data_191227_b12c_0m _audit_creation_date 2019-12-30 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2016/6' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(C10 H25 B12 N O3), C3 H6 O, 4(C6 H16 N)' _chemical_formula_sum 'C47 H120 B24 N6 O7' _chemical_formula_weight 1140.92 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'B' 'B' 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 4 _space_group_name_H-M_alt 'P 1 21 1' _space_group_name_Hall 'P 2yb' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 18.2099(5) _cell_length_b 10.1365(3) _cell_length_c 19.5538(5) _cell_angle_alpha 90 _cell_angle_beta 103.5480(10) _cell_angle_gamma 90 _cell_volume 3508.90(17) _cell_formula_units_Z 2 _cell_measurement_reflns_used 9830 _cell_measurement_temperature 170(2) _cell_measurement_theta_max 68.30 _cell_measurement_theta_min 4.74 _shelx_estimated_absorpt_T_max 0.953 _shelx_estimated_absorpt_T_min 0.801 _exptl_absorpt_coefficient_mu 0.483 _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.6548 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1498 before and 0.0795 after correction. The Ratio of minimum to maximum transmission is 0.8695. The \l/2 correction factor is Not present. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.080 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1240 _exptl_crystal_size_max 0.48 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.1 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0312 _diffrn_reflns_av_unetI/netI 0.0226 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 63896 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 68.452 _diffrn_reflns_theta_min 2.496 _diffrn_ambient_temperature 170.0 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.885 _reflns_Friedel_fraction_full 0.996 _reflns_Friedel_fraction_max 0.994 _reflns_number_gt 12514 _reflns_number_total 12833 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_collection ? _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.875 _refine_diff_density_min -0.264 _refine_diff_density_rms 0.046 _refine_ls_abs_structure_details ; Flack x determined using 5715 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.02(3) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.039 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 835 _refine_ls_number_reflns 12833 _refine_ls_number_restraints 4 _refine_ls_R_factor_all 0.0536 _refine_ls_R_factor_gt 0.0526 _refine_ls_restrained_S_all 1.054 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0988P)^2^+0.8081P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1432 _refine_ls_wR_factor_ref 0.1446 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H,H) groups, All N(H) groups, All N(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances N6-C41 \\sim N6-C41A with sigma of 0.02 N6-C39 \\sim N6-C39A with sigma of 0.02 N6-C43 \\sim N6-C43A with sigma of 0.02 C40-C39 \\sim C40-C39A with sigma of 0.02 C41-C42 \\sim C41A-C42 with sigma of 0.02 C44-C43 \\sim C44-C43A with sigma of 0.02 3. Others Sof(H6B)=Sof(C44)=Sof(H44A)=Sof(H44B)=Sof(H44C)=Sof(C39A)=Sof(H39C)=Sof(H39D)= Sof(C40A)=Sof(H40D)=Sof(H40E)=Sof(H40F)=Sof(C41A)=Sof(H41C)=Sof(H41D)= Sof(C42A)=Sof(H42D)=Sof(H42E)=Sof(H42F)=Sof(C43A)=Sof(H43C)=Sof(H43D)=1-FVAR(1) Sof(H6A)=Sof(C39)=Sof(H39A)=Sof(H39B)=Sof(C40)=Sof(H40A)=Sof(H40B)=Sof(H40C)= Sof(C41)=Sof(H41A)=Sof(H41B)=Sof(C42)=Sof(H42A)=Sof(H42B)=Sof(H42C)=Sof(C43)= Sof(H43A)=Sof(H43B)=Sof(C44A)=Sof(H44D)=Sof(H44E)=Sof(H44F)=FVAR(1) 4.a Ternary CH refined with riding coordinates: N3(H3C), N4(H4C), N5(H5A), N6(H6A), N6(H6B) 4.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C4(H4A,H4B), C13(H13A,H13B), C14(H14A,H14B), C21(H21A,H21B), C23(H23A,H23B), C25(H25A,H25B), C27(H27A,H27B), C29(H29A,H29B), C31(H31A,H31B), C33(H33A,H33B), C35(H35A,H35B), C37(H37A,H37B), C39(H39A,H39B), C41(H41A, H41B), C43(H43A,H43B), C39A(H39C,H39D), C41A(H41C,H41D), C43A(H43C,H43D) 4.c Aromatic/amide H refined with riding coordinates: N1(H1), N2(H2A) 4.d Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C9(H9A,H9B,H9C), C10(H10A,H10B,H10C), C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C20(H20A,H20B,H20C), C45(H45A,H45B,H45C), C47(H47A,H47B, H47C), C22(H22A,H22B,H22C), C24(H24A,H24B,H24C), C26(H26A,H26B,H26C), C28(H28A, H28B,H28C), C30(H30A,H30B,H30C), C32(H32A,H32B,H32C), C34(H34A,H34B,H34C), C36(H36A,H36B,H36C), C38(H38A,H38B,H38C), C40(H40A,H40B,H40C), C42(H42A,H42B, H42C), C44(H44A,H44B,H44C), C40A(H40D,H40E,H40F), C42A(H42D,H42E,H42F), C44A(H44D,H44E,H44F) 4.e Boron cage BH refined with riding coordinates: B2(H2), B3(H3), B4(H4), B5(H5), B6(H6), B7(H7), B8(H8), B9(H9), B10(H10), B11(H11), B12(H12), B14(H14), B15(H15), B16(H16), B17(H17), B18(H18), B19(H19), B20(H20), B21(H21), B22(H22), B23(H23), B24(H24) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 1.05946(12) 0.6222(2) 0.70298(11) 0.0416(5) Uani 1 1 d . . . . . O2 O 0.94369(11) 0.47542(18) 0.54751(9) 0.0334(4) Uani 1 1 d . . . . . O3 O 0.85420(14) 0.4647(2) 0.44767(11) 0.0476(6) Uani 1 1 d . . . . . N1 N 1.00921(16) 0.4172(2) 0.67878(12) 0.0412(6) Uani 1 1 d . . . . . H1 H 0.987315 0.368305 0.642527 0.049 Uiso 1 1 calc R . . . . C1 C 1.02210(14) 0.5397(3) 0.66251(14) 0.0300(5) Uani 1 1 d . . . . . C2 C 0.98793(14) 0.5841(2) 0.58779(13) 0.0274(5) Uani 1 1 d . . . . . C3 C 1.04312(15) 0.6257(3) 0.54395(15) 0.0352(6) Uani 1 1 d . . . . . H3A H 1.071053 0.549008 0.531531 0.042 Uiso 1 1 calc R . . . . H3B H 1.079634 0.691945 0.568983 0.042 Uiso 1 1 calc R . . . . C4 C 0.98976(16) 0.6855(3) 0.47832(15) 0.0376(6) Uani 1 1 d . . . . . H4A H 0.991181 0.633911 0.435659 0.045 Uiso 1 1 calc R . . . . H4B H 1.003547 0.778115 0.471247 0.045 Uiso 1 1 calc R . . . . C5 C 0.91054(15) 0.6773(3) 0.49510(14) 0.0335(6) Uani 1 1 d . . . . . C6 C 0.89559(16) 0.5313(3) 0.49080(14) 0.0334(6) Uani 1 1 d . . . . . C7 C 0.92859(14) 0.6968(3) 0.57616(14) 0.0304(5) Uani 1 1 d . . . . . C8 C 0.8498(2) 0.7589(4) 0.44786(19) 0.0515(8) Uani 1 1 d . . . . . H8A H 0.847499 0.737010 0.398588 0.077 Uiso 1 1 calc GR . . . . H8B H 0.861532 0.852811 0.455808 0.077 Uiso 1 1 calc GR . . . . H8C H 0.800898 0.739830 0.458536 0.077 Uiso 1 1 calc GR . . . . C9 C 0.86212(16) 0.6649(4) 0.60935(17) 0.0465(7) Uani 1 1 d . . . . . H9A H 0.838675 0.581682 0.590008 0.070 Uiso 1 1 calc GR . . . . H9B H 0.824733 0.735998 0.598779 0.070 Uiso 1 1 calc GR . . . . H9C H 0.880545 0.656524 0.660429 0.070 Uiso 1 1 calc GR . . . . C10 C 0.95987(19) 0.8327(3) 0.60055(18) 0.0436(7) Uani 1 1 d . . . . . H10A H 0.976732 0.833493 0.651967 0.065 Uiso 1 1 calc GR . . . . H10B H 0.920314 0.899152 0.585523 0.065 Uiso 1 1 calc GR . . . . H10C H 1.002674 0.852699 0.579861 0.065 Uiso 1 1 calc GR . . . . B1 B 1.02533(18) 0.3446(3) 0.74901(15) 0.0317(6) Uani 1 1 d . . . . . B2 B 0.9674(2) 0.3740(6) 0.80790(19) 0.0719(17) Uani 1 1 d . . . . . H2 H 0.923539 0.453651 0.798435 0.086 Uiso 1 1 calc R . . . . B3 B 1.0643(3) 0.4097(4) 0.83387(18) 0.0531(10) Uani 1 1 d . . . . . H3 H 1.085220 0.513797 0.841888 0.064 Uiso 1 1 calc R . . . . B4 B 1.11434(18) 0.2891(4) 0.79809(16) 0.0395(7) Uani 1 1 d . . . . . H4 H 1.168046 0.313842 0.782379 0.047 Uiso 1 1 calc R . . . . B5 B 1.0486(2) 0.1762(3) 0.74963(17) 0.0422(8) Uani 1 1 d . . . . . H5 H 1.058875 0.125056 0.701950 0.051 Uiso 1 1 calc R . . . . B6 B 0.9571(2) 0.2267(5) 0.75618(19) 0.0573(12) Uani 1 1 d . . . . . H6 H 0.906079 0.207838 0.712588 0.069 Uiso 1 1 calc R . . . . B7 B 0.9525(2) 0.2215(8) 0.8461(2) 0.090(2) Uani 1 1 d . . . . . H7 H 0.898700 0.200725 0.862487 0.109 Uiso 1 1 calc R . . . . B8 B 1.0199(2) 0.3334(5) 0.89354(18) 0.0581(12) Uani 1 1 d . . . . . H8 H 1.011401 0.386499 0.941312 0.070 Uiso 1 1 calc R . . . . B9 B 1.10952(17) 0.2776(3) 0.88728(15) 0.0323(6) Uani 1 1 d . . . . . H9 H 1.160354 0.293080 0.931519 0.039 Uiso 1 1 calc R . . . . B10 B 1.1012(2) 0.1352(4) 0.83590(17) 0.0468(9) Uani 1 1 d . . . . . H10 H 1.146153 0.057413 0.845329 0.056 Uiso 1 1 calc R . . . . B11 B 1.0018(4) 0.0968(5) 0.8093(2) 0.083(2) Uani 1 1 d . . . . . H11 H 0.980569 -0.006981 0.800906 0.099 Uiso 1 1 calc R . . . . B12 B 1.0406(2) 0.1602(5) 0.89425(18) 0.0499(10) Uani 1 1 d . . . . . H12 H 1.044882 0.097288 0.942093 0.060 Uiso 1 1 calc R . . . . O4 O 0.45091(11) 0.63319(19) 0.29189(9) 0.0331(4) Uani 1 1 d . . . . . O5 O 0.56820(11) 0.50398(17) 0.45172(9) 0.0296(4) Uani 1 1 d . . . . . O6 O 0.65644(14) 0.5052(2) 0.55279(10) 0.0479(6) Uani 1 1 d . . . . . N2 N 0.50770(13) 0.4339(2) 0.32160(11) 0.0289(5) Uani 1 1 d . . . . . H2A H 0.539137 0.395442 0.357034 0.035 Uiso 1 1 calc R . . . . C11 C 0.49039(13) 0.5561(2) 0.33488(12) 0.0239(5) Uani 1 1 d . . . . . C12 C 0.52167(13) 0.6070(2) 0.40885(12) 0.0235(5) Uani 1 1 d . . . . . C13 C 0.46393(14) 0.6462(3) 0.45090(13) 0.0319(6) Uani 1 1 d . . . . . H13A H 0.438332 0.567940 0.464761 0.038 Uiso 1 1 calc R . . . . H13B H 0.425543 0.707553 0.423934 0.038 Uiso 1 1 calc R . . . . C14 C 0.51472(15) 0.7150(3) 0.51581(14) 0.0349(6) Uani 1 1 d . . . . . H14A H 0.513567 0.666924 0.559614 0.042 Uiso 1 1 calc R . . . . H14B H 0.498239 0.807141 0.519988 0.042 Uiso 1 1 calc R . . . . C15 C 0.59511(14) 0.7108(3) 0.50111(12) 0.0274(5) Uani 1 1 d . . . . . C16 C 0.61351(15) 0.5663(3) 0.50816(13) 0.0304(5) Uani 1 1 d . . . . . C17 C 0.57754(14) 0.7251(2) 0.41957(13) 0.0277(5) Uani 1 1 d . . . . . C18 C 0.65335(18) 0.7995(3) 0.54690(16) 0.0413(7) Uani 1 1 d . . . . . H18A H 0.658168 0.776729 0.596466 0.062 Uiso 1 1 calc GR . . . . H18B H 0.637403 0.891681 0.539079 0.062 Uiso 1 1 calc GR . . . . H18C H 0.702193 0.787466 0.534807 0.062 Uiso 1 1 calc GR . . . . C19 C 0.54218(19) 0.8582(3) 0.39290(16) 0.0421(7) Uani 1 1 d . . . . . H19A H 0.524725 0.855516 0.341549 0.063 Uiso 1 1 calc GR . . . . H19B H 0.579958 0.928209 0.406302 0.063 Uiso 1 1 calc GR . . . . H19C H 0.499250 0.876112 0.413788 0.063 Uiso 1 1 calc GR . . . . C20 C 0.64572(16) 0.6985(4) 0.38821(15) 0.0437(7) Uani 1 1 d . . . . . H20A H 0.671561 0.618252 0.409204 0.066 Uiso 1 1 calc GR . . . . H20B H 0.680664 0.773299 0.398146 0.066 Uiso 1 1 calc GR . . . . H20C H 0.628537 0.686735 0.337203 0.066 Uiso 1 1 calc GR . . . . B13 B 0.48389(15) 0.3466(3) 0.25691(14) 0.0239(5) Uani 1 1 d . . . . . B14 B 0.46314(16) 0.3953(3) 0.16704(14) 0.0259(5) Uani 1 1 d . . . . . H14 H 0.462949 0.501210 0.150707 0.031 Uiso 1 1 calc R . . . . B15 B 0.39057(15) 0.3280(3) 0.20492(14) 0.0254(5) Uani 1 1 d . . . . . H15 H 0.342563 0.389822 0.213560 0.031 Uiso 1 1 calc R . . . . B16 B 0.43163(16) 0.2011(3) 0.26484(14) 0.0279(6) Uani 1 1 d . . . . . H16 H 0.410560 0.179520 0.313075 0.033 Uiso 1 1 calc R . . . . B17 B 0.52926(16) 0.1897(3) 0.26479(14) 0.0280(6) Uani 1 1 d . . . . . H17 H 0.572821 0.160821 0.313045 0.034 Uiso 1 1 calc R . . . . B18 B 0.54880(16) 0.3091(3) 0.20424(15) 0.0280(6) Uani 1 1 d . . . . . H18 H 0.605144 0.358738 0.212389 0.034 Uiso 1 1 calc R . . . . B19 B 0.49519(16) 0.2665(3) 0.11894(14) 0.0294(6) Uani 1 1 d . . . . . H19 H 0.516013 0.287897 0.070536 0.035 Uiso 1 1 calc R . . . . B20 B 0.39785(15) 0.2782(3) 0.11920(13) 0.0245(5) Uani 1 1 d . . . . . H20 H 0.354340 0.307309 0.070952 0.029 Uiso 1 1 calc R . . . . B21 B 0.37858(17) 0.1587(3) 0.17960(15) 0.0299(6) Uani 1 1 d . . . . . H21 H 0.322254 0.108907 0.171108 0.036 Uiso 1 1 calc R . . . . B22 B 0.46397(19) 0.0734(3) 0.21717(15) 0.0324(6) Uani 1 1 d . . . . . H22 H 0.464201 -0.032394 0.233783 0.039 Uiso 1 1 calc R . . . . B23 B 0.53634(17) 0.1395(3) 0.17962(15) 0.0319(6) Uani 1 1 d . . . . . H23 H 0.584366 0.077256 0.171405 0.038 Uiso 1 1 calc R . . . . B24 B 0.44308(17) 0.1207(3) 0.12694(15) 0.0316(6) Uani 1 1 d . . . . . H24 H 0.429514 0.045718 0.083728 0.038 Uiso 1 1 calc R . . . . O7 O 0.75888(19) 0.0369(3) 0.49065(17) 0.0762(9) Uani 1 1 d . . . . . C45 C 0.6938(2) 0.2393(4) 0.46329(19) 0.0569(9) Uani 1 1 d . . . . . H45A H 0.659388 0.187119 0.427336 0.085 Uiso 1 1 calc GR . . . . H45B H 0.714755 0.311893 0.440726 0.085 Uiso 1 1 calc GR . . . . H45C H 0.666110 0.275258 0.496430 0.085 Uiso 1 1 calc GR . . . . C46 C 0.75625(16) 0.1538(3) 0.50176(14) 0.0383(7) Uani 1 1 d . . . . . C47 C 0.8173(2) 0.2204(4) 0.55387(19) 0.0549(9) Uani 1 1 d . . . . . H47A H 0.849099 0.154012 0.583115 0.082 Uiso 1 1 calc GR . . . . H47B H 0.795028 0.278244 0.583743 0.082 Uiso 1 1 calc GR . . . . H47C H 0.848151 0.273072 0.529167 0.082 Uiso 1 1 calc GR . . . . N3 N 0.80332(13) 0.2316(2) 0.25733(12) 0.0347(5) Uani 1 1 d . . . . . H3C H 0.849691 0.175745 0.263863 0.042 Uiso 1 1 calc R . . . . C21 C 0.82998(16) 0.3713(3) 0.27492(16) 0.0388(6) Uani 1 1 d . . . . . H21A H 0.861237 0.373037 0.323711 0.047 Uiso 1 1 calc R . . . . H21B H 0.862748 0.397482 0.243357 0.047 Uiso 1 1 calc R . . . . C22 C 0.76768(19) 0.4719(3) 0.26856(18) 0.0467(7) Uani 1 1 d . . . . . H22A H 0.736894 0.472557 0.220197 0.070 Uiso 1 1 calc GR . . . . H22B H 0.789808 0.559441 0.280471 0.070 Uiso 1 1 calc GR . . . . H22C H 0.735882 0.448990 0.300896 0.070 Uiso 1 1 calc GR . . . . C23 C 0.75998(19) 0.2117(4) 0.18300(16) 0.0474(7) Uani 1 1 d . . . . . H23A H 0.713198 0.265139 0.174458 0.057 Uiso 1 1 calc R . . . . H23B H 0.745155 0.117823 0.176088 0.057 Uiso 1 1 calc R . . . . C24 C 0.8049(3) 0.2499(4) 0.1302(2) 0.0643(10) Uani 1 1 d . . . . . H24A H 0.776163 0.227436 0.082730 0.096 Uiso 1 1 calc GR . . . . H24B H 0.853000 0.202013 0.140543 0.096 Uiso 1 1 calc GR . . . . H24C H 0.814735 0.345038 0.133122 0.096 Uiso 1 1 calc GR . . . . C25 C 0.75954(17) 0.1811(3) 0.30813(17) 0.0440(7) Uani 1 1 d . . . . . H25A H 0.708314 0.220227 0.296349 0.053 Uiso 1 1 calc R . . . . H25B H 0.784850 0.209962 0.356239 0.053 Uiso 1 1 calc R . . . . C26 C 0.7528(2) 0.0333(4) 0.3071(2) 0.0563(9) Uani 1 1 d . . . . . H26A H 0.718822 0.005313 0.262809 0.084 Uiso 1 1 calc GR . . . . H26B H 0.732301 0.004273 0.346676 0.084 Uiso 1 1 calc GR . . . . H26C H 0.802720 -0.006122 0.311004 0.084 Uiso 1 1 calc GR . . . . N4 N 0.61485(12) 0.7694(2) 0.06153(11) 0.0318(5) Uani 1 1 d . . . . . H4C H 0.590601 0.759474 0.010342 0.038 Uiso 1 1 calc R . . . . C27 C 0.55273(17) 0.7595(4) 0.09984(15) 0.0422(7) Uani 1 1 d . . . . . H27A H 0.521961 0.680428 0.082716 0.051 Uiso 1 1 calc R . . . . H27B H 0.519553 0.837575 0.087949 0.051 Uiso 1 1 calc R . . . . C28 C 0.5794(2) 0.7507(4) 0.17911(16) 0.0460(7) Uani 1 1 d . . . . . H28A H 0.608592 0.669468 0.191802 0.069 Uiso 1 1 calc GR . . . . H28B H 0.535581 0.749892 0.200179 0.069 Uiso 1 1 calc GR . . . . H28C H 0.611271 0.827063 0.196645 0.069 Uiso 1 1 calc GR . . . . C29 C 0.67403(19) 0.6628(4) 0.07958(17) 0.0457(7) Uani 1 1 d . . . . . H29A H 0.704166 0.676564 0.128204 0.055 Uiso 1 1 calc R . . . . H29B H 0.708632 0.669481 0.047505 0.055 Uiso 1 1 calc R . . . . C30 C 0.6396(3) 0.5258(4) 0.07372(19) 0.0609(10) Uani 1 1 d . . . . . H30A H 0.603327 0.516685 0.028247 0.091 Uiso 1 1 calc GR . . . . H30B H 0.613640 0.512423 0.111776 0.091 Uiso 1 1 calc GR . . . . H30C H 0.679615 0.459667 0.077358 0.091 Uiso 1 1 calc GR . . . . C31 C 0.6541(2) 0.9023(3) 0.06999(17) 0.0436(7) Uani 1 1 d . . . . . H31A H 0.668044 0.925419 0.120574 0.052 Uiso 1 1 calc R . . . . H31B H 0.701309 0.895248 0.053431 0.052 Uiso 1 1 calc R . . . . C32 C 0.6067(2) 1.0111(3) 0.03041(16) 0.0504(8) Uani 1 1 d . . . . . H32A H 0.593086 0.989606 -0.019843 0.076 Uiso 1 1 calc GR . . . . H32B H 0.635301 1.093842 0.037509 0.076 Uiso 1 1 calc GR . . . . H32C H 0.560608 1.021042 0.047691 0.076 Uiso 1 1 calc GR . . . . N5 N 0.31270(13) 0.7455(2) 0.24899(13) 0.0391(5) Uani 1 1 d . . . . . H5A H 0.363206 0.701394 0.261602 0.047 Uiso 1 1 calc R . . . . C33 C 0.31807(19) 0.8601(4) 0.29644(18) 0.0504(8) Uani 1 1 d . . . . . H33A H 0.361545 0.914877 0.291488 0.060 Uiso 1 1 calc R . . . . H33B H 0.328805 0.827644 0.345533 0.060 Uiso 1 1 calc R . . . . C34 C 0.2488(2) 0.9465(4) 0.28404(19) 0.0580(10) Uani 1 1 d . . . . . H34A H 0.239553 0.984729 0.236756 0.087 Uiso 1 1 calc GR . . . . H34B H 0.256714 1.017508 0.319037 0.087 Uiso 1 1 calc GR . . . . H34C H 0.205075 0.893495 0.288285 0.087 Uiso 1 1 calc GR . . . . C35 C 0.3043(2) 0.8006(4) 0.17337(19) 0.0578(9) Uani 1 1 d . . . . . H35A H 0.249882 0.807805 0.150441 0.069 Uiso 1 1 calc R . . . . H35B H 0.326070 0.890466 0.176535 0.069 Uiso 1 1 calc R . . . . C36 C 0.3403(2) 0.7211(5) 0.1302(2) 0.0674(11) Uani 1 1 d . . . . . H36A H 0.333244 0.761784 0.083602 0.101 Uiso 1 1 calc GR . . . . H36B H 0.317867 0.632746 0.125301 0.101 Uiso 1 1 calc GR . . . . H36C H 0.394389 0.714541 0.152022 0.101 Uiso 1 1 calc GR . . . . C37 C 0.2567(2) 0.6406(4) 0.2486(2) 0.0553(8) Uani 1 1 d . . . . . H37A H 0.254597 0.583729 0.207022 0.066 Uiso 1 1 calc R . . . . H37B H 0.206352 0.681925 0.243094 0.066 Uiso 1 1 calc R . . . . C38 C 0.2716(2) 0.5557(4) 0.3126(2) 0.0577(9) Uani 1 1 d . . . . . H38A H 0.231438 0.489676 0.308127 0.087 Uiso 1 1 calc GR . . . . H38B H 0.272869 0.610480 0.354173 0.087 Uiso 1 1 calc GR . . . . H38C H 0.320332 0.511105 0.317646 0.087 Uiso 1 1 calc GR . . . . N6 N 0.11379(16) 0.2525(4) 0.06727(14) 0.0614(10) Uani 1 1 d D . . . . H6A H 0.097260 0.243488 0.014987 0.074 Uiso 0.502(6) 1 calc R . P A 1 H6B H 0.094553 0.262280 0.015256 0.074 Uiso 0.498(6) 1 calc R . P A 2 C39 C 0.1202(5) 0.4144(8) 0.0874(4) 0.0508(18) Uani 0.502(6) 1 d D . P A 1 H39A H 0.069674 0.455764 0.073272 0.061 Uiso 0.502(6) 1 calc R . P A 1 H39B H 0.138980 0.425587 0.138878 0.061 Uiso 0.502(6) 1 calc R . P A 1 C40 C 0.1754(11) 0.4825(17) 0.0483(8) 0.062(4) Uani 0.502(6) 1 d D . P A 1 H40A H 0.226401 0.446872 0.065728 0.093 Uiso 0.502(6) 1 calc GR . P A 1 H40B H 0.175932 0.577784 0.056940 0.093 Uiso 0.502(6) 1 calc GR . P A 1 H40C H 0.158587 0.465692 -0.002298 0.093 Uiso 0.502(6) 1 calc GR . P A 1 C41 C 0.0511(5) 0.2118(7) 0.0980(5) 0.042(2) Uani 0.502(6) 1 d D . P A 1 H41A H 0.050548 0.114105 0.098733 0.050 Uiso 0.502(6) 1 calc R . P A 1 H41B H 0.063324 0.241414 0.147668 0.050 Uiso 0.502(6) 1 calc R . P A 1 C42 C -0.0248(4) 0.2552(9) 0.0665(4) 0.061(2) Uani 0.502(6) 1 d D . P A 1 H42A H -0.033902 0.340610 0.086510 0.092 Uiso 0.502(6) 1 calc GR . P A 1 H42B H -0.061009 0.190242 0.076145 0.092 Uiso 0.502(6) 1 calc GR . P A 1 H42C H -0.031076 0.264054 0.015595 0.092 Uiso 0.502(6) 1 calc GR . P A 1 C43 C 0.1849(4) 0.1949(8) 0.0896(4) 0.0538(19) Uani 0.502(6) 1 d D . P A 1 H43A H 0.201206 0.196482 0.141541 0.065 Uiso 0.502(6) 1 calc R . P A 1 H43B H 0.222548 0.243498 0.070084 0.065 Uiso 0.502(6) 1 calc R . P A 1 C44 C 0.1779(13) 0.0563(19) 0.0634(9) 0.084(7) Uani 0.498(6) 1 d D . P A 1 H44A H 0.143143 0.007756 0.085618 0.127 Uiso 0.498(6) 1 calc GR . P A 1 H44B H 0.227674 0.013877 0.075228 0.127 Uiso 0.498(6) 1 calc GR . P A 1 H44C H 0.158426 0.056071 0.012275 0.127 Uiso 0.498(6) 1 calc GR . P A 1 C39A C 0.1858(4) 0.3170(8) 0.0861(4) 0.056(2) Uani 0.498(6) 1 d D . P A 2 H39C H 0.220901 0.282802 0.058630 0.067 Uiso 0.498(6) 1 calc R . P A 2 H39D H 0.209166 0.307988 0.136985 0.067 Uiso 0.498(6) 1 calc R . P A 2 C40A C 0.1622(14) 0.463(2) 0.0660(11) 0.104(7) Uani 0.498(6) 1 d . . P A 2 H40D H 0.137073 0.467528 0.015937 0.156 Uiso 0.498(6) 1 calc GR . P A 2 H40E H 0.207322 0.518971 0.075331 0.156 Uiso 0.498(6) 1 calc GR . P A 2 H40F H 0.127560 0.493558 0.094123 0.156 Uiso 0.498(6) 1 calc GR . P A 2 C41A C 0.0529(7) 0.283(2) 0.0989(6) 0.096(5) Uani 0.498(6) 1 d D . P A 2 H41C H 0.006232 0.239436 0.072113 0.115 Uiso 0.498(6) 1 calc R . P A 2 H41D H 0.044204 0.379162 0.097384 0.115 Uiso 0.498(6) 1 calc R . P A 2 C42A C 0.0718(6) 0.2313(11) 0.1821(4) 0.077(3) Uani 0.498(6) 1 d . . P A 2 H42D H 0.087744 0.138734 0.184344 0.116 Uiso 0.498(6) 1 calc GR . P A 2 H42E H 0.026319 0.239502 0.200554 0.116 Uiso 0.498(6) 1 calc GR . P A 2 H42F H 0.112284 0.285288 0.210502 0.116 Uiso 0.498(6) 1 calc GR . P A 2 C43A C 0.1361(6) 0.0924(10) 0.0835(4) 0.060(2) Uani 0.498(6) 1 d D . P A 2 H43C H 0.158730 0.081722 0.134373 0.072 Uiso 0.498(6) 1 calc R . P A 2 H43D H 0.088949 0.039747 0.072142 0.072 Uiso 0.498(6) 1 calc R . P A 2 C44A C 0.1911(12) 0.0359(18) 0.0420(7) 0.061(4) Uani 0.502(6) 1 d . . P A 2 H44D H 0.177281 0.068431 -0.006535 0.092 Uiso 0.502(6) 1 calc GR . P A 2 H44E H 0.188505 -0.060619 0.041952 0.092 Uiso 0.502(6) 1 calc GR . P A 2 H44F H 0.242701 0.064136 0.064174 0.092 Uiso 0.502(6) 1 calc GR . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0418(11) 0.0366(11) 0.0396(11) 0.0010(9) -0.0043(9) -0.0092(9) O2 0.0454(11) 0.0229(9) 0.0282(9) 0.0017(7) 0.0014(8) -0.0050(8) O3 0.0575(13) 0.0458(12) 0.0332(10) 0.0016(9) -0.0022(9) -0.0180(11) N1 0.0661(17) 0.0242(12) 0.0263(11) 0.0017(9) -0.0035(11) -0.0026(11) C1 0.0296(12) 0.0281(13) 0.0303(12) 0.0016(10) 0.0028(10) 0.0031(10) C2 0.0285(12) 0.0211(11) 0.0305(13) 0.0005(10) 0.0030(10) -0.0015(9) C3 0.0310(13) 0.0378(15) 0.0369(14) 0.0051(12) 0.0085(11) 0.0028(11) C4 0.0387(14) 0.0361(15) 0.0367(14) 0.0091(12) 0.0063(11) -0.0044(12) C5 0.0321(13) 0.0315(14) 0.0337(13) 0.0063(11) 0.0013(10) -0.0011(11) C6 0.0357(13) 0.0334(14) 0.0284(12) 0.0038(11) 0.0025(10) -0.0051(11) C7 0.0270(12) 0.0268(13) 0.0352(13) 0.0018(10) 0.0027(10) 0.0048(10) C8 0.0469(17) 0.0448(18) 0.0518(18) 0.0132(15) -0.0108(14) 0.0070(15) C9 0.0318(14) 0.061(2) 0.0479(17) -0.0039(15) 0.0114(12) 0.0018(14) C10 0.0500(17) 0.0254(14) 0.0498(17) -0.0024(12) 0.0001(13) 0.0071(12) B1 0.0380(15) 0.0281(14) 0.0262(14) 0.0011(11) 0.0021(11) 0.0038(12) B2 0.052(2) 0.133(5) 0.0280(17) 0.009(2) 0.0035(15) 0.056(3) B3 0.086(3) 0.0323(17) 0.0309(17) -0.0031(14) -0.0071(17) 0.0099(18) B4 0.0289(14) 0.059(2) 0.0285(14) 0.0070(14) 0.0032(12) -0.0008(14) B5 0.068(2) 0.0253(15) 0.0270(14) 0.0011(12) -0.0010(14) 0.0050(15) B6 0.0380(18) 0.094(3) 0.0332(17) 0.0203(19) -0.0056(14) -0.024(2) B7 0.0308(18) 0.199(7) 0.0368(19) 0.034(3) -0.0018(15) -0.025(3) B8 0.050(2) 0.096(3) 0.0266(16) 0.0055(19) 0.0062(15) 0.036(2) B9 0.0301(14) 0.0392(16) 0.0244(13) 0.0029(12) -0.0002(11) 0.0025(12) B10 0.071(2) 0.0355(17) 0.0288(15) 0.0018(13) 0.0016(15) 0.0205(17) B11 0.118(4) 0.070(3) 0.038(2) 0.021(2) -0.026(2) -0.065(3) B12 0.0488(19) 0.065(2) 0.0293(16) 0.0164(16) -0.0047(14) -0.0222(18) O4 0.0352(9) 0.0321(10) 0.0271(9) -0.0024(7) -0.0024(7) 0.0105(8) O5 0.0414(10) 0.0227(9) 0.0206(8) -0.0006(6) -0.0012(7) 0.0058(7) O6 0.0651(14) 0.0424(12) 0.0264(10) -0.0009(8) -0.0089(9) 0.0190(11) N2 0.0358(11) 0.0274(11) 0.0198(9) -0.0015(8) -0.0011(8) 0.0059(9) C11 0.0224(11) 0.0260(12) 0.0227(11) -0.0028(9) 0.0038(9) 0.0014(9) C12 0.0270(11) 0.0198(11) 0.0228(11) 0.0002(9) 0.0040(9) 0.0041(9) C13 0.0280(12) 0.0407(14) 0.0279(12) -0.0084(11) 0.0083(10) -0.0020(11) C14 0.0334(13) 0.0409(15) 0.0291(13) -0.0125(11) 0.0051(10) 0.0044(11) C15 0.0296(12) 0.0259(12) 0.0236(11) -0.0046(9) 0.0003(9) 0.0010(10) C16 0.0376(13) 0.0293(13) 0.0212(11) -0.0030(10) 0.0007(10) 0.0069(11) C17 0.0274(12) 0.0271(13) 0.0264(12) 0.0002(10) 0.0017(9) -0.0026(10) C18 0.0409(15) 0.0364(15) 0.0387(15) -0.0094(12) -0.0065(12) -0.0023(12) C19 0.0502(17) 0.0269(14) 0.0414(16) 0.0061(12) -0.0051(13) -0.0041(12) C20 0.0327(14) 0.065(2) 0.0342(14) 0.0038(14) 0.0095(11) -0.0066(14) B13 0.0269(13) 0.0242(12) 0.0197(12) -0.0025(10) 0.0036(10) 0.0016(10) B14 0.0304(13) 0.0270(13) 0.0196(12) 0.0025(10) 0.0047(10) 0.0015(11) B15 0.0237(12) 0.0304(14) 0.0220(12) 0.0001(10) 0.0047(10) 0.0012(10) B16 0.0312(13) 0.0272(13) 0.0235(12) 0.0019(11) 0.0030(10) -0.0022(11) B17 0.0307(13) 0.0269(14) 0.0229(12) -0.0029(10) -0.0008(10) 0.0050(11) B18 0.0250(13) 0.0330(15) 0.0251(13) -0.0032(11) 0.0044(10) -0.0002(11) B19 0.0295(13) 0.0371(15) 0.0214(12) -0.0016(11) 0.0055(10) 0.0017(12) B20 0.0275(13) 0.0251(13) 0.0189(11) 0.0005(10) 0.0017(10) -0.0006(10) B21 0.0322(14) 0.0268(14) 0.0263(13) 0.0024(11) -0.0018(11) -0.0044(11) B22 0.0431(16) 0.0231(13) 0.0259(13) -0.0003(11) -0.0023(11) 0.0029(12) B23 0.0341(14) 0.0331(15) 0.0260(13) -0.0057(11) 0.0021(11) 0.0102(12) B24 0.0370(15) 0.0306(15) 0.0235(13) -0.0069(11) -0.0007(11) 0.0043(12) O7 0.104(3) 0.0374(14) 0.085(2) -0.0107(13) 0.0185(19) -0.0016(14) C45 0.0480(18) 0.073(2) 0.0499(18) -0.0081(17) 0.0114(15) 0.0122(17) C46 0.0452(16) 0.0350(16) 0.0402(16) -0.0025(11) 0.0209(13) -0.0046(12) C47 0.0489(18) 0.064(2) 0.0544(19) -0.0019(17) 0.0167(15) -0.0159(17) N3 0.0332(11) 0.0323(12) 0.0359(12) 0.0043(9) 0.0025(9) 0.0035(9) C21 0.0358(14) 0.0354(15) 0.0394(15) 0.0023(12) -0.0031(11) -0.0031(12) C22 0.0480(17) 0.0341(15) 0.0517(18) -0.0017(13) -0.0008(14) 0.0049(13) C23 0.0533(18) 0.0441(17) 0.0397(15) -0.0040(13) 0.0009(13) -0.0003(14) C24 0.088(3) 0.062(2) 0.0462(18) 0.0007(17) 0.0238(19) 0.007(2) C25 0.0372(14) 0.0452(17) 0.0492(16) 0.0098(14) 0.0091(12) 0.0020(13) C26 0.062(2) 0.0450(19) 0.060(2) 0.0164(16) 0.0115(17) -0.0033(16) N4 0.0315(11) 0.0409(13) 0.0220(10) 0.0013(9) 0.0045(8) -0.0011(10) C27 0.0338(14) 0.0572(19) 0.0368(15) 0.0061(14) 0.0109(11) -0.0009(13) C28 0.0604(19) 0.0497(18) 0.0329(14) 0.0002(13) 0.0209(14) 0.0006(15) C29 0.0488(17) 0.0488(18) 0.0411(16) 0.0089(14) 0.0139(13) 0.0167(15) C30 0.100(3) 0.0415(18) 0.0356(16) 0.0039(14) 0.0046(17) 0.0091(19) C31 0.0511(17) 0.0432(17) 0.0369(15) -0.0005(13) 0.0113(13) -0.0062(14) C32 0.082(2) 0.0356(16) 0.0350(15) -0.0046(12) 0.0165(15) 0.0021(16) N5 0.0278(11) 0.0358(13) 0.0462(13) 0.0004(11) -0.0063(9) 0.0055(10) C33 0.0400(16) 0.0533(19) 0.0477(17) -0.0155(15) -0.0102(13) 0.0126(14) C34 0.0502(19) 0.067(2) 0.0492(19) -0.0168(17) -0.0029(15) 0.0262(18) C35 0.058(2) 0.060(2) 0.0480(18) 0.0039(16) -0.0013(15) 0.0111(17) C36 0.068(2) 0.081(3) 0.051(2) 0.018(2) 0.0088(18) -0.007(2) C37 0.0461(17) 0.053(2) 0.064(2) -0.0032(17) 0.0072(15) 0.0016(15) C38 0.073(2) 0.051(2) 0.058(2) 0.0118(17) 0.0341(18) 0.0117(18) N6 0.0363(14) 0.119(3) 0.0270(12) 0.0000(15) 0.0028(10) -0.0133(17) C39 0.060(5) 0.054(4) 0.038(3) -0.007(3) 0.009(3) 0.013(4) C40 0.078(6) 0.066(6) 0.053(7) -0.028(5) 0.038(6) -0.044(5) C41 0.045(4) 0.038(3) 0.047(4) 0.016(4) 0.019(3) 0.005(3) C42 0.051(4) 0.070(5) 0.079(5) -0.002(4) 0.046(4) -0.009(4) C43 0.045(4) 0.059(5) 0.049(4) -0.005(3) -0.006(3) 0.013(3) C44 0.094(13) 0.065(7) 0.063(13) -0.006(8) -0.044(11) 0.028(7) C39A 0.053(4) 0.061(5) 0.044(4) -0.004(3) -0.006(3) -0.007(3) C40A 0.12(2) 0.106(15) 0.074(13) -0.018(10) 0.006(10) 0.013(13) C41A 0.071(7) 0.176(16) 0.042(5) -0.021(9) 0.017(4) 0.040(10) C42A 0.111(7) 0.083(6) 0.047(4) 0.005(4) 0.038(5) 0.010(6) C43A 0.063(5) 0.077(6) 0.034(4) 0.014(4) 0.001(4) -0.017(5) C44A 0.080(8) 0.058(8) 0.033(6) 0.009(5) -0.012(5) 0.000(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.239(3) . ? O2 C2 1.478(3) . ? O2 C6 1.365(3) . ? O3 C6 1.199(4) . ? N1 H1 0.8800 . ? N1 C1 1.316(4) . ? N1 B1 1.525(4) . ? C1 C2 1.516(3) . ? C2 C3 1.525(4) . ? C2 C7 1.552(3) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C3 C4 1.541(4) . ? C4 H4A 0.9900 . ? C4 H4B 0.9900 . ? C4 C5 1.555(4) . ? C5 C6 1.504(4) . ? C5 C7 1.554(4) . ? C5 C8 1.511(4) . ? C7 C9 1.536(4) . ? C7 C10 1.524(4) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? B1 B2 1.760(5) . ? B1 B3 1.772(4) . ? B1 B4 1.771(4) . ? B1 B5 1.758(4) . ? B1 B6 1.753(5) . ? B2 H2 1.1200 . ? B2 B3 1.756(7) . ? B2 B6 1.788(8) . ? B2 B7 1.765(9) . ? B2 B8 1.771(5) . ? B3 H3 1.1200 . ? B3 B4 1.764(5) . ? B3 B8 1.748(6) . ? B3 B9 1.777(5) . ? B4 H4 1.1200 . ? B4 B5 1.763(5) . ? B4 B9 1.771(4) . ? B4 B10 1.766(5) . ? B5 H5 1.1200 . ? B5 B6 1.778(6) . ? B5 B10 1.783(5) . ? B5 B11 1.789(6) . ? B6 H6 1.1200 . ? B6 B7 1.780(5) . ? B6 B11 1.755(7) . ? B7 H7 1.1200 . ? B7 B8 1.767(8) . ? B7 B11 1.796(10) . ? B7 B12 1.772(6) . ? B8 H8 1.1200 . ? B8 B9 1.758(5) . ? B8 B12 1.795(7) . ? B9 H9 1.1200 . ? B9 B10 1.745(5) . ? B9 B12 1.757(5) . ? B10 H10 1.1200 . ? B10 B11 1.805(7) . ? B10 B12 1.782(6) . ? B11 H11 1.1200 . ? B11 B12 1.767(6) . ? B12 H12 1.1200 . ? O4 C11 1.246(3) . ? O5 C12 1.476(3) . ? O5 C16 1.368(3) . ? O6 C16 1.199(3) . ? N2 H2A 0.8800 . ? N2 C11 1.318(3) . ? N2 B13 1.522(3) . ? C11 C12 1.515(3) . ? C12 C13 1.531(3) . ? C12 C17 1.554(3) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.550(3) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C14 C15 1.557(4) . ? C15 C16 1.501(4) . ? C15 C17 1.558(3) . ? C15 C18 1.513(4) . ? C17 C19 1.533(4) . ? C17 C20 1.532(4) . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? B13 B14 1.779(4) . ? B13 B15 1.774(4) . ? B13 B16 1.781(4) . ? B13 B17 1.783(4) . ? B13 B18 1.781(4) . ? B14 H14 1.1200 . ? B14 B15 1.794(4) . ? B14 B18 1.787(4) . ? B14 B19 1.785(4) . ? B14 B20 1.782(4) . ? B15 H15 1.1200 . ? B15 B16 1.782(4) . ? B15 B20 1.785(4) . ? B15 B21 1.786(4) . ? B16 H16 1.1200 . ? B16 B17 1.782(4) . ? B16 B21 1.772(4) . ? B16 B22 1.775(4) . ? B17 H17 1.1200 . ? B17 B18 1.787(4) . ? B17 B22 1.775(4) . ? B17 B23 1.775(4) . ? B18 H18 1.1200 . ? B18 B19 1.777(4) . ? B18 B23 1.786(4) . ? B19 H19 1.1200 . ? B19 B20 1.778(4) . ? B19 B23 1.792(4) . ? B19 B24 1.783(4) . ? B20 H20 1.1200 . ? B20 B21 1.783(4) . ? B20 B24 1.787(4) . ? B21 H21 1.1200 . ? B21 B22 1.781(4) . ? B21 B24 1.776(4) . ? B22 H22 1.1200 . ? B22 B23 1.783(5) . ? B22 B24 1.781(4) . ? B23 H23 1.1200 . ? B23 B24 1.778(4) . ? B24 H24 1.1200 . ? O7 C46 1.208(4) . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C45 C46 1.486(5) . ? C46 C47 1.483(4) . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? N3 H3C 1.0000 . ? N3 C21 1.509(4) . ? N3 C23 1.496(4) . ? N3 C25 1.502(4) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C22 1.509(4) . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C24 1.510(5) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C25 C26 1.503(5) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? N4 H4C 1.0000 . ? N4 C27 1.499(3) . ? N4 C29 1.509(4) . ? N4 C31 1.515(4) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C27 C28 1.514(4) . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C29 C30 1.517(5) . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C31 C32 1.499(5) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? N5 H5A 1.0000 . ? N5 C33 1.476(4) . ? N5 C35 1.554(4) . ? N5 C37 1.472(5) . ? C33 H33A 0.9900 . ? C33 H33B 0.9900 . ? C33 C34 1.508(4) . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 H35A 0.9900 . ? C35 H35B 0.9900 . ? C35 C36 1.432(6) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9900 . ? C37 H37B 0.9900 . ? C37 C38 1.491(5) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? N6 H6A 1.0000 . ? N6 H6B 1.0000 . ? N6 C39 1.685(9) . ? N6 C41 1.469(8) . ? N6 C43 1.394(7) . ? N6 C39A 1.434(8) . ? N6 C41A 1.424(10) . ? N6 C43A 1.685(11) . ? C39 H39A 0.9900 . ? C39 H39B 0.9900 . ? C39 C40 1.560(11) . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C41 H41A 0.9900 . ? C41 H41B 0.9900 . ? C41 C42 1.444(13) . ? C42 H42A 0.9800 . ? C42 H42B 0.9800 . ? C42 H42C 0.9800 . ? C43 H43A 0.9900 . ? C43 H43B 0.9900 . ? C43 C44 1.49(2) . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C39A H39C 0.9900 . ? C39A H39D 0.9900 . ? C39A C40A 1.56(2) . ? C40A H40D 0.9800 . ? C40A H40E 0.9800 . ? C40A H40F 0.9800 . ? C41A H41C 0.9900 . ? C41A H41D 0.9900 . ? C41A C42A 1.666(15) . ? C42A H42D 0.9800 . ? C42A H42E 0.9800 . ? C42A H42F 0.9800 . ? C43A H43C 0.9900 . ? C43A H43D 0.9900 . ? C43A C44A 1.540(18) . ? C44A H44D 0.9800 . ? C44A H44E 0.9800 . ? C44A H44F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 O2 C2 106.86(19) . . ? C1 N1 H1 114.2 . . ? C1 N1 B1 131.7(2) . . ? B1 N1 H1 114.2 . . ? O1 C1 N1 125.8(3) . . ? O1 C1 C2 117.1(2) . . ? N1 C1 C2 117.2(2) . . ? O2 C2 C1 110.0(2) . . ? O2 C2 C3 104.8(2) . . ? O2 C2 C7 101.33(19) . . ? C1 C2 C3 116.6(2) . . ? C1 C2 C7 118.3(2) . . ? C3 C2 C7 104.0(2) . . ? C2 C3 H3A 111.4 . . ? C2 C3 H3B 111.4 . . ? C2 C3 C4 101.9(2) . . ? H3A C3 H3B 109.2 . . ? C4 C3 H3A 111.4 . . ? C4 C3 H3B 111.4 . . ? C3 C4 H4A 111.0 . . ? C3 C4 H4B 111.0 . . ? C3 C4 C5 103.8(2) . . ? H4A C4 H4B 109.0 . . ? C5 C4 H4A 111.0 . . ? C5 C4 H4B 111.0 . . ? C6 C5 C4 101.9(2) . . ? C6 C5 C7 100.0(2) . . ? C6 C5 C8 114.1(2) . . ? C7 C5 C4 102.9(2) . . ? C8 C5 C4 115.1(2) . . ? C8 C5 C7 120.2(3) . . ? O2 C6 C5 106.8(2) . . ? O3 C6 O2 121.1(3) . . ? O3 C6 C5 132.0(3) . . ? C2 C7 C5 91.7(2) . . ? C9 C7 C2 111.9(2) . . ? C9 C7 C5 113.9(2) . . ? C10 C7 C2 115.0(2) . . ? C10 C7 C5 114.1(2) . . ? C10 C7 C9 109.4(3) . . ? C5 C8 H8A 109.5 . . ? C5 C8 H8B 109.5 . . ? C5 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C7 C9 H9A 109.5 . . ? C7 C9 H9B 109.5 . . ? C7 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C7 C10 H10A 109.5 . . ? C7 C10 H10B 109.5 . . ? C7 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? N1 B1 B2 119.3(3) . . ? N1 B1 B3 127.9(3) . . ? N1 B1 B4 126.9(3) . . ? N1 B1 B5 118.0(2) . . ? N1 B1 B6 114.2(2) . . ? B2 B1 B3 59.6(3) . . ? B2 B1 B4 108.2(2) . . ? B4 B1 B3 59.7(2) . . ? B5 B1 B2 109.9(3) . . ? B5 B1 B3 108.2(2) . . ? B5 B1 B4 59.9(2) . . ? B6 B1 B2 61.2(3) . . ? B6 B1 B3 108.4(3) . . ? B6 B1 B4 108.4(2) . . ? B6 B1 B5 60.8(2) . . ? B1 B2 H2 121.8 . . ? B1 B2 B6 59.2(2) . . ? B1 B2 B7 107.7(4) . . ? B1 B2 B8 107.8(2) . . ? B3 B2 B1 60.5(2) . . ? B3 B2 H2 121.9 . . ? B3 B2 B6 107.5(3) . . ? B3 B2 B7 107.6(3) . . ? B3 B2 B8 59.4(2) . . ? B6 B2 H2 122.1 . . ? B7 B2 H2 121.8 . . ? B7 B2 B6 60.1(3) . . ? B7 B2 B8 60.0(3) . . ? B8 B2 H2 122.0 . . ? B8 B2 B6 107.6(3) . . ? B1 B3 H3 122.0 . . ? B1 B3 B9 107.4(2) . . ? B2 B3 B1 59.8(2) . . ? B2 B3 H3 121.3 . . ? B2 B3 B4 108.7(3) . . ? B2 B3 B9 108.1(3) . . ? B4 B3 B1 60.11(18) . . ? B4 B3 H3 121.2 . . ? B4 B3 B9 60.00(19) . . ? B8 B3 B1 108.3(3) . . ? B8 B3 B2 60.7(3) . . ? B8 B3 H3 121.2 . . ? B8 B3 B4 108.7(3) . . ? B8 B3 B9 59.8(2) . . ? B9 B3 H3 122.2 . . ? B1 B4 H4 121.8 . . ? B3 B4 B1 60.19(19) . . ? B3 B4 H4 121.3 . . ? B3 B4 B9 60.38(19) . . ? B3 B4 B10 108.3(2) . . ? B5 B4 B1 59.68(18) . . ? B5 B4 B3 108.3(3) . . ? B5 B4 H4 121.6 . . ? B5 B4 B9 107.6(2) . . ? B5 B4 B10 60.7(2) . . ? B9 B4 B1 107.7(2) . . ? B9 B4 H4 122.2 . . ? B10 B4 B1 108.1(2) . . ? B10 B4 H4 121.6 . . ? B10 B4 B9 59.11(18) . . ? B1 B5 B4 60.39(19) . . ? B1 B5 H5 122.1 . . ? B1 B5 B6 59.5(2) . . ? B1 B5 B10 107.9(2) . . ? B1 B5 B11 106.9(3) . . ? B4 B5 H5 121.6 . . ? B4 B5 B6 107.7(3) . . ? B4 B5 B10 59.7(2) . . ? B4 B5 B11 108.0(2) . . ? B6 B5 H5 122.4 . . ? B6 B5 B10 107.7(3) . . ? B6 B5 B11 59.0(3) . . ? B10 B5 H5 121.5 . . ? B10 B5 B11 60.7(2) . . ? B11 B5 H5 122.1 . . ? B1 B6 B2 59.6(2) . . ? B1 B6 B5 59.72(19) . . ? B1 B6 H6 122.2 . . ? B1 B6 B7 107.3(3) . . ? B1 B6 B11 108.6(3) . . ? B2 B6 H6 122.1 . . ? B5 B6 B2 107.8(3) . . ? B5 B6 H6 121.3 . . ? B5 B6 B7 108.9(3) . . ? B7 B6 B2 59.3(3) . . ? B7 B6 H6 121.6 . . ? B11 B6 B2 108.6(3) . . ? B11 B6 B5 60.8(3) . . ? B11 B6 H6 120.6 . . ? B11 B6 B7 61.1(3) . . ? B2 B7 B6 60.6(3) . . ? B2 B7 H7 121.1 . . ? B2 B7 B8 60.2(3) . . ? B2 B7 B11 107.8(3) . . ? B2 B7 B12 108.8(3) . . ? B6 B7 H7 122.3 . . ? B6 B7 B11 58.8(3) . . ? B8 B7 B6 108.2(3) . . ? B8 B7 H7 121.1 . . ? B8 B7 B11 108.1(3) . . ? B8 B7 B12 60.9(2) . . ? B11 B7 H7 122.4 . . ? B12 B7 B6 106.8(3) . . ? B12 B7 H7 121.7 . . ? B12 B7 B11 59.4(3) . . ? B2 B8 H8 121.8 . . ? B2 B8 B12 107.5(3) . . ? B3 B8 B2 59.9(3) . . ? B3 B8 B7 107.9(3) . . ? B3 B8 H8 121.4 . . ? B3 B8 B9 60.9(2) . . ? B3 B8 B12 108.0(3) . . ? B7 B8 B2 59.8(3) . . ? B7 B8 H8 122.1 . . ? B7 B8 B12 59.7(3) . . ? B9 B8 B2 108.3(2) . . ? B9 B8 B7 107.4(3) . . ? B9 B8 H8 121.7 . . ? B9 B8 B12 59.3(2) . . ? B12 B8 H8 122.2 . . ? B3 B9 H9 122.2 . . ? B4 B9 B3 59.6(2) . . ? B4 B9 H9 121.9 . . ? B8 B9 B3 59.3(2) . . ? B8 B9 B4 108.0(2) . . ? B8 B9 H9 120.9 . . ? B10 B9 B3 108.6(2) . . ? B10 B9 B4 60.3(2) . . ? B10 B9 B8 110.5(3) . . ? B10 B9 H9 120.3 . . ? B10 B9 B12 61.2(2) . . ? B12 B9 B3 108.4(3) . . ? B12 B9 B4 108.8(2) . . ? B12 B9 B8 61.4(3) . . ? B12 B9 H9 120.7 . . ? B4 B10 B5 59.56(18) . . ? B4 B10 H10 121.7 . . ? B4 B10 B11 107.1(3) . . ? B4 B10 B12 107.9(3) . . ? B5 B10 H10 122.0 . . ? B5 B10 B11 59.8(2) . . ? B9 B10 B4 60.57(19) . . ? B9 B10 B5 107.9(2) . . ? B9 B10 H10 121.8 . . ? B9 B10 B11 106.9(3) . . ? B9 B10 B12 59.8(2) . . ? B11 B10 H10 122.7 . . ? B12 B10 B5 107.3(3) . . ? B12 B10 H10 122.2 . . ? B12 B10 B11 59.0(3) . . ? B5 B11 B7 107.7(3) . . ? B5 B11 B10 59.5(2) . . ? B5 B11 H11 121.9 . . ? B6 B11 B5 60.2(2) . . ? B6 B11 B7 60.2(3) . . ? B6 B11 B10 107.7(3) . . ? B6 B11 H11 121.4 . . ? B6 B11 B12 108.1(4) . . ? B7 B11 B10 107.1(3) . . ? B7 B11 H11 122.1 . . ? B10 B11 H11 122.3 . . ? B12 B11 B5 107.6(3) . . ? B12 B11 B7 59.6(3) . . ? B12 B11 B10 59.8(2) . . ? B12 B11 H11 121.8 . . ? B7 B12 B8 59.4(3) . . ? B7 B12 B10 109.2(3) . . ? B7 B12 H12 121.4 . . ? B8 B12 H12 122.5 . . ? B9 B12 B7 107.2(3) . . ? B9 B12 B8 59.3(2) . . ? B9 B12 B10 59.1(2) . . ? B9 B12 B11 108.0(3) . . ? B9 B12 H12 122.7 . . ? B10 B12 B8 107.1(3) . . ? B10 B12 H12 121.5 . . ? B11 B12 B7 61.0(3) . . ? B11 B12 B8 108.1(3) . . ? B11 B12 B10 61.1(3) . . ? B11 B12 H12 120.8 . . ? C16 O5 C12 106.79(18) . . ? C11 N2 H2A 113.7 . . ? C11 N2 B13 132.5(2) . . ? B13 N2 H2A 113.7 . . ? O4 C11 N2 125.7(2) . . ? O4 C11 C12 117.3(2) . . ? N2 C11 C12 117.0(2) . . ? O5 C12 C11 109.79(18) . . ? O5 C12 C13 104.71(19) . . ? O5 C12 C17 101.42(18) . . ? C11 C12 C13 116.7(2) . . ? C11 C12 C17 118.6(2) . . ? C13 C12 C17 103.7(2) . . ? C12 C13 H13A 111.4 . . ? C12 C13 H13B 111.4 . . ? C12 C13 C14 101.7(2) . . ? H13A C13 H13B 109.3 . . ? C14 C13 H13A 111.4 . . ? C14 C13 H13B 111.4 . . ? C13 C14 H14A 110.9 . . ? C13 C14 H14B 110.9 . . ? C13 C14 C15 104.05(19) . . ? H14A C14 H14B 109.0 . . ? C15 C14 H14A 110.9 . . ? C15 C14 H14B 110.9 . . ? C14 C15 C17 102.11(19) . . ? C16 C15 C14 102.1(2) . . ? C16 C15 C17 99.96(19) . . ? C16 C15 C18 114.5(2) . . ? C18 C15 C14 115.7(2) . . ? C18 C15 C17 119.8(2) . . ? O5 C16 C15 107.3(2) . . ? O6 C16 O5 121.1(2) . . ? O6 C16 C15 131.6(2) . . ? C12 C17 C15 92.13(18) . . ? C19 C17 C12 115.0(2) . . ? C19 C17 C15 113.6(2) . . ? C20 C17 C12 112.1(2) . . ? C20 C17 C15 113.7(2) . . ? C20 C17 C19 109.5(2) . . ? C15 C18 H18A 109.5 . . ? C15 C18 H18B 109.5 . . ? C15 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C17 C19 H19A 109.5 . . ? C17 C19 H19B 109.5 . . ? C17 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C20 H20A 109.5 . . ? C17 C20 H20B 109.5 . . ? C17 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N2 B13 B14 127.8(2) . . ? N2 B13 B15 125.9(2) . . ? N2 B13 B16 117.6(2) . . ? N2 B13 B17 114.29(19) . . ? N2 B13 B18 120.4(2) . . ? B14 B13 B16 108.76(19) . . ? B14 B13 B17 108.66(18) . . ? B14 B13 B18 60.26(15) . . ? B15 B13 B14 60.66(15) . . ? B15 B13 B16 60.17(15) . . ? B15 B13 B17 108.50(19) . . ? B15 B13 B18 108.81(18) . . ? B16 B13 B17 59.99(16) . . ? B18 B13 B16 108.3(2) . . ? B18 B13 B17 60.18(16) . . ? B13 B14 H14 122.2 . . ? B13 B14 B15 59.54(15) . . ? B13 B14 B18 59.94(15) . . ? B13 B14 B19 107.33(19) . . ? B13 B14 B20 107.16(19) . . ? B15 B14 H14 121.9 . . ? B18 B14 H14 121.9 . . ? B18 B14 B15 107.66(19) . . ? B19 B14 H14 122.0 . . ? B19 B14 B15 107.7(2) . . ? B19 B14 B18 59.69(15) . . ? B20 B14 H14 122.1 . . ? B20 B14 B15 59.89(15) . . ? B20 B14 B18 107.4(2) . . ? B20 B14 B19 59.79(16) . . ? B13 B15 B14 59.80(15) . . ? B13 B15 H15 122.1 . . ? B13 B15 B16 60.13(15) . . ? B13 B15 B20 107.24(18) . . ? B13 B15 B21 107.42(19) . . ? B14 B15 H15 121.8 . . ? B16 B15 B14 108.03(19) . . ? B16 B15 H15 121.8 . . ? B16 B15 B20 107.52(19) . . ? B16 B15 B21 59.58(15) . . ? B20 B15 B14 59.73(15) . . ? B20 B15 H15 122.1 . . ? B20 B15 B21 59.92(15) . . ? B21 B15 B14 107.75(19) . . ? B21 B15 H15 122.0 . . ? B13 B16 B15 59.70(15) . . ? B13 B16 H16 122.0 . . ? B13 B16 B17 60.03(16) . . ? B15 B16 H16 121.4 . . ? B17 B16 B15 108.16(19) . . ? B17 B16 H16 121.8 . . ? B21 B16 B13 107.67(19) . . ? B21 B16 B15 60.31(16) . . ? B21 B16 H16 121.7 . . ? B21 B16 B17 107.9(2) . . ? B21 B16 B22 60.27(16) . . ? B22 B16 B13 108.0(2) . . ? B22 B16 B15 108.73(19) . . ? B22 B16 H16 121.4 . . ? B22 B16 B17 59.89(17) . . ? B13 B17 H17 121.9 . . ? B13 B17 B18 59.87(15) . . ? B16 B17 B13 59.97(16) . . ? B16 B17 H17 121.8 . . ? B16 B17 B18 108.05(19) . . ? B18 B17 H17 121.6 . . ? B22 B17 B13 107.90(19) . . ? B22 B17 B16 59.86(17) . . ? B22 B17 H17 121.6 . . ? B22 B17 B18 108.38(19) . . ? B23 B17 B13 107.98(19) . . ? B23 B17 B16 108.12(19) . . ? B23 B17 H17 121.5 . . ? B23 B17 B18 60.19(17) . . ? B23 B17 B22 60.30(17) . . ? B13 B18 B14 59.80(15) . . ? B13 B18 B17 59.95(16) . . ? B13 B18 H18 122.1 . . ? B13 B18 B23 107.6(2) . . ? B14 B18 H18 121.5 . . ? B17 B18 B14 108.10(19) . . ? B17 B18 H18 121.9 . . ? B19 B18 B13 107.54(19) . . ? B19 B18 B14 60.10(16) . . ? B19 B18 B17 107.8(2) . . ? B19 B18 H18 121.7 . . ? B19 B18 B23 60.39(16) . . ? B23 B18 B14 108.5(2) . . ? B23 B18 B17 59.57(16) . . ? B23 B18 H18 121.7 . . ? B14 B19 H19 121.4 . . ? B14 B19 B23 108.31(19) . . ? B18 B19 B14 60.22(15) . . ? B18 B19 H19 121.7 . . ? B18 B19 B20 108.06(18) . . ? B18 B19 B23 60.04(16) . . ? B18 B19 B24 107.8(2) . . ? B20 B19 B14 60.04(15) . . ? B20 B19 H19 121.7 . . ? B20 B19 B23 108.0(2) . . ? B20 B19 B24 60.23(16) . . ? B23 B19 H19 121.8 . . ? B24 B19 B14 108.28(19) . . ? B24 B19 H19 121.8 . . ? B24 B19 B23 59.64(17) . . ? B14 B20 B15 60.39(15) . . ? B14 B20 H20 121.3 . . ? B14 B20 B21 108.38(18) . . ? B14 B20 B24 108.24(19) . . ? B15 B20 H20 121.5 . . ? B15 B20 B24 107.90(19) . . ? B19 B20 B14 60.17(16) . . ? B19 B20 B15 108.35(18) . . ? B19 B20 H20 121.6 . . ? B19 B20 B21 107.9(2) . . ? B19 B20 B24 60.04(17) . . ? B21 B20 B15 60.06(16) . . ? B21 B20 H20 121.8 . . ? B21 B20 B24 59.68(17) . . ? B24 B20 H20 121.9 . . ? B15 B21 H21 121.5 . . ? B16 B21 B15 60.12(15) . . ? B16 B21 B20 108.04(19) . . ? B16 B21 H21 121.8 . . ? B16 B21 B22 59.92(16) . . ? B16 B21 B24 108.0(2) . . ? B20 B21 B15 60.03(15) . . ? B20 B21 H21 121.6 . . ? B22 B21 B15 108.31(19) . . ? B22 B21 B20 108.4(2) . . ? B22 B21 H21 121.5 . . ? B24 B21 B15 108.3(2) . . ? B24 B21 B20 60.26(16) . . ? B24 B21 H21 121.6 . . ? B24 B21 B22 60.10(17) . . ? B16 B22 B17 60.26(16) . . ? B16 B22 B21 59.81(16) . . ? B16 B22 H22 121.7 . . ? B16 B22 B23 108.1(2) . . ? B16 B22 B24 107.7(2) . . ? B17 B22 B21 107.9(2) . . ? B17 B22 H22 121.8 . . ? B17 B22 B23 59.84(17) . . ? B17 B22 B24 107.6(2) . . ? B21 B22 H22 121.9 . . ? B21 B22 B23 107.8(2) . . ? B21 B22 B24 59.83(16) . . ? B23 B22 H22 121.8 . . ? B24 B22 H22 122.0 . . ? B24 B22 B23 59.86(17) . . ? B17 B23 B18 60.24(16) . . ? B17 B23 B19 107.7(2) . . ? B17 B23 B22 59.87(16) . . ? B17 B23 H23 121.8 . . ? B17 B23 B24 107.8(2) . . ? B18 B23 B19 59.57(16) . . ? B18 B23 H23 121.8 . . ? B19 B23 H23 122.0 . . ? B22 B23 B18 108.1(2) . . ? B22 B23 B19 107.9(2) . . ? B22 B23 H23 121.6 . . ? B24 B23 B18 107.7(2) . . ? B24 B23 B19 59.94(17) . . ? B24 B23 B22 60.03(17) . . ? B24 B23 H23 121.9 . . ? B19 B24 B20 59.73(16) . . ? B19 B24 H24 121.6 . . ? B20 B24 H24 121.8 . . ? B21 B24 B19 108.0(2) . . ? B21 B24 B20 60.06(15) . . ? B21 B24 B22 60.07(17) . . ? B21 B24 B23 108.20(19) . . ? B21 B24 H24 121.7 . . ? B22 B24 B19 108.4(2) . . ? B22 B24 B20 108.16(19) . . ? B22 B24 H24 121.5 . . ? B23 B24 B19 60.42(17) . . ? B23 B24 B20 108.2(2) . . ? B23 B24 B22 60.11(17) . . ? B23 B24 H24 121.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? C46 C45 H45A 109.5 . . ? C46 C45 H45B 109.5 . . ? C46 C45 H45C 109.5 . . ? O7 C46 C45 122.6(3) . . ? O7 C46 C47 121.0(3) . . ? C47 C46 C45 116.3(3) . . ? C46 C47 H47A 109.5 . . ? C46 C47 H47B 109.5 . . ? C46 C47 H47C 109.5 . . ? H47A C47 H47B 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? C21 N3 H3C 106.6 . . ? C23 N3 H3C 106.6 . . ? C23 N3 C21 114.6(2) . . ? C23 N3 C25 110.8(2) . . ? C25 N3 H3C 106.6 . . ? C25 N3 C21 111.2(2) . . ? N3 C21 H21A 108.6 . . ? N3 C21 H21B 108.6 . . ? H21A C21 H21B 107.5 . . ? C22 C21 N3 114.8(2) . . ? C22 C21 H21A 108.6 . . ? C22 C21 H21B 108.6 . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? N3 C23 H23A 109.1 . . ? N3 C23 H23B 109.1 . . ? N3 C23 C24 112.5(3) . . ? H23A C23 H23B 107.8 . . ? C24 C23 H23A 109.1 . . ? C24 C23 H23B 109.1 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? N3 C25 H25A 109.1 . . ? N3 C25 H25B 109.1 . . ? N3 C25 C26 112.7(3) . . ? H25A C25 H25B 107.8 . . ? C26 C25 H25A 109.1 . . ? C26 C25 H25B 109.1 . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C27 N4 H4C 106.6 . . ? C27 N4 C29 114.6(2) . . ? C27 N4 C31 113.4(2) . . ? C29 N4 H4C 106.6 . . ? C29 N4 C31 108.6(2) . . ? C31 N4 H4C 106.6 . . ? N4 C27 H27A 108.6 . . ? N4 C27 H27B 108.6 . . ? N4 C27 C28 114.6(2) . . ? H27A C27 H27B 107.6 . . ? C28 C27 H27A 108.6 . . ? C28 C27 H27B 108.6 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28B 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? N4 C29 H29A 109.2 . . ? N4 C29 H29B 109.2 . . ? N4 C29 C30 112.2(3) . . ? H29A C29 H29B 107.9 . . ? C30 C29 H29A 109.2 . . ? C30 C29 H29B 109.2 . . ? C29 C30 H30A 109.5 . . ? C29 C30 H30B 109.5 . . ? C29 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? N4 C31 H31A 108.9 . . ? N4 C31 H31B 108.9 . . ? H31A C31 H31B 107.7 . . ? C32 C31 N4 113.4(3) . . ? C32 C31 H31A 108.9 . . ? C32 C31 H31B 108.9 . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C33 N5 H5A 106.0 . . ? C33 N5 C35 107.0(3) . . ? C35 N5 H5A 106.0 . . ? C37 N5 H5A 106.0 . . ? C37 N5 C33 121.0(3) . . ? C37 N5 C35 109.9(3) . . ? N5 C33 H33A 108.5 . . ? N5 C33 H33B 108.5 . . ? N5 C33 C34 115.2(3) . . ? H33A C33 H33B 107.5 . . ? C34 C33 H33A 108.5 . . ? C34 C33 H33B 108.5 . . ? C33 C34 H34A 109.5 . . ? C33 C34 H34B 109.5 . . ? C33 C34 H34C 109.5 . . ? H34A C34 H34B 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? N5 C35 H35A 108.8 . . ? N5 C35 H35B 108.8 . . ? H35A C35 H35B 107.7 . . ? C36 C35 N5 113.7(3) . . ? C36 C35 H35A 108.8 . . ? C36 C35 H35B 108.8 . . ? C35 C36 H36A 109.5 . . ? C35 C36 H36B 109.5 . . ? C35 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? N5 C37 H37A 108.5 . . ? N5 C37 H37B 108.5 . . ? N5 C37 C38 115.0(3) . . ? H37A C37 H37B 107.5 . . ? C38 C37 H37A 108.5 . . ? C38 C37 H37B 108.5 . . ? C37 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? C37 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C39 N6 H6A 108.4 . . ? C41 N6 H6A 108.4 . . ? C41 N6 C39 101.3(5) . . ? C43 N6 H6A 108.4 . . ? C43 N6 C39 109.0(5) . . ? C43 N6 C41 120.5(5) . . ? C39A N6 H6B 107.3 . . ? C39A N6 C43A 103.1(5) . . ? C41A N6 H6B 107.3 . . ? C41A N6 C39A 123.3(8) . . ? C41A N6 C43A 107.6(9) . . ? C43A N6 H6B 107.3 . . ? N6 C39 H39A 109.8 . . ? N6 C39 H39B 109.8 . . ? H39A C39 H39B 108.2 . . ? C40 C39 N6 109.5(8) . . ? C40 C39 H39A 109.8 . . ? C40 C39 H39B 109.8 . . ? C39 C40 H40A 109.5 . . ? C39 C40 H40B 109.5 . . ? C39 C40 H40C 109.5 . . ? H40A C40 H40B 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? N6 C41 H41A 107.4 . . ? N6 C41 H41B 107.4 . . ? H41A C41 H41B 106.9 . . ? C42 C41 N6 119.8(6) . . ? C42 C41 H41A 107.4 . . ? C42 C41 H41B 107.4 . . ? C41 C42 H42A 109.5 . . ? C41 C42 H42B 109.5 . . ? C41 C42 H42C 109.5 . . ? H42A C42 H42B 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? N6 C43 H43A 110.4 . . ? N6 C43 H43B 110.4 . . ? N6 C43 C44 106.8(9) . . ? H43A C43 H43B 108.6 . . ? C44 C43 H43A 110.4 . . ? C44 C43 H43B 110.4 . . ? C43 C44 H44A 109.5 . . ? C43 C44 H44B 109.5 . . ? C43 C44 H44C 109.5 . . ? H44A C44 H44B 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? N6 C39A H39C 111.6 . . ? N6 C39A H39D 111.6 . . ? N6 C39A C40A 100.7(10) . . ? H39C C39A H39D 109.4 . . ? C40A C39A H39C 111.6 . . ? C40A C39A H39D 111.6 . . ? C39A C40A H40D 109.5 . . ? C39A C40A H40E 109.5 . . ? C39A C40A H40F 109.5 . . ? H40D C40A H40E 109.5 . . ? H40D C40A H40F 109.5 . . ? H40E C40A H40F 109.5 . . ? N6 C41A H41C 109.5 . . ? N6 C41A H41D 109.5 . . ? N6 C41A C42A 110.7(9) . . ? H41C C41A H41D 108.1 . . ? C42A C41A H41C 109.5 . . ? C42A C41A H41D 109.5 . . ? C41A C42A H42D 109.5 . . ? C41A C42A H42E 109.5 . . ? C41A C42A H42F 109.5 . . ? H42D C42A H42E 109.5 . . ? H42D C42A H42F 109.5 . . ? H42E C42A H42F 109.5 . . ? N6 C43A H43C 108.6 . . ? N6 C43A H43D 108.6 . . ? H43C C43A H43D 107.6 . . ? C44A C43A N6 114.6(9) . . ? C44A C43A H43C 108.6 . . ? C44A C43A H43D 108.6 . . ? C43A C44A H44D 109.5 . . ? C43A C44A H44E 109.5 . . ? C43A C44A H44F 109.5 . . ? H44D C44A H44E 109.5 . . ? H44D C44A H44F 109.5 . . ? H44E C44A H44F 109.5 . . ? _shelx_res_file ; TITL 191227_b12c_0m_a.res in P2(1) 191227_b12c_0m.res created by SHELXL-2016/6 at 10:11:18 on 30-Dec-2019 REM Old TITL 191227_b12c_0m_a.res in P2(1) REM SHELXT solution in P2(1) REM R1 0.154, Rweak 0.023, Alpha 0.008, Orientation as input REM Flack x = 0.090 ( 0.024 ) from Parsons' quotients REM Formula found by SHELXT: C52 B22 N4 O8 CELL 1.54178 18.2099 10.1365 19.5538 90 103.548 90 ZERR 2 0.0005 0.0003 0.0005 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H B N O UNIT 94 240 48 12 14 SADI N6 C41 N6 C41A SADI N6 C39 N6 C39A SADI N6 C43 N6 C43A SADI C40 C39 C40 C39A SADI C41 C42 C41A C42 SADI C44 C43 C44 C43A L.S. 4 0 0 PLAN 20 SIZE 0.1 0.18 0.48 TEMP -103.15 BOND $H htab list 4 fmap 2 53 acta REM REM REM WGHT 0.098800 0.808100 FVAR 0.88734 0.50180 O1 5 1.059460 0.622171 0.702980 11.00000 0.04176 0.03657 = 0.03960 0.00096 -0.00435 -0.00924 O2 5 0.943695 0.475422 0.547509 11.00000 0.04543 0.02291 = 0.02820 0.00166 0.00136 -0.00505 O3 5 0.854196 0.464707 0.447668 11.00000 0.05748 0.04579 = 0.03318 0.00159 -0.00223 -0.01796 N1 4 1.009208 0.417184 0.678775 11.00000 0.06610 0.02422 = 0.02626 0.00169 -0.00350 -0.00261 AFIX 43 H1 2 0.987315 0.368305 0.642527 11.00000 -1.20000 AFIX 0 C1 1 1.022095 0.539680 0.662513 11.00000 0.02957 0.02813 = 0.03031 0.00159 0.00282 0.00314 C2 1 0.987932 0.584055 0.587788 11.00000 0.02851 0.02110 = 0.03050 0.00048 0.00297 -0.00146 C3 1 1.043116 0.625706 0.543951 11.00000 0.03102 0.03781 = 0.03693 0.00511 0.00854 0.00285 AFIX 23 H3A 2 1.071053 0.549008 0.531531 11.00000 -1.20000 H3B 2 1.079634 0.691945 0.568983 11.00000 -1.20000 AFIX 0 C4 1 0.989760 0.685484 0.478325 11.00000 0.03867 0.03611 = 0.03675 0.00912 0.00631 -0.00437 AFIX 23 H4A 2 0.991181 0.633911 0.435659 11.00000 -1.20000 H4B 2 1.003547 0.778115 0.471247 11.00000 -1.20000 AFIX 0 C5 1 0.910545 0.677298 0.495100 11.00000 0.03215 0.03155 = 0.03374 0.00634 0.00131 -0.00109 C6 1 0.895590 0.531257 0.490800 11.00000 0.03575 0.03344 = 0.02839 0.00384 0.00245 -0.00509 C7 1 0.928588 0.696754 0.576158 11.00000 0.02697 0.02685 = 0.03521 0.00182 0.00270 0.00481 C8 1 0.849780 0.758907 0.447857 11.00000 0.04690 0.04485 = 0.05180 0.01322 -0.01081 0.00703 AFIX 137 H8A 2 0.847499 0.737010 0.398588 11.00000 -1.50000 H8B 2 0.861532 0.852811 0.455808 11.00000 -1.50000 H8C 2 0.800898 0.739830 0.458536 11.00000 -1.50000 AFIX 0 C9 1 0.862122 0.664854 0.609346 11.00000 0.03181 0.06099 = 0.04786 -0.00386 0.01139 0.00178 AFIX 137 H9A 2 0.838675 0.581682 0.590008 11.00000 -1.50000 H9B 2 0.824733 0.735998 0.598779 11.00000 -1.50000 H9C 2 0.880545 0.656524 0.660429 11.00000 -1.50000 AFIX 0 C10 1 0.959868 0.832650 0.600554 11.00000 0.04996 0.02538 = 0.04981 -0.00237 0.00011 0.00714 AFIX 137 H10A 2 0.976732 0.833493 0.651967 11.00000 -1.50000 H10B 2 0.920314 0.899152 0.585523 11.00000 -1.50000 H10C 2 1.002674 0.852699 0.579861 11.00000 -1.50000 AFIX 0 B1 3 1.025328 0.344632 0.749008 11.00000 0.03801 0.02809 = 0.02622 0.00109 0.00205 0.00383 B2 3 0.967393 0.374011 0.807902 11.00000 0.05177 0.13308 = 0.02799 0.00947 0.00352 0.05628 AFIX 153 H2 2 0.923539 0.453651 0.798435 11.00000 -1.20000 AFIX 0 B3 3 1.064337 0.409712 0.833867 11.00000 0.08589 0.03226 = 0.03091 -0.00310 -0.00712 0.00987 AFIX 153 H3 2 1.085220 0.513797 0.841888 11.00000 -1.20000 AFIX 0 B4 3 1.114338 0.289132 0.798090 11.00000 0.02889 0.05935 = 0.02847 0.00696 0.00323 -0.00076 AFIX 153 H4 2 1.168046 0.313842 0.782379 11.00000 -1.20000 AFIX 0 B5 3 1.048639 0.176240 0.749625 11.00000 0.06809 0.02534 = 0.02702 0.00111 -0.00103 0.00498 AFIX 153 H5 2 1.058875 0.125056 0.701950 11.00000 -1.20000 AFIX 0 B6 3 0.957060 0.226743 0.756180 11.00000 0.03797 0.09375 = 0.03322 0.02027 -0.00558 -0.02369 AFIX 153 H6 2 0.906079 0.207838 0.712588 11.00000 -1.20000 AFIX 0 B7 3 0.952498 0.221476 0.846068 11.00000 0.03077 0.19906 = 0.03682 0.03371 -0.00180 -0.02523 AFIX 153 H7 2 0.898700 0.200725 0.862487 11.00000 -1.20000 AFIX 0 B8 3 1.019931 0.333411 0.893536 11.00000 0.05006 0.09612 = 0.02662 0.00551 0.00616 0.03570 AFIX 153 H8 2 1.011401 0.386499 0.941312 11.00000 -1.20000 AFIX 0 B9 3 1.109524 0.277608 0.887284 11.00000 0.03015 0.03920 = 0.02437 0.00294 -0.00016 0.00251 AFIX 153 H9 2 1.160354 0.293080 0.931519 11.00000 -1.20000 AFIX 0 B10 3 1.101248 0.135241 0.835902 11.00000 0.07109 0.03554 = 0.02876 0.00176 0.00160 0.02051 AFIX 153 H10 2 1.146153 0.057413 0.845329 11.00000 -1.20000 AFIX 0 B11 3 1.001838 0.096831 0.809270 11.00000 0.11847 0.06958 = 0.03845 0.02122 -0.02610 -0.06475 AFIX 153 H11 2 0.980569 -0.006981 0.800906 11.00000 -1.20000 AFIX 0 B12 3 1.040630 0.160247 0.894254 11.00000 0.04878 0.06475 = 0.02933 0.01638 -0.00470 -0.02217 AFIX 153 H12 2 1.044882 0.097288 0.942093 11.00000 -1.20000 AFIX 0 O4 5 0.450914 0.633188 0.291885 11.00000 0.03518 0.03210 = 0.02713 -0.00243 -0.00235 0.01053 O5 5 0.568203 0.503976 0.451722 11.00000 0.04138 0.02271 = 0.02058 -0.00062 -0.00124 0.00576 O6 5 0.656435 0.505249 0.552794 11.00000 0.06515 0.04237 = 0.02637 -0.00095 -0.00891 0.01896 N2 4 0.507696 0.433941 0.321595 11.00000 0.03576 0.02744 = 0.01982 -0.00148 -0.00110 0.00587 AFIX 43 H2A 2 0.539137 0.395442 0.357034 11.00000 -1.20000 AFIX 0 C11 1 0.490393 0.556052 0.334882 11.00000 0.02243 0.02601 = 0.02265 -0.00282 0.00381 0.00143 C12 1 0.521674 0.606979 0.408846 11.00000 0.02699 0.01982 = 0.02281 0.00025 0.00401 0.00412 C13 1 0.463932 0.646248 0.450895 11.00000 0.02804 0.04073 = 0.02790 -0.00838 0.00831 -0.00204 AFIX 23 H13A 2 0.438332 0.567940 0.464761 11.00000 -1.20000 H13B 2 0.425543 0.707553 0.423934 11.00000 -1.20000 AFIX 0 C14 1 0.514719 0.715023 0.515813 11.00000 0.03344 0.04089 = 0.02914 -0.01248 0.00509 0.00439 AFIX 23 H14A 2 0.513567 0.666924 0.559614 11.00000 -1.20000 H14B 2 0.498239 0.807141 0.519988 11.00000 -1.20000 AFIX 0 C15 1 0.595111 0.710785 0.501112 11.00000 0.02963 0.02592 = 0.02364 -0.00462 0.00031 0.00102 C16 1 0.613509 0.566343 0.508159 11.00000 0.03758 0.02932 = 0.02118 -0.00297 0.00068 0.00689 C17 1 0.577541 0.725138 0.419573 11.00000 0.02738 0.02708 = 0.02638 0.00020 0.00166 -0.00264 C18 1 0.653349 0.799478 0.546899 11.00000 0.04095 0.03636 = 0.03868 -0.00945 -0.00654 -0.00234 AFIX 137 H18A 2 0.658168 0.776729 0.596466 11.00000 -1.50000 H18B 2 0.637403 0.891681 0.539079 11.00000 -1.50000 H18C 2 0.702193 0.787466 0.534807 11.00000 -1.50000 AFIX 0 C19 1 0.542180 0.858247 0.392898 11.00000 0.05017 0.02695 = 0.04144 0.00609 -0.00511 -0.00405 AFIX 137 H19A 2 0.524725 0.855516 0.341549 11.00000 -1.50000 H19B 2 0.579958 0.928209 0.406302 11.00000 -1.50000 H19C 2 0.499250 0.876112 0.413788 11.00000 -1.50000 AFIX 0 C20 1 0.645718 0.698452 0.388205 11.00000 0.03274 0.06497 = 0.03420 0.00381 0.00954 -0.00661 AFIX 137 H20A 2 0.671561 0.618252 0.409204 11.00000 -1.50000 H20B 2 0.680664 0.773299 0.398146 11.00000 -1.50000 H20C 2 0.628537 0.686735 0.337203 11.00000 -1.50000 AFIX 0 B13 3 0.483885 0.346592 0.256907 11.00000 0.02689 0.02425 = 0.01971 -0.00255 0.00361 0.00160 B14 3 0.463144 0.395280 0.167036 11.00000 0.03040 0.02697 = 0.01960 0.00253 0.00465 0.00153 AFIX 153 H14 2 0.462949 0.501210 0.150707 11.00000 -1.20000 AFIX 0 B15 3 0.390574 0.328028 0.204924 11.00000 0.02365 0.03036 = 0.02195 0.00012 0.00470 0.00120 AFIX 153 H15 2 0.342563 0.389822 0.213560 11.00000 -1.20000 AFIX 0 B16 3 0.431632 0.201098 0.264835 11.00000 0.03122 0.02719 = 0.02351 0.00187 0.00297 -0.00216 AFIX 153 H16 2 0.410560 0.179520 0.313075 11.00000 -1.20000 AFIX 0 B17 3 0.529258 0.189652 0.264788 11.00000 0.03069 0.02695 = 0.02291 -0.00295 -0.00076 0.00501 AFIX 153 H17 2 0.572821 0.160821 0.313045 11.00000 -1.20000 AFIX 0 B18 3 0.548797 0.309137 0.204242 11.00000 0.02503 0.03305 = 0.02513 -0.00324 0.00437 -0.00025 AFIX 153 H18 2 0.605144 0.358738 0.212389 11.00000 -1.20000 AFIX 0 B19 3 0.495191 0.266549 0.118936 11.00000 0.02950 0.03712 = 0.02140 -0.00156 0.00553 0.00169 AFIX 153 H19 2 0.516013 0.287897 0.070536 11.00000 -1.20000 AFIX 0 B20 3 0.397845 0.278203 0.119196 11.00000 0.02752 0.02512 = 0.01891 0.00054 0.00169 -0.00057 AFIX 153 H20 2 0.354340 0.307309 0.070952 11.00000 -1.20000 AFIX 0 B21 3 0.378576 0.158696 0.179597 11.00000 0.03218 0.02684 = 0.02633 0.00243 -0.00180 -0.00443 AFIX 153 H21 2 0.322254 0.108907 0.171108 11.00000 -1.20000 AFIX 0 B22 3 0.463973 0.073375 0.217167 11.00000 0.04315 0.02311 = 0.02586 -0.00034 -0.00226 0.00289 AFIX 153 H22 2 0.464201 -0.032394 0.233783 11.00000 -1.20000 AFIX 0 B23 3 0.536344 0.139494 0.179624 11.00000 0.03408 0.03309 = 0.02596 -0.00570 0.00208 0.01022 AFIX 153 H23 2 0.584366 0.077256 0.171405 11.00000 -1.20000 AFIX 0 B24 3 0.443085 0.120673 0.126938 11.00000 0.03701 0.03061 = 0.02347 -0.00687 -0.00069 0.00427 AFIX 153 H24 2 0.429514 0.045718 0.083728 11.00000 -1.20000 AFIX 0 O7 5 0.758884 0.036871 0.490647 11.00000 0.10448 0.03743 = 0.08482 -0.01072 0.01852 -0.00163 C45 1 0.693809 0.239301 0.463287 11.00000 0.04798 0.07275 = 0.04985 -0.00809 0.01144 0.01219 AFIX 137 H45A 2 0.659388 0.187119 0.427336 11.00000 -1.50000 H45B 2 0.714755 0.311893 0.440726 11.00000 -1.50000 H45C 2 0.666110 0.275258 0.496430 11.00000 -1.50000 AFIX 0 C46 1 0.756254 0.153810 0.501764 11.00000 0.04516 0.03499 = 0.04020 -0.00250 0.02092 -0.00461 C47 1 0.817311 0.220434 0.553865 11.00000 0.04891 0.06363 = 0.05444 -0.00189 0.01669 -0.01594 AFIX 137 H47A 2 0.849099 0.154012 0.583115 11.00000 -1.50000 H47B 2 0.795028 0.278244 0.583743 11.00000 -1.50000 H47C 2 0.848151 0.273072 0.529167 11.00000 -1.50000 AFIX 0 N3 4 0.803317 0.231648 0.257325 11.00000 0.03318 0.03231 = 0.03593 0.00431 0.00245 0.00352 AFIX 13 H3C 2 0.849691 0.175745 0.263863 11.00000 -1.20000 AFIX 0 C21 1 0.829983 0.371251 0.274918 11.00000 0.03582 0.03538 = 0.03935 0.00235 -0.00310 -0.00315 AFIX 23 H21A 2 0.861237 0.373037 0.323711 11.00000 -1.20000 H21B 2 0.862748 0.397482 0.243357 11.00000 -1.20000 AFIX 0 C22 1 0.767682 0.471878 0.268563 11.00000 0.04799 0.03408 = 0.05175 -0.00172 -0.00081 0.00490 AFIX 137 H22A 2 0.736894 0.472557 0.220197 11.00000 -1.50000 H22B 2 0.789808 0.559441 0.280471 11.00000 -1.50000 H22C 2 0.735882 0.448990 0.300896 11.00000 -1.50000 AFIX 0 C23 1 0.759981 0.211728 0.182997 11.00000 0.05329 0.04409 = 0.03974 -0.00405 0.00091 -0.00026 AFIX 23 H23A 2 0.713198 0.265139 0.174458 11.00000 -1.20000 H23B 2 0.745155 0.117823 0.176088 11.00000 -1.20000 AFIX 0 C24 1 0.804912 0.249903 0.130217 11.00000 0.08846 0.06209 = 0.04622 0.00074 0.02378 0.00690 AFIX 137 H24A 2 0.776163 0.227436 0.082730 11.00000 -1.50000 H24B 2 0.853000 0.202013 0.140543 11.00000 -1.50000 H24C 2 0.814735 0.345038 0.133122 11.00000 -1.50000 AFIX 0 C25 1 0.759541 0.181072 0.308126 11.00000 0.03719 0.04517 = 0.04918 0.00975 0.00908 0.00199 AFIX 23 H25A 2 0.708314 0.220227 0.296349 11.00000 -1.20000 H25B 2 0.784850 0.209962 0.356239 11.00000 -1.20000 AFIX 0 C26 1 0.752756 0.033278 0.307061 11.00000 0.06242 0.04499 = 0.06006 0.01639 0.01146 -0.00327 AFIX 137 H26A 2 0.718822 0.005313 0.262809 11.00000 -1.50000 H26B 2 0.732301 0.004273 0.346676 11.00000 -1.50000 H26C 2 0.802720 -0.006122 0.311004 11.00000 -1.50000 AFIX 0 N4 4 0.614848 0.769443 0.061532 11.00000 0.03148 0.04091 = 0.02204 0.00126 0.00450 -0.00109 AFIX 13 H4C 2 0.590601 0.759474 0.010342 11.00000 -1.20000 AFIX 0 C27 1 0.552731 0.759469 0.099841 11.00000 0.03380 0.05717 = 0.03679 0.00607 0.01085 -0.00088 AFIX 23 H27A 2 0.521961 0.680428 0.082716 11.00000 -1.20000 H27B 2 0.519553 0.837575 0.087949 11.00000 -1.20000 AFIX 0 C28 1 0.579396 0.750699 0.179111 11.00000 0.06043 0.04974 = 0.03291 0.00023 0.02092 0.00055 AFIX 137 H28A 2 0.608592 0.669468 0.191802 11.00000 -1.50000 H28B 2 0.535581 0.749892 0.200179 11.00000 -1.50000 H28C 2 0.611271 0.827063 0.196645 11.00000 -1.50000 AFIX 0 C29 1 0.674035 0.662765 0.079583 11.00000 0.04877 0.04879 = 0.04114 0.00891 0.01385 0.01669 AFIX 23 H29A 2 0.704166 0.676564 0.128204 11.00000 -1.20000 H29B 2 0.708632 0.669481 0.047505 11.00000 -1.20000 AFIX 0 C30 1 0.639608 0.525762 0.073722 11.00000 0.10015 0.04151 = 0.03557 0.00388 0.00465 0.00915 AFIX 137 H30A 2 0.603327 0.516685 0.028247 11.00000 -1.50000 H30B 2 0.613640 0.512423 0.111776 11.00000 -1.50000 H30C 2 0.679615 0.459667 0.077358 11.00000 -1.50000 AFIX 0 C31 1 0.654080 0.902298 0.069990 11.00000 0.05109 0.04316 = 0.03690 -0.00047 0.01129 -0.00622 AFIX 23 H31A 2 0.668044 0.925419 0.120574 11.00000 -1.20000 H31B 2 0.701309 0.895248 0.053431 11.00000 -1.20000 AFIX 0 C32 1 0.606662 1.011122 0.030409 11.00000 0.08204 0.03561 = 0.03499 -0.00460 0.01649 0.00208 AFIX 137 H32A 2 0.593086 0.989606 -0.019843 11.00000 -1.50000 H32B 2 0.635301 1.093842 0.037509 11.00000 -1.50000 H32C 2 0.560608 1.021042 0.047691 11.00000 -1.50000 AFIX 0 N5 4 0.312700 0.745468 0.248989 11.00000 0.02783 0.03579 = 0.04623 0.00040 -0.00630 0.00554 AFIX 13 H5A 2 0.363206 0.701394 0.261602 11.00000 -1.20000 AFIX 0 C33 1 0.318072 0.860120 0.296442 11.00000 0.04003 0.05329 = 0.04772 -0.01547 -0.01020 0.01257 AFIX 23 H33A 2 0.361545 0.914877 0.291488 11.00000 -1.20000 H33B 2 0.328805 0.827644 0.345533 11.00000 -1.20000 AFIX 0 C34 1 0.248788 0.946527 0.284045 11.00000 0.05015 0.06744 = 0.04922 -0.01684 -0.00293 0.02615 AFIX 137 H34A 2 0.239553 0.984729 0.236756 11.00000 -1.50000 H34B 2 0.256714 1.017508 0.319037 11.00000 -1.50000 H34C 2 0.205075 0.893495 0.288285 11.00000 -1.50000 AFIX 0 C35 1 0.304297 0.800557 0.173366 11.00000 0.05832 0.06010 = 0.04803 0.00394 -0.00127 0.01113 AFIX 23 H35A 2 0.249882 0.807805 0.150441 11.00000 -1.20000 H35B 2 0.326070 0.890466 0.176535 11.00000 -1.20000 AFIX 0 C36 1 0.340290 0.721140 0.130164 11.00000 0.06770 0.08070 = 0.05130 0.01766 0.00878 -0.00675 AFIX 137 H36A 2 0.333244 0.761784 0.083602 11.00000 -1.50000 H36B 2 0.317867 0.632746 0.125301 11.00000 -1.50000 H36C 2 0.394389 0.714541 0.152022 11.00000 -1.50000 AFIX 0 C37 1 0.256659 0.640600 0.248591 11.00000 0.04611 0.05261 = 0.06433 -0.00317 0.00721 0.00157 AFIX 23 H37A 2 0.254597 0.583729 0.207022 11.00000 -1.20000 H37B 2 0.206352 0.681925 0.243094 11.00000 -1.20000 AFIX 0 C38 1 0.271605 0.555692 0.312619 11.00000 0.07278 0.05140 = 0.05836 0.01182 0.03412 0.01172 AFIX 137 H38A 2 0.231438 0.489676 0.308127 11.00000 -1.50000 H38B 2 0.272869 0.610480 0.354173 11.00000 -1.50000 H38C 2 0.320332 0.511105 0.317646 11.00000 -1.50000 AFIX 0 N6 4 0.113790 0.252530 0.067271 11.00000 0.03629 0.11850 = 0.02703 -0.00005 0.00284 -0.01326 PART 1 AFIX 13 H6A 2 0.097260 0.243488 0.014987 21.00000 -1.20000 AFIX 13 PART 0 PART 2 H6B 2 0.094553 0.262280 0.015256 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C39 1 0.120201 0.414356 0.087449 21.00000 0.05963 0.05419 = 0.03770 -0.00651 0.00938 0.01329 AFIX 23 H39A 2 0.069674 0.455764 0.073272 21.00000 -1.20000 H39B 2 0.138980 0.425587 0.138878 21.00000 -1.20000 AFIX 0 C40 1 0.175413 0.482512 0.048317 21.00000 0.07778 0.06577 = 0.05301 -0.02785 0.03799 -0.04385 AFIX 137 H40A 2 0.226401 0.446872 0.065728 21.00000 -1.50000 H40B 2 0.175932 0.577784 0.056940 21.00000 -1.50000 H40C 2 0.158587 0.465692 -0.002298 21.00000 -1.50000 AFIX 0 C41 1 0.051112 0.211754 0.098050 21.00000 0.04463 0.03841 = 0.04693 0.01565 0.01880 0.00490 AFIX 23 H41A 2 0.050548 0.114105 0.098733 21.00000 -1.20000 H41B 2 0.063324 0.241414 0.147668 21.00000 -1.20000 AFIX 0 C42 1 -0.024821 0.255153 0.066543 21.00000 0.05119 0.06958 = 0.07869 -0.00231 0.04577 -0.00873 AFIX 137 H42A 2 -0.033902 0.340610 0.086510 21.00000 -1.50000 H42B 2 -0.061009 0.190242 0.076145 21.00000 -1.50000 H42C 2 -0.031076 0.264054 0.015595 21.00000 -1.50000 AFIX 0 C43 1 0.184888 0.194931 0.089562 21.00000 0.04527 0.05917 = 0.04854 -0.00475 -0.00617 0.01346 AFIX 23 H43A 2 0.201206 0.196482 0.141541 21.00000 -1.20000 H43B 2 0.222548 0.243498 0.070084 21.00000 -1.20000 AFIX 0 C44 1 0.177938 0.056286 0.063433 -21.00000 0.09430 0.06464 = 0.06338 -0.00585 -0.04363 0.02819 AFIX 137 H44A 2 0.143143 0.007756 0.085618 -21.00000 -1.50000 H44B 2 0.227674 0.013877 0.075228 -21.00000 -1.50000 H44C 2 0.158426 0.056071 0.012275 -21.00000 -1.50000 AFIX 0 PART 0 PART 2 C39A 1 0.185772 0.317039 0.086135 -21.00000 0.05255 0.06140 = 0.04424 -0.00359 -0.00645 -0.00704 AFIX 23 H39C 2 0.220901 0.282802 0.058630 -21.00000 -1.20000 H39D 2 0.209166 0.307988 0.136985 -21.00000 -1.20000 AFIX 0 C40A 1 0.162235 0.462884 0.066003 -21.00000 0.12296 0.10595 = 0.07395 -0.01822 0.00634 0.01286 AFIX 137 H40D 2 0.137073 0.467528 0.015937 -21.00000 -1.50000 H40E 2 0.207322 0.518971 0.075331 -21.00000 -1.50000 H40F 2 0.127560 0.493558 0.094123 -21.00000 -1.50000 AFIX 0 C41A 1 0.052884 0.282682 0.098928 -21.00000 0.07087 0.17643 = 0.04187 -0.02096 0.01730 0.04046 AFIX 23 H41C 2 0.006232 0.239436 0.072113 -21.00000 -1.20000 H41D 2 0.044204 0.379162 0.097384 -21.00000 -1.20000 AFIX 0 C42A 1 0.071750 0.231257 0.182150 -21.00000 0.11116 0.08333 = 0.04698 0.00508 0.03813 0.01008 AFIX 137 H42D 2 0.087744 0.138734 0.184344 -21.00000 -1.50000 H42E 2 0.026319 0.239502 0.200554 -21.00000 -1.50000 H42F 2 0.112284 0.285288 0.210502 -21.00000 -1.50000 AFIX 0 C43A 1 0.136051 0.092355 0.083476 -21.00000 0.06263 0.07707 = 0.03408 0.01354 0.00074 -0.01680 AFIX 23 H43C 2 0.158730 0.081722 0.134373 -21.00000 -1.20000 H43D 2 0.088949 0.039747 0.072142 -21.00000 -1.20000 AFIX 0 C44A 1 0.191145 0.035946 0.041994 21.00000 0.08035 0.05790 = 0.03253 0.00897 -0.01216 0.00045 AFIX 137 H44D 2 0.177281 0.068431 -0.006535 21.00000 -1.50000 H44E 2 0.188505 -0.060619 0.041952 21.00000 -1.50000 H44F 2 0.242701 0.064136 0.064174 21.00000 -1.50000 AFIX 0 HKLF 4 REM 191227_b12c_0m_a.res in P2(1) REM R1 = 0.0526 for 12514 Fo > 4sig(Fo) and 0.0536 for all 12833 data REM 835 parameters refined using 4 restraints END WGHT 0.0988 0.8081 REM Instructions for potential hydrogen bonds HTAB N1 O2 HTAB N2 O5 HTAB C45 O6 HTAB C47 O2 HTAB C47 O3 EQIV $1 -x+2, y-1/2, -z+1 HTAB N3 O1_$1 HTAB C21 O3 HTAB N5 O4 EQIV $2 -x+1, y+1/2, -z+1 HTAB C33 O6_$2 HTAB C34 O6_$2 REM Highest difference peak 0.875, deepest hole -0.264, 1-sigma level 0.046 Q1 1 0.2548 0.6902 0.3073 11.00000 0.05 0.88 Q2 1 0.2717 0.7204 0.1863 11.00000 0.05 0.83 Q3 1 1.0022 0.2590 0.8821 11.00000 0.05 0.28 Q4 1 0.2670 1.0086 0.2580 11.00000 0.05 0.24 Q5 1 0.4389 0.6110 0.3025 11.00000 0.05 0.23 Q6 1 0.9154 0.7062 0.5385 11.00000 0.05 0.23 Q7 1 0.2376 0.5214 0.2965 11.00000 0.05 0.23 Q8 1 0.9574 0.1333 0.8089 11.00000 0.05 0.22 Q9 1 0.7416 0.0514 0.5150 11.00000 0.05 0.22 Q10 1 0.6924 0.5672 0.0554 11.00000 0.05 0.22 Q11 1 0.9986 0.4231 0.6948 11.00000 0.05 0.21 Q12 1 0.5906 0.7238 0.4623 11.00000 0.05 0.20 Q13 1 1.0234 0.0566 0.7838 11.00000 0.05 0.20 Q14 1 0.9978 0.4584 0.6820 11.00000 0.05 0.20 Q15 1 0.6209 0.7135 0.0677 11.00000 0.05 0.20 Q16 1 0.9532 0.2941 0.8040 11.00000 0.05 0.20 Q17 1 0.4835 0.0895 0.1815 11.00000 0.05 0.20 Q18 1 0.4652 0.1654 0.2512 11.00000 0.05 0.20 Q19 1 0.1193 0.1855 0.0669 11.00000 0.05 0.20 Q20 1 0.5532 0.8044 0.4071 11.00000 0.05 0.20 ; _shelx_res_checksum 19651 _shelx_hkl_file ; 1 0 0 29.70 1.20 1 0 0 31.90 1.40 -1 0 0 28.60 1.30 -1 0 0 27.70 1.20 -1 0 0 30.80 1.10 -1 0 0 29.10 1.20 -3 0 0 124.09 5.00 3 0 0 123.89 4.90 3 0 0 124.79 5.00 3 0 0 123.29 4.40 4 0 0 3580.04 117.89 4 0 0 3643.14 116.99 -4 0 0 3671.73 117.99 -5 0 0 376.56 13.70 5 0 0 366.06 12.40 5 0 0 383.56 13.70 6 0 0 1050.99 36.00 6 0 0 1077.59 35.20 -6 0 0 1052.49 36.10 7 0 0 206.98 8.90 -7 0 0 215.38 9.20 7 0 0 216.98 8.10 8 0 0 1.70 0.80 -8 0 0 -0.70 1.10 9 0 0 49.40 6.00 -9 0 0 52.99 4.30 10 0 0 1230.18 41.20 -10 0 0 1202.38 43.30 11 0 0 217.28 10.10 -11 0 0 208.48 10.90 11 0 0 211.78 9.00 -12 0 0 11.90 2.10 -12 0 0 13.90 3.30 -12 0 0 11.30 1.60 12 0 0 16.20 2.30 12 0 0 14.50 2.80 13 0 0 0.70 1.30 -13 0 0 -1.70 1.70 -13 0 0 -0.30 1.30 13 0 0 2.80 2.20 -13 0 0 -0.30 0.90 -14 0 0 879.91 32.30 14 0 0 1099.59 37.90 14 0 0 1004.30 34.30 14 0 0 809.72 35.70 14 0 0 935.31 33.60 -14 0 0 955.70 37.30 -14 0 0 905.21 33.20 -14 0 0 931.81 32.50 -15 0 0 -2.70 1.50 15 0 0 -1.20 2.00 -15 0 0 -1.00 1.10 15 0 0 1.10 2.70 15 0 0 -2.20 2.70 15 0 0 2.90 3.50 -15 0 0 1.20 3.40 -16 0 0 136.19 7.40 -16 0 0 154.08 7.30 16 0 0 145.39 10.10 16 0 0 130.29 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93.89 9.10 -14 3 0 92.69 6.40 -14 3 0 94.29 6.30 15 -3 0 108.09 6.30 15 -3 0 100.09 7.70 -15 -3 0 96.49 4.90 -15 3 0 91.49 6.40 -15 3 0 103.19 6.10 16 -3 0 95.69 7.70 16 -3 0 107.29 7.90 -16 -3 0 86.29 4.70 16 -3 0 103.59 8.20 16 -3 0 91.09 6.10 -16 3 0 94.99 5.40 16 3 0 87.59 6.70 -16 3 0 99.59 5.80 -16 3 0 93.49 6.40 -16 3 0 90.29 6.30 -17 -3 0 101.39 5.30 17 -3 0 121.19 7.30 17 -3 0 111.49 7.00 17 -3 0 101.29 8.60 17 -3 0 114.79 8.50 -17 3 0 109.79 5.90 -17 3 0 116.29 6.30 -17 3 0 108.79 6.70 -17 3 0 111.49 6.90 18 -3 0 41.90 6.00 18 -3 0 54.59 5.10 -18 -3 0 53.29 3.30 18 -3 0 38.80 6.70 -18 3 0 55.99 3.80 -18 3 0 49.50 4.30 -18 3 0 56.49 4.70 18 3 0 49.90 5.00 -18 3 0 53.29 4.40 19 -3 0 91.29 7.60 -19 -3 0 97.79 4.80 19 -3 0 102.99 6.30 19 -3 0 85.99 5.40 19 3 0 102.09 6.10 -19 3 0 90.69 4.90 -19 3 0 104.09 5.00 -19 3 0 103.39 5.80 20 -3 0 3.40 3.70 20 -3 0 0.80 1.90 20 -3 0 8.10 2.70 -20 -3 0 1.00 0.90 -20 3 0 2.80 1.10 -20 3 0 0.60 1.00 0 -4 0 4859.91 162.08 0 -4 0 4846.92 160.98 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556.54 22.80 5 4 0 551.74 20.10 -5 4 0 546.75 20.70 -6 -4 0 731.83 26.40 6 -4 0 757.72 27.70 -6 -4 0 755.02 29.00 6 -4 0 781.02 29.40 6 4 0 782.92 29.80 6 4 0 752.32 27.00 -6 4 0 768.72 29.20 -6 4 0 772.12 26.90 -7 -4 0 261.87 13.00 -7 -4 0 252.07 10.40 7 -4 0 269.47 11.50 7 -4 0 269.77 13.20 7 4 0 259.97 11.00 7 4 0 253.57 12.90 8 -4 0 198.68 11.00 8 -4 0 195.38 9.20 -8 -4 0 192.08 11.10 -8 -4 0 195.58 8.70 8 -4 0 188.88 8.90 8 4 0 206.18 10.90 -8 4 0 183.18 9.60 -8 4 0 189.78 10.90 8 4 0 186.78 9.20 9 -4 0 12.70 2.40 -9 -4 0 20.70 2.60 9 -4 0 14.10 3.70 9 -4 0 11.20 3.20 9 4 0 11.70 2.40 -9 4 0 18.20 2.20 9 4 0 11.20 2.80 -9 4 0 10.50 3.10 10 -4 0 1002.30 34.10 10 -4 0 1005.30 34.40 10 -4 0 966.10 37.70 -10 -4 0 920.71 34.00 -10 4 0 968.20 34.60 -10 4 0 968.80 38.10 10 4 0 951.40 35.20 -10 4 0 928.61 33.10 10 4 0 920.71 35.80 11 -4 0 339.77 17.60 11 -4 0 356.26 14.50 11 -4 0 353.36 14.50 -11 4 0 331.37 13.60 11 4 0 311.67 17.60 -11 4 0 348.97 18.70 -11 4 0 405.16 24.00 -11 4 0 343.47 14.90 12 -4 0 330.27 18.30 12 -4 0 274.87 10.90 12 -4 0 297.97 12.90 12 -4 0 280.47 12.40 -12 -4 0 284.07 17.00 -12 4 0 263.17 15.90 -12 4 0 261.57 12.90 -12 4 0 273.67 13.20 -12 4 0 262.57 11.80 -12 4 0 294.87 13.90 13 -4 0 286.17 13.20 13 -4 0 286.57 12.60 13 -4 0 282.77 12.20 -13 -4 0 275.07 17.40 13 -4 0 308.17 13.80 13 -4 0 291.97 11.20 -13 4 0 266.37 16.50 -13 4 0 263.97 11.60 -13 4 0 291.97 13.00 -13 4 0 279.97 11.90 -13 4 0 285.07 11.90 -13 4 0 282.17 13.20 14 -4 0 246.28 10.70 -14 -4 0 266.67 17.90 14 -4 0 274.97 13.40 14 -4 0 270.27 11.90 14 -4 0 271.47 12.90 14 -4 0 262.37 11.70 -14 4 0 247.08 10.90 -14 4 0 254.77 16.40 -14 4 0 268.67 11.10 -14 4 0 270.67 12.40 -14 4 0 263.67 12.50 -14 4 0 249.18 11.10 15 -4 0 117.69 8.10 15 -4 0 123.89 8.60 15 -4 0 111.19 6.90 15 -4 0 116.89 6.90 -15 4 0 122.39 6.30 -15 4 0 113.99 7.20 -15 4 0 112.09 7.30 -15 4 0 104.79 6.20 16 -4 0 86.89 7.30 16 -4 0 88.09 6.10 16 -4 0 90.29 7.70 -16 -4 0 81.59 4.50 16 -4 0 83.89 5.70 -16 4 0 89.49 6.30 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14.40 -2 5 0 336.47 15.60 2 5 0 357.46 13.80 3 -5 0 3038.90 97.39 -3 -5 0 2796.12 94.89 3 -5 0 2828.62 96.39 3 -5 0 2816.02 94.69 -3 -5 0 2777.72 94.39 3 5 0 2889.61 95.19 3 5 0 2907.71 98.79 -3 5 0 2879.51 97.09 -3 5 0 3035.20 97.79 -3 5 0 2851.81 96.29 4 -5 0 1843.62 62.29 -4 -5 0 1680.93 58.19 4 -5 0 1771.32 60.99 -4 -5 0 1758.22 60.19 -4 5 0 1777.92 61.09 4 5 0 1774.02 63.39 -4 5 0 1758.02 61.59 4 5 0 1838.02 59.89 -4 5 0 1801.62 62.09 5 -5 0 597.04 22.80 5 -5 0 585.14 24.10 -5 -5 0 571.24 22.60 -5 5 0 630.14 25.80 -5 5 0 587.24 22.90 -5 5 0 589.74 23.10 5 5 0 568.84 21.50 -6 -5 0 331.77 12.50 -6 -5 0 319.47 14.50 6 -5 0 310.77 11.40 6 -5 0 309.27 15.30 6 -5 0 318.97 13.80 -6 5 0 323.67 15.40 6 5 0 306.47 12.90 -6 5 0 314.47 13.40 6 5 0 315.37 15.80 -6 5 0 309.17 13.30 7 -5 0 358.46 12.90 -7 -5 0 362.66 16.70 7 -5 0 354.36 14.20 7 -5 0 365.36 15.40 7 -5 0 389.46 17.70 -7 -5 0 363.16 14.10 -7 5 0 368.86 15.80 7 5 0 355.96 17.50 -7 5 0 368.06 17.60 8 -5 0 21.70 4.30 8 -5 0 25.80 1.90 8 -5 0 27.60 2.80 8 -5 0 28.90 3.50 8 5 0 30.80 3.40 8 5 0 26.90 4.70 -8 5 0 25.10 3.40 -8 5 0 30.60 5.10 9 -5 0 242.48 11.00 -9 -5 0 224.68 13.40 9 -5 0 232.28 10.20 9 -5 0 216.28 13.00 9 -5 0 220.78 8.40 -9 5 0 212.48 9.20 9 5 0 216.88 10.90 -9 5 0 233.18 13.60 -9 5 0 231.28 10.90 9 5 0 222.18 12.50 10 -5 0 30.70 4.00 10 -5 0 32.20 3.90 10 -5 0 34.30 3.60 10 -5 0 32.10 2.50 10 -5 0 32.00 2.20 -10 -5 0 45.10 5.40 -10 5 0 32.00 3.70 -10 5 0 26.70 5.00 -10 5 0 25.90 3.00 -10 5 0 31.70 2.50 10 5 0 27.20 4.70 -10 5 0 34.00 3.20 10 5 0 28.40 3.90 -10 5 0 37.70 4.10 11 -5 0 728.13 30.80 -11 -5 0 695.33 31.30 11 -5 0 733.33 26.70 11 -5 0 702.63 26.30 11 -5 0 738.73 27.10 -11 5 0 695.83 25.10 -11 5 0 699.53 26.60 -11 5 0 684.13 25.10 -11 5 0 708.03 27.10 -11 5 0 678.43 31.10 11 5 0 689.03 29.50 12 -5 0 28.70 2.60 12 -5 0 31.90 3.90 12 -5 0 25.60 3.20 12 -5 0 24.10 5.80 12 -5 0 32.00 4.00 12 -5 0 33.20 4.20 -12 -5 0 29.90 5.90 -12 5 0 31.80 3.40 -12 5 0 25.10 3.80 -12 5 0 24.60 3.60 -12 5 0 22.80 5.20 -12 5 0 27.60 3.10 -12 5 0 27.50 3.20 13 -5 0 447.96 23.80 13 -5 0 426.16 16.20 13 -5 0 444.46 17.30 13 -5 0 450.75 18.60 13 -5 0 466.85 18.20 13 -5 0 475.05 19.10 -13 -5 0 425.46 23.80 -13 5 0 433.86 17.00 -13 5 0 449.46 16.90 -13 5 0 426.16 16.70 -13 5 0 434.96 18.20 -13 5 0 456.75 18.90 -13 5 0 398.66 22.50 14 -5 0 27.00 3.00 14 -5 0 24.20 3.90 14 -5 0 22.90 3.50 14 -5 0 19.60 3.10 14 -5 0 27.00 4.70 -14 5 0 26.10 3.10 -14 5 0 25.10 3.90 -14 5 0 19.80 2.60 -14 5 0 28.20 3.00 -14 5 0 25.00 3.70 15 -5 0 114.49 6.80 15 -5 0 107.69 7.70 15 -5 0 107.69 6.60 15 -5 0 125.19 8.40 15 -5 0 106.29 5.80 -15 5 0 112.69 7.20 -15 5 0 103.69 5.70 -15 5 0 113.79 6.00 -15 5 0 112.19 7.10 -15 5 0 111.49 5.90 16 -5 0 3.10 2.80 16 -5 0 7.50 2.90 -16 5 0 4.70 2.10 -16 5 0 1.60 1.20 -16 5 0 2.10 1.60 17 -5 0 121.39 8.40 17 -5 0 125.69 8.70 17 -5 0 129.19 7.20 -17 5 0 130.79 7.20 -17 5 0 121.29 7.10 -17 5 0 131.29 6.10 -17 5 0 127.69 6.10 18 -5 0 41.00 4.10 18 -5 0 31.70 5.40 18 -5 0 44.30 5.40 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318.37 15.70 -5 6 0 318.27 13.60 -5 6 0 314.47 15.40 -5 6 0 319.17 14.90 5 6 0 300.37 13.50 5 6 0 313.27 16.60 6 -6 0 397.26 18.80 6 -6 0 375.96 13.90 6 -6 0 394.56 15.30 6 -6 0 399.26 17.00 6 6 0 399.06 15.90 6 6 0 377.86 14.40 6 6 0 394.76 19.60 -6 6 0 388.16 17.80 -6 6 0 399.46 19.00 -6 6 0 393.76 16.30 7 -6 0 58.09 3.20 7 -6 0 57.29 5.10 7 -6 0 60.39 4.20 7 -6 0 61.89 6.30 7 6 0 54.69 6.40 -7 6 0 57.09 5.90 -7 6 0 62.89 4.90 -7 6 0 60.29 6.50 7 6 0 59.29 4.70 8 -6 0 12.90 2.90 8 -6 0 12.70 1.80 8 -6 0 13.50 3.00 8 -6 0 14.70 1.80 8 -6 0 12.30 4.00 -8 6 0 18.30 3.70 -8 6 0 15.80 2.40 8 6 0 16.20 2.90 -8 6 0 12.70 3.90 8 6 0 16.70 3.70 -8 6 0 12.30 2.90 -8 6 0 14.90 2.00 9 -6 0 3.70 3.50 9 -6 0 6.80 1.80 9 -6 0 5.30 1.20 9 -6 0 4.50 2.50 -9 6 0 5.80 1.60 -9 6 0 6.30 2.50 9 6 0 10.80 4.70 -9 6 0 10.60 3.40 -9 6 0 16.00 4.30 9 6 0 6.40 2.90 -9 6 0 8.80 2.00 10 -6 0 906.21 37.50 10 -6 0 913.91 31.40 10 -6 0 891.31 29.90 10 -6 0 903.01 33.00 10 -6 0 921.11 32.50 10 -6 0 919.31 33.30 -10 6 0 882.91 31.50 -10 6 0 831.72 31.20 -10 6 0 879.41 31.10 -10 6 0 874.41 37.60 10 6 0 866.51 36.00 -10 6 0 915.11 30.60 -10 6 0 896.91 36.70 -10 6 0 904.61 32.90 -10 6 0 911.31 33.50 11 -6 0 8.30 2.00 11 -6 0 9.60 1.70 11 -6 0 9.80 2.70 11 -6 0 9.50 2.80 11 -6 0 8.30 2.70 -11 6 0 9.30 1.70 -11 6 0 13.10 6.50 -11 6 0 10.20 3.00 -11 6 0 11.70 2.20 -11 6 0 13.00 2.30 -11 6 0 7.10 2.70 -11 6 0 12.40 1.80 11 6 0 6.10 7.30 12 -6 0 231.78 11.30 12 -6 0 226.18 11.30 -12 6 0 227.48 11.70 13 -6 0 83.09 4.70 13 -6 0 86.39 7.80 13 -6 0 86.69 5.60 13 -6 0 90.19 6.70 13 -6 0 83.59 6.70 -13 6 0 83.09 6.50 -13 6 0 81.39 5.20 -13 6 0 88.39 6.40 -13 6 0 81.79 5.10 14 -6 0 136.49 8.40 14 -6 0 132.39 6.40 14 -6 0 120.29 7.00 14 -6 0 141.29 7.80 14 -6 0 137.29 8.70 -14 6 0 131.09 6.60 -14 6 0 133.09 8.20 -14 6 0 130.79 7.80 -14 6 0 137.29 6.80 15 -6 0 37.00 3.40 15 -6 0 47.90 5.10 15 -6 0 42.90 4.30 -15 6 0 43.00 3.40 -15 6 0 44.60 4.60 -15 6 0 42.00 3.60 16 -6 0 84.19 5.50 16 -6 0 68.89 6.00 16 -6 0 87.29 6.80 16 -6 0 74.49 6.80 -16 6 0 80.89 4.40 -16 6 0 83.79 5.60 -16 6 0 78.19 4.50 -16 6 0 84.49 5.80 17 -6 0 4.60 2.50 17 -6 0 2.60 2.50 17 -6 0 2.90 2.50 -17 6 0 2.20 1.20 -17 6 0 3.60 2.20 -17 6 0 2.00 1.80 -17 6 0 2.40 1.10 18 -6 0 113.49 7.40 18 -6 0 107.59 7.40 18 -6 0 117.79 5.80 -18 6 0 123.29 6.10 -18 6 0 104.19 6.80 -18 6 0 113.79 4.90 -18 6 0 119.89 4.90 0 -7 0 1.20 1.80 0 -7 0 -1.80 1.30 0 7 0 -0.40 1.50 0 7 0 -0.50 1.20 0 7 0 1.40 1.70 -1 -7 0 279.07 10.40 -1 -7 0 268.37 13.70 1 -7 0 279.17 13.90 -1 -7 0 274.97 12.80 1 -7 0 289.37 13.80 1 -7 0 277.07 10.50 -1 7 0 273.67 12.20 -1 7 0 296.07 13.30 -1 7 0 295.17 15.70 1 7 0 286.57 12.10 1 7 0 281.97 15.80 1 7 0 299.07 13.40 2 -7 0 78.79 6.10 -2 -7 0 60.29 5.70 -2 -7 0 72.79 5.00 2 -7 0 66.39 6.10 2 -7 0 69.49 3.60 2 7 0 71.29 4.70 2 7 0 69.89 5.10 -2 7 0 72.59 5.30 -2 7 0 65.79 5.60 2 7 0 68.09 7.20 -2 7 0 60.19 6.80 3 -7 0 146.19 7.20 3 -7 0 135.49 6.10 -3 -7 0 144.29 9.00 3 -7 0 142.99 9.00 -3 -7 0 141.99 7.00 3 -7 0 160.98 9.80 -3 7 0 143.09 9.50 -3 7 0 141.09 8.90 -3 7 0 150.18 10.00 3 7 0 142.09 7.10 3 7 0 151.68 11.00 3 7 0 145.29 7.80 -3 7 0 147.29 8.00 4 -7 0 662.23 25.80 4 -7 0 642.74 23.10 4 -7 0 586.84 28.00 -4 -7 0 587.14 25.40 4 -7 0 655.23 22.00 -4 7 0 672.43 27.30 -4 7 0 630.64 25.80 -4 7 0 636.14 24.30 4 7 0 655.13 24.00 4 7 0 620.64 23.00 -4 7 0 629.24 26.60 5 -7 0 1561.44 51.49 5 -7 0 1546.95 52.79 -5 -7 0 1440.06 55.19 5 -7 0 1559.24 57.39 5 -7 0 1563.24 55.39 5 7 0 1565.14 59.09 -5 7 0 1468.75 52.19 -5 7 0 1531.85 52.89 -5 7 0 1615.84 54.29 -5 7 0 1592.64 56.09 -5 7 0 1558.44 52.19 -5 7 0 1615.44 57.69 -5 7 0 1554.54 56.09 5 7 0 1576.94 53.59 5 7 0 1553.34 52.29 6 -7 0 503.85 20.80 6 -7 0 497.25 18.70 6 -7 0 498.75 17.40 6 -7 0 472.95 22.60 6 -7 0 497.65 19.60 -6 7 0 490.05 19.30 -6 7 0 486.95 21.80 -6 7 0 481.05 18.10 -6 7 0 480.95 20.50 6 7 0 476.75 19.40 6 7 0 481.35 23.60 -6 7 0 499.45 23.00 -6 7 0 509.75 18.40 -6 7 0 443.36 18.30 6 7 0 485.05 17.70 7 -7 0 401.36 18.70 7 -7 0 347.87 13.00 7 -7 0 348.67 17.40 7 -7 0 372.26 13.20 7 -7 0 372.86 18.90 7 -7 0 360.06 15.30 7 7 0 324.87 14.50 -7 7 0 373.56 15.90 -7 7 0 368.56 14.10 -7 7 0 313.17 14.10 -7 7 0 324.87 18.70 7 7 0 363.96 19.30 -7 7 0 349.47 18.80 7 7 0 357.46 12.80 -7 7 0 362.66 18.00 -7 7 0 367.56 13.70 8 -7 0 73.69 6.20 8 -7 0 74.99 3.80 8 -7 0 63.99 7.70 8 -7 0 73.29 5.80 8 -7 0 69.29 5.00 8 -7 0 75.59 4.00 8 7 0 63.99 7.50 -8 7 0 68.79 7.40 8 7 0 58.89 5.60 -8 7 0 74.79 8.10 -8 7 0 67.29 4.20 -8 7 0 66.29 5.30 -8 7 0 69.99 4.50 -8 7 0 69.59 4.80 -8 7 0 71.69 4.20 -8 7 0 70.29 5.80 9 -7 0 699.03 25.70 9 -7 0 644.74 23.70 9 -7 0 635.44 22.60 9 -7 0 701.03 26.30 9 -7 0 684.63 24.90 -9 7 0 620.04 23.50 -9 7 0 693.53 23.30 9 7 0 656.23 25.40 -9 7 0 644.94 29.20 -9 7 0 622.74 23.20 -9 7 0 677.13 26.20 -9 7 0 638.44 25.30 -9 7 0 678.63 24.10 10 -7 0 77.89 5.00 10 -7 0 72.99 8.60 10 -7 0 85.09 5.90 10 -7 0 80.69 3.90 10 -7 0 76.49 6.30 -10 7 0 101.39 7.90 -10 7 0 80.29 6.60 -10 7 0 104.69 10.10 -10 7 0 76.99 11.30 -10 7 0 77.99 5.40 -10 7 0 80.39 5.50 10 7 0 65.79 11.20 11 -7 0 98.69 6.70 11 -7 0 104.89 5.20 11 -7 0 107.49 7.20 11 -7 0 100.99 5.80 11 -7 0 93.79 4.40 11 -7 0 109.29 7.10 -11 7 0 89.09 4.90 -11 7 0 99.19 5.70 -11 7 0 92.49 6.60 -11 7 0 94.59 5.20 -11 7 0 107.89 7.90 12 -7 0 202.48 9.40 12 -7 0 215.98 10.70 12 -7 0 203.28 10.40 12 -7 0 207.08 8.70 12 -7 0 216.18 10.90 -12 7 0 199.08 8.40 -12 7 0 217.18 11.20 -12 7 0 204.78 8.80 -12 7 0 220.08 10.80 -12 7 0 219.28 9.40 13 -7 0 22.10 3.50 13 -7 0 31.30 4.60 13 -7 0 25.50 3.70 13 -7 0 23.10 2.80 -13 7 0 27.80 3.40 -13 7 0 19.90 3.50 -13 7 0 18.30 3.20 -13 7 0 24.40 3.00 14 -7 0 12.20 2.30 14 -7 0 9.60 3.70 14 -7 0 13.60 2.10 14 -7 0 12.90 3.30 14 -7 0 14.60 3.40 -14 7 0 11.40 1.80 -14 7 0 11.00 1.90 -14 7 0 13.90 2.70 15 -7 0 28.50 3.50 15 -7 0 28.50 4.70 15 -7 0 27.00 3.70 15 -7 0 24.60 3.70 -15 7 0 27.50 3.80 -15 7 0 28.60 2.50 -15 7 0 28.60 3.50 -15 7 0 27.10 2.80 16 -7 0 18.40 3.40 16 -7 0 18.80 2.40 16 -7 0 17.00 3.10 16 -7 0 17.50 3.10 -16 7 0 17.80 2.20 -16 7 0 26.80 3.50 -16 7 0 19.20 1.90 -16 7 0 20.40 2.80 17 -7 0 37.70 4.10 17 -7 0 30.60 4.30 17 -7 0 33.00 3.90 -17 7 0 37.20 3.20 -17 7 0 37.50 3.20 -17 7 0 34.40 3.00 -17 7 0 36.90 2.10 0 -8 0 112.89 8.20 0 -8 0 121.49 7.60 0 8 0 102.79 9.50 0 8 0 115.19 6.80 0 8 0 114.79 5.80 0 8 0 111.29 4.90 1 -8 0 119.89 8.50 -1 -8 0 119.39 8.50 1 -8 0 116.49 8.20 1 -8 0 131.29 5.80 -1 -8 0 114.99 7.40 -1 -8 0 119.99 5.30 1 -8 0 126.09 5.70 -1 8 0 120.49 7.10 -1 8 0 121.49 5.60 -1 8 0 124.69 6.20 1 8 0 127.09 6.40 -1 8 0 113.09 7.00 -1 8 0 123.89 9.60 1 8 0 119.89 7.40 1 8 0 121.99 10.30 -2 -8 0 47.80 2.70 2 -8 0 46.10 3.00 2 -8 0 52.39 3.10 2 -8 0 49.30 5.30 -2 -8 0 43.60 5.40 2 -8 0 41.70 4.20 -2 -8 0 41.90 4.00 2 -8 0 44.50 5.30 -2 8 0 39.70 5.60 2 8 0 38.20 4.20 -2 8 0 43.10 3.90 -2 8 0 42.20 3.40 -2 8 0 48.40 3.50 -2 8 0 46.90 4.50 2 8 0 45.90 3.40 -2 8 0 46.60 4.30 2 8 0 48.60 6.40 -3 -8 0 53.79 2.90 3 -8 0 55.99 3.30 3 -8 0 54.39 4.70 -3 -8 0 48.10 5.60 3 -8 0 49.40 6.20 3 8 0 53.19 7.00 -3 8 0 61.89 3.70 3 8 0 53.29 3.50 3 8 0 50.09 4.20 -3 8 0 55.69 4.20 -3 8 0 57.89 5.00 -3 8 0 58.49 6.50 -3 8 0 61.09 4.10 3 8 0 54.49 4.90 4 -8 0 226.48 9.00 4 -8 0 238.98 13.80 4 -8 0 236.38 11.00 4 -8 0 238.98 12.70 4 -8 0 237.48 9.10 -4 -8 0 202.08 12.70 -4 8 0 218.18 10.70 -4 8 0 231.88 10.10 -4 8 0 230.98 9.50 4 8 0 218.78 9.10 4 8 0 220.48 10.40 -4 8 0 238.38 11.50 -4 8 0 231.18 9.90 4 8 0 224.18 14.80 4 8 0 245.98 10.20 -4 8 0 238.78 13.60 5 -8 0 101.69 7.50 5 -8 0 93.39 5.60 5 -8 0 100.29 8.70 5 -8 0 98.49 4.80 5 -8 0 98.09 4.80 5 -8 0 102.79 6.60 -5 8 0 97.69 5.50 -5 8 0 89.59 7.80 -5 8 0 95.19 6.40 5 8 0 99.99 4.80 5 8 0 97.49 5.40 5 8 0 89.99 9.00 -5 8 0 98.09 6.80 -5 8 0 100.39 5.30 -5 8 0 97.49 5.60 5 8 0 102.99 6.20 -6 -8 0 36.40 5.10 6 -8 0 48.80 7.50 6 -8 0 45.90 5.10 6 -8 0 42.40 3.90 6 -8 0 49.50 3.20 6 -8 0 46.60 3.20 6 -8 0 51.09 4.60 -6 8 0 46.20 3.80 -6 8 0 44.30 3.80 6 8 0 55.79 9.80 -6 8 0 52.29 5.20 -6 8 0 49.30 10.60 6 8 0 47.60 3.10 6 8 0 42.50 4.30 -6 8 0 51.39 3.70 -6 8 0 42.90 4.60 7 -8 0 38.30 4.30 7 -8 0 38.90 3.90 7 -8 0 35.90 4.90 -7 -8 0 36.00 4.80 7 -8 0 31.60 5.20 7 -8 0 39.10 2.80 -7 8 0 40.00 3.40 7 8 0 41.40 6.30 -7 8 0 30.00 6.10 -7 8 0 35.90 3.30 -7 8 0 35.70 4.50 -7 8 0 36.70 4.20 7 8 0 35.10 4.10 -7 8 0 34.40 3.30 8 -8 0 835.02 29.60 8 -8 0 859.61 31.30 8 -8 0 799.32 27.30 8 -8 0 810.62 30.10 -8 8 0 783.52 28.20 -8 8 0 784.52 29.90 8 8 0 680.53 30.70 -8 8 0 861.71 31.70 -8 8 0 820.52 27.90 -8 8 0 799.22 28.40 9 -8 0 182.18 9.50 9 -8 0 164.78 6.90 9 -8 0 173.08 9.90 9 -8 0 172.08 8.80 -9 8 0 158.98 7.60 -9 8 0 168.88 9.70 -9 8 0 170.48 9.30 -9 8 0 174.88 8.10 -9 8 0 182.68 7.60 10 -8 0 72.49 5.50 10 -8 0 71.29 5.90 10 -8 0 70.19 3.60 10 -8 0 81.69 6.20 10 -8 0 81.09 4.50 -10 8 0 81.19 4.30 -10 8 0 73.19 4.30 -10 8 0 72.79 4.80 -10 8 0 74.89 5.80 -10 8 0 73.19 6.10 11 -8 0 68.29 5.70 11 -8 0 69.19 4.10 11 -8 0 68.19 5.50 11 -8 0 71.39 5.40 -11 8 0 63.89 5.40 -11 8 0 56.79 3.50 -11 8 0 67.79 4.50 -11 8 0 71.29 6.00 12 -8 0 48.40 5.40 12 -8 0 43.90 4.30 12 -8 0 49.90 5.10 12 -8 0 51.09 3.50 12 -8 0 49.10 5.80 -12 8 0 52.49 3.20 -12 8 0 45.50 3.00 -12 8 0 54.59 4.80 -12 8 0 59.99 5.20 -12 8 0 46.00 3.70 13 -8 0 11.80 1.90 13 -8 0 9.50 2.70 13 -8 0 10.50 2.60 13 -8 0 7.50 2.80 -13 8 0 6.60 2.10 -13 8 0 10.20 2.50 -13 8 0 8.70 1.90 -13 8 0 9.50 1.90 14 -8 0 91.39 6.20 14 -8 0 101.89 6.90 14 -8 0 92.89 4.80 14 -8 0 99.39 6.30 -14 8 0 94.49 5.90 -14 8 0 86.39 3.90 -14 8 0 92.49 5.90 -14 8 0 95.19 4.80 15 -8 0 4.50 2.00 15 -8 0 2.80 2.30 15 -8 0 0.70 1.20 -15 8 0 2.40 1.50 -15 8 0 2.40 1.90 -15 8 0 1.30 1.10 16 -8 0 -0.50 1.80 16 -8 0 2.70 2.40 -16 8 0 1.10 1.10 -16 8 0 3.60 1.60 -16 8 0 1.50 1.10 0 -9 0 -4.10 1.90 0 -9 0 0.50 0.80 0 9 0 0.70 1.40 0 9 0 2.30 1.80 0 9 0 -0.20 1.20 0 9 0 -2.10 1.60 0 9 0 -4.70 2.90 -1 -9 0 385.86 18.00 1 -9 0 377.56 18.70 -1 -9 0 426.16 14.10 1 -9 0 398.36 18.20 1 -9 0 412.76 14.20 -1 9 0 391.46 13.60 -1 9 0 339.47 21.30 -1 9 0 412.76 16.30 1 9 0 324.87 15.50 -1 9 0 335.67 15.40 1 9 0 408.76 15.90 -1 9 0 384.56 15.30 -2 -9 0 90.39 7.50 2 -9 0 93.69 7.50 -2 -9 0 93.89 4.50 2 -9 0 95.59 4.70 2 -9 0 100.49 6.40 -2 9 0 87.09 5.80 -2 9 0 94.39 7.40 2 9 0 104.99 6.10 -2 9 0 94.19 6.50 3 -9 0 23.30 2.30 -3 -9 0 25.10 2.00 3 -9 0 23.90 4.20 -3 -9 0 21.30 3.70 -3 9 0 22.90 3.00 -3 9 0 27.00 3.40 -3 9 0 19.70 3.40 -3 9 0 23.80 3.10 3 9 0 27.50 3.10 3 9 0 25.50 3.50 3 9 0 24.00 4.80 4 -9 0 171.98 8.80 -4 -9 0 156.38 10.00 4 -9 0 173.28 10.50 4 9 0 177.48 7.30 4 9 0 166.08 8.30 -4 9 0 174.78 7.40 -4 9 0 177.68 8.00 -4 9 0 161.68 8.80 -4 9 0 175.28 7.90 5 -9 0 348.37 12.90 5 -9 0 346.97 14.80 5 -9 0 354.66 16.60 -5 -9 0 311.07 16.40 5 9 0 337.57 14.00 -5 9 0 352.06 13.70 5 9 0 355.16 12.80 -5 9 0 368.06 13.70 -5 9 0 365.96 13.30 -5 9 0 346.47 14.70 -5 9 0 342.77 15.40 6 -9 0 202.78 9.90 6 -9 0 179.08 8.90 6 -9 0 194.78 7.90 6 9 0 187.28 8.90 -6 9 0 197.58 8.60 -6 9 0 186.48 9.60 -6 9 0 188.98 8.30 6 9 0 204.28 7.70 -6 9 0 204.08 8.50 -6 9 0 198.18 10.40 7 -9 0 114.59 8.00 7 -9 0 123.49 5.40 7 -9 0 123.29 7.30 7 -9 0 123.19 6.90 -7 9 0 117.79 6.10 7 9 0 120.29 6.40 -7 9 0 123.49 5.90 -7 9 0 116.79 7.50 -7 9 0 126.09 6.10 -7 9 0 117.79 7.30 8 -9 0 30.90 3.70 8 -9 0 30.70 2.40 8 -9 0 30.30 4.30 8 -9 0 31.10 4.00 -8 9 0 33.80 3.20 -8 9 0 33.20 2.90 -8 9 0 31.40 2.90 -8 9 0 30.30 4.00 -8 9 0 34.20 4.40 9 -9 0 39.90 3.70 9 -9 0 31.70 4.20 9 -9 0 33.90 2.40 -9 9 0 33.90 3.30 -9 9 0 36.30 4.50 -9 9 0 45.50 4.60 -9 9 0 32.50 3.10 -9 9 0 36.70 4.30 10 -9 0 6.70 2.00 10 -9 0 6.50 2.40 10 -9 0 6.80 1.60 10 -9 0 5.40 2.60 -10 9 0 6.30 1.40 -10 9 0 7.00 2.00 -10 9 0 4.40 2.20 -10 9 0 5.40 1.50 11 -9 0 36.80 3.80 11 -9 0 37.30 4.40 11 -9 0 36.10 2.90 -11 9 0 36.30 3.10 -11 9 0 38.30 4.00 -11 9 0 36.00 4.20 -11 9 0 35.30 2.40 12 -9 0 38.60 4.30 12 -9 0 28.00 4.20 12 -9 0 34.60 3.00 -12 9 0 35.90 2.10 -12 9 0 32.60 3.60 -12 9 0 34.00 2.90 -12 9 0 40.40 4.10 13 -9 0 20.70 3.60 13 -9 0 23.30 2.50 13 -9 0 17.60 2.70 -13 9 0 21.10 2.60 -13 9 0 24.10 3.30 -13 9 0 26.50 3.10 14 -9 0 4.50 2.00 14 -9 0 2.90 2.00 14 -9 0 4.70 1.70 -14 9 0 4.00 1.10 -14 9 0 3.60 1.40 -14 9 0 3.20 1.40 0 -10 0 44.80 5.00 0 -10 0 53.39 3.10 0 10 0 52.19 3.60 0 10 0 53.59 4.40 0 10 0 49.30 3.90 1 -10 0 31.80 2.40 -1 -10 0 33.20 2.30 1 -10 0 21.50 3.70 -1 -10 0 24.60 3.90 1 10 0 25.80 3.30 1 10 0 31.70 2.80 -1 10 0 29.00 3.10 -1 10 0 33.10 3.70 1 10 0 29.10 3.20 -1 10 0 35.00 3.00 2 -10 0 47.00 3.00 -2 -10 0 46.70 2.70 -2 -10 0 44.30 5.10 2 -10 0 39.60 5.00 2 10 0 46.50 3.80 -2 10 0 48.20 3.50 2 10 0 46.50 3.20 2 10 0 43.10 3.70 -2 10 0 40.00 4.20 -2 10 0 51.59 3.80 3 -10 0 70.79 3.70 -3 -10 0 69.89 3.50 3 -10 0 63.29 4.90 3 -10 0 76.79 6.20 -3 -10 0 63.29 5.90 -3 10 0 63.19 5.20 3 10 0 71.79 3.80 -3 10 0 71.99 5.70 -3 10 0 72.29 4.30 -3 10 0 73.19 4.50 3 10 0 67.79 4.40 4 -10 0 126.99 8.30 4 -10 0 132.99 5.90 4 -10 0 141.59 7.20 -4 -10 0 138.29 5.60 4 10 0 145.39 7.30 -4 10 0 132.59 7.80 -4 10 0 130.99 6.50 -4 10 0 139.19 6.50 -4 10 0 133.19 6.90 5 -10 0 28.20 3.30 -5 -10 0 26.90 1.90 5 -10 0 28.10 4.10 5 -10 0 27.80 2.30 5 10 0 27.30 2.90 -5 10 0 26.90 3.20 -5 10 0 25.10 3.20 -5 10 0 20.10 3.30 6 -10 0 32.70 2.50 6 -10 0 40.10 3.90 6 10 0 32.60 3.00 -6 10 0 26.50 3.50 -6 10 0 33.40 2.90 -6 10 0 33.10 4.10 -6 10 0 34.90 2.90 -6 10 0 35.80 2.60 7 -10 0 7.00 1.40 7 -10 0 6.20 1.60 7 -10 0 6.20 2.00 7 -10 0 8.50 2.40 -7 10 0 5.30 1.40 -7 10 0 3.50 1.30 -7 10 0 7.30 1.40 -7 10 0 8.20 3.50 -7 10 0 6.90 2.00 8 -10 0 90.69 5.60 8 -10 0 87.69 4.50 8 -10 0 78.49 3.80 -8 10 0 75.99 5.10 -8 10 0 87.69 4.40 -8 10 0 80.09 5.80 -8 10 0 85.09 4.30 -8 10 0 89.59 4.30 9 -10 0 64.89 5.30 9 -10 0 66.99 3.80 9 -10 0 59.59 2.90 -9 10 0 60.39 4.90 -9 10 0 61.39 3.40 -9 10 0 61.19 3.60 10 -10 0 1.30 1.70 10 -10 0 1.10 1.20 -10 10 0 1.00 1.50 -10 10 0 2.30 1.70 -10 10 0 1.40 1.10 -10 10 0 2.00 0.90 11 -10 0 54.89 4.40 11 -10 0 51.59 3.30 -11 10 0 52.09 3.60 -11 10 0 53.59 3.10 12 -10 0 37.00 2.80 12 -10 0 39.70 3.80 -12 10 0 41.30 2.90 -12 10 0 38.50 2.40 -12 10 0 36.20 3.30 0 -11 0 0.30 0.70 0 11 0 1.40 1.30 0 11 0 -1.10 1.10 0 11 0 1.40 1.10 -1 -11 0 47.70 2.60 1 -11 0 45.30 2.70 1 11 0 46.80 3.00 1 11 0 47.70 3.40 -1 11 0 39.20 3.60 -1 11 0 46.80 3.10 1 11 0 47.60 3.20 -1 11 0 48.20 3.20 -2 -11 0 38.40 2.30 2 -11 0 41.40 2.50 -2 11 0 41.30 3.00 -2 11 0 38.40 3.50 -2 11 0 42.50 2.90 2 11 0 40.70 2.60 2 11 0 34.90 3.10 3 -11 0 30.40 2.20 -3 -11 0 32.90 1.90 -3 11 0 33.50 2.60 -3 11 0 27.80 3.30 -3 11 0 27.40 2.50 4 -11 0 10.00 1.60 -4 -11 0 9.50 1.30 4 -11 0 7.20 1.20 4 11 0 8.00 1.40 -4 11 0 7.00 1.40 -4 11 0 7.90 2.00 -4 11 0 9.00 1.50 -5 -11 0 181.68 6.60 5 -11 0 191.08 7.40 5 -11 0 180.68 6.90 5 11 0 176.78 8.40 -5 11 0 169.08 6.30 -5 11 0 176.18 7.20 -5 11 0 190.38 7.20 -5 11 0 180.98 8.40 6 -11 0 105.29 4.50 6 -11 0 112.39 5.10 -6 11 0 101.79 6.00 -6 11 0 103.39 4.20 -6 11 0 128.19 5.90 -6 11 0 105.39 5.00 7 -11 0 68.19 4.80 7 -11 0 57.89 2.90 7 -11 0 63.29 4.60 -7 11 0 55.39 2.70 -7 11 0 58.19 3.10 8 -11 0 122.59 6.00 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6.60 6 6 4 105.99 7.20 6 6 4 115.09 8.20 7 -6 4 285.17 10.80 7 -6 4 287.87 10.10 -7 -6 -4 277.57 13.00 7 -6 4 287.17 12.20 7 -6 4 258.07 16.00 7 -6 4 286.27 12.70 7 -6 4 272.37 13.40 7 6 4 277.07 13.30 -7 6 -4 285.77 10.50 -7 6 -4 245.98 10.50 -7 6 -4 269.67 15.40 -7 6 -4 279.37 11.30 7 6 4 258.07 12.60 7 6 4 256.57 13.90 -7 6 -4 282.17 12.50 8 -6 4 161.78 8.50 8 -6 4 175.98 9.20 8 -6 4 164.48 7.10 8 -6 4 164.38 9.40 8 -6 4 175.08 12.00 8 -6 4 159.38 6.30 8 6 4 152.98 9.40 -8 6 -4 150.08 8.50 -8 6 -4 155.88 11.50 -8 6 -4 155.58 6.90 -8 6 -4 155.88 7.40 -8 6 -4 147.39 8.50 8 6 4 141.39 9.50 8 6 4 134.39 8.60 9 -6 4 149.19 6.80 9 -6 4 153.88 8.50 9 -6 4 141.89 11.40 9 -6 4 153.68 5.90 9 -6 4 159.08 9.00 9 -6 4 151.58 8.90 9 6 4 137.39 8.50 -9 6 -4 144.49 11.30 -9 6 -4 128.29 6.60 -9 6 -4 138.99 8.10 9 6 4 140.59 9.20 -9 6 -4 148.29 8.30 10 -6 4 400.36 15.60 10 -6 4 400.46 16.80 10 -6 4 409.96 17.10 10 -6 4 368.16 20.90 10 -6 4 408.36 14.90 10 -6 4 421.56 17.60 -10 6 -4 384.66 16.50 -10 6 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41.90 4.20 10 -8 4 26.80 5.90 10 -8 4 38.30 3.50 10 -8 4 34.00 3.40 -10 8 -4 37.20 4.10 10 8 4 34.10 4.10 -10 8 -4 34.60 2.50 -10 8 -4 35.60 4.50 -10 8 -4 35.30 4.00 11 -8 4 128.59 5.60 11 -8 4 135.49 8.50 11 -8 4 132.99 6.60 11 -8 4 122.79 7.70 11 -8 4 130.09 7.40 -11 8 -4 132.49 6.20 -11 8 -4 126.59 5.30 11 8 4 119.89 6.80 -11 8 -4 128.89 7.50 12 -8 4 54.79 5.80 12 -8 4 41.30 4.80 12 -8 4 52.19 4.00 -12 8 -4 53.09 4.30 12 8 4 49.99 5.50 -12 8 -4 53.49 4.70 -12 8 -4 52.39 3.50 -12 8 -4 51.09 3.60 13 -8 4 59.39 5.00 13 -8 4 57.99 5.70 13 -8 4 53.09 4.20 -13 8 -4 63.49 4.80 -13 8 -4 78.19 6.20 -13 8 -4 56.69 2.90 14 -8 4 15.00 2.10 14 -8 4 10.70 2.80 14 -8 4 10.50 2.90 -14 8 -4 14.60 2.20 -14 8 -4 16.30 1.90 -14 8 -4 12.50 1.90 14 -9 -4 83.69 5.50 14 -9 -4 88.09 5.00 14 -9 -4 79.79 5.00 -14 9 4 81.19 4.10 -14 9 4 78.39 3.40 -14 9 4 84.09 4.30 -14 9 4 81.09 5.20 13 -9 -4 85.09 5.80 13 -9 -4 83.69 4.00 13 -9 -4 73.09 6.50 -13 9 4 86.69 4.50 -13 9 4 82.99 4.70 -13 9 4 82.89 5.60 -13 9 4 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9.60 3 -9 4 49.90 3.40 3 -9 4 51.39 3.20 -3 -9 -4 50.19 3.00 3 -9 4 46.20 5.70 3 9 4 56.69 3.50 -3 9 -4 54.99 3.50 -3 9 -4 49.60 3.50 -3 9 -4 51.79 3.40 3 9 4 56.39 5.10 -3 9 -4 50.29 4.60 -3 9 -4 52.19 4.90 4 -9 4 73.79 4.40 4 -9 4 72.09 3.90 -4 9 -4 71.09 4.20 -4 9 -4 75.79 4.10 -4 9 -4 78.59 5.90 -4 9 -4 73.59 4.20 4 9 4 78.89 5.90 4 9 4 73.89 3.90 -4 9 -4 78.59 5.90 5 -9 4 55.09 5.80 5 -9 4 53.19 4.70 5 -9 4 52.49 3.70 -5 9 -4 48.70 4.70 -5 9 -4 45.80 3.30 5 9 4 46.50 4.70 -5 9 -4 49.00 3.50 5 9 4 51.69 3.00 -5 9 -4 53.39 3.30 -5 9 -4 49.50 4.90 6 -9 4 29.70 2.90 6 -9 4 21.90 2.20 6 -9 4 23.80 4.30 -6 9 -4 24.40 2.70 -6 9 -4 20.50 3.40 -6 9 -4 19.30 3.30 -6 9 -4 22.50 2.40 6 9 4 27.30 3.70 -6 9 -4 29.90 2.60 7 -9 4 82.39 4.60 7 -9 4 79.19 6.40 7 -9 4 75.99 3.70 7 -9 4 77.39 6.20 -7 9 -4 74.09 5.90 -7 9 -4 74.99 5.70 -7 9 -4 76.29 4.40 8 -9 4 14.80 3.00 8 -9 4 15.80 2.40 8 -9 4 12.20 3.20 8 9 4 14.50 2.70 -8 9 -4 15.00 2.90 -8 9 -4 13.20 3.00 -8 9 -4 16.20 2.40 -8 9 -4 14.10 1.70 9 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79.89 4.10 2 -10 4 85.69 7.40 -2 10 -4 81.69 4.00 -2 10 -4 88.49 4.30 -2 10 -4 71.49 6.40 -2 10 -4 85.89 5.90 -2 10 -4 82.09 5.10 2 10 4 93.79 4.60 3 -10 4 96.99 5.00 3 -10 4 92.29 4.40 -3 -10 -4 98.29 4.50 3 -10 4 92.39 7.20 3 10 4 91.09 4.40 -3 10 -4 96.19 4.50 -3 10 -4 89.69 4.20 -3 10 -4 92.19 5.70 3 10 4 88.19 6.00 -3 10 -4 88.09 6.00 4 -10 4 13.30 4.10 4 -10 4 15.30 1.80 -4 -10 -4 12.50 1.50 4 -10 4 10.30 1.80 -4 10 -4 12.20 1.60 -4 10 -4 12.20 2.40 4 10 4 15.50 1.80 4 10 4 9.20 2.30 -4 10 -4 14.40 1.80 -4 10 -4 12.80 2.80 -4 10 -4 12.90 1.70 5 -10 4 95.49 7.00 5 -10 4 102.79 5.00 5 10 4 92.29 5.70 -5 10 -4 98.39 4.60 -5 10 -4 92.59 4.50 -5 10 -4 98.19 5.90 6 -10 4 24.40 2.80 6 -10 4 23.10 2.00 -6 10 -4 25.10 2.10 6 10 4 31.20 3.40 -6 10 -4 22.60 2.30 -6 10 -4 27.10 3.50 -6 10 -4 27.30 3.50 7 -10 4 30.10 2.00 7 -10 4 30.20 2.80 7 -10 4 28.00 4.60 7 10 4 30.30 3.40 -7 10 -4 29.40 2.50 -7 10 -4 28.70 3.60 -7 10 -4 25.20 3.50 -7 10 -4 27.40 2.10 8 -10 4 119.89 5.50 8 -10 4 109.09 6.40 8 -10 4 108.49 4.40 8 -10 4 111.69 6.70 -8 10 -4 113.49 6.30 -8 10 -4 110.99 4.50 -8 10 -4 114.69 6.30 8 10 4 108.09 5.40 -8 10 -4 109.49 5.00 9 -10 4 1.10 2.40 9 -10 4 0.70 1.80 9 -10 4 0.60 1.00 9 -10 4 1.10 1.80 -9 10 -4 0.50 1.70 -9 10 -4 2.10 1.50 9 10 4 -0.30 1.90 -9 10 -4 0.70 1.50 10 -10 4 38.60 2.60 10 -10 4 38.80 3.10 10 -10 4 31.00 3.40 -10 10 -4 35.90 3.10 -10 10 -4 42.40 2.50 -10 10 -4 41.70 3.30 9 -11 -4 30.20 2.20 -9 11 4 28.90 1.60 -9 11 4 34.10 4.10 -9 11 4 33.70 2.10 8 -11 -4 20.60 2.10 8 -11 -4 23.00 2.70 8 -11 -4 20.00 1.50 -8 11 4 20.80 2.50 -8 11 4 24.90 2.10 -8 11 4 22.60 2.00 7 -11 -4 17.50 2.50 -7 -11 4 13.00 1.30 7 -11 -4 11.90 1.70 -7 11 4 18.40 2.30 -7 11 4 17.90 2.30 -7 11 4 15.20 2.10 6 -11 -4 2.50 0.90 -6 -11 4 4.50 0.70 6 -11 -4 2.80 1.40 -6 -11 4 3.50 1.00 -6 11 4 3.30 1.50 -6 11 4 3.60 1.30 -6 11 4 1.90 1.40 5 -11 -4 98.49 5.30 5 -11 -4 91.09 4.30 -5 11 4 95.19 5.20 -5 11 4 101.09 4.80 -5 11 4 95.19 4.80 -4 -11 4 7.80 1.10 4 -11 -4 7.30 1.70 4 -11 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39.60 3.10 -4 -11 -4 133.19 5.20 4 -11 4 159.88 7.40 4 -11 4 131.39 5.40 -4 11 -4 138.69 6.30 -4 11 -4 138.79 6.90 -4 11 -4 152.78 6.80 4 11 4 134.99 6.30 -4 11 -4 129.69 4.90 5 -11 4 55.09 3.40 5 -11 4 54.09 3.40 -5 11 -4 59.09 3.60 -5 11 -4 52.59 2.40 -5 11 -4 52.69 4.10 5 11 4 54.09 3.40 6 -11 4 31.20 1.90 6 -11 4 31.70 2.50 6 -11 4 33.10 2.70 -6 11 -4 35.10 2.80 -6 11 -4 33.70 1.80 6 11 4 33.60 3.40 -6 11 -4 28.40 3.20 7 -11 4 15.70 2.10 7 -11 4 9.80 1.70 -7 11 -4 16.30 1.30 -7 11 -4 11.00 2.10 -7 11 -4 14.50 2.20 7 11 4 14.80 1.80 -2 -12 4 27.60 1.60 -2 -12 4 26.70 2.90 2 -12 -4 27.30 1.70 -2 12 4 27.60 2.10 -2 12 4 26.80 1.90 1 -12 -4 62.49 2.80 -1 -12 4 61.59 2.80 -1 -12 4 61.69 3.30 -1 12 4 69.59 3.30 -1 12 4 64.19 3.20 0 -12 4 9.80 1.20 0 -12 4 11.00 1.40 0 -12 -4 9.90 1.20 0 12 4 10.00 1.80 0 12 4 10.70 1.30 -21 0 5 2.40 1.10 21 0 -5 1.10 1.60 -21 0 5 2.70 1.00 -20 0 5 4.50 1.60 -20 0 5 1.00 1.10 20 0 -5 2.10 1.90 -20 0 5 0.70 1.20 -19 0 5 54.99 3.60 -19 0 5 48.40 6.00 -19 0 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0.60 1.60 14 -4 -9 93.79 6.50 14 -4 -9 93.99 5.60 14 -4 -9 89.39 6.10 14 -4 -9 86.19 6.30 -14 -4 9 83.09 4.40 14 -4 -9 90.99 4.60 -14 4 9 99.19 5.70 -14 4 9 100.29 5.60 -14 4 9 87.29 5.80 -14 4 9 101.39 7.60 -14 4 9 90.99 5.50 13 -4 -9 72.39 5.70 13 -4 -9 67.79 11.90 13 -4 -9 73.59 5.00 -13 -4 9 79.89 9.40 13 -4 -9 71.79 5.00 13 -4 -9 76.39 5.50 13 -4 -9 77.79 5.80 13 -4 -9 69.79 4.10 -13 -4 9 75.19 3.70 -13 4 9 76.39 8.20 -13 4 9 70.79 5.10 -13 4 9 76.29 4.90 -13 4 9 69.69 6.30 13 4 -9 73.79 3.60 -13 4 9 67.29 4.70 -13 4 9 82.69 5.10 -12 -4 9 41.00 6.90 12 -4 -9 41.70 4.10 12 -4 -9 36.60 6.40 12 -4 -9 49.60 4.10 12 -4 -9 43.90 3.40 12 -4 -9 50.89 4.50 12 -4 -9 52.09 4.10 -12 -4 9 45.20 2.60 12 -4 -9 50.49 4.40 -12 4 9 45.00 4.80 12 4 -9 48.60 3.30 12 4 -9 51.19 7.80 -12 4 9 47.70 4.10 -12 4 9 47.00 4.10 -12 4 9 45.60 4.40 -12 4 9 45.30 7.40 -12 4 9 41.00 4.00 12 4 -9 50.39 3.00 11 -4 -9 79.09 4.30 11 -4 -9 82.59 5.40 -11 -4 9 72.99 4.10 -11 -4 9 91.99 8.70 11 -4 -9 80.69 5.40 11 -4 -9 83.19 7.90 11 -4 -9 75.99 5.00 11 -4 -9 75.09 3.90 -11 4 9 75.69 4.80 11 4 -9 79.59 3.80 -11 4 9 81.89 5.20 11 4 -9 78.09 4.30 11 4 -9 71.49 9.00 -11 4 9 76.59 6.10 -11 4 9 84.99 8.30 -10 -4 9 260.27 9.50 -10 -4 9 279.67 16.10 10 -4 -9 260.07 10.00 10 -4 -9 265.07 11.80 10 -4 -9 265.97 10.50 10 -4 -9 274.87 11.80 10 -4 -9 258.17 10.80 10 -4 -9 272.07 15.20 -10 4 9 254.17 11.50 10 4 -9 289.77 20.90 -10 4 9 263.67 12.30 -10 4 9 281.27 15.30 10 4 -9 261.47 10.40 -10 4 9 273.77 11.00 -10 4 9 261.67 11.30 9 -4 -9 152.68 7.70 -9 -4 9 148.89 10.70 9 -4 -9 164.48 10.90 9 -4 -9 148.99 7.40 -9 -4 9 146.49 5.70 9 -4 -9 147.09 6.30 -9 4 9 146.59 10.40 -9 4 9 139.49 7.60 9 4 -9 145.69 11.60 -9 4 9 140.79 8.00 -8 -4 9 18.00 1.50 -8 -4 9 26.90 2.30 -8 -4 9 28.20 5.00 8 -4 -9 18.80 2.50 8 -4 -9 21.00 2.10 8 -4 -9 21.80 2.90 8 -4 -9 16.50 4.00 -8 4 9 14.90 2.50 -8 4 9 15.30 3.80 -8 4 9 25.00 3.00 8 4 -9 24.10 5.30 7 -4 -9 27.50 2.30 7 -4 -9 26.50 2.90 -7 -4 9 33.30 5.40 7 -4 -9 27.80 2.90 7 -4 -9 29.60 4.70 -7 -4 9 26.70 2.40 -7 -4 9 29.00 2.00 7 4 -9 27.60 5.30 -7 4 9 26.70 4.50 -7 4 9 25.70 3.30 -6 -4 9 390.16 18.40 -6 -4 9 377.06 14.10 6 -4 -9 395.76 14.70 6 -4 -9 375.86 13.90 6 -4 -9 394.76 18.10 -6 -4 9 374.16 13.50 6 4 -9 388.16 20.10 -6 4 9 415.86 18.50 -6 4 9 382.56 15.60 -5 -4 9 261.27 9.50 -5 -4 9 285.87 14.10 5 -4 -9 262.27 13.30 -5 -4 9 255.37 10.20 5 -4 -9 240.68 11.40 5 -4 -9 266.57 10.40 -5 4 9 271.47 13.80 -5 4 9 249.28 11.30 5 4 -9 283.77 10.60 5 4 -9 260.87 15.40 -4 -4 9 27.30 1.90 -4 -4 9 28.70 2.40 -4 -4 9 26.50 4.30 4 -4 -9 25.70 4.00 4 -4 -9 23.60 2.00 4 -4 -9 23.90 2.10 4 4 -9 29.00 2.60 4 4 -9 26.40 5.00 -4 4 9 32.20 3.20 -3 -4 9 51.79 5.30 -3 -4 9 51.69 2.70 3 -4 -9 54.09 5.10 -3 -4 9 56.69 3.20 3 -4 -9 48.90 2.90 3 4 -9 47.30 5.10 3 4 -9 50.79 6.10 3 4 -9 52.29 3.60 -3 4 9 54.19 5.60 -3 4 9 54.19 4.10 2 -4 -9 109.59 7.20 -2 -4 9 122.49 5.40 -2 -4 9 123.99 8.00 -2 -4 9 118.09 4.80 -2 4 9 116.59 8.00 2 4 -9 111.39 7.70 -2 4 9 115.49 6.50 2 4 -9 121.49 9.50 1 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227.88 9.20 4 -4 9 213.08 11.30 4 -4 9 217.38 12.20 4 -4 9 238.88 13.80 -4 4 -9 222.58 12.00 4 4 9 224.18 11.50 -4 4 -9 246.08 13.10 4 4 9 241.48 10.30 -4 4 -9 257.27 13.50 -4 4 -9 220.68 8.60 -4 4 -9 221.08 9.70 5 -4 9 73.89 7.70 5 -4 9 78.39 3.40 5 -4 9 80.19 5.70 5 -4 9 77.69 4.30 5 -4 9 76.59 6.60 -5 -4 -9 65.49 4.70 5 -4 9 74.19 6.50 5 4 9 80.09 5.20 -5 4 -9 77.59 4.80 -5 4 -9 77.99 3.80 -5 4 -9 74.39 7.00 -5 4 -9 64.99 6.50 5 4 9 72.29 6.60 -6 -4 -9 70.19 6.10 6 -4 9 72.09 4.70 -6 -4 -9 53.89 3.40 6 -4 9 67.19 5.20 -6 -4 -9 74.39 4.70 6 -4 9 66.19 6.50 6 -4 9 66.59 5.60 6 -4 9 65.99 4.10 6 -4 9 49.50 5.90 6 -4 9 67.59 8.40 6 4 9 65.89 7.70 -6 4 -9 63.19 3.60 -6 4 -9 60.49 4.40 -6 4 -9 73.69 7.40 -6 4 -9 69.99 3.80 6 4 9 57.09 5.50 6 4 9 64.09 5.00 6 4 9 64.69 5.70 6 4 9 53.99 5.40 -7 -4 -9 29.00 3.10 7 -4 9 22.90 3.30 7 -4 9 25.60 4.60 7 -4 9 23.30 3.40 -7 -4 -9 21.10 4.00 7 -4 9 22.50 3.40 7 -4 9 17.20 4.80 7 -4 9 23.40 2.60 7 4 9 17.50 3.30 7 4 9 22.60 4.50 -7 4 -9 23.90 3.40 -7 4 -9 21.70 4.40 7 4 9 26.40 3.90 -7 4 -9 20.90 2.60 -7 4 -9 24.60 2.30 -7 4 -9 21.50 4.80 8 -4 9 720.63 31.40 8 -4 9 774.12 28.90 8 -4 9 748.03 28.20 8 -4 9 789.22 33.30 8 -4 9 772.82 26.90 8 -4 9 751.82 31.00 -8 -4 -9 782.02 31.10 8 -4 9 780.22 26.90 8 -4 9 802.92 34.60 -8 4 -9 811.12 34.10 8 4 9 770.62 28.50 -8 4 -9 779.42 27.00 8 4 9 775.52 29.60 -8 4 -9 773.22 28.60 -8 4 -9 779.22 27.30 8 4 9 792.82 33.80 -8 4 -9 758.02 26.80 8 4 9 800.42 29.50 8 4 9 769.22 30.70 -8 4 -9 803.62 33.40 -9 -4 -9 121.19 9.40 9 -4 9 93.39 8.40 9 -4 9 90.59 8.90 9 -4 9 107.59 5.20 9 -4 9 93.49 6.80 9 -4 9 97.29 6.70 9 4 9 102.69 7.60 -9 4 -9 105.39 10.00 9 4 9 104.09 7.30 -9 4 -9 100.79 5.20 -9 4 -9 106.69 5.40 9 4 9 104.09 8.10 -9 4 -9 107.09 9.60 -9 4 -9 105.09 6.30 9 4 9 97.69 10.00 9 4 9 112.09 6.60 -9 4 -9 104.99 5.30 10 -4 9 568.54 22.00 10 -4 9 512.85 24.50 10 -4 9 528.85 25.10 10 -4 9 547.65 24.60 10 4 9 576.94 22.80 10 4 9 597.24 23.00 -10 4 -9 558.44 20.00 -10 4 -9 501.75 21.90 -10 4 -9 573.84 20.00 10 4 9 640.74 28.40 10 4 9 509.45 22.70 11 -4 9 1.30 3.20 11 -4 9 -3.60 2.10 11 -4 9 6.90 3.80 11 -4 9 4.70 2.50 -11 4 -9 5.00 1.40 -11 4 -9 5.60 1.30 -11 4 -9 4.50 1.80 11 4 9 2.80 2.40 11 4 9 2.20 2.00 11 4 9 4.60 3.70 -11 4 -9 3.50 1.40 12 -4 9 28.40 5.60 12 -4 9 29.90 3.90 12 -4 9 22.00 3.30 12 -4 9 23.00 5.40 -12 4 -9 29.50 2.50 -12 4 -9 21.40 2.50 12 4 9 22.80 4.00 -12 4 -9 27.00 3.20 12 4 9 18.80 4.70 12 4 9 31.00 4.30 13 -4 9 6.90 3.80 13 -4 9 14.30 3.00 -13 -4 -9 18.70 1.80 13 -4 9 14.00 4.40 13 -4 9 18.40 3.00 -13 4 -9 16.90 2.40 13 4 9 20.60 3.60 -13 4 -9 14.60 2.00 13 4 9 21.70 4.60 -13 4 -9 15.80 2.00 -14 -4 -9 13.90 1.50 14 -4 9 9.80 3.60 14 -4 9 10.20 2.50 14 -4 9 11.90 4.30 14 -4 9 17.10 2.60 14 4 9 9.80 3.30 -14 4 -9 13.10 1.80 14 4 9 12.10 2.70 -14 4 -9 13.60 1.60 -14 4 -9 10.70 1.90 -15 -4 -9 41.60 2.30 15 -4 9 36.10 3.80 15 -4 9 42.60 5.50 15 -4 9 42.90 3.40 15 -4 9 33.80 5.80 -15 4 -9 42.50 2.70 15 4 9 44.40 5.80 -15 4 -9 42.60 2.50 -15 4 -9 40.60 3.00 -16 -4 -9 83.59 3.80 16 -4 9 89.09 5.30 16 -4 9 80.19 7.00 16 -4 9 83.79 5.70 16 -4 9 92.89 4.20 16 -4 9 77.69 6.60 -16 4 -9 88.79 3.80 16 4 9 90.29 4.80 19 -5 -9 6.50 2.00 -19 -5 9 4.30 1.70 19 -5 -9 7.20 1.80 -19 -5 9 8.00 1.20 -19 5 9 9.60 1.70 -19 5 9 6.50 1.40 -19 5 9 7.60 2.10 -18 -5 9 17.90 3.90 18 -5 -9 23.70 3.30 18 -5 -9 24.70 3.40 -18 -5 9 25.10 2.10 18 -5 -9 25.20 3.10 -18 5 9 24.70 2.70 -18 5 9 20.60 3.10 -18 5 9 25.30 2.70 -18 5 9 22.60 2.90 -17 -5 9 26.00 2.20 17 -5 -9 27.40 3.70 17 -5 -9 31.40 3.50 17 -5 -9 30.30 3.60 -17 5 9 29.40 3.00 -17 5 9 22.90 3.60 -17 5 9 30.20 3.90 -17 5 9 31.70 3.30 -17 5 9 29.90 3.10 16 -5 -9 2.20 2.10 16 -5 -9 5.40 2.40 16 -5 -9 4.10 1.90 16 -5 -9 6.30 2.10 -16 5 9 3.20 2.30 -16 5 9 2.20 1.50 -16 5 9 6.50 1.60 -16 5 9 4.20 1.80 -16 5 9 8.50 1.90 -15 -5 9 99.59 4.70 15 -5 -9 106.99 6.90 15 -5 -9 106.19 6.60 15 -5 -9 103.59 6.60 15 -5 -9 99.19 4.80 15 -5 -9 101.39 5.90 -15 5 9 114.79 6.00 -15 5 9 111.49 7.60 -15 5 9 104.69 6.10 -15 5 9 105.39 5.80 -15 5 9 108.29 6.60 14 -5 -9 -0.50 1.40 14 -5 -9 0.60 1.90 14 -5 -9 -1.00 2.20 -14 -5 9 1.40 0.90 14 -5 -9 1.00 1.80 14 -5 -9 -2.00 1.00 -14 5 9 1.60 1.60 -14 5 9 2.90 1.80 -14 5 9 4.10 2.50 -14 5 9 1.40 1.50 -14 5 9 1.20 1.60 13 -5 -9 13.10 1.90 13 -5 -9 12.70 2.80 13 -5 -9 12.60 2.60 13 -5 -9 11.10 2.30 -13 5 9 15.70 2.80 -13 5 9 12.00 2.30 -13 5 9 13.80 2.40 -13 5 9 12.20 2.70 12 -5 -9 17.50 3.00 12 -5 -9 15.80 2.80 12 -5 -9 28.80 5.20 12 -5 -9 18.70 2.90 12 -5 -9 19.30 3.30 12 -5 -9 16.00 2.10 -12 -5 9 6.80 4.30 -12 -5 9 17.20 1.60 12 5 -9 6.60 5.90 -12 5 9 20.70 3.70 -12 5 9 17.90 2.30 -12 5 9 26.60 3.10 -12 5 9 12.70 4.90 -12 5 9 18.40 2.60 12 5 -9 21.50 2.60 -12 5 9 13.30 4.40 -12 5 9 17.50 2.70 11 -5 -9 207.68 9.60 11 -5 -9 216.68 13.90 -11 -5 9 221.18 14.50 11 -5 -9 220.18 10.40 11 -5 -9 211.98 8.50 -11 -5 9 213.58 8.00 11 -5 -9 218.28 10.50 11 -5 -9 215.78 9.00 11 -5 -9 219.98 9.80 -11 5 9 220.58 9.60 -11 5 9 220.18 8.70 -11 5 9 213.38 10.10 -11 5 9 212.38 14.10 -11 5 9 217.48 9.90 11 5 -9 232.28 15.80 11 5 -9 222.58 9.00 -11 5 9 208.78 10.40 -11 5 9 214.48 11.20 10 -5 -9 3.90 1.20 10 -5 -9 3.40 1.60 10 -5 -9 -2.00 2.80 10 -5 -9 3.30 1.30 -10 -5 9 8.60 3.40 10 -5 -9 1.60 1.80 -10 -5 9 1.70 0.80 -10 5 9 5.00 2.20 -10 5 9 4.20 1.80 10 5 -9 2.60 1.30 -10 5 9 -0.10 1.80 10 5 -9 4.00 3.60 -10 5 9 7.30 3.50 -10 5 9 3.00 1.90 9 -5 -9 109.99 7.10 9 -5 -9 126.09 6.80 9 -5 -9 124.19 7.00 -9 -5 9 124.39 5.10 9 -5 -9 114.29 7.70 -9 -5 9 119.79 10.20 9 -5 -9 123.69 10.20 -9 5 9 121.09 6.10 9 5 -9 116.49 5.00 -9 5 9 97.49 8.80 -9 5 9 123.69 6.40 9 5 -9 122.79 11.50 9 5 -9 112.39 7.60 -9 5 9 134.59 10.00 -9 5 9 116.89 6.90 8 -5 -9 484.35 18.20 8 -5 -9 466.85 16.90 8 -5 -9 458.05 17.40 -8 -5 9 475.35 16.20 8 -5 -9 464.35 22.10 8 -5 -9 475.95 18.50 -8 -5 9 471.55 22.60 -8 -5 9 468.85 17.10 8 -5 -9 469.85 17.10 -8 5 9 465.85 18.70 8 5 -9 471.45 17.20 8 5 -9 464.35 24.50 -8 5 9 465.65 18.90 -8 5 9 473.45 18.00 -8 5 9 470.45 22.40 -7 -5 9 45.50 2.50 7 -5 -9 40.50 3.00 7 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5.40 -2 5 9 30.90 3.50 2 5 -9 30.50 3.00 -1 -5 9 100.59 4.40 1 -5 -9 102.19 4.70 -1 -5 9 104.59 7.70 1 -5 -9 91.39 6.50 1 5 -9 98.39 9.50 -1 5 9 91.79 7.50 -1 5 9 107.39 6.40 1 5 -9 102.79 5.80 1 5 -9 96.79 7.80 0 -5 9 124.49 8.40 0 -5 9 124.49 5.10 0 -5 -9 121.59 7.10 0 5 9 132.79 8.70 0 5 -9 123.79 10.10 0 5 -9 106.49 8.30 0 5 9 125.79 7.10 0 5 -9 120.69 6.30 -1 -5 -9 86.19 5.30 1 -5 9 82.99 6.70 1 -5 9 76.69 6.50 1 -5 9 81.29 3.80 -1 5 -9 75.59 7.80 1 5 9 80.39 5.50 -1 5 -9 81.89 7.50 -1 5 -9 81.39 5.00 1 5 9 83.39 6.90 2 -5 9 108.39 4.60 2 -5 9 97.79 7.20 -2 -5 -9 98.69 5.80 2 -5 9 102.49 8.00 2 -5 9 109.39 9.10 2 -5 9 103.29 5.20 -2 -5 -9 92.29 5.70 -2 5 -9 94.59 8.10 -2 5 -9 94.89 7.30 -2 5 -9 105.99 5.80 2 5 9 104.99 7.40 2 5 9 106.29 6.40 -2 5 -9 114.89 9.20 -3 -5 -9 45.60 2.70 -3 -5 -9 41.30 3.40 3 -5 9 40.60 4.90 3 -5 9 44.60 7.20 3 -5 9 44.90 2.60 3 -5 9 43.50 5.20 3 -5 9 45.70 3.20 -3 5 -9 30.30 5.50 -3 5 -9 44.90 5.80 -3 5 -9 44.70 6.30 -3 5 -9 47.80 3.70 3 5 9 43.00 4.30 4 -5 9 0.40 0.80 4 -5 9 3.20 2.90 -4 -5 -9 4.70 1.30 4 -5 9 1.40 1.90 4 -5 9 3.40 1.70 4 -5 9 3.00 2.00 4 -5 9 1.90 1.40 4 5 9 2.30 2.00 -4 5 -9 -2.60 2.70 4 5 9 -1.80 3.10 -4 5 -9 -2.20 2.70 -4 5 -9 2.60 1.20 -4 5 -9 1.90 1.30 -4 5 -9 5.10 2.10 -4 5 -9 -0.50 1.40 -4 5 -9 2.60 2.70 4 5 9 2.60 1.90 4 5 9 -2.60 1.70 4 5 9 2.50 2.00 5 -5 9 805.52 31.50 5 -5 9 824.92 34.90 -5 -5 -9 796.12 28.10 5 -5 9 823.12 33.00 5 -5 9 727.63 30.40 5 -5 9 787.82 30.30 -5 -5 -9 770.82 27.50 5 -5 9 786.32 26.50 5 5 9 857.91 30.20 -5 5 -9 759.92 27.80 -5 5 -9 775.12 28.80 -5 5 -9 795.12 33.80 5 5 9 816.82 31.40 -5 5 -9 796.92 28.60 -5 5 -9 750.72 37.60 -5 5 -9 732.13 32.90 5 5 9 825.42 29.20 5 5 9 813.82 28.40 6 -5 9 640.94 30.20 6 -5 9 633.64 27.00 -6 -5 -9 661.93 27.00 6 -5 9 672.43 28.80 6 -5 9 694.43 24.00 6 -5 9 653.53 25.50 6 -5 9 667.23 23.00 6 -5 9 661.43 23.30 6 -5 9 696.83 22.20 -6 5 -9 637.44 22.80 6 5 9 631.64 24.70 6 5 9 656.03 29.40 -6 5 -9 592.54 24.70 -6 5 -9 640.04 29.40 -6 5 -9 637.84 24.70 -6 5 -9 656.23 23.30 6 5 9 624.74 25.40 6 5 9 687.03 27.10 -6 5 -9 681.73 28.80 7 -5 9 101.79 10.50 7 -5 9 123.09 9.70 7 -5 9 112.09 8.60 -7 -5 -9 100.49 8.10 7 -5 9 100.39 7.90 7 -5 9 103.59 5.60 7 -5 9 114.39 7.60 7 -5 9 107.99 6.30 7 -5 9 106.39 5.50 7 5 9 108.39 6.70 7 5 9 122.39 10.70 -7 5 -9 109.49 5.70 -7 5 -9 112.19 9.60 -7 5 -9 113.39 5.40 7 5 9 109.09 7.70 7 5 9 100.19 6.20 -7 5 -9 101.39 6.50 7 5 9 96.39 7.80 -7 5 -9 121.49 10.40 -7 5 -9 111.99 6.20 8 -5 9 40.90 4.30 8 -5 9 32.50 5.00 8 -5 9 30.20 3.10 8 -5 9 30.60 5.50 8 -5 9 21.30 7.30 -8 -5 -9 26.90 4.80 8 -5 9 35.80 3.40 8 -5 9 35.40 4.10 8 5 9 35.50 4.30 -8 5 -9 40.00 3.60 8 5 9 37.70 4.80 -8 5 -9 38.80 4.00 -8 5 -9 31.40 6.00 -8 5 -9 31.30 2.90 8 5 9 27.30 5.90 -8 5 -9 33.00 2.90 8 5 9 32.20 4.50 9 -5 9 13.00 3.80 9 -5 9 18.20 2.30 9 -5 9 13.20 3.10 9 5 9 14.70 3.70 -9 5 -9 13.80 2.00 9 5 9 13.20 2.70 -9 5 -9 12.20 1.90 -9 5 -9 14.20 2.60 9 5 9 15.20 5.20 10 -5 9 41.60 6.60 10 -5 9 57.39 5.20 10 -5 9 60.29 5.00 -10 -5 -9 51.79 3.10 10 -5 9 70.99 7.00 10 -5 9 49.80 3.50 -10 5 -9 62.69 3.80 -10 5 -9 54.19 5.20 10 5 9 56.79 5.70 -10 5 -9 65.49 4.00 10 5 9 56.49 4.70 10 5 9 65.29 7.90 -10 5 -9 50.59 4.60 11 -5 9 20.70 4.30 -11 -5 -9 14.90 1.70 11 -5 9 16.80 3.00 11 -5 9 17.30 3.10 11 -5 9 20.70 5.00 11 5 9 8.20 3.80 11 5 9 15.10 4.30 -11 5 -9 12.90 2.50 -11 5 -9 13.30 2.50 11 5 9 21.00 3.50 -11 5 -9 14.00 1.90 12 -5 9 0.50 2.10 -12 -5 -9 5.70 1.10 12 -5 9 3.20 2.20 12 -5 9 3.00 3.30 12 -5 9 5.40 4.10 -12 5 -9 3.00 1.60 -12 5 -9 5.60 1.60 12 5 9 2.70 3.10 -12 5 -9 1.60 1.30 12 5 9 2.00 2.30 13 -5 9 5.00 3.20 13 -5 9 4.30 2.80 13 -5 9 4.80 2.20 13 -5 9 5.70 3.70 -13 5 -9 5.20 1.30 -13 5 -9 5.20 1.70 -13 5 -9 4.90 1.90 13 5 9 3.00 2.20 14 -5 9 9.40 3.10 14 -5 9 14.20 3.90 14 -5 9 14.40 2.30 14 5 9 11.00 2.60 -14 5 -9 10.30 1.80 -14 5 -9 9.30 1.40 15 -5 9 18.30 2.40 15 -5 9 15.90 3.60 15 -5 9 18.70 2.00 15 -5 9 18.60 3.40 15 5 9 16.90 2.30 -15 5 -9 17.50 2.40 -15 5 -9 22.50 1.80 -18 -6 9 57.59 2.90 18 -6 -9 56.89 4.40 18 -6 -9 61.29 3.90 -18 -6 9 56.29 4.10 18 -6 -9 53.79 6.30 -18 6 9 58.69 4.10 -18 6 9 62.39 4.60 -18 6 9 55.49 3.00 -18 6 9 54.39 3.30 17 -6 -9 11.70 2.50 17 -6 -9 14.60 2.50 17 -6 -9 11.70 2.10 -17 -6 9 15.20 1.60 -17 6 9 14.70 1.80 -17 6 9 18.20 2.90 -17 6 9 12.10 1.90 -17 6 9 14.70 2.10 -17 6 9 10.00 1.60 16 -6 -9 9.50 2.30 16 -6 -9 10.50 2.20 -16 -6 9 8.60 1.30 16 -6 -9 9.80 2.40 -16 6 9 9.40 1.70 -16 6 9 7.90 1.70 -16 6 9 8.90 2.50 -16 6 9 8.50 1.90 -15 -6 9 25.70 2.00 15 -6 -9 26.00 3.70 15 -6 -9 28.30 5.40 15 -6 -9 23.90 3.00 15 -6 -9 25.50 2.20 15 -6 -9 20.70 3.20 -15 6 9 20.60 2.70 -15 6 9 27.80 2.90 -15 6 9 17.30 4.40 -15 6 9 28.60 3.50 -15 6 9 24.50 2.80 -14 -6 9 13.80 1.60 14 -6 -9 13.10 1.80 14 -6 -9 12.40 2.50 14 -6 -9 16.30 3.30 14 -6 -9 14.60 2.40 14 -6 -9 11.80 2.70 -14 6 9 19.30 3.60 -14 6 9 12.50 2.30 -14 6 9 9.80 2.40 -14 6 9 13.00 3.10 -13 -6 9 21.10 1.80 13 -6 -9 19.70 3.20 13 -6 -9 22.10 3.30 13 -6 -9 16.00 3.00 13 -6 -9 17.00 2.50 13 -6 -9 23.70 2.50 -13 6 9 18.50 2.50 -13 6 9 18.40 3.50 -13 6 9 20.60 3.00 -13 6 9 27.10 3.70 -13 6 9 25.40 3.20 12 -6 -9 16.20 3.00 -12 -6 9 20.60 1.70 12 -6 -9 15.20 3.10 12 -6 -9 16.60 2.70 12 -6 -9 17.80 2.20 12 -6 -9 18.60 3.40 12 -6 -9 21.90 2.00 -12 6 9 10.70 3.00 -12 6 9 19.10 2.10 -12 6 9 19.50 2.90 12 6 -9 24.30 2.70 -12 6 9 21.20 2.60 -12 6 9 19.10 3.80 -12 6 9 16.60 2.80 -11 -6 9 22.30 1.70 11 -6 -9 23.10 2.60 11 -6 -9 19.70 3.30 11 -6 -9 22.30 2.10 11 -6 -9 17.30 2.90 11 -6 -9 22.90 3.10 11 -6 -9 20.40 3.50 -11 6 9 21.10 2.90 -11 6 9 23.40 4.10 -11 6 9 32.10 3.70 11 6 -9 22.30 2.60 -11 6 9 19.30 3.20 10 -6 -9 169.78 8.70 10 -6 -9 173.88 7.20 10 -6 -9 167.18 12.60 10 -6 -9 168.28 9.00 -10 -6 9 165.58 6.50 -10 -6 9 160.18 12.40 10 -6 -9 172.78 7.60 10 -6 -9 170.28 8.00 -10 6 9 162.68 8.30 10 6 -9 166.28 7.50 10 6 -9 165.48 13.70 -10 6 9 169.58 8.20 -10 6 9 170.88 7.50 -10 6 9 167.18 12.50 -10 6 9 171.98 8.50 -10 6 9 165.98 9.50 -9 -6 9 5.80 1.00 9 -6 -9 8.30 2.30 9 -6 -9 8.10 1.60 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227.48 9.40 6 -6 -9 214.88 8.70 -6 6 9 193.58 12.20 -6 6 9 214.48 10.20 -6 6 9 215.58 13.30 6 6 -9 208.98 9.20 6 6 -9 203.38 15.50 6 6 -9 196.18 9.50 -6 6 9 222.98 10.90 -6 6 9 186.18 9.90 6 6 -9 203.28 7.90 -6 6 9 211.18 10.60 5 -6 -9 148.79 10.10 -5 -6 9 152.48 6.70 -5 -6 9 152.08 6.00 -5 -6 9 146.99 10.30 5 -6 -9 141.39 6.50 5 -6 -9 147.99 7.10 -5 6 9 157.18 11.00 5 6 -9 134.69 11.90 -5 6 9 147.39 7.10 5 6 -9 139.89 7.40 5 6 -9 142.89 5.90 -5 6 9 147.79 7.40 -5 6 9 150.38 8.00 -5 6 9 134.79 7.50 -5 6 9 146.89 7.70 -4 -6 9 210.48 13.70 -4 -6 9 238.38 8.80 4 -6 -9 245.68 10.00 4 -6 -9 235.38 13.00 4 -6 -9 237.18 9.30 4 6 -9 237.38 10.70 -4 6 9 223.18 10.00 4 6 -9 226.18 8.80 -4 6 9 248.58 11.60 -4 6 9 232.48 10.40 -4 6 9 231.78 13.60 4 6 -9 237.28 16.00 4 6 -9 225.58 10.20 -4 6 9 214.48 10.50 -3 -6 9 16.40 1.70 3 -6 -9 13.10 1.80 3 -6 -9 15.60 3.40 -3 6 9 14.40 2.80 3 6 -9 13.80 2.40 3 6 -9 12.50 1.60 -3 6 9 13.80 3.80 3 6 -9 8.80 3.50 3 6 -9 13.30 2.30 -3 6 9 16.60 2.70 -3 6 9 15.30 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16 -7 -9 4.60 1.70 16 -7 -9 5.00 1.90 -16 7 9 3.80 1.50 -16 7 9 4.70 2.10 -16 7 9 2.30 1.10 15 -7 -9 19.50 3.20 -15 -7 9 17.90 1.60 15 -7 -9 20.30 3.00 15 -7 -9 13.70 2.10 -15 7 9 13.50 2.90 -15 7 9 21.30 2.60 -15 7 9 21.40 2.20 -15 7 9 19.80 2.40 -15 7 9 17.40 3.70 14 -7 -9 3.80 1.90 14 -7 -9 3.80 1.30 -14 -7 9 3.90 0.90 14 -7 -9 2.50 1.50 14 -7 -9 5.30 2.20 -14 7 9 1.50 2.20 -14 7 9 3.50 1.60 -14 7 9 2.80 1.60 -14 7 9 3.80 2.00 13 -7 -9 10.70 2.70 -13 -7 9 13.10 1.60 13 -7 -9 10.70 2.10 13 -7 -9 7.80 2.40 13 -7 -9 7.40 1.50 -13 7 9 8.50 2.10 -13 7 9 10.80 3.10 -13 7 9 7.90 1.90 -13 7 9 9.00 2.20 12 -7 -9 68.49 5.60 12 -7 -9 66.09 3.90 12 -7 -9 61.99 5.10 12 -7 -9 67.99 4.50 12 -7 -9 62.59 3.60 -12 -7 9 63.09 3.10 12 -7 -9 58.89 4.80 -12 7 9 65.49 4.80 12 7 -9 64.59 3.90 -12 7 9 63.09 4.70 -12 7 9 64.19 5.70 11 -7 -9 51.69 5.00 11 -7 -9 58.59 5.00 11 -7 -9 58.49 3.80 -11 -7 9 55.19 2.80 11 -7 -9 54.09 3.20 11 -7 -9 62.19 4.40 11 -7 -9 55.09 4.60 11 7 -9 57.49 3.70 -11 7 9 43.30 5.00 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10.10 3.80 -6 7 9 10.70 3.30 -6 7 9 8.20 2.70 6 7 -9 10.90 1.30 -6 7 9 12.90 2.50 6 7 -9 12.90 2.20 -6 7 9 13.10 2.70 -6 7 9 14.60 2.40 -6 7 9 8.30 2.30 -6 7 9 15.10 2.80 -5 -7 9 290.07 16.10 5 -7 -9 283.17 11.30 5 -7 -9 312.17 14.70 5 -7 -9 294.57 11.40 5 -7 -9 289.47 12.90 5 -7 -9 324.17 17.40 -5 -7 9 268.17 15.70 -5 -7 9 282.87 10.70 5 -7 -9 283.27 11.60 -5 -7 9 292.97 11.50 5 7 -9 285.07 10.50 5 7 -9 288.87 12.10 -5 7 9 279.67 12.70 -5 7 9 294.17 12.30 -5 7 9 291.37 13.70 -5 7 9 275.37 12.40 -5 7 9 306.77 12.00 5 7 -9 287.27 12.20 5 7 -9 315.27 24.80 -5 7 9 278.57 12.50 -5 7 9 296.97 18.10 -4 -7 9 64.69 3.50 -4 -7 9 71.19 7.30 4 -7 -9 59.29 6.40 4 -7 -9 62.79 3.90 4 -7 -9 66.79 5.10 -4 -7 9 51.49 6.50 4 -7 -9 60.59 3.80 4 7 -9 63.19 4.80 4 7 -9 60.39 3.30 4 7 -9 62.99 4.70 -4 7 9 68.79 4.20 -4 7 9 58.09 4.80 -4 7 9 63.39 7.20 -4 7 9 63.29 4.60 4 7 -9 64.99 8.70 -4 7 9 57.59 5.00 -4 7 9 69.49 6.00 3 -7 -9 329.67 12.70 -3 -7 9 334.17 17.40 3 -7 -9 346.37 12.70 -3 -7 9 346.17 12.10 -3 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9 214.58 8.30 0 -7 9 195.98 12.70 0 7 9 207.28 12.70 0 7 -9 215.28 8.70 0 7 9 205.78 10.70 0 7 -9 213.38 10.40 0 7 -9 217.48 10.30 0 7 9 212.78 9.20 0 7 9 231.68 11.40 0 7 -9 208.98 15.80 0 7 9 212.08 10.20 0 7 9 201.78 8.10 1 -7 9 601.84 30.30 1 -7 9 661.83 22.50 -1 -7 -9 623.84 23.30 1 -7 9 660.33 21.60 1 -7 9 616.94 27.20 1 -7 9 607.04 26.80 -1 -7 -9 615.34 21.80 -1 7 -9 610.24 22.00 1 7 9 637.44 22.50 1 7 9 605.24 24.40 1 7 9 616.54 28.00 1 7 9 627.34 23.60 -1 7 -9 623.64 24.00 1 7 9 640.84 24.70 -1 7 -9 599.94 30.20 -1 7 -9 634.64 23.80 2 -7 9 540.95 28.40 2 -7 9 583.54 20.40 2 -7 9 551.24 24.40 -2 -7 -9 533.25 19.50 2 -7 9 587.74 19.40 2 -7 9 539.35 28.10 -2 7 -9 571.94 20.00 -2 7 -9 555.44 21.50 2 7 9 559.04 22.40 2 7 9 512.15 25.40 2 7 9 591.34 22.30 -2 7 -9 512.55 27.20 2 7 9 570.34 21.30 2 7 9 548.55 22.20 -2 7 -9 564.04 21.90 3 -7 9 638.84 22.10 -3 -7 -9 633.94 22.30 3 -7 9 678.43 23.30 3 -7 9 686.13 31.00 3 -7 9 642.24 28.40 3 -7 9 656.03 23.10 3 -7 9 610.44 26.80 -3 7 -9 646.84 24.40 3 7 9 661.43 24.10 3 7 9 624.44 24.70 -3 7 -9 665.03 22.90 -3 7 -9 627.34 24.70 3 7 9 653.83 25.10 3 7 9 589.04 24.90 3 7 9 657.73 27.60 4 -7 9 86.59 5.00 -4 -7 -9 82.29 4.10 4 -7 9 89.09 4.20 4 -7 9 76.09 6.90 4 7 9 82.39 6.20 -4 7 -9 92.89 6.00 5 -7 9 160.78 9.90 5 -7 9 184.68 8.20 -5 7 -9 165.88 9.00 -5 7 -9 155.68 6.50 5 7 9 153.08 9.10 5 7 9 171.68 9.00 -5 7 -9 159.48 7.40 5 7 9 160.58 8.00 6 -7 9 39.90 2.40 6 -7 9 41.40 4.10 6 -7 9 39.00 3.40 6 -7 9 38.70 3.40 6 -7 9 28.10 4.80 6 7 9 39.50 4.90 -6 7 -9 39.40 4.50 -6 7 -9 43.30 3.40 6 7 9 44.60 3.80 6 7 9 46.00 4.40 -6 7 -9 43.50 4.00 -6 7 -9 38.00 2.60 7 -7 9 33.80 3.20 7 -7 9 26.20 4.80 7 -7 9 37.20 4.00 7 -7 9 44.80 4.50 7 -7 9 32.00 3.10 -7 7 -9 33.60 3.10 -7 7 -9 36.90 3.70 -7 7 -9 40.40 4.40 7 7 9 33.50 4.60 -7 7 -9 32.10 2.40 7 7 9 37.80 3.40 8 -7 9 34.70 4.50 8 -7 9 33.40 4.00 8 -7 9 34.00 3.20 8 -7 9 37.90 3.20 8 7 9 36.40 4.80 -8 7 -9 35.60 3.30 -8 7 -9 36.00 3.20 -8 7 -9 35.70 4.20 9 -7 9 28.80 2.80 9 -7 9 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34.90 3.90 -8 8 9 41.00 3.70 -8 8 9 40.50 3.60 -8 8 9 40.20 4.30 -7 -8 9 80.19 4.20 -7 -8 9 75.69 3.80 7 -8 -9 74.79 5.10 7 -8 -9 82.99 5.90 7 -8 -9 78.39 4.90 7 -8 -9 81.69 4.60 7 -8 -9 80.89 4.50 -7 -8 9 75.59 4.60 -7 8 9 85.69 5.10 -7 8 9 82.19 5.80 -7 8 9 78.59 5.20 -7 8 9 87.59 5.50 7 8 -9 82.19 4.80 6 -8 -9 205.98 8.60 -6 -8 9 198.78 7.80 6 -8 -9 203.28 10.10 -6 -8 9 197.08 8.70 6 -8 -9 196.58 8.50 6 -8 -9 198.38 8.70 -6 8 9 200.68 9.50 -6 8 9 187.08 9.70 6 8 -9 206.98 8.90 -6 8 9 201.08 9.40 -6 8 9 195.88 9.30 -6 8 9 209.48 9.00 -5 -8 9 112.79 5.10 5 -8 -9 120.29 5.90 -5 -8 9 111.09 5.90 5 -8 -9 112.59 5.70 5 -8 -9 114.09 7.20 5 -8 -9 123.49 5.90 -5 8 9 105.89 6.70 5 8 -9 114.59 4.60 -5 8 9 119.29 6.00 5 8 -9 120.49 6.50 -5 8 9 113.39 6.70 -5 8 9 114.09 6.60 5 8 -9 116.69 6.20 -4 -8 9 169.68 12.30 4 -8 -9 186.98 8.10 4 -8 -9 184.58 8.20 -4 8 9 206.78 8.30 -4 8 9 194.08 9.50 4 8 -9 191.88 8.90 4 8 -9 191.38 7.20 -4 8 9 197.48 9.00 -4 8 9 190.88 9.40 3 -8 -9 154.88 7.00 3 -8 -9 157.38 6.80 3 -8 -9 182.18 9.20 3 -8 -9 123.99 11.30 -3 -8 9 152.48 7.50 -3 -8 9 154.48 11.20 -3 8 9 151.68 8.20 -3 8 9 156.18 6.70 3 8 -9 156.98 7.90 3 8 -9 147.09 6.10 -3 8 9 157.08 8.50 -3 8 9 157.18 7.60 3 8 -9 130.59 10.50 -2 -8 9 80.99 8.20 2 -8 -9 87.49 4.60 2 -8 -9 66.59 8.00 2 -8 -9 91.39 5.30 -2 -8 9 87.49 4.70 -2 8 9 90.79 4.30 -2 8 9 89.09 6.00 2 8 -9 84.09 6.10 2 8 -9 88.99 4.30 -2 8 9 92.49 7.30 -2 8 9 93.89 5.50 2 8 -9 91.79 6.00 -2 8 9 91.89 6.50 -1 -8 9 10.20 3.40 1 -8 -9 12.50 1.70 1 -8 -9 20.90 3.50 -1 8 9 11.40 5.00 1 8 -9 17.80 2.90 -1 8 9 18.30 2.50 1 8 -9 11.40 1.70 -1 8 9 15.10 3.20 -1 8 9 13.30 3.00 0 -8 9 7.10 1.70 0 -8 9 2.50 3.00 0 8 -9 2.70 1.90 0 8 -9 1.80 1.20 0 8 9 2.70 2.10 0 8 9 0.50 1.30 0 8 9 1.20 2.30 1 -8 9 140.29 6.00 1 -8 9 140.39 6.70 1 -8 9 131.29 9.90 -1 -8 -9 132.89 6.10 -1 8 -9 135.59 7.80 1 8 9 133.49 7.60 -1 8 -9 128.89 6.10 1 8 9 131.69 8.00 1 8 9 144.19 6.50 -1 8 -9 149.39 8.30 1 8 9 138.99 8.50 2 -8 9 133.49 5.80 2 -8 9 129.19 10.20 -2 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-7 8 -9 5.40 2.20 7 8 9 4.70 2.40 -7 8 -9 3.20 1.30 8 -8 9 25.70 2.70 8 -8 9 27.90 3.70 8 -8 9 27.10 6.10 8 -8 9 29.80 2.80 -8 8 -9 29.50 3.70 -8 8 -9 26.90 2.70 -8 8 -9 32.30 3.00 8 8 9 23.40 3.30 9 -8 9 3.20 2.00 9 -8 9 -1.00 2.10 9 -8 9 2.30 1.30 9 -8 9 3.00 2.30 9 8 9 2.10 2.00 -9 8 -9 5.70 1.90 -9 8 -9 4.40 1.30 -9 8 -9 1.70 1.70 10 -8 9 28.50 2.10 10 -8 9 24.50 3.30 10 -8 9 22.30 4.00 -10 8 -9 27.40 3.20 -10 8 -9 26.20 3.20 -10 8 -9 27.40 2.60 11 -8 9 8.40 2.70 11 -8 9 12.50 2.20 -11 8 -9 12.50 2.00 11 8 9 13.70 2.10 -11 8 -9 17.80 1.90 13 -9 -9 29.30 3.20 -13 -9 9 25.30 1.50 13 -9 -9 28.60 3.10 13 -9 -9 26.70 1.80 13 -9 -9 28.00 3.00 -13 9 9 27.30 2.90 -13 9 9 27.70 2.30 -13 9 9 26.90 2.30 12 -9 -9 1.90 1.60 12 -9 -9 0.90 1.10 -12 -9 9 3.20 0.60 -12 9 9 3.50 1.60 -12 9 9 0.10 1.90 -12 9 9 2.90 1.80 11 -9 -9 116.49 5.00 11 -9 -9 103.19 5.10 11 -9 -9 115.49 6.70 11 -9 -9 111.19 6.20 11 -9 -9 107.99 4.50 -11 9 9 117.89 5.50 -11 9 9 111.09 5.70 10 -9 -9 17.70 2.70 -10 -9 9 15.60 1.30 10 -9 -9 12.60 1.70 10 -9 -9 17.30 1.80 10 -9 -9 16.30 3.00 -10 9 9 16.70 2.70 -10 9 9 17.20 2.10 -10 9 9 16.30 2.40 10 9 -9 16.70 2.10 -10 9 9 14.10 2.10 9 -9 -9 18.20 2.20 9 -9 -9 16.50 2.70 -9 -9 9 17.80 1.50 9 -9 -9 18.40 3.20 9 -9 -9 14.50 1.80 9 -9 -9 19.10 2.00 -9 9 9 20.60 2.90 -9 9 9 20.00 2.70 -9 9 9 13.10 2.00 -9 9 9 15.50 2.10 9 9 -9 17.90 2.20 -8 -9 9 9.10 1.20 8 -9 -9 6.90 1.60 -8 -9 9 8.40 1.70 8 -9 -9 8.20 2.40 -8 -9 9 8.50 3.50 8 -9 -9 10.20 1.70 -8 9 9 11.60 1.90 8 9 -9 7.50 1.60 -8 9 9 4.00 1.80 -8 9 9 6.40 2.40 -8 9 9 9.20 2.00 -7 -9 9 20.50 2.80 7 -9 -9 24.20 2.70 7 -9 -9 29.70 3.80 -7 -9 9 20.30 4.90 7 -9 -9 29.70 2.60 -7 -9 9 28.90 2.20 7 -9 -9 27.80 2.70 -7 9 9 25.40 2.70 -7 9 9 25.90 3.20 -7 9 9 32.60 4.10 -7 9 9 28.10 3.30 7 9 -9 27.50 2.80 6 -9 -9 10.60 1.80 6 -9 -9 7.20 2.20 6 -9 -9 8.60 1.60 -6 -9 9 9.40 3.80 -6 -9 9 11.30 1.60 -6 -9 9 10.10 1.40 6 -9 -9 11.30 1.70 -6 -9 9 8.00 1.80 -6 9 9 10.40 2.10 5 -9 -9 8.70 1.50 -5 -9 9 4.30 1.60 -5 -9 9 -2.70 2.30 5 -9 -9 7.10 1.50 5 -9 -9 1.50 1.70 -5 -9 9 3.30 1.10 -5 9 9 4.00 1.70 5 9 -9 3.20 1.50 -5 9 9 3.50 2.00 -4 -9 9 55.69 4.00 4 -9 -9 52.09 3.80 4 -9 -9 56.69 4.70 -4 -9 9 49.80 6.30 -4 -9 9 57.79 3.20 4 -9 -9 54.19 3.60 4 9 -9 61.79 4.40 -4 9 9 58.49 4.70 -4 9 9 56.29 4.20 4 9 -9 58.19 4.20 3 -9 -9 84.69 4.60 -3 -9 9 85.19 5.00 3 -9 -9 83.69 5.70 3 -9 -9 83.49 5.30 -3 -9 9 82.39 7.90 -3 -9 9 89.09 4.20 3 9 -9 82.89 5.20 -3 9 9 77.09 5.70 -3 9 9 89.79 4.20 3 9 -9 86.19 5.40 -3 9 9 85.09 5.00 2 -9 -9 93.69 5.40 2 -9 -9 104.79 6.70 -2 -9 9 97.19 5.50 2 -9 -9 103.69 6.20 -2 -9 9 102.39 4.70 -2 -9 9 97.89 8.70 2 -9 -9 98.79 5.10 -2 9 9 101.49 6.30 2 9 -9 107.09 6.20 2 9 -9 105.99 6.00 -2 9 9 102.49 5.50 2 9 -9 95.59 4.60 -2 9 9 95.59 6.40 -1 -9 9 49.10 3.90 1 -9 -9 51.09 3.40 -1 -9 9 54.69 3.20 -1 -9 9 52.09 3.80 1 -9 -9 55.79 3.30 1 -9 -9 50.79 4.30 -1 -9 9 52.89 6.20 1 9 -9 52.79 4.50 -1 9 9 66.99 5.20 -1 9 9 48.80 4.90 1 9 -9 48.80 2.90 -1 9 9 53.39 4.50 1 9 -9 53.59 4.40 0 -9 9 44.50 3.60 0 -9 -9 41.60 3.10 0 -9 9 41.40 2.80 0 -9 9 40.40 4.80 0 -9 -9 40.20 4.00 0 9 -9 45.30 2.70 0 9 9 39.10 4.50 0 9 -9 43.00 4.10 0 9 9 43.30 4.20 0 9 -9 45.40 4.30 -1 -9 -9 4.30 1.10 1 -9 9 1.60 1.60 -1 -9 -9 -0.90 1.50 1 -9 9 1.20 1.10 1 -9 9 4.00 2.10 1 -9 9 0.10 2.40 -1 9 -9 0.10 1.10 1 9 9 1.40 1.60 1 9 9 1.60 1.20 -1 9 -9 7.20 2.10 -1 9 -9 -1.80 1.50 1 9 9 2.70 2.10 2 -9 9 23.50 3.00 2 -9 9 22.30 4.10 -2 -9 -9 21.60 2.10 2 -9 9 23.30 2.20 2 -9 9 23.20 3.00 -2 9 -9 18.30 4.80 -2 9 -9 26.20 3.30 -3 -9 -9 86.29 4.20 3 -9 9 89.19 4.10 3 -9 9 89.19 5.20 -3 -9 -9 90.09 5.30 3 -9 9 82.09 4.90 -3 9 -9 80.59 5.50 -3 9 -9 82.69 4.40 3 9 9 76.29 6.30 -3 9 -9 94.29 6.50 4 -9 9 33.90 3.00 -4 -9 -9 31.30 2.30 4 -9 9 28.40 2.10 4 -9 9 29.00 3.20 -4 -9 -9 28.80 2.80 4 -9 9 32.40 4.40 -4 9 -9 29.50 2.60 -4 9 -9 30.60 3.80 4 9 9 31.20 4.10 5 -9 9 70.69 3.20 5 -9 9 68.49 4.10 -5 -9 -9 63.29 3.30 5 -9 9 63.69 4.30 5 -9 9 68.69 4.70 -5 9 -9 74.49 3.90 -5 9 -9 73.69 4.80 -5 9 -9 71.49 5.20 5 9 9 72.39 5.40 6 -9 9 6.10 1.90 6 -9 9 6.50 1.60 6 -9 9 7.10 1.70 6 -9 9 6.10 1.60 -6 9 -9 4.50 1.30 -6 9 -9 5.60 1.60 6 9 9 7.90 2.40 -6 9 -9 7.50 2.10 7 -9 9 14.00 2.70 7 -9 9 13.00 2.30 7 -9 9 12.80 1.80 7 9 9 13.50 2.60 -7 9 -9 9.50 2.10 -7 9 -9 14.20 2.10 -7 9 -9 14.00 1.80 8 -9 9 8.20 1.40 8 -9 9 11.10 1.50 -8 9 -9 8.50 1.50 -8 9 -9 15.70 2.90 8 9 9 7.70 2.30 9 -9 9 1.50 1.60 9 -9 9 2.50 1.00 -9 9 -9 3.30 1.50 -9 9 -9 2.70 1.00 9 9 9 5.20 1.60 11 -10 -9 11.50 1.50 11 -10 -9 10.80 2.00 11 -10 -9 5.20 1.60 -11 10 9 10.90 1.40 -11 10 9 10.10 1.30 10 -10 -9 2.40 0.80 10 -10 -9 3.30 1.40 -10 -10 9 4.80 0.70 10 -10 -9 2.70 1.50 -10 10 9 3.90 0.90 -10 10 9 3.50 0.90 -10 10 9 4.40 1.40 9 -10 -9 91.59 3.90 9 -10 -9 87.49 4.10 9 -10 -9 94.29 5.50 -9 -10 9 90.09 3.60 9 -10 -9 92.39 5.10 -9 10 9 95.59 4.20 -9 10 9 92.09 3.90 9 10 -9 94.19 4.00 -9 10 9 86.69 4.80 8 -10 -9 11.50 3.40 8 -10 -9 10.20 1.90 8 -10 -9 7.90 1.20 8 -10 -9 10.30 3.30 8 10 -9 12.10 1.60 -8 10 9 9.00 1.10 -8 10 9 7.10 1.70 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46.20 3.50 -2 -10 9 49.90 3.30 2 -10 -9 47.80 3.70 2 10 -9 50.49 3.60 -2 10 9 45.70 4.00 2 10 -9 45.40 3.60 -2 10 9 45.30 3.10 -1 -10 9 5.30 1.10 -1 -10 9 6.60 1.70 1 -10 -9 5.50 2.10 1 -10 -9 6.90 1.30 -1 10 9 6.70 1.40 1 10 -9 6.70 1.80 -1 10 9 8.50 2.10 1 10 -9 6.30 1.90 0 -10 9 3.80 1.60 0 -10 9 7.20 1.50 0 -10 -9 6.20 1.20 0 -10 9 5.30 1.10 0 10 -9 3.70 1.60 0 10 -9 4.00 0.90 0 10 9 4.40 1.60 0 10 -9 1.80 1.70 0 10 9 4.40 1.90 1 -10 9 7.70 1.80 1 -10 9 8.20 1.20 1 -10 9 8.90 1.70 1 -10 9 7.60 1.80 -1 -10 -9 8.40 1.20 1 10 9 8.30 2.20 -1 10 -9 6.50 1.00 -1 10 -9 5.40 1.80 1 10 9 6.30 1.30 -1 10 -9 5.60 1.80 2 -10 9 56.39 2.90 2 -10 9 56.19 3.50 2 -10 9 46.90 4.00 2 -10 9 48.20 3.70 -2 -10 -9 55.19 2.90 -2 10 -9 59.39 2.80 -2 10 -9 58.19 4.10 2 10 9 58.29 4.50 -2 10 -9 55.79 4.10 3 -10 9 27.20 2.70 3 -10 9 25.60 2.80 -3 -10 -9 29.40 1.90 3 -10 9 31.30 2.90 3 -10 9 30.50 1.90 -3 10 -9 28.00 3.00 -3 10 -9 29.40 2.90 3 10 9 32.90 3.50 -3 10 -9 29.10 2.00 4 -10 9 29.60 2.80 -4 -10 -9 24.40 1.70 4 -10 9 28.00 2.60 4 -10 9 26.50 1.70 4 -10 9 24.20 2.70 -4 10 -9 29.30 3.50 4 10 9 19.80 3.50 -4 10 -9 22.90 2.60 5 -10 9 49.50 3.30 5 -10 9 48.90 3.10 5 -10 9 44.50 3.50 5 -10 9 57.79 3.00 -5 10 -9 47.80 3.60 -5 10 -9 51.19 2.70 5 10 9 52.79 3.90 -5 10 -9 53.29 4.10 6 -10 9 129.99 5.40 6 -10 9 119.59 5.90 6 -10 9 124.89 5.40 -6 10 -9 133.49 6.10 -6 10 -9 131.59 5.10 -6 10 -9 121.49 5.70 6 10 9 123.69 6.10 7 -10 9 3.70 1.00 7 -10 9 3.30 1.30 -7 10 -9 2.90 1.20 -7 10 -9 4.80 1.30 7 10 9 3.80 1.40 -7 10 -9 2.80 0.80 6 -11 -9 19.50 1.50 6 -11 -9 18.00 2.90 -6 -11 9 17.80 1.30 -6 11 9 15.30 1.80 -6 11 9 17.10 1.70 6 11 -9 16.70 1.40 5 -11 -9 55.99 2.80 5 -11 -9 55.29 3.90 -5 -11 9 53.49 2.50 5 11 -9 58.19 3.60 -5 11 9 56.19 2.90 -5 11 9 53.59 3.10 -4 -11 9 7.90 1.40 4 -11 -9 8.60 1.80 -4 -11 9 9.10 1.10 -4 -11 9 9.80 1.20 4 -11 -9 9.40 1.20 4 11 -9 9.30 1.20 -4 11 9 6.60 1.10 -4 11 9 9.10 1.50 3 -11 -9 91.99 3.90 -3 -11 9 87.69 3.60 3 -11 -9 88.29 5.30 -3 -11 9 82.09 4.00 -3 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3.50 -5 -4 14 50.39 2.80 -5 4 14 49.40 5.90 -5 4 14 50.49 3.90 -5 4 14 43.70 4.30 5 4 -14 45.10 3.10 5 4 -14 55.69 7.80 -5 4 14 35.20 4.40 5 4 -14 50.29 3.50 -5 4 14 49.30 4.10 4 -4 -14 730.33 25.70 -4 -4 14 743.03 24.80 4 -4 -14 745.93 25.70 -4 -4 14 737.13 26.20 -4 -4 14 751.12 31.80 4 -4 -14 714.03 29.20 -4 -4 14 756.72 25.80 -4 4 14 746.73 28.10 -4 4 14 729.83 30.70 -4 4 14 728.73 26.80 4 4 -14 728.23 35.00 -4 4 14 736.23 26.30 4 4 -14 753.32 25.50 4 4 -14 741.63 26.00 -4 4 14 695.63 27.20 3 -4 -14 23.10 3.90 -3 -4 14 22.00 2.00 -3 -4 14 24.60 5.20 3 -4 -14 27.10 2.60 -3 -4 14 25.40 3.20 3 -4 -14 26.40 2.50 -3 -4 14 20.10 2.50 -3 4 14 24.10 4.60 -3 4 14 23.50 3.10 3 4 -14 23.60 2.70 -3 4 14 21.60 3.70 -3 4 14 20.80 3.40 3 4 -14 14.70 4.80 3 4 -14 22.50 2.50 3 4 -14 20.00 3.00 -3 4 14 20.00 3.00 -2 -4 14 540.25 19.60 2 -4 -14 539.65 19.00 -2 -4 14 520.55 18.10 2 -4 -14 520.85 22.10 2 -4 -14 548.65 19.00 -2 -4 14 529.85 24.60 -2 -4 14 531.15 19.20 2 4 -14 550.74 25.50 -2 4 14 533.75 20.20 -2 4 14 524.45 23.20 -2 4 14 517.75 21.20 2 4 -14 533.05 18.90 -2 4 14 542.65 21.20 -2 4 14 526.05 20.80 2 4 -14 513.35 18.40 2 4 -14 519.75 27.40 2 4 -14 516.05 19.60 -1 -4 14 180.98 11.80 1 -4 -14 175.28 10.00 -1 -4 14 184.38 6.90 1 -4 -14 186.78 7.70 -1 -4 14 185.28 8.30 -1 -4 14 179.38 7.90 -1 -4 14 159.28 9.90 -1 -4 14 174.98 8.70 1 -4 -14 173.68 7.50 -1 4 14 178.58 8.70 1 4 -14 186.78 7.70 -1 4 14 169.08 9.00 1 4 -14 182.28 8.40 -1 4 14 167.28 10.70 1 4 -14 167.08 12.70 -1 4 14 177.98 9.60 -1 4 14 175.58 9.20 1 4 -14 177.68 14.00 1 4 -14 178.18 7.20 0 -4 14 60.09 6.20 0 -4 14 68.39 4.70 0 -4 14 64.09 5.30 0 -4 14 69.49 3.30 0 -4 -14 75.09 4.00 0 -4 14 69.89 4.50 0 -4 -14 65.69 5.80 0 -4 14 55.49 7.00 0 -4 -14 72.19 4.00 0 4 14 59.19 5.30 0 4 14 66.79 6.20 0 4 -14 87.89 5.10 0 4 14 56.79 5.30 0 4 14 72.29 5.90 0 4 -14 84.39 9.20 0 4 -14 68.49 4.10 0 4 -14 71.59 9.30 0 4 -14 69.89 3.70 0 4 14 65.99 4.90 1 -4 14 48.50 8.60 1 -4 14 31.50 4.00 -1 -4 -14 36.30 2.80 -1 -4 -14 34.90 4.60 1 -4 14 46.40 3.80 -1 -4 -14 38.70 2.90 1 -4 14 38.70 2.30 1 -4 14 38.90 3.30 -1 4 -14 41.70 3.60 1 4 14 38.20 4.50 -1 4 -14 25.80 6.10 -1 4 -14 35.10 3.00 1 4 14 30.40 4.20 1 4 14 45.60 5.60 1 4 14 39.50 3.80 -1 4 -14 40.00 2.70 -1 4 -14 23.30 5.60 1 4 14 38.80 4.50 2 -4 14 25.80 5.60 2 -4 14 22.40 3.50 -2 -4 -14 24.70 2.50 2 -4 14 23.00 3.00 -2 -4 -14 24.80 4.20 -2 -4 -14 28.70 2.50 2 -4 14 28.30 3.20 -2 4 -14 19.80 2.80 2 4 14 31.30 3.80 -2 4 -14 36.90 2.90 2 4 14 27.20 3.80 2 4 14 34.20 5.10 -2 4 -14 31.70 2.50 -2 4 -14 41.90 8.80 2 4 14 35.80 6.60 2 4 14 28.10 3.70 2 4 14 33.70 4.10 3 -4 14 9.50 2.10 -3 -4 -14 7.20 1.50 3 -4 14 8.30 4.50 3 -4 14 1.20 2.20 -3 -4 -14 8.50 1.50 3 -4 14 4.90 1.90 -3 -4 -14 6.80 2.60 -3 -4 -14 2.30 3.10 3 -4 14 2.40 2.90 3 4 14 2.50 4.30 3 4 14 10.40 2.80 3 4 14 8.90 3.20 -3 4 -14 7.70 1.50 -3 4 -14 11.70 1.80 3 4 14 7.10 2.20 3 4 14 7.60 2.30 3 4 14 8.00 2.70 -3 4 -14 4.70 1.60 -3 4 -14 9.60 4.60 4 -4 14 282.57 11.40 -4 -4 -14 303.47 12.60 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4 -14 3.90 1.30 7 4 14 3.40 3.50 7 4 14 3.40 2.20 7 4 14 4.40 2.30 8 -4 14 262.57 9.90 8 -4 14 241.18 14.40 -8 -4 -14 261.17 9.80 8 -4 14 267.37 15.00 8 -4 14 227.58 14.20 8 -4 14 244.38 11.40 8 -4 14 253.47 10.10 -8 4 -14 256.07 10.00 8 4 14 270.37 10.50 9 -4 14 4.60 3.30 9 -4 14 9.70 3.20 -9 -4 -14 6.40 1.20 9 -4 14 4.20 2.00 9 -4 14 7.20 1.40 9 -4 14 4.60 2.30 9 4 14 3.80 2.40 -9 4 -14 5.20 1.30 9 4 14 8.90 2.10 -9 4 -14 6.60 1.50 9 4 14 3.70 3.50 10 -4 14 157.98 6.50 -10 -4 -14 167.38 6.60 10 -4 14 161.68 8.10 10 -4 14 142.99 10.10 10 -4 14 159.68 8.10 10 -4 14 154.58 12.10 -10 4 -14 163.48 6.60 -10 4 -14 184.18 7.20 10 4 14 182.38 11.50 10 4 14 170.38 7.80 10 4 14 159.78 8.60 11 -4 14 63.59 6.50 11 -4 14 65.09 4.60 -11 -4 -14 60.19 3.90 11 -4 14 64.69 4.80 11 4 14 63.59 3.90 -11 4 -14 62.19 3.30 11 4 14 66.99 5.10 12 -4 14 328.67 12.30 12 -4 14 314.37 12.40 -12 -4 -14 330.07 11.30 12 -4 14 301.57 14.40 12 4 14 315.17 11.50 -12 4 -14 325.77 11.20 12 4 14 321.17 12.70 -17 -5 14 23.00 1.80 -17 -5 14 21.50 2.00 -17 -5 14 22.20 2.80 17 -5 -14 20.80 2.60 -17 5 14 21.20 2.20 -17 5 14 19.80 2.20 -17 5 14 25.80 2.80 -17 5 14 25.40 2.80 -16 -5 14 8.80 1.30 -16 -5 14 7.90 1.40 16 -5 -14 9.80 1.10 16 -5 -14 8.80 2.40 16 -5 -14 9.80 1.90 -16 -5 14 8.20 1.40 -16 5 14 8.50 1.50 -16 5 14 7.40 1.70 15 -5 -14 8.60 2.10 15 -5 -14 10.10 1.90 15 -5 -14 6.10 1.70 15 -5 -14 8.10 1.30 -15 -5 14 11.40 1.60 -15 5 14 11.00 2.10 -15 5 14 10.90 2.50 -15 5 14 12.70 2.20 -15 5 14 11.70 2.00 -14 -5 14 24.80 2.40 14 -5 -14 24.20 3.10 14 -5 -14 24.80 3.20 14 -5 -14 25.90 3.10 14 -5 -14 27.50 2.40 -14 -5 14 24.80 2.40 -14 5 14 31.40 2.90 -14 5 14 28.90 3.40 -14 5 14 26.20 3.30 -14 5 14 23.00 3.20 -13 -5 14 21.60 2.20 13 -5 -14 19.50 3.20 13 -5 -14 17.60 2.80 13 -5 -14 18.40 3.10 13 -5 -14 20.60 2.40 -13 5 14 20.60 2.30 -13 5 14 19.20 3.90 -13 5 14 15.80 2.60 13 5 -14 18.90 1.70 12 -5 -14 12.40 2.60 -12 -5 14 18.10 2.00 12 -5 -14 13.00 2.90 12 -5 -14 18.90 2.30 12 -5 -14 15.40 2.40 12 5 -14 15.00 2.10 -12 5 14 14.10 2.60 -12 5 14 18.70 3.00 -12 5 14 19.80 2.90 11 -5 -14 104.49 6.00 -11 -5 14 106.89 4.80 11 -5 -14 94.59 5.70 11 -5 -14 99.59 6.40 11 -5 -14 99.59 5.80 11 -5 -14 106.09 5.40 11 -5 -14 95.99 6.30 11 5 -14 100.79 5.30 -11 5 14 107.99 6.70 -11 5 14 104.99 6.30 -11 5 14 99.79 6.20 11 5 -14 101.29 4.80 -11 5 14 104.59 6.60 -11 5 14 109.19 5.40 10 -5 -14 2.20 1.80 10 -5 -14 2.40 1.50 -10 -5 14 2.80 1.20 10 -5 -14 1.60 1.50 -10 -5 14 -0.30 1.40 10 -5 -14 1.50 1.10 10 -5 -14 1.80 1.60 10 -5 -14 2.60 2.90 -10 5 14 3.10 2.00 -10 5 14 0.30 1.60 -10 5 14 2.40 1.90 10 5 -14 0.90 1.30 -10 5 14 4.20 2.20 -10 5 14 5.30 1.60 10 5 -14 3.90 1.20 -9 -5 14 154.38 7.00 -9 -5 14 163.28 6.40 9 -5 -14 152.68 8.40 9 -5 -14 154.28 7.70 9 -5 -14 156.28 6.90 9 -5 -14 158.68 7.60 9 -5 -14 161.08 7.30 -9 5 14 155.68 7.90 -9 5 14 148.49 7.50 9 5 -14 160.68 7.10 -9 5 14 154.78 8.80 9 5 -14 150.48 6.70 -8 -5 14 76.99 5.00 8 -5 -14 61.99 6.90 -8 -5 14 77.69 6.30 8 -5 -14 72.49 4.70 8 -5 -14 75.09 4.80 8 -5 -14 76.29 4.60 8 5 -14 73.79 4.20 -8 5 14 88.59 8.30 8 5 -14 77.89 4.50 -8 5 14 72.59 5.00 -8 5 14 84.59 5.50 7 -5 -14 59.39 4.90 -7 -5 14 66.29 3.40 -7 -5 14 61.09 4.10 7 -5 -14 67.99 4.10 -7 5 14 61.49 5.70 6 -5 -14 8.00 1.60 6 -5 -14 8.50 1.90 -6 -5 14 5.90 1.30 -6 -5 14 6.20 1.90 -6 -5 14 2.10 3.20 -6 -5 14 8.50 1.60 6 -5 -14 3.40 2.80 -6 5 14 6.30 2.30 -6 5 14 6.70 2.10 -6 5 14 6.80 2.00 6 5 -14 8.70 1.60 -6 5 14 6.70 3.60 6 5 -14 6.70 1.60 6 5 -14 4.70 4.60 -5 -5 14 209.68 9.00 5 -5 -14 227.48 9.20 5 -5 -14 216.88 12.20 -5 -5 14 226.78 8.30 5 -5 -14 224.48 9.10 -5 -5 14 226.98 9.60 -5 -5 14 190.28 13.30 -5 5 14 206.08 13.40 5 5 -14 215.48 8.80 -5 5 14 227.68 11.60 -5 5 14 220.18 9.80 5 5 -14 224.28 9.40 -5 5 14 213.18 10.50 -5 5 14 217.08 10.30 -5 5 14 221.68 9.80 5 5 -14 213.18 17.20 -4 -5 14 143.89 6.80 -4 -5 14 152.48 6.00 4 -5 -14 132.59 9.20 -4 -5 14 134.39 10.70 4 -5 -14 138.49 6.70 -4 -5 14 147.39 7.30 4 -5 -14 151.58 6.80 -4 5 14 142.09 7.80 4 5 -14 148.29 7.10 -4 5 14 152.68 8.30 -4 5 14 138.89 8.70 -4 5 14 139.29 7.10 4 5 -14 146.09 13.30 4 5 -14 148.89 6.40 -4 5 14 145.49 10.60 -4 5 14 145.59 7.60 3 -5 -14 242.18 12.70 -3 -5 14 239.68 10.00 3 -5 -14 242.88 9.80 -3 -5 14 228.38 14.60 -3 -5 14 244.98 9.00 -3 -5 14 243.78 10.50 3 5 -14 244.08 9.60 -3 5 14 239.98 14.10 -3 5 14 243.88 11.20 3 5 -14 235.58 17.80 -3 5 14 247.38 10.30 -3 5 14 247.98 11.60 -3 5 14 238.08 12.10 3 5 -14 234.48 10.30 -3 5 14 230.98 10.90 -2 -5 14 7.00 1.20 -2 -5 14 8.40 2.20 -2 -5 14 8.90 2.00 -2 -5 14 2.80 2.80 2 -5 -14 6.10 1.50 2 -5 -14 6.50 1.60 2 -5 -14 5.90 2.80 2 5 -14 10.60 4.90 -2 5 14 6.10 2.50 -2 5 14 10.40 2.40 -2 5 14 10.70 3.40 2 5 -14 5.60 1.80 -2 5 14 14.20 2.40 2 5 -14 6.60 1.50 -2 5 14 6.80 2.50 -2 5 14 10.50 2.60 1 -5 -14 680.23 27.30 -1 -5 14 720.93 24.80 1 -5 -14 709.13 24.40 -1 -5 14 691.23 30.50 -1 -5 14 712.43 23.50 1 -5 -14 709.93 24.30 -1 -5 14 719.93 25.20 -1 -5 14 660.93 28.20 -1 -5 14 631.64 25.20 -1 5 14 709.43 26.40 -1 5 14 677.63 29.20 1 5 -14 683.73 23.70 -1 5 14 704.03 27.00 -1 5 14 694.73 25.80 1 5 -14 709.03 25.30 1 5 -14 718.33 24.30 -1 5 14 664.13 26.00 0 -5 -14 11.30 3.00 0 -5 -14 5.30 1.40 0 -5 14 6.70 2.00 0 -5 14 8.10 1.20 0 -5 14 2.90 2.90 0 -5 14 6.60 2.20 0 -5 -14 5.20 1.40 0 -5 14 2.70 1.90 0 -5 14 1.40 3.10 0 5 -14 2.20 5.30 0 5 14 1.10 2.20 0 5 14 6.70 2.80 0 5 14 7.10 2.70 0 5 -14 6.30 1.30 0 5 -14 5.50 1.90 0 5 14 10.90 3.10 0 5 14 9.00 2.80 0 5 -14 6.50 1.60 -1 -5 -14 6.80 1.50 1 -5 14 7.20 1.10 1 -5 14 4.60 3.10 1 -5 14 7.00 2.00 1 5 14 4.00 2.40 2 -5 14 8.70 2.10 -2 -5 -14 9.50 2.30 2 -5 14 8.80 2.50 -2 -5 -14 9.60 1.50 2 5 14 8.00 2.60 -2 5 -14 6.90 1.40 -2 5 -14 11.80 1.80 2 5 14 7.30 2.60 -2 5 -14 7.00 1.90 2 5 14 10.90 2.60 3 -5 14 129.59 6.30 -3 -5 -14 128.39 5.80 3 -5 14 109.69 7.10 -3 -5 -14 128.79 5.70 3 -5 14 124.99 6.50 -3 5 -14 121.79 5.50 3 5 14 125.29 7.80 3 5 14 128.89 7.80 3 5 14 124.79 7.10 -3 5 -14 125.09 6.00 -3 5 -14 135.89 6.90 3 5 14 123.39 7.80 -4 -5 -14 49.40 3.10 -4 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5 -14 35.00 2.70 -8 5 -14 36.00 3.20 -9 -5 -14 210.08 7.80 9 -5 14 195.38 9.40 9 5 14 211.88 9.90 9 5 14 200.78 9.00 -9 5 -14 201.68 8.20 -9 5 -14 208.28 7.80 -9 5 -14 199.28 8.20 10 -5 14 12.40 2.30 10 -5 14 8.50 1.80 10 -5 14 11.20 2.00 10 -5 14 11.40 3.20 -10 -5 -14 11.50 1.40 10 5 14 14.80 2.70 10 5 14 11.20 1.90 -10 5 -14 13.60 1.70 -10 5 -14 12.70 2.00 11 -5 14 123.49 6.30 11 -5 14 138.49 6.40 -11 -5 -14 130.79 5.20 11 -5 14 116.59 7.60 -11 5 -14 142.29 5.20 11 5 14 136.49 6.70 -11 5 -14 141.19 5.30 -16 -6 14 60.69 3.10 16 -6 -14 61.49 3.70 16 -6 -14 63.69 4.00 -16 6 14 56.09 5.60 -16 6 14 60.89 3.60 -16 6 14 61.99 3.50 -15 -6 14 10.00 1.30 15 -6 -14 6.40 2.90 15 -6 -14 13.60 1.60 -15 -6 14 8.00 1.80 15 -6 -14 12.20 1.90 -15 -6 14 12.60 1.60 15 -6 -14 9.80 3.20 -15 6 14 12.20 2.10 -15 6 14 12.20 2.80 14 -6 -14 92.69 5.60 14 -6 -14 86.19 5.40 -14 -6 14 93.49 4.20 -14 -6 14 90.59 4.30 14 -6 -14 85.89 5.00 14 -6 -14 88.29 4.20 -14 6 14 90.49 5.20 -14 6 14 89.59 5.20 -14 6 14 84.49 8.00 13 -6 -14 18.30 2.90 -13 -6 14 21.60 2.00 13 -6 -14 12.70 2.20 13 -6 -14 20.30 3.10 -13 -6 14 22.70 2.40 13 -6 -14 17.90 2.00 -13 6 14 23.90 3.00 -13 6 14 15.80 2.80 -13 6 14 18.20 2.60 12 -6 -14 164.08 7.50 12 -6 -14 161.98 6.90 12 -6 -14 145.49 10.40 12 -6 -14 161.78 8.30 12 6 -14 157.88 6.90 -12 6 14 154.08 7.80 -12 6 14 155.38 7.80 -12 6 14 156.08 8.20 -11 -6 14 7.70 1.30 11 -6 -14 6.40 1.30 11 -6 -14 7.80 2.40 11 6 -14 8.10 1.10 -11 6 14 2.30 2.40 10 -6 -14 148.09 8.10 10 -6 -14 151.68 7.30 10 -6 -14 145.19 6.80 10 -6 -14 139.79 6.20 -10 -6 14 147.19 6.00 -10 6 14 144.49 8.10 -10 6 14 149.49 7.30 -10 6 14 145.29 7.60 -10 6 14 152.08 7.80 10 6 -14 152.18 6.70 -9 -6 14 81.39 4.00 9 -6 -14 86.99 6.00 -9 -6 14 82.39 4.70 9 -6 -14 83.29 4.40 9 -6 -14 78.79 5.00 9 -6 -14 85.19 4.90 9 6 -14 83.49 4.70 -9 6 14 79.09 5.50 9 6 -14 79.09 4.00 -9 6 14 81.79 5.90 -9 6 14 76.49 5.00 -9 6 14 86.79 5.60 -8 -6 14 200.68 7.50 -8 -6 14 185.18 8.20 8 -6 -14 198.58 8.40 8 -6 -14 193.48 8.10 8 -6 -14 185.48 9.70 8 -6 -14 192.38 8.70 8 6 -14 191.38 8.20 -8 6 14 180.58 8.80 -8 6 14 199.18 9.10 8 6 -14 187.58 7.70 -8 6 14 193.38 9.10 -8 6 14 185.58 10.00 7 -6 -14 10.60 2.60 -7 -6 14 8.40 1.50 7 -6 -14 12.00 2.10 7 -6 -14 10.70 2.20 7 -6 -14 8.30 1.70 -7 -6 14 5.20 1.80 -7 -6 14 8.90 1.40 -7 6 14 7.70 2.60 7 6 -14 8.00 1.70 -7 6 14 12.10 1.90 -7 6 14 9.30 2.20 -7 6 14 7.60 2.20 7 6 -14 7.90 1.50 6 -6 -14 18.80 3.10 -6 -6 14 24.60 2.10 -6 -6 14 25.90 3.00 6 -6 -14 29.70 2.80 -6 -6 14 26.20 2.70 6 -6 -14 21.00 2.50 6 6 -14 21.40 2.80 -6 6 14 21.70 3.00 -6 6 14 19.90 3.00 -6 6 14 24.30 3.00 -6 6 14 23.70 4.10 6 6 -14 22.00 2.40 -5 -6 14 113.39 5.70 -5 -6 14 118.89 6.30 5 -6 -14 113.89 5.80 -5 -6 14 124.89 5.10 5 6 -14 115.69 5.40 -5 6 14 119.99 7.90 -5 6 14 109.39 6.40 -5 6 14 113.69 6.40 5 6 -14 120.79 6.10 -5 6 14 115.99 6.90 -4 -6 14 232.88 10.00 4 -6 -14 218.98 9.30 -4 -6 14 230.48 9.50 -4 -6 14 229.48 8.60 4 -6 -14 227.18 9.40 -4 6 14 225.98 11.90 -4 6 14 231.18 10.60 4 6 -14 222.08 9.00 -4 6 14 217.58 10.30 -4 6 14 220.08 9.80 4 6 -14 233.68 9.80 3 -6 -14 1.50 1.20 -3 -6 14 5.70 2.90 -3 -6 14 4.00 2.00 -3 -6 14 4.40 1.70 -3 -6 14 2.50 1.00 3 -6 -14 3.30 1.40 -3 6 14 0.00 2.10 3 6 -14 4.30 1.30 -3 6 14 2.50 1.70 -3 6 14 2.30 2.30 3 6 -14 0.50 1.60 -3 6 14 4.70 1.90 -3 6 14 4.20 1.90 2 -6 -14 213.38 8.80 -2 -6 14 189.68 12.10 -2 -6 14 203.48 7.90 -2 -6 14 213.08 9.40 2 -6 -14 217.08 8.70 -2 -6 14 203.78 9.00 -2 6 14 210.08 11.20 -2 6 14 218.98 10.70 -2 6 14 200.68 9.90 -2 6 14 204.18 10.00 -2 6 14 204.78 9.00 2 6 -14 215.88 8.50 2 6 -14 205.88 9.40 -1 -6 14 9.70 4.50 -1 -6 14 16.60 1.80 -1 -6 14 16.00 2.50 -1 -6 14 13.40 2.40 1 -6 -14 15.00 2.00 1 -6 -14 15.20 2.10 -1 -6 14 12.20 2.40 -1 6 14 18.70 3.20 1 6 -14 14.50 2.10 -1 6 14 14.80 2.90 -1 6 14 14.20 3.30 -1 6 14 15.70 3.10 1 6 -14 15.80 2.60 0 -6 14 55.79 4.40 0 -6 -14 53.29 3.50 0 -6 14 57.09 4.20 0 -6 -14 49.00 3.40 0 -6 14 52.79 2.90 0 -6 14 49.70 4.20 0 6 14 53.19 5.20 0 6 14 55.19 4.80 0 6 -14 50.09 4.10 0 6 14 51.79 5.30 0 6 -14 52.19 3.50 0 6 14 48.50 4.70 -1 -6 -14 2.40 1.20 1 -6 14 5.30 3.00 1 -6 14 5.90 2.10 1 -6 14 5.30 1.00 -1 -6 -14 7.20 1.40 1 -6 14 5.90 2.00 1 -6 14 4.60 1.70 -1 6 -14 5.00 1.70 1 6 14 7.80 2.60 1 6 14 5.10 2.40 -1 6 -14 4.00 1.40 1 6 14 8.30 2.70 1 6 14 10.30 2.50 -1 6 -14 4.50 1.80 2 -6 14 86.89 5.10 2 -6 14 87.49 3.70 -2 -6 -14 86.89 4.40 2 -6 14 76.29 5.70 -2 -6 -14 88.79 4.50 2 -6 14 80.09 5.00 -2 6 -14 84.19 3.90 2 6 14 89.59 6.40 2 6 14 87.29 6.40 2 6 14 88.39 5.70 -2 6 -14 79.99 5.40 -2 6 -14 82.69 4.60 2 6 14 92.79 6.40 3 -6 14 23.30 3.00 -3 -6 -14 14.20 1.90 3 -6 14 12.50 2.60 3 -6 14 11.10 2.10 3 6 14 13.80 2.80 3 6 14 12.40 2.70 3 6 14 14.30 2.70 -3 6 -14 13.40 1.90 -3 6 -14 13.80 1.60 3 6 14 12.80 3.00 -3 6 -14 14.50 2.50 4 -6 14 102.79 5.40 4 -6 14 101.69 5.50 4 -6 14 82.59 6.10 -4 -6 -14 103.99 4.90 -4 6 -14 108.19 5.20 4 6 14 102.79 6.70 4 6 14 103.29 6.60 4 6 14 97.79 7.00 4 6 14 100.19 6.80 5 -6 14 39.10 3.20 -5 -6 -14 39.50 2.70 5 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8.20 -9 -7 14 154.88 6.70 9 -7 -14 159.18 7.00 -9 -7 14 158.58 6.20 9 -7 -14 146.69 7.70 -9 7 14 166.88 7.80 9 7 -14 162.78 6.90 -9 7 14 149.29 9.90 9 7 -14 144.09 5.70 -9 7 14 147.99 7.50 -9 7 14 158.18 7.40 -9 7 14 155.58 7.50 -8 -7 14 62.19 3.20 8 -7 -14 66.09 5.20 8 -7 -14 60.09 3.70 -8 -7 14 55.29 5.00 8 -7 -14 60.09 5.10 -8 7 14 56.29 4.40 -8 7 14 67.29 6.00 8 7 -14 60.59 3.10 -8 7 14 53.09 5.00 -8 7 14 66.99 3.90 -7 -7 14 237.38 8.80 7 -7 -14 257.77 11.50 -7 -7 14 228.98 8.90 -7 -7 14 231.48 9.70 7 -7 -14 268.07 10.90 7 -7 -14 237.88 9.50 7 -7 -14 234.58 11.10 -7 7 14 192.28 12.30 -7 7 14 223.88 10.30 7 7 -14 231.38 9.90 -7 7 14 237.48 9.70 -7 7 14 234.08 11.60 6 -7 -14 65.29 4.10 6 -7 -14 62.49 5.20 -6 -7 14 62.19 4.20 6 -7 -14 61.59 3.90 -6 -7 14 56.29 5.20 6 -7 -14 58.89 4.30 -6 -7 14 61.09 3.20 -6 7 14 62.09 4.30 6 7 -14 60.69 4.00 -6 7 14 49.80 5.30 6 7 -14 58.99 3.40 -6 7 14 52.69 4.40 -6 7 14 57.79 4.70 -5 -7 14 94.39 4.30 5 -7 -14 97.69 5.00 5 -7 -14 93.09 6.40 5 -7 -14 95.49 5.10 5 -7 -14 94.29 5.40 -5 -7 14 97.19 5.50 -5 -7 14 91.99 5.60 5 7 -14 107.99 5.50 -5 7 14 84.59 6.70 -5 7 14 95.29 5.30 -5 7 14 93.19 6.90 5 7 -14 95.09 4.50 -5 7 14 89.69 6.00 -5 7 14 94.69 5.50 -4 -7 14 75.59 4.50 -4 -7 14 78.09 5.00 -4 -7 14 76.29 3.70 4 -7 -14 75.29 4.50 -4 -7 14 67.39 7.20 4 -7 -14 76.39 4.40 -4 7 14 76.19 6.30 4 7 -14 75.89 4.80 -4 7 14 71.39 4.70 -4 7 14 73.69 5.20 4 7 -14 76.19 4.00 -4 7 14 78.49 4.50 -4 7 14 72.59 5.40 -3 -7 14 229.48 8.70 -3 -7 14 233.88 9.60 3 -7 -14 224.78 9.40 3 -7 -14 241.08 9.50 -3 -7 14 226.98 13.30 -3 -7 14 232.68 10.10 -3 7 14 221.48 9.20 -3 7 14 244.28 12.10 -3 7 14 230.38 10.50 3 7 -14 231.58 9.00 3 7 -14 235.98 10.00 -3 7 14 229.98 10.70 -2 -7 14 112.59 4.70 -2 -7 14 111.49 5.80 2 -7 -14 101.19 5.30 2 -7 -14 110.69 5.40 -2 -7 14 105.89 8.40 -2 -7 14 104.99 6.00 -2 7 14 99.49 6.50 -2 7 14 113.09 6.80 -2 7 14 104.29 6.00 2 7 -14 105.29 5.10 2 7 -14 110.59 6.20 -2 7 14 114.89 7.60 -1 -7 14 270.27 11.30 1 -7 -14 280.27 10.70 -1 -7 14 250.57 13.90 -1 -7 14 273.37 9.80 -1 -7 14 264.07 10.90 -1 7 14 280.47 13.20 1 7 -14 266.27 11.40 -1 7 14 273.37 12.10 -1 7 14 271.97 12.00 1 7 -14 279.47 10.40 0 -7 14 67.19 4.80 0 -7 -14 67.49 3.80 0 -7 14 72.09 3.30 0 -7 -14 67.89 4.00 0 -7 14 72.59 4.50 0 -7 14 60.99 6.50 0 -7 14 61.89 4.60 0 7 14 66.59 5.40 0 7 -14 70.69 4.80 0 7 -14 65.89 3.90 0 7 14 68.89 5.10 0 7 14 63.49 5.80 1 -7 14 30.90 3.40 -1 -7 -14 27.20 2.50 1 -7 14 24.50 3.30 -1 -7 -14 26.60 2.40 1 -7 14 27.80 1.90 1 -7 14 25.60 3.40 1 7 14 29.40 4.70 -1 7 -14 24.20 2.60 1 7 14 25.90 3.90 -2 -7 -14 59.99 3.40 2 -7 14 54.59 5.00 2 -7 14 50.29 4.00 2 -7 14 53.89 2.70 2 -7 14 49.10 4.30 2 7 14 56.59 4.50 2 7 14 45.40 4.80 2 7 14 55.89 5.30 -2 7 -14 58.39 4.40 -2 7 -14 50.29 4.30 -3 -7 -14 2.80 1.20 3 -7 14 3.20 1.90 3 -7 14 2.90 1.50 -3 7 -14 2.90 1.30 3 7 14 5.20 1.90 -3 7 -14 0.40 1.50 3 7 14 1.40 2.00 3 7 14 0.00 1.90 4 -7 14 57.39 3.80 -4 -7 -14 51.99 3.10 4 -7 14 54.39 3.70 4 -7 14 44.00 4.30 4 7 14 52.59 4.10 -4 7 -14 54.29 4.10 4 7 14 45.30 4.20 -4 7 -14 51.69 3.30 4 7 14 48.30 4.70 5 -7 14 25.30 2.60 -5 -7 -14 22.10 1.90 5 -7 14 19.60 2.80 5 -7 14 18.80 2.50 5 7 14 19.20 3.00 5 7 14 20.50 2.60 -5 7 -14 24.20 2.80 -5 7 -14 25.90 2.40 -6 -7 -14 9.30 1.20 6 -7 14 8.70 1.60 6 -7 14 6.60 2.00 6 -7 14 9.90 2.30 -6 7 -14 7.60 1.40 6 7 14 5.70 2.00 6 7 14 6.10 1.40 7 -7 14 6.90 2.80 7 -7 14 8.80 1.40 -7 -7 -14 8.90 1.10 7 -7 14 7.50 1.30 -7 7 -14 7.90 1.30 -7 7 -14 7.80 1.50 8 -7 14 5.50 1.10 8 -7 14 2.90 1.60 -8 7 -14 6.00 1.60 8 7 14 3.70 1.70 -8 7 -14 5.60 1.10 9 7 14 20.20 3.00 -9 7 -14 14.20 1.90 13 -8 -14 17.80 2.50 -13 -8 14 21.10 1.60 13 -8 -14 20.60 1.70 13 -8 -14 17.90 2.20 -13 8 14 19.40 2.30 -13 8 14 22.30 2.00 12 -8 -14 37.40 2.50 12 -8 -14 39.70 3.30 12 -8 -14 39.80 3.50 12 -8 -14 40.00 2.90 -12 -8 14 37.50 2.20 -12 8 14 38.20 2.90 -12 8 14 37.30 2.70 11 -8 -14 18.20 3.20 11 -8 -14 25.70 2.60 11 -8 -14 24.30 2.70 11 -8 -14 26.70 3.30 -11 8 14 26.80 2.60 -11 8 14 21.10 2.70 10 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7.00 1 2 -22 156.08 6.20 -1 2 22 180.38 10.10 -1 2 22 166.98 7.20 1 2 -22 157.78 6.60 -1 2 22 163.18 7.10 0 -2 22 190.08 7.70 0 -2 22 178.78 7.90 0 -2 -22 187.68 7.30 0 -2 22 184.28 8.20 0 2 22 191.68 8.50 0 2 -22 187.88 8.50 0 2 -22 199.18 7.10 0 2 22 190.78 7.90 0 2 22 189.88 7.90 1 -2 22 124.09 5.30 -1 -2 -22 124.49 4.90 1 -2 22 114.69 5.00 1 -2 22 117.49 5.70 1 2 22 118.29 5.50 -1 2 -22 117.29 4.70 -1 2 -22 115.39 5.00 1 2 22 117.79 5.50 1 2 22 110.59 5.80 -10 -3 22 72.59 4.40 10 -3 -22 63.39 3.40 10 -3 -22 67.49 3.10 -10 -3 22 70.39 3.40 10 -3 -22 70.29 3.90 -10 3 22 72.09 3.40 10 3 -22 71.69 3.50 -9 -3 22 34.90 2.40 -9 -3 22 38.90 2.90 9 -3 -22 32.10 2.50 9 -3 -22 34.50 2.50 9 -3 -22 36.40 2.20 9 3 -22 32.30 2.60 -9 3 22 36.40 2.30 -9 3 22 29.60 3.70 -8 -3 22 3.10 1.20 8 -3 -22 5.20 1.10 -8 -3 22 3.00 1.60 -8 -3 22 5.90 1.20 8 -3 -22 5.30 1.10 8 -3 -22 2.50 1.50 -8 3 22 4.40 1.50 -8 3 22 5.60 1.30 -8 3 22 4.60 1.20 8 3 -22 4.20 1.20 -7 -3 22 9.40 1.80 -7 -3 22 12.30 1.50 -7 -3 22 12.70 1.80 7 -3 -22 10.60 1.40 7 -3 -22 16.10 1.80 -7 -3 22 13.60 1.50 -7 3 22 13.00 1.60 7 3 -22 10.40 1.50 -7 3 22 14.00 2.10 6 -3 -22 3.00 1.00 -6 -3 22 2.60 1.00 -6 -3 22 2.30 1.40 -6 -3 22 0.40 1.10 6 -3 -22 1.70 1.10 -6 -3 22 1.60 1.10 -6 3 22 2.60 1.30 -6 3 22 1.30 1.50 6 3 -22 4.80 1.20 5 -3 -22 36.60 2.50 -5 -3 22 37.40 2.60 -5 -3 22 38.00 2.30 -5 -3 22 43.10 3.60 5 -3 -22 38.00 2.60 5 3 -22 35.70 2.80 -5 3 22 35.90 4.60 -5 3 22 33.50 2.80 -4 -3 22 2.10 1.10 -4 -3 22 3.00 0.90 4 -3 -22 1.50 1.10 4 -3 -22 2.20 1.00 -4 -3 22 4.00 1.80 -4 3 22 3.50 1.40 4 3 -22 1.80 1.10 -4 3 22 2.10 2.00 -3 -3 22 6.90 2.10 -3 -3 22 8.00 1.50 3 -3 -22 9.00 1.40 -3 3 22 11.70 1.80 -3 3 22 10.40 2.70 3 3 -22 11.90 1.60 -2 -3 22 5.30 1.60 2 -3 -22 6.30 1.20 -2 -3 22 5.20 1.30 2 3 -22 6.70 1.00 -2 3 22 4.00 1.60 -2 3 22 5.90 1.50 2 3 -22 5.40 1.20 -1 -3 22 9.70 1.70 1 -3 -22 13.90 1.60 -1 -3 22 16.20 2.00 -1 3 22 15.90 2.00 -1 3 22 13.80 1.90 -1 3 22 11.60 2.10 1 3 -22 16.80 1.90 1 3 -22 13.80 1.30 0 -3 22 1.70 1.10 0 -3 -22 3.60 1.00 0 -3 22 2.60 1.30 0 3 -22 2.50 1.10 0 3 22 0.40 1.20 0 3 22 1.50 1.20 0 3 22 3.60 1.40 0 3 -22 1.70 0.70 8 -4 -22 113.89 5.40 7 -4 -22 8.50 1.20 7 -4 -22 7.00 1.50 -7 -4 22 7.60 1.20 -7 -4 22 6.60 1.30 -7 -4 22 8.60 1.80 -7 4 22 7.50 1.60 -7 4 22 7.60 1.20 7 4 -22 5.20 1.20 -6 -4 22 38.40 2.40 6 -4 -22 34.50 2.30 -6 -4 22 35.20 2.70 -6 -4 22 35.70 2.20 6 -4 -22 36.40 2.40 6 4 -22 35.30 2.50 -6 4 22 33.10 2.90 -6 4 22 32.70 3.10 5 -4 -22 23.00 1.90 -5 -4 22 20.60 2.40 -5 -4 22 18.00 1.80 5 -4 -22 18.10 1.80 -5 -4 22 20.20 1.70 -5 4 22 17.60 2.40 5 4 -22 14.80 1.80 -5 4 22 19.40 2.20 4 -4 -22 33.10 2.30 4 -4 -22 30.30 2.20 -4 -4 22 31.50 2.80 -4 -4 22 32.70 2.80 -4 -4 22 25.30 2.20 -4 4 22 31.10 3.10 4 4 -22 33.90 2.30 -4 4 22 30.70 2.50 -3 -4 22 12.20 1.50 3 -4 -22 14.80 1.60 3 -4 -22 10.90 1.40 -3 -4 22 12.90 1.90 -3 -4 22 14.00 1.40 -3 4 22 10.60 1.60 -3 4 22 11.90 2.10 3 4 -22 12.90 1.50 2 -4 -22 38.50 2.30 -2 -4 22 43.00 3.20 -2 -4 22 34.90 2.50 -2 -4 22 36.80 2.30 -2 4 22 40.40 2.90 -2 4 22 33.00 3.10 2 4 -22 35.40 2.40 -9 0 23 1.70 0.90 9 0 -23 1.60 1.10 8 0 -23 10.90 1.50 -8 0 23 8.90 2.20 7 0 -23 3.60 1.00 7 0 -23 4.80 1.30 -7 0 23 5.70 1.50 -7 0 23 6.00 1.10 6 0 -23 249.97 9.00 -6 0 23 255.67 9.50 6 0 -23 244.68 9.70 -6 0 23 247.58 10.40 -5 0 23 60.99 4.10 5 0 -23 52.39 4.00 -5 0 23 56.99 3.40 5 0 -23 61.89 3.00 4 0 -23 246.28 9.40 -4 0 23 248.68 9.60 -4 0 23 256.57 10.60 4 0 -23 252.47 9.10 3 0 -23 61.39 3.30 -3 0 23 59.29 4.10 3 0 -23 60.69 3.10 -3 0 23 57.29 3.50 -2 0 23 106.39 4.90 2 0 -23 102.29 4.30 2 0 -23 84.99 5.60 -2 0 23 100.49 5.40 1 0 -23 61.59 3.00 -1 0 23 65.59 3.70 -1 0 23 62.39 4.10 -9 -1 23 3.30 0.90 -9 -1 23 2.40 0.90 -9 1 23 6.80 1.60 9 1 -23 3.00 1.10 8 -1 -23 7.80 1.20 -8 -1 23 8.10 2.10 8 -1 -23 8.60 1.50 -8 -1 23 6.40 2.10 -8 -1 23 9.40 1.20 8 1 -23 11.30 1.50 -8 1 23 8.50 1.60 -7 -1 23 117.19 4.80 7 -1 -23 117.89 4.70 7 -1 -23 121.99 5.30 -7 -1 23 119.09 5.90 -7 1 23 113.99 5.90 -7 1 23 116.59 5.30 7 1 -23 114.39 5.20 -6 -1 23 11.30 2.30 6 -1 -23 7.90 1.20 6 -1 -23 7.40 1.30 -6 -1 23 7.70 1.70 6 1 -23 8.10 1.10 -6 1 23 8.40 1.50 6 1 -23 9.00 1.40 -6 1 23 4.50 1.60 -5 -1 23 116.59 5.10 5 -1 -23 113.59 4.80 -5 -1 23 116.19 5.80 5 -1 -23 118.99 5.10 -5 1 23 111.09 6.00 -5 1 23 116.09 5.20 5 1 -23 116.09 5.20 5 1 -23 107.19 4.80 4 -1 -23 1.40 0.90 4 -1 -23 3.30 1.80 -4 -1 23 0.30 1.30 -4 -1 23 2.20 1.10 4 1 -23 1.00 1.10 4 1 -23 0.80 1.40 -4 1 23 3.60 1.50 -4 1 23 1.70 1.10 -3 -1 23 38.50 2.70 -3 -1 23 35.20 3.20 3 -1 -23 36.50 2.30 3 1 -23 38.70 2.60 3 1 -23 37.90 2.20 -3 1 23 36.90 2.80 -3 1 23 32.30 3.30 2 -1 -23 18.50 1.80 -2 -1 23 13.30 1.90 -2 -1 23 20.20 2.20 2 1 -23 19.20 1.60 -2 1 23 17.60 2.20 -2 1 23 19.70 2.60 2 1 -23 15.60 1.90 -1 -1 23 87.39 4.70 1 -1 -23 90.39 3.90 -1 -1 23 90.19 4.40 1 1 -23 90.79 4.10 1 1 -23 83.69 4.60 -1 1 23 82.39 4.90 -1 1 23 92.09 4.60 8 -2 -23 60.49 4.10 8 2 -23 72.69 3.60 -7 -2 23 3.70 0.90 7 -2 -23 4.40 1.50 -7 -2 23 7.70 1.80 7 -2 -23 3.40 0.90 7 2 -23 3.80 1.20 -7 2 23 1.20 1.40 -6 -2 23 35.80 2.20 -6 -2 23 36.70 2.50 -6 -2 23 37.90 3.00 6 -2 -23 32.30 2.30 -6 2 23 33.30 3.10 6 2 -23 35.10 2.50 5 -2 -23 29.70 2.20 -5 -2 23 28.70 2.90 5 2 -23 30.90 2.30 -5 2 23 29.90 2.50 -5 2 23 34.00 3.10 -4 -2 23 19.10 2.30 4 -2 -23 21.40 1.90 -4 -2 23 20.10 2.00 4 -2 -23 18.30 1.80 -4 2 23 23.30 2.30 -4 2 23 22.80 2.80 4 2 -23 22.50 2.20 -3 -2 23 8.10 1.70 3 -2 -23 9.30 1.20 3 -2 -23 8.70 1.30 -3 -2 23 7.30 1.30 -3 2 23 5.10 1.50 -3 2 23 8.50 1.50 3 2 -23 5.50 1.40 3 2 -23 8.00 1.30 2 -2 -23 64.09 3.80 2 2 -23 72.29 3.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 34876 _olex2_submission_special_instructions 'No special instructions were received'