 0 9 1.18 0.85 -1 0 -9 0.66 0.87 1 0 -9 -0.75 0.89 1 0 9 0.25 1.02 1 0 9 -0.08 0.80 -1 0 9 -0.11 0.41 -1 0 -9 0.17 0.66 -1 0 9 0.50 1.03 1 0 -9 0.37 0.88 -1 0 9 0.05 1.09 1 0 10 -0.24 0.52 -1 0 -10 0.68 1.20 1 0 10 0.49 0.50 1 0 -10 0.36 0.93 1 0 -10 0.51 1.00 -1 0 10 -0.22 1.06 -1 0 10 0.47 0.88 -1 0 10 0.17 1.09 -1 0 -10 -0.04 0.81 -1 0 10 1.59 1.09 1 0 10 0.91 0.92 -1 0 10 -0.33 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0.77 2 0 -11 0.90 0.53 2 0 -11 -0.05 0.84 2 0 -11 1.13 1.13 2 0 11 0.19 0.68 -2 0 -11 1.23 1.20 2 0 11 -0.34 1.04 -2 0 11 0.59 0.97 2 0 11 1.20 1.13 2 0 11 -0.06 1.23 2 0 11 -0.32 0.71 2 0 11 -0.18 1.04 -2 0 -11 0.04 0.86 2 0 11 0.73 0.66 2 0 11 0.46 0.67 -2 0 -11 0.82 0.73 2 0 11 0.44 0.60 2 0 -11 0.94 1.00 -2 0 11 1.39 1.14 2 0 11 0.05 0.79 -2 0 11 0.39 1.22 2 0 -11 -0.06 1.09 -2 0 11 0.16 0.91 2 0 12 286.20 7.81 -2 0 -12 268.04 7.74 2 0 -12 299.78 8.01 2 0 12 271.40 7.52 -2 0 12 275.68 7.91 2 0 12 274.81 7.68 2 0 12 281.21 7.96 -2 0 12 282.91 8.07 -2 0 12 269.58 7.42 2 0 12 268.45 7.97 -2 0 12 284.01 7.91 2 0 12 280.50 7.57 2 0 -12 290.22 8.11 2 0 12 283.75 7.69 2 0 -12 284.35 8.05 2 0 12 279.70 7.93 2 0 -12 261.27 7.38 2 0 12 279.94 7.56 -2 0 12 288.06 8.10 2 0 -12 278.32 7.82 -2 0 -12 287.88 8.10 -2 0 -12 284.19 7.78 2 0 12 270.09 7.84 2 0 12 283.92 8.09 2 0 13 0.87 0.71 2 0 13 0.83 0.70 2 0 13 1.21 0.93 2 0 -13 0.60 1.02 2 0 13 -1.00 0.91 -2 0 -13 0.37 0.94 -2 0 13 -0.06 0.49 2 0 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-1 2 4 1.00 0.68 -1 -2 -4 1.26 0.65 1 2 4 0.72 0.56 1 2 -4 0.47 0.77 1 2 -4 0.94 0.59 -1 2 4 1.68 0.55 1 -2 5 138.05 3.95 1 -2 5 147.23 4.37 1 2 -5 156.25 4.29 -1 2 5 148.63 4.36 -1 -2 -5 153.07 4.39 -1 -2 5 145.09 4.35 -1 -2 5 150.93 4.19 1 -2 5 151.25 4.32 1 2 5 146.86 4.13 -1 -2 -5 145.17 4.29 1 -2 -5 152.56 4.39 -1 2 -5 151.74 4.33 1 2 5 141.99 4.21 -1 2 5 150.08 4.11 1 -2 5 153.06 4.29 -1 -2 5 147.68 4.04 1 2 5 153.82 4.31 1 2 5 149.98 4.07 1 -2 5 94.80 4.11 -1 2 -5 146.60 3.95 -1 -2 5 147.59 4.27 -1 2 -5 144.05 4.33 1 -2 -5 148.86 4.09 -1 -2 5 149.81 4.20 -1 -2 5 144.09 4.16 -1 2 -5 145.23 4.10 -1 -2 5 149.35 4.07 1 2 5 151.67 4.33 -1 2 -5 147.12 4.32 1 2 -5 151.29 4.06 -1 2 5 146.86 4.22 1 2 5 147.70 4.24 1 2 -5 151.87 4.18 -1 -2 5 144.08 4.06 1 -2 5 149.38 4.14 1 2 -5 153.75 4.22 1 2 -5 153.73 4.35 -1 2 -5 146.37 4.07 1 2 -5 152.65 4.31 1 2 5 147.05 4.28 -1 -2 -5 141.96 4.28 -1 -2 -5 147.36 4.19 1 -2 -5 149.74 4.28 -1 2 5 155.58 4.34 -1 -2 5 147.04 4.30 1 -2 5 150.41 4.13 1 -2 -6 239.64 6.47 1 -2 6 243.12 6.71 1 2 -6 248.93 6.58 1 2 6 242.29 6.45 -1 -2 -6 249.63 6.72 -1 2 6 231.74 6.48 1 -2 6 238.15 6.73 1 2 6 238.14 6.47 1 -2 -6 235.35 6.60 -1 -2 -6 235.07 6.56 1 -2 6 238.08 6.50 -1 -2 6 227.45 6.36 -1 2 -6 239.68 6.31 1 2 6 238.57 6.67 1 2 -6 239.64 6.71 1 2 -6 232.46 6.36 1 2 6 232.82 6.53 1 -2 6 246.38 6.64 1 2 -6 245.87 6.66 -1 2 6 238.01 6.71 1 2 6 237.50 6.67 -1 -2 -6 230.67 6.60 1 -2 -6 237.21 6.73 -1 2 -6 237.30 6.71 -1 2 -6 235.16 6.38 1 2 -6 236.24 6.68 1 2 6 228.18 6.61 1 2 -6 238.35 6.57 -1 -2 -6 233.28 6.71 -1 2 6 237.39 6.55 1 -2 6 234.99 6.43 -1 -2 6 235.67 6.64 1 2 6 237.03 6.56 1 -2 -6 251.51 6.73 -1 -2 6 236.99 6.69 -1 -2 6 243.17 6.39 -1 -2 6 241.93 6.54 1 2 -6 236.39 6.39 -1 2 -6 241.45 6.69 -1 -2 -6 236.58 6.62 -1 2 6 230.30 6.67 -1 -2 6 233.02 6.59 1 -2 6 240.06 6.31 -1 2 -6 245.24 6.68 -1 -2 6 228.89 6.34 -1 -2 6 238.11 6.74 1 2 6 235.86 6.63 -1 2 7 6.96 0.56 1 -2 7 9.26 0.70 1 2 7 9.86 0.86 1 -2 7 10.20 1.21 1 2 -7 9.27 1.14 1 2 7 9.28 1.01 -1 -2 -7 10.18 1.12 1 2 7 7.69 1.04 1 -2 -7 7.01 0.97 1 -2 -7 11.05 1.16 -1 -2 7 8.26 1.13 1 -2 7 8.44 1.18 1 -2 -7 8.84 0.88 -1 -2 7 7.41 0.89 1 2 -7 10.03 1.12 1 2 7 8.10 0.88 1 -2 7 8.97 1.09 1 2 7 9.65 0.90 1 -2 -7 9.06 0.91 -1 2 -7 9.30 1.05 -1 2 7 9.86 1.14 -1 2 -7 9.58 1.14 -1 2 -7 8.66 0.65 -1 -2 7 9.21 0.62 -1 -2 -7 9.08 1.17 -1 2 7 7.70 0.88 1 -2 7 8.61 0.61 1 2 -7 10.39 0.77 -1 2 7 10.72 0.89 -1 -2 -7 8.66 0.96 -1 -2 -7 7.15 0.98 -1 -2 7 8.97 1.06 -1 2 -7 8.81 0.64 -1 -2 -7 7.86 0.93 -1 -2 7 8.52 1.22 -1 2 7 8.52 1.04 -1 -2 7 8.32 0.70 1 2 -7 7.81 0.64 1 -2 -7 9.17 1.22 1 2 7 8.83 0.85 -1 -2 7 8.39 0.57 1 2 -7 7.91 1.21 1 -2 -7 8.70 0.61 -1 2 -7 8.19 1.15 1 2 -7 8.86 1.00 1 2 7 9.44 1.07 -1 -2 8 2.20 1.12 1 2 8 1.12 0.73 -1 -2 -8 2.40 1.06 1 -2 -8 0.62 0.79 1 2 8 1.43 0.81 1 -2 -8 3.83 1.12 -1 -2 8 2.46 0.97 1 2 8 1.77 0.73 -1 2 8 1.30 0.54 1 2 8 1.42 1.01 1 2 -8 2.75 1.05 -1 2 8 2.65 0.88 -1 2 8 1.33 1.09 1 -2 -8 1.12 0.55 -1 -2 -8 1.93 0.87 -1 -2 8 0.70 1.08 1 2 -8 1.78 0.87 1 -2 8 0.60 1.09 1 -2 -8 1.33 0.88 -1 2 -8 1.29 0.50 -1 2 8 0.68 0.63 -1 -2 8 1.67 0.90 1 -2 8 0.94 0.55 -1 2 8 2.43 0.99 1 -2 -8 0.97 1.14 -1 -2 -8 1.39 1.09 -1 -2 8 1.60 0.47 1 2 8 2.45 0.77 1 -2 8 0.79 1.12 1 2 8 1.60 0.97 1 -2 8 2.02 1.02 1 2 -8 1.97 1.03 -1 2 -8 1.68 0.58 -1 -2 8 1.74 0.82 1 -2 -8 1.81 0.83 1 2 8 0.69 0.81 1 -2 8 1.53 0.56 1 2 -8 1.13 0.48 -1 -2 -8 1.46 0.84 -1 2 8 2.77 0.89 -1 2 -8 1.45 0.99 1 2 8 1.42 0.94 1 2 9 484.40 13.20 -1 -2 -9 477.65 13.28 1 -2 9 514.72 13.60 -1 -2 9 499.52 13.29 1 -2 -9 480.19 13.08 -1 2 9 517.23 13.47 -1 -2 9 511.79 13.57 1 2 9 506.25 13.43 1 2 9 500.72 13.32 -1 -2 -9 506.63 13.54 1 2 -9 514.77 13.47 -1 2 -9 495.60 13.48 1 2 9 510.07 13.48 1 -2 9 487.50 13.54 1 -2 -9 471.76 13.37 -1 2 9 456.08 13.08 -1 -2 9 502.07 13.37 -1 -2 9 512.47 13.57 -1 2 -9 503.53 13.26 1 -2 -9 500.57 13.29 1 -2 -9 523.70 13.57 -1 -2 9 500.86 13.07 -1 2 -9 494.49 12.99 1 2 9 496.70 13.41 1 -2 9 503.85 13.43 1 2 -9 503.59 13.34 -1 2 9 478.32 13.21 1 -2 9 494.58 13.06 1 2 9 509.90 13.42 -1 2 9 498.43 13.45 -1 2 -9 503.57 13.53 -1 2 9 488.81 13.32 -1 -2 -9 495.78 13.52 1 -2 -9 495.75 13.44 1 -2 9 496.78 13.09 1 2 -9 502.45 13.43 -1 -2 -9 483.19 13.30 -1 2 -9 503.97 13.12 -1 -2 9 506.11 13.48 1 -2 -9 507.16 13.56 -1 2 9 511.99 13.56 1 2 9 490.79 13.25 1 -2 -9 484.02 13.26 -1 -2 -10 167.58 4.84 -1 2 10 154.74 4.87 -1 2 -10 164.22 4.45 -1 -2 10 172.79 5.06 1 2 10 160.60 4.74 1 2 10 165.68 4.95 1 2 -10 163.69 5.00 1 -2 -10 162.07 4.77 -1 2 -10 166.47 5.12 1 2 -10 162.35 4.88 -1 -2 10 164.43 4.57 -1 -2 10 171.13 5.12 -1 2 10 168.21 4.72 1 2 -10 170.08 5.03 1 -2 -10 161.40 4.62 1 -2 -10 146.01 4.86 -1 2 10 161.44 5.10 -1 -2 10 165.51 4.92 -1 -2 10 166.94 4.82 1 2 10 168.99 4.88 1 -2 10 168.82 4.99 1 -2 10 174.00 5.16 1 2 10 164.49 4.98 1 -2 -10 167.90 5.13 -1 2 10 158.79 4.99 1 2 10 156.81 4.74 -1 2 -10 163.21 4.74 1 -2 -10 171.81 5.01 1 -2 10 172.09 5.16 1 -2 10 161.27 4.53 -1 -2 -10 159.58 4.81 1 2 10 167.19 5.05 1 -2 -10 170.75 4.86 -1 2 10 159.35 4.63 -1 2 10 163.46 4.99 1 2 10 166.51 4.96 -1 -2 -10 166.73 5.09 -1 -2 10 161.32 5.12 1 -2 10 167.20 4.62 1 -2 -10 166.43 5.13 -1 2 -10 170.95 4.67 -1 -2 -10 173.81 5.12 1 -2 -11 18.48 1.29 1 2 -11 23.37 1.64 -1 -2 -11 26.81 1.69 -1 -2 11 25.85 1.36 -1 2 11 24.18 1.54 -1 2 11 24.80 1.51 1 2 11 22.67 1.67 -1 2 -11 26.78 0.93 -1 -2 11 25.77 1.09 -1 2 -11 24.63 0.97 -1 2 -11 25.83 1.76 1 -2 -11 25.77 1.43 1 -2 -11 24.29 1.32 1 2 11 25.98 1.45 -1 2 -11 24.68 1.22 1 2 11 27.65 1.32 -1 -2 11 25.66 1.63 -1 -2 11 23.80 1.64 1 -2 11 26.91 1.74 1 -2 -11 22.79 1.18 -1 -2 -11 23.21 1.35 -1 2 11 23.11 1.18 1 -2 11 23.74 1.56 -1 -2 11 24.63 1.45 -1 -2 -11 23.52 1.33 1 -2 -11 24.75 1.72 -1 2 11 24.97 1.72 1 2 -11 25.12 1.63 -1 2 11 24.01 1.49 1 2 11 26.75 1.32 1 -2 11 25.31 0.99 1 -2 -11 24.64 1.74 -1 -2 -11 26.34 1.68 -1 2 11 22.86 1.15 1 2 11 26.69 1.21 -1 -2 11 26.12 1.76 1 2 11 23.97 1.55 -1 2 -11 25.74 1.25 1 -2 11 26.89 1.78 1 2 11 28.49 1.54 1 2 11 25.44 1.55 1 2 -11 23.29 1.45 -1 -2 11 24.32 1.56 1 -2 -11 24.26 1.54 1 -2 11 27.35 1.17 -1 2 -12 272.37 7.52 1 -2 12 277.24 7.47 -1 -2 -12 272.52 7.93 1 -2 -12 288.67 7.72 1 -2 12 267.33 7.26 1 -2 -12 273.00 7.99 1 -2 -12 278.37 7.83 -1 -2 12 280.38 7.83 -1 -2 -12 279.59 7.60 -1 2 12 273.78 7.98 -1 2 12 270.62 7.49 -1 -2 12 274.85 7.98 1 2 12 265.69 7.53 1 -2 12 279.90 7.82 1 -2 -12 277.09 7.48 1 2 12 281.17 7.81 1 2 12 270.24 7.61 1 2 12 267.71 7.47 -1 2 -12 284.30 8.01 -1 -2 12 280.06 7.77 1 2 -12 278.95 7.73 -1 2 12 276.86 7.87 -1 2 -12 273.53 7.24 1 -2 -12 277.90 7.55 1 2 -12 280.24 7.86 1 2 -12 285.63 7.93 -1 -2 12 276.72 7.65 -1 -2 12 274.53 7.94 -1 2 -12 271.96 7.18 -1 -2 -12 276.55 7.61 -1 -2 -12 281.34 8.00 -1 -2 12 277.84 8.02 1 2 12 274.00 7.83 -1 2 12 272.81 7.51 -1 2 -12 270.25 7.51 1 2 12 281.08 7.79 -1 -2 12 272.98 7.36 -1 2 12 271.03 7.81 1 -2 12 277.94 8.03 1 -2 -12 270.76 7.99 1 2 12 269.23 7.76 1 2 12 280.98 7.95 -1 2 -12 278.57 7.75 -1 2 12 276.15 7.80 1 2 12 277.49 7.88 1 -2 12 272.18 7.98 -1 -2 -13 2.88 0.97 1 -2 13 1.06 1.47 -1 -2 13 3.55 1.33 -1 -2 -13 1.03 1.32 1 2 13 1.99 0.85 -1 2 13 0.39 1.17 -1 2 13 1.77 1.09 1 2 13 0.82 0.88 1 2 13 1.17 1.08 1 -2 13 1.66 0.49 -1 2 -13 0.81 0.71 1 -2 13 1.85 1.33 1 -2 -13 0.39 0.62 -1 2 -13 1.36 0.90 1 2 13 2.59 1.14 -1 -2 13 1.68 1.10 1 2 13 1.90 1.03 1 2 13 4.38 1.39 1 -2 -13 1.33 1.40 1 2 -13 0.60 0.69 1 -2 -13 2.90 1.14 -1 2 -13 2.50 1.37 -1 -2 13 2.29 1.02 -1 2 -13 1.51 1.04 1 -2 -13 1.53 0.97 1 2 13 0.90 0.72 -1 2 13 2.09 1.32 1 -2 -13 1.76 1.34 1 2 -13 1.48 1.07 -1 -2 -13 0.07 1.19 1 2 -13 1.67 1.34 1 -2 -13 0.17 0.87 -1 2 13 2.35 0.84 -1 -2 13 1.39 0.96 -1 2 13 0.13 1.05 1 -2 13 1.99 1.12 -1 2 -13 0.97 0.46 1 2 13 2.06 1.21 1 -2 -13 1.00 0.76 1 2 13 2.88 1.21 -1 -2 13 1.20 0.70 -1 -2 13 1.25 1.26 -1 2 13 1.84 0.71 -1 -2 -13 2.59 0.90 1 -2 13 2.21 0.76 -1 -2 13 1.96 1.43 -1 2 -13 1.48 0.87 1 2 -13 1.37 1.15 -1 -2 14 158.03 5.13 1 2 -14 156.57 4.90 -1 2 -14 161.51 5.10 1 2 14 165.05 4.88 -1 2 -14 164.90 4.59 -1 -2 14 159.02 4.32 -1 -2 14 159.37 4.83 -1 2 -14 158.16 4.70 1 2 14 167.86 5.11 1 -2 -14 164.13 5.11 1 -2 -14 163.18 4.75 -1 2 14 158.22 4.57 1 2 14 154.62 4.46 -1 -2 14 160.15 5.09 -1 2 -14 161.14 4.46 1 -2 14 165.22 5.19 1 2 14 158.27 4.78 -1 -2 -14 159.02 4.56 -1 -2 14 161.51 4.79 1 -2 14 161.21 4.49 1 2 -14 167.56 4.83 -1 2 14 168.13 5.15 1 2 14 155.09 4.48 1 2 14 164.53 4.88 1 2 14 166.92 5.03 -1 2 14 161.38 4.91 1 -2 14 158.13 4.15 -1 2 14 165.60 4.90 1 -2 -14 159.88 4.50 1 -2 -14 165.49 5.08 1 -2 -14 166.47 4.89 1 2 -14 168.11 5.04 -1 2 -14 168.41 4.92 1 -2 14 164.14 5.14 -1 -2 14 164.86 4.68 -1 2 14 163.61 4.44 -1 -2 -14 159.86 5.07 -1 -2 -14 164.85 4.56 -1 -2 14 172.11 5.12 1 2 14 162.78 4.89 -1 2 14 170.29 4.90 1 2 -14 128.27 4.66 -1 -2 -14 152.38 4.94 1 2 14 150.41 4.63 1 -2 14 154.88 4.85 1 -2 -14 160.54 4.51 -1 2 -15 433.94 9.33 -1 2 -15 462.68 10.18 -1 -2 15 454.02 10.28 1 2 15 420.56 9.35 1 2 15 448.22 9.78 -1 2 15 449.74 10.14 1 2 15 429.93 9.61 -1 2 15 433.82 9.51 -1 -2 15 433.34 9.17 1 2 15 424.62 9.35 1 -2 -15 451.33 9.45 -1 2 -15 442.36 9.52 -1 -2 15 445.54 9.61 1 2 15 453.90 9.87 1 -2 -15 444.90 10.17 1 -2 15 436.90 9.40 1 2 15 442.99 9.90 1 2 15 456.49 9.86 1 2 -15 457.12 9.84 -1 -2 -15 440.92 9.43 1 2 -15 463.00 10.10 1 2 -15 441.80 9.92 1 -2 15 420.94 8.93 -1 -2 15 456.31 10.18 -1 2 15 451.56 9.95 -1 2 -15 443.70 9.70 1 -2 -15 454.68 10.15 1 2 15 450.57 10.13 -1 2 15 446.61 9.90 1 -2 -15 444.12 9.37 -1 2 15 449.21 10.20 -1 2 -15 458.32 9.92 -1 2 15 432.75 9.29 -1 -2 15 464.49 10.23 1 -2 15 444.28 10.17 1 -2 15 441.30 9.90 1 2 -15 419.89 9.83 1 2 15 438.01 10.04 1 -2 -15 450.27 9.73 -1 -2 15 446.58 9.80 -1 -2 -15 443.35 9.47 -1 2 15 440.27 9.82 1 -2 15 447.72 10.22 -1 -2 -15 441.06 10.00 -1 -2 -15 447.30 10.15 -1 2 16 299.51 8.86 -1 -2 -16 319.05 9.38 -1 2 -16 308.06 8.65 1 2 16 318.35 8.61 -1 -2 -16 327.07 9.30 -1 -2 16 314.30 8.55 1 2 16 324.81 9.23 1 2 -16 320.97 9.32 1 -2 -16 327.20 9.39 -1 2 16 311.92 8.63 -1 2 16 313.46 9.39 -1 2 -16 322.14 9.18 1 2 16 299.97 8.69 -1 -2 16 308.80 9.38 1 -2 16 335.30 9.52 1 -2 -16 322.41 8.69 1 2 -16 311.03 9.04 1 2 16 307.28 8.96 1 -2 -16 322.28 9.03 -1 2 16 309.84 8.31 -1 2 -16 311.93 8.85 1 -2 -16 310.71 9.36 -1 2 16 317.53 9.23 -1 2 -16 322.14 8.97 1 2 -16 318.56 9.09 -1 -2 16 323.67 8.91 1 -2 -16 320.15 8.78 -1 -2 -16 308.60 8.73 -1 2 16 321.40 9.37 1 2 16 312.75 8.69 1 -2 16 313.76 9.40 -1 2 -16 319.85 9.40 -1 -2 16 314.07 9.05 1 2 -16 323.14 9.33 1 2 16 316.64 9.34 1 -2 16 305.66 8.32 -1 -2 -16 317.20 8.78 1 -2 16 312.61 8.76 -1 2 16 311.22 9.07 1 2 16 322.10 9.33 1 -2 16 320.47 9.45 -1 -2 16 313.67 9.45 1 2 16 331.77 9.07 -1 -2 16 311.24 9.36 1 2 17 459.47 13.02 1 2 17 462.08 12.20 -1 -2 -17 448.82 12.35 1 -2 -17 450.26 12.38 -1 2 17 456.97 13.03 1 2 17 456.40 12.84 1 -2 -17 461.77 13.04 1 2 17 454.26 12.66 1 2 -17 461.01 12.70 -1 -2 17 462.76 12.98 -1 2 17 441.71 12.48 -1 2 -17 459.81 12.50 -1 -2 17 452.69 12.51 1 -2 17 460.35 13.03 1 2 17 435.22 12.30 1 -2 -17 451.46 12.96 -1 -2 17 469.42 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6 2.80 0.80 -2 3 6 1.79 1.00 2 3 -6 2.11 0.99 -2 -3 -6 1.99 1.17 2 -3 6 3.77 0.75 -2 -3 6 1.32 1.04 2 3 -6 3.76 1.07 -2 -3 6 2.18 0.84 2 -3 6 3.04 0.89 2 3 -6 1.42 1.09 2 -3 -6 1.34 1.06 -2 3 -6 2.98 0.99 -2 3 -6 2.39 1.08 2 3 -6 2.08 0.81 2 3 6 2.41 0.79 -2 -3 -6 2.71 0.81 -2 -3 6 3.39 0.74 -2 -3 6 2.32 0.87 -2 -3 6 2.17 0.82 -2 -3 6 1.56 1.08 2 3 6 4.65 0.70 2 -3 -6 2.15 0.77 -2 -3 -6 2.36 1.06 2 3 6 1.66 0.75 2 3 -6 2.18 0.83 2 3 6 5.13 1.12 2 3 -6 1.40 0.75 2 -3 -6 2.73 1.16 -2 3 6 1.19 1.12 -2 3 6 2.84 0.83 2 3 6 2.36 1.03 2 -3 6 2.38 1.15 2 3 -6 2.70 0.76 2 3 -6 3.25 1.17 -2 -3 -6 3.57 1.08 -2 3 6 1.52 0.43 -2 3 -6 1.85 0.79 -2 -3 -6 2.06 0.83 2 -3 6 3.54 0.98 -2 3 7 10.26 0.99 -2 -3 7 10.86 1.26 -2 -3 7 10.09 1.16 -2 3 7 7.78 0.93 -2 -3 7 11.65 1.05 2 -3 -7 9.97 0.92 -2 3 7 9.26 1.34 2 3 7 10.28 1.01 2 3 7 10.12 1.30 -2 3 -7 11.30 0.93 2 3 -7 10.08 1.19 -2 3 -7 11.90 1.24 2 3 -7 10.43 1.27 -2 -3 -7 9.92 1.25 2 -3 7 9.68 1.19 2 -3 7 8.44 1.31 -2 -3 7 9.87 1.35 2 3 -7 9.74 1.01 -2 -3 7 10.11 0.90 2 -3 7 10.90 0.92 2 -3 7 11.42 1.01 -2 -3 7 11.16 0.91 2 -3 7 9.28 1.14 -2 3 -7 8.65 1.27 2 3 7 9.36 1.09 2 -3 -7 11.25 1.28 2 3 7 9.05 1.08 2 3 7 10.71 0.89 -2 -3 7 5.55 0.89 2 3 7 11.53 0.95 -2 -3 7 11.38 1.06 -2 3 7 10.01 1.23 2 3 -7 10.58 0.88 2 3 7 9.57 1.24 -2 -3 -7 12.22 1.21 -2 3 -7 9.96 1.21 -2 -3 7 8.90 0.92 2 3 -7 12.02 1.21 2 3 -7 10.10 1.17 2 -3 -7 11.51 1.21 -2 3 7 9.50 1.06 -2 -3 -7 8.40 1.34 -2 -3 -7 12.13 1.01 -2 3 8 89.67 2.95 2 -3 8 89.72 2.45 2 3 8 90.78 2.82 -2 -3 8 96.16 3.17 2 -3 8 72.56 2.90 -2 -3 -8 94.85 3.21 2 3 8 96.55 3.16 2 -3 8 98.83 3.08 2 -3 8 97.73 2.80 -2 3 -8 96.54 3.15 2 -3 -8 95.65 3.08 -2 3 8 91.99 3.24 2 -3 8 99.61 3.27 2 3 -8 94.92 3.03 2 3 8 94.81 3.08 2 -3 8 96.27 2.86 -2 3 -8 93.55 2.76 -2 -3 8 95.42 2.99 -2 3 -8 94.44 2.46 -2 -3 8 96.09 3.23 2 3 -8 91.55 3.14 2 -3 -8 90.16 2.47 2 3 8 92.29 2.77 -2 -3 8 94.41 2.73 -2 3 -8 102.23 3.15 -2 -3 -8 93.18 3.08 2 3 -8 96.05 2.92 2 -3 -8 93.30 2.82 -2 3 -8 93.82 3.20 2 3 8 93.50 2.98 2 3 8 98.30 2.98 -2 -3 8 95.68 2.77 2 3 -8 96.60 3.07 -2 3 8 97.51 2.88 2 -3 8 96.81 3.21 2 3 -8 93.05 2.70 2 3 8 93.60 3.02 -2 -3 -8 92.91 3.07 2 3 -8 97.51 2.83 2 3 -8 93.14 3.11 2 -3 -8 100.69 3.24 -2 3 8 98.05 3.20 -2 3 8 89.88 2.47 2 -3 -8 90.41 3.05 -2 -3 8 96.69 3.11 -2 -3 8 98.17 2.96 2 3 -9 73.14 2.40 2 3 -9 78.78 2.17 -2 3 9 73.85 2.56 -2 -3 9 76.92 2.47 -2 3 -9 69.29 2.46 -2 -3 9 79.38 2.34 -2 3 9 72.36 1.82 2 3 9 74.97 2.58 2 3 9 73.40 2.25 -2 3 9 72.36 2.31 2 3 9 75.82 2.22 -2 3 -9 76.86 2.67 2 3 9 77.92 2.42 2 -3 9 80.72 2.50 2 3 -9 71.69 2.59 2 -3 -9 72.90 2.41 -2 3 -9 68.78 2.31 2 -3 9 76.87 2.19 2 3 9 76.37 2.19 2 3 9 73.74 2.45 -2 -3 9 73.48 2.64 2 3 9 77.90 2.30 2 3 -9 70.94 2.31 -2 -3 9 72.91 2.58 2 -3 9 77.07 2.19 2 -3 -9 77.28 2.69 -2 3 -9 74.48 2.05 2 3 -9 73.85 1.99 2 -3 -9 77.00 2.23 2 3 9 75.95 2.33 2 3 9 75.90 2.46 2 -3 9 71.97 2.61 -2 3 9 76.44 2.65 -2 -3 -9 76.59 2.49 -2 3 9 83.12 2.33 2 -3 -9 70.88 2.47 -2 -3 9 73.12 2.08 -2 -3 -9 78.52 2.68 -2 -3 9 74.55 2.41 2 -3 9 76.37 1.79 2 3 -9 73.12 2.50 -2 -3 -9 79.67 2.53 2 3 -9 77.15 2.48 2 -3 9 80.81 2.65 -2 3 9 72.16 2.48 -2 3 -9 73.99 1.80 -2 3 -9 75.25 2.58 2 -3 -9 73.91 1.82 2 -3 10 688.86 18.39 2 -3 -10 656.13 17.72 2 3 10 674.44 18.22 2 -3 -10 688.34 18.26 -2 -3 10 684.07 18.12 2 3 -10 675.09 17.79 2 -3 -10 701.45 18.40 -2 -3 10 671.47 18.23 2 3 -10 675.34 18.20 -2 -3 10 694.14 18.45 2 -3 -10 683.86 18.19 2 3 10 679.04 18.13 -2 -3 10 682.85 17.90 -2 3 -10 698.59 18.31 2 3 -10 679.57 17.93 2 -3 10 673.38 17.70 2 3 -10 682.37 18.28 2 -3 10 682.60 18.43 2 3 10 679.50 18.14 -2 -3 -10 685.68 18.23 -2 -3 -10 681.56 18.23 2 3 -10 687.42 18.16 -2 3 10 645.33 17.73 -2 3 -10 688.36 18.41 2 -3 -10 681.63 18.03 2 -3 10 677.95 17.97 2 3 10 664.74 18.04 2 3 10 680.45 17.98 -2 -3 10 679.48 18.25 2 3 10 673.23 18.13 -2 3 10 670.72 18.40 2 3 10 662.29 18.32 -2 3 10 679.86 18.09 -2 -3 10 688.90 18.38 2 -3 10 691.52 18.22 2 -3 10 685.54 18.01 -2 3 10 688.35 18.10 2 -3 -10 706.70 18.47 2 3 -10 686.45 18.25 2 3 10 676.87 18.22 -2 -3 -10 673.59 18.38 -2 3 -10 673.75 17.86 -2 3 -10 675.81 18.13 -2 3 10 693.91 18.29 -2 3 -10 668.07 17.72 2 3 10 698.83 18.27 2 3 11 2.88 1.00 2 3 -11 -0.25 1.06 -2 -3 -11 1.58 1.24 -2 3 11 2.20 1.06 -2 -3 -11 2.18 1.07 2 3 11 1.79 1.01 2 -3 -11 0.26 1.05 -2 -3 11 1.67 0.97 2 -3 11 2.57 1.14 2 3 -11 1.81 0.64 2 -3 11 1.73 0.57 -2 3 11 2.42 0.62 2 -3 -11 1.64 0.91 2 -3 11 2.82 1.38 -2 3 -11 1.33 0.85 -2 3 -11 1.00 0.65 -2 3 11 1.30 0.89 -2 3 -11 2.43 1.06 2 3 11 1.48 0.97 2 3 11 2.48 1.10 2 3 -11 2.34 1.17 -2 -3 11 1.87 1.10 -2 3 11 1.35 1.04 2 -3 11 1.30 0.76 -2 -3 -11 0.79 1.07 -2 -3 11 0.66 0.75 2 3 11 0.42 0.92 2 -3 -11 1.75 1.06 2 -3 -11 2.18 0.96 -2 -3 11 1.52 1.34 2 3 -11 2.39 1.21 2 -3 -11 1.52 1.40 -2 -3 -11 1.97 1.37 -2 -3 11 2.07 1.09 -2 3 -11 0.07 0.61 -2 3 -11 0.75 0.60 2 3 11 1.45 1.15 2 3 -11 2.11 0.88 2 3 11 1.82 1.11 2 -3 -11 1.44 0.60 -2 -3 11 0.99 1.33 -2 3 11 1.10 1.29 2 -3 -11 2.23 1.28 2 -3 11 1.55 1.41 2 3 11 1.89 0.89 2 3 -11 1.15 1.03 2 3 12 312.12 8.53 2 3 -12 295.63 8.46 -2 -3 12 290.63 8.50 -2 -3 12 304.43 8.72 -2 3 12 291.33 8.01 -2 3 12 284.36 8.37 -2 -3 -12 284.74 8.41 -2 -3 12 295.99 8.57 -2 -3 12 308.06 8.38 -2 -3 12 300.61 8.76 2 -3 12 299.90 8.49 2 3 12 299.88 8.57 2 -3 12 293.81 8.76 2 -3 -12 292.37 7.99 2 3 12 299.67 8.27 2 -3 -12 303.94 8.77 -2 3 -12 297.07 8.54 -2 -3 -12 288.61 8.41 -2 3 -12 297.98 8.32 2 3 -12 301.03 8.50 2 3 12 296.36 8.42 -2 3 -12 288.45 8.44 -2 3 12 285.06 8.26 2 -3 -12 309.38 8.54 2 -3 -12 300.91 8.31 2 -3 12 290.57 7.95 -2 3 -12 295.94 7.99 2 -3 12 297.18 8.73 2 3 12 285.12 8.30 2 3 12 293.48 8.47 -2 3 12 303.88 8.77 -2 3 12 305.93 8.54 2 -3 -12 295.81 8.37 2 3 12 296.20 8.35 -2 -3 12 290.71 8.35 2 -3 12 293.29 8.12 2 -3 -12 306.87 8.49 2 -3 -12 312.19 8.74 -2 -3 -12 306.91 8.73 2 3 -12 300.32 8.53 -2 -3 12 303.65 8.09 2 3 12 294.90 8.27 -2 3 -12 294.65 7.99 2 3 -12 285.33 7.91 2 3 12 294.01 8.47 -2 -3 -12 307.30 8.72 2 3 -12 291.44 7.89 -2 3 13 127.49 4.01 -2 3 13 134.59 4.29 2 -3 -13 128.57 4.22 -2 -3 13 130.90 4.13 2 -3 -13 138.28 4.55 2 3 -13 125.31 3.56 -2 -3 13 130.61 4.54 -2 3 -13 131.62 4.25 2 3 -13 125.09 4.38 2 -3 13 127.85 3.83 2 3 -13 133.69 4.32 2 -3 -13 136.36 4.22 -2 -3 13 133.15 4.58 2 -3 13 130.04 4.26 2 3 13 127.78 4.06 2 -3 -13 129.50 3.77 -2 -3 13 125.16 4.11 -2 -3 -13 124.96 4.40 -2 -3 -13 137.94 4.22 2 3 13 131.89 4.05 2 -3 13 129.80 3.73 -2 3 13 123.37 4.53 -2 -3 13 129.73 4.40 -2 3 -13 131.13 3.71 2 3 -13 133.29 4.35 -2 3 -13 133.62 4.57 2 3 13 131.40 4.40 -2 3 -13 123.81 3.78 2 3 -13 111.42 3.60 2 3 13 130.17 4.27 2 3 13 129.91 4.16 2 -3 -13 119.29 4.15 -2 3 13 133.63 4.23 -2 -3 -13 130.19 4.49 2 -3 13 139.74 4.65 -2 3 -13 125.57 4.02 -2 3 13 125.32 3.79 2 3 13 130.07 4.22 2 -3 13 133.93 4.58 -2 -3 -13 131.01 4.19 2 -3 -13 134.62 4.59 -2 3 -13 133.98 4.35 -2 3 13 131.27 4.30 2 3 13 136.58 4.28 2 3 13 134.58 4.29 2 -3 -13 129.44 4.26 2 3 13 131.77 4.08 -2 -3 -14 298.57 8.82 -2 3 -14 306.26 8.40 -2 -3 14 297.11 8.78 -2 3 14 292.51 8.38 2 -3 -14 293.79 8.59 2 3 14 293.97 8.68 2 -3 -14 296.62 8.92 -2 3 -14 303.79 8.93 2 -3 14 297.45 8.10 -2 -3 14 312.79 9.13 -2 -3 -14 295.56 8.52 2 -3 -14 306.62 8.48 -2 -3 14 294.86 8.49 -2 3 14 286.89 8.18 2 3 14 286.21 8.39 2 -3 -14 289.75 8.42 2 3 -14 304.33 8.71 2 3 14 300.77 8.58 2 3 14 298.34 8.63 2 -3 -14 300.85 8.90 2 -3 14 302.43 8.93 -2 -3 -14 301.43 8.86 2 3 -14 294.91 7.85 -2 3 14 292.99 8.62 2 -3 14 307.74 9.05 -2 3 -14 297.85 8.09 -2 -3 14 293.74 8.50 2 3 14 304.27 8.78 -2 3 14 298.58 8.90 2 3 14 283.31 8.37 2 -3 14 303.02 8.66 2 3 14 297.34 8.42 2 -3 -14 295.11 8.14 -2 3 -14 303.82 8.62 -2 -3 14 306.10 9.00 2 -3 14 297.07 8.17 -2 -3 -14 294.57 8.50 2 3 -14 309.36 8.73 -2 3 -14 296.84 8.15 2 3 14 299.99 8.55 -2 3 -14 303.34 8.02 -2 3 -15 275.19 7.80 2 3 15 268.49 7.85 -2 -3 -15 275.89 8.32 -2 -3 15 273.80 7.91 2 -3 -15 266.91 7.84 2 -3 15 272.54 7.55 -2 -3 -15 270.12 7.93 2 3 15 283.01 8.06 -2 3 -15 280.96 8.03 -2 3 15 263.87 7.63 2 3 15 271.91 8.15 -2 -3 15 286.75 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3.27 -2 -4 -4 70.02 2.53 2 -4 -4 68.61 2.04 -2 4 -4 72.02 2.53 -2 4 -4 69.62 2.19 2 4 -4 72.78 2.42 -2 4 -4 70.86 2.42 2 -4 -4 80.00 2.66 -2 -4 4 72.91 2.60 2 4 -4 75.13 2.65 -2 4 -4 68.51 2.18 2 -4 4 73.63 2.38 -2 -4 4 70.99 2.48 -2 -4 4 70.25 2.55 2 -4 -4 70.08 2.66 2 4 4 75.32 2.31 2 4 -4 72.21 2.71 -2 -4 4 74.78 2.69 2 4 -4 72.92 2.58 2 4 -4 72.76 2.50 2 -4 4 72.14 2.60 2 -4 4 73.52 2.48 -2 -4 -4 73.02 2.14 2 -4 -4 71.20 2.73 -2 4 -4 75.18 2.72 -2 4 -4 71.07 2.70 -2 -4 4 75.35 2.61 -2 -4 -4 76.64 2.78 -2 4 -4 73.56 2.55 -2 -4 -4 74.49 2.80 2 4 -4 69.17 2.24 -2 -4 4 72.38 2.23 -2 4 4 73.43 2.23 2 4 -4 73.51 2.81 -2 -4 4 51.52 2.39 -2 4 -4 75.36 2.57 -2 4 4 73.36 2.71 -2 -4 4 72.54 2.53 2 -4 4 71.34 2.58 -2 4 4 76.46 2.74 2 -4 -4 71.34 2.19 2 4 4 70.77 2.30 2 -4 4 75.72 2.68 2 4 4 75.47 2.67 -2 -4 -4 74.75 2.30 2 4 4 75.13 2.12 2 4 4 71.70 2.07 -2 -4 4 73.55 2.21 2 4 -4 73.59 2.53 2 4 4 77.07 2.73 2 4 4 68.60 2.79 2 4 4 71.08 2.68 -2 4 4 68.73 2.60 -2 4 4 72.80 2.55 -2 4 -4 71.64 2.51 -2 -4 -5 41.08 1.80 2 -4 -5 43.98 1.90 -2 4 -5 42.13 1.69 -2 -4 5 37.77 1.90 2 -4 5 43.37 1.64 -2 4 5 38.57 1.86 -2 -4 -5 41.15 1.59 -2 -4 5 43.50 1.79 -2 4 -5 34.59 1.36 2 4 5 46.38 1.55 -2 -4 5 41.62 2.00 2 4 -5 43.43 1.84 -2 4 5 39.36 2.04 -2 -4 -5 40.50 1.42 2 -4 5 41.84 1.79 2 -4 5 43.84 1.96 2 -4 -5 43.94 2.05 2 4 -5 44.14 2.01 -2 4 -5 42.38 1.84 2 4 5 41.39 1.93 -2 4 -5 41.53 2.00 2 4 -5 45.10 2.10 -2 4 5 42.93 1.81 -2 -4 5 40.97 1.82 -2 -4 -5 43.05 2.08 -2 4 -5 39.88 1.88 2 4 -5 43.23 1.74 -2 -4 5 41.03 1.52 -2 4 -5 41.93 2.00 2 -4 5 38.46 1.86 -2 4 5 46.40 1.51 -2 4 -5 43.02 1.79 -2 4 5 41.77 2.05 -2 -4 5 40.30 1.72 2 -4 -5 43.13 1.47 2 4 -5 40.19 1.89 2 4 5 42.49 1.91 2 -4 5 41.57 1.86 2 4 5 42.13 2.03 2 4 -5 38.70 1.74 2 4 5 42.29 1.40 -2 -4 -5 40.45 1.99 2 4 -5 41.32 1.73 2 -4 -5 43.96 2.04 2 4 5 44.71 1.99 2 4 5 41.71 1.60 -2 4 -5 39.35 1.39 -2 -4 5 42.02 1.82 -2 -4 5 41.21 1.53 -2 4 -5 41.70 1.74 -2 -4 6 49.85 2.10 2 -4 -6 47.10 2.11 -2 -4 -6 49.62 1.96 2 4 -6 48.64 2.03 2 -4 6 48.28 1.75 2 4 6 42.94 2.09 -2 4 -6 42.70 1.46 -2 4 -6 47.96 1.49 -2 -4 6 48.59 1.90 2 4 -6 48.74 1.81 -2 -4 -6 52.26 2.26 2 4 6 51.50 2.21 -2 -4 -6 47.40 2.15 -2 -4 6 49.26 2.15 -2 4 -6 47.55 1.80 -2 -4 6 46.61 1.98 -2 4 6 45.80 1.99 -2 -4 -6 48.97 1.58 2 -4 6 47.75 1.95 2 4 -6 45.31 2.15 2 -4 6 49.45 2.10 -2 4 -6 52.52 2.20 -2 -4 6 48.41 1.89 2 -4 6 48.68 2.04 -2 -4 -6 49.90 2.18 2 4 6 49.94 1.55 -2 4 -6 49.46 1.99 -2 4 -6 49.00 2.15 2 -4 -6 51.19 1.61 -2 -4 6 47.64 1.73 -2 4 6 46.80 1.64 -2 -4 -6 46.63 1.74 -2 -4 6 49.11 1.82 -2 4 6 51.75 2.21 -2 4 -6 52.47 1.87 2 4 6 50.21 1.78 2 4 6 52.41 2.05 2 4 -6 49.64 2.03 2 -4 6 48.10 1.96 2 4 6 49.91 1.59 -2 4 -6 51.28 1.92 2 4 -6 48.22 2.22 2 4 -6 47.85 1.86 2 4 -6 48.23 1.90 2 -4 -6 51.29 2.04 2 -4 -6 52.74 2.25 2 4 6 46.29 2.14 -2 4 6 49.66 2.13 -2 -4 6 46.71 1.67 -2 4 7 26.72 1.74 2 -4 7 27.02 1.61 -2 4 -7 25.34 1.30 2 4 -7 24.20 1.47 -2 4 -7 26.46 1.36 2 4 -7 26.14 1.71 -2 4 -7 25.53 0.96 2 -4 -7 27.53 1.74 -2 -4 7 25.45 1.42 -2 -4 -7 23.09 1.38 2 4 7 23.20 1.60 2 -4 7 26.23 1.27 2 -4 -7 24.37 1.61 2 4 -7 24.31 1.52 -2 4 -7 24.92 1.69 -2 -4 7 24.21 1.25 2 -4 -7 27.89 1.51 -2 4 -7 25.36 1.51 -2 -4 7 25.04 1.57 2 -4 7 23.89 1.40 2 4 7 26.45 1.11 2 4 -7 23.75 1.71 -2 -4 7 26.33 1.35 -2 -4 7 26.78 1.73 2 -4 7 27.04 1.56 2 4 -7 25.57 1.26 2 4 -7 23.85 1.28 -2 -4 -7 23.83 1.78 -2 4 7 24.32 1.19 2 4 7 25.26 1.67 -2 4 7 26.32 1.69 -2 -4 -7 22.65 1.62 2 4 7 23.93 1.31 2 4 7 21.91 1.47 -2 4 -7 22.74 1.63 2 4 7 23.50 1.13 -2 -4 7 25.78 1.28 -2 -4 -7 26.82 1.31 2 -4 -7 26.44 1.15 -2 -4 7 25.55 1.21 2 -4 7 25.12 1.64 -2 4 7 25.87 1.50 -2 -4 7 24.69 1.53 2 4 -7 24.31 1.41 2 4 -7 24.70 1.33 -2 -4 -7 24.82 1.59 -2 4 -7 26.52 1.36 2 -4 7 24.89 1.49 2 -4 8 4.12 0.99 2 4 8 4.28 1.04 2 -4 8 5.60 1.27 2 4 -8 6.11 1.13 2 4 8 4.04 0.83 -2 4 -8 5.63 0.91 -2 4 -8 4.79 0.58 2 4 8 3.95 1.11 2 4 -8 5.30 1.09 2 -4 -8 4.60 1.37 -2 -4 8 7.31 1.15 2 -4 8 4.46 0.94 -2 -4 -8 3.79 1.37 2 4 -8 6.36 0.87 2 4 8 3.49 1.29 -2 -4 8 4.88 1.03 -2 -4 8 4.39 0.97 -2 -4 -8 7.22 1.19 2 4 -8 5.24 1.33 2 4 -8 5.90 1.35 2 4 -8 5.99 0.93 2 -4 8 4.57 0.56 2 -4 8 5.15 1.30 2 -4 8 5.48 1.14 -2 4 -8 4.64 1.23 -2 4 -8 3.59 1.04 2 4 -8 3.89 0.97 2 4 -8 4.98 1.11 -2 -4 8 4.98 0.88 -2 4 -8 5.15 1.33 2 4 8 4.34 1.08 2 4 8 4.53 0.81 -2 -4 8 4.93 0.87 -2 -4 -8 7.07 1.33 2 -4 8 0.49 0.56 2 4 8 4.54 0.97 -2 4 8 3.90 1.05 -2 4 8 4.51 1.34 -2 -4 8 4.79 1.25 -2 4 8 4.28 1.26 -2 4 8 5.72 0.89 2 -4 -8 5.24 1.27 -2 -4 -8 5.62 0.93 -2 -4 8 6.86 1.25 2 -4 -8 4.42 0.82 -2 -4 8 4.41 0.79 2 -4 8 6.93 1.18 -2 4 -8 5.26 0.88 -2 -4 9 151.14 4.09 2 4 9 144.89 3.80 -2 4 -9 147.09 3.56 2 4 9 154.04 4.40 -2 4 9 154.90 4.41 2 4 -9 144.18 4.14 -2 -4 9 150.65 4.25 2 -4 9 147.65 3.93 -2 -4 9 146.98 4.04 2 -4 9 149.50 4.03 2 -4 -9 146.69 4.28 -2 -4 -9 149.49 4.55 2 -4 9 138.02 3.54 -2 -4 9 145.63 4.41 2 4 -9 145.71 4.37 -2 4 -9 150.20 4.36 2 -4 -9 153.85 4.47 2 -4 -9 147.24 3.82 2 -4 9 149.09 4.15 2 -4 9 143.36 4.37 2 -4 9 138.40 4.17 2 4 9 145.89 3.77 -2 -4 9 144.66 3.86 -2 -4 9 145.15 4.28 -2 4 -9 145.15 4.37 -2 -4 -9 145.71 4.33 2 4 -9 142.66 4.03 -2 -4 9 146.12 3.94 -2 4 -9 149.01 3.86 -2 4 -9 151.67 4.24 2 4 9 150.81 3.93 2 4 -9 155.61 4.26 2 4 -9 149.05 4.16 -2 -4 -9 153.80 4.34 -2 4 9 148.66 4.46 -2 4 9 148.20 3.88 2 4 9 146.34 4.11 2 4 9 154.30 4.19 2 4 9 149.19 4.19 -2 -4 -9 142.15 3.97 2 4 -9 146.94 3.83 -2 4 9 151.91 4.16 -2 -4 9 147.18 3.84 2 4 9 147.23 4.28 2 -4 9 149.02 4.32 -2 4 -10 72.10 1.90 2 4 -10 73.41 2.45 2 4 -10 68.70 2.53 2 -4 10 76.18 2.33 2 4 10 75.43 2.78 -2 4 10 73.97 2.77 2 4 10 72.18 2.52 2 -4 10 78.64 2.87 2 -4 10 76.74 2.34 2 -4 -10 74.49 2.64 2 -4 -10 72.42 2.21 2 -4 10 71.09 1.87 -2 4 -10 74.55 2.78 -2 -4 -10 67.52 2.60 -2 4 -10 76.05 2.77 -2 -4 10 75.28 2.85 2 4 -10 74.87 2.60 2 4 10 72.37 2.19 2 -4 10 74.40 2.55 2 -4 10 76.05 2.61 -2 4 -10 74.56 2.61 -2 -4 10 72.88 2.16 -2 -4 -10 74.68 2.69 2 -4 10 80.62 2.79 -2 -4 10 72.74 2.32 -2 -4 -10 71.69 2.35 -2 -4 10 73.34 2.15 2 4 10 77.53 2.52 2 4 10 73.62 2.32 -2 -4 10 73.54 2.74 2 -4 -10 76.86 2.88 -2 4 10 74.38 2.85 -2 4 10 75.34 2.31 2 4 10 71.11 2.49 2 4 -10 71.02 2.20 -2 -4 -10 72.16 2.87 2 4 10 69.73 2.61 -2 -4 10 72.58 2.48 -2 4 10 69.49 2.44 2 4 -10 74.90 2.14 -2 -4 10 75.80 2.13 2 4 -10 77.95 2.88 2 4 -10 73.23 2.54 -2 4 -10 71.66 2.15 -2 -4 10 71.99 2.38 -2 4 10 78.07 2.63 2 4 10 69.12 2.18 -2 -4 10 71.85 2.57 2 4 -11 417.69 11.53 2 4 11 421.24 11.59 2 -4 -11 414.48 11.60 2 4 11 420.22 11.76 -2 -4 11 416.80 11.58 -2 -4 11 420.03 11.41 2 4 11 403.94 11.47 -2 -4 -11 400.84 11.60 -2 4 11 389.95 10.85 2 -4 -11 422.30 11.49 -2 4 11 424.88 11.60 2 4 -11 424.43 11.79 -2 4 -11 414.12 11.74 2 4 -11 423.88 11.57 -2 -4 11 412.11 11.80 2 -4 11 424.92 11.76 2 4 -11 413.41 11.62 2 4 -11 419.66 11.13 2 -4 11 402.43 11.50 2 -4 11 431.29 11.85 2 -4 11 405.83 10.97 2 -4 11 426.01 11.60 -2 4 11 414.75 11.77 2 -4 -11 408.66 10.86 -2 4 -11 412.51 11.60 -2 -4 11 412.52 11.14 -2 -4 -11 413.27 11.62 2 4 -11 418.75 11.48 -2 4 -11 422.33 11.78 -2 -4 11 419.34 11.38 -2 -4 11 420.61 11.73 2 4 11 399.18 11.20 -2 4 -11 419.36 11.00 -2 4 11 424.26 11.80 -2 4 11 419.95 11.33 2 4 11 402.73 11.38 -2 -4 11 421.43 11.55 2 4 -11 415.30 11.19 2 -4 11 421.08 11.34 -2 -4 -11 432.03 11.89 2 -4 11 403.04 11.29 2 -4 -11 415.67 11.26 2 4 11 439.26 11.65 -2 4 11 423.05 11.46 2 -4 -11 436.03 11.87 2 4 11 424.63 11.57 -2 -4 11 410.29 11.15 -2 4 -11 415.26 11.16 2 4 11 419.30 11.28 2 4 -12 29.21 1.86 2 -4 12 18.47 1.85 -2 -4 -12 15.87 1.89 2 4 12 18.65 1.44 2 -4 12 18.86 1.40 -2 -4 12 17.53 1.57 2 -4 12 18.96 0.93 2 -4 12 17.23 1.56 -2 -4 12 18.65 1.39 -2 4 -12 20.44 1.21 2 4 12 19.31 1.56 2 4 12 20.99 1.57 -2 4 -12 24.84 1.21 -2 4 -12 21.32 1.83 2 4 12 22.50 1.89 -2 4 12 20.84 1.85 2 4 -12 20.41 2.03 2 -4 12 13.45 1.34 2 -4 12 14.16 1.92 -2 -4 12 19.08 1.12 2 4 12 20.77 1.36 2 4 -12 19.52 1.59 2 -4 -12 7.29 2.13 -2 -4 12 18.54 1.94 -2 4 -12 22.09 1.91 -2 -4 12 16.13 1.34 2 -4 12 17.76 1.36 -2 -4 -12 17.70 1.57 2 4 -12 12.21 1.17 2 4 12 21.78 1.65 -2 4 12 19.01 0.86 -2 -4 -12 19.88 1.69 2 -4 -12 20.66 0.87 -2 4 12 18.77 1.50 -2 -4 12 17.36 2.21 -2 4 12 15.35 1.83 2 -4 -12 21.95 1.50 2 4 12 21.64 1.42 -2 -4 12 20.39 1.58 -2 4 -12 21.55 1.59 -2 4 12 19.67 1.45 2 4 -12 19.50 1.22 -2 -4 12 20.52 1.14 2 -4 -12 16.41 1.86 2 -4 -12 13.40 1.55 2 4 12 21.60 1.38 -2 4 12 20.64 1.66 2 4 -12 18.08 1.60 2 -4 -13 145.83 4.64 2 4 -13 150.12 4.64 -2 -4 13 151.06 4.48 2 -4 13 156.79 4.46 2 -4 13 146.92 4.02 -2 4 13 131.11 4.53 2 4 13 147.64 4.65 2 4 13 145.78 4.87 -2 -4 -13 163.06 5.01 2 4 -13 143.27 4.07 -2 4 13 151.21 3.98 -2 -4 13 150.76 5.15 2 4 13 152.52 4.36 -2 -4 13 143.88 4.95 -2 -4 -13 152.12 4.71 2 4 13 150.35 4.57 2 4 -13 144.98 4.64 -2 -4 13 148.22 4.49 2 -4 -13 142.99 4.55 -2 -4 -13 140.61 4.65 2 -4 13 145.58 4.63 2 4 13 149.09 4.57 -2 4 13 153.88 4.97 2 4 -13 149.87 4.22 2 -4 13 151.29 4.38 2 4 13 155.17 4.78 -2 4 13 148.65 4.56 -2 -4 13 157.34 4.76 -2 -4 13 150.56 4.15 2 4 13 152.52 4.68 -2 4 -13 151.89 4.49 2 -4 -13 156.88 4.39 2 -4 -13 158.39 5.04 -2 4 13 144.25 4.92 2 4 13 150.97 4.51 2 4 -13 150.59 4.70 -2 4 -13 152.23 4.12 2 4 13 149.37 4.41 -2 4 -13 151.17 4.07 2 -4 13 150.88 4.97 2 -4 13 154.80 5.18 -2 4 -14 112.19 3.63 2 4 -14 104.59 3.76 -2 -4 14 107.22 3.61 2 -4 14 106.64 3.59 2 -4 14 105.57 3.19 -2 -4 -14 103.70 4.07 2 4 14 109.23 4.05 2 4 14 103.56 3.90 -2 4 14 103.47 3.14 -2 -4 14 104.97 4.11 2 4 14 110.45 3.49 -2 -4 -14 108.16 3.81 2 4 14 113.23 3.75 2 4 -14 107.31 3.84 -2 -4 14 101.44 3.62 -2 -4 -14 106.51 3.80 2 -4 -14 103.57 3.77 2 -4 14 105.55 3.38 -2 4 14 108.96 4.12 -2 -4 14 109.41 4.12 2 4 14 106.22 3.53 2 -4 -14 111.32 3.74 2 4 14 116.19 3.80 -2 -4 14 103.68 3.89 -2 -4 14 105.90 3.28 -2 4 14 103.36 4.09 2 4 14 110.62 3.63 -2 4 14 104.49 3.65 2 -4 -14 113.20 3.57 2 -4 -14 104.96 4.15 -2 4 14 104.16 3.59 2 -4 14 102.09 4.14 2 4 14 102.02 3.59 2 -4 14 112.67 4.19 -2 4 -14 108.74 3.25 -2 4 -15 453.85 12.59 2 4 -15 459.57 12.80 -2 4 15 458.90 12.68 -2 -4 15 460.64 12.96 2 -4 -15 471.20 13.18 -2 -4 15 449.54 12.59 -2 -4 -15 457.22 13.09 2 -4 -15 479.27 13.23 2 4 15 452.22 13.08 2 4 15 455.68 12.82 2 -4 -15 468.37 12.56 -2 4 15 452.64 12.58 -2 -4 15 468.97 13.22 2 4 15 450.71 12.50 2 4 15 440.25 12.45 2 4 -15 460.22 12.86 -2 4 -15 463.98 13.11 -2 -4 15 447.22 12.66 -2 4 15 433.68 12.17 2 -4 15 472.14 13.23 2 4 15 454.99 12.62 2 -4 15 449.05 12.34 -2 4 15 465.14 13.17 2 4 15 457.79 12.95 -2 -4 -15 471.61 12.80 2 -4 15 465.78 12.61 2 -4 -15 460.88 12.73 -2 -4 15 468.85 13.15 -2 -4 -15 474.99 12.84 2 -4 15 471.34 13.16 2 4 15 457.48 12.63 -2 4 -15 448.52 12.25 -2 4 -16 231.88 6.86 2 4 16 223.90 6.78 -2 -4 16 249.65 7.37 -2 -4 16 231.42 6.91 -2 4 16 217.40 6.50 2 -4 -16 242.52 6.90 2 4 16 228.28 6.97 -2 -4 16 228.28 7.47 2 4 16 232.07 6.91 -2 -4 16 236.61 7.61 2 4 16 235.13 6.86 2 -4 16 230.32 7.54 2 4 16 235.17 7.19 -2 -4 -16 229.30 7.04 2 4 -16 241.88 7.26 2 -4 -16 247.75 7.60 -2 4 -16 238.32 7.46 2 -4 -16 226.95 6.99 -2 -4 -16 243.42 7.50 2 -4 -16 250.24 7.59 2 -4 16 232.08 6.61 -2 -4 -16 248.54 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22.07 1.40 -4 4 8 23.98 1.47 4 4 -8 19.84 1.77 -4 4 8 21.76 1.53 4 4 -8 22.34 1.72 -4 -4 8 24.51 1.58 -4 -4 8 25.56 1.56 4 4 8 21.40 1.57 4 4 8 21.98 1.29 4 4 8 20.31 1.57 -4 4 8 22.08 1.68 4 4 8 23.26 1.78 4 4 8 20.75 1.54 -4 -4 8 23.33 1.92 4 4 -8 20.98 1.50 4 4 8 23.00 1.81 4 -4 -8 19.93 0.98 -4 4 -8 23.93 1.89 4 4 -8 20.06 1.65 -4 4 -8 24.28 1.63 4 -4 8 23.08 1.83 -4 -4 -8 19.86 1.41 -4 -4 8 21.80 1.41 4 -4 8 23.14 1.54 4 4 -8 23.59 1.32 4 4 8 21.05 1.23 -4 4 8 24.16 1.55 4 -4 -8 22.66 1.75 -4 4 -8 21.01 1.84 4 -4 8 18.84 1.46 4 -4 8 18.92 1.42 4 4 -8 23.23 1.54 4 4 -8 24.34 1.28 4 -4 8 23.39 1.56 -4 4 8 21.33 1.45 -4 4 8 21.47 1.82 4 -4 -8 25.11 1.65 4 -4 -8 22.85 1.37 4 4 -8 22.55 1.28 -4 -4 8 18.90 1.69 -4 4 -8 20.85 1.06 -4 -4 8 22.41 1.41 4 -4 8 23.10 1.10 -4 4 -8 24.70 1.56 4 4 -8 21.16 1.51 4 4 8 20.10 1.48 4 -4 8 22.67 1.50 -4 4 -8 25.32 1.40 4 -4 -8 23.84 1.77 -4 4 8 20.44 1.37 4 4 8 21.89 1.36 -4 4 9 0.07 0.48 -4 4 -9 0.56 0.88 -4 4 9 1.55 0.92 -4 4 9 1.32 1.10 4 4 -9 0.89 1.22 4 -4 9 1.30 1.08 -4 -4 9 0.81 1.06 4 -4 9 1.37 0.69 -4 4 9 0.39 0.90 4 4 9 -0.29 1.14 -4 -4 9 0.82 1.08 4 4 9 0.08 1.33 -4 4 9 1.37 1.29 -4 4 9 0.13 1.03 4 4 -9 -0.50 1.15 4 -4 -9 6.95 0.78 4 4 9 1.31 1.15 4 4 -9 -0.30 1.08 -4 -4 9 0.54 1.53 4 4 -9 -0.45 1.26 -4 4 -9 1.79 1.18 -4 4 -9 0.16 1.47 4 4 -9 1.24 0.88 4 -4 -9 4.06 1.23 -4 -4 -9 2.01 1.10 4 -4 9 2.27 1.44 4 -4 -9 1.73 1.63 4 -4 9 -0.73 1.12 4 4 9 0.86 0.87 4 4 9 -0.27 0.98 -4 4 -9 0.81 1.41 -4 -4 9 0.07 0.99 4 -4 9 -0.06 1.01 4 -4 9 0.74 1.08 4 4 -9 0.14 0.73 4 4 9 0.07 1.06 -4 4 9 1.24 1.07 -4 4 9 -0.09 1.36 4 -4 9 -0.06 0.98 4 4 9 1.13 0.88 4 -4 -9 0.07 1.09 -4 -4 9 2.31 1.58 -4 -4 9 0.45 0.81 -4 -4 9 -0.11 0.95 -4 4 -9 0.27 0.64 -4 4 -9 -0.53 0.96 4 4 -9 0.27 1.13 4 4 9 0.35 0.95 4 4 -9 0.10 0.81 4 4 9 1.13 0.94 4 -4 -9 0.17 1.34 -4 4 -9 1.83 0.92 -4 4 -10 2.22 0.90 4 4 10 1.96 1.01 -4 4 -10 1.98 1.28 -4 4 10 1.92 0.97 -4 4 -10 1.80 1.58 4 -4 10 2.03 0.76 4 4 10 3.44 1.12 -4 4 10 2.44 1.01 4 4 10 3.61 1.31 4 -4 -10 3.22 1.12 4 4 10 2.94 1.30 -4 4 10 6.88 1.86 -4 4 10 2.81 1.31 4 -4 10 1.49 1.21 4 -4 -10 1.08 1.10 4 4 -10 2.56 0.84 4 4 -10 2.00 1.26 -4 -4 -10 2.92 1.15 4 -4 10 2.03 1.08 4 4 10 3.55 0.94 -4 -4 10 1.77 0.96 4 4 10 2.53 1.01 -4 -4 10 2.25 1.05 4 4 -10 3.80 1.42 -4 4 -10 3.10 1.47 -4 4 -10 2.65 0.62 4 -4 10 3.32 1.11 4 -4 10 3.06 1.10 4 -4 -10 12.35 1.65 4 4 -10 2.54 1.25 -4 -4 10 5.26 2.07 -4 4 10 4.05 1.16 -4 4 10 4.12 1.52 4 4 -10 2.17 1.42 4 4 -10 2.13 0.91 -4 -4 10 14.23 2.21 4 4 10 2.76 0.95 -4 -4 10 2.22 0.94 -4 -4 10 3.57 1.21 -4 4 -10 3.10 1.04 4 4 10 1.34 1.13 4 4 -10 2.43 0.76 4 4 10 0.93 0.97 -4 -4 10 2.73 1.06 4 -4 10 1.85 1.51 4 -4 10 3.91 1.15 4 4 -10 2.14 1.12 4 -4 -10 3.72 1.57 -4 4 10 12.41 1.79 -4 4 -10 3.08 0.89 4 4 -11 290.30 8.59 -4 4 -11 291.15 8.40 4 4 11 294.57 8.40 4 4 11 302.69 8.33 4 4 11 289.94 8.53 -4 4 11 295.41 8.60 4 -4 11 291.11 8.00 4 4 11 290.79 8.34 -4 4 11 289.87 8.37 -4 -4 11 307.96 8.74 4 4 -11 288.83 8.57 4 4 -11 296.78 8.48 -4 -4 11 299.41 8.41 -4 -4 11 296.44 8.81 4 4 -11 290.45 8.04 -4 4 -11 291.98 8.51 -4 4 -11 293.97 8.69 -4 -4 11 294.28 8.39 4 -4 11 302.43 8.77 4 -4 11 296.04 8.37 4 4 11 298.13 8.17 4 4 11 291.41 8.19 -4 4 -11 295.30 8.75 4 4 -11 291.91 8.06 4 -4 -11 308.94 8.58 4 -4 11 288.78 8.40 -4 4 11 303.04 8.38 4 4 11 286.41 8.44 -4 4 11 287.30 8.76 -4 -4 11 278.67 8.17 4 4 -11 296.46 8.32 4 4 -11 299.44 8.26 4 -4 -11 301.09 8.23 -4 -4 11 294.64 8.20 -4 4 11 291.99 8.40 -4 4 11 298.89 8.46 4 -4 -11 300.29 8.75 4 4 11 287.15 8.39 4 -4 11 303.24 8.34 -4 4 11 302.72 8.48 -4 4 -11 296.55 8.15 -4 -4 -11 299.56 8.27 4 4 -11 285.27 8.10 4 4 -12 2.06 0.88 -4 4 -12 1.10 0.90 4 -4 -12 2.02 1.35 -4 4 12 1.75 1.01 4 4 -12 0.71 1.33 4 -4 12 0.53 0.79 -4 4 12 1.07 1.39 -4 -4 12 0.44 1.08 4 4 12 2.00 0.98 -4 4 12 1.78 1.06 4 -4 12 1.20 1.11 -4 -4 12 2.29 0.94 4 4 12 0.43 1.33 -4 -4 12 0.57 1.49 -4 -4 12 -1.24 1.52 4 -4 12 2.77 1.53 4 4 12 2.49 1.11 4 4 12 1.41 0.94 4 4 12 0.92 1.06 4 -4 12 1.07 1.07 4 -4 12 2.17 1.02 -4 4 12 0.63 1.11 -4 4 12 2.86 1.65 -4 4 12 1.75 1.16 -4 -4 12 1.12 0.99 4 4 12 1.29 1.01 4 4 12 2.65 1.08 4 4 -12 0.89 1.09 -4 4 -12 1.45 1.52 -4 -4 12 0.56 1.00 4 4 -12 3.23 0.98 4 4 -12 1.59 0.80 4 -4 -12 1.51 1.01 4 4 12 1.33 1.13 4 4 -12 0.79 0.68 -4 -4 -12 1.94 1.50 -4 4 12 1.75 1.08 4 -4 -12 2.43 1.50 -4 4 -12 2.79 0.86 -4 -4 -12 2.27 1.25 -4 4 -13 53.22 2.40 4 4 -13 57.09 2.74 4 -4 13 56.91 2.19 4 4 13 63.61 2.82 4 4 13 58.41 2.49 -4 4 13 57.51 2.77 -4 -4 13 56.48 3.00 4 -4 13 56.78 2.91 4 4 13 60.26 2.39 4 -4 -13 68.00 2.99 4 4 13 59.69 2.38 4 4 -13 62.04 2.45 -4 4 -13 64.24 3.04 4 4 13 55.13 2.47 -4 4 13 57.71 2.94 4 -4 13 58.14 2.43 -4 4 13 55.42 2.54 -4 -4 -13 55.20 2.88 -4 -4 13 58.82 2.45 -4 -4 13 56.83 2.28 -4 4 13 62.57 2.55 -4 -4 13 62.74 3.11 4 4 13 59.44 2.53 4 4 13 58.86 2.49 4 4 -13 58.27 2.45 -4 -4 13 64.25 2.35 4 -4 -13 57.79 2.53 -4 4 13 63.24 2.52 4 -4 -13 59.57 3.00 4 -4 13 57.67 2.32 -4 4 -13 57.67 2.21 4 -4 13 56.48 2.98 4 4 -13 59.28 2.14 4 -4 13 62.23 2.56 -4 4 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133.37 4.97 -4 -4 15 141.41 4.57 -4 4 -15 125.81 4.29 4 -4 -15 144.51 5.08 4 -4 15 134.76 4.25 4 -4 16 125.56 4.79 4 4 16 127.68 4.33 4 4 -16 129.15 4.57 -4 4 -16 122.74 4.11 4 4 16 121.72 4.57 4 -4 -16 122.97 4.63 4 -4 -16 122.40 4.15 -4 -4 16 120.89 4.71 4 -4 16 133.23 4.91 4 4 16 124.65 4.13 -4 -4 16 123.15 4.13 4 -4 -16 127.67 4.32 4 -4 16 123.36 4.06 4 -4 16 113.80 3.91 -4 -4 -16 133.19 4.73 -4 4 16 130.01 4.82 -4 4 16 132.81 4.46 -4 4 16 122.75 4.14 4 4 16 124.40 4.46 -4 -4 16 133.31 4.83 4 4 16 116.74 4.33 -4 -4 16 128.50 4.37 4 -4 -16 128.61 4.88 4 -4 17 300.16 9.39 4 4 -17 296.64 9.10 4 -4 -17 313.18 9.28 4 4 17 303.47 9.21 4 -4 -17 301.29 8.83 4 -4 17 297.26 9.41 -4 -4 17 304.60 9.37 4 4 17 304.05 8.81 -4 4 -17 298.66 9.35 4 -4 17 289.99 8.56 -4 4 17 312.34 9.43 -4 4 17 304.38 8.98 4 4 17 298.13 9.06 -4 -4 17 312.41 9.40 4 4 17 292.84 8.96 -4 -4 17 304.83 8.95 -4 -4 -17 314.54 9.30 -4 4 -17 297.07 8.69 4 -4 -17 306.86 9.43 4 4 17 286.71 8.85 -4 4 -18 279.19 8.36 -4 -4 -18 284.32 8.89 4 4 18 288.37 8.46 -4 -4 18 292.03 9.05 -4 4 -18 281.04 9.02 4 -4 -18 267.79 8.39 4 4 -18 288.16 8.76 -4 4 18 280.89 9.01 4 4 18 282.83 8.75 4 4 18 297.19 8.69 -4 -4 18 291.83 9.04 -4 -4 18 280.80 8.59 -4 -4 -18 283.53 8.87 4 -4 -18 278.78 8.93 4 -4 -18 299.89 9.09 -4 4 18 288.75 8.63 4 4 18 287.77 8.55 4 -4 18 286.78 9.06 4 -4 18 287.90 9.07 -4 4 -19 79.01 3.19 -4 -4 -19 85.69 3.70 4 -4 -19 82.08 3.68 4 4 -19 80.86 3.59 -4 -4 19 81.72 3.83 4 4 19 77.53 3.22 -4 4 -19 74.03 3.79 -4 -4 19 77.10 3.92 -4 -4 -19 76.79 3.67 4 -4 19 87.20 3.90 -4 4 19 84.99 3.86 4 4 19 82.60 3.64 -4 4 19 78.52 3.45 4 -4 -19 79.00 3.78 4 4 19 84.66 3.49 -4 -4 19 79.19 3.46 4 4 19 80.24 3.14 4 4 19 71.29 3.27 4 -4 19 75.46 3.84 -4 -4 -20 68.02 3.41 4 -4 20 62.19 3.54 4 -4 -20 66.74 3.38 4 4 20 64.09 3.07 -4 -4 20 68.11 3.55 -4 4 -20 67.32 3.53 4 4 20 63.12 3.03 4 -4 20 65.00 3.49 4 4 20 59.65 2.81 -4 4 20 66.08 3.56 -4 4 20 62.47 3.14 4 4 20 65.35 3.29 -4 -4 20 60.38 3.09 -4 -4 20 73.46 3.67 4 -4 -20 65.29 3.46 -4 -4 -20 58.98 3.27 4 4 -20 63.68 3.20 -4 -4 -21 287.32 9.19 4 -4 -21 299.96 9.24 4 4 21 280.94 9.01 -4 -4 21 283.89 9.26 4 -4 21 301.93 9.41 4 4 21 280.03 8.62 -4 -4 -21 293.71 9.12 -4 4 -21 283.02 9.26 -4 4 21 296.40 9.36 -4 4 21 277.43 8.84 4 -4 21 281.72 9.32 4 4 21 285.54 8.94 -4 -4 21 285.32 8.92 -4 -4 21 297.68 9.38 4 4 -21 291.88 8.99 4 -4 -21 293.32 9.29 4 4 21 287.52 8.82 -4 -4 -22 101.41 4.51 4 -4 -22 99.65 4.49 -4 -4 -22 97.92 4.37 -4 4 -22 103.57 4.68 4 -4 22 107.57 4.74 4 4 22 104.53 4.44 4 4 -22 107.90 4.37 4 4 22 103.62 4.16 -4 4 22 98.80 4.60 -4 4 22 96.93 4.19 4 4 22 95.55 4.22 -4 -4 22 103.47 4.31 -4 -4 22 107.50 4.77 -4 -4 22 109.18 4.70 4 -4 -22 118.03 4.78 4 -4 22 109.95 4.82 -4 -4 -23 68.13 3.56 4 -4 -23 64.50 3.74 4 4 23 61.85 3.48 -4 -4 23 61.59 3.77 -4 -4 -23 60.46 3.50 4 -4 23 65.41 3.83 -4 4 -23 65.25 3.82 -4 4 23 66.64 3.78 -4 4 23 56.29 3.32 4 4 23 63.32 3.39 -4 -4 23 72.55 4.03 -4 -4 23 68.22 3.46 4 -4 -23 66.25 3.74 4 4 23 62.85 3.30 4 -4 23 70.87 3.93 4 4 -23 69.99 3.47 4 -4 -24 13.10 2.32 4 4 -24 15.59 2.14 4 -4 24 10.83 2.68 4 4 24 13.86 2.15 -4 -4 24 10.31 2.44 -4 -4 -24 12.85 2.38 -4 -4 24 12.40 2.58 -4 4 24 12.88 2.25 4 -4 24 12.32 2.58 -4 4 -24 11.83 2.52 -4 4 24 11.22 2.58 4 4 24 9.95 2.30 -4 -4 24 13.49 2.22 -4 -4 -24 17.46 2.33 4 -4 -24 17.02 2.59 4 4 24 12.20 2.18 4 4 -25 14.70 2.38 4 -4 25 12.47 2.82 -4 -4 -25 16.79 2.50 4 -4 -25 15.64 2.55 4 4 25 15.67 2.34 -4 -4 25 10.79 2.95 -4 -4 25 13.62 2.72 4 -4 25 15.71 2.70 -4 4 25 13.71 2.69 4 -4 -25 17.07 2.64 -4 4 -25 18.39 2.78 4 4 -25 9.81 2.41 4 4 25 16.76 2.48 -4 4 25 14.52 2.51 -4 -4 25 13.13 2.35 -4 -4 -25 12.78 2.39 4 4 25 13.81 2.40 4 -4 26 38.42 3.55 -4 4 -26 40.95 3.42 4 4 -26 45.51 3.34 4 -4 -26 46.31 3.38 -4 -4 -26 47.76 3.28 -4 -4 -26 46.76 3.37 -4 -4 26 44.17 3.31 4 -4 26 46.31 3.47 4 4 26 46.79 3.29 -4 -4 26 43.30 3.07 -4 4 26 53.58 3.60 -4 4 26 46.21 3.22 4 4 -26 45.18 3.11 4 4 26 41.74 3.07 -4 -4 26 44.06 3.53 4 -4 -26 47.36 3.49 4 4 26 41.92 3.06 -4 4 27 45.86 3.17 4 4 -27 48.48 3.52 4 4 -27 45.39 3.21 -4 -4 -27 40.64 3.38 -4 4 27 49.11 3.66 4 -4 -27 43.88 3.50 4 4 27 41.66 3.09 -4 -4 27 46.74 3.42 -4 -4 -27 49.58 3.26 4 -4 27 42.97 3.44 -4 -4 27 46.19 3.64 -4 4 -27 48.97 3.62 4 4 27 46.38 3.37 -4 -4 27 45.83 3.28 4 4 27 45.48 3.22 4 -4 -27 54.55 3.57 4 -4 27 46.92 3.67 4 4 -28 77.72 4.54 4 -4 -28 79.86 4.53 -4 -4 28 88.62 4.98 4 -4 28 96.76 4.80 -4 -4 28 92.39 4.96 -4 4 -28 96.49 4.79 -4 -4 -28 80.44 4.44 4 4 28 86.46 4.48 -4 4 28 78.32 4.64 -4 4 28 94.61 4.39 -4 -4 28 86.30 4.33 4 4 28 87.41 4.38 4 -4 28 78.82 4.49 4 -4 -28 89.39 4.61 4 -4 28 96.33 4.91 -4 -4 29 83.28 4.37 -4 -4 -29 82.19 4.53 -4 -4 29 89.14 4.72 4 -4 29 86.75 4.70 -4 4 -29 90.68 4.80 4 -4 -29 81.32 4.63 -4 -4 29 89.20 4.98 4 4 -29 81.51 4.49 -4 4 29 92.25 4.75 -4 4 29 78.82 4.23 4 4 29 81.42 4.27 4 -4 29 79.27 4.59 4 4 29 90.33 4.56 4 -4 -29 79.51 4.58 4 -4 29 86.50 4.79 4 4 -30 2.38 2.39 -4 -4 -30 1.76 2.41 4 -4 -30 -2.62 2.67 4 -4 -30 4.01 2.48 4 -4 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1.53 6 4 4 4.08 1.08 6 4 4 4.90 1.02 6 -4 -4 -2.14 1.80 6 -4 4 3.21 1.59 -6 4 4 1.13 1.55 6 -4 4 3.46 0.71 -6 4 -4 2.43 0.94 -6 4 4 3.28 1.07 6 -4 -4 1.90 1.18 -6 -4 4 2.86 1.14 6 -4 -5 8.79 1.83 -6 4 5 3.60 1.05 -6 4 5 4.13 1.20 -6 4 -5 3.02 0.58 6 -4 -5 4.53 0.96 -6 4 5 3.65 0.91 -6 -4 5 3.93 1.21 6 4 -5 4.49 1.45 -6 -4 5 4.04 1.01 6 4 5 1.74 1.29 -6 -4 -5 3.99 1.08 -6 -4 5 2.65 1.55 6 4 5 4.17 1.56 6 4 5 3.23 1.35 -6 4 5 4.24 1.16 -6 -4 -5 3.35 0.92 6 4 -5 3.40 1.13 -6 4 -5 4.89 1.61 -6 4 -5 5.09 1.11 -6 -4 5 3.85 0.54 6 4 -5 4.90 1.09 -6 -4 -5 3.06 1.33 6 -4 5 5.13 1.22 6 -4 5 7.59 1.70 6 4 5 4.26 0.72 -6 4 -5 5.96 1.50 -6 4 5 5.09 1.36 6 4 5 4.26 0.99 6 4 -5 5.02 1.33 -6 4 5 5.28 1.60 6 4 5 4.03 0.69 -6 -4 5 5.41 1.45 6 -4 -5 2.90 1.09 -6 -4 5 3.38 0.54 6 -4 -5 2.15 1.23 -6 -4 5 3.86 0.92 -6 4 5 3.73 0.87 6 -4 5 2.49 0.94 6 4 -5 5.22 1.40 -6 4 -5 5.56 1.03 6 -4 5 4.62 1.39 -6 4 -5 3.17 1.11 6 4 -5 2.97 0.94 6 4 -5 2.64 1.52 6 4 5 3.97 1.02 6 -4 5 5.34 0.65 -6 4 5 -2.81 1.89 6 -4 -5 1.31 2.08 6 -4 5 1.35 1.73 -6 4 -5 3.98 1.05 6 -4 -5 4.68 1.33 -6 4 6 162.28 4.94 6 4 6 161.81 4.91 -6 4 6 157.30 4.78 6 4 -6 156.06 5.35 -6 4 6 160.48 4.83 6 4 -6 161.86 5.33 6 4 6 166.75 5.17 6 4 -6 163.90 4.95 -6 -4 -6 166.41 4.79 6 4 6 165.32 5.32 -6 4 6 167.18 4.99 -6 -4 6 169.88 5.44 -6 -4 6 171.27 5.08 -6 4 -6 159.65 4.87 -6 4 -6 167.14 5.33 6 4 -6 164.47 4.97 6 -4 -6 159.13 5.52 -6 -4 -6 156.31 5.01 6 -4 6 161.18 5.41 6 4 6 157.14 4.58 6 -4 6 161.24 5.06 6 -4 -6 173.50 5.57 6 4 6 162.65 4.56 -6 4 -6 162.66 4.77 -6 -4 6 164.05 4.86 -6 4 -6 168.49 5.41 6 -4 -6 160.65 4.77 6 4 6 169.72 4.90 -6 4 6 168.04 5.15 6 -4 6 159.45 4.80 -6 -4 6 159.49 5.23 -6 4 6 165.73 5.43 6 -4 -6 162.06 4.95 6 4 -6 160.22 5.24 -6 -4 6 158.69 4.42 6 4 -6 167.79 5.14 6 4 -6 152.94 4.93 6 4 6 162.83 5.35 -6 4 6 163.23 4.99 6 -4 6 147.50 4.33 6 -4 6 157.60 5.32 6 -4 6 171.85 5.36 -6 4 6 150.31 5.16 6 -4 -6 172.48 5.26 -6 4 -6 158.64 5.00 6 4 -6 168.82 5.15 -6 4 7 212.49 6.44 -6 -4 7 220.92 6.61 -6 4 7 219.02 6.41 6 4 -7 222.50 6.98 6 4 7 221.83 6.39 6 4 7 228.71 6.76 6 -4 -7 215.72 6.29 6 4 7 230.37 6.73 6 4 -7 213.20 6.54 -6 4 7 218.97 6.56 6 4 7 224.33 6.89 -6 -4 7 221.59 6.99 6 4 -7 222.68 6.66 6 -4 7 230.71 6.93 -6 4 -7 225.01 6.50 -6 4 -7 218.80 6.96 6 4 -7 215.54 6.48 6 -4 7 224.54 6.91 -6 -4 -7 223.25 6.58 6 -4 7 215.73 6.61 6 4 7 225.11 6.19 -6 -4 7 218.91 6.44 6 4 7 218.81 6.44 6 -4 7 219.85 6.39 -6 4 7 217.53 6.67 6 4 -7 220.41 6.91 -6 4 7 219.46 6.97 -6 -4 7 213.32 6.81 6 4 7 219.89 6.50 -6 4 -7 223.57 6.91 6 -4 7 222.10 6.99 6 -4 -7 223.27 6.80 6 -4 -7 216.81 6.50 -6 -4 7 207.33 6.06 6 4 7 216.52 6.22 6 4 -7 221.89 6.82 -6 4 7 215.78 6.42 6 4 7 230.28 6.96 6 4 -7 222.19 6.50 -6 4 7 220.42 6.57 -6 4 -7 222.93 6.30 6 -4 -7 218.04 6.95 6 -4 7 219.92 6.82 -6 4 -7 217.77 6.55 6 4 -7 230.03 6.69 6 4 -8 13.81 1.42 -6 4 8 11.26 1.30 -6 4 8 12.32 1.15 6 4 8 12.29 1.27 -6 4 8 13.26 1.17 -6 -4 8 15.04 1.41 6 4 -8 13.23 1.62 -6 4 8 14.49 1.45 6 4 8 13.99 1.16 -6 4 8 12.83 1.17 6 4 8 12.28 1.54 6 -4 -8 11.38 1.01 -6 -4 8 11.24 1.71 6 4 8 11.72 1.63 6 4 8 13.37 1.09 6 -4 8 13.76 1.69 6 4 -8 13.49 1.49 6 4 -8 12.60 1.43 6 4 -8 13.14 1.20 -6 4 -8 12.63 1.34 -6 4 -8 13.13 1.84 6 -4 8 12.76 1.72 6 -4 -8 12.80 1.75 -6 -4 -8 14.74 1.55 6 4 8 11.78 1.03 6 4 8 8.42 1.66 6 4 -8 13.88 1.20 6 -4 -8 14.37 1.04 -6 4 -8 10.78 1.77 6 4 8 11.37 1.20 -6 -4 8 12.70 1.22 6 4 -8 14.75 1.65 -6 4 8 12.78 1.56 6 4 8 12.12 1.43 6 -4 8 12.01 1.22 -6 4 8 12.18 1.73 -6 -4 8 15.15 1.82 -6 -4 8 12.71 1.00 -6 4 -8 14.27 1.10 6 -4 8 15.78 1.80 6 -4 -8 13.71 1.30 6 4 -8 12.14 1.14 6 -4 8 14.88 1.59 -6 4 -8 13.35 1.30 6 -4 -8 14.89 1.68 -6 4 9 32.04 1.60 -6 4 9 32.42 1.94 -6 -4 9 31.39 1.80 -6 4 9 32.67 1.67 -6 4 9 31.79 1.69 6 -4 -9 34.35 2.21 6 4 9 32.02 2.01 6 4 -9 29.23 2.19 6 4 9 29.04 2.13 6 4 -9 29.14 1.56 -6 -4 9 31.17 2.29 6 4 -9 28.91 1.85 -6 4 -9 29.44 1.78 -6 -4 -9 30.67 1.94 6 -4 9 33.35 2.20 6 4 -9 29.39 1.62 -6 4 -9 31.85 2.32 -6 -4 9 30.80 1.68 6 4 9 31.68 1.53 -6 4 9 34.19 2.00 6 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1.38 -4 5 6 23.97 1.67 -4 5 6 24.38 1.97 -4 -5 6 28.30 2.13 4 -5 6 20.36 1.15 4 5 6 22.23 1.18 4 -5 -6 22.43 1.63 4 5 -6 22.51 1.15 4 5 -6 23.07 1.48 4 5 6 18.06 1.59 -4 5 6 22.71 1.15 -4 5 -6 21.54 1.56 4 5 6 19.54 1.68 -4 -5 -6 21.90 1.79 -4 -5 6 25.19 1.62 4 5 6 22.07 1.55 -4 5 -6 27.24 1.89 -4 5 -6 19.46 0.93 -4 5 6 23.59 1.49 4 5 -7 147.70 4.77 -4 5 -7 148.14 4.21 4 5 -7 141.39 4.89 4 -5 7 144.34 4.75 -4 -5 -7 145.41 4.48 -4 -5 7 145.27 4.63 4 -5 -7 142.66 4.51 4 -5 7 137.96 4.11 -4 -5 7 140.14 4.55 -4 5 -7 139.56 4.60 4 5 7 139.39 4.76 4 5 -7 137.20 4.44 -4 -5 7 162.82 5.07 4 5 7 140.68 4.83 4 5 -7 140.27 4.64 4 5 -7 133.43 4.68 -4 5 -7 141.64 4.69 -4 -5 -7 138.02 4.22 4 -5 7 144.28 4.74 -4 -5 -7 144.31 4.88 4 -5 7 141.29 4.48 4 5 7 139.30 4.15 4 5 -7 141.37 4.09 -4 5 -7 143.54 4.68 4 5 7 140.81 4.65 -4 -5 7 135.79 4.04 -4 5 -7 141.21 4.85 -4 -5 7 143.34 4.52 4 5 7 143.08 4.17 -4 5 7 138.53 4.32 4 -5 7 143.14 4.50 4 5 -7 139.16 4.36 4 5 7 143.16 4.62 4 -5 -7 181.46 5.48 4 5 -7 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2.98 4 5 8 63.41 2.35 -4 -5 -8 63.25 2.91 4 5 -8 65.40 2.30 4 5 8 63.85 2.75 -4 5 8 60.83 2.10 4 -5 -8 68.15 2.92 4 5 -8 67.03 2.44 -4 5 8 86.48 3.24 4 5 8 67.16 2.83 -4 5 8 64.56 2.63 4 -5 8 68.56 2.64 -4 5 8 64.92 2.86 -4 5 -9 23.70 1.59 4 -5 9 36.16 2.26 4 5 -9 40.57 2.23 4 5 9 38.68 1.95 -4 5 9 36.17 1.84 4 -5 9 36.33 1.54 -4 -5 9 34.99 1.90 4 5 9 33.63 2.23 -4 -5 -9 32.53 2.09 -4 -5 9 37.81 2.28 4 5 -9 35.09 2.19 -4 5 -9 37.57 2.14 -4 -5 -9 35.81 1.72 4 -5 9 34.17 1.87 -4 -5 -9 36.70 2.22 4 5 -9 32.75 1.59 4 5 9 36.86 1.66 -4 -5 9 38.70 1.91 -4 -5 9 34.14 1.52 4 -5 9 39.62 1.96 -4 5 -9 37.48 2.27 4 -5 -9 37.94 2.25 -4 5 9 33.20 1.76 -4 5 9 42.83 2.26 4 5 -9 35.91 1.72 -4 5 9 34.87 2.36 4 -5 9 40.24 2.32 4 5 -9 40.59 2.03 -4 5 9 38.83 2.17 4 -5 -9 34.60 2.25 -4 -5 9 38.32 2.13 4 5 9 36.99 1.71 4 -5 -9 36.95 1.67 4 5 -9 41.25 2.41 4 5 9 35.09 1.57 4 5 -9 35.37 1.61 -4 5 -9 34.58 2.22 -4 5 9 37.47 1.34 -4 5 -9 35.16 1.77 -4 5 9 32.27 1.82 4 5 9 34.75 2.05 -4 5 9 34.76 2.17 -4 5 10 179.82 5.93 4 5 10 176.43 5.64 -4 5 10 185.73 5.66 -4 -5 10 178.96 5.49 4 5 -10 186.78 5.92 -4 5 10 187.21 5.70 4 -5 10 174.47 5.72 4 -5 10 178.02 5.28 -4 -5 10 182.55 5.68 -4 -5 -10 185.39 5.97 4 5 10 187.15 6.00 -4 -5 10 195.84 6.11 4 5 -10 188.96 5.95 -4 5 -10 189.05 5.89 4 5 10 171.71 5.36 4 5 -10 180.26 5.67 -4 -5 -10 176.05 5.40 4 -5 -10 190.50 6.01 4 -5 10 181.87 6.00 4 -5 10 176.81 5.67 -4 -5 -10 190.04 6.01 4 5 -10 180.06 5.39 4 5 10 182.06 5.41 -4 -5 10 186.95 5.69 4 -5 -10 184.65 5.95 4 5 10 184.20 5.34 4 -5 10 188.21 5.69 -4 5 10 176.72 5.71 -4 -5 10 182.90 5.32 -4 5 -10 188.02 6.10 -4 5 10 188.21 5.72 -4 5 10 182.45 5.51 -4 5 10 181.83 6.08 4 5 -10 175.66 5.42 4 5 10 184.74 5.52 -4 -5 10 183.49 5.89 4 -5 -10 189.81 5.42 4 5 -10 192.38 5.67 -4 5 -10 193.22 5.52 4 5 10 186.58 5.91 4 5 -11 2.56 1.47 4 -5 11 2.08 0.84 4 5 -11 3.59 1.36 -4 5 -11 1.45 1.43 4 5 11 3.32 1.44 4 5 11 2.65 1.16 -4 5 11 3.53 1.46 4 5 11 2.69 1.46 4 -5 11 2.85 1.29 -4 5 11 5.11 1.28 -4 -5 11 6.77 1.90 4 5 -11 3.59 1.21 -4 -5 -11 4.62 1.16 4 -5 11 4.27 1.51 -4 -5 11 5.78 1.88 4 5 -11 4.90 1.09 -4 -5 -11 1.36 1.36 4 5 11 3.31 1.01 -4 -5 11 2.24 0.98 -4 -5 -11 3.46 1.38 4 5 11 1.68 1.02 -4 5 -11 1.70 1.64 4 -5 11 2.80 1.22 -4 5 11 2.40 1.13 -4 5 11 1.81 1.50 4 5 11 4.08 1.05 4 5 11 3.46 0.95 4 -5 -11 9.26 1.28 4 -5 -11 2.28 1.66 -4 5 -11 3.29 0.94 4 5 -11 3.18 0.92 4 -5 -11 6.79 1.90 4 5 12 158.22 5.18 4 5 -12 147.34 5.09 4 -5 12 157.65 5.29 -4 -5 12 134.80 5.32 4 -5 12 153.95 4.94 4 5 -12 152.49 5.18 -4 5 -12 149.92 5.14 4 -5 -12 145.88 5.12 4 -5 12 156.92 5.31 4 5 12 150.13 4.68 4 5 12 151.96 4.59 4 -5 -12 156.98 5.35 -4 5 -12 149.65 5.29 -4 -5 -12 151.35 5.16 -4 5 12 159.87 5.03 -4 5 12 149.38 4.78 -4 5 12 144.57 5.28 4 5 12 149.80 4.82 -4 -5 12 159.18 5.27 -4 5 12 150.99 5.22 4 5 12 147.15 4.69 4 5 -12 152.08 4.80 -4 -5 12 148.31 4.66 -4 5 -12 143.97 4.60 4 -5 13 2.69 1.63 -4 5 13 3.09 1.24 4 -5 13 2.42 1.19 4 5 13 0.71 1.39 -4 5 13 1.56 1.43 4 5 -13 0.83 1.44 -4 5 -13 2.19 1.41 -4 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5 25 60.00 3.40 -4 -5 25 56.84 3.34 -4 -5 -25 63.20 3.62 4 -5 25 56.09 3.88 4 5 -25 55.54 3.24 4 -5 26 0.56 2.51 4 -5 -26 0.91 2.30 4 -5 -26 5.40 2.47 -4 -5 26 4.18 2.39 4 5 26 0.17 2.23 4 -5 26 3.78 2.43 -4 5 -26 7.42 2.52 -4 -5 26 1.66 2.69 -4 5 26 3.16 2.41 4 5 26 3.49 1.83 4 5 26 1.47 2.06 -4 -5 26 4.05 2.06 -4 -5 -26 2.49 2.22 4 5 -27 16.86 2.82 4 -5 -27 20.66 2.91 -4 -5 -27 19.42 2.68 -4 -5 27 25.05 3.51 4 -5 27 21.98 2.96 4 5 27 17.73 2.58 -4 5 -27 22.25 2.95 -4 5 27 24.96 2.99 4 5 27 15.83 2.42 4 5 27 20.86 2.72 -4 -5 27 14.56 2.50 4 -5 27 19.14 2.99 -4 -5 27 15.88 3.37 4 -5 -27 23.44 2.90 4 -5 -28 15.54 2.97 -4 -5 28 20.19 3.24 -4 -5 28 18.82 2.98 4 -5 28 23.43 3.04 -4 5 -28 23.18 3.05 4 5 -28 19.29 2.90 4 -5 -28 19.58 2.93 -4 5 28 16.45 2.96 4 5 28 16.33 2.80 4 5 28 21.29 2.54 4 5 28 18.34 2.85 -4 -5 28 19.25 2.62 -4 -5 -28 22.35 2.75 4 -5 28 17.60 3.04 4 5 -29 33.81 3.06 4 -5 -29 30.51 3.29 -4 -5 -29 35.44 3.15 -4 -5 29 30.76 3.39 4 -5 29 29.44 3.27 4 5 29 31.29 3.15 -4 5 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2.10 5 5 -2 28.07 1.77 -5 5 -2 25.04 1.72 5 -5 -2 27.33 2.20 -5 -5 -2 26.25 1.54 5 -5 -2 25.16 1.47 -5 5 -2 27.65 2.08 5 -5 2 23.61 1.70 5 5 2 27.94 1.38 -5 5 2 25.06 2.02 -5 -5 2 26.19 1.67 5 -5 -2 26.08 1.71 -5 -5 2 27.89 1.57 5 5 -2 27.44 1.51 5 5 2 24.32 1.73 5 -5 2 22.72 1.52 5 5 -2 27.80 1.96 -5 5 2 22.97 1.69 -5 5 2 29.57 1.51 -5 5 2 27.81 1.87 -5 5 2 31.84 1.54 -5 5 -2 31.38 1.36 5 -5 -2 28.09 1.57 -5 5 3 146.16 4.62 -5 5 -3 154.93 4.74 5 -5 -3 149.75 4.50 5 -5 -3 145.18 5.08 5 5 -3 149.93 4.95 5 5 3 139.07 4.92 5 5 -3 147.51 4.94 -5 5 -3 137.76 4.15 5 5 3 146.13 4.87 -5 5 3 150.52 4.42 -5 -5 -3 136.34 4.59 5 5 3 144.47 4.90 -5 -5 3 142.81 4.65 -5 -5 3 142.24 4.87 5 5 3 144.04 4.54 5 5 -3 144.05 4.67 5 -5 3 149.70 4.97 -5 -5 -3 140.66 4.69 -5 5 -3 143.91 4.67 5 -5 3 135.35 4.60 5 5 3 142.66 3.93 5 5 -3 145.52 4.66 5 5 3 143.42 4.71 -5 5 -3 144.66 4.64 -5 5 -3 148.39 4.97 5 -5 -3 143.37 4.42 5 -5 -3 148.67 4.62 5 -5 3 140.19 4.69 5 5 3 149.93 4.34 -5 5 3 142.09 4.94 -5 -5 3 139.36 4.57 5 5 -3 142.60 4.57 5 -5 -3 139.87 4.68 -5 -5 3 142.98 4.49 5 5 3 144.42 3.94 5 5 3 144.20 4.63 5 -5 3 138.07 4.47 5 5 -3 146.42 4.47 -5 5 3 140.01 4.63 5 5 -3 146.02 4.84 -5 5 -3 137.75 4.59 5 -5 3 136.18 4.18 5 5 3 139.19 4.63 -5 5 3 144.50 4.85 -5 5 -3 128.65 4.55 -5 5 3 145.45 4.46 -5 -5 -3 146.67 4.47 -5 5 -3 139.85 4.18 5 5 -3 145.50 4.61 5 -5 -4 181.04 5.71 -5 5 4 173.38 5.16 -5 5 -4 169.90 5.27 -5 -5 -4 165.66 5.00 5 -5 -4 159.78 5.00 5 5 -4 161.99 5.45 5 5 -4 170.47 5.44 5 5 4 157.78 5.35 -5 -5 -4 162.05 5.13 -5 -5 4 153.08 5.16 5 5 4 168.59 5.50 5 5 4 164.19 5.06 5 5 -4 162.58 5.24 5 5 4 167.55 5.20 5 -5 4 174.71 5.55 -5 5 -4 168.87 5.23 5 -5 4 165.36 5.23 5 5 -4 165.15 5.19 5 5 4 161.41 4.52 -5 5 -4 162.93 5.15 5 -5 4 166.84 5.05 -5 -5 -4 162.58 4.92 5 5 -4 167.82 5.13 5 5 4 161.03 5.21 5 -5 -4 163.33 5.16 -5 5 -4 165.48 5.50 5 5 4 158.64 4.82 5 -5 4 158.79 5.22 5 -5 -4 163.06 4.92 -5 5 4 166.45 5.49 -5 -5 4 161.29 5.02 -5 -5 4 164.26 5.16 -5 -5 4 164.19 5.47 5 -5 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5 7 98.62 3.39 -5 5 7 100.24 3.46 5 5 -7 97.40 3.85 5 5 -7 102.82 3.93 -5 -5 -7 99.57 3.40 5 5 7 97.16 3.78 5 -5 7 94.99 3.00 5 5 -7 96.92 3.63 -5 5 7 101.42 3.69 5 -5 -7 103.42 3.96 -5 -5 7 102.04 3.94 -5 5 -7 99.80 3.60 5 5 -7 101.16 3.41 -5 5 -7 98.21 3.75 5 -5 -7 102.81 3.47 5 -5 7 103.83 3.80 -5 -5 -7 102.54 3.37 5 -5 7 105.87 3.89 5 -5 7 97.52 3.50 5 5 7 99.49 3.11 5 5 7 104.80 3.93 5 5 -7 100.48 3.46 -5 5 -7 100.43 3.91 -5 -5 7 103.14 3.48 5 5 7 101.90 3.25 -5 5 7 102.98 3.47 5 -5 7 95.67 3.44 -5 5 7 104.90 3.98 5 -5 -7 101.17 3.33 -5 -5 7 102.17 3.70 5 5 7 98.72 3.15 -5 -5 7 100.16 2.99 5 5 -7 99.31 3.51 5 5 7 97.74 3.61 5 5 -7 104.98 3.20 5 -5 -7 98.33 3.71 5 -5 7 107.67 3.83 -5 5 -7 98.48 3.46 -5 5 7 95.35 3.46 -5 5 8 9.17 1.21 -5 5 8 10.61 1.16 5 5 8 10.38 1.39 -5 5 8 9.98 1.12 -5 5 8 7.60 1.42 5 5 -8 13.35 1.79 -5 5 8 9.14 1.21 5 5 -8 9.07 1.64 5 5 8 9.76 1.01 5 -5 8 9.15 0.84 -5 -5 8 15.91 1.83 5 5 -8 12.15 1.18 5 5 8 9.65 1.68 5 -5 8 11.50 1.53 -5 5 -8 9.84 1.76 5 5 -8 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5 -11 168.29 5.90 -5 5 -11 168.10 5.60 5 5 11 169.64 5.29 -5 5 11 176.65 5.44 -5 -5 -11 172.53 5.32 5 -5 -11 180.35 5.78 -5 5 11 167.65 5.87 -5 -5 11 169.91 5.76 5 5 11 174.41 5.40 5 -5 -11 173.51 5.26 5 5 -11 179.77 5.26 -5 -5 11 174.83 5.16 5 5 -11 174.36 5.51 -5 -5 11 175.83 5.35 5 5 -11 166.73 5.65 5 -5 -11 177.86 5.88 5 -5 11 173.75 5.51 -5 5 -11 167.88 5.26 5 5 11 170.83 5.62 5 5 -12 3.20 1.04 -5 -5 12 2.56 1.04 5 5 -12 0.52 1.49 5 -5 -12 2.80 1.39 5 5 12 2.20 1.34 5 -5 12 1.49 1.17 -5 5 12 1.10 1.38 5 5 12 2.53 1.50 -5 -5 12 0.24 1.61 5 5 -12 4.67 1.50 5 5 12 2.66 1.53 -5 5 -12 2.45 1.70 -5 -5 -12 2.08 1.26 5 -5 12 2.54 1.65 5 5 12 0.49 0.93 5 5 12 3.10 1.05 -5 5 -12 2.36 1.64 -5 -5 12 3.22 1.07 -5 5 12 2.75 1.28 -5 5 12 3.41 1.61 5 5 -12 1.98 1.27 5 5 -12 1.25 0.94 -5 -5 12 0.11 1.60 5 -5 12 1.81 1.17 -5 5 -12 1.88 1.39 5 -5 -12 3.62 1.59 5 5 -13 8.05 1.14 5 -5 -13 9.17 1.58 5 5 -13 7.64 1.61 5 5 13 7.40 1.49 5 5 13 5.54 1.61 -5 5 13 7.00 1.60 -5 -5 13 8.94 1.85 -5 5 -13 7.08 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2.78 1.57 -5 -5 19 4.66 2.06 5 5 19 5.06 1.78 -5 -5 19 4.36 2.07 -5 5 19 4.07 1.92 5 -5 19 7.21 2.02 5 5 -19 3.03 1.73 -5 5 19 5.42 2.08 -5 5 19 6.11 1.65 5 5 19 3.02 1.36 -5 -5 19 2.46 1.42 5 -5 -19 4.70 2.08 5 5 -20 55.30 3.15 5 5 20 56.32 3.22 -5 5 20 52.60 3.26 -5 -5 -20 56.75 3.33 -5 -5 20 57.06 3.44 5 -5 20 55.01 3.35 -5 5 -20 54.71 3.48 -5 -5 20 49.34 3.42 -5 5 20 57.75 2.93 -5 5 20 47.68 3.35 5 5 20 56.14 3.03 5 5 20 56.56 2.88 -5 -5 20 53.48 2.84 5 -5 -20 55.85 3.39 5 5 20 53.27 2.76 5 -5 20 61.40 3.54 5 5 -21 18.01 2.31 5 -5 21 13.14 2.41 5 5 21 11.69 2.31 5 -5 -21 17.43 2.47 -5 5 21 13.07 2.37 5 -5 21 14.00 2.37 -5 5 21 14.97 2.04 -5 5 -21 8.09 2.45 -5 5 21 10.32 2.31 5 5 21 14.70 1.90 5 5 21 13.91 1.99 -5 -5 21 14.96 2.73 -5 -5 21 17.53 2.04 -5 -5 -21 16.49 2.35 -5 -5 21 14.73 2.64 -5 5 22 82.76 4.01 -5 -5 22 73.43 4.14 5 5 22 81.61 4.02 -5 -5 22 75.30 4.18 5 -5 22 84.74 4.21 -5 5 -22 83.34 4.25 -5 5 22 72.68 3.58 -5 5 22 73.95 4.17 5 5 22 80.16 3.61 -5 -5 22 79.61 3.65 -5 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6 2 59.48 2.76 0 -6 2 58.20 2.51 0 -6 -2 59.85 2.64 0 6 -2 61.91 2.37 0 6 2 57.42 2.41 0 -6 2 60.42 2.06 0 -6 2 66.23 2.74 0 -6 -2 59.18 2.53 0 6 -3 1122.76 29.76 0 -6 3 1118.15 29.61 0 6 3 1127.17 29.83 0 6 -3 1111.55 29.57 0 -6 -3 1115.63 29.23 0 6 3 1116.76 29.64 0 -6 3 1146.18 29.61 0 6 3 1077.02 29.20 0 -6 3 1080.83 29.23 0 6 -3 1123.63 29.49 0 6 -3 1137.65 29.66 0 6 -3 1147.33 29.93 0 6 -3 1081.46 29.54 0 6 3 1132.98 29.73 0 6 -3 1110.19 29.50 0 -6 3 1110.82 29.46 0 6 3 1111.31 29.58 0 -6 3 1149.60 29.73 0 -6 -3 1116.55 29.48 0 -6 -3 1159.28 29.85 0 6 3 1164.72 29.93 0 -6 -3 1140.43 29.93 0 -6 3 1107.66 29.29 0 -6 3 1155.19 29.81 0 -6 -3 1140.88 29.71 0 6 -4 2021.53 52.71 0 -6 4 2015.18 52.56 0 6 4 2051.37 52.81 0 -6 -4 2038.79 52.88 0 6 -4 2002.29 52.51 0 6 4 2028.75 52.69 0 -6 4 2008.49 52.61 0 6 4 1905.03 52.10 0 6 -4 2061.60 52.51 0 6 -4 2019.08 52.58 0 -6 -4 2009.12 52.13 0 6 -4 2041.67 52.87 0 6 -4 1974.42 52.52 0 6 4 1994.46 52.62 0 -6 4 2000.61 52.43 0 -6 4 2027.01 52.68 0 6 4 2006.05 52.56 0 -6 -4 2000.70 52.45 0 6 4 1994.74 52.88 0 -6 -4 2142.67 52.86 0 -6 4 2016.76 52.32 0 -6 4 2077.33 52.74 0 -6 -4 1996.04 52.66 0 -6 -5 74.90 2.77 0 6 -5 73.93 2.88 0 -6 5 75.24 2.68 0 6 -5 73.70 2.58 0 6 5 76.31 3.03 0 -6 -5 70.86 2.10 0 6 5 70.72 2.78 0 -6 5 73.31 2.81 0 6 5 67.27 2.08 0 6 -5 73.57 2.62 0 6 -5 68.87 2.59 0 6 -5 73.94 3.03 0 6 -5 69.04 2.64 0 -6 5 71.59 2.52 0 -6 5 75.83 2.80 0 6 5 67.03 2.66 0 -6 -5 72.42 2.53 0 -6 -5 77.30 3.14 0 6 5 70.85 3.06 0 -6 -5 75.06 3.02 0 -6 5 82.88 2.90 0 -6 5 72.21 2.49 0 -6 -6 27.99 2.00 0 -6 6 25.78 1.63 0 6 -6 27.03 1.56 0 -6 -6 23.72 1.68 0 6 6 26.19 1.93 0 6 6 27.53 1.74 0 -6 6 26.76 1.43 0 6 6 24.45 1.01 0 -6 6 23.66 1.81 0 6 -6 26.08 1.60 0 6 -6 27.71 1.59 0 6 -6 24.23 1.68 0 6 -6 29.23 1.99 0 -6 6 26.46 1.50 0 -6 6 28.77 1.73 0 6 6 27.66 1.73 0 6 -6 26.68 1.87 0 -6 -6 23.79 1.51 0 -6 -6 31.36 1.96 0 -6 6 29.56 1.80 0 -6 6 26.22 1.57 0 6 6 26.89 2.07 0 -6 -7 90.90 3.32 0 6 -7 84.95 3.35 0 -6 7 93.13 3.23 0 6 -7 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3.29 0.71 -4 -6 -5 2.64 0.88 4 -6 5 3.09 1.06 -4 -6 5 2.00 1.32 -4 -6 -5 2.22 1.51 4 6 -5 3.96 1.43 -4 6 -5 3.94 1.44 -4 6 -5 5.15 1.55 4 -6 5 5.37 1.73 -4 6 5 1.48 1.47 4 6 5 3.50 0.73 4 -6 -5 2.25 0.83 4 6 5 2.65 0.76 -4 -6 5 1.56 1.12 -4 -6 5 1.98 0.99 4 6 5 3.66 0.49 4 -6 5 2.37 1.12 -4 6 -5 1.88 1.05 4 6 -5 3.04 1.21 -4 6 -5 1.13 1.12 -4 -6 5 1.56 1.15 -4 -6 -5 4.95 1.35 4 -6 -5 1.90 1.30 4 6 5 3.74 1.37 -4 6 -5 3.23 1.09 -4 6 5 3.36 1.42 -4 6 5 2.45 0.83 -4 6 5 3.60 0.99 4 6 -5 3.19 1.05 4 6 -6 37.31 2.07 4 -6 -6 34.90 1.91 4 6 -6 35.13 2.34 -4 6 -6 33.77 1.67 4 6 -6 32.89 2.15 4 6 6 34.05 2.24 4 6 6 32.24 1.65 -4 -6 6 36.37 2.28 -4 6 6 35.91 2.17 -4 6 -6 30.04 1.37 4 6 6 34.45 2.35 -4 -6 -6 41.17 2.27 -4 6 -6 36.90 2.08 4 -6 6 36.60 2.10 4 -6 -6 33.11 1.32 4 6 -6 32.95 2.14 -4 -6 -6 32.86 1.54 -4 -6 6 37.92 2.08 -4 -6 -6 40.56 2.41 -4 6 -6 35.87 2.15 4 -6 6 34.70 1.80 4 6 -6 34.44 1.45 4 -6 -6 38.83 2.35 -4 6 -6 33.41 2.23 4 6 6 34.56 1.45 -4 -6 -6 35.34 1.85 -4 -6 6 39.96 1.99 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6 -6 -4 81.02 3.68 -6 6 4 82.96 2.97 -6 6 5 1.14 1.00 6 6 -5 1.23 1.56 6 6 -5 1.79 1.52 6 6 5 0.21 1.53 6 6 -5 -0.50 1.41 -6 -6 -5 -0.28 0.97 -6 -6 5 -0.22 1.48 6 6 5 -0.07 1.06 6 6 5 0.68 1.63 6 -6 -5 -0.71 1.05 6 -6 -5 0.97 1.27 6 -6 5 1.43 1.62 6 -6 5 -0.09 1.32 -6 6 -5 2.13 1.54 6 -6 5 0.28 1.06 6 6 -5 1.83 1.43 -6 6 5 -1.05 1.30 -6 -6 -5 -0.49 1.20 6 -6 5 0.73 1.12 6 6 -5 0.14 1.11 -6 6 -5 0.84 1.31 -6 6 -5 0.23 1.62 -6 6 5 -0.12 1.53 -6 -6 5 1.08 1.30 6 -6 -5 -2.44 1.85 -6 -6 5 1.32 1.04 6 6 5 -0.46 1.70 6 6 5 1.89 1.36 -6 6 5 -0.17 0.80 6 6 -6 2.29 1.45 -6 -6 6 1.65 1.03 6 6 -6 -0.11 1.70 6 6 -6 4.16 1.64 6 6 6 1.84 1.60 -6 -6 6 0.23 1.56 -6 -6 -6 2.06 1.04 6 6 6 1.50 1.65 6 -6 -6 0.94 1.07 -6 6 -6 3.04 1.62 6 -6 6 1.86 1.43 6 -6 6 3.73 1.62 6 6 -6 -0.09 1.34 -6 -6 -6 0.79 1.17 -6 6 -6 0.09 1.29 -6 6 -6 1.76 1.56 -6 6 6 3.06 1.69 6 -6 -6 -0.23 1.77 -6 -6 6 2.01 1.38 6 -6 6 0.14 1.13 6 6 -6 1.80 1.13 6 6 6 2.64 1.31 6 -6 -6 1.59 1.34 6 6 6 0.52 1.03 -6 6 6 0.27 1.34 -6 6 7 155.39 4.78 6 6 -7 151.15 5.36 6 6 -7 156.98 5.43 -6 -6 -7 150.45 4.80 6 6 7 163.95 5.41 6 6 7 148.23 5.42 6 -6 7 150.65 5.31 -6 -6 7 159.88 5.44 6 6 -7 147.75 5.09 -6 6 -7 152.60 5.21 -6 6 -7 151.50 5.05 6 -6 7 150.53 5.21 -6 -6 -7 146.29 4.73 -6 6 -7 145.11 5.37 -6 6 7 148.90 4.87 6 -6 7 151.56 4.85 -6 6 7 148.71 5.45 -6 -6 7 148.26 5.10 6 6 7 150.75 4.85 6 -6 -7 147.67 5.41 6 6 7 151.75 5.09 6 6 -7 149.49 5.17 6 -6 -7 150.42 5.17 -6 6 7 152.03 5.13 -6 6 8 177.74 5.59 6 6 -8 180.44 6.13 6 6 -8 192.48 6.32 -6 -6 -8 182.60 5.63 6 6 8 185.65 6.19 6 -6 8 170.07 6.02 6 6 8 190.50 6.31 -6 -6 8 179.75 6.22 6 6 -8 183.82 5.95 -6 6 -8 176.45 5.85 -6 6 -8 191.95 6.09 6 -6 8 185.84 6.12 -6 -6 -8 176.23 5.54 6 6 -8 180.46 5.64 -6 6 -8 172.03 6.18 -6 6 8 186.20 5.71 6 -6 8 184.46 5.69 -6 6 8 190.18 6.33 -6 -6 8 180.59 5.96 6 -6 -8 179.22 6.19 6 6 8 189.36 5.95 -6 6 8 182.47 5.96 6 -6 -8 185.49 6.06 6 6 9 3.74 1.38 -6 6 9 2.94 1.05 -6 6 9 0.60 1.52 6 6 -9 1.70 1.78 6 6 -9 1.28 1.56 6 6 9 2.27 1.62 -6 -6 9 2.09 1.59 6 6 9 0.97 1.51 -6 6 -9 2.92 1.70 6 6 -9 2.26 1.45 6 -6 9 3.04 1.57 -6 6 -9 3.35 1.42 6 -6 -9 0.71 1.57 -6 -6 -9 4.37 1.28 6 -6 9 3.02 1.48 -6 6 -9 3.75 1.83 -6 6 9 1.54 1.23 -6 6 9 2.75 1.74 -6 -6 9 -0.70 1.45 6 -6 -9 1.64 1.55 6 6 10 0.20 1.40 -6 6 10 -0.41 1.46 6 6 -10 -0.59 1.58 6 6 10 0.93 1.51 -6 -6 10 0.51 1.55 6 6 10 -0.49 1.61 6 -6 -10 1.07 1.61 -6 6 -10 0.65 1.71 6 6 -10 -0.10 1.44 -6 6 -10 -0.87 1.42 6 -6 10 0.35 1.51 -6 -6 -10 1.66 1.25 6 -6 10 -0.54 1.39 -6 6 -10 0.13 1.63 -6 6 10 1.11 1.22 6 6 -10 0.37 1.74 -6 6 10 0.26 1.60 -6 -6 10 2.21 1.55 6 6 10 0.18 0.96 6 6 -10 2.70 1.43 6 -6 -10 1.15 1.48 6 6 11 -1.03 1.46 -6 6 11 0.96 1.51 6 6 -11 0.72 1.64 6 -6 -11 -0.72 1.56 6 6 11 -2.25 1.58 -6 -6 11 1.18 1.74 6 6 11 1.63 1.61 6 6 -11 0.42 1.55 -6 6 -11 0.91 1.73 -6 6 -11 1.70 1.49 6 -6 11 0.49 1.57 6 -6 11 1.71 1.42 -6 6 -11 1.05 1.75 -6 6 11 1.06 1.20 -6 6 11 0.39 1.65 -6 -6 11 -0.88 1.56 6 6 11 0.33 0.98 6 6 -11 2.50 1.41 6 -6 -11 0.36 1.51 6 6 -12 2.29 1.21 6 6 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33.49 3.22 11 -6 8 34.44 2.93 11 -6 -8 32.50 2.69 11 6 -8 35.15 2.88 11 6 9 10.53 2.59 11 6 -9 9.40 2.64 11 6 9 7.67 2.05 11 6 9 9.18 2.33 11 -6 9 14.31 2.42 11 -6 9 15.58 2.58 -11 6 -9 10.69 2.74 11 -6 9 5.83 2.37 -11 6 -9 15.48 2.65 11 -6 -9 10.42 2.73 -11 6 9 10.77 2.57 -11 -6 9 8.72 2.41 11 6 -9 7.71 2.12 11 6 -9 9.31 2.57 11 6 9 9.78 2.59 11 -6 -9 3.57 2.04 11 6 -9 10.39 2.15 11 6 -10 92.45 4.66 11 6 10 93.93 4.25 11 6 10 87.25 4.44 11 -6 -10 94.17 4.88 -11 6 -10 94.96 4.76 11 -6 10 90.26 4.55 -11 6 -10 103.91 4.79 -11 6 10 96.18 4.40 -11 -6 10 102.86 4.75 11 -6 10 106.78 4.67 -11 6 10 92.71 4.72 11 6 -10 94.06 4.31 11 6 -10 97.04 4.64 11 6 10 98.20 4.74 11 -6 -10 103.79 4.50 11 6 -10 94.58 4.31 11 -6 10 109.02 4.81 11 6 10 95.35 4.69 11 -6 -11 246.87 8.60 11 6 11 247.09 8.37 -11 6 -11 255.17 8.63 11 -6 11 233.29 8.38 -11 6 -11 254.94 8.65 -11 6 11 244.44 8.24 -11 -6 11 239.89 8.43 -11 6 11 253.02 8.60 11 6 -11 234.12 8.02 11 6 -11 247.76 8.43 11 6 11 244.56 8.55 11 6 -11 249.90 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-1.73 3.49 -3 19 9 -0.87 3.42 3 -19 -9 -1.18 3.51 -3 -19 -9 1.45 3.14 3 19 10 -1.98 3.44 3 19 -10 -3.73 3.57 -3 19 -10 -0.29 3.41 -3 -19 -10 -2.05 3.45 3 19 10 2.03 3.40 -3 19 10 0.29 3.36 3 -19 -10 -6.82 3.61 -3 -19 -10 -0.88 3.10 3 19 11 2.27 3.43 3 19 11 0.27 3.13 3 19 -11 -2.59 3.32 -3 19 -11 -2.57 3.41 -3 -19 -11 -2.36 3.54 3 19 11 -0.58 3.49 -3 19 11 -0.29 3.37 3 -19 -11 -4.16 3.64 -3 -19 -11 -0.29 3.31 3 19 12 8.87 3.74 3 19 12 1.37 3.37 -3 19 -12 -0.29 3.35 3 19 13 29.67 4.06 3 19 14 -4.49 3.47 4 19 0 122.20 6.38 -4 -19 0 100.76 6.11 4 19 0 121.90 6.48 -4 19 0 108.32 6.23 4 -19 0 100.68 6.23 -4 -19 0 105.28 5.93 4 19 -1 -0.82 3.28 4 19 1 4.13 3.31 -4 -19 1 0.27 3.25 4 19 -1 0.56 3.30 -4 -19 -1 8.34 3.54 -4 19 -1 4.78 3.48 4 19 1 0.28 3.44 -4 19 1 -1.41 3.46 -4 -19 1 3.48 3.08 -4 -19 -1 4.92 3.21 4 -19 -1 -3.71 3.43 4 -19 1 1.69 3.31 4 19 -2 -0.55 3.33 4 19 2 3.87 3.30 4 19 -2 -2.54 3.52 -4 -19 2 -2.70 3.29 -4 19 -2 0.56 3.45 -4 -19 -2 -1.12 3.46 4 19 2 6.22 3.51 -4 19 2 1.13 3.30 -4 -19 2 0.53 3.00 -4 -19 -2 -3.59 3.25 4 -19 -2 -2.58 3.57 4 -19 2 -0.28 3.40 4 19 -3 11.45 3.55 4 19 3 11.09 3.50 4 19 -3 10.17 3.59 -4 19 -3 7.59 3.50 -4 -19 3 4.81 3.25 -4 -19 -3 8.75 3.57 4 19 3 15.00 3.72 -4 19 3 9.33 3.78 -4 -19 -3 10.32 3.41 4 -19 -3 6.65 3.63 4 -19 3 10.80 3.59 4 19 -4 5.99 3.46 4 19 4 4.45 3.59 4 19 -4 -5.93 3.48 -4 19 -4 1.69 3.57 -4 -19 -4 1.42 3.38 4 19 4 2.55 3.41 -4 19 4 2.55 3.27 -4 -19 -4 -2.81 3.27 4 -19 -4 -0.29 3.54 4 -19 4 2.75 3.29 4 19 -5 3.26 3.28 4 19 5 1.68 3.35 4 19 -5 6.78 3.48 -4 19 -5 1.12 3.37 -4 -19 -5 -3.44 3.32 4 19 5 1.71 3.39 -4 19 5 4.55 3.41 -4 -19 -5 5.39 3.17 4 -19 -5 -0.58 3.65 4 -19 5 -4.35 3.36 4 19 -6 -1.08 3.30 4 19 6 -5.62 3.52 4 19 -6 -1.98 3.50 -4 19 -6 -3.09 3.55 -4 -19 -6 3.46 3.32 4 19 6 2.85 3.41 -4 19 6 -1.14 3.59 -4 -19 -6 -2.00 3.22 4 -19 -6 1.47 3.42 4 19 -7 -2.44 3.29 4 19 7 -3.11 3.62 4 19 -7 -0.85 3.44 -4 19 -7 -1.41 3.63 -4 -19 -7 1.74 3.29 4 19 7 -3.14 3.46 -4 19 7 -0.86 3.50 -4 -19 -7 -3.75 3.15 4 -19 -7 -2.95 3.56 4 19 -8 5.68 3.39 4 19 8 -0.28 3.60 4 19 -8 -4.55 3.48 -4 19 -8 2.25 3.36 -4 -19 -8 2.33 3.26 4 19 8 -1.15 3.51 -4 19 8 4.30 3.46 -4 -19 -8 0.87 3.03 4 -19 -8 5.92 3.40 4 19 -9 0.27 3.38 4 19 9 2.28 3.47 4 19 9 0.54 3.12 4 19 -9 5.98 3.52 -4 19 -9 4.51 3.50 -4 -19 -9 2.34 3.42 4 19 9 4.30 3.55 -4 19 9 -1.44 3.53 -4 -19 -9 6.14 3.15 4 -19 -9 5.94 3.55 4 19 -10 26.70 3.93 4 19 10 20.10 3.94 4 19 10 17.71 3.75 4 19 -10 26.55 4.18 -4 19 -10 21.48 4.02 4 19 10 23.87 4.07 -4 19 10 22.21 4.06 4 19 -11 41.24 4.39 4 19 11 30.85 4.35 4 19 -11 33.77 4.36 -4 19 -11 40.22 4.49 4 19 11 43.00 4.67 -4 19 11 41.99 4.59 4 19 12 26.45 4.01 4 19 13 6.47 3.48 5 -19 0 -2.29 3.59 5 19 0 1.96 3.51 -5 -19 0 -0.55 3.32 5 19 0 -1.40 3.45 -5 19 0 3.90 3.57 -5 -19 0 4.90 3.24 5 -19 -1 13.26 3.75 5 -19 1 10.81 3.66 5 19 -1 17.36 3.83 5 19 1 18.56 4.02 -5 -19 1 18.85 3.75 -5 -19 -1 20.05 3.81 5 19 -1 13.44 3.82 -5 19 -1 22.01 3.99 5 19 1 15.12 3.85 -5 19 1 14.25 3.86 -5 -19 1 17.23 3.45 -5 -19 -1 16.50 3.52 5 -19 -2 33.36 4.31 5 -19 2 29.93 4.21 5 19 -2 30.46 4.16 5 19 2 36.59 4.40 -5 -19 2 33.01 4.04 -5 -19 -2 33.13 4.13 5 19 -2 42.57 4.49 -5 19 -2 33.40 4.33 5 19 2 30.56 4.31 -5 19 2 35.83 4.32 -5 -19 -2 28.61 3.87 5 -19 -3 13.72 3.80 5 -19 3 22.98 3.97 5 19 -3 14.79 3.90 5 19 3 18.37 3.92 -5 -19 3 22.49 3.71 -5 -19 -3 18.40 3.81 5 19 -3 10.09 3.72 -5 19 -3 11.97 3.54 5 19 3 20.22 3.81 -5 19 3 12.34 3.65 -5 -19 -3 12.62 3.39 5 -19 -4 6.75 3.55 5 -19 4 5.28 3.40 5 19 -4 12.53 3.62 5 19 4 8.79 3.59 -5 -19 -4 15.40 3.71 5 19 -4 8.13 3.69 -5 19 -4 5.29 3.41 5 19 4 6.47 3.63 -5 19 4 4.22 3.52 -5 -19 -4 10.19 3.22 5 -19 -5 1.18 3.52 5 -19 5 0.55 3.22 5 19 -5 3.62 3.40 5 19 5 -2.27 3.47 5 19 -5 -3.08 3.52 -5 -19 -5 6.32 3.67 -5 19 -5 -1.67 3.43 5 19 5 1.97 3.45 -5 19 5 -0.28 3.50 -5 -19 -5 2.00 2.99 5 -19 -6 -0.89 3.37 5 -19 6 5.18 3.28 5 19 -6 0.28 3.34 5 19 6 4.86 3.45 5 19 -6 0.28 3.43 -5 19 -6 -2.50 3.59 -5 -19 -6 0.29 3.25 5 19 6 1.41 3.36 -5 19 6 -3.68 3.60 -5 -19 -6 1.73 3.03 5 19 -7 0.28 3.35 5 19 7 -0.29 3.58 5 19 7 1.34 3.25 5 19 -7 2.81 3.54 -5 19 -7 -2.23 3.45 -5 -19 -7 4.07 3.29 5 19 7 -2.83 3.62 -5 19 7 -1.42 3.60 -5 -19 -7 6.96 3.24 5 -19 -7 1.49 3.38 5 19 -8 11.65 3.73 5 19 8 5.20 3.60 5 19 8 4.35 3.44 5 19 -8 4.23 3.51 -5 19 -8 5.02 3.40 5 19 8 10.22 3.71 -5 19 8 10.80 3.55 -5 -19 -8 11.09 3.40 5 19 -9 26.32 4.02 5 19 9 18.15 3.85 5 19 -9 25.72 4.03 -5 19 -9 15.37 3.77 5 19 9 22.19 3.99 -5 19 9 26.23 4.03 5 19 -10 16.32 3.72 5 19 10 16.39 3.68 5 19 -10 13.31 3.76 -5 19 -10 17.63 3.85 5 19 10 14.56 3.83 -5 19 10 16.03 3.92 5 19 -11 4.98 3.49 5 19 11 2.80 3.26 6 19 0 81.50 5.51 -6 -19 0 68.59 5.18 6 19 0 82.86 5.47 -6 19 0 75.02 5.47 -6 -19 0 72.80 5.03 6 -19 -1 8.16 3.64 6 -19 1 11.23 3.82 6 19 -1 11.42 3.90 6 19 1 8.88 3.67 -6 -19 1 12.32 3.54 -6 -19 -1 10.05 3.60 6 19 -1 9.15 3.69 -6 19 -1 9.92 3.67 6 19 1 7.21 3.60 -6 19 1 9.67 3.64 -6 -19 1 9.19 3.16 -6 -19 -1 10.51 3.32 6 -19 -2 6.45 3.69 6 -19 2 6.58 3.57 6 19 -2 8.83 3.55 6 19 2 9.76 3.69 -6 -19 2 4.07 3.34 -6 -19 -2 7.32 3.44 6 19 -2 5.54 3.47 -6 19 -2 4.95 3.38 6 19 2 10.54 3.59 -6 19 2 4.99 3.69 -6 -19 -2 10.06 3.37 6 -19 -3 0.29 3.50 6 -19 3 2.27 3.33 6 19 -3 -6.27 3.72 6 19 3 -3.45 3.47 -6 -19 3 1.07 3.12 -6 -19 -3 -4.26 3.33 6 19 -3 -2.77 3.44 -6 19 -3 -0.83 3.50 6 19 3 1.11 3.36 -6 19 3 -1.66 3.45 -6 -19 -3 0.28 3.04 6 -19 -4 16.01 3.82 6 -19 4 11.82 3.65 6 19 -4 14.50 3.81 6 19 4 13.55 3.78 -6 -19 -4 12.01 3.60 6 19 -4 16.34 3.70 -6 19 -4 15.12 3.66 6 19 4 23.09 3.94 -6 19 4 15.58 3.76 -6 -19 -4 17.64 3.52 6 -19 5 4.74 3.44 6 19 -5 3.69 3.56 6 19 5 0.81 3.25 -6 -19 -5 6.91 3.37 6 19 -5 0.28 3.38 -6 19 -5 5.22 3.59 6 19 5 4.18 3.37 -6 19 5 9.48 3.60 -6 -19 -5 7.75 3.17 6 -19 6 2.21 3.24 6 19 -6 -0.57 3.57 6 19 6 -1.09 3.32 6 19 -6 -1.11 3.39 -6 19 -6 2.47 3.41 6 19 6 -0.28 3.41 -6 19 6 -3.92 3.53 6 19 -7 0.28 3.57 6 19 7 2.47 3.28 6 19 -7 -1.95 3.51 -6 19 -7 -0.28 3.44 6 19 7 -1.68 3.40 -6 19 7 0.84 3.38 6 19 7 -6.24 3.51 6 19 8 -4.16 3.46 6 19 -8 0.28 3.37 -6 19 -8 -1.65 3.41 6 19 8 1.68 3.33 -6 19 8 1.97 3.50 6 19 9 -2.80 3.40 -6 19 -9 4.41 3.45 6 19 9 0.28 3.31 -6 19 9 2.26 3.41 7 19 0 0.27 3.36 7 19 -1 4.92 3.48 7 19 1 5.20 3.57 7 19 -2 8.48 3.53 7 19 2 6.02 3.57 7 -19 3 -1.44 3.39 7 19 -3 -1.91 3.50 7 -19 4 2.28 3.39 7 19 4 6.02 3.45 7 19 -4 3.83 3.40 7 -19 5 2.26 3.43 7 19 5 6.62 3.32 7 19 -5 7.67 3.55 7 -19 6 -4.76 3.57 7 19 6 -0.28 3.30 7 19 -6 0.27 3.32 7 19 -7 1.65 3.42 0 -20 0 -4.02 3.36 0 -20 0 0.28 3.09 0 -20 1 2.85 3.35 0 -20 1 5.27 3.20 0 -20 -1 -0.28 3.11 0 -20 2 59.52 4.97 0 -20 -2 60.00 4.94 0 -20 3 7.27 3.36 0 -20 4 7.47 3.39 -1 -20 0 -2.29 3.44 -1 -20 0 -0.84 3.03 1 -20 0 -3.10 3.05 -1 -20 1 -2.84 3.51 1 -20 1 3.15 3.48 -1 -20 1 3.04 3.05 -1 -20 -1 2.54 3.08 1 -20 1 1.95 3.03 1 -20 -1 -1.99 3.15 -1 -20 2 4.50 3.48 1 -20 2 0.28 3.52 -1 -20 -2 1.99 3.24 1 -20 2 5.24 3.22 -1 -20 3 1.39 3.28 1 -20 3 4.21 3.42 1 -20 4 7.79 3.37 -2 -20 0 -1.67 3.00 2 -20 0 1.98 3.16 -2 -20 1 0.57 3.45 -2 -20 1 -0.28 3.02 -2 -20 -1 0.56 3.10 2 -20 1 -1.68 3.07 -2 -20 2 -0.56 3.39 2 -20 2 -0.28 3.07 2 20 3 21.13 3.82 -2 -20 3 15.54 3.56 2 -20 3 16.67 3.74 2 20 4 1.38 3.28 2 -20 4 0.56 3.34 3 20 -1 8.86 3.64 -3 -20 1 1.11 2.99 3 20 -2 4.14 3.51 -3 -20 3 -1.11 3.35 0 0 0 0.00 0.00 TITL R1 in Pbca REM Pbca (#61, found as Pcab in ba-c setting) CELL 0.71073 15.888682 14.119222 32.263623 90.0000 90.0000 90.0000 ZERR 8.00 0.000326 0.000201 0.000517 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C N O UNIT 368.00 16.00 32.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 15930 _olex2_date_sample_data_collection 2020-10-01 _olex2_exptl_crystal_mounting_method 'Paratone oil was used to mount crystal on a crystal loop.' _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.045 _oxdiff_exptl_absorpt_empirical_full_min 0.953