####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_ca121021_1_1 _database_code_depnum_ccdc_archive 'CCDC 2149823' loop_ _audit_author_name _audit_author_address 'Trapp Nils' ;ETH Zurich Switzerland ; _audit_update_record ; 2022-02-03 deposited with the CCDC. 2022-03-22 downloaded from the CCDC. ; _audit_creation_date 2021-10-13 _audit_creation_method ; Olex2 1.5 (compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6405) ; _shelx_SHELXL_version_number 2018/3 loop_ _audit_author_email david.fischer@org.chem.ethz.ch _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_acknowledgements ; X-Ray services provided by SMoCC - The Small Molecule Crystallography Center of ETH Zurich. ; _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C11 H13 N O3 S' _chemical_formula_sum 'C11 H13 N O3 S' _chemical_formula_weight 239.28 _chemical_melting_point ? _chemical_oxdiff_formula 'C11 H15 N O3 S' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.5584(2) _cell_length_b 11.0650(3) _cell_length_c 14.3491(4) _cell_angle_alpha 83.402(2) _cell_angle_beta 81.007(2) _cell_angle_gamma 75.074(2) _cell_volume 1141.82(6) _cell_formula_units_Z 4 _cell_measurement_reflns_used 16713 _cell_measurement_temperature 100.0(1) _cell_measurement_theta_max 79.0400 _cell_measurement_theta_min 3.1160 _shelx_estimated_absorpt_T_max 0.790 _shelx_estimated_absorpt_T_min 0.679 _exptl_absorpt_coefficient_mu 2.471 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.675 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.101a (Rigaku Oxford Diffraction, 2021) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.392 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 504 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 1 0 9 0.0461 4 3 -2 0.0602 -2 -1 -9 0.0405 2 1 -8 0.0630 -5 -3 -3 0.0670 3 -5 0 0.0631 4 6 1 0.0720 -4 3 -1 0.0567 -3 -6 -1 0.0791 -1 6 0 0.0856 1 -5 -5 0.0654 3 -3 -3 0.0674 -3 -6 -4 0.0703 3 -2 -5 0.0648 -1 -3 -9 0.0404 0 -2 -9 0.0489 3 4 -4 0.0659 4 4 -1 0.0574 -4 -4 3 0.0761 -4 1 -5 0.0430 4 5 -1 0.0576 -4 2 3 0.0613 1 -4 7 0.0719 -4 -5 -5 0.0646 _exptl_crystal_size_max 0.17 _exptl_crystal_size_mid 0.136 _exptl_crystal_size_min 0.099 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 0.5962 0.4521 9.2991 -0.9957 0.0254 0.0889 4.4571 3.1030 -1.8707 0.3295 -0.0068 0.9441 -1.9384 -1.3876 -9.0238 0.9279 -0.0242 -0.3721 2.1140 1.4460 -7.5373 0.8804 -0.0216 0.4738 -4.7567 -3.3292 -2.5351 0.1418 -0.0052 -0.9899 2.5567 -4.9667 0.0563 -0.0216 -0.9481 0.3203 3.7294 5.8615 1.2442 0.0120 0.4587 0.8835 -3.9654 2.5888 -0.5207 0.0143 0.7519 -0.6593 -3.2999 -6.3754 -1.1511 -0.0206 -0.5728 -0.8198 -1.1372 6.3244 0.3335 0.0239 0.9999 -0.0117 1.0343 -5.4471 -4.8942 0.4823 -0.8768 0.0390 3.4005 -2.7258 -3.3857 0.3986 -0.7242 0.5646 -2.8958 -6.2785 -4.2139 0.3221 -0.6057 -0.7284 3.1781 -1.7637 -5.1828 0.6026 -0.5713 0.5610 -1.2968 -3.0581 -8.7969 0.8938 -0.3211 -0.3062 0.4680 -1.8981 -8.7850 0.9413 -0.3318 0.0624 3.4650 4.1179 -3.9989 0.5555 0.2284 0.7990 4.4345 3.9077 -1.1135 0.2570 0.1100 0.9627 -3.8990 -4.1077 2.9351 -0.4478 -0.1867 -0.8759 -3.9625 1.0756 -5.1002 0.4936 0.5291 -0.6889 4.1837 4.7724 -0.8224 0.2317 0.2566 0.9422 -3.7859 1.6839 3.3923 -0.4203 0.6159 -0.6705 1.0884 -3.9789 6.6605 -0.7563 -0.6505 0.0497 -3.6140 -4.9677 -5.4008 0.4546 -0.3538 -0.8164 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0394 _diffrn_reflns_av_unetI/netI 0.0272 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.952 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 24269 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.952 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 80.226 _diffrn_reflns_theta_min 3.128 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.0(1) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 5.8140 _diffrn_detector_type 'Pilatus 300K' _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.952 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 28.00 53.00 0.50 0.10 -- 50.00 75.00 7.50 50 2 \w 29.00 63.00 0.50 0.10 -- 47.25 64.00 22.10 68 3 \w 80.00 107.00 0.50 0.10 -- 50.00 75.00 7.50 54 4 \w 32.00 68.00 0.50 0.10 -- 47.25 57.00 -60.00 72 5 \w 28.00 55.00 0.50 0.10 -- 50.00 77.00-149.50 54 6 \w 34.00 62.00 0.50 0.10 -- 47.25 57.00-150.00 56 7 \w 25.00 53.00 0.50 0.10 -- 47.25 77.00 -90.00 56 8 \w 38.00 84.00 0.50 0.10 -- 47.25 38.00 30.00 92 9 \w 32.00 92.00 0.50 0.10 -- 47.25 57.00 120.00 120 10 \w 30.00 57.00 0.50 0.10 -- 54.00 77.00 136.93 54 11 \w 51.00 90.00 0.50 0.10 -- 74.00 77.00 114.96 78 12 \w 51.00 78.00 0.50 0.10 -- 74.00 77.00 98.95 54 13 \w 47.00 74.00 0.50 0.10 -- 70.00 77.00 69.74 54 14 \w 35.00 85.00 0.50 0.10 -- 58.00 77.00 55.56 100 15 \w 87.00 167.00 0.50 0.30 -- 110.00 77.00 0.00 160 16 \w 136.00 173.00 0.50 0.30 -- 110.00 77.00 -60.00 74 17 \w 87.00 123.00 0.50 0.30 -- 110.00 77.00 -60.00 72 18 \w 132.00 159.00 0.50 0.30 -- 110.00 77.00-180.00 54 19 \w 86.00 126.00 0.50 0.30 -- 110.00 77.00-180.00 80 20 \w 42.00 69.00 0.50 0.10 -- 66.00 77.00 -73.06 54 21 \w 141.00 176.00 0.50 0.30 -- 110.00 77.00 30.00 70 22 \w 134.00 171.00 0.50 0.30 -- 110.00 77.00 90.00 74 23 \w 134.00 174.00 0.50 0.30 -- 110.00 77.00 150.00 80 24 \w 86.00 112.00 0.50 0.30 -- 110.00 77.00 150.00 52 25 \w 87.00 127.00 0.50 0.30 -- 110.00 77.00 90.00 80 26 \w 87.00 129.00 0.50 0.30 -- 110.00 77.00 30.00 84 27 \w 86.00 124.00 0.50 0.30 -- 110.00 77.00 120.00 76 28 \w 87.00 114.00 0.50 0.30 -- 110.00 77.00 -30.00 54 29 \w 130.00 168.00 0.50 0.30 -- 110.00 77.00 -30.00 76 30 \w 132.00 176.00 0.50 0.30 -- 110.00 77.00 -90.00 88 31 \w 122.00 176.00 0.50 0.30 -- 110.00 77.00-150.00 108 32 \w 88.00 113.00 0.50 0.30 -- 110.00 77.00-150.00 50 33 \w 88.00 161.00 0.50 0.30 -- 110.00 77.00-120.00 146 34 \w 87.00 127.00 0.50 0.30 -- 110.00 77.00 -90.00 80 35 \w 48.00 75.00 0.50 0.10 -- 70.00 76.00-125.94 54 36 \w 130.00 162.00 0.50 0.30 -- 110.00 77.00 120.00 64 37 \w 88.00 115.00 0.50 0.10 -- 58.00 76.00 154.41 54 38 \w 36.00 61.00 0.50 0.10 -- 58.00 76.00 154.41 50 39 \w 40.00 65.00 0.50 0.10 -- 62.00 76.00 94.28 50 40 \w 36.00 72.00 0.50 0.10 -- 58.00 74.00 27.11 72 41 \w 44.00 75.00 0.50 0.10 -- 66.00 73.00 65.24 62 42 \w 52.00 78.00 0.50 0.10 -- 74.00 73.00 -35.59 52 43 \w 49.00 77.00 0.50 0.10 -- 70.00 75.00 -61.07 56 44 \w 83.00 110.00 0.50 0.10 -- 70.00 75.00 -61.07 54 45 \w 60.00 119.00 0.50 0.30 -- 82.00 76.00-102.63 118 46 \w 55.00 88.00 0.50 0.10 -- 74.00 66.00 8.60 66 47 \w 57.00 87.00 0.50 0.10 -- 78.00 72.00 141.88 60 48 \w 76.00 128.00 0.50 0.30 -- 94.00 63.00 79.85 104 49 \w 130.00 160.00 0.50 0.30 -- 94.00 63.00 79.85 60 50 \w 144.00 176.00 0.50 0.30 -- 110.00 57.00 60.00 64 51 \w 97.00 140.00 0.50 0.30 -- 110.00 57.00 60.00 86 52 \w 96.00 123.00 0.50 0.30 -- 110.00 57.00 30.00 54 53 \w 101.00 128.00 0.50 0.30 -- 110.00 38.00 0.00 54 54 \w 99.00 135.00 0.50 0.30 -- 110.00 38.00 -60.00 72 55 \w 101.00 137.00 0.50 0.30 -- 110.00 38.00 -30.00 72 56 \w 64.00 100.00 0.50 0.10 -- 78.00 53.00 -28.42 72 57 \w 118.00 150.00 0.50 0.10 -- 78.00 53.00 -28.42 64 58 \w 103.00 133.00 0.50 0.30 -- 110.00 38.00-120.00 60 59 \w 101.00 137.00 0.50 0.30 -- 110.00 38.00-180.00 72 60 \w 100.00 138.00 0.50 0.30 -- 110.00 38.00-150.00 76 61 \w 99.00 126.00 0.50 0.30 -- 110.00 38.00 30.00 54 62 \w 94.00 140.00 0.50 0.30 -- 110.00 57.00 150.00 92 63 \w 58.00 83.00 0.50 0.30 -- 110.00 -99.00 -30.00 50 64 \w 67.00 113.00 0.50 0.30 -- 110.00-125.00 -60.00 92 65 \w 43.00 104.00 0.50 0.30 -- 110.00 -99.00 0.00 122 66 \w 41.00 102.00 0.50 0.30 -- 110.00 -99.00 60.00 122 67 \w 67.00 105.00 0.50 0.30 -- 110.00-125.00-180.00 76 68 \w 55.00 86.00 0.50 0.30 -- 110.00 -99.00-150.00 62 69 \w 65.00 92.00 0.50 0.30 -- 110.00 -99.00 -90.00 54 70 \w -24.00 4.00 0.50 0.10 -- 47.25 -19.00 120.00 56 71 \w 42.00 67.00 0.50 0.30 -- 110.00 -57.00 30.00 50 72 \w 38.00 63.00 0.50 0.30 -- 110.00 -57.00 90.00 50 73 \w 46.00 134.00 0.50 0.30 -- 110.00 -77.00 90.00 176 74 \w 40.00 68.00 0.50 0.30 -- 110.00 -57.00 -30.00 56 75 \w 38.00 68.00 0.50 0.30 -- 110.00 -57.00 -90.00 60 76 \w 38.00 67.00 0.50 0.30 -- 110.00 -57.00-150.00 58 77 \w 80.00 116.00 0.50 0.10 -- 47.25 178.00-150.00 72 78 \w -89.00 -62.00 0.50 0.10 -- -47.25 130.00-145.00 54 79 \w -86.00 -14.00 0.50 0.30 -- -70.00 125.00-180.00 144 80 \w -51.00 -20.00 0.50 0.10 -- -47.25 130.00-145.00 62 81 \w -35.00 4.00 0.50 0.30 -- -70.00 38.00 -30.00 78 82 \w -111.00 -34.00 0.50 0.10 -- -47.25 -17.00-111.25 154 83 \w -77.00 -50.00 0.50 0.10 -- -47.25 -77.00 -30.00 54 84 \w -49.00 -23.00 0.50 0.10 -- -47.25 -77.00 -30.00 52 85 \w -58.00 -31.00 0.50 0.10 -- -47.25 -57.00-150.00 54 86 \w -121.00 -35.00 0.50 0.10 -- -47.25 -24.00-161.98 172 87 \w -80.00 -46.00 0.50 0.30 -- -70.00 -77.00-120.00 68 88 \w -73.00 -46.00 0.50 0.30 -- -70.00 -77.00 -90.00 54 89 \w -74.00 -47.00 0.50 0.30 -- -70.00 -74.00-146.95 54 90 \w -79.00 -50.00 0.50 0.30 -- -70.00 -73.00-171.59 58 91 \w -135.00 -99.00 0.50 0.30 -- -70.00 -73.00-171.59 72 92 \w -74.00 -47.00 0.50 0.30 -- -70.00 -77.00 0.00 54 93 \w -86.00 -51.00 0.50 0.30 -- -70.00 -66.00 140.48 70 94 \w -141.00 -75.00 0.50 0.30 -- -70.00-125.00 -90.00 132 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 300K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0191650000 _diffrn_orient_matrix_UB_12 0.0129753000 _diffrn_orient_matrix_UB_13 -0.1089362000 _diffrn_orient_matrix_UB_21 -0.0982882000 _diffrn_orient_matrix_UB_22 0.1403194000 _diffrn_orient_matrix_UB_23 0.0022144000 _diffrn_orient_matrix_UB_31 0.1877686000 _diffrn_orient_matrix_UB_32 0.0321237000 _diffrn_orient_matrix_UB_33 -0.0040361000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4347 _reflns_number_total 4756 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.41.101a (Rigaku OD, 2021)' _computing_data_collection 'CrysAlisPro 1.171.41.101a (Rigaku OD, 2021)' _computing_data_reduction 'CrysAlisPro 1.171.41.101a (Rigaku OD, 2021)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _refine_diff_density_max 0.513 _refine_diff_density_min -0.656 _refine_diff_density_rms 0.063 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.098 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 368 _refine_ls_number_reflns 4756 _refine_ls_number_restraints 148 _refine_ls_R_factor_all 0.0636 _refine_ls_R_factor_gt 0.0590 _refine_ls_restrained_S_all 1.084 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0336P)^2^+2.2002P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1346 _refine_ls_wR_factor_ref 0.1368 _refine_special_details 'Disorder in both moieties.' _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances O1A-C1A \\sim O1B-C1A with sigma of 0.02 C2B-C1A \\sim C2A-C1A with sigma of 0.02 C4B-C3B \\sim C4A-C3A with sigma of 0.02 N1A-C3B \\sim N1A-C3A with sigma of 0.02 C3A-C2A \\sim C3B-C2B with sigma of 0.02 C2C-C1C \\sim C2D-C1C with sigma of 0.02 C3D-C2D \\sim C3C-C2C with sigma of 0.02 O1D-C1C \\sim O1C-C1C with sigma of 0.02 N1C-C3C \\sim N1C-C3D with sigma of 0.02 C4D-C3D \\sim C4C-C3C with sigma of 0.02 3. Rigid body (RIGU) restrains O1B, N1A, C1A, C2B, C3B, C4B, C2A, C3A, C4A, O1A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 O1D, N1C, C1C, C2D, C3D, C4D, C2C, C3C, C4C, O1C with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 4. Others Sof(O1B)=Sof(C2B)=Sof(H2BA)=Sof(H2BB)=Sof(C3B)=Sof(H3B)=Sof(C4B)=Sof(H4BA)= Sof(H4BB)=Sof(H4BC)=Sof(O1D)=Sof(C2D)=Sof(H2DA)=Sof(H2DB)=Sof(C3D)=Sof(H3D)= Sof(C4D)=Sof(H4DA)=Sof(H4DB)=Sof(H4DC)=1-FVAR(1) Sof(C2A)=Sof(H2AA)=Sof(H2AB)=Sof(C3A)=Sof(H3A)=Sof(C4A)=Sof(H4AA)=Sof(H4AB)= Sof(H4AC)=Sof(O1A)=Sof(C2C)=Sof(H2CA)=Sof(H2CB)=Sof(C3C)=Sof(H3C)=Sof(C4C)= Sof(H4CA)=Sof(H4CB)=Sof(H4CC)=Sof(O1C)=FVAR(1) 5.a Ternary CH refined with riding coordinates: C3B(H3B), C3D(H3D), C3A(H3A), C3C(H3C) 5.b Secondary CH2 refined with riding coordinates: C2B(H2BA,H2BB), C2D(H2DA,H2DB), C2A(H2AA,H2AB), C2C(H2CA,H2CB) 5.c Aromatic/amide H refined with riding coordinates: C6A(H6A), C7A(H7A), C9A(H9A), C10A(H10A), C6C(H6C), C7C(H7C), C9C(H9C), C10C(H10C) 5.d Idealised Me refined as rotating group: C4B(H4BA,H4BB,H4BC), C11A(H11A,H11B,H11C), C4D(H4DA,H4DB,H4DC), C11C(H11D, H11E,H11F), C4A(H4AA,H4AB,H4AC), C4C(H4CA,H4CB,H4CC) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1A S 0.83786(9) -0.07277(6) 0.19013(5) 0.02785(17) Uani 1 1 d . . . . . O1B O 1.2960(17) -0.1871(8) 0.1656(8) 0.048(2) Uani 0.401(6) 1 d D . P A 2 O2A O 0.8728(3) -0.19877(18) 0.16522(15) 0.0351(5) Uani 1 1 d . . . . . O3A O 0.6845(3) 0.02196(19) 0.15965(15) 0.0362(5) Uani 1 1 d . . . . . N1A N 1.0232(3) -0.0223(2) 0.14394(17) 0.0298(5) Uani 1 1 d D . . . . C1A C 1.2122(4) -0.0835(3) 0.1304(3) 0.0408(7) Uani 1 1 d D . . . . C2B C 1.2697(14) 0.0308(11) 0.0818(8) 0.036(3) Uani 0.401(6) 1 d D . P A 2 H2BA H 1.331425 0.020365 0.016041 0.043 Uiso 0.401(6) 1 calc R U P A 2 H2BB H 1.340410 0.067213 0.118859 0.043 Uiso 0.401(6) 1 calc R U P A 2 C3B C 1.0587(9) 0.0969(6) 0.0896(6) 0.0315(17) Uani 0.401(6) 1 d D . P A 2 H3B H 1.012771 0.110962 0.026564 0.038 Uiso 0.401(6) 1 calc R U P A 2 C4B C 0.9898(11) 0.2090(7) 0.1441(7) 0.039(2) Uani 0.401(6) 1 d D . P A 2 H4BA H 0.854608 0.233961 0.150044 0.059 Uiso 0.401(6) 1 calc R U P A 2 H4BB H 1.040226 0.277919 0.111110 0.059 Uiso 0.401(6) 1 calc R U P A 2 H4BC H 1.028880 0.189562 0.207209 0.059 Uiso 0.401(6) 1 calc R U P A 2 C5A C 0.8272(4) -0.0728(2) 0.31312(19) 0.0252(5) Uani 1 1 d . . . . . C6A C 0.7265(4) 0.0327(2) 0.3588(2) 0.0300(6) Uani 1 1 d . . . . . H6A H 0.663352 0.104765 0.323829 0.036 Uiso 1 1 calc R U . . . C7A C 0.7196(4) 0.0315(3) 0.4551(2) 0.0324(6) Uani 1 1 d . . . . . H7A H 0.649898 0.103212 0.486491 0.039 Uiso 1 1 calc R U . . . C8A C 0.8126(4) -0.0730(3) 0.5081(2) 0.0283(6) Uani 1 1 d . . . . . C9A C 0.9145(4) -0.1773(2) 0.4607(2) 0.0290(6) Uani 1 1 d . . . . . H9A H 0.978684 -0.249082 0.495571 0.035 Uiso 1 1 calc R U . . . C10A C 0.9235(4) -0.1779(2) 0.3636(2) 0.0284(6) Uani 1 1 d . . . . . H10A H 0.994368 -0.248948 0.331771 0.034 Uiso 1 1 calc R U . . . C11A C 0.8034(4) -0.0726(3) 0.6134(2) 0.0351(6) Uani 1 1 d . . . . . H11A H 0.839470 0.001349 0.627982 0.053 Uiso 1 1 calc R U . . . H11B H 0.887724 -0.148738 0.637439 0.053 Uiso 1 1 calc R U . . . H11C H 0.676966 -0.070241 0.643402 0.053 Uiso 1 1 calc R U . . . S1C S 0.65314(9) 0.57034(6) 0.65344(5) 0.02907(17) Uani 1 1 d . . . . . O1D O 0.198(2) 0.6728(10) 0.7042(7) 0.044(2) Uani 0.401(6) 1 d D . P A 2 O2C O 0.6119(3) 0.69639(19) 0.61227(15) 0.0378(5) Uani 1 1 d . . . . . O3C O 0.8054(3) 0.4776(2) 0.61267(15) 0.0365(5) Uani 1 1 d . . . . . N1C N 0.4693(3) 0.5163(2) 0.65236(17) 0.0311(5) Uani 1 1 d D . . . . C1C C 0.2791(4) 0.5734(3) 0.6677(3) 0.0446(8) Uani 1 1 d D . . . . C2D C 0.2324(14) 0.4585(11) 0.6405(9) 0.040(3) Uani 0.401(6) 1 d D . P A 2 H2DA H 0.164161 0.474575 0.585080 0.048 Uiso 0.401(6) 1 calc R U P A 2 H2DB H 0.170256 0.413058 0.693855 0.048 Uiso 0.401(6) 1 calc R U P A 2 C3D C 0.4435(9) 0.3981(6) 0.6167(6) 0.0285(16) Uani 0.401(6) 1 d D . P A 2 H3D H 0.484190 0.392123 0.547270 0.034 Uiso 0.401(6) 1 calc R U P A 2 C4D C 0.5221(10) 0.2797(6) 0.6752(6) 0.0332(18) Uani 0.401(6) 1 d D . P A 2 H4DA H 0.657022 0.264017 0.667458 0.050 Uiso 0.401(6) 1 calc R U P A 2 H4DB H 0.487286 0.208881 0.654155 0.050 Uiso 0.401(6) 1 calc R U P A 2 H4DC H 0.473011 0.289367 0.742039 0.050 Uiso 0.401(6) 1 calc R U P A 2 C5C C 0.6698(4) 0.5725(2) 0.7741(2) 0.0272(6) Uani 1 1 d . . . . . C6C C 0.7732(4) 0.4679(2) 0.8214(2) 0.0302(6) Uani 1 1 d . . . . . H6C H 0.837525 0.396184 0.788567 0.036 Uiso 1 1 calc R U . . . C7C C 0.7811(4) 0.4695(3) 0.9163(2) 0.0312(6) Uani 1 1 d . . . . . H7C H 0.852041 0.398135 0.948692 0.037 Uiso 1 1 calc R U . . . C8C C 0.6874(4) 0.5734(3) 0.9663(2) 0.0302(6) Uani 1 1 d . . . . . C9C C 0.5825(4) 0.6769(3) 0.9171(2) 0.0336(6) Uani 1 1 d . . . . . H9C H 0.516004 0.747983 0.949997 0.040 Uiso 1 1 calc R U . . . C10C C 0.5739(4) 0.6777(2) 0.8220(2) 0.0319(6) Uani 1 1 d . . . . . H10C H 0.503341 0.748947 0.789352 0.038 Uiso 1 1 calc R U . . . C11C C 0.6965(4) 0.5748(3) 1.0697(2) 0.0363(7) Uani 1 1 d . . . . . H11D H 0.581649 0.560976 1.106332 0.055 Uiso 1 1 calc R U . . . H11E H 0.712853 0.656219 1.082240 0.055 Uiso 1 1 calc R U . . . H11F H 0.801091 0.508091 1.088304 0.055 Uiso 1 1 calc R U . . . C2A C 1.2636(11) 0.0419(7) 0.1190(7) 0.042(2) Uani 0.599(6) 1 d D . P A 1 H2AA H 1.310444 0.067073 0.053215 0.050 Uiso 0.599(6) 1 calc R U P A 1 H2AB H 1.346773 0.049439 0.163769 0.050 Uiso 0.599(6) 1 calc R U P A 1 C3A C 1.0565(6) 0.1053(4) 0.1493(4) 0.0283(11) Uani 0.599(6) 1 d D . P A 1 H3A H 1.032871 0.130791 0.215651 0.034 Uiso 0.599(6) 1 calc R U P A 1 C4A C 0.9614(7) 0.2068(4) 0.0816(4) 0.0335(12) Uani 0.599(6) 1 d D . P A 1 H4AA H 0.994793 0.180033 0.017054 0.050 Uiso 0.599(6) 1 calc R U P A 1 H4AB H 1.000467 0.284008 0.084649 0.050 Uiso 0.599(6) 1 calc R U P A 1 H4AC H 0.827333 0.222469 0.099016 0.050 Uiso 0.599(6) 1 calc R U P A 1 O1A O 1.2829(12) -0.1913(6) 0.1227(6) 0.0556(19) Uani 0.599(6) 1 d D . P A 1 C2C C 0.2296(11) 0.4488(7) 0.6807(6) 0.041(2) Uani 0.599(6) 1 d D . P A 1 H2CA H 0.174590 0.430529 0.627283 0.050 Uiso 0.599(6) 1 calc R U P A 1 H2CB H 0.155038 0.433809 0.742087 0.050 Uiso 0.599(6) 1 calc R U P A 1 C3C C 0.4390(7) 0.3869(4) 0.6781(4) 0.0314(12) Uani 0.599(6) 1 d D . P A 1 H3C H 0.471138 0.354407 0.742886 0.038 Uiso 0.599(6) 1 calc R U P A 1 C4C C 0.5285(8) 0.2934(5) 0.6075(5) 0.0420(14) Uani 0.599(6) 1 d D . P A 1 H4CA H 0.500791 0.329688 0.544255 0.063 Uiso 0.599(6) 1 calc R U P A 1 H4CB H 0.481028 0.218071 0.623545 0.063 Uiso 0.599(6) 1 calc R U P A 1 H4CC H 0.662468 0.270960 0.608170 0.063 Uiso 0.599(6) 1 calc R U P A 1 O1C O 0.2002(13) 0.6827(6) 0.6630(7) 0.070(3) Uani 0.599(6) 1 d D . P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1A 0.0263(3) 0.0242(3) 0.0345(4) -0.0023(2) -0.0052(3) -0.0080(2) O1B 0.032(3) 0.022(3) 0.089(8) -0.008(4) -0.012(5) -0.002(2) O2A 0.0423(12) 0.0281(10) 0.0388(11) -0.0075(8) -0.0039(9) -0.0143(9) O3A 0.0305(11) 0.0362(11) 0.0427(12) 0.0004(9) -0.0127(9) -0.0064(9) N1A 0.0309(12) 0.0224(11) 0.0355(13) -0.0006(9) -0.0025(10) -0.0069(9) C1A 0.0310(15) 0.0273(14) 0.063(2) -0.0065(13) 0.0004(14) -0.0070(12) C2B 0.018(4) 0.039(5) 0.051(7) 0.000(4) -0.004(4) -0.008(3) C3B 0.026(3) 0.034(4) 0.034(5) 0.009(3) -0.003(3) -0.012(3) C4B 0.033(4) 0.028(4) 0.055(6) 0.006(3) -0.004(4) -0.009(3) C5A 0.0218(12) 0.0212(12) 0.0338(14) -0.0010(10) -0.0046(10) -0.0070(10) C6A 0.0284(14) 0.0186(12) 0.0410(16) -0.0009(11) -0.0063(11) -0.0014(10) C7A 0.0329(15) 0.0225(13) 0.0396(16) -0.0054(11) -0.0018(12) -0.0033(11) C8A 0.0247(13) 0.0250(13) 0.0368(15) 0.0007(11) -0.0038(11) -0.0107(10) C9A 0.0260(13) 0.0198(12) 0.0407(15) 0.0017(11) -0.0055(11) -0.0057(10) C10A 0.0256(13) 0.0165(12) 0.0425(16) -0.0030(10) -0.0031(11) -0.0045(10) C11A 0.0368(16) 0.0314(15) 0.0386(16) -0.0024(12) -0.0046(12) -0.0116(12) S1C 0.0263(3) 0.0238(3) 0.0378(4) 0.0019(3) -0.0043(3) -0.0091(3) O1D 0.038(4) 0.026(4) 0.060(5) 0.005(3) -0.008(4) 0.000(3) O2C 0.0448(12) 0.0287(10) 0.0427(12) 0.0097(9) -0.0092(9) -0.0172(9) O3C 0.0292(10) 0.0369(11) 0.0423(12) -0.0071(9) -0.0004(9) -0.0068(9) N1C 0.0293(12) 0.0222(11) 0.0426(14) 0.0012(10) -0.0085(10) -0.0073(9) C1C 0.0277(15) 0.0278(15) 0.078(2) 0.0043(15) -0.0159(15) -0.0050(12) C2D 0.018(4) 0.040(5) 0.063(8) 0.007(5) -0.008(5) -0.012(3) C3D 0.027(3) 0.033(4) 0.028(4) -0.006(3) -0.002(3) -0.013(3) C4D 0.032(4) 0.026(3) 0.042(5) -0.009(3) 0.001(3) -0.008(3) C5C 0.0221(13) 0.0229(13) 0.0375(15) 0.0010(10) -0.0052(11) -0.0080(10) C6C 0.0264(14) 0.0191(12) 0.0418(16) -0.0017(11) -0.0003(11) -0.0026(10) C7C 0.0271(14) 0.0225(13) 0.0412(16) 0.0033(11) -0.0042(11) -0.0037(11) C8C 0.0262(14) 0.0257(13) 0.0413(16) -0.0022(11) -0.0032(11) -0.0118(11) C9C 0.0312(15) 0.0209(13) 0.0486(17) -0.0059(12) -0.0018(12) -0.0069(11) C10C 0.0299(14) 0.0186(12) 0.0460(17) 0.0014(11) -0.0076(12) -0.0042(11) C11C 0.0352(16) 0.0347(16) 0.0415(17) -0.0024(12) -0.0046(13) -0.0135(13) C2A 0.033(3) 0.025(3) 0.067(6) 0.000(3) -0.006(4) -0.009(2) C3A 0.032(2) 0.022(2) 0.032(3) 0.0023(19) -0.007(2) -0.0072(18) C4A 0.038(3) 0.028(2) 0.035(3) 0.004(2) -0.009(2) -0.008(2) O1A 0.040(3) 0.025(2) 0.098(6) -0.014(3) 0.001(4) -0.0028(18) C2C 0.032(3) 0.025(3) 0.066(6) 0.003(3) -0.006(3) -0.008(2) C3C 0.030(2) 0.021(2) 0.044(3) 0.002(2) -0.006(2) -0.0091(18) C4C 0.043(3) 0.035(3) 0.051(4) -0.014(2) -0.002(3) -0.013(2) O1C 0.035(3) 0.025(2) 0.150(9) 0.010(4) -0.031(6) -0.0019(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1A O2A 1.427(2) . ? S1A O3A 1.435(2) . ? S1A N1A 1.656(2) . ? S1A C5A 1.754(3) . ? O1B C1A 1.251(9) . ? N1A C1A 1.408(4) . ? N1A C3B 1.517(7) . ? N1A C3A 1.508(5) . ? C1A C2B 1.504(11) . ? C1A C2A 1.519(8) . ? C1A O1A 1.186(7) . ? C2B H2BA 0.9900 . ? C2B H2BB 0.9900 . ? C2B C3B 1.566(11) . ? C3B H3B 1.0000 . ? C3B C4B 1.478(10) . ? C4B H4BA 0.9800 . ? C4B H4BB 0.9800 . ? C4B H4BC 0.9800 . ? C5A C6A 1.390(4) . ? C5A C10A 1.393(4) . ? C6A H6A 0.9500 . ? C6A C7A 1.374(4) . ? C7A H7A 0.9500 . ? C7A C8A 1.397(4) . ? C8A C9A 1.395(4) . ? C8A C11A 1.502(4) . ? C9A H9A 0.9500 . ? C9A C10A 1.385(4) . ? C10A H10A 0.9500 . ? C11A H11A 0.9800 . ? C11A H11B 0.9800 . ? C11A H11C 0.9800 . ? S1C O2C 1.427(2) . ? S1C O3C 1.428(2) . ? S1C N1C 1.651(2) . ? S1C C5C 1.759(3) . ? O1D C1C 1.244(10) . ? N1C C1C 1.407(4) . ? N1C C3D 1.525(7) . ? N1C C3C 1.503(5) . ? C1C C2D 1.510(11) . ? C1C C2C 1.503(8) . ? C1C O1C 1.202(7) . ? C2D H2DA 0.9900 . ? C2D H2DB 0.9900 . ? C2D C3D 1.562(11) . ? C3D H3D 1.0000 . ? C3D C4D 1.509(10) . ? C4D H4DA 0.9800 . ? C4D H4DB 0.9800 . ? C4D H4DC 0.9800 . ? C5C C6C 1.390(4) . ? C5C C10C 1.395(4) . ? C6C H6C 0.9500 . ? C6C C7C 1.375(4) . ? C7C H7C 0.9500 . ? C7C C8C 1.396(4) . ? C8C C9C 1.400(4) . ? C8C C11C 1.499(4) . ? C9C H9C 0.9500 . ? C9C C10C 1.375(4) . ? C10C H10C 0.9500 . ? C11C H11D 0.9800 . ? C11C H11E 0.9800 . ? C11C H11F 0.9800 . ? C2A H2AA 0.9900 . ? C2A H2AB 0.9900 . ? C2A C3A 1.557(8) . ? C3A H3A 1.0000 . ? C3A C4A 1.508(7) . ? C4A H4AA 0.9800 . ? C4A H4AB 0.9800 . ? C4A H4AC 0.9800 . ? C2C H2CA 0.9900 . ? C2C H2CB 0.9900 . ? C2C C3C 1.550(8) . ? C3C H3C 1.0000 . ? C3C C4C 1.491(7) . ? C4C H4CA 0.9800 . ? C4C H4CB 0.9800 . ? C4C H4CC 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2A S1A O3A 120.83(13) . . ? O2A S1A N1A 106.22(12) . . ? O2A S1A C5A 109.33(12) . . ? O3A S1A N1A 105.12(12) . . ? O3A S1A C5A 108.57(13) . . ? N1A S1A C5A 105.69(12) . . ? C1A N1A S1A 132.0(2) . . ? C1A N1A C3B 91.9(3) . . ? C1A N1A C3A 94.4(3) . . ? C3B N1A S1A 135.6(3) . . ? C3A N1A S1A 127.6(2) . . ? O1B C1A N1A 130.0(7) . . ? O1B C1A C2B 134.6(8) . . ? N1A C1A C2B 94.0(5) . . ? N1A C1A C2A 90.6(4) . . ? O1A C1A N1A 129.2(5) . . ? O1A C1A C2A 139.8(6) . . ? C1A C2B H2BA 114.2 . . ? C1A C2B H2BB 114.2 . . ? C1A C2B C3B 86.5(6) . . ? H2BA C2B H2BB 111.4 . . ? C3B C2B H2BA 114.2 . . ? C3B C2B H2BB 114.2 . . ? N1A C3B C2B 87.4(5) . . ? N1A C3B H3B 111.8 . . ? C2B C3B H3B 111.8 . . ? C4B C3B N1A 113.6(6) . . ? C4B C3B C2B 118.2(7) . . ? C4B C3B H3B 111.8 . . ? C3B C4B H4BA 109.5 . . ? C3B C4B H4BB 109.5 . . ? C3B C4B H4BC 109.5 . . ? H4BA C4B H4BB 109.5 . . ? H4BA C4B H4BC 109.5 . . ? H4BB C4B H4BC 109.5 . . ? C6A C5A S1A 119.8(2) . . ? C6A C5A C10A 120.8(3) . . ? C10A C5A S1A 119.4(2) . . ? C5A C6A H6A 120.4 . . ? C7A C6A C5A 119.2(3) . . ? C7A C6A H6A 120.4 . . ? C6A C7A H7A 119.3 . . ? C6A C7A C8A 121.5(3) . . ? C8A C7A H7A 119.3 . . ? C7A C8A C11A 120.7(3) . . ? C9A C8A C7A 118.4(3) . . ? C9A C8A C11A 120.9(2) . . ? C8A C9A H9A 119.5 . . ? C10A C9A C8A 121.0(2) . . ? C10A C9A H9A 119.5 . . ? C5A C10A H10A 120.5 . . ? C9A C10A C5A 119.1(2) . . ? C9A C10A H10A 120.5 . . ? C8A C11A H11A 109.5 . . ? C8A C11A H11B 109.5 . . ? C8A C11A H11C 109.5 . . ? H11A C11A H11B 109.5 . . ? H11A C11A H11C 109.5 . . ? H11B C11A H11C 109.5 . . ? O2C S1C O3C 121.02(13) . . ? O2C S1C N1C 106.68(12) . . ? O2C S1C C5C 108.72(13) . . ? O3C S1C N1C 105.26(12) . . ? O3C S1C C5C 109.16(13) . . ? N1C S1C C5C 104.77(13) . . ? C1C N1C S1C 131.9(2) . . ? C1C N1C C3D 94.5(3) . . ? C1C N1C C3C 92.7(3) . . ? C3D N1C S1C 132.7(3) . . ? C3C N1C S1C 130.6(2) . . ? O1D C1C N1C 129.6(8) . . ? O1D C1C C2D 138.3(9) . . ? N1C C1C C2D 91.2(4) . . ? N1C C1C C2C 92.2(4) . . ? O1C C1C N1C 129.8(6) . . ? O1C C1C C2C 137.8(6) . . ? C1C C2D H2DA 113.8 . . ? C1C C2D H2DB 113.8 . . ? C1C C2D C3D 89.0(6) . . ? H2DA C2D H2DB 111.0 . . ? C3D C2D H2DA 113.8 . . ? C3D C2D H2DB 113.8 . . ? N1C C3D C2D 85.0(5) . . ? N1C C3D H3D 113.0 . . ? C2D C3D H3D 113.0 . . ? C4D C3D N1C 113.3(6) . . ? C4D C3D C2D 116.7(7) . . ? C4D C3D H3D 113.0 . . ? C3D C4D H4DA 109.5 . . ? C3D C4D H4DB 109.5 . . ? C3D C4D H4DC 109.5 . . ? H4DA C4D H4DB 109.5 . . ? H4DA C4D H4DC 109.5 . . ? H4DB C4D H4DC 109.5 . . ? C6C C5C S1C 119.6(2) . . ? C6C C5C C10C 120.7(3) . . ? C10C C5C S1C 119.6(2) . . ? C5C C6C H6C 120.5 . . ? C7C C6C C5C 119.1(3) . . ? C7C C6C H6C 120.5 . . ? C6C C7C H7C 119.2 . . ? C6C C7C C8C 121.7(3) . . ? C8C C7C H7C 119.2 . . ? C7C C8C C9C 118.0(3) . . ? C7C C8C C11C 121.5(3) . . ? C9C C8C C11C 120.6(3) . . ? C8C C9C H9C 119.3 . . ? C10C C9C C8C 121.3(3) . . ? C10C C9C H9C 119.3 . . ? C5C C10C H10C 120.4 . . ? C9C C10C C5C 119.2(3) . . ? C9C C10C H10C 120.4 . . ? C8C C11C H11D 109.5 . . ? C8C C11C H11E 109.5 . . ? C8C C11C H11F 109.5 . . ? H11D C11C H11E 109.5 . . ? H11D C11C H11F 109.5 . . ? H11E C11C H11F 109.5 . . ? C1A C2A H2AA 113.9 . . ? C1A C2A H2AB 113.9 . . ? C1A C2A C3A 88.2(4) . . ? H2AA C2A H2AB 111.1 . . ? C3A C2A H2AA 113.9 . . ? C3A C2A H2AB 113.9 . . ? N1A C3A C2A 85.6(4) . . ? N1A C3A H3A 112.3 . . ? C2A C3A H3A 112.3 . . ? C4A C3A N1A 114.6(4) . . ? C4A C3A C2A 117.2(5) . . ? C4A C3A H3A 112.3 . . ? C3A C4A H4AA 109.5 . . ? C3A C4A H4AB 109.5 . . ? C3A C4A H4AC 109.5 . . ? H4AA C4A H4AB 109.5 . . ? H4AA C4A H4AC 109.5 . . ? H4AB C4A H4AC 109.5 . . ? C1C C2C H2CA 114.1 . . ? C1C C2C H2CB 114.1 . . ? C1C C2C C3C 87.3(4) . . ? H2CA C2C H2CB 111.3 . . ? C3C C2C H2CA 114.1 . . ? C3C C2C H2CB 114.1 . . ? N1C C3C C2C 86.8(4) . . ? N1C C3C H3C 111.3 . . ? C2C C3C H3C 111.3 . . ? C4C C3C N1C 115.4(5) . . ? C4C C3C C2C 118.6(5) . . ? C4C C3C H3C 111.3 . . ? C3C C4C H4CA 109.5 . . ? C3C C4C H4CB 109.5 . . ? C3C C4C H4CC 109.5 . . ? H4CA C4C H4CB 109.5 . . ? H4CA C4C H4CC 109.5 . . ? H4CB C4C H4CC 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S1A N1A C1A O1B -15.3(8) . . . . ? S1A N1A C1A C2B 177.4(5) . . . . ? S1A N1A C1A C2A -161.7(4) . . . . ? S1A N1A C1A O1A 24.9(8) . . . . ? S1A N1A C3B C2B -176.8(5) . . . . ? S1A N1A C3B C4B 63.4(9) . . . . ? S1A N1A C3A C2A 163.3(4) . . . . ? S1A N1A C3A C4A -78.7(5) . . . . ? S1A C5A C6A C7A -179.9(2) . . . . ? S1A C5A C10A C9A -180.0(2) . . . . ? O1B C1A C2B C3B -170.3(8) . . . . ? O2A S1A N1A C1A -34.7(3) . . . . ? O2A S1A N1A C3B 135.7(5) . . . . ? O2A S1A N1A C3A 179.7(3) . . . . ? O2A S1A C5A C6A -154.5(2) . . . . ? O2A S1A C5A C10A 26.9(3) . . . . ? O3A S1A N1A C1A -163.8(3) . . . . ? O3A S1A N1A C3B 6.5(6) . . . . ? O3A S1A N1A C3A 50.5(3) . . . . ? O3A S1A C5A C6A -20.8(3) . . . . ? O3A S1A C5A C10A 160.6(2) . . . . ? N1A S1A C5A C6A 91.5(2) . . . . ? N1A S1A C5A C10A -87.1(2) . . . . ? N1A C1A C2B C3B -4.0(6) . . . . ? N1A C1A C2A C3A 8.1(4) . . . . ? C1A N1A C3B C2B -3.9(6) . . . . ? C1A N1A C3B C4B -123.7(6) . . . . ? C1A N1A C3A C2A 8.2(4) . . . . ? C1A N1A C3A C4A 126.2(4) . . . . ? C1A C2B C3B N1A 3.7(5) . . . . ? C1A C2B C3B C4B 119.2(8) . . . . ? C1A C2A C3A N1A -7.6(4) . . . . ? C1A C2A C3A C4A -123.1(5) . . . . ? C3B N1A C1A O1B 171.4(7) . . . . ? C3B N1A C1A C2B 4.1(6) . . . . ? C5A S1A N1A C1A 81.4(3) . . . . ? C5A S1A N1A C3B -108.2(5) . . . . ? C5A S1A N1A C3A -64.2(3) . . . . ? C5A C6A C7A C8A 0.6(4) . . . . ? C6A C5A C10A C9A 1.5(4) . . . . ? C6A C7A C8A C9A 0.1(4) . . . . ? C6A C7A C8A C11A 180.0(3) . . . . ? C7A C8A C9A C10A 0.0(4) . . . . ? C8A C9A C10A C5A -0.7(4) . . . . ? C10A C5A C6A C7A -1.4(4) . . . . ? C11A C8A C9A C10A -179.9(3) . . . . ? S1C N1C C1C O1D -15.7(8) . . . . ? S1C N1C C1C C2D 173.7(5) . . . . ? S1C N1C C1C C2C -164.5(4) . . . . ? S1C N1C C1C O1C 20.5(9) . . . . ? S1C N1C C3D C2D -173.4(5) . . . . ? S1C N1C C3D C4D 69.6(7) . . . . ? S1C N1C C3C C2C 164.7(4) . . . . ? S1C N1C C3C C4C -75.1(6) . . . . ? S1C C5C C6C C7C -178.3(2) . . . . ? S1C C5C C10C C9C 177.8(2) . . . . ? O1D C1C C2D C3D -172.8(8) . . . . ? O2C S1C N1C C1C -37.8(3) . . . . ? O2C S1C N1C C3D 128.4(5) . . . . ? O2C S1C N1C C3C 173.7(4) . . . . ? O2C S1C C5C C6C -155.8(2) . . . . ? O2C S1C C5C C10C 26.4(3) . . . . ? O3C S1C N1C C1C -167.6(3) . . . . ? O3C S1C N1C C3D -1.3(5) . . . . ? O3C S1C N1C C3C 44.0(4) . . . . ? O3C S1C C5C C6C -21.9(3) . . . . ? O3C S1C C5C C10C 160.3(2) . . . . ? N1C S1C C5C C6C 90.4(2) . . . . ? N1C S1C C5C C10C -87.4(2) . . . . ? N1C C1C C2D C3D -3.6(6) . . . . ? N1C C1C C2C C3C 7.7(4) . . . . ? C1C N1C C3D C2D -3.6(6) . . . . ? C1C N1C C3D C4D -120.6(6) . . . . ? C1C N1C C3C C2C 7.7(4) . . . . ? C1C N1C C3C C4C 127.9(5) . . . . ? C1C C2D C3D N1C 3.4(5) . . . . ? C1C C2D C3D C4D 117.0(7) . . . . ? C1C C2C C3C N1C -7.2(4) . . . . ? C1C C2C C3C C4C -124.5(6) . . . . ? C3D N1C C1C O1D 174.4(7) . . . . ? C3D N1C C1C C2D 3.7(6) . . . . ? C5C S1C N1C C1C 77.3(3) . . . . ? C5C S1C N1C C3D -116.4(5) . . . . ? C5C S1C N1C C3C -71.1(4) . . . . ? C5C C6C C7C C8C 0.2(4) . . . . ? C6C C5C C10C C9C 0.0(4) . . . . ? C6C C7C C8C C9C 0.5(4) . . . . ? C6C C7C C8C C11C -179.9(3) . . . . ? C7C C8C C9C C10C -1.1(4) . . . . ? C8C C9C C10C C5C 0.8(4) . . . . ? C10C C5C C6C C7C -0.5(4) . . . . ? C11C C8C C9C C10C 179.4(3) . . . . ? C3A N1A C1A C2A -8.4(4) . . . . ? C3A N1A C1A O1A 178.2(6) . . . . ? O1A C1A C2A C3A -179.8(7) . . . . ? C3C N1C C1C C2C -7.9(4) . . . . ? C3C N1C C1C O1C 177.1(7) . . . . ? O1C C1C C2C C3C -178.0(8) . . . . ? _shelx_res_file ; TITL ca121021_1_1_a.res in P-1 ca121021_1_1.res created by SHELXL-2018/3 at 15:35:56 on 13-Oct-2021 REM Old TITL ca121021_1_1 in P-1 REM SHELXT solution in P-1 REM R1 0.171, Rweak 0.015, Alpha 0.086, Orientation as input REM Formula found by SHELXT: C24 N2 O6 S2 CELL 1.54184 7.5584 11.065 14.3491 83.402 81.007 75.074 ZERR 4 0.0002 0.0003 0.0004 0.002 0.002 0.002 LATT 1 SFAC C H N O S UNIT 44 52 4 12 4 SADI O1A C1A O1B C1A SADI C2B C1A C2A C1A RIGU O1B N1A C1A C2B C3B C4B C2A C3A C4A O1A SADI C4B C3B C4A C3A SADI N1A C3B N1A C3A SADI C3A C2A C3B C2B SADI C2C C1C C2D C1C SADI C3D C2D C3C C2C RIGU O1D N1C C1C C2D C3D C4D C2C C3C C4C O1C SADI O1D C1C O1C C1C SADI N1C C3C N1C C3D SADI C4D C3D C4C C3C L.S. 9 PLAN 20 SIZE 0.1 0.14 0.17 TEMP -173 CONF BOND $H list 4 MORE -1 fmap 2 acta REM REM REM WGHT 0.033600 2.200200 FVAR 0.44814 0.59941 S1A 5 0.837862 -0.072773 0.190127 11.00000 0.02629 0.02420 = 0.03448 -0.00228 -0.00520 -0.00802 PART 2 O1B 4 1.296019 -0.187123 0.165618 -21.00000 0.03243 0.02224 = 0.08878 -0.00777 -0.01232 -0.00244 PART 0 O2A 4 0.872767 -0.198773 0.165218 11.00000 0.04229 0.02813 = 0.03882 -0.00748 -0.00389 -0.01429 O3A 4 0.684550 0.021959 0.159648 11.00000 0.03045 0.03618 = 0.04274 0.00038 -0.01269 -0.00640 N1A 3 1.023235 -0.022264 0.143939 11.00000 0.03087 0.02238 = 0.03548 -0.00064 -0.00250 -0.00694 C1A 1 1.212231 -0.083459 0.130447 11.00000 0.03101 0.02732 = 0.06271 -0.00651 0.00040 -0.00704 PART 2 C2B 1 1.269692 0.030840 0.081759 -21.00000 0.01788 0.03851 = 0.05135 0.00002 -0.00417 -0.00803 AFIX 23 H2BA 2 1.331425 0.020365 0.016041 -21.00000 -1.20000 H2BB 2 1.340410 0.067213 0.118859 -21.00000 -1.20000 AFIX 0 C3B 1 1.058689 0.096926 0.089571 -21.00000 0.02557 0.03432 = 0.03427 0.00878 -0.00309 -0.01237 AFIX 13 H3B 2 1.012771 0.110962 0.026564 -21.00000 -1.20000 AFIX 0 C4B 1 0.989798 0.209036 0.144075 -21.00000 0.03270 0.02795 = 0.05528 0.00617 -0.00401 -0.00881 AFIX 137 H4BA 2 0.854608 0.233961 0.150044 -21.00000 -1.50000 H4BB 2 1.040226 0.277919 0.111110 -21.00000 -1.50000 H4BC 2 1.028880 0.189562 0.207209 -21.00000 -1.50000 AFIX 0 PART 0 C5A 1 0.827204 -0.072762 0.313122 11.00000 0.02182 0.02119 = 0.03376 -0.00103 -0.00459 -0.00704 C6A 1 0.726537 0.032713 0.358811 11.00000 0.02838 0.01857 = 0.04096 -0.00092 -0.00628 -0.00139 AFIX 43 H6A 2 0.663352 0.104765 0.323829 11.00000 -1.20000 AFIX 0 C7A 1 0.719552 0.031471 0.455134 11.00000 0.03291 0.02246 = 0.03957 -0.00543 -0.00184 -0.00327 AFIX 43 H7A 2 0.649898 0.103212 0.486491 11.00000 -1.20000 AFIX 0 C8A 1 0.812606 -0.072953 0.508051 11.00000 0.02473 0.02503 = 0.03684 0.00068 -0.00385 -0.01068 C9A 1 0.914510 -0.177323 0.460684 11.00000 0.02602 0.01985 = 0.04068 0.00169 -0.00545 -0.00571 AFIX 43 H9A 2 0.978684 -0.249082 0.495571 11.00000 -1.20000 AFIX 0 C10A 1 0.923504 -0.177872 0.363557 11.00000 0.02559 0.01649 = 0.04246 -0.00297 -0.00312 -0.00445 AFIX 43 H10A 2 0.994368 -0.248948 0.331771 11.00000 -1.20000 AFIX 0 C11A 1 0.803390 -0.072617 0.613374 11.00000 0.03683 0.03142 = 0.03856 -0.00237 -0.00463 -0.01165 AFIX 137 H11A 2 0.839470 0.001349 0.627982 11.00000 -1.50000 H11B 2 0.887724 -0.148738 0.637439 11.00000 -1.50000 H11C 2 0.676966 -0.070241 0.643402 11.00000 -1.50000 AFIX 0 S1C 5 0.653145 0.570342 0.653441 11.00000 0.02627 0.02377 = 0.03784 0.00187 -0.00429 -0.00912 PART 2 O1D 4 0.197709 0.672827 0.704197 -21.00000 0.03845 0.02648 = 0.05969 0.00482 -0.00808 0.00029 PART 0 O2C 4 0.611891 0.696387 0.612269 11.00000 0.04479 0.02873 = 0.04272 0.00975 -0.00916 -0.01724 O3C 4 0.805434 0.477644 0.612669 11.00000 0.02915 0.03688 = 0.04228 -0.00714 -0.00036 -0.00677 N1C 3 0.469299 0.516253 0.652355 11.00000 0.02926 0.02221 = 0.04264 0.00124 -0.00848 -0.00728 C1C 1 0.279105 0.573352 0.667746 11.00000 0.02773 0.02784 = 0.07827 0.00428 -0.01585 -0.00498 PART 2 C2D 1 0.232447 0.458519 0.640546 -21.00000 0.01770 0.04043 = 0.06307 0.00655 -0.00812 -0.01239 AFIX 23 H2DA 2 0.164161 0.474575 0.585080 -21.00000 -1.20000 H2DB 2 0.170256 0.413058 0.693855 -21.00000 -1.20000 AFIX 0 C3D 1 0.443485 0.398120 0.616684 -21.00000 0.02725 0.03340 = 0.02827 -0.00580 -0.00218 -0.01269 AFIX 13 H3D 2 0.484190 0.392123 0.547270 -21.00000 -1.20000 AFIX 0 C4D 1 0.522089 0.279721 0.675213 -21.00000 0.03179 0.02587 = 0.04174 -0.00948 0.00119 -0.00755 AFIX 137 H4DA 2 0.657022 0.264017 0.667458 -21.00000 -1.50000 H4DB 2 0.487286 0.208881 0.654155 -21.00000 -1.50000 H4DC 2 0.473011 0.289367 0.742039 -21.00000 -1.50000 AFIX 0 PART 0 C5C 1 0.669838 0.572520 0.774085 11.00000 0.02213 0.02289 = 0.03754 0.00102 -0.00516 -0.00800 C6C 1 0.773198 0.467861 0.821365 11.00000 0.02643 0.01911 = 0.04176 -0.00166 -0.00032 -0.00264 AFIX 43 H6C 2 0.837525 0.396184 0.788567 11.00000 -1.20000 AFIX 0 C7C 1 0.781067 0.469496 0.916315 11.00000 0.02706 0.02254 = 0.04125 0.00329 -0.00420 -0.00373 AFIX 43 H7C 2 0.852041 0.398135 0.948692 11.00000 -1.20000 AFIX 0 C8C 1 0.687353 0.573413 0.966318 11.00000 0.02621 0.02571 = 0.04128 -0.00215 -0.00322 -0.01183 C9C 1 0.582510 0.676876 0.917063 11.00000 0.03120 0.02090 = 0.04864 -0.00590 -0.00176 -0.00685 AFIX 43 H9C 2 0.516004 0.747983 0.949997 11.00000 -1.20000 AFIX 0 C10C 1 0.573853 0.677656 0.822012 11.00000 0.02992 0.01861 = 0.04596 0.00137 -0.00756 -0.00416 AFIX 43 H10C 2 0.503341 0.748947 0.789352 11.00000 -1.20000 AFIX 0 C11C 1 0.696530 0.574794 1.069745 11.00000 0.03523 0.03474 = 0.04153 -0.00243 -0.00456 -0.01352 AFIX 137 H11D 2 0.581649 0.560976 1.106332 11.00000 -1.50000 H11E 2 0.712853 0.656219 1.082240 11.00000 -1.50000 H11F 2 0.801091 0.508091 1.088304 11.00000 -1.50000 AFIX 0 PART 1 C2A 1 1.263572 0.041945 0.119015 21.00000 0.03316 0.02517 = 0.06745 -0.00005 -0.00580 -0.00928 AFIX 23 H2AA 2 1.310444 0.067073 0.053215 21.00000 -1.20000 H2AB 2 1.346773 0.049439 0.163769 21.00000 -1.20000 AFIX 0 C3A 1 1.056469 0.105297 0.149320 21.00000 0.03161 0.02168 = 0.03177 0.00234 -0.00660 -0.00723 AFIX 13 H3A 2 1.032871 0.130791 0.215651 21.00000 -1.20000 AFIX 0 C4A 1 0.961446 0.206843 0.081578 21.00000 0.03775 0.02763 = 0.03482 0.00444 -0.00857 -0.00803 AFIX 137 H4AA 2 0.994793 0.180033 0.017054 21.00000 -1.50000 H4AB 2 1.000467 0.284008 0.084649 21.00000 -1.50000 H4AC 2 0.827333 0.222469 0.099016 21.00000 -1.50000 AFIX 0 O1A 4 1.282871 -0.191313 0.122660 21.00000 0.03966 0.02503 = 0.09791 -0.01384 0.00137 -0.00281 C2C 1 0.229638 0.448754 0.680716 21.00000 0.03162 0.02539 = 0.06585 0.00285 -0.00559 -0.00752 AFIX 23 H2CA 2 0.174590 0.430529 0.627283 21.00000 -1.20000 H2CB 2 0.155038 0.433809 0.742087 21.00000 -1.20000 AFIX 0 C3C 1 0.438982 0.386876 0.678147 21.00000 0.03025 0.02113 = 0.04356 0.00202 -0.00578 -0.00907 AFIX 13 H3C 2 0.471138 0.354407 0.742886 21.00000 -1.20000 AFIX 0 C4C 1 0.528482 0.293393 0.607477 21.00000 0.04332 0.03533 = 0.05067 -0.01431 -0.00163 -0.01331 AFIX 137 H4CA 2 0.500791 0.329688 0.544255 21.00000 -1.50000 H4CB 2 0.481028 0.218071 0.623545 21.00000 -1.50000 H4CC 2 0.662468 0.270960 0.608170 21.00000 -1.50000 AFIX 0 O1C 4 0.200211 0.682681 0.663027 21.00000 0.03480 0.02477 = 0.14984 0.00964 -0.03054 -0.00187 HKLF 4 REM ca121021_1_1_a.res in P-1 REM wR2 = 0.1368, GooF = S = 1.098, Restrained GooF = 1.084 for all data REM R1 = 0.0590 for 4347 Fo > 4sig(Fo) and 0.0636 for all 4756 data REM 368 parameters refined using 148 restraints END WGHT 0.0336 2.2000 REM Highest difference peak 0.513, deepest hole -0.656, 1-sigma level 0.063 Q1 1 0.8194 -0.0645 0.2508 11.00000 0.05 0.51 Q2 1 0.5503 0.5412 0.6554 11.00000 0.05 0.40 Q3 1 0.6392 0.5778 0.7147 11.00000 0.05 0.38 Q4 1 0.9431 -0.0492 0.1745 11.00000 0.05 0.28 Q5 1 0.8349 0.1969 0.0796 11.00000 0.05 0.26 Q6 1 0.6226 0.6203 0.7945 11.00000 0.05 0.26 Q7 1 0.7017 -0.0612 0.1810 11.00000 0.05 0.26 Q8 1 0.8135 -0.0792 0.5567 11.00000 0.05 0.24 Q9 1 0.8037 0.6080 1.0655 11.00000 0.05 0.24 Q10 1 0.6860 0.4990 1.1057 11.00000 0.05 0.23 Q11 1 0.5655 0.6555 1.0843 11.00000 0.05 0.23 Q12 1 0.7675 -0.0276 0.3281 11.00000 0.05 0.22 Q13 1 0.8533 -0.1200 0.4789 11.00000 0.05 0.22 Q14 1 0.6886 0.5121 0.8029 11.00000 0.05 0.22 Q15 1 0.8708 -0.1190 0.3368 11.00000 0.05 0.21 Q16 1 0.8407 0.5414 0.5989 11.00000 0.05 0.20 Q17 1 0.2008 0.5170 0.7114 11.00000 0.05 0.19 Q18 1 0.7085 0.2357 0.0209 11.00000 0.05 0.19 Q19 1 0.9059 -0.2400 0.1196 11.00000 0.05 0.19 Q20 1 0.8341 -0.3102 0.1493 11.00000 0.05 0.19 ; _shelx_res_checksum 93360 _shelx_hkl_file ; 0 0 1 14.34 0.68 0 0 -1 14.21 0.73 0 0 2 380.44 14.95 0 0 -2 380.85 14.85 0 0 2 404.08 14.95 0 0 -2 378.43 14.90 0 0 -2 389.56 15.02 0 0 2 398.25 14.90 0 0 3 5.97 0.76 0 0 -3 4.72 0.68 0 0 3 5.10 0.71 0 0 -3 4.53 0.61 0 0 3 5.12 0.64 0 0 -3 5.75 0.72 0 0 4 3718.09 141.83 0 0 4 3696.34 141.94 0 0 4 3817.35 141.92 0 0 -4 3788.87 141.72 0 0 4 3773.07 141.97 0 0 -4 3840.75 141.84 0 0 4 3720.32 141.48 0 0 -4 3722.31 142.08 0 0 4 3780.16 141.82 0 0 -4 3730.54 141.49 0 0 4 3720.55 142.04 0 0 5 17.60 1.50 0 0 5 17.78 1.53 0 0 5 18.52 1.42 0 0 -5 20.37 1.45 0 0 5 18.40 1.47 0 0 5 19.82 1.58 0 0 -5 19.45 1.58 0 0 5 16.37 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13.31 2.41 0 0 12 13.96 1.51 0 0 12 10.68 1.40 0 0 -12 13.98 1.37 0 0 12 12.73 1.46 0 0 12 13.07 2.47 0 0 -12 13.31 1.40 0 0 -13 0.23 1.68 0 0 13 0.66 0.95 0 0 -13 2.09 0.87 0 0 -13 2.29 0.87 0 0 13 3.95 1.51 0 0 -13 1.61 0.89 0 0 13 1.35 0.97 0 0 -13 1.55 0.95 0 0 13 0.25 1.60 0 0 -13 2.21 0.96 0 0 -14 3.61 0.91 0 0 14 3.65 0.90 0 0 14 2.11 0.92 0 0 -14 1.59 0.86 0 0 -14 2.70 0.92 0 0 14 1.69 1.54 0 0 -14 2.20 0.94 0 0 14 4.19 1.05 0 0 15 2.53 0.88 0 0 15 2.58 0.76 0 0 -15 2.16 0.81 0 0 15 1.08 1.63 0 0 -15 3.64 0.92 0 0 15 2.29 0.92 0 0 -15 3.33 0.92 0 0 -16 0.52 0.56 0 0 -16 0.66 0.70 0 0 16 0.35 1.34 0 0 -18 2.34 0.36 0 0 18 0.93 0.36 0 1 -17 12.02 1.00 0 -1 17 12.58 1.02 0 1 -16 20.37 1.43 0 1 -15 15.01 1.21 0 1 -15 15.13 1.38 0 1 -15 19.44 1.48 0 1 -15 17.78 1.34 0 -1 15 17.08 1.56 0 1 -14 0.31 0.82 0 1 -14 0.65 0.81 0 1 -14 0.20 0.84 0 1 -14 0.54 0.86 0 -1 14 0.47 1.50 0 -1 14 1.52 1.01 0 -1 13 2.42 0.82 0 -1 13 3.03 1.51 0 1 -13 1.79 0.90 0 -1 13 3.66 1.11 0 -1 13 4.66 1.87 0 1 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13.43 1.97 0 2 9 12.13 1.25 0 2 9 12.50 1.67 0 2 9 12.63 1.94 0 2 10 4.49 1.39 0 2 10 4.14 0.95 0 -2 -10 4.96 1.18 0 2 10 5.92 0.95 0 -2 -10 4.52 0.89 0 -2 -10 5.20 0.83 0 2 10 5.84 1.68 0 2 10 4.14 0.92 0 -2 -10 5.49 0.92 0 -2 -11 0.78 1.46 0 2 11 1.29 1.13 0 2 11 1.69 0.92 0 2 11 1.69 1.21 0 -2 -11 3.08 0.89 0 2 11 2.13 1.24 0 -2 -11 2.07 0.71 0 2 11 2.02 0.90 0 -2 -11 2.91 0.90 0 -2 -12 79.89 5.36 0 2 12 79.04 3.90 0 2 12 68.88 4.96 0 -2 -12 75.39 3.58 0 2 12 70.69 3.61 0 -2 -12 73.67 3.72 0 -2 -12 73.13 3.52 0 -2 -12 75.21 3.85 0 2 12 76.76 3.86 0 -2 -12 74.25 3.71 0 2 13 14.72 1.54 0 -2 -13 18.22 2.59 0 -2 -13 16.42 1.48 0 2 13 13.04 1.29 0 -2 -13 13.28 1.24 0 2 13 15.73 2.33 0 -2 -13 14.11 1.50 0 2 13 14.72 1.56 0 -2 -13 15.29 1.45 0 -2 -14 4.54 1.83 0 2 14 8.95 1.23 0 -2 -14 4.45 1.02 0 -2 -14 6.18 1.15 0 2 14 6.09 1.16 0 2 14 6.37 1.17 0 -2 -14 6.13 1.09 0 2 14 5.38 1.94 0 -2 -14 6.05 1.06 0 -2 -15 2.22 0.93 0 2 15 2.86 0.96 0 2 15 1.09 1.63 0 -2 -15 3.05 0.88 0 -2 -15 1.76 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1.50 0.68 0 3 1 0.69 0.49 0 3 2 354.12 14.17 0 -3 -2 358.45 14.17 0 -3 -2 357.21 14.25 0 3 2 373.07 14.32 0 -3 -2 354.20 13.75 0 -3 -3 94.85 4.27 0 -3 -3 88.03 4.34 0 -3 -3 92.27 4.36 0 -3 -3 85.67 4.25 0 3 3 88.16 4.28 0 -3 -3 93.37 3.76 0 -3 -4 11.21 1.21 0 -3 -4 11.72 1.38 0 -3 -4 13.67 1.32 0 3 4 10.70 0.84 0 -3 -4 11.50 0.85 0 3 4 11.82 1.26 0 3 5 35.52 2.32 0 -3 -5 36.15 2.51 0 3 5 33.91 2.43 0 -3 -5 29.79 2.27 0 -3 -5 33.32 2.50 0 -3 -5 38.33 2.48 0 3 5 32.87 1.87 0 -3 -5 34.79 1.75 0 3 5 39.68 2.44 0 -3 -6 9.85 1.62 0 3 6 8.51 1.45 0 3 6 7.76 0.97 0 -3 -6 11.30 1.66 0 -3 -6 8.56 0.86 0 3 6 7.89 1.31 0 3 7 35.12 2.79 0 3 7 34.28 1.92 0 3 7 32.77 2.28 0 -3 -7 35.75 2.82 0 3 7 37.21 2.21 0 -3 -7 38.30 1.94 0 3 7 35.52 2.69 0 3 8 17.89 2.04 0 -3 -8 18.90 2.11 0 3 8 16.65 1.66 0 3 8 18.20 1.56 0 -3 -8 16.12 1.35 0 -3 -8 18.68 1.29 0 3 8 16.94 2.05 0 3 8 15.14 1.91 0 3 9 408.02 16.62 0 -3 -9 436.31 17.43 0 -3 -9 419.17 16.35 0 -3 -9 420.58 16.56 0 3 9 422.10 17.38 0 3 9 427.07 18.29 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33.30 1.94 0 3 17 21.82 1.29 0 -3 -17 21.89 1.22 0 -4 16 2.56 0.65 0 -4 16 1.99 0.59 0 -4 15 4.84 0.93 0 -4 15 3.71 0.72 0 -4 15 3.94 0.83 0 -4 14 80.52 3.70 0 4 -14 75.20 3.58 0 -4 14 76.01 3.65 0 -4 13 13.17 1.48 0 4 -13 14.62 1.46 0 4 -13 11.34 1.24 0 -4 13 11.66 1.45 0 -4 13 11.14 1.36 0 -4 12 28.40 1.97 0 -4 12 33.81 3.59 0 -4 12 33.24 2.25 0 4 -12 27.29 2.01 0 4 -12 25.00 1.71 0 -4 12 30.64 2.13 0 4 -12 27.56 1.96 0 4 -11 14.69 1.37 0 -4 11 14.48 2.63 0 -4 11 14.51 1.64 0 4 -11 18.13 1.69 0 4 -11 17.39 1.51 0 4 -11 7.92 2.06 0 4 -11 14.11 1.31 0 -4 11 14.74 1.58 0 4 -11 17.55 1.57 0 4 -11 15.54 1.57 0 -4 11 14.17 2.47 0 4 -10 243.14 10.29 0 4 -10 260.97 10.59 0 -4 10 269.72 12.60 0 -4 10 257.43 10.63 0 4 -10 251.79 10.33 0 4 -10 264.07 10.52 0 4 -10 262.67 10.54 0 4 -10 260.24 10.57 0 -4 10 235.89 12.00 0 4 -9 10.71 1.23 0 -4 9 12.34 2.31 0 -4 9 10.89 1.36 0 4 -9 11.46 1.33 0 -4 9 7.77 1.66 0 4 -9 8.78 1.06 0 4 -9 11.07 1.18 0 -4 9 8.72 1.07 0 4 -9 9.10 1.80 0 4 -9 10.68 1.28 0 4 -9 9.70 1.21 0 -4 9 6.83 1.92 0 -4 8 100.79 5.21 0 -4 8 101.88 5.28 0 -4 8 95.00 5.77 0 4 -8 91.71 4.33 0 -4 8 93.86 4.40 0 4 -8 78.42 5.38 0 4 -8 95.03 4.31 0 -4 8 86.77 4.60 0 -4 8 95.98 4.12 0 4 -8 86.77 4.27 0 -4 8 99.56 5.54 0 4 -8 92.66 4.33 0 -4 7 42.14 2.94 0 -4 7 34.85 3.17 0 -4 7 34.82 2.68 0 4 -7 41.65 2.20 0 4 -7 37.96 3.09 0 -4 7 38.43 1.98 0 -4 7 38.22 3.00 0 -4 6 15.64 1.99 0 -4 6 15.37 1.82 0 4 -6 12.30 1.67 0 -4 6 13.82 1.82 0 -4 5 17.37 1.99 0 -4 5 18.52 2.03 0 4 -5 16.88 1.81 0 -4 5 17.91 1.84 0 -4 4 344.72 13.97 0 4 -4 334.17 13.97 0 4 -4 323.82 13.06 0 -4 4 347.71 14.00 0 -4 4 335.85 14.00 0 -4 3 376.74 15.52 0 4 -3 381.02 15.51 0 -4 3 383.79 15.51 0 -4 3 377.51 15.54 0 -4 3 375.61 15.49 0 -4 2 10.22 1.46 0 4 -2 8.74 1.24 0 4 -2 10.25 1.21 0 4 -2 8.58 0.97 0 -4 2 8.63 1.34 0 -4 2 9.42 1.40 0 -4 2 11.41 1.46 0 -4 1 64.04 3.48 0 -4 1 67.58 3.43 0 4 -1 65.39 3.42 0 4 -1 65.87 3.47 0 -4 1 66.97 3.53 0 -4 1 63.45 3.47 0 -4 0 171.35 7.48 0 -4 0 178.07 7.46 0 4 0 172.07 6.69 0 4 0 173.82 7.48 0 -4 0 175.95 7.42 0 -4 0 173.76 7.50 0 -4 0 164.86 7.46 0 4 0 163.09 7.14 0 4 1 86.94 3.66 0 4 1 87.07 3.98 0 -4 -1 91.22 4.32 0 4 1 86.80 4.27 0 -4 -1 89.64 4.28 0 -4 -1 96.20 4.40 0 -4 -1 87.96 4.30 0 -4 -1 79.40 4.22 0 4 2 2.36 0.49 0 -4 -2 2.37 0.57 0 4 2 3.15 0.88 0 -4 -2 2.19 0.79 0 -4 -2 2.67 0.92 0 -4 -2 2.97 1.09 0 4 3 752.24 28.58 0 -4 -3 735.58 28.57 0 4 3 782.44 29.41 0 -4 -3 724.88 29.15 0 -4 -3 759.59 29.35 0 -4 -3 755.94 29.33 0 -4 -3 747.70 29.38 0 4 4 54.41 2.51 0 4 4 55.00 3.01 0 4 4 53.72 2.35 0 -4 -4 53.39 2.51 0 4 4 57.82 3.30 0 -4 -4 55.07 3.34 0 -4 -4 55.92 3.26 0 -4 -4 51.99 3.18 0 -4 -4 58.17 3.40 0 4 5 9.05 1.47 0 4 5 9.48 0.89 0 -4 -5 9.58 1.64 0 -4 -5 11.47 0.94 0 4 5 10.54 1.51 0 -4 -5 10.93 1.73 0 4 5 9.09 0.80 0 -4 -5 11.54 1.54 0 -4 -6 45.94 3.20 0 4 6 48.41 3.29 0 -4 -6 46.96 3.28 0 -4 -6 49.14 3.25 0 -4 -6 48.41 2.39 0 4 6 50.52 3.33 0 4 7 107.48 6.02 0 -4 -7 115.43 5.94 0 4 7 108.48 5.06 0 -4 -7 117.24 6.05 0 4 7 110.82 6.07 0 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5 -4 23.64 2.08 0 -5 4 21.90 2.28 0 -5 4 24.96 2.27 0 5 -4 20.95 1.55 0 5 -3 23.96 1.33 0 -5 3 23.02 2.24 0 5 -3 24.54 2.05 0 -5 3 19.23 2.10 0 5 -3 28.04 1.71 0 -5 3 21.11 2.21 0 -5 2 147.58 7.21 0 5 -2 156.91 6.23 0 5 -2 147.50 7.22 0 5 -2 152.94 7.14 0 -5 2 152.78 7.23 0 -5 2 157.22 7.29 0 5 -2 156.59 6.62 0 -5 1 32.74 2.52 0 -5 1 29.85 2.33 0 5 -1 34.55 2.35 0 5 -1 29.87 2.36 0 -5 1 34.37 2.57 0 -5 1 32.01 2.53 0 5 -1 33.53 2.01 0 -5 1 36.18 2.43 0 -5 0 1.86 1.20 0 -5 0 0.39 1.09 0 5 0 1.09 0.60 0 5 0 1.56 0.57 0 5 0 1.78 0.90 0 5 0 0.76 0.44 0 -5 0 1.06 0.45 0 5 0 1.62 0.64 0 -5 0 1.33 1.21 0 -5 0 1.43 0.97 0 -5 0 0.83 1.14 0 5 1 98.13 4.20 0 -5 -1 91.27 4.95 0 5 1 104.20 5.06 0 -5 -1 102.87 4.14 0 -5 -1 101.09 5.11 0 -5 -1 99.85 5.07 0 -5 -1 98.34 4.95 0 -5 -1 95.46 5.02 0 5 2 241.91 9.78 0 5 2 260.77 10.74 0 -5 -2 245.98 10.71 0 -5 -2 247.61 10.63 0 -5 -2 251.68 10.65 0 5 3 84.29 4.02 0 5 3 85.07 3.72 0 -5 -3 86.82 4.65 0 -5 -3 85.32 4.55 0 -5 -3 83.00 4.59 0 5 3 86.44 4.55 0 5 4 17.16 1.20 0 -5 -4 16.45 2.01 0 -5 -4 13.42 1.86 0 -5 -4 18.19 1.86 0 -5 -4 16.20 1.83 0 -5 -4 17.63 1.21 0 5 4 18.47 1.88 0 5 4 19.33 1.68 0 5 5 18.46 1.99 0 5 5 18.76 1.30 0 -5 -5 21.77 2.22 0 -5 -5 23.01 2.17 0 5 5 23.20 2.18 0 -5 -5 18.49 1.33 0 5 5 20.29 1.87 0 5 6 34.53 1.92 0 5 6 34.51 2.78 0 -5 -6 34.01 1.95 0 5 6 30.29 2.73 0 -5 -6 35.31 2.88 0 -5 -6 35.78 2.86 0 -5 -7 17.06 1.31 0 -5 -7 17.95 2.18 0 5 7 17.78 2.15 0 -5 -7 14.60 2.11 0 -5 -7 17.20 1.33 0 5 7 19.28 2.18 0 -5 -8 84.54 5.02 0 5 8 88.95 5.33 0 5 8 77.07 3.82 0 5 8 76.63 5.08 0 -5 -8 85.20 3.87 0 5 8 77.40 3.83 0 -5 -9 96.67 4.46 0 5 9 99.98 6.11 0 5 9 92.18 4.36 0 -5 -9 111.49 6.02 0 -5 -9 97.04 4.26 0 5 9 95.94 5.41 0 5 9 89.04 4.47 0 -5 -9 100.94 4.51 0 5 9 88.06 5.87 0 5 9 93.15 4.50 0 5 9 90.12 5.98 0 5 9 96.69 4.29 0 -5 -10 386.78 14.79 0 5 10 382.31 15.04 0 -5 -10 351.81 15.69 0 5 10 363.34 16.10 0 -5 -10 375.30 14.65 0 5 10 366.75 14.81 0 5 10 376.02 17.11 0 -5 -10 366.34 14.88 0 5 10 365.93 14.97 0 5 10 390.82 14.99 0 5 10 382.96 17.22 0 5 10 352.01 14.65 0 -5 -11 13.53 1.22 0 -5 -11 16.77 1.58 0 5 11 16.13 1.45 0 5 11 14.52 1.51 0 5 11 10.80 1.86 0 -5 -11 18.31 1.64 0 5 11 13.79 2.45 0 5 11 17.08 1.54 0 -5 -12 2.51 1.02 0 5 12 0.26 0.85 0 -5 -12 3.58 1.73 0 5 12 1.22 0.88 0 5 12 0.32 0.93 0 -5 -12 2.34 0.98 0 5 12 0.24 1.29 0 -5 -12 2.04 0.92 0 5 12 1.90 1.42 0 5 12 0.92 0.94 0 5 13 15.68 1.41 0 5 13 13.57 1.39 0 -5 -13 17.63 2.43 0 -5 -13 16.69 1.55 0 5 13 15.08 1.49 0 -5 -13 11.26 1.15 0 -5 -13 16.36 1.55 0 -5 -13 15.89 1.43 0 5 13 15.86 1.51 0 5 14 11.40 1.18 0 -5 -14 13.84 1.37 0 5 14 15.31 1.44 0 5 14 12.29 1.27 0 -5 -14 15.61 1.36 0 -5 -15 60.53 2.83 0 5 15 51.99 2.88 0 5 16 5.49 0.83 0 -5 -16 6.15 0.82 0 -5 -16 4.92 0.75 0 5 17 24.95 1.39 0 -6 15 3.96 0.61 0 6 -15 3.31 0.55 0 6 -14 4.46 0.65 0 -6 14 4.33 0.82 0 6 -14 5.89 0.83 0 -6 14 5.50 0.84 0 6 -13 29.06 1.88 0 -6 13 33.52 2.08 0 -6 13 33.66 2.06 0 -6 12 6.62 1.14 0 6 -12 4.77 0.97 0 6 -12 6.62 0.95 0 6 -12 6.49 1.00 0 -6 12 4.45 1.02 0 -6 12 5.11 1.11 0 -6 11 20.73 1.78 0 6 -11 19.03 1.64 0 6 -11 23.83 1.85 0 6 -11 22.27 1.73 0 -6 11 20.41 1.83 0 -6 11 20.52 1.77 0 6 -11 23.60 1.78 0 6 -10 24.15 1.85 0 -6 10 29.72 2.10 0 -6 10 29.50 2.11 0 6 -10 29.46 2.10 0 6 -10 29.24 2.00 0 -6 10 25.67 3.27 0 6 -10 29.95 2.01 0 -6 10 26.44 2.07 0 6 -10 29.00 2.02 0 -6 10 25.17 2.04 0 -6 9 42.56 2.63 0 -6 9 41.49 4.01 0 -6 9 37.11 3.41 0 -6 9 41.76 2.60 0 6 -9 39.28 2.59 0 6 -9 38.16 2.46 0 6 -9 36.88 2.46 0 6 -9 45.80 2.61 0 -6 9 41.71 2.66 0 -6 9 44.38 2.66 0 -6 8 12.98 2.12 0 -6 8 13.52 1.96 0 -6 8 16.71 2.37 0 6 -8 13.94 1.39 0 -6 8 14.51 2.34 0 6 -8 13.50 1.47 0 6 -8 15.45 1.42 0 6 -8 13.58 1.44 0 -6 8 15.01 1.50 0 -6 8 15.13 1.57 0 -6 7 12.53 2.16 0 -6 7 6.66 1.90 0 -6 7 10.66 1.84 0 6 -7 9.76 1.28 0 6 -7 10.51 1.19 0 6 -7 7.76 1.07 0 -6 7 9.23 1.21 0 -6 7 8.08 1.29 0 6 -7 11.49 1.26 0 6 -6 64.59 3.34 0 -6 6 61.18 3.95 0 6 -6 68.33 3.41 0 -6 6 61.90 4.45 0 -6 6 71.40 4.72 0 -6 6 65.58 3.36 0 -6 6 64.18 4.32 0 6 -6 67.49 3.38 0 -6 6 65.00 3.38 0 -6 6 69.77 3.42 0 6 -6 73.79 3.44 0 -6 5 60.48 3.74 0 -6 5 59.32 4.08 0 6 -5 59.08 3.03 0 -6 5 62.93 4.25 0 6 -5 53.06 3.89 0 6 -5 60.92 3.02 0 -6 5 61.24 3.06 0 6 -5 57.93 3.00 0 -6 4 33.64 2.80 0 -6 4 27.70 2.39 0 6 -4 29.35 2.53 0 6 -4 28.41 1.72 0 6 -4 25.35 1.80 0 -6 4 29.45 2.78 0 6 -4 29.44 1.82 0 6 -3 0.36 0.49 0 -6 3 0.74 1.20 0 6 -3 0.71 0.80 0 6 -3 0.41 0.49 0 -6 3 -0.29 1.24 0 -6 3 0.31 1.25 0 -6 2 28.25 2.60 0 6 -2 34.40 1.75 0 6 -2 33.21 2.65 0 6 -2 28.34 2.41 0 -6 2 30.54 2.64 0 -6 2 29.31 2.72 0 -6 2 33.38 2.61 0 6 -2 34.71 2.07 0 -6 1 86.42 4.87 0 -6 1 76.64 4.57 0 6 -1 91.41 4.87 0 6 -1 86.72 4.69 0 -6 1 85.90 4.86 0 -6 1 90.29 4.73 0 -6 1 78.84 4.74 0 -6 0 37.11 2.94 0 6 0 42.25 2.16 0 6 0 46.21 3.08 0 6 0 45.49 2.99 0 -6 0 43.29 2.06 0 6 0 40.35 2.38 0 -6 0 42.67 3.10 0 -6 0 47.58 3.14 0 -6 0 44.88 3.02 0 -6 0 42.03 3.11 0 6 1 73.90 3.38 0 -6 -1 72.37 3.42 0 -6 -1 78.44 3.29 0 6 1 76.43 4.37 0 6 1 74.87 3.63 0 -6 -1 72.12 4.26 0 -6 -1 74.47 4.33 0 6 2 24.71 1.51 0 -6 -2 23.23 1.55 0 6 2 23.75 2.21 0 -6 -2 24.83 1.41 0 -6 -2 26.30 2.32 0 -6 -2 24.34 2.04 0 -6 -2 25.77 2.44 0 6 3 108.15 4.86 0 -6 -3 109.66 4.86 0 -6 -3 112.81 5.99 0 -6 -3 111.56 5.86 0 -6 -3 118.35 5.94 0 6 3 122.02 6.01 0 -6 -3 116.46 4.81 0 -6 -4 64.63 3.16 0 6 4 68.84 3.22 0 -6 -4 66.03 3.78 0 -6 -4 65.43 4.16 0 -6 -4 65.59 4.25 0 -6 -4 64.59 4.13 0 6 4 76.80 4.35 0 6 4 72.17 3.84 0 6 5 77.08 3.60 0 -6 -5 74.21 4.24 0 -6 -5 76.12 4.68 0 -6 -5 73.52 4.65 0 6 5 85.62 4.83 0 6 5 74.83 4.28 0 6 6 13.50 1.99 0 6 6 13.40 1.25 0 -6 -6 15.08 1.79 0 6 6 15.67 1.32 0 -6 -6 15.39 1.39 0 -6 -6 17.56 2.25 0 -6 -6 15.48 2.24 0 6 6 15.84 2.07 0 -6 -6 16.84 1.23 0 6 6 15.17 1.26 0 6 6 17.33 1.90 0 6 7 224.04 9.20 0 6 7 232.65 10.89 0 6 7 223.45 9.33 0 -6 -7 248.01 11.00 0 6 7 227.12 10.96 0 -6 -7 227.79 9.17 0 6 7 227.15 10.47 0 6 7 212.70 9.26 0 6 8 16.49 1.47 0 6 8 15.28 2.31 0 6 8 13.35 2.22 0 -6 -8 17.38 1.43 0 6 8 15.82 2.18 0 6 8 14.36 1.36 0 -6 -9 8.54 1.03 0 -6 -9 6.95 1.18 0 6 9 6.82 1.11 0 6 9 9.52 2.09 0 6 9 8.38 1.19 0 6 9 5.52 1.37 0 -6 -9 7.07 1.10 0 6 9 7.19 1.72 0 6 9 7.48 1.89 0 6 9 7.65 1.15 0 6 10 0.88 0.84 0 -6 -10 0.62 1.02 0 -6 -10 1.71 0.79 0 -6 -10 0.30 1.04 0 6 10 1.74 1.00 0 6 10 1.85 1.01 0 -6 -10 1.52 0.96 0 6 10 1.59 1.66 0 6 10 1.51 0.69 0 6 10 1.85 0.93 0 6 11 9.68 1.13 0 -6 -11 7.68 0.97 0 -6 -11 7.83 1.23 0 -6 -11 8.73 1.17 0 -6 -11 7.90 1.09 0 6 11 9.10 1.26 0 6 11 9.23 2.03 0 6 11 7.60 1.99 0 6 11 11.03 1.28 0 -6 -12 3.86 0.90 0 6 12 2.71 0.97 0 -6 -12 3.37 1.67 0 -6 -12 2.93 1.07 0 -6 -12 2.88 0.91 0 6 12 3.33 1.03 0 -6 -13 41.24 2.36 0 -6 -13 48.56 2.52 0 6 13 48.33 2.74 0 6 13 46.99 2.61 0 -6 -13 51.22 2.70 0 6 13 47.96 2.71 0 -6 -13 49.01 2.59 0 -6 -14 4.52 0.94 0 6 14 2.72 0.89 0 -6 -14 3.07 0.88 0 -6 -14 3.31 0.82 0 6 14 2.70 0.92 0 6 14 6.42 1.72 0 6 15 4.44 0.82 0 -6 -15 2.58 0.75 0 6 16 10.61 0.97 0 -6 -16 12.60 0.92 0 -6 -16 11.30 0.86 0 -7 14 2.67 0.58 0 7 -14 3.59 0.57 0 -7 13 1.13 0.67 0 7 -13 -0.24 0.63 0 -7 13 -0.08 0.72 0 7 -12 3.94 0.91 0 7 -12 3.98 0.74 0 -7 12 3.40 0.93 0 7 -12 3.87 0.80 0 -7 12 3.39 0.98 0 -7 11 11.43 1.32 0 -7 11 11.78 1.28 0 7 -11 9.57 1.06 0 7 -11 10.72 1.16 0 -7 11 9.83 1.21 0 -7 11 10.55 1.30 0 7 -11 9.77 1.15 0 -7 10 75.68 3.79 0 7 -10 64.42 3.52 0 7 -10 74.88 3.75 0 -7 10 77.61 3.83 0 -7 10 75.08 3.80 0 7 -10 71.81 3.56 0 7 -10 74.35 3.69 0 -7 9 15.70 1.67 0 7 -9 15.97 1.44 0 7 -9 14.26 2.28 0 7 -9 18.64 1.59 0 7 -9 19.23 1.57 0 7 -9 19.23 1.63 0 -7 9 16.74 1.73 0 -7 9 16.47 1.61 0 -7 8 1.40 1.55 0 7 -8 3.93 0.93 0 -7 8 3.63 1.18 0 7 -8 3.00 1.40 0 7 -8 4.03 0.92 0 -7 8 2.11 1.01 0 7 -8 3.89 1.07 0 -7 8 3.19 1.13 0 7 -8 3.19 0.92 0 7 -7 4.27 1.08 0 7 -7 3.95 0.93 0 -7 7 4.48 1.05 0 -7 7 5.70 1.22 0 7 -7 5.44 1.01 0 7 -7 4.46 1.39 0 7 -7 4.36 1.01 0 -7 7 7.14 1.11 0 -7 7 4.41 1.14 0 7 -6 1.33 0.94 0 -7 6 1.44 1.52 0 -7 6 1.44 1.58 0 -7 6 0.08 0.94 0 -7 6 0.71 0.86 0 7 -6 0.91 0.72 0 7 -6 -0.21 0.91 0 -7 6 0.22 0.98 0 -7 6 0.37 0.84 0 7 -6 0.80 0.88 0 -7 5 5.40 1.73 0 7 -5 5.48 1.07 0 -7 5 4.47 1.34 0 7 -5 4.36 0.88 0 -7 5 4.02 1.67 0 -7 5 3.70 1.06 0 7 -5 3.70 1.31 0 7 -5 5.08 0.87 0 7 -5 5.65 1.02 0 -7 4 15.42 2.23 0 -7 4 12.05 1.37 0 -7 4 12.59 1.94 0 -7 4 12.64 2.11 0 7 -4 14.49 1.06 0 7 -4 16.53 1.34 0 7 -4 15.62 1.42 0 -7 4 12.01 1.83 0 7 -4 17.05 1.39 0 7 -4 15.24 1.37 0 7 -3 232.35 9.58 0 -7 3 245.15 11.19 0 -7 3 227.91 10.92 0 -7 3 233.93 10.52 0 7 -3 232.11 9.32 0 -7 3 239.57 10.65 0 7 -3 224.58 9.55 0 7 -2 14.05 1.11 0 -7 2 11.69 1.99 0 -7 2 15.11 2.14 0 -7 2 15.72 2.05 0 7 -2 14.95 1.14 0 7 -2 14.49 1.33 0 -7 1 12.26 1.97 0 7 -1 11.07 0.93 0 7 -1 9.24 1.60 0 7 -1 11.87 1.15 0 -7 0 3.70 0.92 0 -7 0 4.52 1.31 0 7 0 2.50 0.53 0 7 0 2.85 1.17 0 7 0 3.42 0.82 0 -7 -1 46.64 2.55 0 7 1 47.92 2.51 0 7 1 51.91 2.62 0 -7 -1 48.14 3.09 0 -7 -1 48.35 3.43 0 -7 -1 50.26 3.61 0 -7 -1 50.72 2.38 0 7 1 55.00 3.67 0 7 1 44.83 2.55 0 -7 -2 66.00 3.20 0 7 2 68.29 3.25 0 7 2 64.53 3.18 0 7 2 63.31 4.20 0 -7 -2 66.79 3.04 0 -7 -2 65.16 4.20 0 -7 -2 60.65 4.21 0 -7 -2 59.35 3.74 0 7 3 293.75 11.99 0 -7 -3 301.12 11.95 0 7 3 284.69 11.95 0 7 3 305.35 12.83 0 -7 -3 306.99 13.37 0 -7 -3 297.08 12.83 0 -7 -3 304.50 13.41 0 7 3 291.08 13.32 0 -7 -3 302.65 11.84 0 7 4 47.20 2.52 0 7 4 43.25 2.46 0 7 4 45.28 2.46 0 -7 -4 44.71 2.46 0 7 4 48.95 3.29 0 -7 -4 45.60 3.02 0 -7 -4 43.93 3.47 0 -7 -4 43.14 3.46 0 7 4 44.53 3.47 0 -7 -4 44.10 2.33 0 7 4 43.13 2.90 0 -7 -5 10.58 1.89 0 7 5 5.74 0.96 0 7 5 3.11 1.32 0 -7 -5 9.19 1.44 0 7 5 5.97 0.97 0 -7 -5 7.10 1.60 0 -7 -5 8.69 1.86 0 7 5 6.43 1.57 0 -7 -5 9.93 0.97 0 7 5 7.87 1.33 0 7 6 5.34 0.94 0 7 6 4.12 0.93 0 -7 -6 4.83 1.68 0 -7 -6 4.15 1.06 0 7 6 5.45 0.89 0 -7 -6 4.18 1.46 0 -7 -6 5.54 1.88 0 7 6 4.63 1.48 0 7 6 5.72 1.29 0 7 6 5.73 0.96 0 7 7 21.82 1.67 0 7 7 21.65 1.63 0 -7 -7 21.32 2.72 0 -7 -7 18.30 1.67 0 7 7 20.70 1.59 0 -7 -7 21.55 1.51 0 7 7 22.57 1.63 0 7 7 20.76 2.26 0 7 8 52.51 2.94 0 7 8 49.56 2.78 0 -7 -8 53.65 2.75 0 7 8 48.68 3.77 0 7 8 54.28 2.91 0 7 9 55.60 3.01 0 7 9 63.60 3.28 0 -7 -9 60.25 3.00 0 -7 -9 59.44 3.15 0 7 9 56.83 4.62 0 -7 -9 56.16 3.04 0 7 9 60.15 3.21 0 7 9 58.87 4.81 0 7 10 105.76 5.06 0 -7 -10 119.96 5.10 0 -7 -10 117.63 5.31 0 7 10 121.45 5.40 0 -7 -10 120.53 5.27 0 7 10 103.08 6.95 0 7 10 111.20 5.07 0 7 10 126.20 7.58 0 7 10 113.69 5.40 0 -7 -11 6.57 0.92 0 -7 -11 8.26 1.21 0 7 11 8.69 1.17 0 -7 -11 9.17 0.99 0 -7 -11 6.07 1.07 0 7 11 6.28 0.83 0 -7 -12 1.71 0.93 0 7 12 1.48 0.89 0 -7 -12 0.79 0.78 0 -7 -12 0.79 0.75 0 -7 -13 0.47 0.63 0 -7 -13 3.02 0.89 0 -7 -13 1.92 0.78 0 -7 -14 15.11 1.27 0 7 14 15.74 1.21 0 -7 -14 16.99 1.22 0 7 16 14.94 1.08 0 -7 -16 22.54 1.08 0 8 -13 9.68 0.82 0 8 -12 10.77 1.05 0 -8 12 9.76 1.02 0 8 -11 11.51 1.19 0 -8 11 10.95 1.18 0 -8 11 10.09 1.19 0 -8 10 3.45 1.00 0 8 -10 3.55 0.99 0 8 -10 2.35 0.79 0 -8 10 4.60 1.07 0 -8 9 0.51 0.99 0 -8 9 -0.19 0.86 0 8 -9 1.63 0.96 0 8 -9 1.09 0.74 0 8 -9 0.93 0.77 0 8 -9 1.85 0.77 0 -8 9 1.70 1.08 0 -8 8 4.26 1.15 0 8 -8 6.22 1.14 0 -8 8 7.15 1.15 0 8 -8 3.86 0.83 0 8 -8 6.89 1.07 0 -8 8 5.17 1.23 0 -8 7 124.59 5.56 0 8 -7 128.02 5.61 0 -8 7 109.76 5.29 0 8 -7 119.70 5.42 0 -8 7 121.12 5.49 0 8 -6 11.11 1.17 0 -8 6 13.52 1.52 0 -8 6 13.66 1.37 0 -8 6 11.87 1.98 0 8 -6 13.92 1.36 0 8 -6 12.73 2.05 0 -8 6 14.77 1.54 0 -8 5 37.89 2.45 0 8 -5 40.02 2.25 0 -8 5 41.24 3.38 0 -8 5 34.65 3.54 0 -8 5 33.87 2.16 0 8 -5 32.83 3.19 0 8 -4 6.42 1.03 0 -8 4 7.68 1.22 0 -8 4 6.90 1.63 0 8 -4 5.05 1.10 0 -8 4 5.09 1.55 0 -8 4 4.01 1.84 0 8 -4 6.03 1.47 0 8 -4 6.19 1.05 0 8 -3 0.93 0.59 0 -8 3 -0.54 1.24 0 8 -3 1.78 0.86 0 -8 3 0.94 1.47 0 8 -3 0.74 0.67 0 8 -3 0.38 0.88 0 8 -3 0.92 0.82 0 -8 2 33.98 2.26 0 8 -2 37.51 2.08 0 8 -2 36.37 2.19 0 -8 2 34.73 3.10 0 -8 2 32.57 3.07 0 8 -2 38.55 2.06 0 8 -2 41.64 3.21 0 8 -2 37.34 2.26 0 8 -1 79.80 3.77 0 8 -1 83.64 3.95 0 -8 1 79.55 3.94 0 -8 1 81.42 5.11 0 -8 1 79.97 4.82 0 -8 1 80.04 4.41 0 8 -1 74.15 3.55 0 8 -1 86.64 5.09 0 -8 1 80.70 3.97 0 8 -1 81.51 3.94 0 8 0 817.60 31.37 0 -8 0 793.48 31.40 0 -8 0 823.97 31.55 0 8 0 822.56 31.59 0 -8 0 820.17 32.25 0 -8 0 819.27 32.69 0 8 0 843.56 33.07 0 8 0 831.90 33.34 0 8 0 796.70 31.56 0 8 1 39.82 2.46 0 -8 -1 42.76 2.58 0 8 1 38.64 2.39 0 8 1 39.82 2.38 0 -8 -1 42.85 3.54 0 -8 -1 46.71 3.62 0 -8 -1 43.06 3.01 0 8 1 46.24 3.45 0 8 1 40.67 3.47 0 8 1 42.39 2.30 0 -8 -2 17.76 1.60 0 8 2 18.00 1.54 0 8 2 19.54 1.54 0 8 2 20.66 1.57 0 8 2 16.34 1.44 0 -8 -2 15.88 1.92 0 -8 -2 20.96 2.38 0 -8 -2 15.23 2.39 0 -8 -2 18.87 1.29 0 8 2 17.63 2.34 0 8 2 15.32 2.01 0 8 2 18.62 1.35 0 8 3 1.73 0.82 0 8 3 0.74 0.80 0 -8 -3 1.16 0.98 0 -8 -3 0.95 0.94 0 8 3 1.08 0.79 0 -8 -3 2.92 1.49 0 8 3 -0.41 1.25 0 -8 -3 0.77 0.54 0 8 3 0.76 0.59 0 -8 -4 122.84 6.21 0 8 4 123.49 5.60 0 -8 -4 129.90 5.62 0 8 4 117.19 6.43 0 8 4 127.91 5.67 0 8 4 121.56 5.65 0 -8 -4 129.30 5.46 0 -8 -4 123.05 7.07 0 8 5 3.09 0.98 0 -8 -5 1.53 1.51 0 -8 -5 3.14 1.19 0 8 5 0.17 1.28 0 8 5 2.74 0.97 0 -8 -5 3.20 1.09 0 8 5 2.19 0.90 0 -8 -5 3.07 0.75 0 -8 -5 3.64 1.14 0 -8 -5 1.49 1.47 0 -8 -5 3.16 1.89 0 -8 -6 135.08 7.19 0 8 6 136.73 6.15 0 8 6 137.17 7.45 0 -8 -6 135.49 7.65 0 -8 -6 143.09 7.95 0 -8 -6 145.59 6.14 0 8 6 132.63 5.91 0 -8 -6 131.94 5.96 0 8 7 17.49 2.42 0 -8 -7 21.96 2.64 0 8 7 24.67 1.85 0 -8 -7 23.50 1.83 0 -8 -7 25.75 3.03 0 8 7 21.98 1.64 0 8 7 20.28 2.69 0 -8 -7 20.69 1.59 0 8 7 18.46 2.13 0 -8 -7 22.99 1.53 0 8 7 23.36 1.76 0 -8 -8 27.29 1.93 0 8 8 24.62 1.95 0 8 8 24.47 1.85 0 -8 -8 31.07 2.05 0 8 8 26.90 1.87 0 8 8 24.59 2.95 0 -8 -8 25.21 1.80 0 8 8 23.36 1.86 0 8 9 2.88 0.91 0 -8 -9 3.10 0.83 0 -8 -9 4.26 1.05 0 8 9 2.65 0.98 0 -8 -9 1.60 1.09 0 8 9 3.60 1.49 0 -8 -9 0.92 0.70 0 8 9 1.79 0.92 0 8 9 1.35 1.52 0 8 9 4.00 0.97 0 -8 -10 0.26 0.88 0 -8 -10 -0.67 0.71 0 -8 -10 -0.07 0.67 0 8 10 1.00 0.80 0 8 10 0.73 0.60 0 8 10 0.44 0.75 0 -8 -11 23.43 1.49 0 -8 -11 19.24 1.61 0 8 11 21.40 1.42 0 8 12 23.31 1.68 0 -8 -12 23.89 1.60 0 -8 -13 5.63 0.69 0 -8 -13 3.87 0.86 0 8 14 2.74 0.64 0 8 15 2.18 0.47 0 9 -12 29.68 1.50 0 -9 12 28.69 1.48 0 -9 11 1.09 0.60 0 9 -11 0.79 0.60 0 -9 11 0.60 0.66 0 -9 10 25.02 1.57 0 9 -10 30.12 1.78 0 -9 10 30.48 1.81 0 -9 9 0.18 0.67 0 9 -9 0.98 0.78 0 9 -9 1.23 0.82 0 -9 9 1.21 0.86 0 -9 9 1.76 0.97 0 -9 8 0.45 0.81 0 9 -8 0.97 0.83 0 -9 8 1.98 1.01 0 9 -8 1.39 0.94 0 -9 8 1.03 1.01 0 9 -8 0.33 0.77 0 -9 7 17.10 1.41 0 -9 7 15.96 1.50 0 -9 7 18.13 1.67 0 9 -7 19.89 1.73 0 -9 7 16.81 1.61 0 -9 6 6.34 1.22 0 -9 5 9.34 1.38 0 9 -5 8.95 1.10 0 9 -5 10.81 1.28 0 9 -5 10.03 1.75 0 9 -5 8.85 1.07 0 9 -5 9.73 1.25 0 -9 4 81.47 4.09 0 9 -4 82.96 3.99 0 9 -4 93.79 4.33 0 -9 4 86.08 5.28 0 9 -4 82.39 4.06 0 9 -4 78.12 3.88 0 9 -4 68.77 5.05 0 9 -4 82.99 4.07 0 -9 3 1.82 1.16 0 9 -3 1.31 0.62 0 9 -3 1.19 1.08 0 -9 3 1.15 1.47 0 -9 3 1.76 1.47 0 9 -3 0.48 0.85 0 9 -3 4.87 1.32 0 9 -3 0.23 0.65 0 -9 3 1.76 1.23 0 9 -3 1.65 0.90 0 9 -2 29.26 1.79 0 9 -2 31.66 2.20 0 -9 2 28.41 2.07 0 -9 2 33.80 3.10 0 -9 2 28.99 2.95 0 9 -2 25.47 1.86 0 9 -2 27.47 1.70 0 9 -2 31.10 2.88 0 9 -2 26.64 1.96 0 -9 2 28.40 2.14 0 9 -1 30.45 2.08 0 9 -1 26.61 1.77 0 -9 1 23.70 1.81 0 9 -1 26.03 1.91 0 -9 1 24.79 1.97 0 -9 1 25.28 2.85 0 -9 1 22.76 2.48 0 -9 1 28.26 2.90 0 9 -1 27.31 2.72 0 -9 1 23.80 1.97 0 -9 0 2.39 1.10 0 -9 0 4.16 0.99 0 9 0 2.97 0.80 0 9 0 5.63 1.09 0 -9 0 2.63 1.56 0 -9 0 4.25 1.64 0 9 0 3.32 1.15 0 -9 0 2.68 1.18 0 9 0 3.51 0.80 0 9 1 22.20 1.61 0 -9 -1 22.66 1.87 0 9 1 23.56 1.80 0 -9 -1 16.97 2.51 0 9 1 19.38 2.34 0 9 1 21.09 1.55 0 9 2 75.52 3.81 0 9 2 80.81 3.85 0 -9 -2 75.14 3.84 0 9 2 76.12 3.72 0 9 2 77.90 3.88 0 -9 -2 71.40 4.91 0 9 2 76.95 4.97 0 9 2 73.57 3.60 0 -9 -3 25.06 1.96 0 9 3 24.27 1.88 0 9 3 28.41 2.04 0 9 3 28.10 1.97 0 -9 -3 24.98 2.89 0 9 3 28.60 2.83 0 9 3 28.83 1.85 0 9 4 35.79 2.36 0 9 4 36.44 2.22 0 -9 -4 41.31 3.12 0 -9 -4 36.69 2.36 0 9 4 36.04 2.34 0 -9 -4 43.11 3.78 0 -9 -4 35.13 2.36 0 9 4 30.77 3.13 0 -9 -4 31.65 1.98 0 9 4 35.60 2.17 0 -9 -4 37.89 2.26 0 -9 -5 14.32 1.47 0 9 5 14.50 1.39 0 9 5 11.70 1.38 0 -9 -5 13.62 2.08 0 9 5 10.63 1.20 0 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13 1.27 0.74 1 -5 13 1.37 1.00 -1 5 -13 1.20 0.81 1 -5 13 0.46 0.79 1 -5 14 40.62 2.20 -1 5 -14 32.36 1.89 1 -5 14 34.00 1.85 -1 5 -14 42.06 2.10 1 -5 15 0.55 0.62 -1 5 -15 0.60 0.54 -1 5 -16 2.42 0.44 1 -5 16 2.15 0.45 1 -4 -16 99.51 4.24 1 -4 -16 98.44 4.17 1 -4 -15 11.99 1.18 -1 4 15 14.46 1.25 1 -4 -15 13.91 1.17 -1 4 15 10.35 2.01 -1 4 15 11.14 1.23 1 -4 -14 27.58 1.67 -1 4 14 31.82 2.06 1 -4 -14 30.95 2.09 1 -4 -14 31.79 1.93 1 -4 -14 30.13 1.81 -1 4 14 33.04 2.08 1 -4 -13 6.34 1.16 1 -4 -13 9.28 1.86 1 -4 -13 6.97 0.97 -1 4 13 8.24 1.17 1 -4 -13 8.97 1.25 1 -4 -13 7.86 1.11 -1 4 13 6.31 1.18 -1 4 12 2.63 0.85 1 -4 -12 1.35 0.98 1 -4 -12 1.60 1.53 -1 4 12 1.97 0.92 -1 4 12 2.31 1.40 1 -4 -12 0.91 0.77 1 -4 -12 1.89 0.77 -1 4 12 1.30 1.37 1 -4 -12 1.49 0.95 -1 4 12 1.26 1.03 1 -4 -12 1.53 0.88 -1 4 11 32.71 3.57 1 -4 -11 40.36 2.39 1 -4 -11 36.68 3.27 1 -4 -11 34.07 2.14 -1 4 11 31.31 3.25 -1 4 11 34.43 2.35 1 -4 -11 36.95 2.39 -1 4 11 33.96 3.61 -1 4 11 37.48 3.71 -1 4 11 37.37 2.38 -1 4 11 34.59 3.56 1 -4 -10 136.89 6.91 -1 4 10 138.70 7.68 1 -4 -10 127.79 5.63 1 -4 -10 124.52 5.45 -1 4 10 113.24 6.35 -1 4 10 120.12 5.52 1 -4 -10 127.30 5.49 -1 4 10 122.10 5.70 -1 4 10 105.34 6.77 -1 4 10 112.86 7.31 1 -4 -10 133.07 5.74 -1 4 10 126.89 7.38 -1 4 10 124.62 5.66 -1 4 10 118.50 7.36 -1 4 9 503.19 20.38 -1 4 9 506.38 21.46 1 -4 -9 490.25 19.27 -1 4 9 492.65 19.38 1 -4 -9 501.58 19.41 -1 4 9 483.72 19.49 1 -4 -9 504.52 19.28 -1 4 9 466.85 20.13 1 -4 -9 516.49 19.52 1 -4 -9 480.58 19.21 -1 4 9 469.14 21.40 -1 4 9 491.66 19.47 -1 4 9 494.32 21.39 -1 4 9 486.48 21.22 1 -4 -8 10.34 1.16 -1 4 8 12.49 2.06 -1 4 8 8.16 1.11 -1 4 8 10.52 1.41 1 -4 -8 11.25 1.23 -1 4 8 8.28 1.78 1 -4 -8 11.10 1.21 -1 4 8 10.52 1.13 -1 4 8 13.97 1.99 -1 4 7 7.34 1.43 -1 4 7 9.31 0.92 -1 4 7 10.73 1.81 -1 4 7 7.94 1.11 -1 4 7 10.32 1.83 1 -4 -7 7.85 1.02 -1 4 7 9.36 1.63 -1 4 6 23.37 1.75 1 -4 -6 25.21 1.57 -1 4 6 21.18 2.29 -1 4 6 23.21 2.22 1 -4 -5 29.47 1.74 -1 4 5 32.34 2.66 1 -4 -5 31.37 2.60 -1 4 4 23.97 2.14 1 -4 -4 26.83 1.58 -1 4 4 27.50 1.54 -1 4 4 26.88 1.49 -1 4 4 27.82 2.34 1 -4 -4 27.69 2.33 1 -4 -4 27.11 2.26 -1 4 3 267.33 11.59 -1 4 3 276.61 10.77 -1 4 3 287.96 11.83 1 -4 -3 256.90 11.49 1 -4 -3 275.04 11.58 -1 4 2 274.88 10.91 -1 4 2 279.01 11.62 -1 4 2 274.16 11.80 1 -4 -2 285.44 10.93 -1 4 2 268.09 11.62 -1 4 2 275.62 11.70 1 -4 -2 280.03 11.59 -1 4 1 106.53 4.50 -1 4 1 114.67 5.37 -1 4 1 112.79 4.53 1 -4 -1 106.82 4.50 -1 4 1 111.36 5.20 -1 4 1 111.52 5.14 1 -4 -1 102.76 5.14 1 -4 -1 105.20 4.70 1 -4 -1 104.48 5.04 -1 4 0 0.19 0.50 -1 4 0 0.54 0.59 -1 4 0 0.98 0.79 1 -4 0 0.06 0.44 1 -4 0 0.12 0.56 1 -4 0 -0.14 0.79 -1 4 0 -0.08 0.71 -1 4 -1 85.72 3.71 1 -4 1 88.83 3.70 -1 4 -1 88.17 3.74 -1 4 -1 84.85 4.47 -1 4 -1 86.46 4.29 -1 4 -2 217.62 9.24 -1 4 -2 207.97 8.98 -1 4 -2 209.55 9.17 -1 4 -2 202.27 8.22 1 -4 2 209.30 9.09 1 -4 3 335.26 13.58 -1 4 -3 344.45 14.13 -1 4 -3 334.77 14.18 -1 4 -3 331.34 13.08 -1 4 -3 342.35 13.19 -1 4 -3 348.66 14.24 -1 4 -3 335.44 14.05 1 -4 3 333.08 14.04 1 -4 4 2.27 0.92 -1 4 -4 3.36 1.14 -1 4 -4 4.51 1.06 -1 4 -4 4.68 0.77 1 -4 4 3.26 1.30 -1 4 -4 4.09 0.90 1 -4 4 2.35 1.19 -1 4 -5 2.15 1.15 -1 4 -5 0.86 0.80 -1 4 -5 1.73 0.68 1 -4 5 2.21 1.27 -1 4 -5 1.85 0.72 1 -4 6 59.85 3.59 1 -4 6 60.29 4.04 1 -4 6 57.40 3.47 -1 4 -6 63.28 2.76 -1 4 -6 55.84 3.89 1 -4 7 39.97 3.27 -1 4 -7 35.90 2.15 1 -4 7 35.92 2.18 1 -4 7 40.88 2.91 -1 4 -7 34.25 3.06 -1 4 -7 37.81 1.91 -1 4 -7 35.58 2.15 1 -4 7 38.00 2.20 1 -4 8 66.47 3.40 -1 4 -8 69.76 3.40 -1 4 -8 64.55 3.08 -1 4 -8 57.94 4.45 -1 4 -8 68.67 3.37 1 -4 8 66.77 3.40 -1 4 -8 64.66 3.32 1 -4 9 44.42 3.92 1 -4 9 37.92 2.48 -1 4 -9 40.12 2.48 -1 4 -9 43.34 2.51 -1 4 -9 38.91 2.45 1 -4 9 42.54 2.51 1 -4 10 377.32 15.42 1 -4 10 394.70 17.51 -1 4 -10 381.01 15.41 -1 4 -10 373.87 15.31 -1 4 -10 327.74 17.13 -1 4 -10 396.92 15.40 -1 4 -10 384.25 15.35 1 -4 10 385.67 15.36 1 -4 10 383.64 15.42 -1 4 -11 34.97 2.19 1 -4 11 29.30 2.13 -1 4 -11 35.02 2.34 1 -4 11 33.47 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90.79 4.44 1 -3 -13 110.53 4.91 1 -3 -13 105.29 4.70 -1 3 13 100.55 4.84 -1 3 12 8.51 1.24 -1 3 12 8.13 1.67 1 -3 -12 6.19 1.18 1 -3 -12 6.41 1.86 -1 3 12 8.47 1.21 1 -3 -12 5.68 0.98 -1 3 12 8.75 1.86 1 -3 -12 8.00 1.27 1 -3 -12 7.63 1.11 -1 3 12 6.71 1.22 -1 3 11 28.56 2.07 1 -3 -11 31.15 3.07 -1 3 11 25.06 2.70 -1 3 11 30.62 3.38 1 -3 -11 30.93 2.09 -1 3 11 26.04 2.01 1 -3 -11 26.36 1.83 1 -3 -11 30.93 2.14 -1 3 11 28.77 2.06 1 -3 -11 30.04 1.97 1 -3 -10 21.28 1.54 1 -3 -10 23.30 1.77 1 -3 -10 19.93 2.57 -1 3 10 21.93 2.40 -1 3 10 24.56 2.92 1 -3 -10 22.21 1.65 -1 3 10 21.05 2.17 -1 3 10 20.63 1.72 1 -3 -10 22.44 1.78 -1 3 10 22.72 2.82 -1 3 10 21.17 2.71 1 -3 -10 21.21 1.66 -1 3 10 24.25 1.81 1 -3 -9 49.57 2.79 1 -3 -9 56.53 2.71 -1 3 9 49.79 3.62 -1 3 9 49.62 2.69 -1 3 9 57.95 4.22 -1 3 9 51.72 3.48 -1 3 9 60.42 4.03 1 -3 -9 54.91 2.75 -1 3 9 50.92 2.84 1 -3 -9 55.82 2.92 -1 3 9 55.99 4.09 -1 3 9 53.42 4.08 1 -3 -8 59.11 3.01 -1 3 8 67.99 4.39 -1 3 8 65.82 3.78 1 -3 -8 57.67 3.23 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0.35 -1 3 -1 0.13 0.46 1 -3 1 0.14 0.57 -1 3 -1 1.17 0.69 -1 3 -2 89.87 4.35 -1 3 -2 88.59 4.30 -1 3 -2 85.92 3.72 -1 3 -2 94.20 4.46 -1 3 -2 91.61 4.39 -1 3 -2 91.52 3.75 -1 3 -2 93.12 4.20 1 -3 2 83.53 4.26 -1 3 -3 209.93 9.03 1 -3 3 210.67 8.92 -1 3 -3 220.90 9.10 -1 3 -3 206.60 9.07 -1 3 -3 206.61 8.34 -1 3 -3 212.80 9.15 -1 3 -3 223.44 8.84 1 -3 3 208.31 8.94 1 -3 3 203.04 9.08 -1 3 -4 16.29 1.71 1 -3 4 15.16 1.27 -1 3 -4 16.81 1.07 -1 3 -4 17.16 1.15 -1 3 -4 16.66 1.64 1 -3 4 16.77 1.80 1 -3 4 14.66 1.58 1 -3 5 14.72 1.24 -1 3 -5 16.60 1.70 -1 3 -5 14.30 1.11 -1 3 -5 15.97 1.07 -1 3 -5 14.10 1.60 -1 3 -5 14.82 1.37 1 -3 5 18.07 1.88 1 -3 6 38.60 2.53 -1 3 -6 37.98 2.87 -1 3 -6 40.82 1.94 -1 3 -6 39.11 2.02 1 -3 6 37.80 2.44 1 -3 6 41.37 3.00 1 -3 6 35.77 2.57 -1 3 -6 38.82 2.38 -1 3 -7 162.64 7.28 1 -3 7 149.37 6.90 1 -3 7 148.73 7.64 1 -3 7 149.01 7.02 -1 3 -7 156.09 7.76 -1 3 -7 154.56 6.32 1 -3 8 5.47 1.23 -1 3 -8 6.24 1.37 1 -3 8 8.51 1.81 -1 3 -8 5.58 1.00 1 -3 8 5.90 1.03 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0.61 2 -5 -14 10.69 0.90 -2 5 14 13.70 1.17 2 -5 -14 11.01 1.08 -2 5 14 12.67 1.15 -2 5 13 1.99 0.81 -2 5 13 1.90 0.85 2 -5 -13 1.84 0.72 2 -5 -13 0.99 0.71 -2 5 13 1.89 0.85 -2 5 12 8.00 1.19 -2 5 12 7.08 1.02 -2 5 12 8.52 1.13 2 -5 -12 7.70 0.99 -2 5 12 9.77 1.27 2 -5 -11 5.28 1.11 -2 5 11 3.02 1.70 -2 5 11 4.07 1.04 -2 5 11 6.77 1.15 2 -5 -11 4.65 0.81 -2 5 11 6.39 1.17 2 -5 -11 5.07 0.92 -2 5 11 4.99 0.99 -2 5 11 6.17 1.82 -2 5 10 137.34 8.03 2 -5 -10 131.79 5.88 -2 5 10 127.62 5.83 -2 5 10 124.48 7.61 -2 5 10 145.81 6.11 2 -5 -10 122.50 5.68 -2 5 10 113.28 7.85 -2 5 10 138.70 5.99 2 -5 -10 131.88 5.67 -2 5 10 134.97 7.78 -2 5 10 125.41 7.84 2 -5 -9 69.47 3.55 -2 5 9 76.08 5.44 -2 5 9 75.89 3.74 -2 5 9 60.92 5.23 2 -5 -9 68.39 3.43 -2 5 9 70.44 3.62 -2 5 9 74.99 5.26 2 -5 -9 68.17 3.46 2 -5 -9 69.36 3.35 2 -5 -8 8.42 1.07 2 -5 -8 8.83 1.12 2 -5 -8 8.63 1.23 -2 5 8 7.17 1.98 -2 5 8 9.52 1.18 -2 5 8 8.53 1.89 2 -5 -8 7.97 0.99 2 -5 -7 17.08 1.41 -2 5 7 17.25 1.37 2 -5 -7 15.02 1.45 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40.91 2.18 -2 5 -2 42.15 3.16 -2 5 -2 50.76 3.43 -2 5 -2 38.34 2.98 2 -5 2 39.74 2.46 -2 5 -2 41.00 2.83 -2 5 -2 42.37 3.02 -2 5 -3 75.20 3.48 2 -5 3 76.12 3.43 2 -5 3 68.80 3.68 -2 5 -3 76.20 4.20 -2 5 -3 74.74 4.70 -2 5 -3 74.88 4.61 -2 5 -3 80.25 4.63 -2 5 -3 75.33 3.52 2 -5 4 55.76 2.87 2 -5 4 57.14 2.72 -2 5 -4 52.46 3.76 -2 5 -4 53.81 2.71 -2 5 -4 60.41 4.09 -2 5 -4 54.73 2.85 2 -5 4 57.29 2.89 2 -5 5 5.69 0.91 2 -5 5 5.74 1.00 -2 5 -5 6.52 1.39 -2 5 -5 6.16 0.83 -2 5 -5 6.02 0.95 2 -5 5 4.43 0.99 2 -5 6 3.73 1.00 -2 5 -6 3.57 0.77 -2 5 -6 3.57 0.92 -2 5 -6 2.93 0.71 -2 5 -6 3.61 1.24 2 -5 6 4.74 1.02 -2 5 -6 3.49 0.86 2 -5 7 11.14 1.18 2 -5 7 8.90 1.26 -2 5 -7 10.98 1.06 -2 5 -7 9.37 1.18 2 -5 7 11.19 1.32 2 -5 7 8.68 1.50 -2 5 -7 11.52 1.89 -2 5 -7 11.32 0.95 2 -5 7 10.16 1.27 -2 5 -7 10.86 1.24 2 -5 8 69.87 3.55 2 -5 8 69.69 3.64 2 -5 8 73.23 3.73 -2 5 -8 60.40 4.91 -2 5 -8 67.09 3.30 -2 5 -8 71.89 3.67 2 -5 8 79.18 3.76 2 -5 8 76.72 3.72 2 -5 9 22.46 1.74 -2 5 -9 24.88 1.90 2 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62.36 3.19 2 -4 -13 61.29 2.96 -2 4 12 -0.82 0.95 2 -4 -12 1.45 0.95 2 -4 -12 0.38 0.76 -2 4 12 -0.15 0.92 2 -4 -11 19.61 1.73 -2 4 11 17.74 2.27 -2 4 11 25.31 3.09 -2 4 11 26.89 1.92 -2 4 11 21.03 2.96 2 -4 -11 25.43 1.93 2 -4 -11 19.29 1.50 2 -4 -11 19.89 1.58 -2 4 11 22.58 2.91 -2 4 11 19.68 2.80 -2 4 11 24.36 1.87 2 -4 -10 13.71 1.46 -2 4 10 12.04 1.96 -2 4 10 11.69 1.28 -2 4 10 17.21 2.77 -2 4 10 12.50 1.51 2 -4 -10 12.15 1.20 -2 4 10 10.98 2.37 2 -4 -10 12.68 1.52 -2 4 10 12.25 2.31 -2 4 10 12.78 2.39 2 -4 -10 13.96 1.30 2 -4 -9 33.88 2.25 -2 4 9 39.07 3.73 -2 4 9 35.27 2.20 -2 4 9 32.80 2.90 -2 4 9 34.87 2.33 2 -4 -9 36.73 2.13 -2 4 9 30.51 3.52 2 -4 -9 38.11 2.38 -2 4 9 38.14 3.61 2 -4 -9 36.36 2.09 -2 4 8 3.55 1.43 2 -4 -8 3.51 1.00 -2 4 8 4.00 0.94 2 -4 -8 5.31 0.96 2 -4 -8 4.88 0.95 -2 4 8 2.26 1.55 -2 4 8 4.78 1.14 2 -4 -8 4.06 1.08 2 -4 -8 4.29 1.09 -2 4 8 3.42 1.56 -2 4 8 6.64 1.76 -2 4 8 5.87 0.99 2 -4 -8 3.70 0.84 -2 4 7 119.83 6.79 2 -4 -7 124.18 5.44 -2 4 7 118.22 5.36 2 -4 -7 124.80 5.50 -2 4 7 127.91 6.30 -2 4 7 108.71 7.01 2 -4 -7 129.71 5.58 -2 4 7 127.42 5.53 -2 4 7 139.29 7.16 -2 4 6 33.92 2.92 -2 4 6 34.79 1.96 -2 4 6 30.78 2.87 2 -4 -6 33.19 2.65 2 -4 -6 36.69 2.09 -2 4 6 34.19 3.12 2 -4 -6 36.24 2.07 -2 4 5 10.78 1.64 2 -4 -5 13.62 1.22 -2 4 5 12.36 1.76 2 -4 -5 15.68 1.23 -2 4 5 13.76 1.92 2 -4 -4 23.94 1.58 -2 4 4 22.66 2.24 -2 4 4 24.17 2.38 2 -4 -3 228.84 9.38 -2 4 3 231.34 9.38 -2 4 3 235.30 10.49 -2 4 3 232.80 10.64 2 -4 -3 243.10 9.49 -2 4 3 238.06 10.54 -2 4 3 230.08 10.52 2 -4 -2 37.58 2.07 -2 4 2 40.53 2.08 -2 4 2 37.41 2.75 -2 4 2 48.23 3.13 -2 4 2 40.82 2.11 2 -4 -2 41.75 2.11 -2 4 2 39.65 2.82 -2 4 2 39.93 2.85 2 -4 -1 85.95 3.85 -2 4 1 89.37 3.88 -2 4 1 86.57 4.79 -2 4 1 90.01 3.93 2 -4 -1 89.82 3.90 -2 4 1 86.30 4.68 -2 4 1 89.75 4.78 -2 4 0 39.40 2.04 -2 4 0 40.25 2.11 -2 4 0 40.43 2.83 2 -4 0 39.60 2.04 2 -4 0 41.94 2.42 -2 4 0 42.62 2.82 -2 4 0 37.38 2.65 2 -4 1 115.75 4.87 -2 4 -1 112.21 4.88 -2 4 -1 117.23 5.83 2 -4 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9.31 1.36 -2 3 -7 3.51 1.26 -2 3 -7 1.82 1.34 -2 3 -7 3.09 0.99 2 -3 7 1.45 0.93 -2 3 -7 2.45 0.76 -2 3 -7 1.98 1.00 -2 3 -7 1.54 0.67 2 -3 8 8.15 1.11 2 -3 8 9.56 1.17 2 -3 8 8.90 1.15 -2 3 -8 10.02 1.14 -2 3 -8 8.52 1.32 -2 3 -8 7.30 1.55 -2 3 -8 9.99 1.07 2 -3 8 11.51 1.20 -2 3 -8 8.63 1.11 2 -3 9 546.47 21.34 -2 3 -9 565.94 22.77 2 -3 9 539.48 21.53 -2 3 -9 547.45 21.48 -2 3 -9 486.19 23.15 -2 3 -9 546.33 21.34 2 -3 9 560.87 21.52 2 -3 10 99.05 4.83 -2 3 -10 105.60 6.05 -2 3 -10 114.79 5.09 2 -3 10 113.52 5.12 -2 3 -10 103.32 4.85 2 -3 10 109.64 4.99 2 -3 10 110.56 5.04 2 -3 11 21.89 1.65 2 -3 11 22.09 1.84 -2 3 -11 20.92 1.81 2 -3 11 22.32 1.74 -2 3 -11 20.10 2.69 -2 3 -11 22.94 1.82 2 -3 11 21.45 1.74 2 -3 12 0.08 0.92 -2 3 -12 0.46 0.93 -2 3 -12 1.34 1.16 2 -3 12 0.48 0.75 2 -3 12 0.31 0.95 -2 3 -12 0.45 0.86 -2 3 -12 0.57 0.85 -2 3 -13 10.35 1.22 2 -3 13 10.65 1.31 -2 3 -13 12.24 1.39 2 -3 13 6.80 1.03 2 -3 13 7.99 1.17 -2 3 -13 10.88 1.26 2 -3 14 45.06 2.61 -2 3 -14 48.95 2.62 -2 3 -14 42.44 2.44 -2 3 -14 44.84 2.57 2 -3 15 7.11 0.98 -2 3 -15 6.54 0.82 -2 3 -15 7.01 0.99 -2 3 -15 7.20 0.93 2 -3 16 56.09 2.74 -2 3 -16 59.59 2.77 -2 3 -16 60.70 2.73 2 -2 -16 0.69 0.61 -2 2 16 1.50 0.62 2 -2 -15 1.93 0.74 -2 2 15 0.16 0.78 -2 2 15 1.66 1.47 -2 2 15 1.62 0.79 -2 2 14 55.02 2.99 2 -2 -14 54.30 2.91 2 -2 -14 52.76 2.97 -2 2 14 55.99 2.94 2 -2 -13 4.91 1.12 -2 2 13 4.94 1.62 -2 2 13 5.71 1.15 2 -2 -13 6.31 0.93 2 -2 -13 4.40 1.07 -2 2 13 5.20 1.09 -2 2 12 34.38 2.30 -2 2 12 29.35 3.40 2 -2 -12 33.43 2.06 2 -2 -12 35.08 2.31 2 -2 -12 36.03 2.02 -2 2 12 29.48 2.17 -2 2 11 0.60 1.55 -2 2 11 2.88 1.28 -2 2 11 1.42 1.43 2 -2 -11 0.44 0.76 2 -2 -11 1.49 0.98 2 -2 -11 1.34 0.72 2 -2 -11 2.17 0.74 -2 2 11 4.18 1.73 -2 2 11 2.03 0.99 2 -2 -10 219.40 8.82 -2 2 10 181.27 9.59 2 -2 -10 209.69 10.11 -2 2 10 220.39 10.70 -2 2 10 198.00 10.49 -2 2 10 183.30 10.00 2 -2 -10 200.86 8.62 2 -2 -10 220.36 8.90 -2 2 10 212.31 10.70 -2 2 10 203.30 10.59 -2 2 10 194.27 10.39 -2 2 10 221.07 8.86 2 -2 -9 12.20 1.99 2 -2 -9 11.57 1.30 -2 2 9 13.19 2.14 -2 2 9 10.47 1.70 -2 2 9 12.31 2.03 -2 2 9 10.59 1.81 -2 2 9 11.85 2.21 2 -2 -9 10.19 1.14 2 -2 -9 12.46 1.38 -2 2 9 9.78 1.17 -2 2 9 9.29 1.86 -2 2 9 11.83 2.13 2 -2 -9 12.65 1.22 -2 2 8 14.51 2.09 2 -2 -8 15.71 1.36 2 -2 -8 15.41 1.91 -2 2 8 18.05 2.28 -2 2 8 15.72 1.87 2 -2 -8 16.65 1.29 -2 2 8 13.18 2.14 2 -2 -8 16.60 1.41 -2 2 8 17.26 2.19 -2 2 7 73.31 4.69 2 -2 -7 77.87 4.27 2 -2 -7 76.04 3.50 -2 2 7 71.70 3.29 -2 2 7 82.45 4.88 2 -2 -7 80.52 3.63 -2 2 7 82.53 4.82 -2 2 6 73.61 4.50 2 -2 -6 82.08 3.52 2 -2 -6 79.95 4.12 -2 2 6 72.58 3.32 -2 2 6 74.08 4.47 -2 2 6 77.44 4.71 2 -2 -6 81.43 3.59 -2 2 6 78.10 4.60 2 -2 -5 5.23 0.75 2 -2 -5 2.72 0.99 -2 2 5 3.89 0.60 -2 2 5 6.15 1.21 2 -2 -5 3.11 0.89 -2 2 5 8.36 1.58 2 -2 -5 5.15 0.81 -2 2 4 90.01 4.82 -2 2 4 87.96 4.94 2 -2 -4 96.88 4.09 -2 2 4 99.14 4.89 -2 2 3 508.60 19.68 2 -2 -3 480.09 18.75 -2 2 3 495.31 19.68 -2 2 3 480.21 19.57 -2 2 3 482.36 19.56 -2 2 2 108.93 5.35 -2 2 2 117.99 5.40 -2 2 2 112.05 5.34 -2 2 2 114.13 5.37 -2 2 1 11.54 1.28 2 -2 -1 12.81 0.88 -2 2 1 12.94 1.36 -2 2 1 13.56 1.32 -2 2 1 13.79 1.30 -2 2 0 78.69 3.90 2 -2 0 78.81 3.37 -2 2 0 83.80 3.96 -2 2 0 80.10 3.98 -2 2 -1 37.49 2.25 -2 2 -1 33.21 2.15 2 -2 1 33.85 1.66 -2 2 -1 34.35 2.21 -2 2 -2 123.88 5.56 -2 2 -2 112.13 5.32 -2 2 -2 116.00 4.78 -2 2 -3 713.03 27.90 -2 2 -3 732.32 28.48 -2 2 -3 725.20 28.68 -2 2 -3 725.51 27.77 -2 2 -3 762.25 28.70 -2 2 -4 65.60 3.06 -2 2 -4 67.39 3.55 -2 2 -4 58.92 3.47 -2 2 -4 61.16 2.71 -2 2 -4 61.38 2.67 -2 2 -5 17.81 1.80 -2 2 -5 17.26 1.86 -2 2 -5 19.10 1.27 -2 2 -6 138.58 6.43 -2 2 -6 137.78 6.83 -2 2 -6 137.55 5.77 -2 2 -6 135.65 5.75 2 -2 6 137.55 6.90 -2 2 -7 54.70 3.77 -2 2 -7 56.16 2.78 -2 2 -7 58.31 2.82 2 -2 7 54.31 3.87 -2 2 -8 54.11 3.99 -2 2 -8 56.96 2.83 -2 2 -8 57.43 2.91 2 -2 8 66.55 4.34 -2 2 -9 12.57 1.76 2 -2 9 10.77 1.25 2 -2 9 11.86 1.17 -2 2 -9 8.63 1.72 -2 2 -9 12.02 1.13 2 -2 9 10.28 2.07 2 -2 9 10.56 1.24 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-2 -4 -6 80.89 4.57 -2 -4 -6 82.34 4.65 2 4 6 82.26 4.16 2 4 6 87.54 4.66 2 4 7 5.19 0.77 -2 -4 -7 5.56 1.44 2 4 7 5.72 1.32 -2 -4 -8 83.44 4.97 -2 -4 -8 73.47 4.77 -2 -4 -8 82.91 3.76 2 4 8 81.70 4.95 -2 -4 -9 2.03 1.62 -2 -4 -9 3.09 0.85 2 4 9 2.13 1.35 2 4 9 1.85 0.81 -2 -4 -10 22.48 2.81 -2 -4 -10 23.11 2.52 2 4 10 22.28 1.50 -2 -4 -10 23.71 1.70 2 4 10 24.90 2.78 2 4 10 21.93 1.56 -2 -4 -11 20.21 1.62 -2 -4 -11 24.79 3.02 -2 -4 -11 22.86 2.27 -2 -4 -11 22.91 1.70 2 4 11 17.99 1.48 -2 -4 -12 55.14 2.97 2 4 12 54.00 3.08 -2 -4 -12 52.86 4.21 2 4 12 44.48 3.96 -2 -4 -12 59.20 3.11 -2 -4 -12 65.30 3.12 2 4 12 55.51 2.94 -2 -4 -13 10.20 1.93 -2 -4 -13 12.03 1.35 -2 -4 -13 10.87 1.22 2 4 13 8.14 1.21 -2 -4 -13 10.95 1.28 2 4 13 8.79 1.14 -2 -4 -14 12.39 1.33 -2 -4 -14 15.67 2.58 2 4 14 14.29 1.41 2 4 14 15.18 1.58 -2 -4 -14 15.76 1.44 -2 -4 -14 13.72 1.32 -2 -4 -14 14.49 1.45 -2 -4 -14 16.22 1.45 2 4 15 1.73 0.85 -2 -4 -15 0.18 0.77 -2 -4 -15 0.06 0.79 -2 -4 -15 0.80 0.77 -2 -4 -15 0.50 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104.63 4.66 2 5 -8 91.92 4.42 -2 -5 7 3.94 1.62 -2 -5 7 1.74 1.47 2 5 -7 1.35 0.85 -2 -5 7 2.63 1.59 2 5 -7 1.29 0.91 2 5 -7 2.11 0.83 2 5 -7 2.13 0.82 -2 -5 7 2.31 0.85 2 5 -7 1.04 0.77 -2 -5 6 2.80 1.29 2 5 -6 1.53 0.85 2 5 -6 3.71 0.80 2 5 -6 4.95 0.81 -2 -5 6 0.87 1.37 2 5 -6 2.87 0.85 -2 -5 5 4.49 1.43 2 5 -5 4.22 0.95 2 5 -5 4.41 0.75 -2 -5 5 4.36 1.43 -2 -5 4 11.43 1.78 2 5 -4 12.94 1.41 2 5 -4 16.74 1.18 -2 -5 4 12.58 1.92 -2 -5 3 10.65 1.58 -2 -5 3 10.23 1.40 2 5 -3 11.05 1.12 2 5 -3 10.07 0.95 -2 -5 3 7.98 1.62 -2 -5 2 16.58 1.79 -2 -5 2 18.48 1.71 2 5 -2 15.05 1.26 2 5 -2 15.71 1.13 -2 -5 2 18.18 2.00 2 5 -1 7.10 1.31 2 5 -1 7.20 0.79 2 5 -1 8.03 0.78 -2 -5 1 6.48 1.43 -2 -5 0 6.18 1.13 2 5 0 5.05 0.61 -2 -5 0 4.79 1.36 -2 -5 -1 17.53 1.82 2 5 1 16.53 1.02 2 5 1 16.89 1.35 -2 -5 -1 17.83 1.06 -2 -5 -1 16.76 1.78 2 5 2 30.23 1.60 2 5 2 29.20 1.52 2 5 2 33.60 1.92 -2 -5 -2 32.52 2.37 -2 -5 -3 150.18 7.08 2 5 3 157.19 6.52 -2 -5 -3 154.97 7.04 -2 -5 -3 139.45 6.63 -2 -5 -4 9.86 1.53 -2 -5 -4 10.87 1.53 -2 -5 -4 9.05 1.44 -2 -5 -4 8.38 1.34 -2 -5 -4 8.61 1.44 -2 -5 -4 9.32 0.91 2 5 4 9.86 1.12 -2 -5 -5 28.06 2.36 -2 -5 -5 24.75 2.44 -2 -5 -5 30.85 2.53 -2 -5 -5 28.35 1.67 2 5 5 29.32 2.01 -2 -5 -6 75.09 4.46 -2 -5 -6 76.21 4.39 -2 -5 -6 69.09 4.40 -2 -5 -6 72.89 4.47 2 5 6 77.12 3.97 -2 -5 -6 75.52 3.46 2 5 6 71.69 4.34 -2 -5 -7 12.17 1.81 -2 -5 -7 9.57 1.91 -2 -5 -7 12.22 1.09 2 5 7 6.50 1.22 2 5 7 8.18 1.53 -2 -5 -8 24.54 2.63 -2 -5 -8 24.48 2.60 2 5 8 20.74 1.62 -2 -5 -8 18.40 2.41 2 5 8 21.32 2.06 -2 -5 -8 23.48 1.61 2 5 8 23.31 2.50 -2 -5 -9 358.62 15.43 2 5 9 352.37 13.92 2 5 9 341.19 13.67 -2 -5 -9 340.68 13.85 2 5 9 321.02 14.76 2 5 9 350.25 15.60 2 5 9 346.83 13.74 2 5 10 5.36 1.15 -2 -5 -10 3.03 1.90 -2 -5 -10 7.02 1.12 2 5 10 5.94 1.39 2 5 10 7.19 1.83 2 5 10 7.81 1.97 2 5 10 5.21 1.08 -2 -5 -11 57.47 4.57 -2 -5 -11 55.83 3.77 -2 -5 -11 58.26 3.06 2 5 11 52.51 2.73 2 5 11 58.92 4.32 -2 -5 -12 11.62 1.96 -2 -5 -12 8.19 1.19 2 5 12 10.00 2.13 -2 -5 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11.15 2.42 2 6 -9 10.01 1.44 -2 -6 9 6.32 1.98 -2 -6 9 5.90 1.78 -2 -6 9 8.81 1.72 2 6 -9 9.93 1.22 -2 -6 9 10.15 1.27 2 6 -9 8.21 1.11 2 6 -8 7.66 1.10 2 6 -8 9.29 1.34 -2 -6 8 9.68 2.20 2 6 -8 7.34 1.12 2 6 -8 10.24 1.20 2 6 -8 8.33 1.11 -2 -6 7 24.08 2.92 -2 -6 7 22.80 2.83 2 6 -7 25.78 1.77 -2 -6 7 26.89 3.01 2 6 -7 27.43 1.97 2 6 -7 26.93 1.87 2 6 -7 21.77 2.34 2 6 -7 28.22 1.88 2 6 -7 24.07 1.69 -2 -6 6 49.24 3.97 -2 -6 6 48.72 3.95 2 6 -6 48.78 2.62 -2 -6 6 41.03 3.80 2 6 -6 44.47 2.71 2 6 -6 50.17 2.68 2 6 -6 48.61 2.63 2 6 -6 36.25 3.06 2 6 -6 48.04 2.51 -2 -6 5 50.74 3.91 2 6 -5 60.06 2.87 -2 -6 5 57.34 4.16 2 6 -5 52.87 2.87 2 6 -5 52.27 2.80 2 6 -5 51.86 3.35 2 6 -5 54.65 2.79 2 6 -5 47.55 2.63 -2 -6 4 38.61 3.17 2 6 -4 31.60 2.41 2 6 -4 37.71 2.11 2 6 -4 41.26 2.22 2 6 -4 34.85 2.60 2 6 -4 38.58 2.25 -2 -6 4 38.83 3.24 2 6 -4 37.07 2.22 -2 -6 3 125.34 6.25 2 6 -3 119.97 5.84 2 6 -3 109.23 5.39 2 6 -3 112.36 4.97 -2 -6 3 115.71 6.30 -2 -6 2 1.06 1.20 2 6 -2 1.05 0.58 2 6 -2 1.67 0.60 -2 -6 2 1.35 1.25 -2 -6 1 3.24 1.47 2 6 -1 -0.25 0.95 2 6 -1 -0.18 0.47 -2 -6 1 2.35 1.41 -2 -6 0 37.83 2.87 2 6 0 36.11 1.98 -2 -6 0 35.25 2.16 -2 -6 0 37.47 2.86 -2 -6 -1 8.35 1.60 2 6 1 8.36 0.82 2 6 1 9.46 0.80 -2 -6 -1 8.28 1.64 -2 -6 -1 7.50 1.48 -2 -6 -1 6.39 1.46 -2 -6 -2 14.43 1.87 2 6 2 12.76 1.02 -2 -6 -2 12.48 1.00 2 6 2 10.99 1.27 -2 -6 -2 14.83 1.78 -2 -6 -2 13.84 1.85 -2 -6 -3 514.46 21.03 2 6 3 521.78 20.36 -2 -6 -3 523.22 21.01 -2 -6 -3 485.20 20.53 -2 -6 -4 24.90 2.41 2 6 4 25.59 1.93 -2 -6 -4 27.14 2.44 -2 -6 -4 22.75 2.23 -2 -6 -4 22.36 2.20 -2 -6 -4 23.08 2.45 -2 -6 -5 22.73 1.54 -2 -6 -5 24.93 2.40 -2 -6 -5 28.69 2.61 -2 -6 -5 28.66 2.68 -2 -6 -5 27.08 2.56 -2 -6 -5 26.69 1.65 2 6 5 30.59 2.15 -2 -6 -6 68.90 4.42 -2 -6 -6 68.26 4.46 -2 -6 -6 72.16 4.61 -2 -6 -6 73.81 4.60 2 6 6 65.02 3.90 -2 -6 -6 73.15 3.40 -2 -6 -7 100.75 5.74 -2 -6 -7 101.91 5.73 -2 -6 -7 95.55 5.69 -2 -6 -7 97.80 5.77 2 6 7 89.08 5.06 -2 -6 -7 99.52 4.46 2 6 7 95.04 4.35 -2 -6 -8 14.92 2.16 -2 -6 -8 14.08 2.37 -2 -6 -8 10.69 2.12 2 6 8 15.45 1.81 2 6 8 15.37 1.23 -2 -6 -8 12.54 1.31 2 6 8 13.69 1.22 -2 -6 -9 97.43 5.93 -2 -6 -9 95.86 5.90 2 6 9 97.35 4.48 -2 -6 -9 106.31 6.04 2 6 9 91.36 4.20 2 6 9 78.21 5.10 -2 -6 -9 93.06 4.41 2 6 9 90.86 5.89 2 6 9 84.75 4.18 -2 -6 -10 85.40 5.61 2 6 10 78.65 3.92 -2 -6 -10 87.55 5.49 -2 -6 -10 83.49 3.94 2 6 10 53.19 4.40 2 6 10 77.06 3.61 2 6 10 73.33 4.96 2 6 10 62.23 5.17 2 6 10 74.37 3.71 -2 -6 -11 20.41 1.73 2 6 11 23.76 1.87 -2 -6 -11 28.04 3.27 -2 -6 -11 19.78 2.50 2 6 11 18.02 1.43 -2 -6 -11 21.40 1.76 -2 -6 -11 19.71 1.67 2 6 11 19.62 2.58 2 6 11 24.24 1.71 2 6 11 16.03 2.73 -2 -6 -12 56.23 2.88 2 6 12 53.76 2.99 -2 -6 -12 43.46 3.79 -2 -6 -12 48.48 2.89 -2 -6 -12 48.80 2.81 2 6 12 50.14 4.04 2 6 12 49.75 2.83 -2 -6 -13 15.59 1.49 -2 -6 -13 15.85 1.47 -2 -6 -13 14.68 1.40 2 6 13 13.13 2.17 2 6 14 72.12 3.71 -2 -6 -14 73.39 3.54 -2 -6 -14 67.08 3.56 -2 -6 -14 74.94 3.54 2 6 15 6.70 1.02 -2 -6 -15 5.96 0.93 2 6 15 7.40 1.03 -2 -6 -15 6.89 0.95 2 6 16 6.94 0.90 -2 -6 -16 7.02 0.81 -2 -6 -16 6.70 0.80 -2 -6 -16 6.84 0.82 2 6 17 0.54 0.45 -2 -6 -17 1.36 0.43 -2 -6 -17 1.96 0.46 2 7 -14 1.36 0.38 -2 -7 14 2.66 0.53 -2 -7 13 15.82 1.20 2 7 -12 0.58 0.66 -2 -7 12 -0.15 0.81 2 7 -12 0.46 0.69 -2 -7 12 0.52 0.82 2 7 -11 0.07 0.76 2 7 -11 0.19 0.77 2 7 -11 0.49 0.64 -2 -7 11 1.89 0.99 -2 -7 10 26.22 2.86 -2 -7 10 25.51 1.85 2 7 -10 31.01 2.02 -2 -7 10 28.36 2.98 2 7 -10 30.46 2.09 2 7 -10 30.74 2.11 -2 -7 9 345.99 16.39 -2 -7 9 343.66 16.19 -2 -7 9 351.67 16.52 2 7 -9 368.19 14.91 2 7 -9 389.94 14.99 -2 -7 9 349.67 14.62 2 7 -9 388.88 14.87 2 7 -8 29.27 1.91 -2 -7 8 24.67 1.96 2 7 -8 30.78 2.17 2 7 -8 29.93 2.13 -2 -7 8 27.21 3.06 2 7 -8 29.86 2.02 -2 -7 8 27.34 1.98 -2 -7 7 53.33 4.33 2 7 -7 51.73 2.86 -2 -7 7 52.93 4.26 -2 -7 7 50.62 2.89 -2 -7 7 51.29 4.31 2 7 -7 52.70 3.04 2 7 -7 50.63 3.02 2 7 -7 54.03 2.95 2 7 -7 51.92 2.91 -2 -7 7 50.17 2.87 -2 -7 6 10.47 2.18 2 7 -6 11.60 1.29 -2 -7 6 8.91 1.17 -2 -7 6 9.97 2.15 -2 -7 6 7.43 2.07 -2 -7 6 10.96 2.24 2 7 -6 11.00 1.35 2 7 -6 11.68 1.26 2 7 -6 7.22 1.31 2 7 -6 10.50 1.23 -2 -7 6 9.75 1.20 -2 -7 5 15.74 2.48 -2 -7 5 14.95 2.27 -2 -7 5 13.88 2.48 2 7 -5 15.94 1.50 2 7 -5 11.95 1.58 2 7 -5 14.97 1.34 2 7 -5 15.29 1.40 -2 -7 5 15.37 1.36 -2 -7 4 69.94 4.87 2 7 -4 57.35 3.71 2 7 -4 69.44 3.35 2 7 -4 65.84 3.96 -2 -7 4 69.75 4.46 -2 -7 4 66.74 4.77 2 7 -4 67.64 3.47 -2 -7 3 184.91 8.96 2 7 -3 177.25 7.14 2 7 -3 148.15 7.50 2 7 -3 165.50 8.01 2 7 -3 167.61 7.27 -2 -7 3 164.94 8.10 -2 -7 3 183.62 8.89 -2 -7 2 238.07 10.81 2 7 -2 224.69 9.24 2 7 -2 216.15 9.50 2 7 -2 228.50 10.22 -2 -7 2 223.51 10.71 -2 -7 2 230.17 10.72 2 7 -2 216.46 9.24 -2 -7 1 7.37 1.66 2 7 -1 4.61 0.92 2 7 -1 4.20 0.74 2 7 -1 4.85 0.88 -2 -7 1 4.56 1.06 -2 -7 1 5.05 1.58 -2 -7 1 5.08 1.60 -2 -7 0 1.78 1.35 -2 -7 0 3.56 1.31 2 7 0 5.49 1.38 2 7 0 3.38 0.63 2 7 0 2.88 0.63 -2 -7 0 4.84 1.55 -2 -7 0 4.89 1.34 -2 -7 0 2.84 1.48 -2 -7 -1 2.59 1.51 -2 -7 -1 3.16 1.36 2 7 1 1.70 0.58 -2 -7 -1 1.65 1.19 -2 -7 -1 2.24 1.36 -2 -7 -2 286.14 12.45 2 7 2 254.83 11.05 2 7 2 287.09 11.73 -2 -7 -2 286.42 12.41 -2 -7 -2 276.38 12.28 -2 -7 -3 1.16 1.28 -2 -7 -3 0.82 1.07 -2 -7 -3 0.90 1.28 2 7 3 0.41 0.50 2 7 3 0.33 0.75 -2 -7 -3 0.45 0.67 -2 -7 -4 14.65 2.03 2 7 4 13.94 1.31 -2 -7 -4 17.31 2.10 -2 -7 -4 13.31 1.91 -2 -7 -4 14.46 2.16 2 7 4 15.60 1.63 2 7 4 17.23 1.27 2 7 5 6.26 0.98 -2 -7 -5 8.21 1.91 -2 -7 -5 8.04 1.75 -2 -7 -5 4.73 1.53 -2 -7 -5 8.84 1.89 -2 -7 -5 6.00 0.93 2 7 5 4.78 1.09 -2 -7 -6 48.02 3.76 2 7 6 46.76 2.70 -2 -7 -6 47.05 3.74 -2 -7 -6 50.93 3.91 -2 -7 -6 56.55 4.07 -2 -7 -6 51.79 3.87 2 7 6 46.22 3.20 -2 -7 -6 49.98 2.66 2 7 6 49.93 2.56 -2 -7 -7 20.20 2.50 -2 -7 -7 17.02 1.34 2 7 7 16.10 1.46 -2 -7 -7 16.19 2.34 -2 -7 -7 19.56 2.63 -2 -7 -7 16.93 1.51 2 7 7 16.63 1.90 2 7 7 19.55 1.43 -2 -7 -8 14.53 2.21 -2 -7 -8 9.51 2.22 -2 -7 -8 10.21 2.00 -2 -7 -8 9.73 1.26 -2 -7 -8 11.21 2.30 -2 -7 -8 11.45 1.29 2 7 8 12.28 1.70 2 7 8 11.80 1.17 -2 -7 -9 74.49 5.28 -2 -7 -9 84.65 5.61 2 7 9 86.00 4.10 -2 -7 -9 86.10 5.65 -2 -7 -9 75.13 3.76 2 7 9 77.94 3.76 -2 -7 -9 73.58 3.72 -2 -7 -9 82.05 4.00 -2 -7 -10 339.91 15.29 2 7 10 340.39 13.47 -2 -7 -10 321.33 13.04 -2 -7 -10 362.45 15.49 2 7 10 327.99 13.08 -2 -7 -10 331.57 13.15 -2 -7 -10 351.37 13.47 2 7 10 295.07 13.06 -2 -7 -11 6.98 1.21 2 7 11 6.41 1.23 -2 -7 -11 8.66 2.35 -2 -7 -11 5.09 1.15 -2 -7 -11 7.91 1.12 2 7 11 6.09 1.02 2 7 12 10.42 1.33 -2 -7 -12 10.13 1.28 -2 -7 -12 7.07 1.15 -2 -7 -12 5.24 1.04 2 7 12 10.33 1.11 2 7 12 5.58 1.04 -2 -7 -13 21.95 1.65 2 7 13 20.49 1.72 -2 -7 -13 19.60 1.60 -2 -7 -13 21.51 1.61 2 7 14 9.69 1.21 -2 -7 -14 9.24 1.06 -2 -7 -14 10.30 1.16 -2 -7 -14 10.52 1.10 2 7 15 54.88 2.79 -2 -7 -15 53.68 2.62 2 7 15 48.77 2.58 2 7 16 9.92 0.92 -2 -7 -16 10.00 0.87 -2 -7 -16 11.11 0.87 2 8 -13 3.46 0.54 -2 -8 13 9.54 0.74 2 8 -12 8.93 0.90 -2 -8 12 9.80 0.99 -2 -8 12 11.54 1.03 -2 -8 11 5.54 0.94 2 8 -11 7.83 0.99 -2 -8 11 7.86 1.07 -2 -8 11 6.88 1.06 -2 -8 10 0.96 0.81 -2 -8 10 2.34 1.02 2 8 -10 0.99 0.87 2 8 -10 0.94 0.71 -2 -8 10 1.21 1.00 -2 -8 9 0.56 1.60 -2 -8 9 1.65 1.46 -2 -8 9 0.96 0.87 -2 -8 9 3.18 1.57 2 8 -9 2.50 0.95 2 8 -9 1.69 0.80 -2 -8 9 0.81 0.99 -2 -8 9 1.22 0.90 2 8 -8 6.79 1.13 -2 -8 8 10.77 2.07 -2 -8 8 4.66 1.92 -2 -8 8 7.49 1.14 2 8 -8 9.88 1.33 2 8 -8 8.91 1.14 -2 -8 8 8.36 1.12 -2 -8 8 10.43 1.26 -2 -8 7 2.06 1.78 -2 -8 7 1.14 1.64 2 8 -7 2.03 0.97 -2 -8 7 3.51 1.57 -2 -8 7 2.45 0.96 -2 -8 7 0.71 1.69 2 8 -7 2.81 1.08 2 8 -7 1.75 0.87 -2 -8 7 2.61 0.92 -2 -8 6 263.85 12.16 -2 -8 6 229.99 11.62 -2 -8 6 223.82 9.81 2 8 -6 249.56 10.19 -2 -8 6 252.61 12.13 2 8 -6 247.01 10.03 -2 -8 6 234.71 9.91 -2 -8 5 4.01 1.90 -2 -8 5 1.38 1.74 -2 -8 5 3.83 1.63 -2 -8 5 4.31 1.86 2 8 -5 4.24 1.11 2 8 -5 4.23 0.92 -2 -8 5 3.03 1.06 -2 -8 5 4.92 0.97 -2 -8 4 8.56 2.20 2 8 -4 13.14 1.44 -2 -8 4 13.07 2.07 -2 -8 4 13.75 2.53 -2 -8 4 11.16 2.33 2 8 -4 13.37 1.43 2 8 -4 11.62 1.21 -2 -8 4 9.74 1.28 -2 -8 3 3.12 1.84 -2 -8 3 1.67 1.43 2 8 -3 2.36 1.00 -2 -8 3 1.16 1.16 -2 -8 3 2.01 1.72 -2 -8 3 2.00 1.77 2 8 -3 2.37 0.93 2 8 -3 2.50 1.22 -2 -8 3 2.39 0.98 -2 -8 2 159.10 8.38 2 8 -2 151.47 6.45 -2 -8 2 155.87 8.24 2 8 -2 153.31 6.71 -2 -8 2 161.15 8.34 -2 -8 2 161.43 8.39 -2 -8 2 159.21 8.45 2 8 -2 142.89 6.64 2 8 -2 145.43 7.64 2 8 -2 151.65 6.43 -2 -8 1 22.72 2.79 -2 -8 1 25.56 2.85 2 8 -1 22.22 1.66 2 8 -1 23.68 1.80 -2 -8 1 27.96 2.91 -2 -8 1 22.26 2.77 -2 -8 1 26.88 3.03 2 8 -1 23.51 1.78 2 8 -1 23.76 1.55 2 8 -1 21.20 2.40 -2 -8 0 355.27 15.37 -2 -8 0 347.61 15.31 2 8 0 336.89 13.66 -2 -8 0 369.87 15.44 -2 -8 0 341.99 15.21 -2 -8 0 356.03 15.39 2 8 0 322.58 13.30 2 8 0 336.20 13.51 -2 -8 -1 20.13 2.52 -2 -8 -1 19.41 2.49 -2 -8 -1 21.50 2.58 -2 -8 -1 19.05 2.43 2 8 1 22.18 1.73 2 8 1 24.14 1.57 -2 -8 -2 17.26 2.26 -2 -8 -2 18.01 2.40 -2 -8 -2 11.91 2.30 -2 -8 -2 17.82 2.46 2 8 2 13.50 1.35 2 8 2 13.20 1.37 2 8 2 16.04 1.33 -2 -8 -3 84.77 5.41 2 8 3 83.16 4.05 2 8 3 80.74 4.03 -2 -8 -3 88.56 5.32 -2 -8 -3 85.97 5.42 -2 -8 -3 84.27 5.49 2 8 3 84.81 4.73 2 8 3 86.92 4.04 2 8 4 -0.07 0.77 -2 -8 -4 -0.39 1.21 -2 -8 -4 0.20 1.48 -2 -8 -4 0.80 1.31 -2 -8 -4 2.43 1.84 2 8 4 0.14 0.82 2 8 4 0.65 0.65 2 8 5 5.53 1.00 -2 -8 -5 2.44 0.88 -2 -8 -5 3.02 1.43 -2 -8 -5 2.48 1.44 -2 -8 -5 2.69 1.77 -2 -8 -5 3.77 1.76 2 8 5 3.89 1.08 2 8 5 4.20 0.77 2 8 6 25.52 1.87 -2 -8 -6 27.45 2.98 -2 -8 -6 26.15 3.08 -2 -8 -6 20.63 2.91 -2 -8 -6 30.30 3.04 2 8 6 26.90 2.36 -2 -8 -6 21.04 1.71 2 8 6 23.39 1.65 -2 -8 -7 104.82 4.65 2 8 7 104.70 4.93 -2 -8 -7 99.38 6.49 -2 -8 -7 96.14 6.41 -2 -8 -7 111.29 4.94 2 8 7 101.01 4.75 2 8 7 103.85 6.30 2 8 8 1.98 0.95 2 8 8 2.64 1.08 -2 -8 -8 -0.43 2.06 -2 -8 -8 2.49 1.68 -2 -8 -8 2.48 1.08 -2 -8 -8 2.07 1.85 -2 -8 -8 2.71 0.99 2 8 8 2.95 1.43 2 8 8 2.00 0.81 -2 -8 -9 27.07 3.24 2 8 9 24.49 2.00 -2 -8 -9 24.58 1.81 -2 -8 -9 27.61 3.31 2 8 9 23.19 1.69 -2 -8 -9 26.77 1.98 2 8 9 27.58 3.19 -2 -8 -10 2.36 1.00 -2 -8 -10 2.51 2.04 2 8 10 3.00 1.11 -2 -8 -10 4.79 2.17 2 8 10 3.16 1.64 2 8 10 3.28 0.80 -2 -8 -11 14.79 1.34 -2 -8 -11 15.93 1.51 -2 -8 -11 15.76 2.64 2 8 11 18.09 1.62 2 8 12 7.20 1.18 -2 -8 -12 8.65 1.18 2 8 12 5.79 0.94 -2 -8 -13 40.59 2.27 2 8 13 43.37 2.42 -2 -8 -13 44.26 2.28 2 8 14 3.94 0.86 -2 -8 -14 5.59 0.91 -2 -8 -14 6.26 0.84 2 8 15 2.20 0.62 -2 -8 -15 0.67 0.59 -2 -8 -15 1.31 0.56 -2 -8 -16 5.31 0.55 -2 -8 -16 5.95 0.55 -2 -9 12 0.07 0.44 2 9 -12 -0.02 0.33 2 9 -11 18.98 1.23 -2 -9 11 18.62 1.26 -2 -9 11 17.32 1.24 -2 -9 10 35.11 1.88 2 9 -10 38.20 2.11 -2 -9 10 37.43 2.13 -2 -9 10 35.65 2.08 -2 -9 9 41.36 2.41 2 9 -9 38.02 2.27 -2 -9 9 40.01 2.13 2 9 -9 45.42 2.43 2 9 -8 5.23 0.97 2 9 -8 6.79 0.98 -2 -9 8 6.10 0.94 -2 -9 8 7.42 1.24 -2 -9 8 7.82 1.80 2 9 -8 7.05 1.08 -2 -9 7 19.62 1.79 -2 -9 7 17.80 2.58 -2 -9 7 23.20 2.79 2 9 -7 23.47 1.82 2 9 -7 20.36 1.61 -2 -9 6 9.77 2.20 -2 -9 6 9.50 1.96 -2 -9 6 11.01 2.25 -2 -9 6 8.17 2.34 2 9 -6 11.12 1.36 2 9 -6 10.74 1.21 -2 -9 6 10.53 1.34 -2 -9 5 31.72 3.42 2 9 -5 26.88 2.02 -2 -9 5 26.62 3.29 2 9 -5 27.27 2.04 -2 -9 5 30.48 3.42 -2 -9 5 27.98 3.05 -2 -9 5 26.19 1.92 -2 -9 4 0.96 1.77 -2 -9 4 3.37 1.82 -2 -9 4 1.99 1.89 2 9 -4 3.79 1.09 -2 -9 4 4.41 2.15 2 9 -4 1.90 1.04 -2 -9 4 5.16 1.08 -2 -9 3 346.70 15.86 2 9 -3 331.88 13.77 2 9 -3 342.50 13.43 -2 -9 3 344.38 15.77 -2 -9 3 350.06 15.93 -2 -9 3 342.38 15.80 2 9 -3 330.19 13.74 2 9 -3 326.67 13.50 -2 -9 3 338.56 13.46 2 9 -2 43.73 2.80 -2 -9 2 56.32 4.44 -2 -9 2 54.58 4.31 2 9 -2 47.88 2.63 -2 -9 2 50.21 2.78 -2 -9 2 56.65 4.40 -2 -9 2 48.22 4.24 -2 -9 2 55.29 4.41 2 9 -2 47.11 2.79 2 9 -2 46.17 2.55 2 9 -2 42.11 3.54 2 9 -2 45.94 2.68 2 9 -1 7.49 1.12 -2 -9 1 9.62 2.28 -2 -9 1 8.37 2.03 2 9 -1 12.31 1.44 -2 -9 1 11.67 2.30 -2 -9 1 13.65 2.23 -2 -9 1 12.03 2.31 2 9 -1 12.64 1.90 2 9 -1 8.42 0.95 2 9 -1 9.18 1.08 -2 -9 0 4.30 1.77 2 9 0 3.05 1.08 -2 -9 0 7.08 1.92 -2 -9 0 5.46 2.01 -2 -9 0 4.76 1.84 2 9 0 2.67 0.67 2 9 0 2.99 1.40 2 9 0 2.80 0.80 -2 -9 -1 93.72 5.83 -2 -9 -1 87.05 5.79 -2 -9 -1 87.88 5.78 -2 -9 -1 81.66 5.72 2 9 1 84.85 4.27 2 9 1 92.72 4.25 2 9 1 84.43 4.03 -2 -9 -2 56.82 4.52 -2 -9 -2 55.68 4.44 -2 -9 -2 61.07 4.52 -2 -9 -2 53.51 2.90 2 9 2 48.34 2.86 2 9 2 48.41 2.84 2 9 2 52.60 2.82 2 9 2 45.62 2.56 -2 -9 -3 253.04 12.22 -2 -9 -3 257.71 12.23 -2 -9 -3 254.05 12.24 2 9 3 246.32 10.37 2 9 3 242.89 10.36 2 9 3 252.71 10.33 2 9 4 11.56 1.34 -2 -9 -4 10.09 2.09 -2 -9 -4 9.85 2.28 -2 -9 -4 14.39 2.65 2 9 4 8.73 1.42 2 9 4 12.17 1.24 -2 -9 -5 2.10 1.64 -2 -9 -5 3.00 2.01 -2 -9 -5 0.69 1.89 2 9 5 2.15 0.94 -2 -9 -5 4.01 1.54 -2 -9 -5 1.46 0.95 -2 -9 -6 22.10 2.90 -2 -9 -6 28.24 3.26 -2 -9 -6 20.27 2.60 -2 -9 -6 22.13 1.64 2 9 6 20.74 1.79 2 9 6 19.08 1.49 -2 -9 -7 22.42 3.05 -2 -9 -7 24.73 3.29 -2 -9 -7 21.90 2.69 -2 -9 -7 17.69 2.71 -2 -9 -7 23.49 1.66 2 9 7 24.66 1.90 2 9 7 24.11 1.86 2 9 7 26.69 2.87 -2 -9 -8 7.34 2.08 -2 -9 -8 11.52 2.55 2 9 8 11.21 1.35 -2 -9 -8 10.65 2.14 -2 -9 -8 11.48 1.18 -2 -9 -8 10.79 2.30 2 9 8 13.56 1.47 2 9 8 12.15 1.20 2 9 8 12.74 2.19 -2 -9 -9 30.39 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1.76 4 5 -12 26.18 1.67 4 5 -12 24.90 1.61 4 5 -11 20.34 1.62 4 5 -11 22.41 1.59 -4 -5 11 19.26 1.64 4 5 -11 17.90 1.38 -4 -5 10 36.60 3.92 -4 -5 10 51.65 4.14 -4 -5 10 41.48 3.79 4 5 -10 49.29 2.67 4 5 -10 40.90 2.53 4 5 -10 39.10 2.38 -4 -5 10 43.30 2.60 4 5 -10 40.25 2.41 4 5 -9 19.51 1.72 4 5 -9 16.06 1.36 4 5 -9 16.95 1.57 -4 -5 9 17.66 1.67 4 5 -9 19.73 1.57 -4 -5 8 2.25 1.67 -4 -5 8 0.70 1.67 4 5 -8 4.39 1.07 4 5 -8 3.26 0.83 4 5 -8 3.09 0.93 4 5 -8 2.91 0.84 -4 -5 8 3.13 1.05 4 5 -8 2.63 0.88 -4 -5 7 3.41 1.63 4 5 -7 2.33 0.97 4 5 -7 2.87 0.88 4 5 -7 3.16 0.89 -4 -5 7 3.13 1.57 4 5 -7 0.97 0.92 -4 -5 6 19.24 2.58 4 5 -6 17.16 1.57 4 5 -6 14.27 1.37 4 5 -6 16.41 1.52 4 5 -6 15.38 1.41 4 5 -6 17.49 1.48 -4 -5 5 11.00 2.05 -4 -5 5 12.28 2.06 4 5 -5 13.51 1.42 4 5 -5 16.07 1.36 4 5 -5 16.19 1.45 4 5 -5 17.17 1.40 4 5 -5 15.26 1.44 -4 -5 4 0.79 1.26 -4 -5 4 1.33 1.29 4 5 -4 3.20 0.90 4 5 -4 2.27 0.82 4 5 -4 2.14 0.79 4 5 -4 3.44 0.82 4 5 -4 2.87 0.81 -4 -5 3 35.89 3.12 -4 -5 3 32.71 2.75 4 5 -3 30.55 2.05 -4 -5 3 27.71 2.70 -4 -5 3 32.16 2.79 4 5 -3 34.33 2.01 4 5 -3 30.89 2.02 4 5 -3 36.98 2.05 4 5 -3 33.61 2.10 4 5 -3 35.01 2.04 4 5 -3 37.78 2.12 -4 -5 2 2.81 1.14 -4 -5 2 1.89 0.96 4 5 -2 2.38 0.81 4 5 -2 2.74 0.70 4 5 -2 2.47 0.75 4 5 -2 2.08 0.73 4 5 -2 3.06 0.73 4 5 -2 3.34 0.75 4 5 -1 24.67 1.55 4 5 -1 22.30 2.36 -4 -5 1 20.37 2.00 -4 -5 1 25.39 2.17 4 5 0 3.53 1.35 -4 -5 0 1.68 0.95 -4 -5 0 2.41 0.86 4 5 1 10.17 1.70 -4 -5 -1 8.83 1.07 -4 -5 -1 9.94 1.18 -4 -5 -2 9.72 1.26 4 5 2 10.14 1.72 -4 -5 -2 9.38 1.48 -4 -5 -2 11.04 1.14 4 5 3 222.63 10.22 -4 -5 -3 230.82 9.79 -4 -5 -3 204.88 9.45 -4 -5 -4 44.34 2.75 -4 -5 -4 44.45 3.12 -4 -5 -4 46.37 3.04 4 5 4 48.39 3.49 -4 -5 -5 1.59 1.13 -4 -5 -5 2.46 1.16 -4 -5 -5 2.40 1.08 -4 -5 -5 2.54 0.58 4 5 5 1.48 1.17 4 5 5 2.49 0.76 4 5 5 1.75 0.66 4 5 5 1.21 0.65 -4 -5 -6 0.81 0.99 4 5 6 1.67 0.86 -4 -5 -6 0.52 1.21 4 5 6 1.67 0.78 -4 -5 -6 0.70 1.00 -4 -5 -6 1.15 1.32 4 5 6 1.01 0.65 -4 -5 -6 1.28 0.59 4 5 6 1.28 0.67 4 5 6 0.36 0.66 4 5 6 1.39 0.72 -4 -5 -7 166.09 8.48 4 5 7 160.35 7.00 -4 -5 -7 144.67 7.56 -4 -5 -7 155.85 7.96 -4 -5 -7 150.98 8.19 4 5 7 172.56 6.82 4 5 7 162.37 6.92 -4 -5 -7 166.21 6.80 4 5 7 151.53 8.06 4 5 7 159.34 6.91 4 5 7 157.90 6.95 -4 -5 -8 39.19 3.61 4 5 8 41.12 2.57 -4 -5 -8 45.09 3.48 -4 -5 -8 43.83 2.41 4 5 8 41.81 3.37 4 5 8 45.76 2.54 4 5 8 43.96 2.51 -4 -5 -9 7.72 2.08 4 5 9 9.42 1.12 4 5 9 7.97 1.25 4 5 9 6.95 1.19 -4 -5 -9 7.49 1.90 -4 -5 -9 7.61 1.02 4 5 9 6.38 1.61 4 5 9 8.58 1.13 4 5 9 9.62 1.19 4 5 10 41.62 2.50 4 5 10 43.05 2.67 -4 -5 -10 41.02 2.49 -4 -5 -10 43.09 3.76 4 5 10 47.29 2.77 -4 -5 -10 43.22 3.54 4 5 11 23.80 1.82 -4 -5 -11 26.31 1.75 4 5 11 23.49 1.96 4 5 11 20.94 1.94 -4 -5 -11 25.17 3.01 -4 -5 -11 28.40 2.01 4 5 12 8.71 1.15 -4 -5 -12 7.90 1.07 4 5 12 9.82 1.35 -4 -5 -12 6.98 1.86 4 5 12 9.55 1.39 -4 -5 -12 11.11 1.99 -4 -5 -12 9.19 1.28 4 5 12 7.75 1.09 4 5 13 0.41 0.71 4 5 13 1.43 0.92 4 5 13 1.47 0.90 -4 -5 -13 1.95 0.84 4 5 13 1.49 0.68 -4 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42.25 3.78 -4 -6 6 31.77 3.25 -4 -6 6 39.58 3.84 4 6 -6 38.55 2.51 4 6 -6 38.19 2.44 4 6 -6 39.55 2.38 4 6 -6 41.15 2.45 -4 -6 5 3.61 1.54 -4 -6 5 4.65 1.61 4 6 -5 8.07 1.17 -4 -6 5 3.98 1.92 4 6 -5 6.61 1.19 -4 -6 4 19.99 2.39 4 6 -4 20.54 1.71 4 6 -4 20.93 1.64 4 6 -4 19.60 1.54 4 6 -3 19.83 1.44 -4 -6 3 16.88 2.08 4 6 -3 16.38 1.52 4 6 -3 21.91 1.62 4 6 -3 20.17 1.53 4 6 -3 21.33 1.65 -4 -6 2 112.10 6.35 4 6 -2 114.37 5.01 4 6 -2 102.97 5.13 4 6 -2 118.18 5.12 4 6 -2 116.49 5.16 4 6 -2 116.54 5.22 4 6 -2 116.29 5.24 -4 -6 1 1.06 1.21 4 6 -1 1.97 0.74 4 6 -1 1.25 1.44 4 6 -1 1.89 0.75 4 6 -1 5.01 0.94 -4 -6 0 603.58 24.94 4 6 0 605.58 23.90 4 6 0 620.95 25.58 4 6 0 623.67 24.09 4 6 0 621.09 24.04 4 6 0 619.10 24.07 -4 -6 -1 0.77 0.99 4 6 1 0.18 1.25 4 6 1 1.51 0.70 4 6 1 0.32 0.66 4 6 1 0.90 0.70 -4 -6 -2 35.52 2.83 4 6 2 33.71 2.06 -4 -6 -2 38.23 2.93 4 6 2 34.79 3.05 4 6 2 35.73 2.14 4 6 2 37.08 2.13 -4 -6 -3 26.62 2.38 4 6 3 23.07 1.74 -4 -6 -3 29.15 2.54 -4 -6 -3 27.42 1.60 4 6 3 28.13 2.87 4 6 3 28.28 1.82 4 6 3 27.29 1.78 -4 -6 -4 131.58 6.43 4 6 4 127.97 5.90 -4 -6 -4 140.93 6.91 -4 -6 -4 132.50 6.36 4 6 4 146.52 7.51 4 6 4 134.74 5.97 4 6 4 142.52 5.96 -4 -6 -5 23.83 2.45 -4 -6 -5 24.22 2.65 -4 -6 -5 25.77 2.38 4 6 5 25.47 2.65 4 6 5 23.60 1.65 4 6 5 22.07 1.63 4 6 6 199.57 8.53 -4 -6 -6 200.64 9.54 -4 -6 -6 196.26 9.65 -4 -6 -6 205.71 10.15 4 6 6 202.71 8.57 -4 -6 -6 204.56 8.30 4 6 6 215.35 10.21 4 6 6 211.56 8.58 4 6 6 206.22 8.62 -4 -6 -7 4.67 1.62 4 6 7 6.30 1.11 -4 -6 -7 5.76 1.71 4 6 7 6.12 1.04 -4 -6 -7 3.69 1.27 -4 -6 -7 6.84 1.71 -4 -6 -7 8.20 0.88 4 6 7 6.97 1.01 4 6 7 5.17 0.92 -4 -6 -8 12.27 2.34 4 6 8 12.00 1.38 4 6 8 12.05 1.37 -4 -6 -8 10.24 2.17 4 6 8 16.30 2.18 -4 -6 -8 13.71 1.37 4 6 8 11.08 1.26 4 6 8 12.31 1.30 -4 -6 -9 0.47 1.35 -4 -6 -9 -1.44 1.95 4 6 9 1.13 0.96 -4 -6 -9 -0.18 1.67 -4 -6 -9 0.68 0.89 4 6 9 -0.19 1.17 4 6 9 -0.21 0.79 4 6 9 1.04 0.82 -4 -6 -10 2.96 1.88 4 6 10 4.61 1.12 -4 -6 -10 2.92 1.40 -4 -6 -10 1.26 1.68 -4 -6 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11.34 1.34 4 7 -7 12.56 1.29 4 7 -7 11.67 1.20 -4 -7 7 9.58 1.13 -4 -7 6 2.42 1.65 -4 -7 6 1.99 1.77 4 7 -6 1.29 0.95 4 7 -6 1.78 0.94 4 7 -6 2.05 0.83 4 7 -6 1.52 0.79 -4 -7 5 7.05 1.63 -4 -7 5 7.92 2.29 4 7 -5 9.45 1.28 4 7 -5 8.96 1.19 4 7 -5 8.47 1.20 4 7 -5 10.33 1.22 4 7 -5 9.35 1.16 4 7 -4 49.25 2.66 -4 -7 4 51.40 3.72 -4 -7 4 51.71 4.38 4 7 -4 48.91 2.94 4 7 -4 55.44 2.91 4 7 -4 47.77 2.79 4 7 -4 47.91 2.85 4 7 -4 54.89 2.91 -4 -7 3 115.57 6.94 4 7 -3 122.42 5.52 -4 -7 3 131.15 7.50 4 7 -3 118.93 5.74 4 7 -3 131.53 5.66 4 7 -3 125.10 5.69 4 7 -3 133.18 5.83 -4 -7 2 88.46 5.68 4 7 -2 96.90 4.53 -4 -7 2 106.29 6.27 4 7 -2 98.07 4.56 4 7 -2 102.87 4.75 -4 -7 1 68.24 4.37 -4 -7 1 69.32 4.80 4 7 -1 69.62 3.36 4 7 -1 65.52 4.60 4 7 -1 69.07 3.50 4 7 -1 64.54 3.27 4 7 -1 70.60 3.52 4 7 0 -0.20 0.79 -4 -7 0 0.28 1.10 4 7 0 0.39 1.23 4 7 0 0.93 0.73 4 7 0 1.21 0.76 4 7 0 0.60 0.67 4 7 1 255.01 10.42 4 7 1 245.43 10.28 -4 -7 -1 245.32 11.64 4 7 1 245.33 11.95 4 7 1 255.59 10.50 4 7 1 258.43 10.39 4 7 1 258.75 10.47 -4 -7 -2 34.50 3.07 4 7 2 31.74 2.19 -4 -7 -2 39.49 3.14 4 7 2 40.67 3.53 4 7 2 35.93 2.24 4 7 2 35.07 2.13 4 7 2 36.34 2.20 -4 -7 -3 399.37 17.04 4 7 3 397.00 16.03 4 7 3 378.41 15.82 -4 -7 -3 397.01 16.93 -4 -7 -3 420.05 17.33 -4 -7 -3 410.74 15.74 4 7 3 426.24 17.91 4 7 3 406.98 16.10 4 7 3 394.39 15.95 4 7 3 413.84 16.04 4 7 4 1.30 0.88 4 7 4 1.65 0.85 4 7 4 1.44 0.86 -4 -7 -4 1.04 1.15 -4 -7 -4 4.31 1.47 4 7 4 0.63 1.32 -4 -7 -4 1.49 0.75 4 7 4 0.95 0.69 -4 -7 -5 0.89 1.39 -4 -7 -5 -0.21 1.24 -4 -7 -5 1.21 1.18 -4 -7 -5 0.53 1.13 4 7 5 0.64 1.34 -4 -7 -5 0.63 0.74 -4 -7 -6 20.47 2.57 4 7 6 17.65 1.39 -4 -7 -6 18.46 2.27 -4 -7 -6 17.18 2.45 -4 -7 -6 16.49 2.60 4 7 6 15.86 2.35 4 7 6 18.54 1.53 -4 -7 -7 116.46 7.09 4 7 7 117.43 5.48 4 7 7 112.24 5.34 -4 -7 -7 110.95 6.53 -4 -7 -7 121.78 6.74 -4 -7 -7 121.74 7.15 4 7 7 122.53 5.46 4 7 7 126.89 5.48 -4 -7 -8 11.38 2.29 4 7 8 15.83 1.55 4 7 8 8.24 1.22 -4 -7 -8 11.12 2.03 4 7 8 17.57 2.47 -4 -7 -8 12.92 1.34 4 7 8 12.77 1.33 4 7 8 12.15 1.31 -4 -7 -9 237.00 11.97 -4 -7 -9 241.37 11.76 4 7 9 242.47 10.05 4 7 9 224.03 9.91 -4 -7 -9 241.59 11.60 4 7 9 232.09 9.90 -4 -7 -9 245.97 10.00 4 7 9 214.44 11.52 4 7 9 250.38 10.00 -4 -7 -10 6.33 2.16 4 7 10 4.43 1.19 -4 -7 -10 3.51 1.86 -4 -7 -10 4.45 1.07 4 7 10 1.57 1.40 4 7 10 3.86 0.96 -4 -7 -11 0.84 1.74 4 7 11 0.48 0.99 -4 -7 -11 0.15 0.84 4 7 11 1.98 0.83 -4 -7 -12 3.54 1.89 -4 -7 -12 3.33 0.92 4 7 12 4.07 1.02 -4 -7 -12 3.56 0.94 4 7 12 4.03 0.80 -4 -7 -13 12.17 1.13 4 7 13 10.02 1.25 4 7 13 12.03 1.07 -4 -7 -13 12.14 1.26 4 7 13 10.31 1.23 4 7 14 6.60 0.97 -4 -7 -14 6.24 0.81 4 7 14 4.95 0.93 4 7 15 13.37 1.14 -4 -7 -15 14.80 1.10 4 7 16 10.36 0.86 -4 -7 -16 12.24 0.82 -4 -8 12 1.49 0.38 -4 -8 11 7.08 0.81 4 8 -11 4.61 0.64 -4 -8 10 41.56 2.17 4 8 -10 47.77 2.35 -4 -8 9 1.16 0.80 4 8 -9 3.43 0.84 4 8 -9 2.35 0.76 4 8 -9 1.38 0.71 -4 -8 8 0.82 1.51 -4 -8 8 0.74 0.76 4 8 -8 -0.07 0.78 4 8 -8 0.52 0.68 4 8 -8 0.35 0.73 4 8 -8 -0.31 0.52 -4 -8 7 30.08 3.30 -4 -8 7 26.23 1.83 -4 -8 7 20.86 3.10 4 8 -7 29.37 2.02 -4 -8 7 28.95 3.26 4 8 -7 27.83 1.92 4 8 -7 29.64 1.77 -4 -8 6 0.25 1.65 -4 -8 6 -0.05 0.81 -4 -8 6 1.23 1.71 4 8 -6 -0.58 0.94 4 8 -6 -0.37 0.74 4 8 -6 0.99 0.72 -4 -8 5 81.58 6.00 4 8 -5 89.06 4.09 -4 -8 5 92.64 6.23 4 8 -5 87.03 4.40 4 8 -5 88.93 4.31 4 8 -5 87.02 4.22 4 8 -5 91.42 4.46 -4 -8 4 25.68 3.24 4 8 -4 29.59 1.91 -4 -8 4 29.33 3.41 4 8 -4 31.11 2.03 4 8 -4 31.31 2.02 4 8 -4 28.05 2.08 -4 -8 3 44.36 4.20 4 8 -3 50.24 2.76 -4 -8 3 53.66 4.46 4 8 -3 47.46 2.74 4 8 -3 51.72 2.82 4 8 -3 49.95 2.91 -4 -8 2 15.98 2.70 -4 -8 2 17.45 2.75 4 8 -2 18.36 1.51 4 8 -2 19.39 1.64 -4 -8 1 120.19 7.01 4 8 -1 113.45 5.33 4 8 0 94.97 4.61 4 8 0 96.65 4.43 -4 -8 0 109.90 6.34 -4 -8 0 98.53 6.21 4 8 0 90.15 5.93 4 8 0 98.11 4.65 4 8 0 99.85 4.60 4 8 0 90.67 4.42 4 8 0 107.23 4.72 4 8 1 22.69 1.82 4 8 1 23.44 1.71 -4 -8 -1 30.31 3.04 -4 -8 -1 28.31 2.96 4 8 1 25.04 2.84 4 8 1 26.43 1.90 4 8 1 25.31 1.78 4 8 1 24.16 1.80 -4 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8 9 7.31 1.08 4 8 9 7.15 1.89 4 8 9 6.67 1.10 4 8 9 6.17 1.11 -4 -8 -10 1.73 1.89 4 8 10 1.26 0.98 4 8 10 1.28 0.85 -4 -8 -10 2.00 1.67 -4 -8 -10 1.80 0.89 4 8 10 0.80 0.77 -4 -8 -11 7.08 2.15 4 8 11 6.10 1.15 4 8 11 5.33 1.03 -4 -8 -11 7.25 1.15 4 8 11 7.56 1.01 4 8 11 8.01 1.12 -4 -8 -12 17.90 2.53 4 8 12 14.02 1.43 -4 -8 -12 11.85 1.31 4 8 12 15.75 1.24 -4 -8 -13 1.59 0.71 4 8 13 2.78 0.85 4 8 13 2.47 0.59 -4 -8 -13 3.09 0.79 -4 -8 -14 5.45 0.79 -4 -8 -14 5.90 0.74 4 8 14 5.81 0.92 -4 -8 -15 0.38 0.47 -4 -9 11 1.59 0.40 4 9 -11 0.84 0.30 -4 -9 10 4.83 0.74 4 9 -10 3.43 0.56 -4 -9 10 3.38 0.67 -4 -9 9 112.78 4.89 4 9 -9 124.64 5.10 -4 -9 8 13.75 1.18 4 9 -8 12.90 1.21 -4 -9 7 3.82 1.68 4 9 -7 2.89 0.77 4 9 -7 4.48 0.89 -4 -9 7 3.62 0.91 -4 -9 6 2.69 1.70 -4 -9 6 -0.23 1.82 -4 -9 6 0.22 1.54 4 9 -6 0.87 0.70 4 9 -6 3.29 0.88 4 9 -6 2.63 0.65 -4 -9 6 1.12 0.82 -4 -9 5 2.87 1.94 -4 -9 5 6.26 2.04 -4 -9 5 3.79 2.05 4 9 -5 4.51 0.92 4 9 -5 4.37 0.97 4 9 -5 4.75 0.87 -4 -9 5 5.04 1.01 -4 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1.86 -4 -9 -3 30.59 3.24 -4 -9 -3 22.18 2.59 -4 -9 -3 24.24 2.96 4 9 3 22.52 2.98 4 9 3 25.53 1.87 4 9 3 24.77 1.82 4 9 4 14.88 1.53 -4 -9 -4 16.09 1.39 4 9 4 13.48 1.34 4 9 4 13.44 1.43 -4 -9 -4 16.28 2.50 4 9 4 12.72 2.38 4 9 4 15.25 1.39 4 9 5 3.60 0.96 -4 -9 -5 2.72 1.78 -4 -9 -5 3.74 1.60 -4 -9 -5 2.95 1.89 -4 -9 -5 5.05 2.03 4 9 5 4.29 1.71 4 9 5 3.38 0.88 -4 -9 -6 2.19 1.78 -4 -9 -6 3.97 1.76 -4 -9 -6 2.82 1.53 -4 -9 -6 4.27 2.07 4 9 6 1.76 1.66 -4 -9 -6 3.11 0.85 4 9 6 1.87 0.82 4 9 6 3.80 0.93 -4 -9 -7 110.50 6.79 -4 -9 -7 94.43 6.36 -4 -9 -7 99.45 6.52 -4 -9 -7 97.60 6.59 4 9 7 106.04 4.90 -4 -9 -7 99.31 4.84 4 9 7 112.05 6.94 4 9 7 111.73 4.93 4 9 7 101.45 4.79 -4 -9 -8 31.84 3.39 -4 -9 -8 33.89 3.49 4 9 8 28.37 2.09 -4 -9 -8 35.37 3.53 -4 -9 -8 27.81 2.04 4 9 8 30.93 2.08 4 9 8 31.16 2.07 -4 -9 -9 70.43 5.25 -4 -9 -9 81.03 5.42 4 9 9 68.04 3.69 4 9 9 70.82 3.60 4 9 9 75.20 3.68 -4 -9 -10 124.53 7.07 4 9 10 116.45 5.42 4 9 10 118.85 5.36 -4 -9 -11 2.36 1.67 4 9 11 3.05 0.94 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5 2 7 35.13 2.28 5 2 7 34.38 2.06 -5 -2 -7 30.02 3.04 5 2 7 39.01 2.19 5 2 7 32.68 2.85 5 2 7 33.76 2.12 -5 -2 -7 33.87 2.01 5 2 7 31.47 1.99 5 2 7 32.28 2.08 5 2 8 65.91 3.57 5 2 8 74.62 3.72 5 2 8 68.79 3.40 -5 -2 -8 72.67 4.89 5 2 8 74.29 3.53 5 2 8 71.12 3.53 -5 -2 -8 71.41 3.34 5 2 8 56.78 3.23 5 2 8 67.36 3.45 5 2 9 30.97 2.17 5 2 9 27.78 2.15 5 2 9 28.29 1.93 -5 -2 -9 30.10 3.14 5 2 9 30.26 2.05 -5 -2 -9 32.71 2.12 5 2 9 30.39 1.96 5 2 10 164.34 7.12 5 2 10 167.92 7.22 5 2 10 144.11 6.73 -5 -2 -10 146.53 8.58 5 2 10 148.05 6.84 5 2 10 169.87 7.03 -5 -2 -10 173.24 7.12 -5 -2 -10 157.59 6.93 5 2 11 7.35 1.30 5 2 11 10.18 1.39 -5 -2 -11 11.23 2.16 5 2 11 7.77 1.05 -5 -2 -11 9.75 1.23 5 2 11 9.85 1.22 5 2 12 2.16 0.96 -5 -2 -12 3.44 1.53 5 2 12 1.79 0.90 -5 -2 -12 1.35 0.75 5 2 12 -0.11 0.71 -5 -2 -12 1.51 0.77 -5 -2 -12 0.53 0.72 5 2 12 1.05 0.82 5 2 13 1.96 0.91 5 2 13 2.54 0.94 -5 -2 -13 1.37 0.70 -5 -2 -13 1.39 0.74 -5 -2 -13 1.30 0.67 -5 -2 -14 34.57 1.92 -5 -2 -14 33.93 1.84 5 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3 -6 123.16 5.49 5 3 -6 114.13 5.24 -5 -3 5 34.41 2.99 -5 -3 5 28.18 3.11 -5 -3 5 31.65 2.98 5 3 -5 33.67 2.11 -5 -3 5 28.38 3.16 -5 -3 5 32.52 3.32 5 3 -5 35.91 2.30 5 3 -5 35.00 2.05 5 3 -5 31.81 2.19 5 3 -5 32.77 2.03 -5 -3 4 5.16 1.38 -5 -3 4 3.38 1.02 -5 -3 4 4.95 1.41 5 3 -4 2.96 0.89 -5 -3 4 3.17 1.29 -5 -3 4 3.27 1.42 5 3 -4 3.05 0.80 5 3 -4 3.06 0.91 5 3 -4 3.14 0.87 5 3 -4 3.96 0.81 5 3 -4 3.83 0.88 -5 -3 3 1.16 0.94 5 3 -3 0.51 0.70 -5 -3 3 0.96 0.98 -5 -3 3 1.11 0.82 -5 -3 3 0.40 1.11 5 3 -3 0.30 0.70 5 3 -3 0.74 0.65 5 3 -3 0.52 0.72 5 3 -3 1.58 0.79 5 3 -3 0.90 0.78 -5 -3 2 123.14 6.32 -5 -3 2 123.80 6.15 5 3 -2 130.59 5.66 5 3 -2 124.81 6.92 5 3 -2 129.35 5.84 5 3 -2 132.02 5.85 5 3 -2 136.62 5.79 5 3 -2 127.05 5.78 5 3 -2 138.29 5.72 -5 -3 1 163.20 7.59 5 3 -1 168.75 8.30 5 3 -1 158.68 6.95 5 3 -1 162.12 6.90 5 3 -1 165.26 6.99 5 3 -1 161.25 6.90 5 3 -1 158.35 6.94 -5 -3 0 433.06 17.56 5 3 0 438.62 17.11 5 3 0 416.43 18.54 5 3 0 449.37 17.16 5 3 0 417.31 17.13 5 3 0 437.96 17.10 5 3 0 433.76 17.12 5 3 0 428.69 17.17 5 3 1 43.13 2.36 5 3 1 39.57 3.26 5 3 1 45.22 2.41 5 3 1 44.29 2.36 5 3 1 44.14 2.37 5 3 1 39.65 2.37 5 3 2 37.20 2.07 5 3 2 36.52 3.03 5 3 2 34.35 2.04 5 3 2 34.09 2.03 5 3 2 32.65 2.07 -5 -3 -3 12.49 1.51 5 3 3 13.61 1.23 -5 -3 -3 11.87 1.47 5 3 3 12.95 1.84 5 3 3 12.92 1.22 5 3 3 13.57 1.20 5 3 3 13.29 1.25 -5 -3 -4 33.35 2.55 -5 -3 -4 28.90 2.46 -5 -3 -4 32.26 2.42 5 3 4 36.00 2.01 5 3 4 27.73 2.71 5 3 4 31.14 2.01 5 3 4 30.24 1.96 -5 -3 -5 3.50 1.25 -5 -3 -5 4.10 1.26 -5 -3 -5 2.00 1.18 5 3 5 3.01 0.80 5 3 5 2.84 1.12 5 3 5 2.22 0.73 5 3 5 1.55 0.75 5 3 5 2.07 0.74 5 3 5 2.98 0.84 5 3 6 149.96 6.59 -5 -3 -6 152.76 7.67 5 3 6 155.70 6.71 -5 -3 -6 134.17 7.30 -5 -3 -6 161.31 7.78 5 3 6 159.90 6.62 5 3 6 169.35 6.68 -5 -3 -6 153.61 6.34 5 3 6 147.87 6.49 5 3 6 134.05 6.61 5 3 7 42.27 2.50 -5 -3 -7 36.35 3.25 5 3 7 43.28 2.60 5 3 7 41.31 2.46 5 3 7 46.45 2.49 -5 -3 -7 41.61 2.34 5 3 7 36.98 2.26 5 3 7 46.81 2.55 5 3 8 1.68 0.90 -5 -3 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5 4 -10 44.40 2.62 -5 -4 9 15.53 2.66 -5 -4 9 16.41 2.63 5 4 -9 19.94 1.61 -5 -4 9 15.72 1.62 5 4 -9 20.36 1.66 5 4 -9 18.95 1.47 -5 -4 8 1.48 1.55 -5 -4 8 -0.46 1.59 -5 -4 8 -1.24 1.52 5 4 -8 0.91 0.82 -5 -4 8 0.08 0.98 5 4 -8 0.18 0.63 5 4 -8 0.66 0.77 5 4 -8 0.20 0.72 -5 -4 7 3.77 1.62 -5 -4 7 3.78 1.52 -5 -4 7 1.53 1.59 5 4 -7 2.15 0.89 -5 -4 7 5.30 1.17 5 4 -7 3.20 0.78 5 4 -7 2.31 0.95 -5 -4 6 1.98 1.62 -5 -4 6 7.60 1.93 -5 -4 6 6.92 1.65 -5 -4 6 5.28 1.74 5 4 -6 5.54 1.05 5 4 -6 3.93 0.92 5 4 -6 5.32 1.06 -5 -4 5 38.88 3.14 -5 -4 5 30.83 3.14 5 4 -5 40.35 2.44 -5 -4 5 36.15 3.55 -5 -4 5 40.70 3.77 5 4 -5 43.48 2.61 5 4 -5 36.67 2.30 5 4 -5 46.66 2.58 5 4 -5 42.86 2.44 -5 -4 4 88.34 4.93 -5 -4 4 69.94 4.71 5 4 -4 81.43 3.96 5 4 -4 79.01 3.96 5 4 -4 83.65 4.17 5 4 -4 82.92 4.08 5 4 -4 84.40 3.99 -5 -4 3 5.58 1.24 -5 -4 3 5.13 1.53 5 4 -3 4.30 0.89 5 4 -3 4.16 0.85 5 4 -3 3.97 0.84 5 4 -3 4.72 0.97 5 4 -3 3.20 0.89 5 4 -3 4.11 0.93 -5 -4 2 46.95 3.54 5 4 -2 44.66 2.47 5 4 -2 47.78 2.68 5 4 -2 43.32 2.53 5 4 -2 51.24 2.72 5 4 -2 46.72 2.59 -5 -4 1 10.77 1.71 -5 -4 1 9.75 1.31 5 4 -1 9.49 1.14 5 4 -1 11.12 1.12 5 4 -1 11.67 1.19 5 4 -1 10.17 1.13 -5 -4 0 17.27 2.00 5 4 0 18.70 1.51 5 4 0 20.57 1.51 5 4 0 20.06 1.55 5 4 0 19.06 1.48 5 4 0 23.35 1.52 5 4 0 20.46 1.55 5 4 1 32.81 2.04 5 4 1 33.58 2.03 5 4 1 32.18 2.02 5 4 1 36.27 2.02 5 4 1 30.13 2.03 5 4 1 35.03 2.03 -5 -4 -2 155.55 7.00 5 4 2 154.01 6.52 5 4 2 153.50 6.53 5 4 2 150.31 6.42 5 4 2 145.26 6.55 5 4 2 149.43 6.50 5 4 3 16.65 1.35 5 4 3 14.74 1.30 5 4 3 16.79 1.41 5 4 3 15.43 1.31 5 4 4 12.80 1.17 5 4 4 10.31 1.11 5 4 4 9.47 1.13 5 4 4 9.17 1.07 -5 -4 -5 25.43 2.48 5 4 5 28.82 1.82 5 4 5 25.69 1.75 5 4 5 27.19 1.75 5 4 5 22.96 1.68 5 4 5 25.04 1.85 5 4 5 26.56 1.83 5 4 6 107.10 5.09 5 4 6 113.06 5.25 -5 -4 -6 115.96 6.28 5 4 6 128.96 5.25 5 4 6 113.26 5.16 -5 -4 -6 116.02 4.97 5 4 6 108.26 5.05 5 4 6 116.44 5.31 5 4 6 110.45 5.23 5 4 7 39.13 2.34 5 4 7 39.97 2.50 5 4 7 41.63 2.43 -5 -4 -7 44.85 2.26 5 4 7 36.77 2.20 5 4 8 3.20 0.95 -5 -4 -8 3.62 1.76 5 4 8 3.75 1.08 -5 -4 -8 4.38 1.56 5 4 8 4.53 1.06 5 4 8 3.79 0.84 -5 -4 -8 3.71 0.75 5 4 8 4.24 0.93 5 4 9 12.95 1.40 -5 -4 -9 17.44 2.40 5 4 9 14.53 1.54 -5 -4 -9 16.14 2.31 -5 -4 -9 13.31 2.27 5 4 9 15.19 1.34 5 4 9 17.16 1.47 5 4 10 37.80 2.40 -5 -4 -10 43.96 3.53 5 4 10 41.71 2.61 -5 -4 -10 40.95 3.79 -5 -4 -10 38.31 3.64 5 4 10 35.33 2.23 5 4 10 43.13 2.47 5 4 10 35.17 2.35 -5 -4 -11 6.34 1.78 5 4 11 5.12 1.20 -5 -4 -11 6.94 1.84 5 4 11 6.25 1.07 5 4 11 5.04 1.03 5 4 11 3.86 0.91 5 4 12 11.75 1.33 5 4 12 11.25 1.42 5 4 12 12.52 1.27 5 4 12 9.91 1.08 5 4 13 5.62 0.96 5 4 13 6.39 1.10 -5 -4 -13 5.99 0.99 -5 -4 -13 4.40 0.83 5 4 14 15.02 1.29 5 4 14 16.26 1.43 -5 -4 -14 14.51 1.24 5 4 14 15.54 1.25 -5 -4 -14 15.87 1.37 -5 -4 -14 14.72 1.16 5 4 15 3.88 0.82 -5 -4 -15 4.00 0.71 5 4 15 3.40 0.61 -5 -4 -15 3.64 0.60 -5 -4 -16 32.59 1.68 -5 -5 12 6.53 0.78 5 5 -12 5.14 0.68 5 5 -11 2.01 0.66 5 5 -11 3.33 0.63 -5 -5 11 3.10 0.66 5 5 -10 2.67 0.84 5 5 -10 2.58 0.78 -5 -5 10 2.32 0.88 5 5 -9 42.31 2.48 5 5 -9 41.79 2.47 -5 -5 9 42.71 2.57 5 5 -9 42.11 2.35 -5 -5 8 13.48 2.46 5 5 -8 16.63 1.50 -5 -5 8 13.66 2.61 5 5 -8 13.12 1.36 -5 -5 8 13.62 1.51 5 5 -8 11.87 1.36 5 5 -8 13.90 1.33 -5 -5 7 124.27 8.08 -5 -5 7 136.96 7.96 5 5 -7 142.55 6.39 -5 -5 7 129.93 8.13 -5 -5 7 149.96 6.47 5 5 -7 145.79 6.49 5 5 -7 151.16 6.36 5 5 -7 135.51 6.32 -5 -5 6 -0.74 1.54 -5 -5 6 -0.43 1.41 -5 -5 6 0.95 1.22 -5 -5 6 1.02 1.58 5 5 -6 0.84 0.80 5 5 -6 0.17 0.83 -5 -5 5 32.40 3.34 -5 -5 5 31.87 3.19 -5 -5 5 30.82 3.23 5 5 -5 30.42 2.10 5 5 -5 31.10 2.23 5 5 -5 37.21 2.26 -5 -5 4 2.92 1.41 -5 -5 4 -0.22 1.03 -5 -5 4 2.50 1.55 -5 -5 4 1.14 1.28 5 5 -4 2.58 0.89 5 5 -4 2.83 0.91 -5 -5 3 0.38 1.08 -5 -5 3 0.20 0.99 5 5 -3 -0.13 0.76 5 5 -3 0.97 0.83 5 5 -3 -0.07 0.71 5 5 -3 0.15 0.79 -5 -5 2 23.58 2.49 -5 -5 2 17.80 2.26 5 5 -2 20.86 1.59 5 5 -2 21.96 1.75 5 5 -2 23.55 1.70 5 5 -2 25.29 1.80 5 5 -2 21.70 1.63 5 5 -2 24.21 1.72 -5 -5 1 542.08 23.26 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2.45 0.89 5 6 -2 2.59 0.87 5 6 -2 2.34 0.75 -5 -6 1 79.95 5.00 5 6 -1 79.41 3.93 5 6 -1 87.95 3.92 5 6 -1 72.11 3.59 5 6 -1 75.56 3.62 5 6 -1 70.91 3.70 5 6 -1 80.98 3.89 -5 -6 0 2.44 0.89 -5 -6 0 1.90 1.21 5 6 0 1.46 0.80 5 6 0 0.57 0.78 5 6 0 1.98 0.72 5 6 0 0.76 0.65 5 6 0 0.81 0.75 -5 -6 -1 39.67 3.15 -5 -6 -1 36.17 3.17 -5 -6 -1 36.83 2.88 5 6 1 39.03 2.36 5 6 1 41.31 2.32 5 6 1 36.48 2.12 5 6 1 34.06 2.04 5 6 1 36.50 2.28 -5 -6 -2 5.64 1.43 -5 -6 -2 2.92 1.47 5 6 2 3.19 1.47 5 6 2 2.22 0.81 5 6 2 2.62 0.81 5 6 2 3.63 0.73 5 6 2 2.61 0.66 5 6 2 1.45 0.73 5 6 2 3.59 0.88 -5 -6 -3 6.14 1.46 -5 -6 -3 7.08 1.41 -5 -6 -3 3.73 1.31 5 6 3 4.88 1.59 5 6 3 7.40 1.05 5 6 3 7.24 0.89 5 6 3 8.25 0.90 5 6 3 7.41 1.06 5 6 3 6.07 1.00 -5 -6 -4 17.65 2.16 5 6 4 14.36 1.43 -5 -6 -4 16.37 1.92 -5 -6 -4 14.65 1.96 5 6 4 17.00 1.40 5 6 4 20.86 2.52 5 6 4 16.24 1.46 5 6 4 15.53 1.29 5 6 4 16.82 1.30 5 6 4 16.92 1.46 -5 -6 -5 9.31 1.77 -5 -6 -5 12.79 1.70 5 6 5 10.82 2.03 5 6 5 9.17 1.09 5 6 5 10.10 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107.02 6.20 -5 -7 -7 94.22 6.30 5 7 7 106.45 4.74 -5 -7 -7 109.44 4.72 5 7 7 88.33 6.13 5 7 7 98.68 4.64 5 7 7 86.41 4.46 5 7 7 103.94 4.80 -5 -7 -8 4.57 1.89 5 7 8 4.45 1.15 5 7 8 2.84 0.92 -5 -7 -8 5.50 1.80 5 7 8 5.18 1.65 5 7 8 3.36 0.93 5 7 8 3.51 0.88 -5 -7 -9 -0.24 1.63 5 7 9 1.05 1.01 5 7 9 -0.07 0.83 -5 -7 -9 -0.18 1.54 5 7 9 -0.20 1.23 5 7 9 0.07 0.83 5 7 9 1.41 0.86 5 7 10 10.25 1.35 5 7 10 10.07 1.30 -5 -7 -10 10.66 2.04 5 7 10 12.81 1.29 -5 -7 -10 13.90 1.37 5 7 11 0.67 0.92 -5 -7 -11 1.55 0.82 5 7 11 0.06 0.74 -5 -7 -12 32.36 1.86 5 7 12 35.45 2.21 -5 -7 -12 33.16 2.13 5 7 13 1.54 0.59 -5 -7 -13 1.48 0.61 5 7 13 1.21 0.64 5 7 14 2.65 0.69 -5 -7 -14 3.07 0.68 -5 -7 -14 1.44 0.55 5 7 14 2.43 0.52 -5 -7 -14 2.28 0.53 5 7 14 2.18 0.52 -5 -7 -15 0.68 0.47 -5 -8 9 45.00 2.21 -5 -8 9 50.02 2.37 5 8 -9 53.25 2.46 -5 -8 8 1.70 0.66 5 8 -8 2.88 0.71 5 8 -8 2.81 0.60 -5 -8 7 7.15 1.91 -5 -8 7 6.39 0.88 -5 -8 7 6.11 1.03 5 8 -7 7.28 1.00 5 8 -7 7.04 0.88 -5 -8 6 1.82 1.71 -5 -8 6 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1.95 0.70 6 3 12 2.17 0.81 6 3 13 5.68 0.85 6 3 14 11.53 1.00 -6 -3 -15 5.32 0.69 6 3 15 3.25 0.57 6 4 -11 0.35 0.44 6 4 -11 0.20 0.42 6 4 -10 12.52 1.02 6 4 -10 10.30 1.02 -6 -4 9 27.14 1.72 6 4 -9 32.33 1.85 6 4 -9 33.53 1.97 6 4 -8 60.06 3.19 -6 -4 7 7.70 1.85 6 4 -7 6.08 1.08 6 4 -7 4.41 0.93 -6 -4 6 0.98 1.42 -6 -4 6 -0.22 1.32 6 4 -6 0.71 0.71 6 4 -6 0.50 0.80 6 4 -6 1.68 0.86 -6 -4 5 1.24 1.46 -6 -4 5 0.70 1.21 6 4 -5 1.35 0.74 -6 -4 5 -0.25 1.28 6 4 -5 0.77 0.81 6 4 -5 1.46 0.85 6 4 -5 1.50 0.66 -6 -4 4 19.74 2.24 -6 -4 4 16.13 2.57 6 4 -4 20.28 1.56 -6 -4 4 18.02 2.65 6 4 -4 22.21 1.81 6 4 -4 25.86 1.88 6 4 -4 23.55 1.60 -6 -4 3 2.82 1.11 -6 -4 3 0.92 1.23 -6 -4 3 3.02 1.40 6 4 -3 1.11 0.70 6 4 -3 1.27 0.84 6 4 -3 2.16 0.87 6 4 -3 1.72 0.74 -6 -4 2 25.67 2.92 -6 -4 2 28.75 3.09 6 4 -2 25.79 1.75 6 4 -2 28.76 2.06 6 4 -2 30.03 2.00 6 4 -2 27.51 2.03 6 4 -2 29.30 1.99 6 4 -2 29.41 1.92 -6 -4 1 164.69 8.94 -6 -4 1 149.17 8.61 -6 -4 1 169.46 9.04 6 4 -1 177.88 7.62 6 4 -1 172.76 7.54 6 4 -1 173.16 7.60 6 4 -1 182.72 7.56 6 4 -1 173.11 7.57 6 4 -1 178.60 7.45 -6 -4 0 8.04 1.55 6 4 0 6.44 1.06 6 4 0 5.83 0.98 6 4 0 5.98 1.08 6 4 0 6.50 1.06 6 4 0 6.25 1.11 6 4 0 8.25 1.08 -6 -4 -1 166.58 8.91 6 4 1 183.25 7.83 6 4 1 210.14 8.26 6 4 1 185.14 8.13 6 4 1 194.92 8.12 6 4 1 199.77 8.25 6 4 2 35.09 2.09 6 4 2 38.65 2.30 6 4 2 36.26 2.32 6 4 3 11.44 1.12 6 4 3 8.69 1.17 6 4 3 8.63 1.11 6 4 3 10.01 1.19 6 4 3 9.50 1.12 6 4 3 9.91 1.15 6 4 3 9.08 1.20 6 4 3 8.49 1.16 -6 -4 -4 12.18 1.79 -6 -4 -4 7.89 1.48 6 4 4 12.11 1.31 6 4 4 10.43 1.16 6 4 4 8.14 1.17 6 4 4 10.39 1.16 6 4 4 12.60 1.24 6 4 4 12.83 1.36 6 4 4 11.77 1.26 -6 -4 -5 74.40 4.91 -6 -4 -5 75.59 4.83 -6 -4 -5 74.27 4.80 6 4 5 87.85 4.10 6 4 5 75.31 3.85 6 4 5 80.38 3.82 6 4 5 87.67 4.09 6 4 5 89.71 4.18 6 4 5 78.00 4.03 -6 -4 -6 120.79 6.96 -6 -4 -6 110.08 6.79 6 4 6 142.96 5.98 -6 -4 -6 128.70 5.64 6 4 6 126.34 5.81 6 4 6 128.92 5.76 6 4 6 120.65 5.57 6 4 6 132.63 5.94 6 4 6 146.00 6.05 6 4 6 129.32 5.93 -6 -4 -7 80.63 5.26 -6 -4 -7 86.04 5.64 -6 -4 -7 83.21 5.36 6 4 7 86.77 4.17 -6 -4 -7 81.12 3.90 6 4 7 81.65 4.07 6 4 7 82.67 3.96 -6 -4 -8 48.13 4.05 -6 -4 -8 36.61 3.60 -6 -4 -8 45.10 2.58 6 4 8 46.41 2.64 -6 -4 -8 46.79 2.46 6 4 8 40.93 2.35 -6 -4 -9 6.18 1.75 -6 -4 -9 7.58 1.97 6 4 9 10.78 1.21 -6 -4 -9 9.52 1.18 6 4 9 10.58 1.29 6 4 9 10.10 1.23 -6 -4 -10 18.93 2.53 6 4 10 15.46 1.39 6 4 10 15.65 1.47 -6 -4 -10 16.54 1.47 6 4 10 18.39 1.47 -6 -4 -11 1.50 0.71 6 4 11 0.75 0.75 6 4 11 0.70 0.65 -6 -4 -12 27.02 1.67 6 4 12 29.88 1.90 -6 -4 -12 29.69 1.89 6 4 12 26.35 1.58 -6 -4 -13 4.82 0.71 6 4 13 5.28 0.84 -6 -4 -15 0.29 0.53 6 4 15 0.27 0.36 6 4 15 -0.03 0.38 -6 -5 11 38.36 1.67 6 5 -11 28.49 1.49 6 5 -10 0.28 0.49 6 5 -9 2.33 0.67 6 5 -9 3.52 0.73 -6 -5 8 1.01 1.41 6 5 -8 1.25 0.69 -6 -5 8 0.25 0.83 6 5 -8 0.57 0.64 -6 -5 7 24.97 2.99 -6 -5 7 27.60 2.02 -6 -5 6 25.40 3.14 -6 -5 6 27.76 1.99 6 5 -6 26.31 1.96 6 5 -6 29.38 1.97 6 5 -6 27.28 1.78 -6 -5 5 3.77 1.55 6 5 -5 4.57 0.92 6 5 -5 5.46 1.05 6 5 -5 7.41 1.14 6 5 -5 4.15 0.84 -6 -5 4 5.24 1.74 -6 -5 4 9.18 1.90 -6 -5 4 8.18 1.80 6 5 -4 6.48 1.03 -6 -5 4 7.42 1.89 6 5 -4 7.54 1.16 6 5 -4 8.48 1.18 6 5 -4 8.39 1.06 -6 -5 3 51.79 4.30 -6 -5 3 43.80 3.93 -6 -5 3 47.36 4.12 -6 -5 3 48.90 4.28 6 5 -3 48.42 2.70 6 5 -3 55.01 3.02 6 5 -3 52.45 2.87 6 5 -3 52.73 2.98 -6 -5 2 3.95 1.53 -6 -5 2 1.50 1.23 -6 -5 2 4.18 1.43 6 5 -2 2.58 0.76 6 5 -2 4.57 1.04 6 5 -2 3.46 0.92 6 5 -2 4.49 1.03 6 5 -1 187.25 8.14 6 5 -1 198.37 8.12 6 5 -1 186.78 8.12 -6 -5 0 8.31 1.59 6 5 0 6.76 1.11 6 5 0 8.13 1.17 6 5 0 6.44 1.12 6 5 0 7.57 1.10 6 5 0 7.14 1.13 -6 -5 -1 181.47 9.26 6 5 1 180.34 7.99 6 5 1 201.21 8.37 6 5 1 201.38 8.37 6 5 1 191.86 8.35 6 5 1 211.20 8.37 6 5 2 37.43 2.29 6 5 2 44.38 2.55 6 5 2 41.19 2.50 6 5 2 41.79 2.41 6 5 2 44.25 2.44 6 5 2 41.59 2.55 6 5 2 43.89 2.53 6 5 3 9.10 1.18 6 5 3 9.84 1.12 6 5 3 9.41 1.11 6 5 3 11.97 1.19 6 5 3 8.79 1.20 6 5 3 11.01 1.26 -6 -5 -4 40.76 3.32 -6 -5 -4 49.66 3.74 6 5 4 50.75 2.64 6 5 4 50.85 2.94 6 5 4 49.79 2.83 -6 -5 -5 19.67 2.41 -6 -5 -5 21.29 2.35 6 5 5 20.90 1.65 6 5 5 20.01 1.67 6 5 5 21.55 1.49 6 5 5 25.32 1.88 6 5 5 18.96 1.69 -6 -5 -6 36.12 3.39 -6 -5 -6 36.00 3.19 -6 -5 -6 32.99 3.14 6 5 6 35.45 2.24 -6 -5 -6 39.06 2.16 6 5 6 31.43 2.11 6 5 6 38.65 2.42 6 5 6 35.01 2.36 -6 -5 -7 0.81 1.44 -6 -5 -7 1.40 1.57 -6 -5 -7 2.89 1.44 -6 -5 -7 2.34 0.73 6 5 7 0.60 0.64 6 5 7 1.69 0.84 6 5 7 2.63 0.94 -6 -5 -8 11.68 2.05 -6 -5 -8 7.91 2.03 -6 -5 -8 10.87 1.98 -6 -5 -8 10.23 2.10 -6 -5 -8 10.83 1.16 6 5 8 10.36 1.05 6 5 8 9.95 1.24 6 5 8 11.45 1.31 -6 -5 -9 57.83 4.54 -6 -5 -9 47.38 4.18 -6 -5 -9 56.16 2.98 6 5 9 56.74 3.07 6 5 10 22.04 1.68 -6 -5 -10 18.84 1.53 6 5 10 17.76 1.58 6 5 11 41.57 2.35 -6 -5 -11 36.60 2.35 -6 -5 -11 36.31 2.22 6 5 11 36.31 2.22 -6 -5 -12 7.43 1.01 6 5 12 5.45 0.93 6 5 12 5.23 0.80 -6 -5 -13 2.93 0.67 6 5 13 3.10 0.71 -6 -5 -14 1.88 0.53 6 5 14 1.81 0.56 6 6 -10 2.35 0.47 6 6 -8 73.38 3.50 6 6 -8 76.74 3.56 -6 -6 7 17.09 2.25 -6 -6 7 16.80 1.57 6 6 -7 18.90 1.46 6 6 -7 19.66 1.52 6 6 -7 18.63 1.36 -6 -6 6 12.42 2.00 -6 -6 6 12.33 2.35 -6 -6 6 14.71 1.44 6 6 -6 19.14 1.53 -6 -6 5 2.88 1.71 -6 -6 5 0.85 1.24 6 6 -5 1.28 0.83 -6 -6 4 27.45 3.27 6 6 -4 34.57 2.09 6 6 -4 32.94 2.24 -6 -6 3 11.51 2.22 6 6 -3 13.01 1.43 6 6 -3 10.71 1.21 -6 -6 2 0.21 1.22 6 6 -2 0.43 0.83 6 6 -2 0.68 0.76 -6 -6 1 32.28 3.10 6 6 -1 32.26 2.23 6 6 -1 32.23 2.19 6 6 -1 33.95 2.17 -6 -6 0 158.60 8.74 -6 -6 0 182.32 8.89 6 6 0 171.19 7.36 6 6 0 182.26 7.82 6 6 0 192.28 7.81 6 6 0 177.84 7.70 -6 -6 -1 56.79 4.35 6 6 1 56.73 2.99 6 6 1 56.24 3.23 6 6 1 64.23 3.29 6 6 1 63.69 3.29 6 6 1 60.56 3.23 -6 -6 -2 1.16 1.28 6 6 2 0.24 0.81 6 6 2 -0.39 0.77 6 6 2 -0.36 0.71 6 6 2 -0.56 0.80 6 6 2 0.16 0.75 6 6 3 1.48 0.89 6 6 3 2.26 0.82 6 6 3 2.01 0.68 6 6 3 1.23 0.81 6 6 3 1.50 0.83 -6 -6 -4 2.06 1.39 -6 -6 -4 -0.64 1.21 6 6 4 0.46 0.81 6 6 4 0.84 0.67 6 6 4 0.42 0.78 6 6 4 0.48 0.82 -6 -6 -5 62.15 4.51 6 6 5 61.99 3.26 6 6 5 61.55 3.20 6 6 5 65.99 3.48 6 6 5 63.42 3.40 -6 -6 -6 0.20 1.33 -6 -6 -6 0.38 1.25 -6 -6 -6 2.12 1.43 -6 -6 -6 1.30 1.53 6 6 6 1.53 0.76 6 6 6 1.67 0.83 6 6 6 3.04 0.82 6 6 6 1.10 0.88 6 6 6 1.87 0.94 -6 -6 -7 167.18 8.89 -6 -6 -7 141.37 8.46 -6 -6 -7 144.18 8.54 6 6 7 167.99 7.18 6 6 7 157.87 6.93 6 6 7 168.00 7.12 6 6 7 173.47 7.34 6 6 7 173.77 7.36 -6 -6 -8 3.87 1.48 -6 -6 -8 3.89 1.63 -6 -6 -8 5.43 1.85 6 6 8 4.11 0.99 6 6 8 2.39 0.78 6 6 8 2.77 0.96 -6 -6 -9 2.23 1.48 -6 -6 -9 2.90 1.81 6 6 9 3.44 0.94 6 6 9 1.67 0.72 6 6 9 3.45 0.96 -6 -6 -10 2.08 1.64 6 6 10 1.96 0.84 6 6 10 1.77 0.70 -6 -6 -11 47.28 2.75 6 6 11 49.97 2.70 6 6 12 34.43 1.95 -6 -6 -12 32.63 2.01 6 6 12 27.99 1.83 6 6 12 29.39 1.82 6 6 13 7.94 0.88 6 6 13 5.93 0.74 6 6 13 6.36 0.70 -6 -6 -14 6.66 0.69 -6 -7 9 5.40 0.66 6 7 -9 5.92 0.60 6 7 -8 4.30 0.65 6 7 -7 3.92 0.82 -6 -7 6 10.24 1.26 6 7 -6 11.93 1.18 -6 -7 5 20.60 2.91 6 7 -5 22.58 1.72 6 7 -5 22.75 1.65 -6 -7 4 3.52 1.68 -6 -7 4 0.83 1.26 6 7 -4 1.55 0.79 6 7 -4 1.85 0.80 -6 -7 3 4.69 1.65 6 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65.29 3.35 7 3 1 63.90 3.18 -7 -3 -2 0.80 1.21 7 3 2 0.19 0.64 7 3 2 0.55 0.73 7 3 2 0.88 0.78 7 3 2 0.65 0.75 7 3 2 0.24 0.72 7 3 2 0.62 0.73 -7 -3 -3 2.36 1.24 7 3 3 0.96 0.78 7 3 3 1.70 0.73 7 3 3 1.94 0.79 7 3 3 0.95 0.63 7 3 3 1.83 0.76 7 3 3 1.81 0.88 -7 -3 -4 21.89 2.57 -7 -3 -4 24.73 2.91 7 3 4 27.16 1.76 7 3 4 26.55 1.94 7 3 4 23.61 1.61 7 3 4 26.58 1.90 7 3 4 29.26 1.99 7 3 4 28.59 2.00 -7 -3 -5 42.51 3.56 7 3 5 40.98 2.52 7 3 5 39.41 2.35 -7 -3 -5 42.96 2.37 7 3 5 39.58 2.43 7 3 5 39.26 2.34 7 3 5 42.06 2.53 7 3 5 42.59 2.55 -7 -3 -6 7.43 1.79 7 3 6 6.42 1.08 -7 -3 -6 5.87 0.96 7 3 6 5.59 0.90 7 3 6 8.05 1.11 -7 -3 -7 21.51 2.72 7 3 7 24.97 1.77 7 3 7 26.54 1.88 -7 -3 -7 22.99 1.68 7 3 7 21.98 1.67 7 3 7 26.97 1.91 7 3 8 1.10 0.74 -7 -3 -8 -0.07 0.67 -7 -3 -8 0.48 0.63 7 3 8 0.27 0.61 7 3 8 2.14 0.86 7 3 8 0.54 0.74 7 3 8 1.08 0.76 -7 -3 -9 1.83 0.68 7 3 9 3.95 0.87 7 3 9 2.56 0.81 7 3 9 2.58 0.78 7 3 10 40.58 2.27 7 3 10 36.44 2.20 7 3 10 36.68 2.27 7 3 11 10.78 1.09 7 3 11 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2.10 7 4 4 31.85 2.16 -7 -4 -5 1.37 1.06 -7 -4 -5 0.58 0.61 7 4 5 1.44 0.79 7 4 5 1.45 0.80 7 4 5 0.99 0.65 7 4 5 0.62 0.70 7 4 5 1.37 0.83 -7 -4 -6 2.65 1.42 7 4 6 2.38 0.85 -7 -4 -6 2.75 0.71 7 4 6 2.40 0.68 7 4 6 2.86 0.84 7 4 6 1.64 0.83 7 4 7 19.89 1.60 7 4 7 16.16 1.43 -7 -4 -7 17.70 1.44 7 4 7 15.07 1.33 7 4 7 18.72 1.55 7 4 8 46.46 2.64 -7 -4 -8 46.69 2.61 7 4 8 47.76 2.72 -7 -4 -9 1.80 0.72 7 4 9 0.70 0.76 7 4 9 1.41 0.74 7 4 9 1.66 0.74 7 4 10 70.28 3.32 -7 -4 -10 69.71 3.30 7 4 10 64.05 3.32 7 4 10 61.22 3.11 7 4 11 -0.27 0.68 7 4 11 0.28 0.66 7 4 12 0.18 0.57 7 4 12 -0.14 0.54 7 4 13 5.30 0.67 7 4 13 4.87 0.66 7 4 14 9.94 0.70 7 4 14 7.14 0.65 7 5 -9 2.53 0.46 7 5 -8 22.52 1.39 7 5 -7 78.45 3.64 7 5 -6 14.41 1.28 -7 -5 5 16.45 1.39 7 5 -5 16.17 1.42 -7 -5 4 25.97 1.82 7 5 -4 27.93 1.91 -7 -5 3 3.16 1.56 -7 -5 3 3.66 0.91 7 5 -3 5.39 0.98 7 5 -3 3.60 0.75 7 5 -2 7.99 1.15 7 5 -2 7.88 1.09 7 5 -2 9.18 1.04 -7 -5 1 31.08 3.22 7 5 -1 32.15 2.18 7 5 -1 33.10 2.19 7 5 -1 35.34 2.09 -7 -5 0 4.65 1.47 7 5 0 8.43 1.15 7 5 0 8.86 1.16 7 5 0 6.80 1.02 7 5 1 0.45 0.80 7 5 1 0.62 0.78 7 5 1 0.40 0.79 7 5 2 9.10 1.19 7 5 2 9.59 0.96 7 5 2 10.40 1.24 7 5 3 -0.97 0.86 7 5 3 0.15 0.72 7 5 3 0.50 0.65 7 5 3 -0.06 0.71 7 5 3 1.57 0.82 7 5 3 0.66 0.78 -7 -5 -4 47.77 3.89 7 5 4 47.67 2.61 7 5 4 46.31 2.67 7 5 4 49.89 2.77 7 5 4 48.26 2.59 7 5 4 49.07 2.85 7 5 4 50.69 2.82 -7 -5 -5 9.68 1.83 7 5 5 9.81 1.04 7 5 5 10.98 1.27 7 5 5 10.82 1.32 -7 -5 -6 2.45 1.43 -7 -5 -6 5.09 0.82 7 5 6 4.12 0.96 7 5 7 34.32 2.10 -7 -5 -7 31.71 1.96 7 5 7 29.38 1.92 7 5 7 35.48 2.15 7 5 7 33.97 2.20 7 5 8 25.42 1.78 -7 -5 -8 25.92 1.67 7 5 8 25.27 1.78 7 5 8 24.76 1.82 7 5 9 11.02 1.20 -7 -5 -9 12.64 1.11 7 5 9 11.74 1.19 7 5 10 17.35 1.43 7 5 10 18.84 1.44 7 5 10 17.81 1.37 7 5 11 31.76 1.82 7 5 11 28.73 1.75 7 5 12 -0.25 0.55 7 5 12 -0.37 0.52 7 5 13 32.41 1.69 -7 -5 -14 0.92 0.38 7 5 14 -0.29 0.34 7 6 -8 1.11 0.45 7 6 -7 5.27 0.74 7 6 -6 0.90 0.61 7 6 -5 11.89 1.18 -7 -6 4 29.52 1.90 7 6 -4 27.64 1.93 7 6 -4 30.40 1.77 7 6 -3 21.73 1.69 7 6 -3 21.15 1.51 -7 -6 2 2.30 1.66 7 6 -2 0.45 0.77 -7 -6 1 12.51 2.25 7 6 -1 13.37 1.34 -7 -6 0 2.08 1.66 7 6 0 2.00 0.90 7 6 0 1.28 0.79 7 6 1 91.37 4.32 7 6 1 87.84 4.30 7 6 1 86.88 4.29 7 6 1 86.81 4.23 -7 -6 -2 4.42 1.32 7 6 2 2.60 0.89 7 6 2 3.43 0.92 7 6 2 3.23 0.91 7 6 2 2.71 0.88 7 6 3 15.11 1.28 7 6 3 16.45 1.47 7 6 3 16.45 1.52 7 6 3 18.35 1.56 -7 -6 -4 0.72 1.31 7 6 4 1.50 0.78 7 6 4 1.12 0.74 7 6 4 0.69 0.65 7 6 4 0.32 0.83 7 6 4 1.05 0.79 -7 -6 -5 41.79 3.47 7 6 5 41.84 2.40 7 6 5 44.34 2.61 7 6 5 42.05 2.56 -7 -6 -6 12.90 2.04 7 6 6 10.82 1.22 7 6 6 10.54 1.12 7 6 6 11.88 1.16 7 6 6 13.38 1.36 -7 -6 -7 2.89 0.83 7 6 7 4.46 0.87 7 6 7 6.04 0.90 7 6 7 5.22 0.99 7 6 8 23.74 1.68 7 6 8 23.89 1.61 7 6 8 23.48 1.72 -7 -6 -9 4.02 0.85 7 6 9 5.32 0.90 7 6 9 3.79 0.78 7 6 9 3.57 0.85 7 6 10 41.71 2.20 7 6 10 34.22 2.05 7 6 11 3.33 0.71 7 6 11 3.58 0.65 7 6 11 2.88 0.65 7 6 12 7.16 0.81 7 6 12 5.15 0.62 7 6 13 13.99 0.94 7 7 -7 52.79 2.45 7 7 -6 0.22 0.50 7 7 -5 14.53 1.20 7 7 -5 15.02 1.08 7 7 -4 0.91 0.67 7 7 -3 -0.07 0.67 7 7 -2 15.93 1.41 7 7 -2 13.87 1.29 -7 -7 1 118.46 6.93 7 7 -1 128.85 5.75 7 7 -1 128.71 5.67 7 7 0 10.92 1.27 7 7 0 9.48 1.17 7 7 1 93.53 4.51 7 7 1 89.20 4.41 7 7 1 100.41 4.52 7 7 2 40.71 2.43 7 7 2 39.79 2.40 7 7 2 39.86 2.42 7 7 3 2.37 0.84 7 7 3 1.87 0.72 7 7 3 2.79 0.81 7 7 3 1.55 0.82 -7 -7 -4 18.76 2.44 7 7 4 18.31 1.43 7 7 4 19.48 1.60 7 7 4 17.42 1.58 -7 -7 -5 0.94 1.26 7 7 5 0.38 0.76 7 7 5 0.37 0.77 7 7 6 66.56 3.41 7 7 6 74.93 3.64 7 7 7 8.77 1.10 7 7 7 9.95 1.20 7 7 8 107.58 4.98 7 7 8 117.25 5.13 7 7 9 3.78 0.82 7 7 9 2.29 0.75 7 7 10 1.60 0.68 7 7 10 2.03 0.67 7 7 11 5.95 0.80 7 7 12 23.28 1.30 7 7 12 19.83 1.15 7 7 13 16.98 0.99 7 8 -6 2.03 0.50 7 8 -5 0.78 0.53 7 8 -4 33.83 1.87 7 8 -4 29.58 1.75 7 8 -3 -0.11 0.64 7 8 -3 0.86 0.61 7 8 -2 7.57 1.03 7 8 -2 9.77 1.05 -7 -8 1 31.05 3.03 7 8 -1 33.51 2.10 7 8 -1 35.13 2.07 -7 -8 0 1.84 1.53 7 8 0 3.07 0.90 7 8 0 3.18 0.84 7 8 1 35.07 2.18 7 8 1 34.38 2.14 7 8 2 13.02 1.29 7 8 2 12.35 1.25 7 8 2 12.86 1.30 7 8 3 10.13 1.03 7 8 3 10.70 1.15 7 8 3 10.96 1.18 7 8 4 5.30 0.94 7 8 4 4.21 0.91 7 8 5 10.69 1.17 7 8 5 11.05 1.20 7 8 6 12.42 1.17 7 8 6 12.16 1.25 -7 -8 -7 2.68 1.46 7 8 7 2.22 0.73 7 8 7 3.41 0.82 7 8 8 4.70 0.85 7 8 8 5.28 0.90 7 8 9 40.10 2.12 7 8 9 37.27 2.16 7 8 10 1.40 0.61 7 8 10 0.88 0.57 7 8 11 21.31 1.30 7 8 12 3.35 0.49 7 9 -5 16.93 1.01 7 9 -4 0.40 0.51 7 9 -4 0.18 0.46 7 9 -3 3.09 0.64 7 9 -3 2.98 0.64 7 9 -2 0.05 0.61 7 9 -2 0.93 0.62 7 9 -1 134.07 5.69 7 9 -1 128.10 5.64 7 9 0 22.79 1.61 7 9 0 22.73 1.58 7 9 1 76.57 3.67 -7 -9 -2 2.64 1.56 7 9 2 3.78 0.81 7 9 3 4.56 0.74 7 9 3 5.15 0.90 -7 -9 -4 2.54 1.54 7 9 4 2.01 0.77 7 9 4 4.30 0.86 7 9 5 39.05 2.30 7 9 5 44.23 2.38 7 9 6 19.11 1.42 7 9 6 22.16 1.54 7 9 7 28.24 1.76 7 9 7 31.47 1.86 7 9 8 10.74 0.99 7 9 8 10.82 1.04 7 9 9 0.19 0.52 7 9 9 0.22 0.51 7 9 10 2.70 0.55 7 9 10 2.31 0.55 7 9 11 -0.14 0.37 7 9 11 0.39 0.37 7 10 -4 24.84 1.27 7 10 -3 63.14 2.81 7 10 -2 16.13 1.10 7 10 -1 2.15 0.61 7 10 0 8.73 0.91 7 10 1 14.44 1.18 7 10 2 127.11 5.46 7 10 3 10.35 0.95 7 10 3 12.50 1.11 7 10 4 29.17 1.74 7 10 5 3.13 0.70 7 10 6 20.15 1.34 7 10 6 21.76 1.39 7 10 7 0.43 0.53 7 10 7 0.33 0.55 7 10 8 45.89 2.24 7 10 8 48.81 2.32 7 10 9 1.26 0.45 7 10 9 0.52 0.46 7 10 10 21.10 1.08 7 10 10 17.62 1.06 7 11 -2 28.36 1.39 7 11 -1 18.62 1.09 7 11 0 40.60 1.96 7 11 1 24.02 1.36 7 11 2 0.31 0.48 7 11 3 9.26 0.83 7 11 6 1.83 0.46 7 11 7 3.12 0.46 7 11 7 2.94 0.47 7 11 8 5.92 0.52 7 11 8 4.38 0.50 8 -4 2 9.44 0.69 8 -4 2 9.43 0.70 8 -4 3 0.74 0.37 8 -4 3 0.78 0.38 8 -4 4 13.55 0.83 8 -4 4 13.49 0.84 8 -4 5 5.72 0.51 8 -4 5 5.38 0.52 -8 3 1 9.26 0.78 8 -3 -1 8.92 0.66 8 -3 0 1.05 0.50 8 -3 1 17.03 1.11 8 -3 1 18.47 1.15 8 -3 2 3.84 0.63 8 -3 2 4.43 0.66 8 -3 3 42.82 2.10 8 -3 3 43.00 2.10 -8 3 -4 1.15 0.56 8 -3 4 1.58 0.49 8 -3 4 1.58 0.52 8 -3 5 0.72 0.42 8 -3 5 0.92 0.45 8 -3 6 16.52 1.02 8 -3 6 17.47 1.02 8 -3 7 8.30 0.63 -8 2 2 15.15 0.94 8 -2 -2 12.87 0.88 8 -2 -1 35.71 1.84 8 -2 -1 38.00 1.93 8 -2 0 0.12 0.55 8 -2 1 39.96 2.06 8 -2 1 38.37 2.07 8 -2 2 22.48 1.41 8 -2 2 19.99 1.37 -8 2 -3 1.21 0.60 8 -2 3 1.05 0.56 8 -2 3 0.89 0.57 8 -2 4 4.19 0.65 8 -2 4 5.38 0.74 8 -2 5 2.50 0.57 8 -2 5 1.77 0.55 8 -2 6 49.03 2.43 8 -2 6 54.45 2.45 8 -2 7 4.56 0.58 8 -2 7 3.78 0.57 8 -1 -6 8.34 0.65 8 -1 -5 0.67 0.42 8 -1 -4 8.03 0.78 8 -1 -3 1.60 0.42 8 -1 -2 2.22 0.53 8 -1 -2 2.61 0.63 8 -1 -1 15.33 1.20 8 -1 0 0.38 0.56 8 -1 0 0.54 0.59 8 -1 1 11.53 1.02 8 -1 1 9.12 1.00 -8 1 -2 3.03 1.18 -8 1 -2 1.41 0.60 8 -1 2 3.67 0.72 8 -1 2 2.45 0.71 -8 1 -3 1.66 0.66 8 -1 3 1.50 0.65 8 -1 3 1.39 0.64 8 -1 4 6.48 0.85 8 -1 4 5.89 0.83 8 -1 5 5.64 0.77 8 -1 5 5.33 0.80 -8 1 -6 7.02 0.89 8 -1 6 6.24 0.77 8 -1 6 6.86 0.82 -8 1 -7 4.96 0.76 8 -1 7 3.66 0.61 8 0 -6 14.09 0.95 8 0 -5 3.91 0.61 8 0 -4 0.82 0.53 8 0 -3 2.78 0.55 8 0 -3 1.96 0.60 8 0 -2 0.76 0.52 8 0 -2 1.11 0.63 8 0 -1 36.92 2.10 8 0 -1 43.90 2.24 -8 0 0 55.60 3.92 8 0 0 51.60 2.70 8 0 0 54.93 2.76 8 0 1 36.72 2.11 8 0 1 36.04 2.11 -8 0 -2 2.37 0.69 8 0 2 2.24 0.71 8 0 2 3.15 0.77 -8 0 -3 0.25 0.63 8 0 3 -0.41 0.58 8 0 3 0.39 0.64 -8 0 -4 1.57 0.77 8 0 4 1.44 0.67 8 0 4 1.35 0.65 8 0 5 10.29 1.02 8 0 5 8.82 0.96 8 0 6 13.90 1.15 8 0 8 6.61 0.77 8 0 9 -0.34 0.48 8 1 -6 5.09 0.63 8 1 -5 3.80 0.68 8 1 -4 8.84 0.94 8 1 -3 38.93 2.05 8 1 -3 42.75 2.23 -8 -1 2 -0.51 0.99 8 1 -2 0.62 0.64 8 1 -2 0.63 0.66 8 1 -1 -0.32 0.59 8 1 -1 0.17 0.64 -8 -1 0 2.94 1.18 -8 -1 0 0.18 0.77 8 1 0 1.05 0.64 8 1 0 1.68 0.65 8 1 0 1.89 0.73 -8 -1 -1 1.05 1.09 -8 -1 -1 1.33 0.81 8 1 1 1.48 0.68 8 1 1 1.03 0.67 -8 -1 -2 27.75 1.78 -8 -1 -2 31.49 2.94 -8 -1 -2 27.66 1.88 8 1 2 34.50 2.02 -8 -1 -3 4.12 0.98 8 1 3 3.79 0.81 8 1 3 4.07 0.83 -8 -1 -4 16.43 1.40 8 1 4 15.84 1.32 8 1 4 16.34 1.31 8 1 5 -0.06 0.61 -8 -1 -5 0.61 0.64 8 1 5 0.52 0.62 8 1 6 7.39 0.94 8 1 6 6.69 0.87 8 1 6 7.57 0.94 8 1 7 4.37 0.78 8 1 8 29.28 1.74 8 1 9 0.56 0.50 8 1 10 26.87 1.50 8 1 11 2.17 0.43 8 2 -6 34.63 1.80 8 2 -5 0.57 0.50 8 2 -5 1.76 0.57 8 2 -4 3.00 0.69 8 2 -3 4.60 0.73 8 2 -3 4.49 0.81 8 2 -2 45.30 2.37 8 2 -2 43.24 2.35 8 2 -1 20.37 1.48 8 2 -1 21.57 1.54 -8 -2 0 49.63 3.55 8 2 0 47.15 2.61 8 2 0 49.56 2.64 -8 -2 -1 24.22 2.44 -8 -2 -1 18.61 1.57 8 2 1 26.07 1.72 8 2 1 23.86 1.68 -8 -2 -2 5.33 1.41 8 2 2 7.27 0.99 8 2 2 5.40 0.94 8 2 3 11.04 1.14 8 2 3 12.51 1.19 -8 -2 -4 2.50 0.83 8 2 4 1.40 0.75 8 2 4 0.96 0.73 -8 -2 -5 41.95 2.38 8 2 5 41.72 2.40 8 2 5 48.76 2.53 8 2 6 6.11 0.94 8 2 6 7.68 0.91 8 2 6 6.49 0.84 8 2 6 6.12 0.91 8 2 7 7.93 1.01 8 2 7 7.23 0.89 8 2 8 0.86 0.61 8 2 9 0.95 0.57 8 2 10 19.93 1.28 8 2 10 20.63 1.31 8 2 11 2.99 0.52 8 2 11 2.63 0.49 8 2 12 0.14 0.25 8 3 -7 6.19 0.55 8 3 -6 1.77 0.49 8 3 -4 0.25 0.60 8 3 -3 93.95 4.27 8 3 -2 24.62 1.62 8 3 -2 27.50 1.76 8 3 -1 30.52 1.83 8 3 -1 31.23 1.95 8 3 -1 33.95 2.00 8 3 -1 33.16 1.99 8 3 0 1.00 0.70 8 3 0 2.02 0.79 8 3 1 128.62 5.64 8 3 1 124.90 5.59 -8 -3 -2 1.79 1.17 8 3 2 0.80 0.75 8 3 2 0.73 0.82 8 3 3 127.57 5.54 8 3 3 119.26 5.42 8 3 4 39.89 2.31 -8 -3 -5 2.23 1.20 8 3 5 1.26 0.68 8 3 5 1.13 0.61 8 3 5 1.70 0.70 -8 -3 -6 6.06 1.48 8 3 6 4.35 0.82 8 3 7 7.84 0.96 8 3 7 12.01 1.11 8 3 8 63.06 3.10 8 3 9 89.66 4.10 8 3 9 98.00 4.21 8 3 10 15.38 1.15 8 3 10 17.26 1.19 8 3 11 -0.15 0.45 8 3 11 -0.36 0.39 8 3 12 0.84 0.36 8 3 12 0.78 0.31 8 4 -7 14.48 0.87 8 4 -6 6.96 0.68 8 4 -5 9.08 0.87 8 4 -4 7.64 0.85 8 4 -3 19.73 1.41 8 4 -2 41.49 2.27 8 4 -1 10.63 1.14 8 4 0 79.00 3.79 8 4 0 87.17 3.97 8 4 1 0.95 0.62 8 4 1 0.26 0.66 8 4 1 -0.24 0.73 8 4 2 9.93 1.12 8 4 2 11.22 1.15 8 4 3 6.00 0.98 8 4 4 18.70 1.46 8 4 4 17.11 1.34 8 4 5 1.11 0.70 8 4 5 0.31 0.63 8 4 6 41.06 2.22 8 4 6 45.47 2.41 8 4 7 5.48 0.79 8 4 7 5.74 0.87 8 4 8 4.08 0.76 8 4 9 8.59 0.92 8 4 9 9.91 0.97 8 4 10 18.76 1.26 8 4 10 19.66 1.27 8 4 11 7.71 0.74 8 4 11 7.73 0.72 8 4 12 4.23 0.49 8 4 12 3.42 0.44 8 5 -7 0.67 0.27 8 5 -6 1.11 0.41 8 5 -5 6.65 0.74 8 5 -4 38.41 2.05 8 5 -3 8.75 0.96 8 5 -2 21.04 1.46 8 5 -1 4.88 0.85 8 5 -1 6.41 0.93 8 5 0 6.85 0.97 8 5 1 26.72 1.77 8 5 1 28.50 1.85 8 5 2 54.73 2.78 8 5 2 57.51 2.95 8 5 3 20.59 1.55 8 5 4 1.44 0.74 8 5 5 11.45 1.12 8 5 6 22.29 1.45 8 5 6 21.94 1.53 8 5 6 22.13 1.61 8 5 7 1.70 0.64 8 5 8 2.12 0.63 8 5 9 56.39 2.75 8 5 9 60.24 2.77 8 5 10 1.54 0.60 8 5 10 1.20 0.54 8 5 11 16.45 1.07 8 5 12 2.38 0.41 8 6 -6 0.35 0.34 8 6 -5 23.85 1.36 8 6 -4 1.04 0.52 8 6 -3 5.37 0.79 8 6 -2 7.92 0.94 8 6 -1 174.59 7.30 8 6 0 27.46 1.77 8 6 0 28.40 1.68 8 6 1 122.21 5.28 8 6 2 23.39 1.64 8 6 3 4.63 0.87 8 6 4 5.62 0.89 8 6 5 37.42 2.21 8 6 6 28.98 1.76 8 6 6 32.74 1.96 8 6 7 43.78 2.37 8 6 8 65.35 3.10 8 6 9 3.96 0.68 8 6 10 0.41 0.51 8 6 11 0.45 0.40 8 7 -5 1.33 0.41 8 7 -4 38.78 1.92 8 7 -3 0.36 0.51 8 7 -2 20.06 1.35 8 7 -1 47.89 2.47 8 7 -1 49.02 2.36 8 7 0 9.07 0.99 8 7 1 25.45 1.62 8 7 2 31.49 1.85 8 7 3 1.35 0.69 8 7 4 26.58 1.72 8 7 5 15.77 1.31 8 7 6 7.42 0.80 8 7 6 6.74 0.90 8 7 7 3.84 0.74 8 7 8 3.09 0.64 8 7 8 3.86 0.67 8 7 9 20.47 1.26 8 7 9 21.40 1.30 8 7 10 9.11 0.76 8 7 11 21.55 1.15 8 8 -3 2.83 0.52 8 8 -2 9.08 0.83 8 8 -1 51.39 2.49 8 8 0 113.22 4.82 8 8 1 52.01 2.54 8 8 2 0.50 0.59 8 8 3 4.26 0.76 8 8 5 33.71 1.90 8 8 6 -0.14 0.61 8 8 7 60.99 2.86 8 8 8 2.22 0.53 8 8 8 2.94 0.58 8 8 9 3.25 0.53 8 8 9 4.88 0.59 8 8 10 0.38 0.33 8 9 -1 4.82 0.59 8 9 0 0.92 0.50 8 9 1 -0.39 0.53 8 9 2 17.36 1.16 8 9 6 2.26 0.52 8 9 7 5.01 0.62 8 9 8 18.07 1.06 8 10 0 36.30 1.67 9 -1 1 2.32 0.40 9 -1 2 0.04 0.28 9 -1 2 0.16 0.30 9 -1 3 4.96 0.47 9 -1 3 5.11 0.48 9 -1 4 0.61 0.28 9 -1 4 0.45 0.29 9 0 1 0.33 0.36 9 0 1 0.05 0.41 9 0 2 5.36 0.59 9 0 2 6.77 0.63 9 0 3 6.51 0.63 9 0 3 6.79 0.64 9 0 4 8.64 0.69 9 0 4 8.76 0.67 9 0 5 0.38 0.36 9 1 0 55.10 2.47 9 1 1 1.76 0.50 9 1 1 1.45 0.50 9 1 2 10.95 0.85 9 1 2 10.04 0.85 9 1 3 0.20 0.43 9 1 3 1.13 0.47 9 1 4 11.74 0.87 9 1 4 11.78 0.84 9 1 5 2.22 0.51 9 2 0 2.33 0.55 9 2 1 45.23 2.19 9 2 2 22.86 1.37 9 2 3 60.61 2.76 9 2 3 58.65 2.72 9 2 4 2.30 0.54 9 2 5 0.16 0.43 9 3 0 19.70 1.21 9 3 1 9.51 0.85 9 3 2 4.99 0.67 9 3 3 0.43 0.52 9 3 4 29.07 1.60 9 3 5 4.78 0.65 9 4 1 3.40 0.64 9 4 2 82.86 3.65 9 4 3 9.26 0.85 9 4 4 5.28 0.67 9 4 5 0.26 0.46 TITL ca121021_1_1 in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 7.558354 11.064981 14.349059 83.4022 81.0067 75.0739 ZERR 4.00 0.000196 0.000279 0.000366 0.0021 0.0021 0.0022 LATT 1 SFAC C H N O S UNIT 44.00 60.00 4.00 12.00 4.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.1; aver:100.0 TEMP -173 SIZE 0.10 0.14 0.17 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 63950 _olex2_date_sample_submission 2021-10-12 _olex2_submission_original_sample_id ca121021_1_1 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.171 _oxdiff_exptl_absorpt_empirical_full_min 0.877