# Electronic Supplementary Material (ESI) for Chemical Science. # This journal is © The Royal Society of Chemistry 2022 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_rom167_0m_a _database_code_depnum_ccdc_archive 'CCDC 2122218' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-15 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_date 2021-10-28 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _shelx_SHELXL_version_number 2017/1 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C35 H47 N2 O2 P' _chemical_formula_sum 'C35 H47 N2 O2 P' _chemical_formula_weight 558.71 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 10.1764(4) _cell_length_b 16.6491(7) _cell_length_c 18.7925(8) _cell_angle_alpha 90 _cell_angle_beta 94.7280(10) _cell_angle_gamma 90 _cell_volume 3173.1(2) _cell_formula_units_Z 4 _cell_measurement_reflns_used 10579 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 63.388 _cell_measurement_theta_min 4.016 _shelx_estimated_absorpt_T_max 0.989 _shelx_estimated_absorpt_T_min 0.943 _exptl_absorpt_coefficient_mu 0.119 _exptl_absorpt_correction_T_max 0.989 _exptl_absorpt_correction_T_min 0.943 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Sadabs, Bruker-AXS' _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.170 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1208 _exptl_crystal_size_max 0.5 _exptl_crystal_size_mid 0.166 _exptl_crystal_size_min 0.094 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0757 _diffrn_reflns_av_unetI/netI 0.0565 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 69450 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.694 _diffrn_reflns_theta_min 2.008 _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 1.75 _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device_type 'ApexDuo, Bruker-AXS' _diffrn_measurement_method '1 deg. \f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 7481 _reflns_number_total 10579 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'Saint, Bruker-AXS' _computing_data_collection 'Apex2, Bruker-AXS' _computing_data_reduction 'Saint, Bruker-AXS' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2017/1 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _refine_diff_density_max 0.534 _refine_diff_density_min -0.367 _refine_diff_density_rms 0.057 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.016 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 413 _refine_ls_number_reflns 10579 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0782 _refine_ls_R_factor_gt 0.0472 _refine_ls_restrained_S_all 1.016 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0506P)^2^+0.9803P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1079 _refine_ls_wR_factor_ref 0.1240 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Others Fixed Sof: C18(0.5) C20A(0.65) H20A(0.65) H20B(0.65) H20C(0.65) C21A(0.65) H21A(0.65) H21B(0.65) H21C(0.65) C19A(0.65) H19A(0.65) H19B(0.65) H19C(0.65) C20B(0.35) H20D(0.35) H20E(0.35) H20F(0.35) C19B(0.35) H19D(0.35) H19E(0.35) H19F(0.35) C21B(0.35) H21D(0.35) H21E(0.35) H21F(0.35) C19(0.5) 3.a Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C5(H5), C6(H6), C10(H10), C12(H12), C24(H24), C26(H26) 3.b Idealised Me refined as rotating group: C1(H1A,H1B,H1C), C29(H29A,H29B,H29C), C30(H30A,H30B,H30C), C31(H31A,H31B, H31C), C33(H33A,H33B,H33C), C34(H34A,H34B,H34C), C35(H35A,H35B,H35C), C17(H17A, H17B,H17C), C16(H16A,H16B,H16C), C15(H15A,H15B,H15C), C20A(H20A,H20B,H20C), C21A(H21A,H21B,H21C), C19A(H19A,H19B,H19C), C20B(H20D,H20E,H20F), C19B(H19D, H19E,H19F), C21B(H21D,H21E,H21F) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 0.44000(3) 0.62179(2) 0.69446(2) 0.01367(8) Uani 1 1 d . . . . . O1 O 0.38531(9) 0.66540(5) 0.61715(5) 0.01681(19) Uani 1 1 d . . . . . O2 O 0.28426(9) 0.62833(5) 0.71434(5) 0.01585(18) Uani 1 1 d . . . . . N1 N 0.55997(11) 0.57414(7) 0.64917(6) 0.0162(2) Uani 1 1 d . . . . . N2 N 0.46388(11) 0.54496(6) 0.75790(6) 0.0155(2) Uani 1 1 d . . . . . C1 C 0.51905(13) 0.70725(8) 0.73772(7) 0.0192(3) Uani 1 1 d . . . . . H1A H 0.583896 0.729464 0.707331 0.029 Uiso 1 1 calc R U . . . H1B H 0.563646 0.690713 0.783588 0.029 Uiso 1 1 calc R U . . . H1C H 0.452756 0.748206 0.745834 0.029 Uiso 1 1 calc R U . . . C2 C 0.62268(13) 0.50852(7) 0.68323(7) 0.0152(2) Uani 1 1 d . . . . . C3 C 0.72240(14) 0.46021(8) 0.66096(7) 0.0192(3) Uani 1 1 d . . . . . H3 H 0.754698 0.468044 0.615462 0.023 Uiso 1 1 calc R U . . . C4 C 0.77448(15) 0.39997(8) 0.70641(8) 0.0228(3) Uani 1 1 d . . . . . H4 H 0.843493 0.366898 0.691895 0.027 Uiso 1 1 calc R U . . . C5 C 0.72693(14) 0.38777(8) 0.77239(8) 0.0225(3) Uani 1 1 d . . . . . H5 H 0.765277 0.347460 0.803285 0.027 Uiso 1 1 calc R U . . . C6 C 0.62310(13) 0.43414(8) 0.79400(8) 0.0201(3) Uani 1 1 d . . . . . H6 H 0.589744 0.425237 0.839085 0.024 Uiso 1 1 calc R U . . . C7 C 0.56944(12) 0.49339(7) 0.74862(7) 0.0154(2) Uani 1 1 d . . . . . C8 C 0.47117(12) 0.66007(7) 0.56440(7) 0.0150(2) Uani 1 1 d . . . . . C9 C 0.57443(13) 0.60656(7) 0.58138(7) 0.0155(2) Uani 1 1 d . . . . . C10 C 0.67000(13) 0.59382(8) 0.53451(7) 0.0171(2) Uani 1 1 d . . . . . H10 H 0.741723 0.558576 0.546779 0.021 Uiso 1 1 calc R U . . . C11 C 0.65965(13) 0.63358(8) 0.46869(7) 0.0174(3) Uani 1 1 d . . . . . C12 C 0.55440(13) 0.68626(8) 0.45315(7) 0.0169(2) Uani 1 1 d . . . . . H12 H 0.548117 0.713015 0.408342 0.020 Uiso 1 1 calc R U . . . C13 C 0.45727(13) 0.70176(7) 0.50040(7) 0.0152(2) Uani 1 1 d . . . . . C14 C 0.34337(13) 0.76067(8) 0.48373(7) 0.0168(2) Uani 1 1 d . . . . . C18 C 0.7539(16) 0.6208(8) 0.4137(7) 0.0162(19) Uani 0.5 1 d . . P A 2 C22 C 0.24829(13) 0.57723(7) 0.76721(7) 0.0145(2) Uani 1 1 d . . . . . C23 C 0.35163(13) 0.52787(7) 0.79385(7) 0.0150(2) Uani 1 1 d . . . . . C24 C 0.33121(14) 0.47123(8) 0.84551(7) 0.0188(3) Uani 1 1 d . . . . . H24 H 0.401721 0.438153 0.864417 0.023 Uiso 1 1 calc R U . . . C25 C 0.20523(14) 0.46314(8) 0.86969(7) 0.0192(3) Uani 1 1 d . . . . . C26 C 0.10444(13) 0.51360(8) 0.84165(7) 0.0178(3) Uani 1 1 d . . . . . H26 H 0.019648 0.508176 0.858812 0.021 Uiso 1 1 calc R U . . . C27 C 0.12196(12) 0.57207(7) 0.78930(7) 0.0149(2) Uani 1 1 d . . . . . C28 C 0.00996(13) 0.62670(8) 0.75861(7) 0.0171(2) Uani 1 1 d . . . . . C29 C 0.04870(14) 0.71506(8) 0.77255(8) 0.0230(3) Uani 1 1 d . . . . . H29A H 0.064074 0.724141 0.824085 0.034 Uiso 1 1 calc R U . . . H29B H -0.022698 0.750107 0.752908 0.034 Uiso 1 1 calc R U . . . H29C H 0.129372 0.727160 0.749521 0.034 Uiso 1 1 calc R U . . . C30 C -0.01519(15) 0.61305(9) 0.67757(8) 0.0241(3) Uani 1 1 d . . . . . H30A H -0.089709 0.646231 0.658799 0.036 Uiso 1 1 calc R U . . . H30B H -0.035587 0.556296 0.668305 0.036 Uiso 1 1 calc R U . . . H30C H 0.063707 0.627955 0.654032 0.036 Uiso 1 1 calc R U . . . C31 C -0.11889(13) 0.61087(9) 0.79315(8) 0.0225(3) Uani 1 1 d . . . . . H31A H -0.145437 0.554795 0.785143 0.034 Uiso 1 1 calc R U . . . H31B H -0.188055 0.646441 0.771815 0.034 Uiso 1 1 calc R U . . . H31C H -0.105549 0.621242 0.844569 0.034 Uiso 1 1 calc R U . . . C32 C 0.18424(15) 0.39911(9) 0.92661(8) 0.0251(3) Uani 1 1 d . . . . . C33 C 0.23501(17) 0.31744(9) 0.90169(9) 0.0307(3) Uani 1 1 d . . . . . H33A H 0.190878 0.304054 0.854866 0.046 Uiso 1 1 calc R U . . . H33B H 0.216030 0.275805 0.936247 0.046 Uiso 1 1 calc R U . . . H33C H 0.330400 0.320543 0.898093 0.046 Uiso 1 1 calc R U . . . C34 C 0.26149(18) 0.42246(10) 0.99707(8) 0.0335(4) Uani 1 1 d . . . . . H34A H 0.354775 0.429504 0.989148 0.050 Uiso 1 1 calc R U . . . H34B H 0.252685 0.379940 1.032428 0.050 Uiso 1 1 calc R U . . . H34C H 0.226392 0.472851 1.014671 0.050 Uiso 1 1 calc R U . . . C35 C 0.03884(17) 0.38924(12) 0.93984(12) 0.0444(5) Uani 1 1 d . . . . . H35A H 0.005493 0.439686 0.958302 0.067 Uiso 1 1 calc R U . . . H35B H 0.029733 0.346306 0.974766 0.067 Uiso 1 1 calc R U . . . H35C H -0.011894 0.375400 0.894915 0.067 Uiso 1 1 calc R U . . . C17 C 0.21141(14) 0.71574(9) 0.48299(8) 0.0226(3) Uani 1 1 d . . . . . H17A H 0.208514 0.673322 0.446742 0.034 Uiso 1 1 calc R U . . . H17B H 0.138737 0.753472 0.471765 0.034 Uiso 1 1 calc R U . . . H17C H 0.202793 0.691755 0.530007 0.034 Uiso 1 1 calc R U . . . C16 C 0.34832(15) 0.82720(8) 0.54038(8) 0.0221(3) Uani 1 1 d . . . . . H16A H 0.345415 0.803085 0.587796 0.033 Uiso 1 1 calc R U . . . H16B H 0.272579 0.863091 0.530873 0.033 Uiso 1 1 calc R U . . . H16C H 0.430141 0.857926 0.538656 0.033 Uiso 1 1 calc R U . . . C15 C 0.35083(15) 0.80107(9) 0.41082(8) 0.0252(3) Uani 1 1 d . . . . . H15A H 0.433672 0.831035 0.410572 0.038 Uiso 1 1 calc R U . . . H15B H 0.276323 0.838017 0.401905 0.038 Uiso 1 1 calc R U . . . H15C H 0.347246 0.759955 0.373384 0.038 Uiso 1 1 calc R U . . . C20A C 0.8935(2) 0.6493(2) 0.44273(15) 0.0384(7) Uani 0.65 1 d . . P A 1 H20A H 0.960250 0.636642 0.409740 0.058 Uiso 0.65 1 calc R U P A 1 H20B H 0.920672 0.627186 0.489982 0.058 Uiso 0.65 1 calc R U P A 1 H20C H 0.884130 0.707747 0.446291 0.058 Uiso 0.65 1 calc R U P A 1 C21A C 0.7242(3) 0.65459(19) 0.34094(13) 0.0363(6) Uani 0.65 1 d . . P A 1 H21A H 0.722938 0.713272 0.344848 0.055 Uiso 0.65 1 calc R U P A 1 H21B H 0.635193 0.635113 0.326277 0.055 Uiso 0.65 1 calc R U P A 1 H21C H 0.784345 0.638684 0.305317 0.055 Uiso 0.65 1 calc R U P A 1 C19A C 0.7693(3) 0.52586(14) 0.40244(15) 0.0382(7) Uani 0.65 1 d . . P A 1 H19A H 0.826249 0.513384 0.364319 0.057 Uiso 0.65 1 calc R U P A 1 H19B H 0.678519 0.509944 0.387498 0.057 Uiso 0.65 1 calc R U P A 1 H19C H 0.800223 0.496436 0.445796 0.057 Uiso 0.65 1 calc R U P A 1 C20B C 0.8305(6) 0.7050(3) 0.4023(3) 0.0432(13) Uani 0.35 1 d . . P A 2 H20D H 0.768966 0.743914 0.378895 0.065 Uiso 0.35 1 calc R U P A 2 H20E H 0.903433 0.695663 0.372311 0.065 Uiso 0.35 1 calc R U P A 2 H20F H 0.865367 0.726078 0.448739 0.065 Uiso 0.35 1 calc R U P A 2 C19B C 0.8857(6) 0.5698(4) 0.4493(3) 0.0523(17) Uani 0.35 1 d . . P A 2 H19D H 0.915932 0.593307 0.495569 0.079 Uiso 0.35 1 calc R U P A 2 H19E H 0.956696 0.572897 0.417133 0.079 Uiso 0.35 1 calc R U P A 2 H19F H 0.861535 0.513501 0.455844 0.079 Uiso 0.35 1 calc R U P A 2 C21B C 0.7091(6) 0.5876(5) 0.3503(3) 0.0510(16) Uani 0.35 1 d . . P A 2 H21D H 0.677086 0.533132 0.358427 0.076 Uiso 0.35 1 calc R U P A 2 H21E H 0.780922 0.585428 0.318733 0.076 Uiso 0.35 1 calc R U P A 2 H21F H 0.636860 0.620337 0.328142 0.076 Uiso 0.35 1 calc R U P A 2 C19 C 0.7740(16) 0.6161(9) 0.4176(6) 0.017(2) Uani 0.5 1 d . . P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.01375(15) 0.01387(14) 0.01370(15) 0.00202(11) 0.00295(11) 0.00166(12) O1 0.0165(4) 0.0201(4) 0.0143(4) 0.0039(3) 0.0047(3) 0.0046(4) O2 0.0136(4) 0.0177(4) 0.0167(4) 0.0054(3) 0.0042(3) 0.0017(3) N1 0.0169(5) 0.0171(5) 0.0152(5) 0.0032(4) 0.0042(4) 0.0050(4) N2 0.0147(5) 0.0160(5) 0.0162(5) 0.0048(4) 0.0043(4) 0.0029(4) C1 0.0174(6) 0.0194(6) 0.0210(6) 0.0005(5) 0.0026(5) -0.0002(5) C2 0.0156(6) 0.0133(5) 0.0166(6) 0.0011(4) 0.0006(5) 0.0007(4) C3 0.0212(7) 0.0168(6) 0.0205(6) 0.0007(5) 0.0060(5) 0.0036(5) C4 0.0233(7) 0.0177(6) 0.0281(7) 0.0027(5) 0.0067(6) 0.0069(5) C5 0.0214(7) 0.0186(6) 0.0279(7) 0.0073(5) 0.0042(6) 0.0051(5) C6 0.0179(6) 0.0206(6) 0.0223(7) 0.0060(5) 0.0044(5) 0.0024(5) C7 0.0128(6) 0.0142(5) 0.0194(6) 0.0017(5) 0.0017(5) 0.0006(4) C8 0.0151(6) 0.0161(6) 0.0142(6) 0.0004(4) 0.0043(5) 0.0002(5) C9 0.0175(6) 0.0146(5) 0.0145(6) 0.0009(4) 0.0023(5) 0.0005(5) C10 0.0173(6) 0.0159(5) 0.0186(6) 0.0007(5) 0.0041(5) 0.0017(5) C11 0.0195(6) 0.0158(6) 0.0175(6) -0.0015(5) 0.0055(5) -0.0021(5) C12 0.0198(6) 0.0167(6) 0.0145(6) 0.0003(5) 0.0034(5) -0.0010(5) C13 0.0156(6) 0.0153(5) 0.0145(6) 0.0003(4) 0.0007(5) -0.0006(5) C14 0.0174(6) 0.0189(6) 0.0144(6) 0.0012(5) 0.0024(5) 0.0024(5) C18 0.007(3) 0.013(2) 0.028(3) 0.0013(18) -0.0010(16) 0.006(2) C22 0.0169(6) 0.0136(5) 0.0132(5) 0.0016(4) 0.0023(5) -0.0008(4) C23 0.0142(6) 0.0154(5) 0.0157(6) 0.0005(4) 0.0033(5) 0.0005(4) C24 0.0183(6) 0.0180(6) 0.0204(6) 0.0051(5) 0.0036(5) 0.0031(5) C25 0.0186(6) 0.0178(6) 0.0218(6) 0.0049(5) 0.0048(5) -0.0004(5) C26 0.0143(6) 0.0183(6) 0.0212(6) 0.0024(5) 0.0047(5) -0.0016(5) C27 0.0147(6) 0.0140(5) 0.0159(6) -0.0009(4) 0.0008(5) -0.0008(4) C28 0.0141(6) 0.0161(6) 0.0208(6) 0.0013(5) 0.0007(5) 0.0006(5) C29 0.0193(7) 0.0161(6) 0.0335(8) 0.0007(5) 0.0012(6) 0.0015(5) C30 0.0197(7) 0.0304(7) 0.0217(7) 0.0012(6) -0.0023(5) 0.0006(6) C31 0.0141(6) 0.0243(7) 0.0295(7) 0.0013(6) 0.0040(5) 0.0004(5) C32 0.0223(7) 0.0244(7) 0.0296(8) 0.0120(6) 0.0081(6) 0.0008(6) C33 0.0351(9) 0.0216(7) 0.0354(9) 0.0094(6) 0.0025(7) -0.0023(6) C34 0.0436(10) 0.0343(8) 0.0238(8) 0.0089(6) 0.0104(7) 0.0044(7) C35 0.0281(9) 0.0465(10) 0.0607(13) 0.0338(9) 0.0172(8) 0.0029(8) C17 0.0179(7) 0.0278(7) 0.0220(7) 0.0006(6) 0.0004(5) 0.0009(5) C16 0.0267(7) 0.0191(6) 0.0206(7) -0.0004(5) 0.0013(6) 0.0040(5) C15 0.0269(8) 0.0303(7) 0.0188(7) 0.0078(6) 0.0037(6) 0.0076(6) C20A 0.0208(12) 0.0644(19) 0.0315(13) -0.0155(13) 0.0113(10) -0.0137(12) C21A 0.0371(15) 0.0526(17) 0.0215(12) 0.0104(11) 0.0153(11) 0.0154(13) C19A 0.0571(18) 0.0222(11) 0.0399(15) -0.0060(10) 0.0310(14) 0.0019(11) C20B 0.039(3) 0.039(3) 0.056(3) -0.003(3) 0.029(3) -0.006(2) C19B 0.046(3) 0.070(4) 0.046(3) 0.022(3) 0.032(3) 0.031(3) C21B 0.037(3) 0.082(5) 0.036(3) -0.030(3) 0.013(2) -0.008(3) C19 0.015(5) 0.026(3) 0.010(2) 0.0058(17) 0.010(3) 0.009(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 O1 1.6776(9) . ? P1 O2 1.6616(10) . ? P1 N1 1.7365(11) . ? P1 N2 1.7518(11) . ? P1 C1 1.7956(14) . ? O1 C8 1.3772(15) . ? O2 C22 1.3802(15) . ? N1 C2 1.3940(16) . ? N1 C9 1.4024(16) . ? N2 C7 1.3974(16) . ? N2 C23 1.4034(16) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C2 C3 1.3862(18) . ? C2 C7 1.4060(18) . ? C3 H3 0.9500 . ? C3 C4 1.3934(19) . ? C4 H4 0.9500 . ? C4 C5 1.383(2) . ? C5 H5 0.9500 . ? C5 C6 1.3957(19) . ? C6 H6 0.9500 . ? C6 C7 1.3863(18) . ? C8 C9 1.3945(18) . ? C8 C13 1.3857(17) . ? C9 C10 1.3814(18) . ? C10 H10 0.9500 . ? C10 C11 1.3992(18) . ? C11 C12 1.3965(19) . ? C11 C18 1.482(13) . ? C11 C19 1.595(12) . ? C12 H12 0.9500 . ? C12 C13 1.4060(18) . ? C13 C14 1.5309(18) . ? C14 C17 1.5362(19) . ? C14 C16 1.5342(19) . ? C14 C15 1.5340(18) . ? C18 C20B 1.626(14) . ? C18 C19B 1.679(18) . ? C18 C21B 1.357(14) . ? C22 C23 1.3946(18) . ? C22 C27 1.3858(18) . ? C23 C24 1.3813(18) . ? C24 H24 0.9500 . ? C24 C25 1.4015(19) . ? C25 C26 1.3952(19) . ? C25 C32 1.5376(19) . ? C26 H26 0.9500 . ? C26 C27 1.4057(17) . ? C27 C28 1.5332(18) . ? C28 C29 1.5398(18) . ? C28 C30 1.5402(19) . ? C28 C31 1.5331(19) . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C32 C33 1.541(2) . ? C32 C34 1.533(2) . ? C32 C35 1.529(2) . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C20A H20A 0.9800 . ? C20A H20B 0.9800 . ? C20A H20C 0.9800 . ? C20A C19 1.383(16) . ? C21A H21A 0.9800 . ? C21A H21B 0.9800 . ? C21A H21C 0.9800 . ? C21A C19 1.620(14) . ? C19A H19A 0.9800 . ? C19A H19B 0.9800 . ? C19A H19C 0.9800 . ? C19A C19 1.528(14) . ? C20B H20D 0.9800 . ? C20B H20E 0.9800 . ? C20B H20F 0.9800 . ? C19B H19D 0.9800 . ? C19B H19E 0.9800 . ? C19B H19F 0.9800 . ? C21B H21D 0.9800 . ? C21B H21E 0.9800 . ? C21B H21F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 P1 N1 88.27(5) . . ? O1 P1 N2 157.35(5) . . ? O1 P1 C1 98.83(6) . . ? O2 P1 O1 84.94(5) . . ? O2 P1 N1 149.57(5) . . ? O2 P1 N2 88.64(5) . . ? O2 P1 C1 104.26(6) . . ? N1 P1 N2 86.34(5) . . ? N1 P1 C1 106.08(6) . . ? N2 P1 C1 103.81(6) . . ? C8 O1 P1 114.24(8) . . ? C22 O2 P1 115.84(8) . . ? C2 N1 P1 116.54(9) . . ? C2 N1 C9 129.82(11) . . ? C9 N1 P1 113.58(9) . . ? C7 N2 P1 115.39(8) . . ? C7 N2 C23 126.88(11) . . ? C23 N2 P1 113.76(8) . . ? P1 C1 H1A 109.5 . . ? P1 C1 H1B 109.5 . . ? P1 C1 H1C 109.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? N1 C2 C7 110.29(11) . . ? C3 C2 N1 129.42(12) . . ? C3 C2 C7 120.28(12) . . ? C2 C3 H3 120.5 . . ? C2 C3 C4 118.91(12) . . ? C4 C3 H3 120.5 . . ? C3 C4 H4 119.6 . . ? C5 C4 C3 120.79(13) . . ? C5 C4 H4 119.6 . . ? C4 C5 H5 119.7 . . ? C4 C5 C6 120.60(13) . . ? C6 C5 H5 119.7 . . ? C5 C6 H6 120.5 . . ? C7 C6 C5 118.93(13) . . ? C7 C6 H6 120.5 . . ? N2 C7 C2 110.77(11) . . ? C6 C7 N2 128.93(12) . . ? C6 C7 C2 120.30(12) . . ? O1 C8 C9 112.78(11) . . ? O1 C8 C13 124.54(11) . . ? C13 C8 C9 122.67(12) . . ? C8 C9 N1 108.68(11) . . ? C10 C9 N1 130.72(12) . . ? C10 C9 C8 120.60(12) . . ? C9 C10 H10 120.5 . . ? C9 C10 C11 119.04(12) . . ? C11 C10 H10 120.5 . . ? C10 C11 C18 122.9(6) . . ? C10 C11 C19 116.1(5) . . ? C12 C11 C10 118.85(12) . . ? C12 C11 C18 118.3(6) . . ? C12 C11 C19 125.0(5) . . ? C11 C12 H12 118.3 . . ? C11 C12 C13 123.38(12) . . ? C13 C12 H12 118.3 . . ? C8 C13 C12 115.44(12) . . ? C8 C13 C14 121.32(11) . . ? C12 C13 C14 123.24(11) . . ? C13 C14 C17 109.66(11) . . ? C13 C14 C16 109.85(11) . . ? C13 C14 C15 111.79(11) . . ? C16 C14 C17 109.67(11) . . ? C15 C14 C17 108.24(11) . . ? C15 C14 C16 107.58(11) . . ? C11 C18 C20B 108.3(8) . . ? C11 C18 C19B 109.7(8) . . ? C20B C18 C19B 96.5(9) . . ? C21B C18 C11 118.7(11) . . ? C21B C18 C20B 111.4(9) . . ? C21B C18 C19B 110.1(10) . . ? O2 C22 C23 112.64(11) . . ? O2 C22 C27 124.16(11) . . ? C27 C22 C23 123.13(11) . . ? C22 C23 N2 109.10(11) . . ? C24 C23 N2 130.72(12) . . ? C24 C23 C22 120.13(12) . . ? C23 C24 H24 120.4 . . ? C23 C24 C25 119.22(12) . . ? C25 C24 H24 120.4 . . ? C24 C25 C32 118.39(12) . . ? C26 C25 C24 118.90(12) . . ? C26 C25 C32 122.70(12) . . ? C25 C26 H26 118.3 . . ? C25 C26 C27 123.33(12) . . ? C27 C26 H26 118.3 . . ? C22 C27 C26 115.28(12) . . ? C22 C27 C28 121.98(11) . . ? C26 C27 C28 122.74(11) . . ? C27 C28 C29 109.32(11) . . ? C27 C28 C30 110.02(11) . . ? C29 C28 C30 109.18(11) . . ? C31 C28 C27 111.96(11) . . ? C31 C28 C29 107.95(11) . . ? C31 C28 C30 108.36(11) . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C28 C30 H30A 109.5 . . ? C28 C30 H30B 109.5 . . ? C28 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C28 C31 H31A 109.5 . . ? C28 C31 H31B 109.5 . . ? C28 C31 H31C 109.5 . . ? H31A C31 H31B 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C25 C32 C33 109.32(12) . . ? C34 C32 C25 109.53(12) . . ? C34 C32 C33 108.99(13) . . ? C35 C32 C25 112.29(12) . . ? C35 C32 C33 107.92(14) . . ? C35 C32 C34 108.73(14) . . ? C32 C33 H33A 109.5 . . ? C32 C33 H33B 109.5 . . ? C32 C33 H33C 109.5 . . ? H33A C33 H33B 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C32 C34 H34A 109.5 . . ? C32 C34 H34B 109.5 . . ? C32 C34 H34C 109.5 . . ? H34A C34 H34B 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C32 C35 H35A 109.5 . . ? C32 C35 H35B 109.5 . . ? C32 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C14 C17 H17A 109.5 . . ? C14 C17 H17B 109.5 . . ? C14 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C14 C16 H16A 109.5 . . ? C14 C16 H16B 109.5 . . ? C14 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C14 C15 H15A 109.5 . . ? C14 C15 H15B 109.5 . . ? C14 C15 H15C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? H20A C20A H20B 109.5 . . ? H20A C20A H20C 109.5 . . ? H20B C20A H20C 109.5 . . ? C19 C20A H20A 109.5 . . ? C19 C20A H20B 109.5 . . ? C19 C20A H20C 109.5 . . ? H21A C21A H21B 109.5 . . ? H21A C21A H21C 109.5 . . ? H21B C21A H21C 109.5 . . ? C19 C21A H21A 109.5 . . ? C19 C21A H21B 109.5 . . ? C19 C21A H21C 109.5 . . ? H19A C19A H19B 109.5 . . ? H19A C19A H19C 109.5 . . ? H19B C19A H19C 109.5 . . ? C19 C19A H19A 109.5 . . ? C19 C19A H19B 109.5 . . ? C19 C19A H19C 109.5 . . ? C18 C20B H20D 109.5 . . ? C18 C20B H20E 109.5 . . ? C18 C20B H20F 109.5 . . ? H20D C20B H20E 109.5 . . ? H20D C20B H20F 109.5 . . ? H20E C20B H20F 109.5 . . ? C18 C19B H19D 109.5 . . ? C18 C19B H19E 109.5 . . ? C18 C19B H19F 109.5 . . ? H19D C19B H19E 109.5 . . ? H19D C19B H19F 109.5 . . ? H19E C19B H19F 109.5 . . ? C18 C21B H21D 109.5 . . ? C18 C21B H21E 109.5 . . ? C18 C21B H21F 109.5 . . ? H21D C21B H21E 109.5 . . ? H21D C21B H21F 109.5 . . ? H21E C21B H21F 109.5 . . ? C11 C19 C21A 105.8(10) . . ? C20A C19 C11 112.7(8) . . ? C20A C19 C21A 110.3(8) . . ? C20A C19 C19A 118.0(11) . . ? C19A C19 C11 106.2(7) . . ? C19A C19 C21A 102.7(7) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag P1 O1 C8 C9 11.55(14) . . . . ? P1 O1 C8 C13 -169.49(10) . . . . ? P1 O2 C22 C23 -0.82(14) . . . . ? P1 O2 C22 C27 -177.71(10) . . . . ? P1 N1 C2 C3 -178.83(12) . . . . ? P1 N1 C2 C7 1.91(14) . . . . ? P1 N1 C9 C8 -10.09(14) . . . . ? P1 N1 C9 C10 169.11(12) . . . . ? P1 N2 C7 C2 -8.34(14) . . . . ? P1 N2 C7 C6 171.11(12) . . . . ? P1 N2 C23 C22 1.25(13) . . . . ? P1 N2 C23 C24 178.48(12) . . . . ? O1 P1 O2 C22 159.53(9) . . . . ? O1 P1 N1 C2 -163.40(10) . . . . ? O1 P1 N1 C9 13.97(9) . . . . ? O1 P1 N2 C7 84.36(16) . . . . ? O1 P1 N2 C23 -74.83(16) . . . . ? O1 C8 C9 N1 -0.64(15) . . . . ? O1 C8 C9 C10 -179.93(11) . . . . ? O1 C8 C13 C12 -178.60(12) . . . . ? O1 C8 C13 C14 1.7(2) . . . . ? O2 P1 O1 C8 -164.62(9) . . . . ? O2 P1 N1 C2 -86.44(13) . . . . ? O2 P1 N1 C9 90.93(13) . . . . ? O2 P1 N2 C7 157.74(10) . . . . ? O2 P1 N2 C23 -1.44(9) . . . . ? O2 C22 C23 N2 -0.30(15) . . . . ? O2 C22 C23 C24 -177.88(11) . . . . ? O2 C22 C27 C26 177.22(11) . . . . ? O2 C22 C27 C28 -2.92(19) . . . . ? N1 P1 O1 C8 -14.31(9) . . . . ? N1 P1 O2 C22 81.69(13) . . . . ? N1 P1 N2 C7 7.76(10) . . . . ? N1 P1 N2 C23 -151.42(10) . . . . ? N1 C2 C3 C4 176.72(13) . . . . ? N1 C2 C7 N2 3.96(15) . . . . ? N1 C2 C7 C6 -175.54(12) . . . . ? N1 C9 C10 C11 178.98(13) . . . . ? N2 P1 O1 C8 -90.53(15) . . . . ? N2 P1 O2 C22 1.27(9) . . . . ? N2 P1 N1 C2 -5.41(10) . . . . ? N2 P1 N1 C9 171.96(10) . . . . ? N2 C23 C24 C25 -175.85(13) . . . . ? C1 P1 O1 C8 91.70(9) . . . . ? C1 P1 O2 C22 -102.63(9) . . . . ? C1 P1 N1 C2 97.91(10) . . . . ? C1 P1 N1 C9 -84.71(10) . . . . ? C1 P1 N2 C7 -97.91(10) . . . . ? C1 P1 N2 C23 102.91(10) . . . . ? C2 N1 C9 C8 166.86(13) . . . . ? C2 N1 C9 C10 -13.9(2) . . . . ? C2 C3 C4 C5 0.7(2) . . . . ? C3 C2 C7 N2 -175.37(12) . . . . ? C3 C2 C7 C6 5.1(2) . . . . ? C3 C4 C5 C6 1.8(2) . . . . ? C4 C5 C6 C7 -0.8(2) . . . . ? C5 C6 C7 N2 177.98(13) . . . . ? C5 C6 C7 C2 -2.6(2) . . . . ? C7 N2 C23 C22 -155.09(12) . . . . ? C7 N2 C23 C24 22.1(2) . . . . ? C7 C2 C3 C4 -4.1(2) . . . . ? C8 C9 C10 C11 -1.91(19) . . . . ? C8 C13 C14 C17 -61.47(16) . . . . ? C8 C13 C14 C16 59.12(16) . . . . ? C8 C13 C14 C15 178.48(12) . . . . ? C9 N1 C2 C3 4.3(2) . . . . ? C9 N1 C2 C7 -174.95(13) . . . . ? C9 C8 C13 C12 0.26(19) . . . . ? C9 C8 C13 C14 -179.43(12) . . . . ? C9 C10 C11 C12 1.37(19) . . . . ? C9 C10 C11 C18 -177.1(6) . . . . ? C9 C10 C11 C19 179.8(6) . . . . ? C10 C11 C12 C13 0.0(2) . . . . ? C10 C11 C18 C20B -116.2(8) . . . . ? C10 C11 C18 C19B -12.1(10) . . . . ? C10 C11 C18 C21B 115.5(11) . . . . ? C10 C11 C19 C20A -70.1(10) . . . . ? C10 C11 C19 C21A 169.3(4) . . . . ? C10 C11 C19 C19A 60.6(9) . . . . ? C11 C12 C13 C8 -0.80(19) . . . . ? C11 C12 C13 C14 178.89(12) . . . . ? C12 C11 C18 C20B 65.3(10) . . . . ? C12 C11 C18 C19B 169.4(5) . . . . ? C12 C11 C18 C21B -63.0(12) . . . . ? C12 C11 C19 C20A 108.2(9) . . . . ? C12 C11 C19 C21A -12.4(10) . . . . ? C12 C11 C19 C19A -121.1(7) . . . . ? C12 C13 C14 C17 118.86(13) . . . . ? C12 C13 C14 C16 -120.55(13) . . . . ? C12 C13 C14 C15 -1.20(18) . . . . ? C13 C8 C9 N1 -179.62(12) . . . . ? C13 C8 C9 C10 1.1(2) . . . . ? C18 C11 C12 C13 178.6(6) . . . . ? C22 C23 C24 C25 1.1(2) . . . . ? C22 C27 C28 C29 -58.83(16) . . . . ? C22 C27 C28 C30 61.05(16) . . . . ? C22 C27 C28 C31 -178.39(12) . . . . ? C23 N2 C7 C2 147.66(13) . . . . ? C23 N2 C7 C6 -32.9(2) . . . . ? C23 C22 C27 C26 0.65(18) . . . . ? C23 C22 C27 C28 -179.49(12) . . . . ? C23 C24 C25 C26 -1.1(2) . . . . ? C23 C24 C25 C32 179.34(13) . . . . ? C24 C25 C26 C27 0.8(2) . . . . ? C24 C25 C32 C33 -52.13(18) . . . . ? C24 C25 C32 C34 67.23(17) . . . . ? C24 C25 C32 C35 -171.87(15) . . . . ? C25 C26 C27 C22 -0.59(19) . . . . ? C25 C26 C27 C28 179.55(13) . . . . ? C26 C25 C32 C33 128.30(15) . . . . ? C26 C25 C32 C34 -112.34(16) . . . . ? C26 C25 C32 C35 8.6(2) . . . . ? C26 C27 C28 C29 121.02(13) . . . . ? C26 C27 C28 C30 -119.10(14) . . . . ? C26 C27 C28 C31 1.45(17) . . . . ? C27 C22 C23 N2 176.62(12) . . . . ? C27 C22 C23 C24 -1.0(2) . . . . ? C32 C25 C26 C27 -179.61(13) . . . . ? C19 C11 C12 C13 -178.3(6) . . . . ? _shelx_res_file ; TITL rom167_0m_a.res in P2(1)/c rom167_0m_a.res created by SHELXL-2017/1 at 14:34:32 on 28-Oct-2021 REM Old TITL rom167_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.142, Rweak 0.005, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C35 N2 O2 P CELL 0.71073 10.1764 16.6491 18.7925 90 94.728 90 ZERR 4 0.0004 0.0007 0.0008 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O P UNIT 140 188 8 8 4 L.S. 10 PLAN 8 SIZE 0.094 0.166 0.5 TEMP -173(2) CONF BOND $H LIST 6 MORE -1 fmap 2 acta OMIT -1 1 4 OMIT -2 1 3 OMIT 0 1 1 OMIT -2 1 6 OMIT -3 1 5 OMIT -1 1 1 OMIT -3 1 8 OMIT -1 0 2 OMIT -2 0 4 OMIT -2 6 1 OMIT -3 0 4 OMIT -2 2 5 OMIT 0 6 3 OMIT -1 2 1 OMIT 2 0 0 OMIT 3 1 3 OMIT 1 1 0 OMIT -1 2 3 OMIT 1 2 1 OMIT -1 3 10 OMIT 2 1 1 OMIT -2 3 3 OMIT -2 1 5 OMIT -2 3 2 OMIT -3 0 2 OMIT 2 0 6 OMIT 2 5 1 OMIT 0 1 2 OMIT -4 1 4 OMIT -2 1 2 OMIT -3 2 7 OMIT 3 1 5 OMIT -2 4 6 OMIT -4 1 9 OMIT -3 1 1 OMIT 3 0 4 OMIT -6 1 10 OMIT -4 0 8 OMIT 0 6 0 OMIT -3 2 9 OMIT 0 0 12 OMIT 4 0 2 OMIT -1 3 4 OMIT 1 1 3 OMIT -3 1 4 OMIT -3 0 6 OMIT 2 5 5 OMIT 2 1 5 OMIT -3 3 9 OMIT 1 2 5 OMIT 3 3 12 OMIT 1 5 9 OMIT 0 6 6 OMIT -2 0 8 OMIT 6 6 0 OMIT -1 1 2 OMIT -1 3 6 OMIT -1 2 6 OMIT -5 2 10 OMIT -3 2 10 OMIT 0 5 5 OMIT 4 4 4 OMIT -2 7 2 OMIT 2 6 5 OMIT -3 7 2 REM REM REM WGHT 0.050600 0.980300 FVAR 0.37495 P1 5 0.440004 0.621794 0.694460 11.00000 0.01375 0.01387 = 0.01370 0.00202 0.00295 0.00166 O1 4 0.385313 0.665401 0.617149 11.00000 0.01652 0.02014 = 0.01433 0.00385 0.00473 0.00460 O2 4 0.284258 0.628334 0.714340 11.00000 0.01365 0.01767 = 0.01671 0.00541 0.00423 0.00174 N1 3 0.559971 0.574141 0.649174 11.00000 0.01694 0.01707 = 0.01521 0.00318 0.00423 0.00498 N2 3 0.463876 0.544961 0.757896 11.00000 0.01468 0.01603 = 0.01618 0.00482 0.00427 0.00291 C1 1 0.519052 0.707248 0.737715 11.00000 0.01739 0.01943 = 0.02104 0.00046 0.00262 -0.00018 AFIX 137 H1A 2 0.583896 0.729464 0.707331 11.00000 -1.50000 H1B 2 0.563646 0.690713 0.783588 11.00000 -1.50000 H1C 2 0.452756 0.748206 0.745834 11.00000 -1.50000 AFIX 0 C2 1 0.622685 0.508516 0.683228 11.00000 0.01564 0.01334 = 0.01658 0.00112 0.00060 0.00066 C3 1 0.722400 0.460210 0.660963 11.00000 0.02119 0.01678 = 0.02048 0.00073 0.00603 0.00361 AFIX 43 H3 2 0.754698 0.468044 0.615462 11.00000 -1.20000 AFIX 0 C4 1 0.774483 0.399975 0.706414 11.00000 0.02331 0.01771 = 0.02806 0.00273 0.00673 0.00689 AFIX 43 H4 2 0.843493 0.366898 0.691895 11.00000 -1.20000 AFIX 0 C5 1 0.726934 0.387770 0.772385 11.00000 0.02136 0.01857 = 0.02786 0.00725 0.00425 0.00508 AFIX 43 H5 2 0.765277 0.347460 0.803285 11.00000 -1.20000 AFIX 0 C6 1 0.623104 0.434136 0.793999 11.00000 0.01787 0.02056 = 0.02229 0.00599 0.00445 0.00239 AFIX 43 H6 2 0.589744 0.425237 0.839085 11.00000 -1.20000 AFIX 0 C7 1 0.569437 0.493385 0.748616 11.00000 0.01278 0.01423 = 0.01938 0.00167 0.00172 0.00058 C8 1 0.471172 0.660075 0.564401 11.00000 0.01513 0.01607 = 0.01424 0.00038 0.00428 0.00022 C9 1 0.574430 0.606559 0.581385 11.00000 0.01747 0.01463 = 0.01451 0.00088 0.00228 0.00045 C10 1 0.670001 0.593821 0.534506 11.00000 0.01729 0.01593 = 0.01859 0.00065 0.00415 0.00171 AFIX 43 H10 2 0.741723 0.558576 0.546779 11.00000 -1.20000 AFIX 0 C11 1 0.659646 0.633579 0.468685 11.00000 0.01947 0.01579 = 0.01750 -0.00151 0.00546 -0.00206 C12 1 0.554403 0.686264 0.453146 11.00000 0.01982 0.01673 = 0.01449 0.00026 0.00335 -0.00103 AFIX 43 H12 2 0.548117 0.713015 0.408342 11.00000 -1.20000 AFIX 0 C13 1 0.457267 0.701756 0.500399 11.00000 0.01555 0.01535 = 0.01448 0.00028 0.00072 -0.00058 C14 1 0.343368 0.760669 0.483734 11.00000 0.01741 0.01887 = 0.01436 0.00121 0.00235 0.00243 PART 2 C18 1 0.753932 0.620836 0.413698 10.50000 0.00685 0.01348 = 0.02772 0.00125 -0.00102 0.00551 PART 0 C22 1 0.248294 0.577228 0.767207 11.00000 0.01692 0.01361 = 0.01315 0.00165 0.00225 -0.00076 C23 1 0.351625 0.527872 0.793852 11.00000 0.01418 0.01537 = 0.01570 0.00051 0.00331 0.00055 C24 1 0.331205 0.471231 0.845506 11.00000 0.01830 0.01799 = 0.02036 0.00506 0.00364 0.00305 AFIX 43 H24 2 0.401721 0.438153 0.864417 11.00000 -1.20000 AFIX 0 C25 1 0.205231 0.463138 0.869687 11.00000 0.01865 0.01781 = 0.02175 0.00495 0.00481 -0.00035 C26 1 0.104435 0.513602 0.841652 11.00000 0.01429 0.01832 = 0.02124 0.00242 0.00474 -0.00163 AFIX 43 H26 2 0.019648 0.508176 0.858812 11.00000 -1.20000 AFIX 0 C27 1 0.121962 0.572067 0.789303 11.00000 0.01472 0.01399 = 0.01587 -0.00089 0.00084 -0.00084 C28 1 0.009960 0.626700 0.758608 11.00000 0.01410 0.01611 = 0.02084 0.00126 0.00066 0.00059 C29 1 0.048698 0.715058 0.772548 11.00000 0.01928 0.01609 = 0.03345 0.00073 0.00119 0.00150 AFIX 137 H29A 2 0.064074 0.724141 0.824085 11.00000 -1.50000 H29B 2 -0.022698 0.750107 0.752908 11.00000 -1.50000 H29C 2 0.129372 0.727160 0.749521 11.00000 -1.50000 AFIX 0 C30 1 -0.015195 0.613055 0.677567 11.00000 0.01973 0.03035 = 0.02166 0.00124 -0.00229 0.00059 AFIX 137 H30A 2 -0.089709 0.646231 0.658799 11.00000 -1.50000 H30B 2 -0.035587 0.556296 0.668305 11.00000 -1.50000 H30C 2 0.063707 0.627955 0.654032 11.00000 -1.50000 AFIX 0 C31 1 -0.118892 0.610866 0.793149 11.00000 0.01408 0.02427 = 0.02951 0.00127 0.00397 0.00043 AFIX 137 H31A 2 -0.145437 0.554795 0.785143 11.00000 -1.50000 H31B 2 -0.188055 0.646441 0.771815 11.00000 -1.50000 H31C 2 -0.105549 0.621242 0.844569 11.00000 -1.50000 AFIX 0 C32 1 0.184237 0.399106 0.926614 11.00000 0.02232 0.02435 = 0.02959 0.01205 0.00815 0.00080 C33 1 0.235007 0.317445 0.901686 11.00000 0.03513 0.02162 = 0.03536 0.00939 0.00248 -0.00229 AFIX 137 H33A 2 0.190878 0.304054 0.854866 11.00000 -1.50000 H33B 2 0.216030 0.275805 0.936247 11.00000 -1.50000 H33C 2 0.330400 0.320543 0.898093 11.00000 -1.50000 AFIX 0 C34 1 0.261491 0.422456 0.997071 11.00000 0.04358 0.03429 = 0.02382 0.00886 0.01037 0.00441 AFIX 137 H34A 2 0.354775 0.429504 0.989148 11.00000 -1.50000 H34B 2 0.252685 0.379940 1.032428 11.00000 -1.50000 H34C 2 0.226392 0.472851 1.014671 11.00000 -1.50000 AFIX 0 C35 1 0.038836 0.389238 0.939837 11.00000 0.02811 0.04650 = 0.06074 0.03383 0.01719 0.00294 AFIX 137 H35A 2 0.005493 0.439686 0.958302 11.00000 -1.50000 H35B 2 0.029733 0.346306 0.974766 11.00000 -1.50000 H35C 2 -0.011894 0.375400 0.894915 11.00000 -1.50000 AFIX 0 C17 1 0.211408 0.715737 0.482995 11.00000 0.01791 0.02782 = 0.02195 0.00060 0.00040 0.00091 AFIX 137 H17A 2 0.208514 0.673322 0.446742 11.00000 -1.50000 H17B 2 0.138737 0.753472 0.471765 11.00000 -1.50000 H17C 2 0.202793 0.691755 0.530007 11.00000 -1.50000 AFIX 0 C16 1 0.348324 0.827202 0.540381 11.00000 0.02665 0.01905 = 0.02060 -0.00039 0.00128 0.00400 AFIX 137 H16A 2 0.345415 0.803085 0.587796 11.00000 -1.50000 H16B 2 0.272579 0.863091 0.530873 11.00000 -1.50000 H16C 2 0.430141 0.857926 0.538656 11.00000 -1.50000 AFIX 0 C15 1 0.350826 0.801066 0.410815 11.00000 0.02695 0.03031 = 0.01875 0.00778 0.00371 0.00762 AFIX 137 H15A 2 0.433672 0.831035 0.410572 11.00000 -1.50000 H15B 2 0.276323 0.838017 0.401905 11.00000 -1.50000 H15C 2 0.347246 0.759955 0.373384 11.00000 -1.50000 AFIX 0 PART 1 C20A 1 0.893472 0.649332 0.442735 10.65000 0.02076 0.06444 = 0.03148 -0.01549 0.01129 -0.01372 AFIX 137 H20A 2 0.960250 0.636642 0.409740 10.65000 -1.50000 H20B 2 0.920672 0.627186 0.489982 10.65000 -1.50000 H20C 2 0.884130 0.707747 0.446291 10.65000 -1.50000 AFIX 0 C21A 1 0.724204 0.654585 0.340941 10.65000 0.03711 0.05258 = 0.02147 0.01038 0.01534 0.01537 AFIX 137 H21A 2 0.722938 0.713272 0.344848 10.65000 -1.50000 H21B 2 0.635193 0.635113 0.326277 10.65000 -1.50000 H21C 2 0.784345 0.638684 0.305317 10.65000 -1.50000 AFIX 0 C19A 1 0.769332 0.525865 0.402444 10.65000 0.05708 0.02216 = 0.03988 -0.00600 0.03102 0.00188 AFIX 137 H19A 2 0.826249 0.513384 0.364319 10.65000 -1.50000 H19B 2 0.678519 0.509944 0.387498 10.65000 -1.50000 H19C 2 0.800223 0.496436 0.445796 10.65000 -1.50000 AFIX 0 PART 2 C20B 1 0.830533 0.704980 0.402276 10.35000 0.03875 0.03888 = 0.05630 -0.00323 0.02928 -0.00618 AFIX 137 H20D 2 0.768966 0.743914 0.378895 10.35000 -1.50000 H20E 2 0.903433 0.695663 0.372311 10.35000 -1.50000 H20F 2 0.865367 0.726078 0.448739 10.35000 -1.50000 AFIX 0 C19B 1 0.885745 0.569825 0.449263 10.35000 0.04556 0.07024 = 0.04591 0.02247 0.03185 0.03086 AFIX 137 H19D 2 0.915932 0.593307 0.495569 10.35000 -1.50000 H19E 2 0.956696 0.572897 0.417133 10.35000 -1.50000 H19F 2 0.861535 0.513501 0.455844 10.35000 -1.50000 AFIX 0 C21B 1 0.709085 0.587626 0.350349 10.35000 0.03723 0.08174 = 0.03565 -0.03009 0.01285 -0.00820 AFIX 137 H21D 2 0.677086 0.533132 0.358427 10.35000 -1.50000 H21E 2 0.780922 0.585428 0.318733 10.35000 -1.50000 H21F 2 0.636860 0.620337 0.328142 10.35000 -1.50000 AFIX 0 PART 1 C19 1 0.774015 0.616054 0.417601 10.50000 0.01512 0.02595 = 0.01021 0.00582 0.00990 0.00863 HKLF 4 REM rom167_0m_a.res in P2(1)/c REM R1 = 0.0472 for 7481 Fo > 4sig(Fo) and 0.0782 for all 10579 data REM 413 parameters refined using 0 restraints END WGHT 0.0507 0.9804 REM Highest difference peak 0.534, deepest hole -0.367, 1-sigma 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8.90 7 -6 0 63.39 6.10 -7 -6 0 59.59 6.60 -7 6 0 58.89 4.20 7 6 0 46.90 7.40 -7 6 0 56.69 8.40 -8 -6 0 3.70 2.10 -8 -6 0 13.30 4.50 -8 -6 0 8.90 2.20 -8 -6 0 2.20 2.90 8 -6 0 6.40 4.10 8 6 0 8.30 4.40 -8 6 0 8.40 4.10 -8 6 0 4.30 1.90 -9 -6 0 5.80 3.40 -9 -6 0 1.70 3.20 -9 -6 0 4.90 1.70 9 -6 0 9.90 5.00 9 6 0 3.70 4.50 -9 6 0 9.10 4.90 -9 6 0 1.70 2.00 10 -6 0 1.70 4.10 -10 -6 0 10.80 4.20 -10 -6 0 7.70 4.50 -10 6 0 5.70 5.10 10 6 0 9.10 5.20 -11 -6 0 28.30 6.30 -11 -6 0 22.60 6.50 11 -6 0 26.30 7.40 11 6 0 18.10 6.90 -11 6 0 15.20 6.40 -12 -6 0 4.70 4.20 -12 -6 0 7.50 5.00 12 -6 0 9.50 5.60 -12 -6 0 -2.10 4.50 12 6 0 -0.50 4.50 -12 6 0 1.90 5.40 -13 -6 0 14.00 7.00 -13 -6 0 31.00 8.70 13 -6 0 14.20 7.10 -13 6 0 14.90 7.20 13 6 0 11.60 6.70 -14 -6 0 0.00 5.80 -14 -6 0 -0.80 4.50 14 -6 0 13.60 7.00 14 6 0 -4.50 5.40 -14 6 0 -1.80 4.70 0 -7 0 1.90 2.40 0 -7 0 6.60 2.00 0 7 0 6.60 1.70 0 7 0 4.40 1.90 -1 -7 0 2.00 1.80 -1 -7 0 3.30 2.50 1 -7 0 4.60 2.50 -1 -7 0 4.90 1.40 1 -7 0 0.50 1.60 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11.70 -1 8 0 225.48 10.40 1 8 0 212.88 11.30 1 8 0 216.28 11.20 -1 8 0 222.88 12.10 -2 -8 0 21.90 3.70 -2 -8 0 15.40 3.80 -2 -8 0 14.90 2.10 2 -8 0 17.40 3.30 2 -8 0 20.70 3.70 2 -8 0 19.70 4.20 -2 8 0 21.70 4.20 2 8 0 19.20 2.40 2 8 0 16.80 2.90 2 8 0 15.00 3.40 3 -8 0 266.87 14.40 -3 -8 0 267.57 14.20 -3 -8 0 275.37 12.10 3 -8 0 264.47 15.00 -3 -8 0 249.28 14.50 3 -8 0 280.17 14.50 -3 8 0 252.67 15.00 3 8 0 264.07 14.40 3 8 0 276.87 12.50 3 8 0 246.38 13.30 -4 -8 0 0.10 2.00 4 -8 0 1.10 2.10 -4 -8 0 1.50 1.10 4 -8 0 -1.20 2.50 -4 -8 0 -0.80 1.80 -4 8 0 3.30 2.70 4 8 0 -0.90 1.60 -5 -8 0 12.20 3.50 5 -8 0 11.00 3.50 -5 -8 0 9.50 2.00 -5 -8 0 9.10 3.00 5 -8 0 8.50 3.30 -5 -8 0 12.30 3.30 5 8 0 10.90 3.80 -5 8 0 9.30 4.10 6 -8 0 3.30 3.20 -6 -8 0 6.10 3.20 -6 -8 0 4.60 2.80 -6 -8 0 5.70 2.80 6 -8 0 6.50 2.90 -6 -8 0 6.20 2.10 -6 8 0 9.70 4.20 6 8 0 2.40 2.60 -7 -8 0 217.48 13.90 7 -8 0 204.88 12.50 -7 -8 0 188.98 11.80 -7 -8 0 206.08 11.40 7 -8 0 217.78 14.70 -7 8 0 193.28 15.00 7 8 0 215.98 14.60 -8 -8 0 66.19 6.90 -8 -8 0 58.29 8.20 8 -8 0 46.80 8.20 -8 -8 0 57.89 6.10 -8 8 0 46.60 8.70 8 8 0 87.79 10.90 -9 -8 0 56.59 8.70 9 -8 0 62.89 9.70 -9 -8 0 68.39 7.50 -9 -8 0 71.49 6.60 9 8 0 75.09 10.70 -9 8 0 51.29 9.30 -10 -8 0 6.20 4.60 10 -8 0 2.90 4.40 -10 -8 0 7.70 3.60 -10 -8 0 1.40 1.90 -10 8 0 0.40 4.50 10 8 0 -1.00 4.50 11 -8 0 -3.50 4.30 -11 -8 0 0.80 3.50 11 8 0 -0.40 4.80 -11 8 0 15.40 6.10 12 -8 0 39.70 9.00 -12 -8 0 21.40 6.80 12 8 0 31.10 8.50 -12 8 0 18.90 7.70 13 -8 0 28.30 9.10 -13 -8 0 44.40 9.20 -13 -8 0 26.90 9.10 -13 8 0 32.10 9.00 13 8 0 43.20 10.20 -14 -8 0 24.70 9.10 14 -8 0 42.40 11.00 14 8 0 43.70 10.40 -14 8 0 19.60 8.80 0 -9 0 -0.30 1.70 0 -9 0 7.00 3.00 0 9 0 2.50 1.50 0 9 0 2.60 2.10 1 -9 0 16.50 3.30 -1 -9 0 21.00 3.70 -1 -9 0 16.60 4.20 1 -9 0 19.10 4.40 1 9 0 21.50 3.50 1 9 0 14.20 3.20 -1 9 0 21.40 2.90 -1 9 0 17.40 3.80 -2 -9 0 233.28 13.20 2 -9 0 186.48 11.80 2 -9 0 209.18 13.10 -2 -9 0 217.68 10.10 2 -9 0 211.68 11.70 -2 -9 0 201.18 11.80 -2 9 0 218.18 10.10 -2 9 0 206.08 12.50 2 9 0 208.58 11.30 2 9 0 188.58 11.60 3 -9 0 138.29 10.00 -3 -9 0 131.09 8.90 3 -9 0 121.69 9.00 3 -9 0 126.19 8.90 -3 -9 0 138.89 9.80 -3 -9 0 134.89 6.90 -3 9 0 133.79 10.00 3 9 0 146.19 8.50 3 9 0 119.39 8.90 -4 -9 0 85.49 8.30 4 -9 0 80.69 8.40 4 -9 0 73.29 8.00 4 -9 0 65.79 7.50 -4 -9 0 82.69 8.40 -4 -9 0 72.89 4.50 4 9 0 72.99 8.10 -4 9 0 85.79 9.10 -5 -9 0 240.98 11.30 5 -9 0 223.88 14.00 -5 -9 0 251.47 14.30 -5 -9 0 237.68 13.90 5 -9 0 211.58 14.20 5 9 0 214.88 14.30 -5 9 0 274.27 16.30 -6 -9 0 470.65 20.50 -6 -9 0 426.36 22.90 6 -9 0 477.25 24.60 6 -9 0 455.15 23.20 -6 -9 0 423.36 23.20 -6 -9 0 445.36 22.70 6 9 0 444.46 24.20 -6 9 0 472.25 25.60 7 -9 0 73.59 7.90 -7 -9 0 67.29 6.00 -7 -9 0 68.79 7.50 -7 -9 0 64.39 8.30 7 -9 0 60.29 8.80 7 9 0 61.29 9.00 -7 9 0 55.29 9.00 -8 -9 0 31.20 4.50 -8 -9 0 22.80 6.00 8 -9 0 30.10 6.50 -8 -9 0 34.30 5.20 -8 9 0 29.40 7.40 8 9 0 38.30 7.60 -9 -9 0 5.30 3.80 -9 -9 0 6.00 2.90 9 -9 0 8.00 4.90 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6.20 -3 10 0 30.60 5.70 4 -10 0 9.10 3.60 -4 -10 0 16.40 2.30 -4 -10 0 17.50 4.10 -4 -10 0 12.10 3.90 4 -10 0 17.10 4.30 4 -10 0 9.90 3.70 -4 10 0 20.30 4.80 4 10 0 12.50 3.10 4 10 0 12.40 3.80 -5 -10 0 63.69 7.50 5 -10 0 47.30 7.00 -5 -10 0 63.39 4.30 5 -10 0 76.89 8.60 -5 -10 0 54.99 7.10 -5 10 0 62.49 8.60 5 10 0 55.49 7.80 -6 -10 0 39.70 4.00 -6 -10 0 42.00 6.50 -6 -10 0 46.80 6.50 6 -10 0 28.90 6.20 6 -10 0 41.50 6.70 -6 10 0 27.70 6.50 6 10 0 42.90 7.40 7 -10 0 3.60 4.00 -7 -10 0 3.60 3.00 -7 -10 0 10.00 4.10 -7 -10 0 6.30 2.10 7 -10 0 -0.90 2.90 7 10 0 4.70 4.10 -7 10 0 3.20 4.40 -8 -10 0 34.60 5.50 -8 -10 0 26.40 6.30 8 -10 0 35.20 7.40 -8 -10 0 33.30 4.30 -8 10 0 23.30 7.00 8 10 0 28.40 6.80 9 -10 0 52.59 9.60 -9 -10 0 46.80 6.40 -9 -10 0 47.00 8.00 -9 10 0 53.29 9.80 9 10 0 29.50 7.70 -10 -10 0 17.80 5.90 -10 -10 0 10.80 3.40 10 -10 0 6.40 5.40 -10 10 0 17.40 7.00 10 10 0 9.90 5.80 11 -10 0 15.00 6.90 -11 -10 0 11.80 5.20 11 10 0 17.90 7.30 -11 10 0 11.40 6.70 -12 -10 0 8.50 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274.97 16.70 5 -11 0 290.27 16.90 -5 -11 0 276.07 12.60 -5 -11 0 244.38 15.50 5 11 0 241.78 16.20 -5 11 0 259.07 17.40 -6 -11 0 186.28 12.60 -6 -11 0 180.58 9.00 6 -11 0 168.18 13.00 -6 -11 0 152.58 11.70 6 -11 0 178.78 12.70 -6 11 0 164.38 15.70 6 11 0 147.39 14.40 7 -11 0 10.70 4.80 -7 -11 0 5.30 3.70 7 -11 0 10.40 4.30 -7 -11 0 7.60 4.00 -7 -11 0 11.20 2.40 7 11 0 11.10 4.80 -7 11 0 8.70 4.90 -8 -11 0 14.30 4.40 -8 -11 0 1.80 3.60 8 -11 0 8.70 5.20 8 11 0 4.10 4.50 -8 11 0 3.10 5.10 9 -11 0 61.19 10.20 -9 -11 0 44.70 7.90 -9 -11 0 52.69 7.10 -9 11 0 58.49 10.40 9 11 0 67.49 10.50 10 -11 0 -1.90 4.70 -10 -11 0 0.20 3.60 -10 -11 0 -1.90 2.60 10 11 0 -0.80 4.40 -10 11 0 7.40 5.50 -11 -11 0 61.89 10.10 11 -11 0 61.29 11.70 -11 11 0 66.69 12.20 11 11 0 49.99 10.40 -12 -11 0 115.09 17.10 -12 -11 0 160.58 16.40 12 -11 0 148.69 17.80 -12 11 0 118.59 17.20 12 11 0 117.99 16.00 -13 -11 0 90.79 13.00 13 -11 0 94.79 15.20 -13 -11 0 111.19 16.60 13 11 0 87.99 13.90 -13 11 0 105.89 16.20 0 -12 0 323.47 18.60 0 -12 0 380.86 21.10 0 12 0 363.96 18.00 0 12 0 382.36 19.30 -1 -12 0 1.80 2.40 1 -12 0 3.40 3.20 1 -12 0 -1.90 1.90 -1 -12 0 -2.80 2.60 -1 12 0 -1.10 2.50 -1 12 0 1.60 1.80 1 12 0 -2.50 1.90 1 12 0 0.00 2.20 -2 -12 0 50.79 7.70 -2 -12 0 53.19 6.70 2 -12 0 58.69 8.10 2 -12 0 47.30 6.10 2 -12 0 53.79 4.90 2 -12 0 54.79 7.00 2 12 0 43.30 5.80 -2 12 0 42.10 4.60 -2 12 0 47.20 7.00 2 12 0 35.10 5.40 -3 -12 0 8.60 3.40 3 -12 0 3.10 3.00 3 -12 0 6.80 3.00 -3 -12 0 9.20 2.10 3 -12 0 8.20 4.10 3 -12 0 7.80 1.30 3 -12 0 6.20 1.40 -3 -12 0 8.00 4.00 3 12 0 8.60 3.10 -3 12 0 11.80 2.40 3 12 0 3.90 3.20 -3 12 0 8.50 4.00 -4 -12 0 320.97 19.30 4 -12 0 330.47 18.80 4 -12 0 347.07 19.90 -4 -12 0 323.77 15.00 4 -12 0 339.47 18.80 -4 -12 0 294.37 17.80 4 12 0 304.37 17.10 4 12 0 329.37 18.80 -4 12 0 347.17 20.10 -5 -12 0 3.20 2.90 -5 -12 0 3.50 1.50 5 -12 0 5.50 3.80 5 -12 0 5.10 3.70 -5 -12 0 0.50 3.00 5 12 0 -1.30 3.10 -5 12 0 7.10 4.50 -6 -12 0 13.70 4.90 -6 -12 0 16.30 4.70 6 -12 0 20.90 5.60 -6 -12 0 12.40 2.30 6 -12 0 11.70 4.70 6 12 0 11.80 5.10 -6 12 0 2.60 3.40 -7 -12 0 56.09 7.80 -7 -12 0 51.29 7.80 7 -12 0 54.69 8.60 7 -12 0 41.10 8.50 7 12 0 49.60 8.50 -7 12 0 57.79 9.80 8 -12 0 127.19 14.20 -8 -12 0 115.89 12.20 -8 -12 0 119.39 11.80 8 12 0 118.09 13.70 -8 12 0 113.99 14.00 -9 -12 0 32.70 7.10 9 -12 0 20.60 7.00 -9 -12 0 28.80 6.00 9 12 0 49.60 9.70 -9 12 0 35.50 8.80 10 -12 0 14.10 6.70 -10 -12 0 22.20 6.60 -10 -12 0 10.30 4.00 -10 12 0 5.20 5.90 10 12 0 14.50 6.60 -11 -12 0 18.50 6.30 11 -12 0 11.10 6.70 11 12 0 28.70 8.80 -11 12 0 24.60 8.70 -12 -12 0 24.10 7.20 -12 -12 0 28.60 9.80 12 -12 0 21.00 7.50 12 12 0 22.10 8.70 -12 12 0 20.30 8.30 13 -12 0 13.80 7.80 -13 -12 0 9.20 7.20 -13 12 0 -8.20 4.60 13 12 0 -7.50 5.00 0 -13 0 12.40 3.70 0 -13 0 15.60 5.10 0 13 0 12.60 3.80 0 13 0 16.40 3.50 1 -13 0 49.60 6.30 -1 -13 0 48.50 8.10 -1 -13 0 56.79 7.30 1 -13 0 51.59 8.50 1 -13 0 41.70 6.50 -1 13 0 50.39 5.50 1 13 0 56.09 6.70 -1 13 0 59.49 7.40 1 13 0 52.29 6.80 2 -13 0 -2.10 1.60 -2 -13 0 7.50 4.20 2 -13 0 -0.90 2.50 -2 -13 0 0.80 2.30 2 -13 0 -0.60 2.40 2 -13 0 3.80 2.60 -2 13 0 1.60 3.30 -2 13 0 3.10 2.00 2 13 0 -1.10 2.30 2 13 0 2.10 2.70 3 -13 0 0.70 1.20 3 -13 0 3.20 3.20 3 -13 0 2.10 3.10 3 -13 0 0.80 2.60 -3 -13 0 -0.40 2.30 -3 -13 0 3.10 2.90 -3 13 0 7.70 3.80 3 13 0 -0.20 2.30 -3 13 0 2.10 1.80 3 13 0 -5.30 2.60 -4 -13 0 10.40 4.80 -4 -13 0 19.50 2.90 4 -13 0 9.90 4.50 -4 -13 0 14.90 4.40 4 -13 0 30.20 6.60 4 -13 0 15.30 4.60 4 13 0 12.90 3.80 -4 13 0 15.60 5.30 4 13 0 11.10 4.60 -4 13 0 19.40 2.90 -5 -13 0 85.29 10.60 -5 -13 0 99.79 10.30 5 -13 0 101.19 11.10 5 -13 0 85.59 10.60 -5 -13 0 94.09 5.80 -5 13 0 98.29 12.00 5 13 0 99.29 11.20 6 -13 0 4.00 4.20 6 -13 0 12.80 4.80 -6 -13 0 7.10 3.90 -6 -13 0 8.40 4.60 -6 13 0 13.30 6.20 6 13 0 4.10 4.30 -7 -13 0 37.80 7.20 -7 -13 0 56.49 8.50 7 -13 0 42.80 8.40 7 13 0 49.50 9.00 -7 13 0 40.60 8.30 -8 -13 0 56.29 8.30 -8 -13 0 32.70 6.70 8 -13 0 44.50 9.00 8 13 0 34.80 8.20 -8 13 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15.70 5.80 -4 -14 0 8.90 3.90 4 -14 0 17.20 6.00 4 -14 0 20.50 5.60 -4 14 0 14.00 5.40 4 14 0 14.00 4.00 -4 14 0 14.60 2.80 4 14 0 22.00 5.60 -5 -14 0 20.90 6.40 5 -14 0 23.20 6.00 -5 -14 0 24.50 5.60 5 -14 0 13.50 5.40 5 14 0 8.40 4.80 -5 14 0 18.70 6.30 6 -14 0 10.10 5.10 -6 -14 0 -2.80 3.70 -6 -14 0 6.10 3.80 6 -14 0 2.00 4.10 -6 14 0 -4.50 3.70 6 14 0 5.90 4.70 -7 -14 0 1.90 3.90 7 -14 0 -1.70 2.90 -7 -14 0 3.90 3.80 -7 14 0 3.50 5.10 7 14 0 2.10 4.40 -8 -14 0 24.80 6.30 8 -14 0 16.40 6.40 -8 -14 0 18.70 5.70 -8 14 0 17.90 7.40 8 14 0 14.00 5.90 9 -14 0 30.70 8.30 -9 -14 0 42.50 7.90 -9 -14 0 23.40 6.40 9 14 0 18.90 7.10 -9 14 0 27.60 8.50 -10 -14 0 0.60 3.80 10 -14 0 20.60 8.20 -10 -14 0 8.70 4.90 -10 14 0 0.30 5.50 10 14 0 15.30 6.90 11 -14 0 5.80 6.10 -11 -14 0 5.50 5.40 11 14 0 9.80 7.20 -11 14 0 -6.30 5.40 -12 -14 0 4.90 7.10 -12 -14 0 21.60 7.40 12 -14 0 15.50 8.60 12 14 0 10.90 8.20 -12 14 0 14.00 8.30 0 -15 0 4.70 3.20 0 -15 0 3.50 4.40 0 15 0 3.90 2.90 0 15 0 4.10 3.60 1 -15 0 4.20 4.40 1 -15 0 1.90 3.30 1 -15 0 4.80 3.00 -1 -15 0 -0.70 3.90 1 -15 0 -0.60 2.30 -1 -15 0 0.20 2.80 -1 15 0 2.70 2.60 1 15 0 2.50 3.00 -1 15 0 2.70 3.70 1 15 0 5.60 3.40 2 -15 0 292.77 19.70 2 -15 0 267.67 17.40 2 -15 0 275.67 14.60 -2 -15 0 303.57 19.80 2 -15 0 253.67 16.30 -2 -15 0 274.77 17.00 -2 15 0 299.67 15.10 2 15 0 287.47 16.70 2 15 0 277.57 16.80 -2 15 0 300.57 18.20 -3 -15 0 0.40 2.70 3 -15 0 2.60 3.60 -3 -15 0 0.80 4.00 3 -15 0 -2.50 2.60 3 -15 0 2.70 3.10 3 15 0 0.10 3.10 -3 15 0 -1.10 3.40 3 15 0 3.10 3.10 -3 15 0 -2.10 1.80 4 -15 0 1.50 4.00 -4 -15 0 5.00 4.30 4 -15 0 1.70 3.20 4 -15 0 -5.10 2.70 -4 -15 0 -3.40 2.80 -4 15 0 2.60 3.40 4 15 0 3.20 3.30 -4 15 0 0.60 1.70 4 15 0 -1.40 3.30 5 -15 0 3.10 3.70 5 -15 0 -5.50 3.00 -5 -15 0 1.00 3.30 -5 -15 0 -2.30 3.60 -5 15 0 0.40 3.20 5 15 0 -6.70 2.80 -6 -15 0 102.19 11.30 -6 -15 0 121.79 13.30 6 -15 0 92.39 12.20 6 -15 0 81.79 11.60 6 15 0 107.49 12.70 -6 15 0 131.39 14.80 -7 -15 0 23.00 6.10 -7 -15 0 30.40 7.30 7 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4.50 3 -16 0 3.10 3.30 3 16 0 -3.00 3.20 -3 16 0 2.10 2.30 3 16 0 1.80 3.20 -3 16 0 -5.10 3.60 4 -16 0 7.90 4.50 -4 -16 0 -3.10 2.70 4 -16 0 5.70 4.90 -4 -16 0 -6.90 2.50 4 -16 0 4.40 3.70 4 16 0 8.00 4.40 4 16 0 2.80 3.20 -4 16 0 6.00 4.70 -5 -16 0 15.30 4.80 -5 -16 0 21.60 6.70 5 -16 0 4.90 4.00 5 -16 0 15.50 6.10 -5 16 0 -1.20 4.30 5 16 0 6.20 4.70 -6 -16 0 74.19 10.80 -6 -16 0 58.19 8.70 6 -16 0 58.59 9.70 6 -16 0 65.99 10.70 -6 16 0 58.99 10.20 6 16 0 63.09 10.20 -7 -16 0 220.88 16.00 -7 -16 0 219.28 16.90 7 -16 0 207.18 19.60 -7 16 0 192.78 19.50 7 16 0 207.48 20.10 8 -16 0 -4.30 4.10 -8 -16 0 0.30 3.40 -8 -16 0 0.90 5.10 8 16 0 -2.70 4.40 -8 16 0 2.60 4.50 9 -16 0 71.49 12.20 -9 -16 0 44.00 8.70 -9 -16 0 38.90 8.80 -9 16 0 29.00 9.20 9 16 0 36.20 9.50 -10 -16 0 20.70 6.50 -10 -16 0 18.20 6.60 10 -16 0 14.30 7.50 -10 16 0 11.20 8.00 10 16 0 19.30 7.90 11 -16 0 42.10 10.70 -11 -16 0 23.70 7.00 -11 -16 0 49.60 12.20 -11 -16 0 48.50 9.70 -11 16 0 59.89 12.80 11 16 0 33.20 10.20 0 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26.40 9.00 -9 19 0 17.00 8.90 9 19 0 38.30 10.10 0 -20 0 99.29 12.80 0 -20 0 106.79 11.70 0 -20 0 124.49 16.70 0 20 0 125.39 13.50 -1 -20 0 -1.40 3.50 -1 -20 0 0.20 4.00 1 -20 0 -6.20 4.90 -1 -20 0 6.10 6.00 1 -20 0 2.30 3.60 -1 -20 0 -0.80 3.00 1 -20 0 3.10 4.70 1 20 0 6.20 4.20 -1 20 0 -8.00 3.70 1 20 0 -1.80 3.90 -2 -20 0 -1.40 3.70 -2 -20 0 2.20 5.60 -2 -20 0 11.60 5.30 2 -20 0 -5.00 4.70 2 -20 0 8.70 4.40 2 -20 0 -1.20 4.30 2 20 0 -0.60 3.80 2 20 0 12.30 5.10 -2 20 0 1.00 5.20 3 -20 0 28.80 9.20 3 -20 0 19.40 6.80 -3 -20 0 12.50 5.50 -3 -20 0 25.60 7.90 3 -20 0 21.90 6.40 -3 -20 0 27.30 8.60 3 20 0 23.70 7.00 -3 20 0 23.40 7.50 3 20 0 15.60 5.80 4 -20 0 -2.40 5.80 4 -20 0 -4.70 3.90 4 -20 0 -2.40 4.30 -4 -20 0 15.10 6.50 -4 -20 0 0.40 3.90 -4 -20 0 -0.50 5.20 4 20 0 0.70 4.30 -4 20 0 1.30 5.50 4 20 0 -2.20 3.60 5 -20 0 2.40 6.60 5 -20 0 3.40 4.90 -5 -20 0 4.30 4.50 -5 -20 0 3.90 6.00 -5 -20 0 6.10 6.60 -5 20 0 -0.60 4.20 5 20 0 9.30 5.20 -6 -20 0 27.70 8.60 -6 -20 0 9.40 7.30 -6 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3 43.50 3.10 -6 7 3 54.59 8.20 -5 -7 3 8.30 1.40 -5 -7 3 2.50 2.30 -5 -7 3 11.30 2.80 5 -7 -3 16.10 3.80 5 -7 -3 11.70 3.30 -5 7 3 3.50 3.00 -5 7 3 7.40 1.30 5 7 -3 8.10 3.40 -5 7 3 12.90 4.20 4 -7 -3 6.70 1.40 -4 -7 3 11.50 2.90 4 -7 -3 1.90 2.30 -4 -7 3 6.10 0.60 4 -7 -3 9.60 2.80 4 -7 -3 4.90 2.40 -4 -7 3 6.80 2.20 -4 7 3 5.20 1.20 -4 7 3 5.60 3.00 -4 7 3 3.90 3.20 4 7 -3 6.30 2.90 -3 -7 3 38.60 5.20 3 -7 -3 36.10 4.80 -3 -7 3 46.30 4.60 3 -7 -3 48.90 5.30 3 -7 -3 37.40 2.90 3 7 -3 32.70 4.40 3 7 -3 41.80 5.40 -3 7 3 44.40 6.30 -3 7 3 48.40 6.40 -2 -7 3 27.30 3.50 2 -7 -3 22.70 3.60 -2 -7 3 26.10 4.20 2 -7 -3 25.80 2.60 -2 -7 3 32.40 4.80 -2 7 3 22.70 4.20 -2 7 3 16.20 4.30 2 7 -3 22.40 3.60 2 7 -3 24.20 1.40 2 7 -3 25.90 3.70 1 -7 -3 264.27 13.50 1 -7 -3 268.27 13.40 -1 -7 3 267.47 13.10 -1 -7 3 242.68 13.70 -1 -7 3 252.47 14.40 -1 7 3 268.57 15.30 1 7 -3 280.77 13.10 1 7 -3 270.67 11.60 -1 7 3 259.17 14.00 1 7 -3 270.07 13.40 0 -7 -3 352.96 17.30 0 -7 -3 343.67 16.50 0 -7 3 360.26 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11.30 6.50 12 -9 -3 12.90 7.10 12 9 -3 6.40 6.00 -12 9 3 2.00 5.70 11 -9 -3 3.50 5.50 -11 -9 3 5.40 4.00 -11 -9 3 2.00 4.80 -11 9 3 11.40 7.00 11 9 -3 7.90 6.40 -10 -9 3 7.80 4.10 -10 -9 3 3.90 2.60 -10 -9 3 20.00 7.00 10 -9 -3 9.90 5.70 -10 9 3 3.10 5.40 10 9 -3 17.10 6.20 -9 -9 3 -1.10 4.40 -9 -9 3 0.90 2.60 9 -9 -3 -0.70 3.80 -9 -9 3 3.70 3.20 -9 9 3 16.40 6.20 9 9 -3 -0.70 3.80 -8 -9 3 -1.30 2.00 8 -9 -3 -1.60 3.20 -8 -9 3 -1.90 3.70 -8 -9 3 2.70 2.70 8 9 -3 -2.20 3.50 -8 9 3 12.10 5.60 7 -9 -3 20.70 5.70 -7 -9 3 18.30 2.40 -7 -9 3 13.00 3.80 -7 -9 3 15.20 4.10 7 -9 -3 16.80 4.40 -7 9 3 13.20 5.00 7 9 -3 7.80 4.40 6 -9 -3 4.60 3.10 -6 -9 3 -0.60 2.10 -6 -9 3 1.00 0.80 -6 -9 3 0.20 2.60 6 -9 -3 2.90 2.80 6 9 -3 5.30 3.60 -6 9 3 2.90 3.80 -5 -9 3 121.69 8.40 5 -9 -3 112.59 10.70 5 -9 -3 120.49 9.40 -5 -9 3 130.89 9.30 5 -9 -3 122.19 9.30 -5 9 3 111.19 11.90 5 9 -3 119.99 11.30 -4 -9 3 2.00 2.00 4 -9 -3 1.50 2.30 4 -9 -3 -0.40 0.80 4 -9 -3 2.40 2.10 4 -9 -3 3.40 2.60 -4 -9 3 -2.80 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6.20 3 -10 3 41.80 2.60 -3 10 -3 44.00 2.40 3 10 3 36.60 4.40 3 10 3 41.70 6.20 -3 10 -3 46.90 6.40 4 -10 3 4.20 2.50 -4 -10 -3 0.40 2.70 -4 -10 -3 4.00 2.00 4 -10 3 6.00 3.80 -4 10 -3 10.40 4.10 4 10 3 11.60 3.80 4 10 3 9.30 2.60 -5 -10 -3 222.78 12.20 5 -10 3 223.68 14.70 -5 -10 -3 255.17 15.30 -5 -10 -3 222.88 14.80 5 -10 3 269.57 15.50 -5 10 -3 213.28 14.80 5 10 3 242.88 15.30 -6 -10 -3 182.98 12.80 6 -10 3 152.48 11.60 -6 -10 -3 146.89 9.20 6 -10 3 139.29 13.30 -6 -10 -3 151.68 11.10 6 10 3 143.19 13.70 -6 10 -3 144.29 14.00 -7 -10 -3 6.50 4.00 7 -10 3 5.40 3.90 7 -10 3 6.60 3.70 -7 -10 -3 1.70 3.10 -7 -10 -3 7.30 2.70 -7 10 -3 5.20 4.20 7 10 3 3.40 4.20 -8 -10 -3 7.40 4.50 8 -10 3 -3.20 3.30 -8 -10 -3 -1.10 2.30 -8 -10 -3 -1.10 2.80 8 10 3 -2.10 3.80 -8 10 -3 -6.60 3.10 -9 -10 -3 4.50 3.20 9 -10 3 5.10 4.60 -9 -10 -3 11.60 5.20 -9 -10 -3 2.60 3.10 9 10 3 -2.90 3.90 -9 10 -3 3.30 4.80 -10 -10 -3 10.10 5.30 -10 -10 -3 17.80 4.20 10 -10 3 24.00 7.60 10 10 3 9.30 5.50 -10 10 -3 17.80 6.90 -11 -10 -3 26.50 7.50 11 -10 3 15.10 7.00 -11 10 -3 26.80 8.20 11 10 3 31.10 9.00 -12 -10 -3 -5.10 4.20 12 -10 3 -3.10 5.10 -12 10 -3 -1.50 4.60 12 10 3 -2.20 5.50 13 -10 3 12.00 7.20 -13 -10 -3 6.40 5.80 -13 10 -3 0.20 6.30 13 10 3 7.70 6.70 13 -11 -3 27.00 9.10 -13 -11 3 39.40 10.70 -13 11 3 29.80 10.20 13 11 -3 15.90 8.90 12 -11 -3 17.90 7.40 -12 -11 3 6.70 6.40 12 11 -3 -2.80 5.20 -12 11 3 16.20 7.80 11 -11 -3 46.40 10.20 -11 -11 3 39.30 7.60 -11 -11 3 34.40 9.60 -11 11 3 39.00 10.10 11 11 -3 38.30 9.40 -10 -11 3 21.90 5.70 -10 -11 3 25.60 5.30 -10 -11 3 30.30 8.30 10 -11 -3 20.80 7.30 10 11 -3 23.10 7.30 -10 11 3 25.70 8.00 -9 -11 3 15.70 6.00 -9 -11 3 9.10 4.00 9 -11 -3 12.60 5.10 -9 -11 3 9.40 4.10 9 11 -3 9.20 5.60 -9 11 3 9.40 5.90 8 -11 -3 -3.50 3.40 -8 -11 3 0.80 5.10 -8 -11 3 1.80 3.00 -8 -11 3 4.70 3.00 8 11 -3 0.50 4.30 -8 11 3 6.60 5.20 -7 -11 3 223.08 13.90 7 -11 -3 220.58 15.80 -7 -11 3 228.58 14.50 7 -11 -3 216.38 14.50 -7 11 3 174.18 17.90 7 11 -3 225.78 16.00 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3.70 2.50 0 -11 3 1.90 2.20 0 -11 -3 2.80 2.10 0 -11 3 4.00 1.80 0 -11 3 2.00 2.30 0 -11 3 0.10 3.00 0 -11 -3 4.50 3.60 0 11 -3 3.50 1.90 0 11 3 2.10 2.10 0 11 3 4.10 2.70 0 11 -3 3.50 2.80 1 -11 3 135.59 10.10 -1 -11 -3 94.69 9.00 -1 -11 -3 97.09 7.00 -1 -11 -3 92.99 10.40 1 -11 3 109.29 7.50 1 -11 3 120.69 8.60 1 -11 3 100.69 7.00 -1 11 -3 107.59 8.20 1 11 3 105.29 7.60 1 11 3 105.49 7.80 -1 11 -3 103.69 6.40 2 -11 3 50.69 4.50 -2 -11 -3 45.30 7.30 -2 -11 -3 47.00 5.00 2 -11 3 49.30 6.50 -2 -11 -3 40.70 6.00 2 -11 3 38.50 5.40 2 -11 3 43.40 7.20 -2 11 -3 51.49 6.70 2 11 3 51.29 5.50 -2 11 -3 46.00 3.40 2 11 3 42.70 6.10 3 -11 3 90.09 9.70 -3 -11 -3 81.69 8.60 3 -11 3 80.69 8.20 -3 -11 -3 73.49 5.50 -3 -11 -3 65.79 8.50 3 -11 3 65.99 3.90 3 -11 3 40.20 6.70 -3 11 -3 84.79 9.00 3 11 3 72.99 6.60 -3 11 -3 76.69 3.90 3 11 3 73.09 8.30 4 -11 3 156.28 13.80 4 -11 3 122.69 11.50 -4 -11 -3 132.59 12.40 -4 -11 -3 138.89 8.30 -4 -11 -3 148.59 10.60 -4 11 -3 123.29 12.20 4 11 3 135.79 10.80 4 11 3 145.29 8.90 5 -11 3 485.75 25.30 5 -11 3 437.36 24.50 -5 -11 -3 498.95 21.80 -5 -11 -3 437.16 24.50 -5 -11 -3 452.15 24.70 5 11 3 454.65 25.10 -5 11 -3 456.05 25.40 -6 -11 -3 -2.40 2.60 -6 -11 -3 1.20 1.90 6 -11 3 -1.30 2.80 -6 -11 -3 -1.00 3.10 6 -11 3 1.10 3.10 -6 11 -3 3.00 3.90 6 11 3 2.20 3.80 7 -11 3 56.89 8.50 -7 -11 -3 58.09 8.20 7 -11 3 68.49 9.90 -7 -11 -3 86.49 10.50 -7 -11 -3 75.29 7.20 7 11 3 56.59 9.30 -7 11 -3 86.99 11.10 -8 -11 -3 46.50 7.30 -8 -11 -3 43.00 8.20 8 -11 3 42.90 8.50 -8 -11 -3 52.09 6.10 8 11 3 35.30 8.00 -8 11 -3 51.19 9.20 -9 -11 -3 -3.50 3.50 -9 -11 -3 -1.60 2.70 9 -11 3 -0.40 3.80 -9 -11 -3 -0.90 2.90 9 11 3 0.60 4.30 -9 11 -3 1.40 4.40 -10 -11 -3 1.40 3.20 -10 -11 -3 4.70 4.60 10 -11 3 -1.00 4.50 -10 11 -3 7.30 5.80 10 11 3 6.10 5.70 -11 -11 -3 1.60 4.70 11 -11 3 5.70 5.90 11 11 3 0.20 5.00 -11 11 -3 2.80 5.60 -12 -11 -3 1.00 5.40 12 -11 3 3.10 4.60 12 11 3 -1.00 5.40 -12 11 -3 7.10 6.50 13 -11 3 -0.10 6.20 -13 -11 -3 9.60 6.10 13 11 3 6.70 7.60 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-5 12 3 -4.70 3.10 5 12 -3 -1.10 2.90 -4 -12 3 33.80 6.50 -4 -12 3 50.09 6.40 4 -12 -3 53.19 7.30 4 -12 -3 49.99 7.10 4 -12 -3 55.09 8.30 -4 12 3 44.40 7.80 4 12 -3 45.10 6.90 4 12 -3 37.40 5.90 3 -12 -3 7.00 3.40 -3 -12 3 2.00 2.70 3 -12 -3 8.10 3.90 -3 -12 3 2.40 3.50 -3 -12 3 7.50 3.00 3 -12 -3 3.70 2.80 3 12 -3 1.40 1.00 3 12 -3 6.40 3.10 -3 12 3 3.50 3.50 3 12 -3 5.50 3.10 2 -12 -3 5.70 3.00 -2 -12 3 4.70 2.70 2 -12 -3 -0.30 3.30 -2 -12 3 9.80 4.30 -2 -12 3 7.70 3.70 2 12 -3 5.50 2.90 2 12 -3 1.30 2.00 2 12 -3 4.90 1.60 -2 12 3 2.50 2.60 -1 -12 3 72.69 7.80 1 -12 -3 62.39 8.70 1 -12 -3 78.29 8.20 -1 -12 3 63.69 8.80 -1 -12 3 67.79 7.70 1 12 -3 69.49 7.40 -1 12 3 78.29 7.00 -1 12 3 63.79 7.90 1 12 -3 78.49 7.30 0 -12 3 13.50 3.00 0 -12 3 6.70 3.00 0 -12 3 8.70 2.90 0 -12 -3 4.70 3.70 0 -12 3 9.50 4.00 0 -12 -3 11.80 3.70 0 12 -3 10.60 2.80 0 12 3 6.40 3.30 0 12 3 11.20 3.10 0 12 -3 2.40 2.90 1 -12 3 16.60 3.60 1 -12 3 16.00 4.70 -1 -12 -3 16.70 4.20 -1 -12 -3 21.30 5.10 1 -12 3 16.50 3.30 -1 -12 -3 23.20 3.90 1 -12 3 14.50 4.20 -1 12 -3 22.20 4.60 1 12 3 21.90 4.30 -1 12 -3 17.70 3.00 1 12 3 18.00 4.00 2 -12 3 4.90 4.00 -2 -12 -3 2.90 2.00 2 -12 3 3.60 1.80 2 -12 3 2.30 2.40 -2 -12 -3 6.20 3.80 -2 -12 -3 3.80 2.80 2 -12 3 4.00 3.00 -2 12 -3 5.90 1.70 2 12 3 6.40 2.70 2 12 3 2.30 2.70 -2 12 -3 1.10 2.90 -3 -12 -3 18.80 5.10 3 -12 3 6.70 1.40 3 -12 3 12.40 4.10 -3 -12 -3 5.70 3.60 -3 -12 -3 9.20 2.60 3 -12 3 7.00 3.30 3 -12 3 0.40 3.20 -3 12 -3 13.80 4.00 3 12 3 6.80 2.90 -3 12 -3 9.20 1.50 3 12 3 9.60 3.80 -4 -12 -3 33.30 6.60 4 -12 3 34.30 6.20 4 -12 3 42.70 7.40 -4 -12 -3 37.00 4.60 -4 -12 -3 34.90 6.30 4 12 3 33.70 4.90 -4 12 -3 40.50 7.10 4 12 3 47.20 7.40 5 -12 3 102.19 11.40 5 -12 3 105.29 11.40 -5 -12 -3 124.59 12.30 -5 -12 -3 115.99 7.50 -5 -12 -3 126.59 12.10 5 12 3 102.19 11.50 -5 12 -3 105.49 11.80 -6 -12 -3 1.00 3.10 6 -12 3 -1.60 3.10 -6 -12 -3 -5.50 3.00 -6 -12 -3 -2.10 1.70 6 -12 3 -0.70 3.10 -6 12 -3 -2.50 2.40 6 12 3 -1.60 3.40 -7 -12 -3 23.30 5.90 7 -12 3 18.30 5.90 -7 -12 -3 30.00 4.40 -7 -12 -3 12.40 5.20 7 12 3 13.30 5.50 -7 12 -3 19.70 6.20 -8 -12 -3 1.50 3.60 -8 -12 -3 -3.90 3.10 -8 -12 -3 2.90 2.80 8 -12 3 -1.60 3.80 -8 12 -3 -0.60 4.20 8 12 3 -3.80 3.90 -9 -12 -3 5.30 3.80 -9 -12 -3 -0.50 3.90 9 -12 3 -0.30 3.40 9 12 3 2.40 5.10 -9 12 -3 5.10 5.20 -10 -12 -3 2.00 3.50 10 -12 3 11.40 6.40 -10 -12 -3 4.10 4.80 10 12 3 6.50 6.20 -10 12 -3 0.50 5.20 11 -12 3 5.00 5.90 -11 -12 -3 3.10 5.00 -11 12 -3 -5.20 4.80 11 12 3 1.10 5.50 -12 -12 -3 9.80 6.70 12 -12 3 27.70 8.10 12 12 3 16.40 7.50 -12 12 -3 -0.40 6.10 12 -13 -3 0.80 5.50 -12 -13 3 2.80 6.20 -12 13 3 6.80 7.00 12 13 -3 4.70 6.30 -11 -13 3 2.50 4.20 -11 -13 3 -1.40 4.90 11 -13 -3 5.90 6.50 -11 -13 3 4.00 5.90 11 13 -3 9.50 6.10 -11 13 3 -4.90 5.10 -10 -13 3 1.50 3.30 10 -13 -3 7.10 6.00 -10 -13 3 1.80 6.10 -10 -13 3 8.50 4.30 -10 13 3 -2.10 4.80 10 13 -3 6.40 5.40 -9 -13 3 13.00 4.90 -9 -13 3 10.70 5.00 9 -13 -3 29.10 8.00 -9 -13 3 4.00 5.00 -9 13 3 12.90 6.70 9 13 -3 18.60 7.00 -8 -13 3 -4.60 2.10 -8 -13 3 0.40 2.70 8 -13 -3 -1.20 3.10 -8 -13 3 3.60 5.10 8 13 -3 -3.00 3.80 -8 13 3 -3.40 4.10 -7 -13 3 129.09 11.80 7 -13 -3 125.69 14.80 -7 -13 3 120.59 12.30 -7 -13 3 99.69 13.50 7 -13 -3 123.19 13.70 -7 13 3 110.09 13.90 7 13 -3 114.19 13.20 -6 -13 3 100.79 10.10 6 -13 -3 85.49 11.00 -6 -13 3 103.09 13.10 6 -13 -3 108.79 12.10 -6 -13 3 106.59 11.60 6 13 -3 101.59 11.80 -6 13 3 98.29 12.50 5 -13 -3 -0.60 3.40 5 -13 -3 -3.60 2.00 -5 -13 3 -2.40 2.30 -5 -13 3 -3.00 2.80 -5 -13 3 -5.40 2.60 5 -13 -3 -1.90 2.80 5 13 -3 -0.50 2.90 -5 13 3 -2.30 3.90 -4 -13 3 -0.30 2.30 4 -13 -3 1.10 3.10 -4 -13 3 -1.80 3.00 4 -13 -3 -3.50 2.90 4 -13 -3 7.50 3.80 -4 -13 3 1.20 3.80 4 13 -3 -3.90 2.30 -4 13 3 -3.00 3.60 4 13 -3 2.30 3.10 3 -13 -3 117.39 11.10 -3 -13 3 147.09 13.60 3 -13 -3 118.79 12.80 3 -13 -3 135.29 12.20 -3 -13 3 109.59 11.90 -3 -13 3 129.49 9.50 3 13 -3 120.39 9.60 -3 13 3 144.49 13.20 3 13 -3 124.69 9.80 2 -13 -3 69.89 9.70 2 -13 -3 75.69 8.50 -2 -13 3 68.59 7.90 -2 -13 3 71.29 9.60 -2 -13 3 75.79 9.00 -2 13 3 65.09 8.70 -2 13 3 84.09 7.50 2 13 -3 84.79 8.40 2 13 -3 66.19 7.80 1 -13 -3 -2.00 2.30 -1 -13 3 -2.90 2.70 -1 -13 3 -2.90 1.90 1 -13 -3 0.70 2.80 -1 -13 3 1.70 2.40 1 13 -3 -0.40 2.00 -1 13 3 2.20 3.00 1 13 -3 -1.20 2.50 -1 13 3 1.70 2.10 0 -13 -3 3.30 3.10 0 -13 -3 0.40 2.60 0 -13 3 -2.10 3.20 0 -13 3 -2.30 1.90 0 -13 3 -0.20 1.90 0 -13 3 -1.00 2.20 0 13 3 -0.90 2.30 0 13 3 -5.40 2.00 0 13 -3 -0.90 1.90 0 13 -3 2.00 2.40 -1 -13 -3 141.19 10.50 1 -13 3 136.59 9.00 1 -13 3 159.18 14.50 1 -13 3 122.69 9.10 -1 -13 -3 127.99 8.90 1 -13 3 143.99 10.50 -1 -13 -3 131.09 13.30 1 13 3 132.89 9.70 1 13 3 146.09 10.00 -1 13 -3 153.68 10.90 -1 13 -3 138.89 8.30 2 -13 3 351.46 19.40 -2 -13 -3 386.56 22.50 2 -13 3 363.76 17.60 2 -13 3 351.16 22.00 -2 -13 -3 378.36 20.60 2 -13 3 368.36 20.70 -2 -13 -3 354.66 18.30 2 13 3 376.06 20.20 -2 13 -3 416.56 21.40 -2 13 -3 376.26 17.10 2 13 3 389.86 19.30 -3 -13 -3 255.27 17.80 3 -13 3 258.27 17.90 3 -13 3 289.37 16.50 -3 -13 -3 271.57 16.80 3 -13 3 268.67 12.50 -3 -13 -3 277.57 14.50 3 -13 3 272.67 17.10 3 13 3 275.97 16.80 -3 13 -3 288.47 17.60 -3 13 -3 286.87 12.60 3 13 3 300.77 15.40 -4 -13 -3 88.29 9.90 -4 -13 -3 105.39 11.80 -4 -13 -3 83.49 6.50 4 -13 3 91.19 10.20 4 -13 3 98.09 11.50 4 13 3 102.19 11.10 4 13 3 92.49 8.40 -4 13 -3 81.99 9.90 -5 -13 -3 -3.40 2.40 -5 -13 -3 5.20 4.10 5 -13 3 1.20 3.30 5 -13 3 -0.70 3.20 -5 -13 -3 -0.10 1.80 5 13 3 -2.90 3.40 -5 13 -3 0.10 3.30 -6 -13 -3 -0.30 1.90 -6 -13 -3 -3.80 3.20 -6 -13 -3 -6.10 2.20 6 -13 3 -2.20 2.80 6 -13 3 -0.10 3.50 -6 13 -3 5.40 4.70 6 13 3 0.80 3.50 -7 -13 -3 3.50 4.30 -7 -13 -3 6.30 4.40 7 -13 3 3.50 4.40 -7 -13 -3 4.50 2.50 7 13 3 2.50 4.40 -7 13 -3 6.20 4.80 -8 -13 -3 4.50 4.10 8 -13 3 15.30 6.00 -8 -13 -3 -0.20 3.70 -8 13 -3 13.70 6.10 8 13 3 9.60 5.60 9 -13 3 23.70 7.40 -9 -13 -3 19.90 6.30 -9 -13 -3 19.60 5.90 -9 13 -3 25.60 8.00 9 13 3 18.80 7.10 -10 -13 -3 23.10 7.40 10 -13 3 10.80 6.70 -10 -13 -3 18.20 5.50 10 13 3 16.90 7.40 -10 13 -3 29.50 8.70 -11 -13 -3 8.40 6.00 11 -13 3 -3.90 4.70 -11 13 -3 3.60 6.40 11 13 3 5.30 7.10 -12 -13 -3 -2.70 5.10 12 -13 3 7.20 7.20 -12 13 -3 -6.50 5.00 12 13 3 4.20 5.70 -12 -14 3 66.89 13.60 12 -14 -3 56.59 12.50 -12 14 3 72.59 13.80 12 14 -3 62.79 13.00 -11 -14 3 12.20 7.20 -11 -14 3 15.50 5.50 11 -14 -3 10.10 6.80 11 14 -3 19.90 7.80 -11 14 3 9.60 6.80 10 -14 -3 -4.50 4.50 -10 -14 3 -1.20 3.70 -10 -14 3 -0.90 3.30 -10 -14 3 -5.50 4.90 -10 14 3 1.00 5.50 10 14 -3 3.10 5.10 -9 -14 3 85.89 10.40 9 -14 -3 75.69 12.10 -9 -14 3 85.89 10.70 -9 -14 3 80.39 13.50 9 14 -3 74.59 11.90 -9 14 3 69.99 12.50 -8 -14 3 26.30 6.00 -8 -14 3 17.80 7.10 8 -14 -3 34.20 8.50 -8 -14 3 34.10 7.40 8 14 -3 30.70 8.10 -8 14 3 23.30 7.70 -7 -14 3 80.29 10.40 -7 -14 3 79.29 12.40 7 -14 -3 84.49 11.50 -7 -14 3 89.39 10.00 -7 14 3 73.09 11.90 7 14 -3 84.29 11.50 -6 -14 3 54.69 7.50 -6 -14 3 50.39 8.50 -6 -14 3 55.49 10.00 6 -14 -3 49.00 8.40 6 -14 -3 56.29 9.40 -6 14 3 41.10 8.30 6 14 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52.39 7.90 4 -10 -4 64.29 4.20 4 -10 -4 67.19 7.50 4 -10 -4 62.29 7.60 -4 -10 4 69.59 6.70 -4 -10 4 64.89 7.90 -4 10 4 70.69 8.90 -4 10 4 55.99 8.50 4 10 -4 62.69 7.80 3 -10 -4 96.29 9.90 3 -10 -4 81.49 8.30 -3 -10 4 91.19 9.40 -3 -10 4 78.19 8.90 3 -10 -4 71.79 7.60 -3 -10 4 87.09 6.60 3 10 -4 74.89 7.90 3 10 -4 73.19 7.50 -3 10 4 80.69 9.10 -3 10 4 79.89 10.00 -2 -10 4 3.90 2.30 -2 -10 4 0.70 2.50 2 -10 -4 3.90 2.40 -2 -10 4 4.30 3.00 2 10 -4 2.80 2.40 2 10 -4 3.20 2.50 2 10 -4 3.20 0.90 -2 10 4 3.40 3.80 -2 10 4 4.20 3.00 1 -10 -4 111.49 8.10 -1 -10 4 114.09 8.50 -1 -10 4 101.79 7.70 -1 -10 4 133.59 11.80 1 -10 -4 122.89 8.40 -1 10 4 120.59 8.90 1 10 -4 119.19 6.50 1 10 -4 119.79 8.20 1 10 -4 105.39 7.40 -1 10 4 147.59 13.00 0 -10 4 76.49 8.60 0 -10 4 82.49 7.40 0 -10 4 64.49 6.50 0 -10 -4 65.69 7.20 0 -10 4 60.69 5.60 0 -10 -4 60.49 6.30 0 10 4 69.69 6.50 0 10 4 73.59 9.10 0 10 -4 61.49 4.90 0 10 -4 58.29 6.70 0 10 4 61.29 6.60 1 -10 4 0.20 2.10 -1 -10 -4 3.90 2.40 1 -10 4 5.70 2.10 1 -10 4 3.50 2.80 1 -10 4 1.00 1.70 -1 -10 -4 4.20 2.10 -1 10 -4 4.20 2.70 1 10 4 -0.60 2.40 1 10 4 3.30 2.20 1 10 4 1.40 2.00 -1 10 -4 2.10 1.30 2 -10 4 4.60 2.70 -2 -10 -4 5.60 2.20 2 -10 4 7.10 3.20 2 -10 4 9.10 2.10 -2 -10 -4 7.30 3.20 2 -10 4 15.10 3.40 2 10 4 9.70 4.20 2 10 4 8.10 3.10 2 10 4 7.40 2.40 -2 10 -4 7.90 1.30 -2 10 -4 6.20 3.10 -3 -10 -4 -1.90 2.20 3 -10 4 0.40 0.90 3 -10 4 3.30 2.60 3 -10 4 -2.40 2.30 -3 -10 -4 1.10 1.70 -3 10 -4 1.90 2.40 3 10 4 -1.20 1.40 3 10 4 -0.40 2.50 -4 -10 -4 46.90 5.00 4 -10 4 45.50 6.50 -4 -10 -4 41.70 6.70 4 -10 4 44.80 6.90 4 10 4 46.40 4.90 4 10 4 43.30 6.80 -4 10 -4 32.00 6.10 -5 -10 -4 1.10 1.90 5 -10 4 0.10 3.30 -5 -10 -4 0.50 2.70 5 -10 4 -2.00 2.60 5 10 4 -0.70 2.70 -5 10 -4 3.30 3.60 6 -10 4 162.28 11.70 -6 -10 -4 165.38 9.90 -6 -10 -4 135.39 13.30 6 -10 4 138.69 13.50 -6 10 -4 156.78 14.30 6 10 4 132.09 13.40 7 -10 4 33.20 6.40 -7 -10 -4 39.70 7.40 7 -10 4 48.30 8.10 -7 -10 -4 39.60 5.50 -7 -10 -4 42.50 6.70 7 10 4 41.70 7.70 -7 10 -4 21.40 6.30 8 -10 4 14.30 5.50 -8 -10 -4 13.40 4.20 -8 -10 -4 20.50 6.20 -8 -10 -4 19.60 4.30 -8 10 -4 18.00 5.90 8 10 4 9.10 5.20 -9 -10 -4 16.00 4.30 9 -10 4 14.20 5.90 -9 -10 -4 12.60 4.20 -9 -10 -4 7.80 4.90 9 10 4 8.10 5.50 -9 10 -4 6.40 5.10 -10 -10 -4 7.40 5.40 -10 -10 -4 8.50 4.00 -10 -10 -4 8.00 3.60 10 -10 4 18.20 6.70 10 10 4 10.70 6.20 -10 10 -4 6.20 5.20 -11 -10 -4 23.00 7.30 11 -10 4 14.40 7.10 11 10 4 17.30 7.20 -12 -10 -4 0.10 5.30 12 -10 4 -1.70 4.40 12 10 4 -5.00 4.70 -12 10 -4 -5.20 4.20 -13 -10 -4 3.60 5.40 13 -10 4 6.40 6.40 -13 10 -4 -3.20 5.40 13 10 4 0.90 6.20 -13 -11 4 10.10 7.40 13 -11 -4 -2.90 4.60 13 11 -4 1.10 6.00 -13 11 4 2.80 6.70 -12 -11 4 -2.80 5.30 12 -11 -4 3.10 5.80 -12 11 4 3.60 6.60 12 11 -4 -3.20 5.50 -11 -11 4 24.80 8.30 11 -11 -4 19.10 6.90 -11 -11 4 16.10 7.70 11 11 -4 14.70 7.40 -11 11 4 13.10 7.30 10 -11 -4 17.30 6.80 -10 -11 4 28.60 8.30 -10 -11 4 25.50 5.60 -10 -11 4 23.70 5.30 10 11 -4 4.20 5.40 -10 11 4 23.90 7.90 -9 -11 4 6.70 5.40 9 -11 -4 2.50 4.70 -9 -11 4 1.10 3.10 -9 -11 4 6.40 3.70 9 11 -4 2.00 4.70 -9 11 4 0.00 4.70 -8 -11 4 6.70 5.70 -8 -11 4 1.40 2.60 8 -11 -4 -0.30 4.00 -8 -11 4 4.40 3.50 -8 11 4 11.00 5.20 8 11 -4 1.60 4.00 7 -11 -4 61.59 9.20 -7 -11 4 65.49 10.30 -7 -11 4 78.69 8.10 7 -11 -4 65.39 8.70 -7 -11 4 50.69 7.40 -7 11 4 43.00 9.20 7 11 -4 65.69 9.70 6 -11 -4 35.80 6.50 6 -11 -4 25.60 5.80 -6 -11 4 39.70 7.90 -6 -11 4 34.40 6.20 -6 -11 4 34.90 5.40 -6 11 4 30.50 7.40 6 11 -4 39.80 7.40 -5 -11 4 64.19 8.40 -5 -11 4 56.59 6.70 -5 -11 4 68.69 9.90 5 -11 -4 62.19 8.00 5 -11 -4 52.69 7.60 5 -11 -4 58.59 8.50 5 11 -4 71.59 8.90 -5 11 4 65.39 9.30 4 -11 -4 32.20 5.50 -4 -11 4 28.80 5.90 4 -11 -4 30.40 3.00 -4 -11 4 27.10 4.50 4 -11 -4 21.40 5.40 -4 -11 4 32.10 6.50 4 -11 -4 25.40 5.30 -4 11 4 25.10 6.10 4 11 -4 25.30 5.30 -3 -11 4 30.90 6.20 -3 -11 4 33.10 6.20 3 -11 -4 59.29 8.30 3 -11 -4 42.90 6.00 -3 -11 4 46.40 5.70 3 -11 -4 41.00 6.00 -3 11 4 46.80 6.90 3 11 -4 49.50 6.50 -3 11 4 39.50 7.20 3 11 -4 28.90 5.10 -2 -11 4 21.90 5.00 -2 -11 4 20.20 4.60 2 -11 -4 16.00 4.00 2 -11 -4 24.20 5.40 -2 -11 4 17.60 3.70 -2 11 4 13.40 4.00 -2 11 4 22.70 6.00 2 11 -4 20.30 2.00 2 11 -4 20.20 3.90 2 11 -4 28.20 4.60 -1 -11 4 12.30 3.70 -1 -11 4 18.70 3.00 -1 -11 4 21.30 4.90 -1 -11 4 22.40 4.20 1 -11 -4 20.00 4.30 -1 11 4 13.60 4.00 1 11 -4 21.60 4.40 1 11 -4 15.60 3.30 -1 11 4 18.10 5.80 0 -11 -4 115.49 8.60 0 -11 4 132.59 8.30 0 -11 -4 156.78 10.10 0 -11 4 130.79 9.00 0 -11 4 139.89 9.50 0 -11 4 131.09 12.30 0 11 -4 144.89 8.30 0 11 4 145.09 14.00 0 11 4 146.29 9.10 0 11 -4 144.29 9.60 0 11 4 145.29 9.70 1 -11 4 467.55 21.90 -1 -11 -4 434.46 21.90 1 -11 4 467.35 22.20 1 -11 4 464.15 25.10 -1 -11 -4 451.85 23.40 1 -11 4 448.76 23.20 1 11 4 464.35 25.70 -1 11 -4 484.65 23.60 1 11 4 456.65 22.80 1 11 4 495.85 22.60 -1 11 -4 479.85 20.80 2 -11 4 8.80 2.20 2 -11 4 10.40 4.50 -2 -11 -4 8.00 2.50 2 -11 4 8.00 3.40 -2 -11 -4 12.70 4.00 2 -11 4 11.80 3.30 -2 11 -4 11.40 4.00 2 11 4 16.10 4.00 -2 11 -4 7.70 1.50 2 11 4 7.20 2.60 3 -11 4 1.30 3.20 -3 -11 -4 3.30 2.90 3 -11 4 2.70 2.70 3 -11 4 3.60 1.30 -3 -11 -4 4.00 2.10 3 11 4 -1.50 2.50 -3 11 -4 4.10 3.40 3 11 4 1.50 2.10 -4 -11 -4 216.58 14.70 4 -11 4 243.68 15.60 -4 -11 -4 254.47 12.70 4 -11 4 219.58 14.30 4 11 4 239.38 15.00 -4 11 -4 222.08 15.00 4 11 4 227.78 12.50 -5 -11 -4 63.29 8.50 -5 -11 -4 50.59 5.70 5 -11 4 61.59 8.30 5 -11 4 52.09 7.90 -5 11 -4 57.59 8.30 5 11 4 43.00 7.40 6 -11 4 41.40 7.40 -6 -11 -4 38.50 7.20 -6 -11 -4 49.80 5.60 6 -11 4 41.70 7.40 -6 -11 -4 36.30 6.50 6 11 4 45.20 8.10 -6 11 -4 42.60 7.90 7 -11 4 11.20 5.10 -7 -11 -4 16.90 5.60 -7 -11 -4 16.80 4.80 7 -11 4 11.70 5.90 -7 -11 -4 18.70 4.00 7 11 4 20.30 6.20 -7 11 -4 17.40 6.00 8 -11 4 41.60 7.70 -8 -11 -4 44.10 8.30 -8 -11 -4 33.80 6.40 -8 -11 -4 36.90 5.70 -8 11 -4 28.30 7.30 8 11 4 40.10 8.40 -9 -11 -4 52.69 7.60 9 -11 4 52.39 9.70 -9 -11 -4 59.19 7.30 -9 -11 -4 31.20 8.00 9 11 4 47.00 9.60 -9 11 -4 53.99 10.00 10 -11 4 25.70 7.70 -10 -11 -4 26.50 5.50 -10 -11 -4 25.50 7.30 10 11 4 25.30 7.90 -10 11 -4 1.50 5.30 -11 -11 -4 0.80 5.00 11 -11 4 6.40 6.20 11 11 4 9.90 6.30 -11 11 -4 -0.50 5.40 -12 -11 -4 -1.30 5.30 12 -11 4 -5.10 4.70 -12 11 -4 -3.00 5.40 12 11 4 -1.50 5.70 -13 -12 4 181.98 21.70 13 -12 -4 137.39 18.50 13 12 -4 165.48 20.40 -13 12 4 156.58 20.70 -12 -12 4 195.88 21.70 12 -12 -4 173.88 20.00 12 12 -4 172.58 19.60 -12 12 4 121.49 18.30 -11 -12 4 21.30 8.50 11 -12 -4 23.80 8.30 11 12 -4 20.90 7.70 -11 12 4 19.80 8.50 10 -12 -4 1.40 4.80 -10 -12 4 -2.60 4.70 -10 -12 4 -1.60 3.00 -10 -12 4 0.50 3.30 10 12 -4 3.30 4.90 -10 12 4 4.40 5.60 9 -12 -4 0.20 4.40 -9 -12 4 4.90 5.40 -9 -12 4 4.10 3.80 -9 -12 4 4.40 3.90 9 12 -4 -4.30 3.80 -9 12 4 -1.30 4.80 8 -12 -4 -4.00 3.20 -8 -12 4 3.80 3.60 -8 -12 4 5.80 5.50 -8 -12 4 -0.40 2.50 8 12 -4 -6.40 3.10 -8 12 4 2.60 4.30 -7 -12 4 28.70 8.00 -7 -12 4 32.20 6.30 -7 -12 4 34.40 5.80 7 -12 -4 34.90 7.50 7 -12 -4 36.10 7.20 -7 12 4 33.20 7.70 7 12 -4 31.30 7.20 -6 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4 12 4 63.09 6.40 -5 -12 -4 54.09 8.10 -5 -12 -4 26.80 6.40 5 -12 4 33.30 6.50 5 -12 4 38.50 7.30 -5 -12 -4 46.00 5.30 5 12 4 51.19 8.30 -5 12 -4 45.30 7.90 -6 -12 -4 84.79 10.50 6 -12 4 67.49 9.70 -6 -12 -4 92.39 10.60 -6 -12 -4 87.09 6.80 6 -12 4 101.19 11.30 6 12 4 74.89 10.40 -6 12 -4 93.09 11.10 -7 -12 -4 7.80 4.40 7 -12 4 -0.70 3.70 -7 -12 -4 7.70 4.10 -7 -12 -4 4.60 2.70 7 12 4 1.30 4.00 -7 12 -4 1.10 4.10 -8 -12 -4 11.00 5.00 8 -12 4 2.00 4.00 -8 -12 -4 -0.30 2.50 -8 -12 -4 0.60 3.40 -8 12 -4 -0.70 4.10 8 12 4 7.50 5.30 9 -12 4 11.60 6.00 -9 -12 -4 -2.00 3.70 -9 -12 -4 14.30 4.70 9 12 4 7.40 5.90 -9 12 -4 10.80 5.70 10 -12 4 20.60 7.50 -10 -12 -4 6.60 4.10 -10 -12 -4 10.60 5.70 -10 12 -4 2.60 5.00 10 12 4 27.70 8.30 -11 -12 -4 22.30 8.10 11 -12 4 14.90 7.00 -11 12 -4 22.90 7.80 11 12 4 31.30 9.20 -12 -12 -4 0.20 5.40 12 -12 4 -2.60 5.80 12 12 4 10.80 7.10 -12 12 -4 -6.70 4.70 -12 -13 4 3.40 6.40 12 -13 -4 3.60 6.10 -12 13 4 -5.60 5.60 12 13 -4 0.00 5.80 -11 -13 4 100.39 15.40 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21.20 5.30 4 13 -4 8.00 3.70 3 -13 -4 34.30 6.10 3 -13 -4 39.60 7.70 3 -13 -4 30.90 5.80 -3 -13 4 44.80 6.20 -3 -13 4 37.20 7.30 -3 -13 4 41.10 7.20 3 13 -4 44.50 6.40 3 13 -4 39.80 6.30 -3 13 4 32.20 6.70 -2 -13 4 0.90 2.60 -2 -13 4 -6.10 2.20 -2 -13 4 3.70 3.60 2 -13 -4 -0.30 3.40 2 -13 -4 -1.10 2.50 2 13 -4 2.30 2.70 -2 13 4 2.40 2.60 2 13 -4 -2.10 2.30 -2 13 4 0.80 1.90 -1 -13 4 93.09 10.90 1 -13 -4 82.59 10.80 -1 -13 4 79.99 6.20 -1 -13 4 97.79 9.40 1 -13 -4 74.09 8.70 -1 -13 4 84.29 8.80 1 13 -4 94.39 8.30 -1 13 4 83.19 7.90 1 13 -4 71.09 8.30 -1 13 4 85.49 9.40 0 -13 4 392.26 23.80 0 -13 -4 401.56 22.00 0 -13 4 402.96 20.30 0 -13 4 427.96 21.40 0 -13 -4 403.56 24.10 0 -13 -4 391.66 20.80 0 -13 4 403.06 21.70 0 13 -4 412.26 20.00 0 13 4 438.86 21.90 0 13 -4 443.76 22.10 0 13 4 451.15 21.50 -1 -13 -4 68.59 7.10 1 -13 4 70.79 6.90 -1 -13 -4 74.69 10.00 1 -13 4 95.09 8.20 -1 -13 -4 71.09 8.50 1 -13 4 73.09 10.20 1 -13 4 61.29 7.90 -1 13 -4 65.49 8.30 -1 13 -4 67.29 5.30 1 13 4 75.79 8.30 1 13 4 75.09 7.90 2 -13 4 41.40 6.80 2 -13 4 42.00 7.90 2 -13 4 48.50 5.00 2 -13 4 42.80 6.00 -2 -13 -4 37.30 7.60 -2 -13 -4 56.49 6.20 -2 -13 -4 32.80 6.10 -2 13 -4 47.00 7.10 2 13 4 54.19 7.30 2 13 4 45.30 5.80 -2 13 -4 50.89 4.20 3 -13 4 68.29 8.90 3 -13 4 45.40 3.50 -3 -13 -4 58.69 6.20 3 -13 4 32.90 7.40 -3 -13 -4 46.50 7.70 3 -13 4 54.79 7.30 -3 -13 -4 45.30 6.90 -3 13 -4 43.00 7.20 3 13 4 50.39 7.60 3 13 4 53.39 6.10 -4 -13 -4 1.30 3.50 4 -13 4 2.00 3.00 4 -13 4 -8.50 2.20 -4 -13 -4 4.00 3.40 -4 -13 -4 3.80 2.40 4 13 4 1.90 3.80 4 13 4 -0.40 2.10 -4 13 -4 -2.00 3.20 -5 -13 -4 20.50 5.70 5 -13 4 30.20 6.90 5 -13 4 23.20 5.70 -5 -13 -4 34.70 4.70 -5 -13 -4 22.30 5.90 5 13 4 29.20 6.70 -5 13 -4 31.90 6.70 6 -13 4 -2.50 3.50 -6 -13 -4 5.40 4.10 -6 -13 -4 -1.10 2.00 -6 -13 -4 4.60 4.10 6 -13 4 6.10 4.50 -6 13 -4 3.20 4.40 6 13 4 6.10 4.60 -7 -13 -4 5.50 2.90 -7 -13 -4 6.50 4.70 7 -13 4 5.70 4.30 -7 -13 -4 3.30 4.00 7 13 4 8.30 5.30 -7 13 -4 7.70 5.20 8 -13 4 78.49 11.40 -8 -13 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6.20 -7 -14 4 10.60 4.20 -7 -14 4 19.80 7.20 7 -14 -4 15.30 6.00 -7 14 4 3.40 4.80 7 14 -4 8.30 5.20 6 -14 -4 83.59 11.00 -6 -14 4 76.09 8.90 6 -14 -4 111.49 12.80 6 -14 -4 72.09 10.70 -6 -14 4 71.59 10.30 -6 -14 4 113.99 13.60 -6 14 4 77.49 11.80 6 14 -4 88.39 11.20 5 -14 -4 58.29 9.00 5 -14 -4 56.29 8.40 -5 -14 4 53.99 8.70 -5 -14 4 61.39 7.70 -5 -14 4 52.09 9.30 5 -14 -4 66.89 9.70 -5 14 4 47.40 9.10 5 14 -4 66.89 9.30 -4 -14 4 10.50 3.70 4 -14 -4 5.00 3.80 4 -14 -4 6.30 3.90 -4 -14 4 14.80 5.10 -4 -14 4 6.00 4.30 4 -14 -4 1.70 4.00 4 14 -4 6.20 4.10 -4 14 4 5.80 4.70 4 14 -4 -1.00 1.90 3 -14 -4 92.39 10.40 -3 -14 4 87.89 9.20 -3 -14 4 76.39 10.00 -3 -14 4 76.69 10.60 3 -14 -4 88.39 11.50 3 -14 -4 112.19 10.70 -3 14 4 101.09 11.40 3 14 -4 94.79 10.00 3 14 -4 88.29 9.60 -2 -14 4 3.50 2.80 -2 -14 4 -0.80 2.50 2 -14 -4 1.20 3.10 -2 -14 4 1.10 3.10 2 -14 -4 -3.00 3.60 -2 14 4 -0.50 3.60 2 14 -4 -5.10 2.10 -2 14 4 -1.00 2.30 2 14 -4 -1.10 2.80 1 -14 -4 9.00 4.80 -1 -14 4 10.40 4.50 -1 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5 -5 14 37.90 6.20 5 -5 14 47.10 5.10 5 -5 14 33.30 7.10 -5 -5 -14 39.80 7.30 5 5 14 47.90 8.50 5 5 14 38.10 6.70 -5 5 -14 44.80 8.40 -5 5 -14 54.59 5.80 -6 -5 -14 100.59 13.40 -6 -5 -14 77.49 10.40 6 -5 14 85.99 10.80 -6 5 -14 87.69 6.80 -6 5 -14 88.09 11.90 6 5 14 93.39 10.40 -7 -5 -14 1.10 4.00 -7 -5 -14 1.80 4.70 7 5 14 2.30 4.00 -7 5 -14 -2.60 4.10 -8 -5 -14 11.60 6.90 -8 -5 -14 13.90 5.80 8 5 14 3.30 4.40 -8 5 -14 5.00 5.40 -9 -5 -14 12.50 7.00 -9 -5 -14 31.80 8.50 -9 5 -14 14.30 7.30 9 5 14 16.60 6.50 -10 -5 -14 2.70 5.60 -10 -5 -14 -1.90 6.00 -10 5 -14 1.00 5.40 10 5 14 5.50 5.40 -11 -5 -14 3.60 5.80 -11 -5 -14 3.90 6.70 -11 5 -14 -7.80 4.70 11 5 14 -1.50 4.80 -12 -6 14 34.30 8.80 12 -6 -14 33.60 8.30 -12 6 14 31.20 8.00 -12 6 14 31.90 10.10 -11 -6 14 35.60 7.50 -11 -6 14 37.40 9.60 11 -6 -14 42.90 8.80 -11 6 14 29.00 10.00 -11 6 14 31.20 8.20 10 -6 -14 2.60 4.80 -10 -6 14 2.70 4.00 -10 -6 14 10.30 5.80 -10 6 14 10.60 4.50 -10 6 14 -4.70 3.90 -10 6 14 -1.10 5.10 -9 -6 14 2.60 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97.39 12.90 -9 -7 14 63.49 9.90 -9 -7 14 75.79 11.80 9 -7 -14 90.99 11.40 -9 7 14 74.09 9.00 -9 7 14 78.29 11.50 -9 7 14 74.99 12.90 8 -7 -14 39.60 7.50 -8 -7 14 53.79 8.70 -8 -7 14 54.39 9.80 -8 7 14 55.29 11.00 -8 7 14 52.29 9.30 -8 7 14 51.29 7.50 7 -7 -14 19.30 5.10 -7 -7 14 15.70 5.70 -7 -7 14 8.20 5.10 -7 7 14 15.80 6.80 -7 7 14 3.30 5.40 -7 7 14 10.80 4.10 6 -7 -14 14.50 4.50 -6 -7 14 15.80 5.30 -6 -7 14 8.40 4.20 6 -7 -14 14.20 3.40 -6 7 14 16.20 6.20 -6 7 14 18.50 4.50 -6 7 14 11.50 5.60 5 -7 -14 5.80 4.10 -5 -7 14 4.80 4.40 5 -7 -14 8.90 2.90 5 -7 -14 7.80 3.80 -5 -7 14 8.40 4.70 -5 7 14 9.30 5.00 -5 7 14 9.60 3.70 -5 7 14 9.80 5.30 4 -7 -14 97.79 7.20 4 -7 -14 109.79 11.20 -4 -7 14 107.09 11.70 -4 -7 14 95.99 12.00 -4 7 14 82.59 11.10 4 7 -14 93.39 6.20 -4 7 14 105.49 10.10 -4 7 14 119.29 13.40 -3 -7 14 8.10 4.30 -3 -7 14 9.40 5.00 3 -7 -14 6.70 3.80 3 -7 -14 4.80 2.40 3 7 -14 12.40 2.60 -3 7 14 9.40 4.40 -3 7 14 25.20 6.90 -3 7 14 8.60 3.70 2 -7 -14 7.10 3.50 -2 -7 14 6.90 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14 29.90 7.40 -4 7 -14 42.90 5.70 4 7 14 34.60 6.40 -5 -7 -14 25.80 7.00 -5 -7 -14 24.00 6.00 5 -7 14 26.10 6.90 5 -7 14 37.50 6.20 5 -7 14 20.30 4.90 -5 7 -14 35.10 7.70 5 7 14 27.90 7.10 -5 7 -14 40.80 5.60 5 7 14 31.90 6.60 -6 -7 -14 -4.90 3.10 6 -7 14 0.70 3.10 -6 -7 -14 -1.70 4.50 -6 7 -14 -2.50 2.30 -6 7 -14 -0.40 4.30 6 7 14 -1.30 3.40 7 -7 14 1.80 3.50 -7 -7 -14 5.40 5.80 -7 -7 -14 -7.10 3.60 7 7 14 -4.00 3.10 -7 7 -14 -6.70 3.60 -7 7 -14 2.40 2.90 -8 -7 -14 32.10 7.80 8 -7 14 41.40 8.10 -8 -7 -14 22.70 8.20 -8 7 -14 22.00 8.10 -9 -7 -14 67.89 12.70 -9 -7 -14 91.49 12.30 9 7 14 48.80 9.90 -9 7 -14 69.59 12.60 -10 -7 -14 76.09 14.10 -10 -7 -14 83.29 12.30 -10 7 -14 49.10 11.90 10 7 14 49.10 10.10 -11 -7 -14 -2.30 4.90 -11 -7 -14 1.70 6.70 11 7 14 8.40 6.30 -11 7 -14 -1.50 6.40 12 -8 -14 60.79 11.30 -12 -8 14 53.39 11.10 -12 8 14 45.90 12.40 -12 8 14 33.40 8.70 -11 -8 14 0.70 5.40 -11 -8 14 -1.00 4.00 11 -8 -14 -7.60 4.20 -11 8 14 -0.70 5.50 -11 8 14 5.40 4.90 -10 -8 14 30.10 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49.80 10.70 -4 -4 26 7.40 5.60 4 -4 -26 8.00 5.90 -4 -4 26 -0.50 7.10 -4 4 26 13.50 8.90 -4 4 26 5.00 6.20 3 -4 -26 6.20 5.40 -3 -4 26 3.90 7.10 -3 -4 26 -1.40 4.90 -3 4 26 -5.10 5.20 -3 4 26 2.20 6.60 -2 -4 26 -7.60 5.70 2 -4 -26 -2.90 4.50 -2 -4 26 -3.80 4.70 -2 4 26 6.50 5.80 -2 4 26 4.10 7.10 -1 -4 26 45.40 10.40 1 -4 -26 60.39 10.50 -1 -4 26 62.89 14.40 -1 4 26 24.30 9.80 -1 4 26 30.10 8.90 1 4 -26 43.40 8.40 0 -4 26 67.09 12.00 0 -4 26 91.59 16.00 0 -4 -26 41.20 9.20 0 4 26 62.59 13.70 0 4 26 58.29 11.60 0 4 -26 59.49 9.50 1 -4 26 122.59 18.70 1 -4 26 96.29 14.20 -1 -4 -26 98.49 13.80 -1 4 -26 121.39 13.60 1 4 26 129.39 18.60 1 4 26 105.79 14.80 2 -4 26 4.90 5.90 2 -4 26 4.80 8.60 -2 -4 -26 2.40 5.30 2 4 26 4.70 5.40 -2 4 -26 1.20 5.50 2 4 26 5.10 7.90 3 -4 26 4.60 6.20 -3 -4 -26 9.40 6.40 3 4 26 2.80 5.50 -3 4 -26 -5.10 5.00 -5 -5 26 4.50 6.20 -5 -5 26 17.10 9.30 5 -5 -26 11.80 6.50 -5 5 26 2.10 6.40 -5 5 26 3.00 6.90 -4 -5 26 8.80 8.20 -4 -5 26 -2.30 5.20 4 -5 -26 3.60 5.40 -4 5 26 12.20 8.50 -4 5 26 -3.00 5.60 -3 -5 26 39.90 9.80 -3 -5 26 61.19 14.00 3 -5 -26 46.10 9.60 -3 5 26 27.00 10.50 -3 5 26 29.20 8.80 -2 -5 26 42.60 10.10 -2 -5 26 46.30 12.40 2 -5 -26 31.00 9.00 -2 5 26 40.20 10.00 1 -5 -26 42.30 9.80 -1 -5 26 54.89 13.10 -1 -5 26 48.50 10.30 -1 5 26 73.69 12.60 -1 5 26 32.60 11.10 0 -5 26 -3.40 4.70 0 -5 26 0.30 7.00 0 -5 -26 9.00 6.40 0 5 -26 4.40 4.90 0 5 26 6.50 7.40 0 5 26 -3.60 5.20 1 -5 26 -2.10 6.70 1 -5 26 -3.10 5.10 -1 -5 -26 6.90 6.20 1 5 26 0.40 7.30 1 5 26 0.50 6.00 -1 5 -26 -4.50 4.80 2 -5 26 27.70 8.60 -2 -5 -26 35.60 8.80 2 -5 26 46.40 12.90 -2 5 -26 22.30 7.50 2 5 26 9.20 8.40 2 5 26 29.20 9.20 -4 -6 26 23.70 8.40 -4 -6 26 58.79 13.40 4 -6 -26 50.39 10.10 -4 6 26 51.89 11.10 -4 6 26 39.50 12.00 3 -6 -26 -3.40 4.40 -3 -6 26 2.10 5.50 -3 -6 26 5.20 7.80 -3 6 26 -2.10 4.80 -3 6 26 8.20 7.90 2 -6 -26 0.10 5.70 -2 -6 26 -2.10 5.00 -2 -6 26 10.10 7.80 -2 6 26 5.60 7.40 -2 6 26 -3.00 5.90 -1 -6 26 10.80 7.00 1 -6 -26 12.90 6.70 -1 -6 26 1.10 7.10 -1 6 26 0.10 6.00 -1 6 26 -0.10 6.80 0 -6 -26 -9.10 4.00 0 -6 26 3.80 5.70 0 -6 26 9.60 8.00 0 6 26 -1.00 7.30 0 6 26 1.00 5.30 1 -6 26 9.50 8.40 -1 -6 -26 3.20 5.50 1 -6 26 -8.70 4.20 -1 6 -26 11.60 5.60 1 6 26 12.40 7.30 1 6 26 10.80 9.10 -2 -6 -26 5.70 5.90 2 -6 26 -0.90 6.70 2 -6 26 8.80 6.70 2 6 26 25.20 10.60 2 6 26 0.90 5.00 -2 6 -26 -1.10 5.10 -4 -7 26 13.10 8.40 -4 7 26 2.60 6.60 -3 -7 26 26.20 9.70 3 -7 -26 47.50 10.10 -3 -7 26 41.40 9.90 -3 7 26 27.60 10.80 -3 7 26 41.40 10.50 -2 -7 26 20.20 8.20 -2 -7 26 14.30 9.00 2 -7 -26 17.30 7.20 -2 7 26 24.90 8.50 -2 7 26 17.50 9.60 -1 -7 26 7.20 6.30 -1 -7 26 1.30 7.70 1 -7 -26 3.50 5.70 -1 7 26 0.90 6.10 -1 7 26 -4.50 6.60 0 -7 26 -3.90 4.90 0 -7 -26 4.50 6.10 0 -7 26 17.60 9.10 0 7 26 0.80 5.60 0 7 26 3.70 7.60 1 -7 26 91.79 13.40 -1 -7 -26 96.49 13.70 1 -7 26 65.09 15.30 1 7 26 88.19 16.00 -3 -8 26 43.10 12.10 -3 8 26 12.60 9.50 -2 -8 26 1.70 7.50 2 -8 -26 2.80 5.70 -2 -8 26 -1.00 5.60 -2 8 26 -4.80 7.00 -2 8 26 3.20 5.40 -1 -8 26 -11.60 3.20 -1 -8 26 7.40 8.10 1 -8 -26 1.30 6.20 -1 8 26 -5.10 5.70 -1 8 26 -7.30 6.20 0 -8 26 -1.10 5.20 0 -8 26 -1.40 5.40 0 -8 -26 1.00 5.70 0 8 26 -7.00 6.30 0 8 26 -7.40 4.70 -4 0 27 7.30 8.00 -4 0 27 -1.60 5.50 4 0 -27 2.20 5.00 -3 0 27 -1.40 3.80 3 0 -27 4.40 5.20 -3 0 27 -4.30 6.70 2 0 -27 -5.00 4.70 -2 0 27 -1.10 5.50 -2 0 27 -5.10 6.50 -1 0 27 -3.40 5.10 -1 0 27 1.20 7.40 1 0 -27 1.60 4.90 0 0 -27 -3.40 4.50 0 0 27 -1.90 5.50 0 0 27 6.00 8.10 1 0 27 -3.40 5.30 -1 0 -27 1.50 5.70 1 0 27 -10.00 6.00 -2 0 -27 -6.90 4.40 2 0 27 6.00 8.10 2 0 27 -5.70 4.90 -4 -1 27 44.10 9.60 -4 -1 27 41.20 11.60 4 -1 -27 61.69 10.20 -4 1 27 52.69 11.00 -4 1 27 55.59 13.90 3 -1 -27 39.90 8.70 -3 -1 27 38.60 10.00 -3 -1 27 35.90 12.40 -3 1 27 22.60 8.30 3 1 -27 31.30 7.60 -3 1 27 30.70 11.00 -2 -1 27 -0.90 5.20 2 -1 -27 15.30 6.90 -2 -1 27 2.80 5.60 2 1 -27 0.10 4.70 -2 1 27 12.30 7.10 -2 1 27 1.20 7.10 -1 -1 27 0.30 5.70 1 -1 -27 2.40 5.40 -1 -1 27 7.60 6.40 -1 1 27 6.50 7.90 1 1 -27 13.30 6.60 -1 1 27 5.70 6.10 0 -1 -27 32.30 8.60 0 -1 27 26.70 11.00 0 -1 27 50.09 10.60 0 1 27 34.90 11.80 0 1 -27 46.40 9.10 0 1 27 25.30 8.90 -1 -1 -27 43.30 9.90 1 -1 27 45.40 12.80 1 -1 27 12.10 6.80 1 1 27 32.50 9.70 -1 1 -27 36.50 8.60 1 1 27 12.50 9.00 2 -1 27 40.80 12.20 2 -1 27 43.10 10.50 2 1 27 40.00 11.80 2 1 27 23.10 8.50 -4 -2 27 -5.70 6.10 -4 -2 27 8.10 6.70 4 -2 -27 19.80 6.90 -4 2 27 15.50 9.20 -4 2 27 2.20 4.60 -3 -2 27 15.40 8.80 -3 -2 27 6.00 5.30 3 -2 -27 19.70 6.80 -3 2 27 9.00 8.10 -3 2 27 -1.30 5.80 -2 -2 27 12.40 7.20 -2 -2 27 10.40 8.60 2 -2 -27 18.90 7.40 -2 2 27 17.70 7.00 -2 2 27 20.10 10.30 2 2 -27 17.10 7.10 1 -2 -27 19.20 7.30 -1 -2 27 11.70 7.00 -1 -2 27 21.50 9.90 -1 2 27 18.60 7.40 1 2 -27 36.80 8.20 -1 2 27 29.30 10.70 0 -2 27 0.10 5.40 0 -2 -27 -5.20 4.60 0 -2 27 -4.70 4.50 0 2 27 -2.20 6.40 0 2 -27 -1.90 4.70 0 2 27 7.60 5.30 -1 -2 -27 26.30 7.70 1 -2 27 22.50 10.50 1 -2 27 28.20 8.90 1 2 27 34.80 9.90 -1 2 -27 29.40 8.50 1 2 27 33.40 11.30 2 -2 27 -4.90 6.70 2 2 27 21.40 10.10 -4 -3 27 3.30 7.40 -4 3 27 4.70 7.20 -3 -3 27 6.90 6.60 -3 -3 27 25.20 10.40 3 -3 -27 26.40 7.80 -3 3 27 12.70 7.80 -3 3 27 7.80 8.40 -2 -3 27 -2.40 7.50 -2 -3 27 9.90 6.70 2 -3 -27 -2.60 4.80 -2 3 27 -1.20 5.80 -2 3 27 2.70 7.60 1 -3 -27 -5.00 4.50 -1 -3 27 -1.90 7.80 -1 -3 27 -4.60 4.60 -1 3 27 11.80 7.20 1 3 -27 0.40 4.90 -1 3 27 -4.30 5.90 0 -3 -27 6.70 5.30 0 -3 27 2.20 5.50 0 -3 27 -0.10 7.80 0 3 -27 9.90 5.80 0 3 27 -4.80 5.30 0 3 27 10.00 8.00 -1 -3 -27 -3.90 4.70 1 -3 27 -2.60 7.10 1 -3 27 -0.80 5.60 -1 3 -27 2.20 5.20 1 3 27 -8.50 5.90 1 3 27 1.10 6.10 -3 -4 27 6.90 6.50 3 -4 -27 -4.50 4.90 -3 -4 27 -3.00 7.10 -3 4 27 -0.50 5.90 -3 4 27 5.30 7.80 2 -4 -27 -3.60 4.80 -2 -4 27 -9.60 4.20 -2 -4 27 -8.20 6.20 -2 4 27 4.90 6.10 -2 4 27 4.20 6.90 1 -4 -27 4.60 5.70 -1 -4 27 -1.40 5.20 -1 -4 27 18.20 9.90 -1 4 27 -6.60 4.70 -1 4 27 8.30 7.60 0 -4 27 -9.00 6.70 0 -4 27 -6.00 4.80 0 -4 -27 9.60 6.90 0 4 27 3.60 6.80 0 4 -27 2.10 4.80 0 4 27 2.20 6.10 1 -4 27 4.10 8.50 1 4 27 3.90 7.70 -3 5 27 7.50 7.50 -2 -5 27 8.50 8.90 2 -5 -27 12.40 7.10 -2 -5 27 21.20 8.00 -2 5 27 9.10 7.90 -2 5 27 19.80 8.40 -1 -5 27 -3.10 4.80 -1 -5 27 9.70 9.30 1 -5 -27 -3.80 5.40 -1 5 27 7.70 6.20 -1 5 27 16.20 8.70 0 -5 27 -4.10 5.20 0 -5 27 -7.00 6.70 0 5 27 8.40 7.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 17849 _olex2_submission_special_instructions 'No special instructions were received' ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_RomanTA52b _database_code_depnum_ccdc_archive 'CCDC 2122223' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-15 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common RomanTA52b _chemical_melting_point ? _chemical_formula_moiety 'C34 H45 N2 O3 P [+ solvent]' _chemical_formula_sum 'C34 H45 N2 O3 P [+ solvent]' _chemical_formula_weight 560.69 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system tetragonal _space_group_IT_number 88 _space_group_name_H-M_alt 'I 41/a' _space_group_name_Hall '-I 4ad' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' _cell_length_a 33.201(5) _cell_length_b 33.201(5) _cell_length_c 15.661(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 17263(6) _cell_formula_units_Z 16 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 6418 _cell_measurement_theta_min 1.735 _cell_measurement_theta_max 23.554 _exptl_crystal_description block _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 0.863 _exptl_crystal_F_000 4832 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.210 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.150 _exptl_absorpt_coefficient_mu 0.090 _shelx_estimated_absorpt_T_min 0.981 _shelx_estimated_absorpt_T_max 0.987 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.961 _exptl_absorpt_correction_T_max 0.967 _exptl_absorpt_process_details 'SADABS V2008/1 (Bruker AXS)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'APEX2 (Bruker AXS)' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 95 _diffrn_reflns_number 27868 _diffrn_reflns_av_unetI/netI 0.1218 _diffrn_reflns_av_R_equivalents 0.1105 _diffrn_reflns_limit_h_min -37 _diffrn_reflns_limit_h_max 37 _diffrn_reflns_limit_k_min -37 _diffrn_reflns_limit_k_max 37 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_theta_min 1.735 _diffrn_reflns_theta_max 23.554 _diffrn_reflns_theta_full 23.554 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 6418 _reflns_number_gt 2906 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker Instrument Service v2010.7.0.0' _computing_cell_refinement 'APEX2 v2010.7-0 (Bruker AXS)' _computing_data_reduction 'SAINT V7.68A (Bruker AXS, 2009)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1334P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_extinction_coef 0.00031(9) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_number_reflns 6418 _refine_ls_number_parameters 446 _refine_ls_number_restraints 547 _refine_ls_R_factor_all 0.1679 _refine_ls_R_factor_gt 0.0934 _refine_ls_wR_factor_ref 0.2667 _refine_ls_wR_factor_gt 0.2295 _refine_ls_goodness_of_fit_ref 0.962 _refine_ls_restrained_S_all 0.929 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 # start Validation Reply Form _vrf_THETM01_RomanTA52b ; PROBLEM: The value of sine(theta_max)/wavelength is less than 0.575 RESPONSE: Very sensitive, weak diffracted crystal ; _vrf_PLAT420_RomanTA52b ; PROBLEM: D-H Bond Without Acceptor O3 --H3 . Please Check RESPONSE: Partly disordered hydroxy group in the structure ; # end Validation Reply Form loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 0.43037(4) 0.55967(4) 0.55414(10) 0.0640(5) Uani 1 1 d . U . . . O1 O 0.39143(9) 0.54065(9) 0.6083(2) 0.0671(10) Uani 1 1 d . U . . . O2 O 0.3962(8) 0.5585(4) 0.4726(5) 0.062(3) Uani 0.88(8) 1 d . U P A 1 O2A O 0.411(5) 0.554(2) 0.468(4) 0.062(7) Uani 0.12(8) 1 d . U P A 2 O3 O 0.45958(9) 0.52726(10) 0.5349(2) 0.0773(11) Uani 1 1 d . U . . . H3 H 0.4558 0.5078 0.5683 0.116 Uiso 1 1 calc R U . . . N1 N 0.44726(12) 0.57989(13) 0.6535(3) 0.0691(11) Uani 1 1 d . U . . . N2 N 0.44868(12) 0.60489(12) 0.5114(3) 0.0659(11) Uani 1 1 d . U . . . C1 C 0.47279(15) 0.61235(15) 0.6486(4) 0.0651(14) Uani 1 1 d . U . . . C2 C 0.49515(16) 0.63040(18) 0.7125(4) 0.0839(17) Uani 1 1 d . U . . . H2 H 0.4938 0.6210 0.7697 0.101 Uiso 1 1 calc R U . . . C3 C 0.51975(17) 0.6627(2) 0.6907(5) 0.0953(19) Uani 1 1 d . U . . . H3A H 0.5350 0.6759 0.7337 0.114 Uiso 1 1 calc R U . . . C4 C 0.52226(17) 0.67586(18) 0.6073(5) 0.0882(18) Uani 1 1 d . U . . . H4 H 0.5397 0.6975 0.5933 0.106 Uiso 1 1 calc R U . . . C5 C 0.49934(15) 0.65760(15) 0.5433(4) 0.0741(15) Uani 1 1 d . U . . . H5 H 0.5015 0.6667 0.4860 0.089 Uiso 1 1 calc R U . . . C6 C 0.47411(14) 0.62700(15) 0.5625(4) 0.0609(13) Uani 1 1 d . U . . . C7 C 0.42858(15) 0.56192(15) 0.7232(4) 0.0641(13) Uani 1 1 d . U . . . C8 C 0.39614(14) 0.53932(15) 0.6951(4) 0.0592(13) Uani 1 1 d . U . . . C9 C 0.37005(15) 0.51870(15) 0.7483(4) 0.0655(14) Uani 1 1 d . U . . . C10 C 0.37963(15) 0.52056(17) 0.8351(4) 0.0748(15) Uani 1 1 d . U . . . H10 H 0.3629 0.5068 0.8747 0.090 Uiso 1 1 calc R U . . . C11 C 0.41315(17) 0.54204(17) 0.8662(4) 0.0764(15) Uani 1 1 d . U . . . C12 C 0.43761(15) 0.56324(17) 0.8102(4) 0.0763(16) Uani 1 1 d . U . . . H12 H 0.4600 0.5783 0.8306 0.092 Uiso 1 1 calc R U . . . C13 C 0.33376(16) 0.49581(16) 0.7144(4) 0.0732(15) Uani 1 1 d . U . . . C14 C 0.34768(17) 0.46277(17) 0.6525(4) 0.0930(18) Uani 1 1 d . U . . . H14A H 0.3633 0.4749 0.6061 0.139 Uiso 1 1 calc R U . . . H14B H 0.3241 0.4490 0.6288 0.139 Uiso 1 1 calc R U . . . H14C H 0.3645 0.4433 0.6832 0.139 Uiso 1 1 calc R U . . . C15 C 0.30544(16) 0.52443(18) 0.6672(4) 0.0910(19) Uani 1 1 d . U . . . H15A H 0.2967 0.5459 0.7060 0.136 Uiso 1 1 calc R U . . . H15B H 0.2819 0.5095 0.6468 0.136 Uiso 1 1 calc R U . . . H15C H 0.3196 0.5363 0.6184 0.136 Uiso 1 1 calc R U . . . C16 C 0.30947(16) 0.47541(17) 0.7856(4) 0.0884(18) Uani 1 1 d . U . . . H16A H 0.3256 0.4539 0.8114 0.133 Uiso 1 1 calc R U . . . H16B H 0.2848 0.4639 0.7616 0.133 Uiso 1 1 calc R U . . . H16C H 0.3025 0.4954 0.8293 0.133 Uiso 1 1 calc R U . . . C17 C 0.4223(2) 0.5415(2) 0.9632(4) 0.106(2) Uani 1 1 d . U . . . C18 C 0.3882(5) 0.5551(8) 1.0148(10) 0.155(8) Uani 0.528(12) 1 d . U P B 1 H18A H 0.3633 0.5435 0.9921 0.232 Uiso 0.528(12) 1 calc R U P B 1 H18B H 0.3865 0.5846 1.0126 0.232 Uiso 0.528(12) 1 calc R U P B 1 H18C H 0.3919 0.5464 1.0740 0.232 Uiso 0.528(12) 1 calc R U P B 1 C18A C 0.4095(6) 0.5892(6) 0.9911(12) 0.142(7) Uani 0.472(12) 1 d . U P B 2 H18D H 0.4258 0.6084 0.9585 0.213 Uiso 0.472(12) 1 calc R U P B 2 H18E H 0.4144 0.5931 1.0523 0.213 Uiso 0.472(12) 1 calc R U P B 2 H18F H 0.3809 0.5937 0.9788 0.213 Uiso 0.472(12) 1 calc R U P B 2 C19 C 0.4613(5) 0.5636(5) 0.9810(13) 0.118(6) Uani 0.528(12) 1 d . U P B 1 H19A H 0.4831 0.5513 0.9479 0.177 Uiso 0.528(12) 1 calc R U P B 1 H19B H 0.4676 0.5618 1.0420 0.177 Uiso 0.528(12) 1 calc R U P B 1 H19C H 0.4584 0.5919 0.9647 0.177 Uiso 0.528(12) 1 calc R U P B 1 C19A C 0.4647(7) 0.5323(9) 0.9815(17) 0.169(10) Uani 0.472(12) 1 d . U P B 2 H19D H 0.4819 0.5459 0.9398 0.253 Uiso 0.472(12) 1 calc R U P B 2 H19E H 0.4689 0.5031 0.9777 0.253 Uiso 0.472(12) 1 calc R U P B 2 H19F H 0.4714 0.5416 1.0391 0.253 Uiso 0.472(12) 1 calc R U P B 2 C20 C 0.4342(5) 0.4926(4) 0.9841(9) 0.119(5) Uani 0.528(12) 1 d . U P B 1 H20A H 0.4121 0.4752 0.9656 0.178 Uiso 0.528(12) 1 calc R U P B 1 H20B H 0.4386 0.4892 1.0456 0.178 Uiso 0.528(12) 1 calc R U P B 1 H20C H 0.4588 0.4854 0.9532 0.178 Uiso 0.528(12) 1 calc R U P B 1 C20A C 0.3954(6) 0.5162(7) 1.0163(11) 0.131(8) Uani 0.472(12) 1 d . U P B 2 H20D H 0.3673 0.5213 1.0003 0.197 Uiso 0.472(12) 1 calc R U P B 2 H20E H 0.3993 0.5228 1.0767 0.197 Uiso 0.472(12) 1 calc R U P B 2 H20F H 0.4017 0.4877 1.0069 0.197 Uiso 0.472(12) 1 calc R U P B 2 C21 C 0.43200(15) 0.61471(15) 0.4326(3) 0.0589(13) Uani 1 1 d . U . . . C22 C 0.43946(16) 0.64696(15) 0.3769(4) 0.0714(15) Uani 1 1 d . U . . . H22 H 0.4599 0.6661 0.3896 0.086 Uiso 1 1 calc R U . . . C23 C 0.41644(18) 0.65063(16) 0.3023(4) 0.0717(15) Uani 1 1 d . U . . . C24 C 0.38817(16) 0.62176(15) 0.2853(3) 0.0702(15) Uani 1 1 d . U . . . H24 H 0.3735 0.6242 0.2334 0.084 Uiso 1 1 calc R U . . . C25 C 0.37900(15) 0.58910(15) 0.3375(4) 0.0639(13) Uani 1 1 d . U . . . C26 C 0.40271(15) 0.58699(15) 0.4121(3) 0.0597(13) Uani 1 1 d . U . . . C27 C 0.4236(2) 0.68746(19) 0.2449(4) 0.100(2) Uani 1 1 d . U . . . C28 C 0.4241(9) 0.7258(5) 0.2950(12) 0.136(8) Uani 0.472(15) 1 d . U P C 1 H28A H 0.4176 0.7484 0.2573 0.204 Uiso 0.472(15) 1 calc R U P C 1 H28B H 0.4509 0.7298 0.3198 0.204 Uiso 0.472(15) 1 calc R U P C 1 H28C H 0.4041 0.7243 0.3409 0.204 Uiso 0.472(15) 1 calc R U P C 1 C28A C 0.3891(7) 0.7156(6) 0.2519(16) 0.166(9) Uani 0.528(15) 1 d . U P C 2 H28D H 0.3639 0.7008 0.2434 0.250 Uiso 0.528(15) 1 calc R U P C 2 H28E H 0.3916 0.7366 0.2082 0.250 Uiso 0.528(15) 1 calc R U P C 2 H28F H 0.3891 0.7280 0.3087 0.250 Uiso 0.528(15) 1 calc R U P C 2 C29 C 0.3907(6) 0.6909(6) 0.1780(12) 0.131(8) Uani 0.472(15) 1 d . U P C 1 H29A H 0.3837 0.6640 0.1569 0.196 Uiso 0.472(15) 1 calc R U P C 1 H29B H 0.4002 0.7075 0.1304 0.196 Uiso 0.472(15) 1 calc R U P C 1 H29C H 0.3668 0.7034 0.2034 0.196 Uiso 0.472(15) 1 calc R U P C 1 C29A C 0.4320(6) 0.6705(5) 0.1513(9) 0.138(7) Uani 0.528(15) 1 d . U P C 2 H29D H 0.4064 0.6643 0.1234 0.207 Uiso 0.528(15) 1 calc R U P C 2 H29E H 0.4484 0.6460 0.1552 0.207 Uiso 0.528(15) 1 calc R U P C 2 H29F H 0.4465 0.6909 0.1179 0.207 Uiso 0.528(15) 1 calc R U P C 2 C30 C 0.4654(6) 0.6860(5) 0.2070(15) 0.127(8) Uani 0.472(15) 1 d . U P C 1 H30A H 0.4677 0.7062 0.1618 0.191 Uiso 0.472(15) 1 calc R U P C 1 H30B H 0.4703 0.6591 0.1830 0.191 Uiso 0.472(15) 1 calc R U P C 1 H30C H 0.4853 0.6915 0.2516 0.191 Uiso 0.472(15) 1 calc R U P C 1 C30A C 0.4653(7) 0.7091(7) 0.2699(13) 0.173(9) Uani 0.528(15) 1 d . U P C 2 H30D H 0.4875 0.6898 0.2642 0.259 Uiso 0.528(15) 1 calc R U P C 2 H30E H 0.4639 0.7186 0.3291 0.259 Uiso 0.528(15) 1 calc R U P C 2 H30F H 0.4699 0.7320 0.2318 0.259 Uiso 0.528(15) 1 calc R U P C 2 C31 C 0.34661(16) 0.55799(16) 0.3177(3) 0.0688(14) Uani 1 1 d . U . . . C32 C 0.36579(18) 0.51646(16) 0.3145(4) 0.0940(19) Uani 1 1 d . U . . . H32A H 0.3878 0.5165 0.2729 0.141 Uiso 1 1 calc R U . . . H32B H 0.3455 0.4966 0.2974 0.141 Uiso 1 1 calc R U . . . H32C H 0.3763 0.5095 0.3710 0.141 Uiso 1 1 calc R U . . . C33 C 0.32540(19) 0.56669(19) 0.2318(4) 0.104(2) Uani 1 1 d . U . . . H33A H 0.3448 0.5639 0.1850 0.156 Uiso 1 1 calc R U . . . H33B H 0.3147 0.5942 0.2322 0.156 Uiso 1 1 calc R U . . . H33C H 0.3033 0.5475 0.2236 0.156 Uiso 1 1 calc R U . . . C34 C 0.31436(16) 0.55929(18) 0.3876(4) 0.0899(18) Uani 1 1 d . U . . . H34A H 0.3268 0.5538 0.4431 0.135 Uiso 1 1 calc R U . . . H34B H 0.2938 0.5389 0.3758 0.135 Uiso 1 1 calc R U . . . H34C H 0.3019 0.5860 0.3887 0.135 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.0674(9) 0.0688(9) 0.0559(11) 0.0036(8) -0.0020(8) -0.0011(7) O1 0.070(2) 0.079(2) 0.052(2) 0.0138(19) -0.0116(18) -0.0171(17) O2 0.065(7) 0.080(3) 0.042(3) 0.012(2) -0.003(3) -0.010(4) O2A 0.068(16) 0.071(13) 0.048(8) 0.006(10) -0.003(9) -0.008(12) O3 0.072(2) 0.074(2) 0.086(3) 0.000(2) -0.004(2) 0.0112(19) N1 0.072(3) 0.084(3) 0.052(3) 0.002(2) 0.001(2) -0.013(2) N2 0.068(3) 0.073(3) 0.057(3) -0.002(2) -0.001(2) -0.011(2) C1 0.058(3) 0.069(3) 0.068(4) -0.007(3) -0.002(3) 0.005(3) C2 0.073(4) 0.105(4) 0.074(4) -0.014(3) -0.007(3) -0.013(3) C3 0.068(4) 0.122(5) 0.096(5) -0.026(4) 0.001(4) -0.022(3) C4 0.074(4) 0.092(4) 0.099(5) -0.011(4) 0.002(4) -0.021(3) C5 0.066(3) 0.074(4) 0.082(4) -0.008(3) 0.007(3) -0.010(3) C6 0.055(3) 0.062(3) 0.066(4) -0.007(3) 0.001(3) 0.001(2) C7 0.067(3) 0.076(3) 0.050(3) 0.001(3) -0.002(3) -0.003(3) C8 0.054(3) 0.071(3) 0.053(3) 0.005(3) -0.003(3) 0.002(2) C9 0.064(3) 0.073(3) 0.059(4) 0.015(3) 0.000(3) -0.003(3) C10 0.067(3) 0.103(4) 0.054(4) 0.015(3) -0.002(3) -0.004(3) C11 0.078(4) 0.101(4) 0.050(3) 0.003(3) -0.009(3) -0.002(3) C12 0.063(3) 0.114(4) 0.052(4) 0.008(3) -0.011(3) -0.012(3) C13 0.073(3) 0.085(4) 0.062(4) 0.018(3) -0.004(3) -0.019(3) C14 0.101(4) 0.102(4) 0.077(5) -0.005(3) 0.001(3) -0.021(3) C15 0.073(4) 0.122(5) 0.078(5) 0.023(4) -0.018(3) -0.007(3) C16 0.088(4) 0.110(4) 0.067(4) 0.027(3) -0.003(3) -0.026(3) C17 0.096(4) 0.171(6) 0.050(4) 0.012(4) -0.010(3) -0.002(4) C18 0.134(10) 0.28(2) 0.048(9) -0.045(17) -0.018(8) 0.034(14) C18A 0.145(15) 0.177(11) 0.105(15) -0.057(11) 0.009(12) -0.037(10) C19 0.136(10) 0.160(12) 0.058(10) -0.001(12) -0.039(8) -0.013(10) C19A 0.121(9) 0.30(3) 0.087(15) 0.05(2) -0.040(10) 0.024(15) C20 0.113(12) 0.174(9) 0.069(10) 0.050(9) -0.023(8) -0.014(8) C20A 0.160(16) 0.188(15) 0.046(9) 0.011(13) -0.017(10) -0.049(15) C21 0.070(3) 0.061(3) 0.046(3) -0.008(2) 0.011(3) -0.002(3) C22 0.084(4) 0.068(3) 0.062(4) 0.000(3) 0.020(3) -0.011(3) C23 0.095(4) 0.071(3) 0.049(4) 0.006(3) 0.024(3) 0.002(3) C24 0.092(4) 0.074(3) 0.045(4) 0.005(3) 0.006(3) 0.005(3) C25 0.078(3) 0.068(3) 0.046(4) 0.002(3) 0.004(3) 0.012(3) C26 0.074(3) 0.064(3) 0.041(3) 0.002(3) 0.014(3) -0.003(3) C27 0.141(5) 0.088(4) 0.070(5) 0.023(3) 0.026(4) -0.014(4) C28 0.26(3) 0.083(7) 0.070(12) 0.023(7) 0.023(13) -0.006(13) C28A 0.230(15) 0.122(16) 0.15(2) 0.080(14) 0.069(16) 0.051(12) C29 0.179(14) 0.119(14) 0.093(15) 0.058(11) -0.006(11) -0.018(12) C29A 0.22(2) 0.131(12) 0.065(8) 0.026(7) 0.036(10) -0.025(11) C30 0.152(11) 0.100(13) 0.13(2) 0.035(11) 0.055(11) -0.028(10) C30A 0.218(14) 0.19(2) 0.113(16) 0.034(13) 0.026(14) -0.110(14) C31 0.081(4) 0.089(4) 0.036(3) 0.007(3) -0.002(3) 0.004(3) C32 0.118(5) 0.081(4) 0.083(5) -0.011(3) -0.024(4) 0.003(3) C33 0.130(5) 0.120(5) 0.062(4) 0.003(4) -0.036(4) -0.004(4) C34 0.087(4) 0.112(5) 0.071(4) 0.006(4) -0.001(3) -0.009(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 O3 1.479(3) . ? P1 O2A 1.51(8) . ? P1 O1 1.671(3) . ? P1 O2 1.710(15) . ? P1 N2 1.753(4) . ? P1 N1 1.785(5) . ? O1 C8 1.368(6) . ? O2 C26 1.355(8) . ? O2A C26 1.42(8) . ? O3 H3 0.8400 . ? N1 C1 1.373(6) . ? N1 C7 1.389(6) . ? N2 C6 1.376(6) . ? N2 C21 1.391(6) . ? C1 C2 1.383(7) . ? C1 C6 1.433(7) . ? C2 C3 1.392(8) . ? C2 H2 0.9500 . ? C3 C4 1.378(8) . ? C3 H3A 0.9500 . ? C4 C5 1.398(8) . ? C4 H4 0.9500 . ? C5 C6 1.351(6) . ? C5 H5 0.9500 . ? C7 C8 1.384(6) . ? C7 C12 1.396(7) . ? C8 C9 1.384(7) . ? C9 C10 1.397(7) . ? C9 C13 1.520(7) . ? C10 C11 1.409(7) . ? C10 H10 0.9500 . ? C11 C12 1.387(7) . ? C11 C17 1.550(8) . ? C12 H12 0.9500 . ? C13 C15 1.528(7) . ? C13 C14 1.535(7) . ? C13 C16 1.534(7) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 C18 1.463(16) . ? C17 C19A 1.47(2) . ? C17 C20A 1.482(17) . ? C17 C19 1.513(17) . ? C17 C18A 1.698(18) . ? C17 C20 1.701(15) . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C18A H18D 0.9800 . ? C18A H18E 0.9800 . ? C18A H18F 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C19A H19D 0.9800 . ? C19A H19E 0.9800 . ? C19A H19F 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C20A H20D 0.9800 . ? C20A H20E 0.9800 . ? C20A H20F 0.9800 . ? C21 C26 1.377(6) . ? C21 C22 1.404(7) . ? C22 C23 1.402(7) . ? C22 H22 0.9500 . ? C23 C24 1.368(7) . ? C23 C27 1.536(8) . ? C24 C25 1.392(7) . ? C24 H24 0.9500 . ? C25 C26 1.410(7) . ? C25 C31 1.523(7) . ? C27 C28A 1.482(18) . ? C27 C28 1.495(17) . ? C27 C30 1.510(17) . ? C27 C29 1.521(17) . ? C27 C29A 1.595(16) . ? C27 C30A 1.607(18) . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C28A H28D 0.9800 . ? C28A H28E 0.9800 . ? C28A H28F 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C29A H29D 0.9800 . ? C29A H29E 0.9800 . ? C29A H29F 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C30A H30D 0.9800 . ? C30A H30E 0.9800 . ? C30A H30F 0.9800 . ? C31 C32 1.520(7) . ? C31 C34 1.532(7) . ? C31 C33 1.547(7) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 P1 O2A 91(5) . . ? O3 P1 O1 109.62(19) . . ? O2A P1 O1 94(5) . . ? O3 P1 O2 105.5(8) . . ? O1 P1 O2 81.8(6) . . ? O3 P1 N2 108.5(2) . . ? O2A P1 N2 85(3) . . ? O1 P1 N2 141.8(2) . . ? O2 P1 N2 87.9(3) . . ? O3 P1 N1 104.2(2) . . ? O2A P1 N1 164(4) . . ? O1 P1 N1 86.70(19) . . ? O2 P1 N1 150.3(8) . . ? N2 P1 N1 84.4(2) . . ? C8 O1 P1 115.4(3) . . ? C26 O2 P1 113.6(10) . . ? C26 O2A P1 123(5) . . ? P1 O3 H3 109.5 . . ? C1 N1 C7 131.1(5) . . ? C1 N1 P1 116.1(4) . . ? C7 N1 P1 112.5(3) . . ? C6 N2 C21 129.5(4) . . ? C6 N2 P1 116.6(4) . . ? C21 N2 P1 113.7(3) . . ? N1 C1 C2 129.1(6) . . ? N1 C1 C6 109.8(5) . . ? C2 C1 C6 121.1(5) . . ? C1 C2 C3 118.1(6) . . ? C1 C2 H2 120.9 . . ? C3 C2 H2 120.9 . . ? C4 C3 C2 120.8(6) . . ? C4 C3 H3A 119.6 . . ? C2 C3 H3A 119.6 . . ? C3 C4 C5 120.6(6) . . ? C3 C4 H4 119.7 . . ? C5 C4 H4 119.7 . . ? C6 C5 C4 120.2(6) . . ? C6 C5 H5 119.9 . . ? C4 C5 H5 119.9 . . ? C5 C6 N2 130.7(6) . . ? C5 C6 C1 119.0(5) . . ? N2 C6 C1 110.3(5) . . ? C8 C7 N1 109.3(5) . . ? C8 C7 C12 119.6(5) . . ? N1 C7 C12 131.1(5) . . ? O1 C8 C9 122.9(5) . . ? O1 C8 C7 112.8(5) . . ? C9 C8 C7 124.3(5) . . ? C8 C9 C10 114.9(5) . . ? C8 C9 C13 122.2(5) . . ? C10 C9 C13 122.8(5) . . ? C9 C10 C11 122.6(5) . . ? C9 C10 H10 118.7 . . ? C11 C10 H10 118.7 . . ? C12 C11 C10 120.0(5) . . ? C12 C11 C17 120.7(5) . . ? C10 C11 C17 119.3(6) . . ? C11 C12 C7 118.4(5) . . ? C11 C12 H12 120.8 . . ? C7 C12 H12 120.8 . . ? C9 C13 C15 110.2(4) . . ? C9 C13 C14 109.8(4) . . ? C15 C13 C14 108.9(5) . . ? C9 C13 C16 112.6(5) . . ? C15 C13 C16 107.7(5) . . ? C14 C13 C16 107.6(4) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C13 C16 H16A 109.5 . . ? C13 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C13 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C19A C17 C20A 110.5(14) . . ? C18 C17 C19 114.3(13) . . ? C18 C17 C11 112.6(8) . . ? C19A C17 C11 112.5(12) . . ? C20A C17 C11 115.9(9) . . ? C19 C17 C11 110.1(9) . . ? C19A C17 C18A 112.6(14) . . ? C20A C17 C18A 103.5(11) . . ? C11 C17 C18A 101.1(8) . . ? C18 C17 C20 111.6(12) . . ? C19 C17 C20 103.2(9) . . ? C11 C17 C20 104.2(7) . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C17 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C17 C18A H18D 109.5 . . ? C17 C18A H18E 109.5 . . ? H18D C18A H18E 109.5 . . ? C17 C18A H18F 109.5 . . ? H18D C18A H18F 109.5 . . ? H18E C18A H18F 109.5 . . ? C17 C19 H19A 109.5 . . ? C17 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C17 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C19A H19D 109.5 . . ? C17 C19A H19E 109.5 . . ? H19D C19A H19E 109.5 . . ? C17 C19A H19F 109.5 . . ? H19D C19A H19F 109.5 . . ? H19E C19A H19F 109.5 . . ? C17 C20 H20A 109.5 . . ? C17 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C17 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C17 C20A H20D 109.5 . . ? C17 C20A H20E 109.5 . . ? H20D C20A H20E 109.5 . . ? C17 C20A H20F 109.5 . . ? H20D C20A H20F 109.5 . . ? H20E C20A H20F 109.5 . . ? C26 C21 N2 109.4(4) . . ? C26 C21 C22 119.3(5) . . ? N2 C21 C22 131.3(5) . . ? C23 C22 C21 119.3(5) . . ? C23 C22 H22 120.4 . . ? C21 C22 H22 120.4 . . ? C24 C23 C22 118.4(5) . . ? C24 C23 C27 123.5(6) . . ? C22 C23 C27 118.2(6) . . ? C23 C24 C25 125.6(5) . . ? C23 C24 H24 117.2 . . ? C25 C24 H24 117.2 . . ? C24 C25 C26 113.8(5) . . ? C24 C25 C31 124.3(5) . . ? C26 C25 C31 121.9(5) . . ? O2 C26 C21 114.6(7) . . ? O2 C26 C25 121.6(8) . . ? C21 C26 C25 123.7(5) . . ? C21 C26 O2A 104(4) . . ? C25 C26 O2A 131(4) . . ? C28 C27 C30 103.0(12) . . ? C28 C27 C29 107.8(12) . . ? C30 C27 C29 113.1(13) . . ? C28A C27 C23 109.8(8) . . ? C28 C27 C23 111.9(9) . . ? C30 C27 C23 110.3(8) . . ? C29 C27 C23 110.5(8) . . ? C28A C27 C29A 115.1(12) . . ? C23 C27 C29A 106.5(7) . . ? C28A C27 C30A 111.4(13) . . ? C23 C27 C30A 110.3(9) . . ? C29A C27 C30A 103.4(11) . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C27 C28A H28D 109.5 . . ? C27 C28A H28E 109.5 . . ? H28D C28A H28E 109.5 . . ? C27 C28A H28F 109.5 . . ? H28D C28A H28F 109.5 . . ? H28E C28A H28F 109.5 . . ? C27 C29 H29A 109.5 . . ? C27 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C27 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C27 C29A H29D 109.5 . . ? C27 C29A H29E 109.5 . . ? H29D C29A H29E 109.5 . . ? C27 C29A H29F 109.5 . . ? H29D C29A H29F 109.5 . . ? H29E C29A H29F 109.5 . . ? C27 C30 H30A 109.5 . . ? C27 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C27 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C27 C30A H30D 109.5 . . ? C27 C30A H30E 109.5 . . ? H30D C30A H30E 109.5 . . ? C27 C30A H30F 109.5 . . ? H30D C30A H30F 109.5 . . ? H30E C30A H30F 109.5 . . ? C32 C31 C25 109.1(4) . . ? C32 C31 C34 110.0(5) . . ? C25 C31 C34 109.2(5) . . ? C32 C31 C33 109.3(5) . . ? C25 C31 C33 111.9(5) . . ? C34 C31 C33 107.4(5) . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C31 C33 H33A 109.5 . . ? C31 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C31 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C31 C34 H34A 109.5 . . ? C31 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? C31 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3 P1 O1 C8 87.3(4) . . . . ? O2A P1 O1 C8 180(4) . . . . ? O2 P1 O1 C8 -169.1(7) . . . . ? N2 P1 O1 C8 -93.1(4) . . . . ? N1 P1 O1 C8 -16.6(3) . . . . ? O3 P1 O2 C26 -100.0(14) . . . . ? O1 P1 O2 C26 151.8(16) . . . . ? N2 P1 O2 C26 8.7(15) . . . . ? N1 P1 O2 C26 84(2) . . . . ? O3 P1 O2A C26 -131(11) . . . . ? O1 P1 O2A C26 120(11) . . . . ? N2 P1 O2A C26 -22(10) . . . . ? N1 P1 O2A C26 27(27) . . . . ? O3 P1 N1 C1 93.1(4) . . . . ? O2A P1 N1 C1 -63(17) . . . . ? O1 P1 N1 C1 -157.5(4) . . . . ? O2 P1 N1 C1 -90.4(9) . . . . ? N2 P1 N1 C1 -14.6(4) . . . . ? O3 P1 N1 C7 -93.0(4) . . . . ? O2A P1 N1 C7 111(17) . . . . ? O1 P1 N1 C7 16.5(3) . . . . ? O2 P1 N1 C7 83.5(9) . . . . ? N2 P1 N1 C7 159.3(4) . . . . ? O3 P1 N2 C6 -87.4(4) . . . . ? O2A P1 N2 C6 -177(6) . . . . ? O1 P1 N2 C6 93.0(4) . . . . ? O2 P1 N2 C6 166.9(9) . . . . ? N1 P1 N2 C6 15.7(4) . . . . ? O3 P1 N2 C21 98.2(4) . . . . ? O2A P1 N2 C21 9(6) . . . . ? O1 P1 N2 C21 -81.4(5) . . . . ? O2 P1 N2 C21 -7.5(9) . . . . ? N1 P1 N2 C21 -158.7(4) . . . . ? C7 N1 C1 C2 18.0(9) . . . . ? P1 N1 C1 C2 -169.5(4) . . . . ? C7 N1 C1 C6 -162.1(5) . . . . ? P1 N1 C1 C6 10.4(5) . . . . ? N1 C1 C2 C3 178.5(5) . . . . ? C6 C1 C2 C3 -1.4(8) . . . . ? C1 C2 C3 C4 -1.2(9) . . . . ? C2 C3 C4 C5 1.6(9) . . . . ? C3 C4 C5 C6 0.6(9) . . . . ? C4 C5 C6 N2 179.4(5) . . . . ? C4 C5 C6 C1 -3.1(7) . . . . ? C21 N2 C6 C5 -22.3(8) . . . . ? P1 N2 C6 C5 164.3(4) . . . . ? C21 N2 C6 C1 160.0(5) . . . . ? P1 N2 C6 C1 -13.4(5) . . . . ? N1 C1 C6 C5 -176.4(4) . . . . ? C2 C1 C6 C5 3.5(7) . . . . ? N1 C1 C6 N2 1.6(6) . . . . ? C2 C1 C6 N2 -178.5(4) . . . . ? C1 N1 C7 C8 160.4(5) . . . . ? P1 N1 C7 C8 -12.4(5) . . . . ? C1 N1 C7 C12 -20.2(9) . . . . ? P1 N1 C7 C12 167.1(5) . . . . ? P1 O1 C8 C9 -169.1(4) . . . . ? P1 O1 C8 C7 13.2(5) . . . . ? N1 C7 C8 O1 0.2(6) . . . . ? C12 C7 C8 O1 -179.3(5) . . . . ? N1 C7 C8 C9 -177.4(5) . . . . ? C12 C7 C8 C9 3.1(8) . . . . ? O1 C8 C9 C10 179.8(4) . . . . ? C7 C8 C9 C10 -2.8(7) . . . . ? O1 C8 C9 C13 -0.1(7) . . . . ? C7 C8 C9 C13 177.2(5) . . . . ? C8 C9 C10 C11 0.4(8) . . . . ? C13 C9 C10 C11 -179.6(5) . . . . ? C9 C10 C11 C12 1.6(8) . . . . ? C9 C10 C11 C17 -178.2(5) . . . . ? C10 C11 C12 C7 -1.3(8) . . . . ? C17 C11 C12 C7 178.4(5) . . . . ? C8 C7 C12 C11 -0.8(8) . . . . ? N1 C7 C12 C11 179.8(5) . . . . ? C8 C9 C13 C15 -59.8(7) . . . . ? C10 C9 C13 C15 120.2(6) . . . . ? C8 C9 C13 C14 60.1(6) . . . . ? C10 C9 C13 C14 -119.8(6) . . . . ? C8 C9 C13 C16 179.9(5) . . . . ? C10 C9 C13 C16 0.0(7) . . . . ? C12 C11 C17 C18 124.4(14) . . . . ? C10 C11 C17 C18 -55.8(15) . . . . ? C12 C11 C17 C19A -48.5(16) . . . . ? C10 C11 C17 C19A 131.3(14) . . . . ? C12 C11 C17 C20A -177.0(12) . . . . ? C10 C11 C17 C20A 2.7(14) . . . . ? C12 C11 C17 C19 -4.3(11) . . . . ? C10 C11 C17 C19 175.5(9) . . . . ? C12 C11 C17 C18A 71.9(9) . . . . ? C10 C11 C17 C18A -108.4(9) . . . . ? C12 C11 C17 C20 -114.4(8) . . . . ? C10 C11 C17 C20 65.4(8) . . . . ? C6 N2 C21 C26 -169.1(5) . . . . ? P1 N2 C21 C26 4.5(5) . . . . ? C6 N2 C21 C22 9.0(9) . . . . ? P1 N2 C21 C22 -177.5(4) . . . . ? C26 C21 C22 C23 1.1(7) . . . . ? N2 C21 C22 C23 -176.8(5) . . . . ? C21 C22 C23 C24 -1.9(8) . . . . ? C21 C22 C23 C27 176.7(5) . . . . ? C22 C23 C24 C25 2.2(8) . . . . ? C27 C23 C24 C25 -176.3(5) . . . . ? C23 C24 C25 C26 -1.6(8) . . . . ? C23 C24 C25 C31 178.5(5) . . . . ? P1 O2 C26 C21 -8.2(19) . . . . ? P1 O2 C26 C25 176.2(8) . . . . ? N2 C21 C26 O2 2.2(13) . . . . ? C22 C21 C26 O2 -176.1(13) . . . . ? N2 C21 C26 C25 177.8(5) . . . . ? C22 C21 C26 C25 -0.5(8) . . . . ? N2 C21 C26 O2A -17(5) . . . . ? C22 C21 C26 O2A 165(5) . . . . ? C24 C25 C26 O2 176.0(13) . . . . ? C31 C25 C26 O2 -4.1(14) . . . . ? C24 C25 C26 C21 0.7(7) . . . . ? C31 C25 C26 C21 -179.4(5) . . . . ? C24 C25 C26 O2A -160(8) . . . . ? C31 C25 C26 O2A 19(8) . . . . ? P1 O2A C26 C21 28(12) . . . . ? P1 O2A C26 C25 -168(6) . . . . ? C24 C23 C27 C28A 70.6(14) . . . . ? C22 C23 C27 C28A -107.9(14) . . . . ? C24 C23 C27 C28 130.2(14) . . . . ? C22 C23 C27 C28 -48.2(15) . . . . ? C24 C23 C27 C30 -115.7(12) . . . . ? C22 C23 C27 C30 65.8(13) . . . . ? C24 C23 C27 C29 10.1(13) . . . . ? C22 C23 C27 C29 -168.4(11) . . . . ? C24 C23 C27 C29A -54.7(11) . . . . ? C22 C23 C27 C29A 126.8(10) . . . . ? C24 C23 C27 C30A -166.2(12) . . . . ? C22 C23 C27 C30A 15.3(13) . . . . ? C24 C25 C31 C32 121.8(5) . . . . ? C26 C25 C31 C32 -58.1(6) . . . . ? C24 C25 C31 C34 -117.9(5) . . . . ? C26 C25 C31 C34 62.2(6) . . . . ? C24 C25 C31 C33 0.8(7) . . . . ? C26 C25 C31 C33 -179.2(5) . . . . ? _refine_diff_density_max 0.276 _refine_diff_density_min -0.202 _refine_diff_density_rms 0.046 _shelx_res_file ; romanta52b.res created by SHELXL-2014/7 TITL mo_RomanTA52b_0m_a.res in I4(1)/a REM Old TITL mo_RomanTA52b_0m in I4(1)/a REM SHELXT solution in I4(1)/a REM R1 0.399, Rweak 0.088, Alpha 0.078, Orientation as input REM Formula found by SHELXT: C30 N1A O1 P CELL 0.71073 33.2008 33.2008 15.6607 90 90 90 ZERR 16 0.005 0.005 0.003 0 0 0 LATT 2 SYMM 0.5-X,-Y,0.5+Z SYMM 0.75-Y,0.25+X,0.25+Z SYMM 0.75+Y,0.75-X,0.75+Z SFAC C H N O P UNIT 544 720 32 48 16 DELU SIMU L.S. 10 PLAN 28 SIZE 0.15 0.15 0.21 TEMP -73 CONF LIST 6 MORE -1 ABIN BOND $H fmap 2 acta OMIT 12 12 0 OMIT -2 12 2 OMIT -3 4 1 OMIT -4 10 2 OMIT 12 14 0 OMIT 1 15 2 OMIT 0 6 4 OMIT 2 5 3 OMIT 9 11 2 OMIT -3 5 4 REM REM REM WGHT 0.133400 EXTI 0.000307 FVAR 0.11863 0.52768 0.47232 0.11521 P1 5 0.430372 0.559668 0.554141 11.00000 0.06736 0.06885 = 0.05586 0.00362 -0.00196 -0.00105 O1 4 0.391429 0.540652 0.608339 11.00000 0.07034 0.07900 = 0.05194 0.01383 -0.01158 -0.01706 PART 1 O2 4 0.396172 0.558525 0.472552 -41.00000 0.06527 0.07952 = 0.04197 0.01206 -0.00255 -0.01040 PART 2 O2A 4 0.410778 0.554244 0.467915 41.00000 0.06803 0.07130 = 0.04774 0.00615 -0.00255 -0.00817 PART 0 O3 4 0.459583 0.527264 0.534936 11.00000 0.07214 0.07404 = 0.08566 -0.00019 -0.00359 0.01116 AFIX 83 H3 2 0.455750 0.507817 0.568270 11.00000 -1.50000 AFIX 0 N1 3 0.447265 0.579895 0.653516 11.00000 0.07160 0.08382 = 0.05183 0.00163 0.00116 -0.01333 N2 3 0.448680 0.604894 0.511400 11.00000 0.06790 0.07260 = 0.05713 -0.00156 -0.00063 -0.01056 C1 1 0.472786 0.612353 0.648569 11.00000 0.05796 0.06942 = 0.06784 -0.00669 -0.00206 0.00504 C2 1 0.495150 0.630403 0.712530 11.00000 0.07285 0.10460 = 0.07424 -0.01442 -0.00669 -0.01306 AFIX 43 H2 2 0.493756 0.620993 0.769741 11.00000 -1.20000 AFIX 0 C3 1 0.519747 0.662735 0.690673 11.00000 0.06778 0.12164 = 0.09649 -0.02643 0.00095 -0.02182 AFIX 43 H3A 2 0.534994 0.675927 0.733717 11.00000 -1.20000 AFIX 0 C4 1 0.522261 0.675859 0.607338 11.00000 0.07430 0.09185 = 0.09853 -0.01127 0.00245 -0.02119 AFIX 43 H4 2 0.539744 0.697523 0.593316 11.00000 -1.20000 AFIX 0 C5 1 0.499339 0.657599 0.543275 11.00000 0.06565 0.07426 = 0.08237 -0.00761 0.00673 -0.00951 AFIX 43 H5 2 0.501507 0.666743 0.485978 11.00000 -1.20000 AFIX 0 C6 1 0.474115 0.627001 0.562528 11.00000 0.05482 0.06237 = 0.06561 -0.00734 0.00098 0.00053 C7 1 0.428584 0.561922 0.723161 11.00000 0.06657 0.07590 = 0.04981 0.00083 -0.00198 -0.00323 C8 1 0.396145 0.539315 0.695090 11.00000 0.05404 0.07093 = 0.05266 0.00544 -0.00324 0.00191 C9 1 0.370049 0.518701 0.748334 11.00000 0.06448 0.07316 = 0.05880 0.01498 -0.00026 -0.00343 C10 1 0.379634 0.520564 0.835094 11.00000 0.06746 0.10281 = 0.05419 0.01502 -0.00171 -0.00353 AFIX 43 H10 2 0.362882 0.506803 0.874685 11.00000 -1.20000 AFIX 0 C11 1 0.413154 0.542036 0.866207 11.00000 0.07825 0.10110 = 0.04980 0.00306 -0.00894 -0.00199 C12 1 0.437613 0.563241 0.810199 11.00000 0.06339 0.11379 = 0.05171 0.00818 -0.01051 -0.01164 AFIX 43 H12 2 0.459968 0.578297 0.830570 11.00000 -1.20000 AFIX 0 C13 1 0.333755 0.495809 0.714434 11.00000 0.07255 0.08466 = 0.06234 0.01839 -0.00432 -0.01939 C14 1 0.347682 0.462768 0.652545 11.00000 0.10067 0.10153 = 0.07669 -0.00509 0.00108 -0.02071 AFIX 137 H14A 2 0.363293 0.474930 0.606114 11.00000 -1.50000 H14B 2 0.324118 0.448963 0.628800 11.00000 -1.50000 H14C 2 0.364526 0.443318 0.683213 11.00000 -1.50000 AFIX 0 C15 1 0.305436 0.524434 0.667157 11.00000 0.07327 0.12208 = 0.07753 0.02280 -0.01763 -0.00722 AFIX 137 H15A 2 0.296691 0.545870 0.705977 11.00000 -1.50000 H15B 2 0.281872 0.509468 0.646818 11.00000 -1.50000 H15C 2 0.319583 0.536320 0.618358 11.00000 -1.50000 AFIX 0 C16 1 0.309466 0.475407 0.785630 11.00000 0.08795 0.10988 = 0.06730 0.02680 -0.00320 -0.02609 AFIX 137 H16A 2 0.325636 0.453924 0.811447 11.00000 -1.50000 H16B 2 0.284754 0.463905 0.761618 11.00000 -1.50000 H16C 2 0.302489 0.495355 0.829317 11.00000 -1.50000 AFIX 0 C17 1 0.422337 0.541491 0.963233 11.00000 0.09565 0.17138 = 0.05010 0.01227 -0.00994 -0.00218 PART 1 C18 1 0.388200 0.555118 1.014753 21.00000 0.13365 0.28163 = 0.04849 -0.04459 -0.01783 0.03413 AFIX 137 H18A 2 0.363260 0.543481 0.992135 21.00000 -1.50000 H18B 2 0.386536 0.584571 1.012604 21.00000 -1.50000 H18C 2 0.391938 0.546431 1.074031 21.00000 -1.50000 AFIX 0 PART 2 C18A 1 0.409526 0.589224 0.991145 -21.00000 0.14489 0.17661 = 0.10519 -0.05651 0.00917 -0.03688 AFIX 137 H18D 2 0.425839 0.608397 0.958468 -21.00000 -1.50000 H18E 2 0.414404 0.593119 1.052307 -21.00000 -1.50000 H18F 2 0.380941 0.593705 0.978768 -21.00000 -1.50000 AFIX 0 PART 1 C19 1 0.461304 0.563594 0.981031 21.00000 0.13591 0.15992 = 0.05760 -0.00069 -0.03935 -0.01281 AFIX 137 H19A 2 0.483133 0.551340 0.947874 21.00000 -1.50000 H19B 2 0.467621 0.561817 1.042042 21.00000 -1.50000 H19C 2 0.458394 0.591940 0.964702 21.00000 -1.50000 AFIX 0 PART 2 C19A 1 0.464679 0.532258 0.981490 -21.00000 0.12121 0.29783 = 0.08719 0.04622 -0.03967 0.02371 AFIX 137 H19D 2 0.481929 0.545936 0.939803 -21.00000 -1.50000 H19E 2 0.468949 0.503104 0.977748 -21.00000 -1.50000 H19F 2 0.471448 0.541565 1.039115 -21.00000 -1.50000 AFIX 0 PART 1 C20 1 0.434220 0.492627 0.984136 21.00000 0.11268 0.17416 = 0.06910 0.05043 -0.02344 -0.01445 AFIX 137 H20A 2 0.412090 0.475162 0.965595 21.00000 -1.50000 H20B 2 0.438576 0.489218 1.045604 21.00000 -1.50000 H20C 2 0.458840 0.485356 0.953248 21.00000 -1.50000 AFIX 0 PART 2 C20A 1 0.395400 0.516197 1.016270 -21.00000 0.15959 0.18825 = 0.04587 0.01135 -0.01714 -0.04882 AFIX 137 H20D 2 0.367317 0.521320 1.000350 -21.00000 -1.50000 H20E 2 0.399333 0.522831 1.076673 -21.00000 -1.50000 H20F 2 0.401731 0.487710 1.006868 -21.00000 -1.50000 AFIX 0 PART 0 C21 1 0.432000 0.614709 0.432644 11.00000 0.06961 0.06089 = 0.04626 -0.00812 0.01052 -0.00184 C22 1 0.439456 0.646959 0.376898 11.00000 0.08418 0.06822 = 0.06168 0.00031 0.02044 -0.01134 AFIX 43 H22 2 0.459876 0.666086 0.389603 11.00000 -1.20000 AFIX 0 C23 1 0.416440 0.650631 0.302275 11.00000 0.09487 0.07099 = 0.04937 0.00647 0.02413 0.00158 C24 1 0.388171 0.621759 0.285309 11.00000 0.09204 0.07360 = 0.04504 0.00536 0.00631 0.00548 AFIX 43 H24 2 0.373538 0.624205 0.233438 11.00000 -1.20000 AFIX 0 C25 1 0.379002 0.589098 0.337532 11.00000 0.07785 0.06765 = 0.04634 0.00233 0.00359 0.01191 C26 1 0.402714 0.586991 0.412105 11.00000 0.07403 0.06394 = 0.04100 0.00249 0.01353 -0.00270 C27 1 0.423640 0.687463 0.244949 11.00000 0.14083 0.08770 = 0.07023 0.02322 0.02596 -0.01354 PART 1 C28 1 0.424105 0.725793 0.295047 31.00000 0.25624 0.08287 = 0.06970 0.02338 0.02273 -0.00605 AFIX 137 H28A 2 0.417620 0.748415 0.257274 31.00000 -1.50000 H28B 2 0.450914 0.729832 0.319789 31.00000 -1.50000 H28C 2 0.404084 0.724257 0.340914 31.00000 -1.50000 AFIX 0 PART 2 C28A 1 0.389141 0.715595 0.251901 -31.00000 0.22967 0.12230 = 0.14724 0.08006 0.06864 0.05053 AFIX 137 H28D 2 0.363936 0.700763 0.243423 -31.00000 -1.50000 H28E 2 0.391576 0.736593 0.208226 -31.00000 -1.50000 H28F 2 0.389098 0.728033 0.308652 -31.00000 -1.50000 AFIX 0 PART 1 C29 1 0.390660 0.690873 0.177955 31.00000 0.17946 0.11938 = 0.09300 0.05779 -0.00571 -0.01822 AFIX 137 H29A 2 0.383741 0.663957 0.156872 31.00000 -1.50000 H29B 2 0.400217 0.707498 0.130381 31.00000 -1.50000 H29C 2 0.366769 0.703364 0.203439 31.00000 -1.50000 AFIX 0 PART 2 C29A 1 0.432030 0.670518 0.151349 -31.00000 0.21768 0.13128 = 0.06462 0.02576 0.03621 -0.02533 AFIX 137 H29D 2 0.406370 0.664264 0.123408 -31.00000 -1.50000 H29E 2 0.448391 0.646016 0.155185 -31.00000 -1.50000 H29F 2 0.446487 0.690860 0.117931 -31.00000 -1.50000 AFIX 0 PART 1 C30 1 0.465415 0.685961 0.207016 31.00000 0.15235 0.10009 = 0.13000 0.03517 0.05485 -0.02810 AFIX 137 H30A 2 0.467713 0.706225 0.161777 31.00000 -1.50000 H30B 2 0.470309 0.659147 0.183002 31.00000 -1.50000 H30C 2 0.485341 0.691537 0.251643 31.00000 -1.50000 AFIX 0 PART 2 C30A 1 0.465295 0.709096 0.269946 -31.00000 0.21800 0.18754 = 0.11346 0.03403 0.02644 -0.11037 AFIX 137 H30D 2 0.487497 0.689835 0.264191 -31.00000 -1.50000 H30E 2 0.463884 0.718615 0.329104 -31.00000 -1.50000 H30F 2 0.469910 0.732031 0.231789 -31.00000 -1.50000 AFIX 0 PART 0 C31 1 0.346612 0.557991 0.317739 11.00000 0.08109 0.08897 = 0.03629 0.00692 -0.00206 0.00439 C32 1 0.365786 0.516458 0.314459 11.00000 0.11765 0.08119 = 0.08316 -0.01148 -0.02434 0.00317 AFIX 137 H32A 2 0.387850 0.516531 0.272890 11.00000 -1.50000 H32B 2 0.345527 0.496562 0.297374 11.00000 -1.50000 H32C 2 0.376348 0.509498 0.370999 11.00000 -1.50000 AFIX 0 C33 1 0.325396 0.566685 0.231780 11.00000 0.12965 0.12050 = 0.06234 0.00288 -0.03612 -0.00385 AFIX 137 H33A 2 0.344803 0.563872 0.185009 11.00000 -1.50000 H33B 2 0.314656 0.594179 0.232228 11.00000 -1.50000 H33C 2 0.303283 0.547514 0.223632 11.00000 -1.50000 AFIX 0 C34 1 0.314364 0.559286 0.387617 11.00000 0.08664 0.11194 = 0.07121 0.00626 -0.00143 -0.00916 AFIX 137 H34A 2 0.326827 0.553762 0.443121 11.00000 -1.50000 H34B 2 0.293761 0.538900 0.375774 11.00000 -1.50000 H34C 2 0.301869 0.586024 0.388669 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_RomanTA52b_0m_a.res in I4(1)/a REM R1 = 0.0934 for 2906 Fo > 4sig(Fo) and 0.1679 for all 6418 data REM 446 parameters refined using 547 restraints END WGHT 0.1316 0.0000 REM Highest difference peak 0.276, deepest hole -0.202, 1-sigma level 0.046 Q1 1 0.4642 0.4710 0.4245 11.00000 0.05 0.28 Q2 1 0.5075 0.5116 0.5278 11.00000 0.05 0.24 Q3 1 0.4897 0.5482 0.5203 11.00000 0.05 0.24 Q4 1 0.5008 0.5189 0.5454 11.00000 0.05 0.24 Q5 1 0.4504 0.5893 0.5574 11.00000 0.05 0.22 Q6 1 0.4884 0.7344 0.1440 11.00000 0.05 0.21 Q7 1 0.4825 0.4905 0.5520 11.00000 0.05 0.21 Q8 1 0.4030 0.5894 0.5519 11.00000 0.05 0.19 Q9 1 0.4907 0.5611 0.5609 11.00000 0.05 0.19 Q10 1 0.4182 0.6065 0.6539 11.00000 0.05 0.19 Q11 1 0.3056 0.5134 0.3943 11.00000 0.05 0.18 Q12 1 0.4789 0.5837 0.4796 11.00000 0.05 0.18 Q13 1 0.3739 0.5882 0.4873 11.00000 0.05 0.18 Q14 1 0.4735 0.5461 0.6413 11.00000 0.05 0.18 Q15 1 0.3728 0.5335 0.4648 11.00000 0.05 0.18 Q16 1 0.3450 0.5188 1.0200 11.00000 0.05 0.18 Q17 1 0.3606 0.5102 0.5946 11.00000 0.05 0.18 Q18 1 0.4844 0.7211 0.1248 11.00000 0.05 0.17 Q19 1 0.3379 0.4492 0.7953 11.00000 0.05 0.17 Q20 1 0.4403 0.5793 0.3924 11.00000 0.05 0.17 Q21 1 0.4211 0.6180 0.5471 11.00000 0.05 0.17 Q22 1 0.4374 0.6162 0.9683 11.00000 0.05 0.17 Q23 1 0.3792 0.4606 0.9526 11.00000 0.05 0.17 Q24 1 0.5798 0.7200 0.6231 11.00000 0.05 0.16 Q25 1 0.4306 0.5863 0.4858 11.00000 0.05 0.16 Q26 1 0.4337 0.5018 0.5518 11.00000 0.05 0.16 Q27 1 0.4706 0.6181 0.3726 11.00000 0.05 0.16 Q28 1 0.5486 0.6416 0.6948 11.00000 0.05 0.16 ; _shelx_res_checksum 89680 _shelx_hkl_file ; -1 1 0 -5.20 0.30 1 -1 0 -4.80 0.20 -1 1 0 -5.20 0.20 -2 2 0 3554.34 72.69 2 -2 0 3524.05 72.59 2 2 0 3425.86 72.09 -2 2 0 3298.17 72.69 2 -2 0 3446.66 71.99 -2 -2 0 3501.55 72.09 1 -3 0 5.60 1.20 3 1 0 3.50 1.10 -1 -3 0 1.70 0.90 3 -1 0 1.20 0.80 3 -1 0 1.90 0.80 1 3 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7.60 -6 -10 0 71.59 5.30 10 -6 0 71.59 6.10 -10 8 0 14.80 5.00 10 -8 0 17.60 4.90 8 10 0 25.60 4.40 -8 -10 0 24.60 4.10 -10 -10 0 88.79 5.20 -10 10 0 76.89 8.50 10 10 0 88.09 5.90 10 10 0 87.79 8.00 10 -10 0 94.19 7.40 -11 -9 0 0.10 2.70 11 9 0 -4.00 3.40 11 9 0 1.20 4.70 9 -11 0 1.30 4.70 -11 -7 0 2.20 2.30 11 7 0 1.30 2.80 11 7 0 0.60 4.00 7 -11 0 2.50 4.70 11 5 0 -0.80 3.80 5 -11 0 5.40 4.50 3 -11 0 2.30 4.40 11 1 0 -2.60 3.40 1 -11 0 2.10 4.30 -11 -1 0 0.60 1.00 -11 -1 0 1.00 2.30 -11 1 0 0.90 2.80 -11 1 0 1.30 1.10 -1 -11 0 3.00 4.20 11 -1 0 1.90 3.10 11 -3 0 0.30 3.10 -3 -11 0 5.10 4.00 -11 3 0 3.20 3.30 11 -3 0 3.00 3.40 -5 -11 0 4.10 3.80 11 -5 0 4.80 3.90 11 -7 0 0.20 4.00 -11 7 0 -0.90 4.50 -7 -11 0 -0.50 3.50 9 11 0 0.10 4.70 -11 9 0 -1.70 4.50 11 -9 0 -2.50 4.50 -9 -11 0 -0.20 3.30 -11 11 0 1.00 5.80 11 11 0 9.00 5.80 11 11 0 11.00 4.50 11 -11 0 18.80 5.90 -12 -10 0 501.25 13.10 12 10 0 518.45 13.80 10 -12 0 494.15 16.80 8 -12 0 241.78 11.30 12 8 0 244.08 10.40 -12 -8 0 240.98 7.00 12 8 0 243.98 7.60 12 6 0 115.79 7.50 6 -12 0 103.69 7.80 4 -12 0 41.50 6.10 12 4 0 47.10 5.70 -12 -2 0 311.57 8.10 2 -12 0 311.97 11.50 -12 -2 0 303.17 7.90 12 2 0 306.87 10.80 12 0 0 279.47 8.60 -12 0 0 284.87 8.10 0 -12 0 295.37 11.10 -12 0 0 285.37 8.20 12 0 0 270.47 10.10 -2 -12 0 53.49 5.90 -12 2 0 45.70 4.50 12 -2 0 47.40 4.80 -12 2 0 45.40 4.00 12 -2 0 46.40 5.00 12 -4 0 429.26 12.70 12 -4 0 425.16 13.20 -4 -12 0 431.96 13.30 12 -6 0 8.10 4.40 -6 -12 0 7.00 4.10 -8 -12 0 141.49 7.10 -12 8 0 122.49 10.10 12 -8 0 143.09 8.10 12 -10 0 2020.10 48.50 -12 10 0 2119.19 52.49 -10 -12 0 2011.30 45.90 10 12 0 2124.29 49.70 -12 -12 0 141.09 7.00 -12 12 0 142.49 11.60 12 12 0 135.79 10.30 12 -12 0 142.49 9.90 13 11 0 5.10 4.40 -13 -11 0 7.60 3.50 11 -13 0 5.50 6.00 13 9 0 3.20 3.60 9 -13 0 11.00 5.70 13 9 0 12.10 5.20 7 -13 0 0.40 4.70 13 7 0 4.10 4.50 5 -13 0 -1.60 4.50 13 5 0 0.60 4.00 -13 -3 0 2.80 1.80 13 3 0 2.90 3.90 3 -13 0 1.00 4.50 -13 -1 0 0.90 2.30 -13 -1 0 0.40 1.10 13 1 0 2.20 3.70 1 -13 0 4.50 4.40 -13 1 0 3.70 2.90 -13 1 0 0.50 1.10 13 -1 0 -1.70 3.20 -1 -13 0 -0.10 4.30 13 -3 0 4.60 3.60 13 -3 0 6.10 3.70 -3 -13 0 7.30 4.60 -5 -13 0 0.40 4.10 13 -5 0 1.30 3.90 -7 -13 0 4.20 4.10 13 -7 0 2.60 4.50 -13 7 0 5.10 5.00 -13 9 0 19.40 6.70 -13 11 0 9.10 6.10 -11 -13 0 9.00 4.30 13 -11 0 11.20 6.00 11 13 0 9.70 5.90 13 13 0 8.40 6.20 -13 13 0 9.60 6.90 -13 -13 0 4.70 4.00 13 -13 0 1.00 6.30 -14 -12 0 161.78 6.90 12 -14 0 157.38 10.90 14 12 0 165.18 8.20 10 -14 0 223.08 11.80 -14 -10 0 223.78 7.30 14 10 0 220.88 11.50 14 10 0 230.28 8.20 8 -14 0 70.99 8.40 14 8 0 74.59 7.60 -14 -8 0 70.39 3.50 14 6 0 4.60 4.70 6 -14 0 3.00 5.50 4 -14 0 227.98 10.70 14 2 0 393.86 13.20 2 -14 0 400.96 14.00 -14 -2 0 383.36 10.10 -14 -2 0 394.26 9.80 -14 0 0 62.29 4.20 14 0 0 71.29 6.60 0 -14 0 71.09 7.50 -14 0 0 54.79 4.20 -14 2 0 202.18 9.00 14 -2 0 194.78 7.90 -2 -14 0 208.18 9.50 14 -2 0 202.98 9.10 -14 2 0 207.18 7.50 14 -4 0 96.69 7.10 -14 4 0 93.59 5.80 14 -4 0 84.19 6.30 -4 -14 0 98.69 7.40 14 -6 0 30.10 5.70 -6 -14 0 25.00 5.40 14 -8 0 11.20 5.50 -14 8 0 0.70 5.40 -8 -14 0 8.50 4.60 -14 10 0 11.20 6.20 14 -10 0 3.00 5.70 -10 -14 0 4.40 4.50 10 14 0 1.80 5.70 -14 12 0 38.80 8.60 12 14 0 27.20 7.20 -12 -14 0 36.00 5.60 14 -12 0 29.10 7.60 -14 -14 0 450.45 13.70 14 -14 0 463.45 18.20 14 14 0 469.15 19.10 15 13 0 5.80 5.80 15 11 0 11.70 6.00 -15 -11 0 9.10 3.40 15 11 0 4.90 4.20 11 -15 0 16.20 6.90 9 -15 0 12.70 6.40 15 9 0 3.90 5.30 15 7 0 2.10 4.80 7 -15 0 5.10 5.70 5 -15 0 -1.10 5.50 15 3 0 5.50 4.60 -15 -3 0 0.60 2.00 3 -15 0 -6.50 4.80 -15 -1 0 -0.20 1.20 1 -15 0 0.50 5.00 15 1 0 -2.00 4.00 -15 -1 0 1.10 2.50 15 -1 0 6.60 3.70 -15 1 0 4.00 3.00 15 -1 0 12.80 4.20 -15 1 0 0.60 1.20 -1 -15 0 10.40 5.20 15 -3 0 1.10 3.90 15 -3 0 -2.80 3.70 -15 3 0 1.40 1.40 -3 -15 0 -5.90 4.40 15 -5 0 4.80 4.60 -15 5 0 -0.20 1.50 -5 -15 0 4.20 4.80 15 -7 0 0.40 5.00 -7 -15 0 -1.50 4.60 -15 7 0 -2.50 5.40 -15 9 0 -0.10 5.50 15 -9 0 -0.50 5.40 -9 -15 0 -3.00 4.60 -11 -15 0 1.60 4.60 11 15 0 0.50 6.20 15 -11 0 3.70 6.20 -15 11 0 3.50 6.30 13 15 0 10.80 6.90 -15 13 0 -0.30 6.90 15 -15 0 13.30 8.30 -15 -15 0 12.30 4.80 14 -16 0 109.09 12.10 16 14 0 110.89 10.70 -16 -14 0 102.29 6.90 12 -16 0 145.19 11.50 16 12 0 149.09 11.30 -16 -12 0 163.18 6.60 16 12 0 151.38 7.70 10 -16 0 571.34 20.00 16 10 0 552.94 18.80 8 -16 0 267.27 13.30 16 8 0 287.07 13.00 6 -16 0 17.50 6.50 16 4 0 17.50 5.50 4 -16 0 34.20 6.80 2 -16 0 75.09 8.60 -16 -2 0 61.09 4.00 16 2 0 73.69 7.50 -16 -2 0 64.09 4.50 0 -16 0 22.10 6.10 -16 0 0 22.80 3.70 -2 -16 0 35.40 6.60 16 -2 0 34.40 5.20 16 -2 0 26.90 4.90 16 -4 0 22.10 5.00 16 -4 0 24.20 5.40 -4 -16 0 21.50 5.80 -16 4 0 12.10 2.10 16 -6 0 5.00 5.10 -6 -16 0 1.50 5.10 -16 6 0 2.50 1.80 -8 -16 0 5.60 5.10 -16 8 0 0.70 5.40 16 -8 0 3.90 5.50 -16 10 0 167.08 12.80 16 -10 0 164.28 10.90 -10 -16 0 148.89 8.90 16 -12 0 243.48 13.20 -12 -16 0 229.98 10.20 -16 12 0 221.78 15.30 12 16 0 222.08 14.00 -14 -16 0 50.19 6.60 16 -14 0 52.79 9.80 -16 14 0 42.80 9.80 14 16 0 56.79 9.40 -16 -16 0 70.59 7.30 16 -16 0 66.09 11.20 15 -17 0 9.10 9.00 -17 -15 0 7.10 4.80 17 15 0 -0.60 6.80 -17 -13 0 8.50 3.90 13 -17 0 0.80 7.90 17 13 0 4.30 6.60 17 13 0 2.60 4.80 17 11 0 7.10 6.10 11 -17 0 4.20 6.90 17 9 0 16.80 6.00 7 -17 0 7.20 6.40 5 -17 0 1.10 6.10 17 5 0 -2.10 4.80 17 3 0 5.50 4.90 3 -17 0 -0.90 5.80 -17 -1 0 3.30 2.90 -17 -1 0 1.10 1.40 1 -17 0 0.10 5.80 17 1 0 -1.70 4.50 -1 -17 0 -1.20 5.40 -17 1 0 9.10 6.30 -17 1 0 0.00 1.40 17 -1 0 -4.90 3.90 17 -3 0 0.90 4.60 -3 -17 0 -0.40 5.40 17 -3 0 7.00 4.40 -17 3 0 1.40 1.60 17 -5 0 -0.10 5.00 -17 5 0 -0.70 1.70 -5 -17 0 -1.50 5.30 -7 -17 0 -0.80 5.10 17 -7 0 8.30 5.70 -17 7 0 1.40 1.90 -17 9 0 -0.60 6.10 -9 -17 0 5.30 5.50 17 -9 0 1.20 6.00 -11 -17 0 10.30 5.60 -17 11 0 12.60 7.00 11 17 0 5.30 6.80 17 -11 0 10.10 7.30 -13 -17 0 7.10 5.40 17 -13 0 0.10 7.90 13 17 0 1.40 7.20 -17 13 0 6.00 7.20 17 -15 0 2.40 8.30 -15 -17 0 1.00 5.40 15 17 0 -7.70 7.20 -17 15 0 1.10 8.00 17 -17 0 -3.50 9.40 -17 -17 0 2.90 5.60 18 16 0 16.30 8.40 -18 -16 0 16.20 5.60 16 -18 0 14.90 9.90 18 14 0 52.29 10.40 -18 -14 0 46.70 5.40 18 14 0 56.99 9.30 14 -18 0 46.70 10.70 12 -18 0 106.59 11.60 18 12 0 111.69 11.10 18 10 0 15.50 6.40 10 -18 0 21.90 8.00 8 -18 0 356.16 15.70 6 -18 0 52.79 8.70 18 6 0 63.19 7.80 4 -18 0 11.90 6.60 18 4 0 18.40 5.80 2 -18 0 27.40 7.40 -18 -2 0 18.10 1.90 18 2 0 32.90 6.30 0 -18 0 63.59 8.50 -18 0 0 54.89 5.10 -18 0 0 54.69 5.10 -18 2 0 2.00 1.60 18 -2 0 9.00 4.90 -2 -18 0 -0.40 5.80 18 -2 0 4.40 4.50 18 -4 0 239.18 11.40 -4 -18 0 220.38 11.30 18 -4 0 221.88 10.00 -18 4 0 236.88 9.40 -18 6 0 18.50 2.70 -6 -18 0 30.40 6.80 18 -6 0 45.70 7.10 -18 8 0 24.50 7.60 -18 8 0 9.90 2.50 -8 -18 0 9.20 5.90 18 -8 0 14.00 6.50 18 -10 0 5.90 6.70 -10 -18 0 14.20 6.10 -18 10 0 4.80 6.80 -18 12 0 -2.70 6.50 12 18 0 -4.00 7.20 18 -12 0 0.50 7.50 -12 -18 0 3.70 5.70 14 18 0 128.89 13.50 -14 -18 0 116.59 9.50 18 -14 0 121.19 12.90 -18 14 0 109.99 13.70 18 -16 0 22.10 10.00 -16 -18 0 37.80 7.20 18 18 0 16.00 8.70 -18 -18 0 14.90 6.60 18 -18 0 21.30 11.20 17 -19 0 11.20 10.90 19 17 0 10.50 8.60 19 15 0 12.30 7.80 15 -19 0 -4.40 9.20 -19 -15 0 6.10 5.70 13 -19 0 -1.10 8.50 19 13 0 -5.90 6.60 11 -19 0 6.70 8.20 19 11 0 3.00 6.50 9 -19 0 -1.50 6.90 19 7 0 3.40 5.80 7 -19 0 9.60 7.30 5 -19 0 1.70 6.30 19 5 0 3.80 5.60 19 3 0 4.70 5.10 3 -19 0 -0.60 6.50 1 -19 0 4.90 6.50 -19 -1 0 4.30 3.40 -19 -1 0 0.60 1.50 19 -1 0 3.40 4.60 -1 -19 0 2.90 6.20 -19 1 0 -0.60 1.60 -3 -19 0 11.30 6.30 -19 3 0 1.00 1.80 19 -3 0 6.00 5.10 19 -3 0 -1.90 4.60 -5 -19 0 1.30 6.10 -19 5 0 -2.30 1.70 19 -5 0 4.00 5.50 -7 -19 0 4.10 6.10 19 -7 0 4.40 6.20 -19 7 0 -0.80 2.00 -19 9 0 6.20 6.80 19 -9 0 4.40 6.80 -9 -19 0 -1.10 5.90 -19 9 0 -0.40 2.10 -19 11 0 1.60 6.80 -11 -19 0 3.10 6.10 19 -11 0 1.80 7.60 19 -13 0 8.70 8.80 -13 -19 0 5.60 6.60 -19 13 0 2.90 7.90 13 19 0 5.30 8.30 -15 -19 0 10.00 6.70 15 19 0 5.60 8.50 19 -15 0 3.80 9.10 -19 15 0 17.00 9.30 19 -17 0 4.60 9.80 -17 -19 0 0.30 6.30 19 19 0 17.90 9.20 19 -19 0 15.20 12.10 20 18 0 6.10 8.80 18 -20 0 17.60 12.10 20 16 0 153.68 14.00 16 -20 0 156.38 15.80 20 14 0 108.89 11.70 14 -20 0 125.09 13.70 12 -20 0 27.50 9.70 20 12 0 29.70 8.40 10 -20 0 6.10 8.40 8 -20 0 20.50 8.00 20 8 0 33.70 7.40 6 -20 0 57.29 9.80 20 6 0 58.49 8.50 20 4 0 9.60 5.90 4 -20 0 5.70 6.70 -20 -2 0 238.18 8.40 20 2 0 251.07 12.50 2 -20 0 221.78 13.10 -20 -2 0 231.68 7.70 -20 0 0 59.69 6.90 20 0 0 73.49 8.20 -20 0 0 65.19 6.00 0 -20 0 70.29 9.40 -20 2 0 214.28 9.00 20 -2 0 198.38 10.90 -2 -20 0 203.48 12.00 20 -4 0 104.49 9.40 20 -4 0 113.19 8.80 -4 -20 0 115.29 10.30 -20 4 0 117.59 7.70 -20 6 0 7.60 2.40 -6 -20 0 17.40 7.00 20 -6 0 17.60 6.80 -20 8 0 5.60 2.50 -20 8 0 7.70 7.20 -8 -20 0 9.50 6.90 20 -8 0 7.90 7.30 20 -10 0 24.10 8.50 -10 -20 0 26.30 7.60 -20 10 0 26.40 8.80 20 -12 0 10.00 9.00 12 20 0 9.60 8.80 -12 -20 0 7.10 7.00 -20 12 0 18.90 8.80 -14 -20 0 22.80 7.70 20 -14 0 8.60 9.30 -20 14 0 21.70 9.60 14 20 0 14.60 9.10 -16 -20 0 9.50 7.00 -20 16 0 22.10 11.10 16 20 0 21.90 9.90 20 -16 0 28.70 11.20 20 -18 0 147.39 15.40 20 -20 0 -1.60 12.10 20 20 0 4.70 9.10 21 19 0 7.40 8.90 19 -21 0 12.40 12.60 21 17 0 -0.20 8.60 17 -21 0 10.40 11.20 15 -21 0 4.30 10.00 21 15 0 8.80 8.10 21 13 0 9.50 7.70 13 -21 0 0.10 9.20 11 -21 0 8.20 8.70 9 -21 0 2.20 7.80 21 9 0 3.10 6.60 21 7 0 -10.00 5.70 7 -21 0 -4.50 7.60 21 5 0 7.70 6.50 5 -21 0 5.30 7.60 21 3 0 -2.10 5.90 3 -21 0 3.30 7.10 -21 -1 0 -1.10 1.90 -21 -1 0 5.00 3.70 1 -21 0 -3.40 6.90 21 -1 0 2.40 5.20 -21 1 0 0.90 1.90 -1 -21 0 -1.80 6.80 21 -3 0 5.90 6.00 -3 -21 0 6.40 7.10 -21 3 0 -0.20 1.90 21 -3 0 -4.40 5.20 -5 -21 0 3.20 7.00 -21 5 0 2.90 2.20 21 -5 0 2.40 6.10 -7 -21 0 -2.80 6.80 21 -7 0 4.10 6.90 -21 7 0 -0.20 2.30 -9 -21 0 -2.20 6.90 -21 9 0 -1.00 7.10 -21 9 0 0.70 2.60 21 -9 0 0.40 7.50 -21 11 0 2.60 2.80 -21 11 0 -0.10 7.50 21 -11 0 -3.40 8.30 -11 -21 0 4.90 7.00 21 -13 0 9.00 9.30 -13 -21 0 -0.70 7.30 13 21 0 -3.60 9.20 -21 13 0 2.00 3.10 -21 13 0 -7.70 7.90 21 -15 0 3.30 10.00 -15 -21 0 0.10 7.10 15 21 0 7.10 9.40 -21 15 0 -4.50 8.80 -21 17 0 7.90 10.90 21 -17 0 11.50 11.80 -17 -21 0 12.20 7.80 21 -19 0 -1.50 11.20 19 21 0 4.10 8.70 21 -21 0 2.40 11.50 21 21 0 9.50 8.40 22 20 0 21.60 9.70 20 -22 0 23.00 12.50 22 18 0 127.39 13.70 18 -22 0 127.69 15.70 16 -22 0 12.80 11.50 22 16 0 25.00 9.20 22 14 0 18.40 8.70 14 -22 0 22.10 11.20 12 -22 0 63.99 12.00 10 -22 0 158.08 14.30 22 10 0 155.48 12.50 8 -22 0 7.30 8.50 22 8 0 3.50 6.60 6 -22 0 6.60 8.30 22 6 0 -6.60 6.20 22 4 0 201.98 12.80 4 -22 0 203.78 14.00 -22 -2 0 68.99 6.30 2 -22 0 94.09 11.70 -22 -2 0 80.19 5.60 0 -22 0 24.60 8.40 22 0 0 28.10 6.80 -22 0 0 14.40 2.50 22 -2 0 0.40 5.50 -2 -22 0 4.70 7.50 -22 2 0 0.40 2.10 22 -4 0 28.00 7.30 -4 -22 0 33.40 8.90 -6 -22 0 -4.70 7.40 -22 6 0 -1.70 2.30 22 -6 0 2.40 7.10 22 -8 0 -8.80 7.50 -22 8 0 0.90 2.60 -8 -22 0 -7.40 7.20 -22 8 0 -2.70 6.90 -22 10 0 4.10 3.10 -10 -22 0 13.80 8.00 22 -10 0 9.90 8.80 -22 10 0 1.90 7.70 -12 -22 0 109.99 11.70 12 22 0 119.49 13.50 -22 12 0 122.59 11.00 -22 12 0 118.39 15.60 22 -12 0 128.69 14.00 -22 14 0 2.90 3.40 22 -14 0 2.30 10.30 14 22 0 12.10 10.00 -14 -22 0 13.40 7.90 -22 14 0 2.80 9.20 -16 -22 0 52.89 9.50 22 -16 0 45.30 12.80 16 22 0 59.39 12.30 -22 16 0 62.69 14.40 22 -18 0 0.10 11.60 20 22 0 -2.80 8.90 22 -20 0 11.00 11.60 22 -22 0 -0.70 11.70 22 22 0 8.60 8.60 21 -23 0 -9.20 11.10 23 21 0 6.60 8.60 19 -23 0 13.10 11.80 23 19 0 2.10 8.40 17 -23 0 8.90 12.30 23 17 0 17.40 9.00 15 -23 0 15.80 11.50 13 -23 0 0.10 10.80 23 11 0 -1.00 7.60 11 -23 0 2.40 9.60 23 9 0 11.70 7.70 9 -23 0 24.30 10.30 23 7 0 -5.60 6.70 7 -23 0 -1.50 8.70 23 5 0 5.80 6.70 5 -23 0 6.40 8.60 3 -23 0 6.30 8.50 1 -23 0 -4.40 7.70 23 1 0 -1.50 6.00 -23 -1 0 0.70 2.20 -23 1 0 2.40 2.20 23 -1 0 -1.10 5.60 -1 -23 0 -2.90 7.80 23 -3 0 9.90 6.30 -3 -23 0 9.50 8.20 -5 -23 0 -2.00 7.60 23 -5 0 2.50 7.00 -23 5 0 -0.40 2.30 -23 7 0 1.40 2.60 -7 -23 0 -0.70 7.90 23 -7 0 3.70 7.90 -9 -23 0 10.80 8.30 -23 9 0 6.10 8.40 -23 9 0 0.00 2.80 23 -9 0 0.00 8.40 -23 11 0 6.40 9.00 23 -11 0 10.60 9.60 -11 -23 0 -0.40 8.20 -23 11 0 6.80 3.40 23 -13 0 -2.10 9.80 13 23 0 9.00 10.20 -23 13 0 -2.50 3.20 -13 -23 0 8.40 8.20 -23 13 0 3.20 9.20 -15 -23 0 6.50 8.30 -23 15 0 4.70 3.80 -23 15 0 1.50 9.70 15 23 0 3.10 10.10 23 -15 0 3.90 10.80 -23 17 0 -2.80 11.40 23 -17 0 9.50 11.50 -23 17 0 4.90 3.90 17 23 0 3.80 10.20 23 -19 0 -9.60 10.70 -23 19 0 3.50 3.90 19 23 0 -11.70 7.80 -23 21 0 4.90 3.80 23 -21 0 5.50 11.50 21 23 0 -1.00 8.30 23 23 0 -4.00 8.70 -23 23 0 -2.70 3.60 23 -23 0 -1.90 12.40 22 -24 0 4.10 12.30 24 22 0 10.80 8.70 24 20 0 13.50 8.60 20 -24 0 6.30 11.60 24 18 0 50.39 10.80 18 -24 0 44.70 13.60 16 -24 0 103.49 15.30 14 -24 0 136.59 15.50 24 12 0 68.79 10.80 12 -24 0 59.89 13.10 10 -24 0 2.20 9.90 24 10 0 -1.00 7.40 8 -24 0 222.58 16.00 24 8 0 236.78 14.80 24 6 0 35.30 8.70 6 -24 0 30.30 10.50 4 -24 0 16.10 9.30 2 -24 0 -2.00 8.20 24 2 0 0.10 6.40 0 -24 0 62.19 11.20 -24 0 0 39.30 3.50 24 0 0 69.99 9.10 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39.50 6.70 -18 0 2 45.90 5.20 0 -18 2 29.10 7.30 -2 -18 -2 12.70 6.80 -18 2 -2 3.00 2.20 18 -2 -2 7.60 4.40 18 -2 2 12.50 5.20 -2 -18 2 1.80 5.90 -4 -18 -2 0.90 6.30 -18 4 -2 0.40 2.00 18 -4 -2 4.90 4.90 -18 4 2 1.80 6.10 -4 -18 2 6.30 6.40 6 18 -2 22.80 6.10 18 -6 -2 39.60 6.80 -6 -18 -2 23.70 7.30 -18 6 2 31.40 8.40 -6 -18 2 22.60 7.00 18 -6 2 24.20 5.50 -8 -18 -2 10.70 6.80 -18 8 -2 7.80 2.70 18 -8 -2 18.90 6.70 8 18 -2 15.30 6.40 18 -8 2 16.50 7.30 -8 -18 2 14.50 6.40 -18 8 2 5.60 7.30 18 -10 -2 8.10 7.00 -18 10 -2 2.20 2.50 -10 -18 -2 0.90 6.70 -10 -18 2 7.60 6.00 -18 10 2 0.70 6.80 18 -10 2 -3.60 7.30 12 18 -2 197.48 12.00 -12 -18 -2 180.88 11.50 18 -12 -2 190.78 13.10 -18 12 -2 187.38 13.90 12 18 -2 193.58 9.60 -18 12 -2 191.58 11.90 -18 12 2 185.58 16.10 -12 -18 2 193.98 11.10 18 -12 2 197.38 13.30 -18 14 -2 4.20 3.20 -14 -18 -2 10.10 7.00 -18 14 -2 7.40 7.10 14 18 -2 4.40 2.10 18 -14 -2 8.20 8.70 14 18 -2 16.70 6.80 18 -14 2 10.90 9.20 -14 -18 2 11.20 6.60 16 18 -2 87.09 10.20 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3.50 3.10 -13 -19 2 18.40 7.40 19 -13 2 13.10 9.20 -19 13 2 15.20 9.90 -19 15 -2 52.79 10.80 19 -15 -2 57.19 11.10 -15 -19 -2 54.39 8.90 15 19 -2 51.39 9.20 -15 -19 2 54.99 8.60 19 -15 2 57.29 12.00 17 19 -2 42.50 9.00 19 -17 -2 39.40 11.30 -17 -19 -2 49.00 8.80 -19 17 -2 45.20 11.20 17 19 2 49.90 12.20 19 -17 2 53.29 12.50 -17 -19 2 58.89 10.10 19 -19 -2 69.09 13.40 -19 19 -2 40.60 5.70 19 -19 2 65.59 14.00 19 19 2 62.09 12.80 18 -20 -2 17.70 11.70 20 18 -2 21.30 8.70 18 -20 2 22.70 12.10 20 18 2 26.20 11.00 20 16 -2 87.69 11.00 16 -20 -2 98.39 14.00 16 -20 2 85.89 13.90 -20 -14 -2 15.40 6.00 20 14 -2 25.00 8.20 14 -20 -2 8.70 10.00 -14 20 -2 6.80 3.40 14 -20 2 12.90 9.80 -20 -12 -2 41.60 6.40 20 12 -2 34.80 8.50 12 -20 -2 35.90 10.60 20 12 2 39.80 9.00 12 -20 2 49.30 10.70 20 10 -2 98.69 10.20 10 -20 -2 96.19 11.90 -20 -10 -2 83.09 7.40 10 -20 2 93.59 12.00 20 10 2 98.99 11.40 8 -20 -2 1.00 7.60 -20 -8 -2 1.90 5.30 8 -20 2 3.20 8.10 20 8 2 -1.30 6.60 20 8 2 -1.60 1.70 -20 -6 -2 5.90 6.10 -20 -6 -2 11.10 5.80 20 6 -2 11.00 5.90 6 -20 -2 9.50 7.60 6 -20 2 2.40 7.70 20 6 2 4.70 2.60 20 6 2 12.60 6.90 4 -20 -2 39.50 8.70 20 4 -2 50.69 7.40 4 -20 2 52.49 9.40 -20 -2 -2 -0.40 2.40 2 -20 -2 6.80 7.40 20 2 -2 8.60 5.50 2 -20 2 2.00 7.10 20 2 2 -3.60 5.70 -20 0 -2 7.30 2.60 0 -20 -2 8.50 7.20 20 0 -2 14.40 4.20 0 -20 2 3.10 7.40 -20 0 2 14.20 4.60 20 0 2 13.00 6.20 -20 0 2 6.30 1.50 -20 2 -2 4.80 2.50 20 -2 -2 15.30 5.00 -2 -20 -2 12.50 7.60 -2 -20 2 6.00 7.20 20 -2 2 11.60 6.10 20 -4 -2 52.19 7.00 -4 -20 -2 47.50 8.60 -4 -20 2 41.70 8.50 20 -4 2 39.90 6.60 -20 4 2 52.19 10.20 -6 -20 -2 3.70 7.40 20 -6 -2 15.00 6.60 -20 6 -2 5.10 2.70 -20 6 2 5.00 7.40 -6 -20 2 11.50 7.20 20 -6 2 13.80 5.60 -8 -20 -2 3.10 7.60 8 20 -2 6.60 6.80 -20 8 -2 1.60 2.60 20 -8 -2 -0.80 6.80 -20 8 2 -5.30 6.80 -8 -20 2 -3.70 6.90 20 -8 2 5.90 7.90 10 20 -2 28.80 8.30 20 -10 -2 39.80 9.10 -10 -20 -2 32.70 8.70 -10 -20 2 38.80 8.20 -20 10 2 30.10 10.10 20 -10 2 45.70 10.40 -12 -20 -2 54.39 9.60 20 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6.60 7.20 -21 7 -2 3.60 2.80 -7 -21 -2 -3.10 7.50 -7 -21 2 4.20 7.60 21 -7 2 6.00 5.80 -21 7 2 5.30 7.60 -9 -21 -2 12.90 8.00 21 -9 -2 14.20 8.00 -21 9 -2 4.40 3.00 9 21 -2 14.60 7.60 -9 -21 2 15.10 7.80 21 -9 2 8.30 8.90 -21 9 2 12.30 8.30 -21 11 -2 7.70 7.60 -21 11 -2 5.20 3.30 21 -11 -2 0.60 8.50 -11 -21 -2 2.20 7.80 21 -11 2 8.90 9.80 -11 -21 2 12.70 8.00 -21 11 2 9.30 9.40 -21 13 -2 30.10 9.30 -13 -21 -2 33.00 8.90 -21 13 -2 13.60 4.10 13 21 -2 23.70 7.80 21 -13 -2 29.10 10.00 21 -13 2 26.20 10.90 -21 13 2 30.50 11.60 -13 -21 2 32.30 8.50 15 21 -2 17.90 8.10 15 21 -2 2.70 2.50 -15 -21 -2 6.00 8.10 21 -15 -2 1.10 10.00 -21 15 -2 -0.90 3.40 -21 15 -2 1.90 8.20 21 -15 2 -4.70 10.80 -15 -21 2 14.50 8.20 -21 17 -2 13.70 10.30 17 21 -2 17.70 8.60 -21 17 -2 1.30 3.80 -17 -21 -2 7.10 8.10 21 -17 -2 6.20 11.20 21 -17 2 27.10 12.10 17 21 2 11.50 11.50 21 -19 -2 -1.20 10.70 -21 19 -2 3.60 4.00 21 -19 2 0.70 11.30 19 21 2 8.70 10.30 -21 21 -2 7.20 4.20 21 -21 -2 9.50 10.90 21 -21 2 11.00 12.50 21 21 2 14.30 10.50 22 20 -2 5.30 8.30 20 -22 -2 25.50 11.90 -20 22 -2 7.20 4.20 20 -22 2 15.90 12.60 22 18 -2 2.00 7.90 -18 22 -2 -0.40 3.70 18 -22 -2 -4.20 10.80 18 -22 2 0.20 11.30 22 16 -2 5.10 8.50 -16 22 -2 3.40 3.60 16 -22 -2 16.20 11.50 16 -22 2 1.60 10.70 22 16 2 22.60 10.10 22 14 -2 11.80 8.10 14 -22 -2 14.60 10.90 -14 22 -2 4.70 3.30 22 14 2 2.80 8.90 14 -22 2 9.10 10.50 12 -22 -2 16.60 10.30 22 12 -2 9.90 7.60 -12 22 -2 5.00 3.50 22 12 2 9.20 8.60 12 -22 2 11.60 10.10 22 10 -2 -12.10 6.50 10 -22 -2 5.40 9.30 10 -22 2 9.30 9.50 22 10 2 2.80 7.70 8 -22 -2 21.30 9.70 -22 -8 -2 29.90 6.10 22 8 2 26.90 8.40 8 -22 2 16.30 9.40 -22 -6 -2 2.80 6.00 22 6 -2 0.10 6.20 6 -22 -2 0.00 8.20 6 -22 2 -4.80 8.50 4 -22 -2 25.50 9.20 22 4 -2 14.80 6.50 22 4 2 22.10 7.70 4 -22 2 21.10 9.30 22 2 -2 22.70 6.80 -22 -2 -2 9.70 3.20 2 -22 -2 12.80 8.60 22 2 2 27.50 7.90 2 -22 2 40.80 9.60 -22 0 -2 3.00 2.90 22 0 -2 7.50 4.50 0 -22 -2 6.90 8.20 -22 0 2 2.40 1.50 -22 0 2 5.20 8.00 0 -22 2 6.60 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2.50 -5 2 3 25.30 6.00 -2 -5 3 27.10 3.40 -5 4 -3 7.00 2.10 5 -4 -3 6.50 5.90 4 5 -3 6.50 1.70 -4 -5 -3 19.60 6.90 -4 -5 3 7.10 1.60 5 -4 3 9.50 3.50 -5 6 -3 2.30 1.80 5 -6 -3 3.10 5.50 -6 -5 -3 5.60 6.20 6 5 -3 3.30 1.50 5 -6 3 5.20 2.30 -6 -5 3 1.80 1.30 6 3 -3 364.66 10.70 -6 -3 -3 358.46 13.20 3 -6 -3 355.16 13.00 -3 6 -3 363.66 11.70 -6 -3 3 364.36 12.80 -6 -3 3 367.66 10.40 6 1 -3 29.20 5.40 1 -6 -3 34.90 7.10 -1 6 -3 15.20 2.10 -6 -1 -3 22.00 2.80 -6 -1 3 31.40 5.50 1 6 -3 2.80 1.70 -1 -6 -3 6.30 6.80 6 -1 -3 3.10 5.20 -6 1 -3 1.90 2.00 -6 1 3 7.70 5.60 -1 -6 3 4.00 1.90 -1 -6 3 7.10 2.40 -6 1 3 9.10 4.70 3 6 -3 18.80 5.50 3 6 -3 10.20 1.90 -6 3 -3 11.20 2.30 -3 -6 -3 22.70 7.30 6 -3 -3 20.30 5.70 6 -3 3 20.60 4.20 -3 -6 3 23.90 2.90 -3 -6 3 9.70 1.80 -6 5 -3 72.69 6.30 -5 -6 -3 67.79 8.00 6 -5 -3 62.49 6.90 5 6 -3 71.69 4.40 5 6 -3 68.89 5.00 5 6 -3 68.79 5.60 -5 -6 3 72.09 4.80 6 -5 3 66.09 4.60 -5 -6 3 68.99 4.50 -7 -6 -3 49.50 7.00 6 -7 -3 48.10 6.40 -6 7 -3 47.90 4.30 7 6 -3 45.70 4.10 7 6 -3 46.00 4.50 7 6 -3 42.00 4.60 -7 -6 3 44.30 3.90 6 -7 3 54.39 7.00 7 4 -3 6.40 1.60 -7 -4 -3 20.50 6.30 -4 7 -3 4.50 1.80 4 -7 -3 11.30 5.60 4 -7 3 19.30 5.60 4 -7 3 10.30 1.80 -7 -4 3 8.40 1.50 -2 7 -3 304.57 10.50 -7 -2 -3 307.87 11.30 2 -7 -3 292.77 12.00 7 2 -3 284.47 9.80 -7 -2 3 299.87 9.30 2 -7 3 316.57 11.50 -7 -2 3 292.97 12.20 0 7 -3 90.39 5.80 7 0 -3 75.99 6.60 -7 0 -3 91.19 7.40 0 -7 -3 76.39 8.80 -7 0 3 72.19 7.10 -7 0 3 79.09 7.60 -2 -7 -3 1922.01 44.50 2 7 -3 1870.11 42.90 7 -2 -3 2018.30 43.20 -7 2 -3 1948.51 43.50 -7 2 3 2045.80 43.40 7 -2 3 1953.00 43.20 -7 2 3 1789.02 46.10 -2 -7 3 1810.72 40.70 -7 4 -3 206.68 8.90 -4 -7 -3 196.88 10.60 7 -4 -3 214.98 9.10 4 7 -3 200.18 7.70 4 7 -3 201.38 6.50 7 -4 3 204.98 7.50 -4 -7 3 187.48 6.70 6 7 -3 140.59 6.50 -7 6 -3 131.69 7.30 7 -6 -3 128.29 8.20 6 7 -3 132.39 6.10 -6 -7 -3 128.19 9.20 -7 6 -3 138.29 6.50 6 7 -3 137.29 5.80 7 -6 3 126.59 5.50 -6 -7 3 127.79 5.80 8 7 -3 23.50 3.70 7 -8 -3 31.70 6.40 -8 -7 -3 32.90 6.70 8 7 -3 26.70 4.00 7 -8 3 25.30 2.90 7 -8 3 30.90 6.10 8 5 -3 37.20 4.20 -8 -5 -3 47.90 6.80 -5 8 -3 37.90 3.50 8 5 -3 41.20 4.30 5 -8 -3 40.20 6.20 5 -8 3 45.20 6.60 -8 -5 3 40.40 3.70 8 3 -3 84.59 5.60 3 -8 -3 89.89 8.00 -3 8 -3 83.79 6.10 3 -8 3 90.09 7.40 -8 -3 3 90.59 5.00 -1 8 -3 153.78 7.60 8 1 -3 134.59 7.20 1 -8 -3 146.59 9.30 -8 -1 -3 148.89 7.90 1 -8 3 163.18 8.40 -8 -1 3 146.49 9.30 -8 1 -3 356.56 11.70 -1 -8 -3 325.47 13.00 8 -1 -3 365.46 11.30 1 8 -3 349.87 11.30 8 -1 3 364.66 12.10 -8 1 3 370.16 11.60 -8 1 3 316.87 13.70 -1 -8 3 334.77 11.80 -8 3 -3 8.30 2.10 -3 -8 -3 21.10 6.40 8 -3 -3 20.40 4.90 3 8 -3 18.30 2.40 -3 -8 3 14.10 3.10 -8 3 3 16.80 5.70 5 8 -3 829.72 21.00 8 -5 -3 910.21 22.40 -5 -8 -3 867.71 23.20 -8 5 -3 863.71 22.40 -8 5 -3 840.42 22.50 -7 -8 -3 89.59 8.10 7 8 -3 91.99 5.20 -8 7 -3 88.79 5.60 8 -7 -3 93.39 7.70 7 8 -3 90.49 5.50 -8 7 -3 92.29 6.80 8 -7 3 87.79 7.60 -7 -8 3 90.89 4.80 -9 -8 -3 84.29 8.10 9 8 -3 60.89 4.80 8 -9 -3 63.29 7.00 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9 -8 3 51.79 7.00 10 9 -3 209.78 7.40 -10 -9 -3 183.68 10.10 10 9 -3 193.48 7.30 -9 10 -3 196.18 9.60 10 9 -3 191.58 8.30 -9 10 -3 205.88 9.30 9 -10 -3 188.98 10.20 9 -10 3 202.38 10.80 10 7 -3 7.40 1.50 -10 -7 -3 14.90 5.90 -7 10 -3 14.20 2.80 10 7 -3 15.90 3.40 -7 10 -3 5.40 2.00 7 -10 -3 14.60 5.40 10 7 -3 11.50 3.60 -7 10 -3 13.80 3.80 7 -10 3 12.60 5.50 10 5 -3 18.00 3.80 -10 -5 -3 10.40 5.70 -5 10 -3 6.40 2.00 5 -10 -3 14.90 5.90 -10 -5 3 7.50 1.20 5 -10 3 20.90 5.60 10 3 -3 3.40 3.40 -3 10 -3 0.50 1.70 3 -10 -3 4.70 5.60 -10 -3 3 0.90 1.30 3 -10 3 2.10 4.70 1 -10 -3 50.29 7.20 10 1 -3 49.30 4.90 -1 10 -3 53.69 5.70 -10 -1 3 44.40 5.30 1 -10 3 55.29 6.70 -10 -1 3 53.19 7.30 10 1 3 46.50 6.20 -1 -10 -3 213.98 10.90 10 -1 -3 204.58 8.10 1 10 -3 211.58 8.80 -10 1 -3 210.08 9.20 -10 1 3 194.98 11.70 10 -1 3 213.68 10.00 -1 -10 3 221.88 9.90 -10 1 3 203.18 8.50 -3 -10 -3 29.90 6.60 3 10 -3 26.40 2.90 10 -3 -3 29.40 5.00 10 -3 3 28.70 4.60 -3 -10 3 32.20 5.60 -10 3 3 32.30 6.90 5 10 -3 145.59 7.00 -5 -10 -3 149.99 9.50 5 10 -3 146.09 5.90 -10 5 -3 156.98 8.00 10 -5 -3 146.79 7.90 -5 -10 3 150.48 7.80 -10 5 3 167.68 11.20 10 -5 3 148.09 6.90 -7 -10 -3 96.79 8.40 -10 7 -3 88.49 7.00 7 10 -3 88.19 5.50 10 -7 -3 101.09 7.70 7 10 -3 89.49 5.40 10 -7 3 97.89 8.50 -10 9 -3 450.55 15.00 -9 -10 -3 448.16 14.90 9 10 -3 428.06 12.30 9 10 -3 431.16 12.90 10 -9 -3 437.86 14.90 10 -9 3 421.76 15.40 11 10 -3 56.99 4.90 11 10 -3 47.40 4.60 11 10 -3 69.89 6.50 10 -11 -3 60.19 8.30 -10 11 -3 59.69 6.90 -11 -10 -3 57.89 7.80 10 -11 3 62.59 8.70 11 8 -3 31.30 3.60 8 -11 -3 23.10 6.40 -11 -8 -3 25.00 6.60 -8 11 -3 28.00 4.70 8 -11 3 29.30 6.70 -11 -6 -3 228.58 10.30 11 6 -3 221.08 7.00 11 6 -3 234.58 9.10 6 -11 -3 216.18 10.80 -6 11 -3 236.48 10.30 -11 -6 3 212.38 6.50 6 -11 3 217.78 10.70 -11 -4 -3 420.86 14.00 11 4 -3 424.16 13.10 4 -11 -3 427.76 15.20 11 4 -3 403.06 11.10 -4 11 -3 410.66 13.80 4 -11 3 414.16 14.50 -11 -4 3 412.66 10.60 -2 11 -3 1.30 1.60 2 -11 -3 2.10 5.50 11 2 -3 5.30 3.40 -11 -2 -3 0.70 2.00 2 -11 3 6.70 5.00 11 2 3 6.70 4.70 -11 0 -3 90.79 6.90 0 -11 -3 89.59 8.10 11 0 -3 89.69 5.60 0 11 -3 101.39 6.40 -11 0 3 90.99 9.00 -11 0 3 87.79 6.20 11 0 3 75.39 7.40 0 -11 3 93.69 7.40 -2 -11 -3 148.79 9.50 11 -2 -3 159.38 7.30 -11 2 -3 161.08 8.30 2 11 -3 164.98 8.00 -11 2 3 146.09 10.70 11 -2 3 164.28 8.20 -2 -11 3 163.38 8.90 -11 4 -3 492.15 14.90 -4 -11 -3 446.66 15.80 4 11 -3 505.05 14.40 11 -4 -3 485.55 14.40 -4 -11 3 481.65 14.80 -11 4 3 470.75 18.70 -6 -11 -3 54.79 7.50 6 11 -3 48.30 4.50 -11 6 -3 53.59 6.20 6 11 -3 55.89 5.10 11 -6 -3 63.79 7.00 11 -6 3 55.99 5.50 -11 6 3 56.79 8.50 -6 -11 3 57.39 6.40 8 11 -3 58.59 5.20 -11 8 -3 65.49 6.90 -8 -11 -3 74.59 8.20 8 11 -3 62.59 5.50 11 -8 -3 63.59 7.50 11 -8 3 64.89 5.20 -8 -11 3 54.09 6.20 11 -8 3 76.99 8.50 11 -10 -3 39.90 7.40 -10 -11 -3 34.40 7.00 10 11 -3 40.80 5.30 11 -10 3 37.00 7.80 12 11 -3 44.50 6.00 -12 -11 -3 27.90 7.10 -11 12 -3 35.70 6.20 11 -12 -3 36.70 7.70 12 11 -3 32.70 4.50 11 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23.70 4.70 13 6 -3 26.60 3.10 -13 -6 -3 34.10 6.30 13 6 -3 36.60 3.60 6 -13 -3 31.00 7.30 6 -13 3 24.80 6.30 13 6 3 26.10 6.50 4 -13 -3 271.07 12.60 -4 13 -3 304.57 12.00 13 4 -3 311.27 11.20 13 4 -3 282.37 8.10 4 -13 3 271.07 12.10 -13 -4 3 281.77 7.80 13 4 3 297.67 13.60 -2 13 -3 92.69 7.20 13 2 -3 82.79 4.80 -13 -2 -3 85.49 7.30 2 -13 -3 91.39 8.60 2 -13 3 85.59 8.20 13 2 3 79.39 8.70 -13 0 -3 3.00 2.10 0 13 -3 3.90 1.80 13 0 -3 15.60 3.60 0 -13 -3 13.10 6.10 -13 0 3 8.90 5.80 0 -13 3 5.50 5.20 -13 0 3 9.50 4.20 13 0 3 13.10 4.70 -13 2 -3 100.19 7.30 13 -2 -3 89.59 6.20 2 13 -3 102.49 6.90 -2 -13 -3 101.69 8.90 -2 -13 3 98.29 8.00 13 -2 3 102.69 7.50 -13 2 3 99.49 9.80 -4 -13 -3 257.97 12.10 13 -4 -3 271.87 10.50 4 13 -3 276.67 8.80 -13 4 -3 290.37 11.10 4 13 -3 298.97 10.80 -13 4 3 271.17 14.80 -4 -13 3 280.07 11.40 13 -4 3 301.07 10.90 6 13 -3 72.29 6.20 13 -6 -3 90.59 7.50 -6 -13 -3 75.89 8.80 6 13 -3 74.39 5.80 -13 6 -3 111.89 7.70 -13 6 3 84.79 10.40 13 -6 3 97.49 7.00 -6 -13 3 77.49 7.40 13 -8 -3 10.00 5.80 8 13 -3 4.80 1.80 -13 8 -3 5.40 2.30 -8 -13 -3 1.70 6.30 -13 8 3 8.70 6.80 13 -8 3 12.80 6.80 -8 -13 3 10.20 5.30 13 -8 3 15.30 3.90 10 13 -3 164.88 7.90 -10 -13 -3 178.98 11.00 -13 10 -3 157.98 10.00 10 13 -3 171.78 8.50 13 -10 -3 174.18 10.80 13 -10 3 163.28 11.20 -10 -13 3 163.58 8.80 -12 -13 -3 37.00 7.60 13 -12 -3 37.00 7.80 12 13 -3 43.10 6.30 -13 12 -3 33.20 6.90 13 -12 3 39.50 8.50 -13 14 -3 68.99 9.00 -14 -13 -3 79.79 8.80 14 13 -3 60.89 5.20 -13 14 -3 71.59 8.30 14 13 -3 74.29 7.80 13 -14 -3 65.09 9.50 13 -14 3 76.79 10.30 11 -14 -3 58.69 8.50 14 11 -3 58.89 5.00 -14 -11 -3 73.49 8.40 -11 14 -3 71.19 8.10 14 11 -3 61.99 7.30 14 11 -3 53.39 4.60 11 -14 3 62.89 9.20 9 -14 -3 70.39 9.10 14 9 -3 55.89 3.90 -14 -9 -3 59.79 7.70 9 -14 3 56.59 8.60 14 9 3 43.20 7.90 7 -14 -3 2.10 6.10 -14 -7 -3 0.00 5.90 -7 14 -3 -2.20 1.90 14 7 -3 -2.50 4.00 7 -14 3 0.90 6.10 14 7 3 0.50 5.80 5 -14 -3 3.80 6.50 -5 14 -3 1.60 1.90 -14 -5 -3 7.90 5.80 14 5 -3 2.10 4.00 5 -14 3 6.40 6.00 14 5 3 4.00 5.60 -14 -3 -3 7.00 2.40 -3 14 -3 9.40 2.40 14 3 -3 18.10 3.10 3 -14 -3 20.50 6.80 -14 -3 3 5.00 1.40 14 3 3 14.00 6.10 3 -14 3 19.40 6.10 14 1 -3 93.69 5.30 -14 -1 -3 97.79 7.50 1 -14 -3 86.39 8.90 -1 14 -3 89.99 7.40 -14 -1 3 93.99 6.00 1 -14 3 99.29 8.80 14 1 3 91.99 8.20 14 -1 -3 116.39 6.40 -14 1 -3 120.99 7.90 1 14 -3 113.59 5.70 -1 -14 -3 105.79 9.20 1 14 -3 129.19 7.90 -1 -14 3 119.29 8.60 -14 1 3 116.99 7.10 14 -1 3 113.59 8.50 -14 1 3 109.89 10.50 3 14 -3 11.90 2.30 14 -3 -3 26.80 5.10 -14 3 -3 12.90 2.60 -3 -14 -3 21.30 7.00 -3 -14 3 24.30 6.00 -14 3 3 24.10 7.20 -14 5 -3 2.90 2.10 5 14 -3 0.80 1.70 5 14 -3 5.30 3.40 14 -5 -3 4.50 4.90 -5 -14 -3 3.90 6.60 -5 -14 3 9.20 5.40 14 -5 3 1.80 4.20 -14 5 3 1.80 5.70 -14 7 -3 69.89 7.30 14 -7 -3 70.69 8.10 -7 -14 -3 76.59 9.20 7 14 -3 63.19 6.10 7 14 -3 68.49 6.30 -7 -14 3 66.19 7.40 14 -7 3 71.99 6.20 -14 7 3 79.49 10.90 14 -9 -3 59.59 8.00 9 14 -3 55.89 5.90 -9 -14 -3 64.99 8.40 14 -9 3 69.89 9.20 -14 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8.10 12 15 -3 16.60 2.40 -15 12 -3 24.60 7.00 -15 12 -3 19.60 3.60 -12 -15 -3 34.90 7.90 15 -12 3 36.10 9.30 -12 -15 3 33.20 6.30 -14 -15 -3 12.30 7.00 -15 14 -3 4.20 5.90 15 -14 -3 -2.60 7.40 14 15 -3 4.10 1.80 -15 14 -3 1.30 2.80 14 15 -3 1.50 5.40 15 -14 3 0.10 8.50 15 -16 -3 4.70 8.50 -15 16 -3 -0.10 2.90 16 15 -3 1.20 1.70 -16 -15 -3 10.90 7.30 -15 16 -3 1.30 6.50 16 15 -3 11.90 6.50 15 -16 3 6.70 8.90 16 15 3 -2.30 8.60 13 -16 -3 10.60 8.00 -13 16 -3 0.60 2.70 -16 -13 -3 8.70 6.90 16 13 -3 2.50 5.80 16 13 -3 8.10 4.10 16 13 3 0.80 7.90 13 -16 3 4.80 7.70 -16 -11 -3 79.79 8.50 16 11 -3 84.89 8.50 11 -16 -3 81.89 10.00 -11 16 -3 79.39 9.10 16 11 3 71.49 10.20 11 -16 3 78.79 10.40 9 -16 -3 5.00 6.50 -9 16 -3 -0.80 2.10 -16 -9 -3 1.20 6.10 16 9 3 3.60 6.80 9 -16 3 -2.70 6.50 -16 -7 -3 30.10 7.00 7 -16 -3 30.00 8.30 16 7 -3 30.40 5.80 -7 16 -3 30.20 3.60 16 7 3 18.90 7.00 7 -16 3 25.70 7.50 -16 -5 -3 67.89 8.00 16 5 -3 75.39 7.50 5 -16 -3 75.19 9.60 5 -16 3 59.79 8.40 3 -16 -3 20.30 7.30 -16 -3 -3 5.20 2.60 -3 16 -3 4.10 2.20 3 -16 3 10.00 3.40 16 3 3 8.40 5.50 3 -16 3 12.10 6.50 1 -16 -3 203.88 12.40 -1 16 -3 206.18 10.60 -16 -1 -3 215.88 10.20 16 1 -3 201.38 7.30 1 -16 3 195.48 11.20 -16 -1 3 190.48 8.00 16 1 3 212.18 10.90 1 16 -3 2.50 2.10 16 -1 -3 5.40 4.00 -16 1 -3 1.30 2.20 -1 -16 -3 4.90 6.50 -16 1 3 4.60 6.40 16 -1 3 -0.70 4.80 -16 1 3 1.10 5.70 -1 -16 3 12.50 6.30 3 16 -3 58.89 5.60 16 -3 -3 63.19 6.60 -3 -16 -3 52.99 8.50 -3 -16 3 59.59 8.10 -16 3 3 58.39 9.60 16 -3 3 57.59 7.10 -5 -16 -3 243.48 12.70 -16 5 -3 251.87 11.40 16 -5 -3 240.48 10.50 5 16 -3 256.57 10.90 -5 -16 3 242.88 11.80 -16 5 3 245.08 15.50 16 -5 3 243.88 10.90 16 -7 -3 112.69 8.60 7 16 -3 113.29 7.90 -7 -16 -3 101.89 10.30 -16 7 -3 128.39 8.90 7 16 -3 112.49 7.50 16 -7 3 97.79 7.60 -7 -16 3 126.69 9.50 -16 7 3 110.89 12.30 9 16 -3 282.97 11.10 -9 -16 -3 276.17 13.90 9 16 -3 287.77 11.40 16 -9 -3 272.27 12.60 -16 9 -3 274.97 12.80 -9 -16 3 267.47 12.20 16 -9 3 286.37 14.40 16 -9 3 265.87 11.40 -16 9 3 300.87 17.70 16 -11 -3 -4.50 6.20 -16 11 -3 0.40 2.50 -11 -16 -3 10.40 7.20 11 16 -3 0.80 1.90 -16 11 3 6.30 8.20 -11 -16 3 8.70 5.80 16 -11 3 3.80 7.60 -16 13 -3 3.80 3.00 16 -13 -3 11.00 8.10 -16 13 -3 15.20 6.60 13 16 -3 9.90 2.20 -13 -16 -3 11.10 7.40 16 -13 3 12.90 8.80 -13 -16 3 16.00 6.20 15 16 -3 30.00 7.50 16 -15 -3 27.40 9.60 -16 15 -3 34.50 8.50 -15 -16 -3 32.90 8.30 16 -15 3 22.00 9.90 -17 -16 -3 8.40 7.60 16 -17 -3 -2.90 8.70 17 16 -3 12.00 7.10 17 16 -3 3.80 1.90 -16 17 -3 7.40 7.40 -16 17 -3 2.50 3.30 16 -17 3 11.40 9.90 17 16 3 15.70 10.20 17 14 -3 75.59 9.20 17 14 -3 63.99 5.30 -17 -14 -3 82.99 9.20 14 -17 -3 77.29 11.70 14 -17 3 71.59 11.40 17 14 3 69.89 11.80 12 -17 -3 9.00 8.00 -17 -12 -3 6.20 6.50 17 12 -3 6.10 5.80 -12 17 -3 3.10 2.90 12 -17 3 -1.70 7.70 17 12 3 13.20 8.60 -17 -10 -3 115.99 9.10 10 -17 -3 122.69 11.00 -10 17 -3 125.79 9.90 17 10 3 120.19 12.90 10 -17 3 114.69 11.10 -8 17 -3 -0.10 2.20 8 -17 -3 6.50 6.80 17 8 -3 5.10 4.80 -17 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4.80 7.20 10 17 -3 6.00 5.00 10 17 -3 2.90 2.00 -17 10 -3 1.80 2.60 17 -10 3 -1.20 7.70 -17 10 3 6.80 7.80 -10 -17 3 3.30 6.20 -17 12 -3 70.99 9.50 -12 -17 -3 71.59 9.60 17 -12 -3 67.39 10.10 12 17 -3 57.39 6.70 17 -12 3 81.19 11.50 -12 -17 3 64.59 8.30 -17 14 -3 13.50 7.20 17 -14 -3 13.30 9.00 -17 14 -3 6.70 3.30 -14 -17 -3 14.30 7.80 14 17 -3 5.90 2.20 -14 -17 3 8.20 6.50 17 -14 3 8.00 10.20 17 -16 -3 76.59 12.10 16 17 -3 65.09 9.30 -16 -17 -3 78.49 9.80 16 17 -3 63.89 6.70 -17 16 -3 68.89 10.70 17 -16 3 75.59 12.90 -18 -17 -3 -1.30 7.30 -17 18 -3 6.80 8.30 -17 18 -3 3.20 3.40 17 -18 -3 -2.30 9.60 18 17 -3 13.40 7.60 18 17 3 10.30 10.00 17 -18 3 3.30 11.00 18 15 -3 45.40 8.30 -18 -15 -3 45.10 8.50 15 -18 -3 37.40 10.70 15 -18 3 43.60 11.10 18 15 3 44.40 10.90 13 -18 -3 1.40 8.50 -13 18 -3 3.20 3.10 18 13 -3 2.00 6.40 -18 -13 -3 2.10 6.90 13 -18 3 1.70 8.70 18 13 3 5.50 8.70 -18 -11 -3 21.50 7.00 -11 18 -3 9.00 3.10 11 -18 -3 13.60 8.60 11 -18 3 3.00 8.00 18 11 3 10.90 8.00 18 9 -3 13.50 5.70 9 -18 -3 15.80 7.90 -9 18 -3 7.40 2.90 -18 -9 -3 18.60 6.90 9 -18 3 18.60 8.00 18 9 3 5.90 7.10 -18 -7 -3 64.39 8.30 18 7 -3 64.59 7.50 7 -18 -3 52.19 9.50 7 -18 3 56.89 9.20 5 -18 -3 50.59 9.30 -18 -5 -3 41.20 7.60 18 5 -3 44.70 6.70 5 -18 3 29.00 7.60 18 5 3 38.30 7.50 5 -18 3 52.39 5.60 -18 -3 -3 3.10 2.70 3 -18 -3 15.70 7.50 -3 18 -3 6.30 2.40 3 -18 3 11.60 6.80 3 -18 3 0.70 3.80 18 3 3 7.70 6.00 -1 18 -3 4.80 2.40 18 1 -3 17.20 3.60 1 -18 -3 11.40 7.50 -18 -1 -3 7.50 2.70 -18 -1 3 7.80 4.40 1 -18 3 20.10 6.80 18 1 3 13.40 6.00 -18 1 -3 16.70 3.00 18 -1 -3 39.00 5.00 1 18 -3 20.60 3.30 -1 -18 -3 39.80 8.80 -1 -18 3 34.10 7.30 -3 -18 -3 43.00 9.00 18 -3 -3 48.50 6.20 3 18 -3 43.30 5.80 18 -3 3 42.50 7.20 -3 -18 3 40.70 7.90 -18 3 3 43.90 9.40 -5 -18 -3 -0.50 6.90 -18 5 -3 3.40 2.50 5 18 -3 2.80 4.80 5 18 -3 -0.40 2.00 18 -5 -3 -0.60 5.10 -5 -18 3 0.30 6.10 -18 5 3 -0.20 6.40 18 -5 3 4.00 5.30 18 -7 -3 2.50 5.90 7 18 -3 1.80 2.00 -7 -18 -3 6.20 7.60 7 18 -3 2.10 4.60 -18 7 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2.20 3.90 -18 -19 -3 5.50 8.00 18 19 -3 1.40 7.40 19 -18 3 6.80 12.10 18 19 3 8.30 11.20 19 -20 -3 20.60 11.70 -19 20 -3 11.00 4.60 20 19 -3 25.90 9.00 19 -20 3 31.90 13.20 20 19 3 27.20 12.00 17 -20 -3 16.80 11.70 -20 -17 -3 32.30 11.00 -17 20 -3 12.40 4.10 20 17 -3 17.30 8.40 20 17 3 23.60 11.40 17 -20 3 25.00 12.10 15 -20 -3 75.49 12.90 -20 -15 -3 82.09 9.50 20 15 -3 84.49 10.80 15 -20 3 71.89 12.90 20 15 3 80.19 13.50 -20 -13 -3 13.70 7.20 -13 20 -3 5.70 3.40 13 -20 -3 13.40 10.10 20 13 -3 9.00 7.50 13 -20 3 3.50 9.40 20 13 3 13.90 9.00 -11 20 -3 4.30 3.10 -20 -11 -3 18.40 7.20 11 -20 -3 16.10 9.20 11 -20 3 3.80 8.50 20 9 -3 -1.80 5.90 -20 -9 -3 -2.90 6.70 -9 20 -3 0.30 2.70 9 -20 -3 0.90 8.10 20 9 3 -0.70 6.90 9 -20 3 -0.60 8.30 -20 -7 -3 16.10 7.40 -7 20 -3 7.40 2.90 20 7 -3 18.70 6.20 7 -20 -3 18.50 8.50 20 7 3 16.20 7.50 7 -20 3 13.20 8.10 -5 20 -3 3.70 2.60 5 -20 -3 8.80 7.90 -20 -5 -3 10.40 6.80 20 5 -3 6.60 5.90 5 -20 3 3.10 7.00 20 5 3 8.00 6.80 3 -20 -3 165.78 12.90 -3 20 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2.80 -6 -21 -3 15.90 8.70 21 -6 -3 8.60 6.90 21 -6 3 11.60 5.90 -6 -21 3 19.90 8.50 -21 6 3 13.30 8.70 8 21 -3 8.50 2.90 -21 8 -3 9.30 3.30 -8 -21 -3 8.10 8.70 21 -8 -3 13.90 7.90 -21 8 3 12.40 9.40 -8 -21 3 19.50 8.50 21 -8 3 5.10 5.80 10 21 -3 51.89 8.00 -10 -21 -3 42.10 9.90 21 -10 -3 55.99 10.20 -10 -21 3 50.89 9.80 -21 10 3 46.00 12.00 -21 12 -3 1.00 3.30 21 -12 -3 7.70 8.90 -12 -21 -3 10.20 8.60 12 21 -3 16.20 7.20 12 21 -3 3.90 2.70 -21 12 3 0.10 10.20 21 -12 3 8.00 10.40 -12 -21 3 12.20 8.30 21 -14 -3 18.60 10.60 -21 14 -3 -0.90 7.20 14 21 -3 8.90 7.30 -21 14 -3 3.50 3.60 14 21 -3 3.60 2.50 -14 -21 -3 5.10 8.40 21 -14 3 10.80 11.40 -14 -21 3 2.40 8.00 -21 16 -3 0.00 3.80 -21 16 -3 0.10 8.20 16 21 -3 2.60 2.70 21 -16 -3 1.00 10.50 -16 -21 -3 8.20 8.80 21 -16 3 12.00 12.30 -16 -21 3 12.30 10.90 -21 18 -3 16.30 10.00 -21 18 -3 9.40 4.30 18 21 -3 25.30 8.70 21 -18 -3 6.20 11.80 -18 -21 -3 21.60 8.70 21 -18 3 10.90 12.30 18 21 3 8.90 11.30 21 -20 -3 14.00 11.20 -21 20 -3 8.30 4.40 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8.80 3.20 3 -22 -3 11.50 8.80 3 -22 3 16.70 8.50 1 -22 -3 27.30 9.40 -1 22 -3 9.20 3.10 -22 -1 -3 8.90 3.60 22 1 -3 16.20 4.30 1 -22 3 18.70 8.50 22 1 3 10.10 7.20 22 -1 -3 31.10 5.70 1 22 -3 15.00 3.40 -1 -22 -3 34.40 9.90 -22 1 -3 17.90 3.90 -1 -22 3 34.50 9.10 22 -1 3 27.20 8.00 3 22 -3 10.70 3.20 22 -3 -3 29.30 6.70 -3 -22 -3 24.30 10.00 -22 3 -3 14.60 3.70 -3 -22 3 19.10 8.60 -22 3 3 16.40 8.80 22 -3 3 13.70 7.40 -5 -22 -3 70.29 11.30 22 -5 -3 61.59 8.60 5 22 -3 72.99 8.80 -22 5 3 66.49 12.40 -5 -22 3 61.19 10.30 22 -5 3 55.59 8.00 -7 -22 -3 33.30 10.10 7 22 -3 17.10 3.50 22 -7 -3 27.50 8.40 -22 7 -3 17.30 3.80 -7 -22 3 37.90 9.70 22 -7 3 27.60 6.80 -22 7 3 31.00 10.40 22 -9 -3 -5.20 7.90 -9 -22 -3 3.50 8.90 9 22 -3 1.70 2.70 -22 9 -3 -0.90 3.20 9 22 -3 2.90 6.30 -9 -22 3 -2.60 8.40 -22 9 3 1.50 8.50 22 -11 -3 -0.30 8.70 11 22 -3 1.90 2.70 11 22 -3 11.90 6.90 -22 11 -3 0.50 3.40 -11 -22 -3 10.60 9.00 -11 -22 3 11.70 8.80 -22 11 3 10.30 10.50 -13 -22 -3 3.50 8.70 13 22 -3 -0.50 2.60 13 22 -3 14.90 7.50 -22 13 -3 2.00 3.70 22 -13 -3 1.00 9.90 -22 13 -3 12.00 8.30 -13 -22 3 11.40 9.10 -22 13 3 -1.50 10.50 22 -13 3 -6.90 10.90 22 -15 -3 79.99 13.30 -15 -22 -3 69.19 11.20 -22 15 -3 84.59 13.00 22 -15 3 96.69 15.30 -15 -22 3 85.69 11.00 -22 17 -3 103.39 15.10 -17 -22 -3 102.09 12.00 22 -17 -3 116.59 15.00 22 -17 3 114.99 16.40 -22 19 -3 2.50 4.00 22 -19 -3 11.40 11.00 19 22 -3 5.10 7.90 -22 19 -3 -11.60 8.50 22 -19 3 9.40 12.70 19 22 3 5.10 10.80 21 22 -3 24.30 8.90 22 -21 -3 0.40 10.90 -22 21 -3 2.30 4.10 22 -21 3 1.70 12.70 21 22 3 3.30 10.40 -22 23 -3 4.20 4.30 22 -23 -3 3.10 11.80 23 22 -3 15.30 8.70 22 -23 3 14.60 13.30 23 22 3 9.90 10.30 20 -23 -3 1.10 11.20 -20 23 -3 3.40 4.00 23 20 -3 1.80 7.60 20 -23 3 -7.50 11.30 -18 23 -3 7.40 4.10 18 -23 -3 27.20 12.00 23 18 -3 14.20 8.40 18 -23 3 11.30 12.20 16 -23 -3 89.19 14.30 -16 23 -3 47.30 6.30 23 16 -3 76.59 11.20 16 -23 3 76.09 14.60 14 -23 -3 87.59 14.60 14 -23 3 87.99 14.80 23 14 3 82.19 12.40 23 12 -3 7.10 7.80 12 -23 -3 7.40 10.40 -12 23 -3 2.40 3.40 12 -23 3 6.40 10.60 23 12 3 -6.00 8.10 -10 23 -3 -2.90 2.90 23 10 -3 -5.50 6.80 10 -23 -3 5.70 10.00 10 -23 3 4.20 9.30 23 10 3 8.60 9.00 8 -23 -3 29.50 10.50 23 8 -3 29.20 8.00 -8 23 -3 18.10 4.20 -23 -8 -3 37.50 8.50 8 -23 3 31.30 10.00 23 8 3 33.00 10.00 -6 23 -3 11.50 3.60 -23 -6 -3 25.00 8.10 6 -23 -3 23.10 9.80 23 6 -3 26.80 7.80 6 -23 3 24.00 10.00 23 6 3 26.60 8.40 4 -23 -3 -1.30 8.20 -4 23 -3 0.60 2.80 23 4 -3 1.80 6.40 4 -23 3 -3.10 8.00 -2 23 -3 4.40 3.00 2 -23 -3 0.60 8.60 -23 -2 -3 7.00 3.60 23 2 3 9.90 7.50 2 -23 3 10.20 8.50 -23 0 -3 4.70 3.60 0 -23 -3 24.80 9.80 0 23 -3 8.20 3.20 23 0 -3 18.40 5.00 0 -23 3 7.80 8.50 -23 0 3 10.90 1.90 23 0 3 6.10 7.30 -2 -23 -3 -7.20 8.30 23 -2 -3 3.70 5.60 -23 2 -3 5.40 3.30 2 23 -3 3.90 2.90 -2 -23 3 10.40 8.50 -23 2 3 3.90 8.10 23 -2 3 -2.10 7.10 4 23 -3 1.30 2.70 23 -4 -3 0.30 6.20 -23 4 -3 2.20 3.30 -4 -23 -3 3.80 9.40 4 23 -3 5.20 6.60 -23 4 3 2.20 8.50 -4 -23 3 8.10 8.60 6 23 -3 41.80 8.30 6 23 -3 23.30 3.90 -23 6 -3 21.10 4.10 23 -6 -3 31.70 8.60 -6 -23 -3 50.69 11.30 -23 6 3 37.00 11.00 23 -6 3 27.40 6.90 -6 -23 3 42.40 10.00 23 -8 -3 2.00 8.00 -8 -23 -3 10.50 9.60 -23 8 -3 2.30 3.30 8 23 -3 -1.10 2.80 23 -8 3 -5.80 5.70 -23 8 3 -6.50 8.10 -8 -23 3 -1.80 8.70 23 -10 -3 27.60 9.60 10 23 -3 24.80 7.80 -10 -23 -3 32.20 10.50 -23 10 -3 13.30 4.10 10 23 -3 13.20 3.50 -10 -23 3 21.30 9.80 -23 10 3 14.80 10.60 23 -12 -3 0.70 9.60 -23 12 -3 3.50 3.90 -12 -23 -3 4.50 9.30 12 23 -3 11.00 7.70 12 23 -3 2.30 2.90 -23 12 3 14.20 11.50 -12 -23 3 7.60 9.40 14 23 -3 127.49 13.00 -23 14 -3 135.29 13.70 -23 14 -3 127.09 14.90 23 -14 -3 134.79 15.40 -14 -23 -3 114.59 13.50 14 23 -3 125.09 11.00 -14 -23 3 123.29 13.60 23 -14 3 143.89 16.50 -23 14 3 133.69 19.90 23 -16 -3 11.30 11.10 -16 -23 -3 7.80 9.20 -23 16 -3 3.30 4.10 -23 16 -3 -0.10 8.50 23 -16 3 1.20 12.00 -23 18 -3 0.30 9.30 23 -18 -3 6.50 10.60 -23 18 -3 1.40 4.20 18 23 -3 2.70 7.60 23 -18 3 5.50 12.30 18 23 3 7.10 10.80 -23 20 -3 2.50 4.30 23 -20 -3 6.80 10.90 20 23 -3 -0.60 7.90 -23 20 -3 -7.00 10.10 23 -20 3 5.60 12.00 20 23 3 4.10 10.60 22 23 -3 6.70 8.50 -23 22 -3 7.20 4.60 23 -22 -3 19.20 12.50 22 23 3 18.20 11.50 23 -22 3 4.90 13.70 23 -24 -3 5.80 12.20 -23 24 -3 7.70 4.90 24 23 -3 6.80 8.90 23 -24 3 -8.60 13.50 21 -24 -3 14.70 12.40 24 21 -3 11.20 8.60 -21 24 -3 1.90 4.20 21 -24 3 -6.50 12.40 -19 24 -3 4.10 4.00 24 19 -3 12.10 8.30 19 -24 -3 35.00 12.50 19 -24 3 21.80 13.10 17 -24 -3 26.00 11.80 24 17 -3 22.30 9.10 -17 24 -3 12.60 4.40 24 17 3 26.10 10.20 17 -24 3 29.00 12.50 15 -24 -3 43.80 12.60 24 15 3 29.00 10.40 15 -24 3 38.60 13.00 13 -24 -3 0.40 11.50 -13 24 -3 5.80 3.70 13 -24 3 22.20 11.50 24 13 3 15.90 10.20 24 11 -3 10.50 8.20 -11 24 -3 4.10 3.70 11 -24 -3 13.30 10.80 24 11 3 3.30 8.90 11 -24 3 7.10 10.60 9 -24 -3 13.60 10.70 -9 24 -3 6.60 3.30 24 9 -3 14.60 7.90 9 -24 3 2.40 9.70 24 9 3 8.40 9.20 7 -24 -3 -9.00 9.10 -7 24 -3 0.80 3.00 24 7 -3 0.50 6.80 7 -24 3 9.20 9.40 24 7 3 7.30 8.10 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6.30 -8 2 -4 9.30 2.40 8 -2 -4 10.80 5.30 -2 -8 -4 17.10 6.90 2 8 -4 5.60 1.90 -2 -8 4 17.90 3.20 -8 2 4 10.70 5.70 8 -4 -4 177.38 9.40 4 8 -4 171.18 7.90 -4 -8 -4 178.18 10.50 -8 4 -4 180.28 9.20 -4 -8 4 174.38 7.70 8 -4 4 176.48 8.30 -6 -8 -4 54.79 8.40 6 8 -4 44.40 5.20 8 -6 -4 57.49 7.30 8 -6 4 51.29 4.60 8 8 -4 100.49 6.30 -8 8 -4 96.99 7.30 -8 -8 -4 110.79 9.60 8 -8 -4 107.09 8.70 8 -8 4 95.59 5.20 -9 -7 -4 170.58 10.40 9 7 -4 164.28 7.40 7 -9 -4 156.68 9.60 -7 9 -4 156.38 8.70 9 7 -4 168.48 8.50 7 -9 4 147.29 5.60 -9 -7 4 170.98 7.10 -5 9 -4 13.90 2.40 9 5 -4 14.40 2.10 5 -9 -4 24.30 6.70 -9 -5 -4 31.40 7.00 -9 -5 4 14.90 1.90 9 3 -4 30.40 5.10 -3 9 -4 11.60 2.30 3 -9 -4 25.40 7.00 -9 -3 4 24.40 5.70 -9 -3 4 13.70 2.00 -9 -1 -4 446.56 14.70 1 -9 -4 454.85 15.90 9 1 -4 430.26 13.40 -1 9 -4 456.05 14.40 -9 -1 4 445.86 16.80 9 -1 -4 69.79 6.90 -1 -9 -4 70.19 8.60 -9 1 -4 81.59 7.50 1 9 -4 73.39 5.90 -9 1 4 69.69 8.40 -3 -9 -4 14.30 6.60 -9 3 -4 8.60 2.30 3 9 -4 9.50 2.10 9 -3 -4 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3 4 324.77 14.80 -13 -1 -4 80.99 7.70 -1 13 -4 73.29 7.20 1 -13 -4 79.69 9.30 13 1 -4 65.69 6.40 1 -13 4 75.99 8.80 13 1 4 77.89 8.30 -13 -1 4 72.79 9.50 -13 1 -4 6.00 2.50 1 13 -4 5.00 2.00 13 -1 -4 11.40 5.00 -1 -13 -4 14.20 6.90 -13 1 4 11.10 6.40 -1 -13 4 14.60 6.20 13 -3 -4 309.77 11.80 3 13 -4 343.67 12.50 -13 3 -4 343.77 13.10 -3 -13 -4 309.27 14.20 13 -3 4 343.77 12.70 -3 -13 4 329.67 13.30 -13 3 4 322.57 16.50 13 -5 -4 95.39 8.10 -5 -13 -4 78.19 9.90 -13 5 -4 83.09 8.00 5 13 -4 80.49 7.10 -13 5 4 81.59 10.60 -5 -13 4 84.09 8.40 13 -7 -4 674.33 20.00 -13 7 -4 664.23 20.30 -7 -13 -4 643.24 20.90 7 13 -4 655.93 18.80 13 -7 4 662.63 18.20 -13 7 4 653.93 25.10 -9 -13 -4 89.89 10.20 13 -9 -4 116.09 9.10 -13 9 -4 106.79 9.10 9 13 -4 110.19 7.20 13 -9 4 108.89 6.80 -11 -13 -4 211.38 12.60 13 -11 -4 204.18 11.90 11 13 -4 175.68 8.60 -13 11 -4 178.48 11.30 13 -11 4 203.58 13.40 13 -13 -4 19.40 8.00 13 13 -4 4.80 1.90 -13 13 -4 4.30 2.80 -13 13 -4 9.80 5.20 -13 -13 -4 10.10 7.50 13 -13 4 11.40 8.10 14 12 -4 59.29 6.40 12 -14 -4 52.09 9.90 -12 14 -4 30.90 4.00 14 12 -4 29.90 2.80 -14 -12 -4 63.29 9.10 12 -14 4 50.99 9.40 -14 -10 -4 11.50 7.60 14 10 -4 7.80 4.70 14 10 -4 6.50 1.90 14 10 -4 17.80 4.00 -10 14 -4 16.80 5.00 10 -14 -4 20.30 7.80 -10 14 -4 10.20 2.90 10 -14 4 20.60 8.30 14 8 -4 22.60 3.80 8 -14 -4 14.90 7.40 -14 -8 -4 5.90 7.20 14 8 -4 22.70 4.90 -8 14 -4 11.00 2.90 8 -14 4 22.80 7.90 -14 -6 -4 25.00 7.60 14 6 -4 34.50 4.90 6 -14 -4 31.70 7.90 14 6 4 35.20 7.90 6 -14 4 38.90 8.30 -4 14 -4 0.90 2.10 4 -14 -4 -0.20 6.60 14 4 -4 5.50 4.00 14 4 4 6.60 6.30 -14 -4 4 -0.40 1.50 4 -14 4 1.60 6.50 -2 14 -4 25.70 3.30 -14 -2 -4 33.90 3.70 2 -14 -4 68.09 9.30 14 2 4 65.29 8.30 -14 -2 4 60.29 9.00 2 -14 4 63.99 8.60 -14 -2 4 31.70 2.70 -14 0 -4 2.20 2.60 0 14 -4 5.10 2.20 0 -14 -4 10.20 6.90 14 0 -4 14.90 4.90 -14 0 4 8.00 5.70 0 -14 4 9.50 6.30 -14 2 -4 105.79 8.70 14 -2 -4 94.29 7.40 -2 -14 -4 93.29 10.50 2 14 -4 99.79 7.70 14 -2 4 117.29 9.00 -14 2 4 84.69 10.30 -2 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35.00 6.50 11 -15 4 29.20 8.90 9 -15 -4 1.40 7.20 -9 15 -4 4.00 2.50 -15 -9 -4 1.00 7.20 15 9 -4 5.50 3.20 15 9 -4 2.60 4.40 -9 15 -4 0.80 2.80 9 -15 4 -7.10 6.90 15 7 -4 4.90 4.50 -7 15 -4 -3.00 2.10 15 7 -4 -2.10 3.00 -7 15 -4 -1.10 2.30 7 -15 -4 2.90 6.80 15 7 -4 2.60 3.90 -15 -7 -4 -5.30 6.70 15 7 4 -0.70 6.10 -15 -7 4 -0.30 1.00 7 -15 4 -3.70 6.40 5 -15 -4 65.59 9.30 -15 -5 -4 63.39 8.80 15 5 -4 56.99 5.20 -15 -5 4 52.69 4.40 15 5 4 54.19 8.40 5 -15 4 57.29 8.80 3 -15 -4 4.10 7.00 15 3 -4 12.90 4.00 3 -15 4 17.30 7.20 15 3 4 10.50 6.60 15 1 -4 84.69 6.20 -1 15 -4 93.09 8.20 1 -15 -4 90.89 10.50 -15 -1 -4 87.99 8.70 -15 -1 4 90.79 10.40 1 -15 4 79.29 9.70 -1 -15 -4 38.90 8.50 15 -1 -4 41.70 5.70 -15 1 4 45.90 8.80 -1 -15 4 50.69 8.30 15 -1 4 44.40 6.80 3 15 -4 12.20 2.80 -3 -15 -4 14.50 7.50 -15 3 -4 7.10 2.80 3 15 -4 9.00 2.40 15 -3 -4 14.20 5.20 -3 -15 4 15.90 6.70 -15 3 4 9.80 6.50 15 -3 4 15.70 5.30 -5 -15 -4 25.50 8.20 15 -5 -4 21.20 6.10 -15 5 -4 11.90 2.90 5 15 -4 25.70 3.80 5 15 -4 17.30 2.80 -5 -15 4 25.60 7.00 -15 5 4 28.80 8.40 15 -5 4 30.00 6.00 -15 7 -4 7.60 2.80 15 -7 -4 14.80 6.20 -7 -15 -4 5.20 7.80 7 15 -4 15.80 3.90 7 15 -4 3.90 2.10 -7 -15 4 14.30 6.40 -15 7 4 8.90 7.40 15 -7 4 16.80 5.10 9 15 -4 63.19 6.40 -15 9 -4 82.59 8.80 15 -9 -4 87.19 9.60 9 15 -4 65.39 6.80 -9 -15 -4 71.39 10.10 15 -9 4 65.49 6.20 11 15 -4 365.06 12.80 -15 11 -4 369.56 15.70 -11 -15 -4 386.96 16.20 15 -11 -4 357.96 15.80 11 15 -4 362.86 13.10 13 15 -4 3.60 5.10 -13 -15 -4 7.10 8.10 15 -13 -4 12.90 8.00 -15 13 -4 0.00 2.80 -15 13 -4 7.90 5.30 13 15 -4 0.80 1.90 15 -13 4 10.10 9.00 15 -15 -4 69.29 11.30 15 15 -4 73.09 6.90 15 15 -4 92.59 8.90 -15 15 -4 76.99 9.70 -15 -15 -4 92.79 11.00 15 -15 4 73.09 12.10 -14 16 -4 3.60 3.10 16 14 -4 3.90 2.10 -14 16 -4 7.10 6.30 14 -16 -4 13.80 9.20 -16 -14 -4 1.80 7.90 14 -16 4 -1.20 8.80 12 -16 -4 22.70 9.20 -12 16 -4 12.40 3.50 -16 -12 -4 21.00 8.20 16 12 -4 23.60 6.10 16 12 -4 28.90 4.60 12 -16 4 25.70 9.70 -16 -10 -4 1.10 7.40 16 10 -4 2.90 4.80 10 -16 -4 -1.50 7.60 16 10 -4 2.70 3.10 -10 16 -4 2.50 2.60 16 10 4 4.20 7.50 10 -16 4 3.10 7.60 16 8 -4 20.80 5.40 8 -16 -4 29.00 8.30 16 8 -4 27.40 3.30 -16 -8 -4 17.80 7.80 16 8 4 26.80 8.10 8 -16 4 27.90 8.50 -16 -6 -4 87.39 10.00 6 -16 -4 89.79 11.10 16 6 -4 74.29 5.10 -6 16 -4 81.59 8.30 6 -16 4 86.19 10.20 16 6 4 76.99 10.10 4 -16 -4 96.59 11.00 -4 16 -4 104.19 8.90 16 4 -4 90.69 5.60 -16 -4 4 87.99 5.40 16 4 4 101.19 10.80 4 -16 4 89.79 9.80 -16 -2 -4 4.00 2.80 -2 16 -4 5.90 2.40 16 2 -4 6.30 3.90 2 -16 -4 13.10 7.60 2 -16 4 8.20 6.80 -16 -2 4 6.40 6.60 -16 -2 4 0.50 1.90 16 0 -4 115.19 7.10 0 -16 -4 115.99 10.90 -16 0 -4 112.19 9.40 0 16 -4 121.69 8.90 -16 0 4 115.49 11.70 16 0 4 133.79 9.90 0 -16 4 116.09 10.00 -2 -16 -4 -5.40 6.80 2 16 -4 1.00 2.10 16 -2 -4 1.40 4.70 -16 2 -4 1.20 2.50 -16 2 4 -5.90 5.30 -2 -16 4 1.30 6.50 16 -2 4 -5.40 4.80 16 -4 -4 33.60 6.30 -4 -16 -4 31.30 8.50 -16 4 -4 18.30 3.30 4 16 -4 15.90 2.80 -4 -16 4 36.30 7.50 -16 4 4 46.40 9.50 16 -6 -4 64.49 7.90 6 16 -4 58.29 5.20 -6 -16 -4 54.39 9.50 -16 6 4 64.79 11.10 16 -6 4 70.49 7.30 -6 -16 4 59.19 8.50 -16 8 -4 2.50 2.60 8 16 -4 0.90 3.80 16 -8 -4 -4.90 6.00 -8 -16 -4 -0.60 7.20 8 16 -4 2.90 2.00 -16 8 4 1.20 7.30 -8 -16 4 3.60 6.30 -16 10 -4 5.00 2.80 16 -10 -4 8.80 7.30 10 16 -4 2.30 4.40 10 16 -4 2.30 2.10 -10 -16 -4 -9.10 7.30 16 -10 4 8.90 4.50 -12 -16 -4 71.29 10.70 12 16 -4 60.69 7.20 16 -12 -4 64.09 10.20 16 -12 4 66.49 11.10 -14 -16 -4 50.89 9.90 -16 14 -4 41.60 8.10 14 16 -4 22.90 2.90 -16 14 -4 12.90 3.80 16 -14 -4 49.30 10.10 14 16 -4 36.10 7.10 16 -14 4 44.20 10.70 16 16 -4 0.10 2.10 -16 16 -4 2.20 3.30 16 -16 -4 0.60 9.00 -16 -16 -4 4.30 8.50 -16 16 -4 -5.10 6.00 16 16 -4 8.10 6.40 16 -16 4 2.20 10.20 17 15 -4 5.00 2.20 15 -17 -4 9.40 9.30 -15 17 -4 12.50 7.20 -17 -15 -4 1.10 8.20 -15 17 -4 5.40 3.50 15 -17 4 5.90 10.10 17 13 -4 -3.50 1.90 13 -17 -4 -0.60 8.50 17 13 -4 2.10 5.70 -17 -13 -4 0.40 7.80 -13 17 -4 3.70 3.00 13 -17 4 5.30 9.40 17 13 4 0.20 8.50 -11 17 -4 107.59 10.60 17 11 -4 95.29 8.80 -17 -11 -4 103.99 10.90 11 -17 -4 100.39 11.90 17 11 -4 101.19 5.30 17 11 4 91.59 12.50 11 -17 4 99.99 12.20 9 -17 -4 8.80 8.50 17 9 -4 8.60 5.50 -9 17 -4 6.40 3.00 -17 -9 -4 10.00 7.70 17 9 4 19.60 8.20 9 -17 4 8.20 8.30 7 -17 -4 39.30 9.00 17 7 -4 36.60 6.40 -17 -7 -4 46.60 8.50 7 -17 4 42.70 9.30 17 7 4 48.80 9.60 5 -17 -4 4.20 7.50 -17 -5 -4 -0.10 7.00 -5 17 -4 -0.10 2.30 17 5 4 5.60 7.00 5 -17 4 2.90 6.90 17 3 -4 3.30 3.50 3 -17 -4 6.70 7.50 -3 17 -4 0.10 2.20 3 -17 4 3.80 6.60 -17 -3 4 -2.20 1.60 17 1 -4 84.19 6.10 1 -17 -4 99.69 11.40 -17 -1 -4 94.99 9.20 -1 17 -4 84.99 8.50 17 1 4 83.89 8.90 -17 -1 4 84.89 11.20 1 -17 4 90.09 10.50 -1 -17 -4 49.90 9.40 17 -1 -4 48.50 6.00 17 -1 4 48.00 7.40 -1 -17 4 46.50 8.30 -17 1 4 35.80 8.70 17 -3 -4 18.40 5.40 -17 3 -4 11.00 3.10 3 17 -4 11.00 2.70 -3 -17 -4 16.60 8.40 -17 3 4 21.80 8.10 -3 -17 4 17.40 7.30 -17 5 -4 74.49 8.60 -5 -17 -4 65.29 10.10 17 -5 -4 69.69 8.00 5 17 -4 72.09 7.90 -17 5 4 68.39 11.10 17 -5 4 74.39 8.00 -5 -17 4 67.19 9.10 -17 7 -4 6.50 2.90 7 17 -4 4.40 2.30 17 -7 -4 10.10 6.60 -7 -17 -4 11.00 8.30 7 17 -4 10.20 4.10 -17 7 4 8.10 7.60 -7 -17 4 19.10 7.20 17 -9 -4 113.49 10.20 9 17 -4 112.79 7.80 -17 9 -4 113.49 9.90 9 17 -4 114.09 8.50 -9 -17 -4 105.59 11.50 17 -9 4 101.79 8.00 -17 9 4 118.59 14.20 -9 -17 4 105.39 10.10 11 17 -4 3.40 2.30 11 17 -4 14.10 5.30 17 -11 -4 8.40 8.00 -11 -17 -4 2.80 8.30 -17 11 -4 4.60 3.00 -13 -17 -4 30.90 9.40 13 17 -4 15.80 2.80 13 17 -4 41.40 6.90 -17 13 -4 16.50 3.90 17 -13 -4 42.10 9.90 17 -13 4 29.40 11.30 17 -15 -4 -10.50 8.80 -15 -17 -4 5.90 8.50 -17 15 -4 3.30 6.50 15 17 -4 9.10 6.40 -17 15 -4 0.60 3.20 15 17 -4 1.90 2.20 17 -15 4 -5.80 9.50 -17 -17 -4 4.90 8.50 -17 17 -4 4.40 7.40 -17 17 -4 3.70 3.70 17 17 -4 0.00 2.30 17 17 -4 8.50 6.90 17 -17 -4 4.60 10.10 17 -17 4 1.30 11.40 16 -18 -4 7.30 10.20 -18 -16 -4 6.30 8.60 -16 18 -4 6.60 7.50 -16 18 -4 0.10 3.50 18 16 4 -6.70 9.00 16 -18 4 -8.00 10.80 14 -18 -4 12.40 9.70 -14 18 -4 8.10 3.60 -18 -14 -4 17.90 8.70 14 -18 4 13.70 10.20 18 14 4 23.40 10.40 -12 18 -4 0.90 3.00 18 12 -4 7.70 6.10 -18 -12 -4 6.10 8.00 12 -18 -4 3.40 8.80 18 12 4 6.90 8.90 12 -18 4 0.60 9.20 -10 18 -4 12.10 3.50 10 -18 -4 27.20 9.40 -18 -10 -4 23.80 8.30 18 10 -4 32.20 6.70 18 10 4 15.40 8.80 10 -18 4 26.80 9.20 -18 -8 -4 -1.90 7.50 8 -18 -4 9.10 8.50 -8 18 -4 0.30 2.60 18 8 -4 9.50 5.50 18 8 4 9.60 7.80 8 -18 4 2.30 8.10 6 -18 -4 -5.30 7.60 -6 18 -4 2.20 2.60 -18 -6 -4 -0.50 7.40 18 6 4 2.90 7.10 6 -18 4 8.30 7.70 4 -18 -4 61.09 10.50 4 -18 4 44.20 9.00 18 2 -4 4.20 3.70 2 -18 -4 -4.10 7.30 -2 18 -4 1.50 2.40 -18 -2 -4 0.50 2.90 2 -18 4 1.30 6.80 -18 -2 4 -2.80 1.80 18 2 4 1.20 5.90 0 -18 -4 6.60 7.80 18 0 -4 7.70 4.40 -18 0 -4 4.50 3.00 0 18 -4 3.60 2.40 0 -18 4 6.80 7.40 -18 0 4 3.50 6.40 18 0 4 2.10 6.10 2 18 -4 55.29 4.80 -2 -18 -4 61.89 10.30 18 -2 -4 64.89 6.80 -2 -18 4 54.49 9.10 -18 2 4 67.99 11.00 -18 4 -4 3.20 2.80 18 -4 -4 7.60 5.70 -4 -18 -4 -5.30 7.80 4 18 -4 4.00 2.40 -4 -18 4 8.60 7.20 -18 4 4 7.70 7.10 18 -4 4 -0.20 5.50 -6 -18 -4 23.50 8.70 -18 6 -4 16.50 3.40 6 18 -4 14.50 3.00 18 -6 -4 39.70 7.30 18 -6 4 25.90 6.40 -18 6 4 26.10 9.10 -6 -18 4 27.30 8.10 -18 8 -4 82.69 9.50 -8 -18 -4 95.59 11.60 8 18 -4 97.79 8.50 18 -8 -4 90.99 10.00 -8 -18 4 82.89 10.00 18 -8 4 79.59 7.90 -18 8 4 88.09 13.00 -18 10 -4 19.50 3.90 10 18 -4 42.70 6.40 10 18 -4 21.20 3.30 -10 -18 -4 27.70 9.30 18 -10 -4 38.10 8.90 18 -10 4 39.10 6.30 -18 10 4 33.60 10.90 -10 -18 4 46.80 8.60 12 18 -4 16.00 6.00 -18 12 -4 2.30 3.20 -12 -18 -4 11.30 9.00 18 -12 -4 5.10 8.60 12 18 -4 4.00 2.40 18 -14 -4 16.20 9.40 -14 -18 -4 18.30 9.30 -18 14 -4 5.10 3.60 -18 14 -4 14.00 7.30 14 18 -4 8.90 2.60 14 18 -4 16.10 6.70 18 -14 4 18.10 11.30 -18 16 -4 12.70 7.60 18 -16 -4 -0.80 9.20 -16 -18 -4 11.40 9.20 -18 16 -4 6.10 3.70 16 18 -4 12.60 7.00 16 18 -4 2.60 2.40 18 -16 4 11.00 11.50 -18 18 -4 108.79 13.40 18 18 -4 104.89 11.40 -18 -18 -4 110.19 12.30 18 -18 -4 115.49 14.90 18 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-4 81.29 7.10 -1 -19 -4 89.69 11.80 1 19 -4 77.79 8.80 19 -1 4 86.89 9.60 -1 -19 4 89.79 10.70 -19 1 4 95.19 12.40 3 19 -4 11.30 2.90 -3 -19 -4 18.50 8.90 19 -3 -4 24.20 6.00 -19 3 -4 11.60 3.50 3 19 -4 16.60 4.00 19 -3 4 20.90 6.70 -19 3 4 16.90 7.60 -3 -19 4 18.80 8.00 19 -5 -4 84.69 8.70 -19 5 -4 90.29 10.20 5 19 -4 89.99 6.60 5 19 -4 89.49 9.00 -5 -19 -4 99.09 11.80 -19 5 4 77.99 12.80 19 -5 4 97.09 9.40 -5 -19 4 100.89 11.10 7 19 -4 0.70 2.40 -19 7 -4 5.70 3.20 19 -7 -4 9.20 6.90 -7 -19 -4 8.30 8.90 -19 7 4 4.80 7.70 -7 -19 4 3.90 7.60 -19 9 -4 11.80 3.50 19 -9 -4 20.10 8.20 9 19 -4 9.70 2.90 -9 -19 -4 23.40 9.40 -19 9 4 29.00 10.20 -9 -19 4 16.60 8.00 19 -9 4 22.60 5.70 19 -11 -4 9.10 8.20 11 19 -4 7.40 2.70 11 19 -4 1.10 5.50 -19 11 -4 8.40 3.50 -11 -19 -4 16.90 9.30 -19 11 4 12.20 9.80 -11 -19 4 21.20 8.20 -13 -19 -4 16.00 9.50 19 -13 -4 17.60 9.80 13 19 -4 31.20 7.10 -19 13 -4 14.70 4.10 13 19 -4 12.00 2.90 15 19 -4 1.20 6.40 19 -15 -4 3.50 9.70 -15 -19 -4 5.70 9.00 15 19 -4 -0.70 2.30 -19 15 -4 3.80 3.60 -19 15 -4 8.20 6.90 19 -15 4 -5.80 10.50 -19 17 -4 17.60 8.90 -17 -19 -4 27.40 9.90 17 19 -4 10.30 7.50 19 -17 -4 21.80 11.30 19 -17 4 28.20 12.90 -19 -19 -4 3.40 9.00 -19 19 -4 8.50 9.50 19 19 -4 2.10 7.70 19 -19 -4 -1.80 11.00 -19 19 -4 1.40 4.00 19 -19 4 -11.10 12.30 19 19 4 15.10 11.40 -20 -18 -4 21.20 10.90 18 -20 -4 20.90 12.40 -18 20 -4 9.70 4.40 18 -20 4 17.10 12.80 20 18 4 3.50 11.10 16 -20 -4 13.30 11.50 -16 20 -4 5.60 3.80 -20 -16 -4 21.00 9.00 16 -20 4 0.90 11.50 20 16 4 1.40 10.40 20 14 -4 85.49 9.90 -20 -14 -4 88.99 10.60 14 -20 -4 87.39 13.60 14 -20 4 83.59 14.10 20 14 4 63.59 12.80 20 12 -4 11.00 6.70 12 -20 -4 5.80 9.80 -20 -12 -4 18.10 8.50 -12 20 -4 7.50 3.50 12 -20 4 12.40 9.90 20 12 4 -3.10 9.10 20 10 -4 4.10 6.20 -20 -10 -4 3.70 8.50 -10 20 -4 3.60 3.10 10 -20 -4 -8.50 8.30 10 -20 4 0.00 9.10 20 10 4 8.20 9.20 -8 20 -4 8.50 3.20 -20 -8 -4 15.10 8.60 8 -20 -4 13.10 9.70 20 8 -4 21.40 6.90 8 -20 4 11.30 8.90 -20 -6 -4 12.70 8.30 6 -20 -4 13.20 9.50 -6 20 -4 7.00 3.10 6 -20 4 14.70 8.80 20 6 4 8.80 7.00 4 -20 -4 22.40 9.70 4 -20 4 15.80 8.40 20 4 4 26.90 8.30 -20 -2 -4 7.10 3.60 20 2 -4 13.00 3.90 2 -20 -4 -2.00 8.20 -2 20 -4 2.40 2.60 -20 -2 4 -1.50 1.90 2 -20 4 4.50 8.00 20 2 4 13.60 7.00 -20 0 -4 -4.40 3.00 0 -20 -4 6.70 8.80 20 0 -4 4.70 4.40 0 20 -4 0.20 2.40 0 -20 4 1.70 7.50 -20 0 4 3.70 6.60 20 0 4 4.30 6.50 -2 -20 -4 147.59 12.90 -20 2 -4 159.88 11.90 2 20 -4 164.58 11.10 20 -2 -4 162.68 9.10 20 -2 4 141.59 11.00 -2 -20 4 152.48 12.90 -20 2 4 157.28 14.40 20 -4 -4 -1.40 5.80 4 20 -4 3.00 2.60 -4 -20 -4 9.60 9.00 4 20 -4 6.90 4.10 -20 4 -4 6.30 3.30 -4 -20 4 9.80 7.90 20 -4 4 7.50 6.50 -20 4 4 3.30 7.70 -6 -20 -4 27.90 9.90 6 20 -4 16.70 3.30 6 20 -4 34.20 5.40 20 -6 -4 33.90 7.70 -6 -20 4 31.40 9.10 20 -6 4 29.00 7.50 -20 6 4 26.40 9.60 20 -8 -4 8.50 7.50 -8 -20 -4 10.50 9.10 -20 8 -4 1.30 3.20 8 20 -4 4.50 2.70 -20 8 4 2.50 8.40 -8 -20 4 14.00 8.40 20 -8 4 3.10 5.30 -20 10 -4 20.30 4.10 20 -10 -4 34.50 9.20 10 20 -4 15.60 3.40 -10 -20 -4 36.80 10.40 -10 -20 4 40.90 9.40 -20 10 4 27.60 11.30 20 -10 4 31.20 6.70 -12 -20 -4 11.60 9.30 12 20 -4 13.00 6.40 12 20 -4 5.50 2.90 20 -12 -4 10.00 9.00 -20 12 -4 5.10 3.60 -12 -20 4 8.50 8.40 14 20 -4 28.60 7.50 14 20 -4 12.60 3.10 -14 -20 -4 24.30 9.80 -20 14 -4 8.80 4.00 -20 14 -4 17.10 7.80 20 -14 -4 19.10 10.10 20 -16 -4 22.80 10.60 -20 16 -4 20.50 9.10 -20 16 -4 5.90 4.10 -16 -20 -4 13.80 9.50 16 20 -4 9.20 2.80 16 20 -4 9.40 7.30 20 -16 4 32.00 13.20 -20 18 -4 8.70 9.00 -18 -20 -4 11.80 9.10 -20 18 -4 7.60 4.40 20 -18 -4 8.80 11.40 18 20 -4 11.00 8.20 20 -18 4 3.60 12.30 20 20 -4 -0.90 7.50 -20 20 -4 0.40 4.00 20 -20 -4 -5.40 10.80 20 -20 4 -6.90 11.40 20 20 4 -0.10 10.50 -19 21 -4 3.40 4.20 19 -21 -4 8.50 11.40 19 -21 4 2.00 12.40 21 19 4 11.70 11.00 17 -21 -4 134.89 16.40 -17 21 -4 124.49 13.60 17 -21 4 147.79 17.70 21 17 4 108.49 15.70 21 15 -4 22.90 8.30 -21 -15 -4 27.20 9.40 -15 21 -4 9.30 4.30 15 -21 -4 28.80 12.20 21 15 4 35.50 11.60 15 -21 4 23.10 12.50 21 13 -4 6.30 7.20 13 -21 -4 3.20 10.30 -13 21 -4 1.80 3.40 -21 -13 -4 14.90 8.30 13 -21 4 -0.30 10.50 21 13 4 3.40 9.30 -21 -11 -4 5.60 8.30 21 11 -4 0.50 6.40 -11 21 -4 0.30 3.20 11 -21 -4 -3.70 9.50 11 -21 4 4.10 9.70 21 11 4 -2.60 8.50 9 -21 -4 37.80 10.90 -21 -9 -4 59.49 10.10 21 9 -4 59.59 8.60 9 -21 4 44.50 10.80 7 -21 -4 2.70 9.20 -21 -7 -4 2.40 8.60 21 7 -4 11.70 6.60 -7 21 -4 0.20 2.80 21 7 4 4.90 7.60 7 -21 4 9.10 8.70 -21 -5 -4 1.60 8.40 -5 21 -4 4.60 3.00 5 -21 -4 21.00 9.60 5 -21 4 13.90 9.10 21 5 4 16.00 8.10 3 -21 -4 75.89 11.90 -3 21 -4 36.80 4.60 3 -21 4 66.09 10.80 21 3 4 59.69 9.50 1 -21 -4 33.50 10.20 -21 -1 -4 22.30 4.30 -1 21 -4 13.90 3.50 -21 -1 4 20.60 8.30 21 1 4 26.40 8.00 1 -21 4 38.10 9.70 1 21 -4 30.70 4.20 -1 -21 -4 62.99 11.20 -21 1 -4 30.60 4.60 21 -1 -4 55.79 6.50 -1 -21 4 61.59 10.30 -21 1 4 52.99 11.10 21 -3 -4 18.60 6.30 -3 -21 -4 23.10 10.00 3 21 -4 8.30 4.40 3 21 -4 3.50 2.90 -21 3 -4 6.80 3.50 -21 3 4 16.60 8.60 -3 -21 4 10.40 8.30 21 -3 4 15.20 7.20 5 21 -4 1.80 4.70 5 21 -4 6.30 2.90 -21 5 -4 1.90 3.30 21 -5 -4 10.20 6.90 -5 -21 -4 14.50 9.50 -5 -21 4 13.00 8.40 -21 5 4 6.50 8.50 21 -5 4 4.10 6.70 -7 -21 -4 65.59 11.90 7 21 -4 75.89 7.90 21 -7 -4 85.69 10.10 21 -7 4 79.39 8.40 -7 -21 4 79.79 11.30 -21 7 4 66.89 12.30 -9 -21 -4 5.00 9.50 -21 9 -4 7.40 3.60 21 -9 -4 3.00 7.80 9 21 -4 2.40 2.80 21 -9 4 -4.10 5.20 -9 -21 4 7.30 8.60 -21 9 4 9.40 9.60 -11 -21 -4 46.70 10.70 11 21 -4 16.40 3.50 -21 11 -4 18.20 4.30 21 -11 -4 36.50 9.80 -11 -21 4 31.40 9.70 -21 11 4 23.50 12.00 -13 -21 -4 39.40 10.70 21 -13 -4 33.50 10.70 13 21 -4 42.80 8.10 -13 -21 4 42.20 10.10 -21 15 -4 60.99 11.10 -15 -21 -4 49.90 11.30 15 21 -4 50.79 9.00 21 -15 -4 60.09 12.40 21 -15 4 41.80 13.70 -17 -21 -4 3.30 9.10 17 21 -4 9.60 7.70 -21 17 -4 16.10 9.20 -21 17 -4 3.70 4.20 21 -17 -4 0.60 10.30 21 -17 4 -3.90 12.30 21 -19 -4 7.20 10.60 -19 -21 -4 12.40 11.40 -21 19 -4 4.50 4.10 -21 19 -4 -2.30 8.90 19 21 -4 13.50 8.20 19 21 4 -5.90 10.40 21 -19 4 10.80 12.80 21 -21 -4 10.50 10.80 -21 21 -4 1.20 3.90 21 21 -4 -1.80 7.60 21 -21 4 -9.90 12.00 21 21 4 -4.20 10.40 -20 22 -4 -2.70 3.60 20 -22 -4 7.90 10.90 20 -22 4 7.70 12.30 22 20 4 -12.30 9.40 -18 22 -4 6.00 4.30 18 -22 -4 21.30 11.60 18 -22 4 11.70 12.80 22 18 4 23.70 11.40 16 -22 -4 63.99 13.60 22 16 -4 66.79 10.00 16 -22 4 83.89 15.10 22 16 4 54.79 12.90 22 14 -4 53.89 9.60 14 -22 -4 43.40 12.80 14 -22 4 48.70 13.40 22 14 4 37.10 12.10 -12 22 -4 4.70 3.60 -22 -12 -4 11.70 8.50 22 12 -4 5.60 7.30 12 -22 -4 5.40 10.50 12 -22 4 -8.40 10.10 22 12 4 -8.20 9.20 -22 -10 -4 -5.30 8.30 -10 22 -4 -4.10 2.90 22 10 -4 -1.50 6.80 10 -22 -4 15.60 10.00 10 -22 4 4.70 9.60 -22 -8 -4 -0.40 8.70 22 8 -4 1.90 6.40 8 -22 -4 9.20 10.00 -8 22 -4 3.40 3.30 8 -22 4 -4.10 9.20 22 8 4 -0.60 7.90 -22 -6 -4 0.80 8.60 -6 22 -4 1.80 3.00 6 -22 -4 0.80 9.30 22 6 4 -0.50 7.70 6 -22 4 -1.90 8.50 -4 22 -4 1.80 3.00 4 -22 -4 8.70 9.90 22 4 4 5.30 7.90 4 -22 4 16.10 9.00 2 -22 -4 26.50 10.10 -22 -2 -4 16.70 4.30 -2 22 -4 15.80 3.90 2 -22 4 15.00 9.10 22 2 4 27.40 8.30 0 22 -4 55.89 5.90 -22 0 -4 32.50 4.70 22 0 -4 56.89 6.30 0 -22 -4 43.10 11.10 0 -22 4 45.00 10.50 -22 0 4 51.89 11.00 -22 2 -4 11.60 4.00 2 22 -4 9.80 3.30 -2 -22 -4 10.40 9.60 22 -2 -4 13.70 6.10 -22 2 4 19.40 9.20 22 -2 4 14.20 7.70 -2 -22 4 20.30 9.40 22 -4 -4 77.89 9.30 -4 -22 -4 77.09 12.90 4 22 -4 78.99 7.00 4 22 -4 91.79 10.10 -22 4 4 84.29 13.00 22 -4 4 92.49 10.70 -4 -22 4 93.99 12.10 6 22 -4 27.50 4.10 -6 -22 -4 46.00 11.40 6 22 -4 57.69 6.70 -22 6 -4 28.50 4.70 22 -6 -4 47.90 8.60 -22 6 4 46.80 11.90 -6 -22 4 55.09 11.00 8 22 -4 141.89 9.70 22 -8 -4 133.69 11.80 8 22 -4 140.49 11.40 -8 -22 -4 144.79 14.50 -22 8 -4 156.28 12.80 -8 -22 4 134.19 13.40 -22 8 4 141.69 16.80 22 -8 4 129.09 10.80 -10 -22 -4 -0.60 9.50 -22 10 -4 -0.20 3.40 10 22 -4 -2.00 2.70 22 -10 -4 8.30 8.50 -22 10 4 -6.80 9.70 -10 -22 4 19.70 9.50 22 -10 4 9.80 5.90 12 22 -4 3.10 3.00 -22 12 -4 10.70 4.10 -12 -22 -4 4.30 9.80 12 22 -4 1.90 6.70 22 -12 -4 13.20 9.70 -12 -22 4 10.30 9.40 -22 12 4 25.20 12.80 -22 14 -4 17.00 8.60 22 -14 -4 7.00 10.60 14 22 -4 -1.00 7.20 -22 14 -4 4.70 4.10 14 22 -4 2.20 3.00 -14 -22 -4 6.50 9.90 -22 16 -4 19.30 9.20 -16 -22 -4 5.10 9.60 22 -16 -4 19.00 11.00 -22 16 -4 4.70 4.30 16 22 -4 19.20 8.30 22 -16 4 -2.60 12.80 -18 -22 -4 10.40 8.80 -22 18 -4 9.10 9.00 -22 18 -4 -2.00 3.90 18 22 -4 11.60 7.70 22 -18 -4 2.00 10.50 22 -18 4 -1.20 12.10 -22 20 -4 -2.90 3.80 20 22 -4 -7.80 7.10 22 -20 -4 6.30 10.80 22 -20 4 -6.20 11.90 20 22 4 -8.30 10.00 -22 22 -4 -0.90 3.90 22 -22 -4 4.40 11.40 22 22 -4 7.70 8.50 22 22 4 -2.40 10.40 22 -22 4 4.90 12.70 -21 23 -4 2.10 4.20 21 -23 -4 7.10 11.50 23 21 4 -8.10 9.70 21 -23 4 -1.90 12.80 19 -23 -4 4.80 10.90 -19 23 -4 7.50 4.20 23 19 4 1.10 10.00 19 -23 4 -7.80 11.50 -17 23 -4 6.90 4.30 23 17 -4 9.70 8.00 17 -23 -4 11.50 11.70 23 17 4 9.90 10.30 17 -23 4 -2.70 12.00 15 -23 -4 5.90 11.20 23 15 -4 27.60 8.70 -15 23 -4 8.50 4.40 15 -23 4 9.50 12.00 23 15 4 3.30 10.50 13 -23 -4 179.18 16.50 23 13 -4 222.48 14.30 -13 23 -4 202.08 15.60 13 -23 4 193.88 18.20 23 11 -4 -1.70 7.30 11 -23 -4 10.30 10.90 -11 23 -4 -2.00 3.20 11 -23 4 1.60 10.60 23 11 4 9.50 8.90 -23 -9 -4 -2.10 8.70 9 -23 -4 -8.00 9.60 -9 23 -4 -1.20 3.00 23 9 -4 -2.50 7.30 9 -23 4 7.10 10.10 23 9 4 -0.50 8.50 7 -23 -4 -0.80 8.90 -7 23 -4 2.80 3.30 -23 -7 -4 3.20 8.90 23 7 4 6.40 8.30 7 -23 4 4.90 9.80 -5 23 -4 99.49 11.40 5 -23 -4 97.79 13.10 -23 -5 -4 113.39 12.20 23 5 4 107.29 12.60 5 -23 4 101.59 13.30 3 -23 -4 -3.30 9.00 -3 23 -4 2.90 3.10 23 3 4 6.30 7.70 3 -23 4 -2.70 8.90 -1 23 -4 9.30 3.60 23 1 -4 13.50 5.80 -23 -1 -4 6.50 4.10 1 -23 -4 12.70 9.90 -23 -1 4 10.60 8.30 1 -23 4 9.00 8.90 1 23 -4 3.10 3.10 1 23 -4 9.20 5.70 -23 1 -4 1.70 4.00 -1 -23 -4 -1.50 9.80 23 -1 -4 15.40 5.80 23 -1 4 10.70 7.70 -1 -23 4 10.60 9.60 -23 1 4 10.40 8.60 -3 -23 -4 17.50 10.10 23 -3 -4 29.50 7.00 -23 3 -4 11.10 4.00 3 23 -4 5.90 3.40 -3 -23 4 16.70 9.90 23 -3 4 19.40 8.10 -23 3 4 20.60 9.90 5 23 -4 4.60 5.40 23 -5 -4 14.10 7.30 -5 -23 -4 1.10 9.90 -23 5 -4 8.30 3.90 5 23 -4 1.80 3.00 -23 5 4 -0.20 8.30 -5 -23 4 7.90 9.50 -7 -23 -4 70.69 12.40 7 23 -4 87.79 8.90 23 -7 -4 69.59 10.10 -7 -23 4 76.99 12.30 -23 7 4 56.59 13.00 23 -7 4 70.29 8.90 -23 9 -4 2.50 3.60 9 23 -4 2.40 3.00 -9 -23 -4 -7.50 9.50 23 -9 -4 -2.00 8.20 -23 9 4 -9.80 8.70 23 -9 4 -5.60 6.00 -9 -23 4 -2.70 9.50 23 -11 -4 109.29 13.30 -23 11 -4 108.79 12.50 11 23 -4 118.19 11.70 -11 -23 -4 109.89 13.80 -23 11 4 137.59 18.90 -11 -23 4 122.39 13.60 -13 -23 -4 59.19 11.70 13 23 -4 49.60 8.90 23 -13 -4 55.19 11.90 -13 -23 4 61.49 11.40 15 23 -4 6.00 7.60 -23 15 -4 6.20 4.30 23 -15 -4 4.40 10.40 15 23 -4 1.20 3.10 -23 15 -4 14.50 8.90 -15 -23 -4 6.00 9.50 17 23 -4 -1.20 7.20 23 -17 -4 6.00 10.30 -23 17 -4 1.30 8.30 -17 -23 -4 2.90 8.50 -23 17 -4 -2.90 4.00 23 -17 4 -11.30 12.10 -23 19 -4 -1.10 4.00 -23 19 -4 -6.20 8.70 23 -19 -4 2.20 10.80 19 23 -4 7.70 7.60 19 23 4 -6.60 10.10 23 -19 4 0.20 12.70 -23 21 -4 0.00 4.20 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9.80 -4 24 -4 -1.10 3.10 4 -24 4 -5.50 9.10 24 4 4 -1.90 8.00 2 -24 -4 7.10 10.20 -2 24 -4 3.90 3.20 -24 -2 -4 2.10 4.20 2 -24 4 4.30 9.10 0 24 -4 -0.90 3.00 0 -24 -4 0.90 10.00 -24 0 -4 2.50 4.00 24 0 4 12.10 7.90 -24 0 4 6.90 8.60 0 -24 4 8.00 9.70 24 -2 -4 13.40 6.50 -2 -24 -4 8.30 10.50 -24 2 -4 5.40 4.00 2 24 -4 4.20 3.30 -2 -24 4 3.20 9.90 24 -2 4 1.90 7.80 -24 2 4 22.50 9.60 24 -4 -4 23.70 7.60 -24 4 -4 12.40 4.40 4 24 -4 4.80 3.40 -4 -24 -4 14.70 10.90 24 -4 4 20.70 8.60 -4 -24 4 23.70 10.40 -24 4 4 13.30 9.30 6 24 -4 -2.90 2.80 6 24 -4 5.30 5.70 -24 6 -4 2.70 4.00 -6 -24 -4 3.70 10.00 24 -6 -4 9.30 8.10 -6 -24 4 0.10 9.70 24 -6 4 -1.20 6.20 -24 6 4 3.50 9.10 24 -8 -4 14.30 8.80 -24 8 -4 3.40 3.90 8 24 -4 11.90 6.10 8 24 -4 -4.80 2.80 -8 -24 -4 -6.60 10.10 24 -8 4 -3.20 6.30 -24 8 4 -4.90 9.80 -8 -24 4 11.90 10.50 -24 10 -4 7.30 4.20 -10 -24 -4 18.20 10.30 10 24 -4 4.70 3.30 24 -10 -4 15.50 9.70 -24 10 4 13.40 12.00 -10 -24 4 2.40 10.20 -24 12 -4 3.00 3.90 12 24 -4 4.20 3.30 24 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11.80 15 -25 -4 81.79 14.30 25 15 -4 74.09 10.50 25 15 4 28.60 10.60 15 -25 4 64.19 14.20 -13 25 -4 5.50 3.80 25 13 -4 24.20 8.50 13 -25 -4 3.30 11.00 13 -25 4 0.10 10.40 25 13 4 -2.20 8.70 25 11 -4 -3.30 7.70 -11 25 -4 5.80 3.90 11 -25 -4 6.90 11.00 25 11 4 -10.80 8.60 11 -25 4 -1.60 9.90 9 -25 -4 -3.60 10.30 -9 25 -4 2.00 3.50 25 9 -4 -1.00 7.60 9 -25 4 -2.60 10.40 25 9 4 13.60 9.10 -7 25 -4 -1.60 3.20 7 -25 -4 1.90 10.30 7 -25 4 0.40 10.40 25 7 4 -3.00 8.30 5 -25 -4 -8.90 9.30 -5 25 -4 1.80 3.40 -25 -5 -4 0.50 15.60 25 5 4 -1.00 7.80 5 -25 4 2.90 9.80 3 -25 -4 17.10 10.40 -3 25 -4 5.00 3.60 3 -25 4 19.20 11.00 -25 -1 -4 35.00 5.40 -1 25 -4 40.70 5.50 1 -25 -4 52.09 12.00 25 1 4 60.69 10.50 -25 -1 4 81.49 13.70 1 -25 4 62.09 12.20 1 25 -4 5.20 3.60 -25 1 -4 0.90 4.10 -1 -25 -4 6.10 10.90 -1 -25 4 -2.50 9.70 25 -1 4 7.50 8.30 -25 1 4 9.80 9.40 3 25 -4 14.60 4.10 -3 -25 -4 22.30 11.60 -25 3 -4 16.30 4.60 25 -3 4 38.30 9.30 -3 -25 4 27.30 10.90 -25 3 4 23.20 11.10 25 -5 -4 0.20 7.50 -25 5 -4 -3.50 4.10 -5 -25 -4 9.60 10.60 5 25 -4 -1.30 3.20 -5 -25 4 -8.30 10.00 -25 5 4 4.30 9.60 -7 -25 -4 49.99 12.00 25 -7 -4 55.59 10.10 -7 -25 4 39.70 11.90 25 -7 4 40.10 8.10 -25 7 4 47.40 13.60 -25 9 -4 20.80 5.00 9 25 -4 40.00 10.00 9 25 -4 20.30 4.30 -9 -25 -4 37.00 11.70 25 -9 -4 39.60 10.40 -25 9 4 18.70 11.90 -9 -25 4 40.90 11.80 25 -9 4 20.50 7.40 -11 -25 -4 27.30 11.10 25 -11 -4 37.60 10.90 -25 11 -4 13.50 4.90 -11 -25 4 25.40 11.10 -25 11 4 45.00 15.10 -13 -25 -4 26.20 10.40 -25 13 -4 14.90 4.70 25 -13 -4 39.80 11.20 13 25 -4 8.70 3.60 -13 -25 4 21.30 10.50 -25 13 4 26.20 14.80 -25 15 -4 4.50 8.50 15 25 -4 0.90 7.00 25 -15 -4 12.00 10.30 -15 -25 -4 4.90 8.70 -25 15 -4 -1.00 4.00 25 -17 -4 31.60 11.70 -25 17 -4 26.40 10.90 -17 -25 -4 51.39 10.50 -25 17 -4 10.70 5.00 17 25 -4 39.00 8.80 25 -19 -4 26.00 11.80 19 25 -4 4.90 8.10 -25 19 -4 -3.20 4.10 -25 19 -4 -11.00 14.00 25 -19 4 -8.60 13.00 19 25 4 -11.70 10.30 -25 21 -4 -1.20 4.60 25 -21 -4 11.80 12.20 21 25 -4 -1.50 8.60 21 25 4 3.70 11.90 25 -21 4 -3.20 14.00 23 25 -4 7.80 9.10 25 -23 -4 21.30 12.70 -25 23 -4 1.10 4.80 25 -23 4 6.20 15.20 23 25 4 7.50 11.80 -25 25 -4 0.40 5.20 25 -25 -4 20.30 14.20 25 -25 4 -7.80 14.30 25 25 4 19.60 11.50 24 -26 -4 11.50 13.30 -24 26 -4 0.10 4.60 24 -26 4 -12.90 14.30 22 -26 -4 4.10 12.40 -22 26 -4 2.30 4.70 26 22 -4 1.20 9.20 22 -26 4 -8.70 14.20 26 20 -4 1.90 8.80 20 -26 -4 20.20 12.90 -20 26 -4 -3.00 4.00 20 -26 4 8.70 13.40 -18 26 -4 3.90 4.30 18 -26 -4 19.60 11.90 26 18 -4 18.30 9.10 26 18 4 2.20 9.60 18 -26 4 2.30 13.20 26 16 -4 5.60 8.30 16 -26 -4 12.60 11.50 -16 26 -4 -2.00 3.70 16 -26 4 2.70 11.70 26 16 4 -5.70 8.90 26 14 -4 9.20 8.40 -14 26 -4 1.70 3.70 14 -26 -4 1.80 10.40 26 14 4 5.00 9.10 14 -26 4 -2.40 11.60 12 -26 -4 8.40 11.10 -12 26 -4 0.70 3.50 26 12 -4 8.10 8.60 26 12 4 2.80 9.10 12 -26 4 13.60 11.10 -10 26 -4 0.50 3.50 10 -26 -4 -5.70 10.10 26 10 -4 5.60 7.90 10 -26 4 9.90 10.40 26 10 4 5.10 8.40 -8 26 -4 0.40 3.40 8 -26 -4 -4.60 9.80 8 -26 4 10.00 10.20 26 8 4 -1.10 8.60 6 -26 -4 2.60 10.60 -6 26 -4 2.80 3.50 6 -26 4 -1.90 10.20 26 6 4 -1.10 8.40 -4 26 -4 32.60 5.30 4 -26 -4 39.40 12.00 4 -26 4 72.59 13.40 2 -26 -4 -1.80 10.00 -2 26 -4 0.40 3.30 2 -26 4 7.40 10.20 26 2 4 -2.20 8.00 -26 0 -4 11.90 5.00 0 -26 -4 35.20 11.30 0 26 -4 20.70 4.60 -26 0 4 31.20 10.80 0 -26 4 26.60 11.20 26 0 4 25.90 9.30 -26 2 -4 21.70 5.20 2 26 -4 23.10 4.70 -2 -26 -4 52.89 12.30 -2 -26 4 38.10 11.80 -26 2 4 47.10 12.40 26 -2 4 52.09 10.60 -26 4 -4 -1.10 4.20 4 26 -4 -0.20 3.40 -4 -26 -4 -6.90 10.40 -26 4 4 12.40 10.80 -4 -26 4 -2.80 10.30 26 -6 -4 12.50 9.20 6 26 -4 12.40 4.00 -26 6 -4 13.40 4.80 -6 -26 -4 22.10 11.50 -26 6 4 22.10 11.80 -6 -26 4 26.80 11.60 26 -6 4 31.20 8.30 -26 8 -4 -0.80 4.30 8 26 -4 1.30 3.30 26 -8 -4 4.10 8.60 -8 -26 -4 4.70 10.50 26 -8 4 -1.30 6.40 -26 8 4 12.60 12.10 -8 -26 4 -4.00 10.40 -10 -26 -4 15.80 10.90 26 -10 -4 16.80 9.40 10 26 -4 4.70 3.50 -26 10 -4 5.40 4.30 -26 10 4 -2.50 11.30 -10 -26 4 -1.30 10.10 -12 -26 -4 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-1.30 3.80 17 -27 -4 1.90 11.10 17 -27 4 -5.50 11.80 27 17 4 1.50 10.00 15 -27 -4 16.70 12.00 -15 27 -4 2.50 3.80 27 15 -4 6.40 8.40 27 15 4 14.40 10.10 15 -27 4 5.30 11.90 27 13 -4 -3.50 8.20 -13 27 -4 0.50 3.40 13 -27 -4 7.00 10.90 27 13 4 -5.60 8.40 13 -27 4 9.20 11.40 11 -27 -4 46.00 12.70 27 11 -4 42.60 10.10 27 11 4 53.09 11.70 11 -27 4 34.00 12.20 -9 27 -4 4.50 3.70 9 -27 -4 9.30 10.60 27 9 -4 7.10 8.00 9 -27 4 5.00 10.10 27 9 4 7.20 8.60 -7 27 -4 1.40 3.50 7 -27 -4 8.60 10.50 27 7 4 6.60 8.30 7 -27 4 -12.30 9.30 -5 27 -4 -0.30 3.40 5 -27 -4 4.40 10.40 5 -27 4 5.80 10.10 3 -27 -4 79.99 13.50 27 3 4 67.69 11.60 3 -27 4 79.49 13.50 1 -27 -4 15.70 10.60 -1 27 -4 6.10 3.70 -27 -1 4 17.20 10.00 27 1 4 14.10 8.90 1 -27 4 15.90 10.90 -27 1 -4 4.50 4.80 1 27 -4 6.00 3.90 -1 -27 -4 16.20 11.00 -27 1 4 12.50 10.30 -1 -27 4 9.60 11.10 27 -1 4 11.10 8.50 3 27 -4 5.00 3.60 -27 3 -4 0.50 4.40 -3 -27 -4 3.30 10.30 -3 -27 4 -1.40 10.40 -27 3 4 2.20 10.00 5 27 -4 15.70 4.30 -27 5 -4 10.90 4.90 -5 -27 -4 26.60 11.50 27 -5 4 22.50 8.10 -27 5 4 33.80 12.50 -5 -27 4 12.00 10.90 -27 7 -4 1.00 4.40 7 27 -4 0.30 3.40 -7 -27 -4 18.60 10.70 -7 -27 4 1.90 10.40 -27 7 4 7.80 11.20 27 -7 4 9.80 7.10 -9 -27 -4 64.99 12.70 9 27 -4 29.00 4.90 -27 9 -4 23.00 5.30 27 -9 -4 61.29 11.20 27 -9 4 37.10 8.50 -9 -27 4 45.50 12.00 -27 9 4 42.60 14.00 27 -11 -4 -5.70 8.90 -11 -27 -4 -4.90 9.40 11 27 -4 1.20 3.40 -27 11 -4 -0.50 4.20 -27 11 4 -3.10 12.20 -11 -27 4 -3.40 9.80 13 27 -4 1.50 3.40 -13 -27 -4 14.80 9.70 27 -13 -4 9.80 10.00 -27 13 -4 3.70 4.30 -27 13 4 -1.80 13.60 -13 -27 4 -3.50 9.80 -15 -27 -4 14.60 9.70 -27 15 -4 26.40 10.30 -27 15 -4 0.50 4.20 27 -15 -4 3.30 10.30 27 -17 -4 12.40 11.40 -27 17 -4 -2.60 9.60 -27 17 -4 -5.70 4.10 27 -19 -4 3.90 11.90 -27 19 -4 -4.00 4.70 19 27 4 -18.10 10.60 -27 21 -4 0.80 4.90 27 -21 -4 12.40 12.60 21 27 4 1.30 12.00 -27 23 -4 -1.70 4.90 27 -23 -4 0.90 12.30 23 27 4 15.10 12.70 27 -23 4 -7.50 14.20 -22 28 -4 0.70 4.50 28 22 -4 10.10 10.00 22 -28 -4 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0 -36 -4 9.70 12.20 0 -36 4 -13.80 12.10 -36 0 4 9.00 12.30 36 0 4 1.80 8.70 2 36 -4 1.10 4.20 -2 -36 -4 14.00 12.00 -2 -36 4 -5.00 12.30 -36 2 4 3.10 13.00 36 -2 4 -9.20 8.10 4 36 -4 0.90 4.30 -4 -36 -4 4.50 11.40 36 -4 4 3.50 8.80 -4 -36 4 -19.00 12.30 -36 4 4 3.60 14.10 0 1 -5 23.10 3.00 0 -1 -5 48.70 7.80 1 -2 -5 149.79 10.10 -1 2 -5 137.99 8.60 -2 1 -5 139.39 9.30 1 2 -5 150.18 9.00 2 -1 -5 136.69 9.70 -1 -2 -5 147.79 10.20 2 -3 -5 10.40 6.40 -2 3 -5 3.10 2.30 3 2 -5 3.50 2.30 0 3 -5 95.59 7.90 3 0 -5 100.99 9.00 -3 0 -5 93.29 8.00 0 -3 -5 97.69 9.30 2 3 -5 21.20 2.90 3 -2 -5 31.00 7.00 -3 2 -5 21.40 3.10 -2 -3 -5 47.00 8.20 -4 -3 -5 18.20 7.20 3 -4 -5 17.80 7.00 -3 4 -5 5.40 2.40 4 3 -5 7.20 2.30 1 -4 -5 131.69 10.00 -1 4 -5 129.49 8.50 4 -1 -5 12.60 6.10 1 4 -5 3.10 2.20 -1 -4 -5 10.70 6.60 -4 1 -5 4.50 2.40 3 4 -5 193.38 9.30 4 -3 -5 186.68 10.50 -3 -4 -5 198.98 11.20 -4 3 -5 195.98 10.00 3 4 -5 192.68 9.10 -4 5 -5 11.20 2.50 -5 -4 -5 30.20 7.40 4 -5 -5 25.30 7.20 5 4 -5 11.40 2.40 -2 5 -5 20.20 2.80 0 -5 -5 38.90 8.00 5 0 -5 35.40 6.70 -5 0 -5 18.70 3.00 0 5 -5 18.10 2.70 2 5 -5 11.40 3.70 5 -2 -5 12.60 6.30 2 5 -5 4.10 2.20 -5 2 -5 6.90 2.40 -2 -5 -5 6.60 6.50 -4 -5 -5 55.49 8.20 4 5 -5 54.19 7.50 -5 4 -5 29.90 3.30 4 5 -5 28.60 3.00 5 -4 -5 56.69 8.10 5 -6 -5 44.20 7.40 6 5 -5 23.30 2.70 -5 6 -5 22.30 3.00 -6 -5 -5 49.99 8.20 -3 6 -5 140.99 8.70 -6 -3 -5 138.59 10.00 3 -6 -5 157.18 10.40 -1 6 -5 6.10 2.20 6 1 -5 5.40 5.50 -6 -1 -5 2.60 2.40 1 -6 -5 8.50 7.00 -6 1 -5 145.59 8.90 -1 -6 -5 151.48 10.60 1 6 -5 162.68 8.80 6 -1 -5 151.38 9.60 1 6 -5 147.39 6.80 3 6 -5 2.80 2.10 -6 3 -5 3.10 2.30 -3 -6 -5 1.50 6.50 6 -3 -5 9.70 6.30 6 -5 -5 72.79 8.50 5 6 -5 57.19 6.60 -5 -6 -5 72.59 9.00 -5 -6 5 61.59 6.70 7 6 -5 65.29 6.50 -6 7 -5 75.89 7.70 6 -7 -5 87.09 9.20 -7 -6 -5 81.49 9.40 -7 -6 5 71.79 7.40 6 -7 5 73.69 5.30 4 -7 -5 7.10 6.50 -7 -4 -5 5.70 6.50 -4 7 -5 3.70 2.20 7 4 -5 6.00 2.20 -7 -4 5 14.50 5.20 2 -7 -5 398.26 15.70 7 2 -5 399.76 13.90 -2 7 -5 402.76 14.10 -7 -2 5 402.36 15.50 0 7 -5 3.20 2.10 0 7 -5 4.90 2.60 -7 0 -5 3.30 2.40 0 -7 -5 5.20 6.90 7 0 -5 7.50 5.50 -7 2 -5 226.88 10.90 2 7 -5 241.88 10.30 7 -2 -5 248.58 11.20 -2 -7 -5 226.98 12.30 -4 -7 -5 10.30 7.10 7 -4 -5 15.60 6.20 4 7 -5 6.30 2.20 -7 4 -5 6.80 2.50 -4 -7 5 15.40 4.30 -4 -7 5 12.90 2.90 -6 -7 -5 30.30 8.00 7 -6 -5 38.50 7.40 -6 -7 5 34.80 5.80 7 -6 5 39.80 4.80 -8 -7 -5 212.78 12.40 -7 8 -5 200.18 10.70 8 7 -5 192.68 9.00 7 -8 -5 214.18 11.80 7 -8 5 206.78 7.30 -8 -7 5 211.78 10.90 -8 -5 -5 84.59 9.60 -5 8 -5 78.19 7.60 8 5 -5 83.99 6.80 5 -8 -5 85.69 9.50 -8 -5 5 92.99 8.30 8 3 -5 11.80 5.30 3 -8 -5 9.30 6.90 -3 8 -5 8.30 2.30 -8 -3 5 17.50 5.60 8 1 -5 27.80 6.10 1 -8 -5 31.20 8.00 -8 -1 -5 11.40 2.90 -1 8 -5 13.30 2.50 -8 -1 5 24.50 6.30 8 -1 -5 391.96 13.70 -1 -8 -5 378.56 15.70 -8 1 -5 404.46 14.20 1 8 -5 365.26 13.10 8 -3 -5 17.80 6.20 -3 -8 -5 2.10 7.30 -8 3 -5 0.50 2.30 3 8 -5 3.10 2.10 -5 -8 -5 13.50 7.40 -8 5 -5 3.10 2.30 8 -5 -5 5.30 6.30 5 8 -5 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8 5 59.99 12.20 -21 -6 -5 19.70 10.50 6 -21 -5 19.90 10.50 -6 21 -5 6.10 3.40 6 -21 5 10.70 9.90 4 -21 -5 -4.30 9.30 -4 21 -5 -1.40 2.90 -21 -4 5 -1.10 7.00 4 -21 5 8.40 9.50 21 4 5 11.50 7.90 2 -21 -5 0.20 9.60 21 2 -5 2.90 4.80 -21 -2 -5 -1.70 4.00 -2 21 -5 3.80 3.10 2 -21 5 6.70 9.60 -21 -2 5 4.60 8.10 21 2 5 0.70 7.10 0 -21 -5 60.39 11.70 21 0 -5 54.29 7.00 0 21 -5 27.40 4.40 -21 0 -5 35.20 5.20 -21 0 5 48.30 11.00 0 -21 5 59.49 11.40 21 0 5 57.59 9.80 -21 2 -5 -2.20 3.70 21 -2 -5 5.00 6.20 -2 -21 -5 -1.40 9.50 2 21 -5 0.90 2.80 -21 2 5 -2.70 7.50 -2 -21 5 2.60 9.20 4 21 -5 4.60 3.00 -4 -21 -5 13.00 10.10 21 -4 -5 5.50 7.00 -21 4 -5 5.80 3.90 21 -4 5 6.50 7.10 -4 -21 5 4.10 9.30 -21 4 5 0.10 8.00 6 21 -5 52.69 5.60 21 -6 -5 57.39 9.30 -6 -21 -5 56.79 12.10 21 -6 5 54.19 8.80 -21 6 5 50.19 11.90 -6 -21 5 66.59 11.40 21 -8 -5 8.40 8.00 8 21 -5 0.90 2.90 -8 -21 -5 7.30 10.50 8 21 -5 3.80 4.70 -21 8 -5 0.20 3.80 -21 8 5 8.00 10.00 -8 -21 5 -1.60 9.10 10 21 -5 0.30 2.90 -21 10 -5 2.90 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5 7.90 8.50 1 26 -5 6.00 3.90 -26 1 -5 -5.90 4.60 -1 -26 -5 6.90 11.20 26 -1 5 11.40 8.60 -1 -26 5 5.70 11.10 -26 1 5 0.20 9.10 -3 -26 -5 15.40 11.60 3 26 -5 3.30 3.70 -26 3 -5 -0.50 4.80 -3 -26 5 -1.90 10.50 -26 3 5 6.40 9.60 26 -3 5 16.90 8.30 5 26 -5 6.70 4.00 -26 5 -5 5.30 4.80 -5 -26 -5 11.40 11.10 -5 -26 5 14.50 11.30 -26 5 5 12.50 11.10 -7 -26 -5 9.10 10.40 26 -7 -5 6.20 9.30 -26 7 -5 -2.70 4.60 7 26 -5 2.40 3.60 -7 -26 5 0.30 10.70 26 -7 5 4.30 6.80 -26 7 5 1.70 10.90 -9 -26 -5 14.70 10.60 9 26 -5 8.90 4.10 -26 9 -5 3.80 4.80 26 -9 -5 19.80 9.10 26 -9 5 7.30 6.90 -26 9 5 30.30 13.90 -9 -26 5 11.70 11.00 -11 -26 -5 7.90 9.70 -26 11 -5 3.70 4.50 26 -11 -5 5.60 8.90 11 26 -5 4.60 3.60 -11 -26 5 -14.70 9.60 -26 11 5 8.80 13.40 -13 -26 -5 3.40 9.20 13 26 -5 -4.20 3.30 26 -13 -5 12.70 9.80 -26 13 -5 -4.00 4.10 -26 15 -5 29.00 9.60 -15 -26 -5 14.90 9.60 26 -15 -5 28.40 11.10 -26 17 -5 15.10 15.60 -26 17 -5 6.40 4.80 26 -17 -5 20.20 11.50 -17 -26 -5 19.00 10.00 -26 19 -5 -3.80 4.30 26 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48.50 13.20 -27 -2 5 49.00 12.60 27 2 5 37.10 9.70 2 -27 5 46.30 12.70 0 -27 -5 -9.70 10.60 -27 0 -5 -11.50 4.80 0 27 -5 -0.90 3.50 0 -27 5 -6.70 10.40 27 0 5 8.80 8.70 -27 0 5 12.50 10.30 2 27 -5 9.20 4.20 -27 2 -5 5.10 5.10 -2 -27 -5 20.50 11.60 -2 -27 5 18.20 11.50 -27 2 5 15.10 10.60 27 -2 5 20.50 9.20 -4 -27 -5 46.10 12.70 27 -4 5 39.80 10.10 -4 -27 5 48.70 12.80 -27 4 5 50.39 13.40 -6 -27 -5 50.99 12.80 27 -6 5 47.80 8.90 -6 -27 5 59.19 13.10 -27 6 5 32.00 13.40 -27 8 -5 11.80 5.00 8 27 -5 17.00 4.40 -8 -27 -5 26.90 11.50 27 -8 5 34.30 8.10 -27 8 5 25.80 13.60 -8 -27 5 27.20 11.50 27 -10 -5 17.90 10.20 -27 10 -5 -0.60 4.40 10 27 -5 -0.90 3.40 -10 -27 -5 5.10 10.00 -10 -27 5 -0.60 10.20 27 -10 5 0.70 6.30 -27 10 5 4.10 12.90 12 27 -5 0.40 3.60 -27 12 -5 -3.30 4.40 27 -12 -5 23.30 10.30 -12 -27 -5 18.70 10.50 -27 12 5 -7.00 13.30 -14 -27 -5 7.70 9.30 27 -14 -5 9.40 10.30 -27 14 -5 4.10 4.70 -27 16 -5 20.70 10.00 27 -16 -5 8.60 11.20 -16 -27 -5 13.50 9.80 -27 16 -5 -0.90 4.70 27 -18 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23.70 10.90 3 -28 5 0.20 10.80 28 3 5 -0.20 8.40 -1 28 -5 4.50 3.80 1 -28 -5 7.60 9.90 28 1 5 1.30 8.20 -28 -1 5 0.00 9.40 1 -28 5 5.50 11.10 1 28 -5 1.50 3.60 -1 -28 -5 3.20 10.90 28 -1 5 5.30 8.60 -1 -28 5 -0.80 10.30 -28 1 5 6.70 10.00 3 28 -5 5.40 3.80 -28 3 -5 1.50 4.90 -3 -28 -5 22.10 11.10 -28 3 5 18.00 11.00 28 -3 5 18.90 9.00 -3 -28 5 15.30 11.60 -28 5 -5 -1.60 4.60 -5 -28 -5 12.50 10.80 5 28 -5 4.20 3.70 -28 5 5 11.70 11.80 -5 -28 5 9.90 11.00 7 28 -5 9.50 4.20 -28 7 -5 8.20 5.00 -7 -28 -5 37.70 11.70 -28 7 5 28.90 12.80 28 -7 5 26.10 7.80 -7 -28 5 23.90 11.90 -9 -28 -5 8.90 10.00 9 28 -5 0.10 3.50 -28 9 -5 1.10 4.60 -9 -28 5 -6.60 10.50 28 -9 5 7.40 6.90 -28 9 5 -1.90 12.30 11 28 -5 -1.70 3.40 -28 11 -5 -3.70 4.50 -11 -28 -5 9.90 10.00 -11 -28 5 -13.00 10.30 -28 11 5 9.90 14.10 28 -13 -5 16.30 12.00 -13 -28 -5 9.20 10.10 -28 13 -5 -3.00 4.80 28 -15 -5 0.20 10.50 -28 15 -5 18.80 10.20 -15 -28 -5 9.80 10.00 -28 15 -5 -3.70 4.60 -28 17 -5 -1.50 5.10 28 -17 -5 14.20 11.70 -28 19 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37.20 10.60 -17 -7 6 45.90 9.70 -5 17 -6 3.20 2.80 -17 -5 -6 10.80 9.70 17 5 -6 14.30 6.60 5 -17 -6 13.90 9.60 17 5 6 18.80 8.90 -17 -5 6 13.20 7.40 3 -17 -6 3.20 8.60 -3 17 -6 0.90 2.60 17 3 -6 8.40 6.30 -17 -3 6 2.90 6.80 17 3 6 1.60 7.60 1 -17 -6 27.80 9.90 17 1 -6 35.50 7.20 -17 -1 -6 11.90 4.10 -17 -1 6 24.20 8.90 17 1 6 23.00 8.40 17 -1 -6 43.00 7.80 1 17 -6 18.10 3.60 -1 -17 -6 31.00 10.40 -17 1 -6 22.40 4.40 -17 1 6 31.60 9.40 -3 -17 -6 -5.60 8.60 3 17 -6 -0.10 2.50 -17 3 -6 -0.80 3.40 17 -3 -6 -4.10 6.70 -17 3 6 -2.90 7.30 17 -3 6 4.00 6.40 -5 -17 -6 93.49 12.90 17 -5 -6 88.79 10.60 -17 5 6 88.89 13.60 17 -5 6 87.39 9.20 -5 -17 6 76.19 6.40 7 17 -6 4.40 2.80 -17 7 -6 5.20 3.80 -7 -17 -6 4.70 9.80 17 -7 -6 11.80 8.10 17 -7 6 3.00 5.80 -9 -17 -6 13.40 10.50 17 -9 -6 23.10 9.10 9 17 -6 10.60 3.10 -17 9 -6 10.80 4.00 17 -9 6 17.80 6.40 -17 11 -6 227.78 14.80 -11 -17 -6 214.48 16.40 11 17 -6 210.08 11.90 17 -11 -6 220.48 14.90 17 -11 6 210.28 10.40 13 17 -6 1.80 2.70 -17 13 -6 2.10 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102.59 14.90 8 -14 -8 81.79 12.90 14 8 -8 101.79 11.70 -14 -8 8 93.39 12.40 -6 14 -8 112.39 12.10 6 -14 -8 124.69 14.70 14 6 -8 103.19 12.60 -14 -6 -8 135.19 15.60 -14 -6 8 101.29 12.80 4 -14 -8 11.70 10.80 -14 -4 -8 18.00 11.30 14 4 -8 15.70 9.20 -4 14 -8 10.20 3.80 -14 -4 8 14.70 9.00 14 2 -8 105.59 12.50 -2 14 -8 99.89 11.40 2 -14 -8 126.39 14.90 14 0 -8 25.00 9.50 0 -14 -8 33.70 12.40 -14 0 -8 8.90 4.60 -2 -14 -8 14.90 11.10 14 -2 -8 5.50 9.10 -14 2 -8 -0.20 4.00 2 14 -8 4.90 3.30 4 14 -8 6.20 3.50 -14 4 -8 9.00 4.30 -4 -14 -8 23.80 12.60 14 -4 -8 13.60 9.70 14 -4 8 12.70 7.90 -4 -14 8 7.60 3.80 -14 6 -8 41.90 5.70 6 14 -8 41.70 5.10 8 14 -8 3.30 3.50 14 -8 -8 2.00 10.10 -8 -14 -8 10.80 12.10 -14 8 -8 5.10 4.20 14 -8 8 4.60 6.10 -14 10 -8 3.30 4.20 14 -10 -8 17.80 10.50 -10 -14 -8 15.60 12.50 10 14 -8 2.90 3.60 -10 -14 8 7.30 7.10 12 14 -8 26.70 4.60 -14 12 -8 20.50 5.20 14 -12 -8 39.40 11.50 -12 -14 -8 42.10 13.90 -12 -14 8 49.60 9.90 14 -14 -8 83.59 14.10 -14 -14 -8 91.29 15.90 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26.10 4.70 9 -4 -9 58.79 12.00 -9 4 -9 22.30 4.80 -9 6 -9 14.70 4.40 6 9 -9 12.90 4.20 9 -6 -9 24.00 11.20 -6 -9 -9 19.20 12.10 -8 -9 -9 -4.00 11.50 -9 8 -9 6.80 4.20 8 9 -9 0.40 3.80 9 -8 -9 11.30 10.90 -9 10 -9 9.70 4.30 10 9 -9 12.80 4.40 -10 -9 -9 22.20 12.70 9 -10 -9 9.40 11.20 9 -10 9 24.00 6.20 7 -10 -9 7.80 11.10 -10 -7 -9 9.20 11.60 -7 10 -9 5.10 4.00 5 -10 -9 163.28 15.70 -5 10 -9 182.18 13.80 10 5 -9 192.58 14.70 -10 -5 -9 182.38 16.40 -10 -3 -9 82.09 13.80 3 -10 -9 100.79 14.20 10 3 -9 97.09 12.60 10 1 -9 20.60 10.00 1 -10 -9 24.60 12.10 -1 10 -9 17.40 4.30 -10 1 -9 24.20 4.80 1 10 -9 26.20 4.80 -1 -10 -9 48.30 12.90 10 -1 -9 51.89 11.40 -3 -10 -9 20.50 12.40 3 10 -9 13.40 4.20 -10 3 -9 9.10 4.50 10 -3 -9 29.00 11.00 10 -5 -9 -4.90 10.30 -5 -10 -9 17.90 12.30 -10 5 -9 3.60 4.20 5 10 -9 4.60 3.90 -7 -10 -9 0.40 11.70 10 -7 -9 -9.80 9.70 -10 7 -9 -3.80 3.90 7 10 -9 0.00 3.70 9 10 -9 10.50 4.40 -9 -10 -9 20.20 13.20 -10 9 -9 12.90 4.60 10 -9 -9 14.50 12.00 10 -9 9 31.10 7.30 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4.60 11.90 4 1 -11 -1.80 11.40 -4 -1 -11 23.00 13.00 4 -1 -11 7.60 12.00 -1 -4 -11 5.80 12.10 -3 -4 -11 6.60 12.70 4 -3 -11 -0.30 11.90 -4 5 -11 21.40 5.60 -5 -4 -11 44.30 14.50 4 -5 -11 31.10 13.20 -2 5 -11 12.70 5.10 2 -5 -11 22.20 13.40 5 2 -11 34.40 12.70 -5 -2 -11 19.30 12.60 0 5 -11 0.80 4.70 0 -5 -11 12.00 13.00 5 0 -11 22.20 12.90 -2 -5 -11 47.60 13.70 5 -2 -11 50.49 13.70 -5 4 -11 130.89 15.30 -4 -5 -11 155.58 18.20 5 -4 -11 133.49 16.80 5 -6 -11 3.80 13.30 -6 -5 -11 10.60 12.70 -5 6 -11 2.80 5.10 -6 -3 -11 127.89 17.10 3 -6 -11 133.59 17.00 6 3 -11 119.69 16.30 -1 6 -11 -0.30 4.90 1 -6 -11 23.00 13.50 -6 -1 -11 18.50 12.70 6 1 -11 15.90 12.60 6 -1 -11 34.20 12.60 -1 -6 -11 22.10 13.10 1 6 -11 17.20 5.40 -3 -6 -11 22.50 13.10 -6 3 -11 9.90 5.10 6 -3 -11 20.80 13.00 6 -5 -11 55.59 14.00 -6 5 -11 25.70 5.90 -5 -6 -11 45.30 14.10 -7 -6 -11 68.09 15.20 6 -7 -11 82.99 16.00 -6 7 -11 42.10 6.70 7 4 -11 1.40 11.70 -7 -4 -11 8.90 13.40 -4 7 -11 5.70 5.00 4 -7 -11 21.80 14.00 2 -7 -11 -14.00 12.20 -7 -2 -11 12.20 12.90 -2 7 -11 3.60 5.00 7 2 -11 -2.40 11.50 0 -7 -11 1.90 12.80 0 7 -11 0.10 4.90 7 0 -11 5.60 11.70 2 7 -11 2.20 4.70 -2 -7 -11 8.20 13.40 7 -2 -11 10.90 12.10 -7 4 -11 8.80 5.40 7 -4 -11 15.70 12.70 4 7 -11 7.30 5.10 -4 -7 -11 11.00 13.10 -7 6 -11 1.90 5.00 7 -6 -11 6.10 12.70 -6 -7 -11 7.50 12.80 7 -8 -11 8.10 13.20 -7 8 -11 -0.30 5.00 -8 -7 -11 -5.00 12.80 -5 8 -11 4.10 5.20 8 5 -11 7.30 12.10 -8 -5 -11 10.20 13.50 5 -8 -11 -0.70 12.90 8 3 -11 -2.40 12.20 -3 8 -11 1.20 4.80 3 -8 -11 -3.50 13.10 -8 -3 -11 8.40 12.70 -1 8 -11 -2.80 4.70 8 1 -11 -2.00 12.20 1 -8 -11 -9.50 13.10 -1 -8 -11 5.90 13.00 8 -1 -11 10.50 12.60 1 8 -11 4.00 5.00 8 -3 -11 79.99 15.10 -8 3 -11 36.50 6.50 -3 -8 -11 73.19 16.20 3 8 -11 41.30 6.30 -8 5 -11 13.10 5.60 -5 -8 -11 43.00 15.10 8 -5 -11 46.80 14.40 5 8 -11 18.70 5.70 8 -7 -11 77.99 15.80 -7 -8 -11 81.89 17.10 -9 -8 -11 22.10 15.20 -8 9 -11 19.30 5.80 8 -9 -11 27.50 13.70 6 -9 -11 4.50 12.90 -9 -6 -11 11.30 13.20 9 6 -11 2.20 11.70 -6 9 -11 1.90 4.90 9 4 -11 13.00 11.90 4 -9 -11 9.50 13.90 -9 -4 -11 10.80 14.00 -4 9 -11 2.70 5.10 2 -9 -11 24.80 14.50 9 2 -11 25.70 12.50 -9 -2 -11 21.30 13.40 -2 9 -11 12.90 5.40 0 -9 -11 59.09 15.80 9 0 -11 59.79 14.10 2 9 -11 5.10 5.00 -2 -9 -11 0.80 13.40 9 -2 -11 9.80 12.20 -9 2 -11 0.00 5.20 -9 4 -11 9.40 5.40 4 9 -11 10.90 5.20 9 -4 -11 13.30 12.80 -4 -9 -11 18.20 14.60 -9 6 -11 17.70 5.70 6 9 -11 17.70 5.50 -6 -9 -11 46.40 15.10 9 -6 -11 38.50 14.20 9 -8 -11 -5.80 13.30 -8 -9 -11 21.50 15.20 -9 8 -11 4.60 5.30 9 -10 -11 47.80 15.40 -10 -9 -11 36.70 15.70 -9 10 -11 21.70 6.10 7 -10 -11 36.10 14.50 -7 10 -11 23.50 6.00 10 7 -11 66.49 14.20 -10 -7 -11 39.40 15.40 -5 10 -11 4.20 5.10 10 5 -11 0.10 11.60 -10 -5 -11 -3.80 13.10 5 -10 -11 0.20 13.30 -3 10 -11 4.40 5.10 3 -10 -11 36.00 14.60 -10 -3 -11 21.70 14.00 10 3 -11 7.90 11.50 1 -10 -11 18.70 14.50 -1 10 -11 11.50 5.40 10 1 -11 35.10 13.00 -1 -10 -11 10.90 14.60 10 -1 -11 11.50 12.30 1 10 -11 8.00 5.20 10 -3 -11 48.90 14.10 3 10 -11 25.30 6.00 -10 3 -11 22.20 6.00 -3 -10 -11 61.09 15.90 5 10 -11 9.10 5.20 -10 5 -11 5.20 5.70 10 -5 -11 5.30 12.90 -5 -10 -11 5.10 14.60 -10 7 -11 4.30 5.40 -7 -10 -11 14.10 14.40 7 10 -11 1.10 4.80 10 -7 -11 -3.70 12.90 10 -9 -11 156.68 18.00 -9 -10 -11 169.18 20.40 -10 11 -11 -2.50 5.00 10 -11 -11 2.70 13.00 -11 -10 -11 -2.90 15.30 8 -11 -11 146.19 18.70 -11 -8 -11 127.09 18.90 11 8 -11 144.19 16.90 11 6 -11 72.29 14.70 6 -11 -11 79.59 15.90 -11 -6 -11 84.99 17.20 -11 -4 -11 1.30 13.50 -4 11 -11 1.10 4.80 4 -11 -11 -1.80 13.30 11 4 -11 5.00 12.00 2 -11 -11 15.60 14.10 -2 11 -11 10.30 5.30 -11 -2 -11 14.80 13.40 11 2 -11 6.60 12.00 11 0 -11 22.00 12.30 0 -11 -11 7.80 13.90 0 11 -11 7.60 5.20 -11 2 -11 0.60 5.40 11 -2 -11 -15.70 12.10 -2 -11 -11 10.80 14.20 2 11 -11 -2.50 4.80 -4 -11 -11 33.70 15.20 -11 4 -11 14.20 5.90 11 -4 -11 19.50 13.20 4 11 -11 11.80 5.30 -6 -11 -11 6.80 14.80 6 11 -11 0.90 5.00 -11 6 -11 6.00 5.60 11 -6 -11 7.90 13.40 -8 -11 -11 19.80 16.10 8 11 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-11 30.60 16.70 11 12 -11 16.70 5.80 -12 11 -11 23.50 6.40 12 -11 -11 47.90 14.60 12 -13 -11 47.70 13.90 -13 -12 -11 51.79 17.00 -12 13 -11 26.80 6.50 -13 -10 -11 -10.00 14.80 10 -13 -11 -2.80 12.00 -10 13 -11 4.00 5.20 -8 13 -11 0.30 5.00 8 -13 -11 -4.70 12.90 13 8 -11 1.60 12.30 -13 -8 -11 2.60 14.40 -6 13 -11 0.20 5.00 6 -13 -11 -0.20 14.20 13 6 -11 7.20 12.40 -13 -6 -11 2.20 13.50 -13 -4 -11 131.19 19.00 13 4 -11 137.69 16.70 4 -13 -11 116.69 18.10 -4 13 -11 133.49 15.60 2 -13 -11 -4.20 14.10 -2 13 -11 -0.50 4.80 13 2 -11 -17.20 12.10 13 0 -11 8.00 12.90 0 13 -11 14.80 5.70 0 -13 -11 16.20 14.80 -13 2 -11 9.70 6.00 -2 -13 -11 -1.70 13.70 13 -2 -11 7.60 12.80 2 13 -11 7.00 5.20 13 -4 -11 166.78 18.60 -4 -13 -11 184.78 21.60 4 13 -11 176.78 17.10 -13 4 -11 191.68 18.40 -6 -13 -11 34.60 16.80 6 13 -11 13.80 5.60 13 -6 -11 28.30 13.80 -13 6 -11 11.50 6.10 13 -8 -11 30.50 14.60 8 13 -11 12.60 5.50 -13 8 -11 11.20 6.30 -8 -13 -11 38.70 16.90 13 -8 11 33.70 9.90 13 -10 -11 -2.20 12.90 10 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8 2 -12 -1.80 12.50 -2 8 -12 3.40 5.50 -8 -2 -12 -4.10 14.00 2 -8 -12 6.20 14.80 0 -8 -12 63.89 16.50 8 0 -12 48.10 14.90 0 8 -12 28.80 6.80 8 -2 -12 48.60 15.40 -2 -8 -12 35.30 15.40 2 8 -12 18.80 6.20 8 -4 -12 56.89 15.50 -4 -8 -12 43.70 16.00 4 8 -12 22.50 6.50 -8 4 -12 16.60 6.20 -6 -8 -12 22.30 14.90 -8 6 -12 9.60 6.10 8 -6 -12 11.90 14.40 -8 8 -12 10.80 6.10 8 -8 -12 32.40 15.70 -8 -8 -12 35.30 15.90 -7 9 -12 57.79 7.80 -9 -7 -12 97.29 18.40 7 -9 -12 93.49 16.90 9 7 -12 103.79 16.90 9 5 -12 61.49 15.70 -9 -5 -12 57.89 16.20 -5 9 -12 31.70 6.90 5 -9 -12 62.29 16.40 9 3 -12 77.59 16.30 3 -9 -12 101.49 18.30 -9 -3 -12 88.49 17.20 9 1 -12 36.80 14.30 -9 -1 -12 25.20 14.80 1 -9 -12 26.70 15.50 -1 9 -12 20.50 6.40 9 -1 -12 11.70 14.00 -1 -9 -12 15.90 15.50 1 9 -12 8.10 5.70 -9 3 -12 2.90 5.80 -3 -9 -12 24.80 15.30 3 9 -12 2.20 5.40 9 -3 -12 -2.90 14.20 -5 -9 -12 153.68 19.60 -9 5 -12 80.49 8.80 5 9 -12 69.59 8.20 -7 -9 -12 4.80 14.90 -9 7 -12 5.10 6.00 9 -7 -12 10.90 13.90 -9 9 -12 47.20 7.60 -9 -9 -12 85.79 18.30 9 -9 -12 89.99 16.70 8 -10 -12 9.00 13.80 -8 10 -12 4.40 5.70 10 8 -12 6.90 13.00 -10 -8 -12 -1.40 14.40 10 6 -12 21.90 14.10 -10 -6 -12 26.70 15.00 -6 10 -12 15.30 6.20 6 -10 -12 21.70 14.20 -10 -4 -12 15.50 15.10 10 4 -12 42.40 14.50 -4 10 -12 10.60 6.00 4 -10 -12 26.10 15.50 -10 -2 -12 119.19 18.50 2 -10 -12 103.79 18.40 10 2 -12 95.49 16.30 0 10 -12 218.88 18.70 10 0 -12 206.48 20.60 0 -10 -12 187.48 20.70 -2 -10 -12 18.30 16.30 2 10 -12 12.40 6.10 10 -2 -12 19.30 14.40 -10 4 -12 7.20 6.10 -4 -10 -12 24.90 15.90 4 10 -12 9.80 6.00 10 -4 -12 30.80 15.20 -6 -10 -12 85.39 17.90 -10 6 -12 61.79 8.10 10 -6 -12 109.29 17.40 6 10 -12 63.29 8.10 10 -8 -12 6.50 13.90 -8 -10 -12 9.20 15.00 -10 8 -12 0.50 5.80 10 -10 -12 19.70 13.70 -10 -10 -12 13.80 15.60 -10 10 -12 13.40 6.10 9 -11 -12 10.60 13.80 -11 -9 -12 -8.90 15.10 -9 11 -12 5.70 5.70 11 7 -12 140.89 17.70 7 -11 -12 115.19 17.70 -11 -7 -12 120.49 18.70 11 5 -12 27.00 14.00 5 -11 -12 27.30 15.40 -11 -5 -12 33.60 15.40 -5 11 -12 12.80 6.10 -11 -3 -12 33.10 15.20 11 3 -12 28.50 13.90 -3 11 -12 10.20 6.00 3 -11 -12 39.40 15.90 1 -11 -12 -6.40 14.50 11 1 -12 3.10 13.80 -1 11 -12 3.10 5.80 -1 -11 -12 182.68 21.00 1 11 -12 202.08 19.50 11 -1 -12 204.38 20.40 -11 3 -12 21.60 6.80 -3 -11 -12 28.00 16.20 3 11 -12 23.30 6.40 11 -3 -12 37.40 15.40 5 11 -12 12.70 6.00 -11 5 -12 9.60 6.30 11 -5 -12 -4.30 13.50 -5 -11 -12 38.80 17.20 7 11 -12 4.50 5.80 11 -7 -12 10.20 13.70 -7 -11 -12 11.00 15.60 -11 7 -12 8.10 6.20 -9 -11 -12 91.39 18.40 11 -9 -12 100.89 16.80 -11 11 -12 28.80 6.80 11 -11 -12 53.89 15.00 -11 -11 -12 61.89 17.00 -12 -10 -12 53.49 16.20 10 -12 -12 44.40 14.00 -12 -8 -12 2.00 14.70 8 -12 -12 12.90 13.80 -8 12 -12 6.90 5.70 12 8 -12 23.70 13.10 12 6 -12 8.40 13.20 6 -12 -12 24.90 14.70 -12 -6 -12 8.70 14.70 -6 12 -12 6.40 5.60 -4 12 -12 21.70 6.30 4 -12 -12 31.50 14.90 -12 -4 -12 37.40 15.90 12 4 -12 34.80 14.50 2 -12 -12 12.10 14.90 -12 -2 -12 7.00 14.30 -2 12 -12 2.60 5.40 12 2 -12 7.60 13.80 12 0 -12 -5.80 13.10 0 12 -12 -1.30 5.60 0 -12 -12 -12.20 14.50 2 12 -12 190.98 19.20 -2 -12 -12 182.48 21.90 12 -2 -12 166.48 19.70 12 -4 -12 21.60 14.60 -4 -12 -12 8.20 15.50 -12 4 -12 7.70 6.30 4 12 -12 5.90 5.80 12 -6 -12 9.70 13.30 6 12 -12 8.20 5.70 -12 6 -12 7.50 6.30 -6 -12 -12 25.30 16.30 8 12 -12 7.40 5.70 12 -8 -12 22.70 13.70 -8 -12 -12 31.70 16.40 -12 8 -12 11.90 6.40 12 -10 -12 31.30 14.00 -10 -12 -12 29.50 15.80 -12 12 -12 -4.10 5.20 12 -12 -12 6.30 11.80 -12 -12 -12 0.70 14.70 -13 -11 -12 27.00 14.90 11 -13 -12 20.90 12.80 -11 13 -12 13.90 6.00 -9 13 -12 5.20 5.40 13 9 -12 18.30 12.10 -13 -9 -12 -8.50 14.00 9 -13 -12 -0.10 12.10 13 7 -12 17.00 12.80 -13 -7 -12 11.00 14.50 7 -13 -12 19.50 14.30 -7 13 -12 7.80 5.80 -13 -5 -12 -4.80 13.70 13 5 -12 7.40 12.90 5 -13 -12 -7.20 14.10 -5 13 -12 4.60 5.50 3 -13 -12 96.19 17.70 -13 -3 -12 87.09 17.60 13 3 -12 101.39 16.60 -1 13 -12 14.20 6.00 1 -13 -12 3.40 14.40 13 1 -12 18.60 13.70 13 -1 -12 161.08 18.40 1 13 -12 90.49 9.20 -1 -13 -12 165.08 20.90 -3 -13 -12 110.89 19.20 3 13 -12 58.69 7.90 13 -3 -12 97.79 16.40 -13 3 -12 52.09 8.20 -5 -13 -12 8.20 15.00 5 13 -12 -0.40 5.40 13 -5 -12 15.20 13.90 -13 5 -12 2.60 6.30 -7 -13 -12 73.79 17.70 7 13 -12 32.20 6.70 13 -7 -12 90.89 16.40 -13 7 -12 45.90 7.80 -13 9 -12 1.50 5.80 9 13 -12 -4.60 5.00 13 -9 -12 23.00 13.70 -9 -13 -12 3.70 14.40 -11 -13 -12 3.20 14.60 -13 11 -12 -6.20 5.40 13 -11 -12 3.20 11.90 -13 -13 -12 6.40 14.70 -13 13 -12 -1.70 5.40 13 -13 -12 20.30 12.60 -12 14 -12 -6.00 5.00 -14 -12 -12 0.10 14.60 12 -14 -12 10.20 12.00 -10 14 -12 -2.50 5.10 14 10 -12 11.40 11.90 -14 -10 -12 -3.60 13.70 10 -14 -12 19.90 12.70 14 8 -12 43.90 13.40 -14 -8 -12 33.40 15.70 -8 14 -12 12.50 5.80 8 -14 -12 32.40 13.70 14 6 -12 16.90 12.40 -14 -6 -12 -2.00 13.70 -6 14 -12 -0.30 5.30 6 -14 -12 18.60 14.10 4 -14 -12 11.70 14.20 14 4 -12 0.40 12.40 -4 14 -12 -4.40 5.10 -14 -4 -12 14.90 15.00 14 2 -12 86.59 15.70 -14 -2 -12 77.79 16.90 2 -14 -12 89.99 17.80 0 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9 13 8 2.2155 0.0059 9 13 10 -16.4242 0.0032 9 13 12 -8.5634 -0.0051 9 13 14 0.3231 0.0110 9 14 1 58.3956 -0.0348 9 14 3 6.7780 0.0302 9 14 5 29.1889 0.0039 9 14 7 18.2810 -0.0199 9 14 9 -21.2765 0.0036 9 14 11 -8.4069 0.0068 9 14 13 4.1001 0.0074 9 14 15 -1.6573 0.0047 9 15 2 1.5307 -0.0304 9 15 4 21.4175 -0.0133 9 15 6 -1.7247 0.0053 9 15 8 -22.8843 0.0121 9 15 10 -4.6366 0.0132 9 15 12 -4.4741 -0.0029 9 15 14 -9.3289 -0.0103 9 16 1 16.1692 -0.0798 9 16 3 34.3744 -0.0469 9 16 5 4.9904 0.0113 9 16 7 -14.4389 0.0145 9 16 9 -2.5186 -0.0022 9 16 11 -20.4125 0.0010 9 16 13 2.7052 -0.0035 9 16 15 17.2093 0.0014 9 17 2 43.7719 -0.0154 9 17 4 -3.3657 0.0194 9 17 6 -1.8837 0.0025 9 17 8 4.0606 -0.0030 9 17 10 -12.5260 0.0040 9 17 12 -2.8504 0.0089 9 17 14 0.4637 0.0173 9 18 1 17.5340 0.1595 9 18 3 -12.0640 0.0180 9 18 5 1.4941 -0.0477 9 18 7 -12.8893 -0.0148 9 18 9 -15.9781 0.0131 9 18 11 12.1920 0.0277 9 18 13 -6.5335 0.0024 9 19 2 0.9089 -0.0181 9 19 4 15.3285 0.0018 9 19 6 1.4971 0.0087 9 19 8 -2.7245 0.0004 9 19 10 10.5561 0.0045 9 19 12 -1.4595 -0.0034 9 19 14 10.0622 -0.0255 9 20 1 2.3914 -0.0088 9 20 3 7.3750 -0.0141 9 20 5 -2.7423 0.0171 9 20 7 -10.8108 -0.0078 9 20 9 -12.1156 -0.0044 9 20 11 7.4221 0.0071 9 20 13 -9.9590 -0.0150 9 21 2 11.6622 0.0213 9 21 4 19.5980 0.0117 9 21 6 2.8055 -0.0147 9 21 8 2.2645 -0.0011 9 21 10 0.8326 0.0069 9 21 12 0.8274 0.0125 9 22 1 -1.2645 -0.0113 9 22 3 -4.1190 -0.0291 9 22 5 -2.3017 -0.0010 9 22 7 -12.5458 0.0302 9 22 9 -1.7132 0.0031 9 22 11 16.6780 -0.0072 9 22 13 11.1350 0.0064 9 23 2 -4.6751 0.0324 9 23 4 -5.0840 -0.0030 9 23 6 -5.9495 0.0084 9 23 8 0.1572 -0.0065 9 23 10 -8.2545 -0.0243 9 23 12 16.2712 0.0240 9 24 1 -4.8715 0.0756 9 24 3 -1.6086 0.0157 9 24 5 5.3263 -0.0014 9 24 7 -2.6938 -0.0163 9 24 9 6.1939 0.0064 9 24 11 2.3517 0.0091 9 25 2 -12.1408 0.0008 9 25 4 2.5029 0.0075 9 25 6 -7.4179 -0.0133 9 25 8 -3.8945 0.0121 9 25 10 13.2897 0.0047 9 25 12 16.1897 0.0559 9 26 1 -12.8943 -0.0930 9 26 3 12.8295 0.0117 9 26 5 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0.0033 10 1 11 -1.7291 -0.0027 10 1 13 4.1174 0.0015 10 1 15 -9.4551 0.0001 10 2 0 -81.1650 0.1550 10 2 2 -64.3828 -0.0574 10 2 4 -21.1757 -0.0173 10 2 6 38.5633 0.0368 10 2 8 41.5454 0.0062 10 2 10 -14.1804 -0.0215 10 2 12 7.8979 -0.0115 10 2 14 4.4747 -0.0003 10 2 16 -5.8539 0.0320 10 3 1 -15.0372 0.0130 10 3 3 -31.3644 0.0187 10 3 5 33.8608 0.0090 10 3 7 14.2789 -0.0037 10 3 9 -10.7703 -0.0001 10 3 11 12.2020 -0.0060 10 3 13 -7.9000 0.0017 10 3 15 -2.6547 -0.0176 10 4 0 -7.7826 0.1757 10 4 4 36.1113 -0.0310 10 4 6 -7.4820 -0.0002 10 4 8 13.0761 0.0008 10 4 10 15.8409 0.0024 10 4 12 -8.3762 -0.0053 10 4 14 3.7961 0.0078 10 4 16 2.4222 -0.0109 10 5 1 -43.8491 0.0669 10 5 3 18.9360 -0.0222 10 5 5 -55.8485 -0.0180 10 5 7 23.2461 0.0113 10 5 9 9.2301 0.0157 10 5 11 -28.9501 -0.0027 10 5 13 -3.8043 -0.0193 10 5 15 3.4175 -0.0151 10 6 0 -81.2451 -0.0381 10 6 2 -59.2178 -0.1025 10 6 4 -27.7942 0.0014 10 6 6 51.8263 0.0466 10 6 8 15.6665 -0.0081 10 6 10 -4.3879 -0.0047 10 6 12 1.8161 0.0052 10 6 14 -3.2026 -0.0003 10 6 16 -1.6879 -0.0262 10 7 1 -38.0517 0.1530 10 7 3 13.0092 -0.0112 10 7 5 28.5682 -0.0290 10 7 7 -3.6385 0.0099 10 7 9 7.5031 0.0109 10 7 11 -0.6079 -0.0051 10 7 13 -11.2347 0.0050 10 7 15 5.4531 -0.0070 10 8 0 -114.4721 0.0614 10 8 2 -12.9338 0.0426 10 8 4 19.2037 -0.0191 10 8 6 0.5517 -0.0095 10 8 8 27.6398 0.0138 10 8 10 1.5932 0.0109 10 8 12 -24.2157 -0.0028 10 8 14 -0.5196 -0.0088 10 8 16 3.1479 0.0309 10 9 1 48.7748 0.0887 10 9 3 3.1544 -0.0192 10 9 5 -4.5375 -0.0305 10 9 7 9.3642 0.0130 10 9 9 -13.5360 0.0052 10 9 11 -11.6522 -0.0127 10 9 13 1.9949 -0.0005 10 9 15 2.0864 0.0022 10 10 0 76.2563 -0.0839 10 10 2 -16.9716 0.0677 10 10 4 23.2160 0.0220 10 10 6 18.1588 -0.0373 10 10 8 0.7537 -0.0103 10 10 10 -10.1213 0.0156 10 10 12 -8.2220 0.0200 10 10 14 -1.9272 -0.0217 10 10 16 0.3711 -0.0185 10 11 1 -26.9788 -0.0210 10 11 3 52.5916 -0.0119 10 11 5 21.2683 -0.0139 10 11 7 -15.7845 -0.0007 10 11 9 -3.3998 0.0054 10 11 11 2.4486 0.0171 10 11 13 0.1776 0.0019 10 11 15 0.5952 -0.0132 10 12 0 -8.0807 -0.2549 10 12 2 48.1384 0.0011 10 12 4 0.5150 0.0302 10 12 6 0.0369 0.0103 10 12 8 13.1072 0.0027 10 12 10 -5.4451 0.0047 10 12 12 -13.6671 0.0028 10 12 14 8.3516 -0.0040 10 13 1 20.0659 -0.0035 10 13 3 -36.3572 0.0298 10 13 5 0.1245 0.0101 10 13 7 1.5348 -0.0063 10 13 9 -28.0862 -0.0091 10 13 11 -11.3534 -0.0029 10 13 13 11.2113 -0.0001 10 13 15 -0.4149 -0.0160 10 14 0 15.3705 0.0491 10 14 2 -17.7867 0.0902 10 14 4 31.4169 -0.0216 10 14 6 25.8808 -0.0335 10 14 8 -28.2804 0.0122 10 14 10 -10.2000 0.0125 10 14 12 -2.9538 -0.0064 10 14 14 -1.6307 -0.0102 10 15 1 22.2579 -0.1253 10 15 3 41.0406 0.0037 10 15 5 5.2391 0.0327 10 15 7 -24.3673 -0.0063 10 15 9 -0.3082 0.0008 10 15 11 -19.3294 0.0072 10 15 13 4.1474 0.0145 10 15 15 -5.6580 -0.0107 10 16 0 52.4477 -0.0469 10 16 2 37.2281 -0.0224 10 16 4 16.5175 0.0418 10 16 6 -2.4458 -0.0086 10 16 8 -2.0073 -0.0154 10 16 10 -22.3606 0.0031 10 16 12 0.9445 -0.0040 10 16 14 0.6221 0.0072 10 17 1 19.8052 -0.0889 10 17 3 7.5913 0.0361 10 17 5 19.7813 0.0207 10 17 7 5.4689 -0.0193 10 17 9 -15.1106 0.0096 10 17 11 11.6021 0.0046 10 17 13 1.5234 0.0208 10 18 0 -2.4809 -0.0131 10 18 2 -12.0751 -0.0768 10 18 4 -2.7399 -0.0148 10 18 6 -9.4665 0.0341 10 18 8 -16.4199 0.0076 10 18 10 5.0612 -0.0157 10 18 12 -2.4656 0.0126 10 18 14 4.8898 -0.0030 10 19 1 6.5932 0.0187 10 19 3 10.3381 0.0068 10 19 5 -11.7078 0.0135 10 19 7 1.4658 0.0095 10 19 9 -0.7667 -0.0090 10 19 11 1.3636 -0.0076 10 19 13 3.0669 -0.0183 10 20 0 5.1923 0.1868 10 20 2 7.3184 0.0177 10 20 4 -13.6168 -0.0242 10 20 6 1.0168 -0.0123 10 20 8 -11.1831 0.0086 10 20 10 -5.9158 0.0057 10 20 12 21.6260 -0.0147 10 20 14 2.2380 -0.0210 10 21 1 -12.1963 -0.0062 10 21 3 5.7275 -0.0231 10 21 5 24.0586 -0.0125 10 21 7 -4.9998 0.0083 10 21 9 -2.8048 0.0075 10 21 11 15.4331 -0.0030 10 21 13 12.2294 -0.0051 10 22 0 -7.8253 -0.0237 10 22 2 2.7034 -0.0596 10 22 4 7.1245 0.0152 10 22 6 -3.3639 0.0262 10 22 8 -1.4469 -0.0173 10 22 10 2.6371 0.0062 10 22 12 5.0445 0.0158 10 23 1 11.0914 0.0908 10 23 3 -0.3782 -0.0082 10 23 5 -16.5996 -0.0121 10 23 7 -5.1987 0.0095 10 23 9 7.6294 0.0065 10 23 11 -3.3664 0.0038 10 23 13 -1.9931 0.0129 10 24 0 12.8311 0.0169 10 24 2 -8.8418 -0.0127 10 24 4 -10.4129 -0.0224 10 24 6 -3.6248 0.0129 10 24 8 2.7300 0.0233 10 24 10 1.9132 0.0046 10 24 12 4.7533 -0.0189 10 25 1 -11.3931 0.0552 10 25 3 1.3225 -0.0126 10 25 5 1.1685 -0.0159 10 25 7 -0.1335 0.0128 10 25 9 0.8326 -0.0094 10 25 11 10.1764 0.0146 10 26 0 -20.9641 0.0183 10 26 2 5.8128 0.0607 10 26 4 -0.9557 -0.0017 10 26 6 -5.6471 -0.0287 10 26 8 -4.2541 0.0017 10 26 10 7.7488 0.0372 10 27 1 11.7230 0.0016 10 27 3 1.4171 -0.0188 10 27 5 -5.4481 -0.0182 10 27 7 5.6729 0.0094 10 27 9 2.8241 0.0410 10 27 11 4.7875 0.0148 10 28 0 -1.7196 -0.1002 10 28 2 -9.0748 0.0045 10 28 4 -7.5580 0.0171 10 28 6 9.6184 0.0091 10 28 8 -1.8484 0.0062 10 28 10 5.2206 0.0073 10 29 1 -5.5017 0.0155 10 29 3 -5.4788 0.0285 10 29 5 -6.6224 0.0176 10 29 7 -3.5397 0.0044 10 29 9 -3.1465 -0.0124 10 30 0 -6.9983 0.0177 10 30 2 -1.6996 0.0239 10 30 4 13.7191 -0.0067 10 30 6 -1.6965 -0.0101 10 30 8 13.5336 0.0166 10 31 1 -2.0813 -0.0469 10 31 3 5.6597 0.0106 10 31 5 3.3290 0.0125 10 31 7 4.1957 0.0155 10 32 0 10.7637 0.0087 10 32 2 -5.0628 0.0271 10 32 4 -3.3261 0.0211 10 32 6 -3.1492 0.0058 10 33 1 -2.9513 -0.0309 10 33 3 -0.1437 0.0152 10 33 5 2.0894 0.0318 10 34 0 0.4298 -0.0174 10 34 2 9.6016 -0.0144 10 34 4 0.3498 0.0147 10 35 1 -1.1185 0.0318 10 35 3 0.6789 0.0256 11 1 2 -53.2867 -0.0506 11 1 4 -35.1236 0.0004 11 1 6 9.3520 0.0092 11 1 8 31.8150 0.0002 11 1 10 -13.6529 0.0123 11 1 12 -0.2259 0.0017 11 1 14 -7.1041 0.0194 11 1 16 -2.3137 0.0116 11 2 1 -113.0118 -0.0934 11 2 3 -44.2722 -0.0601 11 2 5 22.1379 0.0151 11 2 7 35.4495 0.0077 11 2 9 -9.8212 -0.0188 11 2 11 11.7229 0.0058 11 2 13 6.0993 0.0091 11 2 15 -2.8963 0.0068 11 3 2 2.1659 -0.0002 11 3 4 32.4967 0.0147 11 3 6 8.1137 0.0019 11 3 8 -7.1684 -0.0061 11 3 10 30.3524 0.0072 11 3 12 -5.4405 -0.0106 11 3 14 -5.7246 -0.0045 11 3 16 -5.9347 -0.0384 11 4 1 -75.8166 0.1275 11 4 3 -4.5618 0.0151 11 4 5 0.7266 -0.0396 11 4 7 30.3916 -0.0017 11 4 9 36.8458 0.0076 11 4 11 -22.1136 0.0028 11 4 13 -7.1619 -0.0154 11 4 15 0.4256 0.0058 11 5 2 22.7798 0.0094 11 5 4 -23.0667 0.0338 11 5 6 9.7844 0.0099 11 5 8 -1.8218 -0.0044 11 5 10 -29.8505 -0.0157 11 5 12 -7.6786 0.0009 11 5 14 1.3402 -0.0029 11 5 16 -0.8572 0.0027 11 6 1 -24.2830 0.1072 11 6 3 -37.1598 0.0119 11 6 5 27.8103 -0.0068 11 6 7 -1.5966 -0.0013 11 6 9 1.3768 -0.0045 11 6 11 3.6851 0.0017 11 6 13 -2.1409 0.0042 11 6 15 -4.4259 -0.0051 11 7 2 -23.5844 0.0227 11 7 4 22.9843 0.0278 11 7 6 -7.7480 -0.0069 11 7 8 9.5636 -0.0044 11 7 10 7.0707 -0.0044 11 7 12 -11.4277 0.0082 11 7 14 3.4567 -0.0115 11 7 16 15.1731 0.0368 11 8 1 -45.2237 -0.1324 11 8 3 10.2179 -0.0640 11 8 5 15.5565 0.0407 11 8 7 35.7995 0.0191 11 8 9 5.0735 -0.0161 11 8 11 -25.6241 0.0039 11 8 13 3.4606 0.0100 11 8 15 3.3674 -0.0026 11 9 2 5.3625 0.0508 11 9 4 30.8688 0.0033 11 9 6 9.6832 -0.0088 11 9 8 -13.0808 -0.0054 11 9 10 -15.1547 -0.0130 11 9 12 1.8473 0.0041 11 9 14 5.2234 -0.0147 11 9 16 2.0744 -0.0126 11 10 1 -22.4094 0.0807 11 10 3 34.1700 0.0357 11 10 5 8.3514 -0.0090 11 10 7 -4.1999 -0.0032 11 10 9 -5.2243 0.0110 11 10 11 -4.6489 -0.0019 11 10 13 -5.3827 -0.0023 11 10 15 -5.4672 -0.0061 11 11 2 61.4101 0.0161 11 11 4 -3.0814 -0.0048 11 11 6 -3.8899 0.0052 11 11 8 -2.4952 0.0045 11 11 10 -12.5798 -0.0147 11 11 12 -2.7287 -0.0015 11 11 14 -0.6130 0.0107 11 11 16 2.3633 0.0292 11 12 1 80.0255 -0.0614 11 12 3 -6.5000 0.0004 11 12 5 35.6761 0.0270 11 12 7 18.4395 -0.0128 11 12 9 -9.2090 -0.0017 11 12 11 -15.3810 0.0010 11 12 13 -5.2907 0.0009 11 12 15 19.3721 0.0187 11 13 2 -29.2775 0.0072 11 13 4 20.4738 -0.0137 11 13 6 -10.6456 -0.0165 11 13 8 -23.3092 0.0075 11 13 10 -7.9753 0.0140 11 13 12 5.4647 0.0016 11 13 14 -0.0385 -0.0199 11 14 1 -22.5379 -0.1455 11 14 3 30.0703 -0.0344 11 14 5 -10.7944 0.0242 11 14 7 -20.8858 0.0119 11 14 9 1.5329 -0.0002 11 14 11 6.0664 -0.0054 11 14 13 -7.3976 -0.0017 11 14 15 5.2926 0.0150 11 15 2 58.7023 -0.0051 11 15 4 -7.9163 -0.0152 11 15 6 -4.9578 0.0060 11 15 8 3.2696 0.0053 11 15 10 -11.3732 -0.0046 11 15 12 -10.5440 0.0039 11 15 14 5.2009 0.0229 11 16 1 46.1096 0.0857 11 16 3 -8.7792 0.0461 11 16 5 18.0612 -0.0392 11 16 7 -4.1761 -0.0105 11 16 9 -18.2397 0.0187 11 16 11 -6.4663 0.0080 11 16 13 6.2545 -0.0091 11 16 15 -4.1989 -0.0224 11 17 2 2.3377 -0.0443 11 17 4 35.8640 -0.0028 11 17 6 6.8714 0.0121 11 17 8 -17.0294 0.0109 11 17 10 4.8404 0.0183 11 17 12 -7.0518 0.0006 11 17 14 -2.5070 -0.0348 11 18 1 5.1305 -0.0640 11 18 3 17.4791 -0.0058 11 18 5 -10.9262 0.0115 11 18 7 -20.5426 -0.0095 11 18 9 -2.5574 -0.0049 11 18 11 -5.1613 0.0022 11 18 13 4.2540 -0.0073 11 19 2 14.3403 0.0034 11 19 4 -3.3434 0.0093 11 19 6 -2.7284 0.0013 11 19 8 6.5127 -0.0016 11 19 10 5.1791 0.0001 11 19 12 19.1187 0.0049 11 19 14 10.4142 -0.0190 11 20 1 -3.2876 0.0156 11 20 3 -13.9416 -0.0185 11 20 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13 32 1 2.0523 -0.0388 13 32 3 -12.9489 0.0080 13 32 5 -0.7367 0.0049 13 33 2 -8.9794 0.0289 13 33 4 -10.7473 -0.0168 13 34 1 1.4150 -0.0516 13 34 3 8.4902 -0.0469 14 1 1 -38.9098 -0.1033 14 1 3 39.4710 0.0011 14 1 5 8.9725 0.0087 14 1 7 -11.0719 -0.0002 14 1 9 5.7708 -0.0126 14 1 11 -15.5988 0.0068 14 1 13 -4.2972 0.0026 14 1 15 4.7355 -0.0199 14 2 0 -70.9689 -0.2081 14 2 2 -28.0366 -0.0345 14 2 4 -26.3171 0.0026 14 2 6 13.1070 0.0063 14 2 8 30.0226 -0.0079 14 2 10 -5.1791 -0.0158 14 2 12 -4.8329 -0.0027 14 2 14 3.2336 0.0041 14 2 16 -2.8862 -0.0104 14 3 1 3.4336 -0.0654 14 3 3 0.1030 0.0329 14 3 5 0.5206 0.0450 14 3 7 19.3837 -0.0031 14 3 9 -17.5518 -0.0161 14 3 11 -0.2346 -0.0013 14 3 13 -2.2221 0.0168 14 3 15 1.8808 -0.0062 14 4 0 -11.3808 0.1521 14 4 2 -26.5660 0.0589 14 4 4 17.4719 -0.0294 14 4 6 22.2113 -0.0294 14 4 8 -13.5891 0.0187 14 4 10 9.5975 0.0024 14 4 12 -4.9539 -0.0089 14 4 14 -2.2780 0.0122 14 4 16 9.5383 0.0494 14 5 1 -14.1352 -0.1143 14 5 3 35.2593 0.0182 14 5 5 3.9428 0.0270 14 5 7 -2.8664 -0.0086 14 5 9 4.8176 -0.0031 14 5 11 -18.8047 -0.0015 14 5 13 -2.0735 0.0026 14 5 15 6.8633 0.0205 14 6 0 -77.6172 0.1218 14 6 2 -4.4351 -0.0424 14 6 4 -3.9517 0.0019 14 6 6 21.6956 0.0099 14 6 8 31.8135 -0.0090 14 6 10 -20.1950 -0.0171 14 6 12 -1.0113 0.0038 14 6 14 4.0365 -0.0043 14 6 16 -0.4549 0.0234 14 7 1 28.8104 -0.0320 14 7 3 6.0697 0.0029 14 7 5 32.4999 -0.0029 14 7 7 -9.6219 -0.0204 14 7 9 -27.5019 -0.0002 14 7 11 11.5769 0.0059 14 7 13 -0.7557 -0.0055 14 7 15 -1.7132 -0.0358 14 8 0 49.0934 0.0181 14 8 2 10.0440 -0.1441 14 8 4 37.1690 -0.0171 14 8 6 -7.2378 0.0507 14 8 8 5.9975 0.0098 14 8 10 4.1087 -0.0089 14 8 12 -11.2836 -0.0057 14 8 14 -5.3100 0.0050 14 9 1 3.7306 0.1014 14 9 3 24.0803 -0.0011 14 9 5 -11.8382 -0.0058 14 9 7 0.9166 0.0122 14 9 9 -15.8644 -0.0046 14 9 11 -16.7459 -0.0170 14 9 13 10.1345 -0.0100 14 9 15 3.6570 0.0090 14 10 0 43.5809 0.2296 14 10 2 13.6303 0.0356 14 10 4 1.1736 -0.0259 14 10 6 16.5891 -0.0037 14 10 8 -17.0402 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9.0051 -0.0220 16 10 12 -6.8000 0.0172 16 10 14 -2.4343 0.0307 16 11 1 8.4667 0.0391 16 11 3 23.6959 0.0173 16 11 5 -10.8941 -0.0051 16 11 7 -0.9067 -0.0185 16 11 9 -5.4932 0.0003 16 11 11 -8.0583 -0.0066 16 11 13 6.7455 -0.0049 16 11 15 2.9364 0.0390 16 12 0 40.1942 0.0509 16 12 2 22.7232 -0.0847 16 12 4 -12.0887 -0.0279 16 12 6 -1.7823 0.0205 16 12 8 -22.3338 0.0128 16 12 10 -7.1755 0.0021 16 12 12 10.9023 0.0013 16 12 14 5.3455 -0.0306 16 13 1 -1.1483 0.0942 16 13 3 -0.1817 -0.0248 16 13 5 10.2882 -0.0145 16 13 7 -8.9427 0.0203 16 13 9 1.9001 -0.0030 16 13 11 9.9760 -0.0140 16 13 13 6.4714 -0.0203 16 14 0 -8.5947 0.1294 16 14 2 7.7995 0.0664 16 14 4 0.9769 0.0124 16 14 6 -14.2579 -0.0064 16 14 8 -9.9610 -0.0067 16 14 10 -4.6510 0.0058 16 14 12 -5.3367 -0.0156 16 14 14 6.0106 -0.0092 16 15 1 12.1843 0.0297 16 15 3 4.2642 -0.0131 16 15 5 -3.5980 -0.0200 16 15 7 -12.8321 -0.0052 16 15 9 1.5097 0.0017 16 15 11 -4.7496 0.0174 16 15 13 6.4602 0.0074 16 16 0 20.5481 -0.1889 16 16 2 8.3609 -0.0314 16 16 4 3.9118 0.0114 16 16 6 -12.6849 0.0099 16 16 8 -10.5203 -0.0226 16 16 10 -6.3956 -0.0005 16 16 12 -12.7246 0.0090 16 17 1 1.8224 0.0783 16 17 3 10.4868 -0.0104 16 17 5 1.4601 -0.0086 16 17 7 -1.4219 0.0016 16 17 9 10.9988 0.0061 16 17 11 3.2523 -0.0116 16 17 13 -6.3416 0.0128 16 18 0 6.4235 -0.0527 16 18 2 13.6926 0.0543 16 18 4 -16.4845 -0.0120 16 18 6 -8.1258 -0.0345 16 18 8 13.3907 0.0102 16 18 10 1.5351 0.0064 16 18 12 1.1083 -0.0026 16 19 1 6.2191 -0.0279 16 19 3 -17.5378 -0.0014 16 19 5 -7.6633 0.0111 16 19 7 -1.9577 0.0092 16 19 9 5.7136 0.0021 16 19 11 5.2420 -0.0111 16 19 13 1.2908 0.0045 16 20 0 -12.0717 -0.0291 16 20 2 -20.1542 0.0913 16 20 4 -2.3743 0.0295 16 20 6 -7.5026 -0.0340 16 20 8 2.3073 -0.0057 16 20 10 1.4091 -0.0162 16 20 12 -7.5194 0.0147 16 21 1 -7.4050 -0.0603 16 21 3 10.8254 0.0105 16 21 5 -2.6508 -0.0080 16 21 7 7.2302 -0.0020 16 21 9 3.1697 -0.0029 16 21 11 -3.0302 -0.0065 16 22 0 -1.4281 -0.1175 16 22 2 -0.9430 -0.0481 16 22 4 -13.9585 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0.3804 0.0011 16 30 4 -1.3737 0.0030 16 30 6 -13.5118 0.0070 16 31 1 0.4795 -0.0247 16 31 3 -7.4610 -0.0167 16 31 5 1.1741 -0.0110 16 32 0 2.4329 -0.0571 16 32 2 3.8225 0.0021 16 32 4 -3.0986 0.0229 16 33 1 -2.3156 0.0207 16 33 3 1.0544 0.0019 17 1 2 0.1421 -0.0015 17 1 4 22.8963 -0.0047 17 1 6 -2.8283 -0.0108 17 1 8 -4.2487 -0.0126 17 1 10 -4.1082 0.0060 17 1 12 -8.8869 0.0215 17 1 14 13.1749 0.0011 17 2 1 -46.7594 -0.1261 17 2 3 1.6375 -0.0229 17 2 5 1.7448 0.0186 17 2 7 7.1428 0.0092 17 2 9 9.0204 -0.0117 17 2 11 1.5609 -0.0156 17 2 13 5.5859 0.0210 17 2 15 -9.0121 0.0236 17 3 2 33.2021 0.0070 17 3 4 6.4229 0.0018 17 3 6 13.1116 0.0141 17 3 8 -3.7316 0.0157 17 3 10 -19.9145 -0.0111 17 3 12 -2.0942 -0.0066 17 3 14 7.9687 0.0284 17 4 1 -2.5405 0.0584 17 4 3 -1.2569 0.0266 17 4 5 23.3118 -0.0193 17 4 7 13.7411 -0.0111 17 4 9 -4.8970 0.0092 17 4 11 -8.2445 -0.0104 17 4 13 3.7307 -0.0112 17 4 15 -9.7522 -0.0190 17 5 2 10.6280 -0.0405 17 5 4 21.8057 -0.0092 17 5 6 2.4670 0.0112 17 5 8 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11 2 -2.2269 0.0141 19 11 4 12.6292 0.0028 19 11 6 -18.4449 0.0020 19 11 8 -10.1681 -0.0081 19 11 10 3.4946 -0.0052 19 11 12 0.3979 -0.0010 19 11 14 1.8425 0.0055 19 12 1 10.8511 0.0560 19 12 3 18.4371 -0.0220 19 12 5 -10.9108 -0.0080 19 12 7 -2.8827 0.0076 19 12 9 -0.4655 0.0169 19 12 11 -13.1581 0.0091 19 12 13 11.8462 0.0324 19 13 2 5.3690 -0.0155 19 13 4 -4.9251 -0.0043 19 13 6 -3.4052 0.0063 19 13 8 0.6146 0.0086 19 13 10 -3.4239 0.0039 19 13 12 5.5662 -0.0182 19 14 1 5.3500 0.0924 19 14 3 6.9107 0.0281 19 14 5 -13.9114 -0.0032 19 14 7 -20.5518 -0.0120 19 14 9 0.9182 -0.0148 19 14 11 -6.6428 0.0253 19 14 13 5.4551 0.0145 19 15 2 -5.7284 0.0036 19 15 4 -8.3602 -0.0090 19 15 6 -10.0757 -0.0159 19 15 8 10.5038 -0.0113 19 15 10 -1.3600 0.0118 19 15 12 0.7118 0.0210 19 16 1 -1.3559 -0.0484 19 16 3 8.1395 -0.0128 19 16 5 -13.5156 0.0213 19 16 7 10.8904 0.0118 19 16 9 0.7717 -0.0088 19 16 11 8.1667 -0.0015 19 16 13 -7.2967 -0.0258 19 17 2 4.6678 0.0395 19 17 4 3.6300 0.0131 19 17 6 12.2476 0.0221 19 17 8 -5.9351 -0.0030 19 17 10 0.3975 -0.0063 19 17 12 -4.2973 -0.0261 19 18 1 -12.2972 0.0384 19 18 3 -8.4472 -0.0068 19 18 5 -5.6189 -0.0314 19 18 7 -10.4331 0.0032 19 18 9 4.1290 0.0256 19 18 11 7.6137 -0.0207 19 19 2 -5.8335 -0.0051 19 19 4 -3.6915 0.0052 19 19 6 -0.6143 0.0172 19 19 8 11.4774 0.0127 19 19 10 -0.8922 0.0071 19 19 12 -10.9099 0.0214 19 20 1 -1.3537 -0.0128 19 20 3 -8.2649 0.0198 19 20 5 1.9455 0.0273 19 20 7 2.4838 -0.0019 19 20 9 5.2443 -0.0258 19 20 11 8.1755 0.0032 19 21 2 3.1534 0.0039 19 21 4 -0.7115 0.0152 19 21 6 1.3765 -0.0191 19 21 8 9.4857 0.0121 19 21 10 10.0493 -0.0039 19 22 1 -10.9657 -0.0809 19 22 3 -3.4995 0.0008 19 22 5 6.8223 -0.0021 19 22 7 11.3821 0.0163 19 22 9 1.1572 0.0201 19 22 11 1.9967 0.0516 19 23 2 -5.8812 0.0184 19 23 4 -7.6493 0.0192 19 23 6 -3.7032 0.0206 19 23 8 -6.8007 0.0069 19 23 10 3.9998 0.0122 19 24 1 -9.4551 0.0303 19 24 3 -7.6335 -0.0036 19 24 5 14.2358 -0.0013 19 24 7 -16.8788 0.0146 19 24 9 15.8105 0.0127 19 25 2 -9.6644 -0.0277 19 25 4 -1.6820 -0.0139 19 25 6 -13.9708 -0.0002 19 25 8 -6.6663 0.0084 19 26 1 2.4258 -0.0095 19 26 3 4.8848 0.0271 19 26 5 7.1603 0.0473 19 26 7 -17.8228 0.0049 19 27 2 0.5279 0.0045 19 27 4 6.9626 -0.0090 19 27 6 4.6366 0.0139 19 27 8 7.2387 -0.0030 19 28 1 -6.1560 -0.0072 19 28 3 3.0046 -0.0237 19 28 5 3.5397 0.0240 19 28 7 1.5494 -0.0151 19 29 2 -6.2036 -0.0157 19 29 4 5.6076 0.0607 19 29 6 5.3937 0.0134 19 30 1 1.0000 0.0368 19 30 3 0.9098 0.0428 19 30 5 -3.8502 -0.0143 19 31 2 2.6855 0.0232 19 32 1 5.1615 0.0169 20 1 1 13.9059 0.0785 20 1 3 27.5089 -0.0008 20 1 5 2.2351 -0.0360 20 1 7 4.5859 -0.0152 20 1 9 -18.0639 0.0169 20 1 11 -13.1110 0.0124 20 1 13 5.1909 0.0071 20 2 0 8.9705 -0.0791 20 2 2 3.5416 -0.0484 20 2 4 5.5252 0.0087 20 2 6 7.5871 0.0046 20 2 8 -1.8130 -0.0135 20 2 10 2.5070 0.0078 20 2 12 1.7024 0.0036 20 2 14 -10.6808 -0.0298 20 3 1 10.0618 0.1327 20 3 3 17.4397 -0.0250 20 3 5 -2.1306 -0.0268 20 3 7 -2.6769 0.0235 20 3 9 -10.5935 0.0127 20 3 11 -2.2574 0.0035 20 3 13 -7.6564 0.0083 20 4 0 13.2510 0.0352 20 4 2 10.1070 0.1122 20 4 4 8.5606 0.0105 20 4 6 0.8837 -0.0226 20 4 8 -8.2232 -0.0043 20 4 10 -9.4510 -0.0044 20 4 12 -5.1730 -0.0074 20 4 14 5.2184 -0.0124 20 5 1 8.9272 0.0030 20 5 3 8.8758 -0.0336 20 5 5 0.4225 -0.0139 20 5 7 -2.9328 0.0016 20 5 9 -4.4179 0.0149 20 5 11 -5.4015 0.0123 20 5 13 9.9189 0.0201 20 6 0 22.5609 -0.1859 20 6 2 -1.7525 0.0076 20 6 4 -0.7073 0.0085 20 6 6 0.9290 0.0015 20 6 8 -10.8947 -0.0114 20 6 10 10.1427 -0.0045 20 6 12 -0.5747 0.0074 20 6 14 3.7198 0.0318 20 7 1 3.5557 0.0069 20 7 3 19.9380 0.0097 20 7 5 9.4003 0.0143 20 7 7 -25.0902 0.0026 20 7 9 -0.0169 -0.0112 20 7 11 -10.5243 -0.0047 20 7 13 4.0598 0.0169 20 8 0 32.7718 -0.0604 20 8 2 18.9889 0.0463 20 8 4 -9.7925 -0.0068 20 8 6 -22.1731 -0.0358 20 8 8 -6.7985 0.0005 20 8 10 -6.3640 0.0079 20 8 12 -2.4018 0.0165 20 8 14 2.9752 -0.0028 20 9 1 1.0773 -0.0593 20 9 3 -8.9450 -0.0043 20 9 5 -1.5020 0.0275 20 9 7 3.3152 0.0232 20 9 9 -7.5703 -0.0135 20 9 11 10.0309 -0.0202 20 9 13 0.7456 -0.0273 20 10 0 32.5721 0.0842 20 10 2 20.5506 0.0755 20 10 4 6.2326 0.0034 20 10 6 -8.2495 -0.0089 20 10 8 -15.4422 0.0108 20 10 10 1.0957 -0.0037 20 10 12 -3.5075 -0.0141 20 10 14 6.0555 -0.0224 20 11 1 -13.1844 -0.1258 20 11 3 9.1279 0.0230 20 11 5 -8.4639 0.0243 20 11 7 -14.0845 -0.0225 20 11 9 -1.3080 -0.0159 20 11 11 -4.7977 0.0120 20 11 13 -7.4001 0.0113 20 12 0 -28.6753 -0.0433 20 12 2 11.0857 -0.0786 20 12 4 -13.5503 -0.0040 20 12 6 -10.2945 0.0224 20 12 8 2.0372 0.0011 20 12 10 -5.8283 0.0022 20 12 12 -1.3088 0.0272 20 13 1 11.0882 -0.0043 20 13 3 -6.8583 0.0316 20 13 5 1.7624 0.0154 20 13 7 -5.9655 -0.0092 20 13 9 0.9821 -0.0085 20 13 11 0.9295 -0.0061 20 13 13 10.3182 0.0126 20 14 0 38.9450 0.1522 20 14 2 4.3076 -0.0369 20 14 4 -0.9798 -0.0149 20 14 6 -13.1945 0.0123 20 14 8 7.7658 0.0217 20 14 10 0.2391 -0.0000 20 14 12 0.9477 -0.0093 20 15 1 5.1513 -0.0259 20 15 3 -0.2652 -0.0010 20 15 5 -0.2043 0.0035 20 15 7 10.7141 -0.0040 20 15 9 -8.1714 0.0070 20 15 11 3.7711 -0.0059 20 15 13 -4.0797 0.0154 20 16 0 5.6977 0.0988 20 16 2 -5.8006 -0.0107 20 16 4 -12.8066 0.0207 20 16 6 -7.0885 0.0224 20 16 8 -5.4449 -0.0015 20 16 10 -5.8086 0.0052 20 16 12 -3.1888 -0.0110 20 17 1 2.5551 0.0548 20 17 3 -5.4281 0.0005 20 17 5 -6.4330 -0.0283 20 17 7 10.1457 0.0016 20 17 9 2.8686 0.0120 20 17 11 5.6680 0.0119 20 18 0 -19.7694 -0.0381 20 18 2 3.6581 -0.0665 20 18 4 -9.9456 -0.0044 20 18 6 4.3788 0.0271 20 18 8 7.6502 -0.0137 20 18 10 13.8566 -0.0375 20 18 12 6.9324 -0.0037 20 19 1 1.6189 0.0906 20 19 3 -4.8772 0.0048 20 19 5 -3.9645 0.0056 20 19 7 2.4411 0.0028 20 19 9 1.0651 0.0115 20 19 11 -9.7070 0.0269 20 20 0 -0.9377 0.0283 20 20 2 -10.7732 0.0433 20 20 4 -7.4462 0.0051 20 20 6 1.4779 -0.0164 20 20 8 2.5165 -0.0053 20 20 10 11.3927 0.0223 20 21 1 -10.8976 0.0212 20 21 3 1.3730 -0.0195 20 21 5 -1.1402 -0.0097 20 21 7 0.0757 0.0285 20 21 9 12.8039 0.0263 20 21 11 14.1527 0.0002 20 22 0 -6.0865 -0.0765 20 22 2 -12.2364 0.0480 20 22 4 1.4097 0.0154 20 22 6 7.3166 0.0007 20 22 8 6.2802 -0.0003 20 22 10 -2.2003 0.0242 20 23 1 -7.8941 0.0237 20 23 3 -6.8788 0.0050 20 23 5 1.9029 -0.0029 20 23 7 0.1925 -0.0089 20 23 9 -6.8750 -0.0034 20 24 0 -6.9240 -0.0730 20 24 2 -2.6715 -0.0073 20 24 4 13.0954 -0.0064 20 24 6 5.5615 0.0051 20 24 8 -10.1599 0.0520 20 25 1 -0.2549 -0.0169 20 25 3 1.5353 0.0040 20 25 5 -0.8682 0.0270 20 25 7 -3.2942 0.0464 20 25 9 -14.5307 -0.0395 20 26 0 -0.6915 0.0272 20 26 2 -5.4431 0.0377 20 26 4 -6.4240 0.0220 20 26 6 1.4058 0.0034 20 26 8 0.6599 -0.0111 20 27 1 0.3933 -0.0743 20 27 3 3.8505 0.0091 20 27 5 1.8713 0.0093 20 27 7 4.2990 0.0051 20 28 0 7.2859 -0.0238 20 28 2 7.7081 0.0123 20 28 4 9.1875 0.0076 20 28 6 -14.2064 -0.0134 20 29 1 -1.5138 0.0153 20 29 3 -0.6931 0.0209 20 29 5 -2.6679 0.0162 20 30 0 -1.5511 0.0405 20 30 2 2.2677 -0.0054 20 30 4 -0.3348 -0.0238 20 31 1 2.5972 0.0114 21 1 2 21.6899 0.0040 21 1 4 11.4700 -0.0160 21 1 6 8.1314 -0.0091 21 1 8 -14.2155 0.0057 21 1 10 -16.2180 0.0004 21 1 12 4.3523 -0.0215 21 1 14 -0.5378 -0.0001 21 2 1 4.0026 -0.0364 21 2 3 2.6870 0.0005 21 2 5 3.4244 0.0165 21 2 7 1.1058 -0.0067 21 2 9 -3.4146 -0.0120 21 2 11 -2.7744 0.0011 21 2 13 -5.1123 -0.0280 21 3 2 21.2375 0.0274 21 3 4 5.0972 -0.0112 21 3 6 -0.2008 0.0001 21 3 8 -5.2121 0.0089 21 3 10 -12.7418 -0.0088 21 3 12 -1.0037 0.0064 21 3 14 1.5827 0.0541 21 4 1 24.7032 -0.0526 21 4 3 5.8339 -0.0067 21 4 5 2.4452 -0.0001 21 4 7 2.7626 0.0076 21 4 9 -13.6081 -0.0018 21 4 11 4.2049 -0.0064 21 4 13 1.0111 -0.0149 21 5 2 -1.3055 0.0095 21 5 4 11.9012 0.0075 21 5 6 -8.3521 0.0111 21 5 8 -12.9789 0.0067 21 5 10 3.9508 -0.0049 21 5 12 3.1946 -0.0083 21 5 14 11.0130 0.0067 21 6 1 10.3050 0.0450 21 6 3 -0.7773 0.0324 21 6 5 -13.2887 -0.0111 21 6 7 -8.3171 -0.0044 21 6 9 -6.5205 -0.0001 21 6 11 6.1444 -0.0046 21 6 13 -3.8652 0.0215 21 7 2 1.9204 -0.0166 21 7 4 11.8229 -0.0035 21 7 6 -0.5701 -0.0127 21 7 8 -14.1762 0.0025 21 7 10 -8.3556 0.0108 21 7 12 -3.2614 0.0046 21 7 14 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8 -4.2369 0.0056 22 2 10 1.5331 -0.0149 22 2 12 8.3261 -0.0210 22 2 14 6.8516 -0.0299 22 3 1 11.7422 0.0269 22 3 3 23.0163 -0.0289 22 3 5 -9.3632 -0.0306 22 3 7 -2.8306 -0.0147 22 3 9 -0.1846 0.0164 22 3 11 -4.5846 0.0151 22 3 13 7.4288 0.0146 22 4 0 34.2432 -0.0934 22 4 2 16.3084 -0.0540 22 4 4 -0.8104 0.0201 22 4 6 -0.2231 0.0212 22 4 8 -4.6772 -0.0076 22 4 10 -0.4595 -0.0132 22 4 12 -4.2534 0.0009 22 4 14 -4.4286 0.0103 22 5 1 2.2652 0.1194 22 5 3 4.1888 -0.0140 22 5 5 -1.8514 -0.0229 22 5 7 -5.8322 0.0037 22 5 9 -5.7693 0.0125 22 5 11 -6.3961 -0.0197 22 5 13 -2.7335 0.0437 22 6 0 26.7694 -0.0357 22 6 2 9.9271 0.0179 22 6 4 -10.6245 0.0040 22 6 6 -9.8276 -0.0154 22 6 8 -20.0044 -0.0119 22 6 10 3.7708 0.0016 22 6 12 -3.5173 0.0106 22 7 1 -9.7625 0.0628 22 7 3 -6.7192 -0.0321 22 7 5 0.3988 -0.0066 22 7 7 -16.9835 0.0390 22 7 9 -4.1732 0.0040 22 7 11 3.7278 -0.0145 22 7 13 10.9189 -0.0106 22 8 0 4.1870 -0.0134 22 8 2 15.3105 0.0886 22 8 4 -1.7863 0.0125 22 8 6 -8.9871 -0.0140 22 8 8 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12 2.0383 -0.0054 22 15 1 22.8267 -0.0464 22 15 3 -12.8620 0.0191 22 15 5 5.2843 -0.0044 22 15 7 5.9975 -0.0212 22 15 9 2.4814 -0.0054 22 15 11 4.7789 0.0099 22 16 0 35.1275 0.0226 22 16 2 -6.1267 -0.0745 22 16 4 -0.7873 -0.0154 22 16 6 -2.2032 0.0321 22 16 8 4.8292 -0.0037 22 16 10 2.6401 -0.0309 22 16 12 7.3718 -0.0341 22 17 1 -9.3251 0.0114 22 17 3 3.8608 0.0219 22 17 5 0.9738 0.0155 22 17 7 10.8137 -0.0066 22 17 9 4.4700 -0.0150 22 17 11 1.0574 0.0413 22 18 0 -25.3129 0.1197 22 18 2 -8.7019 -0.0091 22 18 4 -7.2054 -0.0134 22 18 6 2.2083 -0.0052 22 18 8 -1.6037 0.0218 22 18 10 0.1257 0.0242 22 19 1 -17.0229 0.0101 22 19 3 -4.3574 -0.0120 22 19 5 -5.8395 -0.0198 22 19 7 1.5260 0.0026 22 19 9 4.0211 0.0444 22 19 11 1.5361 0.0100 22 20 0 -15.7219 -0.0028 22 20 2 -5.4102 -0.0129 22 20 4 4.3333 0.0214 22 20 6 12.5338 0.0153 22 20 8 14.2560 -0.0235 22 20 10 17.2475 -0.0209 22 21 1 -2.5483 0.0823 22 21 3 -1.5287 -0.0071 22 21 5 -3.5558 -0.0113 22 21 7 -11.8721 0.0016 22 21 9 1.9490 0.0043 22 22 0 6.9890 -0.0287 22 22 2 -10.5063 -0.0190 22 22 4 4.0867 -0.0134 22 22 6 -2.8827 -0.0056 22 22 8 -1.9987 0.0159 22 23 1 0.1338 0.0465 22 23 3 6.3707 0.0039 22 23 5 2.7628 0.0143 22 23 7 -6.2817 0.0473 22 23 9 -4.0210 -0.0485 22 24 0 -6.2794 -0.0021 22 24 2 -4.6912 0.0571 22 24 4 1.1231 0.0114 22 24 6 -0.5027 0.0143 22 24 8 -7.9485 -0.0307 22 25 1 -2.4489 -0.0312 22 25 3 3.4126 -0.0168 22 25 5 6.8421 -0.0058 22 25 7 10.5444 -0.0279 22 26 0 0.4723 -0.0901 22 26 2 13.2180 0.0137 22 26 4 8.7394 0.0217 22 26 6 0.7411 -0.0219 22 27 1 -1.2843 0.0033 22 27 3 -4.0158 -0.0027 22 27 5 -1.4878 0.0051 22 28 0 5.4276 -0.0100 22 28 2 3.0166 -0.0060 22 28 4 1.0501 -0.0414 22 29 1 1.2958 0.0037 22 29 3 -3.6016 -0.0159 22 30 0 -3.6797 0.0221 23 1 2 9.3472 0.0257 23 1 4 13.3348 -0.0036 23 1 6 0.6357 -0.0193 23 1 8 -6.2984 0.0006 23 1 10 -2.2303 0.0027 23 1 12 -6.5251 -0.0095 23 2 1 8.2947 0.0193 23 2 3 6.4157 -0.0157 23 2 5 -5.0624 -0.0069 23 2 7 2.1561 0.0014 23 2 9 -3.0053 -0.0033 23 2 11 1.0483 0.0056 23 2 13 4.9543 0.0108 23 3 2 13.4759 0.0224 23 3 4 9.3430 -0.0043 23 3 6 -0.9776 0.0163 23 3 8 -16.6492 0.0065 23 3 10 -7.9978 -0.0132 23 3 12 -0.2300 -0.0156 23 4 1 15.8908 0.0862 23 4 3 4.0459 0.0330 23 4 5 -9.5417 -0.0060 23 4 7 -10.4676 -0.0152 23 4 9 -7.5677 -0.0052 23 4 11 2.4259 0.0028 23 4 13 3.2894 -0.0025 23 5 2 -0.1686 -0.0030 23 5 4 2.6005 -0.0157 23 5 6 -4.9535 -0.0113 23 5 8 -4.4941 0.0019 23 5 10 4.0294 0.0190 23 5 12 -3.1279 0.0137 23 6 1 28.9850 -0.1004 23 6 3 3.9482 -0.0144 23 6 5 -9.2444 0.0219 23 6 7 -4.9502 0.0068 23 6 9 -4.5905 -0.0137 23 6 11 0.1053 -0.0143 23 6 13 1.6355 -0.0287 23 7 2 -4.7104 0.0468 23 7 4 -3.2330 -0.0013 23 7 6 -7.9209 0.0072 23 7 8 -7.0192 -0.0028 23 7 10 -2.9022 -0.0119 23 7 12 2.0306 0.0040 23 8 1 7.9471 0.0016 23 8 3 3.6335 0.0044 23 8 5 -8.4462 -0.0259 23 8 7 -5.4702 0.0003 23 8 9 -10.2350 0.0084 23 8 11 2.3331 -0.0011 23 8 13 4.0955 0.0236 23 9 2 -4.5191 -0.0116 23 9 4 -4.2854 0.0061 23 9 6 -5.2429 0.0183 23 9 8 4.3921 0.0092 23 9 10 5.4091 -0.0125 23 9 12 -1.7819 0.0142 23 10 1 13.0132 -0.0010 23 10 3 7.9410 0.0309 23 10 5 -10.6895 0.0137 23 10 7 -6.6485 -0.0005 23 10 9 5.0574 -0.0041 23 10 11 1.1234 -0.0058 23 10 13 4.3542 0.0306 23 11 2 6.7211 -0.0244 23 11 4 1.5324 0.0029 23 11 6 -10.8792 -0.0266 23 11 8 0.9929 -0.0088 23 11 10 2.0493 0.0164 23 11 12 3.8292 0.0174 23 12 1 8.2411 -0.0886 23 12 3 9.8579 -0.0231 23 12 5 -19.7565 0.0110 23 12 7 -8.4365 0.0162 23 12 9 11.1211 -0.0043 23 12 11 -1.5789 0.0201 23 13 2 1.7572 0.0111 23 13 4 -14.0983 0.0036 23 13 6 11.8611 0.0072 23 13 8 16.8412 0.0016 23 13 10 3.6126 -0.0093 23 13 12 7.5416 -0.0535 23 14 1 0.9773 0.0761 23 14 3 -7.9927 0.0008 23 14 5 1.2819 -0.0188 23 14 7 1.0097 -0.0066 23 14 9 -6.4894 0.0232 23 14 11 16.2097 -0.0241 23 15 2 -8.4184 -0.0419 23 15 4 -0.7163 -0.0114 23 15 6 -3.3827 -0.0033 23 15 8 -9.7412 0.0153 23 15 10 12.8231 0.0103 23 16 1 -17.0248 0.0203 23 16 3 -2.1520 0.0072 23 16 5 -3.7129 0.0290 23 16 7 3.9735 -0.0086 23 16 9 3.4345 -0.0104 23 16 11 3.6741 -0.0149 23 17 2 3.9837 0.0028 23 17 4 -3.7950 -0.0081 23 17 6 7.1258 -0.0208 23 17 8 12.4356 -0.0104 23 17 10 0.0191 0.0056 23 18 1 1.1353 -0.0151 23 18 3 -5.8585 -0.0297 23 18 5 9.7531 -0.0081 23 18 7 -0.7036 0.0108 23 18 9 3.2367 0.0011 23 19 2 -11.0409 0.0263 23 19 4 0.9534 -0.0060 23 19 6 -1.0807 0.0280 23 19 8 10.6421 0.0220 23 19 10 1.9700 0.0140 23 20 1 -17.9061 0.0783 23 20 3 -0.6458 0.0066 23 20 5 0.0025 -0.0059 23 20 7 11.6326 -0.0091 23 20 9 1.8209 -0.0069 23 21 2 -1.1256 -0.0137 23 21 4 -6.4485 0.0077 23 21 6 -12.2936 0.0161 23 21 8 -8.8762 -0.0038 23 22 1 -7.2884 -0.0322 23 22 3 9.7390 0.0176 23 22 5 7.7375 0.0164 23 22 7 -1.0057 -0.0171 23 22 9 4.4121 -0.0253 23 23 2 3.8314 0.0368 23 23 4 -1.9894 0.0039 23 23 6 -3.1655 -0.0206 23 23 8 5.7857 -0.0430 23 24 1 3.7207 -0.0259 23 24 3 1.1704 -0.0200 23 24 5 -3.2631 -0.0028 23 24 7 -10.2818 -0.0100 23 25 2 5.1796 -0.0124 23 25 4 0.3787 0.0265 23 25 6 3.3700 -0.0253 23 26 1 2.0928 0.0213 23 26 3 7.8549 0.0525 23 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1.3164 0.0252 28 5 5 -7.4200 0.0147 28 5 7 0.5724 -0.0144 28 5 9 -2.2078 -0.0244 28 5 11 10.1450 0.0269 28 6 0 6.1038 0.1047 28 6 2 8.9362 -0.0080 28 6 4 -8.2550 -0.0272 28 6 6 5.8772 -0.0063 28 6 8 0.7912 0.0216 28 6 10 2.8121 0.0083 28 7 1 4.6893 -0.0323 28 7 3 -15.1702 0.0078 28 7 5 -3.9561 0.0022 28 7 7 4.5092 0.0018 28 7 9 2.6431 0.0054 28 7 11 -0.5445 0.0062 28 8 0 16.9115 0.0296 28 8 2 -11.3016 -0.0302 28 8 4 -7.2590 0.0138 28 8 6 0.3796 0.0130 28 8 8 2.7427 -0.0052 28 8 10 1.3017 -0.0240 28 9 1 -3.3677 0.0480 28 9 3 -3.1186 0.0066 28 9 5 1.7197 -0.0228 28 9 7 -1.8504 0.0052 28 9 9 5.3557 0.0301 28 10 0 -5.0538 0.0105 28 10 2 -10.3736 -0.0636 28 10 4 -4.5305 0.0022 28 10 6 0.2068 0.0148 28 10 8 6.2430 -0.0048 28 10 10 7.3649 -0.0073 28 11 1 -7.9223 0.0658 28 11 3 -5.6037 -0.0039 28 11 5 -4.3509 0.0025 28 11 7 3.3257 0.0161 28 11 9 7.7603 -0.0295 28 12 0 2.9583 0.0336 28 12 2 -4.7506 0.0360 28 12 4 6.7828 0.0095 28 12 6 2.2282 -0.0108 28 12 8 4.0757 -0.0352 28 12 10 -2.0177 0.0465 28 13 1 -6.6316 0.0136 28 13 3 -5.3857 -0.0295 28 13 5 -4.1087 -0.0020 28 13 7 9.8519 -0.0174 28 13 9 -6.0089 0.0306 28 14 0 -6.2702 -0.0820 28 14 2 -13.4928 0.0074 28 14 4 -8.7500 0.0411 28 14 6 -1.8301 -0.0032 28 14 8 -4.2583 0.0029 28 15 1 -0.4858 0.0239 28 15 3 -0.4727 -0.0005 28 15 5 5.6475 -0.0247 28 15 7 -6.0894 -0.0081 28 15 9 2.0713 -0.0049 28 16 0 -6.6692 -0.0392 28 16 2 1.3812 0.0253 28 16 4 -3.2313 -0.0101 28 16 6 0.8311 -0.0187 28 16 8 2.3346 0.0318 28 17 1 7.5234 -0.0295 28 17 3 -0.7102 -0.0083 28 17 5 4.2594 0.0095 28 17 7 0.5253 0.0438 28 18 0 0.4711 -0.0055 28 18 2 8.4181 0.0273 28 18 4 1.2359 -0.0030 28 18 6 2.4438 0.0122 28 19 1 5.7556 -0.0692 28 19 3 -7.1868 0.0123 28 19 5 -0.6611 0.0174 28 19 7 3.1732 -0.0062 28 20 0 3.5151 -0.0428 28 20 2 7.8113 -0.0016 28 20 4 1.8469 -0.0077 28 20 6 -9.3530 0.0024 28 21 1 -0.3888 0.0166 28 21 3 1.1390 0.0178 28 21 5 -2.2034 0.0224 28 22 0 -2.9182 0.0734 28 22 2 -0.3414 -0.0152 28 22 4 -3.2766 -0.0200 28 23 1 -7.5293 -0.0118 28 23 3 1.2850 -0.0083 28 24 0 -8.9281 0.0708 28 24 2 5.4007 -0.0079 29 1 2 -2.1620 -0.0007 29 1 4 5.0622 -0.0130 29 1 6 6.6731 -0.0008 29 1 8 -2.7935 0.0000 29 1 10 3.8255 0.0026 29 2 1 2.8522 0.0313 29 2 3 4.2982 0.0060 29 2 5 -0.8020 -0.0149 29 2 7 -10.3691 0.0020 29 2 9 6.8383 0.0168 29 2 11 1.8377 -0.0338 29 3 2 -9.6971 -0.0384 29 3 4 0.7712 0.0009 29 3 6 -7.0697 -0.0068 29 3 8 8.2704 0.0014 29 3 10 -6.5411 -0.0070 29 4 1 19.9467 0.0004 29 4 3 3.1704 0.0002 29 4 5 -5.9771 0.0102 29 4 7 3.0455 0.0136 29 4 9 0.7565 0.0020 29 5 2 -6.1814 -0.0185 29 5 4 -2.6335 0.0094 29 5 6 -0.2823 -0.0242 29 5 8 -6.6348 -0.0111 29 5 10 -0.6799 0.0026 29 6 1 7.1250 -0.0366 29 6 3 -4.2142 -0.0244 29 6 5 1.9187 0.0036 29 6 7 9.0946 0.0037 29 6 9 0.6079 -0.0146 29 7 2 -6.7279 0.0275 29 7 4 -0.5342 -0.0020 29 7 6 -0.6353 0.0034 29 7 8 -0.9503 0.0220 29 7 10 7.3554 0.0277 29 8 1 -6.3625 0.0818 29 8 3 -4.6227 -0.0109 29 8 5 -15.4174 0.0079 29 8 7 1.3535 -0.0015 29 8 9 -2.3742 -0.0062 29 9 2 -12.9157 -0.0095 29 9 4 -6.0764 0.0057 29 9 6 -2.4339 -0.0013 29 9 8 4.3444 -0.0061 29 9 10 0.9879 0.0061 29 10 1 -10.2082 -0.0175 29 10 3 1.9709 0.0073 29 10 5 -1.8265 0.0178 29 10 7 9.2188 -0.0025 29 10 9 -7.4534 -0.0123 29 11 2 -0.6771 0.0327 29 11 4 4.8267 -0.0089 29 11 6 -0.1634 0.0128 29 11 8 5.3879 -0.0032 29 12 1 -5.5675 -0.0156 29 12 3 -0.9746 -0.0031 29 12 5 -2.5331 -0.0075 29 12 7 7.9009 -0.0178 29 12 9 0.0217 0.0178 29 13 2 -4.4207 0.0118 29 13 4 -16.2806 0.0114 29 13 6 -4.3042 -0.0033 29 13 8 -0.4693 0.0010 29 14 1 -1.5375 0.0248 29 14 3 0.5533 0.0304 29 14 5 2.5153 -0.0345 29 14 7 -7.0084 0.0209 29 15 2 7.6791 -0.0085 29 15 4 3.8514 -0.0280 29 15 6 4.9857 0.0294 29 15 8 1.9297 0.0075 29 16 1 -13.1502 -0.0427 29 16 3 0.3026 -0.0101 29 16 5 6.6247 0.0339 29 16 7 -9.4234 0.0140 29 17 2 2.2975 -0.0078 29 17 4 -2.7117 -0.0043 29 17 6 -1.6135 -0.0035 29 18 1 4.9379 -0.0227 29 18 3 4.2632 -0.0165 29 18 5 5.8541 -0.0077 29 18 7 4.7072 0.0056 29 19 2 1.0283 -0.0287 29 19 4 -2.2443 0.0330 29 19 6 5.8984 0.0126 29 20 1 1.5969 0.0026 29 20 3 -1.2966 0.0461 29 20 5 -0.3904 -0.0282 29 21 2 -1.0328 0.0338 29 21 4 9.4112 -0.0187 29 22 1 -0.0796 0.0165 29 22 3 0.9475 -0.0048 29 23 2 -1.7936 0.0022 30 1 1 -3.4454 -0.0065 30 1 3 -4.1999 -0.0134 30 1 5 1.8516 0.0000 30 1 7 7.9682 -0.0102 30 1 9 1.2530 0.0022 30 2 0 -0.1014 -0.1049 30 2 2 17.3343 0.0092 30 2 4 1.0528 -0.0020 30 2 6 5.4216 -0.0004 30 2 8 -7.9930 0.0302 30 2 10 -0.2698 0.0075 30 3 1 2.9777 -0.0098 30 3 3 -4.1651 -0.0039 30 3 5 -1.8579 0.0138 30 3 7 -11.7960 -0.0011 30 3 9 -0.0333 -0.0466 30 4 0 13.4208 0.0236 30 4 2 1.7407 0.0567 30 4 4 -9.1452 -0.0097 30 4 6 3.2489 -0.0206 30 4 8 12.8513 0.0136 30 4 10 4.5457 0.0207 30 5 1 -7.2378 -0.0736 30 5 3 -12.3400 0.0093 30 5 5 -2.8069 0.0103 30 5 7 3.1829 -0.0105 30 5 9 -3.4744 0.0193 30 6 0 14.2123 -0.0186 30 6 2 -3.6268 -0.0118 30 6 4 3.7356 -0.0039 30 6 6 0.6824 0.0043 30 6 8 -1.6664 -0.0065 30 6 10 -0.7243 -0.0704 30 7 1 -7.6387 -0.0265 30 7 3 -11.9744 0.0262 30 7 5 1.6994 -0.0089 30 7 7 4.6267 0.0032 30 7 9 -0.2947 -0.0048 30 8 0 -3.3677 0.0313 30 8 2 -8.1100 -0.0471 30 8 4 -7.5260 -0.0175 30 8 6 0.4359 0.0187 30 8 8 2.9789 0.0145 30 9 1 3.6290 -0.0032 30 9 3 -7.5494 0.0201 30 9 5 3.8347 0.0029 30 9 7 0.1445 0.0183 30 9 9 1.7511 -0.0086 30 10 0 0.4507 0.0912 30 10 2 -14.8771 0.0052 30 10 4 -5.4251 -0.0027 30 10 6 -1.3477 0.0083 30 10 8 0.6206 -0.0418 30 11 1 -18.8758 0.0043 30 11 3 0.7654 0.0021 30 11 5 -3.8057 0.0048 30 11 7 3.1079 -0.0245 30 11 9 6.4653 0.0291 30 12 0 -8.4881 -0.0127 30 12 2 -0.2829 -0.0478 30 12 4 -0.7606 0.0227 30 12 6 2.2539 0.0179 30 12 8 4.6072 0.0078 30 13 1 1.7586 0.0648 30 13 3 2.5873 0.0117 30 13 5 2.0622 -0.0196 30 13 7 -1.0018 -0.0107 30 14 0 2.4121 0.0097 30 14 2 4.2406 0.0001 30 14 4 3.2469 -0.0132 30 14 6 2.2401 -0.0147 30 14 8 -0.8206 0.0221 30 15 1 11.5376 0.0336 30 15 3 -8.5245 -0.0373 30 15 5 2.6857 -0.0140 30 15 7 1.0183 0.0213 30 16 0 4.5293 -0.0098 30 16 2 -5.1208 0.0203 30 16 4 -2.5629 0.0254 30 16 6 1.3559 0.0040 30 17 1 1.8348 -0.0408 30 17 3 -7.1596 -0.0066 30 17 5 1.5065 0.0104 30 18 0 2.6920 -0.1064 30 18 2 2.6421 0.0166 30 18 4 -0.4046 0.0095 30 18 6 0.8375 0.0092 30 19 1 0.1461 0.0176 30 19 3 4.4764 0.0028 30 19 5 3.0273 0.0123 30 20 0 -7.9158 0.0166 30 20 2 8.3658 0.0182 30 20 4 -3.4668 -0.0345 30 21 1 -0.3969 -0.0222 30 21 3 -1.3469 -0.0044 30 22 0 -8.6487 0.0403 31 1 2 2.1630 -0.0204 31 1 4 4.3952 0.0087 31 1 6 0.6772 -0.0114 31 1 8 1.2465 -0.0127 31 2 1 13.3304 -0.0304 31 2 3 -1.0539 0.0328 31 2 5 -8.1726 -0.0040 31 2 7 1.9953 0.0218 31 2 9 4.7143 0.0286 31 3 2 -11.1303 -0.0043 31 3 4 0.3907 0.0047 31 3 6 0.4957 -0.0091 31 3 8 -1.1769 -0.0060 31 4 1 8.9629 -0.0504 31 4 3 2.0068 -0.0124 31 4 5 2.4817 0.0014 31 4 7 -0.8184 0.0098 31 4 9 5.3454 0.0031 31 5 2 -6.5641 -0.0102 31 5 4 -7.8800 0.0009 31 5 6 -8.6320 -0.0281 31 5 8 -3.1730 0.0051 31 6 1 2.2916 0.0472 31 6 3 -5.4325 0.0015 31 6 5 -6.5683 -0.0202 31 6 7 8.4062 0.0205 31 6 9 -7.5309 -0.0144 31 7 2 -10.6816 -0.0337 31 7 4 -3.9114 0.0014 31 7 6 7.7063 0.0091 31 7 8 -0.9810 0.0093 31 8 1 -5.0793 -0.0101 31 8 3 -1.6175 -0.0063 31 8 5 -1.6273 0.0057 31 8 7 5.3136 -0.0137 31 8 9 -2.1360 -0.0336 31 9 2 1.1805 0.0103 31 9 4 4.5674 0.0012 31 9 6 -8.1271 0.0139 31 9 8 1.5671 0.0041 31 10 1 -12.8690 0.0040 31 10 3 0.1032 -0.0334 31 10 5 -3.3479 0.0220 31 10 7 6.7239 -0.0090 31 11 2 -8.0933 0.0107 31 11 4 -9.2550 0.0243 31 11 6 -2.5021 -0.0048 31 11 8 9.2817 -0.0121 31 12 1 -5.7885 0.0399 31 12 3 1.1199 0.0244 31 12 5 -0.5689 -0.0209 31 12 7 -7.1923 -0.0095 31 13 2 7.6587 0.0239 31 13 4 5.8100 -0.0470 31 13 6 2.5936 0.0135 31 14 1 -0.2784 -0.0078 31 14 3 1.1388 -0.0177 31 14 5 5.2520 0.0330 31 14 7 6.6995 0.0141 31 15 2 6.6516 0.0087 31 15 4 -10.4673 -0.0088 31 15 6 -2.9014 -0.0018 31 16 1 -0.0968 -0.0091 31 16 3 3.7665 -0.0105 31 16 5 12.0096 -0.0079 31 17 2 3.3326 -0.0267 31 17 4 4.3893 0.0094 31 18 1 0.9714 -0.0339 31 18 3 -1.5997 0.0356 31 19 2 -4.6167 0.0114 31 19 4 6.5580 -0.0149 31 20 1 -2.5827 -0.0301 32 1 1 -1.4585 0.0574 32 1 3 -5.0915 -0.0131 32 1 5 -2.6891 -0.0131 32 1 7 -7.0871 0.0142 32 1 9 -4.4836 -0.0164 32 2 0 12.6808 0.0058 32 2 2 8.2219 0.0503 32 2 4 -2.3335 0.0065 32 2 6 7.6712 -0.0227 32 2 8 0.1713 -0.0072 32 3 1 -9.2771 -0.0265 32 3 3 -9.3232 -0.0209 32 3 5 -3.7531 -0.0027 32 3 7 3.2560 -0.0294 32 4 0 11.1701 -0.0754 32 4 2 0.7782 0.0244 32 4 4 1.1146 0.0189 32 4 6 1.5245 0.0093 32 4 8 -7.1493 0.0295 32 5 1 -4.7330 -0.0162 32 5 3 -9.6361 0.0049 32 5 5 4.4668 -0.0054 32 5 7 -2.3914 0.0070 32 6 0 2.4627 -0.0431 32 6 2 -16.4736 0.0213 32 6 4 -6.3037 -0.0436 32 6 6 -3.9539 -0.0047 32 6 8 10.3655 -0.0034 32 7 1 -2.3635 -0.0255 32 7 3 -8.1721 -0.0141 32 7 5 -0.4315 0.0258 32 7 7 3.9092 0.0312 32 8 0 -1.4246 0.0434 32 8 2 4.3830 0.0158 32 8 4 -0.4521 -0.0110 32 8 6 3.3938 0.0031 32 8 8 6.3096 -0.0437 32 9 1 -6.0055 -0.0611 32 9 3 -1.9687 0.0122 32 9 5 6.8001 0.0331 32 9 7 5.1223 -0.0179 32 10 0 -15.2982 -0.0094 32 10 2 -0.7750 -0.0467 32 10 4 -2.6566 0.0027 32 10 6 7.7444 0.0080 32 11 1 0.8084 0.0059 32 11 3 3.4401 0.0250 32 11 5 -1.8281 0.0004 32 11 7 -3.1466 -0.0120 32 12 0 3.4958 0.0678 32 12 2 -7.0818 -0.0104 32 12 4 -4.7069 -0.0168 32 12 6 -6.9841 -0.0022 32 13 1 -6.0639 0.0277 32 13 3 -3.6757 -0.0006 32 13 5 -0.9951 -0.0217 32 14 0 3.2982 0.0506 32 14 2 2.7254 -0.0063 32 14 4 6.6177 0.0134 32 14 6 6.1314 0.0204 32 15 1 9.5478 -0.0045 32 15 3 8.5273 -0.0226 32 15 5 7.4273 -0.0224 32 16 0 -1.0375 -0.0706 32 16 2 1.6767 -0.0107 32 16 4 4.9521 0.0152 32 17 1 0.4481 0.0389 32 17 3 -11.1411 -0.0076 32 18 0 7.0392 -0.0153 32 18 2 2.1520 0.0005 32 19 1 -2.4732 -0.0057 33 1 2 -11.8457 0.0213 33 1 4 -3.7159 -0.0329 33 1 6 -5.8890 -0.0339 33 1 8 -1.5658 0.0052 33 2 1 8.9306 -0.0308 33 2 3 -1.5335 0.0046 33 2 5 -4.3171 0.0160 33 2 7 4.3530 0.0301 33 3 2 -4.8917 -0.0043 33 3 4 -4.6514 -0.0141 33 3 6 -5.7046 -0.0197 33 3 8 -2.1345 -0.0047 33 4 1 4.6107 0.0127 33 4 3 -2.1812 0.0131 33 4 5 -2.4567 -0.0295 33 4 7 -1.4482 0.0226 33 5 2 -9.2526 -0.0231 33 5 4 -1.5334 -0.0104 33 5 6 5.8491 0.0348 33 6 1 -7.2106 -0.0342 33 6 3 1.9999 -0.0033 33 6 5 -1.5500 0.0108 33 6 7 3.7501 -0.0007 33 7 2 0.3233 0.0016 33 7 4 -0.3224 0.0095 33 7 6 -4.7553 0.0036 33 8 1 -9.3466 -0.0157 33 8 3 -2.4819 -0.0401 33 8 5 -3.7365 -0.0157 33 8 7 8.9085 0.0087 33 9 2 -2.4294 -0.0277 33 9 4 -0.2310 0.0361 33 9 6 0.0814 0.0237 33 10 1 -0.3454 0.0303 33 10 3 0.4345 0.0177 33 10 5 4.0324 -0.0174 33 11 2 3.3113 0.0188 33 11 4 0.4553 -0.0264 33 11 6 0.0615 -0.0013 33 12 1 -1.5627 0.0218 33 12 3 -3.0550 -0.0257 33 12 5 6.3273 0.0373 33 13 2 4.9903 0.0119 33 13 4 -0.0966 -0.0098 33 14 1 -1.6331 0.0174 33 14 3 0.7675 -0.0062 33 15 2 5.8461 -0.0236 33 15 4 5.8677 -0.0298 33 16 1 1.8545 -0.0152 33 16 3 1.7910 0.0201 34 1 1 -7.2068 0.0100 34 1 3 -8.3654 -0.0210 34 1 5 1.3972 -0.0354 34 1 7 2.0877 -0.0344 34 2 0 -0.6820 -0.0329 34 2 2 -9.6048 -0.0157 34 2 4 -5.3886 0.0207 34 2 6 4.1512 -0.0021 34 3 1 -12.4198 0.0146 34 3 3 -9.0809 -0.0228 34 3 5 -5.4632 -0.0168 34 3 7 -4.5199 0.0107 34 4 0 5.1890 -0.0571 34 4 2 -1.3528 0.0192 34 4 4 6.0769 -0.0075 34 4 6 0.1265 -0.0020 34 5 1 3.3986 0.0241 34 5 3 0.4804 -0.0479 34 5 5 7.3378 0.0135 34 6 0 1.0759 -0.0216 34 6 2 -5.7988 0.0157 34 6 4 -2.7040 0.0040 34 6 6 -3.7157 0.0112 34 7 1 -1.2218 -0.0399 34 7 3 -0.6265 0.0073 34 7 5 5.4730 0.0580 34 8 0 -17.4741 -0.0835 34 8 2 -0.1191 0.0112 34 8 4 -8.7771 -0.0149 34 8 6 1.8629 -0.0090 34 9 1 2.0799 0.0068 34 9 3 0.3050 0.0025 34 9 5 -6.9527 0.0342 34 10 0 -1.2804 0.0360 34 10 2 7.5090 -0.0033 34 10 4 1.2548 -0.0222 34 11 1 -5.5422 -0.0307 34 11 3 3.5175 0.0025 34 11 5 5.2788 0.0135 34 12 0 -2.0939 0.0658 34 12 2 2.1683 0.0099 34 12 4 4.4756 0.0070 34 13 1 6.5671 -0.0319 34 13 3 4.8531 -0.0059 34 14 0 6.6071 0.0063 34 14 2 -4.4154 -0.0101 34 15 1 -7.4477 0.0183 35 1 2 0.0621 -0.0077 35 1 4 -4.6952 -0.0237 35 1 6 -0.6637 -0.0274 35 2 1 7.9251 0.0273 35 2 3 -0.7599 0.0228 35 2 5 7.1432 -0.0222 35 3 2 -11.5337 0.0065 35 3 4 -2.7542 -0.0631 35 4 1 -8.2057 -0.0188 35 4 3 -2.8885 -0.0238 35 4 5 -2.5324 0.0360 35 5 2 -0.0236 0.0035 35 5 4 4.1266 0.0065 35 6 1 -3.2360 -0.0462 35 6 3 -0.5580 -0.0235 35 6 5 -6.9586 -0.0211 35 7 2 2.8832 -0.0094 35 7 4 0.9652 0.0315 35 8 1 -1.8254 -0.0200 35 8 3 1.0991 0.0176 35 9 2 -3.4981 0.0225 35 9 4 1.4465 0.0205 35 10 1 -5.9907 0.0063 35 10 3 -3.2661 -0.0194 35 11 2 6.4140 0.0059 35 12 1 8.7961 0.0566 36 1 1 -12.1333 0.0514 36 1 3 -0.0446 -0.0317 36 2 0 4.3010 0.0174 36 2 2 1.9757 -0.0370 36 2 4 1.1755 0.0068 36 3 1 -4.1598 0.0176 36 3 3 5.6531 -0.0273 36 4 0 -7.0068 0.0048 36 4 2 -1.2101 -0.0150 36 4 4 -6.8940 0.0136 36 5 1 7.3382 -0.0018 36 5 3 -5.6778 -0.0155 36 6 0 -4.3192 -0.1035 36 6 2 -0.0380 -0.0054 36 7 1 6.9252 0.0501 36 7 3 3.6615 -0.0104 36 8 0 -2.6304 -0.0298 36 8 2 3.4287 -0.0130 36 9 1 -6.4321 -0.0225 37 1 2 -3.7221 0.0077 37 2 1 -7.2067 0.0224 37 4 1 5.5544 -0.0090 0 0 0 0.0 0.0 ; _shelx_fab_checksum 96208 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_rom152_0ma_a _database_code_depnum_ccdc_archive 'CCDC 2122222' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-15 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_date 2021-02-25 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _shelx_SHELXL_version_number 2017/1 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C46 H68 K N2 O8 P' _chemical_formula_sum 'C46 H68 K N2 O8 P' _chemical_formula_weight 847.09 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_H-M_alt 'P n m a' _space_group_name_Hall '-P 2ac 2n' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' _cell_length_a 19.6406(14) _cell_length_b 24.8694(15) _cell_length_c 9.5347(6) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4657.2(5) _cell_formula_units_Z 4 _cell_measurement_reflns_used 36517 _cell_measurement_temperature 110(2) _cell_measurement_theta_max 28.303 _cell_measurement_theta_min 2.074 _shelx_estimated_absorpt_T_max 0.964 _shelx_estimated_absorpt_T_min 0.946 _exptl_absorpt_coefficient_mu 0.200 _exptl_absorpt_correction_T_max 0.964 _exptl_absorpt_correction_T_min 0.946 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Sadabs, Bruker-AXS' _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.208 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1824 _exptl_crystal_size_max 0.281 _exptl_crystal_size_mid 0.196 _exptl_crystal_size_min 0.186 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0555 _diffrn_reflns_av_unetI/netI 0.0388 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_k_max 33 _diffrn_reflns_limit_k_min -32 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 36517 _diffrn_reflns_point_group_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.303 _diffrn_reflns_theta_min 2.074 _diffrn_ambient_temperature 110(2) _diffrn_detector_area_resol_mean 1.75 _diffrn_measured_fraction_theta_full 0.991 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'ApexDuo, Bruker-AXS' _diffrn_measurement_method '1 deg. \f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'ImuS micro-focus' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4596 _reflns_number_total 5883 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'Saint, Bruker-AXS' _computing_data_collection 'Apex2, Bruker-AXS' _computing_data_reduction 'Saint, Bruker-AXS' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2017/1 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 1.583 _refine_diff_density_min -0.492 _refine_diff_density_rms 0.080 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.113 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 274 _refine_ls_number_reflns 5883 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0890 _refine_ls_R_factor_gt 0.0686 _refine_ls_restrained_S_all 1.113 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0759P)^2^+6.4178P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1678 _refine_ls_wR_factor_ref 0.1807 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C17(H17) 2.b Secondary CH2 refined with riding coordinates: C18(H18A,H18B), C19(H19A,H19B), C20(H20A,H20B), C21(H21A,H21B), C22(H22A, H22B), C23(H23A,H23B) 2.c Aromatic/amide H refined with riding coordinates: C3(H3), C5(H5), C16(H16) 2.d Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C9(H9A,H9B,H9C), C10(H10A,H10B,H10C), C12(H12A,H12B,H12C), C13(H13A,H13B,H13C), C14(H14A,H14B,H14C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group K1 K 0.64101(4) 0.250000 0.18672(8) 0.02128(18) Uani 1 2 d S T P . . P1 P 0.59416(4) 0.250000 0.82279(10) 0.0201(2) Uani 1 2 d S T P . . O1 O 0.52603(8) 0.29622(7) 0.80078(19) 0.0212(4) Uani 1 1 d . . . . . O2 O 0.53879(14) 0.250000 0.3842(3) 0.0329(6) Uani 1 2 d S T P . . O3 O 0.57589(10) 0.34649(7) 0.2514(2) 0.0275(4) Uani 1 1 d . . . . . O4 O 0.70632(10) 0.34958(7) 0.1208(2) 0.0265(4) Uani 1 1 d . . . . . O5 O 0.75832(13) 0.250000 0.0348(3) 0.0317(6) Uani 1 2 d S T P . . N1 N 0.64280(10) 0.29824(8) 0.7183(2) 0.0211(4) Uani 1 1 d . . . . . C1 C 0.54790(12) 0.34694(9) 0.7757(2) 0.0177(5) Uani 1 1 d . . . . . C2 C 0.61551(12) 0.34978(10) 0.7255(2) 0.0188(5) Uani 1 1 d . . . . . C3 C 0.64457(12) 0.39892(10) 0.6940(3) 0.0198(5) Uani 1 1 d . . . . . H3 H 0.690561 0.400635 0.663436 0.024 Uiso 1 1 calc R U . . . C4 C 0.60632(12) 0.44622(10) 0.7070(2) 0.0197(5) Uani 1 1 d . . . . . C5 C 0.53988(12) 0.44230(10) 0.7573(3) 0.0206(5) Uani 1 1 d . . . . . H5 H 0.513956 0.474346 0.766784 0.025 Uiso 1 1 calc R U . . . C6 C 0.50932(12) 0.39312(10) 0.7947(2) 0.0184(5) Uani 1 1 d . . . . . C7 C 0.43662(12) 0.38963(10) 0.8537(3) 0.0208(5) Uani 1 1 d . . . . . C8 C 0.39214(12) 0.35649(11) 0.7527(3) 0.0260(5) Uani 1 1 d . . . . . H8A H 0.389971 0.374616 0.661559 0.039 Uiso 1 1 calc R U . . . H8B H 0.346117 0.353137 0.791452 0.039 Uiso 1 1 calc R U . . . H8C H 0.412010 0.320636 0.740845 0.039 Uiso 1 1 calc R U . . . C9 C 0.40346(13) 0.44506(11) 0.8699(3) 0.0275(6) Uani 1 1 d . . . . . H9A H 0.430521 0.466974 0.934667 0.041 Uiso 1 1 calc R U . . . H9B H 0.357274 0.440820 0.907240 0.041 Uiso 1 1 calc R U . . . H9C H 0.401375 0.462824 0.778303 0.041 Uiso 1 1 calc R U . . . C10 C 0.43792(13) 0.36226(12) 0.9983(3) 0.0268(6) Uani 1 1 d . . . . . H10A H 0.454695 0.325348 0.988292 0.040 Uiso 1 1 calc R U . . . H10B H 0.391793 0.361652 1.037441 0.040 Uiso 1 1 calc R U . . . H10C H 0.468082 0.382339 1.061195 0.040 Uiso 1 1 calc R U . . . C11 C 0.63867(13) 0.49999(10) 0.6656(3) 0.0214(5) Uani 1 1 d . . . . . C12 C 0.69770(16) 0.51301(13) 0.7656(3) 0.0376(7) Uani 1 1 d . . . . . H12A H 0.680927 0.513495 0.862366 0.056 Uiso 1 1 calc R U . . . H12B H 0.716678 0.548307 0.741937 0.056 Uiso 1 1 calc R U . . . H12C H 0.733177 0.485529 0.756224 0.056 Uiso 1 1 calc R U . . . C13 C 0.58818(16) 0.54648(11) 0.6683(4) 0.0363(7) Uani 1 1 d . . . . . H13A H 0.550292 0.538651 0.604558 0.054 Uiso 1 1 calc R U . . . H13B H 0.611059 0.579538 0.638157 0.054 Uiso 1 1 calc R U . . . H13C H 0.570697 0.551145 0.763751 0.054 Uiso 1 1 calc R U . . . C14 C 0.66694(19) 0.49611(12) 0.5157(3) 0.0378(7) Uani 1 1 d . . . . . H14A H 0.701966 0.468089 0.511788 0.057 Uiso 1 1 calc R U . . . H14B H 0.686928 0.530713 0.488753 0.057 Uiso 1 1 calc R U . . . H14C H 0.629950 0.487069 0.450848 0.057 Uiso 1 1 calc R U . . . C15 C 0.68807(11) 0.27816(10) 0.6188(2) 0.0193(5) Uani 1 1 d . . . . . C16 C 0.72737(12) 0.30622(11) 0.5219(3) 0.0226(5) Uani 1 1 d . . . . . H16 H 0.727000 0.344418 0.520614 0.027 Uiso 1 1 calc R U . . . C17 C 0.76742(13) 0.27753(11) 0.4265(3) 0.0253(5) Uani 1 1 d . . . . . H17 H 0.809257 0.295801 0.390374 0.030 Uiso 1 1 calc R U . . . C18 C 0.49949(16) 0.29753(14) 0.3961(4) 0.0445(8) Uani 1 1 d . . . . . H18A H 0.475209 0.297790 0.487113 0.053 Uiso 1 1 calc R U . . . H18B H 0.465180 0.298788 0.320146 0.053 Uiso 1 1 calc R U . . . C19 C 0.54518(17) 0.34535(13) 0.3864(3) 0.0384(7) Uani 1 1 d . . . . . H19A H 0.518547 0.378647 0.401614 0.046 Uiso 1 1 calc R U . . . H19B H 0.580810 0.343285 0.459674 0.046 Uiso 1 1 calc R U . . . C20 C 0.61428(16) 0.39397(11) 0.2310(3) 0.0332(7) Uani 1 1 d . . . . . H20A H 0.645241 0.399566 0.311647 0.040 Uiso 1 1 calc R U . . . H20B H 0.583342 0.425305 0.224800 0.040 Uiso 1 1 calc R U . . . C21 C 0.65478(15) 0.38923(11) 0.0990(3) 0.0321(6) Uani 1 1 d . . . . . H21A H 0.624854 0.378432 0.020333 0.039 Uiso 1 1 calc R U . . . H21B H 0.675871 0.424254 0.075561 0.039 Uiso 1 1 calc R U . . . C22 C 0.74936(14) 0.34347(12) 0.0024(3) 0.0309(6) Uani 1 1 d . . . . . H22A H 0.775536 0.376948 -0.013356 0.037 Uiso 1 1 calc R U . . . H22B H 0.721614 0.336288 -0.082247 0.037 Uiso 1 1 calc R U . . . C23 C 0.79692(14) 0.29779(12) 0.0278(3) 0.0310(6) Uani 1 1 d . . . . . H23A H 0.830547 0.295410 -0.049286 0.037 Uiso 1 1 calc R U . . . H23B H 0.821847 0.303358 0.116897 0.037 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 K1 0.0178(3) 0.0181(4) 0.0280(4) 0.000 0.0066(3) 0.000 P1 0.0153(4) 0.0214(4) 0.0238(4) 0.000 0.0046(3) 0.000 O1 0.0158(8) 0.0191(9) 0.0286(9) -0.0010(7) 0.0032(7) 0.0017(6) O2 0.0249(13) 0.0436(17) 0.0301(15) 0.000 0.0076(12) 0.000 O3 0.0287(10) 0.0306(10) 0.0233(9) -0.0074(8) -0.0054(8) 0.0067(8) O4 0.0281(9) 0.0243(9) 0.0271(9) 0.0021(8) -0.0027(8) -0.0006(7) O5 0.0226(12) 0.0288(14) 0.0438(16) 0.000 0.0106(12) 0.000 N1 0.0179(9) 0.0203(10) 0.0253(11) 0.0014(8) 0.0074(8) -0.0002(8) C1 0.0175(11) 0.0205(11) 0.0151(10) -0.0012(9) -0.0007(9) -0.0001(9) C2 0.0182(11) 0.0228(12) 0.0153(10) -0.0004(9) -0.0002(9) 0.0017(9) C3 0.0180(10) 0.0229(12) 0.0184(11) 0.0008(9) 0.0023(9) -0.0007(9) C4 0.0223(11) 0.0211(12) 0.0155(10) -0.0008(9) 0.0000(9) -0.0020(9) C5 0.0212(11) 0.0217(12) 0.0190(11) -0.0027(9) -0.0009(9) 0.0025(9) C6 0.0166(10) 0.0233(12) 0.0153(10) -0.0028(9) -0.0010(8) 0.0003(9) C7 0.0155(10) 0.0245(12) 0.0224(12) -0.0032(10) 0.0005(9) 0.0013(9) C8 0.0152(11) 0.0341(14) 0.0285(13) -0.0072(11) -0.0019(10) -0.0014(10) C9 0.0226(12) 0.0278(14) 0.0320(14) -0.0018(11) 0.0028(11) 0.0046(11) C10 0.0237(12) 0.0339(14) 0.0229(12) -0.0008(11) 0.0051(10) 0.0010(11) C11 0.0248(12) 0.0186(11) 0.0207(11) -0.0025(9) 0.0021(10) -0.0026(9) C12 0.0355(16) 0.0416(17) 0.0356(16) -0.0015(14) -0.0025(13) -0.0161(13) C13 0.0383(16) 0.0215(13) 0.0491(18) -0.0013(13) 0.0063(14) -0.0019(12) C14 0.062(2) 0.0250(14) 0.0268(14) -0.0004(11) 0.0127(14) -0.0082(14) C15 0.0104(9) 0.0323(13) 0.0151(10) 0.0054(9) -0.0009(8) -0.0017(9) C16 0.0200(11) 0.0269(13) 0.0208(12) 0.0018(10) 0.0034(10) -0.0011(10) C17 0.0195(11) 0.0357(14) 0.0208(12) 0.0030(10) 0.0041(10) -0.0026(10) C18 0.0320(15) 0.063(2) 0.0384(17) -0.0032(16) 0.0148(14) 0.0141(15) C19 0.0404(16) 0.0467(18) 0.0280(15) -0.0114(13) 0.0036(13) 0.0179(14) C20 0.0401(16) 0.0249(14) 0.0347(15) -0.0059(12) -0.0099(13) 0.0089(12) C21 0.0358(15) 0.0207(13) 0.0398(16) 0.0031(11) -0.0134(13) 0.0007(11) C22 0.0311(13) 0.0300(14) 0.0316(14) 0.0061(11) 0.0004(12) -0.0104(11) C23 0.0226(12) 0.0401(16) 0.0303(14) 0.0045(12) 0.0060(11) -0.0066(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag K1 P1 3.5898(13) 1_554 ? K1 O2 2.752(3) . ? K1 O3 2.7883(18) . ? K1 O3 2.7883(18) 7_565 ? K1 O4 2.8589(19) 7_565 ? K1 O4 2.8589(19) . ? K1 O5 2.722(3) . ? K1 C17 3.444(3) . ? K1 C17 3.444(3) 7_565 ? P1 O1 1.7764(18) . ? P1 O1 1.7763(18) 7_565 ? P1 N1 1.829(2) 7_565 ? P1 N1 1.829(2) . ? O1 C1 1.354(3) . ? O2 C18 1.416(4) 7_565 ? O2 C18 1.416(4) . ? O3 C19 1.422(4) . ? O3 C20 1.414(4) . ? O4 C21 1.428(3) . ? O4 C22 1.419(3) . ? O5 C23 1.411(3) 7_565 ? O5 C23 1.411(3) . ? N1 C2 1.391(3) . ? N1 C15 1.393(3) . ? C1 C2 1.413(3) . ? C1 C6 1.388(3) . ? C2 C3 1.382(3) . ? C3 H3 0.9500 . ? C3 C4 1.401(3) . ? C4 C5 1.394(3) . ? C4 C11 1.532(3) . ? C5 H5 0.9500 . ? C5 C6 1.408(3) . ? C6 C7 1.537(3) . ? C7 C8 1.539(3) . ? C7 C9 1.532(3) . ? C7 C10 1.537(4) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 C12 1.535(4) . ? C11 C13 1.523(4) . ? C11 C14 1.537(4) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C15 1.401(5) 7_565 ? C15 C16 1.392(3) . ? C16 H16 0.9500 . ? C16 C17 1.399(4) . ? C17 C17 1.369(6) 7_565 ? C17 H17 1.0000 . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C18 C19 1.493(5) . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C20 C21 1.494(4) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C22 C23 1.491(4) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 K1 P1 118.31(7) . 1_554 ? O2 K1 O3 60.93(4) . 7_565 ? O2 K1 O3 60.93(4) . . ? O2 K1 O4 118.53(4) . 7_565 ? O2 K1 O4 118.53(4) . . ? O2 K1 C17 94.12(8) . 7_565 ? O2 K1 C17 94.12(8) . . ? O3 K1 P1 95.52(4) 7_565 1_554 ? O3 K1 P1 95.52(4) . 1_554 ? O3 K1 O3 118.77(9) 7_565 . ? O3 K1 O4 179.34(6) . 7_565 ? O3 K1 O4 60.59(6) 7_565 7_565 ? O3 K1 O4 179.34(6) 7_565 . ? O3 K1 O4 60.59(6) . . ? O3 K1 C17 110.79(6) 7_565 . ? O3 K1 C17 90.73(6) 7_565 7_565 ? O3 K1 C17 90.73(6) . . ? O3 K1 C17 110.79(6) . 7_565 ? O4 K1 P1 84.41(4) 7_565 1_554 ? O4 K1 P1 84.41(4) . 1_554 ? O4 K1 O4 120.05(8) 7_565 . ? O4 K1 C17 69.52(6) . . ? O4 K1 C17 89.69(6) 7_565 . ? O4 K1 C17 69.52(6) 7_565 7_565 ? O4 K1 C17 89.69(6) . 7_565 ? O5 K1 P1 72.70(7) . 1_554 ? O5 K1 O2 168.99(10) . . ? O5 K1 O3 120.40(4) . . ? O5 K1 O3 120.40(4) . 7_565 ? O5 K1 O4 60.21(4) . 7_565 ? O5 K1 O4 60.21(4) . . ? O5 K1 C17 75.10(8) . 7_565 ? O5 K1 C17 75.10(8) . . ? C17 K1 P1 145.73(5) . 1_554 ? C17 K1 P1 145.73(5) 7_565 1_554 ? C17 K1 C17 22.94(9) . 7_565 ? O1 P1 K1 107.90(7) 7_565 1_556 ? O1 P1 K1 107.90(7) . 1_556 ? O1 P1 O1 80.64(11) 7_565 . ? O1 P1 N1 84.53(9) . . ? O1 P1 N1 84.53(9) 7_565 7_565 ? O1 P1 N1 138.90(11) 7_565 . ? O1 P1 N1 138.90(11) . 7_565 ? N1 P1 K1 113.12(8) 7_565 1_556 ? N1 P1 K1 113.12(8) . 1_556 ? N1 P1 N1 81.99(13) 7_565 . ? C1 O1 P1 112.63(14) . . ? C18 O2 K1 116.91(17) 7_565 . ? C18 O2 K1 116.91(17) . . ? C18 O2 C18 113.1(3) . 7_565 ? C19 O3 K1 112.19(16) . . ? C20 O3 K1 116.33(16) . . ? C20 O3 C19 111.5(2) . . ? C21 O4 K1 108.18(15) . . ? C22 O4 K1 110.46(15) . . ? C22 O4 C21 112.4(2) . . ? C23 O5 K1 118.68(16) 7_565 . ? C23 O5 K1 118.68(16) . . ? C23 O5 C23 114.7(3) 7_565 . ? C2 N1 P1 112.10(15) . . ? C2 N1 C15 127.6(2) . . ? C15 N1 P1 117.98(16) . . ? O1 C1 C2 113.9(2) . . ? O1 C1 C6 125.1(2) . . ? C6 C1 C2 121.0(2) . . ? N1 C2 C1 109.4(2) . . ? C3 C2 N1 130.2(2) . . ? C3 C2 C1 120.4(2) . . ? C2 C3 H3 119.9 . . ? C2 C3 C4 120.1(2) . . ? C4 C3 H3 119.9 . . ? C3 C4 C11 119.2(2) . . ? C5 C4 C3 118.3(2) . . ? C5 C4 C11 122.5(2) . . ? C4 C5 H5 118.4 . . ? C4 C5 C6 123.2(2) . . ? C6 C5 H5 118.4 . . ? C1 C6 C5 116.9(2) . . ? C1 C6 C7 120.5(2) . . ? C5 C6 C7 122.5(2) . . ? C6 C7 C8 109.2(2) . . ? C6 C7 C10 109.8(2) . . ? C9 C7 C6 112.4(2) . . ? C9 C7 C8 107.7(2) . . ? C9 C7 C10 108.3(2) . . ? C10 C7 C8 109.5(2) . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C7 C9 H9A 109.5 . . ? C7 C9 H9B 109.5 . . ? C7 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C7 C10 H10A 109.5 . . ? C7 C10 H10B 109.5 . . ? C7 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C4 C11 C12 109.7(2) . . ? C4 C11 C14 109.5(2) . . ? C12 C11 C14 108.5(2) . . ? C13 C11 C4 112.8(2) . . ? C13 C11 C12 108.7(2) . . ? C13 C11 C14 107.3(2) . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C11 C13 H13A 109.5 . . ? C11 C13 H13B 109.5 . . ? C11 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C11 C14 H14A 109.5 . . ? C11 C14 H14B 109.5 . . ? C11 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? N1 C15 C15 111.02(13) . 7_565 ? C16 C15 N1 128.8(2) . . ? C16 C15 C15 120.10(15) . 7_565 ? C15 C16 H16 120.4 . . ? C15 C16 C17 119.2(3) . . ? C17 C16 H16 120.4 . . ? K1 C17 H17 117.0 . . ? C16 C17 K1 97.34(16) . . ? C16 C17 H17 117.0 . . ? C17 C17 K1 78.53(5) 7_565 . ? C17 C17 C16 120.68(15) 7_565 . ? C17 C17 H17 117.0 7_565 . ? O2 C18 H18A 109.8 . . ? O2 C18 H18B 109.8 . . ? O2 C18 C19 109.4(2) . . ? H18A C18 H18B 108.2 . . ? C19 C18 H18A 109.8 . . ? C19 C18 H18B 109.8 . . ? O3 C19 C18 109.1(2) . . ? O3 C19 H19A 109.9 . . ? O3 C19 H19B 109.9 . . ? C18 C19 H19A 109.9 . . ? C18 C19 H19B 109.9 . . ? H19A C19 H19B 108.3 . . ? O3 C20 H20A 109.8 . . ? O3 C20 H20B 109.8 . . ? O3 C20 C21 109.5(2) . . ? H20A C20 H20B 108.2 . . ? C21 C20 H20A 109.8 . . ? C21 C20 H20B 109.8 . . ? O4 C21 C20 108.0(2) . . ? O4 C21 H21A 110.1 . . ? O4 C21 H21B 110.1 . . ? C20 C21 H21A 110.1 . . ? C20 C21 H21B 110.1 . . ? H21A C21 H21B 108.4 . . ? O4 C22 H22A 109.9 . . ? O4 C22 H22B 109.9 . . ? O4 C22 C23 109.0(2) . . ? H22A C22 H22B 108.3 . . ? C23 C22 H22A 109.9 . . ? C23 C22 H22B 109.9 . . ? O5 C23 C22 108.2(2) . . ? O5 C23 H23A 110.1 . . ? O5 C23 H23B 110.1 . . ? C22 C23 H23A 110.1 . . ? C22 C23 H23B 110.1 . . ? H23A C23 H23B 108.4 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag K1 P1 O1 C1 88.10(15) 1_556 . . . ? K1 P1 N1 C2 -83.47(17) 1_556 . . . ? K1 P1 N1 C15 112.48(17) 1_556 . . . ? K1 O2 C18 C19 -41.4(3) . . . . ? K1 O3 C19 C18 -53.6(3) . . . . ? K1 O3 C20 C21 40.1(3) . . . . ? K1 O4 C21 C20 60.0(2) . . . . ? K1 O4 C22 C23 -53.4(2) . . . . ? K1 O5 C23 C22 -44.5(3) . . . . ? P1 O1 C1 C2 20.5(2) . . . . ? P1 O1 C1 C6 -160.13(19) . . . . ? P1 N1 C2 C1 -17.5(2) . . . . ? P1 N1 C2 C3 161.6(2) . . . . ? P1 N1 C15 C15 -0.56(18) . . . 7_565 ? P1 N1 C15 C16 175.8(2) . . . . ? O1 P1 O1 C1 -165.99(12) 7_565 . . . ? O1 P1 N1 C2 23.67(17) . . . . ? O1 P1 N1 C2 92.7(2) 7_565 . . . ? O1 P1 N1 C15 -71.4(2) 7_565 . . . ? O1 P1 N1 C15 -140.38(19) . . . . ? O1 C1 C2 N1 -1.5(3) . . . . ? O1 C1 C2 C3 179.3(2) . . . . ? O1 C1 C6 C5 -177.4(2) . . . . ? O1 C1 C6 C7 2.6(4) . . . . ? O2 C18 C19 O3 63.6(3) . . . . ? O3 C20 C21 O4 -69.0(3) . . . . ? O4 C22 C23 O5 65.7(3) . . . . ? N1 P1 O1 C1 -95.63(19) 7_565 . . . ? N1 P1 O1 C1 -24.45(17) . . . . ? N1 P1 N1 C2 164.75(12) 7_565 . . . ? N1 P1 N1 C15 0.7(2) 7_565 . . . ? N1 C2 C3 C4 178.8(2) . . . . ? N1 C15 C16 C17 -177.0(2) . . . . ? C1 C2 C3 C4 -2.2(4) . . . . ? C1 C6 C7 C8 -62.1(3) . . . . ? C1 C6 C7 C9 178.6(2) . . . . ? C1 C6 C7 C10 57.9(3) . . . . ? C2 N1 C15 C15 -161.8(2) . . . 7_565 ? C2 N1 C15 C16 14.6(4) . . . . ? C2 C1 C6 C5 2.0(3) . . . . ? C2 C1 C6 C7 -178.1(2) . . . . ? C2 C3 C4 C5 2.4(3) . . . . ? C2 C3 C4 C11 -177.5(2) . . . . ? C3 C4 C5 C6 -0.4(4) . . . . ? C3 C4 C11 C12 -65.8(3) . . . . ? C3 C4 C11 C13 172.8(2) . . . . ? C3 C4 C11 C14 53.3(3) . . . . ? C4 C5 C6 C1 -1.8(4) . . . . ? C4 C5 C6 C7 178.3(2) . . . . ? C5 C4 C11 C12 114.3(3) . . . . ? C5 C4 C11 C13 -7.1(3) . . . . ? C5 C4 C11 C14 -126.6(3) . . . . ? C5 C6 C7 C8 117.8(3) . . . . ? C5 C6 C7 C9 -1.5(3) . . . . ? C5 C6 C7 C10 -122.2(2) . . . . ? C6 C1 C2 N1 179.1(2) . . . . ? C6 C1 C2 C3 -0.1(3) . . . . ? C11 C4 C5 C6 179.5(2) . . . . ? C15 N1 C2 C1 144.7(2) . . . . ? C15 N1 C2 C3 -36.2(4) . . . . ? C15 C15 C16 C17 -0.9(3) 7_565 . . . ? C15 C16 C17 K1 81.9(2) . . . . ? C15 C16 C17 C17 1.0(3) . . . 7_565 ? C18 O2 C18 C19 178.39(19) 7_565 . . . ? C19 O3 C20 C21 170.5(2) . . . . ? C20 O3 C19 C18 173.9(2) . . . . ? C21 O4 C22 C23 -174.3(2) . . . . ? C22 O4 C21 C20 -177.8(2) . . . . ? C23 O5 C23 C22 166.8(2) 7_565 . . . ? _shelx_res_file ; TITL rom152_0ma_a_a.res in Pnma rom152_0ma_a.res created by SHELXL-2017/1 at 14:16:50 on 25-Feb-2021 REM Old TITL rom152_0ma_a in Pn21a #33 REM SHELXT solution in Pnma REM R1 0.137, Rweak 0.007, Alpha 0.031, Orientation as input REM Formula found by SHELXT: C46 K1 N2 O8 P CELL 0.71073 19.6406 24.8694 9.5347 90 90 90 ZERR 4 0.0014 0.0015 0.0006 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,-Z SYMM 0.5+X,0.5-Y,0.5-Z SFAC C H K N O P UNIT 184 272 4 8 32 4 L.S. 10 PLAN 6 SIZE 0.186 0.196 0.281 TEMP -163 CONF BOND $H list 4 fmap 2 acta MORE -1 OMIT 1 6 2 OMIT 3 4 2 OMIT 3 6 3 OMIT 1 3 1 OMIT 5 12 1 OMIT 8 8 0 OMIT 0 4 0 OMIT 5 1 3 OMIT 6 0 1 OMIT 6 3 0 OMIT 6 9 0 OMIT 8 3 0 OMIT 1 5 4 OMIT 0 12 0 OMIT 0 3 5 OMIT 0 6 0 OMIT 4 0 1 OMIT 4 11 4 OMIT 1 0 1 OMIT 2 6 5 OMIT 11 2 1 OMIT 6 0 6 OMIT 3 2 5 OMIT 0 2 4 OMIT 7 0 7 OMIT 0 0 6 OMIT 3 0 6 OMIT 6 3 6 OMIT 1 1 3 OMIT 6 2 8 OMIT 0 5 1 OMIT 9 3 6 OMIT 12 3 5 OMIT 2 4 6 OMIT 2 8 4 OMIT 6 1 1 OMIT 1 1 10 OMIT 5 0 5 REM REM REM WGHT 0.075900 6.417800 FVAR 0.27861 K1 3 0.641005 0.250000 0.186720 10.50000 0.01777 0.01812 = 0.02795 0.00000 0.00663 0.00000 P1 6 0.594157 0.250000 0.822795 10.50000 0.01533 0.02135 = 0.02376 0.00000 0.00462 0.00000 O1 5 0.526032 0.296219 0.800776 11.00000 0.01576 0.01911 = 0.02859 -0.00101 0.00325 0.00173 O2 5 0.538792 0.250000 0.384183 10.50000 0.02491 0.04358 = 0.03011 0.00000 0.00764 0.00000 O3 5 0.575888 0.346491 0.251404 11.00000 0.02866 0.03062 = 0.02333 -0.00736 -0.00539 0.00672 O4 5 0.706316 0.349580 0.120811 11.00000 0.02806 0.02435 = 0.02705 0.00215 -0.00271 -0.00055 O5 5 0.758324 0.250000 0.034797 10.50000 0.02258 0.02877 = 0.04376 0.00000 0.01063 0.00000 N1 4 0.642800 0.298244 0.718302 11.00000 0.01789 0.02031 = 0.02525 0.00136 0.00737 -0.00023 C1 1 0.547901 0.346936 0.775741 11.00000 0.01750 0.02053 = 0.01514 -0.00120 -0.00072 -0.00010 C2 1 0.615515 0.349779 0.725537 11.00000 0.01823 0.02276 = 0.01529 -0.00044 -0.00020 0.00174 C3 1 0.644572 0.398918 0.693983 11.00000 0.01802 0.02295 = 0.01843 0.00078 0.00228 -0.00070 AFIX 43 H3 2 0.690561 0.400635 0.663436 11.00000 -1.20000 AFIX 0 C4 1 0.606319 0.446218 0.706967 11.00000 0.02234 0.02114 = 0.01548 -0.00077 -0.00002 -0.00199 C5 1 0.539875 0.442301 0.757266 11.00000 0.02120 0.02168 = 0.01897 -0.00272 -0.00094 0.00251 AFIX 43 H5 2 0.513956 0.474346 0.766784 11.00000 -1.20000 AFIX 0 C6 1 0.509317 0.393122 0.794655 11.00000 0.01663 0.02334 = 0.01530 -0.00277 -0.00104 0.00035 C7 1 0.436623 0.389628 0.853723 11.00000 0.01546 0.02446 = 0.02240 -0.00322 0.00047 0.00134 C8 1 0.392139 0.356494 0.752719 11.00000 0.01522 0.03414 = 0.02849 -0.00716 -0.00194 -0.00138 AFIX 137 H8A 2 0.389971 0.374616 0.661559 11.00000 -1.50000 H8B 2 0.346117 0.353137 0.791452 11.00000 -1.50000 H8C 2 0.412010 0.320636 0.740845 11.00000 -1.50000 AFIX 0 C9 1 0.403459 0.445057 0.869945 11.00000 0.02257 0.02783 = 0.03202 -0.00185 0.00281 0.00462 AFIX 137 H9A 2 0.430521 0.466974 0.934667 11.00000 -1.50000 H9B 2 0.357274 0.440820 0.907240 11.00000 -1.50000 H9C 2 0.401375 0.462824 0.778303 11.00000 -1.50000 AFIX 0 C10 1 0.437915 0.362262 0.998261 11.00000 0.02373 0.03386 = 0.02291 -0.00077 0.00509 0.00101 AFIX 137 H10A 2 0.454695 0.325348 0.988292 11.00000 -1.50000 H10B 2 0.391793 0.361652 1.037441 11.00000 -1.50000 H10C 2 0.468082 0.382339 1.061195 11.00000 -1.50000 AFIX 0 C11 1 0.638674 0.499987 0.665614 11.00000 0.02479 0.01863 = 0.02073 -0.00250 0.00214 -0.00261 C12 1 0.697702 0.513007 0.765574 11.00000 0.03550 0.04162 = 0.03559 -0.00148 -0.00252 -0.01606 AFIX 137 H12A 2 0.680927 0.513495 0.862366 11.00000 -1.50000 H12B 2 0.716678 0.548307 0.741937 11.00000 -1.50000 H12C 2 0.733177 0.485529 0.756224 11.00000 -1.50000 AFIX 0 C13 1 0.588177 0.546476 0.668256 11.00000 0.03829 0.02146 = 0.04906 -0.00134 0.00632 -0.00186 AFIX 137 H13A 2 0.550292 0.538651 0.604558 11.00000 -1.50000 H13B 2 0.611059 0.579538 0.638157 11.00000 -1.50000 H13C 2 0.570697 0.551145 0.763751 11.00000 -1.50000 AFIX 0 C14 1 0.666940 0.496114 0.515671 11.00000 0.06170 0.02497 = 0.02678 -0.00041 0.01271 -0.00825 AFIX 137 H14A 2 0.701966 0.468089 0.511788 11.00000 -1.50000 H14B 2 0.686928 0.530713 0.488753 11.00000 -1.50000 H14C 2 0.629950 0.487069 0.450848 11.00000 -1.50000 AFIX 0 C15 1 0.688071 0.278160 0.618810 11.00000 0.01045 0.03229 = 0.01510 0.00541 -0.00093 -0.00169 C16 1 0.727371 0.306223 0.521916 11.00000 0.01997 0.02691 = 0.02079 0.00177 0.00337 -0.00106 AFIX 43 H16 2 0.727000 0.344418 0.520614 11.00000 -1.20000 AFIX 0 C17 1 0.767422 0.277532 0.426470 11.00000 0.01945 0.03565 = 0.02080 0.00297 0.00406 -0.00259 AFIX 13 H17 2 0.809257 0.295801 0.390374 11.00000 -1.20000 AFIX 0 C18 1 0.499495 0.297526 0.396131 11.00000 0.03201 0.06292 = 0.03845 -0.00320 0.01480 0.01410 AFIX 23 H18A 2 0.475209 0.297790 0.487113 11.00000 -1.20000 H18B 2 0.465180 0.298788 0.320146 11.00000 -1.20000 AFIX 0 C19 1 0.545177 0.345353 0.386433 11.00000 0.04044 0.04672 = 0.02795 -0.01137 0.00357 0.01786 AFIX 23 H19A 2 0.518547 0.378647 0.401614 11.00000 -1.20000 H19B 2 0.580810 0.343285 0.459674 11.00000 -1.20000 AFIX 0 C20 1 0.614276 0.393967 0.231030 11.00000 0.04005 0.02485 = 0.03469 -0.00589 -0.00990 0.00886 AFIX 23 H20A 2 0.645241 0.399566 0.311647 11.00000 -1.20000 H20B 2 0.583342 0.425305 0.224800 11.00000 -1.20000 AFIX 0 C21 1 0.654778 0.389233 0.098994 11.00000 0.03580 0.02070 = 0.03978 0.00308 -0.01345 0.00069 AFIX 23 H21A 2 0.624854 0.378432 0.020333 11.00000 -1.20000 H21B 2 0.675871 0.424254 0.075561 11.00000 -1.20000 AFIX 0 C22 1 0.749359 0.343469 0.002392 11.00000 0.03109 0.02998 = 0.03164 0.00607 0.00045 -0.01036 AFIX 23 H22A 2 0.775536 0.376948 -0.013356 11.00000 -1.20000 H22B 2 0.721614 0.336288 -0.082247 11.00000 -1.20000 AFIX 0 C23 1 0.796925 0.297793 0.027821 11.00000 0.02261 0.04011 = 0.03029 0.00452 0.00602 -0.00664 AFIX 23 H23A 2 0.830547 0.295410 -0.049286 11.00000 -1.20000 H23B 2 0.821847 0.303358 0.116897 11.00000 -1.20000 AFIX 0 HKLF 4 REM rom152_0ma_a_a.res in Pnma REM R1 = 0.0686 for 4596 Fo > 4sig(Fo) and 0.0890 for all 5883 data REM 274 parameters refined using 0 restraints END WGHT 0.0754 6.4337 REM Highest difference peak 1.583, deepest hole -0.492, 1-sigma level 0.080 Q1 1 0.6146 0.2500 0.9317 10.50000 0.05 1.58 Q2 1 0.6977 0.2500 0.5714 10.50000 0.05 1.39 Q3 1 0.6352 0.2500 0.2593 10.50000 0.05 0.76 Q4 1 0.6102 0.2792 0.7532 11.00000 0.05 0.63 Q5 1 0.7859 0.2500 0.1050 10.50000 0.05 0.57 Q6 1 0.6401 0.2887 0.1813 11.00000 0.05 0.55 ; _shelx_res_checksum 10494 _shelx_hkl_file ; 0 0 1 0.10 0.40 0 0 1 0.40 0.30 0 0 -1 0.80 0.40 0 0 -1 0.50 0.40 0 0 -1 0.40 0.30 0 0 1 0.30 0.40 0 0 2 7456.35 254.57 0 0 2 7296.37 254.27 0 0 -2 7325.87 254.17 0 0 -2 7073.19 255.17 0 0 -2 7709.83 254.37 0 0 2 7321.07 253.07 0 0 -4 1703.23 58.09 0 0 4 1670.43 57.99 0 0 -4 1593.84 58.39 0 0 -4 1685.03 58.09 0 0 -5 11.70 2.20 0 0 5 11.00 2.20 0 0 -5 6.40 2.50 0 0 -6 57.49 4.20 0 0 6 52.89 3.90 0 0 7 21.70 3.20 0 0 -7 26.20 3.80 0 0 -8 219.68 10.50 0 0 8 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14.30 4.90 10 -4 -10 16.00 4.80 10 -4 11 7.70 5.00 10 4 -11 10.80 4.70 10 -4 -11 12.90 5.30 -10 -4 11 9.30 5.10 10 4 11 7.10 4.90 11 -4 0 -2.30 1.50 11 -4 0 -1.60 1.40 11 4 0 -1.60 1.10 -11 -4 0 0.30 0.80 -11 -4 0 -1.20 3.10 11 4 -1 -0.30 0.90 11 -4 1 -1.40 1.60 11 -4 -1 0.30 1.70 -11 -4 1 1.60 3.20 11 4 1 -1.20 1.20 11 -4 -1 0.50 1.60 -11 -4 1 0.10 0.80 11 -4 2 10.70 2.50 11 4 -2 17.50 2.80 11 4 2 11.80 2.10 11 -4 -2 9.70 2.50 -11 -4 2 13.20 1.50 -11 -4 2 9.80 3.70 11 -4 -2 18.30 2.70 11 4 -3 1.50 1.90 -11 4 3 -0.70 3.30 11 -4 3 0.60 2.00 -11 -4 3 5.70 3.20 11 -4 -3 0.30 1.80 11 -4 -3 4.10 2.10 -11 -4 3 0.40 1.10 11 4 3 1.10 1.50 -11 4 4 72.69 6.20 11 -4 4 73.29 5.50 11 4 -4 60.69 4.70 -11 -4 4 59.19 3.70 11 4 4 63.49 4.60 11 -4 -4 72.99 5.10 -11 -4 4 64.19 6.00 11 -4 5 -1.70 2.60 11 4 -5 -0.70 2.30 -11 4 5 -2.40 3.10 11 -4 -5 2.10 2.40 -11 -4 5 -3.90 3.10 11 4 5 -2.10 2.40 -11 4 6 50.19 6.00 11 -4 6 61.19 6.00 11 4 -6 49.90 5.30 -11 -4 6 59.69 7.00 11 -4 -6 62.99 5.80 11 4 6 48.40 5.20 11 -4 7 46.90 5.50 11 4 -7 45.30 5.00 -11 4 7 49.20 6.30 11 4 7 48.30 5.60 11 -4 -7 43.90 5.40 -11 -4 7 53.29 6.60 -11 4 8 10.00 4.10 11 -4 8 9.70 4.00 11 4 -8 8.40 3.40 11 -4 -8 7.60 3.70 -11 -4 8 10.60 4.30 11 4 8 8.30 3.80 11 -4 9 5.00 4.10 11 4 -9 -0.90 2.80 -11 4 9 3.20 3.50 11 -4 -9 3.60 3.60 -11 -4 9 3.50 3.90 11 4 9 -0.90 3.70 11 4 -10 26.50 4.90 11 -4 10 34.50 6.30 -11 4 10 44.10 6.00 11 -4 -10 29.30 5.70 -11 -4 10 42.10 6.70 11 4 10 25.50 5.70 11 4 -11 13.10 4.80 11 -4 11 15.70 5.90 11 4 11 7.80 5.00 11 -4 -11 11.90 4.90 -11 -4 11 20.40 5.80 12 -4 0 23.90 3.20 -12 -4 0 32.40 2.30 12 -4 0 31.70 3.60 -12 -4 0 29.80 5.10 12 4 0 26.60 2.60 12 4 -1 190.38 8.00 12 -4 1 202.18 9.40 12 -4 -1 207.68 9.30 12 -4 -1 205.08 9.40 12 4 1 210.48 8.60 -12 -4 1 184.78 10.70 -12 -4 1 208.28 7.90 12 4 -2 10.70 2.60 12 -4 2 13.30 2.80 12 4 -2 10.20 1.60 -12 -4 2 12.30 1.50 -12 -4 2 11.70 4.20 12 4 2 13.80 2.40 12 -4 -2 12.30 2.40 12 -4 -2 13.70 2.70 12 4 -3 197.58 9.90 -12 4 3 236.18 11.80 12 -4 3 214.38 10.30 12 -4 -3 242.48 10.40 -12 -4 3 200.28 8.50 12 4 3 201.48 9.50 12 -4 -3 240.28 10.10 -12 -4 3 207.28 11.30 12 -4 4 16.00 3.30 12 4 -4 7.70 2.60 -12 4 4 12.70 4.40 -12 -4 4 11.40 3.70 -12 -4 4 4.20 1.40 12 -4 -4 13.50 3.00 12 4 4 5.70 2.40 12 -4 5 3.10 3.00 12 4 -5 2.10 2.40 -12 4 5 2.90 3.90 12 -4 -5 -0.20 2.50 -12 -4 5 7.70 4.10 12 4 5 4.90 2.60 12 4 -6 2.60 2.50 12 -4 6 4.10 2.70 -12 4 6 10.60 4.20 -12 -4 6 4.40 3.80 12 4 6 2.60 2.80 12 -4 7 30.90 4.80 -12 4 7 42.70 6.00 12 4 -7 31.10 4.40 -12 -4 7 38.70 6.10 12 4 7 41.80 5.20 12 -4 -7 47.40 5.60 12 -4 8 5.50 3.80 -12 4 8 3.30 3.90 12 4 -8 5.20 3.30 12 -4 -8 6.30 3.50 -12 -4 8 8.20 4.20 12 4 8 3.50 3.50 12 4 -9 18.50 4.30 12 -4 9 30.80 6.00 -12 4 9 37.20 5.80 12 -4 -9 25.80 5.00 -12 -4 9 27.40 5.60 12 4 9 27.40 5.30 12 -4 10 7.90 4.90 -12 4 10 8.00 4.10 12 4 -10 -1.90 3.10 -12 -4 10 3.90 4.00 12 4 10 10.40 4.90 12 -4 -10 -0.40 4.30 12 4 -11 10.70 4.80 12 -4 11 10.20 5.60 -12 -4 11 19.30 5.50 12 4 11 3.80 4.90 12 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29.20 6.20 14 4 -5 23.70 4.00 -14 -4 5 25.20 5.60 14 4 5 14.70 3.40 14 -4 -5 20.30 3.90 -14 4 6 4.40 4.10 14 -4 6 9.30 3.90 14 4 -6 2.40 2.80 14 -4 -6 10.10 3.60 14 4 6 8.20 3.30 -14 -4 6 3.20 4.10 14 -4 7 72.89 7.30 -14 4 7 58.89 7.00 14 4 -7 36.50 5.20 14 -4 -7 63.09 6.60 14 4 7 48.00 5.90 -14 -4 7 61.29 7.70 14 4 -8 18.40 4.50 -14 4 8 26.40 5.60 14 -4 8 15.70 4.90 -14 -4 8 16.10 5.50 14 4 8 12.60 4.50 14 -4 -8 13.40 4.40 14 -4 9 42.00 6.90 14 4 -9 27.20 5.30 -14 4 9 40.70 6.10 14 4 9 19.00 5.40 14 -4 -9 28.40 5.70 -14 -4 9 35.60 6.30 14 4 -10 5.80 4.30 -14 4 10 14.20 4.70 14 -4 10 -4.50 4.60 -14 -4 10 8.50 4.80 14 4 10 -4.90 4.30 14 -4 -10 4.80 5.00 15 -4 0 -2.00 2.10 15 4 0 -0.20 1.50 -15 -4 0 -1.90 4.30 15 -4 0 0.00 2.10 15 4 -1 69.89 4.20 15 -4 1 67.29 5.50 15 -4 1 76.69 5.60 15 4 -1 61.09 5.80 15 -4 -1 70.19 5.20 15 4 1 63.79 4.50 15 -4 -1 69.09 5.50 -15 -4 1 78.39 8.50 15 4 -2 11.20 3.10 15 4 -2 9.30 1.90 15 -4 2 15.60 3.40 15 -4 -2 12.40 3.30 15 -4 -2 23.60 3.50 15 4 2 12.50 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-4 0 180.38 11.70 16 -4 0 190.68 9.70 16 -4 1 1.00 2.60 16 4 -1 1.70 2.80 16 4 -1 1.50 1.80 -16 -4 -1 -1.10 4.70 16 -4 1 3.80 2.80 16 4 1 -0.90 1.90 16 -4 -1 3.90 2.70 16 -4 -1 4.90 2.60 -16 -4 1 -1.50 4.50 16 4 -2 48.30 5.30 16 -4 2 42.30 5.00 16 4 -2 36.40 3.20 -16 4 2 52.59 7.90 16 4 2 37.00 4.20 16 -4 -2 46.20 5.20 -16 -4 2 43.10 7.20 16 -4 -2 47.50 4.60 16 -4 3 -0.50 2.80 16 4 -3 -1.30 2.70 -16 4 3 0.40 4.90 16 -4 -3 1.30 2.80 16 4 3 1.50 2.60 -16 -4 3 4.40 4.90 16 -4 -3 1.90 2.30 16 -4 4 52.19 5.90 16 4 -4 51.39 5.70 -16 4 4 63.49 8.60 -16 -4 4 61.99 8.00 16 4 4 54.09 5.40 16 -4 -4 43.20 5.50 16 -4 5 4.90 3.60 -16 4 5 5.50 4.80 16 4 -5 1.10 3.00 16 -4 -5 1.30 3.00 16 4 5 2.60 2.80 -16 -4 5 0.10 4.20 -16 4 6 125.59 9.70 16 -4 6 127.19 9.30 16 4 -6 136.29 8.90 16 4 6 128.59 8.60 -16 -4 6 128.99 9.90 16 -4 -6 142.09 9.10 16 4 -7 77.99 7.50 -16 4 7 86.29 8.60 16 -4 7 85.79 8.30 16 4 7 64.99 7.20 -16 -4 7 90.29 8.50 16 -4 -7 79.79 7.90 16 -4 8 14.00 5.20 -16 4 8 13.50 5.30 16 4 -8 5.30 3.70 -16 -4 8 5.00 4.70 16 -4 -8 2.40 4.30 16 4 8 2.50 3.90 16 4 -9 49.00 6.60 16 -4 9 53.89 8.10 -16 4 9 75.39 8.70 -16 -4 9 60.39 8.40 16 -4 -9 49.10 7.00 16 4 9 60.89 8.00 17 -4 0 -2.70 2.60 -17 -4 0 0.00 4.70 17 -4 0 -0.70 2.70 17 4 0 -2.80 1.80 17 4 -1 25.50 4.40 17 4 -1 27.30 3.10 -17 -4 -1 30.40 6.80 17 -4 1 31.50 4.60 17 -4 1 25.40 4.40 17 -4 -1 36.60 4.40 17 -4 -1 34.10 4.70 -17 -4 1 30.20 6.90 17 4 1 34.10 3.90 17 4 -2 95.39 7.20 17 -4 2 118.99 7.60 -17 4 2 105.39 9.60 17 4 -2 109.99 5.60 17 4 2 109.89 6.60 17 -4 -2 106.39 7.10 -17 -4 2 114.49 9.60 17 -4 -2 111.69 7.50 17 4 -3 57.49 6.20 17 -4 3 56.09 6.00 -17 4 3 83.89 9.40 17 4 3 49.60 5.20 -17 -4 3 60.59 8.30 17 -4 -3 65.79 6.50 17 -4 -3 59.09 5.20 17 4 -4 20.60 4.20 17 -4 4 25.30 4.60 -17 4 4 17.00 6.00 17 -4 -4 18.40 4.10 17 4 4 17.10 3.70 -17 -4 4 21.70 5.90 -17 4 5 287.27 16.00 17 -4 5 341.17 15.50 17 4 -5 272.67 14.20 17 -4 -5 345.67 15.10 17 4 5 295.87 14.20 -17 -4 5 301.77 16.20 -17 4 6 5.20 4.90 17 -4 6 5.20 4.00 17 4 -6 0.80 3.20 17 -4 -6 0.90 3.30 -17 -4 6 5.60 4.70 17 4 6 7.10 3.90 17 4 -7 1.90 3.60 -17 4 7 8.40 4.90 17 -4 7 3.00 4.00 17 -4 -7 5.80 4.70 17 4 7 0.50 3.40 -17 -4 7 10.20 5.50 17 4 -8 0.20 3.60 17 -4 8 4.00 4.70 -17 4 8 8.30 5.10 -17 -4 8 5.70 4.70 17 4 8 -2.40 4.20 17 -4 -8 -3.60 4.10 -17 4 9 9.40 5.20 17 -4 9 7.20 5.40 17 4 -9 -0.70 3.60 17 -4 -9 3.80 4.80 17 4 9 0.90 4.40 -17 -4 9 8.00 5.00 18 -4 0 567.54 22.90 18 -4 0 569.54 23.40 -18 -4 0 578.34 25.60 18 4 0 561.54 21.70 18 -4 1 7.10 3.30 18 4 -1 0.80 3.10 -18 -4 -1 -3.60 4.90 18 -4 1 5.10 3.10 18 4 -1 3.40 2.10 18 -4 -1 10.90 3.60 -18 -4 1 6.10 5.30 18 -4 -1 5.90 3.20 18 4 1 4.10 2.50 18 -4 2 245.88 12.20 18 -4 2 234.28 12.10 18 4 -2 263.27 12.50 18 4 -2 236.48 10.10 -18 4 2 225.38 14.40 -18 -4 2 236.38 14.30 18 -4 -2 265.37 12.50 18 4 2 229.88 11.10 18 -4 -2 233.88 11.40 18 4 -3 10.90 3.70 18 -4 3 5.30 3.40 -18 4 3 5.00 5.40 18 -4 -3 1.90 3.40 -18 -4 3 10.10 5.60 18 4 3 4.00 2.90 18 -4 -3 3.80 3.00 -18 4 4 10.00 6.00 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1.50 3.80 8 -5 9 9.60 3.90 -8 -5 9 8.90 2.70 8 -5 -9 7.80 3.70 8 5 9 5.50 3.40 -8 -5 9 10.20 4.00 8 5 -10 7.50 3.70 8 -5 10 9.40 4.40 -8 5 10 16.10 3.90 -8 -5 10 5.70 3.20 -8 -5 10 7.20 4.10 8 -5 -10 11.50 4.80 8 5 10 10.50 4.30 8 -5 11 1.30 4.60 8 5 -11 2.90 3.90 -8 -5 11 2.50 4.00 8 -5 -11 1.20 4.80 8 5 11 -1.80 4.20 -8 -5 11 -3.70 3.20 9 5 0 -0.10 0.90 -9 -5 0 -2.00 2.60 9 -5 0 -0.20 1.60 9 -5 0 -0.70 1.40 9 -5 1 27.40 3.20 9 5 -1 23.90 1.60 -9 -5 -1 29.10 4.10 9 5 1 24.10 2.20 -9 -5 1 27.90 4.20 9 -5 -1 26.20 3.00 -9 -5 1 25.90 1.50 9 -5 -1 30.50 3.10 9 5 -2 373.66 15.00 9 -5 2 365.76 15.20 9 -5 -2 409.36 15.30 9 5 2 391.16 14.40 9 -5 -2 419.36 15.30 -9 -5 2 364.06 16.00 -9 -5 2 360.86 13.50 9 5 -3 158.68 7.50 -9 5 3 155.88 8.50 9 -5 3 156.38 8.00 -9 -5 3 147.39 6.20 9 -5 -3 161.48 7.70 -9 -5 3 154.98 8.50 9 5 3 164.98 7.30 9 -5 -3 188.18 8.00 -9 5 4 78.29 5.70 9 -5 4 80.29 5.40 9 5 -4 61.19 4.30 -9 -5 4 62.29 3.60 9 5 4 65.89 4.30 -9 -5 4 57.39 5.30 9 -5 -4 73.19 4.90 9 -5 5 18.60 3.40 9 5 -5 22.20 3.10 -9 5 5 23.90 4.30 9 5 5 24.40 3.30 -9 -5 5 30.70 4.70 9 -5 -5 26.00 3.60 9 5 -6 0.20 2.20 -9 5 6 -2.20 2.80 9 -5 6 -0.30 2.60 9 -5 -6 3.40 2.60 -9 -5 6 -3.50 2.90 9 5 6 0.90 2.30 -9 5 7 9.20 3.30 9 -5 7 8.70 3.00 9 5 -7 4.00 2.60 -9 -5 7 15.00 4.20 9 5 7 14.30 3.40 9 -5 -7 5.60 3.10 9 -5 8 3.20 2.80 -9 5 8 9.90 3.50 9 5 -8 2.00 2.40 9 -5 -8 -0.30 2.90 9 5 8 3.60 3.00 -9 -5 8 2.90 3.50 9 -5 9 11.90 4.40 9 5 -9 15.10 3.80 -9 5 9 22.30 4.20 9 5 -9 13.00 4.40 -9 -5 9 6.00 2.90 9 -5 -9 15.10 4.40 -9 -5 9 19.30 4.90 9 5 9 22.30 4.60 9 5 -10 32.50 5.30 9 -5 10 33.30 6.10 -9 5 10 39.70 5.40 -9 -5 10 25.00 4.40 9 5 10 33.60 6.00 -9 -5 10 37.60 6.70 9 -5 -10 34.90 6.00 9 -5 11 19.40 5.10 9 5 -11 20.30 5.00 9 5 11 19.10 5.60 -9 -5 11 24.30 5.50 9 -5 -11 10.10 5.00 -10 -5 0 13.40 3.80 10 -5 0 16.50 2.50 10 -5 0 15.40 2.60 10 5 0 16.20 1.70 -10 -5 -1 488.85 19.80 10 -5 1 492.05 18.70 10 -5 1 489.55 19.00 10 5 -1 459.35 17.30 -10 -5 1 482.35 17.20 10 5 1 505.35 17.90 10 -5 -1 488.35 18.80 -10 -5 1 478.55 19.90 10 -5 -1 510.65 18.90 10 -5 2 441.46 17.60 10 5 -2 414.16 17.20 -10 -5 2 436.36 18.40 10 -5 -2 474.25 17.60 10 -5 -2 464.05 17.50 -10 -5 2 419.86 15.70 10 5 2 466.45 16.80 10 -5 3 102.69 6.20 -10 5 3 98.19 6.90 10 5 -3 102.79 5.70 10 -5 -3 109.89 6.00 -10 -5 3 92.99 4.30 10 5 3 95.19 5.20 -10 -5 3 90.79 6.60 10 -5 -3 114.09 6.00 -10 5 4 51.99 5.70 10 -5 4 52.39 5.00 10 5 -4 46.20 3.90 -10 -5 4 50.69 5.80 10 5 4 45.10 3.80 10 -5 -4 53.29 4.30 -10 -5 4 41.30 2.90 10 -5 5 163.88 8.90 10 5 -5 153.28 8.10 -10 5 5 149.19 8.80 10 5 5 170.78 8.20 10 -5 -5 172.78 8.60 -10 -5 5 159.98 9.20 10 5 -6 8.40 2.70 -10 5 6 17.70 4.20 10 -5 6 12.00 3.50 10 -5 -6 18.00 3.50 -10 -5 6 7.90 4.10 10 5 6 8.90 2.90 -10 5 7 107.09 7.40 10 5 -7 110.49 6.90 10 -5 7 106.19 7.30 10 5 7 105.69 7.30 10 -5 -7 113.89 7.50 -10 -5 7 109.39 8.00 10 5 -8 3.50 2.90 -10 5 8 1.60 2.90 10 -5 8 -3.90 3.00 -10 -5 8 -0.60 3.50 10 5 8 -0.10 2.20 10 -5 -8 0.50 3.30 10 -5 9 43.60 6.20 10 5 -9 40.70 5.00 -10 5 9 34.10 5.20 -10 -5 9 39.90 6.20 -10 -5 9 27.10 3.90 10 5 9 33.20 5.50 10 -5 -9 33.10 5.50 10 -5 10 17.40 5.10 -10 5 10 26.70 4.90 10 5 -10 19.60 4.20 -10 -5 10 22.30 6.20 -10 -5 10 29.80 6.30 10 -5 -10 19.60 5.60 10 5 10 28.70 5.80 10 5 -11 23.50 5.30 10 -5 11 30.40 6.70 10 5 11 27.80 6.20 -10 -5 11 41.90 6.90 10 -5 -11 28.70 6.20 11 -5 0 -2.20 1.80 -11 -5 0 -5.10 2.90 -11 -5 0 -0.10 0.70 11 5 0 -1.40 0.90 11 -5 0 -1.40 1.90 11 5 -1 83.59 4.00 11 -5 1 92.29 5.30 -11 -5 -1 98.59 6.80 11 -5 1 89.69 5.60 -11 -5 1 97.29 3.90 -11 -5 1 89.59 6.70 11 5 1 86.79 4.50 11 -5 -1 91.79 5.30 11 -5 -1 91.49 5.50 11 5 -2 282.97 12.20 11 -5 2 304.77 12.70 -11 -5 2 273.77 10.60 11 5 2 295.87 11.60 11 -5 -2 306.57 12.50 -11 -5 2 280.47 13.50 11 -5 -2 295.57 12.30 11 5 -3 77.79 5.10 -11 5 3 77.89 6.50 11 -5 3 72.69 5.50 -11 -5 3 78.19 6.30 11 5 3 72.69 4.80 -11 -5 3 76.89 3.70 11 -5 -3 90.89 5.40 11 -5 -3 84.89 5.40 11 5 -4 305.27 13.40 -11 5 4 325.17 14.80 11 -5 4 326.87 14.20 11 -5 -4 344.97 13.90 -11 -5 4 307.57 12.10 11 5 4 333.67 13.40 -11 -5 4 307.07 14.70 11 5 -5 0.90 2.40 11 -5 5 1.50 2.70 -11 5 5 1.10 3.70 11 5 5 6.30 2.40 11 -5 -5 2.40 2.60 -11 -5 5 -0.30 3.30 -11 5 6 24.50 4.80 11 5 -6 14.90 3.20 11 -5 6 16.60 3.50 -11 -5 6 20.90 4.90 11 -5 -6 15.50 3.60 11 5 6 16.60 3.50 -11 5 7 20.50 4.50 11 -5 7 13.70 3.60 11 5 -7 10.30 3.40 -11 -5 7 15.60 4.70 11 -5 -7 15.80 3.90 11 5 7 10.40 3.60 11 5 -8 16.30 3.70 -11 5 8 12.40 4.00 11 -5 8 6.60 3.90 11 -5 -8 8.10 3.70 11 5 8 2.10 3.50 -11 -5 8 10.40 4.40 -11 5 9 5.00 3.60 11 5 -9 1.50 2.90 11 -5 9 1.20 3.20 11 -5 -9 9.10 4.10 -11 -5 9 8.00 4.20 11 5 9 4.10 3.80 -11 5 10 80.49 7.00 11 -5 10 76.29 8.60 11 5 -10 70.39 7.00 11 -5 -10 65.69 7.70 11 5 10 71.99 8.10 -11 -5 10 73.09 8.80 11 -5 11 2.00 5.10 11 5 -11 4.70 4.30 11 -5 -11 0.20 4.40 -11 -5 11 8.20 5.20 11 5 11 4.90 4.80 -12 -5 0 70.59 3.50 -12 -5 0 65.19 6.20 12 -5 0 70.29 5.10 12 5 0 73.79 3.90 12 -5 0 76.69 5.10 12 5 -1 94.29 4.40 12 -5 1 111.19 6.20 -12 -5 -1 86.09 7.00 12 -5 1 100.59 5.90 12 5 1 86.19 4.90 12 -5 -1 102.89 5.90 -12 -5 1 101.39 4.30 12 -5 -1 106.89 6.00 -12 -5 1 90.89 7.20 12 5 -2 3.20 2.00 12 -5 2 6.20 2.40 -12 -5 2 1.50 3.40 -12 -5 2 3.40 1.00 12 -5 -2 3.80 2.10 12 5 2 2.80 1.70 12 -5 -2 7.60 2.20 -12 5 3 197.78 10.80 12 -5 3 188.58 9.60 12 5 -3 178.48 9.00 -12 -5 3 165.68 10.20 12 5 3 191.28 8.60 12 -5 -3 210.88 9.20 12 -5 -3 214.38 9.50 -12 -5 3 173.28 7.40 12 5 -4 10.00 2.70 -12 5 4 13.80 4.50 12 -5 4 8.50 2.70 -12 -5 4 15.20 3.90 -12 -5 4 10.00 1.70 12 5 4 13.40 2.90 12 -5 -4 12.60 3.00 12 5 -5 9.50 2.90 -12 5 5 6.60 4.40 12 -5 5 10.50 2.90 12 5 5 10.10 2.90 12 -5 -5 17.90 3.60 -12 -5 5 14.90 4.60 12 -5 6 116.99 7.70 -12 5 6 119.09 8.00 12 5 -6 123.99 7.20 12 -5 -6 125.29 7.80 12 5 6 121.29 7.50 -12 -5 6 111.69 8.40 -12 5 7 8.10 4.00 12 -5 7 8.70 3.70 12 5 -7 1.70 2.90 12 -5 -7 9.40 3.40 12 5 7 1.90 3.10 -12 -5 7 7.20 4.50 -12 5 8 1.90 3.50 12 -5 8 4.00 4.00 12 5 -8 -1.40 2.80 12 -5 -8 0.90 3.70 12 5 8 -0.40 3.20 -12 -5 8 1.80 3.80 -12 5 9 8.40 3.90 12 -5 9 3.90 4.40 12 5 -9 0.30 3.30 -12 -5 9 3.10 4.00 12 5 9 3.20 3.90 12 -5 -9 4.50 3.80 12 5 -10 8.30 3.80 -12 5 10 18.60 4.80 12 -5 10 15.00 5.60 12 -5 -10 12.40 4.80 12 5 10 15.30 5.30 -12 -5 10 13.60 5.00 12 5 -11 2.80 4.30 12 -5 11 0.50 5.20 12 5 11 14.20 5.40 12 -5 -11 9.20 5.40 -12 -5 11 15.80 5.70 -13 -5 0 -0.50 0.80 13 5 0 -4.20 1.20 13 -5 0 -0.60 1.90 13 -5 0 -2.60 1.80 -13 -5 0 -3.50 3.60 13 5 -1 16.20 1.90 -13 -5 -1 12.60 4.40 13 -5 1 16.80 3.20 13 -5 1 16.30 3.00 13 -5 -1 18.30 3.20 -13 -5 1 20.40 1.80 -13 -5 1 19.60 5.00 13 5 1 16.50 2.40 13 -5 -1 19.40 3.10 13 -5 2 1.40 2.20 13 5 -2 0.70 2.40 -13 -5 2 2.40 1.00 13 -5 -2 2.70 2.30 13 -5 -2 7.60 2.60 -13 -5 2 0.00 3.90 13 5 2 -0.60 1.40 13 5 -3 11.80 3.10 -13 5 3 19.20 5.10 13 -5 3 17.40 3.50 13 -5 -3 19.10 3.10 13 5 3 14.90 2.70 -13 -5 3 17.60 1.80 13 -5 -3 20.00 3.50 -13 -5 3 15.10 4.60 13 5 -4 2.90 2.40 -13 5 4 4.90 4.50 13 -5 4 6.70 3.10 13 -5 -4 10.30 3.00 -13 -5 4 2.10 3.90 -13 -5 4 0.80 1.40 13 5 4 0.20 2.20 13 -5 5 25.10 4.00 13 5 -5 21.50 3.80 -13 5 5 24.60 5.60 13 -5 -5 16.60 3.80 13 5 5 16.50 3.50 -13 -5 5 23.90 5.30 13 5 -6 1.20 2.80 13 -5 6 4.20 2.80 -13 5 6 6.90 3.90 13 5 6 2.70 2.80 -13 -5 6 5.00 4.00 13 -5 -6 3.20 3.00 13 -5 7 17.20 4.40 13 5 -7 10.00 3.30 -13 5 7 11.50 4.20 -13 -5 7 16.30 5.00 13 -5 -7 11.00 4.00 13 5 7 10.60 3.60 13 -5 8 6.20 4.00 -13 5 8 0.40 3.50 13 5 -8 -1.40 3.00 13 5 8 -2.10 3.20 13 -5 -8 1.60 3.50 -13 -5 8 4.00 3.90 13 5 -9 22.50 4.70 -13 5 9 33.10 5.50 13 -5 9 33.10 6.40 13 -5 -9 25.10 5.40 13 5 9 31.90 5.50 -13 -5 9 36.30 6.40 13 -5 10 15.70 5.60 13 5 -10 10.30 4.10 13 -5 -10 14.80 5.40 -13 -5 10 20.30 5.80 13 5 10 9.30 4.80 14 -5 0 10.70 2.90 14 -5 0 7.90 2.60 14 5 0 5.40 1.70 -14 -5 0 8.40 4.40 14 -5 1 45.60 4.60 14 -5 1 42.80 4.50 -14 -5 -1 40.70 6.40 14 5 -1 41.00 2.90 14 -5 -1 39.70 4.50 14 -5 -1 36.20 4.20 -14 -5 1 44.20 6.50 -14 -5 1 39.50 2.60 14 5 1 40.80 3.50 14 -5 2 165.88 8.70 14 5 -2 149.79 8.30 -14 -5 2 162.38 10.30 14 -5 -2 157.18 8.40 -14 -5 2 147.39 6.30 14 -5 -2 160.38 8.30 14 5 2 159.88 7.50 -14 5 3 -2.00 4.40 14 5 -3 -3.20 2.20 14 -5 3 -1.40 2.60 -14 -5 3 3.60 4.30 14 -5 -3 0.60 2.50 -14 -5 3 0.00 1.10 14 5 3 -3.80 2.00 14 -5 -3 -1.00 2.40 14 5 -4 4.40 2.60 -14 5 4 10.40 4.90 14 -5 4 3.80 3.00 14 -5 -4 6.20 2.90 -14 -5 4 2.60 4.30 14 5 4 -1.70 2.20 14 -5 5 100.19 7.70 -14 5 5 112.19 8.50 14 5 -5 94.29 6.80 -14 -5 5 106.69 8.50 14 -5 -5 115.59 7.40 14 5 5 104.89 7.30 14 -5 6 1.00 3.10 14 5 -6 -0.60 3.00 -14 5 6 -0.50 3.60 14 5 6 0.70 2.80 -14 -5 6 7.50 4.30 14 -5 -6 2.40 3.20 14 -5 7 161.18 10.30 -14 5 7 160.88 9.80 14 5 -7 152.18 9.10 -14 -5 7 150.58 10.30 14 -5 -7 147.79 9.40 14 5 7 132.09 9.20 14 -5 8 21.10 5.20 -14 5 8 14.10 4.30 14 5 -8 2.10 3.20 14 5 8 3.10 3.60 -14 -5 8 13.30 5.60 14 -5 -8 10.00 4.10 -14 5 9 63.99 7.90 14 -5 9 50.49 7.30 14 5 -9 50.89 6.50 14 5 9 56.29 7.30 14 -5 -9 61.99 7.70 -14 -5 9 51.29 7.60 14 5 -10 2.80 4.30 14 -5 10 11.30 5.10 -14 5 10 17.70 4.90 14 -5 -10 -0.30 4.20 -14 -5 10 5.80 4.60 14 5 10 2.20 5.00 15 -5 0 0.40 2.30 15 5 0 -0.90 1.40 15 -5 0 -2.40 2.10 -15 -5 0 -4.10 4.00 -15 -5 -1 2.60 4.60 15 5 -1 4.30 1.60 15 -5 1 10.00 2.90 15 -5 1 5.90 3.10 15 5 1 8.70 2.20 15 -5 -1 6.70 2.70 -15 -5 1 5.10 4.70 15 -5 -1 11.80 3.20 -15 -5 1 4.70 1.20 15 5 -2 112.19 7.30 15 -5 2 128.29 7.80 15 -5 -2 124.89 7.60 15 5 2 129.49 6.80 15 -5 -2 144.39 7.70 -15 -5 2 116.89 9.30 15 -5 3 86.59 6.70 -15 5 3 90.99 8.60 15 5 -3 85.69 6.30 15 -5 -3 105.29 6.50 -15 -5 3 78.39 7.90 15 -5 -3 94.59 6.50 15 5 3 77.69 5.80 15 5 -4 125.79 8.00 -15 5 4 151.38 10.20 15 -5 4 150.68 8.90 15 5 4 135.59 7.80 -15 -5 4 123.79 9.10 15 -5 -4 151.58 8.50 -15 5 5 140.49 9.80 15 -5 5 125.09 8.90 15 5 -5 143.59 8.60 -15 -5 5 118.09 9.30 15 -5 -5 148.29 8.70 15 5 5 136.69 8.40 15 -5 6 4.10 3.80 15 5 -6 9.30 3.70 -15 5 6 7.90 5.10 15 5 6 10.50 3.60 15 -5 -6 10.30 3.90 -15 -5 6 12.60 4.90 -15 5 7 0.30 3.90 15 -5 7 3.20 3.80 15 5 -7 7.10 3.30 15 5 7 5.90 3.60 15 -5 -7 4.90 3.60 -15 -5 7 6.70 5.10 15 5 -8 30.50 5.10 15 -5 8 31.00 6.10 -15 5 8 46.20 6.90 15 -5 -8 30.70 5.70 15 5 8 24.30 5.30 -15 -5 8 40.10 6.90 15 5 -9 10.40 4.00 -15 5 9 7.80 4.30 15 -5 9 2.10 4.90 -15 -5 9 14.80 5.30 15 5 9 10.10 4.70 15 -5 -9 6.10 4.40 15 5 -10 3.80 4.00 -15 5 10 16.40 5.00 15 -5 10 8.90 5.90 15 5 10 7.90 5.10 -15 -5 10 18.10 5.80 15 -5 -10 7.70 4.90 16 5 0 2.50 1.80 -16 -5 0 4.70 5.00 16 -5 0 10.60 3.20 16 5 -1 95.19 6.70 16 5 -1 92.89 5.00 -16 -5 -1 106.29 10.40 16 -5 1 100.69 6.80 16 -5 1 94.59 6.60 16 5 1 92.19 5.50 16 -5 -1 89.19 6.40 16 -5 -1 99.39 6.70 -16 -5 1 89.29 8.70 16 5 -2 12.60 3.40 16 -5 2 16.70 3.80 16 5 -2 9.80 1.90 16 -5 -2 16.50 3.60 16 -5 -2 18.60 3.40 -16 -5 2 11.00 5.40 16 5 2 10.50 2.80 -16 5 3 4.40 5.00 16 -5 3 7.90 3.30 16 5 -3 11.60 3.50 -16 -5 3 8.10 5.10 16 -5 -3 12.10 3.50 16 5 3 7.00 2.80 16 -5 -3 5.60 3.00 -16 5 4 2.50 5.00 16 -5 4 5.50 3.40 16 5 -4 5.50 3.10 16 -5 -4 7.60 3.30 -16 -5 4 6.90 4.80 16 5 4 8.30 3.20 16 -5 5 1.30 3.50 -16 5 5 -1.90 5.10 16 5 -5 0.30 2.90 16 5 5 4.20 3.00 16 -5 -5 4.00 3.40 -16 -5 5 1.60 4.30 -16 5 6 47.10 7.10 16 5 -6 37.30 5.10 16 -5 6 40.10 6.00 16 5 6 37.70 5.20 16 -5 -6 37.80 5.60 -16 -5 6 39.70 6.90 16 -5 7 15.40 5.00 -16 5 7 25.20 5.90 16 5 -7 11.60 4.10 16 5 7 10.70 4.00 16 -5 -7 9.70 4.20 -16 -5 7 21.50 6.30 16 5 -8 74.49 7.80 16 -5 8 95.09 9.50 -16 5 8 97.29 8.80 16 -5 -8 79.69 8.30 -16 -5 8 91.49 8.80 16 5 8 88.59 8.50 -16 5 9 10.60 4.50 16 -5 9 5.90 5.00 16 5 -9 0.30 3.60 16 5 9 2.10 4.40 16 -5 -9 2.60 4.40 -16 -5 9 5.30 4.70 17 -5 0 -0.80 2.90 -17 -5 0 1.10 4.80 17 5 0 -3.70 1.70 17 -5 0 -1.30 2.60 17 5 -1 2.90 3.00 17 -5 1 4.60 3.00 17 -5 1 2.30 3.10 -17 -5 -1 6.50 5.20 17 5 -1 -1.20 1.60 17 -5 -1 2.90 2.90 -17 -5 1 3.30 4.80 17 -5 -1 0.60 2.60 17 5 1 -2.00 2.00 17 5 -2 122.59 7.90 17 -5 2 133.29 8.30 17 -5 2 114.19 7.80 17 5 -2 114.49 5.80 17 -5 -2 134.79 7.70 17 5 2 117.59 6.90 -17 -5 2 125.99 10.00 17 -5 -2 140.79 8.30 17 -5 3 20.90 4.60 -17 5 3 23.00 6.50 17 5 -3 13.50 3.70 17 -5 -3 16.10 3.60 17 -5 -3 12.10 3.70 -17 -5 3 12.80 5.40 17 5 3 13.40 3.20 17 -5 4 1.50 3.20 -17 5 4 3.00 5.00 17 5 -4 3.20 3.00 -17 -5 4 5.50 4.70 17 -5 -4 -1.10 3.10 17 5 4 4.50 3.00 -17 5 5 15.40 6.30 17 5 -5 7.00 3.50 17 -5 5 14.40 4.30 17 5 5 8.90 3.40 17 -5 -5 14.90 4.00 -17 -5 5 11.40 5.30 17 5 -6 46.90 5.90 -17 5 6 61.49 8.60 17 -5 6 56.89 7.10 17 5 6 53.09 6.10 17 -5 -6 57.69 6.70 -17 -5 6 54.69 8.10 -17 5 7 19.50 5.80 17 5 -7 6.30 4.20 17 -5 7 9.10 4.80 -17 -5 7 14.90 5.70 17 5 7 9.60 4.10 17 -5 -7 11.90 5.20 17 5 -8 -4.50 3.20 -17 5 8 4.70 4.40 17 -5 8 -0.30 4.40 17 5 8 2.60 3.90 -17 -5 8 1.20 4.60 17 -5 -8 1.40 3.90 17 5 -9 3.70 3.80 -17 5 9 11.20 4.80 17 -5 9 1.70 4.70 17 -5 -9 -1.70 4.10 17 5 9 1.90 4.40 -17 -5 9 11.20 5.40 18 5 0 50.99 4.40 -18 -5 0 50.69 8.20 18 5 -1 6.80 3.60 -18 -5 -1 6.90 5.60 18 -5 1 6.70 3.30 18 -5 1 9.30 3.50 18 5 -1 10.60 2.30 -18 -5 1 10.20 5.60 18 -5 -1 12.60 3.50 18 -5 -1 16.30 4.00 18 5 1 8.30 2.70 -18 5 2 120.89 10.10 -18 -5 -2 80.49 9.60 18 5 -2 83.79 7.00 18 -5 2 100.49 7.50 18 -5 2 103.99 7.70 -18 -5 2 83.19 9.90 18 -5 -2 106.39 7.50 18 -5 -2 125.29 7.50 18 5 2 82.89 6.00 18 5 -3 14.30 4.00 -18 5 3 8.40 6.10 18 -5 3 8.50 3.70 18 -5 -3 11.00 3.50 18 5 3 14.10 3.40 -18 -5 3 12.10 5.40 18 -5 -3 9.20 3.70 -18 5 4 117.29 10.40 18 5 -4 107.09 8.00 18 -5 4 116.59 9.10 -18 -5 4 118.09 10.10 18 -5 -4 128.79 8.50 18 5 4 122.49 7.60 -18 5 5 53.99 8.80 18 -5 5 40.60 6.00 18 5 -5 46.10 5.80 18 5 5 48.50 5.60 -18 -5 5 40.20 7.40 18 -5 -5 43.80 6.00 -18 5 6 16.90 6.10 18 5 -6 1.60 3.50 18 -5 6 5.40 4.10 18 5 6 6.10 3.80 -18 -5 6 14.40 5.50 18 -5 -6 3.80 4.00 18 5 -7 67.79 7.40 -18 5 7 97.09 10.40 18 -5 7 78.69 8.80 18 5 7 86.89 8.20 -18 -5 7 97.99 10.50 18 -5 -7 70.99 8.20 18 5 -8 47.90 6.50 18 -5 8 48.90 7.40 -18 5 8 65.79 8.70 18 -5 -8 43.10 6.80 -18 -5 8 53.19 8.40 18 5 8 37.40 6.60 18 5 -9 30.30 5.80 -18 5 9 35.50 6.80 18 -5 9 44.10 7.60 -18 -5 9 28.70 6.70 18 5 9 24.00 6.30 18 -5 -9 28.00 6.20 -19 -5 0 -2.90 5.20 19 -5 0 -3.70 2.50 19 5 0 -5.00 1.90 19 -5 0 -0.10 2.90 19 -5 1 1.80 3.30 19 5 -1 4.70 3.30 -19 -5 -1 -1.80 5.20 19 -5 1 2.70 3.50 -19 -5 1 4.70 5.50 19 -5 -1 11.50 3.50 19 -5 -1 -1.50 3.00 19 5 1 1.10 2.40 19 -5 2 34.50 5.10 19 -5 2 25.40 4.70 -19 -5 -2 20.30 6.60 19 5 -2 27.50 4.90 -19 5 2 39.20 8.00 19 -5 -2 29.90 4.60 -19 -5 2 35.20 7.50 19 -5 -2 40.90 5.60 19 5 2 29.80 4.10 -19 5 3 83.59 10.40 19 5 -3 73.09 7.30 19 -5 3 81.59 7.50 19 5 3 72.09 6.40 19 -5 -3 77.09 7.60 -19 -5 3 75.79 9.40 19 -5 -3 70.59 6.20 19 -5 4 0.40 4.00 19 5 -4 -3.30 2.90 -19 5 4 0.40 5.40 19 -5 -4 1.10 3.70 -19 -5 4 6.00 5.60 19 5 4 1.10 2.60 19 5 -5 48.50 6.20 19 -5 5 46.00 6.50 -19 5 5 51.39 8.40 19 -5 -5 54.09 6.70 -19 -5 5 59.29 9.20 19 5 5 45.40 5.70 19 5 -6 37.20 6.10 -19 5 6 49.50 7.90 19 -5 6 33.60 6.50 19 5 6 31.70 5.40 -19 -5 6 42.70 7.70 19 -5 -6 33.90 6.00 19 5 -7 27.10 5.70 -19 5 7 29.30 6.60 19 -5 7 21.40 5.90 19 5 7 21.70 5.10 -19 -5 7 30.00 7.30 19 -5 -7 22.00 5.60 19 5 -8 0.60 4.30 19 -5 8 5.00 5.10 -19 5 8 13.70 5.30 -19 -5 8 4.90 5.20 19 -5 -8 1.20 4.30 19 5 8 1.40 4.10 20 -5 0 34.00 5.30 20 -5 0 30.40 4.80 -20 -5 0 46.30 8.90 20 -5 1 5.10 3.60 -20 -5 -1 0.90 5.60 20 5 -1 1.30 3.30 20 -5 1 4.90 3.30 -20 -5 1 -2.30 5.30 20 -5 -1 2.20 3.50 20 -5 -1 2.50 3.00 20 5 1 -1.80 2.10 -20 -5 -2 85.99 10.50 20 -5 2 73.99 7.60 20 -5 2 79.49 7.60 20 5 -2 74.49 7.60 -20 5 2 91.99 11.30 20 -5 -2 82.39 7.90 20 5 2 77.79 6.30 20 -5 -2 84.79 7.10 -20 -5 2 87.59 10.50 20 -5 3 80.19 7.80 20 5 -3 83.69 7.90 -20 5 3 78.79 10.50 20 -5 3 82.79 7.20 -20 -5 3 85.09 10.50 20 -5 -3 79.29 7.90 20 -5 -3 89.49 7.10 20 5 3 67.29 6.40 -20 5 4 26.60 8.10 20 -5 4 18.90 5.30 20 5 -4 15.50 4.50 -20 -5 4 26.10 7.00 20 5 4 15.80 3.90 20 -5 -4 28.00 5.20 20 5 -5 75.29 7.60 20 -5 5 65.79 7.60 -20 5 5 67.39 9.70 -20 -5 5 78.49 9.90 20 -5 -5 68.79 7.60 20 5 5 74.79 7.30 -20 5 6 9.20 6.40 20 -5 6 -1.70 4.60 20 5 -6 3.60 4.30 20 -5 -6 2.60 4.10 -20 -5 6 6.00 5.00 20 5 6 1.10 4.00 20 -5 7 4.50 4.70 -20 5 7 11.00 5.60 20 5 -7 8.60 4.10 20 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3.50 4.10 21 -5 -7 0.90 4.30 -21 -5 7 10.30 5.60 22 5 0 39.80 6.30 -22 -5 0 54.19 9.40 22 -5 0 66.29 6.70 22 -5 0 73.39 7.50 22 5 -1 -2.00 3.30 22 -5 1 -0.90 3.20 -22 -5 -1 4.80 6.20 22 -5 1 1.40 3.70 -22 5 1 7.40 7.10 -22 -5 1 -7.70 5.20 22 -5 -1 6.90 4.30 22 -5 -1 6.30 3.80 22 5 -2 40.20 6.10 -22 5 2 53.79 9.90 -22 -5 -2 56.19 10.00 22 -5 2 44.60 6.20 22 -5 2 42.00 6.10 22 -5 -2 33.70 5.90 -22 -5 2 55.49 9.40 22 -5 -2 36.90 5.30 22 -5 3 -0.80 3.40 -22 -5 -3 -4.30 5.50 -22 5 3 2.10 6.70 22 -5 3 8.90 4.30 22 5 -3 -2.40 4.10 22 -5 -3 2.80 4.00 22 -5 -3 1.70 3.30 -22 -5 3 1.30 5.70 22 -5 4 -0.10 4.40 22 5 -4 2.40 3.80 -22 5 4 7.10 6.80 22 -5 4 8.60 4.20 22 5 4 7.70 3.60 -22 -5 4 9.50 6.30 22 -5 -4 2.00 4.40 22 5 -5 -4.70 3.40 -22 5 5 10.10 6.30 22 -5 5 3.20 5.00 22 5 5 -2.50 3.50 22 -5 -5 1.40 4.30 -22 -5 5 3.20 5.80 -22 5 6 19.40 7.20 22 5 -6 7.10 4.90 22 -5 6 8.60 5.50 -22 -5 6 18.20 6.80 22 -5 -6 14.30 5.20 22 5 6 9.30 4.30 23 -5 0 -2.20 4.00 -23 -5 0 -0.10 6.30 23 -5 0 -1.80 3.80 23 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1 -0.60 0.90 0 6 1 0.10 0.80 0 6 -1 -0.30 1.00 0 -6 -1 -0.20 1.00 0 6 -1 -0.20 0.80 0 -6 -1 -0.70 0.60 0 6 1 0.10 0.50 0 -6 1 -0.80 1.00 0 6 2 382.76 14.20 0 -6 2 371.96 14.10 0 -6 -2 389.16 14.40 0 6 -2 381.16 14.50 0 -6 2 385.16 14.50 0 6 -2 396.06 14.00 0 6 -3 1.20 0.70 0 -6 3 1.10 0.60 0 6 -3 3.40 1.00 0 6 3 2.40 0.40 0 6 -3 1.90 1.80 0 -6 -3 1.40 1.50 0 -6 3 2.30 1.10 0 -6 3 0.00 1.40 0 6 -4 1347.07 48.00 0 -6 4 1355.96 49.30 0 6 4 1361.86 47.80 0 -6 4 1441.06 48.80 0 -6 4 1447.86 48.00 0 -6 -4 1417.06 48.00 0 -6 -4 1358.56 49.20 0 6 -4 1353.66 50.29 0 -6 5 3.20 1.60 0 6 -5 -2.50 2.40 0 -6 5 -0.20 1.80 0 6 -5 -0.80 1.30 0 -6 5 -0.10 1.00 0 6 5 1.50 1.00 0 -6 -5 3.20 1.40 0 6 -6 122.49 8.70 0 -6 6 131.89 7.50 0 -6 -6 144.49 6.30 0 -6 6 147.79 7.00 0 6 -6 139.89 6.60 0 -6 -6 139.29 7.60 0 6 6 141.19 6.00 0 6 -7 2.10 2.00 0 -6 7 2.90 2.80 0 -6 -7 5.40 2.80 0 6 -7 3.00 3.70 0 6 7 2.50 1.70 0 -6 7 5.50 2.30 0 -6 -8 744.73 29.60 0 6 -8 727.83 30.70 0 6 8 762.62 27.50 0 6 -8 741.43 28.10 0 -6 8 770.52 28.60 0 -6 8 739.93 29.30 0 -6 9 5.30 3.40 0 6 -9 8.90 3.20 0 -6 -9 1.40 3.70 0 6 -9 -1.60 3.90 0 6 9 -0.90 2.30 0 -6 9 2.00 2.80 0 -6 10 28.10 5.70 0 -6 10 18.30 4.10 0 6 -10 23.00 4.40 0 -6 -10 21.40 5.60 0 -6 11 -2.00 3.40 0 -6 -11 -3.70 4.20 0 -6 11 -0.90 4.30 0 -6 -12 7.20 5.30 0 -6 12 13.00 5.60 0 -6 12 8.90 4.50 1 6 0 0.70 0.80 -1 -6 0 -0.30 0.80 -1 6 0 -0.10 0.80 -1 6 0 0.40 0.60 1 6 0 -1.60 0.70 1 -6 0 -0.10 1.00 -1 -6 0 -1.40 0.80 1 6 0 -2.00 0.80 1 -6 0 0.00 0.60 -1 6 0 -0.30 0.90 1 -6 0 -1.10 0.80 1 -6 1 429.36 15.90 1 -6 1 438.96 15.10 1 6 -1 434.56 16.00 -1 6 1 433.96 15.60 -1 -6 -1 430.76 15.20 1 6 -1 449.56 15.50 1 -6 1 434.96 16.00 -1 6 1 428.36 15.90 -1 -6 -1 439.46 15.90 -1 6 1 441.56 15.40 -1 6 -1 437.36 15.80 -1 -6 1 433.46 15.60 -1 6 -1 442.06 15.10 1 6 1 424.16 15.80 1 6 1 436.26 15.30 1 6 1 456.95 15.80 -1 6 -1 445.56 16.00 -1 6 -1 429.16 16.70 1 -6 -1 418.96 15.90 1 -6 -1 445.46 15.70 -1 -6 1 414.86 15.90 1 6 -2 36.30 2.60 1 6 -2 32.10 1.50 -1 -6 -2 34.20 2.60 -1 6 2 32.30 2.60 1 -6 2 37.80 2.50 1 -6 2 35.60 2.40 -1 6 2 36.40 2.40 1 6 -2 33.00 1.90 1 6 2 32.80 2.40 -1 -6 2 33.20 2.20 1 -6 -2 30.00 2.40 -1 6 -2 23.20 2.20 -1 6 -2 33.10 3.40 -1 6 -2 35.80 2.20 -1 -6 2 33.00 2.50 1 6 -3 390.36 14.10 1 -6 3 384.46 15.30 -1 -6 -3 402.26 15.30 1 -6 3 392.66 15.00 1 6 -3 420.36 14.60 -1 6 3 394.16 14.10 1 -6 3 402.26 14.00 -1 -6 3 389.06 15.40 1 -6 -3 389.26 15.20 -1 6 -3 399.76 16.30 -1 6 -3 416.46 14.80 -1 -6 3 398.36 14.10 -1 -6 3 410.96 14.80 1 -6 4 91.59 4.70 1 6 -4 81.29 5.70 -1 6 4 85.99 3.60 1 -6 4 80.99 4.90 1 6 -4 90.59 3.80 1 -6 4 89.19 3.70 -1 -6 -4 86.89 5.00 -1 -6 -4 81.99 3.50 -1 -6 4 85.49 3.70 -1 6 -4 74.59 5.90 -1 -6 4 85.59 5.00 -1 6 -4 76.29 3.90 1 -6 -4 74.09 4.00 -1 -6 4 86.09 4.30 1 -6 -4 86.09 4.90 1 6 -5 97.99 7.00 1 -6 5 89.09 5.10 -1 6 5 94.49 4.20 -1 -6 -5 91.79 5.70 -1 -6 -5 95.99 4.30 1 6 -5 88.59 4.50 1 -6 5 89.09 5.60 1 -6 5 101.49 4.40 1 6 5 87.39 4.60 -1 6 -5 103.09 7.40 -1 6 -5 85.59 4.60 -1 -6 5 96.29 5.70 -1 -6 5 92.29 4.90 1 -6 -5 96.09 4.70 1 -6 -5 99.49 5.70 1 6 5 93.89 4.10 -1 -6 5 92.39 4.30 1 6 -6 10.90 3.70 -1 -6 -6 22.50 2.40 -1 6 6 19.50 2.20 -1 -6 -6 14.60 3.20 1 -6 6 18.10 2.80 1 6 -6 17.90 2.50 1 -6 6 12.10 3.10 1 -6 -6 23.20 2.90 -1 -6 6 20.00 2.70 1 6 6 17.70 2.20 1 -6 -6 18.20 3.30 -1 -6 6 18.00 3.50 -1 6 -6 14.90 2.60 1 6 6 20.90 2.30 -1 6 -6 9.30 4.10 1 -6 7 -2.70 2.50 -1 6 7 1.80 1.60 1 6 -7 -2.20 3.10 1 -6 7 1.60 2.10 1 6 -7 1.40 2.00 -1 -6 -7 2.60 2.70 -1 6 -7 1.80 3.40 -1 6 -7 -1.00 1.90 1 6 7 1.40 1.60 -1 -6 7 -0.10 1.90 -1 -6 7 -1.70 2.80 1 -6 -7 2.20 2.50 1 -6 8 49.60 6.00 1 -6 8 45.00 4.90 1 6 -8 44.00 6.40 -1 6 8 49.80 3.80 1 6 -8 45.40 4.60 -1 -6 -8 45.30 5.80 -1 -6 8 44.50 4.90 -1 -6 8 48.80 6.00 1 -6 -8 44.80 5.50 -1 6 -8 36.60 6.50 -1 6 -8 50.09 4.80 1 6 8 42.50 3.90 1 -6 9 41.70 6.10 1 6 -9 32.70 4.40 -1 6 9 34.50 4.10 -1 -6 -9 35.50 5.60 1 -6 9 25.50 4.30 1 6 -9 38.50 6.40 1 6 9 43.10 4.40 -1 -6 9 35.50 4.60 -1 -6 9 44.50 6.00 1 -6 -9 32.30 5.40 -1 -6 -10 -0.20 4.20 1 6 -10 -1.80 2.90 1 -6 10 1.80 3.20 1 -6 10 -2.40 3.20 -1 -6 10 4.50 4.10 1 -6 -10 4.00 4.50 -1 -6 10 -2.30 2.70 1 -6 11 17.00 4.70 -1 -6 -11 1.20 4.70 1 -6 11 17.90 5.60 -1 -6 11 8.30 4.00 1 -6 -11 14.80 5.90 -1 -6 11 15.30 5.40 1 -6 12 -6.40 3.50 -1 -6 -12 0.50 5.40 1 -6 12 -0.40 5.00 -1 -6 12 -2.40 3.80 1 6 12 -2.70 4.00 -1 -6 12 -4.40 3.80 1 -6 -12 5.40 5.60 -2 6 0 287.97 11.10 -2 -6 0 270.67 10.10 -2 -6 0 269.67 10.30 -2 6 0 290.37 10.50 2 6 0 272.37 10.10 -2 6 0 276.67 10.60 2 -6 0 274.77 10.70 -2 6 0 273.97 10.00 2 -6 0 278.97 10.10 2 6 0 280.17 10.40 -2 -6 -1 111.39 4.50 2 -6 1 106.59 4.20 2 -6 1 116.89 5.80 2 -6 1 119.69 5.20 2 -6 1 109.89 5.10 -2 6 1 109.39 5.10 -2 6 1 124.89 5.20 -2 6 1 112.79 4.80 2 6 -1 115.49 5.10 2 6 -1 114.59 4.40 2 6 1 115.49 5.00 -2 6 -1 114.59 5.10 2 -6 -1 112.89 4.80 -2 6 -1 116.59 6.00 2 -6 -1 104.69 5.10 -2 -6 1 106.69 5.00 -2 -6 1 112.49 4.50 -2 6 -1 116.49 5.10 2 6 1 114.99 4.60 2 6 -2 18.00 1.30 2 6 -2 23.50 2.50 -2 -6 -2 21.00 2.30 2 6 -2 20.60 1.30 2 -6 2 23.00 2.50 -2 6 2 21.80 2.10 2 -6 2 20.80 2.80 2 -6 2 19.20 2.10 -2 6 2 20.90 1.70 -2 -6 -2 18.00 1.10 -2 6 -2 22.20 3.10 -2 -6 2 19.60 2.40 -2 -6 2 20.20 1.60 -2 6 -2 19.20 1.90 2 -6 -2 20.80 2.10 2 6 2 22.30 2.20 -2 -6 -3 0.20 0.40 2 -6 3 -1.40 1.30 -2 6 3 0.00 0.90 -2 -6 -3 -1.40 1.40 2 -6 3 -0.50 0.60 2 -6 3 -0.20 1.20 2 6 -3 0.10 0.70 -2 6 -3 -2.20 1.90 -2 -6 3 -0.10 0.90 -2 -6 3 -0.50 1.20 -2 -6 3 -0.60 0.60 2 -6 -3 -1.60 1.30 2 -6 4 0.70 1.80 2 -6 4 3.70 1.00 2 6 -4 4.00 1.10 -2 -6 -4 4.70 0.90 -2 -6 -4 3.10 1.60 -2 6 4 2.70 1.10 2 -6 4 4.00 1.60 2 -6 -4 2.90 1.70 -2 -6 4 4.40 1.30 -2 -6 4 1.70 1.90 -2 6 -4 -2.20 2.20 -2 -6 4 2.90 1.00 2 -6 5 11.10 2.20 -2 -6 -5 13.30 2.90 2 -6 5 11.00 1.60 2 6 -5 11.60 2.90 2 6 -5 11.50 1.80 -2 6 5 14.10 1.80 2 -6 5 12.70 2.80 -2 -6 -5 14.20 1.70 2 -6 -5 12.30 2.30 -2 -6 5 13.10 1.90 -2 -6 5 13.40 1.70 2 -6 -5 12.10 2.50 -2 6 -5 12.80 3.40 -2 -6 5 11.20 2.70 -2 -6 -6 146.99 8.00 2 -6 6 139.19 7.80 2 6 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8 -6 4 86.09 5.70 -8 6 4 89.49 6.10 -8 -6 4 89.39 4.20 8 6 4 92.59 5.00 -8 -6 4 84.99 6.00 8 -6 -4 93.09 5.50 8 6 -5 33.70 3.50 -8 6 5 41.80 4.70 8 -6 5 46.90 4.60 8 -6 -5 50.49 4.70 -8 -6 5 40.90 5.20 8 6 5 44.20 3.80 8 -6 6 2.30 2.80 8 6 -6 11.10 2.60 -8 6 6 5.10 2.70 8 6 6 7.00 2.60 8 -6 -6 3.90 2.70 -8 -6 6 3.50 3.20 8 6 -7 44.90 4.50 -8 6 7 49.60 5.30 8 -6 7 46.30 5.40 -8 -6 7 42.60 3.80 8 -6 -7 50.69 5.50 -8 -6 7 47.20 6.00 8 6 7 48.70 5.00 8 6 -8 14.30 3.20 -8 6 8 15.90 3.60 8 -6 8 16.60 4.20 8 -6 -8 11.40 3.70 8 6 8 16.00 3.80 -8 -6 8 13.30 2.80 -8 -6 8 11.30 4.50 8 -6 9 32.00 5.40 8 6 -9 21.60 5.30 -8 6 9 33.60 4.70 8 6 -9 31.70 4.50 -8 -6 9 28.30 4.00 8 -6 -9 32.60 5.30 -8 -6 9 32.40 5.60 8 6 9 25.80 4.80 8 6 -10 10.70 4.00 8 -6 10 21.10 5.30 -8 -6 10 17.70 3.90 8 -6 -10 15.70 4.80 -8 -6 10 12.30 5.10 8 6 10 21.80 5.20 8 -6 11 1.10 4.50 -8 -6 11 8.90 4.90 8 6 11 0.40 4.20 -8 -6 11 1.10 5.10 8 -6 -11 3.00 4.50 9 6 0 -0.50 0.80 9 -6 0 -0.40 1.70 -9 -6 0 -0.80 2.70 9 -6 0 0.80 1.40 -9 -6 -1 2.00 2.70 9 6 -1 -0.80 0.50 9 -6 1 1.00 1.50 9 -6 1 0.70 1.90 9 -6 -1 0.80 1.60 9 6 1 -0.20 1.00 9 -6 -1 3.30 1.80 -9 -6 1 0.00 2.60 9 -6 2 81.59 5.20 9 6 -2 75.49 4.70 -9 -6 2 70.39 2.70 9 6 2 75.49 4.00 9 -6 -2 79.49 4.70 9 -6 -2 75.89 4.90 -9 -6 2 72.89 5.60 9 -6 3 16.80 2.70 -9 6 3 17.10 3.60 9 6 -3 16.40 2.50 9 -6 -3 18.40 2.80 -9 -6 3 15.60 3.40 9 -6 -3 16.40 2.70 -9 -6 3 16.00 1.40 9 6 3 16.20 2.30 -9 6 4 91.29 6.20 9 -6 4 90.29 5.90 9 6 -4 84.99 5.10 9 6 4 91.89 5.00 9 -6 -4 86.09 5.40 -9 -6 4 79.99 4.00 -9 -6 4 86.49 6.20 9 6 -5 96.69 5.60 -9 6 5 83.59 6.10 9 -6 5 82.79 5.90 9 -6 -5 102.99 6.20 -9 -6 5 104.19 6.90 9 6 5 94.69 5.70 -9 6 6 60.59 5.50 9 -6 6 57.29 5.70 9 6 -6 58.59 4.80 9 -6 -6 71.89 5.50 9 6 6 64.89 5.10 -9 -6 6 59.49 6.00 -9 6 7 23.90 4.00 9 -6 7 18.00 4.20 9 6 -7 21.10 3.60 9 -6 -7 20.50 4.10 -9 -6 7 22.50 4.70 9 6 7 20.20 3.50 9 6 -8 5.90 2.70 9 -6 8 5.80 3.00 -9 6 8 6.60 3.40 -9 -6 8 4.80 3.60 9 -6 -8 5.00 3.40 9 6 8 -2.40 2.90 -9 -6 8 -0.20 2.00 9 6 -9 -1.70 2.70 -9 6 9 2.40 3.10 9 -6 9 3.30 3.80 9 6 -9 -4.00 3.80 -9 -6 9 2.70 3.50 9 -6 -9 1.50 3.90 9 6 9 -1.20 3.10 -9 -6 9 -2.00 2.50 9 6 -10 29.90 4.90 9 -6 10 30.60 6.10 -9 -6 10 24.00 5.50 9 -6 -10 29.40 5.90 9 6 10 26.90 5.70 -9 -6 10 27.00 4.40 9 -6 11 -0.10 4.60 9 6 11 2.50 4.60 -9 -6 11 7.20 4.90 9 -6 -11 2.10 4.70 10 6 0 9.10 1.30 10 -6 0 9.30 2.40 10 -6 0 8.30 2.10 -10 -6 0 10.20 3.40 -10 -6 -1 254.97 12.20 10 -6 1 272.67 11.60 10 -6 1 280.37 11.20 10 6 -1 254.17 9.60 10 -6 -1 288.17 11.60 10 -6 -1 270.97 11.30 10 6 1 256.97 10.20 -10 -6 1 259.87 12.30 10 6 -2 31.20 3.40 10 -6 2 36.40 3.80 -10 -6 2 31.80 4.80 10 6 2 31.10 2.60 10 -6 -2 32.60 3.50 -10 -6 2 28.90 1.40 10 -6 -2 29.40 3.40 10 6 -3 192.68 9.00 -10 6 3 182.38 10.00 10 -6 3 190.68 9.40 10 -6 -3 205.68 9.20 -10 -6 3 181.08 9.90 10 6 3 201.08 8.50 -10 -6 3 182.88 7.20 10 -6 -3 213.08 9.30 10 -6 4 4.60 2.60 -10 6 4 4.40 3.30 10 6 -4 1.60 1.80 10 -6 -4 2.50 1.90 -10 -6 4 2.30 1.20 10 6 4 2.40 1.90 -10 -6 4 2.00 3.20 -10 6 5 2.40 2.90 10 -6 5 1.20 2.10 10 6 -5 2.90 2.30 -10 -6 5 1.40 3.10 -10 -6 5 -1.40 0.80 10 6 5 1.30 2.10 10 -6 -5 3.20 1.90 -10 6 6 99.19 7.00 10 -6 6 126.19 7.90 10 6 -6 104.09 6.30 -10 -6 6 113.99 8.40 10 6 6 107.29 6.90 10 -6 -6 121.19 7.40 10 6 -7 11.70 3.00 -10 6 7 10.10 3.80 10 -6 7 15.50 3.60 10 6 7 8.50 3.30 10 -6 -7 12.60 3.70 -10 -6 7 17.50 4.50 -10 6 8 -1.10 2.80 10 6 -8 -1.10 2.50 10 -6 8 -3.00 3.10 -10 -6 8 0.00 3.40 10 6 8 -8.50 2.70 10 -6 -8 3.90 3.30 -10 -6 8 -2.80 2.10 10 6 -9 2.10 2.70 -10 6 9 2.50 3.10 10 -6 9 5.50 4.00 -10 -6 9 -3.20 3.30 10 6 9 0.60 3.70 10 -6 -9 4.00 4.20 -10 -6 9 -3.60 2.30 10 -6 10 3.20 4.60 10 6 -10 5.40 3.80 -10 6 10 14.30 6.30 10 6 10 14.40 5.00 10 -6 -10 12.70 5.00 -10 -6 10 6.80 4.30 10 -6 11 11.10 5.40 10 -6 -11 6.80 4.90 10 6 11 4.50 4.70 -10 -6 11 6.60 4.90 -11 -6 0 -5.60 3.00 11 6 0 -1.40 0.90 11 -6 0 2.70 1.70 11 -6 0 3.10 2.00 11 -6 1 4.10 2.10 11 -6 1 1.70 2.10 -11 -6 -1 -1.40 3.50 11 6 -1 0.80 0.80 11 6 1 1.50 1.40 11 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11 6 9 -4.50 3.30 -11 -6 9 3.80 4.10 11 -6 -9 2.00 3.70 11 -6 10 5.80 4.90 -11 6 10 17.50 7.50 11 6 -10 8.20 3.60 11 6 10 4.00 4.30 11 -6 -10 -0.70 4.00 -11 -6 10 14.20 5.30 11 -6 11 6.00 5.30 11 -6 -11 -2.30 4.80 11 6 11 7.70 4.80 -11 -6 11 7.20 4.60 -12 -6 0 106.69 7.80 12 6 0 117.09 5.30 12 -6 0 133.79 7.00 12 -6 0 117.39 6.50 12 -6 1 260.67 11.80 12 -6 1 270.07 11.50 -12 -6 -1 269.17 13.20 12 6 -1 247.78 9.80 -12 -6 1 262.37 9.60 12 -6 -1 280.37 11.80 12 -6 -1 256.27 11.50 -12 -6 1 272.67 13.10 12 6 1 266.47 10.50 12 6 -2 28.00 3.70 12 -6 2 24.60 3.70 12 -6 -2 27.80 3.50 12 6 2 31.20 3.00 -12 -6 2 27.40 1.60 12 -6 -2 28.20 3.70 -12 -6 2 32.00 5.20 12 -6 3 2.20 2.50 12 6 -3 1.50 2.30 -12 6 3 2.00 3.70 12 -6 -3 4.50 2.30 12 6 3 5.30 2.10 12 -6 -3 5.70 2.50 -12 -6 3 3.20 0.90 -12 -6 3 3.90 3.80 12 6 -4 83.39 5.70 -12 6 4 89.89 7.10 12 -6 4 71.89 6.00 -12 -6 4 81.39 3.90 -12 -6 4 72.59 6.20 12 -6 -4 86.39 5.80 12 6 4 67.39 5.20 12 -6 5 139.29 8.20 12 6 -5 128.89 7.50 -12 6 5 133.19 8.80 12 6 5 143.99 7.70 -12 -6 5 127.99 8.90 12 -6 -5 147.09 8.20 -12 6 6 8.30 3.70 12 -6 6 10.10 3.10 12 6 -6 4.70 2.80 12 -6 -6 4.30 2.90 12 6 6 4.40 2.80 -12 -6 6 6.70 4.10 12 6 -7 84.49 6.20 12 -6 7 100.59 7.90 -12 6 7 100.19 7.40 12 6 7 87.39 7.00 12 -6 -7 98.59 7.40 -12 -6 7 88.09 7.80 12 6 -8 18.50 3.80 -12 6 8 20.00 4.40 12 -6 8 25.80 5.20 -12 -6 8 20.70 5.60 12 -6 -8 15.10 4.20 12 6 8 16.40 4.30 12 6 -9 18.80 4.30 -12 6 9 21.60 4.70 12 -6 9 23.30 5.50 -12 -6 9 16.10 5.20 12 -6 -9 14.30 4.60 12 6 9 15.80 4.70 -12 6 10 16.00 6.30 12 -6 10 12.00 5.40 12 6 -10 7.90 3.80 12 -6 -10 3.70 4.70 12 6 10 6.10 4.70 -12 -6 10 10.00 4.80 12 -6 11 2.10 5.30 12 6 11 2.30 4.60 12 -6 -11 3.90 5.00 -12 -6 11 11.90 5.00 13 6 0 0.50 1.20 13 -6 0 -3.70 1.80 -13 -6 0 -2.70 3.50 13 -6 0 -1.80 1.90 13 -6 1 133.09 7.30 13 6 -1 115.89 5.20 -13 -6 -1 118.69 8.30 13 -6 1 123.39 7.00 13 6 1 113.19 5.80 13 -6 -1 129.09 7.10 -13 -6 1 117.99 8.40 -13 -6 1 120.39 4.90 13 -6 -1 130.69 7.00 13 -6 2 38.20 4.50 13 6 -2 32.70 4.00 -13 -6 2 37.00 5.90 13 6 2 40.70 3.50 -13 -6 2 32.60 1.90 13 -6 -2 37.50 4.20 13 -6 -2 32.50 3.90 -13 6 3 96.79 7.80 13 6 -3 86.99 6.20 13 -6 3 88.49 6.40 -13 -6 3 84.99 3.80 13 -6 -3 91.19 6.10 -13 -6 3 82.19 7.30 13 6 3 87.99 5.50 13 -6 -3 98.99 6.40 13 -6 4 223.18 11.30 -13 6 4 253.37 13.00 13 6 -4 211.08 10.50 13 -6 -4 239.38 11.00 -13 -6 4 212.28 12.10 13 6 4 208.08 10.10 -13 6 5 2.30 4.00 13 -6 5 5.40 2.80 13 6 -5 0.90 2.50 13 6 5 -0.50 2.50 13 -6 -5 5.70 3.00 -13 -6 5 0.70 3.90 -13 6 6 100.79 7.60 13 -6 6 100.39 7.70 13 6 -6 99.39 6.50 13 -6 -6 93.59 7.10 -13 -6 6 96.99 8.00 13 6 6 90.69 6.70 13 -6 7 -1.30 3.40 13 6 -7 5.60 3.20 -13 6 7 4.70 4.00 13 -6 -7 4.20 3.50 -13 -6 7 -2.90 3.60 13 6 7 2.10 3.20 13 6 -8 -2.80 2.80 -13 6 8 5.40 3.90 13 -6 8 6.20 4.10 13 -6 -8 -0.50 3.40 13 6 8 1.10 3.30 -13 -6 8 3.40 4.10 13 -6 9 3.30 4.60 13 6 -9 5.40 3.80 -13 6 9 15.00 4.70 -13 -6 9 5.90 4.40 13 -6 -9 2.20 4.50 13 6 9 2.80 4.00 13 6 -10 23.60 4.90 -13 6 10 42.60 9.10 13 -6 10 35.10 7.00 13 -6 -10 25.90 5.90 13 6 10 29.00 5.90 -13 -6 10 35.10 6.60 -14 -6 0 1.40 4.10 14 6 0 6.10 1.70 14 -6 0 6.00 2.60 14 -6 0 7.30 2.60 -14 -6 -1 202.38 11.90 14 -6 1 213.78 10.40 14 -6 1 222.78 10.80 14 6 -1 218.68 8.70 14 -6 -1 232.68 10.60 -14 -6 1 221.68 8.40 14 6 1 221.18 9.40 14 -6 -1 238.68 10.90 -14 -6 1 217.28 12.30 14 6 -2 15.00 3.20 14 -6 2 18.70 3.60 -14 -6 2 14.70 1.50 14 -6 -2 23.90 3.70 -14 -6 2 19.20 5.10 14 -6 -2 20.40 3.30 14 6 2 15.80 2.70 14 6 -3 170.28 9.30 -14 6 3 176.48 11.30 14 -6 3 196.08 10.10 14 6 3 190.28 9.00 -14 -6 3 170.48 11.00 14 -6 -3 197.58 9.50 -14 -6 3 186.48 7.60 14 -6 -3 197.28 9.80 -14 6 4 22.40 6.00 14 -6 4 25.10 4.40 14 6 -4 18.10 3.80 -14 -6 4 18.00 5.20 14 -6 -4 21.00 3.70 14 6 4 15.20 3.10 -14 6 5 8.20 4.30 14 -6 5 9.00 3.70 14 6 -5 9.10 3.10 14 6 5 9.60 3.00 14 -6 -5 7.90 3.20 -14 -6 5 11.00 4.70 -14 6 6 39.80 6.20 14 6 -6 33.10 4.50 14 -6 6 33.50 5.40 -14 -6 6 34.10 6.20 14 6 6 29.50 4.50 14 -6 -6 41.50 5.40 14 -6 7 50.09 6.50 14 6 -7 43.50 5.20 -14 6 7 47.50 6.50 14 -6 -7 47.00 6.10 14 6 7 37.60 5.40 -14 -6 7 51.59 7.50 14 -6 8 49.20 6.70 14 6 -8 59.49 6.30 -14 6 8 66.39 7.30 -14 -6 8 54.19 7.60 14 -6 -8 52.89 7.00 14 6 8 59.79 6.80 14 6 -9 13.50 4.30 -14 6 9 19.20 5.00 14 -6 9 18.10 5.00 14 -6 -9 10.00 4.80 -14 -6 9 10.20 5.00 14 6 9 14.30 4.70 14 6 -10 36.20 6.00 14 -6 10 47.70 7.80 14 -6 -10 41.80 6.90 -14 -6 10 39.90 7.10 14 6 10 32.80 6.50 -15 -6 0 -1.00 4.20 15 6 0 -1.80 1.50 15 -6 0 -0.20 2.30 15 -6 0 -1.70 2.30 15 -6 1 20.60 3.70 15 6 -1 19.70 2.20 15 -6 1 25.60 4.00 -15 -6 -1 16.20 6.00 -15 -6 1 22.20 2.00 15 -6 -1 23.40 3.70 15 -6 -1 22.30 3.80 -15 -6 1 19.10 5.70 15 6 1 19.50 2.80 15 -6 2 16.10 3.50 15 6 -2 18.40 3.80 -15 -6 -2 18.80 5.70 15 -6 2 23.50 4.00 15 -6 -2 20.40 3.80 -15 -6 2 14.40 5.40 15 6 2 18.20 3.10 15 -6 -2 24.60 3.90 -15 6 3 30.80 6.40 15 -6 3 27.80 4.50 15 6 -3 20.70 3.90 15 -6 -3 29.10 4.00 -15 -6 3 22.50 5.70 15 6 3 27.50 3.80 15 -6 -3 31.60 4.50 15 -6 4 0.30 3.00 -15 6 4 2.60 5.10 15 6 -4 -3.50 2.40 15 6 4 -3.20 2.40 15 -6 -4 -0.40 2.60 -15 -6 4 -4.60 3.80 15 -6 5 22.10 4.60 -15 6 5 17.40 6.00 15 6 -5 12.50 3.50 -15 -6 5 9.90 4.90 15 6 5 18.40 3.60 15 -6 -5 17.90 4.10 15 -6 6 5.30 3.80 -15 6 6 2.10 4.70 15 6 -6 2.10 2.90 15 -6 -6 0.40 3.20 -15 -6 6 2.60 4.30 15 6 6 1.50 3.00 15 6 -7 11.40 3.60 15 -6 7 9.50 4.50 -15 6 7 13.20 4.70 -15 -6 7 14.00 5.20 15 -6 -7 13.10 4.20 15 6 7 15.80 4.70 15 6 -8 -1.10 3.50 15 -6 8 1.10 4.30 -15 6 8 19.80 4.90 15 -6 -8 9.00 4.20 15 6 8 1.00 3.60 -15 -6 8 6.80 4.80 -15 6 9 15.10 5.20 15 6 -9 10.90 4.00 15 -6 9 6.90 5.20 15 -6 -9 8.20 4.70 -15 -6 9 13.00 5.30 15 6 9 9.60 4.60 15 6 -10 13.80 4.40 15 -6 10 23.60 6.60 -15 -6 10 26.50 6.70 15 -6 -10 20.50 6.20 15 6 10 11.60 5.20 16 -6 0 113.89 7.30 16 -6 0 110.69 7.30 16 6 0 109.19 5.70 -16 -6 0 105.09 9.10 16 -6 1 8.80 2.90 16 -6 1 11.70 3.40 -16 -6 -1 6.70 5.30 16 6 -1 5.00 1.70 16 -6 -1 12.30 3.10 16 6 1 2.10 2.00 16 -6 -1 7.40 3.00 -16 -6 1 7.10 5.10 16 -6 2 37.20 5.00 -16 -6 -2 41.00 6.70 16 -6 2 31.60 4.60 16 6 -2 36.20 4.80 16 6 2 31.30 3.80 -16 -6 2 39.00 6.90 16 -6 -2 30.60 4.30 16 -6 -2 36.00 4.80 -16 6 3 5.60 5.20 16 6 -3 -3.70 2.40 16 -6 3 -0.30 3.00 16 -6 -3 2.50 2.60 16 -6 -3 2.10 2.80 16 6 3 -4.20 2.10 -16 -6 3 3.70 4.50 16 -6 4 3.00 3.40 16 6 -4 0.70 2.90 -16 6 4 2.60 4.70 16 -6 -4 2.70 3.10 -16 -6 4 8.80 4.60 16 6 4 4.90 2.60 16 -6 5 15.20 4.40 -16 6 5 18.10 5.90 16 6 -5 24.20 4.30 -16 -6 5 20.40 5.60 16 6 5 24.00 4.00 16 -6 -5 20.70 4.40 16 6 -6 6.10 3.30 16 -6 6 11.10 4.50 -16 6 6 11.00 4.80 -16 -6 6 4.70 4.90 16 6 6 9.90 3.50 16 -6 -6 6.80 3.70 16 6 -7 39.70 5.50 16 -6 7 52.39 7.10 -16 6 7 59.19 7.80 -16 -6 7 44.60 7.50 16 6 7 40.60 5.70 16 -6 -7 58.09 6.70 16 6 -8 6.90 4.20 16 -6 8 9.30 5.30 -16 6 8 17.20 5.00 16 -6 -8 7.20 4.50 -16 -6 8 10.50 5.30 16 6 8 8.80 4.60 -16 6 9 28.30 6.00 16 -6 9 20.40 6.30 16 6 -9 13.00 4.80 16 6 9 19.20 5.40 16 -6 -9 13.70 5.30 -16 -6 9 28.20 6.60 17 6 0 -4.50 1.60 -17 -6 0 1.10 5.00 17 -6 0 -3.40 2.60 17 -6 0 0.80 2.80 17 6 -1 -2.10 2.60 17 -6 1 -1.90 3.10 -17 -6 -1 -3.60 4.50 17 -6 1 0.20 2.70 17 6 -1 -1.40 1.50 17 -6 -1 -2.80 2.90 17 -6 -1 -0.40 2.60 -17 -6 1 -3.10 4.30 17 6 1 -2.40 2.00 17 -6 2 34.90 4.70 17 -6 2 29.60 4.70 17 6 -2 20.50 4.10 -17 -6 -2 20.80 6.10 -17 -6 2 21.90 6.30 17 -6 -2 22.80 4.30 17 6 2 31.40 3.80 17 -6 -2 25.40 4.10 17 6 -3 11.30 3.60 17 -6 3 7.00 3.60 -17 6 3 11.40 5.90 17 -6 -3 9.60 3.30 17 6 3 8.70 2.90 17 -6 -3 15.30 4.00 -17 -6 3 7.40 5.00 17 -6 4 4.60 3.60 -17 6 4 2.80 5.10 17 6 -4 -0.30 2.90 17 -6 -4 -2.00 3.10 17 6 4 -1.30 2.80 -17 -6 4 2.50 4.60 -17 6 5 66.39 8.70 17 6 -5 53.99 6.10 17 -6 5 61.49 7.00 17 6 5 54.09 6.00 -17 -6 5 50.99 8.00 17 -6 -5 55.79 6.60 17 6 -6 7.10 3.90 -17 6 6 -0.50 5.30 17 -6 6 6.30 4.20 17 -6 -6 10.30 4.10 17 6 6 7.30 3.50 -17 -6 6 10.30 5.30 17 6 -7 -0.20 3.30 -17 6 7 3.20 4.60 17 -6 7 6.40 4.60 17 6 7 4.70 3.70 17 -6 -7 -1.70 4.20 -17 -6 7 5.60 4.80 17 6 -8 19.50 5.00 17 -6 8 17.70 6.00 -17 6 8 32.40 6.20 17 6 8 23.80 5.30 17 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4.20 20 -6 5 18.40 5.10 -20 6 5 7.50 6.20 -20 -6 5 11.10 5.80 20 -6 -5 9.80 4.30 20 6 5 6.00 3.80 -20 6 6 38.20 8.20 20 6 -6 26.30 5.40 20 -6 6 19.80 5.60 20 6 6 29.80 5.60 -20 -6 6 32.60 7.40 20 -6 -6 35.40 6.30 20 6 -7 3.00 4.00 -20 6 7 18.00 6.20 20 -6 7 5.40 4.90 20 6 7 7.40 4.70 20 -6 -7 8.60 4.90 -20 -6 7 7.40 5.50 21 6 0 0.90 3.40 21 -6 0 1.60 3.20 21 -6 0 -0.60 3.30 -21 -6 0 -5.90 5.50 21 -6 1 7.10 4.20 21 6 -1 11.20 4.60 -21 -6 -1 10.60 6.50 21 -6 1 9.10 4.00 21 -6 -1 10.80 4.20 -21 -6 1 9.30 6.20 21 -6 -1 2.60 3.70 21 6 -2 -0.30 3.40 21 -6 2 2.20 3.40 -21 6 2 12.40 7.10 21 -6 2 4.90 3.80 -21 -6 -2 2.20 6.40 -21 -6 2 3.10 6.20 21 -6 -2 4.30 3.60 21 -6 -2 2.00 3.30 -21 6 3 118.99 12.70 21 -6 3 90.79 8.70 21 6 -3 93.19 8.70 -21 -6 -3 97.29 11.50 21 -6 3 98.19 7.90 21 -6 -3 85.89 7.80 21 6 3 89.39 7.20 -21 -6 3 100.19 11.50 21 -6 -3 109.69 8.50 -21 -6 -4 -4.00 5.60 21 6 -4 -0.30 4.00 21 -6 4 0.10 4.40 21 -6 4 3.40 3.60 -21 6 4 -5.70 5.80 21 -6 -4 3.00 4.00 21 6 4 4.90 3.40 -21 -6 4 8.20 6.60 21 6 -5 2.10 3.80 -21 6 5 1.10 6.00 21 -6 5 4.20 4.50 -21 -6 5 4.40 5.60 21 -6 -5 5.80 4.30 21 6 5 -1.40 3.60 -21 6 6 -0.10 6.00 21 -6 6 8.60 4.90 21 6 -6 1.60 4.00 -21 -6 6 3.90 5.30 21 6 6 3.30 4.10 21 -6 -6 3.10 4.40 21 6 -7 4.40 4.80 -21 6 7 25.00 6.70 21 -6 7 1.70 5.00 21 -6 -7 3.70 4.80 -21 -6 7 17.50 6.20 21 6 7 2.40 3.90 22 -6 0 171.38 10.60 22 -6 0 162.48 10.60 22 6 0 142.99 10.20 -22 -6 0 163.98 12.90 -22 -6 -1 0.40 6.80 22 6 -1 -0.80 3.40 22 -6 1 -2.10 3.30 22 -6 1 1.40 3.50 22 -6 -1 -3.40 3.60 -22 -6 1 -4.00 5.80 22 -6 -1 -2.70 3.40 22 -6 2 44.40 6.30 -22 -6 -2 46.00 9.40 22 6 -2 45.40 6.40 -22 6 2 46.50 9.60 22 -6 2 49.70 6.50 22 -6 -2 32.10 5.30 22 -6 -2 38.60 6.10 -22 -6 2 40.90 8.40 -22 6 3 3.00 7.00 22 6 -3 14.80 4.60 22 -6 3 15.60 4.80 -22 -6 -3 0.70 6.10 22 -6 3 6.10 4.40 22 -6 -3 8.60 4.20 22 -6 -3 11.90 4.70 -22 -6 3 13.40 6.50 22 -6 4 4.80 4.30 22 -6 4 12.30 5.20 -22 -6 -4 2.20 6.70 -22 6 4 3.40 6.70 22 6 -4 2.50 4.00 22 -6 -4 0.30 3.90 -22 -6 4 4.30 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8.20 25 6 -2 25.40 5.80 25 -6 -2 22.40 6.40 -25 -6 2 15.10 7.50 25 -6 3 47.50 7.50 -25 6 3 44.30 10.40 -25 -6 -3 45.30 10.40 25 6 -3 41.60 6.90 25 -6 3 38.50 7.10 25 -6 -3 48.10 7.50 -25 -6 3 55.69 9.90 0 -7 0 27.80 1.90 0 7 1 118.09 5.10 0 7 -1 115.49 5.10 0 7 1 113.19 4.40 0 7 -1 116.79 4.20 0 7 1 108.89 4.80 0 -7 1 110.79 5.00 0 -7 -1 109.79 4.90 0 7 -1 119.59 4.90 0 -7 -1 115.09 4.50 0 -7 1 108.79 5.00 0 7 2 0.00 0.30 0 -7 -2 -0.60 1.10 0 -7 2 0.60 1.00 0 -7 2 -1.20 1.20 0 7 -2 -0.70 1.20 0 7 -2 0.30 0.70 0 7 2 1.20 1.30 0 7 2 -0.30 1.00 0 -7 -3 31.70 3.10 0 7 -3 34.20 1.60 0 7 -3 36.40 2.30 0 -7 3 35.20 2.70 0 -7 3 30.60 1.50 0 -7 3 33.20 3.00 0 7 -3 32.40 3.90 0 7 4 14.60 1.00 0 -7 -4 11.40 2.30 0 -7 4 8.10 1.80 0 -7 4 11.70 2.50 0 7 -5 469.65 19.60 0 -7 5 455.25 18.40 0 7 -5 474.55 17.00 0 -7 5 467.15 17.80 0 7 5 438.66 16.60 0 7 5 465.55 16.60 0 -7 -5 482.15 18.40 0 -7 5 469.95 16.70 0 -7 -5 459.45 16.80 0 7 6 7.00 1.40 0 -7 6 2.00 2.60 0 7 -6 4.20 3.50 0 7 -6 4.10 1.70 0 -7 -6 7.90 2.70 0 -7 -6 11.70 2.00 0 7 7 13.60 2.20 0 7 -7 12.90 4.10 0 -7 7 11.60 2.70 0 -7 7 10.80 3.60 0 7 -7 12.50 2.50 0 -7 -7 9.20 3.30 0 -7 -7 14.70 2.60 0 7 -8 10.90 4.50 0 -7 -8 10.70 3.70 0 -7 8 18.40 4.00 0 -7 8 11.00 3.00 0 -7 -9 2.00 3.70 0 -7 9 3.30 3.40 0 7 -9 5.50 4.40 0 7 -9 4.80 2.90 0 -7 9 2.60 3.10 0 -7 -10 4.70 4.70 0 -7 10 0.00 4.00 0 -7 10 0.10 2.90 0 -7 -11 25.20 6.10 0 -7 11 24.70 5.40 0 -7 11 26.50 6.40 0 -7 12 11.50 5.60 0 -7 12 5.80 4.20 0 -7 -12 5.20 5.20 -1 7 0 0.00 0.70 -1 -7 0 0.70 1.00 1 -7 0 -0.80 0.70 1 7 0 -0.70 0.90 1 -7 0 1.00 1.10 1 7 0 -1.10 0.70 -1 7 0 0.30 1.00 1 7 0 -1.50 0.80 1 -7 0 -0.80 0.80 -1 7 0 -0.30 0.60 -1 -7 0 -2.30 0.80 1 7 -1 146.09 6.30 1 7 -1 153.68 5.90 1 -7 1 139.59 6.30 -1 -7 -1 145.29 6.20 1 7 -1 142.99 5.50 -1 7 1 146.69 5.70 1 -7 1 144.59 6.30 -1 -7 -1 148.49 5.60 -1 7 1 144.59 6.30 -1 7 1 154.18 6.00 1 -7 1 144.39 5.30 -1 7 -1 150.08 7.20 1 7 1 149.79 6.10 1 7 1 151.08 6.10 -1 -7 1 145.59 6.30 1 -7 -1 148.59 6.00 -1 7 -1 152.18 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232.18 11.40 1 -7 -5 208.48 9.90 -1 -7 5 207.88 10.00 1 -7 -5 215.68 8.80 -1 -7 5 236.08 9.40 -1 -7 5 226.28 8.50 -1 7 -5 210.28 11.40 -1 -7 -6 2.90 1.50 1 -7 6 1.90 1.90 1 7 -6 0.00 1.50 1 7 -6 -0.30 2.70 -1 -7 -6 0.30 2.40 1 -7 6 -1.30 2.30 -1 7 6 2.80 1.30 -1 -7 6 3.10 2.60 1 7 6 3.30 1.30 1 -7 -6 3.90 2.50 1 -7 -6 1.80 2.00 1 7 6 1.70 1.30 -1 7 -6 -3.70 2.80 -1 -7 6 2.10 1.80 -1 7 -6 -0.20 1.60 -1 -7 -7 62.39 6.10 1 7 -7 51.39 4.10 1 7 -7 45.60 6.00 -1 7 7 51.09 3.40 -1 -7 -7 60.09 3.70 1 -7 7 50.39 5.10 1 -7 7 51.09 4.80 1 -7 -7 53.89 5.60 -1 7 -7 48.20 6.30 -1 7 -7 48.00 4.00 -1 -7 7 49.60 5.10 1 7 7 56.09 3.40 -1 -7 7 56.39 4.70 1 -7 8 22.20 4.60 1 -7 8 15.90 3.70 1 7 -8 20.70 3.30 -1 -7 -8 19.60 4.50 -1 7 8 21.60 2.90 1 7 -8 27.40 5.40 -1 7 -8 21.20 5.20 1 -7 -8 23.40 4.50 -1 -7 8 19.50 4.20 -1 -7 8 16.00 3.60 1 -7 9 0.50 2.80 1 7 -9 0.70 2.70 -1 7 9 -2.20 2.30 1 -7 9 -1.50 3.00 -1 -7 -9 -0.80 3.50 1 7 -9 2.60 4.20 -1 -7 9 -2.50 2.40 -1 -7 9 0.00 3.50 1 -7 -9 -1.90 3.30 -1 -7 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11 -8 -9 15.90 4.90 11 -8 10 18.80 5.40 11 8 -10 10.00 4.70 -11 -8 10 9.30 4.90 11 -8 -10 18.10 5.60 11 8 10 7.90 4.60 11 -8 11 3.20 5.40 11 8 11 0.20 4.50 11 -8 -11 2.30 5.30 -11 -8 11 14.90 5.50 12 8 0 -0.10 1.00 12 -8 0 0.30 1.80 12 -8 0 1.90 2.40 -12 -8 0 4.30 3.60 12 -8 1 111.69 6.90 12 8 -1 105.49 4.00 -12 -8 -1 107.59 8.00 12 -8 1 124.29 6.40 12 -8 -1 106.69 6.20 12 -8 -1 110.49 6.80 -12 -8 1 115.39 7.70 12 8 1 94.69 5.00 -12 -8 -2 14.70 4.10 12 -8 2 13.70 2.60 12 -8 2 16.20 3.10 12 8 -2 6.90 2.50 12 -8 -2 15.60 3.00 -12 -8 2 12.90 4.20 12 -8 -2 15.80 3.20 12 8 2 17.80 2.40 12 8 -3 7.40 2.60 12 -8 3 15.20 3.50 -12 -8 -3 16.80 4.10 12 -8 -3 15.70 3.30 -12 -8 3 12.90 4.30 12 8 3 13.10 2.40 12 -8 -3 18.00 3.20 12 -8 4 166.78 9.60 -12 8 4 180.58 10.70 12 8 -4 176.18 8.90 -12 -8 4 164.08 6.20 12 -8 -4 171.88 9.00 -12 -8 4 169.58 6.10 12 8 4 175.08 8.30 -12 -8 4 177.38 10.00 -12 8 5 34.40 5.60 12 -8 5 33.80 5.00 12 8 -5 35.60 4.50 -12 -8 5 38.40 6.20 -12 -8 5 31.80 2.30 12 -8 -5 40.80 5.00 12 8 5 36.40 4.20 -12 8 6 7.60 4.30 12 -8 6 11.40 3.50 12 8 -6 1.50 2.50 12 -8 -6 3.60 3.20 12 8 6 4.70 2.80 -12 -8 6 5.20 4.20 -12 8 7 26.80 4.90 12 -8 7 17.40 4.70 12 8 -7 18.10 3.50 -12 -8 7 16.80 5.10 12 8 7 18.60 4.10 12 -8 -7 15.00 4.30 12 -8 8 7.80 3.80 -12 8 8 21.20 4.40 12 8 -8 11.00 3.40 12 -8 -8 11.70 4.30 -12 -8 8 12.20 4.90 12 8 8 7.50 3.70 -12 8 9 5.60 3.60 12 8 -9 -3.00 2.90 12 -8 9 3.60 3.70 12 -8 -9 10.20 4.40 12 8 9 6.20 4.10 -12 -8 9 5.20 4.40 12 -8 10 13.00 5.60 12 -8 -10 11.00 5.00 12 8 10 7.50 5.00 -12 -8 10 17.10 5.50 13 8 0 -0.50 1.00 13 -8 0 1.00 1.90 13 -8 0 0.40 2.30 -13 -8 0 -3.50 3.50 -13 -8 -1 73.29 7.50 13 -8 1 75.09 5.70 13 -8 1 71.99 5.00 13 8 -1 65.49 2.80 -13 -8 1 67.49 6.50 13 -8 -1 64.39 5.00 13 -8 -1 71.49 5.50 13 8 1 62.19 3.90 13 -8 2 375.26 15.90 -13 -8 -2 379.86 17.50 13 8 -2 397.66 16.30 13 -8 2 376.16 16.70 13 -8 -2 408.66 16.40 13 8 2 408.76 15.20 -13 -8 2 376.16 17.60 13 -8 -2 392.06 16.50 13 -8 3 87.69 6.20 13 8 -3 86.59 5.90 -13 -8 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14 8 -1 28.40 1.90 14 8 1 35.10 3.10 14 -8 -1 34.20 4.50 14 -8 -1 36.70 4.30 -14 -8 1 34.40 6.00 14 -8 2 171.18 9.10 -14 -8 -2 184.08 11.10 14 8 -2 175.68 9.40 14 -8 2 173.78 9.80 14 -8 -2 189.48 9.80 14 -8 -2 183.58 9.30 -14 -8 2 159.48 10.60 14 8 2 180.38 8.20 -14 -8 -3 11.00 5.00 14 8 -3 14.00 3.70 14 -8 3 18.30 4.00 14 -8 -3 13.70 3.50 14 -8 -3 19.90 3.70 -14 -8 3 13.90 4.80 14 8 3 12.30 2.80 -14 8 4 6.70 5.30 14 -8 4 11.50 3.80 14 8 -4 6.90 3.30 14 8 4 11.10 2.90 -14 -8 4 11.40 4.90 14 -8 -4 16.80 3.70 14 8 -5 22.80 3.90 -14 8 5 20.50 5.50 14 -8 5 18.90 4.50 14 -8 -5 25.40 4.50 14 8 5 17.00 3.60 -14 -8 5 22.10 5.40 -14 8 6 62.09 7.60 14 8 -6 58.09 5.80 14 -8 6 61.59 7.00 -14 -8 6 62.59 7.90 14 8 6 57.49 5.70 14 -8 -6 57.79 6.40 -14 8 7 19.90 5.10 14 8 -7 13.20 3.50 14 -8 7 17.50 4.30 14 8 7 17.90 4.20 14 -8 -7 14.30 4.40 -14 -8 7 19.10 5.50 14 8 -8 39.70 5.30 14 -8 8 39.80 6.70 -14 8 8 46.40 6.50 14 -8 -8 37.10 6.00 -14 -8 8 48.80 7.60 14 8 8 39.40 5.80 -14 8 9 12.40 4.40 14 -8 9 1.50 4.70 14 8 -9 3.50 3.30 14 8 9 0.40 4.00 -14 -8 9 10.70 5.20 14 -8 -9 3.20 4.40 14 -8 10 23.80 6.50 14 -8 -10 12.50 5.20 14 8 10 3.90 4.70 -14 -8 10 28.90 6.90 15 -8 0 -1.70 2.20 15 8 0 -3.10 1.30 -15 -8 0 0.20 4.30 15 -8 0 -2.00 2.70 15 -8 1 75.99 6.10 -15 -8 -1 81.89 8.70 15 8 -1 72.19 3.40 15 -8 1 77.49 6.40 15 -8 -1 73.59 6.20 15 8 1 64.99 4.40 15 -8 -1 75.49 5.80 -15 -8 1 75.79 7.70 15 -8 2 2.40 3.20 15 -8 2 4.50 2.70 -15 -8 -2 -2.90 4.50 15 8 -2 7.20 2.90 15 -8 -2 9.40 3.20 15 8 2 6.90 2.20 15 -8 -2 1.70 2.70 -15 -8 2 4.60 4.70 -15 -8 -3 5.10 4.60 -15 8 3 5.30 4.80 15 -8 3 -0.70 2.40 15 -8 3 5.40 3.40 15 8 -3 5.00 2.90 15 8 3 2.20 2.10 -15 -8 3 4.50 4.40 15 -8 -3 2.40 2.70 15 -8 -3 1.20 2.80 -15 8 4 5.10 4.80 15 8 -4 5.80 3.40 15 -8 4 6.90 3.80 15 -8 -4 5.00 3.20 -15 -8 4 6.10 4.40 15 8 4 7.60 2.70 -15 8 5 4.20 4.50 15 -8 5 11.50 4.10 15 8 -5 11.00 3.30 -15 -8 5 3.90 4.20 15 8 5 6.60 2.90 15 -8 -5 0.40 3.30 15 8 -6 5.90 3.40 -15 8 6 5.90 4.30 15 -8 6 9.40 4.30 -15 -8 6 5.30 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9 -9 -2 71.59 5.30 9 9 2 68.69 3.80 9 -9 3 149.49 8.60 -9 -9 -3 165.98 8.60 9 9 -3 182.48 8.00 -9 -9 3 170.48 9.10 9 -9 -3 177.28 8.30 9 9 3 171.58 7.40 9 -9 -3 168.68 8.70 9 -9 4 8.20 2.90 -9 9 4 6.80 3.20 9 9 -4 3.50 1.90 9 -9 -4 4.10 2.30 9 9 4 6.90 2.00 -9 -9 4 4.20 0.90 -9 -9 4 4.10 1.00 9 -9 -4 4.10 1.90 -9 -9 4 4.80 3.20 -9 9 5 165.48 9.40 9 9 -5 184.28 8.50 9 -9 5 197.38 10.10 -9 -9 5 186.78 7.30 9 -9 -5 195.78 9.50 9 9 5 199.88 8.90 9 -9 -5 169.68 7.90 -9 -9 5 172.48 10.00 9 9 -6 21.40 3.20 -9 9 6 26.10 4.30 9 -9 6 23.40 4.50 -9 -9 6 23.40 4.90 9 -9 -6 31.40 4.60 -9 -9 6 21.80 2.40 9 9 6 20.70 3.30 9 -9 7 15.10 4.30 -9 9 7 31.10 4.20 9 9 -7 20.10 3.20 9 9 7 19.90 3.70 -9 -9 7 15.20 2.60 9 -9 -7 20.80 4.50 -9 -9 7 27.40 5.30 -9 9 8 95.09 6.40 9 9 -8 92.79 6.20 9 -9 8 108.29 8.40 -9 -9 8 93.69 5.90 9 9 8 101.99 7.40 -9 -9 8 95.49 8.00 9 -9 -8 103.39 7.90 9 -9 9 13.80 4.60 9 9 -9 2.00 3.00 9 -9 -9 8.80 4.20 9 9 9 4.40 3.60 -9 -9 9 16.70 5.20 9 -9 10 41.80 6.80 9 9 10 49.50 6.70 -9 -9 10 50.39 7.80 9 -9 -10 38.40 6.60 9 -9 11 7.70 5.20 9 9 11 2.60 4.60 -9 -9 11 8.50 5.50 9 -9 -11 6.80 5.60 10 -9 0 39.70 3.60 10 9 0 33.00 2.00 10 -9 0 36.30 4.10 -10 -9 0 40.80 4.80 10 -9 1 652.03 25.00 -10 -9 -1 621.04 24.90 10 -9 1 627.84 24.00 -10 -9 1 671.83 25.30 10 -9 -1 652.53 24.90 10 9 1 649.74 23.00 10 -9 -1 643.14 24.20 10 -9 2 46.80 4.90 -10 -9 -2 50.39 5.50 10 -9 2 51.69 3.90 10 -9 -2 44.90 4.30 10 -9 -2 48.10 4.70 10 9 2 51.69 3.20 -10 -9 2 54.49 5.90 10 9 -3 2.30 2.00 -10 -9 -3 7.20 3.50 10 -9 3 6.10 2.80 10 -9 -3 9.10 2.50 -10 -9 3 8.80 3.40 10 -9 -3 5.40 2.50 10 9 3 6.10 1.90 10 9 -4 131.09 6.60 10 -9 4 126.49 7.70 -10 9 4 126.19 8.20 -10 -9 4 118.89 7.80 -10 -9 4 115.79 4.50 10 9 4 119.49 6.40 -10 -9 4 117.49 4.40 10 -9 -4 113.79 6.90 -10 9 5 6.50 3.90 10 9 -5 4.50 2.40 10 -9 5 2.60 2.30 10 9 5 4.70 2.30 10 -9 -5 3.30 2.90 -10 -9 5 3.60 1.20 -10 -9 5 -1.20 3.30 -10 -9 5 1.80 2.10 10 -9 6 7.10 3.80 -10 9 6 8.40 3.90 10 9 -6 6.90 2.80 -10 -9 6 9.30 4.30 10 9 6 11.70 3.10 -10 -9 6 8.00 1.90 10 -9 -6 13.10 3.60 10 9 -7 97.19 6.20 -10 9 7 95.39 6.70 10 -9 7 111.69 8.30 -10 -9 7 100.79 8.10 10 -9 -7 98.39 7.60 -10 -9 7 101.29 5.50 10 9 7 99.59 7.00 -10 9 8 10.10 3.30 10 9 -8 3.70 2.80 10 -9 8 3.80 3.90 -10 -9 8 15.00 4.80 10 -9 -8 5.00 3.80 10 9 8 6.60 3.50 10 -9 9 25.60 5.60 10 9 -9 16.90 3.80 10 -9 -9 30.30 5.60 10 9 9 19.50 4.80 -10 -9 9 17.40 5.70 10 -9 10 2.90 4.60 -10 -9 10 16.20 5.90 10 9 10 -2.10 3.90 10 -9 -10 5.10 4.50 10 -9 11 5.50 5.30 10 9 11 15.40 5.50 10 -9 -11 8.80 5.20 -10 -9 11 18.10 6.10 11 -9 0 -2.30 1.80 11 9 0 0.90 0.80 -11 -9 0 -6.90 2.50 11 -9 0 -2.90 1.90 -11 -9 -1 28.30 4.60 11 -9 1 27.70 3.30 11 -9 1 25.50 3.80 11 -9 -1 22.20 3.20 -11 -9 1 28.10 5.10 11 9 1 24.30 2.20 11 -9 -1 24.70 3.80 -11 -9 -2 2.30 3.60 11 -9 2 3.30 2.00 11 -9 2 1.50 2.50 11 9 2 2.50 1.40 -11 -9 2 4.70 3.30 11 -9 -2 2.60 1.90 11 -9 -2 4.20 2.10 11 9 -3 27.10 3.40 11 -9 3 25.90 4.00 -11 -9 -3 22.10 4.40 -11 -9 3 20.70 4.20 11 -9 -3 19.80 3.60 11 9 3 18.50 2.70 11 -9 -3 22.00 3.40 11 9 -4 210.18 9.80 11 -9 4 234.88 11.30 -11 9 4 203.58 11.20 -11 -9 4 199.18 11.30 11 -9 -4 227.48 10.60 11 9 4 219.38 9.60 11 -9 5 226.38 11.70 -11 9 5 217.08 11.70 11 9 -5 211.18 10.00 11 9 5 226.58 10.30 -11 -9 5 213.28 8.20 -11 -9 5 209.08 11.80 11 -9 -5 233.58 11.10 11 -9 6 2.00 3.60 11 9 -6 -1.40 2.40 -11 9 6 0.60 3.60 -11 -9 6 6.40 1.50 -11 -9 6 7.40 4.30 11 -9 -6 -0.70 2.90 11 9 6 0.50 2.50 -11 9 7 98.29 7.10 11 -9 7 116.89 8.50 11 9 -7 92.19 6.40 -11 -9 7 100.39 8.30 11 9 7 106.29 7.30 11 -9 -7 102.59 7.80 11 9 -8 44.20 4.90 11 -9 8 60.39 7.20 -11 9 8 64.19 5.80 -11 -9 8 46.80 7.00 11 -9 -8 56.89 6.80 11 9 8 55.49 6.30 11 9 -9 9.40 3.40 11 -9 9 8.70 4.80 -11 -9 9 13.30 5.00 11 -9 -9 9.60 4.60 11 9 9 10.90 4.70 11 -9 10 166.88 12.00 -11 -9 10 164.38 11.40 11 -9 -10 160.28 11.50 11 9 10 169.88 11.40 11 -9 11 9.80 6.00 -11 -9 11 20.90 6.10 11 -9 -11 16.00 6.00 11 9 11 11.60 5.10 -12 -9 0 2.40 3.50 12 -9 0 7.90 2.30 12 9 0 5.50 1.10 12 -9 0 5.10 2.80 12 -9 1 74.39 4.90 12 -9 1 74.19 5.80 -12 -9 -1 70.59 6.10 12 9 1 66.29 3.70 12 -9 -1 74.49 5.10 12 -9 -1 65.39 5.50 -12 -9 1 69.59 6.30 12 -9 2 294.07 13.60 -12 -9 -2 295.77 13.90 12 -9 2 304.17 12.70 12 9 2 310.37 11.90 -12 -9 2 305.47 14.30 12 -9 -2 279.87 13.20 12 -9 -2 297.27 13.00 12 9 -3 95.09 5.90 -12 -9 -3 86.89 7.20 12 -9 3 96.99 5.70 12 -9 3 98.09 7.00 12 9 3 99.19 5.40 12 -9 -3 101.39 6.30 12 -9 -3 90.39 6.50 -12 -9 3 90.99 7.30 12 -9 4 12.00 3.70 -12 9 4 9.70 4.50 12 9 -4 5.60 3.00 12 9 4 8.60 2.50 12 -9 -4 11.60 3.30 -12 -9 4 6.20 3.50 12 9 -5 184.48 9.40 12 -9 5 176.08 10.50 -12 9 5 183.68 10.90 12 9 5 202.38 9.60 -12 -9 5 175.68 10.90 12 -9 -5 194.28 10.20 12 9 -6 52.69 5.20 12 -9 6 45.00 6.00 -12 9 6 46.90 6.30 12 9 6 48.00 5.20 12 -9 -6 53.39 5.90 -12 -9 6 48.40 6.80 -12 9 7 2.90 3.50 12 -9 7 1.90 3.60 12 9 -7 1.80 2.70 12 9 7 -0.80 3.00 12 -9 -7 6.90 3.70 -12 -9 7 4.40 4.10 -12 9 8 10.90 3.70 12 -9 8 6.30 4.40 12 9 -8 4.80 3.10 12 -9 -8 10.90 4.40 12 9 8 10.70 4.00 -12 -9 8 -1.20 4.10 12 -9 9 39.70 6.60 12 9 -9 29.50 4.70 12 9 9 29.20 5.50 -12 -9 9 34.70 6.70 12 -9 -9 35.60 6.10 12 -9 10 8.80 5.30 -12 -9 10 7.60 5.00 12 9 10 7.20 4.80 12 -9 -10 11.90 5.70 13 9 0 1.30 1.00 13 -9 0 -2.30 1.90 13 -9 0 -2.50 1.60 -13 -9 0 -1.60 3.40 13 -9 1 6.30 3.00 13 -9 1 5.80 2.30 -13 -9 -1 3.70 4.30 13 9 1 3.40 1.50 -13 -9 1 2.40 3.80 13 -9 -1 5.60 2.50 13 -9 -1 3.30 2.90 -13 -9 -2 4.10 3.70 13 -9 2 8.00 2.60 13 -9 2 6.50 2.30 13 -9 -2 2.60 2.40 13 9 2 3.40 1.80 -13 -9 2 -0.20 3.80 13 -9 -2 4.80 2.70 13 -9 3 245.98 11.80 13 -9 3 215.28 10.20 -13 -9 -3 212.28 11.90 13 9 -3 211.38 10.50 -13 -9 3 231.38 12.00 13 -9 -3 208.28 10.60 13 9 3 223.08 9.80 13 -9 -3 233.78 11.20 13 -9 4 5.70 3.30 -13 -9 -4 1.00 4.10 -13 9 4 10.00 4.70 13 9 -4 -0.60 2.50 13 9 4 1.40 2.40 -13 -9 4 -1.80 3.90 13 -9 -4 2.70 2.80 -13 9 5 5.40 4.50 13 9 -5 7.20 3.00 13 -9 5 4.50 3.50 -13 -9 5 2.90 4.10 13 9 5 8.10 2.80 13 -9 -5 0.20 2.90 13 -9 6 79.89 7.90 -13 9 6 81.79 7.40 13 9 -6 87.29 6.00 13 9 6 87.49 6.50 13 -9 -6 93.29 7.20 -13 -9 6 95.59 8.10 13 -9 7 63.79 7.50 13 9 -7 68.69 5.50 -13 9 7 72.09 6.70 -13 -9 7 66.49 8.20 13 -9 -7 67.69 7.20 13 9 7 62.69 6.50 13 -9 8 11.80 5.00 13 9 -8 10.70 3.50 -13 9 8 22.40 4.80 13 -9 -8 9.00 4.40 -13 -9 8 16.80 5.40 13 9 8 8.80 4.10 13 -9 9 23.70 6.00 13 9 -9 11.60 3.90 13 -9 -9 11.60 4.90 13 9 9 13.20 5.20 -13 -9 9 16.60 5.40 13 -9 10 13.10 5.70 13 -9 -10 16.60 5.40 13 9 10 23.80 5.70 -13 -9 10 24.80 6.20 14 9 0 75.09 3.90 14 -9 0 85.39 6.50 14 -9 0 75.19 5.60 -14 -9 0 82.89 7.40 -14 -9 -1 407.86 18.70 14 -9 1 415.26 17.10 14 -9 1 410.66 18.00 14 -9 -1 421.36 17.30 14 9 1 420.36 15.70 -14 -9 1 415.36 18.80 14 -9 -1 423.76 17.90 14 -9 2 10.50 2.90 -14 -9 -2 8.90 4.40 14 9 -2 10.90 3.10 14 -9 2 10.00 3.60 -14 -9 2 10.00 4.70 14 -9 -2 15.00 3.60 14 -9 -2 15.90 3.30 14 9 2 12.80 2.40 -14 -9 -3 273.87 14.20 14 -9 3 294.37 13.90 14 -9 3 272.87 12.40 14 9 -3 280.27 13.00 14 -9 -3 275.27 13.00 -14 -9 3 269.57 14.30 14 -9 -3 281.77 13.20 14 9 3 294.67 12.00 14 9 -4 -1.80 2.40 -14 -9 -4 1.60 4.30 -14 9 4 2.20 4.50 14 -9 4 4.80 3.50 14 9 4 4.40 2.70 -14 -9 4 1.20 3.90 14 -9 -4 8.00 3.20 -14 9 5 6.90 4.60 14 -9 5 -2.20 3.20 14 9 -5 4.00 2.70 14 -9 -5 1.70 3.10 14 9 5 3.10 2.50 -14 -9 5 4.70 4.20 14 -9 6 4.00 3.80 14 9 -6 5.40 2.80 -14 9 6 10.50 4.70 14 -9 -6 9.50 4.00 14 9 6 6.90 3.30 -14 -9 6 4.90 4.30 14 -9 7 8.00 4.40 14 9 -7 1.30 2.90 -14 9 7 11.50 4.70 -14 -9 7 7.50 4.80 14 9 7 3.90 3.40 14 -9 -7 5.60 3.80 14 9 -8 1.40 2.80 14 -9 8 0.80 3.30 -14 9 8 2.60 3.30 14 -9 -8 0.60 3.90 -14 -9 8 0.50 4.50 14 9 8 6.40 3.80 14 9 -9 5.80 3.60 14 -9 9 6.10 5.00 14 9 9 2.30 4.20 -14 -9 9 15.30 5.40 14 -9 -9 3.00 4.30 14 -9 10 0.30 5.10 14 -9 -10 2.60 4.70 -14 -9 10 9.90 5.70 14 9 10 5.60 4.80 15 -9 0 -5.10 2.60 15 9 0 -1.60 1.30 15 -9 0 -0.30 2.80 -15 -9 0 -8.70 4.40 15 -9 1 46.90 5.50 15 -9 1 40.10 4.60 -15 -9 -1 33.10 6.50 -15 -9 1 45.20 6.90 15 -9 -1 33.50 4.80 15 -9 -1 47.70 5.00 15 9 1 32.40 3.20 15 -9 2 189.28 9.80 15 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2.80 16 -9 0 36.40 4.90 -16 -9 0 42.00 6.90 16 -9 0 31.60 4.90 16 -9 1 -0.70 2.60 16 -9 1 6.80 3.40 -16 -9 -1 8.00 4.80 -16 -9 1 6.50 5.20 16 -9 -1 6.70 3.00 16 -9 -1 0.20 3.00 16 9 1 8.70 2.10 16 9 -2 29.40 4.40 -16 -9 -2 25.80 5.90 16 -9 2 23.30 4.60 16 -9 2 20.50 4.30 -16 -9 2 23.10 6.30 16 9 2 18.40 3.10 16 -9 -2 26.40 4.40 16 -9 -2 28.80 4.40 16 -9 3 3.10 2.90 16 9 -3 6.00 3.40 16 -9 3 4.50 3.60 -16 -9 -3 6.00 5.00 -16 -9 3 3.90 4.40 16 -9 -3 1.50 2.90 16 9 3 2.40 2.30 16 -9 -3 3.40 3.30 16 -9 4 8.50 4.00 -16 -9 -4 2.90 4.70 16 9 -4 2.20 2.90 -16 9 4 9.20 5.40 16 9 4 6.20 2.90 16 -9 -4 1.60 3.10 -16 -9 4 11.70 5.00 -16 9 5 11.00 5.40 16 9 -5 11.60 3.40 16 -9 5 15.40 4.80 16 -9 -5 14.60 4.20 -16 -9 5 15.70 5.50 16 9 5 10.80 3.20 16 -9 6 18.60 5.00 16 9 -6 11.70 3.90 -16 9 6 17.80 5.20 16 -9 -6 9.50 4.30 -16 -9 6 11.90 5.80 16 9 6 9.40 3.40 16 -9 7 23.20 5.60 16 9 -7 17.50 4.50 -16 9 7 27.90 5.80 16 -9 -7 22.50 5.20 -16 -9 7 32.90 6.90 16 9 7 14.60 4.50 16 -9 8 6.00 5.00 -16 9 8 1.40 3.70 16 9 -8 -2.50 3.40 -16 -9 8 2.80 4.70 16 -9 -8 -2.00 4.10 16 9 8 -2.90 3.70 16 -9 9 -1.30 4.60 16 9 -9 -0.90 3.70 -16 -9 9 4.80 5.00 16 -9 -9 0.70 4.40 16 9 9 -7.50 3.90 -17 -9 0 -0.10 4.60 17 -9 0 1.10 3.70 17 -9 0 -1.50 3.10 17 -9 1 4.10 3.40 17 -9 1 3.40 2.90 -17 -9 -1 1.20 4.80 17 9 1 -1.30 1.60 -17 -9 1 -0.90 4.50 17 -9 -1 0.70 2.90 17 -9 -1 1.00 3.10 17 9 -2 5.30 3.10 17 -9 2 6.40 3.10 -17 -9 -2 5.40 5.40 17 -9 2 7.40 4.10 -17 -9 2 1.60 4.80 17 -9 -2 2.20 3.60 17 9 2 1.30 2.10 17 -9 -2 7.70 3.40 -17 -9 -3 2.80 5.20 17 -9 3 4.70 3.80 -17 9 3 6.60 5.50 17 9 -3 2.40 3.00 17 -9 3 4.50 3.20 17 9 3 5.00 2.50 -17 -9 3 6.80 4.90 17 -9 -3 2.60 3.30 17 -9 -3 3.50 3.20 -17 -9 -4 10.50 5.30 17 -9 4 16.00 4.70 17 -9 4 13.00 3.70 17 9 -4 10.10 3.60 -17 9 4 9.70 6.60 17 9 4 14.10 3.30 -17 -9 4 20.00 5.90 17 -9 -4 22.20 4.70 17 9 -5 4.60 3.30 -17 -9 -5 3.40 5.20 17 -9 5 6.20 4.10 -17 9 5 7.80 5.40 -17 -9 5 3.60 5.30 17 -9 -5 7.30 4.00 17 9 5 12.10 3.50 -17 9 6 17.20 5.90 17 -9 6 19.70 5.30 17 9 -6 15.50 4.20 17 -9 -6 13.90 4.80 -17 -9 6 22.30 6.10 17 9 6 20.80 4.20 -17 9 7 10.30 5.40 17 -9 7 1.90 4.70 17 9 -7 -3.00 2.90 17 -9 -7 -0.50 3.70 -17 -9 7 6.70 5.10 17 9 7 6.10 4.10 17 -9 8 8.00 5.30 17 9 -8 3.40 3.90 -17 9 8 19.30 5.50 17 9 8 9.30 4.30 17 -9 -8 2.40 4.40 -17 -9 8 13.80 5.70 17 -9 9 1.70 5.20 17 9 -9 1.50 3.90 -17 -9 9 8.50 5.30 17 -9 -9 0.40 4.60 17 9 9 -2.50 4.50 -18 -9 0 165.38 11.60 18 -9 0 167.68 10.20 18 -9 0 179.78 9.90 18 -9 1 414.26 18.60 18 -9 1 409.16 18.00 -18 -9 -1 425.86 20.40 18 -9 -1 396.76 18.00 -18 -9 1 423.26 20.20 18 -9 -1 416.46 18.70 -18 -9 -2 19.50 6.20 18 -9 2 18.70 4.00 18 9 -2 21.70 4.40 18 -9 2 21.60 4.80 18 9 2 22.10 3.20 -18 -9 2 25.80 6.50 18 -9 -2 16.70 4.30 18 -9 -2 23.60 4.50 -18 -9 -3 147.79 10.70 18 -9 3 150.58 9.20 18 -9 3 151.48 10.10 18 9 -3 143.89 9.10 -18 9 3 148.49 11.80 -18 -9 3 135.59 10.90 18 9 3 162.98 8.20 18 -9 -3 163.38 9.90 18 -9 -3 143.09 9.30 -18 -9 -4 5.10 5.10 18 -9 4 7.60 3.30 18 9 -4 10.30 3.60 18 -9 4 15.40 4.80 -18 9 4 1.40 5.80 18 9 4 10.40 3.10 -18 -9 4 17.90 6.00 18 -9 -4 8.00 3.80 -18 -9 -5 13.70 6.00 18 9 -5 13.10 3.90 18 -9 5 14.30 4.90 -18 9 5 7.80 6.50 -18 -9 5 11.80 5.70 18 -9 -5 5.30 4.00 18 9 5 18.10 3.80 -18 9 6 51.79 8.50 18 -9 6 54.49 7.80 18 9 -6 49.60 6.50 18 -9 -6 54.09 7.10 18 9 6 51.19 6.20 -18 -9 6 64.89 9.00 18 9 -7 1.50 3.80 -18 9 7 9.80 5.30 18 -9 7 1.20 4.70 18 -9 -7 4.00 4.50 -18 -9 7 11.90 5.70 18 9 7 8.10 4.40 18 9 -8 7.10 4.30 18 -9 8 6.00 5.30 -18 9 8 13.30 5.60 18 9 8 6.80 4.80 -18 -9 8 15.10 6.00 18 -9 -8 0.80 4.30 -19 -9 0 2.50 5.10 19 -9 0 -0.50 3.70 19 -9 0 -1.20 3.00 19 -9 1 42.90 5.60 19 -9 1 33.90 5.60 -19 -9 -1 28.00 6.80 19 -9 -1 40.80 5.80 19 -9 -1 42.60 5.70 -19 -9 1 37.90 7.50 19 -9 2 0.10 3.40 19 -9 2 -1.00 3.40 19 9 -2 0.60 3.20 -19 -9 -2 -2.20 5.50 19 -9 -2 2.30 3.80 -19 -9 2 9.30 5.40 19 -9 -2 2.40 3.30 19 -9 3 155.08 9.30 -19 9 3 157.08 12.50 19 9 -3 157.38 9.70 19 -9 3 158.08 10.60 -19 -9 -3 141.49 11.60 19 9 3 170.08 8.60 19 -9 -3 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52.49 3.70 7 -10 4 49.99 5.00 7 10 -4 49.90 3.40 -7 10 4 51.89 5.00 7 -10 -4 50.79 4.60 -7 -10 4 48.80 2.70 -7 -10 4 50.89 4.80 7 -10 5 34.20 4.40 -7 10 5 44.30 4.50 -7 -10 -5 38.20 2.60 7 10 -5 37.40 3.00 7 -10 -5 36.00 4.40 -7 -10 5 38.10 2.80 -7 -10 5 43.80 5.40 -7 10 6 7.20 2.60 7 10 -6 4.70 2.00 7 -10 6 8.60 3.30 -7 -10 6 4.70 1.90 -7 -10 6 7.20 3.60 7 -10 -6 10.00 3.30 7 -10 7 13.20 3.90 7 10 -7 11.80 2.60 -7 10 7 17.60 3.10 -7 -10 7 11.90 4.10 -7 -10 7 11.30 2.60 7 -10 -7 19.40 4.20 7 -10 8 16.70 4.40 7 10 -8 13.60 3.00 -7 10 8 16.80 3.10 -7 -10 8 11.60 2.80 -7 -10 8 15.00 4.60 7 -10 -8 9.70 4.20 7 -10 9 68.69 7.50 7 10 -9 67.89 5.70 7 10 -9 61.49 8.50 7 -10 -9 70.99 7.80 -7 -10 9 71.39 8.30 -7 -10 9 74.09 5.80 7 10 -10 125.49 11.50 7 -10 10 138.39 10.10 -7 -10 10 124.09 9.70 7 10 10 132.79 9.40 7 -10 -10 113.49 9.70 7 -10 11 18.00 5.60 7 10 11 19.40 5.50 7 -10 -11 22.00 6.20 -7 -10 11 24.10 6.10 -8 -10 0 180.18 8.80 8 10 0 180.28 6.90 8 -10 0 169.88 8.90 8 -10 0 189.88 8.10 8 10 0 183.08 6.70 8 -10 1 696.73 27.00 8 -10 1 728.33 25.90 -8 -10 -1 724.73 26.60 -8 -10 1 709.13 26.90 8 -10 -1 699.53 26.20 8 -10 -1 717.53 27.10 -8 -10 -2 187.18 8.60 8 -10 2 189.08 9.10 8 -10 2 190.18 8.00 8 -10 -2 192.78 9.30 -8 -10 2 192.08 9.30 8 -10 -2 184.58 8.60 8 -10 3 148.09 8.40 -8 -10 -3 164.88 7.80 8 -10 3 150.98 7.00 8 10 -3 161.98 7.30 -8 -10 3 152.28 8.50 8 -10 -3 163.48 7.90 8 -10 -3 164.28 8.50 8 -10 -3 171.68 7.90 -8 10 4 8.10 3.20 8 10 -4 9.90 2.10 8 -10 4 7.50 2.90 -8 -10 -4 11.10 2.90 -8 -10 4 6.90 3.20 -8 -10 4 6.50 1.10 8 -10 -4 10.50 2.00 8 -10 -4 7.10 2.50 -8 -10 -5 217.38 8.70 8 -10 5 215.58 10.80 8 10 -5 205.78 9.10 -8 10 5 194.28 10.00 -8 -10 5 200.08 10.80 8 -10 -5 213.28 10.30 -8 -10 5 217.08 8.40 -8 10 6 95.29 6.20 8 -10 6 89.79 7.10 8 10 -6 95.29 5.50 -8 -10 6 92.69 4.90 8 -10 -6 89.09 6.80 -8 -10 6 92.69 7.30 8 10 -7 549.74 20.70 -8 10 7 509.15 20.90 8 -10 7 579.24 23.00 8 -10 -7 551.24 22.40 -8 -10 7 530.05 22.90 -8 -10 7 526.45 20.30 -8 10 8 16.90 3.40 8 -10 8 18.50 4.50 8 10 -8 14.10 3.10 8 -10 -8 14.80 4.40 -8 -10 8 21.00 5.00 -8 -10 8 12.60 2.90 8 10 -9 318.77 17.80 8 -10 9 336.07 16.40 8 10 -9 312.07 14.20 8 10 9 360.86 15.90 -8 -10 9 322.77 16.40 8 -10 -9 317.77 16.20 8 -10 10 15.10 5.30 8 10 -10 13.50 6.30 -8 -10 10 22.00 5.90 8 -10 -10 21.10 5.80 8 10 10 10.70 4.60 8 -10 11 24.70 6.20 8 -10 -11 31.80 6.90 -8 -10 11 33.60 6.90 8 10 11 24.50 5.90 9 -10 0 -0.90 2.10 -9 -10 0 -1.70 2.20 9 10 0 -1.00 0.60 9 -10 0 -2.20 1.30 9 -10 1 103.69 5.40 9 -10 1 104.99 6.10 -9 -10 -1 93.49 6.20 9 10 1 95.39 4.40 9 -10 -1 102.49 5.50 -9 -10 1 102.89 6.40 9 -10 -1 95.29 5.90 9 -10 2 42.50 4.60 9 -10 2 37.80 3.40 -9 -10 -2 42.30 4.60 9 -10 -2 34.30 4.10 9 10 2 41.40 2.80 9 -10 -2 29.10 3.60 -9 -10 2 48.50 5.10 9 -10 3 8.50 2.10 -9 -10 -3 13.40 3.30 9 -10 3 4.90 2.80 9 10 -3 11.40 2.40 -9 -10 3 15.30 3.70 9 -10 -3 6.70 2.80 9 -10 -3 8.30 2.60 9 10 -4 14.90 2.50 -9 -10 -4 13.70 3.20 -9 10 4 15.50 3.90 9 -10 4 11.80 3.30 9 -10 -4 12.20 2.40 -9 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10.70 10 10 7 197.78 10.10 10 -10 8 30.00 5.70 10 10 -8 28.70 4.00 -10 10 8 33.30 4.70 10 -10 -8 34.90 5.60 -10 -10 8 29.00 6.10 10 10 8 33.10 5.00 10 -10 9 65.59 7.90 10 10 -9 55.19 5.80 10 10 9 77.39 7.60 10 -10 -9 53.09 7.10 -10 -10 9 93.79 9.70 10 -10 10 19.40 5.80 10 -10 -10 15.70 6.10 -10 -10 10 18.00 5.60 10 10 10 15.10 5.60 10 -10 11 6.20 5.40 -10 -10 11 17.90 5.80 10 10 11 7.70 5.00 10 -10 -11 7.00 5.20 -11 -10 0 -3.60 2.70 11 -10 0 -0.20 2.30 11 10 0 -1.50 0.70 11 -10 0 -0.70 1.90 11 -10 1 6.20 2.30 -11 -10 -1 3.20 3.30 11 -10 1 7.30 2.10 11 10 1 3.10 1.30 11 -10 -1 5.80 2.20 11 -10 -1 2.90 2.60 -11 -10 1 8.00 3.90 11 -10 2 184.48 8.40 -11 -10 -2 171.88 9.50 11 -10 2 181.48 9.60 -11 -10 2 187.68 9.90 11 -10 -2 176.58 9.30 11 10 2 179.68 7.60 11 -10 -2 177.68 8.70 11 10 -3 41.20 4.10 11 -10 3 38.80 5.00 11 -10 3 45.10 3.80 -11 -10 -3 46.80 5.40 11 10 3 47.70 3.50 11 -10 -3 46.80 4.90 -11 -10 3 44.00 5.80 11 -10 -3 48.80 4.80 -11 -10 -4 135.69 8.50 11 -10 4 145.19 8.80 11 10 -4 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166.78 8.50 12 -10 2 1.40 2.70 12 -10 2 3.30 2.00 -12 -10 -2 -1.10 3.10 12 10 2 -0.10 1.30 12 -10 -2 1.90 2.60 -12 -10 2 -1.60 3.10 12 -10 -2 4.40 2.30 12 -10 3 185.48 8.80 12 -10 3 195.58 10.30 -12 -10 -3 187.68 10.20 12 10 -3 180.58 8.90 12 10 3 183.28 8.30 12 -10 -3 181.58 9.30 -12 -10 3 175.88 10.40 12 -10 -3 175.48 9.70 -12 -10 -4 83.79 7.20 12 -10 4 69.19 7.00 -12 10 4 84.19 7.90 12 10 -4 86.99 6.00 12 10 4 82.99 5.60 -12 -10 4 81.59 6.90 12 -10 -4 94.29 6.50 12 10 -5 4.20 2.50 12 -10 5 6.20 3.50 -12 10 5 6.20 4.40 12 -10 -5 2.40 3.10 -12 -10 5 7.80 4.20 12 10 5 8.80 2.70 -12 10 6 160.38 9.70 12 10 -6 155.08 8.50 12 -10 6 166.88 10.40 -12 -10 6 157.78 10.40 12 10 6 179.98 9.10 12 -10 -6 167.38 9.70 -12 10 7 135.19 8.60 12 -10 7 153.88 10.20 12 10 -7 143.89 8.10 12 -10 -7 134.29 9.30 12 10 7 151.38 8.90 -12 -10 7 137.29 10.00 -12 10 8 32.60 5.00 12 -10 8 30.00 6.00 12 10 -8 26.20 4.30 -12 -10 8 38.60 6.70 12 -10 -8 30.60 5.60 12 10 8 36.90 5.40 12 10 -9 71.09 7.10 12 -10 9 105.19 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15.90 4.90 15 10 -8 14.50 4.20 15 -10 8 2.00 4.80 -15 10 8 16.00 5.00 15 -10 -8 8.20 4.50 15 10 8 4.40 3.90 -15 -10 8 10.60 5.50 15 -10 9 8.50 5.30 15 10 9 -6.00 4.30 15 -10 -9 2.20 4.50 -15 -10 9 7.10 5.20 -16 -10 0 56.09 7.40 16 -10 0 44.50 6.20 16 -10 0 50.39 5.40 16 -10 1 931.21 35.40 -16 -10 -1 931.01 37.10 16 -10 1 956.20 36.40 -16 -10 1 952.00 37.50 16 -10 -1 971.10 36.40 16 10 1 924.21 33.70 16 -10 -1 925.71 35.60 16 -10 2 135.79 7.90 16 -10 2 120.89 8.80 -16 -10 -2 131.39 9.60 16 10 -2 136.99 8.60 16 -10 -2 133.09 8.70 16 10 2 132.49 6.80 16 -10 -2 146.09 8.40 -16 -10 2 132.79 9.80 -16 -10 -3 343.67 17.10 16 10 -3 341.17 15.50 16 -10 3 354.06 15.40 16 -10 3 366.16 16.90 16 -10 -3 370.26 16.30 16 -10 -3 338.47 15.80 -16 -10 3 349.47 17.40 16 10 3 355.36 14.60 16 -10 4 195.58 11.50 16 -10 4 209.58 10.50 -16 -10 -4 214.98 12.40 -16 10 4 216.38 13.10 16 10 -4 198.88 10.70 -16 -10 4 221.78 12.90 16 10 4 219.08 10.10 16 -10 -4 209.58 11.30 -16 -10 -5 20.40 5.90 -16 10 5 30.10 6.50 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86.89 7.40 18 10 -3 70.19 6.90 18 -10 3 73.79 6.20 -18 10 3 71.59 9.70 18 -10 3 72.59 7.50 -18 -10 -3 70.79 8.90 18 -10 -3 66.39 7.20 18 -10 -3 70.89 7.10 -18 -10 3 76.89 9.40 18 10 3 67.49 5.30 -18 10 4 13.10 6.70 18 -10 4 19.50 5.20 18 10 -4 25.80 4.90 -18 -10 -4 25.50 6.10 18 -10 4 26.80 4.60 18 10 4 23.80 4.00 18 -10 -4 32.20 5.40 -18 -10 4 24.80 6.30 18 10 -5 9.50 4.00 18 -10 5 7.60 3.20 -18 -10 -5 -0.30 5.30 -18 10 5 2.50 6.10 18 -10 5 11.90 5.00 18 -10 -5 12.20 4.40 -18 -10 5 12.80 6.10 18 10 5 9.00 3.50 18 10 -6 39.60 5.60 18 -10 6 56.99 7.70 -18 10 6 43.90 7.40 18 -10 -6 42.10 6.50 18 10 6 34.90 5.30 -18 -10 6 42.00 7.60 -18 10 7 14.80 6.00 18 -10 7 13.70 5.60 18 10 -7 13.30 4.30 18 -10 -7 13.10 5.10 -18 -10 7 25.70 6.60 18 10 7 15.80 4.80 18 -10 8 9.10 5.40 -18 10 8 9.90 4.70 18 10 -8 1.20 3.90 18 10 8 7.50 4.70 -18 -10 8 10.40 5.70 18 -10 -8 3.00 4.60 19 -10 0 6.00 3.30 -19 -10 0 -1.70 5.20 19 -10 0 -2.60 3.40 19 -10 1 12.20 4.30 19 -10 1 15.70 4.00 -19 -10 -1 13.20 5.90 -19 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12.10 2.90 -10 -11 -6 1.90 2.90 10 -11 6 -1.10 2.40 -10 11 6 2.30 3.10 10 11 -6 -0.10 2.10 10 11 6 6.30 2.70 -10 -11 6 3.50 4.00 10 -11 -6 -1.00 3.10 10 -11 7 134.39 9.30 10 11 -7 115.19 6.70 -10 11 7 105.59 7.10 10 11 7 134.99 8.00 10 -11 -7 120.39 8.40 -10 -11 7 124.69 9.00 10 -11 8 13.10 4.60 10 11 -8 8.10 2.80 -10 11 8 12.80 3.40 10 -11 -8 10.90 4.30 -10 -11 8 6.80 4.40 10 11 8 13.00 3.80 10 -11 9 -1.00 4.40 10 -11 -9 2.50 4.00 10 11 9 3.70 3.60 -10 -11 9 6.30 5.00 10 -11 10 13.20 5.20 10 11 -10 -0.30 5.90 -10 -11 10 9.40 5.30 10 11 10 3.60 4.40 10 -11 -10 3.00 4.70 11 -11 0 -0.10 2.60 11 11 0 -0.60 0.70 -11 -11 0 4.60 3.20 11 -11 0 -1.00 1.70 -11 -11 -1 128.59 7.80 11 -11 1 119.69 7.70 11 -11 1 118.49 6.50 11 -11 -1 122.09 7.50 11 11 1 129.49 5.30 -11 -11 1 113.59 7.80 11 -11 -1 116.79 6.60 -11 -11 -2 -3.00 2.60 11 -11 2 3.40 2.90 11 -11 2 0.50 1.80 11 11 2 -4.00 1.20 11 -11 -2 1.90 2.60 -11 -11 2 1.00 3.00 11 -11 -2 0.00 2.00 11 -11 3 23.70 3.00 -11 -11 -3 23.80 4.40 11 11 -3 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2.90 -2 12 4 17.40 1.90 -2 -12 4 20.00 2.50 2 -12 -4 16.90 3.10 -2 12 -4 19.40 4.30 -2 -12 4 16.70 3.30 2 -12 5 23.70 4.20 2 12 -5 20.40 1.50 -2 -12 -5 21.30 3.90 2 -12 5 18.30 3.20 2 -12 -5 18.50 3.60 -2 -12 5 21.20 2.90 -2 -12 5 21.70 4.00 -2 12 -5 21.50 5.20 2 -12 6 50.59 4.90 2 12 -6 45.60 6.40 2 -12 6 53.39 2.30 2 -12 6 46.20 5.90 2 12 -6 50.59 2.80 -2 -12 -6 53.89 6.10 -2 -12 6 51.19 6.10 2 -12 -6 48.60 5.50 -2 -12 6 49.80 4.30 -2 12 -6 50.99 7.30 2 12 -7 1.00 1.40 2 12 -7 -4.50 3.70 2 -12 7 -0.80 3.30 2 -12 7 3.10 2.70 -2 -12 -7 0.70 3.50 -2 -12 7 3.10 3.70 2 -12 -7 -0.90 3.10 -2 -12 7 3.80 2.60 -2 12 -7 -2.80 3.80 2 -12 8 -1.10 3.60 2 12 -8 -1.30 4.20 -2 -12 -8 1.60 4.10 2 -12 8 1.40 2.90 -2 12 -8 0.50 4.40 -2 -12 8 0.20 3.50 -2 -12 8 -2.40 2.40 2 -12 -8 -0.30 3.60 2 12 -9 11.80 6.10 2 -12 9 21.30 4.40 2 -12 9 20.20 5.60 -2 -12 -9 17.70 5.60 -2 -12 9 13.20 5.10 -2 -12 9 18.10 3.90 -2 12 -9 17.30 6.20 2 -12 -9 8.40 4.80 -2 -12 -10 13.30 5.80 2 12 -10 10.20 6.40 2 -12 10 14.80 5.50 2 -12 10 10.00 4.10 -2 -12 10 17.20 4.40 2 -12 -10 16.00 5.70 -2 -12 10 8.20 4.70 2 -12 11 27.00 5.70 2 -12 11 24.40 6.70 2 12 -11 32.80 8.30 -2 -12 -11 25.10 7.10 2 -12 -11 3.60 5.60 -2 -12 11 36.90 5.50 -2 -12 11 20.30 6.20 -3 12 0 -1.70 0.90 3 12 0 -0.70 1.10 3 12 0 -0.90 1.10 3 -12 0 -0.50 1.10 -3 -12 0 -3.50 1.30 3 12 0 -4.10 1.30 3 -12 0 0.60 1.90 -3 12 0 0.40 2.00 3 -12 1 59.69 4.40 3 -12 1 63.39 3.10 3 -12 1 68.89 4.40 3 12 -1 63.19 3.40 -3 12 1 62.89 3.60 -3 12 1 59.39 4.70 3 12 -1 62.79 3.30 -3 -12 -1 63.49 3.40 3 12 1 67.19 3.70 3 -12 -1 52.89 3.70 -3 -12 1 62.69 4.10 -3 -12 1 63.99 3.50 3 -12 -1 58.09 4.50 -3 12 -1 68.29 3.10 -3 12 -1 64.49 5.40 3 -12 2 309.07 11.20 3 -12 2 304.57 13.00 -3 12 2 316.77 13.00 -3 -12 -2 311.57 11.60 3 12 -2 336.87 11.90 -3 12 2 329.97 12.00 3 -12 2 306.87 13.20 3 12 2 319.37 11.80 -3 -12 2 310.07 12.10 -3 12 -2 324.17 14.80 3 -12 -2 316.17 13.20 -3 -12 2 297.17 12.90 3 -12 -2 314.77 12.60 -3 -12 -3 302.17 13.30 -3 12 3 307.77 11.70 3 12 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5.20 4.10 3 -12 8 5.10 3.20 -3 -12 8 2.80 3.70 -3 -12 8 1.50 2.60 -3 12 -8 4.20 5.00 3 -12 -8 1.60 3.90 -3 -12 -9 8.80 5.30 3 -12 9 5.20 4.50 3 12 -9 4.60 4.90 3 -12 9 14.90 4.10 3 -12 -9 6.60 4.80 -3 12 -9 6.50 5.80 -3 -12 9 8.90 4.70 -3 -12 9 12.40 3.60 3 -12 10 4.20 3.80 3 -12 10 2.80 4.80 3 12 -10 -2.80 5.50 -3 -12 10 -0.90 2.80 -3 -12 10 0.40 4.20 3 -12 -10 4.10 4.90 3 -12 11 -0.80 5.00 3 12 -11 -13.10 5.20 3 -12 11 4.50 4.10 -3 -12 11 -1.60 4.40 3 -12 -11 -6.10 4.80 -3 -12 11 8.20 4.20 4 12 0 334.87 12.40 -4 -12 0 334.97 12.90 -4 12 0 311.27 14.20 4 -12 0 315.07 13.50 -4 12 0 336.97 12.40 4 -12 0 325.67 12.40 4 -12 1 5.10 2.20 -4 -12 -1 7.80 1.70 -4 12 1 7.60 2.50 4 12 -1 8.90 1.40 4 -12 1 9.30 1.40 -4 12 -1 9.80 3.00 -4 -12 1 9.00 2.20 4 12 1 6.60 1.50 4 -12 -1 8.50 2.40 4 12 1 8.30 2.00 -4 -12 1 7.80 1.40 4 -12 -1 4.00 1.90 -4 12 -1 10.90 1.40 -4 12 2 137.79 6.90 4 -12 2 129.29 5.10 -4 12 2 128.39 5.80 -4 -12 -2 129.09 5.40 4 12 -2 136.09 5.40 4 -12 2 139.59 7.10 4 -12 2 129.99 6.90 4 -12 -2 124.19 7.00 -4 -12 2 132.19 6.80 -4 -12 2 127.29 5.60 4 -12 -2 121.89 6.30 -4 12 -2 123.69 8.20 4 12 -3 10.90 1.40 4 -12 3 14.80 3.20 4 -12 3 10.70 2.70 -4 -12 -3 12.50 1.10 4 -12 3 14.10 1.10 4 12 -3 13.40 1.50 -4 -12 3 11.90 3.10 4 -12 -3 11.90 2.60 -4 -12 3 12.40 1.80 -4 12 -3 14.10 4.00 4 -12 4 5.00 2.40 -4 12 4 8.50 2.00 4 -12 4 4.00 0.60 4 -12 4 4.30 0.70 4 -12 4 4.80 2.70 4 12 -4 6.40 1.10 -4 -12 4 6.60 2.80 4 -12 -4 2.80 2.30 -4 -12 4 4.30 1.60 -4 12 -4 6.30 3.40 -4 12 5 38.20 2.80 4 -12 5 41.70 5.30 4 12 -5 35.90 2.40 4 -12 5 39.00 4.50 4 -12 5 37.40 1.90 -4 12 -5 37.90 6.20 4 -12 -5 41.20 4.60 -4 -12 5 38.80 3.20 -4 -12 5 43.90 5.10 4 -12 6 113.09 7.80 -4 12 6 110.19 4.90 4 -12 6 118.99 7.30 -4 -12 -6 89.99 7.60 4 12 -6 106.29 5.00 -4 12 -6 104.39 9.50 -4 -12 6 103.89 7.50 4 -12 -6 103.39 7.30 -4 -12 6 119.49 6.10 4 -12 7 26.00 5.40 -4 -12 -7 19.00 4.90 4 -12 7 22.80 4.20 4 12 -7 24.20 5.40 4 12 -7 26.70 2.70 -4 12 7 30.80 2.40 -4 -12 7 25.90 5.20 -4 -12 7 32.00 3.70 4 -12 -7 16.50 4.40 -4 12 -7 21.90 6.10 4 -12 8 156.38 10.20 4 12 -8 146.59 11.30 4 -12 8 155.48 9.40 -4 -12 8 155.38 8.40 -4 12 -8 159.48 12.30 4 -12 -8 138.79 9.70 -4 -12 8 151.58 9.90 4 -12 9 -0.10 4.40 4 12 -9 -3.40 4.40 4 -12 9 -0.90 3.50 4 -12 -9 -5.50 3.60 -4 -12 9 -0.30 3.80 -4 -12 9 1.50 2.90 4 12 -10 -2.00 5.60 4 -12 10 3.20 4.50 4 -12 10 7.00 5.10 -4 -12 10 1.90 4.90 4 -12 -10 -2.30 4.10 -4 -12 10 -2.10 3.10 4 -12 11 -6.10 5.20 4 12 -11 -7.30 5.90 4 -12 11 3.40 4.70 4 -12 -11 0.50 5.00 -4 -12 11 1.30 5.30 5 12 0 0.90 1.00 -5 12 0 -3.00 2.10 5 -12 0 -2.80 1.20 -5 -12 0 -4.20 1.50 5 -12 0 -3.90 1.90 -5 12 0 -3.20 1.10 5 -12 1 26.40 3.50 -5 12 1 27.40 3.60 -5 -12 -1 23.40 2.70 5 -12 1 24.80 2.20 5 12 -1 23.90 1.90 -5 12 -1 28.10 2.10 5 12 1 30.20 2.50 5 -12 -1 28.00 3.40 -5 -12 1 26.70 3.50 5 12 1 30.00 3.30 -5 12 -1 32.50 4.60 5 -12 -1 25.30 2.70 5 -12 2 176.98 7.20 -5 -12 -2 187.68 7.60 5 -12 2 196.58 9.10 5 12 -2 198.28 7.10 -5 -12 2 187.88 7.30 5 -12 -2 179.08 8.30 -5 12 -2 205.98 11.00 -5 -12 2 185.28 8.90 5 -12 -2 178.78 8.90 -5 -12 -3 287.77 10.90 5 -12 3 278.57 12.80 5 -12 3 297.67 10.70 5 12 -3 296.37 11.20 5 -12 -3 308.57 12.50 -5 -12 3 290.57 12.90 -5 12 -3 307.77 14.90 -5 -12 3 294.17 11.10 5 12 -4 127.59 5.40 -5 -12 -4 120.29 4.60 5 -12 4 130.49 4.90 -5 -12 -4 123.49 4.60 5 -12 4 124.99 7.20 5 -12 4 118.19 5.00 -5 12 4 123.29 6.30 5 -12 4 119.89 7.40 -5 -12 4 104.49 7.00 -5 -12 4 128.59 5.60 5 -12 -4 123.39 6.90 -5 12 -4 127.49 9.30 5 -12 5 211.28 7.90 5 12 -5 208.88 8.30 5 -12 5 215.08 11.00 5 -12 5 217.88 10.50 -5 12 5 200.38 8.80 -5 12 -5 202.68 12.70 -5 -12 5 202.18 10.60 5 -12 -5 220.68 10.30 -5 -12 5 204.08 8.80 -5 12 6 3.00 1.70 5 -12 6 6.70 3.60 5 12 -6 2.00 1.50 5 -12 6 3.30 2.90 -5 12 -6 -1.70 4.30 -5 -12 6 2.90 2.00 -5 -12 6 -4.20 3.10 5 -12 -6 -2.30 2.90 5 12 -7 42.60 3.50 -5 12 7 46.80 3.30 5 -12 7 46.30 5.50 5 -12 7 44.30 6.40 5 -12 -7 45.50 5.80 -5 12 -7 47.60 8.10 -5 -12 7 44.90 6.50 -5 -12 7 39.90 4.00 5 12 -8 25.60 6.50 5 -12 8 52.69 7.10 5 -12 8 45.40 5.70 -5 -12 8 35.20 6.10 5 -12 -8 38.60 6.00 -5 -12 8 27.00 3.90 5 -12 9 56.09 7.90 5 -12 9 62.69 7.00 5 12 -9 51.69 8.50 5 -12 -9 64.69 7.80 -5 -12 9 50.79 5.40 -5 -12 9 62.39 8.00 5 12 -10 -4.00 5.20 5 -12 10 2.10 3.90 5 -12 10 4.50 5.50 -5 -12 10 14.60 5.40 -5 -12 10 3.50 3.50 5 -12 -10 2.40 4.50 5 12 -11 25.20 10.20 5 -12 11 40.00 7.20 5 -12 -11 33.20 7.20 -5 -12 11 44.60 7.70 6 -12 0 72.09 5.10 -6 -12 0 60.89 4.20 6 12 0 60.69 3.20 -6 12 0 66.89 5.80 6 -12 0 61.19 3.80 6 12 -1 100.59 4.10 6 -12 1 105.89 6.30 -6 -12 -1 90.49 5.00 6 -12 1 96.79 4.70 6 -12 -1 96.39 5.10 6 -12 -1 97.79 6.20 6 12 1 109.79 4.80 -6 -12 1 92.29 5.60 -6 12 -1 91.59 7.10 -6 -12 -2 11.70 2.00 6 -12 2 8.80 2.60 6 12 -2 11.70 1.00 6 -12 2 11.20 1.60 6 -12 -2 6.80 2.60 -6 -12 2 10.00 2.80 -6 -12 2 10.00 1.20 6 -12 -2 12.90 2.50 -6 12 -2 17.40 4.00 -6 -12 -3 168.68 7.00 6 -12 3 170.18 8.90 6 12 -3 180.08 7.30 6 -12 3 177.38 6.90 -6 12 -3 173.48 10.80 6 -12 -3 172.88 8.30 -6 -12 3 177.58 6.80 -6 -12 3 162.98 8.80 6 -12 4 22.20 1.90 -6 -12 -4 17.30 1.70 6 12 -4 21.50 2.20 -6 12 4 19.80 3.40 6 -12 4 19.10 3.50 -6 12 -4 16.40 5.20 6 -12 -4 14.50 3.10 -6 -12 4 21.40 4.10 -6 -12 4 21.90 2.10 -6 -12 -5 12.40 1.10 -6 -12 -5 12.60 1.00 -6 12 5 12.60 2.90 6 12 -5 14.30 2.00 6 -12 5 15.40 3.50 6 -12 5 16.20 1.80 -6 -12 5 13.10 2.00 -6 -12 5 9.50 3.70 -6 12 -5 11.00 4.90 6 -12 -5 12.30 3.30 6 -12 6 51.69 5.70 6 -12 6 65.49 7.10 -6 12 6 54.99 4.00 6 12 -6 50.59 3.50 6 -12 -6 61.09 6.00 -6 -12 6 54.39 6.50 -6 -12 6 48.10 3.90 6 12 -7 21.70 2.70 -6 12 7 21.20 2.80 6 -12 7 16.50 4.10 6 -12 7 12.30 4.60 -6 -12 7 12.30 2.80 6 -12 -7 11.90 4.00 -6 -12 7 22.60 5.20 6 -12 8 7.40 3.70 6 12 -8 10.20 5.10 -6 -12 8 3.60 2.50 6 -12 -8 4.80 3.90 -6 -12 8 1.70 3.90 6 12 -9 15.90 5.80 6 -12 9 22.90 5.10 -6 -12 9 29.90 6.30 6 -12 -9 16.00 5.00 -6 -12 9 22.10 3.80 6 -12 10 6.40 4.40 6 12 -10 -5.00 5.40 -6 -12 10 1.10 4.20 6 -12 -10 7.40 5.40 6 -12 11 2.20 5.20 6 -12 -11 -0.30 4.60 -6 -12 11 3.70 5.00 7 12 0 -0.90 0.80 7 -12 0 -1.70 1.40 7 -12 0 -0.80 2.10 -7 -12 0 -5.10 1.60 7 -12 1 8.80 1.80 -7 -12 -1 8.00 2.30 7 12 -1 10.40 1.00 7 -12 1 7.30 2.70 -7 -12 1 8.90 2.60 7 -12 -1 9.80 2.90 7 -12 -1 10.10 2.30 7 12 1 5.90 1.60 7 -12 2 6.70 2.30 -7 -12 -2 7.60 2.10 7 -12 2 5.10 1.50 7 -12 -2 6.00 2.70 -7 -12 2 5.60 2.80 7 -12 -2 6.40 2.40 7 -12 3 -2.00 2.20 7 12 -3 2.30 1.50 -7 -12 -3 -0.20 1.50 7 -12 3 0.80 1.20 7 -12 -3 -3.10 2.40 7 -12 -3 -1.30 1.90 -7 -12 3 0.70 0.60 -7 -12 3 -3.40 2.40 7 12 -4 197.68 8.10 7 -12 4 186.38 7.60 7 -12 4 178.98 9.60 -7 -12 -4 185.28 7.70 -7 12 4 183.08 9.20 -7 -12 4 191.08 7.40 7 -12 -4 196.88 9.40 -7 -12 4 187.58 9.90 7 -12 5 18.50 2.20 7 12 -5 14.50 2.20 -7 12 5 12.40 3.20 7 -12 5 10.70 3.40 -7 -12 -5 15.30 1.70 -7 -12 -5 16.00 2.00 -7 -12 5 10.70 3.90 -7 -12 5 14.60 2.00 7 -12 -5 10.50 3.40 -7 12 6 65.69 4.70 7 12 -6 68.09 4.20 7 -12 6 66.59 6.40 7 -12 -6 55.79 6.00 -7 -12 6 62.89 4.10 -7 -12 6 62.99 6.30 7 -12 7 23.80 4.80 7 12 -7 21.40 2.90 -7 12 7 29.30 3.50 7 -12 -7 25.80 4.80 -7 -12 7 20.40 5.10 -7 -12 7 22.10 3.10 7 -12 8 8.90 4.00 -7 -12 8 8.90 2.80 7 -12 -8 6.00 4.10 -7 -12 8 11.20 4.90 7 12 -9 3.60 5.40 7 -12 9 7.20 4.40 7 -12 -9 2.70 4.10 -7 -12 9 6.90 4.50 7 12 -10 23.60 6.80 7 -12 10 28.10 6.00 7 -12 -10 26.20 6.10 -7 -12 10 25.50 6.00 7 -12 11 4.60 4.80 -7 -12 11 9.20 5.30 7 -12 -11 5.70 5.10 7 12 11 5.40 4.50 -8 -12 0 8.40 2.90 8 -12 0 8.80 2.80 8 12 0 12.30 1.40 8 -12 0 13.60 2.20 8 -12 1 392.26 16.50 -8 -12 -1 394.46 15.60 8 -12 1 383.16 14.90 -8 -12 1 373.26 16.00 8 -12 -1 431.96 16.70 8 -12 -1 382.16 15.30 -8 -12 -2 85.39 5.00 8 -12 2 92.09 6.30 8 -12 2 86.89 4.60 8 -12 -2 88.99 5.30 -8 -12 2 76.99 5.80 8 -12 -2 81.09 6.10 -8 -12 -3 73.19 4.50 8 12 -3 73.39 4.40 8 -12 3 70.49 4.00 8 -12 3 74.19 5.90 -8 -12 3 73.99 5.80 8 -12 -3 74.09 5.20 8 -12 -3 64.89 5.70 8 -12 4 7.60 1.60 -8 -12 -4 5.60 2.20 8 12 -4 6.70 1.90 -8 12 4 8.40 3.50 8 -12 4 7.00 3.10 -8 -12 4 5.20 3.30 8 -12 -4 7.80 2.80 -8 -12 4 5.70 1.00 8 -12 5 37.80 5.10 -8 12 5 34.70 4.60 8 12 -5 33.30 3.30 -8 -12 -5 32.60 3.20 8 -12 -5 30.90 4.60 -8 -12 5 35.10 5.20 -8 -12 5 30.00 2.50 8 -12 6 238.58 12.40 8 12 -6 237.18 10.10 -8 12 6 238.48 10.80 8 -12 -6 231.58 11.90 -8 -12 6 235.18 9.70 -8 -12 6 242.58 12.60 8 12 -7 12.80 2.70 -8 12 7 15.80 3.10 8 -12 7 19.50 4.40 -8 -12 7 13.90 4.60 8 -12 -7 9.80 3.90 -8 -12 7 14.60 2.60 8 12 -8 10.20 3.20 8 -12 8 5.40 4.10 -8 -12 8 5.90 4.40 8 -12 -8 7.40 4.10 8 12 -9 30.30 6.60 8 -12 9 30.60 5.80 -8 -12 9 49.50 7.30 8 -12 -9 26.80 5.90 8 -12 10 1.70 4.80 8 12 -10 1.30 5.70 -8 -12 10 8.90 5.10 8 -12 -10 5.70 5.40 8 12 10 -4.00 3.90 8 -12 11 2.00 4.90 -8 -12 11 11.60 5.60 8 -12 -11 0.00 5.00 8 12 11 -2.00 4.40 9 12 0 -0.30 0.80 9 12 0 0.20 0.70 9 -12 0 0.60 1.60 -9 -12 0 -0.40 2.10 9 -12 0 -0.90 2.40 -9 -12 -1 146.59 7.70 9 -12 1 155.08 8.60 9 -12 1 157.68 7.20 9 -12 -1 156.08 8.50 9 -12 -1 165.48 7.50 -9 -12 1 139.79 8.10 -9 -12 -2 372.66 15.80 9 -12 2 399.56 15.20 9 -12 2 368.46 16.60 9 -12 -2 409.36 15.90 9 -12 -2 404.56 16.80 -9 -12 2 409.76 16.80 -9 -12 -3 3.30 2.30 9 12 -3 2.90 1.70 9 -12 3 1.70 1.60 9 -12 3 1.80 2.70 9 -12 -3 7.20 2.50 9 -12 -3 1.10 2.20 -9 -12 3 2.70 3.00 9 -12 4 382.26 16.60 -9 12 4 345.37 16.00 9 12 -4 380.16 14.80 -9 -12 -4 367.06 14.80 9 -12 4 356.96 14.30 9 -12 -4 393.66 15.10 -9 -12 4 375.26 16.60 9 -12 -4 384.76 15.80 9 12 -5 2.90 2.10 -9 12 5 3.90 3.40 9 -12 5 6.30 3.40 -9 -12 -5 7.10 2.60 9 -12 -5 6.70 3.20 -9 -12 5 1.50 1.20 -9 -12 5 -4.70 3.40 9 12 -6 159.48 8.10 -9 12 6 173.08 9.20 9 -12 6 188.58 10.70 9 -12 -6 182.18 10.10 -9 -12 6 183.98 7.50 -9 -12 6 181.78 10.60 -9 12 7 43.10 4.80 9 -12 7 39.00 5.90 9 12 -7 36.90 3.90 -9 -12 7 29.20 5.80 9 -12 -7 35.70 5.50 9 -12 8 59.79 7.30 9 12 -8 67.89 5.60 9 -12 -8 74.69 7.60 -9 -12 8 64.79 8.10 9 -12 9 -0.10 4.10 9 -12 -9 4.50 4.50 -9 -12 9 8.90 4.80 9 12 9 2.90 3.60 9 12 -10 58.09 9.40 9 -12 10 47.20 7.60 9 12 10 49.80 6.90 9 -12 -10 65.09 8.20 -9 -12 10 54.99 8.20 9 -12 11 16.80 6.00 9 -12 -11 20.20 6.40 -9 -12 11 30.10 7.20 9 12 11 20.90 5.60 10 12 0 294.77 11.00 10 12 0 304.47 10.90 10 -12 0 299.27 13.70 10 -12 0 302.07 12.50 -10 -12 0 316.77 13.60 10 -12 1 108.29 7.30 10 -12 1 113.39 6.00 -10 -12 -1 111.19 6.80 10 -12 -1 110.49 6.30 10 12 1 113.79 4.90 -10 -12 1 111.99 7.20 10 -12 -1 104.99 7.10 10 -12 2 24.10 2.80 10 -12 2 19.40 3.90 -10 -12 -2 20.40 3.70 10 -12 -2 17.20 3.70 10 12 2 20.10 2.30 10 -12 -2 24.20 3.40 -10 -12 2 21.50 4.10 10 -12 3 -0.70 1.70 -10 -12 -3 -1.50 2.50 10 -12 3 -3.60 2.40 10 12 -3 0.70 1.90 10 -12 -3 0.00 2.00 -10 -12 3 -1.00 3.00 10 -12 -3 -2.00 2.00 10 -12 4 5.70 3.40 -10 12 4 0.80 3.80 10 12 -4 -1.90 2.10 -10 -12 -4 3.00 2.90 10 -12 4 2.60 1.90 -10 -12 4 0.40 3.60 10 -12 -4 4.20 2.90 10 12 -5 6.20 2.50 10 -12 5 26.40 4.70 -10 12 5 11.90 4.10 -10 -12 -5 3.30 3.00 -10 -12 5 1.00 3.90 10 -12 -5 2.60 3.10 10 -12 6 37.00 5.60 -10 12 6 39.60 5.10 10 12 -6 36.70 3.90 10 -12 -6 34.20 5.30 -10 -12 6 43.00 6.30 -10 12 7 48.70 4.70 10 12 -7 40.80 4.20 10 -12 7 48.60 6.60 10 -12 -7 43.10 5.90 10 12 7 41.40 5.00 -10 -12 7 51.79 7.10 10 12 -8 0.70 2.60 10 -12 8 4.70 4.20 10 12 8 0.80 3.30 10 -12 -8 2.60 3.70 -10 -12 8 0.80 4.10 10 -12 9 18.90 5.70 10 -12 -9 19.50 5.40 10 12 9 25.60 5.20 -10 -12 9 36.70 7.30 10 12 -10 15.40 7.20 10 -12 10 31.70 6.60 10 -12 -10 32.40 6.60 -10 -12 10 28.10 6.60 10 12 10 25.70 6.20 11 12 0 0.80 0.70 11 -12 0 0.70 1.80 11 -12 0 -2.50 2.50 -11 -12 0 -3.70 2.90 11 12 0 -1.80 0.70 11 -12 1 87.79 6.80 -11 -12 -1 102.59 6.90 11 -12 1 96.59 5.60 11 -12 -1 109.99 6.20 -11 -12 1 100.59 7.10 11 -12 -1 93.29 6.90 11 12 1 103.59 4.60 11 -12 2 3.30 2.00 -11 -12 -2 -4.90 2.70 11 -12 2 -0.80 2.60 11 12 2 -0.10 1.40 11 -12 -2 -0.20 2.50 -11 -12 2 2.10 3.50 11 -12 -2 1.90 2.20 11 -12 3 52.89 5.90 11 -12 3 55.09 4.50 -11 -12 -3 57.79 5.60 11 12 -3 45.90 4.40 11 -12 -3 53.59 5.10 -11 -12 3 54.59 6.50 11 12 3 46.80 3.80 11 -12 -3 42.20 5.20 -11 -12 -4 19.10 4.10 11 -12 4 14.70 2.80 11 -12 4 16.10 3.80 -11 12 4 22.30 5.40 11 12 -4 19.00 3.20 11 -12 -4 17.40 3.80 11 12 4 15.20 2.80 -11 -12 4 20.70 4.90 -11 -12 -5 53.79 5.30 11 -12 5 60.49 6.60 -11 12 5 63.69 6.80 11 12 -5 49.80 4.70 11 -12 -5 53.69 5.80 11 12 5 52.19 4.60 -11 -12 5 58.49 7.10 11 -12 6 5.70 4.00 11 12 -6 10.50 2.70 -11 12 6 9.10 3.70 -11 -12 6 10.40 4.40 11 -12 -6 6.10 3.50 11 12 6 9.00 3.10 11 12 -7 18.50 3.30 11 -12 7 17.70 4.80 -11 12 7 21.20 4.10 -11 -12 7 20.20 5.30 11 12 7 23.20 4.20 11 -12 -7 15.60 4.50 11 -12 8 30.10 5.90 11 12 -8 30.90 4.10 -11 -12 8 29.70 6.20 11 -12 -8 38.00 6.00 11 12 8 24.40 4.70 11 -12 9 10.10 5.10 11 -12 -9 10.50 4.70 -11 -12 9 17.40 5.50 11 12 9 8.10 4.20 11 12 -10 3.40 6.30 11 -12 10 6.10 5.00 -11 -12 10 12.00 5.80 11 12 10 4.20 4.30 11 -12 -10 5.90 5.00 12 -12 0 1.70 2.20 -12 -12 0 2.30 3.20 12 12 0 0.70 0.70 12 -12 0 -0.60 2.10 12 12 0 0.20 0.80 12 -12 1 22.60 4.30 -12 -12 -1 26.20 4.80 12 -12 1 27.10 3.60 12 -12 -1 25.20 3.50 -12 -12 1 31.00 4.90 12 12 1 28.50 2.40 12 -12 -1 16.90 3.90 12 -12 2 35.10 4.70 12 -12 2 31.30 3.50 -12 -12 -2 32.00 5.00 12 12 2 34.70 2.90 -12 -12 2 40.90 5.90 12 -12 -2 26.90 4.50 12 -12 -2 33.40 4.20 12 -12 3 59.99 4.70 12 -12 3 67.19 6.60 12 12 -3 59.99 5.30 -12 -12 -3 65.09 6.60 12 -12 -3 59.29 6.20 -12 -12 3 66.89 7.30 12 -12 -3 57.19 5.60 12 12 3 55.59 4.40 12 -12 4 263.37 11.50 12 12 -4 264.57 12.00 -12 12 4 239.58 13.30 12 -12 4 279.67 13.80 -12 -12 -4 257.87 12.40 12 -12 -4 273.27 12.90 -12 -12 4 276.27 13.90 12 12 4 292.77 11.80 12 12 -5 11.70 2.70 12 -12 5 11.10 2.60 12 -12 5 10.90 3.60 -12 12 5 15.10 4.80 -12 -12 -5 9.80 3.70 12 -12 -5 10.50 3.60 -12 -12 5 14.60 4.70 12 12 5 15.50 3.20 -12 12 6 35.50 5.70 12 -12 6 37.60 5.90 12 12 -6 37.80 4.30 12 -12 -6 40.00 5.50 12 12 6 32.60 4.60 -12 -12 6 35.10 6.40 12 12 -7 5.50 2.70 -12 12 7 7.20 3.50 12 -12 7 0.60 3.90 12 12 7 3.00 3.00 12 -12 -7 8.10 3.90 -12 -12 7 7.50 4.40 12 12 -8 -1.70 2.70 12 -12 8 1.60 4.40 12 -12 -8 1.30 3.90 12 12 8 -4.00 3.00 -12 -12 8 3.20 4.90 12 -12 9 18.60 6.00 -12 -12 9 12.80 5.50 12 12 9 12.00 4.40 12 -12 -9 14.30 5.20 12 -12 10 12.10 5.80 12 -12 -10 9.30 5.30 12 12 10 2.40 4.40 -12 -12 10 14.60 5.60 13 -12 0 -1.20 2.90 13 12 0 -0.40 0.70 -13 -12 0 -2.20 3.90 13 -12 0 -4.00 1.90 13 12 0 -0.60 0.70 -13 -12 -1 -0.40 3.80 13 -12 1 2.70 2.20 13 -12 1 1.00 2.90 13 12 1 1.10 1.40 13 -12 -1 -0.20 2.70 -13 -12 1 2.00 3.90 13 -12 -1 -5.00 2.90 -13 -12 -2 97.89 7.60 13 -12 2 99.09 6.30 13 -12 2 105.49 7.80 13 12 2 109.99 5.40 13 -12 -2 109.99 7.10 -13 -12 2 95.19 7.80 13 -12 -2 82.49 7.30 13 -12 3 70.29 5.30 13 -12 3 85.99 7.20 13 12 -3 68.09 6.00 -13 -12 -3 66.59 6.90 13 12 3 68.99 4.70 13 -12 -3 68.29 6.70 13 -12 -3 67.69 5.80 -13 -12 3 62.99 7.50 13 -12 4 183.28 9.00 13 12 -4 181.88 9.50 13 -12 4 192.58 11.10 -13 -12 -4 189.58 10.30 -13 12 4 180.78 11.30 13 -12 -4 188.38 10.10 -13 -12 4 194.78 11.30 13 12 4 179.88 8.90 13 -12 5 7.50 2.40 13 -12 5 2.50 3.70 13 12 -5 2.20 2.50 -13 -12 -5 4.00 3.70 -13 12 5 1.10 3.90 13 12 5 2.70 2.70 -13 -12 5 1.20 4.00 13 -12 -5 3.70 3.10 13 12 -6 23.40 3.70 13 -12 6 29.50 5.40 -13 12 6 33.00 5.70 -13 -12 6 21.30 5.60 13 -12 -6 17.00 4.40 13 12 6 20.90 3.90 -13 12 7 10.10 4.00 13 12 -7 2.40 2.70 13 -12 7 4.50 4.20 -13 -12 7 7.00 4.70 13 12 7 9.10 3.60 13 -12 -7 -1.00 3.70 13 12 -8 14.80 3.60 13 -12 8 25.60 6.00 13 12 8 29.60 5.50 -13 -12 8 30.30 6.50 13 -12 -8 21.90 5.20 13 -12 9 0.50 4.90 13 12 9 -0.40 3.80 13 -12 -9 5.20 4.40 -13 -12 9 11.80 5.40 13 -12 10 91.19 10.50 13 -12 -10 110.29 11.00 -13 -12 10 114.79 10.60 13 12 10 101.79 9.90 14 -12 0 7.00 3.00 -14 -12 0 -2.00 4.00 14 -12 0 5.10 3.40 14 12 0 2.60 1.30 -14 -12 -1 -1.80 3.90 14 -12 1 4.00 3.40 14 -12 1 0.90 2.70 14 12 1 0.20 1.40 14 -12 -1 -1.60 2.60 14 -12 -1 4.00 3.40 -14 -12 1 0.60 3.90 14 -12 2 274.37 13.50 14 -12 2 274.47 12.00 -14 -12 -2 258.37 12.90 14 12 2 262.57 10.70 14 -12 -2 252.17 13.00 -14 -12 2 248.48 13.40 14 -12 -2 248.48 12.10 14 -12 3 72.79 5.50 14 -12 3 70.59 7.10 14 12 -3 68.69 5.50 -14 -12 -3 70.69 6.80 14 -12 -3 75.59 7.10 -14 -12 3 76.39 8.30 14 12 3 67.19 4.80 14 -12 -3 75.49 6.20 14 -12 4 1.00 3.50 14 12 -4 2.60 2.70 -14 -12 -4 5.30 3.90 14 -12 4 1.60 2.40 -14 12 4 0.00 4.20 -14 -12 4 6.60 4.10 14 -12 -4 -3.10 2.70 14 12 4 1.30 2.40 -14 -12 -5 13.40 4.50 14 -12 5 10.90 4.40 14 12 -5 13.00 3.40 -14 12 5 11.30 5.30 14 -12 5 12.40 3.00 -14 -12 5 9.50 4.80 14 -12 -5 7.20 3.80 14 12 5 12.00 3.40 14 12 -6 -1.50 2.50 -14 12 6 3.10 3.80 14 -12 6 0.00 3.90 14 12 6 -1.30 2.90 -14 -12 6 3.60 4.50 14 -12 -6 3.50 3.50 14 -12 7 10.60 4.10 14 12 -7 7.10 3.10 -14 12 7 6.70 4.20 14 -12 -7 11.00 4.40 -14 -12 7 16.10 5.50 14 12 7 5.40 3.50 14 -12 8 51.39 7.60 14 12 -8 40.80 5.70 -14 -12 8 42.10 7.40 14 12 8 42.90 5.90 14 -12 -8 43.10 6.60 14 -12 9 6.20 5.40 14 12 9 2.90 4.30 -14 -12 9 7.00 5.50 14 -12 -9 2.80 4.50 15 -12 0 1.60 3.50 15 -12 0 -2.10 2.30 -15 -12 0 -6.60 4.20 15 -12 1 57.79 6.50 15 -12 1 59.89 5.60 -15 -12 -1 52.49 7.00 15 -12 -1 55.39 5.60 15 12 1 54.89 3.50 -15 -12 1 52.79 7.20 15 -12 -1 50.09 6.30 -15 -12 -2 13.60 5.00 15 -12 2 16.70 3.50 15 -12 2 17.60 4.40 15 -12 -2 14.00 3.60 15 -12 -2 6.00 3.80 -15 -12 2 12.40 4.90 15 12 2 14.20 2.50 -15 -12 -3 3.40 4.20 15 -12 3 0.60 3.60 15 -12 3 0.60 2.60 15 12 -3 8.30 3.20 15 -12 -3 -0.40 3.30 15 12 3 4.20 2.20 15 -12 -3 2.10 3.10 -15 -12 3 4.10 4.20 15 12 -4 19.90 3.90 -15 12 4 16.60 6.20 15 -12 4 19.70 4.90 -15 -12 -4 16.20 4.90 15 -12 4 14.90 3.30 15 -12 -4 15.40 4.30 15 12 4 19.90 3.20 15 -12 -4 12.50 3.90 -15 -12 4 18.40 5.40 -15 12 5 7.30 5.00 15 -12 5 13.50 4.00 15 -12 5 8.50 2.80 15 12 -5 10.20 3.10 -15 -12 -5 8.60 4.50 -15 -12 5 14.00 5.20 15 -12 -5 5.30 3.70 15 12 5 11.30 3.10 15 12 -6 -0.10 2.30 15 -12 6 -3.40 3.80 -15 12 6 -2.00 4.60 15 12 6 -2.10 2.50 -15 -12 6 4.50 4.70 15 -12 -6 -1.50 3.60 -15 12 7 14.60 5.20 15 -12 7 19.00 5.60 15 12 -7 15.30 3.80 15 12 7 7.20 3.70 15 -12 -7 16.90 5.00 -15 -12 7 26.10 6.30 15 -12 8 12.10 5.50 15 12 -8 8.40 4.20 15 12 8 22.20 4.90 -15 -12 8 21.00 6.50 15 -12 -8 21.60 5.60 15 -12 9 46.50 8.00 15 12 9 31.60 6.40 15 -12 -9 24.00 6.00 -15 -12 9 36.80 7.40 -16 -12 0 3.50 4.30 16 -12 0 2.40 3.00 16 -12 0 -4.50 3.10 16 -12 1 116.99 7.30 -16 -12 -1 103.59 9.00 16 -12 1 122.09 8.70 16 -12 -1 111.49 7.50 -16 -12 1 126.49 9.60 16 -12 -1 127.29 8.70 16 -12 2 5.50 3.00 -16 -12 -2 -0.70 4.30 16 -12 2 0.10 3.70 16 12 -2 1.30 2.80 16 -12 -2 4.20 3.50 16 -12 -2 5.00 3.00 16 12 2 4.50 2.00 -16 -12 2 8.60 4.70 16 12 -3 42.10 5.30 16 -12 3 47.90 6.50 16 -12 3 44.90 5.00 -16 -12 -3 41.80 6.60 16 12 3 42.30 4.20 16 -12 -3 36.30 5.60 -16 -12 3 49.30 7.20 16 -12 -3 41.70 5.40 16 12 -4 67.29 5.60 16 -12 4 52.89 5.40 16 -12 4 60.79 7.20 -16 -12 -4 56.29 7.30 -16 12 4 55.09 8.20 16 12 4 49.99 4.80 -16 -12 4 52.09 8.10 16 -12 -4 51.69 6.30 16 -12 -4 42.70 6.00 -16 -12 -5 7.40 4.40 16 -12 5 4.60 2.80 -16 12 5 9.90 5.30 16 12 -5 7.40 3.40 16 -12 5 5.70 4.30 16 12 5 5.80 3.10 16 -12 -5 9.30 4.10 -16 -12 5 11.30 5.20 16 12 -6 11.70 3.70 16 -12 6 7.50 4.80 16 -12 6 9.40 3.20 -16 12 6 10.20 5.40 -16 -12 6 8.50 5.20 16 12 6 6.20 3.40 16 -12 -6 6.70 4.20 -16 12 7 28.00 6.00 16 -12 7 33.20 6.70 16 12 -7 20.50 4.10 16 12 7 26.70 5.00 16 -12 -7 21.40 5.40 -16 -12 7 29.90 6.70 16 -12 8 0.30 4.90 16 -12 -8 -2.20 4.40 16 12 8 -0.20 3.60 -16 -12 8 11.00 6.00 17 -12 0 1.90 3.80 17 -12 0 -1.10 2.80 -17 -12 0 -2.30 4.70 17 -12 1 34.00 5.60 -17 -12 -1 34.80 6.50 17 -12 1 33.90 4.60 17 -12 -1 28.70 5.20 17 -12 -1 33.00 5.10 -17 -12 1 37.70 6.70 17 -12 2 77.69 7.00 17 12 -2 75.39 7.10 17 -12 2 82.09 8.20 -17 -12 -2 75.89 7.70 17 -12 -2 80.19 6.70 -17 -12 2 99.69 10.10 17 -12 -2 90.89 8.20 17 -12 3 6.60 3.20 17 12 -3 8.90 3.40 17 -12 3 1.40 3.80 -17 -12 -3 2.80 4.60 -17 -12 3 5.00 4.90 17 -12 -3 2.20 3.70 17 -12 -3 8.20 3.50 17 12 3 4.70 2.40 -17 -12 -4 72.59 8.30 -17 12 4 81.49 10.20 17 -12 4 72.89 8.20 17 12 -4 68.69 6.60 17 -12 4 70.69 6.50 17 12 4 66.79 5.60 -17 -12 4 77.09 9.20 17 -12 -4 74.69 7.30 17 -12 -4 71.59 7.40 17 12 -5 111.89 7.80 -17 12 5 103.79 10.20 -17 -12 -5 94.79 8.60 17 -12 5 107.79 9.90 17 -12 5 81.69 6.80 17 -12 -5 107.79 8.50 -17 -12 5 109.19 9.50 17 12 5 108.09 7.00 -17 12 6 22.00 6.30 17 -12 6 9.80 3.60 17 12 -6 9.90 3.50 17 -12 6 10.60 5.00 -17 -12 6 16.20 6.10 17 12 6 11.40 4.00 17 -12 -6 7.80 4.60 -17 12 7 4.60 4.90 17 12 -7 0.40 3.20 17 -12 7 1.10 4.70 -17 -12 7 -1.90 4.60 17 -12 -7 -4.30 3.90 17 12 7 2.30 3.80 17 -12 8 3.40 5.10 -17 -12 8 10.00 6.30 17 -12 -8 10.30 5.30 17 12 8 2.10 3.80 18 -12 0 97.49 8.20 -18 -12 0 83.49 8.40 18 -12 0 92.49 7.10 18 -12 1 10.20 3.60 18 -12 1 14.20 4.60 -18 -12 -1 3.70 4.70 -18 -12 1 11.30 5.80 18 -12 -1 7.70 4.10 18 -12 -1 10.30 3.50 18 12 -2 2.10 3.10 18 -12 2 2.20 2.90 18 -12 2 1.80 4.00 -18 -12 -2 -1.50 4.30 18 -12 -2 -0.30 3.50 -18 -12 2 4.90 5.20 18 -12 -2 1.90 3.00 -18 -12 -3 9.70 5.50 18 -12 3 8.90 3.30 18 12 -3 12.30 3.70 18 -12 3 12.80 4.50 18 -12 -3 6.40 3.70 18 -12 -3 8.30 4.50 -18 -12 3 13.10 5.90 18 12 -4 1.50 3.40 18 -12 4 2.10 4.30 -18 -12 -4 -0.90 4.70 18 -12 4 1.40 3.30 -18 12 4 -7.10 5.90 18 -12 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1.40 1.70 10 -13 -2 -0.90 2.00 -10 -13 2 1.10 2.90 10 -13 -2 3.80 2.80 10 13 -3 2.00 1.90 10 -13 3 6.70 3.40 -10 -13 -3 1.80 2.40 10 -13 3 2.10 1.80 10 -13 -3 5.80 3.10 -10 -13 3 0.50 3.20 10 -13 -3 2.80 2.50 10 13 -4 46.30 4.00 10 -13 4 46.70 3.80 -10 -13 -4 47.20 4.40 10 -13 4 49.70 5.60 -10 -13 4 41.40 6.00 10 -13 -4 55.29 5.40 10 -13 5 3.10 1.90 10 13 -5 4.70 2.20 10 -13 5 2.50 3.60 -10 13 5 3.70 3.70 -10 -13 -5 2.60 2.30 -10 -13 5 3.70 3.80 10 -13 -5 -1.90 3.00 10 13 -6 12.30 2.60 -10 13 6 17.60 3.90 10 -13 6 10.50 4.20 10 -13 -6 10.20 3.80 -10 -13 6 15.80 4.70 -10 13 7 85.99 6.20 10 13 -7 81.79 5.50 10 -13 7 86.59 8.30 10 -13 -7 86.09 7.50 -10 -13 7 85.89 7.80 10 -13 8 -0.10 4.00 10 -13 -8 -0.20 3.70 10 13 8 -4.10 2.80 -10 -13 8 1.30 4.20 10 -13 9 16.40 5.50 10 13 9 17.70 4.70 -10 -13 9 30.50 6.90 10 -13 -9 18.80 5.40 10 13 -10 -4.50 6.10 10 -13 10 8.80 5.40 10 -13 -10 11.10 5.20 10 13 10 3.60 4.50 -10 -13 10 7.60 5.00 -11 -13 0 -0.60 2.50 11 -13 0 -0.80 2.10 11 13 0 -0.70 0.60 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4.40 11 13 7 -2.70 2.60 11 -13 -7 3.30 3.70 11 -13 8 -4.60 3.80 11 -13 -8 -0.50 3.90 11 13 8 -3.70 3.00 -11 -13 8 4.00 4.40 11 -13 9 5.00 4.90 11 -13 -9 11.20 4.70 11 13 9 5.90 4.20 -11 -13 9 8.30 5.10 11 -13 10 43.70 7.60 11 13 -10 34.90 8.40 11 -13 -10 41.20 7.20 -11 -13 10 33.20 6.90 11 13 10 34.00 6.20 12 13 0 54.19 2.50 12 13 0 51.49 2.40 12 -13 0 57.69 5.10 12 -13 0 50.99 5.80 -12 -13 0 55.59 5.50 -12 -13 -1 358.06 16.00 12 -13 1 362.16 14.90 12 -13 1 370.36 16.50 12 -13 -1 361.36 16.40 12 -13 -1 358.56 15.30 -12 -13 1 359.96 16.50 12 13 1 379.46 13.60 12 -13 2 14.60 4.20 -12 -13 -2 15.90 4.30 12 -13 2 19.40 3.20 -12 -13 2 15.70 4.40 12 -13 -2 18.80 3.60 12 -13 -2 16.30 4.00 12 13 2 17.70 2.30 -12 -13 -3 140.59 8.10 12 13 -3 132.79 7.60 12 -13 3 130.39 8.60 12 -13 3 133.19 7.00 -12 -13 3 136.59 9.10 12 13 3 131.59 6.80 12 -13 -3 129.49 7.90 12 -13 -3 140.69 8.80 12 -13 4 18.70 3.00 -12 -13 -4 14.40 3.80 12 13 -4 15.40 3.30 12 -13 4 16.50 3.90 12 13 4 14.40 2.70 -12 -13 4 13.10 4.70 12 -13 -4 12.80 3.60 12 -13 5 5.80 2.30 -12 -13 -5 -0.50 2.80 12 -13 5 4.60 3.00 12 13 -5 -0.80 2.20 -12 13 5 -4.90 3.70 12 13 5 -1.40 2.00 -12 -13 5 4.50 4.10 12 -13 -5 0.50 2.90 12 13 -6 3.80 2.40 -12 13 6 2.60 3.70 12 -13 6 3.40 3.70 12 -13 -6 4.50 3.60 -12 -13 6 0.50 3.80 12 13 6 2.50 2.60 12 13 -7 0.30 2.40 -12 13 7 7.90 3.60 12 -13 7 -4.60 3.40 -12 -13 7 4.30 4.30 12 13 7 -2.40 2.70 12 -13 -7 3.90 3.60 12 -13 8 34.10 6.50 12 13 8 25.80 4.80 -12 -13 8 26.30 6.10 12 -13 -8 23.80 5.50 12 -13 9 14.90 5.80 12 -13 -9 10.20 5.10 -12 -13 9 16.90 5.90 12 13 9 15.00 4.70 12 -13 10 90.49 10.60 12 13 10 82.39 8.50 12 -13 -10 91.89 10.20 -12 -13 10 92.29 9.30 13 13 0 -0.20 0.60 13 -13 0 -3.60 2.10 -13 -13 0 -2.80 3.80 13 -13 0 -8.20 2.80 -13 -13 -1 17.30 4.40 13 -13 1 16.90 3.10 13 -13 1 16.50 4.20 -13 -13 1 12.30 4.40 13 -13 -1 7.50 3.90 13 13 1 17.00 2.00 13 -13 -1 15.40 3.30 13 -13 2 30.70 5.20 -13 -13 -2 25.40 5.10 13 -13 2 30.20 3.70 -13 -13 2 28.80 5.40 13 13 2 27.80 2.80 13 -13 -2 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14 -13 8 4.30 5.20 14 13 8 3.20 4.20 14 -13 -8 -6.80 4.20 -14 -13 8 13.40 5.50 14 -13 9 20.70 6.50 14 -13 -9 24.30 6.20 -14 -13 9 35.00 7.50 14 13 9 13.90 5.10 15 -13 0 -1.80 3.30 15 -13 0 -1.50 2.80 -15 -13 0 -0.80 3.80 -15 -13 -1 4.10 4.00 15 -13 1 8.60 2.90 15 -13 1 4.90 3.50 15 -13 -1 2.30 2.70 15 -13 -1 -5.20 3.10 -15 -13 1 3.90 3.90 15 -13 2 46.60 6.30 -15 -13 -2 56.39 7.00 15 -13 2 46.90 5.00 15 -13 -2 56.99 6.00 -15 -13 2 51.29 7.00 15 -13 -2 52.69 6.30 15 13 2 47.60 3.70 -15 -13 -3 21.90 5.00 15 -13 3 21.20 3.60 15 13 -3 22.30 3.90 15 -13 3 23.10 5.10 15 13 3 17.90 2.90 15 -13 -3 15.30 4.30 -15 -13 3 22.70 5.60 15 -13 -3 19.20 4.20 15 13 -4 4.80 3.00 -15 13 4 0.60 5.10 -15 -13 -4 5.60 4.00 15 -13 4 4.80 2.70 15 -13 4 1.20 3.90 15 -13 -4 1.20 3.80 15 13 4 4.10 2.40 15 -13 -4 7.00 3.70 -15 -13 4 0.40 4.10 -15 -13 -5 -1.10 3.80 15 -13 5 2.80 2.50 -15 13 5 -1.90 4.50 15 -13 5 3.00 4.00 15 13 -5 3.60 2.80 15 -13 -5 -1.80 3.10 15 13 5 0.50 2.50 -15 -13 5 -2.70 4.10 15 13 -6 42.80 5.10 15 -13 6 46.30 7.00 -15 13 6 43.30 6.90 15 13 6 41.30 5.10 15 -13 -6 42.50 6.10 -15 -13 6 59.09 8.50 15 -13 7 13.70 5.40 -15 13 7 8.70 4.20 15 13 -7 7.50 3.50 15 -13 -7 7.90 4.50 15 13 7 5.10 3.40 -15 -13 7 5.90 5.10 15 -13 8 4.40 5.20 -15 -13 8 5.30 5.10 15 13 8 4.60 3.80 15 -13 -8 9.80 4.80 15 -13 9 4.00 5.50 15 13 9 8.20 4.60 15 -13 -9 7.90 5.20 -15 -13 9 12.60 6.00 -16 -13 0 62.79 7.80 16 -13 0 46.70 6.20 16 -13 0 46.80 5.30 -16 -13 -1 -1.00 4.20 16 -13 1 1.50 3.60 16 -13 1 0.20 2.70 -16 -13 1 2.40 4.10 16 -13 -1 -3.80 2.40 16 -13 -1 2.20 3.50 16 -13 2 13.60 4.50 -16 -13 -2 16.40 5.20 16 -13 2 12.20 3.20 16 -13 -2 11.20 3.60 -16 -13 2 13.20 4.90 16 -13 -2 9.30 4.00 -16 -13 -3 5.60 4.50 16 -13 3 6.70 3.50 16 -13 3 1.80 2.40 16 13 -3 0.20 2.50 16 13 3 6.50 2.30 16 -13 -3 -1.40 3.00 -16 -13 3 4.70 4.50 16 -13 -3 -0.20 3.50 16 13 -4 2.90 3.10 -16 -13 -4 11.70 4.50 16 -13 4 3.10 2.50 -16 13 4 12.20 5.60 16 -13 4 -2.40 3.70 -16 -13 4 5.20 4.60 16 -13 -4 5.60 4.00 16 13 4 7.50 2.90 16 -13 -4 3.90 3.60 -16 13 5 3.30 5.70 -16 -13 -5 5.10 5.20 16 -13 5 8.10 3.10 16 13 -5 2.70 3.10 16 -13 5 8.60 4.70 16 13 5 5.50 2.70 -16 -13 5 6.80 5.10 16 -13 -5 8.10 3.80 16 13 -6 70.79 6.60 -16 13 6 77.49 9.00 16 -13 6 68.79 8.40 -16 -13 6 79.99 9.70 16 13 6 85.69 6.80 16 -13 -6 61.89 7.40 16 -13 7 29.30 6.60 -16 13 7 39.00 6.70 16 13 -7 33.60 5.00 16 13 7 33.20 5.30 16 -13 -7 32.60 6.20 -16 -13 7 39.30 7.40 16 -13 8 57.59 8.50 16 -13 -8 39.70 7.00 -16 -13 8 63.89 8.90 16 13 8 44.10 6.00 17 -13 0 -3.70 3.40 -17 -13 0 -2.70 4.00 17 -13 0 0.20 3.10 17 -13 1 5.90 4.00 17 -13 1 0.40 2.90 -17 -13 -1 -2.80 3.80 17 -13 -1 -4.30 3.40 17 -13 -1 1.80 2.90 -17 -13 1 1.00 4.30 17 -13 2 43.50 5.10 -17 -13 -2 54.19 7.10 17 13 -2 54.19 6.20 17 -13 2 47.50 6.60 -17 -13 2 60.19 7.70 17 -13 -2 39.40 6.00 17 -13 -2 44.50 5.60 17 13 -3 9.60 3.70 -17 -13 -3 4.20 4.80 17 -13 3 13.50 3.50 17 -13 3 3.40 4.20 17 -13 -3 12.40 3.90 17 -13 -3 7.40 4.50 -17 -13 3 12.10 5.20 -17 13 4 18.60 6.80 -17 -13 -4 20.50 5.40 17 -13 4 19.10 3.90 17 13 -4 24.10 4.10 17 -13 4 17.60 5.20 -17 -13 4 26.90 6.70 17 -13 -4 19.30 4.70 17 13 4 18.30 3.40 17 -13 -4 18.30 4.90 17 13 -5 -0.50 3.10 17 -13 5 9.50 5.00 -17 13 5 -0.90 5.50 17 -13 5 3.80 3.00 -17 -13 5 14.70 5.60 17 13 5 7.30 3.10 17 -13 -5 7.90 4.00 -17 13 6 55.69 8.50 17 13 -6 47.90 5.90 17 -13 6 59.69 8.20 17 -13 -6 52.49 7.10 17 13 6 49.80 5.90 -17 -13 6 62.59 9.00 17 -13 7 -1.30 4.80 17 13 -7 1.10 3.20 -17 13 7 8.80 4.90 17 -13 -7 4.80 4.50 -17 -13 7 6.80 5.40 17 13 7 -0.40 3.90 17 -13 8 1.70 5.10 -17 -13 8 10.50 5.70 17 13 8 2.40 3.60 17 -13 -8 3.70 4.80 18 -13 0 60.89 6.20 -18 -13 0 70.69 8.50 18 -13 0 62.29 7.40 -18 -13 -1 31.50 6.70 18 -13 1 22.00 5.30 18 -13 1 28.90 4.70 18 -13 -1 16.80 4.80 -18 -13 1 32.20 6.70 18 -13 -1 25.90 4.60 18 -13 2 -2.80 2.90 18 -13 2 3.00 4.10 18 13 -2 -0.80 2.90 -18 -13 -2 2.40 4.30 -18 -13 2 -0.90 4.40 18 -13 -2 -3.30 3.30 18 -13 -2 -5.50 3.30 18 -13 3 4.00 3.10 18 13 -3 1.20 3.30 -18 -13 -3 -0.90 4.70 18 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198.38 9.90 0 -14 4 200.08 10.10 0 -14 5 -0.50 2.10 0 14 -5 1.60 3.50 0 -14 -5 -2.20 2.60 0 -14 5 1.70 2.00 0 -14 6 223.28 10.70 0 -14 -6 220.58 11.80 0 -14 6 230.28 12.00 0 14 -6 235.08 13.80 0 -14 7 -4.30 3.30 0 14 -7 5.00 4.50 0 -14 7 0.20 2.40 0 -14 -7 -2.20 3.50 0 14 -8 453.75 23.00 0 -14 -8 442.26 20.60 0 -14 8 449.95 20.80 0 -14 8 486.65 19.70 0 -14 9 -9.60 3.50 0 -14 -9 -0.10 4.10 0 -14 9 -0.20 3.00 0 14 -9 -8.40 4.20 0 14 -10 7.10 6.00 0 -14 10 14.80 5.80 0 -14 10 16.20 4.70 0 -14 -10 8.40 5.40 0 -14 -11 -6.80 4.70 0 -14 11 2.00 4.20 0 -14 11 -1.40 4.90 0 14 -11 -5.70 5.10 -1 -14 0 1.10 1.40 -1 -14 0 -0.50 1.40 -1 14 0 -1.30 0.80 1 -14 0 -2.40 1.40 1 -14 0 -1.00 1.30 1 -14 0 -3.30 1.40 1 14 0 -0.80 1.00 1 -14 1 100.49 5.60 -1 -14 -1 91.39 5.10 -1 14 1 97.19 4.60 1 14 -1 95.89 4.10 -1 -14 -1 95.79 4.70 1 -14 1 95.09 5.50 1 -14 1 85.39 4.20 -1 -14 1 94.99 5.40 1 -14 -1 85.39 4.90 1 14 1 96.59 4.60 -1 14 -1 100.29 6.90 1 -14 -1 98.19 5.80 -1 14 -1 94.19 4.00 -1 -14 1 92.29 5.10 1 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2.80 -8 -14 -4 59.59 3.60 8 -14 4 69.09 6.50 8 -14 4 60.49 3.50 8 14 -4 67.09 4.10 8 -14 -4 63.09 5.40 -8 -14 4 59.59 5.90 -8 -14 4 56.59 2.70 8 -14 5 42.90 5.50 8 14 -5 43.00 3.50 -8 14 5 43.80 5.00 8 -14 5 40.20 2.90 -8 -14 -5 42.60 2.60 -8 -14 5 41.30 2.90 -8 -14 5 41.70 6.10 8 -14 -5 46.40 5.50 -8 14 6 6.90 2.80 8 -14 6 9.70 3.90 8 14 -6 5.50 2.00 8 -14 -6 8.10 3.60 -8 -14 6 1.90 3.80 8 -14 7 29.90 5.40 8 -14 -7 22.70 4.80 -8 -14 7 33.40 6.00 8 -14 8 1.50 3.90 -8 -14 8 2.90 4.30 8 -14 -8 1.20 3.80 8 -14 9 -4.00 3.80 8 14 -9 1.90 4.90 -8 -14 9 5.40 4.70 8 -14 -9 -3.50 3.70 8 14 -10 26.80 8.00 8 -14 10 28.20 6.40 8 -14 -10 52.69 7.60 -8 -14 10 36.40 7.10 9 14 0 -0.10 1.00 9 -14 0 -1.20 2.50 9 -14 0 0.10 1.60 -9 -14 0 -1.20 2.00 9 -14 1 40.20 3.60 9 -14 1 38.40 4.80 -9 -14 -1 37.00 4.20 -9 -14 1 39.90 4.90 9 -14 -1 42.00 5.00 9 14 1 41.70 3.00 9 -14 -1 36.60 3.80 9 -14 2 199.88 8.70 9 -14 2 199.68 10.60 -9 -14 -2 191.28 9.10 9 -14 -2 209.18 10.70 -9 -14 2 207.78 10.40 9 -14 -2 226.58 9.70 9 -14 3 17.90 4.10 9 -14 3 18.70 2.50 9 14 -3 20.20 2.90 -9 -14 -3 19.10 3.00 9 -14 -3 21.00 4.10 -9 -14 3 20.30 4.20 9 -14 -3 18.40 3.60 9 -14 4 38.20 3.20 -9 -14 -4 36.30 3.30 9 14 -4 43.00 3.70 9 -14 4 33.70 5.10 9 -14 -4 38.80 4.80 -9 -14 4 36.00 5.50 9 -14 5 118.89 5.80 9 14 -5 123.49 6.30 9 -14 5 124.19 8.60 -9 14 5 119.99 7.80 -9 -14 -5 120.89 5.70 -9 -14 5 131.39 8.80 9 -14 -5 128.29 8.10 9 14 -6 44.10 3.80 -9 14 6 51.69 4.90 9 -14 6 45.60 6.10 -9 -14 6 56.29 7.10 9 -14 -6 51.69 5.90 9 -14 7 37.10 6.00 9 14 -7 45.00 5.50 -9 -14 7 48.90 7.00 9 -14 -7 37.10 5.70 9 -14 8 -7.70 3.60 -9 -14 8 4.50 4.30 9 -14 -8 -1.70 3.60 9 14 -9 8.70 5.50 9 -14 9 4.90 4.70 9 -14 -9 4.70 4.50 -9 -14 9 5.40 4.70 9 14 -10 0.10 6.50 9 -14 10 7.90 5.20 9 14 10 -8.40 4.20 -9 -14 10 1.10 4.40 9 -14 -10 2.80 4.60 10 -14 0 38.10 3.80 10 -14 0 40.80 5.20 10 14 0 38.60 2.10 10 14 0 41.10 2.30 -10 -14 0 47.10 5.10 -10 -14 -1 206.68 10.20 10 -14 1 227.18 9.60 10 -14 1 214.38 10.90 10 14 1 225.48 8.90 -10 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9.00 5.30 10 -14 -10 10.20 5.40 10 14 10 -0.90 4.30 11 14 0 0.50 0.70 11 -14 0 -1.90 1.70 11 14 0 0.80 0.80 11 -14 0 -3.10 2.80 -11 -14 0 2.50 2.80 -11 -14 -1 56.29 5.60 11 -14 1 47.30 4.10 11 -14 1 43.10 5.60 11 14 1 53.69 3.10 -11 -14 1 44.20 5.60 11 -14 -1 49.99 5.80 11 14 1 51.29 3.30 11 -14 -1 51.89 4.40 -11 -14 -2 212.88 10.50 11 -14 2 218.88 11.80 11 -14 2 221.38 9.80 11 14 2 231.68 9.20 11 -14 -2 221.18 11.60 11 -14 -2 214.88 10.60 -11 -14 2 226.88 11.70 -11 -14 -3 22.90 3.90 11 -14 3 21.20 4.30 11 -14 3 25.80 3.10 11 14 -3 15.90 3.20 -11 -14 3 18.50 4.80 11 -14 -3 22.70 3.90 11 -14 -3 20.00 4.40 11 14 3 16.50 2.70 -11 -14 -4 0.00 2.60 11 -14 4 -0.30 1.90 11 -14 4 -1.00 2.60 11 14 -4 -0.70 2.10 11 -14 -4 -3.00 2.60 -11 -14 4 0.90 3.70 -11 -14 -5 0.60 2.30 -11 14 5 0.20 3.70 11 -14 5 3.40 2.00 11 -14 5 2.60 3.60 11 14 -5 -2.20 1.90 11 -14 -5 -0.70 3.00 11 14 5 -0.40 2.10 -11 -14 5 1.30 3.60 -11 14 6 15.90 4.20 11 14 -6 12.70 2.80 11 -14 6 14.60 4.70 11 -14 -6 16.80 4.50 -11 -14 6 23.90 5.40 11 14 6 15.90 3.70 11 -14 7 5.00 4.30 -11 14 7 13.10 4.20 11 14 -7 14.00 3.10 11 -14 -7 12.10 4.30 11 14 7 6.60 3.60 -11 -14 7 10.90 4.90 11 -14 8 -5.50 3.90 -11 -14 8 1.70 4.80 11 -14 -8 4.10 4.10 11 14 8 3.40 3.70 11 -14 9 22.00 6.10 -11 -14 9 17.50 5.90 11 14 9 17.60 4.80 11 -14 -9 21.10 6.00 11 -14 10 6.60 5.60 11 14 -10 -0.70 6.00 -11 -14 10 1.80 4.80 11 -14 -10 8.10 5.30 11 14 10 0.30 4.30 -12 -14 0 140.79 8.30 12 -14 0 142.39 7.50 12 -14 0 131.99 8.80 12 14 0 135.99 5.10 12 -14 1 147.89 9.30 12 -14 1 139.99 7.60 -12 -14 -1 153.08 8.50 -12 -14 1 147.59 8.90 12 -14 -1 138.79 7.80 12 -14 -1 167.38 9.60 12 14 1 144.89 6.20 -12 -14 -2 75.49 6.10 12 -14 2 67.69 5.00 12 -14 2 75.49 7.40 -12 -14 2 75.79 6.60 12 14 2 74.49 4.30 12 -14 -2 73.39 6.90 12 -14 -2 72.59 5.70 -12 -14 -3 0.80 3.20 12 14 -3 -3.50 2.40 12 -14 3 1.20 2.20 12 -14 3 6.50 3.80 12 -14 -3 -3.20 2.60 12 14 3 0.50 1.90 -12 -14 3 -1.40 3.60 12 -14 -3 1.90 3.40 12 -14 4 2.20 2.20 12 -14 4 3.00 3.60 -12 -14 -4 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160.78 8.90 14 14 1 179.08 7.40 -14 -14 1 185.58 10.40 14 -14 2 92.49 7.90 -14 -14 -2 89.39 6.70 14 -14 2 76.89 5.80 -14 -14 2 88.99 7.50 14 14 2 89.59 4.80 14 -14 -2 87.59 6.40 14 -14 -2 84.99 7.50 -14 -14 -3 81.59 6.80 14 -14 3 89.79 8.40 14 14 -3 96.19 6.30 14 -14 3 91.19 5.90 14 -14 -3 85.39 7.50 14 14 3 94.19 5.50 14 -14 -3 89.89 6.80 -14 -14 3 96.59 8.00 14 14 -4 1.50 2.70 -14 14 4 -3.30 4.00 14 -14 4 4.30 3.30 -14 -14 -4 5.80 3.60 14 -14 4 4.90 2.40 14 14 4 2.30 2.30 14 -14 -4 -0.30 3.10 -14 -14 4 5.00 4.30 14 -14 5 1.30 3.90 14 14 -5 1.10 2.60 14 -14 5 0.80 2.30 -14 14 5 9.40 4.60 14 14 5 5.60 2.50 -14 -14 5 8.60 4.70 14 -14 -5 -0.60 3.30 -14 14 6 2.30 4.40 14 14 -6 2.50 2.70 14 -14 6 2.30 3.40 14 -14 -6 6.90 4.10 -14 -14 6 0.80 4.30 14 14 6 9.80 3.10 -14 14 7 49.00 6.30 14 14 -7 41.30 5.20 14 -14 7 42.20 7.30 -14 -14 7 52.39 7.90 14 -14 -7 39.70 6.50 14 14 7 41.70 5.60 14 -14 8 16.60 5.90 -14 -14 8 18.10 5.80 14 14 8 18.60 5.10 14 -14 -8 17.20 5.60 14 -14 9 13.30 5.90 14 -14 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14 -6 3.10 2.80 16 14 6 0.50 3.20 -16 -14 6 12.30 5.60 16 -14 -6 2.40 4.20 16 14 -7 44.70 7.60 -16 14 7 54.69 7.50 16 -14 7 47.90 7.20 -16 -14 7 63.59 9.10 16 -14 -7 42.80 7.00 16 14 7 50.09 6.30 16 -14 8 -2.50 4.80 16 14 8 4.60 4.20 16 -14 -8 0.40 4.50 -16 -14 8 16.60 5.90 17 -14 0 2.80 2.80 -17 -14 0 3.10 4.90 17 -14 0 0.30 3.90 17 -14 1 2.90 2.80 17 -14 1 6.60 4.40 -17 -14 -1 17.80 5.70 17 -14 -1 10.00 4.40 17 -14 -1 5.50 3.30 -17 -14 1 13.10 5.20 17 -14 2 3.70 2.60 17 14 -2 -0.30 2.90 -17 -14 -2 -0.20 3.80 17 -14 2 0.30 3.90 17 -14 -2 1.50 3.10 17 -14 -2 -0.50 3.50 -17 -14 2 5.70 4.40 -17 -14 -3 18.90 5.30 17 14 -3 13.00 3.80 17 -14 3 17.00 5.30 17 -14 3 10.60 3.40 -17 -14 3 19.50 5.80 17 -14 -3 20.80 4.60 17 -14 -3 16.00 4.70 17 14 -4 11.70 3.90 -17 -14 -4 18.50 5.10 17 -14 4 21.00 5.60 17 -14 4 19.40 3.90 -17 14 4 15.20 6.30 17 -14 -4 9.30 4.50 17 -14 -4 13.50 4.30 -17 -14 4 15.40 5.70 17 -14 5 23.40 6.00 -17 14 5 16.00 6.10 17 14 -5 23.00 4.30 17 -14 5 28.20 4.50 17 14 5 22.00 4.00 17 -14 -5 30.60 5.60 -17 -14 5 28.60 6.80 17 14 -6 -0.50 3.30 17 -14 6 3.00 4.70 -17 14 6 6.40 5.50 -17 -14 6 4.40 5.20 17 14 6 4.80 3.50 17 -14 -6 5.20 4.40 17 -14 7 1.90 5.10 -17 14 7 13.20 5.40 17 14 7 5.60 3.90 -17 -14 7 12.50 6.30 17 -14 -7 -7.70 3.70 17 -14 8 24.20 6.90 -17 -14 8 35.60 7.70 17 -14 -8 22.60 6.20 17 14 8 28.90 5.50 -18 -14 0 30.10 6.40 18 -14 0 25.60 5.50 18 -14 0 29.50 5.10 -18 -14 -1 12.70 5.50 18 -14 1 17.90 4.20 18 -14 1 11.90 4.80 -18 -14 1 24.50 5.90 18 -14 -1 16.30 4.40 18 -14 -1 14.30 4.70 -18 -14 -2 7.30 4.90 18 -14 2 -1.30 3.90 18 14 -2 -2.20 2.90 18 -14 2 0.80 2.80 -18 -14 2 2.70 4.60 18 -14 -2 -2.20 3.40 18 -14 -2 1.10 3.70 18 14 -3 13.10 3.90 18 -14 3 12.10 5.10 18 -14 3 11.00 3.70 -18 -14 -3 17.30 5.50 18 -14 -3 7.50 4.40 -18 -14 3 16.70 5.50 18 -14 -3 11.10 4.10 18 -14 4 6.30 5.00 18 14 -4 10.70 3.90 -18 14 4 6.20 6.20 -18 -14 -4 10.00 5.10 18 -14 4 7.90 3.40 18 -14 -4 4.20 4.40 18 -14 -4 3.50 3.90 -18 -14 4 11.50 5.40 18 14 -5 75.29 6.60 -18 14 5 75.39 10.40 18 -14 5 79.39 9.10 -18 -14 5 86.79 10.40 18 -14 -5 70.09 8.00 18 14 -6 8.20 3.80 -18 14 6 5.20 5.80 18 -14 6 8.70 5.50 18 -14 -6 11.90 4.90 -18 -14 6 7.00 5.60 18 14 6 16.90 6.10 -18 14 7 9.80 7.30 18 -14 7 4.70 5.60 18 -14 -7 -3.80 4.30 -18 -14 7 5.10 5.20 18 14 7 6.40 3.80 19 -14 0 1.30 3.50 19 -14 0 -2.90 3.80 -19 -14 0 4.00 4.60 19 -14 1 7.20 3.70 -19 -14 -1 12.10 5.00 19 -14 1 4.10 4.50 -19 -14 1 13.70 5.30 19 -14 -1 12.50 4.60 19 -14 -1 6.30 3.60 19 -14 2 2.80 3.00 19 -14 2 2.20 4.30 19 14 -2 7.00 4.30 -19 -14 -2 7.70 5.30 19 -14 -2 8.00 3.90 -19 -14 2 6.80 4.90 19 -14 -2 2.20 4.20 -19 -14 -3 13.60 5.50 19 -14 3 4.70 4.80 19 14 -3 6.80 3.60 19 -14 3 2.10 3.50 19 -14 -3 1.70 4.30 19 -14 -3 2.30 3.80 -19 -14 3 13.00 5.70 -19 14 4 3.00 7.40 19 -14 4 15.90 5.60 19 -14 4 15.70 4.20 -19 -14 -4 15.90 5.70 19 14 -4 12.60 4.40 19 -14 -4 16.10 4.80 -19 -14 4 20.00 6.50 19 14 -5 -3.40 2.90 -19 14 5 -1.60 5.60 19 -14 5 2.10 5.00 -19 -14 5 3.90 5.40 19 -14 -5 5.50 4.90 19 -14 6 39.50 7.80 -19 14 6 52.79 9.10 19 14 -6 44.50 5.90 -19 -14 6 67.19 9.60 19 -14 -6 60.39 7.80 20 -14 0 19.20 5.60 20 -14 0 21.00 4.90 -20 -14 0 32.10 7.00 20 -14 1 13.90 5.40 -20 -14 -1 25.30 6.30 20 -14 1 16.90 4.20 20 -14 -1 4.10 4.50 -20 -14 1 21.40 6.60 20 -14 -1 16.30 4.40 -20 -14 -2 25.30 6.60 20 -14 2 17.00 5.60 20 -14 2 20.50 4.70 20 14 -2 22.40 5.10 20 -14 -2 13.70 5.10 20 -14 -2 18.80 4.70 -20 -14 2 23.90 6.60 -20 -14 -3 2.80 5.10 20 -14 3 -7.60 3.30 20 -14 3 -1.10 5.10 20 14 -3 0.10 3.70 20 -14 -3 -5.00 3.90 20 -14 -3 -4.10 3.70 -20 -14 3 2.50 5.20 20 -14 4 -2.00 4.60 20 14 -4 1.70 3.30 -20 14 4 0.10 7.30 20 -14 4 0.40 3.30 -20 -14 4 12.90 6.40 20 -14 -4 1.50 4.00 -20 14 5 -5.20 6.80 20 -14 5 0.70 4.90 20 14 -5 3.00 3.90 -20 -14 5 13.00 6.20 20 -14 -5 -4.70 3.80 -20 14 6 12.40 7.00 20 14 -6 11.50 4.20 20 -14 6 17.00 6.30 20 -14 -6 7.40 5.20 -20 -14 6 20.80 7.10 -21 -14 0 7.90 5.80 21 -14 0 -0.90 4.30 21 -14 0 -3.70 3.60 -21 -14 -1 8.30 5.40 21 -14 1 1.00 4.50 21 -14 1 10.80 4.10 21 -14 -1 13.40 4.50 21 -14 -1 11.40 5.50 -21 -14 1 10.00 5.80 21 -14 2 1.60 3.30 21 14 -2 -1.70 3.40 21 -14 2 -4.30 4.10 -21 -14 -2 4.30 5.00 21 -14 -2 -6.40 3.50 -21 -14 2 2.20 5.10 21 -14 -2 -7.50 4.00 -21 -14 -3 95.69 9.70 21 14 -3 100.59 9.10 21 -14 3 96.09 8.10 -21 14 3 89.09 12.10 21 -14 3 101.29 10.20 21 -14 -3 82.09 8.90 -21 -14 3 107.89 10.20 21 -14 -3 74.89 8.40 21 -14 4 2.30 5.20 -21 14 4 -10.30 7.60 21 -14 4 -0.50 3.20 21 14 -4 -0.70 4.10 21 -14 -4 -3.40 4.00 -21 -14 4 7.80 6.00 -21 14 5 8.60 7.00 21 -14 5 5.70 5.30 21 14 -5 8.30 4.40 21 -14 -5 5.90 5.30 -21 -14 5 11.90 6.10 22 -14 0 68.69 8.40 -22 -14 0 83.29 10.00 22 -14 0 71.29 7.80 22 -14 1 3.00 4.90 22 14 -1 -3.90 3.50 22 -14 1 -5.30 3.60 -22 -14 -1 0.80 5.60 22 -14 -1 -1.40 4.20 22 -14 -1 -1.30 3.60 -22 -14 1 -0.60 5.00 22 14 -2 31.80 5.70 -22 -14 -2 33.20 7.20 22 -14 2 19.50 5.10 22 -14 2 35.90 7.10 22 -14 -2 29.20 6.40 22 -14 -2 25.00 5.70 -22 -14 2 33.40 7.50 -22 14 3 5.10 7.70 22 -14 3 7.10 4.30 22 14 -3 5.40 4.60 22 -14 3 5.00 5.30 -22 -14 -3 10.00 6.20 22 -14 -3 1.30 4.60 22 -14 -3 7.30 4.80 -22 -14 3 14.40 6.30 22 14 -4 23.10 5.60 22 -14 4 17.80 5.60 -22 14 4 22.60 9.80 22 -14 4 18.90 6.50 22 -14 -4 23.90 6.00 -22 -14 4 30.80 7.40 -23 -14 0 11.30 5.80 23 -14 0 -1.30 4.60 23 -14 0 -0.80 3.60 -23 -14 -1 22.60 7.10 23 -14 1 0.40 3.80 23 14 -1 3.70 4.30 23 -14 1 5.60 5.20 -23 -14 1 17.10 6.90 23 -14 -1 3.60 4.10 23 -14 -1 6.10 5.00 23 14 -2 0.30 4.00 23 -14 2 -2.70 5.70 -23 -14 -2 5.50 6.20 23 -14 2 -9.50 3.00 23 -14 -2 6.40 4.90 23 -14 -2 1.90 4.70 -23 -14 2 10.40 6.00 0 15 0 0.40 1.00 0 -15 0 -0.80 1.50 0 -15 0 1.60 1.70 0 -15 0 1.00 1.40 0 -15 1 6.40 2.10 0 -15 -1 9.80 2.30 0 -15 -1 8.40 1.90 0 -15 1 7.20 2.00 0 15 -1 7.60 1.20 0 -15 -1 4.40 2.00 0 15 1 9.80 1.70 0 15 2 2.40 1.10 0 -15 2 -2.00 1.80 0 -15 2 1.50 1.70 0 -15 -2 -4.60 1.60 0 15 3 59.59 2.70 0 -15 3 58.19 4.30 0 15 -3 59.39 6.70 0 -15 -3 58.79 5.20 0 -15 3 54.69 4.80 0 -15 -4 -3.50 2.20 0 15 -4 4.10 3.60 0 -15 4 1.50 2.10 0 -15 4 -2.90 2.30 0 15 -5 12.10 4.60 0 -15 5 11.40 2.90 0 -15 5 11.80 3.80 0 -15 -5 8.60 3.60 0 -15 -6 2.70 3.40 0 -15 6 5.50 3.00 0 -15 6 1.90 3.50 0 15 -6 6.20 4.70 0 15 -7 1.60 4.70 0 -15 7 10.00 4.00 0 -15 7 10.60 3.10 0 -15 -7 5.30 4.10 0 -15 8 3.90 3.20 0 15 -8 -1.60 4.80 0 -15 -8 9.60 4.60 0 -15 8 8.60 4.50 0 -15 -9 23.30 6.00 0 15 -9 36.10 8.20 0 -15 9 26.70 4.60 0 -15 9 29.30 6.50 0 -15 10 1.10 3.30 0 15 -10 -7.70 6.00 0 -15 10 -0.50 4.60 0 -15 -10 -4.30 4.60 0 -15 -11 16.30 6.40 0 -15 11 6.10 4.00 0 15 -11 6.50 7.60 0 -15 11 7.40 5.80 -1 -15 0 -0.10 1.60 1 -15 0 -1.50 1.30 -1 15 0 -1.00 0.90 1 -15 0 -2.30 1.50 1 -15 0 -1.20 1.70 1 15 0 -1.30 1.00 -1 -15 0 -2.80 1.40 -1 15 1 59.89 3.90 1 -15 1 65.19 4.60 1 -15 1 56.79 4.40 1 -15 1 64.39 3.30 -1 -15 -1 54.59 3.50 1 15 -1 59.29 3.00 -1 -15 -1 57.69 4.20 -1 -15 1 52.99 4.10 1 -15 -1 60.29 3.90 1 15 1 58.39 3.50 -1 15 -1 59.09 2.90 -1 -15 1 54.59 4.00 1 -15 -1 59.99 4.50 -1 15 -1 59.79 5.60 -1 -15 -2 56.69 4.80 -1 15 2 72.39 3.60 1 -15 2 63.49 4.60 1 -15 2 64.39 4.80 1 15 -2 70.39 2.90 -1 15 -2 65.19 6.70 -1 -15 2 62.39 4.70 1 15 2 78.89 3.60 1 -15 -2 61.99 4.70 -1 15 -2 75.09 2.80 -1 -15 2 72.99 4.60 1 -15 3 81.19 5.80 1 -15 3 83.39 5.40 -1 -15 -3 88.99 5.90 -1 15 3 98.69 3.80 1 -15 -3 81.79 5.60 -1 15 -3 80.29 7.40 -1 -15 3 89.49 5.20 -1 -15 3 77.39 5.70 1 15 3 84.29 3.60 1 15 -4 3.00 3.60 1 -15 4 -1.30 2.60 1 -15 4 3.20 2.10 -1 -15 -4 4.30 2.80 -1 -15 4 3.30 2.80 -1 -15 4 2.60 2.10 1 -15 -4 3.70 2.60 -1 15 -4 4.50 3.50 1 15 -5 55.19 7.10 -1 15 5 46.40 3.60 1 -15 5 52.39 5.00 -1 -15 -5 44.70 5.60 1 -15 5 43.90 5.80 -1 -15 5 47.70 5.90 1 -15 -5 43.10 5.40 -1 -15 5 52.99 4.30 -1 15 -5 45.30 6.90 1 -15 6 63.39 5.30 -1 -15 -6 58.59 6.60 1 -15 6 58.49 7.00 1 15 -6 56.29 7.80 -1 -15 6 62.49 7.20 -1 -15 6 60.49 5.20 1 -15 -6 57.69 6.50 -1 15 -6 59.89 8.10 1 -15 7 77.99 6.60 -1 -15 -7 78.49 7.90 1 15 -7 69.59 8.90 1 -15 7 72.39 7.10 -1 -15 7 81.49 7.30 -1 15 -7 67.79 8.90 -1 -15 7 74.79 6.10 1 -15 -7 79.49 7.80 1 -15 8 55.19 5.80 1 15 -8 36.60 7.50 1 -15 8 39.70 6.80 -1 -15 -8 38.20 6.40 -1 15 -8 28.70 7.90 -1 -15 8 48.80 7.10 -1 -15 8 42.60 5.10 1 -15 -8 50.59 6.90 1 15 -9 14.70 6.20 1 -15 9 14.30 4.50 1 -15 9 9.50 5.70 -1 -15 -9 17.90 5.50 1 -15 -9 20.20 5.80 -1 15 -9 8.90 6.20 -1 -15 9 17.90 5.50 -1 -15 9 18.30 4.30 1 -15 10 0.60 3.90 -1 -15 -10 0.00 5.00 1 15 -10 -5.50 5.40 1 -15 10 -3.20 4.60 -1 -15 10 6.00 5.00 -1 -15 10 -4.60 3.20 1 -15 -10 0.60 4.80 -1 15 -10 -2.40 5.40 1 15 -11 -0.60 6.80 -1 -15 -11 4.60 5.70 1 -15 11 9.00 6.40 1 -15 11 12.20 5.10 -1 15 -11 9.70 7.50 1 -15 -11 14.70 6.20 -1 -15 11 10.10 4.70 -1 -15 11 11.70 6.00 2 -15 0 17.50 2.80 -2 15 0 17.80 2.00 2 -15 0 17.00 2.90 -2 15 0 19.30 3.60 -2 -15 0 17.60 2.40 -2 -15 0 16.10 2.60 2 -15 0 17.20 2.20 2 -15 1 19.00 3.10 -2 -15 -1 18.40 2.30 2 -15 1 16.30 1.80 -2 15 1 19.20 3.40 2 -15 1 18.30 2.90 2 15 -1 19.70 1.90 2 -15 -1 17.00 2.90 -2 15 -1 20.50 1.70 2 -15 -1 13.00 2.40 2 15 1 23.70 2.50 -2 -15 1 17.40 3.00 -2 15 -1 15.70 3.80 -2 -15 1 14.30 2.30 2 15 -2 31.40 1.90 2 -15 2 31.80 4.10 -2 -15 -2 29.40 2.30 -2 -15 -2 38.00 4.00 2 -15 2 31.80 3.60 -2 15 2 31.70 2.40 -2 15 2 36.90 4.20 2 15 2 32.60 2.40 -2 15 -2 29.80 4.80 -2 -15 2 32.00 4.20 2 -15 -2 29.10 3.40 -2 -15 2 33.70 3.20 2 -15 3 8.50 3.00 2 -15 3 13.70 2.80 -2 -15 -3 7.50 2.80 -2 15 3 10.50 2.60 -2 15 3 16.20 1.70 -2 15 -3 10.00 3.80 2 -15 -3 7.90 2.60 -2 -15 3 12.00 3.40 -2 -15 3 11.60 2.30 -2 15 4 41.40 1.90 2 -15 4 41.60 5.30 2 -15 4 44.40 4.50 -2 -15 -4 40.60 4.90 -2 15 4 34.90 2.10 -2 15 4 40.30 3.60 -2 -15 4 45.70 5.30 2 -15 -4 35.90 4.40 -2 15 -4 32.20 5.80 -2 -15 4 39.90 3.80 2 -15 5 5.70 2.60 -2 15 5 6.00 1.60 -2 -15 -5 6.20 3.40 2 15 -5 2.80 3.80 2 -15 5 3.40 3.30 2 -15 -5 3.80 3.10 -2 15 -5 4.10 4.30 -2 -15 5 9.20 3.80 -2 -15 5 7.80 2.50 2 -15 6 40.90 6.20 -2 -15 -6 47.60 6.10 2 -15 6 39.30 4.80 2 15 -6 43.20 7.00 -2 -15 6 42.30 4.40 -2 -15 6 43.20 6.10 2 -15 -6 40.00 5.50 -2 15 -6 31.80 6.60 2 15 -7 2.10 4.40 -2 -15 -7 1.60 3.90 2 -15 7 2.20 3.90 2 -15 7 0.60 2.60 -2 15 -7 -2.80 4.60 -2 -15 7 0.70 2.70 2 -15 -7 0.80 3.50 -2 -15 7 1.80 3.60 -2 -15 -8 177.78 11.70 2 15 -8 165.78 13.20 2 -15 8 214.98 11.10 2 -15 8 169.58 11.40 -2 -15 8 191.68 12.00 2 -15 -8 179.58 11.40 -2 15 -8 196.48 14.30 -2 -15 8 188.88 9.80 2 -15 9 4.90 3.50 2 15 -9 -3.60 5.60 2 -15 9 2.10 4.50 -2 -15 -9 -1.70 4.40 2 -15 -9 2.50 4.50 -2 15 -9 -2.80 5.60 -2 -15 9 -1.60 3.90 -2 -15 9 2.70 3.20 -2 -15 -10 15.90 6.40 2 -15 10 26.00 5.30 2 -15 10 16.80 6.30 2 15 -10 14.80 7.60 -2 15 -10 21.20 7.40 -2 -15 10 31.30 6.90 2 -15 -10 19.20 6.30 -2 -15 10 30.80 5.20 2 15 -11 -3.00 5.80 2 -15 11 0.00 4.00 2 -15 11 -2.50 5.00 2 -15 -11 -3.10 4.70 -2 -15 11 8.20 6.10 -3 -15 0 -1.80 1.40 3 -15 0 -2.90 1.20 3 -15 0 -1.40 1.80 -3 15 0 -0.70 2.00 -3 15 1 24.30 3.80 3 -15 1 27.10 3.60 -3 -15 -1 28.40 2.80 3 -15 1 26.10 2.20 3 -15 1 25.70 3.50 3 15 -1 24.70 2.10 3 -15 -1 24.90 2.80 3 15 1 27.80 2.60 3 -15 -1 24.20 3.50 -3 -15 1 28.80 3.40 -3 15 -1 28.30 2.00 -3 15 -1 28.50 4.40 -3 -15 1 27.30 2.70 3 -15 2 3.90 1.10 -3 -15 -2 7.40 1.50 3 15 -2 9.40 1.30 -3 15 2 12.40 1.80 3 -15 2 5.40 2.70 3 -15 2 6.00 2.40 -3 15 2 10.60 2.80 3 -15 -2 4.60 2.50 -3 -15 2 8.00 2.70 -3 -15 2 8.60 1.90 3 15 2 6.00 1.70 -3 15 -2 7.20 3.40 3 -15 -2 4.30 2.20 3 -15 3 27.90 3.70 3 -15 3 27.40 4.30 3 15 -3 27.30 1.70 3 15 -3 26.80 1.70 -3 15 3 28.00 3.60 -3 15 3 30.30 2.20 -3 15 -3 37.90 5.80 -3 -15 3 33.20 4.40 -3 -15 3 30.40 3.00 3 -15 -3 30.70 3.80 -3 15 4 34.90 2.10 -3 15 4 29.90 2.70 3 -15 4 34.10 4.40 -3 15 4 36.40 3.50 3 -15 4 32.00 4.80 -3 -15 -4 35.10 4.80 -3 -15 4 40.90 5.10 3 -15 -4 36.70 4.40 -3 -15 4 39.80 3.60 -3 15 -4 41.10 6.70 -3 -15 -5 131.39 8.30 -3 15 5 119.19 4.40 3 -15 5 128.99 7.50 3 -15 5 122.89 8.10 -3 15 5 113.39 4.40 -3 -15 5 109.69 7.80 3 -15 -5 108.59 7.50 -3 -15 5 124.69 6.50 -3 15 -5 112.69 9.70 -3 -15 -6 36.80 5.90 3 -15 6 47.10 5.40 3 -15 6 38.50 6.10 3 15 -6 35.70 6.50 -3 -15 6 46.80 4.40 3 -15 -6 44.60 5.70 -3 15 -6 37.60 7.20 -3 -15 6 40.60 6.00 3 -15 7 14.10 4.10 -3 -15 -7 19.80 5.20 3 -15 7 8.70 4.50 3 15 -7 15.00 5.40 3 -15 -7 13.20 4.40 -3 -15 7 20.20 5.00 -3 -15 7 9.10 2.90 -3 15 -7 12.50 6.00 3 -15 8 5.80 4.80 3 -15 8 3.20 3.40 -3 -15 -8 -5.80 3.90 3 15 -8 0.30 5.50 -3 -15 8 5.50 4.30 -3 15 -8 -2.30 5.20 3 -15 -8 4.00 4.00 -3 -15 8 7.20 3.10 3 -15 9 3.60 4.10 3 -15 9 0.90 4.90 3 15 -9 -8.10 4.30 -3 -15 -9 -3.40 4.40 -3 15 -9 2.60 5.60 3 -15 -9 1.20 4.30 -3 -15 9 2.20 3.10 -3 -15 9 3.60 4.50 3 15 -10 30.60 8.50 3 -15 10 44.80 6.40 3 -15 10 38.60 8.10 3 -15 -10 41.70 7.50 -3 -15 10 38.60 7.50 -3 -15 10 39.60 6.20 3 15 -11 42.00 9.50 3 -15 11 52.79 7.60 3 -15 11 41.60 8.30 -3 -15 11 48.80 8.20 3 -15 -11 49.40 8.90 -4 15 0 105.49 7.20 -4 -15 0 103.99 5.50 4 -15 0 94.49 6.20 4 -15 0 103.49 5.00 -4 15 1 148.09 8.40 -4 -15 -1 140.89 6.40 4 15 -1 140.29 6.20 4 -15 1 145.69 7.70 4 15 -1 141.09 6.20 4 -15 1 129.89 5.90 4 -15 -1 139.09 6.60 -4 -15 1 132.39 7.00 -4 15 -1 143.29 5.90 -4 -15 1 135.49 6.20 -4 15 -1 140.99 8.90 4 -15 -1 136.59 7.70 -4 15 2 128.79 7.40 4 -15 2 123.69 7.20 4 15 -2 132.99 5.60 4 -15 2 115.39 5.00 4 15 -2 126.29 5.50 4 -15 2 121.69 7.20 -4 -15 -2 122.39 5.50 4 -15 -2 125.09 7.00 -4 -15 2 121.39 6.90 4 15 2 127.29 6.00 4 -15 -2 122.69 6.50 -4 -15 2 128.59 5.80 -4 15 -2 137.19 9.10 4 -15 3 15.10 3.80 -4 15 3 19.90 2.30 4 -15 3 15.50 3.20 4 15 -3 20.40 2.00 4 15 -3 21.60 1.90 4 15 -3 19.40 1.80 -4 -15 -3 15.40 1.50 -4 15 3 19.00 3.10 -4 -15 3 19.30 3.70 -4 -15 3 19.40 2.30 4 -15 -3 12.00 3.10 -4 15 -3 22.00 4.70 4 15 -4 41.70 2.20 4 -15 4 47.50 4.90 4 -15 4 44.80 5.60 -4 15 4 41.10 2.80 -4 15 -4 45.60 6.50 4 -15 -4 49.60 4.90 -4 -15 4 45.20 5.40 -4 -15 4 42.00 3.60 -4 15 5 25.90 2.40 4 -15 5 19.90 3.80 4 15 -5 21.70 1.60 4 -15 5 23.70 4.90 4 -15 -5 26.20 4.30 -4 -15 5 27.80 4.90 -4 15 -5 27.30 5.90 -4 -15 5 29.40 3.20 4 -15 6 18.10 5.10 4 -15 6 19.40 4.00 -4 -15 6 20.80 4.90 -4 15 -6 17.80 6.30 -4 -15 6 17.40 3.00 4 -15 -6 23.00 4.50 4 -15 7 11.00 3.80 4 -15 7 16.60 5.20 4 15 -7 6.70 5.10 -4 15 -7 9.40 5.70 -4 -15 7 12.70 4.40 -4 -15 7 10.50 2.80 4 -15 -7 12.60 4.30 4 -15 8 6.30 3.60 4 15 -8 8.50 5.60 4 -15 8 2.90 4.60 -4 -15 8 -1.90 3.80 -4 15 -8 -0.70 5.50 4 -15 -8 8.00 4.30 -4 -15 8 -2.30 2.50 4 15 -9 -5.70 5.40 4 -15 9 0.80 3.60 4 -15 9 -1.60 4.60 -4 -15 9 3.00 4.30 4 -15 -9 3.30 4.20 -4 -15 9 3.80 3.00 -4 15 -9 0.30 5.50 4 -15 10 18.40 5.60 4 15 -10 7.00 6.10 4 -15 10 7.60 5.70 -4 -15 10 12.80 5.70 4 -15 -10 16.70 5.70 4 15 -11 -1.40 6.50 4 -15 11 -1.50 4.20 4 -15 11 7.00 5.80 -4 -15 11 4.90 5.20 4 -15 -11 -6.30 4.60 5 -15 0 1.90 2.40 5 -15 0 -2.80 1.30 -5 -15 0 -0.10 1.80 -5 15 0 0.50 2.60 5 15 0 0.10 1.30 5 -15 1 86.89 4.40 -5 15 1 99.79 6.60 5 -15 1 80.09 5.60 5 15 -1 90.59 4.40 -5 -15 -1 82.69 4.80 5 -15 -1 91.69 6.30 -5 15 -1 96.59 7.30 -5 15 -1 98.89 4.40 -5 -15 1 85.89 5.40 5 -15 -1 93.69 5.00 5 15 -2 4.30 1.40 5 -15 2 9.50 3.00 -5 -15 -2 6.40 1.70 5 15 -2 5.10 1.30 -5 15 2 9.50 2.70 5 -15 2 6.60 1.30 5 -15 -2 5.80 2.90 5 15 2 9.10 2.40 -5 -15 2 6.90 2.80 -5 15 -2 6.20 3.50 -5 -15 2 7.60 1.60 5 -15 -2 5.90 2.20 -5 -15 -3 153.78 6.00 5 15 -3 152.48 6.30 5 15 -3 150.68 6.10 5 -15 3 147.19 5.70 5 -15 3 140.79 8.20 -5 -15 3 151.28 8.30 -5 -15 3 148.79 6.50 5 -15 -3 151.18 8.00 -5 15 -3 144.39 10.30 -5 15 4 24.30 2.40 5 15 -4 27.50 2.10 5 -15 4 26.40 4.80 5 -15 4 18.50 3.70 -5 -15 4 30.70 4.70 5 -15 -4 19.50 3.60 -5 15 -4 32.10 6.00 -5 -15 4 24.60 2.60 5 15 -5 70.79 3.40 5 -15 5 71.69 6.10 -5 15 5 74.49 4.40 5 -15 5 62.19 6.40 -5 -15 5 65.39 4.50 -5 15 -5 76.59 8.70 5 -15 -5 69.09 5.90 -5 -15 5 62.79 6.10 5 -15 6 5.50 3.30 5 -15 6 0.00 3.80 -5 15 -6 -6.60 4.60 -5 -15 6 3.60 3.70 -5 -15 6 -3.30 1.90 5 -15 -6 3.20 3.40 5 -15 7 -2.80 3.00 5 -15 7 -4.20 3.60 5 15 -7 0.80 4.30 -5 -15 7 -0.30 3.60 -5 -15 7 -0.50 2.00 -5 15 -7 -0.30 4.90 5 -15 -7 0.80 3.40 5 15 -8 48.30 8.40 5 -15 8 46.90 6.20 5 -15 8 56.09 8.10 -5 -15 8 47.80 4.90 5 -15 -8 52.79 6.80 -5 15 -8 47.90 8.80 -5 -15 8 62.69 7.70 5 -15 9 20.90 5.00 5 15 -9 15.00 6.20 5 -15 9 39.30 7.40 -5 -15 9 37.70 6.80 5 -15 -9 27.20 5.90 5 15 -10 22.30 7.60 5 -15 10 39.70 6.40 5 -15 10 32.50 7.60 5 -15 -10 35.80 6.70 -5 -15 10 36.50 7.20 5 15 -11 -7.70 6.20 5 -15 11 -4.20 4.10 -5 -15 11 2.60 5.10 5 -15 -11 -0.80 5.10 -6 15 0 582.44 23.40 6 15 0 538.35 20.20 -6 -15 0 554.24 21.10 6 -15 0 538.95 20.40 6 -15 0 550.64 22.10 6 -15 1 272.87 11.10 -6 15 1 291.77 13.50 6 15 -1 290.97 10.80 6 -15 1 298.67 13.10 -6 -15 -1 282.47 11.70 -6 -15 1 282.77 12.40 6 -15 -1 278.57 11.70 -6 15 -1 286.37 14.50 6 -15 -1 291.87 13.00 6 -15 2 123.69 7.60 6 -15 2 120.09 5.30 6 15 -2 130.29 5.10 -6 -15 -2 122.59 5.80 -6 15 -2 121.59 8.90 -6 -15 2 125.19 5.30 -6 -15 2 120.19 7.00 6 -15 -2 113.29 7.50 6 -15 -2 122.19 6.60 -6 -15 -3 22.00 2.20 6 -15 3 18.10 3.70 6 15 -3 21.10 2.20 6 15 -3 20.90 1.60 6 -15 3 20.30 1.70 -6 15 -3 10.70 4.50 -6 -15 3 23.00 2.10 6 -15 -3 21.70 3.40 -6 -15 3 22.90 4.10 6 -15 4 62.69 6.20 -6 -15 -4 67.69 2.90 6 15 -4 74.29 3.80 6 -15 4 65.59 2.90 6 -15 -4 72.49 5.50 -6 -15 4 67.29 3.90 -6 15 -4 64.29 7.90 -6 -15 4 64.79 5.90 6 -15 5 30.40 4.70 6 15 -5 30.70 2.50 -6 15 5 39.80 4.00 -6 15 -5 34.80 6.90 6 -15 -5 33.80 4.70 -6 -15 5 32.00 5.30 -6 -15 5 37.10 3.30 6 -15 6 31.70 5.00 -6 15 6 27.20 3.00 6 15 -6 30.10 2.60 -6 -15 6 25.70 5.30 -6 15 -6 26.10 7.00 6 -15 -6 33.20 5.10 -6 -15 6 27.50 3.30 6 -15 7 4.90 3.70 6 -15 7 9.70 4.90 6 -15 -7 6.10 3.90 -6 -15 7 6.50 2.50 -6 15 -7 10.20 5.80 -6 -15 7 8.00 4.30 6 15 -8 2.10 4.80 6 -15 8 8.40 4.10 6 -15 -8 9.40 4.50 -6 -15 8 15.10 5.10 6 -15 9 4.90 4.20 6 15 -9 4.80 6.00 -6 -15 9 14.40 5.30 6 -15 -9 12.60 4.80 6 15 -10 8.40 6.90 6 -15 10 13.90 5.20 -6 -15 10 16.90 5.90 6 -15 -10 12.90 5.40 7 15 0 -0.10 1.20 7 -15 0 0.70 2.70 7 -15 0 -2.70 1.60 -7 15 0 6.30 3.10 -7 -15 0 -3.30 1.80 7 -15 1 7.30 3.10 7 15 -1 11.30 1.50 7 -15 1 11.70 2.00 -7 -15 -1 6.30 2.40 -7 15 -1 16.90 4.10 -7 -15 1 9.70 3.20 7 -15 -1 15.10 2.60 7 -15 -1 7.30 2.70 7 15 -2 573.14 19.80 7 -15 2 553.94 20.50 7 -15 2 601.34 23.00 -7 -15 -2 567.14 21.00 7 -15 -2 558.44 22.70 -7 15 -2 564.14 24.70 -7 -15 2 549.54 22.30 7 -15 -2 554.24 21.60 7 -15 3 62.99 6.00 7 15 -3 60.79 3.80 -7 -15 -3 61.49 3.60 7 -15 3 57.49 3.20 7 -15 -3 57.29 5.00 7 -15 -3 52.99 4.70 -7 15 -3 54.69 7.50 -7 -15 3 57.89 2.90 -7 -15 3 62.99 5.40 -7 -15 -4 74.79 3.70 7 -15 4 84.79 6.70 7 -15 4 82.99 3.70 7 15 -4 74.79 4.20 -7 -15 4 77.59 6.40 7 -15 -4 81.19 6.30 -7 15 -4 82.89 9.70 -7 -15 4 77.39 3.90 7 -15 5 28.80 2.10 7 15 -5 31.40 2.80 -7 15 5 26.30 4.00 7 -15 5 33.50 4.90 -7 -15 5 33.90 5.50 -7 15 -5 24.90 6.30 7 -15 -5 26.40 4.50 -7 -15 5 24.10 2.60 7 -15 6 12.70 4.10 7 15 -6 13.20 2.10 -7 15 6 15.70 2.80 -7 -15 6 11.40 2.40 7 -15 -6 17.60 4.20 -7 -15 6 14.70 4.60 7 -15 7 26.20 5.10 7 -15 -7 38.20 5.70 -7 -15 7 29.40 5.70 7 -15 8 2.30 3.80 7 -15 -8 6.90 4.20 -7 -15 8 4.30 4.30 7 -15 9 45.90 6.90 7 15 -9 45.80 9.00 7 -15 -9 44.80 6.90 -7 -15 9 56.39 8.00 7 15 -10 26.70 7.90 7 -15 10 23.90 6.10 7 -15 -10 34.00 6.80 -7 -15 10 31.70 6.80 8 15 0 70.69 3.60 8 -15 0 69.29 4.40 -8 -15 0 67.89 4.80 8 -15 0 63.79 6.10 -8 -15 -1 241.98 10.50 8 15 -1 246.98 8.90 8 -15 1 231.28 9.90 8 -15 1 237.78 11.80 8 -15 -1 243.48 11.80 8 -15 -1 240.48 10.40 -8 -15 1 240.68 11.10 -8 -15 -2 4.20 2.10 8 -15 2 1.90 2.90 8 -15 2 4.70 1.60 8 -15 -2 7.40 2.40 8 -15 -2 1.80 2.30 -8 -15 2 4.50 3.20 8 15 -3 109.19 5.50 8 -15 3 101.49 4.90 -8 -15 -3 101.39 5.30 8 -15 3 114.99 7.60 -8 -15 3 93.39 6.90 8 -15 -3 116.39 6.70 8 -15 -3 110.49 7.60 8 -15 4 71.39 3.70 8 15 -4 73.79 4.30 8 -15 4 79.59 6.70 -8 -15 -4 65.39 3.70 -8 -15 4 67.39 6.30 8 -15 -4 68.09 5.70 -8 -15 4 67.29 3.00 8 15 -5 9.20 2.10 8 -15 5 16.60 4.30 -8 15 5 8.60 3.40 8 -15 5 11.10 1.70 -8 -15 5 13.60 4.30 8 -15 -5 9.70 3.60 8 15 -6 1.80 1.80 8 -15 6 2.10 3.60 -8 15 6 7.20 2.70 8 -15 -6 8.20 3.70 -8 -15 6 6.00 4.00 8 -15 7 12.30 4.30 8 -15 -7 11.90 4.10 -8 -15 7 8.30 4.50 8 -15 8 27.90 5.70 -8 -15 8 35.60 6.50 8 -15 -8 33.00 5.90 8 15 -9 26.50 7.40 8 -15 9 25.30 6.00 -8 -15 9 29.90 6.60 8 -15 -9 34.30 6.40 8 -15 10 0.40 4.70 8 15 -10 1.50 6.40 -8 -15 10 2.40 4.80 8 -15 -10 3.80 5.00 9 -15 0 -2.60 2.60 9 15 0 -0.60 1.10 -9 -15 0 -0.30 2.60 9 -15 0 -1.70 1.80 9 -15 1 9.00 2.20 -9 -15 -1 7.50 2.80 9 -15 1 6.20 3.20 9 15 1 12.40 1.90 9 -15 -1 8.90 2.40 9 -15 -1 5.90 3.20 -9 -15 1 10.70 3.30 -9 -15 -2 94.79 5.50 9 -15 2 89.39 5.00 9 -15 2 110.49 7.60 -9 -15 2 94.99 6.60 9 -15 -2 100.59 6.80 9 -15 -2 93.09 5.90 9 15 -3 16.80 2.60 -9 -15 -3 11.80 2.50 9 -15 3 14.00 2.10 9 -15 3 7.90 3.80 9 -15 -3 10.80 3.70 -9 -15 3 12.40 4.30 9 -15 -3 6.80 3.20 -9 -15 -4 8.70 2.10 9 -15 4 10.00 1.80 9 15 -4 9.30 2.20 9 -15 4 6.70 3.70 9 -15 -4 0.80 2.80 -9 -15 4 6.40 3.90 -9 15 5 6.60 3.70 9 -15 5 8.70 1.90 9 -15 5 6.00 3.20 9 15 -5 10.20 2.20 -9 -15 5 15.50 4.50 9 -15 -5 7.30 3.50 9 -15 6 3.70 3.70 -9 15 6 6.80 2.90 9 15 -6 2.70 1.90 -9 -15 6 7.00 4.10 9 -15 -6 4.80 3.70 9 -15 7 9.60 4.50 -9 -15 7 15.40 5.00 9 -15 -7 15.60 4.50 9 -15 8 24.10 5.70 9 -15 -8 28.10 5.80 -9 -15 8 36.10 6.70 9 -15 9 -2.10 4.30 9 15 -9 0.20 5.90 9 -15 -9 2.90 4.50 -9 -15 9 8.90 5.00 9 15 -10 4.50 6.60 9 -15 10 3.80 4.80 9 -15 -10 17.70 5.80 -9 -15 10 13.80 6.20 9 15 10 -2.60 3.80 10 15 0 201.68 7.30 10 15 0 191.68 7.60 -10 -15 0 196.98 9.90 10 -15 0 191.18 9.00 10 -15 0 198.08 10.70 -10 -15 -1 291.87 13.10 10 -15 1 304.57 14.40 10 -15 1 307.97 12.50 10 -15 -1 300.47 12.90 10 15 1 304.17 11.80 -10 -15 1 311.57 14.00 10 -15 -1 309.87 14.40 -10 -15 -2 35.10 4.20 10 -15 2 32.60 4.80 10 -15 2 34.80 3.40 10 -15 -2 24.20 3.90 10 -15 -2 31.90 4.90 -10 -15 2 35.50 5.30 10 -15 3 2.20 1.70 10 -15 3 3.60 3.40 10 15 -3 -1.40 1.90 -10 -15 -3 0.20 2.10 10 -15 -3 -1.60 3.10 -10 -15 3 -1.50 3.20 10 -15 -3 0.00 2.60 10 -15 4 -0.40 1.70 10 -15 4 -0.50 3.40 -10 -15 -4 3.50 2.10 10 15 -4 1.90 2.00 -10 -15 4 -0.40 3.60 10 -15 -4 2.50 3.00 10 15 -5 30.50 3.40 10 -15 5 21.60 2.70 10 -15 5 29.10 5.30 -10 15 5 25.60 4.90 -10 -15 5 33.60 5.70 10 -15 -5 21.80 4.40 10 15 -6 2.30 2.00 -10 15 6 -2.00 2.90 10 -15 6 0.70 3.80 -10 -15 6 4.10 4.10 10 -15 -6 3.80 3.60 10 -15 7 69.49 7.70 10 -15 -7 60.29 7.10 -10 -15 7 72.89 8.50 10 -15 8 2.20 4.40 10 -15 -8 3.40 4.20 -10 -15 8 15.20 5.10 10 -15 9 59.39 8.20 10 15 9 48.40 6.50 -10 -15 9 76.69 9.30 10 -15 -9 58.69 8.00 10 -15 10 4.40 5.30 10 15 -10 14.50 7.10 -10 -15 10 15.30 6.10 10 15 10 4.00 4.80 10 -15 -10 16.80 5.80 11 -15 0 -3.00 3.10 11 15 0 0.50 0.70 -11 -15 0 0.40 2.70 11 -15 0 -6.20 2.00 -11 -15 -1 65.49 5.40 11 -15 1 58.89 6.40 11 -15 1 55.39 4.40 11 -15 -1 51.09 6.20 11 15 1 61.69 3.30 11 -15 -1 56.69 4.70 -11 -15 1 57.59 5.70 -11 -15 -2 232.68 11.10 11 -15 2 249.97 10.50 11 -15 2 246.08 12.80 11 -15 -2 238.68 12.40 -11 -15 2 236.48 12.20 11 -15 -2 243.38 11.20 11 15 2 243.18 9.80 11 15 -3 -0.30 2.20 11 -15 3 -2.60 1.90 -11 -15 -3 -1.00 2.50 11 -15 3 -2.40 3.40 -11 -15 3 3.20 3.70 11 -15 -3 5.90 3.00 11 -15 -3 5.90 3.00 11 -15 4 282.77 11.50 11 15 -4 303.07 12.30 11 -15 4 273.07 14.20 -11 -15 -4 269.47 11.80 11 -15 -4 282.67 13.20 -11 -15 4 270.67 14.10 -11 15 5 24.40 4.90 11 15 -5 19.40 3.10 11 -15 5 15.40 4.60 11 -15 5 23.00 2.80 -11 -15 5 20.90 5.20 11 -15 -5 15.80 4.40 11 -15 6 9.70 4.60 -11 15 6 20.90 4.40 11 15 -6 10.80 2.80 11 -15 -6 11.70 4.20 -11 -15 6 14.00 4.90 11 -15 7 -1.80 3.80 11 15 7 -1.70 3.10 -11 -15 7 4.00 4.80 11 -15 -7 -2.80 3.40 11 -15 8 8.40 4.90 11 15 8 -1.60 3.20 -11 -15 8 7.50 4.90 11 -15 -8 -7.00 3.80 11 -15 9 3.90 4.90 11 -15 -9 4.50 5.20 11 15 9 -1.10 4.20 -11 -15 9 5.50 5.00 11 -15 10 -3.20 4.70 11 15 10 -0.60 4.10 -11 -15 10 9.60 5.40 11 -15 -10 0.70 4.90 12 -15 0 1.90 3.40 -12 -15 0 2.30 3.00 12 -15 0 -0.60 2.20 12 -15 1 72.19 5.20 12 -15 1 81.19 7.50 -12 -15 -1 71.19 6.00 12 15 1 79.39 3.90 12 -15 -1 72.69 5.40 -12 -15 1 82.89 6.50 12 -15 -1 87.29 7.30 -12 -15 -2 60.29 5.40 12 -15 2 66.49 4.80 12 -15 2 75.89 7.30 -12 -15 2 68.09 6.40 12 15 2 65.29 4.00 12 -15 -2 71.09 7.00 12 -15 -2 71.99 5.60 12 -15 3 118.59 8.80 -12 -15 -3 107.89 6.80 12 15 -3 121.29 6.90 12 -15 3 119.19 6.30 -12 -15 3 116.59 8.50 12 -15 -3 111.29 7.30 12 15 3 117.59 6.00 12 -15 -3 110.09 8.30 -12 -15 -4 57.89 5.00 12 -15 4 68.19 7.30 12 15 -4 56.09 4.70 12 -15 4 57.99 4.40 -12 -15 4 65.19 7.60 12 -15 -4 56.29 6.00 12 15 4 52.99 4.30 -12 15 5 -3.50 3.80 12 -15 5 1.90 2.00 12 -15 5 5.00 4.00 12 15 -5 1.10 2.30 12 -15 -5 2.90 3.40 12 15 5 0.90 2.50 -12 -15 5 1.70 3.80 12 15 -6 13.90 2.80 12 -15 6 8.50 4.50 -12 15 6 16.90 4.60 12 -15 -6 14.40 4.50 12 15 6 7.30 3.00 -12 -15 6 10.60 4.80 12 -15 7 5.40 4.30 12 -15 -7 -0.20 3.90 -12 -15 7 11.30 5.10 12 15 7 6.90 3.30 12 -15 8 3.20 4.60 12 15 8 6.20 3.80 12 -15 -8 8.00 5.20 -12 -15 8 14.60 5.60 12 -15 9 20.80 6.20 12 15 9 14.80 4.80 12 -15 -9 19.70 6.00 -12 -15 9 29.40 7.20 13 -15 0 -1.90 2.10 13 -15 0 -10.10 2.80 -13 -15 0 -0.50 3.40 13 -15 1 1.10 3.50 -13 -15 -1 6.00 3.70 13 -15 1 6.20 2.80 13 -15 -1 3.70 3.60 13 15 1 6.00 1.50 13 -15 -1 1.60 2.50 -13 -15 1 3.30 4.00 13 -15 2 -0.20 3.60 -13 -15 -2 1.10 3.10 13 -15 2 -1.30 2.10 13 15 2 5.50 1.80 13 -15 -2 -2.60 3.30 13 -15 -2 4.40 2.90 -13 -15 2 4.30 4.10 -13 -15 -3 15.50 3.60 13 -15 3 8.40 4.00 13 15 -3 11.80 3.10 13 -15 3 9.70 2.60 13 -15 -3 7.00 3.20 13 15 3 9.30 2.40 -13 -15 3 14.30 5.00 13 -15 -3 10.80 3.50 13 -15 4 -2.70 3.50 13 15 -4 1.40 2.60 -13 -15 -4 1.90 2.80 13 -15 4 0.50 2.10 13 15 4 3.80 2.30 13 -15 -4 2.80 3.10 -13 -15 4 1.50 3.70 13 15 -5 10.50 2.90 13 -15 5 6.50 4.40 13 -15 5 10.80 3.90 -13 15 5 10.50 4.90 13 -15 -5 4.50 3.50 13 15 5 10.40 3.00 -13 -15 5 17.30 5.30 13 15 -6 11.20 3.10 -13 15 6 13.90 4.90 13 -15 6 25.10 5.80 13 -15 -6 17.80 4.60 -13 -15 6 21.00 5.60 13 15 6 20.10 3.90 13 -15 7 6.80 4.80 13 15 7 -0.10 3.20 -13 -15 7 8.20 4.90 13 -15 -7 0.40 4.30 13 -15 8 3.60 4.90 13 15 8 4.20 3.60 13 -15 -8 1.50 4.50 -13 -15 8 6.40 5.10 13 -15 9 -0.20 5.20 -13 -15 9 14.70 5.70 13 15 9 3.30 4.10 13 -15 -9 5.70 4.80 14 -15 0 58.09 6.70 14 -15 0 57.39 5.40 -14 -15 0 60.79 6.70 -14 -15 -1 2.20 3.30 14 -15 1 0.40 3.40 14 -15 1 -0.30 2.40 14 -15 -1 0.40 3.40 14 -15 -1 -0.70 2.50 -14 -15 1 2.70 3.50 -14 -15 -2 0.40 3.30 14 -15 2 0.60 3.40 14 -15 2 2.00 2.20 14 15 2 2.70 1.70 14 -15 -2 1.80 2.80 -14 -15 2 1.30 3.60 14 -15 -2 0.40 2.80 14 -15 3 -2.70 3.30 -14 -15 -3 2.60 3.00 14 15 -3 -3.50 2.30 14 -15 3 0.00 2.20 14 15 3 -0.10 1.70 14 -15 -3 -1.90 2.80 -14 -15 3 -4.10 3.50 14 -15 -3 -0.70 3.50 14 -15 4 73.59 7.90 14 -15 4 56.99 4.70 14 15 -4 53.69 5.50 -14 -15 -4 64.89 5.80 14 -15 -4 51.39 6.10 14 15 4 57.19 4.80 -14 -15 4 70.39 8.30 -14 15 5 51.79 7.50 14 -15 5 50.49 7.20 14 15 -5 55.79 5.30 -14 -15 5 54.19 8.00 14 15 5 56.69 5.40 14 -15 -5 54.09 6.40 14 -15 6 -3.00 3.90 14 15 -6 1.00 2.60 -14 15 6 4.70 4.70 14 -15 -6 3.20 3.70 -14 -15 6 2.70 4.40 14 15 6 5.30 3.00 14 -15 7 89.89 9.70 14 -15 -7 103.29 9.50 -14 -15 7 102.29 9.30 14 15 7 91.79 7.40 14 -15 8 0.90 5.00 14 15 8 7.10 4.40 14 -15 -8 8.00 5.00 -14 -15 8 10.10 5.50 14 -15 9 64.29 9.00 14 15 9 67.49 8.00 14 -15 -9 70.79 8.80 -14 -15 9 81.89 10.10 -15 -15 0 -2.50 3.20 15 -15 0 3.30 2.80 15 -15 0 -1.50 3.30 15 -15 1 -3.70 3.10 -15 -15 -1 0.60 3.40 15 -15 1 -1.40 2.50 15 -15 -1 -2.90 3.40 15 -15 -1 -0.80 2.30 -15 -15 1 -4.70 3.10 15 -15 2 8.60 4.30 -15 -15 -2 25.50 5.00 15 -15 2 20.20 3.60 15 -15 -2 12.40 3.70 -15 -15 2 17.20 5.00 15 -15 -2 19.10 4.20 15 -15 3 36.50 4.30 15 -15 3 36.10 5.60 -15 -15 -3 36.10 5.30 15 15 -3 36.00 4.60 15 15 3 34.10 3.60 15 -15 -3 33.70 5.10 15 -15 -3 36.10 5.80 -15 -15 3 35.70 6.30 15 15 -4 9.10 3.10 15 -15 4 5.50 4.20 15 -15 4 4.30 2.60 -15 -15 -4 12.80 4.00 -15 -15 4 5.80 4.80 15 15 4 2.20 2.40 15 -15 -4 7.20 3.60 15 -15 5 89.79 8.90 15 15 -5 75.09 6.10 -15 15 5 90.99 9.60 15 -15 -5 92.89 8.50 -15 -15 5 88.09 8.50 15 15 5 77.09 6.20 15 -15 6 9.30 5.20 15 15 -6 3.80 3.10 -15 15 6 10.50 5.40 15 -15 -6 15.40 4.80 -15 -15 6 16.80 5.60 15 15 6 7.70 3.50 15 -15 7 6.80 5.40 -15 -15 7 14.00 5.90 15 -15 -7 10.60 5.00 15 15 7 7.70 4.00 15 -15 8 22.70 6.60 -15 -15 8 27.20 7.00 15 -15 -8 25.10 6.10 15 15 8 18.30 4.90 16 -15 0 2.80 2.70 16 -15 0 -2.40 3.50 -16 -15 0 4.20 3.80 16 -15 1 11.20 4.00 16 -15 1 12.50 3.20 -16 -15 -1 9.50 4.20 16 -15 -1 8.50 3.30 16 -15 -1 9.40 4.40 -16 -15 1 9.60 4.40 16 -15 2 -2.70 3.60 -16 -15 -2 -0.50 3.60 16 -15 2 -1.60 2.20 16 -15 -2 -2.90 2.70 -16 -15 2 4.40 4.10 16 -15 -2 -1.40 3.50 -16 -15 -3 2.70 3.70 16 15 -3 2.20 2.80 16 -15 3 -1.10 2.30 16 -15 3 -3.00 3.80 16 -15 -3 -6.50 3.30 -16 -15 3 0.90 4.00 16 -15 -3 1.40 3.10 16 -15 4 0.30 2.60 -16 -15 -4 -0.30 3.50 16 -15 4 7.80 4.60 -16 15 4 -2.20 5.60 16 15 -4 1.90 2.90 16 15 4 0.20 2.20 -16 -15 4 3.50 4.60 16 -15 -4 -3.10 3.00 16 -15 -4 -4.20 3.60 -16 15 5 -1.70 5.20 16 -15 5 7.50 4.80 16 15 -5 4.90 3.10 16 15 5 2.20 2.60 -16 -15 5 10.40 5.20 16 -15 -5 -1.40 3.60 16 -15 6 54.49 8.00 -16 15 6 39.30 7.30 16 15 -6 38.40 5.10 16 -15 -6 42.60 6.40 -16 -15 6 51.29 8.80 16 15 6 34.90 5.00 16 -15 7 1.30 5.10 -16 -15 7 12.50 5.80 16 15 7 -2.60 3.60 16 -15 -7 5.80 4.70 16 -15 8 21.30 6.80 -16 -15 8 25.60 6.70 16 15 8 21.00 5.10 16 -15 -8 16.00 6.20 -17 -15 0 -0.10 3.90 17 -15 0 -3.90 3.60 17 -15 0 -4.50 2.40 17 -15 1 3.10 4.20 -17 -15 -1 0.70 4.40 17 -15 1 -1.00 3.00 17 -15 -1 4.50 3.20 17 -15 -1 -1.20 3.60 -17 -15 1 0.60 4.10 17 -15 2 5.50 3.10 -17 -15 -2 6.60 4.10 17 -15 2 1.30 4.00 17 -15 -2 1.80 3.20 17 -15 -2 2.40 3.90 -17 -15 2 2.30 4.40 17 15 -3 18.30 4.20 -17 -15 -3 28.60 5.50 17 -15 3 17.90 3.80 17 -15 3 21.70 5.70 -17 -15 3 23.70 5.90 17 -15 -3 20.20 4.60 17 -15 -3 14.30 4.90 -17 15 4 -9.20 5.50 17 -15 4 1.60 4.30 17 -15 4 -0.50 2.80 -17 -15 -4 8.10 4.80 17 15 -4 1.70 2.90 -17 -15 4 4.00 4.90 17 -15 -4 2.70 4.20 17 -15 -4 -1.50 3.50 -17 15 5 13.80 6.50 17 -15 5 12.20 5.30 17 15 -5 6.40 3.50 -17 -15 5 14.30 5.80 17 -15 -5 9.80 5.00 17 -15 6 13.30 6.00 17 15 -6 19.80 4.40 -17 15 6 28.50 6.80 17 15 6 23.50 4.10 -17 -15 6 22.20 6.40 17 -15 -6 22.40 5.40 17 -15 7 2.40 5.10 17 15 7 6.60 3.50 17 -15 -7 -4.60 4.50 -17 -15 7 6.30 5.70 18 -15 0 57.69 7.40 -18 -15 0 69.69 8.40 18 -15 0 56.49 6.10 18 -15 1 -1.30 2.60 18 -15 1 -3.20 3.90 -18 -15 -1 2.20 4.10 18 -15 -1 -4.90 3.10 18 -15 -1 0.60 3.90 -18 -15 1 6.20 4.90 18 15 -2 61.39 6.60 -18 -15 -2 60.59 7.70 18 -15 2 57.39 7.50 18 -15 2 48.40 5.80 18 -15 -2 50.09 7.00 -18 -15 2 68.39 8.60 18 -15 -2 61.19 6.60 18 15 -3 53.59 6.50 18 -15 3 53.49 5.70 18 -15 3 57.59 7.90 -18 -15 -3 58.49 7.60 18 -15 -3 57.09 7.20 -18 -15 3 65.79 8.60 18 -15 -3 51.99 6.40 18 -15 4 18.80 4.10 18 15 -4 22.10 4.70 -18 15 4 19.70 7.00 18 -15 4 17.60 5.60 -18 -15 4 29.00 6.80 18 -15 -4 15.10 4.80 18 -15 -4 21.20 5.60 18 15 -5 67.99 7.00 -18 15 5 71.99 10.10 18 -15 5 97.99 10.20 -18 -15 5 105.79 9.70 18 -15 -5 88.19 8.80 18 15 -6 -0.70 3.30 18 -15 6 5.20 5.20 -18 15 6 4.90 5.90 -18 -15 6 9.70 5.60 18 -15 -6 1.80 4.30 18 -15 7 81.49 10.10 -18 -15 7 87.39 10.80 18 -15 -7 64.29 8.60 -19 -15 0 -1.50 4.00 19 -15 0 0.00 3.30 19 -15 0 -2.50 3.90 19 -15 1 -1.80 4.10 19 -15 1 -0.30 2.90 -19 -15 -1 5.50 5.00 19 -15 -1 -1.40 3.00 19 -15 -1 -2.30 3.90 -19 -15 1 5.40 4.60 -19 -15 -2 2.30 4.70 19 -15 2 -7.00 3.90 19 -15 2 -0.90 3.30 19 15 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6.00 2.90 0 -16 5 -0.90 2.00 0 -16 -5 1.30 3.10 0 16 -5 -1.70 3.70 0 -16 5 -1.20 3.00 0 -16 -6 435.56 18.90 0 -16 6 427.36 19.10 0 -16 6 420.46 17.60 0 16 -6 410.76 21.40 0 -16 -7 5.60 4.00 0 -16 7 -0.50 3.40 0 -16 7 0.80 2.90 0 16 -7 2.30 4.80 0 -16 8 143.29 10.10 0 -16 8 130.39 8.90 0 16 -8 139.69 13.00 0 -16 -8 145.49 10.30 0 -16 9 -1.40 4.10 0 -16 9 5.60 3.40 0 -16 -9 -2.80 4.20 0 16 -9 1.00 5.40 0 -16 10 1.30 5.00 0 -16 -10 -6.20 4.50 0 -16 10 1.60 3.50 0 16 -10 -4.50 5.70 0 16 -11 -8.20 5.60 0 -16 11 1.20 4.50 0 -16 -11 -1.50 6.00 0 -16 11 2.20 6.00 1 -16 0 0.00 1.90 -1 -16 0 -2.30 1.70 1 -16 0 -2.50 1.40 -1 -16 0 -1.50 1.50 1 -16 0 -1.30 1.70 1 16 -1 26.50 2.00 -1 -16 -1 32.10 3.40 1 -16 1 30.30 3.50 -1 -16 -1 25.30 2.50 1 -16 1 26.40 3.70 1 -16 -1 24.10 3.30 -1 16 -1 25.60 4.60 -1 -16 1 29.00 3.60 -1 16 -1 27.30 1.90 -1 -16 1 24.90 3.00 1 -16 -1 25.00 3.00 1 -16 2 4.50 2.50 1 -16 2 10.10 2.70 -1 -16 -2 6.90 2.80 -1 16 2 11.60 1.70 1 16 -2 10.00 1.00 1 -16 -2 6.90 2.40 -1 -16 2 8.50 2.10 -1 16 -2 9.30 3.50 -1 16 -2 10.20 0.90 -1 -16 2 4.10 2.50 1 16 2 11.30 1.70 -1 16 3 87.19 3.80 1 -16 3 79.19 5.90 1 -16 3 90.09 5.70 -1 -16 -3 85.99 6.20 1 16 3 82.99 3.70 1 -16 -3 80.09 5.60 -1 16 -3 72.69 7.40 -1 -16 3 81.99 5.90 -1 -16 3 85.29 5.30 1 -16 4 12.60 3.70 -1 16 4 15.10 2.90 1 -16 4 16.50 3.10 1 16 -4 12.30 4.80 -1 -16 -4 8.60 3.60 -1 -16 4 11.00 3.60 -1 16 -4 16.20 4.50 -1 -16 4 11.80 2.60 1 -16 -4 18.10 3.60 -1 16 5 8.00 2.10 1 -16 5 3.40 3.60 1 16 -5 5.20 4.40 1 -16 5 5.00 2.50 -1 -16 -5 4.00 3.30 -1 -16 5 4.30 3.50 -1 16 -5 10.00 4.70 1 -16 -5 -0.10 3.10 -1 -16 5 8.60 2.70 1 16 -6 95.19 9.50 -1 -16 -6 107.59 8.00 1 -16 6 91.99 7.70 1 -16 6 103.19 6.80 -1 -16 6 99.29 7.80 -1 -16 6 100.69 6.70 1 -16 -6 95.09 7.70 -1 16 -6 89.99 10.30 1 16 -7 -0.80 4.50 1 -16 7 6.20 4.20 1 -16 7 3.90 3.30 -1 -16 -7 5.20 3.90 -1 -16 7 7.40 4.10 -1 -16 7 -0.20 2.70 -1 16 -7 4.70 5.00 1 -16 -7 1.70 3.70 1 16 -8 15.50 6.20 -1 -16 -8 21.90 5.40 1 -16 8 20.70 4.30 1 -16 8 29.70 6.30 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16 2 25.50 2.30 -2 -16 2 23.70 2.90 -2 -16 2 23.60 3.70 -2 16 -2 13.10 4.00 2 -16 -2 14.90 3.00 2 -16 3 5.30 3.00 -2 -16 -3 6.90 2.90 2 -16 3 5.30 2.40 -2 16 3 7.60 2.50 -2 16 3 11.60 1.60 -2 -16 3 8.70 2.30 -2 -16 3 7.50 3.00 -2 16 -3 13.50 4.20 2 16 3 10.60 1.50 2 -16 -3 8.20 2.70 -2 16 4 147.49 5.50 -2 16 4 143.59 7.50 2 -16 4 144.39 8.60 -2 16 4 140.89 5.70 2 -16 4 157.78 8.30 -2 -16 -4 150.08 8.50 -2 -16 4 138.19 8.50 -2 16 -4 158.98 11.20 2 -16 -4 147.49 8.40 -2 -16 4 144.29 7.30 2 -16 5 25.10 3.80 2 -16 5 24.30 4.80 2 16 -5 24.40 5.60 -2 -16 -5 18.80 4.40 -2 16 5 19.10 2.50 2 -16 -5 20.80 4.20 -2 -16 5 16.00 3.00 -2 16 -5 14.40 5.20 -2 -16 5 18.80 4.50 2 -16 6 1.30 2.70 2 16 -6 7.50 4.70 -2 -16 -6 5.40 3.90 2 -16 6 3.70 3.70 -2 -16 6 1.30 3.40 -2 16 -6 -7.40 4.60 2 -16 -6 3.40 3.50 -2 -16 6 2.50 2.50 2 -16 7 1.40 3.90 -2 -16 -7 6.30 4.10 2 -16 7 2.40 2.90 2 16 -7 0.70 4.70 2 -16 -7 3.00 3.60 -2 16 -7 -5.80 4.30 -2 -16 7 3.10 3.80 -2 -16 7 -1.70 2.40 2 -16 8 12.30 5.10 2 -16 8 15.80 4.00 2 16 -8 6.40 5.30 -2 -16 -8 7.60 4.50 -2 -16 8 4.80 3.20 2 -16 -8 14.10 4.90 -2 16 -8 6.60 6.10 -2 -16 8 13.20 4.80 2 -16 9 41.00 6.00 -2 -16 -9 31.00 6.60 2 -16 9 33.70 7.10 2 16 -9 31.20 7.80 -2 -16 9 40.30 5.40 -2 -16 9 46.60 7.50 -2 16 -9 38.90 8.40 2 -16 -9 28.20 6.30 -2 -16 -10 3.30 5.30 2 -16 10 -0.40 4.90 2 -16 10 4.00 4.40 2 16 -10 -0.40 6.60 -2 -16 10 4.00 3.90 2 -16 -10 3.60 5.10 -2 -16 10 4.70 4.90 -2 16 -10 0.20 6.80 2 -16 11 12.10 4.80 2 16 -11 4.90 7.50 2 -16 11 19.30 7.00 2 -16 -11 13.70 6.30 -2 -16 11 21.70 6.70 3 -16 0 -1.10 1.90 -3 -16 0 -3.80 1.50 -3 16 0 0.50 2.30 3 -16 0 -3.20 1.30 3 -16 1 5.10 2.40 -3 16 1 2.50 2.50 -3 -16 -1 -1.30 1.30 3 -16 1 0.20 1.20 3 -16 1 3.40 2.20 3 16 -1 1.80 1.10 3 -16 -1 -0.40 1.80 -3 -16 1 2.00 1.60 -3 16 -1 1.40 1.00 -3 16 -1 1.70 2.90 3 -16 -1 2.50 2.40 -3 -16 1 -1.10 1.90 -3 16 2 9.30 2.70 -3 -16 -2 4.40 1.50 -3 16 2 7.80 2.70 3 -16 2 0.30 1.00 3 -16 2 4.60 2.30 3 16 -2 6.00 1.20 3 -16 2 4.40 2.60 -3 -16 2 7.90 2.00 3 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4.80 3 -16 -8 15.80 5.00 -3 -16 8 11.00 3.50 -3 -16 8 17.20 5.20 -3 16 -8 2.60 6.40 -3 -16 -9 7.50 5.10 3 16 -9 -2.10 5.90 3 -16 9 5.20 3.80 3 -16 9 -6.20 4.10 -3 -16 9 5.00 4.60 -3 -16 9 3.90 3.30 3 -16 -9 1.20 4.40 -3 16 -9 -2.70 5.50 3 -16 10 23.00 6.90 3 -16 10 23.90 5.40 3 16 -10 11.40 6.80 3 -16 -10 26.30 6.50 -3 16 -10 9.30 6.60 -3 -16 10 26.80 6.50 3 -16 11 0.70 6.50 3 -16 11 8.20 4.60 3 16 -11 -2.90 6.80 3 -16 -11 1.30 5.70 -3 -16 11 19.30 6.50 4 -16 0 375.36 14.90 -4 -16 0 385.06 15.40 -4 16 0 410.46 17.70 4 -16 0 393.76 16.40 4 -16 1 96.89 4.70 -4 16 1 106.89 7.30 -4 -16 -1 100.79 5.30 4 -16 1 96.79 6.50 -4 16 -1 100.19 8.10 4 -16 -1 104.29 6.60 -4 -16 1 109.89 5.30 -4 16 -1 106.89 4.80 4 -16 -1 98.29 5.40 -4 -16 1 103.79 6.00 4 -16 2 4.20 1.10 4 -16 2 6.10 2.80 -4 -16 -2 5.70 1.60 4 16 -2 3.90 1.40 -4 16 2 4.20 2.50 4 -16 2 1.50 2.30 4 16 -2 4.30 1.30 -4 16 -2 4.00 3.20 -4 -16 2 5.30 2.70 4 -16 -2 -3.20 1.70 4 16 2 5.60 2.10 4 -16 -2 0.40 2.60 -4 -16 2 4.10 1.70 4 16 -3 66.69 3.20 -4 16 3 66.69 3.70 4 -16 3 69.99 5.70 4 16 -3 61.29 3.30 -4 16 3 64.89 5.30 4 -16 3 66.39 5.40 -4 -16 -3 67.89 3.10 -4 -16 3 67.49 4.20 -4 -16 3 54.59 5.10 4 -16 -3 67.29 5.00 -4 16 -3 61.39 7.40 4 -16 4 111.29 7.60 4 16 -4 103.19 4.20 -4 16 4 104.99 4.80 4 -16 4 116.19 7.20 4 16 -4 106.89 4.30 -4 -16 4 99.39 7.20 4 -16 -4 106.09 6.80 -4 -16 4 104.79 5.70 -4 16 -4 104.39 9.20 4 -16 5 1.30 2.80 -4 16 5 2.70 1.40 4 -16 5 1.40 3.30 -4 16 -5 1.50 4.40 -4 -16 5 1.80 2.10 4 -16 -5 5.70 3.30 -4 -16 5 -0.10 3.30 4 -16 6 173.68 10.60 4 -16 6 175.28 9.80 4 -16 -6 166.08 9.90 -4 -16 6 171.58 8.50 -4 16 -6 159.08 12.70 -4 -16 6 167.38 10.20 4 -16 7 -4.60 3.70 4 16 -7 -4.10 4.00 4 -16 7 0.70 3.00 -4 -16 7 1.40 2.50 -4 -16 7 6.60 4.20 4 -16 -7 0.50 3.40 -4 16 -7 -5.10 4.40 4 -16 8 60.39 6.70 4 16 -8 47.70 8.50 4 -16 8 66.49 8.60 -4 -16 8 62.89 7.90 4 -16 -8 53.19 7.20 -4 -16 8 59.09 5.60 -4 16 -8 58.49 9.70 4 -16 9 11.90 4.40 4 16 -9 11.30 6.70 4 -16 9 22.70 6.50 -4 16 -9 7.20 6.30 -4 -16 9 16.30 5.40 4 -16 -9 20.50 5.70 4 16 -10 23.00 7.50 4 -16 10 39.20 7.90 4 -16 10 25.30 5.70 4 -16 -10 27.20 6.40 -4 -16 10 36.60 7.40 5 -16 0 0.50 2.50 5 -16 0 -3.60 1.40 -5 -16 0 -3.80 1.80 -5 16 0 1.40 2.90 5 -16 1 186.58 7.80 -5 -16 -1 190.68 8.30 -5 16 1 202.78 10.50 5 -16 1 198.38 9.80 5 16 -1 203.68 8.00 5 -16 -1 176.18 9.60 -5 16 -1 189.38 7.80 -5 -16 1 187.38 9.20 -5 16 -1 191.48 11.10 5 -16 -1 178.88 8.50 5 -16 2 15.10 3.10 -5 16 2 12.10 3.10 5 16 -2 16.10 1.90 5 -16 2 18.10 1.70 -5 -16 -2 16.60 2.20 5 16 -2 17.50 2.10 -5 16 -2 28.40 5.20 5 -16 -2 13.80 3.40 5 -16 -2 12.20 2.90 -5 -16 2 17.40 3.40 5 16 2 17.30 2.90 -5 -16 2 16.10 2.10 -5 -16 -3 34.60 2.20 5 16 -3 37.50 2.50 -5 16 3 34.20 4.30 5 -16 3 38.30 4.60 5 -16 3 32.20 1.80 5 16 -3 37.30 2.40 -5 -16 3 35.60 3.00 5 -16 -3 41.20 4.50 -5 16 -3 27.00 5.90 -5 -16 3 40.10 4.90 -5 16 4 100.59 5.00 5 -16 4 93.79 6.90 5 16 -4 97.09 4.30 5 -16 4 98.49 7.30 5 -16 -4 100.89 6.60 -5 -16 4 90.09 6.90 -5 -16 4 92.89 5.20 -5 16 -4 103.79 9.30 5 -16 5 18.80 4.90 5 -16 5 24.20 4.30 -5 16 5 18.50 2.70 5 16 -5 18.00 1.70 -5 -16 5 19.00 2.80 -5 16 -5 15.20 5.50 5 -16 -5 14.40 3.80 -5 -16 5 20.20 4.60 5 -16 6 4.40 4.10 5 -16 6 4.70 3.20 -5 -16 6 -1.50 2.00 -5 -16 6 0.00 3.50 -5 16 -6 -1.80 5.00 5 -16 -6 5.90 3.50 5 16 -7 0.30 4.80 5 -16 7 -0.60 4.20 5 -16 7 -1.20 3.20 -5 -16 7 3.10 2.40 -5 -16 7 -0.70 3.60 5 -16 -7 2.10 3.70 -5 16 -7 1.90 5.90 5 16 -8 17.60 6.90 5 -16 8 23.20 4.90 5 -16 8 23.80 6.40 -5 16 -8 18.20 7.20 -5 -16 8 36.30 6.60 5 -16 -8 22.70 5.40 5 -16 9 14.50 6.00 5 -16 9 6.20 4.60 5 16 -9 -5.40 4.80 5 -16 -9 13.50 5.30 -5 -16 9 14.00 5.30 5 -16 10 39.20 8.10 5 -16 10 44.00 7.00 5 16 -10 26.20 8.30 -5 -16 10 36.00 7.40 5 -16 -10 51.19 7.60 6 16 0 23.60 2.50 6 -16 0 18.60 2.60 -6 16 0 19.60 4.10 6 -16 0 24.80 3.70 -6 -16 0 20.00 3.30 -6 -16 -1 41.90 3.50 6 -16 1 47.90 5.20 -6 16 1 52.89 5.30 6 16 -1 48.20 3.00 6 -16 1 38.10 3.10 -6 16 -1 53.89 6.30 6 -16 -1 47.40 3.70 6 -16 -1 52.29 5.20 -6 -16 1 44.40 4.30 6 -16 2 3.00 2.90 6 16 -2 3.90 1.10 -6 16 2 3.00 2.50 -6 -16 -2 -0.50 1.50 6 -16 2 3.50 1.20 -6 16 -2 0.70 3.20 6 -16 -2 -1.90 2.20 6 -16 -2 1.40 2.20 -6 -16 2 3.50 2.90 6 16 -3 2.80 1.40 6 -16 3 0.20 2.60 6 16 -3 4.00 1.00 6 -16 3 2.90 1.00 -6 -16 -3 4.70 1.40 -6 16 -3 -4.00 3.40 -6 -16 3 4.00 1.50 6 -16 -3 1.00 2.20 -6 -16 3 2.40 2.90 -6 -16 -4 92.19 3.60 6 16 -4 90.99 4.40 6 -16 4 87.39 4.20 6 -16 4 91.89 7.00 6 -16 4 86.99 3.40 -6 -16 4 96.19 4.80 -6 16 -4 79.19 9.20 -6 -16 4 86.19 6.80 6 -16 -4 94.99 6.40 -6 16 5 8.30 2.60 6 -16 5 9.90 3.50 6 16 -5 8.30 1.50 -6 -16 5 7.00 3.90 -6 -16 5 5.50 1.90 6 -16 -5 4.20 3.30 -6 16 -5 2.00 4.80 6 -16 6 41.30 5.60 -6 -16 6 42.20 3.90 -6 -16 6 46.80 6.40 6 -16 -6 38.40 5.40 -6 16 -6 38.90 7.90 6 -16 7 4.00 3.60 6 -16 -7 0.70 3.60 -6 -16 7 3.20 3.90 -6 16 -7 -5.50 5.50 6 -16 8 12.30 4.50 6 16 -8 14.40 5.90 6 -16 -8 18.70 5.10 -6 -16 8 17.80 5.30 6 -16 9 7.80 4.50 6 16 -9 8.00 6.40 6 -16 -9 7.90 4.70 -6 -16 9 14.40 5.30 6 16 -10 0.30 6.50 6 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31.00 5.50 -7 -16 7 36.90 6.30 7 16 -8 4.10 5.00 7 -16 8 3.20 4.60 -7 -16 8 5.00 4.40 7 -16 -8 1.70 4.10 7 16 -9 4.50 6.30 7 -16 9 -2.70 4.00 -7 -16 9 6.80 4.80 7 -16 -9 3.20 4.50 7 -16 10 -1.90 4.50 7 16 -10 9.00 7.20 -7 -16 10 4.70 5.00 7 -16 -10 -1.20 5.00 8 -16 0 158.78 9.20 -8 -16 0 150.08 8.00 8 16 0 159.18 6.70 8 -16 0 156.08 7.40 8 -16 1 255.97 10.60 8 -16 1 251.97 12.60 -8 -16 -1 261.57 11.20 8 16 -1 271.37 9.60 8 -16 -1 259.97 11.10 8 -16 -1 248.28 12.20 -8 -16 1 251.47 11.70 8 -16 2 37.00 3.00 8 -16 2 41.90 5.30 -8 -16 -2 39.80 3.50 8 -16 -2 44.80 4.40 8 -16 -2 31.70 4.90 -8 -16 2 42.90 5.20 8 -16 3 37.90 2.80 -8 -16 -3 41.80 3.30 8 16 -3 44.00 3.60 8 -16 3 47.90 5.60 8 -16 -3 46.40 5.20 -8 -16 3 46.70 5.80 8 -16 -3 45.80 5.00 8 -16 4 75.29 7.20 -8 -16 -4 76.29 3.90 8 -16 4 75.79 3.70 8 16 -4 84.19 4.50 8 -16 -4 73.59 6.40 -8 -16 4 66.79 6.40 8 16 -5 4.20 1.80 8 -16 5 2.30 3.50 -8 16 5 2.70 3.00 -8 -16 5 1.50 3.60 8 -16 -5 2.60 3.10 8 -16 6 0.00 3.50 -8 16 6 9.10 4.10 8 -16 -6 6.20 3.70 -8 -16 6 2.60 3.70 8 -16 7 68.89 7.50 8 -16 -7 53.89 6.90 -8 -16 7 72.99 8.60 8 -16 8 -2.00 3.60 -8 -16 8 5.30 4.70 8 -16 -8 0.00 3.90 8 16 -9 29.70 8.00 8 -16 9 26.30 6.00 -8 -16 9 24.80 6.40 8 -16 -9 25.20 6.00 8 -16 10 3.10 4.90 8 16 -10 6.00 7.00 -8 -16 10 10.40 5.60 8 -16 -10 10.30 5.30 9 -16 0 -2.40 2.10 9 16 0 -0.50 1.10 9 -16 0 0.30 1.70 -9 -16 0 -4.00 2.30 9 -16 1 43.90 3.70 9 -16 1 38.20 4.90 9 16 -1 38.40 1.90 -9 -16 -1 37.70 4.40 9 -16 -1 45.90 4.40 -9 -16 1 39.30 4.90 9 -16 -1 52.19 5.80 9 -16 2 275.67 13.70 9 -16 2 295.57 11.30 -9 -16 -2 270.97 11.80 9 -16 -2 272.97 12.20 9 -16 -2 291.67 13.70 -9 -16 2 266.47 13.00 9 -16 3 3.20 1.60 9 16 -3 3.10 2.00 -9 -16 -3 2.90 2.10 9 -16 3 -3.20 3.00 9 -16 -3 -2.80 2.40 -9 -16 3 1.80 3.30 9 -16 -3 0.70 3.10 9 -16 4 95.79 4.60 9 -16 4 92.99 7.70 -9 -16 -4 88.49 4.70 9 16 -4 87.69 5.20 9 -16 -4 97.29 6.90 -9 -16 4 91.69 7.30 9 16 -5 14.20 2.50 -9 16 5 10.30 3.80 9 -16 5 17.20 4.50 -9 -16 5 13.10 4.40 9 -16 -5 10.70 3.80 -9 16 6 10.40 3.20 9 -16 6 6.90 4.10 -9 -16 6 7.30 4.10 9 -16 -6 12.00 4.10 9 -16 7 2.40 4.00 9 -16 -7 -0.20 3.50 -9 -16 7 3.90 4.20 9 -16 8 13.30 5.00 9 -16 -8 10.40 4.80 -9 -16 8 15.90 5.30 9 16 -9 17.70 7.30 9 -16 9 4.70 4.80 9 -16 -9 6.60 5.00 -9 -16 9 18.00 5.70 9 -16 10 9.10 5.30 9 16 -10 16.80 8.10 -9 -16 10 33.60 7.70 9 -16 -10 18.00 6.10 9 16 10 3.90 4.50 -10 -16 0 25.90 4.10 10 -16 0 23.40 3.10 10 -16 0 27.60 4.90 10 -16 1 51.69 5.80 -10 -16 -1 51.19 5.20 10 -16 1 48.10 4.20 10 -16 -1 49.00 4.60 10 -16 -1 41.30 5.50 -10 -16 1 53.99 5.80 10 -16 2 -0.20 1.60 10 -16 2 -3.90 3.20 -10 -16 -2 -2.10 2.20 10 -16 -2 -0.70 2.60 10 -16 -2 2.10 2.60 -10 -16 2 -1.10 3.00 10 -16 3 33.60 3.20 10 -16 3 36.10 5.10 10 16 -3 34.00 3.70 -10 -16 -3 34.10 3.80 10 -16 -3 39.60 4.60 10 -16 -3 26.60 4.40 -10 -16 3 31.80 5.30 10 16 -4 -1.30 1.70 -10 -16 -4 2.30 1.80 10 -16 4 -5.50 3.00 10 -16 4 0.60 1.60 10 -16 -4 -4.80 2.50 -10 -16 4 -3.80 3.30 10 16 -5 8.60 2.30 -10 16 5 10.50 4.10 10 -16 5 9.70 4.10 10 -16 -5 9.70 3.70 -10 -16 5 11.90 4.50 10 -16 6 -7.10 3.50 -10 16 6 -0.50 3.00 -10 -16 6 1.90 3.90 10 -16 -6 -0.30 3.50 10 -16 7 0.70 4.00 -10 -16 7 14.70 5.00 10 -16 -7 6.80 4.20 10 -16 8 9.90 4.90 10 -16 -8 7.90 4.70 -10 -16 8 15.40 5.40 10 -16 9 18.60 5.80 -10 -16 9 30.40 6.70 10 16 9 15.30 4.60 10 -16 -9 16.60 5.70 10 16 -10 1.80 6.60 10 -16 10 3.70 5.00 -10 -16 10 14.70 6.00 10 16 10 -0.80 4.20 10 -16 -10 8.90 5.40 11 16 0 1.40 0.80 -11 -16 0 0.10 2.90 11 -16 0 -5.30 3.00 11 -16 0 -3.90 2.00 11 -16 1 64.79 6.60 11 -16 1 60.79 4.50 -11 -16 -1 47.50 4.90 -11 -16 1 53.99 5.50 11 -16 -1 57.19 6.30 11 16 1 56.99 3.30 11 -16 -1 65.59 5.60 -11 -16 -2 88.59 6.00 11 -16 2 87.59 7.00 11 -16 2 92.89 5.40 -11 -16 2 90.69 7.30 11 -16 -2 83.59 7.40 11 -16 -2 91.49 6.40 11 -16 3 -1.10 3.40 11 -16 3 -1.20 1.70 11 16 -3 -1.90 2.00 -11 -16 -3 0.60 2.20 11 -16 -3 -2.00 3.10 -11 -16 3 -2.20 3.40 11 -16 -3 -4.00 2.50 -11 -16 -4 3.10 2.10 11 -16 4 0.90 1.70 11 16 -4 1.00 2.00 11 -16 4 -1.90 3.40 -11 -16 4 2.80 3.80 11 -16 -4 2.40 3.00 -11 16 5 11.40 4.40 11 16 -5 15.30 2.90 11 -16 5 15.10 4.80 11 -16 -5 10.70 4.00 -11 -16 5 18.50 5.20 11 -16 6 -1.70 4.00 -11 16 6 -0.30 3.10 -11 -16 6 -1.10 4.00 11 -16 -6 -1.50 3.30 11 -16 7 13.10 5.10 11 -16 -7 11.80 4.60 -11 -16 7 12.10 5.30 11 -16 8 1.90 4.50 11 16 8 1.00 3.50 11 -16 -8 4.30 4.50 -11 -16 8 6.80 5.00 11 -16 9 0.20 4.90 11 16 9 0.30 3.90 -11 -16 9 5.90 5.20 11 -16 -9 1.00 5.30 -12 -16 0 1.90 2.90 12 -16 0 2.40 3.50 12 -16 0 0.30 2.50 -12 -16 -1 40.30 5.30 12 -16 1 40.80 4.20 12 -16 1 40.50 5.80 12 -16 -1 45.70 4.90 12 -16 -1 43.90 5.80 -12 -16 1 44.90 5.70 12 16 1 36.20 2.70 12 -16 2 -3.40 1.90 12 -16 2 -2.00 3.30 -12 -16 -2 2.90 2.80 -12 -16 2 -1.90 3.70 12 -16 -2 -2.60 2.50 12 -16 -2 -4.10 2.70 12 16 2 0.10 1.50 12 16 -3 30.80 3.90 12 -16 3 27.20 3.30 -12 -16 -3 32.30 4.10 12 -16 3 37.30 5.70 -12 -16 3 32.40 5.60 12 -16 -3 25.10 4.20 12 16 3 29.10 3.20 12 -16 -3 26.80 5.10 12 -16 4 34.60 3.50 -12 -16 -4 31.60 3.90 12 -16 4 36.40 5.90 12 16 -4 26.30 3.70 12 16 4 26.90 3.50 -12 -16 4 30.30 5.70 12 -16 -4 33.70 4.90 12 -16 5 -3.20 3.60 12 16 -5 1.40 2.40 -12 16 5 3.50 4.20 12 16 5 5.20 2.70 12 -16 -5 -0.30 3.10 -12 -16 5 3.80 4.20 12 -16 6 3.30 4.20 -12 16 6 1.40 3.60 12 16 -6 2.50 2.60 -12 -16 6 4.00 4.40 12 -16 -6 1.10 3.60 12 16 6 1.50 2.60 12 -16 7 66.99 8.20 12 -16 -7 72.19 7.90 -12 -16 7 70.69 8.90 12 16 7 64.19 6.50 12 -16 8 -5.10 4.30 -12 -16 8 5.40 4.90 12 16 8 -0.90 3.30 12 -16 -8 0.00 4.40 12 -16 9 101.09 10.60 12 16 9 108.39 9.40 12 -16 -9 99.59 10.40 -12 -16 9 112.19 10.00 -13 -16 0 -0.40 3.30 13 -16 0 -2.70 2.30 13 -16 0 -1.70 3.40 -13 -16 -1 34.70 4.80 13 -16 1 25.80 5.20 13 -16 1 27.80 3.80 13 -16 -1 25.80 5.00 -13 -16 1 35.70 5.40 13 -16 -1 23.80 3.90 13 -16 2 52.39 4.60 -13 -16 -2 51.49 5.00 13 -16 2 47.20 6.00 13 16 2 46.30 3.40 13 -16 -2 45.30 5.40 -13 -16 2 45.00 6.20 13 -16 -2 44.40 6.10 13 -16 3 69.09 7.50 13 16 -3 62.99 5.20 -13 -16 -3 60.59 5.30 13 -16 3 56.19 4.50 -13 -16 3 64.59 7.40 13 -16 -3 54.69 6.50 13 16 3 54.49 4.20 13 -16 -3 63.99 6.20 13 -16 4 118.79 6.50 13 16 -4 120.99 7.00 -13 -16 -4 115.29 6.90 13 -16 4 101.69 9.00 -13 -16 4 119.79 8.90 13 16 4 119.89 6.60 13 -16 -4 109.99 7.90 -13 16 5 17.60 5.30 13 -16 5 23.10 5.50 13 16 -5 24.50 3.80 13 16 5 26.70 3.90 -13 -16 5 23.90 5.80 13 -16 -5 16.70 4.40 -13 16 6 10.70 4.90 13 -16 6 13.60 5.20 13 16 -6 19.10 5.10 -13 -16 6 13.60 5.30 13 16 6 14.50 3.90 13 -16 -6 14.00 4.60 13 -16 7 15.00 5.50 -13 -16 7 15.60 5.60 13 -16 -7 7.70 4.70 13 16 7 8.80 3.60 13 -16 8 12.50 5.70 -13 -16 8 12.60 5.60 13 -16 -8 1.20 4.40 13 16 8 -1.40 3.40 13 -16 9 6.50 5.50 13 -16 -9 -1.40 4.50 -13 -16 9 10.20 5.80 13 16 9 1.10 4.00 -14 -16 0 16.10 4.30 14 -16 0 11.30 3.30 14 -16 0 16.10 4.00 14 -16 1 23.80 4.60 -14 -16 -1 20.10 4.50 14 -16 1 11.40 3.10 14 -16 -1 14.20 4.40 14 -16 -1 15.90 3.50 -14 -16 1 23.40 5.20 -14 -16 -2 3.70 3.20 14 -16 2 -7.70 3.00 14 -16 2 -1.50 2.20 14 -16 -2 6.20 3.80 -14 -16 2 1.40 3.70 14 -16 -2 -1.20 2.60 14 16 -3 27.80 4.10 14 -16 3 30.40 3.80 -14 -16 -3 31.70 4.80 14 -16 3 24.20 5.40 14 -16 -3 21.10 5.00 14 -16 -3 24.70 4.40 -14 -16 3 38.40 6.20 14 16 3 28.00 3.20 14 -16 4 -5.40 3.40 -14 -16 -4 5.60 3.40 14 16 -4 -0.10 2.40 14 -16 4 0.10 2.00 14 16 4 1.40 2.20 -14 -16 4 4.60 4.30 14 -16 -4 -2.30 2.90 14 -16 5 6.10 4.50 -14 16 5 -2.30 4.60 14 16 -5 -1.20 2.40 14 -16 -5 3.20 3.50 -14 -16 5 -3.30 3.80 14 16 5 -0.10 2.60 -14 16 6 23.60 5.70 14 16 -6 25.60 4.50 14 -16 6 39.30 6.90 -14 -16 6 29.20 6.40 14 16 6 23.10 4.10 14 -16 -6 27.20 5.50 14 -16 7 40.50 7.40 14 -16 -7 24.60 5.60 14 16 7 31.00 5.10 -14 -16 7 43.40 7.90 14 -16 8 6.20 5.50 -14 -16 8 5.80 5.10 14 16 8 -0.40 3.30 14 -16 -8 3.30 4.70 15 -16 0 1.70 2.50 15 -16 0 -5.60 3.40 -15 -16 0 3.10 3.80 15 -16 1 15.50 3.60 15 -16 1 21.60 5.20 -15 -16 -1 12.10 4.20 -15 -16 1 18.00 4.80 15 -16 -1 17.80 4.90 15 -16 -1 21.00 3.90 15 -16 2 0.30 3.80 15 -16 2 0.70 2.50 -15 -16 -2 9.50 3.80 15 -16 -2 -0.90 3.70 15 -16 -2 9.50 3.40 -15 -16 2 8.90 4.40 15 -16 3 43.40 6.60 15 -16 3 40.90 4.50 15 16 -3 39.40 4.80 -15 -16 -3 48.30 5.90 15 -16 -3 39.80 6.10 -15 -16 3 42.00 6.80 15 -16 -3 45.90 5.60 15 -16 4 -3.50 3.60 15 16 -4 0.30 2.60 15 -16 4 -4.40 2.20 15 -16 -4 -1.00 3.00 -15 -16 4 1.30 4.10 15 16 4 0.30 2.30 15 -16 5 31.60 6.20 15 16 -5 29.20 4.30 -15 16 5 17.40 6.10 -15 -16 5 29.90 6.70 15 16 5 23.10 4.00 15 -16 -5 22.80 5.10 15 -16 6 -1.70 4.70 15 16 -6 -1.70 4.00 -15 16 6 2.40 4.60 -15 -16 6 0.60 4.90 15 -16 -6 -0.40 3.90 15 16 6 -0.30 3.00 15 -16 7 17.00 5.80 15 -16 -7 15.40 5.20 -15 -16 7 11.70 5.70 15 16 7 9.10 4.30 15 -16 8 3.60 5.20 -15 -16 8 6.80 6.00 15 -16 -8 -2.10 4.50 15 16 8 5.30 3.70 -16 -16 0 204.48 11.90 16 -16 0 201.98 10.60 16 -16 0 200.38 12.20 16 -16 1 -6.20 3.40 -16 -16 -1 2.40 3.50 16 -16 1 -1.50 2.50 16 -16 -1 -0.30 2.70 -16 -16 1 6.80 4.20 16 -16 -1 -1.60 3.90 -16 -16 -2 19.40 4.90 16 -16 2 11.70 4.20 16 -16 2 22.00 3.80 16 -16 -2 23.80 5.50 16 -16 -2 27.10 4.50 -16 -16 2 32.10 6.00 16 -16 3 4.00 2.80 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6.60 -6 -17 6 19.90 5.00 -6 -17 6 14.20 3.10 6 -17 -6 12.40 4.00 6 -17 7 40.30 5.90 -6 -17 7 53.09 7.10 -6 17 -7 31.80 7.80 6 -17 -7 41.20 6.10 6 -17 8 2.20 3.80 6 17 -8 2.80 5.80 6 -17 -8 -0.40 4.10 -6 -17 8 11.10 4.90 6 17 -9 21.50 7.10 6 -17 9 38.30 6.70 -6 -17 9 31.60 6.80 6 -17 -9 20.20 6.40 6 -17 10 4.20 4.60 6 17 -10 4.10 6.90 -6 -17 10 2.50 4.90 6 -17 -10 10.20 5.50 7 17 0 -1.10 1.40 7 -17 0 -3.00 1.60 -7 -17 0 -2.00 2.10 -7 17 0 -4.80 2.90 7 -17 0 1.10 3.00 7 17 -1 22.60 2.10 7 -17 1 11.60 2.20 -7 -17 -1 18.10 3.10 7 -17 1 17.90 3.80 7 -17 -1 16.20 3.80 -7 -17 1 16.40 3.40 -7 17 -1 7.60 4.20 7 -17 -1 18.80 3.00 7 -17 2 12.60 2.00 7 -17 2 6.60 3.30 7 17 -2 17.80 1.60 -7 -17 -2 13.90 2.50 -7 -17 2 17.30 4.00 7 -17 -2 16.90 3.90 -7 17 -2 9.30 5.00 7 -17 -2 13.70 3.00 -7 -17 -3 27.80 2.50 7 -17 3 26.10 4.50 7 17 -3 27.30 2.80 7 -17 3 27.30 2.20 7 -17 -3 20.90 4.30 -7 17 -3 22.30 6.90 -7 -17 3 26.80 4.70 7 -17 -3 20.90 4.00 -7 -17 3 23.90 2.10 7 -17 4 34.90 5.10 7 17 -4 30.70 2.80 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8 -17 -3 2.10 2.90 -8 -17 3 5.50 3.50 -8 17 -3 -1.20 4.50 8 -17 -3 11.70 3.80 8 -17 4 55.49 3.90 -8 -17 -4 54.49 4.60 8 17 -4 49.00 3.60 8 -17 4 64.19 6.70 -8 -17 4 67.89 7.40 8 -17 -4 57.29 5.80 8 -17 5 7.00 3.80 8 17 -5 3.10 1.70 -8 17 5 5.10 3.20 -8 -17 5 3.90 3.70 8 -17 -5 1.30 3.10 8 -17 6 32.40 5.50 -8 -17 6 33.50 5.90 8 -17 -6 28.70 5.30 8 -17 7 69.69 7.60 8 -17 -7 59.19 7.10 -8 -17 7 64.49 8.10 8 -17 8 21.80 6.00 8 -17 -8 22.90 5.60 -8 -17 8 29.50 6.70 8 17 -9 30.40 7.80 8 -17 9 32.80 6.50 8 -17 -9 27.20 6.20 -8 -17 9 38.50 7.20 8 -17 10 6.60 5.20 8 17 -10 -0.50 6.90 8 -17 -10 6.60 5.80 -8 -17 10 0.40 4.90 9 -17 0 -3.80 1.70 -9 -17 0 -2.40 2.10 9 -17 0 -2.50 2.90 9 -17 1 -2.40 3.00 -9 -17 -1 -1.10 2.30 9 -17 1 1.40 1.90 9 -17 -1 -0.40 2.20 -9 -17 1 1.00 2.90 9 -17 -1 0.00 3.00 -9 -17 -2 30.50 3.70 9 -17 2 23.80 4.70 9 -17 2 27.60 2.90 9 -17 -2 29.90 5.00 -9 -17 2 27.50 5.00 9 -17 -2 27.50 3.70 9 -17 3 7.00 3.80 9 17 -3 7.30 2.20 9 -17 3 10.40 1.90 -9 -17 -3 15.30 2.60 9 -17 -3 11.40 3.80 -9 -17 3 10.10 3.90 9 -17 -3 7.40 3.10 9 -17 4 7.70 1.90 9 -17 4 4.80 3.80 9 17 -4 6.00 2.10 -9 -17 4 9.10 4.20 9 -17 -4 11.80 3.60 -9 17 5 18.10 4.20 9 17 -5 17.80 2.60 9 -17 5 21.60 5.00 9 -17 -5 21.80 4.40 -9 -17 5 29.50 5.50 9 -17 6 8.90 4.40 9 -17 -6 10.00 4.10 -9 -17 6 10.50 4.50 9 -17 7 26.50 5.60 -9 -17 7 26.20 5.90 9 -17 -7 25.50 5.40 9 -17 8 5.70 4.50 -9 -17 8 2.70 4.40 9 -17 -8 4.30 4.50 9 -17 9 24.90 6.10 9 17 -9 21.40 7.30 -9 -17 9 30.80 6.70 9 -17 -9 21.00 5.90 9 -17 10 0.00 4.60 -9 -17 10 13.30 5.90 9 -17 -10 -0.30 5.20 10 -17 0 16.10 2.90 10 -17 0 8.00 3.30 -10 -17 0 9.50 3.10 10 -17 1 64.49 4.60 10 -17 1 78.29 7.40 -10 -17 -1 65.09 5.20 10 -17 -1 65.29 5.10 -10 -17 1 69.49 5.70 10 -17 -1 70.19 6.90 10 -17 2 22.90 3.00 10 -17 2 19.90 4.60 -10 -17 -2 27.10 3.70 10 -17 -2 18.90 3.60 10 -17 -2 26.80 4.80 -10 -17 2 25.20 4.60 10 17 -3 43.10 4.00 10 -17 3 39.10 3.40 -10 -17 -3 38.20 3.90 10 -17 3 39.00 5.80 10 -17 -3 33.20 5.40 -10 -17 3 33.80 5.60 10 -17 -3 41.80 5.00 10 17 -4 0.90 2.00 10 -17 4 -4.30 3.20 10 -17 4 -1.30 1.60 -10 -17 4 -3.10 3.30 10 -17 -4 0.10 3.20 -10 17 5 46.00 5.80 10 -17 5 47.40 6.20 10 17 -5 44.40 3.90 10 -17 -5 54.79 6.10 -10 -17 5 61.09 7.70 10 -17 6 -2.40 3.80 -10 -17 6 9.40 4.60 10 -17 -6 5.80 3.90 10 -17 7 117.29 9.90 -10 -17 7 134.79 10.00 10 -17 -7 130.29 9.50 10 -17 8 4.10 4.70 10 -17 -8 -3.00 4.20 -10 -17 8 4.10 4.60 10 -17 9 11.10 5.40 -10 -17 9 14.00 5.50 10 -17 -9 12.90 5.50 11 -17 0 -3.20 3.10 -11 -17 0 -1.00 2.90 11 -17 0 -3.40 2.00 11 -17 1 1.50 3.70 11 -17 1 3.50 2.40 -11 -17 -1 8.00 3.20 -11 -17 1 6.00 3.70 11 -17 -1 5.00 2.80 11 -17 -1 2.50 3.40 11 -17 2 36.30 5.60 -11 -17 -2 40.80 4.60 11 -17 2 44.50 3.90 11 -17 -2 38.40 4.50 11 -17 -2 35.40 5.10 -11 -17 2 39.30 5.60 -11 -17 -3 39.20 4.20 11 -17 3 43.10 6.10 11 17 -3 42.00 4.30 11 -17 3 41.90 3.70 11 -17 -3 34.60 5.40 -11 -17 3 40.70 6.00 11 -17 -3 44.40 5.00 11 -17 4 64.49 7.50 11 17 -4 65.19 4.70 11 -17 4 69.29 4.80 11 -17 -4 82.59 7.40 -11 -17 4 68.89 7.80 -11 17 5 -1.90 3.80 11 17 -5 0.40 2.00 11 -17 5 1.90 4.00 11 -17 -5 1.50 3.30 -11 -17 5 0.20 3.60 11 -17 6 4.10 4.60 11 -17 -6 5.40 4.00 -11 -17 6 6.30 4.40 11 -17 7 20.10 5.60 11 -17 -7 16.30 5.00 -11 -17 7 29.00 6.30 11 -17 8 5.90 4.90 11 -17 -8 5.50 4.50 11 17 8 1.70 3.40 -11 -17 8 13.50 5.40 11 -17 9 8.90 5.40 -11 -17 9 7.00 5.20 11 -17 -9 5.20 5.60 11 17 9 2.20 4.20 12 -17 0 84.49 7.90 12 -17 0 83.49 5.80 -12 -17 0 80.49 6.50 12 -17 1 60.09 6.90 12 -17 1 64.39 4.80 -12 -17 -1 60.69 5.40 -12 -17 1 62.89 6.30 12 17 1 62.69 3.40 12 -17 -1 56.99 5.00 12 -17 -1 68.89 7.00 12 -17 2 24.50 4.60 -12 -17 -2 30.70 4.20 12 -17 2 24.50 3.30 12 17 2 24.40 2.60 12 -17 -2 25.30 4.00 -12 -17 2 31.80 5.30 12 -17 -2 30.60 5.30 12 17 -3 24.30 3.60 -12 -17 -3 16.10 3.30 12 -17 3 14.90 2.80 12 -17 3 13.90 4.60 12 -17 -3 19.60 4.80 12 -17 -3 12.60 3.60 -12 -17 3 18.30 4.80 12 17 3 15.50 2.60 12 -17 4 -1.70 3.70 12 17 -4 5.30 2.50 12 -17 -4 1.20 3.00 12 17 4 -1.00 2.10 -12 -17 4 4.50 4.20 12 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13 17 4 41.70 4.30 13 -17 5 10.20 4.70 -13 17 5 1.10 4.30 13 17 -5 1.00 2.50 13 -17 -5 3.50 3.60 -13 -17 5 8.50 4.70 13 17 5 9.10 3.10 13 -17 6 0.60 4.50 -13 -17 6 7.50 4.80 13 17 6 2.30 3.20 13 -17 -6 3.00 3.90 13 -17 7 -3.30 4.50 -13 -17 7 9.40 5.40 13 -17 -7 0.20 4.30 13 17 7 0.10 3.00 13 -17 8 4.50 5.10 13 17 8 4.70 3.80 13 -17 -8 -0.40 4.40 -13 -17 8 9.30 5.40 -14 -17 0 255.77 12.90 14 -17 0 242.68 13.10 14 -17 0 255.07 11.70 14 -17 1 40.90 4.70 14 -17 1 45.80 6.50 -14 -17 -1 52.19 6.10 14 -17 -1 38.30 5.60 14 -17 -1 31.00 4.50 -14 -17 1 53.69 6.50 -14 -17 -2 7.00 3.30 14 -17 2 5.80 3.40 14 -17 2 3.80 2.60 -14 -17 2 4.10 4.30 14 -17 -2 6.60 4.10 14 -17 -2 6.30 3.50 14 -17 3 16.00 3.20 -14 -17 -3 23.20 4.10 14 17 -3 22.70 3.80 14 -17 3 22.30 5.30 14 17 3 21.70 3.00 -14 -17 3 26.70 5.60 14 -17 -3 14.30 4.90 14 -17 -3 13.00 3.90 14 17 -4 4.70 2.80 14 -17 4 5.20 4.50 14 17 4 2.40 2.50 14 -17 -4 5.40 4.00 -14 -17 4 5.70 4.50 14 -17 5 26.90 6.00 14 17 -5 17.90 3.60 -14 17 5 18.50 6.00 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41.70 5.00 -15 -17 6 56.89 8.30 15 -17 7 8.00 5.60 -15 -17 7 12.20 5.80 15 17 7 10.40 4.10 15 -17 -7 4.60 5.10 15 -17 8 8.30 5.90 15 17 8 10.40 4.10 15 -17 -8 6.00 5.20 -15 -17 8 11.20 5.90 16 -17 0 13.40 4.90 16 -17 0 8.60 3.20 -16 -17 0 13.40 4.40 16 -17 1 81.19 8.90 16 -17 1 103.29 6.90 -16 -17 -1 90.49 7.40 -16 -17 1 102.79 8.60 16 -17 -1 101.39 7.50 16 -17 -1 105.19 8.90 16 -17 2 67.99 8.00 16 -17 2 54.29 5.50 -16 -17 -2 74.69 6.60 16 -17 -2 65.89 6.70 16 -17 -2 67.09 7.70 -16 -17 2 70.79 8.10 16 -17 3 10.80 3.10 -16 -17 -3 14.30 4.20 16 -17 3 11.30 4.90 16 17 -3 7.40 3.50 16 -17 -3 14.00 4.80 -16 -17 3 10.90 5.00 16 -17 -3 12.10 4.30 16 -17 4 -1.00 4.20 16 17 -4 1.60 2.90 -16 -17 4 7.90 4.60 16 -17 -4 2.10 3.60 16 -17 5 15.70 5.70 -16 17 5 22.80 6.90 16 17 -5 19.50 4.10 16 -17 -5 21.20 5.50 -16 -17 5 30.20 6.60 16 -17 6 -0.70 4.80 -16 -17 6 8.90 5.30 16 17 6 9.00 4.00 16 -17 -6 -0.10 4.20 16 -17 7 5.80 5.60 -16 -17 7 14.90 6.00 16 17 7 11.00 4.10 16 -17 -7 6.90 5.50 -17 -17 0 1.40 4.10 17 -17 0 -0.30 2.70 17 -17 0 -8.70 3.30 -17 -17 -1 11.20 4.20 17 -17 1 3.70 4.40 17 -17 1 2.10 3.00 -17 -17 1 2.30 4.00 17 -17 -1 -4.30 3.90 17 -17 -1 -0.50 3.30 17 -17 2 -0.30 2.90 -17 -17 -2 6.20 4.00 17 -17 2 4.00 4.40 -17 -17 2 6.70 4.50 17 -17 -2 -7.00 3.70 17 -17 -2 -1.30 3.10 17 17 -3 -2.10 3.00 -17 -17 -3 6.40 4.00 17 -17 3 -0.70 4.30 17 -17 3 0.10 2.70 17 -17 -3 -3.50 3.90 17 -17 -3 3.90 4.10 -17 -17 3 6.80 4.90 17 17 -4 0.50 3.10 -17 17 4 0.10 5.10 17 -17 4 1.10 4.50 -17 -17 4 7.20 5.00 17 -17 -4 3.50 3.90 17 -17 5 11.20 5.40 17 17 -5 5.40 3.50 -17 17 5 9.30 6.30 -17 -17 5 18.70 6.00 17 -17 -5 5.70 4.80 17 -17 6 -3.80 4.90 -17 -17 6 5.40 5.10 17 -17 -6 -4.30 4.00 17 -17 7 -9.10 4.70 -17 -17 7 10.60 5.80 17 -17 -7 -0.20 5.30 18 -17 0 11.10 5.00 -18 -17 0 19.10 5.70 18 -17 0 14.50 4.20 18 -17 1 1.70 4.50 -18 -17 -1 12.60 4.90 18 -17 1 2.30 3.30 18 -17 -1 0.40 4.10 18 -17 -1 7.50 3.70 -18 -17 1 7.30 4.50 18 -17 2 24.70 4.20 18 17 -2 31.20 5.40 18 -17 2 23.20 6.10 -18 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12.50 4.80 -20 -19 2 22.00 6.70 20 -19 -2 9.20 5.60 20 -19 -2 9.30 4.40 20 19 -3 43.10 6.30 20 -19 3 31.10 7.20 20 -19 -3 34.70 6.20 20 -19 -3 37.10 7.80 -20 -19 3 49.00 8.10 21 -19 0 -2.10 4.80 21 -19 0 -4.70 3.30 -21 -19 0 10.30 4.90 21 -19 1 -6.80 4.70 -21 -19 -1 10.60 5.10 21 -19 1 0.70 4.00 -21 -19 1 6.10 4.80 21 -19 -1 3.80 4.00 21 -19 -1 -0.30 4.90 21 19 -2 18.10 4.90 21 -19 2 7.60 5.90 21 -19 -2 7.10 4.50 -21 -19 2 15.70 6.20 21 -19 -2 6.90 5.50 0 -20 0 5743.52 202.08 0 -20 0 5965.50 202.48 0 -20 1 13.10 3.60 0 20 -1 10.40 1.90 0 20 -2 1006.20 40.60 0 -20 2 1003.40 38.00 0 -20 -2 991.00 37.40 0 -20 2 1039.10 37.50 0 -20 3 5.40 2.80 0 -20 -3 8.50 3.40 0 20 -3 -1.80 3.70 0 -20 3 3.40 3.20 0 -20 4 158.58 9.50 0 -20 -4 144.19 9.00 0 20 -4 142.69 11.70 0 -20 4 145.69 8.50 0 20 5 1.10 2.90 0 -20 5 3.60 3.10 0 20 -5 4.40 5.30 0 -20 -5 -2.60 3.40 0 -20 5 5.70 4.10 0 20 -6 120.79 11.90 0 -20 -6 117.49 9.10 0 -20 6 127.39 8.20 0 -20 6 118.29 9.20 0 -20 7 -1.40 3.30 0 20 -7 -7.50 5.50 0 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33.20 4.40 -1 -20 5 37.20 6.00 1 -20 -5 49.10 6.10 -1 20 -5 29.40 7.20 1 -20 6 122.09 8.30 1 -20 6 143.79 9.90 1 20 -6 132.69 12.10 -1 -20 -6 139.49 9.80 1 -20 -6 130.49 9.50 -1 20 -6 107.39 12.40 -1 -20 6 140.89 8.40 -1 -20 6 136.99 9.70 1 -20 7 7.30 3.60 -1 -20 -7 11.00 4.80 1 20 -7 15.00 7.50 1 -20 7 4.10 4.70 -1 -20 7 4.50 3.40 -1 20 -7 3.70 6.40 -1 -20 7 4.40 4.50 1 -20 -7 4.40 4.40 1 -20 8 -0.60 3.50 1 -20 8 2.30 5.10 1 20 -8 -1.60 5.90 -1 -20 -8 1.80 4.80 -1 -20 8 1.80 4.90 -1 -20 8 1.20 3.50 1 -20 -8 -2.00 4.50 -1 20 -8 -5.10 6.50 1 20 -9 -6.20 6.20 1 -20 9 0.70 3.60 -1 -20 -9 2.10 5.50 1 -20 9 8.70 5.70 -1 20 -9 1.00 6.80 -1 -20 9 6.40 5.50 1 -20 -9 -0.10 4.90 1 -20 10 14.50 6.50 1 20 -10 15.40 7.70 1 -20 10 18.30 8.10 -1 -20 -10 12.30 6.60 -1 -20 10 15.90 7.40 1 -20 -10 12.80 6.20 -1 20 -10 6.40 7.50 2 -20 0 106.09 5.90 -2 -20 0 103.59 6.30 -2 20 0 105.69 9.10 2 -20 0 98.59 6.90 -2 -20 0 90.79 6.10 -2 20 1 44.90 6.30 2 -20 1 46.30 5.10 -2 -20 -1 56.99 4.40 2 -20 1 46.20 5.40 -2 -20 1 62.89 5.30 -2 20 -1 44.60 6.60 2 -20 -1 50.49 5.30 -2 -20 1 45.00 4.60 2 -20 -1 61.59 5.00 2 -20 2 326.47 14.70 -2 20 2 328.37 16.10 -2 -20 -2 338.67 13.10 2 -20 2 326.17 15.20 2 -20 -2 340.87 14.30 -2 20 -2 311.07 17.70 -2 -20 2 338.27 14.80 -2 -20 2 331.37 13.90 2 -20 3 72.09 6.40 2 -20 3 79.79 6.20 -2 20 3 72.59 7.20 -2 -20 3 78.89 5.50 -2 20 -3 55.19 8.00 -2 -20 3 77.99 6.30 2 -20 -3 70.19 6.00 2 -20 4 10.40 4.40 -2 20 4 9.40 3.50 2 -20 4 7.80 3.60 -2 -20 -4 7.60 4.00 -2 -20 4 11.70 3.10 -2 -20 4 11.50 4.10 -2 20 -4 11.20 5.90 2 -20 -4 11.40 3.90 -2 -20 -5 2.00 4.30 2 20 -5 -0.10 5.60 2 -20 5 1.30 2.90 2 -20 5 8.10 4.80 -2 20 -5 2.50 5.40 -2 -20 5 9.40 4.20 -2 -20 5 5.80 2.80 -2 -20 -6 88.59 8.60 2 -20 6 78.39 8.70 2 20 -6 58.49 9.30 2 -20 6 86.69 7.40 -2 -20 6 70.29 6.00 -2 -20 6 76.39 7.60 2 -20 -6 86.19 8.50 -2 20 -6 68.89 10.40 -2 -20 -7 147.29 11.50 2 -20 7 154.38 9.90 2 20 -7 166.68 13.90 2 -20 7 176.38 11.60 -2 -20 7 163.68 11.10 -2 -20 7 156.08 9.40 -2 20 -7 160.88 14.10 2 -20 -7 175.98 11.20 2 -20 8 0.20 4.80 -2 -20 -8 0.90 5.00 2 20 -8 0.80 7.10 2 -20 8 3.50 3.60 -2 -20 8 2.90 4.80 2 -20 -8 8.20 5.30 -2 20 -8 0.20 6.50 -2 -20 -9 12.90 6.30 2 -20 9 25.80 7.20 2 20 -9 14.20 7.80 2 -20 9 15.60 4.70 -2 -20 9 20.70 6.40 2 -20 -9 22.70 6.30 -2 20 -9 18.50 8.40 2 -20 10 -6.60 5.00 2 20 -10 -5.50 7.20 2 -20 10 1.40 4.50 -2 -20 10 7.20 5.90 2 -20 -10 13.80 6.10 -2 20 -10 0.20 6.80 3 -20 0 -1.80 1.80 -3 20 0 -6.30 3.40 3 -20 0 -0.10 2.60 -3 -20 0 0.20 2.20 3 -20 1 5.70 3.40 -3 -20 -1 2.80 2.20 3 -20 1 0.30 1.70 -3 20 1 3.20 3.80 3 -20 -1 8.80 3.40 -3 -20 1 2.30 2.30 -3 20 -1 -2.10 3.80 -3 -20 1 2.10 2.30 -3 20 2 6.40 4.00 3 -20 2 9.20 4.30 3 -20 2 11.30 3.30 -3 -20 -2 12.60 2.40 -3 -20 2 12.20 3.40 3 -20 -2 16.30 3.30 -3 -20 2 13.70 2.80 -3 20 -2 -2.40 4.90 3 -20 3 18.40 4.60 -3 20 3 20.00 4.50 3 -20 3 15.70 3.80 -3 -20 3 30.90 3.60 3 -20 -3 28.40 4.40 -3 -20 3 30.30 5.00 -3 20 -3 14.40 6.30 -3 20 4 121.19 8.00 3 -20 4 121.29 8.10 3 -20 4 124.69 8.80 -3 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1 98.19 5.00 -4 -20 1 104.49 6.30 4 -20 -1 92.19 7.00 4 -20 -1 95.59 5.90 -4 20 -1 87.69 8.90 4 -20 2 487.65 20.10 4 -20 2 475.85 17.30 -4 -20 -2 483.35 18.10 -4 20 2 457.65 20.80 -4 20 -2 463.15 22.80 -4 -20 2 495.15 18.60 4 -20 -2 492.35 20.30 4 -20 -2 473.05 19.20 -4 -20 2 470.45 19.70 4 -20 3 17.90 5.00 4 20 -3 33.30 2.70 4 -20 3 15.90 3.90 -4 20 3 11.00 3.90 -4 20 -3 17.50 6.10 -4 -20 3 21.90 3.10 -4 -20 3 23.70 4.50 4 -20 4 1.80 3.90 -4 20 4 6.60 3.20 4 -20 4 3.40 3.30 -4 -20 4 3.80 2.30 -4 20 -4 0.40 4.70 4 -20 -4 3.80 3.50 -4 -20 4 9.50 3.80 4 -20 5 40.20 5.40 4 -20 5 39.00 6.80 -4 -20 5 33.70 4.00 4 -20 -5 52.89 6.20 -4 -20 5 54.89 6.70 -4 20 -5 27.10 7.50 4 20 -6 11.90 6.00 4 -20 6 26.30 6.10 4 -20 6 10.90 4.10 -4 -20 6 17.60 3.80 -4 -20 6 19.60 5.30 -4 20 -6 13.10 6.70 4 -20 -6 24.20 5.00 4 -20 7 -0.90 3.40 4 -20 7 -0.30 4.70 4 20 -7 8.20 6.10 4 -20 -7 -2.80 3.60 -4 -20 7 5.20 4.30 -4 20 -7 -6.90 6.60 4 -20 8 107.29 8.70 4 -20 8 97.79 11.00 4 20 -8 90.79 11.70 4 -20 -8 93.69 9.60 -4 -20 8 91.09 10.10 -4 20 -8 84.29 12.00 4 20 -9 43.40 9.30 4 -20 9 58.09 9.20 4 -20 9 55.69 7.60 -4 20 -9 47.00 10.20 -4 -20 9 58.59 8.70 4 -20 -9 55.29 8.30 5 -20 0 1.30 1.90 -5 -20 0 1.30 2.30 5 -20 0 2.60 3.00 -5 -20 -1 29.20 3.50 5 -20 1 24.70 4.40 5 -20 1 24.90 2.60 -5 20 1 12.90 5.10 5 -20 -1 22.40 3.30 -5 -20 1 29.00 4.00 5 -20 -1 22.70 4.40 -5 20 -1 12.40 6.00 5 -20 2 165.88 9.50 -5 -20 -2 160.78 7.30 5 -20 2 152.98 6.50 -5 20 2 143.09 10.10 -5 -20 2 163.98 9.10 5 -20 -2 162.78 8.40 5 -20 -2 152.68 8.90 -5 -20 2 172.88 7.50 -5 20 -2 114.39 11.20 -5 20 3 45.50 5.70 5 -20 3 51.69 5.80 5 20 -3 53.79 3.10 -5 -20 -3 50.19 3.50 -5 -20 3 52.09 4.20 -5 -20 3 54.39 6.20 -5 20 -3 40.30 8.10 5 -20 -3 45.50 5.10 5 -20 4 505.85 20.70 -5 20 -4 453.25 23.80 -5 -20 4 476.25 18.40 5 -20 -4 475.15 20.00 -5 -20 4 467.75 20.60 5 -20 5 0.60 4.10 5 -20 5 -1.50 3.00 -5 20 -5 -2.10 4.90 5 -20 -5 5.20 3.50 -5 -20 5 3.40 3.70 5 -20 6 129.49 10.10 5 -20 6 130.29 9.30 -5 -20 6 139.09 9.80 -5 20 -6 132.69 12.90 5 -20 -6 160.88 9.80 5 -20 7 20.00 4.90 5 -20 7 16.80 6.20 5 20 -7 12.00 6.50 -5 -20 7 22.10 5.80 -5 20 -7 0.50 6.60 5 -20 -7 30.00 5.80 5 -20 8 69.49 10.10 5 -20 8 62.39 7.70 5 20 -8 68.69 10.70 -5 20 -8 58.49 11.00 -5 -20 8 82.79 9.50 5 -20 -8 44.50 7.20 5 -20 9 37.10 6.50 5 20 -9 40.50 9.90 5 -20 9 43.00 8.40 5 -20 -9 55.69 8.20 -5 -20 9 58.79 8.70 -5 20 -9 35.30 9.60 -6 -20 0 27.50 3.70 6 -20 0 28.00 3.20 6 -20 0 22.60 4.40 -6 20 0 3.70 4.70 -6 -20 -1 3.90 2.30 -6 20 1 -10.40 3.60 6 -20 1 8.30 3.60 6 -20 1 3.30 1.80 -6 -20 1 7.30 3.00 6 -20 -1 4.20 2.30 -6 20 -1 -9.50 4.70 6 -20 -1 4.40 3.20 6 -20 2 4.20 1.50 6 -20 2 2.10 3.20 -6 -20 -2 5.30 2.00 -6 20 2 -9.30 3.50 6 -20 -2 3.00 2.60 6 -20 -2 6.40 3.50 -6 -20 2 3.30 3.20 6 -20 3 69.99 6.80 6 20 -3 60.69 3.80 -6 -20 -3 67.19 5.30 -6 -20 3 65.89 6.10 -6 20 -3 62.49 9.00 6 -20 -3 62.89 5.50 -6 -20 3 67.09 4.20 6 -20 4 8.00 3.60 6 -20 -4 5.50 3.30 -6 20 -4 -1.80 5.30 -6 -20 4 6.00 3.80 6 -20 5 73.19 7.40 -6 20 -5 68.59 9.90 6 -20 -5 85.19 7.10 -6 -20 5 79.89 7.30 6 -20 6 2.40 4.30 6 -20 -6 9.70 4.00 -6 20 -6 2.00 6.00 -6 -20 6 1.50 4.10 6 -20 7 29.70 5.60 6 20 -7 28.40 7.60 6 -20 -7 31.10 6.00 -6 -20 7 35.20 6.60 -6 20 -7 13.70 7.30 6 20 -8 56.59 10.30 6 -20 8 68.49 7.90 -6 -20 8 77.39 9.20 -6 20 -8 57.19 10.60 6 -20 -8 54.39 7.90 6 20 -9 9.20 7.80 6 -20 9 4.30 4.60 -6 -20 9 12.40 5.70 6 -20 -9 5.20 5.00 -7 20 0 -12.00 3.80 7 -20 0 -4.30 1.60 -7 -20 0 0.10 2.00 7 -20 0 -0.40 3.10 -7 20 1 -5.10 3.40 7 -20 1 -2.50 1.70 7 -20 1 -2.50 2.80 -7 -20 -1 1.20 2.10 7 -20 -1 -0.70 3.10 7 -20 -1 -3.30 1.80 -7 20 -1 -8.50 4.20 -7 -20 1 -1.70 2.60 -7 -20 -2 100.89 5.50 7 -20 2 103.89 7.80 7 -20 2 96.59 4.90 7 -20 -2 94.59 6.20 -7 20 -2 90.69 10.30 7 -20 -2 88.99 7.50 -7 -20 2 105.49 7.00 7 -20 3 45.70 5.80 7 20 -3 40.00 3.30 -7 -20 3 42.40 5.80 7 -20 -3 38.80 4.90 -7 20 -3 31.10 7.50 7 -20 4 20.10 4.60 -7 20 -4 14.40 6.50 -7 -20 4 18.50 4.60 7 -20 -4 21.40 4.60 7 -20 5 8.90 4.10 -7 20 -5 -1.60 5.60 -7 -20 5 14.30 4.80 7 -20 -5 8.60 4.30 7 -20 6 13.60 4.60 7 -20 -6 18.00 5.10 -7 20 -6 10.30 6.70 -7 -20 6 20.60 5.40 7 -20 7 12.20 4.80 7 -20 -7 15.50 5.10 -7 -20 7 21.80 5.80 7 20 -8 78.79 11.70 7 -20 8 74.19 8.50 7 -20 -8 82.79 9.10 -7 -20 8 88.89 10.10 7 -20 9 18.20 5.50 7 20 -9 17.90 7.60 -7 -20 9 17.20 6.30 7 -20 -9 32.80 7.20 -8 -20 0 164.38 8.70 8 -20 0 168.68 10.20 8 -20 0 172.78 8.20 -8 -20 -1 14.60 3.10 8 -20 1 9.90 2.30 8 -20 1 9.40 3.90 8 -20 -1 9.20 3.90 -8 20 -1 11.80 5.10 -8 -20 1 12.80 3.70 8 -20 -1 11.60 2.90 8 -20 2 66.69 4.10 8 -20 2 70.09 7.20 -8 -20 -2 64.39 4.50 8 -20 -2 72.89 7.30 -8 -20 2 62.09 5.80 -8 20 -2 63.49 8.90 8 -20 -2 72.59 5.40 8 -20 3 16.80 4.40 8 20 -3 15.60 2.50 -8 20 -3 15.20 6.30 8 -20 -3 16.00 4.50 -8 -20 3 22.60 4.90 8 -20 -3 20.20 3.90 8 -20 4 8.10 4.10 -8 -20 4 14.80 4.40 8 -20 -4 13.20 3.70 -8 20 -4 4.70 5.70 8 -20 5 42.60 6.20 -8 -20 5 51.19 6.80 -8 20 -5 35.60 8.30 8 -20 -5 33.20 5.50 8 -20 6 33.30 6.00 8 -20 -6 46.60 6.40 -8 -20 6 41.90 6.90 8 -20 7 101.59 9.50 -8 -20 7 84.89 8.60 8 -20 -7 96.09 9.30 8 -20 8 33.30 6.60 8 20 -8 25.90 8.30 -8 -20 8 35.40 7.20 8 -20 -8 20.50 6.00 8 20 -9 17.20 7.70 8 -20 9 9.30 5.40 -8 -20 9 29.00 7.00 8 -20 -9 8.70 5.40 -9 -20 0 1.40 2.30 9 -20 0 -4.90 2.20 9 -20 0 -0.50 2.10 9 -20 1 0.80 2.80 9 -20 1 1.90 2.00 -9 -20 -1 3.60 2.50 -9 -20 1 4.70 3.10 9 -20 -1 -3.70 3.00 9 -20 -1 3.70 2.30 -9 -20 -2 43.60 4.00 9 -20 2 35.50 5.60 9 -20 2 39.50 3.40 9 -20 -2 45.80 6.00 -9 -20 2 50.69 6.20 9 -20 -2 43.40 4.90 9 20 -3 24.30 3.10 9 -20 3 20.30 4.90 -9 -20 3 24.30 5.00 9 -20 -3 23.60 4.20 9 -20 -3 23.60 5.10 9 -20 4 92.49 8.60 9 -20 -4 77.59 7.30 -9 -20 4 75.69 7.10 9 -20 5 -3.70 3.50 9 -20 -5 -0.40 3.20 -9 -20 5 4.50 4.40 9 -20 6 59.39 7.80 9 -20 -6 57.99 7.00 -9 -20 6 56.19 7.80 9 -20 7 31.60 6.20 9 -20 -7 24.60 5.80 -9 -20 7 29.80 6.70 9 -20 8 1.70 5.30 9 -20 -8 -0.60 4.50 -9 -20 8 11.60 5.50 9 -20 9 0.50 4.60 9 20 -9 -2.10 6.10 -9 -20 9 10.70 5.60 9 -20 -9 4.50 5.10 -10 -20 0 17.20 3.50 10 -20 0 12.50 4.60 10 -20 0 11.30 2.90 10 -20 1 22.00 3.10 -10 -20 -1 29.10 4.10 10 -20 1 19.60 4.80 10 -20 -1 22.20 4.80 10 -20 -1 25.10 3.70 -10 -20 1 23.80 4.30 10 -20 2 -1.50 3.50 10 -20 2 2.90 1.90 -10 -20 -2 3.60 2.50 10 -20 -2 -2.00 2.60 -10 -20 2 5.10 3.30 10 -20 -2 4.20 3.90 10 20 -3 49.00 4.20 10 -20 3 56.19 6.90 -10 -20 3 52.39 6.60 10 -20 -3 42.20 6.30 10 -20 -3 47.40 5.50 10 -20 4 19.70 5.10 10 -20 -4 18.90 4.30 -10 -20 4 24.00 5.60 10 -20 5 26.00 5.50 10 -20 -5 21.20 4.80 -10 -20 5 27.10 6.10 10 -20 6 3.30 4.50 -10 -20 6 11.70 5.00 10 -20 -6 12.70 4.40 10 -20 7 2.20 4.70 -10 -20 7 13.60 5.70 10 -20 -7 8.20 4.80 10 -20 8 3.60 5.10 -10 -20 8 3.60 5.70 10 -20 -8 -8.50 3.80 -11 -20 0 1.00 2.90 11 -20 0 3.00 3.80 11 -20 0 -2.20 2.10 -11 -20 -1 44.50 5.00 11 -20 1 36.40 4.00 11 -20 1 43.20 6.30 11 -20 -1 42.30 6.20 11 -20 -1 46.80 5.00 -11 -20 1 42.60 5.70 11 -20 2 14.40 2.70 -11 -20 -2 18.60 3.40 11 -20 2 11.50 4.60 11 -20 -2 12.20 3.40 -11 -20 2 19.60 4.50 11 -20 -2 10.90 4.40 11 20 -3 8.20 2.70 11 -20 3 4.90 4.40 11 -20 -3 10.80 3.80 11 -20 -3 4.70 4.20 -11 -20 3 16.70 4.80 11 -20 4 14.80 5.00 11 -20 -4 17.40 4.20 -11 -20 4 23.60 5.70 11 -20 5 10.20 5.10 -11 -20 5 11.80 4.90 11 -20 -5 2.80 3.60 11 -20 6 10.40 4.90 -11 -20 6 12.80 5.40 11 -20 -6 12.90 5.00 11 -20 7 3.60 5.00 11 -20 -7 6.40 4.80 -11 -20 7 2.30 4.80 11 -20 8 5.80 5.30 11 -20 -8 3.20 5.00 -11 -20 8 12.20 5.80 -12 -20 0 17.90 3.90 12 -20 0 20.80 3.60 12 -20 0 10.30 4.40 12 -20 1 42.20 4.30 -12 -20 -1 41.50 5.10 12 -20 1 41.00 6.40 -12 -20 1 46.00 5.90 12 -20 -1 40.70 6.10 12 -20 -1 41.10 4.70 -12 -20 -2 43.70 4.80 12 -20 2 31.90 6.10 12 -20 2 38.60 4.00 12 -20 -2 31.50 4.70 -12 -20 2 53.19 6.60 12 -20 -2 31.20 5.80 12 -20 3 11.50 4.60 12 20 -3 7.90 2.70 -12 -20 3 7.90 4.00 12 -20 -3 13.40 4.10 12 -20 -3 7.60 4.50 12 -20 4 4.50 4.40 12 -20 -4 0.50 3.30 -12 -20 4 5.20 4.10 12 -20 5 -3.80 3.90 12 -20 -5 1.00 3.50 -12 -20 5 4.50 4.50 12 -20 6 34.10 6.50 -12 -20 6 36.00 7.00 12 -20 -6 24.70 5.50 12 -20 7 51.09 7.80 12 20 7 42.60 5.50 -12 -20 7 60.29 8.60 12 -20 -7 50.49 7.20 12 -20 8 4.50 5.30 12 -20 -8 2.00 5.30 -12 -20 8 2.90 5.80 12 20 8 -1.20 3.80 13 -20 0 -2.60 3.60 -13 -20 0 1.80 3.20 13 -20 0 1.20 2.70 13 -20 1 20.30 3.50 13 -20 1 16.00 5.10 -13 -20 -1 24.30 4.40 13 -20 -1 24.30 3.80 -13 -20 1 22.50 4.90 13 -20 -1 16.20 5.00 -13 -20 -2 112.79 7.20 13 -20 2 103.99 9.30 13 -20 2 113.39 6.50 13 -20 -2 116.99 7.60 -13 -20 2 116.89 8.50 13 -20 -2 102.89 9.20 13 -20 3 5.20 4.30 13 20 -3 2.60 2.60 13 -20 -3 -2.90 2.80 -13 -20 3 2.40 3.90 13 -20 -3 -10.70 3.40 13 -20 4 168.78 11.80 -13 -20 4 174.28 11.10 13 -20 -4 157.78 10.40 13 -20 5 2.50 4.70 13 -20 -5 -2.10 3.50 -13 -20 5 3.30 5.20 13 20 5 1.90 2.60 13 -20 6 16.30 5.90 13 20 6 16.70 4.10 -13 -20 6 36.00 7.20 13 -20 -6 19.10 5.40 13 -20 7 -8.80 4.10 -13 -20 7 9.10 5.60 13 20 7 1.00 3.20 13 -20 -7 -1.90 4.20 14 -20 0 41.00 6.40 14 -20 0 33.40 4.60 -14 -20 0 43.10 5.80 14 -20 1 57.69 7.60 14 -20 1 54.69 5.30 -14 -20 -1 59.99 5.80 14 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4 5.60 5.30 15 -20 5 3.20 4.80 -15 -20 5 11.60 5.40 15 -20 -5 8.00 4.30 15 -20 6 12.20 5.90 15 -20 -6 14.00 5.00 -15 -20 6 32.80 7.20 15 -20 7 -3.20 5.10 -15 -20 7 4.40 5.40 15 -20 -7 3.00 4.60 16 -20 0 99.59 9.80 16 -20 0 85.89 7.10 -16 -20 0 106.19 8.30 -16 -20 -1 5.70 3.90 16 -20 1 1.60 2.90 16 -20 1 -0.40 4.40 16 -20 -1 6.70 4.60 16 -20 -1 6.30 3.60 -16 -20 1 8.90 4.30 -16 -20 -2 31.90 5.80 16 -20 2 28.90 6.60 16 -20 -2 42.30 5.90 16 -20 -2 33.30 6.50 -16 -20 2 36.70 6.40 16 20 -3 13.50 3.70 16 -20 3 8.10 5.30 16 -20 -3 8.90 5.30 16 -20 -3 11.10 4.60 -16 -20 3 18.60 5.50 16 -20 4 12.00 5.70 16 -20 -4 10.60 4.90 -16 -20 4 13.10 5.40 16 -20 5 5.80 5.20 -16 -20 5 6.90 4.90 16 -20 -5 0.00 4.40 16 -20 6 19.40 6.40 16 -20 -6 12.20 5.70 -16 -20 6 22.70 6.60 17 -20 0 3.20 3.40 -17 -20 0 6.30 4.00 17 -20 0 2.00 4.60 17 -20 1 22.90 4.30 -17 -20 -1 37.10 6.10 17 -20 1 24.10 6.30 17 -20 -1 15.70 5.60 17 -20 -1 34.20 5.40 -17 -20 1 30.50 5.90 17 -20 2 1.80 5.00 17 -20 -2 11.30 4.40 -17 -20 2 10.30 4.80 17 -20 -2 10.00 5.40 17 -20 3 8.80 5.40 17 20 -3 15.80 4.00 17 -20 -3 19.80 5.20 17 -20 -3 13.80 5.70 -17 -20 3 30.60 6.50 17 -20 4 17.10 6.00 -17 -20 4 35.10 7.00 17 -20 -4 22.40 5.60 17 -20 5 -3.30 5.20 17 -20 -5 3.00 4.80 -17 -20 5 9.70 5.30 18 -20 0 51.39 6.10 18 -20 0 47.00 7.70 -18 -20 0 63.19 7.70 -18 -20 -1 33.90 6.10 18 -20 1 23.40 6.40 18 -20 1 22.90 4.60 -18 -20 1 34.30 6.30 18 -20 -1 29.70 5.20 18 -20 -1 11.10 5.60 18 -20 2 13.40 6.00 18 20 -2 20.20 4.50 -18 -20 2 25.50 6.10 18 -20 -2 24.00 5.10 18 -20 -2 9.70 5.60 18 -20 3 25.10 6.90 18 20 -3 24.10 4.60 18 -20 -3 33.90 6.20 -18 -20 3 53.19 8.10 18 -20 -3 24.50 6.70 -18 20 4 1.40 5.90 18 -20 4 2.10 5.20 -18 -20 4 4.80 5.70 18 -20 -4 3.60 4.70 18 -20 5 7.20 5.80 -18 -20 5 17.70 6.40 18 -20 -5 5.90 5.20 19 -20 0 1.70 4.70 -19 -20 0 8.50 4.80 19 -20 0 -3.40 3.40 19 -20 1 -1.00 3.50 -19 -20 -1 12.60 4.70 19 -20 1 -7.20 4.70 -19 -20 1 7.30 4.80 19 -20 -1 -6.10 4.20 19 -20 -1 -2.70 3.20 19 20 -2 17.60 4.80 19 -20 2 -3.00 4.90 19 -20 -2 7.50 4.20 -19 -20 2 12.30 5.40 19 -20 -2 0.20 5.00 19 20 -3 -2.70 3.10 19 -20 3 -2.70 5.00 -19 -20 3 8.60 5.30 19 -20 -3 -3.90 4.60 19 -20 -3 5.00 4.10 19 -20 4 17.00 6.30 -19 20 4 3.70 6.70 -19 -20 4 28.80 7.20 19 -20 -4 11.10 4.90 -20 -20 0 180.38 12.10 20 -20 0 175.08 13.00 20 -20 0 175.18 11.00 -20 -20 -1 8.90 4.60 20 -20 1 -2.40 4.90 -20 -20 1 6.10 5.30 20 -20 -1 -1.00 4.00 20 -20 -1 -1.70 5.00 20 -20 2 14.20 6.10 20 20 -2 7.10 4.50 20 -20 -2 5.40 4.50 -20 -20 2 26.20 6.70 20 -20 -2 10.00 5.70 0 -21 1 85.39 6.50 0 -21 1 74.69 6.10 0 21 -1 97.39 9.00 0 -21 2 7.90 3.20 0 -21 -2 10.30 3.40 0 -21 2 5.90 3.40 0 -21 3 207.38 10.60 0 -21 3 211.48 11.30 0 -21 -3 211.68 11.20 0 21 -3 217.08 14.00 0 -21 -4 32.70 5.10 0 -21 4 9.80 4.60 0 21 -4 1.00 5.00 0 -21 4 3.60 3.10 0 -21 5 1.90 3.90 0 -21 -5 5.40 3.90 0 -21 5 6.70 3.20 0 21 -5 -0.40 4.90 0 -21 -6 4.00 4.10 0 -21 6 3.30 4.30 0 21 -6 0.60 5.60 0 -21 6 4.30 3.40 0 -21 7 109.29 8.20 0 21 -7 97.19 12.10 0 -21 -7 105.49 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5.20 -4 -23 -2 30.90 4.10 -4 23 2 34.00 5.90 4 -23 2 26.10 4.70 4 -23 -2 28.70 4.40 -4 -23 2 27.60 3.70 -4 -23 2 34.30 5.20 -4 23 -2 31.50 6.70 4 -23 3 23.50 4.40 -4 23 3 20.80 4.60 -4 23 -3 26.60 7.10 4 -23 -3 19.70 4.10 -4 -23 3 18.00 4.40 -4 -23 3 20.60 3.40 4 -23 4 5.30 4.60 4 -23 4 10.80 4.00 4 -23 -4 9.00 3.80 -4 -23 4 2.30 3.80 -4 23 -4 20.00 6.90 4 -23 5 6.00 4.20 4 -23 5 -3.80 4.20 -4 23 -5 10.00 7.20 4 -23 -5 2.10 3.80 -4 -23 5 8.00 4.40 4 -23 6 54.99 8.30 4 23 -6 58.39 10.20 4 -23 6 66.89 7.60 -4 23 -6 57.69 10.30 -4 -23 6 78.79 8.80 4 -23 -6 63.69 7.70 4 -23 7 1.20 3.90 4 -23 7 1.70 5.60 4 23 -7 10.60 7.40 4 -23 -7 -4.70 4.30 -4 -23 7 5.40 5.00 -4 23 -7 8.50 8.30 4 -23 8 3.20 5.90 4 23 -8 1.00 6.80 4 -23 8 0.50 4.50 4 -23 -8 4.50 5.30 -4 23 -8 6.40 7.70 -4 -23 8 12.30 5.70 -5 -23 0 -2.10 2.30 5 -23 0 -0.10 2.20 5 -23 0 0.60 3.20 -5 23 0 -3.30 3.60 5 -23 1 1.90 2.30 5 -23 1 1.90 3.30 -5 -23 -1 -0.50 2.30 -5 23 1 4.90 4.00 5 -23 -1 0.50 2.40 -5 23 -1 -2.00 3.90 -5 -23 1 2.00 3.00 5 -23 -1 0.10 3.20 5 -23 2 25.80 4.90 -5 23 2 17.70 4.80 5 -23 -2 19.90 4.60 5 -23 -2 24.90 3.80 -5 -23 2 22.60 4.80 -5 23 -2 19.80 6.00 5 -23 3 75.79 7.50 -5 23 3 73.99 7.20 -5 23 -3 82.29 10.10 5 -23 -3 73.49 6.20 -5 -23 3 88.29 7.00 5 -23 4 35.50 5.80 -5 -23 4 42.00 6.40 5 -23 -4 29.20 5.20 -5 23 -4 24.40 7.30 5 -23 5 0.60 3.70 5 -23 -5 8.50 4.00 -5 -23 5 6.00 4.30 -5 23 -5 8.00 6.20 5 23 -6 24.30 7.50 5 -23 6 10.90 4.40 5 -23 -6 27.90 6.20 -5 23 -6 12.50 7.80 -5 -23 6 29.10 6.20 5 -23 7 5.90 4.50 5 23 -7 5.90 6.60 5 -23 -7 4.80 4.70 -5 23 -7 6.70 7.30 -5 -23 7 1.70 4.60 5 -23 8 8.60 5.10 5 23 -8 -0.80 6.50 -5 -23 8 12.70 5.80 -5 23 -8 7.70 7.80 5 -23 -8 6.30 6.00 -6 -23 0 41.00 4.90 6 -23 0 40.40 5.70 -6 23 0 41.90 6.70 6 -23 0 39.40 4.10 -6 23 1 21.60 5.50 -6 -23 -1 25.30 3.70 6 -23 1 17.20 4.50 6 -23 -1 20.10 3.40 6 -23 -1 23.60 4.70 -6 23 -1 16.20 5.60 -6 -23 1 23.10 4.10 6 -23 2 -2.70 3.30 -6 23 2 1.60 3.50 6 -23 -2 4.90 3.00 6 -23 -2 -0.80 3.40 -6 23 -2 1.40 5.10 -6 -23 2 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24 -7 -4.90 6.80 7 -24 -7 1.10 4.60 -7 -24 7 5.00 4.90 7 -24 8 2.50 4.90 7 24 -8 2.60 7.00 7 -24 -8 5.00 5.10 -7 -24 8 5.80 5.30 8 -24 0 29.00 5.50 -8 24 0 27.40 6.50 -8 -24 0 25.50 4.30 8 -24 0 21.10 3.40 -8 -24 -1 135.39 7.80 8 -24 1 159.68 10.30 -8 24 -1 154.38 12.50 8 -24 -1 132.69 8.00 -8 -24 1 141.09 8.50 8 -24 -1 138.39 9.30 8 -24 2 -2.20 3.50 -8 -24 2 1.60 3.20 8 -24 -2 1.80 3.00 8 -24 -2 1.40 4.20 -8 24 -2 -3.60 4.60 8 -24 3 24.50 5.40 -8 24 -3 19.80 7.10 -8 -24 3 26.90 5.40 8 -24 -3 23.40 4.40 8 -24 4 25.50 6.10 -8 24 -4 36.50 8.70 8 -24 -4 27.40 5.10 -8 -24 4 27.40 5.70 8 -24 5 5.60 4.50 -8 24 -5 9.80 7.80 -8 -24 5 14.70 5.30 8 -24 -5 15.70 5.00 8 -24 6 9.60 5.10 -8 -24 6 23.70 6.70 8 -24 -6 20.80 5.50 8 -24 7 2.00 5.00 -8 -24 7 2.40 5.00 8 -24 -7 2.10 4.80 -9 -24 0 1.70 2.80 9 -24 0 -4.30 3.50 9 -24 0 -1.10 2.40 9 -24 1 6.10 4.20 -9 -24 -1 2.60 2.70 9 -24 -1 -2.00 3.90 9 -24 -1 -0.20 2.50 -9 -24 1 4.50 3.60 9 -24 2 56.59 7.40 9 -24 -2 63.79 6.30 9 -24 -2 56.89 7.50 -9 -24 2 69.79 6.70 9 -24 3 1.80 4.30 -9 -24 3 2.60 3.70 9 -24 -3 -1.10 3.40 9 -24 4 68.69 8.10 9 -24 -4 72.99 7.30 -9 -24 4 71.09 8.20 9 -24 5 15.10 5.20 9 -24 -5 5.00 4.80 -9 -24 5 15.20 5.50 9 -24 6 2.40 4.90 9 -24 -6 4.40 4.30 -9 -24 6 3.40 5.40 9 -24 7 2.40 4.90 9 -24 -7 6.50 4.80 -9 -24 7 10.90 5.60 10 -24 0 27.70 3.90 -10 -24 0 28.70 4.60 10 -24 0 29.20 6.00 10 -24 1 11.00 4.90 -10 -24 -1 15.10 3.70 10 -24 -1 16.30 3.70 10 -24 -1 7.00 4.60 -10 -24 1 17.20 4.40 10 -24 2 13.90 5.10 -10 -24 2 32.10 5.40 10 -24 -2 24.00 4.40 10 -24 -2 13.90 4.40 10 -24 3 -1.50 4.00 -10 -24 3 6.60 3.90 10 -24 -3 -1.60 3.10 10 -24 4 10.00 5.40 -10 -24 4 13.70 5.00 10 -24 -4 6.00 4.40 10 -24 5 -3.90 4.30 -10 -24 5 4.60 4.50 10 -24 -5 3.60 4.50 10 -24 6 -2.70 4.50 10 -24 -6 -3.00 4.70 -10 -24 6 4.10 4.80 10 -24 7 12.20 5.60 -10 -24 7 17.90 6.00 10 -24 -7 4.90 5.60 -11 -24 0 1.50 3.10 11 -24 0 -4.90 3.70 11 -24 0 0.10 4.00 11 -24 1 0.20 4.00 11 -24 -1 -1.40 2.70 -11 -24 1 5.70 3.60 11 -24 -1 -1.50 4.20 11 -24 2 29.30 6.20 -11 -24 2 34.10 5.60 11 -24 -2 33.10 5.00 11 -24 -2 31.20 6.20 11 -24 3 -7.80 3.80 -11 -24 3 2.40 3.60 11 -24 -3 -3.10 4.40 11 -24 -3 -4.50 2.90 11 -24 4 16.00 5.70 11 -24 -4 9.70 4.60 -11 -24 4 23.70 5.60 11 -24 5 8.60 5.30 -11 -24 5 30.10 6.80 11 -24 -5 15.70 5.40 11 -24 6 4.50 5.30 -11 -24 6 9.90 5.50 11 -24 -6 8.70 5.20 -12 -24 0 36.90 5.30 12 -24 0 29.30 6.00 12 -24 1 35.10 6.00 12 -24 -1 39.20 5.10 -12 -24 1 51.39 6.50 12 -24 -1 42.50 6.90 12 -24 2 0.40 4.50 -12 -24 2 7.90 4.00 12 -24 -2 5.70 3.60 12 -24 -2 1.40 3.60 12 -24 3 13.50 5.50 12 -24 -3 6.40 5.20 -12 -24 3 23.50 5.50 12 -24 -3 16.40 4.30 12 -24 4 7.20 5.20 12 -24 -4 10.70 4.20 -12 -24 4 14.40 5.30 12 -24 5 -0.60 4.50 12 -24 -5 -0.60 3.80 -12 -24 5 5.00 4.70 12 -24 6 -6.30 5.30 12 -24 -6 2.00 4.70 -12 -24 6 6.30 4.90 -13 -24 0 2.40 3.40 13 -24 0 -3.30 4.20 13 -24 1 4.10 4.80 13 -24 -1 4.00 3.30 -13 -24 1 6.80 4.00 13 -24 -1 0.30 4.50 13 -24 2 42.80 7.30 -13 -24 2 39.40 6.30 13 -24 -2 22.10 6.10 13 -24 -2 30.50 5.10 13 -24 3 -0.90 4.80 -13 -24 3 8.70 4.50 13 -24 -3 2.30 5.00 13 -24 -3 -0.80 3.30 13 -24 4 86.09 9.70 13 -24 -4 78.19 8.00 -13 -24 4 74.29 9.20 13 -24 5 2.50 5.00 13 -24 -5 11.00 4.60 -13 -24 5 2.00 4.70 13 -24 6 18.60 6.70 13 -24 -6 16.00 5.90 -13 -24 6 20.70 6.30 -14 -24 0 22.00 4.80 14 -24 0 13.80 5.60 14 -24 1 23.30 6.30 -14 -24 1 39.80 6.30 14 -24 -1 33.20 6.90 14 -24 -1 34.30 5.20 14 -24 2 63.59 8.70 14 -24 -2 60.99 8.40 -14 -24 2 83.19 8.10 14 -24 -2 71.39 7.30 14 -24 3 14.30 5.90 -14 -24 3 20.90 5.80 14 -24 -3 25.70 5.40 14 -24 -3 11.50 5.70 14 -24 4 7.80 5.50 14 -24 -4 26.60 5.70 -14 -24 4 22.00 6.10 14 -24 5 -1.70 4.80 -14 -24 5 15.80 5.80 14 -24 -5 -1.90 4.10 15 -24 0 -0.20 4.80 -15 -24 0 7.50 3.90 15 -24 1 -2.90 4.80 15 -24 -1 6.80 5.30 15 -24 -1 4.30 3.30 -15 -24 1 5.20 3.90 15 -24 2 5.00 4.30 -15 -24 2 7.90 4.30 15 -24 -2 0.40 4.90 15 -24 -2 2.40 3.50 15 -24 3 5.70 5.60 -15 -24 3 26.50 6.30 15 -24 -3 19.50 6.20 15 -24 -3 11.70 4.30 15 -24 4 6.80 6.10 15 -24 -4 8.90 4.60 -15 -24 4 27.30 6.60 -16 -24 0 61.49 7.60 16 -24 0 50.59 8.00 16 -24 1 3.60 5.40 16 -24 -1 1.70 3.80 -16 -24 1 12.70 4.90 16 -24 -1 -4.90 5.10 16 -24 2 48.80 8.10 16 -24 -2 42.70 6.40 16 -24 -2 32.90 7.20 -16 -24 2 70.19 8.50 16 -24 3 2.60 5.60 -16 -24 3 14.20 5.30 16 -24 -3 8.20 4.70 16 -24 -3 -6.90 4.80 16 -24 4 -7.40 4.60 -16 -24 4 4.90 4.90 16 -24 -4 3.80 4.40 17 -24 0 2.50 5.00 17 -24 1 -1.50 5.20 -17 -24 1 9.80 5.00 17 -24 -1 4.40 5.50 17 -24 2 41.60 8.10 17 -24 -2 29.00 5.80 17 -24 -2 37.80 7.50 -17 -24 2 47.60 7.50 18 -24 0 198.98 14.20 0 25 0 3.90 4.10 0 -25 0 4.30 3.00 0 -25 1 0.40 2.90 0 25 -1 -3.30 3.80 0 25 1 1.30 4.10 0 -25 1 -0.80 2.70 0 25 -2 -1.40 4.70 0 -25 2 -1.90 3.20 0 -25 2 -2.50 2.60 0 25 2 -0.60 3.60 0 25 -3 27.90 7.70 0 -25 3 16.00 3.90 0 -25 3 23.40 5.40 0 -25 -3 23.70 4.80 0 25 3 24.90 5.40 0 -25 4 -2.70 3.90 0 -25 4 -3.50 3.00 0 25 -4 1.00 6.30 0 25 4 2.40 4.20 0 -25 -4 -1.60 4.00 0 -25 5 -1.40 3.30 0 25 -5 3.70 6.70 0 -25 -5 3.20 4.30 0 -25 5 2.50 4.30 0 -25 6 6.50 5.00 0 -25 6 6.00 4.00 0 25 -6 -3.90 6.20 0 -25 -6 1.70 4.80 0 25 -7 36.30 10.30 0 -25 7 35.80 7.80 0 -25 -7 45.70 7.70 0 -25 8 9.50 6.10 0 -25 -8 10.80 5.90 0 25 -8 -5.30 6.90 -1 25 0 -6.00 3.80 1 -25 0 -1.70 2.80 -1 -25 0 -4.40 2.50 1 -25 1 2.30 3.60 1 25 -1 -2.80 4.30 -1 25 1 -0.20 4.20 1 -25 1 0.80 2.90 -1 25 -1 4.40 4.50 -1 -25 1 -3.00 2.80 -1 -25 1 0.40 3.30 1 -25 2 5.20 4.20 1 -25 2 6.30 3.20 -1 25 2 7.40 4.40 1 25 -2 4.30 5.00 -1 25 -2 11.50 5.60 1 -25 -2 9.40 3.80 -1 -25 2 7.00 4.20 -1 -25 2 4.00 3.20 -1 25 3 7.20 4.30 1 -25 3 17.20 5.00 1 -25 3 12.70 3.80 1 25 -3 13.80 6.40 -1 -25 3 16.00 3.80 1 -25 -3 18.40 4.50 -1 25 -3 16.50 6.90 -1 -25 3 10.60 4.50 1 -25 4 4.60 3.60 1 25 -4 12.70 6.90 1 -25 4 2.70 4.40 1 25 4 5.60 3.80 -1 25 -4 -7.20 5.10 -1 -25 4 2.40 3.20 -1 -25 4 6.60 4.30 1 -25 -4 5.70 4.30 1 25 -5 48.80 9.60 1 -25 5 55.59 8.10 1 -25 5 55.89 6.40 -1 25 -5 39.20 8.80 1 -25 -5 53.39 7.00 -1 -25 5 50.99 5.80 -1 -25 5 58.99 7.90 -1 -25 -6 11.70 5.40 1 -25 6 3.30 4.10 1 -25 6 21.50 6.40 1 25 -6 11.30 8.10 -1 25 -6 25.20 8.30 1 -25 -6 19.60 5.90 -1 -25 6 19.80 6.10 1 25 -7 5.60 7.00 1 -25 7 3.10 6.10 -1 25 -7 2.50 7.10 1 -25 -7 4.30 5.50 -1 -25 7 4.70 5.50 1 25 -8 14.30 8.50 1 -25 8 8.60 6.20 1 -25 -8 5.60 5.30 -1 -25 8 14.40 6.30 -1 25 -8 7.20 8.20 -2 25 0 1.00 3.80 2 -25 0 3.10 3.20 -2 -25 0 -1.30 2.80 2 -25 1 -2.40 2.90 -2 25 1 -0.90 3.60 -2 -25 -1 -2.90 2.60 2 -25 -1 -0.50 2.90 -2 -25 1 2.50 3.30 -2 -25 1 -1.00 2.80 -2 25 -1 -2.50 3.80 2 -25 2 6.70 4.30 2 -25 2 15.80 4.00 -2 25 2 11.20 4.50 -2 -25 2 12.60 4.50 2 -25 -2 7.20 3.40 -2 25 -2 5.30 5.20 -2 -25 2 7.70 3.20 -2 25 3 20.70 5.10 2 -25 3 23.40 4.90 2 -25 3 25.70 5.60 2 25 -3 33.60 7.30 -2 -25 3 18.10 3.80 2 -25 -3 17.50 4.50 -2 25 -3 28.80 7.30 -2 -25 3 22.70 5.10 2 -25 4 -0.50 4.20 2 25 -4 1.20 5.50 2 -25 4 -1.30 3.40 -2 25 -4 -4.50 5.30 -2 -25 4 1.30 4.30 -2 -25 4 -0.20 2.90 2 -25 -4 5.20 4.30 2 -25 5 14.50 5.60 2 -25 5 17.90 4.80 2 25 -5 9.40 6.50 -2 -25 5 15.40 5.80 2 -25 -5 12.10 4.90 -2 25 -5 19.70 7.40 2 -25 6 106.49 8.90 2 25 -6 109.09 13.30 2 -25 6 113.79 10.10 2 -25 -6 112.39 10.80 -2 -25 6 133.99 10.30 -2 25 -6 98.59 13.10 2 -25 7 10.50 4.40 2 25 -7 10.60 7.70 2 -25 7 10.70 6.30 2 -25 -7 13.70 5.40 -2 25 -7 12.90 8.30 -2 -25 7 28.20 7.50 2 25 -8 109.29 14.50 2 -25 8 126.29 11.30 2 -25 -8 101.59 10.90 -2 25 -8 112.29 15.10 -2 -25 8 124.89 11.70 -3 -25 0 -0.20 2.90 3 -25 0 -2.70 3.60 3 -25 0 -6.20 2.90 -3 25 0 3.80 4.60 -3 -25 -1 1.30 2.80 -3 25 1 11.20 4.50 3 -25 1 3.50 3.50 -3 -25 1 7.40 3.70 3 -25 -1 5.90 3.70 3 -25 -1 0.90 2.90 -3 25 -1 3.50 5.00 -3 25 2 9.60 4.40 3 -25 2 12.60 4.30 3 -25 -2 6.20 3.40 -3 -25 2 7.10 4.10 -3 -25 2 2.30 2.80 -3 25 -2 13.10 5.50 -3 25 3 147.19 10.10 3 -25 3 143.49 9.20 -3 -25 3 141.49 8.30 -3 -25 3 146.19 9.40 3 -25 -3 129.59 8.60 -3 25 -3 132.39 12.40 3 25 -4 22.60 7.00 3 -25 4 12.00 5.30 3 -25 4 18.10 4.60 -3 25 -4 24.80 7.60 -3 -25 4 28.70 5.70 3 -25 -4 21.40 5.20 3 -25 5 11.00 5.50 3 -25 5 1.60 4.20 3 25 -5 0.10 5.70 -3 -25 5 18.30 5.60 -3 25 -5 12.00 6.90 3 -25 -5 7.60 5.20 3 -25 6 16.10 5.00 3 25 -6 22.50 8.20 3 -25 6 17.20 6.40 -3 -25 6 31.50 7.50 -3 25 -6 26.60 8.70 3 -25 -6 22.70 6.10 3 -25 7 4.90 5.80 3 -25 7 2.10 4.30 3 25 -7 12.40 7.80 -3 25 -7 6.80 7.50 -3 -25 7 10.80 5.80 3 -25 -7 15.80 5.60 3 -25 8 6.10 6.20 3 -25 8 4.80 4.70 3 25 -8 -0.70 7.10 3 -25 -8 -0.50 5.20 -3 25 -8 -1.20 7.70 -3 -25 8 16.70 6.90 -4 25 0 14.50 5.00 4 -25 0 13.40 4.60 -4 -25 0 14.10 3.80 4 -25 1 -1.00 3.10 -4 25 1 4.00 4.30 -4 -25 -1 1.40 2.70 -4 -25 1 1.60 3.10 4 -25 -1 -0.80 2.60 -4 25 -1 3.80 4.40 4 -25 -1 -1.00 3.40 4 -25 2 2.80 3.50 -4 25 2 4.50 4.10 -4 -25 2 -2.50 2.40 4 -25 -2 4.40 3.30 -4 25 -2 3.30 5.30 -4 -25 2 3.20 3.60 -4 25 3 2.10 3.90 4 -25 3 3.70 3.50 -4 25 -3 1.50 5.20 -4 -25 3 8.80 4.60 4 -25 -3 1.20 3.40 4 -25 4 35.50 5.80 -4 25 -4 43.90 9.60 -4 -25 4 43.60 6.70 4 -25 -4 42.70 6.20 4 25 -5 -6.60 5.70 4 -25 5 11.20 4.40 -4 25 -5 19.80 7.60 4 -25 -5 5.70 4.40 -4 -25 5 18.00 5.80 4 -25 6 0.30 5.30 4 -25 6 -2.20 3.60 4 25 -6 0.20 6.50 -4 25 -6 11.80 7.40 -4 -25 6 7.60 5.10 4 -25 -6 2.50 5.10 4 -25 7 1.50 5.70 4 25 -7 6.20 7.20 4 -25 7 -4.30 3.60 4 -25 -7 -2.00 4.90 -4 25 -7 9.30 7.60 -4 -25 7 3.00 4.90 4 -25 8 -5.80 5.80 4 25 -8 18.50 8.70 4 -25 8 4.10 4.90 4 -25 -8 11.20 6.10 -4 -25 8 5.90 6.50 -4 25 -8 -4.10 7.30 -5 -25 0 3.00 2.90 5 -25 0 2.50 3.70 -5 25 0 4.90 4.70 -5 -25 -1 11.80 3.40 5 -25 1 11.00 4.20 -5 25 1 19.30 5.40 -5 -25 1 22.50 4.60 5 -25 -1 13.30 3.30 -5 25 -1 15.40 6.30 5 -25 -1 9.40 4.10 5 -25 2 -1.90 3.20 -5 25 2 3.60 4.00 -5 -25 2 1.20 3.50 5 -25 -2 3.20 3.20 -5 25 -2 -3.90 5.10 5 -25 3 4.90 3.90 -5 25 3 12.00 4.50 -5 -25 3 9.60 4.60 -5 25 -3 6.00 5.60 5 -25 -3 9.50 3.90 5 -25 4 39.70 6.30 -5 25 -4 32.30 8.00 -5 -25 4 57.59 7.30 5 -25 -4 42.90 6.20 5 -25 5 25.30 5.80 -5 25 -5 20.30 8.60 5 -25 -5 24.90 5.40 -5 -25 5 29.40 6.10 5 25 -6 6.40 7.00 5 -25 6 8.70 4.50 -5 -25 6 17.10 5.90 -5 25 -6 15.90 7.80 5 -25 -6 9.30 5.00 5 -25 7 8.60 5.10 5 25 -7 -2.20 6.90 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2 49.10 6.60 -7 -25 2 53.49 6.60 -7 25 -2 48.30 8.70 7 -25 -2 46.60 6.60 7 -25 -2 51.39 5.60 7 -25 3 2.40 4.00 -7 -25 3 11.00 4.50 -7 25 -3 2.80 5.30 7 -25 -3 -0.10 3.30 7 -25 4 41.30 6.40 7 -25 -4 43.70 6.30 -7 -25 4 45.60 6.80 -7 25 -4 43.20 9.20 7 -25 5 11.40 4.90 -7 -25 5 17.10 5.30 7 -25 -5 20.80 5.60 -7 25 -5 12.00 7.60 7 -25 6 16.60 5.40 7 -25 -6 22.90 5.80 -7 25 -6 13.80 7.90 -7 -25 6 33.30 7.00 7 25 -7 -6.10 6.40 7 -25 7 3.90 5.20 7 -25 -7 -3.10 4.40 -7 25 -7 -2.10 7.40 -7 -25 7 4.00 5.00 -8 -25 0 72.89 6.00 8 -25 0 66.59 7.70 -8 25 0 74.29 9.50 8 -25 1 11.40 4.60 -8 -25 1 17.40 4.40 -8 25 -1 17.60 6.50 8 -25 -1 16.30 3.60 8 -25 -1 4.40 4.20 8 -25 2 3.10 4.10 8 -25 -2 0.80 3.20 -8 -25 2 5.20 3.50 -8 25 -2 2.90 5.40 8 -25 -2 -1.90 4.00 8 -25 3 0.60 3.80 -8 25 -3 -0.60 5.10 8 -25 -3 0.20 3.10 -8 -25 3 2.10 3.70 8 -25 4 9.30 4.80 -8 25 -4 4.60 6.50 -8 -25 4 19.00 5.20 8 -25 -4 15.80 4.50 8 -25 5 -4.20 3.80 8 -25 -5 1.90 3.90 -8 25 -5 5.80 7.90 -8 -25 5 5.80 4.40 8 -25 6 2.00 4.40 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21.10 5.10 3 -26 4 4.90 3.60 3 26 -4 14.20 6.60 3 -26 4 3.00 4.50 -3 26 -4 3.00 6.10 3 -26 -4 5.10 4.00 -3 -26 4 9.00 4.70 3 -26 5 63.09 8.80 3 -26 5 56.69 6.90 3 26 -5 59.49 10.30 3 -26 -5 61.19 7.60 -3 -26 5 66.59 8.50 -3 26 -5 57.19 10.40 3 -26 6 0.80 3.90 3 26 -6 7.40 6.90 3 -26 6 1.90 5.30 -3 -26 6 0.90 4.80 -3 26 -6 5.60 7.80 3 -26 -6 -0.90 5.00 3 -26 7 -4.10 5.20 3 -26 7 -3.60 4.10 3 26 -7 -2.70 7.80 3 -26 -7 4.00 5.00 -3 26 -7 -7.60 7.90 -3 -26 7 5.80 6.00 -4 -26 0 78.39 6.20 4 -26 0 57.29 6.80 -4 26 0 76.29 9.30 4 -26 1 30.80 5.20 -4 26 1 26.40 6.40 4 -26 -1 34.70 4.60 -4 26 -1 26.80 7.20 4 -26 -1 26.00 5.20 -4 -26 1 32.90 5.40 -4 26 2 9.40 4.60 4 -26 2 8.00 3.90 -4 -26 2 2.00 3.50 -4 26 -2 6.60 5.70 4 -26 -2 4.50 3.30 4 -26 3 21.70 4.90 -4 26 3 25.70 5.50 4 -26 -3 25.70 5.20 -4 -26 3 32.50 5.80 -4 26 -3 30.40 7.50 4 -26 4 -1.60 3.40 4 -26 -4 0.80 3.70 -4 -26 4 3.50 4.10 -4 26 -4 4.60 6.30 4 26 -5 -12.80 5.10 4 -26 5 1.00 3.90 -4 26 -5 2.20 6.50 -4 -26 5 8.70 4.90 4 -26 -5 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1.20 5.00 -7 -26 4 9.50 5.20 -7 26 -4 10.10 7.20 7 -26 -4 10.30 4.60 7 -26 5 -2.00 3.90 -7 26 -5 -0.40 6.50 7 -26 -5 11.80 4.70 -7 -26 5 4.30 4.60 7 -26 6 6.60 5.40 -7 26 -6 4.30 7.40 -7 -26 6 13.30 5.50 7 -26 -6 1.60 4.30 7 26 -7 0.50 7.10 7 -26 7 -0.80 5.00 -7 -26 7 14.80 6.30 -7 26 -7 -12.60 6.60 7 -26 -7 -9.70 4.00 8 -26 0 36.20 6.70 -8 -26 0 49.90 5.80 -8 26 0 37.20 7.50 8 -26 1 51.09 7.30 -8 -26 1 61.79 6.70 8 -26 -1 50.09 7.10 -8 26 -1 55.09 8.90 8 -26 -1 37.80 5.50 8 -26 2 42.80 6.60 8 -26 -2 43.60 6.80 -8 -26 2 43.60 6.10 -8 26 -2 34.60 7.90 8 -26 -2 35.40 5.00 8 -26 3 19.30 5.20 8 -26 -3 17.80 4.50 -8 26 -3 6.50 6.10 -8 -26 3 17.30 4.90 8 -26 4 7.90 4.90 -8 -26 4 15.80 5.50 8 -26 -4 14.30 4.60 -8 26 -4 2.90 6.60 8 -26 5 2.20 5.10 -8 26 -5 4.80 7.10 8 -26 -5 14.40 4.90 -8 -26 5 22.20 5.70 8 -26 6 2.30 4.60 8 -26 -6 4.30 4.50 -8 -26 6 3.00 4.80 9 -26 0 2.80 4.50 -9 -26 0 6.90 3.50 9 -26 1 -3.00 4.00 -9 -26 1 6.50 3.40 9 -26 -1 2.30 4.30 9 -26 2 27.10 5.90 9 -26 -2 27.10 4.60 9 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11.20 5.90 6 -28 6 4.50 4.60 6 28 -6 3.50 8.00 6 -28 -6 5.40 6.00 -6 -28 6 23.40 6.60 -6 28 -6 13.10 8.20 7 -28 0 -3.80 4.00 -7 28 0 -6.20 4.90 7 -28 1 4.60 4.60 -7 28 1 10.10 5.70 -7 28 -1 0.80 5.20 7 -28 -1 4.80 4.70 -7 -28 1 11.20 4.30 7 -28 2 51.49 7.50 -7 -28 2 48.40 7.00 -7 28 -2 32.30 8.20 7 -28 3 18.60 5.40 -7 28 -3 17.20 7.50 7 -28 -3 16.40 4.60 -7 -28 3 17.20 5.30 7 -28 4 8.50 4.80 -7 28 -4 3.20 7.60 7 -28 -4 13.50 4.70 -7 -28 4 12.90 5.20 7 -28 5 4.30 5.40 7 -28 -5 -0.80 5.10 -7 28 -5 -8.00 7.50 -7 -28 5 1.70 5.40 8 -28 0 37.60 6.70 8 -28 1 29.10 6.00 -8 -28 1 25.30 5.10 -8 28 -1 25.30 7.20 8 -28 -1 24.80 6.00 8 -28 2 84.19 9.10 -8 28 -2 89.39 12.00 -8 -28 2 83.69 7.40 8 -28 3 -4.80 4.10 8 -28 -3 4.10 4.00 -8 -28 3 7.10 4.70 -8 28 -3 -6.30 5.40 8 -28 4 7.40 4.80 -8 28 -4 -2.40 6.70 8 -28 -4 12.10 5.00 -8 -28 4 12.70 5.20 8 -28 5 14.50 5.50 -8 28 -5 -2.20 7.10 8 -28 -5 17.60 5.90 -8 -28 5 17.00 6.40 9 -28 0 -4.50 4.20 9 -28 1 3.90 4.70 9 -28 -1 7.80 5.30 -9 -28 1 12.30 4.40 9 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108.79 9.10 13 -28 -2 84.09 10.20 14 -28 0 41.20 8.00 0 29 0 3.50 5.00 0 29 -1 66.79 10.40 0 -29 1 64.39 7.00 0 29 1 58.09 8.60 0 29 -2 0.70 5.90 0 -29 2 3.20 4.50 0 -29 2 -0.30 3.60 0 29 2 -0.70 5.00 0 29 -3 1.60 5.90 0 -29 3 2.90 4.90 0 -29 3 -2.40 4.10 0 -29 4 0.30 4.70 0 29 -4 -6.00 6.00 0 29 -5 4.40 7.50 0 -29 5 4.50 5.30 0 29 -6 -4.90 6.70 0 -29 6 0.40 5.40 -1 29 0 0.70 4.80 1 29 0 -0.20 4.60 1 29 -1 23.60 7.10 -1 29 1 25.80 6.90 1 -29 1 13.60 4.90 1 29 1 18.40 6.00 -1 -29 1 23.30 5.30 -1 29 -1 23.40 7.50 1 -29 2 -4.40 3.80 1 29 -2 0.50 5.60 -1 29 2 -2.80 4.80 -1 -29 2 -4.30 4.50 1 29 2 -0.10 4.80 -1 29 -2 -2.00 5.30 -1 -29 2 0.50 4.40 1 29 -3 61.89 10.30 1 -29 3 67.29 8.40 1 -29 3 68.49 7.20 -1 29 -3 51.39 9.70 -1 -29 3 80.39 9.00 1 29 3 59.19 8.40 1 -29 4 15.50 6.30 1 29 -4 22.90 8.40 -1 29 -4 3.40 6.80 -1 -29 4 20.70 6.60 1 29 -5 11.30 7.70 1 -29 5 18.00 6.30 -1 29 -5 11.90 8.00 -1 -29 5 16.40 6.30 1 29 -6 15.30 8.40 1 -29 6 7.20 5.80 -1 29 -6 0.20 7.30 -1 -29 6 10.90 5.90 1 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44.70 10.00 3 29 -4 2.50 7.70 3 -29 4 -0.30 4.40 -3 29 -4 2.00 7.50 -3 -29 4 -1.60 5.00 3 -29 -4 -1.40 3.70 3 -29 5 22.40 5.80 3 29 -5 24.80 9.60 -3 -29 5 29.00 7.40 -3 29 -5 19.70 8.90 3 -29 -5 27.60 6.70 -4 29 0 21.40 7.30 4 -29 0 20.60 5.70 4 -29 1 4.60 4.30 -4 29 1 7.70 5.80 -4 29 -1 2.80 6.20 -4 -29 1 13.00 4.70 4 -29 2 0.00 3.90 -4 29 2 5.80 5.50 -4 29 -2 1.30 6.30 -4 -29 2 0.00 4.40 4 -29 3 0.70 4.60 4 29 -3 2.60 6.80 4 -29 -3 -1.40 4.20 -4 29 -3 3.30 6.10 -4 -29 3 0.70 4.20 4 29 -4 4.50 7.30 4 -29 4 7.90 4.90 4 -29 -4 7.60 5.00 -4 29 -4 -4.60 6.20 -4 -29 4 8.60 5.20 4 29 -5 7.10 8.00 4 -29 5 4.40 5.10 -4 29 -5 6.20 8.40 4 -29 -5 6.40 5.10 -4 -29 5 7.90 5.70 5 -29 0 -2.20 3.90 -5 29 0 -5.50 5.00 -5 29 1 0.40 5.10 5 -29 1 4.40 4.80 -5 -29 1 7.90 4.40 -5 29 -1 -0.10 5.80 5 -29 -1 3.60 4.60 5 -29 2 50.79 7.10 -5 29 2 49.90 8.10 -5 -29 2 68.39 8.20 -5 29 -2 41.10 9.40 5 -29 3 81.19 8.80 -5 -29 3 84.59 9.50 5 -29 -3 65.99 7.70 -5 29 -3 73.69 11.20 5 -29 4 2.40 4.90 5 29 -4 3.50 6.60 5 -29 -4 7.70 5.00 -5 29 -4 3.60 7.00 -5 -29 4 5.00 4.90 5 -29 5 -2.30 4.60 5 29 -5 13.80 7.50 -5 29 -5 -4.60 6.70 -5 -29 5 -1.00 5.00 5 -29 -5 -1.80 5.10 -6 29 0 33.60 7.40 6 -29 0 34.40 6.40 -6 29 1 35.90 7.60 6 -29 1 28.00 5.90 -6 29 -1 30.80 8.20 6 -29 -1 32.00 6.30 -6 -29 1 40.90 6.50 6 -29 2 14.50 5.30 -6 -29 2 33.10 5.90 -6 29 -2 16.80 7.10 6 -29 3 26.40 6.10 6 -29 -3 29.50 6.60 -6 -29 3 31.60 6.20 -6 29 -3 29.80 9.20 6 -29 4 1.50 4.90 -6 29 -4 2.10 7.20 -6 -29 4 9.90 5.20 6 -29 -4 1.80 4.70 6 -29 5 8.00 4.80 6 29 -5 5.70 7.40 6 -29 -5 8.80 5.60 -6 -29 5 11.80 5.90 -6 29 -5 11.20 8.10 7 -29 0 -1.60 4.30 -7 29 0 3.60 5.80 -7 29 1 18.80 6.90 7 -29 1 33.40 6.90 -7 -29 1 35.10 9.30 -7 29 -1 25.70 8.50 7 -29 -1 25.40 6.10 7 -29 2 39.10 6.70 -7 29 -2 20.30 7.50 -7 -29 2 35.00 6.50 7 -29 3 12.00 5.30 -7 29 -3 20.80 8.00 -7 -29 3 26.00 6.10 7 -29 4 20.50 5.90 -7 29 -4 23.20 8.80 -7 -29 4 17.80 6.40 7 -29 -4 20.30 5.60 7 -29 5 14.50 5.90 7 -29 -5 10.70 5.70 -7 29 -5 16.60 8.70 -7 -29 5 21.30 6.60 8 -29 0 -5.70 4.20 8 -29 1 9.70 5.10 -8 29 -1 7.40 6.90 8 -29 -1 2.20 4.80 8 -29 2 13.00 5.90 -8 -29 2 28.60 5.60 -8 29 -2 20.90 7.60 8 -29 3 4.50 4.60 -8 -29 3 13.70 5.40 -8 29 -3 8.40 6.90 8 -29 4 -1.90 4.90 -8 -29 4 11.90 5.50 -8 29 -4 2.10 7.70 8 -29 -4 -2.30 4.70 9 -29 0 -5.90 4.90 9 -29 1 1.00 4.70 9 -29 -1 -1.20 4.90 9 -29 2 4.30 4.90 -9 -29 2 2.50 4.20 9 -29 3 -3.30 4.50 -9 -29 3 9.30 5.20 9 -29 4 -1.20 4.60 -9 -29 4 10.70 5.50 9 -29 -4 3.90 4.90 10 -29 0 5.30 5.30 10 -29 1 72.69 9.00 10 -29 -1 66.09 8.50 10 -29 2 5.10 5.80 10 -29 -2 -4.50 5.10 -10 -29 2 15.70 5.20 10 -29 3 -0.80 4.80 -10 -29 3 12.60 5.50 11 -29 0 -0.70 5.70 11 -29 1 -0.20 4.90 11 -29 -1 2.30 5.20 11 -29 2 6.80 5.60 11 -29 -2 9.30 5.70 -11 -29 2 16.80 5.40 11 -29 3 -5.60 5.60 -11 -29 3 -0.10 4.60 12 -29 0 9.40 6.10 12 -29 1 22.10 6.70 12 -29 -1 18.00 7.00 12 -29 2 -5.80 5.10 -12 -29 2 9.80 5.20 0 30 0 222.08 15.60 0 30 -1 2.80 6.20 0 30 1 -0.90 5.60 0 -30 2 70.59 8.50 0 30 2 73.19 9.70 0 -30 2 65.89 7.90 0 30 -2 70.19 11.20 0 -30 3 -0.70 4.90 0 30 -3 12.80 7.80 0 30 -4 16.40 8.10 0 -30 4 23.00 7.00 0 -30 5 -6.40 5.60 0 30 -5 5.20 7.50 1 30 0 -4.30 5.60 -1 30 0 -7.90 4.50 1 30 -1 23.50 7.40 -1 30 1 2.00 5.70 1 -30 1 15.90 4.70 -1 30 -1 7.40 6.70 1 30 1 18.30 6.60 1 -30 2 2.70 4.20 -1 30 2 2.80 5.20 1 30 -2 12.40 6.90 1 30 2 1.40 5.70 -1 -30 2 12.70 5.00 -1 30 -2 7.30 6.30 1 -30 3 16.60 5.60 1 30 -3 33.50 8.80 -1 -30 3 24.90 6.10 -1 30 -3 11.50 7.40 1 30 -4 5.20 6.90 1 -30 4 0.90 4.90 -1 -30 4 -1.40 4.80 -1 30 -4 -3.90 6.80 1 30 -5 9.80 8.50 1 -30 5 -2.90 5.20 -1 -30 5 4.50 5.50 -1 30 -5 14.50 8.30 -2 30 0 1.10 5.20 2 30 0 3.40 6.00 2 30 -1 14.60 7.20 -2 30 1 8.70 6.20 2 -30 1 18.50 4.80 2 30 1 10.00 6.10 -2 30 -1 11.40 6.50 -2 -30 1 23.60 8.10 2 30 -2 2.60 6.50 -2 30 2 6.00 5.50 2 -30 2 3.40 4.50 -2 30 -2 6.60 7.00 2 30 2 13.90 6.20 -2 -30 2 4.50 4.70 2 30 -3 0.10 6.20 2 -30 3 8.70 4.20 -2 -30 3 9.60 5.50 -2 30 -3 -0.10 7.00 2 -30 4 13.70 8.60 2 30 -4 16.70 8.70 -2 -30 4 7.00 6.10 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1 147.59 11.40 -8 30 -1 157.98 14.60 8 -30 -1 135.29 11.40 8 -30 2 34.10 6.60 -8 -30 2 28.00 6.10 -8 30 -2 35.60 9.20 8 -30 3 14.40 5.80 -8 30 -3 11.90 8.30 -8 -30 3 29.50 6.60 9 -30 0 0.50 5.00 9 -30 1 -6.40 5.40 9 -30 -1 2.10 5.20 9 -30 2 -2.90 5.30 -9 -30 2 12.40 5.60 9 -30 3 -0.10 5.40 -9 -30 3 10.20 5.20 10 -30 0 41.40 7.60 10 -30 1 21.00 6.50 10 -30 -1 20.90 6.40 10 -30 2 22.10 6.40 11 -30 0 1.70 5.50 0 31 0 -5.40 5.60 0 31 -1 -2.20 6.30 0 31 1 -6.40 5.40 0 31 2 2.00 5.70 0 31 -2 0.10 6.80 0 31 -3 -0.40 7.00 0 -31 3 -1.40 4.50 0 31 -4 -3.10 6.80 0 -31 4 1.00 5.60 -1 31 0 -6.50 4.60 1 31 0 -4.70 5.70 -1 31 1 11.70 6.70 1 -31 1 1.50 4.50 1 31 -1 6.50 6.40 -1 31 -1 3.00 7.00 1 31 1 -4.20 5.80 1 31 -2 -3.50 5.80 1 -31 2 -1.70 3.60 -1 31 2 5.20 5.40 -1 -31 2 0.90 4.70 -1 31 -2 4.30 6.30 1 31 2 -2.10 5.30 1 31 -3 10.40 7.00 -1 -31 3 -1.00 5.20 -1 31 -3 3.50 6.30 1 -31 4 3.80 5.20 1 31 -4 -9.30 7.10 -1 31 -4 -0.40 7.00 -1 -31 4 6.00 5.50 -2 31 0 128.19 12.30 2 31 0 132.59 12.50 2 -31 1 -1.80 4.30 -2 31 1 2.00 5.90 2 31 -1 3.70 6.60 2 31 1 0.10 5.80 -2 31 -1 9.50 6.50 -2 31 2 36.30 9.20 2 -31 2 29.60 5.60 2 31 -2 42.50 9.80 -2 31 -2 50.39 10.50 2 31 2 35.30 7.90 -2 -31 2 43.80 7.20 2 31 -3 -2.30 6.10 2 -31 3 -3.20 4.40 -2 31 -3 0.80 6.10 -2 -31 3 -5.30 4.30 2 31 -4 3.70 8.00 -2 -31 4 1.00 5.30 -2 31 -4 1.20 7.50 -3 31 0 -4.80 4.70 3 31 0 -2.10 5.40 3 -31 1 -4.90 3.60 3 31 -1 10.50 6.10 -3 31 1 -1.60 5.60 -3 31 -1 -0.60 5.40 3 31 1 4.30 5.10 3 31 -2 0.70 5.80 3 -31 2 2.40 4.70 3 31 2 2.70 5.50 -3 31 -2 0.80 5.90 -3 -31 2 -3.20 4.50 3 31 -3 5.00 6.90 3 -31 3 1.70 4.70 -3 31 -3 -1.30 6.10 -3 -31 3 5.90 5.60 3 31 -4 3.50 8.30 -3 -31 4 3.20 5.80 -3 31 -4 13.30 8.00 -4 31 0 40.30 8.60 4 -31 0 37.60 6.60 -4 31 1 9.80 6.50 4 -31 1 -0.80 4.80 4 31 -1 5.90 5.90 -4 31 -1 7.40 7.00 4 -31 2 19.20 5.30 4 31 -2 14.00 7.10 -4 -31 2 19.70 6.10 -4 31 -2 13.60 7.00 4 -31 3 6.10 4.50 4 31 -3 2.10 7.10 -4 -31 3 4.70 5.40 -4 31 -3 -0.90 6.60 4 -31 4 28.30 6.10 4 31 -4 33.00 10.10 -4 31 -4 25.80 9.10 -4 -31 4 47.60 8.40 -5 31 0 4.90 5.70 5 -31 0 -5.60 4.20 -5 31 1 1.00 5.60 5 -31 1 -4.10 4.20 -5 31 -1 5.40 6.60 5 -31 2 44.70 7.20 -5 31 -2 43.40 9.70 -5 -31 2 59.09 9.50 5 -31 3 40.80 6.80 5 31 -3 44.80 10.10 -5 -31 3 43.00 7.80 -5 31 -3 33.70 9.30 6 -31 0 29.30 6.80 -6 31 0 35.60 8.00 6 -31 1 81.49 8.80 -6 31 1 87.49 11.00 -6 31 -1 74.29 11.30 6 -31 2 -0.70 4.40 -6 31 -2 -0.90 6.00 6 -31 3 54.39 7.50 -6 -31 3 51.19 8.00 -6 31 -3 43.80 10.60 7 -31 0 4.20 5.50 -7 31 0 0.40 6.10 7 -31 1 8.80 5.20 -7 31 1 8.10 6.30 -7 31 -1 8.30 7.00 7 -31 -1 0.10 5.10 7 -31 2 -1.20 4.50 -7 31 -2 4.90 6.90 8 -31 0 42.20 7.50 8 -31 1 14.90 6.50 8 -31 -1 12.00 6.00 8 -31 2 17.50 6.50 -8 31 -2 2.50 7.30 9 -31 0 -5.50 4.60 9 -31 1 4.30 5.30 9 -31 -1 4.00 5.50 0 32 0 35.60 8.80 0 32 -1 -1.40 6.20 0 32 1 5.20 6.40 0 32 -2 -1.90 6.60 0 32 -3 0.00 7.20 -1 32 0 1.70 5.40 1 32 0 -3.70 5.70 -1 32 1 4.80 6.30 1 32 -1 -0.90 5.40 -1 32 -1 1.30 6.10 1 32 1 -3.70 6.00 1 32 -2 -5.10 5.60 1 32 2 -3.70 5.50 -1 32 -2 -4.60 5.40 1 32 -3 -1.90 6.60 -1 32 -3 -4.70 7.00 -1 -32 3 5.60 5.20 -2 32 0 40.60 8.30 2 32 0 28.20 7.60 2 32 -1 -5.40 6.20 -2 32 1 -0.60 5.60 2 -32 1 -2.70 4.00 -2 32 -1 0.30 6.20 2 32 1 2.40 5.50 2 -32 2 8.90 5.10 2 32 -2 0.70 7.30 -2 32 -2 -0.10 6.70 2 32 2 8.00 6.30 2 32 -3 5.10 7.50 -2 -32 3 7.30 5.80 -2 32 -3 5.60 7.10 3 32 0 3.80 6.10 -3 32 0 -5.10 5.40 3 -32 1 -5.10 4.70 -3 32 1 3.50 6.00 3 32 -1 1.60 6.10 -3 32 -1 -3.60 6.70 3 32 1 8.90 6.20 3 -32 2 19.10 5.70 3 32 -2 19.40 8.50 -3 32 -2 28.10 8.60 3 32 2 30.90 7.40 -4 32 0 6.20 6.50 4 32 0 13.20 7.10 4 -32 1 3.80 4.70 -4 32 1 14.80 6.70 4 32 -1 16.40 7.00 -4 32 -1 6.30 7.30 4 32 -2 26.80 7.90 4 -32 2 35.00 6.50 -4 32 -2 25.30 8.80 -5 32 0 -5.50 5.60 5 -32 0 1.40 4.80 5 -32 1 5.20 4.90 -5 32 1 6.30 6.20 -5 32 -1 4.30 6.60 5 32 -2 40.60 9.30 5 -32 2 31.40 6.90 -5 32 -2 35.10 9.00 6 -32 0 17.10 6.00 -6 32 0 8.30 7.00 6 -32 1 -4.10 4.40 -6 32 -1 3.20 6.30 0 33 0 1.10 6.80 0 33 1 58.19 10.00 0 33 -1 45.10 10.10 1 33 0 2.60 5.80 -1 33 0 -0.60 5.80 1 33 -1 1.50 6.20 -1 33 1 8.90 6.50 -1 33 -1 -2.00 5.90 1 33 1 2.90 6.40 2 33 0 81.89 11.90 -2 33 0 98.09 12.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 95453 _olex2_submission_special_instructions 'No special instructions were received' ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_RomanTA54b _database_code_depnum_ccdc_archive 'CCDC 2122219' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-15 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common RomanTA54b _chemical_melting_point ? _chemical_formula_moiety 'C26 H20 O' _chemical_formula_sum 'C26 H20 O' _chemical_formula_weight 348.42 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 3 _space_group_name_H-M_alt 'P 2' _space_group_name_Hall 'P 2y' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' _cell_length_a 28.975(5) _cell_length_b 5.9041(9) _cell_length_c 17.275(3) _cell_angle_alpha 90 _cell_angle_beta 106.661(4) _cell_angle_gamma 90 _cell_volume 2831.2(8) _cell_formula_units_Z 6 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 7003 _cell_measurement_theta_min 1.603 _cell_measurement_theta_max 24.483 _exptl_crystal_description needle _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.226 _exptl_crystal_F_000 1104 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.210 _exptl_crystal_size_mid 0.090 _exptl_crystal_size_min 0.090 _exptl_absorpt_coefficient_mu 0.073 _shelx_estimated_absorpt_T_min 0.985 _shelx_estimated_absorpt_T_max 0.993 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.965 _exptl_absorpt_correction_T_max 0.973 _exptl_absorpt_process_details 'SADABS V2008/1 (Bruker AXS)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'APEX2 (Bruker AXS)' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 95 _diffrn_reflns_number 17031 _diffrn_reflns_av_unetI/netI 0.1970 _diffrn_reflns_av_R_equivalents 0.0892 _diffrn_reflns_limit_h_min -33 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_theta_min 1.603 _diffrn_reflns_theta_max 24.483 _diffrn_reflns_theta_full 24.483 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measured_fraction_theta_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.958 _diffrn_reflns_point_group_measured_fraction_full 0.958 _reflns_number_total 7003 _reflns_number_gt 3599 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker Instrument Service v2010.7.0.0' _computing_cell_refinement 'APEX2 v2010.7-0 (Bruker AXS)' _computing_data_reduction 'SAINT V7.68A (Bruker AXS, 2009)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0522P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 1001 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.0 _chemical_absolute_configuration unk _refine_ls_number_reflns 7003 _refine_ls_number_parameters 731 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.2118 _refine_ls_R_factor_gt 0.0698 _refine_ls_wR_factor_ref 0.1768 _refine_ls_wR_factor_gt 0.1250 _refine_ls_goodness_of_fit_ref 0.913 _refine_ls_restrained_S_all 0.913 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 # start Validation Reply Form _vrf_PLAT340_RomanTA54b ; PROBLEM: Low Bond Precision on C-C Bonds ............... 0.01448 Ang. RESPONSE: Slight disordered phenyl groups in the structure ; # end Validation Reply Form loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.8315(2) -0.1643(9) 1.1438(3) 0.0351(16) Uani 1 1 d . . . . . C1 C 0.8201(4) 0.0299(13) 1.1874(5) 0.035(3) Uani 1 1 d . . . . . C2 C 0.8361(4) 0.0619(14) 1.1114(6) 0.041(3) Uani 1 1 d . . . . . C3 C 0.8549(3) 0.0754(15) 1.2683(5) 0.028(2) Uani 1 1 d . . . . . C4 C 0.8521(4) 0.2698(16) 1.3092(6) 0.048(3) Uani 1 1 d . . . . . H4 H 0.8284 0.3797 1.2848 0.057 Uiso 1 1 calc R U . . . C5 C 0.8826(4) 0.3104(17) 1.3847(7) 0.052(3) Uani 1 1 d . . . . . H5 H 0.8804 0.4492 1.4113 0.063 Uiso 1 1 calc R U . . . C6 C 0.9160(4) 0.1544(19) 1.4219(6) 0.049(3) Uani 1 1 d . . . . . H6 H 0.9367 0.1803 1.4748 0.059 Uiso 1 1 calc R U . . . C7 C 0.9191(4) -0.041(2) 1.3813(7) 0.067(4) Uani 1 1 d . . . . . H7 H 0.9426 -0.1515 1.4061 0.081 Uiso 1 1 calc R U . . . C8 C 0.8886(4) -0.0821(17) 1.3049(6) 0.049(3) Uani 1 1 d . . . . . H8 H 0.8912 -0.2196 1.2778 0.059 Uiso 1 1 calc R U . . . C9 C 0.7677(3) 0.0478(16) 1.1829(5) 0.036(2) Uani 1 1 d . . . . . C10 C 0.7399(4) 0.2368(15) 1.1560(6) 0.043(3) Uani 1 1 d . . . . . H10 H 0.7535 0.3646 1.1371 0.051 Uiso 1 1 calc R U . . . C11 C 0.6924(4) 0.2406(16) 1.1563(6) 0.045(3) Uani 1 1 d . . . . . H11 H 0.6731 0.3701 1.1371 0.054 Uiso 1 1 calc R U . . . C12 C 0.6732(3) 0.0575(17) 1.1844(6) 0.046(3) Uani 1 1 d . . . . . H12 H 0.6404 0.0605 1.1843 0.055 Uiso 1 1 calc R U . . . C13 C 0.7009(4) -0.1322(17) 1.2129(6) 0.046(3) Uani 1 1 d . . . . . H13 H 0.6874 -0.2581 1.2330 0.056 Uiso 1 1 calc R U . . . C14 C 0.7478(4) -0.1357(15) 1.2117(5) 0.044(3) Uani 1 1 d . . . . . H14 H 0.7671 -0.2656 1.2308 0.053 Uiso 1 1 calc R U . . . C15 C 0.8882(3) 0.1280(16) 1.1207(6) 0.037(3) Uani 1 1 d . . . . . C16 C 0.9069(4) 0.3393(16) 1.1491(5) 0.045(3) Uani 1 1 d . . . . . H16 H 0.8872 0.4466 1.1657 0.054 Uiso 1 1 calc R U . . . C17 C 0.9541(4) 0.3941(17) 1.1533(6) 0.051(3) Uani 1 1 d . . . . . H17 H 0.9666 0.5393 1.1719 0.062 Uiso 1 1 calc R U . . . C18 C 0.9830(4) 0.236(2) 1.1304(7) 0.059(3) Uani 1 1 d . . . . . H18 H 1.0157 0.2697 1.1350 0.070 Uiso 1 1 calc R U . . . C19 C 0.9636(4) 0.0324(19) 1.1010(6) 0.050(3) Uani 1 1 d . . . . . H19 H 0.9830 -0.0722 1.0824 0.060 Uiso 1 1 calc R U . . . C20 C 0.9170(4) -0.0279(16) 1.0973(6) 0.047(3) Uani 1 1 d . . . . . H20 H 0.9049 -0.1739 1.0789 0.057 Uiso 1 1 calc R U . . . C21 C 0.8008(3) 0.1158(15) 1.0311(5) 0.031(2) Uani 1 1 d . . . . . C22 C 0.8018(3) 0.3258(15) 0.9944(6) 0.040(3) Uani 1 1 d . . . . . H22 H 0.8237 0.4391 1.0219 0.048 Uiso 1 1 calc R U . . . C23 C 0.7714(3) 0.3697(17) 0.9191(6) 0.044(3) Uani 1 1 d . . . . . H23 H 0.7729 0.5114 0.8939 0.052 Uiso 1 1 calc R U . . . C24 C 0.7385(3) 0.2079(17) 0.8799(6) 0.047(3) Uani 1 1 d . . . . . H24 H 0.7169 0.2377 0.8281 0.056 Uiso 1 1 calc R U . . . C25 C 0.7378(4) 0.0058(18) 0.9166(6) 0.048(3) Uani 1 1 d . . . . . H25 H 0.7154 -0.1061 0.8896 0.058 Uiso 1 1 calc R U . . . C26 C 0.7685(3) -0.0433(16) 0.9921(6) 0.045(3) Uani 1 1 d . . . . . H26 H 0.7671 -0.1865 1.0164 0.055 Uiso 1 1 calc R U . . . O1A O 0.8282(2) 0.1602(9) 0.6669(3) 0.0398(17) Uani 1 1 d . . . . . C1A C 0.8208(3) 0.3872(14) 0.6957(6) 0.037(3) Uani 1 1 d . . . . . C2A C 0.8363(3) 0.3564(14) 0.6198(6) 0.039(2) Uani 1 1 d . . . . . C3A C 0.8561(3) 0.4556(15) 0.7708(6) 0.033(2) Uani 1 1 d . . . . . C4A C 0.8660(3) 0.3112(16) 0.8378(6) 0.044(3) Uani 1 1 d . . . . . H4A H 0.8502 0.1688 0.8336 0.053 Uiso 1 1 calc R U . . . C5A C 0.8982(4) 0.374(2) 0.9094(7) 0.056(3) Uani 1 1 d . . . . . H5A H 0.9054 0.2729 0.9540 0.067 Uiso 1 1 calc R U . . . C6A C 0.9205(4) 0.585(2) 0.9172(7) 0.058(3) Uani 1 1 d . . . . . H6A H 0.9428 0.6287 0.9670 0.070 Uiso 1 1 calc R U . . . C7A C 0.9102(4) 0.7269(18) 0.8530(7) 0.059(3) Uani 1 1 d . . . . . H7A H 0.9248 0.8723 0.8576 0.071 Uiso 1 1 calc R U . . . C8A C 0.8786(3) 0.6603(16) 0.7815(6) 0.047(3) Uani 1 1 d . . . . . H8A H 0.8720 0.7620 0.7370 0.056 Uiso 1 1 calc R U . . . C9A C 0.7687(3) 0.4371(15) 0.6895(5) 0.034(2) Uani 1 1 d . . . . . C10A C 0.7326(3) 0.2853(16) 0.6565(5) 0.038(3) Uani 1 1 d . . . . . H10A H 0.7401 0.1466 0.6351 0.046 Uiso 1 1 calc R U . . . C11A C 0.6852(3) 0.3308(17) 0.6540(6) 0.048(3) Uani 1 1 d . . . . . H11A H 0.6608 0.2215 0.6331 0.057 Uiso 1 1 calc R U . . . C12A C 0.6736(4) 0.5400(16) 0.6828(5) 0.043(3) Uani 1 1 d . . . . . H12A H 0.6411 0.5742 0.6800 0.052 Uiso 1 1 calc R U . . . C13A C 0.7089(4) 0.6918(16) 0.7143(6) 0.043(3) Uani 1 1 d . . . . . H13A H 0.7011 0.8333 0.7336 0.052 Uiso 1 1 calc R U . . . C14A C 0.7562(4) 0.6429(15) 0.7187(5) 0.042(3) Uani 1 1 d . . . . . H14A H 0.7807 0.7504 0.7418 0.050 Uiso 1 1 calc R U . . . C15A C 0.8883(3) 0.3909(15) 0.6229(6) 0.036(2) Uani 1 1 d . . . . . C16A C 0.9234(4) 0.2337(16) 0.6565(5) 0.043(3) Uani 1 1 d . . . . . H16A H 0.9150 0.1000 0.6799 0.052 Uiso 1 1 calc R U . . . C17A C 0.9698(4) 0.2662(18) 0.6568(6) 0.046(3) Uani 1 1 d . . . . . H17A H 0.9933 0.1531 0.6785 0.055 Uiso 1 1 calc R U . . . C18A C 0.9828(4) 0.4576(19) 0.6265(6) 0.054(3) Uani 1 1 d . . . . . H18A H 1.0155 0.4817 0.6284 0.065 Uiso 1 1 calc R U . . . C19A C 0.9486(4) 0.6195(17) 0.5926(6) 0.053(3) Uani 1 1 d . . . . . H19A H 0.9576 0.7546 0.5709 0.064 Uiso 1 1 calc R U . . . C20A C 0.9013(4) 0.5839(16) 0.5904(6) 0.048(3) Uani 1 1 d . . . . . H20A H 0.8775 0.6937 0.5662 0.058 Uiso 1 1 calc R U . . . C21A C 0.8004(3) 0.3694(17) 0.5370(6) 0.038(3) Uani 1 1 d . . . . . C22A C 0.7960(4) 0.1877(17) 0.4851(6) 0.049(3) Uani 1 1 d . . . . . H22A H 0.8142 0.0541 0.5027 0.059 Uiso 1 1 calc R U . . . C23A C 0.7652(4) 0.1994(18) 0.4078(7) 0.051(3) Uani 1 1 d . . . . . H23A H 0.7627 0.0743 0.3723 0.061 Uiso 1 1 calc R U . . . C24A C 0.7385(4) 0.386(2) 0.3821(6) 0.057(3) Uani 1 1 d . . . . . H24A H 0.7163 0.3905 0.3297 0.069 Uiso 1 1 calc R U . . . C25A C 0.7438(4) 0.573(2) 0.4331(7) 0.058(3) Uani 1 1 d . . . . . H25A H 0.7262 0.7071 0.4141 0.069 Uiso 1 1 calc R U . . . C26A C 0.7741(4) 0.5654(18) 0.5104(6) 0.050(3) Uani 1 1 d . . . . . H26A H 0.7770 0.6924 0.5452 0.060 Uiso 1 1 calc R U . . . O1B O 0.5000 0.6434(12) 0.5000 0.035(2) Uani 1 2 d S T P . . C1B C 0.5071(3) 0.8546(14) 0.4612(5) 0.033(2) Uani 1 1 d . . . . . C2B C 0.5591(3) 0.9035(14) 0.4657(5) 0.032(2) Uani 1 1 d . . . . . C3B C 0.5955(4) 0.7549(16) 0.4973(5) 0.041(3) Uani 1 1 d . . . . . H3B H 0.5885 0.6159 0.5193 0.049 Uiso 1 1 calc R U . . . C4B C 0.6423(3) 0.8019(16) 0.4981(6) 0.042(3) Uani 1 1 d . . . . . H4B H 0.6669 0.6927 0.5186 0.051 Uiso 1 1 calc R U . . . C5B C 0.6538(4) 1.0050(16) 0.4695(5) 0.040(3) Uani 1 1 d . . . . . H5B H 0.6861 1.0373 0.4707 0.048 Uiso 1 1 calc R U . . . C6B C 0.6181(4) 1.1608(16) 0.4391(6) 0.043(3) Uani 1 1 d . . . . . H6B H 0.6257 1.3030 0.4201 0.051 Uiso 1 1 calc R U . . . C7B C 0.5706(4) 1.1105(15) 0.4360(5) 0.043(3) Uani 1 1 d . . . . . H7B H 0.5458 1.2173 0.4136 0.052 Uiso 1 1 calc R U . . . C8B C 0.4721(3) 0.8924(15) 0.3812(5) 0.032(2) Uani 1 1 d . . . . . C9B C 0.4643(4) 0.7199(17) 0.3247(6) 0.047(3) Uani 1 1 d . . . . . H9B H 0.4811 0.5807 0.3387 0.056 Uiso 1 1 calc R U . . . C10B C 0.4330(4) 0.7454(19) 0.2489(7) 0.054(3) Uani 1 1 d . . . . . H10B H 0.4281 0.6255 0.2107 0.065 Uiso 1 1 calc R U . . . C11B C 0.4089(4) 0.945(2) 0.2290(6) 0.054(3) Uani 1 1 d . . . . . H11B H 0.3871 0.9620 0.1765 0.065 Uiso 1 1 calc R U . . . C12B C 0.4151(4) 1.1259(17) 0.2828(7) 0.055(3) Uani 1 1 d . . . . . H12B H 0.3987 1.2657 0.2679 0.065 Uiso 1 1 calc R U . . . C13B C 0.4465(4) 1.0914(17) 0.3595(6) 0.049(3) Uani 1 1 d . . . . . H13B H 0.4506 1.2090 0.3984 0.059 Uiso 1 1 calc R U . . . O1C O 0.5000 0.3056(13) 0.0000 0.036(2) Uani 1 2 d S T P . . C1C C 0.4910(3) 0.5194(13) 0.0365(5) 0.031(2) Uani 1 1 d . . . . . C2C C 0.5264(3) 0.5690(15) 0.1182(5) 0.031(2) Uani 1 1 d . . . . . C3C C 0.5239(3) 0.7768(16) 0.1552(6) 0.044(3) Uani 1 1 d . . . . . H3C H 0.5007 0.8852 0.1278 0.053 Uiso 1 1 calc R U . . . C4C C 0.5542(3) 0.8295(16) 0.2308(6) 0.043(3) Uani 1 1 d . . . . . H4C H 0.5519 0.9718 0.2550 0.051 Uiso 1 1 calc R U . . . C5C C 0.5877(4) 0.6733(18) 0.2700(6) 0.045(3) Uani 1 1 d . . . . . H5C H 0.6091 0.7061 0.3218 0.053 Uiso 1 1 calc R U . . . C6C C 0.5901(4) 0.4662(17) 0.2332(6) 0.051(3) Uani 1 1 d . . . . . H6C H 0.6131 0.3571 0.2605 0.061 Uiso 1 1 calc R U . . . C7C C 0.5599(4) 0.4155(15) 0.1580(6) 0.044(3) Uani 1 1 d . . . . . H7C H 0.5624 0.2732 0.1338 0.053 Uiso 1 1 calc R U . . . C8C C 0.4393(3) 0.5545(16) 0.0316(5) 0.035(2) Uani 1 1 d . . . . . C9C C 0.4154(3) 0.3822(16) 0.0577(6) 0.044(3) Uani 1 1 d . . . . . H9C H 0.4325 0.2477 0.0783 0.053 Uiso 1 1 calc R U . . . C10C C 0.3682(4) 0.3979(17) 0.0551(6) 0.051(3) Uani 1 1 d . . . . . H10C H 0.3524 0.2748 0.0722 0.062 Uiso 1 1 calc R U . . . C11C C 0.3436(3) 0.5942(18) 0.0273(6) 0.047(3) Uani 1 1 d . . . . . H11C H 0.3107 0.6072 0.0259 0.056 Uiso 1 1 calc R U . . . C12C C 0.3660(4) 0.7724(17) 0.0013(6) 0.049(3) Uani 1 1 d . . . . . H12C H 0.3486 0.9074 -0.0176 0.059 Uiso 1 1 calc R U . . . C13C C 0.4149(4) 0.7542(16) 0.0030(6) 0.046(3) Uani 1 1 d . . . . . H13C H 0.4307 0.8755 -0.0151 0.056 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.041(4) 0.030(3) 0.031(4) 0.004(3) 0.006(3) 0.006(3) C1 0.050(7) 0.027(5) 0.033(6) 0.003(5) 0.017(6) 0.010(5) C2 0.046(7) 0.036(5) 0.043(7) 0.018(5) 0.015(6) 0.009(5) C3 0.026(6) 0.033(5) 0.021(6) 0.003(5) 0.003(5) -0.007(5) C4 0.045(7) 0.053(7) 0.043(8) 0.005(6) 0.008(6) 0.004(6) C5 0.058(8) 0.052(7) 0.044(8) -0.007(6) 0.010(7) -0.005(6) C6 0.049(8) 0.063(7) 0.028(7) -0.003(6) -0.001(6) -0.017(6) C7 0.053(8) 0.067(8) 0.071(10) 0.018(8) 0.002(8) 0.011(7) C8 0.053(7) 0.049(6) 0.036(7) -0.005(6) -0.001(6) 0.004(6) C9 0.032(6) 0.048(6) 0.026(6) 0.006(5) 0.003(5) 0.000(6) C10 0.045(7) 0.040(5) 0.043(7) 0.004(5) 0.012(6) 0.001(6) C11 0.047(7) 0.038(6) 0.046(8) 0.002(5) 0.007(6) 0.007(6) C12 0.029(6) 0.060(7) 0.045(7) -0.011(6) 0.005(6) -0.002(6) C13 0.040(7) 0.054(7) 0.044(7) 0.006(6) 0.011(6) -0.011(6) C14 0.047(7) 0.042(6) 0.037(7) 0.012(5) 0.001(6) 0.000(6) C15 0.030(6) 0.046(6) 0.030(6) 0.016(5) 0.001(5) -0.006(5) C16 0.047(7) 0.053(7) 0.033(7) 0.005(6) 0.008(6) 0.000(6) C17 0.046(7) 0.051(6) 0.050(8) 0.007(6) 0.002(6) -0.012(6) C18 0.037(7) 0.070(8) 0.064(9) 0.019(7) 0.007(7) -0.003(7) C19 0.038(7) 0.061(7) 0.053(8) 0.003(6) 0.014(6) 0.018(6) C20 0.043(7) 0.044(6) 0.053(8) 0.004(5) 0.011(6) 0.001(6) C21 0.029(6) 0.041(6) 0.020(6) 0.008(5) 0.003(5) 0.007(5) C22 0.041(7) 0.039(6) 0.035(7) 0.001(5) 0.004(6) -0.008(5) C23 0.039(6) 0.058(6) 0.032(7) 0.009(6) 0.007(6) 0.004(6) C24 0.038(7) 0.067(7) 0.032(7) 0.003(6) 0.006(6) 0.005(6) C25 0.039(7) 0.062(7) 0.033(7) -0.006(6) -0.005(6) -0.010(6) C26 0.038(7) 0.049(6) 0.043(7) 0.007(6) 0.002(6) -0.010(6) O1A 0.046(4) 0.039(4) 0.033(4) 0.008(3) 0.008(4) 0.002(3) C1A 0.041(6) 0.029(5) 0.041(7) -0.003(5) 0.014(6) -0.001(5) C2A 0.042(6) 0.034(5) 0.039(7) 0.012(5) 0.010(6) 0.001(5) C3A 0.023(6) 0.038(5) 0.033(7) -0.003(5) 0.000(5) -0.003(5) C4A 0.039(7) 0.052(6) 0.044(8) 0.003(6) 0.014(6) -0.003(5) C5A 0.037(7) 0.087(9) 0.040(8) 0.016(7) 0.007(6) 0.022(7) C6A 0.029(7) 0.097(10) 0.043(8) -0.014(8) 0.002(6) 0.011(7) C7A 0.050(8) 0.052(7) 0.068(9) -0.020(7) 0.007(7) -0.008(6) C8A 0.028(6) 0.055(7) 0.046(7) 0.009(6) -0.006(6) 0.008(5) C9A 0.031(6) 0.042(6) 0.030(6) 0.000(5) 0.010(5) -0.005(5) C10A 0.036(6) 0.047(6) 0.027(6) 0.004(5) 0.000(5) 0.004(5) C11A 0.031(7) 0.063(7) 0.045(8) 0.007(6) 0.003(6) -0.013(6) C12A 0.044(7) 0.049(6) 0.034(7) 0.007(5) 0.009(6) 0.019(6) C13A 0.038(7) 0.045(6) 0.039(7) -0.004(6) -0.002(6) -0.001(6) C14A 0.040(7) 0.046(6) 0.033(7) -0.006(5) -0.002(6) -0.009(5) C15A 0.037(6) 0.038(5) 0.030(6) 0.001(5) 0.005(5) -0.006(5) C16A 0.049(7) 0.044(6) 0.030(7) 0.003(5) 0.001(6) -0.002(6) C17A 0.031(7) 0.055(7) 0.043(8) -0.005(6) -0.001(6) 0.005(6) C18A 0.031(7) 0.078(8) 0.053(8) -0.005(7) 0.010(6) 0.001(7) C19A 0.049(8) 0.060(7) 0.051(8) 0.008(6) 0.012(7) -0.013(6) C20A 0.038(7) 0.045(6) 0.058(8) -0.002(6) 0.009(6) 0.003(6) C21A 0.025(6) 0.049(6) 0.041(7) 0.003(6) 0.010(5) 0.001(5) C22A 0.054(8) 0.045(6) 0.053(8) 0.002(6) 0.023(7) 0.001(6) C23A 0.049(8) 0.055(7) 0.049(8) -0.014(6) 0.013(7) -0.011(6) C24A 0.042(7) 0.095(9) 0.025(7) 0.006(7) -0.008(6) -0.014(8) C25A 0.045(7) 0.074(8) 0.050(8) 0.004(7) 0.008(7) 0.011(7) C26A 0.054(8) 0.055(7) 0.038(7) 0.004(6) 0.010(7) 0.003(6) O1B 0.040(6) 0.029(5) 0.033(6) 0.000 0.006(5) 0.000 C1B 0.039(6) 0.032(5) 0.029(6) 0.001(5) 0.009(5) 0.004(5) C2B 0.032(6) 0.038(6) 0.023(6) -0.003(5) 0.005(5) 0.001(5) C3B 0.049(7) 0.047(6) 0.027(7) 0.002(5) 0.011(6) -0.003(6) C4B 0.031(7) 0.054(7) 0.039(7) -0.001(6) 0.004(6) 0.011(5) C5B 0.041(7) 0.051(6) 0.023(6) -0.006(5) 0.005(6) -0.012(6) C6B 0.050(7) 0.038(6) 0.037(7) 0.004(5) 0.006(6) -0.005(6) C7B 0.049(8) 0.043(6) 0.034(7) -0.001(5) 0.007(6) 0.018(5) C8B 0.027(6) 0.038(5) 0.028(6) 0.011(5) 0.000(5) 0.006(5) C9B 0.047(7) 0.053(6) 0.040(7) -0.007(6) 0.013(6) 0.008(6) C10B 0.057(8) 0.063(7) 0.041(8) -0.006(6) 0.013(7) -0.010(7) C11B 0.040(7) 0.085(8) 0.034(7) 0.003(7) 0.004(6) -0.010(7) C12B 0.050(8) 0.052(7) 0.058(9) 0.021(7) 0.010(7) 0.021(6) C13B 0.051(7) 0.061(7) 0.038(7) -0.007(6) 0.016(7) -0.002(6) O1C 0.031(6) 0.034(5) 0.041(6) 0.000 0.007(5) 0.000 C1C 0.036(6) 0.030(5) 0.029(6) 0.000(5) 0.013(5) 0.005(5) C2C 0.027(6) 0.038(6) 0.027(6) 0.000(5) 0.003(5) -0.005(5) C3C 0.034(6) 0.051(7) 0.042(8) 0.007(6) 0.001(6) 0.003(5) C4C 0.044(7) 0.043(6) 0.043(8) -0.015(6) 0.013(6) -0.007(6) C5C 0.038(7) 0.068(7) 0.023(6) -0.001(6) 0.002(6) -0.011(6) C6C 0.049(8) 0.057(7) 0.041(7) 0.004(6) 0.004(7) 0.012(6) C7C 0.046(7) 0.042(6) 0.040(7) -0.001(6) 0.005(6) 0.006(6) C8C 0.029(6) 0.043(5) 0.028(6) 0.003(5) 0.001(5) 0.010(5) C9C 0.033(7) 0.045(6) 0.049(7) 0.004(6) 0.004(6) 0.002(6) C10C 0.040(7) 0.050(7) 0.064(9) -0.003(6) 0.016(6) -0.002(6) C11C 0.024(6) 0.074(8) 0.038(7) -0.018(6) 0.000(6) 0.010(6) C12C 0.057(8) 0.051(7) 0.035(7) 0.001(5) 0.006(6) 0.018(6) C13C 0.051(8) 0.052(6) 0.039(7) 0.005(6) 0.017(6) -0.002(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.460(9) . ? O1 C2 1.468(9) . ? C1 C3 1.496(11) . ? C1 C9 1.502(12) . ? C1 C2 1.523(12) . ? C2 C21 1.503(12) . ? C2 C15 1.524(12) . ? C3 C4 1.363(12) . ? C3 C8 1.365(11) . ? C4 C5 1.373(13) . ? C4 H4 0.9500 . ? C5 C6 1.356(13) . ? C5 H5 0.9500 . ? C6 C7 1.369(14) . ? C6 H6 0.9500 . ? C7 C8 1.382(13) . ? C7 H7 0.9500 . ? C8 H8 0.9500 . ? C9 C10 1.376(12) . ? C9 C14 1.384(12) . ? C10 C11 1.379(12) . ? C10 H10 0.9500 . ? C11 C12 1.366(12) . ? C11 H11 0.9500 . ? C12 C13 1.382(12) . ? C12 H12 0.9500 . ? C13 C14 1.368(12) . ? C13 H13 0.9500 . ? C14 H14 0.9500 . ? C15 C20 1.378(12) . ? C15 C16 1.391(12) . ? C16 C17 1.389(12) . ? C16 H16 0.9500 . ? C17 C18 1.382(12) . ? C17 H17 0.9500 . ? C18 C19 1.364(13) . ? C18 H18 0.9500 . ? C19 C20 1.382(12) . ? C19 H19 0.9500 . ? C20 H20 0.9500 . ? C21 C26 1.360(11) . ? C21 C22 1.396(12) . ? C22 C23 1.371(11) . ? C22 H22 0.9500 . ? C23 C24 1.381(12) . ? C23 H23 0.9500 . ? C24 C25 1.354(12) . ? C24 H24 0.9500 . ? C25 C26 1.382(12) . ? C25 H25 0.9500 . ? C26 H26 0.9500 . ? O1A C1A 1.467(9) . ? O1A C2A 1.473(9) . ? C1A C3A 1.461(12) . ? C1A C9A 1.512(11) . ? C1A C2A 1.513(12) . ? C2A C15A 1.506(12) . ? C2A C21A 1.512(12) . ? C3A C8A 1.360(11) . ? C3A C4A 1.398(12) . ? C4A C5A 1.370(13) . ? C4A H4A 0.9500 . ? C5A C6A 1.392(14) . ? C5A H5A 0.9500 . ? C6A C7A 1.353(13) . ? C6A H6A 0.9500 . ? C7A C8A 1.368(13) . ? C7A H7A 0.9500 . ? C8A H8A 0.9500 . ? C9A C10A 1.371(11) . ? C9A C14A 1.402(11) . ? C10A C11A 1.387(12) . ? C10A H10A 0.9500 . ? C11A C12A 1.408(13) . ? C11A H11A 0.9500 . ? C12A C13A 1.352(12) . ? C12A H12A 0.9500 . ? C13A C14A 1.383(12) . ? C13A H13A 0.9500 . ? C14A H14A 0.9500 . ? C15A C20A 1.370(11) . ? C15A C16A 1.376(11) . ? C16A C17A 1.358(12) . ? C16A H16A 0.9500 . ? C17A C18A 1.343(13) . ? C17A H17A 0.9500 . ? C18A C19A 1.380(13) . ? C18A H18A 0.9500 . ? C19A C20A 1.377(12) . ? C19A H19A 0.9500 . ? C20A H20A 0.9500 . ? C21A C22A 1.380(12) . ? C21A C26A 1.389(13) . ? C22A C23A 1.378(12) . ? C22A H22A 0.9500 . ? C23A C24A 1.346(13) . ? C23A H23A 0.9500 . ? C24A C25A 1.390(14) . ? C24A H24A 0.9500 . ? C25A C26A 1.372(13) . ? C25A H25A 0.9500 . ? C26A H26A 0.9500 . ? O1B C1B 1.458(9) . ? O1B C1B 1.458(9) 2_656 ? C1B C8B 1.479(11) . ? C1B C2B 1.512(11) . ? C1B C1B 1.512(15) 2_656 ? C2B C3B 1.360(11) . ? C2B C7B 1.402(11) . ? C3B C4B 1.383(12) . ? C3B H3B 0.9500 . ? C4B C5B 1.373(12) . ? C4B H4B 0.9500 . ? C5B C6B 1.372(12) . ? C5B H5B 0.9500 . ? C6B C7B 1.393(12) . ? C6B H6B 0.9500 . ? C7B H7B 0.9500 . ? C8B C13B 1.382(12) . ? C8B C9B 1.384(12) . ? C9B C10B 1.371(13) . ? C9B H9B 0.9500 . ? C10B C11B 1.365(13) . ? C10B H10B 0.9500 . ? C11B C12B 1.391(13) . ? C11B H11B 0.9500 . ? C12B C13B 1.391(13) . ? C12B H12B 0.9500 . ? C13B H13B 0.9500 . ? O1C C1C 1.467(9) 2_655 ? O1C C1C 1.467(9) . ? C1C C8C 1.491(11) . ? C1C C1C 1.496(15) 2_655 ? C1C C2C 1.516(11) . ? C2C C7C 1.362(11) . ? C2C C3C 1.395(12) . ? C3C C4C 1.385(12) . ? C3C H3C 0.9500 . ? C4C C5C 1.369(12) . ? C4C H4C 0.9500 . ? C5C C6C 1.389(12) . ? C5C H5C 0.9500 . ? C6C C7C 1.375(12) . ? C6C H6C 0.9500 . ? C7C H7C 0.9500 . ? C8C C9C 1.377(11) . ? C8C C13C 1.391(12) . ? C9C C10C 1.359(12) . ? C9C H9C 0.9500 . ? C10C C11C 1.373(13) . ? C10C H10C 0.9500 . ? C11C C12C 1.377(12) . ? C11C H11C 0.9500 . ? C12C C13C 1.412(12) . ? C12C H12C 0.9500 . ? C13C H13C 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 O1 C2 62.7(5) . . ? O1 C1 C3 115.6(7) . . ? O1 C1 C9 113.8(8) . . ? C3 C1 C9 115.9(7) . . ? O1 C1 C2 58.9(5) . . ? C3 C1 C2 119.6(8) . . ? C9 C1 C2 120.0(9) . . ? O1 C2 C21 115.6(8) . . ? O1 C2 C1 58.4(5) . . ? C21 C2 C1 121.8(8) . . ? O1 C2 C15 112.8(7) . . ? C21 C2 C15 115.8(8) . . ? C1 C2 C15 118.5(9) . . ? C4 C3 C8 118.4(9) . . ? C4 C3 C1 120.7(9) . . ? C8 C3 C1 120.8(8) . . ? C3 C4 C5 121.4(10) . . ? C3 C4 H4 119.3 . . ? C5 C4 H4 119.3 . . ? C6 C5 C4 120.7(10) . . ? C6 C5 H5 119.7 . . ? C4 C5 H5 119.7 . . ? C5 C6 C7 118.2(10) . . ? C5 C6 H6 120.9 . . ? C7 C6 H6 120.9 . . ? C6 C7 C8 121.2(11) . . ? C6 C7 H7 119.4 . . ? C8 C7 H7 119.4 . . ? C3 C8 C7 120.0(10) . . ? C3 C8 H8 120.0 . . ? C7 C8 H8 120.0 . . ? C10 C9 C14 119.5(9) . . ? C10 C9 C1 124.0(9) . . ? C14 C9 C1 116.4(9) . . ? C9 C10 C11 120.0(9) . . ? C9 C10 H10 120.0 . . ? C11 C10 H10 120.0 . . ? C12 C11 C10 119.8(10) . . ? C12 C11 H11 120.1 . . ? C10 C11 H11 120.1 . . ? C11 C12 C13 121.0(9) . . ? C11 C12 H12 119.5 . . ? C13 C12 H12 119.5 . . ? C14 C13 C12 119.0(9) . . ? C14 C13 H13 120.5 . . ? C12 C13 H13 120.5 . . ? C13 C14 C9 120.8(9) . . ? C13 C14 H14 119.6 . . ? C9 C14 H14 119.6 . . ? C20 C15 C16 119.8(9) . . ? C20 C15 C2 117.5(8) . . ? C16 C15 C2 122.6(9) . . ? C17 C16 C15 120.3(10) . . ? C17 C16 H16 119.9 . . ? C15 C16 H16 119.9 . . ? C18 C17 C16 119.8(10) . . ? C18 C17 H17 120.1 . . ? C16 C17 H17 120.1 . . ? C19 C18 C17 118.9(10) . . ? C19 C18 H18 120.5 . . ? C17 C18 H18 120.5 . . ? C18 C19 C20 122.5(10) . . ? C18 C19 H19 118.8 . . ? C20 C19 H19 118.8 . . ? C15 C20 C19 118.7(9) . . ? C15 C20 H20 120.7 . . ? C19 C20 H20 120.7 . . ? C26 C21 C22 119.3(9) . . ? C26 C21 C2 120.0(8) . . ? C22 C21 C2 120.7(9) . . ? C23 C22 C21 120.5(9) . . ? C23 C22 H22 119.8 . . ? C21 C22 H22 119.8 . . ? C22 C23 C24 120.0(10) . . ? C22 C23 H23 120.0 . . ? C24 C23 H23 120.0 . . ? C25 C24 C23 118.7(10) . . ? C25 C24 H24 120.7 . . ? C23 C24 H24 120.7 . . ? C24 C25 C26 122.3(10) . . ? C24 C25 H25 118.8 . . ? C26 C25 H25 118.8 . . ? C21 C26 C25 119.2(9) . . ? C21 C26 H26 120.4 . . ? C25 C26 H26 120.4 . . ? C1A O1A C2A 62.0(5) . . ? C3A C1A O1A 114.9(8) . . ? C3A C1A C9A 116.1(8) . . ? O1A C1A C9A 113.2(7) . . ? C3A C1A C2A 119.8(8) . . ? O1A C1A C2A 59.2(5) . . ? C9A C1A C2A 120.1(9) . . ? O1A C2A C15A 113.9(8) . . ? O1A C2A C21A 112.7(8) . . ? C15A C2A C21A 115.9(8) . . ? O1A C2A C1A 58.8(5) . . ? C15A C2A C1A 119.8(9) . . ? C21A C2A C1A 121.2(8) . . ? C8A C3A C4A 117.0(9) . . ? C8A C3A C1A 123.5(9) . . ? C4A C3A C1A 119.5(8) . . ? C5A C4A C3A 120.4(9) . . ? C5A C4A H4A 119.8 . . ? C3A C4A H4A 119.8 . . ? C4A C5A C6A 120.5(11) . . ? C4A C5A H5A 119.7 . . ? C6A C5A H5A 119.7 . . ? C7A C6A C5A 119.1(11) . . ? C7A C6A H6A 120.5 . . ? C5A C6A H6A 120.5 . . ? C6A C7A C8A 119.7(10) . . ? C6A C7A H7A 120.1 . . ? C8A C7A H7A 120.1 . . ? C3A C8A C7A 123.2(10) . . ? C3A C8A H8A 118.4 . . ? C7A C8A H8A 118.4 . . ? C10A C9A C14A 118.1(8) . . ? C10A C9A C1A 122.0(8) . . ? C14A C9A C1A 119.9(9) . . ? C9A C10A C11A 121.1(9) . . ? C9A C10A H10A 119.4 . . ? C11A C10A H10A 119.4 . . ? C10A C11A C12A 119.6(9) . . ? C10A C11A H11A 120.2 . . ? C12A C11A H11A 120.2 . . ? C13A C12A C11A 119.6(9) . . ? C13A C12A H12A 120.2 . . ? C11A C12A H12A 120.2 . . ? C12A C13A C14A 120.5(9) . . ? C12A C13A H13A 119.7 . . ? C14A C13A H13A 119.7 . . ? C13A C14A C9A 121.0(9) . . ? C13A C14A H14A 119.5 . . ? C9A C14A H14A 119.5 . . ? C20A C15A C16A 118.5(9) . . ? C20A C15A C2A 119.2(9) . . ? C16A C15A C2A 122.3(8) . . ? C17A C16A C15A 121.2(10) . . ? C17A C16A H16A 119.4 . . ? C15A C16A H16A 119.4 . . ? C18A C17A C16A 120.3(10) . . ? C18A C17A H17A 119.9 . . ? C16A C17A H17A 119.9 . . ? C17A C18A C19A 120.1(10) . . ? C17A C18A H18A 119.9 . . ? C19A C18A H18A 119.9 . . ? C20A C19A C18A 119.6(10) . . ? C20A C19A H19A 120.2 . . ? C18A C19A H19A 120.2 . . ? C15A C20A C19A 120.2(10) . . ? C15A C20A H20A 119.9 . . ? C19A C20A H20A 119.9 . . ? C22A C21A C26A 119.5(10) . . ? C22A C21A C2A 119.1(9) . . ? C26A C21A C2A 121.3(9) . . ? C23A C22A C21A 120.2(10) . . ? C23A C22A H22A 119.9 . . ? C21A C22A H22A 119.9 . . ? C24A C23A C22A 120.7(11) . . ? C24A C23A H23A 119.6 . . ? C22A C23A H23A 119.6 . . ? C23A C24A C25A 119.4(10) . . ? C23A C24A H24A 120.3 . . ? C25A C24A H24A 120.3 . . ? C26A C25A C24A 121.0(11) . . ? C26A C25A H25A 119.5 . . ? C24A C25A H25A 119.5 . . ? C25A C26A C21A 119.0(10) . . ? C25A C26A H26A 120.5 . . ? C21A C26A H26A 120.5 . . ? C1B O1B C1B 62.5(7) . 2_656 ? O1B C1B C8B 114.1(7) . . ? O1B C1B C2B 114.2(7) . . ? C8B C1B C2B 115.2(7) . . ? O1B C1B C1B 58.8(3) . 2_656 ? C8B C1B C1B 122.7(10) . 2_656 ? C2B C1B C1B 118.4(10) . 2_656 ? C3B C2B C7B 118.1(8) . . ? C3B C2B C1B 122.9(8) . . ? C7B C2B C1B 119.1(8) . . ? C2B C3B C4B 121.4(9) . . ? C2B C3B H3B 119.3 . . ? C4B C3B H3B 119.3 . . ? C5B C4B C3B 120.6(10) . . ? C5B C4B H4B 119.7 . . ? C3B C4B H4B 119.7 . . ? C6B C5B C4B 119.3(9) . . ? C6B C5B H5B 120.3 . . ? C4B C5B H5B 120.3 . . ? C5B C6B C7B 120.0(9) . . ? C5B C6B H6B 120.0 . . ? C7B C6B H6B 120.0 . . ? C6B C7B C2B 120.6(9) . . ? C6B C7B H7B 119.7 . . ? C2B C7B H7B 119.7 . . ? C13B C8B C9B 118.0(9) . . ? C13B C8B C1B 123.5(9) . . ? C9B C8B C1B 118.5(8) . . ? C10B C9B C8B 121.4(10) . . ? C10B C9B H9B 119.3 . . ? C8B C9B H9B 119.3 . . ? C11B C10B C9B 119.1(11) . . ? C11B C10B H10B 120.4 . . ? C9B C10B H10B 120.4 . . ? C10B C11B C12B 122.4(11) . . ? C10B C11B H11B 118.8 . . ? C12B C11B H11B 118.8 . . ? C13B C12B C11B 116.7(10) . . ? C13B C12B H12B 121.7 . . ? C11B C12B H12B 121.7 . . ? C8B C13B C12B 122.4(9) . . ? C8B C13B H13B 118.8 . . ? C12B C13B H13B 118.8 . . ? C1C O1C C1C 61.3(7) 2_655 . ? O1C C1C C8C 113.2(7) . . ? O1C C1C C1C 59.3(3) . 2_655 ? C8C C1C C1C 122.6(11) . 2_655 ? O1C C1C C2C 114.3(7) . . ? C8C C1C C2C 115.2(7) . . ? C1C C1C C2C 118.6(10) 2_655 . ? C7C C2C C3C 118.5(9) . . ? C7C C2C C1C 122.3(8) . . ? C3C C2C C1C 119.1(9) . . ? C4C C3C C2C 121.8(9) . . ? C4C C3C H3C 119.1 . . ? C2C C3C H3C 119.1 . . ? C5C C4C C3C 119.0(9) . . ? C5C C4C H4C 120.5 . . ? C3C C4C H4C 120.5 . . ? C4C C5C C6C 119.2(10) . . ? C4C C5C H5C 120.4 . . ? C6C C5C H5C 120.4 . . ? C7C C6C C5C 121.5(10) . . ? C7C C6C H6C 119.2 . . ? C5C C6C H6C 119.2 . . ? C2C C7C C6C 120.0(9) . . ? C2C C7C H7C 120.0 . . ? C6C C7C H7C 120.0 . . ? C9C C8C C13C 119.4(8) . . ? C9C C8C C1C 118.0(8) . . ? C13C C8C C1C 122.6(9) . . ? C10C C9C C8C 122.3(9) . . ? C10C C9C H9C 118.8 . . ? C8C C9C H9C 118.8 . . ? C9C C10C C11C 119.1(10) . . ? C9C C10C H10C 120.5 . . ? C11C C10C H10C 120.5 . . ? C10C C11C C12C 120.9(9) . . ? C10C C11C H11C 119.6 . . ? C12C C11C H11C 119.6 . . ? C11C C12C C13C 119.9(10) . . ? C11C C12C H12C 120.0 . . ? C13C C12C H12C 120.0 . . ? C8C C13C C12C 118.5(9) . . ? C8C C13C H13C 120.8 . . ? C12C C13C H13C 120.8 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 O1 C1 C3 -110.5(9) . . . . ? C2 O1 C1 C9 111.8(9) . . . . ? C1 O1 C2 C21 -113.1(9) . . . . ? C1 O1 C2 C15 110.5(9) . . . . ? C3 C1 C2 O1 103.7(8) . . . . ? C9 C1 C2 O1 -101.3(9) . . . . ? O1 C1 C2 C21 102.5(9) . . . . ? C3 C1 C2 C21 -153.8(8) . . . . ? C9 C1 C2 C21 1.1(13) . . . . ? O1 C1 C2 C15 -100.6(8) . . . . ? C3 C1 C2 C15 3.1(12) . . . . ? C9 C1 C2 C15 158.1(8) . . . . ? O1 C1 C3 C4 170.3(7) . . . . ? C9 C1 C3 C4 -52.9(11) . . . . ? C2 C1 C3 C4 103.0(10) . . . . ? O1 C1 C3 C8 -13.2(12) . . . . ? C9 C1 C3 C8 123.6(10) . . . . ? C2 C1 C3 C8 -80.5(11) . . . . ? C8 C3 C4 C5 1.1(14) . . . . ? C1 C3 C4 C5 177.6(9) . . . . ? C3 C4 C5 C6 -1.6(15) . . . . ? C4 C5 C6 C7 1.6(16) . . . . ? C5 C6 C7 C8 -1.0(17) . . . . ? C4 C3 C8 C7 -0.5(14) . . . . ? C1 C3 C8 C7 -177.1(9) . . . . ? C6 C7 C8 C3 0.5(17) . . . . ? O1 C1 C9 C10 -124.9(9) . . . . ? C3 C1 C9 C10 97.6(11) . . . . ? C2 C1 C9 C10 -58.2(13) . . . . ? O1 C1 C9 C14 58.4(11) . . . . ? C3 C1 C9 C14 -79.2(10) . . . . ? C2 C1 C9 C14 125.0(9) . . . . ? C14 C9 C10 C11 -1.3(14) . . . . ? C1 C9 C10 C11 -178.0(9) . . . . ? C9 C10 C11 C12 0.8(15) . . . . ? C10 C11 C12 C13 0.3(15) . . . . ? C11 C12 C13 C14 -0.9(15) . . . . ? C12 C13 C14 C9 0.4(15) . . . . ? C10 C9 C14 C13 0.7(14) . . . . ? C1 C9 C14 C13 177.6(9) . . . . ? O1 C2 C15 C20 48.1(12) . . . . ? C21 C2 C15 C20 -88.4(10) . . . . ? C1 C2 C15 C20 113.3(9) . . . . ? O1 C2 C15 C16 -134.1(8) . . . . ? C21 C2 C15 C16 89.5(11) . . . . ? C1 C2 C15 C16 -68.8(12) . . . . ? C20 C15 C16 C17 0.4(14) . . . . ? C2 C15 C16 C17 -177.3(9) . . . . ? C15 C16 C17 C18 -1.0(15) . . . . ? C16 C17 C18 C19 2.5(16) . . . . ? C17 C18 C19 C20 -3.6(17) . . . . ? C16 C15 C20 C19 -1.4(14) . . . . ? C2 C15 C20 C19 176.5(9) . . . . ? C18 C19 C20 C15 3.0(16) . . . . ? O1 C2 C21 C26 -2.2(12) . . . . ? C1 C2 C21 C26 -69.5(11) . . . . ? C15 C2 C21 C26 133.0(9) . . . . ? O1 C2 C21 C22 -180.0(7) . . . . ? C1 C2 C21 C22 112.8(10) . . . . ? C15 C2 C21 C22 -44.8(12) . . . . ? C26 C21 C22 C23 -1.5(14) . . . . ? C2 C21 C22 C23 176.3(8) . . . . ? C21 C22 C23 C24 1.8(14) . . . . ? C22 C23 C24 C25 -1.2(14) . . . . ? C23 C24 C25 C26 0.4(15) . . . . ? C22 C21 C26 C25 0.7(14) . . . . ? C2 C21 C26 C25 -177.1(8) . . . . ? C24 C25 C26 C21 -0.2(15) . . . . ? C2A O1A C1A C3A -111.1(9) . . . . ? C2A O1A C1A C9A 112.3(9) . . . . ? C1A O1A C2A C15A 111.5(9) . . . . ? C1A O1A C2A C21A -113.8(9) . . . . ? C3A C1A C2A O1A 102.9(9) . . . . ? C9A C1A C2A O1A -100.6(9) . . . . ? C3A C1A C2A C15A 1.5(13) . . . . ? O1A C1A C2A C15A -101.5(9) . . . . ? C9A C1A C2A C15A 157.9(8) . . . . ? C3A C1A C2A C21A -157.8(9) . . . . ? O1A C1A C2A C21A 99.3(9) . . . . ? C9A C1A C2A C21A -1.3(13) . . . . ? O1A C1A C3A C8A 132.9(9) . . . . ? C9A C1A C3A C8A -91.8(11) . . . . ? C2A C1A C3A C8A 65.5(12) . . . . ? O1A C1A C3A C4A -50.9(11) . . . . ? C9A C1A C3A C4A 84.4(10) . . . . ? C2A C1A C3A C4A -118.2(9) . . . . ? C8A C3A C4A C5A -2.2(14) . . . . ? C1A C3A C4A C5A -178.6(9) . . . . ? C3A C4A C5A C6A 1.9(15) . . . . ? C4A C5A C6A C7A -0.4(16) . . . . ? C5A C6A C7A C8A -0.9(16) . . . . ? C4A C3A C8A C7A 1.0(15) . . . . ? C1A C3A C8A C7A 177.3(9) . . . . ? C6A C7A C8A C3A 0.5(16) . . . . ? C3A C1A C9A C10A -138.8(9) . . . . ? O1A C1A C9A C10A -2.8(12) . . . . ? C2A C1A C9A C10A 63.9(12) . . . . ? C3A C1A C9A C14A 40.6(12) . . . . ? O1A C1A C9A C14A 176.6(7) . . . . ? C2A C1A C9A C14A -116.7(10) . . . . ? C14A C9A C10A C11A -1.8(14) . . . . ? C1A C9A C10A C11A 177.7(9) . . . . ? C9A C10A C11A C12A 2.6(14) . . . . ? C10A C11A C12A C13A -1.6(14) . . . . ? C11A C12A C13A C14A -0.2(15) . . . . ? C12A C13A C14A C9A 1.1(16) . . . . ? C10A C9A C14A C13A -0.1(14) . . . . ? C1A C9A C14A C13A -179.5(9) . . . . ? O1A C2A C15A C20A -171.6(8) . . . . ? C21A C2A C15A C20A 55.2(12) . . . . ? C1A C2A C15A C20A -105.1(11) . . . . ? O1A C2A C15A C16A 9.2(13) . . . . ? C21A C2A C15A C16A -124.0(10) . . . . ? C1A C2A C15A C16A 75.6(12) . . . . ? C20A C15A C16A C17A -0.9(15) . . . . ? C2A C15A C16A C17A 178.4(9) . . . . ? C15A C16A C17A C18A 2.3(16) . . . . ? C16A C17A C18A C19A -2.0(16) . . . . ? C17A C18A C19A C20A 0.3(17) . . . . ? C16A C15A C20A C19A -0.8(15) . . . . ? C2A C15A C20A C19A 179.8(9) . . . . ? C18A C19A C20A C15A 1.1(16) . . . . ? O1A C2A C21A C22A -56.9(11) . . . . ? C15A C2A C21A C22A 76.8(11) . . . . ? C1A C2A C21A C22A -123.2(9) . . . . ? O1A C2A C21A C26A 127.3(9) . . . . ? C15A C2A C21A C26A -99.0(10) . . . . ? C1A C2A C21A C26A 61.0(12) . . . . ? C26A C21A C22A C23A -0.9(14) . . . . ? C2A C21A C22A C23A -176.9(9) . . . . ? C21A C22A C23A C24A -0.9(15) . . . . ? C22A C23A C24A C25A 2.9(16) . . . . ? C23A C24A C25A C26A -3.1(16) . . . . ? C24A C25A C26A C21A 1.3(15) . . . . ? C22A C21A C26A C25A 0.7(14) . . . . ? C2A C21A C26A C25A 176.5(9) . . . . ? C1B O1B C1B C8B -114.8(10) 2_656 . . . ? C1B O1B C1B C2B 109.7(10) 2_656 . . . ? O1B C1B C2B C3B 5.1(12) . . . . ? C8B C1B C2B C3B -129.9(9) . . . . ? C1B C1B C2B C3B 71.3(9) 2_656 . . . ? O1B C1B C2B C7B -175.0(7) . . . . ? C8B C1B C2B C7B 50.0(11) . . . . ? C1B C1B C2B C7B -108.8(8) 2_656 . . . ? C7B C2B C3B C4B -2.0(14) . . . . ? C1B C2B C3B C4B 177.9(8) . . . . ? C2B C3B C4B C5B 2.5(15) . . . . ? C3B C4B C5B C6B -0.7(15) . . . . ? C4B C5B C6B C7B -1.3(15) . . . . ? C5B C6B C7B C2B 1.6(15) . . . . ? C3B C2B C7B C6B 0.0(13) . . . . ? C1B C2B C7B C6B -179.9(9) . . . . ? O1B C1B C8B C13B 130.1(8) . . . . ? C2B C1B C8B C13B -94.9(10) . . . . ? C1B C1B C8B C13B 63.0(10) 2_656 . . . ? O1B C1B C8B C9B -50.0(10) . . . . ? C2B C1B C8B C9B 85.0(10) . . . . ? C1B C1B C8B C9B -117.2(7) 2_656 . . . ? C13B C8B C9B C10B 1.1(14) . . . . ? C1B C8B C9B C10B -178.8(9) . . . . ? C8B C9B C10B C11B -0.1(16) . . . . ? C9B C10B C11B C12B 0.4(17) . . . . ? C10B C11B C12B C13B -1.6(16) . . . . ? C9B C8B C13B C12B -2.4(14) . . . . ? C1B C8B C13B C12B 177.5(9) . . . . ? C11B C12B C13B C8B 2.6(15) . . . . ? C1C O1C C1C C8C 115.3(11) 2_655 . . . ? C1C O1C C1C C2C -110.1(10) 2_655 . . . ? O1C C1C C2C C7C -7.3(11) . . . . ? C8C C1C C2C C7C 126.3(9) . . . . ? C1C C1C C2C C7C -74.3(9) 2_655 . . . ? O1C C1C C2C C3C 174.4(7) . . . . ? C8C C1C C2C C3C -52.0(11) . . . . ? C1C C1C C2C C3C 107.4(8) 2_655 . . . ? C7C C2C C3C C4C -0.2(14) . . . . ? C1C C2C C3C C4C 178.1(8) . . . . ? C2C C3C C4C C5C 0.2(14) . . . . ? C3C C4C C5C C6C -0.4(14) . . . . ? C4C C5C C6C C7C 0.6(15) . . . . ? C3C C2C C7C C6C 0.4(14) . . . . ? C1C C2C C7C C6C -177.9(8) . . . . ? C5C C6C C7C C2C -0.6(15) . . . . ? O1C C1C C8C C9C 50.8(11) . . . . ? C1C C1C C8C C9C 118.2(7) 2_655 . . . ? C2C C1C C8C C9C -83.3(10) . . . . ? O1C C1C C8C C13C -130.1(8) . . . . ? C1C C1C C8C C13C -62.7(11) 2_655 . . . ? C2C C1C C8C C13C 95.8(11) . . . . ? C13C C8C C9C C10C 1.4(15) . . . . ? C1C C8C C9C C10C -179.5(10) . . . . ? C8C C9C C10C C11C -1.6(16) . . . . ? C9C C10C C11C C12C 0.8(16) . . . . ? C10C C11C C12C C13C 0.2(15) . . . . ? C9C C8C C13C C12C -0.3(14) . . . . ? C1C C8C C13C C12C -179.4(9) . . . . ? C11C C12C C13C C8C -0.4(15) . . . . ? _refine_diff_density_max 0.261 _refine_diff_density_min -0.266 _refine_diff_density_rms 0.049 _shelx_res_file ; romanta54b.res created by SHELXL-2014/7 TITL mo_RomanTA54b_0ma_a.res in P2 REM Old TITL mo_RomanTA54b_0ma in P2/c REM SHELXT solution in P2 REM R1 0.194, Rweak 0.024, Alpha 0.006, Orientation as input REM Flack x = 0.282 ( 2.370 ) from Parsons' quotients REM Formula found by SHELXT: C78 O3 CELL 0.71073 28.9754 5.9041 17.2749 90 106.661 90 ZERR 6 0.005 0.0009 0.003 0 0.004 0 LATT -1 SYMM -X,+Y,-Z SFAC C H O UNIT 156 120 6 L.S. 10 PLAN 20 SIZE 0.09 0.09 0.21 TEMP -73 CONF LIST 6 MORE -1 BOND $H fmap 2 acta OMIT 1 0 0 OMIT 2 0 0 OMIT -1 0 1 OMIT 0 0 1 OMIT 0 -1 1 OMIT -8 4 16 OMIT 0 -1 0 OMIT 0 1 1 OMIT 0 1 0 OMIT 3 2 15 OMIT -3 -1 1 REM REM REM WGHT 0.052200 FVAR 0.27494 O1 3 0.831487 -0.164273 1.143807 11.00000 0.04101 0.03028 = 0.03113 0.00447 0.00596 0.00561 C1 1 0.820105 0.029861 1.187356 11.00000 0.04956 0.02681 = 0.03265 0.00259 0.01713 0.01015 C2 1 0.836073 0.061866 1.111413 11.00000 0.04617 0.03563 = 0.04331 0.01801 0.01511 0.00932 C3 1 0.854923 0.075350 1.268324 11.00000 0.02597 0.03343 = 0.02125 0.00322 0.00251 -0.00696 C4 1 0.852063 0.269841 1.309163 11.00000 0.04506 0.05264 = 0.04293 0.00531 0.00789 0.00440 AFIX 43 H4 2 0.828401 0.379704 1.284796 11.00000 -1.20000 AFIX 0 C5 1 0.882635 0.310425 1.384747 11.00000 0.05825 0.05150 = 0.04395 -0.00735 0.01025 -0.00481 AFIX 43 H5 2 0.880407 0.449189 1.411284 11.00000 -1.20000 AFIX 0 C6 1 0.915997 0.154393 1.421935 11.00000 0.04864 0.06350 = 0.02811 -0.00323 -0.00098 -0.01712 AFIX 43 H6 2 0.936671 0.180320 1.474796 11.00000 -1.20000 AFIX 0 C7 1 0.919091 -0.041436 1.381283 11.00000 0.05343 0.06726 = 0.07120 0.01832 0.00239 0.01065 AFIX 43 H7 2 0.942615 -0.151471 1.406052 11.00000 -1.20000 AFIX 0 C8 1 0.888640 -0.082076 1.304893 11.00000 0.05286 0.04912 = 0.03600 -0.00458 -0.00140 0.00435 AFIX 43 H8 2 0.891171 -0.219562 1.277830 11.00000 -1.20000 AFIX 0 C9 1 0.767711 0.047800 1.182875 11.00000 0.03176 0.04765 = 0.02567 0.00592 0.00300 -0.00019 C10 1 0.739924 0.236783 1.155959 11.00000 0.04456 0.03960 = 0.04330 0.00394 0.01233 0.00115 AFIX 43 H10 2 0.753486 0.364572 1.137147 11.00000 -1.20000 AFIX 0 C11 1 0.692407 0.240592 1.156306 11.00000 0.04741 0.03843 = 0.04619 0.00159 0.00725 0.00734 AFIX 43 H11 2 0.673058 0.370107 1.137096 11.00000 -1.20000 AFIX 0 C12 1 0.673240 0.057460 1.184371 11.00000 0.02930 0.06022 = 0.04526 -0.01106 0.00465 -0.00157 AFIX 43 H12 2 0.640447 0.060522 1.184295 11.00000 -1.20000 AFIX 0 C13 1 0.700856 -0.132177 1.212870 11.00000 0.03978 0.05400 = 0.04448 0.00616 0.01123 -0.01093 AFIX 43 H13 2 0.687412 -0.258085 1.232971 11.00000 -1.20000 AFIX 0 C14 1 0.747848 -0.135703 1.211673 11.00000 0.04667 0.04190 = 0.03686 0.01207 0.00082 0.00025 AFIX 43 H14 2 0.767082 -0.265599 1.230829 11.00000 -1.20000 AFIX 0 C15 1 0.888240 0.127999 1.120744 11.00000 0.03028 0.04588 = 0.03048 0.01588 0.00076 -0.00597 C16 1 0.906854 0.339316 1.149103 11.00000 0.04696 0.05288 = 0.03330 0.00515 0.00833 0.00049 AFIX 43 H16 2 0.887152 0.446578 1.165667 11.00000 -1.20000 AFIX 0 C17 1 0.954131 0.394055 1.153289 11.00000 0.04557 0.05082 = 0.05024 0.00688 0.00169 -0.01186 AFIX 43 H17 2 0.966605 0.539312 1.171853 11.00000 -1.20000 AFIX 0 C18 1 0.982970 0.236452 1.130351 11.00000 0.03723 0.07046 = 0.06396 0.01850 0.00734 -0.00296 AFIX 43 H18 2 1.015727 0.269746 1.134971 11.00000 -1.20000 AFIX 0 C19 1 0.963632 0.032430 1.100988 11.00000 0.03750 0.06082 = 0.05295 0.00255 0.01413 0.01789 AFIX 43 H19 2 0.982975 -0.072219 1.082381 11.00000 -1.20000 AFIX 0 C20 1 0.916960 -0.027889 1.097269 11.00000 0.04292 0.04374 = 0.05310 0.00429 0.01077 0.00093 AFIX 43 H20 2 0.904925 -0.173941 1.078890 11.00000 -1.20000 AFIX 0 C21 1 0.800801 0.115816 1.031086 11.00000 0.02866 0.04104 = 0.02032 0.00807 0.00340 0.00745 C22 1 0.801789 0.325797 0.994418 11.00000 0.04060 0.03912 = 0.03536 0.00078 0.00404 -0.00764 AFIX 43 H22 2 0.823699 0.439078 1.021860 11.00000 -1.20000 AFIX 0 C23 1 0.771366 0.369673 0.919090 11.00000 0.03922 0.05820 = 0.03189 0.00890 0.00737 0.00384 AFIX 43 H23 2 0.772867 0.511401 0.893887 11.00000 -1.20000 AFIX 0 C24 1 0.738545 0.207879 0.879854 11.00000 0.03782 0.06733 = 0.03206 0.00312 0.00628 0.00489 AFIX 43 H24 2 0.716887 0.237704 0.828096 11.00000 -1.20000 AFIX 0 C25 1 0.737840 0.005834 0.916615 11.00000 0.03943 0.06163 = 0.03317 -0.00622 -0.00497 -0.01046 AFIX 43 H25 2 0.715436 -0.106104 0.889576 11.00000 -1.20000 AFIX 0 C26 1 0.768550 -0.043275 0.992055 11.00000 0.03770 0.04940 = 0.04316 0.00660 0.00170 -0.00970 AFIX 43 H26 2 0.767147 -0.186471 1.016361 11.00000 -1.20000 AFIX 0 O1A 3 0.828153 0.160156 0.666863 11.00000 0.04561 0.03891 = 0.03311 0.00765 0.00822 0.00193 C1A 1 0.820800 0.387235 0.695678 11.00000 0.04074 0.02917 = 0.04139 -0.00288 0.01449 -0.00134 C2A 1 0.836320 0.356376 0.619834 11.00000 0.04198 0.03421 = 0.03859 0.01157 0.01003 0.00092 C3A 1 0.856108 0.455570 0.770842 11.00000 0.02332 0.03753 = 0.03327 -0.00302 -0.00043 -0.00279 C4A 1 0.865963 0.311240 0.837788 11.00000 0.03870 0.05217 = 0.04399 0.00299 0.01407 -0.00268 AFIX 43 H4A 2 0.850202 0.168761 0.833609 11.00000 -1.20000 AFIX 0 C5A 1 0.898209 0.374084 0.909361 11.00000 0.03742 0.08704 = 0.04013 0.01591 0.00723 0.02164 AFIX 43 H5A 2 0.905386 0.272882 0.953982 11.00000 -1.20000 AFIX 0 C6A 1 0.920542 0.585003 0.917237 11.00000 0.02853 0.09714 = 0.04321 -0.01403 0.00169 0.01059 AFIX 43 H6A 2 0.942755 0.628720 0.966995 11.00000 -1.20000 AFIX 0 C7A 1 0.910178 0.726926 0.853039 11.00000 0.04999 0.05245 = 0.06782 -0.01975 0.00672 -0.00807 AFIX 43 H7A 2 0.924780 0.872276 0.857634 11.00000 -1.20000 AFIX 0 C8A 1 0.878586 0.660250 0.781489 11.00000 0.02814 0.05535 = 0.04626 0.00902 -0.00582 0.00808 AFIX 43 H8A 2 0.872026 0.761957 0.737045 11.00000 -1.20000 AFIX 0 C9A 1 0.768688 0.437071 0.689515 11.00000 0.03131 0.04203 = 0.03043 -0.00007 0.00963 -0.00480 C10A 1 0.732578 0.285288 0.656543 11.00000 0.03589 0.04654 = 0.02741 0.00385 0.00033 0.00353 AFIX 43 H10A 2 0.740135 0.146631 0.635056 11.00000 -1.20000 AFIX 0 C11A 1 0.685200 0.330795 0.654035 11.00000 0.03128 0.06291 = 0.04474 0.00734 0.00350 -0.01302 AFIX 43 H11A 2 0.660756 0.221461 0.633053 11.00000 -1.20000 AFIX 0 C12A 1 0.673575 0.539975 0.682773 11.00000 0.04425 0.04924 = 0.03393 0.00725 0.00878 0.01895 AFIX 43 H12A 2 0.641110 0.574226 0.680039 11.00000 -1.20000 AFIX 0 C13A 1 0.708868 0.691822 0.714280 11.00000 0.03782 0.04483 = 0.03916 -0.00358 -0.00236 -0.00056 AFIX 43 H13A 2 0.701082 0.833295 0.733554 11.00000 -1.20000 AFIX 0 C14A 1 0.756224 0.642874 0.718682 11.00000 0.03976 0.04576 = 0.03264 -0.00635 -0.00172 -0.00911 AFIX 43 H14A 2 0.780685 0.750368 0.741827 11.00000 -1.20000 AFIX 0 C15A 1 0.888291 0.390886 0.622851 11.00000 0.03716 0.03754 = 0.02961 0.00059 0.00475 -0.00556 C16A 1 0.923389 0.233655 0.656465 11.00000 0.04896 0.04446 = 0.02965 0.00306 0.00150 -0.00207 AFIX 43 H16A 2 0.914972 0.099986 0.679881 11.00000 -1.20000 AFIX 0 C17A 1 0.969850 0.266208 0.656756 11.00000 0.03141 0.05485 = 0.04288 -0.00450 -0.00141 0.00483 AFIX 43 H17A 2 0.993301 0.153061 0.678463 11.00000 -1.20000 AFIX 0 C18A 1 0.982767 0.457640 0.626490 11.00000 0.03126 0.07754 = 0.05267 -0.00540 0.01024 0.00109 AFIX 43 H18A 2 1.015498 0.481710 0.628433 11.00000 -1.20000 AFIX 0 C19A 1 0.948581 0.619509 0.592560 11.00000 0.04903 0.05950 = 0.05066 0.00835 0.01250 -0.01266 AFIX 43 H19A 2 0.957647 0.754645 0.570865 11.00000 -1.20000 AFIX 0 C20A 1 0.901262 0.583926 0.590352 11.00000 0.03789 0.04505 = 0.05777 -0.00220 0.00882 0.00298 AFIX 43 H20A 2 0.877519 0.693655 0.566200 11.00000 -1.20000 AFIX 0 C21A 1 0.800367 0.369390 0.536972 11.00000 0.02507 0.04860 = 0.04063 0.00343 0.01020 0.00053 C22A 1 0.795956 0.187682 0.485064 11.00000 0.05357 0.04530 = 0.05279 0.00205 0.02288 0.00094 AFIX 43 H22A 2 0.814220 0.054071 0.502658 11.00000 -1.20000 AFIX 0 C23A 1 0.765154 0.199394 0.407813 11.00000 0.04948 0.05463 = 0.04861 -0.01422 0.01333 -0.01064 AFIX 43 H23A 2 0.762692 0.074263 0.372283 11.00000 -1.20000 AFIX 0 C24A 1 0.738517 0.386174 0.382138 11.00000 0.04153 0.09488 = 0.02509 0.00566 -0.00785 -0.01381 AFIX 43 H24A 2 0.716286 0.390534 0.329663 11.00000 -1.20000 AFIX 0 C25A 1 0.743829 0.572596 0.433087 11.00000 0.04521 0.07394 = 0.04981 0.00446 0.00771 0.01063 AFIX 43 H25A 2 0.726242 0.707130 0.414077 11.00000 -1.20000 AFIX 0 C26A 1 0.774077 0.565366 0.510410 11.00000 0.05361 0.05528 = 0.03835 0.00369 0.01043 0.00276 AFIX 43 H26A 2 0.776992 0.692416 0.545230 11.00000 -1.20000 AFIX 0 O1B 3 0.500000 0.643449 0.500000 10.50000 0.04016 0.02933 = 0.03349 0.00000 0.00592 0.00000 C1B 1 0.507124 0.854639 0.461174 11.00000 0.03915 0.03244 = 0.02864 0.00074 0.00940 0.00367 C2B 1 0.559058 0.903532 0.465666 11.00000 0.03193 0.03805 = 0.02332 -0.00265 0.00500 0.00066 C3B 1 0.595456 0.754902 0.497320 11.00000 0.04937 0.04677 = 0.02656 0.00191 0.01109 -0.00265 AFIX 43 H3B 2 0.588522 0.615897 0.519344 11.00000 -1.20000 AFIX 0 C4B 1 0.642332 0.801946 0.498104 11.00000 0.03108 0.05370 = 0.03880 -0.00122 0.00375 0.01127 AFIX 43 H4B 2 0.666866 0.692723 0.518648 11.00000 -1.20000 AFIX 0 C5B 1 0.653775 1.005046 0.469473 11.00000 0.04139 0.05121 = 0.02339 -0.00582 0.00468 -0.01191 AFIX 43 H5B 2 0.686102 1.037303 0.470725 11.00000 -1.20000 AFIX 0 C6B 1 0.618051 1.160840 0.439052 11.00000 0.04963 0.03817 = 0.03680 0.00354 0.00591 -0.00491 AFIX 43 H6B 2 0.625677 1.303040 0.420089 11.00000 -1.20000 AFIX 0 C7B 1 0.570599 1.110490 0.435975 11.00000 0.04929 0.04335 = 0.03430 -0.00124 0.00661 0.01750 AFIX 43 H7B 2 0.545843 1.217256 0.413571 11.00000 -1.20000 AFIX 0 C8B 1 0.472063 0.892405 0.381160 11.00000 0.02673 0.03799 = 0.02773 0.01122 0.00040 0.00566 C9B 1 0.464336 0.719884 0.324657 11.00000 0.04671 0.05266 = 0.04017 -0.00707 0.01253 0.00817 AFIX 43 H9B 2 0.481111 0.580727 0.338693 11.00000 -1.20000 AFIX 0 C10B 1 0.433000 0.745403 0.248867 11.00000 0.05708 0.06289 = 0.04089 -0.00614 0.01331 -0.00958 AFIX 43 H10B 2 0.428130 0.625481 0.210704 11.00000 -1.20000 AFIX 0 C11B 1 0.408901 0.945390 0.228987 11.00000 0.04006 0.08461 = 0.03387 0.00314 0.00351 -0.01013 AFIX 43 H11B 2 0.387079 0.961964 0.176510 11.00000 -1.20000 AFIX 0 C12B 1 0.415127 1.125885 0.282778 11.00000 0.05000 0.05193 = 0.05789 0.02083 0.00955 0.02057 AFIX 43 H12B 2 0.398747 1.265651 0.267856 11.00000 -1.20000 AFIX 0 C13B 1 0.446535 1.091441 0.359492 11.00000 0.05068 0.06061 = 0.03789 -0.00716 0.01598 -0.00239 AFIX 43 H13B 2 0.450585 1.209023 0.398412 11.00000 -1.20000 AFIX 0 O1C 3 0.500000 0.305613 0.000000 10.50000 0.03130 0.03406 = 0.04110 0.00000 0.00736 0.00000 C1C 1 0.491013 0.519351 0.036513 11.00000 0.03599 0.03022 = 0.02902 0.00016 0.01271 0.00493 C2C 1 0.526367 0.569041 0.118218 11.00000 0.02664 0.03785 = 0.02653 0.00022 0.00278 -0.00474 C3C 1 0.523852 0.776848 0.155213 11.00000 0.03405 0.05103 = 0.04187 0.00737 0.00107 0.00285 AFIX 43 H3C 2 0.500658 0.885195 0.127814 11.00000 -1.20000 AFIX 0 C4C 1 0.554247 0.829507 0.230794 11.00000 0.04359 0.04279 = 0.04261 -0.01510 0.01282 -0.00685 AFIX 43 H4C 2 0.551901 0.971826 0.255044 11.00000 -1.20000 AFIX 0 C5C 1 0.587725 0.673314 0.270020 11.00000 0.03808 0.06831 = 0.02311 -0.00121 0.00215 -0.01095 AFIX 43 H5C 2 0.609068 0.706117 0.321785 11.00000 -1.20000 AFIX 0 C6C 1 0.590096 0.466198 0.233174 11.00000 0.04901 0.05681 = 0.04057 0.00425 0.00370 0.01241 AFIX 43 H6C 2 0.613124 0.357130 0.260540 11.00000 -1.20000 AFIX 0 C7C 1 0.559887 0.415488 0.158032 11.00000 0.04563 0.04169 = 0.04005 -0.00122 0.00457 0.00641 AFIX 43 H7C 2 0.562389 0.273239 0.133849 11.00000 -1.20000 AFIX 0 C8C 1 0.439295 0.554488 0.031620 11.00000 0.02877 0.04323 = 0.02848 0.00322 0.00117 0.00987 C9C 1 0.415398 0.382191 0.057734 11.00000 0.03305 0.04500 = 0.04922 0.00401 0.00421 0.00179 AFIX 43 H9C 2 0.432525 0.247654 0.078324 11.00000 -1.20000 AFIX 0 C10C 1 0.368188 0.397898 0.055080 11.00000 0.04008 0.04974 = 0.06444 -0.00255 0.01569 -0.00242 AFIX 43 H10C 2 0.352416 0.274805 0.072234 11.00000 -1.20000 AFIX 0 C11C 1 0.343592 0.594164 0.027257 11.00000 0.02423 0.07353 = 0.03767 -0.01831 0.00026 0.01024 AFIX 43 H11C 2 0.310685 0.607171 0.025864 11.00000 -1.20000 AFIX 0 C12C 1 0.366006 0.772362 0.001350 11.00000 0.05659 0.05066 = 0.03530 0.00136 0.00598 0.01824 AFIX 43 H12C 2 0.348615 0.907440 -0.017596 11.00000 -1.20000 AFIX 0 C13C 1 0.414871 0.754165 0.002966 11.00000 0.05083 0.05196 = 0.03913 0.00530 0.01739 -0.00236 AFIX 43 H13C 2 0.430693 0.875471 -0.015095 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_RomanTA54b_0ma_a.res in P2 REM R1 = 0.0698 for 3599 Fo > 4sig(Fo) and 0.2118 for all 9003 data REM 731 parameters refined using 1 restraints END WGHT 0.0522 0.0000 REM Highest difference peak 0.261, deepest hole -0.266, 1-sigma level 0.049 Q1 1 0.8227 0.4188 1.1615 11.00000 0.05 0.26 Q2 1 0.4381 0.9308 0.4374 11.00000 0.05 0.24 Q3 1 0.8326 0.7479 0.6314 11.00000 0.05 0.21 Q4 1 0.7665 0.4690 0.7801 11.00000 0.05 0.21 Q5 1 0.5582 0.5523 0.0630 11.00000 0.05 0.21 Q6 1 0.5000 0.9212 0.0000 10.50000 0.05 0.20 Q7 1 0.4404 1.2944 0.4812 11.00000 0.05 0.20 Q8 1 0.9029 0.1165 0.7202 11.00000 0.05 0.19 Q9 1 0.5710 0.6267 0.5604 11.00000 0.05 0.19 Q10 1 0.4977 1.2513 0.4846 11.00000 0.05 0.19 Q11 1 0.8971 0.4248 0.7229 11.00000 0.05 0.18 Q12 1 0.8379 -0.0954 1.1249 11.00000 0.05 0.18 Q13 1 0.7956 -0.2923 1.1024 11.00000 0.05 0.18 Q14 1 0.8502 0.4139 0.7990 11.00000 0.05 0.17 Q15 1 0.3097 0.6804 -0.0214 11.00000 0.05 0.17 Q16 1 0.8352 0.5376 0.7418 11.00000 0.05 0.17 Q17 1 0.8513 0.3833 0.7411 11.00000 0.05 0.17 Q18 1 0.7499 0.7546 0.3978 11.00000 0.05 0.17 Q19 1 0.9083 -0.0694 1.1804 11.00000 0.05 0.16 Q20 1 0.8624 0.0351 0.8189 11.00000 0.05 0.16 ; _shelx_res_checksum 27544 _shelx_hkl_file ; 0 0 1 -0.30 0.30 0 0 1 0.40 0.30 0 0 1 0.00 0.20 0 0 -1 0.50 0.30 0 0 -1 -0.10 0.20 0 0 2 8.60 1.00 0 0 -2 10.60 1.40 0 0 2 12.40 1.50 0 0 -2 12.40 1.50 0 0 -2 8.40 1.00 0 0 2 10.70 1.40 0 0 -3 1.40 1.40 0 0 3 0.10 0.90 0 0 3 -1.60 1.30 0 0 3 -0.10 1.40 0 0 -3 -0.60 0.90 0 0 -3 2.00 1.70 0 0 4 118.29 5.80 0 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6.40 -2 2 -12 -2.10 7.40 2 2 12 7.10 4.70 2 2 12 11.80 5.70 -2 -2 -12 11.10 6.00 -2 2 -13 4.90 8.30 2 2 13 4.10 5.70 2 2 13 7.20 4.80 -2 -2 -13 7.00 5.50 -2 2 -14 24.00 9.40 2 2 14 12.00 5.70 2 2 14 7.40 6.20 -2 -2 -14 24.90 6.40 2 2 15 -4.30 4.90 -2 2 -15 -7.80 8.30 2 2 15 -17.60 6.00 -2 -2 -15 6.90 5.50 2 2 16 -8.50 5.80 -2 2 -16 5.70 9.30 -2 -2 -16 20.20 6.60 2 2 17 -16.50 6.30 -2 2 -17 -3.40 8.80 -2 -2 -17 10.50 6.30 -2 2 -18 -12.90 8.70 2 3 -17 -7.30 8.60 -2 3 17 -4.30 5.50 2 3 -16 -7.30 8.40 -2 3 16 -8.60 4.20 2 3 -15 11.40 8.70 -2 3 15 -16.40 5.90 -2 3 15 -0.30 4.40 -2 3 14 66.69 8.30 -2 3 14 97.99 12.40 2 3 -14 122.49 13.10 -2 3 13 -8.90 4.40 2 3 -13 13.60 7.70 -2 3 13 -0.60 4.00 -2 3 12 5.50 5.00 2 3 -12 14.40 8.20 -2 3 12 4.90 4.20 2 -3 -12 7.80 4.30 -2 3 11 9.20 4.60 -2 3 11 11.10 4.60 2 3 -11 9.70 7.90 2 -3 -11 12.10 4.50 -2 3 10 6.70 4.20 -2 3 10 5.70 3.70 2 -3 -10 4.20 3.90 -2 3 9 8.50 3.40 -2 3 9 7.20 3.90 2 -3 -9 11.20 5.20 2 -3 -9 9.40 3.80 -2 3 8 58.39 6.50 -2 3 8 61.69 8.30 2 -3 -8 48.30 5.70 2 -3 -8 57.09 7.70 2 3 -7 26.80 3.10 -2 3 7 24.80 5.20 -2 3 7 22.40 3.40 -2 -3 7 24.40 2.90 2 -3 -7 36.30 6.20 2 -3 -7 24.60 4.00 -2 3 6 21.80 4.60 -2 3 6 20.90 3.00 2 3 -6 17.00 2.50 2 -3 -6 29.60 5.50 -2 -3 6 23.90 5.80 -2 -3 6 21.10 2.70 2 -3 -6 27.10 3.70 -2 3 5 7.10 2.20 -2 3 5 7.60 3.30 2 -3 -5 8.50 2.90 -2 -3 5 2.40 1.90 -2 -3 5 6.70 4.90 2 -3 -5 5.30 3.60 -2 3 4 10.20 2.30 -2 3 4 10.70 3.50 2 3 -4 7.60 2.20 2 -3 -4 12.50 3.20 2 -3 -4 12.80 3.90 -2 -3 4 12.50 2.70 -2 -3 4 22.80 5.70 2 3 -3 50.39 5.10 -2 3 3 53.49 6.70 -2 3 3 51.19 5.00 -2 -3 3 44.10 4.50 2 -3 -3 45.40 5.70 -2 -3 3 52.29 6.10 2 -3 -3 52.79 5.10 -2 3 2 61.19 5.60 -2 3 2 52.69 6.70 2 3 -2 63.39 5.80 -2 -3 2 62.69 6.80 2 -3 -2 51.39 5.50 2 -3 -2 54.89 6.00 -2 -3 2 57.59 5.00 -2 3 1 6.10 2.30 2 3 -1 10.30 2.80 2 -3 -1 8.50 3.40 2 -3 -1 7.90 3.20 -2 -3 1 13.60 4.20 -2 -3 1 12.70 3.20 2 3 0 21.50 3.70 -2 3 0 16.90 3.10 2 3 0 18.80 2.80 -2 -3 0 24.30 4.40 2 -3 0 22.00 4.20 2 -3 0 17.60 3.70 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6.00 -2 -4 3 60.79 7.80 -2 -4 3 41.50 5.50 2 -4 -3 40.60 6.20 2 -4 -3 41.50 5.60 2 4 -2 7.80 2.90 -2 4 2 10.60 3.80 -2 4 2 5.70 2.80 2 -4 -2 11.60 4.50 -2 -4 2 11.70 3.70 2 -4 -2 10.90 4.50 -2 -4 2 15.30 5.70 2 4 -1 6.00 2.90 2 4 -1 4.80 2.80 -2 4 1 10.30 3.00 -2 4 1 8.20 3.40 -2 -4 1 7.70 3.70 2 -4 -1 4.60 3.70 -2 -4 1 7.80 5.20 2 -4 -1 11.40 4.50 -2 4 0 2.40 2.90 -2 4 0 3.20 2.70 2 4 0 5.00 2.80 2 4 0 3.40 2.60 2 -4 0 5.50 4.80 2 -4 0 5.80 3.60 -2 -4 0 2.50 3.50 -2 -4 0 3.30 4.70 2 4 1 60.99 7.90 -2 4 -1 73.39 8.10 -2 4 -1 62.59 7.20 2 4 1 68.79 6.40 2 -4 1 64.29 7.40 -2 -4 -1 73.09 8.30 -2 -4 -1 66.89 7.20 2 -4 1 56.39 6.50 -2 4 -2 34.60 5.00 2 4 2 39.20 5.80 2 4 2 45.50 5.50 -2 4 -2 39.00 5.30 -2 -4 -2 41.00 6.00 2 -4 2 40.70 6.80 2 -4 2 40.00 5.40 2 4 3 40.90 5.00 2 4 3 38.10 6.20 2 -4 3 37.10 5.20 -2 -4 -3 37.70 6.00 2 -4 3 31.40 6.60 2 4 4 9.80 4.10 2 4 4 11.30 2.60 2 -4 4 11.80 3.50 -2 -4 -4 11.10 4.70 2 4 5 6.00 2.40 2 4 5 10.60 4.30 -2 -4 -5 7.80 4.50 2 -4 5 13.90 3.60 2 4 6 5.70 2.60 2 4 6 6.90 4.10 -2 -4 -6 5.90 4.50 2 -4 6 2.30 2.70 2 4 7 19.90 3.50 2 4 7 22.20 5.70 2 -4 7 16.10 3.60 -2 -4 -7 32.10 5.80 2 4 8 3.10 4.00 2 4 8 2.20 3.60 -2 -4 -8 5.00 4.70 2 4 9 25.60 6.40 -2 4 -9 53.19 10.00 -2 -4 -9 27.70 5.70 -2 4 -10 19.20 8.50 2 4 10 7.00 4.80 -2 -4 -10 10.10 4.60 2 4 11 0.20 4.60 -2 4 -11 14.80 8.60 -2 -4 -11 5.00 4.50 2 4 12 -5.00 4.30 -2 4 -12 20.50 9.40 -2 4 -13 8.00 9.60 2 4 13 -5.70 4.80 -2 4 -14 -6.30 9.70 2 4 14 -5.80 5.20 -2 4 -15 -1.30 9.70 2 4 15 -2.10 6.20 2 5 -13 10.40 8.20 -2 5 13 -2.30 5.50 -2 5 12 -1.20 5.10 -2 5 11 -1.90 4.50 -2 5 10 0.80 4.60 -2 5 9 9.10 5.30 -2 5 8 0.50 4.10 -2 5 7 2.80 2.90 -2 5 7 11.70 5.20 2 -5 -7 3.30 5.20 -2 5 6 9.30 3.30 -2 5 6 12.50 5.00 -2 -5 6 6.90 6.80 2 -5 -6 13.70 5.90 2 -5 -6 10.90 4.90 -2 5 5 2.90 2.80 -2 5 5 4.20 4.40 2 -5 -5 5.10 4.60 2 -5 -5 5.10 4.40 -2 -5 5 -4.10 6.20 2 5 -4 4.50 3.10 -2 5 4 7.00 4.20 -2 5 4 4.10 3.00 2 -5 -4 5.50 4.60 2 -5 -4 2.80 4.50 -2 -5 4 0.80 6.50 2 5 -3 1.60 2.80 -2 5 3 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5.50 3.00 -4 2 -6 9.50 4.60 4 2 6 8.30 2.40 -4 -2 -6 5.40 3.50 -4 2 -7 -6.30 4.50 4 2 7 3.00 2.90 4 2 7 0.30 2.70 -4 -2 -7 5.80 3.60 4 2 8 9.30 3.40 4 2 8 10.40 3.80 -4 2 -8 21.20 6.30 -4 -2 -8 8.10 4.50 -4 2 -9 15.10 7.00 4 2 9 15.10 4.50 4 2 9 9.70 4.10 -4 -2 -9 12.20 5.20 4 2 10 13.60 4.80 -4 2 -10 10.90 7.40 4 2 10 7.80 4.20 -4 -2 -10 10.80 5.60 -4 2 -11 95.99 11.60 4 2 11 99.19 11.20 4 2 11 70.69 7.50 -4 -2 -11 88.69 10.20 4 2 12 -4.40 5.60 4 2 12 3.20 4.60 -4 2 -12 13.20 9.10 -4 -2 -12 1.60 6.00 -4 2 -13 -3.30 8.20 4 2 13 -1.40 5.60 4 2 13 -7.20 4.60 -4 -2 -13 5.10 5.80 -4 2 -14 0.80 8.60 4 2 14 -11.40 5.00 4 2 14 -10.20 6.00 -4 -2 -14 4.50 5.70 -4 2 -15 -8.30 8.20 -4 -2 -15 12.90 6.50 -4 2 -16 1.80 9.00 -4 -2 -16 10.20 6.50 -4 2 -17 2.90 9.30 -4 -2 -17 22.90 7.40 -4 3 17 -9.70 4.40 4 3 -17 2.40 9.10 4 3 -16 13.60 8.70 -4 3 15 2.00 4.60 4 3 -15 9.50 8.20 -4 3 15 -15.60 5.40 -4 3 14 -8.80 4.90 4 3 -14 1.00 6.90 -4 3 14 -0.90 4.00 -4 3 13 11.70 5.00 4 3 -13 16.10 7.50 -4 3 13 7.90 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36.80 7.80 4 -4 -5 24.70 5.70 4 -4 -5 20.60 4.50 -4 4 4 62.79 8.60 4 4 -4 45.60 5.80 -4 4 4 37.70 4.70 -4 -4 4 46.30 7.60 4 -4 -4 44.10 5.30 4 -4 -4 41.20 6.40 -4 4 3 -0.80 2.60 4 4 -3 0.60 2.20 -4 4 3 0.70 2.50 4 -4 -3 2.50 3.70 4 -4 -3 -2.00 3.90 -4 -4 3 -0.30 5.40 -4 4 2 17.50 4.30 4 4 -2 12.90 3.40 -4 4 2 15.40 3.50 -4 -4 2 16.30 5.90 4 -4 -2 20.30 4.90 4 -4 -2 24.10 5.00 4 4 -1 101.09 8.70 4 4 -1 94.69 7.70 -4 4 1 103.29 8.60 4 -4 -1 93.09 8.50 4 -4 -1 93.69 8.40 -4 -4 1 101.59 9.90 4 4 0 6.00 2.60 4 4 0 10.70 3.50 -4 4 0 8.70 3.40 -4 -4 0 12.00 5.10 4 -4 0 6.60 4.80 4 -4 0 7.00 3.60 4 4 1 12.10 2.80 4 4 1 16.90 4.20 -4 4 -1 11.40 3.80 -4 -4 -1 22.40 5.70 4 -4 1 15.60 4.30 4 -4 1 15.90 5.40 -4 4 -2 6.60 3.50 4 4 2 6.40 3.50 4 4 2 5.90 2.20 -4 -4 -2 5.60 5.00 4 -4 2 4.60 3.40 4 4 3 15.40 2.60 4 4 3 20.30 4.80 4 -4 3 23.50 4.60 -4 -4 -3 23.70 5.40 4 4 4 77.29 5.80 4 4 4 83.09 9.80 4 -4 4 70.89 6.90 -4 -4 -4 75.59 8.40 4 4 5 31.40 3.60 4 4 5 33.70 6.20 -4 -4 -5 37.00 6.10 4 -4 5 41.60 5.40 4 4 6 -0.70 3.10 4 4 6 3.30 3.90 4 -4 6 8.60 3.50 -4 -4 -6 4.30 5.00 4 4 7 13.60 5.00 -4 4 -7 4.60 7.60 4 -4 7 7.20 3.30 -4 -4 -7 16.30 5.40 -4 4 -8 6.00 8.20 4 4 8 4.50 4.50 -4 -4 -8 -1.70 4.50 4 4 9 40.00 7.40 -4 4 -9 68.79 11.00 -4 -4 -9 55.19 7.20 -4 4 -10 42.90 9.90 4 4 10 25.10 6.90 -4 -4 -10 49.99 7.10 -4 4 -11 1.10 8.80 4 4 11 -8.00 4.10 -4 -4 -11 7.70 5.10 -4 4 -12 -1.40 9.40 4 4 12 -5.70 4.60 -4 -4 -12 2.50 5.30 4 4 13 -6.70 5.20 -4 4 -13 -9.40 9.40 4 4 14 -9.00 5.70 -4 4 -14 -11.90 10.00 -4 5 13 -3.60 5.10 -4 5 12 -2.60 5.20 -4 5 11 -2.60 4.30 -4 5 10 0.90 4.50 4 -5 -10 -5.40 5.80 -4 5 9 -4.60 3.10 -4 5 9 -0.30 4.10 4 -5 -9 1.90 5.30 -4 5 8 -1.40 2.90 -4 5 8 -1.10 3.80 4 -5 -8 -1.60 4.90 -4 5 7 -0.20 2.60 -4 5 7 -0.50 4.00 -4 -5 7 -2.60 6.60 4 -5 -7 2.00 4.90 -4 5 6 4.90 3.10 -4 5 6 12.30 4.80 -4 -5 6 1.20 6.40 4 -5 -6 12.80 5.70 -4 5 5 14.40 3.80 -4 5 5 19.60 5.70 -4 -5 5 14.10 7.20 4 -5 -5 18.00 5.80 -4 5 4 20.10 5.80 -4 5 4 21.40 4.20 4 5 -4 13.00 3.90 4 -5 -4 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76.59 8.30 5 -1 -9 78.09 6.40 -5 1 8 559.74 21.70 -5 1 8 574.54 23.10 5 -1 -8 542.45 21.60 -5 -1 8 532.65 22.30 5 -1 -8 526.85 20.00 -5 1 7 1.70 2.00 -5 -1 7 4.00 3.20 5 -1 -7 0.90 2.00 5 -1 -7 1.10 2.30 -5 1 6 22.50 2.90 5 -1 -6 30.60 2.90 5 -1 -6 23.80 3.50 -5 -1 6 20.00 3.60 -5 -1 6 22.30 4.10 -5 1 5 1.90 1.70 -5 -1 5 6.30 2.60 5 -1 -5 3.90 1.40 -5 -1 5 0.20 3.30 5 -1 -5 1.50 2.40 -5 -1 4 113.39 7.30 -5 -1 4 109.49 7.10 -5 -1 4 116.69 5.20 5 -1 -4 107.29 6.90 -5 1 3 32.30 3.90 -5 -1 3 35.90 3.40 -5 -1 3 24.80 4.00 -5 -1 3 24.30 3.00 5 -1 -3 31.00 4.10 5 1 -2 100.29 5.60 -5 1 2 84.49 3.80 -5 1 2 85.29 5.30 -5 1 2 79.19 3.70 -5 -1 2 86.69 5.00 5 -1 -2 82.09 6.10 -5 -1 2 83.79 6.20 -5 -1 2 89.39 5.70 5 1 -1 338.07 13.40 5 1 -1 337.47 11.70 -5 1 1 315.97 11.70 -5 1 1 320.37 12.80 -5 -1 1 319.67 13.00 -5 -1 1 314.27 12.70 -5 -1 1 327.37 11.90 5 -1 -1 314.07 13.10 -5 1 0 174.18 7.50 5 1 0 171.48 8.90 5 1 0 163.78 6.20 -5 1 0 191.28 8.40 -5 -1 0 157.48 8.30 5 -1 0 166.28 7.40 -5 1 -1 44.80 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7.20 -5 5 4 24.70 6.20 5 5 -4 20.20 4.50 -5 5 4 16.70 3.90 5 -5 -4 12.70 5.00 5 -5 -4 26.10 6.30 -5 -5 4 24.20 7.40 -5 5 3 4.50 3.70 -5 5 3 3.30 3.10 5 5 -3 2.80 3.30 5 -5 -3 8.50 4.50 -5 -5 3 7.70 6.30 5 -5 -3 3.40 4.80 -5 5 2 47.40 7.40 5 5 -2 47.30 5.80 5 5 -2 46.00 6.60 -5 5 2 46.20 6.10 5 -5 -2 58.19 7.60 5 -5 -2 43.50 6.70 -5 -5 2 52.79 8.30 5 5 -1 38.30 6.30 -5 5 1 40.70 6.70 5 5 -1 39.80 5.40 -5 5 1 33.60 5.70 5 -5 -1 44.10 6.90 5 -5 -1 45.30 7.10 -5 -5 1 49.10 7.90 5 5 0 13.90 4.70 -5 5 0 9.80 4.00 -5 5 0 16.30 4.80 5 5 0 8.90 3.40 5 -5 0 15.80 4.90 -5 -5 0 16.50 6.50 -5 5 -1 11.40 4.20 5 5 1 11.70 4.50 5 5 1 12.00 5.10 5 -5 1 15.60 4.70 -5 -5 -1 6.30 5.90 -5 5 -2 5.80 4.00 5 5 2 5.10 4.20 -5 -5 -2 0.60 5.30 5 -5 2 7.50 4.10 5 5 3 3.70 4.20 -5 5 -3 6.80 3.90 5 -5 3 10.50 4.10 -5 -5 -3 7.80 5.60 5 5 4 107.09 12.00 -5 5 -4 88.59 10.80 5 -5 4 85.29 7.80 -5 -5 -4 95.69 9.80 5 5 5 22.40 6.20 5 -5 5 34.70 5.60 -5 -5 -5 32.60 6.50 5 5 6 15.80 6.00 -5 5 -6 40.30 9.00 -5 -5 -6 12.20 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9.40 10 6 4 -4.00 5.90 -10 6 -4 9.00 5.00 -10 -6 -4 10.60 6.70 -10 6 -5 3.40 9.50 10 6 5 -6.50 5.90 -10 6 -5 1.40 4.30 -10 -6 -5 -1.30 6.40 -11 0 18 1.40 7.20 -11 0 17 -0.60 7.00 11 0 -17 7.00 6.70 -11 0 16 -9.70 5.90 11 0 -16 -4.10 5.80 -11 0 15 -4.30 6.20 11 0 -15 0.10 5.40 11 0 -14 -0.80 5.60 -11 0 14 -0.90 5.40 -11 0 14 0.60 2.40 11 0 -14 0.80 3.30 11 0 -13 2.60 3.10 -11 0 13 -0.20 4.80 11 0 -13 0.90 5.20 -11 0 13 2.20 2.40 11 0 -12 17.40 5.20 11 0 -12 17.40 3.70 -11 0 12 13.70 5.50 11 0 -11 -0.70 2.60 -11 0 11 3.10 4.10 11 0 -11 -3.40 3.70 -11 0 10 118.89 9.10 11 0 -10 118.09 7.30 -11 0 9 6.10 3.50 11 0 -9 3.80 2.90 -11 0 8 -3.20 2.90 -11 0 8 0.00 2.70 11 0 -8 -0.60 2.40 -11 0 7 2.60 2.50 11 0 -7 2.90 3.10 -11 0 7 3.80 3.00 -11 0 6 2.30 2.10 -11 0 6 1.90 2.60 -11 0 5 0.90 2.50 -11 0 5 0.20 1.60 -11 0 4 1812.22 62.59 -11 0 4 1833.32 61.89 -11 0 3 13.00 2.10 -11 0 3 17.60 3.10 -11 0 2 2.70 1.50 -11 0 2 -0.40 2.40 -11 0 1 1.00 1.40 -11 0 1 4.70 2.80 -11 0 0 -2.00 2.80 -11 0 0 -0.30 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5.30 6.50 -15 3 4 41.80 4.30 -15 3 4 32.00 4.90 -15 -3 4 37.90 7.50 15 -3 -4 40.20 7.00 -15 3 3 2.70 3.80 15 3 -3 11.80 8.50 -15 3 3 1.50 2.80 -15 -3 3 -4.60 5.50 15 -3 -3 -0.10 5.20 -15 3 2 57.29 6.00 15 3 -2 53.19 9.90 -15 3 2 39.30 5.70 -15 -3 2 51.99 8.10 15 -3 -2 58.29 8.10 15 3 -1 46.90 9.70 -15 3 1 35.90 5.40 -15 3 1 49.20 6.30 15 -3 -1 47.10 7.60 -15 -3 1 51.49 8.00 15 3 0 17.00 8.30 -15 3 0 13.60 4.30 -15 3 0 11.70 5.30 -15 -3 0 2.40 5.70 15 -3 0 13.80 5.90 -15 3 -1 21.40 6.20 -15 3 -1 15.50 4.50 15 3 1 14.30 8.20 15 -3 1 22.50 6.80 -15 -3 -1 21.30 6.80 15 3 2 9.50 7.90 -15 3 -2 2.00 3.70 -15 3 -2 6.30 6.20 -15 -3 -2 1.70 6.10 15 -3 2 2.60 6.10 -15 3 -3 0.30 3.90 -15 3 -3 3.20 6.70 15 3 3 1.60 7.80 -15 -3 -3 -3.30 6.20 -15 3 -4 14.90 5.00 15 3 4 13.80 8.90 -15 3 -4 23.30 7.90 -15 -3 -4 23.40 7.60 -15 3 -5 12.70 4.80 15 3 5 5.80 8.40 -15 3 -5 20.50 7.80 -15 -3 -5 13.50 7.00 -15 3 -6 8.90 7.70 15 3 6 -1.60 8.50 -15 3 -6 4.00 4.10 -15 -3 -6 9.20 6.70 -15 3 -7 2.30 7.00 15 3 7 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3.20 -20 0 8 9.00 4.40 -20 0 7 2.70 4.30 -20 0 7 3.00 3.10 -20 0 6 4.90 3.10 -20 0 6 8.20 4.50 -20 0 5 6.00 4.60 -20 0 5 4.90 2.70 -20 0 4 122.69 9.30 -20 0 4 127.69 8.90 -20 0 3 -3.50 4.50 -20 0 3 -0.80 2.10 -20 0 2 0.40 2.10 -20 0 2 0.20 4.70 -20 0 1 -1.50 5.20 -20 0 1 2.50 2.30 -20 0 0 -1.20 2.20 -20 0 0 3.00 5.90 -20 0 -1 5.20 6.00 -20 0 -1 2.50 2.40 -20 0 -2 89.49 10.00 -20 0 -2 82.29 7.40 -20 0 -3 78.49 10.10 -20 0 -3 71.19 7.10 -20 0 -4 177.18 10.60 -20 0 -4 160.08 14.60 -20 0 -5 0.10 2.60 -20 0 -5 -2.40 7.00 -20 0 -6 12.90 3.80 -20 0 -6 14.60 7.30 -20 0 -7 8.50 6.90 -20 0 -8 65.99 10.20 -20 0 -9 3.40 7.70 -20 0 -10 13.10 8.40 -20 0 -11 -2.00 7.60 -20 0 -12 21.50 9.10 -20 1 17 -15.20 6.10 -20 1 16 -9.90 6.20 -20 -1 16 -13.50 7.00 -20 1 15 -4.80 5.60 20 -1 -15 9.10 4.70 -20 -1 15 -11.30 6.50 -20 1 14 1.70 5.70 -20 -1 14 5.00 6.70 20 -1 -14 21.50 5.40 -20 1 13 20.00 6.20 -20 -1 13 19.50 6.80 20 -1 -13 32.60 6.50 -20 -1 13 13.90 6.50 -20 1 12 12.60 5.30 20 -1 -12 15.00 5.70 -20 -1 12 5.70 6.10 -20 -1 12 7.10 5.80 -20 1 11 -0.10 4.30 20 1 -11 -7.00 5.50 -20 -1 11 -0.70 5.40 -20 -1 11 4.30 6.00 20 -1 -11 0.50 5.20 -20 1 10 0.40 3.80 20 -1 -10 -2.00 5.70 -20 -1 10 -0.20 5.60 -20 -1 10 -3.80 4.60 -20 1 9 3.10 3.80 -20 -1 9 2.80 4.40 20 -1 -9 11.60 6.20 -20 -1 9 2.70 5.50 -20 1 8 89.09 7.00 -20 1 8 107.19 9.40 -20 -1 8 97.89 9.80 20 -1 -8 82.99 10.70 -20 -1 8 99.89 9.50 -20 1 7 33.80 5.10 -20 1 7 29.40 4.30 -20 -1 7 27.40 4.90 -20 -1 7 38.60 6.60 -20 1 6 3.10 3.70 -20 1 6 -0.90 2.80 -20 -1 6 3.80 4.90 -20 -1 6 2.50 3.30 -20 1 5 15.20 4.30 -20 1 5 10.30 3.40 -20 -1 5 11.40 5.50 -20 -1 5 14.50 3.60 -20 1 4 10.30 4.30 -20 1 4 10.00 3.20 -20 -1 4 13.20 5.50 -20 -1 4 10.90 3.00 -20 1 3 4.70 2.80 -20 1 3 1.50 4.40 -20 -1 3 1.90 2.40 -20 -1 3 2.90 5.20 -20 1 2 5.00 2.90 -20 1 2 2.20 4.70 -20 -1 2 4.40 2.30 -20 -1 2 6.20 5.60 -20 1 1 114.19 9.90 -20 1 1 104.99 8.40 -20 -1 1 99.49 6.60 -20 -1 1 94.29 10.20 -20 1 0 6.00 5.80 -20 1 0 2.80 3.00 -20 -1 0 10.40 6.40 -20 -1 0 2.60 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21.90 9.20 -28 3 11 -6.00 4.60 -28 -3 11 -13.10 7.10 28 -3 -11 11.70 6.90 -28 3 10 2.00 4.80 28 -3 -10 16.70 7.20 -28 -3 10 4.30 8.50 -28 3 9 -0.80 4.70 28 -3 -9 9.60 6.80 -28 -3 9 -9.20 7.10 -28 3 8 -8.50 4.10 28 -3 -8 4.30 7.30 -28 -3 8 -4.90 7.20 -28 3 7 -3.80 4.10 28 -3 -7 0.00 7.20 -28 -3 7 7.30 7.80 -28 3 6 3.00 4.40 -28 -3 6 4.50 7.80 28 -3 -6 7.90 7.80 -28 3 5 4.40 4.60 28 -3 -5 -3.10 7.80 -28 -3 5 -3.80 7.00 -28 3 4 6.60 4.70 28 -3 -4 0.20 7.90 -28 -3 4 8.20 7.30 -28 3 3 9.10 4.90 28 -3 -3 -14.90 8.50 -28 -3 3 3.10 7.30 -28 3 2 0.70 4.40 28 -3 -2 -20.00 8.70 -28 -3 2 2.90 8.00 -28 3 1 0.50 4.40 -28 -3 1 7.10 8.00 -28 3 0 2.10 4.50 -28 -3 0 11.80 8.40 -28 3 -1 0.00 4.30 -28 -3 -1 11.20 8.50 -29 0 14 -16.20 6.00 -29 0 13 -11.30 5.80 29 0 -12 -19.60 7.20 -29 0 12 -12.50 5.20 -29 0 11 -7.20 5.00 -29 0 10 -0.70 5.00 -29 0 9 -0.50 4.60 -29 0 8 0.40 4.30 -29 0 7 -1.30 3.90 -29 0 6 0.80 7.00 -29 0 6 -5.10 3.60 -29 0 5 -2.00 3.40 -29 0 5 2.70 5.90 -29 0 4 -1.80 3.40 -29 0 4 0.60 5.90 -29 0 3 -1.50 3.40 -29 0 3 0.00 6.00 -29 0 2 4.50 6.60 -29 0 1 3.20 7.10 -29 0 0 10.10 7.20 -29 0 -1 6.40 7.20 -29 0 -2 25.50 8.70 -29 0 -3 16.10 8.30 -29 0 -4 9.90 8.30 -29 1 14 -11.70 6.10 29 -1 -14 6.80 6.10 -29 1 13 0.90 5.80 29 -1 -13 9.10 6.70 -29 1 12 -7.50 5.00 29 -1 -12 10.70 7.90 -29 1 11 -6.20 4.30 29 -1 -11 -2.00 7.30 -29 1 10 -4.80 4.30 29 -1 -10 -16.50 7.70 -29 -1 10 -15.10 5.30 -29 1 9 -2.50 4.20 -29 -1 9 -8.80 4.90 -29 -1 9 0.50 6.60 -29 1 8 0.00 4.20 -29 -1 8 -6.80 4.60 -29 -1 8 -2.10 6.30 -29 1 7 11.80 4.90 -29 -1 7 1.90 5.00 -29 -1 7 16.40 6.60 -29 1 6 13.10 5.10 -29 -1 6 20.40 7.20 -29 1 5 1.20 4.00 -29 -1 5 8.30 6.80 -29 1 4 -2.10 3.60 -29 -1 4 8.90 7.10 -29 1 3 -0.70 3.40 -29 -1 3 1.80 7.00 -29 1 2 2.80 3.70 -29 1 2 4.90 6.30 -29 -1 2 2.60 6.70 -29 1 1 33.60 8.10 -29 1 1 20.80 5.00 -29 -1 1 39.70 9.10 -29 1 0 17.40 7.90 -29 1 0 4.40 4.10 -29 -1 0 11.80 8.10 -29 1 -1 11.90 7.70 -29 1 -1 4.00 4.20 -29 -1 -1 5.30 7.80 -29 1 -2 8.10 7.50 -29 -1 -2 -4.60 6.90 -29 1 -3 14.30 7.90 -29 -1 -3 3.00 7.70 -29 1 -4 18.50 8.30 -29 -1 -4 10.40 8.00 -29 2 13 -8.10 5.10 29 -2 -13 13.90 7.20 -29 2 12 -4.40 4.90 -29 -2 12 -10.70 9.40 29 -2 -12 9.30 6.30 -29 2 11 6.90 5.60 29 -2 -11 21.20 8.10 -29 -2 11 10.10 7.60 -29 2 10 -5.40 4.70 29 -2 -10 -9.00 6.60 -29 -2 10 -8.10 6.50 -29 2 9 -2.00 4.40 -29 -2 9 6.80 7.50 29 -2 -9 -1.60 7.40 -29 2 8 1.80 4.70 -29 -2 8 0.90 7.30 29 -2 -8 -6.60 7.80 -29 2 7 -2.00 4.10 29 -2 -7 -15.40 8.10 -29 -2 7 -1.00 7.20 -29 2 6 -1.50 4.00 -29 -2 6 -2.00 6.80 29 -2 -6 -17.10 8.80 -29 2 5 -0.10 3.70 -29 -2 5 -1.70 6.80 -29 2 4 5.50 4.20 -29 -2 4 8.10 7.70 -29 2 3 18.60 5.40 -29 -2 3 17.70 8.10 -29 2 2 3.50 4.10 -29 -2 2 -5.80 7.10 -29 2 1 -3.80 3.60 -29 -2 1 0.60 7.60 -29 2 0 -2.70 3.90 -29 -2 0 7.90 8.00 -29 2 -1 1.80 4.20 -29 -2 -1 -2.30 7.30 -29 2 -2 1.30 4.00 -29 2 -2 8.70 7.20 -29 -2 -2 4.80 7.60 -29 2 -3 4.10 4.40 -29 2 -3 10.20 7.50 -29 -2 -3 8.10 8.20 -29 3 10 -0.10 5.30 29 -3 -10 20.10 7.50 -29 3 9 -0.50 4.70 -29 -3 9 -7.10 7.30 29 -3 -9 10.00 6.70 -29 3 8 3.00 5.00 29 -3 -8 2.10 7.60 -29 -3 8 -0.20 7.40 -29 3 7 -4.80 4.10 29 -3 -7 10.80 7.90 -29 -3 7 -9.50 7.60 -29 3 6 4.90 4.80 -29 -3 6 7.10 8.20 29 -3 -6 7.30 8.00 -29 3 5 5.30 4.70 -29 -3 5 -2.00 7.80 29 -3 -5 6.40 8.40 -29 3 4 2.00 4.60 -29 -3 4 -5.10 7.40 29 -3 -4 -9.50 7.90 -29 3 3 4.30 4.60 29 -3 -3 -17.70 8.00 -29 -3 3 -0.30 7.40 -29 3 2 3.20 4.90 29 -3 -2 -25.10 9.20 -29 -3 2 5.50 8.10 -29 3 1 8.20 5.20 -29 -3 1 3.30 7.50 -29 3 0 4.40 5.10 -29 -3 0 2.40 7.90 -30 0 13 -17.40 6.10 30 0 -12 0.80 9.00 -30 0 12 2.20 6.20 -30 0 11 -7.80 5.00 -30 0 10 -3.80 4.90 -30 0 9 -7.20 4.50 -30 0 8 -1.90 4.20 -30 0 7 -6.70 3.80 -30 0 6 42.40 6.30 -30 0 5 -3.00 3.80 -30 0 5 6.00 6.10 -30 0 4 5.30 6.30 -30 0 4 -3.50 3.50 -30 0 3 4.90 6.60 -30 0 2 14.10 7.40 -30 0 1 3.40 6.90 -30 0 0 14.90 8.00 -30 0 -1 9.70 7.40 -30 0 -2 37.60 9.40 -30 0 -3 13.50 8.50 -30 1 13 -12.60 5.30 30 -1 -13 4.30 6.70 -30 1 12 1.80 5.60 30 -1 -12 7.70 7.70 -30 1 11 -2.90 4.80 30 -1 -11 -4.30 7.40 -30 1 10 -5.80 4.70 30 -1 -10 -13.60 8.50 -30 1 9 -2.80 4.40 -30 1 8 -2.10 4.30 -30 -1 8 -8.40 5.90 -30 1 7 -4.60 3.80 -30 -1 7 -2.40 6.10 -30 1 6 -1.50 4.10 -30 -1 6 -5.30 6.20 -30 1 5 -2.50 3.60 -30 -1 5 -0.80 6.60 -30 1 4 -2.40 3.60 -30 -1 4 4.70 6.80 -30 1 3 -1.30 3.50 -30 -1 3 9.60 7.00 -30 1 2 0.10 3.80 -30 -1 2 -0.40 6.90 -30 1 1 23.50 7.60 -30 1 1 11.00 4.60 -30 -1 1 21.40 8.20 -30 1 0 -1.70 5.20 -30 1 0 15.00 7.40 -30 -1 0 -2.40 7.20 -30 1 -1 10.60 7.60 -30 -1 -1 12.20 8.40 -30 1 -2 21.50 7.80 -30 -1 -2 -2.20 7.30 -30 1 -3 17.30 8.20 -30 -1 -3 4.00 7.60 30 -2 -12 22.90 7.70 -30 2 11 6.90 6.00 30 -2 -11 22.20 8.50 -30 -2 11 15.80 8.30 -30 2 10 -2.40 4.80 -30 -2 10 6.00 7.30 30 -2 -10 9.70 8.00 -30 2 9 -4.60 4.50 -30 -2 9 -9.00 6.80 30 -2 -9 -4.00 7.80 -30 2 8 -3.30 4.30 30 -2 -8 -13.00 7.40 -30 -2 8 3.10 7.40 -30 2 7 -1.80 4.50 -30 -2 7 0.30 7.00 30 -2 -7 -17.30 8.70 -30 2 6 -3.30 4.00 -30 -2 6 6.10 7.50 -30 2 5 -3.40 3.90 -30 -2 5 -1.60 6.70 -30 2 4 0.10 4.00 -30 -2 4 2.50 7.20 -30 2 3 -0.70 4.20 -30 -2 3 -7.20 7.00 -30 2 2 -3.80 3.80 -30 -2 2 4.50 7.80 -30 2 1 3.30 4.50 -30 -2 1 4.50 7.80 -30 2 0 -0.20 3.90 -30 -2 0 -3.90 7.20 -30 2 -1 -1.40 4.40 -30 -2 -1 -4.00 7.30 -30 3 7 -4.90 4.10 -30 -3 7 6.20 7.80 30 -3 -7 6.80 7.90 -30 3 6 0.30 4.30 -30 -3 6 12.30 8.80 30 -3 -6 -8.20 7.20 -30 3 5 -1.60 4.40 -30 -3 5 17.80 8.80 30 -3 -5 -6.90 8.10 -30 3 4 0.60 4.70 -30 -3 4 6.70 8.10 30 -3 -4 -9.60 8.00 -30 3 3 4.20 5.00 -30 -3 3 7.70 7.90 -31 0 12 -11.10 5.60 -31 0 11 -14.10 5.20 -31 0 10 -7.90 5.20 -31 0 9 -7.40 4.80 -31 0 8 5.70 5.10 -31 0 7 -8.50 4.00 -31 0 6 1.90 4.40 -31 0 5 -3.60 5.20 -31 0 4 0.20 6.20 -31 0 3 8.30 7.00 -31 0 2 0.60 6.90 -31 0 1 11.50 7.40 -31 0 0 17.50 8.30 -31 0 -1 4.30 7.20 -31 0 -2 18.60 8.60 -31 1 12 -8.00 5.40 31 -1 -12 15.00 8.50 -31 1 11 -3.10 4.90 31 -1 -11 -4.80 8.00 -31 1 10 -10.20 4.50 31 -1 -10 -14.70 8.20 -31 1 9 -6.20 4.10 -31 1 8 -1.70 4.60 -31 1 7 -4.40 4.00 -31 -1 7 -6.50 6.30 -31 1 6 2.20 4.40 -31 -1 6 4.30 6.80 -31 1 5 0.60 4.30 -31 -1 5 2.40 6.80 -31 1 4 -2.30 3.80 -31 -1 4 -5.40 7.00 -31 1 3 -4.00 3.70 -31 -1 3 7.40 7.50 -31 1 2 -0.60 3.60 -31 -1 2 4.30 7.20 -31 -1 1 8.00 8.00 -31 1 0 13.30 7.70 -31 -1 0 6.40 7.80 -31 1 -1 39.90 9.50 -31 -1 -1 25.30 8.70 -31 2 10 -0.80 5.10 31 -2 -10 10.60 8.10 -31 -2 10 -5.30 6.90 -31 2 9 -5.20 4.50 31 -2 -9 3.20 8.50 -31 -2 9 2.10 6.90 -31 2 8 -0.80 4.60 -31 -2 8 -4.50 7.30 31 -2 -8 -8.80 8.00 -31 2 7 -3.60 4.60 -31 -2 7 -4.00 7.20 31 -2 -7 -17.50 8.90 -31 2 6 -4.90 4.10 -31 -2 6 1.40 7.50 -31 2 5 -2.10 3.80 -31 -2 5 2.10 7.40 -31 2 4 -4.70 3.90 -31 -2 4 0.10 7.70 -31 2 3 1.60 4.60 -31 -2 3 3.50 7.80 -31 2 2 4.40 4.90 -31 -2 2 7.40 8.00 -31 2 1 2.90 4.80 -31 -2 1 9.50 8.10 -32 0 11 -14.50 5.40 -32 0 10 5.20 5.80 -32 0 9 -8.60 4.80 -32 0 8 -11.80 4.30 -32 0 7 -5.80 4.30 -32 0 3 9.50 7.10 -32 0 2 6.90 7.40 -32 0 1 8.50 7.70 -32 0 0 25.40 8.80 32 -1 -11 -10.10 8.60 -32 1 10 -11.00 4.80 -32 1 9 -3.50 5.10 -32 1 8 -7.00 4.70 -32 1 7 0.00 4.60 -32 1 6 -3.90 4.10 -32 -1 6 1.90 6.80 -32 1 5 -4.40 4.20 -32 -1 5 -7.10 6.60 -32 1 4 -4.40 4.20 -32 -1 4 17.20 8.00 -32 1 3 -3.20 4.00 -32 -1 3 4.30 7.60 -32 -1 2 6.20 7.30 -32 -1 1 24.70 9.00 32 -2 -8 -8.00 8.70 -32 2 7 -5.00 4.30 -32 -2 7 -6.90 7.10 -32 2 6 -4.10 4.60 -32 -2 6 -0.90 7.40 -32 2 5 6.30 5.00 -32 -2 5 1.90 7.70 -32 2 4 -0.30 4.30 -32 -2 4 -2.70 7.20 -33 0 8 -8.60 4.50 -33 0 2 15.70 7.60 -33 1 8 -6.40 5.00 -33 1 7 -5.20 4.50 -33 1 6 -4.10 4.40 -33 -1 6 -9.60 7.40 -33 1 5 -3.90 4.50 -33 -1 5 1.60 7.30 -33 1 4 -7.80 4.30 -33 -1 4 5.20 7.60 -33 -1 3 12.20 7.80 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 45626 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_RomanTA63b _database_code_depnum_ccdc_archive 'CCDC 2122224' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-15 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C34 H45 N2 O2 P [+ solvent]' _chemical_formula_sum 'C34 H45 N2 O2 P [+ solvent]' _chemical_formula_weight 544.69 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.0161(11) _cell_length_b 18.175(2) _cell_length_c 26.111(3) _cell_angle_alpha 79.325(4) _cell_angle_beta 78.548(3) _cell_angle_gamma 76.878(2) _cell_volume 4935.8(9) _cell_formula_units_Z 6 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 15649 _cell_measurement_theta_min 1.609 _cell_measurement_theta_max 24.359 _exptl_crystal_description block _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.099 _exptl_crystal_F_000 1764 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.210 _exptl_crystal_size_min 0.180 _exptl_absorpt_coefficient_mu 0.113 _shelx_estimated_absorpt_T_min 0.973 _shelx_estimated_absorpt_T_max 0.980 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.953 _exptl_absorpt_correction_T_max 0.960 _exptl_absorpt_process_details 'SADABS V2008/1 (Bruker AXS)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'APEX2 (Bruker AXS)' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 95 _diffrn_reflns_number 40836 _diffrn_reflns_av_unetI/netI 0.1212 _diffrn_reflns_av_R_equivalents 0.0759 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_theta_min 1.609 _diffrn_reflns_theta_max 24.359 _diffrn_reflns_theta_full 24.359 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measured_fraction_theta_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_point_group_measured_fraction_full 0.989 _reflns_number_total 15649 _reflns_number_gt 7866 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker Instrument Service v2010.7.0.0' _computing_cell_refinement 'APEX2 v2010.7-0 (Bruker AXS)' _computing_data_reduction 'SAINT V7.68A (Bruker AXS, 2009)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0675P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 15649 _refine_ls_number_parameters 1220 _refine_ls_number_restraints 1380 _refine_ls_R_factor_all 0.1472 _refine_ls_R_factor_gt 0.0601 _refine_ls_wR_factor_ref 0.1563 _refine_ls_wR_factor_gt 0.1214 _refine_ls_goodness_of_fit_ref 0.956 _refine_ls_restrained_S_all 0.919 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 1.36524(9) -0.36915(5) -0.12151(4) 0.0421(3) Uani 1 1 d . U . . . H1 H 1.483(3) -0.3671(14) -0.1123(11) 0.039(8) Uiso 1 1 d . . . . . O1 O 1.3326(2) -0.44045(12) -0.07488(9) 0.0462(7) Uani 1 1 d . U . . . O2 O 1.2817(2) -0.31324(12) -0.07756(9) 0.0469(7) Uani 1 1 d . U . . . N1 N 1.3938(3) -0.42988(15) -0.16811(12) 0.0422(8) Uani 1 1 d . U . . . N2 N 1.3312(2) -0.29519(15) -0.17143(11) 0.0371(7) Uani 1 1 d . U . . . C1 C 1.3817(3) -0.39476(19) -0.21987(16) 0.0392(9) Uani 1 1 d . U . . . C2 C 1.3994(3) -0.4270(2) -0.26521(16) 0.0487(10) Uani 1 1 d . U . . . H2 H 1.4285 -0.4805 -0.2646 0.058 Uiso 1 1 calc R U . . . C3 C 1.3740(3) -0.3800(2) -0.31202(16) 0.0483(10) Uani 1 1 d . U . . . H3 H 1.3852 -0.4019 -0.3434 0.058 Uiso 1 1 calc R U . . . C4 C 1.3330(3) -0.3024(2) -0.31350(15) 0.0460(10) Uani 1 1 d . U . . . H4 H 1.3148 -0.2712 -0.3456 0.055 Uiso 1 1 calc R U . . . C5 C 1.3182(3) -0.2696(2) -0.26795(15) 0.0405(9) Uani 1 1 d . U . . . H5 H 1.2907 -0.2160 -0.2689 0.049 Uiso 1 1 calc R U . . . C6 C 1.3436(3) -0.31538(19) -0.22157(15) 0.0350(9) Uani 1 1 d . U . . . C7 C 1.3873(3) -0.5059(2) -0.14618(16) 0.0439(10) Uani 1 1 d . U . . . C8 C 1.3520(3) -0.51082(19) -0.09208(17) 0.0448(10) Uani 1 1 d . U . . . C9 C 1.3308(3) -0.5772(2) -0.05847(16) 0.0463(10) Uani 1 1 d . U . . . C10 C 1.3518(3) -0.6406(2) -0.08432(18) 0.0584(12) Uani 1 1 d . U . . . H10 H 1.3412 -0.6880 -0.0634 0.070 Uiso 1 1 calc R U . . . C11 C 1.3871(4) -0.6392(2) -0.13840(19) 0.0581(12) Uani 1 1 d . U . . . C12 C 1.4074(3) -0.5706(2) -0.16985(17) 0.0550(11) Uani 1 1 d . U . . . H12 H 1.4345 -0.5685 -0.2069 0.066 Uiso 1 1 calc R U . . . C13 C 1.2859(3) -0.5800(2) 0.00073(16) 0.0511(11) Uani 1 1 d . U . . . C14 C 1.3774(4) -0.5531(3) 0.02722(18) 0.0820(15) Uani 1 1 d . U . . . H14D H 1.4612 -0.5860 0.0213 0.123 Uiso 1 1 calc R U . . . H14E H 1.3462 -0.5558 0.0652 0.123 Uiso 1 1 calc R U . . . H14F H 1.3831 -0.5003 0.0120 0.123 Uiso 1 1 calc R U . . . C15 C 1.1564(4) -0.5273(2) 0.01029(17) 0.0731(14) Uani 1 1 d . U . . . H15D H 1.1636 -0.4748 -0.0053 0.110 Uiso 1 1 calc R U . . . H15E H 1.1264 -0.5294 0.0484 0.110 Uiso 1 1 calc R U . . . H15F H 1.0964 -0.5438 -0.0061 0.110 Uiso 1 1 calc R U . . . C16 C 1.2727(4) -0.6605(2) 0.02889(18) 0.0824(15) Uani 1 1 d . U . . . H16D H 1.2131 -0.6791 0.0136 0.124 Uiso 1 1 calc R U . . . H16E H 1.2413 -0.6589 0.0666 0.124 Uiso 1 1 calc R U . . . H16F H 1.3553 -0.6951 0.0245 0.124 Uiso 1 1 calc R U . . . C17 C 1.4099(5) -0.7127(2) -0.1625(2) 0.0745(14) Uani 1 1 d . U . . . C18 C 1.5140(19) -0.7744(10) -0.1362(9) 0.103(6) Uani 0.51(3) 1 d . U P A 1 H18D H 1.5341 -0.8201 -0.1536 0.154 Uiso 0.51(3) 1 calc R U P A 1 H18E H 1.4821 -0.7881 -0.0986 0.154 Uiso 0.51(3) 1 calc R U P A 1 H18F H 1.5904 -0.7535 -0.1400 0.154 Uiso 0.51(3) 1 calc R U P A 1 C18D C 1.5479(15) -0.7475(12) -0.1699(12) 0.108(7) Uani 0.49(3) 1 d . U P A 2 H18G H 1.5616 -0.7957 -0.1839 0.162 Uiso 0.49(3) 1 calc R U P A 2 H18H H 1.5777 -0.7572 -0.1359 0.162 Uiso 0.49(3) 1 calc R U P A 2 H18I H 1.5947 -0.7123 -0.1949 0.162 Uiso 0.49(3) 1 calc R U P A 2 C19 C 1.293(2) -0.7464(14) -0.1472(10) 0.099(6) Uani 0.51(3) 1 d . U P A 1 H19D H 1.3089 -0.7951 -0.1607 0.148 Uiso 0.51(3) 1 calc R U P A 1 H19E H 1.2233 -0.7111 -0.1624 0.148 Uiso 0.51(3) 1 calc R U P A 1 H19F H 1.2707 -0.7549 -0.1087 0.148 Uiso 0.51(3) 1 calc R U P A 1 C19D C 1.329(3) -0.7717(16) -0.1288(12) 0.142(10) Uani 0.49(3) 1 d . U P A 2 H19G H 1.3284 -0.8109 -0.1500 0.213 Uiso 0.49(3) 1 calc R U P A 2 H19H H 1.2417 -0.7449 -0.1185 0.213 Uiso 0.49(3) 1 calc R U P A 2 H19I H 1.3652 -0.7959 -0.0971 0.213 Uiso 0.49(3) 1 calc R U P A 2 C20 C 1.454(3) -0.7017(9) -0.2206(6) 0.100(6) Uani 0.51(3) 1 d . U P A 1 H20D H 1.5326 -0.6820 -0.2283 0.149 Uiso 0.51(3) 1 calc R U P A 1 H20E H 1.3895 -0.6653 -0.2381 0.149 Uiso 0.51(3) 1 calc R U P A 1 H20F H 1.4697 -0.7508 -0.2337 0.149 Uiso 0.51(3) 1 calc R U P A 1 C20D C 1.366(3) -0.6946(10) -0.2181(7) 0.109(6) Uani 0.49(3) 1 d . U P A 2 H20G H 1.4162 -0.6604 -0.2421 0.164 Uiso 0.49(3) 1 calc R U P A 2 H20H H 1.2764 -0.6698 -0.2142 0.164 Uiso 0.49(3) 1 calc R U P A 2 H20I H 1.3776 -0.7422 -0.2326 0.164 Uiso 0.49(3) 1 calc R U P A 2 C21 C 1.2780(3) -0.22493(19) -0.15376(15) 0.0395(9) Uani 1 1 d . U . . . C22 C 1.2569(3) -0.15130(19) -0.18058(15) 0.0436(10) Uani 1 1 d . U . . . H22 H 1.2792 -0.1423 -0.2179 0.052 Uiso 1 1 calc R U . . . C23 C 1.2025(4) -0.09027(19) -0.15256(16) 0.0473(10) Uani 1 1 d . U . . . C24 C 1.1723(4) -0.1061(2) -0.09814(16) 0.0527(11) Uani 1 1 d . U . . . H24 H 1.1348 -0.0643 -0.0794 0.063 Uiso 1 1 calc R U . . . C25 C 1.1930(4) -0.1791(2) -0.06883(16) 0.0502(10) Uani 1 1 d . U . . . C26 C 1.2498(3) -0.23677(19) -0.09907(16) 0.0437(10) Uani 1 1 d . U . . . C27 C 1.1824(4) -0.0087(2) -0.18232(16) 0.0535(11) Uani 1 1 d . U . . . C28 C 1.0871(4) -0.0003(2) -0.21905(18) 0.0792(14) Uani 1 1 d . U . . . H28G H 1.1162 -0.0394 -0.2425 0.119 Uiso 1 1 calc R U . . . H28H H 1.0788 0.0505 -0.2402 0.119 Uiso 1 1 calc R U . . . H28I H 1.0049 -0.0067 -0.1980 0.119 Uiso 1 1 calc R U . . . C29 C 1.1337(6) 0.0512(2) -0.14550(19) 0.106(2) Uani 1 1 d . U . . . H29G H 1.0528 0.0427 -0.1243 0.160 Uiso 1 1 calc R U . . . H29H H 1.1220 0.1022 -0.1664 0.160 Uiso 1 1 calc R U . . . H29I H 1.1951 0.0472 -0.1221 0.160 Uiso 1 1 calc R U . . . C30 C 1.3070(4) 0.0074(2) -0.2148(2) 0.0862(15) Uani 1 1 d . U . . . H30G H 1.3689 0.0014 -0.1913 0.129 Uiso 1 1 calc R U . . . H30H H 1.2938 0.0597 -0.2337 0.129 Uiso 1 1 calc R U . . . H30I H 1.3385 -0.0286 -0.2404 0.129 Uiso 1 1 calc R U . . . C31 C 1.1604(4) -0.1951(2) -0.00873(17) 0.0623(12) Uani 1 1 d . U . . . C32 C 1.2835(5) -0.2264(3) 0.01438(17) 0.0836(15) Uani 1 1 d . U . . . H32D H 1.3237 -0.2760 0.0030 0.125 Uiso 1 1 calc R U . . . H32E H 1.2641 -0.2326 0.0530 0.125 Uiso 1 1 calc R U . . . H32F H 1.3411 -0.1905 0.0017 0.125 Uiso 1 1 calc R U . . . C33 C 1.0915(5) -0.1221(2) 0.01469(17) 0.0975(18) Uani 1 1 d . U . . . H33D H 1.1466 -0.0846 0.0062 0.146 Uiso 1 1 calc R U . . . H33E H 1.0700 -0.1345 0.0531 0.146 Uiso 1 1 calc R U . . . H33F H 1.0140 -0.1007 -0.0004 0.146 Uiso 1 1 calc R U . . . C34 C 1.0729(4) -0.2528(2) 0.00712(16) 0.0742(13) Uani 1 1 d . U . . . H34D H 0.9962 -0.2327 -0.0087 0.111 Uiso 1 1 calc R U . . . H34E H 1.0501 -0.2615 0.0457 0.111 Uiso 1 1 calc R U . . . H34F H 1.1164 -0.3010 -0.0055 0.111 Uiso 1 1 calc R U . . . P1A P 1.02168(9) 0.19370(5) 0.28967(4) 0.0416(3) Uani 1 1 d . U . . . H1A H 0.904(2) 0.1728(14) 0.3042(10) 0.032(8) Uiso 1 1 d . . . . . O1A O 1.1154(2) 0.10906(12) 0.29434(9) 0.0454(7) Uani 1 1 d . U . . . O2A O 1.0461(2) 0.19546(12) 0.35023(9) 0.0416(3) Uani 1 1 d . U . . . N1A N 1.0530(3) 0.19928(15) 0.22194(11) 0.0405(8) Uani 1 1 d . U . . . N2A N 0.9899(2) 0.29202(14) 0.27939(12) 0.0358(7) Uani 1 1 d . U . . . C1A C 1.0133(3) 0.27124(18) 0.19386(15) 0.0354(9) Uani 1 1 d . U . . . C2A C 1.0011(3) 0.2906(2) 0.14111(16) 0.0469(10) Uani 1 1 d . U . . . H2A H 1.0221 0.2527 0.1185 0.056 Uiso 1 1 calc R U . . . C3A C 0.9573(3) 0.3672(2) 0.12171(16) 0.0484(10) Uani 1 1 d . U . . . H3A H 0.9493 0.3816 0.0855 0.058 Uiso 1 1 calc R U . . . C4A C 0.9258(3) 0.4215(2) 0.15474(17) 0.0496(11) Uani 1 1 d . U . . . H4A H 0.8966 0.4733 0.1409 0.060 Uiso 1 1 calc R U . . . C5A C 0.9356(3) 0.40236(19) 0.20793(16) 0.0449(10) Uani 1 1 d . U . . . H5A H 0.9143 0.4406 0.2304 0.054 Uiso 1 1 calc R U . . . C6A C 0.9771(3) 0.32630(19) 0.22777(15) 0.0364(9) Uani 1 1 d . U . . . C7A C 1.1343(3) 0.13488(19) 0.20368(15) 0.0415(10) Uani 1 1 d . U . . . C8A C 1.1670(3) 0.08250(19) 0.24698(15) 0.0424(10) Uani 1 1 d . U . . . C9A C 1.2491(3) 0.01272(19) 0.24218(16) 0.0453(10) Uani 1 1 d . U . . . C10A C 1.2977(4) 0.0006(2) 0.19049(17) 0.0552(11) Uani 1 1 d . U . . . H10A H 1.3535 -0.0465 0.1851 0.066 Uiso 1 1 calc R U . . . C11A C 1.2704(4) 0.0527(2) 0.14595(17) 0.0548(11) Uani 1 1 d . U . . . C12A C 1.1856(3) 0.1214(2) 0.15300(16) 0.0504(11) Uani 1 1 d . U . . . H12A H 1.1640 0.1579 0.1235 0.061 Uiso 1 1 calc R U . . . C13A C 1.2789(4) -0.04525(19) 0.29111(16) 0.0508(11) Uani 1 1 d . U . . . C14A C 1.1570(4) -0.0676(2) 0.32326(18) 0.0744(14) Uani 1 1 d . U . . . H14A H 1.1005 -0.0224 0.3361 0.112 Uiso 1 1 calc R U . . . H14B H 1.1772 -0.1064 0.3534 0.112 Uiso 1 1 calc R U . . . H14C H 1.1152 -0.0881 0.3008 0.112 Uiso 1 1 calc R U . . . C15A C 1.3443(4) -0.0116(2) 0.32491(17) 0.0681(13) Uani 1 1 d . U . . . H15A H 1.4224 0.0019 0.3040 0.102 Uiso 1 1 calc R U . . . H15B H 1.3643 -0.0494 0.3556 0.102 Uiso 1 1 calc R U . . . H15C H 1.2881 0.0342 0.3369 0.102 Uiso 1 1 calc R U . . . C16A C 1.3682(4) -0.1187(2) 0.27536(18) 0.0776(15) Uani 1 1 d . U . . . H16A H 1.3278 -0.1425 0.2543 0.116 Uiso 1 1 calc R U . . . H16B H 1.3867 -0.1542 0.3073 0.116 Uiso 1 1 calc R U . . . H16C H 1.4471 -0.1061 0.2544 0.116 Uiso 1 1 calc R U . . . C17A C 1.3345(5) 0.0379(3) 0.09014(19) 0.0755(14) Uani 1 1 d . U . . . C18A C 1.3038(14) 0.1015(7) 0.0475(4) 0.123(6) Uani 0.568(12) 1 d . U P B 1 H18A H 1.2129 0.1119 0.0467 0.185 Uiso 0.568(12) 1 calc R U P B 1 H18B H 1.3505 0.0875 0.0135 0.185 Uiso 0.568(12) 1 calc R U P B 1 H18C H 1.3276 0.1473 0.0541 0.185 Uiso 0.568(12) 1 calc R U P B 1 C19A C 1.2954(13) -0.0330(7) 0.0795(5) 0.116(5) Uani 0.568(12) 1 d . U P B 1 H19A H 1.3093 -0.0745 0.1088 0.175 Uiso 0.568(12) 1 calc R U P B 1 H19B H 1.3461 -0.0491 0.0466 0.175 Uiso 0.568(12) 1 calc R U P B 1 H19C H 1.2057 -0.0207 0.0761 0.175 Uiso 0.568(12) 1 calc R U P B 1 C20A C 1.4787(9) 0.0153(8) 0.0887(4) 0.104(5) Uani 0.568(12) 1 d . U P B 1 H20A H 1.5107 0.0592 0.0935 0.156 Uiso 0.568(12) 1 calc R U P B 1 H20B H 1.5193 -0.0008 0.0545 0.156 Uiso 0.568(12) 1 calc R U P B 1 H20C H 1.4976 -0.0270 0.1171 0.156 Uiso 0.568(12) 1 calc R U P B 1 C21A C 0.9671(3) 0.32344(18) 0.32643(14) 0.0359(9) Uani 1 1 d . U . . . C22A C 0.9219(3) 0.39776(19) 0.33644(15) 0.0425(10) Uani 1 1 d . U . . . H22A H 0.9025 0.4378 0.3085 0.051 Uiso 1 1 calc R U . . . C23A C 0.9052(3) 0.4132(2) 0.38777(17) 0.0476(10) Uani 1 1 d . U . . . C24A C 0.9343(3) 0.3529(2) 0.42802(15) 0.0464(10) Uani 1 1 d . U . . . H24A H 0.9202 0.3637 0.4632 0.056 Uiso 1 1 calc R U . . . C25A C 0.9832(3) 0.2772(2) 0.41910(15) 0.0424(9) Uani 1 1 d . U . . . C26A C 0.9978(3) 0.26607(18) 0.36729(15) 0.0380(9) Uani 1 1 d . U . . . C27A C 0.8506(4) 0.4940(2) 0.40065(17) 0.0559(11) Uani 1 1 d . U . . . C28A C 0.8209(18) 0.5516(5) 0.3523(4) 0.102(5) Uani 0.637(18) 1 d . U P C 1 H28A H 0.7657 0.5336 0.3343 0.154 Uiso 0.637(18) 1 calc R U P C 1 H28B H 0.8997 0.5574 0.3281 0.154 Uiso 0.637(18) 1 calc R U P C 1 H28C H 0.7783 0.6011 0.3633 0.154 Uiso 0.637(18) 1 calc R U P C 1 C28D C 0.918(2) 0.5515(8) 0.3546(6) 0.067(5) Uani 0.363(18) 1 d . U P C 2 H28D H 0.8944 0.5495 0.3208 0.101 Uiso 0.363(18) 1 calc R U P C 2 H28E H 1.0101 0.5362 0.3522 0.101 Uiso 0.363(18) 1 calc R U P C 2 H28F H 0.8909 0.6037 0.3630 0.101 Uiso 0.363(18) 1 calc R U P C 2 C29A C 0.9335(14) 0.5142(9) 0.4310(7) 0.112(6) Uani 0.637(18) 1 d . U P C 1 H29A H 0.8980 0.5654 0.4404 0.168 Uiso 0.637(18) 1 calc R U P C 1 H29B H 1.0175 0.5136 0.4096 0.168 Uiso 0.637(18) 1 calc R U P C 1 H29C H 0.9403 0.4772 0.4632 0.168 Uiso 0.637(18) 1 calc R U P C 1 C29D C 0.896(3) 0.5139(14) 0.4500(8) 0.075(6) Uani 0.363(18) 1 d . U P C 2 H29D H 0.8762 0.5693 0.4495 0.112 Uiso 0.363(18) 1 calc R U P C 2 H29E H 0.9871 0.4952 0.4479 0.112 Uiso 0.363(18) 1 calc R U P C 2 H29F H 0.8518 0.4893 0.4828 0.112 Uiso 0.363(18) 1 calc R U P C 2 C30A C 0.7156(8) 0.4933(6) 0.4375(5) 0.057(3) Uani 0.637(18) 1 d . U P C 1 H30A H 0.6774 0.5449 0.4456 0.086 Uiso 0.637(18) 1 calc R U P C 1 H30B H 0.7266 0.4584 0.4705 0.086 Uiso 0.637(18) 1 calc R U P C 1 H30C H 0.6603 0.4760 0.4191 0.086 Uiso 0.637(18) 1 calc R U P C 1 C30D C 0.7194(15) 0.5118(13) 0.4015(14) 0.100(8) Uani 0.363(18) 1 d . U P C 2 H30D H 0.6798 0.4741 0.4272 0.150 Uiso 0.363(18) 1 calc R U P C 2 H30E H 0.7014 0.5109 0.3663 0.150 Uiso 0.363(18) 1 calc R U P C 2 H30F H 0.6854 0.5628 0.4114 0.150 Uiso 0.363(18) 1 calc R U P C 2 C31A C 1.0186(3) 0.2121(2) 0.46325(15) 0.0478(10) Uani 1 1 d . U . . . C32A C 0.9491(4) 0.1478(2) 0.46495(16) 0.0650(12) Uani 1 1 d . U . . . H32A H 0.8583 0.1686 0.4673 0.098 Uiso 1 1 calc R U . . . H32B H 0.9644 0.1093 0.4959 0.098 Uiso 1 1 calc R U . . . H32C H 0.9800 0.1241 0.4328 0.098 Uiso 1 1 calc R U . . . C33A C 0.9862(4) 0.2386(2) 0.51755(16) 0.0757(14) Uani 1 1 d . U . . . H33A H 1.0293 0.2804 0.5170 0.113 Uiso 1 1 calc R U . . . H33B H 1.0137 0.1959 0.5444 0.113 Uiso 1 1 calc R U . . . H33C H 0.8946 0.2565 0.5260 0.113 Uiso 1 1 calc R U . . . C34A C 1.1620(3) 0.1821(2) 0.45189(17) 0.0699(13) Uani 1 1 d . U . . . H34A H 1.1847 0.1646 0.4173 0.105 Uiso 1 1 calc R U . . . H34B H 1.1863 0.1395 0.4793 0.105 Uiso 1 1 calc R U . . . H34C H 1.2063 0.2232 0.4518 0.105 Uiso 1 1 calc R U . . . C35 C 1.408(2) -0.0420(9) 0.0872(6) 0.132(8) Uani 0.432(12) 1 d . U P B 2 H35A H 1.4751 -0.0529 0.1086 0.198 Uiso 0.432(12) 1 calc R U P B 2 H35B H 1.4451 -0.0472 0.0504 0.198 Uiso 0.432(12) 1 calc R U P B 2 H35C H 1.3511 -0.0782 0.1006 0.198 Uiso 0.432(12) 1 calc R U P B 2 C36 C 1.4214(15) 0.0983(10) 0.0681(6) 0.117(7) Uani 0.432(12) 1 d . U P B 2 H36A H 1.3727 0.1495 0.0730 0.175 Uiso 0.432(12) 1 calc R U P B 2 H36B H 1.4523 0.0966 0.0303 0.175 Uiso 0.432(12) 1 calc R U P B 2 H36C H 1.4933 0.0865 0.0871 0.175 Uiso 0.432(12) 1 calc R U P B 2 C37 C 1.2280(16) 0.0544(10) 0.0549(6) 0.109(6) Uani 0.432(12) 1 d . U P B 2 H37A H 1.1613 0.0263 0.0724 0.164 Uiso 0.432(12) 1 calc R U P B 2 H37B H 1.2641 0.0380 0.0205 0.164 Uiso 0.432(12) 1 calc R U P B 2 H37C H 1.1922 0.1093 0.0499 0.164 Uiso 0.432(12) 1 calc R U P B 2 P1B P 1.69362(9) -0.34977(5) -0.35671(4) 0.0380(3) Uani 1 1 d . U . . . H1B H 1.815(2) -0.3470(13) -0.3812(10) 0.027(7) Uiso 1 1 d . . . . . O1B O 1.6219(2) -0.32574(11) -0.40977(9) 0.0415(6) Uani 1 1 d . U . . . O2B O 1.6844(2) -0.43880(11) -0.35966(9) 0.0402(6) Uani 1 1 d . U . . . N1B N 1.6257(2) -0.26022(14) -0.33973(12) 0.0372(7) Uani 1 1 d . U . . . N2B N 1.7179(2) -0.37762(14) -0.29174(11) 0.0362(7) Uani 1 1 d . U . . . C1B C 1.6314(3) -0.25124(18) -0.28787(15) 0.0355(9) Uani 1 1 d . U . . . C2B C 1.5925(3) -0.18696(19) -0.26362(16) 0.0432(10) Uani 1 1 d . U . . . H2B H 1.5579 -0.1396 -0.2828 0.052 Uiso 1 1 calc R U . . . C3B C 1.6039(3) -0.1914(2) -0.21097(16) 0.0476(10) Uani 1 1 d . U . . . H3B H 1.5776 -0.1470 -0.1941 0.057 Uiso 1 1 calc R U . . . C4B C 1.6532(3) -0.2599(2) -0.18338(15) 0.0466(10) Uani 1 1 d . U . . . H4B H 1.6586 -0.2626 -0.1472 0.056 Uiso 1 1 calc R U . . . C5B C 1.6951(3) -0.3252(2) -0.20705(15) 0.0433(10) Uani 1 1 d . U . . . H5B H 1.7306 -0.3721 -0.1878 0.052 Uiso 1 1 calc R U . . . C6B C 1.6842(3) -0.32034(18) -0.25927(15) 0.0354(9) Uani 1 1 d . U . . . C7B C 1.5520(3) -0.21300(18) -0.37575(14) 0.0369(9) Uani 1 1 d . U . . . C8B C 1.5530(3) -0.25200(18) -0.41639(15) 0.0367(9) Uani 1 1 d . U . . . C9B C 1.4892(3) -0.22117(19) -0.45870(14) 0.0384(9) Uani 1 1 d . U . . . C10B C 1.4174(3) -0.14696(19) -0.45602(15) 0.0419(10) Uani 1 1 d . U . . . H10B H 1.3719 -0.1230 -0.4840 0.050 Uiso 1 1 calc R U . . . C11B C 1.4094(3) -0.10689(18) -0.41463(15) 0.0387(9) Uani 1 1 d . U . . . C12B C 1.4799(3) -0.14027(18) -0.37412(14) 0.0400(9) Uani 1 1 d . U . . . H12B H 1.4781 -0.1133 -0.3460 0.048 Uiso 1 1 calc R U . . . C13B C 1.4985(3) -0.2644(2) -0.50436(15) 0.0446(10) Uani 1 1 d . U . . . C14B C 1.6370(4) -0.2869(2) -0.52933(15) 0.0592(12) Uani 1 1 d . U . . . H14G H 1.6737 -0.2411 -0.5407 0.089 Uiso 1 1 calc R U . . . H14H H 1.6422 -0.3122 -0.5600 0.089 Uiso 1 1 calc R U . . . H14I H 1.6837 -0.3219 -0.5033 0.089 Uiso 1 1 calc R U . . . C15B C 1.4413(4) -0.3362(2) -0.48366(16) 0.0629(12) Uani 1 1 d . U . . . H15G H 1.4875 -0.3687 -0.4565 0.094 Uiso 1 1 calc R U . . . H15H H 1.4479 -0.3645 -0.5129 0.094 Uiso 1 1 calc R U . . . H15I H 1.3523 -0.3211 -0.4684 0.094 Uiso 1 1 calc R U . . . C16B C 1.4266(4) -0.2159(2) -0.54819(15) 0.0597(12) Uani 1 1 d . U . . . H16G H 1.3365 -0.2026 -0.5338 0.090 Uiso 1 1 calc R U . . . H16H H 1.4376 -0.2453 -0.5773 0.090 Uiso 1 1 calc R U . . . H16I H 1.4599 -0.1691 -0.5613 0.090 Uiso 1 1 calc R U . . . C17B C 1.3246(3) -0.02761(19) -0.41161(15) 0.0464(10) Uani 1 1 d . U . . . C18B C 1.2241(8) -0.0356(5) -0.3636(3) 0.082(4) Uani 0.734(14) 1 d . U P D 1 H18J H 1.1661 0.0136 -0.3610 0.123 Uiso 0.734(14) 1 calc R U P D 1 H18K H 1.2639 -0.0518 -0.3319 0.123 Uiso 0.734(14) 1 calc R U P D 1 H18L H 1.1772 -0.0739 -0.3668 0.123 Uiso 0.734(14) 1 calc R U P D 1 C18E C 1.301(3) 0.0015(13) -0.3556(8) 0.081(9) Uani 0.266(14) 1 d . U P D 2 H18M H 1.2191 0.0370 -0.3511 0.122 Uiso 0.266(14) 1 calc R U P D 2 H18N H 1.3682 0.0276 -0.3540 0.122 Uiso 0.266(14) 1 calc R U P D 2 H18O H 1.2999 -0.0423 -0.3274 0.122 Uiso 0.266(14) 1 calc R U P D 2 C19B C 1.2533(10) -0.0009(5) -0.4597(4) 0.084(3) Uani 0.734(14) 1 d . U P D 1 H19J H 1.2031 -0.0384 -0.4611 0.126 Uiso 0.734(14) 1 calc R U P D 1 H19K H 1.3147 0.0038 -0.4924 0.126 Uiso 0.734(14) 1 calc R U P D 1 H19L H 1.1973 0.0488 -0.4560 0.126 Uiso 0.734(14) 1 calc R U P D 1 C19E C 1.196(2) -0.0176(11) -0.4253(12) 0.066(7) Uani 0.266(14) 1 d . U P D 2 H19M H 1.1462 0.0325 -0.4181 0.100 Uiso 0.266(14) 1 calc R U P D 2 H19N H 1.1535 -0.0578 -0.4040 0.100 Uiso 0.266(14) 1 calc R U P D 2 H19O H 1.2032 -0.0210 -0.4629 0.100 Uiso 0.266(14) 1 calc R U P D 2 C20B C 1.3996(8) 0.0282(4) -0.4090(5) 0.093(4) Uani 0.734(14) 1 d . U P D 1 H20J H 1.4692 0.0275 -0.4390 0.139 Uiso 0.734(14) 1 calc R U P D 1 H20K H 1.4338 0.0151 -0.3759 0.139 Uiso 0.734(14) 1 calc R U P D 1 H20L H 1.3458 0.0793 -0.4105 0.139 Uiso 0.734(14) 1 calc R U P D 1 C20E C 1.395(2) 0.0335(11) -0.4512(13) 0.096(10) Uani 0.266(14) 1 d . U P D 2 H20M H 1.4101 0.0212 -0.4872 0.144 Uiso 0.266(14) 1 calc R U P D 2 H20N H 1.4766 0.0320 -0.4406 0.144 Uiso 0.266(14) 1 calc R U P D 2 H20O H 1.3430 0.0847 -0.4501 0.144 Uiso 0.266(14) 1 calc R U P D 2 C21B C 1.7463(3) -0.45704(19) -0.27804(15) 0.0393(9) Uani 1 1 d . U . . . C22B C 1.7895(3) -0.50114(19) -0.23364(15) 0.0499(11) Uani 1 1 d . U . . . H22B H 1.8049 -0.4776 -0.2066 0.060 Uiso 1 1 calc R U . . . C23B C 1.8101(4) -0.5801(2) -0.22910(16) 0.0498(11) Uani 1 1 d . U . . . C24B C 1.7836(3) -0.6124(2) -0.26868(16) 0.0473(10) Uani 1 1 d . U . . . H24B H 1.7968 -0.6665 -0.2648 0.057 Uiso 1 1 calc R U . . . C25B C 1.7383(3) -0.56967(19) -0.31437(15) 0.0385(9) Uani 1 1 d . U . . . C26B C 1.7254(3) -0.49134(19) -0.31762(15) 0.0378(9) Uani 1 1 d . U . . . C27B C 1.8572(5) -0.6273(2) -0.17913(18) 0.0654(13) Uani 1 1 d . U . . . C28B C 1.9784(5) -0.6049(3) -0.1731(2) 0.119(2) Uani 1 1 d . U . . . H28J H 2.0434 -0.6160 -0.2037 0.179 Uiso 1 1 calc R U . . . H28K H 2.0078 -0.6342 -0.1409 0.179 Uiso 1 1 calc R U . . . H28L H 1.9619 -0.5502 -0.1709 0.179 Uiso 1 1 calc R U . . . C29B C 1.7559(5) -0.6103(2) -0.13097(18) 0.0986(18) Uani 1 1 d . U . . . H29J H 1.7332 -0.5550 -0.1305 0.148 Uiso 1 1 calc R U . . . H29K H 1.7889 -0.6357 -0.0986 0.148 Uiso 1 1 calc R U . . . H29L H 1.6808 -0.6293 -0.1330 0.148 Uiso 1 1 calc R U . . . C30B C 1.8849(5) -0.7132(2) -0.18067(17) 0.0843(16) Uani 1 1 d . U . . . H30J H 1.8071 -0.7291 -0.1829 0.126 Uiso 1 1 calc R U . . . H30K H 1.9169 -0.7405 -0.1485 0.126 Uiso 1 1 calc R U . . . H30L H 1.9485 -0.7250 -0.2116 0.126 Uiso 1 1 calc R U . . . C31B C 1.7050(3) -0.60655(18) -0.35662(15) 0.0426(9) Uani 1 1 d . U . . . C32B C 1.7844(4) -0.5866(2) -0.41071(16) 0.0648(12) Uani 1 1 d . U . . . H32G H 1.7700 -0.5310 -0.4207 0.097 Uiso 1 1 calc R U . . . H32H H 1.7598 -0.6096 -0.4372 0.097 Uiso 1 1 calc R U . . . H32I H 1.8741 -0.6064 -0.4088 0.097 Uiso 1 1 calc R U . . . C33B C 1.7280(4) -0.69395(19) -0.34363(16) 0.0632(12) Uani 1 1 d . U . . . H33G H 1.8174 -0.7140 -0.3412 0.095 Uiso 1 1 calc R U . . . H33H H 1.7053 -0.7150 -0.3716 0.095 Uiso 1 1 calc R U . . . H33I H 1.6760 -0.7087 -0.3098 0.095 Uiso 1 1 calc R U . . . C34B C 1.5648(3) -0.5779(2) -0.36091(16) 0.0616(12) Uani 1 1 d . U . . . H34G H 1.5130 -0.5935 -0.3272 0.092 Uiso 1 1 calc R U . . . H34H H 1.5445 -0.5999 -0.3890 0.092 Uiso 1 1 calc R U . . . H34I H 1.5473 -0.5221 -0.3693 0.092 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.0439(6) 0.0394(6) 0.0421(7) -0.0005(5) -0.0072(5) -0.0106(5) O1 0.0547(16) 0.0360(14) 0.0440(17) 0.0037(12) -0.0068(13) -0.0096(12) O2 0.0683(17) 0.0341(14) 0.0371(17) -0.0036(12) -0.0075(13) -0.0098(12) N1 0.0479(18) 0.0325(17) 0.041(2) -0.0025(15) -0.0005(16) -0.0060(14) N2 0.0429(17) 0.0348(16) 0.0328(19) -0.0021(14) -0.0061(15) -0.0082(13) C1 0.035(2) 0.038(2) 0.042(3) -0.0046(19) -0.0006(18) -0.0077(16) C2 0.047(2) 0.044(2) 0.052(3) -0.014(2) 0.004(2) -0.0062(18) C3 0.049(2) 0.053(2) 0.045(3) -0.013(2) -0.005(2) -0.0113(19) C4 0.042(2) 0.052(2) 0.041(3) -0.005(2) -0.0048(19) -0.0069(18) C5 0.040(2) 0.038(2) 0.041(3) -0.0030(19) -0.0041(19) -0.0083(17) C6 0.033(2) 0.038(2) 0.034(2) -0.0049(18) -0.0036(17) -0.0099(16) C7 0.042(2) 0.038(2) 0.045(3) -0.0023(19) 0.002(2) -0.0057(17) C8 0.039(2) 0.033(2) 0.057(3) 0.000(2) -0.005(2) -0.0018(17) C9 0.035(2) 0.037(2) 0.057(3) 0.0060(19) -0.0011(19) -0.0015(17) C10 0.052(3) 0.033(2) 0.078(3) 0.002(2) 0.004(2) -0.0035(19) C11 0.059(3) 0.038(2) 0.070(3) -0.010(2) 0.004(2) -0.0028(19) C12 0.060(3) 0.039(2) 0.056(3) -0.007(2) 0.003(2) -0.001(2) C13 0.042(2) 0.050(2) 0.054(3) 0.008(2) -0.003(2) -0.0099(18) C14 0.078(3) 0.097(4) 0.070(4) 0.011(3) -0.020(3) -0.026(3) C15 0.057(3) 0.074(3) 0.068(3) 0.003(2) 0.006(2) 0.003(2) C16 0.094(4) 0.058(3) 0.076(4) 0.020(2) 0.007(3) -0.018(2) C17 0.091(3) 0.041(2) 0.084(4) -0.016(2) 0.002(3) -0.008(2) C18 0.112(10) 0.058(8) 0.110(13) -0.015(8) -0.004(9) 0.031(7) C18D 0.109(8) 0.072(11) 0.132(19) -0.050(11) -0.002(9) 0.019(7) C19 0.121(9) 0.067(14) 0.117(15) -0.041(10) 0.000(8) -0.031(8) C19D 0.19(2) 0.065(15) 0.170(17) -0.025(10) 0.029(16) -0.066(15) C20 0.148(15) 0.052(7) 0.082(6) -0.024(5) 0.006(9) 0.005(10) C20D 0.161(17) 0.067(9) 0.114(9) -0.043(7) -0.028(11) -0.021(11) C21 0.045(2) 0.035(2) 0.038(3) -0.0031(18) -0.0019(19) -0.0116(17) C22 0.057(2) 0.041(2) 0.031(2) -0.0004(18) -0.0006(19) -0.0167(18) C23 0.063(3) 0.033(2) 0.046(3) -0.0077(19) -0.006(2) -0.0123(18) C24 0.074(3) 0.037(2) 0.047(3) -0.0148(19) -0.003(2) -0.012(2) C25 0.071(3) 0.044(2) 0.039(3) -0.0090(19) -0.007(2) -0.017(2) C26 0.060(3) 0.034(2) 0.041(3) -0.0029(19) -0.012(2) -0.0171(18) C27 0.073(3) 0.037(2) 0.048(3) -0.0022(19) -0.008(2) -0.012(2) C28 0.095(3) 0.052(3) 0.089(4) 0.006(3) -0.028(3) -0.015(2) C29 0.191(6) 0.036(3) 0.079(4) -0.009(2) -0.009(4) -0.008(3) C30 0.096(4) 0.055(3) 0.106(4) 0.011(3) -0.007(3) -0.038(3) C31 0.097(3) 0.050(3) 0.040(3) -0.010(2) -0.007(2) -0.017(2) C32 0.123(4) 0.087(3) 0.053(3) -0.003(3) -0.030(3) -0.040(3) C33 0.174(5) 0.072(3) 0.040(3) -0.027(3) 0.002(3) -0.012(3) C34 0.099(4) 0.079(3) 0.042(3) -0.006(2) 0.006(3) -0.028(3) P1A 0.0437(5) 0.0347(5) 0.0421(6) -0.0067(5) -0.0026(5) -0.0022(4) O1A 0.0516(15) 0.0336(13) 0.0427(17) -0.0083(12) 0.0006(13) 0.0034(11) O2A 0.0437(5) 0.0347(5) 0.0421(6) -0.0067(5) -0.0026(5) -0.0022(4) N1A 0.0478(18) 0.0336(16) 0.0348(19) -0.0081(14) 0.0013(15) -0.0015(14) N2A 0.0429(17) 0.0316(16) 0.0297(19) -0.0066(14) -0.0028(14) -0.0019(13) C1A 0.034(2) 0.034(2) 0.036(2) -0.0036(18) -0.0033(17) -0.0074(16) C2A 0.048(2) 0.050(2) 0.042(3) -0.007(2) -0.004(2) -0.0120(19) C3A 0.043(2) 0.058(3) 0.041(3) 0.007(2) -0.008(2) -0.0151(19) C4A 0.047(2) 0.042(2) 0.052(3) 0.005(2) -0.006(2) -0.0056(18) C5A 0.047(2) 0.037(2) 0.047(3) -0.0024(19) -0.005(2) -0.0064(17) C6A 0.0308(19) 0.038(2) 0.040(2) -0.0026(18) -0.0046(18) -0.0082(16) C7A 0.044(2) 0.039(2) 0.042(3) -0.0115(19) -0.0035(19) -0.0077(17) C8A 0.043(2) 0.037(2) 0.046(3) -0.0126(19) -0.0010(19) -0.0063(17) C9A 0.045(2) 0.033(2) 0.057(3) -0.0100(19) 0.000(2) -0.0096(17) C10A 0.057(3) 0.041(2) 0.063(3) -0.020(2) 0.004(2) -0.0013(19) C11A 0.064(3) 0.049(2) 0.051(3) -0.020(2) 0.002(2) -0.009(2) C12A 0.058(3) 0.047(2) 0.047(3) -0.016(2) -0.001(2) -0.0109(19) C13A 0.057(3) 0.029(2) 0.063(3) -0.008(2) -0.003(2) -0.0055(18) C14A 0.070(3) 0.053(3) 0.090(4) 0.006(2) 0.000(3) -0.017(2) C15A 0.083(3) 0.045(2) 0.076(4) -0.002(2) -0.027(3) -0.007(2) C16A 0.088(3) 0.036(2) 0.094(4) -0.012(2) -0.003(3) 0.010(2) C17A 0.092(3) 0.071(3) 0.057(3) -0.032(3) 0.005(3) -0.001(3) C18A 0.167(15) 0.131(9) 0.037(6) -0.023(6) 0.011(8) 0.026(9) C19A 0.139(10) 0.134(9) 0.096(9) -0.080(7) -0.008(9) -0.026(8) C20A 0.083(6) 0.156(13) 0.063(7) -0.043(7) 0.022(5) -0.010(6) C21A 0.0322(19) 0.033(2) 0.039(2) -0.0027(18) -0.0025(17) -0.0043(16) C22A 0.041(2) 0.035(2) 0.047(3) -0.0052(19) -0.0047(19) -0.0018(17) C23A 0.046(2) 0.045(2) 0.053(3) -0.018(2) -0.003(2) -0.0065(18) C24A 0.045(2) 0.051(2) 0.042(3) -0.015(2) 0.0002(19) -0.0064(18) C25A 0.039(2) 0.048(2) 0.039(2) -0.0090(19) -0.0018(18) -0.0080(17) C26A 0.036(2) 0.033(2) 0.043(2) -0.0121(18) -0.0022(18) -0.0009(16) C27A 0.063(3) 0.041(2) 0.063(3) -0.020(2) -0.003(2) -0.004(2) C28A 0.149(13) 0.037(4) 0.091(6) -0.015(4) 0.029(6) 0.006(6) C28D 0.093(12) 0.039(6) 0.067(8) -0.017(6) -0.004(8) -0.005(8) C29A 0.075(7) 0.099(8) 0.192(16) -0.110(10) -0.010(8) -0.016(6) C29D 0.114(17) 0.052(9) 0.047(9) -0.024(8) -0.005(10) 0.015(9) C30A 0.049(4) 0.049(5) 0.071(7) -0.025(5) 0.001(4) 0.002(3) C30D 0.057(7) 0.066(13) 0.18(2) -0.074(17) 0.003(11) 0.001(6) C31A 0.048(2) 0.052(2) 0.040(3) -0.004(2) -0.005(2) -0.0075(19) C32A 0.070(3) 0.058(3) 0.060(3) -0.002(2) 0.005(2) -0.019(2) C33A 0.105(4) 0.074(3) 0.045(3) -0.008(2) -0.014(3) -0.011(3) C34A 0.055(3) 0.074(3) 0.070(3) 0.015(2) -0.016(2) -0.004(2) C35 0.19(2) 0.103(8) 0.078(11) -0.058(9) 0.005(13) 0.034(11) C36 0.123(13) 0.144(13) 0.077(11) -0.044(10) 0.052(9) -0.050(11) C37 0.137(12) 0.134(15) 0.064(9) -0.056(10) -0.012(8) -0.014(8) P1B 0.0429(6) 0.0312(5) 0.0398(7) -0.0050(5) -0.0083(5) -0.0061(4) O1B 0.0541(15) 0.0308(13) 0.0391(16) -0.0045(11) -0.0157(12) -0.0010(11) O2B 0.0530(15) 0.0278(13) 0.0385(16) -0.0017(11) -0.0122(12) -0.0040(11) N1B 0.0435(17) 0.0299(16) 0.038(2) -0.0063(14) -0.0107(15) -0.0026(13) N2B 0.0483(18) 0.0280(16) 0.0339(19) -0.0003(14) -0.0147(15) -0.0071(13) C1B 0.040(2) 0.031(2) 0.038(2) -0.0058(18) -0.0056(18) -0.0126(16) C2B 0.054(2) 0.030(2) 0.047(3) -0.0059(19) -0.014(2) -0.0075(17) C3B 0.060(3) 0.040(2) 0.047(3) -0.015(2) -0.013(2) -0.0080(19) C4B 0.057(2) 0.047(2) 0.041(3) -0.010(2) -0.011(2) -0.0139(19) C5B 0.048(2) 0.041(2) 0.043(3) -0.0046(19) -0.012(2) -0.0084(17) C6B 0.039(2) 0.0296(19) 0.041(2) -0.0070(18) -0.0078(18) -0.0102(16) C7B 0.041(2) 0.033(2) 0.035(2) -0.0012(18) -0.0053(18) -0.0075(16) C8B 0.042(2) 0.0257(19) 0.040(3) -0.0007(17) -0.0053(18) -0.0060(16) C9B 0.044(2) 0.038(2) 0.034(2) 0.0005(18) -0.0076(18) -0.0137(17) C10B 0.044(2) 0.039(2) 0.039(3) 0.0051(18) -0.0103(19) -0.0078(17) C11B 0.041(2) 0.0332(19) 0.041(3) 0.0019(18) -0.0068(18) -0.0109(16) C12B 0.048(2) 0.033(2) 0.040(3) -0.0059(18) -0.0074(19) -0.0105(17) C13B 0.053(2) 0.044(2) 0.039(3) -0.0067(19) -0.0124(19) -0.0092(18) C14B 0.069(3) 0.059(3) 0.049(3) -0.016(2) -0.011(2) -0.002(2) C15B 0.086(3) 0.056(3) 0.057(3) -0.006(2) -0.018(2) -0.030(2) C16B 0.072(3) 0.066(3) 0.046(3) -0.006(2) -0.024(2) -0.013(2) C17B 0.048(2) 0.036(2) 0.049(3) 0.0002(19) -0.009(2) -0.0013(17) C18B 0.068(5) 0.069(5) 0.081(6) -0.002(4) 0.012(4) 0.015(4) C18E 0.104(18) 0.061(13) 0.075(10) -0.030(9) -0.036(10) 0.028(12) C19B 0.116(7) 0.044(5) 0.082(6) -0.003(4) -0.040(5) 0.018(5) C19E 0.068(10) 0.041(11) 0.09(2) -0.005(12) -0.041(11) 0.003(7) C20B 0.082(5) 0.035(4) 0.163(11) -0.025(6) -0.020(7) -0.006(3) C20E 0.074(12) 0.029(8) 0.141(19) 0.013(13) 0.040(16) 0.008(8) C21B 0.046(2) 0.031(2) 0.041(3) -0.0027(18) -0.0136(19) -0.0044(16) C22B 0.069(3) 0.038(2) 0.045(3) -0.0020(19) -0.023(2) -0.0075(19) C23B 0.069(3) 0.034(2) 0.045(3) 0.0019(19) -0.020(2) -0.0043(19) C24B 0.057(2) 0.030(2) 0.054(3) -0.0029(19) -0.013(2) -0.0044(18) C25B 0.040(2) 0.033(2) 0.043(3) -0.0052(18) -0.0070(18) -0.0075(16) C26B 0.042(2) 0.0305(19) 0.038(3) 0.0000(18) -0.0095(18) -0.0022(16) C27B 0.106(4) 0.035(2) 0.058(3) 0.005(2) -0.038(3) -0.005(2) C28B 0.141(5) 0.087(4) 0.148(6) 0.036(4) -0.109(4) -0.030(3) C29B 0.171(5) 0.063(3) 0.053(3) -0.002(3) -0.031(3) -0.001(3) C30B 0.132(4) 0.043(2) 0.072(4) 0.009(2) -0.044(3) 0.003(3) C31B 0.047(2) 0.031(2) 0.049(3) -0.0071(18) -0.0064(19) -0.0067(17) C32B 0.079(3) 0.064(3) 0.055(3) -0.022(2) 0.003(2) -0.023(2) C33B 0.088(3) 0.037(2) 0.072(3) -0.015(2) -0.028(3) -0.007(2) C34B 0.055(3) 0.062(3) 0.071(3) -0.020(2) -0.014(2) -0.006(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 O1 1.657(2) . ? P1 O2 1.669(2) . ? P1 N2 1.721(3) . ? P1 N1 1.728(3) . ? P1 H1 1.38(3) . ? O1 C8 1.391(4) . ? O2 C26 1.392(4) . ? N1 C1 1.402(4) . ? N1 C7 1.406(4) . ? N2 C6 1.397(4) . ? N2 C21 1.399(4) . ? C1 C2 1.378(5) . ? C1 C6 1.403(4) . ? C2 C3 1.393(5) . ? C2 H2 0.9500 . ? C3 C4 1.377(4) . ? C3 H3 0.9500 . ? C4 C5 1.391(5) . ? C4 H4 0.9500 . ? C5 C6 1.376(4) . ? C5 H5 0.9500 . ? C7 C8 1.380(5) . ? C7 C12 1.384(5) . ? C8 C9 1.390(5) . ? C9 C10 1.393(5) . ? C9 C13 1.521(5) . ? C10 C11 1.385(5) . ? C10 H10 0.9500 . ? C11 C12 1.397(5) . ? C11 C17 1.529(5) . ? C12 H12 0.9500 . ? C13 C15 1.531(5) . ? C13 C16 1.536(5) . ? C13 C14 1.537(5) . ? C14 H14D 0.9800 . ? C14 H14E 0.9800 . ? C14 H14F 0.9800 . ? C15 H15D 0.9800 . ? C15 H15E 0.9800 . ? C15 H15F 0.9800 . ? C16 H16D 0.9800 . ? C16 H16E 0.9800 . ? C16 H16F 0.9800 . ? C17 C20 1.489(14) . ? C17 C18D 1.497(14) . ? C17 C19 1.50(2) . ? C17 C20D 1.575(17) . ? C17 C18 1.578(13) . ? C17 C19D 1.58(2) . ? C18 H18D 0.9800 . ? C18 H18E 0.9800 . ? C18 H18F 0.9800 . ? C18D H18G 0.9800 . ? C18D H18H 0.9800 . ? C18D H18I 0.9800 . ? C19 H19D 0.9800 . ? C19 H19E 0.9800 . ? C19 H19F 0.9800 . ? C19D H19G 0.9800 . ? C19D H19H 0.9800 . ? C19D H19I 0.9800 . ? C20 H20D 0.9800 . ? C20 H20E 0.9800 . ? C20 H20F 0.9800 . ? C20D H20G 0.9800 . ? C20D H20H 0.9800 . ? C20D H20I 0.9800 . ? C21 C22 1.383(4) . ? C21 C26 1.386(5) . ? C22 C23 1.396(5) . ? C22 H22 0.9500 . ? C23 C24 1.384(5) . ? C23 C27 1.531(5) . ? C24 C25 1.398(5) . ? C24 H24 0.9500 . ? C25 C26 1.387(5) . ? C25 C31 1.527(5) . ? C27 C29 1.521(5) . ? C27 C30 1.522(5) . ? C27 C28 1.523(5) . ? C28 H28G 0.9800 . ? C28 H28H 0.9800 . ? C28 H28I 0.9800 . ? C29 H29G 0.9800 . ? C29 H29H 0.9800 . ? C29 H29I 0.9800 . ? C30 H30G 0.9800 . ? C30 H30H 0.9800 . ? C30 H30I 0.9800 . ? C31 C34 1.529(6) . ? C31 C33 1.539(5) . ? C31 C32 1.542(6) . ? C32 H32D 0.9800 . ? C32 H32E 0.9800 . ? C32 H32F 0.9800 . ? C33 H33D 0.9800 . ? C33 H33E 0.9800 . ? C33 H33F 0.9800 . ? C34 H34D 0.9800 . ? C34 H34E 0.9800 . ? C34 H34F 0.9800 . ? P1A O1A 1.645(2) . ? P1A O2A 1.663(2) . ? P1A N2A 1.722(3) . ? P1A N1A 1.722(3) . ? P1A H1A 1.39(3) . ? O1A C8A 1.379(4) . ? O2A C26A 1.391(4) . ? N1A C1A 1.397(4) . ? N1A C7A 1.400(4) . ? N2A C6A 1.396(4) . ? N2A C21A 1.404(4) . ? C1A C2A 1.383(5) . ? C1A C6A 1.397(5) . ? C2A C3A 1.398(4) . ? C2A H2A 0.9500 . ? C3A C4A 1.372(5) . ? C3A H3A 0.9500 . ? C4A C5A 1.388(5) . ? C4A H4A 0.9500 . ? C5A C6A 1.389(4) . ? C5A H5A 0.9500 . ? C7A C12A 1.375(5) . ? C7A C8A 1.386(5) . ? C8A C9A 1.391(4) . ? C9A C10A 1.388(5) . ? C9A C13A 1.537(5) . ? C10A C11A 1.393(5) . ? C10A H10A 0.9500 . ? C11A C12A 1.398(4) . ? C11A C17A 1.531(5) . ? C12A H12A 0.9500 . ? C13A C15A 1.524(5) . ? C13A C14A 1.532(5) . ? C13A C16A 1.538(4) . ? C14A H14A 0.9800 . ? C14A H14B 0.9800 . ? C14A H14C 0.9800 . ? C15A H15A 0.9800 . ? C15A H15B 0.9800 . ? C15A H15C 0.9800 . ? C16A H16A 0.9800 . ? C16A H16B 0.9800 . ? C16A H16C 0.9800 . ? C17A C18A 1.478(11) . ? C17A C35 1.501(13) . ? C17A C19A 1.536(11) . ? C17A C20A 1.542(10) . ? C17A C36 1.573(14) . ? C17A C37 1.575(15) . ? C18A H18A 0.9800 . ? C18A H18B 0.9800 . ? C18A H18C 0.9800 . ? C19A H19A 0.9800 . ? C19A H19B 0.9800 . ? C19A H19C 0.9800 . ? C20A H20A 0.9800 . ? C20A H20B 0.9800 . ? C20A H20C 0.9800 . ? C21A C26A 1.382(4) . ? C21A C22A 1.384(4) . ? C22A C23A 1.389(5) . ? C22A H22A 0.9500 . ? C23A C24A 1.399(5) . ? C23A C27A 1.526(5) . ? C24A C25A 1.403(4) . ? C24A H24A 0.9500 . ? C25A C26A 1.377(5) . ? C25A C31A 1.531(5) . ? C27A C30D 1.405(17) . ? C27A C29A 1.464(15) . ? C27A C28A 1.523(10) . ? C27A C29D 1.60(2) . ? C27A C30A 1.605(10) . ? C27A C28D 1.620(16) . ? C28A H28A 0.9800 . ? C28A H28B 0.9800 . ? C28A H28C 0.9800 . ? C28D H28D 0.9800 . ? C28D H28E 0.9800 . ? C28D H28F 0.9800 . ? C29A H29A 0.9800 . ? C29A H29B 0.9800 . ? C29A H29C 0.9800 . ? C29D H29D 0.9800 . ? C29D H29E 0.9800 . ? C29D H29F 0.9800 . ? C30A H30A 0.9800 . ? C30A H30B 0.9800 . ? C30A H30C 0.9800 . ? C30D H30D 0.9800 . ? C30D H30E 0.9800 . ? C30D H30F 0.9800 . ? C31A C32A 1.526(5) . ? C31A C33A 1.531(5) . ? C31A C34A 1.536(5) . ? C32A H32A 0.9800 . ? C32A H32B 0.9800 . ? C32A H32C 0.9800 . ? C33A H33A 0.9800 . ? C33A H33B 0.9800 . ? C33A H33C 0.9800 . ? C34A H34A 0.9800 . ? C34A H34B 0.9800 . ? C34A H34C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? P1B O2B 1.661(2) . ? P1B O1B 1.670(2) . ? P1B N1B 1.729(3) . ? P1B N2B 1.734(3) . ? P1B H1B 1.37(3) . ? O1B C8B 1.381(3) . ? O2B C26B 1.391(4) . ? N1B C7B 1.402(4) . ? N1B C1B 1.409(4) . ? N2B C21B 1.399(4) . ? N2B C6B 1.402(4) . ? C1B C2B 1.374(4) . ? C1B C6B 1.402(4) . ? C2B C3B 1.391(5) . ? C2B H2B 0.9500 . ? C3B C4B 1.371(4) . ? C3B H3B 0.9500 . ? C4B C5B 1.382(5) . ? C4B H4B 0.9500 . ? C5B C6B 1.378(5) . ? C5B H5B 0.9500 . ? C7B C8B 1.378(5) . ? C7B C12B 1.383(4) . ? C8B C9B 1.389(5) . ? C9B C10B 1.407(4) . ? C9B C13B 1.520(5) . ? C10B C11B 1.390(5) . ? C10B H10B 0.9500 . ? C11B C12B 1.402(4) . ? C11B C17B 1.535(4) . ? C12B H12B 0.9500 . ? C13B C14B 1.530(5) . ? C13B C15B 1.539(5) . ? C13B C16B 1.543(5) . ? C14B H14G 0.9800 . ? C14B H14H 0.9800 . ? C14B H14I 0.9800 . ? C15B H15G 0.9800 . ? C15B H15H 0.9800 . ? C15B H15I 0.9800 . ? C16B H16G 0.9800 . ? C16B H16H 0.9800 . ? C16B H16I 0.9800 . ? C17B C20B 1.463(8) . ? C17B C19E 1.495(18) . ? C17B C18B 1.507(7) . ? C17B C19B 1.557(8) . ? C17B C18E 1.599(19) . ? C17B C20E 1.60(2) . ? C18B H18J 0.9800 . ? C18B H18K 0.9800 . ? C18B H18L 0.9800 . ? C18E H18M 0.9800 . ? C18E H18N 0.9800 . ? C18E H18O 0.9800 . ? C19B H19J 0.9800 . ? C19B H19K 0.9800 . ? C19B H19L 0.9800 . ? C19E H19M 0.9800 . ? C19E H19N 0.9800 . ? C19E H19O 0.9800 . ? C20B H20J 0.9800 . ? C20B H20K 0.9800 . ? C20B H20L 0.9800 . ? C20E H20M 0.9800 . ? C20E H20N 0.9800 . ? C20E H20O 0.9800 . ? C21B C26B 1.382(5) . ? C21B C22B 1.383(5) . ? C22B C23B 1.387(4) . ? C22B H22B 0.9500 . ? C23B C24B 1.385(5) . ? C23B C27B 1.537(5) . ? C24B C25B 1.412(5) . ? C24B H24B 0.9500 . ? C25B C26B 1.387(4) . ? C25B C31B 1.532(5) . ? C27B C28B 1.525(6) . ? C27B C30B 1.528(5) . ? C27B C29B 1.534(6) . ? C28B H28J 0.9800 . ? C28B H28K 0.9800 . ? C28B H28L 0.9800 . ? C29B H29J 0.9800 . ? C29B H29K 0.9800 . ? C29B H29L 0.9800 . ? C30B H30J 0.9800 . ? C30B H30K 0.9800 . ? C30B H30L 0.9800 . ? C31B C34B 1.533(5) . ? C31B C33B 1.534(4) . ? C31B C32B 1.535(5) . ? C32B H32G 0.9800 . ? C32B H32H 0.9800 . ? C32B H32I 0.9800 . ? C33B H33G 0.9800 . ? C33B H33H 0.9800 . ? C33B H33I 0.9800 . ? C34B H34G 0.9800 . ? C34B H34H 0.9800 . ? C34B H34I 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 P1 O2 84.84(12) . . ? O1 P1 N2 154.56(14) . . ? O2 P1 N2 89.18(13) . . ? O1 P1 N1 89.22(14) . . ? O2 P1 N1 158.06(14) . . ? N2 P1 N1 87.17(14) . . ? O1 P1 H1 99.1(11) . . ? O2 P1 H1 97.1(11) . . ? N2 P1 H1 106.2(11) . . ? N1 P1 H1 104.7(11) . . ? C8 O1 P1 115.1(2) . . ? C26 O2 P1 113.7(2) . . ? C1 N1 C7 127.4(3) . . ? C1 N1 P1 115.9(2) . . ? C7 N1 P1 113.6(3) . . ? C6 N2 C21 129.4(3) . . ? C6 N2 P1 116.1(2) . . ? C21 N2 P1 113.8(2) . . ? C2 C1 N1 129.6(3) . . ? C2 C1 C6 120.1(3) . . ? N1 C1 C6 110.2(3) . . ? C1 C2 C3 119.0(3) . . ? C1 C2 H2 120.5 . . ? C3 C2 H2 120.5 . . ? C4 C3 C2 121.0(4) . . ? C4 C3 H3 119.5 . . ? C2 C3 H3 119.5 . . ? C3 C4 C5 119.9(3) . . ? C3 C4 H4 120.0 . . ? C5 C4 H4 120.0 . . ? C6 C5 C4 119.6(3) . . ? C6 C5 H5 120.2 . . ? C4 C5 H5 120.2 . . ? C5 C6 N2 129.1(3) . . ? C5 C6 C1 120.3(3) . . ? N2 C6 C1 110.5(3) . . ? C8 C7 C12 119.5(3) . . ? C8 C7 N1 109.6(3) . . ? C12 C7 N1 130.9(4) . . ? C7 C8 O1 112.2(3) . . ? C7 C8 C9 124.5(4) . . ? O1 C8 C9 123.2(4) . . ? C8 C9 C10 113.6(4) . . ? C8 C9 C13 123.3(4) . . ? C10 C9 C13 123.1(3) . . ? C11 C10 C9 124.6(4) . . ? C11 C10 H10 117.7 . . ? C9 C10 H10 117.7 . . ? C10 C11 C12 118.8(4) . . ? C10 C11 C17 120.2(4) . . ? C12 C11 C17 120.9(4) . . ? C7 C12 C11 118.9(4) . . ? C7 C12 H12 120.6 . . ? C11 C12 H12 120.6 . . ? C9 C13 C15 109.1(3) . . ? C9 C13 C16 112.9(3) . . ? C15 C13 C16 107.9(3) . . ? C9 C13 C14 111.4(3) . . ? C15 C13 C14 108.2(3) . . ? C16 C13 C14 107.2(3) . . ? C13 C14 H14D 109.5 . . ? C13 C14 H14E 109.5 . . ? H14D C14 H14E 109.5 . . ? C13 C14 H14F 109.5 . . ? H14D C14 H14F 109.5 . . ? H14E C14 H14F 109.5 . . ? C13 C15 H15D 109.5 . . ? C13 C15 H15E 109.5 . . ? H15D C15 H15E 109.5 . . ? C13 C15 H15F 109.5 . . ? H15D C15 H15F 109.5 . . ? H15E C15 H15F 109.5 . . ? C13 C16 H16D 109.5 . . ? C13 C16 H16E 109.5 . . ? H16D C16 H16E 109.5 . . ? C13 C16 H16F 109.5 . . ? H16D C16 H16F 109.5 . . ? H16E C16 H16F 109.5 . . ? C20 C17 C19 112.8(12) . . ? C20 C17 C11 113.1(7) . . ? C18D C17 C11 109.8(7) . . ? C19 C17 C11 109.1(10) . . ? C18D C17 C20D 108.4(8) . . ? C11 C17 C20D 110.1(7) . . ? C20 C17 C18 107.8(7) . . ? C19 C17 C18 104.4(9) . . ? C11 C17 C18 109.2(7) . . ? C18D C17 C19D 111.3(10) . . ? C11 C17 C19D 112.6(12) . . ? C20D C17 C19D 104.6(13) . . ? C17 C18 H18D 109.5 . . ? C17 C18 H18E 109.5 . . ? H18D C18 H18E 109.5 . . ? C17 C18 H18F 109.5 . . ? H18D C18 H18F 109.5 . . ? H18E C18 H18F 109.5 . . ? C17 C18D H18G 109.5 . . ? C17 C18D H18H 109.5 . . ? H18G C18D H18H 109.5 . . ? C17 C18D H18I 109.5 . . ? H18G C18D H18I 109.5 . . ? H18H C18D H18I 109.5 . . ? C17 C19 H19D 109.5 . . ? C17 C19 H19E 109.5 . . ? H19D C19 H19E 109.5 . . ? C17 C19 H19F 109.5 . . ? H19D C19 H19F 109.5 . . ? H19E C19 H19F 109.5 . . ? C17 C19D H19G 109.5 . . ? C17 C19D H19H 109.5 . . ? H19G C19D H19H 109.5 . . ? C17 C19D H19I 109.5 . . ? H19G C19D H19I 109.5 . . ? H19H C19D H19I 109.5 . . ? C17 C20 H20D 109.5 . . ? C17 C20 H20E 109.5 . . ? H20D C20 H20E 109.5 . . ? C17 C20 H20F 109.5 . . ? H20D C20 H20F 109.5 . . ? H20E C20 H20F 109.5 . . ? C17 C20D H20G 109.5 . . ? C17 C20D H20H 109.5 . . ? H20G C20D H20H 109.5 . . ? C17 C20D H20I 109.5 . . ? H20G C20D H20I 109.5 . . ? H20H C20D H20I 109.5 . . ? C22 C21 C26 119.4(3) . . ? C22 C21 N2 131.6(3) . . ? C26 C21 N2 108.9(3) . . ? C21 C22 C23 119.7(4) . . ? C21 C22 H22 120.1 . . ? C23 C22 H22 120.1 . . ? C24 C23 C22 118.1(3) . . ? C24 C23 C27 122.4(3) . . ? C22 C23 C27 119.5(4) . . ? C23 C24 C25 124.7(3) . . ? C23 C24 H24 117.6 . . ? C25 C24 H24 117.6 . . ? C26 C25 C24 114.1(4) . . ? C26 C25 C31 122.1(3) . . ? C24 C25 C31 123.8(3) . . ? C21 C26 C25 123.9(3) . . ? C21 C26 O2 112.8(3) . . ? C25 C26 O2 123.3(4) . . ? C29 C27 C30 107.5(4) . . ? C29 C27 C28 108.5(4) . . ? C30 C27 C28 109.3(4) . . ? C29 C27 C23 112.7(3) . . ? C30 C27 C23 109.7(3) . . ? C28 C27 C23 109.1(3) . . ? C27 C28 H28G 109.5 . . ? C27 C28 H28H 109.5 . . ? H28G C28 H28H 109.5 . . ? C27 C28 H28I 109.5 . . ? H28G C28 H28I 109.5 . . ? H28H C28 H28I 109.5 . . ? C27 C29 H29G 109.5 . . ? C27 C29 H29H 109.5 . . ? H29G C29 H29H 109.5 . . ? C27 C29 H29I 109.5 . . ? H29G C29 H29I 109.5 . . ? H29H C29 H29I 109.5 . . ? C27 C30 H30G 109.5 . . ? C27 C30 H30H 109.5 . . ? H30G C30 H30H 109.5 . . ? C27 C30 H30I 109.5 . . ? H30G C30 H30I 109.5 . . ? H30H C30 H30I 109.5 . . ? C25 C31 C34 109.8(4) . . ? C25 C31 C33 111.5(3) . . ? C34 C31 C33 107.6(4) . . ? C25 C31 C32 108.9(4) . . ? C34 C31 C32 110.5(4) . . ? C33 C31 C32 108.5(4) . . ? C31 C32 H32D 109.5 . . ? C31 C32 H32E 109.5 . . ? H32D C32 H32E 109.5 . . ? C31 C32 H32F 109.5 . . ? H32D C32 H32F 109.5 . . ? H32E C32 H32F 109.5 . . ? C31 C33 H33D 109.5 . . ? C31 C33 H33E 109.5 . . ? H33D C33 H33E 109.5 . . ? C31 C33 H33F 109.5 . . ? H33D C33 H33F 109.5 . . ? H33E C33 H33F 109.5 . . ? C31 C34 H34D 109.5 . . ? C31 C34 H34E 109.5 . . ? H34D C34 H34E 109.5 . . ? C31 C34 H34F 109.5 . . ? H34D C34 H34F 109.5 . . ? H34E C34 H34F 109.5 . . ? O1A P1A O2A 85.49(11) . . ? O1A P1A N2A 154.17(14) . . ? O2A P1A N2A 89.14(13) . . ? O1A P1A N1A 89.19(12) . . ? O2A P1A N1A 158.23(14) . . ? N2A P1A N1A 86.50(13) . . ? O1A P1A H1A 100.4(10) . . ? O2A P1A H1A 97.2(11) . . ? N2A P1A H1A 105.4(10) . . ? N1A P1A H1A 104.6(11) . . ? C8A O1A P1A 115.3(2) . . ? C26A O2A P1A 113.2(2) . . ? C1A N1A C7A 129.2(3) . . ? C1A N1A P1A 115.4(2) . . ? C7A N1A P1A 114.2(2) . . ? C6A N2A C21A 131.0(3) . . ? C6A N2A P1A 115.7(2) . . ? C21A N2A P1A 112.8(2) . . ? C2A C1A C6A 120.8(3) . . ? C2A C1A N1A 128.9(3) . . ? C6A C1A N1A 110.3(3) . . ? C1A C2A C3A 118.7(4) . . ? C1A C2A H2A 120.6 . . ? C3A C2A H2A 120.6 . . ? C4A C3A C2A 120.3(4) . . ? C4A C3A H3A 119.8 . . ? C2A C3A H3A 119.8 . . ? C3A C4A C5A 121.3(3) . . ? C3A C4A H4A 119.3 . . ? C5A C4A H4A 119.3 . . ? C4A C5A C6A 118.8(3) . . ? C4A C5A H5A 120.6 . . ? C6A C5A H5A 120.6 . . ? C5A C6A N2A 130.0(3) . . ? C5A C6A C1A 120.0(3) . . ? N2A C6A C1A 110.0(3) . . ? C12A C7A C8A 121.2(3) . . ? C12A C7A N1A 130.2(3) . . ? C8A C7A N1A 108.5(3) . . ? O1A C8A C7A 112.7(3) . . ? O1A C8A C9A 124.4(3) . . ? C7A C8A C9A 122.7(4) . . ? C10A C9A C8A 114.5(3) . . ? C10A C9A C13A 124.3(3) . . ? C8A C9A C13A 121.2(3) . . ? C9A C10A C11A 124.6(3) . . ? C9A C10A H10A 117.7 . . ? C11A C10A H10A 117.7 . . ? C10A C11A C12A 118.6(4) . . ? C10A C11A C17A 121.8(3) . . ? C12A C11A C17A 119.6(4) . . ? C7A C12A C11A 118.4(4) . . ? C7A C12A H12A 120.8 . . ? C11A C12A H12A 120.8 . . ? C15A C13A C14A 110.4(4) . . ? C15A C13A C9A 110.1(3) . . ? C14A C13A C9A 110.0(3) . . ? C15A C13A C16A 107.5(3) . . ? C14A C13A C16A 107.6(3) . . ? C9A C13A C16A 111.2(3) . . ? C13A C14A H14A 109.5 . . ? C13A C14A H14B 109.5 . . ? H14A C14A H14B 109.5 . . ? C13A C14A H14C 109.5 . . ? H14A C14A H14C 109.5 . . ? H14B C14A H14C 109.5 . . ? C13A C15A H15A 109.5 . . ? C13A C15A H15B 109.5 . . ? H15A C15A H15B 109.5 . . ? C13A C15A H15C 109.5 . . ? H15A C15A H15C 109.5 . . ? H15B C15A H15C 109.5 . . ? C13A C16A H16A 109.5 . . ? C13A C16A H16B 109.5 . . ? H16A C16A H16B 109.5 . . ? C13A C16A H16C 109.5 . . ? H16A C16A H16C 109.5 . . ? H16B C16A H16C 109.5 . . ? C18A C17A C11A 115.2(5) . . ? C35 C17A C11A 114.2(7) . . ? C18A C17A C19A 108.7(8) . . ? C11A C17A C19A 107.7(6) . . ? C18A C17A C20A 110.4(8) . . ? C11A C17A C20A 109.1(5) . . ? C19A C17A C20A 105.3(7) . . ? C35 C17A C36 111.4(10) . . ? C11A C17A C36 107.3(6) . . ? C35 C17A C37 108.7(10) . . ? C11A C17A C37 107.5(6) . . ? C36 C17A C37 107.6(10) . . ? C17A C18A H18A 109.5 . . ? C17A C18A H18B 109.5 . . ? H18A C18A H18B 109.5 . . ? C17A C18A H18C 109.5 . . ? H18A C18A H18C 109.5 . . ? H18B C18A H18C 109.5 . . ? C17A C19A H19A 109.5 . . ? C17A C19A H19B 109.5 . . ? H19A C19A H19B 109.5 . . ? C17A C19A H19C 109.5 . . ? H19A C19A H19C 109.5 . . ? H19B C19A H19C 109.5 . . ? C17A C20A H20A 109.5 . . ? C17A C20A H20B 109.5 . . ? H20A C20A H20B 109.5 . . ? C17A C20A H20C 109.5 . . ? H20A C20A H20C 109.5 . . ? H20B C20A H20C 109.5 . . ? C26A C21A C22A 119.7(3) . . ? C26A C21A N2A 109.2(3) . . ? C22A C21A N2A 131.1(3) . . ? C21A C22A C23A 119.3(3) . . ? C21A C22A H22A 120.3 . . ? C23A C22A H22A 120.3 . . ? C22A C23A C24A 118.8(3) . . ? C22A C23A C27A 120.8(3) . . ? C24A C23A C27A 120.3(4) . . ? C23A C24A C25A 123.4(4) . . ? C23A C24A H24A 118.3 . . ? C25A C24A H24A 118.3 . . ? C26A C25A C24A 114.7(3) . . ? C26A C25A C31A 122.5(3) . . ? C24A C25A C31A 122.9(4) . . ? C25A C26A C21A 124.1(3) . . ? C25A C26A O2A 123.5(3) . . ? C21A C26A O2A 112.4(3) . . ? C29A C27A C28A 114.8(8) . . ? C30D C27A C23A 110.6(8) . . ? C29A C27A C23A 108.7(7) . . ? C28A C27A C23A 113.0(5) . . ? C30D C27A C29D 114.9(13) . . ? C23A C27A C29D 115.1(9) . . ? C29A C27A C30A 107.9(7) . . ? C28A C27A C30A 104.1(6) . . ? C23A C27A C30A 107.9(5) . . ? C30D C27A C28D 109.8(11) . . ? C23A C27A C28D 106.9(6) . . ? C29D C27A C28D 98.5(11) . . ? C27A C28A H28A 109.5 . . ? C27A C28A H28B 109.5 . . ? H28A C28A H28B 109.5 . . ? C27A C28A H28C 109.5 . . ? H28A C28A H28C 109.5 . . ? H28B C28A H28C 109.5 . . ? C27A C28D H28D 109.5 . . ? C27A C28D H28E 109.5 . . ? H28D C28D H28E 109.5 . . ? C27A C28D H28F 109.5 . . ? H28D C28D H28F 109.5 . . ? H28E C28D H28F 109.5 . . ? C27A C29A H29A 109.5 . . ? C27A C29A H29B 109.5 . . ? H29A C29A H29B 109.5 . . ? C27A C29A H29C 109.5 . . ? H29A C29A H29C 109.5 . . ? H29B C29A H29C 109.5 . . ? C27A C29D H29D 109.5 . . ? C27A C29D H29E 109.5 . . ? H29D C29D H29E 109.5 . . ? C27A C29D H29F 109.5 . . ? H29D C29D H29F 109.5 . . ? H29E C29D H29F 109.5 . . ? C27A C30A H30A 109.5 . . ? C27A C30A H30B 109.5 . . ? H30A C30A H30B 109.5 . . ? C27A C30A H30C 109.5 . . ? H30A C30A H30C 109.5 . . ? H30B C30A H30C 109.5 . . ? C27A C30D H30D 109.5 . . ? C27A C30D H30E 109.5 . . ? H30D C30D H30E 109.5 . . ? C27A C30D H30F 109.5 . . ? H30D C30D H30F 109.5 . . ? H30E C30D H30F 109.5 . . ? C32A C31A C33A 108.4(3) . . ? C32A C31A C25A 110.2(3) . . ? C33A C31A C25A 112.1(3) . . ? C32A C31A C34A 109.7(3) . . ? C33A C31A C34A 108.2(3) . . ? C25A C31A C34A 108.2(3) . . ? C31A C32A H32A 109.5 . . ? C31A C32A H32B 109.5 . . ? H32A C32A H32B 109.5 . . ? C31A C32A H32C 109.5 . . ? H32A C32A H32C 109.5 . . ? H32B C32A H32C 109.5 . . ? C31A C33A H33A 109.5 . . ? C31A C33A H33B 109.5 . . ? H33A C33A H33B 109.5 . . ? C31A C33A H33C 109.5 . . ? H33A C33A H33C 109.5 . . ? H33B C33A H33C 109.5 . . ? C31A C34A H34A 109.5 . . ? C31A C34A H34B 109.5 . . ? H34A C34A H34B 109.5 . . ? C31A C34A H34C 109.5 . . ? H34A C34A H34C 109.5 . . ? H34B C34A H34C 109.5 . . ? C17A C35 H35A 109.5 . . ? C17A C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? C17A C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C17A C36 H36A 109.5 . . ? C17A C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C17A C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C17A C37 H37A 109.5 . . ? C17A C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C17A C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? O2B P1B O1B 85.66(12) . . ? O2B P1B N1B 150.86(13) . . ? O1B P1B N1B 88.49(12) . . ? O2B P1B N2B 89.30(12) . . ? O1B P1B N2B 161.03(14) . . ? N1B P1B N2B 87.05(14) . . ? O2B P1B H1B 102.1(10) . . ? O1B P1B H1B 99.0(10) . . ? N1B P1B H1B 107.0(10) . . ? N2B P1B H1B 99.9(10) . . ? C8B O1B P1B 115.3(2) . . ? C26B O2B P1B 113.6(2) . . ? C7B N1B C1B 129.1(3) . . ? C7B N1B P1B 114.3(2) . . ? C1B N1B P1B 115.3(2) . . ? C21B N2B C6B 129.6(3) . . ? C21B N2B P1B 112.7(2) . . ? C6B N2B P1B 116.5(2) . . ? C2B C1B C6B 119.3(3) . . ? C2B C1B N1B 129.3(3) . . ? C6B C1B N1B 111.4(3) . . ? C1B C2B C3B 119.8(3) . . ? C1B C2B H2B 120.1 . . ? C3B C2B H2B 120.1 . . ? C4B C3B C2B 119.9(3) . . ? C4B C3B H3B 120.0 . . ? C2B C3B H3B 120.0 . . ? C3B C4B C5B 121.5(4) . . ? C3B C4B H4B 119.3 . . ? C5B C4B H4B 119.3 . . ? C6B C5B C4B 118.3(3) . . ? C6B C5B H5B 120.8 . . ? C4B C5B H5B 120.8 . . ? C5B C6B C1B 121.1(3) . . ? C5B C6B N2B 129.3(3) . . ? C1B C6B N2B 109.5(3) . . ? C8B C7B C12B 120.2(3) . . ? C8B C7B N1B 109.2(3) . . ? C12B C7B N1B 130.5(3) . . ? C7B C8B O1B 112.6(3) . . ? C7B C8B C9B 123.7(3) . . ? O1B C8B C9B 123.7(3) . . ? C8B C9B C10B 114.6(3) . . ? C8B C9B C13B 122.2(3) . . ? C10B C9B C13B 123.2(3) . . ? C11B C10B C9B 123.5(3) . . ? C11B C10B H10B 118.3 . . ? C9B C10B H10B 118.3 . . ? C10B C11B C12B 118.9(3) . . ? C10B C11B C17B 122.0(3) . . ? C12B C11B C17B 119.0(3) . . ? C7B C12B C11B 119.0(3) . . ? C7B C12B H12B 120.5 . . ? C11B C12B H12B 120.5 . . ? C9B C13B C14B 109.7(3) . . ? C9B C13B C15B 109.2(3) . . ? C14B C13B C15B 110.1(3) . . ? C9B C13B C16B 112.3(3) . . ? C14B C13B C16B 107.4(3) . . ? C15B C13B C16B 108.1(3) . . ? C13B C14B H14G 109.5 . . ? C13B C14B H14H 109.5 . . ? H14G C14B H14H 109.5 . . ? C13B C14B H14I 109.5 . . ? H14G C14B H14I 109.5 . . ? H14H C14B H14I 109.5 . . ? C13B C15B H15G 109.5 . . ? C13B C15B H15H 109.5 . . ? H15G C15B H15H 109.5 . . ? C13B C15B H15I 109.5 . . ? H15G C15B H15I 109.5 . . ? H15H C15B H15I 109.5 . . ? C13B C16B H16G 109.5 . . ? C13B C16B H16H 109.5 . . ? H16G C16B H16H 109.5 . . ? C13B C16B H16I 109.5 . . ? H16G C16B H16I 109.5 . . ? H16H C16B H16I 109.5 . . ? C20B C17B C18B 112.3(5) . . ? C20B C17B C11B 110.4(4) . . ? C19E C17B C11B 116.0(8) . . ? C18B C17B C11B 106.9(4) . . ? C20B C17B C19B 109.9(5) . . ? C18B C17B C19B 106.0(5) . . ? C11B C17B C19B 111.2(4) . . ? C19E C17B C18E 104.8(11) . . ? C11B C17B C18E 115.3(6) . . ? C19E C17B C20E 107.9(12) . . ? C11B C17B C20E 107.9(8) . . ? C18E C17B C20E 104.1(13) . . ? C17B C18B H18J 109.5 . . ? C17B C18B H18K 109.5 . . ? H18J C18B H18K 109.5 . . ? C17B C18B H18L 109.5 . . ? H18J C18B H18L 109.5 . . ? H18K C18B H18L 109.5 . . ? C17B C18E H18M 109.5 . . ? C17B C18E H18N 109.5 . . ? H18M C18E H18N 109.5 . . ? C17B C18E H18O 109.5 . . ? H18M C18E H18O 109.5 . . ? H18N C18E H18O 109.5 . . ? C17B C19B H19J 109.5 . . ? C17B C19B H19K 109.5 . . ? H19J C19B H19K 109.5 . . ? C17B C19B H19L 109.5 . . ? H19J C19B H19L 109.5 . . ? H19K C19B H19L 109.5 . . ? C17B C19E H19M 109.5 . . ? C17B C19E H19N 109.5 . . ? H19M C19E H19N 109.5 . . ? C17B C19E H19O 109.5 . . ? H19M C19E H19O 109.5 . . ? H19N C19E H19O 109.5 . . ? C17B C20B H20J 109.5 . . ? C17B C20B H20K 109.5 . . ? H20J C20B H20K 109.5 . . ? C17B C20B H20L 109.5 . . ? H20J C20B H20L 109.5 . . ? H20K C20B H20L 109.5 . . ? C17B C20E H20M 109.5 . . ? C17B C20E H20N 109.5 . . ? H20M C20E H20N 109.5 . . ? C17B C20E H20O 109.5 . . ? H20M C20E H20O 109.5 . . ? H20N C20E H20O 109.5 . . ? C26B C21B C22B 120.3(3) . . ? C26B C21B N2B 109.4(3) . . ? C22B C21B N2B 130.2(3) . . ? C21B C22B C23B 119.2(4) . . ? C21B C22B H22B 120.4 . . ? C23B C22B H22B 120.4 . . ? C24B C23B C22B 118.8(3) . . ? C24B C23B C27B 123.3(3) . . ? C22B C23B C27B 117.9(4) . . ? C23B C24B C25B 123.9(3) . . ? C23B C24B H24B 118.1 . . ? C25B C24B H24B 118.1 . . ? C26B C25B C24B 114.3(3) . . ? C26B C25B C31B 122.7(3) . . ? C24B C25B C31B 123.0(3) . . ? C21B C26B C25B 123.3(3) . . ? C21B C26B O2B 112.8(3) . . ? C25B C26B O2B 123.9(3) . . ? C28B C27B C30B 108.2(4) . . ? C28B C27B C29B 109.3(4) . . ? C30B C27B C29B 108.4(4) . . ? C28B C27B C23B 109.2(4) . . ? C30B C27B C23B 112.7(4) . . ? C29B C27B C23B 108.9(3) . . ? C27B C28B H28J 109.5 . . ? C27B C28B H28K 109.5 . . ? H28J C28B H28K 109.5 . . ? C27B C28B H28L 109.5 . . ? H28J C28B H28L 109.5 . . ? H28K C28B H28L 109.5 . . ? C27B C29B H29J 109.5 . . ? C27B C29B H29K 109.5 . . ? H29J C29B H29K 109.5 . . ? C27B C29B H29L 109.5 . . ? H29J C29B H29L 109.5 . . ? H29K C29B H29L 109.5 . . ? C27B C30B H30J 109.5 . . ? C27B C30B H30K 109.5 . . ? H30J C30B H30K 109.5 . . ? C27B C30B H30L 109.5 . . ? H30J C30B H30L 109.5 . . ? H30K C30B H30L 109.5 . . ? C25B C31B C34B 109.6(3) . . ? C25B C31B C33B 112.3(3) . . ? C34B C31B C33B 107.6(3) . . ? C25B C31B C32B 111.0(3) . . ? C34B C31B C32B 108.8(3) . . ? C33B C31B C32B 107.4(3) . . ? C31B C32B H32G 109.5 . . ? C31B C32B H32H 109.5 . . ? H32G C32B H32H 109.5 . . ? C31B C32B H32I 109.5 . . ? H32G C32B H32I 109.5 . . ? H32H C32B H32I 109.5 . . ? C31B C33B H33G 109.5 . . ? C31B C33B H33H 109.5 . . ? H33G C33B H33H 109.5 . . ? C31B C33B H33I 109.5 . . ? H33G C33B H33I 109.5 . . ? H33H C33B H33I 109.5 . . ? C31B C34B H34G 109.5 . . ? C31B C34B H34H 109.5 . . ? H34G C34B H34H 109.5 . . ? C31B C34B H34I 109.5 . . ? H34G C34B H34I 109.5 . . ? H34H C34B H34I 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O2 P1 O1 C8 163.8(2) . . . . ? N2 P1 O1 C8 86.7(4) . . . . ? N1 P1 O1 C8 5.0(2) . . . . ? O1 P1 O2 C26 -166.8(2) . . . . ? N2 P1 O2 C26 -11.5(2) . . . . ? N1 P1 O2 C26 -91.9(4) . . . . ? O1 P1 N1 C1 156.7(2) . . . . ? O2 P1 N1 C1 82.6(4) . . . . ? N2 P1 N1 C1 1.9(3) . . . . ? O1 P1 N1 C7 -4.8(2) . . . . ? O2 P1 N1 C7 -78.9(4) . . . . ? N2 P1 N1 C7 -159.6(2) . . . . ? O1 P1 N2 C6 -83.5(4) . . . . ? O2 P1 N2 C6 -159.7(2) . . . . ? N1 P1 N2 C6 -1.3(2) . . . . ? O1 P1 N2 C21 88.0(4) . . . . ? O2 P1 N2 C21 11.8(2) . . . . ? N1 P1 N2 C21 170.2(2) . . . . ? C7 N1 C1 C2 -22.3(6) . . . . ? P1 N1 C1 C2 179.2(3) . . . . ? C7 N1 C1 C6 156.5(3) . . . . ? P1 N1 C1 C6 -2.0(4) . . . . ? N1 C1 C2 C3 176.1(3) . . . . ? C6 C1 C2 C3 -2.5(5) . . . . ? C1 C2 C3 C4 0.6(5) . . . . ? C2 C3 C4 C5 1.0(5) . . . . ? C3 C4 C5 C6 -0.6(5) . . . . ? C4 C5 C6 N2 -177.6(3) . . . . ? C4 C5 C6 C1 -1.3(5) . . . . ? C21 N2 C6 C5 7.1(6) . . . . ? P1 N2 C6 C5 177.0(3) . . . . ? C21 N2 C6 C1 -169.4(3) . . . . ? P1 N2 C6 C1 0.5(4) . . . . ? C2 C1 C6 C5 2.9(5) . . . . ? N1 C1 C6 C5 -176.0(3) . . . . ? C2 C1 C6 N2 179.8(3) . . . . ? N1 C1 C6 N2 0.9(4) . . . . ? C1 N1 C7 C8 -155.5(3) . . . . ? P1 N1 C7 C8 3.4(4) . . . . ? C1 N1 C7 C12 23.1(6) . . . . ? P1 N1 C7 C12 -178.0(3) . . . . ? C12 C7 C8 O1 -178.5(3) . . . . ? N1 C7 C8 O1 0.3(4) . . . . ? C12 C7 C8 C9 -2.0(6) . . . . ? N1 C7 C8 C9 176.8(3) . . . . ? P1 O1 C8 C7 -4.1(4) . . . . ? P1 O1 C8 C9 179.4(3) . . . . ? C7 C8 C9 C10 1.7(5) . . . . ? O1 C8 C9 C10 177.7(3) . . . . ? C7 C8 C9 C13 -177.0(3) . . . . ? O1 C8 C9 C13 -0.9(5) . . . . ? C8 C9 C10 C11 -1.7(6) . . . . ? C13 C9 C10 C11 176.9(4) . . . . ? C9 C10 C11 C12 2.1(6) . . . . ? C9 C10 C11 C17 179.0(4) . . . . ? C8 C7 C12 C11 2.2(6) . . . . ? N1 C7 C12 C11 -176.3(4) . . . . ? C10 C11 C12 C7 -2.2(6) . . . . ? C17 C11 C12 C7 -179.0(4) . . . . ? C8 C9 C13 C15 61.4(5) . . . . ? C10 C9 C13 C15 -117.2(4) . . . . ? C8 C9 C13 C16 -178.7(3) . . . . ? C10 C9 C13 C16 2.8(5) . . . . ? C8 C9 C13 C14 -58.0(4) . . . . ? C10 C9 C13 C14 123.5(4) . . . . ? C10 C11 C17 C20 -176.7(13) . . . . ? C12 C11 C17 C20 0.1(14) . . . . ? C10 C11 C17 C18D -95.9(14) . . . . ? C12 C11 C17 C18D 80.9(14) . . . . ? C10 C11 C17 C19 56.9(11) . . . . ? C12 C11 C17 C19 -126.3(11) . . . . ? C10 C11 C17 C20D 144.9(13) . . . . ? C12 C11 C17 C20D -38.3(13) . . . . ? C10 C11 C17 C18 -56.7(12) . . . . ? C12 C11 C17 C18 120.1(11) . . . . ? C10 C11 C17 C19D 28.7(16) . . . . ? C12 C11 C17 C19D -154.5(15) . . . . ? C6 N2 C21 C22 -22.0(6) . . . . ? P1 N2 C21 C22 167.9(3) . . . . ? C6 N2 C21 C26 161.2(3) . . . . ? P1 N2 C21 C26 -8.9(4) . . . . ? C26 C21 C22 C23 -2.7(5) . . . . ? N2 C21 C22 C23 -179.3(4) . . . . ? C21 C22 C23 C24 0.5(6) . . . . ? C21 C22 C23 C27 178.5(3) . . . . ? C22 C23 C24 C25 0.5(6) . . . . ? C27 C23 C24 C25 -177.5(4) . . . . ? C23 C24 C25 C26 0.9(6) . . . . ? C23 C24 C25 C31 179.2(4) . . . . ? C22 C21 C26 C25 4.4(6) . . . . ? N2 C21 C26 C25 -178.4(3) . . . . ? C22 C21 C26 O2 -177.1(3) . . . . ? N2 C21 C26 O2 0.2(4) . . . . ? C24 C25 C26 C21 -3.3(6) . . . . ? C31 C25 C26 C21 178.3(4) . . . . ? C24 C25 C26 O2 178.3(3) . . . . ? C31 C25 C26 O2 -0.1(6) . . . . ? P1 O2 C26 C21 8.9(4) . . . . ? P1 O2 C26 C25 -172.6(3) . . . . ? C24 C23 C27 C29 3.2(6) . . . . ? C22 C23 C27 C29 -174.7(4) . . . . ? C24 C23 C27 C30 123.0(4) . . . . ? C22 C23 C27 C30 -54.9(5) . . . . ? C24 C23 C27 C28 -117.3(4) . . . . ? C22 C23 C27 C28 64.8(5) . . . . ? C26 C25 C31 C34 -57.5(5) . . . . ? C24 C25 C31 C34 124.3(4) . . . . ? C26 C25 C31 C33 -176.7(4) . . . . ? C24 C25 C31 C33 5.1(6) . . . . ? C26 C25 C31 C32 63.6(5) . . . . ? C24 C25 C31 C32 -114.6(4) . . . . ? O2A P1A O1A C8A -161.1(2) . . . . ? N2A P1A O1A C8A -82.5(4) . . . . ? N1A P1A O1A C8A -2.2(3) . . . . ? O1A P1A O2A C26A 171.3(2) . . . . ? N2A P1A O2A C26A 16.6(2) . . . . ? N1A P1A O2A C26A 94.9(4) . . . . ? O1A P1A N1A C1A -167.9(2) . . . . ? O2A P1A N1A C1A -92.2(4) . . . . ? N2A P1A N1A C1A -13.4(2) . . . . ? O1A P1A N1A C7A 1.0(3) . . . . ? O2A P1A N1A C7A 76.6(4) . . . . ? N2A P1A N1A C7A 155.5(3) . . . . ? O1A P1A N2A C6A 93.7(4) . . . . ? O2A P1A N2A C6A 171.5(2) . . . . ? N1A P1A N2A C6A 12.8(2) . . . . ? O1A P1A N2A C21A -93.1(4) . . . . ? O2A P1A N2A C21A -15.3(2) . . . . ? N1A P1A N2A C21A -174.0(2) . . . . ? C7A N1A C1A C2A 27.7(6) . . . . ? P1A N1A C1A C2A -165.5(3) . . . . ? C7A N1A C1A C6A -155.9(3) . . . . ? P1A N1A C1A C6A 10.9(4) . . . . ? C6A C1A C2A C3A 2.9(5) . . . . ? N1A C1A C2A C3A 179.0(3) . . . . ? C1A C2A C3A C4A -0.7(5) . . . . ? C2A C3A C4A C5A -0.4(6) . . . . ? C3A C4A C5A C6A -0.6(6) . . . . ? C4A C5A C6A N2A -176.9(3) . . . . ? C4A C5A C6A C1A 2.8(5) . . . . ? C21A N2A C6A C5A -1.3(6) . . . . ? P1A N2A C6A C5A 170.4(3) . . . . ? C21A N2A C6A C1A 179.0(3) . . . . ? P1A N2A C6A C1A -9.3(4) . . . . ? C2A C1A C6A C5A -4.0(5) . . . . ? N1A C1A C6A C5A 179.3(3) . . . . ? C2A C1A C6A N2A 175.7(3) . . . . ? N1A C1A C6A N2A -1.0(4) . . . . ? C1A N1A C7A C12A -8.4(6) . . . . ? P1A N1A C7A C12A -175.4(3) . . . . ? C1A N1A C7A C8A 167.5(3) . . . . ? P1A N1A C7A C8A 0.5(4) . . . . ? P1A O1A C8A C7A 3.0(4) . . . . ? P1A O1A C8A C9A 179.6(3) . . . . ? C12A C7A C8A O1A 174.2(3) . . . . ? N1A C7A C8A O1A -2.1(4) . . . . ? C12A C7A C8A C9A -2.4(6) . . . . ? N1A C7A C8A C9A -178.7(3) . . . . ? O1A C8A C9A C10A -174.8(3) . . . . ? C7A C8A C9A C10A 1.4(5) . . . . ? O1A C8A C9A C13A 6.3(6) . . . . ? C7A C8A C9A C13A -177.5(3) . . . . ? C8A C9A C10A C11A 0.7(6) . . . . ? C13A C9A C10A C11A 179.5(4) . . . . ? C9A C10A C11A C12A -1.8(6) . . . . ? C9A C10A C11A C17A 175.6(4) . . . . ? C8A C7A C12A C11A 1.2(6) . . . . ? N1A C7A C12A C11A 176.6(4) . . . . ? C10A C11A C12A C7A 0.8(6) . . . . ? C17A C11A C12A C7A -176.7(4) . . . . ? C10A C9A C13A C15A 118.4(4) . . . . ? C8A C9A C13A C15A -62.9(5) . . . . ? C10A C9A C13A C14A -119.7(4) . . . . ? C8A C9A C13A C14A 59.0(5) . . . . ? C10A C9A C13A C16A -0.6(5) . . . . ? C8A C9A C13A C16A 178.1(3) . . . . ? C10A C11A C17A C18A -174.9(9) . . . . ? C12A C11A C17A C18A 2.6(10) . . . . ? C10A C11A C17A C35 11.3(12) . . . . ? C12A C11A C17A C35 -171.3(11) . . . . ? C10A C11A C17A C19A 63.7(8) . . . . ? C12A C11A C17A C19A -118.9(7) . . . . ? C10A C11A C17A C20A -50.1(8) . . . . ? C12A C11A C17A C20A 127.4(7) . . . . ? C10A C11A C17A C36 -112.7(9) . . . . ? C12A C11A C17A C36 64.8(9) . . . . ? C10A C11A C17A C37 131.9(8) . . . . ? C12A C11A C17A C37 -50.7(9) . . . . ? C6A N2A C21A C26A -178.1(3) . . . . ? P1A N2A C21A C26A 10.1(3) . . . . ? C6A N2A C21A C22A 1.9(6) . . . . ? P1A N2A C21A C22A -169.9(3) . . . . ? C26A C21A C22A C23A -1.5(5) . . . . ? N2A C21A C22A C23A 178.4(3) . . . . ? C21A C22A C23A C24A -0.2(5) . . . . ? C21A C22A C23A C27A -177.6(3) . . . . ? C22A C23A C24A C25A 1.9(6) . . . . ? C27A C23A C24A C25A 179.2(3) . . . . ? C23A C24A C25A C26A -1.5(5) . . . . ? C23A C24A C25A C31A 177.9(3) . . . . ? C24A C25A C26A C21A -0.3(5) . . . . ? C31A C25A C26A C21A -179.8(3) . . . . ? C24A C25A C26A O2A 179.3(3) . . . . ? C31A C25A C26A O2A -0.2(5) . . . . ? C22A C21A C26A C25A 1.9(5) . . . . ? N2A C21A C26A C25A -178.1(3) . . . . ? C22A C21A C26A O2A -177.8(3) . . . . ? N2A C21A C26A O2A 2.3(4) . . . . ? P1A O2A C26A C25A 166.1(3) . . . . ? P1A O2A C26A C21A -14.2(4) . . . . ? C22A C23A C27A C30D 76.2(16) . . . . ? C24A C23A C27A C30D -101.1(16) . . . . ? C22A C23A C27A C29A -129.6(9) . . . . ? C24A C23A C27A C29A 53.1(9) . . . . ? C22A C23A C27A C28A -0.8(10) . . . . ? C24A C23A C27A C28A -178.1(9) . . . . ? C22A C23A C27A C29D -151.5(11) . . . . ? C24A C23A C27A C29D 31.2(12) . . . . ? C22A C23A C27A C30A 113.7(6) . . . . ? C24A C23A C27A C30A -63.6(6) . . . . ? C22A C23A C27A C28D -43.3(10) . . . . ? C24A C23A C27A C28D 139.4(9) . . . . ? C26A C25A C31A C32A -55.9(5) . . . . ? C24A C25A C31A C32A 124.7(4) . . . . ? C26A C25A C31A C33A -176.7(4) . . . . ? C24A C25A C31A C33A 3.9(5) . . . . ? C26A C25A C31A C34A 64.1(5) . . . . ? C24A C25A C31A C34A -115.4(4) . . . . ? O2B P1B O1B C8B 153.9(2) . . . . ? N1B P1B O1B C8B 2.5(2) . . . . ? N2B P1B O1B C8B 78.9(4) . . . . ? O1B P1B O2B C26B -174.7(2) . . . . ? N1B P1B O2B C26B -95.6(3) . . . . ? N2B P1B O2B C26B -13.0(2) . . . . ? O2B P1B N1B C7B -79.9(4) . . . . ? O1B P1B N1B C7B -1.6(2) . . . . ? N2B P1B N1B C7B -163.1(2) . . . . ? O2B P1B N1B C1B 88.1(4) . . . . ? O1B P1B N1B C1B 166.4(2) . . . . ? N2B P1B N1B C1B 4.8(3) . . . . ? O2B P1B N2B C21B 13.5(2) . . . . ? O1B P1B N2B C21B 87.9(4) . . . . ? N1B P1B N2B C21B 164.6(2) . . . . ? O2B P1B N2B C6B -155.2(2) . . . . ? O1B P1B N2B C6B -80.8(5) . . . . ? N1B P1B N2B C6B -4.1(3) . . . . ? C7B N1B C1B C2B -17.9(6) . . . . ? P1B N1B C1B C2B 176.3(3) . . . . ? C7B N1B C1B C6B 161.3(3) . . . . ? P1B N1B C1B C6B -4.5(4) . . . . ? C6B C1B C2B C3B -1.0(5) . . . . ? N1B C1B C2B C3B 178.2(3) . . . . ? C1B C2B C3B C4B -0.4(6) . . . . ? C2B C3B C4B C5B 1.5(6) . . . . ? C3B C4B C5B C6B -1.2(6) . . . . ? C4B C5B C6B C1B -0.3(5) . . . . ? C4B C5B C6B N2B -179.2(3) . . . . ? C2B C1B C6B C5B 1.4(5) . . . . ? N1B C1B C6B C5B -178.0(3) . . . . ? C2B C1B C6B N2B -179.5(3) . . . . ? N1B C1B C6B N2B 1.2(4) . . . . ? C21B N2B C6B C5B 15.1(6) . . . . ? P1B N2B C6B C5B -178.4(3) . . . . ? C21B N2B C6B C1B -164.0(3) . . . . ? P1B N2B C6B C1B 2.5(4) . . . . ? C1B N1B C7B C8B -165.6(3) . . . . ? P1B N1B C7B C8B 0.2(4) . . . . ? C1B N1B C7B C12B 10.8(6) . . . . ? P1B N1B C7B C12B 176.7(3) . . . . ? C12B C7B C8B O1B -175.3(3) . . . . ? N1B C7B C8B O1B 1.6(4) . . . . ? C12B C7B C8B C9B 3.3(6) . . . . ? N1B C7B C8B C9B -179.9(3) . . . . ? P1B O1B C8B C7B -2.9(4) . . . . ? P1B O1B C8B C9B 178.6(3) . . . . ? C7B C8B C9B C10B -2.7(5) . . . . ? O1B C8B C9B C10B 175.6(3) . . . . ? C7B C8B C9B C13B 176.5(3) . . . . ? O1B C8B C9B C13B -5.1(5) . . . . ? C8B C9B C10B C11B -0.2(5) . . . . ? C13B C9B C10B C11B -179.4(3) . . . . ? C9B C10B C11B C12B 2.5(5) . . . . ? C9B C10B C11B C17B -176.8(3) . . . . ? C8B C7B C12B C11B -0.7(5) . . . . ? N1B C7B C12B C11B -176.8(3) . . . . ? C10B C11B C12B C7B -2.0(5) . . . . ? C17B C11B C12B C7B 177.3(3) . . . . ? C8B C9B C13B C14B -56.6(5) . . . . ? C10B C9B C13B C14B 122.6(4) . . . . ? C8B C9B C13B C15B 64.1(4) . . . . ? C10B C9B C13B C15B -116.7(4) . . . . ? C8B C9B C13B C16B -176.0(3) . . . . ? C10B C9B C13B C16B 3.1(5) . . . . ? C10B C11B C17B C20B -122.4(7) . . . . ? C12B C11B C17B C20B 58.3(7) . . . . ? C10B C11B C17B C19E 42.8(14) . . . . ? C12B C11B C17B C19E -136.5(14) . . . . ? C10B C11B C17B C18B 115.2(6) . . . . ? C12B C11B C17B C18B -64.1(6) . . . . ? C10B C11B C17B C19B -0.1(7) . . . . ? C12B C11B C17B C19B -179.4(6) . . . . ? C10B C11B C17B C18E 165.9(14) . . . . ? C12B C11B C17B C18E -13.4(15) . . . . ? C10B C11B C17B C20E -78.3(16) . . . . ? C12B C11B C17B C20E 102.4(16) . . . . ? C6B N2B C21B C26B 156.4(3) . . . . ? P1B N2B C21B C26B -10.4(4) . . . . ? C6B N2B C21B C22B -23.9(6) . . . . ? P1B N2B C21B C22B 169.3(3) . . . . ? C26B C21B C22B C23B -0.7(6) . . . . ? N2B C21B C22B C23B 179.6(3) . . . . ? C21B C22B C23B C24B -1.6(6) . . . . ? C21B C22B C23B C27B -179.6(4) . . . . ? C22B C23B C24B C25B 1.0(6) . . . . ? C27B C23B C24B C25B 178.9(4) . . . . ? C23B C24B C25B C26B 1.9(5) . . . . ? C23B C24B C25B C31B -177.6(3) . . . . ? C22B C21B C26B C25B 3.9(5) . . . . ? N2B C21B C26B C25B -176.3(3) . . . . ? C22B C21B C26B O2B -178.9(3) . . . . ? N2B C21B C26B O2B 0.8(4) . . . . ? C24B C25B C26B C21B -4.3(5) . . . . ? C31B C25B C26B C21B 175.2(3) . . . . ? C24B C25B C26B O2B 178.8(3) . . . . ? C31B C25B C26B O2B -1.6(5) . . . . ? P1B O2B C26B C21B 9.6(4) . . . . ? P1B O2B C26B C25B -173.3(3) . . . . ? C24B C23B C27B C28B 126.4(5) . . . . ? C22B C23B C27B C28B -55.6(5) . . . . ? C24B C23B C27B C30B 6.1(6) . . . . ? C22B C23B C27B C30B -176.0(4) . . . . ? C24B C23B C27B C29B -114.2(4) . . . . ? C22B C23B C27B C29B 63.7(5) . . . . ? C26B C25B C31B C34B -60.5(4) . . . . ? C24B C25B C31B C34B 119.0(4) . . . . ? C26B C25B C31B C33B 179.9(3) . . . . ? C24B C25B C31B C33B -0.6(5) . . . . ? C26B C25B C31B C32B 59.7(4) . . . . ? C24B C25B C31B C32B -120.8(4) . . . . ? _refine_diff_density_max 0.225 _refine_diff_density_min -0.313 _refine_diff_density_rms 0.046 _shelx_res_file ; romanta63b.res created by SHELXL-2014/7 TITL mo_RomanTA63b_0ma_a.res in P-1 REM Old TITL mo_RomanTA63b_0ma in P-1 REM SHELXT solution in P-1 REM R1 0.247, Rweak 0.025, Alpha 0.079, Orientation as input REM Formula found by SHELXT: C99 N8 O6 P3 CELL 0.71073 11.0161 18.175 26.1106 79.325 78.548 76.878 ZERR 6 0.0011 0.0021 0.0025 0.004 0.003 0.002 LATT 1 SFAC C H N O P UNIT 204 270 12 12 6 DELU SIMU EADP O2A P1A L.S. 10 PLAN 34 SIZE 0.18 0.21 0.24 TEMP -73 CONF LIST 6 MORE -1 ABIN BOND $H fmap 2 acta OMIT 0 0 1 OMIT 0 1 1 OMIT 0 -1 1 OMIT 0 4 4 OMIT 3 -5 22 OMIT 2 2 6 OMIT 1 -1 3 OMIT -1 1 0 OMIT 0 -1 3 OMIT 0 -3 5 OMIT 3 -3 3 OMIT 0 -4 2 OMIT 4 -3 7 REM REM REM WGHT 0.067500 FVAR 0.26201 0.43218 0.26582 0.63705 0.50967 P1 5 1.365236 -0.369152 -0.121514 11.00000 0.04390 0.03937 = 0.04208 -0.00046 -0.00716 -0.01063 H1 2 1.483299 -0.367072 -0.112266 11.00000 0.03920 O1 4 1.332591 -0.440449 -0.074880 11.00000 0.05468 0.03600 = 0.04397 0.00372 -0.00681 -0.00961 O2 4 1.281726 -0.313236 -0.077562 11.00000 0.06828 0.03405 = 0.03713 -0.00357 -0.00746 -0.00984 N1 3 1.393840 -0.429881 -0.168115 11.00000 0.04793 0.03248 = 0.04107 -0.00251 -0.00047 -0.00602 N2 3 1.331164 -0.295191 -0.171430 11.00000 0.04292 0.03477 = 0.03281 -0.00214 -0.00608 -0.00821 C1 1 1.381704 -0.394756 -0.219866 11.00000 0.03486 0.03786 = 0.04212 -0.00464 -0.00059 -0.00769 C2 1 1.399397 -0.427022 -0.265215 11.00000 0.04730 0.04376 = 0.05157 -0.01424 0.00370 -0.00618 AFIX 43 H2 2 1.428462 -0.480503 -0.264587 11.00000 -1.20000 AFIX 0 C3 1 1.374020 -0.380035 -0.312021 11.00000 0.04876 0.05293 = 0.04480 -0.01287 -0.00487 -0.01135 AFIX 43 H3 2 1.385192 -0.401922 -0.343385 11.00000 -1.20000 AFIX 0 C4 1 1.332999 -0.302363 -0.313497 11.00000 0.04189 0.05229 = 0.04100 -0.00516 -0.00485 -0.00687 AFIX 43 H4 2 1.314836 -0.271152 -0.345579 11.00000 -1.20000 AFIX 0 C5 1 1.318181 -0.269642 -0.267955 11.00000 0.03972 0.03840 = 0.04140 -0.00302 -0.00415 -0.00827 AFIX 43 H5 2 1.290662 -0.216015 -0.268882 11.00000 -1.20000 AFIX 0 C6 1 1.343602 -0.315379 -0.221571 11.00000 0.03280 0.03847 = 0.03413 -0.00490 -0.00359 -0.00989 C7 1 1.387311 -0.505854 -0.146176 11.00000 0.04207 0.03754 = 0.04546 -0.00232 0.00236 -0.00574 C8 1 1.352018 -0.510820 -0.092075 11.00000 0.03864 0.03287 = 0.05667 -0.00020 -0.00523 -0.00178 C9 1 1.330778 -0.577168 -0.058468 11.00000 0.03516 0.03655 = 0.05663 0.00597 -0.00106 -0.00151 C10 1 1.351814 -0.640550 -0.084321 11.00000 0.05196 0.03288 = 0.07791 0.00190 0.00353 -0.00349 AFIX 43 H10 2 1.341197 -0.688027 -0.063398 11.00000 -1.20000 AFIX 0 C11 1 1.387126 -0.639186 -0.138399 11.00000 0.05850 0.03763 = 0.06954 -0.00991 0.00410 -0.00278 C12 1 1.407392 -0.570630 -0.169855 11.00000 0.06031 0.03850 = 0.05638 -0.00722 0.00348 -0.00059 AFIX 43 H12 2 1.434510 -0.568517 -0.206888 11.00000 -1.20000 AFIX 0 C13 1 1.285901 -0.580049 0.000725 11.00000 0.04193 0.04972 = 0.05381 0.00831 -0.00318 -0.00994 C14 1 1.377395 -0.553090 0.027221 11.00000 0.07807 0.09653 = 0.06981 0.01143 -0.02005 -0.02638 AFIX 137 H14D 2 1.461187 -0.585991 0.021319 11.00000 -1.50000 H14E 2 1.346216 -0.555833 0.065249 11.00000 -1.50000 H14F 2 1.383132 -0.500254 0.011991 11.00000 -1.50000 AFIX 0 C15 1 1.156419 -0.527260 0.010288 11.00000 0.05711 0.07358 = 0.06844 0.00314 0.00649 0.00255 AFIX 137 H15D 2 1.163617 -0.474755 -0.005313 11.00000 -1.50000 H15E 2 1.126376 -0.529430 0.048367 11.00000 -1.50000 H15F 2 1.096374 -0.543802 -0.006070 11.00000 -1.50000 AFIX 0 C16 1 1.272730 -0.660547 0.028893 11.00000 0.09371 0.05799 = 0.07649 0.01995 0.00717 -0.01849 AFIX 137 H16D 2 1.213117 -0.679102 0.013555 11.00000 -1.50000 H16E 2 1.241344 -0.658860 0.066587 11.00000 -1.50000 H16F 2 1.355323 -0.695054 0.024513 11.00000 -1.50000 AFIX 0 C17 1 1.409925 -0.712652 -0.162514 11.00000 0.09124 0.04128 = 0.08432 -0.01634 0.00178 -0.00753 PART 1 C18 1 1.513966 -0.774436 -0.136161 51.00000 0.11215 0.05809 = 0.11003 -0.01531 -0.00381 0.03068 AFIX 137 H18D 2 1.534056 -0.820076 -0.153581 51.00000 -1.50000 H18E 2 1.482084 -0.788058 -0.098575 51.00000 -1.50000 H18F 2 1.590365 -0.753540 -0.139964 51.00000 -1.50000 AFIX 0 PART 2 C18D 1 1.547889 -0.747486 -0.169917 -51.00000 0.10922 0.07160 = 0.13211 -0.04983 -0.00157 0.01874 AFIX 137 H18G 2 1.561574 -0.795732 -0.183851 -51.00000 -1.50000 H18H 2 1.577720 -0.757192 -0.135883 -51.00000 -1.50000 H18I 2 1.594712 -0.712343 -0.194866 -51.00000 -1.50000 AFIX 0 PART 1 C19 1 1.293076 -0.746353 -0.147239 51.00000 0.12139 0.06656 = 0.11731 -0.04092 -0.00009 -0.03118 AFIX 137 H19D 2 1.308925 -0.795105 -0.160721 51.00000 -1.50000 H19E 2 1.223333 -0.711079 -0.162368 51.00000 -1.50000 H19F 2 1.270711 -0.754871 -0.108659 51.00000 -1.50000 AFIX 0 PART 2 C19D 1 1.328584 -0.771676 -0.128840 -51.00000 0.18860 0.06490 = 0.16975 -0.02485 0.02876 -0.06556 AFIX 137 H19G 2 1.328413 -0.810861 -0.150031 -51.00000 -1.50000 H19H 2 1.241706 -0.744871 -0.118522 -51.00000 -1.50000 H19I 2 1.365226 -0.795872 -0.097099 -51.00000 -1.50000 AFIX 0 PART 1 C20 1 1.454211 -0.701748 -0.220613 51.00000 0.14835 0.05159 = 0.08155 -0.02387 0.00638 0.00486 AFIX 137 H20D 2 1.532628 -0.682014 -0.228261 51.00000 -1.50000 H20E 2 1.389461 -0.665263 -0.238140 51.00000 -1.50000 H20F 2 1.469691 -0.750790 -0.233674 51.00000 -1.50000 AFIX 0 PART 2 C20D 1 1.365874 -0.694555 -0.218105 -51.00000 0.16056 0.06660 = 0.11376 -0.04347 -0.02776 -0.02130 AFIX 137 H20G 2 1.416205 -0.660399 -0.242138 -51.00000 -1.50000 H20H 2 1.276384 -0.669799 -0.214195 -51.00000 -1.50000 H20I 2 1.377627 -0.742209 -0.232569 -51.00000 -1.50000 AFIX 0 PART 0 C21 1 1.278015 -0.224926 -0.153757 11.00000 0.04531 0.03457 = 0.03764 -0.00307 -0.00194 -0.01165 C22 1 1.256869 -0.151303 -0.180579 11.00000 0.05737 0.04138 = 0.03079 -0.00041 -0.00061 -0.01666 AFIX 43 H22 2 1.279241 -0.142274 -0.217931 11.00000 -1.20000 AFIX 0 C23 1 1.202508 -0.090273 -0.152560 11.00000 0.06329 0.03296 = 0.04636 -0.00768 -0.00567 -0.01228 C24 1 1.172294 -0.106106 -0.098140 11.00000 0.07432 0.03745 = 0.04713 -0.01484 -0.00315 -0.01172 AFIX 43 H24 2 1.134756 -0.064340 -0.079361 11.00000 -1.20000 AFIX 0 C25 1 1.193042 -0.179127 -0.068829 11.00000 0.07120 0.04392 = 0.03865 -0.00900 -0.00665 -0.01743 C26 1 1.249782 -0.236768 -0.099068 11.00000 0.05972 0.03435 = 0.04147 -0.00287 -0.01217 -0.01714 C27 1 1.182414 -0.008709 -0.182325 11.00000 0.07305 0.03705 = 0.04839 -0.00225 -0.00798 -0.01201 C28 1 1.087089 -0.000323 -0.219045 11.00000 0.09545 0.05234 = 0.08901 0.00581 -0.02796 -0.01470 AFIX 137 H28G 2 1.116204 -0.039359 -0.242484 11.00000 -1.50000 H28H 2 1.078776 0.050504 -0.240243 11.00000 -1.50000 H28I 2 1.004932 -0.006716 -0.198043 11.00000 -1.50000 AFIX 0 C29 1 1.133745 0.051165 -0.145497 11.00000 0.19130 0.03580 = 0.07935 -0.00875 -0.00890 -0.00758 AFIX 137 H29G 2 1.052799 0.042698 -0.124274 11.00000 -1.50000 H29H 2 1.122030 0.102176 -0.166407 11.00000 -1.50000 H29I 2 1.195053 0.047193 -0.122088 11.00000 -1.50000 AFIX 0 C30 1 1.307011 0.007370 -0.214835 11.00000 0.09563 0.05469 = 0.10632 0.01145 -0.00749 -0.03774 AFIX 137 H30G 2 1.368904 0.001382 -0.191348 11.00000 -1.50000 H30H 2 1.293818 0.059703 -0.233693 11.00000 -1.50000 H30I 2 1.338521 -0.028623 -0.240393 11.00000 -1.50000 AFIX 0 C31 1 1.160360 -0.195080 -0.008727 11.00000 0.09745 0.05025 = 0.04010 -0.01001 -0.00711 -0.01739 C32 1 1.283534 -0.226405 0.014382 11.00000 0.12321 0.08726 = 0.05343 -0.00324 -0.02997 -0.03963 AFIX 137 H32D 2 1.323684 -0.275964 0.003050 11.00000 -1.50000 H32E 2 1.264140 -0.232619 0.053041 11.00000 -1.50000 H32F 2 1.341080 -0.190545 0.001746 11.00000 -1.50000 AFIX 0 C33 1 1.091496 -0.122081 0.014692 11.00000 0.17403 0.07171 = 0.03954 -0.02713 0.00220 -0.01158 AFIX 137 H33D 2 1.146645 -0.084614 0.006215 11.00000 -1.50000 H33E 2 1.069992 -0.134495 0.053133 11.00000 -1.50000 H33F 2 1.014006 -0.100655 -0.000359 11.00000 -1.50000 AFIX 0 C34 1 1.072924 -0.252770 0.007117 11.00000 0.09901 0.07855 = 0.04190 -0.00637 0.00600 -0.02812 AFIX 137 H34D 2 0.996241 -0.232703 -0.008714 11.00000 -1.50000 H34E 2 1.050102 -0.261536 0.045674 11.00000 -1.50000 H34F 2 1.116390 -0.301045 -0.005454 11.00000 -1.50000 AFIX 0 P1A 5 1.021683 0.193697 0.289667 11.00000 0.04371 0.03473 = 0.04214 -0.00674 -0.00264 -0.00222 H1A 2 0.904222 0.172757 0.304176 11.00000 0.03229 O1A 4 1.115394 0.109058 0.294335 11.00000 0.05165 0.03365 = 0.04273 -0.00825 0.00058 0.00341 O2A 4 1.046066 0.195461 0.350230 11.00000 0.04371 0.03473 = 0.04214 -0.00674 -0.00264 -0.00222 N1A 3 1.053009 0.199278 0.221938 11.00000 0.04775 0.03359 = 0.03481 -0.00810 0.00129 -0.00153 N2A 3 0.989857 0.292021 0.279394 11.00000 0.04291 0.03158 = 0.02967 -0.00661 -0.00279 -0.00193 C1A 1 1.013327 0.271242 0.193865 11.00000 0.03425 0.03432 = 0.03615 -0.00360 -0.00332 -0.00741 C2A 1 1.001119 0.290639 0.141108 11.00000 0.04805 0.05012 = 0.04238 -0.00706 -0.00440 -0.01196 AFIX 43 H2A 2 1.022119 0.252701 0.118474 11.00000 -1.20000 AFIX 0 C3A 1 0.957269 0.367169 0.121707 11.00000 0.04260 0.05848 = 0.04148 0.00683 -0.00796 -0.01508 AFIX 43 H3A 2 0.949260 0.381581 0.085469 11.00000 -1.20000 AFIX 0 C4A 1 0.925762 0.421534 0.154741 11.00000 0.04715 0.04207 = 0.05235 0.00491 -0.00559 -0.00558 AFIX 43 H4A 2 0.896647 0.473337 0.140924 11.00000 -1.20000 AFIX 0 C5A 1 0.935573 0.402364 0.207932 11.00000 0.04741 0.03699 = 0.04664 -0.00235 -0.00460 -0.00645 AFIX 43 H5A 2 0.914270 0.440554 0.230379 11.00000 -1.20000 AFIX 0 C6A 1 0.977118 0.326304 0.227770 11.00000 0.03077 0.03753 = 0.03985 -0.00264 -0.00457 -0.00820 C7A 1 1.134270 0.134884 0.203680 11.00000 0.04437 0.03865 = 0.04199 -0.01153 -0.00351 -0.00771 C8A 1 1.167040 0.082503 0.246980 11.00000 0.04310 0.03748 = 0.04573 -0.01259 -0.00100 -0.00633 C9A 1 1.249095 0.012716 0.242179 11.00000 0.04487 0.03302 = 0.05680 -0.01002 -0.00001 -0.00964 C10A 1 1.297690 0.000576 0.190495 11.00000 0.05733 0.04072 = 0.06273 -0.02003 0.00366 -0.00127 AFIX 43 H10A 2 1.353495 -0.046550 0.185111 11.00000 -1.20000 AFIX 0 C11A 1 1.270361 0.052664 0.145951 11.00000 0.06430 0.04875 = 0.05055 -0.02044 0.00187 -0.00896 C12A 1 1.185592 0.121397 0.153004 11.00000 0.05788 0.04695 = 0.04727 -0.01650 -0.00101 -0.01092 AFIX 43 H12A 2 1.163959 0.157914 0.123497 11.00000 -1.20000 AFIX 0 C13A 1 1.278900 -0.045248 0.291113 11.00000 0.05695 0.02892 = 0.06271 -0.00826 -0.00308 -0.00547 C14A 1 1.156965 -0.067559 0.323255 11.00000 0.06974 0.05313 = 0.09024 0.00639 0.00016 -0.01686 AFIX 137 H14A 2 1.100484 -0.022393 0.336083 11.00000 -1.50000 H14B 2 1.177222 -0.106417 0.353401 11.00000 -1.50000 H14C 2 1.115185 -0.088140 0.300844 11.00000 -1.50000 AFIX 0 C15A 1 1.344256 -0.011628 0.324915 11.00000 0.08289 0.04548 = 0.07627 -0.00164 -0.02698 -0.00722 AFIX 137 H15A 2 1.422400 0.001919 0.303956 11.00000 -1.50000 H15B 2 1.364316 -0.049388 0.355624 11.00000 -1.50000 H15C 2 1.288078 0.034203 0.336900 11.00000 -1.50000 AFIX 0 C16A 1 1.368210 -0.118663 0.275358 11.00000 0.08796 0.03607 = 0.09366 -0.01166 -0.00348 0.01021 AFIX 137 H16A 2 1.327806 -0.142518 0.254330 11.00000 -1.50000 H16B 2 1.386693 -0.154170 0.307262 11.00000 -1.50000 H16C 2 1.447056 -0.106094 0.254441 11.00000 -1.50000 AFIX 0 C17A 1 1.334548 0.037914 0.090137 11.00000 0.09207 0.07130 = 0.05731 -0.03197 0.00485 -0.00063 PART 1 C18A 1 1.303793 0.101519 0.047513 -21.00000 0.16745 0.13062 = 0.03714 -0.02275 0.01143 0.02553 AFIX 137 H18A 2 1.212873 0.111889 0.046698 -21.00000 -1.50000 H18B 2 1.350497 0.087535 0.013510 -21.00000 -1.50000 H18C 2 1.327618 0.147301 0.054072 -21.00000 -1.50000 AFIX 0 C19A 1 1.295353 -0.033002 0.079463 -21.00000 0.13893 0.13415 = 0.09594 -0.08034 -0.00766 -0.02608 AFIX 137 H19A 2 1.309312 -0.074477 0.108846 -21.00000 -1.50000 H19B 2 1.346052 -0.049076 0.046640 -21.00000 -1.50000 H19C 2 1.205685 -0.020704 0.076094 -21.00000 -1.50000 AFIX 0 C20A 1 1.478666 0.015292 0.088673 -21.00000 0.08312 0.15565 = 0.06339 -0.04290 0.02227 -0.01004 AFIX 137 H20A 2 1.510676 0.059204 0.093529 -21.00000 -1.50000 H20B 2 1.519327 -0.000755 0.054497 -21.00000 -1.50000 H20C 2 1.497614 -0.026953 0.117063 -21.00000 -1.50000 AFIX 0 PART 0 C21A 1 0.967114 0.323439 0.326434 11.00000 0.03222 0.03311 = 0.03885 -0.00267 -0.00254 -0.00431 C22A 1 0.921913 0.397757 0.336439 11.00000 0.04114 0.03532 = 0.04671 -0.00521 -0.00468 -0.00182 AFIX 43 H22A 2 0.902501 0.437776 0.308475 11.00000 -1.20000 AFIX 0 C23A 1 0.905214 0.413245 0.387773 11.00000 0.04557 0.04526 = 0.05290 -0.01834 -0.00302 -0.00650 C24A 1 0.934281 0.352912 0.428020 11.00000 0.04548 0.05082 = 0.04169 -0.01545 0.00025 -0.00641 AFIX 43 H24A 2 0.920211 0.363731 0.463190 11.00000 -1.20000 AFIX 0 C25A 1 0.983162 0.277221 0.419103 11.00000 0.03927 0.04765 = 0.03914 -0.00899 -0.00180 -0.00804 C26A 1 0.997793 0.266065 0.367291 11.00000 0.03636 0.03271 = 0.04286 -0.01206 -0.00223 -0.00089 C27A 1 0.850645 0.493985 0.400645 11.00000 0.06265 0.04087 = 0.06275 -0.01990 -0.00279 -0.00411 PART 1 C28A 1 0.820930 0.551639 0.352281 41.00000 0.14943 0.03658 = 0.09111 -0.01518 0.02900 0.00594 AFIX 137 H28A 2 0.765665 0.533596 0.334283 41.00000 -1.50000 H28B 2 0.899654 0.557380 0.328121 41.00000 -1.50000 H28C 2 0.778345 0.601051 0.363310 41.00000 -1.50000 AFIX 0 PART 2 C28D 1 0.918164 0.551515 0.354624 -41.00000 0.09254 0.03943 = 0.06653 -0.01743 -0.00416 -0.00503 AFIX 137 H28D 2 0.894382 0.549463 0.320762 -41.00000 -1.50000 H28E 2 1.010096 0.536168 0.352233 -41.00000 -1.50000 H28F 2 0.890869 0.603724 0.363031 -41.00000 -1.50000 AFIX 0 PART 1 C29A 1 0.933460 0.514227 0.430995 41.00000 0.07471 0.09910 = 0.19232 -0.10990 -0.01033 -0.01636 AFIX 137 H29A 2 0.898047 0.565419 0.440425 41.00000 -1.50000 H29B 2 1.017464 0.513636 0.409630 41.00000 -1.50000 H29C 2 0.940307 0.477177 0.463248 41.00000 -1.50000 AFIX 0 PART 2 C29D 1 0.895794 0.513878 0.449960 -41.00000 0.11429 0.05196 = 0.04672 -0.02444 -0.00536 0.01476 AFIX 137 H29D 2 0.876248 0.569336 0.449492 -41.00000 -1.50000 H29E 2 0.987118 0.495231 0.447920 -41.00000 -1.50000 H29F 2 0.851753 0.489289 0.482765 -41.00000 -1.50000 AFIX 0 PART 1 C30A 1 0.715584 0.493250 0.437542 41.00000 0.04889 0.04869 = 0.07055 -0.02466 0.00063 0.00167 AFIX 137 H30A 2 0.677409 0.544880 0.445593 41.00000 -1.50000 H30B 2 0.726578 0.458399 0.470484 41.00000 -1.50000 H30C 2 0.660314 0.476022 0.419073 41.00000 -1.50000 AFIX 0 PART 2 C30D 1 0.719380 0.511818 0.401465 -41.00000 0.05668 0.06598 = 0.18365 -0.07422 0.00310 0.00050 AFIX 137 H30D 2 0.679758 0.474147 0.427233 -41.00000 -1.50000 H30E 2 0.701449 0.510914 0.366321 -41.00000 -1.50000 H30F 2 0.685372 0.562833 0.411414 -41.00000 -1.50000 AFIX 0 PART 0 C31A 1 1.018650 0.212113 0.463246 11.00000 0.04813 0.05199 = 0.03978 -0.00387 -0.00466 -0.00750 C32A 1 0.949142 0.147761 0.464955 11.00000 0.06990 0.05840 = 0.06028 -0.00150 0.00522 -0.01911 AFIX 137 H32A 2 0.858310 0.168556 0.467289 11.00000 -1.50000 H32B 2 0.964449 0.109323 0.495888 11.00000 -1.50000 H32C 2 0.980042 0.124090 0.432784 11.00000 -1.50000 AFIX 0 C33A 1 0.986156 0.238634 0.517550 11.00000 0.10496 0.07431 = 0.04503 -0.00800 -0.01427 -0.01111 AFIX 137 H33A 2 1.029313 0.280413 0.517036 11.00000 -1.50000 H33B 2 1.013723 0.195934 0.544351 11.00000 -1.50000 H33C 2 0.894635 0.256531 0.526021 11.00000 -1.50000 AFIX 0 C34A 1 1.161954 0.182148 0.451890 11.00000 0.05465 0.07367 = 0.06955 0.01532 -0.01635 -0.00379 AFIX 137 H34A 2 1.184653 0.164592 0.417311 11.00000 -1.50000 H34B 2 1.186341 0.139521 0.479280 11.00000 -1.50000 H34C 2 1.206280 0.223216 0.451836 11.00000 -1.50000 AFIX 0 PART 2 C35 1 1.407821 -0.042047 0.087161 21.00000 0.19122 0.10274 = 0.07804 -0.05786 0.00548 0.03408 AFIX 137 H35A 2 1.475143 -0.052863 0.108614 21.00000 -1.50000 H35B 2 1.445091 -0.047249 0.050356 21.00000 -1.50000 H35C 2 1.351058 -0.078225 0.100570 21.00000 -1.50000 AFIX 0 C36 1 1.421394 0.098301 0.068068 21.00000 0.12256 0.14366 = 0.07744 -0.04369 0.05185 -0.05048 AFIX 137 H36A 2 1.372651 0.149480 0.073011 21.00000 -1.50000 H36B 2 1.452305 0.096574 0.030348 21.00000 -1.50000 H36C 2 1.493322 0.086461 0.087100 21.00000 -1.50000 AFIX 0 C37 1 1.227964 0.054442 0.054901 21.00000 0.13737 0.13373 = 0.06428 -0.05550 -0.01208 -0.01357 AFIX 137 H37A 2 1.161262 0.026339 0.072418 21.00000 -1.50000 H37B 2 1.264119 0.037961 0.020461 21.00000 -1.50000 H37C 2 1.192206 0.109307 0.049903 21.00000 -1.50000 AFIX 0 PART 0 P1B 5 1.693621 -0.349770 -0.356712 11.00000 0.04289 0.03119 = 0.03985 -0.00496 -0.00826 -0.00614 H1B 2 1.815204 -0.347050 -0.381214 11.00000 0.02678 O1B 4 1.621883 -0.325738 -0.409775 11.00000 0.05413 0.03084 = 0.03912 -0.00452 -0.01569 -0.00099 O2B 4 1.684356 -0.438797 -0.359658 11.00000 0.05303 0.02785 = 0.03848 -0.00169 -0.01220 -0.00402 N1B 3 1.625691 -0.260222 -0.339733 11.00000 0.04347 0.02990 = 0.03828 -0.00633 -0.01066 -0.00256 N2B 3 1.717903 -0.377623 -0.291740 11.00000 0.04831 0.02798 = 0.03390 -0.00034 -0.01467 -0.00710 C1B 1 1.631406 -0.251237 -0.287873 11.00000 0.03952 0.03143 = 0.03819 -0.00579 -0.00558 -0.01259 C2B 1 1.592490 -0.186959 -0.263619 11.00000 0.05413 0.03018 = 0.04750 -0.00589 -0.01424 -0.00755 AFIX 43 H2B 2 1.557899 -0.139625 -0.282756 11.00000 -1.20000 AFIX 0 C3B 1 1.603888 -0.191397 -0.210972 11.00000 0.05957 0.04049 = 0.04672 -0.01462 -0.01264 -0.00802 AFIX 43 H3B 2 1.577552 -0.147009 -0.194144 11.00000 -1.20000 AFIX 0 C4B 1 1.653190 -0.259924 -0.183382 11.00000 0.05730 0.04664 = 0.04055 -0.01024 -0.01110 -0.01395 AFIX 43 H4B 2 1.658641 -0.262615 -0.147202 11.00000 -1.20000 AFIX 0 C5B 1 1.695120 -0.325157 -0.207052 11.00000 0.04762 0.04059 = 0.04300 -0.00464 -0.01231 -0.00844 AFIX 43 H5B 2 1.730608 -0.372144 -0.187788 11.00000 -1.20000 AFIX 0 C6B 1 1.684167 -0.320341 -0.259272 11.00000 0.03880 0.02959 = 0.04091 -0.00697 -0.00778 -0.01022 C7B 1 1.552036 -0.212998 -0.375746 11.00000 0.04087 0.03308 = 0.03493 -0.00120 -0.00534 -0.00754 C8B 1 1.553030 -0.252001 -0.416390 11.00000 0.04154 0.02570 = 0.04038 -0.00067 -0.00533 -0.00596 C9B 1 1.489230 -0.221165 -0.458697 11.00000 0.04373 0.03822 = 0.03427 0.00049 -0.00757 -0.01374 C10B 1 1.417369 -0.146960 -0.456021 11.00000 0.04421 0.03940 = 0.03905 0.00512 -0.01029 -0.00782 AFIX 43 H10B 2 1.371911 -0.122970 -0.483995 11.00000 -1.20000 AFIX 0 C11B 1 1.409351 -0.106888 -0.414627 11.00000 0.04083 0.03315 = 0.04107 0.00195 -0.00681 -0.01086 C12B 1 1.479853 -0.140265 -0.374118 11.00000 0.04785 0.03333 = 0.04040 -0.00591 -0.00743 -0.01047 AFIX 43 H12B 2 1.478070 -0.113339 -0.345987 11.00000 -1.20000 AFIX 0 C13B 1 1.498484 -0.264368 -0.504360 11.00000 0.05340 0.04358 = 0.03903 -0.00668 -0.01237 -0.00916 C14B 1 1.636960 -0.286913 -0.529332 11.00000 0.06902 0.05854 = 0.04873 -0.01570 -0.01149 -0.00197 AFIX 137 H14G 2 1.673694 -0.241051 -0.540686 11.00000 -1.50000 H14H 2 1.642189 -0.312215 -0.559963 11.00000 -1.50000 H14I 2 1.683704 -0.321915 -0.503344 11.00000 -1.50000 AFIX 0 C15B 1 1.441338 -0.336198 -0.483665 11.00000 0.08637 0.05559 = 0.05661 -0.00633 -0.01812 -0.03011 AFIX 137 H15G 2 1.487475 -0.368679 -0.456536 11.00000 -1.50000 H15H 2 1.447900 -0.364539 -0.512907 11.00000 -1.50000 H15I 2 1.352255 -0.321108 -0.468376 11.00000 -1.50000 AFIX 0 C16B 1 1.426563 -0.215942 -0.548190 11.00000 0.07154 0.06623 = 0.04619 -0.00579 -0.02374 -0.01319 AFIX 137 H16G 2 1.336499 -0.202644 -0.533825 11.00000 -1.50000 H16H 2 1.437615 -0.245315 -0.577272 11.00000 -1.50000 H16I 2 1.459911 -0.169121 -0.561301 11.00000 -1.50000 AFIX 0 C17B 1 1.324606 -0.027614 -0.411609 11.00000 0.04837 0.03583 = 0.04945 0.00023 -0.00884 -0.00133 PART 1 C18B 1 1.224145 -0.035607 -0.363627 -31.00000 0.06791 0.06892 = 0.08133 -0.00168 0.01202 0.01513 AFIX 137 H18J 2 1.166052 0.013630 -0.360992 -31.00000 -1.50000 H18K 2 1.263887 -0.051774 -0.331885 -31.00000 -1.50000 H18L 2 1.177159 -0.073877 -0.366799 -31.00000 -1.50000 AFIX 0 PART 2 C18E 1 1.300601 0.001466 -0.355598 31.00000 0.10372 0.06052 = 0.07506 -0.02957 -0.03634 0.02780 AFIX 137 H18M 2 1.219050 0.036985 -0.351124 31.00000 -1.50000 H18N 2 1.368156 0.027555 -0.353993 31.00000 -1.50000 H18O 2 1.299886 -0.042323 -0.327354 31.00000 -1.50000 AFIX 0 PART 1 C19B 1 1.253338 -0.000903 -0.459749 -31.00000 0.11621 0.04433 = 0.08247 -0.00270 -0.03975 0.01832 AFIX 137 H19J 2 1.203140 -0.038418 -0.461145 -31.00000 -1.50000 H19K 2 1.314684 0.003768 -0.492379 -31.00000 -1.50000 H19L 2 1.197336 0.048751 -0.456022 -31.00000 -1.50000 AFIX 0 PART 2 C19E 1 1.195746 -0.017625 -0.425301 31.00000 0.06777 0.04143 = 0.09312 -0.00528 -0.04084 0.00328 AFIX 137 H19M 2 1.146164 0.032479 -0.418053 31.00000 -1.50000 H19N 2 1.153476 -0.057779 -0.403968 31.00000 -1.50000 H19O 2 1.203153 -0.021030 -0.462855 31.00000 -1.50000 AFIX 0 PART 1 C20B 1 1.399554 0.028164 -0.409046 -31.00000 0.08228 0.03462 = 0.16254 -0.02528 -0.02031 -0.00624 AFIX 137 H20J 2 1.469195 0.027478 -0.438969 -31.00000 -1.50000 H20K 2 1.433833 0.015111 -0.375912 -31.00000 -1.50000 H20L 2 1.345830 0.079260 -0.410542 -31.00000 -1.50000 AFIX 0 PART 2 C20E 1 1.395424 0.033463 -0.451213 31.00000 0.07446 0.02857 = 0.14111 0.01287 0.03986 0.00825 AFIX 137 H20M 2 1.410130 0.021179 -0.487211 31.00000 -1.50000 H20N 2 1.476553 0.031953 -0.440611 31.00000 -1.50000 H20O 2 1.342985 0.084682 -0.450085 31.00000 -1.50000 AFIX 0 PART 0 C21B 1 1.746326 -0.457042 -0.278038 11.00000 0.04562 0.03130 = 0.04122 -0.00265 -0.01363 -0.00440 C22B 1 1.789493 -0.501135 -0.233642 11.00000 0.06919 0.03835 = 0.04477 -0.00200 -0.02303 -0.00754 AFIX 43 H22B 2 1.804859 -0.477628 -0.206584 11.00000 -1.20000 AFIX 0 C23B 1 1.810070 -0.580077 -0.229105 11.00000 0.06884 0.03373 = 0.04541 0.00189 -0.01968 -0.00434 C24B 1 1.783636 -0.612385 -0.268679 11.00000 0.05689 0.02974 = 0.05354 -0.00292 -0.01260 -0.00437 AFIX 43 H24B 2 1.796824 -0.666489 -0.264845 11.00000 -1.20000 AFIX 0 C25B 1 1.738255 -0.569673 -0.314373 11.00000 0.03971 0.03309 = 0.04281 -0.00521 -0.00701 -0.00752 C26B 1 1.725357 -0.491341 -0.317616 11.00000 0.04220 0.03047 = 0.03769 0.00003 -0.00951 -0.00225 C27B 1 1.857207 -0.627303 -0.179126 11.00000 0.10572 0.03451 = 0.05765 0.00505 -0.03798 -0.00529 C28B 1 1.978402 -0.604916 -0.173110 11.00000 0.14108 0.08736 = 0.14803 0.03622 -0.10890 -0.03017 AFIX 137 H28J 2 2.043442 -0.615998 -0.203747 11.00000 -1.50000 H28K 2 2.007782 -0.634155 -0.140864 11.00000 -1.50000 H28L 2 1.961854 -0.550211 -0.170853 11.00000 -1.50000 AFIX 0 C29B 1 1.755877 -0.610291 -0.130973 11.00000 0.17123 0.06326 = 0.05310 -0.00170 -0.03101 -0.00069 AFIX 137 H29J 2 1.733217 -0.555031 -0.130542 11.00000 -1.50000 H29K 2 1.788872 -0.635662 -0.098608 11.00000 -1.50000 H29L 2 1.680796 -0.629312 -0.133003 11.00000 -1.50000 AFIX 0 C30B 1 1.884899 -0.713185 -0.180673 11.00000 0.13181 0.04338 = 0.07218 0.00936 -0.04399 0.00315 AFIX 137 H30J 2 1.807116 -0.729118 -0.182917 11.00000 -1.50000 H30K 2 1.916859 -0.740535 -0.148492 11.00000 -1.50000 H30L 2 1.948489 -0.725000 -0.211605 11.00000 -1.50000 AFIX 0 C31B 1 1.704995 -0.606546 -0.356624 11.00000 0.04728 0.03087 = 0.04908 -0.00710 -0.00644 -0.00669 C32B 1 1.784395 -0.586576 -0.410711 11.00000 0.07919 0.06406 = 0.05483 -0.02202 0.00284 -0.02309 AFIX 137 H32G 2 1.770019 -0.530974 -0.420696 11.00000 -1.50000 H32H 2 1.759772 -0.609593 -0.437206 11.00000 -1.50000 H32I 2 1.874101 -0.606408 -0.408772 11.00000 -1.50000 AFIX 0 C33B 1 1.727978 -0.693946 -0.343628 11.00000 0.08769 0.03688 = 0.07195 -0.01520 -0.02846 -0.00695 AFIX 137 H33G 2 1.817384 -0.713980 -0.341165 11.00000 -1.50000 H33H 2 1.705277 -0.714963 -0.371583 11.00000 -1.50000 H33I 2 1.675951 -0.708717 -0.309834 11.00000 -1.50000 AFIX 0 C34B 1 1.564832 -0.577904 -0.360909 11.00000 0.05482 0.06184 = 0.07147 -0.01994 -0.01446 -0.00633 AFIX 137 H34G 2 1.513047 -0.593451 -0.327233 11.00000 -1.50000 H34H 2 1.544490 -0.599879 -0.388961 11.00000 -1.50000 H34I 2 1.547349 -0.522071 -0.369273 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_RomanTA63b_0ma_a.res in P-1 REM R1 = 0.0601 for 7866 Fo > 4sig(Fo) and 0.1472 for all 15649 data REM 1220 parameters refined using 1380 restraints END WGHT 0.0675 0.0000 REM Highest difference peak 0.225, deepest hole -0.313, 1-sigma level 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0 135.99 5.90 -4 -8 0 139.29 8.00 5 9 0 7.00 4.30 -5 -9 0 0.60 4.10 -5 -9 0 6.20 6.00 -5 -9 0 3.40 2.00 6 10 0 1.50 4.40 -6 -10 0 2.70 4.40 -6 -10 0 6.30 2.30 -6 -10 0 8.30 7.40 7 11 0 -2.00 5.60 -7 -11 0 3.80 6.90 -7 -11 0 3.60 5.10 8 12 0 88.19 9.10 -8 -12 0 86.49 11.00 -8 -12 0 97.39 10.10 -9 -13 0 10.20 7.70 -9 -13 0 14.10 6.10 -10 -14 0 6.00 7.10 -10 -14 0 5.50 5.40 -12 -7 0 54.39 9.20 12 7 0 57.19 9.80 -11 -6 0 11.40 5.60 11 6 0 4.30 6.20 -10 -5 0 13.60 6.10 10 5 0 4.20 5.70 -9 -4 0 75.59 9.40 9 4 0 96.29 9.70 -8 -3 0 6.60 4.90 -8 -3 0 4.60 5.60 8 3 0 8.50 5.40 -7 -2 0 14.30 5.10 -7 -2 0 21.70 4.50 7 2 0 13.40 4.90 7 2 0 12.90 2.60 -6 -1 0 12.10 4.10 -6 -1 0 14.80 3.70 -6 -1 0 8.60 2.70 6 1 0 9.90 2.30 6 1 0 12.70 4.00 -5 0 0 -1.50 2.90 -5 0 0 1.10 3.10 5 0 0 2.90 1.80 5 0 0 -1.90 2.50 -4 1 0 99.39 6.20 -4 1 0 115.69 5.80 4 -1 0 104.69 5.10 4 -1 0 100.19 5.70 -3 2 0 14.00 2.90 3 -2 0 11.90 2.50 3 -2 0 12.00 2.70 -2 3 0 262.47 7.50 -2 3 0 263.47 7.40 -2 3 0 269.67 8.30 2 -3 0 258.67 7.80 2 -3 0 269.47 8.70 2 -3 0 266.17 7.70 -1 4 0 9.70 1.80 -1 4 0 17.60 4.00 -1 4 0 16.70 2.10 1 -4 0 16.10 3.30 1 -4 0 9.80 3.10 1 -4 0 13.50 1.90 0 5 0 674.53 13.20 0 5 0 695.03 15.40 0 -5 0 676.53 15.80 0 -5 0 690.43 16.90 0 -5 0 685.63 13.10 1 6 0 10.00 2.40 1 6 0 6.30 2.20 -1 -6 0 5.60 3.70 -1 -6 0 6.00 2.10 -1 -6 0 5.80 2.30 2 7 0 0.10 2.40 -2 -7 0 2.20 2.10 -2 -7 0 0.90 4.10 3 8 0 45.10 4.70 -3 -8 0 45.70 6.60 -3 -8 0 37.90 3.70 4 9 0 21.20 4.10 -4 -9 0 27.30 4.90 -4 -9 0 14.40 5.70 -4 -9 0 19.80 3.00 5 10 0 275.17 11.70 -5 -10 0 281.27 9.30 -5 -10 0 280.07 12.20 -5 -10 0 255.67 15.00 6 11 0 29.70 6.60 -6 -11 0 26.40 3.50 -6 -11 0 31.50 8.00 -6 -11 0 20.60 6.10 7 12 0 9.60 5.90 -7 -12 0 4.20 7.90 -7 -12 0 2.20 5.20 8 13 0 8.90 5.90 -8 -13 0 13.20 5.70 -8 -13 0 0.30 6.30 -9 -14 0 25.70 9.00 -9 -14 0 15.70 6.50 -10 -15 0 -2.50 4.80 -10 -15 0 8.50 7.40 -12 -6 0 1.50 5.80 12 6 0 1.30 5.90 -11 -5 0 5.90 5.60 11 5 0 2.60 5.90 -10 -4 0 22.20 6.70 10 4 0 24.70 6.70 -9 -3 0 26.30 6.80 9 3 0 39.90 7.30 -8 -2 0 2.50 4.50 -8 -2 0 -0.70 4.30 8 2 0 1.50 4.50 8 2 0 1.80 3.10 -7 -1 0 2.70 3.90 -7 -1 0 6.60 3.90 7 1 0 1.80 3.90 7 1 0 7.00 2.60 -6 0 0 120.59 8.30 6 0 0 118.39 6.00 6 0 0 123.99 7.60 -5 1 0 65.79 5.00 -5 1 0 63.69 6.10 5 -1 0 62.39 4.90 5 -1 0 53.19 5.10 -4 2 0 84.59 4.20 -4 2 0 89.09 5.80 4 -2 0 82.19 5.30 4 -2 0 84.69 5.40 -3 3 0 65.29 3.80 -3 3 0 65.89 4.40 3 -3 0 62.09 4.40 3 -3 0 79.79 5.30 3 -3 0 62.49 4.00 -2 4 0 117.09 4.70 -2 4 0 126.69 6.10 -2 4 0 123.99 5.70 2 -4 0 120.49 6.50 2 -4 0 119.39 5.40 2 -4 0 118.99 5.30 2 -4 0 118.79 5.30 -1 5 0 9.70 1.90 -1 5 0 14.30 2.00 1 -5 0 13.00 1.90 1 -5 0 12.20 3.20 1 -5 0 8.60 2.60 0 6 0 2.10 1.50 0 6 0 0.20 1.80 0 -6 0 3.30 1.50 0 -6 0 -0.70 2.40 0 -6 0 -2.30 2.90 1 7 0 576.14 12.70 1 7 0 582.24 15.50 -1 -7 0 590.04 16.90 -1 -7 0 584.94 12.90 -1 -7 0 568.84 14.80 2 8 0 2.60 2.60 2 8 0 3.40 3.30 -2 -8 0 0.20 4.00 -2 -8 0 -0.60 2.20 3 9 0 151.18 7.30 -3 -9 0 138.39 10.10 -3 -9 0 155.58 7.40 4 10 0 -4.60 3.30 -4 -10 0 0.40 3.80 -4 -10 0 4.40 5.40 -4 -10 0 1.60 2.40 5 11 0 24.30 5.30 -5 -11 0 18.70 3.50 -5 -11 0 18.10 7.90 -5 -11 0 28.70 5.80 6 12 0 14.50 5.80 -6 -12 0 6.50 8.10 -6 -12 0 7.90 5.40 7 13 0 -3.10 4.80 -7 -13 0 1.80 4.50 -7 -13 0 6.40 7.60 8 14 0 -4.10 5.20 -8 -14 0 2.80 4.90 -8 -14 0 -4.10 6.20 -9 -15 0 8.00 5.30 -9 -15 0 -3.80 5.80 -12 -5 0 15.80 6.20 12 5 0 31.30 7.70 -11 -4 0 2.00 5.00 11 4 0 1.00 5.10 -10 -3 0 2.90 4.60 10 3 0 8.40 5.40 -9 -2 0 94.59 10.10 9 2 0 94.39 9.40 -8 -1 0 25.20 6.40 -8 -1 0 28.40 4.80 8 1 0 17.40 3.60 8 1 0 21.40 5.50 -7 0 0 20.70 5.20 -7 0 0 22.10 4.10 7 0 0 15.00 3.10 7 0 0 9.40 4.20 -6 1 0 10.70 4.10 -6 1 0 8.70 3.40 6 -1 0 6.60 2.50 6 -1 0 6.30 3.40 -5 2 0 -1.20 3.00 -5 2 0 0.10 2.60 -5 2 0 0.40 2.10 5 -2 0 2.80 2.40 5 -2 0 -2.50 3.10 -4 3 0 55.39 3.70 -4 3 0 60.89 5.20 4 -3 0 57.29 4.80 4 -3 0 56.99 5.10 -3 4 0 41.30 3.80 -3 4 0 43.60 4.10 -3 4 0 45.60 3.70 3 -4 0 35.80 4.00 3 -4 0 40.60 4.00 3 -4 0 44.90 4.10 -2 5 0 -0.80 1.50 -2 5 0 -0.10 1.10 2 -5 0 0.20 2.40 2 -5 0 -0.40 1.60 2 -5 0 -1.50 2.10 -1 6 0 10.10 2.10 -1 6 0 9.00 2.00 1 -6 0 10.70 1.80 1 -6 0 9.50 3.30 1 -6 0 10.60 2.90 0 7 0 54.89 4.20 0 7 0 52.59 3.60 0 -7 0 51.59 4.90 0 -7 0 51.49 3.30 0 -7 0 52.19 6.00 1 8 0 315.77 11.30 1 8 0 313.57 8.70 -1 -8 0 320.97 11.00 -1 -8 0 302.87 12.40 2 9 0 13.40 4.60 2 9 0 15.10 3.40 -2 -9 0 13.90 3.40 -2 -9 0 12.00 5.50 3 10 0 6.50 3.40 -3 -10 0 12.80 5.50 -3 -10 0 5.20 2.90 4 11 0 3.30 4.00 -4 -11 0 5.80 4.40 -4 -11 0 0.90 5.90 -4 -11 0 1.40 2.80 5 12 0 88.59 8.10 -5 -12 0 96.99 7.10 -5 -12 0 79.29 10.50 -5 -12 0 106.39 8.70 6 13 0 4.30 5.30 -6 -13 0 2.20 7.30 -6 -13 0 7.00 5.20 7 14 0 12.50 5.70 -7 -14 0 7.80 7.80 -7 -14 0 10.40 5.20 8 15 0 1.50 5.30 -8 -15 0 4.10 5.00 -8 -15 0 -0.40 6.30 -9 -16 0 17.40 6.50 -9 -16 0 22.30 8.90 -12 -4 0 40.00 8.40 12 4 0 41.10 8.20 -11 -3 0 1.50 4.70 11 3 0 10.60 5.60 -10 -2 0 -0.50 5.00 10 2 0 -4.10 4.30 -9 -1 0 7.00 5.00 9 1 0 2.70 4.90 -8 0 0 -3.00 4.40 8 0 0 -2.40 2.80 8 0 0 0.20 4.10 -7 1 0 32.20 4.60 -7 1 0 42.30 6.60 7 -1 0 35.80 4.40 7 -1 0 39.20 5.80 -6 2 0 9.30 3.30 -6 2 0 0.80 2.30 -6 2 0 2.20 3.40 6 -2 0 -2.60 2.30 6 -2 0 2.00 3.00 -5 3 0 166.88 5.80 -5 3 0 166.98 8.30 5 -3 0 171.48 8.20 5 -3 0 171.28 8.30 -4 4 0 18.20 2.90 -4 4 0 11.80 2.80 -4 4 0 19.40 3.50 4 -4 0 15.90 3.30 4 -4 0 13.80 3.30 -3 5 0 255.07 9.50 -3 5 0 250.87 8.20 3 -5 0 238.28 9.70 3 -5 0 254.77 9.00 3 -5 0 240.48 8.30 -2 6 0 134.19 5.40 -2 6 0 148.99 6.90 2 -6 0 150.18 8.00 2 -6 0 148.49 6.80 -1 7 0 125.19 6.20 -1 7 0 114.39 4.70 1 -7 0 113.89 4.50 1 -7 0 112.59 6.90 1 -7 0 113.19 7.10 0 8 0 45.40 3.70 0 8 0 28.80 3.60 0 -8 0 30.80 5.20 0 -8 0 33.60 4.40 0 -8 0 33.00 3.70 1 9 0 424.46 14.10 1 9 0 425.76 11.00 -1 -9 0 425.96 13.80 -1 -9 0 445.96 15.90 2 10 0 1.70 3.00 2 10 0 8.80 4.60 -2 -10 0 0.40 5.40 -2 -10 0 5.20 3.10 3 11 0 15.00 4.00 -3 -11 0 13.20 3.70 -3 -11 0 6.00 6.40 4 12 0 60.29 6.60 -4 -12 0 49.80 9.70 -4 -12 0 66.09 7.20 -4 -12 0 53.39 5.70 5 13 0 6.30 5.10 -5 -13 0 3.00 4.70 -5 -13 0 -3.50 7.80 -5 -13 0 0.00 3.10 6 14 0 37.60 6.80 -6 -14 0 19.60 8.90 -6 -14 0 33.30 6.70 7 15 0 5.40 5.20 -7 -15 0 -0.30 6.80 -7 -15 0 1.30 4.60 8 16 0 1.20 5.10 -8 -16 0 -2.90 6.50 -8 -16 0 -1.00 5.00 -9 -17 0 7.50 5.30 -12 -3 0 1.10 5.10 12 3 0 0.30 5.40 -11 -2 0 -1.40 5.10 11 2 0 0.00 5.10 -10 -1 0 20.10 6.00 10 1 0 11.20 5.20 -9 0 0 25.80 6.60 9 0 0 18.20 5.70 -8 1 0 6.40 4.50 8 -1 0 9.40 4.70 8 -1 0 8.10 3.60 -7 2 0 2.70 3.70 -7 2 0 1.20 3.80 7 -2 0 5.40 3.30 7 -2 0 9.00 4.30 -6 3 0 134.59 7.70 -6 3 0 125.99 8.30 -6 3 0 117.59 5.20 6 -3 0 126.19 7.90 6 -3 0 120.09 7.60 -5 4 0 27.70 4.30 -5 4 0 20.90 3.10 5 -4 0 20.50 3.90 5 -4 0 42.00 5.00 -4 5 0 22.70 3.70 -4 5 0 24.00 3.80 4 -5 0 21.40 4.10 4 -5 0 28.80 4.20 4 -5 0 22.90 3.40 -3 6 0 163.38 6.70 -3 6 0 159.58 7.70 3 -6 0 156.98 8.90 3 -6 0 174.38 7.50 3 -6 0 151.28 7.30 -2 7 0 3.50 2.10 -2 7 0 0.20 1.50 2 -7 0 8.70 3.20 2 -7 0 2.60 2.80 -1 8 0 780.82 16.10 -1 8 0 799.42 19.70 1 -8 0 788.42 20.70 1 -8 0 775.22 19.90 0 9 0 47.90 3.90 0 9 0 44.40 4.50 0 -9 0 43.60 6.70 0 -9 0 47.90 5.80 1 10 0 300.97 9.20 1 10 0 292.77 11.90 -1 -10 0 276.27 13.90 -1 -10 0 307.37 12.00 2 11 0 31.80 4.40 2 11 0 33.30 6.50 -2 -11 0 32.60 7.10 -2 -11 0 32.70 5.00 3 12 0 31.20 4.90 -3 -12 0 26.70 7.70 -3 -12 0 28.00 4.90 4 13 0 6.90 4.40 -4 -13 0 11.80 5.20 -4 -13 0 10.50 7.30 -4 -13 0 6.80 3.80 5 14 0 21.40 5.60 -5 -14 0 15.20 4.40 -5 -14 0 21.80 5.80 -5 -14 0 19.40 8.40 6 15 0 11.60 5.10 -6 -15 0 5.10 7.40 -6 -15 0 10.80 5.20 7 16 0 0.20 4.70 -7 -16 0 0.80 6.60 -7 -16 0 2.20 4.60 -8 -17 0 20.90 8.40 -8 -17 0 10.80 6.50 -12 -2 0 5.60 5.20 12 2 0 13.30 6.00 -11 -1 0 6.40 5.10 11 1 0 24.30 6.40 -10 0 0 13.30 5.40 10 0 0 5.40 4.50 -9 1 0 -8.60 4.20 9 -1 0 5.00 4.60 -8 2 0 7.50 5.00 8 -2 0 8.80 4.00 8 -2 0 7.80 4.70 -7 3 0 7.20 4.00 -7 3 0 3.00 4.00 7 -3 0 0.10 3.10 7 -3 0 -2.00 3.60 -6 4 0 4.40 3.00 -6 4 0 2.40 3.40 6 -4 0 -1.50 2.70 6 -4 0 -0.20 3.10 -5 5 0 1.70 2.90 -5 5 0 0.70 2.10 5 -5 0 2.80 2.80 5 -5 0 0.20 3.00 -4 6 0 170.38 7.70 -4 6 0 153.38 8.30 4 -6 0 159.58 7.50 4 -6 0 150.18 7.80 4 -6 0 152.48 9.20 -3 7 0 257.67 10.30 -3 7 0 281.77 8.90 3 -7 0 236.28 11.30 3 -7 0 252.07 9.60 -2 8 0 28.30 3.60 -2 8 0 35.30 3.50 2 -8 0 28.70 5.10 2 -8 0 35.10 4.90 -1 9 0 0.70 1.60 -1 9 0 0.60 2.30 1 -9 0 -1.90 2.80 1 -9 0 -0.50 3.40 0 10 0 210.78 7.50 0 10 0 212.48 9.90 0 -10 0 219.88 10.50 1 11 0 236.28 8.40 1 11 0 230.28 11.50 -1 -11 0 239.48 13.80 -1 -11 0 226.78 11.20 2 12 0 6.00 3.60 2 12 0 12.10 5.70 -2 -12 0 5.50 6.10 -2 -12 0 10.00 4.10 3 13 0 54.49 5.90 -3 -13 0 50.89 9.70 -3 -13 0 55.19 6.50 4 14 0 46.50 6.30 -4 -14 0 43.70 6.10 -4 -14 0 36.50 10.00 -4 -14 0 50.59 7.10 5 15 0 3.80 4.70 -5 -15 0 3.90 3.90 -5 -15 0 18.10 5.70 -5 -15 0 12.60 7.60 6 16 0 3.50 4.70 -6 -16 0 -1.50 4.30 -6 -16 0 4.50 7.40 -7 -17 0 7.20 7.70 -8 -18 0 5.10 7.80 -12 -1 0 1.50 5.60 12 1 0 14.70 5.70 -11 0 0 5.90 5.10 11 0 0 6.60 5.20 -10 1 0 3.70 5.10 10 -1 0 2.10 4.30 -9 2 0 4.90 4.70 9 -2 0 -0.70 4.00 9 -2 0 0.80 4.00 -8 3 0 -0.60 4.40 8 -3 0 0.20 3.70 8 -3 0 -6.80 3.90 -7 4 0 28.00 5.60 7 -4 0 34.20 5.40 7 -4 0 25.80 5.20 -6 5 0 5.10 2.80 -6 5 0 0.80 3.60 6 -5 0 3.30 3.20 6 -5 0 1.90 3.60 -5 6 0 39.40 5.10 -5 6 0 36.40 4.90 5 -6 0 42.30 5.50 5 -6 0 40.00 5.80 -4 7 0 4.40 2.70 -4 7 0 3.80 2.10 4 -7 0 2.00 3.50 4 -7 0 2.50 2.80 4 -7 0 2.80 3.50 -3 8 0 56.49 4.70 -3 8 0 48.40 5.20 3 -8 0 56.29 5.70 3 -8 0 53.39 6.30 -2 9 0 40.60 3.90 -2 9 0 25.60 3.70 2 -9 0 35.80 5.40 2 -9 0 34.60 5.30 -1 10 0 143.19 6.20 -1 10 0 136.39 8.10 1 -10 0 144.49 9.70 1 -10 0 136.69 9.10 0 11 0 0.30 2.20 0 11 0 -0.20 2.70 0 -11 0 3.40 5.40 0 -11 0 1.70 4.00 1 12 0 157.48 7.40 1 12 0 154.88 10.50 -1 -12 0 165.78 10.60 -1 -12 0 135.19 12.60 2 13 0 -0.60 5.70 2 13 0 1.50 3.70 -2 -13 0 13.30 7.70 -2 -13 0 0.00 4.10 3 14 0 7.50 4.30 -3 -14 0 4.00 4.20 -3 -14 0 5.20 7.30 4 15 0 9.80 4.80 -4 -15 0 8.40 4.40 -4 -15 0 3.90 4.90 -4 -15 0 11.00 8.40 5 16 0 7.20 4.60 -5 -16 0 0.40 3.50 -5 -16 0 5.60 7.80 -5 -16 0 -3.60 4.30 -6 -17 0 5.20 7.40 -7 -18 0 17.50 8.40 -12 0 0 -13.40 4.20 12 0 0 5.30 5.20 -11 1 0 -0.60 4.90 11 -1 0 8.90 4.70 -10 2 0 1.50 4.60 10 -2 0 -3.20 4.10 -9 3 0 1.70 4.50 9 -3 0 -0.40 4.00 9 -3 0 1.80 3.70 -8 4 0 7.00 4.80 8 -4 0 -4.50 3.60 8 -4 0 0.10 3.90 -7 5 0 50.99 6.50 -7 5 0 39.40 6.20 7 -5 0 32.30 5.80 7 -5 0 50.69 6.70 -6 6 0 2.80 2.70 -6 6 0 3.60 3.80 6 -6 0 8.00 4.00 6 -6 0 4.80 4.10 -5 7 0 26.60 4.50 -5 7 0 17.20 3.50 5 -7 0 22.30 4.50 5 -7 0 22.80 5.40 5 -7 0 19.60 4.20 -4 8 0 207.08 8.70 -4 8 0 202.68 10.10 4 -8 0 201.08 10.00 4 -8 0 221.38 11.90 -3 9 0 49.30 5.40 -3 9 0 55.69 4.90 3 -9 0 43.00 6.10 3 -9 0 56.99 6.20 -2 10 0 38.90 4.90 -2 10 0 45.80 4.40 2 -10 0 35.90 5.70 2 -10 0 47.90 6.30 -1 11 0 9.20 3.20 -1 11 0 13.10 3.50 1 -11 0 1.40 5.20 1 -11 0 0.30 4.20 0 12 0 0.70 3.10 0 12 0 6.30 3.40 0 -12 0 -0.60 3.60 0 -12 0 -6.90 5.40 1 13 0 13.80 3.90 1 13 0 16.60 5.00 -1 -13 0 12.20 4.60 2 14 0 25.10 5.00 2 14 0 27.40 7.70 -2 -14 0 28.30 5.90 -2 -14 0 27.30 9.10 3 15 0 1.00 4.20 -3 -15 0 2.30 4.50 -3 -15 0 5.70 7.40 -4 -16 0 24.10 5.40 -4 -16 0 20.00 7.80 -5 -17 0 52.19 11.10 -6 -18 0 0.60 7.00 -12 1 0 7.60 5.90 12 -1 0 -1.00 4.90 -11 2 0 -0.50 4.80 11 -2 0 0.40 4.40 -10 3 0 28.10 6.80 10 -3 0 23.50 6.10 -9 4 0 -1.90 4.10 9 -4 0 -0.80 3.80 9 -4 0 -2.40 3.60 -8 5 0 16.90 4.50 -8 5 0 28.80 6.10 8 -5 0 27.50 5.90 8 -5 0 25.10 5.60 -7 6 0 78.89 7.90 -7 6 0 66.49 7.60 7 -6 0 68.49 7.60 7 -6 0 61.69 7.30 -6 7 0 38.00 5.80 -6 7 0 39.40 5.80 6 -7 0 30.50 5.50 6 -7 0 28.20 5.90 -5 8 0 30.40 5.00 -5 8 0 17.50 3.90 5 -8 0 21.80 5.20 5 -8 0 15.40 4.60 5 -8 0 28.80 5.20 -4 9 0 6.60 3.30 -4 9 0 0.60 2.10 4 -9 0 -3.60 4.00 4 -9 0 6.40 4.80 -3 10 0 2.50 3.10 -3 10 0 1.40 2.10 3 -10 0 3.80 4.20 3 -10 0 -0.30 4.10 -2 11 0 208.48 10.60 -2 11 0 218.48 8.50 2 -11 0 176.08 11.00 2 -11 0 181.68 11.60 -1 12 0 31.00 4.20 -1 12 0 28.50 4.50 1 -12 0 34.60 6.20 1 -12 0 39.70 7.80 0 13 0 170.28 10.30 0 13 0 164.08 8.00 0 -13 0 161.58 11.70 1 14 0 36.10 7.00 1 14 0 53.09 5.40 -1 -14 0 44.90 9.20 -1 -14 0 36.80 6.70 2 15 0 139.59 13.00 -2 -15 0 143.49 11.30 -3 -16 0 10.90 4.70 -4 -17 0 2.40 4.10 -11 3 0 1.20 5.10 11 -3 0 8.60 5.20 -10 4 0 28.20 6.60 10 -4 0 28.00 6.40 -9 5 0 -0.50 3.10 -9 5 0 9.70 5.00 9 -5 0 8.20 4.50 9 -5 0 6.30 4.30 -8 6 0 10.50 4.00 -8 6 0 5.50 4.50 8 -6 0 7.60 4.20 8 -6 0 6.40 4.60 -7 7 0 4.10 3.60 -7 7 0 3.90 4.40 7 -7 0 2.90 4.10 7 -7 0 6.50 4.90 -6 8 0 -1.30 2.10 -6 8 0 3.20 4.00 6 -8 0 -1.50 3.50 6 -8 0 2.90 4.50 -5 9 0 127.49 8.90 -5 9 0 118.59 7.90 5 -9 0 126.99 11.00 5 -9 0 127.39 8.90 -4 10 0 5.30 2.90 -4 10 0 4.40 3.50 4 -10 0 4.90 4.60 4 -10 0 -0.90 4.90 -3 11 0 121.79 7.40 -3 11 0 126.89 8.90 3 -11 0 136.39 9.90 3 -11 0 135.39 11.40 -2 12 0 87.89 6.50 -2 12 0 87.69 7.90 2 -12 0 72.69 8.20 2 -12 0 85.09 9.20 -1 13 0 1.30 3.60 -1 13 0 2.20 3.30 1 -13 0 0.60 6.10 1 -13 0 2.30 4.40 0 14 0 47.80 6.90 0 -14 0 50.09 9.60 0 -14 0 37.50 7.00 1 15 0 81.59 9.30 -1 -15 0 94.19 9.80 -1 -15 0 109.29 12.40 2 16 0 -4.80 6.00 -2 -16 0 9.40 5.10 -2 -16 0 7.70 7.10 -3 -17 0 13.30 8.50 -3 -17 0 20.40 5.50 -4 -18 0 -0.30 8.70 -4 -18 0 22.10 5.70 -5 -19 0 -1.90 7.40 -11 4 0 1.40 3.10 -11 4 0 6.30 5.40 11 -4 0 3.30 4.40 -10 5 0 9.30 5.50 -10 5 0 7.10 4.20 10 -5 0 22.90 6.10 -9 6 0 9.80 4.90 -9 6 0 4.30 3.60 9 -6 0 9.60 4.90 9 -6 0 5.00 4.40 -8 7 0 12.90 4.10 -8 7 0 14.80 5.00 8 -7 0 8.40 4.40 8 -7 0 12.60 5.10 -7 8 0 59.89 7.40 -7 8 0 52.29 7.10 7 -8 0 60.59 7.60 7 -8 0 48.40 7.30 -6 9 0 30.50 5.30 -6 9 0 34.70 5.60 6 -9 0 35.00 6.10 6 -9 0 34.70 6.90 6 -9 0 30.90 6.50 -5 10 0 6.10 3.80 -5 10 0 0.50 2.90 5 -10 0 8.80 5.10 5 -10 0 6.00 5.20 -4 11 0 41.00 5.60 -4 11 0 46.10 5.60 4 -11 0 44.10 7.80 -3 12 0 2.10 2.90 -3 12 0 -0.40 3.70 3 -12 0 -3.00 5.10 3 -12 0 -2.10 5.10 -2 13 0 181.38 11.00 -2 13 0 205.08 10.40 2 -13 0 195.28 13.80 2 -13 0 185.68 12.70 -1 14 0 140.59 10.70 1 -14 0 145.99 12.70 1 -14 0 151.98 12.70 0 15 0 3.00 4.00 0 -15 0 6.10 6.60 0 -15 0 7.50 5.70 1 16 0 3.50 6.00 -1 -16 0 4.10 4.40 -1 -16 0 1.60 7.30 2 17 0 -3.50 7.20 -2 -17 0 4.80 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134.59 8.40 -7 0 -3 10.40 5.10 -7 0 -3 20.80 5.60 7 0 3 9.50 3.50 7 0 3 15.30 4.40 -6 1 -3 1.50 4.40 -6 1 -3 -0.90 3.40 6 -1 3 1.50 2.70 6 -1 3 -0.70 2.60 -5 2 -3 43.00 5.10 5 -2 3 55.89 5.40 5 -2 3 44.80 4.70 -4 3 -3 46.80 4.40 -4 3 -3 57.59 4.60 4 -3 3 54.29 4.60 4 -3 3 49.50 4.90 -3 4 -3 186.78 7.70 -3 4 -3 182.78 6.40 3 -4 3 187.18 7.90 3 -4 3 193.38 8.70 3 -4 3 182.58 7.30 -2 5 -3 9.50 1.60 -2 5 -3 8.10 1.90 -2 5 -3 6.30 1.80 2 -5 3 11.40 2.00 2 -5 3 7.00 2.80 2 -5 3 10.00 3.30 -1 6 -3 300.27 6.10 -1 6 -3 307.37 10.00 1 -6 3 311.37 6.30 1 -6 3 300.97 10.80 1 -6 3 300.07 10.80 0 7 -3 96.39 3.20 0 7 -3 98.59 6.20 0 -7 3 108.09 6.60 0 -7 3 100.59 3.10 0 -7 3 120.29 7.30 1 8 -3 51.79 3.40 1 8 -3 39.30 5.10 -1 -8 3 47.90 6.10 -1 -8 3 36.20 4.30 -1 -8 3 52.49 3.40 -1 -8 3 54.09 3.60 2 9 -3 97.69 5.30 2 9 -3 65.89 7.40 -2 -9 3 102.79 7.10 -2 -9 3 98.79 5.40 -2 -9 3 88.79 8.10 3 10 -3 7.80 3.30 -3 -10 3 5.10 3.20 -3 -10 3 9.20 3.20 4 11 -3 1.30 3.80 -4 -11 3 -1.60 3.00 -4 -11 3 -3.80 3.30 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6 -3 22.60 2.80 -3 6 -3 23.50 3.40 3 -6 3 21.90 4.20 3 -6 3 23.70 4.50 -2 7 -3 91.89 3.90 -2 7 -3 85.79 5.80 2 -7 3 98.39 7.80 2 -7 3 92.09 4.10 2 -7 3 91.39 7.20 -1 8 -3 47.60 2.80 -1 8 -3 37.10 4.50 1 -8 3 36.10 5.50 1 -8 3 40.60 5.10 1 -8 3 40.70 2.40 0 9 -3 306.17 12.00 0 9 -3 317.07 7.30 0 -9 3 335.17 7.30 0 -9 3 319.17 12.60 0 -9 3 304.97 13.10 1 10 -3 21.30 4.50 1 10 -3 23.30 2.80 -1 -10 3 22.60 2.60 -1 -10 3 23.90 4.60 -1 -10 3 35.60 6.10 2 11 -3 17.90 6.70 2 11 -3 7.80 3.00 -2 -11 3 12.70 4.10 -2 -11 3 7.20 6.20 -2 -11 3 5.30 2.90 3 12 -3 81.59 6.60 -3 -12 3 90.49 8.00 -3 -12 3 84.19 6.60 -3 -12 3 82.89 10.20 4 13 -3 7.10 4.30 -4 -13 3 1.50 3.80 -4 -13 3 0.40 6.80 -4 -13 3 5.00 3.80 5 14 -3 6.50 4.70 -5 -14 3 0.20 3.80 -5 -14 3 -7.00 6.40 -5 -14 3 2.30 3.70 -6 -15 3 63.89 7.70 -6 -15 3 46.40 9.40 -7 -16 3 -2.90 8.00 -8 -17 3 -8.50 8.10 -12 -2 -3 4.40 5.90 12 2 3 10.10 5.40 -11 -1 -3 9.00 5.80 11 1 3 7.00 5.10 -10 0 -3 -0.30 4.50 10 0 3 1.60 4.50 -9 1 -3 2.30 5.30 9 -1 3 3.80 4.60 9 -1 3 0.20 4.10 -8 2 -3 2.10 4.60 8 -2 3 -1.00 3.80 8 -2 3 6.00 4.30 -7 3 -3 -5.50 3.60 -7 3 -3 4.40 5.70 7 -3 3 0.50 3.30 7 -3 3 2.20 3.70 -6 4 -3 122.29 8.20 -6 4 -3 123.59 8.10 6 -4 3 118.69 7.80 6 -4 3 112.89 8.60 -5 5 -3 34.30 4.60 -5 5 -3 34.00 4.40 5 -5 3 36.70 4.90 5 -5 3 21.50 4.50 -4 6 -3 125.09 6.20 -4 6 -3 133.59 8.10 4 -6 3 127.09 8.10 4 -6 3 111.79 7.10 4 -6 3 122.99 8.40 -3 7 -3 18.80 3.40 -3 7 -3 19.50 2.70 3 -7 3 13.90 4.70 3 -7 3 18.60 4.60 -2 8 -3 0.90 1.60 -2 8 -3 0.70 1.90 2 -8 3 0.70 3.30 2 -8 3 3.10 3.80 2 -8 3 0.50 1.50 -1 9 -3 22.60 2.30 -1 9 -3 18.00 3.40 1 -9 3 24.70 5.50 1 -9 3 21.50 4.70 1 -9 3 20.00 1.90 0 10 -3 22.70 2.40 0 10 -3 18.50 4.10 0 -10 3 23.40 2.20 0 -10 3 20.00 4.50 0 -10 3 15.80 5.00 1 11 -3 14.20 4.80 1 11 -3 23.80 3.00 -1 -11 3 14.50 6.40 -1 -11 3 24.10 5.00 2 12 -3 64.89 9.20 2 12 -3 67.89 5.10 -2 -12 3 63.19 6.70 -2 -12 3 64.09 5.30 -2 -12 3 50.69 8.30 3 13 -3 11.40 4.00 -3 -13 3 11.60 3.90 -3 -13 3 10.10 4.40 -3 -13 3 7.20 7.80 4 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11.10 5.50 4 -9 3 12.50 5.60 -3 10 -3 -0.80 2.00 -3 10 -3 3.00 2.60 3 -10 3 1.00 4.60 -2 11 -3 35.30 5.00 -2 11 -3 25.90 3.20 2 -11 3 24.30 6.80 2 -11 3 16.30 5.50 -1 12 -3 5.90 3.20 1 -12 3 2.90 4.40 1 -12 3 9.60 5.80 0 13 -3 151.08 11.20 0 -13 3 178.08 13.50 0 -13 3 152.98 11.10 1 14 -3 48.40 8.30 -1 -14 3 32.40 6.80 -1 -14 3 49.60 9.60 2 15 -3 -2.70 7.80 -2 -15 3 7.60 5.30 -2 -15 3 16.10 7.50 -3 -16 3 -1.90 4.10 -3 -16 3 0.00 7.60 -4 -17 3 1.00 4.30 -4 -17 3 12.90 9.20 -5 -18 3 20.30 10.30 -6 -19 3 5.60 9.60 -12 2 -3 30.50 7.10 12 -2 3 32.40 7.10 -11 3 -3 15.40 6.10 -11 3 -3 9.60 4.80 11 -3 3 24.50 6.70 -10 4 -3 7.60 4.20 -10 4 -3 25.00 6.50 10 -4 3 10.30 5.40 -9 5 -3 100.59 9.80 -9 5 -3 70.29 8.30 9 -5 3 63.49 8.10 9 -5 3 83.99 8.90 -8 6 -3 1.90 3.90 -8 6 -3 5.10 3.50 8 -6 3 4.80 4.70 8 -6 3 -4.60 3.50 -7 7 -3 0.30 3.70 -7 7 -3 4.00 3.20 7 -7 3 -0.90 4.80 7 -7 3 3.40 4.30 -6 8 -3 49.90 6.50 -6 8 -3 45.40 5.80 6 -8 3 45.20 6.80 6 -8 3 49.90 7.80 -5 9 -3 2.80 3.00 -5 9 -3 1.20 2.70 5 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3 -4 4 33.80 4.20 3 -4 4 41.00 3.90 -2 5 -4 7.20 1.70 -2 5 -4 14.10 2.50 -2 5 -4 9.20 1.50 2 -5 4 3.20 3.60 2 -5 4 4.70 2.70 2 -5 4 9.20 1.80 -1 6 -4 16.60 2.80 1 -6 4 18.50 4.10 1 -6 4 17.40 3.80 0 7 -4 95.89 6.30 0 -7 4 100.59 7.00 0 -7 4 93.69 7.10 1 8 -4 56.59 3.40 1 8 -4 56.29 6.40 -1 -8 4 50.99 5.20 -1 -8 4 55.79 3.40 -1 -8 4 56.59 6.30 -1 -8 4 61.09 3.50 2 9 -4 0.00 2.30 -2 -9 4 7.10 5.10 -2 -9 4 0.70 2.60 -2 -9 4 1.90 2.30 3 10 -4 170.68 7.60 -3 -10 4 163.38 8.80 -3 -10 4 170.08 7.80 -3 -10 4 170.98 12.00 -4 -11 4 5.50 3.60 -4 -11 4 9.40 3.70 -4 -11 4 -7.70 5.50 -5 -12 4 14.20 4.20 -5 -12 4 21.50 5.00 -5 -12 4 26.70 8.60 -6 -13 4 45.90 8.80 -6 -13 4 43.80 6.50 -7 -14 4 -10.70 7.10 -7 -14 4 -3.00 4.10 -8 -15 4 -3.60 7.80 -8 -15 4 1.30 4.40 -12 -4 -4 4.30 5.60 12 4 4 8.40 5.70 -11 -3 -4 9.80 6.10 11 3 4 29.50 6.90 -10 -2 -4 7.20 5.10 10 2 4 13.20 5.50 -9 -1 -4 49.60 8.60 -9 -1 -4 46.50 7.70 9 1 4 45.80 7.70 9 1 4 59.29 7.60 -8 0 -4 22.00 6.70 -8 0 -4 17.30 5.40 8 0 4 19.00 5.20 8 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10.70 4.00 1 10 -4 8.10 4.40 1 10 -4 0.60 1.90 -1 -10 4 3.40 2.00 -1 -10 4 2.20 1.80 -1 -10 4 -7.40 5.20 -1 -10 4 -2.80 3.10 2 11 -4 61.79 4.90 2 11 -4 53.39 8.60 -2 -11 4 54.79 8.60 -2 -11 4 61.19 4.80 -2 -11 4 59.69 6.50 3 12 -4 -2.00 3.10 -3 -12 4 3.60 3.70 -3 -12 4 -0.40 6.90 -3 -12 4 1.90 3.00 -4 -13 4 4.40 4.00 -4 -13 4 3.60 3.80 -4 -13 4 9.30 8.30 -5 -14 4 37.20 9.60 -5 -14 4 53.59 6.60 -6 -15 4 -3.10 6.80 -7 -16 4 3.60 9.00 -8 -17 4 -3.10 8.20 -12 -2 -4 1.00 5.00 12 2 4 15.60 5.70 -11 -1 -4 -2.60 5.20 11 1 4 -5.40 4.10 -10 0 -4 6.30 5.10 10 0 4 11.20 5.00 -9 1 -4 9.20 5.80 9 -1 4 -0.50 4.60 9 -1 4 7.60 4.80 -8 2 -4 4.60 4.80 -8 2 -4 7.10 6.60 8 -2 4 -3.20 3.60 8 -2 4 -3.40 3.90 -7 3 -4 16.60 4.00 -7 3 -4 15.60 4.80 -7 3 -4 20.50 7.00 7 -3 4 23.30 4.90 7 -3 4 25.90 5.20 -6 4 -4 37.90 5.30 -6 4 -4 32.40 4.80 6 -4 4 32.20 5.40 6 -4 4 28.20 4.80 -5 5 -4 92.69 6.40 -5 5 -4 83.79 6.50 5 -5 4 87.59 6.60 5 -5 4 89.39 8.00 -4 6 -4 47.20 5.00 -4 6 -4 47.80 4.30 4 -6 4 47.50 5.80 4 -6 4 45.50 6.00 -3 7 -4 3.60 1.80 -3 7 -4 5.60 2.60 3 -7 4 -0.50 3.20 3 -7 4 4.60 4.30 -2 8 -4 21.70 2.20 -2 8 -4 17.90 3.30 -2 8 -4 23.50 2.10 2 -8 4 22.60 2.30 2 -8 4 22.00 5.30 -1 9 -4 35.30 4.70 1 -9 4 36.70 6.30 1 -9 4 43.60 6.10 0 10 -4 -0.30 2.90 0 10 -4 0.70 1.30 0 -10 4 -0.50 4.30 0 -10 4 -0.30 1.40 0 -10 4 -1.00 3.60 0 -10 4 -0.20 1.00 1 11 -4 4.60 4.40 1 11 -4 12.30 2.40 -1 -11 4 13.60 6.30 -1 -11 4 4.40 4.10 -1 -11 4 0.00 1.90 -1 -11 4 3.00 2.20 2 12 -4 -3.30 2.60 2 12 -4 4.60 6.70 -2 -12 4 2.70 6.00 -2 -12 4 -1.00 4.00 -2 -12 4 3.70 2.70 3 13 -4 -1.70 3.30 -3 -13 4 4.00 4.40 -3 -13 4 5.10 6.80 -3 -13 4 4.20 3.40 -4 -14 4 7.40 8.30 -4 -14 4 5.80 4.10 -4 -14 4 8.50 4.70 -5 -15 4 -14.10 6.90 -6 -16 4 12.60 7.90 -7 -17 4 7.20 9.10 -12 -1 -4 3.60 4.80 12 1 4 8.00 5.40 -11 0 -4 15.60 6.60 11 0 4 33.10 6.90 -10 1 -4 12.00 5.60 10 -1 4 16.80 5.40 -9 2 -4 0.10 5.00 9 -2 4 3.10 4.40 9 -2 4 3.70 4.60 -8 3 -4 7.50 6.60 -8 3 -4 -0.90 4.50 -8 3 -4 -4.10 2.60 8 -3 4 1.10 4.10 8 -3 4 2.10 4.40 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15 125.69 9.60 -4 -2 -15 177.68 15.40 -4 -2 -15 188.98 6.30 4 2 15 191.28 10.10 -3 -1 -15 70.39 4.30 3 1 15 71.59 6.80 -2 0 -15 21.40 3.70 2 0 15 20.20 4.30 1 -1 15 35.70 4.80 0 -2 15 35.20 4.80 -1 -3 15 16.40 4.00 -2 -4 15 5.90 3.70 -2 -4 15 8.40 6.50 -3 -5 15 36.70 5.50 -3 -5 15 34.80 7.60 -4 -6 15 2.80 3.80 -4 -6 15 6.00 6.80 -5 -7 15 39.40 8.20 -5 -7 15 11.90 4.80 -6 -8 15 3.50 6.50 -6 -8 15 7.60 4.60 -7 -9 15 24.40 6.20 -8 -10 15 -1.50 5.00 -11 -8 -15 5.90 8.10 -11 -8 -15 9.00 10.40 11 8 15 28.50 8.60 -10 -7 -15 -5.00 6.40 -10 -7 -15 -2.80 9.00 10 7 15 3.90 5.70 -9 -6 -15 6.70 8.90 9 6 15 3.60 5.60 9 6 15 1.50 3.30 -8 -5 -15 114.29 15.20 8 5 15 77.19 9.50 8 5 15 102.89 6.90 -7 -4 -15 2.40 9.70 -7 -4 -15 0.50 1.70 7 4 15 6.00 6.80 7 4 15 3.40 2.80 -6 -3 -15 0.50 8.80 -6 -3 -15 5.00 1.80 6 3 15 8.20 5.80 6 3 15 7.60 2.60 -5 -2 -15 151.78 15.70 -5 -2 -15 164.38 6.60 5 2 15 158.38 10.10 -4 -1 -15 15.90 8.60 -4 -1 -15 8.80 1.90 4 1 15 2.80 4.30 -3 0 -15 8.10 2.20 3 0 15 13.80 4.40 -2 1 -15 34.90 4.20 2 -1 15 38.20 4.90 1 -2 15 72.29 5.90 0 -3 15 5.40 3.20 -1 -4 15 130.49 7.50 -2 -5 15 35.70 5.10 -2 -5 15 27.60 7.20 -3 -6 15 14.40 4.20 -3 -6 15 4.60 7.00 -4 -7 15 34.90 5.80 -4 -7 15 32.40 8.30 -5 -8 15 2.80 4.10 -5 -8 15 -0.80 6.10 -6 -9 15 4.20 7.00 -6 -9 15 4.80 4.30 -7 -10 15 -5.60 7.00 -12 -8 -15 -2.40 6.60 -11 -7 -15 14.50 10.90 -11 -7 -15 9.80 7.90 11 7 15 13.10 7.40 -10 -6 -15 -9.20 6.40 -10 -6 -15 -2.20 9.10 10 6 15 6.20 6.30 10 6 15 -0.70 5.00 -9 -5 -15 7.20 9.00 9 5 15 4.60 5.50 9 5 15 0.50 3.10 -8 -4 -15 2.80 2.30 -8 -4 -15 14.30 9.90 8 4 15 -0.80 6.30 8 4 15 -3.00 2.90 -7 -3 -15 1.30 10.00 -7 -3 -15 8.10 2.60 7 3 15 15.10 6.60 7 3 15 6.50 3.20 -6 -2 -15 14.00 9.10 -6 -2 -15 23.00 3.10 6 2 15 32.50 6.50 6 2 15 28.60 3.80 -5 -1 -15 -0.60 7.30 -5 -1 -15 4.70 1.80 5 1 15 9.60 5.20 -4 0 -15 183.48 7.30 4 0 15 175.48 9.20 -3 1 -15 58.19 4.90 3 -1 15 68.59 6.10 3 -1 15 43.40 7.50 -2 2 -15 3.20 2.90 2 -2 15 0.00 3.20 2 -2 15 -1.80 5.40 -1 3 -15 27.00 5.40 1 -3 15 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6.20 3 -2 15 5.70 3.80 -2 3 -15 59.89 5.80 2 -3 15 57.39 5.20 2 -3 15 47.10 7.80 -1 4 -15 32.40 5.70 1 -4 15 43.60 4.60 1 -4 15 55.19 8.50 0 -5 15 23.90 7.30 0 -5 15 26.70 4.10 0 -5 15 18.20 6.60 -1 -6 15 15.60 6.90 -1 -6 15 13.00 6.70 -1 -6 15 16.70 3.80 -2 -7 15 1.50 6.70 -2 -7 15 -2.10 3.00 -2 -7 15 0.30 7.20 -3 -8 15 11.00 4.10 -3 -8 15 13.00 8.10 -3 -8 15 21.60 7.30 -4 -9 15 20.50 7.70 -4 -9 15 8.90 6.00 -5 -10 15 7.20 7.40 -6 -11 15 3.80 7.30 -7 -12 15 18.60 8.40 -12 -6 -15 -11.80 9.20 -12 -6 -15 5.70 6.90 12 6 15 7.00 6.50 -11 -5 -15 31.10 8.80 -11 -5 -15 19.00 10.10 11 5 15 29.30 7.90 -10 -4 -15 6.40 3.00 -10 -4 -15 -0.80 8.50 -10 -4 -15 -2.60 6.10 10 4 15 12.60 4.30 10 4 15 12.40 6.50 -9 -3 -15 0.90 6.20 -9 -3 -15 6.80 2.90 9 3 15 -2.00 5.60 9 3 15 8.80 3.80 -8 -2 -15 -0.10 2.10 -8 -2 -15 5.20 9.70 8 2 15 -0.50 5.80 8 2 15 -5.30 2.90 -7 -1 -15 10.00 9.80 -7 -1 -15 2.70 2.20 7 1 15 0.30 3.00 7 1 15 -4.60 5.50 -6 0 -15 10.40 9.00 -6 0 -15 7.30 2.30 6 0 15 5.90 6.60 6 0 15 11.90 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0.0209 0.0007 0 2 29 0.7321 -0.0096 0 3 0 -32.2088 0.0207 0 3 1 -24.1195 -0.0213 0 3 2 49.5481 0.0139 0 3 3 -16.4220 -0.0036 0 3 4 -23.1099 -0.0112 0 3 5 27.8119 -0.0020 0 3 6 -8.2125 0.0000 0 3 7 -10.5297 0.0052 0 3 8 14.0522 -0.0100 0 3 9 -4.4429 0.0088 0 3 10 -4.1522 0.0017 0 3 11 5.3895 -0.0080 0 3 12 -2.7327 0.0032 0 3 13 -0.5946 0.0003 0 3 14 3.5910 0.0041 0 3 15 -1.3969 0.0025 0 3 16 -1.3107 -0.0016 0 3 17 2.3614 -0.0001 0 3 18 0.1390 -0.0010 0 3 19 -1.6759 0.0028 0 3 20 0.7798 0.0011 0 3 21 0.4576 -0.0030 0 3 22 -1.1243 0.0001 0 3 23 -0.5469 0.0003 0 3 24 0.3030 0.0014 0 3 25 -0.2792 -0.0015 0 3 26 -0.3678 -0.0007 0 3 27 0.3475 -0.0006 0 3 28 -0.1237 0.0015 0 3 29 0.7863 0.0001 0 4 0 24.5718 0.0381 0 4 1 -39.9670 0.0110 0 4 2 7.4170 -0.0069 0 4 3 27.0467 0.0175 0 4 5 0.9706 0.0049 0 4 6 14.1301 -0.0104 0 4 7 -12.7101 0.0002 0 4 8 2.8362 0.0007 0 4 9 5.7293 -0.0099 0 4 10 -5.9821 0.0058 0 4 11 2.4264 -0.0043 0 4 12 0.5366 -0.0054 0 4 13 -3.6182 -0.0016 0 4 14 2.6878 0.0010 0 4 15 1.1833 0.0032 0 4 16 -2.5845 0.0000 0 4 17 0.8540 0.0003 0 4 18 1.7255 -0.0001 0 4 19 -1.0590 -0.0004 0 4 20 -0.0853 0.0032 0 4 21 0.8873 0.0024 0 4 22 0.3579 -0.0013 0 4 23 -0.1266 -0.0012 0 4 24 -0.5791 0.0026 0 4 25 0.2229 0.0016 0 4 26 -0.2407 -0.0039 0 4 27 -0.1941 -0.0007 0 4 28 -0.2224 -0.0017 0 4 29 -0.3061 0.0003 0 5 0 27.0901 -0.0306 0 5 1 -1.3663 0.0346 0 5 2 -25.0475 -0.0093 0 5 3 19.5685 0.0109 0 5 4 3.6131 0.0049 0 5 5 -16.3426 0.0037 0 5 6 9.2049 0.0170 0 5 7 0.0532 -0.0065 0 5 8 -6.3768 0.0076 0 5 9 5.9817 0.0018 0 5 10 -1.8038 -0.0010 0 5 11 -1.3028 0.0029 0 5 12 3.6059 -0.0030 0 5 13 -3.1734 -0.0053 0 5 14 -0.9379 -0.0040 0 5 15 3.3535 0.0019 0 5 16 -1.1495 -0.0001 0 5 17 -1.8598 -0.0009 0 5 18 1.6792 -0.0005 0 5 19 0.0391 -0.0006 0 5 20 -1.2646 -0.0013 0 5 21 0.0991 0.0020 0 5 22 0.1356 0.0029 0 5 23 0.7769 -0.0019 0 5 24 -0.5047 -0.0002 0 5 25 -0.6195 0.0062 0 5 26 0.5182 0.0014 0 5 27 -0.1892 -0.0029 0 5 28 0.3293 0.0005 0 5 29 -0.3118 -0.0008 0 6 0 -2.7533 -0.0501 0 6 1 19.8157 -0.0038 0 6 2 -13.3585 0.0060 0 6 3 -5.5853 -0.0139 0 6 4 14.7483 0.0076 0 6 5 -6.5868 -0.0176 0 6 6 -3.3097 0.0043 0 6 7 5.7292 0.0090 0 6 8 -5.0682 -0.0045 0 6 9 0.8454 0.0049 0 6 10 1.9509 0.0044 0 6 11 -3.8527 0.0047 0 6 12 2.6031 0.0037 0 6 13 0.8375 0.0025 0 6 14 -3.5894 -0.0050 0 6 15 1.4829 -0.0013 0 6 16 2.3393 0.0020 0 6 17 -1.6988 -0.0000 0 6 18 -0.2112 -0.0001 0 6 19 1.8737 -0.0008 0 6 20 -0.4753 0.0007 0 6 21 -0.5835 -0.0015 0 6 22 -0.2579 0.0016 0 6 23 0.5414 0.0014 0 6 24 0.7727 -0.0031 0 6 25 -1.4743 0.0014 0 6 26 -0.2339 0.0065 0 6 27 -0.1218 0.0008 0 6 28 -0.2891 -0.0021 0 6 29 0.4802 0.0031 0 7 0 -15.0154 0.0072 0 7 1 8.1262 -0.0266 0 7 2 6.0200 0.0154 0 7 3 -11.4809 -0.0049 0 7 4 4.4875 0.0059 0 7 5 4.2332 0.0034 0 7 6 -5.2480 -0.0166 0 7 7 3.3971 0.0020 0 7 8 -0.2799 0.0023 0 7 9 -2.4621 -0.0056 0 7 10 3.6128 -0.0041 0 7 11 -2.0231 0.0028 0 7 12 -1.4943 0.0004 0 7 13 2.9941 0.0041 0 7 14 -1.7606 0.0025 0 7 15 -2.3712 -0.0051 0 7 16 1.7255 -0.0001 0 7 17 0.6967 -0.0004 0 7 18 -1.8645 0.0012 0 7 19 0.6373 -0.0017 0 7 20 1.3584 -0.0017 0 7 21 -0.4269 0.0011 0 7 22 -0.2963 -0.0010 0 7 23 -0.0967 0.0013 0 7 24 1.7223 -0.0004 0 7 25 0.2904 -0.0015 0 7 26 -0.9952 0.0026 0 7 27 0.3277 0.0057 0 7 28 -0.7070 -0.0006 0 7 29 0.4391 -0.0034 0 8 0 -3.8132 0.0249 0 8 1 -5.8568 -0.0215 0 8 2 8.5081 -0.0086 0 8 3 -2.4115 0.0017 0 8 4 -3.7513 -0.0056 0 8 5 4.5265 0.0085 0 8 6 -2.5544 0.0019 0 8 7 -0.1730 -0.0055 0 8 8 2.6520 0.0012 0 8 9 -3.3681 0.0086 0 8 10 1.3292 -0.0037 0 8 11 2.0796 -0.0027 0 8 12 -2.5847 0.0020 0 8 13 1.3175 -0.0018 0 8 14 1.7843 0.0061 0 8 15 -1.9065 0.0006 0 8 16 -0.7821 -0.0024 0 8 17 1.6456 -0.0012 0 8 18 -0.4310 -0.0004 0 8 19 -1.7102 0.0032 0 8 20 1.0316 -0.0033 0 8 21 0.3558 -0.0024 0 8 22 -0.6947 -0.0000 0 8 23 -0.7442 -0.0013 0 8 24 0.1252 -0.0021 0 8 25 1.6018 -0.0021 0 8 26 -0.3121 0.0003 0 8 27 -0.0182 0.0025 0 8 28 -0.1578 0.0062 0 9 0 5.5258 0.0274 0 9 1 -5.4264 0.0093 0 9 2 0.8332 -0.0120 0 9 3 3.4789 -0.0012 0 9 4 -3.2449 -0.0054 0 9 5 2.1692 -0.0039 0 9 6 0.4121 -0.0072 0 9 7 -2.8795 0.0005 0 9 8 3.3421 -0.0104 0 9 9 -0.6675 -0.0033 0 9 10 -2.7059 0.0075 0 9 11 2.3600 -0.0055 0 9 12 -0.6657 0.0006 0 9 13 -1.4711 -0.0015 0 9 14 1.8242 0.0003 0 9 15 0.3804 0.0055 0 9 16 -1.5006 -0.0001 0 9 17 0.4470 -0.0004 0 9 18 1.7200 -0.0033 0 9 19 -1.2381 0.0018 0 9 20 -0.4755 0.0046 0 9 21 1.5042 -0.0020 0 9 22 -0.3134 -0.0013 0 9 23 -0.4103 0.0011 0 9 24 -0.7166 -0.0009 0 9 25 0.2139 -0.0056 0 9 26 0.8061 -0.0020 0 9 27 -0.0780 -0.0003 0 9 28 0.0211 0.0011 0 10 0 2.7261 -0.0023 0 10 1 0.3735 0.0305 0 10 2 -2.6679 0.0020 0 10 3 2.0478 0.0087 0 10 4 -1.2660 0.0018 0 10 5 -0.3848 0.0144 0 10 6 2.9006 0.0021 0 10 7 -3.1977 -0.0044 0 10 8 0.1946 0.0074 0 10 9 3.5732 -0.0123 0 10 10 -2.3895 -0.0006 0 10 11 -0.1757 0.0003 0 10 12 1.6229 -0.0050 0 10 13 -1.6496 -0.0013 0 10 14 -0.1547 -0.0048 0 10 15 1.4042 0.0022 0 10 16 -0.7276 0.0021 0 10 17 -1.5649 0.0006 0 10 18 1.3701 -0.0016 0 10 19 0.5964 -0.0048 0 10 20 -1.9991 0.0013 0 10 21 0.9604 0.0028 0 10 22 0.8388 -0.0016 0 10 23 -0.6891 -0.0014 0 10 24 0.2305 0.0028 0 10 25 -0.6223 -0.0013 0 10 26 -0.0480 -0.0061 0 10 27 0.6144 0.0003 0 11 0 -0.8977 -0.0453 0 11 1 1.3824 0.0068 0 11 2 -0.8881 0.0002 0 11 3 0.5912 -0.0022 0 11 4 0.2664 -0.0011 0 11 5 -2.3233 -0.0060 0 11 6 2.5653 0.0213 0 11 7 0.0215 -0.0019 0 11 8 -4.1119 0.0059 0 11 9 2.6275 0.0092 0 11 10 1.1652 -0.0024 0 11 11 -2.4523 0.0052 0 11 12 1.2823 -0.0002 0 11 13 0.3543 0.0011 0 11 14 -1.4077 -0.0039 0 11 15 0.8901 -0.0020 0 11 16 1.4599 0.0028 0 11 17 -1.4163 0.0015 0 11 18 -0.6658 0.0021 0 11 19 2.2397 -0.0008 0 11 20 -1.0236 -0.0016 0 11 21 -1.2707 0.0005 0 11 22 1.7573 0.0023 0 11 23 -0.4464 -0.0013 0 11 24 -0.3297 -0.0017 0 11 25 0.5166 0.0027 0 11 26 -0.9641 -0.0038 0 12 0 -0.5957 -0.0092 0 12 1 0.0670 -0.0212 0 12 2 -0.3555 0.0118 0 12 3 0.1967 -0.0113 0 12 4 1.6083 0.0073 0 12 5 -1.7439 -0.0156 0 12 6 -0.0180 -0.0081 0 12 7 3.6612 0.0092 0 12 8 -2.7372 -0.0082 0 12 9 -1.8975 0.0023 0 12 10 3.4621 0.0011 0 12 11 -1.0734 0.0034 0 12 12 -1.5065 0.0015 0 12 13 1.2051 0.0036 0 12 14 -0.8983 0.0023 0 12 15 -1.4745 -0.0045 0 12 16 1.2085 0.0011 0 12 17 0.8204 0.0009 0 12 18 -2.1342 0.0016 0 12 19 0.7213 -0.0003 0 12 20 1.7010 0.0017 0 12 21 -1.8725 0.0016 0 12 22 0.4177 0.0001 0 12 23 1.4124 0.0044 0 12 24 -0.7838 0.0008 0 12 25 0.5599 0.0006 0 12 26 0.2736 0.0022 0 13 0 -0.0484 0.0344 0 13 1 0.1358 -0.0228 0 13 2 -0.5620 0.0044 0 13 3 -0.8685 -0.0002 0 13 4 1.4132 -0.0026 0 13 5 -0.0516 0.0158 0 13 6 -2.5768 -0.0122 0 13 7 2.5308 -0.0011 0 13 8 1.9289 0.0037 0 13 9 -3.7876 -0.0023 0 13 10 1.0730 -0.0044 0 13 11 2.8619 -0.0004 0 13 12 -1.4944 0.0007 0 13 13 0.0031 -0.0028 0 13 14 1.0384 0.0061 0 13 15 -1.1177 -0.0014 0 13 16 -1.1325 -0.0016 0 13 17 1.4630 0.0004 0 13 18 -0.2625 0.0013 0 13 19 -1.9950 0.0000 0 13 20 1.2886 -0.0046 0 13 21 0.0145 0.0043 0 13 22 -1.5506 0.0001 0 13 23 0.9639 -0.0020 0 13 24 0.4610 0.0044 0 13 25 -0.2586 0.0022 0 14 0 -0.1345 0.0220 0 14 1 0.5212 0.0055 0 14 2 0.2433 -0.0150 0 14 3 -1.1220 0.0065 0 14 4 0.3721 -0.0169 0 14 5 1.8362 0.0003 0 14 6 -2.1162 0.0085 0 14 7 -1.2847 -0.0073 0 14 8 3.3952 -0.0039 0 14 9 -0.9433 0.0049 0 14 10 -3.1224 0.0023 0 14 11 2.2278 -0.0045 0 14 12 1.1492 0.0033 0 14 13 -1.0469 -0.0043 0 14 14 0.5083 -0.0000 0 14 15 0.7167 0.0038 0 14 16 -0.8645 -0.0023 0 14 17 -0.4598 -0.0001 0 14 18 1.5335 -0.0022 0 14 19 -0.7072 0.0052 0 14 20 -0.8576 -0.0031 0 14 21 0.8752 -0.0041 0 14 22 -0.6888 0.0073 0 14 23 -0.6913 -0.0024 0 14 24 0.4695 -0.0031 0 15 0 -0.5109 -0.0034 0 15 1 0.0351 0.0261 0 15 2 0.7366 -0.0023 0 15 3 -0.5195 0.0083 0 15 4 -1.2300 0.0035 0 15 5 1.9457 -0.0115 0 15 6 0.7584 0.0005 0 15 7 -2.6570 0.0050 0 15 8 1.0036 -0.0065 0 15 9 2.5742 -0.0110 0 15 10 -2.1655 0.0044 0 15 11 -1.1348 -0.0011 0 15 12 1.8111 -0.0015 0 15 13 0.2419 0.0006 0 15 14 -0.2654 -0.0051 0 15 15 0.1009 0.0030 0 15 16 0.4344 0.0001 0 15 17 -0.7949 0.0014 0 15 18 -0.1467 -0.0042 0 15 19 1.0046 -0.0032 0 15 20 -0.6082 0.0058 0 15 21 -0.3560 -0.0078 0 15 22 0.0185 -0.0006 0 16 0 0.0919 -0.0240 0 16 1 -0.7415 0.0102 0 16 2 0.3567 0.0052 0 16 3 0.7542 0.0034 0 16 4 -1.5756 0.0112 0 16 5 -0.4631 0.0032 0 16 6 2.1720 0.0018 0 16 7 -1.1133 0.0026 0 16 8 -1.7717 0.0127 0 16 9 1.7111 -0.0042 0 16 10 0.6283 -0.0079 0 16 11 -1.6432 0.0045 0 16 12 0.1501 -0.0011 0 16 13 0.6621 -0.0003 0 16 14 0.6366 -0.0044 0 16 15 0.2429 -0.0016 0 16 16 -0.0466 0.0009 0 16 17 0.6282 0.0020 0 16 18 -0.5162 0.0048 0 16 19 0.2568 -0.0079 0 16 20 0.7779 0.0002 0 16 21 -0.1120 0.0022 0 17 0 1.0945 -0.0183 0 17 1 -0.3097 -0.0120 0 17 2 -0.7349 0.0016 0 17 3 0.8750 -0.0068 0 17 4 0.4946 0.0057 0 17 5 -1.7292 -0.0063 0 17 6 0.9663 0.0026 0 17 7 1.1790 0.0004 0 17 8 -1.5234 0.0018 0 17 9 -0.2630 0.0138 0 17 10 0.7767 -0.0042 0 17 11 -0.6558 -0.0015 0 17 12 -0.4813 0.0068 0 17 13 -0.2018 0.0033 0 17 14 -0.3381 -0.0023 0 17 15 0.9292 -0.0032 0 17 16 -0.1313 0.0001 0 17 17 -0.0577 -0.0018 0 17 18 0.3983 0.0068 0 17 19 -0.2991 0.0031 0 18 0 0.4155 0.0152 0 18 1 0.6676 -0.0153 0 18 2 -0.5038 0.0027 0 18 3 -0.8774 -0.0086 0 18 4 1.1050 0.0056 0 18 5 -0.3527 0.0035 0 18 6 -0.9233 -0.0136 0 18 7 1.3025 0.0040 0 18 8 -0.0161 -0.0052 0 18 9 -0.4139 0.0015 0 18 10 0.5050 0.0050 0 18 11 -0.2983 -0.0079 0 18 12 -0.3541 -0.0001 0 18 13 0.4853 0.0084 0 18 14 -0.8052 0.0020 0 18 15 -0.3144 -0.0041 0 18 16 0.7985 0.0008 0 18 17 -0.3409 -0.0017 0 19 0 -0.4110 0.0159 0 19 1 0.2914 0.0013 0 19 2 0.7193 -0.0035 0 19 3 -0.7266 -0.0025 0 19 4 -0.5525 -0.0111 0 19 5 0.7927 0.0164 0 19 6 -0.7217 -0.0020 0 19 7 -0.0274 -0.0078 0 19 8 0.3406 0.0048 0 19 9 -0.3457 -0.0012 0 19 10 0.4466 0.0049 0 19 11 0.0622 -0.0017 0 19 12 -0.8242 -0.0091 0 19 13 0.2724 0.0022 0 19 14 0.5338 0.0075 0 20 0 -0.3219 -0.0101 0 20 1 -0.1248 0.0111 0 20 2 0.2188 0.0001 0 20 3 0.6997 0.0041 0 20 4 -0.7978 -0.0127 0 20 5 -0.0983 -0.0069 0 20 6 0.3048 0.0121 0 20 7 -0.1804 -0.0066 0 20 8 0.1245 -0.0059 0 20 9 -0.2504 0.0010 0 20 10 0.2009 0.0044 1 -19 0 -0.5016 0.0039 1 -19 1 0.2589 0.0020 1 -19 2 0.0173 0.0039 1 -19 3 0.5407 -0.0021 1 -19 4 -0.7727 -0.0070 1 -19 5 0.5188 0.0014 1 -18 0 -0.9500 0.0076 1 -18 1 -0.0652 -0.0087 1 -18 2 -0.5896 0.0060 1 -18 3 0.5668 0.0037 1 -18 4 -0.1224 -0.0034 1 -18 5 -0.9567 -0.0080 1 -18 6 1.1034 0.0026 1 -18 7 -0.2855 0.0059 1 -18 8 -0.8202 -0.0082 1 -18 9 0.6623 -0.0013 1 -17 0 -0.4927 0.0216 1 -17 1 0.0172 0.0016 1 -17 2 -0.2813 -0.0055 1 -17 3 -0.2228 0.0111 1 -17 4 0.7702 0.0023 1 -17 5 -0.8257 0.0019 1 -17 6 0.0387 -0.0083 1 -17 7 0.4222 0.0059 1 -17 8 -1.0440 0.0054 1 -17 9 -0.2619 -0.0081 1 -17 10 0.2235 0.0000 1 -17 11 0.1716 -0.0034 1 -17 12 0.4960 -0.0053 1 -16 0 0.0521 -0.0123 1 -16 1 -0.5144 0.0208 1 -16 2 0.0880 -0.0101 1 -16 3 -0.3881 0.0042 1 -16 4 0.5546 0.0048 1 -16 5 -0.1839 0.0055 1 -16 6 -0.0111 0.0061 1 -16 7 0.7649 -0.0062 1 -16 8 -0.7245 0.0097 1 -16 9 -0.3469 0.0044 1 -16 10 0.3761 -0.0021 1 -16 11 -0.2139 0.0023 1 -16 12 0.3775 -0.0033 1 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0.0021 1 -13 5 1.6825 0.0035 1 -13 6 0.0920 -0.0019 1 -13 7 -1.6986 -0.0035 1 -13 8 2.5897 -0.0010 1 -13 9 0.3364 0.0052 1 -13 10 -1.8273 -0.0066 1 -13 11 1.1930 -0.0006 1 -13 12 0.4804 0.0044 1 -13 13 -1.3777 -0.0021 1 -13 14 0.9488 0.0024 1 -13 15 1.0172 0.0017 1 -13 16 -1.8188 0.0020 1 -13 17 -0.8019 -0.0016 1 -13 18 -0.0097 -0.0025 1 -13 19 0.6038 0.0022 1 -12 0 -0.4697 0.0225 1 -12 1 -0.6078 -0.0054 1 -12 2 1.3924 -0.0041 1 -12 3 0.1245 0.0005 1 -12 4 -1.8318 -0.0041 1 -12 5 0.2448 0.0040 1 -12 6 1.8519 -0.0054 1 -12 7 -2.2438 0.0031 1 -12 8 0.0091 -0.0064 1 -12 9 2.4379 0.0017 1 -12 10 -1.9569 0.0056 1 -12 11 -0.7824 -0.0088 1 -12 12 1.8093 0.0019 1 -12 13 -0.8084 -0.0020 1 -12 14 -0.6658 -0.0012 1 -12 15 2.2789 0.0037 1 -12 16 -0.0379 -0.0002 1 -12 17 -0.5210 0.0027 1 -12 18 0.1663 0.0020 1 -12 19 -0.8791 -0.0008 1 -12 20 1.7768 0.0041 1 -12 21 -0.4753 0.0025 1 -11 0 1.5847 0.0112 1 -11 1 -2.3805 0.0246 1 -11 2 0.6771 -0.0074 1 -11 3 2.4877 0.0119 1 -11 4 -1.7423 -0.0036 1 -11 5 -1.6554 0.0096 1 -11 6 2.7387 0.0010 1 -11 7 -0.0237 -0.0054 1 -11 8 -2.4633 0.0047 1 -11 9 2.5635 -0.0096 1 -11 10 0.7761 0.0059 1 -11 11 -2.6821 -0.0005 1 -11 12 0.8640 -0.0045 1 -11 13 1.1124 0.0004 1 -11 14 -2.4139 -0.0055 1 -11 15 0.2069 0.0011 1 -11 16 1.3024 0.0001 1 -11 17 -1.2547 -0.0032 1 -11 18 1.0159 0.0007 1 -11 19 -0.9233 0.0001 1 -11 20 -0.2500 -0.0019 1 -11 21 3.1989 0.0058 1 -11 22 -1.6066 0.0010 1 -10 0 3.5880 -0.0491 1 -10 1 -0.4831 0.0198 1 -10 2 -4.1472 -0.0030 1 -10 3 3.3877 -0.0032 1 -10 4 1.6516 0.0042 1 -10 5 -4.3580 -0.0047 1 -10 6 0.6627 0.0200 1 -10 7 3.2316 -0.0013 1 -10 8 -2.8523 0.0049 1 -10 9 -0.6734 0.0040 1 -10 10 3.4302 -0.0015 1 -10 11 -1.1566 0.0067 1 -10 12 -1.6399 -0.0018 1 -10 13 2.7182 0.0012 1 -10 14 0.2931 -0.0026 1 -10 15 -2.2508 -0.0014 1 -10 16 1.6253 0.0024 1 -10 17 -0.3344 0.0005 1 -10 18 -0.7507 -0.0019 1 -10 19 1.0280 -0.0002 1 -10 20 -2.8628 -0.0016 1 -10 21 1.0874 -0.0016 1 -10 22 1.9355 0.0030 1 -10 23 -2.4154 -0.0029 1 -9 0 -0.8552 -0.0264 1 -9 1 6.5736 -0.0242 1 -9 2 -4.7045 0.0151 1 -9 3 -3.0053 -0.0173 1 -9 4 6.3519 -0.0002 1 -9 5 -1.6884 -0.0173 1 -9 6 -4.7849 -0.0075 1 -9 7 3.8039 0.0081 1 -9 8 1.1648 -0.0055 1 -9 9 -4.1826 0.0029 1 -9 10 1.4326 0.0003 1 -9 11 2.1596 0.0049 1 -9 12 -2.9220 0.0027 1 -9 13 -0.4437 0.0025 1 -9 14 3.1352 0.0005 1 -9 15 -1.3719 -0.0025 1 -9 16 -1.0553 0.0003 1 -9 17 2.1741 0.0003 1 -9 18 -1.1009 0.0031 1 -9 19 1.2732 -0.0010 1 -9 20 0.1731 0.0007 1 -9 21 -2.3778 0.0010 1 -9 22 2.2770 0.0016 1 -9 23 -0.2056 0.0004 1 -9 24 -1.5047 -0.0008 1 -8 0 -9.2701 0.0383 1 -8 1 5.3541 -0.0256 1 -8 2 5.6771 0.0099 1 -8 3 -8.8398 0.0090 1 -8 4 1.8758 -0.0002 1 -8 5 6.6350 0.0072 1 -8 6 -5.4662 -0.0152 1 -8 7 -1.9791 -0.0036 1 -8 8 5.4355 -0.0003 1 -8 9 -1.5569 -0.0044 1 -8 10 -3.1238 -0.0063 1 -8 11 3.1827 -0.0014 1 -8 12 0.5422 0.0008 1 -8 13 -3.3296 0.0002 1 -8 14 1.4641 0.0039 1 -8 15 2.2430 -0.0022 1 -8 16 -3.0071 0.0007 1 -8 17 0.2674 -0.0029 1 -8 18 0.7515 -0.0005 1 -8 19 -1.3434 0.0020 1 -8 20 1.9242 -0.0041 1 -8 21 -1.1621 -0.0005 1 -8 22 -0.5458 0.0017 1 -8 23 1.7577 0.0002 1 -7 0 -4.7159 0.0253 1 -7 1 -9.2237 -0.0005 1 -7 2 11.9588 -0.0161 1 -7 3 -0.9242 0.0078 1 -7 4 -9.3601 -0.0023 1 -7 5 7.3545 0.0070 1 -7 6 2.8293 0.0054 1 -7 7 -7.0576 -0.0032 1 -7 8 1.8817 -0.0019 1 -7 9 4.4943 0.0055 1 -7 10 -3.7555 0.0003 1 -7 11 -1.1582 -0.0055 1 -7 12 3.6955 0.0005 1 -7 13 -1.4386 -0.0038 1 -7 14 -2.2074 0.0022 1 -7 15 3.7265 0.0008 1 -7 16 0.5369 -0.0006 1 -7 17 -2.4453 0.0022 1 -7 18 1.8437 -0.0030 1 -7 19 -0.7498 0.0030 1 -7 20 -0.3336 0.0013 1 -7 21 1.2491 -0.0039 1 -7 22 -1.5227 -0.0001 1 -6 0 14.6390 0.0077 1 -6 1 -15.0278 0.0215 1 -6 2 -1.0757 -0.0078 1 -6 3 13.9846 0.0030 1 -6 4 -9.3858 -0.0010 1 -6 5 -4.2988 -0.0007 1 -6 6 9.5005 -0.0023 1 -6 7 -2.5567 0.0021 1 -6 8 -5.6636 -0.0042 1 -6 9 4.6862 -0.0076 1 -6 10 2.0484 0.0073 1 -6 11 -4.7662 -0.0013 1 -6 12 1.1084 -0.0005 1 -6 13 2.5011 -0.0015 1 -6 14 -3.7224 -0.0031 1 -6 15 -0.0062 0.0029 1 -6 16 3.7873 -0.0020 1 -6 17 -1.9539 -0.0000 1 -6 18 -0.4125 -0.0008 1 -6 19 1.7638 -0.0020 1 -6 20 -1.3913 0.0032 1 -6 21 1.1133 0.0015 1 -5 0 18.2842 -0.0259 1 -5 1 5.5866 0.0239 1 -5 2 -20.6859 -0.0012 1 -5 3 11.4708 0.0059 1 -5 4 8.0196 0.0069 1 -5 5 -13.5265 0.0074 1 -5 6 3.5035 0.0100 1 -5 7 7.4314 -0.0024 1 -5 8 -6.0437 0.0118 1 -5 9 -2.4894 -0.0056 1 -5 10 5.8873 -0.0042 1 -5 11 -0.8433 0.0043 1 -5 12 -4.0140 -0.0011 1 -5 13 3.4546 0.0007 1 -5 14 -0.0743 -0.0048 1 -5 15 -4.0092 0.0002 1 -5 16 2.9406 0.0021 1 -5 17 1.4582 -0.0008 1 -5 18 -2.7234 -0.0014 1 -5 19 1.4474 -0.0018 1 -4 0 -13.4649 -0.0425 1 -4 1 29.4046 -0.0101 1 -4 2 -12.2600 0.0047 1 -4 3 -15.5681 -0.0165 1 -4 4 19.3575 0.0036 1 -4 5 -3.3223 -0.0125 1 -4 6 -11.2715 0.0107 1 -4 7 8.5330 0.0017 1 -4 8 2.9628 0.0009 1 -4 9 -6.9155 0.0134 1 -4 10 0.8716 -0.0028 1 -4 11 5.3338 0.0035 1 -4 12 -3.6301 0.0034 1 -4 13 -1.5630 0.0049 1 -4 14 3.9489 -0.0009 1 -4 15 -3.4094 -0.0031 1 -4 16 -1.6745 0.0017 1 -4 17 4.0325 0.0030 1 -4 18 -1.3882 0.0007 1 -4 19 -0.8023 -0.0004 1 -4 20 1.7264 0.0018 1 -4 21 -1.5447 -0.0023 1 -3 0 -38.5619 0.0290 1 -3 1 9.3539 -0.0334 1 -3 2 26.8547 0.0125 1 -3 3 -26.6366 -0.0085 1 -3 4 -0.7859 0.0013 1 -3 5 17.7847 -0.0038 1 -3 6 -11.9007 -0.0169 1 -3 7 -4.9575 0.0068 1 -3 8 8.9731 -0.0095 1 -3 9 -1.2878 -0.0001 1 -3 10 -6.0121 0.0006 1 -3 11 3.5889 -0.0017 1 -3 12 3.0264 0.0002 1 -3 13 -4.7685 0.0040 1 -3 14 1.8899 0.0059 1 -3 15 1.7761 -0.0026 1 -3 16 -4.9925 -0.0000 1 -3 17 1.5281 0.0004 1 -3 18 1.9395 0.0036 1 -3 19 -2.5880 -0.0020 1 -3 20 1.0259 0.0005 1 -3 21 -0.0025 0.0016 1 -3 22 -1.8780 -0.0015 1 -3 23 0.4770 0.0016 1 -2 0 -2.2512 0.0448 1 -2 1 -40.2267 0.0035 1 -2 2 32.1546 -0.0126 1 -2 3 9.1933 0.0049 1 -2 4 -27.9552 -0.0081 1 -2 5 13.1482 0.0170 1 -2 6 9.1128 -0.0064 1 -2 7 -13.0366 -0.0049 1 -2 8 1.2737 0.0035 1 -2 9 6.9113 -0.0023 1 -2 10 -3.7430 -0.0014 1 -2 11 -3.7311 -0.0043 1 -2 12 4.8960 -0.0014 1 -2 13 -0.3738 -0.0052 1 -2 14 -3.2754 0.0053 1 -2 15 4.1040 0.0003 1 -2 16 -1.5474 -0.0010 1 -2 17 -3.1661 0.0003 1 -2 18 3.3548 0.0012 1 -2 19 -0.4862 0.0041 1 -2 20 -1.0943 -0.0032 1 -2 21 1.5438 0.0008 1 -2 22 -1.1357 -0.0012 1 -2 23 -1.5772 -0.0020 1 -2 24 0.4380 -0.0007 1 -2 25 1.1261 0.0011 1 -1 1 -31.9333 0.0317 1 -1 2 -20.8002 -0.0011 1 -1 4 -11.3257 -0.0123 1 -1 5 -17.1941 -0.0017 1 -1 6 17.0933 0.0110 1 -1 7 -0.3826 -0.0051 1 -1 8 -9.2920 -0.0041 1 -1 9 4.2906 0.0008 1 -1 10 4.1006 0.0057 1 -1 11 -4.4080 -0.0043 1 -1 12 -0.6090 0.0004 1 -1 13 4.1598 -0.0038 1 -1 14 -2.9892 -0.0033 1 -1 15 -0.1413 0.0041 1 -1 16 3.1996 -0.0038 1 -1 17 -3.9039 0.0009 1 -1 18 -0.3482 -0.0027 1 -1 19 2.3306 0.0030 1 -1 20 -1.5060 0.0035 1 -1 21 0.4118 -0.0010 1 -1 22 1.1882 0.0017 1 -1 23 -1.0315 0.0001 1 -1 24 -1.2490 -0.0003 1 -1 25 1.5639 -0.0010 1 -1 26 1.4217 0.0002 1 -1 27 -0.8808 -0.0045 1 0 0 23.8506 -0.0296 1 0 1 33.0241 -0.0017 1 0 2 -45.6268 0.0150 1 0 3 6.7838 0.0108 1 0 4 28.4218 -0.0022 1 0 5 -20.1571 -0.0097 1 0 6 -3.0170 0.0034 1 0 7 12.4749 0.0062 1 0 8 -4.9906 0.0013 1 0 9 -4.7094 -0.0093 1 0 10 4.3138 0.0039 1 0 11 1.3737 0.0039 1 0 12 -3.7265 -0.0036 1 0 13 2.0021 0.0025 1 0 14 1.8250 -0.0065 1 0 15 -2.9793 0.0016 1 0 16 2.8468 0.0001 1 0 17 0.7918 -0.0019 1 0 18 -3.4555 -0.0001 1 0 19 1.4456 -0.0052 1 0 20 0.5889 0.0026 1 0 21 -1.4395 0.0005 1 0 22 0.3958 -0.0007 1 0 23 0.7273 0.0000 1 0 24 -1.8609 0.0014 1 0 25 -1.4182 0.0003 1 0 26 2.3410 0.0005 1 0 27 0.4553 0.0019 1 0 28 -0.5550 -0.0028 1 1 0 -40.4813 -0.0131 1 1 1 43.5079 -0.0123 1 1 2 1.9355 -0.0058 1 1 3 -36.8216 0.0097 1 1 4 22.5287 0.0096 1 1 5 9.7529 -0.0098 1 1 6 -15.8889 -0.0010 1 1 7 5.0860 -0.0027 1 1 8 5.7920 0.0081 1 1 9 -4.3670 0.0021 1 1 10 -1.5072 -0.0081 1 1 11 3.2893 0.0072 1 1 12 -0.5561 0.0004 1 1 13 -2.1829 0.0023 1 1 14 2.6421 -0.0001 1 1 15 -1.0619 -0.0043 1 1 16 -1.2356 0.0027 1 1 17 3.5347 -0.0013 1 1 18 -1.2343 0.0023 1 1 19 -1.4520 -0.0018 1 1 20 2.1045 -0.0031 1 1 21 0.2589 0.0017 1 1 22 -0.8803 -0.0002 1 1 23 1.1326 -0.0008 1 1 24 1.0866 -0.0025 1 1 25 -2.7338 0.0004 1 1 26 -0.3491 -0.0030 1 1 27 2.0817 0.0000 1 1 28 -0.8331 0.0015 1 1 29 -0.3495 -0.0047 1 2 0 -33.0541 0.0045 1 2 1 -12.1951 -0.0182 1 2 2 39.0647 0.0004 1 2 3 -20.1677 -0.0087 1 2 4 -15.7803 0.0176 1 2 5 20.4802 -0.0023 1 2 6 -3.2787 -0.0052 1 2 7 -7.1375 0.0018 1 2 8 4.8218 -0.0083 1 2 9 1.5522 0.0087 1 2 10 -2.2956 -0.0029 1 2 11 -0.2138 -0.0031 1 2 12 2.4501 0.0033 1 2 13 -1.1813 0.0010 1 2 14 -0.0629 0.0047 1 2 15 1.7272 -0.0024 1 2 16 -2.6226 -0.0008 1 2 17 0.6631 0.0003 1 2 18 1.9471 0.0005 1 2 19 -2.4790 0.0026 1 2 20 -0.4953 -0.0021 1 2 21 1.5351 -0.0003 1 2 22 -0.5862 0.0005 1 2 23 -1.1315 0.0026 1 2 24 2.3086 0.0005 1 2 25 0.4943 -0.0016 1 2 26 -2.5027 0.0010 1 2 27 1.5866 -0.0050 1 2 28 1.5184 0.0024 1 2 29 -0.4753 -0.0011 1 3 0 19.2774 0.0566 1 3 1 -35.1866 -0.0176 1 3 2 12.1090 -0.0088 1 3 3 19.1062 -0.0053 1 3 4 -22.3543 -0.0017 1 3 5 1.2934 0.0167 1 3 6 10.0606 -0.0128 1 3 7 -5.2518 0.0041 1 3 8 -1.4371 -0.0021 1 3 9 1.3788 -0.0053 1 3 10 0.6519 0.0046 1 3 11 -1.6787 -0.0032 1 3 12 -0.1208 -0.0007 1 3 13 1.5236 -0.0012 1 3 14 -1.0342 0.0039 1 3 15 1.6678 0.0021 1 3 16 0.3860 -0.0013 1 3 17 -1.8551 0.0000 1 3 18 2.3269 -0.0002 1 3 19 0.6506 0.0024 1 3 20 -2.0909 0.0004 1 3 21 0.4224 -0.0002 1 3 22 1.1181 -0.0008 1 3 23 -2.1606 -0.0010 1 3 24 -1.0278 0.0045 1 3 25 2.3413 -0.0005 1 3 26 -1.7232 0.0005 1 3 27 -1.9255 0.0004 1 3 28 1.6184 -0.0035 1 3 29 0.3453 0.0068 1 4 0 26.8728 0.0210 1 4 1 -3.6685 0.0493 1 4 2 -20.5186 -0.0188 1 4 3 18.2758 0.0022 1 4 4 0.4672 -0.0094 1 4 5 -12.5960 0.0142 1 4 6 5.9150 0.0084 1 4 7 1.9975 -0.0101 1 4 8 -1.4371 0.0055 1 4 9 -0.6768 -0.0047 1 4 10 0.0346 -0.0021 1 4 11 1.2831 -0.0018 1 4 12 -2.1336 -0.0008 1 4 13 0.0741 -0.0041 1 4 14 0.1658 -0.0013 1 4 15 -0.7859 0.0033 1 4 16 1.6656 -0.0011 1 4 17 -1.3552 -0.0002 1 4 18 -0.6344 -0.0017 1 4 19 2.4681 0.0014 1 4 20 -0.2498 0.0014 1 4 21 -1.0397 -0.0002 1 4 22 1.9246 0.0024 1 4 23 0.9239 -0.0018 1 4 24 -2.6155 0.0003 1 4 25 1.0423 0.0045 1 4 26 1.8710 -0.0020 1 4 27 -2.6240 0.0013 1 4 28 -0.6995 -0.0028 1 4 29 0.5762 -0.0011 1 5 0 -2.1852 -0.0737 1 5 1 18.7428 0.0323 1 5 2 -12.4362 0.0202 1 5 3 -3.8013 -0.0125 1 5 4 11.3226 -0.0042 1 5 5 -6.2498 -0.0065 1 5 6 -3.2730 0.0207 1 5 7 2.3016 0.0054 1 5 8 0.0489 0.0017 1 5 9 0.8114 0.0039 1 5 10 -2.2701 0.0024 1 5 11 1.1775 -0.0001 1 5 12 1.1179 -0.0006 1 5 13 -1.8089 0.0005 1 5 14 0.9206 -0.0062 1 5 15 -0.5884 0.0020 1 5 16 0.3453 0.0001 1 5 17 0.8695 -0.0009 1 5 18 -2.1763 -0.0014 1 5 19 0.2977 -0.0025 1 5 20 1.2900 0.0019 1 5 21 -1.4223 -0.0017 1 5 22 -0.5370 -0.0003 1 5 23 2.3816 0.0023 1 5 24 -0.8258 -0.0017 1 5 25 -2.3166 0.0026 1 5 26 2.7385 0.0037 1 5 27 0.6491 -0.0005 1 5 28 -1.8667 0.0020 1 5 29 0.4679 -0.0022 1 6 0 -14.8680 -0.0253 1 6 1 7.7899 -0.0454 1 6 2 6.2358 0.0271 1 6 3 -8.6980 0.0033 1 6 4 3.9439 -0.0105 1 6 5 3.1037 -0.0181 1 6 6 -3.2879 -0.0073 1 6 7 0.1215 0.0069 1 6 8 -0.9669 0.0038 1 6 9 1.7982 0.0006 1 6 10 -0.2908 0.0000 1 6 11 -2.8174 0.0067 1 6 12 1.9079 0.0001 1 6 13 -0.5961 0.0049 1 6 14 -0.8344 -0.0014 1 6 15 0.7416 -0.0029 1 6 16 -0.7493 0.0036 1 6 17 1.6145 -0.0009 1 6 18 0.0512 0.0014 1 6 19 -1.2552 -0.0028 1 6 20 1.4925 -0.0007 1 6 21 0.6136 0.0016 1 6 22 -1.4944 -0.0029 1 6 23 0.8046 -0.0008 1 6 24 2.1543 0.0012 1 6 25 -2.6921 -0.0010 1 6 26 -1.0590 0.0021 1 6 27 2.7006 0.0022 1 6 28 -0.9377 0.0000 1 6 29 -1.0176 0.0021 1 7 0 -4.0496 0.0363 1 7 1 -6.1366 -0.0273 1 7 2 6.8724 -0.0132 1 7 3 -0.9844 0.0210 1 7 4 -2.3963 0.0110 1 7 5 2.5140 -0.0057 1 7 6 -0.2853 -0.0111 1 7 7 0.8368 -0.0057 1 7 8 -0.9645 -0.0008 1 7 9 -0.5028 0.0055 1 7 10 3.2535 -0.0072 1 7 11 -1.6178 -0.0020 1 7 12 -0.9704 0.0015 1 7 13 1.2735 0.0002 1 7 14 -1.5562 0.0049 1 7 15 0.1655 -0.0045 1 7 16 -0.7955 0.0004 1 7 17 -0.6494 0.0010 1 7 18 1.2296 0.0005 1 7 19 -1.3939 0.0009 1 7 20 -0.3407 -0.0039 1 7 21 1.4870 0.0000 1 7 22 -0.2812 0.0004 1 7 23 -0.9022 -0.0032 1 7 24 2.4250 -0.0019 1 7 25 1.3013 0.0019 1 7 26 -2.8389 -0.0007 1 7 27 1.1389 0.0006 1 7 28 1.9625 0.0008 1 7 29 -1.2164 -0.0025 1 8 0 5.4725 0.0204 1 8 1 -4.7877 0.0027 1 8 2 -0.0409 -0.0213 1 8 3 2.3541 -0.0113 1 8 4 -0.9245 0.0119 1 8 5 0.4728 0.0086 1 8 6 -1.2529 -0.0069 1 8 7 0.5738 0.0001 1 8 8 1.3420 -0.0063 1 8 9 -2.8574 0.0044 1 8 10 1.0266 0.0074 1 8 11 2.1736 -0.0054 1 8 12 -1.4436 0.0002 1 8 13 0.9327 -0.0018 1 8 14 0.0892 0.0038 1 8 15 -0.2230 0.0018 1 8 16 0.9532 -0.0031 1 8 17 -1.3686 0.0011 1 8 18 0.6541 0.0004 1 8 19 0.1605 0.0034 1 8 20 -1.8489 0.0002 1 8 21 0.4313 -0.0026 1 8 22 0.2958 -0.0007 1 8 23 -1.4773 -0.0004 1 8 24 -0.3911 -0.0048 1 8 25 2.4261 -0.0025 1 8 26 -0.6858 0.0030 1 8 27 -1.9432 -0.0021 1 8 28 2.1133 0.0011 1 8 29 0.7518 -0.0007 1 9 0 2.8192 0.0250 1 9 1 0.5840 0.0216 1 9 2 -1.7683 -0.0021 1 9 3 0.6277 -0.0063 1 9 4 -0.2181 -0.0111 1 9 5 1.9162 0.0133 1 9 6 -0.2192 -0.0032 1 9 7 -2.1146 -0.0078 1 9 8 2.7759 -0.0020 1 9 9 -0.1145 -0.0111 1 9 10 -2.7483 0.0037 1 9 11 1.3930 0.0017 1 9 12 0.0912 -0.0018 1 9 13 -0.5350 -0.0020 1 9 14 0.3657 -0.0009 1 9 15 -1.1596 0.0040 1 9 16 1.1361 -0.0005 1 9 17 0.1158 -0.0012 1 9 18 -0.7892 -0.0011 1 9 19 1.6991 0.0021 1 9 20 -0.8485 0.0035 1 9 21 -0.4590 0.0015 1 9 22 1.2231 -0.0001 1 9 23 -0.6109 -0.0002 1 9 24 -1.2834 0.0006 1 9 25 0.6943 -0.0060 1 9 26 1.2957 -0.0002 1 9 27 -1.9024 0.0021 1 9 28 -0.5170 -0.0039 1 10 0 -1.0253 -0.0308 1 10 1 0.8461 0.0375 1 10 2 -0.5361 0.0050 1 10 3 0.2841 0.0067 1 10 4 -1.5508 -0.0017 1 10 5 -0.0622 0.0021 1 10 6 2.7358 0.0217 1 10 7 -2.4085 -0.0018 1 10 8 -0.6179 0.0030 1 10 9 3.4985 -0.0013 1 10 10 -1.0643 -0.0054 1 10 11 -0.9683 0.0005 1 10 12 1.0978 -0.0002 1 10 13 -0.0919 -0.0016 1 10 14 0.7435 -0.0043 1 10 15 -1.0180 0.0009 1 10 16 -0.8446 0.0004 1 10 17 1.3284 0.0003 1 10 18 -1.4358 -0.0026 1 10 19 0.1844 -0.0019 1 10 20 0.7280 0.0019 1 10 21 -1.6733 0.0005 1 10 22 1.0082 0.0027 1 10 23 0.5471 -0.0007 1 10 24 -1.3227 0.0009 1 10 25 -0.1539 -0.0001 1 10 26 1.2560 -0.0053 1 10 27 -0.1742 0.0038 1 10 28 -1.3623 -0.0001 1 11 0 -0.0315 -0.0588 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-0.0512 2 -5 1 7.6477 0.0156 2 -5 2 -6.1312 0.0091 2 -5 3 -0.6826 0.0001 2 -5 4 3.2091 0.0050 2 -5 5 -0.2844 -0.0089 2 -5 6 -1.1442 0.0162 2 -5 7 -1.8539 0.0077 2 -5 8 3.7713 0.0012 2 -5 9 -0.1826 0.0020 2 -5 10 -3.9730 -0.0017 2 -5 11 3.5840 0.0015 2 -5 12 0.6628 0.0012 2 -5 13 -4.0463 0.0022 2 -5 14 1.9563 -0.0031 2 -5 15 1.8299 0.0003 2 -5 16 -2.5840 0.0006 2 -5 17 1.1205 0.0015 2 -5 18 0.4048 -0.0008 2 -5 19 -1.6065 -0.0029 2 -5 20 0.7443 0.0010 2 -5 21 -0.3944 -0.0031 2 -4 0 -11.4803 -0.0268 2 -4 1 7.2992 -0.0430 2 -4 2 2.2880 0.0182 2 -4 3 -6.0261 -0.0102 2 -4 4 1.3784 -0.0021 2 -4 5 0.3649 -0.0131 2 -4 6 1.0280 -0.0105 2 -4 7 -2.4959 0.0082 2 -4 8 -1.4251 0.0022 2 -4 9 5.3696 0.0029 2 -4 10 -2.9586 0.0002 2 -4 11 -2.4691 0.0049 2 -4 12 4.8816 0.0007 2 -4 13 -2.2133 0.0052 2 -4 14 -3.2167 0.0011 2 -4 15 3.3740 -0.0018 2 -4 16 -0.5595 0.0023 2 -4 17 -1.6466 -0.0002 2 -4 18 2.2046 0.0048 2 -4 19 -1.1307 -0.0022 2 -4 20 -0.7025 0.0007 2 -3 0 -7.0624 0.0634 2 -3 1 -5.4442 -0.0350 2 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-0.5800 0.0027 2 -2 24 -1.6817 -0.0017 2 -1 0 12.8875 -0.0223 2 -1 1 1.6682 0.0386 2 -1 2 -9.2882 0.0068 2 -1 3 4.5014 -0.0199 2 -1 4 0.6925 -0.0087 2 -1 5 1.8254 0.0070 2 -1 6 -2.7351 0.0057 2 -1 7 -3.0234 -0.0026 2 -1 8 8.2552 0.0019 2 -1 9 -4.0279 -0.0081 2 -1 10 -4.8727 0.0076 2 -1 11 8.3952 0.0041 2 -1 12 -2.2309 -0.0039 2 -1 13 -3.5887 -0.0005 2 -1 14 5.0778 -0.0039 2 -1 15 -1.9129 0.0046 2 -1 16 -2.4012 -0.0052 2 -1 17 2.1608 -0.0017 2 -1 18 -0.7177 0.0008 2 -1 19 -0.3870 -0.0011 2 -1 20 1.5803 0.0034 2 -1 21 -0.8832 0.0005 2 -1 22 -0.7640 -0.0014 2 -1 23 1.8161 -0.0002 2 -1 24 -1.3488 0.0050 2 -1 25 0.0738 -0.0029 2 -1 26 3.7414 -0.0018 2 0 0 -7.6474 -0.0359 2 0 1 12.9802 0.0118 2 0 2 -4.0203 0.0226 2 0 3 -2.2647 0.0028 2 0 4 1.2195 -0.0091 2 0 5 1.4463 -0.0063 2 0 6 4.5756 0.0117 2 0 7 -8.0043 -0.0009 2 0 8 1.7022 0.0038 2 0 9 7.8696 -0.0012 2 0 10 -9.0374 -0.0076 2 0 11 0.3620 0.0075 2 0 12 6.9981 0.0007 2 0 13 -5.1575 0.0002 2 0 14 0.8282 -0.0037 2 0 15 3.4846 0.0009 2 0 16 -2.9431 0.0025 2 0 17 0.3465 -0.0042 2 0 18 1.1678 -0.0000 2 0 19 -0.8605 -0.0025 2 0 20 0.4638 0.0001 2 0 21 0.6929 -0.0001 2 0 22 -1.9590 0.0009 2 0 23 -0.2318 -0.0026 2 0 24 1.0663 -0.0002 2 0 25 -2.8549 0.0051 2 0 26 1.4649 -0.0020 2 0 27 2.5466 0.0012 2 0 28 -2.4867 0.0017 2 0 29 0.9390 -0.0015 2 1 0 -15.2182 -0.0407 2 1 1 -0.1541 -0.0213 2 1 2 5.8957 0.0233 2 1 3 -3.1543 0.0015 2 1 4 0.0428 0.0036 2 1 5 -3.7546 -0.0132 2 1 6 6.5278 -0.0010 2 1 7 1.4835 0.0069 2 1 8 -9.7325 -0.0022 2 1 9 8.3903 0.0070 2 1 10 2.6144 -0.0031 2 1 11 -9.4297 -0.0008 2 1 12 5.4029 0.0040 2 1 13 1.9104 0.0028 2 1 14 -4.6494 0.0003 2 1 15 3.3723 -0.0029 2 1 16 -0.1498 0.0029 2 1 17 -1.9178 -0.0001 2 1 18 1.4960 0.0007 2 1 19 0.1716 -0.0014 2 1 20 -0.0017 -0.0007 2 1 21 1.4729 0.0008 2 1 22 0.4123 -0.0013 2 1 23 -1.8131 0.0024 2 1 24 1.6115 -0.0048 2 1 25 0.1124 -0.0007 2 1 26 -2.8946 0.0026 2 1 27 2.5464 -0.0033 2 1 28 0.4630 0.0019 2 1 29 -2.3833 -0.0002 2 2 0 4.5342 0.0342 2 2 1 -11.1297 -0.0609 2 2 2 1.9910 0.0097 2 2 3 0.8077 0.0156 2 2 4 1.7611 0.0014 2 2 5 -3.7822 0.0026 2 2 7 9.7636 0.0030 2 2 8 -5.8701 -0.0007 2 2 9 -5.7128 -0.0011 2 2 10 10.9158 0.0005 2 2 11 -4.1566 -0.0016 2 2 12 -4.5128 -0.0001 2 2 13 6.6733 0.0008 2 2 14 -2.5190 0.0041 2 2 15 -0.7142 -0.0013 2 2 16 2.8143 0.0009 2 2 17 -2.6523 0.0003 2 2 18 -0.1934 0.0010 2 2 19 0.6698 0.0022 2 2 20 -1.0854 -0.0032 2 2 21 0.0644 0.0026 2 2 22 1.2987 -0.0002 2 2 23 -1.2489 0.0008 2 2 24 -1.1526 0.0041 2 2 25 2.6821 -0.0045 2 2 26 -1.2983 0.0023 2 2 27 -1.2417 0.0007 2 2 28 3.2193 -0.0026 2 2 29 -0.2777 0.0048 2 2 30 -1.0702 -0.0049 2 3 0 12.3780 0.0774 2 3 1 -0.2875 -0.0029 2 3 2 -5.4594 -0.0478 2 3 3 -0.7826 0.0201 2 3 4 2.0656 0.0045 2 3 5 4.1235 0.0104 2 3 6 -8.0867 -0.0033 2 3 7 1.9168 -0.0076 2 3 8 7.5071 0.0026 2 3 9 -10.7767 0.0002 2 3 10 1.4635 -0.0012 2 3 11 7.0380 -0.0037 2 3 12 -7.7234 0.0016 2 3 13 1.2900 -0.0035 2 3 14 3.1753 0.0012 2 3 15 -3.3553 0.0004 2 3 16 3.1067 -0.0011 2 3 17 0.5473 0.0019 2 3 18 -2.0177 -0.0023 2 3 19 1.8770 0.0037 2 3 20 0.1615 -0.0003 2 3 21 -1.0006 -0.0029 2 3 22 1.0575 0.0034 2 3 23 0.4517 -0.0021 2 3 24 -2.7315 0.0025 2 3 25 0.1195 0.0019 2 3 26 1.2437 -0.0030 2 3 27 -3.0056 0.0052 2 3 28 -0.2747 -0.0027 2 3 29 1.9512 0.0031 2 3 30 -0.8581 0.0074 2 4 0 -2.0209 -0.0179 2 4 1 8.1204 0.0702 2 4 2 -0.2955 -0.0267 2 4 3 -4.1847 -0.0190 2 4 4 -3.2794 0.0091 2 4 5 5.8455 0.0075 2 4 6 0.6201 0.0127 2 4 7 -8.0842 -0.0050 2 4 8 7.9082 -0.0018 2 4 9 1.0469 -0.0004 2 4 10 -9.1969 0.0049 2 4 11 6.8362 -0.0043 2 4 12 0.5948 -0.0014 2 4 13 -5.8343 0.0008 2 4 14 3.7125 -0.0035 2 4 15 -1.7586 0.0021 2 4 16 -1.4704 -0.0039 2 4 17 3.2301 0.0008 2 4 18 -2.2826 -0.0004 2 4 19 -0.5267 -0.0021 2 4 20 2.2792 0.0038 2 4 21 -0.6100 -0.0029 2 4 22 0.2286 -0.0012 2 4 23 2.4093 0.0026 2 4 24 -0.4462 -0.0018 2 4 25 -1.2665 0.0026 2 4 26 2.0857 -0.0024 2 4 27 -0.2263 0.0004 2 4 28 -2.4092 0.0032 2 4 29 0.3882 -0.0065 2 4 30 0.5363 0.0085 2 5 0 -6.5612 -0.0621 2 5 1 0.1535 0.0120 2 5 2 6.0717 0.0302 2 5 3 1.3457 -0.0244 2 5 4 -5.8639 -0.0099 2 5 5 -1.2366 -0.0047 2 5 6 7.2419 0.0134 2 5 7 -5.0693 0.0066 2 5 8 -3.4626 0.0019 2 5 9 8.7913 -0.0014 2 5 10 -5.2657 0.0018 2 5 11 -3.4826 0.0077 2 5 12 7.1065 -0.0036 2 5 13 -3.3946 0.0023 2 5 14 -0.8522 -0.0021 2 5 15 2.7453 0.0014 2 5 16 -3.4050 0.0008 2 5 17 1.5791 -0.0043 2 5 18 1.2324 0.0019 2 5 19 -3.2526 -0.0020 2 5 20 0.8207 -0.0006 2 5 21 0.7485 0.0018 2 5 22 -1.7705 -0.0037 2 5 23 1.1273 -0.0005 2 5 24 1.1802 0.0017 2 5 25 -1.7256 0.0004 2 5 26 0.8673 0.0008 2 5 27 1.9226 -0.0037 2 5 28 -0.9243 0.0056 2 5 29 -0.6495 -0.0010 2 5 30 0.8728 -0.0045 2 6 0 2.1807 -0.0063 2 6 1 -4.7310 -0.0295 2 6 2 -0.2139 0.0198 2 6 3 6.4978 0.0039 2 6 4 0.4913 -0.0086 2 6 5 -6.6748 -0.0183 2 6 6 3.8050 -0.0076 2 6 7 4.6996 0.0052 2 6 8 -7.4676 -0.0010 2 6 9 2.6830 0.0038 2 6 10 4.8997 -0.0075 2 6 11 -7.5679 0.0035 2 6 12 1.3988 0.0050 2 6 13 3.0964 0.0005 2 6 14 -3.9287 0.0014 2 6 15 2.1175 -0.0019 2 6 16 -0.2439 0.0050 2 6 17 -2.0630 -0.0012 2 6 18 3.1648 -0.0020 2 6 19 -0.7382 0.0011 2 6 20 -1.5622 -0.0013 2 6 21 2.1489 0.0000 2 6 22 -0.5220 0.0004 2 6 23 -0.8142 -0.0032 2 6 24 1.9994 -0.0010 2 6 25 -0.8603 0.0014 2 6 26 -1.2455 0.0013 2 6 27 1.8303 -0.0032 2 6 28 0.0773 -0.0019 2 6 29 -1.0673 0.0070 2 7 0 3.3035 0.0143 2 7 1 1.6618 -0.0195 2 7 2 -5.0137 0.0056 2 7 3 -0.0055 0.0093 2 7 4 6.7653 0.0075 2 7 5 -3.2516 0.0029 2 7 6 -4.8604 -0.0149 2 7 7 7.0714 0.0009 2 7 8 -0.2511 -0.0026 2 7 9 -5.2000 0.0026 2 7 10 6.5163 0.0005 2 7 11 0.3358 -0.0098 2 7 12 -4.9864 0.0015 2 7 13 3.5880 0.0015 2 7 14 -0.5792 0.0018 2 7 15 -1.7081 -0.0022 2 7 16 1.8890 0.0007 2 7 17 -2.8420 0.0038 2 7 18 -0.1825 -0.0007 2 7 19 1.6722 -0.0011 2 7 20 -2.5751 -0.0001 2 7 21 0.1052 -0.0002 2 7 22 1.3669 -0.0013 2 7 23 -1.5125 0.0002 2 7 24 0.9128 -0.0029 2 7 25 1.5892 -0.0013 2 7 26 -1.5679 0.0019 2 7 27 0.9041 -0.0008 2 7 28 1.8276 -0.0058 2 7 29 -0.5465 -0.0003 2 8 0 -2.8029 0.0367 2 8 1 3.5145 -0.0174 2 8 2 1.4202 -0.0136 2 8 3 -5.6898 0.0100 2 8 4 2.3597 -0.0054 2 8 5 5.3389 0.0102 2 8 6 -6.5600 -0.0026 2 8 7 -0.8597 -0.0060 2 8 8 6.0357 0.0011 2 8 9 -4.5724 -0.0020 2 8 10 -1.2633 0.0080 2 8 11 5.6450 -0.0013 2 8 12 -2.6157 -0.0047 2 8 13 -1.0131 0.0002 2 8 14 2.8952 0.0019 2 8 15 -1.4638 -0.0001 2 8 16 1.6005 -0.0017 2 8 17 0.4941 0.0019 2 8 18 -2.4283 0.0024 2 8 19 2.0296 0.0023 2 8 20 -0.4272 -0.0015 2 8 21 -2.4154 0.0018 2 8 22 1.0651 0.0002 2 8 23 -0.5893 -0.0017 2 8 24 -1.7913 0.0008 2 8 25 1.1539 -0.0028 2 8 26 -0.4533 0.0007 2 8 27 -1.5186 0.0012 2 8 28 1.7066 -0.0029 2 8 29 0.7196 -0.0039 2 9 0 -2.8709 0.0217 2 9 1 -2.5247 0.0379 2 9 2 4.3475 -0.0256 2 9 3 -0.2796 0.0065 2 9 4 -5.2806 0.0055 2 9 5 5.2635 -0.0014 2 9 6 2.1246 0.0069 2 9 7 -6.3821 -0.0057 2 9 8 3.4517 -0.0034 2 9 9 2.6044 -0.0059 2 9 10 -5.0266 0.0002 2 9 11 1.8916 0.0028 2 9 12 2.0461 -0.0021 2 9 13 -3.0979 -0.0027 2 9 14 1.0077 -0.0001 2 9 15 -0.1547 0.0008 2 9 16 -0.7607 -0.0026 2 9 17 2.7059 0.0007 2 9 18 -1.8892 -0.0011 2 9 19 -0.3038 0.0031 2 9 20 2.8233 0.0021 2 9 21 -1.6628 -0.0020 2 9 22 -0.4429 0.0041 2 9 23 1.4975 -0.0005 2 9 24 -1.1076 0.0002 2 9 25 -0.5949 0.0002 2 9 26 0.8738 -0.0006 2 9 27 -1.5512 0.0032 2 9 28 -0.6864 -0.0025 2 9 29 1.2866 -0.0024 2 10 0 2.2416 -0.0570 2 10 1 -3.6034 0.0350 2 10 2 -1.3397 0.0132 2 10 3 4.5239 -0.0200 2 10 4 -3.0434 0.0101 2 10 5 -3.3098 0.0036 2 10 6 5.7505 0.0091 2 10 7 -1.9763 0.0072 2 10 8 -3.4838 0.0038 2 10 9 4.8122 -0.0022 2 10 10 -0.6681 -0.0008 2 10 11 -2.0492 0.0030 2 10 12 3.0832 -0.0009 2 10 13 -0.5023 -0.0001 2 10 14 -0.5765 -0.0027 2 10 15 1.3241 0.0018 2 10 16 -2.2769 -0.0028 2 10 17 1.5244 -0.0014 2 10 18 1.3108 0.0006 2 10 19 -3.5620 -0.0028 2 10 20 1.6680 0.0041 2 10 21 1.2818 -0.0014 2 10 22 -2.1688 -0.0010 2 10 23 0.5583 0.0024 2 10 24 0.6835 -0.0005 2 10 25 -0.8975 0.0010 2 10 26 0.3152 -0.0018 2 10 27 0.3667 0.0044 2 10 28 -1.4691 0.0024 2 11 0 2.9628 -0.0262 2 11 1 1.4305 -0.0371 2 11 2 -3.8061 0.0292 2 11 3 1.0530 -0.0073 2 11 4 3.4218 -0.0151 2 11 5 -4.3242 -0.0061 2 11 6 -0.0067 -0.0020 2 11 7 3.5391 0.0023 2 11 8 -4.1309 0.0046 2 11 9 -0.3212 0.0033 2 11 10 2.4264 -0.0037 2 11 11 -2.4175 0.0064 2 11 12 0.5649 0.0018 2 11 13 1.1497 0.0027 2 11 14 -1.3942 0.0003 2 11 15 2.1426 0.0000 2 11 16 -0.2789 0.0034 2 11 17 -1.8194 -0.0043 2 11 18 3.9330 0.0016 2 11 19 -0.8911 -0.0006 2 11 20 -2.4039 0.0005 2 11 21 3.0069 0.0035 2 11 22 -0.0531 -0.0014 2 11 23 -1.2204 0.0005 2 11 24 0.6123 -0.0001 2 11 25 -0.0143 0.0022 2 11 26 -0.4938 -0.0015 2 11 27 0.5726 -0.0011 2 11 28 -0.3061 0.0086 2 12 0 -1.2798 0.0361 2 12 1 3.2792 -0.0270 2 12 2 -0.3257 -0.0040 2 12 3 -2.9340 0.0204 2 12 4 2.7056 0.0012 2 12 5 1.0097 -0.0069 2 12 6 -3.0448 -0.0092 2 12 7 2.4125 -0.0019 2 12 8 0.7796 -0.0047 2 12 9 -2.6580 0.0030 2 12 10 1.6481 -0.0065 2 12 11 -0.2081 -0.0043 2 12 12 -1.2712 0.0024 2 12 13 1.4872 -0.0009 2 12 14 -1.7191 0.0041 2 12 15 -0.4347 -0.0040 2 12 16 2.5043 0.0028 2 12 17 -2.8960 0.0010 2 12 18 -0.0194 -0.0040 2 12 19 3.4026 0.0002 2 12 20 -2.8833 -0.0013 2 12 21 -0.4365 0.0017 2 12 22 2.4356 0.0004 2 12 23 -0.3760 0.0016 2 12 24 -0.1637 -0.0012 2 12 25 0.3274 0.0004 2 12 26 -0.0258 0.0039 2 12 27 0.1779 -0.0042 2 13 0 -2.9825 0.0166 2 13 1 0.1050 0.0030 2 13 2 2.5414 -0.0168 2 13 3 -1.8301 0.0024 2 13 4 -1.1100 0.0095 2 13 5 2.1077 0.0108 2 13 6 -1.1476 -0.0049 2 13 7 -1.0035 -0.0003 2 13 8 1.7864 0.0006 2 13 9 -1.0389 0.0008 2 13 10 -0.4606 0.0043 2 13 11 1.1714 -0.0072 2 13 12 -1.1370 -0.0006 2 13 13 1.1622 -0.0033 2 13 14 0.8143 0.0029 2 13 15 -2.5037 0.0013 2 13 16 1.9796 -0.0050 2 13 17 1.2558 0.0042 2 13 18 -3.1399 -0.0004 2 13 19 1.9239 -0.0018 2 13 20 1.1562 -0.0023 2 13 21 -2.8201 0.0004 2 13 22 0.5467 -0.0020 2 13 23 0.9972 -0.0010 2 13 24 -0.2175 0.0019 2 13 25 -0.1976 -0.0048 2 13 26 -0.2804 0.0020 2 14 0 0.1434 0.0138 2 14 1 -2.4342 0.0100 2 14 2 1.3832 -0.0114 2 14 3 1.1548 -0.0020 2 14 4 -1.5783 -0.0059 2 14 5 0.6062 0.0064 2 14 6 0.6847 0.0051 2 14 7 -0.9436 -0.0078 2 14 8 0.2142 0.0011 2 14 9 0.2522 -0.0022 2 14 10 -1.0516 0.0043 2 14 11 0.0785 0.0004 2 14 12 -0.5987 -0.0020 2 14 13 -0.8415 -0.0011 2 14 14 1.8078 -0.0030 2 14 15 -1.2375 0.0060 2 14 16 -1.5874 -0.0026 2 14 17 2.7144 -0.0022 2 14 18 -0.3967 0.0019 2 14 19 -1.3094 0.0021 2 14 20 2.0646 -0.0004 2 14 21 -0.2770 -0.0009 2 14 22 -1.2285 0.0028 2 14 23 0.6709 -0.0045 2 14 24 0.6026 0.0015 2 14 25 0.2075 0.0001 2 15 0 1.9488 -0.0118 2 15 1 -0.8037 0.0300 2 15 2 -1.4423 -0.0055 2 15 3 1.4952 -0.0029 2 15 4 -0.1019 0.0049 2 15 5 -0.5079 -0.0029 2 15 6 0.6329 0.0125 2 15 7 0.1812 0.0011 2 15 8 0.2026 -0.0024 2 15 9 0.2506 -0.0003 2 15 10 0.4060 -0.0006 2 15 11 -0.1759 0.0021 2 15 12 -0.1368 -0.0030 2 15 13 -0.9092 0.0003 2 15 14 0.3341 -0.0031 2 15 15 0.8944 0.0009 2 15 16 -2.1653 0.0020 2 15 17 -0.2077 -0.0023 2 15 18 1.3225 -0.0023 2 15 19 -0.7194 -0.0019 2 15 20 -0.0824 0.0043 2 15 21 0.5525 -0.0023 2 15 22 -0.5242 0.0016 2 15 23 -0.4712 0.0019 2 15 24 0.3342 -0.0044 2 16 0 -0.2159 -0.0429 2 16 1 1.3686 0.0009 2 16 2 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0.0012 3 8 9 2.3420 0.0018 3 8 10 -6.4110 0.0015 3 8 11 3.9893 -0.0020 3 8 12 2.0113 -0.0014 3 8 13 -4.1995 -0.0016 3 8 14 2.5165 0.0008 3 8 15 2.2072 0.0002 3 8 16 -1.5454 -0.0022 3 8 17 1.0987 0.0025 3 8 18 0.6046 0.0005 3 8 19 0.0083 0.0040 3 8 20 0.4281 -0.0013 3 8 21 -1.1829 -0.0019 3 8 22 -0.0679 0.0045 3 8 23 0.2800 -0.0006 3 8 24 -1.9665 0.0007 3 8 25 -0.3145 0.0028 3 8 26 0.2842 -0.0017 3 8 27 -1.8947 -0.0006 3 8 28 0.7630 0.0045 3 8 29 0.5787 -0.0059 3 9 0 4.3690 -0.0102 3 9 1 -6.9791 0.0403 3 9 2 -0.1345 -0.0149 3 9 3 8.5385 -0.0097 3 9 4 -6.8231 0.0160 3 9 5 -3.1536 0.0033 3 9 6 8.9860 -0.0012 3 9 7 -4.5225 -0.0016 3 9 8 -3.8289 0.0011 3 9 9 6.3565 -0.0029 3 9 10 -2.2788 0.0027 3 9 11 -2.7896 -0.0000 3 9 12 3.8805 -0.0032 3 9 13 -1.6910 -0.0000 3 9 14 -2.5847 -0.0022 3 9 15 2.7569 0.0015 3 9 16 -0.0721 -0.0038 3 9 17 -0.9510 -0.0000 3 9 18 0.8743 0.0009 3 9 19 0.1880 -0.0009 3 9 20 1.2312 0.0041 3 9 21 0.2009 -0.0037 3 9 22 -0.6985 -0.0006 3 9 23 1.1494 0.0035 3 9 24 0.6098 -0.0005 3 9 25 -1.1885 0.0017 3 9 26 0.1557 0.0027 3 9 27 -0.1474 -0.0013 3 9 28 -1.0945 0.0007 3 9 29 0.7550 0.0026 3 10 0 4.4592 -0.0376 3 10 1 0.7006 0.0063 3 10 2 -6.6916 0.0148 3 10 3 4.2664 -0.0140 3 10 4 3.7475 -0.0037 3 10 5 -8.1482 0.0049 3 10 6 2.2814 0.0112 3 10 7 4.5286 -0.0024 3 10 8 -5.9711 0.0033 3 10 9 1.1107 0.0028 3 10 10 3.4377 -0.0018 3 10 11 -2.9690 0.0079 3 10 12 0.9607 -0.0020 3 10 13 2.3309 -0.0007 3 10 14 -2.6568 -0.0004 3 10 15 0.3108 0.0007 3 10 16 1.9963 0.0001 3 10 17 -1.2289 -0.0042 3 10 18 0.1467 0.0024 3 10 19 -0.3014 -0.0013 3 10 20 0.0700 0.0011 3 10 21 1.3149 0.0017 3 10 22 -0.7381 -0.0044 3 10 23 -0.7022 -0.0005 3 10 24 0.9642 0.0018 3 10 25 0.6950 0.0008 3 10 26 -0.8554 0.0008 3 10 27 0.1480 0.0018 3 10 28 0.1508 -0.0000 3 11 0 -0.9316 -0.0079 3 11 1 4.7224 -0.0166 3 11 2 -2.4164 0.0105 3 11 3 -3.2803 -0.0047 3 11 4 6.0107 -0.0038 3 11 5 -1.0514 -0.0140 3 11 6 -5.1805 -0.0012 3 11 7 4.4506 0.0064 3 11 8 -0.5335 -0.0078 3 11 9 -3.9904 0.0043 3 11 10 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25 -0.5352 -0.0033 3 12 26 1.4088 0.0042 3 12 27 0.7136 0.0011 3 13 0 -0.6697 0.0274 3 13 1 -2.1763 -0.0157 3 13 2 2.1178 -0.0118 3 13 3 -0.2479 0.0189 3 13 4 -2.6045 -0.0094 3 13 5 2.2850 0.0086 3 13 6 0.8401 0.0044 3 13 7 -2.6312 -0.0082 3 13 8 1.5712 0.0078 3 13 9 0.5506 0.0016 3 13 10 -1.3616 0.0029 3 13 11 1.5243 -0.0051 3 13 12 -0.8032 -0.0021 3 13 13 -0.6585 0.0033 3 13 14 2.6305 -0.0009 3 13 15 -1.6545 0.0008 3 13 16 -2.2518 -0.0021 3 13 17 3.0542 -0.0006 3 13 18 -0.5079 0.0008 3 13 19 -1.6776 0.0015 3 13 20 1.1478 -0.0037 3 13 21 -1.3331 -0.0002 3 13 22 0.1269 0.0014 3 13 23 0.9293 -0.0026 3 13 24 -0.3258 0.0013 3 13 25 -0.6972 -0.0044 3 13 26 -0.6744 -0.0024 3 14 0 1.9208 0.0094 3 14 1 -1.1936 0.0258 3 14 2 -0.2132 -0.0294 3 14 3 1.3829 0.0036 3 14 4 -1.3247 0.0098 3 14 5 -0.1309 -0.0098 3 14 6 1.7675 0.0073 3 14 7 -0.8270 -0.0034 3 14 8 -0.4574 -0.0037 3 14 9 1.0828 0.0026 3 14 10 -1.0516 0.0042 3 14 11 0.1843 -0.0003 3 14 12 0.6319 -0.0043 3 14 13 -2.2540 0.0027 3 14 14 1.2061 -0.0005 3 14 15 1.6138 0.0012 3 14 16 -3.6083 -0.0008 3 14 17 0.1956 -0.0017 3 14 18 2.6518 -0.0010 3 14 19 -1.6546 0.0025 3 14 20 -0.1527 0.0030 3 14 21 -0.0307 -0.0034 3 14 22 -0.7371 0.0033 3 14 23 1.4445 -0.0002 3 14 24 0.0782 -0.0010 3 14 25 -0.2645 0.0009 3 15 0 0.5719 -0.0370 3 15 1 0.6632 0.0269 3 15 2 -0.7371 0.0085 3 15 3 0.5323 -0.0224 3 15 4 -0.2608 0.0096 3 15 5 -0.6695 0.0053 3 15 6 0.9872 0.0004 3 15 7 0.2578 0.0027 3 15 8 -0.1008 -0.0006 3 15 9 0.8168 -0.0016 3 15 10 0.3582 0.0027 3 15 11 -0.3064 0.0044 3 15 12 1.2671 -0.0043 3 15 13 -0.3862 0.0014 3 15 14 -1.3588 0.0007 3 15 15 2.3919 0.0008 3 15 16 -0.6592 0.0009 3 15 17 -2.8922 -0.0043 3 15 18 1.5583 -0.0003 3 15 19 0.7065 -0.0031 3 15 20 -0.9380 0.0025 3 15 21 -0.2970 0.0008 3 15 22 -1.4326 -0.0022 3 15 23 0.5885 0.0029 3 15 24 1.2195 -0.0006 3 16 0 -0.7837 -0.0185 3 16 1 0.3465 -0.0214 3 16 2 -0.0161 0.0217 3 16 3 0.1120 -0.0060 3 16 4 -0.1052 -0.0147 3 16 5 -1.1867 -0.0007 3 16 6 0.3509 0.0059 3 16 7 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28 -2.0373 0.0019 4 2 29 -0.3821 0.0013 4 3 0 13.4090 0.0191 4 3 1 -14.5857 0.0072 4 3 2 0.3965 -0.0152 4 3 3 17.5352 0.0064 4 3 4 -16.5359 -0.0062 4 3 5 -1.5924 0.0162 4 3 6 17.7497 0.0012 4 3 7 -12.7861 -0.0101 4 3 8 -3.3420 0.0093 4 3 9 12.9586 -0.0014 4 3 10 -7.7781 0.0058 4 3 11 -4.4792 -0.0034 4 3 12 7.7645 -0.0050 4 3 13 -2.4616 0.0034 4 3 14 -3.2573 -0.0013 4 3 15 3.0101 -0.0007 4 3 16 -0.3963 -0.0039 4 3 17 -2.0574 -0.0016 4 3 18 0.6959 0.0008 4 3 19 1.4408 0.0017 4 3 20 -0.6989 -0.0008 4 3 21 0.4432 -0.0012 4 3 22 2.0281 -0.0007 4 3 23 -0.9625 0.0002 4 3 24 -1.1519 0.0029 4 3 25 0.8158 -0.0043 4 3 26 -0.0550 -0.0005 4 3 27 0.3550 0.0028 4 3 28 -0.0034 -0.0025 4 3 29 -2.1526 0.0016 4 4 0 10.5253 -0.0112 4 4 1 3.1883 0.0283 4 4 2 -16.3294 -0.0224 4 4 3 12.9042 0.0021 4 4 4 6.0055 0.0006 4 4 5 -17.7962 -0.0136 4 4 6 10.4510 0.0198 4 4 7 7.2082 -0.0077 4 4 8 -13.3589 -0.0043 4 4 9 6.1934 0.0046 4 4 10 5.6030 0.0018 4 4 11 -8.0884 0.0072 4 4 12 1.8245 -0.0039 4 4 13 3.7271 0.0002 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-0.5571 -0.0024 10 0 11 1.3149 0.0004 10 0 12 -1.6874 -0.0010 10 0 13 0.0542 -0.0042 10 0 14 1.6583 0.0029 10 0 15 -2.0089 -0.0021 10 0 16 1.8334 0.0022 10 0 17 1.3823 0.0008 10 0 18 -2.4749 -0.0038 10 0 19 0.8743 0.0040 10 0 20 0.9440 -0.0060 10 0 21 -1.0151 0.0017 10 1 0 0.1635 0.0176 10 1 1 1.3977 -0.0213 10 1 2 -0.6141 0.0030 10 1 3 -0.5602 0.0079 10 1 4 0.4846 -0.0045 10 1 5 0.3134 0.0045 10 1 6 0.1718 -0.0013 10 1 7 -0.3676 -0.0001 10 1 8 -0.2510 0.0038 10 1 9 0.5054 0.0023 10 1 10 -1.1158 -0.0025 10 1 11 0.9363 -0.0006 10 1 12 0.2959 0.0040 10 1 13 -2.6709 -0.0046 10 1 14 1.7303 -0.0002 10 1 15 -0.3283 -0.0011 10 1 16 -1.3402 -0.0011 10 1 17 2.8227 0.0056 10 1 18 -1.2164 -0.0066 10 1 19 -1.1545 0.0041 10 1 20 1.8448 0.0027 10 1 21 -0.2549 -0.0068 10 1 22 0.1311 0.0089 10 2 0 -1.6838 0.0223 10 2 1 1.0413 0.0032 10 2 2 0.8643 -0.0153 10 2 3 -0.8057 0.0075 10 2 4 -0.1535 0.0014 10 2 5 0.8202 -0.0008 10 2 6 0.3890 -0.0007 10 2 7 0.3529 -0.0013 10 2 8 -0.3254 -0.0008 10 2 9 0.6814 0.0011 10 2 10 -0.3117 0.0028 10 2 11 -1.0178 -0.0049 10 2 12 2.2396 0.0031 10 2 13 -1.5851 0.0018 10 2 14 -1.4832 -0.0025 10 2 15 1.9034 0.0016 10 2 16 -1.8894 -0.0051 10 2 17 0.9302 0.0059 10 2 18 1.4984 -0.0013 10 2 19 -2.3711 -0.0078 10 2 20 0.5495 0.0084 10 2 21 0.6415 -0.0058 10 2 22 -0.5924 0.0002 10 3 0 -1.6925 -0.0064 10 3 1 -0.8024 0.0185 10 3 2 0.8980 -0.0070 10 3 3 0.1864 -0.0041 10 3 4 -1.0184 0.0034 10 3 5 0.0630 0.0032 10 3 6 0.4046 0.0010 10 3 7 0.5372 -0.0024 10 3 8 0.0964 0.0035 10 3 9 -0.0089 -0.0022 10 3 10 1.4633 0.0026 10 3 11 -1.5159 0.0007 10 3 12 0.3562 -0.0044 10 3 13 1.8843 0.0037 10 3 14 -2.6427 -0.0018 10 3 15 0.2702 0.0017 10 3 16 0.0985 -0.0022 10 3 17 -1.4769 -0.0009 10 3 18 2.2633 0.0086 10 3 19 -0.3699 -0.0081 10 3 20 -1.1553 0.0003 10 3 21 1.2306 0.0028 10 3 22 -0.0765 -0.0095 10 4 0 -0.2787 -0.0188 10 4 1 -1.2668 0.0071 10 4 2 -0.1187 0.0042 10 4 3 0.3930 -0.0056 10 4 4 -0.3289 -0.0013 10 4 5 -0.6248 -0.0029 10 4 6 -0.1036 0.0053 10 4 7 -0.1719 -0.0047 10 4 8 0.8189 -0.0010 10 4 9 -0.7372 0.0037 10 4 10 0.9912 -0.0031 10 4 11 1.1263 0.0043 10 4 12 -1.7533 -0.0019 10 4 13 2.0099 -0.0003 10 4 14 0.4047 0.0016 10 4 15 -1.5354 -0.0017 10 4 16 0.7325 0.0019 10 4 17 -1.7668 -0.0046 10 4 18 -0.1863 0.0057 10 4 19 1.3344 0.0027 10 4 20 -1.4876 -0.0047 10 4 21 -0.3022 0.0073 10 4 22 0.6135 -0.0026 10 5 0 0.9928 -0.0097 10 5 1 -1.0625 -0.0052 10 5 2 0.0306 0.0100 10 5 3 0.0446 -0.0036 10 5 4 -0.2422 0.0043 10 5 5 -0.4322 -0.0036 10 5 6 0.2956 -0.0002 10 5 7 -0.9303 0.0047 10 5 8 0.0344 -0.0078 10 5 9 0.3988 0.0023 10 5 10 -1.2463 -0.0001 10 5 11 1.7504 -0.0016 10 5 12 -0.4409 0.0012 10 5 13 -0.5808 -0.0036 10 5 14 1.9658 0.0022 10 5 15 -0.4769 -0.0017 10 5 16 0.7786 -0.0007 10 5 17 0.0608 -0.0019 10 5 18 -1.6420 -0.0020 10 5 19 1.0927 0.0044 10 5 20 0.4419 -0.0056 10 5 21 -1.4404 0.0012 10 5 22 -0.4120 0.0026 10 5 23 0.1138 -0.0041 10 6 0 1.5348 0.0089 10 6 1 -0.6749 -0.0167 10 6 2 -0.6253 0.0072 10 6 3 0.8803 -0.0002 10 6 4 -0.1231 -0.0016 10 6 5 -1.1894 0.0072 10 6 6 0.3118 -0.0055 10 6 7 0.6408 0.0050 10 6 8 -1.4484 0.0009 10 6 9 0.8269 -0.0033 10 6 10 -0.5602 0.0038 10 6 11 -0.2607 0.0001 10 6 12 1.1780 0.0023 10 6 13 -1.2342 -0.0024 10 6 14 0.7897 -0.0005 10 6 15 -0.1386 0.0025 10 6 16 -0.0801 -0.0018 10 6 17 1.6093 -0.0002 10 6 18 -1.3072 -0.0029 10 6 19 -0.8314 0.0041 10 6 20 1.5933 -0.0010 10 6 21 0.3919 -0.0051 10 6 22 -1.0770 0.0042 10 6 23 0.0180 -0.0039 10 7 0 0.5579 0.0218 10 7 1 1.1444 -0.0059 10 7 2 -1.3493 -0.0087 10 7 3 0.3004 0.0081 10 7 4 1.4039 -0.0079 10 7 5 -0.6805 0.0042 10 7 6 -1.8380 0.0022 10 7 7 1.2025 -0.0033 10 7 8 -0.2075 0.0031 10 7 9 -1.0998 -0.0022 10 7 10 0.4294 0.0002 10 7 11 -0.9246 0.0005 10 7 12 0.8916 0.0029 10 7 13 -0.3764 0.0012 10 7 14 0.3817 -0.0034 10 7 15 1.0030 0.0023 10 7 16 -1.5444 0.0002 10 7 17 1.6553 0.0005 10 7 18 0.9855 -0.0028 10 7 19 -2.0641 -0.0007 10 7 20 -0.4486 0.0060 10 7 21 1.3751 -0.0056 10 7 22 -0.1556 0.0012 10 7 23 -1.1495 0.0036 10 8 0 -0.2673 0.0007 10 8 1 1.2301 0.0169 10 8 2 0.3032 -0.0122 10 8 3 -0.8644 0.0018 10 8 4 1.1216 0.0005 10 8 5 2.0192 -0.0050 10 8 6 -1.1066 0.0051 10 8 7 -1.0677 0.0002 10 8 8 1.6198 0.0006 10 8 9 -0.4451 -0.0011 10 8 10 -0.4198 0.0010 10 8 11 -0.8644 0.0004 10 8 12 -0.0940 0.0004 10 8 13 -0.1911 0.0047 10 8 14 -1.4261 -0.0018 10 8 15 2.1677 0.0002 10 8 16 -0.8335 0.0004 10 8 17 -1.0692 0.0001 10 8 18 2.8798 0.0023 10 8 19 0.2829 -0.0063 10 8 20 -1.4494 0.0027 10 8 21 0.2110 0.0010 10 8 22 1.3637 -0.0077 10 9 0 0.6449 -0.0208 10 9 1 -0.1293 0.0108 10 9 2 0.2798 0.0042 10 9 3 -0.3621 -0.0075 10 9 4 -0.8551 0.0021 10 9 5 1.0980 -0.0046 10 9 6 1.6690 -0.0013 10 9 7 -1.4125 -0.0002 10 9 8 -0.2426 0.0019 10 9 9 1.4613 -0.0024 10 9 10 0.5723 -0.0035 10 9 11 -0.3671 0.0029 10 9 12 -0.4911 -0.0015 10 9 13 1.1594 0.0036 10 9 14 -2.1434 0.0018 10 9 15 -0.1378 0.0003 10 9 16 2.0316 0.0040 10 9 17 -2.7879 -0.0027 10 9 18 -0.0164 0.0052 10 9 19 1.9244 0.0022 10 9 20 -0.2922 -0.0040 10 9 21 -0.8588 0.0064 10 9 22 0.6034 -0.0028 10 10 0 -0.3030 -0.0082 10 10 1 1.3326 -0.0082 10 10 2 -0.1639 0.0108 10 10 3 -0.1047 -0.0009 10 10 4 -0.0586 -0.0004 10 10 5 -0.8806 -0.0016 10 10 6 0.8481 -0.0006 10 10 7 0.9645 -0.0019 10 10 8 -1.5959 -0.0011 10 10 9 -0.5846 0.0036 10 10 10 1.1846 -0.0074 10 10 11 0.5633 -0.0023 10 10 12 -1.2059 -0.0009 10 10 13 1.0729 -0.0019 10 10 14 0.5989 0.0019 10 10 15 -2.5468 -0.0045 10 10 16 2.1730 0.0038 10 10 17 0.7490 0.0002 10 10 18 -2.2491 -0.0038 10 10 19 0.6218 0.0075 10 10 20 0.5344 -0.0007 10 10 21 -0.1835 0.0009 10 11 0 -3.1098 0.0084 10 11 1 0.1592 -0.0111 10 11 2 1.2467 0.0018 10 11 3 -0.7735 0.0044 10 11 4 0.1658 0.0010 10 11 5 0.4035 -0.0005 10 11 6 -0.7887 -0.0015 10 11 7 1.0012 0.0033 10 11 8 1.1440 -0.0046 10 11 9 -1.4536 0.0034 10 11 10 -0.3057 0.0021 10 11 11 1.5376 -0.0057 10 11 12 -0.5508 0.0007 10 11 13 -1.0800 -0.0029 10 11 14 1.6460 0.0025 10 11 15 -1.4746 -0.0025 10 11 16 -1.5704 -0.0050 10 11 17 2.3367 0.0048 10 11 18 -0.3915 -0.0052 10 11 19 -0.6434 -0.0015 10 11 20 0.1378 0.0038 10 11 21 0.3672 -0.0016 10 12 0 -0.5116 0.0121 10 12 1 -2.8315 -0.0026 10 12 2 0.6224 -0.0053 10 12 3 0.2673 0.0040 10 12 4 -1.2745 0.0013 10 12 5 0.2523 0.0035 10 12 6 0.0075 -0.0030 10 12 7 -1.4885 0.0026 10 12 8 1.0220 0.0017 10 12 9 0.7335 -0.0048 10 12 10 -1.5950 0.0041 10 12 11 0.8040 -0.0026 10 12 12 1.3619 -0.0016 10 12 13 -0.9405 -0.0012 10 12 14 0.4666 -0.0020 10 12 15 1.1407 0.0049 10 12 16 -2.0609 -0.0052 10 12 17 -0.2878 -0.0007 10 12 18 0.9564 0.0025 10 12 19 -0.4004 -0.0044 10 12 20 -0.2670 0.0005 10 13 0 2.7192 0.0056 10 13 1 -0.7763 0.0073 10 13 2 -1.2303 -0.0079 10 13 3 0.8774 0.0009 10 13 4 0.0935 0.0003 10 13 5 -0.6542 0.0024 10 13 6 0.9420 0.0032 10 13 7 -0.3650 -0.0022 10 13 8 -1.6048 0.0070 10 13 9 1.2608 0.0012 10 13 10 -0.5254 -0.0000 10 13 11 -1.3365 0.0024 10 13 12 1.0287 -0.0021 10 13 13 0.0174 0.0017 10 13 14 -0.5913 -0.0046 10 13 15 1.0233 -0.0003 10 13 16 0.2894 0.0018 10 13 17 -1.0912 -0.0056 10 13 18 0.2878 -0.0001 10 14 0 0.5206 -0.0088 10 14 1 1.3011 0.0115 10 14 2 -0.5940 -0.0018 10 14 3 -0.6342 -0.0051 10 14 4 0.2188 0.0011 10 14 5 0.0722 -0.0046 10 14 6 -0.1506 0.0038 10 14 7 1.4629 -0.0012 10 14 8 -0.7420 -0.0022 10 14 9 -0.5287 0.0066 10 14 10 1.4067 0.0010 10 14 11 -0.8088 0.0023 10 14 12 0.0411 0.0012 10 14 13 0.5296 0.0032 10 14 14 -0.4265 0.0040 10 14 15 -0.1204 -0.0023 10 14 16 0.3412 0.0030 10 14 17 -0.2175 0.0003 10 15 0 -0.3031 -0.0133 10 15 1 0.4539 0.0008 10 15 2 0.5578 0.0091 10 15 3 0.3138 -0.0056 10 15 4 -0.9572 0.0022 10 15 5 -0.0151 -0.0033 10 15 6 -0.2109 -0.0037 10 15 7 -0.0773 0.0062 10 15 8 0.9541 -0.0053 10 15 9 -1.3505 -0.0012 10 15 10 0.0307 0.0046 10 15 11 0.4890 -0.0018 10 15 12 -0.2140 -0.0008 10 15 13 0.6695 -0.0002 10 15 14 0.1471 0.0038 10 15 15 0.3658 0.0020 10 16 3 0.9974 0.0002 10 16 4 0.6571 -0.0017 10 16 5 -0.9782 0.0035 10 16 6 0.6376 -0.0103 10 16 7 -0.2748 0.0020 10 16 8 0.4578 0.0053 10 16 9 0.5051 -0.0074 10 16 10 -1.1735 0.0040 10 16 11 -0.1342 0.0040 10 16 12 -0.2056 -0.0037 11 -6 0 -0.3163 -0.0066 11 -6 1 -0.2813 -0.0010 11 -6 2 0.6573 0.0068 11 -6 3 0.0426 -0.0032 11 -6 4 -0.8996 0.0001 11 -6 5 0.0657 0.0030 11 -6 6 0.3102 -0.0009 11 -5 0 0.4016 0.0008 11 -5 1 -0.4690 -0.0064 11 -5 2 0.1559 0.0060 11 -5 3 0.4354 0.0014 11 -5 4 -0.7276 0.0018 11 -5 5 -0.5322 0.0028 11 -5 6 0.3348 0.0009 11 -5 7 -0.6571 0.0039 11 -5 8 -0.0237 -0.0050 11 -5 9 0.6897 0.0012 11 -5 10 -1.2238 0.0027 11 -4 0 0.9961 0.0080 11 -4 1 0.0079 -0.0109 11 -4 2 0.2058 -0.0011 11 -4 3 1.1522 0.0018 11 -4 4 -0.2414 -0.0048 11 -4 5 -0.5459 0.0066 11 -4 6 0.9842 -0.0029 11 -4 7 -0.0443 0.0035 11 -4 8 -1.2617 0.0052 11 -4 9 0.8545 -0.0060 11 -4 10 -0.0385 0.0075 11 -4 11 -1.5599 0.0017 11 -4 12 0.5613 -0.0031 11 -3 0 0.4884 0.0128 11 -3 1 0.2300 0.0013 11 -3 2 -1.0826 -0.0123 11 -3 3 1.2496 0.0066 11 -3 4 0.7518 -0.0067 11 -3 5 -1.7130 -0.0019 11 -3 6 0.7532 0.0044 11 -3 7 1.9182 -0.0084 11 -3 8 -1.1148 0.0058 11 -3 9 -0.3030 -0.0031 11 -3 10 1.5519 -0.0045 11 -3 11 -0.9343 0.0073 11 -3 12 -0.2146 -0.0021 11 -3 13 0.7951 0.0008 11 -3 14 -0.9531 0.0018 11 -2 0 -0.5607 -0.0077 11 -2 1 1.3893 0.0179 11 -2 2 -0.9700 -0.0089 11 -2 3 -0.8216 -0.0048 11 -2 4 2.5437 0.0065 11 -2 5 -1.2060 -0.0090 11 -2 6 -2.2649 0.0050 11 -2 7 2.2321 -0.0002 11 -2 8 0.6341 -0.0030 11 -2 9 -1.9428 0.0049 11 -2 10 0.9497 -0.0067 11 -2 11 0.2536 0.0008 11 -2 12 -0.9551 0.0012 11 -2 13 1.3522 -0.0028 11 -2 14 -0.2150 -0.0001 11 -2 15 -0.5902 -0.0001 11 -1 0 -1.2190 -0.0179 11 -1 1 0.1756 0.0047 11 -1 2 1.3752 0.0136 11 -1 3 -2.1669 -0.0120 11 -1 4 1.2032 0.0012 11 -1 5 2.5939 -0.0003 11 -1 6 -2.7772 -0.0058 11 -1 7 -0.3167 0.0025 11 -1 8 2.8399 -0.0031 11 -1 9 -1.1173 0.0014 11 -1 10 -0.6819 -0.0012 11 -1 11 0.9944 -0.0022 11 -1 12 -1.6491 0.0023 11 -1 13 0.5417 -0.0010 11 -1 14 1.1603 0.0000 11 -1 15 -1.1721 -0.0018 11 -1 16 0.5044 0.0016 11 0 0 0.2671 0.0026 11 0 1 -1.5584 -0.0142 11 0 2 0.9591 0.0131 11 0 3 -0.3372 0.0073 11 0 4 -2.1336 -0.0048 11 0 5 2.5018 0.0028 11 0 6 0.1898 0.0006 11 0 7 -2.7446 -0.0003 11 0 8 1.8290 -0.0011 11 0 9 1.2571 0.0010 11 0 10 -1.3820 -0.0014 11 0 11 1.4500 -0.0040 11 0 12 -0.6997 0.0009 11 0 13 -1.5930 -0.0017 11 0 14 2.0705 0.0005 11 0 15 -0.3762 -0.0014 11 0 16 -0.5063 0.0014 11 0 17 0.7888 0.0021 11 0 18 -0.5470 -0.0077 11 1 0 0.5518 0.0127 11 1 1 0.1730 -0.0089 11 1 2 -0.5543 -0.0067 11 1 3 1.0058 0.0079 11 1 4 -1.3228 0.0029 11 1 5 0.0622 -0.0020 11 1 6 1.7742 -0.0006 11 1 7 -1.9112 0.0050 11 1 8 -0.7216 -0.0008 11 1 9 1.9648 0.0015 11 1 10 -1.2249 0.0050 11 1 11 0.1320 -0.0037 11 1 12 1.6779 0.0013 11 1 13 -2.7098 0.0001 11 1 14 0.2159 -0.0012 11 1 15 1.5210 -0.0000 11 1 16 -1.2781 -0.0036 11 1 17 0.6402 0.0070 11 1 18 -0.4424 -0.0047 11 2 0 -1.0980 0.0104 11 2 1 0.4587 0.0034 11 2 2 0.0167 -0.0072 11 2 3 0.0740 -0.0003 11 2 4 -0.5231 0.0012 11 2 5 -0.2521 0.0044 11 2 6 1.6640 -0.0053 11 2 7 -0.3395 -0.0012 11 2 8 -1.4430 0.0038 11 2 9 1.7600 -0.0051 11 2 10 0.5013 0.0043 11 2 11 -1.8963 0.0003 11 2 12 2.2541 -0.0025 11 2 13 -0.0315 0.0032 11 2 14 -2.6826 -0.0014 11 2 15 1.6587 0.0029 11 2 16 -0.1974 -0.0045 11 2 17 -0.3221 0.0011 11 2 18 0.7406 0.0062 11 2 19 -1.4166 -0.0134 11 3 0 -0.2797 -0.0008 11 3 1 -0.8146 0.0108 11 3 2 0.1159 -0.0065 11 3 3 0.6404 0.0012 11 3 4 -0.9551 -0.0015 11 3 5 -1.4808 0.0008 11 3 6 1.5323 0.0062 11 3 7 0.5323 -0.0060 11 3 8 -2.0449 0.0039 11 3 9 0.2308 0.0005 11 3 10 2.5536 -0.0023 11 3 11 -1.3593 0.0043 11 3 12 -0.5515 -0.0038 11 3 13 2.9627 0.0012 11 3 14 -1.7575 -0.0006 11 3 15 -0.9050 0.0011 11 3 16 1.1258 0.0021 11 3 17 -1.0875 -0.0058 11 3 18 0.9252 0.0096 11 3 19 -0.2984 -0.0013 11 4 0 0.8836 -0.0184 11 4 1 -0.2519 0.0109 11 4 2 -0.6427 0.0017 11 4 3 0.5269 -0.0077 11 4 4 0.9511 0.0048 11 4 5 -2.3162 -0.0074 11 4 6 -0.1042 0.0019 11 4 7 2.0027 0.0012 11 4 8 -1.2973 -0.0044 11 4 9 -2.2490 0.0037 11 4 10 1.5327 -0.0022 11 4 11 1.6959 0.0024 11 4 12 -2.3979 -0.0000 11 4 13 1.3653 -0.0015 11 4 14 1.9053 0.0019 11 4 15 -1.7418 -0.0028 11 4 16 0.7532 0.0040 11 4 17 -0.2932 -0.0041 11 4 18 -0.4943 -0.0003 11 4 19 0.9299 0.0100 11 4 20 -1.3997 -0.0079 11 5 0 0.8364 -0.0099 11 5 1 0.1263 -0.0094 11 5 2 0.2197 0.0167 11 5 3 -0.6027 -0.0048 11 5 4 1.1848 0.0013 11 5 5 -0.2142 0.0044 11 5 6 -2.0206 -0.0061 11 5 7 1.4791 0.0033 11 5 8 1.0778 -0.0015 11 5 9 -1.8859 -0.0006 11 5 10 -1.8120 -0.0005 11 5 11 2.2680 -0.0006 11 5 12 0.0101 0.0017 11 5 13 -2.1341 -0.0038 11 5 14 2.2191 0.0016 11 5 15 0.1370 -0.0013 11 5 16 -0.3408 -0.0000 11 5 17 1.0942 0.0013 11 5 18 -0.7837 -0.0072 11 5 19 0.8425 0.0055 11 5 20 0.5810 0.0003 11 6 0 0.3592 0.0145 11 6 1 0.0560 -0.0186 11 6 2 -0.0097 -0.0003 11 6 3 0.6354 0.0091 11 6 4 -0.1599 -0.0060 11 6 5 0.8044 0.0058 11 6 6 -1.2658 0.0004 11 6 7 -0.4544 -0.0017 11 6 8 1.2748 0.0023 11 6 9 0.6148 0.0014 11 6 10 -2.0009 0.0013 11 6 11 -1.0506 -0.0008 11 6 12 2.4992 0.0041 11 6 13 -1.5311 -0.0010 11 6 14 -0.6202 -0.0014 11 6 15 1.4343 0.0022 11 6 16 -1.0356 -0.0013 11 6 17 0.7504 0.0043 11 6 18 0.0632 -0.0033 11 6 19 -0.7119 -0.0015 11 6 20 1.2940 0.0075 11 7 0 -0.7663 0.0124 11 7 1 1.0621 0.0045 11 7 2 -1.0817 -0.0150 11 7 3 0.6402 0.0039 11 7 4 1.0501 0.0001 11 7 5 0.1905 -0.0015 11 7 6 -0.2188 0.0021 11 7 7 -0.6189 -0.0024 11 7 8 0.1088 -0.0014 11 7 9 0.6088 -0.0005 11 7 10 0.7477 0.0025 11 7 11 -2.6543 -0.0018 11 7 12 0.2334 0.0014 11 7 13 1.4555 0.0033 11 7 14 -1.7754 -0.0027 11 7 15 1.1774 0.0014 11 7 16 0.0111 -0.0011 11 7 17 -0.5651 0.0020 11 7 18 1.2510 0.0031 11 7 19 -0.7198 -0.0061 11 7 20 -0.3632 0.0041 11 8 0 -0.6736 -0.0059 11 8 1 0.6249 0.0117 11 8 2 0.0940 -0.0029 11 8 3 -1.5303 -0.0054 11 8 4 1.4466 0.0007 11 8 5 1.1360 0.0003 11 8 6 -0.1175 0.0028 11 8 7 -0.1404 -0.0019 11 8 8 0.5116 -0.0001 11 8 9 -0.3635 -0.0020 11 8 10 1.3625 0.0007 11 8 11 0.2417 0.0013 11 8 12 -2.5853 -0.0020 11 8 13 1.1033 0.0036 11 8 14 -0.7130 -0.0008 11 8 15 -0.7202 -0.0000 11 8 16 1.2997 0.0009 11 8 17 -1.2880 -0.0027 11 8 18 0.3874 0.0054 11 8 19 1.1216 -0.0009 11 9 0 0.3285 -0.0064 11 9 1 -0.4343 0.0015 11 9 2 1.0629 0.0031 11 9 3 -1.6749 -0.0026 11 9 4 -1.0328 -0.0025 11 9 5 1.4515 -0.0048 11 9 6 0.1383 0.0046 11 9 7 -0.5282 -0.0008 11 9 8 0.5599 -0.0039 11 9 9 0.0767 0.0003 11 9 10 -0.2595 -0.0030 11 9 11 2.2815 0.0009 11 9 12 -0.5979 -0.0018 11 9 13 -0.7691 0.0013 11 9 14 0.8011 0.0016 11 9 15 -1.5965 -0.0023 11 9 16 0.8996 0.0040 11 9 17 0.1059 -0.0014 11 9 18 -1.7608 0.0002 11 9 19 0.4174 0.0071 11 10 0 -0.5784 -0.0006 11 10 1 -0.2532 0.0009 11 10 2 1.0942 0.0042 11 10 3 0.3320 -0.0008 11 10 4 -2.0673 0.0038 11 10 5 0.3374 -0.0049 11 10 6 0.5966 -0.0010 11 10 7 -0.7034 0.0074 11 10 8 0.0465 -0.0054 11 10 9 0.3303 -0.0015 11 10 10 -1.0358 -0.0006 11 10 11 0.3553 -0.0023 11 10 12 1.3938 -0.0023 11 10 13 -0.8096 -0.0033 11 10 14 0.6380 0.0021 11 10 15 -0.4514 -0.0047 11 10 16 -0.5990 -0.0020 11 10 17 1.8555 0.0024 11 10 18 -0.4508 -0.0042 11 11 0 -0.9444 -0.0010 11 11 1 -1.3669 -0.0031 11 11 2 0.1408 0.0055 11 11 3 1.5761 -0.0007 11 11 4 -1.0611 0.0018 11 11 5 -0.9438 0.0037 11 11 6 0.9288 -0.0066 11 11 7 -0.7170 0.0075 11 11 8 -0.0098 0.0041 11 11 9 0.8391 -0.0049 11 11 10 -0.3185 0.0024 11 11 11 -0.7016 0.0008 11 11 12 0.6051 0.0009 11 11 13 0.1843 -0.0031 11 11 14 -0.1483 0.0005 11 11 15 0.2786 0.0013 11 11 16 -1.4836 -0.0061 11 11 17 0.2512 -0.0001 11 12 0 1.3785 0.0028 11 12 1 -0.9621 -0.0053 11 12 2 -1.4131 -0.0000 11 12 3 1.0292 0.0035 11 12 4 0.7402 -0.0028 11 12 5 -1.5648 0.0051 11 12 6 0.4402 -0.0035 11 12 7 -0.3632 -0.0019 11 12 8 -1.4338 0.0098 11 12 9 0.9526 -0.0029 11 12 10 0.2040 -0.0020 11 12 11 -0.4012 0.0019 11 12 12 0.0190 0.0012 11 12 13 0.2654 0.0013 11 12 14 0.2795 -0.0025 11 12 15 0.6593 0.0028 11 12 16 -0.2355 -0.0000 11 13 0 1.3317 0.0030 11 13 1 1.2400 0.0005 11 13 2 -0.8312 -0.0053 11 13 3 -0.5148 0.0023 11 13 4 1.5209 -0.0015 11 13 5 0.0215 0.0019 11 13 6 -0.2732 0.0025 11 13 7 1.0952 -0.0067 11 13 8 -1.6823 0.0070 11 13 9 -0.3732 0.0056 11 13 10 0.8850 -0.0037 11 13 11 -0.6150 0.0026 11 13 12 -0.0076 0.0007 11 13 13 -0.4265 0.0022 11 13 14 -0.1767 0.0012 11 13 15 0.4574 -0.0017 11 14 3 -0.6556 -0.0020 11 14 4 -0.1658 -0.0016 11 14 5 0.9101 -0.0033 11 14 6 -0.2380 0.0046 11 14 7 1.0023 -0.0060 11 14 8 0.2430 -0.0038 11 14 9 -1.5258 0.0084 11 14 10 0.9875 -0.0022 11 14 11 0.2095 -0.0008 11 14 12 0.0794 0.0042 12 -2 1 0.4761 0.0062 12 -2 2 1.0663 0.0066 12 -2 3 -1.8986 -0.0114 12 -2 4 0.4241 0.0041 12 -2 5 1.0070 0.0030 12 -2 6 -2.1432 -0.0044 12 -2 7 0.0831 0.0032 12 -2 8 1.9286 -0.0013 12 -1 0 -0.1484 0.0016 12 -1 1 -1.7625 -0.0043 12 -1 2 1.9694 0.0084 12 -1 3 -0.0204 0.0013 12 -1 4 -2.2845 -0.0076 12 -1 5 2.1311 0.0032 12 -1 6 0.1957 0.0002 12 -1 7 -2.1719 -0.0023 12 -1 8 1.8660 -0.0003 12 -1 9 1.1017 0.0001 12 -1 10 -1.5524 0.0008 12 0 0 1.5463 0.0015 12 0 1 -1.4479 0.0002 12 0 2 -0.8748 0.0012 12 0 3 2.4601 0.0064 12 0 4 -2.0544 0.0028 12 0 5 -1.3502 -0.0024 12 0 6 2.0170 0.0028 12 0 7 -1.5757 0.0036 12 0 8 -0.6518 -0.0019 12 0 9 2.2685 -0.0013 12 0 10 -0.7179 0.0019 12 0 11 -0.2852 -0.0020 12 0 12 0.7734 -0.0030 12 1 0 0.5417 0.0017 12 1 1 1.3180 -0.0065 12 1 2 -1.8888 0.0014 12 1 3 1.1861 -0.0018 12 1 4 1.4971 0.0011 12 1 5 -2.0221 0.0035 12 1 6 0.3258 -0.0042 12 1 7 0.2071 0.0036 12 1 8 -1.5832 0.0051 12 1 9 1.2824 -0.0023 12 1 10 0.1694 0.0025 12 1 11 -1.6288 0.0030 12 1 12 1.3933 -0.0021 12 1 13 -0.3984 -0.0002 12 2 0 -1.1045 0.0127 12 2 1 1.0093 -0.0026 12 2 2 -0.3065 -0.0057 12 2 3 -0.9624 0.0056 12 2 4 1.3279 -0.0058 12 2 5 0.0009 0.0016 12 2 6 -0.1291 0.0014 12 2 7 0.2140 -0.0063 12 2 8 -1.2938 0.0038 12 2 9 0.9303 0.0002 12 2 10 1.9475 -0.0029 12 2 11 -2.1491 0.0029 12 2 12 -0.0909 -0.0001 12 2 13 1.8669 -0.0008 12 2 14 -1.7375 0.0019 12 3 0 -0.2034 -0.0049 12 3 1 -0.0834 0.0143 12 3 2 0.2932 -0.0093 12 3 3 -0.6111 -0.0005 12 3 4 0.2922 0.0050 12 3 5 -0.4894 -0.0057 12 3 6 0.1365 0.0046 12 3 7 0.8829 -0.0003 12 3 8 -2.0497 -0.0016 12 3 9 -1.3470 0.0035 12 3 10 3.2146 -0.0017 12 3 11 0.2938 0.0003 12 3 12 -2.8310 0.0004 12 3 13 2.1734 -0.0019 12 3 14 0.8455 0.0009 12 3 15 -1.5749 0.0016 12 4 0 0.5715 -0.0187 12 4 1 0.0995 0.0050 12 4 2 0.3971 0.0093 12 4 3 -0.7263 -0.0112 12 4 4 0.9151 0.0023 12 4 5 0.1023 -0.0003 12 4 6 -1.2023 -0.0042 12 4 7 1.8402 0.0015 12 4 8 0.2821 -0.0015 12 4 9 -3.6636 0.0007 12 4 10 0.0158 -0.0003 12 4 11 3.6194 0.0003 12 4 12 -2.2051 0.0014 12 4 13 -1.7563 -0.0021 12 4 14 2.8413 -0.0004 12 4 15 -0.4796 0.0016 12 5 0 0.2525 0.0010 12 5 1 0.0141 -0.0133 12 5 2 0.8713 0.0116 12 5 3 -0.5152 0.0048 12 5 4 -0.5711 -0.0050 12 5 5 1.5511 0.0035 12 5 6 -1.1319 0.0002 12 5 7 -0.1456 -0.0010 12 5 8 2.5019 -0.0004 12 5 9 -0.6687 0.0012 12 5 10 -3.6070 -0.0011 12 5 11 1.6828 -0.0016 12 5 12 2.5772 0.0024 12 5 13 -3.4241 -0.0014 12 5 14 -0.0760 -0.0026 12 5 15 1.6994 0.0011 12 6 0 -0.6261 0.0090 12 6 1 0.0975 -0.0076 12 6 2 0.1257 -0.0074 12 6 3 1.0562 0.0072 12 6 4 -1.0154 0.0008 12 6 5 0.3894 -0.0022 12 6 6 0.5010 0.0004 12 6 7 -1.0622 0.0020 12 6 8 0.5662 -0.0004 12 6 9 1.8487 0.0016 12 6 10 -1.0429 0.0026 12 6 11 -3.0596 -0.0021 12 6 12 2.6467 0.0023 12 6 13 1.0129 0.0023 12 6 14 -2.7689 -0.0024 12 6 15 0.8615 -0.0007 12 7 0 -0.9761 0.0030 12 7 1 0.0894 0.0021 12 7 2 -0.3231 -0.0053 12 7 3 0.2798 -0.0022 12 7 4 0.6930 0.0014 12 7 5 -0.2681 0.0015 12 7 6 0.2870 -0.0039 12 7 7 0.0018 -0.0028 12 7 8 0.1648 0.0009 12 7 9 -0.0447 -0.0016 12 7 10 1.8403 0.0017 12 7 11 -1.2495 -0.0017 12 7 12 -2.4951 -0.0011 12 7 13 2.5659 0.0032 12 7 14 -0.1679 -0.0008 12 7 15 -1.2753 -0.0018 12 8 0 0.3117 0.0034 12 8 1 -0.8818 0.0003 12 8 2 0.5046 -0.0029 12 8 3 -0.9208 0.0019 12 8 4 -0.0627 -0.0018 12 8 5 0.7182 0.0011 12 8 6 0.0453 0.0049 12 8 7 -0.7663 -0.0052 12 8 8 1.0884 -0.0020 12 8 9 0.1994 0.0013 12 8 10 -0.5182 0.0011 12 8 11 2.6805 -0.0005 12 8 12 -1.6116 -0.0034 12 8 13 -1.6615 0.0025 12 8 14 1.7423 0.0006 12 8 15 -0.3985 -0.0014 12 9 0 1.0206 0.0020 12 9 1 -0.8728 0.0072 12 9 2 0.1181 -0.0072 12 9 3 0.4067 -0.0023 12 9 4 -1.5494 0.0045 12 9 5 -0.1280 -0.0060 12 9 6 0.9771 0.0032 12 9 7 -0.9641 0.0035 12 9 8 -0.9132 -0.0073 12 9 9 1.9027 -0.0020 12 9 10 -1.2653 0.0028 12 9 11 0.1123 0.0018 12 9 12 2.8950 -0.0051 12 9 13 -1.6962 -0.0006 12 9 14 -0.8049 0.0031 12 10 1 0.2570 0.0105 12 10 2 -0.8645 0.0061 12 10 3 1.2887 -0.0095 12 10 4 -0.1693 0.0050 12 10 5 -1.5078 0.0034 12 10 6 0.4930 -0.0049 12 10 7 0.6933 0.0075 12 10 8 -1.6462 0.0009 12 10 9 0.1480 -0.0074 12 10 10 1.2308 -0.0006 12 10 11 -2.3036 0.0055 12 10 12 0.9276 -0.0016 12 10 13 2.0117 -0.0070 12 11 4 1.3597 -0.0072 12 11 5 -0.8456 0.0078 12 11 6 -0.7878 -0.0012 12 11 7 0.5980 -0.0000 12 11 8 0.0945 0.0091 12 11 9 -1.0825 -0.0013 12 11 10 0.9234 -0.0052 0 0 0 0.0 0.0 ; _shelx_fab_checksum 40809 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_rom205_sq _database_code_depnum_ccdc_archive 'CCDC 2122221' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-15 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_method SHELXL-2016/6 _shelx_SHELXL_version_number 2016/6 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C68 H88 N4 O4 P2' _chemical_formula_sum 'C68 H88 N4 O4 P2' _chemical_formula_weight 1087.36 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 60 _space_group_name_H-M_alt 'P b c n' _space_group_name_Hall '-P 2n 2ab' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 49.285(2) _cell_length_b 13.0502(6) _cell_length_c 22.4161(11) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 14417.5(12) _cell_formula_units_Z 8 _cell_measurement_temperature 110(2) _cell_measurement_reflns_used 155807 _cell_measurement_theta_min 1.614 _cell_measurement_theta_max 28.453 _exptl_crystal_description plate _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.002 _exptl_crystal_F_000 4688 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.258 _exptl_crystal_size_mid 0.158 _exptl_crystal_size_min 0.050 _exptl_absorpt_coefficient_mu 0.104 _shelx_estimated_absorpt_T_min 0.974 _shelx_estimated_absorpt_T_max 0.995 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.980 _exptl_absorpt_correction_T_max 0.995 _exptl_absorpt_process_details 'Sadabs, Bruker-AXS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 110(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'ImuS micro focus' _diffrn_measurement_device_type 'ApexDuo, Bruker-AXS' _diffrn_measurement_method '0.4 deg. \f and \w scans' _diffrn_detector_area_resol_mean 1.75 _diffrn_reflns_number 155807 _diffrn_reflns_av_unetI/netI 0.0459 _diffrn_reflns_av_R_equivalents 0.0769 _diffrn_reflns_limit_h_min -66 _diffrn_reflns_limit_h_max 63 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_theta_min 1.614 _diffrn_reflns_theta_max 28.453 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 18163 _reflns_number_gt 12938 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. The structure contains additional molecules of disordered n-hexaane solvent and traces of acetonitrile and DCM, which could not be modelled by discrete atoms. Their contribution was subtracted from the diffraction pattern by the Squeeze technique, using the PLATON software (Spek, 2009). The T-butyl fragment also reveals partial disorder. ; _computing_data_collection 'Apex3, Bruker-AXS' _computing_cell_refinement 'Saint, Bruker-AXS' _computing_data_reduction 'Saint, Bruker-AXS' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0644P)^2^+11.3078P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary diffmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 18163 _refine_ls_number_parameters 758 _refine_ls_number_restraints 79 _refine_ls_R_factor_all 0.0866 _refine_ls_R_factor_gt 0.0613 _refine_ls_wR_factor_ref 0.1648 _refine_ls_wR_factor_gt 0.1518 _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_restrained_S_all 1.057 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 0.33876(2) 0.42113(4) 0.49603(2) 0.02029(11) Uani 1 1 d . . . . . P2 P 0.37203(2) 0.30553(4) 0.49514(2) 0.02637(12) Uani 1 1 d . . . . . O3 O 0.31602(3) 0.38702(10) 0.44511(5) 0.0236(3) Uani 1 1 d . . . . . C5 C 0.27280(4) 0.29736(15) 0.43182(8) 0.0271(4) Uani 1 1 d . . . . . C4 C 0.29437(4) 0.33088(14) 0.46631(8) 0.0238(4) Uani 1 1 d . . . . . C6 C 0.25329(4) 0.23919(16) 0.46229(9) 0.0298(4) Uani 1 1 d . . . . . H6 H 0.238015 0.215158 0.440546 0.036 Uiso 1 1 calc R U . . . C7 C 0.25505(4) 0.21463(15) 0.52276(9) 0.0282(4) Uani 1 1 d . . . . . C8 C 0.27677(4) 0.25328(15) 0.55576(9) 0.0272(4) Uani 1 1 d . . . . . H8 H 0.278424 0.238008 0.597039 0.033 Uiso 1 1 calc R U . . . C9 C 0.29587(4) 0.31417(14) 0.52759(8) 0.0223(4) Uani 1 1 d . . . . . N10 N 0.31821(3) 0.36755(12) 0.55079(7) 0.0213(3) Uani 1 1 d . . . . . C11 C 0.32101(4) 0.40884(14) 0.60806(8) 0.0207(4) Uani 1 1 d . . . . . C12 C 0.30696(4) 0.38390(15) 0.65972(8) 0.0245(4) Uani 1 1 d . . . . . H12 H 0.294334 0.328890 0.660030 0.029 Uiso 1 1 calc R U . . . C13 C 0.31175(4) 0.44116(16) 0.71115(8) 0.0272(4) Uani 1 1 d . . . . . H13 H 0.302167 0.425154 0.746732 0.033 Uiso 1 1 calc R U . . . C14 C 0.33017(4) 0.52067(16) 0.71118(8) 0.0281(4) Uani 1 1 d . . . . . H14 H 0.333066 0.558852 0.746696 0.034 Uiso 1 1 calc R U . . . C15 C 0.34458(4) 0.54569(15) 0.65975(8) 0.0248(4) Uani 1 1 d . . . . . H15 H 0.357228 0.600615 0.659872 0.030 Uiso 1 1 calc R U . . . C16 C 0.34012(4) 0.48882(14) 0.60827(8) 0.0209(4) Uani 1 1 d . . . . . N17 N 0.35135(3) 0.50169(12) 0.55128(7) 0.0219(3) Uani 1 1 d . . . . . C18 C 0.36658(4) 0.58451(15) 0.52886(8) 0.0234(4) Uani 1 1 d . . . . . C19 C 0.38285(4) 0.65565(17) 0.55717(9) 0.0296(4) Uani 1 1 d . . . . . H19 H 0.385098 0.653824 0.599245 0.036 Uiso 1 1 calc R U . . . C20 C 0.39597(4) 0.73042(18) 0.52302(9) 0.0334(5) Uani 1 1 d . . . . . C21 C 0.39163(4) 0.73239(17) 0.46158(9) 0.0321(5) Uani 1 1 d . . . . . H21 H 0.400262 0.784621 0.438973 0.039 Uiso 1 1 calc R U . . . C22 C 0.37531(4) 0.66198(16) 0.43137(8) 0.0257(4) Uani 1 1 d . . . . . C23 C 0.36409(4) 0.58578(15) 0.46690(8) 0.0230(4) Uani 1 1 d . . . . . O24 O 0.34872(3) 0.50592(10) 0.44520(5) 0.0225(3) Uani 1 1 d . . . . . C25 C 0.27031(5) 0.32371(16) 0.36531(9) 0.0315(5) Uani 1 1 d . . . . . C26 C 0.24506(5) 0.2758(2) 0.33732(10) 0.0476(7) Uani 1 1 d . . . . . H26A H 0.244184 0.294152 0.294975 0.071 Uiso 1 1 calc R U . . . H26B H 0.228834 0.301372 0.357745 0.071 Uiso 1 1 calc R U . . . H26C H 0.245951 0.201070 0.341291 0.071 Uiso 1 1 calc R U . . . C27 C 0.29522(5) 0.28398(19) 0.33108(9) 0.0396(5) Uani 1 1 d . . . . . H27A H 0.293308 0.300491 0.288637 0.059 Uiso 1 1 calc R U . . . H27B H 0.296596 0.209540 0.335975 0.059 Uiso 1 1 calc R U . . . H27C H 0.311645 0.316599 0.346804 0.059 Uiso 1 1 calc R U . . . C28 C 0.26843(5) 0.44062(17) 0.35834(10) 0.0392(5) Uani 1 1 d . . . . . H28A H 0.265941 0.457831 0.316134 0.059 Uiso 1 1 calc R U . . . H28B H 0.285177 0.472272 0.373032 0.059 Uiso 1 1 calc R U . . . H28C H 0.252967 0.466333 0.381393 0.059 Uiso 1 1 calc R U . . . C29 C 0.23454(5) 0.14489(16) 0.55435(10) 0.0344(5) Uani 1 1 d . . . . . C30 C 0.21092(5) 0.11558(18) 0.51369(10) 0.0399(5) Uani 1 1 d . . . . . H30A H 0.202095 0.177850 0.498841 0.060 Uiso 1 1 calc R U . . . H30B H 0.197766 0.074648 0.536210 0.060 Uiso 1 1 calc R U . . . H30C H 0.217742 0.075427 0.479926 0.060 Uiso 1 1 calc R U . . . C31 C 0.22276(6) 0.2007(2) 0.60898(11) 0.0494(7) Uani 1 1 d . . . . . H31A H 0.213991 0.264380 0.596097 0.074 Uiso 1 1 calc R U . . . H31B H 0.237407 0.216699 0.637033 0.074 Uiso 1 1 calc R U . . . H31C H 0.209363 0.156603 0.628599 0.074 Uiso 1 1 calc R U . . . C32 C 0.24873(6) 0.04667(19) 0.57439(13) 0.0511(7) Uani 1 1 d . . . . . H32A H 0.254525 0.007640 0.539279 0.077 Uiso 1 1 calc R U . . . H32B H 0.236153 0.005202 0.598128 0.077 Uiso 1 1 calc R U . . . H32C H 0.264623 0.064166 0.598617 0.077 Uiso 1 1 calc R U . . . C33 C 0.41466(6) 0.8076(2) 0.55479(10) 0.0472(7) Uani 1 1 d . . . . . C34 C 0.39783(6) 0.8703(2) 0.59958(11) 0.0531(7) Uani 1 1 d . . . . . H34A H 0.383540 0.907559 0.578278 0.080 Uiso 1 1 calc R U . . . H34B H 0.409662 0.919303 0.620128 0.080 Uiso 1 1 calc R U . . . H34C H 0.389583 0.824109 0.628874 0.080 Uiso 1 1 calc R U . . . C35 C 0.43731(6) 0.7503(3) 0.58681(11) 0.0593(8) Uani 1 1 d . . . . . H35A H 0.448010 0.711550 0.557666 0.089 Uiso 1 1 calc R U . . . H35B H 0.429434 0.702989 0.616010 0.089 Uiso 1 1 calc R U . . . H35C H 0.449073 0.799508 0.607357 0.089 Uiso 1 1 calc R U . . . C36 C 0.42810(7) 0.8822(3) 0.51072(12) 0.0733(11) Uani 1 1 d . . . . . H36A H 0.437224 0.843317 0.479157 0.110 Uiso 1 1 calc R U . . . H36B H 0.441434 0.924403 0.531909 0.110 Uiso 1 1 calc R U . . . H36C H 0.414217 0.926524 0.492992 0.110 Uiso 1 1 calc R U . . . C37 C 0.36914(4) 0.66814(16) 0.36452(8) 0.0284(4) Uani 1 1 d . . . . . C38 C 0.38428(5) 0.75735(18) 0.33516(9) 0.0396(6) Uani 1 1 d . . . . . H38A H 0.379376 0.761062 0.292851 0.059 Uiso 1 1 calc R U . . . H38B H 0.403880 0.746496 0.338920 0.059 Uiso 1 1 calc R U . . . H38C H 0.379267 0.821600 0.354937 0.059 Uiso 1 1 calc R U . . . C39 C 0.37769(5) 0.56904(16) 0.33300(9) 0.0318(5) Uani 1 1 d . . . . . H39A H 0.373961 0.574957 0.290196 0.048 Uiso 1 1 calc R U . . . H39B H 0.367434 0.511277 0.349496 0.048 Uiso 1 1 calc R U . . . H39C H 0.397138 0.557519 0.339155 0.048 Uiso 1 1 calc R U . . . C40 C 0.33854(5) 0.68583(17) 0.35605(9) 0.0335(5) Uani 1 1 d . . . . . H40A H 0.334363 0.689186 0.313350 0.050 Uiso 1 1 calc R U . . . H40B H 0.333304 0.750402 0.375167 0.050 Uiso 1 1 calc R U . . . H40C H 0.328444 0.629165 0.374231 0.050 Uiso 1 1 calc R U . . . O41 O 0.35524(3) 0.19675(11) 0.48410(6) 0.0314(3) Uani 1 1 d . . . . . C42 C 0.34816(5) 0.14393(16) 0.53512(9) 0.0319(5) Uani 1 1 d . . . . . C43 C 0.33421(5) 0.05218(16) 0.53475(9) 0.0378(5) Uani 1 1 d . . . . . C44 C 0.32807(6) 0.01285(17) 0.59132(10) 0.0429(6) Uani 1 1 d . . . . . H44 H 0.318248 -0.049649 0.593699 0.051 Uiso 1 1 calc R U . . . C45 C 0.33567(6) 0.06092(17) 0.64426(10) 0.0418(6) Uani 1 1 d . . . . . C46 C 0.35103(5) 0.15014(16) 0.64182(9) 0.0363(5) Uani 1 1 d . . . . . H46 H 0.356880 0.182695 0.677476 0.044 Uiso 1 1 calc R U . . . C47 C 0.35768(5) 0.19091(16) 0.58673(9) 0.0306(5) Uani 1 1 d . . . . . N48 N 0.37326(4) 0.27670(14) 0.57064(7) 0.0285(4) Uani 1 1 d . . . . . C49 C 0.39175(4) 0.33394(17) 0.60402(9) 0.0290(4) Uani 1 1 d . . . . . C50 C 0.39554(5) 0.33673(19) 0.66532(9) 0.0365(5) Uani 1 1 d . . . . . H50 H 0.384616 0.295787 0.690844 0.044 Uiso 1 1 calc R U . . . C51 C 0.41546(5) 0.4000(2) 0.68894(10) 0.0434(6) Uani 1 1 d . . . . . H51 H 0.418264 0.401478 0.730860 0.052 Uiso 1 1 calc R U . . . C52 C 0.43124(5) 0.4607(2) 0.65250(10) 0.0423(6) Uani 1 1 d . . . . . H52 H 0.444743 0.503756 0.669456 0.051 Uiso 1 1 calc R U . . . C53 C 0.42747(4) 0.4593(2) 0.59097(9) 0.0372(5) Uani 1 1 d . . . . . H53 H 0.438372 0.500865 0.565740 0.045 Uiso 1 1 calc R U . . . C54 C 0.40768(4) 0.39677(18) 0.56713(8) 0.0312(5) Uani 1 1 d . . . . . N55 N 0.40002(3) 0.38351(15) 0.50733(7) 0.0308(4) Uani 1 1 d . . . . . C56 C 0.41486(4) 0.40569(19) 0.45514(8) 0.0331(5) Uani 1 1 d . . . . . C57 C 0.43658(4) 0.4707(2) 0.44572(9) 0.0405(6) Uani 1 1 d . . . . . H57 H 0.443298 0.512536 0.477079 0.049 Uiso 1 1 calc R U . . . C58 C 0.44854(5) 0.4736(2) 0.38885(10) 0.0469(7) Uani 1 1 d . U . . . C59 C 0.43849(5) 0.4082(2) 0.34477(10) 0.0455(6) Uani 1 1 d . . . . . H59 H 0.447218 0.408377 0.306985 0.055 Uiso 1 1 calc R U . . . C60 C 0.41630(5) 0.3422(2) 0.35280(9) 0.0365(5) Uani 1 1 d . . . . . C61 C 0.40433(4) 0.34738(18) 0.40875(9) 0.0321(5) Uani 1 1 d . . . . . O62 O 0.38198(3) 0.29128(12) 0.42515(6) 0.0309(3) Uani 1 1 d . . . . . C63 C 0.32707(6) -0.00348(16) 0.47621(10) 0.0413(6) Uani 1 1 d . . . . . C64 C 0.35289(6) -0.02390(19) 0.44071(11) 0.0511(7) Uani 1 1 d . . . . . H64A H 0.348190 -0.055709 0.402477 0.077 Uiso 1 1 calc R U . . . H64B H 0.364710 -0.070065 0.463369 0.077 Uiso 1 1 calc R U . . . H64C H 0.362362 0.040936 0.433466 0.077 Uiso 1 1 calc R U . . . C65 C 0.31338(7) -0.10702(18) 0.48838(11) 0.0553(8) Uani 1 1 d . . . . . H65A H 0.309274 -0.140890 0.450422 0.083 Uiso 1 1 calc R U . . . H65B H 0.296510 -0.095932 0.510624 0.083 Uiso 1 1 calc R U . . . H65C H 0.325603 -0.150352 0.511884 0.083 Uiso 1 1 calc R U . . . C66 C 0.30771(6) 0.06291(18) 0.43918(11) 0.0475(6) Uani 1 1 d . . . . . H66A H 0.316817 0.126950 0.428188 0.071 Uiso 1 1 calc R U . . . H66B H 0.291469 0.078404 0.462718 0.071 Uiso 1 1 calc R U . . . H66C H 0.302484 0.025818 0.402942 0.071 Uiso 1 1 calc R U . . . C67 C 0.32761(7) 0.01718(18) 0.70571(10) 0.0539(8) Uani 1 1 d . U . . . C68 C 0.30905(8) 0.0946(2) 0.73726(13) 0.0724(10) Uani 1 1 d . U . . . H68A H 0.318513 0.160325 0.741175 0.109 Uiso 1 1 calc R U . . . H68B H 0.304307 0.068768 0.776955 0.109 Uiso 1 1 calc R U . . . H68C H 0.292469 0.104228 0.713763 0.109 Uiso 1 1 calc R U . . . C69 C 0.31238(10) -0.0846(2) 0.70041(13) 0.0859(13) Uani 1 1 d . U . . . H69A H 0.295943 -0.074723 0.676501 0.129 Uiso 1 1 calc R U . . . H69B H 0.307376 -0.108917 0.740286 0.129 Uiso 1 1 calc R U . . . H69C H 0.324079 -0.135436 0.681042 0.129 Uiso 1 1 calc R U . . . C70 C 0.35327(8) -0.0017(2) 0.74249(12) 0.0721(10) Uani 1 1 d . U . . . H70A H 0.365212 -0.049113 0.721005 0.108 Uiso 1 1 calc R U . . . H70B H 0.348303 -0.031588 0.781094 0.108 Uiso 1 1 calc R U . . . H70C H 0.362745 0.063351 0.748942 0.108 Uiso 1 1 calc R U . . . C71 C 0.40591(5) 0.2684(2) 0.30489(9) 0.0413(6) Uani 1 1 d . . . . . C72 C 0.40758(7) 0.1579(2) 0.32878(11) 0.0571(8) Uani 1 1 d . . . . . H72A H 0.401016 0.110264 0.298228 0.086 Uiso 1 1 calc R U . . . H72B H 0.396331 0.151620 0.364644 0.086 Uiso 1 1 calc R U . . . H72C H 0.426460 0.141539 0.338675 0.086 Uiso 1 1 calc R U . . . C73 C 0.42313(7) 0.2743(3) 0.24789(11) 0.0656(9) Uani 1 1 d . . . . . H73A H 0.416451 0.224150 0.218864 0.098 Uiso 1 1 calc R U . . . H73B H 0.442109 0.259211 0.257563 0.098 Uiso 1 1 calc R U . . . H73C H 0.421830 0.343309 0.230886 0.098 Uiso 1 1 calc R U . . . C74 C 0.37661(5) 0.2941(2) 0.28832(11) 0.0461(6) Uani 1 1 d . . . . . H74A H 0.375647 0.364722 0.273643 0.069 Uiso 1 1 calc R U . . . H74B H 0.365024 0.286841 0.323599 0.069 Uiso 1 1 calc R U . . . H74C H 0.370366 0.247116 0.257086 0.069 Uiso 1 1 calc R U . . . C75 C 0.47228(5) 0.5476(3) 0.37775(11) 0.0622(9) Uani 1 1 d . U . . . C76A C 0.48308(12) 0.5429(6) 0.3138(2) 0.0712(17) Uani 0.679(7) 1 d . U P A 1 H76A H 0.468320 0.557767 0.285852 0.107 Uiso 0.679(7) 1 calc R U P A 1 H76B H 0.490289 0.474272 0.305880 0.107 Uiso 0.679(7) 1 calc R U P A 1 H76C H 0.497554 0.593684 0.308843 0.107 Uiso 0.679(7) 1 calc R U P A 1 C77A C 0.49499(9) 0.5305(5) 0.4205(2) 0.0743(18) Uani 0.679(7) 1 d . U P A 1 H77A H 0.500279 0.458135 0.419773 0.111 Uiso 0.679(7) 1 calc R U P A 1 H77B H 0.489089 0.549120 0.460831 0.111 Uiso 0.679(7) 1 calc R U P A 1 H77C H 0.510524 0.573031 0.409042 0.111 Uiso 0.679(7) 1 calc R U P A 1 C78A C 0.46202(11) 0.6626(4) 0.3880(3) 0.0749(17) Uani 0.679(7) 1 d . U P A 1 H78A H 0.477137 0.710185 0.381616 0.112 Uiso 0.679(7) 1 calc R U P A 1 H78B H 0.455224 0.669969 0.428813 0.112 Uiso 0.679(7) 1 calc R U P A 1 H78C H 0.447425 0.678141 0.359675 0.112 Uiso 0.679(7) 1 calc R U P A 1 C76B C 0.4989(3) 0.4675(13) 0.3807(8) 0.108(5) Uani 0.321(7) 1 d . U P A 2 H76D H 0.515719 0.506635 0.376669 0.162 Uiso 0.321(7) 1 calc R U P A 2 H76E H 0.497547 0.417580 0.348164 0.162 Uiso 0.321(7) 1 calc R U P A 2 H76F H 0.498823 0.431352 0.419049 0.162 Uiso 0.321(7) 1 calc R U P A 2 C77B C 0.4754(3) 0.6227(10) 0.4249(5) 0.077(4) Uani 0.321(7) 1 d . U P A 2 H77D H 0.489107 0.673239 0.413272 0.115 Uiso 0.321(7) 1 calc R U P A 2 H77E H 0.481133 0.588261 0.461664 0.115 Uiso 0.321(7) 1 calc R U P A 2 H77F H 0.458023 0.657380 0.431732 0.115 Uiso 0.321(7) 1 calc R U P A 2 C78B C 0.4702(3) 0.5958(11) 0.3187(5) 0.076(3) Uani 0.321(7) 1 d . U P A 2 H78D H 0.469015 0.542565 0.287979 0.114 Uiso 0.321(7) 1 calc R U P A 2 H78E H 0.486334 0.638098 0.311505 0.114 Uiso 0.321(7) 1 calc R U P A 2 H78F H 0.453967 0.638966 0.317176 0.114 Uiso 0.321(7) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.0246(2) 0.0253(2) 0.0110(2) -0.00134(17) 0.00125(18) -0.00086(18) P2 0.0323(3) 0.0355(3) 0.0113(2) -0.00042(19) 0.00045(19) 0.0065(2) O3 0.0278(7) 0.0295(7) 0.0135(6) -0.0002(5) -0.0002(5) -0.0055(6) C5 0.0355(11) 0.0282(10) 0.0175(9) -0.0022(7) -0.0001(8) -0.0059(8) C4 0.0301(10) 0.0240(9) 0.0173(9) -0.0001(7) 0.0026(8) -0.0029(8) C6 0.0358(11) 0.0317(10) 0.0221(10) -0.0018(8) -0.0015(8) -0.0111(9) C7 0.0382(12) 0.0251(9) 0.0214(9) -0.0027(7) 0.0043(8) -0.0074(8) C8 0.0400(12) 0.0248(9) 0.0169(9) -0.0005(7) 0.0030(8) -0.0062(8) C9 0.0292(10) 0.0227(9) 0.0151(8) -0.0035(7) 0.0013(7) -0.0017(7) N10 0.0276(8) 0.0240(8) 0.0125(7) -0.0007(6) 0.0026(6) -0.0013(6) C11 0.0233(9) 0.0254(9) 0.0133(8) -0.0007(7) -0.0002(7) 0.0036(7) C12 0.0286(10) 0.0288(9) 0.0162(9) 0.0020(7) 0.0004(7) -0.0010(8) C13 0.0303(10) 0.0375(11) 0.0140(9) 0.0008(8) 0.0032(8) 0.0002(8) C14 0.0297(10) 0.0396(11) 0.0150(9) -0.0045(8) 0.0002(8) 0.0013(9) C15 0.0253(10) 0.0322(10) 0.0167(9) -0.0027(7) 0.0002(7) -0.0025(8) C16 0.0222(9) 0.0276(9) 0.0129(8) 0.0002(7) 0.0004(7) 0.0028(7) N17 0.0242(8) 0.0298(8) 0.0118(7) -0.0025(6) 0.0019(6) -0.0021(7) C18 0.0227(9) 0.0333(10) 0.0143(9) 0.0003(7) 0.0024(7) -0.0026(8) C19 0.0314(11) 0.0436(12) 0.0139(9) -0.0015(8) -0.0002(8) -0.0096(9) C20 0.0340(11) 0.0472(12) 0.0190(10) -0.0008(9) 0.0002(8) -0.0172(10) C21 0.0361(11) 0.0424(12) 0.0178(9) 0.0011(8) 0.0020(8) -0.0155(9) C22 0.0291(10) 0.0347(10) 0.0133(8) -0.0013(7) 0.0009(7) -0.0056(8) C23 0.0234(9) 0.0317(10) 0.0140(8) -0.0030(7) -0.0006(7) -0.0042(8) O24 0.0283(7) 0.0269(7) 0.0122(6) -0.0010(5) -0.0003(5) -0.0063(5) C25 0.0395(12) 0.0358(11) 0.0192(10) 0.0017(8) -0.0044(8) -0.0122(9) C26 0.0513(15) 0.0639(16) 0.0276(12) 0.0082(11) -0.0128(11) -0.0246(13) C27 0.0525(15) 0.0495(13) 0.0168(10) -0.0033(9) 0.0005(9) -0.0072(11) C28 0.0508(14) 0.0391(12) 0.0276(11) 0.0068(9) -0.0070(10) -0.0068(10) C29 0.0430(13) 0.0333(11) 0.0269(11) -0.0003(9) 0.0032(9) -0.0157(9) C30 0.0463(14) 0.0411(12) 0.0322(12) -0.0012(10) 0.0054(10) -0.0204(11) C31 0.0570(16) 0.0587(16) 0.0326(13) -0.0095(11) 0.0160(12) -0.0294(13) C32 0.0584(16) 0.0410(13) 0.0538(16) 0.0171(12) 0.0020(13) -0.0183(12) C33 0.0583(16) 0.0623(16) 0.0210(11) -0.0024(10) -0.0003(11) -0.0363(13) C34 0.077(2) 0.0525(15) 0.0293(13) -0.0093(11) -0.0051(12) -0.0328(14) C35 0.0467(15) 0.102(2) 0.0290(13) -0.0068(14) -0.0062(11) -0.0373(16) C36 0.094(2) 0.093(2) 0.0321(14) 0.0012(14) -0.0052(15) -0.070(2) C37 0.0369(11) 0.0348(10) 0.0137(9) 0.0019(8) 0.0005(8) -0.0062(9) C38 0.0571(15) 0.0454(13) 0.0163(10) 0.0025(9) 0.0029(10) -0.0162(11) C39 0.0420(12) 0.0386(11) 0.0148(9) -0.0014(8) 0.0018(8) -0.0032(9) C40 0.0424(13) 0.0368(11) 0.0212(10) 0.0000(8) -0.0057(9) -0.0018(10) O41 0.0498(9) 0.0300(7) 0.0144(6) -0.0002(5) 0.0003(6) 0.0050(6) C42 0.0509(13) 0.0295(10) 0.0154(9) 0.0028(8) 0.0033(9) 0.0105(9) C43 0.0675(16) 0.0258(10) 0.0202(10) -0.0018(8) 0.0027(10) 0.0073(10) C44 0.0790(18) 0.0270(10) 0.0226(11) 0.0006(8) 0.0046(11) 0.0009(11) C45 0.0764(18) 0.0300(11) 0.0190(10) 0.0029(8) 0.0036(11) 0.0063(11) C46 0.0602(15) 0.0318(11) 0.0168(10) -0.0008(8) 0.0002(10) 0.0085(10) C47 0.0422(12) 0.0315(10) 0.0182(9) 0.0010(8) 0.0000(9) 0.0105(9) N48 0.0344(9) 0.0385(9) 0.0126(7) 0.0003(7) 0.0000(7) 0.0074(8) C49 0.0263(10) 0.0439(12) 0.0169(9) -0.0003(8) -0.0013(8) 0.0085(9) C50 0.0368(12) 0.0577(14) 0.0150(9) 0.0025(9) -0.0007(8) 0.0067(11) C51 0.0398(13) 0.0765(18) 0.0139(10) -0.0031(10) -0.0047(9) 0.0056(12) C52 0.0316(12) 0.0748(17) 0.0205(10) -0.0060(11) -0.0041(9) 0.0008(11) C53 0.0270(11) 0.0658(15) 0.0188(10) -0.0015(10) 0.0011(8) -0.0001(10) C54 0.0271(10) 0.0542(13) 0.0123(9) -0.0019(8) 0.0007(8) 0.0083(9) N55 0.0278(9) 0.0530(11) 0.0115(8) -0.0010(7) 0.0000(6) 0.0039(8) C56 0.0287(11) 0.0587(14) 0.0120(9) 0.0005(9) 0.0012(8) 0.0078(10) C57 0.0260(11) 0.0781(18) 0.0175(10) -0.0021(10) 0.0016(8) -0.0007(11) C58 0.0254(11) 0.094(2) 0.0209(11) 0.0000(12) 0.0024(9) -0.0005(12) C59 0.0307(12) 0.088(2) 0.0177(10) 0.0002(11) 0.0060(9) 0.0078(12) C60 0.0317(12) 0.0625(15) 0.0154(9) -0.0017(9) 0.0007(8) 0.0147(10) C61 0.0274(11) 0.0517(13) 0.0172(9) -0.0002(9) 0.0007(8) 0.0086(9) O62 0.0348(8) 0.0451(8) 0.0127(6) -0.0023(6) 0.0029(6) 0.0055(7) C63 0.0785(18) 0.0246(10) 0.0208(10) -0.0029(8) 0.0028(11) 0.0026(11) C64 0.090(2) 0.0351(13) 0.0286(12) -0.0082(10) 0.0060(13) 0.0099(13) C65 0.104(2) 0.0316(12) 0.0303(13) -0.0054(10) 0.0024(14) -0.0045(13) C66 0.080(2) 0.0358(12) 0.0265(12) -0.0056(9) -0.0073(12) -0.0003(12) C67 0.108(2) 0.0321(12) 0.0212(11) 0.0018(9) 0.0075(13) -0.0061(13) C68 0.125(3) 0.0555(17) 0.0370(15) 0.0007(13) 0.0328(17) -0.0092(18) C69 0.175(4) 0.0522(17) 0.0301(14) 0.0074(12) 0.0141(19) -0.035(2) C70 0.137(3) 0.0532(16) 0.0265(13) 0.0106(12) -0.0060(16) 0.0005(19) C71 0.0440(13) 0.0654(16) 0.0144(10) -0.0060(10) 0.0017(9) 0.0135(12) C72 0.078(2) 0.0632(17) 0.0301(13) -0.0079(12) -0.0054(13) 0.0303(15) C73 0.073(2) 0.101(2) 0.0232(12) -0.0158(14) 0.0131(13) 0.0029(18) C74 0.0505(15) 0.0601(16) 0.0276(12) -0.0108(11) -0.0103(11) 0.0138(12) C75 0.0319(13) 0.129(3) 0.0260(12) 0.0034(15) 0.0054(10) -0.0176(15) C76A 0.059(3) 0.120(5) 0.035(2) 0.003(3) 0.016(2) -0.016(3) C77A 0.039(2) 0.132(5) 0.052(3) 0.013(3) -0.005(2) -0.017(3) C78A 0.051(3) 0.099(4) 0.075(4) 0.004(3) 0.014(2) -0.022(2) C76B 0.058(6) 0.133(8) 0.133(9) -0.014(7) 0.006(6) -0.003(5) C77B 0.072(6) 0.093(6) 0.066(5) 0.003(5) 0.016(5) -0.026(5) C78B 0.079(7) 0.094(7) 0.056(5) 0.003(5) 0.002(5) -0.039(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 O3 1.6603(13) . ? P1 O24 1.6623(13) . ? P1 N10 1.7384(16) . ? P1 N17 1.7391(16) . ? P1 P2 2.2282(7) . ? P2 O62 1.6545(14) . ? P2 O41 1.6615(16) . ? P2 N48 1.7348(16) . ? P2 N55 1.7359(19) . ? O3 C4 1.379(2) . ? C5 C4 1.385(3) . ? C5 C6 1.403(3) . ? C5 C25 1.535(3) . ? C4 C9 1.393(3) . ? C6 C7 1.396(3) . ? C6 H6 0.9500 . ? C7 C8 1.396(3) . ? C7 C29 1.534(3) . ? C8 C9 1.384(3) . ? C8 H8 0.9500 . ? C9 N10 1.403(2) . ? N10 C11 1.399(2) . ? C11 C12 1.388(3) . ? C11 C16 1.406(3) . ? C12 C13 1.394(3) . ? C12 H12 0.9500 . ? C13 C14 1.379(3) . ? C13 H13 0.9500 . ? C14 C15 1.393(3) . ? C14 H14 0.9500 . ? C15 C16 1.390(3) . ? C15 H15 0.9500 . ? C16 N17 1.402(2) . ? N17 C18 1.409(2) . ? C18 C19 1.381(3) . ? C18 C23 1.394(3) . ? C19 C20 1.399(3) . ? C19 H19 0.9500 . ? C20 C21 1.394(3) . ? C20 C33 1.539(3) . ? C21 C22 1.396(3) . ? C21 H21 0.9500 . ? C22 C23 1.389(3) . ? C22 C37 1.531(3) . ? C23 O24 1.377(2) . ? C25 C26 1.528(3) . ? C25 C28 1.537(3) . ? C25 C27 1.538(3) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 C30 1.527(3) . ? C29 C32 1.528(3) . ? C29 C31 1.539(3) . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C33 C35 1.523(4) . ? C33 C36 1.538(3) . ? C33 C34 1.538(4) . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 C38 1.531(3) . ? C37 C39 1.533(3) . ? C37 C40 1.538(3) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? O41 C42 1.380(2) . ? C42 C43 1.381(3) . ? C42 C47 1.391(3) . ? C43 C44 1.401(3) . ? C43 C63 1.541(3) . ? C44 C45 1.394(3) . ? C44 H44 0.9500 . ? C45 C46 1.390(3) . ? C45 C67 1.543(3) . ? C46 C47 1.384(3) . ? C46 H46 0.9500 . ? C47 N48 1.405(3) . ? N48 C49 1.396(3) . ? C49 C50 1.387(3) . ? C49 C54 1.405(3) . ? C50 C51 1.388(3) . ? C50 H50 0.9500 . ? C51 C52 1.379(4) . ? C51 H51 0.9500 . ? C52 C53 1.392(3) . ? C52 H52 0.9500 . ? C53 C54 1.380(3) . ? C53 H53 0.9500 . ? C54 N55 1.403(2) . ? N55 C56 1.410(3) . ? C56 C57 1.382(3) . ? C56 C61 1.389(3) . ? C57 C58 1.405(3) . ? C57 H57 0.9500 . ? C58 C59 1.396(4) . ? C58 C75 1.537(4) . ? C59 C60 1.404(4) . ? C59 H59 0.9500 . ? C60 C61 1.388(3) . ? C60 C71 1.530(3) . ? C61 O62 1.373(3) . ? C63 C64 1.524(4) . ? C63 C66 1.533(3) . ? C63 C65 1.535(3) . ? C64 H64A 0.9800 . ? C64 H64B 0.9800 . ? C64 H64C 0.9800 . ? C65 H65A 0.9800 . ? C65 H65B 0.9800 . ? C65 H65C 0.9800 . ? C66 H66A 0.9800 . ? C66 H66B 0.9800 . ? C66 H66C 0.9800 . ? C67 C70 1.530(5) . ? C67 C69 1.531(4) . ? C67 C68 1.536(4) . ? C68 H68A 0.9800 . ? C68 H68B 0.9800 . ? C68 H68C 0.9800 . ? C69 H69A 0.9800 . ? C69 H69B 0.9800 . ? C69 H69C 0.9800 . ? C70 H70A 0.9800 . ? C70 H70B 0.9800 . ? C70 H70C 0.9800 . ? C71 C74 1.528(3) . ? C71 C73 1.536(3) . ? C71 C72 1.541(4) . ? C72 H72A 0.9800 . ? C72 H72B 0.9800 . ? C72 H72C 0.9800 . ? C73 H73A 0.9800 . ? C73 H73B 0.9800 . ? C73 H73C 0.9800 . ? C74 H74A 0.9800 . ? C74 H74B 0.9800 . ? C74 H74C 0.9800 . ? C75 C77B 1.450(12) . ? C75 C78B 1.469(12) . ? C75 C77A 1.490(5) . ? C75 C76A 1.530(5) . ? C75 C78A 1.600(7) . ? C75 C76B 1.677(14) . ? C76A H76A 0.9800 . ? C76A H76B 0.9800 . ? C76A H76C 0.9800 . ? C77A H77A 0.9800 . ? C77A H77B 0.9800 . ? C77A H77C 0.9800 . ? C78A H78A 0.9800 . ? C78A H78B 0.9800 . ? C78A H78C 0.9800 . ? C76B H76D 0.9800 . ? C76B H76E 0.9800 . ? C76B H76F 0.9800 . ? C77B H77D 0.9800 . ? C77B H77E 0.9800 . ? C77B H77F 0.9800 . ? C78B H78D 0.9800 . ? C78B H78E 0.9800 . ? C78B H78F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 P1 O24 84.64(6) . . ? O3 P1 N10 89.11(7) . . ? O24 P1 N10 157.48(8) . . ? O3 P1 N17 153.19(8) . . ? O24 P1 N17 88.87(7) . . ? N10 P1 N17 87.02(7) . . ? O3 P1 P2 108.00(5) . . ? O24 P1 P2 103.14(5) . . ? N10 P1 P2 99.36(6) . . ? N17 P1 P2 98.80(6) . . ? O62 P2 O41 84.86(7) . . ? O62 P2 N48 152.94(8) . . ? O41 P2 N48 88.70(8) . . ? O62 P2 N55 88.82(8) . . ? O41 P2 N55 156.92(9) . . ? N48 P2 N55 86.90(8) . . ? O62 P2 P1 107.62(6) . . ? O41 P2 P1 102.32(6) . . ? N48 P2 P1 99.43(6) . . ? N55 P2 P1 100.75(7) . . ? C4 O3 P1 115.33(11) . . ? C4 C5 C6 115.16(18) . . ? C4 C5 C25 122.18(17) . . ? C6 C5 C25 122.66(18) . . ? O3 C4 C5 124.70(17) . . ? O3 C4 C9 112.46(16) . . ? C5 C4 C9 122.80(18) . . ? C7 C6 C5 123.68(19) . . ? C7 C6 H6 118.2 . . ? C5 C6 H6 118.2 . . ? C8 C7 C6 118.67(18) . . ? C8 C7 C29 118.38(18) . . ? C6 C7 C29 122.94(18) . . ? C9 C8 C7 119.15(18) . . ? C9 C8 H8 120.4 . . ? C7 C8 H8 120.4 . . ? C8 C9 C4 120.25(18) . . ? C8 C9 N10 130.51(17) . . ? C4 C9 N10 109.24(16) . . ? C11 N10 C9 127.50(16) . . ? C11 N10 P1 115.82(12) . . ? C9 N10 P1 113.28(12) . . ? C12 C11 N10 128.76(17) . . ? C12 C11 C16 120.37(17) . . ? N10 C11 C16 110.80(15) . . ? C11 C12 C13 118.68(18) . . ? C11 C12 H12 120.7 . . ? C13 C12 H12 120.7 . . ? C14 C13 C12 121.01(18) . . ? C14 C13 H13 119.5 . . ? C12 C13 H13 119.5 . . ? C13 C14 C15 120.79(18) . . ? C13 C14 H14 119.6 . . ? C15 C14 H14 119.6 . . ? C16 C15 C14 118.78(18) . . ? C16 C15 H15 120.6 . . ? C14 C15 H15 120.6 . . ? C15 C16 N17 129.06(17) . . ? C15 C16 C11 120.35(17) . . ? N17 C16 C11 110.51(16) . . ? C16 N17 C18 128.85(16) . . ? C16 N17 P1 115.82(12) . . ? C18 N17 P1 113.57(12) . . ? C19 C18 C23 120.05(18) . . ? C19 C18 N17 131.39(17) . . ? C23 C18 N17 108.51(16) . . ? C18 C19 C20 119.08(18) . . ? C18 C19 H19 120.5 . . ? C20 C19 H19 120.5 . . ? C21 C20 C19 118.85(19) . . ? C21 C20 C33 122.47(19) . . ? C19 C20 C33 118.68(18) . . ? C20 C21 C22 123.75(19) . . ? C20 C21 H21 118.1 . . ? C22 C21 H21 118.1 . . ? C23 C22 C21 114.98(17) . . ? C23 C22 C37 121.31(17) . . ? C21 C22 C37 123.68(18) . . ? O24 C23 C22 123.94(16) . . ? O24 C23 C18 113.03(16) . . ? C22 C23 C18 122.99(17) . . ? C23 O24 P1 115.10(11) . . ? C26 C25 C5 111.85(17) . . ? C26 C25 C28 108.4(2) . . ? C5 C25 C28 109.03(17) . . ? C26 C25 C27 107.91(19) . . ? C5 C25 C27 110.22(18) . . ? C28 C25 C27 109.41(19) . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C25 C27 H27A 109.5 . . ? C25 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C25 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C25 C28 H28A 109.5 . . ? C25 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C25 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C30 C29 C32 108.32(19) . . ? C30 C29 C7 112.05(18) . . ? C32 C29 C7 109.4(2) . . ? C30 C29 C31 107.8(2) . . ? C32 C29 C31 109.6(2) . . ? C7 C29 C31 109.60(17) . . ? C29 C30 H30A 109.5 . . ? C29 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C29 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C29 C31 H31A 109.5 . . ? C29 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? C29 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C29 C32 H32A 109.5 . . ? C29 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C29 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C35 C33 C36 107.3(2) . . ? C35 C33 C34 110.4(2) . . ? C36 C33 C34 108.3(2) . . ? C35 C33 C20 109.6(2) . . ? C36 C33 C20 112.03(19) . . ? C34 C33 C20 109.1(2) . . ? C33 C34 H34A 109.5 . . ? C33 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? C33 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C33 C35 H35A 109.5 . . ? C33 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? C33 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C33 C36 H36A 109.5 . . ? C33 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C33 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C22 C37 C38 111.33(17) . . ? C22 C37 C39 110.63(17) . . ? C38 C37 C39 108.03(17) . . ? C22 C37 C40 108.88(16) . . ? C38 C37 C40 108.10(18) . . ? C39 C37 C40 109.84(17) . . ? C37 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C37 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C37 C39 H39A 109.5 . . ? C37 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C37 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C37 C40 H40A 109.5 . . ? C37 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C37 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C42 O41 P2 115.42(13) . . ? O41 C42 C43 123.65(19) . . ? O41 C42 C47 112.57(19) . . ? C43 C42 C47 123.72(19) . . ? C42 C43 C44 114.8(2) . . ? C42 C43 C63 121.85(19) . . ? C44 C43 C63 123.3(2) . . ? C45 C44 C43 123.2(2) . . ? C45 C44 H44 118.4 . . ? C43 C44 H44 118.4 . . ? C46 C45 C44 119.3(2) . . ? C46 C45 C67 119.0(2) . . ? C44 C45 C67 121.6(2) . . ? C47 C46 C45 119.1(2) . . ? C47 C46 H46 120.5 . . ? C45 C46 H46 120.5 . . ? C46 C47 C42 119.5(2) . . ? C46 C47 N48 131.7(2) . . ? C42 C47 N48 108.80(17) . . ? C49 N48 C47 130.24(17) . . ? C49 N48 P2 115.45(14) . . ? C47 N48 P2 113.84(14) . . ? C50 C49 N48 129.3(2) . . ? C50 C49 C54 119.5(2) . . ? N48 C49 C54 111.22(17) . . ? C49 C50 C51 119.3(2) . . ? C49 C50 H50 120.4 . . ? C51 C50 H50 120.4 . . ? C52 C51 C50 121.0(2) . . ? C52 C51 H51 119.5 . . ? C50 C51 H51 119.5 . . ? C51 C52 C53 120.3(2) . . ? C51 C52 H52 119.9 . . ? C53 C52 H52 119.9 . . ? C54 C53 C52 119.1(2) . . ? C54 C53 H53 120.5 . . ? C52 C53 H53 120.5 . . ? C53 C54 N55 129.3(2) . . ? C53 C54 C49 120.84(18) . . ? N55 C54 C49 109.87(19) . . ? C54 N55 C56 128.89(18) . . ? C54 N55 P2 115.87(14) . . ? C56 N55 P2 113.71(14) . . ? C57 C56 C61 120.72(19) . . ? C57 C56 N55 130.9(2) . . ? C61 C56 N55 108.4(2) . . ? C56 C57 C58 118.7(2) . . ? C56 C57 H57 120.6 . . ? C58 C57 H57 120.6 . . ? C59 C58 C57 118.5(2) . . ? C59 C58 C75 122.7(2) . . ? C57 C58 C75 118.9(2) . . ? C58 C59 C60 124.1(2) . . ? C58 C59 H59 117.9 . . ? C60 C59 H59 117.9 . . ? C61 C60 C59 114.6(2) . . ? C61 C60 C71 121.5(2) . . ? C59 C60 C71 123.82(19) . . ? O62 C61 C60 123.8(2) . . ? O62 C61 C56 113.04(17) . . ? C60 C61 C56 123.0(2) . . ? C61 O62 P2 115.58(13) . . ? C64 C63 C66 109.6(2) . . ? C64 C63 C65 107.8(2) . . ? C66 C63 C65 108.7(2) . . ? C64 C63 C43 109.6(2) . . ? C66 C63 C43 109.70(18) . . ? C65 C63 C43 111.35(19) . . ? C63 C64 H64A 109.5 . . ? C63 C64 H64B 109.5 . . ? H64A C64 H64B 109.5 . . ? C63 C64 H64C 109.5 . . ? H64A C64 H64C 109.5 . . ? H64B C64 H64C 109.5 . . ? C63 C65 H65A 109.5 . . ? C63 C65 H65B 109.5 . . ? H65A C65 H65B 109.5 . . ? C63 C65 H65C 109.5 . . ? H65A C65 H65C 109.5 . . ? H65B C65 H65C 109.5 . . ? C63 C66 H66A 109.5 . . ? C63 C66 H66B 109.5 . . ? H66A C66 H66B 109.5 . . ? C63 C66 H66C 109.5 . . ? H66A C66 H66C 109.5 . . ? H66B C66 H66C 109.5 . . ? C70 C67 C69 107.9(3) . . ? C70 C67 C68 110.5(2) . . ? C69 C67 C68 108.4(3) . . ? C70 C67 C45 109.1(3) . . ? C69 C67 C45 112.2(2) . . ? C68 C67 C45 108.7(2) . . ? C67 C68 H68A 109.5 . . ? C67 C68 H68B 109.5 . . ? H68A C68 H68B 109.5 . . ? C67 C68 H68C 109.5 . . ? H68A C68 H68C 109.5 . . ? H68B C68 H68C 109.5 . . ? C67 C69 H69A 109.5 . . ? C67 C69 H69B 109.5 . . ? H69A C69 H69B 109.5 . . ? C67 C69 H69C 109.5 . . ? H69A C69 H69C 109.5 . . ? H69B C69 H69C 109.5 . . ? C67 C70 H70A 109.5 . . ? C67 C70 H70B 109.5 . . ? H70A C70 H70B 109.5 . . ? C67 C70 H70C 109.5 . . ? H70A C70 H70C 109.5 . . ? H70B C70 H70C 109.5 . . ? C74 C71 C60 110.42(19) . . ? C74 C71 C73 108.0(2) . . ? C60 C71 C73 111.6(2) . . ? C74 C71 C72 109.9(2) . . ? C60 C71 C72 109.08(19) . . ? C73 C71 C72 107.8(2) . . ? C71 C72 H72A 109.5 . . ? C71 C72 H72B 109.5 . . ? H72A C72 H72B 109.5 . . ? C71 C72 H72C 109.5 . . ? H72A C72 H72C 109.5 . . ? H72B C72 H72C 109.5 . . ? C71 C73 H73A 109.5 . . ? C71 C73 H73B 109.5 . . ? H73A C73 H73B 109.5 . . ? C71 C73 H73C 109.5 . . ? H73A C73 H73C 109.5 . . ? H73B C73 H73C 109.5 . . ? C71 C74 H74A 109.5 . . ? C71 C74 H74B 109.5 . . ? H74A C74 H74B 109.5 . . ? C71 C74 H74C 109.5 . . ? H74A C74 H74C 109.5 . . ? H74B C74 H74C 109.5 . . ? C77B C75 C78B 112.0(8) . . ? C77A C75 C76A 109.6(3) . . ? C77B C75 C58 112.8(5) . . ? C78B C75 C58 111.3(5) . . ? C77A C75 C58 111.9(3) . . ? C76A C75 C58 113.0(3) . . ? C77A C75 C78A 106.6(4) . . ? C76A C75 C78A 106.3(4) . . ? C58 C75 C78A 109.0(3) . . ? C77B C75 C76B 108.1(8) . . ? C78B C75 C76B 110.9(9) . . ? C58 C75 C76B 101.3(6) . . ? C75 C76A H76A 109.5 . . ? C75 C76A H76B 109.5 . . ? H76A C76A H76B 109.5 . . ? C75 C76A H76C 109.5 . . ? H76A C76A H76C 109.5 . . ? H76B C76A H76C 109.5 . . ? C75 C77A H77A 109.5 . . ? C75 C77A H77B 109.5 . . ? H77A C77A H77B 109.5 . . ? C75 C77A H77C 109.5 . . ? H77A C77A H77C 109.5 . . ? H77B C77A H77C 109.5 . . ? C75 C78A H78A 109.5 . . ? C75 C78A H78B 109.5 . . ? H78A C78A H78B 109.5 . . ? C75 C78A H78C 109.5 . . ? H78A C78A H78C 109.5 . . ? H78B C78A H78C 109.5 . . ? C75 C76B H76D 109.5 . . ? C75 C76B H76E 109.5 . . ? H76D C76B H76E 109.5 . . ? C75 C76B H76F 109.5 . . ? H76D C76B H76F 109.5 . . ? H76E C76B H76F 109.5 . . ? C75 C77B H77D 109.5 . . ? C75 C77B H77E 109.5 . . ? H77D C77B H77E 109.5 . . ? C75 C77B H77F 109.5 . . ? H77D C77B H77F 109.5 . . ? H77E C77B H77F 109.5 . . ? C75 C78B H78D 109.5 . . ? C75 C78B H78E 109.5 . . ? H78D C78B H78E 109.5 . . ? C75 C78B H78F 109.5 . . ? H78D C78B H78F 109.5 . . ? H78E C78B H78F 109.5 . . ? _refine_diff_density_max 0.483 _refine_diff_density_min -0.466 _refine_diff_density_rms 0.054 _shelx_res_file ; TITL rom205_0m_a.res in Pbcn rom205_sq.res created by SHELXL-2016/6 at 09:41:18 on 12-Aug-2021 REM Old TITL rom205_0m in Pbcm REM SHELXT solution in Pbcn REM R1 0.262, Rweak 0.011, Alpha 0.060, Orientation a'=c, b'=a, c'=b REM Formula found by SHELXT: C68 N4 O4 P2 CELL 0.71073 49.2848 13.0502 22.4161 90.000 90.000 90.000 ZERR 8.000 0.0024 0.0006 0.0011 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, 1/2-Y, 1/2+Z SYMM -X, Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N O P UNIT 544 704 32 32 16 LIST 4 TEMP -163.000 SIZE 0.05 0.158 0.258 DELU C58 C75 DELU C75 > LAST ISOR 0.01 0.01 C75 > LAST ISOR 0.01 0.01 C67 > C70 ACTA OMIT 4 0 0 OMIT 2 0 0 OMIT 9 3 6 OMIT 2 4 1 OMIT 1 10 10 OMIT 22 10 3 OMIT 8 6 4 OMIT 8 0 0 OMIT 18 6 0 OMIT 3 1 0 OMIT 6 0 0 OMIT 22 0 0 L.S. 10 0 138 BOND $H FMAP 2 PLAN 20 ABIN WGHT 0.064400 11.307800 FVAR 0.10052 0.67891 P1 5 0.338758 0.421126 0.496026 11.00000 0.02458 0.02534 = 0.01095 -0.00134 0.00125 -0.00086 P2 5 0.372030 0.305528 0.495145 11.00000 0.03229 0.03554 = 0.01128 -0.00042 0.00045 0.00645 O3 4 0.316021 0.387016 0.445108 11.00000 0.02778 0.02950 = 0.01347 -0.00020 -0.00020 -0.00555 C5 1 0.272797 0.297364 0.431817 11.00000 0.03552 0.02823 = 0.01748 -0.00220 -0.00012 -0.00591 C4 1 0.294367 0.330878 0.466308 11.00000 0.03013 0.02404 = 0.01734 -0.00010 0.00263 -0.00294 C6 1 0.253288 0.239190 0.462291 11.00000 0.03576 0.03166 = 0.02206 -0.00181 -0.00150 -0.01111 AFIX 43 H6 2 0.238015 0.215158 0.440546 11.00000 -1.20000 AFIX 0 C7 1 0.255052 0.214630 0.522758 11.00000 0.03817 0.02509 = 0.02143 -0.00266 0.00432 -0.00737 C8 1 0.276769 0.253285 0.555763 11.00000 0.04002 0.02483 = 0.01688 -0.00052 0.00297 -0.00618 AFIX 43 H8 2 0.278424 0.238008 0.597039 11.00000 -1.20000 AFIX 0 C9 1 0.295866 0.314168 0.527592 11.00000 0.02917 0.02274 = 0.01506 -0.00354 0.00129 -0.00169 N10 3 0.318207 0.367547 0.550793 11.00000 0.02758 0.02399 = 0.01246 -0.00068 0.00262 -0.00126 C11 1 0.321007 0.408845 0.608058 11.00000 0.02331 0.02539 = 0.01328 -0.00070 -0.00019 0.00365 C12 1 0.306959 0.383896 0.659724 11.00000 0.02865 0.02882 = 0.01615 0.00203 0.00043 -0.00100 AFIX 43 H12 2 0.294334 0.328890 0.660030 11.00000 -1.20000 AFIX 0 C13 1 0.311745 0.441159 0.711154 11.00000 0.03028 0.03751 = 0.01395 0.00078 0.00319 0.00018 AFIX 43 H13 2 0.302167 0.425154 0.746732 11.00000 -1.20000 AFIX 0 C14 1 0.330168 0.520673 0.711179 11.00000 0.02969 0.03964 = 0.01499 -0.00451 0.00016 0.00129 AFIX 43 H14 2 0.333066 0.558852 0.746696 11.00000 -1.20000 AFIX 0 C15 1 0.344580 0.545685 0.659754 11.00000 0.02532 0.03219 = 0.01674 -0.00272 0.00017 -0.00251 AFIX 43 H15 2 0.357228 0.600615 0.659872 11.00000 -1.20000 AFIX 0 C16 1 0.340116 0.488817 0.608268 11.00000 0.02216 0.02757 = 0.01290 0.00024 0.00042 0.00283 N17 3 0.351349 0.501690 0.551282 11.00000 0.02416 0.02981 = 0.01181 -0.00245 0.00193 -0.00210 C18 1 0.366581 0.584511 0.528859 11.00000 0.02270 0.03330 = 0.01426 0.00025 0.00241 -0.00261 C19 1 0.382851 0.655653 0.557167 11.00000 0.03137 0.04364 = 0.01393 -0.00147 -0.00022 -0.00956 AFIX 43 H19 2 0.385098 0.653824 0.599245 11.00000 -1.20000 AFIX 0 C20 1 0.395972 0.730422 0.523023 11.00000 0.03402 0.04725 = 0.01899 -0.00082 0.00022 -0.01717 C21 1 0.391628 0.732389 0.461579 11.00000 0.03612 0.04236 = 0.01779 0.00111 0.00200 -0.01553 AFIX 43 H21 2 0.400262 0.784621 0.438973 11.00000 -1.20000 AFIX 0 C22 1 0.375312 0.661978 0.431365 11.00000 0.02914 0.03474 = 0.01331 -0.00128 0.00091 -0.00565 C23 1 0.364089 0.585775 0.466898 11.00000 0.02336 0.03172 = 0.01400 -0.00303 -0.00061 -0.00423 O24 4 0.348716 0.505923 0.445204 11.00000 0.02829 0.02685 = 0.01224 -0.00104 -0.00028 -0.00632 C25 1 0.270315 0.323707 0.365311 11.00000 0.03950 0.03575 = 0.01921 0.00166 -0.00441 -0.01219 C26 1 0.245056 0.275779 0.337321 11.00000 0.05126 0.06388 = 0.02761 0.00816 -0.01281 -0.02462 AFIX 137 H26A 2 0.244184 0.294152 0.294975 11.00000 -1.50000 H26B 2 0.228834 0.301372 0.357745 11.00000 -1.50000 H26C 2 0.245951 0.201070 0.341291 11.00000 -1.50000 AFIX 0 C27 1 0.295225 0.283982 0.331077 11.00000 0.05252 0.04950 = 0.01682 -0.00329 0.00050 -0.00718 AFIX 137 H27A 2 0.293308 0.300491 0.288637 11.00000 -1.50000 H27B 2 0.296596 0.209540 0.335975 11.00000 -1.50000 H27C 2 0.311645 0.316599 0.346804 11.00000 -1.50000 AFIX 0 C28 1 0.268429 0.440623 0.358336 11.00000 0.05084 0.03908 = 0.02758 0.00676 -0.00705 -0.00677 AFIX 137 H28A 2 0.265941 0.457831 0.316134 11.00000 -1.50000 H28B 2 0.285177 0.472272 0.373032 11.00000 -1.50000 H28C 2 0.252967 0.466333 0.381393 11.00000 -1.50000 AFIX 0 C29 1 0.234542 0.144889 0.554352 11.00000 0.04295 0.03329 = 0.02692 -0.00028 0.00324 -0.01575 C30 1 0.210920 0.115578 0.513690 11.00000 0.04632 0.04106 = 0.03223 -0.00120 0.00541 -0.02041 AFIX 137 H30A 2 0.202095 0.177850 0.498841 11.00000 -1.50000 H30B 2 0.197766 0.074648 0.536210 11.00000 -1.50000 H30C 2 0.217742 0.075427 0.479926 11.00000 -1.50000 AFIX 0 C31 1 0.222756 0.200710 0.608979 11.00000 0.05697 0.05871 = 0.03258 -0.00946 0.01602 -0.02939 AFIX 137 H31A 2 0.213991 0.264380 0.596097 11.00000 -1.50000 H31B 2 0.237407 0.216699 0.637033 11.00000 -1.50000 H31C 2 0.209363 0.156603 0.628599 11.00000 -1.50000 AFIX 0 C32 1 0.248733 0.046671 0.574390 11.00000 0.05840 0.04104 = 0.05383 0.01709 0.00199 -0.01834 AFIX 137 H32A 2 0.254525 0.007640 0.539279 11.00000 -1.50000 H32B 2 0.236153 0.005202 0.598128 11.00000 -1.50000 H32C 2 0.264623 0.064166 0.598617 11.00000 -1.50000 AFIX 0 C33 1 0.414657 0.807579 0.554789 11.00000 0.05834 0.06227 = 0.02098 -0.00237 -0.00029 -0.03631 C34 1 0.397834 0.870331 0.599581 11.00000 0.07741 0.05247 = 0.02934 -0.00931 -0.00510 -0.03280 AFIX 137 H34A 2 0.383540 0.907559 0.578278 11.00000 -1.50000 H34B 2 0.409662 0.919303 0.620128 11.00000 -1.50000 H34C 2 0.389583 0.824109 0.628874 11.00000 -1.50000 AFIX 0 C35 1 0.437314 0.750298 0.586811 11.00000 0.04672 0.10209 = 0.02896 -0.00681 -0.00622 -0.03733 AFIX 137 H35A 2 0.448010 0.711550 0.557666 11.00000 -1.50000 H35B 2 0.429434 0.702989 0.616010 11.00000 -1.50000 H35C 2 0.449073 0.799508 0.607357 11.00000 -1.50000 AFIX 0 C36 1 0.428102 0.882222 0.510716 11.00000 0.09431 0.09337 = 0.03210 0.00123 -0.00519 -0.06984 AFIX 137 H36A 2 0.437224 0.843317 0.479157 11.00000 -1.50000 H36B 2 0.441434 0.924403 0.531909 11.00000 -1.50000 H36C 2 0.414217 0.926524 0.492992 11.00000 -1.50000 AFIX 0 C37 1 0.369143 0.668135 0.364521 11.00000 0.03685 0.03478 = 0.01370 0.00191 0.00053 -0.00621 C38 1 0.384279 0.757354 0.335165 11.00000 0.05708 0.04538 = 0.01627 0.00252 0.00287 -0.01618 AFIX 137 H38A 2 0.379376 0.761062 0.292851 11.00000 -1.50000 H38B 2 0.403880 0.746496 0.338920 11.00000 -1.50000 H38C 2 0.379267 0.821600 0.354937 11.00000 -1.50000 AFIX 0 C39 1 0.377690 0.569039 0.333000 11.00000 0.04195 0.03858 = 0.01483 -0.00144 0.00180 -0.00319 AFIX 137 H39A 2 0.373961 0.574957 0.290196 11.00000 -1.50000 H39B 2 0.367434 0.511277 0.349496 11.00000 -1.50000 H39C 2 0.397138 0.557519 0.339155 11.00000 -1.50000 AFIX 0 C40 1 0.338539 0.685826 0.356049 11.00000 0.04237 0.03682 = 0.02121 -0.00001 -0.00572 -0.00178 AFIX 137 H40A 2 0.334363 0.689186 0.313350 11.00000 -1.50000 H40B 2 0.333304 0.750402 0.375167 11.00000 -1.50000 H40C 2 0.328444 0.629165 0.374231 11.00000 -1.50000 AFIX 0 O41 4 0.355244 0.196753 0.484105 11.00000 0.04984 0.02999 = 0.01436 -0.00022 0.00027 0.00499 C42 1 0.348161 0.143927 0.535122 11.00000 0.05086 0.02947 = 0.01541 0.00282 0.00326 0.01051 C43 1 0.334215 0.052182 0.534755 11.00000 0.06746 0.02578 = 0.02022 -0.00181 0.00266 0.00730 C44 1 0.328072 0.012849 0.591318 11.00000 0.07898 0.02699 = 0.02265 0.00058 0.00463 0.00094 AFIX 43 H44 2 0.318248 -0.049649 0.593699 11.00000 -1.20000 AFIX 0 C45 1 0.335667 0.060921 0.644257 11.00000 0.07643 0.03001 = 0.01901 0.00294 0.00363 0.00631 C46 1 0.351027 0.150142 0.641821 11.00000 0.06015 0.03181 = 0.01680 -0.00079 0.00019 0.00853 AFIX 43 H46 2 0.356880 0.182695 0.677476 11.00000 -1.20000 AFIX 0 C47 1 0.357675 0.190905 0.586729 11.00000 0.04220 0.03149 = 0.01818 0.00097 0.00004 0.01047 N48 3 0.373259 0.276696 0.570645 11.00000 0.03445 0.03847 = 0.01258 0.00028 0.00004 0.00739 C49 1 0.391748 0.333942 0.604022 11.00000 0.02628 0.04390 = 0.01686 -0.00029 -0.00125 0.00846 C50 1 0.395536 0.336729 0.665319 11.00000 0.03680 0.05775 = 0.01503 0.00251 -0.00066 0.00667 AFIX 43 H50 2 0.384616 0.295787 0.690844 11.00000 -1.20000 AFIX 0 C51 1 0.415459 0.400004 0.688940 11.00000 0.03981 0.07651 = 0.01385 -0.00312 -0.00468 0.00557 AFIX 43 H51 2 0.418264 0.401478 0.730860 11.00000 -1.20000 AFIX 0 C52 1 0.431238 0.460746 0.652499 11.00000 0.03157 0.07478 = 0.02045 -0.00597 -0.00408 0.00078 AFIX 43 H52 2 0.444743 0.503756 0.669456 11.00000 -1.20000 AFIX 0 C53 1 0.427469 0.459327 0.590972 11.00000 0.02699 0.06582 = 0.01879 -0.00153 0.00110 -0.00011 AFIX 43 H53 2 0.438372 0.500865 0.565740 11.00000 -1.20000 AFIX 0 C54 1 0.407683 0.396768 0.567133 11.00000 0.02714 0.05421 = 0.01228 -0.00187 0.00065 0.00831 N55 3 0.400020 0.383512 0.507330 11.00000 0.02782 0.05298 = 0.01145 -0.00096 -0.00002 0.00388 C56 1 0.414855 0.405693 0.455144 11.00000 0.02868 0.05871 = 0.01203 0.00054 0.00116 0.00781 C57 1 0.436581 0.470662 0.445715 11.00000 0.02596 0.07812 = 0.01753 -0.00210 0.00163 -0.00067 AFIX 43 H57 2 0.443298 0.512536 0.477079 11.00000 -1.20000 AFIX 0 C58 1 0.448540 0.473579 0.388845 11.00000 0.02541 0.09441 = 0.02088 0.00001 0.00243 -0.00052 C59 1 0.438491 0.408186 0.344773 11.00000 0.03075 0.08822 = 0.01767 0.00021 0.00603 0.00784 AFIX 43 H59 2 0.447218 0.408377 0.306985 11.00000 -1.20000 AFIX 0 C60 1 0.416300 0.342176 0.352803 11.00000 0.03171 0.06246 = 0.01543 -0.00171 0.00075 0.01472 C61 1 0.404332 0.347384 0.408754 11.00000 0.02741 0.05172 = 0.01718 -0.00022 0.00068 0.00855 O62 4 0.381983 0.291281 0.425146 11.00000 0.03477 0.04514 = 0.01268 -0.00226 0.00292 0.00555 C63 1 0.327065 -0.003479 0.476207 11.00000 0.07851 0.02460 = 0.02083 -0.00288 0.00279 0.00260 C64 1 0.352887 -0.023902 0.440711 11.00000 0.08962 0.03512 = 0.02862 -0.00821 0.00597 0.00994 AFIX 137 H64A 2 0.348190 -0.055709 0.402477 11.00000 -1.50000 H64B 2 0.364710 -0.070065 0.463369 11.00000 -1.50000 H64C 2 0.362362 0.040936 0.433466 11.00000 -1.50000 AFIX 0 C65 1 0.313376 -0.107020 0.488384 11.00000 0.10411 0.03155 = 0.03031 -0.00543 0.00235 -0.00449 AFIX 137 H65A 2 0.309274 -0.140890 0.450422 11.00000 -1.50000 H65B 2 0.296510 -0.095932 0.510624 11.00000 -1.50000 H65C 2 0.325603 -0.150352 0.511884 11.00000 -1.50000 AFIX 0 C66 1 0.307714 0.062908 0.439175 11.00000 0.08031 0.03578 = 0.02647 -0.00561 -0.00734 -0.00025 AFIX 137 H66A 2 0.316817 0.126950 0.428188 11.00000 -1.50000 H66B 2 0.291469 0.078404 0.462718 11.00000 -1.50000 H66C 2 0.302484 0.025818 0.402942 11.00000 -1.50000 AFIX 0 C67 1 0.327609 0.017185 0.705713 11.00000 0.10834 0.03207 = 0.02125 0.00185 0.00754 -0.00611 C68 1 0.309045 0.094633 0.737255 11.00000 0.12454 0.05555 = 0.03700 0.00066 0.03280 -0.00917 AFIX 137 H68A 2 0.318513 0.160325 0.741175 11.00000 -1.50000 H68B 2 0.304307 0.068768 0.776955 11.00000 -1.50000 H68C 2 0.292469 0.104228 0.713763 11.00000 -1.50000 AFIX 0 C69 1 0.312382 -0.084629 0.700408 11.00000 0.17544 0.05225 = 0.03006 0.00741 0.01410 -0.03468 AFIX 137 H69A 2 0.295943 -0.074723 0.676501 11.00000 -1.50000 H69B 2 0.307376 -0.108917 0.740286 11.00000 -1.50000 H69C 2 0.324079 -0.135436 0.681042 11.00000 -1.50000 AFIX 0 C70 1 0.353273 -0.001742 0.742494 11.00000 0.13666 0.05321 = 0.02653 0.01060 -0.00596 0.00045 AFIX 137 H70A 2 0.365212 -0.049113 0.721005 11.00000 -1.50000 H70B 2 0.348303 -0.031588 0.781094 11.00000 -1.50000 H70C 2 0.362745 0.063351 0.748942 11.00000 -1.50000 AFIX 0 C71 1 0.405915 0.268426 0.304889 11.00000 0.04401 0.06541 = 0.01443 -0.00602 0.00172 0.01347 C72 1 0.407582 0.157906 0.328783 11.00000 0.07801 0.06325 = 0.03007 -0.00787 -0.00544 0.03025 AFIX 137 H72A 2 0.401016 0.110264 0.298228 11.00000 -1.50000 H72B 2 0.396331 0.151620 0.364644 11.00000 -1.50000 H72C 2 0.426460 0.141539 0.338675 11.00000 -1.50000 AFIX 0 C73 1 0.423134 0.274306 0.247895 11.00000 0.07263 0.10093 = 0.02322 -0.01577 0.01312 0.00286 AFIX 137 H73A 2 0.416451 0.224150 0.218864 11.00000 -1.50000 H73B 2 0.442109 0.259211 0.257563 11.00000 -1.50000 H73C 2 0.421830 0.343309 0.230886 11.00000 -1.50000 AFIX 0 C74 1 0.376609 0.294077 0.288318 11.00000 0.05046 0.06008 = 0.02764 -0.01081 -0.01028 0.01381 AFIX 137 H74A 2 0.375647 0.364722 0.273643 11.00000 -1.50000 H74B 2 0.365024 0.286841 0.323599 11.00000 -1.50000 H74C 2 0.370366 0.247116 0.257086 11.00000 -1.50000 AFIX 0 C75 1 0.472278 0.547606 0.377753 11.00000 0.03194 0.12876 = 0.02601 0.00341 0.00539 -0.01758 PART 1 C76A 1 0.483081 0.542911 0.313841 21.00000 0.05912 0.12000 = 0.03461 0.00302 0.01645 -0.01608 AFIX 137 H76A 2 0.468320 0.557767 0.285852 21.00000 -1.50000 H76B 2 0.490289 0.474272 0.305880 21.00000 -1.50000 H76C 2 0.497554 0.593684 0.308843 21.00000 -1.50000 AFIX 0 C77A 1 0.494986 0.530509 0.420510 21.00000 0.03939 0.13156 = 0.05201 0.01282 -0.00482 -0.01718 AFIX 137 H77A 2 0.500279 0.458135 0.419773 21.00000 -1.50000 H77B 2 0.489089 0.549120 0.460831 21.00000 -1.50000 H77C 2 0.510524 0.573031 0.409042 21.00000 -1.50000 AFIX 0 C78A 1 0.462022 0.662619 0.387952 21.00000 0.05142 0.09884 = 0.07453 0.00441 0.01438 -0.02188 AFIX 137 H78A 2 0.477137 0.710185 0.381616 21.00000 -1.50000 H78B 2 0.455224 0.669969 0.428813 21.00000 -1.50000 H78C 2 0.447425 0.678141 0.359675 21.00000 -1.50000 AFIX 0 PART 0 PART 2 C76B 1 0.498854 0.467463 0.380717 -21.00000 0.05786 0.13269 = 0.13261 -0.01432 0.00624 -0.00284 AFIX 137 H76D 2 0.515719 0.506635 0.376669 -21.00000 -1.50000 H76E 2 0.497547 0.417580 0.348164 -21.00000 -1.50000 H76F 2 0.498823 0.431352 0.419049 -21.00000 -1.50000 AFIX 0 C77B 1 0.475387 0.622707 0.424928 -21.00000 0.07154 0.09275 = 0.06605 0.00256 0.01623 -0.02624 AFIX 137 H77D 2 0.489107 0.673239 0.413272 -21.00000 -1.50000 H77E 2 0.481133 0.588261 0.461664 -21.00000 -1.50000 H77F 2 0.458023 0.657380 0.431732 -21.00000 -1.50000 AFIX 0 C78B 1 0.470228 0.595824 0.318684 -21.00000 0.07860 0.09450 = 0.05575 0.00320 0.00157 -0.03874 AFIX 137 H78D 2 0.469015 0.542565 0.287979 -21.00000 -1.50000 H78E 2 0.486334 0.638098 0.311505 -21.00000 -1.50000 H78F 2 0.453967 0.638966 0.317176 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM rom205_0m_a.res in Pbcn REM R1 = 0.0613 for 12938 Fo > 4sig(Fo) and 0.0866 for all 18163 data REM 758 parameters refined using 79 restraints END WGHT 0.0644 11.3078 REM Highest difference peak 0.483, deepest hole -0.466, 1-sigma level 0.054 Q1 1 0.3545 0.3580 0.4799 11.00000 0.05 0.48 Q2 1 0.3546 0.3629 0.5057 11.00000 0.05 0.34 Q3 1 0.3444 0.4745 0.5215 11.00000 0.05 0.33 Q4 1 0.2455 0.1748 0.5424 11.00000 0.05 0.29 Q5 1 0.3261 0.3831 0.5215 11.00000 0.05 0.28 Q6 1 0.4960 0.5161 0.3635 11.00000 0.05 0.27 Q7 1 0.3254 0.4051 0.4698 11.00000 0.05 0.26 Q8 1 0.4072 0.7609 0.5384 11.00000 0.05 0.26 Q9 1 0.3345 0.0797 0.7603 11.00000 0.05 0.26 Q10 1 0.4426 0.8802 0.6318 11.00000 0.05 0.25 Q11 1 0.3625 0.6057 0.4997 11.00000 0.05 0.25 Q12 1 0.3684 0.1568 0.4793 11.00000 0.05 0.25 Q13 1 0.3941 0.2357 0.4235 11.00000 0.05 0.25 Q14 1 0.3391 0.5266 0.6323 11.00000 0.05 0.25 Q15 1 0.4372 0.9788 0.5417 11.00000 0.05 0.25 Q16 1 0.2234 0.1416 0.5355 11.00000 0.05 0.25 Q17 1 0.4445 0.8292 0.4822 11.00000 0.05 0.24 Q18 1 0.3835 0.2621 0.4808 11.00000 0.05 0.24 Q19 1 0.3728 0.5646 0.4975 11.00000 0.05 0.24 Q20 1 0.2885 0.3403 0.5017 11.00000 0.05 0.24 ; _shelx_res_checksum 82564 _shelx_hkl_file ; 0 -1 0 0.00 0.10 0 -2 0 34.80 1.50 0 -3 0 0.40 0.40 0 -4 0 2.20 0.50 0 5 0 0.40 0.50 0 5 0 -0.10 0.50 0 5 0 -0.60 0.30 0 5 0 -0.70 0.30 0 -5 0 0.30 0.40 0 6 0 30.40 1.70 0 6 0 29.80 1.80 0 6 0 31.70 1.60 0 -6 0 32.30 1.80 0 6 0 30.40 1.70 0 7 0 0.40 0.50 0 -7 0 0.30 0.50 0 7 0 0.40 0.40 0 7 0 0.40 0.60 0 7 0 -0.30 0.50 0 8 0 37.40 2.10 0 8 0 33.90 2.00 0 8 0 36.80 2.20 0 8 0 33.40 2.20 0 -8 0 41.30 2.30 0 9 0 -0.60 0.70 0 9 0 0.30 0.70 0 9 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13 -4 -1.30 0.90 0 13 -4 0.10 1.00 0 14 -4 11.80 1.70 0 14 -4 6.80 1.80 0 14 4 10.20 1.70 0 14 4 6.90 1.50 0 14 -4 9.30 1.60 0 -14 -4 7.70 2.00 0 14 4 7.90 2.10 0 15 4 0.70 1.40 0 15 -4 -1.40 1.40 0 15 -4 0.50 1.20 0 15 4 1.90 1.90 0 15 -4 1.20 1.20 0 15 4 0.10 1.10 0 16 -4 0.40 1.40 0 16 4 3.40 1.60 0 16 -4 3.70 1.80 0 16 4 0.90 1.50 0 16 4 3.40 2.00 0 17 4 1.80 2.30 0 17 4 -0.30 1.60 0 17 -4 -0.30 1.50 0 17 -4 0.30 1.50 0 -1 5 0.60 0.30 0 1 5 -0.30 0.40 0 2 5 391.16 14.20 0 -2 5 383.56 13.90 0 -3 5 0.00 0.30 0 3 5 -0.50 0.40 0 3 5 -0.10 0.40 0 3 -5 -0.10 0.40 0 3 5 -0.30 0.40 0 3 -5 0.20 0.30 0 3 5 0.10 0.30 0 4 -5 1.40 0.50 0 4 5 0.80 0.40 0 -4 5 1.60 0.40 0 4 -5 0.60 0.30 0 4 5 0.70 0.60 0 4 5 0.60 0.40 0 4 -5 1.60 0.40 0 5 -5 0.00 0.40 0 5 5 0.60 0.40 0 5 5 0.60 0.40 0 5 -5 0.30 0.40 0 -5 5 0.00 0.40 0 5 -5 -0.10 0.50 0 5 5 0.80 0.60 0 6 5 23.10 1.50 0 6 -5 20.90 1.40 0 6 5 24.10 1.40 0 6 -5 23.00 1.60 0 6 -5 24.40 1.40 0 6 5 24.80 1.40 0 6 -5 22.70 1.40 0 6 5 30.40 2.00 0 -6 5 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218.68 8.60 0 6 6 218.28 8.90 0 6 -6 226.28 8.30 0 6 -6 220.98 8.30 0 6 6 217.88 8.20 0 -6 6 217.48 8.40 0 6 6 212.58 8.50 0 6 6 216.58 8.30 0 6 -6 220.88 8.30 0 7 6 0.10 0.60 0 7 6 0.40 0.70 0 7 -6 0.20 0.50 0 7 -6 0.00 0.60 0 7 6 -0.30 0.50 0 7 6 0.00 0.50 0 7 -6 0.10 0.40 0 7 -6 0.00 0.40 0 -7 6 0.00 0.50 0 8 6 161.58 7.50 0 -8 6 170.78 7.00 0 8 6 176.28 7.20 0 8 6 173.78 7.00 0 8 -6 177.38 7.00 0 8 6 180.38 6.90 0 8 -6 169.68 7.30 0 -8 -6 186.68 7.60 0 8 -6 170.08 6.90 0 8 -6 180.48 7.00 0 9 -6 0.50 0.60 0 9 6 -0.10 0.60 0 9 6 0.00 0.60 0 9 6 -0.70 0.60 0 9 -6 -0.90 0.50 0 9 -6 0.70 0.90 0 -9 6 0.10 0.70 0 9 6 0.30 0.90 0 -9 -6 -2.00 0.70 0 9 -6 -0.50 0.60 0 10 -6 12.00 1.30 0 10 6 10.90 1.40 0 10 6 9.80 1.80 0 10 -6 8.60 1.50 0 10 -6 12.10 1.40 0 10 -6 12.20 1.40 0 10 6 11.30 1.50 0 10 6 10.60 1.40 0 -10 -6 10.80 1.70 0 11 6 -0.80 0.80 0 11 6 -1.10 0.70 0 11 -6 1.00 0.90 0 11 -6 -0.10 0.90 0 -11 -6 -0.10 1.00 0 11 6 -1.60 1.00 0 11 -6 1.30 0.80 0 12 6 2.10 1.00 0 -12 -6 1.10 1.10 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0.40 0.90 0 11 7 -0.50 0.80 0 11 -7 0.40 0.70 0 11 7 -0.70 1.00 0 11 7 0.00 0.80 0 12 -7 2.20 1.00 0 12 7 2.10 1.10 0 12 -7 3.70 1.40 0 -12 -7 1.30 1.40 0 12 -7 1.70 1.00 0 12 7 2.20 1.00 0 12 7 3.80 1.60 0 13 7 0.70 1.50 0 13 -7 0.20 0.90 0 -13 -7 -0.40 1.30 0 13 -7 -1.50 1.10 0 13 -7 0.40 1.00 0 13 7 0.00 1.10 0 13 7 -0.50 1.00 0 14 -7 7.00 1.70 0 14 7 7.90 2.10 0 14 -7 6.20 2.10 0 14 7 4.40 1.40 0 14 7 9.10 1.90 0 14 -7 8.50 1.60 0 -14 -7 7.50 2.00 0 15 -7 -0.10 1.30 0 15 7 1.80 2.10 0 15 7 -2.30 1.30 0 15 -7 -1.90 1.20 0 15 7 -0.20 1.20 0 16 -7 -0.60 1.30 0 16 7 -0.10 1.50 0 16 7 0.50 1.70 0 16 -7 2.30 1.70 0 0 -8 291.97 10.90 0 0 8 291.07 10.80 0 -1 8 0.50 0.40 0 -1 -8 0.00 0.50 0 1 8 0.20 0.50 0 1 -8 -0.10 0.40 0 -2 -8 3.10 0.70 0 2 8 1.40 0.60 0 2 8 2.90 0.80 0 2 8 3.70 0.60 0 2 -8 3.00 0.60 0 2 -8 2.80 0.50 0 -2 8 2.90 0.60 0 3 8 -0.10 0.30 0 3 -8 0.10 0.40 0 3 8 0.10 0.50 0 -3 8 0.00 0.50 0 3 8 0.30 0.40 0 3 8 -0.60 0.40 0 -3 -8 -0.70 0.40 0 4 8 209.28 8.40 0 4 8 204.38 8.40 0 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4.70 1.50 2 15 2 4.10 2.00 2 15 2 4.90 1.40 2 15 2 4.30 2.50 -2 15 -2 4.30 1.50 -2 16 2 1.90 2.00 -2 16 2 2.30 1.40 -2 16 2 2.80 1.50 2 16 -2 4.00 1.60 2 16 -2 1.10 1.50 -2 16 -2 2.30 1.50 2 16 2 2.60 2.10 2 16 2 2.20 1.50 -2 16 -2 3.40 1.40 -2 16 -2 4.20 2.00 -2 17 2 -0.80 2.00 -2 17 2 -0.70 1.50 2 17 -2 -2.60 1.40 -2 17 2 0.70 1.50 2 17 2 -2.00 2.00 -2 17 -2 -0.80 1.70 -2 17 -2 -0.50 1.40 2 0 3 0.20 0.20 -2 0 3 -0.30 0.20 -2 1 3 6.20 0.50 2 -1 3 5.70 0.50 2 1 3 6.40 0.60 -2 -1 3 7.20 0.40 2 -2 3 385.66 14.10 -2 -2 3 401.56 14.00 2 2 3 387.76 14.20 2 -3 3 29.50 1.40 -2 -3 3 29.70 1.30 2 3 3 30.30 1.60 2 4 -3 9.10 0.70 2 4 -3 8.40 0.90 -2 4 3 9.50 0.90 2 -4 3 8.20 0.80 -2 4 3 7.40 0.70 -2 4 3 8.50 1.00 -2 4 -3 7.60 0.70 2 4 3 8.10 0.80 -2 -4 3 8.30 0.70 -2 4 -3 9.30 0.80 2 4 3 9.90 0.90 -2 4 -3 7.40 0.80 2 4 3 7.80 0.90 2 5 -3 27.20 1.50 2 5 -3 24.80 1.30 -2 5 3 23.90 1.60 -2 5 3 23.50 1.50 2 5 -3 24.50 1.50 2 5 -3 24.40 1.30 2 -5 3 24.70 1.40 -2 5 3 26.90 1.40 -2 5 3 26.90 1.40 -2 5 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0.60 -2 8 3 1.00 0.60 -2 -8 -3 0.60 0.60 -2 8 3 0.80 0.50 2 8 3 1.30 0.80 2 8 3 1.00 0.60 -2 -8 3 0.70 0.60 2 8 3 0.90 0.60 2 8 3 1.20 0.60 -2 8 -3 1.30 0.70 -2 8 -3 0.80 0.50 -2 8 -3 1.50 0.70 2 -8 -3 0.90 0.80 -2 8 -3 1.40 0.60 2 9 -3 115.89 5.00 2 -9 3 126.79 5.40 -2 9 3 116.19 5.20 2 9 -3 113.49 5.30 2 9 -3 121.59 5.00 -2 9 3 124.09 5.10 -2 9 3 115.79 5.20 -2 9 3 122.99 5.60 2 9 -3 120.99 5.30 -2 -9 -3 116.89 5.50 2 9 3 118.89 5.20 2 9 3 119.09 5.10 -2 9 -3 119.09 5.30 2 9 3 114.89 5.60 2 9 3 116.59 5.20 2 -9 -3 121.19 5.60 -2 9 -3 113.29 5.00 -2 -9 3 121.79 5.30 -2 9 -3 120.99 5.40 -2 9 -3 127.59 5.10 -2 -10 -3 -0.40 0.80 2 10 -3 0.20 0.80 2 -10 3 0.30 0.80 2 10 -3 0.90 0.80 -2 10 3 -0.20 0.80 2 10 -3 0.60 0.70 -2 10 3 0.00 0.80 -2 10 3 -0.40 0.70 -2 10 3 0.20 0.70 2 10 -3 0.90 0.70 2 10 3 0.80 0.70 -2 10 -3 -0.30 0.80 -2 10 -3 1.90 1.00 2 10 3 0.20 0.70 2 10 3 0.60 0.80 -2 10 -3 0.20 0.60 -2 -10 3 0.50 0.80 -2 10 -3 0.70 0.70 2 10 3 -0.50 1.00 2 -10 -3 -0.80 0.80 2 11 -3 0.90 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6.70 1.40 -2 14 3 5.40 1.50 -2 14 3 8.20 1.70 2 14 -3 6.80 1.80 -2 14 3 9.60 1.80 -2 14 3 7.70 2.00 2 14 -3 6.50 1.60 -2 14 -3 7.30 1.80 -2 14 -3 9.20 1.90 2 -14 -3 7.60 1.90 2 14 3 6.50 1.60 -2 14 -3 8.60 1.60 2 14 3 4.90 1.50 -2 14 -3 9.60 1.70 2 14 3 5.90 2.00 -2 15 3 12.20 2.30 2 15 -3 9.90 2.10 -2 15 3 10.00 1.90 -2 15 3 6.30 1.60 2 15 -3 10.10 1.70 -2 15 -3 11.50 1.80 2 15 3 8.40 1.80 2 15 3 5.50 1.70 2 15 3 9.50 2.40 -2 15 -3 8.80 1.70 -2 15 -3 10.40 2.00 -2 16 3 0.20 1.40 -2 16 3 0.20 1.70 2 16 -3 -0.30 1.60 2 16 -3 0.60 1.30 -2 16 3 0.50 1.30 -2 16 -3 0.30 1.30 -2 16 -3 -2.10 1.20 2 16 3 2.50 2.10 2 16 3 0.90 1.40 -2 16 -3 -1.20 1.60 -2 17 3 11.50 2.30 2 17 -3 15.00 2.70 -2 17 3 14.50 2.40 -2 17 3 15.30 3.10 -2 17 -3 12.20 2.60 2 17 3 17.00 3.20 2 17 3 12.30 2.40 -2 17 -3 15.30 2.40 -2 0 4 493.55 17.60 2 0 4 491.95 17.70 -2 1 4 1.80 0.40 2 -1 4 0.80 0.30 2 1 4 1.50 0.40 -2 -1 4 1.20 0.20 2 -2 4 250.47 9.00 -2 -2 4 245.18 8.90 2 2 4 244.08 9.20 -2 3 4 49.30 2.20 -2 3 4 50.09 2.20 -2 3 4 48.50 2.40 2 3 -4 49.10 2.20 2 -3 4 46.00 2.10 -2 3 -4 47.90 2.20 2 3 4 58.89 2.40 -2 3 -4 46.30 2.10 2 3 4 48.70 2.10 -2 -3 4 46.20 2.00 2 3 4 49.90 2.30 2 4 -4 23.80 1.40 -2 4 4 25.00 1.40 -2 4 4 21.50 1.50 2 4 -4 25.30 1.30 -2 4 4 24.00 1.30 2 -4 4 23.90 1.40 -2 4 -4 24.60 1.30 2 4 4 23.20 1.20 -2 4 -4 25.20 1.30 2 4 4 24.10 1.30 2 4 4 26.90 1.60 -2 -4 4 24.50 1.30 -2 4 -4 24.10 1.40 -2 5 4 1.50 0.50 -2 5 4 0.50 0.50 -2 5 4 0.70 0.40 -2 5 4 0.60 0.50 2 5 -4 0.30 0.50 2 5 -4 0.90 0.40 2 -5 4 1.10 0.50 2 5 -4 0.40 0.40 -2 -5 4 0.50 0.40 -2 5 -4 0.50 0.40 2 5 4 0.50 0.60 -2 5 -4 1.10 0.50 -2 5 -4 0.20 0.40 -2 5 -4 0.40 0.60 2 5 4 1.00 0.50 2 5 4 0.40 0.40 2 -6 4 1.90 0.60 -2 6 4 0.40 0.70 2 6 -4 1.60 0.50 -2 6 4 2.10 0.60 -2 6 4 1.30 0.50 2 6 -4 1.10 0.60 2 6 -4 0.50 0.50 2 6 -4 1.10 0.50 -2 6 4 0.70 0.50 2 6 4 0.80 0.70 2 6 4 0.90 0.50 2 -6 -4 1.20 0.70 2 6 4 0.60 0.50 -2 6 -4 0.40 0.50 -2 6 -4 1.00 0.40 2 6 4 0.30 0.50 -2 -6 4 1.30 0.50 -2 6 -4 1.20 0.70 -2 6 -4 1.50 0.40 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47.60 2.50 5 1 11 53.09 2.70 -5 -1 11 49.60 2.40 -5 2 11 307.57 11.50 5 2 -11 318.97 11.40 -5 2 11 307.77 11.70 5 -2 11 306.07 11.60 -5 2 11 303.27 11.80 -5 -2 -11 308.37 11.80 5 2 11 309.37 11.80 5 -2 -11 325.47 11.80 -5 2 -11 302.37 11.40 -5 2 -11 310.07 11.70 -5 -2 11 306.87 11.40 5 2 11 292.57 11.70 -5 -3 -11 -0.60 0.50 -5 3 11 -0.60 0.50 5 3 -11 -0.80 0.40 -5 3 11 -1.10 0.50 -5 3 11 0.00 0.40 5 -3 11 2.20 0.80 5 3 11 -0.90 0.40 5 -3 -11 0.80 0.60 -5 3 -11 0.60 0.50 5 3 11 0.20 0.70 -5 -3 11 -0.40 0.40 5 3 11 -1.00 0.70 -5 3 -11 -0.30 0.50 -5 -4 -11 16.70 1.50 -5 4 11 14.50 1.40 -5 4 11 17.10 1.60 5 -4 11 17.40 1.40 5 4 -11 19.00 1.30 -5 4 11 15.10 1.30 5 4 11 18.00 1.70 -5 4 -11 17.90 1.50 5 4 11 22.10 1.90 5 4 11 17.80 1.30 5 4 11 15.10 1.20 5 -4 -11 17.10 1.50 -5 4 -11 16.40 1.40 -5 -4 11 16.40 1.10 -5 5 11 74.49 3.90 5 5 -11 77.79 3.60 -5 5 11 78.39 3.60 5 -5 11 79.99 3.60 -5 -5 -11 79.09 3.70 -5 5 11 82.59 3.70 5 5 11 77.69 3.70 5 -5 -11 75.09 3.70 5 5 11 82.79 3.50 5 5 11 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12.00 2.30 -8 14 -1 11.50 2.20 -8 14 -1 12.00 1.80 8 -14 -1 8.60 2.10 -8 14 -1 12.50 2.00 -8 15 1 11.60 1.90 8 15 -1 7.30 1.80 -8 15 1 7.00 1.80 -8 15 1 8.10 2.10 -8 15 1 8.60 1.90 -8 15 -1 11.40 2.00 8 -15 -1 9.80 2.60 -8 15 -1 8.30 2.00 -8 15 -1 8.90 2.20 8 15 1 10.00 1.90 8 15 1 8.50 2.20 -8 15 -1 7.90 1.70 -8 16 1 -1.00 1.30 -8 16 1 -0.30 1.70 -8 16 1 -0.60 1.80 8 16 -1 -2.70 1.30 -8 16 1 1.70 1.50 -8 16 -1 -2.80 1.20 -8 16 -1 1.90 1.60 -8 16 -1 0.70 1.40 -8 16 -1 0.50 1.80 8 17 -1 4.20 2.10 -8 17 1 8.10 2.40 -8 17 1 4.60 2.30 -8 17 1 7.60 1.90 -8 17 1 6.20 1.80 -8 17 -1 8.10 2.50 -8 17 -1 5.20 1.90 -8 17 -1 7.70 1.90 -8 17 -1 8.10 2.30 8 0 2 713.73 26.30 8 0 -2 759.22 26.20 8 1 -2 205.68 7.40 8 -1 2 205.08 7.70 8 -1 -2 210.68 7.70 8 1 2 209.68 7.60 8 2 -2 291.77 9.60 8 -2 2 259.27 10.00 8 -2 -2 260.47 10.00 8 2 2 265.37 9.90 -8 3 2 199.88 7.50 -8 3 2 198.98 7.50 8 3 -2 200.68 7.50 -8 3 2 196.28 7.60 8 -3 2 208.48 7.70 8 3 2 208.68 7.60 -8 3 -2 203.98 7.60 -8 3 -2 199.28 7.50 -8 3 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7 -2 23.70 1.60 -8 7 2 19.60 1.40 8 7 -2 21.30 1.30 -8 7 2 21.10 1.50 8 7 2 20.90 1.30 8 7 2 21.30 1.40 8 -7 -2 20.80 1.70 -8 7 -2 20.80 1.80 -8 7 -2 21.50 1.50 -8 7 -2 22.80 1.60 8 7 2 20.10 1.40 -8 7 -2 21.60 1.40 -8 -7 2 23.60 1.50 8 7 2 21.30 1.80 -8 8 2 37.50 2.30 -8 8 2 38.70 2.50 8 8 -2 38.80 2.00 8 8 -2 35.00 2.20 8 -8 2 37.90 2.40 -8 8 2 40.80 2.20 8 8 -2 39.10 2.00 -8 8 2 40.80 2.20 8 8 -2 39.40 2.30 8 8 2 36.80 2.10 8 8 2 37.10 2.10 8 8 2 41.30 2.60 -8 8 -2 33.30 2.10 -8 -8 2 38.20 2.20 -8 8 -2 36.20 2.30 -8 8 -2 36.20 2.30 8 -8 -2 40.70 2.60 -8 8 -2 37.40 2.10 8 8 2 39.30 2.00 8 9 -2 20.00 1.40 8 9 -2 21.70 1.80 -8 9 2 19.30 1.80 -8 -9 -2 19.70 1.90 8 9 -2 22.90 2.00 8 -9 2 20.60 2.00 -8 9 2 19.10 1.70 -8 9 2 21.80 1.90 -8 9 2 17.80 1.90 8 9 -2 20.00 1.40 -8 9 -2 21.40 1.90 8 9 2 16.60 1.40 -8 -9 2 18.90 1.70 -8 9 -2 16.10 1.60 8 9 2 20.10 1.70 8 9 2 18.70 1.90 8 9 2 19.60 1.70 -8 9 -2 19.30 1.70 -8 9 -2 16.20 1.80 8 -9 -2 19.20 2.00 -8 10 2 14.30 1.70 -8 10 2 14.10 1.50 8 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1.50 1.90 -8 17 -2 0.20 1.50 8 0 3 -0.50 0.30 8 0 -3 0.20 0.30 8 1 -3 1185.58 41.30 8 -1 3 1144.29 41.60 8 1 3 1188.18 41.60 8 -1 -3 1151.78 41.60 8 -2 3 50.29 2.30 8 -2 -3 50.99 2.30 8 2 3 51.69 2.20 8 3 -3 76.99 3.10 8 -3 3 75.69 3.20 -8 3 3 77.19 3.10 -8 3 3 73.89 3.10 -8 3 3 80.59 3.30 8 3 3 77.99 3.20 -8 3 -3 74.39 3.00 -8 3 -3 76.59 3.20 -8 3 -3 75.89 3.00 -8 -3 3 74.89 2.80 8 -3 -3 72.19 3.30 8 3 3 73.09 3.20 -8 4 3 1.00 0.40 -8 4 3 -0.10 0.50 -8 4 3 1.80 0.50 8 4 -3 0.90 0.40 -8 4 3 0.80 0.40 8 -4 3 1.20 0.50 -8 4 -3 0.70 0.40 -8 -4 3 0.90 0.30 -8 4 -3 1.30 0.50 8 4 3 0.80 0.40 8 -4 -3 0.40 0.50 -8 4 -3 0.60 0.50 8 4 3 0.50 0.50 8 4 3 -0.20 0.60 -8 4 -3 0.70 0.40 8 -5 3 0.70 0.50 8 5 -3 1.00 0.40 -8 5 3 0.40 0.40 -8 5 3 0.90 0.50 -8 5 3 0.20 0.40 -8 5 3 1.00 0.50 8 5 -3 0.50 0.50 8 5 3 0.30 0.40 8 5 3 0.30 0.50 -8 -5 3 0.20 0.30 8 5 3 -1.00 0.60 8 5 3 0.40 0.30 -8 5 -3 0.60 0.50 8 -5 -3 1.00 0.60 -8 5 -3 0.40 0.40 -8 5 -3 0.50 0.40 -8 5 -3 0.50 0.40 8 5 3 0.20 0.40 -8 6 3 29.60 1.70 -8 6 3 28.40 1.60 -8 6 3 27.40 1.90 8 6 -3 26.00 1.70 8 -6 3 30.20 1.90 8 6 -3 26.90 1.70 -8 6 3 26.20 1.60 8 6 -3 28.40 1.50 8 6 -3 30.40 1.50 -8 -6 3 28.30 1.50 8 6 3 26.70 1.50 8 -6 -3 28.50 2.00 8 6 3 30.40 1.60 -8 6 -3 27.40 1.60 8 6 3 29.40 1.60 8 6 3 28.30 2.10 -8 6 -3 25.70 1.70 -8 6 -3 29.30 1.70 -8 6 -3 25.60 1.50 -8 7 3 33.50 2.00 8 7 -3 31.60 1.70 -8 7 3 34.30 2.00 -8 7 3 35.20 2.00 8 -7 3 33.60 2.10 -8 7 3 32.10 2.20 8 7 -3 31.40 2.00 8 7 -3 31.40 1.70 8 7 -3 34.00 2.00 -8 7 -3 30.70 2.00 -8 -7 3 33.70 1.80 -8 7 -3 33.50 1.90 -8 7 -3 31.80 1.80 8 7 3 33.00 1.90 8 7 3 36.40 1.80 8 7 3 31.30 2.30 8 -7 -3 34.80 2.30 -8 7 -3 36.80 2.10 8 7 3 34.40 1.90 -8 8 3 0.50 0.70 8 8 -3 0.60 0.50 8 8 -3 0.40 0.70 -8 8 3 1.00 0.70 8 8 -3 0.50 0.60 8 -8 3 1.70 0.80 -8 8 3 0.70 0.70 8 8 -3 0.60 0.50 -8 8 3 1.70 0.70 -8 8 -3 0.90 0.60 8 8 3 0.50 0.50 -8 8 -3 0.70 0.70 -8 8 -3 0.20 0.70 8 -8 -3 0.00 0.70 -8 -8 3 0.00 0.50 8 8 3 0.20 0.60 -8 8 -3 -0.40 0.50 8 8 3 -0.70 0.60 8 8 3 0.50 0.50 -8 9 3 18.70 1.70 -8 9 3 20.20 2.00 8 -9 3 18.00 1.80 -8 9 3 18.00 1.80 8 9 -3 16.80 1.40 -8 -9 -3 19.10 1.90 8 9 -3 19.20 1.80 8 9 -3 17.30 1.70 -8 9 3 20.80 1.90 8 9 -3 18.90 1.40 8 9 3 19.70 1.40 -8 -9 3 18.20 1.60 8 -9 -3 19.50 2.10 8 9 3 18.90 1.70 -8 9 -3 16.40 1.50 8 9 3 20.50 1.70 -8 9 -3 15.40 1.80 -8 9 -3 20.30 1.80 -8 9 -3 16.80 1.60 8 9 3 20.60 2.10 -8 10 3 1.00 0.80 8 -10 3 0.80 0.90 8 10 -3 0.00 0.90 -8 10 3 0.50 0.80 -8 10 3 0.70 0.80 8 10 -3 0.10 0.80 8 10 -3 -0.40 0.60 -8 -10 -3 1.00 0.80 -8 10 3 -0.40 0.80 8 10 -3 1.00 0.70 -8 10 -3 0.10 0.70 8 10 3 1.40 0.80 8 10 3 1.20 0.80 -8 10 -3 0.50 0.70 8 -10 -3 1.20 0.90 -8 10 -3 -0.90 0.90 8 10 3 0.20 1.00 8 10 3 -0.20 0.60 -8 10 -3 1.60 0.90 8 11 -3 10.30 1.60 -8 11 3 7.30 1.60 -8 11 3 7.00 1.50 -8 11 3 9.60 1.40 8 11 -3 8.30 1.20 -8 11 3 10.40 1.50 8 11 -3 11.20 1.40 8 11 -3 9.70 1.60 8 -11 3 15.60 1.90 -8 -11 -3 11.50 1.70 8 11 3 9.40 1.80 -8 11 -3 11.00 1.80 -8 11 -3 9.40 1.40 8 -11 -3 12.30 1.90 -8 11 -3 10.60 1.50 8 11 3 8.50 1.20 -8 11 -3 9.10 1.50 8 11 3 13.70 1.60 8 11 3 10.20 1.50 -8 12 3 -0.30 0.90 -8 -12 -3 0.80 1.10 -8 12 3 -0.40 0.90 8 -12 3 0.00 1.10 -8 12 3 1.60 1.00 -8 12 3 2.00 1.40 8 12 -3 0.30 1.10 8 12 -3 0.00 0.80 -8 12 -3 -0.40 1.00 -8 12 -3 1.90 1.10 8 -12 -3 -0.90 0.90 -8 12 -3 0.80 0.90 8 12 3 1.00 1.10 8 12 3 0.80 0.90 -8 12 -3 -0.60 1.00 8 12 3 1.00 1.00 8 12 3 0.00 0.80 -8 13 3 5.40 1.40 8 -13 3 5.80 1.60 -8 13 3 2.30 1.40 8 13 -3 4.60 1.50 8 13 -3 3.90 1.20 -8 13 3 5.30 1.60 -8 13 3 6.90 1.40 -8 13 -3 4.10 1.30 -8 13 -3 2.90 1.40 8 13 3 6.70 1.50 -8 13 -3 5.30 1.40 -8 13 -3 5.60 1.60 8 13 3 2.50 1.40 8 -13 -3 4.00 1.60 -8 14 3 7.60 1.60 8 14 -3 10.80 1.80 -8 14 3 5.80 1.50 -8 14 3 6.50 1.90 -8 14 3 8.30 1.70 8 14 3 4.70 1.50 -8 14 -3 5.20 1.40 -8 14 -3 9.70 1.80 8 14 3 5.30 1.90 8 -14 -3 7.80 2.00 -8 14 -3 7.50 2.00 -8 14 -3 5.80 1.70 -8 15 3 -0.90 1.50 8 15 -3 2.30 1.40 -8 15 3 1.30 1.80 -8 15 3 -0.70 1.20 -8 15 3 3.50 1.50 -8 15 -3 -0.10 1.60 -8 15 -3 -0.90 1.20 -8 15 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1.40 0.70 10 10 -4 0.90 0.90 10 10 4 3.90 0.90 10 10 4 3.70 1.30 -10 10 -4 4.80 1.10 -10 10 -4 2.70 1.00 10 10 4 2.30 0.90 -10 10 -4 1.50 1.00 10 10 4 2.20 0.90 -10 10 -4 1.60 0.80 10 -10 -4 4.50 1.40 -10 11 4 3.20 1.10 10 11 -4 6.20 1.30 -10 11 4 4.30 1.50 -10 11 4 4.20 1.30 10 11 -4 4.20 1.00 -10 11 4 3.00 1.10 10 -11 4 5.30 1.40 -10 -11 -4 5.40 1.40 10 11 4 4.00 1.10 10 11 4 4.30 1.30 -10 11 -4 5.80 1.20 10 -11 -4 2.10 1.30 10 11 4 5.70 1.20 -10 11 -4 4.80 1.20 -10 11 -4 3.70 1.20 -10 11 -4 5.10 1.20 10 11 4 2.40 0.90 10 -12 4 2.80 1.40 -10 12 4 7.70 1.40 -10 12 4 8.30 1.70 -10 12 4 10.80 1.70 10 12 -4 7.30 1.50 -10 12 4 7.50 1.80 10 12 -4 7.80 1.30 -10 -12 -4 8.70 1.70 -10 12 -4 6.90 1.50 -10 12 -4 5.50 1.30 10 -12 -4 6.80 1.70 10 12 4 7.70 1.40 -10 12 -4 6.90 1.30 -10 12 -4 5.50 1.50 10 12 4 5.80 1.70 10 -13 4 0.00 1.20 -10 13 4 -0.90 1.00 -10 13 4 1.50 1.30 -10 13 4 0.20 1.20 10 13 -4 2.90 1.40 -10 13 4 1.70 1.20 -10 13 -4 1.70 1.30 10 13 4 3.20 1.70 -10 13 -4 -0.20 1.00 -10 13 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5 52.99 2.50 -10 2 5 49.99 2.20 10 -2 5 53.29 2.40 -10 2 5 49.30 2.20 -10 -2 -5 48.30 2.30 -10 2 5 51.59 2.20 10 2 -5 51.79 1.90 10 -2 -5 48.70 2.40 -10 2 -5 52.29 2.30 -10 2 -5 49.60 2.30 -10 2 -5 53.89 2.20 10 2 5 54.29 2.50 10 2 5 50.29 2.40 10 3 -5 2.60 0.60 -10 3 5 3.00 0.60 10 -3 5 3.00 0.60 -10 -3 -5 3.00 0.50 -10 3 5 3.00 0.60 -10 3 5 3.30 0.70 -10 3 5 3.30 0.50 -10 3 -5 2.80 0.50 10 3 5 3.20 0.70 -10 3 -5 3.70 0.70 -10 3 -5 4.00 0.70 -10 3 -5 1.90 0.40 10 3 5 2.90 0.50 10 -3 -5 2.60 0.80 10 3 5 3.50 0.70 -10 4 5 2.50 0.70 -10 -4 -5 2.20 0.50 10 4 -5 2.10 0.50 -10 4 5 1.80 0.60 -10 4 5 2.30 0.50 -10 4 5 2.00 0.50 10 -4 5 2.60 0.60 -10 4 -5 1.50 0.50 10 -4 -5 1.50 0.70 -10 4 -5 3.30 0.70 10 4 5 3.20 0.60 10 4 5 1.70 0.60 10 4 5 2.20 0.80 -10 4 -5 2.20 0.50 -10 -5 -5 162.08 6.10 10 5 -5 159.38 6.30 10 -5 5 160.08 6.50 -10 5 5 155.48 6.20 -10 5 5 150.98 6.50 10 5 -5 157.08 6.00 -10 5 5 157.78 6.20 -10 5 5 159.68 6.30 10 -5 -5 153.88 6.60 10 5 5 161.48 6.00 -10 5 -5 168.78 6.20 10 5 5 159.88 6.20 -10 5 -5 157.58 6.20 -10 5 -5 155.38 6.40 10 5 5 155.18 6.40 -10 -5 5 161.78 5.90 10 5 5 167.78 6.70 -10 5 -5 160.88 6.20 10 6 -5 50.49 2.20 -10 6 5 48.10 2.70 -10 6 5 46.90 2.40 10 6 -5 52.79 2.20 10 -6 5 50.09 2.70 10 6 -5 52.09 2.60 -10 6 5 48.40 2.40 10 6 -5 51.29 2.40 -10 -6 -5 49.60 2.20 -10 6 5 46.80 2.50 -10 6 -5 49.60 2.40 -10 -6 5 48.10 2.10 10 6 5 49.60 2.40 10 6 5 52.29 2.30 10 6 5 52.59 2.90 -10 6 -5 49.60 2.60 -10 6 -5 50.39 2.40 10 6 5 46.90 2.60 -10 6 -5 53.19 2.50 10 -6 -5 47.60 2.80 10 6 5 50.49 2.30 -10 7 5 97.39 4.40 -10 7 5 91.89 4.60 10 7 -5 104.39 4.10 10 7 -5 103.59 4.30 10 7 -5 98.49 4.40 10 -7 5 98.49 4.50 10 7 -5 105.29 4.00 -10 7 5 98.89 4.30 -10 7 5 94.89 4.30 10 -7 -5 102.79 4.80 -10 7 -5 99.79 4.30 -10 -7 5 99.99 4.00 -10 7 -5 97.29 4.50 10 7 5 95.89 4.10 -10 7 -5 102.69 4.30 10 7 5 97.79 4.30 10 7 5 96.29 4.70 10 7 5 99.09 4.10 -10 7 -5 104.09 4.40 -10 8 5 11.70 1.30 10 8 -5 12.10 1.40 10 -8 5 8.60 1.20 -10 8 5 10.00 1.50 10 8 -5 10.50 1.20 -10 8 5 12.40 1.40 -10 8 5 13.00 1.40 10 8 -5 12.30 1.00 10 8 -5 9.50 1.00 10 -8 -5 10.90 1.60 10 8 5 11.50 1.10 -10 8 -5 11.00 1.20 -10 8 -5 9.30 1.40 10 8 5 12.50 1.40 -10 8 -5 11.10 1.30 10 8 5 9.00 1.50 10 8 5 8.90 1.10 -10 8 -5 12.00 1.30 -10 9 5 0.20 0.70 10 -9 5 0.90 0.80 10 9 -5 1.50 0.60 10 9 -5 1.60 0.60 -10 9 5 0.80 0.80 -10 9 5 0.60 0.80 10 9 -5 0.80 0.80 -10 9 5 0.70 0.70 -10 9 -5 1.00 1.00 -10 9 -5 0.30 0.60 10 9 5 0.40 0.60 10 9 5 -0.50 0.50 10 9 5 0.40 0.90 10 -9 -5 0.70 0.80 -10 9 -5 1.30 0.80 -10 9 -5 0.40 0.70 10 9 5 1.70 0.80 -10 10 5 1.40 1.10 10 -10 5 1.10 1.00 10 10 -5 0.70 0.90 -10 10 5 1.30 0.90 10 10 -5 0.70 0.70 -10 10 5 -0.30 0.80 -10 10 5 0.40 0.90 10 10 5 0.60 0.70 -10 10 -5 1.30 0.80 -10 10 -5 1.10 0.80 -10 10 -5 1.50 0.90 10 -10 -5 0.80 1.00 -10 10 -5 -0.40 0.90 10 10 5 1.10 0.80 10 10 5 0.80 1.00 -10 11 5 52.99 3.30 -10 11 5 60.69 3.80 10 11 -5 52.59 2.90 -10 -11 -5 49.20 3.40 -10 11 5 51.09 3.20 10 -11 5 49.90 3.30 10 11 -5 56.19 3.30 -10 11 5 55.49 3.20 10 11 5 53.49 3.10 10 -11 -5 48.40 3.70 -10 11 -5 56.89 3.10 -10 11 -5 54.69 3.40 10 11 5 58.79 3.90 10 11 5 57.49 3.20 -10 11 -5 51.79 3.10 -10 11 -5 57.39 3.30 10 12 -5 0.10 1.00 10 12 -5 1.10 0.90 -10 12 5 0.80 1.00 -10 12 5 0.40 1.10 -10 -12 -5 1.10 1.00 -10 12 5 1.30 1.40 10 -12 5 -0.40 1.00 -10 12 5 0.60 1.00 10 12 5 -0.80 1.30 10 -12 -5 1.00 1.30 -10 12 -5 -0.60 1.10 -10 12 -5 0.70 0.90 10 12 5 0.50 1.00 -10 12 -5 0.00 0.80 -10 12 -5 0.10 1.10 -10 13 5 1.00 1.30 10 13 -5 -1.20 1.10 -10 13 5 2.30 1.40 -10 13 5 -0.40 1.00 -10 13 5 2.70 1.40 10 13 -5 -0.70 1.00 10 13 5 -0.30 1.50 10 -13 -5 0.10 1.30 10 13 5 2.40 1.20 -10 13 -5 0.70 1.30 -10 13 -5 -0.20 1.10 -10 13 -5 2.20 1.30 -10 13 -5 -1.00 0.90 -10 14 5 3.70 1.50 10 14 -5 2.80 1.50 -10 14 5 5.10 1.90 -10 14 5 3.40 1.40 -10 14 -5 6.80 1.50 -10 14 -5 3.90 1.60 10 14 5 2.70 1.70 -10 14 -5 4.30 1.40 10 -14 -5 5.00 1.90 10 14 5 5.20 1.50 -10 14 -5 3.20 1.60 10 15 -5 3.30 1.50 -10 15 5 -1.10 1.60 -10 15 5 0.90 1.40 -10 15 5 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6 55.09 2.50 -12 3 6 53.49 2.40 -12 3 -6 54.39 2.40 -12 3 -6 52.29 2.50 12 3 6 54.19 2.70 12 3 6 57.69 2.70 -12 3 -6 55.59 2.50 12 -3 -6 54.59 2.80 -12 4 6 6.40 0.80 -12 4 6 8.80 0.80 -12 4 6 7.90 0.80 12 4 -6 4.80 0.80 12 -4 6 6.20 0.90 -12 4 6 5.90 0.80 -12 4 6 7.60 1.00 -12 -4 -6 7.80 0.80 12 4 6 5.30 1.00 -12 4 -6 7.80 0.80 -12 4 -6 6.90 0.80 -12 4 -6 7.30 1.00 12 4 6 5.80 0.70 12 -4 -6 9.00 1.20 -12 4 -6 7.20 0.80 12 -5 6 -0.30 0.50 -12 5 6 1.10 0.50 -12 5 6 0.50 0.60 -12 5 6 0.60 0.50 -12 -5 -6 0.60 0.50 12 5 -6 0.40 0.50 -12 5 6 0.80 0.60 12 5 6 0.70 0.70 12 -5 -6 0.40 0.70 12 5 6 -0.20 0.40 12 5 6 0.80 0.50 -12 5 -6 0.80 0.40 12 5 6 0.80 0.80 -12 5 -6 0.30 0.60 -12 5 -6 0.90 0.50 -12 5 -6 -0.20 0.40 -12 6 6 32.70 2.20 -12 6 6 32.90 1.90 -12 -6 -6 34.80 1.80 12 -6 6 36.00 2.20 -12 6 6 32.70 2.00 -12 6 6 35.70 2.00 12 6 -6 34.60 1.60 12 6 -6 33.50 2.00 12 6 6 34.30 1.90 12 -6 -6 33.80 2.30 -12 6 -6 35.70 1.90 12 6 6 36.20 1.70 12 6 6 37.00 2.20 -12 6 -6 34.60 2.10 12 6 6 35.80 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13 -7 0.30 1.00 -12 13 -7 1.20 1.00 12 13 7 0.20 1.70 -12 14 7 1.60 1.20 12 14 -7 2.80 1.40 -12 14 7 3.80 1.90 -12 14 7 2.30 1.30 12 14 7 2.00 1.30 -12 14 -7 4.20 1.40 -12 14 -7 4.10 1.30 -12 14 -7 3.60 1.70 12 14 7 3.20 1.90 -12 15 7 3.70 1.70 -12 15 7 6.00 1.70 12 15 -7 -1.40 1.40 -12 15 7 3.50 2.00 -12 15 -7 5.30 1.50 12 15 7 5.00 2.10 -12 15 -7 1.90 1.80 -12 15 -7 2.30 1.40 -12 16 7 4.30 1.70 12 16 -7 2.60 1.70 -12 16 7 2.80 1.90 -12 16 7 1.60 1.60 12 16 7 2.00 2.00 -12 16 -7 0.40 1.40 -12 16 -7 1.00 1.60 -12 16 -7 1.20 1.50 -12 0 -8 7.20 0.90 -12 0 8 9.30 0.80 12 -1 8 168.38 6.70 -12 1 8 170.88 6.40 -12 -1 -8 167.88 6.70 -12 1 -8 164.68 6.70 12 1 8 174.88 6.80 -12 2 8 6.40 0.80 -12 2 8 5.10 0.70 -12 -2 -8 8.00 1.00 -12 2 -8 5.60 0.70 12 2 8 6.50 0.90 12 2 8 4.20 0.90 -12 2 -8 6.80 0.90 -12 3 8 87.89 3.90 -12 -3 -8 91.49 3.90 12 3 -8 86.59 3.80 -12 3 8 88.79 3.80 12 -3 8 92.89 4.00 -12 3 8 94.49 3.80 -12 3 8 93.19 3.80 12 3 8 86.29 4.00 12 -3 -8 89.09 4.20 -12 3 -8 88.59 3.80 -12 3 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40.30 2.30 -12 7 8 45.00 2.60 -12 7 8 43.10 2.80 -12 -7 -8 44.90 2.30 -12 7 8 43.00 2.40 12 -7 8 41.00 2.60 -12 7 -8 44.90 2.70 -12 7 -8 45.70 2.30 -12 7 -8 44.40 2.30 12 -7 -8 43.90 2.90 12 7 8 47.60 2.50 12 7 8 46.50 2.80 12 7 8 45.70 2.20 12 7 8 47.40 3.10 12 -8 8 2.40 0.90 12 8 -8 2.20 1.00 -12 8 8 2.30 0.80 -12 8 8 2.70 1.10 -12 8 8 2.50 0.90 -12 8 8 2.90 0.90 12 8 8 0.30 1.20 12 -8 -8 3.90 1.20 12 8 8 2.30 0.90 -12 8 -8 1.30 1.00 -12 8 -8 2.70 0.70 12 8 8 3.20 0.70 -12 8 -8 3.20 0.80 -12 9 8 1.20 1.10 -12 9 8 3.30 1.00 12 9 -8 2.70 1.10 12 -9 8 3.80 1.10 -12 9 8 3.60 1.00 12 9 -8 3.10 0.80 -12 9 8 1.00 0.90 -12 9 -8 2.90 0.90 12 -9 -8 3.10 1.30 12 9 8 -0.20 1.10 -12 9 -8 1.20 0.90 12 9 8 1.70 0.80 -12 9 -8 2.10 0.80 -12 9 -8 2.30 0.90 12 9 8 3.20 0.80 12 10 -8 12.40 1.70 12 10 -8 15.00 1.40 -12 10 8 13.80 1.70 -12 10 8 13.20 1.60 12 -10 8 14.20 1.80 -12 10 8 13.60 1.80 -12 10 8 14.50 2.10 -12 10 -8 12.40 1.40 -12 10 -8 16.20 1.80 -12 10 -8 12.00 1.80 12 -10 -8 14.00 2.20 -12 10 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15 -8 0.00 1.30 12 15 8 0.60 2.10 -12 15 -8 0.50 1.40 -12 15 -8 0.70 1.30 -12 16 8 2.40 1.70 12 16 -8 1.30 1.70 -12 16 8 0.50 1.50 -12 16 8 2.40 1.90 -12 16 -8 1.40 1.70 -12 16 -8 0.70 1.40 -12 16 -8 1.50 1.50 12 16 8 6.40 2.80 -12 0 9 0.10 0.30 12 0 9 -1.60 0.60 -12 0 -9 -1.50 0.40 -12 1 9 19.50 1.30 -12 1 9 18.00 1.10 -12 -1 -9 16.80 1.30 12 -1 9 18.90 1.50 -12 1 -9 18.00 1.40 -12 1 -9 18.60 1.10 12 1 9 22.70 1.60 -12 2 9 59.09 2.80 -12 2 9 65.79 2.90 12 -2 9 69.09 3.20 -12 -2 -9 65.89 3.00 -12 2 9 63.29 2.80 12 2 9 61.79 3.30 -12 2 -9 63.89 3.00 -12 2 -9 67.39 2.80 12 2 9 57.89 3.10 -12 3 9 94.59 4.10 -12 3 9 97.59 4.00 12 -3 9 95.09 4.20 -12 3 9 86.99 3.90 -12 -3 -9 104.09 4.20 12 3 -9 89.09 3.90 -12 3 9 91.39 3.90 12 3 9 92.89 4.30 -12 3 -9 92.99 4.10 12 3 9 90.79 4.20 -12 3 -9 98.19 4.00 -12 4 9 6.60 1.00 -12 4 9 8.90 0.80 -12 4 9 7.90 0.90 -12 -4 -9 6.30 0.90 12 -4 9 6.20 1.10 -12 4 9 5.00 0.80 -12 4 9 6.50 0.90 12 4 -9 6.70 0.90 12 4 9 6.40 1.30 -12 4 -9 5.90 0.90 -12 4 -9 5.90 0.80 -12 4 -9 6.70 1.00 12 4 9 7.00 0.70 12 4 9 8.40 0.90 12 -4 -9 6.20 1.10 12 4 9 9.10 1.20 -12 -5 -9 19.90 1.50 -12 5 9 17.70 1.20 12 -5 9 18.70 1.70 -12 5 9 17.70 1.30 -12 5 9 16.50 1.50 -12 5 9 16.50 1.60 12 5 -9 20.70 1.50 -12 5 9 17.90 1.20 12 5 9 17.90 1.20 12 5 9 21.10 1.70 -12 5 -9 18.80 1.30 12 -5 -9 16.30 1.90 -12 5 -9 18.80 1.70 12 5 9 17.80 1.90 -12 5 -9 16.50 1.30 12 5 9 17.40 1.40 -12 -6 -9 8.90 1.10 -12 6 9 9.50 1.00 -12 6 9 9.30 1.10 12 -6 9 7.80 1.20 12 6 -9 9.00 1.10 -12 6 9 8.60 1.30 -12 6 9 10.00 1.20 12 6 9 10.20 1.40 12 6 9 11.50 1.30 -12 6 -9 11.30 1.40 12 -6 -9 7.40 1.30 -12 6 -9 8.80 1.00 -12 6 -9 9.30 1.00 12 6 9 9.00 0.90 12 6 9 7.70 1.30 -12 7 9 1.50 0.70 -12 7 9 2.80 1.00 12 -7 9 3.70 0.90 -12 7 9 3.30 0.80 -12 -7 -9 3.80 0.90 -12 7 9 3.70 1.00 12 7 -9 4.00 0.90 -12 7 -9 4.50 0.80 -12 7 -9 5.00 1.20 -12 7 -9 5.30 0.90 12 7 9 4.30 1.00 12 7 9 3.90 0.70 12 7 9 2.80 1.10 12 -7 -9 4.40 1.20 12 7 9 1.30 1.10 12 8 -9 14.40 1.70 -12 8 9 18.30 1.60 -12 8 9 15.80 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14 14 9 5.10 2.10 14 14 9 5.30 1.70 -14 14 -9 6.10 1.60 -14 14 -9 7.10 1.50 -14 14 -9 2.80 1.70 -14 15 9 6.90 2.10 -14 15 9 5.20 1.80 -14 15 9 7.30 1.90 14 15 -9 4.70 1.70 -14 15 -9 6.60 2.10 -14 15 -9 9.30 1.90 14 15 9 8.00 2.80 -14 15 -9 7.10 1.70 -14 16 9 -0.30 1.70 14 16 -9 0.80 1.60 -14 16 9 1.10 2.20 -14 16 9 2.00 1.50 14 16 9 1.80 2.60 -14 16 -9 1.80 1.40 -14 16 -9 -1.60 1.70 -14 16 -9 0.20 1.50 -14 0 -10 204.18 8.60 14 0 10 237.38 8.70 -14 0 10 214.08 8.20 -14 -1 -10 29.20 1.90 -14 1 10 31.60 1.70 -14 1 10 31.00 1.70 14 1 10 30.70 2.10 -14 1 -10 32.10 1.90 -14 -1 10 33.20 1.60 -14 1 -10 32.30 1.60 -14 2 10 330.87 12.30 -14 2 10 322.17 12.20 -14 2 10 326.57 12.20 -14 -2 -10 327.77 12.50 14 -2 10 310.87 12.40 14 2 10 322.27 12.50 14 2 10 353.66 12.70 -14 2 -10 328.17 12.50 -14 2 -10 328.97 12.20 -14 -3 -10 4.30 0.90 14 -3 10 6.00 1.10 -14 3 10 5.60 0.80 -14 3 10 4.40 0.80 -14 3 10 5.00 0.80 -14 3 10 5.20 0.80 -14 3 -10 7.30 1.10 14 3 10 5.20 1.10 14 3 10 6.50 1.20 -14 3 -10 5.10 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25.00 1.30 -15 2 4 26.40 1.40 15 2 -4 24.50 1.10 -15 -2 -4 24.30 1.40 -15 2 4 25.40 1.40 -15 2 4 24.40 1.30 15 -2 4 23.40 1.60 -15 2 -4 24.60 1.20 -15 2 -4 23.40 1.40 -15 -2 4 22.30 1.30 15 -2 -4 24.60 1.60 15 2 4 24.60 1.50 -15 2 -4 24.40 1.40 -15 3 4 127.09 5.00 -15 3 4 128.29 5.00 -15 3 4 123.89 5.10 -15 3 4 123.89 5.00 -15 3 4 129.39 5.00 15 -3 4 117.59 5.20 -15 -3 -4 128.79 5.00 -15 3 -4 128.49 5.10 15 3 4 127.09 5.10 -15 -3 4 127.29 5.00 15 3 4 142.39 5.50 15 -3 -4 126.39 5.30 -15 3 -4 122.09 4.90 -15 3 -4 132.79 5.00 -15 3 -4 124.29 4.90 -15 4 4 0.20 0.50 -15 4 4 -0.30 0.40 -15 -4 -4 0.20 0.40 15 4 -4 0.00 0.50 -15 4 4 0.10 0.40 -15 4 4 -0.40 0.40 -15 4 4 1.10 0.50 15 -4 4 0.10 0.50 -15 4 -4 0.10 0.40 -15 4 -4 -0.20 0.30 -15 4 -4 0.00 0.50 15 4 4 0.40 0.50 15 -4 -4 0.60 0.60 15 4 4 -0.20 0.40 -15 4 -4 0.60 0.50 15 4 4 -0.20 0.60 15 -5 4 323.97 12.60 -15 5 4 316.67 12.30 -15 5 4 324.97 12.30 15 5 -4 348.67 12.50 15 5 -4 329.37 12.30 -15 5 4 328.67 12.50 -15 5 4 329.67 12.30 -15 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0.80 15 -8 4 1.20 0.80 -15 8 4 0.70 0.70 -15 8 -4 1.50 0.60 -15 8 -4 2.10 0.80 -15 8 -4 2.00 0.90 15 8 4 1.30 0.60 15 8 4 0.90 1.10 15 -8 -4 0.10 0.90 15 8 4 1.60 0.70 -15 8 -4 -0.60 0.50 -15 9 4 21.40 2.00 15 9 -4 20.70 1.50 -15 9 4 25.40 2.10 15 9 -4 23.50 2.00 -15 9 4 20.00 1.90 -15 9 4 21.20 2.20 15 -9 4 25.40 2.10 15 9 4 23.00 1.70 -15 9 -4 24.90 2.30 -15 9 -4 22.60 1.90 15 9 4 21.40 1.70 -15 9 -4 21.70 1.90 15 9 4 28.00 2.60 -15 9 -4 24.00 2.00 15 -9 -4 25.40 2.40 -15 10 4 2.70 1.00 -15 10 4 3.00 1.10 15 10 -4 1.80 1.10 -15 10 4 1.70 1.00 -15 10 4 1.70 1.00 15 -10 4 2.50 1.10 15 10 4 1.40 1.10 -15 10 -4 1.90 0.90 15 -10 -4 2.30 1.20 -15 10 -4 2.90 1.00 15 10 4 3.80 0.90 -15 10 -4 2.10 0.90 -15 10 -4 1.90 1.20 15 10 4 4.30 1.00 15 11 -4 17.40 1.90 15 -11 4 15.50 2.10 -15 11 4 17.10 2.00 -15 11 4 19.90 2.10 -15 11 4 16.90 1.90 -15 11 4 10.20 1.90 15 11 4 18.90 2.40 15 -11 -4 16.60 2.30 -15 11 -4 17.30 2.20 -15 11 -4 11.60 1.60 -15 11 -4 16.30 1.80 -15 11 -4 13.70 1.80 15 11 4 11.80 1.60 -15 12 4 0.90 1.30 -15 12 4 1.20 1.00 15 -12 4 1.60 1.30 15 12 -4 0.30 1.00 -15 12 4 3.00 1.20 -15 12 4 1.40 1.10 -15 12 -4 0.90 0.90 15 12 4 -0.10 1.40 -15 12 -4 1.60 1.00 -15 12 -4 0.60 1.30 15 -12 -4 -2.00 0.90 -15 12 -4 -0.50 0.90 -15 13 4 16.60 2.40 -15 13 4 20.80 2.30 15 -13 4 19.80 2.60 15 13 -4 17.20 2.20 -15 13 4 19.40 2.40 -15 13 4 17.40 2.30 15 13 4 15.40 2.40 15 -13 -4 15.50 2.40 -15 13 -4 17.30 2.10 -15 13 -4 18.20 2.20 -15 13 -4 21.50 2.60 -15 13 -4 20.40 2.40 15 14 -4 6.90 1.70 15 -14 4 4.90 1.90 -15 14 4 6.40 1.80 -15 14 4 3.50 1.50 -15 14 4 6.10 2.00 -15 14 4 9.10 1.80 15 -14 -4 5.50 1.90 15 14 4 9.00 2.10 -15 14 -4 6.50 1.60 -15 14 -4 5.80 1.80 -15 14 -4 4.70 1.60 -15 14 -4 0.50 1.50 -15 15 4 1.50 1.80 -15 15 4 2.80 1.80 -15 15 4 2.50 1.40 -15 15 4 2.90 1.50 15 15 -4 5.20 1.80 -15 15 -4 0.70 1.30 -15 15 -4 1.00 1.20 -15 15 -4 1.30 1.60 -15 15 -4 1.50 1.60 15 15 4 2.30 2.10 15 16 -4 4.60 1.80 -15 16 4 5.70 1.80 -15 16 4 2.30 2.10 -15 16 4 5.10 1.80 -15 16 -4 6.60 2.20 -15 16 -4 5.40 1.70 15 16 4 6.30 2.80 -15 16 -4 4.20 1.70 15 0 5 0.50 0.60 -15 0 -5 -0.30 0.40 15 0 -5 -0.10 0.30 -15 0 5 -0.20 0.40 -15 -1 -5 1.20 0.50 -15 1 5 0.60 0.40 -15 1 5 1.90 0.50 15 1 -5 1.50 0.40 15 1 5 1.50 0.60 -15 -1 5 0.30 0.40 -15 1 -5 0.40 0.40 15 -1 -5 1.30 0.50 -15 1 -5 0.60 0.50 -15 -2 -5 14.90 1.10 -15 2 5 14.70 1.00 15 2 -5 13.80 0.70 -15 2 5 15.40 1.10 -15 2 5 14.70 1.00 15 -2 5 15.40 1.20 -15 2 5 15.70 1.10 -15 2 -5 15.10 0.90 -15 2 -5 11.80 1.10 -15 2 -5 12.80 1.00 15 2 5 15.30 1.30 15 -2 -5 15.30 1.20 -15 -3 -5 17.10 1.10 -15 3 5 14.20 1.00 -15 3 5 14.70 1.20 -15 3 5 15.10 1.00 15 -3 5 12.30 1.20 -15 3 5 13.60 1.00 15 3 5 12.30 1.20 15 3 5 17.20 1.80 -15 3 -5 15.90 1.20 -15 3 -5 13.60 1.00 15 -3 -5 12.10 1.20 -15 3 -5 16.20 1.20 -15 4 5 5.70 0.80 -15 4 5 6.00 0.70 15 -4 5 6.80 1.00 -15 -4 -5 6.00 0.70 -15 4 5 5.40 0.70 -15 4 5 4.30 0.70 -15 4 5 4.70 0.70 15 4 -5 6.20 0.80 -15 4 -5 4.10 0.60 15 -4 -5 5.20 0.90 15 4 5 6.70 1.00 15 4 5 5.60 1.20 15 4 5 7.10 0.80 -15 4 -5 5.40 0.80 -15 4 -5 5.10 0.70 -15 4 -5 4.80 0.70 -15 5 5 6.60 0.90 15 5 -5 8.20 1.00 15 -5 5 5.20 1.00 -15 5 5 6.20 0.90 -15 5 5 4.70 0.90 -15 5 5 6.20 0.70 -15 5 5 8.00 1.00 15 5 5 9.40 0.90 -15 5 -5 5.90 0.90 -15 5 -5 6.60 0.80 15 5 5 6.60 1.10 15 -5 -5 6.10 1.10 15 5 5 9.40 1.20 -15 5 -5 8.90 0.90 -15 5 -5 7.70 0.80 15 -6 5 2.00 0.80 -15 6 5 0.40 0.50 -15 6 5 1.20 0.50 -15 6 5 0.10 0.50 -15 6 5 0.20 0.50 15 6 -5 -0.20 0.50 -15 -6 -5 0.90 0.50 15 6 -5 0.60 0.50 15 -6 -5 0.60 0.80 15 6 5 0.00 0.40 15 6 5 0.70 0.40 -15 6 -5 2.20 0.60 15 6 5 0.10 0.80 -15 6 -5 -0.20 0.60 -15 6 -5 1.00 0.60 15 6 5 0.80 0.60 15 6 5 0.90 0.50 -15 -7 -5 3.10 0.60 15 -7 5 3.60 1.00 -15 7 5 3.60 0.80 -15 7 5 6.30 1.00 15 7 -5 3.10 0.80 -15 7 5 4.30 0.80 15 7 -5 3.50 0.70 15 7 -5 3.10 0.60 -15 7 5 5.40 1.10 15 -7 -5 2.80 1.00 -15 7 -5 5.10 1.00 15 7 5 3.60 0.70 -15 7 -5 4.60 0.80 15 7 5 3.50 0.90 15 7 5 3.80 1.20 15 7 5 4.90 0.70 -15 7 -5 4.60 0.80 15 7 5 2.20 0.60 -15 7 -5 3.80 0.80 -15 8 5 34.30 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1.50 -15 16 5 -0.40 1.40 -15 16 5 -1.50 1.40 15 16 5 4.50 2.50 -15 16 -5 0.20 1.80 -15 16 -5 1.90 1.50 -15 16 -5 0.00 1.30 -15 0 -6 4.50 0.70 15 0 -6 4.30 0.60 15 0 6 2.90 0.70 15 1 -6 19.00 1.10 -15 1 6 20.60 1.30 -15 1 6 21.40 1.30 -15 -1 -6 20.90 1.40 -15 1 6 18.50 1.10 15 -1 6 19.00 1.40 -15 1 -6 21.00 1.40 -15 1 -6 21.80 1.10 -15 1 -6 20.00 1.20 15 -1 -6 20.10 1.30 15 1 6 19.30 1.50 -15 2 6 125.19 4.90 -15 2 6 130.29 4.90 -15 2 6 125.69 5.00 -15 2 6 126.19 5.00 -15 -2 -6 133.09 5.10 15 2 -6 125.79 4.60 15 -2 6 118.59 5.20 -15 2 -6 124.29 4.80 -15 2 -6 127.19 5.00 15 -2 -6 125.39 5.20 -15 2 -6 128.49 5.10 15 2 6 120.09 5.10 -15 3 6 63.49 2.80 -15 -3 -6 60.19 2.80 -15 3 6 59.59 2.70 -15 3 6 55.19 2.60 -15 3 6 57.59 2.60 15 -3 6 59.09 2.90 -15 3 -6 63.09 2.80 15 -3 -6 59.69 3.00 -15 3 -6 62.79 2.80 15 3 6 62.79 3.10 15 3 6 59.79 2.90 -15 3 -6 59.09 2.60 15 4 -6 26.00 1.60 15 -4 6 25.60 1.70 -15 4 6 24.50 1.50 -15 4 6 26.10 1.60 -15 -4 -6 28.60 1.60 -15 4 6 25.10 1.50 -15 4 6 25.10 1.40 -15 4 6 25.50 1.70 15 4 6 27.60 1.90 -15 4 -6 26.00 1.60 -15 4 -6 26.60 1.50 15 4 6 25.30 1.50 15 -4 -6 31.00 2.00 -15 4 -6 29.10 1.50 15 4 6 22.50 1.90 -15 4 -6 27.90 1.60 -15 5 6 52.39 2.30 15 -5 6 56.09 2.90 -15 5 6 52.29 2.50 -15 5 6 49.00 2.50 -15 5 6 49.20 2.70 -15 5 6 53.69 2.40 15 5 -6 49.20 2.50 -15 -5 -6 54.69 2.50 15 5 6 51.29 2.20 15 -5 -6 44.20 2.80 15 5 6 47.20 2.90 -15 5 -6 51.09 2.40 15 5 6 50.09 2.40 -15 5 -6 46.50 2.40 -15 5 -6 46.70 2.40 -15 5 -6 52.19 2.60 15 5 6 51.59 2.80 -15 6 6 18.10 1.40 15 6 -6 19.90 1.50 -15 -6 -6 17.60 1.30 -15 6 6 20.80 1.70 15 -6 6 15.40 1.60 -15 6 6 19.50 1.40 -15 6 6 17.30 1.60 -15 6 -6 19.30 1.30 15 -6 -6 21.20 2.00 -15 6 -6 17.20 1.30 15 6 6 15.90 1.70 15 6 6 19.30 1.10 -15 6 -6 20.40 1.70 15 6 6 18.30 1.30 15 6 6 17.70 1.70 -15 6 -6 17.70 1.40 15 7 -6 0.00 0.60 -15 7 6 0.00 0.50 -15 -7 -6 0.80 0.50 -15 7 6 0.20 0.50 15 -7 6 0.70 0.80 -15 7 6 -0.40 0.60 -15 7 6 0.20 0.60 15 7 6 1.40 0.60 15 7 6 0.30 0.50 -15 7 -6 -0.70 0.50 15 7 6 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1.40 15 -11 -6 3.40 1.50 -15 11 -6 8.10 1.50 -15 11 -6 3.20 1.30 15 11 6 5.90 1.80 15 11 6 5.30 1.20 -15 11 -6 6.50 1.30 -15 11 -6 5.80 1.30 -15 12 6 3.30 1.30 15 -12 6 4.20 1.40 -15 12 6 2.50 1.50 -15 12 6 2.90 1.20 -15 -12 -6 3.50 1.80 -15 12 6 4.10 1.40 15 12 -6 3.90 1.40 -15 12 -6 2.10 1.10 15 12 6 2.80 1.60 -15 12 -6 6.20 1.60 -15 12 -6 2.70 1.20 15 12 6 3.70 1.30 -15 12 -6 3.30 1.10 15 -12 -6 1.10 1.40 -15 13 6 11.00 1.90 15 13 -6 12.90 1.90 15 -13 6 8.30 1.90 -15 13 6 14.40 2.00 -15 13 6 13.20 2.30 -15 13 6 13.90 2.10 15 13 6 14.30 2.50 -15 13 -6 9.50 1.60 15 -13 -6 11.30 2.20 -15 13 -6 12.80 1.90 -15 13 -6 14.60 2.00 -15 13 -6 10.90 2.00 -15 14 6 7.80 1.90 15 14 -6 4.30 1.50 -15 14 6 7.50 2.00 -15 14 6 6.70 1.70 15 14 6 7.70 2.30 -15 14 -6 7.90 1.80 -15 14 -6 10.40 1.90 -15 14 -6 10.30 1.70 -15 14 -6 8.40 2.10 -15 15 6 4.90 2.00 15 15 -6 8.30 2.00 -15 15 6 7.10 1.90 -15 15 6 6.10 1.80 15 15 6 7.50 2.60 -15 15 -6 6.20 1.70 -15 15 -6 5.70 1.60 -15 15 -6 7.00 2.10 -15 16 6 3.40 1.80 15 16 -6 2.40 1.70 -15 16 6 3.00 2.10 -15 16 6 3.30 1.60 -15 16 -6 3.40 1.50 -15 16 -6 5.30 1.70 15 16 6 5.00 2.60 -15 16 -6 1.50 1.60 15 0 -7 0.10 0.40 15 0 7 -0.50 0.60 -15 0 -7 0.10 0.50 -15 1 7 38.70 1.90 -15 1 7 39.50 1.80 15 -1 7 38.30 2.20 15 1 -7 42.70 1.90 -15 -1 -7 40.50 2.10 -15 1 7 40.20 1.90 -15 1 7 40.50 2.10 -15 1 -7 40.00 1.90 -15 1 -7 43.00 2.20 15 1 7 41.80 2.30 15 -1 -7 41.10 2.10 -15 2 7 34.40 1.80 -15 2 7 34.60 1.80 -15 2 7 34.40 1.70 -15 -2 -7 33.90 1.90 -15 2 7 29.70 1.70 15 2 -7 33.90 1.50 -15 2 -7 33.20 1.60 15 2 7 39.80 2.10 15 2 7 39.80 2.20 -15 2 -7 32.80 1.90 -15 2 -7 34.90 1.80 15 -2 -7 34.70 2.00 -15 3 7 7.00 0.80 15 -3 7 7.20 1.10 -15 3 7 6.70 0.80 -15 -3 -7 8.30 0.90 -15 3 7 6.90 0.90 -15 3 7 6.00 0.80 15 3 7 5.40 1.40 -15 3 -7 7.50 0.90 -15 3 -7 6.70 0.90 15 3 7 6.60 1.00 15 -3 -7 6.90 1.00 -15 3 -7 7.60 0.80 15 4 -7 11.20 1.10 -15 4 7 10.00 1.10 -15 4 7 8.60 0.90 -15 4 7 9.80 0.90 -15 -4 -7 9.60 1.00 15 -4 7 8.70 1.10 -15 4 7 9.90 1.10 -15 4 7 9.10 1.00 15 4 7 8.50 1.30 15 -4 -7 8.20 1.20 -15 4 -7 11.00 1.10 15 4 7 4.50 1.30 15 4 7 9.00 1.00 15 4 7 11.20 0.80 -15 4 -7 10.70 1.10 -15 4 -7 10.60 1.00 -15 5 7 1.30 0.50 15 -5 7 2.30 0.70 -15 5 7 2.60 0.60 -15 5 7 2.70 0.60 -15 -5 -7 2.70 0.60 -15 5 7 3.20 0.70 -15 5 7 2.40 0.70 15 5 -7 1.40 0.60 15 5 7 2.60 0.70 -15 5 -7 2.10 0.60 15 5 7 2.60 0.90 15 -5 -7 2.10 0.80 15 5 7 2.20 0.90 -15 5 -7 1.30 0.50 -15 5 -7 1.70 0.70 15 5 7 3.20 0.50 -15 5 -7 1.80 0.50 -15 -6 -7 0.90 0.60 15 -6 7 0.50 0.60 -15 6 7 0.40 0.50 -15 6 7 -0.50 0.50 -15 6 7 0.50 0.60 -15 6 7 0.10 0.60 15 6 -7 -0.30 0.60 -15 6 -7 -0.10 0.40 15 6 7 0.60 0.60 15 -6 -7 1.00 0.80 -15 6 -7 -0.20 0.40 15 6 7 -0.40 0.50 -15 6 -7 0.00 0.50 15 6 7 0.10 0.40 15 6 7 -0.50 0.70 -15 6 -7 0.10 0.70 -15 7 7 4.50 0.90 15 -7 7 4.40 1.10 -15 7 7 3.40 0.90 -15 -7 -7 3.80 0.80 -15 7 7 4.50 0.90 -15 7 7 4.00 1.10 15 7 -7 3.30 0.90 15 7 7 5.10 0.70 -15 7 -7 4.40 0.90 15 7 7 4.50 1.30 -15 7 -7 5.20 1.10 15 -7 -7 4.90 1.20 15 7 7 3.30 1.00 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50.09 2.40 -15 0 -8 51.89 2.60 -15 0 8 54.89 2.40 15 1 -8 116.19 4.50 -15 1 8 118.99 4.50 -15 1 8 113.69 4.70 15 -1 8 106.49 4.80 -15 -1 -8 114.89 4.80 -15 1 8 113.89 4.50 15 -1 -8 115.69 4.80 15 1 8 111.79 4.80 -15 1 -8 111.79 4.80 -15 1 -8 112.69 4.50 -15 2 8 53.99 2.50 -15 2 8 53.09 2.60 -15 2 8 53.49 2.50 15 2 -8 54.59 2.20 -15 2 8 54.59 2.50 15 -2 8 57.59 2.80 -15 -2 -8 53.79 2.70 15 -2 -8 54.29 2.80 -15 2 -8 54.59 2.70 -15 2 -8 57.59 2.60 15 2 8 58.09 2.90 15 2 8 52.69 2.80 -15 3 8 29.50 1.60 -15 3 8 27.30 1.70 15 -3 8 31.80 1.90 -15 3 8 25.10 1.60 -15 -3 -8 31.00 1.80 -15 3 8 24.00 1.50 15 3 8 29.20 1.90 -15 3 -8 26.10 1.50 15 -3 -8 29.10 2.00 -15 3 -8 28.50 1.70 15 3 8 30.60 2.10 -15 3 -8 26.80 1.70 -15 4 8 5.10 0.80 -15 4 8 5.60 0.70 -15 4 8 7.90 1.00 15 -4 8 5.80 1.00 -15 -4 -8 7.20 0.90 15 4 -8 5.80 0.80 -15 4 8 5.70 0.80 -15 4 8 4.50 0.80 -15 4 -8 5.70 0.80 -15 4 -8 5.40 0.90 15 -4 -8 3.80 0.90 15 4 8 5.60 0.80 15 4 8 6.60 0.70 15 4 8 5.60 1.20 -15 4 -8 5.50 0.80 15 4 8 5.30 1.00 -15 5 8 44.70 2.50 15 -5 8 45.00 2.60 15 5 -8 40.90 2.30 -15 5 8 39.00 2.30 -15 5 8 42.40 2.30 -15 -5 -8 43.90 2.30 -15 5 8 44.40 2.10 -15 5 8 42.90 2.20 -15 5 -8 43.60 2.20 15 5 8 44.30 2.80 15 5 8 43.30 2.60 15 5 8 43.50 2.30 -15 5 -8 42.40 2.40 15 -5 -8 45.30 2.70 -15 5 -8 45.00 2.30 15 5 8 46.20 2.00 -15 -6 -8 57.49 2.80 -15 6 8 58.59 2.80 -15 6 8 56.99 2.90 15 -6 8 57.59 3.20 -15 6 8 59.99 3.00 -15 6 8 58.69 3.20 15 6 -8 58.69 2.90 -15 6 -8 54.39 2.80 15 6 8 58.79 3.30 -15 6 -8 59.39 2.90 15 6 8 62.49 2.90 -15 6 -8 58.19 3.10 15 6 8 54.19 3.30 15 -6 -8 65.99 3.60 -15 6 -8 59.19 2.70 15 6 8 63.19 2.60 15 7 -8 0.90 0.70 -15 7 8 0.90 0.70 -15 7 8 0.10 0.80 -15 -7 -8 1.40 0.60 15 -7 8 2.60 0.90 -15 7 8 1.30 0.70 -15 7 8 1.10 0.70 15 7 8 1.60 0.70 15 7 8 1.00 1.10 -15 7 -8 0.90 0.60 -15 7 -8 1.00 0.80 15 7 8 0.70 0.80 -15 7 -8 0.40 0.60 15 -7 -8 1.10 0.90 15 7 8 1.50 0.60 -15 8 8 18.50 1.90 -15 8 8 22.20 1.80 15 -8 8 19.00 2.00 15 8 -8 16.00 1.70 -15 8 8 13.90 1.80 -15 8 8 17.40 1.60 15 -8 -8 19.30 2.20 -15 8 -8 19.70 1.70 15 8 8 17.50 1.70 15 8 8 19.80 2.10 15 8 8 20.80 2.40 -15 8 -8 21.10 1.70 -15 8 -8 19.70 2.10 -15 9 8 0.40 0.80 15 -9 8 0.60 0.90 -15 9 8 -0.20 0.80 -15 9 8 -0.20 0.90 15 9 -8 0.20 0.80 -15 9 8 0.90 0.90 -15 9 -8 -0.20 0.60 -15 9 -8 0.00 0.90 15 -9 -8 -0.40 0.90 15 9 8 0.40 1.20 15 9 8 -0.40 0.80 -15 9 -8 0.40 0.60 -15 10 8 24.30 2.20 15 10 -8 26.20 2.40 -15 10 8 20.80 2.40 15 -10 8 23.70 2.50 -15 10 8 22.80 2.20 -15 10 8 32.20 2.50 15 -10 -8 25.90 2.90 -15 10 -8 28.60 2.30 -15 10 -8 26.60 2.20 -15 10 -8 24.20 2.50 15 10 8 24.30 2.90 15 10 8 27.20 2.30 -15 11 8 1.30 1.20 15 -11 8 2.30 1.20 -15 11 8 1.30 1.10 -15 11 8 5.40 1.40 15 11 -8 4.70 1.40 -15 11 -8 3.50 1.10 -15 11 -8 2.80 1.40 -15 11 -8 2.20 1.00 -15 11 -8 2.30 0.90 15 11 8 3.40 1.20 15 -11 -8 3.00 1.40 15 11 8 4.50 1.80 -15 12 8 4.00 1.40 15 -12 8 5.00 1.50 -15 12 8 3.70 1.40 -15 12 8 5.20 1.70 15 12 -8 3.70 1.50 -15 12 -8 3.80 1.20 15 12 8 4.40 1.40 -15 12 -8 4.50 1.30 -15 12 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-9 60.59 3.10 15 -2 9 22.80 1.80 -15 2 9 23.70 1.40 -15 -2 -9 22.10 1.60 -15 2 9 23.80 1.50 -15 2 9 22.50 1.40 -15 2 9 24.80 1.50 15 2 -9 24.00 1.20 15 2 9 20.80 1.60 -15 2 -9 24.70 1.70 -15 2 -9 25.30 1.50 15 -2 -9 22.20 1.70 15 2 9 25.10 1.80 -15 3 9 6.10 0.80 15 -3 9 4.80 1.10 -15 3 9 5.30 0.90 -15 -3 -9 4.20 0.80 -15 3 9 4.30 0.80 -15 3 9 5.30 0.80 15 3 -9 4.10 0.40 -15 3 -9 5.40 0.80 15 -3 -9 4.50 1.00 -15 3 -9 3.20 0.60 -15 3 -9 4.80 0.80 15 3 9 5.50 1.10 15 3 9 5.10 1.10 -15 4 9 31.70 1.80 -15 4 9 33.00 2.00 15 -4 9 33.10 2.20 -15 -4 -9 33.20 2.00 -15 4 9 33.60 1.80 -15 4 9 34.10 1.90 -15 4 9 34.30 1.90 15 4 -9 33.10 1.90 -15 4 -9 32.70 2.00 15 4 9 33.70 1.90 15 4 9 33.80 2.20 15 4 9 33.10 1.60 15 -4 -9 31.00 2.20 -15 4 -9 31.30 1.90 15 4 9 35.00 2.40 -15 4 -9 32.80 1.80 15 5 -9 -0.20 0.60 -15 5 9 0.50 0.50 -15 5 9 0.50 0.50 -15 5 9 1.10 0.50 -15 5 9 0.20 0.60 -15 5 9 0.50 0.50 -15 -5 -9 1.00 0.60 15 -5 9 0.00 0.70 -15 5 -9 0.90 0.70 -15 5 -9 0.90 0.60 15 5 9 -0.20 0.80 15 -5 -9 0.60 0.90 -15 5 -9 0.50 0.60 15 5 9 0.40 0.50 15 5 9 0.60 0.40 15 5 9 0.10 0.70 -15 6 9 61.49 3.00 -15 6 9 55.59 3.20 15 -6 9 58.19 3.20 -15 6 9 61.19 2.80 -15 -6 -9 60.99 3.00 15 6 -9 59.69 3.00 -15 6 9 57.39 2.90 -15 6 -9 60.09 2.80 15 6 9 50.59 3.40 15 6 9 57.39 2.90 15 6 9 59.69 3.30 15 -6 -9 52.19 3.30 -15 6 -9 58.09 3.10 -15 6 -9 55.49 2.80 15 6 9 57.79 2.60 15 -7 9 6.20 1.10 -15 7 9 5.80 1.20 -15 7 9 6.50 1.10 -15 7 9 6.30 1.10 15 7 -9 6.10 1.10 -15 -7 -9 5.50 1.00 -15 7 9 3.70 0.90 -15 7 -9 4.60 1.20 15 -7 -9 6.60 1.40 15 7 9 6.40 1.00 -15 7 -9 5.30 0.90 15 7 9 4.80 1.40 15 7 9 4.60 1.00 15 7 9 4.60 1.20 -15 8 9 2.40 0.90 -15 8 9 3.50 1.10 15 -8 9 1.70 0.80 15 8 -9 2.00 0.90 -15 8 9 1.60 0.90 -15 8 9 3.40 1.00 15 8 9 0.20 1.20 15 -8 -9 2.40 1.20 -15 8 -9 1.20 0.70 -15 8 -9 1.90 1.00 15 8 9 2.10 0.80 15 8 9 0.20 1.00 -15 8 -9 1.20 0.60 -15 9 9 -0.60 0.80 -15 9 9 0.30 0.80 15 -9 9 1.00 0.90 15 9 -9 0.40 0.80 -15 9 9 -1.30 0.80 -15 9 9 -0.70 1.00 -15 9 -9 -1.40 1.00 -15 9 -9 0.80 0.70 -15 9 -9 -0.20 0.60 15 9 9 0.00 0.80 15 9 9 -1.10 1.30 15 -9 -9 -1.20 0.80 15 10 -9 17.50 2.00 -15 10 9 14.30 1.90 15 -10 9 22.40 2.30 -15 10 9 16.00 2.20 -15 10 9 18.80 2.00 -15 10 -9 16.80 1.80 -15 10 -9 16.10 2.00 15 10 9 19.60 2.00 15 -10 -9 15.90 2.40 -15 10 -9 19.00 1.80 15 10 9 13.90 2.20 -15 11 9 1.90 1.20 -15 11 9 1.90 1.00 15 11 -9 2.90 1.20 15 -11 9 2.10 1.20 -15 11 9 1.60 1.00 15 11 9 1.90 1.70 15 -11 -9 1.00 1.30 -15 11 -9 1.70 1.20 15 11 9 1.70 1.10 -15 11 -9 4.90 1.20 -15 11 -9 3.00 1.10 -15 12 9 7.80 1.60 -15 12 9 5.20 1.80 15 12 -9 3.50 1.30 -15 12 9 3.10 1.20 -15 12 -9 3.10 1.40 15 12 9 3.40 1.30 -15 12 -9 3.70 1.20 15 12 9 5.70 1.80 15 -12 -9 6.20 1.90 -15 12 -9 4.20 1.20 -15 13 9 5.80 1.60 -15 13 9 12.60 2.40 -15 13 9 10.00 1.90 15 13 -9 9.70 1.80 -15 13 -9 9.10 1.60 -15 13 -9 11.80 1.80 -15 13 -9 8.60 1.90 15 -13 -9 7.00 2.20 15 13 9 11.00 1.90 15 13 9 11.70 2.60 -15 14 9 3.50 2.00 -15 14 9 1.30 1.50 -15 14 9 5.30 1.60 15 14 -9 2.20 1.40 -15 14 -9 4.20 1.80 -15 14 -9 4.50 1.40 -15 14 -9 2.90 1.20 15 14 9 4.90 2.00 -15 15 9 1.20 1.70 -15 15 9 2.90 1.60 -15 15 9 -0.20 1.40 15 15 -9 -0.40 1.50 -15 15 -9 1.00 1.70 15 15 9 1.70 2.20 -15 15 -9 0.30 1.10 -15 15 -9 0.00 1.30 15 16 -9 0.70 1.50 -15 16 9 0.00 1.60 -15 16 9 1.10 1.60 -15 16 9 0.50 2.10 -15 16 -9 1.20 1.90 -15 16 -9 0.70 1.40 -15 16 -9 -1.40 1.30 15 16 9 1.10 2.50 -15 0 -10 2.00 0.70 15 0 10 0.40 0.80 -15 0 10 2.70 0.50 15 -1 10 101.99 4.70 -15 1 10 111.59 4.40 -15 -1 -10 109.19 4.80 -15 1 10 108.89 4.40 -15 1 -10 108.09 4.40 15 -1 -10 109.59 4.70 -15 1 -10 110.29 4.80 15 1 10 113.69 4.80 -15 -1 10 106.69 4.30 -15 2 10 13.80 1.20 -15 2 10 12.20 1.10 -15 2 10 11.60 1.10 -15 -2 -10 10.60 1.20 15 -2 10 13.50 1.50 15 -2 -10 7.60 1.10 -15 2 -10 8.30 1.10 15 2 10 9.50 1.30 -15 2 -10 10.30 1.00 15 2 10 12.40 1.50 -15 -3 -10 -0.70 0.50 -15 3 10 0.80 0.50 -15 3 10 0.50 0.50 15 -3 10 -0.50 0.80 -15 3 10 0.20 0.50 -15 3 10 0.00 0.50 15 3 10 1.30 0.90 -15 3 -10 -0.30 0.60 15 -3 -10 -0.20 0.60 15 3 10 1.20 0.70 -15 3 -10 -0.20 0.50 -15 4 10 5.60 1.00 -15 4 10 6.60 1.00 -15 4 10 5.70 0.90 -15 4 10 4.90 0.80 15 -4 10 4.20 1.00 -15 -4 -10 4.90 0.90 15 4 10 5.30 0.70 15 4 10 4.70 1.20 -15 4 -10 3.80 0.90 -15 4 -10 2.90 0.80 15 4 10 5.70 1.10 15 -4 -10 6.20 1.20 -15 4 -10 3.50 0.70 15 4 10 6.00 0.90 -15 -5 -10 78.09 3.50 -15 5 10 71.29 3.40 -15 5 10 75.59 3.20 15 5 -10 65.19 3.30 -15 5 10 70.79 3.20 15 -5 10 71.69 3.60 -15 5 10 70.29 3.30 -15 5 10 71.89 3.60 15 5 10 72.09 3.40 -15 5 -10 75.59 3.40 -15 5 -10 70.59 3.50 15 5 10 71.69 3.70 15 5 10 70.49 3.10 15 5 10 69.69 3.80 -15 5 -10 70.49 3.20 15 -5 -10 71.99 3.90 -15 6 10 55.79 2.80 -15 6 10 57.59 2.70 -15 6 10 59.19 3.00 15 -6 10 53.89 3.10 -15 6 10 55.29 3.10 -15 -6 -10 57.99 2.90 15 6 -10 53.19 2.80 15 6 10 54.29 2.50 -15 6 -10 49.50 2.70 -15 6 -10 55.09 2.70 15 6 10 54.09 2.80 15 6 10 47.90 3.10 15 6 10 52.69 3.40 15 -6 -10 56.39 3.40 -15 6 -10 49.60 2.90 -15 7 10 12.30 1.50 15 -7 10 12.30 1.60 -15 7 10 11.20 1.50 -15 -7 -10 8.80 1.20 -15 7 10 10.70 1.20 15 7 -10 7.50 1.30 -15 7 10 9.90 1.20 15 7 10 8.30 1.60 15 7 10 11.60 1.70 15 -7 -10 9.70 1.60 -15 7 -10 8.40 1.30 -15 7 -10 11.30 1.30 15 7 10 7.40 1.20 15 8 -10 46.80 2.80 -15 8 10 41.90 2.70 -15 8 10 44.00 3.00 -15 8 10 46.20 2.80 15 -8 10 47.80 3.10 -15 8 10 46.20 2.60 -15 8 -10 46.20 2.90 15 -8 -10 49.20 3.40 15 8 10 47.40 3.10 15 8 10 47.10 2.80 15 8 10 43.20 3.50 -15 8 -10 47.60 2.60 -15 9 10 0.80 0.80 -15 9 10 0.00 0.90 15 -9 10 1.30 1.00 15 9 -10 1.10 1.00 -15 9 10 1.50 1.20 -15 9 -10 1.90 0.90 15 9 10 1.80 1.00 -15 9 -10 1.70 0.80 -15 9 -10 2.30 1.10 15 -9 -10 1.00 1.10 15 9 10 -0.40 1.30 15 -10 10 0.70 1.00 -15 10 10 0.40 1.00 15 10 -10 0.10 1.00 -15 10 10 1.30 1.00 -15 10 10 1.10 1.20 -15 10 -10 0.80 0.90 15 10 10 2.00 1.00 -15 10 -10 2.00 1.20 15 -10 -10 0.70 1.30 -15 10 -10 0.40 0.70 15 10 10 1.10 1.50 -15 11 10 4.10 1.50 15 11 -10 3.00 1.30 15 -11 10 5.50 1.40 -15 11 10 3.50 1.30 -15 11 10 3.60 1.40 15 -11 -10 3.70 1.60 -15 11 -10 2.10 1.30 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1.60 -25 15 -1 0.10 1.40 -25 15 -1 2.10 1.30 -25 15 -1 -0.50 1.70 -25 15 -1 1.80 1.50 -25 16 1 7.40 2.30 -25 16 1 8.60 2.30 -25 16 1 8.60 2.10 -25 16 1 11.70 2.20 -25 16 -1 5.40 2.00 -25 16 -1 4.90 1.70 -25 16 -1 8.80 2.00 -25 16 -1 11.10 2.40 -25 0 2 101.99 4.40 25 0 2 103.39 4.50 -25 0 -2 106.89 4.50 25 0 -2 104.49 4.40 -25 -1 -2 1.30 0.50 25 1 -2 1.00 0.50 25 -1 2 1.10 0.70 -25 1 2 0.60 0.40 -25 1 2 0.40 0.30 -25 1 2 0.80 0.50 -25 -1 2 1.00 0.50 -25 1 -2 0.40 0.30 -25 1 -2 1.30 0.60 25 1 2 0.50 0.70 25 -1 -2 0.60 0.50 -25 2 2 55.89 2.50 -25 2 2 53.79 2.70 -25 2 2 57.89 2.50 -25 -2 -2 55.29 2.80 25 -2 2 55.79 3.00 -25 2 -2 52.19 2.60 -25 2 -2 49.99 2.70 -25 -2 2 55.39 2.70 -25 2 -2 56.49 2.50 25 -2 -2 57.19 2.90 -25 2 -2 57.29 2.50 25 2 2 72.79 3.00 25 3 -2 3.10 0.60 -25 3 2 3.20 0.70 -25 3 2 3.60 0.70 -25 3 2 4.70 0.70 -25 -3 -2 4.30 0.80 -25 3 2 3.20 0.70 25 -3 2 3.60 0.90 -25 3 -2 3.00 0.70 25 -3 -2 2.60 0.80 -25 -3 2 2.50 0.70 -25 3 -2 4.10 0.70 -25 3 -2 3.40 0.70 -25 3 -2 3.90 0.60 25 3 2 3.60 0.80 -25 4 2 34.70 1.90 25 4 -2 34.70 1.70 -25 -4 -2 31.50 1.90 25 -4 2 31.50 2.30 -25 4 2 31.20 1.80 25 4 -2 28.60 1.90 -25 4 2 29.40 1.80 -25 4 2 32.10 1.90 25 4 2 33.50 2.10 -25 4 -2 32.00 2.00 -25 4 -2 31.00 1.90 -25 4 -2 31.00 1.80 -25 -4 2 32.90 1.90 25 4 2 32.80 1.70 25 -4 -2 35.20 2.20 25 4 2 38.10 2.00 -25 4 -2 32.30 1.80 -25 5 2 37.50 2.20 -25 5 2 38.20 2.10 25 5 -2 40.00 2.20 25 -5 2 40.10 2.60 -25 5 2 39.30 2.00 -25 5 2 39.80 2.10 -25 5 2 38.40 2.30 -25 -5 -2 35.70 2.10 25 5 2 34.50 2.30 -25 5 -2 42.20 2.30 -25 5 -2 36.70 2.00 25 5 2 38.00 2.20 25 -5 -2 41.80 2.60 -25 -5 2 35.60 2.10 -25 5 -2 36.10 2.10 -25 5 -2 40.50 2.10 -25 6 2 48.00 2.60 -25 6 2 47.60 2.60 25 6 -2 45.90 2.70 -25 6 2 43.70 2.40 -25 -6 -2 43.90 2.40 -25 6 2 46.50 2.70 -25 6 2 47.40 2.50 25 -6 2 44.30 2.90 -25 -6 2 48.10 2.50 25 6 2 44.60 2.80 -25 6 -2 48.70 2.50 -25 6 -2 48.20 2.40 -25 6 -2 48.40 2.50 25 -6 -2 45.20 2.90 -25 6 -2 48.40 2.80 25 6 2 46.20 2.60 -25 7 2 3.10 0.90 -25 7 2 3.90 0.90 -25 7 2 5.00 1.10 -25 7 2 4.80 1.00 25 -7 2 2.80 1.10 -25 -7 -2 4.10 0.80 -25 7 -2 3.10 1.00 -25 7 -2 4.40 1.00 25 7 2 5.10 1.00 -25 -7 2 4.20 0.80 -25 7 -2 4.40 0.90 -25 7 -2 3.40 0.80 25 7 2 2.40 1.20 25 -7 -2 5.10 1.20 25 -8 2 0.80 0.90 -25 8 2 3.00 1.10 -25 8 2 2.10 0.90 -25 8 2 3.80 0.90 -25 8 2 2.50 1.10 25 8 -2 0.80 1.10 -25 8 -2 4.30 1.00 25 -8 -2 1.90 1.10 25 8 2 0.90 1.30 -25 8 -2 1.40 0.80 -25 8 -2 1.50 1.00 -25 8 -2 2.60 0.90 -25 9 2 42.80 3.00 -25 9 2 45.50 2.80 25 -9 2 41.50 3.10 -25 9 2 41.70 2.60 -25 9 2 43.00 2.90 25 9 2 43.80 3.40 25 -9 -2 44.00 3.30 -25 9 -2 45.20 2.80 -25 9 -2 43.30 2.90 -25 9 -2 42.70 2.90 -25 9 -2 40.40 2.60 -25 10 2 16.90 2.00 -25 10 2 19.20 2.20 -25 10 2 24.90 2.30 -25 10 2 25.80 2.30 25 -10 2 18.70 2.30 25 10 -2 16.20 1.90 25 -10 -2 18.80 2.40 -25 10 -2 23.40 2.30 -25 10 -2 21.00 2.10 -25 10 -2 22.50 2.40 -25 10 -2 19.00 1.90 25 10 2 20.70 2.60 -25 11 2 18.20 2.30 -25 11 2 26.50 2.50 25 11 -2 24.50 2.20 -25 11 2 23.50 2.40 25 -11 2 19.30 2.70 -25 11 2 26.30 2.40 -25 11 -2 24.80 2.40 25 11 2 26.70 2.90 25 -11 -2 23.70 2.80 -25 11 -2 31.00 2.60 -25 11 -2 21.70 2.50 -25 11 -2 24.90 2.40 25 -12 2 5.30 1.70 -25 12 2 5.90 1.30 -25 12 2 3.10 1.30 25 12 -2 5.40 1.40 -25 12 2 4.90 1.40 -25 12 2 3.90 1.40 -25 12 -2 5.40 1.40 25 -12 -2 7.00 1.80 -25 12 -2 3.80 1.30 -25 12 -2 5.80 1.40 25 12 2 4.90 1.80 -25 12 -2 2.40 1.60 -25 13 2 5.30 1.50 -25 13 2 5.50 1.50 25 -13 2 4.30 1.80 -25 13 2 5.70 1.70 -25 13 2 4.90 1.70 25 13 -2 2.90 1.40 -25 13 -2 3.70 1.50 -25 13 -2 5.60 1.90 25 -13 -2 10.30 2.30 -25 13 -2 5.90 1.40 -25 13 -2 4.50 1.70 -25 14 2 0.60 1.30 -25 14 2 0.20 1.50 -25 14 2 2.70 1.70 -25 14 2 0.00 1.30 25 14 -2 0.30 1.10 -25 14 -2 -0.80 1.00 -25 14 -2 -1.10 1.10 -25 14 -2 -0.40 1.00 -25 14 -2 -2.20 1.10 -25 15 2 2.20 1.50 -25 15 2 0.40 1.70 25 15 -2 2.70 1.60 -25 15 2 -0.10 1.50 -25 15 2 1.40 1.40 -25 15 -2 0.80 1.40 -25 15 -2 0.50 1.60 -25 15 -2 2.00 1.90 -25 15 -2 1.50 1.20 -25 16 2 2.00 1.70 -25 16 2 -0.60 1.30 -25 16 2 0.90 2.00 -25 16 2 2.70 2.10 -25 16 -2 3.90 2.30 -25 16 -2 4.10 1.70 -25 16 -2 3.30 1.70 -25 16 -2 2.40 1.90 25 0 -3 -0.20 0.50 -25 0 -3 -0.20 0.40 -25 0 3 0.10 0.50 -25 0 3 0.10 0.30 -25 1 3 4.00 0.60 -25 -1 -3 3.70 0.70 -25 1 3 3.80 0.70 25 -1 3 3.30 0.80 25 1 -3 2.70 0.60 -25 1 3 2.80 0.50 25 -1 -3 3.70 0.80 25 1 3 5.30 1.00 -25 1 -3 2.80 0.70 -25 -1 3 4.60 0.80 -25 1 -3 3.10 0.50 -25 2 3 102.19 4.00 -25 -2 -3 98.29 4.30 25 -2 3 99.89 4.50 -25 2 3 93.69 4.20 25 2 -3 101.09 4.00 -25 2 3 101.69 4.00 -25 2 -3 99.89 4.30 -25 2 -3 97.79 4.20 25 2 3 91.19 4.30 -25 2 -3 99.39 3.90 25 -2 -3 94.89 4.40 -25 -2 3 99.69 4.30 25 -3 3 11.60 1.40 -25 -3 -3 14.20 1.30 -25 3 3 12.90 1.00 -25 3 3 11.10 1.10 -25 3 3 14.30 1.10 25 3 -3 13.20 1.00 -25 -3 3 12.30 1.20 -25 3 -3 13.80 1.30 -25 3 -3 11.10 1.20 25 3 3 14.40 1.40 -25 3 -3 12.00 1.00 25 -3 -3 14.20 1.50 -25 3 -3 10.90 1.00 -25 4 3 82.59 3.60 -25 -4 -3 82.29 3.70 25 4 -3 84.09 3.40 -25 4 3 85.39 3.60 -25 4 3 87.09 3.80 -25 4 3 80.49 3.60 25 4 -3 75.19 3.60 25 -4 3 85.49 4.10 -25 4 3 87.89 3.80 -25 4 -3 77.49 3.80 25 4 3 80.09 3.90 25 -4 -3 81.59 4.00 25 4 3 82.79 3.40 -25 -4 3 79.99 3.70 25 4 3 83.59 3.80 -25 4 -3 85.49 3.60 -25 4 -3 82.79 3.60 -25 4 -3 79.89 3.70 -25 5 3 3.10 0.70 -25 5 3 3.50 0.90 -25 5 3 2.10 0.70 25 5 -3 0.70 0.70 -25 5 3 1.80 0.70 -25 5 3 2.10 0.70 -25 -5 -3 2.90 0.70 25 -5 3 3.40 1.00 25 5 3 3.00 0.80 -25 5 -3 3.00 0.90 25 5 3 -0.20 1.00 25 -5 -3 3.20 0.90 25 5 3 1.50 0.50 -25 5 -3 3.80 0.70 -25 5 -3 2.50 0.60 -25 5 -3 2.40 0.70 -25 -5 3 2.60 0.70 25 6 -3 44.80 2.60 25 -6 3 42.70 2.80 -25 6 3 41.30 2.60 -25 -6 -3 43.40 2.40 -25 6 3 45.30 2.50 -25 6 3 44.60 2.40 -25 6 3 46.70 2.60 -25 6 3 41.70 2.40 25 -6 -3 46.70 2.90 -25 6 -3 47.20 2.50 25 6 3 48.60 2.70 -25 6 -3 43.70 2.70 -25 6 -3 46.60 2.40 25 6 3 41.60 2.90 -25 -6 3 45.90 2.40 -25 6 -3 41.30 2.30 25 -7 3 16.90 2.00 -25 7 3 19.00 1.90 -25 7 3 20.20 1.70 25 7 -3 25.80 2.20 -25 -7 -3 19.70 1.50 -25 7 3 18.20 1.80 -25 7 3 16.60 1.60 25 7 3 19.10 2.20 25 -7 -3 18.10 2.10 25 7 3 20.50 1.70 -25 7 -3 20.50 2.00 -25 -7 3 19.40 1.50 -25 7 -3 18.40 1.60 -25 7 -3 17.10 1.60 25 -8 3 17.70 2.10 -25 8 3 21.10 1.90 -25 8 3 24.50 2.20 -25 8 3 16.00 1.80 -25 8 3 21.40 1.90 25 -8 -3 21.40 2.40 25 8 3 18.70 2.40 -25 8 -3 21.40 1.90 -25 8 -3 21.50 2.10 -25 8 -3 21.40 1.90 25 -9 3 6.70 1.40 -25 9 3 4.70 1.10 -25 9 3 2.90 1.30 -25 9 3 4.70 1.20 -25 9 3 4.40 1.20 25 9 3 4.10 1.70 -25 9 -3 6.90 1.30 25 -9 -3 1.10 1.20 -25 9 -3 5.40 1.10 -25 9 -3 4.50 1.40 -25 9 -3 5.10 1.20 25 10 -3 30.80 2.30 -25 10 3 39.60 2.60 -25 10 3 32.40 2.70 -25 10 3 31.50 2.60 25 -10 3 37.00 3.10 -25 10 3 31.10 2.80 25 10 3 32.40 3.20 -25 10 -3 31.30 2.30 -25 10 -3 28.00 2.90 -25 10 -3 33.70 2.50 25 -10 -3 39.20 3.20 -25 10 -3 38.90 2.80 -25 11 3 10.10 1.60 25 11 -3 5.40 1.30 -25 11 3 5.60 1.60 25 -11 3 5.70 1.60 -25 11 3 7.40 1.50 -25 11 3 5.30 1.50 -25 11 -3 4.90 1.50 -25 11 -3 4.80 1.50 -25 11 -3 6.00 1.30 25 11 3 6.40 1.90 -25 11 -3 5.40 1.20 25 -11 -3 4.20 1.70 25 12 -3 3.30 1.30 -25 12 3 5.10 1.70 -25 12 3 5.70 1.60 25 -12 3 4.20 1.50 -25 12 3 4.40 1.60 -25 12 3 4.10 1.30 -25 12 -3 5.40 1.60 -25 12 -3 4.30 1.40 -25 12 -3 4.10 1.30 -25 12 -3 4.60 1.50 25 -12 -3 4.70 1.90 25 12 3 5.90 2.00 25 -13 3 0.80 1.40 -25 13 3 3.10 1.40 -25 13 3 0.40 1.20 25 13 -3 1.00 1.20 -25 13 3 4.20 1.70 -25 13 3 0.90 1.40 25 -13 -3 2.00 2.80 -25 13 -3 0.50 1.20 25 13 3 2.60 1.90 -25 13 -3 1.80 1.30 -25 13 -3 3.10 1.40 -25 13 -3 1.40 1.60 -25 14 3 1.30 1.60 -25 14 3 1.00 1.30 -25 14 3 1.10 1.30 25 14 -3 0.30 1.40 -25 14 3 1.00 1.80 -25 14 -3 1.00 1.50 -25 14 -3 1.30 1.40 -25 14 -3 1.20 1.10 -25 14 -3 0.90 1.30 -25 15 3 0.60 1.30 -25 15 3 1.20 1.70 -25 15 3 2.00 1.30 -25 15 3 1.70 1.80 25 15 -3 -0.10 1.20 -25 15 -3 2.00 1.70 -25 15 -3 0.10 1.10 -25 15 -3 -0.20 1.20 -25 15 -3 -1.10 1.70 -25 16 3 2.10 2.00 -25 16 3 0.10 1.90 -25 16 3 2.60 1.50 -25 16 3 2.10 1.70 25 16 -3 2.30 1.70 -25 16 -3 -0.40 1.40 -25 16 -3 2.30 1.60 -25 16 -3 4.50 2.20 -25 16 -3 0.30 1.60 -25 0 4 172.18 6.30 25 0 -4 165.48 6.60 -25 0 -4 162.98 6.70 -25 0 4 166.38 6.70 -25 1 4 7.10 0.90 -25 1 4 3.90 0.60 25 -1 4 3.40 1.00 25 1 -4 4.30 0.70 -25 1 4 4.90 0.60 -25 -1 -4 5.30 0.90 -25 -1 4 5.10 0.60 -25 -1 4 4.10 0.70 -25 1 -4 2.80 0.70 25 -1 -4 5.50 0.90 -25 1 -4 3.70 0.60 -25 1 -4 4.20 0.50 -25 2 4 6.20 0.80 -25 2 4 8.30 0.80 25 -2 4 8.60 1.20 25 2 -4 7.90 0.80 -25 2 4 9.80 0.90 -25 -2 -4 5.20 0.90 -25 -2 4 4.60 0.80 25 2 4 4.60 0.90 -25 2 -4 6.20 0.90 25 -2 -4 7.80 1.10 -25 2 -4 5.20 0.80 -25 2 -4 7.00 0.70 -25 3 4 4.00 0.70 -25 3 4 3.90 0.70 -25 -3 -4 3.60 0.80 25 -3 4 4.10 0.90 -25 3 4 2.70 0.70 25 3 -4 3.80 0.60 -25 3 -4 2.90 0.60 -25 3 -4 3.40 0.70 -25 -3 4 3.20 0.70 -25 3 -4 2.50 0.70 -25 3 -4 2.40 0.50 25 3 4 3.10 0.80 25 -3 -4 4.60 1.00 25 -4 4 13.50 1.60 -25 4 4 15.80 1.20 -25 4 4 15.00 1.30 -25 4 4 14.50 1.40 -25 4 4 12.60 1.20 25 4 -4 12.40 1.20 -25 -4 -4 13.30 1.30 -25 4 4 16.90 1.40 -25 4 -4 16.30 1.30 25 4 4 13.80 1.00 25 4 4 13.80 1.40 25 -4 -4 17.70 1.80 -25 4 -4 15.20 1.30 -25 4 -4 15.90 1.20 25 4 4 13.50 1.50 -25 4 -4 14.60 1.50 -25 -4 4 14.50 1.30 -25 5 4 1.30 0.60 -25 5 4 0.40 0.60 25 5 -4 1.20 0.60 -25 -5 -4 0.90 0.60 -25 5 4 2.20 0.80 -25 5 4 0.80 0.60 25 -5 4 0.70 0.80 -25 5 4 1.00 0.50 25 -5 -4 0.10 0.80 -25 5 -4 1.60 0.70 -25 5 -4 1.10 0.60 25 5 4 0.90 0.70 25 5 4 1.60 0.50 25 5 4 0.20 0.80 -25 5 -4 0.60 0.50 -25 5 -4 -0.70 0.60 -25 -5 4 1.00 0.60 -25 6 4 23.70 1.70 -25 6 4 20.90 1.60 -25 -6 -4 24.20 1.60 25 -6 4 20.30 2.10 -25 6 4 25.20 2.10 25 6 -4 23.50 2.10 -25 6 4 18.20 1.80 -25 6 4 24.10 1.70 25 -6 -4 18.70 2.00 -25 -6 4 19.50 1.60 -25 6 -4 23.00 2.00 25 6 4 24.50 1.90 -25 6 -4 20.70 1.60 -25 6 -4 22.00 1.60 25 6 4 24.70 2.30 -25 6 -4 23.00 1.60 -25 7 4 42.90 2.70 25 -7 4 48.80 3.00 -25 7 4 41.20 2.60 -25 -7 -4 46.90 2.50 -25 7 4 42.00 2.70 -25 7 4 42.00 2.50 -25 -7 4 53.09 2.60 25 7 4 47.50 2.80 -25 7 -4 42.30 2.80 25 -7 -4 51.29 3.20 25 7 4 42.00 3.00 -25 7 -4 43.50 2.50 -25 7 -4 43.40 2.50 -25 8 4 18.30 2.00 -25 8 4 22.90 2.00 -25 8 4 26.00 1.90 -25 8 4 20.10 2.00 25 -8 4 21.20 2.40 -25 8 -4 22.30 1.70 -25 8 -4 20.70 1.80 25 8 4 25.40 2.70 25 -8 -4 19.60 2.40 -25 8 -4 22.50 2.20 25 8 4 20.00 2.00 -25 9 4 7.80 1.40 -25 9 4 9.80 1.50 25 -9 4 8.50 1.60 -25 9 4 10.00 1.40 -25 9 4 9.80 1.40 -25 9 -4 10.00 1.40 25 -9 -4 8.80 1.70 -25 9 -4 9.40 1.40 25 9 4 6.30 2.10 -25 9 -4 14.30 1.90 -25 10 4 13.30 1.80 25 -10 4 10.60 1.90 -25 10 4 14.10 1.90 -25 10 4 14.00 2.00 -25 10 4 12.90 1.80 25 10 -4 12.10 1.70 -25 10 -4 14.30 1.80 25 10 4 12.90 2.30 -25 10 -4 11.30 1.90 -25 10 -4 14.00 1.70 -25 10 -4 13.90 1.70 25 -10 -4 16.90 2.30 -25 11 4 30.90 2.80 25 -11 4 35.40 3.40 25 11 -4 25.20 2.40 -25 11 4 29.00 2.80 -25 11 4 36.80 2.70 -25 11 4 33.30 2.80 -25 11 -4 32.00 2.60 -25 11 -4 24.80 2.70 25 11 4 31.80 3.50 25 -11 -4 33.60 3.40 -25 11 -4 31.30 2.30 -25 11 -4 37.20 2.60 -25 12 4 16.30 2.20 -25 12 4 17.70 2.40 25 -12 4 12.50 2.20 -25 12 4 16.10 2.10 25 12 -4 21.40 2.30 -25 12 4 19.80 2.50 -25 12 -4 14.20 2.30 -25 12 -4 12.70 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30.50 1.90 -30 5 -3 33.60 2.20 30 -5 -3 31.50 2.40 -30 -5 3 27.10 2.00 30 5 3 32.10 2.20 -30 5 -3 29.10 2.00 30 5 3 28.80 2.30 -30 5 -3 32.20 1.90 -30 6 3 4.80 1.10 -30 6 3 3.70 1.00 30 -6 3 3.40 1.10 -30 6 3 4.80 1.00 -30 6 3 4.10 0.90 30 6 -3 3.80 1.00 -30 -6 -3 5.10 0.90 -30 6 3 6.20 1.00 30 6 3 5.30 1.10 -30 6 -3 4.90 0.90 -30 6 -3 4.30 0.90 30 -6 -3 5.20 1.20 -30 -6 3 5.00 1.00 30 6 3 3.10 1.30 -30 6 -3 5.20 1.20 -30 6 -3 5.10 1.00 -30 -7 -3 1.30 0.80 -30 7 3 1.50 0.90 -30 7 3 0.20 0.90 30 -7 3 0.20 0.90 -30 7 3 1.00 0.80 -30 7 3 0.70 0.70 -30 7 -3 0.10 0.70 30 7 3 -0.20 1.10 -30 7 -3 0.90 0.80 30 -7 -3 1.10 1.20 -30 7 -3 -0.60 0.80 -30 -7 3 1.30 0.80 -30 8 3 3.60 1.10 -30 8 3 0.00 0.70 -30 8 3 -1.10 0.70 -30 8 3 -0.70 0.70 30 -8 3 2.50 1.30 -30 8 -3 0.60 0.80 -30 8 -3 0.90 0.80 -30 8 -3 -0.20 1.00 30 8 3 2.30 1.60 30 -8 -3 1.60 1.20 -30 9 3 28.30 2.50 30 -9 3 25.90 2.70 -30 9 3 32.50 2.80 -30 9 3 34.80 2.50 -30 9 3 34.00 2.50 30 -9 -3 28.60 2.90 -30 9 -3 31.80 2.20 -30 9 -3 36.70 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0.00 59 0 14 -2.09 0.00 58 2 14 -0.54 0.00 57 4 14 0.01 0.00 54 6 14 -0.16 0.00 48 9 14 -0.35 0.00 45 10 14 -1.29 0.00 37 12 14 -2.71 0.00 32 13 14 0.84 0.00 25 14 14 -2.89 0.00 26 14 14 -0.92 0.00 15 15 14 0.20 0.00 16 15 14 -0.89 0.00 57 2 15 -2.52 0.00 53 6 15 -0.05 0.00 51 7 15 2.05 0.00 49 8 15 -0.03 0.00 43 10 15 1.25 0.00 40 11 15 -0.45 0.00 35 12 15 -1.32 0.00 30 13 15 0.16 0.00 22 14 15 0.64 0.00 23 14 15 1.70 0.00 9 15 15 0.24 0.00 10 15 15 -0.29 0.00 11 15 15 0.36 0.00 56 0 16 -1.18 0.00 56 1 16 1.32 0.00 56 2 16 -0.51 0.00 55 3 16 -1.29 0.00 54 4 16 2.57 0.00 53 5 16 -3.43 0.00 45 9 16 0.60 0.00 42 10 16 -1.40 0.00 38 11 16 2.53 0.00 33 12 16 -1.26 0.00 27 13 16 -0.60 0.00 19 14 16 -0.59 0.00 15 1 17 4.39 0.00 54 2 17 -0.58 0.00 30 3 17 0.45 0.00 50 6 17 1.35 0.00 48 7 17 -1.13 0.00 46 8 17 -0.65 0.00 43 9 17 0.66 0.00 40 10 17 1.23 0.00 36 11 17 0.23 0.00 31 12 17 0.01 0.00 24 13 17 -1.51 0.00 13 14 17 0.87 0.00 14 14 17 0.35 0.00 15 14 17 0.13 0.00 53 0 18 1.03 0.00 53 1 18 0.63 0.00 52 3 18 1.32 0.00 51 4 18 -0.65 0.00 50 5 18 0.46 0.00 48 6 18 0.58 0.00 46 7 18 0.47 0.00 44 8 18 0.85 0.00 41 9 18 -0.27 0.00 37 10 18 -0.71 0.00 33 11 18 1.30 0.00 28 12 18 0.71 0.00 20 13 18 -1.72 0.00 21 13 18 -0.40 0.00 0 14 18 2.14 0.00 1 14 18 0.31 0.00 2 14 18 2.00 0.00 3 14 18 0.34 0.00 4 14 18 3.00 0.00 5 14 18 1.10 0.00 6 14 18 2.48 0.00 7 14 18 1.02 0.00 8 14 18 1.84 0.00 51 2 19 1.66 0.00 50 3 19 0.27 0.00 49 4 19 -1.33 0.00 48 5 19 -0.35 0.00 46 6 19 1.26 0.00 44 7 19 -0.12 0.00 42 8 19 -1.13 0.00 39 9 19 1.12 0.00 35 10 19 0.26 0.00 30 11 19 0.44 0.00 24 12 19 0.88 0.00 25 12 19 0.61 0.00 15 13 19 -1.75 0.00 16 13 19 -0.66 0.00 49 2 20 -3.53 0.00 47 4 20 1.09 0.00 46 5 20 -0.34 0.00 44 6 20 -0.01 0.00 42 7 20 -0.28 0.00 39 8 20 0.36 0.00 36 9 20 -1.86 0.00 32 10 20 -0.49 0.00 27 11 20 -0.67 0.00 20 12 20 -0.61 0.00 21 12 20 0.84 0.00 5 13 20 1.34 0.00 6 13 20 1.82 0.00 7 13 20 1.50 0.00 8 13 20 1.04 0.00 9 13 20 0.98 0.00 47 2 21 0.04 0.00 46 3 21 1.24 0.00 45 4 21 -0.42 0.00 44 5 21 1.25 0.00 42 6 21 0.09 0.00 40 7 21 0.01 0.00 37 8 21 -1.28 0.00 33 9 21 -0.89 0.00 29 10 21 -0.33 0.00 23 11 21 -0.60 0.00 14 12 21 0.72 0.00 15 12 21 -0.55 0.00 45 1 22 -0.88 0.00 45 2 22 0.24 0.00 44 3 22 -0.22 0.00 43 4 22 -1.72 0.00 41 5 22 -0.02 0.00 39 6 22 -0.06 0.00 37 7 22 0.85 0.00 34 8 22 0.07 0.00 30 9 22 -1.97 0.00 25 10 22 -1.32 0.00 18 11 22 0.67 0.00 19 11 22 -0.32 0.00 0 12 22 0.31 0.00 1 12 22 0.31 0.00 2 12 22 0.23 0.00 3 12 22 -0.61 0.00 4 12 22 -0.38 0.00 5 12 22 -0.10 0.00 6 12 22 -0.62 0.00 43 1 23 0.50 0.00 42 2 23 1.61 0.00 41 3 23 -0.52 0.00 40 4 23 -1.39 0.00 36 6 23 -2.33 0.00 34 7 23 0.74 0.00 30 8 23 -1.25 0.00 31 8 23 -1.85 0.00 26 9 23 0.97 0.00 20 10 23 1.77 0.00 21 10 23 -0.57 0.00 10 11 23 -0.37 0.00 11 11 23 -1.42 0.00 12 11 23 -0.50 0.00 40 0 24 0.20 0.00 40 1 24 0.75 0.00 37 4 24 -1.41 0.00 35 5 24 -1.53 0.00 33 6 24 1.07 0.00 30 7 24 -0.64 0.00 26 8 24 -1.26 0.00 27 8 24 -0.26 0.00 21 9 24 0.36 0.00 22 9 24 -1.08 0.00 13 10 24 3.01 0.00 14 10 24 0.95 0.00 37 1 25 0.88 0.00 36 2 25 -1.44 0.00 35 3 25 1.41 0.00 34 4 25 -0.39 0.00 32 5 25 -0.89 0.00 29 6 25 -1.68 0.00 26 7 25 0.90 0.00 21 8 25 -2.24 0.00 22 8 25 -0.16 0.00 14 9 25 0.31 0.00 15 9 25 -1.07 0.00 34 0 26 -0.15 0.00 33 1 26 1.41 0.00 33 2 26 0.28 0.00 32 3 26 1.01 0.00 30 4 26 -0.59 0.00 28 5 26 3.32 0.00 25 6 26 -2.86 0.00 20 7 26 -0.75 0.00 21 7 26 -0.77 0.00 14 8 26 1.90 0.00 15 8 26 0.58 0.00 1 9 26 -0.14 0.00 2 9 26 -0.33 0.00 29 1 27 1.30 0.00 29 2 27 1.40 0.00 27 3 27 0.24 0.00 25 4 27 -0.53 0.00 26 4 27 0.35 0.00 23 5 27 -2.11 0.00 19 6 27 -0.70 0.00 12 7 27 -2.18 0.00 13 7 27 -0.00 0.00 14 7 27 -1.89 0.00 25 0 28 1.02 0.00 24 1 28 -1.34 0.00 25 1 28 0.70 0.00 23 2 28 -0.04 0.00 24 2 28 -0.91 0.00 22 3 28 1.65 0.00 19 4 28 -0.64 0.00 20 4 28 0.10 0.00 15 5 28 -1.00 0.00 16 5 28 -1.38 0.00 8 6 28 -0.53 0.00 9 6 28 1.88 0.00 10 6 28 0.09 0.00 11 6 28 0.55 0.00 17 1 29 -0.17 0.00 18 1 29 -0.38 0.00 16 2 29 0.94 0.00 17 2 29 -0.36 0.00 14 3 29 -1.53 0.00 15 3 29 -1.07 0.00 9 4 29 1.96 0.00 10 4 29 0.91 0.00 11 4 29 0.88 0.00 1 5 29 1.22 0.00 2 5 29 -0.37 0.00 3 5 29 0.36 0.00 4 0 30 -0.08 0.00 5 0 30 -0.26 0.00 6 0 30 0.17 0.00 7 0 30 0.90 0.00 8 0 30 -0.29 0.00 1 1 30 -0.30 0.00 2 1 30 0.33 0.00 3 1 30 -0.45 0.00 4 1 30 0.05 0.00 5 1 30 -0.19 0.00 6 1 30 -0.67 0.00 7 1 30 -0.52 0.00 8 1 30 -1.35 0.00 0 2 30 0.68 0.00 1 2 30 0.27 0.00 2 2 30 0.38 0.00 3 2 30 0.37 0.00 4 2 30 0.80 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 30118) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.249 0.053 0.220 31 3 ' ' 2 0.249 -0.054 0.720 31 3 ' ' 3 0.500 -0.000 0.221 1380 478 ' ' 4 0.751 0.053 0.280 31 3 ' ' 5 0.750 -0.054 0.780 31 3 ' ' 6 -0.000 0.500 0.753 1380 478 ' ' 7 0.250 0.446 0.720 31 3 ' ' 8 0.749 0.446 0.780 31 3 ' ' 9 0.250 0.553 0.220 31 3 ' ' 10 0.749 0.553 0.280 31 3 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 11 2 6 7.776 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL x_dummy P b c n R = 0.07 CELL 49.2850 13.0502 22.4161 90.00 90.00 90.00 SPGR Pbcn # Solvent Accessible Volume = 3058 # Electrons Found in S.A.V. = 981 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.966 0.308 0.473 ! 2.68 eA-3 C102 0.949 0.390 0.315 ! 2.54 eA-3 C103 0.453 0.858 0.232 ! 2.44 eA-3 C104 0.041 0.311 0.138 ! 2.43 eA-3 C105 0.984 0.700 0.084 ! 2.36 eA-3 C106 0.464 0.855 0.069 ! 2.33 eA-3 C107 1.000 0.656 0.250 ! 2.33 eA-3 C108 0.991 0.360 0.638 ! 2.25 eA-3 C109 0.551 0.856 0.374 ! 2.15 eA-3 C110 0.499 0.206 0.303 ! 2.06 eA-3 C111 0.025 0.312 0.952 ! 2.06 eA-3 C112 0.975 0.688 0.048 ! 2.06 eA-3 C113 0.558 0.078 0.727 ! 1.88 eA-3 C114 0.438 0.885 0.238 ! 1.81 eA-3 C115 0.049 0.418 0.332 ! 1.26 eA-3 C116 0.515 0.074 0.143 ! 1.21 eA-3 Q117 0.497 0.480 0.422 ! 0.96 eA-3 C118 0.438 0.858 0.045 ! 0.96 eA-3 C119 0.480 0.929 0.897 ! 0.89 eA-3 C120 0.020 0.516 0.391 ! 0.85 eA-3 Q121 0.987 0.994 0.185 ! 0.79 eA-3 C122 0.496 0.051 0.206 ! 0.79 eA-3 C123 0.972 0.499 0.192 ! 0.78 eA-3 C124 0.015 0.564 0.301 ! 0.78 eA-3 Q125 0.992 0.928 0.571 ! 0.76 eA-3 Q126 0.981 0.064 0.191 ! 0.76 eA-3 Q127 0.002 0.996 0.868 ! 0.76 eA-3 Q128 0.036 0.125 0.319 ! 0.74 eA-3 C129 0.969 0.408 0.194 ! 0.71 eA-3 C130 0.966 0.533 0.105 ! 0.69 eA-3 C131 0.486 0.017 0.252 ! 0.69 eA-3 C132 0.483 0.110 0.194 ! 0.66 eA-3 C133 0.515 0.885 0.445 ! 0.66 eA-3 C134 0.523 0.996 0.292 ! 0.65 eA-3 C135 0.487 0.894 0.126 ! 0.64 eA-3 C136 0.004 0.582 0.472 ! 0.62 eA-3 C137 0.967 0.452 0.271 ! 0.62 eA-3 Q138 0.531 0.263 0.092 ! 0.62 eA-3 C139 0.999 0.579 0.805 ! 0.62 eA-3 C140 0.987 0.635 0.355 ! 0.61 eA-3 C141 0.518 0.887 0.228 ! 0.60 eA-3 C142 0.487 0.033 0.166 ! 0.59 eA-3 C143 0.468 0.020 0.256 ! 0.58 eA-3 C144 0.487 0.998 0.290 ! 0.57 eA-3 C145 0.513 0.999 0.040 ! 0.57 eA-3 C146 0.488 0.067 0.671 ! 0.57 eA-3 C147 0.026 0.559 0.267 ! 0.56 eA-3 C148 0.494 0.979 0.918 ! 0.55 eA-3 C149 0.507 0.941 0.232 ! 0.54 eA-3 C150 0.985 0.547 0.380 ! 0.54 eA-3 Q151 0.443 0.222 0.474 ! 0.53 eA-3 C152 0.009 0.361 0.096 ! 0.53 eA-3 C153 0.017 0.315 0.218 ! 0.53 eA-3 C154 0.488 0.936 0.239 ! 0.53 eA-3 C155 0.999 0.517 0.773 ! 0.52 eA-3 C156 0.552 0.018 0.230 ! 0.51 eA-3 C157 0.518 0.279 0.215 ! 0.50 eA-3 ) ; _shelx_fab_checksum 24323 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_rom219_sq _database_code_depnum_ccdc_archive 'CCDC 2122220' loop_ _audit_author_name _audit_author_address 'Sophia Lipstman' ;Tel Aviv University Israel ; _audit_update_record ; 2021-11-25 deposited with the CCDC. 2022-04-27 downloaded from the CCDC. ; _audit_creation_method SHELXL-2018/1 _shelx_SHELXL_version_number 2018/1 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C136 H176 K4 N8 O12 P4, C6 H14' _chemical_formula_sum 'C142 H190 K4 N8 O12 P4' _chemical_formula_weight 2481.29 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 17.4664(8) _cell_length_b 33.4388(14) _cell_length_c 26.6896(12) _cell_angle_alpha 90 _cell_angle_beta 97.2220(10) _cell_angle_gamma 90 _cell_volume 15464.5(12) _cell_formula_units_Z 4 _cell_measurement_temperature 110(2) _cell_measurement_reflns_used 211335 _cell_measurement_theta_min 1.440 _cell_measurement_theta_max 25.744 _exptl_crystal_description rod _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.066 _exptl_crystal_F_000 5320 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.496 _exptl_crystal_size_mid 0.149 _exptl_crystal_size_min 0.136 _exptl_absorpt_coefficient_mu 0.211 _shelx_estimated_absorpt_T_min 0.903 _shelx_estimated_absorpt_T_max 0.972 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.963 _exptl_absorpt_correction_T_max 0.972 _exptl_absorpt_process_details 'Sadabs, Bruker-AXS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 110(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'ImuS micro-focus' _diffrn_measurement_device_type 'ApexDuo, Bruker-AXS' _diffrn_measurement_method '0.5 deg. \f and \w scans' _diffrn_detector_area_resol_mean 1.75 _diffrn_reflns_number 211335 _diffrn_reflns_av_unetI/netI 0.0580 _diffrn_reflns_av_R_equivalents 0.0821 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_k_min -40 _diffrn_reflns_limit_k_max 40 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_theta_min 1.440 _diffrn_reflns_theta_max 25.744 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 29478 _reflns_number_gt 20079 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. The structure contains additional 2 molecules of disordered n-hexane solvent, which could not be modelled by discrete atoms. Their contribution was subtracted from the diffraction pattern by the Squeeze technique, using the PLATON software (Spek, 2009). One of the t-butyl fragments also reveals partial disorder. ; _computing_data_collection 'Apex3, Bruker-AXS' _computing_cell_refinement 'Saint, Bruker-AXS' _computing_data_reduction 'Saint, Bruker-AXS' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0647P)^2^+12.6487P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 29478 _refine_ls_number_parameters 1595 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0888 _refine_ls_R_factor_gt 0.0530 _refine_ls_wR_factor_ref 0.1507 _refine_ls_wR_factor_gt 0.1294 _refine_ls_goodness_of_fit_ref 1.018 _refine_ls_restrained_S_all 1.018 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 0.61115(4) 0.60170(2) 0.80239(3) 0.02688(16) Uani 1 1 d . . . . . O2 O 0.58951(10) 0.55562(5) 0.78290(7) 0.0283(4) Uani 1 1 d . . . . . C3 C 0.51161(15) 0.54658(8) 0.77553(10) 0.0274(6) Uani 1 1 d . . . . . C4 C 0.48210(16) 0.51122(8) 0.75384(10) 0.0282(6) Uani 1 1 d . . . . . C5 C 0.40171(16) 0.50679(8) 0.75176(10) 0.0324(7) Uani 1 1 d . . . . . H5 H 0.378804 0.483036 0.737207 0.039 Uiso 1 1 calc R U . . . C7 C 0.38692(16) 0.57013(9) 0.79142(11) 0.0358(7) Uani 1 1 d . . . . . H7 H 0.355481 0.589977 0.804079 0.043 Uiso 1 1 calc R U . . . C6 C 0.35389(17) 0.53514(9) 0.76975(11) 0.0361(7) Uani 1 1 d . . . . . C8 C 0.46596(16) 0.57560(8) 0.79427(10) 0.0294(6) Uani 1 1 d . . . . . C9 C 0.53412(17) 0.47906(8) 0.73531(11) 0.0328(7) Uani 1 1 d . . . . . C10 C 0.58300(19) 0.49671(9) 0.69703(11) 0.0409(7) Uani 1 1 d . . . . . H10A H 0.614662 0.475587 0.684634 0.061 Uiso 1 1 calc R U . . . H10B H 0.616593 0.517674 0.713310 0.061 Uiso 1 1 calc R U . . . H10C H 0.549041 0.508183 0.668632 0.061 Uiso 1 1 calc R U . . . C11 C 0.48745(19) 0.44434(9) 0.70985(13) 0.0456(8) Uani 1 1 d . . . . . H11A H 0.452688 0.454377 0.680900 0.068 Uiso 1 1 calc R U . . . H11B H 0.457081 0.431840 0.734081 0.068 Uiso 1 1 calc R U . . . H11C H 0.522638 0.424528 0.698245 0.068 Uiso 1 1 calc R U . . . C12 C 0.58740(19) 0.46222(9) 0.78086(12) 0.0441(8) Uani 1 1 d . . . . . H12A H 0.619634 0.440918 0.769435 0.066 Uiso 1 1 calc R U . . . H12B H 0.555988 0.451374 0.805626 0.066 Uiso 1 1 calc R U . . . H12C H 0.620449 0.483652 0.796492 0.066 Uiso 1 1 calc R U . . . C13 C 0.26695(18) 0.52710(10) 0.76862(14) 0.0467(8) Uani 1 1 d . . . . . C14 C 0.2368(2) 0.49949(15) 0.7251(2) 0.0940(17) Uani 1 1 d . . . . . H14A H 0.180273 0.499085 0.721332 0.141 Uiso 1 1 calc R U . . . H14B H 0.256587 0.472378 0.732193 0.141 Uiso 1 1 calc R U . . . H14C H 0.254194 0.509248 0.693799 0.141 Uiso 1 1 calc R U . . . C15 C 0.2535(2) 0.50863(15) 0.8186(2) 0.0937(16) Uani 1 1 d . . . . . H15A H 0.198183 0.504099 0.818931 0.141 Uiso 1 1 calc R U . . . H15B H 0.272743 0.526762 0.846181 0.141 Uiso 1 1 calc R U . . . H15C H 0.281041 0.483075 0.822978 0.141 Uiso 1 1 calc R U . . . C16 C 0.22117(19) 0.56578(11) 0.76140(17) 0.0655(11) Uani 1 1 d . . . . . H16A H 0.233862 0.579505 0.731068 0.098 Uiso 1 1 calc R U . . . H16B H 0.234293 0.583046 0.790899 0.098 Uiso 1 1 calc R U . . . H16C H 0.165851 0.559717 0.757582 0.098 Uiso 1 1 calc R U . . . N17 N 0.51280(13) 0.60647(7) 0.81480(9) 0.0303(5) Uani 1 1 d . . . . . C18 C 0.50290(17) 0.63192(8) 0.85480(11) 0.0326(7) Uani 1 1 d . . . . . C19 C 0.43598(18) 0.64778(9) 0.86945(12) 0.0385(7) Uani 1 1 d . . . . . H19 H 0.386958 0.640731 0.852138 0.046 Uiso 1 1 calc R U . . . C20 C 0.4418(2) 0.67427(9) 0.91004(13) 0.0459(8) Uani 1 1 d . . . . . H20 H 0.396086 0.684693 0.920942 0.055 Uiso 1 1 calc R U . . . C21 C 0.5123(2) 0.68564(9) 0.93465(13) 0.0467(8) Uani 1 1 d . . . . . H21 H 0.514880 0.704498 0.961438 0.056 Uiso 1 1 calc R U . . . C23 C 0.57486(17) 0.64224(8) 0.88161(10) 0.0315(6) Uani 1 1 d . . . . . C22 C 0.57960(18) 0.66974(8) 0.92058(11) 0.0365(7) Uani 1 1 d . . . . . H22 H 0.628406 0.677614 0.937469 0.044 Uiso 1 1 calc R U . . . N24 N 0.63521(13) 0.62295(7) 0.86160(8) 0.0294(5) Uani 1 1 d . . . . . C25 C 0.70558(16) 0.61025(8) 0.88723(10) 0.0290(6) Uani 1 1 d . . . . . C26 C 0.73315(18) 0.61302(8) 0.93816(11) 0.0352(7) Uani 1 1 d . . . . . H26 H 0.704325 0.626577 0.960857 0.042 Uiso 1 1 calc R U . . . C27 C 0.80438(19) 0.59540(9) 0.95546(11) 0.0391(7) Uani 1 1 d . . . . . C29 C 0.81763(17) 0.57165(8) 0.86947(11) 0.0330(7) Uani 1 1 d . . . . . C28 C 0.84513(19) 0.57600(9) 0.92118(11) 0.0393(7) Uani 1 1 d . . . . . H28 H 0.894202 0.565060 0.933214 0.047 Uiso 1 1 calc R U . . . C30 C 0.74591(16) 0.58894(8) 0.85437(10) 0.0289(6) Uani 1 1 d . . . . . O31 O 0.70610(10) 0.58634(5) 0.80696(7) 0.0291(4) Uani 1 1 d . . . . . C32 C 0.8328(2) 0.59637(10) 1.01262(12) 0.0509(9) Uani 1 1 d . . . . . C33 C 0.8287(2) 0.63897(10) 1.03214(12) 0.0550(10) Uani 1 1 d . . . . . H33A H 0.860340 0.656493 1.013664 0.083 Uiso 1 1 calc R U . . . H33B H 0.848077 0.639667 1.068221 0.083 Uiso 1 1 calc R U . . . H33C H 0.775023 0.648195 1.027117 0.083 Uiso 1 1 calc R U . . . C34 C 0.7795(3) 0.56909(12) 1.03964(13) 0.0730(13) Uani 1 1 d . . . . . H34A H 0.726237 0.578835 1.032997 0.109 Uiso 1 1 calc R U . . . H34B H 0.796213 0.569467 1.076084 0.109 Uiso 1 1 calc R U . . . H34C H 0.782117 0.541687 1.026964 0.109 Uiso 1 1 calc R U . . . C35 C 0.9155(3) 0.58193(12) 1.02439(14) 0.0726(13) Uani 1 1 d . . . . . H35A H 0.918692 0.553853 1.014328 0.109 Uiso 1 1 calc R U . . . H35B H 0.932133 0.584445 1.060712 0.109 Uiso 1 1 calc R U . . . H35C H 0.949099 0.598167 1.005731 0.109 Uiso 1 1 calc R U . . . C36 C 0.86065(17) 0.54834(9) 0.83245(11) 0.0372(7) Uani 1 1 d . . . . . C37 C 0.8136(2) 0.51074(9) 0.81523(13) 0.0459(8) Uani 1 1 d . . . . . H37A H 0.762535 0.518707 0.798756 0.069 Uiso 1 1 calc R U . . . H37B H 0.807682 0.493992 0.844628 0.069 Uiso 1 1 calc R U . . . H37C H 0.840561 0.495606 0.791337 0.069 Uiso 1 1 calc R U . . . C38 C 0.9414(2) 0.53542(11) 0.85735(13) 0.0555(9) Uani 1 1 d . . . . . H38A H 0.967748 0.520719 0.832782 0.083 Uiso 1 1 calc R U . . . H38B H 0.936045 0.518174 0.886401 0.083 Uiso 1 1 calc R U . . . H38C H 0.971546 0.559176 0.868701 0.083 Uiso 1 1 calc R U . . . C39 C 0.87151(18) 0.57378(9) 0.78617(12) 0.0397(7) Uani 1 1 d . . . . . H39C H 0.914700 0.560100 0.763600 0.060 Uiso 1 1 d . U . . . H39B H 0.818100 0.575800 0.761900 0.060 Uiso 1 1 d . U . . . H39A H 0.891700 0.601900 0.795700 0.060 Uiso 1 1 d . U . . . K40 K 0.75865(3) 0.65332(2) 0.75439(2) 0.03025(14) Uani 1 1 d . . . . . O41 O 0.61162(10) 0.62987(5) 0.75879(7) 0.0288(4) Uani 1 1 d . . . . . P42 P 0.74328(4) 0.64029(2) 0.60957(3) 0.02626(16) Uani 1 1 d . . . . . C45 C 0.95061(16) 0.59738(9) 0.64371(12) 0.0393(7) Uani 1 1 d . . . . . C44 C 0.87193(15) 0.60296(8) 0.63223(11) 0.0314(6) Uani 1 1 d . . . . . O43 O 0.83862(10) 0.63916(5) 0.61623(7) 0.0326(5) Uani 1 1 d . . . . . C46 C 0.97334(16) 0.55828(9) 0.65650(12) 0.0399(7) Uani 1 1 d . . . . . H46 H 1.026847 0.553212 0.665379 0.048 Uiso 1 1 calc R U . . . C47 C 0.92274(16) 0.52636(9) 0.65705(11) 0.0338(7) Uani 1 1 d . . . . . C49 C 0.81928(15) 0.57199(8) 0.63176(10) 0.0282(6) Uani 1 1 d . . . . . C48 C 0.84402(16) 0.53347(8) 0.64457(10) 0.0313(6) Uani 1 1 d . . . . . H48 H 0.807854 0.512275 0.644822 0.038 Uiso 1 1 calc R U . . . C50 C 1.00806(18) 0.63189(11) 0.64033(17) 0.0586(11) Uani 1 1 d . . . . . C51 C 0.9942(2) 0.66286(12) 0.6809(2) 0.0828(15) Uani 1 1 d . . . . . H51A H 1.028868 0.685682 0.679007 0.124 Uiso 1 1 calc R U . . . H51B H 1.004293 0.650546 0.714441 0.124 Uiso 1 1 calc R U . . . H51C H 0.940501 0.672048 0.675217 0.124 Uiso 1 1 calc R U . . . C52 C 0.9967(2) 0.65044(14) 0.5876(2) 0.0860(15) Uani 1 1 d . . . . . H52A H 1.005852 0.630129 0.562520 0.129 Uiso 1 1 calc R U . . . H52B H 1.033077 0.672577 0.586081 0.129 Uiso 1 1 calc R U . . . H52C H 0.943737 0.660504 0.580231 0.129 Uiso 1 1 calc R U . . . C53 C 1.0915(2) 0.61715(12) 0.6499(2) 0.0782(14) Uani 1 1 d . . . . . H53A H 1.099174 0.595635 0.626137 0.117 Uiso 1 1 calc R U . . . H53B H 1.102164 0.607065 0.684576 0.117 Uiso 1 1 calc R U . . . H53C H 1.126596 0.639317 0.645223 0.117 Uiso 1 1 calc R U . . . C54 C 0.95431(18) 0.48435(9) 0.67109(12) 0.0420(8) Uani 1 1 d . . . . . C55 C 0.9934(2) 0.48436(12) 0.72624(13) 0.0590(10) Uani 1 1 d . . . . . H55A H 1.016167 0.458021 0.734525 0.089 Uiso 1 1 calc R U . . . H55B H 0.954881 0.490291 0.748912 0.089 Uiso 1 1 calc R U . . . H55C H 1.033976 0.504763 0.730328 0.089 Uiso 1 1 calc R U . . . C56 C 1.0155(2) 0.47289(11) 0.63778(14) 0.0545(9) Uani 1 1 d . . . . . H56A H 0.992691 0.473066 0.602297 0.082 Uiso 1 1 calc R U . . . H56B H 1.035066 0.446065 0.646942 0.082 Uiso 1 1 calc R U . . . H56C H 1.058035 0.492157 0.642652 0.082 Uiso 1 1 calc R U . . . C57 C 0.8912(2) 0.45297(10) 0.66662(16) 0.0584(10) Uani 1 1 d . . . . . H57A H 0.867876 0.450975 0.631347 0.088 Uiso 1 1 calc R U . . . H57B H 0.851655 0.460577 0.687802 0.088 Uiso 1 1 calc R U . . . H57C H 0.913347 0.427053 0.677813 0.088 Uiso 1 1 calc R U . . . N58 N 0.74577(12) 0.58665(6) 0.61548(8) 0.0270(5) Uani 1 1 d . . . . . C59 C 0.68349(14) 0.56690(8) 0.58880(10) 0.0246(6) Uani 1 1 d . . . . . C60 C 0.66004(15) 0.52752(8) 0.59112(10) 0.0289(6) Uani 1 1 d . . . . . H60 H 0.689712 0.508916 0.612338 0.035 Uiso 1 1 calc R U . . . C61 C 0.59217(16) 0.51553(8) 0.56183(10) 0.0306(6) Uani 1 1 d . . . . . H61 H 0.576400 0.488369 0.562534 0.037 Uiso 1 1 calc R U . . . C62 C 0.54737(16) 0.54258(8) 0.53174(10) 0.0293(6) Uani 1 1 d . . . . . H62 H 0.500581 0.533942 0.512821 0.035 Uiso 1 1 calc R U . . . C63 C 0.57018(15) 0.58223(8) 0.52894(10) 0.0266(6) Uani 1 1 d . . . . . H63 H 0.539242 0.600935 0.508663 0.032 Uiso 1 1 calc R U . . . C64 C 0.63918(15) 0.59382(8) 0.55647(10) 0.0241(6) Uani 1 1 d . . . . . N65 N 0.67159(12) 0.63222(6) 0.55935(8) 0.0258(5) Uani 1 1 d . . . . . C66 C 0.67180(15) 0.65917(8) 0.51907(10) 0.0271(6) Uani 1 1 d . . . . . C67 C 0.63970(16) 0.65491(8) 0.46952(10) 0.0301(6) Uani 1 1 d . . . . . H67 H 0.608133 0.632504 0.459232 0.036 Uiso 1 1 calc R U . . . C68 C 0.65454(18) 0.68422(9) 0.43470(11) 0.0355(7) Uani 1 1 d . . . . . C69 C 0.69903(19) 0.71716(9) 0.45197(12) 0.0412(8) Uani 1 1 d . . . . . H69 H 0.706744 0.737615 0.428415 0.049 Uiso 1 1 calc R U . . . C70 C 0.73310(18) 0.72193(9) 0.50199(12) 0.0368(7) Uani 1 1 d . . . . . C71 C 0.71920(16) 0.69122(8) 0.53473(10) 0.0299(6) Uani 1 1 d . . . . . O72 O 0.75230(11) 0.68736(5) 0.58391(7) 0.0313(4) Uani 1 1 d . . . . . C73 C 0.6257(2) 0.68015(10) 0.37818(11) 0.0447(8) Uani 1 1 d . . . . . C74 C 0.5749(2) 0.64316(10) 0.36706(12) 0.0545(9) Uani 1 1 d . . . . . H74A H 0.554409 0.642742 0.331159 0.082 Uiso 1 1 calc R U . . . H74B H 0.532090 0.644015 0.387484 0.082 Uiso 1 1 calc R U . . . H74C H 0.605745 0.619032 0.375407 0.082 Uiso 1 1 calc R U . . . C75 C 0.6967(2) 0.67564(12) 0.34965(13) 0.0615(11) Uani 1 1 d . . . . . H75A H 0.679633 0.673260 0.313360 0.092 Uiso 1 1 calc R U . . . H75B H 0.725528 0.651609 0.361539 0.092 Uiso 1 1 calc R U . . . H75C H 0.729915 0.699174 0.355910 0.092 Uiso 1 1 calc R U . . . C76 C 0.5789(2) 0.71703(10) 0.35911(13) 0.0574(10) Uani 1 1 d . . . . . H76A H 0.560761 0.713898 0.323053 0.086 Uiso 1 1 calc R U . . . H76B H 0.611449 0.740906 0.364201 0.086 Uiso 1 1 calc R U . . . H76C H 0.534405 0.719888 0.377860 0.086 Uiso 1 1 calc R U . . . C77 C 0.7860(2) 0.75731(10) 0.51882(13) 0.0496(9) Uani 1 1 d . . . . . C78 C 0.7657(2) 0.77571(9) 0.56777(12) 0.0454(8) Uani 1 1 d . . . . . H78A H 0.794590 0.800636 0.574661 0.068 Uiso 1 1 calc R U . . . H78B H 0.779133 0.756938 0.595691 0.068 Uiso 1 1 calc R U . . . H78C H 0.710205 0.781366 0.564406 0.068 Uiso 1 1 calc R U . . . C79 C 0.7780(3) 0.79069(12) 0.47862(16) 0.0836(15) Uani 1 1 d . . . . . H79A H 0.790448 0.779942 0.446444 0.125 Uiso 1 1 calc R U . . . H79B H 0.813618 0.812549 0.489582 0.125 Uiso 1 1 calc R U . . . H79C H 0.724942 0.800799 0.474277 0.125 Uiso 1 1 calc R U . . . C80 C 0.8688(2) 0.74198(13) 0.52714(18) 0.0821(15) Uani 1 1 d . . . . . H80A H 0.881770 0.729741 0.495928 0.123 Uiso 1 1 calc R U . . . H80B H 0.873873 0.722007 0.554228 0.123 Uiso 1 1 calc R U . . . H80C H 0.903945 0.764324 0.536620 0.123 Uiso 1 1 calc R U . . . K81 K 0.57557(3) 0.61610(2) 0.66255(2) 0.03017(14) Uani 1 1 d . . . . . O82 O 0.71354(10) 0.65225(5) 0.65757(7) 0.0290(4) Uani 1 1 d . . . . . P83 P 0.46309(4) 0.70089(2) 0.62806(3) 0.02491(16) Uani 1 1 d . . . . . O84 O 0.43179(10) 0.65224(5) 0.61826(6) 0.0261(4) Uani 1 1 d . . . . . C85 C 0.41228(15) 0.64196(8) 0.56848(9) 0.0242(6) Uani 1 1 d . . . . . C86 C 0.37189(15) 0.60785(8) 0.55149(10) 0.0265(6) Uani 1 1 d . . . . . C87 C 0.35245(16) 0.60562(8) 0.49882(10) 0.0287(6) Uani 1 1 d . . . . . H87 H 0.326417 0.582333 0.485282 0.034 Uiso 1 1 calc R U . . . C88 C 0.36890(16) 0.63540(8) 0.46516(10) 0.0276(6) Uani 1 1 d . . . . . C89 C 0.41196(16) 0.66827(8) 0.48412(10) 0.0279(6) Uani 1 1 d . . . . . H89 H 0.425647 0.688696 0.462159 0.033 Uiso 1 1 calc R U . . . C90 C 0.43454(15) 0.67064(8) 0.53584(10) 0.0253(6) Uani 1 1 d . . . . . C91 C 0.34527(16) 0.57660(8) 0.58759(10) 0.0317(6) Uani 1 1 d . . . . . C92 C 0.27925(17) 0.59502(10) 0.61303(12) 0.0421(8) Uani 1 1 d . . . . . H92A H 0.236344 0.601940 0.587203 0.063 Uiso 1 1 calc R U . . . H92B H 0.297773 0.619201 0.631463 0.063 Uiso 1 1 calc R U . . . H92C H 0.261575 0.575654 0.636633 0.063 Uiso 1 1 calc R U . . . C93 C 0.41073(17) 0.56452(9) 0.62882(11) 0.0340(7) Uani 1 1 d . . . . . H93A H 0.455958 0.556303 0.613047 0.051 Uiso 1 1 calc R U . . . H93B H 0.393593 0.542209 0.648464 0.051 Uiso 1 1 calc R U . . . H93C H 0.424340 0.587337 0.651214 0.051 Uiso 1 1 calc R U . . . C94 C 0.3167(2) 0.53822(9) 0.55981(12) 0.0458(8) Uani 1 1 d . . . . . H94A H 0.271834 0.544365 0.535135 0.069 Uiso 1 1 calc R U . . . H94B H 0.302060 0.518653 0.584232 0.069 Uiso 1 1 calc R U . . . H94C H 0.357984 0.527117 0.542308 0.069 Uiso 1 1 calc R U . . . C95 C 0.33474(17) 0.63245(8) 0.40900(10) 0.0324(7) Uani 1 1 d . . . . . C96 C 0.3569(2) 0.66802(9) 0.37776(11) 0.0421(8) Uani 1 1 d . . . . . H96A H 0.335973 0.664093 0.342284 0.063 Uiso 1 1 calc R U . . . H96B H 0.413226 0.670117 0.380621 0.063 Uiso 1 1 calc R U . . . H96C H 0.335624 0.692642 0.390378 0.063 Uiso 1 1 calc R U . . . C97 C 0.24685(18) 0.63151(10) 0.40518(12) 0.0449(8) Uani 1 1 d . . . . . H97A H 0.224957 0.628978 0.369673 0.067 Uiso 1 1 calc R U . . . H97B H 0.228396 0.656313 0.419124 0.067 Uiso 1 1 calc R U . . . H97C H 0.230759 0.608635 0.424294 0.067 Uiso 1 1 calc R U . . . C98 C 0.3631(2) 0.59402(9) 0.38586(11) 0.0427(8) Uani 1 1 d . . . . . H98A H 0.342422 0.592646 0.350034 0.064 Uiso 1 1 calc R U . . . H98B H 0.345471 0.570754 0.403569 0.064 Uiso 1 1 calc R U . . . H98C H 0.419662 0.594113 0.389209 0.064 Uiso 1 1 calc R U . . . N99 N 0.47202(12) 0.70184(6) 0.56428(8) 0.0262(5) Uani 1 1 d . . . . . C100 C 0.49629(15) 0.73826(8) 0.54574(10) 0.0272(6) Uani 1 1 d . . . . . C101 C 0.52526(17) 0.74537(9) 0.50059(11) 0.0354(7) Uani 1 1 d . . . . . H101 H 0.530567 0.724086 0.477702 0.043 Uiso 1 1 calc R U . . . C102 C 0.54640(18) 0.78394(9) 0.48925(12) 0.0408(7) Uani 1 1 d . . . . . H102 H 0.565664 0.789189 0.458169 0.049 Uiso 1 1 calc R U . . . C103 C 0.53967(18) 0.81484(9) 0.52284(12) 0.0400(7) Uani 1 1 d . . . . . H103 H 0.553081 0.841259 0.514164 0.048 Uiso 1 1 calc R U . . . C104 C 0.51355(16) 0.80777(9) 0.56915(11) 0.0341(7) Uani 1 1 d . . . . . H104 H 0.510823 0.828994 0.592521 0.041 Uiso 1 1 calc R U . . . C105 C 0.49156(15) 0.76944(8) 0.58079(10) 0.0276(6) Uani 1 1 d . . . . . N106 N 0.46625(12) 0.75443(6) 0.62446(8) 0.0260(5) Uani 1 1 d . . . . . C107 C 0.42074(15) 0.77316(8) 0.65687(10) 0.0261(6) Uani 1 1 d . . . . . C108 C 0.41101(15) 0.81320(8) 0.66774(10) 0.0292(6) Uani 1 1 d . . . . . H108 H 0.440713 0.833013 0.653486 0.035 Uiso 1 1 calc R U . . . C109 C 0.35743(16) 0.82426(8) 0.69970(10) 0.0298(6) Uani 1 1 d . . . . . C110 C 0.31691(16) 0.79427(8) 0.72129(10) 0.0313(6) Uani 1 1 d . . . . . H110 H 0.281601 0.801983 0.743841 0.038 Uiso 1 1 calc R U . . . C111 C 0.32518(15) 0.75349(8) 0.71170(10) 0.0292(6) Uani 1 1 d . . . . . C112 C 0.37771(15) 0.74431(8) 0.67854(10) 0.0265(6) Uani 1 1 d . . . . . O113 O 0.38944(10) 0.70602(5) 0.66128(7) 0.0271(4) Uani 1 1 d . . . . . C114 C 0.33958(17) 0.86836(9) 0.70926(11) 0.0351(7) Uani 1 1 d . . . . . C115 C 0.3408(2) 0.87673(10) 0.76579(13) 0.0582(10) Uani 1 1 d . . . . . H11D H 0.328632 0.904949 0.770782 0.087 Uiso 1 1 calc R U . . . H11E H 0.392118 0.870698 0.783413 0.087 Uiso 1 1 calc R U . . . H11F H 0.302295 0.859883 0.779333 0.087 Uiso 1 1 calc R U . . . C116 C 0.3963(2) 0.89672(9) 0.68908(13) 0.0495(9) Uani 1 1 d . . . . . H11G H 0.394092 0.893195 0.652478 0.074 Uiso 1 1 calc R U . . . H11H H 0.448578 0.890924 0.705291 0.074 Uiso 1 1 calc R U . . . H11I H 0.382711 0.924360 0.696443 0.074 Uiso 1 1 calc R U . . . C117 C 0.2582(2) 0.87731(11) 0.68225(17) 0.0684(12) Uani 1 1 d . . . . . H11J H 0.257185 0.872584 0.645936 0.103 Uiso 1 1 calc R U . . . H11K H 0.245059 0.905281 0.688010 0.103 Uiso 1 1 calc R U . . . H11L H 0.220711 0.859759 0.695627 0.103 Uiso 1 1 calc R U . . . C118 C 0.27937(16) 0.72103(9) 0.73546(11) 0.0346(7) Uani 1 1 d . . . . . C119 C 0.33387(19) 0.68980(10) 0.76210(13) 0.0476(8) Uani 1 1 d . . . . . H11M H 0.363657 0.677276 0.737569 0.071 Uiso 1 1 calc R U . . . H11N H 0.303741 0.669328 0.777170 0.071 Uiso 1 1 calc R U . . . H11O H 0.369178 0.702747 0.788660 0.071 Uiso 1 1 calc R U . . . C120 C 0.22537(19) 0.70000(11) 0.69379(13) 0.0500(9) Uani 1 1 d . . . . . H12D H 0.190336 0.719671 0.675962 0.075 Uiso 1 1 calc R U . . . H12E H 0.195245 0.679566 0.708929 0.075 Uiso 1 1 calc R U . . . H12F H 0.256063 0.687327 0.669868 0.075 Uiso 1 1 calc R U . . . C121 C 0.2314(2) 0.73784(11) 0.77403(14) 0.0574(10) Uani 1 1 d . . . . . H12G H 0.196076 0.758208 0.758020 0.086 Uiso 1 1 calc R U . . . H12H H 0.265497 0.749935 0.801896 0.086 Uiso 1 1 calc R U . . . H12I H 0.201541 0.716257 0.787110 0.086 Uiso 1 1 calc R U . . . O122 O 0.72161(10) 0.79889(5) 0.75977(7) 0.0296(4) Uani 1 1 d . . . . . P123 P 0.72365(4) 0.75443(2) 0.78771(3) 0.02578(16) Uani 1 1 d . . . . . K124 K 0.54558(3) 0.70090(2) 0.76293(2) 0.02931(14) Uani 1 1 d . . . . . O125 O 0.64361(10) 0.77015(5) 0.81308(7) 0.0288(4) Uani 1 1 d . . . . . C126 C 0.64831(16) 0.76728(8) 0.86480(10) 0.0267(6) Uani 1 1 d . . . . . C127 C 0.59547(16) 0.78329(8) 0.89381(10) 0.0291(6) Uani 1 1 d . . . . . C128 C 0.61577(16) 0.78011(8) 0.94613(11) 0.0314(6) Uani 1 1 d . . . . . H128 H 0.580378 0.789890 0.967484 0.038 Uiso 1 1 calc R U . . . C129 C 0.68473(16) 0.76346(8) 0.96875(10) 0.0292(6) Uani 1 1 d . . . . . C130 C 0.73482(16) 0.74637(8) 0.93803(10) 0.0279(6) Uani 1 1 d . . . . . H130 H 0.781512 0.734051 0.952348 0.033 Uiso 1 1 calc R U . . . C131 C 0.71488(15) 0.74776(7) 0.88604(10) 0.0259(6) Uani 1 1 d . . . . . C132 C 0.52193(17) 0.80489(9) 0.87019(11) 0.0361(7) Uani 1 1 d . . . . . C133 C 0.4676(2) 0.81382(13) 0.90931(14) 0.0628(11) Uani 1 1 d . . . . . H13A H 0.420426 0.826350 0.892665 0.094 Uiso 1 1 calc R U . . . H13B H 0.493080 0.832007 0.934976 0.094 Uiso 1 1 calc R U . . . H13C H 0.454476 0.788830 0.925414 0.094 Uiso 1 1 calc R U . . . C134 C 0.5462(2) 0.84419(9) 0.84711(15) 0.0546(10) Uani 1 1 d . . . . . H13D H 0.579847 0.838378 0.821253 0.082 Uiso 1 1 calc R U . . . H13E H 0.574157 0.860802 0.873627 0.082 Uiso 1 1 calc R U . . . H13F H 0.500254 0.858508 0.831702 0.082 Uiso 1 1 calc R U . . . C135 C 0.47729(17) 0.77916(9) 0.82908(11) 0.0374(7) Uani 1 1 d . . . . . H13G H 0.426700 0.791244 0.818582 0.056 Uiso 1 1 calc R U . . . H13H H 0.470314 0.752246 0.842326 0.056 Uiso 1 1 calc R U . . . H13I H 0.506237 0.777487 0.799991 0.056 Uiso 1 1 calc R U . . . C136 C 0.70445(17) 0.76575(9) 1.02655(10) 0.0337(7) Uani 1 1 d . . . . . C137 C 0.6429(2) 0.74315(11) 1.05193(12) 0.0509(9) Uani 1 1 d . . . . . H13J H 0.592121 0.754998 1.041455 0.076 Uiso 1 1 calc R U . . . H13K H 0.655078 0.745076 1.088707 0.076 Uiso 1 1 calc R U . . . H13L H 0.642409 0.714972 1.041783 0.076 Uiso 1 1 calc R U . . . C138 C 0.78258(18) 0.74793(9) 1.04484(11) 0.0408(7) Uani 1 1 d . . . . . H13M H 0.782966 0.719598 1.035466 0.061 Uiso 1 1 calc R U . . . H13N H 0.792855 0.750468 1.081647 0.061 Uiso 1 1 calc R U . . . H13O H 0.822540 0.762172 1.029236 0.061 Uiso 1 1 calc R U . . . C139 C 0.7064(2) 0.80997(9) 1.04230(11) 0.0425(8) Uani 1 1 d . . . . . H13P H 0.745200 0.824138 1.025493 0.064 Uiso 1 1 calc R U . . . H13Q H 0.719783 0.811965 1.078993 0.064 Uiso 1 1 calc R U . . . H13R H 0.655618 0.822003 1.032462 0.064 Uiso 1 1 calc R U . . . N140 N 0.75681(13) 0.73600(6) 0.84718(8) 0.0267(5) Uani 1 1 d . . . . . C141 C 0.82845(15) 0.71660(8) 0.85119(10) 0.0267(6) Uani 1 1 d . . . . . C142 C 0.85910(16) 0.68911(8) 0.88713(11) 0.0324(7) Uani 1 1 d . . . . . H142 H 0.832177 0.682365 0.914755 0.039 Uiso 1 1 calc R U . . . C143 C 0.92986(17) 0.67159(9) 0.88206(12) 0.0372(7) Uani 1 1 d . . . . . H143 H 0.951825 0.653026 0.906735 0.045 Uiso 1 1 calc R U . . . C144 C 0.96840(18) 0.68081(9) 0.84177(12) 0.0392(7) Uani 1 1 d . . . . . H144 H 1.017028 0.668781 0.839203 0.047 Uiso 1 1 calc R U . . . C145 C 0.93722(16) 0.70759(8) 0.80451(11) 0.0343(7) Uani 1 1 d . . . . . H145 H 0.963717 0.713418 0.776397 0.041 Uiso 1 1 calc R U . . . C146 C 0.86722(15) 0.72545(8) 0.80926(10) 0.0277(6) Uani 1 1 d . . . . . N147 N 0.82245(13) 0.75098(7) 0.77651(8) 0.0288(5) Uani 1 1 d . . . . . C148 C 0.84340(16) 0.77943(8) 0.74297(10) 0.0290(6) Uani 1 1 d . . . . . C149 C 0.91070(17) 0.78436(9) 0.72161(11) 0.0331(7) Uani 1 1 d . . . . . H149 H 0.951840 0.765794 0.728483 0.040 Uiso 1 1 calc R U . . . C150 C 0.91772(18) 0.81691(9) 0.68980(11) 0.0347(7) Uani 1 1 d . . . . . C151 C 0.85529(17) 0.84275(9) 0.67953(11) 0.0349(7) Uani 1 1 d . . . . . H151 H 0.859904 0.864304 0.656912 0.042 Uiso 1 1 calc R U . . . C152 C 0.78576(17) 0.83892(8) 0.70058(10) 0.0308(6) Uani 1 1 d . . . . . C153 C 0.78275(16) 0.80647(8) 0.73286(10) 0.0292(6) Uani 1 1 d . . . . . C154 C 0.71848(18) 0.86790(8) 0.68958(11) 0.0356(7) Uani 1 1 d . . . . . C155 C 0.64470(18) 0.84494(10) 0.66938(13) 0.0442(8) Uani 1 1 d . . . . . H15D H 0.601897 0.863835 0.661933 0.066 Uiso 1 1 calc R U . . . H15E H 0.632247 0.825719 0.694869 0.066 Uiso 1 1 calc R U . . . H15F H 0.652957 0.830630 0.638464 0.066 Uiso 1 1 calc R U . . . C156 C 0.7332(2) 0.89899(9) 0.64992(12) 0.0468(8) Uani 1 1 d . . . . . H15G H 0.744040 0.885389 0.619067 0.070 Uiso 1 1 calc R U . . . H15H H 0.777483 0.915590 0.662953 0.070 Uiso 1 1 calc R U . . . H15I H 0.687406 0.915937 0.642310 0.070 Uiso 1 1 calc R U . . . C157 C 0.70498(19) 0.89010(9) 0.73816(12) 0.0421(8) Uani 1 1 d . . . . . H15J H 0.661252 0.908454 0.730883 0.063 Uiso 1 1 calc R U . . . H15K H 0.751368 0.905313 0.750818 0.063 Uiso 1 1 calc R U . . . H15L H 0.693721 0.870687 0.763754 0.063 Uiso 1 1 calc R U . . . C162 C 0.8961(3) 0.42463(14) 0.50778(18) 0.0925(15) Uani 1 1 d . . . . . H16D H 0.915874 0.402780 0.488577 0.139 Uiso 1 1 calc R U . . . H16E H 0.842718 0.418850 0.513121 0.139 Uiso 1 1 calc R U . . . H16F H 0.928061 0.427202 0.540535 0.139 Uiso 1 1 calc R U . . . C163 C 0.8987(3) 0.46351(15) 0.47848(18) 0.0853(14) Uani 1 1 d . . . . . H16G H 0.866595 0.460390 0.445394 0.102 Uiso 1 1 calc R U . . . H16H H 0.952440 0.468272 0.471895 0.102 Uiso 1 1 calc R U . . . C164 C 0.8705(3) 0.50048(14) 0.50504(17) 0.0770(13) Uani 1 1 d . . . . . H16I H 0.818287 0.494848 0.514038 0.092 Uiso 1 1 calc R U . . . H16J H 0.905107 0.504773 0.536913 0.092 Uiso 1 1 calc R U . . . C165 C 0.8672(3) 0.53927(14) 0.47416(17) 0.0754(12) Uani 1 1 d . . . . . H16K H 0.919842 0.545374 0.466360 0.091 Uiso 1 1 calc R U . . . H16L H 0.834408 0.534507 0.441661 0.091 Uiso 1 1 calc R U . . . C166 C 0.8380(3) 0.57402(14) 0.49765(18) 0.0873(15) Uani 1 1 d . . . . . H16M H 0.868474 0.578009 0.531126 0.105 Uiso 1 1 calc R U . . . H16N H 0.783880 0.568887 0.503217 0.105 Uiso 1 1 calc R U . . . C167 C 0.8407(3) 0.61200(16) 0.4673(2) 0.1083(19) Uani 1 1 d . . . . . H16O H 0.808829 0.608804 0.434605 0.162 Uiso 1 1 calc R U . . . H16P H 0.894132 0.617534 0.461836 0.162 Uiso 1 1 calc R U . . . H16Q H 0.820925 0.634292 0.485739 0.162 Uiso 1 1 calc R U . . . O168 O 0.68688(11) 0.72353(5) 0.75128(7) 0.0288(4) Uani 1 1 d . . . . . O169 O 0.53597(10) 0.69268(5) 0.66279(7) 0.0291(4) Uani 1 1 d . . . . . K170 K 0.66560(3) 0.72895(2) 0.65189(2) 0.02920(14) Uani 1 1 d . . . . . C158 C 0.99336(18) 0.82427(9) 0.66702(12) 0.0406(7) Uani 1 1 d . . . . . 160A C 1.0644(6) 0.7959(3) 0.6885(4) 0.030(2) Uiso 0.3333 1 d . . P A 1 H16R H 1.050691 0.767877 0.681052 0.045 Uiso 0.3333 1 calc R U P A 1 H16S H 1.075891 0.799478 0.725078 0.045 Uiso 0.3333 1 calc R U P A 1 H16T H 1.109962 0.802935 0.672318 0.045 Uiso 0.3333 1 calc R U P A 1 159A C 1.0249(7) 0.8663(3) 0.6755(5) 0.051(3) Uiso 0.3333 1 d . . P A 1 H15M H 1.075422 0.868084 0.663390 0.076 Uiso 0.3333 1 calc R U P A 1 H15N H 1.030291 0.872498 0.711698 0.076 Uiso 0.3333 1 calc R U P A 1 H15O H 0.989308 0.885368 0.657069 0.076 Uiso 0.3333 1 calc R U P A 1 161A C 0.9838(6) 0.8166(4) 0.6100(4) 0.047(3) Uiso 0.3333 1 d . . P A 1 H16U H 0.942321 0.833502 0.593453 0.071 Uiso 0.3333 1 calc R U P A 1 H16V H 0.970922 0.788404 0.603425 0.071 Uiso 0.3333 1 calc R U P A 1 H16W H 1.032182 0.822963 0.596688 0.071 Uiso 0.3333 1 calc R U P A 1 160B C 1.0474(7) 0.7898(3) 0.6709(5) 0.044(3) Uiso 0.3333 1 d . . P A 2 H16X H 1.022028 0.766712 0.653320 0.065 Uiso 0.3333 1 calc R U P A 2 H16Y H 1.062374 0.783143 0.706494 0.065 Uiso 0.3333 1 calc R U P A 2 H16Z H 1.093494 0.796865 0.655282 0.065 Uiso 0.3333 1 calc R U P A 2 159B C 1.0323(6) 0.8610(3) 0.6969(4) 0.030(2) Uiso 0.3333 1 d . . P A 2 H15P H 1.080452 0.867846 0.683547 0.045 Uiso 0.3333 1 calc R U P A 2 H15Q H 1.043630 0.854179 0.732773 0.045 Uiso 0.3333 1 calc R U P A 2 H15R H 0.997223 0.883997 0.693012 0.045 Uiso 0.3333 1 calc R U P A 2 161B C 0.9763(6) 0.8377(4) 0.6111(4) 0.041(3) Uiso 0.3333 1 d . . P A 2 H111 H 0.951326 0.815782 0.590827 0.062 Uiso 0.3333 1 calc R U P A 2 H112 H 1.024728 0.844803 0.598386 0.062 Uiso 0.3333 1 calc R U P A 2 H113 H 0.941950 0.860988 0.608777 0.062 Uiso 0.3333 1 calc R U P A 2 159C C 1.0486(8) 0.8396(4) 0.7088(5) 0.069(3) Uiso 0.3333 1 d . . P A 3 H15S H 1.099843 0.841777 0.697743 0.104 Uiso 0.3333 1 calc R U P A 3 H15T H 1.050929 0.821212 0.737571 0.104 Uiso 0.3333 1 calc R U P A 3 H15U H 1.031802 0.866024 0.718998 0.104 Uiso 0.3333 1 calc R U P A 3 161C C 0.9783(9) 0.8552(5) 0.6234(6) 0.076(4) Uiso 0.3333 1 d . . P A 3 H114 H 1.026440 0.860402 0.609300 0.114 Uiso 0.3333 1 calc R U P A 3 H115 H 0.959076 0.880141 0.636484 0.114 Uiso 0.3333 1 calc R U P A 3 H116 H 0.939726 0.844464 0.596950 0.114 Uiso 0.3333 1 calc R U P A 3 160C C 1.0162(7) 0.7857(3) 0.6470(5) 0.055(3) Uiso 0.3333 1 d . . P A 3 H117 H 0.976018 0.776625 0.620436 0.083 Uiso 0.3333 1 calc R U P A 3 H118 H 1.022717 0.765924 0.674241 0.083 Uiso 0.3333 1 calc R U P A 3 H119 H 1.064939 0.788904 0.632827 0.083 Uiso 0.3333 1 calc R U P A 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.0292(4) 0.0250(4) 0.0274(4) -0.0024(3) 0.0074(3) -0.0014(3) O2 0.0289(10) 0.0256(10) 0.0311(10) -0.0033(8) 0.0062(8) -0.0009(8) C3 0.0284(15) 0.0273(15) 0.0267(14) 0.0023(12) 0.0042(12) -0.0005(12) C4 0.0369(16) 0.0223(14) 0.0253(14) 0.0022(11) 0.0034(12) -0.0011(12) C5 0.0381(17) 0.0284(15) 0.0300(15) -0.0020(12) 0.0015(13) -0.0060(13) C7 0.0304(16) 0.0315(16) 0.0464(18) -0.0030(14) 0.0089(14) -0.0012(13) C6 0.0330(16) 0.0345(17) 0.0414(17) -0.0005(14) 0.0077(13) -0.0048(13) C8 0.0322(15) 0.0254(14) 0.0316(15) 0.0001(12) 0.0084(12) -0.0028(12) C9 0.0394(17) 0.0263(15) 0.0324(16) -0.0037(12) 0.0029(13) 0.0022(13) C10 0.0498(19) 0.0376(17) 0.0367(17) -0.0041(14) 0.0106(15) 0.0071(15) C11 0.053(2) 0.0331(17) 0.050(2) -0.0133(15) 0.0048(16) -0.0009(15) C12 0.052(2) 0.0337(17) 0.0451(19) 0.0000(14) 0.0013(16) 0.0081(15) C13 0.0340(18) 0.0408(19) 0.067(2) -0.0072(17) 0.0116(16) -0.0083(15) C14 0.040(2) 0.098(4) 0.145(5) -0.063(3) 0.015(3) -0.027(2) C15 0.052(3) 0.109(4) 0.126(4) 0.044(3) 0.033(3) -0.011(3) C16 0.0307(19) 0.062(2) 0.102(3) -0.009(2) 0.000(2) -0.0047(17) N17 0.0293(13) 0.0259(12) 0.0377(14) -0.0070(10) 0.0128(10) -0.0027(10) C18 0.0400(17) 0.0235(14) 0.0374(16) -0.0032(12) 0.0167(13) -0.0032(13) C19 0.0365(17) 0.0313(16) 0.0500(19) -0.0021(14) 0.0149(15) 0.0011(13) C20 0.049(2) 0.0354(18) 0.059(2) -0.0093(16) 0.0268(17) 0.0051(15) C21 0.058(2) 0.0362(18) 0.050(2) -0.0119(15) 0.0236(17) -0.0002(16) C23 0.0389(17) 0.0261(15) 0.0322(15) -0.0019(12) 0.0152(13) -0.0035(13) C22 0.0446(18) 0.0286(15) 0.0389(17) -0.0082(13) 0.0146(14) -0.0061(13) N24 0.0315(13) 0.0290(13) 0.0289(12) -0.0059(10) 0.0089(10) -0.0020(10) C25 0.0362(16) 0.0230(14) 0.0287(15) -0.0009(12) 0.0078(12) -0.0045(12) C26 0.0516(19) 0.0276(15) 0.0276(15) -0.0020(12) 0.0094(14) -0.0038(14) C27 0.060(2) 0.0288(16) 0.0272(15) 0.0002(13) -0.0003(15) -0.0015(15) C29 0.0399(17) 0.0259(15) 0.0325(16) -0.0023(12) 0.0017(13) -0.0008(13) C28 0.0471(19) 0.0312(16) 0.0368(17) 0.0015(13) -0.0051(14) 0.0035(14) C30 0.0362(16) 0.0271(15) 0.0230(14) -0.0006(11) 0.0023(12) -0.0037(12) O31 0.0299(10) 0.0323(11) 0.0250(10) -0.0033(8) 0.0025(8) 0.0019(8) C32 0.080(3) 0.0414(19) 0.0273(16) -0.0012(14) -0.0073(17) 0.0055(18) C33 0.080(3) 0.046(2) 0.0336(18) -0.0064(15) -0.0114(17) 0.0018(19) C34 0.132(4) 0.056(2) 0.0294(19) 0.0085(17) 0.004(2) -0.014(2) C35 0.099(3) 0.068(3) 0.043(2) -0.0089(19) -0.025(2) 0.024(2) C36 0.0361(17) 0.0355(17) 0.0387(17) -0.0052(14) -0.0007(14) 0.0082(14) C37 0.053(2) 0.0344(18) 0.050(2) -0.0066(15) 0.0088(16) 0.0064(15) C38 0.049(2) 0.064(2) 0.051(2) -0.0086(18) -0.0022(17) 0.0187(18) C39 0.0416(18) 0.0371(17) 0.0419(18) -0.0025(14) 0.0113(14) 0.0032(14) K40 0.0288(3) 0.0281(3) 0.0328(3) -0.0009(3) -0.0001(3) -0.0010(3) O41 0.0316(10) 0.0256(10) 0.0299(10) 0.0014(8) 0.0066(8) -0.0017(8) P42 0.0212(4) 0.0284(4) 0.0302(4) -0.0056(3) 0.0069(3) -0.0016(3) C45 0.0228(15) 0.0434(18) 0.0525(19) -0.0135(15) 0.0078(14) 0.0017(13) C44 0.0238(14) 0.0326(16) 0.0387(16) -0.0100(13) 0.0078(12) 0.0034(12) O43 0.0214(10) 0.0296(11) 0.0477(12) -0.0072(9) 0.0072(9) -0.0018(8) C46 0.0197(14) 0.049(2) 0.0502(19) -0.0118(15) 0.0028(13) 0.0033(14) C47 0.0263(15) 0.0397(17) 0.0357(16) -0.0080(13) 0.0055(12) 0.0059(13) C49 0.0219(14) 0.0347(16) 0.0285(15) -0.0060(12) 0.0048(11) 0.0020(12) C48 0.0266(15) 0.0326(16) 0.0349(16) -0.0021(13) 0.0046(12) 0.0006(12) C50 0.0227(17) 0.047(2) 0.106(3) -0.017(2) 0.0089(18) -0.0023(15) C51 0.037(2) 0.056(2) 0.152(5) -0.039(3) -0.002(2) -0.0091(18) C52 0.047(2) 0.082(3) 0.136(4) 0.034(3) 0.036(3) -0.004(2) C53 0.0288(19) 0.057(2) 0.148(4) -0.016(3) 0.006(2) -0.0064(17) C54 0.0351(17) 0.0412(18) 0.0493(19) -0.0032(15) 0.0043(15) 0.0096(14) C55 0.056(2) 0.071(3) 0.048(2) 0.0014(19) -0.0012(18) 0.024(2) C56 0.052(2) 0.050(2) 0.064(2) -0.0094(18) 0.0150(18) 0.0162(17) C57 0.048(2) 0.040(2) 0.086(3) 0.0061(19) 0.003(2) 0.0120(17) N58 0.0207(11) 0.0281(12) 0.0320(13) -0.0030(10) 0.0029(10) -0.0007(10) C59 0.0208(13) 0.0276(14) 0.0259(14) -0.0040(11) 0.0050(11) 0.0000(11) C60 0.0283(15) 0.0268(15) 0.0308(15) 0.0007(12) 0.0002(12) 0.0015(12) C61 0.0332(16) 0.0226(14) 0.0354(16) -0.0004(12) 0.0020(13) -0.0022(12) C62 0.0256(14) 0.0309(15) 0.0302(15) -0.0041(12) -0.0009(12) -0.0018(12) C63 0.0271(14) 0.0287(15) 0.0241(14) -0.0005(11) 0.0036(11) 0.0006(12) C64 0.0247(14) 0.0241(14) 0.0254(14) -0.0036(11) 0.0106(11) -0.0006(11) N65 0.0259(12) 0.0247(12) 0.0272(12) -0.0010(10) 0.0056(9) -0.0016(10) C66 0.0283(14) 0.0265(14) 0.0290(15) 0.0012(12) 0.0135(12) -0.0007(12) C67 0.0353(16) 0.0285(15) 0.0285(15) -0.0019(12) 0.0117(12) -0.0013(12) C68 0.0449(18) 0.0334(16) 0.0317(16) -0.0015(13) 0.0178(14) 0.0008(14) C69 0.058(2) 0.0335(17) 0.0376(18) 0.0031(14) 0.0282(16) -0.0049(15) C70 0.0421(18) 0.0317(16) 0.0411(18) -0.0029(13) 0.0226(14) -0.0068(14) C71 0.0319(15) 0.0300(15) 0.0303(15) -0.0025(12) 0.0136(12) -0.0004(12) O72 0.0319(11) 0.0290(10) 0.0337(11) -0.0049(8) 0.0071(9) -0.0062(8) C73 0.069(2) 0.0416(19) 0.0267(16) 0.0035(14) 0.0180(15) -0.0004(17) C74 0.085(3) 0.053(2) 0.0247(16) -0.0008(15) 0.0029(17) -0.007(2) C75 0.090(3) 0.067(3) 0.0341(19) 0.0042(17) 0.0340(19) 0.003(2) C76 0.089(3) 0.048(2) 0.0360(19) 0.0067(16) 0.0108(19) 0.005(2) C77 0.058(2) 0.0417(19) 0.055(2) -0.0094(16) 0.0324(18) -0.0237(17) C78 0.056(2) 0.0318(17) 0.053(2) -0.0083(15) 0.0233(17) -0.0154(15) C79 0.133(4) 0.057(3) 0.069(3) -0.003(2) 0.045(3) -0.052(3) C80 0.058(3) 0.083(3) 0.115(4) -0.049(3) 0.045(3) -0.034(2) K81 0.0241(3) 0.0337(3) 0.0331(3) -0.0094(3) 0.0053(3) -0.0011(3) O82 0.0245(10) 0.0327(10) 0.0308(10) -0.0057(8) 0.0073(8) 0.0006(8) P83 0.0231(4) 0.0295(4) 0.0220(3) -0.0036(3) 0.0025(3) -0.0008(3) O84 0.0292(10) 0.0280(10) 0.0207(9) -0.0005(8) 0.0020(8) -0.0001(8) C85 0.0239(14) 0.0279(14) 0.0204(13) -0.0011(11) 0.0005(11) 0.0036(11) C86 0.0266(14) 0.0244(14) 0.0280(14) 0.0017(11) 0.0015(11) 0.0045(11) C87 0.0309(15) 0.0246(14) 0.0291(15) -0.0021(12) -0.0024(12) 0.0017(12) C88 0.0325(15) 0.0259(14) 0.0238(14) -0.0014(11) 0.0008(12) 0.0056(12) C89 0.0343(16) 0.0249(14) 0.0250(14) 0.0011(11) 0.0054(12) 0.0053(12) C90 0.0233(14) 0.0251(14) 0.0278(14) -0.0019(11) 0.0042(11) 0.0019(11) C91 0.0334(16) 0.0305(15) 0.0303(15) 0.0030(12) 0.0008(12) -0.0021(13) C92 0.0331(17) 0.0456(19) 0.0483(19) 0.0111(15) 0.0079(14) -0.0003(14) C93 0.0362(16) 0.0333(16) 0.0322(16) 0.0082(13) 0.0026(13) 0.0010(13) C94 0.057(2) 0.0347(17) 0.0438(19) 0.0070(15) -0.0017(16) -0.0119(15) C95 0.0410(17) 0.0291(15) 0.0254(14) -0.0041(12) -0.0032(13) 0.0067(13) C96 0.063(2) 0.0368(17) 0.0244(15) -0.0006(13) -0.0017(15) 0.0101(16) C97 0.047(2) 0.053(2) 0.0316(17) -0.0047(15) -0.0082(14) 0.0090(16) C98 0.060(2) 0.0367(18) 0.0286(16) -0.0083(13) -0.0033(15) 0.0106(15) N99 0.0296(12) 0.0259(12) 0.0233(11) -0.0031(9) 0.0044(10) -0.0034(10) C100 0.0248(14) 0.0284(15) 0.0286(14) -0.0018(12) 0.0043(11) -0.0040(12) C101 0.0362(17) 0.0364(17) 0.0356(16) -0.0047(13) 0.0120(13) -0.0039(13) C102 0.0451(19) 0.0399(18) 0.0403(18) 0.0009(14) 0.0172(15) -0.0080(15) C103 0.0422(18) 0.0317(16) 0.0487(19) -0.0007(14) 0.0161(15) -0.0077(14) C104 0.0326(16) 0.0322(16) 0.0379(17) -0.0076(13) 0.0062(13) -0.0100(13) C105 0.0200(13) 0.0315(15) 0.0314(15) -0.0039(12) 0.0035(11) -0.0019(12) N106 0.0249(12) 0.0291(12) 0.0246(12) -0.0045(10) 0.0049(9) -0.0024(10) C107 0.0214(13) 0.0329(15) 0.0228(13) -0.0050(12) -0.0018(11) 0.0001(12) C108 0.0278(15) 0.0322(15) 0.0264(14) -0.0048(12) -0.0010(12) -0.0036(12) C109 0.0299(15) 0.0313(15) 0.0264(14) -0.0047(12) -0.0041(12) 0.0024(12) C110 0.0262(15) 0.0380(17) 0.0294(15) -0.0071(13) 0.0023(12) 0.0056(13) C111 0.0254(14) 0.0348(16) 0.0269(14) -0.0022(12) 0.0015(12) 0.0024(12) C112 0.0245(14) 0.0290(15) 0.0253(14) -0.0067(12) 0.0007(11) 0.0025(12) O113 0.0265(10) 0.0283(10) 0.0269(10) -0.0036(8) 0.0057(8) -0.0013(8) C114 0.0325(16) 0.0328(16) 0.0386(17) -0.0064(13) -0.0009(13) 0.0061(13) C115 0.090(3) 0.040(2) 0.046(2) -0.0121(16) 0.017(2) 0.0182(19) C116 0.062(2) 0.0315(17) 0.055(2) -0.0152(15) 0.0097(18) -0.0032(16) C117 0.050(2) 0.040(2) 0.107(3) -0.001(2) -0.023(2) 0.0124(17) C118 0.0302(16) 0.0405(17) 0.0340(16) -0.0051(13) 0.0080(13) -0.0017(13) C119 0.049(2) 0.047(2) 0.048(2) 0.0033(16) 0.0126(16) -0.0059(16) C120 0.0377(18) 0.062(2) 0.051(2) -0.0058(17) 0.0090(16) -0.0115(17) C121 0.064(2) 0.057(2) 0.057(2) -0.0066(18) 0.0322(19) -0.0082(19) O122 0.0294(10) 0.0261(10) 0.0336(11) 0.0027(8) 0.0044(8) -0.0034(8) P123 0.0273(4) 0.0244(4) 0.0253(4) -0.0004(3) 0.0019(3) -0.0019(3) K124 0.0317(3) 0.0284(3) 0.0290(3) -0.0041(3) 0.0087(3) -0.0009(3) O125 0.0281(10) 0.0331(11) 0.0250(10) 0.0000(8) 0.0030(8) 0.0023(8) C126 0.0311(15) 0.0247(14) 0.0245(14) -0.0031(11) 0.0040(12) -0.0057(12) C127 0.0297(15) 0.0239(14) 0.0335(15) -0.0044(12) 0.0038(12) -0.0016(12) C128 0.0331(16) 0.0300(15) 0.0325(16) -0.0086(12) 0.0097(13) -0.0031(12) C129 0.0351(16) 0.0218(14) 0.0310(15) -0.0032(12) 0.0054(12) -0.0052(12) C130 0.0303(15) 0.0252(14) 0.0278(14) 0.0004(12) 0.0020(12) -0.0022(12) C131 0.0288(15) 0.0196(13) 0.0296(15) -0.0016(11) 0.0052(12) -0.0034(11) C132 0.0308(16) 0.0367(17) 0.0398(17) -0.0102(14) 0.0010(13) 0.0036(13) C133 0.046(2) 0.090(3) 0.051(2) -0.018(2) 0.0043(17) 0.026(2) C134 0.044(2) 0.0309(17) 0.083(3) 0.0034(17) -0.0147(19) 0.0056(15) C135 0.0289(16) 0.0381(17) 0.0432(18) -0.0037(14) -0.0039(13) -0.0008(13) C136 0.0414(17) 0.0344(16) 0.0257(15) -0.0026(12) 0.0059(13) -0.0048(13) C137 0.054(2) 0.067(2) 0.0329(17) 0.0003(16) 0.0078(15) -0.0153(18) C138 0.052(2) 0.0425(18) 0.0274(16) -0.0004(14) 0.0019(14) -0.0030(15) C139 0.058(2) 0.0396(18) 0.0297(16) -0.0096(14) 0.0028(15) -0.0017(15) N140 0.0283(12) 0.0282(12) 0.0232(11) -0.0001(9) 0.0022(10) 0.0016(10) C141 0.0266(14) 0.0226(14) 0.0302(15) -0.0029(11) 0.0011(12) -0.0017(11) C142 0.0362(16) 0.0282(15) 0.0323(15) 0.0016(12) 0.0024(13) 0.0003(13) C143 0.0374(17) 0.0312(16) 0.0413(18) 0.0043(14) -0.0012(14) 0.0049(13) C144 0.0341(17) 0.0365(17) 0.0476(19) 0.0006(14) 0.0074(14) 0.0075(14) C145 0.0323(16) 0.0335(16) 0.0377(17) 0.0017(13) 0.0072(13) 0.0021(13) C146 0.0274(15) 0.0229(14) 0.0317(15) -0.0016(12) -0.0007(12) -0.0033(12) N147 0.0268(12) 0.0282(12) 0.0312(13) 0.0036(10) 0.0034(10) -0.0001(10) C148 0.0331(16) 0.0279(15) 0.0258(14) 0.0003(12) 0.0023(12) -0.0058(12) C149 0.0351(16) 0.0318(16) 0.0331(16) -0.0036(13) 0.0071(13) -0.0040(13) C150 0.0446(18) 0.0319(16) 0.0281(15) -0.0037(13) 0.0063(13) -0.0072(14) C151 0.0466(18) 0.0304(16) 0.0279(15) 0.0010(12) 0.0053(13) -0.0117(14) C152 0.0420(17) 0.0244(14) 0.0249(14) -0.0041(12) -0.0004(13) -0.0066(13) C153 0.0334(16) 0.0265(15) 0.0275(14) -0.0040(12) 0.0033(12) -0.0085(12) C154 0.0434(18) 0.0303(16) 0.0319(16) 0.0018(13) 0.0003(13) -0.0040(14) C155 0.0399(18) 0.0411(18) 0.0476(19) 0.0003(15) -0.0101(15) -0.0012(15) C156 0.059(2) 0.0376(18) 0.0423(19) 0.0093(15) 0.0013(16) 0.0004(16) C157 0.053(2) 0.0318(17) 0.0408(18) -0.0029(14) 0.0013(15) -0.0005(15) C162 0.115(4) 0.077(3) 0.081(3) 0.001(3) -0.003(3) -0.024(3) C163 0.078(3) 0.095(4) 0.085(3) -0.015(3) 0.019(3) -0.019(3) C164 0.070(3) 0.091(3) 0.070(3) -0.014(3) 0.011(2) -0.017(2) C165 0.065(3) 0.091(3) 0.072(3) 0.010(3) 0.017(2) -0.009(2) C166 0.107(4) 0.082(3) 0.083(3) -0.003(3) 0.051(3) -0.007(3) C167 0.108(4) 0.094(4) 0.134(5) 0.016(4) 0.060(4) 0.012(3) O168 0.0339(11) 0.0242(10) 0.0276(10) -0.0027(8) 0.0013(8) -0.0043(8) O169 0.0238(10) 0.0343(11) 0.0285(10) -0.0033(8) 0.0014(8) -0.0001(8) K170 0.0306(3) 0.0306(3) 0.0276(3) 0.0020(3) 0.0084(3) 0.0013(3) C158 0.0458(19) 0.0404(18) 0.0378(17) -0.0019(14) 0.0134(15) -0.0078(15) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 O41 1.4979(19) . ? P1 O2 1.6548(18) . ? P1 O31 1.7258(19) . ? P1 N24 1.735(2) . ? P1 N17 1.797(2) . ? P1 K40 3.4767(9) . ? P1 K124 3.6222(9) . ? P1 K81 3.7370(9) . ? O2 C3 1.383(3) . ? C3 C4 1.387(4) . ? C3 C8 1.388(4) . ? C4 C5 1.406(4) . ? C4 C9 1.530(4) . ? C5 C6 1.389(4) . ? C5 H5 0.9500 . ? C7 C8 1.385(4) . ? C7 C6 1.397(4) . ? C7 H7 0.9500 . ? C6 C13 1.539(4) . ? C8 N17 1.387(3) . ? C9 C11 1.528(4) . ? C9 C10 1.530(4) . ? C9 C12 1.542(4) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C15 1.514(5) . ? C13 C16 1.520(5) . ? C13 C14 1.525(5) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? N17 C18 1.393(3) . ? C18 C19 1.384(4) . ? C18 C23 1.409(4) . ? C18 K124 3.514(3) . ? C19 C20 1.393(4) . ? C19 H19 0.9500 . ? C20 C21 1.375(5) . ? C20 H20 0.9500 . ? C21 C22 1.384(4) . ? C21 H21 0.9500 . ? C23 C22 1.383(4) . ? C23 N24 1.398(3) . ? C22 H22 0.9500 . ? N24 C25 1.396(4) . ? C25 C26 1.387(4) . ? C25 C30 1.389(4) . ? C26 C27 1.401(4) . ? C26 H26 0.9500 . ? C27 C28 1.389(4) . ? C27 C32 1.544(4) . ? C29 C30 1.392(4) . ? C29 C28 1.411(4) . ? C29 C36 1.528(4) . ? C28 H28 0.9500 . ? C30 O31 1.368(3) . ? C30 K40 3.457(3) . ? O31 K40 2.8547(19) . ? C32 C35 1.518(5) . ? C32 C33 1.522(5) . ? C32 C34 1.546(5) . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 C39 1.531(4) . ? C36 C37 1.540(4) . ? C36 C38 1.543(4) . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 K40 3.355(3) . ? C39 H39C 1.1204 . ? C39 H39B 1.0688 . ? C39 H39A 1.0252 . ? K40 O82 2.6055(19) . ? K40 O168 2.6577(19) . ? K40 O41 2.7017(19) . ? K40 C146 3.295(3) . ? K40 C141 3.442(3) . ? K40 P123 3.5684(9) . ? K40 P42 3.8653(9) . ? K40 K170 3.9247(8) . ? K40 H39B 2.7902 . ? K40 H39A 2.9880 . ? O41 K81 2.6077(19) . ? O41 K124 2.6487(19) . ? P42 O82 1.4959(19) . ? P42 O43 1.6528(19) . ? P42 O72 1.731(2) . ? P42 N65 1.737(2) . ? P42 N58 1.801(2) . ? P42 K81 3.5037(9) . ? P42 K170 3.5058(9) . ? C45 C44 1.383(4) . ? C45 C46 1.396(4) . ? C45 C50 1.539(5) . ? C44 C49 1.384(4) . ? C44 O43 1.387(3) . ? C46 C47 1.387(4) . ? C46 H46 0.9500 . ? C47 C48 1.394(4) . ? C47 C54 1.538(4) . ? C49 C48 1.388(4) . ? C49 N58 1.392(3) . ? C48 H48 0.9500 . ? C50 C52 1.529(6) . ? C50 C53 1.529(5) . ? C50 C51 1.540(5) . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C52 H52A 0.9800 . ? C52 H52B 0.9800 . ? C52 H52C 0.9800 . ? C53 H53A 0.9800 . ? C53 H53B 0.9800 . ? C53 H53C 0.9800 . ? C54 C57 1.515(5) . ? C54 C56 1.522(4) . ? C54 C55 1.543(5) . ? C55 H55A 0.9800 . ? C55 H55B 0.9800 . ? C55 H55C 0.9800 . ? C56 H56A 0.9800 . ? C56 H56B 0.9800 . ? C56 H56C 0.9800 . ? C57 H57A 0.9800 . ? C57 H57B 0.9800 . ? C57 H57C 0.9800 . ? N58 C59 1.390(3) . ? C59 C60 1.383(4) . ? C59 C64 1.409(4) . ? C59 K81 3.327(3) . ? C60 C61 1.394(4) . ? C60 H60 0.9500 . ? C61 C62 1.385(4) . ? C61 H61 0.9500 . ? C62 C63 1.389(4) . ? C62 H62 0.9500 . ? C63 C64 1.386(4) . ? C63 H63 0.9500 . ? C64 N65 1.402(3) . ? C64 K81 3.255(3) . ? N65 C66 1.403(3) . ? N65 K81 3.443(2) . ? C66 C67 1.377(4) . ? C66 C71 1.386(4) . ? C67 C68 1.397(4) . ? C67 H67 0.9500 . ? C68 C69 1.393(4) . ? C68 C73 1.535(4) . ? C69 C70 1.401(4) . ? C69 H69 0.9500 . ? C70 C71 1.390(4) . ? C70 C77 1.534(4) . ? C71 O72 1.372(3) . ? O72 K170 2.8653(19) . ? C73 C74 1.529(5) . ? C73 C76 1.531(5) . ? C73 C75 1.541(5) . ? C74 H74A 0.9800 . ? C74 H74B 0.9800 . ? C74 H74C 0.9800 . ? C75 H75A 0.9800 . ? C75 H75B 0.9800 . ? C75 H75C 0.9800 . ? C76 H76A 0.9800 . ? C76 H76B 0.9800 . ? C76 H76C 0.9800 . ? C77 C80 1.523(6) . ? C77 C78 1.526(4) . ? C77 C79 1.542(5) . ? C78 K170 3.395(3) . ? C78 H78A 0.9800 . ? C78 H78B 0.9800 . ? C78 H78C 0.9800 . ? C79 H79A 0.9800 . ? C79 H79B 0.9800 . ? C79 H79C 0.9800 . ? C80 H80A 0.9800 . ? C80 H80B 0.9800 . ? C80 H80C 0.9800 . ? K81 O169 2.6528(19) . ? K81 O82 2.7141(19) . ? K81 O84 2.9015(18) . ? K81 C93 3.380(3) . ? K81 P83 3.5059(9) . ? O82 K170 2.6964(19) . ? P83 O169 1.5028(19) . ? P83 O113 1.6605(19) . ? P83 O84 1.7257(19) . ? P83 N99 1.729(2) . ? P83 N106 1.794(2) . ? P83 K170 3.6374(9) . ? P83 K124 3.7053(9) . ? O84 C85 1.373(3) . ? C85 C90 1.384(4) . ? C85 C86 1.387(4) . ? C86 C87 1.406(4) . ? C86 C91 1.533(4) . ? C87 C88 1.395(4) . ? C87 H87 0.9500 . ? C88 C89 1.391(4) . ? C88 C95 1.545(4) . ? C89 C90 1.389(4) . ? C89 H89 0.9500 . ? C90 N99 1.403(3) . ? C91 C94 1.534(4) . ? C91 C93 1.538(4) . ? C91 C92 1.538(4) . ? C92 H92A 0.9800 . ? C92 H92B 0.9800 . ? C92 H92C 0.9800 . ? C93 H93A 0.9800 . ? C93 H93B 0.9800 . ? C93 H93C 0.9800 . ? C94 H94A 0.9800 . ? C94 H94B 0.9800 . ? C94 H94C 0.9800 . ? C95 C97 1.526(4) . ? C95 C96 1.530(4) . ? C95 C98 1.535(4) . ? C96 H96A 0.9800 . ? C96 H96B 0.9800 . ? C96 H96C 0.9800 . ? C97 H97A 0.9800 . ? C97 H97B 0.9800 . ? C97 H97C 0.9800 . ? C98 H98A 0.9800 . ? C98 H98B 0.9800 . ? C98 H98C 0.9800 . ? N99 C100 1.400(3) . ? C100 C101 1.385(4) . ? C100 C105 1.410(4) . ? C101 C102 1.385(4) . ? C101 H101 0.9500 . ? C102 C103 1.383(4) . ? C102 H102 0.9500 . ? C103 C104 1.390(4) . ? C103 H103 0.9500 . ? C104 C105 1.385(4) . ? C104 H104 0.9500 . ? C105 N106 1.391(3) . ? N106 C107 1.395(3) . ? C107 C108 1.385(4) . ? C107 C112 1.393(4) . ? C108 C109 1.393(4) . ? C108 H108 0.9500 . ? C109 C110 1.393(4) . ? C109 C114 1.535(4) . ? C110 C111 1.398(4) . ? C110 H110 0.9500 . ? C111 C112 1.387(4) . ? C111 C118 1.532(4) . ? C112 O113 1.385(3) . ? C114 C116 1.518(4) . ? C114 C115 1.532(4) . ? C114 C117 1.539(4) . ? C115 H11D 0.9800 . ? C115 H11E 0.9800 . ? C115 H11F 0.9800 . ? C116 H11G 0.9800 . ? C116 H11H 0.9800 . ? C116 H11I 0.9800 . ? C117 H11J 0.9800 . ? C117 H11K 0.9800 . ? C117 H11L 0.9800 . ? C118 C121 1.515(4) . ? C118 C119 1.527(4) . ? C118 C120 1.536(4) . ? C119 H11M 0.9800 . ? C119 H11N 0.9800 . ? C119 H11O 0.9800 . ? C120 H12D 0.9800 . ? C120 H12E 0.9800 . ? C120 H12F 0.9800 . ? C121 H12G 0.9800 . ? C121 H12H 0.9800 . ? C121 H12I 0.9800 . ? O122 C153 1.383(3) . ? O122 P123 1.6614(19) . ? P123 O168 1.5062(18) . ? P123 O125 1.7109(19) . ? P123 N140 1.733(2) . ? P123 N147 1.792(2) . ? P123 K124 3.5775(9) . ? P123 K170 3.7376(9) . ? K124 O168 2.6369(19) . ? K124 O169 2.6710(19) . ? K124 O125 3.0838(19) . ? K124 C135 3.452(3) . ? K124 K170 3.9522(8) . ? O125 C126 1.376(3) . ? C126 C127 1.385(4) . ? C126 C131 1.391(4) . ? C127 C128 1.401(4) . ? C127 C132 1.538(4) . ? C128 C129 1.394(4) . ? C128 H128 0.9500 . ? C129 C130 1.395(4) . ? C129 C136 1.540(4) . ? C130 C131 1.388(4) . ? C130 H130 0.9500 . ? C131 N140 1.399(3) . ? C132 C133 1.526(4) . ? C132 C135 1.529(4) . ? C132 C134 1.534(4) . ? C133 H13A 0.9800 . ? C133 H13B 0.9800 . ? C133 H13C 0.9800 . ? C134 H13D 0.9800 . ? C134 H13E 0.9800 . ? C134 H13F 0.9800 . ? C135 H13G 0.9800 . ? C135 H13H 0.9800 . ? C135 H13I 0.9800 . ? C136 C138 1.513(4) . ? C136 C139 1.536(4) . ? C136 C137 1.539(4) . ? C137 H13J 0.9800 . ? C137 H13K 0.9800 . ? C137 H13L 0.9800 . ? C138 H13M 0.9800 . ? C138 H13N 0.9800 . ? C138 H13O 0.9800 . ? C139 H13P 0.9800 . ? C139 H13Q 0.9800 . ? C139 H13R 0.9800 . ? N140 C141 1.402(3) . ? C141 C142 1.387(4) . ? C141 C146 1.410(4) . ? C142 C143 1.390(4) . ? C142 H142 0.9500 . ? C143 C144 1.373(4) . ? C143 H143 0.9500 . ? C144 C145 1.397(4) . ? C144 H144 0.9500 . ? C145 C146 1.381(4) . ? C145 H145 0.9500 . ? C146 N147 1.390(3) . ? N147 C148 1.387(3) . ? C148 C149 1.379(4) . ? C148 C153 1.393(4) . ? C149 C150 1.395(4) . ? C149 H149 0.9500 . ? C150 C151 1.391(4) . ? C150 C158 1.542(4) . ? C151 C152 1.407(4) . ? C151 H151 0.9500 . ? C152 C153 1.391(4) . ? C152 C154 1.523(4) . ? C154 C156 1.528(4) . ? C154 C157 1.538(4) . ? C154 C155 1.538(4) . ? C155 H15D 0.9800 . ? C155 H15E 0.9800 . ? C155 H15F 0.9800 . ? C156 H15G 0.9800 . ? C156 H15H 0.9800 . ? C156 H15I 0.9800 . ? C157 H15J 0.9800 . ? C157 H15K 0.9800 . ? C157 H15L 0.9800 . ? C162 C163 1.521(6) . ? C162 H16D 0.9800 . ? C162 H16E 0.9800 . ? C162 H16F 0.9800 . ? C163 C164 1.536(6) . ? C163 H16G 0.9900 . ? C163 H16H 0.9900 . ? C164 C165 1.534(6) . ? C164 H16I 0.9900 . ? C164 H16J 0.9900 . ? C165 C166 1.443(6) . ? C165 H16K 0.9900 . ? C165 H16L 0.9900 . ? C166 C167 1.510(6) . ? C166 H16M 0.9900 . ? C166 H16N 0.9900 . ? C167 H16O 0.9800 . ? C167 H16P 0.9800 . ? C167 H16Q 0.9800 . ? O168 K170 2.6382(19) . ? O169 K170 2.6168(19) . ? C158 160C 1.470(12) . ? C158 159C 1.472(13) . ? C158 160B 1.485(11) . ? C158 159A 1.515(12) . ? C158 161A 1.531(11) . ? C158 161B 1.551(11) . ? C158 161C 1.554(14) . ? C158 159B 1.573(10) . ? C158 160A 1.610(10) . ? 160A H16R 0.9800 . ? 160A H16S 0.9800 . ? 160A H16T 0.9800 . ? 159A H15M 0.9800 . ? 159A H15N 0.9800 . ? 159A H15O 0.9800 . ? 161A H16U 0.9800 . ? 161A H16V 0.9800 . ? 161A H16W 0.9800 . ? 160B H16X 0.9800 . ? 160B H16Y 0.9800 . ? 160B H16Z 0.9800 . ? 159B H15P 0.9800 . ? 159B H15Q 0.9800 . ? 159B H15R 0.9800 . ? 161B H111 0.9800 . ? 161B H112 0.9800 . ? 161B H113 0.9800 . ? 159C H15S 0.9800 . ? 159C H15T 0.9800 . ? 159C H15U 0.9800 . ? 161C H114 0.9800 . ? 161C H115 0.9800 . ? 161C H116 0.9800 . ? 160C H117 0.9800 . ? 160C H118 0.9800 . ? 160C H119 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O41 P1 O2 111.39(10) . . ? O41 P1 O31 98.21(10) . . ? O2 P1 O31 85.68(9) . . ? O41 P1 N24 115.18(11) . . ? O2 P1 N24 133.41(11) . . ? O31 P1 N24 86.39(10) . . ? O41 P1 N17 100.73(11) . . ? O2 P1 N17 87.41(10) . . ? O31 P1 N17 161.06(11) . . ? N24 P1 N17 85.61(11) . . ? O41 P1 K40 47.53(7) . . ? O2 P1 K40 119.80(7) . . ? O31 P1 K40 54.81(6) . . ? N24 P1 K40 91.51(8) . . ? N17 P1 K40 142.53(8) . . ? O41 P1 K124 39.71(7) . . ? O2 P1 K124 135.23(7) . . ? O31 P1 K124 123.98(7) . . ? N24 P1 K124 85.48(8) . . ? N17 P1 K124 72.40(8) . . ? K40 P1 K124 70.128(19) . . ? O41 P1 K81 32.81(7) . . ? O2 P1 K81 78.66(7) . . ? O31 P1 K81 98.43(6) . . ? N24 P1 K81 147.93(8) . . ? N17 P1 K81 97.46(8) . . ? K40 P1 K81 66.789(18) . . ? K124 P1 K81 65.468(18) . . ? C3 O2 P1 115.46(16) . . ? O2 C3 C4 123.6(2) . . ? O2 C3 C8 113.3(2) . . ? C4 C3 C8 123.1(3) . . ? C3 C4 C5 115.0(2) . . ? C3 C4 C9 122.0(2) . . ? C5 C4 C9 122.9(2) . . ? C6 C5 C4 123.7(3) . . ? C6 C5 H5 118.1 . . ? C4 C5 H5 118.1 . . ? C8 C7 C6 119.3(3) . . ? C8 C7 H7 120.3 . . ? C6 C7 H7 120.3 . . ? C5 C6 C7 118.7(3) . . ? C5 C6 C13 120.6(3) . . ? C7 C6 C13 120.6(3) . . ? C7 C8 N17 130.9(3) . . ? C7 C8 C3 120.1(3) . . ? N17 C8 C3 109.0(2) . . ? C11 C9 C10 107.9(2) . . ? C11 C9 C4 111.9(2) . . ? C10 C9 C4 110.4(2) . . ? C11 C9 C12 108.0(2) . . ? C10 C9 C12 109.6(3) . . ? C4 C9 C12 109.0(2) . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C9 C12 H12A 109.5 . . ? C9 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C9 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C15 C13 C16 108.8(3) . . ? C15 C13 C14 110.3(4) . . ? C16 C13 C14 107.0(3) . . ? C15 C13 C6 108.4(3) . . ? C16 C13 C6 110.8(3) . . ? C14 C13 C6 111.5(3) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C13 C16 H16A 109.5 . . ? C13 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C13 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C8 N17 C18 129.3(2) . . ? C8 N17 P1 113.03(18) . . ? C18 N17 P1 114.16(19) . . ? C19 C18 N17 129.9(3) . . ? C19 C18 C23 119.6(3) . . ? N17 C18 C23 110.5(2) . . ? C19 C18 K124 101.91(18) . . ? N17 C18 K124 78.97(15) . . ? C23 C18 K124 86.54(16) . . ? C18 C19 C20 118.8(3) . . ? C18 C19 H19 120.6 . . ? C20 C19 H19 120.6 . . ? C21 C20 C19 121.4(3) . . ? C21 C20 H20 119.3 . . ? C19 C20 H20 119.3 . . ? C20 C21 C22 120.3(3) . . ? C20 C21 H21 119.9 . . ? C22 C21 H21 119.9 . . ? C22 C23 N24 128.1(3) . . ? C22 C23 C18 120.7(3) . . ? N24 C23 C18 111.1(2) . . ? C23 C22 C21 119.1(3) . . ? C23 C22 H22 120.4 . . ? C21 C22 H22 120.4 . . ? C25 N24 C23 127.8(2) . . ? C25 N24 P1 114.78(18) . . ? C23 N24 P1 115.40(19) . . ? C26 C25 C30 120.8(3) . . ? C26 C25 N24 129.5(3) . . ? C30 C25 N24 109.4(2) . . ? C25 C26 C27 118.6(3) . . ? C25 C26 H26 120.7 . . ? C27 C26 H26 120.7 . . ? C28 C27 C26 119.1(3) . . ? C28 C27 C32 122.2(3) . . ? C26 C27 C32 118.6(3) . . ? C30 C29 C28 115.1(3) . . ? C30 C29 C36 121.5(2) . . ? C28 C29 C36 123.4(3) . . ? C27 C28 C29 123.6(3) . . ? C27 C28 H28 118.2 . . ? C29 C28 H28 118.2 . . ? O31 C30 C25 112.2(2) . . ? O31 C30 C29 125.1(2) . . ? C25 C30 C29 122.6(3) . . ? O31 C30 K40 53.14(12) . . ? C25 C30 K40 104.78(17) . . ? C29 C30 K40 109.82(18) . . ? C30 O31 P1 114.75(16) . . ? C30 O31 K40 104.32(15) . . ? P1 O31 K40 95.59(8) . . ? C35 C32 C33 108.2(3) . . ? C35 C32 C27 112.2(3) . . ? C33 C32 C27 109.6(3) . . ? C35 C32 C34 109.2(3) . . ? C33 C32 C34 109.6(3) . . ? C27 C32 C34 108.1(3) . . ? C32 C33 H33A 109.5 . . ? C32 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C32 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C32 C34 H34A 109.5 . . ? C32 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? C32 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C32 C35 H35A 109.5 . . ? C32 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? C32 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C29 C36 C39 111.0(2) . . ? C29 C36 C37 108.8(3) . . ? C39 C36 C37 109.2(2) . . ? C29 C36 C38 111.2(2) . . ? C39 C36 C38 107.7(3) . . ? C37 C36 C38 108.9(3) . . ? C36 C37 H37A 109.5 . . ? C36 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C36 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C36 C38 H38A 109.5 . . ? C36 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C36 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C36 C39 K40 121.05(18) . . ? C36 C39 H39C 111.5 . . ? K40 C39 H39C 127.0 . . ? C36 C39 H39B 109.7 . . ? K40 C39 H39B 49.9 . . ? H39C C39 H39B 107.2 . . ? C36 C39 H39A 112.5 . . ? K40 C39 H39A 60.6 . . ? H39C C39 H39A 105.9 . . ? H39B C39 H39A 109.8 . . ? O82 K40 O168 84.18(6) . . ? O82 K40 O41 82.45(6) . . ? O168 K40 O41 79.08(6) . . ? O82 K40 O31 113.63(6) . . ? O168 K40 O31 121.92(6) . . ? O41 K40 O31 52.04(5) . . ? O82 K40 C146 122.42(7) . . ? O168 K40 C146 67.06(6) . . ? O41 K40 C146 133.64(7) . . ? O31 K40 C146 123.94(6) . . ? O82 K40 C39 109.55(7) . . ? O168 K40 C39 165.44(7) . . ? O41 K40 C39 106.88(7) . . ? O31 K40 C39 57.92(7) . . ? C146 K40 C39 100.42(7) . . ? O82 K40 C141 141.94(6) . . ? O168 K40 C141 66.52(6) . . ? O41 K40 C141 113.25(6) . . ? O31 K40 C141 102.64(6) . . ? C146 K40 C141 24.04(6) . . ? C39 K40 C141 98.99(7) . . ? O82 K40 C30 135.74(6) . . ? O168 K40 C30 119.88(6) . . ? O41 K40 C30 68.41(6) . . ? O31 K40 C30 22.54(6) . . ? C146 K40 C30 101.66(7) . . ? C39 K40 C30 53.43(7) . . ? C141 K40 C30 81.64(6) . . ? O82 K40 P1 102.30(4) . . ? O168 K40 P1 94.68(4) . . ? O41 K40 P1 24.14(4) . . ? O31 K40 P1 29.61(4) . . ? C146 K40 P1 127.68(5) . . ? C39 K40 P1 87.27(6) . . ? C141 K40 P1 103.75(5) . . ? C30 K40 P1 44.27(5) . . ? O82 K40 P123 102.72(4) . . ? O168 K40 P123 22.46(4) . . ? O41 K40 P123 94.05(4) . . ? O31 K40 P123 123.03(4) . . ? C146 K40 P123 45.80(5) . . ? C39 K40 P123 143.29(6) . . ? C141 K40 P123 44.44(5) . . ? C30 K40 P123 111.59(5) . . ? P1 K40 P123 102.74(2) . . ? O82 K40 P42 14.60(4) . . ? O168 K40 P42 95.46(4) . . ? O41 K40 P42 93.66(4) . . ? O31 K40 P42 114.64(4) . . ? C146 K40 P42 119.38(5) . . ? C39 K40 P42 97.36(6) . . ? C141 K40 P42 142.50(5) . . ? C30 K40 P42 134.31(5) . . ? P1 K40 P42 110.55(2) . . ? P123 K40 P42 111.31(2) . . ? O82 K40 K170 43.15(4) . . ? O168 K40 K170 41.99(4) . . ? O41 K40 K170 84.53(4) . . ? O31 K40 K170 135.85(4) . . ? C146 K40 K170 90.16(5) . . ? C39 K40 K170 149.95(6) . . ? C141 K40 K170 101.75(5) . . ? C30 K40 K170 151.40(5) . . ? P1 K40 K170 108.40(2) . . ? P123 K40 K170 59.616(17) . . ? P42 K40 K170 53.485(16) . . ? O82 K40 H39B 97.0 . . ? O168 K40 H39B 173.1 . . ? O41 K40 H39B 94.3 . . ? O31 K40 H39B 51.4 . . ? C146 K40 H39B 117.4 . . ? C39 K40 H39B 17.0 . . ? C141 K40 H39B 115.1 . . ? C30 K40 H39B 54.9 . . ? P1 K40 H39B 78.4 . . ? P123 K40 H39B 159.4 . . ? P42 K40 H39B 86.9 . . ? K170 K40 H39B 140.0 . . ? O82 K40 H39A 118.8 . . ? O168 K40 H39A 149.5 . . ? O41 K40 H39A 121.1 . . ? O31 K40 H39A 69.5 . . ? C146 K40 H39A 83.1 . . ? C39 K40 H39A 17.4 . . ? C141 K40 H39A 83.8 . . ? C30 K40 H39A 58.6 . . ? P1 K40 H39A 99.0 . . ? P123 K40 H39A 127.1 . . ? P42 K40 H39A 104.9 . . ? K170 K40 H39A 149.6 . . ? H39B K40 H39A 34.3 . . ? P1 O41 K81 129.05(10) . . ? P1 O41 K124 119.11(10) . . ? K81 O41 K124 98.45(6) . . ? P1 O41 K40 108.32(9) . . ? K81 O41 K40 96.98(6) . . ? K124 O41 K40 99.37(6) . . ? O82 P42 O43 111.57(10) . . ? O82 P42 O72 98.88(10) . . ? O43 P42 O72 85.58(10) . . ? O82 P42 N65 114.09(11) . . ? O43 P42 N65 134.30(11) . . ? O72 P42 N65 85.91(10) . . ? O82 P42 N58 101.44(11) . . ? O43 P42 N58 87.41(10) . . ? O72 P42 N58 159.67(10) . . ? N65 P42 N58 85.40(10) . . ? O82 P42 K81 47.01(7) . . ? O43 P42 K81 146.45(8) . . ? O72 P42 K81 119.45(7) . . ? N65 P42 K81 73.58(7) . . ? N58 P42 K81 75.34(7) . . ? O82 P42 K170 46.21(7) . . ? O43 P42 K170 114.22(7) . . ? O72 P42 K170 54.33(6) . . ? N65 P42 K170 96.29(8) . . ? N58 P42 K170 145.10(8) . . ? K81 P42 K170 71.829(19) . . ? O82 P42 K40 26.05(7) . . ? O43 P42 K40 87.29(7) . . ? O72 P42 K40 107.14(7) . . ? N65 P42 K40 137.91(8) . . ? N58 P42 K40 91.54(7) . . ? K81 P42 K40 65.098(18) . . ? K170 P42 K40 64.124(17) . . ? C44 C45 C46 115.1(3) . . ? C44 C45 C50 121.5(3) . . ? C46 C45 C50 123.3(3) . . ? C45 C44 C49 122.8(3) . . ? C45 C44 O43 123.5(3) . . ? C49 C44 O43 113.4(2) . . ? C44 O43 P42 115.54(17) . . ? C47 C46 C45 124.1(3) . . ? C47 C46 H46 117.9 . . ? C45 C46 H46 117.9 . . ? C46 C47 C48 118.5(3) . . ? C46 C47 C54 119.7(3) . . ? C48 C47 C54 121.8(3) . . ? C44 C49 C48 120.4(2) . . ? C44 C49 N58 109.0(2) . . ? C48 C49 N58 130.6(3) . . ? C49 C48 C47 119.0(3) . . ? C49 C48 H48 120.5 . . ? C47 C48 H48 120.5 . . ? C52 C50 C53 107.2(3) . . ? C52 C50 C45 110.4(3) . . ? C53 C50 C45 111.3(3) . . ? C52 C50 C51 111.2(4) . . ? C53 C50 C51 109.3(3) . . ? C45 C50 C51 107.5(3) . . ? C50 C51 H51A 109.5 . . ? C50 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C50 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C50 C52 H52A 109.5 . . ? C50 C52 H52B 109.5 . . ? H52A C52 H52B 109.5 . . ? C50 C52 H52C 109.5 . . ? H52A C52 H52C 109.5 . . ? H52B C52 H52C 109.5 . . ? C50 C53 H53A 109.5 . . ? C50 C53 H53B 109.5 . . ? H53A C53 H53B 109.5 . . ? C50 C53 H53C 109.5 . . ? H53A C53 H53C 109.5 . . ? H53B C53 H53C 109.5 . . ? C57 C54 C56 109.7(3) . . ? C57 C54 C47 112.2(3) . . ? C56 C54 C47 110.1(3) . . ? C57 C54 C55 107.8(3) . . ? C56 C54 C55 107.4(3) . . ? C47 C54 C55 109.5(3) . . ? C54 C55 H55A 109.5 . . ? C54 C55 H55B 109.5 . . ? H55A C55 H55B 109.5 . . ? C54 C55 H55C 109.5 . . ? H55A C55 H55C 109.5 . . ? H55B C55 H55C 109.5 . . ? C54 C56 H56A 109.5 . . ? C54 C56 H56B 109.5 . . ? H56A C56 H56B 109.5 . . ? C54 C56 H56C 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? C54 C57 H57A 109.5 . . ? C54 C57 H57B 109.5 . . ? H57A C57 H57B 109.5 . . ? C54 C57 H57C 109.5 . . ? H57A C57 H57C 109.5 . . ? H57B C57 H57C 109.5 . . ? C59 N58 C49 128.6(2) . . ? C59 N58 P42 114.83(17) . . ? C49 N58 P42 112.91(17) . . ? C60 C59 N58 130.3(2) . . ? C60 C59 C64 119.5(2) . . ? N58 C59 C64 110.1(2) . . ? C60 C59 K81 104.56(17) . . ? N58 C59 K81 85.81(14) . . ? C64 C59 K81 74.81(14) . . ? C59 C60 C61 119.0(2) . . ? C59 C60 H60 120.5 . . ? C61 C60 H60 120.5 . . ? C62 C61 C60 121.1(3) . . ? C62 C61 H61 119.5 . . ? C60 C61 H61 119.5 . . ? C61 C62 C63 120.6(2) . . ? C61 C62 H62 119.7 . . ? C63 C62 H62 119.7 . . ? C64 C63 C62 118.3(2) . . ? C64 C63 H63 120.8 . . ? C62 C63 H63 120.8 . . ? C63 C64 N65 127.1(2) . . ? C63 C64 C59 121.3(2) . . ? N65 C64 C59 111.4(2) . . ? C63 C64 K81 98.97(16) . . ? N65 C64 K81 85.54(14) . . ? C59 C64 K81 80.50(15) . . ? C64 N65 C66 125.9(2) . . ? C64 N65 P42 115.59(17) . . ? C66 N65 P42 114.86(17) . . ? C64 N65 K81 70.52(13) . . ? C66 N65 K81 139.64(16) . . ? P42 N65 K81 77.48(8) . . ? C67 C66 C71 121.7(2) . . ? C67 C66 N65 129.0(2) . . ? C71 C66 N65 108.9(2) . . ? C66 C67 C68 118.6(3) . . ? C66 C67 H67 120.7 . . ? C68 C67 H67 120.7 . . ? C69 C68 C67 118.5(3) . . ? C69 C68 C73 119.7(3) . . ? C67 C68 C73 121.7(3) . . ? C68 C69 C70 123.9(3) . . ? C68 C69 H69 118.0 . . ? C70 C69 H69 118.0 . . ? C71 C70 C69 115.4(3) . . ? C71 C70 C77 122.2(3) . . ? C69 C70 C77 122.4(3) . . ? O72 C71 C66 112.3(2) . . ? O72 C71 C70 125.8(3) . . ? C66 C71 C70 121.8(3) . . ? C71 O72 P42 114.54(16) . . ? C71 O72 K170 111.55(15) . . ? P42 O72 K170 96.27(8) . . ? C74 C73 C76 108.3(3) . . ? C74 C73 C68 111.9(2) . . ? C76 C73 C68 110.5(3) . . ? C74 C73 C75 107.9(3) . . ? C76 C73 C75 110.1(3) . . ? C68 C73 C75 108.0(3) . . ? C73 C74 H74A 109.5 . . ? C73 C74 H74B 109.5 . . ? H74A C74 H74B 109.5 . . ? C73 C74 H74C 109.5 . . ? H74A C74 H74C 109.5 . . ? H74B C74 H74C 109.5 . . ? C73 C75 H75A 109.5 . . ? C73 C75 H75B 109.5 . . ? H75A C75 H75B 109.5 . . ? C73 C75 H75C 109.5 . . ? H75A C75 H75C 109.5 . . ? H75B C75 H75C 109.5 . . ? C73 C76 H76A 109.5 . . ? C73 C76 H76B 109.5 . . ? H76A C76 H76B 109.5 . . ? C73 C76 H76C 109.5 . . ? H76A C76 H76C 109.5 . . ? H76B C76 H76C 109.5 . . ? C80 C77 C78 109.3(3) . . ? C80 C77 C70 108.0(3) . . ? C78 C77 C70 111.4(2) . . ? C80 C77 C79 110.3(3) . . ? C78 C77 C79 107.1(3) . . ? C70 C77 C79 110.9(3) . . ? C77 C78 K170 125.12(18) . . ? C77 C78 H78A 109.5 . . ? K170 C78 H78A 124.3 . . ? C77 C78 H78B 109.5 . . ? K170 C78 H78B 45.3 . . ? H78A C78 H78B 109.5 . . ? C77 C78 H78C 109.5 . . ? K170 C78 H78C 64.2 . . ? H78A C78 H78C 109.5 . . ? H78B C78 H78C 109.5 . . ? C77 C79 H79A 109.5 . . ? C77 C79 H79B 109.5 . . ? H79A C79 H79B 109.5 . . ? C77 C79 H79C 109.5 . . ? H79A C79 H79C 109.5 . . ? H79B C79 H79C 109.5 . . ? C77 C80 H80A 109.5 . . ? C77 C80 H80B 109.5 . . ? H80A C80 H80B 109.5 . . ? C77 C80 H80C 109.5 . . ? H80A C80 H80C 109.5 . . ? H80B C80 H80C 109.5 . . ? O41 K81 O169 81.83(6) . . ? O41 K81 O82 82.17(6) . . ? O169 K81 O82 78.68(6) . . ? O41 K81 O84 114.66(6) . . ? O169 K81 O84 52.15(5) . . ? O82 K81 O84 121.53(6) . . ? O41 K81 C64 146.16(7) . . ? O169 K81 C64 109.92(6) . . ? O82 K81 C64 69.95(6) . . ? O84 K81 C64 96.52(6) . . ? O41 K81 C59 125.84(6) . . ? O169 K81 C59 130.25(6) . . ? O82 K81 C59 67.58(6) . . ? O84 K81 C59 119.39(6) . . ? C64 K81 C59 24.69(6) . . ? O41 K81 C93 116.40(7) . . ? O169 K81 C93 106.24(6) . . ? O82 K81 C93 161.10(7) . . ? O84 K81 C93 55.90(6) . . ? C64 K81 C93 91.37(7) . . ? C59 K81 C93 96.72(7) . . ? O41 K81 N65 132.76(6) . . ? O169 K81 N65 90.24(6) . . ? O82 K81 N65 50.67(5) . . ? O84 K81 N65 95.32(5) . . ? C64 K81 N65 23.95(6) . . ? C59 K81 N65 40.07(6) . . ? C93 K81 N65 110.56(6) . . ? O41 K81 P42 104.25(4) . . ? O169 K81 P42 90.55(4) . . ? O82 K81 P42 23.78(4) . . ? O84 K81 P42 117.66(4) . . ? C64 K81 P42 46.19(5) . . ? C59 K81 P42 46.43(5) . . ? C93 K81 P42 137.54(5) . . ? N65 K81 P42 28.94(4) . . ? O41 K81 P83 100.01(4) . . ? O169 K81 P83 23.41(4) . . ? O82 K81 P83 95.66(4) . . ? O84 K81 P83 29.36(4) . . ? C64 K81 P83 101.42(5) . . ? C59 K81 P83 125.81(5) . . ? C93 K81 P83 84.97(5) . . ? N65 K81 P83 88.66(4) . . ? P42 K81 P83 100.18(2) . . ? O41 K81 P1 18.14(4) . . ? O169 K81 P1 97.62(4) . . ? O82 K81 P1 93.97(4) . . ? O84 K81 P1 119.16(4) . . ? C64 K81 P1 143.81(5) . . ? C59 K81 P1 119.46(5) . . ? C93 K81 P1 103.26(5) . . ? N65 K81 P1 141.51(4) . . ? P42 K81 P1 112.98(2) . . ? P83 K81 P1 112.57(2) . . ? O41 K81 K40 42.41(4) . . ? O169 K81 K40 83.46(4) . . ? O82 K81 K40 40.60(4) . . ? O84 K81 K40 135.12(4) . . ? C64 K81 K40 105.77(5) . . ? C59 K81 K40 92.75(5) . . ? C93 K81 K40 156.35(5) . . ? N65 K81 K40 90.54(4) . . ? P42 K81 K40 61.848(18) . . ? P83 K81 K40 106.82(2) . . ? P1 K81 K40 53.473(16) . . ? P42 O82 K40 139.35(10) . . ? P42 O82 K170 110.17(10) . . ? K40 O82 K170 95.49(6) . . ? P42 O82 K81 109.21(9) . . ? K40 O82 K81 96.73(6) . . ? K170 O82 K81 98.92(6) . . ? O169 P83 O113 110.03(10) . . ? O169 P83 O84 98.57(10) . . ? O113 P83 O84 85.77(9) . . ? O169 P83 N99 115.87(11) . . ? O113 P83 N99 134.08(10) . . ? O84 P83 N99 86.22(9) . . ? O169 P83 N106 100.71(10) . . ? O113 P83 N106 87.52(10) . . ? O84 P83 N106 160.72(10) . . ? N99 P83 N106 85.52(10) . . ? O169 P83 K81 44.52(7) . . ? O113 P83 K81 112.92(7) . . ? O84 P83 K81 55.52(6) . . ? N99 P83 K81 98.99(8) . . ? N106 P83 K81 143.23(8) . . ? O169 P83 K170 37.77(7) . . ? O113 P83 K170 132.97(7) . . ? O84 P83 K170 123.52(7) . . ? N99 P83 K170 87.78(8) . . ? N106 P83 K170 73.51(7) . . ? K81 P83 K170 70.254(18) . . ? O169 P83 K124 37.35(7) . . ? O113 P83 K124 73.38(6) . . ? O84 P83 K124 102.97(6) . . ? N99 P83 K124 152.15(8) . . ? N106 P83 K124 92.36(7) . . ? K81 P83 K124 66.942(18) . . ? K170 P83 K124 65.122(17) . . ? C85 O84 P83 114.70(16) . . ? C85 O84 K81 112.75(14) . . ? P83 O84 K81 95.13(7) . . ? O84 C85 C90 112.4(2) . . ? O84 C85 C86 125.2(2) . . ? C90 C85 C86 122.4(2) . . ? C85 C86 C87 114.8(2) . . ? C85 C86 C91 122.5(2) . . ? C87 C86 C91 122.6(2) . . ? C88 C87 C86 124.2(2) . . ? C88 C87 H87 117.9 . . ? C86 C87 H87 117.9 . . ? C89 C88 C87 118.4(2) . . ? C89 C88 C95 121.9(2) . . ? C87 C88 C95 119.6(2) . . ? C90 C89 C88 118.7(2) . . ? C90 C89 H89 120.7 . . ? C88 C89 H89 120.7 . . ? C85 C90 C89 121.3(2) . . ? C85 C90 N99 108.9(2) . . ? C89 C90 N99 129.4(2) . . ? C86 C91 C94 111.9(2) . . ? C86 C91 C93 111.8(2) . . ? C94 C91 C93 107.1(2) . . ? C86 C91 C92 107.9(2) . . ? C94 C91 C92 109.4(3) . . ? C93 C91 C92 108.7(2) . . ? C91 C92 H92A 109.5 . . ? C91 C92 H92B 109.5 . . ? H92A C92 H92B 109.5 . . ? C91 C92 H92C 109.5 . . ? H92A C92 H92C 109.5 . . ? H92B C92 H92C 109.5 . . ? C91 C93 K81 126.03(17) . . ? C91 C93 H93A 109.5 . . ? K81 C93 H93A 63.4 . . ? C91 C93 H93B 109.5 . . ? K81 C93 H93B 123.6 . . ? H93A C93 H93B 109.5 . . ? C91 C93 H93C 109.5 . . ? K81 C93 H93C 46.1 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.5 . . ? C91 C94 H94A 109.5 . . ? C91 C94 H94B 109.5 . . ? H94A C94 H94B 109.5 . . ? C91 C94 H94C 109.5 . . ? H94A C94 H94C 109.5 . . ? H94B C94 H94C 109.5 . . ? C97 C95 C96 107.5(2) . . ? C97 C95 C98 109.2(2) . . ? C96 C95 C98 108.4(2) . . ? C97 C95 C88 109.2(2) . . ? C96 C95 C88 112.7(2) . . ? C98 C95 C88 109.8(2) . . ? C95 C96 H96A 109.5 . . ? C95 C96 H96B 109.5 . . ? H96A C96 H96B 109.5 . . ? C95 C96 H96C 109.5 . . ? H96A C96 H96C 109.5 . . ? H96B C96 H96C 109.5 . . ? C95 C97 H97A 109.5 . . ? C95 C97 H97B 109.5 . . ? H97A C97 H97B 109.5 . . ? C95 C97 H97C 109.5 . . ? H97A C97 H97C 109.5 . . ? H97B C97 H97C 109.5 . . ? C95 C98 H98A 109.5 . . ? C95 C98 H98B 109.5 . . ? H98A C98 H98B 109.5 . . ? C95 C98 H98C 109.5 . . ? H98A C98 H98C 109.5 . . ? H98B C98 H98C 109.5 . . ? C100 N99 C90 126.7(2) . . ? C100 N99 P83 115.63(17) . . ? C90 N99 P83 115.17(17) . . ? C101 C100 N99 128.1(2) . . ? C101 C100 C105 120.6(3) . . ? N99 C100 C105 111.3(2) . . ? C100 C101 C102 119.1(3) . . ? C100 C101 H101 120.4 . . ? C102 C101 H101 120.4 . . ? C103 C102 C101 120.5(3) . . ? C103 C102 H102 119.8 . . ? C101 C102 H102 119.8 . . ? C102 C103 C104 120.9(3) . . ? C102 C103 H103 119.6 . . ? C104 C103 H103 119.6 . . ? C105 C104 C103 119.2(3) . . ? C105 C104 H104 120.4 . . ? C103 C104 H104 120.4 . . ? C104 C105 N106 130.4(3) . . ? C104 C105 C100 119.6(3) . . ? N106 C105 C100 109.9(2) . . ? C105 N106 C107 128.6(2) . . ? C105 N106 P83 114.83(17) . . ? C107 N106 P83 113.02(17) . . ? C108 C107 C112 119.7(2) . . ? C108 C107 N106 131.2(3) . . ? C112 C107 N106 109.0(2) . . ? C107 C108 C109 119.6(3) . . ? C107 C108 H108 120.2 . . ? C109 C108 H108 120.2 . . ? C108 C109 C110 118.5(3) . . ? C108 C109 C114 121.5(3) . . ? C110 C109 C114 119.9(3) . . ? C109 C110 C111 123.8(3) . . ? C109 C110 H110 118.1 . . ? C111 C110 H110 118.1 . . ? C112 C111 C110 115.1(3) . . ? C112 C111 C118 122.0(2) . . ? C110 C111 C118 122.9(2) . . ? O113 C112 C111 123.7(2) . . ? O113 C112 C107 113.1(2) . . ? C111 C112 C107 123.1(2) . . ? C112 O113 P83 115.46(16) . . ? C116 C114 C115 107.9(3) . . ? C116 C114 C109 112.7(2) . . ? C115 C114 C109 111.2(2) . . ? C116 C114 C117 108.5(3) . . ? C115 C114 C117 108.8(3) . . ? C109 C114 C117 107.7(2) . . ? C114 C115 H11D 109.5 . . ? C114 C115 H11E 109.5 . . ? H11D C115 H11E 109.5 . . ? C114 C115 H11F 109.5 . . ? H11D C115 H11F 109.5 . . ? H11E C115 H11F 109.5 . . ? C114 C116 H11G 109.5 . . ? C114 C116 H11H 109.5 . . ? H11G C116 H11H 109.5 . . ? C114 C116 H11I 109.5 . . ? H11G C116 H11I 109.5 . . ? H11H C116 H11I 109.5 . . ? C114 C117 H11J 109.5 . . ? C114 C117 H11K 109.5 . . ? H11J C117 H11K 109.5 . . ? C114 C117 H11L 109.5 . . ? H11J C117 H11L 109.5 . . ? H11K C117 H11L 109.5 . . ? C121 C118 C119 107.6(3) . . ? C121 C118 C111 112.4(3) . . ? C119 C118 C111 110.5(2) . . ? C121 C118 C120 108.7(3) . . ? C119 C118 C120 108.3(3) . . ? C111 C118 C120 109.3(2) . . ? C118 C119 H11M 109.5 . . ? C118 C119 H11N 109.5 . . ? H11M C119 H11N 109.5 . . ? C118 C119 H11O 109.5 . . ? H11M C119 H11O 109.5 . . ? H11N C119 H11O 109.5 . . ? C118 C120 H12D 109.5 . . ? C118 C120 H12E 109.5 . . ? H12D C120 H12E 109.5 . . ? C118 C120 H12F 109.5 . . ? H12D C120 H12F 109.5 . . ? H12E C120 H12F 109.5 . . ? C118 C121 H12G 109.5 . . ? C118 C121 H12H 109.5 . . ? H12G C121 H12H 109.5 . . ? C118 C121 H12I 109.5 . . ? H12G C121 H12I 109.5 . . ? H12H C121 H12I 109.5 . . ? C153 O122 P123 114.99(17) . . ? O168 P123 O122 109.94(10) . . ? O168 P123 O125 99.38(10) . . ? O122 P123 O125 86.00(9) . . ? O168 P123 N140 114.42(11) . . ? O122 P123 N140 135.65(10) . . ? O125 P123 N140 86.69(10) . . ? O168 P123 N147 100.93(11) . . ? O122 P123 N147 87.11(10) . . ? O125 P123 N147 159.69(10) . . ? N140 P123 N147 84.94(11) . . ? O168 P123 K40 42.40(7) . . ? O122 P123 K40 136.94(7) . . ? O125 P123 K40 124.32(7) . . ? N140 P123 K40 80.98(8) . . ? N147 P123 K40 72.46(7) . . ? O168 P123 K124 41.16(7) . . ? O122 P123 K124 113.31(7) . . ? O125 P123 K124 59.49(7) . . ? N140 P123 K124 100.02(8) . . ? N147 P123 K124 140.37(8) . . ? K40 P123 K124 69.635(18) . . ? O168 P123 K170 34.51(7) . . ? O122 P123 K170 77.34(7) . . ? O125 P123 K170 108.57(7) . . ? N140 P123 K170 145.67(8) . . ? N147 P123 K170 88.46(8) . . ? K40 P123 K170 64.937(17) . . ? K124 P123 K170 65.363(17) . . ? O168 K124 O41 80.41(6) . . ? O168 K124 O169 81.58(6) . . ? O41 K124 O169 80.73(6) . . ? O168 K124 O125 50.12(5) . . ? O41 K124 O125 118.07(6) . . ? O169 K124 O125 118.24(6) . . ? O168 K124 C135 103.38(6) . . ? O41 K124 C135 151.80(7) . . ? O169 K124 C135 127.40(7) . . ? O125 K124 C135 54.37(6) . . ? O168 K124 C18 123.67(7) . . ? O41 K124 C18 64.67(6) . . ? O169 K124 C18 129.69(6) . . ? O125 K124 C18 110.18(6) . . ? C135 K124 C18 91.34(7) . . ? O168 K124 P123 22.08(4) . . ? O41 K124 P123 94.78(4) . . ? O169 K124 P123 100.38(4) . . ? O125 K124 P123 28.55(4) . . ? C135 K124 P123 82.78(5) . . ? C18 K124 P123 117.08(5) . . ? O168 K124 P1 91.76(4) . . ? O41 K124 P1 21.18(4) . . ? O169 K124 P1 100.05(4) . . ? O125 K124 P1 115.05(4) . . ? C135 K124 P1 131.49(6) . . ? C18 K124 P1 44.20(5) . . ? P123 K124 P1 99.72(2) . . ? O168 K124 P83 98.10(4) . . ? O41 K124 P83 94.45(4) . . ? O169 K124 P83 19.96(4) . . ? O125 K124 P83 123.27(4) . . ? C135 K124 P83 112.32(5) . . ? C18 K124 P83 125.96(5) . . ? P123 K124 P83 113.73(2) . . ? P1 K124 P83 110.64(2) . . ? O168 K124 K170 41.49(4) . . ? O41 K124 K170 84.65(4) . . ? O169 K124 K170 41.11(4) . . ? O125 K124 K170 80.17(4) . . ? C135 K124 K170 116.97(6) . . ? C18 K124 K170 149.11(5) . . ? P123 K124 K170 59.273(17) . . ? P1 K124 K170 104.91(2) . . ? P83 K124 K170 56.609(16) . . ? O168 K124 K81 85.45(4) . . ? O41 K124 K81 40.39(4) . . ? O169 K124 K81 41.44(4) . . ? O125 K124 K81 135.57(4) . . ? C135 K124 K81 165.32(5) . . ? C18 K124 K81 93.41(5) . . ? P123 K124 K81 107.21(2) . . ? P1 K124 K81 58.656(17) . . ? P83 K124 K81 54.135(16) . . ? K170 K124 K81 62.436(15) . . ? O168 K124 K40 39.78(4) . . ? O41 K124 K40 40.79(4) . . ? O169 K124 K40 81.20(4) . . ? O125 K124 K40 81.75(4) . . ? C135 K124 K40 134.46(5) . . ? C18 K124 K40 93.33(5) . . ? P123 K124 K40 55.078(16) . . ? P1 K124 K40 53.264(16) . . ? P83 K124 K40 101.054(19) . . ? K170 K124 K40 58.475(15) . . ? K81 K124 K40 59.102(14) . . ? C126 O125 P123 115.28(16) . . ? C126 O125 K124 110.06(14) . . ? P123 O125 K124 91.96(7) . . ? O125 C126 C127 125.0(2) . . ? O125 C126 C131 112.5(2) . . ? C127 C126 C131 122.4(2) . . ? C126 C127 C128 115.1(3) . . ? C126 C127 C132 122.2(2) . . ? C128 C127 C132 122.5(2) . . ? C129 C128 C127 124.0(3) . . ? C129 C128 H128 118.0 . . ? C127 C128 H128 118.0 . . ? C128 C129 C130 118.7(3) . . ? C128 C129 C136 119.1(2) . . ? C130 C129 C136 122.1(3) . . ? C131 C130 C129 118.5(3) . . ? C131 C130 H130 120.8 . . ? C129 C130 H130 120.8 . . ? C130 C131 C126 121.0(2) . . ? C130 C131 N140 130.0(2) . . ? C126 C131 N140 108.6(2) . . ? C133 C132 C135 107.2(3) . . ? C133 C132 C134 109.5(3) . . ? C135 C132 C134 109.6(3) . . ? C133 C132 C127 111.7(3) . . ? C135 C132 C127 110.8(2) . . ? C134 C132 C127 107.9(2) . . ? C132 C133 H13A 109.5 . . ? C132 C133 H13B 109.5 . . ? H13A C133 H13B 109.5 . . ? C132 C133 H13C 109.5 . . ? H13A C133 H13C 109.5 . . ? H13B C133 H13C 109.5 . . ? C132 C134 H13D 109.5 . . ? C132 C134 H13E 109.5 . . ? H13D C134 H13E 109.5 . . ? C132 C134 H13F 109.5 . . ? H13D C134 H13F 109.5 . . ? H13E C134 H13F 109.5 . . ? C132 C135 K124 128.02(18) . . ? C132 C135 H13G 109.5 . . ? K124 C135 H13G 121.6 . . ? C132 C135 H13H 109.5 . . ? K124 C135 H13H 63.6 . . ? H13G C135 H13H 109.5 . . ? C132 C135 H13I 109.5 . . ? K124 C135 H13I 46.0 . . ? H13G C135 H13I 109.5 . . ? H13H C135 H13I 109.5 . . ? C138 C136 C139 107.6(2) . . ? C138 C136 C137 108.4(3) . . ? C139 C136 C137 110.2(3) . . ? C138 C136 C129 112.5(2) . . ? C139 C136 C129 108.4(2) . . ? C137 C136 C129 109.6(2) . . ? C136 C137 H13J 109.5 . . ? C136 C137 H13K 109.5 . . ? H13J C137 H13K 109.5 . . ? C136 C137 H13L 109.5 . . ? H13J C137 H13L 109.5 . . ? H13K C137 H13L 109.5 . . ? C136 C138 H13M 109.5 . . ? C136 C138 H13N 109.5 . . ? H13M C138 H13N 109.5 . . ? C136 C138 H13O 109.5 . . ? H13M C138 H13O 109.5 . . ? H13N C138 H13O 109.5 . . ? C136 C139 H13P 109.5 . . ? C136 C139 H13Q 109.5 . . ? H13P C139 H13Q 109.5 . . ? C136 C139 H13R 109.5 . . ? H13P C139 H13R 109.5 . . ? H13Q C139 H13R 109.5 . . ? C131 N140 C141 128.3(2) . . ? C131 N140 P123 115.66(17) . . ? C141 N140 P123 115.27(18) . . ? C142 C141 N140 128.5(3) . . ? C142 C141 C146 120.4(3) . . ? N140 C141 C146 110.8(2) . . ? C142 C141 K40 100.44(17) . . ? N140 C141 K40 89.92(14) . . ? C146 C141 K40 72.15(15) . . ? C141 C142 C143 118.9(3) . . ? C141 C142 H142 120.6 . . ? C143 C142 H142 120.6 . . ? C144 C143 C142 120.7(3) . . ? C144 C143 H143 119.6 . . ? C142 C143 H143 119.6 . . ? C143 C144 C145 121.0(3) . . ? C143 C144 H144 119.5 . . ? C145 C144 H144 119.5 . . ? C146 C145 C144 118.8(3) . . ? C146 C145 H145 120.6 . . ? C144 C145 H145 120.6 . . ? C145 C146 N147 130.0(3) . . ? C145 C146 C141 120.1(2) . . ? N147 C146 C141 109.8(2) . . ? C145 C146 K40 96.29(17) . . ? N147 C146 K40 85.61(15) . . ? C141 C146 K40 83.82(15) . . ? C148 N147 C146 130.8(2) . . ? C148 N147 P123 113.67(18) . . ? C146 N147 P123 114.34(18) . . ? C149 C148 N147 131.1(3) . . ? C149 C148 C153 120.6(3) . . ? N147 C148 C153 108.3(2) . . ? C148 C149 C150 119.3(3) . . ? C148 C149 H149 120.3 . . ? C150 C149 H149 120.3 . . ? C151 C150 C149 118.5(3) . . ? C151 C150 C158 120.8(3) . . ? C149 C150 C158 120.6(3) . . ? C150 C151 C152 124.0(3) . . ? C150 C151 H151 118.0 . . ? C152 C151 H151 118.0 . . ? C153 C152 C151 114.9(3) . . ? C153 C152 C154 121.8(3) . . ? C151 C152 C154 123.3(3) . . ? O122 C153 C152 123.8(3) . . ? O122 C153 C148 113.5(2) . . ? C152 C153 C148 122.6(3) . . ? C152 C154 C156 112.0(3) . . ? C152 C154 C157 109.9(2) . . ? C156 C154 C157 108.2(2) . . ? C152 C154 C155 110.0(2) . . ? C156 C154 C155 107.6(2) . . ? C157 C154 C155 109.0(3) . . ? C154 C155 H15D 109.5 . . ? C154 C155 H15E 109.5 . . ? H15D C155 H15E 109.5 . . ? C154 C155 H15F 109.5 . . ? H15D C155 H15F 109.5 . . ? H15E C155 H15F 109.5 . . ? C154 C156 H15G 109.5 . . ? C154 C156 H15H 109.5 . . ? H15G C156 H15H 109.5 . . ? C154 C156 H15I 109.5 . . ? H15G C156 H15I 109.5 . . ? H15H C156 H15I 109.5 . . ? C154 C157 H15J 109.5 . . ? C154 C157 H15K 109.5 . . ? H15J C157 H15K 109.5 . . ? C154 C157 H15L 109.5 . . ? H15J C157 H15L 109.5 . . ? H15K C157 H15L 109.5 . . ? C163 C162 H16D 109.5 . . ? C163 C162 H16E 109.5 . . ? H16D C162 H16E 109.5 . . ? C163 C162 H16F 109.5 . . ? H16D C162 H16F 109.5 . . ? H16E C162 H16F 109.5 . . ? C162 C163 C164 114.8(4) . . ? C162 C163 H16G 108.6 . . ? C164 C163 H16G 108.6 . . ? C162 C163 H16H 108.6 . . ? C164 C163 H16H 108.6 . . ? H16G C163 H16H 107.6 . . ? C165 C164 C163 115.2(4) . . ? C165 C164 H16I 108.5 . . ? C163 C164 H16I 108.5 . . ? C165 C164 H16J 108.5 . . ? C163 C164 H16J 108.5 . . ? H16I C164 H16J 107.5 . . ? C166 C165 C164 116.1(4) . . ? C166 C165 H16K 108.3 . . ? C164 C165 H16K 108.3 . . ? C166 C165 H16L 108.3 . . ? C164 C165 H16L 108.3 . . ? H16K C165 H16L 107.4 . . ? C165 C166 C167 114.0(4) . . ? C165 C166 H16M 108.7 . . ? C167 C166 H16M 108.7 . . ? C165 C166 H16N 108.7 . . ? C167 C166 H16N 108.7 . . ? H16M C166 H16N 107.6 . . ? C166 C167 H16O 109.5 . . ? C166 C167 H16P 109.5 . . ? H16O C167 H16P 109.5 . . ? C166 C167 H16Q 109.5 . . ? H16O C167 H16Q 109.5 . . ? H16P C167 H16Q 109.5 . . ? P123 O168 K124 116.76(10) . . ? P123 O168 K170 126.62(10) . . ? K124 O168 K170 97.04(6) . . ? P123 O168 K40 115.14(10) . . ? K124 O168 K40 100.81(6) . . ? K170 O168 K40 95.65(6) . . ? P83 O169 K170 121.63(10) . . ? P83 O169 K81 112.07(9) . . ? K170 O169 K81 102.57(6) . . ? P83 O169 K124 122.70(10) . . ? K170 O169 K124 96.73(6) . . ? K81 O169 K124 96.78(6) . . ? O169 K170 O168 82.58(6) . . ? O169 K170 O82 79.62(6) . . ? O168 K170 O82 82.80(6) . . ? O169 K170 O72 112.28(6) . . ? O168 K170 O72 125.76(6) . . ? O82 K170 O72 52.32(5) . . ? O169 K170 C78 144.25(7) . . ? O168 K170 C78 132.64(7) . . ? O82 K170 C78 107.05(7) . . ? O72 K170 C78 56.48(6) . . ? O169 K170 P42 91.10(4) . . ? O168 K170 P42 104.74(4) . . ? O82 K170 P42 23.61(4) . . ? O72 K170 P42 29.40(4) . . ? C78 K170 P42 85.65(6) . . ? O169 K170 P83 20.60(4) . . ? O168 K170 P83 99.73(4) . . ? O82 K170 P83 93.02(4) . . ? O72 K170 P83 110.11(4) . . ? C78 K170 P83 124.98(6) . . ? P42 K170 P83 97.63(2) . . ? O169 K170 P123 97.52(4) . . ? O168 K170 P123 18.87(4) . . ? O82 K170 P123 96.77(4) . . ? O72 K170 P123 128.63(4) . . ? C78 K170 P123 115.91(6) . . ? P42 K170 P123 115.88(2) . . ? P83 K170 P123 111.57(2) . . ? O169 K170 K40 84.96(4) . . ? O168 K170 K40 42.37(4) . . ? O82 K170 K40 41.36(4) . . ? O72 K170 K40 85.59(4) . . ? C78 K170 K40 123.73(6) . . ? P42 K170 K40 62.391(18) . . ? P83 K170 K40 105.31(2) . . ? P123 K170 K40 55.446(16) . . ? O169 K170 K124 42.16(4) . . ? O168 K170 K124 41.47(4) . . ? O82 K170 K124 85.55(4) . . ? O72 K170 K124 137.06(4) . . ? C78 K170 K124 166.14(5) . . ? P42 K170 K124 107.71(2) . . ? P83 K170 K124 58.269(16) . . ? P123 K170 K124 55.364(16) . . ? K40 K170 K124 62.391(16) . . ? O169 K170 K81 39.03(4) . . ? O168 K170 K81 82.77(4) . . ? O82 K170 K81 40.70(4) . . ? O72 K170 K81 80.53(4) . . ? C78 K170 K81 134.55(5) . . ? P42 K170 K81 54.062(16) . . ? P83 K170 K81 53.375(16) . . ? P123 K170 K81 101.631(19) . . ? K40 K170 K81 59.259(15) . . ? K124 K170 K81 59.120(14) . . ? 160C C158 159C 113.6(8) . . ? 159A C158 161A 107.2(7) . . ? 160C C158 C150 106.8(5) . . ? 159C C158 C150 105.6(6) . . ? 160B C158 C150 114.7(5) . . ? 159A C158 C150 113.7(5) . . ? 161A C158 C150 111.9(5) . . ? 160B C158 161B 109.6(7) . . ? C150 C158 161B 110.8(5) . . ? 160C C158 161C 109.8(8) . . ? 159C C158 161C 111.7(8) . . ? C150 C158 161C 109.2(6) . . ? 160B C158 159B 109.9(7) . . ? C150 C158 159B 105.2(4) . . ? 161B C158 159B 106.3(7) . . ? 159A C158 160A 104.1(6) . . ? 161A C158 160A 103.7(6) . . ? C150 C158 160A 115.2(4) . . ? C158 160A H16R 109.5 . . ? C158 160A H16S 109.5 . . ? H16R 160A H16S 109.5 . . ? C158 160A H16T 109.5 . . ? H16R 160A H16T 109.5 . . ? H16S 160A H16T 109.5 . . ? C158 159A H15M 109.5 . . ? C158 159A H15N 109.5 . . ? H15M 159A H15N 109.5 . . ? C158 159A H15O 109.5 . . ? H15M 159A H15O 109.5 . . ? H15N 159A H15O 109.5 . . ? C158 161A H16U 109.5 . . ? C158 161A H16V 109.5 . . ? H16U 161A H16V 109.5 . . ? C158 161A H16W 109.5 . . ? H16U 161A H16W 109.5 . . ? H16V 161A H16W 109.5 . . ? C158 160B H16X 109.5 . . ? C158 160B H16Y 109.5 . . ? H16X 160B H16Y 109.5 . . ? C158 160B H16Z 109.5 . . ? H16X 160B H16Z 109.5 . . ? H16Y 160B H16Z 109.5 . . ? C158 159B H15P 109.5 . . ? C158 159B H15Q 109.5 . . ? H15P 159B H15Q 109.5 . . ? C158 159B H15R 109.5 . . ? H15P 159B H15R 109.5 . . ? H15Q 159B H15R 109.5 . . ? C158 161B H111 109.5 . . ? C158 161B H112 109.5 . . ? H111 161B H112 109.5 . . ? C158 161B H113 109.5 . . ? H111 161B H113 109.5 . . ? H112 161B H113 109.5 . . ? C158 159C H15S 109.5 . . ? C158 159C H15T 109.5 . . ? H15S 159C H15T 109.5 . . ? C158 159C H15U 109.5 . . ? H15S 159C H15U 109.5 . . ? H15T 159C H15U 109.5 . . ? C158 161C H114 109.5 . . ? C158 161C H115 109.5 . . ? H114 161C H115 109.5 . . ? C158 161C H116 109.5 . . ? H114 161C H116 109.5 . . ? H115 161C H116 109.5 . . ? C158 160C H117 109.5 . . ? C158 160C H118 109.5 . . ? H117 160C H118 109.5 . . ? C158 160C H119 109.5 . . ? H117 160C H119 109.5 . . ? H118 160C H119 109.5 . . ? _refine_diff_density_max 0.699 _refine_diff_density_min -0.489 _refine_diff_density_rms 0.061 _shelx_res_file ; TITL rom219_0m_a.res in P2(1)/n rom219_sq.res created by SHELXL-2018/1 at 14:45:41 on 24-Nov-2021 REM Old TITL rom219_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.176, Rweak 0.011, Alpha 0.041, Orientation as input REM Formula found by SHELXT: C303 K8 N16 O24 P8 CELL 0.71073 17.4664 33.4388 26.6896 90.000 97.222 90.000 ZERR 4.000 0.0008 0.0014 0.0012 0.000 0.001 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H K N O P UNIT 568 760 16 32 48 16 LIST 4 TEMP -163.000 SIZE 0.136 0.149 0.496 ACTA L.S. 10 0 110 OMIT -2 1 1 OMIT 0 1 1 OMIT -2 6 6 OMIT 3 3 2 OMIT 3 1 2 OMIT 1 3 2 OMIT -1 6 7 OMIT -1 12 3 OMIT 0 1 4 OMIT 14 30 3 OMIT -20 6 14 OMIT 3 9 0 OMIT -3 1 2 OMIT -1 5 4 OMIT -21 5 8 BOND $H FMAP 2 PLAN 20 ABIN WGHT 0.064700 12.648701 FVAR 0.19161 P1 6 0.611148 0.601699 0.802391 11.00000 0.02924 0.02497 = 0.02740 -0.00244 0.00736 -0.00137 O2 5 0.589508 0.555619 0.782900 11.00000 0.02894 0.02556 = 0.03114 -0.00328 0.00620 -0.00093 C3 1 0.511613 0.546581 0.775527 11.00000 0.02836 0.02732 = 0.02674 0.00235 0.00421 -0.00049 C4 1 0.482104 0.511224 0.753843 11.00000 0.03690 0.02230 = 0.02527 0.00215 0.00336 -0.00106 C5 1 0.401707 0.506787 0.751755 11.00000 0.03808 0.02840 = 0.03003 -0.00201 0.00152 -0.00596 AFIX 43 H5 2 0.378804 0.483036 0.737207 11.00000 -1.20000 AFIX 0 C7 1 0.386917 0.570134 0.791421 11.00000 0.03035 0.03154 = 0.04641 -0.00304 0.00890 -0.00123 AFIX 43 H7 2 0.355481 0.589977 0.804079 11.00000 -1.20000 AFIX 0 C6 1 0.353886 0.535144 0.769747 11.00000 0.03304 0.03455 = 0.04136 -0.00049 0.00770 -0.00477 C8 1 0.465964 0.575597 0.794267 11.00000 0.03217 0.02543 = 0.03163 0.00014 0.00841 -0.00283 C9 1 0.534120 0.479056 0.735307 11.00000 0.03940 0.02630 = 0.03243 -0.00370 0.00294 0.00217 C10 1 0.582995 0.496711 0.697032 11.00000 0.04982 0.03761 = 0.03671 -0.00406 0.01064 0.00709 AFIX 137 H10A 2 0.614662 0.475587 0.684634 11.00000 -1.50000 H10B 2 0.616593 0.517674 0.713310 11.00000 -1.50000 H10C 2 0.549041 0.508183 0.668632 11.00000 -1.50000 AFIX 0 C11 1 0.487447 0.444337 0.709851 11.00000 0.05289 0.03305 = 0.05037 -0.01326 0.00485 -0.00094 AFIX 137 H11A 2 0.452688 0.454377 0.680900 11.00000 -1.50000 H11B 2 0.457081 0.431840 0.734081 11.00000 -1.50000 H11C 2 0.522638 0.424528 0.698245 11.00000 -1.50000 AFIX 0 C12 1 0.587401 0.462216 0.780865 11.00000 0.05223 0.03368 = 0.04511 0.00000 0.00125 0.00815 AFIX 137 H12A 2 0.619634 0.440918 0.769435 11.00000 -1.50000 H12B 2 0.555988 0.451374 0.805626 11.00000 -1.50000 H12C 2 0.620449 0.483652 0.796492 11.00000 -1.50000 AFIX 0 C13 1 0.266950 0.527101 0.768623 11.00000 0.03397 0.04076 = 0.06665 -0.00719 0.01160 -0.00834 C14 1 0.236808 0.499486 0.725098 11.00000 0.04020 0.09754 = 0.14521 -0.06275 0.01525 -0.02671 AFIX 137 H14A 2 0.180273 0.499085 0.721332 11.00000 -1.50000 H14B 2 0.256587 0.472378 0.732193 11.00000 -1.50000 H14C 2 0.254194 0.509248 0.693799 11.00000 -1.50000 AFIX 0 C15 1 0.253547 0.508630 0.818585 11.00000 0.05170 0.10892 = 0.12599 0.04379 0.03277 -0.01099 AFIX 137 H15A 2 0.198183 0.504099 0.818931 11.00000 -1.50000 H15B 2 0.272743 0.526762 0.846181 11.00000 -1.50000 H15C 2 0.281041 0.483075 0.822978 11.00000 -1.50000 AFIX 0 C16 1 0.221173 0.565777 0.761402 11.00000 0.03073 0.06174 = 0.10175 -0.00853 -0.00011 -0.00466 AFIX 137 H16A 2 0.233862 0.579505 0.731068 11.00000 -1.50000 H16B 2 0.234293 0.583046 0.790899 11.00000 -1.50000 H16C 2 0.165851 0.559717 0.757582 11.00000 -1.50000 AFIX 0 N17 4 0.512804 0.606472 0.814805 11.00000 0.02934 0.02595 = 0.03765 -0.00698 0.01276 -0.00268 C18 1 0.502903 0.631924 0.854800 11.00000 0.04005 0.02348 = 0.03737 -0.00316 0.01667 -0.00320 C19 1 0.435976 0.647779 0.869445 11.00000 0.03653 0.03131 = 0.05000 -0.00211 0.01494 0.00113 AFIX 43 H19 2 0.386958 0.640731 0.852138 11.00000 -1.20000 AFIX 0 C20 1 0.441814 0.674269 0.910040 11.00000 0.04871 0.03540 = 0.05880 -0.00926 0.02682 0.00513 AFIX 43 H20 2 0.396086 0.684693 0.920942 11.00000 -1.20000 AFIX 0 C21 1 0.512319 0.685643 0.934654 11.00000 0.05810 0.03616 = 0.05009 -0.01194 0.02356 -0.00022 AFIX 43 H21 2 0.514880 0.704498 0.961438 11.00000 -1.20000 AFIX 0 C23 1 0.574862 0.642237 0.881606 11.00000 0.03891 0.02610 = 0.03223 -0.00189 0.01523 -0.00355 C22 1 0.579604 0.669740 0.920579 11.00000 0.04455 0.02858 = 0.03888 -0.00819 0.01456 -0.00605 AFIX 43 H22 2 0.628406 0.677614 0.937469 11.00000 -1.20000 AFIX 0 N24 4 0.635209 0.622954 0.861596 11.00000 0.03153 0.02899 = 0.02887 -0.00595 0.00890 -0.00203 C25 1 0.705580 0.610246 0.887233 11.00000 0.03623 0.02302 = 0.02874 -0.00087 0.00780 -0.00454 C26 1 0.733146 0.613017 0.938164 11.00000 0.05158 0.02760 = 0.02765 -0.00199 0.00941 -0.00384 AFIX 43 H26 2 0.704325 0.626577 0.960857 11.00000 -1.20000 AFIX 0 C27 1 0.804382 0.595403 0.955464 11.00000 0.05973 0.02876 = 0.02722 0.00020 -0.00034 -0.00147 C29 1 0.817631 0.571653 0.869474 11.00000 0.03988 0.02591 = 0.03255 -0.00226 0.00173 -0.00084 C28 1 0.845127 0.576002 0.921184 11.00000 0.04713 0.03117 = 0.03682 0.00151 -0.00509 0.00345 AFIX 43 H28 2 0.894202 0.565060 0.933214 11.00000 -1.20000 AFIX 0 C30 1 0.745912 0.588941 0.854368 11.00000 0.03621 0.02707 = 0.02304 -0.00061 0.00226 -0.00373 O31 5 0.706105 0.586345 0.806958 11.00000 0.02987 0.03230 = 0.02496 -0.00335 0.00254 0.00186 C32 1 0.832820 0.596373 1.012616 11.00000 0.08033 0.04139 = 0.02734 -0.00120 -0.00734 0.00554 C33 1 0.828698 0.638973 1.032142 11.00000 0.08027 0.04647 = 0.03361 -0.00636 -0.01141 0.00182 AFIX 137 H33A 2 0.860340 0.656493 1.013664 11.00000 -1.50000 H33B 2 0.848077 0.639667 1.068221 11.00000 -1.50000 H33C 2 0.775023 0.648195 1.027117 11.00000 -1.50000 AFIX 0 C34 1 0.779464 0.569094 1.039638 11.00000 0.13204 0.05590 = 0.02943 0.00848 0.00413 -0.01356 AFIX 137 H34A 2 0.726237 0.578835 1.032997 11.00000 -1.50000 H34B 2 0.796213 0.569467 1.076084 11.00000 -1.50000 H34C 2 0.782117 0.541687 1.026964 11.00000 -1.50000 AFIX 0 C35 1 0.915512 0.581930 1.024390 11.00000 0.09891 0.06768 = 0.04270 -0.00894 -0.02478 0.02411 AFIX 137 H35A 2 0.918692 0.553853 1.014328 11.00000 -1.50000 H35B 2 0.932133 0.584445 1.060712 11.00000 -1.50000 H35C 2 0.949099 0.598167 1.005731 11.00000 -1.50000 AFIX 0 C36 1 0.860646 0.548337 0.832450 11.00000 0.03610 0.03547 = 0.03870 -0.00523 -0.00066 0.00821 C37 1 0.813575 0.510741 0.815226 11.00000 0.05335 0.03442 = 0.05049 -0.00663 0.00876 0.00645 AFIX 137 H37A 2 0.762535 0.518707 0.798756 11.00000 -1.50000 H37B 2 0.807682 0.493992 0.844628 11.00000 -1.50000 H37C 2 0.840561 0.495606 0.791337 11.00000 -1.50000 AFIX 0 C38 1 0.941356 0.535424 0.857355 11.00000 0.04903 0.06376 = 0.05141 -0.00858 -0.00219 0.01875 AFIX 137 H38A 2 0.967748 0.520719 0.832782 11.00000 -1.50000 H38B 2 0.936045 0.518174 0.886401 11.00000 -1.50000 H38C 2 0.971546 0.559176 0.868701 11.00000 -1.50000 AFIX 0 C39 1 0.871508 0.573777 0.786166 11.00000 0.04158 0.03712 = 0.04189 -0.00250 0.01127 0.00320 AFIX 1 H39C 2 0.914700 0.560100 0.763600 11.00000 -1.50000 H39B 2 0.818100 0.575800 0.761900 11.00000 -1.50000 H39A 2 0.891700 0.601900 0.795700 11.00000 -1.50000 AFIX 0 K40 3 0.758648 0.653318 0.754393 11.00000 0.02881 0.02812 = 0.03283 -0.00093 -0.00008 -0.00100 O41 5 0.611621 0.629869 0.758793 11.00000 0.03162 0.02556 = 0.02993 0.00143 0.00656 -0.00171 P42 6 0.743282 0.640293 0.609571 11.00000 0.02117 0.02836 = 0.03020 -0.00561 0.00692 -0.00158 C45 1 0.950613 0.597381 0.643715 11.00000 0.02279 0.04343 = 0.05248 -0.01352 0.00783 0.00167 C44 1 0.871926 0.602955 0.632229 11.00000 0.02380 0.03258 = 0.03869 -0.00999 0.00778 0.00344 O43 5 0.838625 0.639156 0.616233 11.00000 0.02139 0.02959 = 0.04770 -0.00717 0.00723 -0.00181 C46 1 0.973343 0.558276 0.656498 11.00000 0.01966 0.04938 = 0.05016 -0.01184 0.00282 0.00332 AFIX 43 H46 2 1.026847 0.553212 0.665379 11.00000 -1.20000 AFIX 0 C47 1 0.922736 0.526360 0.657047 11.00000 0.02627 0.03970 = 0.03574 -0.00798 0.00553 0.00594 C49 1 0.819283 0.571994 0.631762 11.00000 0.02191 0.03474 = 0.02852 -0.00597 0.00479 0.00199 C48 1 0.844015 0.533473 0.644566 11.00000 0.02660 0.03257 = 0.03490 -0.00206 0.00455 0.00063 AFIX 43 H48 2 0.807854 0.512275 0.644822 11.00000 -1.20000 AFIX 0 C50 1 1.008058 0.631890 0.640328 11.00000 0.02265 0.04706 = 0.10615 -0.01658 0.00893 -0.00226 C51 1 0.994167 0.662857 0.680941 11.00000 0.03667 0.05637 = 0.15166 -0.03914 -0.00235 -0.00908 AFIX 137 H51A 2 1.028868 0.685682 0.679007 11.00000 -1.50000 H51B 2 1.004293 0.650546 0.714441 11.00000 -1.50000 H51C 2 0.940501 0.672048 0.675217 11.00000 -1.50000 AFIX 0 C52 1 0.996657 0.650440 0.587552 11.00000 0.04695 0.08184 = 0.13557 0.03392 0.03586 -0.00428 AFIX 137 H52A 2 1.005852 0.630129 0.562520 11.00000 -1.50000 H52B 2 1.033077 0.672577 0.586081 11.00000 -1.50000 H52C 2 0.943737 0.660504 0.580231 11.00000 -1.50000 AFIX 0 C53 1 1.091488 0.617154 0.649928 11.00000 0.02882 0.05705 = 0.14757 -0.01604 0.00616 -0.00642 AFIX 137 H53A 2 1.099174 0.595635 0.626137 11.00000 -1.50000 H53B 2 1.102164 0.607065 0.684576 11.00000 -1.50000 H53C 2 1.126596 0.639317 0.645223 11.00000 -1.50000 AFIX 0 C54 1 0.954314 0.484347 0.671088 11.00000 0.03513 0.04115 = 0.04934 -0.00315 0.00434 0.00963 C55 1 0.993399 0.484357 0.726244 11.00000 0.05562 0.07115 = 0.04832 0.00140 -0.00118 0.02365 AFIX 137 H55A 2 1.016167 0.458021 0.734525 11.00000 -1.50000 H55B 2 0.954881 0.490291 0.748912 11.00000 -1.50000 H55C 2 1.033976 0.504763 0.730328 11.00000 -1.50000 AFIX 0 C56 1 1.015472 0.472888 0.637779 11.00000 0.05160 0.04972 = 0.06405 -0.00940 0.01496 0.01620 AFIX 137 H56A 2 0.992691 0.473066 0.602297 11.00000 -1.50000 H56B 2 1.035066 0.446065 0.646942 11.00000 -1.50000 H56C 2 1.058035 0.492157 0.642652 11.00000 -1.50000 AFIX 0 C57 1 0.891225 0.452966 0.666618 11.00000 0.04793 0.03964 = 0.08630 0.00614 0.00313 0.01199 AFIX 137 H57A 2 0.867876 0.450975 0.631347 11.00000 -1.50000 H57B 2 0.851655 0.460577 0.687802 11.00000 -1.50000 H57C 2 0.913347 0.427053 0.677813 11.00000 -1.50000 AFIX 0 N58 4 0.745771 0.586654 0.615478 11.00000 0.02071 0.02808 = 0.03204 -0.00296 0.00286 -0.00068 C59 1 0.683492 0.566897 0.588796 11.00000 0.02079 0.02759 = 0.02588 -0.00404 0.00499 0.00004 C60 1 0.660038 0.527517 0.591117 11.00000 0.02828 0.02683 = 0.03081 0.00070 0.00023 0.00155 AFIX 43 H60 2 0.689712 0.508916 0.612338 11.00000 -1.20000 AFIX 0 C61 1 0.592167 0.515532 0.561831 11.00000 0.03323 0.02263 = 0.03542 -0.00036 0.00205 -0.00222 AFIX 43 H61 2 0.576400 0.488369 0.562534 11.00000 -1.20000 AFIX 0 C62 1 0.547369 0.542584 0.531737 11.00000 0.02560 0.03095 = 0.03019 -0.00414 -0.00087 -0.00179 AFIX 43 H62 2 0.500581 0.533942 0.512821 11.00000 -1.20000 AFIX 0 C63 1 0.570178 0.582231 0.528940 11.00000 0.02705 0.02866 = 0.02411 -0.00055 0.00362 0.00058 AFIX 43 H63 2 0.539242 0.600935 0.508663 11.00000 -1.20000 AFIX 0 C64 1 0.639185 0.593815 0.556467 11.00000 0.02474 0.02414 = 0.02542 -0.00364 0.01061 -0.00059 N65 4 0.671592 0.632216 0.559347 11.00000 0.02594 0.02473 = 0.02718 -0.00098 0.00558 -0.00159 C66 1 0.671805 0.659166 0.519068 11.00000 0.02830 0.02652 = 0.02902 0.00119 0.01347 -0.00069 C67 1 0.639702 0.654906 0.469519 11.00000 0.03529 0.02852 = 0.02852 -0.00192 0.01173 -0.00132 AFIX 43 H67 2 0.608133 0.632504 0.459232 11.00000 -1.20000 AFIX 0 C68 1 0.654540 0.684222 0.434702 11.00000 0.04494 0.03338 = 0.03165 -0.00147 0.01782 0.00083 C69 1 0.699035 0.717160 0.451969 11.00000 0.05825 0.03353 = 0.03756 0.00308 0.02817 -0.00490 AFIX 43 H69 2 0.706744 0.737615 0.428415 11.00000 -1.20000 AFIX 0 C70 1 0.733100 0.721932 0.501986 11.00000 0.04215 0.03173 = 0.04109 -0.00287 0.02255 -0.00681 C71 1 0.719196 0.691217 0.534731 11.00000 0.03187 0.03005 = 0.03027 -0.00252 0.01364 -0.00040 O72 5 0.752303 0.687360 0.583914 11.00000 0.03187 0.02905 = 0.03366 -0.00488 0.00706 -0.00621 C73 1 0.625703 0.680152 0.378179 11.00000 0.06876 0.04165 = 0.02670 0.00349 0.01797 -0.00045 C74 1 0.574929 0.643165 0.367059 11.00000 0.08461 0.05328 = 0.02472 -0.00081 0.00285 -0.00663 AFIX 137 H74A 2 0.554409 0.642742 0.331159 11.00000 -1.50000 H74B 2 0.532090 0.644015 0.387484 11.00000 -1.50000 H74C 2 0.605745 0.619032 0.375407 11.00000 -1.50000 AFIX 0 C75 1 0.696654 0.675638 0.349649 11.00000 0.08959 0.06738 = 0.03412 0.00423 0.03397 0.00289 AFIX 137 H75A 2 0.679633 0.673260 0.313360 11.00000 -1.50000 H75B 2 0.725528 0.651609 0.361539 11.00000 -1.50000 H75C 2 0.729915 0.699174 0.355910 11.00000 -1.50000 AFIX 0 C76 1 0.578865 0.717030 0.359107 11.00000 0.08889 0.04808 = 0.03602 0.00671 0.01085 0.00510 AFIX 137 H76A 2 0.560761 0.713898 0.323053 11.00000 -1.50000 H76B 2 0.611449 0.740906 0.364201 11.00000 -1.50000 H76C 2 0.534405 0.719888 0.377860 11.00000 -1.50000 AFIX 0 C77 1 0.786028 0.757313 0.518817 11.00000 0.05814 0.04167 = 0.05545 -0.00936 0.03243 -0.02369 C78 1 0.765668 0.775709 0.567774 11.00000 0.05553 0.03177 = 0.05322 -0.00827 0.02327 -0.01540 AFIX 137 H78A 2 0.794590 0.800636 0.574661 11.00000 -1.50000 H78B 2 0.779133 0.756938 0.595691 11.00000 -1.50000 H78C 2 0.710205 0.781366 0.564406 11.00000 -1.50000 AFIX 0 C79 1 0.778030 0.790694 0.478615 11.00000 0.13327 0.05661 = 0.06913 -0.00259 0.04534 -0.05184 AFIX 137 H79A 2 0.790448 0.779942 0.446444 11.00000 -1.50000 H79B 2 0.813618 0.812549 0.489582 11.00000 -1.50000 H79C 2 0.724942 0.800799 0.474277 11.00000 -1.50000 AFIX 0 C80 1 0.868785 0.741979 0.527141 11.00000 0.05766 0.08253 = 0.11479 -0.04915 0.04535 -0.03358 AFIX 137 H80A 2 0.881770 0.729741 0.495928 11.00000 -1.50000 H80B 2 0.873873 0.722007 0.554228 11.00000 -1.50000 H80C 2 0.903945 0.764324 0.536620 11.00000 -1.50000 AFIX 0 K81 3 0.575572 0.616103 0.662550 11.00000 0.02412 0.03368 = 0.03313 -0.00936 0.00531 -0.00113 O82 5 0.713539 0.652247 0.657566 11.00000 0.02451 0.03266 = 0.03081 -0.00573 0.00734 0.00058 P83 6 0.463088 0.700893 0.628063 11.00000 0.02309 0.02950 = 0.02204 -0.00357 0.00248 -0.00077 O84 5 0.431785 0.652241 0.618261 11.00000 0.02916 0.02802 = 0.02074 -0.00051 0.00203 -0.00011 C85 1 0.412285 0.641964 0.568482 11.00000 0.02386 0.02789 = 0.02042 -0.00113 0.00053 0.00364 C86 1 0.371894 0.607847 0.551488 11.00000 0.02663 0.02438 = 0.02804 0.00173 0.00155 0.00448 C87 1 0.352449 0.605622 0.498821 11.00000 0.03094 0.02456 = 0.02909 -0.00207 -0.00243 0.00169 AFIX 43 H87 2 0.326417 0.582333 0.485282 11.00000 -1.20000 AFIX 0 C88 1 0.368905 0.635399 0.465156 11.00000 0.03246 0.02590 = 0.02384 -0.00142 0.00080 0.00558 C89 1 0.411956 0.668273 0.484124 11.00000 0.03429 0.02486 = 0.02501 0.00112 0.00536 0.00532 AFIX 43 H89 2 0.425647 0.688696 0.462159 11.00000 -1.20000 AFIX 0 C90 1 0.434535 0.670642 0.535842 11.00000 0.02327 0.02510 = 0.02778 -0.00187 0.00418 0.00191 C91 1 0.345267 0.576605 0.587590 11.00000 0.03337 0.03051 = 0.03028 0.00300 0.00081 -0.00206 C92 1 0.279249 0.595021 0.613031 11.00000 0.03309 0.04560 = 0.04828 0.01115 0.00789 -0.00033 AFIX 137 H92A 2 0.236344 0.601940 0.587203 11.00000 -1.50000 H92B 2 0.297773 0.619201 0.631463 11.00000 -1.50000 H92C 2 0.261575 0.575654 0.636633 11.00000 -1.50000 AFIX 0 C93 1 0.410726 0.564517 0.628818 11.00000 0.03623 0.03328 = 0.03216 0.00816 0.00264 0.00101 AFIX 137 H93A 2 0.455958 0.556303 0.613047 11.00000 -1.50000 H93B 2 0.393593 0.542209 0.648464 11.00000 -1.50000 H93C 2 0.424340 0.587337 0.651214 11.00000 -1.50000 AFIX 0 C94 1 0.316707 0.538219 0.559808 11.00000 0.05690 0.03471 = 0.04384 0.00699 -0.00169 -0.01186 AFIX 137 H94A 2 0.271834 0.544365 0.535135 11.00000 -1.50000 H94B 2 0.302060 0.518653 0.584232 11.00000 -1.50000 H94C 2 0.357984 0.527117 0.542308 11.00000 -1.50000 AFIX 0 C95 1 0.334745 0.632454 0.408998 11.00000 0.04096 0.02911 = 0.02540 -0.00411 -0.00316 0.00670 C96 1 0.356881 0.668022 0.377764 11.00000 0.06326 0.03683 = 0.02440 -0.00062 -0.00170 0.01013 AFIX 137 H96A 2 0.335973 0.664093 0.342284 11.00000 -1.50000 H96B 2 0.413226 0.670117 0.380621 11.00000 -1.50000 H96C 2 0.335624 0.692642 0.390378 11.00000 -1.50000 AFIX 0 C97 1 0.246851 0.631511 0.405181 11.00000 0.04689 0.05296 = 0.03163 -0.00465 -0.00822 0.00904 AFIX 137 H97A 2 0.224957 0.628978 0.369673 11.00000 -1.50000 H97B 2 0.228396 0.656313 0.419124 11.00000 -1.50000 H97C 2 0.230759 0.608635 0.424294 11.00000 -1.50000 AFIX 0 C98 1 0.363142 0.594017 0.385861 11.00000 0.06042 0.03674 = 0.02860 -0.00826 -0.00326 0.01059 AFIX 137 H98A 2 0.342422 0.592646 0.350034 11.00000 -1.50000 H98B 2 0.345471 0.570754 0.403569 11.00000 -1.50000 H98C 2 0.419662 0.594113 0.389209 11.00000 -1.50000 AFIX 0 N99 4 0.472022 0.701837 0.564276 11.00000 0.02962 0.02592 = 0.02330 -0.00307 0.00436 -0.00337 C100 1 0.496292 0.738262 0.545741 11.00000 0.02478 0.02845 = 0.02858 -0.00176 0.00429 -0.00400 C101 1 0.525263 0.745370 0.500590 11.00000 0.03622 0.03641 = 0.03558 -0.00468 0.01204 -0.00392 AFIX 43 H101 2 0.530567 0.724086 0.477702 11.00000 -1.20000 AFIX 0 C102 1 0.546402 0.783935 0.489253 11.00000 0.04514 0.03994 = 0.04032 0.00093 0.01719 -0.00803 AFIX 43 H102 2 0.565664 0.789189 0.458169 11.00000 -1.20000 AFIX 0 C103 1 0.539674 0.814841 0.522842 11.00000 0.04216 0.03172 = 0.04868 -0.00071 0.01611 -0.00766 AFIX 43 H103 2 0.553081 0.841259 0.514164 11.00000 -1.20000 AFIX 0 C104 1 0.513552 0.807773 0.569146 11.00000 0.03263 0.03219 = 0.03786 -0.00756 0.00625 -0.01002 AFIX 43 H104 2 0.510823 0.828994 0.592521 11.00000 -1.20000 AFIX 0 C105 1 0.491560 0.769437 0.580789 11.00000 0.02005 0.03153 = 0.03139 -0.00391 0.00352 -0.00191 N106 4 0.466255 0.754432 0.624463 11.00000 0.02485 0.02905 = 0.02457 -0.00454 0.00492 -0.00240 C107 1 0.420742 0.773162 0.656868 11.00000 0.02136 0.03291 = 0.02282 -0.00500 -0.00183 0.00011 C108 1 0.411010 0.813199 0.667742 11.00000 0.02780 0.03220 = 0.02641 -0.00476 -0.00098 -0.00362 AFIX 43 H108 2 0.440713 0.833013 0.653486 11.00000 -1.20000 AFIX 0 C109 1 0.357431 0.824263 0.699696 11.00000 0.02987 0.03125 = 0.02639 -0.00467 -0.00411 0.00238 C110 1 0.316912 0.794273 0.721289 11.00000 0.02617 0.03797 = 0.02942 -0.00712 0.00233 0.00558 AFIX 43 H110 2 0.281601 0.801983 0.743841 11.00000 -1.20000 AFIX 0 C111 1 0.325181 0.753486 0.711704 11.00000 0.02545 0.03477 = 0.02691 -0.00216 0.00150 0.00241 C112 1 0.377713 0.744313 0.678540 11.00000 0.02449 0.02895 = 0.02528 -0.00668 0.00066 0.00249 O113 5 0.389436 0.706018 0.661282 11.00000 0.02651 0.02832 = 0.02694 -0.00358 0.00573 -0.00127 C114 1 0.339580 0.868362 0.709260 11.00000 0.03254 0.03282 = 0.03858 -0.00645 -0.00088 0.00614 C115 1 0.340763 0.876726 0.765789 11.00000 0.09036 0.04029 = 0.04629 -0.01206 0.01732 0.01819 AFIX 137 H11D 2 0.328632 0.904949 0.770782 11.00000 -1.50000 H11E 2 0.392118 0.870698 0.783413 11.00000 -1.50000 H11F 2 0.302295 0.859883 0.779333 11.00000 -1.50000 AFIX 0 C116 1 0.396261 0.896722 0.689081 11.00000 0.06224 0.03151 = 0.05534 -0.01516 0.00967 -0.00321 AFIX 137 H11G 2 0.394092 0.893195 0.652478 11.00000 -1.50000 H11H 2 0.448578 0.890924 0.705291 11.00000 -1.50000 H11I 2 0.382711 0.924360 0.696443 11.00000 -1.50000 AFIX 0 C117 1 0.258245 0.877309 0.682255 11.00000 0.05049 0.03952 = 0.10677 -0.00134 -0.02329 0.01242 AFIX 137 H11J 2 0.257185 0.872584 0.645936 11.00000 -1.50000 H11K 2 0.245059 0.905281 0.688010 11.00000 -1.50000 H11L 2 0.220711 0.859759 0.695627 11.00000 -1.50000 AFIX 0 C118 1 0.279373 0.721030 0.735461 11.00000 0.03020 0.04045 = 0.03404 -0.00515 0.00799 -0.00166 C119 1 0.333868 0.689798 0.762101 11.00000 0.04936 0.04748 = 0.04762 0.00328 0.01263 -0.00593 AFIX 137 H11M 2 0.363657 0.677276 0.737569 11.00000 -1.50000 H11N 2 0.303741 0.669328 0.777170 11.00000 -1.50000 H11O 2 0.369178 0.702747 0.788660 11.00000 -1.50000 AFIX 0 C120 1 0.225370 0.699996 0.693786 11.00000 0.03773 0.06237 = 0.05068 -0.00581 0.00902 -0.01145 AFIX 137 H12D 2 0.190336 0.719671 0.675962 11.00000 -1.50000 H12E 2 0.195245 0.679566 0.708929 11.00000 -1.50000 H12F 2 0.256063 0.687327 0.669868 11.00000 -1.50000 AFIX 0 C121 1 0.231386 0.737841 0.774026 11.00000 0.06447 0.05738 = 0.05662 -0.00656 0.03222 -0.00820 AFIX 137 H12G 2 0.196076 0.758208 0.758020 11.00000 -1.50000 H12H 2 0.265497 0.749935 0.801896 11.00000 -1.50000 H12I 2 0.201541 0.716257 0.787110 11.00000 -1.50000 AFIX 0 O122 5 0.721605 0.798890 0.759773 11.00000 0.02937 0.02606 = 0.03357 0.00266 0.00438 -0.00341 P123 6 0.723645 0.754433 0.787708 11.00000 0.02728 0.02444 = 0.02526 -0.00036 0.00187 -0.00188 K124 3 0.545579 0.700896 0.762933 11.00000 0.03174 0.02841 = 0.02902 -0.00406 0.00874 -0.00087 O125 5 0.643611 0.770150 0.813083 11.00000 0.02808 0.03313 = 0.02499 -0.00003 0.00296 0.00235 C126 1 0.648310 0.767281 0.864797 11.00000 0.03111 0.02467 = 0.02445 -0.00312 0.00404 -0.00571 C127 1 0.595466 0.783295 0.893809 11.00000 0.02974 0.02390 = 0.03349 -0.00441 0.00376 -0.00157 C128 1 0.615766 0.780110 0.946127 11.00000 0.03310 0.03000 = 0.03251 -0.00857 0.00966 -0.00309 AFIX 43 H128 2 0.580378 0.789890 0.967484 11.00000 -1.20000 AFIX 0 C129 1 0.684733 0.763462 0.968751 11.00000 0.03513 0.02183 = 0.03102 -0.00317 0.00539 -0.00519 C130 1 0.734818 0.746368 0.938028 11.00000 0.03032 0.02519 = 0.02775 0.00045 0.00204 -0.00218 AFIX 43 H130 2 0.781512 0.734051 0.952348 11.00000 -1.20000 AFIX 0 C131 1 0.714879 0.747763 0.886038 11.00000 0.02878 0.01959 = 0.02964 -0.00156 0.00523 -0.00341 C132 1 0.521925 0.804886 0.870187 11.00000 0.03083 0.03672 = 0.03976 -0.01018 0.00096 0.00364 C133 1 0.467620 0.813817 0.909309 11.00000 0.04643 0.09042 = 0.05101 -0.01807 0.00430 0.02620 AFIX 137 H13A 2 0.420426 0.826350 0.892665 11.00000 -1.50000 H13B 2 0.493080 0.832007 0.934976 11.00000 -1.50000 H13C 2 0.454476 0.788830 0.925414 11.00000 -1.50000 AFIX 0 C134 1 0.546241 0.844192 0.847109 11.00000 0.04378 0.03093 = 0.08316 0.00344 -0.01468 0.00563 AFIX 137 H13D 2 0.579847 0.838378 0.821253 11.00000 -1.50000 H13E 2 0.574157 0.860802 0.873627 11.00000 -1.50000 H13F 2 0.500254 0.858508 0.831702 11.00000 -1.50000 AFIX 0 C135 1 0.477289 0.779157 0.829084 11.00000 0.02886 0.03806 = 0.04315 -0.00369 -0.00386 -0.00082 AFIX 137 H13G 2 0.426700 0.791244 0.818582 11.00000 -1.50000 H13H 2 0.470314 0.752246 0.842326 11.00000 -1.50000 H13I 2 0.506237 0.777487 0.799991 11.00000 -1.50000 AFIX 0 C136 1 0.704449 0.765746 1.026553 11.00000 0.04138 0.03444 = 0.02574 -0.00256 0.00589 -0.00485 C137 1 0.642931 0.743147 1.051928 11.00000 0.05378 0.06650 = 0.03291 0.00029 0.00784 -0.01528 AFIX 137 H13J 2 0.592121 0.754998 1.041455 11.00000 -1.50000 H13K 2 0.655078 0.745076 1.088707 11.00000 -1.50000 H13L 2 0.642409 0.714972 1.041783 11.00000 -1.50000 AFIX 0 C138 1 0.782580 0.747928 1.044835 11.00000 0.05163 0.04253 = 0.02738 -0.00038 0.00186 -0.00300 AFIX 137 H13M 2 0.782966 0.719598 1.035466 11.00000 -1.50000 H13N 2 0.792855 0.750468 1.081647 11.00000 -1.50000 H13O 2 0.822540 0.762172 1.029236 11.00000 -1.50000 AFIX 0 C139 1 0.706443 0.809967 1.042301 11.00000 0.05755 0.03960 = 0.02971 -0.00958 0.00275 -0.00169 AFIX 137 H13P 2 0.745200 0.824138 1.025493 11.00000 -1.50000 H13Q 2 0.719783 0.811965 1.078993 11.00000 -1.50000 H13R 2 0.655618 0.822003 1.032462 11.00000 -1.50000 AFIX 0 N140 4 0.756809 0.736000 0.847182 11.00000 0.02830 0.02821 = 0.02320 -0.00010 0.00218 0.00158 C141 1 0.828453 0.716602 0.851187 11.00000 0.02660 0.02259 = 0.03022 -0.00288 0.00108 -0.00166 C142 1 0.859097 0.689108 0.887134 11.00000 0.03616 0.02819 = 0.03233 0.00157 0.00242 0.00028 AFIX 43 H142 2 0.832177 0.682365 0.914755 11.00000 -1.20000 AFIX 0 C143 1 0.929863 0.671587 0.882062 11.00000 0.03744 0.03124 = 0.04134 0.00429 -0.00122 0.00493 AFIX 43 H143 2 0.951825 0.653026 0.906735 11.00000 -1.20000 AFIX 0 C144 1 0.968399 0.680808 0.841772 11.00000 0.03413 0.03652 = 0.04758 0.00056 0.00735 0.00750 AFIX 43 H144 2 1.017028 0.668781 0.839203 11.00000 -1.20000 AFIX 0 C145 1 0.937219 0.707591 0.804511 11.00000 0.03228 0.03350 = 0.03774 0.00174 0.00722 0.00213 AFIX 43 H145 2 0.963717 0.713418 0.776397 11.00000 -1.20000 AFIX 0 C146 1 0.867217 0.725446 0.809257 11.00000 0.02736 0.02285 = 0.03170 -0.00157 -0.00074 -0.00329 N147 4 0.822452 0.750982 0.776514 11.00000 0.02685 0.02820 = 0.03118 0.00359 0.00341 -0.00007 C148 1 0.843404 0.779429 0.742974 11.00000 0.03309 0.02790 = 0.02579 0.00026 0.00227 -0.00577 C149 1 0.910698 0.784365 0.721608 11.00000 0.03514 0.03176 = 0.03313 -0.00362 0.00714 -0.00403 AFIX 43 H149 2 0.951840 0.765794 0.728483 11.00000 -1.20000 AFIX 0 C150 1 0.917721 0.816909 0.689799 11.00000 0.04463 0.03186 = 0.02809 -0.00369 0.00631 -0.00722 C151 1 0.855291 0.842750 0.679528 11.00000 0.04661 0.03035 = 0.02790 0.00097 0.00531 -0.01167 AFIX 43 H151 2 0.859904 0.864304 0.656912 11.00000 -1.20000 AFIX 0 C152 1 0.785763 0.838916 0.700580 11.00000 0.04203 0.02441 = 0.02488 -0.00411 -0.00035 -0.00661 C153 1 0.782750 0.806465 0.732862 11.00000 0.03338 0.02652 = 0.02755 -0.00396 0.00333 -0.00852 C154 1 0.718481 0.867902 0.689577 11.00000 0.04343 0.03026 = 0.03188 0.00184 0.00025 -0.00403 C155 1 0.644702 0.844938 0.669378 11.00000 0.03993 0.04109 = 0.04761 0.00035 -0.01014 -0.00125 AFIX 137 H15D 2 0.601897 0.863835 0.661933 11.00000 -1.50000 H15E 2 0.632247 0.825719 0.694869 11.00000 -1.50000 H15F 2 0.652957 0.830630 0.638464 11.00000 -1.50000 AFIX 0 C156 1 0.733170 0.898993 0.649921 11.00000 0.05939 0.03757 = 0.04228 0.00929 0.00128 0.00043 AFIX 137 H15G 2 0.744040 0.885389 0.619067 11.00000 -1.50000 H15H 2 0.777483 0.915590 0.662953 11.00000 -1.50000 H15I 2 0.687406 0.915937 0.642310 11.00000 -1.50000 AFIX 0 C157 1 0.704981 0.890103 0.738165 11.00000 0.05254 0.03183 = 0.04080 -0.00286 0.00134 -0.00046 AFIX 137 H15J 2 0.661252 0.908454 0.730883 11.00000 -1.50000 H15K 2 0.751368 0.905313 0.750818 11.00000 -1.50000 H15L 2 0.693721 0.870687 0.763754 11.00000 -1.50000 AFIX 0 C162 1 0.896101 0.424629 0.507784 11.00000 0.11521 0.07710 = 0.08120 0.00070 -0.00300 -0.02371 AFIX 137 H16D 2 0.915874 0.402780 0.488577 11.00000 -1.50000 H16E 2 0.842718 0.418850 0.513121 11.00000 -1.50000 H16F 2 0.928061 0.427202 0.540535 11.00000 -1.50000 AFIX 0 C163 1 0.898660 0.463515 0.478481 11.00000 0.07831 0.09497 = 0.08487 -0.01526 0.01902 -0.01950 AFIX 23 H16G 2 0.866595 0.460390 0.445394 11.00000 -1.20000 H16H 2 0.952440 0.468272 0.471895 11.00000 -1.20000 AFIX 0 C164 1 0.870509 0.500479 0.505043 11.00000 0.07036 0.09096 = 0.07044 -0.01410 0.01134 -0.01695 AFIX 23 H16I 2 0.818287 0.494848 0.514038 11.00000 -1.20000 H16J 2 0.905107 0.504773 0.536913 11.00000 -1.20000 AFIX 0 C165 1 0.867152 0.539271 0.474160 11.00000 0.06549 0.09065 = 0.07217 0.01038 0.01653 -0.00861 AFIX 23 H16K 2 0.919842 0.545374 0.466360 11.00000 -1.20000 H16L 2 0.834408 0.534507 0.441661 11.00000 -1.20000 AFIX 0 C166 1 0.837990 0.574021 0.497647 11.00000 0.10661 0.08227 = 0.08284 -0.00335 0.05074 -0.00651 AFIX 23 H16M 2 0.868474 0.578009 0.531126 11.00000 -1.20000 H16N 2 0.783880 0.568887 0.503217 11.00000 -1.20000 AFIX 0 C167 1 0.840707 0.611996 0.467293 11.00000 0.10840 0.09414 = 0.13372 0.01631 0.05992 0.01237 AFIX 137 H16O 2 0.808829 0.608804 0.434605 11.00000 -1.50000 H16P 2 0.894132 0.617534 0.461836 11.00000 -1.50000 H16Q 2 0.820925 0.634292 0.485739 11.00000 -1.50000 AFIX 0 O168 5 0.686881 0.723526 0.751284 11.00000 0.03386 0.02421 = 0.02758 -0.00273 0.00127 -0.00431 O169 5 0.535969 0.692684 0.662792 11.00000 0.02380 0.03434 = 0.02854 -0.00332 0.00137 -0.00008 K170 3 0.665601 0.728949 0.651891 11.00000 0.03062 0.03057 = 0.02761 0.00199 0.00840 0.00131 C158 1 0.993364 0.824266 0.667024 11.00000 0.04584 0.04038 = 0.03777 -0.00192 0.01336 -0.00783 PART 01 PART 1 160A 1 1.064428 0.795860 0.688465 10.33333 0.02978 AFIX 137 H16R 2 1.050691 0.767877 0.681052 10.33333 -1.50000 H16S 2 1.075891 0.799478 0.725078 10.33333 -1.50000 H16T 2 1.109962 0.802935 0.672318 10.33333 -1.50000 AFIX 0 159A 1 1.024879 0.866262 0.675548 10.33333 0.05052 AFIX 137 H15M 2 1.075422 0.868084 0.663390 10.33333 -1.50000 H15N 2 1.030291 0.872498 0.711698 10.33333 -1.50000 H15O 2 0.989308 0.885368 0.657069 10.33333 -1.50000 AFIX 0 161A 1 0.983840 0.816593 0.610017 10.33333 0.04736 AFIX 137 H16U 2 0.942321 0.833502 0.593453 10.33333 -1.50000 H16V 2 0.970922 0.788404 0.603425 10.33333 -1.50000 H16W 2 1.032182 0.822963 0.596688 10.33333 -1.50000 AFIX 0 PART 0 PART 2 160B 1 1.047407 0.789820 0.670856 10.33334 0.04361 AFIX 137 H16X 2 1.022028 0.766712 0.653320 10.33334 -1.50000 H16Y 2 1.062374 0.783143 0.706494 10.33334 -1.50000 H16Z 2 1.093494 0.796865 0.655282 10.33334 -1.50000 AFIX 0 159B 1 1.032341 0.861039 0.696906 10.33334 0.03028 AFIX 137 H15P 2 1.080452 0.867846 0.683547 10.33334 -1.50000 H15Q 2 1.043630 0.854179 0.732773 10.33334 -1.50000 H15R 2 0.997223 0.883997 0.693012 10.33334 -1.50000 AFIX 0 161B 1 0.976268 0.837696 0.611106 10.33334 0.04139 AFIX 137 H111 2 0.951326 0.815782 0.590827 10.33334 -1.50000 H112 2 1.024728 0.844803 0.598386 10.33334 -1.50000 H113 2 0.941950 0.860988 0.608777 10.33334 -1.50000 AFIX 0 PART 0 PART 3 159C 1 1.048603 0.839602 0.708830 10.33334 0.06900 AFIX 137 H15S 2 1.099843 0.841777 0.697743 10.33334 -1.50000 H15T 2 1.050929 0.821212 0.737571 10.33334 -1.50000 H15U 2 1.031802 0.866024 0.718998 10.33334 -1.50000 AFIX 0 161C 1 0.978256 0.855173 0.623411 10.33334 0.07587 AFIX 137 H114 2 1.026440 0.860402 0.609300 10.33334 -1.50000 H115 2 0.959076 0.880141 0.636484 10.33334 -1.50000 H116 2 0.939726 0.844464 0.596950 10.33334 -1.50000 AFIX 0 160C 1 1.016158 0.785718 0.646960 10.33334 0.05521 AFIX 137 H117 2 0.976018 0.776625 0.620436 10.33334 -1.50000 H118 2 1.022717 0.765924 0.674241 10.33334 -1.50000 H119 2 1.064939 0.788904 0.632827 10.33334 -1.50000 PART 0 REM ##### AFIX 0 HKLF 4 REM rom219_0m_a.res in P2(1)/n REM R1 = 0.0530 for 20079 Fo > 4sig(Fo) and 0.0888 for all 29478 data REM 1595 parameters refined using 0 restraints END WGHT 0.0647 12.6558 REM Highest difference peak 0.699, deepest hole -0.489, 1-sigma level 0.061 Q1 1 0.9422 0.5795 0.4853 11.00000 0.05 0.70 Q2 1 0.8328 0.7126 0.6775 11.00000 0.05 0.65 Q3 1 0.9911 0.4373 0.4919 11.00000 0.05 0.61 Q4 1 0.7788 0.5705 0.4609 11.00000 0.05 0.59 Q5 1 0.2960 0.7291 0.7977 11.00000 0.05 0.41 Q6 1 0.8335 0.7798 0.4884 11.00000 0.05 0.41 Q7 1 0.9536 0.8531 0.6069 11.00000 0.05 0.39 Q8 1 0.9251 0.4588 0.5961 11.00000 0.05 0.39 Q9 1 1.0926 0.6108 0.6943 11.00000 0.05 0.38 Q10 1 1.0039 0.8650 0.6443 11.00000 0.05 0.37 Q11 1 0.2867 0.6798 0.7277 11.00000 0.05 0.36 Q12 1 0.1888 0.7325 0.7243 11.00000 0.05 0.36 Q13 1 0.8635 0.7394 0.5105 11.00000 0.05 0.31 Q14 1 1.0677 0.8292 0.7360 11.00000 0.05 0.30 Q15 1 0.7167 0.6383 0.5725 11.00000 0.05 0.28 Q16 1 1.0677 0.8210 0.7199 11.00000 0.05 0.28 Q17 1 0.9671 0.7980 0.6037 11.00000 0.05 0.28 Q18 1 1.0016 0.8314 0.6206 11.00000 0.05 0.27 Q19 1 0.2231 0.8606 0.6597 11.00000 0.05 0.26 Q20 1 1.0384 0.8498 0.7132 11.00000 0.05 0.24 ; _shelx_res_checksum 76834 _shelx_hkl_file ; -1 0 0 1.10 0.50 -1 0 0 1.50 0.80 1 0 0 -0.10 0.20 1 0 0 -0.10 0.10 1 0 0 -0.10 0.20 -1 0 0 0.00 0.40 2 0 0 542.65 29.20 2 0 0 530.75 30.00 2 0 0 478.85 30.50 -2 0 0 550.04 30.10 -2 0 0 563.44 29.30 -2 0 0 549.05 30.10 -2 0 0 508.85 30.50 3 0 0 3.90 2.50 3 0 0 0.20 1.10 3 0 0 -0.30 2.00 -3 0 0 1.30 2.20 -3 0 0 0.40 2.20 -3 0 0 1.20 1.20 3 0 0 2.40 2.40 -3 0 0 2.40 2.30 4 0 0 471.45 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122.49 24.70 14 -14 0 305.47 25.80 -14 -14 0 264.17 31.10 14 -14 0 339.57 25.70 14 -14 0 290.37 31.10 -14 14 0 310.67 23.30 14 14 0 297.37 30.70 14 14 0 300.67 41.00 15 -14 0 28.20 12.00 15 -14 0 19.60 9.20 15 -14 0 17.10 8.40 -15 -14 0 24.10 13.30 15 14 0 18.80 10.70 -15 14 0 18.30 7.20 15 14 0 4.30 13.50 16 -14 0 15.70 10.10 16 -14 0 13.90 8.50 16 -14 0 19.60 9.10 -16 -14 0 -1.90 8.70 16 14 0 18.30 11.40 16 14 0 26.10 16.20 -16 14 0 4.60 6.30 17 -14 0 1.90 9.70 17 -14 0 -4.30 6.30 -17 -14 0 4.10 11.50 17 -14 0 -0.70 6.80 17 14 0 4.10 10.20 17 14 0 18.10 15.60 18 -14 0 2.30 9.60 -18 -14 0 14.00 13.60 18 -14 0 12.30 10.10 18 -14 0 3.00 8.60 18 14 0 6.70 11.20 -19 -14 0 40.10 16.20 19 -14 0 14.10 12.60 19 -14 0 24.90 11.50 19 -14 0 4.60 8.60 19 14 0 8.40 11.80 0 -15 0 1.50 3.40 0 -15 0 -1.10 3.30 0 -15 0 -0.20 2.70 0 15 0 -8.40 3.70 0 15 0 -3.90 2.70 0 15 0 0.70 1.10 0 15 0 -0.40 3.90 -1 -15 0 457.15 29.20 1 -15 0 460.45 28.60 -1 -15 0 385.06 28.60 1 -15 0 415.96 28.40 -1 -15 0 462.25 28.40 -1 -15 0 437.26 28.30 1 -15 0 401.96 28.50 1 15 0 454.15 26.80 1 15 0 481.25 28.80 -1 15 0 477.85 27.50 -1 15 0 440.66 26.70 -1 15 0 427.56 24.50 1 15 0 456.65 29.80 -1 15 0 493.65 30.80 -2 -15 0 72.59 9.90 2 -15 0 103.99 11.10 2 -15 0 74.49 9.00 2 -15 0 77.49 9.90 -2 -15 0 84.49 9.30 -2 -15 0 75.09 10.10 -2 -15 0 89.19 9.60 2 15 0 69.99 10.20 -2 15 0 73.49 7.70 2 15 0 86.09 7.70 -2 15 0 87.19 11.70 -2 15 0 89.49 8.00 2 15 0 80.39 10.40 3 -15 0 1174.78 77.59 -3 -15 0 1329.17 78.49 -3 -15 0 1418.16 76.69 3 -15 0 1382.56 73.39 3 -15 0 1404.36 78.29 3 -15 0 1417.76 78.59 3 15 0 1296.37 75.59 3 15 0 1400.96 78.49 -3 15 0 1347.37 75.89 3 15 0 1379.76 75.89 -3 15 0 1314.67 75.39 3 15 0 1402.76 78.99 -4 -15 0 42.00 6.30 4 -15 0 53.29 8.40 -4 -15 0 33.20 8.00 4 -15 0 34.00 7.20 4 -15 0 37.70 4.30 4 15 0 39.90 7.70 4 15 0 32.00 8.90 4 15 0 59.79 6.50 4 15 0 29.60 5.30 -4 15 0 37.10 5.80 -4 15 0 40.80 6.30 -5 -15 0 403.76 28.40 5 -15 0 396.46 27.00 5 -15 0 393.66 27.40 5 -15 0 410.26 23.40 5 15 0 421.96 24.00 5 15 0 439.86 27.80 -5 15 0 351.56 25.50 -5 15 0 393.46 24.50 5 15 0 325.77 28.20 6 -15 0 207.38 17.50 -6 -15 0 210.68 18.00 6 -15 0 210.38 16.70 6 -15 0 196.68 13.20 6 15 0 179.98 18.00 -6 15 0 176.78 15.60 -6 15 0 180.68 13.90 6 15 0 167.28 18.30 6 15 0 173.48 12.70 7 -15 0 23.20 6.40 -7 -15 0 20.30 7.30 7 -15 0 21.90 7.10 7 -15 0 23.30 4.70 -7 15 0 14.00 5.80 7 15 0 11.80 6.40 7 15 0 16.70 3.60 7 15 0 14.30 7.40 -7 15 0 15.20 4.70 8 -15 0 110.49 11.40 8 -15 0 124.49 14.90 8 -15 0 124.89 15.30 -8 -15 0 123.49 16.30 -8 15 0 126.89 11.00 8 15 0 88.89 13.30 8 15 0 102.69 17.40 8 15 0 111.49 8.80 -9 -15 0 -7.80 5.40 9 -15 0 5.20 5.10 9 -15 0 -2.80 3.50 9 -15 0 -5.20 5.20 -9 15 0 3.80 4.30 9 15 0 3.10 6.00 9 15 0 5.10 7.20 9 15 0 6.80 2.80 10 -15 0 103.79 11.60 -10 -15 0 59.09 12.50 10 -15 0 86.79 13.50 10 -15 0 67.59 13.40 -10 15 0 76.39 9.70 10 15 0 70.39 17.00 10 15 0 83.99 13.60 10 15 0 88.29 7.00 10 15 0 85.09 7.30 11 -15 0 61.69 13.30 11 -15 0 73.29 12.00 11 -15 0 81.49 11.10 -11 -15 0 71.89 14.80 11 15 0 66.49 6.00 11 15 0 59.99 16.40 11 15 0 75.19 8.50 11 15 0 78.79 13.90 -11 15 0 58.29 9.10 -12 -15 0 -3.70 6.60 12 -15 0 6.70 5.70 12 -15 0 13.40 8.20 12 -15 0 6.10 6.80 12 15 0 -1.90 10.20 12 15 0 9.70 7.90 -12 15 0 1.00 4.70 12 15 0 -0.10 2.30 13 -15 0 171.38 19.70 13 -15 0 193.78 23.40 -13 -15 0 175.48 23.10 13 -15 0 177.48 18.30 -13 15 0 170.28 15.80 13 15 0 183.28 22.60 13 15 0 112.69 24.40 14 -15 0 173.48 19.60 14 -15 0 181.58 23.10 -14 -15 0 170.18 23.60 14 -15 0 191.18 21.60 -14 15 0 174.48 16.20 14 15 0 155.08 28.20 14 15 0 143.59 21.20 15 -15 0 32.10 10.30 -15 -15 0 20.90 11.70 15 -15 0 14.20 10.10 15 -15 0 18.90 8.10 -15 15 0 13.20 6.90 15 15 0 49.60 18.20 15 15 0 19.10 10.70 16 -15 0 14.00 8.90 16 -15 0 -0.50 7.50 16 -15 0 13.00 11.10 -16 -15 0 5.20 11.00 16 15 0 12.90 10.30 16 15 0 39.60 16.70 -16 15 0 6.40 6.60 17 -15 0 18.10 11.80 -17 -15 0 36.90 14.50 17 -15 0 30.40 11.40 17 -15 0 24.90 10.90 17 15 0 64.99 20.40 17 15 0 43.80 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3.90 4.60 -1 -22 0 -1.20 4.70 1 -22 0 3.90 4.60 -1 -22 0 -5.30 4.10 -1 22 0 -0.70 4.30 1 22 0 2.10 6.40 -1 22 0 5.20 6.00 -1 22 0 -1.40 5.80 1 22 0 1.40 1.80 1 22 0 -6.50 4.60 1 22 0 -3.30 4.00 2 -22 0 45.70 9.40 2 -22 0 39.40 8.30 -2 -22 0 43.30 9.50 2 -22 0 41.40 8.80 -2 -22 0 41.80 8.20 -2 22 0 53.99 11.30 -2 22 0 44.90 8.30 2 22 0 29.90 8.70 2 22 0 30.30 6.90 2 22 0 42.10 10.20 -2 22 0 37.90 6.80 3 -22 0 0.80 5.20 3 -22 0 4.60 4.50 -3 -22 0 -1.20 3.90 3 -22 0 3.20 4.80 -3 -22 0 1.50 4.90 -3 22 0 -2.20 4.30 3 22 0 -2.80 5.50 3 22 0 6.60 7.30 3 22 0 -3.00 4.10 -3 22 0 -1.20 6.20 -3 22 0 6.90 5.10 -4 -22 0 152.58 18.20 4 -22 0 169.38 18.30 -4 -22 0 179.78 15.40 4 -22 0 181.98 19.30 4 22 0 160.58 14.10 -4 22 0 167.78 20.80 4 22 0 165.88 19.30 -4 22 0 188.88 15.10 -4 22 0 181.38 14.20 4 22 0 145.19 18.10 5 -22 0 7.90 6.40 -5 -22 0 10.70 7.30 -5 -22 0 4.90 4.40 5 -22 0 17.10 7.60 -5 22 0 4.00 4.40 -5 22 0 3.60 6.00 5 22 0 -5.80 6.70 5 22 0 13.90 7.10 5 22 0 4.10 4.60 6 -22 0 177.98 19.70 6 -22 0 161.58 10.70 6 -22 0 165.58 19.10 -6 -22 0 169.18 19.80 6 22 0 166.48 22.00 -6 22 0 167.08 14.60 -6 22 0 148.79 13.50 6 22 0 166.08 19.60 7 -22 0 278.87 23.60 -7 -22 0 307.37 25.60 7 -22 0 256.07 16.20 7 -22 0 227.38 23.90 -7 22 0 223.58 18.50 7 22 0 257.67 22.90 7 22 0 227.58 24.40 -7 22 0 256.77 19.00 8 -22 0 120.79 17.40 -8 -22 0 129.79 19.70 8 -22 0 172.08 12.20 8 -22 0 126.49 17.80 -8 22 0 149.19 14.40 8 22 0 165.48 23.90 8 22 0 140.39 18.90 -8 22 0 141.69 14.60 9 -22 0 22.90 9.70 -9 -22 0 12.40 9.30 9 -22 0 44.50 12.10 9 -22 0 25.50 6.00 9 22 0 35.80 10.70 -9 22 0 24.50 7.60 9 22 0 26.60 13.60 -9 22 0 38.80 8.00 10 -22 0 2.00 6.80 10 -22 0 17.50 5.70 -10 -22 0 -0.70 7.70 10 -22 0 1.70 7.30 -10 22 0 2.90 5.90 -10 22 0 1.30 5.90 10 22 0 1.80 10.90 10 22 0 0.60 7.30 11 -22 0 -0.40 7.50 -11 -22 0 5.10 9.90 11 -22 0 4.80 5.10 11 -22 0 -0.60 7.30 -11 22 0 -12.50 5.60 11 22 0 5.60 11.30 11 22 0 -0.20 8.00 -12 -22 0 292.57 32.80 12 -22 0 278.07 22.50 12 -22 0 297.07 31.10 12 -22 0 250.37 29.20 12 22 0 318.77 35.00 -12 22 0 327.87 23.40 12 22 0 262.17 30.00 13 -22 0 101.19 17.30 -13 -22 0 127.49 22.30 13 -22 0 96.39 18.20 13 -22 0 124.19 15.00 13 22 0 122.49 25.40 13 22 0 62.19 15.90 -13 22 0 89.39 12.50 14 -22 0 3.50 8.00 14 -22 0 11.90 8.10 14 -22 0 -11.00 7.80 -14 -22 0 6.10 11.30 -14 22 0 -3.60 6.60 14 22 0 23.30 10.90 14 22 0 9.90 13.00 15 -22 0 55.59 14.60 15 -22 0 25.40 12.80 -15 -22 0 53.39 16.70 15 22 0 92.69 22.00 15 22 0 59.59 15.90 -15 22 0 44.30 9.90 16 -22 0 38.90 15.20 16 -22 0 62.29 15.80 -16 -22 0 6.70 12.10 16 22 0 128.39 24.40 16 22 0 26.80 13.40 -17 -22 0 -5.00 12.70 17 -22 0 21.10 12.90 17 -22 0 13.00 11.40 17 22 0 8.60 12.10 0 -23 0 4.00 5.20 0 -23 0 4.20 5.20 0 23 0 -1.20 5.80 0 23 0 -0.30 6.50 0 23 0 1.70 5.00 -1 -23 0 20.00 6.50 1 -23 0 27.40 7.40 1 -23 0 34.30 8.30 -1 -23 0 36.00 8.60 1 23 0 32.60 9.30 -1 23 0 21.50 8.50 1 23 0 20.80 5.90 -1 23 0 34.60 8.80 1 23 0 30.60 3.60 -1 23 0 33.60 7.40 1 23 0 23.00 8.40 -2 -23 0 96.99 12.60 2 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22.20 8.90 7 -23 0 26.50 4.40 7 23 0 32.50 12.10 -7 23 0 27.30 6.70 7 23 0 28.10 9.90 -7 23 0 30.60 7.60 8 -23 0 81.09 14.50 -8 -23 0 105.59 17.70 8 -23 0 105.39 16.60 8 -23 0 108.79 10.00 -8 23 0 96.69 12.10 8 23 0 114.99 17.30 8 23 0 118.49 21.50 -8 23 0 105.99 12.10 -9 -23 0 95.19 16.30 9 -23 0 82.49 15.20 9 -23 0 84.99 15.70 9 -23 0 97.09 10.40 -9 23 0 96.69 11.90 9 23 0 89.89 21.00 -9 23 0 85.39 12.30 9 23 0 116.09 17.90 10 -23 0 -1.80 3.70 10 -23 0 5.70 8.00 -10 -23 0 -5.40 7.20 10 -23 0 7.30 8.60 10 23 0 3.80 8.50 10 23 0 -3.90 10.30 -10 23 0 0.80 5.90 -11 -23 0 2.00 8.70 11 -23 0 5.60 8.30 11 -23 0 -0.80 5.10 11 -23 0 15.30 9.70 -11 23 0 18.30 7.70 11 23 0 2.00 9.30 11 23 0 24.10 13.10 -12 -23 0 95.59 18.70 12 -23 0 79.19 16.70 12 -23 0 64.09 14.60 12 -23 0 113.39 14.90 12 23 0 108.09 19.40 -12 23 0 57.19 10.50 12 23 0 77.19 20.50 -13 -23 0 54.89 16.50 13 -23 0 45.80 13.70 13 -23 0 111.09 18.10 -13 23 0 77.29 11.80 13 23 0 108.79 18.80 13 23 0 87.49 21.70 14 -23 0 8.80 9.80 14 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7.60 -3 24 0 12.10 6.80 -3 24 0 3.60 7.90 3 24 0 17.20 9.00 -3 24 0 1.40 5.20 3 24 0 3.60 6.80 3 24 0 9.10 5.30 -4 -24 0 -1.80 5.10 4 -24 0 8.90 6.60 -4 -24 0 -2.60 4.30 4 -24 0 8.90 6.00 4 24 0 -5.00 5.60 -4 24 0 0.00 5.50 4 24 0 -2.40 7.60 4 24 0 4.80 5.20 -4 24 0 -7.30 6.40 -4 24 0 7.40 5.60 5 -24 0 95.09 15.50 -5 -24 0 113.39 15.90 -5 -24 0 97.09 12.60 5 -24 0 67.19 12.80 5 24 0 93.79 16.30 -5 24 0 108.99 11.00 5 24 0 75.89 10.80 5 24 0 111.19 16.00 -5 24 0 110.79 17.70 -5 24 0 81.79 11.00 -6 -24 0 41.70 11.30 6 -24 0 33.20 3.20 6 -24 0 42.80 10.40 6 -24 0 50.69 11.90 6 24 0 39.60 10.70 -6 24 0 24.50 7.30 6 24 0 31.30 12.20 -6 24 0 29.00 6.80 -7 -24 0 2.40 8.00 7 -24 0 11.40 7.60 7 -24 0 8.50 2.90 7 -24 0 6.40 7.30 7 24 0 18.40 9.20 7 24 0 10.70 10.20 -7 24 0 10.90 5.60 -7 24 0 12.70 6.40 8 -24 0 106.39 16.20 8 -24 0 109.59 16.70 -8 -24 0 115.69 17.80 8 -24 0 103.19 9.40 -8 24 0 88.39 12.00 8 24 0 116.39 17.10 -8 24 0 89.09 11.20 8 24 0 110.49 20.40 -9 -24 0 2.50 9.20 9 -24 0 4.10 7.70 9 -24 0 0.30 4.20 9 -24 0 -4.30 6.40 9 24 0 1.70 8.20 -9 24 0 10.90 7.10 9 24 0 17.60 12.70 10 -24 0 2.40 7.60 -10 -24 0 8.60 10.50 10 -24 0 -12.80 7.40 -10 24 0 13.90 7.60 10 24 0 8.30 9.20 10 24 0 -0.20 11.30 11 -24 0 123.29 19.40 11 -24 0 92.09 17.50 -11 -24 0 80.19 17.40 11 24 0 114.79 23.60 -11 24 0 113.59 13.60 11 24 0 128.09 19.70 -12 -24 0 59.39 16.60 12 -24 0 51.69 13.60 12 -24 0 57.09 13.60 -12 24 0 51.09 10.50 12 24 0 109.19 24.10 12 24 0 61.79 15.30 13 -24 0 2.70 8.50 13 -24 0 9.40 9.60 -13 -24 0 -9.60 8.60 13 24 0 10.80 11.40 13 24 0 27.10 13.70 -13 24 0 6.30 7.30 14 -24 0 19.30 10.20 -14 -24 0 8.40 12.50 14 -24 0 28.50 11.40 14 24 0 -2.90 8.40 14 24 0 54.89 18.30 -14 24 0 -13.10 6.20 15 -24 0 10.40 9.40 15 -24 0 6.70 10.20 -15 -24 0 10.10 13.10 15 24 0 -6.20 8.50 15 24 0 53.49 14.30 -16 -24 0 -9.90 9.20 16 -24 0 -4.40 9.30 16 -24 0 9.40 11.60 16 24 0 -20.20 8.90 17 -24 0 1.10 9.30 -17 -24 0 -19.70 12.30 17 -24 0 -2.60 11.30 17 24 0 -1.70 11.00 0 -25 0 3.10 5.60 0 -25 0 10.10 6.40 0 25 0 4.30 7.90 0 25 0 9.20 5.70 0 25 0 -4.30 6.70 1 -25 0 45.50 10.20 1 -25 0 69.39 11.40 -1 -25 0 83.89 13.60 -1 -25 0 61.89 11.30 1 25 0 67.49 12.50 -1 25 0 77.19 12.00 1 25 0 76.29 13.70 1 25 0 62.39 9.40 -1 25 0 85.09 10.80 -1 25 0 82.79 14.90 1 25 0 67.89 5.70 -2 -25 0 126.69 15.30 2 -25 0 108.79 14.70 2 -25 0 122.09 16.00 -2 -25 0 126.69 16.60 -2 25 0 117.49 12.80 2 25 0 128.69 17.10 2 25 0 83.49 11.30 -2 25 0 123.59 14.00 -2 25 0 121.19 18.20 2 25 0 111.99 16.50 -3 -25 0 281.27 24.60 -3 -25 0 289.47 23.00 3 -25 0 258.17 23.90 3 -25 0 284.37 23.40 3 25 0 264.87 21.20 -3 25 0 304.47 29.70 -3 25 0 308.47 21.40 -3 25 0 331.67 22.50 3 25 0 311.97 26.30 3 25 0 277.47 26.10 4 -25 0 56.09 10.20 -4 -25 0 47.70 9.50 -4 -25 0 52.19 11.20 4 -25 0 51.79 10.90 -4 25 0 44.70 8.90 4 25 0 39.00 8.00 -4 25 0 42.00 12.70 4 25 0 40.50 11.80 4 25 0 53.19 12.00 -4 25 0 52.69 8.90 5 -25 0 -4.60 4.40 5 -25 0 -4.20 4.50 -5 -25 0 12.90 7.50 -5 -25 0 6.50 5.30 5 -25 0 2.70 6.30 -5 25 0 5.40 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97.89 19.70 13 -25 0 84.69 16.50 13 -25 0 73.59 17.00 13 25 0 116.39 26.00 13 25 0 74.99 17.30 -13 25 0 76.49 12.30 14 -25 0 23.00 12.00 -14 -25 0 18.90 13.60 14 -25 0 17.50 11.70 -14 25 0 12.20 8.10 14 25 0 63.29 19.20 14 25 0 15.00 11.50 15 -25 0 4.40 10.90 -15 -25 0 0.60 12.50 15 -25 0 5.70 10.90 15 25 0 63.49 15.70 15 25 0 15.80 12.60 -16 -25 0 11.60 12.40 16 -25 0 16.30 11.40 16 -25 0 3.90 9.80 16 25 0 -5.10 10.30 0 -26 0 34.50 9.10 0 -26 0 30.80 8.50 0 26 0 38.20 8.80 0 26 0 52.39 12.80 0 26 0 39.50 10.60 1 -26 0 200.48 20.80 1 -26 0 179.28 19.20 -1 -26 0 152.68 18.10 -1 -26 0 181.78 19.80 1 26 0 152.08 20.40 1 26 0 168.18 15.20 -1 26 0 164.98 17.40 -1 26 0 162.68 21.00 -1 26 0 182.68 15.40 1 26 0 188.18 19.40 2 -26 0 69.69 12.60 -2 -26 0 57.29 10.60 -2 -26 0 64.19 12.50 2 -26 0 42.60 9.90 -2 26 0 70.79 14.90 2 26 0 56.99 9.70 -2 26 0 54.19 10.90 2 26 0 51.39 12.30 -2 26 0 42.50 8.60 2 26 0 51.19 11.80 -3 -26 0 38.80 10.70 3 -26 0 46.90 9.80 3 -26 0 31.90 9.90 -3 -26 0 32.30 8.90 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3 -4 113.39 7.90 0 3 4 91.09 6.10 0 3 4 99.69 6.10 0 3 -4 103.89 7.50 0 3 -4 113.69 7.30 0 3 4 104.89 7.10 1 -3 4 2056.39 109.99 -1 -3 -4 1992.70 110.19 1 -3 4 2019.90 109.79 -1 -3 -4 2107.79 109.89 1 -3 4 1934.01 110.29 -1 -3 -4 2084.09 109.29 -1 -3 -4 1994.80 108.79 -1 3 -4 2014.10 110.29 -1 3 -4 2038.40 109.99 1 3 4 2027.70 108.89 1 3 4 2020.40 110.09 -1 3 -4 2011.70 110.49 -1 3 -4 1863.41 113.19 -1 3 -4 2074.29 109.79 1 3 4 1956.60 109.79 -2 -3 -4 340.87 21.80 2 -3 4 354.66 22.50 -2 -3 -4 354.66 20.70 2 -3 4 353.06 21.50 2 -3 4 338.07 21.50 -2 -3 -4 372.66 21.50 2 -3 4 358.96 20.40 2 -3 4 364.66 21.60 -2 3 -4 378.76 21.60 -2 3 -4 356.56 21.60 2 3 4 371.76 21.90 2 3 4 344.57 21.50 -2 3 -4 336.37 22.30 -2 3 -4 352.76 20.40 2 3 4 364.46 20.80 -2 3 -4 370.36 21.60 3 -3 4 4.20 2.70 3 -3 4 4.90 2.80 -3 -3 -4 -2.70 2.30 -3 -3 -4 0.40 2.00 3 -3 4 1.30 2.10 -3 -3 -4 4.30 2.40 3 -3 4 0.70 2.80 -3 -3 -4 1.50 1.30 3 -3 4 5.90 2.70 -3 3 -4 0.30 2.10 -3 3 -4 -0.30 2.30 -3 3 -4 3.40 2.20 -3 3 -4 0.90 2.20 3 3 4 0.60 2.10 3 3 4 -0.40 2.30 3 3 4 1.70 2.80 -3 3 -4 2.30 2.80 4 -3 4 1876.31 108.49 4 -3 4 1999.90 108.09 -4 -3 -4 1941.61 106.09 4 -3 4 1971.70 109.79 4 -3 4 1893.31 108.69 4 -3 4 1914.01 107.99 -4 -3 -4 1981.30 109.39 -4 -3 -4 2062.09 108.39 -4 3 -4 1922.31 108.79 4 3 4 1955.30 108.39 4 3 4 1991.60 109.19 -4 3 -4 1941.41 109.59 4 3 4 2004.90 108.69 -4 3 -4 2003.60 108.29 -4 3 -4 1976.70 107.99 -4 3 -4 1988.90 107.79 5 -3 4 0.10 2.90 -5 -3 -4 1.30 1.10 -5 -3 -4 1.60 2.70 5 -3 4 2.30 2.80 -5 -3 -4 -3.00 3.10 5 -3 4 0.80 3.20 5 -3 4 0.50 2.30 5 -3 4 1.90 3.00 -5 3 -4 -3.70 2.50 5 3 4 0.70 1.40 5 3 4 6.80 3.50 5 3 4 0.00 3.00 5 3 4 -0.10 2.70 -5 3 -4 -1.60 2.70 -5 3 -4 2.20 2.10 -5 3 -4 -1.70 2.90 -6 -3 -4 239.98 17.00 -6 -3 -4 231.48 13.70 6 -3 4 247.28 17.10 6 -3 4 246.88 17.80 6 -3 4 283.27 20.70 6 -3 4 220.88 15.80 6 -3 4 235.28 16.90 -6 -3 -4 213.38 17.60 -6 3 -4 242.28 16.90 -6 3 -4 247.68 17.50 -6 3 -4 218.08 15.20 6 3 4 246.08 17.40 6 3 4 230.28 14.00 -6 3 -4 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4 43.50 11.10 -16 -3 -4 18.60 12.50 16 -3 4 44.10 13.10 16 3 4 34.20 10.80 16 3 4 51.99 14.50 -16 3 -4 44.40 12.80 -16 3 -4 39.40 11.80 17 -3 4 3.50 9.70 17 -3 4 -1.90 8.50 -17 -3 -4 7.90 9.80 -17 -3 -4 1.30 10.10 17 3 4 13.20 8.60 17 3 4 4.20 8.80 -17 3 -4 2.20 8.40 -17 3 -4 6.60 8.10 -18 -3 -4 9.20 10.70 18 -3 4 -8.70 8.30 18 -3 4 -0.40 7.90 -18 -3 -4 -2.10 9.10 18 3 4 8.50 9.60 -18 3 -4 5.20 11.00 -18 3 -4 -11.10 7.70 18 3 4 0.00 7.80 -19 -3 -4 17.60 13.90 19 -3 4 20.30 12.60 19 -3 4 18.80 11.30 -19 -3 -4 23.60 11.80 19 3 4 37.90 13.00 -19 3 -4 25.60 14.70 -19 3 -4 16.00 11.20 19 3 4 32.50 14.00 -20 -3 -4 168.78 26.90 20 -3 4 170.58 26.60 -20 -3 -4 193.78 30.00 20 -3 4 156.18 24.00 20 3 4 163.48 26.30 -20 3 -4 185.08 27.00 20 3 4 100.59 20.60 -21 -4 4 -8.50 10.80 21 -4 -4 -1.70 11.20 21 4 -4 4.70 12.10 -21 4 4 3.30 11.60 -20 -4 4 50.79 17.10 20 -4 -4 41.80 15.40 -20 4 4 4.60 11.20 20 4 -4 38.00 15.50 -19 -4 4 -4.40 8.80 19 -4 -4 -0.20 5.90 19 -4 -4 14.80 12.20 19 4 -4 -5.90 10.50 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13 -4 0.00 2.80 5 -13 -4 -1.70 3.70 -5 -13 4 1.50 4.00 5 -13 -4 2.60 2.40 5 -13 -4 1.00 3.70 -5 13 4 5.50 3.00 5 13 -4 0.00 2.00 5 13 -4 -1.50 5.90 5 13 -4 4.70 4.60 5 13 -4 0.80 2.70 4 -13 -4 0.40 2.20 -4 -13 4 -1.20 3.70 4 -13 -4 0.60 3.20 4 -13 -4 0.10 3.70 4 13 -4 6.50 4.80 4 13 -4 3.20 3.10 4 13 -4 1.90 2.40 -4 13 4 1.80 2.60 4 13 -4 -1.20 4.60 3 -13 -4 150.68 9.00 3 -13 -4 151.18 12.90 3 -13 -4 150.58 10.60 3 -13 -4 141.19 12.60 -3 -13 4 146.49 13.20 3 13 -4 159.28 14.20 3 13 -4 156.38 11.30 -3 13 4 153.38 10.60 3 13 -4 156.88 13.60 3 13 -4 146.89 12.40 -2 -13 4 116.09 11.00 2 -13 -4 133.89 8.80 2 -13 -4 118.99 11.20 2 -13 -4 138.89 11.30 -2 -13 4 142.39 13.70 2 -13 -4 155.98 10.00 2 13 -4 154.08 12.50 -2 13 4 138.39 9.80 2 13 -4 127.19 11.00 2 13 -4 137.19 10.00 2 13 -4 141.39 14.10 -2 13 4 113.09 9.10 -1 -13 4 4.40 3.30 -1 -13 4 1.10 3.30 1 -13 -4 0.20 3.40 1 -13 -4 -2.30 2.60 -1 -13 4 3.30 3.00 1 -13 -4 0.90 2.20 1 13 -4 -0.90 2.50 -1 13 4 -3.40 2.20 1 13 -4 -0.10 4.10 1 13 -4 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17.00 12.60 16 22 -4 35.00 14.80 16 22 -4 52.59 15.00 -15 -22 4 1.30 10.90 15 -22 -4 -11.20 5.80 15 -22 -4 -0.20 9.00 15 22 -4 -2.10 8.80 15 22 -4 21.80 12.10 -14 -22 4 -10.60 9.10 14 -22 -4 -6.30 8.10 14 -22 -4 -2.80 7.80 14 22 -4 -1.50 8.40 14 22 -4 16.70 11.10 13 -22 -4 15.50 10.00 -13 -22 4 9.40 10.40 13 -22 -4 13.40 9.80 -13 22 4 14.60 7.20 13 22 -4 31.40 14.30 12 -22 -4 201.48 16.20 12 -22 -4 220.98 24.50 -12 -22 4 211.18 26.80 12 -22 -4 188.18 23.90 -12 22 4 152.48 15.20 12 22 -4 178.18 23.80 12 22 -4 132.39 24.40 11 -22 -4 249.38 19.70 -11 -22 4 304.77 31.70 11 -22 -4 315.97 29.80 11 -22 -4 259.37 28.10 11 22 -4 248.38 28.60 -11 22 4 281.97 20.20 11 22 -4 257.07 29.80 10 -22 -4 219.08 23.80 10 -22 -4 224.18 16.80 -10 -22 4 271.67 28.80 10 -22 -4 228.88 25.80 10 22 -4 220.78 29.50 -10 22 4 219.38 17.30 10 22 -4 223.68 26.10 9 -22 -4 4.80 7.00 -9 -22 4 39.50 12.30 9 -22 -4 18.60 8.80 9 -22 -4 15.30 4.50 -9 22 4 15.30 7.00 9 22 -4 18.30 9.80 9 22 -4 13.10 11.90 -8 -22 4 410.26 34.60 8 -22 -4 423.86 33.60 8 -22 -4 490.95 33.90 8 -22 -4 415.16 26.60 8 22 -4 516.35 35.90 8 22 -4 369.26 36.10 -8 22 4 531.65 29.40 7 -22 -4 13.50 7.00 7 -22 -4 16.40 7.30 -7 -22 4 13.20 8.40 7 -22 -4 13.80 3.00 7 22 -4 7.10 7.70 7 22 -4 8.80 11.20 -7 22 4 11.80 6.20 7 22 -4 7.50 5.80 6 -22 -4 2.80 5.40 6 -22 -4 10.90 6.50 -6 -22 4 13.00 7.00 6 22 -4 15.70 8.90 6 22 -4 13.10 10.70 -6 22 4 15.80 6.00 6 22 -4 6.70 5.20 -5 -22 4 449.76 32.50 5 -22 -4 422.86 31.90 5 -22 -4 501.65 33.00 5 22 -4 428.96 34.50 -5 22 4 461.45 28.20 5 22 -4 424.96 29.00 5 22 -4 419.06 33.60 -4 -22 4 32.80 8.20 -4 -22 4 34.10 8.70 4 -22 -4 24.30 7.50 4 -22 -4 24.90 8.00 4 22 -4 30.30 6.80 4 22 -4 26.40 9.80 -4 22 4 28.10 8.80 -4 22 4 27.70 6.50 -4 22 4 22.30 3.90 4 22 -4 28.10 8.80 3 -22 -4 47.70 7.40 -3 -22 4 65.09 10.80 3 -22 -4 56.39 10.60 -3 -22 4 50.59 9.60 3 -22 -4 43.00 8.90 3 22 -4 45.50 7.60 -3 22 4 59.89 8.20 -3 22 4 50.59 6.80 -3 22 4 61.89 12.10 3 22 -4 45.80 10.70 3 22 -4 54.89 11.60 -2 -22 4 504.35 34.30 -2 -22 4 487.05 34.80 2 -22 -4 535.15 34.90 2 -22 -4 456.45 31.80 2 -22 -4 550.54 35.70 2 22 -4 556.54 37.60 2 22 -4 513.35 31.90 2 22 -4 576.04 36.30 -2 22 4 534.35 36.30 -2 22 4 505.75 31.60 -2 22 4 478.25 31.90 1 -22 -4 51.69 10.70 -1 -22 4 56.69 9.60 -1 -22 4 57.79 10.80 1 -22 -4 52.39 8.00 1 -22 -4 62.69 9.90 1 22 -4 57.49 10.70 -1 22 4 48.40 10.50 1 22 -4 54.49 11.70 1 22 -4 45.30 7.60 -1 22 4 47.90 7.80 -1 22 4 46.70 8.30 1 22 -4 45.90 6.00 0 -22 4 295.67 23.40 0 -22 -4 269.27 23.30 0 -22 4 280.87 21.60 0 -22 -4 291.57 20.60 0 -22 -4 254.77 21.30 0 22 -4 326.37 26.10 0 22 4 333.87 24.30 0 22 4 264.07 21.80 0 22 4 260.77 20.10 0 22 -4 311.27 23.00 0 22 -4 294.57 18.50 0 22 -4 302.67 20.90 1 -22 4 52.79 10.30 -1 -22 -4 33.90 8.90 1 -22 4 29.20 7.00 -1 -22 -4 44.60 8.20 -1 22 -4 46.50 7.80 -1 22 -4 46.40 9.30 -1 22 -4 37.40 10.10 1 22 4 40.40 7.50 1 22 4 30.90 8.70 1 22 4 37.90 4.30 -1 22 -4 40.80 5.40 1 22 4 41.70 9.20 2 -22 4 174.28 19.30 -2 -22 -4 147.09 14.70 2 -22 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12 3 -8 46.50 11.30 -12 3 8 66.09 12.50 -12 3 8 68.69 4.70 12 3 -8 49.70 11.90 -12 3 8 55.59 4.90 11 -3 -8 -0.90 5.20 11 -3 -8 -4.30 5.20 -11 -3 8 -4.50 2.40 -11 -3 8 2.10 7.40 11 -3 -8 -6.30 3.40 11 3 -8 -2.80 3.70 11 3 -8 -0.30 6.70 11 3 -8 1.30 5.70 -11 3 8 2.20 5.80 10 -3 -8 8.60 5.80 -10 -3 8 4.60 2.50 10 -3 -8 1.20 4.10 10 -3 -8 6.40 5.60 -10 -3 8 1.50 6.30 10 3 -8 7.20 4.70 -10 3 8 2.40 5.30 10 3 -8 5.60 7.00 10 3 -8 5.70 6.40 -9 -3 8 225.28 13.30 9 -3 -8 230.78 17.50 9 -3 -8 217.88 18.30 -9 -3 8 230.08 20.00 9 -3 -8 213.18 18.80 9 3 -8 203.48 16.90 9 3 -8 226.08 19.30 -9 3 8 213.78 19.30 9 3 -8 220.28 19.90 8 -3 -8 26.00 6.20 8 -3 -8 13.10 5.90 8 -3 -8 12.50 4.80 -8 -3 8 18.90 2.60 -8 -3 8 13.50 6.50 -8 3 8 17.10 6.20 8 3 -8 15.40 7.20 8 3 -8 18.20 5.30 8 3 -8 20.90 6.30 7 -3 -8 47.90 8.10 7 -3 -8 52.99 8.10 7 -3 -8 69.29 8.90 -7 -3 8 55.19 4.90 -7 -3 8 48.80 8.70 -7 3 8 58.39 8.10 7 3 -8 64.59 9.70 7 3 -8 74.79 9.60 7 3 -8 69.19 10.10 -6 -3 8 4.70 1.90 6 -3 -8 3.90 3.80 -6 -3 8 -1.20 3.70 6 -3 -8 0.40 3.60 6 -3 -8 5.10 3.90 6 3 -8 6.70 4.80 -6 3 8 7.30 3.50 6 3 -8 4.00 1.60 6 3 -8 7.60 4.20 -5 -3 8 -0.50 1.40 5 -3 -8 -4.00 2.40 -5 -3 8 -2.00 3.50 5 -3 -8 -0.70 2.60 5 -3 -8 0.70 3.00 -5 3 8 2.10 2.80 5 3 -8 -1.10 3.00 5 3 -8 -1.20 3.40 5 3 -8 0.70 3.60 5 3 -8 1.70 1.60 4 -3 -8 25.30 4.60 4 -3 -8 20.00 2.90 -4 -3 8 22.70 3.50 -4 -3 8 25.60 5.20 4 -3 -8 19.00 5.20 4 -3 -8 19.20 4.30 4 -3 -8 14.40 4.20 4 3 -8 22.30 2.90 4 3 -8 18.20 4.80 4 3 -8 16.90 4.90 -4 3 8 19.40 4.90 -4 3 8 26.60 4.30 4 3 -8 14.50 4.30 3 -3 -8 461.55 28.30 -3 -3 8 450.35 26.60 3 -3 -8 465.55 26.10 3 -3 -8 460.15 26.10 3 -3 -8 431.46 27.60 -3 -3 8 396.46 29.20 3 -3 -8 456.45 26.20 -3 -3 8 430.76 26.30 -3 -3 8 427.96 26.90 -3 3 8 370.56 28.20 3 3 -8 487.15 27.50 3 3 -8 478.15 29.70 3 3 -8 457.35 25.80 3 3 -8 427.96 26.80 -3 3 8 446.56 26.00 -2 -3 8 1898.51 103.89 2 -3 -8 1935.41 104.69 2 -3 -8 1890.01 106.69 -2 -3 8 1808.32 103.09 -2 -3 8 1640.84 106.89 2 -3 -8 1823.02 102.29 2 -3 -8 1962.80 103.49 2 -3 -8 1960.50 103.89 2 3 -8 1972.40 103.69 -2 3 8 1940.71 102.39 2 3 -8 1962.80 103.49 2 3 -8 1954.80 107.69 2 3 -8 2003.30 103.59 -2 3 8 1597.34 105.99 1 -3 -8 573.84 38.80 1 -3 -8 566.54 32.70 -1 -3 8 623.44 35.70 -1 -3 8 593.54 34.30 1 -3 -8 585.04 35.50 -1 -3 8 606.74 34.60 1 -3 -8 602.14 34.90 -1 -3 8 541.25 38.60 -1 3 8 595.84 32.70 -1 3 8 612.64 34.60 1 3 -8 617.34 39.80 1 3 -8 654.93 34.40 1 3 -8 611.74 34.40 1 3 -8 606.24 35.30 0 -3 8 312.47 21.10 0 -3 -8 334.17 20.50 0 -3 8 314.07 20.10 0 3 -8 334.57 19.70 0 3 8 315.77 20.20 0 3 -8 313.37 21.10 0 3 -8 332.57 19.40 0 3 -8 311.37 25.20 1 -3 8 518.75 29.50 -1 -3 -8 487.25 30.60 1 -3 8 517.75 31.90 -1 -3 -8 517.45 27.70 1 -3 8 494.65 30.60 -1 -3 -8 521.05 30.70 1 3 8 508.65 30.60 -1 3 -8 473.35 31.40 -1 3 -8 519.05 29.60 -1 3 -8 513.45 28.70 -1 3 -8 481.45 36.20 -1 3 -8 512.75 29.90 1 3 8 514.35 27.90 -2 -3 -8 2.70 3.00 2 -3 8 0.50 2.10 2 -3 8 5.40 3.40 -2 -3 -8 4.70 1.70 -2 -3 -8 6.30 3.30 2 -3 8 3.90 2.50 2 3 8 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19.20 -7 28 -10 109.59 16.30 8 -28 10 14.10 11.10 -8 -28 -10 1.70 9.60 -8 28 -10 0.10 7.50 8 28 10 3.00 9.90 -8 28 -10 -3.90 11.10 -8 28 -10 -2.20 9.80 -9 -28 -10 7.80 12.00 9 -28 10 -2.40 9.00 9 -28 10 -2.10 10.20 -9 28 -10 -7.60 7.10 -9 28 -10 1.20 11.00 -9 28 -10 -3.30 10.50 9 28 10 1.70 8.50 10 -28 10 68.79 15.70 10 -28 10 102.79 21.20 -10 -28 -10 67.69 18.80 -10 28 -10 74.79 14.90 10 28 10 65.59 13.80 11 -28 10 31.80 13.50 -11 -28 -10 38.50 16.10 11 -28 10 34.70 13.90 -11 28 -10 31.30 11.30 11 28 10 45.20 12.20 12 -28 10 2.30 11.90 12 -28 10 -0.30 9.70 -12 -28 -10 -4.70 10.20 -12 28 -10 -9.70 8.60 12 28 10 -12.30 9.00 -13 -28 -10 15.90 14.30 13 -28 10 33.20 14.60 13 -28 10 15.60 11.10 13 28 10 52.89 14.50 -13 28 -10 28.80 11.80 -14 -29 10 50.19 17.30 14 -29 -10 42.30 14.30 14 -29 -10 43.70 14.20 14 29 -10 91.09 19.20 14 29 -10 58.19 19.30 13 -29 -10 8.10 10.10 -13 -29 10 8.80 11.60 13 -29 -10 14.40 10.60 13 29 -10 47.40 15.70 13 29 -10 13.50 13.90 -12 -29 10 -7.40 9.90 12 -29 -10 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19.00 4 29 -10 91.29 13.90 4 29 -10 109.09 20.40 -3 -29 10 46.70 10.70 3 -29 -10 60.89 12.60 3 -29 -10 47.90 12.70 3 29 -10 43.80 14.00 3 29 -10 58.69 10.90 3 29 -10 66.99 16.50 2 -29 -10 5.90 6.60 2 -29 -10 2.50 8.10 -2 -29 10 -6.20 4.90 2 29 -10 -5.20 8.00 2 29 -10 -5.90 8.70 2 29 -10 -11.10 9.70 1 -29 -10 206.88 25.60 -1 -29 10 204.78 27.70 1 -29 -10 247.88 24.10 1 29 -10 272.77 30.50 1 29 -10 230.48 21.60 1 29 -10 231.28 25.50 0 -29 -10 15.80 10.30 0 -29 -10 21.50 8.00 0 -29 10 28.00 11.20 0 29 -10 16.40 8.90 0 29 -10 9.30 11.20 0 29 -10 6.20 11.50 -1 -29 -10 76.89 16.20 1 -29 10 63.99 15.70 -1 -29 -10 61.49 11.40 -1 29 -10 56.69 11.50 -1 29 -10 54.19 15.20 -1 29 -10 59.99 15.20 2 -29 10 11.80 11.00 -2 -29 -10 10.60 6.60 -2 -29 -10 15.00 9.70 -2 29 -10 14.50 11.60 -2 29 -10 15.60 8.50 -2 29 -10 0.70 11.00 -3 -29 -10 15.80 6.90 3 -29 10 27.20 11.10 -3 -29 -10 11.90 9.60 -3 29 -10 6.40 8.20 -3 29 -10 11.00 11.00 -3 29 -10 32.10 14.30 -4 -29 -10 24.30 11.90 -4 -29 -10 11.30 5.90 4 -29 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30 -10 10.50 12.60 12 -30 -10 6.60 9.90 -12 -30 10 14.00 12.50 12 -30 -10 6.60 9.30 12 30 -10 21.20 13.00 12 30 -10 -23.50 8.30 11 -30 -10 30.70 12.90 -11 -30 10 40.50 15.30 11 -30 -10 32.40 12.80 11 30 -10 30.20 14.60 11 30 -10 64.19 19.40 -10 -30 10 2.80 9.90 10 -30 -10 9.80 9.10 10 -30 -10 -3.20 9.10 10 30 -10 26.30 15.20 10 30 -10 12.90 15.30 10 30 -10 20.30 7.60 9 -30 -10 -10.50 6.60 9 -30 -10 2.00 8.00 -9 -30 10 1.20 9.10 9 30 -10 1.30 10.60 9 30 -10 -0.50 5.40 9 30 -10 2.70 14.60 -8 -30 10 4.50 8.70 8 -30 -10 24.80 11.10 8 30 -10 -2.50 14.00 8 30 -10 -1.50 11.70 8 30 -10 28.70 8.50 -7 -30 10 -3.30 7.70 7 -30 -10 6.80 7.90 7 30 -10 -12.50 9.50 7 30 -10 -9.60 14.30 7 30 -10 10.50 8.00 6 -30 -10 212.48 24.70 -6 -30 10 184.28 22.90 6 -30 -10 228.58 27.00 6 30 -10 225.18 20.70 6 30 -10 200.98 28.80 6 30 -10 216.98 28.10 -5 -30 10 9.10 7.80 5 -30 -10 -5.30 6.30 5 -30 -10 -8.10 7.50 5 30 -10 -12.20 12.60 5 30 -10 -8.90 6.20 5 30 -10 -10.30 8.80 4 -30 -10 14.10 9.20 -4 -30 10 11.00 8.30 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30 -10 31.20 13.00 -4 30 -10 50.09 16.30 5 -30 10 6.50 9.60 -5 -30 -10 -1.20 8.40 -5 30 -10 13.30 8.80 -5 30 -10 -2.70 10.00 -5 30 -10 7.60 11.20 6 -30 10 -1.00 9.80 -6 -30 -10 6.40 11.20 -6 30 -10 -10.00 9.50 -6 30 -10 -1.90 7.70 -6 30 -10 5.70 10.50 7 -30 10 -7.70 8.80 -7 -30 -10 2.00 10.40 -7 30 -10 29.40 13.80 -7 30 -10 -0.60 9.10 -7 30 -10 -5.90 10.30 8 -30 10 151.88 24.00 -8 -30 -10 118.09 22.90 -8 30 -10 160.38 26.10 -8 30 -10 145.59 18.90 9 -30 10 -10.60 8.70 -9 -30 -10 5.30 10.70 -9 30 -10 3.50 12.30 -9 30 -10 -3.20 8.80 10 -30 10 -2.20 8.80 10 -30 10 5.40 11.20 -10 -30 -10 -13.40 11.10 -10 30 -10 -3.10 12.50 -10 30 -10 -6.40 8.80 11 -30 10 5.70 11.40 -11 -30 -10 61.09 18.60 11 -30 10 30.50 13.40 -11 30 -10 15.50 9.70 12 -31 -10 3.00 8.50 12 -31 -10 1.20 9.20 -12 -31 10 -9.50 9.70 12 31 -10 -1.00 12.60 12 31 -10 30.80 14.10 11 -31 -10 5.50 9.00 11 -31 -10 1.90 8.60 -11 -31 10 -6.50 9.60 11 31 -10 -0.10 12.40 11 31 -10 27.30 14.70 -10 -31 10 29.60 13.40 10 -31 -10 32.00 12.00 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13.90 -7 31 -10 66.19 19.40 -7 31 -10 39.90 19.80 -7 31 -10 29.70 12.10 -8 -31 -10 3.50 10.50 8 -31 10 -11.00 8.00 -8 31 -10 -4.00 8.10 -8 31 -10 4.90 12.50 9 -31 10 56.99 18.10 -9 -31 -10 10.60 11.80 -9 31 -10 32.70 15.80 -9 31 -10 36.10 11.60 10 -31 10 -18.30 9.40 -10 -31 -10 -5.40 10.20 -10 31 -10 -0.80 9.30 -10 31 -10 -4.90 12.50 -11 -31 -10 5.50 13.60 11 -31 10 20.40 13.10 11 -31 10 -5.70 8.10 -11 31 -10 -12.70 8.00 -11 31 -10 7.30 14.50 12 -32 -10 12.20 9.90 -12 -32 10 15.90 13.30 12 -32 -10 15.80 11.10 12 32 -10 34.40 14.10 12 32 -10 11.70 12.90 -11 -32 10 9.30 11.90 11 -32 -10 17.50 9.90 11 -32 -10 0.10 9.40 11 32 -10 17.20 14.60 11 32 -10 -3.70 11.60 -10 -32 10 -8.70 8.70 10 -32 -10 4.50 8.70 10 -32 -10 0.20 9.10 10 32 -10 3.40 12.90 10 32 -10 27.80 15.50 9 -32 -10 -0.40 9.50 -9 -32 10 5.00 10.20 9 32 -10 31.30 9.20 9 32 -10 -2.60 14.10 9 32 -10 -12.40 10.00 8 -32 -10 15.70 10.10 -8 -32 10 0.70 8.90 8 32 -10 5.20 12.20 8 32 -10 36.90 9.40 8 32 -10 7.50 15.20 -7 -32 10 30.70 11.70 7 -32 -10 16.90 10.10 7 -32 -10 32.00 12.20 7 32 -10 41.80 10.10 7 32 -10 29.20 15.70 7 32 -10 50.69 17.40 6 -32 -10 21.40 10.40 -6 -32 10 9.40 9.10 6 -32 -10 -1.30 8.10 6 32 -10 14.50 9.10 6 32 -10 -5.90 13.90 6 32 -10 20.30 12.90 5 -32 -10 105.49 18.90 -5 -32 10 110.19 17.60 5 -32 -10 115.49 18.30 5 32 -10 88.79 20.20 5 32 -10 94.39 21.20 5 32 -10 85.09 13.60 4 -32 -10 -2.80 7.50 4 -32 -10 -20.20 6.60 4 32 -10 8.40 11.10 4 32 -10 -13.00 13.50 4 32 -10 -0.70 8.60 3 -32 -10 15.60 11.40 3 -32 -10 42.70 11.60 3 32 -10 18.20 15.10 3 32 -10 36.30 14.80 3 32 -10 21.20 10.60 2 -32 -10 37.00 13.80 2 -32 -10 73.39 13.50 2 32 -10 61.49 16.30 2 32 -10 57.19 12.60 2 32 -10 46.50 17.00 1 -32 -10 -7.80 7.20 1 -32 -10 8.60 7.10 1 32 -10 -4.10 10.30 1 32 -10 -10.70 7.30 1 32 -10 -31.60 9.90 0 -32 -10 18.90 8.20 0 -32 -10 13.50 10.90 0 -32 10 6.10 10.00 0 32 -10 -3.20 9.30 0 32 -10 4.50 11.90 0 32 -10 -4.30 11.10 -1 -32 -10 39.10 13.60 -1 -32 -10 61.19 12.00 1 -32 10 65.79 16.70 -1 32 -10 63.59 17.60 -1 32 -10 73.89 16.90 -1 32 -10 69.19 13.80 2 -32 10 43.10 13.90 -2 -32 -10 28.50 12.20 -2 -32 -10 19.40 7.90 -2 32 -10 30.50 13.60 -2 32 -10 23.20 13.00 -2 32 -10 25.00 11.20 -3 -32 -10 36.80 13.80 -3 -32 -10 32.70 9.90 3 -32 10 46.90 15.20 -3 32 -10 30.50 13.20 -3 32 -10 1.70 9.00 -3 32 -10 5.50 13.00 -4 -32 -10 -3.30 10.00 4 -32 10 -1.10 9.30 -4 32 -10 0.70 10.30 -4 32 -10 -23.50 8.20 -4 32 -10 5.10 11.50 -5 -32 -10 16.10 11.60 5 -32 10 3.90 10.40 -5 32 -10 -5.60 11.40 -5 32 -10 -8.20 9.50 -5 32 -10 -2.20 10.10 6 -32 10 7.60 10.60 -6 -32 -10 1.70 9.50 -6 32 -10 -0.80 12.30 -6 32 -10 1.90 11.40 -6 32 -10 -4.30 9.80 -7 -32 -10 74.79 18.50 7 -32 10 88.19 19.90 -7 32 -10 94.89 15.70 -7 32 -10 120.49 24.20 8 -32 10 120.69 23.40 -8 -32 -10 53.89 17.80 -8 32 -10 64.39 13.80 -9 -32 -10 21.00 15.40 9 -32 10 5.30 12.50 -9 32 -10 -1.40 8.60 -9 32 -10 10.60 14.00 -10 -32 -10 55.49 17.90 10 -32 10 25.00 15.10 -10 32 -10 46.20 18.50 -10 32 -10 22.50 12.60 11 -33 -10 20.80 12.10 -11 -33 10 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27.40 5 -14 -15 357.06 25.00 -5 -14 15 356.46 25.70 5 14 -15 422.56 33.50 5 14 -15 412.36 26.00 5 14 -15 375.46 28.90 4 -14 -15 257.17 21.40 4 -14 -15 228.98 21.10 -4 -14 15 265.77 19.50 4 -14 -15 306.57 19.10 4 14 -15 262.97 22.80 4 14 -15 283.27 20.40 4 14 -15 288.07 20.30 4 14 -15 317.67 27.70 -3 -14 15 110.29 10.30 3 -14 -15 115.49 13.60 3 -14 -15 124.49 14.90 3 14 -15 132.69 11.40 3 14 -15 146.89 14.20 3 14 -15 123.69 15.30 3 14 -15 146.29 21.40 -3 14 15 121.39 10.40 2 -14 -15 5.70 4.60 2 -14 -15 8.80 6.50 -2 14 15 4.80 2.90 2 14 -15 6.10 6.10 2 14 -15 6.20 3.00 2 14 -15 2.40 7.20 2 14 -15 6.90 5.20 1 -14 -15 78.99 10.40 1 -14 -15 96.09 14.20 -1 14 15 74.49 7.20 1 14 -15 81.49 10.90 1 14 -15 75.89 11.80 -1 14 15 77.79 9.20 1 14 -15 78.99 6.00 1 14 -15 75.89 16.20 0 -14 -15 12.10 6.90 0 -14 -15 9.30 4.80 0 14 15 12.30 3.10 0 14 -15 10.50 9.90 0 14 15 21.90 6.00 0 14 -15 12.80 6.60 0 14 -15 20.50 7.10 -1 -14 -15 627.54 37.70 1 -14 15 589.64 37.70 -1 -14 -15 523.65 40.30 -1 14 -15 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5.50 6 -15 -15 2.60 3.70 6 -15 -15 0.60 4.20 -6 -15 15 5.00 5.00 6 15 -15 8.50 5.70 6 15 -15 8.10 9.40 6 15 -15 2.10 6.40 5 -15 -15 -3.10 3.40 5 -15 -15 1.80 4.50 5 -15 -15 -1.90 3.30 -5 -15 15 -5.80 3.70 5 15 -15 -2.60 7.70 5 15 -15 1.10 5.80 5 15 -15 -4.00 4.50 4 -15 -15 -6.00 4.30 -4 -15 15 1.40 3.90 4 -15 -15 1.50 3.20 4 -15 -15 1.80 4.30 4 15 -15 -3.80 5.50 4 15 -15 2.40 5.10 4 15 -15 -0.30 6.70 4 15 -15 -0.50 3.80 -3 -15 15 109.19 9.70 3 -15 -15 120.59 13.80 3 -15 -15 108.99 13.60 3 15 -15 117.19 11.10 3 15 -15 101.89 11.90 -3 15 15 111.39 10.60 3 15 -15 101.99 17.90 3 15 -15 116.59 15.10 2 -15 -15 33.10 9.40 2 -15 -15 41.20 8.20 2 15 -15 30.20 12.10 2 15 -15 29.10 6.90 2 15 -15 42.60 5.50 -2 15 15 35.80 5.50 2 15 -15 30.10 8.70 1 -15 -15 122.99 13.20 1 -15 -15 99.69 14.90 1 15 -15 136.49 16.30 -1 15 15 106.19 9.20 1 15 -15 105.99 13.10 -1 15 15 126.29 11.80 1 15 -15 135.69 22.20 1 15 -15 126.89 8.00 0 -15 -15 122.19 12.90 0 -15 -15 116.99 16.30 0 15 -15 112.99 14.50 0 15 -15 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15 119.19 15.60 -6 -15 -15 140.69 19.60 -6 15 -15 136.79 25.70 -6 15 -15 127.89 18.00 6 15 15 125.49 16.80 -7 -15 -15 33.30 10.90 7 -15 15 34.80 9.70 7 -15 15 50.89 12.10 7 -15 15 41.50 11.90 -7 15 -15 46.60 17.70 7 15 15 63.89 12.50 -7 15 -15 21.10 9.90 8 -15 15 115.59 18.50 8 -15 15 108.39 16.40 8 -15 15 136.79 18.20 -8 -15 -15 110.59 17.80 8 15 15 111.79 17.00 -8 15 -15 97.99 24.40 -8 15 -15 115.89 17.80 9 -15 15 -4.20 6.90 9 -15 15 -6.40 6.00 9 -15 15 -4.60 8.20 -9 -15 -15 -6.60 6.50 -9 15 -15 -5.10 11.10 -9 15 -15 7.10 8.30 9 15 15 12.70 8.50 -10 -15 -15 -4.30 9.00 10 -15 15 21.90 10.00 10 -15 15 4.90 9.00 10 -15 15 25.80 10.40 10 15 15 15.40 9.20 -10 15 -15 1.70 8.10 -10 15 -15 11.30 13.20 11 -15 15 -0.50 7.70 -11 -15 -15 -5.70 9.20 11 -15 15 -9.30 6.10 11 -15 15 -9.80 6.70 -11 15 -15 -4.60 10.70 11 15 15 -10.90 8.60 -11 15 -15 -1.60 8.00 -12 -15 -15 59.89 16.10 12 -15 15 27.70 11.20 12 -15 15 6.80 8.60 12 -15 15 20.10 11.40 -12 15 -15 23.90 15.80 -12 15 -15 17.60 11.80 12 15 15 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14.70 -5 5 -28 56.79 17.00 -5 5 -28 55.09 24.00 5 5 28 51.89 14.80 -6 -5 -28 133.39 24.00 -6 -5 -28 73.19 24.70 6 -5 28 138.89 20.70 -6 5 -28 149.99 25.30 6 5 28 136.29 21.70 -6 5 -28 157.08 35.50 -7 -5 -28 50.99 21.90 -7 -5 -28 55.29 17.10 7 -5 28 69.59 16.70 -7 5 -28 112.99 23.30 7 5 28 89.99 19.00 -7 5 -28 69.59 27.20 -8 -5 -28 22.60 15.40 8 -5 28 24.90 14.30 -8 -5 -28 18.10 15.90 8 5 28 39.50 14.40 -8 5 -28 -3.20 15.10 -8 5 -28 -7.90 11.00 12 -6 -28 23.60 12.30 12 -6 -28 10.60 8.50 12 6 -28 -19.40 15.50 12 6 -28 -2.30 8.60 12 6 -28 12.40 12.30 11 -6 -28 -2.10 7.80 11 -6 -28 3.50 8.70 11 6 -28 -8.40 6.80 11 6 -28 -21.90 12.70 11 6 -28 -1.70 9.10 10 -6 -28 48.40 13.50 10 6 -28 40.10 13.70 10 6 -28 43.30 11.30 10 6 -28 33.10 18.20 9 -6 -28 -7.00 9.30 9 -6 -28 -11.70 9.60 9 6 -28 1.20 9.00 9 6 -28 -15.50 12.10 9 6 -28 12.10 8.20 8 -6 -28 -7.10 9.30 8 -6 -28 21.10 11.30 8 6 -28 -4.50 6.50 8 6 -28 -10.00 8.70 8 6 -28 4.30 13.20 7 -6 -28 0.30 10.90 7 -6 -28 -4.10 7.70 7 6 -28 -6.50 12.40 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10.60 1 6 -32 -16.10 13.10 4 -7 -32 -4.10 9.60 3 -7 -32 -14.90 11.20 3 -7 -32 -8.20 9.60 3 7 -32 -5.80 12.00 3 7 -32 1.60 15.20 2 -7 -32 -15.10 11.80 2 -7 -32 -8.30 6.80 2 7 -32 -4.00 16.70 2 7 -32 -2.90 9.90 1 -7 -32 10.60 12.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 81529 _shelx_fab_file ; 2 0 0 55.07 0.00 4 0 0 -63.78 0.00 6 0 0 28.89 0.00 8 0 0 8.28 0.00 10 0 0 -5.03 0.00 12 0 0 -11.20 0.00 14 0 0 -3.29 0.00 16 0 0 -2.28 0.00 18 0 0 0.46 0.00 20 0 0 -0.53 0.00 2 1 0 57.23 0.00 3 1 0 124.39 0.00 4 1 0 -35.23 0.00 5 1 0 -0.73 0.00 6 1 0 1.98 0.00 7 1 0 -20.53 0.00 8 1 0 3.87 0.00 9 1 0 -2.61 0.00 10 1 0 -4.08 0.00 11 1 0 2.40 0.00 12 1 0 -3.97 0.00 13 1 0 -8.16 0.00 14 1 0 -0.83 0.00 15 1 0 -7.37 0.00 16 1 0 3.63 0.00 17 1 0 -0.74 0.00 18 1 0 1.18 0.00 19 1 0 -0.57 0.00 20 1 0 -1.31 0.00 21 1 0 -4.71 0.00 1 2 0 -131.38 0.00 2 2 0 84.84 0.00 3 2 0 -38.31 0.00 4 2 0 -32.04 0.00 5 2 0 52.99 0.00 6 2 0 6.12 0.00 7 2 0 -4.18 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2.09 0.00 -10 35 10 -4.43 0.00 8 35 10 2.57 0.00 7 36 10 3.88 0.00 4 38 10 0.74 0.00 -3 39 10 0.85 0.00 -2 39 10 -1.43 0.00 -1 39 10 4.31 0.00 0 39 10 0.94 0.00 1 39 10 2.31 0.00 -21 0 11 -1.38 0.00 -21 1 11 0.50 0.00 -21 2 11 2.07 0.00 19 2 11 -2.08 0.00 19 3 11 -2.77 0.00 19 4 11 -0.38 0.00 19 5 11 -3.20 0.00 -20 12 11 -3.28 0.00 18 13 11 -2.39 0.00 17 17 11 -1.36 0.00 -18 20 11 -2.86 0.00 16 21 11 0.56 0.00 -17 23 11 -0.96 0.00 14 26 11 -0.78 0.00 13 28 11 1.10 0.00 -13 31 11 -0.16 0.00 11 31 11 -1.49 0.00 -12 32 11 0.36 0.00 -8 36 11 3.12 0.00 -7 37 11 1.95 0.00 5 37 11 -0.86 0.00 -5 38 11 -2.04 0.00 3 38 11 -1.31 0.00 -20 10 12 -1.95 0.00 18 10 12 -0.44 0.00 -20 11 12 3.53 0.00 18 11 12 1.44 0.00 -19 16 12 1.26 0.00 17 16 12 1.56 0.00 -16 25 12 -2.84 0.00 14 25 12 -0.71 0.00 -15 27 12 1.03 0.00 13 27 12 -1.92 0.00 -14 29 12 -0.57 0.00 12 29 12 1.12 0.00 -11 33 12 2.03 0.00 9 33 12 0.85 0.00 -10 34 12 0.15 0.00 8 34 12 -1.53 0.00 -9 35 12 -1.59 0.00 7 35 12 -0.71 0.00 -6 37 12 -1.56 0.00 4 37 12 -0.51 0.00 -3 38 12 -3.15 0.00 -2 38 12 -0.04 0.00 -1 38 12 -1.68 0.00 0 38 12 2.94 0.00 1 38 12 -1.30 0.00 -20 1 13 2.66 0.00 18 7 13 1.64 0.00 18 8 13 -1.54 0.00 -20 9 13 1.66 0.00 17 14 13 -0.53 0.00 -19 15 13 -1.57 0.00 16 18 13 -0.01 0.00 -18 19 13 -0.24 0.00 15 21 13 -0.20 0.00 -17 22 13 -1.89 0.00 -16 24 13 2.30 0.00 14 24 13 0.48 0.00 13 26 13 0.08 0.00 -14 28 13 0.00 0.00 12 28 13 -0.78 0.00 -13 30 13 -1.48 0.00 -12 31 13 -1.05 0.00 10 31 13 -1.12 0.00 6 35 13 -1.16 0.00 -7 36 13 1.31 0.00 -5 37 13 -0.09 0.00 2 37 13 0.63 0.00 3 37 13 -0.66 0.00 18 0 14 1.09 0.00 18 1 14 0.73 0.00 18 2 14 0.77 0.00 18 3 14 0.69 0.00 18 4 14 -0.70 0.00 -20 7 14 0.37 0.00 -20 8 14 -5.97 0.00 17 12 14 0.12 0.00 -19 14 14 1.06 0.00 16 17 14 -0.43 0.00 -18 18 14 -0.54 0.00 15 20 14 0.93 0.00 -17 21 14 3.20 0.00 14 23 14 0.33 0.00 13 25 14 1.52 0.00 -15 26 14 -1.40 0.00 12 27 14 1.10 0.00 -13 29 14 3.44 0.00 10 30 14 2.10 0.00 -11 32 14 -0.65 0.00 -10 33 14 1.24 0.00 -9 34 14 2.66 0.00 5 35 14 0.50 0.00 -6 36 14 1.15 0.00 3 36 14 1.01 0.00 -3 37 14 0.82 0.00 -2 37 14 0.96 0.00 -1 37 14 -1.55 0.00 0 37 14 0.12 0.00 1 37 14 -0.50 0.00 -20 1 15 2.87 0.00 -20 3 15 4.16 0.00 -20 4 15 -4.07 0.00 -20 5 15 7.00 0.00 17 9 15 0.11 0.00 17 10 15 2.84 0.00 -19 12 15 4.34 0.00 -19 13 15 -1.14 0.00 16 15 15 0.01 0.00 -18 17 15 -0.53 0.00 15 19 15 0.89 0.00 -17 20 15 -3.13 0.00 -16 23 15 -1.86 0.00 13 24 15 -3.74 0.00 -15 25 15 -0.32 0.00 12 26 15 -1.42 0.00 -14 27 15 -2.67 0.00 11 28 15 -1.51 0.00 -12 30 15 -0.75 0.00 8 32 15 0.44 0.00 7 33 15 0.05 0.00 -8 34 15 -2.33 0.00 4 35 15 2.68 0.00 -4 36 15 -0.41 0.00 1 36 15 -0.09 0.00 2 36 15 0.75 0.00 17 5 16 -1.99 0.00 17 6 16 0.95 0.00 -19 11 16 -4.04 0.00 16 13 16 -1.73 0.00 -18 16 16 -0.30 0.00 15 17 16 1.58 0.00 -17 19 16 1.55 0.00 14 20 16 0.70 0.00 -16 22 16 2.00 0.00 13 23 16 2.61 0.00 -15 24 16 0.87 0.00 12 25 16 2.10 0.00 -14 26 16 2.84 0.00 11 27 16 1.94 0.00 -13 28 16 1.74 0.00 8 31 16 -0.42 0.00 7 32 16 -1.94 0.00 6 33 16 0.84 0.00 -7 34 16 0.70 0.00 -5 35 16 -1.58 0.00 2 35 16 -1.69 0.00 3 35 16 -2.63 0.00 -19 8 17 0.50 0.00 -19 9 17 2.36 0.00 16 10 17 1.10 0.00 -18 14 17 -2.00 0.00 15 15 17 2.45 0.00 -17 18 17 0.13 0.00 14 19 17 -0.16 0.00 -16 21 17 0.29 0.00 -15 23 17 -1.67 0.00 -14 25 17 -2.43 0.00 -13 27 17 -1.61 0.00 9 29 17 1.02 0.00 -11 30 17 -1.16 0.00 8 30 17 0.36 0.00 -10 31 17 -1.29 0.00 7 31 17 1.60 0.00 -9 32 17 -1.45 0.00 6 32 17 1.79 0.00 5 33 17 2.35 0.00 -6 34 17 0.79 0.00 3 34 17 3.21 0.00 -3 35 17 1.59 0.00 -2 35 17 1.37 0.00 -1 35 17 3.63 0.00 0 35 17 -1.06 0.00 -19 4 18 1.78 0.00 -19 5 18 -0.78 0.00 16 5 18 1.39 0.00 -19 6 18 0.80 0.00 16 6 18 1.02 0.00 16 7 18 -1.32 0.00 -18 12 18 0.36 0.00 -18 13 18 -0.01 0.00 15 13 18 -2.60 0.00 -17 17 18 -0.92 0.00 14 17 18 -2.44 0.00 -16 20 18 -1.58 0.00 13 20 18 0.04 0.00 -15 22 18 1.10 0.00 12 22 18 -1.14 0.00 -13 26 18 1.21 0.00 10 26 18 0.83 0.00 -11 29 18 -0.49 0.00 8 29 18 -0.82 0.00 -10 30 18 1.15 0.00 7 30 18 -1.05 0.00 -9 31 18 0.39 0.00 6 31 18 -1.86 0.00 -8 32 18 1.65 0.00 5 32 18 -1.98 0.00 -6 33 18 -1.64 0.00 3 33 18 -1.59 0.00 -4 34 18 -3.35 0.00 -3 34 18 -1.47 0.00 0 34 18 0.19 0.00 1 34 18 0.84 0.00 15 9 19 -0.02 0.00 -18 10 19 -1.34 0.00 15 10 19 3.63 0.00 -18 11 19 -0.79 0.00 -17 15 19 -0.90 0.00 14 15 19 1.89 0.00 13 18 19 0.66 0.00 -15 21 19 -0.16 0.00 12 21 19 1.76 0.00 -14 23 19 -0.17 0.00 11 23 19 3.82 0.00 -13 25 19 0.34 0.00 10 25 19 -0.07 0.00 -11 28 19 0.99 0.00 8 28 19 1.76 0.00 -10 29 19 -1.58 0.00 7 29 19 0.97 0.00 -9 30 19 0.90 0.00 6 30 19 1.55 0.00 -8 31 19 -2.59 0.00 5 31 19 3.29 0.00 3 32 19 1.25 0.00 -4 33 19 4.36 0.00 1 33 19 -2.50 0.00 15 3 20 -0.42 0.00 15 4 20 0.52 0.00 15 5 20 -1.33 0.00 15 6 20 0.57 0.00 -18 7 20 -0.38 0.00 -18 8 20 0.28 0.00 14 12 20 -1.86 0.00 -17 13 20 -0.68 0.00 13 16 20 -1.85 0.00 -16 17 20 1.46 0.00 12 19 20 -1.65 0.00 -15 20 20 0.57 0.00 -14 22 20 -0.22 0.00 -13 24 20 -0.78 0.00 9 25 20 -0.18 0.00 -11 27 20 -0.03 0.00 -10 28 20 0.20 0.00 7 28 20 -0.47 0.00 -9 29 20 -0.89 0.00 6 29 20 -0.27 0.00 -8 30 20 2.41 0.00 5 30 20 -3.58 0.00 -7 31 20 0.02 0.00 3 31 20 -1.01 0.00 -5 32 20 1.70 0.00 -4 32 20 -2.76 0.00 1 32 20 3.91 0.00 -18 1 21 0.25 0.00 -18 2 21 1.79 0.00 -18 3 21 -0.07 0.00 -18 4 21 1.25 0.00 14 8 21 -1.73 0.00 14 9 21 1.37 0.00 -17 11 21 -1.23 0.00 13 13 21 -0.49 0.00 13 14 21 2.42 0.00 -16 15 21 1.88 0.00 12 17 21 2.26 0.00 -15 18 21 0.59 0.00 11 20 21 -0.86 0.00 -14 21 21 0.50 0.00 10 22 21 -0.93 0.00 -13 23 21 1.11 0.00 9 24 21 0.51 0.00 8 25 21 -0.44 0.00 -11 26 21 -0.24 0.00 -10 27 21 -0.20 0.00 -9 28 21 0.61 0.00 -8 29 21 -0.23 0.00 -7 30 21 -1.38 0.00 3 30 21 1.23 0.00 -5 31 21 -1.50 0.00 -4 31 21 0.03 0.00 1 31 21 -4.19 0.00 14 0 22 3.46 0.00 14 1 22 0.17 0.00 14 2 22 2.20 0.00 -17 7 22 0.91 0.00 -17 8 22 0.64 0.00 13 10 22 0.58 0.00 13 11 22 -0.59 0.00 -16 13 22 -0.54 0.00 12 15 22 1.03 0.00 -15 17 22 -0.20 0.00 11 18 22 1.31 0.00 -14 19 22 -1.52 0.00 10 20 22 0.04 0.00 9 22 22 0.97 0.00 -12 23 22 -1.18 0.00 8 24 22 0.04 0.00 7 25 22 -1.32 0.00 -10 26 22 0.31 0.00 -9 27 22 -0.88 0.00 -8 28 22 -0.59 0.00 4 28 22 0.80 0.00 3 29 22 -0.38 0.00 -5 30 22 -0.26 0.00 -4 30 22 1.78 0.00 0 30 22 -0.98 0.00 1 30 22 3.62 0.00 -17 0 23 -1.72 0.00 -17 1 23 0.27 0.00 -17 2 23 0.76 0.00 -17 3 23 0.27 0.00 -17 4 23 0.87 0.00 13 4 23 -0.62 0.00 13 5 23 -0.98 0.00 13 6 23 -1.66 0.00 -16 10 23 0.71 0.00 -16 11 23 0.08 0.00 12 11 23 -1.64 0.00 12 12 23 0.71 0.00 -15 15 23 0.07 0.00 11 15 23 -1.08 0.00 10 18 23 -0.96 0.00 -13 20 23 0.23 0.00 9 20 23 0.84 0.00 -12 22 23 2.01 0.00 8 22 23 -1.68 0.00 6 25 23 2.33 0.00 -9 26 23 0.94 0.00 5 26 23 -1.28 0.00 4 27 23 -0.34 0.00 -6 28 23 0.34 0.00 2 28 23 -1.80 0.00 -4 29 23 -0.89 0.00 -3 29 23 3.24 0.00 -2 29 23 -0.99 0.00 -1 29 23 0.39 0.00 0 29 23 0.08 0.00 -16 6 24 -1.06 0.00 12 6 24 2.48 0.00 -16 7 24 -0.72 0.00 12 7 24 1.60 0.00 12 8 24 3.12 0.00 -15 12 24 0.38 0.00 11 12 24 1.08 0.00 -14 15 24 -0.71 0.00 10 16 24 -0.62 0.00 -13 18 24 -0.06 0.00 9 18 24 -0.21 0.00 -12 20 24 -4.24 0.00 8 20 24 -2.06 0.00 -11 22 24 -3.24 0.00 7 22 24 -1.69 0.00 -10 23 24 -0.64 0.00 6 23 24 1.75 0.00 -7 26 24 -2.25 0.00 3 26 24 0.26 0.00 -6 27 24 -0.10 0.00 2 27 24 0.49 0.00 -3 28 24 -1.58 0.00 -2 28 24 1.52 0.00 -1 28 24 1.22 0.00 -15 8 25 0.71 0.00 11 8 25 -1.51 0.00 -15 9 25 -0.07 0.00 11 9 25 -0.35 0.00 -14 13 25 -4.01 0.00 10 13 25 0.39 0.00 -13 16 25 1.04 0.00 9 16 25 -1.22 0.00 -12 18 25 2.66 0.00 8 18 25 0.50 0.00 -11 20 25 1.62 0.00 7 20 25 -0.35 0.00 -9 23 25 -2.37 0.00 5 23 25 -0.61 0.00 -8 24 25 -1.92 0.00 4 24 25 -1.39 0.00 -7 25 25 2.58 0.00 2 25 25 -1.48 0.00 -5 26 25 2.08 0.00 -4 26 25 1.10 0.00 0 26 25 -1.98 0.00 1 26 25 0.26 0.00 -15 1 26 3.22 0.00 -15 2 26 -0.17 0.00 -15 3 26 2.12 0.00 -15 4 26 -1.88 0.00 10 8 26 0.82 0.00 10 9 26 1.49 0.00 -14 10 26 1.64 0.00 -13 13 26 -0.09 0.00 9 13 26 2.13 0.00 -13 14 26 -2.74 0.00 8 15 26 2.60 0.00 -12 16 26 -2.24 0.00 -11 18 26 -2.18 0.00 7 18 26 0.49 0.00 -10 20 26 -3.56 0.00 -9 21 26 -3.62 0.00 5 21 26 3.05 0.00 -8 22 26 0.55 0.00 4 22 26 1.14 0.00 -7 23 26 -1.47 0.00 3 23 26 1.90 0.00 -6 24 26 0.33 0.00 1 24 26 0.95 0.00 -3 25 26 -1.98 0.00 -2 25 26 2.23 0.00 -1 25 26 -1.41 0.00 -14 2 27 1.80 0.00 -14 3 27 -0.10 0.00 -14 4 27 1.05 0.00 -14 5 27 -0.35 0.00 -14 6 27 1.33 0.00 9 8 27 -1.71 0.00 9 9 27 -1.04 0.00 -13 10 27 -1.98 0.00 8 12 27 -2.28 0.00 -12 13 27 -0.60 0.00 -12 14 27 -1.32 0.00 7 15 27 -4.59 0.00 -11 16 27 3.67 0.00 6 17 27 1.14 0.00 -10 18 27 2.58 0.00 -9 19 27 3.37 0.00 -8 20 27 1.64 0.00 4 20 27 -0.74 0.00 -7 21 27 2.12 0.00 3 21 27 -1.87 0.00 -6 22 27 3.99 0.00 2 22 27 0.23 0.00 -4 23 27 1.89 0.00 -3 23 27 0.22 0.00 -2 23 27 0.92 0.00 -1 23 27 -1.31 0.00 0 23 27 -2.08 0.00 -13 3 28 -1.02 0.00 -13 4 28 -1.70 0.00 -13 5 28 -0.14 0.00 -13 6 28 -1.54 0.00 8 7 28 2.14 0.00 8 8 28 1.07 0.00 -12 10 28 2.38 0.00 7 11 28 1.12 0.00 7 12 28 4.51 0.00 -11 13 28 1.33 0.00 6 14 28 -0.34 0.00 -10 15 28 -0.86 0.00 5 16 28 3.62 0.00 -9 17 28 -1.84 0.00 -8 18 28 -1.24 0.00 -7 19 28 0.78 0.00 3 19 28 1.67 0.00 -6 20 28 -0.32 0.00 1 20 28 2.17 0.00 -4 21 28 -0.77 0.00 -3 21 28 -0.69 0.00 -2 21 28 1.00 0.00 -1 21 28 0.46 0.00 0 21 28 2.27 0.00 -12 1 29 -0.07 0.00 -12 2 29 1.67 0.00 -12 3 29 -0.33 0.00 -12 4 29 1.35 0.00 -12 5 29 -0.81 0.00 7 5 29 0.82 0.00 7 6 29 0.29 0.00 7 7 29 -0.71 0.00 -11 9 29 0.09 0.00 -11 10 29 -2.41 0.00 6 10 29 -1.01 0.00 -10 12 29 -0.29 0.00 5 13 29 -1.58 0.00 -9 14 29 0.66 0.00 4 14 29 -3.23 0.00 4 15 29 -0.55 0.00 -8 16 29 2.76 0.00 3 16 29 -2.29 0.00 -7 17 29 1.39 0.00 2 17 29 -0.69 0.00 -6 18 29 0.66 0.00 -5 18 29 0.36 0.00 1 18 29 -0.79 0.00 -4 19 29 -1.22 0.00 -3 19 29 1.74 0.00 -2 19 29 -1.14 0.00 -1 19 29 -2.35 0.00 6 0 30 -0.61 0.00 -11 1 30 0.22 0.00 6 1 30 0.69 0.00 -11 2 30 -0.11 0.00 6 2 30 0.12 0.00 -11 3 30 1.25 0.00 6 3 30 0.69 0.00 6 4 30 -0.38 0.00 -10 7 30 -3.75 0.00 5 7 30 -1.37 0.00 -10 8 30 1.12 0.00 5 8 30 -1.99 0.00 -9 10 30 0.23 0.00 4 10 30 -0.43 0.00 -9 11 30 3.27 0.00 4 11 30 0.13 0.00 -8 12 30 0.90 0.00 3 12 30 1.04 0.00 -8 13 30 -1.50 0.00 3 13 30 0.53 0.00 -7 14 30 -2.62 0.00 2 14 30 2.26 0.00 -6 15 30 -1.73 0.00 1 15 30 0.13 0.00 -5 16 30 -0.83 0.00 -4 16 30 1.69 0.00 -3 16 30 0.80 0.00 -2 16 30 -1.93 0.00 -1 16 30 0.81 0.00 0 16 30 0.85 0.00 4 1 31 -1.65 0.00 -9 2 31 0.15 0.00 4 2 31 0.59 0.00 -9 3 31 -1.39 0.00 4 3 31 0.85 0.00 -9 4 31 0.44 0.00 4 4 31 1.02 0.00 -9 5 31 -0.78 0.00 4 5 31 1.88 0.00 -8 7 31 0.63 0.00 3 7 31 1.22 0.00 -8 8 31 0.97 0.00 3 8 31 0.24 0.00 -7 10 31 -0.72 0.00 2 10 31 0.53 0.00 -6 11 31 -0.04 0.00 1 11 31 0.28 0.00 -6 12 31 -1.23 0.00 -5 12 31 -0.73 0.00 0 12 31 -0.03 0.00 -4 13 31 -0.77 0.00 -3 13 31 -1.93 0.00 -2 13 31 0.60 0.00 -1 13 31 1.68 0.00 2 0 32 0.87 0.00 -7 1 32 0.85 0.00 2 1 32 -0.31 0.00 -7 2 32 2.05 0.00 2 2 32 1.15 0.00 -7 3 32 1.69 0.00 2 3 32 -0.53 0.00 -7 4 32 0.50 0.00 -6 4 32 0.85 0.00 1 4 32 -0.63 0.00 -6 5 32 1.22 0.00 1 5 32 0.64 0.00 -6 6 32 1.51 0.00 0 6 32 1.07 0.00 1 6 32 0.26 0.00 -5 7 32 2.77 0.00 0 7 32 0.89 0.00 -5 8 32 2.70 0.00 -4 8 32 0.55 0.00 -3 8 32 1.10 0.00 -2 8 32 1.77 0.00 -1 8 32 0.83 0.00 0 8 32 0.89 0.00 -4 9 32 1.10 0.00 -3 9 32 -1.14 0.00 -2 9 32 0.30 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 30118) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.583 0.500 -0.000 1549 195 ' ' 2 0.982 -0.000 0.500 1549 195 ' ' 3 0.259 0.043 0.066 13 -1 ' ' 4 0.671 0.246 0.119 15 0 ' ' 5 0.578 0.111 0.128 6 0 ' ' 6 0.655 0.970 0.129 7 -1 ' ' 7 0.393 0.774 0.136 7 0 ' ' 8 0.246 0.027 0.207 12 0 ' ' 9 0.093 0.127 0.215 16 0 ' ' 10 0.254 0.527 0.293 12 0 ' ' 11 0.407 0.628 0.285 16 0 ' ' 12 0.107 0.274 0.364 7 0 ' ' 13 0.845 0.470 0.371 7 -1 ' ' 14 0.922 0.611 0.372 6 0 ' ' 15 0.829 0.746 0.381 15 0 ' ' 16 0.241 0.543 0.434 14 -1 ' ' 17 0.759 0.457 0.566 14 -1 ' ' 18 0.171 0.254 0.619 15 0 ' ' 19 0.078 0.389 0.628 6 0 ' ' 20 0.155 0.530 0.629 7 -1 ' ' 21 0.893 0.726 0.636 7 0 ' ' 22 0.746 0.473 0.707 13 0 ' ' 23 0.592 0.372 0.715 16 0 ' ' 24 0.907 0.872 0.785 16 0 ' ' 25 0.754 0.973 0.792 13 0 ' ' 26 0.607 0.226 0.864 7 0 ' ' 27 0.345 0.030 0.871 6 -1 ' ' 28 0.329 0.754 0.881 15 0 ' ' 29 0.422 0.889 0.872 6 0 ' ' 30 0.741 0.957 0.934 14 -1 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 1 0 1.324 0 2 0 1.218 -1 0 1 1.321 1 0 1 1.483 1 1 1 1.603 0 0 2 1.538 0 1 2 1.654 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL x_dummy P 21/n R = 0.09 CELL 17.4664 33.4388 26.6896 90.00 97.22 90.00 SPGR P21/n # Solvent Accessible Volume = 3435 # Electrons Found in S.A.V. = 389 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.471 0.509 0.056 ! 7.63 eA-3 C102 0.047 0.055 0.499 ! 7.55 eA-3 C103 0.527 0.483 0.065 ! 6.86 eA-3 C104 0.807 0.353 0.130 ! 4.57 eA-3 C105 0.500 0.500 0.000 ! 3.95 eA-3 C106 0.627 0.931 0.455 ! 3.70 eA-3 C107 0.122 0.529 0.044 ! 3.68 eA-3 C108 0.655 0.932 0.499 ! 3.62 eA-3 C109 0.068 0.967 0.411 ! 3.55 eA-3 C110 0.560 0.533 0.099 ! 3.09 eA-3 C111 0.890 0.945 0.436 ! 3.09 eA-3 C112 0.393 0.552 0.054 ! 3.05 eA-3 C113 0.653 0.891 0.432 ! 3.05 eA-3 C114 0.703 0.882 0.403 ! 2.79 eA-3 C115 0.639 0.899 0.413 ! 2.78 eA-3 C116 0.986 0.955 0.454 ! 2.51 eA-3 C117 0.412 0.492 0.083 ! 2.38 eA-3 C118 0.859 0.391 0.118 ! 2.38 eA-3 C119 0.072 0.959 0.453 ! 2.26 eA-3 C120 0.172 0.999 0.423 ! 2.22 eA-3 C121 0.520 0.592 0.010 ! 2.07 eA-3 C122 0.532 0.415 0.010 ! 1.58 eA-3 C123 0.881 0.905 0.493 ! 1.23 eA-3 C124 0.615 0.423 0.023 ! 1.16 eA-3 Q125 0.061 0.797 0.686 ! 1.07 eA-3 Q126 0.944 0.163 0.293 ! 1.01 eA-3 Q127 0.860 0.866 0.657 ! 0.98 eA-3 Q128 0.311 0.083 0.357 ! 0.93 eA-3 C129 0.127 0.539 0.984 ! 0.87 eA-3 Q130 0.997 0.209 0.359 ! 0.86 eA-3 Q131 0.795 0.802 0.576 ! 0.86 eA-3 Q132 0.778 0.569 0.417 ! 0.85 eA-3 Q133 0.876 0.978 0.706 ! 0.85 eA-3 Q134 0.099 0.640 0.162 ! 0.85 eA-3 Q135 0.228 0.305 0.757 ! 0.83 eA-3 Q136 0.572 0.210 0.183 ! 0.83 eA-3 Q137 0.235 0.134 0.091 ! 0.83 eA-3 Q138 0.154 0.095 0.146 ! 0.82 eA-3 Q139 0.464 0.399 0.490 ! 0.82 eA-3 Q140 0.028 0.867 0.668 ! 0.82 eA-3 Q141 0.608 0.631 0.457 ! 0.82 eA-3 Q142 0.163 0.197 0.108 ! 0.82 eA-3 Q143 0.167 0.291 0.319 ! 0.82 eA-3 Q144 0.016 0.138 0.369 ! 0.81 eA-3 Q145 0.947 0.345 0.985 ! 0.81 eA-3 Q146 0.699 0.478 0.416 ! 0.80 eA-3 Q147 0.279 0.579 0.161 ! 0.80 eA-3 C148 0.497 0.547 0.037 ! 0.80 eA-3 Q149 0.546 0.570 0.265 ! 0.80 eA-3 Q150 0.806 0.509 0.635 ! 0.80 eA-3 Q151 0.841 0.407 0.766 ! 0.80 eA-3 Q152 0.325 0.578 0.488 ! 0.80 eA-3 Q153 0.694 0.006 0.869 ! 0.79 eA-3 Q154 0.078 0.173 0.117 ! 0.79 eA-3 Q155 0.426 0.517 0.426 ! 0.79 eA-3 Q156 0.077 0.711 0.467 ! 0.79 eA-3 Q157 0.903 0.211 0.131 ! 0.78 eA-3 Q158 0.466 0.789 0.271 ! 0.78 eA-3 Q159 0.717 0.220 0.460 ! 0.78 eA-3 Q160 0.012 0.727 0.295 ! 0.78 eA-3 Q161 0.286 0.258 0.573 ! 0.77 eA-3 Q162 0.616 0.516 0.712 ! 0.77 eA-3 Q163 0.706 0.376 0.371 ! 0.77 eA-3 Q164 0.238 0.071 0.863 ! 0.76 eA-3 Q165 0.195 0.721 0.062 ! 0.76 eA-3 Q166 0.300 0.366 0.042 ! 0.75 eA-3 Q167 0.307 0.491 0.391 ! 0.75 eA-3 Q168 0.100 0.437 0.071 ! 0.75 eA-3 Q169 0.707 0.416 0.386 ! 0.75 eA-3 Q170 0.751 0.993 0.314 ! 0.75 eA-3 Q171 0.058 0.415 0.519 ! 0.75 eA-3 Q172 0.438 0.838 0.648 ! 0.74 eA-3 Q173 0.223 0.430 0.534 ! 0.74 eA-3 Q174 0.246 0.096 0.244 ! 0.74 eA-3 Q175 0.657 0.079 0.000 ! 0.74 eA-3 Q176 0.621 0.514 0.268 ! 0.73 eA-3 Q177 0.595 0.893 0.187 ! 0.73 eA-3 Q178 0.577 0.789 0.453 ! 0.73 eA-3 Q179 0.521 0.834 0.344 ! 0.73 eA-3 Q180 0.383 0.565 0.223 ! 0.72 eA-3 Q181 0.082 0.571 0.315 ! 0.72 eA-3 Q182 0.194 0.626 0.262 ! 0.72 eA-3 Q183 0.124 0.682 0.185 ! 0.72 eA-3 Q184 0.580 0.415 0.340 ! 0.72 eA-3 Q185 0.480 0.685 0.116 ! 0.71 eA-3 Q186 0.969 0.444 0.338 ! 0.71 eA-3 Q187 0.456 0.356 0.672 ! 0.71 eA-3 Q188 0.354 0.747 0.023 ! 0.71 eA-3 Q189 0.462 0.733 0.234 ! 0.71 eA-3 Q190 0.852 0.907 0.305 ! 0.71 eA-3 Q191 0.160 0.070 0.093 ! 0.71 eA-3 Q192 0.765 0.265 0.232 ! 0.70 eA-3 Q193 0.758 0.610 0.188 ! 0.70 eA-3 Q194 0.267 0.726 0.057 ! 0.70 eA-3 C195 0.440 0.491 0.126 ! 0.70 eA-3 Q196 0.874 0.572 0.192 ! 0.70 eA-3 Q197 0.939 0.507 0.359 ! 0.70 eA-3 Q198 0.725 0.460 0.469 ! 0.70 eA-3 Q199 1.008 0.171 0.399 ! 0.70 eA-3 ) ; _shelx_fab_checksum 39986