# Electronic Supplementary Material (ESI) for Chemical Science. # This journal is © The Royal Society of Chemistry 2022 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3a _database_code_depnum_ccdc_archive 'CCDC 2116002' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C64 H84 Cr Mg2 N4 O6, C7 H8' _chemical_formula_sum 'C71 H92 Cr Mg2 N4 O6' _chemical_formula_weight 1198.10 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr -0.1635 2.4439 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.1719 0.1771 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_H-M_alt 'P n a 21' _space_group_name_Hall 'P 2c -2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 35.2188(4) _cell_length_b 15.39140(16) _cell_length_c 12.77462(11) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 6924.70(12) _cell_formula_units_Z 4 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 6951 _cell_measurement_theta_min 4.2660 _cell_measurement_theta_max 73.5620 _exptl_crystal_description plates _exptl_crystal_colour Yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.149 _exptl_crystal_F_000 2568 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.37 _exptl_crystal_size_mid 0.27 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 1.934 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type analytical _exptl_absorpt_correction_T_min 0.660 _exptl_absorpt_correction_T_max 0.904 _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'Enhance Ultra (Cu) X-ray Source' _diffrn_measurement_device_type 'Agilent Xcalibur PX Ultra A' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean 10.3745 _diffrn_reflns_number 14191 _diffrn_reflns_av_unetI/netI 0.0426 _diffrn_reflns_av_R_equivalents 0.0276 _diffrn_reflns_limit_h_min -42 _diffrn_reflns_limit_h_max 43 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 3.814 _diffrn_reflns_theta_max 73.759 _diffrn_reflns_theta_full 67.684 _diffrn_measured_fraction_theta_max 0.959 _diffrn_measured_fraction_theta_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.959 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.697 _diffrn_reflns_point_group_measured_fraction_full 0.731 _reflns_number_total 9749 _reflns_number_gt 8954 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.387 _reflns_Friedel_fraction_max 0.408 _reflns_Friedel_fraction_full 0.449 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro, Agilent Technologies' _computing_cell_refinement 'CrysAlisPro, Agilent Technologies' _computing_data_reduction 'CrysAlisPro, Agilent Technologies' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2014)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0536P)^2^+0.5382P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2322 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.002(4) _chemical_absolute_configuration . _refine_ls_number_reflns 9749 _refine_ls_number_parameters 797 _refine_ls_number_restraints 56 _refine_ls_R_factor_all 0.0427 _refine_ls_R_factor_gt 0.0376 _refine_ls_wR_factor_ref 0.0978 _refine_ls_wR_factor_gt 0.0931 _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_restrained_S_all 1.029 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cr1 Cr 0.67626(2) 0.68153(3) 0.23143(4) 0.04587(13) Uani 1 1 d . . . . . Mg1 Mg 0.63492(2) 0.65273(6) 0.58429(7) 0.03378(17) Uani 1 1 d . . . . . Mg2 Mg 0.60625(2) 0.85421(5) 0.47425(7) 0.03233(17) Uani 1 1 d . . . . . H1 H 0.6159(10) 0.769(2) 0.549(3) 0.049(9) Uiso 1 1 d . . . . . N1 N 0.59768(6) 0.59100(15) 0.68241(17) 0.0353(4) Uani 1 1 d . . . . . C1 C 0.60718(8) 0.57579(19) 0.7811(2) 0.0385(6) Uani 1 1 d . . . . . C2 C 0.64361(8) 0.5893(2) 0.8229(2) 0.0410(6) Uani 1 1 d . . . . . H2A H 0.6450 0.5873 0.8971 0.049 Uiso 1 1 calc R U . . . C3 C 0.67841(8) 0.6052(2) 0.7721(2) 0.0392(6) Uani 1 1 d . . . . . N3 N 0.68151(6) 0.62331(15) 0.67057(18) 0.0348(4) Uani 1 1 d . . . . . C4 C 0.57859(9) 0.5393(3) 0.8578(2) 0.0524(7) Uani 1 1 d . . . . . H4A H 0.5620 0.5860 0.8826 0.079 Uiso 1 1 calc R U . . . H4B H 0.5920 0.5134 0.9174 0.079 Uiso 1 1 calc R U . . . H4C H 0.5633 0.4947 0.8230 0.079 Uiso 1 1 calc R U . . . C5 C 0.71326(9) 0.6002(3) 0.8405(3) 0.0603(9) Uani 1 1 d . . . . . H5A H 0.7237 0.6587 0.8504 0.090 Uiso 1 1 calc R U . . . H5B H 0.7323 0.5631 0.8070 0.090 Uiso 1 1 calc R U . . . H5C H 0.7064 0.5757 0.9087 0.090 Uiso 1 1 calc R U . . . C6 C 0.56071(8) 0.56428(19) 0.6478(2) 0.0392(6) Uani 1 1 d . . . . . C7 C 0.52844(8) 0.6155(2) 0.6686(2) 0.0434(6) Uani 1 1 d . . . . . C8 C 0.49316(9) 0.5851(3) 0.6340(3) 0.0528(7) Uani 1 1 d . . . . . H8A H 0.4711 0.6190 0.6469 0.063 Uiso 1 1 calc R U . . . C9 C 0.48966(10) 0.5072(3) 0.5817(3) 0.0606(9) Uani 1 1 d . . . . . H9A H 0.4653 0.4868 0.5612 0.073 Uiso 1 1 calc R U . . . C10 C 0.52138(11) 0.4592(2) 0.5594(3) 0.0552(8) Uani 1 1 d . . . . . H10A H 0.5188 0.4062 0.5220 0.066 Uiso 1 1 calc R U . . . C11 C 0.55746(9) 0.48648(19) 0.5904(2) 0.0460(6) Uani 1 1 d . . . . . C12 C 0.53042(7) 0.7031(2) 0.7232(2) 0.0433(6) Uani 1 1 d . . . . . H12A H 0.5565 0.7098 0.7530 0.052 Uiso 1 1 calc R U . . . C13 C 0.52388(10) 0.7769(2) 0.6463(3) 0.0534(7) Uani 1 1 d . . . . . H13A H 0.5431 0.7745 0.5910 0.080 Uiso 1 1 calc R U . . . H13B H 0.5258 0.8326 0.6832 0.080 Uiso 1 1 calc R U . . . H13C H 0.4986 0.7712 0.6153 0.080 Uiso 1 1 calc R U . . . C14 C 0.50188(11) 0.7114(3) 0.8133(3) 0.0655(9) Uani 1 1 d . . . . . H14A H 0.4760 0.7072 0.7856 0.098 Uiso 1 1 calc R U . . . H14B H 0.5052 0.7678 0.8479 0.098 Uiso 1 1 calc R U . . . H14C H 0.5062 0.6647 0.8640 0.098 Uiso 1 1 calc R U . . . C15 C 0.59225(11) 0.4327(2) 0.5626(3) 0.0535(7) Uani 1 1 d . . . . . H15A H 0.6144 0.4732 0.5656 0.064 Uiso 1 1 calc R U . . . C16 C 0.59984(17) 0.3631(4) 0.6423(4) 0.0875(14) Uani 1 1 d . . . . . H16A H 0.6012 0.3893 0.7122 0.131 Uiso 1 1 calc R U . . . H16B H 0.6240 0.3345 0.6263 0.131 Uiso 1 1 calc R U . . . H16C H 0.5793 0.3202 0.6406 0.131 Uiso 1 1 calc R U . . . C17 C 0.59143(18) 0.3964(4) 0.4521(4) 0.0926(15) Uani 1 1 d . . . . . H17A H 0.5747 0.3455 0.4498 0.139 Uiso 1 1 calc R U . . . H17B H 0.6172 0.3793 0.4313 0.139 Uiso 1 1 calc R U . . . H17C H 0.5819 0.4409 0.4039 0.139 Uiso 1 1 calc R U . . . C18 C 0.71894(7) 0.6184(2) 0.6252(2) 0.0388(6) Uani 1 1 d . . . . . C19 C 0.73123(9) 0.5383(2) 0.5850(3) 0.0507(7) Uani 1 1 d . . . . . C20 C 0.76766(11) 0.5331(2) 0.5421(3) 0.0606(9) Uani 1 1 d . . . . . H20A H 0.7766 0.4790 0.5160 0.073 Uiso 1 1 calc R U . . . C21 C 0.79096(9) 0.6052(3) 0.5370(3) 0.0589(9) Uani 1 1 d . . . . . H21A H 0.8157 0.6006 0.5081 0.071 Uiso 1 1 calc R U . . . C22 C 0.77812(8) 0.6828(2) 0.5738(3) 0.0527(7) Uani 1 1 d . . . . . H22A H 0.7942 0.7323 0.5694 0.063 Uiso 1 1 calc R U . . . C23 C 0.74200(8) 0.6919(2) 0.6179(2) 0.0427(6) Uani 1 1 d . . . . . C24 C 0.70640(12) 0.4574(2) 0.5872(5) 0.0763(13) Uani 1 1 d . . . . . H24A H 0.6799 0.4762 0.6043 0.092 Uiso 1 1 calc R U . . . C25 C 0.7195(2) 0.3956(3) 0.6738(6) 0.114(2) Uani 1 1 d . . . . . H25A H 0.7466 0.3832 0.6652 0.171 Uiso 1 1 calc R U . . . H25B H 0.7051 0.3413 0.6694 0.171 Uiso 1 1 calc R U . . . H25C H 0.7152 0.4226 0.7422 0.171 Uiso 1 1 calc R U . . . C26 C 0.70530(19) 0.4122(3) 0.4828(7) 0.1028(19) Uani 1 1 d . . . . . H26A H 0.6977 0.4536 0.4285 0.154 Uiso 1 1 calc R U . . . H26B H 0.6870 0.3644 0.4855 0.154 Uiso 1 1 calc R U . . . H26C H 0.7306 0.3891 0.4665 0.154 Uiso 1 1 calc R U . . . C27 C 0.72895(9) 0.7802(2) 0.6565(3) 0.0506(7) Uani 1 1 d . . . . . H27A H 0.7041 0.7718 0.6930 0.061 Uiso 1 1 calc R U . . . C28 C 0.72226(11) 0.8417(2) 0.5656(3) 0.0623(9) Uani 1 1 d . . . . . H28A H 0.7463 0.8522 0.5291 0.093 Uiso 1 1 calc R U . . . H28B H 0.7122 0.8968 0.5920 0.093 Uiso 1 1 calc R U . . . H28C H 0.7040 0.8157 0.5170 0.093 Uiso 1 1 calc R U . . . C29 C 0.75661(13) 0.8206(3) 0.7353(4) 0.0757(10) Uani 1 1 d . . . . . H29A H 0.7617 0.7790 0.7916 0.114 Uiso 1 1 calc R U . . . H29B H 0.7454 0.8734 0.7649 0.114 Uiso 1 1 calc R U . . . H29C H 0.7804 0.8353 0.6998 0.114 Uiso 1 1 calc R U . . . N31 N 0.60440(6) 0.96336(14) 0.56415(17) 0.0334(4) Uani 1 1 d . . . . . C31 C 0.57309(8) 1.01183(17) 0.5706(2) 0.0388(5) Uani 1 1 d . . . . . C32 C 0.53908(8) 0.9924(2) 0.5182(3) 0.0448(6) Uani 1 1 d . . . . . H32A H 0.5172 1.0208 0.5449 0.054 Uiso 1 1 calc R U . . . N33 N 0.55854(6) 0.88405(15) 0.39269(18) 0.0363(5) Uani 1 1 d . . . . . C33 C 0.53257(8) 0.9380(2) 0.4333(3) 0.0439(6) Uani 1 1 d . . . . . C34 C 0.57293(10) 1.0951(2) 0.6340(3) 0.0539(7) Uani 1 1 d . . . . . H34A H 0.5862 1.0854 0.7005 0.081 Uiso 1 1 calc R U . . . H34B H 0.5467 1.1126 0.6480 0.081 Uiso 1 1 calc R U . . . H34C H 0.5859 1.1410 0.5946 0.081 Uiso 1 1 calc R U . . . C35 C 0.49348(10) 0.9423(3) 0.3840(4) 0.0692(11) Uani 1 1 d . . . . . H35A H 0.4956 0.9654 0.3128 0.104 Uiso 1 1 calc R U . . . H35B H 0.4771 0.9804 0.4258 0.104 Uiso 1 1 calc R U . . . H35C H 0.4824 0.8839 0.3815 0.104 Uiso 1 1 calc R U . . . C36 C 0.63706(7) 0.99164(18) 0.6234(2) 0.0398(6) Uani 1 1 d . . . . . C37 C 0.64301(7) 0.9558(2) 0.7238(3) 0.0456(6) Uani 1 1 d . . . . . C38 C 0.67389(9) 0.9862(3) 0.7820(3) 0.0644(10) Uani 1 1 d . . . . . H38A H 0.6782 0.9637 0.8503 0.077 Uiso 1 1 calc R U . . . C39 C 0.69807(11) 1.0477(3) 0.7426(4) 0.0778(13) Uani 1 1 d . . . . . H39A H 0.7185 1.0685 0.7843 0.093 Uiso 1 1 calc R U . . . C40 C 0.69307(10) 1.0794(3) 0.6434(5) 0.0720(12) Uani 1 1 d . . . . . H40A H 0.7106 1.1207 0.6167 0.086 Uiso 1 1 calc R U . . . C41 C 0.66230(9) 1.0519(2) 0.5795(3) 0.0522(8) Uani 1 1 d . . . . . C42 C 0.61678(9) 0.8878(2) 0.7693(2) 0.0480(7) Uani 1 1 d . . . . . H42A H 0.6077 0.8519 0.7091 0.058 Uiso 1 1 calc R U . . . C43 C 0.63517(13) 0.8250(3) 0.8465(4) 0.0763(12) Uani 1 1 d . . . . . H43A H 0.6582 0.8002 0.8152 0.114 Uiso 1 1 calc R U . . . H43B H 0.6173 0.7781 0.8631 0.114 Uiso 1 1 calc R U . . . H43C H 0.6419 0.8561 0.9108 0.114 Uiso 1 1 calc R U . . . C44 C 0.58181(11) 0.9268(3) 0.8186(3) 0.0601(8) Uani 1 1 d . . . . . H44A H 0.5894 0.9699 0.8711 0.090 Uiso 1 1 calc R U . . . H44B H 0.5669 0.8809 0.8522 0.090 Uiso 1 1 calc R U . . . H44C H 0.5664 0.9550 0.7644 0.090 Uiso 1 1 calc R U . . . C45 C 0.65831(11) 1.0827(2) 0.4684(4) 0.0635(9) Uani 1 1 d . . . . . H45A H 0.6322 1.0677 0.4437 0.076 Uiso 1 1 calc R U . . . C46 C 0.6634(3) 1.1813(3) 0.4587(7) 0.122(3) Uani 1 1 d . . . . . H46A H 0.6470 1.2106 0.5096 0.183 Uiso 1 1 calc R U . . . H46B H 0.6565 1.1998 0.3878 0.183 Uiso 1 1 calc R U . . . H46C H 0.6900 1.1965 0.4725 0.183 Uiso 1 1 calc R U . . . C47 C 0.68661(14) 1.0375(4) 0.3976(4) 0.0811(12) Uani 1 1 d . . . . . H47A H 0.7123 1.0445 0.4262 0.122 Uiso 1 1 calc R U . . . H47B H 0.6855 1.0631 0.3275 0.122 Uiso 1 1 calc R U . . . H47C H 0.6804 0.9755 0.3935 0.122 Uiso 1 1 calc R U . . . C48 C 0.55238(8) 0.8534(2) 0.2875(2) 0.0419(6) Uani 1 1 d . . . . . C49 C 0.56663(11) 0.9039(2) 0.2050(3) 0.0544(8) Uani 1 1 d . . . . . C50 C 0.56047(14) 0.8753(3) 0.1032(3) 0.0695(11) Uani 1 1 d . . . . . H50A H 0.5695 0.9091 0.0462 0.083 Uiso 1 1 calc R U . . . C51 C 0.54147(15) 0.7988(3) 0.0833(3) 0.0744(11) Uani 1 1 d . . . . . H51A H 0.5374 0.7805 0.0132 0.089 Uiso 1 1 calc R U . . . C52 C 0.52846(12) 0.7493(3) 0.1642(3) 0.0622(9) Uani 1 1 d . . . . . H52A H 0.5156 0.6965 0.1496 0.075 Uiso 1 1 calc R U . . . C53 C 0.53369(9) 0.7748(2) 0.2679(2) 0.0459(7) Uani 1 1 d . . . . . C54 C 0.58782(14) 0.9887(3) 0.2241(3) 0.0705(10) Uani 1 1 d . . . . . H54A H 0.5981 0.9861 0.2970 0.085 Uiso 1 1 calc R U . . . C55 C 0.5615(2) 1.0661(3) 0.2191(6) 0.1024(18) Uani 1 1 d . . . . . H55A H 0.5514 1.0719 0.1479 0.154 Uiso 1 1 calc R U . . . H55B H 0.5755 1.1188 0.2377 0.154 Uiso 1 1 calc R U . . . H55C H 0.5404 1.0578 0.2683 0.154 Uiso 1 1 calc R U . . . C56 C 0.62177(17) 1.0016(4) 0.1508(5) 0.0970(17) Uani 1 1 d . . . . . H56A H 0.6376 0.9493 0.1513 0.146 Uiso 1 1 calc R U . . . H56B H 0.6368 1.0514 0.1747 0.146 Uiso 1 1 calc R U . . . H56C H 0.6126 1.0125 0.0796 0.146 Uiso 1 1 calc R U . . . C57 C 0.52087(10) 0.7162(2) 0.3561(3) 0.0513(7) Uani 1 1 d . . . . . H57A H 0.5209 0.7508 0.4223 0.062 Uiso 1 1 calc R U . . . C58 C 0.54823(13) 0.6415(3) 0.3691(3) 0.0713(11) Uani 1 1 d . . . . . H58A H 0.5485 0.6064 0.3050 0.107 Uiso 1 1 calc R U . . . H58B H 0.5402 0.6054 0.4282 0.107 Uiso 1 1 calc R U . . . H58C H 0.5738 0.6642 0.3823 0.107 Uiso 1 1 calc R U . . . C59 C 0.48071(13) 0.6808(4) 0.3392(4) 0.0822(13) Uani 1 1 d . . . . . H59A H 0.4637 0.7285 0.3194 0.123 Uiso 1 1 calc R U . . . H59B H 0.4716 0.6540 0.4041 0.123 Uiso 1 1 calc R U . . . H59C H 0.4811 0.6372 0.2833 0.123 Uiso 1 1 calc R U . . . C61 C 0.6575(2) 0.6015(8) 0.3492(5) 0.065(2) Uani 0.616(16) 1 d . U P A 1 H61A H 0.6549 0.5424 0.3289 0.078 Uiso 0.616(16) 1 calc R U P A 1 C61' C 0.6629(3) 0.6419(9) 0.3597(8) 0.045(2) Uiso 0.384(16) 1 d . U P A 2 O61 O 0.64929(7) 0.61556(16) 0.43962(16) 0.0475(5) Uani 1 1 d . . . . . C62 C 0.65184(17) 0.7698(5) 0.2992(4) 0.0444(15) Uani 0.616(16) 1 d . U P A 1 C62' C 0.6621(4) 0.8039(10) 0.2860(9) 0.054(3) Uiso 0.384(16) 1 d . U P A 2 H62A H 0.6738 0.8504 0.2492 0.065 Uiso 0.384(16) 1 calc R U P A 2 O62 O 0.64172(6) 0.82607(15) 0.35595(17) 0.0472(5) Uani 1 1 d . . . . . C63 C 0.69000(12) 0.7470(3) 0.1106(3) 0.0612(9) Uani 1 1 d . . . . . O63 O 0.69825(12) 0.7877(3) 0.0402(3) 0.1001(13) Uani 1 1 d . . . . . C64 C 0.69898(11) 0.5792(3) 0.1739(3) 0.0634(9) Uani 1 1 d . . . . . O64 O 0.71187(10) 0.5186(2) 0.1383(4) 0.1019(13) Uani 1 1 d . . . . . C65 C 0.72260(12) 0.7111(3) 0.2981(3) 0.0595(9) Uani 1 1 d . . . . . O65 O 0.75038(11) 0.7314(3) 0.3367(3) 0.0857(9) Uani 1 1 d . . . . . C66 C 0.62967(12) 0.6504(3) 0.1656(3) 0.0681(10) Uani 1 1 d . . . . . O66 O 0.60241(10) 0.6282(3) 0.1248(4) 0.1000(12) Uani 1 1 d . . . . . C70 C 0.3823(4) 0.6275(11) 0.6648(13) 0.132(5) Uani 0.535(11) 1 d D U P B 2 H70A H 0.3833 0.5644 0.6555 0.199 Uiso 0.535(11) 1 calc R U P B 2 H70B H 0.3613 0.6424 0.7118 0.199 Uiso 0.535(11) 1 calc R U P B 2 H70C H 0.4062 0.6478 0.6953 0.199 Uiso 0.535(11) 1 calc R U P B 2 C71 C 0.3764(2) 0.6693(5) 0.5636(7) 0.093(3) Uani 0.535(11) 1 d DG . P B 2 C72 C 0.3946(2) 0.7476(5) 0.5426(8) 0.101(5) Uani 0.535(11) 1 d DG U P B 2 H72A H 0.4118 0.7715 0.5921 0.121 Uiso 0.535(11) 1 calc R U P B 2 C73 C 0.3875(3) 0.7909(6) 0.4491(9) 0.144(7) Uani 0.535(11) 1 d G . P B 2 H73A H 0.3999 0.8444 0.4347 0.173 Uiso 0.535(11) 1 calc R U P B 2 C74 C 0.3624(3) 0.7559(8) 0.3766(7) 0.142(6) Uani 0.535(11) 1 d G U P B 2 H74A H 0.3576 0.7856 0.3127 0.170 Uiso 0.535(11) 1 calc R U P B 2 C75 C 0.3443(3) 0.6776(8) 0.3976(7) 0.126(5) Uani 0.535(11) 1 d G U P B 2 H75A H 0.3271 0.6537 0.3480 0.151 Uiso 0.535(11) 1 calc R U P B 2 C76 C 0.3513(2) 0.6343(5) 0.4911(8) 0.115(5) Uani 0.535(11) 1 d DG U P B 2 H76A H 0.3389 0.5808 0.5054 0.138 Uiso 0.535(11) 1 calc R U P B 2 C70' C 0.3771(6) 0.7965(12) 0.3705(15) 0.121(6) Uiso 0.465(11) 1 d D U P B 1 H70D H 0.3614 0.7776 0.3114 0.181 Uiso 0.465(11) 1 calc R U P B 1 H70E H 0.4037 0.8009 0.3480 0.181 Uiso 0.465(11) 1 calc R U P B 1 H70F H 0.3684 0.8534 0.3950 0.181 Uiso 0.465(11) 1 calc R U P B 1 C71' C 0.3741(3) 0.7332(5) 0.4558(6) 0.073(3) Uiso 0.465(11) 1 d DG . P B 1 C72' C 0.3550(3) 0.6549(6) 0.4434(7) 0.111(5) Uiso 0.465(11) 1 d DG U P B 1 H72B H 0.3435 0.6411 0.3783 0.133 Uiso 0.465(11) 1 calc R U P B 1 C73' C 0.3527(4) 0.5967(6) 0.5264(9) 0.129(6) Uiso 0.465(11) 1 d G U P B 1 H73B H 0.3396 0.5432 0.5180 0.155 Uiso 0.465(11) 1 calc R U P B 1 C74' C 0.3696(3) 0.6169(6) 0.6218(7) 0.112(5) Uiso 0.465(11) 1 d G U P B 1 H74B H 0.3680 0.5771 0.6785 0.134 Uiso 0.465(11) 1 calc R U P B 1 C75' C 0.3887(3) 0.6952(7) 0.6341(6) 0.100(4) Uiso 0.465(11) 1 d G . P B 1 H75B H 0.4002 0.7090 0.6993 0.120 Uiso 0.465(11) 1 calc R U P B 1 C76' C 0.3910(3) 0.7534(6) 0.5511(7) 0.115(7) Uiso 0.465(11) 1 d DG U P B 1 H76B H 0.4040 0.8069 0.5596 0.138 Uiso 0.465(11) 1 calc R U P B 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cr1 0.0577(3) 0.0495(3) 0.03042(19) 0.0008(2) 0.0090(2) 0.0125(2) Mg1 0.0342(4) 0.0375(4) 0.0297(4) 0.0068(3) -0.0015(3) -0.0032(3) Mg2 0.0310(3) 0.0317(4) 0.0343(4) -0.0043(3) -0.0048(3) 0.0035(3) N1 0.0357(10) 0.0391(11) 0.0312(10) 0.0040(9) -0.0009(8) -0.0077(9) C1 0.0399(12) 0.0451(14) 0.0305(12) 0.0048(11) 0.0022(11) -0.0030(11) C2 0.0409(13) 0.0555(16) 0.0266(11) 0.0066(11) -0.0008(10) -0.0027(12) C3 0.0364(12) 0.0478(15) 0.0335(12) 0.0055(11) -0.0020(10) 0.0016(11) N3 0.0325(9) 0.0385(11) 0.0333(10) 0.0027(9) 0.0022(8) 0.0029(9) C4 0.0464(15) 0.073(2) 0.0384(14) 0.0167(14) 0.0018(12) -0.0117(15) C5 0.0398(15) 0.095(3) 0.0463(16) 0.0158(18) -0.0049(13) 0.0025(17) C6 0.0401(12) 0.0457(14) 0.0318(11) 0.0079(11) -0.0013(10) -0.0123(11) C7 0.0381(12) 0.0551(16) 0.0370(13) 0.0057(12) -0.0028(10) -0.0104(12) C8 0.0394(13) 0.069(2) 0.0504(16) 0.0062(16) -0.0060(12) -0.0128(15) C9 0.0532(17) 0.072(2) 0.0567(18) 0.0084(18) -0.0147(15) -0.0286(17) C10 0.0673(19) 0.0501(16) 0.0481(16) 0.0045(14) -0.0092(14) -0.0246(16) C11 0.0586(16) 0.0420(14) 0.0374(13) 0.0058(12) -0.0039(13) -0.0136(13) C12 0.0373(12) 0.0553(15) 0.0373(13) 0.0001(13) -0.0002(11) -0.0019(11) C13 0.0512(15) 0.0583(18) 0.0508(17) 0.0011(15) -0.0024(14) -0.0023(15) C14 0.0583(19) 0.092(3) 0.0463(17) -0.0019(18) 0.0121(15) -0.002(2) C15 0.0649(18) 0.0411(14) 0.0544(18) -0.0032(14) 0.0051(15) -0.0090(14) C16 0.105(3) 0.088(3) 0.069(3) 0.021(2) 0.016(3) 0.026(3) C17 0.108(4) 0.109(4) 0.061(2) -0.021(3) -0.003(2) 0.021(3) C18 0.0334(12) 0.0479(15) 0.0350(12) 0.0063(11) 0.0017(10) 0.0056(11) C19 0.0455(14) 0.0467(15) 0.0600(17) 0.0042(15) 0.0116(14) 0.0098(13) C20 0.0576(18) 0.0538(18) 0.071(2) 0.0055(17) 0.0193(17) 0.0186(16) C21 0.0418(14) 0.073(2) 0.062(2) 0.0104(18) 0.0165(15) 0.0115(16) C22 0.0382(13) 0.0626(18) 0.0572(17) 0.0041(16) 0.0072(13) -0.0035(13) C23 0.0348(12) 0.0523(16) 0.0411(13) 0.0008(12) 0.0010(10) 0.0018(12) C24 0.067(2) 0.0406(16) 0.121(4) -0.002(2) 0.035(3) 0.0067(16) C25 0.151(6) 0.066(3) 0.124(5) 0.026(3) 0.057(5) -0.002(3) C26 0.111(4) 0.058(2) 0.139(6) -0.023(3) 0.014(4) -0.007(3) C27 0.0414(13) 0.0524(17) 0.0579(18) -0.0113(15) 0.0057(13) -0.0066(13) C28 0.0616(18) 0.0530(17) 0.072(2) -0.0085(17) -0.0023(17) 0.0115(16) C29 0.078(2) 0.075(2) 0.074(2) -0.018(2) -0.016(2) -0.011(2) N31 0.0294(9) 0.0324(10) 0.0384(11) -0.0054(9) 0.0011(8) 0.0009(8) C31 0.0385(12) 0.0360(12) 0.0420(13) -0.0024(11) 0.0057(11) 0.0056(11) C32 0.0348(12) 0.0477(15) 0.0517(15) -0.0023(13) 0.0007(11) 0.0144(12) N33 0.0353(10) 0.0386(11) 0.0349(10) 0.0017(9) -0.0066(9) 0.0031(9) C33 0.0355(12) 0.0472(15) 0.0488(14) 0.0017(12) -0.0076(11) 0.0099(12) C34 0.0546(16) 0.0430(15) 0.0642(19) -0.0160(15) 0.0072(15) 0.0114(14) C35 0.0425(16) 0.086(3) 0.079(2) -0.014(2) -0.0195(17) 0.0204(18) C36 0.0311(11) 0.0379(13) 0.0504(14) -0.0156(12) 0.0045(11) -0.0004(11) C37 0.0341(11) 0.0589(16) 0.0438(14) -0.0200(14) -0.0007(11) 0.0047(12) C38 0.0427(15) 0.093(3) 0.0574(19) -0.032(2) -0.0082(14) 0.0005(18) C39 0.0505(18) 0.098(3) 0.085(3) -0.038(3) -0.0086(19) -0.016(2) C40 0.0454(16) 0.061(2) 0.109(4) -0.027(2) 0.013(2) -0.0180(16) C41 0.0402(13) 0.0406(14) 0.076(2) -0.0163(16) 0.0129(15) -0.0070(12) C42 0.0486(15) 0.0591(18) 0.0362(12) -0.0066(13) 0.0014(12) 0.0060(14) C43 0.067(2) 0.085(3) 0.077(3) 0.010(2) 0.004(2) 0.026(2) C44 0.0571(18) 0.074(2) 0.0497(17) 0.0016(16) 0.0073(15) 0.0105(18) C45 0.0557(17) 0.0419(15) 0.093(3) 0.0025(18) 0.023(2) -0.0088(15) C46 0.182(7) 0.056(2) 0.128(6) 0.013(3) 0.047(5) -0.005(4) C47 0.071(2) 0.090(3) 0.083(3) -0.007(3) 0.022(2) 0.000(2) C48 0.0412(13) 0.0495(15) 0.0350(13) 0.0042(12) -0.0110(11) 0.0040(12) C49 0.0679(19) 0.0532(17) 0.0421(16) 0.0116(13) -0.0104(14) 0.0004(16) C50 0.100(3) 0.074(2) 0.0349(16) 0.0176(16) -0.0108(16) -0.009(2) C51 0.109(3) 0.080(2) 0.0348(15) 0.0017(17) -0.0216(19) -0.006(2) C52 0.077(2) 0.066(2) 0.0427(16) -0.0014(16) -0.0189(16) -0.0121(19) C53 0.0511(15) 0.0509(16) 0.0358(13) -0.0008(12) -0.0131(12) -0.0011(14) C54 0.100(3) 0.0594(19) 0.0522(18) 0.0163(18) -0.009(2) -0.013(2) C55 0.145(5) 0.056(2) 0.107(4) 0.011(3) 0.007(4) -0.004(3) C56 0.105(4) 0.093(3) 0.093(4) 0.026(3) 0.005(3) -0.034(3) C57 0.0538(16) 0.0600(18) 0.0400(14) -0.0003(14) -0.0052(13) -0.0154(15) C58 0.076(2) 0.079(3) 0.060(2) 0.029(2) -0.0003(18) -0.003(2) C59 0.063(2) 0.107(4) 0.077(3) 0.001(3) -0.007(2) -0.029(2) C61 0.083(4) 0.070(5) 0.043(3) 0.008(3) 0.009(3) -0.003(4) O61 0.0583(12) 0.0541(12) 0.0301(9) -0.0019(8) 0.0058(8) 0.0049(10) C62 0.044(2) 0.044(3) 0.045(2) 0.002(2) 0.011(2) -0.011(3) O62 0.0470(10) 0.0534(12) 0.0413(10) -0.0058(9) 0.0092(9) 0.0073(9) C63 0.074(2) 0.070(2) 0.0395(16) 0.0050(15) -0.0033(15) -0.0075(19) O63 0.118(3) 0.129(3) 0.0536(17) 0.0356(19) -0.0129(17) -0.043(3) C64 0.0581(18) 0.064(2) 0.068(2) -0.0110(19) 0.0045(17) 0.0039(18) O64 0.087(2) 0.081(2) 0.137(3) -0.050(2) -0.004(2) 0.0284(19) C65 0.076(2) 0.063(2) 0.0395(15) -0.0051(15) -0.0036(16) 0.0211(18) O65 0.091(2) 0.099(2) 0.0680(18) -0.0117(17) -0.0241(17) 0.0151(19) C66 0.064(2) 0.087(3) 0.0528(19) -0.0037(19) 0.0107(18) 0.012(2) O66 0.0681(18) 0.141(3) 0.090(2) -0.021(3) -0.0047(18) -0.001(2) C70 0.082(7) 0.173(13) 0.142(12) 0.018(11) -0.022(8) 0.002(8) C71 0.070(5) 0.102(7) 0.106(8) -0.010(6) -0.001(5) -0.003(5) C72 0.094(7) 0.085(7) 0.124(10) -0.046(7) 0.011(6) -0.032(5) C73 0.136(13) 0.118(11) 0.18(2) -0.009(13) 0.038(13) 0.035(11) C74 0.116(10) 0.174(14) 0.135(11) -0.049(12) 0.035(9) 0.044(11) C75 0.104(8) 0.158(12) 0.115(10) -0.041(10) -0.002(8) 0.034(9) C76 0.092(7) 0.108(8) 0.145(11) -0.071(9) -0.005(7) 0.023(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cr1 C61' 1.811(10) . ? Cr1 C62 1.826(5) . ? Cr1 C65 1.896(4) . ? Cr1 C66 1.905(5) . ? Cr1 C63 1.906(4) . ? Cr1 C64 1.913(4) . ? Cr1 C61 2.053(8) . ? Cr1 C62' 2.069(12) . ? Mg1 O61 2.000(2) . ? Mg1 N3 2.028(2) . ? Mg1 N1 2.048(2) . ? Mg1 Mg2 3.5515(11) . ? Mg2 O62 2.008(2) . ? Mg2 N33 2.030(2) . ? Mg2 N31 2.036(2) . ? N1 C1 1.326(3) . ? N1 C6 1.435(3) . ? C1 C2 1.405(4) . ? C1 C4 1.513(4) . ? C2 C3 1.408(4) . ? C3 N3 1.331(4) . ? C3 C5 1.509(4) . ? N3 C18 1.442(3) . ? C6 C7 1.409(5) . ? C6 C11 1.409(4) . ? C7 C8 1.399(4) . ? C7 C12 1.520(5) . ? C8 C9 1.378(6) . ? C9 C10 1.369(6) . ? C10 C11 1.396(5) . ? C11 C15 1.521(5) . ? C12 C13 1.518(5) . ? C12 C14 1.534(5) . ? C15 C16 1.501(6) . ? C15 C17 1.518(6) . ? C18 C23 1.395(4) . ? C18 C19 1.403(5) . ? C19 C20 1.397(5) . ? C19 C24 1.522(5) . ? C20 C21 1.382(6) . ? C21 C22 1.361(6) . ? C22 C23 1.398(4) . ? C23 C27 1.517(5) . ? C24 C26 1.505(9) . ? C24 C25 1.530(9) . ? C27 C28 1.516(6) . ? C27 C29 1.533(5) . ? N31 C31 1.334(3) . ? N31 C36 1.444(4) . ? C31 C32 1.404(4) . ? C31 C34 1.516(4) . ? C32 C33 1.390(5) . ? N33 C33 1.340(4) . ? N33 C48 1.441(4) . ? C33 C35 1.515(4) . ? C36 C41 1.402(4) . ? C36 C37 1.411(5) . ? C37 C38 1.398(4) . ? C37 C42 1.512(5) . ? C38 C39 1.370(7) . ? C39 C40 1.368(8) . ? C40 C41 1.421(6) . ? C41 C45 1.503(7) . ? C42 C44 1.508(5) . ? C42 C43 1.525(6) . ? C45 C47 1.516(6) . ? C45 C46 1.533(6) . ? C48 C53 1.400(5) . ? C48 C49 1.402(5) . ? C49 C50 1.390(5) . ? C49 C54 1.523(6) . ? C50 C51 1.378(6) . ? C51 C52 1.362(6) . ? C52 C53 1.394(5) . ? C53 C57 1.512(5) . ? C54 C55 1.511(7) . ? C54 C56 1.532(8) . ? C57 C58 1.509(6) . ? C57 C59 1.531(5) . ? C61 O61 1.211(8) . ? C61' O61 1.199(10) . ? C62 O62 1.184(6) . ? C62' O62 1.196(12) . ? C63 O63 1.133(5) . ? C64 O64 1.132(5) . ? C65 O65 1.140(6) . ? C66 O66 1.144(6) . ? C70 C71 1.459(16) . ? C71 C72 1.3900 . ? C71 C76 1.3900 . ? C72 C73 1.3900 . ? C73 C74 1.3900 . ? C74 C75 1.3900 . ? C75 C76 1.3900 . ? C70' C71' 1.466(17) . ? C71' C72' 1.3900 . ? C71' C76' 1.3900 . ? C72' C73' 1.3900 . ? C73' C74' 1.3900 . ? C74' C75' 1.3900 . ? C75' C76' 1.3900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C61' Cr1 C65 84.1(4) . . ? C62 Cr1 C65 90.8(2) . . ? C61' Cr1 C66 95.3(4) . . ? C62 Cr1 C66 89.5(2) . . ? C65 Cr1 C66 179.2(2) . . ? C61' Cr1 C63 167.7(4) . . ? C62 Cr1 C63 96.4(3) . . ? C65 Cr1 C63 91.05(17) . . ? C66 Cr1 C63 89.66(18) . . ? C61' Cr1 C64 100.3(4) . . ? C62 Cr1 C64 172.5(3) . . ? C65 Cr1 C64 90.59(16) . . ? C66 Cr1 C64 89.05(18) . . ? C63 Cr1 C64 91.02(19) . . ? C62 Cr1 C61 87.0(3) . . ? C65 Cr1 C61 95.2(3) . . ? C66 Cr1 C61 84.0(3) . . ? C63 Cr1 C61 172.8(3) . . ? C64 Cr1 C61 85.5(3) . . ? C61' Cr1 C62' 86.5(5) . . ? C65 Cr1 C62' 80.7(4) . . ? C66 Cr1 C62' 99.8(4) . . ? C63 Cr1 C62' 81.6(5) . . ? C64 Cr1 C62' 168.4(5) . . ? O61 Mg1 N3 103.51(10) . . ? O61 Mg1 N1 126.52(10) . . ? N3 Mg1 N1 94.70(10) . . ? O61 Mg1 Mg2 87.47(7) . . ? N3 Mg1 Mg2 129.80(7) . . ? N1 Mg1 Mg2 117.73(7) . . ? O62 Mg2 N33 100.22(10) . . ? O62 Mg2 N31 128.49(10) . . ? N33 Mg2 N31 94.38(9) . . ? O62 Mg2 Mg1 86.14(7) . . ? N33 Mg2 Mg1 129.51(7) . . ? N31 Mg2 Mg1 120.41(7) . . ? C1 N1 C6 118.1(2) . . ? C1 N1 Mg1 120.19(19) . . ? C6 N1 Mg1 121.69(17) . . ? N1 C1 C2 124.4(2) . . ? N1 C1 C4 120.9(3) . . ? C2 C1 C4 114.6(2) . . ? C1 C2 C3 130.2(2) . . ? N3 C3 C2 123.8(3) . . ? N3 C3 C5 120.6(3) . . ? C2 C3 C5 115.6(3) . . ? C3 N3 C18 117.1(2) . . ? C3 N3 Mg1 120.66(19) . . ? C18 N3 Mg1 122.19(18) . . ? C7 C6 C11 120.6(3) . . ? C7 C6 N1 120.9(3) . . ? C11 C6 N1 118.5(3) . . ? C8 C7 C6 118.0(3) . . ? C8 C7 C12 118.8(3) . . ? C6 C7 C12 123.1(2) . . ? C9 C8 C7 121.6(3) . . ? C10 C9 C8 119.8(3) . . ? C9 C10 C11 121.4(3) . . ? C10 C11 C6 118.5(3) . . ? C10 C11 C15 120.2(3) . . ? C6 C11 C15 121.3(3) . . ? C13 C12 C7 111.1(3) . . ? C13 C12 C14 108.9(3) . . ? C7 C12 C14 112.9(3) . . ? C16 C15 C17 111.8(4) . . ? C16 C15 C11 111.9(3) . . ? C17 C15 C11 113.7(4) . . ? C23 C18 C19 120.5(3) . . ? C23 C18 N3 121.1(3) . . ? C19 C18 N3 118.3(3) . . ? C20 C19 C18 118.5(3) . . ? C20 C19 C24 119.2(3) . . ? C18 C19 C24 122.3(3) . . ? C21 C20 C19 121.2(3) . . ? C22 C21 C20 119.4(3) . . ? C21 C22 C23 122.0(3) . . ? C18 C23 C22 118.4(3) . . ? C18 C23 C27 121.9(2) . . ? C22 C23 C27 119.7(3) . . ? C26 C24 C19 112.2(4) . . ? C26 C24 C25 111.1(4) . . ? C19 C24 C25 110.4(5) . . ? C28 C27 C23 111.0(3) . . ? C28 C27 C29 110.4(3) . . ? C23 C27 C29 112.6(3) . . ? C31 N31 C36 117.2(2) . . ? C31 N31 Mg2 121.50(18) . . ? C36 N31 Mg2 121.26(16) . . ? N31 C31 C32 123.8(3) . . ? N31 C31 C34 120.6(3) . . ? C32 C31 C34 115.6(3) . . ? C33 C32 C31 129.9(3) . . ? C33 N33 C48 117.5(2) . . ? C33 N33 Mg2 120.43(19) . . ? C48 N33 Mg2 121.96(18) . . ? N33 C33 C32 124.3(2) . . ? N33 C33 C35 119.1(3) . . ? C32 C33 C35 116.6(3) . . ? C41 C36 C37 121.9(3) . . ? C41 C36 N31 119.6(3) . . ? C37 C36 N31 118.5(2) . . ? C38 C37 C36 117.9(3) . . ? C38 C37 C42 120.2(3) . . ? C36 C37 C42 122.0(3) . . ? C39 C38 C37 121.3(4) . . ? C40 C39 C38 120.4(3) . . ? C39 C40 C41 121.6(4) . . ? C36 C41 C40 116.8(4) . . ? C36 C41 C45 121.8(3) . . ? C40 C41 C45 121.3(3) . . ? C44 C42 C37 112.6(3) . . ? C44 C42 C43 109.3(3) . . ? C37 C42 C43 115.3(3) . . ? C41 C45 C47 110.9(4) . . ? C41 C45 C46 112.2(5) . . ? C47 C45 C46 109.2(4) . . ? C53 C48 C49 120.9(3) . . ? C53 C48 N33 121.4(3) . . ? C49 C48 N33 117.7(3) . . ? C50 C49 C48 118.1(3) . . ? C50 C49 C54 119.8(3) . . ? C48 C49 C54 122.0(3) . . ? C51 C50 C49 121.2(4) . . ? C52 C51 C50 120.1(3) . . ? C51 C52 C53 121.3(4) . . ? C52 C53 C48 118.4(3) . . ? C52 C53 C57 120.1(3) . . ? C48 C53 C57 121.5(3) . . ? C55 C54 C49 111.6(4) . . ? C55 C54 C56 110.5(4) . . ? C49 C54 C56 113.3(4) . . ? C58 C57 C53 110.2(3) . . ? C58 C57 C59 109.5(4) . . ? C53 C57 C59 112.5(3) . . ? O61 C61 Cr1 132.0(9) . . ? O61 C61' Cr1 171.3(8) . . ? C61' O61 Mg1 142.3(7) . . ? C61 O61 Mg1 173.6(6) . . ? O62 C62 Cr1 167.4(5) . . ? O62 C62' Cr1 131.0(13) . . ? C62 O62 Mg2 143.7(4) . . ? C62' O62 Mg2 175.8(9) . . ? O63 C63 Cr1 178.3(4) . . ? O64 C64 Cr1 178.6(4) . . ? O65 C65 Cr1 177.9(4) . . ? O66 C66 Cr1 177.0(4) . . ? C72 C71 C76 120.0 . . ? C72 C71 C70 119.2(7) . . ? C76 C71 C70 120.7(7) . . ? C71 C72 C73 120.0 . . ? C74 C73 C72 120.0 . . ? C73 C74 C75 120.0 . . ? C74 C75 C76 120.0 . . ? C75 C76 C71 120.0 . . ? C72' C71' C76' 120.0 . . ? C72' C71' C70' 121.8(7) . . ? C76' C71' C70' 118.2(7) . . ? C73' C72' C71' 120.0 . . ? C72' C73' C74' 120.0 . . ? C73' C74' C75' 120.0 . . ? C76' C75' C74' 120.0 . . ? C75' C76' C71' 120.0 . . ? _refine_diff_density_max 0.240 _refine_diff_density_min -0.259 _refine_diff_density_rms 0.036 _shelx_res_file ; MRC1605.res created by SHELXL-2014/7 TITL MRC1605 in Pna2(1) REM Pna2(1) (#33, found as P2(1)cn in -cba setting) REM OLE212 CELL 1.54184 35.218812 15.391399 12.774625 90.0000 90.0000 90.0000 ZERR 4.00 0.000362 0.000164 0.000111 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H Cr Mg N O UNIT 284 368 4 8 16 24 TEMP -100 L.S. 6 FMAP 2 PLAN 10 ACTA REM 'C64 H84 Cr Mg2 N4 O6, C7 H8' REM C71 H92 Cr Mg2 N4 O6 SIMU 0.01 0.01 1 C61 C61' SIMU 0.01 0.01 1 C62 C62' REM Modelled as mixed CO/CHO species, so disorders at C61 and C62 linked SADI C70 C71 C70' C71' SADI C70 C72 C70 C76 C70' C72' C70' C76' SIMU 0.02 0.02 1 C70 > C76' RTAB MgH MG1 H1 RTAB MgH MG2 H1 RTAB MHM MG1 H1 MG2 WGHT 0.053600 0.538200 FVAR 3.42111 0.53492 0.61582 CR1 3 0.676261 0.681525 0.231428 11.00000 0.05771 0.04949 = 0.03042 0.00083 0.00903 0.01251 MG1 4 0.634917 0.652725 0.584295 11.00000 0.03416 0.03745 = 0.02972 0.00681 -0.00153 -0.00323 MG2 4 0.606246 0.854211 0.474245 11.00000 0.03101 0.03174 = 0.03425 -0.00426 -0.00480 0.00348 H1 2 0.615880 0.768647 0.548511 11.00000 0.04898 N1 5 0.597683 0.591005 0.682411 11.00000 0.03571 0.03908 = 0.03119 0.00396 -0.00086 -0.00767 C1 1 0.607175 0.575790 0.781134 11.00000 0.03986 0.04506 = 0.03045 0.00480 0.00220 -0.00302 C2 1 0.643609 0.589264 0.822883 11.00000 0.04094 0.05546 = 0.02658 0.00661 -0.00081 -0.00274 AFIX 43 H2A 2 0.644985 0.587284 0.897114 11.00000 -1.20000 AFIX 0 C3 1 0.678414 0.605240 0.772124 11.00000 0.03643 0.04781 = 0.03345 0.00547 -0.00204 0.00165 N3 5 0.681511 0.623307 0.670571 11.00000 0.03251 0.03847 = 0.03330 0.00266 0.00218 0.00290 C4 1 0.578589 0.539253 0.857783 11.00000 0.04638 0.07254 = 0.03841 0.01666 0.00176 -0.01171 AFIX 137 H4A 2 0.562005 0.586031 0.882650 11.00000 -1.50000 H4B 2 0.591985 0.513406 0.917378 11.00000 -1.50000 H4C 2 0.563260 0.494654 0.822976 11.00000 -1.50000 AFIX 0 C5 1 0.713259 0.600228 0.840532 11.00000 0.03979 0.09476 = 0.04627 0.01585 -0.00490 0.00254 AFIX 137 H5A 2 0.723729 0.658655 0.850353 11.00000 -1.50000 H5B 2 0.732310 0.563110 0.806969 11.00000 -1.50000 H5C 2 0.706374 0.575663 0.908714 11.00000 -1.50000 AFIX 0 C6 1 0.560711 0.564281 0.647800 11.00000 0.04009 0.04570 = 0.03184 0.00785 -0.00130 -0.01233 C7 1 0.528441 0.615511 0.668587 11.00000 0.03808 0.05515 = 0.03695 0.00569 -0.00284 -0.01035 C8 1 0.493164 0.585123 0.634023 11.00000 0.03939 0.06875 = 0.05039 0.00622 -0.00601 -0.01277 AFIX 43 H8A 2 0.471103 0.618994 0.646894 11.00000 -1.20000 AFIX 0 C9 1 0.489665 0.507203 0.581738 11.00000 0.05320 0.07185 = 0.05673 0.00845 -0.01470 -0.02861 AFIX 43 H9A 2 0.465309 0.486843 0.561243 11.00000 -1.20000 AFIX 0 C10 1 0.521378 0.459224 0.559416 11.00000 0.06731 0.05007 = 0.04813 0.00445 -0.00923 -0.02463 AFIX 43 H10A 2 0.518767 0.406219 0.521997 11.00000 -1.20000 AFIX 0 C11 1 0.557464 0.486477 0.590430 11.00000 0.05862 0.04197 = 0.03740 0.00575 -0.00394 -0.01355 C12 1 0.530423 0.703130 0.723181 11.00000 0.03733 0.05530 = 0.03732 0.00011 -0.00017 -0.00194 AFIX 13 H12A 2 0.556519 0.709831 0.752959 11.00000 -1.20000 AFIX 0 C13 1 0.523881 0.776887 0.646343 11.00000 0.05118 0.05834 = 0.05076 0.00111 -0.00241 -0.00231 AFIX 137 H13A 2 0.543106 0.774456 0.590960 11.00000 -1.50000 H13B 2 0.525760 0.832576 0.683172 11.00000 -1.50000 H13C 2 0.498555 0.771236 0.615303 11.00000 -1.50000 AFIX 0 C14 1 0.501876 0.711444 0.813305 11.00000 0.05834 0.09178 = 0.04626 -0.00189 0.01206 -0.00151 AFIX 137 H14A 2 0.475991 0.707227 0.785619 11.00000 -1.50000 H14B 2 0.505227 0.767755 0.847898 11.00000 -1.50000 H14C 2 0.506172 0.664663 0.863980 11.00000 -1.50000 AFIX 0 C15 1 0.592254 0.432664 0.562595 11.00000 0.06495 0.04114 = 0.05436 -0.00317 0.00512 -0.00903 AFIX 13 H15A 2 0.614415 0.473207 0.565583 11.00000 -1.20000 AFIX 0 C16 1 0.599841 0.363141 0.642313 11.00000 0.10547 0.08770 = 0.06919 0.02139 0.01567 0.02580 AFIX 137 H16A 2 0.601189 0.389303 0.712154 11.00000 -1.50000 H16B 2 0.623999 0.334490 0.626260 11.00000 -1.50000 H16C 2 0.579288 0.320244 0.640568 11.00000 -1.50000 AFIX 0 C17 1 0.591433 0.396369 0.452139 11.00000 0.10827 0.10902 = 0.06058 -0.02097 -0.00329 0.02121 AFIX 137 H17A 2 0.574705 0.345523 0.449829 11.00000 -1.50000 H17B 2 0.617154 0.379291 0.431325 11.00000 -1.50000 H17C 2 0.581910 0.440860 0.403947 11.00000 -1.50000 AFIX 0 C18 1 0.718938 0.618419 0.625174 11.00000 0.03341 0.04788 = 0.03497 0.00626 0.00168 0.00556 C19 1 0.731229 0.538346 0.585028 11.00000 0.04548 0.04667 = 0.05998 0.00423 0.01156 0.00983 C20 1 0.767656 0.533103 0.542136 11.00000 0.05758 0.05377 = 0.07051 0.00549 0.01930 0.01862 AFIX 43 H20A 2 0.776553 0.479014 0.516026 11.00000 -1.20000 AFIX 0 C21 1 0.790962 0.605177 0.537026 11.00000 0.04176 0.07315 = 0.06189 0.01042 0.01648 0.01146 AFIX 43 H21A 2 0.815730 0.600612 0.508089 11.00000 -1.20000 AFIX 0 C22 1 0.778116 0.682779 0.573822 11.00000 0.03815 0.06263 = 0.05724 0.00405 0.00721 -0.00354 AFIX 43 H22A 2 0.794166 0.732251 0.569399 11.00000 -1.20000 AFIX 0 C23 1 0.742002 0.691863 0.617942 11.00000 0.03477 0.05228 = 0.04111 0.00084 0.00099 0.00184 C24 1 0.706399 0.457442 0.587216 11.00000 0.06735 0.04057 = 0.12085 -0.00168 0.03549 0.00667 AFIX 13 H24A 2 0.679932 0.476221 0.604288 11.00000 -1.20000 AFIX 0 C25 1 0.719491 0.395575 0.673773 11.00000 0.15130 0.06592 = 0.12443 0.02637 0.05734 -0.00170 AFIX 137 H25A 2 0.746607 0.383203 0.665154 11.00000 -1.50000 H25B 2 0.705057 0.341260 0.669402 11.00000 -1.50000 H25C 2 0.715193 0.422644 0.742191 11.00000 -1.50000 AFIX 0 C26 1 0.705304 0.412205 0.482840 11.00000 0.11091 0.05814 = 0.13928 -0.02349 0.01411 -0.00705 AFIX 137 H26A 2 0.697681 0.453645 0.428519 11.00000 -1.50000 H26B 2 0.686965 0.364370 0.485541 11.00000 -1.50000 H26C 2 0.730552 0.389139 0.466481 11.00000 -1.50000 AFIX 0 C27 1 0.728953 0.780174 0.656457 11.00000 0.04138 0.05245 = 0.05792 -0.01128 0.00570 -0.00660 AFIX 13 H27A 2 0.704109 0.771833 0.693001 11.00000 -1.20000 AFIX 0 C28 1 0.722261 0.841652 0.565619 11.00000 0.06164 0.05304 = 0.07211 -0.00851 -0.00227 0.01148 AFIX 137 H28A 2 0.746298 0.852201 0.529122 11.00000 -1.50000 H28B 2 0.712180 0.896798 0.592040 11.00000 -1.50000 H28C 2 0.703979 0.815706 0.516962 11.00000 -1.50000 AFIX 0 C29 1 0.756615 0.820636 0.735282 11.00000 0.07831 0.07460 = 0.07418 -0.01769 -0.01581 -0.01066 AFIX 137 H29A 2 0.761733 0.779006 0.791587 11.00000 -1.50000 H29B 2 0.745364 0.873435 0.764884 11.00000 -1.50000 H29C 2 0.780427 0.835328 0.699757 11.00000 -1.50000 AFIX 0 N31 5 0.604401 0.963362 0.564155 11.00000 0.02941 0.03241 = 0.03837 -0.00545 0.00112 0.00091 C31 1 0.573085 1.011830 0.570577 11.00000 0.03847 0.03604 = 0.04201 -0.00242 0.00568 0.00558 C32 1 0.539082 0.992406 0.518230 11.00000 0.03485 0.04770 = 0.05173 -0.00232 0.00070 0.01438 AFIX 43 H32A 2 0.517178 1.020804 0.544933 11.00000 -1.20000 AFIX 0 N33 5 0.558540 0.884051 0.392689 11.00000 0.03533 0.03858 = 0.03494 0.00171 -0.00660 0.00315 C33 1 0.532571 0.937976 0.433310 11.00000 0.03553 0.04720 = 0.04884 0.00173 -0.00759 0.00992 C34 1 0.572929 1.095083 0.634022 11.00000 0.05456 0.04302 = 0.06425 -0.01598 0.00724 0.01136 AFIX 137 H34A 2 0.586167 1.085433 0.700490 11.00000 -1.50000 H34B 2 0.546661 1.112617 0.647968 11.00000 -1.50000 H34C 2 0.585857 1.141010 0.594617 11.00000 -1.50000 AFIX 0 C35 1 0.493483 0.942307 0.383998 11.00000 0.04248 0.08639 = 0.07887 -0.01402 -0.01950 0.02036 AFIX 137 H35A 2 0.495587 0.965428 0.312756 11.00000 -1.50000 H35B 2 0.477139 0.980400 0.425812 11.00000 -1.50000 H35C 2 0.482445 0.883895 0.381537 11.00000 -1.50000 AFIX 0 C36 1 0.637063 0.991635 0.623447 11.00000 0.03106 0.03790 = 0.05036 -0.01562 0.00453 -0.00039 C37 1 0.643008 0.955759 0.723799 11.00000 0.03410 0.05891 = 0.04379 -0.02000 -0.00070 0.00466 C38 1 0.673892 0.986185 0.782015 11.00000 0.04268 0.09324 = 0.05737 -0.03246 -0.00815 0.00054 AFIX 43 H38A 2 0.678185 0.963744 0.850273 11.00000 -1.20000 AFIX 0 C39 1 0.698072 1.047707 0.742555 11.00000 0.05050 0.09795 = 0.08484 -0.03796 -0.00863 -0.01619 AFIX 43 H39A 2 0.718454 1.068544 0.784301 11.00000 -1.20000 AFIX 0 C40 1 0.693074 1.079352 0.643446 11.00000 0.04542 0.06131 = 0.10920 -0.02695 0.01293 -0.01799 AFIX 43 H40A 2 0.710597 1.120689 0.616688 11.00000 -1.20000 AFIX 0 C41 1 0.662301 1.051885 0.579535 11.00000 0.04022 0.04062 = 0.07585 -0.01631 0.01295 -0.00700 C42 1 0.616783 0.887812 0.769335 11.00000 0.04858 0.05912 = 0.03615 -0.00665 0.00144 0.00600 AFIX 13 H42A 2 0.607742 0.851851 0.709092 11.00000 -1.20000 AFIX 0 C43 1 0.635172 0.824951 0.846481 11.00000 0.06696 0.08464 = 0.07724 0.01050 0.00369 0.02571 AFIX 137 H43A 2 0.658157 0.800214 0.815157 11.00000 -1.50000 H43B 2 0.617296 0.778139 0.863074 11.00000 -1.50000 H43C 2 0.641876 0.856114 0.910775 11.00000 -1.50000 AFIX 0 C44 1 0.581806 0.926823 0.818580 11.00000 0.05706 0.07359 = 0.04967 0.00164 0.00728 0.01048 AFIX 137 H44A 2 0.589356 0.969899 0.871099 11.00000 -1.50000 H44B 2 0.566897 0.880881 0.852220 11.00000 -1.50000 H44C 2 0.566432 0.955044 0.764426 11.00000 -1.50000 AFIX 0 C45 1 0.658305 1.082704 0.468429 11.00000 0.05573 0.04194 = 0.09287 0.00247 0.02317 -0.00878 AFIX 13 H45A 2 0.632171 1.067695 0.443738 11.00000 -1.20000 AFIX 0 C46 1 0.663414 1.181280 0.458703 11.00000 0.18160 0.05622 = 0.12803 0.01322 0.04713 -0.00451 AFIX 137 H46A 2 0.647013 1.210633 0.509596 11.00000 -1.50000 H46B 2 0.656523 1.199774 0.387797 11.00000 -1.50000 H46C 2 0.689970 1.196455 0.472500 11.00000 -1.50000 AFIX 0 C47 1 0.686613 1.037460 0.397632 11.00000 0.07104 0.08970 = 0.08266 -0.00694 0.02170 -0.00015 AFIX 137 H47A 2 0.712259 1.044538 0.426154 11.00000 -1.50000 H47B 2 0.685461 1.063107 0.327488 11.00000 -1.50000 H47C 2 0.680425 0.975479 0.393474 11.00000 -1.50000 AFIX 0 C48 1 0.552379 0.853365 0.287486 11.00000 0.04123 0.04950 = 0.03495 0.00424 -0.01099 0.00403 C49 1 0.566629 0.903881 0.205027 11.00000 0.06788 0.05323 = 0.04209 0.01157 -0.01037 0.00038 C50 1 0.560471 0.875288 0.103197 11.00000 0.09963 0.07383 = 0.03493 0.01760 -0.01081 -0.00873 AFIX 43 H50A 2 0.569532 0.909130 0.046243 11.00000 -1.20000 AFIX 0 C51 1 0.541471 0.798773 0.083331 11.00000 0.10862 0.07966 = 0.03485 0.00174 -0.02164 -0.00600 AFIX 43 H51A 2 0.537442 0.780492 0.013176 11.00000 -1.20000 AFIX 0 C52 1 0.528458 0.749318 0.164163 11.00000 0.07749 0.06649 = 0.04271 -0.00135 -0.01886 -0.01214 AFIX 43 H52A 2 0.515571 0.696467 0.149563 11.00000 -1.20000 AFIX 0 C53 1 0.533690 0.774775 0.267904 11.00000 0.05105 0.05085 = 0.03575 -0.00077 -0.01308 -0.00107 C54 1 0.587817 0.988688 0.224112 11.00000 0.09980 0.05945 = 0.05218 0.01632 -0.00914 -0.01324 AFIX 13 H54A 2 0.598075 0.986140 0.297041 11.00000 -1.20000 AFIX 0 C55 1 0.561482 1.066092 0.219053 11.00000 0.14513 0.05557 = 0.10651 0.01115 0.00730 -0.00381 AFIX 137 H55A 2 0.551409 1.071865 0.147881 11.00000 -1.50000 H55B 2 0.575512 1.118848 0.237735 11.00000 -1.50000 H55C 2 0.540448 1.057760 0.268263 11.00000 -1.50000 AFIX 0 C56 1 0.621773 1.001611 0.150824 11.00000 0.10485 0.09278 = 0.09348 0.02645 0.00519 -0.03423 AFIX 137 H56A 2 0.637604 0.949250 0.151337 11.00000 -1.50000 H56B 2 0.636811 1.051388 0.174686 11.00000 -1.50000 H56C 2 0.612627 1.012461 0.079560 11.00000 -1.50000 AFIX 0 C57 1 0.520871 0.716178 0.356081 11.00000 0.05378 0.06000 = 0.04002 -0.00034 -0.00518 -0.01537 AFIX 13 H57A 2 0.520949 0.750816 0.422308 11.00000 -1.20000 AFIX 0 C58 1 0.548231 0.641491 0.369053 11.00000 0.07551 0.07880 = 0.05967 0.02906 -0.00033 -0.00346 AFIX 137 H58A 2 0.548455 0.606400 0.305043 11.00000 -1.50000 H58B 2 0.540227 0.605359 0.428240 11.00000 -1.50000 H58C 2 0.573777 0.664211 0.382299 11.00000 -1.50000 AFIX 0 C59 1 0.480707 0.680807 0.339177 11.00000 0.06274 0.10674 = 0.07726 0.00120 -0.00721 -0.02909 AFIX 137 H59A 2 0.463738 0.728523 0.319393 11.00000 -1.50000 H59B 2 0.471579 0.654024 0.404066 11.00000 -1.50000 H59C 2 0.481093 0.637233 0.283251 11.00000 -1.50000 AFIX 0 PART 1 C61 1 0.657550 0.601477 0.349156 31.00000 0.08276 0.06999 = 0.04318 0.00842 0.00945 -0.00331 AFIX 43 H61A 2 0.654868 0.542401 0.328922 31.00000 -1.20000 AFIX 0 PART 2 C61' 1 0.662925 0.641941 0.359727 -31.00000 0.04492 PART 0 O61 6 0.649293 0.615561 0.439623 11.00000 0.05831 0.05413 = 0.03009 -0.00186 0.00576 0.00495 PART 1 C62 1 0.651838 0.769782 0.299235 31.00000 0.04442 0.04355 = 0.04525 0.00160 0.01068 -0.01082 PART 2 C62' 1 0.662082 0.803894 0.286001 -31.00000 0.05417 AFIX 43 H62A 2 0.673751 0.850399 0.249178 -31.00000 -1.20000 AFIX 0 PART 0 O62 6 0.641716 0.826065 0.355946 11.00000 0.04701 0.05335 = 0.04131 -0.00577 0.00918 0.00730 C63 1 0.690004 0.746975 0.110577 11.00000 0.07398 0.07018 = 0.03947 0.00496 -0.00327 -0.00750 O63 6 0.698249 0.787666 0.040204 11.00000 0.11789 0.12882 = 0.05357 0.03561 -0.01290 -0.04325 C64 1 0.698983 0.579206 0.173904 11.00000 0.05812 0.06357 = 0.06847 -0.01098 0.00448 0.00386 O64 6 0.711869 0.518610 0.138349 11.00000 0.08720 0.08126 = 0.13719 -0.04982 -0.00445 0.02844 C65 1 0.722599 0.711136 0.298108 11.00000 0.07616 0.06285 = 0.03950 -0.00507 -0.00362 0.02111 O65 6 0.750385 0.731412 0.336737 11.00000 0.09068 0.09852 = 0.06802 -0.01174 -0.02413 0.01508 C66 1 0.629674 0.650366 0.165570 11.00000 0.06405 0.08744 = 0.05279 -0.00370 0.01075 0.01191 O66 6 0.602406 0.628245 0.124769 11.00000 0.06811 0.14149 = 0.09031 -0.02124 -0.00466 -0.00067 PART 2 C70 1 0.382288 0.627517 0.664846 21.00000 0.08183 0.17299 = 0.14244 0.01781 -0.02169 0.00233 AFIX 137 H70A 2 0.383284 0.564365 0.655455 21.00000 -1.50000 H70B 2 0.361267 0.642369 0.711818 21.00000 -1.50000 H70C 2 0.406247 0.647776 0.695282 21.00000 -1.50000 AFIX 66 C71 1 0.376430 0.669278 0.563555 21.00000 0.06981 0.10206 = 0.10575 -0.01014 -0.00096 -0.00317 C72 1 0.394566 0.747573 0.542558 21.00000 0.09394 0.08528 = 0.12426 -0.04589 0.01062 -0.03151 AFIX 43 H72A 2 0.411760 0.771471 0.592099 21.00000 -1.20000 AFIX 65 C73 1 0.387544 0.790903 0.449074 21.00000 0.13632 0.11847 = 0.17666 -0.00937 0.03836 0.03533 AFIX 43 H73A 2 0.399939 0.844414 0.434723 21.00000 -1.20000 AFIX 65 C74 1 0.362387 0.755938 0.376587 21.00000 0.11568 0.17396 = 0.13524 -0.04907 0.03508 0.04433 AFIX 43 H74A 2 0.357588 0.785553 0.312695 21.00000 -1.20000 AFIX 65 C75 1 0.344251 0.677643 0.397583 21.00000 0.10410 0.15822 = 0.11530 -0.04141 -0.00241 0.03447 AFIX 43 H75A 2 0.327058 0.653747 0.348041 21.00000 -1.20000 AFIX 65 C76 1 0.351273 0.634313 0.491066 21.00000 0.09192 0.10760 = 0.14524 -0.07079 -0.00469 0.02268 AFIX 43 H76A 2 0.338878 0.580802 0.505416 21.00000 -1.20000 AFIX 0 PART 1 C70' 1 0.377146 0.796499 0.370470 -21.00000 0.12091 AFIX 137 H70D 2 0.361427 0.777562 0.311423 -21.00000 -1.50000 H70E 2 0.403681 0.800861 0.347972 -21.00000 -1.50000 H70F 2 0.368366 0.853394 0.394971 -21.00000 -1.50000 AFIX 66 C71' 1 0.374103 0.733214 0.455775 -21.00000 0.07294 C72' 1 0.354980 0.654881 0.443421 -21.00000 0.11077 AFIX 43 H72B 2 0.343465 0.641100 0.378253 -21.00000 -1.20000 AFIX 65 C73' 1 0.352705 0.596712 0.526416 -21.00000 0.12892 AFIX 43 H73B 2 0.339636 0.543175 0.517972 -21.00000 -1.20000 AFIX 65 C74' 1 0.369554 0.616875 0.621766 -21.00000 0.11170 AFIX 43 H74B 2 0.367999 0.577118 0.678489 -21.00000 -1.20000 AFIX 65 C75' 1 0.388677 0.695207 0.634122 -21.00000 0.09989 AFIX 43 H75B 2 0.400192 0.708987 0.699289 -21.00000 -1.20000 AFIX 65 C76' 1 0.390952 0.753377 0.551127 -21.00000 0.11506 AFIX 43 H76B 2 0.404022 0.806914 0.559572 -21.00000 -1.20000 PART 0 AFIX 0 HKLF 4 REM MRC1605 in Pna2(1) REM R1 = 0.0376 for 8954 Fo > 4sig(Fo) and 0.0427 for all 9749 data REM 797 parameters refined using 56 restraints END WGHT 0.0536 0.5379 REM Highest difference peak 0.240, deepest hole -0.259, 1-sigma level 0.036 Q1 1 0.3624 0.5953 0.5686 11.00000 0.05 0.24 Q2 1 0.6019 0.9431 0.8877 11.00000 0.05 0.22 Q3 1 0.3491 0.7359 0.3714 11.00000 0.05 0.21 Q4 1 0.6342 0.8207 0.7813 11.00000 0.05 0.20 Q5 1 0.6016 0.6122 0.7363 11.00000 0.05 0.19 Q6 1 0.6798 0.6127 0.2484 11.00000 0.05 0.18 Q7 1 0.6077 0.6207 0.6479 11.00000 0.05 0.18 Q8 1 0.6327 0.7185 0.5816 11.00000 0.05 0.18 Q9 1 0.6873 0.7439 0.1914 11.00000 0.05 0.17 Q10 1 0.6343 1.1560 0.4325 11.00000 0.05 0.17 ; _shelx_res_checksum 47970 _shelx_hkl_file ; 0 0 -13 18.5045 89.7607 2 0 0 -12 12121.9 405.242 2 0 0 -11-42.3111 102.527 2 0 0 -10 38875.6 711.852 2 0 0 15-169.301 86.5313 3 0 -1 -14 26.3993 75.5883 2 0 -1 -13 1568.05 168.379 2 0 -1 -12 58.2177 108.720 2 0 1 -12 56.3520 89.9868 2 0 -1 -11 7123.12 327.525 2 0 1 -11 7122.61 318.202 2 0 1 -10-11.4306 86.0309 2 0 -1 -10-5.61471 93.5119 2 0 -1 -9 33554.8 617.003 2 0 1 9 37918.0 2135.08 1 0 1 15 5734.17 228.888 3 0 -1 15 5255.31 201.439 3 0 -2 -14 3489.90 195.613 2 0 -2 -13-88.1482 111.720 2 0 -2 -12 583.239 145.631 2 0 -2 -11-54.7105 127.134 2 0 -2 -10 5001.58 272.546 2 0 -2 -9-70.3052 88.6724 2 0 2 -1-16.1490 50.2884 1 0 2 0 57103.9 937.475 1 0 2 9-3.62460 192.302 1 0 2 10 4365.24 794.335 1 0 -2 14 5052.57 255.338 3 0 2 15 176.215 120.147 3 0 -2 15 262.833 77.6859 3 0 -3 -14 164.411 97.3543 2 0 -3 -13 2451.24 206.191 2 0 -3 -12-219.865 143.893 2 0 -3 -11 2124.59 213.829 2 0 -3 -10 26.9166 103.904 2 0 -3 -9 2023.19 177.716 2 0 3 -2 38.7807 45.2306 1 0 3 -1 322324. 2499.75 1 0 3 0-1.28584 103.801 1 0 3 8 347.740 324.908 1 0 3 9 2878.89 672.291 1 0 3 10 288.505 273.334 1 0 -3 14 24.4602 99.5376 3 0 3 15 676.608 149.302 3 0 -4 -15 47.9527 43.8070 2 0 -4 -14 1594.10 146.290 2 0 -4 -13 165.083 117.505 2 0 -4 -12 720.813 164.482 2 0 -4 -11-83.6301 127.573 2 0 -4 -10 9498.44 373.192 2 0 -4 -9 93.2414 102.328 2 0 4 -2 15132.4 482.073 1 0 4 -1 121.712 102.632 1 0 4 0 180331. 2414.73 1 0 4 1-61.7445 172.484 1 0 4 7 121.438 340.827 1 0 4 8 3346.55 722.904 1 0 4 9-293.057 373.070 1 0 4 10 9688.42 1310.50 1 0 4 15-95.5455 72.1810 3 0 -5 -15 901.300 78.5674 2 0 -5 -14 42.5235 89.3277 2 0 -5 -13 3121.58 223.691 2 0 -5 -12-50.3321 147.925 2 0 -5 -11 19855.8 552.948 2 0 -5 -10-57.5475 118.801 2 0 -5 -9 37712.3 700.749 2 0 5 -2 92.9571 93.2975 1 0 5 -1 225645. 2881.33 1 0 5 0 132.328 154.196 1 0 5 1 244894. 3514.54 1 0 5 2-63.4747 174.640 1 0 5 6 156.295 296.210 1 0 5 7 1369.13 485.427 1 0 5 8-377.388 399.457 1 0 5 9 44959.3 2789.37 1 0 5 10 388.602 405.860 1 0 5 14-236.464 110.092 3 0 5 15 541.765 82.0571 3 0 -6 -14 9207.86 285.361 2 0 -6 -13-132.289 118.078 2 0 -6 -12 7851.06 350.013 2 0 -6 -11 92.4776 133.583 2 0 -6 -10 1890.51 202.842 2 0 -6 -9-91.6522 101.547 2 0 6 -2 44690.4 1141.29 1 0 6 -1 70.1602 124.309 1 0 6 0 1284.82 301.762 1 0 6 1-85.8894 205.003 1 0 6 2 32983.4 1535.21 1 0 6 3-15.6911 309.446 1 0 6 4 58935.7 2392.15 1 0 6 5-156.981 305.090 1 0 6 6 138436. 4199.26 1 0 6 7 395.002 445.849 1 0 6 8 108111. 4264.13 1 0 6 9 789.240 435.012 1 0 6 14 6688.63 251.664 3 0 -7 -14 127.490 81.0008 2 0 -7 -13 1228.74 156.235 2 0 -7 -12-82.6840 141.125 2 0 -7 -11 3027.75 249.942 2 0 -7 -10-57.2708 133.501 2 0 -7 -9 6676.92 319.697 2 0 7 -1 12092.3 849.262 1 0 7 0-8.92860 143.975 1 0 7 1 10991.4 900.580 1 0 7 2 335.653 296.326 1 0 7 3 71560.9 2642.82 1 0 7 4 259.888 321.561 1 0 7 5 15306.8 1409.64 1 0 7 6 7.74813 363.447 1 0 7 7 620.406 474.017 1 0 7 8-79.4636 383.317 1 0 7 9 12447.9 1589.40 1 0 7 13 2800.12 196.742 3 0 7 14 47.7504 77.7257 3 0 -8 -14 4684.34 181.868 2 0 -8 -13-143.678 105.564 2 0 -8 -12 14580.4 441.372 2 0 -8 -11-129.756 143.408 2 0 -8 -10 15447.9 489.383 2 0 -8 -9-69.7156 128.990 2 0 8 -1 74.7748 156.410 1 0 8 0 219.114 201.329 1 0 8 1-136.687 260.049 1 0 8 2 84161.2 2863.99 1 0 8 3-101.381 289.923 1 0 8 4 39761.1 2250.90 1 0 8 5-146.007 461.999 1 0 8 6 77829.3 3539.66 1 0 8 7-72.7823 449.116 1 0 8 8 21462.9 2057.02 1 0 8 12 13920.6 396.050 3 0 8 13-178.526 81.5504 3 0 -9 -14 49.1926 44.6074 2 0 -9 -13 3107.77 183.081 2 0 -9 -12-73.3899 125.503 2 0 -9 -11 6742.24 329.749 2 0 -9 -10 85.1445 147.486 2 0 -9 -9 5097.68 293.819 2 0 9 -6-16.2036 70.4715 4 0 9 0 448.734 305.386 1 0 9 1 45235.9 2169.91 1 0 9 2-325.055 291.229 1 0 9 3 27770.8 1872.69 1 0 9 4-64.8345 343.061 1 0 9 5 42047.4 2593.68 1 0 9 6-295.271 445.543 1 0 9 7 20538.8 2004.61 1 0 9 8 293.026 434.553 1 0 9 11 8587.29 313.099 3 0 9 12-107.337 76.7752 3 0 -10 -13-68.8153 72.1888 2 0 -10 -12 1741.14 165.410 2 0 -10 -11 148.504 135.430 2 0 -10 -10 18359.7 505.085 2 0 -10 -9 132.860 146.284 2 0 10 -7 68.5905 81.4945 4 0 10 -6 6799.62 296.463 4 0 10 -5 56.3146 94.1236 4 0 10 -4 11038.3 365.407 4 0 10 -3-37.5947 79.3536 4 0 10 1-130.819 292.573 1 0 10 2 49600.6 2568.90 1 0 10 3-301.557 340.713 1 0 10 4 8203.04 1169.26 1 0 10 5-902.154 640.424 1 0 10 6 5403.27 1063.37 1 0 10 7-485.918 445.755 1 0 -11 -13 1052.20 83.3222 2 0 -11 -12-133.762 88.7148 2 0 -11 -11 480.805 128.259 2 0 -11 -10-80.6665 125.770 2 0 -11 -9 9820.94 375.518 2 0 -11 -8 69.1652 117.774 2 0 11 -7 9836.70 363.478 4 0 11 -6 37.9457 98.6452 4 0 11 -5 3717.60 238.104 4 0 11 -4-10.9454 92.3092 4 0 11 -3 8319.37 336.435 4 0 11 -2-34.5147 89.9145 4 0 11 -1 2747.09 196.606 4 0 11 0-29.0027 87.0932 4 0 11 1 2596.67 191.008 4 0 11 2 34.3517 80.7830 4 0 11 2-884.270 424.352 1 0 11 3 8531.60 1189.30 1 0 11 3 8388.02 308.956 4 0 11 4-463.821 450.923 1 0 11 5 3957.79 983.130 1 0 11 6-495.296 424.288 1 0 -12 -12 466.762 78.0791 2 0 -12 -11-52.8619 88.5829 2 0 -12 -10 975.913 148.872 2 0 -12 -9 34.3325 118.676 2 0 -12 -8 2640.31 212.412 2 0 12 -7-237.721 120.188 4 0 12 -6 2396.13 212.784 4 0 12 -5 23.6024 118.560 4 0 12 -4 3720.48 248.324 4 0 12 -3 107.761 107.067 4 0 12 -2 3346.06 238.130 4 0 12 -1-29.2098 104.155 4 0 12 0 2115.39 192.464 4 0 12 1 22.8014 95.3160 4 0 12 2 2526.84 195.788 4 0 12 3-22.8208 87.3524 4 0 12 4 4232.82 1001.59 1 0 12 5-354.624 460.685 1 0 -13 -11 4096.04 172.544 2 0 -13 -10 123.933 90.4718 2 0 -13 -9 4502.69 234.017 2 0 -13 -8-12.0594 104.142 2 0 13 -7 5683.20 278.899 4 0 -13 -7 5904.79 283.441 2 0 13 -6-132.981 127.419 4 0 13 -5 17373.8 512.116 4 0 13 -4 48.1201 137.540 4 0 13 -3 26921.5 641.013 4 0 13 -2 36.7215 123.331 4 0 13 -1 9941.29 392.607 4 0 13 0-25.3934 125.212 4 0 13 1 6254.35 308.147 4 0 13 2-71.9880 111.267 4 0 13 3 24302.5 557.291 4 0 -14 -10 4636.42 176.670 2 0 -14 -9-70.0288 75.6374 2 0 -14 -8 1884.25 155.767 2 0 -14 -7 28.9485 91.5548 2 0 14 -7-25.2957 96.5798 4 0 14 -6 20124.7 513.086 4 0 -14 -6 19786.3 458.924 2 0 14 -5-67.3467 132.482 4 0 14 -4 120.291 140.222 4 0 14 -3-145.537 150.667 4 0 14 -2 4120.33 279.437 4 0 14 -1-184.521 151.095 4 0 14 0 540.696 152.650 4 0 14 1-109.387 128.788 4 0 14 2 4702.92 266.553 4 0 14 3 42.7532 102.888 4 0 -15 -9 3867.77 144.615 2 0 -15 -8-147.018 67.2520 2 0 -15 -7 2419.67 150.515 2 0 15 -7 2425.65 174.273 4 0 15 -6-65.4484 112.558 4 0 -15 -6 104.263 76.3771 2 0 15 -5 1890.33 194.991 4 0 15 -4-112.878 143.024 4 0 15 -3-86.1452 154.759 4 0 15 -2-161.261 156.394 4 0 15 -1 3079.24 245.189 4 0 15 0 6.78461 129.074 4 0 15 1 2095.90 202.453 4 0 15 2 145.163 113.900 4 0 15 3 989.332 140.890 4 0 16 -7 102.155 62.6414 4 0 16 -6 1650.77 149.577 4 0 16 -5 39.0191 112.162 4 0 16 -4 5549.13 281.771 4 0 16 -3-26.5546 134.026 4 0 16 -2 3172.81 238.278 4 0 16 -1-35.0402 131.820 4 0 16 0 284.164 139.045 4 0 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55195.6 1473.93 1 2 6 -1 106848. 2452.90 1 -2 6 -1 107845. 2085.82 1 -2 6 0 19036.5 972.004 1 2 6 0 17738.2 1044.98 1 -2 6 1 117387. 2627.79 1 2 6 1 114516. 2727.65 1 2 6 2 51371.0 1949.80 1 2 6 3 124824. 3276.09 1 2 6 4 34154.9 1849.29 1 2 6 5 6515.17 888.135 1 2 6 6 15190.2 1426.12 1 2 6 7 1282.57 589.292 1 -2 6 7 636.335 390.209 1 -2 6 8 5069.93 995.298 1 2 6 8 5162.12 1004.51 1 2 6 9 21716.3 2008.60 1 -2 6 9 23229.2 2078.74 1 2 6 13 2872.56 243.476 3 -2 6 14 389.662 105.514 3 2 6 14 425.858 100.005 3 2 -7 -14 7015.41 234.883 2 -2 -7 -14 6765.83 235.872 2 2 -7 -13 208.576 120.328 2 -2 -7 -13 104.575 115.319 2 -2 -7 -12 10915.2 404.226 2 2 -7 -12 11085.4 392.998 2 2 -7 -11 3271.83 255.688 2 -2 -7 -11 3540.74 264.367 2 -2 -7 -10 9790.14 398.089 2 2 -7 -10 9803.78 393.204 2 2 -7 -9 7752.41 339.910 2 -2 -7 -9 7767.53 345.401 2 -2 -7 -8 34194.5 657.689 2 2 7 -2 5547.13 511.036 1 -2 7 -1 6970.59 601.660 1 2 7 -1 5438.28 616.864 1 2 7 0 4094.81 591.938 1 -2 7 0 4889.11 545.656 1 2 7 1 9720.31 896.986 1 -2 7 1 9038.52 817.050 1 -2 7 2 2506.59 505.889 1 2 7 2 1932.33 458.745 1 -2 7 3 54701.3 2294.10 1 2 7 3 56455.9 2365.67 1 2 7 4 21688.2 1576.45 1 -2 7 4 22784.4 1599.63 1 -2 7 5 5433.10 887.883 1 2 7 5 5041.43 850.119 1 2 7 6 13200.9 1417.05 1 -2 7 6 16680.4 1578.76 1 2 7 7 8164.24 1228.67 1 -2 7 7 7533.15 1140.84 1 2 7 8 35479.3 2535.93 1 -2 7 8 34929.4 2536.25 1 2 7 9 8023.31 1257.45 1 -2 7 9 10870.3 1476.01 1 2 7 12 8105.39 335.074 3 2 7 13 544.015 118.921 3 2 7 14 4314.50 182.656 3 -2 7 14 4731.40 190.179 3 2 -8 -14 2304.89 131.819 2 -2 -8 -14 2432.85 136.510 2 -2 -8 -13 2.90696 100.816 2 2 -8 -13 78.3944 98.4343 2 2 -8 -12 2058.67 203.252 2 -2 -8 -12 2119.77 207.947 2 2 -8 -11 1044.31 187.884 2 -2 -8 -11 744.012 176.517 2 -2 -8 -10 1073.58 188.011 2 2 -8 -10 1114.77 187.088 2 2 -8 -9 1158.82 178.913 2 -2 -8 -9 1288.76 177.216 2 -2 -8 -8 7743.07 331.297 2 2 8 -1 2047.47 419.314 1 2 8 0 36827.2 1802.21 1 -2 8 0 32171.3 1539.55 1 2 8 1 633.480 323.288 1 -2 8 1 401.725 252.234 1 2 8 2 10223.7 1036.92 1 -2 8 2 9100.04 952.086 1 2 8 3 27982.0 1774.25 1 -2 8 3 29645.9 1816.97 1 2 8 4 9579.33 1143.92 1 -2 8 4 11102.4 1187.18 1 -2 8 5 7110.68 1056.07 1 2 8 5 7606.71 1097.25 1 -2 8 6 19015.7 1763.08 1 2 8 6 20845.6 1845.01 1 -2 8 7 10460.2 1404.97 1 2 8 7 11352.2 1438.17 1 -2 8 8 8349.05 1293.42 1 2 8 8 6779.12 1209.72 1 2 8 11 2283.53 193.362 3 2 8 12 2926.89 201.022 3 -2 8 13 331.806 99.1193 3 2 8 13 366.504 93.3078 3 -2 -9 -14 251.042 53.6779 2 -2 -9 -13 3318.60 185.199 2 2 -9 -13 3183.15 180.583 2 2 -9 -12 669.289 141.104 2 -2 -9 -12 543.671 133.561 2 2 -9 -11 1485.12 198.889 2 -2 -9 -11 1436.78 191.649 2 2 -9 -10 9074.94 381.759 2 -2 -9 -10 9773.45 389.657 2 -2 -9 -9 3385.18 254.348 2 2 -9 -9 2911.36 237.404 2 -2 -9 -8 1903.87 195.255 2 -2 9 -6 15402.5 425.775 4 2 9 -6 15675.1 416.058 4 -2 9 -5 7189.98 290.493 4 2 9 0 19041.3 1433.66 1 2 9 1 27157.5 1747.85 1 -2 9 1 26943.9 1627.01 1 -2 9 2 68812.1 2749.34 1 2 9 2 70645.8 2904.90 1 2 9 3 10934.6 1229.88 1 -2 9 3 11198.0 1196.97 1 -2 9 4 6830.35 1014.65 1 2 9 4 7009.16 1005.31 1 2 9 5 7028.41 1081.54 1 -2 9 5 5961.87 994.811 1 -2 9 6 15053.3 1639.81 1 2 9 6 12315.4 1505.19 1 -2 9 7-498.783 593.331 1 2 9 7-152.435 328.936 1 2 9 8 2990.54 918.874 1 -2 9 8 1648.75 636.775 1 2 9 10 7965.79 314.427 3 2 9 11 855.422 125.266 3 -2 9 12 1457.18 129.562 3 2 9 12 1268.07 123.344 3 -2 -10 -13 5323.59 199.446 2 2 -10 -13 5382.84 201.979 2 2 -10 -12 1452.48 154.807 2 -2 -10 -12 1399.33 149.885 2 -2 -10 -11 5456.88 276.895 2 2 -10 -11 5520.11 279.545 2 -2 -10 -10 2063.40 206.253 2 2 -10 -10 2119.83 216.845 2 2 -10 -9 5181.58 297.112 2 -2 -10 -9 5725.21 301.847 2 -2 -10 -8 4272.66 263.927 2 -2 10 -7 19024.3 490.838 4 -2 10 -6 5110.12 265.844 4 2 10 -6 4889.91 255.563 4 2 10 -5 12994.1 401.155 4 -2 10 -5 13552.9 415.458 4 2 10 -4 6893.05 292.452 4 -2 10 -4 6860.37 292.002 4 -2 10 -3 6249.76 275.281 4 2 10 -3 5840.28 267.367 4 2 10 1 12600.2 1288.92 1 -2 10 1 13082.6 1243.36 1 -2 10 2 8643.61 1085.46 1 2 10 2 7646.83 1067.69 1 -2 10 3 7236.75 1035.38 1 2 10 3 5468.91 923.576 1 -2 10 4 4952.21 943.441 1 2 10 4 6027.42 1008.21 1 -2 10 5 12147.1 1473.38 1 2 10 5 13399.0 1567.80 1 2 10 6 4758.48 948.309 1 -2 10 6 4583.68 1024.01 1 2 10 7 18971.5 1999.84 1 -2 10 7 16204.0 1832.28 1 2 -11 -13 386.582 62.7936 2 -2 -11 -12 1554.22 133.506 2 2 -11 -12 1959.15 148.821 2 -2 -11 -11 178.988 110.104 2 2 -11 -11 125.449 107.066 2 -2 -11 -10 3886.50 242.639 2 2 -11 -10 4268.46 260.589 2 -2 -11 -9 476.561 142.612 2 2 -11 -9 480.224 156.850 2 -2 -11 -8 3205.93 233.386 2 -2 11 -7 3292.79 228.405 4 2 11 -7 2937.72 208.867 4 2 11 -6 1694.47 175.857 4 -2 11 -6 1551.70 178.749 4 2 11 -5 3791.67 237.941 4 -2 11 -5 3291.03 230.248 4 2 11 -4 2815.66 211.061 4 -2 11 -4 3195.18 223.759 4 2 11 -3 1178.41 149.574 4 -2 11 -3 1175.80 145.162 4 2 11 -2 4222.08 240.230 4 -2 11 -2 4074.25 236.696 4 2 11 -1 6976.91 299.818 4 -2 11 -1 6645.50 291.296 4 2 11 0 380.407 107.778 4 -2 11 0 195.270 85.5267 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142.277 2 3 1 -1 162530. 1773.24 1 3 1 0 13857.5 552.216 1 3 1 1 162320. 1900.09 1 3 -1 1 164287. 1248.45 1 3 -1 2 21572.2 537.540 1 3 1 2 22940.7 812.019 1 3 1 3 270881. 3176.56 1 3 -1 3 271582. 2395.50 1 3 -1 4 57743.8 1348.14 1 3 1 4 59725.1 1689.23 1 3 -1 5 3093.81 376.755 1 3 1 5 3165.04 451.854 1 3 -1 6 1228.62 281.394 1 3 1 6 1264.51 345.964 1 3 1 7 5197.74 690.595 1 3 -1 7 4573.17 549.091 1 3 1 8 444.776 291.860 1 3 1 9 1484.75 439.710 1 3 1 14 3306.22 219.889 3 3 -1 14 3569.51 219.365 3 3 1 15 2493.49 158.235 3 3 -1 15 2638.68 153.241 3 -3 1 15 2948.94 180.758 3 -3 -1 15 3037.07 165.023 3 3 -2 -14 3534.05 181.215 2 -3 -2 -14 3819.12 205.040 2 -3 -2 -13 6377.11 304.090 2 3 -2 -13 5830.12 276.063 2 -3 2 -12 4980.51 261.001 2 -3 -2 -12 4856.40 288.347 2 3 -2 -12 4913.86 272.225 2 -3 -2 -11 13727.5 461.873 2 -3 2 -11 13303.8 421.416 2 3 -2 -11 13442.1 442.059 2 -3 2 -10 355.897 104.215 2 3 -2 -10 572.360 131.940 2 -3 -2 -10 317.085 115.567 2 -3 2 -9 10063.5 345.301 2 -3 -2 -9 10852.3 371.544 2 3 -2 -9 10831.1 353.692 2 3 2 -2 50951.8 1103.56 1 3 2 -1 130786. 1766.80 1 3 2 0 324709. 2996.96 1 3 2 1 144898. 2079.86 1 3 2 2 52433.9 1383.98 1 3 2 3 65859.7 1738.61 1 3 -2 3 66454.6 892.192 1 3 -2 4 48120.4 1014.40 1 3 2 4 47098.3 1646.87 1 3 -2 5 106097. 1860.11 1 3 2 5 94255.4 2556.73 1 3 -2 6 14434.6 787.897 1 3 2 6 11637.1 974.438 1 3 2 7 19483.4 1387.94 1 3 2 8 7685.33 966.779 1 3 2 9 10366.8 1166.14 1 -3 2 10 301.763 296.680 1 3 2 14 4100.71 245.425 3 3 -2 14 3940.39 205.967 3 3 2 15 4395.45 200.001 3 3 -2 15 4083.75 158.639 3 -3 -2 15 3857.74 161.496 3 -3 2 15 4720.55 210.161 3 3 -3 -14 8395.03 277.125 2 -3 -3 -14 8353.16 295.830 2 -3 -3 -13 9958.78 373.008 2 3 -3 -13 9910.70 354.362 2 -3 -3 -12 8110.59 361.228 2 3 -3 -12 7693.20 341.265 2 -3 -3 -11 1383.93 188.848 2 3 -3 -11 1746.94 187.656 2 3 -3 -10 4429.35 258.310 2 -3 3 -10 4258.54 236.948 2 -3 -3 -10 4937.19 277.159 2 3 -3 -9 5345.12 258.743 2 -3 -3 -9 5742.83 280.557 2 -3 3 -9 5208.06 248.527 2 3 3 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7892.78 795.624 1 3 4 5 102770. 3000.80 1 3 4 6 81226.1 2901.26 1 3 4 7 13959.2 1325.67 1 3 4 8 8493.44 1143.32 1 3 4 9 6611.82 1041.29 1 -3 4 9 8826.43 1228.45 1 -3 4 10 1409.85 506.295 1 3 4 10 2141.42 666.501 1 3 4 14 376.233 120.842 3 3 4 15 1619.72 124.874 3 -3 4 15 1671.06 125.887 3 3 -5 -14 2892.35 172.006 2 -3 -5 -14 2844.78 179.234 2 3 -5 -13 125.083 115.561 2 -3 -5 -13 50.9542 134.376 2 -3 -5 -12 9210.89 387.418 2 3 -5 -12 8995.21 369.054 2 -3 -5 -11 2684.82 236.979 2 3 -5 -11 2968.72 242.126 2 3 -5 -10 5965.68 306.649 2 -3 -5 -10 5893.42 313.053 2 -3 -5 -9 18592.6 499.780 2 3 -5 -9 18782.1 494.237 2 -3 -5 -8 17562.6 456.069 2 3 5 -3 55172.8 1338.11 1 3 5 -2 112863. 2093.70 1 3 5 -1 61679.5 1765.51 1 -3 5 -1 65951.2 1330.22 1 3 5 0 331770. 4186.54 1 3 5 1 64346.2 1920.35 1 3 5 2 85924.4 2370.45 1 3 5 3 59820.8 2131.41 1 3 5 4 85022.3 2743.99 1 3 5 5 9811.27 1021.14 1 3 5 6 25931.9 1768.55 1 3 5 7 9663.88 1150.21 1 3 5 8 23908.6 1931.62 1 -3 5 9 19961.5 1892.18 1 3 5 9 17548.0 1744.39 1 3 5 10 3664.28 839.563 1 -3 5 10 2509.91 756.125 1 3 5 13 103.817 136.970 3 3 5 14 3560.98 213.506 3 3 5 15 786.376 86.2955 3 -3 5 15 862.369 88.9631 3 3 -6 -14 1269.33 121.587 2 -3 -6 -14 1294.23 129.787 2 3 -6 -13 5714.92 279.346 2 -3 -6 -13 5850.10 281.892 2 -3 -6 -12 2826.61 250.268 2 3 -6 -12 2443.28 220.733 2 -3 -6 -11 2785.77 243.241 2 3 -6 -11 2760.69 234.197 2 3 -6 -10 752.257 168.560 2 -3 -6 -10 893.053 175.299 2 -3 -6 -9 5631.64 293.756 2 3 -6 -9 5795.16 291.711 2 -3 -6 -8 11654.0 382.442 2 3 6 -3 23808.0 917.343 1 3 6 -2 44827.5 1429.58 1 3 6 -1 43436.6 1622.72 1 -3 6 -1 43159.7 1269.41 1 -3 6 0 26263.7 1107.76 1 3 6 0 24926.0 1271.26 1 3 6 1 45730.5 1772.91 1 3 6 2 40820.4 1772.99 1 3 6 3 20313.1 1322.77 1 3 6 4 57653.0 2400.77 1 3 6 5 11628.6 1161.30 1 3 6 6 17685.3 1529.61 1 3 6 7 13329.5 1424.11 1 -3 6 8 11484.5 1417.77 1 3 6 8 9742.43 1287.77 1 -3 6 9 3406.66 855.841 1 3 6 9 3082.75 811.584 1 3 6 13 6538.71 292.284 3 -3 6 14 989.987 125.179 3 3 6 14 1137.03 123.132 3 -3 -7 -14 2020.31 143.155 2 3 -7 -14 2130.78 139.285 2 3 -7 -13 2576.47 195.997 2 -3 -7 -13 2312.92 190.665 2 -3 -7 -12 260.445 154.897 2 3 -7 -12 378.717 140.983 2 -3 -7 -11 2141.45 228.370 2 3 -7 -11 2153.81 219.115 2 -3 -7 -10 664.901 163.902 2 3 -7 -10 898.594 173.440 2 -3 -7 -9 1386.29 180.044 2 -3 -7 -8 1186.28 158.503 2 3 7 -2 16315.7 924.942 1 -3 7 -1 20945.7 1012.41 1 3 7 -1 20398.2 1216.25 1 3 7 0 13270.2 1028.51 1 -3 7 0 13454.5 884.653 1 3 7 1 21358.3 1331.87 1 -3 7 1 24002.8 1298.32 1 3 7 2 17182.4 1265.33 1 -3 7 2 16998.8 1211.28 1 3 7 3 15347.1 1251.79 1 3 7 4 3648.44 679.132 1 3 7 5 20239.3 1624.80 1 3 7 6 2481.96 643.405 1 -3 7 6 3529.62 770.933 1 3 7 7 3509.06 774.095 1 -3 7 7 4367.55 899.047 1 -3 7 8 663.770 497.652 1 3 7 8 1480.23 638.532 1 -3 7 9 2408.49 689.122 1 3 7 9 236.518 383.738 1 3 7 12 112.758 135.701 3 3 7 13 2427.25 175.006 3 -3 7 14 2298.86 141.631 3 3 7 14 2418.86 147.371 3 3 -8 -14 521.001 80.2903 2 -3 -8 -14 417.667 79.4859 2 3 -8 -13 1934.05 166.324 2 -3 -8 -13 2281.14 176.795 2 -3 -8 -12 1820.01 192.967 2 3 -8 -12 1710.75 187.258 2 -3 -8 -11 5256.71 307.198 2 3 -8 -11 5899.54 312.532 2 -3 -8 -10 842.511 176.865 2 3 -8 -10 756.686 170.486 2 -3 -8 -9 1340.69 179.305 2 -3 -8 -8 232.264 118.807 2 3 8 -1 4573.45 641.329 1 3 8 0 17084.1 1277.30 1 -3 8 0 18817.6 1157.34 1 3 8 1 5555.07 776.869 1 -3 8 1 6045.07 726.727 1 -3 8 2 8121.75 889.467 1 3 8 2 7776.12 929.292 1 -3 8 3 11236.6 1126.27 1 3 8 3 11097.5 1173.75 1 -3 8 4 26964.6 1851.30 1 3 8 4 28876.9 1933.66 1 3 8 5 4837.18 878.867 1 -3 8 5 3808.40 755.887 1 3 8 6 7621.57 1152.66 1 -3 8 6 7079.00 1101.81 1 3 8 7 3058.25 759.446 1 -3 8 7 3128.67 881.094 1 3 8 8-905.524 547.012 1 -3 8 8 124.872 402.850 1 3 8 11 5310.53 272.287 3 3 8 12 1662.35 160.831 3 3 8 13 1618.83 136.765 3 -3 8 13 1601.72 137.425 3 -3 -9 -14 2282.60 112.365 2 3 -9 -13 1851.68 149.444 2 -3 -9 -13 1992.90 155.632 2 -3 -9 -12 913.290 148.800 2 3 -9 -12 1099.50 156.215 2 -3 -9 -11 311.559 146.786 2 3 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6009.39 307.466 2 -3 -10 -8 2011.47 198.927 2 -3 10 -7 3880.30 236.980 4 -3 10 -6 6375.06 301.553 4 3 10 -6 6634.95 288.775 4 3 10 -5 13285.2 406.993 4 -3 10 -5 13454.7 422.316 4 -3 10 -4 1019.31 134.174 4 3 10 -4 1279.10 148.332 4 -3 10 -3 12380.3 385.360 4 3 10 -3 13121.0 391.704 4 3 10 1 934.768 457.617 1 3 10 2 3771.47 756.873 1 -3 10 2 4398.15 764.137 1 3 10 3 8150.43 1141.07 1 -3 10 3 7635.74 1036.25 1 3 10 4 339.073 301.913 1 -3 10 4 782.601 457.586 1 3 10 5 11142.0 1441.13 1 -3 10 5 11462.2 1438.55 1 -3 10 6 4657.58 967.804 1 3 10 6 5696.74 1085.14 1 -3 10 7 2633.70 851.317 1 3 10 7 3929.33 969.415 1 3 -11 -12 4591.14 204.866 2 -3 -11 -12 4853.04 205.960 2 3 -11 -11 352.678 118.073 2 -3 -11 -11 314.788 113.371 2 -3 -11 -10 6195.69 294.811 2 3 -11 -10 6447.43 304.041 2 3 -11 -9 1757.28 203.727 2 -3 -11 -9 1492.67 181.945 2 -3 -11 -8 3434.76 237.438 2 -3 11 -7 3657.61 244.615 4 -3 -11 -7 3625.10 238.042 2 -3 11 -6 18905.0 515.288 4 3 11 -6 18957.0 499.265 4 -3 11 -5 10379.2 385.609 4 3 11 -5 9685.91 364.635 4 3 11 -4 34417.9 669.087 4 -3 11 -4 34841.4 682.689 4 3 11 -3 5751.58 286.211 4 -3 11 -3 5937.80 290.606 4 -3 11 -2 15040.6 437.939 4 3 11 -2 14846.3 437.810 4 3 11 -1 3272.31 212.695 4 -3 11 -1 3166.87 210.791 4 3 11 0 3186.50 205.904 4 -3 11 0 3670.83 220.258 4 3 11 1 2415.30 181.767 4 -3 11 1 2288.50 179.468 4 3 11 2 18092.4 463.257 4 -3 11 2 17500.8 447.405 4 3 11 3 3522.45 798.698 1 -3 11 3 4395.82 889.607 1 3 11 3 4976.65 247.298 4 -3 11 3 5035.75 242.605 4 -3 11 4 39151.1 2592.88 1 3 11 4 35042.3 615.773 4 3 11 4 38256.3 2651.33 1 -3 11 5 8894.34 1321.28 1 3 11 5 9289.82 1382.49 1 3 11 6 14425.3 1762.53 1 -3 11 6 13653.0 1670.81 1 3 -12 -12 192.286 65.1755 2 -3 -12 -12 132.223 55.5223 2 -3 -12 -11 1522.22 133.482 2 3 -12 -11 1568.47 141.085 2 -3 -12 -10 530.162 114.113 2 3 -12 -10 760.013 139.701 2 3 -12 -9 2421.73 207.271 2 -3 -12 -9 2150.96 189.178 2 -3 -12 -8 1174.55 157.727 2 -3 12 -8 1079.01 145.002 4 3 12 -7 8317.75 321.900 4 -3 12 -7 8211.93 347.431 4 -3 -12 -7 9087.68 343.182 2 -3 12 -6 10556.8 397.778 4 3 12 -6 10674.7 390.774 4 3 12 -5 6441.78 316.497 4 -3 12 -5 6578.82 328.570 4 3 12 -4 8772.46 362.282 4 -3 12 -4 8702.56 370.034 4 -3 12 -3 7724.63 343.563 4 3 12 -3 8146.75 349.518 4 -3 12 -2 10223.1 390.030 4 3 12 -2 11024.2 395.069 4 -3 12 -1 16884.2 481.150 4 3 12 -1 16940.5 481.319 4 -3 12 0 3705.83 241.425 4 3 12 0 3228.29 223.830 4 3 12 1 15921.3 455.572 4 -3 12 1 14792.1 443.512 4 3 12 2 8998.35 345.262 4 -3 12 2 9420.88 348.997 4 -3 12 3 3857.67 223.195 4 3 12 3 3921.74 233.822 4 3 12 4 9105.42 326.823 4 3 12 4 7319.97 1249.06 1 3 -13 -11 846.815 94.6255 2 -3 -13 -11 748.336 82.6675 2 -3 -13 -10 2297.27 153.233 2 3 -13 -10 2116.16 160.584 2 3 -13 -9 978.185 141.266 2 -3 -13 -9 923.531 125.378 2 3 -13 -8 4044.92 236.287 2 -3 13 -8 3388.14 209.785 4 -3 -13 -8 4019.26 225.464 2 -3 13 -7 1874.04 183.905 4 3 13 -7 1446.91 153.501 4 -3 -13 -7 1520.00 156.763 2 -3 13 -6 923.820 157.990 4 3 13 -6 941.151 151.012 4 -3 -13 -6 1074.89 143.790 2 -3 13 -5 17986.7 525.344 4 3 13 -5 18213.9 514.831 4 3 13 -4 7223.56 346.032 4 -3 13 -4 7133.65 348.276 4 3 13 -3 10764.6 407.662 4 -3 13 -3 9691.74 398.302 4 3 13 -2 362.124 134.952 4 -3 13 -2 539.361 155.288 4 3 13 -1 15150.5 476.459 4 -3 13 -1 15046.3 479.102 4 -3 13 0 348.742 136.068 4 3 13 0 165.930 122.123 4 -3 13 1 14774.2 454.527 4 3 13 1 14695.5 457.823 4 3 13 2 775.183 151.875 4 -3 13 2 739.306 138.154 4 -3 13 3 11114.3 377.885 4 3 13 3 10461.6 372.515 4 3 13 4 4148.64 231.438 4 -3 -14 -10 679.449 72.9069 2 3 -14 -10 909.881 95.5205 2 -3 -14 -9 1724.29 126.780 2 3 -14 -9 1915.98 144.336 2 -3 -14 -8 424.861 92.8824 2 3 -14 -8 762.540 125.270 2 -3 14 -8 490.375 104.378 4 -3 14 -7 1565.68 167.147 4 3 -14 -7 1825.67 167.510 2 -3 -14 -7 1815.36 151.347 2 3 14 -7 1780.56 155.808 4 -3 14 -6 916.904 158.459 4 3 14 -6 944.175 152.338 4 3 14 -5 757.761 157.808 4 -3 14 -5 1016.68 179.905 4 3 14 -4 1387.68 185.469 4 -3 14 -4 1758.50 214.162 4 3 14 -3 773.179 175.485 4 -3 14 -3 813.742 178.362 4 -3 14 -2 2607.02 233.222 4 3 14 -2 2581.62 225.976 4 -3 14 -1 1508.18 200.468 4 3 14 -1 1327.37 191.181 4 3 14 0 1264.74 179.650 4 -3 14 0 1312.51 191.538 4 -3 14 1 1992.79 195.783 4 3 14 1 2302.35 216.719 4 -3 14 2 2211.29 200.036 4 3 14 2 2444.15 210.290 4 3 14 3 931.400 147.282 4 -3 14 3 989.896 138.795 4 3 14 4 1648.64 161.047 4 3 -15 -9 615.017 72.9240 2 3 -15 -8 1274.12 115.590 2 3 15 -7 245.492 84.1164 4 3 -15 -7 75.0009 78.1123 2 -3 15 -7 158.544 94.3692 4 -3 15 -6 813.545 141.501 4 3 15 -6 1146.64 147.430 4 -3 15 -5 2660.39 221.978 4 3 15 -5 2883.74 218.916 4 -3 15 -4-71.6808 142.759 4 3 15 -4 293.541 149.752 4 -3 15 -3 1029.60 181.442 4 3 15 -3 1389.10 189.085 4 -3 15 -2 1104.91 188.823 4 3 15 -2 1453.64 204.074 4 3 15 -1 1421.17 195.395 4 -3 15 -1 1588.13 194.517 4 -3 15 0 370.757 138.848 4 3 15 0 332.968 145.883 4 3 15 1 1645.97 185.458 4 -3 15 1 1202.17 169.132 4 -3 15 2 978.202 145.907 4 3 15 2 1189.56 166.759 4 3 15 3 1272.14 152.067 4 -3 15 3 917.323 132.438 4 3 16 -7 762.056 84.7748 4 3 -16 -7 639.338 74.8905 2 -3 16 -6 3029.05 193.586 4 3 16 -6 3223.78 181.253 4 3 16 -5 4155.40 226.525 4 -3 16 -5 3682.87 227.414 4 -3 16 -4 1068.54 160.108 4 3 16 -4 1313.77 167.790 4 -3 16 -3 172.032 138.377 4 3 16 -3 452.558 150.158 4 -3 16 -2 808.576 164.584 4 3 16 -2 781.728 173.946 4 3 16 -1 387.424 150.972 4 -3 16 -1 169.547 127.656 4 3 16 0 148.008 133.168 4 -3 16 0-0.33903 123.879 4 3 16 1 816.895 144.189 4 -3 16 1 858.127 140.965 4 3 16 2 908.761 142.800 4 -3 16 2 814.502 129.462 4 -3 16 3 84.3723 84.4836 4 3 17 -6 706.813 82.4941 4 -3 17 -6 584.991 82.9214 4 -3 17 -5 2845.55 177.337 4 3 17 -5 3158.80 173.135 4 3 17 -4 8205.88 284.619 4 -3 17 -4 8326.89 300.190 4 -3 17 -3 680.209 133.841 4 3 17 -3 1040.23 146.385 4 3 17 -2 198.163 122.149 4 -3 17 -2 74.7443 116.150 4 3 17 -1 428.931 131.776 4 -3 17 -1 436.425 129.280 4 3 17 0 823.481 138.400 4 -3 17 0 1143.36 150.166 4 3 17 1 262.016 107.877 4 -3 17 1 138.894 89.0748 4 -3 17 2 531.558 98.2788 4 -3 18 -5 1657.72 105.913 4 -3 18 -4 2589.50 146.562 4 3 18 -4 2541.76 141.731 4 -3 18 -3 1285.46 121.014 4 3 18 -3 1333.03 123.207 4 -3 18 -2 975.659 115.568 4 3 18 -2 994.317 121.366 4 -3 18 -1 838.904 111.151 4 3 18 -1 954.008 120.618 4 -3 18 0 1188.84 117.823 4 -3 18 1 1339.96 116.628 4 -4 0 -13 6024.19 280.894 2 -4 0 -12 878.295 156.651 2 -4 0 -11 27343.8 624.471 2 -4 0 -10 13885.6 441.861 2 -4 0 -9 16787.2 457.027 2 4 0 0 179980. 1871.31 1 4 0 1 17715.1 624.931 1 4 0 2 83533.9 1410.27 1 4 0 3 33452.2 1022.62 1 4 0 4 128429. 2285.10 1 4 0 5 53934.2 1655.40 1 4 0 6 33034.5 1457.75 1 4 0 7 25540.6 1405.52 1 4 0 8 44128.9 1976.04 1 4 0 14 115.232 109.994 3 4 0 15 6794.54 231.501 3 -4 0 15 6755.43 238.299 3 -4 -1 -13 3487.39 229.935 2 4 -1 -12 1423.23 163.609 2 -4 -1 -12 1540.95 186.542 2 -4 1 -12 1261.09 163.661 2 -4 1 -11 14850.7 455.628 2 4 -1 -11 14801.7 451.524 2 -4 -1 -11 15038.3 476.466 2 4 -1 -10 35286.5 656.718 2 -4 -1 -10 35735.9 704.007 2 -4 1 -10 33998.6 668.731 2 -4 1 -9 28539.7 588.114 2 4 -1 -9 27526.1 548.053 2 4 1 -1 10503.6 511.615 1 4 1 0 732.419 164.476 1 4 1 1 9440.38 508.558 1 4 -1 1 9035.80 365.536 1 4 1 2 110962. 1856.57 1 4 -1 2 117683. 1402.28 1 4 -1 3 232734. 2283.22 1 4 1 3 224356. 2984.82 1 4 1 4 27909.2 1175.57 1 4 -1 4 29487.8 962.527 1 4 1 5 783.914 254.048 1 4 -1 5 711.514 202.983 1 4 -1 6 10145.2 737.271 1 4 1 6 10752.3 902.296 1 4 -1 7 3009.92 440.760 1 4 1 7 2156.83 458.838 1 4 1 8 4382.25 685.045 1 4 -1 14 2291.51 175.720 3 4 1 14 2225.65 191.236 3 -4 -1 15 496.343 96.1279 3 4 -1 15 458.882 84.2880 3 4 1 15 441.294 92.6044 3 -4 -2 -14 570.252 116.313 2 -4 -2 -13 2009.32 193.449 2 4 -2 -13 1830.45 168.861 2 4 -2 -12 111.960 104.959 2 -4 -2 -12 96.2348 130.756 2 4 -2 -11 16284.0 474.325 2 -4 2 -11 16758.7 468.726 2 -4 -2 -11 16982.1 511.711 2 -4 -2 -10 1813.28 190.978 2 -4 2 -10 1591.42 165.218 2 4 -2 -10 1756.20 171.512 2 4 -2 -9 38108.8 654.579 2 -4 2 -9 36824.5 661.021 2 -4 -2 -9 38789.0 692.653 2 4 2 -2 377079. 3318.19 1 4 2 -1 58349.2 1299.09 1 4 2 0 79321.3 1636.00 1 4 2 1 65766.9 1491.36 1 4 -2 2 364680. 1543.79 1 4 2 2 380149. 3854.35 1 4 2 3 291502. 3737.67 1 4 -2 3 293430. 2020.47 1 4 -2 4 5565.76 352.464 1 4 2 4 5164.65 570.114 1 4 -2 5 68023.3 1446.53 1 4 2 5 68117.6 2174.25 1 4 2 6 20318.9 1298.19 1 4 2 7 37279.8 1922.86 1 4 2 8 2208.01 545.806 1 4 2 9 32876.9 2067.14 1 -4 2 10 4506.57 851.505 1 4 -2 13 755.464 143.353 3 4 2 14 725.024 170.485 3 4 -2 14 694.691 123.173 3 4 2 15 3517.86 179.521 3 4 -2 15 3109.98 139.094 3 -4 -2 15 3321.29 148.627 3 -4 -3 -14 1335.82 144.046 2 4 -3 -14 1316.11 123.138 2 4 -3 -13 1808.87 173.840 2 -4 -3 -13 1944.71 193.181 2 4 -3 -12 4231.80 258.768 2 -4 -3 -12 4436.27 281.781 2 -4 -3 -11 663.872 158.825 2 4 -3 -11 670.837 146.354 2 -4 -3 -10 7557.10 340.571 2 4 -3 -10 7236.88 322.338 2 -4 3 -10 6959.02 299.668 2 -4 3 -9 10620.7 350.964 2 4 -3 -9 10915.6 364.528 2 -4 -3 -9 11245.1 384.246 2 4 3 -2 22179.7 856.374 1 4 3 -1 118329. 2097.60 1 4 3 0 182854. 2717.67 1 4 3 1 128093. 2300.34 1 4 3 2 19967.8 980.919 1 4 3 3 47784.7 1666.34 1 4 3 4 9512.52 812.415 1 4 3 5 14008.8 1072.32 1 4 3 6 2885.29 582.547 1 4 3 7 8113.83 960.272 1 4 3 8 3646.31 708.062 1 4 3 9 10917.0 1274.27 1 -4 3 10 3968.63 842.999 1 4 3 10 5582.90 959.592 1 4 -3 13 1753.38 164.471 3 4 3 14 2056.84 201.476 3 4 -3 14 1617.68 132.270 3 4 3 15 429.084 97.3754 3 -4 3 15 332.068 99.2176 3 -4 -4 -14 601.962 116.463 2 4 -4 -14 562.287 99.1716 2 4 -4 -13 494.087 128.822 2 -4 -4 -13 475.363 140.028 2 -4 -4 -12 4983.47 299.985 2 4 -4 -12 4954.80 279.997 2 4 -4 -11 7525.05 336.384 2 -4 -4 -11 7313.54 354.897 2 -4 -4 -10 8418.84 359.610 2 4 -4 -10 9547.32 364.730 2 4 -4 -9 1050.73 143.954 2 -4 -4 -9 1134.57 153.207 2 -4 -4 -8 13805.8 399.563 2 4 4 -3 134373. 2187.48 1 4 4 -2 6125.52 498.769 1 4 4 -1 65991.7 1750.84 1 4 4 0 486589. 4872.04 1 4 4 1 72632.6 1926.98 1 4 4 2 5712.84 598.263 1 4 4 3 134887. 2987.95 1 4 4 4 958.053 378.762 1 4 4 5 14838.4 1176.39 1 4 4 6 27590.2 1728.96 1 4 4 7 1376.47 473.839 1 4 4 8 13843.2 1398.67 1 4 4 9 542.186 424.649 1 4 4 10 7457.83 1127.55 1 -4 4 10 7551.85 1224.40 1 4 -4 12 5323.09 260.411 3 4 4 13 459.562 161.909 3 4 4 14 570.364 132.013 3 4 4 15 621.405 91.2023 3 -4 4 15 516.372 88.7511 3 -4 -5 -14 3644.68 196.733 2 4 -5 -14 3857.70 189.206 2 -4 -5 -13 552.293 142.673 2 4 -5 -13 866.831 140.773 2 -4 -5 -12 3452.61 266.404 2 4 -5 -12 3764.10 251.812 2 -4 -5 -11 2206.24 225.665 2 4 -5 -11 2605.66 226.244 2 -4 -5 -10 14740.7 476.405 2 4 -5 -10 15121.5 461.225 2 4 -5 -9 22657.2 535.007 2 -4 -5 -9 22043.8 550.137 2 -4 -5 -8 1254.00 141.654 2 4 5 -3 10558.3 640.031 1 4 5 -2 28800.6 1117.18 1 4 5 -1 157974. 2935.23 1 -4 5 -1 162624. 2069.92 1 4 5 0 58099.4 1847.02 1 4 5 1 156248. 3097.91 1 4 5 2 33139.1 1496.09 1 4 5 3 8910.73 841.946 1 4 5 4 5772.66 742.361 1 4 5 5 6670.65 868.819 1 4 5 6 7327.64 973.646 1 4 5 7 11731.2 1307.75 1 4 5 8 1912.98 625.953 1 4 5 9 28707.4 2219.65 1 -4 5 9 25513.0 2154.03 1 -4 5 10 17795.4 1833.22 1 4 5 10 18608.4 1871.54 1 4 5 13 397.067 142.851 3 4 5 14 2417.39 179.151 3 -4 5 15 251.310 64.9730 3 4 5 15 285.148 66.7050 3 4 -6 -14 681.333 99.9704 2 -4 -6 -14 695.556 112.207 2 4 -6 -13 1826.60 177.181 2 -4 -6 -13 1931.59 192.078 2 4 -6 -12 1501.90 189.138 2 -4 -6 -12 1266.07 194.296 2 4 -6 -11 8970.34 375.981 2 -4 -6 -11 9328.29 391.591 2 4 -6 -10 1549.66 190.099 2 -4 -6 -10 1271.92 189.823 2 -4 -6 -9 15046.9 463.546 2 -4 -6 -8 15637.3 443.876 2 4 6 -3 20148.1 922.441 1 4 6 -2 5146.43 523.893 1 4 6 -1 43061.2 1679.44 1 -4 6 -1 43481.7 1262.33 1 -4 6 0 77796.5 1915.51 1 4 6 0 75630.8 2296.63 1 4 6 1 42907.2 1770.31 1 4 6 2 4204.01 607.106 1 4 6 3 24060.1 1478.87 1 4 6 4 56589.7 2405.96 1 4 6 5 42270.1 2223.54 1 4 6 6 7708.13 1060.57 1 4 6 7 25281.8 1954.71 1 -4 6 8 17551.6 1768.56 1 4 6 8 18453.0 1774.01 1 4 6 9 13679.9 1641.60 1 -4 6 9 12504.4 1559.13 1 4 6 12 1969.37 202.758 3 4 6 13 1816.28 174.817 3 -4 6 14 517.858 105.816 3 4 6 14 395.230 100.435 3 -4 -7 -14 1963.12 138.144 2 4 -7 -14 1658.68 123.714 2 -4 -7 -13 1511.52 161.972 2 4 -7 -13 1428.96 158.706 2 -4 -7 -12 6468.29 326.652 2 4 -7 -12 6665.49 310.068 2 -4 -7 -11 489.044 169.435 2 4 -7 -11 543.838 154.270 2 4 -7 -10 3766.90 268.461 2 -4 -7 -10 3191.14 249.455 2 -4 -7 -9 83.0406 121.254 2 -4 -7 -8 5851.28 286.752 2 4 7 -2 45679.1 1635.41 1 -4 7 -1 11116.1 725.598 1 4 7 -1 10450.2 908.825 1 4 7 0 20272.4 1314.45 1 -4 7 0 18958.3 1049.25 1 4 7 1 9677.08 913.738 1 -4 7 1 9207.57 825.832 1 4 7 2 37656.0 1893.43 1 4 7 3 30264.3 1773.05 1 4 7 4 17576.2 1446.87 1 4 7 5 10215.7 1171.94 1 4 7 6 22335.1 1820.13 1 4 7 7 1203.07 561.654 1 -4 7 7 1306.09 539.849 1 -4 7 8 6373.83 1064.50 1 4 7 8 6228.96 1079.47 1 -4 7 9 449.231 355.631 1 4 7 9 1063.08 563.471 1 4 7 12 5674.89 281.122 3 4 7 13 2005.69 165.206 3 -4 7 14 2164.39 133.895 3 4 7 14 2463.67 139.516 3 -4 -8 -14 201.070 66.9032 2 4 -8 -14 275.063 66.9277 2 4 -8 -13 3238.43 197.747 2 -4 -8 -13 3451.20 203.984 2 -4 -8 -12 869.947 167.688 2 4 -8 -12 605.213 143.871 2 -4 -8 -11 3876.58 266.789 2 4 -8 -11 4216.28 275.583 2 -4 -8 -10 70.3433 135.808 2 4 -8 -10-4.59305 137.801 2 -4 -8 -9 4297.12 272.548 2 -4 -8 -8 366.923 130.426 2 4 8 -1 102987. 2976.69 1 -4 8 0 8583.28 778.948 1 4 8 0 9055.79 968.788 1 -4 8 1 118650. 3150.23 1 4 8 1 121861. 3534.38 1 -4 8 2 12252.2 1086.18 1 4 8 2 11923.8 1166.19 1 4 8 3 25960.5 1765.72 1 -4 8 3 28184.2 1771.38 1 4 8 4 3032.44 709.012 1 -4 8 4 4038.35 746.943 1 -4 8 5 3696.55 785.110 1 4 8 5 3072.78 714.303 1 4 8 6 15847.2 1627.98 1 -4 8 6 16504.0 1675.53 1 -4 8 7 2840.85 747.787 1 4 8 7 4448.01 903.421 1 -4 8 8 1414.90 640.520 1 4 8 8-92.2318 365.804 1 4 8 10 234.504 114.035 3 4 8 11 2057.29 191.440 3 4 8 12 986.126 135.149 3 4 8 13 2922.06 163.468 3 -4 8 13 2789.15 163.253 3 4 -9 -13 1608.91 137.883 2 -4 -9 -13 1960.66 151.892 2 -4 -9 -12 2061.22 191.766 2 4 -9 -12 1874.06 178.988 2 -4 -9 -11 3478.41 248.675 2 4 -9 -11 3567.01 255.086 2 -4 -9 -10 3422.23 253.708 2 4 -9 -10 3296.77 253.408 2 -4 -9 -9 1224.23 179.306 2 -4 -9 -8 6666.26 316.973 2 -4 -9 -7 21188.3 511.443 2 -4 9 -7 20208.6 501.531 4 -4 9 -6 6246.77 282.424 4 -4 9 -5 446.093 102.459 4 4 9 -5 413.921 91.6460 4 4 9 -1 34525.0 1800.10 1 4 9 0 4388.62 701.007 1 4 9 1 37479.0 2130.92 1 -4 9 1 34613.7 1837.50 1 -4 9 2 34725.5 1961.77 1 4 9 2 33825.0 2073.70 1 4 9 3 3536.79 776.926 1 -4 9 3 4258.20 772.496 1 4 9 4 8298.95 1139.22 1 -4 9 4 9122.90 1157.69 1 -4 9 5 380.537 319.330 1 4 9 5 382.856 467.395 1 -4 9 6 4619.05 970.216 1 4 9 6 5562.95 1104.26 1 -4 9 7 22009.5 2101.64 1 4 9 7 21329.5 2075.66 1 4 9 8 7439.52 1300.67 1 -4 9 8 8386.52 1362.71 1 4 9 10 3946.87 228.074 3 4 9 11 3506.18 202.193 3 4 9 12 1342.18 124.482 3 -4 9 12 1266.28 120.713 3 4 -10 -13 2755.00 147.560 2 -4 -10 -13 2870.12 146.711 2 -4 -10 -12 2215.91 165.397 2 4 -10 -12 2381.00 177.295 2 -4 -10 -11-134.903 120.702 2 4 -10 -11-95.3464 134.449 2 4 -10 -10 3198.27 247.049 2 -4 -10 -10 3206.67 238.268 2 -4 -10 -9-10.9598 122.612 2 -4 -10 -8 8440.84 354.361 2 -4 10 -7 5460.34 282.436 4 -4 -10 -7 5983.62 288.062 2 4 10 -6 257.835 95.1493 4 -4 10 -6 263.576 112.260 4 -4 10 -5 19849.4 510.369 4 4 10 -5 19522.9 483.353 4 4 10 -4 3887.84 225.010 4 -4 10 -4 4086.74 242.546 4 -4 10 -3 4015.41 226.524 4 4 10 -3 4626.93 240.043 4 4 10 0 20106.6 1632.28 1 4 10 1 8127.37 1044.66 1 -4 10 2 21192.3 1630.46 1 4 10 2 24398.1 1903.46 1 4 10 3 2109.39 644.855 1 -4 10 3 1925.74 587.338 1 -4 10 4 3057.22 752.226 1 4 10 4 2752.28 745.031 1 4 10 5 22234.4 2043.09 1 -4 10 5 19903.8 1878.01 1 -4 10 6 482.964 425.801 1 4 10 6-206.742 403.650 1 4 10 7 3416.40 856.202 1 -4 10 7 2352.88 772.313 1 -4 -11 -12 174.132 82.7536 2 4 -11 -12 201.246 88.1510 2 -4 -11 -11 281.298 108.974 2 4 -11 -11 262.712 116.833 2 -4 -11 -10 1365.45 164.579 2 4 -11 -10 1742.65 195.733 2 -4 -11 -9 5235.93 279.122 2 4 -11 -9 5004.08 286.419 2 -4 -11 -8 2200.30 198.165 2 -4 11 -7 1164.50 159.837 4 -4 -11 -7 1033.78 154.821 2 -4 11 -6 24502.5 587.223 4 4 11 -6 23825.8 556.235 4 -4 11 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7139.81 1 5 3 3 57081.2 1847.29 1 5 3 4 147075. 3184.57 1 5 3 5 32591.6 1636.49 1 5 3 6 15517.6 1223.19 1 5 3 7 14210.0 1259.36 1 5 3 8 43004.4 2347.16 1 5 3 9 4416.24 807.912 1 5 -3 12 162.112 111.742 3 5 3 13 195.392 146.644 3 5 -3 13 112.425 91.8699 3 5 -3 14 1762.51 132.698 3 5 3 14 1879.85 174.058 3 5 3 15 1111.65 110.485 3 5 -4 -14 5606.05 221.105 2 -5 -4 -14 6247.85 256.996 2 5 -4 -13 9209.66 334.686 2 -5 -4 -13 9491.68 364.990 2 -5 -4 -12 7783.86 360.572 2 5 -4 -12 7425.62 328.636 2 5 -4 -11 6793.27 324.895 2 -5 -4 -11 6353.75 335.258 2 -5 -4 -10 1070.90 174.642 2 5 -4 -10 1058.86 160.715 2 -5 -4 -9 11026.2 391.359 2 5 -4 -9 11724.6 380.117 2 -5 -4 -8 6106.12 271.199 2 5 4 -3 9606.20 636.280 1 5 4 -2 296123. 3576.10 1 5 4 -1 73697.9 1939.42 1 5 4 0 10670.1 771.859 1 5 4 1 86585.5 2199.32 1 5 4 2 266059. 4008.17 1 5 4 3 3786.24 545.390 1 5 4 4 41557.6 1819.48 1 5 4 5 44671.6 2043.56 1 5 4 6 24597.2 1640.84 1 5 4 7 45652.9 2384.90 1 5 4 8 8931.64 1125.79 1 5 4 9 11503.6 1341.80 1 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58730.8 1629.57 1 7 2 -1 341115. 3896.09 1 7 2 0 374365. 4246.53 1 7 2 1 338384. 4093.43 1 7 -2 2 62323.8 1204.33 1 7 2 2 63643.0 1820.01 1 7 -2 3 117164. 1661.21 1 7 2 3 113790. 2547.19 1 7 2 4 230801. 3887.68 1 7 -2 4 234780. 2578.25 1 7 -2 5 17492.4 786.050 1 7 2 5 15365.7 1086.92 1 7 2 6 7937.79 861.608 1 7 2 7 13155.4 1169.21 1 7 2 8 28321.7 1842.41 1 7 2 9 20854.8 1660.14 1 7 -2 12 15725.1 469.371 3 7 -2 13 5271.71 265.159 3 7 2 13 5597.28 304.920 3 7 2 14 1433.11 160.897 3 7 -2 14 1810.15 145.527 3 7 2 15 45.3922 70.7170 3 -7 -2 15 3.75114 46.1533 3 -7 -3 -14 2750.65 183.198 2 -7 -3 -13 6231.37 298.626 2 7 -3 -13 6274.58 267.032 2 -7 -3 -12 2393.87 232.254 2 7 -3 -12 1897.74 183.722 2 7 -3 -11 9755.26 367.096 2 -7 -3 -11 9130.84 393.481 2 -7 -3 -10 4227.89 273.804 2 7 -3 -10 4576.70 254.415 2 7 -3 -9 26204.2 548.632 2 -7 3 -9 25672.9 554.918 2 -7 -3 -9 26589.9 592.773 2 -7 -3 -8 7130.69 293.591 2 7 3 -3 62434.5 1758.23 1 7 3 -2 195396. 3062.86 1 7 3 -1 99001.5 2260.74 1 7 3 0 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456.605 1 10 7 1 64879.9 2766.89 1 10 7 2 42783.5 2343.35 1 10 7 3 3696.66 735.010 1 10 7 4 29950.6 2100.02 1 10 7 5 7869.93 1159.47 1 10 7 6 1260.32 556.391 1 10 7 7 7.46953 83.8925 3 10 7 7 66.0218 343.918 1 10 7 8 5013.13 1020.50 1 10 7 8 4962.59 270.737 3 10 7 9 3648.45 247.699 3 10 7 10 18922.8 512.057 3 10 7 11 431.628 140.342 3 10 7 12 4680.44 243.298 3 10 7 13 513.381 101.079 3 10 7 14 661.416 71.2359 3 -10 7 14 559.020 67.5088 3 10 -8 -13 1964.54 137.456 2 -10 -8 -13 2074.93 146.334 2 10 -8 -12 421.209 118.591 2 -10 -8 -12 464.971 127.530 2 -10 -8 -11 2316.04 209.545 2 10 -8 -11 2698.78 213.167 2 -10 -8 -10 1468.91 189.242 2 10 -8 -10 1614.79 191.708 2 -10 -8 -9 946.429 160.407 2 -10 -8 -8 4816.88 273.103 2 -10 8 -7 7818.30 334.687 4 -10 -8 -7 8174.35 330.236 2 -10 8 -6 2615.06 200.402 4 -10 -8 -6 2785.84 189.429 2 -10 8 -5 19437.0 486.309 4 10 8 -3 40280.3 1962.85 1 10 8 -2 13066.2 1204.85 1 10 8 -1 17687.1 1482.91 1 10 8 0-192.032 354.184 1 10 8 1 17183.5 1511.42 1 10 8 2 15176.1 1474.18 1 10 8 3 44145.5 2589.56 1 10 8 4 8620.00 1221.65 1 10 8 5 21399.5 1969.92 1 10 8 6 2488.56 747.068 1 10 8 7 4962.38 256.740 3 10 8 7 4698.08 1019.30 1 10 8 8 4363.86 250.450 3 10 8 8 3922.68 960.720 1 10 8 9 2229.22 193.588 3 10 8 10 1436.21 161.663 3 10 8 11 2771.26 202.891 3 10 8 12 632.927 113.603 3 10 8 13 2305.40 134.598 3 10 -9 -13 179.946 65.4599 2 -10 -9 -13 322.270 74.0107 2 -10 -9 -12 5086.93 230.763 2 10 -9 -12 5400.57 240.059 2 -10 -9 -11 3031.90 212.176 2 10 -9 -11 3043.76 215.326 2 -10 -9 -10 86.0063 122.649 2 10 -9 -10 333.764 144.591 2 -10 -9 -9 851.206 151.146 2 -10 9 -8 3560.68 239.134 4 -10 -9 -8 3885.73 246.949 2 -10 -9 -7 151.172 99.5520 2 -10 9 -7 106.009 114.670 4 -10 9 -6 9496.81 376.587 4 -10 -9 -6 9223.80 329.256 2 10 9 -5 4911.17 239.911 4 -10 9 -5 4910.95 272.004 4 10 9 -4 5686.22 254.410 4 -10 9 -4 6056.10 289.746 4 -10 9 -3 7415.03 302.864 4 10 9 -2 21817.8 1596.23 1 10 9 -1 589.427 311.160 1 10 9 0 18171.6 1622.62 1 10 9 1 999.953 466.314 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96.0548 86.3516 4 10 10 0 146.313 84.7345 4 10 10 1 14304.9 412.780 4 -10 10 1 13960.6 399.745 4 10 10 1 15586.6 1617.96 1 10 10 2 17075.1 444.327 4 10 10 2 17859.8 1770.36 1 -10 10 2 19538.6 456.021 4 10 10 3 16887.3 442.850 4 10 10 3 18931.2 1903.08 1 -10 10 3 18605.6 1670.10 1 10 10 4 156.561 470.847 1 -10 10 4 929.757 408.137 1 -10 10 5 15801.2 1711.90 1 10 10 5 14749.3 1769.30 1 -10 10 6 804.350 504.215 1 10 10 6 1511.62 662.100 1 10 -11 -12 732.262 90.3797 2 -10 -11 -12 700.066 70.0711 2 10 -11 -11 1101.92 130.925 2 -10 -11 -11 1028.81 110.846 2 -10 -11 -10 3950.32 214.802 2 10 -11 -10 4437.92 248.664 2 -10 -11 -9 669.429 123.857 2 -10 11 -8 2727.14 219.808 4 -10 -11 -8 2723.46 200.017 2 -10 11 -7 1841.00 200.080 4 -10 -11 -7 1942.70 171.207 2 10 11 -6 2381.94 182.763 4 -10 11 -6 2169.41 222.824 4 10 11 -5 2552.07 200.632 4 -10 11 -5 3120.00 244.958 4 10 11 -4 948.572 142.618 4 -10 11 -4 868.356 163.558 4 10 11 -3 16243.8 465.893 4 -10 11 -3 16415.4 494.319 4 -10 11 -2 1631.93 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331.398 3 11 1 10 7256.14 349.077 3 11 1 11 1938.31 219.015 3 11 -1 11 1828.32 200.009 3 11 -1 12 2636.88 217.966 3 11 1 12 2370.43 228.131 3 11 -1 13 142.185 112.848 3 11 1 13 135.696 121.243 3 11 -1 14 188.002 90.0804 3 11 1 14 78.8046 94.7332 3 11 1 15 111.507 57.0640 3 -11 -2 -13 4694.69 260.650 2 -11 -2 -12 3190.14 252.313 2 -11 -2 -11 8987.81 386.339 2 -11 -2 -10 12982.3 455.828 2 -11 2 -10 13880.4 446.866 2 -11 2 -9 27223.4 598.940 2 -11 -2 -9 26904.2 614.887 2 -11 2 -8 16211.5 441.195 2 -11 -2 -8 15996.3 450.692 2 11 2 -2 77943.8 2323.26 1 11 2 -1 62308.2 2068.11 1 11 2 0 38224.2 1632.00 1 11 -2 1 48593.4 1526.08 1 11 2 1 49831.0 1867.95 1 11 -2 2 81096.5 1915.80 1 11 2 2 74683.1 2328.07 1 11 -2 3 45428.8 1393.41 1 11 2 3 37637.6 1739.35 1 11 -2 4 19164.5 905.737 1 11 2 4 18905.5 1282.23 1 11 2 5 18437.5 1337.71 1 11 2 6 23594.8 1595.31 1 11 2 7 89619.2 3259.95 1 11 -2 8 14266.3 415.254 3 11 2 8 15073.4 1432.25 1 11 -2 9 21492.9 528.709 3 11 -2 10 15220.6 461.166 3 11 2 10 15741.4 504.328 3 11 -2 11 8290.39 349.198 3 11 2 11 8249.97 376.205 3 11 -2 12 2863.03 214.724 3 11 2 12 2938.65 247.298 3 11 -2 13 5081.29 245.071 3 11 2 13 5291.16 278.732 3 11 -2 14 934.883 105.093 3 11 2 14 1037.85 133.836 3 11 2 15 560.815 76.8962 3 -11 -3 -13 3009.33 223.328 2 -11 -3 -12 3113.91 246.976 2 -11 -3 -11 1338.11 192.936 2 -11 -3 -10 2757.46 236.351 2 11 -3 -10 2809.56 202.148 2 -11 -3 -9 22032.5 562.077 2 -11 -3 -8 2958.89 211.358 2 11 3 -3 7088.31 747.075 1 11 3 -2 189191. 3758.59 1 11 3 -1 3687.90 584.150 1 11 3 0 69357.0 2281.72 1 11 3 1 5045.00 659.658 1 11 3 2 210857. 4173.38 1 11 3 3 8936.15 925.134 1 11 3 4 11292.2 1054.00 1 11 3 5 17708.6 1367.78 1 11 3 6 22593.4 1648.08 1 11 3 7 25314.8 1829.13 1 11 -3 8 5059.79 244.768 3 11 3 8 6375.48 987.980 1 11 -3 9 22320.0 525.644 3 11 3 9 24231.0 594.917 3 11 3 9 23314.2 1944.90 1 11 -3 10 5239.34 273.690 3 11 3 10 5412.28 307.997 3 11 -3 11 1618.19 170.154 3 11 3 11 1347.10 195.845 3 11 -3 12 3860.22 227.214 3 11 3 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457.531 1 11 8 -2 3461.58 660.823 1 11 8 -1 14323.7 1386.06 1 11 8 0 11380.5 1245.32 1 11 8 1 14170.6 1419.09 1 11 8 2 3298.43 772.625 1 11 8 3-38.1536 455.664 1 11 8 4 2214.60 704.362 1 11 8 5 3638.64 878.922 1 11 8 6 14353.7 1691.19 1 11 8 7 3275.87 211.995 3 11 8 7 4049.91 946.365 1 11 8 8 7486.40 317.363 3 11 8 9 5453.20 276.295 3 11 8 10 2946.25 213.816 3 11 8 11 2792.89 200.885 3 11 8 12 1262.47 134.026 3 11 8 13 434.482 72.5499 3 11 -9 -13 723.004 81.8238 2 -11 -9 -13 770.173 84.3118 2 11 -9 -12 1506.72 143.794 2 -11 -9 -12 1461.05 135.095 2 11 -9 -11 1625.43 174.099 2 -11 -9 -11 1810.26 175.413 2 -11 -9 -10 14198.6 435.245 2 11 -9 -10 13823.8 433.360 2 -11 -9 -9 1827.44 192.987 2 -11 -9 -8 5582.94 285.082 2 -11 9 -8 5580.91 301.560 4 -11 9 -7 8488.37 370.566 4 -11 -9 -7 8387.39 333.227 2 -11 9 -6 7990.30 351.248 4 -11 -9 -6 7707.25 304.525 2 -11 9 -5 5060.79 277.987 4 11 9 -5 4141.73 220.919 4 11 9 -4 9242.61 324.286 4 -11 9 -4 8676.41 345.508 4 -11 9 -3 1068.32 139.368 4 11 9 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4 81014.3 3206.39 1 12 5 5 9342.56 1156.94 1 12 5 6 5084.28 927.285 1 12 5 7 7238.37 308.283 3 12 5 7 7504.38 1124.34 1 12 5 8 5498.95 1041.74 1 12 5 8 4730.02 270.446 3 12 5 9 3994.02 261.608 3 12 5 9 3215.40 852.987 1 12 5 10 1297.78 188.023 3 12 5 11 1680.81 201.977 3 12 5 12 15720.9 455.415 3 12 5 13 405.122 123.463 3 12 5 14 1484.58 118.837 3 -12 -6 -13 2809.93 184.382 2 12 -6 -13 2098.99 141.689 2 12 -6 -12 1206.70 151.751 2 -12 -6 -12 1055.05 159.001 2 12 -6 -11 1982.99 188.983 2 -12 -6 -11 2251.00 220.546 2 -12 -6 -10 7689.97 359.413 2 12 -6 -10 7836.91 337.135 2 -12 -6 -9 2207.79 212.494 2 -12 -6 -8 2595.83 208.801 2 -12 6 -7 16873.6 473.094 4 -12 -6 -7 18742.2 475.637 2 12 6 -3 27006.2 1651.31 1 12 6 -2 22938.3 1555.59 1 12 6 -1 14587.9 1289.24 1 12 6 0 339.190 327.232 1 12 6 1 14193.5 1297.23 1 12 6 2 25943.9 1791.06 1 12 6 3 23275.6 1761.05 1 12 6 4 68795.5 3127.20 1 12 6 5 73009.9 3341.71 1 12 6 6 14750.1 1602.52 1 12 6 7 17175.7 461.973 3 12 6 7 15227.0 1683.10 1 12 6 8 4504.34 259.256 3 12 6 8 5185.55 1069.31 1 12 6 9 782.711 153.930 3 12 6 10 8383.38 363.293 3 12 6 11 1220.89 181.285 3 12 6 12 987.677 152.986 3 12 6 13 2854.26 182.064 3 12 6 14 358.416 68.9204 3 -12 -7 -13 5384.02 222.109 2 12 -7 -13 4947.54 196.040 2 -12 -7 -12 8191.56 314.481 2 12 -7 -12 7389.91 287.234 2 12 -7 -11 661.368 144.762 2 -12 -7 -11 595.611 161.643 2 -12 -7 -10 11710.7 423.504 2 -12 -7 -9 1820.06 199.827 2 -12 -7 -8 8728.61 355.891 2 -12 7 -8 8069.94 346.877 4 -12 7 -7 6961.85 323.238 4 -12 -7 -7 7130.54 307.434 2 -12 7 -6 19366.7 514.477 4 -12 -7 -6 19928.8 468.637 2 12 7 -3 19177.6 1441.00 1 12 7 -2 11863.5 1192.86 1 12 7 -1 4217.28 780.866 1 12 7 0 2274.64 611.799 1 12 7 1 2538.47 617.440 1 12 7 2 17337.9 1556.35 1 12 7 3 18068.9 1644.58 1 12 7 4 35664.4 2374.49 1 12 7 5 28209.9 2222.32 1 12 7 6 20879.6 485.110 3 12 7 6 22334.9 2062.18 1 12 7 7 6867.85 300.962 3 12 7 7 7481.70 1277.62 1 12 7 8 4632.70 264.673 3 12 7 8 5004.63 1099.64 1 12 7 9 418.707 137.995 3 12 7 10 9566.02 371.521 3 12 7 11 1176.63 169.287 3 12 7 12 5605.25 255.584 3 12 7 13 5699.74 215.963 3 12 -8 -13 233.405 63.7203 2 -12 -8 -13 392.945 83.7121 2 -12 -8 -12 2508.89 180.535 2 12 -8 -12 2324.80 169.961 2 12 -8 -11 1706.20 176.673 2 -12 -8 -11 1561.64 174.556 2 -12 -8 -10 2850.33 227.106 2 -12 -8 -9 593.644 148.737 2 -12 8 -8 6565.22 323.714 4 -12 -8 -8 6813.46 317.224 2 -12 8 -7 7134.19 339.979 4 -12 -8 -7 7166.84 310.706 2 -12 -8 -6 216.554 91.6802 2 -12 8 -6 252.232 110.163 4 -12 8 -5 21953.2 543.673 4 -12 8 -4 2514.73 188.603 4 12 8 -3 16526.4 1378.82 1 12 8 -2 9864.90 1121.73 1 12 8 -1 4862.71 865.118 1 12 8 0 34767.2 2183.37 1 12 8 1 8495.52 1124.49 1 12 8 2 6048.50 996.731 1 12 8 3 19711.7 1820.40 1 12 8 4 1265.27 506.454 1 12 8 5 17467.6 1852.76 1 12 8 6 537.078 426.465 1 12 8 7 11085.0 375.091 3 12 8 7 12943.6 1697.71 1 12 8 8 9888.01 364.124 3 12 8 9 633.317 129.589 3 12 8 10 2744.83 207.501 3 12 8 11 1999.78 174.073 3 12 8 12 1996.24 148.712 3 12 8 13 666.847 78.4057 3 -12 -9 -13 384.187 64.5124 2 12 -9 -12 168.145 87.9663 2 -12 -9 -12 65.3720 76.9804 2 12 -9 -11 970.722 144.825 2 -12 -9 -11 910.218 141.523 2 -12 -9 -10 406.075 127.009 2 12 -9 -10 716.544 154.851 2 -12 -9 -9 2429.47 209.919 2 -12 -9 -8-11.8800 105.790 2 -12 9 -8 70.0010 110.489 4 -12 -9 -7 645.602 129.587 2 -12 9 -7 829.904 159.200 4 -12 9 -6 33676.8 720.568 4 -12 9 -5 4096.02 261.020 4 12 9 -5 4594.73 232.269 4 12 9 -4 1091.68 132.459 4 -12 9 -4 1314.38 155.409 4 12 9 -3 8768.70 316.728 4 -12 9 -3 8329.41 332.987 4 12 9 -2 17700.4 445.172 4 -12 9 -2 17229.1 456.666 4 12 9 -2 15991.5 1454.80 1 12 9 -1 1724.71 559.484 1 12 9 0 3096.67 712.798 1 12 9 1 3813.70 785.463 1 12 9 2 18417.8 1753.93 1 12 9 2 16854.9 431.421 4 12 9 3 9442.31 1306.81 1 12 9 4 2166.60 735.809 1 12 9 5 3498.37 917.870 1 12 9 6 32173.0 2667.61 1 12 9 9 4216.27 233.683 3 12 9 10 549.191 117.868 3 12 9 11 490.523 94.4084 3 12 9 12 459.772 74.1771 3 12 -10 -12 76.7155 68.3036 2 -12 -10 -12 156.177 62.8700 2 -12 -10 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89.9847 2 12 -11 -11 652.161 108.894 2 -12 -11 -11 607.542 84.3894 2 -12 -11 -10 1947.52 145.788 2 12 -11 -10 2132.78 183.207 2 -12 -11 -9 1905.27 165.619 2 -12 -11 -8 595.683 117.926 2 -12 11 -8 403.588 128.348 4 -12 11 -7 3568.36 263.782 4 -12 11 -6 9408.24 407.752 4 12 11 -5 4657.02 257.997 4 -12 11 -5 5324.15 320.986 4 12 11 -4 15262.4 449.737 4 -12 11 -4 15804.0 510.871 4 12 11 -3 5814.34 291.907 4 -12 11 -3 5905.07 319.060 4 12 11 -2 11254.7 396.436 4 -12 11 -2 10938.2 411.236 4 12 11 -1 2447.35 200.792 4 -12 11 -1 2784.83 220.725 4 12 11 0 506.110 353.185 1 12 11 0 664.765 135.132 4 -12 11 0 818.515 142.025 4 -12 11 1 2168.90 185.673 4 12 11 1 2315.14 202.117 4 12 11 2 10366.2 371.944 4 -12 11 2 9662.43 344.508 4 12 11 3 6503.38 1205.21 1 12 11 4 15480.4 1838.98 1 12 -12 -11 1028.10 103.436 2 12 -12 -10 1242.20 138.355 2 -12 12 -8 886.051 146.963 4 -12 12 -7 160.472 127.269 4 12 12 -6 3087.83 201.033 4 -12 12 -6 2364.50 232.496 4 -12 12 -5 2198.24 231.688 4 12 12 -5 2398.73 198.305 4 12 12 -4 4642.39 267.438 4 -12 12 -4 4671.16 306.254 4 12 12 -3 4973.24 282.616 4 -12 12 -3 4886.37 306.035 4 12 12 -2 3831.20 252.242 4 -12 12 -2 3755.99 261.451 4 -12 12 -1 9875.35 396.785 4 12 12 -1 9747.02 383.478 4 -12 12 0 642.647 145.164 4 12 12 0 879.913 163.215 4 12 12 1 8640.91 360.324 4 -12 12 1 9340.73 358.503 4 -12 12 2 3789.84 228.757 4 12 12 2 4347.12 265.185 4 12 -13 -10 112.386 72.2095 2 12 -13 -9 1576.77 151.612 2 -12 13 -8 1360.58 149.541 4 -12 13 -7 1404.82 179.179 4 -12 13 -6 3674.52 267.490 4 12 13 -5 1545.13 167.156 4 -12 13 -5 1268.72 202.569 4 12 13 -4 275.562 132.614 4 -12 13 -4-27.7420 163.034 4 12 13 -3 765.943 154.443 4 -12 13 -3 612.441 167.100 4 12 13 -2 10347.7 403.533 4 -12 13 -2 10390.9 420.802 4 12 13 -1 2476.30 227.081 4 -12 13 -1 2564.42 229.326 4 12 13 0 1152.46 179.876 4 -12 13 0 1239.27 173.805 4 -12 13 1 2912.34 218.646 4 12 13 1 2590.03 231.824 4 -12 13 2 8455.87 329.639 4 12 -14 -9 1948.65 132.770 2 -12 14 -8 595.016 92.8182 4 -12 14 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424.880 4 -13 12 -2 12167.7 451.993 4 -13 12 -1 4399.72 279.530 4 13 12 -1 4607.46 280.357 4 13 12 0 32304.3 677.782 4 -13 12 0 32031.7 671.735 4 -13 12 1 4816.60 270.284 4 13 12 1 5195.85 290.930 4 -13 12 2 7667.87 316.602 4 13 -13 -10 215.196 77.0998 2 13 -13 -9 1917.07 156.841 2 -13 13 -8 916.969 126.840 4 -13 13 -7 641.852 148.301 4 -13 13 -6 758.541 171.952 4 13 13 -5 2864.53 206.057 4 -13 13 -5 2767.40 249.471 4 13 13 -4 3269.66 234.773 4 -13 13 -4 2945.35 259.276 4 -13 13 -3 2671.40 241.388 4 13 13 -3 2860.89 237.271 4 13 13 -2 535.741 153.205 4 -13 13 -2 529.179 165.074 4 13 13 -1 386.275 156.260 4 -13 13 -1 168.136 130.292 4 13 13 0 75.8931 138.312 4 -13 13 0 99.0720 117.604 4 -13 13 1 1106.48 160.831 4 -13 13 2 262.948 106.552 4 13 -14 -9 571.506 87.5756 2 -13 14 -8 575.699 88.5167 4 -13 14 -7 744.755 131.239 4 -13 14 -6 853.048 166.173 4 -13 14 -5 1347.12 196.857 4 -13 14 -4 528.680 165.922 4 13 14 -3 222.017 148.522 4 -13 14 -3 280.227 174.994 4 13 14 -2 2365.82 222.604 4 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4988.94 258.259 3 19 6 5 3097.42 852.456 1 19 6 6 18715.7 493.595 3 19 6 6 17630.4 1896.34 1 19 6 7 2665.43 213.819 3 19 6 7 2216.54 739.009 1 19 6 8 2668.62 220.437 3 19 6 9 1127.54 171.317 3 19 6 10 142.072 124.019 3 19 6 11 4429.41 239.158 3 19 6 12 283.235 96.7975 3 19 6 13 501.042 76.8802 3 -19 -7 -10 6954.88 281.351 2 19 -7 -10 6238.83 268.031 2 -19 7 -9 709.666 125.697 4 -19 -7 -9 846.616 138.021 2 -19 7 -8 5385.05 289.521 4 -19 -7 -8 5122.56 261.776 2 -19 7 -7 4926.88 296.411 4 19 7 -3 5111.13 974.921 1 19 7 -2-148.653 407.956 1 19 7 -1 833.870 595.531 1 19 7 0 10464.5 1367.19 1 19 7 1 801.537 472.152 1 19 7 2 819.208 597.386 1 19 7 3 6537.69 1145.89 1 19 7 4 2122.85 169.832 3 19 7 4 2062.07 719.276 1 19 7 5 909.845 137.002 3 19 7 5 455.358 458.294 1 19 7 6 19472.9 499.300 3 19 7 6 17830.0 1929.37 1 19 7 7 4894.73 267.623 3 19 7 8 4658.78 265.245 3 19 7 9 747.826 146.570 3 19 7 10 6698.63 290.648 3 19 7 11 1047.60 132.055 3 19 7 12 894.022 99.0306 3 19 -8 -11 3211.97 170.376 2 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564.477 1 20 -1 2 30853.3 1800.83 1 20 1 2 28484.9 1839.82 1 20 -1 3 68455.3 2661.43 1 20 1 3 70833.2 2901.14 1 20 -1 4 10839.3 1041.88 1 20 1 4 9139.00 1088.00 1 20 -1 5 17191.7 438.332 3 20 1 5 17530.0 450.548 3 20 1 5 16895.5 1460.72 1 20 -1 6 4337.62 242.955 3 20 1 6 4384.17 249.983 3 20 -1 7 5316.95 277.703 3 20 1 7 5354.82 285.860 3 20 -1 8 1395.87 178.307 3 20 1 8 1155.58 173.049 3 20 -1 9 7584.46 339.294 3 20 1 9 8202.37 360.979 3 20 -1 10 173.365 121.562 3 20 1 10 383.169 152.256 3 20 -1 11 4761.70 255.989 3 20 1 11 4592.90 269.993 3 20 -1 12 6655.81 267.054 3 20 1 12 6512.11 280.198 3 20 -1 13 482.123 86.6742 3 20 1 13 550.296 100.408 3 -20 -2 -8 2106.97 194.480 2 -20 -2 -7 478.493 120.813 2 -20 -2 -6 7461.96 295.386 2 20 2 -5 4575.35 242.094 3 20 2 -1 2621.54 691.770 1 20 2 0 21778.1 1669.41 1 20 2 1 1495.29 533.719 1 20 2 2 33030.3 2060.95 1 20 -2 3 9823.55 961.453 1 20 2 3 11302.6 1217.48 1 20 2 4 24951.7 1831.70 1 20 2 5 4943.37 876.165 1 20 -2 5 4252.70 221.153 3 20 2 5 4056.57 229.354 3 20 2 6 7513.58 1058.17 1 20 -2 6 6980.14 291.595 3 20 2 6 6526.20 301.911 3 20 -2 7 606.457 124.948 3 20 2 7 551.974 136.019 3 20 -2 8 2036.16 189.958 3 20 2 8 1965.41 201.061 3 20 -2 9 5651.75 294.246 3 20 2 9 5745.81 316.914 3 20 -2 10 2256.52 198.116 3 20 2 10 1895.75 212.433 3 20 -2 11 91.1591 106.110 3 20 2 11 133.463 132.646 3 20 -2 12 3803.96 198.433 3 20 2 12 3644.00 223.346 3 20 -2 13 732.864 82.0508 3 20 2 13 869.757 111.712 3 20 2 14 2028.26 103.109 3 -20 -3 -9 682.310 154.788 2 -20 -3 -8 7253.39 323.241 2 -20 -3 -7 2564.92 198.481 2 -20 -3 -6 3283.54 203.983 2 20 3 -5 607.988 107.951 3 20 3 -2 615.002 405.163 1 20 3 -1 22846.2 1809.04 1 20 3 0 2918.28 695.409 1 20 3 1 23282.4 1778.47 1 20 3 2 855.027 356.312 1 20 3 3 202.602 284.098 1 20 3 4-207.516 383.239 1 20 -3 5 1093.89 126.533 3 20 3 5 939.137 132.679 3 20 -3 6 3239.04 205.630 3 20 3 6 3440.09 228.883 3 20 3 6 3788.38 789.421 1 20 -3 7 3119.24 210.338 3 20 3 7 3626.40 244.745 3 20 -3 8 7939.07 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2267.45 749.962 1 20 6 2 11788.2 1437.27 1 20 6 3 18189.0 1819.27 1 20 6 3 16861.9 439.192 3 20 6 4 4544.53 242.439 3 20 6 4 3231.85 790.118 1 20 6 5 12822.8 403.241 3 20 6 5 13010.4 1593.58 1 20 6 6 14045.0 432.411 3 20 6 6 13842.1 1683.08 1 20 6 7 7126.73 318.401 3 20 6 8 3355.02 237.540 3 20 6 9 232.409 130.367 3 20 6 10 2670.16 205.583 3 20 6 11 4153.29 224.891 3 20 6 12 2921.17 168.726 3 20 6 13 82.4000 47.9644 3 20 -7 -10 439.931 103.456 2 -20 -7 -10 300.816 99.5802 2 -20 7 -9 5470.42 266.063 4 -20 -7 -9 5518.80 259.560 2 -20 7 -8 18657.1 512.409 4 -20 -7 -8 18942.2 465.503 2 -20 7 -7 2687.20 228.532 4 20 7 -3 12295.6 1507.41 1 20 7 -2 945.199 544.005 1 20 7 -1 10989.0 1433.58 1 20 7 0 25565.1 2146.65 1 20 7 1 13785.2 1603.00 1 20 7 2 1171.07 525.242 1 20 7 3 13394.5 1602.34 1 20 7 3 13865.3 401.345 3 20 7 4 13302.0 1663.41 1 20 7 4 13627.2 408.661 3 20 7 5 3950.78 233.754 3 20 7 5 3597.11 896.811 1 20 7 6 7772.51 326.742 3 20 7 6 7213.55 1257.55 1 20 7 7 7038.83 313.808 3 20 7 8 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1189.34 133.096 4 -20 15 -6 670.039 83.2261 4 -20 15 -5 2054.68 147.565 4 -20 15 -4 980.932 118.914 4 -20 15 -3 1529.56 154.516 4 -20 15 -2 679.613 129.230 4 -20 15 -1 682.210 122.332 4 -20 15 0-64.1995 86.1192 4 -20 16 -4 2682.77 140.673 4 -20 16 -3 712.754 91.6717 4 -20 16 -2 436.530 87.1304 4 -20 16 -1 633.063 88.3781 4 -20 16 0 410.753 67.7554 4 21 0 -5 150.052 94.9506 3 21 0 0-68.7626 302.115 1 21 0 1-39.5109 281.970 1 21 0 2 102.615 290.300 1 21 0 3-99.0274 335.510 1 21 0 4-333.019 357.573 1 21 0 5 3.50453 83.0766 3 21 0 6 106.379 105.217 3 21 0 7 70.8779 112.811 3 21 0 8-44.8708 115.172 3 21 0 9 69.3938 128.393 3 21 0 10 115.127 124.608 3 21 0 11 85.6843 126.253 3 21 0 12 28.9612 100.733 3 21 0 13 36.7928 69.8543 3 21 -1 -5 700.883 123.479 3 21 1 -5 549.728 109.598 3 21 1 -1 7484.56 1019.57 1 21 1 0-199.157 333.640 1 21 -1 1 9083.86 1056.99 1 21 1 1 9751.64 1136.73 1 21 -1 2 14161.4 1276.22 1 21 1 2 13710.4 1322.12 1 21 -1 3 13810.6 1232.48 1 21 1 3 13920.1 1351.83 1 21 -1 4 360.754 223.748 1 21 1 4 959.085 372.412 1 21 -1 5 1825.12 162.644 3 21 1 5 1848.65 167.946 3 21 -1 6 11278.2 380.792 3 21 1 6 11227.2 390.215 3 21 -1 7 2655.59 209.009 3 21 1 7 2700.66 222.517 3 21 -1 8 11833.0 414.174 3 21 1 8 11585.4 419.377 3 21 -1 9 4001.59 253.585 3 21 1 9 4198.21 271.958 3 21 -1 10 4308.35 259.242 3 21 1 10 4013.58 267.645 3 21 -1 11 9587.93 343.005 3 21 1 11 9987.28 367.697 3 21 -1 12 1122.01 130.704 3 21 1 12 1140.25 147.519 3 21 -1 13 925.095 92.6495 3 21 1 13 1145.71 114.035 3 21 2 -5 4975.10 258.927 3 21 -2 -4 10608.7 356.946 3 21 2 -1 15981.4 1513.48 1 21 2 0 61653.1 2910.12 1 21 2 1 17568.7 1558.89 1 21 2 2 15306.1 1443.95 1 21 2 3 7432.27 995.910 1 21 2 4 12653.4 387.070 3 21 2 4 11609.4 1278.67 1 21 -2 5 6271.47 276.441 3 21 2 5 6884.79 300.730 3 21 2 5 6004.55 972.228 1 21 -2 6 10228.6 356.570 3 21 2 6 10807.9 383.503 3 21 2 6 10351.7 1224.60 1 21 -2 7 3134.42 212.759 3 21 2 7 3291.93 237.905 3 21 -2 8 12722.4 412.619 3 21 2 8 12221.6 431.874 3 21 -2 9 257.748 129.238 3 21 2 9 391.604 152.351 3 21 -2 10 5671.35 278.776 3 21 2 10 6002.01 311.811 3 21 -2 11 171.404 99.6830 3 21 2 11 228.514 141.245 3 21 -2 12 6856.71 247.124 3 21 2 12 7705.97 290.523 3 21 2 13 1499.14 122.717 3 21 -2 13 1212.06 88.1524 3 -21 -3 -8 1587.50 175.904 2 -21 -3 -7 10116.0 363.386 2 -21 -3 -6 4197.71 227.301 2 21 3 -5 16574.5 449.239 3 21 -3 -4 1006.67 135.320 3 21 3 -4 810.831 122.772 3 21 3 -2 11344.9 1349.74 1 21 3 -1 30056.9 2138.38 1 21 3 0 4505.73 872.337 1 21 3 1 43168.1 2490.09 1 21 3 2 16569.5 1562.17 1 21 3 3 4060.80 835.654 1 21 3 4 1568.86 542.018 1 21 3 4 2154.12 178.803 3 21 -3 5 15455.3 418.329 3 21 3 5 16041.7 452.043 3 21 3 5 17442.1 1668.39 1 21 -3 6 2974.96 199.364 3 21 3 6 2489.78 673.598 1 21 3 6 2945.30 221.512 3 21 -3 7 5752.46 278.928 3 21 3 7 5621.39 297.677 3 21 -3 8 1018.18 146.081 3 21 3 8 828.306 160.703 3 21 -3 9 11083.6 375.079 3 21 3 9 11307.6 421.290 3 21 -3 10 696.834 127.074 3 21 3 10 825.559 168.227 3 21 -3 11 9105.26 299.756 3 21 3 11 9414.85 353.786 3 21 -3 12 232.976 71.1720 3 21 3 12 316.515 118.545 3 21 3 13 2001.17 135.789 3 -21 -4 -8 3737.60 236.729 2 -21 -4 -7 10314.9 362.145 2 -21 -4 -6 2125.57 167.597 2 21 4 -4 41011.4 690.190 3 21 4 -2 16134.2 1665.44 1 21 4 -1 13596.2 1487.74 1 21 4 0 71618.9 3302.48 1 21 4 1 13112.3 1439.52 1 21 4 2 20251.1 1785.77 1 21 4 3 7625.89 1147.83 1 21 4 3 7940.02 303.720 3 21 4 4 39240.9 685.121 3 21 4 4 42401.7 2642.50 1 21 4 5 2018.28 185.491 3 21 4 5 2275.61 676.106 1 21 -4 5 1766.09 149.633 3 21 4 6 3990.87 247.578 3 21 -4 6 3726.23 215.004 3 21 -4 7 9227.47 335.200 3 21 4 7 9516.64 376.554 3 21 4 7 8314.37 1269.54 1 21 -4 8 2166.39 180.006 3 21 4 8 1880.73 206.733 3 21 -4 9 1493.04 154.444 3 21 4 9 1362.26 189.357 3 21 4 10 1819.16 199.883 3 21 4 11 1040.70 160.612 3 21 4 12 4589.43 221.565 3 21 4 13 1159.70 105.083 3 -21 -5 -9 2380.92 197.610 2 -21 5 -9 2450.80 188.355 4 -21 -5 -8 1513.54 165.496 2 -21 -5 -7 2908.77 201.834 2 21 5 -4 2840.26 190.582 3 21 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25980.5 589.367 3 21 6 6 23491.9 2185.92 1 21 6 7 886.699 154.767 3 21 6 8 3975.16 256.777 3 21 6 9 2736.53 217.511 3 21 6 10 4426.53 249.594 3 21 6 11 241.032 104.577 3 21 6 12 701.440 100.037 3 -21 7 -9 3770.99 223.653 4 -21 -7 -9 3815.03 212.523 2 -21 7 -8 1101.74 160.676 4 -21 -7 -8 1231.13 137.131 2 -21 7 -7 497.559 144.941 4 21 7 -3 2877.52 790.297 1 21 7 -2 1534.54 663.853 1 21 7 -1 10187.6 1416.37 1 21 7 0 1745.50 605.121 1 21 7 1 11390.3 1498.90 1 21 7 2 1034.58 627.290 1 21 7 3 3406.21 834.289 1 21 7 3 3625.64 217.953 3 21 7 4 2028.15 743.661 1 21 7 4 1516.42 156.062 3 21 7 5 1534.05 666.745 1 21 7 5 2647.75 204.278 3 21 7 6 5913.02 286.149 3 21 7 7 694.167 142.882 3 21 7 8 1361.45 171.084 3 21 7 9 3736.20 234.295 3 21 7 10 1897.13 166.968 3 21 7 11 1294.01 126.315 3 21 7 12 305.729 68.0539 3 21 -8 -10 6182.66 244.326 2 -21 8 -9 783.241 120.630 4 -21 8 -8 12605.7 415.296 4 -21 8 -7 3355.18 250.374 4 -21 8 -6 1402.12 200.692 4 -21 8 -5 1189.20 183.805 4 21 8 -2 6983.11 1227.76 1 21 8 -1 1063.90 489.359 1 21 8 0 43875.2 2933.75 1 -21 8 0 41880.5 765.897 4 -21 8 1 74.7752 86.7284 4 21 8 1 290.923 531.041 1 21 8 2 8069.60 1315.54 1 21 8 3 738.391 439.255 1 21 8 4 1890.36 774.700 1 21 8 5 1601.81 161.652 3 21 8 6 1324.51 158.587 3 21 8 7 4068.15 235.722 3 21 8 8 11413.0 369.123 3 21 8 9 357.707 108.466 3 21 8 10 7098.42 256.699 3 21 8 11 197.236 70.6779 3 21 -9 -10 527.367 93.9725 2 -21 9 -9 3849.75 205.367 4 -21 9 -8 236.183 125.899 4 -21 9 -7 660.614 150.949 4 -21 9 -6 1161.99 196.961 4 -21 9 -5 335.803 153.258 4 -21 9 -4 1195.19 202.928 4 -21 9 -3 24720.4 659.192 4 -21 9 -2 4847.08 305.746 4 21 9 -2 3170.14 888.969 1 -21 9 -1 7087.15 349.007 4 21 9 -1 7316.56 1254.49 1 -21 9 0 6513.96 320.283 4 21 9 0 6758.01 1216.78 1 -21 9 1 9287.60 360.670 4 21 9 1 9245.13 1367.26 1 21 9 2 3740.81 920.298 1 21 9 7 292.906 99.4180 3 21 9 8 352.663 98.8613 3 21 9 9 4739.01 207.449 3 21 9 10 825.962 88.5549 3 21 -10 -10 6021.71 212.526 2 -21 10 -9 2108.53 147.311 4 -21 10 -8 6754.61 289.045 4 -21 10 -7 1590.64 183.600 4 -21 10 -6 1740.44 204.341 4 -21 10 -5 272.436 151.554 4 -21 10 -4 8684.26 409.865 4 -21 10 -3 1827.65 225.572 4 -21 10 -2 3491.17 275.179 4 -21 10 -1 3830.71 269.025 4 -21 10 0 5800.87 308.455 4 -21 10 1 4137.13 249.009 4 21 -11 -10 122.821 51.1922 2 -21 11 -9 2600.45 139.174 4 -21 11 -8 732.203 120.768 4 -21 11 -7 5719.07 284.800 4 -21 11 -6-53.0725 144.536 4 -21 11 -5 5344.43 319.601 4 -21 11 -4 104.039 151.171 4 -21 11 -3 1730.92 219.021 4 -21 11 -2 158.660 146.639 4 -21 11 -1 10123.9 421.637 4 -21 11 0 3121.57 240.060 4 -21 11 1 8136.92 347.476 4 21 -12 -9 67.0054 59.8991 2 -21 12 -8 458.744 90.4636 4 -21 12 -7 292.285 114.635 4 -21 12 -6 9777.31 368.560 4 -21 12 -5 560.644 161.110 4 -21 12 -4 6.33194 159.681 4 -21 12 -3 278.980 153.234 4 -21 12 -2 12140.8 459.771 4 -21 12 -1 296.152 150.388 4 -21 12 0 5495.61 300.223 4 -21 12 1 81.4757 100.905 4 -21 13 -8 671.624 74.7963 4 -21 13 -7 6791.68 249.160 4 -21 13 -6 1437.09 158.133 4 -21 13 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7 2219.20 202.089 3 22 0 8 1790.94 197.601 3 22 0 9 1394.81 190.954 3 22 0 10 2045.83 205.496 3 22 0 11 11718.1 376.174 3 22 0 12 3382.71 193.643 3 22 0 13 2193.25 127.688 3 22 -1 -5 16247.8 456.260 3 22 1 -5 15669.0 450.531 3 22 -1 -4 7373.01 310.310 3 22 1 -4 7862.55 320.674 3 22 1 0-94.3359 335.150 1 22 1 1 1603.11 579.720 1 22 -1 2 37838.6 2126.14 1 22 1 2 39744.0 2311.41 1 22 -1 3 42771.3 2228.88 1 22 1 3 41676.2 2356.38 1 22 1 4 8587.70 325.300 3 22 1 4 8049.32 1046.78 1 22 -1 4 8505.38 321.500 3 22 -1 5 14106.0 416.629 3 22 1 5 14155.0 423.829 3 22 1 5 14061.5 1393.58 1 22 -1 6 9101.87 349.286 3 22 1 6 8961.85 355.890 3 22 -1 7 12991.6 419.930 3 22 1 7 12088.2 421.785 3 22 -1 8 712.273 150.637 3 22 1 8 523.635 154.808 3 22 -1 9 7197.01 330.341 3 22 1 9 7032.04 337.206 3 22 -1 10 6207.60 295.392 3 22 1 10 6449.90 316.678 3 22 -1 11 4233.44 236.357 3 22 1 11 4233.11 254.470 3 22 -1 12 2977.94 178.211 3 22 1 12 2987.91 187.535 3 22 -1 13 551.122 72.9822 3 22 1 13 534.579 86.1079 3 22 2 -5 125.192 94.3599 3 22 -2 -4 843.289 133.796 3 22 2 -4 809.016 131.407 3 22 2 -1-77.9432 374.235 1 22 2 0 569.940 424.200 1 22 2 1 323.592 332.446 1 22 2 2 8129.40 1118.01 1 22 2 3 9914.25 1221.51 1 22 2 4 2085.95 173.997 3 22 2 4 2170.87 618.884 1 22 -2 4 2444.17 175.822 3 22 -2 5 99.3512 94.0624 3 22 2 5 137.157 106.441 3 22 2 5-258.215 354.362 1 22 -2 6 10547.3 370.470 3 22 2 6 10193.9 378.062 3 22 2 6 10542.4 1270.98 1 22 -2 7 780.179 136.117 3 22 2 7 927.154 160.680 3 22 -2 8 2476.40 205.932 3 22 2 8 2093.19 211.938 3 22 -2 9 57.4480 114.105 3 22 2 9 293.115 149.227 3 22 -2 10 1730.02 172.686 3 22 2 10 1832.92 197.447 3 22 -2 11 296.002 107.394 3 22 2 11 338.226 140.507 3 22 2 12 2807.86 186.123 3 22 -2 12 2381.69 148.982 3 22 2 13 462.701 81.7114 3 22 3 -5 3584.45 224.031 3 22 -3 -4 8679.38 336.926 3 22 3 -4 8520.87 331.314 3 22 -3 -3 14331.2 414.422 3 22 3 -3 14386.1 414.775 3 22 3 -2 2717.45 772.579 1 22 3 -1 28007.2 2095.20 1 22 3 0 3951.38 806.611 1 22 3 1 22588.9 1843.50 1 22 3 2 2758.25 710.982 1 22 3 3 12378.4 1403.53 1 22 3 3 13559.6 401.548 3 22 3 4 9510.28 344.728 3 22 -3 4 8985.05 322.263 3 22 3 5 3651.61 234.801 3 22 -3 5 3829.07 221.993 3 22 3 5 4261.71 861.908 1 22 3 6 570.716 433.391 1 22 -3 6 572.229 118.115 3 22 3 6 626.247 144.878 3 22 -3 7 4487.07 246.565 3 22 3 7 4481.85 273.818 3 22 -3 8 1042.46 145.704 3 22 3 8 844.937 172.413 3 22 -3 9 2852.21 211.210 3 22 3 9 2632.17 237.078 3 22 -3 10 1085.90 137.934 3 22 3 10 894.059 169.910 3 22 -3 11 176.080 86.1452 3 22 3 11-122.608 135.028 3 22 3 12 1077.05 133.980 3 22 3 13 463.315 84.1383 3 22 4 -4 13555.6 413.260 3 22 -4 -3 16619.9 443.655 3 22 4 -3 16618.5 448.616 3 22 4 -2 9125.76 1295.89 1 22 4 -1 14581.5 1556.87 1 22 4 0 2946.50 729.157 1 22 4 1 12997.4 1453.15 1 22 4 2 8584.00 1199.25 1 22 4 2 8204.14 313.888 3 22 4 3 19573.1 1815.50 1 22 4 3 18890.8 478.019 3 22 4 4 13891.7 417.047 3 22 4 4 14002.0 1573.46 1 22 -4 4 13313.7 383.194 3 22 4 5 6150.91 1032.43 1 22 4 5 5701.73 290.189 3 22 -4 5 5479.83 253.362 3 22 -4 6 1425.04 146.113 3 22 4 6 1924.67 195.521 3 22 -4 7 1611.29 161.797 3 22 4 7 1819.80 201.822 3 22 4 8 4542.93 278.803 3 22 -4 8 4381.65 238.414 3 22 -4 9 890.486 133.723 3 22 4 9 617.999 169.418 3 22 4 10 1983.63 203.028 3 22 4 11 231.787 124.801 3 22 4 12 2502.93 168.556 3 22 4 13 10.2619 55.4217 3 -22 5 -9 780.332 134.078 4 -22 -5 -7 60.2081 84.9187 2 22 5 -4 83.5504 88.2668 3 22 -5 -3 11092.1 366.777 3 22 5 -3 10572.1 362.397 3 22 5 -2 35012.6 2526.46 1 22 -5 -2 34210.7 618.991 3 22 5 -2 31339.9 613.521 3 22 5 -1 9013.03 1288.51 1 22 5 -1 8003.65 317.792 3 22 5 0 5119.24 934.938 1 22 5 1 6838.51 1109.28 1 22 5 1 7944.61 318.203 3 22 5 2 29671.5 2282.36 1 22 5 2 29086.8 591.631 3 22 5 3 12542.9 1524.47 1 22 5 3 12902.1 399.685 3 22 5 4 320.576 418.785 1 22 5 4 600.750 123.801 3 22 5 5 5779.64 287.193 3 22 5 5 5724.99 1119.30 1 22 5 6 4794.79 273.298 3 22 5 6 6325.29 1128.42 1 22 5 7 614.587 157.982 3 22 5 8 727.349 164.123 3 22 5 9 554.195 151.363 3 22 5 10 999.018 163.732 3 22 5 11 2942.44 201.650 3 22 5 12 1188.86 119.763 3 22 5 13 125.622 51.6291 3 -22 6 -9 6403.68 279.344 4 -22 6 -8 2484.44 208.326 4 22 6 -2 4869.00 1014.50 1 22 6 -2 5286.01 255.080 3 22 6 -1 5343.73 1029.08 1 22 6 -1 5116.10 259.303 3 22 6 0 58113.9 3246.13 1 22 6 0 49502.7 793.538 3 22 6 1 3830.40 230.076 3 22 6 1 3578.53 885.531 1 22 6 2 3474.05 219.507 3 22 6 2 3641.07 884.803 1 22 6 3 2854.67 203.938 3 22 6 3 2784.25 786.245 1 22 6 4 2872.73 822.849 1 22 6 4 4510.00 249.794 3 22 6 5 1406.36 643.096 1 22 6 5 501.903 129.783 3 22 6 6 4649.14 270.884 3 22 6 7 3406.87 238.479 3 22 6 8 2043.72 204.717 3 22 6 9 6472.80 308.845 3 22 6 10 188.893 111.987 3 22 6 11 3187.73 192.437 3 22 6 12 374.046 79.6427 3 -22 7 -9 3948.85 219.662 4 -22 7 -8 1039.73 157.907 4 -22 7 -7 531.923 153.118 4 22 7 -2 5805.65 1108.71 1 22 7 -1 8051.25 1319.80 1 22 7 0 12466.5 1566.35 1 22 7 1 10254.4 1450.77 1 22 7 2 8483.42 325.830 3 22 7 2 7446.39 1241.20 1 22 7 3 26740.1 2321.55 1 22 7 3 24410.4 547.450 3 22 7 4 7483.66 1248.34 1 22 7 4 6142.34 283.846 3 22 7 5 7080.93 1205.25 1 22 7 5 8716.40 346.632 3 22 7 6 4046.38 249.632 3 22 7 7 1402.64 173.871 3 22 7 8 727.742 144.966 3 22 7 9 4233.02 241.457 3 22 7 10 4387.01 225.103 3 22 7 11 229.755 86.7471 3 22 7 12 45.5139 44.8700 3 22 -8 -10 687.590 98.2221 2 -22 8 -9 969.810 127.082 4 -22 8 -8 2443.48 200.780 4 -22 8 -7 1634.74 192.903 4 -22 8 -6 4478.18 294.019 4 -22 8 -5 8309.97 389.745 4 22 8 -2 1518.91 716.866 1 22 8 -1 18910.8 1983.71 1 -22 8 0 1540.61 181.648 4 22 8 0 1861.77 710.330 1 22 8 1 19532.3 1998.36 1 -22 8 1 18196.8 495.048 4 22 8 2 2737.13 796.553 1 22 8 3 2657.77 842.606 1 22 8 4 2224.69 176.698 3 22 8 5 10834.9 370.400 3 22 8 6 2877.25 203.643 3 22 8 7 3202.00 218.074 3 22 8 8 1332.83 153.191 3 22 8 9 891.414 128.021 3 22 8 10 1214.96 122.276 3 22 8 11 285.194 64.8246 3 22 -9 -10 614.530 87.0913 2 -22 9 -9 132.719 76.2109 4 -22 9 -8 7425.19 310.674 4 -22 9 -7 6916.20 328.655 4 -22 9 -6 3688.83 269.366 4 -22 9 -5 16596.7 532.845 4 -22 9 -4 6383.20 358.766 4 -22 9 -3 4718.33 313.215 4 22 9 -2 1656.90 745.919 1 -22 9 -2 1302.44 198.576 4 -22 9 -1 6217.15 332.047 4 22 9 -1 6596.60 1268.72 1 -22 9 0 1601.56 179.882 4 22 9 0 792.861 622.812 1 -22 9 1 4974.24 273.221 4 22 9 1 5258.92 1089.83 1 22 9 7 5478.83 250.145 3 22 9 8 6887.03 260.126 3 22 9 9 366.473 82.5327 3 22 9 10 324.356 66.2898 3 22 -10 -10 626.980 78.7162 2 -22 10 -9 244.599 76.0297 4 -22 10 -8-121.135 105.590 4 -22 10 -7 1680.93 187.586 4 -22 10 -6 1103.43 183.049 4 -22 10 -5 4086.52 290.437 4 -22 10 -4 6873.50 364.070 4 -22 10 -3 170.803 154.800 4 -22 10 -2 804.120 174.347 4 -22 10 -1 1243.15 182.332 4 -22 10 0 34.9150 119.182 4 -22 10 1 1642.42 177.770 4 -22 11 -9 858.274 82.2532 4 -22 11 -8 1000.83 124.117 4 -22 11 -7 1268.23 155.516 4 -22 11 -6 3999.41 259.095 4 -22 11 -5 984.977 192.323 4 -22 11 -4 1699.85 214.163 4 -22 11 -3 289.512 157.313 4 -22 11 -2 476.410 170.498 4 -22 11 -1 715.546 165.528 4 -22 11 0 169.114 125.322 4 -22 11 1 432.152 127.422 4 22 -12 -9 178.136 55.9483 2 -22 12 -8 1635.77 124.307 4 -22 12 -7 174.810 102.763 4 -22 12 -6 2653.16 207.784 4 -22 12 -5 2456.40 218.061 4 -22 12 -4 3275.93 257.467 4 -22 12 -3 928.862 181.524 4 -22 12 -2 744.378 171.889 4 -22 12 -1 2182.15 219.321 4 -22 12 0 1980.52 198.850 4 -22 12 1 2426.64 196.285 4 -22 13 -8 935.955 75.5332 4 -22 13 -7 1587.94 128.602 4 -22 13 -6 182.264 98.8558 4 -22 13 -5 1866.09 185.634 4 -22 13 -4 1138.31 176.383 4 -22 13 -3 115.777 131.774 4 -22 13 -2 456.636 150.208 4 -22 13 -1 188.177 124.747 4 -22 13 0 3440.60 229.787 4 -22 13 1 697.633 120.536 4 -22 14 -7 4094.09 150.441 4 -22 14 -6 242.820 75.7543 4 -22 14 -5 4373.75 212.770 4 -22 14 -4 4978.88 244.253 4 -22 14 -3 641.058 130.674 4 -22 14 -2 1912.20 179.642 4 -22 14 -1 125.775 106.434 4 -22 14 0 149.176 97.0325 4 -22 14 1 136.993 83.3871 4 -22 15 -5 23.3595 55.7103 4 -22 15 -4 3974.91 183.557 4 -22 15 -3 449.867 100.568 4 -22 15 -2 2091.10 153.333 4 -22 15 -1 2131.82 152.768 4 -22 15 0-22.0196 65.1922 4 -22 16 -3 655.732 73.6061 4 -22 16 -2-95.1443 52.0005 4 23 0 -5-70.3075 92.3258 3 23 0 -4-197.249 110.030 3 23 0 -3 62.6536 105.759 3 23 0 1 59.3470 276.058 1 23 0 2 378.481 328.327 1 23 0 3 170.759 101.643 3 23 0 3-647.451 355.119 1 23 0 4-87.7348 99.0990 3 23 0 4-141.263 291.474 1 23 0 5 96.0541 99.8234 3 23 0 6 24.3572 109.781 3 23 0 7 99.6388 127.224 3 23 0 8 67.8950 122.676 3 23 0 9-75.5909 132.131 3 23 0 10-86.5101 133.585 3 23 0 11 7.80088 114.143 3 23 0 12 58.9195 85.5710 3 23 0 13 115.436 56.5086 3 23 1 -5 4553.02 260.267 3 23 -1 -4 4657.92 256.950 3 23 1 -4 4320.90 249.722 3 23 -1 -3 1726.55 163.576 3 23 1 -3 1598.06 165.821 3 23 1 0 14436.0 1481.75 1 23 1 1 14404.6 1460.27 1 23 -1 2 4376.86 776.623 1 23 1 2 5167.19 898.562 1 23 -1 3 1050.86 132.422 3 23 1 3 1536.25 154.782 3 23 -1 3 1342.42 447.308 1 23 1 3 1323.91 564.518 1 23 1 4 3386.23 222.170 3 23 1 4 3289.04 729.636 1 23 -1 4 3246.98 208.539 3 23 -1 5 3886.47 235.872 3 23 1 5 4088.71 243.883 3 23 -1 6 5027.80 274.019 3 23 1 6 4498.57 264.061 3 23 -1 7 1212.77 159.949 3 23 1 7 1294.03 178.520 3 23 -1 8 6147.93 306.760 3 23 1 8 6196.95 320.839 3 23 -1 9 8016.09 344.623 3 23 1 9 8435.47 359.917 3 23 -1 10 1046.93 154.750 3 23 1 10 1285.68 179.879 3 23 -1 11 1346.67 146.792 3 23 1 11 1574.36 169.456 3 23 1 12 2285.16 166.757 3 23 -1 12 2186.74 149.830 3 23 -1 13 1705.21 96.0792 3 23 1 13 1974.00 117.779 3 23 2 -5 8441.17 341.582 3 23 -2 -4 1604.26 170.857 3 23 2 -4 1545.98 161.317 3 23 -2 -3 20733.2 507.194 3 23 2 -3 20366.0 509.680 3 23 2 -1 6179.28 1046.34 1 23 2 0 49.7661 347.222 1 23 2 1 7437.40 1060.93 1 23 2 2 12028.3 1383.03 1 23 2 2 10035.9 347.740 3 23 2 3 20273.6 1760.28 1 23 -2 3 18266.4 457.456 3 23 2 3 18883.1 478.223 3 23 -2 4 1433.53 150.018 3 23 2 4 1572.61 164.768 3 23 2 5 7800.22 333.120 3 23 2 5 7532.05 1092.22 1 23 -2 5 7864.88 315.501 3 23 -2 6 8212.44 332.363 3 23 2 6 7818.30 339.035 3 23 -2 7 1644.63 171.134 3 23 2 7 1383.87 181.726 3 23 -2 8 3595.72 235.345 3 23 2 8 3653.43 261.358 3 23 -2 9 6312.39 293.115 3 23 2 9 6503.23 327.479 3 23 -2 10 923.825 138.162 3 23 2 10 811.181 167.103 3 23 2 11 7448.07 306.122 3 23 -2 11 6765.26 262.362 3 23 2 12 4010.60 203.875 3 23 -2 12 3655.26 166.889 3 23 2 13 3215.75 146.037 3 23 3 -5 6497.87 307.428 3 23 -3 -4 16693.3 468.098 3 23 3 -4 16952.4 477.036 3 23 -3 -3 3345.97 217.512 3 23 3 -3 3061.31 211.552 3 23 -3 -2 7149.63 300.440 3 23 3 -2 6710.17 295.156 3 23 3 -1 9762.31 1312.97 1 23 3 0 44123.1 2673.41 1 23 3 1 6631.53 1057.11 1 23 3 2 5915.86 997.296 1 23 3 2 5912.60 273.393 3 23 3 3 3373.98 765.060 1 23 -3 3 3169.07 199.399 3 23 3 3 3398.43 214.877 3 23 3 4 16419.4 1668.20 1 23 -3 4 16107.8 435.483 3 23 3 4 17441.5 473.576 3 23 3 5 6725.36 314.657 3 23 3 5 6074.41 1035.56 1 23 -3 5 6873.66 294.734 3 23 3 6 2354.04 209.584 3 23 3 6 1812.78 638.576 1 23 -3 6 2493.58 193.096 3 23 -3 7 1525.80 165.275 3 23 3 7 1277.10 173.361 3 23 -3 8 7310.98 306.172 3 23 3 8 7214.05 341.393 3 23 -3 9 222.810 102.743 3 23 3 9 134.014 148.872 3 23 -3 10 703.498 117.444 3 23 3 10 914.704 172.869 3 23 -3 11 1407.75 127.011 3 23 3 11 1451.89 171.731 3 23 3 12 2668.20 171.278 3 23 3 13 260.277 64.0080 3 23 4 -4 4405.15 248.502 3 23 -4 -3 10415.5 362.771 3 23 4 -3 9363.91 350.246 3 23 4 -2 18044.5 1797.65 1 23 -4 -2 17621.6 467.105 3 23 4 -2 17218.9 471.860 3 23 4 -1 5540.48 1104.62 1 23 4 -1 5237.64 269.616 3 23 4 0 265.305 401.239 1 23 4 0 220.648 95.9298 3 23 4 1 7891.62 1165.91 1 23 4 1 7443.00 313.917 3 23 4 2 16199.9 1690.78 1 23 -4 2 14025.7 400.030 3 23 4 2 15581.3 438.173 3 23 -4 3 6712.05 277.695 3 23 4 3 6429.84 1067.86 1 23 4 3 7206.98 305.944 3 23 -4 4 5548.83 256.847 3 23 4 4 5378.83 1011.60 1 23 4 4 5867.06 289.506 3 23 4 5 25951.1 590.342 3 23 4 5 26767.0 2197.52 1 23 -4 5 24330.9 533.479 3 23 4 6 11474.7 410.424 3 23 4 6 11387.6 1471.64 1 23 -4 6 11092.5 367.424 3 23 4 7 6264.80 318.350 3 23 -4 7 6244.56 281.240 3 23 -4 8 1599.59 156.727 3 23 4 8 1552.65 196.279 3 23 4 9 6862.67 330.001 3 23 -4 9 6912.61 278.143 3 23 4 10 594.945 151.086 3 23 4 11 2347.88 185.392 3 23 4 12 997.817 117.605 3 23 4 13 552.022 70.3026 3 -23 5 -9 358.662 110.629 4 23 5 -4 11460.1 386.708 3 23 -5 -3 22316.9 520.903 3 23 5 -3 22199.3 533.521 3 23 -5 -2 1050.45 132.234 3 23 5 -2 1065.04 138.636 3 23 5 -1 18017.6 1844.69 1 23 -5 -1 19281.8 474.456 3 23 5 -1 17741.1 484.149 3 23 5 0 3506.04 879.602 1 23 5 0 2667.59 204.558 3 23 5 1 18669.7 1828.05 1 23 5 1 18045.5 483.496 3 23 5 2 2264.67 695.077 1 23 5 2 2466.74 195.006 3 23 5 3 21464.1 1989.14 1 23 5 3 21520.6 524.034 3 23 5 4 12380.4 1537.60 1 23 5 4 13303.0 421.337 3 23 5 5 964.155 537.200 1 23 5 5 303.095 123.809 3 23 5 6-944.115 578.039 1 23 5 6 801.547 155.939 3 23 5 7 2623.11 225.382 3 23 5 8 4250.62 269.200 3 23 5 9 454.587 145.404 3 23 5 10 1892.74 186.730 3 23 5 11 134.649 98.9764 3 23 5 12 3110.01 160.393 3 -23 6 -9 2972.62 196.563 4 -23 6 -8 2713.04 216.022 4 23 6 -4 1352.97 144.625 3 23 6 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107.201 3 23 7 7 989.177 158.070 3 23 7 8 4543.14 258.115 3 23 7 9 604.103 130.031 3 23 7 10 7750.18 278.360 3 23 7 11 766.468 94.7562 3 -23 8 -9 7726.09 280.650 4 -23 8 -8 194.892 112.511 4 -23 8 -7 445.188 142.723 4 -23 8 -6 1892.12 216.544 4 -23 8 -5 551.900 160.299 4 23 8 -2 7674.29 1307.21 1 23 8 -1 10245.4 1499.38 1 -23 8 0 4707.05 280.092 4 23 8 0 3008.56 842.023 1 23 8 1 12119.9 1601.38 1 -23 8 1 12412.5 414.266 4 23 8 2 9289.28 1403.52 1 23 8 4 3782.02 230.253 3 23 8 5 573.720 120.144 3 23 8 6 1483.54 161.676 3 23 8 7 104.092 100.951 3 23 8 8 192.375 98.1787 3 23 8 9 9040.22 296.958 3 23 8 10 595.146 94.5839 3 23 8 11 141.047 52.0172 3 -23 9 -9-68.7844 84.3139 4 -23 9 -8 6742.61 289.105 4 -23 9 -7 699.228 149.108 4 -23 9 -6 6646.85 338.910 4 -23 9 -5 2681.06 243.367 4 -23 9 -4 6876.82 365.209 4 -23 9 -3 658.701 169.514 4 -23 9 -2 1577.45 197.449 4 -23 9 -1 2352.68 223.775 4 -23 9 0 653.596 141.331 4 -23 9 1 2618.93 211.762 4 23 9 7 776.836 119.198 3 23 9 8 6164.59 241.905 3 23 9 9 105.709 66.7175 3 -23 10 -9 1352.17 110.891 4 -23 10 -8 312.367 101.723 4 -23 10 -7 2583.22 203.893 4 -23 10 -6 678.935 152.901 4 -23 10 -5 1855.00 221.949 4 -23 10 -4 713.047 171.568 4 -23 10 -3 1535.52 215.286 4 -23 10 -2 1644.95 207.894 4 -23 10 -1 16310.0 520.260 4 -23 10 0 2093.22 205.757 4 -23 10 1 14012.3 451.704 4 23 -11 -9 282.791 69.0817 2 -23 11 -9 175.162 48.7468 4 -23 11 -8 464.941 96.7369 4 -23 11 -7 427.083 119.811 4 -23 11 -6 5711.29 292.012 4 -23 11 -5 888.259 178.142 4 -23 11 -4 2675.16 258.225 4 -23 11 -3 2137.26 225.094 4 -23 11 -2 4215.51 294.330 4 -23 11 -1 159.686 133.267 4 -23 11 0 2184.14 217.594 4 -23 11 1 209.304 113.551 4 -23 12 -8 69.7505 57.3806 4 -23 12 -7 6403.98 252.647 4 -23 12 -6 190.671 116.001 4 -23 12 -5 1593.98 188.095 4 -23 12 -4 6589.93 329.821 4 -23 12 -3 577.040 162.046 4 -23 12 -2 943.983 169.448 4 -23 12 -1 7608.60 355.813 4 -23 12 0 319.621 119.317 4 -23 12 1 5227.96 263.395 4 -23 13 -7 2245.54 137.782 4 -23 13 -6 1521.24 141.808 4 -23 13 -5 470.218 122.296 4 -23 13 -4 937.038 154.799 4 -23 13 -3 206.954 123.493 4 -23 13 -2 6004.05 302.658 4 -23 13 -1 1383.70 170.275 4 -23 13 0 288.679 112.166 4 -23 13 1 910.519 118.436 4 -23 14 -6 372.407 74.4842 4 -23 14 -5-65.0523 81.0029 4 -23 14 -4 319.123 99.8446 4 -23 14 -3-9.16909 97.4762 4 -23 14 -2 358.131 110.502 4 -23 14 -1 606.306 117.842 4 -23 14 0 1234.75 135.259 4 -23 15 -5 20.3597 48.5755 4 -23 15 -4 68.2992 65.3196 4 -23 15 -3 86.6755 68.7661 4 -23 15 -2 1675.19 131.016 4 -23 15 -1 336.661 77.7362 4 -23 15 0 1468.67 107.986 4 24 0 -5 8877.49 362.777 3 24 0 -4 9923.13 378.202 3 24 0 -3 24007.1 568.856 3 24 0 -2 6812.50 305.534 3 24 0 -1 3202.00 216.613 3 24 0 1 927.321 497.172 1 24 0 1 1026.38 132.841 3 24 0 2 7833.80 1075.15 1 24 0 2 8269.20 324.415 3 24 0 3 28004.9 1974.40 1 24 0 3 30048.8 603.903 3 24 0 4 9359.15 1139.62 1 24 0 4 10834.7 373.029 3 24 0 5 6268.28 298.587 3 24 0 6 1274.31 168.875 3 24 0 7 17333.6 499.359 3 24 0 8 1070.43 171.625 3 24 0 9 5332.18 286.332 3 24 0 10 5704.85 287.663 3 24 0 11 8661.66 309.780 3 24 0 12 1250.56 120.330 3 24 0 13 3979.71 140.614 3 24 1 -5 6573.23 313.556 3 24 -1 -4 674.763 135.573 3 24 1 -4 561.842 130.463 3 24 -1 -3 6436.36 302.131 3 24 1 -3 5794.83 286.071 3 24 -1 -2 10799.1 378.014 3 24 1 -2 10734.6 383.233 3 24 -1 -1 21999.8 534.912 3 24 1 -1 22124.0 543.510 3 24 1 0 19970.6 1784.37 1 24 1 0 22485.3 532.244 3 24 -1 1 21660.4 510.912 3 24 1 1 21038.0 512.840 3 24 1 2 11021.9 1311.85 1 24 -1 2 11710.1 379.876 3 24 1 2 11629.4 379.210 3 24 -1 3 5608.13 850.794 1 24 1 3 6480.36 1012.85 1 24 -1 3 6017.26 279.287 3 24 1 3 5897.15 280.063 3 24 1 4 2501.42 625.483 1 24 -1 4 3273.33 217.259 3 24 1 4 2802.73 205.185 3 24 1 5 6593.42 307.493 3 24 -1 5 6087.76 292.088 3 24 -1 6 9016.75 354.820 3 24 1 6 8688.01 361.499 3 24 -1 7 392.956 136.946 3 24 1 7 374.763 133.582 3 24 -1 8 6262.01 306.687 3 24 1 8 6056.00 316.645 3 24 -1 9 4107.61 255.097 3 24 1 9 3846.31 263.439 3 24 -1 10 353.005 123.106 3 24 1 10 380.563 142.778 3 24 1 11 4314.52 233.314 3 24 -1 11 3992.41 215.315 3 24 -1 12 3956.99 178.581 3 24 1 12 4087.49 193.520 3 24 1 13 652.142 71.7299 3 24 2 -5 7153.96 323.966 3 24 -2 -4 2683.14 211.899 3 24 2 -4 2843.88 220.716 3 24 -2 -3 12225.6 407.019 3 24 2 -3 11734.4 404.176 3 24 -2 -2 1011.45 137.132 3 24 2 -2 1118.71 141.671 3 24 2 -1 6188.74 1044.92 1 24 -2 -1 6445.39 295.325 3 24 2 -1 7042.95 314.068 3 24 2 0 808.842 409.954 1 24 -2 0 712.856 121.680 3 24 2 0 571.434 116.180 3 24 2 1 10641.3 1313.71 1 24 -2 1 9863.58 352.050 3 24 2 1 9664.71 355.584 3 24 -2 2 1053.00 134.585 3 24 2 2 949.171 137.379 3 24 2 2 1498.40 587.467 1 24 -2 3 10874.4 367.979 3 24 2 3 10339.6 368.885 3 24 2 4 2923.82 728.360 1 24 -2 4 2723.45 199.454 3 24 2 4 2733.02 213.326 3 24 2 5 4591.22 268.072 3 24 2 5 3592.94 797.899 1 24 -2 5 4076.51 238.128 3 24 2 6 9120.57 370.153 3 24 -2 6 9402.08 357.335 3 24 -2 7 810.304 142.787 3 24 2 7 1188.45 176.698 3 24 -2 8 3612.26 240.339 3 24 2 8 3673.93 263.069 3 24 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143.650 3 24 3 7 1291.39 190.734 3 24 -3 8 917.546 152.680 3 24 3 8 795.760 164.841 3 24 3 9 3927.88 268.923 3 24 -3 9 4085.68 228.298 3 24 -3 10 321.924 98.1826 3 24 3 10 506.452 151.961 3 24 -3 11 499.389 90.8357 3 24 3 11 660.023 136.818 3 24 3 12-72.3216 80.5950 3 24 3 13 19.6801 44.1700 3 24 4 -4 7199.27 321.285 3 24 -4 -3 8906.93 352.464 3 24 4 -3 9915.39 371.604 3 24 -4 -2 5015.46 262.466 3 24 4 -2 5243.11 276.183 3 24 4 -1 1581.84 645.313 1 24 -4 -1 1558.59 162.129 3 24 4 -1 1600.89 167.680 3 24 4 0 12217.0 1493.65 1 24 -4 0 13148.8 412.635 3 24 4 0 12407.5 415.956 3 24 4 1 1520.07 654.664 1 24 -4 1 2006.25 173.686 3 24 4 1 1760.28 174.766 3 24 -4 2 4278.22 230.674 3 24 4 2 4802.72 259.034 3 24 4 3 10209.8 1371.22 1 24 -4 3 9586.22 337.985 3 24 4 3 10120.4 368.603 3 24 -4 4 7501.79 302.900 3 24 4 4 6602.31 1112.35 1 24 4 4 7538.67 328.225 3 24 -4 5 1113.99 137.740 3 24 4 5 1095.64 157.757 3 24 4 6 7196.62 339.204 3 24 -4 6 6264.83 286.274 3 24 4 7 13704.0 452.348 3 24 -4 7 13595.4 403.647 3 24 -4 8 696.653 117.441 3 24 4 8 651.872 154.896 3 24 4 9 2646.65 229.657 3 24 -4 9 2463.43 173.616 3 24 4 10 863.750 155.641 3 24 4 11 2735.88 189.151 3 24 4 12 3.24083 71.5355 3 -24 5 -9 1891.00 168.458 4 24 5 -4 4568.30 260.007 3 24 -5 -3 16300.2 457.832 3 24 5 -3 16090.7 465.260 3 24 5 -2 3554.93 848.675 1 24 -5 -2 2902.08 203.921 3 24 5 -2 3138.31 219.561 3 24 5 -1 8602.16 1315.83 1 24 -5 -1 7954.06 322.710 3 24 5 -1 8460.92 352.283 3 24 -5 0 32945.7 635.126 3 24 5 0 33582.4 677.970 3 24 5 1 9562.35 1349.30 1 24 5 1 7890.38 333.765 3 24 5 2 2624.31 768.460 1 24 5 2 3492.37 231.773 3 24 5 3 17757.5 1856.56 1 24 5 3 17611.0 487.594 3 24 5 4 5837.81 1080.40 1 24 5 4 5290.31 282.650 3 24 5 5 7460.93 1236.71 1 24 5 5 9494.28 369.727 3 24 5 6 8703.43 364.504 3 24 5 7 833.631 163.325 3 24 5 8 370.267 147.608 3 24 5 9 1671.38 189.547 3 24 5 10 733.881 139.250 3 24 5 11 68.5635 91.0545 3 24 5 12 925.986 97.5372 3 -24 6 -9 168.322 91.7815 4 -24 6 -8 4277.92 257.797 4 24 6 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4685.35 260.223 3 24 7 8 768.150 138.952 3 24 7 9 1455.70 157.560 3 24 7 10 2662.65 167.783 3 24 7 11 1266.36 107.889 3 -24 8 -9 4026.53 204.173 4 -24 8 -8 1365.88 153.877 4 -24 8 -7 2674.16 224.748 4 -24 8 -6 2820.03 246.484 4 -24 8 -5 106.168 137.071 4 24 8 -2 1307.98 574.150 1 24 8 -1 20196.4 2073.22 1 -24 8 0 1530.21 183.552 4 24 8 0 904.015 712.367 1 24 8 1 19626.3 2053.63 1 -24 8 1 16273.5 480.827 4 24 8 4 2481.37 189.155 3 24 8 5 1748.82 166.761 3 24 8 6 2283.19 189.415 3 24 8 7 3580.70 216.985 3 24 8 8 1451.02 147.939 3 24 8 9 4109.56 204.158 3 24 8 10 2054.65 129.991 3 -24 9 -9 56.9353 68.2630 4 -24 9 -8 2508.71 183.976 4 -24 9 -7 1117.07 169.889 4 -24 9 -6 1961.83 209.662 4 -24 9 -5 1334.59 200.387 4 -24 9 -4 9780.28 418.587 4 -24 9 -3 1406.23 205.657 4 -24 9 -2 4569.92 302.629 4 -24 9 -1 3981.54 278.038 4 -24 9 0 571.989 132.863 4 -24 9 1 3814.98 249.691 4 24 9 7 771.748 115.115 3 24 9 8 2935.20 169.694 3 24 9 9 156.790 63.0019 3 -24 10 -9 918.204 89.6194 4 24 -10 -9 1042.05 102.420 2 -24 10 -8 31.6337 88.3529 4 -24 10 -7 2319.99 192.171 4 -24 10 -6 1303.43 181.647 4 -24 10 -5 2602.60 238.705 4 -24 10 -4 4243.20 292.451 4 -24 10 -3 4809.59 302.790 4 -24 10 -2 5820.66 334.597 4 -24 10 -1 2682.74 237.948 4 -24 10 0 3697.69 259.696 4 -24 10 1 1873.47 183.976 4 24 -11 -9 95.0447 46.6977 2 -24 11 -8 2194.99 144.280 4 -24 11 -7 521.624 117.221 4 -24 11 -6 1499.93 179.235 4 -24 11 -5 1070.72 177.389 4 -24 11 -4 1119.54 184.817 4 -24 11 -3 2800.58 247.496 4 -24 11 -2 1296.17 182.342 4 -24 11 -1 398.953 141.167 4 -24 11 0 132.896 116.284 4 -24 11 1 472.046 121.779 4 -24 12 -8 152.499 54.3583 4 -24 12 -7 374.494 93.5687 4 -24 12 -6 979.728 141.776 4 -24 12 -5 614.020 139.000 4 -24 12 -4 926.408 164.428 4 -24 12 -3 674.643 155.865 4 -24 12 -2 1683.79 190.768 4 -24 12 -1 220.083 129.087 4 -24 12 0 4093.53 251.752 4 -24 12 1 560.342 115.128 4 -24 13 -7 342.738 68.1352 4 -24 13 -6 562.260 101.908 4 -24 13 -5 1045.12 137.731 4 -24 13 -4 1935.85 176.465 4 -24 13 -3 444.772 131.387 4 -24 13 -2 891.478 150.782 4 -24 13 -1 1152.27 150.571 4 -24 13 0 5978.98 273.448 4 -24 13 1 1436.52 136.623 4 -24 14 -6 2665.08 133.485 4 -24 14 -5 982.220 108.127 4 -24 14 -4 1708.37 142.485 4 -24 14 -3 1911.16 156.259 4 -24 14 -2 42.6767 88.0064 4 -24 14 -1 1608.92 144.638 4 -24 14 0 47.1224 71.3101 4 -24 15 -4 1901.83 115.162 4 -24 15 -3 340.857 72.1889 4 -24 15 -2 1204.49 105.314 4 -24 15 -1-17.4876 53.5326 4 25 0 -5 68.7618 114.965 3 25 0 -4 137.292 121.736 3 25 0 -3 7.58357 107.268 3 25 0 -2-21.6668 95.4838 3 25 0 -1 139.503 95.5601 3 25 0 0 245.479 117.831 3 25 0 1 71.8650 92.3471 3 25 0 2 195.225 110.041 3 25 0 2 3.98864 267.064 1 25 0 3-61.3904 96.0010 3 25 0 3 713.238 393.654 1 25 0 4 26.9840 95.5316 3 25 0 5-73.9044 103.418 3 25 0 6-13.7219 115.610 3 25 0 7-121.269 130.663 3 25 0 8-57.9896 123.987 3 25 0 9 5.56608 125.781 3 25 0 10 11.7343 115.985 3 25 0 11-41.5472 99.3845 3 25 0 12 82.1051 69.4792 3 25 1 -5 1003.30 157.838 3 25 -1 -4 1212.42 169.169 3 25 1 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487.158 3 25 3 -3 17572.8 503.002 3 25 -3 -2 24140.2 579.011 3 25 3 -2 25044.9 593.578 3 25 3 -1 5205.24 1032.06 1 25 -3 -1 4821.89 267.828 3 25 3 -1 5409.42 289.534 3 25 3 0 1832.39 683.215 1 25 -3 0 2331.02 195.477 3 25 3 0 2478.14 206.285 3 25 -3 1 7469.74 319.734 3 25 3 1 7639.14 331.542 3 25 3 2 23959.7 2038.97 1 25 -3 2 23857.0 543.956 3 25 3 2 23356.4 551.954 3 25 3 3 18022.5 1777.07 1 25 -3 3 16663.1 457.768 3 25 3 3 16740.9 479.705 3 25 3 4 2391.19 722.865 1 25 -3 4 2303.00 189.313 3 25 3 4 2307.06 201.874 3 25 3 5 11629.5 1451.21 1 25 -3 5 10945.9 379.345 3 25 3 5 11530.3 411.086 3 25 3 6 6218.30 323.197 3 25 -3 6 6716.11 298.126 3 25 3 7 12451.6 436.754 3 25 -3 7 12526.7 400.832 3 25 -3 8 198.636 105.872 3 25 3 8 146.274 148.393 3 25 3 9 6001.35 310.088 3 25 -3 9 5966.94 264.733 3 25 -3 10 1303.30 133.013 3 25 3 10 1448.43 176.383 3 25 3 11 1289.64 146.741 3 25 -3 11 1162.65 103.958 3 25 3 12 489.179 88.1689 3 25 4 -4 1622.54 178.214 3 25 -4 -3 16074.8 473.278 3 25 4 -3 14887.5 465.412 3 25 -4 -2 8377.67 344.005 3 25 4 -2 8615.54 359.257 3 25 4 -1 18723.1 1930.34 1 25 -4 -1 19170.7 510.453 3 25 4 -1 19096.3 532.463 3 25 4 0 37880.9 2645.67 1 25 -4 0 37948.9 710.480 3 25 4 0 38219.4 732.187 3 25 4 1 18764.8 1846.62 1 25 -4 1 18927.9 492.080 3 25 4 1 18741.6 507.247 3 25 4 2 6260.16 1109.51 1 25 -4 2 5816.64 281.029 3 25 4 2 6253.96 301.566 3 25 4 3 17366.0 1815.91 1 25 -4 3 17510.7 460.820 3 25 4 3 17229.8 486.008 3 25 -4 4 1084.13 139.867 3 25 4 4 1325.41 161.573 3 25 4 4 1161.92 603.206 1 25 -4 5 412.644 106.908 3 25 4 5 209.390 126.941 3 25 4 5 288.238 366.245 1 25 -4 6 3614.47 226.713 3 25 4 6 3876.64 260.913 3 25 4 7 2444.05 227.513 3 25 -4 7 2451.63 185.174 3 25 4 8 2091.22 211.751 3 25 -4 8 2077.40 170.462 3 25 -4 9 1233.29 128.986 3 25 4 9 1569.54 191.633 3 25 4 10 698.548 145.718 3 25 4 11 2672.87 176.975 3 25 4 12 1447.55 115.308 3 -25 5 -9 1179.43 137.598 4 25 5 -4 8566.16 354.000 3 25 -5 -3 2497.78 196.903 3 25 5 -3 2370.19 206.607 3 25 -5 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1469.24 595.515 1 25 6 4 4845.13 270.992 3 25 6 5 6939.87 324.358 3 25 6 6 1507.78 176.619 3 25 6 7 8613.74 350.353 3 25 6 8 2803.96 217.517 3 25 6 9 281.174 120.514 3 25 6 10 2681.64 181.843 3 25 6 11 340.474 78.2132 3 -25 7 -9 5663.94 237.382 4 -25 7 -8 195.247 113.224 4 -25 7 -7 3477.93 244.680 4 25 7 -2 14036.4 1730.39 1 25 7 -1 245.927 348.246 1 25 7 0 2974.20 817.333 1 25 7 0 4251.94 259.966 3 25 7 1 141.998 384.519 1 25 7 1 459.056 122.275 3 25 7 2 14945.0 1784.23 1 25 7 2 15454.2 450.008 3 25 7 3 11238.1 389.483 3 25 7 4 2612.22 210.504 3 25 7 5 3042.23 223.196 3 25 7 6 502.996 131.847 3 25 7 7 3226.70 221.959 3 25 7 8-2.08438 105.517 3 25 7 9 6025.88 256.458 3 25 7 10 589.285 99.3490 3 25 7 11 113.438 54.8229 3 -25 8 -9 188.185 81.4202 4 -25 8 -8 5396.30 259.134 4 -25 8 -7 1095.75 165.733 4 -25 8 -6 1133.80 187.396 4 -25 8 -5 1390.56 207.070 4 -25 8 0 4343.71 275.946 4 -25 8 1 4983.05 277.900 4 25 8 3 1123.88 139.110 3 25 8 4 3946.22 231.356 3 25 8 5 1212.88 151.748 3 25 8 6 1373.42 155.253 3 25 8 7 669.076 123.377 3 25 8 8 4655.94 226.725 3 25 8 9 101.667 74.0452 3 25 8 10 321.420 68.9248 3 -25 9 -9 1643.15 121.282 4 25 -9 -9 1229.25 99.1637 2 -25 9 -8 44.4174 90.5342 4 -25 9 -7 106.809 120.929 4 -25 9 -6 1607.51 194.258 4 -25 9 -5 3842.45 272.158 4 -25 9 -4 1821.34 220.185 4 -25 9 -3 881.366 183.519 4 -25 9 -2 150.452 133.509 4 -25 9 -1 2826.28 239.469 4 -25 9 0 3357.20 245.504 4 -25 9 1 4158.59 253.036 4 25 9 7 247.161 88.2794 3 25 9 8 298.850 79.4576 3 25 -10 -9 351.879 61.2985 2 -25 10 -9 390.485 61.1500 4 -25 10 -8 2283.93 157.691 4 -25 10 -7 2477.73 191.254 4 -25 10 -6 5811.75 292.074 4 -25 10 -5 5051.55 294.889 4 -25 10 -4 2760.39 246.231 4 -25 10 -3 1392.81 201.049 4 -25 10 -2 272.426 145.114 4 -25 10 -1 1543.17 190.167 4 -25 10 0-157.456 132.905 4 -25 10 1 415.074 112.267 4 -25 11 -8 1115.57 106.540 4 -25 11 -7 1102.86 135.115 4 -25 11 -6 401.098 123.908 4 -25 11 -5 692.365 155.244 4 -25 11 -4 7401.25 342.532 4 -25 11 -3 2274.20 227.077 4 -25 11 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668.303 3 26 0 2 22900.4 1874.54 1 26 0 2 25009.6 578.184 3 26 0 3 2713.65 726.928 1 26 0 3 4026.66 246.657 3 26 0 4 3726.61 242.843 3 26 0 5 9394.79 368.427 3 26 0 6 6410.96 313.679 3 26 0 7 5098.85 291.286 3 26 0 8 12873.6 429.565 3 26 0 9 5975.86 295.727 3 26 0 10 70.8700 109.026 3 26 0 11 1696.95 146.627 3 26 0 12 1697.63 118.348 3 26 1 -5 8433.04 371.686 3 26 -1 -4 14415.7 470.582 3 26 1 -4 14214.4 469.807 3 26 -1 -3 11339.0 416.227 3 26 1 -3 11034.2 410.161 3 26 -1 -2 4543.79 278.441 3 26 1 -2 4084.80 266.459 3 26 -1 -1 5102.83 286.476 3 26 1 -1 4927.70 285.531 3 26 -1 0 76356.6 1021.57 3 26 1 0 75963.1 1024.84 3 26 1 1 8822.16 1228.96 1 26 -1 1 8716.20 349.553 3 26 1 1 9102.78 355.456 3 26 1 2 3789.60 833.093 1 26 -1 2 3916.90 244.298 3 26 1 2 4577.77 264.892 3 26 1 3 13686.9 1505.31 1 26 -1 3 14115.5 438.456 3 26 1 3 14721.0 449.305 3 26 -1 4 12238.4 408.391 3 26 1 4 12544.6 420.558 3 26 -1 5 5035.83 270.535 3 26 1 5 5156.30 291.238 3 26 -1 6 2002.43 197.840 3 26 1 6 1750.58 194.300 3 26 -1 7 1528.11 183.418 3 26 1 7 1429.46 184.055 3 26 1 8 2544.80 225.998 3 26 -1 8 2830.18 222.247 3 26 -1 9 2805.46 211.029 3 26 1 9 3013.70 236.925 3 26 -1 10 2238.97 183.449 3 26 1 10 2321.09 191.809 3 26 -1 11 3866.33 192.401 3 26 1 11 3964.81 207.432 3 26 -1 12 1214.63 93.6293 3 26 1 12 1467.20 114.051 3 26 2 -5 4928.30 286.187 3 26 -2 -4 372.319 129.524 3 26 2 -4 435.845 137.093 3 26 -2 -3 2011.20 193.897 3 26 2 -3 2106.64 202.596 3 26 -2 -2 4457.92 268.163 3 26 2 -2 4528.80 279.135 3 26 -2 -1 15203.6 473.502 3 26 2 -1 14685.6 474.460 3 26 -2 0 3529.55 237.759 3 26 2 0 3614.32 245.402 3 26 2 1 13434.9 1561.42 1 26 -2 1 13782.5 432.403 3 26 2 1 13945.1 440.669 3 26 2 2 8243.03 1230.00 1 26 -2 2 7408.82 318.479 3 26 2 2 7764.99 333.370 3 26 -2 3 1310.42 156.682 3 26 2 3 1145.56 154.782 3 26 2 3 1615.16 577.338 1 26 -2 4 431.103 115.626 3 26 2 4 538.295 137.893 3 26 2 4 439.750 357.470 1 26 -2 5 6456.92 305.374 3 26 2 5 6813.44 327.460 3 26 -2 6 8149.47 337.177 3 26 2 6 8023.06 358.601 3 26 -2 7-32.9700 117.610 3 26 2 7 172.632 139.297 3 26 2 8 5152.10 297.914 3 26 -2 8 4928.93 268.667 3 26 -2 9 865.135 141.828 3 26 2 9 862.352 165.366 3 26 -2 10 2106.32 164.501 3 26 2 10 2255.72 195.162 3 26 -2 11 189.461 76.3670 3 26 2 11 282.668 110.282 3 26 2 12 810.296 95.7070 3 26 -3 -4 147.657 122.348 3 26 3 -4 200.746 121.986 3 26 -3 -3 2665.36 215.417 3 26 3 -3 2745.53 225.696 3 26 -3 -2 10305.8 390.065 3 26 3 -2 10863.7 410.111 3 26 -3 -1 5298.90 284.909 3 26 3 -1 5641.25 303.717 3 26 3 0 36292.3 2593.67 1 26 -3 0 37030.8 712.067 3 26 3 0 37243.8 726.493 3 26 -3 1 5468.67 282.369 3 26 3 1 5878.52 297.098 3 26 3 2 12670.1 1546.07 1 26 -3 2 10807.2 380.004 3 26 3 2 12012.6 409.623 3 26 3 3 2714.75 718.964 1 26 -3 3 2240.47 187.507 3 26 3 3 2102.54 196.924 3 26 -3 4 287.551 111.245 3 26 3 4 227.590 132.058 3 26 -3 5 5363.30 275.499 3 26 3 5 4960.58 288.384 3 26 -3 6 685.875 130.909 3 26 3 6 973.876 187.061 3 26 -3 7 5372.81 273.651 3 26 3 7 5197.61 299.388 3 26 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26 4 10 1179.39 152.298 3 26 4 11 910.051 122.141 3 26 4 12 839.248 87.8017 3 -26 5 -9 1254.13 136.054 4 26 5 -4 2648.24 215.967 3 26 -5 -3 24649.3 580.039 3 26 5 -3 23967.5 588.413 3 26 -5 -2 3205.05 223.368 3 26 5 -2 3461.22 239.160 3 26 5 -1 3479.72 881.206 1 26 -5 -1 3281.69 228.056 3 26 5 -1 3341.91 248.324 3 26 5 0 216.863 494.208 1 26 -5 0 919.556 143.811 3 26 5 0 531.011 127.289 3 26 5 1 3946.43 874.155 1 26 -5 1 4829.56 259.008 3 26 5 1 4963.89 278.969 3 26 -5 2 3558.22 223.171 3 26 5 2 3673.43 902.091 1 26 5 2 3878.91 247.187 3 26 5 3 23797.0 2177.74 1 26 5 3 24220.7 574.978 3 26 5 4 2021.33 197.716 3 26 5 4 3183.80 924.331 1 26 5 5 3136.73 239.845 3 26 5 6 2573.58 224.969 3 26 5 7 5330.39 290.522 3 26 5 8 4161.73 256.546 3 26 5 9 2541.45 201.007 3 26 5 10 114.273 99.7886 3 26 5 11 2299.55 147.706 3 26 5 12 130.213 50.0711 3 -26 6 -9 4885.58 226.820 4 -26 6 -8 5510.24 271.975 4 26 6 -4 175.000 94.3912 3 26 6 -3 2445.48 208.542 3 26 -6 -2 13459.8 419.406 3 26 6 -2 13147.3 443.632 3 26 6 -1 2229.69 722.189 1 26 6 -1 3323.78 241.395 3 26 6 0 23978.8 2245.17 1 26 6 0 23753.2 589.401 3 26 6 1 4415.09 981.207 1 26 6 1 4383.91 263.913 3 26 6 2 12056.4 1591.70 1 26 6 2 13131.6 430.404 3 26 6 3 2054.88 194.982 3 26 6 4 614.446 140.941 3 26 6 5 3413.78 237.229 3 26 6 6 13068.1 428.571 3 26 6 7 67.1833 120.128 3 26 6 8 6066.88 287.568 3 26 6 9 5617.68 263.042 3 26 6 10 448.607 102.555 3 26 6 11 148.001 63.3698 3 -26 7 -9 3539.37 188.540 4 -26 7 -8 3769.90 225.404 4 -26 7 -7 2994.08 230.985 4 26 7 -1 10496.2 392.014 3 26 7 0 58.0353 103.832 3 26 7 1 9673.43 372.601 3 26 7 2 379.105 124.370 3 26 7 3 2444.88 209.949 3 26 7 4 6643.89 307.954 3 26 7 5 1266.24 163.032 3 26 7 6 9354.11 353.317 3 26 7 7 984.354 149.462 3 26 7 8 3838.97 225.715 3 26 7 9 4209.53 209.079 3 26 7 10 1054.68 108.051 3 26 7 11 853.752 73.4641 3 -26 8 -9 1.04645 66.6669 4 -26 8 -8 2440.68 178.669 4 -26 8 -7 3067.44 223.741 4 -26 8 -6 2161.18 220.060 4 -26 8 -5 2121.42 225.506 4 -26 8 0 54.8736 112.769 4 -26 8 1 12318.4 422.667 4 26 8 3 1163.61 150.230 3 26 8 4 9490.98 345.319 3 26 8 5 1123.83 147.220 3 26 8 6 1135.08 151.083 3 26 8 7 3060.51 196.460 3 26 8 8 1912.47 152.994 3 26 8 9-8.64164 67.8743 3 26 8 10 2417.96 118.861 3 -26 9 -9 1962.02 122.004 4 -26 9 -8 470.671 105.930 4 -26 9 -7 2216.57 191.311 4 -26 9 -6 2649.13 216.141 4 -26 9 -5 2972.75 250.676 4 -26 9 -4 973.937 185.445 4 -26 9 -3 989.608 182.274 4 -26 9 -2 13177.8 468.652 4 -26 9 -1 355.401 138.530 4 -26 9 0 102.607 115.416 4 -26 9 1 1268.07 163.881 4 26 9 7 2077.64 143.648 3 26 9 8 913.247 95.6871 3 -26 10 -8 590.602 97.1170 4 -26 10 -7 1143.02 138.682 4 -26 10 -6 708.747 145.989 4 -26 10 -5 2229.07 216.230 4 -26 10 -4 1691.99 201.702 4 -26 10 -3 5488.46 317.310 4 -26 10 -2 4036.09 272.318 4 -26 10 -1 1691.43 189.414 4 -26 10 0 20.5713 118.774 4 -26 10 1 1313.15 160.155 4 -26 11 -8 720.963 84.3935 4 -26 11 -7 1168.20 128.198 4 -26 11 -6 483.429 118.225 4 -26 11 -5 103.440 119.889 4 -26 11 -4 387.160 146.102 4 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3 28 6 3 6252.55 308.876 3 28 6 4 5966.32 299.377 3 28 6 5 3785.61 251.521 3 28 6 6 850.654 150.785 3 28 6 7 1460.87 169.407 3 28 6 8 5879.12 264.401 3 28 6 9 2002.65 158.701 3 28 6 10 744.732 97.7581 3 28 6 11 786.817 69.4493 3 -28 7 -9 1059.94 102.284 4 -28 7 -8 875.790 128.739 4 -28 7 -7 1132.38 159.378 4 -28 7 -6 2731.19 233.572 4 28 7 -2 316.394 117.610 3 28 7 -1 3313.72 237.464 3 28 7 0 4216.70 258.855 3 28 7 1 4691.31 263.428 3 28 7 2 217.485 118.921 3 28 7 3 920.839 148.170 3 28 7 4 1480.35 166.011 3 28 7 5 167.505 119.412 3 28 7 6 3545.68 227.164 3 28 7 7 864.232 139.434 3 28 7 8 794.330 119.327 3 28 7 9 1343.82 126.013 3 28 7 10 1139.63 92.2176 3 -28 8 -9 1538.74 106.676 4 -28 8 -8 2897.48 178.093 4 -28 8 -7 125.136 112.283 4 -28 8 -6 5912.52 297.401 4 -28 8 -5 735.844 170.220 4 -28 8 -4 1906.83 225.793 4 -28 8 -3 1273.52 195.383 4 -28 8 -1 4378.02 284.527 4 -28 8 0 538.118 147.101 4 -28 8 1 5337.25 281.176 4 28 8 2 14882.3 430.020 3 28 8 3 1571.09 161.138 3 28 8 4 850.870 134.114 3 28 8 5 511.428 115.830 3 28 8 6 5984.56 258.683 3 28 8 7 152.300 91.4091 3 28 8 8 2614.33 154.146 3 28 8 9 1416.87 102.854 3 -28 9 -8 183.237 76.1151 4 -28 9 -7 2157.29 168.772 4 -28 9 -6 491.310 135.981 4 -28 9 -5 4443.24 268.654 4 -28 9 -4 3176.14 246.839 4 -28 9 -3 1735.33 206.617 4 -28 9 -2 1882.89 202.888 4 -28 9 -1 2219.70 208.811 4 -28 9 0 1656.89 181.011 4 -28 9 1 1437.71 159.699 4 -28 10 -8 880.523 90.4568 4 -28 10 -7 520.453 103.993 4 -28 10 -6 601.559 125.914 4 -28 10 -5 581.348 138.392 4 -28 10 -4 2533.42 219.028 4 -28 10 -3 2199.53 207.386 4 -28 10 -2 7101.94 329.807 4 -28 10 -1 1747.95 187.803 4 -28 10 0 2077.81 187.372 4 -28 10 1 1600.03 156.436 4 -28 11 -7 374.281 78.6284 4 -28 11 -6 331.013 90.0109 4 -28 11 -5 184.438 107.494 4 -28 11 -4 166.970 121.754 4 -28 11 -3-12.8646 121.920 4 -28 11 -2 359.576 117.602 4 -28 11 -1 2346.08 191.759 4 -28 11 0 1661.99 162.135 4 -28 12 -6 793.282 95.4142 4 -28 12 -5 2628.41 163.937 4 -28 12 -4 1951.55 160.085 4 -28 12 -3 1194.00 145.449 4 -28 12 -2 192.442 102.250 4 -28 12 -1 72.1811 88.6852 4 -28 12 0 618.756 106.308 4 -28 13 -5 709.119 84.1443 4 -28 13 -4 362.258 80.7899 4 -28 13 -3 207.225 79.9612 4 -28 13 -2 1941.94 141.811 4 -28 13 -1 1941.58 135.676 4 -28 13 0 1838.72 119.890 4 -28 14 -3 374.857 59.9751 4 -28 14 -2 4043.04 150.772 4 29 0 -4-187.343 160.651 3 29 0 -3 5.75730 139.524 3 29 0 -2 184.054 147.322 3 29 0 -1 122.900 133.918 3 29 0 0 173.253 126.769 3 29 0 1 41.2765 114.888 3 29 0 2-25.8586 126.163 3 29 0 3 243.738 140.311 3 29 0 4 34.3263 121.013 3 29 0 5 163.811 139.834 3 29 0 6-113.964 139.521 3 29 0 7-157.904 137.682 3 29 0 8 106.163 133.872 3 29 0 9-39.8802 109.953 3 29 0 10-41.1903 90.9352 3 29 0 11 19.9472 63.4250 3 29 -1 -4 256.715 133.275 3 29 1 -4 103.793 127.739 3 29 -1 -3 4578.31 294.794 3 29 1 -3 5267.28 322.520 3 29 -1 -2 12851.5 469.734 3 29 1 -2 13470.7 478.814 3 29 -1 -1 14471.8 483.095 3 29 1 -1 14325.2 482.733 3 29 -1 0 10.1482 125.804 3 29 1 0 90.6673 131.076 3 29 -1 1 13614.4 454.713 3 29 1 1 12866.4 450.100 3 29 -1 2 13230.9 441.551 3 29 1 2 13682.2 458.311 3 29 1 3 4937.28 903.104 1 29 -1 3 4887.09 281.868 3 29 1 3 4588.59 281.228 3 29 -1 4 169.710 134.647 3 29 1 4 370.481 140.094 3 29 -1 5 6786.18 327.710 3 29 1 5 6862.25 333.416 3 29 -1 6 1132.12 172.094 3 29 1 6 1321.61 184.999 3 29 1 7 1989.55 210.271 3 29 -1 7 2202.57 208.895 3 29 -1 8 596.914 141.725 3 29 1 8 326.543 140.530 3 29 -1 9 1168.94 147.467 3 29 1 9 1187.01 158.438 3 29 -1 10 292.371 93.8955 3 29 1 10 390.472 105.541 3 29 1 11 567.395 85.9214 3 29 -1 11 543.288 74.6196 3 29 -2 -4 248.764 145.266 3 29 2 -4 617.614 154.296 3 29 -2 -3 7030.48 355.843 3 29 2 -3 7585.13 369.645 3 29 -2 -2 8072.66 375.455 3 29 2 -2 8277.09 387.304 3 29 -2 -1 12442.8 442.568 3 29 2 -1 11931.1 448.869 3 29 -2 0 309.908 126.340 3 29 2 0 442.820 141.967 3 29 -2 1 9493.14 381.917 3 29 2 1 8465.44 372.370 3 29 2 2 10531.3 1387.48 1 29 -2 2 11261.0 408.534 3 29 2 2 10543.5 402.088 3 29 2 3 7377.07 1163.88 1 29 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3 29 3 6 23831.5 590.456 3 29 -3 7 7930.46 308.423 3 29 3 7 7806.64 343.924 3 29 -3 8 218.128 102.447 3 29 3 8 369.706 154.529 3 29 3 9 644.435 138.400 3 29 -3 9 559.719 99.6579 3 29 3 10 766.363 121.347 3 29 -3 10 624.744 80.4573 3 29 3 11 345.647 78.3846 3 -29 4 -9 307.174 84.5284 4 29 4 -4 4020.60 272.474 3 29 -4 -3 9945.23 400.671 3 29 4 -3 10302.0 421.183 3 29 -4 -2 18246.1 528.490 3 29 4 -2 18434.4 556.495 3 29 -4 -1 3720.54 255.082 3 29 4 -1 3604.19 267.403 3 29 -4 0 1170.79 166.618 3 29 4 0 1288.72 186.878 3 29 -4 1 6332.52 308.966 3 29 4 1 6357.44 322.068 3 29 -4 2 14778.6 451.153 3 29 4 2 15667.8 485.366 3 29 -4 3 12016.8 398.516 3 29 4 3 12224.0 431.969 3 29 -4 4 3830.94 238.976 3 29 4 4 3871.30 263.700 3 29 -4 5 5460.21 269.359 3 29 4 5 5535.36 303.923 3 29 4 6 48.7204 134.176 3 29 -4 6 33.2014 95.2932 3 29 4 7 1467.68 186.878 3 29 -4 7 1339.61 140.732 3 29 4 8 1061.78 165.179 3 29 -4 8 939.413 109.510 3 29 4 9 153.638 109.777 3 29 4 10 1798.08 144.805 3 29 4 11 652.227 82.1132 3 -29 5 -9 1395.04 127.601 4 29 5 -4 8570.10 368.596 3 29 5 -3 3443.83 251.537 3 29 -5 -2 4401.76 273.624 3 29 5 -2 4280.43 285.802 3 29 -5 -1 5547.96 294.102 3 29 5 -1 5770.27 314.645 3 29 -5 0 556.108 119.230 3 29 5 0 615.033 146.542 3 29 -5 1 4111.03 247.656 3 29 5 1 4368.02 271.091 3 29 -5 2 2648.89 197.020 3 29 5 2 2642.58 227.125 3 29 -5 3 4790.49 251.488 3 29 5 3 4789.19 286.529 3 29 5 4 7217.53 334.068 3 29 5 5 7527.65 342.020 3 29 5 6 2660.97 218.312 3 29 5 7 643.956 141.296 3 29 5 8 1301.20 164.029 3 29 5 9 1018.64 134.195 3 29 5 10 4361.29 188.426 3 29 5 11 190.614 53.2191 3 -29 6 -9 153.246 68.6892 4 -29 6 -8 334.820 107.948 4 29 6 -3 824.759 150.942 3 29 6 -2 77.1849 115.795 3 29 -6 -1 297.446 112.021 3 29 6 -1 382.885 130.621 3 29 6 0 46.3609 116.157 3 29 6 1 404.615 139.901 3 29 6 2 295.813 122.902 3 29 6 3 362.890 123.647 3 29 6 4 482.454 140.624 3 29 6 5 4696.71 265.392 3 29 6 6 909.003 158.045 3 29 6 7 4409.81 243.944 3 29 6 8 159.289 109.947 3 29 6 9 79.8417 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231.911 50.8574 3 -29 9 -8 631.731 85.6241 4 -29 9 -7 3.19892 87.1170 4 -29 9 -6 3737.70 225.568 4 -29 9 -5 649.004 151.124 4 -29 9 -4 2114.38 211.472 4 -29 9 -3 600.114 147.162 4 -29 9 -2 5433.69 295.603 4 -29 9 -1 1339.44 171.755 4 -29 9 0 2155.72 195.000 4 -29 9 1 704.833 117.129 4 -29 10 -8 508.668 66.3738 4 -29 10 -7 584.529 94.6420 4 -29 10 -6 2539.42 177.619 4 -29 10 -5 2200.44 186.897 4 -29 10 -4 7810.46 323.246 4 -29 10 -3 4493.08 262.470 4 -29 10 -2 1248.17 168.809 4 -29 10 -1 404.948 117.250 4 -29 10 0 1388.27 153.406 4 -29 11 -7 31.8639 53.5338 4 -29 11 -6 366.605 91.2724 4 -29 11 -5 350.926 101.966 4 -29 11 -4 7999.24 300.554 4 -29 11 -3 4267.00 235.599 4 -29 11 -2 506.661 123.656 4 -29 11 -1 1776.51 164.562 4 -29 11 0 3745.80 207.140 4 -29 12 -6 414.534 71.8027 4 -29 12 -5 1555.42 124.980 4 -29 12 -4 260.759 93.7701 4 -29 12 -3 2075.62 159.054 4 -29 12 -2 660.021 115.443 4 -29 12 -1 671.288 106.323 4 -29 12 0 6559.90 235.702 4 -29 13 -5 932.032 78.7129 4 -29 13 -4 1201.59 98.1422 4 -29 13 -3 1164.05 105.261 4 -29 13 -2 180.561 70.7640 4 -29 13 -1 665.652 83.9214 4 30 0 -4 264.600 160.462 3 30 0 -3 29160.9 714.498 3 30 0 -2 37136.3 786.968 3 30 0 -1 2699.24 239.838 3 30 0 0 7886.35 363.301 3 30 0 1 548.130 148.006 3 30 0 2 40191.7 768.314 3 30 0 3 22570.1 580.441 3 30 0 4 612.368 155.136 3 30 0 5 4897.96 288.847 3 30 0 6 580.484 151.418 3 30 0 7 3170.30 236.370 3 30 0 8 1577.73 175.819 3 30 0 9 8267.46 298.214 3 30 0 10 2019.64 146.061 3 30 0 11 3142.61 138.972 3 30 -1 -4 5710.48 331.061 3 30 1 -4 5805.42 336.779 3 30 -1 -3 2119.21 225.566 3 30 1 -3 1886.60 223.317 3 30 -1 -2 1167.75 189.966 3 30 1 -2 1109.11 196.263 3 30 -1 -1 1059.71 186.278 3 30 1 -1 1095.91 184.434 3 30 -1 0 7249.46 349.527 3 30 1 0 7914.41 366.888 3 30 -1 1 1432.60 185.193 3 30 1 1 1422.47 190.514 3 30 -1 2 3210.72 244.762 3 30 1 2 3431.82 259.585 3 30 -1 3 2362.50 220.256 3 30 1 3 2561.74 227.896 3 30 -1 4 8195.45 352.955 3 30 1 4 8636.03 373.014 3 30 -1 5 482.006 146.930 3 30 1 5 434.512 161.653 3 30 -1 6 4362.93 268.132 3 30 1 6 3920.08 266.903 3 30 -1 7 1444.57 180.699 3 30 1 7 1248.17 179.727 3 30 -1 8 12820.2 390.515 3 30 1 8 13260.6 412.190 3 30 -1 9 2026.76 164.644 3 30 1 9 1928.19 174.979 3 30 -1 10 431.266 89.4680 3 30 1 10 421.058 100.805 3 30 -1 11 30.9290 40.7943 3 30 1 11 153.761 64.9051 3 30 -2 -4-15.0683 148.652 3 30 2 -4 139.952 138.286 3 30 -2 -3 3278.33 267.753 3 30 2 -3 3209.25 270.139 3 30 -2 -2 1074.11 181.125 3 30 2 -2 1045.01 185.977 3 30 -2 -1 9761.37 403.226 3 30 2 -1 9961.63 421.455 3 30 -2 0 1545.69 183.991 3 30 2 0 1757.93 207.098 3 30 -2 1 11768.7 428.020 3 30 2 1 12509.1 446.008 3 30 -2 2 585.585 137.177 3 30 2 2 751.566 162.976 3 30 -2 3 4069.46 267.121 3 30 2 3 4677.44 289.250 3 30 2 4 436.735 157.563 3 30 -2 4 300.987 132.286 3 30 -2 5 6963.05 324.083 3 30 2 5 7198.53 341.568 3 30 -2 6 848.311 153.299 3 30 2 6 625.876 173.731 3 30 -2 7 1305.10 157.896 3 30 2 7 1325.20 184.383 3 30 -2 8-15.4368 100.135 3 30 2 8 182.309 143.199 3 30 -2 9 3813.36 199.292 3 30 2 9 4025.85 227.354 3 30 2 10 300.119 98.4990 3 30 -2 10 155.646 62.2919 3 30 2 11 720.455 85.0137 3 30 3 -4 4885.37 301.326 3 30 -3 -3 1238.30 185.765 3 30 3 -3 1343.54 203.870 3 30 -3 -2 1234.94 184.003 3 30 3 -2 1168.45 192.048 3 30 -3 -1 10556.9 410.751 3 30 3 -1 11337.5 439.516 3 30 -3 0 5594.51 302.451 3 30 3 0 5517.50 321.872 3 30 -3 1 11276.6 412.268 3 30 3 1 10213.9 414.511 3 30 -3 2 688.033 147.730 3 30 3 2 644.317 166.253 3 30 -3 3 1763.02 190.722 3 30 3 3 1727.52 200.910 3 30 -3 4 4390.99 255.853 3 30 3 4 4564.03 290.933 3 30 3 5 1605.42 201.133 3 30 -3 5 1854.67 181.808 3 30 3 6 1748.35 208.383 3 30 -3 6 1416.62 158.872 3 30 3 7 117.253 140.081 3 30 -3 7 142.381 99.9508 3 30 -3 8 2399.44 168.628 3 30 3 8 2533.82 211.435 3 30 3 9 1488.78 153.949 3 30 -3 9 1563.87 125.355 3 30 3 10 615.973 103.629 3 30 3 11 209.984 59.9799 3 -30 4 -9 1055.34 110.711 4 30 4 -4 1703.27 198.182 3 30 -4 -3 1249.66 182.978 3 30 4 -3 1333.09 191.312 3 30 -4 -2 1408.23 179.987 3 30 4 -2 1500.10 203.340 3 30 -4 -1 612.252 139.711 3 30 4 -1 504.476 154.607 3 30 -4 0 1167.28 169.719 3 30 4 0 949.801 169.523 3 30 -4 1 773.950 150.007 3 30 4 1 269.876 136.599 3 30 -4 2 937.923 158.199 3 30 4 2 1346.23 189.018 3 30 -4 3 1048.70 152.100 3 30 4 3 1050.15 178.376 3 30 -4 4 2159.97 182.806 3 30 4 4 2460.83 227.079 3 30 4 5 1151.33 187.842 3 30 -4 5 1096.50 152.997 3 30 4 6 669.302 168.176 3 30 -4 6 634.018 125.033 3 30 4 7 1919.21 193.207 3 30 -4 7 1717.72 149.538 3 30 4 8 4215.97 244.090 3 30 4 9 1212.11 141.460 3 30 4 10 1306.65 117.580 3 30 4 11 945.490 79.0182 3 -30 5 -9 1571.66 119.889 4 -30 5 -8 4176.34 223.270 4 30 5 -3 2562.27 234.084 3 30 -5 -2 369.064 123.664 3 30 5 -2 476.826 151.545 3 30 -5 -1 1438.22 173.371 3 30 5 -1 1550.59 191.412 3 30 -5 0 4048.28 248.744 3 30 5 0 3788.76 260.549 3 30 -5 1 1786.79 175.409 3 30 5 1 1966.32 204.663 3 30 -5 2 26.2487 90.2352 3 30 5 2-143.029 133.574 3 30 -5 3 2822.08 203.231 3 30 5 3 2961.34 233.135 3 30 5 4 1829.70 203.301 3 30 5 5 867.558 167.503 3 30 5 6 1461.47 178.409 3 30 5 7 2108.27 191.769 3 30 5 8 4096.70 223.968 3 30 5 9 1696.19 146.044 3 30 5 10 57.5201 65.2456 3 -30 6 -9 2889.02 144.701 4 -30 6 -8 1573.17 144.539 4 -30 6 -7 4080.75 239.509 4 30 6 -3 2862.91 226.039 3 30 6 -2 2753.68 224.637 3 30 -6 -1 17082.5 465.317 3 30 6 -1 17687.5 511.306 3 30 6 0 207.665 135.311 3 30 6 1 22596.5 568.998 3 30 6 2 2896.32 226.659 3 30 6 3 4438.06 264.269 3 30 6 4 5293.99 284.122 3 30 6 5 869.634 151.941 3 30 6 6 477.258 137.303 3 30 6 7 3174.41 208.167 3 30 6 8 1846.58 157.061 3 30 6 9 2719.11 155.856 3 30 6 10 367.294 64.5842 3 -30 7 -9 313.053 60.0564 4 -30 7 -8 1460.54 133.287 4 -30 7 -7 290.257 112.144 4 -30 7 -6 4572.87 267.116 4 30 7 -2 4650.31 266.226 3 30 7 -1 6540.71 314.767 3 30 7 0 25541.5 584.527 3 -30 7 1 6386.40 296.466 4 30 7 1 6080.86 295.882 3 30 7 2 2866.47 214.767 3 30 7 3 208.086 113.431 3 30 7 4 377.230 120.792 3 30 7 5 974.796 140.633 3 30 7 6 3559.79 212.720 3 30 7 7 271.707 99.9250 3 30 7 8 1826.30 134.942 3 30 7 9 516.485 77.1585 3 -30 8 -8 218.706 75.7545 4 -30 8 -7 1791.99 157.124 4 -30 8 -6 350.059 125.717 4 -30 8 -5 2881.79 224.933 4 -30 8 -4 949.664 171.560 4 -30 8 -3 2401.62 225.138 4 -30 8 -2 462.171 147.831 4 -30 8 -1 6218.09 308.091 4 -30 8 0 3545.48 234.543 4 -30 8 1 5284.63 262.696 4 30 8 2 94.1374 93.2053 3 30 8 3 2897.45 191.634 3 30 8 4 838.952 126.313 3 30 8 5 1158.81 134.046 3 30 8 6 247.434 89.2841 3 30 8 7 2195.20 140.899 3 30 8 8 306.838 66.1660 3 -30 9 -8 283.187 65.2370 4 -30 9 -7 115.465 81.3463 4 -30 9 -6 1063.22 137.314 4 -30 9 -5 1981.86 181.612 4 -30 9 -4 1003.41 166.685 4 -30 9 -3 6552.07 310.531 4 -30 9 -2 3045.27 225.085 4 -30 9 -1 2351.44 199.556 4 -30 9 0 684.777 136.695 4 -30 10 -7 1394.69 112.487 4 -30 10 -6 2502.54 164.225 4 -30 10 -5 2546.35 187.273 4 -30 10 -4 509.826 131.105 4 -30 10 -3 600.235 136.876 4 -30 10 -2 2355.76 193.848 4 -30 10 -1 1554.55 162.428 4 -30 10 0 4734.36 238.752 4 -30 11 -7 1212.55 85.7265 4 -30 11 -6 320.707 80.9032 4 -30 11 -5 1518.27 136.703 4 -30 11 -4 433.303 105.273 4 -30 11 -3 441.777 107.714 4 -30 11 -2 115.317 94.6196 4 -30 11 -1 305.238 98.6678 4 -30 11 0 2058.58 152.851 4 -30 12 -5 527.671 82.5386 4 -30 12 -4 1705.45 130.069 4 -30 12 -3 85.9796 76.6412 4 -30 12 -2 435.178 91.9503 4 -30 12 -1 621.119 93.3866 4 -30 12 0 776.051 87.9487 4 -30 13 -4 59.3902 43.3865 4 -30 13 -3 447.522 67.0022 4 -30 13 -2 2576.05 126.519 4 -30 13 -1 31.2985 36.6858 4 31 0 -4-54.3542 155.366 3 31 0 -3 57.0653 157.637 3 31 0 -2 176.623 148.835 3 31 0 -1 127.364 152.686 3 31 0 0-60.5327 142.718 3 31 0 1 81.2872 134.454 3 31 0 2 219.001 141.507 3 31 0 3 97.6169 133.963 3 31 0 4 23.3462 137.395 3 31 0 5 2.60206 138.575 3 31 0 6 100.884 128.500 3 31 0 7 76.9078 126.187 3 31 0 8-59.6269 114.128 3 31 0 9 40.5898 92.8507 3 31 0 10-32.0994 69.4026 3 31 -1 -4 35.9936 152.889 3 31 1 -4-28.7403 152.655 3 31 -1 -3 2297.73 239.516 3 31 1 -3 2459.40 250.978 3 31 -1 -2 1273.80 195.797 3 31 1 -2 1002.35 189.583 3 31 -1 -1 19617.6 562.795 3 31 1 -1 20214.8 578.399 3 31 -1 0 5504.14 309.701 3 31 1 0 5499.30 321.579 3 31 -1 1 20159.7 559.625 3 31 1 1 19572.4 552.231 3 31 -1 2 2099.32 209.461 3 31 1 2 2088.12 219.870 3 31 -1 3 2420.07 228.899 3 31 1 3 2267.71 220.710 3 31 -1 4 166.055 133.435 3 31 1 4 178.523 139.424 3 31 -1 5 3194.59 233.216 3 31 1 5 3364.13 251.572 3 31 1 6 2351.77 216.894 3 31 -1 6 2444.70 215.458 3 31 1 7 2156.15 207.815 3 31 -1 7 2225.31 196.475 3 31 -1 8 1482.52 158.644 3 31 1 8 1796.28 186.496 3 31 1 9 175.867 98.8698 3 31 -1 9 272.864 98.1646 3 31 1 10 870.952 105.364 3 31 -1 10 846.136 94.2280 3 31 1 11 1212.80 85.2322 3 31 2 -4 5795.29 333.387 3 31 -2 -3 2241.14 230.823 3 31 2 -3 2197.60 227.595 3 31 2 -2 2831.49 253.326 3 31 -2 -2 2376.23 231.991 3 31 -2 -1 6556.68 336.396 3 31 2 -1 6305.86 342.887 3 31 -2 0 227.639 147.668 3 31 2 0 22.7799 145.276 3 31 -2 1 4674.87 288.846 3 31 2 1 4652.57 297.615 3 31 -2 2 3001.86 229.475 3 31 2 2 2931.23 243.532 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246.238 3 31 -3 7 3055.94 194.573 3 31 3 7 3057.56 231.173 3 31 -3 8 1856.82 146.443 3 31 3 8 2020.56 188.892 3 31 3 9 96.8574 98.8251 3 31 -3 9 60.7083 62.3094 3 31 3 10 2195.09 140.964 3 -31 4 -9 796.119 91.4486 4 31 4 -4 589.490 147.259 3 31 4 -3 8789.35 400.948 3 31 -4 -2 2786.48 227.908 3 31 4 -2 3405.42 266.857 3 31 -4 -1 775.745 157.422 3 31 4 -1 446.924 153.415 3 31 -4 0 654.408 146.958 3 31 4 0 464.927 142.584 3 31 -4 1 2412.95 208.763 3 31 4 1 2450.42 225.050 3 31 -4 2 2549.10 207.540 3 31 4 2 2599.51 234.342 3 31 -4 3 12912.4 416.450 3 31 4 3 12879.3 443.556 3 31 -4 4 586.883 126.133 3 31 4 4 519.093 147.224 3 31 -4 5 4159.70 233.907 3 31 4 5 4357.03 270.354 3 31 4 6 784.345 157.052 3 31 -4 6 569.344 116.082 3 31 -4 7 4254.61 209.806 3 31 4 7 4497.93 259.835 3 31 4 8 59.7098 103.709 3 31 4 9 888.347 122.536 3 31 4 10 1275.34 109.290 3 -31 5 -9 1215.22 99.4109 4 -31 5 -8 642.066 112.503 4 31 5 -3 398.347 143.364 3 31 -5 -2 8796.45 359.093 3 31 5 -2 8808.08 379.418 3 31 -5 -1 308.778 122.021 3 31 5 -1 280.774 152.272 3 31 -5 0 3470.68 231.608 3 31 5 0 3267.46 246.916 3 31 -5 1 340.200 115.209 3 31 5 1 251.753 144.513 3 31 -5 2 5348.12 267.277 3 31 5 2 5884.88 309.466 3 31 -5 3 916.028 136.112 3 31 5 3 555.967 152.295 3 31 5 4-4.28462 123.463 3 31 5 5 6803.19 323.356 3 31 5 6 793.245 150.818 3 31 5 7 497.632 131.657 3 31 5 8 1515.67 149.708 3 31 5 9 1303.64 123.433 3 31 5 10 1554.05 103.192 3 -31 6 -9 607.589 70.8182 4 -31 6 -8 284.625 83.5389 4 -31 6 -7 222.139 107.891 4 31 6 -3 3562.80 243.145 3 31 6 -2 105.997 115.783 3 31 -6 -1 4318.57 240.231 3 31 6 -1 5209.52 290.346 3 31 6 0 164.009 135.907 3 31 6 1 4818.45 279.717 3 31 6 2 370.765 134.894 3 31 6 3 4322.21 257.156 3 31 6 4 3101.46 224.460 3 31 6 5 816.840 143.786 3 31 6 6 3332.93 212.630 3 31 6 7 245.929 102.870 3 31 6 8 518.597 102.315 3 31 6 9 567.688 85.2494 3 -31 7 -8 868.199 104.398 4 -31 7 -7 1847.87 160.635 4 -31 7 -6 1593.69 172.591 4 -31 7 -5 1622.89 196.227 4 31 7 -2-199.207 120.404 3 31 7 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115.405 4 -31 10 -7 219.675 60.7231 4 -31 10 -6 133.473 79.3336 4 -31 10 -5 765.696 122.731 4 -31 10 -4 1450.98 152.876 4 -31 10 -3 2839.05 194.445 4 -31 10 -2 757.977 128.561 4 -31 10 -1 1114.85 140.205 4 -31 10 0 2086.87 159.585 4 -31 11 -6 236.991 61.7157 4 -31 11 -5 833.337 100.147 4 -31 11 -4 1736.41 140.224 4 -31 11 -3 4051.41 204.914 4 -31 11 -2 1686.73 145.644 4 -31 11 -1 843.170 111.048 4 -31 11 0 3004.01 161.607 4 -31 12 -5 1782.61 104.424 4 -31 12 -4 2333.87 131.616 4 -31 12 -3 2895.58 151.102 4 -31 12 -2 788.223 95.4623 4 -31 12 -1 334.644 69.0954 4 32 0 -4 8614.77 396.658 3 32 0 -3 2383.52 240.175 3 32 0 -2 605.524 173.048 3 32 0 -1 6386.37 346.191 3 32 0 0 3024.88 253.799 3 32 0 1 4284.31 286.600 3 32 0 2 1444.08 198.381 3 32 0 3 3944.78 271.342 3 32 0 4 12821.2 443.853 3 32 0 5 7105.34 328.586 3 32 0 6 1388.02 181.189 3 32 0 7 6316.77 290.621 3 32 0 8 6305.99 267.723 3 32 0 9 393.736 98.2781 3 32 0 10 341.495 75.8033 3 32 1 -4 2862.90 260.043 3 32 -1 -3 3878.13 288.120 3 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198.558 3 32 2 2 2116.02 221.347 3 32 -2 3 4202.21 269.692 3 32 2 3 4086.26 271.162 3 32 -2 4 7286.37 334.640 3 32 2 4 7195.04 348.123 3 32 -2 5 159.201 128.206 3 32 2 5 34.3046 144.991 3 32 2 6 1002.89 179.780 3 32 -2 6 1293.74 166.577 3 32 2 7 895.059 154.727 3 32 -2 7 941.458 138.618 3 32 2 8 562.390 130.069 3 32 -2 8 573.017 109.487 3 32 -2 9 375.353 80.8053 3 32 2 9 379.154 106.017 3 32 2 10 465.093 81.0413 3 -32 3 -9 1160.35 101.006 4 32 3 -4 1062.65 182.281 3 32 -3 -3 7481.29 354.072 3 32 3 -3 7868.77 380.777 3 32 -3 -2 5765.08 321.210 3 32 3 -2 6046.60 336.906 3 32 -3 -1 204.552 134.438 3 32 3 -1 217.537 147.875 3 32 -3 0 1721.60 199.708 3 32 3 0 1438.39 194.644 3 32 -3 1 148.488 122.653 3 32 3 1-53.6860 138.423 3 32 -3 2 5041.15 284.011 3 32 3 2 5017.03 300.311 3 32 -3 3 8467.03 349.351 3 32 3 3 8232.53 364.638 3 32 -3 4 1057.64 154.764 3 32 3 4 1363.61 192.169 3 32 -3 5 2363.31 193.992 3 32 3 5 2294.82 225.437 3 32 -3 6 2396.37 190.491 3 32 3 6 2747.27 230.553 3 32 -3 7 3490.43 199.656 3 32 3 7 3900.07 240.669 3 32 3 8 1076.28 142.431 3 32 -3 8 1003.74 110.533 3 32 -3 9 836.525 82.7173 3 32 3 9 1024.41 121.785 3 32 3 10 66.5451 62.8012 3 -32 4 -9 2081.39 118.367 4 32 4 -3 2638.08 235.215 3 32 -4 -2 4816.60 288.074 3 32 4 -2 5257.52 308.191 3 32 -4 -1 970.167 164.054 3 32 4 -1 949.090 168.021 3 32 -4 0 38.7634 114.129 3 32 4 0 218.819 140.009 3 32 -4 1 686.978 149.566 3 32 4 1 686.531 160.308 3 32 -4 2 5750.24 289.263 3 32 4 2 5500.49 307.596 3 32 -4 3 2401.63 195.448 3 32 4 3 2591.00 231.651 3 32 -4 4 2762.77 204.511 3 32 4 4 3443.73 252.111 3 32 -4 5 2082.75 172.855 3 32 4 5 2326.03 215.223 3 32 -4 6 1695.26 149.822 3 32 4 6 1851.02 188.926 3 32 -4 7 2676.61 161.727 3 32 4 7 2872.44 209.334 3 32 4 8 660.404 119.764 3 32 4 9 2438.85 154.352 3 32 4 10 26.0192 53.3055 3 -32 5 -9 638.583 71.7754 4 -32 5 -8 2083.27 146.027 4 32 5 -3-121.337 135.440 3 32 5 -2 2396.01 215.817 3 32 -5 -1 10045.8 377.678 3 32 5 -1 10661.9 409.070 3 32 -5 0 2428.30 200.921 3 32 5 0 2788.17 229.235 3 32 -5 1 11056.0 376.283 3 32 5 1 11505.2 418.216 3 32 -5 2 2659.10 194.564 3 32 5 2 2885.94 225.349 3 32 -5 3 68.6623 88.1001 3 32 5 3 100.658 130.717 3 32 5 4 1318.10 176.922 3 32 5 5 3232.42 227.252 3 32 5 6 470.676 135.962 3 32 5 7 1388.12 151.307 3 32 5 8 2698.89 170.767 3 32 5 9 969.916 102.664 3 -32 6 -8 3295.34 166.809 4 -32 6 -7 1247.97 140.272 4 32 6 -3 1229.86 160.188 3 32 6 -2 160.122 119.250 3 32 6 -1 7500.11 337.557 3 32 6 0 19842.1 519.861 3 32 6 1 6455.93 308.475 3 32 6 2-161.992 130.802 3 32 6 3 2227.32 202.144 3 32 6 4 755.302 143.411 3 32 6 5 1078.66 151.639 3 32 6 6 400.319 116.558 3 32 6 7 1459.19 140.659 3 32 6 8 3005.81 161.632 3 32 6 9 972.394 87.8371 3 -32 7 -8 1188.91 102.001 4 -32 7 -7 1321.72 134.306 4 -32 7 -6 2230.70 182.716 4 -32 7 -5 1310.60 173.052 4 32 7 -2 1131.56 145.779 3 32 7 -1 962.572 139.327 3 -32 7 0 2628.40 206.919 4 32 7 0 2337.80 192.074 3 -32 7 1 1823.83 159.277 4 32 7 1 1914.03 178.288 3 32 7 2 1116.27 148.565 3 32 7 3 2300.01 187.525 3 32 7 4 3581.44 213.801 3 32 7 5 1532.68 152.462 3 32 7 6 1498.61 141.495 3 32 7 7 1128.54 114.276 3 32 7 8 1355.42 101.884 3 -32 8 -8 270.652 58.4224 4 -32 8 -7 2198.42 145.853 4 -32 8 -6 1232.64 138.523 4 -32 8 -5 197.810 112.501 4 -32 8 -4 1033.21 159.998 4 -32 8 -3 5910.67 289.753 4 -32 8 -2 5346.09 276.137 4 -32 8 -1 1583.40 169.446 4 -32 8 0 94.9394 91.1449 4 32 8 1 2020.00 161.230 3 32 8 2 5093.95 233.020 3 32 8 3 4970.10 227.711 3 32 8 4 325.876 92.1050 3 32 8 5 205.891 77.1346 3 32 8 6 659.079 89.3658 3 32 8 7 1843.58 112.322 3 -32 9 -7 1306.16 104.657 4 -32 9 -6 1017.84 117.680 4 -32 9 -5 866.462 128.232 4 -32 9 -4 184.798 104.936 4 -32 9 -3 467.442 124.386 4 -32 9 -2 4309.42 239.898 4 -32 9 -1 5585.53 256.977 4 -32 9 0 5663.08 247.853 4 -32 10 -6 220.499 70.9883 4 -32 10 -5 3136.31 172.653 4 -32 10 -4 691.370 112.632 4 -32 10 -3 1774.81 158.604 4 -32 10 -2 90.4132 93.8533 4 -32 10 -1 1226.59 136.012 4 -32 10 0 3134.38 173.625 4 -32 11 -5 73.5593 58.3751 4 -32 11 -4 115.239 70.0727 4 -32 11 -3-17.9976 70.6871 4 -32 11 -2 6.38012 69.8844 4 -32 11 -1 348.719 77.7054 4 -32 12 -4 40.1253 42.9072 4 -32 12 -3 448.834 69.5167 4 -32 12 -2 1985.06 114.884 4 -32 12 -1 1570.09 97.1938 4 33 0 -3-211.036 165.968 3 33 0 -2 10.6652 146.940 3 33 0 -1 9.66907 143.383 3 33 0 0 42.8486 150.021 3 33 0 1 72.3445 146.983 3 33 0 2-31.3643 144.077 3 33 0 3-54.5956 147.800 3 33 0 4 67.0629 141.867 3 33 0 5 152.161 140.883 3 33 0 6-22.6212 120.596 3 33 0 7-103.177 112.570 3 33 0 8 84.1493 97.2485 3 33 0 9 29.9129 73.2364 3 33 0 10 7.16619 44.7067 3 33 1 -4 209.756 155.840 3 33 -1 -3 15877.3 515.071 3 33 1 -3 15865.6 526.308 3 33 -1 -2 6369.02 343.104 3 33 1 -2 6814.38 354.910 3 33 -1 -1 3357.19 260.893 3 33 1 -1 3322.38 268.583 3 33 -1 0 11765.7 435.918 3 33 1 0 11895.1 449.647 3 33 -1 1 5027.91 296.459 3 33 1 1 4904.66 297.945 3 33 -1 2 6214.67 325.951 3 33 1 2 6142.67 328.904 3 33 -1 3 15889.4 487.860 3 33 1 3 16233.5 495.365 3 33 -1 4 374.269 143.390 3 33 1 4 669.945 171.110 3 33 -1 5 2065.82 199.727 3 33 1 5 1710.39 202.380 3 33 -1 6 2663.12 208.512 3 33 1 6 2752.40 221.334 3 33 -1 7 70.5197 104.055 3 33 1 7 179.467 118.503 3 33 -1 8 184.998 93.9284 3 33 1 8 122.923 101.330 3 33 -1 9 1121.40 108.899 3 33 1 9 1090.93 113.318 3 33 1 10 1462.19 100.851 3 -33 2 -9 424.909 65.5921 4 33 -2 -3 1367.27 190.475 3 33 2 -3 1276.74 198.826 3 33 -2 -2 613.269 154.422 3 33 2 -2 714.390 180.842 3 33 -2 -1 1643.20 197.889 3 33 2 -1 1675.34 217.447 3 33 -2 0 1953.64 216.333 3 33 2 0 2061.25 224.950 3 33 -2 1 2189.95 209.778 3 33 2 1 1824.91 218.230 3 33 -2 2 601.837 149.036 3 33 2 2 403.868 159.368 3 33 -2 3 1011.22 168.281 3 33 2 3 1150.83 190.357 3 33 -2 4 5367.92 287.137 3 33 2 4 5927.74 315.352 3 33 -2 5 17441.6 469.601 3 33 2 5 17948.9 506.426 3 33 -2 6 2503.86 192.944 3 33 2 6 2844.03 227.556 3 33 -2 7 1051.38 133.586 3 33 2 7 1061.97 155.512 3 33 -2 8-1.73848 75.4354 3 33 2 8-3.00620 96.6410 3 33 -2 9 233.475 62.7225 3 33 2 9 422.562 92.5664 3 33 2 10 1801.55 108.366 3 -33 3 -9 848.673 78.7113 4 33 -3 -3 2035.31 212.989 3 33 3 -3 2339.90 235.214 3 33 -3 -2 4949.14 295.865 3 33 3 -2 5072.22 307.227 3 33 -3 -1 11334.9 422.274 3 33 3 -1 11603.1 437.840 3 33 3 0 2526.91 241.587 3 33 -3 0 1849.40 198.700 3 33 -3 1 7577.37 337.553 3 33 3 1 7249.77 348.041 3 33 -3 2 5699.84 295.441 3 33 3 2 6109.13 325.514 3 33 -3 3 965.035 155.273 3 33 3 3 925.284 176.853 3 33 -3 4 14032.1 422.280 3 33 3 4 13632.8 446.254 3 33 -3 5 4767.92 251.362 3 33 3 5 4734.85 276.606 3 33 -3 6 3362.29 203.747 3 33 3 6 3430.43 235.730 3 33 -3 7 5080.47 223.604 3 33 3 7 5388.17 257.111 3 33 -3 8 503.775 84.1899 3 33 3 8 501.507 116.063 3 33 3 9 713.643 99.0226 3 33 3 10 1205.41 90.6682 3 -33 4 -9-29.6190 41.3495 4 -33 4 -8 1643.86 134.421 4 33 4 -3 2067.13 208.000 3 33 -4 -2 1512.10 182.002 3 33 4 -2 1435.51 192.793 3 33 -4 -1 1076.14 168.566 3 33 4 -1 1229.53 185.918 3 33 -4 0 1174.00 164.879 3 33 4 0 1509.82 198.030 3 33 -4 1 1681.75 182.705 3 33 4 1 1622.41 190.456 3 33 -4 2 1715.73 182.085 3 33 4 2 1466.29 192.699 3 33 -4 3 1214.54 152.963 3 33 4 3 1563.42 191.016 3 33 -4 4 4034.07 229.226 3 33 4 4 4182.09 262.367 3 33 -4 5 821.091 127.959 3 33 4 5 854.013 157.792 3 33 -4 6 3135.17 182.402 3 33 4 6 3258.26 223.095 3 33 4 7 356.874 120.025 3 33 4 8 2121.07 155.793 3 33 4 9 151.617 72.8777 3 -33 5 -8 903.998 101.773 4 33 5 -3 2160.76 202.413 3 33 5 -2 838.852 160.135 3 33 -5 -1 1829.59 176.825 3 33 5 -1 1913.83 203.524 3 33 -5 0 3513.90 222.142 3 33 5 0 3755.75 255.481 3 33 -5 1 1830.96 171.538 3 33 5 1 1905.03 200.241 3 33 -5 2 282.339 99.8791 3 33 5 2 231.114 131.908 3 33 -5 3 2424.20 173.517 3 33 5 3 2379.08 213.322 3 33 5 4 1659.38 183.689 3 33 5 5 114.757 119.440 3 33 5 6 4194.67 231.331 3 33 5 7 2686.51 178.926 3 33 5 8 793.997 106.961 3 33 5 9 652.033 81.6949 3 -33 6 -8 1010.83 98.0034 4 -33 6 -7 1928.50 152.818 4 -33 6 -6 269.039 122.490 4 33 6 -2 129.256 113.255 3 33 6 -1 892.825 152.781 3 33 6 0 45.7556 117.890 3 33 6 1 736.458 157.328 3 33 6 2-66.5272 122.980 3 33 6 3 1021.98 151.315 3 33 6 4 573.779 133.971 3 33 6 5 3554.71 215.525 3 33 6 6 431.975 109.042 3 33 6 7 1663.64 139.435 3 33 6 8 1538.63 116.740 3 -33 7 -8 386.721 66.5278 4 -33 7 -7 1294.07 119.466 4 -33 7 -6 3676.67 203.992 4 -33 7 -5 1057.47 153.531 4 -33 7 -4 3996.47 244.614 4 33 7 -2 3947.43 218.394 3 -33 7 -1 452.571 127.662 4 33 7 -1 461.595 115.353 3 -33 7 0 157.656 98.7362 4 33 7 0 129.174 94.2666 3 33 7 1 353.688 113.979 3 33 7 2 4273.10 232.947 3 33 7 3-126.561 103.208 3 33 7 4 3887.61 212.733 3 33 7 5 1123.09 132.828 3 33 7 6 3175.69 174.999 3 33 7 7 1240.53 108.716 3 33 7 8 319.489 57.8470 3 -33 8 -7 256.173 72.6927 4 -33 8 -6 347.444 94.8973 4 -33 8 -5 3344.33 200.718 4 -33 8 -4 980.440 143.886 4 -33 8 -3 1799.67 178.451 4 -33 8 -2 892.381 144.791 4 -33 8 -1 3781.36 222.993 4 -33 8 0-30.4615 83.8764 4 33 8 2 297.599 91.4940 3 33 8 3 1517.12 132.135 3 33 8 4 561.637 95.2599 3 33 8 5 2884.28 152.946 3 33 8 6 151.736 58.3813 3 -33 9 -7 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31.6041 84.8146 4 -36 6 -4 229.954 108.798 4 36 6 -1 2642.33 182.054 3 -36 6 0 260.192 87.6184 4 36 6 0 340.531 112.515 3 36 6 1 2104.08 173.109 3 36 6 2 577.989 119.029 3 36 6 3 730.237 122.463 3 36 6 4 384.516 100.789 3 36 6 5 33.9620 74.2685 3 36 6 6 50.2327 62.7371 3 36 6 7 4126.58 148.481 3 -36 7 -6 825.492 93.7273 4 -36 7 -5 654.256 99.8505 4 -36 7 -4 906.003 114.096 4 -36 7 -3 516.081 110.245 4 -36 7 -2 1160.53 129.599 4 -36 7 -1 1570.65 139.015 4 36 7 -1 1416.64 124.164 3 -36 7 0 43.5921 68.5149 4 36 7 0 25.6498 73.6111 3 36 7 1 1285.18 124.669 3 36 7 2 1161.04 121.307 3 36 7 3 205.911 78.8896 3 36 7 4 718.843 95.2955 3 36 7 5 562.366 78.7000 3 36 7 6 594.175 65.0723 3 -36 8 -6 561.004 67.9255 4 -36 8 -5 239.729 69.0163 4 -36 8 -4 532.173 91.3904 4 -36 8 -3 407.991 89.6274 4 -36 8 -2 94.8919 72.7784 4 -36 8 -1 498.421 90.3127 4 -36 9 -5 352.080 58.1073 4 -36 9 -4 891.793 89.6815 4 -36 9 -3 446.720 78.8541 4 -36 9 -2 183.695 64.2988 4 -36 9 -1 256.749 61.8153 4 37 0 -2-19.4182 134.107 3 37 0 -1-82.1190 144.905 3 37 0 0 84.4065 137.790 3 37 0 1 35.3892 140.733 3 37 0 2 15.1731 130.165 3 37 0 3-98.5574 131.258 3 37 0 4-47.9720 121.482 3 37 0 5-48.4351 102.164 3 37 0 6-88.2831 90.7944 3 37 0 7-10.4719 71.3694 3 37 0 8-82.8525 50.7159 3 37 -1 -2 967.010 161.746 3 37 1 -2 796.997 164.534 3 37 -1 -1 1195.98 176.944 3 37 1 -1 918.557 176.898 3 37 -1 0 976.106 171.935 3 37 1 0 652.303 161.963 3 37 -1 1 988.417 162.953 3 37 1 1 1079.07 181.163 3 37 -1 2 1187.83 166.437 3 37 1 2 1278.68 180.128 3 37 -1 3 1299.32 165.738 3 37 1 3 976.986 162.026 3 37 -1 4 870.655 141.307 3 37 1 4 886.145 154.946 3 37 -1 5 76.2601 96.3856 3 37 1 5 326.044 118.629 3 37 -1 6 569.889 99.4392 3 37 1 6 778.990 117.401 3 37 -1 7 29.8684 64.5228 3 37 1 7 149.202 78.3687 3 37 1 8 721.956 78.3827 3 37 -2 -2 109.359 122.474 3 37 2 -2 247.680 138.282 3 37 -2 -1 5639.71 287.631 3 37 2 -1 5651.76 294.102 3 37 -2 0 4016.15 251.541 3 37 2 0 3899.79 260.149 3 37 -2 1 5627.58 278.873 3 37 2 1 5424.33 293.143 3 37 -2 2 295.076 125.568 3 37 2 2 175.537 136.974 3 37 -2 3 1518.36 161.673 3 37 2 3 1572.99 180.590 3 37 -2 4 558.600 121.701 3 37 2 4 455.017 135.273 3 37 -2 5 5697.80 236.683 3 37 2 5 6006.31 258.603 3 37 -2 6 411.759 88.0495 3 37 2 6 317.057 100.985 3 37 -2 7 500.715 72.4888 3 37 2 7 524.684 92.3756 3 37 2 8 711.013 80.6280 3 37 3 -2 4191.36 251.713 3 37 -3 -1 546.788 128.729 3 37 3 -1 532.436 141.474 3 37 -3 0 734.358 138.844 3 37 3 0 779.886 158.181 3 37 -3 1 768.658 140.785 3 37 3 1 616.246 151.428 3 37 -3 2 6729.18 280.044 3 37 3 2 6690.59 304.156 3 37 -3 3 602.149 115.822 3 37 3 3 602.642 137.324 3 37 -3 4 14371.9 361.970 3 37 3 4 14833.4 402.088 3 37 -3 5 913.068 105.311 3 37 3 5 1218.65 145.417 3 37 -3 6 329.102 68.7918 3 37 3 6 338.014 96.8527 3 37 3 7 1310.47 115.139 3 37 3 8 775.886 76.6634 3 -37 4 -7 820.004 86.8974 4 37 4 -2 270.716 118.166 3 37 4 -1 3477.50 224.678 3 37 -4 0 766.200 121.595 3 37 4 0 903.247 146.237 3 37 -4 1 3417.54 201.588 3 37 4 1 4008.93 237.036 3 37 -4 2 66.8836 86.1112 3 37 4 2 537.330 143.210 3 37 -4 3 2674.81 167.018 3 37 4 3 2694.08 196.824 3 37 -4 4 844.438 101.588 3 37 4 4 902.828 134.819 3 37 4 5 1995.32 157.988 3 37 4 6 153.058 81.3805 3 37 4 7 952.234 94.3769 3 -37 5 -7 527.874 69.0641 4 -37 5 -6 888.110 102.690 4 37 5 -2 781.466 125.947 3 37 5 -1 1731.77 163.475 3 37 5 0 741.024 129.197 3 37 -5 1 1325.68 121.156 3 37 5 1 1482.68 159.548 3 37 5 2 765.042 128.430 3 37 5 3 520.225 118.641 3 37 5 4 33.5440 88.3399 3 37 5 5 782.818 109.394 3 37 5 6 842.453 96.0404 3 37 5 7 405.684 63.8014 3 -37 6 -6 96.4158 61.7890 4 -37 6 -5 1594.05 128.851 4 -37 6 -4 674.062 113.307 4 -37 6 -3 4465.06 215.635 4 -37 6 -2 575.707 110.238 4 -37 6 -1 260.311 94.1765 4 37 6 -1 346.824 96.6696 3 -37 6 0 1483.15 123.456 4 37 6 0 1190.74 128.878 3 37 6 1 111.942 90.5878 3 37 6 2 388.712 97.4196 3 37 6 3 4319.82 202.950 3 37 6 4 858.038 108.356 3 37 6 5 1143.77 105.483 3 37 6 6 254.732 61.5310 3 -37 7 -6 1097.49 86.1770 4 -37 7 -5 659.414 86.2494 4 -37 7 -4 1681.44 127.125 4 -37 7 -3 170.577 77.4976 4 -37 7 -2 1464.42 127.709 4 -37 7 -1-40.9960 70.1937 4 -37 7 0-75.6651 56.1555 4 37 7 0 78.4988 64.7334 3 37 7 1 109.608 70.2247 3 37 7 2 1113.56 103.605 3 37 7 3 104.962 61.3362 3 37 7 4 1508.14 105.254 3 37 7 5 577.788 64.2314 3 -37 8 -5 1176.96 90.0541 4 -37 8 -4 295.607 69.0885 4 -37 8 -3 30.4881 60.3324 4 -37 8 -2 141.662 65.3724 4 -37 8 -1 349.177 68.0417 4 -37 9 -3-23.9651 47.6321 4 -37 9 -2 147.852 47.8456 4 38 0 -2 2657.14 208.827 3 38 0 -1 2922.91 220.088 3 38 0 0 5975.39 290.238 3 38 0 1 1875.60 191.688 3 38 0 2 2973.15 214.764 3 38 0 3 577.511 130.370 3 38 0 4 1394.78 150.596 3 38 0 5 380.624 97.6869 3 38 0 6 3014.56 165.069 3 38 0 7 1333.51 102.522 3 38 -1 -2 2180.26 191.353 3 38 1 -2 2147.57 197.774 3 38 -1 -1 2571.87 206.928 3 38 1 -1 2083.95 201.706 3 38 -1 0 296.373 127.620 3 38 1 0 455.621 143.298 3 38 -1 1 2442.74 204.672 3 38 1 1 2749.91 218.816 3 38 1 2 2206.39 200.455 3 38 -1 2 1972.52 178.775 3 38 -1 3 513.767 125.321 3 38 1 3 546.851 138.737 3 38 -1 4 2932.48 186.422 3 38 1 4 3470.12 212.066 3 38 -1 5 422.245 100.342 3 38 1 5 574.616 113.081 3 38 -1 6 381.010 84.7228 3 38 1 6 105.165 79.1182 3 38 -1 7 499.360 69.1904 3 38 1 7 404.336 72.5465 3 38 2 -2 704.804 145.147 3 38 -2 -1 245.813 118.950 3 38 2 -1 281.134 129.781 3 38 -2 0 212.861 110.342 3 38 2 0 362.616 131.590 3 38 -2 1 443.884 123.994 3 38 2 1 318.901 140.534 3 38 -2 2 559.196 127.039 3 38 2 2 939.291 158.298 3 38 -2 3 311.092 103.657 3 38 2 3 510.421 136.455 3 38 -2 4 1702.53 149.820 3 38 2 4 1628.43 163.020 3 38 -2 5 2645.33 158.223 3 38 2 5 2994.79 184.454 3 38 -2 6 491.144 79.3633 3 38 2 6 526.154 98.5545 3 38 2 7 1469.08 107.490 3 -38 3 -7 110.065 51.2185 4 38 3 -2 250.728 117.575 3 38 -3 -1 116.846 103.284 3 38 3 -1 342.219 126.571 3 38 -3 0 339.909 110.469 3 38 3 0 290.782 125.828 3 38 -3 1 87.9985 100.907 3 38 3 1 33.1973 117.666 3 38 -3 2 382.107 109.110 3 38 3 2 289.937 121.596 3 38 -3 3 142.415 86.1734 3 38 3 3 276.480 119.215 3 38 -3 4 250.538 82.5485 3 38 3 4 199.477 104.281 3 38 -3 5 479.841 79.5353 3 38 3 5 522.804 107.853 3 38 -3 6 6.78910 39.5983 3 38 3 6-54.1594 75.6360 3 38 3 7 80.3867 60.4376 3 -38 4 -7 81.2224 43.7221 4 -38 4 -6 1026.65 102.880 4 38 4 -2 341.387 108.677 3 38 4 -1 1457.46 159.814 3 38 -4 0 2068.03 150.138 3 38 4 0 1981.12 178.061 3 38 -4 1 1206.85 126.503 3 38 4 1 1399.31 158.238 3 38 -4 2 554.344 95.9429 3 38 4 2 659.945 121.941 3 38 -4 3 397.228 82.8235 3 38 4 3 482.171 116.813 3 38 -4 4 802.016 89.0814 3 38 4 4 980.890 129.115 3 38 4 5 1283.43 126.584 3 38 4 6 1084.53 103.924 3 38 4 7 81.4106 47.7962 3 -38 5 -6-4.32254 52.4117 4 -38 5 -5 1280.23 116.810 4 38 5 -1 2051.12 161.450 3 -38 5 0 316.753 77.5933 4 38 5 0 306.439 99.7588 3 38 5 1 1537.89 147.743 3 38 5 2 854.358 124.167 3 38 5 3 229.755 95.8614 3 38 5 4 3375.14 175.145 3 38 5 5 929.810 99.7148 3 38 5 6-12.0524 51.4388 3 -38 6 -6 534.649 66.4181 4 -38 6 -5 38.6768 60.6410 4 -38 6 -4 406.319 84.6515 4 -38 6 -3 2664.96 159.864 4 -38 6 -2 104.259 75.5905 4 -38 6 -1 2316.56 143.740 4 -38 6 0 145.620 61.4113 4 38 6 0 75.9240 76.6904 3 38 6 1 1427.33 127.142 3 38 6 2 134.590 75.7558 3 38 6 3 1431.28 120.391 3 38 6 4 778.849 90.5065 3 38 6 5 238.608 57.5292 3 -38 7 -5-5.35583 46.2408 4 -38 7 -4 293.018 69.3811 4 -38 7 -3 185.717 71.3327 4 -38 7 -2 55.8329 64.9648 4 -38 7 -1 109.746 56.2632 4 38 7 1 170.777 58.8587 3 38 7 2 276.411 61.8230 3 38 7 3 255.123 58.8559 3 -38 8 -4 1068.29 81.6665 4 -38 8 -3 936.630 82.0180 4 -38 8 -2 680.671 73.1319 4 39 0 -1 2.05412 115.678 3 39 0 0 73.9212 119.777 3 39 0 1 108.994 113.745 3 39 0 2 231.269 119.505 3 39 0 3-8.23262 95.5660 3 39 0 4 42.6627 91.1799 3 39 0 5-45.6850 76.1481 3 39 0 6 23.1081 59.2127 3 39 1 -2 2157.77 182.039 3 39 -1 -1 3157.84 202.971 3 39 1 -1 3372.34 218.036 3 39 -1 0 1606.84 166.051 3 39 1 0 1402.56 169.843 3 39 -1 1 3279.59 210.149 3 39 1 1 3485.22 222.693 3 39 -1 2 2349.95 183.128 3 39 1 2 2367.34 182.444 3 39 -1 3 227.431 106.183 3 39 1 3 637.828 126.228 3 39 -1 4 887.027 117.439 3 39 1 4 1073.81 129.346 3 39 -1 5 2587.85 150.672 3 39 1 5 2509.25 158.796 3 39 -1 6 604.202 80.0233 3 39 1 6 536.799 85.9492 3 39 1 7 144.649 48.4426 3 39 2 -2 780.652 132.873 3 39 -2 -1 1399.30 147.660 3 39 2 -1 1555.91 167.841 3 39 -2 0 105.567 99.6763 3 39 2 0 142.955 120.147 3 39 -2 1 1063.33 136.855 3 39 2 1 1077.91 154.014 3 39 -2 2 1685.55 152.575 3 39 2 2 1627.63 164.218 3 39 -2 3 1414.52 138.388 3 39 2 3 1462.85 149.757 3 39 -2 4 3803.21 182.697 3 39 2 4 3774.91 198.659 3 39 -2 5 461.890 81.4905 3 39 2 5 513.931 95.7523 3 39 -2 6 658.643 69.6661 3 39 2 6 651.097 87.3807 3 39 2 7 499.939 64.7991 3 39 3 -1 2574.51 189.304 3 39 -3 0 108.517 91.9148 3 39 3 0 81.0750 106.963 3 39 -3 1 1846.47 152.878 3 39 3 1 2197.56 176.905 3 39 -3 2 1130.54 123.519 3 39 3 2 1518.46 154.068 3 39 -3 3 1693.28 133.685 3 39 3 3 1665.30 151.722 3 39 -3 4 254.832 73.6267 3 39 3 4 181.295 92.0559 3 39 -3 5 1232.83 88.7314 3 39 3 5 1396.55 123.663 3 39 3 6 2265.94 128.990 3 -39 4 -6 419.798 65.9188 4 39 4 -1 776.570 123.017 3 39 4 0 28.7171 91.7416 3 39 -4 1 713.284 96.8954 3 39 4 1 866.702 127.837 3 39 -4 2 1643.97 122.401 3 39 4 2 1820.67 156.748 3 39 -4 3 1361.65 104.282 3 39 4 3 1601.91 141.621 3 39 4 4 1715.21 132.675 3 39 4 5 1029.46 102.480 3 39 4 6 276.299 61.1573 3 -39 5 -5 5.24438 53.3573 4 -39 5 -4 404.340 83.2188 4 -39 5 -3 2012.60 139.588 4 -39 5 -2 579.471 92.7550 4 -39 5 -1 710.852 91.7386 4 39 5 -1 704.263 102.962 3 39 5 0 52.7533 78.6787 3 39 5 1 590.377 99.1124 3 39 5 2 771.703 106.438 3 39 5 3 2482.63 151.001 3 39 5 4 841.661 96.1584 3 39 5 5 171.639 59.8895 3 -39 6 -5 214.718 53.8033 4 -39 6 -4 684.279 83.9344 4 -39 6 -3 891.547 96.6600 4 -39 6 -2 800.392 92.9046 4 -39 6 -1 735.129 83.7659 4 39 6 0 134.560 64.9052 3 39 6 1 621.626 84.6990 3 39 6 2 572.390 83.3038 3 39 6 3 644.495 81.2376 3 39 6 4 618.606 68.7526 3 -39 7 -4 1157.81 84.3101 4 -39 7 -3 1413.27 97.6555 4 -39 7 -2 305.427 59.4020 4 40 0 -1 809.672 124.022 3 40 0 0 591.748 122.210 3 40 0 1 1116.87 144.290 3 40 0 2 4976.45 231.104 3 40 0 3 888.559 118.933 3 40 0 4 3445.17 174.546 3 40 0 5 1825.41 122.297 3 40 0 6 176.055 54.8154 3 40 -1 -1 884.061 126.078 3 40 1 -1 1115.86 144.025 3 40 -1 0 4974.50 230.881 3 40 1 0 4965.57 241.146 3 40 -1 1 1244.91 141.376 3 40 1 1 1234.59 145.841 3 40 -1 2 210.136 98.7163 3 40 1 2 192.141 102.656 3 40 -1 3 126.748 85.3934 3 40 1 3 80.0609 88.3646 3 40 -1 4 1317.86 119.475 3 40 1 4 1362.54 129.066 3 40 -1 5 410.162 72.7531 3 40 1 5 485.890 87.0193 3 40 1 6 556.945 70.1870 3 40 2 -1-5.02645 100.199 3 40 -2 0 2989.54 181.179 3 40 2 0 2700.69 183.249 3 40 -2 1 179.920 95.2306 3 40 2 1 203.712 106.256 3 40 -2 2 95.3785 84.4269 3 40 2 2 121.442 97.6908 3 40 -2 3 137.243 73.6548 3 40 2 3 113.827 90.9204 3 40 -2 4-14.7726 60.6629 3 40 2 4-13.3125 75.8826 3 40 -2 5 549.914 66.8248 3 40 2 5 669.364 92.4607 3 40 2 6 157.318 54.4136 3 -40 3 -6 399.436 56.9144 4 40 3 -1 73.2374 87.4976 3 40 3 0 219.657 89.2369 3 40 -3 1 320.532 81.8346 3 40 3 1 314.183 99.7328 3 40 -3 2 740.780 96.0050 3 40 3 2 937.737 124.135 3 40 -3 3 200.998 70.5065 3 40 3 3 385.286 98.0780 3 40 -3 4 285.223 57.7759 3 40 3 4 291.330 84.1704 3 40 3 5 320.926 70.4158 3 40 3 6 294.889 55.3783 3 -40 4 -5 608.950 74.2024 4 40 4 0-21.7032 81.5888 3 40 4 1 1117.51 120.936 3 40 -4 2 438.180 65.0642 3 40 4 2 587.203 100.246 3 40 4 3 1677.24 127.275 3 40 4 4 1276.98 109.504 3 40 4 5 624.742 73.0704 3 -40 5 -5 422.874 58.8458 4 -40 5 -4 947.132 88.6162 4 -40 5 -3 227.768 62.4471 4 -40 5 -2 249.871 65.2551 4 -40 5 -1 723.186 78.2605 4 40 5 0 750.580 92.7957 3 40 5 1 610.905 90.5517 3 40 5 2 244.029 74.7149 3 40 5 3 86.0741 59.9822 3 40 5 4 903.854 81.8830 3 -40 6 -3 383.492 60.2673 4 -40 6 -2 345.995 59.0584 4 40 6 1 677.623 74.4077 3 40 6 2 827.730 76.6499 3 41 0 0 73.1986 91.4804 3 41 0 1 15.0007 82.7423 3 41 0 2 47.8029 84.2941 3 41 0 3-56.9614 70.0719 3 41 0 4 59.6988 61.2491 3 41 0 5 7.98373 45.8545 3 41 -1 0 21.9576 82.8330 3 41 1 0 90.4532 87.8863 3 41 -1 1 222.674 87.2850 3 41 1 1 142.058 93.0753 3 41 -1 2 2585.98 155.634 3 41 1 2 2703.98 166.550 3 41 -1 3 644.318 92.7823 3 41 1 3 715.113 102.289 3 41 -1 4 979.892 92.8574 3 41 1 4 1034.28 99.5083 3 41 1 5 62.6247 51.7830 3 41 2 0 186.297 90.1731 3 41 -2 1 253.092 79.4495 3 41 2 1 278.859 94.2385 3 41 -2 2 5592.06 204.238 3 41 2 2 5593.18 218.884 3 41 -2 3 1150.79 101.910 3 41 2 3 1162.98 113.424 3 41 -2 4 990.464 81.8650 3 41 2 4 948.722 96.4736 3 41 2 5 1600.75 101.396 3 -41 3 -5 880.111 75.2511 4 41 3 0 774.166 106.472 3 41 3 1 1030.81 113.694 3 41 -3 2 616.476 79.3499 3 41 3 2 666.986 97.0877 3 41 -3 3 63.3206 42.2845 3 41 3 3 116.104 66.4131 3 41 3 4 589.559 82.6767 3 41 3 5 339.284 58.2042 3 -41 4 -4 46.9284 48.7884 4 -41 4 -3 569.527 73.4069 4 -41 4 -2 306.711 62.1183 4 -41 4 -1 111.788 43.3286 4 41 4 0 345.247 78.5298 3 41 4 1 157.066 71.6358 3 41 4 2 210.753 70.1475 3 41 4 3 495.535 78.3426 3 41 4 4 187.370 52.8681 3 -41 5 -3 646.631 65.8051 4 -41 5 -2 601.347 64.0820 4 41 5 1 606.270 77.8201 3 41 5 2 513.117 69.1146 3 41 5 3 601.871 66.1001 3 42 0 0 4316.79 185.409 3 42 0 1 806.725 103.916 3 42 0 2 305.220 79.2395 3 42 0 3 546.511 76.8292 3 42 0 4 2614.46 120.608 3 42 1 0 857.095 103.720 3 42 -1 1 1826.06 124.032 3 42 1 1 1934.17 136.682 3 42 -1 2 411.333 80.0620 3 42 1 2 260.319 75.8129 3 42 -1 3 916.548 85.5070 3 42 1 3 1034.29 96.2795 3 42 1 4 893.626 79.6375 3 42 2 0 23.1815 65.0092 3 42 2 1 826.137 102.469 3 42 -2 2 219.828 56.8424 3 42 2 2 291.225 73.5019 3 42 -2 3 538.143 63.2393 3 42 2 3 545.607 77.7770 3 42 2 4 600.663 69.7742 3 -42 3 -3 140.000 47.5803 4 -42 3 -2 862.052 75.2576 4 42 3 1 1304.11 107.872 3 42 3 2 1091.96 97.2515 3 42 3 3 79.2148 52.0517 3 42 4 1 744.814 78.3108 3 42 4 2 415.911 63.6905 3 43 0 2-105.181 51.1576 3 43 1 1 411.209 68.5113 3 43 1 2 1645.43 103.102 3 43 2 1 782.761 80.8693 3 43 2 2 411.066 66.2866 3 0 0 0 0.00 0.00 0 TITL MRC1605 in Pna2(1) REM Pna2(1) (#33, found as P2(1)cn in -cba setting) CELL 1.54184 35.218812 15.391399 12.774625 90.0000 90.0000 90.0000 ZERR 4.00 0.000362 0.000164 0.000111 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H N O Mg Cr UNIT 284.00 364.00 16.00 24.00 8.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 7484 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3b _database_code_depnum_ccdc_archive 'CCDC 2116003' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; _audit_creation_method SHELXL-2018/3 _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C64 H84 Mg2 N4 O6 W, C7 H8' _chemical_formula_sum 'C71 H92 Mg2 N4 O6 W' _chemical_formula_weight 1329.95 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -5.4734 5.5774 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.1719 0.1771 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_H-M_alt 'P n a 21' _space_group_name_Hall 'P 2c -2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 35.3464(8) _cell_length_b 15.4039(3) _cell_length_c 12.8690(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 7006.8(3) _cell_formula_units_Z 4 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 5258 _cell_measurement_theta_min 4.2490 _cell_measurement_theta_max 72.8280 _exptl_crystal_description blocks _exptl_crystal_colour Yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.261 _exptl_crystal_F_000 2768 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.272 _exptl_crystal_size_mid 0.156 _exptl_crystal_size_min 0.126 _exptl_absorpt_coefficient_mu 3.624 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type analytical _exptl_absorpt_correction_T_min 0.570 _exptl_absorpt_correction_T_max 0.726 _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'Enhance Ultra (Cu) X-ray Source' _diffrn_measurement_device_type 'Agilent Xcalibur PX Ultra A' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean 10.4115 _diffrn_reflns_number 14631 _diffrn_reflns_av_unetI/netI 0.0577 _diffrn_reflns_av_R_equivalents 0.0341 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 43 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 4.250 _diffrn_reflns_theta_max 73.525 _diffrn_reflns_theta_full 67.684 _diffrn_measured_fraction_theta_max 0.962 _diffrn_measured_fraction_theta_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.962 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.654 _diffrn_reflns_point_group_measured_fraction_full 0.682 _reflns_number_total 9229 _reflns_number_gt 7525 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.299 _reflns_Friedel_fraction_max 0.316 _reflns_Friedel_fraction_full 0.344 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro, Rigaku OD' _computing_cell_refinement 'CrysAlisPro, Rigaku OD' _computing_data_reduction 'CrysAlisPro, Rigaku OD' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2017)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2017)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0549P)^2^+1.4661P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Classical Flack method preferred over Parsons because s.u. lower. ; _refine_ls_abs_structure_Flack -0.042(12) _chemical_absolute_configuration ? _refine_ls_number_reflns 9229 _refine_ls_number_parameters 809 _refine_ls_number_restraints 136 _refine_ls_R_factor_all 0.0570 _refine_ls_R_factor_gt 0.0427 _refine_ls_wR_factor_ref 0.1166 _refine_ls_wR_factor_gt 0.1045 _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_restrained_S_all 1.018 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W1 W 0.32294(2) 0.31724(2) 0.76956(4) 0.04936(11) Uani 1 1 d . . . . . Mg1 Mg 0.36557(6) 0.35164(15) 0.41435(19) 0.0382(5) Uani 1 1 d . . . . . Mg2 Mg 0.39404(6) 0.14593(15) 0.5221(2) 0.0386(5) Uani 1 1 d . . . . . N1 N 0.40263(19) 0.4121(5) 0.3165(6) 0.0402(15) Uani 1 1 d . . . . . C1 C 0.3932(2) 0.4274(6) 0.2178(7) 0.0403(18) Uani 1 1 d . . . . . C2 C 0.3566(2) 0.4147(5) 0.1777(6) 0.0449(17) Uani 1 1 d . . . . . H2A H 0.355006 0.416466 0.103992 0.054 Uiso 1 1 calc R U . . . C3 C 0.3218(2) 0.3997(6) 0.2287(7) 0.043(2) Uani 1 1 d . . . . . N3 N 0.3193(2) 0.3813(5) 0.3303(6) 0.0406(17) Uani 1 1 d . . . . . C4 C 0.4217(3) 0.4651(7) 0.1420(7) 0.060(2) Uani 1 1 d . . . . . H4A H 0.434324 0.417745 0.104756 0.090 Uiso 1 1 calc R U . . . H4B H 0.440543 0.499087 0.180205 0.090 Uiso 1 1 calc R U . . . H4C H 0.408616 0.502612 0.092135 0.090 Uiso 1 1 calc R U . . . C5 C 0.2871(3) 0.4048(9) 0.1612(9) 0.066(3) Uani 1 1 d . . . . . H5A H 0.274233 0.348387 0.160878 0.099 Uiso 1 1 calc R U . . . H5B H 0.294477 0.420123 0.090167 0.099 Uiso 1 1 calc R U . . . H5C H 0.269899 0.449165 0.188650 0.099 Uiso 1 1 calc R U . . . C6 C 0.4398(2) 0.4390(5) 0.3506(6) 0.0405(15) Uani 1 1 d . . . . . C7 C 0.4713(2) 0.3857(5) 0.3283(6) 0.0460(17) Uani 1 1 d . . . . . C8 C 0.5067(2) 0.4157(6) 0.3623(7) 0.0534(19) Uani 1 1 d . . . . . H8A H 0.528608 0.381635 0.348848 0.064 Uiso 1 1 calc R U . . . C9 C 0.5106(3) 0.4936(6) 0.4148(8) 0.063(2) Uani 1 1 d . . . . . H9A H 0.534979 0.513314 0.434931 0.076 Uiso 1 1 calc R U . . . C10 C 0.4797(3) 0.5418(6) 0.4376(7) 0.057(2) Uani 1 1 d . . . . . H10A H 0.482744 0.594389 0.475265 0.068 Uiso 1 1 calc R U . . . C11 C 0.4431(2) 0.5160(5) 0.4069(6) 0.0493(18) Uani 1 1 d . . . . . C12 C 0.46887(18) 0.2985(4) 0.2753(11) 0.0473(15) Uani 1 1 d . . . . . H12A H 0.442721 0.292471 0.246465 0.057 Uiso 1 1 calc R U . . . C13 C 0.4752(2) 0.2255(6) 0.3490(8) 0.056(2) Uani 1 1 d . . . . . H13A H 0.454318 0.223325 0.399112 0.084 Uiso 1 1 calc R U . . . H13B H 0.499081 0.234434 0.386015 0.084 Uiso 1 1 calc R U . . . H13C H 0.476252 0.170743 0.310379 0.084 Uiso 1 1 calc R U . . . C14 C 0.4970(3) 0.2909(8) 0.1836(9) 0.071(3) Uani 1 1 d . . . . . H14A H 0.522810 0.299998 0.208992 0.106 Uiso 1 1 calc R U . . . H14B H 0.490954 0.334940 0.131149 0.106 Uiso 1 1 calc R U . . . H14C H 0.494965 0.233012 0.152545 0.106 Uiso 1 1 calc R U . . . C15 C 0.4090(3) 0.5712(6) 0.4346(8) 0.058(2) Uani 1 1 d . . . . . H15A H 0.386606 0.531696 0.431286 0.070 Uiso 1 1 calc R U . . . C16 C 0.4021(5) 0.6410(9) 0.3558(11) 0.101(5) Uani 1 1 d . . . . . H16A H 0.397776 0.614633 0.287572 0.152 Uiso 1 1 calc R U . . . H16B H 0.424172 0.679401 0.352364 0.152 Uiso 1 1 calc R U . . . H16C H 0.379772 0.674804 0.376069 0.152 Uiso 1 1 calc R U . . . C17 C 0.4103(4) 0.6066(9) 0.5455(9) 0.088(4) Uani 1 1 d . . . . . H17A H 0.427127 0.657008 0.548250 0.133 Uiso 1 1 calc R U . . . H17B H 0.419702 0.561432 0.592530 0.133 Uiso 1 1 calc R U . . . H17C H 0.384751 0.623911 0.566916 0.133 Uiso 1 1 calc R U . . . C18 C 0.2820(2) 0.3864(6) 0.3756(7) 0.0430(19) Uani 1 1 d . . . . . C19 C 0.2698(3) 0.4669(6) 0.4168(8) 0.058(2) Uani 1 1 d . . . . . C20 C 0.2339(3) 0.4718(6) 0.4593(8) 0.063(2) Uani 1 1 d . . . . . H20A H 0.225378 0.525706 0.486515 0.076 Uiso 1 1 calc R U . . . C21 C 0.2099(2) 0.4010(6) 0.4635(8) 0.063(2) Uani 1 1 d . . . . . H21A H 0.185347 0.406339 0.492566 0.075 Uiso 1 1 calc R U . . . C22 C 0.2225(2) 0.3213(6) 0.4243(8) 0.057(2) Uani 1 1 d . . . . . H22A H 0.206274 0.272210 0.427081 0.068 Uiso 1 1 calc R U . . . C23 C 0.2584(2) 0.3131(5) 0.3813(7) 0.0471(17) Uani 1 1 d . . . . . C24 C 0.2951(3) 0.5457(6) 0.4170(11) 0.077(3) Uani 1 1 d . . . . . H24A H 0.321505 0.525734 0.402124 0.093 Uiso 1 1 calc R U . . . C25 C 0.2837(5) 0.6089(7) 0.3312(12) 0.106(5) Uani 1 1 d . . . . . H25A H 0.256304 0.618189 0.333551 0.159 Uiso 1 1 calc R U . . . H25B H 0.290740 0.584609 0.263532 0.159 Uiso 1 1 calc R U . . . H25C H 0.296767 0.664319 0.341551 0.159 Uiso 1 1 calc R U . . . C26 C 0.2957(4) 0.5924(7) 0.5188(14) 0.102(5) Uani 1 1 d . . . . . H26A H 0.307540 0.555477 0.571590 0.153 Uiso 1 1 calc R U . . . H26B H 0.269681 0.605937 0.539922 0.153 Uiso 1 1 calc R U . . . H26C H 0.310108 0.646380 0.511796 0.153 Uiso 1 1 calc R U . . . C27 C 0.2714(2) 0.2256(6) 0.3425(8) 0.056(2) Uani 1 1 d . . . . . H27A H 0.295774 0.234349 0.304280 0.067 Uiso 1 1 calc R U . . . C28 C 0.2792(3) 0.1655(6) 0.4324(9) 0.065(2) Uani 1 1 d . . . . . H28A H 0.255751 0.155399 0.471138 0.098 Uiso 1 1 calc R U . . . H28B H 0.298065 0.191852 0.478432 0.098 Uiso 1 1 calc R U . . . H28C H 0.288883 0.110034 0.406064 0.098 Uiso 1 1 calc R U . . . C29 C 0.2429(3) 0.1847(7) 0.2659(16) 0.082(3) Uani 1 1 d . . . . . H29A H 0.237913 0.225486 0.209053 0.123 Uiso 1 1 calc R U . . . H29B H 0.219233 0.171949 0.302462 0.123 Uiso 1 1 calc R U . . . H29C H 0.253468 0.130879 0.237608 0.123 Uiso 1 1 calc R U . . . N31 N 0.39568(15) 0.0389(4) 0.4299(5) 0.0372(12) Uani 1 1 d . . . . . C31 C 0.42715(19) -0.0095(5) 0.4215(6) 0.0422(16) Uani 1 1 d . . . . . C32 C 0.4610(2) 0.0093(5) 0.4738(7) 0.0508(19) Uani 1 1 d . . . . . H32A H 0.482636 -0.019291 0.446772 0.061 Uiso 1 1 calc R U . . . N33 N 0.44196(17) 0.1166(4) 0.6013(6) 0.0434(14) Uani 1 1 d . . . . . C33 C 0.4680(2) 0.0627(6) 0.5583(7) 0.0522(19) Uani 1 1 d . . . . . C34 C 0.4273(3) -0.0909(6) 0.3559(9) 0.063(2) Uani 1 1 d . . . . . H34A H 0.410995 -0.082550 0.295254 0.094 Uiso 1 1 calc R U . . . H34B H 0.417938 -0.139802 0.397256 0.094 Uiso 1 1 calc R U . . . H34C H 0.453212 -0.103147 0.332816 0.094 Uiso 1 1 calc R U . . . C35 C 0.5069(3) 0.0569(8) 0.6074(10) 0.079(3) Uani 1 1 d . . . . . H35A H 0.504470 0.037715 0.679733 0.119 Uiso 1 1 calc R U . . . H35B H 0.519093 0.114035 0.605531 0.119 Uiso 1 1 calc R U . . . H35C H 0.522409 0.015066 0.568820 0.119 Uiso 1 1 calc R U . . . C36 C 0.36306(19) 0.0114(5) 0.3721(7) 0.0478(18) Uani 1 1 d . . . . . C37 C 0.35717(17) 0.0471(5) 0.2720(10) 0.0501(15) Uani 1 1 d . . . . . C38 C 0.3260(3) 0.0202(8) 0.2131(9) 0.070(3) Uani 1 1 d . . . . . H38A H 0.321842 0.044235 0.146070 0.084 Uiso 1 1 calc R U . . . C39 C 0.3013(3) -0.0412(7) 0.2524(11) 0.075(4) Uani 1 1 d . . . . . H39A H 0.280901 -0.061425 0.210984 0.090 Uiso 1 1 calc R U . . . C40 C 0.3064(3) -0.0738(7) 0.3531(11) 0.074(3) Uani 1 1 d . . . . . H40A H 0.288726 -0.114355 0.380129 0.089 Uiso 1 1 calc R U . . . C41 C 0.3374(2) -0.0476(5) 0.4155(8) 0.054(2) Uani 1 1 d . . . . . C42 C 0.3838(2) 0.1132(6) 0.2251(7) 0.057(2) Uani 1 1 d . . . . . H42A H 0.394515 0.144898 0.286104 0.069 Uiso 1 1 calc R U . . . C43 C 0.3654(4) 0.1823(8) 0.1607(15) 0.100(5) Uani 1 1 d . . . . . H43A H 0.350879 0.221080 0.205916 0.150 Uiso 1 1 calc R U . . . H43B H 0.348445 0.155284 0.109910 0.150 Uiso 1 1 calc R U . . . H43C H 0.384929 0.215634 0.124213 0.150 Uiso 1 1 calc R U . . . C44 C 0.4169(4) 0.0752(8) 0.1728(11) 0.090(4) Uani 1 1 d . . . . . H44A H 0.408479 0.036658 0.116874 0.134 Uiso 1 1 calc R U . . . H44B H 0.431860 0.042020 0.223170 0.134 Uiso 1 1 calc R U . . . H44C H 0.432544 0.121794 0.143528 0.134 Uiso 1 1 calc R U . . . C45 C 0.3414(3) -0.0799(6) 0.5257(10) 0.070(3) Uani 1 1 d . . . . . H45A H 0.366817 -0.060953 0.551443 0.084 Uiso 1 1 calc R U . . . C46 C 0.3399(8) -0.1797(9) 0.5335(17) 0.144(8) Uani 1 1 d . . . . . H46A H 0.346783 -0.205258 0.466381 0.215 Uiso 1 1 calc R U . . . H46B H 0.314210 -0.197885 0.552299 0.215 Uiso 1 1 calc R U . . . H46C H 0.357694 -0.199530 0.586877 0.215 Uiso 1 1 calc R U . . . C47 C 0.3124(4) -0.0408(10) 0.5952(11) 0.091(4) Uani 1 1 d . . . . . H47A H 0.287217 -0.050049 0.565444 0.136 Uiso 1 1 calc R U . . . H47B H 0.317173 0.021587 0.602085 0.136 Uiso 1 1 calc R U . . . H47C H 0.313776 -0.068289 0.663762 0.136 Uiso 1 1 calc R U . . . C48 C 0.4483(2) 0.1446(5) 0.7046(7) 0.0467(18) Uani 1 1 d . . . . . C49 C 0.4352(3) 0.0937(6) 0.7852(10) 0.065(3) Uani 1 1 d . . . . . C50 C 0.4421(4) 0.1211(8) 0.8886(9) 0.081(4) Uani 1 1 d . . . . . H50A H 0.433610 0.086158 0.944755 0.097 Uiso 1 1 calc R U . . . C51 C 0.4606(4) 0.1963(7) 0.9087(8) 0.075(3) Uani 1 1 d . . . . . H51A H 0.465365 0.213469 0.978354 0.090 Uiso 1 1 calc R U . . . C52 C 0.4724(3) 0.2473(7) 0.8281(9) 0.061(3) Uani 1 1 d . . . . . H52A H 0.485013 0.300393 0.842879 0.074 Uiso 1 1 calc R U . . . C53 C 0.4666(3) 0.2240(7) 0.7261(8) 0.053(2) Uani 1 1 d . . . . . C54 C 0.4141(3) 0.0084(6) 0.7680(13) 0.084(3) Uani 1 1 d . . . . . H54A H 0.403823 0.010170 0.695612 0.101 Uiso 1 1 calc R U . . . C55 C 0.4390(4) -0.0698(6) 0.7747(19) 0.112(4) Uani 1 1 d . . . . . H55A H 0.458429 -0.060368 0.827827 0.168 Uiso 1 1 calc R U . . . H55B H 0.451136 -0.079823 0.707325 0.168 Uiso 1 1 calc R U . . . H55C H 0.423720 -0.120573 0.793434 0.168 Uiso 1 1 calc R U . . . C56 C 0.3807(5) -0.0053(10) 0.8397(13) 0.111(5) Uani 1 1 d . . . . . H56A H 0.363089 0.043458 0.832767 0.167 Uiso 1 1 calc R U . . . H56B H 0.389661 -0.008774 0.911692 0.167 Uiso 1 1 calc R U . . . H56C H 0.367819 -0.059411 0.821183 0.167 Uiso 1 1 calc R U . . . C57 C 0.4787(2) 0.2842(6) 0.6390(7) 0.054(2) Uani 1 1 d . . . . . H57A H 0.477760 0.250166 0.572814 0.065 Uiso 1 1 calc R U . . . C58 C 0.4505(4) 0.3578(9) 0.6293(10) 0.086(4) Uani 1 1 d . . . . . H58A H 0.449049 0.389346 0.695312 0.129 Uiso 1 1 calc R U . . . H58B H 0.425513 0.334245 0.612033 0.129 Uiso 1 1 calc R U . . . H58C H 0.458652 0.397580 0.574186 0.129 Uiso 1 1 calc R U . . . C59 C 0.5191(4) 0.3176(8) 0.6519(11) 0.087(4) Uani 1 1 d . . . . . H59A H 0.536903 0.268993 0.646305 0.131 Uiso 1 1 calc R U . . . H59B H 0.521823 0.345062 0.720184 0.131 Uiso 1 1 calc R U . . . H59C H 0.524627 0.360269 0.597409 0.131 Uiso 1 1 calc R U . . . C61 C 0.3430(5) 0.4071(17) 0.6497(14) 0.060(4) Uani 0.55(2) 1 d . U P A 1 H61A H 0.345352 0.465940 0.671090 0.072 Uiso 0.55(2) 1 calc R U P A 1 C61' C 0.3388(6) 0.3614(16) 0.6332(18) 0.051(4) Uiso 0.45(2) 1 d . U P A 2 O61 O 0.35192(17) 0.3923(4) 0.5569(4) 0.0509(13) Uani 1 1 d . . . . . C62 C 0.3473(4) 0.2239(11) 0.6960(13) 0.047(3) Uani 0.55(2) 1 d . U P A 1 C62' C 0.3366(6) 0.1860(16) 0.7136(17) 0.052(4) Uiso 0.45(2) 1 d . U P A 2 H62A H 0.324732 0.139327 0.749167 0.062 Uiso 0.45(2) 1 calc R U P A 2 O62 O 0.35822(15) 0.1656(4) 0.6399(5) 0.0501(13) Uani 1 1 d . . . . . C63 C 0.3076(3) 0.2480(7) 0.8986(8) 0.067(2) Uani 1 1 d . . . . . O63 O 0.2997(3) 0.2091(7) 0.9707(7) 0.111(4) Uani 1 1 d . . . . . C64 C 0.2998(3) 0.4270(7) 0.8324(9) 0.070(3) Uani 1 1 d . . . . . O64 O 0.2869(3) 0.4880(6) 0.8691(10) 0.108(3) Uani 1 1 d . . . . . C65 C 0.2725(3) 0.2870(6) 0.7004(8) 0.064(2) Uani 1 1 d . . . . . O65 O 0.2443(2) 0.2696(6) 0.6625(7) 0.084(2) Uani 1 1 d . . . . . C66 C 0.3731(4) 0.3458(7) 0.8435(8) 0.073(3) Uani 1 1 d . . . . . O66 O 0.4003(2) 0.3656(7) 0.8839(8) 0.095(3) Uani 1 1 d . . . . . C70 C 0.6195(10) 0.371(2) 0.327(3) 0.117(9) Uani 0.511(4) 1 d D U P B 2 H70A H 0.634450 0.424371 0.326694 0.176 Uiso 0.511(4) 1 calc R U P B 2 H70B H 0.628504 0.332248 0.271572 0.176 Uiso 0.511(4) 1 calc R U P B 2 H70C H 0.592811 0.384705 0.315282 0.176 Uiso 0.511(4) 1 calc R U P B 2 C71 C 0.6242(6) 0.3228(13) 0.4379(16) 0.103(8) Uani 0.511(4) 1 d DG U P B 2 C72 C 0.6056(6) 0.2450(13) 0.4573(18) 0.106(7) Uani 0.511(4) 1 d DG U P B 2 H72A H 0.588849 0.221485 0.406872 0.127 Uiso 0.511(4) 1 calc R U P B 2 C73 C 0.6115(7) 0.2015(13) 0.551(2) 0.123(10) Uani 0.511(4) 1 d G U P B 2 H73A H 0.598794 0.148288 0.563845 0.148 Uiso 0.511(4) 1 calc R U P B 2 C74 C 0.6360(7) 0.2359(16) 0.6244(16) 0.116(9) Uani 0.511(4) 1 d G U P B 2 H74A H 0.640015 0.206162 0.688125 0.140 Uiso 0.511(4) 1 calc R U P B 2 C75 C 0.6546(7) 0.3137(17) 0.6050(17) 0.121(9) Uani 0.511(4) 1 d G U P B 2 H75A H 0.671292 0.337233 0.655432 0.146 Uiso 0.511(4) 1 calc R U P B 2 C76 C 0.6487(7) 0.3572(14) 0.5117(19) 0.117(8) Uani 0.511(4) 1 d DG U P B 2 H76A H 0.661348 0.410431 0.498459 0.141 Uiso 0.511(4) 1 calc R U P B 2 C70' C 0.6220(14) 0.195(2) 0.627(3) 0.103(10) Uiso 0.356(4) 1 d D U P C 1 H70D H 0.608248 0.143612 0.601150 0.155 Uiso 0.356(4) 1 calc R U P C 1 H70E H 0.647483 0.177104 0.648529 0.155 Uiso 0.356(4) 1 calc R U P C 1 H70F H 0.608478 0.219584 0.685970 0.155 Uiso 0.356(4) 1 calc R U P C 1 C71' C 0.6251(8) 0.2659(15) 0.5350(18) 0.074(7) Uiso 0.356(4) 1 d DG U P C 1 C72' C 0.6435(10) 0.3444(17) 0.552(2) 0.118(9) Uiso 0.356(4) 1 d DG U P C 1 H72B H 0.654093 0.356708 0.618379 0.142 Uiso 0.356(4) 1 calc R U P C 1 C73' C 0.6465(11) 0.4047(16) 0.472(3) 0.124(12) Uiso 0.356(4) 1 d G U P C 1 H73B H 0.659064 0.458364 0.483953 0.149 Uiso 0.356(4) 1 calc R U P C 1 C74' C 0.6310(10) 0.3867(18) 0.375(2) 0.120(11) Uiso 0.356(4) 1 d G U P C 1 H74B H 0.633055 0.427941 0.320755 0.144 Uiso 0.356(4) 1 calc R U P C 1 C75' C 0.6126(10) 0.308(2) 0.3582(18) 0.104(10) Uiso 0.356(4) 1 d G U P C 1 H75B H 0.602074 0.295863 0.291983 0.124 Uiso 0.356(4) 1 calc R U P C 1 C76' C 0.6097(9) 0.2478(16) 0.438(2) 0.111(9) Uiso 0.356(4) 1 d DG U P C 1 H76B H 0.597102 0.194206 0.426408 0.133 Uiso 0.356(4) 1 calc R U P C 1 C70" C 0.618(3) 0.411(7) 0.294(7) 0.115(15) Uiso 0.133(4) 1 d D U P D 3 H70G H 0.637371 0.456967 0.293765 0.172 Uiso 0.133(4) 1 calc R U P D 3 H70H H 0.621178 0.375298 0.231077 0.172 Uiso 0.133(4) 1 calc R U P D 3 H70I H 0.593019 0.436152 0.295704 0.172 Uiso 0.133(4) 1 calc R U P D 3 C71" C 0.624(3) 0.350(6) 0.395(6) 0.108(10) Uiso 0.133(4) 1 d DG U P D 3 C72" C 0.601(2) 0.280(5) 0.412(6) 0.110(12) Uiso 0.133(4) 1 d DG U P D 3 H72C H 0.582952 0.262779 0.360255 0.132 Uiso 0.133(4) 1 calc R U P D 3 C73" C 0.603(3) 0.234(5) 0.505(7) 0.114(11) Uiso 0.133(4) 1 d G U P D 3 H73C H 0.586376 0.185591 0.516581 0.137 Uiso 0.133(4) 1 calc R U P D 3 C74" C 0.628(3) 0.258(6) 0.581(7) 0.107(13) Uiso 0.133(4) 1 d G U P D 3 H74C H 0.629836 0.227028 0.644465 0.128 Uiso 0.133(4) 1 calc R U P D 3 C75" C 0.652(3) 0.329(7) 0.564(7) 0.117(11) Uiso 0.133(4) 1 d G U P D 3 H75C H 0.669872 0.345654 0.616023 0.140 Uiso 0.133(4) 1 calc R U P D 3 C76" C 0.650(3) 0.375(6) 0.471(8) 0.116(13) Uiso 0.133(4) 1 d DG U P D 3 H76C H 0.666449 0.422843 0.459697 0.140 Uiso 0.133(4) 1 calc R U P D 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W1 0.05926(17) 0.05488(17) 0.03395(15) 0.0007(3) 0.0076(2) 0.01016(14) Mg1 0.0389(11) 0.0424(11) 0.0334(11) 0.0067(10) -0.0029(10) -0.0045(9) Mg2 0.0372(10) 0.0373(11) 0.0412(12) -0.0052(10) -0.0068(10) 0.0027(9) N1 0.041(3) 0.046(4) 0.033(3) 0.000(3) -0.003(3) -0.006(3) C1 0.043(4) 0.048(4) 0.030(4) 0.005(3) 0.006(3) -0.005(3) C2 0.048(4) 0.061(5) 0.025(3) 0.004(3) -0.003(3) -0.002(3) C3 0.043(4) 0.053(5) 0.034(4) 0.010(4) 0.000(3) 0.007(3) N3 0.044(3) 0.045(4) 0.033(4) 0.008(3) 0.000(3) 0.004(3) C4 0.053(4) 0.087(7) 0.040(4) 0.019(5) 0.003(4) -0.013(5) C5 0.045(5) 0.102(8) 0.050(6) 0.009(6) -0.002(4) 0.002(5) C6 0.047(4) 0.044(4) 0.030(3) 0.006(3) -0.007(3) -0.008(3) C7 0.041(4) 0.058(4) 0.039(4) 0.005(3) -0.004(3) -0.009(3) C8 0.050(4) 0.062(5) 0.048(5) 0.000(4) -0.010(4) -0.009(4) C9 0.064(5) 0.071(6) 0.054(5) 0.011(5) -0.016(4) -0.035(5) C10 0.064(5) 0.051(4) 0.054(5) 0.001(4) -0.007(4) -0.020(4) C11 0.057(4) 0.050(4) 0.041(4) 0.010(4) -0.004(4) -0.015(3) C12 0.044(3) 0.061(4) 0.036(3) -0.006(5) -0.001(5) -0.005(3) C13 0.050(4) 0.059(5) 0.059(5) 0.003(4) 0.002(4) -0.003(4) C14 0.067(6) 0.089(7) 0.055(6) -0.007(5) 0.012(5) -0.004(5) C15 0.072(5) 0.047(4) 0.056(5) -0.005(4) 0.005(4) -0.011(4) C16 0.128(11) 0.104(9) 0.071(8) 0.024(7) 0.017(8) 0.049(9) C17 0.103(8) 0.098(9) 0.064(7) -0.022(6) -0.008(6) 0.022(7) C18 0.036(4) 0.060(5) 0.033(4) -0.006(4) 0.002(3) 0.007(3) C19 0.060(5) 0.052(5) 0.060(5) 0.007(4) 0.011(4) 0.015(4) C20 0.060(5) 0.060(5) 0.070(6) 0.011(5) 0.020(5) 0.020(4) C21 0.049(4) 0.069(6) 0.069(6) 0.005(5) 0.019(4) 0.016(4) C22 0.046(4) 0.064(5) 0.061(5) 0.006(5) 0.004(4) 0.001(4) C23 0.043(4) 0.054(4) 0.045(4) 0.002(4) 0.002(3) 0.002(3) C24 0.075(6) 0.051(5) 0.107(9) 0.005(6) 0.029(6) 0.007(4) C25 0.147(13) 0.057(6) 0.114(11) 0.025(7) 0.060(10) -0.002(7) C26 0.101(9) 0.058(6) 0.147(14) -0.023(8) 0.005(9) -0.003(6) C27 0.044(4) 0.057(5) 0.067(6) -0.013(4) 0.006(4) -0.008(3) C28 0.065(5) 0.051(5) 0.079(7) -0.010(5) 0.001(5) 0.008(4) C29 0.078(5) 0.087(6) 0.081(7) -0.017(8) -0.030(9) -0.006(5) N31 0.034(3) 0.040(3) 0.038(3) -0.003(3) 0.001(2) -0.001(2) C31 0.038(3) 0.044(4) 0.045(4) -0.005(3) 0.004(3) 0.009(3) C32 0.043(4) 0.050(4) 0.059(5) -0.008(4) -0.001(4) 0.010(3) N33 0.041(3) 0.046(3) 0.042(4) 0.000(3) -0.008(3) 0.006(3) C33 0.042(4) 0.059(5) 0.056(5) 0.005(4) -0.006(4) 0.014(3) C34 0.063(5) 0.048(5) 0.077(7) -0.024(5) 0.002(5) 0.014(4) C35 0.055(5) 0.098(8) 0.084(8) -0.012(7) -0.027(5) 0.016(5) C36 0.034(3) 0.044(4) 0.065(5) -0.015(4) 0.013(3) -0.004(3) C37 0.038(3) 0.067(4) 0.045(3) -0.015(6) -0.002(5) 0.003(3) C38 0.052(5) 0.096(7) 0.061(6) -0.022(5) -0.011(4) -0.004(5) C39 0.052(4) 0.080(6) 0.094(12) -0.028(7) -0.013(5) -0.016(4) C40 0.062(5) 0.051(5) 0.110(10) -0.016(6) 0.008(6) -0.012(4) C41 0.038(3) 0.040(4) 0.086(7) -0.021(4) 0.011(4) -0.005(3) C42 0.052(4) 0.079(6) 0.041(4) -0.005(4) 0.009(4) 0.004(4) C43 0.080(7) 0.084(8) 0.135(13) 0.024(9) -0.003(8) 0.020(6) C44 0.086(8) 0.092(8) 0.091(9) 0.008(7) 0.040(7) 0.011(6) C45 0.065(5) 0.044(4) 0.101(8) 0.004(5) 0.026(6) -0.006(4) C46 0.23(2) 0.073(8) 0.126(16) 0.003(10) 0.070(17) 0.009(11) C47 0.079(7) 0.117(10) 0.077(8) -0.007(8) 0.023(6) 0.009(7) C48 0.051(4) 0.048(4) 0.041(4) 0.003(4) -0.018(4) 0.003(3) C49 0.076(5) 0.062(5) 0.057(7) 0.017(5) -0.017(5) -0.003(4) C50 0.111(9) 0.086(8) 0.045(6) 0.022(6) -0.012(6) -0.005(7) C51 0.110(8) 0.076(7) 0.040(5) 0.004(5) -0.017(5) -0.004(6) C52 0.077(6) 0.063(6) 0.044(5) -0.001(5) -0.015(5) -0.005(5) C53 0.058(5) 0.058(5) 0.042(4) 0.000(4) -0.015(4) 0.001(4) C54 0.120(8) 0.068(5) 0.065(6) 0.031(8) -0.019(9) -0.017(5) C55 0.153(11) 0.061(5) 0.123(11) 0.003(12) -0.009(17) 0.001(6) C56 0.128(12) 0.100(10) 0.106(11) 0.029(9) 0.008(10) -0.027(9) C57 0.054(4) 0.067(5) 0.041(4) 0.003(4) -0.007(4) -0.017(4) C58 0.083(7) 0.109(9) 0.066(7) 0.043(7) 0.000(6) 0.006(7) C59 0.081(7) 0.107(9) 0.074(8) 0.003(7) -0.004(6) -0.028(7) C61 0.062(7) 0.073(9) 0.044(7) -0.008(7) -0.002(6) 0.002(7) O61 0.064(3) 0.058(3) 0.031(3) 0.001(2) 0.009(2) 0.003(3) C62 0.039(6) 0.051(7) 0.052(7) 0.015(6) -0.004(5) -0.017(6) O62 0.047(3) 0.059(3) 0.044(3) -0.006(3) 0.010(2) 0.013(2) C63 0.078(6) 0.075(6) 0.048(5) 0.001(5) -0.001(5) -0.018(5) O63 0.145(9) 0.128(8) 0.060(5) 0.037(5) -0.026(5) -0.067(7) C64 0.059(5) 0.077(6) 0.073(7) -0.001(6) -0.007(5) 0.002(5) O64 0.098(6) 0.082(5) 0.143(9) -0.049(6) -0.007(6) 0.035(5) C65 0.085(7) 0.059(5) 0.048(5) -0.006(4) 0.000(5) 0.013(5) O65 0.083(5) 0.098(6) 0.071(5) -0.011(5) -0.016(4) 0.000(4) C66 0.094(8) 0.074(6) 0.050(5) -0.002(5) 0.011(6) 0.016(6) O66 0.071(5) 0.130(7) 0.086(6) -0.021(6) -0.014(5) -0.003(5) C70 0.118(13) 0.124(14) 0.111(14) 0.013(12) -0.010(12) 0.004(12) C71 0.074(12) 0.110(16) 0.127(18) -0.011(15) 0.005(13) -0.025(12) C72 0.108(12) 0.104(12) 0.106(13) -0.012(11) 0.000(11) -0.023(11) C73 0.109(17) 0.117(17) 0.14(2) -0.017(17) 0.017(17) 0.017(15) C74 0.110(14) 0.124(15) 0.115(15) -0.003(14) 0.010(13) 0.036(13) C75 0.116(14) 0.131(15) 0.117(16) -0.011(14) 0.007(13) 0.025(13) C76 0.117(12) 0.119(12) 0.116(13) -0.008(11) -0.003(11) 0.005(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag W1 C62 1.924(17) . ? W1 C61' 1.96(2) . ? W1 C64 2.046(11) . ? W1 C65 2.046(12) . ? W1 C63 2.047(10) . ? W1 C66 2.062(14) . ? W1 C61 2.19(2) . ? W1 C62' 2.20(2) . ? Mg1 O61 1.998(6) . ? Mg1 N3 2.012(7) . ? Mg1 N1 2.042(7) . ? Mg1 Mg2 3.602(3) . ? Mg2 O62 1.998(6) . ? Mg2 N33 2.027(7) . ? Mg2 N31 2.032(6) . ? N1 C1 1.334(9) . ? N1 C6 1.444(10) . ? C1 C2 1.407(11) . ? C1 C4 1.518(11) . ? C2 C3 1.414(12) . ? C3 N3 1.340(10) . ? C3 C5 1.505(13) . ? N3 C18 1.446(11) . ? C6 C11 1.395(11) . ? C6 C7 1.415(11) . ? C7 C8 1.404(11) . ? C7 C12 1.509(12) . ? C8 C9 1.385(13) . ? C9 C10 1.352(14) . ? C10 C11 1.410(12) . ? C11 C15 1.517(13) . ? C12 C13 1.488(14) . ? C12 C14 1.547(15) . ? C15 C16 1.498(15) . ? C15 C17 1.529(14) . ? C18 C23 1.404(12) . ? C18 C19 1.415(13) . ? C19 C20 1.387(13) . ? C19 C24 1.507(14) . ? C20 C21 1.381(14) . ? C21 C22 1.399(13) . ? C22 C23 1.392(12) . ? C23 C27 1.509(12) . ? C24 C26 1.50(2) . ? C24 C25 1.525(18) . ? C27 C28 1.507(15) . ? C27 C29 1.544(15) . ? N31 C31 1.344(9) . ? N31 C36 1.436(10) . ? C31 C32 1.402(11) . ? C31 C34 1.511(11) . ? C32 C33 1.386(13) . ? N33 C33 1.359(10) . ? N33 C48 1.415(11) . ? C33 C35 1.516(12) . ? C36 C41 1.401(11) . ? C36 C37 1.416(16) . ? C37 C38 1.399(12) . ? C37 C42 1.512(13) . ? C38 C39 1.383(15) . ? C39 C40 1.402(19) . ? C40 C41 1.415(15) . ? C41 C45 1.509(16) . ? C42 C44 1.472(13) . ? C42 C43 1.497(15) . ? C45 C47 1.488(15) . ? C45 C46 1.542(16) . ? C48 C49 1.379(14) . ? C48 C53 1.411(13) . ? C49 C50 1.417(17) . ? C49 C54 1.527(13) . ? C50 C51 1.356(16) . ? C51 C52 1.366(15) . ? C52 C53 1.376(12) . ? C53 C57 1.516(13) . ? C54 C55 1.495(16) . ? C54 C56 1.51(2) . ? C57 C58 1.516(15) . ? C57 C59 1.529(14) . ? C61 O61 1.256(19) . ? C61' O61 1.19(2) . ? C62 O62 1.217(18) . ? C62' O62 1.26(2) . ? C63 O63 1.139(13) . ? C64 O64 1.146(13) . ? C65 O65 1.143(13) . ? C66 O66 1.133(15) . ? C70 C71 1.62(3) . ? C71 C72 1.3900 . ? C71 C76 1.3900 . ? C72 C73 1.3900 . ? C73 C74 1.3900 . ? C74 C75 1.3900 . ? C75 C76 1.3900 . ? C70' C71' 1.62(3) . ? C71' C72' 1.3900 . ? C71' C76' 1.3900 . ? C72' C73' 1.3900 . ? C73' C74' 1.3900 . ? C74' C75' 1.3900 . ? C75' C76' 1.3900 . ? C70" C71" 1.62(3) . ? C71" C72" 1.3900 . ? C71" C76" 1.3900 . ? C72" C73" 1.3900 . ? C73" C74" 1.3900 . ? C74" C75" 1.3900 . ? C75" C76" 1.3900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C62 W1 C64 172.3(6) . . ? C61' W1 C64 100.4(8) . . ? C62 W1 C65 90.3(5) . . ? C61' W1 C65 86.5(7) . . ? C64 W1 C65 90.7(4) . . ? C62 W1 C63 97.4(6) . . ? C61' W1 C63 168.9(8) . . ? C64 W1 C63 90.2(5) . . ? C65 W1 C63 90.2(4) . . ? C62 W1 C66 90.1(5) . . ? C61' W1 C66 95.3(7) . . ? C64 W1 C66 89.2(4) . . ? C65 W1 C66 178.2(4) . . ? C63 W1 C66 88.0(4) . . ? C62 W1 C61 88.9(7) . . ? C64 W1 C61 83.4(7) . . ? C65 W1 C61 96.9(6) . . ? C63 W1 C61 170.5(6) . . ? C66 W1 C61 84.9(6) . . ? C61' W1 C62' 87.9(9) . . ? C64 W1 C62' 167.7(8) . . ? C65 W1 C62' 80.7(6) . . ? C63 W1 C62' 81.1(8) . . ? C66 W1 C62' 99.2(6) . . ? O61 Mg1 N3 103.1(3) . . ? O61 Mg1 N1 125.3(3) . . ? N3 Mg1 N1 94.9(3) . . ? O61 Mg1 Mg2 89.41(19) . . ? N3 Mg1 Mg2 129.3(2) . . ? N1 Mg1 Mg2 117.3(2) . . ? O62 Mg2 N33 100.5(3) . . ? O62 Mg2 N31 125.7(3) . . ? N33 Mg2 N31 95.1(3) . . ? O62 Mg2 Mg1 88.94(18) . . ? N33 Mg2 Mg1 128.5(2) . . ? N31 Mg2 Mg1 119.8(2) . . ? C1 N1 C6 117.8(7) . . ? C1 N1 Mg1 120.5(6) . . ? C6 N1 Mg1 121.7(5) . . ? N1 C1 C2 123.7(8) . . ? N1 C1 C4 120.9(8) . . ? C2 C1 C4 115.3(7) . . ? C1 C2 C3 130.7(7) . . ? N3 C3 C2 122.9(8) . . ? N3 C3 C5 121.5(9) . . ? C2 C3 C5 115.6(8) . . ? C3 N3 C18 116.1(8) . . ? C3 N3 Mg1 121.3(7) . . ? C18 N3 Mg1 122.5(6) . . ? C11 C6 C7 122.1(7) . . ? C11 C6 N1 118.6(7) . . ? C7 C6 N1 119.2(7) . . ? C8 C7 C6 116.7(8) . . ? C8 C7 C12 119.0(7) . . ? C6 C7 C12 124.2(6) . . ? C9 C8 C7 121.7(9) . . ? C10 C9 C8 120.2(8) . . ? C9 C10 C11 121.7(8) . . ? C6 C11 C10 117.6(8) . . ? C6 C11 C15 122.1(7) . . ? C10 C11 C15 120.3(8) . . ? C13 C12 C7 112.0(10) . . ? C13 C12 C14 109.4(7) . . ? C7 C12 C14 112.1(7) . . ? C16 C15 C11 112.0(8) . . ? C16 C15 C17 112.3(9) . . ? C11 C15 C17 113.4(9) . . ? C23 C18 C19 120.4(8) . . ? C23 C18 N3 121.2(8) . . ? C19 C18 N3 118.4(8) . . ? C20 C19 C18 118.2(9) . . ? C20 C19 C24 120.0(9) . . ? C18 C19 C24 121.8(8) . . ? C21 C20 C19 122.3(9) . . ? C20 C21 C22 119.0(8) . . ? C23 C22 C21 120.8(8) . . ? C22 C23 C18 119.2(8) . . ? C22 C23 C27 119.4(8) . . ? C18 C23 C27 121.4(7) . . ? C26 C24 C19 113.3(10) . . ? C26 C24 C25 109.3(10) . . ? C19 C24 C25 110.8(11) . . ? C28 C27 C23 110.5(8) . . ? C28 C27 C29 111.0(9) . . ? C23 C27 C29 112.1(8) . . ? C31 N31 C36 117.3(6) . . ? C31 N31 Mg2 121.4(5) . . ? C36 N31 Mg2 121.3(4) . . ? N31 C31 C32 123.5(7) . . ? N31 C31 C34 120.6(7) . . ? C32 C31 C34 115.9(7) . . ? C33 C32 C31 130.8(7) . . ? C33 N33 C48 117.5(7) . . ? C33 N33 Mg2 119.9(6) . . ? C48 N33 Mg2 122.4(5) . . ? N33 C33 C32 124.0(7) . . ? N33 C33 C35 118.8(9) . . ? C32 C33 C35 117.1(8) . . ? C41 C36 C37 121.3(8) . . ? C41 C36 N31 120.4(8) . . ? C37 C36 N31 118.3(6) . . ? C38 C37 C36 119.6(9) . . ? C38 C37 C42 118.2(11) . . ? C36 C37 C42 122.2(7) . . ? C39 C38 C37 120.0(11) . . ? C38 C39 C40 120.1(9) . . ? C39 C40 C41 121.5(9) . . ? C36 C41 C40 117.4(10) . . ? C36 C41 C45 121.8(8) . . ? C40 C41 C45 120.8(9) . . ? C44 C42 C43 112.0(10) . . ? C44 C42 C37 114.2(8) . . ? C43 C42 C37 115.5(9) . . ? C47 C45 C41 111.5(9) . . ? C47 C45 C46 109.8(12) . . ? C41 C45 C46 112.7(12) . . ? C49 C48 C53 120.0(9) . . ? C49 C48 N33 118.7(8) . . ? C53 C48 N33 121.3(8) . . ? C48 C49 C50 118.6(10) . . ? C48 C49 C54 123.0(11) . . ? C50 C49 C54 118.4(11) . . ? C51 C50 C49 121.1(11) . . ? C50 C51 C52 119.6(10) . . ? C51 C52 C53 121.9(10) . . ? C52 C53 C48 118.7(9) . . ? C52 C53 C57 120.3(10) . . ? C48 C53 C57 121.0(8) . . ? C55 C54 C56 108.1(12) . . ? C55 C54 C49 113.4(10) . . ? C56 C54 C49 114.4(13) . . ? C53 C57 C58 109.5(8) . . ? C53 C57 C59 112.9(8) . . ? C58 C57 C59 111.8(9) . . ? O61 C61 W1 129.4(17) . . ? O61 C61' W1 172.2(18) . . ? C61' O61 Mg1 136.8(14) . . ? C61 O61 Mg1 172.2(13) . . ? O62 C62 W1 170.5(11) . . ? O62 C62' W1 127.6(19) . . ? C62 O62 Mg2 139.8(9) . . ? C62' O62 Mg2 174.2(14) . . ? O63 C63 W1 178.8(12) . . ? O64 C64 W1 179.0(11) . . ? O65 C65 W1 179.4(11) . . ? O66 C66 W1 176.8(11) . . ? C72 C71 C76 120.0 . . ? C72 C71 C70 120.3(8) . . ? C76 C71 C70 119.5(8) . . ? C73 C72 C71 120.0 . . ? C72 C73 C74 120.0 . . ? C75 C74 C73 120.0 . . ? C74 C75 C76 120.0 . . ? C75 C76 C71 120.0 . . ? C72' C71' C76' 120.0 . . ? C72' C71' C70' 120.5(9) . . ? C76' C71' C70' 119.5(9) . . ? C73' C72' C71' 120.0 . . ? C74' C73' C72' 120.0 . . ? C73' C74' C75' 120.0 . . ? C76' C75' C74' 120.0 . . ? C75' C76' C71' 120.0 . . ? C72" C71" C76" 120.0 . . ? C72" C71" C70" 119.8(11) . . ? C76" C71" C70" 119.7(11) . . ? C73" C72" C71" 120.0 . . ? C74" C73" C72" 120.0 . . ? C75" C74" C73" 120.0 . . ? C76" C75" C74" 120.0 . . ? C75" C76" C71" 120.0 . . ? _refine_diff_density_max 1.698 _refine_diff_density_min -0.836 _refine_diff_density_rms 0.069 _shelx_res_file ; TITL MRC2109 in Pna2(1) MRC2109.res created by SHELXL-2018/3 at 10:03:28 on 30-Jun-2021 REM Pna2(1) (#33, found as P2(1)cn in -cba setting) REM JMP067 CELL 1.54184 35.346350 15.403868 12.868979 90.0000 90.0000 90.0000 ZERR 4.00 0.000806 0.000343 0.000250 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H W Mg N O UNIT 284 368 4 8 16 24 TEMP -100 L.S. 6 OMIT 19 11 10 OMIT 17 11 10 OMIT 5 10 12 OMIT 7 10 12 OMIT 6 10 12 FMAP 2 PLAN 10 ACTA REM 'C64 H84 Mg2 N4 O6 W, C7 H8' REM C71 H92 Mg2 N4 O6 W SIMU 0.01 0.01 1 C61 C61' SIMU 0.01 0.01 1 C62 C62' REM Modelled as mixed CO/CHO species, so disorders at C61 and C62 linked SADI C70 C71 C70' C71' C70" C71" SADI C70 C72 C70 C76 C70' C72' C70' C76' C70" C72" C70" C76" SIMU 0.02 0.02 1 C70 > C76" SUMP 1 0 1 3 1 4 1 5 REM When refined freely, H1 thermal parameter goes negative REM When set to -1.5 it moves away from the "correct" site, and a new Q peak REM arises in the old position. REM So, it was omitted entirely as unreliable. REM So, asu 1H low, and UNIT 4H low. REM RTAB MgH MG1 H1 REM RTAB MgH MG2 H1 REM RTAB MHM MG1 H1 MG2 WGHT 0.054900 1.466100 FVAR 1.95447 0.55296 0.51073 0.35612 0.13316 W1 3 0.322937 0.317239 0.769559 11.00000 0.05926 0.05488 = 0.03395 0.00073 0.00757 0.01016 MG1 4 0.365570 0.351645 0.414346 11.00000 0.03894 0.04243 = 0.03336 0.00670 -0.00287 -0.00448 MG2 4 0.394044 0.145929 0.522109 11.00000 0.03721 0.03735 = 0.04121 -0.00518 -0.00678 0.00270 REM H1 2 0.382579 0.242776 0.448924 11.00000 -1.50000 N1 5 0.402629 0.412072 0.316470 11.00000 0.04119 0.04606 = 0.03327 -0.00046 -0.00343 -0.00615 C1 1 0.393176 0.427444 0.217846 11.00000 0.04300 0.04808 = 0.02995 0.00496 0.00567 -0.00508 C2 1 0.356588 0.414688 0.177654 11.00000 0.04849 0.06118 = 0.02494 0.00433 -0.00300 -0.00205 AFIX 43 H2A 2 0.355006 0.416466 0.103992 11.00000 -1.20000 AFIX 0 C3 1 0.321766 0.399655 0.228704 11.00000 0.04270 0.05277 = 0.03394 0.00994 0.00035 0.00682 N3 5 0.319336 0.381290 0.330296 11.00000 0.04357 0.04543 = 0.03278 0.00803 -0.00046 0.00391 C4 1 0.421691 0.465053 0.142019 11.00000 0.05308 0.08730 = 0.04026 0.01923 0.00327 -0.01290 AFIX 137 H4A 2 0.434324 0.417745 0.104756 11.00000 -1.50000 H4B 2 0.440543 0.499087 0.180205 11.00000 -1.50000 H4C 2 0.408616 0.502612 0.092135 11.00000 -1.50000 AFIX 0 C5 1 0.287068 0.404779 0.161215 11.00000 0.04502 0.10235 = 0.04996 0.00871 -0.00179 0.00159 AFIX 137 H5A 2 0.274233 0.348387 0.160878 11.00000 -1.50000 H5B 2 0.294477 0.420123 0.090167 11.00000 -1.50000 H5C 2 0.269899 0.449165 0.188650 11.00000 -1.50000 AFIX 0 C6 1 0.439753 0.438961 0.350603 11.00000 0.04658 0.04442 = 0.03044 0.00649 -0.00745 -0.00837 C7 1 0.471321 0.385657 0.328350 11.00000 0.04136 0.05800 = 0.03863 0.00540 -0.00369 -0.00896 C8 1 0.506733 0.415666 0.362277 11.00000 0.04979 0.06222 = 0.04823 0.00044 -0.01040 -0.00865 AFIX 43 H8A 2 0.528608 0.381635 0.348848 11.00000 -1.20000 AFIX 0 C9 1 0.510580 0.493638 0.414835 11.00000 0.06392 0.07063 = 0.05426 0.01129 -0.01552 -0.03492 AFIX 43 H9A 2 0.534979 0.513314 0.434931 11.00000 -1.20000 AFIX 0 C10 1 0.479707 0.541805 0.437604 11.00000 0.06421 0.05137 = 0.05444 0.00106 -0.00653 -0.01983 AFIX 43 H10A 2 0.482744 0.594389 0.475265 11.00000 -1.20000 AFIX 0 C11 1 0.443106 0.515973 0.406870 11.00000 0.05728 0.04981 = 0.04074 0.00953 -0.00408 -0.01472 C12 1 0.468867 0.298530 0.275252 11.00000 0.04441 0.06108 = 0.03630 -0.00573 -0.00138 -0.00478 AFIX 13 H12A 2 0.442721 0.292471 0.246465 11.00000 -1.20000 AFIX 0 C13 1 0.475167 0.225526 0.348983 11.00000 0.05036 0.05905 = 0.05867 0.00341 0.00212 -0.00264 AFIX 137 H13A 2 0.454318 0.223325 0.399112 11.00000 -1.50000 H13B 2 0.499081 0.234434 0.386015 11.00000 -1.50000 H13C 2 0.476252 0.170743 0.310379 11.00000 -1.50000 AFIX 0 C14 1 0.496973 0.290923 0.183588 11.00000 0.06736 0.08937 = 0.05495 -0.00650 0.01154 -0.00359 AFIX 137 H14A 2 0.522810 0.299998 0.208992 11.00000 -1.50000 H14B 2 0.490954 0.334940 0.131149 11.00000 -1.50000 H14C 2 0.494965 0.233012 0.152545 11.00000 -1.50000 AFIX 0 C15 1 0.409032 0.571178 0.434552 11.00000 0.07164 0.04659 = 0.05577 -0.00535 0.00476 -0.01055 AFIX 13 H15A 2 0.386606 0.531696 0.431286 11.00000 -1.20000 AFIX 0 C16 1 0.402087 0.641046 0.355831 11.00000 0.12840 0.10394 = 0.07073 0.02384 0.01703 0.04907 AFIX 137 H16A 2 0.397776 0.614633 0.287572 11.00000 -1.50000 H16B 2 0.424172 0.679401 0.352364 11.00000 -1.50000 H16C 2 0.379772 0.674804 0.376069 11.00000 -1.50000 AFIX 0 C17 1 0.410264 0.606559 0.545526 11.00000 0.10301 0.09801 = 0.06419 -0.02245 -0.00816 0.02210 AFIX 137 H17A 2 0.427127 0.657008 0.548250 11.00000 -1.50000 H17B 2 0.419702 0.561432 0.592530 11.00000 -1.50000 H17C 2 0.384751 0.623911 0.566916 11.00000 -1.50000 AFIX 0 C18 1 0.281967 0.386421 0.375576 11.00000 0.03569 0.06033 = 0.03310 -0.00561 0.00239 0.00742 C19 1 0.269850 0.466922 0.416781 11.00000 0.05994 0.05227 = 0.06042 0.00658 0.01113 0.01508 C20 1 0.233868 0.471785 0.459311 11.00000 0.06041 0.05954 = 0.07025 0.01096 0.02028 0.02046 AFIX 43 H20A 2 0.225378 0.525706 0.486515 11.00000 -1.20000 AFIX 0 C21 1 0.209945 0.401016 0.463511 11.00000 0.04931 0.06947 = 0.06940 0.00534 0.01935 0.01626 AFIX 43 H21A 2 0.185347 0.406339 0.492566 11.00000 -1.20000 AFIX 0 C22 1 0.222498 0.321325 0.424301 11.00000 0.04593 0.06395 = 0.06053 0.00557 0.00411 0.00057 AFIX 43 H22A 2 0.206274 0.272210 0.427081 11.00000 -1.20000 AFIX 0 C23 1 0.258447 0.313106 0.381283 11.00000 0.04291 0.05382 = 0.04466 0.00202 0.00200 0.00163 C24 1 0.295138 0.545719 0.417003 11.00000 0.07464 0.05076 = 0.10709 0.00516 0.02924 0.00695 AFIX 13 H24A 2 0.321505 0.525734 0.402124 11.00000 -1.20000 AFIX 0 C25 1 0.283716 0.608852 0.331244 11.00000 0.14698 0.05657 = 0.11404 0.02538 0.05984 -0.00153 AFIX 137 H25A 2 0.256304 0.618189 0.333551 11.00000 -1.50000 H25B 2 0.290740 0.584609 0.263532 11.00000 -1.50000 H25C 2 0.296767 0.664319 0.341551 11.00000 -1.50000 AFIX 0 C26 1 0.295662 0.592398 0.518849 11.00000 0.10097 0.05796 = 0.14706 -0.02305 0.00490 -0.00316 AFIX 137 H26A 2 0.307540 0.555477 0.571590 11.00000 -1.50000 H26B 2 0.269681 0.605937 0.539922 11.00000 -1.50000 H26C 2 0.310108 0.646380 0.511796 11.00000 -1.50000 AFIX 0 C27 1 0.271434 0.225567 0.342468 11.00000 0.04437 0.05694 = 0.06679 -0.01318 0.00604 -0.00804 AFIX 13 H27A 2 0.295774 0.234349 0.304280 11.00000 -1.20000 AFIX 0 C28 1 0.279214 0.165455 0.432390 11.00000 0.06528 0.05090 = 0.07899 -0.01032 0.00123 0.00787 AFIX 137 H28A 2 0.255751 0.155399 0.471138 11.00000 -1.50000 H28B 2 0.298065 0.191852 0.478432 11.00000 -1.50000 H28C 2 0.288883 0.110034 0.406064 11.00000 -1.50000 AFIX 0 C29 1 0.242908 0.184744 0.265909 11.00000 0.07767 0.08653 = 0.08102 -0.01665 -0.02996 -0.00586 AFIX 137 H29A 2 0.237913 0.225486 0.209053 11.00000 -1.50000 H29B 2 0.219233 0.171949 0.302462 11.00000 -1.50000 H29C 2 0.253468 0.130879 0.237608 11.00000 -1.50000 AFIX 0 N31 5 0.395679 0.038903 0.429858 11.00000 0.03404 0.03982 = 0.03769 -0.00348 0.00123 -0.00079 C31 1 0.427151 -0.009537 0.421476 11.00000 0.03782 0.04360 = 0.04513 -0.00483 0.00394 0.00886 C32 1 0.460950 0.009326 0.473761 11.00000 0.04342 0.04956 = 0.05948 -0.00822 -0.00118 0.00998 AFIX 43 H32A 2 0.482636 -0.019291 0.446772 11.00000 -1.20000 AFIX 0 N33 5 0.441959 0.116648 0.601310 11.00000 0.04144 0.04623 = 0.04250 -0.00049 -0.00801 0.00559 C33 1 0.468050 0.062738 0.558258 11.00000 0.04192 0.05872 = 0.05583 0.00518 -0.00636 0.01374 C34 1 0.427341 -0.090905 0.355945 11.00000 0.06300 0.04811 = 0.07737 -0.02419 0.00158 0.01447 AFIX 137 H34A 2 0.410995 -0.082550 0.295254 11.00000 -1.50000 H34B 2 0.417938 -0.139802 0.397256 11.00000 -1.50000 H34C 2 0.453212 -0.103147 0.332816 11.00000 -1.50000 AFIX 0 C35 1 0.506944 0.056870 0.607433 11.00000 0.05512 0.09816 = 0.08430 -0.01228 -0.02700 0.01561 AFIX 137 H35A 2 0.504470 0.037715 0.679733 11.00000 -1.50000 H35B 2 0.519093 0.114035 0.605531 11.00000 -1.50000 H35C 2 0.522409 0.015066 0.568820 11.00000 -1.50000 AFIX 0 C36 1 0.363061 0.011354 0.372107 11.00000 0.03361 0.04446 = 0.06531 -0.01484 0.01266 -0.00358 C37 1 0.357169 0.047054 0.271997 11.00000 0.03839 0.06661 = 0.04535 -0.01521 -0.00247 0.00310 C38 1 0.326035 0.020229 0.213087 11.00000 0.05178 0.09628 = 0.06124 -0.02208 -0.01136 -0.00410 AFIX 43 H38A 2 0.321842 0.044235 0.146070 11.00000 -1.20000 AFIX 0 C39 1 0.301346 -0.041243 0.252368 11.00000 0.05227 0.07972 = 0.09407 -0.02774 -0.01295 -0.01631 AFIX 43 H39A 2 0.280901 -0.061425 0.210984 11.00000 -1.20000 AFIX 0 C40 1 0.306435 -0.073817 0.353129 11.00000 0.06179 0.05107 = 0.11005 -0.01611 0.00768 -0.01225 AFIX 43 H40A 2 0.288726 -0.114355 0.380129 11.00000 -1.20000 AFIX 0 C41 1 0.337374 -0.047637 0.415504 11.00000 0.03793 0.03968 = 0.08586 -0.02072 0.01058 -0.00549 C42 1 0.383790 0.113154 0.225057 11.00000 0.05205 0.07936 = 0.04052 -0.00454 0.00921 0.00377 AFIX 13 H42A 2 0.394515 0.144898 0.286104 11.00000 -1.20000 AFIX 0 C43 1 0.365426 0.182250 0.160722 11.00000 0.08018 0.08371 = 0.13545 0.02388 -0.00284 0.02028 AFIX 137 H43A 2 0.350879 0.221080 0.205916 11.00000 -1.50000 H43B 2 0.348445 0.155284 0.109910 11.00000 -1.50000 H43C 2 0.384929 0.215634 0.124213 11.00000 -1.50000 AFIX 0 C44 1 0.416937 0.075239 0.172791 11.00000 0.08601 0.09198 = 0.09074 0.00784 0.03994 0.01054 AFIX 137 H44A 2 0.408479 0.036658 0.116874 11.00000 -1.50000 H44B 2 0.431860 0.042020 0.223170 11.00000 -1.50000 H44C 2 0.432544 0.121794 0.143528 11.00000 -1.50000 AFIX 0 C45 1 0.341435 -0.079890 0.525666 11.00000 0.06486 0.04420 = 0.10120 0.00375 0.02594 -0.00616 AFIX 13 H45A 2 0.366817 -0.060953 0.551443 11.00000 -1.20000 AFIX 0 C46 1 0.339890 -0.179743 0.533522 11.00000 0.23180 0.07303 = 0.12589 0.00284 0.07027 0.00930 AFIX 137 H46A 2 0.346783 -0.205258 0.466381 11.00000 -1.50000 H46B 2 0.314210 -0.197885 0.552299 11.00000 -1.50000 H46C 2 0.357694 -0.199530 0.586877 11.00000 -1.50000 AFIX 0 C47 1 0.312425 -0.040827 0.595170 11.00000 0.07855 0.11651 = 0.07665 -0.00750 0.02299 0.00907 AFIX 137 H47A 2 0.287217 -0.050049 0.565444 11.00000 -1.50000 H47B 2 0.317173 0.021587 0.602085 11.00000 -1.50000 H47C 2 0.313776 -0.068289 0.663762 11.00000 -1.50000 AFIX 0 C48 1 0.448273 0.144621 0.704625 11.00000 0.05103 0.04783 = 0.04122 0.00348 -0.01819 0.00259 C49 1 0.435198 0.093734 0.785163 11.00000 0.07616 0.06196 = 0.05712 0.01717 -0.01681 -0.00261 C50 1 0.442102 0.121099 0.888574 11.00000 0.11110 0.08649 = 0.04507 0.02227 -0.01196 -0.00501 AFIX 43 H50A 2 0.433610 0.086158 0.944755 11.00000 -1.20000 AFIX 0 C51 1 0.460624 0.196317 0.908651 11.00000 0.10982 0.07576 = 0.03999 0.00405 -0.01737 -0.00422 AFIX 43 H51A 2 0.465365 0.213469 0.978354 11.00000 -1.20000 AFIX 0 C52 1 0.472433 0.247315 0.828072 11.00000 0.07713 0.06263 = 0.04438 -0.00138 -0.01487 -0.00543 AFIX 43 H52A 2 0.485013 0.300393 0.842879 11.00000 -1.20000 AFIX 0 C53 1 0.466629 0.224005 0.726063 11.00000 0.05779 0.05778 = 0.04249 -0.00019 -0.01490 0.00078 C54 1 0.414093 0.008437 0.767988 11.00000 0.11995 0.06789 = 0.06495 0.03083 -0.01921 -0.01673 AFIX 13 H54A 2 0.403823 0.010170 0.695612 11.00000 -1.20000 AFIX 0 C55 1 0.438989 -0.069822 0.774724 11.00000 0.15284 0.06063 = 0.12277 0.00288 -0.00942 0.00126 AFIX 137 H55A 2 0.458429 -0.060368 0.827827 11.00000 -1.50000 H55B 2 0.451136 -0.079823 0.707325 11.00000 -1.50000 H55C 2 0.423720 -0.120573 0.793434 11.00000 -1.50000 AFIX 0 C56 1 0.380729 -0.005280 0.839721 11.00000 0.12784 0.10043 = 0.10621 0.02943 0.00753 -0.02693 AFIX 137 H56A 2 0.363089 0.043458 0.832767 11.00000 -1.50000 H56B 2 0.389661 -0.008774 0.911692 11.00000 -1.50000 H56C 2 0.367819 -0.059411 0.821183 11.00000 -1.50000 AFIX 0 C57 1 0.478699 0.284159 0.638966 11.00000 0.05364 0.06742 = 0.04081 0.00318 -0.00721 -0.01676 AFIX 13 H57A 2 0.477760 0.250166 0.572814 11.00000 -1.20000 AFIX 0 C58 1 0.450484 0.357847 0.629267 11.00000 0.08309 0.10887 = 0.06626 0.04304 -0.00038 0.00636 AFIX 137 H58A 2 0.449049 0.389346 0.695312 11.00000 -1.50000 H58B 2 0.425513 0.334245 0.612033 11.00000 -1.50000 H58C 2 0.458652 0.397580 0.574186 11.00000 -1.50000 AFIX 0 C59 1 0.519142 0.317624 0.651874 11.00000 0.08113 0.10651 = 0.07438 0.00301 -0.00353 -0.02797 AFIX 137 H59A 2 0.536903 0.268993 0.646305 11.00000 -1.50000 H59B 2 0.521823 0.345062 0.720184 11.00000 -1.50000 H59C 2 0.524627 0.360269 0.597409 11.00000 -1.50000 AFIX 0 PART 1 C61 1 0.343028 0.407147 0.649731 21.00000 0.06239 0.07296 = 0.04422 -0.00833 -0.00202 0.00214 AFIX 43 H61A 2 0.345352 0.465940 0.671090 21.00000 -1.20000 AFIX 0 PART 2 C61' 1 0.338804 0.361404 0.633206 -21.00000 0.05059 PART 0 O61 6 0.351924 0.392306 0.556914 11.00000 0.06360 0.05820 = 0.03099 0.00071 0.00902 0.00325 PART 1 C62 1 0.347277 0.223946 0.696020 21.00000 0.03929 0.05068 = 0.05229 0.01527 -0.00404 -0.01655 PART 2 C62' 1 0.336567 0.186037 0.713573 -21.00000 0.05151 AFIX 43 H62A 2 0.324732 0.139327 0.749167 -21.00000 -1.20000 AFIX 0 PART 0 O62 6 0.358223 0.165597 0.639858 11.00000 0.04747 0.05886 = 0.04409 -0.00615 0.00969 0.01308 C63 1 0.307595 0.248048 0.898648 11.00000 0.07848 0.07503 = 0.04772 0.00120 -0.00076 -0.01784 O63 6 0.299710 0.209118 0.970679 11.00000 0.14513 0.12808 = 0.06007 0.03700 -0.02636 -0.06694 C64 1 0.299777 0.427038 0.832384 11.00000 0.05859 0.07698 = 0.07322 -0.00130 -0.00677 0.00217 O64 6 0.286905 0.488033 0.869061 11.00000 0.09763 0.08226 = 0.14292 -0.04917 -0.00676 0.03548 C65 1 0.272516 0.286976 0.700421 11.00000 0.08510 0.05854 = 0.04752 -0.00631 0.00044 0.01288 O65 6 0.244273 0.269638 0.662541 11.00000 0.08261 0.09814 = 0.07087 -0.01079 -0.01608 -0.00006 C66 1 0.373146 0.345833 0.843548 11.00000 0.09355 0.07400 = 0.05032 -0.00237 0.01091 0.01620 O66 6 0.400293 0.365567 0.883924 11.00000 0.07075 0.12991 = 0.08551 -0.02063 -0.01367 -0.00297 PART 2 C70 1 0.619526 0.370754 0.326949 31.00000 0.11812 0.12364 = 0.11067 0.01267 -0.00990 0.00392 AFIX 33 H70A 2 0.634450 0.424371 0.326694 31.00000 -1.50000 H70B 2 0.628504 0.332248 0.271572 31.00000 -1.50000 H70C 2 0.592811 0.384705 0.315282 31.00000 -1.50000 AFIX 66 C71 1 0.624164 0.322839 0.437906 31.00000 0.07371 0.10950 = 0.12671 -0.01127 0.00504 -0.02539 C72 1 0.605585 0.244981 0.457328 31.00000 0.10814 0.10381 = 0.10644 -0.01178 0.00007 -0.02263 AFIX 43 H72A 2 0.588849 0.221485 0.406872 31.00000 -1.20000 AFIX 65 C73 1 0.611492 0.201501 0.550572 31.00000 0.10882 0.11708 = 0.14408 -0.01708 0.01678 0.01653 AFIX 43 H73A 2 0.598794 0.148288 0.563845 31.00000 -1.20000 AFIX 65 C74 1 0.635978 0.235879 0.624396 31.00000 0.11018 0.12350 = 0.11518 -0.00321 0.00965 0.03636 AFIX 43 H74A 2 0.640015 0.206162 0.688125 31.00000 -1.20000 AFIX 65 C75 1 0.654557 0.313737 0.604976 31.00000 0.11612 0.13090 = 0.11680 -0.01125 0.00742 0.02539 AFIX 43 H75A 2 0.671292 0.337233 0.655432 31.00000 -1.20000 AFIX 65 C76 1 0.648650 0.357218 0.511732 31.00000 0.11712 0.11850 = 0.11614 -0.00803 -0.00348 0.00500 AFIX 43 H76A 2 0.661348 0.410431 0.498459 31.00000 -1.20000 AFIX 0 PART 1 C70' 1 0.622030 0.194526 0.626691 41.00000 0.10308 AFIX 33 H70D 2 0.608248 0.143612 0.601150 41.00000 -1.50000 H70E 2 0.647483 0.177104 0.648529 41.00000 -1.50000 H70F 2 0.608478 0.219584 0.685970 41.00000 -1.50000 AFIX 66 C71' 1 0.625130 0.265900 0.535034 41.00000 0.07376 C72' 1 0.643533 0.344357 0.552124 41.00000 0.11844 AFIX 43 H72B 2 0.654093 0.356708 0.618379 41.00000 -1.20000 AFIX 65 C73' 1 0.646487 0.404742 0.472272 41.00000 0.12405 AFIX 43 H73B 2 0.659064 0.458364 0.483953 41.00000 -1.20000 AFIX 65 C74' 1 0.631037 0.386671 0.375330 41.00000 0.11975 AFIX 43 H74B 2 0.633055 0.427941 0.320755 41.00000 -1.20000 AFIX 65 C75' 1 0.612633 0.308213 0.358239 41.00000 0.10363 AFIX 43 H75B 2 0.602074 0.295863 0.291983 41.00000 -1.20000 AFIX 65 C76' 1 0.609680 0.247827 0.438089 41.00000 0.11122 AFIX 43 H76B 2 0.597102 0.194206 0.426408 41.00000 -1.20000 AFIX 0 PART 3 C70" 1 0.618398 0.410577 0.293986 51.00000 0.11495 AFIX 33 H70G 2 0.637371 0.456967 0.293765 51.00000 -1.50000 H70H 2 0.621178 0.375298 0.231077 51.00000 -1.50000 H70I 2 0.593019 0.436152 0.295704 51.00000 -1.50000 AFIX 66 C71" 1 0.624378 0.350068 0.395277 51.00000 0.10816 C72" 1 0.600596 0.279602 0.412174 51.00000 0.10997 AFIX 43 H72C 2 0.582952 0.262779 0.360255 51.00000 -1.20000 AFIX 65 C73" 1 0.602630 0.233751 0.505034 51.00000 0.11432 AFIX 43 H73C 2 0.586376 0.185591 0.516581 51.00000 -1.20000 AFIX 65 C74" 1 0.628446 0.258365 0.580999 51.00000 0.10670 AFIX 43 H74C 2 0.629836 0.227028 0.644465 51.00000 -1.20000 AFIX 65 C75" 1 0.652228 0.328831 0.564104 51.00000 0.11684 AFIX 43 H75C 2 0.669872 0.345654 0.616023 51.00000 -1.20000 AFIX 65 C76" 1 0.650195 0.374683 0.471244 51.00000 0.11647 AFIX 43 H76C 2 0.666449 0.422843 0.459697 51.00000 -1.20000 PART 0 AFIX 0 HKLF 4 REM MRC2109 in Pna2(1) REM wR2 = 0.1166, GooF = S = 1.023, Restrained GooF = 1.018 for all data REM R1 = 0.0427 for 7525 Fo > 4sig(Fo) and 0.0570 for all 9229 data REM 809 parameters refined using 136 restraints END WGHT 0.0549 1.4661 REM Highest difference peak 1.698, deepest hole -0.836, 1-sigma level 0.069 Q1 1 0.3830 0.2424 0.4470 11.00000 0.05 1.70 Q2 1 0.3830 0.2427 0.0941 11.00000 0.05 0.93 Q3 1 0.3338 0.3633 0.6855 11.00000 0.05 0.45 Q4 1 0.3074 0.2753 0.7600 11.00000 0.05 0.42 Q5 1 0.3352 0.2613 0.7008 11.00000 0.05 0.41 Q6 1 0.3966 0.0534 0.1144 11.00000 0.05 0.40 Q7 1 0.3281 0.2370 0.7156 11.00000 0.05 0.40 Q8 1 0.3425 0.4049 0.7682 11.00000 0.05 0.39 Q9 1 0.4682 -0.1826 0.2678 11.00000 0.05 0.38 Q10 1 0.3260 0.2450 0.8315 11.00000 0.05 0.36 ; _shelx_res_checksum 50721 _shelx_hkl_file ; 0 0 1 178.053 107.279 1 0 0 2 865388. 4790.58 1 0 0 3 264.667 288.616 1 0 0 4 34655.2 1411.59 1 0 0 5-123.169 337.138 1 0 0 9-99.0724 226.990 3 0 0 10 24210.1 1142.58 3 0 0 11-170.763 303.867 3 0 0 12 36595.9 1520.98 3 0 0 13-98.5029 319.415 3 0 0 14 34556.3 1327.69 3 0 0 15-113.895 218.697 3 0 1 1 313960. 2321.63 1 0 1 2 28.3041 208.653 1 0 1 3 49391.4 1490.91 1 0 1 4-46.0067 308.412 1 0 1 5 94582.7 2707.31 1 0 1 6 152.893 343.347 1 0 -1 9 75096.4 1871.07 3 0 1 9 71706.9 1816.93 3 0 -1 10-202.925 236.433 3 0 1 10 93.4744 231.238 3 0 1 11 24796.8 1215.95 3 0 -1 11 25493.0 1259.18 3 0 -1 12 271.706 315.595 3 0 1 12 39.3426 278.371 3 0 1 13 15368.0 976.405 3 0 -1 13 14933.2 991.983 3 0 -1 14-72.7477 283.847 3 0 1 14 127.331 259.243 3 0 -1 15 15815.6 791.979 3 0 2 0 4435.72 281.456 1 0 2 1 7.09100 159.633 1 0 2 2 193933. 2612.86 1 0 2 3-21.5792 282.670 1 0 2 4 73126.3 2168.78 1 0 2 5 38.5470 336.468 1 0 2 6 23780.6 1585.92 1 0 2 7 408.729 460.289 1 0 2 9 26.3985 214.563 3 0 -2 9-380.231 303.309 3 0 -2 10 21505.8 1104.70 3 0 2 10 19224.5 1027.86 3 0 -2 11-28.7484 318.058 3 0 2 11-283.534 315.738 3 0 -2 12 10550.9 865.052 3 0 2 12 8960.04 771.888 3 0 -2 13-11.9823 304.175 3 0 2 13-120.958 282.257 3 0 2 14 8533.23 651.448 3 0 -2 14 9411.43 762.267 3 0 -2 15-48.0671 224.288 3 0 3 0 136.763 151.924 1 0 3 1 166755. 2273.84 1 0 3 2 382.274 280.346 1 0 3 3 94458.8 2276.15 1 0 3 4-61.1530 292.516 1 0 3 5 1905.69 504.145 1 0 3 6-93.0414 399.963 1 0 3 7 2504.06 698.464 1 0 3 8-191.339 410.874 1 0 -3 9 1834.32 359.531 3 0 3 9 1215.28 299.315 3 0 -3 10-19.6231 274.604 3 0 3 10-224.972 260.498 3 0 3 11-260.763 259.540 3 0 -3 11-196.913 325.374 3 0 -3 12 20.3960 310.186 3 0 3 12-295.866 282.460 3 0 3 13 727.734 320.647 3 0 -3 13 258.066 374.398 3 0 -3 14-28.9620 314.922 3 0 -3 15 1312.27 297.993 3 0 4 0 55329.6 1335.55 1 0 4 1-27.0221 217.656 1 0 4 2 5917.22 584.365 1 0 4 3 161.343 258.239 1 0 4 4 109507. 2903.63 1 0 4 5-99.4247 350.365 1 0 4 6 14649.5 1330.12 1 0 4 7 264.540 416.890 1 0 4 8 3095.37 859.128 1 0 -4 9-169.205 251.967 3 0 4 9-989.991 285.100 3 0 -4 10 802.705 321.701 3 0 4 10 660.803 262.850 3 0 4 11-12.1355 225.300 3 0 -4 11-18.4172 294.151 3 0 -4 12 49.7907 345.093 3 0 4 12 430.959 323.956 3 0 -4 13-113.355 315.489 3 0 -4 14 101.731 347.206 3 0 -4 15-51.0113 193.647 3 0 5 -1 127372. 2190.31 1 0 5 0 148.031 181.432 1 0 5 1 115533. 2335.94 1 0 5 2 423.322 283.705 1 0 5 3 46008.7 1798.80 1 0 5 4 269.926 371.298 1 0 5 5 23078.7 1539.83 1 0 5 6-418.127 512.218 1 0 5 7 5317.24 928.791 1 0 5 8 151.903 443.138 1 0 -5 8 44.0145 208.349 3 0 -5 9 27857.3 1216.61 3 0 -5 10 49.1380 268.520 3 0 -5 11 23225.1 1217.64 3 0 -5 12-287.250 332.803 3 0 -5 13 4897.93 591.584 3 0 -5 14 191.991 252.278 3 0 -5 15 3016.76 352.668 3 0 6 -2 26939.5 1131.79 1 0 6 -1-91.7926 183.097 1 0 6 0 46671.1 1536.47 1 0 6 1 96.7947 220.309 1 0 6 2 39052.1 1598.38 1 0 6 3 96.1968 296.076 1 0 6 4 29202.9 1645.96 1 0 6 5-181.086 459.660 1 0 6 6 128698. 4076.37 1 0 6 7-251.352 523.319 1 0 6 8 121161. 4597.85 1 0 -6 8 111241. 2280.42 3 0 -6 9 369.122 290.506 3 0 -6 10 12205.3 863.968 3 0 -6 11-39.2691 275.395 3 0 -6 12 15843.9 999.081 3 0 -6 13-146.347 271.012 3 0 -6 14 12329.9 733.223 3 0 7 -2 255.520 214.006 1 0 7 -1 87694.8 2217.14 1 0 7 0-124.416 252.798 1 0 7 1 95493.5 2513.63 1 0 7 2 61.9457 266.814 1 0 7 3 121044. 3232.41 1 0 7 4 204.637 443.057 1 0 7 5 62647.9 2716.23 1 0 7 6 87.0581 445.017 1 0 7 7 37860.1 2484.62 1 0 -7 8-101.890 259.006 3 0 7 8 478.776 408.641 1 0 -7 9 23996.2 1149.62 3 0 7 9 27094.0 2380.57 1 0 -7 10-224.726 303.233 3 0 -7 11 17124.4 1029.79 3 0 -7 12 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1216.86 1 10 2 3 39227.0 1696.78 1 10 -2 3 40843.5 1192.28 1 10 -2 4 15912.8 883.622 1 10 2 4 16336.8 1216.03 1 10 2 5 14605.2 1239.89 1 10 -2 5 14647.6 974.870 1 10 2 6 600.530 442.263 1 10 2 7 28237.1 2038.36 1 -10 -2 8 1280.65 338.161 3 -10 2 8 1408.30 353.237 3 10 -2 8 1549.05 323.396 3 10 2 8 1361.19 578.451 1 -10 2 9 26456.6 1257.65 3 10 -2 9 27684.9 1194.60 3 10 2 9 25767.1 2230.23 1 -10 -2 9 26611.0 1268.99 3 10 2 9 23787.3 1033.01 3 -10 2 10 4072.35 555.174 3 10 2 10 4590.38 514.033 3 -10 -2 10 5040.79 634.547 3 10 -2 10 5138.65 578.698 3 -10 -2 11 12761.2 983.902 3 -10 2 11 11916.4 928.479 3 10 -2 11 11622.6 852.443 3 10 2 11 11628.6 792.782 3 10 -2 12 46.3634 293.952 3 -10 -2 12-18.0401 346.024 3 10 2 12 460.734 273.899 3 10 2 13 9072.29 650.171 3 10 -2 13 9278.87 739.501 3 10 2 14 762.213 220.470 3 10 -2 14 812.542 284.610 3 10 -2 15 5024.47 404.736 3 10 3 0 841.367 399.396 1 10 3 1 10452.1 867.438 1 10 3 2 481.633 329.480 1 10 3 3 2158.19 553.843 1 10 3 4 8215.88 938.542 1 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526.739 329.727 4 -10 -10 -10 378.343 261.798 4 10 -10 -9 10318.7 847.840 4 -10 -10 -9 9773.47 774.215 4 -10 -10 -8-508.471 321.880 4 10 -10 -8 616.191 383.080 4 -10 -10 -7 443.500 271.323 4 10 -10 -7 1554.69 450.023 4 10 -10 -6 594.924 408.774 4 -10 -10 -6 95.9560 260.090 4 10 10 -5 11003.5 1404.28 1 10 -10 -5 9809.80 826.965 4 10 10 -4-43.1823 354.798 1 10 -10 -4 149.617 320.030 4 10 10 -3 21101.6 1792.13 1 10 -10 -3 20826.2 1149.36 4 10 10 -2 6906.15 1009.31 1 10 -10 -2 5626.67 629.853 4 10 -10 -1 12601.6 903.194 4 10 10 -1 13016.9 1426.68 1 10 10 0 33.7913 392.189 1 10 -10 0 123.514 290.464 4 10 -10 1 10282.7 821.792 4 10 10 1 9634.91 1286.16 1 10 -10 2 6823.44 687.450 4 10 10 2 5362.54 967.310 1 10 -10 3 22974.9 1219.70 4 10 10 3 20683.3 1907.58 1 10 -10 4 323.738 317.133 4 10 10 4 680.318 527.955 1 10 -10 5 13482.4 962.269 4 10 10 5 12789.2 1625.68 1 10 10 6 106.947 636.001 1 10 -10 8-174.181 225.318 3 10 -10 9 10300.3 725.941 3 10 -10 10 305.733 251.306 3 10 -10 11 4252.06 441.893 3 10 -10 12 92.1845 167.122 3 10 -11 -12-220.519 161.650 4 10 -11 -11 123.211 221.910 4 -10 -11 -11 202.553 162.882 4 -10 -11 -10 545.203 249.218 4 10 -11 -10 500.108 323.317 4 -10 -11 -9 555.523 271.983 4 10 -11 -9 783.284 377.491 4 -10 -11 -8 256.846 298.644 4 10 -11 -8 346.499 356.757 4 -10 -11 -7-78.0438 249.430 4 10 -11 -7 514.875 416.161 4 10 -11 -6 694.542 412.652 4 -10 -11 -6 288.246 286.294 4 10 -11 -5 1622.60 463.961 4 10 -11 -4 1121.84 430.529 4 10 -11 -3 7095.64 761.399 4 10 11 -3 6226.19 1028.83 1 10 11 -2-4.04611 412.027 1 10 -11 -2 117.388 270.280 4 10 11 -1 214.721 445.142 1 10 -11 -1 678.643 316.930 4 10 11 0 3034.44 787.802 1 10 -11 0 3043.97 528.114 4 10 11 1-252.375 596.372 1 10 -11 1 700.356 336.511 4 10 -11 2 107.534 312.158 4 10 11 2 87.5625 547.946 1 10 -11 3 6545.79 713.023 4 10 11 3 9061.18 1343.84 1 10 -11 4 402.939 372.452 4 10 11 4 902.280 557.560 1 10 -11 5 2108.35 481.250 4 10 11 5 2023.15 756.317 1 10 -12 -11 507.592 212.666 4 10 -12 -10 159.790 230.001 4 -10 -12 -10-284.281 144.240 4 10 -12 -9 2919.81 483.622 4 -10 -12 -9 1358.15 287.732 4 10 -12 -8 232.673 326.434 4 -10 -12 -8 300.858 245.896 4 10 -12 -7 2636.60 536.560 4 -10 -12 -7 1126.32 314.719 4 10 -12 -6 13.4809 360.619 4 10 -12 -5 3079.15 557.937 4 10 -12 -4 15.6629 342.005 4 10 -12 -3 5839.38 693.382 4 10 -12 -2 1012.06 419.368 4 10 12 -1 1766.36 709.352 1 10 -12 -1 2575.82 514.105 4 10 12 0 266.271 608.684 1 10 -12 0-493.523 435.188 4 10 -12 1 1345.52 445.177 4 10 12 1 260.078 472.211 1 10 -12 2 921.440 398.702 4 10 12 2 55.3337 601.272 1 10 -12 3 5220.37 685.618 4 10 12 3 5270.82 1117.91 1 10 -12 4 316.117 405.896 4 10 -12 5 2598.78 579.484 4 10 -13 -11 97.9890 122.764 4 10 -13 -10 1643.51 304.713 4 10 -13 -9 339.177 262.900 4 10 -13 -8 4561.56 547.695 4 10 -13 -7 14.6547 322.525 4 10 -13 -6 10102.5 855.039 4 10 -13 -5-912.282 449.051 4 10 -13 -4 16013.9 1105.67 4 10 -13 -3 1977.32 479.487 4 10 -13 -2 11821.2 970.514 4 10 -13 -1 329.320 346.385 4 10 -13 0 15018.3 1094.28 4 10 -13 1 233.328 349.636 4 10 -13 2 12011.2 993.930 4 10 -13 3 2464.07 544.811 4 10 -13 4 16537.7 1139.35 4 10 -14 -10 245.841 146.211 4 10 -14 -9 4171.20 415.124 4 10 -14 -8 201.967 245.501 4 10 -14 -7 4734.31 560.601 4 10 -14 -6 1751.58 434.243 4 10 -14 -5 7563.60 734.377 4 10 -14 -4 1501.36 440.674 4 10 -14 -3 10873.1 913.024 4 10 -14 -2 523.907 371.265 4 10 -14 -1 14458.5 1059.15 4 10 -14 0 58.0846 372.889 4 10 -14 1 13089.0 1024.05 4 10 -14 2 527.594 437.779 4 10 -14 3 9731.54 881.497 4 10 -14 4 915.925 408.539 4 10 -15 -9-102.378 147.293 4 10 -15 -8 3963.30 414.761 4 10 -15 -7 198.218 236.463 4 10 -15 -6 5569.42 567.051 4 10 -15 -5 348.284 318.245 4 10 -15 -4 3785.35 560.065 4 10 -15 -3 2138.11 481.373 4 10 -15 -2 7084.02 753.627 4 10 -15 -1 794.579 436.425 4 10 -15 0 23185.2 1293.40 4 10 -15 1 128.198 366.492 4 10 -15 2 8245.22 817.111 4 10 -15 3 2469.76 523.624 4 10 -16 -8-251.754 128.851 4 10 -16 -7 2394.21 306.668 4 10 -16 -6 348.096 248.577 4 10 -16 -5 3947.28 473.066 4 10 -16 -4 326.727 298.907 4 10 -16 -3 7346.65 668.025 4 10 -16 -2 186.005 311.995 4 10 -16 -1 6421.16 681.669 4 10 -16 0-233.292 372.878 4 10 -16 1 5527.64 642.594 4 10 -16 2 1118.04 374.066 4 10 -16 3 7033.47 683.197 4 10 -17 -6 704.961 191.620 4 10 -17 -5 32.8806 169.593 4 10 -17 -4 964.246 262.738 4 10 -17 -3 160.685 223.022 4 10 -17 -2 2392.31 398.722 4 10 -17 -1 572.286 265.720 4 10 -17 0 2127.99 402.424 4 10 -17 1 517.276 267.189 4 10 -17 2 1935.13 358.314 4 10 -18 -4 25.1679 117.354 4 10 -18 -3 280.266 167.980 4 10 -18 -2 76.9080 162.681 4 10 -18 -1 622.297 227.158 4 10 -18 0 528.264 216.087 4 11 0 1-190.574 210.981 1 11 0 2-155.444 247.931 1 11 0 3-106.435 303.465 1 11 0 4 117.907 339.364 1 11 0 5 78.7328 297.192 1 11 0 6-141.614 358.002 1 11 0 7 606.505 437.369 1 11 0 8-23.2682 199.738 3 11 0 8 561.588 497.509 1 -11 0 8-54.8202 253.299 3 11 0 9-321.079 284.953 3 -11 0 9 113.674 293.561 3 11 0 10 60.5003 233.676 3 -11 0 10-238.754 308.220 3 11 0 11-209.147 266.307 3 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1466.78 440.424 3 11 1 12 2291.94 391.626 3 11 1 13 367.187 301.956 3 11 -1 13 255.507 257.419 3 11 1 14 1202.31 261.541 3 11 -1 14 1369.53 312.292 3 11 -1 15 243.488 150.874 3 11 2 1 111318. 2578.02 1 11 -2 1 109454. 1631.12 1 11 -2 2 10499.5 536.279 1 11 2 2 9157.51 835.097 1 11 2 3 20597.8 1280.50 1 11 -2 3 22253.1 906.343 1 11 -2 4 17142.7 927.711 1 11 2 4 17459.7 1262.03 1 11 2 5 12505.6 1201.63 1 11 -2 5 13381.5 938.983 1 11 2 6 1126.31 454.830 1 11 2 7 93311.6 3683.46 1 -11 2 8 12040.7 829.886 3 11 -2 8 11403.7 733.501 3 11 2 8 10986.7 1396.62 1 -11 -2 8 12136.5 835.337 3 -11 2 9 42737.9 1598.93 3 11 -2 9 40646.2 1435.62 3 11 2 9 39956.8 2775.92 1 -11 -2 9 42055.3 1606.26 3 11 2 9 40275.4 1324.71 3 -11 2 10 3123.44 517.508 3 -11 -2 10 2249.69 478.015 3 11 2 10 2758.64 411.118 3 11 -2 10 2770.91 460.427 3 -11 -2 11 18059.6 1147.59 3 11 2 11 18980.7 988.548 3 11 -2 11 18705.2 1053.01 3 11 -2 12 2634.84 459.438 3 11 2 12 3012.90 424.430 3 -11 -2 12 3025.21 549.904 3 11 2 13 10570.3 681.905 3 11 -2 13 10457.3 761.420 3 11 -2 14 1216.89 311.741 3 11 -2 15 4442.53 369.715 3 11 3 0 167752. 3345.45 1 11 3 1 15288.9 1066.28 1 11 3 2 198181. 3879.79 1 11 3 3 13678.6 1125.63 1 11 3 4 26332.0 1599.07 1 11 3 5 18564.7 1466.61 1 11 3 6 72028.2 3078.99 1 11 3 7 15895.8 1562.02 1 -11 3 8 34683.9 1376.92 3 11 -3 8 35105.3 1287.77 3 11 3 8 35596.6 2511.16 1 -11 -3 8 33550.8 1356.36 3 11 -3 9 15194.4 914.501 3 11 3 9 13205.5 1630.59 1 -11 -3 9 15633.0 1007.12 3 11 3 10 21775.9 2179.65 1 -11 -3 10 24480.0 1291.13 3 11 -3 10 23576.3 1178.32 3 -11 -3 11 3856.25 600.962 3 11 3 11 4166.30 483.670 3 11 -3 11 3495.12 508.404 3 -11 -3 12 16599.4 1064.29 3 11 -3 12 15625.6 966.903 3 11 -3 13 2216.47 415.687 3 11 -3 14 9375.05 644.305 3 11 -3 15 1500.55 240.433 3 11 4 0 7668.13 828.633 1 11 4 1 194692. 3923.79 1 11 4 2 27904.0 1588.64 1 11 4 3 172314. 4052.41 1 11 4 4 16477.6 1364.02 1 11 4 5 107571. 3620.22 1 11 4 6 4494.70 829.303 1 11 -4 7 92131.9 2001.93 3 11 4 7 93491.4 3848.25 1 11 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11 -5 12 13263.7 894.941 3 11 -5 13 1315.32 348.415 3 11 -5 14 7701.21 553.199 3 11 -6 -14 177.874 140.862 4 11 6 -1 25503.1 1599.90 1 11 6 0 23369.4 1539.77 1 11 6 1 17541.5 1367.88 1 11 6 2 29766.7 1829.42 1 11 6 3 44506.0 2324.19 1 11 6 4 11086.5 1254.20 1 11 6 5 38732.1 2377.12 1 11 6 6 7205.24 1127.35 1 11 -6 7 11751.2 768.779 3 11 6 7 10630.8 1424.57 1 -11 -6 7 12240.1 801.378 3 -11 -6 8 19.3802 235.933 3 11 6 8 897.447 619.638 1 11 -6 8 259.377 256.243 3 -11 -6 9 6023.22 654.348 3 11 6 9 7730.61 1357.44 1 11 -6 9 6024.42 638.442 3 -11 -6 10 1004.04 384.240 3 11 -6 10 1433.08 391.656 3 -11 -6 11 2285.43 464.178 3 11 -6 11 3848.26 542.834 3 11 -6 12 113.701 271.886 3 11 -6 13 3100.62 435.105 3 11 -6 14 325.443 206.670 3 11 -7 -13 441.785 221.065 4 11 7 -2 5349.01 827.648 1 11 7 -1 7619.47 965.889 1 11 7 0 16625.8 1381.68 1 11 7 1 8314.73 1033.07 1 11 7 2 7297.31 1000.48 1 11 7 3 11229.9 1282.84 1 11 7 4 7571.67 1104.72 1 11 7 5 856.641 552.520 1 11 7 6 7591.94 1192.28 1 11 -7 6 7280.80 597.647 3 11 7 7 773.117 498.915 1 11 -7 7 437.801 226.640 3 11 7 8 6462.58 1254.25 1 11 -7 8 5709.74 596.542 3 -11 -7 9 1997.55 413.263 3 11 -7 9 1727.32 372.653 3 -11 -7 10 500.728 293.067 3 11 -7 10 632.646 322.917 3 11 -7 11 111.835 302.465 3 11 -7 12 1038.17 327.236 3 11 -7 13 900.267 285.212 3 11 -7 14 619.362 195.678 3 -11 -8 -13 536.241 195.378 4 11 -8 -13 558.868 212.551 4 11 -8 -12 786.555 305.156 4 11 -8 -11 804.654 346.643 4 11 -8 -6 6029.43 662.507 4 11 -8 -5 1104.18 342.760 4 11 8 -3 2946.48 713.674 1 11 8 -2 779.779 447.733 1 11 8 -1 10555.0 1194.53 1 11 8 0 3277.27 717.975 1 11 8 1 10801.1 1221.53 1 11 8 2 866.047 515.081 1 11 8 3 1523.86 572.273 1 11 -8 4 332.047 291.475 4 11 8 4-510.963 439.488 1 11 -8 5 644.813 293.810 4 11 -8 5 627.224 239.398 3 11 8 5 236.144 563.898 1 11 8 6 6025.96 1108.73 1 11 -8 6 6300.40 559.755 3 11 8 7 101.272 539.322 1 11 -8 7 225.978 223.740 3 11 8 8 3789.99 961.973 1 11 -8 8 3741.47 486.640 3 11 -8 9 1654.19 395.405 3 11 -8 10 21.0092 251.658 3 11 -8 11 164.035 278.238 3 11 -8 12 1007.79 339.825 3 11 -8 13 621.149 228.172 3 11 -9 -13 456.442 171.348 4 11 -9 -12 1562.36 326.746 4 -11 -9 -12 1639.29 289.466 4 11 -9 -11 1116.57 342.423 4 11 -9 -10 8337.35 756.770 4 11 -9 -9 792.971 378.174 4 11 -9 -8 10171.3 885.469 4 11 -9 -7 6663.61 705.467 4 11 -9 -6 15971.4 1037.48 4 11 9 -5 4518.02 840.216 1 11 -9 -5 4610.45 596.405 4 11 9 -4 18078.4 1654.88 1 11 -9 -4 18238.6 1052.67 4 11 9 -3 647.729 323.007 1 11 -9 -3 2427.78 433.980 4 11 -9 -2 21242.6 1098.51 4 11 9 -2 21980.7 1783.99 1 11 9 -1 2283.48 649.608 1 11 9 0 8092.66 1112.31 1 11 9 1 2143.92 574.613 1 11 -9 2 18317.6 1015.60 4 11 9 2 18512.3 1708.95 1 11 -9 3 2107.50 398.723 4 11 9 3 1273.43 561.805 1 11 -9 4 19049.5 1070.18 4 11 9 4 15874.1 1685.81 1 11 -9 5 4643.69 607.397 4 11 9 5 4111.10 953.008 1 11 9 6 16269.3 1807.69 1 11 -9 6 15305.4 874.218 3 11 9 7 8368.89 1394.07 1 11 -9 7 7258.55 644.470 3 11 -9 8 12420.2 850.308 3 11 -9 9 1224.34 374.695 3 11 -9 10 8110.13 690.982 3 11 -9 11 1480.37 323.019 3 11 -9 12 2268.73 349.105 3 11 -9 13 543.207 179.913 3 11 -10 -12 976.530 248.894 4 -11 -10 -12-81.3047 75.5340 4 11 -10 -11 7164.82 602.843 4 -11 -10 -11 5304.53 477.502 4 11 -10 -10 2330.10 451.048 4 -11 -10 -10 2017.08 371.021 4 11 -10 -9 17501.6 1072.65 4 -11 -10 -9 14756.8 898.702 4 11 -10 -8 4385.95 587.082 4 -11 -10 -8 4566.43 569.558 4 11 -10 -7 12434.8 966.786 4 -11 -10 -7 11870.0 843.508 4 11 10 -6 1423.49 718.617 1 11 -10 -6 1588.09 442.765 4 11 10 -5 17533.8 1779.68 1 11 -10 -5 17353.0 1093.38 4 11 10 -4 3463.17 799.582 1 11 -10 -4 4075.00 586.132 4 11 -10 -3 25206.3 1274.43 4 11 10 -3 26807.3 2068.27 1 11 10 -2 2799.07 763.710 1 11 -10 -2 2795.68 490.864 4 11 -10 -1 31559.0 1402.65 4 11 10 -1 32223.1 2235.88 1 11 10 0 2653.72 713.120 1 11 -10 0 3511.97 536.960 4 11 -10 1 29308.9 1335.90 4 11 10 1 31902.1 2268.81 1 11 -10 2 2315.32 448.105 4 11 10 2 1003.12 546.198 1 11 -10 3 27641.4 1325.06 4 11 10 3 27549.4 2249.96 1 11 -10 4 5079.66 630.847 4 11 10 4 5218.61 1001.98 1 11 -10 5 19050.3 1148.88 4 11 10 5 19171.0 1960.93 1 11 10 6 2454.09 724.852 1 11 -10 7 13652.3 837.307 3 11 -10 8 4699.48 515.837 3 11 -10 9 16659.9 921.692 3 11 -10 10 3296.99 430.983 3 11 -10 11 6652.35 538.723 3 11 -10 12 1399.14 243.343 3 11 -11 -12 4236.25 346.873 4 11 -11 -11 1778.19 344.409 4 11 -11 -10 2810.83 433.630 4 -11 -11 -10 2222.60 336.316 4 -11 -11 -9 952.662 290.724 4 11 -11 -9 990.791 379.016 4 11 -11 -8 16186.6 1040.44 4 -11 -11 -8 15083.8 901.498 4 11 -11 -7 2296.42 488.862 4 11 -11 -6 26687.8 1370.05 4 11 -11 -5 4008.09 601.310 4 11 11 -4 17947.1 1803.71 1 11 -11 -4 17997.4 1124.23 4 11 11 -3 4923.56 909.108 1 11 -11 -3 6425.53 716.187 4 11 -11 -2 14790.2 1012.46 4 11 11 -2 14395.8 1582.34 1 11 11 -1 4230.57 897.177 1 11 -11 -1 4471.80 593.723 4 11 11 0 45669.7 2815.88 1 11 -11 0 45420.8 1742.03 4 11 11 1 5884.22 1094.77 1 11 -11 1 5464.81 657.016 4 11 11 2 17817.8 1848.71 1 11 -11 2 18359.9 1141.64 4 11 11 3 6262.47 1154.90 1 11 -11 3 4610.75 611.618 4 11 11 4 17209.6 1832.68 1 11 -11 4 17061.5 1126.64 4 11 -11 5 4947.69 649.371 4 11 11 5 3097.07 934.571 1 11 -12 -11 6645.22 474.124 4 11 -12 -10 940.557 294.684 4 11 -12 -9 9069.33 716.842 4 11 -12 -8 226.164 332.234 4 11 -12 -7 11904.6 900.398 4 11 -12 -6 1831.50 447.541 4 11 -12 -5 17313.2 1116.83 4 11 -12 -4 403.682 362.012 4 11 -12 -3 27906.6 1412.00 4 11 -12 -2 2555.91 477.544 4 11 -12 -1 12943.6 994.261 4 11 12 -1 13600.4 1579.24 1 11 12 0 800.696 652.594 1 11 -12 0 578.669 411.365 4 11 12 1 10810.2 1496.64 1 11 -12 1 10748.4 914.182 4 11 12 2 999.697 531.882 1 11 -12 2 2413.86 532.426 4 11 12 3 27935.6 2346.12 1 11 -12 3 29267.4 1476.06 4 11 -12 4 278.186 343.013 4 11 -13 -10 1294.32 255.279 4 11 -13 -9 972.521 309.704 4 11 -13 -8 6992.66 644.546 4 11 -13 -7 52.7516 340.920 4 11 -13 -6 4487.35 613.588 4 11 -13 -5 1415.00 428.302 4 11 -13 -4 8452.61 818.774 4 11 -13 -3 1286.40 433.222 4 11 -13 -2 6040.53 717.553 4 11 -13 -1 1380.69 430.162 4 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510.196 1 13 8 6-808.603 543.017 1 13 -8 6 539.479 272.686 3 13 8 7 330.503 402.038 1 13 -8 7 756.346 323.590 3 13 -8 8 431.719 293.971 3 13 -8 9 363.316 306.541 3 13 -8 10 7828.77 700.121 3 13 -8 11 1782.27 370.114 3 13 -8 12 1129.60 301.406 3 13 -8 13-290.814 195.180 3 13 -9 -12 197.121 177.742 4 13 -9 -11 2579.62 408.369 4 13 -9 -10 60.4445 275.457 4 -13 -9 -10 134.729 220.830 4 13 -9 -9 3910.60 564.332 4 13 -9 -8 212.140 341.431 4 13 -9 -7 9868.69 848.923 4 13 9 -6 2291.72 698.879 1 13 -9 -6 2436.17 496.320 4 13 9 -5 11157.1 1423.37 1 13 -9 -5 12071.1 872.921 4 13 9 -4 4238.59 868.109 1 13 -9 -4 4034.91 534.415 4 13 9 -3 24615.1 1981.31 1 13 -9 -3 22644.8 1160.42 4 13 9 -2 287.105 411.444 1 13 -9 -2 159.374 256.691 4 13 9 -1 19098.7 1746.71 1 13 -9 -1 20119.3 1058.41 4 13 9 0 5070.26 924.367 1 13 -9 0 4901.10 558.518 4 13 9 1 24171.8 1985.33 1 13 -9 1 22836.9 1121.05 4 13 9 2-1536.57 604.711 1 13 -9 2-205.141 260.486 4 13 9 3 28011.5 2245.10 1 13 -9 3 23737.4 1182.61 4 13 9 4 3031.94 760.083 1 13 -9 4 3805.20 535.708 4 13 -9 5 10710.8 746.124 3 13 9 5 11943.2 1506.28 1 13 -9 5 11021.2 856.227 4 13 -9 6 2061.65 380.187 3 13 9 6 1377.93 583.450 1 13 -9 7 9266.62 753.536 3 13 -9 8-177.092 264.426 3 13 -9 9 5420.79 579.500 3 13 -9 10 294.210 273.890 3 13 -9 11 1866.36 354.903 3 13 -9 12 72.9223 167.928 3 13 -10 -12 3715.62 346.953 4 13 -10 -11 322.677 252.181 4 13 -10 -10 4748.63 536.471 4 13 -10 -9 1455.92 395.042 4 13 -10 -8 15060.2 1002.58 4 13 -10 -7 1168.06 417.836 4 13 -10 -6 23675.8 1260.98 4 13 10 -5 3125.87 757.458 1 13 -10 -5 2513.44 496.832 4 13 10 -4 33305.2 2429.96 1 13 -10 -4 34002.1 1486.46 4 13 10 -3 9483.69 1329.79 1 13 -10 -3 9998.74 838.184 4 13 10 -2 22420.9 1955.91 1 13 -10 -2 21762.3 1171.63 4 13 10 -1 2832.61 816.691 1 13 -10 -1 1824.72 415.692 4 13 10 0 18382.1 1796.99 1 13 -10 0 19088.0 1090.39 4 13 10 1 1676.82 576.210 1 13 -10 1 1635.20 372.792 4 13 10 2 20489.2 1933.65 1 13 -10 2 22309.6 1200.76 4 13 10 3 10538.0 1488.00 1 13 -10 3 9909.11 828.808 4 13 10 4 32375.1 2527.70 1 13 -10 4 33976.6 1490.99 4 13 10 5 4145.78 986.393 1 13 -10 5 3483.40 586.263 4 13 -10 6 18436.7 971.254 3 13 -10 7 481.868 263.944 3 13 -10 8 15983.9 919.530 3 13 -10 9 1090.37 327.345 3 13 -10 10 5156.88 517.692 3 13 -10 11 843.034 240.288 3 13 -10 12 4532.55 360.147 3 13 -11 -11 8066.58 536.701 4 13 -11 -10 418.341 268.842 4 13 -11 -9 13351.2 868.176 4 13 -11 -8 2145.83 465.035 4 13 -11 -7 13583.1 966.627 4 13 -11 -6 2146.81 471.281 4 13 -11 -5 29983.6 1419.51 4 13 11 -4 6924.13 1095.39 1 13 -11 -4 7178.42 743.661 4 13 11 -3 38037.8 2630.26 1 13 -11 -3 39179.0 1622.38 4 13 11 -2 2503.00 777.814 1 13 -11 -2 1175.90 379.204 4 13 11 -1 17205.9 1775.71 1 13 -11 -1 18286.9 1124.82 4 13 11 0 8285.73 1252.69 1 13 -11 0 7213.29 751.853 4 13 11 1 16320.3 1782.21 1 13 -11 1 15565.8 1050.57 4 13 11 2 1536.56 736.391 1 13 -11 2 1472.50 436.618 4 13 11 3 39324.7 2783.55 1 13 -11 3 37843.0 1627.03 4 13 11 4 7291.56 1368.95 1 13 -11 4 5752.57 686.481 4 13 -12 -11 787.101 181.807 4 13 -12 -10 1986.72 314.287 4 13 -12 -9 1032.54 317.033 4 13 -12 -8 9011.62 749.798 4 13 -12 -7 1781.25 439.928 4 13 -12 -6 8637.74 792.793 4 13 -12 -5 3104.97 557.569 4 13 -12 -4 13330.3 991.900 4 13 -12 -3 3821.26 589.815 4 13 -12 -2 16028.4 1085.00 4 13 12 -1 5421.35 1031.81 1 13 -12 -1 3613.29 590.196 4 13 12 0 34679.5 2595.74 1 13 -12 0 37983.4 1656.43 4 13 12 1 2455.41 616.455 1 13 -12 1 4651.02 645.683 4 13 -12 2 20414.1 990.188 2 13 -12 2 22088.5 1291.74 4 13 -12 3 3094.12 561.153 4 13 -12 4 16933.6 1135.49 4 13 -13 -10 182.599 154.599 4 13 -13 -9 1736.43 322.812 4 13 -13 -8 777.439 299.889 4 13 -13 -7 2728.42 457.188 4 13 -13 -6 800.306 381.986 4 13 -13 -5 7216.95 732.498 4 13 -13 -4 2758.91 541.252 4 13 -13 -3 5762.45 707.838 4 13 -13 -2 770.447 382.184 4 13 -13 -1 4371.69 632.043 4 13 -13 0 488.420 391.912 4 13 -13 1 4899.90 667.962 4 13 -13 2 1502.01 456.424 4 13 -13 3 8419.96 844.607 4 13 -13 4 2739.30 544.784 4 13 -14 -9 343.918 184.748 4 13 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1070.03 1 14 1 5 41331.7 2107.05 1 14 -1 5 42040.0 1876.29 1 14 -1 6 1424.29 433.525 1 14 1 6 2959.75 634.301 1 -14 -1 7 76534.4 1998.57 3 14 1 7 72451.0 3234.75 1 14 1 8 142.354 303.164 1 -14 -1 8 37.9136 264.821 3 14 -1 8 187.305 191.065 3 14 1 8-39.6797 205.810 3 14 -1 8 57.3879 200.777 2 -14 -1 9 51047.6 1816.95 3 14 -1 9 47999.2 1562.10 3 14 1 9 46818.4 1484.91 3 14 -1 10 1050.76 332.325 3 14 1 10 805.725 269.748 3 14 -1 11 21151.4 1095.97 3 14 1 11 21870.6 1054.70 3 14 -1 12 923.961 304.578 3 14 1 12 911.353 278.426 3 14 1 13 15493.3 805.937 3 14 -1 13 14863.0 827.771 3 14 1 14 584.834 192.211 3 14 -1 14 337.966 197.369 3 14 -2 0 180592. 2614.68 1 14 2 0 180807. 3600.39 1 14 -2 1 11311.0 646.417 1 14 2 1 8968.14 871.494 1 14 -2 2 116054. 2061.33 1 14 2 2 115179. 3030.03 1 14 2 3 1775.81 566.907 1 14 -2 3 1734.49 306.124 1 14 2 4 34465.5 1890.14 1 14 2 5 2098.71 581.736 1 14 2 6 22189.8 1742.75 1 -14 -2 7 3873.50 491.534 3 14 2 7 3906.48 853.960 1 14 -2 7 3325.89 400.807 3 -14 -2 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747.077 251.224 3 14 4 0 2202.75 586.329 1 14 4 1 4055.08 685.715 1 14 4 2 13874.9 1221.16 1 14 4 3 1778.40 563.527 1 14 4 4 14196.0 1339.95 1 14 4 5 1637.41 555.079 1 14 4 6 1666.41 625.957 1 14 4 7 982.536 455.164 1 14 -4 7 529.810 239.851 3 -14 -4 7 371.460 279.031 3 -14 -4 8 1710.30 414.624 3 14 4 8 1385.71 703.063 1 14 -4 8 1658.45 365.567 3 -14 -4 9 1135.16 374.770 3 14 -4 9 1060.83 354.880 3 -14 -4 10 830.377 381.263 3 14 -4 10 974.969 386.542 3 14 -4 11 873.449 349.429 3 14 -4 12 815.536 332.946 3 14 -4 13 15.3503 240.106 3 14 -4 14-13.2047 186.638 3 14 -5 -13 4364.11 412.002 4 14 5 -1 28076.1 1740.66 1 14 5 0 9165.08 1041.17 1 14 5 1 33472.4 1923.89 1 14 5 2 7803.53 995.587 1 14 5 3 2757.50 677.146 1 14 5 4 2637.94 672.419 1 14 5 5 35061.7 2296.47 1 14 5 6 1462.77 673.083 1 14 -5 6 1698.90 346.298 3 -14 -5 7 24461.1 1159.73 3 14 -5 7 25278.2 1135.06 3 14 5 7 24357.6 2114.28 1 -14 -5 8 800.227 307.104 3 14 5 8 344.167 354.522 1 14 -5 8 365.975 303.945 3 -14 -5 9 1409.31 409.715 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3071.84 1 14 7 0 794.161 504.739 1 14 7 1 70023.5 3073.67 1 14 7 2 2112.69 695.558 1 14 7 3 85951.8 3580.25 1 14 7 4 898.147 531.172 1 14 -7 5 64648.6 1760.80 3 14 7 5 64000.6 3329.76 1 14 -7 6 3388.95 447.052 3 14 7 6 3696.46 926.045 1 14 7 7 24752.3 2240.07 1 14 -7 7 27527.0 1228.69 3 14 7 8 2722.54 871.618 1 14 -7 8 2177.14 430.427 3 14 -7 9 14072.2 939.815 3 14 -7 10 2082.17 445.196 3 14 -7 11 8308.21 707.374 3 14 -7 12 467.894 268.313 3 14 -7 13 9178.66 589.209 3 14 -8 -12 5886.31 492.896 4 14 -8 -11 1290.77 350.482 4 14 -8 -10 16001.7 975.315 4 14 -8 -9 601.846 315.217 4 14 -8 -8 32640.2 1452.94 4 14 -8 -7 815.139 375.953 4 14 -8 -6 59304.9 1893.67 4 14 -8 -5 2064.83 415.193 4 14 -8 -4 29752.0 1271.94 4 14 8 -4 31973.6 2289.38 1 14 8 -3 5296.60 953.343 1 14 8 -2 39034.9 2414.41 1 14 8 -1 1692.47 562.565 1 14 8 0 38437.9 2371.48 1 14 8 1 1372.52 609.219 1 14 8 2 42467.1 2576.68 1 14 -8 3 5169.05 552.595 4 14 8 3 3835.05 822.790 1 14 -8 4 32503.6 1348.06 4 14 -8 4 31433.9 1221.40 3 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1381.17 1 19 1 6 13461.3 758.058 3 19 -1 6 13467.8 794.071 3 19 -1 7 6452.43 611.063 2 19 1 7 5957.64 593.697 2 19 1 7 5373.88 506.568 3 19 -1 7 5583.70 544.642 3 19 -1 8 5607.08 600.257 2 19 1 8 4853.23 498.701 3 19 -1 8 4854.60 531.050 3 19 -1 9 2155.75 383.559 3 19 1 9 2425.01 389.636 3 19 1 10-116.436 232.357 3 19 -1 10 707.763 304.733 3 19 1 11 1435.93 333.306 3 19 -1 11 1226.20 338.458 3 19 -1 12 2607.92 387.576 3 19 1 12 2794.15 365.248 3 19 -1 13 1406.80 274.439 3 19 2 -1 24944.6 1625.11 1 19 2 0 23480.8 1560.54 1 19 2 1 16755.7 1351.43 1 19 2 2 11977.8 1170.84 1 19 2 3 30003.2 1868.85 1 19 2 4 17578.7 1506.63 1 19 2 5 10556.9 1240.84 1 19 2 5 8499.77 655.225 2 19 -2 6 16380.9 898.849 2 19 2 6 18290.9 984.050 2 19 -2 6 17557.1 922.166 3 19 2 6 19435.4 1739.07 1 19 -2 7 1539.83 296.165 2 19 2 7 1959.34 661.309 1 19 -2 7 1593.25 342.343 3 19 2 7 1579.49 295.051 3 19 -2 8 14577.6 892.955 2 19 2 8 14435.4 804.710 3 19 -2 8 15149.8 910.461 3 19 -2 9 7132.42 662.136 3 19 2 9 7571.14 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5522.65 567.903 3 19 -9 10 576.474 253.028 3 19 -9 11 2180.56 318.842 3 19 -9 12 1155.02 189.985 3 19 -10 -9 1100.52 265.158 4 19 -10 -8 5121.50 534.152 4 19 -10 -7 3982.55 500.800 4 19 -10 -6 11619.6 821.647 4 19 -10 -5 1682.62 372.289 4 19 -10 -4 9918.23 791.278 4 19 -10 -3 6813.62 673.128 4 19 -10 -2 6936.88 674.678 4 19 10 -2 7669.24 1316.96 1 19 -10 -1 11836.1 875.386 4 19 10 -1 8863.33 1406.88 1 19 -10 0 13660.4 931.033 4 19 10 0 16268.1 1866.23 1 19 -10 1 14645.2 894.578 2 19 -10 1 12486.9 902.951 4 19 10 1 11300.4 1550.44 1 19 -10 2 7066.08 629.147 2 19 -10 2 7014.22 692.085 4 19 10 2 6502.10 1228.05 1 19 -10 3 6341.24 601.868 3 19 -10 3 6641.43 689.655 4 19 -10 3 7218.54 640.046 2 19 -10 4 9249.10 713.343 3 19 -10 4 9019.36 691.943 2 19 -10 5 1969.12 406.552 3 19 -10 6 11568.8 804.451 3 19 -10 7 6042.99 597.098 3 19 -10 8 7075.33 617.876 3 19 -10 9 1267.19 308.864 3 19 -10 10 2046.16 299.315 3 19 -10 11 841.132 194.989 3 19 -11 -9 3637.23 370.721 4 19 -11 -8 4013.70 457.536 4 19 -11 -7 7733.35 637.526 4 19 -11 -6 2755.18 442.312 4 19 -11 -5 7105.95 681.190 4 19 -11 -4 9667.97 785.021 4 19 -11 -3 10107.2 815.940 4 19 -11 -2 11842.7 878.004 4 19 -11 -1 11778.5 877.730 4 19 -11 0-65.8026 267.184 4 19 -11 1 10720.6 862.054 4 19 -11 1 10735.2 775.068 2 19 -11 2 11229.8 877.167 4 19 -11 2 12570.9 821.318 2 19 -11 3 11009.4 880.264 4 19 -11 3 10525.7 745.769 2 19 -11 4 11337.7 744.172 2 19 -11 6 5498.59 531.380 3 19 -11 7 9135.49 646.389 3 19 -11 8 2478.50 343.578 3 19 -11 9 4510.21 402.482 3 19 -11 10 64.0444 90.4525 3 19 -12 -9 2190.34 262.266 4 19 -12 -8 4243.33 425.645 4 19 -12 -7 6395.85 562.582 4 19 -12 -6 4054.78 491.767 4 19 -12 -5 3925.27 513.036 4 19 -12 -4 3549.75 509.696 4 19 -12 -3 4146.54 545.937 4 19 -12 -2 5559.26 618.717 4 19 -12 -1 2353.83 444.973 4 19 -12 0 4459.27 516.704 2 19 -12 0 4746.48 609.679 4 19 -12 1 3521.90 479.819 2 19 -12 1 2499.89 473.945 4 19 -12 2 6639.24 702.931 4 19 -12 2 6254.25 584.576 2 19 -12 3 3379.30 522.578 4 19 -12 3 3711.19 452.105 2 19 -13 -8 466.387 172.055 4 19 -13 -7 453.999 222.266 4 19 -13 -6 2952.54 410.610 4 19 -13 -5 1053.06 342.378 4 19 -13 -4 770.878 308.805 4 19 -13 -3 3966.83 531.083 4 19 -13 -2 7666.67 698.029 4 19 -13 -1 395.976 265.498 4 19 -13 0 9478.15 707.315 2 19 -13 0 8461.63 757.611 4 19 -13 1 248.084 282.348 4 19 -13 1 217.980 214.599 2 19 -13 2 9624.65 676.783 2 19 -13 2 10129.4 819.731 4 19 -13 3 4307.01 574.758 4 19 -14 -8 447.225 131.986 2 19 -14 -7 1426.53 238.353 4 19 -14 -6-77.7220 166.963 4 19 -14 -5 1070.04 275.846 4 19 -14 -4-359.733 290.437 4 19 -14 -3 55.5603 242.726 4 19 -14 -2 620.425 313.999 4 19 -14 -1 577.171 282.493 4 19 -14 -1 1119.80 300.931 2 19 -14 0 593.358 331.010 4 19 -14 0 888.919 276.675 2 19 -14 1 1017.64 263.818 2 19 -14 1 931.454 341.701 4 19 -14 2 99.8745 168.433 2 19 -14 2 274.920 269.234 4 19 -15 -7 196.224 111.722 2 19 -15 -6 84.8611 126.675 4 19 -15 -6-319.271 153.463 2 19 -15 -5 557.397 216.989 4 19 -15 -5 339.860 177.242 2 19 -15 -4 323.177 196.653 4 19 -15 -4 386.723 193.590 2 19 -15 -3 107.322 211.853 4 19 -15 -3 464.079 200.532 2 19 -15 -2 112.155 226.203 4 19 -15 -2 240.216 193.560 2 19 -15 -1-83.7688 241.392 4 19 -15 -1 489.915 197.579 2 19 -15 0-70.6882 158.348 2 19 -15 0-193.454 217.015 4 19 -15 1-27.0194 159.285 2 19 -15 1 331.411 245.978 4 19 -16 -5 69.4276 107.172 2 19 -16 -4 201.493 149.856 4 19 -16 -4 429.653 158.065 2 19 -16 -3 25.7966 146.894 4 19 -16 -3 364.255 168.000 2 19 -16 -2 1402.42 251.326 4 19 -16 -2 1051.47 209.731 2 19 -16 -1 293.000 205.153 4 19 -16 -1 83.6622 137.295 2 19 -16 0 788.454 248.199 4 19 -16 0 651.943 147.227 2 20 0 -1 2133.69 448.770 1 20 0 0 39184.0 1835.55 1 20 0 1 778.392 318.668 1 20 0 2 132589. 3463.27 1 20 0 3 5421.75 714.335 1 20 0 5 9959.43 700.250 2 20 0 6 51618.8 1626.19 2 20 0 6 52201.6 1514.76 3 20 0 7 4873.20 559.854 2 20 0 7 5193.72 523.527 3 20 0 8 14845.4 942.932 2 20 0 8 15730.4 897.112 3 20 0 9 280.762 240.770 3 20 0 10 12862.0 820.098 3 20 0 11 3457.58 435.265 3 20 0 12 9628.03 631.178 3 20 0 13 164.857 151.637 3 20 1 -1 24671.5 1581.18 1 20 -1 -1 21537.6 1331.86 1 20 -1 0 16560.8 1112.65 1 20 1 0 18943.2 1392.91 1 20 1 1 19933.1 1404.27 1 20 1 2 17511.7 1350.87 1 20 1 3 87192.1 3097.21 1 20 1 4 285.074 268.753 1 20 1 5 51219.9 2558.44 1 20 -1 5 51978.8 1503.99 3 20 -1 5 53675.6 1578.69 2 20 1 5 49993.0 1559.89 2 20 -1 6 6251.18 588.758 2 20 1 6 5965.34 596.217 2 20 -1 6 7155.90 613.921 3 20 1 6 5748.34 516.321 3 20 1 7 23392.0 1150.00 2 20 -1 7 23032.7 1118.99 2 20 1 7 23757.0 1031.54 3 20 -1 7 22952.9 1073.99 3 20 -1 8 2000.05 402.703 2 20 1 8 2059.20 360.982 3 20 -1 8 2478.96 414.150 3 20 1 9 23453.3 1065.71 3 20 -1 9 24413.8 1147.89 3 20 1 10 321.359 221.948 3 20 -1 10 1372.44 344.615 3 20 -1 11 15332.7 874.449 3 20 1 11 15357.4 826.361 3 20 1 12 1289.99 265.317 3 20 -1 12 2023.11 343.792 3 20 -1 13 7191.59 495.649 3 20 2 -1 3015.92 672.149 1 20 2 0 46537.1 2251.00 1 20 2 1 4538.62 775.476 1 20 2 2 44743.3 2273.52 1 20 2 3 7746.55 1010.53 1 20 2 4 31676.9 2067.61 1 20 2 5 815.824 313.135 1 20 -2 5 1134.69 310.950 3 20 2 5 767.029 288.856 2 20 -2 5 895.010 296.593 2 20 2 6 21549.9 1079.13 2 20 -2 6 23668.5 1095.27 2 20 -2 6 23017.4 1072.18 3 20 2 6 19793.8 1772.42 1 20 -2 7 1326.02 321.038 2 20 2 7 1405.00 304.461 3 20 -2 7 1170.23 334.707 3 20 2 8 9065.91 649.173 3 20 -2 8 9056.39 725.125 3 20 -2 8 8842.14 729.901 2 20 2 9 2935.88 395.598 3 20 -2 9 3133.76 479.274 3 20 2 10 6385.48 542.894 3 20 -2 10 6565.07 643.418 3 20 -2 11 810.544 317.671 3 20 -2 12 6934.33 568.765 3 20 -2 13 241.934 181.445 3 20 3 -1 15407.4 1396.25 1 20 3 0-230.463 411.754 1 20 3 1 17394.2 1476.81 1 20 3 2 1754.86 575.323 1 20 3 3 2275.36 579.960 1 20 3 4 589.281 327.198 1 20 3 5 2212.70 650.631 1 20 -3 5 1479.10 332.118 2 20 3 5 748.489 240.829 2 20 -3 5 1596.50 346.582 3 20 3 6 2058.04 774.260 1 20 -3 6 1415.65 330.686 2 20 3 6 1501.57 377.211 2 20 -3 6 1803.72 387.560 3 20 3 7 3068.37 743.613 1 20 -3 7 3228.01 469.703 3 20 -3 7 2638.96 429.994 2 20 -3 8 1649.96 374.031 3 20 -3 8 2049.79 393.913 2 20 -3 9 956.034 345.743 3 20 -3 10-385.769 301.999 3 20 -3 11-185.978 289.208 3 20 -3 12 827.879 302.518 3 20 -3 13 314.191 184.554 3 20 4 -2 7382.66 1082.55 1 20 4 -1 1074.05 530.494 1 20 4 0 2907.56 686.562 1 20 4 1 1976.10 608.423 1 20 4 2 8444.41 1132.06 1 20 4 3 2230.44 669.199 1 20 4 4 969.532 487.198 1 20 -4 4 1444.40 296.003 2 20 4 4 1238.37 316.378 2 20 4 5 6288.91 1034.98 1 20 -4 5 5595.16 555.640 2 20 -4 5 6350.72 616.172 3 20 4 6 5351.77 1010.92 1 20 -4 6 4516.50 546.683 3 20 -4 6 4119.78 495.649 2 20 4 7 2057.94 447.456 1 20 -4 7 2684.25 452.338 3 20 -4 7 2340.87 406.185 2 20 -4 8 241.617 305.797 3 20 -4 8-135.028 272.309 2 20 -4 9 2089.36 438.057 3 20 -4 10 1151.15 336.201 3 20 -4 11 122.111 274.044 3 20 -4 12 247.114 229.069 3 20 -4 13 1438.28 267.130 3 20 5 -2 2370.01 708.163 1 20 5 -1 3466.06 814.999 1 20 5 0-160.101 345.001 1 20 5 1 7415.58 1092.58 1 20 5 2 908.664 468.382 1 20 -5 3 27098.7 1088.33 2 20 5 3 26536.2 2084.11 1 20 5 4 1689.13 673.460 1 20 -5 4 3488.62 423.233 2 20 -5 5 14097.8 843.191 2 20 -5 5 14179.4 895.320 3 20 5 5 13857.5 1592.99 1 20 -5 6 2137.45 394.451 2 20 -5 6 2160.14 417.640 3 20 5 6 2911.79 853.044 1 20 5 7 7785.48 1290.63 1 20 -5 7 7386.43 640.398 2 20 -5 7 7884.91 720.366 3 20 -5 8 156.032 280.085 3 20 -5 9 9014.37 753.625 3 20 -5 10 690.271 341.517 3 20 -5 11 5423.60 584.107 3 20 -5 12 658.720 260.033 3 20 -5 13 1570.08 258.868 3 20 6 -3 8631.72 1204.84 1 20 6 -2 27716.2 2141.15 1 20 6 -1 1081.67 562.724 1 20 6 0 49771.2 2816.70 1 20 6 1 1196.21 619.248 1 20 -6 1 781.102 242.584 2 20 -6 2 33346.1 1208.77 2 20 6 2 33272.5 2398.66 1 20 6 3 8258.31 1255.19 1 20 -6 3 9506.79 680.559 2 20 -6 4 12337.7 790.473 2 20 6 4 12616.6 1541.26 1 20 -6 5 6991.93 665.528 3 20 -6 5 6074.02 573.850 2 20 6 5 7008.41 1215.46 1 20 -6 6 29481.8 1223.48 2 20 -6 6 29321.7 1317.10 3 20 6 6 27006.4 2348.28 1 20 -6 7 2577.19 390.710 2 20 -6 7 2774.06 477.444 3 20 6 7 1757.23 502.217 1 20 -6 8 16130.2 1001.50 3 20 -6 9 503.437 343.389 3 20 -6 10 9623.27 766.766 3 20 -6 11 2623.65 431.241 3 20 -6 12 4997.38 471.160 3 20 -6 13 419.150 166.997 3 20 7 -5 22346.8 2147.81 1 20 7 -4 1189.64 464.750 1 20 7 -3 33490.1 2455.65 1 20 7 -2 2040.55 624.392 1 20 7 -1 44463.9 2808.19 1 20 7 0 16895.8 1750.64 1 20 7 1 43519.1 2806.99 1 20 -7 1 41742.9 1383.75 2 20 -7 2 1227.32 307.183 2 20 7 2 1899.31 708.340 1 20 7 3 36496.4 2628.52 1 20 -7 3 38233.8 1347.73 2 20 7 4-104.125 530.320 1 20 -7 4 557.265 254.791 3 20 -7 4 577.177 272.102 2 20 -7 5 22581.4 1085.79 2 20 -7 5 23134.9 1175.60 3 20 7 5 20303.4 2038.36 1 20 7 6 6462.20 1168.79 1 20 -7 6 5842.03 598.893 2 20 -7 6 5777.63 634.404 3 20 -7 7 12711.5 893.756 3 20 -7 8 9532.51 779.893 3 20 -7 9 16931.9 1004.68 3 20 -7 10 539.141 303.462 3 20 -7 11 11030.5 712.355 3 20 -7 12-90.6153 182.650 3 20 8 -5 1570.13 627.362 1 20 8 -4 21807.2 2103.64 1 20 8 -3 818.896 589.762 1 20 8 -2 11572.8 1507.73 1 20 8 -1 6254.34 1141.63 1 20 8 0 24814.4 2204.19 1 20 -8 1 6320.39 581.256 2 20 8 1 7418.13 1200.25 1 20 -8 2 9523.22 726.349 4 20 -8 2 10058.2 729.804 2 20 8 2 10390.9 1466.44 1 20 8 3-391.505 631.036 1 20 -8 3 241.453 211.160 2 20 -8 3 433.704 231.582 4 20 -8 4 20417.5 1102.97 3 20 8 4 19632.8 2058.92 1 20 -8 4 19896.9 1009.79 2 20 -8 5 2079.71 429.256 3 20 8 5 2416.57 716.850 1 20 -8 5 1709.28 354.357 2 20 -8 6 20976.1 1123.93 3 20 -8 7 636.319 277.020 3 20 -8 8 24515.1 1197.12 3 20 -8 9 341.066 289.678 3 20 -8 10 12846.1 797.093 3 20 -8 11 484.310 221.594 3 20 -8 12 5502.26 416.198 3 20 -9 -6 297.012 229.827 4 20 -9 -5 5111.19 557.609 4 20 9 -4 8776.44 1394.93 1 20 -9 -4 6474.38 627.138 4 20 9 -3 10980.2 1555.41 1 20 -9 -3 10380.8 773.871 4 20 -9 -2 3099.90 462.554 4 20 9 -2 3139.32 864.840 1 20 -9 -1 34573.8 1379.65 4 20 9 -1 39334.0 2854.65 1 20 -9 0 2873.64 454.951 4 20 9 0 2665.15 866.728 1 20 -9 1 33870.8 1382.40 4 20 -9 1 35313.7 1338.70 2 20 9 1 37784.7 2809.16 1 20 9 2 1890.91 737.651 1 20 -9 2 2410.94 429.327 2 20 -9 2 2136.32 433.127 4 20 -9 3 11962.2 796.278 2 20 -9 3 12063.4 862.485 4 20 -9 3 12305.3 862.244 3 20 9 3 11781.8 1638.62 1 20 -9 4 6345.80 624.014 3 20 -9 4 7065.39 620.841 2 20 9 4 6491.72 1262.10 1 20 -9 5 3719.73 509.406 3 20 -9 5 4467.13 506.314 2 20 -9 6 268.670 249.322 3 20 -9 7 7139.29 664.701 3 20 -9 8 1659.31 366.879 3 20 -9 9 6618.57 599.056 3 20 -9 10 1687.33 327.050 3 20 -9 11 2901.94 346.097 3 20 -10 -8 3897.17 446.334 4 20 -10 -7 1794.92 339.819 4 20 -10 -6 1115.79 329.595 4 20 -10 -5 3172.12 459.352 4 20 -10 -4 4435.28 538.200 4 20 -10 -3 1714.62 417.771 4 20 -10 -2 8961.66 753.845 4 20 -10 -1 758.170 310.956 4 20 10 -1 59.4371 576.313 1 20 -10 0 8748.92 746.286 4 20 10 0 9247.26 1458.77 1 20 -10 1-203.721 321.906 4 20 -10 1 365.160 271.247 2 20 -10 2 7415.40 650.027 3 20 -10 2 8813.15 763.854 4 20 -10 2 8825.11 708.270 2 20 -10 3 1451.46 389.719 4 20 -10 3 1664.53 328.894 3 20 -10 3 1493.34 328.547 2 20 -10 4 4698.97 529.486 2 20 -10 4 4538.83 518.459 3 20 -10 5 3098.21 457.721 3 20 -10 6 973.442 311.653 3 20 -10 7 1509.19 354.404 3 20 -10 8 4089.71 471.611 3 20 -10 9 995.469 283.255 3 20 -10 10 115.399 162.486 3 20 -10 11 13.1553 110.724 3 20 -11 -8-282.318 205.550 4 20 -11 -7 1420.29 318.825 4 20 -11 -6-126.544 275.772 4 20 -11 -5 1006.37 345.421 4 20 -11 -4 1284.32 339.424 4 20 -11 -3 635.698 288.291 4 20 -11 -2 1530.41 382.960 4 20 -11 -1 235.862 293.217 4 20 -11 0 506.873 298.298 4 20 -11 0 855.950 324.544 2 20 -11 1 676.616 344.196 4 20 -11 1 328.885 263.290 2 20 -11 2 2542.59 476.625 4 20 -11 2 1925.69 358.390 2 20 -11 3 1056.77 376.383 4 20 -11 3 819.723 294.840 2 20 -11 4 2125.26 369.978 2 20 -11 5 468.841 232.962 3 20 -11 6 424.919 220.524 3 20 -11 7 1711.35 319.682 3 20 -11 8 67.5130 172.911 3 20 -11 9 81.8315 147.072 3 20 -12 -9 95.9837 108.854 2 20 -12 -8 691.144 210.759 4 20 -12 -7-292.828 252.363 4 20 -12 -6 3308.39 441.596 4 20 -12 -5 586.684 276.878 4 20 -12 -4 1565.24 386.486 4 20 -12 -3 58.8263 249.839 4 20 -12 -2 1169.76 366.844 4 20 -12 -1 1595.15 414.853 4 20 -12 0 439.917 267.360 2 20 -12 0 603.930 321.047 4 20 -12 1 763.762 272.412 2 20 -12 1 1010.45 383.200 4 20 -12 2 1244.78 382.393 4 20 -12 2 644.407 270.575 2 20 -12 3 675.424 338.094 4 20 -12 3 556.943 230.847 2 20 -13 -8 326.746 149.066 2 20 -13 -7 1446.40 268.009 4 20 -13 -6 390.363 217.751 4 20 -13 -5 2114.26 367.099 4 20 -13 -4-81.9409 239.364 4 20 -13 -3 6390.32 620.190 4 20 -13 -2 173.247 268.846 4 20 -13 -1 7045.24 622.424 2 20 -13 -1 6851.73 668.553 4 20 -13 0 1007.79 344.725 4 20 -13 0 1191.17 312.534 2 20 -13 1 4758.65 509.873 2 20 -13 1 5833.23 629.507 4 20 -13 2-128.933 231.622 2 20 -13 2 294.302 311.893 4 20 -13 3 6997.80 555.645 2 20 -14 -7 810.750 188.779 2 20 -14 -6 1245.74 243.668 4 20 -14 -5 910.661 244.650 4 20 -14 -4 5625.98 513.151 4 20 -14 -3 758.848 275.476 4 20 -14 -2 6662.85 558.966 2 20 -14 -2 5459.62 545.885 4 20 -14 -1 792.354 288.959 4 20 -14 -1 1098.06 285.592 2 20 -14 0 12982.4 747.760 2 20 -14 0 13144.0 828.700 4 20 -14 1 1484.93 301.943 2 20 -14 1 1307.20 344.680 4 20 -14 2 6932.00 529.100 2 20 -14 2 6493.18 607.580 4 20 -15 -6 90.3859 123.178 2 20 -15 -5 4253.59 363.214 2 20 -15 -5 3435.84 331.658 4 20 -15 -4 632.660 214.349 4 20 -15 -4 1163.83 242.071 2 20 -15 -3 3723.30 384.096 2 20 -15 -3 3224.27 375.151 4 20 -15 -2 677.396 258.677 4 20 -15 -2 260.393 192.515 2 20 -15 -1 4130.31 456.106 4 20 -15 -1 4001.85 395.925 2 20 -15 0-53.6949 224.878 4 20 -15 0 222.177 189.900 2 20 -15 1 3954.37 446.939 4 20 -15 1 4169.42 376.272 2 20 -16 -4 3641.47 289.012 2 20 -16 -3 187.261 126.268 4 20 -16 -3 338.690 153.296 2 20 -16 -2 1828.62 268.092 4 20 -16 -2 1517.09 229.025 2 20 -16 -1 636.118 207.893 4 20 -16 -1 612.958 170.663 2 20 -16 0 1606.93 270.450 4 20 -16 0 557.284 137.824 2 21 0 -1 283.527 268.164 1 21 0 0 177.045 279.749 1 21 0 1 100.332 290.313 1 21 0 2 4.79736 340.640 1 21 0 5-5.43826 196.544 3 21 0 5 399.882 274.847 2 21 0 6 58.3105 192.220 3 21 0 6 57.2606 215.433 2 21 0 7 76.1530 271.446 2 21 0 7-25.2186 203.616 3 21 0 8 235.323 306.633 2 21 0 8 182.307 210.607 3 21 0 9 42.9763 214.091 3 21 0 10 26.6849 241.080 3 21 0 11 342.063 246.758 3 21 0 12-174.215 201.259 3 21 0 13-242.143 167.333 3 21 -1 -1 5008.14 679.626 1 21 1 -1 6207.01 857.829 1 21 1 0-273.002 257.545 1 21 1 1 5396.57 799.924 1 21 1 2 5324.07 798.457 1 21 1 3 15384.7 1332.00 1 21 1 4 914.841 298.163 2 21 -1 4 482.526 228.800 2 21 1 4 1148.81 473.747 1 21 -1 5 5144.86 517.368 3 21 -1 5 4201.60 488.973 2 21 1 5 4746.03 529.098 2 21 1 5 3677.60 405.040 3 21 1 6 4660.49 556.314 2 21 -1 6 5440.33 573.378 2 21 -1 6 5015.40 531.659 3 21 1 6 4486.49 465.257 3 21 1 7 876.139 256.572 3 21 1 7 317.156 257.743 2 21 -1 7-87.3314 251.574 2 21 -1 7 461.694 246.481 3 21 -1 8 1970.67 383.822 2 21 1 8 2679.18 389.846 3 21 -1 8 3287.25 464.311 3 21 -1 9 5595.46 586.574 3 21 1 9 5454.90 536.961 3 21 1 10 1673.24 320.830 3 21 -1 10 1530.16 369.363 3 21 -1 11 8943.16 673.817 3 21 1 11 9575.88 640.993 3 21 1 12 924.442 252.083 3 21 -1 12 470.738 212.702 3 21 -1 13 1052.99 234.341 3 21 2 -1 6724.17 949.236 1 21 2 0 76838.2 2982.47 1 21 2 1 8878.91 1036.94 1 21 2 2 36938.0 2131.90 1 21 2 3 2052.86 546.345 1 21 -2 4 30691.3 1183.20 2 21 2 4 31078.5 1224.35 2 21 2 4 30152.3 2046.37 1 21 -2 5 271.745 259.942 2 21 -2 5 129.694 207.800 3 21 2 5 100.361 241.076 2 21 2 5 254.679 378.725 1 21 -2 6 24275.1 1139.21 2 21 2 6 24269.5 1168.19 2 21 -2 6 23492.0 1097.90 3 21 -2 7 3717.93 503.681 2 21 -2 7 3870.19 488.389 3 21 2 7 3013.30 396.323 3 21 -2 8 19755.5 1070.09 2 21 2 8 21895.8 987.477 3 21 -2 8 20882.6 1083.09 3 21 2 9 277.032 202.609 3 21 -2 9-132.326 271.443 3 21 -2 10 2785.65 461.731 3 21 -2 11 556.791 273.419 3 21 -2 12 10074.2 653.030 3 21 -2 13 310.858 171.999 3 21 3 -2 6458.44 985.117 1 21 3 -1 58567.7 2725.74 1 21 3 0-69.9497 451.787 1 21 3 1 49044.5 2514.38 1 21 3 2 5084.61 866.820 1 21 3 3 40458.9 2395.12 1 21 3 4 1127.46 310.767 2 21 -3 4 654.057 239.868 2 21 -3 5 44871.6 1492.34 2 21 -3 5 41833.5 1460.84 3 21 3 5 43699.1 1522.52 2 21 3 5 44094.8 2646.20 1 21 3 6 3385.91 799.964 1 21 -3 6 2671.31 423.295 3 21 3 6 3269.13 496.208 2 21 -3 6 2840.54 455.650 2 21 -3 7 22800.9 1130.29 2 21 -3 7 22270.0 1125.82 3 21 -3 8 2542.74 422.305 2 21 -3 8 2373.54 425.779 3 21 -3 9 15968.6 977.543 3 21 -3 10 246.016 289.816 3 21 -3 11 20258.7 1001.77 3 21 -3 12 210.583 214.932 3 21 -3 13 8141.66 508.473 3 21 4 -2 52189.7 2731.76 1 21 4 -1 8102.35 1094.29 1 21 4 0 96075.6 3683.17 1 21 4 1 6697.32 1022.51 1 21 4 2 49976.3 2698.87 1 21 4 3 502.903 238.564 2 21 4 3 747.439 383.536 1 21 -4 3 1067.71 281.469 2 21 4 4 72748.7 1916.42 2 21 -4 4 74787.8 1863.45 2 21 4 4 73764.7 3474.77 1 21 4 5 195.374 462.745 1 21 -4 5 439.250 291.791 3 21 -4 5 901.939 271.200 2 21 -4 6 23337.4 1121.67 2 21 -4 6 22277.9 1125.26 3 21 4 6 19852.8 1949.78 1 21 4 7 4968.16 998.302 1 21 -4 7 6813.34 669.058 3 21 -4 7 6467.04 630.479 2 21 -4 8 19952.2 1098.95 3 21 -4 8 19226.3 1019.42 2 21 -4 9 2611.33 460.094 3 21 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447.190 1 21 -6 1 215.586 200.488 2 21 6 1 260.482 476.030 1 21 6 2 6669.10 1112.26 1 21 -6 2 7575.02 614.994 2 21 6 3 1414.89 669.620 1 21 -6 3 440.709 231.509 2 21 6 4 8135.80 1308.93 1 21 -6 4 9447.05 697.114 2 21 6 5 2171.24 727.622 1 21 -6 5 2094.72 421.257 3 21 -6 5 2499.88 423.835 2 21 -6 6 21944.6 1089.26 2 21 -6 6 26484.3 1266.33 3 21 6 6 23692.6 2226.33 1 21 -6 7-139.859 295.344 3 21 -6 7-442.390 311.308 2 21 -6 8 9377.64 787.158 3 21 -6 9 1151.40 377.889 3 21 -6 10 7982.87 698.783 3 21 -6 11 343.949 274.624 3 21 -6 12 3126.28 372.880 3 21 -6 13 115.291 118.401 3 21 7 -5-413.074 554.137 1 21 7 -4 1884.25 697.014 1 21 7 -3 3419.63 886.928 1 21 7 -2-9.27406 527.970 1 21 7 -1 7424.40 1194.17 1 21 7 0 971.490 420.057 1 21 -7 0 1899.15 330.952 2 21 -7 1 7016.44 610.252 2 21 7 1 7662.21 1219.38 1 21 -7 2 1033.47 330.380 2 21 7 2 123.119 363.871 1 21 -7 3 3054.28 440.578 2 21 7 3 2650.93 824.424 1 21 -7 4 1430.13 344.593 2 21 -7 4 1320.16 336.701 3 21 7 4 433.574 450.682 1 21 -7 5 343.392 246.696 2 21 -7 5 514.330 327.710 3 21 -7 6 1751.11 418.572 3 21 -7 6 2155.48 397.978 2 21 -7 7 1400.85 389.686 3 21 -7 8 786.669 337.585 3 21 -7 9 1599.81 380.984 3 21 -7 10 712.039 314.807 3 21 -7 11 699.456 261.830 3 21 -7 12 246.738 180.792 3 21 8 -4 1092.25 638.987 1 21 8 -3 1575.63 616.486 1 21 8 -2 2020.00 740.664 1 21 8 -1 511.430 424.229 1 21 -8 0 14613.9 871.678 2 21 8 0 16587.8 1851.20 1 21 8 1 270.199 401.888 1 21 -8 1 333.000 249.400 2 21 8 2 3176.64 878.400 1 21 -8 2 2454.39 416.568 2 21 8 3 1150.85 580.713 1 21 -8 3 537.491 273.558 4 21 -8 3 900.363 299.454 2 21 -8 4 361.407 236.204 2 21 -8 4 272.009 281.689 3 21 8 4-21.5512 544.064 1 21 -8 5 577.956 312.953 3 21 -8 5 462.215 238.843 2 21 -8 6 1432.58 392.819 3 21 -8 6 1356.38 310.145 2 21 -8 7 1337.67 380.103 3 21 -8 8 5599.78 606.165 3 21 -8 9 225.083 277.409 3 21 -8 10 747.775 327.912 3 21 -8 11-138.538 198.169 3 21 -8 12 823.611 197.504 3 21 9 -3 20851.8 2175.77 1 21 9 -2 2373.51 758.790 1 21 9 -1 10794.9 1547.68 1 21 -9 0 3069.81 449.419 4 21 9 0 3721.56 872.106 1 21 -9 0 3983.70 513.029 2 21 -9 1 9566.81 731.388 2 21 -9 1 9566.09 742.214 4 21 9 1 10691.6 1526.56 1 21 -9 2 1777.18 360.106 2 21 -9 2 2312.75 394.015 4 21 9 2 2568.29 848.443 1 21 -9 3 20693.2 1052.03 2 21 -9 3 18529.5 1045.74 4 21 -9 3 20129.0 1081.00 3 21 9 3 22321.3 2233.82 1 21 -9 4 1823.94 403.249 3 21 -9 4 2233.93 390.507 2 21 -9 5 4065.46 490.206 2 21 -9 5 3637.19 493.354 3 21 -9 6 1942.47 408.213 3 21 -9 7 2858.83 459.125 3 21 -9 8 638.715 329.019 3 21 -9 9 3493.50 441.773 3 21 -9 10 132.219 187.079 3 21 -9 11 1229.82 238.873 3 21 -10 -5 669.529 299.793 4 21 -10 -4 18424.9 1012.46 4 21 -10 -3 1111.18 325.981 4 21 -10 -2 16434.9 979.815 4 21 -10 -1 3423.64 491.448 4 21 -10 0 3076.10 463.660 4 21 -10 0 2914.44 471.077 2 21 -10 1 2606.42 441.747 4 21 -10 1 3002.88 463.431 2 21 -10 2 15630.2 923.371 3 21 -10 2 16716.3 998.889 4 21 -10 2 16902.8 962.924 2 21 -10 3 1397.17 388.140 4 21 -10 3 1671.62 359.967 3 21 -10 3 1744.35 374.008 2 21 -10 4 19016.4 1003.65 2 21 -10 4 18694.8 1014.42 3 21 -10 5 762.770 292.452 3 21 -10 5 763.172 266.323 2 21 -10 6 8561.57 681.607 3 21 -10 7 1202.37 327.208 3 21 -10 8 8992.16 655.234 3 21 -10 9 1304.91 293.333 3 21 -10 10 7734.64 501.963 3 21 -11 -9 5518.94 375.635 2 21 -11 -7 11402.2 691.921 4 21 -11 -6 418.522 239.806 4 21 -11 -5 11856.7 798.770 4 21 -11 -4 318.871 266.817 4 21 -11 -3 9140.23 742.389 4 21 -11 -2 350.708 276.825 4 21 -11 -1 18083.4 1037.18 4 21 -11 0 75.7634 270.015 2 21 -11 0 45.5153 246.110 4 21 -11 1 20655.6 1064.50 2 21 -11 1 18424.6 1060.93 4 21 -11 2 193.925 260.530 2 21 -11 2 439.905 293.178 4 21 -11 3 7526.54 637.958 2 21 -11 3 6947.70 699.229 4 21 -11 4 347.681 228.634 3 21 -11 4 174.025 205.233 2 21 -11 5 12137.0 754.467 3 21 -11 6 446.845 215.895 3 21 -11 7 13096.1 738.891 3 21 -11 8 812.401 226.796 3 21 -11 9 5790.36 417.590 3 21 -12 -9-109.536 99.2247 2 21 -12 -7 141.087 178.340 4 21 -12 -6 9087.80 633.761 4 21 -12 -5 1194.16 321.436 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1374.40 2 22 0 6 32013.3 1229.87 3 22 0 7 7288.95 700.357 2 22 0 7 7064.86 615.789 3 22 0 8 15350.1 967.824 2 22 0 8 15434.5 892.944 3 22 0 9 4647.19 515.671 3 22 0 10 11912.5 772.654 3 22 0 11 6836.10 568.137 3 22 0 12 7289.70 512.532 3 22 1 -1 12099.6 1196.34 1 22 1 0 9611.08 1042.26 1 22 1 1 12724.5 1183.03 1 22 1 2 34854.2 2004.94 1 22 1 3 49877.9 2444.18 1 22 1 4 14128.8 847.250 2 22 -1 4 14129.1 830.024 2 22 1 5 31529.2 1302.38 2 22 -1 5 28499.3 1175.47 3 22 -1 5 30476.5 1255.69 2 22 1 5 29043.0 1115.79 3 22 1 6 17928.6 1024.00 2 22 -1 6 16669.8 981.699 2 22 -1 6 16886.5 933.658 3 22 1 6 15771.2 851.119 3 22 -1 7 13887.0 918.451 2 22 1 7 14831.8 963.202 2 22 1 7 14491.5 825.194 3 22 -1 7 13581.4 857.272 3 22 -1 8 3823.02 519.706 2 22 1 8 4953.83 514.303 3 22 -1 8 5656.59 575.543 3 22 1 9 11431.4 755.515 3 22 -1 9 12049.1 826.031 3 22 -1 10 7842.18 661.798 3 22 1 10 8142.54 620.840 3 22 -1 11 12370.6 761.759 3 22 1 11 10945.9 667.522 3 22 -1 12 2847.98 347.535 3 22 -1 13 3679.83 322.736 3 22 2 -1 5009.27 844.755 1 22 2 0 11948.2 1257.64 1 22 2 1 4978.36 818.810 1 22 2 2 17508.1 1514.19 1 22 -2 3 7489.98 604.787 2 22 2 3 6114.87 952.272 1 22 2 4 7220.39 635.268 2 22 -2 4 8235.17 662.426 2 22 2 4 7394.67 1030.35 1 22 -2 5 2419.50 390.057 2 22 -2 5 2795.94 430.800 3 22 2 5 2133.32 416.528 2 22 2 5 2514.14 631.403 1 22 -2 6 11978.7 836.987 2 22 2 6 11673.3 843.410 2 22 -2 6 11086.6 785.769 3 22 -2 7 1804.28 386.590 3 22 -2 7 1361.77 382.189 2 22 2 7 1628.88 341.353 3 22 -2 8 7634.24 694.035 2 22 2 8 8099.18 606.922 3 22 -2 8 9356.59 746.001 3 22 -2 9 3165.48 475.816 3 22 -2 10 2025.21 403.527 3 22 -2 11 1143.68 322.044 3 22 -2 12 4096.45 430.201 3 22 -2 13 153.255 150.778 3 22 3 -2 1886.88 587.518 1 22 3 -1 13178.8 1350.84 1 22 3 0 6361.64 989.374 1 22 3 1 16967.8 1548.08 1 22 3 2 2314.55 665.844 1 22 -3 3 6754.73 572.686 2 22 3 3 5698.71 547.907 2 22 3 3 6615.00 1032.13 1 22 3 4 4942.50 544.800 2 22 -3 4 4843.01 512.971 2 22 3 4 5246.35 976.437 1 22 -3 5 4832.05 540.538 3 22 -3 5 4713.76 530.484 2 22 3 5 5726.45 613.631 2 22 3 5 3744.38 858.450 1 22 -3 6 1644.55 373.399 2 22 -3 6 1246.05 359.909 3 22 3 6 1420.90 370.514 2 22 -3 7 3570.39 502.750 2 22 -3 7 4021.41 528.164 3 22 -3 8-42.9985 282.902 2 22 -3 8 530.102 320.114 3 22 -3 9 2141.07 433.107 3 22 -3 10 196.367 274.699 3 22 -3 11 1191.24 317.528 3 22 -3 12 467.692 238.173 3 22 -3 13 1171.26 218.377 3 22 -4 -2 3678.38 410.536 2 22 4 -2 3447.22 844.571 1 22 4 -1 3094.54 762.766 1 22 4 0 2850.10 746.255 1 22 -4 1 4065.81 459.881 2 22 4 1 4100.09 858.415 1 22 -4 2 3629.69 438.523 2 22 4 2 3797.77 804.350 1 22 -4 3 4639.16 489.181 2 22 4 3 5612.11 560.223 2 22 4 3 5101.72 951.183 1 22 -4 4 3803.38 473.763 2 22 4 4 3220.55 468.540 2 22 4 4 4370.49 935.204 1 22 -4 5 3887.43 526.754 3 22 -4 5 4247.59 507.897 2 22 4 5 2623.20 633.422 1 22 -4 6 701.504 304.019 2 22 -4 6 1612.23 384.806 3 22 4 6 740.764 474.402 1 22 -4 7 574.672 264.372 2 22 -4 7 690.076 329.430 3 22 4 7 281.307 357.220 1 22 -4 8 1046.42 376.607 3 22 -4 8 1011.16 324.834 2 22 -4 9 669.564 338.664 3 22 -4 10 677.992 316.479 3 22 -4 11 195.822 254.706 3 22 -4 12 929.501 263.670 3 22 -4 13 139.900 145.750 3 22 5 -3 12063.7 1465.98 1 22 5 -2 21236.6 1895.65 1 22 5 -1 12909.0 1457.85 1 22 -5 -1 14246.4 804.822 2 22 -5 0 48.1555 182.336 2 22 5 0-213.134 533.561 1 22 -5 1 15475.3 841.050 2 22 5 1 14554.7 1575.62 1 22 -5 2 22651.8 1038.04 2 22 5 2 23974.8 2019.75 1 22 5 2 21822.6 1017.51 2 22 -5 3 11035.7 746.409 2 22 5 3 11127.0 1454.69 1 22 -5 4 3040.98 447.833 2 22 5 4 2867.01 777.358 1 22 -5 5 5385.28 616.022 3 22 -5 5 6187.94 599.984 2 22 5 5 6889.12 1181.68 1 22 -5 6 6098.34 644.237 3 22 -5 6 6580.51 637.168 2 22 5 6 5440.56 1007.30 1 22 -5 7 1361.19 399.471 3 22 -5 7 561.145 224.007 2 22 -5 8 2168.17 394.213 2 22 -5 8 2259.28 448.975 3 22 -5 9 4262.80 573.516 3 22 -5 10 2028.43 415.924 3 22 -5 11 2966.76 428.842 3 22 -5 12 1177.69 256.892 3 22 -5 13 215.540 145.992 3 22 6 -4 6679.77 1153.72 1 22 6 -3 9138.78 1276.93 1 22 6 -2 11162.6 1409.67 1 22 -6 -1 10296.4 711.694 2 22 6 -1 12003.6 1500.23 1 22 6 0 47126.5 2877.67 1 22 -6 0 45109.4 1448.61 2 22 6 1 11342.8 1430.33 1 22 -6 1 12508.7 785.288 2 22 6 2 13513.0 1567.39 1 22 -6 2 13335.5 811.143 2 22 6 3 11140.2 1447.12 1 22 -6 3 12443.5 799.139 2 22 -6 4 5343.17 551.901 2 22 6 4 5546.14 1080.39 1 22 -6 5 5523.57 610.806 3 22 -6 5 5653.38 585.082 2 22 6 5 4185.21 931.644 1 22 -6 6 12778.2 855.576 2 22 6 6 12674.8 1672.59 1 22 -6 6 12631.3 906.900 3 22 -6 7 5608.99 622.039 3 22 -6 7 5996.09 593.025 2 22 -6 8 7614.63 717.571 3 22 -6 9 8692.61 742.103 3 22 -6 10 4054.18 523.302 3 22 -6 11 3952.08 457.424 3 22 -6 12 2159.91 307.890 3 22 7 -5 9497.15 1425.49 1 22 7 -4 12691.6 1626.02 1 22 7 -3 33771.6 2582.33 1 22 7 -2 11904.1 1528.53 1 22 7 -1 20534.8 1997.70 1 22 7 0 18716.6 1919.80 1 22 -7 0 20832.9 1032.59 2 22 7 1 17740.7 1864.58 1 22 -7 1 20949.1 1032.24 2 22 7 2 9641.98 1423.09 1 22 -7 2 7602.95 652.924 2 22 7 3 38940.2 2783.68 1 22 -7 3 35942.7 1363.80 2 22 -7 4 13971.4 949.696 3 22 7 4 15387.7 1818.34 1 22 -7 4 14481.6 885.730 2 22 -7 5 14105.3 885.614 2 22 7 5 14844.2 1827.42 1 22 -7 5 14387.7 955.409 3 22 -7 6 12062.5 886.423 3 22 -7 6 10627.7 779.168 2 22 -7 7 5788.36 637.655 3 22 -7 7 5933.64 574.587 2 22 -7 8 5793.40 634.026 3 22 -7 9 9633.89 750.504 3 22 -7 10 6409.72 588.719 3 22 -7 11 3974.76 431.717 3 22 -7 12 2105.98 277.573 3 22 8 -4 15873.0 1898.16 1 22 8 -3 1926.88 827.472 1 22 8 -2 15765.3 1840.20 1 22 8 -1 18103.7 1926.95 1 22 -8 0 11691.9 806.277 2 22 8 0 9966.23 1453.61 1 22 -8 1 18658.6 1006.45 2 22 8 1 18602.0 1971.19 1 22 -8 2 14069.2 874.678 2 22 8 2 13724.4 1719.66 1 22 8 3 2767.82 769.083 1 22 -8 3 3784.15 495.749 2 22 -8 4 11817.2 858.166 3 22 8 4 11704.5 1598.49 1 22 -8 4 12661.5 833.292 2 22 -8 5 7207.04 637.220 2 22 -8 5 6994.17 683.117 3 22 -8 6 12792.0 826.994 2 22 -8 6 12058.9 880.283 3 22 -8 7 3180.13 470.488 3 22 -8 8 6963.16 650.552 3 22 -8 9 2945.21 454.807 3 22 -8 10 4609.75 482.539 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236.244 2 22 -10 6 407.788 259.516 3 22 -10 7 1729.76 360.843 3 22 -10 8 844.102 280.517 3 22 -10 9 178.778 196.288 3 22 -10 10 1000.50 216.480 3 22 -11 -9-78.4108 112.723 2 22 -11 -8 241.235 158.950 2 22 -11 -4 274.618 241.090 4 22 -11 -3 915.372 311.557 4 22 -11 -2 333.720 300.898 4 22 -11 -1 356.035 273.029 2 22 -11 -1 158.915 257.224 4 22 -11 0 534.154 324.004 2 22 -11 0 521.928 275.876 4 22 -11 1-47.3973 248.656 2 22 -11 1-16.8971 256.702 4 22 -11 2 183.521 257.352 4 22 -11 2-213.258 243.580 2 22 -11 3 1559.67 341.149 2 22 -11 4 297.733 228.604 3 22 -11 4 268.181 246.662 2 22 -11 5 44.3074 226.741 3 22 -11 6 583.888 221.545 3 22 -11 7 381.294 216.778 3 22 -11 8-26.1990 166.878 3 22 -11 9 604.060 165.028 3 22 -12 -8 911.283 187.955 2 22 -12 -5 942.742 284.004 4 22 -12 -4 111.581 222.433 4 22 -12 -3 2288.04 379.340 4 22 -12 -2-21.9266 267.332 4 22 -12 -2 165.384 254.814 2 22 -12 -1 2333.76 418.322 4 22 -12 -1 2561.38 443.602 2 22 -12 0 1037.52 332.660 4 22 -12 0 1137.78 328.231 2 22 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1947.81 349.179 4 22 -14 1 1351.68 267.997 2 22 -14 1 1337.49 307.794 4 22 -14 2 2733.21 330.057 2 22 -15 -5 1638.92 224.262 2 22 -15 -4 3308.99 324.250 2 22 -15 -3 1050.11 218.809 4 22 -15 -3 1380.17 238.209 2 22 -15 -2 1714.05 259.456 4 22 -15 -2 2744.76 316.383 2 22 -15 -1 3350.96 363.319 4 22 -15 -1 4255.38 383.189 2 22 -15 0 961.038 243.407 4 22 -15 0 927.248 207.275 2 22 -15 1 3521.68 330.030 2 22 -16 -3 645.695 139.283 2 22 -16 -2 1079.54 175.648 2 22 -16 -1 939.465 160.956 2 23 0 -1-121.431 277.536 1 23 0 0 271.935 228.308 1 23 0 3-72.7820 203.185 2 23 0 4 208.490 236.515 2 23 0 5 8.17301 200.969 3 23 0 5-30.9940 222.723 2 23 0 6 108.594 227.746 3 23 0 6 382.936 276.425 2 23 0 7 124.021 199.970 3 23 0 7 240.714 292.418 2 23 0 8 77.3226 219.169 3 23 0 8 112.314 263.500 2 23 0 9 68.9524 234.043 3 23 0 10 42.1245 207.313 3 23 0 11 480.791 238.370 3 23 0 12-51.9394 182.493 3 23 1 -2 5705.36 904.738 1 23 1 -1 1907.80 502.247 1 23 1 0 21073.2 1588.24 1 23 1 1 1592.08 529.141 1 23 1 2 6996.53 890.484 1 23 -1 3 2803.45 414.213 2 23 1 3 2584.94 381.795 2 23 -1 4 9328.63 703.191 2 23 1 4 7717.79 668.408 2 23 1 5 3387.20 495.023 2 23 -1 5 3893.43 508.785 2 23 -1 5 3400.10 460.780 3 23 1 5 3564.25 430.843 3 23 1 6 6723.06 678.554 2 23 -1 6 6145.95 618.698 2 23 -1 6 6522.59 616.805 3 23 1 6 5428.72 518.386 3 23 1 7 777.166 283.974 3 23 -1 7 969.333 325.534 3 23 1 7 981.758 351.556 2 23 -1 7 1128.62 335.757 2 23 -1 8 7846.65 718.406 2 23 1 8 8017.57 633.438 3 23 -1 8 8015.65 673.325 3 23 1 9 4926.76 522.520 3 23 -1 9 4804.25 534.562 3 23 1 10 633.094 223.951 3 23 -1 10 446.268 278.581 3 23 1 11 852.238 251.270 3 23 -1 11 495.386 231.428 3 23 -1 12 2762.10 338.829 3 23 -1 13 112.861 123.037 3 23 2 -2 8416.00 1096.02 1 23 2 -1 20303.7 1660.67 1 23 2 0 4938.93 834.698 1 23 2 1 20784.4 1650.21 1 23 -2 2 11119.5 715.232 2 23 2 2 10075.8 1165.53 1 23 2 3 33497.9 1277.78 2 23 -2 3 33412.9 1258.74 2 23 2 3 32125.4 2121.17 1 23 -2 4 5497.04 565.238 2 23 2 4 5232.07 559.978 2 23 2 4 7122.84 1049.30 1 23 2 5 20015.7 1069.92 2 23 -2 5 20508.5 1045.38 3 23 -2 5 19715.1 1042.06 2 23 -2 6 6456.76 618.434 3 23 -2 6 6061.80 630.479 2 23 2 6 6604.65 677.822 2 23 -2 7 10074.3 766.082 3 23 -2 7 9445.78 777.067 2 23 -2 8 766.441 345.287 3 23 -2 8 452.378 297.099 2 23 -2 9 7735.94 687.019 3 23 -2 10 241.632 248.416 3 23 -2 11 11846.3 736.776 3 23 -2 12 763.980 230.612 3 23 -2 13 3784.28 311.291 3 23 -3 -4 35503.1 1183.70 2 23 -3 -3 10228.4 663.461 2 23 3 -2 26309.2 2005.44 1 23 -3 -2 26121.8 1025.03 2 23 3 -1 4591.00 883.859 1 23 3 0 58945.7 2885.24 1 23 -3 0 55960.2 1524.02 2 23 3 1 8442.88 1119.55 1 23 -3 1 6983.29 572.885 2 23 3 2 28515.2 1160.55 2 23 3 2 28750.9 2072.18 1 23 -3 2 28118.7 1133.32 2 23 3 3 10131.5 1276.22 1 23 -3 3 10490.3 734.025 2 23 3 3 9015.33 684.252 2 23 3 4 35135.0 2366.47 1 23 -3 4 37800.8 1390.36 2 23 3 4 36962.2 1415.74 2 23 3 5 10854.1 1387.49 1 23 3 5 11242.0 827.018 2 23 -3 5 11277.7 796.106 2 23 -3 5 11080.4 798.195 3 23 -3 6 10608.6 802.248 2 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282.983 3 23 -8 9 2958.45 434.105 3 23 -8 10 424.684 224.633 3 23 -8 11 315.267 165.476 3 23 -9 -8 6397.31 484.137 2 23 -9 -1 275.928 273.621 2 23 -9 0 3773.22 505.663 2 23 -9 1 233.830 253.343 2 23 -9 2 2655.57 448.623 2 23 -9 3 616.156 317.364 3 23 -9 3 725.187 271.320 2 23 -9 4 11553.9 836.429 3 23 -9 4 10832.7 794.417 2 23 -9 5 673.554 266.780 3 23 -9 5 684.747 293.830 2 23 -9 6 7622.26 638.686 2 23 -9 6 8028.90 697.457 3 23 -9 7 1040.82 324.857 3 23 -9 8 7701.00 639.947 3 23 -9 9-50.8026 214.178 3 23 -9 10 2455.97 326.587 3 23 -9 11 109.563 119.518 3 23 -10 -8 915.496 214.305 2 23 -10 -1 17931.4 1009.99 2 23 -10 0 3038.09 473.680 2 23 -10 1 20951.1 1080.10 2 23 -10 2 2078.17 392.562 2 23 -10 2 2098.47 391.146 3 23 -10 2 2365.96 417.633 4 23 -10 3 7558.33 662.778 2 23 -10 3 6435.05 604.937 3 23 -10 4 802.561 293.198 2 23 -10 4 1146.48 328.430 3 23 -10 5 8372.69 664.225 2 23 -10 5 7145.46 636.905 3 23 -10 6 1359.44 334.730 3 23 -10 7 7306.04 602.612 3 23 -10 8 1019.47 272.367 3 23 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481.101 2 23 -13 -7 1082.60 197.265 2 23 -13 -6 1926.95 285.161 2 23 -13 -5 1119.38 266.642 2 23 -13 -4 3418.32 414.172 2 23 -13 -3 674.276 238.777 4 23 -13 -3 1510.54 329.042 2 23 -13 -2 5663.75 544.212 2 23 -13 -2 4979.99 486.341 4 23 -13 -1 2156.83 361.702 4 23 -13 -1 2949.60 409.808 2 23 -13 0 460.218 235.376 2 23 -13 0 43.7636 213.515 4 23 -13 1 3074.96 412.452 2 23 -13 1 2805.97 403.949 4 23 -13 2 4346.82 448.931 2 23 -13 3 1427.03 266.420 2 23 -14 -6 291.136 142.699 2 23 -14 -5 113.325 160.467 2 23 -14 -4 129.319 199.438 2 23 -14 -3 405.968 179.673 4 23 -14 -3 271.799 209.173 2 23 -14 -2 302.659 193.897 4 23 -14 -2 61.7017 187.698 2 23 -14 -1-129.076 213.086 4 23 -14 -1 343.938 206.313 2 23 -14 0 1579.84 312.063 4 23 -14 0 1302.92 280.257 2 23 -14 1 362.416 212.275 2 23 -14 2 500.018 195.254 2 23 -15 -5 242.962 127.034 2 23 -15 -4 228.099 139.765 2 23 -15 -3 213.209 165.492 2 23 -15 -2 209.492 117.870 4 23 -15 -2 1154.95 227.770 2 23 -15 -1 376.079 176.498 4 23 -15 -1 314.261 156.741 2 23 -15 0 239.235 154.291 2 23 -15 1-18.5891 140.940 2 24 0 -2 294.153 303.437 1 24 0 2 270.793 189.442 2 24 0 3 46534.1 1517.98 2 24 0 4 2938.44 422.152 2 24 0 5 33006.3 1369.19 2 24 0 5 32721.6 1262.04 3 24 0 6 616.306 334.705 2 24 0 6 198.425 213.917 3 24 0 7 31685.7 1400.51 2 24 0 7 29740.1 1219.10 3 24 0 8 109.142 209.435 3 24 0 9 18762.9 970.077 3 24 0 10 1808.46 348.153 3 24 0 11 18476.3 829.278 3 24 0 12 461.737 181.487 3 24 1 -2 38016.5 2247.82 1 24 1 -1 7082.98 974.064 1 24 1 0 50749.3 2492.57 1 24 -1 1 7155.43 578.248 2 24 1 1 7019.45 942.279 1 24 -1 2 37802.1 1333.13 2 24 1 2 38273.4 1344.58 2 24 -1 3 1929.42 371.922 2 24 1 3 1808.58 390.308 2 24 -1 4 15932.5 933.663 2 24 1 4 14863.8 909.109 2 24 1 5 4028.67 550.595 2 24 1 5 2641.78 400.643 3 24 -1 5 2728.05 424.600 3 24 -1 5 2931.29 457.959 2 24 1 6 26500.0 1111.11 3 24 -1 6 27129.5 1194.09 3 24 1 6 27090.5 1298.46 2 24 -1 6 26622.8 1264.04 2 24 -1 7 1013.35 320.617 3 24 1 7 334.614 294.480 2 24 1 7 245.499 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572.022 344.348 2 24 -2 9 9667.23 738.596 3 24 -2 10 85.0382 234.746 3 24 -2 11 8090.98 599.291 3 24 -2 12 132.559 157.768 3 24 -3 -4 4816.71 479.707 2 24 -3 -3 2343.14 363.760 2 24 3 -3 1025.29 577.849 1 24 3 -2 4930.85 957.540 1 24 -3 -2 5574.97 501.856 2 24 3 -1 2429.69 673.339 1 24 -3 -1 2397.95 356.150 2 24 3 0 44.6188 390.185 1 24 -3 0 700.012 263.055 2 24 -3 1 3267.61 426.857 2 24 3 1 2875.84 386.489 2 24 3 2 3550.82 787.937 1 24 -3 2 4175.58 479.277 2 24 3 2 4229.32 481.964 2 24 3 3 1394.03 527.062 1 24 -3 3 1892.71 369.743 2 24 3 3 2009.99 392.838 2 24 3 4 4467.83 831.250 1 24 3 4 5543.81 599.777 2 24 -3 4 6914.25 631.625 2 24 3 5 109.688 275.237 2 24 -3 5 287.042 280.837 3 24 -3 5 327.396 277.611 2 24 -3 6 2965.41 471.262 3 24 -3 6 2146.60 407.777 2 24 -3 7 625.926 316.964 3 24 -3 7 527.046 327.934 2 24 -3 8 1422.76 363.415 2 24 -3 8 2038.38 419.885 3 24 -3 9 1235.08 368.187 3 24 -3 10 1419.84 363.617 3 24 -3 11 329.988 242.722 3 24 -3 12 545.636 203.213 3 24 -4 -5 782.518 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471.524 2 24 -13 -3 161.565 208.475 2 24 -13 -2 5092.59 498.832 2 24 -13 -1-229.221 201.933 4 24 -13 -1-33.4292 241.898 2 24 -13 0 5105.39 487.288 4 24 -13 0 6197.41 539.300 2 24 -13 1-34.5736 204.644 2 24 -13 2 3992.73 422.427 2 24 -13 3-141.170 182.165 2 24 -14 -6 558.731 140.838 2 24 -14 -5 4372.55 358.007 2 24 -14 -4 609.138 198.420 2 24 -14 -3 1854.59 283.979 2 24 -14 -2 329.783 192.944 2 24 -14 -1 5634.60 467.567 2 24 -14 -1 4711.46 419.584 4 24 -14 0-66.3929 168.160 2 24 -14 1 5034.49 432.182 2 24 -14 2 356.478 151.890 2 24 -15 -4 3640.02 294.577 2 24 -15 -3 81.2280 130.902 2 24 -15 -2 3768.54 326.672 2 24 -15 -1 75.5375 141.111 2 24 -15 0 2026.15 250.819 2 24 -15 1-7.86273 110.968 2 25 0 -1 382.078 215.437 2 25 0 0 179.810 184.043 2 25 0 1 298.454 243.492 2 25 0 2 157.876 217.475 2 25 0 3-79.8814 246.621 2 25 0 4-119.044 258.623 2 25 0 5 219.847 224.973 3 25 0 5-24.6069 245.220 2 25 0 6 45.2468 265.820 2 25 0 6 137.567 216.397 3 25 0 7-242.916 287.424 2 25 0 7 188.359 236.908 3 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37334.0 2480.52 1 25 -3 -2 37242.5 1285.10 2 25 3 -1 2935.71 659.899 1 25 -3 -1 5796.09 536.842 2 25 3 0 18711.1 1715.04 1 25 -3 0 17625.5 911.609 2 25 3 1 3466.98 755.108 1 25 -3 1 4358.81 478.587 2 25 3 1 4755.70 503.837 2 25 3 2 40249.2 2536.74 1 25 3 2 39337.2 1416.01 2 25 -3 2 40403.7 1421.93 2 25 3 3 13825.1 1493.83 1 25 3 3 14570.8 903.342 2 25 -3 3 13599.0 866.428 2 25 -3 4 17441.2 996.145 2 25 3 4 17537.9 1023.12 2 25 -3 5 11569.5 837.533 3 25 -3 5 10634.9 814.294 2 25 3 5 11544.9 856.090 2 25 -3 6 17518.0 1018.99 3 25 -3 6 17172.9 1027.52 2 25 -3 7 10168.7 793.472 3 25 -3 7 9796.22 798.444 2 25 -3 8 9622.03 771.783 3 25 -3 8 9265.04 760.951 2 25 -3 9 3580.58 499.082 3 25 -3 10 7629.97 620.537 3 25 -3 11 1890.37 307.543 3 25 -3 12 3251.50 337.653 3 25 4 -4 720.662 396.657 1 25 -4 -4 1181.78 292.111 2 25 4 -3 33405.8 2473.70 1 25 -4 -3 29759.0 1172.34 2 25 4 -2 5394.44 1020.34 1 25 -4 -2 5499.77 542.129 2 25 4 -1 45863.1 2792.42 1 25 -4 -1 43457.3 1429.19 2 25 4 0 21404.0 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1114.70 1 25 -6 3 2112.75 413.154 2 25 -6 4 2607.93 506.711 3 25 6 4 3355.24 989.481 1 25 -6 4 3229.70 495.928 2 25 -6 5 4806.92 609.151 3 25 -6 5 4897.30 599.870 2 25 -6 6-15.1017 285.404 3 25 -6 6-141.784 271.236 2 25 -6 7 11814.3 879.015 3 25 -6 7 11369.9 799.210 2 25 -6 8 140.520 286.700 3 25 -6 8 169.852 208.680 2 25 -6 9 2187.37 413.931 3 25 -6 10 1365.91 318.423 3 25 -6 11 1013.63 261.292 3 25 -6 12 469.928 152.988 3 25 -7 -7 523.224 221.594 2 25 -7 -6 169.404 209.010 2 25 -7 -5 378.803 218.177 2 25 -7 -4 1912.03 389.344 2 25 7 -3 1813.76 672.794 1 25 -7 -3 2314.18 425.300 2 25 7 -2 3467.30 879.231 1 25 -7 -2 4779.95 552.116 2 25 7 -1-1384.55 615.488 1 25 -7 -1-350.662 323.910 2 25 7 0 3605.94 942.771 1 25 -7 0 3104.45 466.807 2 25 7 1-306.806 329.006 1 25 -7 1-137.460 314.623 2 25 7 2 3700.32 934.588 1 25 -7 2 3941.38 520.200 2 25 7 3 1740.15 726.620 1 25 -7 3 2554.97 435.541 2 25 -7 4 1711.50 392.565 2 25 -7 4 1492.01 418.913 3 25 -7 5 599.865 291.051 2 25 -7 5 317.614 288.086 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296.174 2 25 -9 -2 3550.79 512.940 2 25 -9 -1 3799.36 531.483 2 25 -9 0 260.021 300.294 2 25 -9 1 2799.39 430.242 2 25 -9 2 2726.67 447.074 2 25 -9 3 467.235 302.150 2 25 -9 3 556.054 302.152 3 25 -9 4 3744.76 506.907 2 25 -9 4 3825.05 517.253 3 25 -9 5 3040.40 438.351 2 25 -9 5 3474.90 486.072 3 25 -9 6 2449.20 388.839 2 25 -9 6 2339.04 422.694 3 25 -9 7 559.490 287.707 3 25 -9 8 1648.68 336.366 3 25 -9 9 1193.38 271.638 3 25 -9 10 2503.68 292.912 3 25 -10 -8 1184.45 210.698 2 25 -10 -7 6151.11 478.964 2 25 -10 -6 3933.08 448.938 2 25 -10 -5 11055.8 733.173 2 25 -10 -4 3282.30 454.076 2 25 -10 -3 4661.17 551.498 2 25 -10 -2 999.819 343.182 2 25 -10 -1 5544.27 612.767 2 25 -10 0 1915.95 421.562 2 25 -10 1 6047.97 622.835 2 25 -10 2 1718.72 376.029 2 25 -10 2 1215.99 316.931 3 25 -10 3 4490.48 535.823 2 25 -10 3 3909.91 492.572 3 25 -10 4 3138.63 457.759 2 25 -10 4 2995.84 434.069 3 25 -10 5 9863.12 705.285 2 25 -10 5 8869.16 695.923 3 25 -10 6 3788.11 445.238 3 25 -10 7 5719.02 520.203 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504.455 161.849 2 25 -13 -5 367.286 187.432 2 25 -13 -4 3447.04 386.122 2 25 -13 -3-57.1247 207.857 2 25 -13 -2 3094.96 398.074 2 25 -13 -1 1939.94 342.303 2 25 -13 0 2473.83 368.841 2 25 -13 1 1887.12 336.188 2 25 -13 2 3566.86 401.814 2 25 -13 3 30.7087 182.244 2 25 -14 -5 1601.13 221.371 2 25 -14 -4 114.169 155.242 2 25 -14 -3 735.652 208.051 2 25 -14 -2 187.157 181.209 2 25 -14 -1 1397.77 265.683 2 25 -14 0 100.198 157.921 2 25 -14 1 1353.48 245.593 2 25 -14 2 179.688 147.475 2 25 -15 -4-48.6060 93.0783 2 25 -15 -3 474.404 148.084 2 25 -15 -2-140.169 132.645 2 25 -15 -1 26.1387 119.338 2 25 -15 0 58.2862 120.645 2 25 -15 1-30.4099 105.933 2 26 0 -1 11947.7 731.987 2 26 0 0 47235.0 1467.33 2 26 0 1 6003.62 570.067 2 26 0 2 37035.2 1384.95 2 26 0 3 1588.30 355.958 2 26 0 4 5354.19 593.694 2 26 0 5 13543.0 844.968 3 26 0 5 14131.7 946.641 2 26 0 6 18822.6 984.475 3 26 0 6 17567.7 1068.57 2 26 0 7 14879.6 881.053 3 26 0 7 13860.1 969.060 2 26 0 8 18205.0 943.597 3 26 0 9 11862.9 745.867 3 26 0 10 5459.55 479.067 3 26 0 11 1650.17 262.677 3 26 1 -3 17642.1 1652.17 1 26 -1 -2 12830.0 759.814 2 26 1 -2 13566.9 1388.84 1 26 1 -1 16810.6 860.883 2 26 -1 -1 14874.8 827.418 2 26 1 0 53682.9 1569.76 2 26 -1 0 52024.9 1549.88 2 26 1 1 14544.9 852.058 2 26 -1 1 14909.8 866.056 2 26 1 2 12337.1 817.051 2 26 -1 2 13217.6 853.888 2 26 1 3 15836.4 935.894 2 26 -1 3 16158.1 953.700 2 26 1 4 19819.0 1084.87 2 26 -1 4 18269.4 1039.80 2 26 -1 5 16613.8 1010.24 2 26 1 5 17593.9 1056.70 2 26 -1 5 15370.6 928.313 3 26 1 5 16858.0 905.648 3 26 1 6 3827.79 561.013 2 26 -1 6 3341.66 524.629 2 26 1 6 3541.03 454.489 3 26 -1 6 4256.35 519.667 3 26 1 7 9965.88 829.561 2 26 -1 7 9518.57 800.314 2 26 -1 7 10334.7 773.519 3 26 1 7 10078.0 706.923 3 26 -1 8 9992.64 798.403 2 26 1 8 9258.46 666.413 3 26 -1 8 8722.00 697.887 3 26 1 9 6442.53 538.762 3 26 -1 9 6202.80 572.629 3 26 -1 10 3173.71 407.838 3 26 1 10 2722.75 358.288 3 26 -1 11 7187.05 510.243 3 26 -1 12 2978.51 281.680 3 26 2 -3 4296.93 881.504 1 26 -2 -3 4709.41 480.357 2 26 2 -2 4075.23 841.464 1 26 -2 -2 4698.08 491.656 2 26 2 -1 14701.3 1521.42 1 26 -2 -1 14531.3 836.731 2 26 2 0 7563.09 1053.00 1 26 2 0 7672.04 604.457 2 26 -2 0 7457.53 615.726 2 26 -2 1 16283.0 914.174 2 26 2 1 15867.4 895.025 2 26 2 1 16702.7 1588.62 1 26 2 2 2894.37 413.048 2 26 -2 2 3549.41 460.974 2 26 2 3 4669.07 553.145 2 26 -2 3 4681.31 557.283 2 26 2 4 7106.86 686.398 2 26 -2 4 6921.03 668.031 2 26 -2 5 1342.57 330.332 3 26 2 5 1519.32 379.823 2 26 -2 5 940.079 338.005 2 26 -2 6 10827.9 809.859 3 26 2 6 11602.5 884.779 2 26 -2 6 12188.7 891.040 2 26 -2 7 3144.15 473.833 3 26 -2 7 3073.66 507.815 2 26 -2 8 7619.76 669.509 3 26 -2 8 7205.66 692.279 2 26 -2 9 1678.27 357.201 3 26 -2 10 3267.27 420.187 3 26 -2 11 1382.15 270.311 3 26 -2 12 772.193 177.684 3 26 3 -4 27.8992 380.588 1 26 -3 -4 785.737 248.108 2 26 3 -3 446.063 435.672 1 26 -3 -3 1752.66 315.963 2 26 3 -2 9165.37 1279.70 1 26 -3 -2 7476.50 611.636 2 26 3 -1 4271.21 854.424 1 26 -3 -1 4037.84 472.986 2 26 3 0 5819.78 557.203 2 26 3 0 6167.04 982.837 1 26 -3 0 6026.28 562.010 2 26 3 1 3810.79 463.281 2 26 3 1 4641.42 919.410 1 26 -3 1 3841.18 483.158 2 26 -3 2 6906.81 645.358 2 26 3 2 7702.64 669.487 2 26 3 2 6588.28 1029.53 1 26 3 3 2795.56 453.411 2 26 -3 3 1550.55 391.288 2 26 3 4 505.081 287.541 2 26 -3 4 442.160 293.297 2 26 -3 5 2981.48 480.918 3 26 3 5 3055.89 525.197 2 26 -3 5 2680.83 470.010 2 26 -3 6 1972.88 426.537 3 26 -3 6 2049.09 434.672 2 26 -3 7 2179.94 458.445 2 26 -3 7 2418.83 448.091 3 26 -3 8 648.981 297.511 2 26 -3 8 292.693 256.678 3 26 -3 9 1318.25 349.590 3 26 -3 10 815.239 289.095 3 26 -3 11 386.579 212.912 3 26 -3 12 382.096 155.553 3 26 4 -5 661.914 385.909 1 26 4 -4 112.926 441.050 1 26 -4 -4 1634.55 318.559 2 26 4 -3 1121.14 560.321 1 26 -4 -3 984.272 270.254 2 26 4 -2 655.963 442.925 1 26 -4 -2 1085.19 279.633 2 26 4 -1 2085.09 693.259 1 26 -4 -1 1846.97 358.897 2 26 4 0 16136.4 1701.74 1 26 -4 0 13911.6 848.591 2 26 4 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26 -9 9 2960.54 335.082 3 26 -9 10 2223.93 255.845 3 26 -10 -8 492.981 146.906 2 26 -10 -7 1709.56 272.479 2 26 -10 -6 519.900 226.000 2 26 -10 -5 1221.99 300.722 2 26 -10 -4 1534.09 342.856 2 26 -10 -3 4749.12 552.853 2 26 -10 -2 1642.39 386.129 2 26 -10 -1 455.432 287.514 2 26 -10 0 383.153 263.566 2 26 -10 1 590.264 319.551 2 26 -10 2 882.704 294.141 3 26 -10 2 1166.32 342.453 2 26 -10 3 2931.08 433.764 3 26 -10 3 3606.36 486.444 2 26 -10 4 1569.85 359.413 3 26 -10 4 1545.62 353.978 2 26 -10 5 1957.93 371.276 3 26 -10 5 1705.97 354.633 2 26 -10 6 597.575 246.308 3 26 -10 7 1323.12 287.972 3 26 -10 8 293.514 170.142 3 26 -10 9 737.394 170.578 3 26 -11 -7 198.816 148.130 2 26 -11 -6 384.259 196.736 2 26 -11 -5 30.1171 202.527 2 26 -11 -4 227.878 241.383 2 26 -11 -3 1512.28 358.033 2 26 -11 -2 2389.38 448.615 2 26 -11 -1-62.7201 251.476 2 26 -11 0-60.7908 270.976 2 26 -11 1-158.928 191.200 3 26 -11 1 153.261 250.737 2 26 -11 2 2111.65 341.999 3 26 -11 2 2333.61 405.897 2 26 -11 3 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344.539 2 26 -14 1 1732.62 257.810 2 26 -14 2 2821.99 285.293 2 26 -15 -3 970.128 160.060 2 26 -15 -2 2150.17 229.007 2 26 -15 -1 2174.92 232.196 2 26 -15 0 620.825 133.144 2 27 0 -1 111.823 207.761 2 27 0 0 425.146 230.848 2 27 0 1-67.9813 220.622 2 27 0 2-66.2322 234.321 2 27 0 3-43.1499 292.568 2 27 0 4-224.035 297.375 2 27 0 5 256.245 299.158 2 27 0 5 157.307 225.819 3 27 0 6 21.7966 293.984 2 27 0 6 20.2645 229.934 3 27 0 7 17.0650 285.546 2 27 0 7-59.2378 218.723 3 27 0 8 101.646 206.732 3 27 0 9 343.126 237.130 3 27 0 10-1.79587 185.528 3 27 0 11-283.991 171.520 3 27 1 -4-1135.92 488.087 1 27 -1 -2 7131.08 584.000 2 27 -1 -1 128.162 225.191 2 27 1 -1-164.569 206.430 2 27 -1 0 2878.63 422.257 2 27 1 0 3131.41 440.376 2 27 1 1 1579.90 359.798 2 27 -1 1 1229.81 356.182 2 27 -1 2 7336.33 658.771 2 27 1 2 6429.76 621.296 2 27 -1 3 4484.35 556.844 2 27 1 3 5365.58 609.983 2 27 1 4 1312.38 383.108 2 27 -1 4 1503.02 378.924 2 27 1 5 4862.49 517.789 3 27 -1 5 5599.70 590.290 3 27 1 5 5082.51 624.196 2 27 -1 5 5699.26 639.563 2 27 1 6 30.8073 199.454 3 27 1 6 396.931 299.333 2 27 -1 6 189.685 261.883 3 27 -1 6-157.654 301.575 2 27 -1 7 5013.49 557.443 3 27 1 7 5187.95 513.990 3 27 1 7 4671.56 615.447 2 27 -1 7 5078.62 627.599 2 27 1 8 1354.31 295.943 3 27 -1 8 1094.15 317.985 3 27 -1 8 773.173 361.632 2 27 -1 9 2877.67 416.285 3 27 1 9 2914.42 370.373 3 27 -1 10 995.969 271.594 3 27 -1 11 3550.06 354.413 3 27 2 -4 7137.21 1165.64 1 27 -2 -3 245.471 160.933 2 27 2 -3-204.481 316.389 1 27 -2 -2 36077.2 1283.92 2 27 2 -2 36826.1 2445.76 1 27 -2 -1 418.456 217.591 2 27 2 -1 2031.80 629.169 1 27 -2 0 18990.6 979.833 2 27 2 0 18110.8 951.814 2 27 -2 1 726.120 271.230 2 27 2 1 419.362 237.802 2 27 2 2 39029.6 1446.91 2 27 -2 2 39115.1 1456.76 2 27 2 3 71.8904 246.430 2 27 -2 3 358.925 304.160 2 27 2 4 7851.02 725.758 2 27 -2 4 6713.94 682.613 2 27 -2 5 4354.66 534.205 3 27 -2 5 4427.08 582.595 2 27 2 5 3971.12 566.193 2 27 -2 6 9641.78 769.124 3 27 -2 6 9922.54 818.726 2 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1516.78 304.729 3 27 -3 11 8695.21 549.955 3 27 -3 12 467.284 149.236 3 27 4 -4 16109.1 1800.41 1 27 -4 -4 18033.3 925.767 2 27 4 -3-469.025 392.856 1 27 -4 -3 165.789 257.483 2 27 4 -2 16908.3 1806.65 1 27 -4 -2 18790.2 971.897 2 27 4 -1 2818.55 714.675 1 27 -4 -1 5611.93 561.473 2 27 4 0 36077.8 2600.71 1 27 -4 0 32892.0 1320.15 2 27 4 1 6253.89 1083.06 1 27 4 1 5457.50 563.432 2 27 -4 1 6140.82 608.789 2 27 -4 2 21932.6 1124.40 2 27 4 2 21088.6 1089.48 2 27 4 2 19990.9 1910.66 1 27 -4 3 387.708 313.428 2 27 4 3-734.282 480.242 1 27 4 3-178.119 291.597 2 27 -4 4 19042.7 1082.84 2 27 -4 5 2342.58 454.326 2 27 -4 5 2655.77 473.882 3 27 -4 6 37444.9 1502.69 2 27 -4 6 39079.5 1526.97 3 27 -4 7 1055.55 368.886 3 27 -4 7 1538.69 406.168 2 27 -4 8 14153.9 889.458 2 27 -4 8 16630.3 969.819 3 27 -4 9 182.318 254.168 3 27 -4 10 9438.82 643.627 3 27 -4 11 709.632 220.963 3 27 -4 12 4998.00 333.233 3 27 -5 -5 7128.24 587.881 2 27 -5 -4 3717.01 464.058 2 27 5 -3 13549.7 1694.80 1 27 -5 -3 12879.8 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27 -8 -5 972.765 279.642 2 27 -8 -4 1419.27 365.978 2 27 -8 -3 145.204 248.037 2 27 -8 -2 386.289 293.352 2 27 -8 -1 2726.29 455.298 2 27 -8 0 2296.67 443.980 2 27 -8 1 1833.30 435.821 2 27 -8 2 1350.30 383.412 2 27 -8 3 93.8250 263.717 2 27 -8 3 385.911 300.834 3 27 -8 4 913.985 324.643 2 27 -8 4 820.039 334.096 3 27 -8 5 1138.85 330.292 2 27 -8 5 911.926 337.452 3 27 -8 6 1253.57 324.150 2 27 -8 6 2280.51 426.473 3 27 -8 7 678.892 301.034 3 27 -8 7 1167.98 284.989 2 27 -8 8 372.495 248.033 3 27 -8 9 424.068 208.238 3 27 -8 10 1063.38 214.351 3 27 -9 -7 1205.97 240.330 2 27 -9 -6-130.731 213.595 2 27 -9 -5 6036.21 550.931 2 27 -9 -4 879.165 302.893 2 27 -9 -3 7221.54 650.593 2 27 -9 -2 534.602 323.590 2 27 -9 -1 7025.06 662.526 2 27 -9 0 2437.92 442.444 2 27 -9 1 6514.73 639.815 2 27 -9 2 703.068 332.372 2 27 -9 3 6295.69 628.814 3 27 -9 3 7681.60 690.574 2 27 -9 4 1047.79 343.412 2 27 -9 4 848.212 303.953 3 27 -9 5 6004.32 594.557 3 27 -9 5 6358.73 601.868 2 27 -9 6 163.620 239.881 3 27 -9 6 158.242 175.452 2 27 -9 7 2238.22 372.028 3 27 -9 8 320.484 215.852 3 27 -9 9 1242.91 231.156 3 27 -10 -7 270.693 169.658 2 27 -10 -6 5033.28 449.661 2 27 -10 -5 338.993 209.424 2 27 -10 -4 7265.24 612.825 2 27 -10 -3 187.051 276.015 2 27 -10 -2 8855.19 718.096 2 27 -10 -1-93.8318 266.492 2 27 -10 0 10295.4 774.056 2 27 -10 1 334.643 261.341 2 27 -10 1-22.9198 199.123 3 27 -10 2 7133.39 620.778 3 27 -10 2 8160.58 684.789 2 27 -10 3 131.189 263.291 2 27 -10 3-1.19201 221.672 3 27 -10 4 5490.57 543.146 3 27 -10 4 5099.91 532.927 2 27 -10 5-26.7038 184.290 2 27 -10 5 439.798 248.978 3 27 -10 6 5358.66 484.251 3 27 -10 7 113.072 176.631 3 27 -10 8 2399.99 292.390 3 27 -10 9-134.555 108.974 3 27 -11 -7 4571.76 349.390 2 27 -11 -6 417.245 192.339 2 27 -11 -5 6915.36 527.855 2 27 -11 -4 1377.50 314.957 2 27 -11 -3 7896.57 621.590 2 27 -11 -2 413.400 278.635 2 27 -11 -1 7703.96 653.039 2 27 -11 0 188.299 250.300 2 27 -11 1 5994.75 588.663 2 27 -11 1 6277.95 520.252 3 27 -11 2 106.078 244.795 2 27 -11 2 255.097 199.988 3 27 -11 3 9291.45 670.469 2 27 -11 3 8667.53 613.456 3 27 -11 4 744.562 250.483 2 27 -11 4 771.583 247.079 3 27 -11 5 5753.37 470.422 2 27 -11 5 5745.86 473.465 3 27 -11 6 430.156 178.505 3 27 -11 7 3632.25 319.008 3 27 -12 -6 2147.13 265.336 2 27 -12 -5 1262.95 248.849 2 27 -12 -4 8893.93 583.220 2 27 -12 -3 833.560 263.192 2 27 -12 -2 3969.89 465.083 2 27 -12 -1 2498.81 387.892 2 27 -12 0 7378.31 596.289 2 27 -12 1 1728.24 337.579 2 27 -12 2 3499.84 419.414 2 27 -12 3 556.849 234.290 2 27 -12 4 9410.28 573.997 2 27 -13 -6 123.528 98.5462 2 27 -13 -5 2152.03 257.202 2 27 -13 -4 553.836 197.080 2 27 -13 -3 757.752 233.261 2 27 -13 -2 585.001 224.638 2 27 -13 -1 2751.76 360.203 2 27 -13 0 3585.62 393.971 2 27 -13 1 2854.23 361.745 2 27 -13 2 610.156 210.054 2 27 -13 3 457.499 168.462 2 27 -14 -4 453.341 149.918 2 27 -14 -3 249.761 150.405 2 27 -14 -2 359.422 167.130 2 27 -14 -1 727.368 205.172 2 27 -14 0-110.897 153.900 2 27 -14 1 539.425 163.563 2 27 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325.168 159.345 2 28 -10 6 1249.17 258.270 3 28 -10 7 247.137 169.980 3 28 -10 8 168.757 135.979 3 28 -11 -7 70.2260 89.9581 2 28 -11 -6 154.233 151.275 2 28 -11 -5-114.481 192.050 2 28 -11 -4 117.802 206.342 2 28 -11 -3 346.718 242.889 2 28 -11 -2 171.240 243.244 2 28 -11 -1 975.836 333.203 2 28 -11 0 1265.44 255.147 3 28 -11 0 2097.55 390.279 2 28 -11 1 796.028 228.698 3 28 -11 1 1044.95 312.837 2 28 -11 2 434.721 216.432 3 28 -11 2 444.856 256.276 2 28 -11 3 43.6893 177.753 3 28 -11 3-151.040 202.789 2 28 -11 4 381.993 220.091 2 28 -11 4 553.199 221.404 3 28 -11 5 368.247 167.483 2 28 -11 5 100.270 159.652 3 28 -11 6 171.501 142.543 3 28 -11 7-148.725 124.183 3 28 -12 -6 305.542 133.770 2 28 -12 -5 969.726 206.812 2 28 -12 -4 518.218 211.329 2 28 -12 -3 822.018 257.707 2 28 -12 -2 318.897 242.654 2 28 -12 -1 653.081 270.013 2 28 -12 0 1082.99 295.149 2 28 -12 1 568.637 246.170 2 28 -12 2 38.7659 191.668 2 28 -12 3 724.852 218.584 2 28 -12 4 381.227 192.405 2 28 -13 -5 1287.67 198.095 2 28 -13 -4 120.390 140.429 2 28 -13 -3 1108.25 232.490 2 28 -13 -2 1777.70 282.562 2 28 -13 -1 2805.90 347.773 2 28 -13 0 653.897 225.330 2 28 -13 1 2955.57 341.527 2 28 -13 2 1891.44 273.103 2 28 -13 3 1612.85 226.912 2 28 -14 -3 381.867 132.232 2 28 -14 -2 4759.68 353.878 2 28 -14 -1 874.241 185.942 2 28 -14 0 2440.41 269.387 2 28 -14 1 751.614 164.075 2 29 0 -1-131.918 240.482 2 29 0 0-213.183 249.668 2 29 0 1-141.488 258.905 2 29 0 2 149.738 249.146 2 29 0 3-129.864 270.308 2 29 0 4-76.4287 307.194 2 29 0 5 78.2732 217.386 3 29 0 5 337.186 330.777 2 29 0 6 88.0913 229.918 3 29 0 6-3.12553 300.076 2 29 0 7 100.501 218.082 3 29 0 7-258.824 292.186 2 29 0 8 153.966 207.286 3 29 0 9-312.393 209.517 3 29 0 10-243.629 169.244 3 29 -1 -2 8457.27 662.592 2 29 -1 -1 6562.04 599.593 2 29 1 -1 5089.30 531.329 2 29 -1 0 307.780 262.143 2 29 1 0 354.888 216.953 2 29 1 1 7103.82 646.968 2 29 -1 1 7254.04 653.342 2 29 1 2 7704.56 693.637 2 29 -1 2 8304.10 716.284 2 29 1 3 1875.36 403.460 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607.114 3 29 -2 7 1450.56 349.297 3 29 -2 7 1003.92 355.442 2 29 -2 8 1063.62 328.967 2 29 -2 8 1314.74 336.238 3 29 -2 9 2704.53 388.348 3 29 -2 10 5121.79 438.211 3 29 -2 11 4104.17 334.816 3 29 -3 -3 14790.0 850.047 2 29 3 -2 17958.4 1848.35 1 29 -3 -2 18690.8 978.056 2 29 -3 -1 7448.06 639.811 2 29 -3 0 21438.0 1095.92 2 29 3 1 6888.47 632.440 2 29 -3 1 6090.12 622.374 2 29 3 2 23062.7 1142.83 2 29 -3 2 20583.2 1112.99 2 29 -3 3 13455.9 949.928 2 29 3 3 14547.0 951.702 2 29 3 4 1062.19 375.027 2 29 -3 4 1563.29 433.372 2 29 -3 5 11583.8 878.814 2 29 -3 5 12072.3 872.102 3 29 -3 6 16307.2 1023.60 2 29 -3 6 16009.8 961.062 3 29 -3 7 8958.88 763.765 2 29 -3 7 8183.90 700.580 3 29 -3 8 3575.33 483.063 2 29 -3 8 3903.39 501.518 3 29 -3 9 4007.47 455.675 3 29 -3 10 4138.89 405.888 3 29 -3 11 2506.65 278.403 3 29 -4 -4 11784.8 752.384 2 29 -4 -3 12545.8 799.978 2 29 4 -2 20884.3 2052.96 1 29 -4 -2 18166.5 981.373 2 29 4 -1 2548.28 713.370 1 29 -4 -1 5288.80 569.330 2 29 4 0 8344.90 1255.81 1 29 -4 0 7346.16 677.344 2 29 4 1 3119.22 454.971 2 29 -4 1 3244.57 474.853 2 29 4 2 22547.6 1135.08 2 29 -4 2 21695.2 1137.04 2 29 4 3 13960.3 921.842 2 29 -4 3 13096.4 911.388 2 29 -4 4 14058.1 956.665 2 29 -4 5 9886.27 800.690 3 29 -4 5 9068.85 782.808 2 29 -4 6 4756.11 578.247 3 29 -4 6 4509.29 587.798 2 29 -4 7 1171.18 347.790 3 29 -4 7 693.195 295.040 2 29 -4 8 3111.93 448.505 3 29 -4 8 2616.61 412.982 2 29 -4 9 3086.32 411.742 3 29 -4 10 4605.89 427.696 3 29 -4 11 2321.71 268.347 3 29 -5 -5 8784.93 629.292 2 29 -5 -4 7835.06 634.221 2 29 -5 -3 8273.64 670.397 2 29 -5 -2 4014.52 502.428 2 29 -5 -1 8702.94 719.396 2 29 -5 0 517.403 304.586 2 29 -5 1 9721.52 783.259 2 29 -5 2 5508.91 624.331 2 29 -5 3 7348.99 705.658 2 29 -5 4 9884.97 809.839 2 29 -5 4 9883.75 837.041 3 29 -5 5 7325.87 724.961 3 29 -5 5 7456.43 717.609 2 29 -5 6 5155.67 595.902 3 29 -5 6 4065.16 543.173 2 29 -5 7 7292.10 677.361 3 29 -5 7 5042.53 559.736 2 29 -5 8 3752.67 495.314 3 29 -5 8 3671.66 447.652 2 29 -5 9 4273.46 460.998 3 29 -5 10 4320.93 406.349 3 29 -5 11 1551.40 219.241 3 29 -6 -5 1788.10 338.019 2 29 -6 -4 2946.55 432.364 2 29 -6 -3 1546.68 374.616 2 29 -6 -2 1667.45 404.891 2 29 -6 -1-87.4916 275.299 2 29 -6 0 2396.73 431.772 2 29 -6 1 666.294 342.663 2 29 -6 2 1707.62 419.288 2 29 -6 3 1169.64 381.543 2 29 -6 4 2359.26 470.340 3 29 -6 4 2850.45 484.416 2 29 -6 5 1228.94 367.360 3 29 -6 5 1214.61 372.348 2 29 -6 6 1348.77 398.823 3 29 -6 6 800.619 342.636 2 29 -6 7 3204.26 485.463 3 29 -6 7 2756.20 400.589 2 29 -6 8 2176.75 347.797 2 29 -6 8 2565.64 421.125 3 29 -6 9 336.057 224.451 3 29 -6 10 196.598 151.704 3 29 -7 -6 1908.80 319.303 2 29 -7 -5 1422.23 289.463 2 29 -7 -4 324.926 243.748 2 29 -7 -3 3033.94 445.527 2 29 -7 -2 239.397 286.495 2 29 -7 -1 1853.42 406.323 2 29 -7 0 1294.05 384.573 2 29 -7 1 980.206 367.289 2 29 -7 2 39.8897 298.102 2 29 -7 3 2477.86 457.710 2 29 -7 4 365.495 322.400 3 29 -7 4 58.9746 253.955 2 29 -7 5 1509.78 395.451 3 29 -7 5 1508.94 390.377 2 29 -7 6 1948.92 404.719 3 29 -7 6 1514.82 348.221 2 29 -7 7 359.154 219.588 2 29 -7 7 378.356 262.150 3 29 -7 8-158.790 140.458 2 29 -7 8 580.287 270.958 3 29 -7 9 1115.08 248.817 3 29 -7 10-10.9092 144.384 3 29 -8 -6 344.083 212.926 2 29 -8 -5 379.982 223.989 2 29 -8 -4-72.7047 224.471 2 29 -8 -3 4166.22 507.328 2 29 -8 -2 587.759 294.172 2 29 -8 -1 5244.78 579.509 2 29 -8 0 2868.53 477.429 2 29 -8 1 4216.52 544.527 2 29 -8 2 593.885 301.122 2 29 -8 3 3351.32 489.452 3 29 -8 3 4178.51 549.612 2 29 -8 4 102.341 255.319 3 29 -8 4 116.835 263.250 2 29 -8 5 1079.10 343.819 3 29 -8 5 666.198 284.122 2 29 -8 6 152.793 269.182 3 29 -8 6 168.675 226.275 2 29 -8 7 162.656 166.524 2 29 -8 7 1.07173 235.613 3 29 -8 8 142.188 210.643 3 29 -8 9 432.801 191.832 3 29 -9 -7 767.277 169.721 2 29 -9 -6 3099.48 357.453 2 29 -9 -5 487.556 227.282 2 29 -9 -4 1973.10 363.104 2 29 -9 -3 1841.24 369.000 2 29 -9 -2 3567.72 491.210 2 29 -9 -1 1600.72 405.044 2 29 -9 0 3097.85 483.683 2 29 -9 1 1620.95 401.199 2 29 -9 2 2403.97 437.282 3 29 -9 2 3423.54 494.755 2 29 -9 3 959.672 313.185 3 29 -9 3 2130.87 412.858 2 29 -9 4 1191.04 341.774 3 29 -9 4 733.225 295.834 2 29 -9 5 183.634 230.306 3 29 -9 5 270.535 238.222 2 29 -9 6 1918.25 320.432 2 29 -9 6 2527.51 377.532 3 29 -9 7 96.6979 187.539 3 29 -9 8 1527.03 256.351 3 29 -9 9 277.448 125.130 3 29 -10 -7 1133.07 176.854 2 29 -10 -6 3824.79 357.932 2 29 -10 -5 3789.44 408.227 2 29 -10 -4 7472.15 574.443 2 29 -10 -3 5482.36 527.413 2 29 -10 -2 2391.34 409.382 2 29 -10 -1 1351.09 353.687 2 29 -10 0 1444.89 364.749 2 29 -10 1 718.778 271.520 3 29 -10 1 1267.34 345.989 2 29 -10 2 1912.30 353.283 3 29 -10 2 2096.38 403.189 2 29 -10 3 6158.12 573.409 2 29 -10 3 5326.47 513.186 3 29 -10 4 5039.58 500.875 2 29 -10 4 4531.27 467.062 3 29 -10 5 3896.98 411.941 2 29 -10 5 3745.72 407.715 3 29 -10 6 98.7936 107.124 2 29 -10 6 3904.70 391.162 3 29 -10 7 1799.94 265.191 3 29 -10 8 1331.91 197.063 3 29 -11 -6 1441.17 231.035 2 29 -11 -5 2190.67 304.127 2 29 -11 -4 6450.75 505.406 2 29 -11 -3 4036.81 441.807 2 29 -11 -2 2979.83 417.027 2 29 -11 -1 5609.51 545.302 2 29 -11 0 4347.41 490.100 2 29 -11 0 3539.20 373.108 3 29 -11 1 4885.79 503.400 2 29 -11 1 4638.67 426.668 3 29 -11 2 1498.96 277.472 3 29 -11 2 2733.47 400.396 2 29 -11 3 4799.38 471.577 2 29 -11 3 4203.15 395.278 3 29 -11 4 5980.28 492.757 2 29 -11 4 5183.09 423.245 3 29 -11 5 2275.94 288.518 2 29 -11 5 1876.23 264.367 3 29 -11 6 1015.59 193.269 3 29 -12 -6 1149.38 166.861 2 29 -12 -5 1518.44 234.108 2 29 -12 -4 989.292 217.963 2 29 -12 -3 322.515 202.976 2 29 -12 -2 2545.42 348.370 2 29 -12 -1 1847.97 322.572 2 29 -12 0 8117.25 585.283 2 29 -12 1 1722.90 293.309 2 29 -12 2 2428.95 330.528 2 29 -12 3 236.744 179.683 2 29 -12 4 1126.82 204.393 2 29 -13 -4 1136.63 197.826 2 29 -13 -3 2123.29 274.009 2 29 -13 -2 251.188 169.061 2 29 -13 -1 2117.32 291.564 2 29 -13 0 320.271 178.245 2 29 -13 1 1473.40 246.793 2 29 -13 2 7.94040 138.317 2 29 -13 3 1747.39 219.228 2 29 -14 -2 333.707 135.437 2 29 -14 -1 79.9747 106.091 2 29 -14 0 273.399 132.074 2 30 0 -1 6662.02 610.513 2 30 0 0 76.2888 245.028 2 30 0 1 8644.92 723.486 2 30 0 2 10487.0 810.586 2 30 0 3 27165.9 1303.79 2 30 0 4 1510.40 348.492 3 30 0 4 1641.59 422.496 2 30 0 5 17677.2 954.964 3 30 0 5 17162.9 1067.38 2 30 0 6 1401.05 322.392 3 30 0 6 1349.24 411.499 2 30 0 7 10369.9 696.641 3 30 0 7 12219.8 890.886 2 30 0 8 916.922 246.290 3 30 0 9 7637.51 535.654 3 30 0 10 3504.55 309.035 3 30 -1 -2 5622.98 559.664 2 30 -1 -1 3480.77 451.971 2 30 1 -1 3044.43 416.061 2 30 1 0 15379.1 912.841 2 30 -1 0 15658.7 936.083 2 30 1 1 3182.97 460.490 2 30 -1 1 2967.32 474.963 2 30 1 2 4526.90 567.219 2 30 -1 2 5201.12 611.198 2 30 1 3 841.532 341.906 2 30 -1 3 980.453 385.471 2 30 1 4 16096.7 1030.32 2 30 -1 4 15612.7 1009.53 2 30 -1 4 15646.2 955.551 3 30 1 4 15795.5 892.903 3 30 1 5 1862.47 347.336 3 30 -1 5 2037.08 406.795 3 30 1 5 1597.12 412.497 2 30 -1 5 1530.84 439.083 2 30 1 6 8274.78 629.768 3 30 -1 6 8148.58 676.732 3 30 -1 6 10231.9 834.375 2 30 1 6 9805.23 843.877 2 30 1 7 3289.60 399.708 3 30 -1 7 3173.54 505.299 2 30 -1 7 3390.75 440.524 3 30 1 8 13219.0 706.493 3 30 -1 8 14289.7 807.668 3 30 -1 9 1399.49 289.847 3 30 -1 10 3101.19 329.679 3 30 -2 -3 8572.93 651.081 2 30 -2 -2 78.8384 212.560 2 30 -2 -1 10708.2 763.215 2 30 2 0 2446.77 399.521 2 30 -2 0 1906.94 394.651 2 30 2 1 10149.6 775.901 2 30 -2 1 10548.2 800.651 2 30 2 2 671.545 306.814 2 30 -2 2 1395.26 378.267 2 30 2 3 7952.88 723.326 2 30 -2 3 7318.52 718.523 2 30 2 4 631.592 298.664 2 30 -2 4 1167.22 396.877 2 30 -2 5 10881.1 810.732 3 30 -2 5 11037.4 868.185 2 30 2 5 10999.4 867.046 2 30 -2 6 2109.19 402.051 3 30 -2 6 2300.08 482.002 2 30 -2 7 4323.46 510.895 3 30 -2 7 4085.69 547.163 2 30 -2 8 453.995 247.418 3 30 -2 9 3784.65 431.693 3 30 -2 10 658.657 200.074 3 30 -2 11 2271.07 234.314 3 30 -3 -3 1672.98 356.010 2 30 -3 -2 701.606 284.548 2 30 -3 -1 3457.28 478.730 2 30 -3 0 793.971 319.956 2 30 -3 1 4151.81 547.279 2 30 3 1 3615.78 487.993 2 30 3 2 1095.84 344.322 2 30 -3 2 701.556 304.374 2 30 3 3 1622.22 404.882 2 30 -3 3 929.229 387.261 2 30 3 4 2237.36 459.489 2 30 -3 4 1681.66 412.978 2 30 -3 5 707.752 349.281 3 30 -3 5 411.356 353.213 2 30 -3 6 2080.89 446.302 3 30 -3 6 1599.99 419.648 2 30 -3 7 200.999 265.402 3 30 -3 7 305.717 300.644 2 30 -3 8 678.961 295.966 2 30 -3 8 585.234 280.661 3 30 -3 9 1675.05 318.122 3 30 -3 10 913.591 227.616 3 30 -3 11 525.451 142.157 3 30 -4 -4 629.954 255.034 2 30 -4 -3 320.065 248.810 2 30 -4 -2 178.204 261.816 2 30 -4 -1 722.905 316.974 2 30 -4 0 440.422 273.608 2 30 4 1 281.912 221.042 2 30 -4 1 347.228 279.735 2 30 4 2 356.048 269.359 2 30 -4 2 1153.11 396.948 2 30 -4 3 628.930 355.108 2 30 -4 4 527.021 281.730 3 30 -4 4 584.825 333.818 2 30 -4 5 94.1394 305.531 3 30 -4 5 402.699 287.083 2 30 -4 6 354.090 310.396 3 30 -4 6 55.8883 280.055 2 30 -4 7 855.370 315.177 3 30 -4 7 486.377 298.546 2 30 -4 8 1272.47 312.418 2 30 -4 8 1279.16 310.612 3 30 -4 9 499.380 241.640 3 30 -4 10 609.182 206.591 3 30 -4 11 228.299 110.927 3 30 -5 -5 445.805 216.365 2 30 -5 -4 2752.20 400.078 2 30 -5 -3-22.4433 227.842 2 30 -5 -2 2004.84 379.072 2 30 -5 -1 1215.17 340.875 2 30 -5 0 7432.87 680.538 2 30 -5 1 1123.19 339.574 2 30 -5 2 2210.34 461.620 2 30 -5 3 554.701 348.568 2 30 -5 4 3644.58 546.352 3 30 -5 4 3526.57 538.009 2 30 -5 5 216.851 298.958 3 30 -5 5 717.608 329.609 2 30 -5 6 792.759 342.391 3 30 -5 6 102.896 250.861 2 30 -5 7 537.143 284.129 3 30 -5 7 816.881 294.057 2 30 -5 8 4022.91 455.684 2 30 -5 8 4144.44 477.959 3 30 -5 9-2.79019 196.538 3 30 -5 10 578.736 189.587 3 30 -6 -5 6171.58 536.168 2 30 -6 -4 2383.61 391.937 2 30 -6 -3 10078.6 744.302 2 30 -6 -2 2759.54 438.111 2 30 -6 -1 17252.6 989.978 2 30 -6 0 347.614 308.396 2 30 -6 1 13514.5 921.800 2 30 -6 2 3932.13 551.467 2 30 -6 3 9369.65 781.124 2 30 -6 4 2381.77 471.725 3 30 -6 4 2557.69 471.096 2 30 -6 5 4500.24 560.375 2 30 -6 5 5807.79 635.692 3 30 -6 6 712.163 325.395 3 30 -6 6 922.275 332.962 2 30 -6 7 8609.64 654.373 2 30 -6 7 8237.06 665.577 3 30 -6 8-33.2274 178.664 2 30 -6 8 379.847 246.683 3 30 -6 9 5352.07 459.140 3 30 -6 10 148.863 136.584 3 30 -7 -6 7670.89 526.985 2 30 -7 -5 994.883 274.189 2 30 -7 -4 2693.61 397.466 2 30 -7 -3 1008.68 305.392 2 30 -7 -2 9524.10 738.527 2 30 -7 -1 4141.91 527.921 2 30 -7 0 26671.1 1240.98 2 30 -7 1 4793.21 574.757 2 30 -7 2 11498.4 849.452 2 30 -7 3 835.384 351.609 3 30 -7 3 597.402 307.279 2 30 -7 4 3389.31 507.106 3 30 -7 4 2929.49 476.106 2 30 -7 5 540.792 317.483 3 30 -7 5 1184.12 342.830 2 30 -7 6 9080.43 715.977 3 30 -7 6 8034.79 649.315 2 30 -7 7 938.344 300.974 3 30 -7 7 919.717 269.544 2 30 -7 8 5601.67 496.845 3 30 -7 9 949.657 230.052 3 30 -7 10 2587.89 258.657 3 30 -8 -6 1904.59 287.694 2 30 -8 -5 5756.94 498.820 2 30 -8 -4 1564.34 338.742 2 30 -8 -3 6087.10 576.109 2 30 -8 -2 698.018 300.185 2 30 -8 -1 9057.26 724.866 2 30 -8 0 500.429 304.377 2 30 -8 1 11876.8 839.605 2 30 -8 2 848.043 329.544 2 30 -8 3 6610.07 633.874 2 30 -8 3 5825.81 601.259 3 30 -8 4 924.298 327.744 3 30 -8 4 239.526 267.513 2 30 -8 5 5602.81 562.169 2 30 -8 5 6200.70 602.688 3 30 -8 6 1311.65 325.233 3 30 -8 6 1692.83 325.199 2 30 -8 7 5121.80 490.592 3 30 -8 7 5719.07 463.060 2 30 -8 8 1147.08 256.203 3 30 -8 9 2551.91 275.813 3 30 -9 -6 3215.91 329.141 2 30 -9 -5 1334.78 275.255 2 30 -9 -4 1114.38 290.913 2 30 -9 -3 4192.73 477.516 2 30 -9 -2 6596.09 614.805 2 30 -9 -1 2230.93 402.317 2 30 -9 0 2970.88 471.391 2 30 -9 1 1294.17 376.064 2 30 -9 2 4012.36 521.813 2 30 -9 2 4329.77 515.932 3 30 -9 3 4490.35 517.023 2 30 -9 3 4970.17 533.674 3 30 -9 4 1640.87 352.292 3 30 -9 4 1061.92 306.116 2 30 -9 5 1508.53 329.750 3 30 -9 5 1817.66 337.543 2 30 -9 6 3011.02 367.897 2 30 -9 6 3358.58 393.725 3 30 -9 7 962.553 234.134 3 30 -9 8 1052.38 204.874 3 30 -10 -6 1598.09 239.755 2 30 -10 -5 1469.50 263.075 2 30 -10 -4-111.515 205.381 2 30 -10 -3 635.253 255.866 2 30 -10 -2 172.366 244.046 2 30 -10 -1 1407.87 353.845 2 30 -10 0 4370.55 529.701 2 30 -10 1 1232.73 284.424 3 30 -10 1 1323.37 347.614 2 30 -10 2 883.222 268.329 3 30 -10 2 1308.25 338.402 2 30 -10 3 722.255 254.301 3 30 -10 3 985.859 295.101 2 30 -10 4 202.927 198.126 3 30 -10 4 506.406 239.655 2 30 -10 5 1341.93 270.297 2 30 -10 5 1192.31 260.148 3 30 -10 6 712.438 207.466 3 30 -10 7 829.892 198.137 3 30 -11 -6-30.3979 100.092 2 30 -11 -5 585.501 175.438 2 30 -11 -4 275.940 188.430 2 30 -11 -3 220.603 209.852 2 30 -11 -2 458.804 247.844 2 30 -11 -1 609.808 267.310 2 30 -11 0 199.028 139.661 3 30 -11 0 880.185 300.809 2 30 -11 1-315.634 220.020 3 30 -11 1 195.905 235.811 2 30 -11 2-212.844 152.717 3 30 -11 2 306.260 206.290 2 30 -11 3 232.461 163.602 3 30 -11 3 366.737 214.105 2 30 -11 4 195.901 193.800 2 30 -11 4 336.293 152.383 3 30 -11 5 146.826 111.443 2 30 -11 5 461.365 152.996 3 30 -11 6-60.5300 94.8802 3 30 -12 -5 549.204 150.481 2 30 -12 -4 343.455 152.570 2 30 -12 -3 298.369 179.656 2 30 -12 -2-172.420 201.621 2 30 -12 -1 1161.72 263.310 2 30 -12 0 28.5664 201.065 2 30 -12 1 1183.54 261.354 2 30 -12 2-17.7457 182.627 2 30 -12 3 334.255 172.370 2 30 -12 4 471.797 135.546 2 30 -13 -4 269.133 116.917 2 30 -13 -3 207.907 134.653 2 30 -13 -2 3269.21 320.266 2 30 -13 -1 209.887 162.235 2 30 -13 0 1735.66 261.457 2 30 -13 1-49.1925 129.565 2 30 -13 2 2182.84 249.499 2 31 0 -1 191.720 222.637 2 31 0 0 13.3504 237.983 2 31 0 1-25.2422 273.429 2 31 0 2-102.378 296.035 2 31 0 3-57.4191 285.808 2 31 0 4 6.43648 241.122 3 31 0 4-50.8659 311.773 2 31 0 5-68.0530 228.730 3 31 0 5 49.3417 313.954 2 31 0 6 286.054 223.731 3 31 0 6 60.3756 343.566 2 31 0 7-32.7870 205.717 3 31 0 8 156.457 199.842 3 31 0 9 150.356 162.989 3 31 -1 -2 990.968 272.301 2 31 1 -1 6857.44 602.791 2 31 -1 -1 5206.02 566.668 2 31 1 0 6657.53 620.961 2 31 -1 0 6012.17 608.213 2 31 1 1 5979.20 614.892 2 31 -1 1 5814.93 626.241 2 31 1 2 778.171 307.058 2 31 -1 2 1163.26 374.148 2 31 1 3 675.026 343.943 2 31 -1 3 334.198 316.243 2 31 1 4 1052.27 386.755 2 31 1 4 1652.56 335.986 3 31 -1 4 1873.02 396.710 3 31 -1 4 1349.19 388.703 2 31 -1 5 1312.60 424.896 2 31 1 5 898.024 272.742 3 31 1 5 917.667 371.155 2 31 -1 5 854.060 278.510 3 31 1 6 2566.50 370.966 3 31 -1 6 2338.67 398.039 3 31 1 6 2326.44 478.627 2 31 -1 6 2331.05 490.808 2 31 -1 7-150.350 327.882 2 31 -1 7 262.989 242.433 3 31 1 7 568.024 231.748 3 31 -1 8 2600.77 351.625 3 31 -1 9-126.570 162.172 3 31 -1 10 905.609 185.115 3 31 -2 -2 530.555 261.624 2 31 -2 -1 11597.8 808.733 2 31 2 0 119.614 226.797 2 31 -2 0 162.485 233.969 2 31 2 1 11503.5 825.585 2 31 -2 1 11288.5 839.997 2 31 2 2 449.569 271.267 2 31 -2 2 1252.75 364.762 2 31 2 3 9473.41 793.483 2 31 -2 3 9249.88 801.881 2 31 2 4 921.588 369.286 2 31 -2 4 871.447 339.195 3 31 -2 4 907.533 378.134 2 31 -2 5 13540.0 969.801 2 31 2 5 15839.1 1027.90 2 31 -2 5 13941.5 899.366 3 31 -2 6 3364.93 457.489 3 31 -2 6 2975.37 520.534 2 31 -2 7 6526.85 667.913 2 31 -2 7 6847.86 607.431 3 31 -2 8 746.554 267.200 3 31 -2 9 4102.40 407.382 3 31 -2 10 1181.37 227.098 3 31 -3 -3 3188.50 437.082 2 31 -3 -2 17948.3 964.049 2 31 -3 -1 1382.19 363.957 2 31 -3 0 8831.25 730.433 2 31 3 1 1017.66 331.164 2 31 -3 1 765.832 326.273 2 31 -3 2 16723.6 1021.92 2 31 3 2 18076.3 1028.83 2 31 3 3 3117.93 501.592 2 31 -3 3 2700.66 493.669 2 31 -3 4 19218.2 1132.84 2 31 -3 4 16717.2 1004.98 3 31 3 4 17021.5 1037.39 2 31 -3 5 4186.54 577.146 2 31 -3 5 3944.29 539.376 3 31 -3 6 10941.7 786.383 3 31 -3 6 10824.1 838.908 2 31 -3 7 285.293 272.515 2 31 -3 7 597.223 273.383 3 31 -3 8 6355.99 549.641 3 31 -3 9 481.080 208.054 3 31 -3 10 5723.92 407.450 3 31 -4 -4 279.045 224.763 2 31 -4 -3 17191.5 935.437 2 31 -4 -2 433.258 237.458 2 31 -4 -1 9166.41 742.026 2 31 -4 0 154.311 266.257 2 31 4 1 7754.09 663.091 2 31 -4 1 7199.00 687.959 2 31 -4 2 1075.01 387.141 2 31 -4 3 14545.4 966.262 2 31 -4 4 19.0338 305.814 3 31 -4 4 242.174 314.170 2 31 -4 5 11906.7 877.590 2 31 -4 5 10893.0 821.497 3 31 -4 6 308.906 273.263 3 31 -4 6-83.4261 277.414 2 31 -4 7 11717.3 801.922 2 31 -4 7 12637.2 812.878 3 31 -4 8 764.802 288.422 2 31 -4 8 278.606 240.393 3 31 -4 9 5393.06 460.129 3 31 -4 10 694.117 195.327 3 31 -5 -4 4829.69 501.374 2 31 -5 -3 484.775 276.598 2 31 -5 -2 9731.10 748.169 2 31 -5 -1 362.083 301.804 2 31 -5 0 11129.6 824.249 2 31 -5 1-111.998 330.601 2 31 -5 2 12263.4 882.871 2 31 -5 3-14.6871 283.681 2 31 -5 4 4283.07 568.705 3 31 -5 4 4441.24 566.230 2 31 -5 5 1291.46 369.720 3 31 -5 5 997.016 390.223 2 31 -5 6 7930.40 678.311 3 31 -5 6 6081.95 613.822 2 31 -5 7 299.691 289.741 3 31 -5 7 513.319 280.310 2 31 -5 8 4687.98 471.458 3 31 -5 8 4065.66 429.436 2 31 -5 9 749.993 227.955 3 31 -5 10 2295.69 263.823 3 31 -6 -5 2775.08 368.086 2 31 -6 -4 270.669 222.364 2 31 -6 -3 5135.73 534.765 2 31 -6 -2-207.721 249.949 2 31 -6 -1 6792.52 656.253 2 31 -6 0 178.084 295.641 2 31 -6 1 7050.75 681.560 2 31 -6 2 305.533 333.954 2 31 -6 3 6458.18 668.012 2 31 -6 4 403.248 318.158 3 31 -6 4 854.509 332.851 2 31 -6 5 2302.51 442.462 3 31 -6 5 2270.79 425.911 2 31 -6 6 1684.41 395.324 3 31 -6 6 1196.32 316.244 2 31 -6 7 2402.72 381.184 2 31 -6 7 1970.32 367.302 3 31 -6 8 100.152 180.905 2 31 -6 8 123.199 196.620 3 31 -6 9 2013.11 288.130 3 31 -6 10-152.514 127.901 3 31 -7 -5 251.406 177.776 2 31 -7 -4 377.271 246.905 2 31 -7 -3 2261.95 384.162 2 31 -7 -2 382.884 266.892 2 31 -7 -1 553.906 317.415 2 31 -7 0 3727.14 525.992 2 31 -7 1 650.260 330.291 2 31 -7 2 110.959 286.391 2 31 -7 3 1601.63 386.298 3 31 -7 3 1353.67 394.025 2 31 -7 4 183.671 264.668 3 31 -7 4 152.494 277.996 2 31 -7 5 120.607 262.178 3 31 -7 5 491.753 295.194 2 31 -7 6 259.865 235.721 3 31 -7 6 313.091 240.481 2 31 -7 7 800.569 242.115 2 31 -7 7 849.460 285.292 3 31 -7 8 276.153 184.353 3 31 -7 9 223.516 142.961 3 31 -8 -6 1511.36 241.388 2 31 -8 -5 610.662 209.641 2 31 -8 -4 320.185 231.663 2 31 -8 -3 351.707 259.922 2 31 -8 -2 358.807 280.389 2 31 -8 -1 845.378 306.793 2 31 -8 0 181.548 280.342 2 31 -8 1 221.642 307.082 2 31 -8 2 1072.85 338.602 3 31 -8 2 537.460 312.947 2 31 -8 3 71.6962 243.232 3 31 -8 3 943.621 357.361 2 31 -8 4 94.1297 247.895 3 31 -8 4-245.009 265.288 2 31 -8 5 886.251 296.996 3 31 -8 5 356.602 252.497 2 31 -8 6 1930.96 328.391 2 31 -8 6 2142.68 363.042 3 31 -8 7 29.1710 147.403 2 31 -8 7 717.638 229.438 3 31 -8 8 630.077 199.010 3 31 -8 9 224.278 135.403 3 31 -9 -6 2220.83 271.465 2 31 -9 -5 1483.05 269.077 2 31 -9 -4 4194.00 434.152 2 31 -9 -3 1520.41 326.092 2 31 -9 -2 1508.18 323.288 2 31 -9 -1 143.904 251.761 2 31 -9 0 3320.62 481.757 2 31 -9 1-123.364 277.719 2 31 -9 2 1517.45 345.092 3 31 -9 2 1793.66 391.579 2 31 -9 3 843.839 286.198 3 31 -9 3 962.024 319.270 2 31 -9 4 2998.58 398.787 3 31 -9 4 3224.60 433.208 2 31 -9 5 1355.27 301.446 3 31 -9 5 1400.82 297.786 2 31 -9 6 2564.40 319.905 2 31 -9 6 2620.37 351.454 3 31 -9 7 127.770 153.257 3 31 -9 8 918.262 179.040 3 31 -10 -6 339.051 144.878 2 31 -10 -5 2727.82 313.246 2 31 -10 -4 547.548 211.192 2 31 -10 -3 4889.85 471.124 2 31 -10 -2 311.244 231.367 2 31 -10 -1 4425.98 487.185 2 31 -10 0 177.610 187.541 3 31 -10 0 152.146 251.595 2 31 -10 1 4908.84 513.705 2 31 -10 1 4961.06 475.577 3 31 -10 2 101.471 188.142 3 31 -10 2 607.697 267.485 2 31 -10 3 5488.36 514.908 2 31 -10 3 5357.58 474.996 3 31 -10 4 941.034 239.226 3 31 -10 4 744.253 247.337 2 31 -10 5 3271.32 348.734 2 31 -10 5 3396.66 354.671 3 31 -10 6 204.056 142.421 3 31 -10 7 1004.05 169.258 3 31 -11 -5-1.19448 129.227 2 31 -11 -4 3911.01 364.639 2 31 -11 -3 1106.98 240.177 2 31 -11 -2 5443.80 475.778 2 31 -11 -1 110.603 213.064 2 31 -11 0 2056.36 270.706 3 31 -11 0 8349.15 596.356 2 31 -11 1 173.675 146.154 3 31 -11 1 208.806 219.058 2 31 -11 2 5212.72 475.131 2 31 -11 2 4253.23 373.674 3 31 -11 3 1004.86 209.073 3 31 -11 3 1234.86 262.935 2 31 -11 4 2765.17 314.558 2 31 -11 4 2715.70 282.596 3 31 -11 5 226.976 110.134 3 31 -12 -4 692.905 173.854 2 31 -12 -3 4141.82 360.674 2 31 -12 -2 483.850 190.389 2 31 -12 -1 3073.65 342.519 2 31 -12 0 87.4873 179.304 2 31 -12 1 2669.04 332.482 2 31 -12 2 437.314 184.327 2 31 -12 3 3547.19 323.086 2 31 -13 -3 165.028 113.817 2 31 -13 -2 755.508 159.490 2 31 -13 -1-55.3731 133.103 2 31 -13 0 2538.51 270.596 2 31 -13 1 6.76013 119.334 2 32 0 -1 12114.7 802.854 2 32 0 0 6114.87 609.347 2 32 0 1 13871.4 909.184 2 32 0 2 1646.34 388.323 2 32 0 3 3445.38 524.722 2 32 0 4 3980.76 488.647 3 32 0 4 3903.61 549.012 2 32 0 5 15675.0 881.864 3 32 0 5 16724.7 1048.53 2 32 0 6 2957.38 515.441 2 32 0 6 2343.36 365.289 3 32 0 7 9421.86 624.304 3 32 0 8 4492.15 415.521 3 32 0 9 4375.64 360.117 3 32 -1 -2 14016.7 846.346 2 32 -1 -1 3722.04 471.999 2 32 1 0 6515.60 617.793 2 32 -1 0 7767.30 694.540 2 32 -1 1 4335.55 549.770 2 32 1 1 3071.77 460.882 2 32 1 2 14032.8 940.512 2 32 -1 2 14314.6 968.459 2 32 1 3 3072.32 505.710 2 32 -1 3 2977.85 493.814 2 32 1 4 9249.51 795.991 2 32 -1 4 9316.53 798.043 2 32 -1 4 8442.54 701.990 3 32 1 4 7859.38 629.048 3 32 1 5 2583.00 497.693 2 32 -1 5 2541.93 494.621 2 32 1 5 2094.72 345.536 3 32 -1 5 2665.60 426.851 3 32 1 6 4705.32 606.240 2 32 -1 6 5180.22 631.846 2 32 1 6 5438.50 488.978 3 32 -1 6 5743.53 558.832 3 32 -1 7 3241.05 498.734 2 32 -1 7 2588.55 388.453 3 32 -1 8 2892.03 364.783 3 32 -1 9 2192.45 276.885 3 32 -2 -2 22.2915 197.161 2 32 -2 -1 5207.12 565.738 2 32 2 0-26.8111 213.988 2 32 -2 0-301.875 262.171 2 32 2 1 3690.92 485.921 2 32 -2 1 3006.55 471.114 2 32 2 2-175.207 281.026 2 32 -2 2-152.454 293.989 2 32 -2 3 7379.71 722.733 2 32 2 3 8874.85 763.053 2 32 2 4 3708.29 556.427 2 32 -2 4 3436.01 487.737 3 32 -2 4 3570.28 541.619 2 32 -2 5 2871.10 446.099 3 32 2 5 3286.10 524.877 2 32 -2 5 3888.29 574.088 2 32 -2 6 883.580 396.842 2 32 -2 6 1376.90 339.339 3 32 -2 7 2810.91 461.948 2 32 -2 7 3296.81 434.554 3 32 -2 8 910.013 262.429 3 32 -2 9 2230.40 303.434 3 32 -2 10 55.4414 111.053 3 32 -3 -3 1297.12 299.155 2 32 -3 -2 1182.49 334.024 2 32 -3 -1-185.908 236.310 2 32 -3 0 284.146 259.321 2 32 3 1 208.787 275.551 2 32 -3 1 646.426 331.192 2 32 3 2 1961.80 411.129 2 32 -3 2 2175.69 433.976 2 32 3 3 1539.88 378.219 2 32 -3 3 1368.67 408.367 2 32 -3 4 1544.60 392.702 3 32 -3 4 1752.12 424.736 2 32 -3 5 368.463 290.559 3 32 -3 5 623.241 348.856 2 32 -3 6 3255.57 523.985 2 32 -3 6 3702.78 489.586 3 32 -3 7 1395.97 370.350 2 32 -3 7 1680.03 353.929 3 32 -3 8 1623.31 309.968 3 32 -3 9 323.166 189.286 3 32 -3 10 21.1874 114.816 3 32 -4 -4 1580.46 330.641 2 32 -4 -3 350.686 250.662 2 32 -4 -2 1982.44 364.317 2 32 -4 -1-125.194 269.590 2 32 -4 0 380.866 246.566 2 32 -4 1-372.414 312.338 2 32 -4 2 1069.53 364.901 2 32 -4 3 546.724 338.331 2 32 -4 4 1128.35 355.811 3 32 -4 4 1382.16 418.783 2 32 -4 5 793.049 345.351 3 32 -4 5 704.558 346.133 2 32 -4 6-74.7036 262.623 3 32 -4 6-345.786 295.529 2 32 -4 7 1085.70 305.316 2 32 -4 7 424.455 268.635 3 32 -4 8 740.530 267.504 3 32 -4 9 662.763 194.929 3 32 -4 10 207.886 127.404 3 32 -5 -4 1461.22 304.082 2 32 -5 -3 609.445 284.664 2 32 -5 -2 3433.55 471.674 2 32 -5 -1 4952.50 565.089 2 32 -5 0-164.325 299.139 2 32 -5 1 5379.83 609.711 2 32 -5 2 3904.85 550.513 2 32 -5 3 420.262 307.101 2 32 -5 4 1851.67 436.515 3 32 -5 4 2224.49 435.446 2 32 -5 5 1539.13 389.453 3 32 -5 5 852.465 328.341 2 32 -5 6 1881.81 376.004 3 32 -5 6 1267.27 354.089 2 32 -5 7 1655.71 338.735 2 32 -5 7 1594.21 339.087 3 32 -5 8-142.390 210.363 3 32 -5 9 691.916 197.271 3 32 -5 10 607.297 152.822 3 32 -6 -5 2451.34 338.860 2 32 -6 -4 1995.21 344.983 2 32 -6 -3 3643.33 456.574 2 32 -6 -2 834.308 305.696 2 32 -6 -1 8637.95 719.609 2 32 -6 0 9548.05 763.306 2 32 -6 1 10400.7 810.645 2 32 -6 2 1173.74 385.448 2 32 -6 3 3187.44 510.423 3 32 -6 3 3660.04 525.012 2 32 -6 4 1761.64 416.115 3 32 -6 4 1824.82 419.837 2 32 -6 5 2140.07 413.183 3 32 -6 5 2352.04 431.319 2 32 -6 6 1128.38 333.301 3 32 -6 6 953.789 312.977 2 32 -6 7 3608.17 424.461 2 32 -6 7 4446.12 466.072 3 32 -6 8 3102.34 360.642 3 32 -6 9 2135.29 264.965 3 32 -7 -5 2975.81 358.654 2 32 -7 -4 6829.18 558.244 2 32 -7 -3 2291.88 390.494 2 32 -7 -2 6725.91 616.405 2 32 -7 -1 2006.10 400.779 2 32 -7 0 1590.44 414.151 2 32 -7 1 1758.88 406.264 2 32 -7 2 5367.71 597.667 2 32 -7 3 2221.97 442.296 3 32 -7 3 1400.14 393.417 2 32 -7 4 6832.80 634.943 2 32 -7 4 6695.01 634.006 3 32 -7 5 2746.22 411.270 3 32 -7 5 2468.58 403.721 2 32 -7 6 5007.68 489.132 2 32 -7 6 4680.16 489.404 3 32 -7 7 2080.04 319.033 2 32 -7 7 2622.82 358.612 3 32 -7 8 4451.69 403.536 3 32 -7 9 444.875 145.309 3 32 -8 -5 3958.86 383.240 2 32 -8 -4 977.911 267.180 2 32 -8 -3 9973.32 681.125 2 32 -8 -2 4233.87 493.177 2 32 -8 -1 6501.36 619.086 2 32 -8 0 569.217 296.953 2 32 -8 1 5581.74 601.096 2 32 -8 2 3418.76 462.703 3 32 -8 2 3266.96 483.319 2 32 -8 3 10113.9 738.546 2 32 -8 3 8738.90 680.499 3 32 -8 4 1271.77 323.311 3 32 -8 4 1150.56 311.232 2 32 -8 5 3573.53 427.779 2 32 -8 5 3891.13 454.145 3 32 -8 6 1307.63 272.583 2 32 -8 6 1347.72 276.585 3 32 -8 7 3980.18 347.996 2 32 -8 7 3901.30 386.452 3 32 -8 8 612.995 169.046 3 32 -9 -6 1634.79 217.811 2 32 -9 -5 671.709 204.143 2 32 -9 -4 1272.91 266.985 2 32 -9 -3 64.1011 204.242 2 32 -9 -2 1366.78 325.615 2 32 -9 -1 2672.94 422.395 2 32 -9 0 7636.76 642.633 2 32 -9 1 1994.33 359.110 3 32 -9 1 2879.80 443.265 2 32 -9 2 2234.43 366.051 3 32 -9 2 2720.62 422.607 2 32 -9 3 361.264 225.080 3 32 -9 3 342.716 234.017 2 32 -9 4 1184.35 287.669 3 32 -9 4 1287.64 301.703 2 32 -9 5 570.378 221.543 3 32 -9 5 312.781 200.077 2 32 -9 6 984.087 210.101 2 32 -9 6 1629.06 272.792 3 32 -9 7 732.446 182.542 3 32 -10 -5 1925.52 262.903 2 32 -10 -4 294.247 175.617 2 32 -10 -3 1658.74 294.479 2 32 -10 -2 1.90584 199.024 2 32 -10 -1 1061.11 291.221 2 32 -10 0 660.407 210.114 3 32 -10 0 1182.13 313.680 2 32 -10 1 514.483 214.389 3 32 -10 1 401.038 238.291 2 32 -10 2-226.676 210.162 3 32 -10 2-34.3579 218.487 2 32 -10 3 1652.74 284.372 3 32 -10 3 1602.13 314.291 2 32 -10 4 362.495 189.521 3 32 -10 4-161.119 189.765 2 32 -10 5 2615.27 298.049 2 32 -10 5 1834.62 256.294 3 32 -10 6-94.5977 129.024 3 32 -11 -5-185.727 131.091 2 32 -11 -4-26.8722 138.187 2 32 -11 -3 116.466 158.073 2 32 -11 -2 209.621 191.562 2 32 -11 -1 179.012 195.092 2 32 -11 0 213.169 124.435 3 32 -11 0 644.719 239.520 2 32 -11 1-68.9038 107.909 3 32 -11 1-112.306 201.896 2 32 -11 2 397.604 164.807 3 32 -11 2-10.0744 170.011 2 32 -11 3 95.6821 151.318 2 32 -11 3-23.0596 125.681 3 32 -11 4 500.295 169.487 2 32 -11 4 245.388 117.187 3 32 -12 -4-0.48709 99.4690 2 32 -12 -3 603.424 160.246 2 32 -12 -2 1588.24 248.151 2 32 -12 -1 279.272 156.794 2 32 -12 0 585.796 197.768 2 32 -12 1 408.412 176.289 2 32 -12 2 1383.71 225.055 2 32 -12 3 487.668 151.165 2 32 -13 -1 461.307 132.559 2 32 -13 0 727.395 152.896 2 33 0 -1-119.675 265.676 2 33 0 0-175.907 266.168 2 33 0 1 71.3744 255.826 2 33 0 2-21.8027 272.933 2 33 0 3 74.2624 330.701 2 33 0 4 43.6106 222.221 3 33 0 4 251.904 351.698 2 33 0 5-185.612 218.286 3 33 0 5-87.8460 334.817 2 33 0 6 125.931 194.426 3 33 0 6 311.015 352.901 2 33 0 7 248.720 183.763 3 33 0 8-28.4919 166.136 3 33 -1 -2 2855.03 409.008 2 33 -1 -1 2741.06 429.379 2 33 1 0 6467.19 620.472 2 33 -1 0 6504.18 639.282 2 33 1 1 1390.41 364.027 2 33 -1 1 1531.72 376.205 2 33 1 2 2791.18 463.875 2 33 -1 2 2115.46 431.307 2 33 1 3 9893.26 798.325 2 33 -1 3 9366.59 791.204 2 33 1 3 7705.69 638.110 3 33 1 4 1443.11 315.459 3 33 1 4 1074.28 371.206 2 33 -1 4 1022.56 324.983 3 33 -1 4 919.190 368.102 2 33 1 5 2435.27 358.693 3 33 -1 5 1508.24 350.183 3 33 -1 5 2585.25 484.482 2 33 1 5 2039.48 437.194 2 33 -1 6-207.286 236.693 3 33 -1 6-309.068 335.459 2 33 1 6 52.9598 173.230 3 33 -1 7 106.862 190.460 3 33 -1 8 594.931 209.093 3 33 -1 9 1486.98 227.125 3 33 -2 -2 4486.36 521.104 2 33 -2 -1 666.939 269.709 2 33 2 0 246.599 229.776 2 33 -2 0 849.402 363.101 2 33 2 1 467.718 269.387 2 33 -2 1 275.564 266.979 2 33 -2 2 4801.29 595.018 2 33 2 2 4207.41 533.080 2 33 2 3 640.877 332.931 2 33 -2 3 505.867 307.165 2 33 -2 4 8544.73 770.461 2 33 2 4 7360.35 697.044 2 33 -2 4 8026.86 689.395 3 33 -2 5 6411.45 687.791 2 33 -2 5 4816.01 521.214 3 33 -2 6 4218.03 557.744 2 33 -2 6 4028.55 474.329 3 33 -2 7 1857.55 381.719 2 33 -2 7 2139.39 352.385 3 33 -2 8 1200.39 261.329 3 33 -2 9 827.760 215.288 3 33 -3 -3 2721.25 394.657 2 33 -3 -2 3273.03 450.163 2 33 -3 -1 8786.82 716.427 2 33 -3 0 4752.31 553.696 2 33 -3 1 12261.3 875.337 2 33 3 1 11798.6 809.135 2 33 3 2 2600.94 451.698 2 33 -3 2 2768.99 475.495 2 33 3 3 4059.52 537.391 2 33 -3 3 2764.34 502.841 2 33 -3 4 12367.6 914.970 2 33 -3 4 11248.4 808.487 3 33 -3 5 5571.81 617.646 2 33 -3 5 6428.58 618.135 3 33 -3 6 859.024 316.809 3 33 -3 6 778.461 320.154 2 33 -3 7 7702.45 638.444 2 33 -3 7 8778.42 628.328 3 33 -3 8 2348.98 334.350 3 33 -3 9 3215.79 322.860 3 33 -4 -3 2763.04 396.803 2 33 -4 -2 6061.39 584.630 2 33 -4 -1 2073.31 406.816 2 33 -4 0 7371.42 681.730 2 33 -4 1 1319.47 388.071 2 33 -4 2 6220.97 661.617 2 33 -4 3 3574.16 539.641 2 33 -4 4 7013.32 693.190 2 33 -4 4 6046.70 633.955 3 33 -4 5 3471.38 491.193 3 33 -4 5 2725.82 473.126 2 33 -4 6 5699.68 582.358 2 33 -4 6 6529.65 588.234 3 33 -4 7 1922.86 373.453 2 33 -4 7 1479.54 309.118 3 33 -4 8 4353.95 424.049 3 33 -4 9 1312.33 216.634 3 33 -5 -4 2217.30 333.581 2 33 -5 -3 5055.84 519.856 2 33 -5 -2 1809.01 372.404 2 33 -5 -1 5145.91 564.750 2 33 -5 0 4769.26 564.988 2 33 -5 1 5198.86 599.030 2 33 -5 2 2385.71 455.384 2 33 -5 3 5021.79 613.768 2 33 -5 3 6086.10 651.234 3 33 -5 4 1899.69 401.383 3 33 -5 4 2122.53 423.909 2 33 -5 5 1527.65 350.998 3 33 -5 5 1786.12 405.688 2 33 -5 6 4840.55 524.742 2 33 -5 6 5736.50 559.734 3 33 -5 7 1352.91 309.729 2 33 -5 7 1924.79 342.318 3 33 -5 8 2485.61 335.131 3 33 -5 9 1387.54 224.326 3 33 -6 -4 905.771 249.742 2 33 -6 -3 1812.30 355.863 2 33 -6 -2 740.273 289.672 2 33 -6 -1 975.352 341.713 2 33 -6 0 1599.42 384.608 2 33 -6 1 1206.37 368.049 2 33 -6 2 1295.59 379.332 2 33 -6 3 1816.50 407.906 3 33 -6 3 1496.58 395.562 2 33 -6 4 293.773 290.702 3 33 -6 4 925.695 351.116 2 33 -6 5 2240.65 423.550 3 33 -6 5 2438.52 422.609 2 33 -6 6 582.482 251.527 3 33 -6 6 472.063 245.251 2 33 -6 7 1773.75 311.601 2 33 -6 7 2109.96 344.150 3 33 -6 8 1097.52 243.336 3 33 -6 9 211.137 129.078 3 33 -7 -5-67.6390 164.166 2 33 -7 -4 93.1779 204.932 2 33 -7 -3-35.4247 213.256 2 33 -7 -2 1371.02 334.290 2 33 -7 -1 426.464 277.637 2 33 -7 0-164.953 278.377 2 33 -7 1 336.856 309.169 2 33 -7 2 1981.94 408.152 2 33 -7 3-26.1573 278.888 3 33 -7 3 128.988 295.330 2 33 -7 4 265.822 242.423 3 33 -7 4 266.137 271.001 2 33 -7 5 124.528 220.501 3 33 -7 5 318.712 238.566 2 33 -7 6 2358.63 340.133 2 33 -7 6 2299.09 357.205 3 33 -7 7 407.814 198.950 2 33 -7 7 39.8886 175.386 3 33 -7 8 504.776 169.007 3 33 -8 -5 649.514 186.881 2 33 -8 -4 1640.79 294.657 2 33 -8 -3 232.173 213.152 2 33 -8 -2 431.014 251.492 2 33 -8 -1 1502.67 367.494 2 33 -8 0 489.716 297.147 2 33 -8 1 1466.32 361.296 2 33 -8 2 286.673 260.299 3 33 -8 2 369.838 292.807 2 33 -8 3 103.406 226.263 3 33 -8 3 363.885 286.247 2 33 -8 4 1847.33 344.036 3 33 -8 4 1287.22 310.490 2 33 -8 5 809.368 262.654 3 33 -8 5 1033.37 276.122 2 33 -8 6 491.674 195.037 2 33 -8 6 346.307 201.704 3 33 -8 7 53.0110 80.4218 2 33 -8 7 37.2450 145.845 3 33 -8 8 58.5254 109.151 3 33 -9 -5 3109.50 306.234 2 33 -9 -4 580.348 206.684 2 33 -9 -3 1690.76 304.639 2 33 -9 -2 159.788 207.468 2 33 -9 -1 1618.88 356.702 2 33 -9 0 360.645 246.284 2 33 -9 1 1595.42 320.400 3 33 -9 1 1771.24 362.455 2 33 -9 2 343.173 218.715 3 33 -9 2-72.2024 251.817 2 33 -9 3 1959.02 324.014 3 33 -9 3 1856.05 340.597 2 33 -9 4 941.598 253.889 3 33 -9 4 629.840 240.370 2 33 -9 5 2985.92 341.541 2 33 -9 5 2838.96 332.802 3 33 -9 6 373.274 148.384 2 33 -9 6 291.593 159.660 3 33 -9 7 1182.19 190.132 3 33 -10 -5 482.323 140.416 2 33 -10 -4 1965.30 258.302 2 33 -10 -3 1330.33 264.373 2 33 -10 -2 4093.89 417.046 2 33 -10 -1 742.589 203.212 3 33 -10 -1 1666.24 314.192 2 33 -10 0 2932.61 387.431 2 33 -10 0 2421.61 315.367 3 33 -10 1 1305.17 254.522 3 33 -10 1 1751.97 312.939 2 33 -10 2 3301.85 388.758 2 33 -10 2 3110.66 342.343 3 33 -10 3 1134.22 230.535 3 33 -10 3 1655.49 302.447 2 33 -10 4 1647.24 263.470 2 33 -10 4 1698.73 242.707 3 33 -10 5 236.699 133.139 2 33 -10 5 365.444 148.365 3 33 -11 -4 143.515 108.891 2 33 -11 -3 2161.55 276.857 2 33 -11 -2 2456.03 308.774 2 33 -11 -1 1734.10 282.481 2 33 -11 0 3028.18 356.317 2 33 -11 1-188.592 86.3919 3 33 -11 1 1734.06 282.337 2 33 -11 2 8.05307 65.3977 3 33 -11 2 1638.76 279.384 2 33 -11 3 2008.57 267.711 2 33 -11 3-325.854 102.601 3 33 -11 4 163.911 127.892 2 33 -12 -3 1261.96 183.316 2 33 -12 -2 994.129 186.254 2 33 -12 -1 203.951 143.665 2 33 -12 0 2905.40 293.780 2 33 -12 1 631.053 170.217 2 33 -12 2 1325.41 197.101 2 34 0 -1 2092.65 357.549 2 34 0 0 9687.27 729.497 2 34 0 1 2810.35 469.490 2 34 0 2 24877.9 1199.50 2 34 0 3 261.588 281.581 2 34 0 3 216.145 227.437 3 34 0 4 23010.4 1173.42 2 34 0 4 20367.1 976.108 3 34 0 5 1697.39 413.384 2 34 0 5 1418.47 314.746 3 34 0 6 8111.33 701.742 2 34 0 6 7636.71 556.731 3 34 0 7 1857.23 289.094 3 34 -1 -1 6079.10 596.888 2 34 1 0 649.495 261.085 2 34 -1 0 377.815 313.498 2 34 1 1 6493.99 627.354 2 34 -1 1 6652.31 652.601 2 34 1 2 1241.81 374.925 2 34 -1 2 875.969 333.702 2 34 1 3 3032.22 408.607 3 34 1 3 2691.39 453.171 2 34 -1 3 2875.13 494.687 2 34 1 4 386.535 309.329 2 34 1 4 313.900 209.840 3 34 -1 4 466.729 264.115 3 34 -1 4 232.113 310.146 2 34 1 5 7925.46 565.351 3 34 -1 5 8589.92 650.417 3 34 1 5 9104.64 760.672 2 34 -1 5 9170.45 766.726 2 34 -1 6 32.7130 279.275 2 34 -1 6 948.016 269.430 3 34 -1 7 7199.13 521.023 3 34 -1 8-15.1839 145.401 3 34 -1 9 2604.24 246.710 3 34 -2 -2 5546.51 548.194 2 34 -2 -1 304.686 249.888 2 34 2 0 3540.87 462.359 2 34 -2 0 3390.97 477.679 2 34 2 1 541.632 298.537 2 34 -2 1 527.933 302.693 2 34 -2 2 4965.76 595.949 2 34 2 2 5102.27 576.742 2 34 2 3 1139.18 351.194 2 34 -2 3 1296.95 399.914 2 34 -2 4 4208.71 585.925 2 34 -2 4 2660.08 435.936 3 34 2 4 3452.51 522.796 2 34 -2 5 957.157 311.416 3 34 -2 5 400.173 334.666 2 34 -2 6 2855.57 473.609 2 34 -2 6 3541.30 435.322 3 34 -2 7 144.832 184.286 3 34 -2 8 1087.33 241.963 3 34 -2 9 35.0203 124.994 3 34 -3 -3 2677.19 377.010 2 34 -3 -2 381.628 252.370 2 34 -3 -1 1470.15 345.171 2 34 -3 0 510.317 303.412 2 34 3 1 2029.72 389.262 2 34 -3 1 1571.59 395.030 2 34 3 2 405.975 293.019 2 34 -3 2 511.439 320.634 2 34 -3 3 3178.57 507.319 2 34 -3 4 415.645 284.610 3 34 -3 4 518.004 368.637 2 34 -3 5 61.7307 303.894 2 34 -3 5 7.17234 247.943 3 34 -3 6 415.168 233.971 3 34 -3 6 654.539 325.000 2 34 -3 7 167.448 243.611 2 34 -3 7 78.7713 198.709 3 34 -3 8-205.331 179.683 3 34 -3 9 352.787 151.065 3 34 -4 -3 766.756 252.471 2 34 -4 -2 785.055 265.252 2 34 -4 -1 1388.03 371.436 2 34 -4 0 357.084 286.231 2 34 -4 1 1185.99 373.703 2 34 -4 2 511.976 331.712 2 34 -4 3 499.694 306.912 3 34 -4 3 1157.18 383.852 2 34 -4 4 160.338 260.863 3 34 -4 4 80.3552 289.190 2 34 -4 5 110.516 240.154 3 34 -4 5 161.458 280.745 2 34 -4 6 1188.57 340.103 2 34 -4 6 1176.50 293.199 3 34 -4 7-99.4827 223.606 2 34 -4 7 100.065 204.353 3 34 -4 8 66.9731 160.105 3 34 -4 9 151.703 125.326 3 34 -5 -4 446.231 210.321 2 34 -5 -3 1106.21 306.523 2 34 -5 -2 389.877 262.655 2 34 -5 -1 4233.27 512.184 2 34 -5 0 426.007 294.983 2 34 -5 1 6459.61 650.599 2 34 -5 2 76.3435 290.465 2 34 -5 3 341.666 302.145 3 34 -5 3 533.615 338.617 2 34 -5 4 441.750 282.423 3 34 -5 4 678.855 314.758 2 34 -5 5 886.068 299.909 3 34 -5 5 1617.12 373.449 2 34 -5 6 67.3340 218.287 3 34 -5 6 255.602 241.352 2 34 -5 7 3765.24 421.123 2 34 -5 7 3422.88 386.626 3 34 -5 8 483.090 197.424 3 34 -5 9 1539.20 204.461 3 34 -6 -4 5966.79 502.793 2 34 -6 -3-271.286 225.882 2 34 -6 -2 10233.2 721.333 2 34 -6 -1 477.117 309.978 2 34 -6 0 71.5876 277.459 2 34 -6 1 370.745 288.485 2 34 -6 2 8629.08 734.870 2 34 -6 3 100.604 264.407 3 34 -6 3 335.829 291.756 2 34 -6 4 6480.77 606.278 2 34 -6 4 7383.00 647.186 3 34 -6 5-100.311 229.048 3 34 -6 5 113.921 243.470 2 34 -6 6 3356.02 408.276 2 34 -6 6 3913.99 430.817 3 34 -6 7 355.776 191.981 2 34 -6 7 443.297 215.090 3 34 -6 8 2867.66 300.738 3 34 -7 -5 3583.25 337.289 2 34 -7 -4 134.723 179.713 2 34 -7 -3 3237.11 396.243 2 34 -7 -2 167.404 218.120 2 34 -7 -1 9224.88 691.414 2 34 -7 0 286.456 275.537 2 34 -7 1 9215.53 717.712 2 34 -7 2 291.968 268.681 3 34 -7 2 67.4397 264.340 2 34 -7 3 4169.47 493.474 2 34 -7 3 3677.03 485.822 3 34 -7 4 271.900 262.646 3 34 -7 4 239.013 246.872 2 34 -7 5 4074.82 457.448 2 34 -7 5 3635.09 427.011 3 34 -7 6 237.826 193.533 2 34 -7 6 231.198 187.814 3 34 -7 7 4789.35 374.813 2 34 -7 7 5164.00 415.077 3 34 -7 8 159.451 126.712 3 34 -8 -5 1320.37 223.461 2 34 -8 -4 3232.93 355.325 2 34 -8 -3 413.984 214.241 2 34 -8 -2 3484.37 428.993 2 34 -8 -1 473.471 253.756 2 34 -8 0 5138.29 538.830 2 34 -8 1 499.172 271.594 2 34 -8 2 3774.88 484.037 2 34 -8 2 4384.44 471.863 3 34 -8 3 532.745 248.574 3 34 -8 3 521.840 265.300 2 34 -8 4 3092.76 397.824 2 34 -8 4 3260.19 395.814 3 34 -8 5 798.705 232.561 3 34 -8 5 759.406 230.037 2 34 -8 6 2875.76 315.524 2 34 -8 6 2856.46 323.676 3 34 -8 7 72.5493 129.157 3 34 -9 -5 2370.63 253.748 2 34 -9 -4 358.783 168.559 2 34 -9 -3 2750.86 338.959 2 34 -9 -2 451.023 216.009 2 34 -9 -1 2587.79 376.443 2 34 -9 0 894.552 251.392 3 34 -9 0 1558.65 326.971 2 34 -9 1 1752.77 304.169 3 34 -9 1 2182.50 360.719 2 34 -9 2 179.304 201.563 3 34 -9 2 395.858 241.796 2 34 -9 3 2910.35 373.491 2 34 -9 3 3111.59 364.961 3 34 -9 4 335.301 188.073 3 34 -9 4 617.013 213.912 2 34 -9 5 2092.61 284.909 2 34 -9 5 2112.43 271.518 3 34 -9 6 100.812 123.314 3 34 -10 -4 917.621 180.802 2 34 -10 -3 129.940 144.838 2 34 -10 -2 73.3412 124.181 3 34 -10 -2-14.1290 157.961 2 34 -10 -1 359.654 175.514 3 34 -10 -1 527.512 229.482 2 34 -10 0 2119.46 276.719 3 34 -10 0 3118.38 367.413 2 34 -10 1 70.1964 145.539 3 34 -10 1-74.6107 194.537 2 34 -10 2 89.0200 143.881 3 34 -10 2 291.441 197.385 2 34 -10 3 225.115 142.795 3 34 -10 3 337.052 183.728 2 34 -10 4 712.123 197.935 2 34 -10 4 841.588 176.673 3 34 -10 5-105.053 105.336 3 34 -11 -3 159.787 141.494 2 34 -11 -2 253.429 159.161 2 34 -11 -1 194.904 164.319 2 34 -11 0 1551.73 255.097 2 34 -11 1 73.6910 159.907 2 34 -11 2 427.441 169.030 2 34 -11 3-63.7455 116.737 2 34 -12 -1-166.380 133.187 2 34 -12 0 133.935 111.788 2 35 0 0-213.652 231.121 2 35 0 1 143.512 227.904 2 35 0 2-243.999 268.969 2 35 0 3-126.197 277.745 2 35 0 3 63.2815 200.362 3 35 0 4 258.718 244.644 3 35 0 4-93.3841 292.020 2 35 0 5 27.3094 178.512 3 35 0 5 223.230 291.118 2 35 0 6-0.85120 194.731 3 35 0 7-85.5031 126.733 3 35 -1 -1 1629.66 337.156 2 35 1 0-405.963 255.952 2 35 -1 0 87.5283 247.652 2 35 1 1 745.429 295.067 2 35 -1 1 1150.58 341.628 2 35 1 2 1153.15 345.731 2 35 -1 2 1445.05 375.009 2 35 1 3 743.050 344.067 2 35 1 3 1328.16 291.226 3 35 -1 3 178.821 237.060 3 35 -1 3 1013.60 365.146 2 35 1 4 104.352 306.123 2 35 1 4 73.0485 205.350 3 35 -1 4 123.604 222.576 3 35 -1 4 370.967 306.345 2 35 -1 5 1249.73 285.882 3 35 -1 5 1519.05 387.544 2 35 -1 6 419.003 209.381 3 35 -1 6 330.049 290.137 2 35 -1 7 933.895 225.326 3 35 -1 8 323.208 148.668 3 35 -2 -2 4796.74 496.637 2 35 -2 -1 1029.73 325.538 2 35 -2 0 4922.93 561.319 2 35 2 1 1327.42 329.631 2 35 -2 1 1513.24 376.769 2 35 2 2 2642.03 408.856 2 35 -2 2 3898.19 541.254 2 35 -2 3 1838.34 355.402 3 35 2 3 1548.00 376.886 2 35 -2 3 938.902 349.838 2 35 -2 4 11276.4 827.783 2 35 -2 4 10586.8 729.936 3 35 -2 5 239.718 302.398 2 35 -2 5 584.180 265.673 3 35 -2 6 1680.10 376.527 2 35 -2 6 1538.41 306.369 3 35 -2 7 330.223 158.942 3 35 -2 8 1247.60 223.123 3 35 -3 -2 2718.69 410.428 2 35 -3 -1 6891.58 615.853 2 35 -3 0 234.616 262.027 2 35 -3 1 9201.06 749.886 2 35 -3 2 1968.05 412.763 2 35 -3 3 6525.81 660.818 2 35 -3 3 6010.27 591.087 3 35 -3 4 4949.73 590.121 2 35 -3 4 4402.07 516.366 3 35 -3 5 5656.14 595.982 2 35 -3 5 5306.68 525.443 3 35 -3 6 713.273 242.142 3 35 -3 6 277.707 273.524 2 35 -3 7 4842.54 430.682 3 35 -3 8 812.769 197.350 3 35 -4 -3 612.015 241.621 2 35 -4 -2 7809.52 631.949 2 35 -4 -1 229.362 257.011 2 35 -4 0 9702.33 745.096 2 35 -4 1 668.730 326.703 2 35 -4 2 8145.60 707.075 2 35 -4 3 498.921 330.060 3 35 -4 3 607.821 317.495 2 35 -4 4 9638.07 761.536 2 35 -4 4 8806.08 683.513 3 35 -4 5 64.6304 231.980 3 35 -4 5-174.891 241.988 2 35 -4 6 2042.09 338.931 3 35 -4 6 1808.43 350.717 2 35 -4 7 141.861 200.645 2 35 -4 7 261.782 187.191 3 35 -4 8 4149.11 351.653 3 35 -5 -3 5165.01 481.048 2 35 -5 -2 195.537 242.793 2 35 -5 -1 4355.58 504.088 2 35 -5 0 232.070 269.345 2 35 -5 1 5291.22 573.282 2 35 -5 2 745.423 344.171 2 35 -5 3 4513.21 555.196 2 35 -5 3 4579.45 546.179 3 35 -5 4 192.107 256.188 3 35 -5 4 255.701 294.659 2 35 -5 5 5649.70 566.048 2 35 -5 5 6591.00 562.414 3 35 -5 6 903.082 268.189 3 35 -5 6 544.943 245.473 2 35 -5 7 3935.35 394.244 2 35 -5 7 3997.93 388.299 3 35 -5 8 626.731 154.475 3 35 -6 -4-255.968 199.403 2 35 -6 -3-20.3336 212.078 2 35 -6 -2 3132.57 410.108 2 35 -6 -1 192.724 263.624 2 35 -6 0 689.518 295.937 2 35 -6 1 181.605 293.341 2 35 -6 2 3115.59 456.192 3 35 -6 2 3739.08 489.974 2 35 -6 3-316.645 267.957 3 35 -6 3 192.123 267.524 2 35 -6 4 142.444 221.724 3 35 -6 4 154.785 251.669 2 35 -6 5 2.96878 205.760 3 35 -6 5 279.929 220.163 2 35 -6 6 2578.54 356.551 2 35 -6 6 2564.24 337.064 3 35 -6 7 155.733 170.614 3 35 -6 8 1140.20 189.614 3 35 -7 -4 760.541 204.055 2 35 -7 -3 771.271 241.257 2 35 -7 -2 144.901 207.523 2 35 -7 -1 365.835 245.464 2 35 -7 0 26.1806 261.180 2 35 -7 1 887.861 315.927 2 35 -7 2 78.2339 217.947 3 35 -7 2 248.246 279.791 2 35 -7 3 1281.01 328.339 3 35 -7 3 579.172 277.322 2 35 -7 4 464.734 247.824 3 35 -7 4 904.368 299.672 2 35 -7 5 1308.91 276.023 3 35 -7 5 1419.56 300.652 2 35 -7 6 264.447 172.674 2 35 -7 6-125.135 191.107 3 35 -7 7 347.433 166.078 3 35 -8 -4 678.708 198.861 2 35 -8 -3 349.439 195.317 2 35 -8 -2 86.2577 212.835 2 35 -8 -1 174.415 234.813 2 35 -8 0 569.584 246.193 2 35 -8 1-96.7767 192.715 3 35 -8 1-86.1982 237.398 2 35 -8 2-65.5902 216.110 3 35 -8 2-6.22530 218.579 2 35 -8 3 200.401 208.992 3 35 -8 3 234.856 232.024 2 35 -8 4 935.901 242.744 3 35 -8 4 1007.92 263.942 2 35 -8 5 1058.78 232.874 2 35 -8 5 1030.01 235.885 3 35 -8 6 56.8255 112.886 2 35 -8 6 28.4406 126.222 3 35 -9 -4 68.2484 126.608 2 35 -9 -3 1272.06 242.056 2 35 -9 -2 896.958 243.031 2 35 -9 -1 2959.82 367.852 2 35 -9 0 387.851 185.057 3 35 -9 0 660.905 242.342 2 35 -9 1 1820.49 289.637 3 35 -9 1 2233.49 341.789 2 35 -9 2 581.062 193.747 3 35 -9 2 789.032 248.458 2 35 -9 3 1112.21 226.101 3 35 -9 3 1236.77 265.437 2 35 -9 4 765.425 194.315 3 35 -9 4 410.848 183.004 2 35 -9 5 303.388 144.417 2 35 -9 5 119.531 125.329 3 35 -10 -3 332.996 156.094 2 35 -10 -2 3157.96 323.742 2 35 -10 -2 1578.47 201.154 3 35 -10 -1 138.465 127.958 3 35 -10 -1 407.506 197.661 2 35 -10 0 1505.03 230.427 3 35 -10 0 2045.46 292.116 2 35 -10 1 415.556 143.980 3 35 -10 1 524.068 212.506 2 35 -10 2 1984.74 241.717 3 35 -10 2 2687.31 316.177 2 35 -10 3 791.829 165.256 3 35 -10 3 798.986 202.704 2 35 -10 4 974.592 179.213 2 35 -11 -2 353.995 129.572 2 35 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36 -2 2 2800.80 460.010 2 36 -2 3 2317.75 388.223 3 36 -2 3 2211.34 426.549 2 36 -2 4 1943.01 414.567 2 36 -2 4 2338.95 384.857 3 36 -2 5 1196.97 296.522 3 36 -2 5 870.854 322.672 2 36 -2 6 786.282 296.133 2 36 -2 6 876.480 243.327 3 36 -2 7 672.213 200.341 3 36 -2 8 1214.01 191.801 3 36 -3 -2 183.168 214.086 2 36 -3 -1 1228.95 345.457 2 36 -3 0 410.196 254.100 2 36 -3 1 530.731 306.372 2 36 -3 2 190.269 259.353 2 36 -3 3 129.766 234.910 3 36 -3 3 220.878 278.287 2 36 -3 4 450.909 252.114 3 36 -3 4 534.606 326.027 2 36 -3 5 1411.69 352.615 2 36 -3 5 1394.32 298.307 3 36 -3 6 206.239 231.543 2 36 -3 6 23.7722 178.747 3 36 -3 7 358.729 179.381 3 36 -3 8 108.631 116.015 3 36 -4 -3 25.1512 188.167 2 36 -4 -2 541.036 247.479 2 36 -4 -1 664.039 263.543 2 36 -4 0 15.8679 260.020 2 36 -4 1 2056.58 419.900 2 36 -4 2 760.994 302.847 2 36 -4 3 182.567 257.167 3 36 -4 3 272.673 288.036 2 36 -4 4 344.965 260.631 3 36 -4 4 298.642 254.954 2 36 -4 5 1298.20 313.521 3 36 -4 5 718.970 303.005 2 36 -4 6 283.261 200.462 3 36 -4 6 107.043 219.449 2 36 -4 7 422.428 181.315 3 36 -4 8-67.8523 123.020 3 36 -5 -3 317.590 167.705 2 36 -5 -2 3182.46 416.427 2 36 -5 -1 2000.79 367.751 2 36 -5 0-48.6901 235.216 2 36 -5 1 1925.44 395.746 2 36 -5 2 2954.87 459.346 2 36 -5 3 211.476 262.298 3 36 -5 3 90.5752 260.511 2 36 -5 4 519.650 254.821 3 36 -5 4 774.639 307.570 2 36 -5 5 723.164 275.824 2 36 -5 5 552.096 249.437 3 36 -5 6 2565.45 353.541 2 36 -5 6 2389.67 324.805 3 36 -5 7 964.306 213.302 3 36 -5 8 218.679 117.138 3 36 -6 -4 1014.98 203.088 2 36 -6 -3 1043.17 237.951 2 36 -6 -2 1486.96 303.263 2 36 -6 -1 2697.46 398.999 2 36 -6 0 1535.52 362.627 2 36 -6 1 3777.72 479.885 2 36 -6 2 1827.18 357.956 3 36 -6 2 1877.03 380.424 2 36 -6 3 232.243 225.025 3 36 -6 3 420.012 287.125 2 36 -6 4 1118.15 293.946 3 36 -6 4 1021.06 285.093 2 36 -6 5 1416.94 289.274 3 36 -6 5 1268.27 294.985 2 36 -6 6 880.286 225.169 2 36 -6 6 793.208 204.107 3 36 -6 7 4340.31 346.432 3 36 -7 -4 2209.69 268.227 2 36 -7 -3 2167.86 302.797 2 36 -7 -2 2296.59 344.433 2 36 -7 -1 2987.33 407.823 2 36 -7 0 1441.46 328.232 2 36 -7 1 2827.28 397.060 3 36 -7 1 2945.66 409.677 2 36 -7 2 2559.85 374.795 3 36 -7 2 2848.36 418.483 2 36 -7 3 2373.91 351.167 3 36 -7 3 2210.56 361.841 2 36 -7 4 2123.04 318.308 3 36 -7 4 2068.05 336.042 2 36 -7 5 2172.21 295.985 2 36 -7 5 2674.50 323.662 3 36 -7 6 1659.93 248.222 2 36 -7 6 1481.37 230.974 3 36 -7 7 1137.47 180.705 3 36 -8 -4 1084.03 192.854 2 36 -8 -3 1824.95 275.490 2 36 -8 -2 1432.34 277.275 2 36 -8 -1 1692.60 299.665 2 36 -8 0 1602.15 311.866 2 36 -8 1 1041.46 263.566 3 36 -8 1 1708.11 309.833 2 36 -8 2 1368.31 280.126 3 36 -8 2 1820.17 323.503 2 36 -8 3 1211.94 249.679 3 36 -8 3 2000.67 328.628 2 36 -8 4 1524.34 262.325 3 36 -8 4 2064.04 300.210 2 36 -8 5 628.098 175.301 2 36 -8 5 1084.01 207.886 3 36 -8 6 1109.78 181.708 3 36 -9 -3 1191.75 214.191 2 36 -9 -2 252.653 172.538 2 36 -9 -1 649.471 187.616 3 36 -9 -1 1535.60 270.973 2 36 -9 0 1899.18 259.669 3 36 -9 0 2610.53 336.630 2 36 -9 1 1106.44 221.861 3 36 -9 1 1627.65 285.848 2 36 -9 2 188.699 140.421 3 36 -9 2 446.242 203.920 2 36 -9 3 1308.54 216.762 3 36 -9 3 1456.29 260.633 2 36 -9 4 928.630 193.448 2 36 -9 4 822.380 174.185 3 36 -10 -2 374.395 154.215 2 36 -10 -1 571.037 147.700 3 36 -10 -1 400.777 169.483 2 36 -10 0 1231.25 173.393 3 36 -10 0 3151.70 316.987 2 36 -10 1 346.863 131.720 3 36 -10 1 347.935 172.784 2 36 -10 2 383.950 126.054 3 36 -10 2 692.712 189.319 2 36 -10 3 340.095 137.969 2 36 -11 0 142.799 114.760 2 37 0 0-284.303 236.416 2 37 0 1 32.9706 236.509 2 37 0 2-81.3583 211.820 3 37 0 2 306.895 250.927 2 37 0 3-94.2474 242.078 2 37 0 3 535.286 224.224 3 37 0 4 88.4429 184.002 3 37 0 4-163.380 277.750 2 37 0 5-358.507 205.324 3 37 -1 -1 254.834 226.545 2 37 1 0 2318.68 350.590 2 37 -1 0 1954.58 347.518 2 37 1 1 168.019 205.598 2 37 -1 1 122.970 251.655 2 37 1 2 76.8049 235.944 2 37 -1 2 503.096 284.689 2 37 1 2 134.629 184.330 3 37 -1 3-28.3617 272.811 2 37 1 3 3.49872 168.895 3 37 -1 3 75.1746 211.605 3 37 1 3-215.963 257.629 2 37 -1 4 1483.09 308.342 3 37 -1 4 1533.42 368.326 2 37 -1 5 304.559 199.898 3 37 -1 5-101.075 237.138 2 37 -1 6 346.005 161.729 3 37 -1 7 331.562 118.765 3 37 -2 -1 7179.70 576.931 2 37 -2 0 1994.90 368.240 2 37 -2 1 7208.01 631.033 2 37 -2 2 899.300 311.747 2 37 -2 3 2239.21 364.866 3 37 -2 3 2300.98 430.967 2 37 -2 4 17.7242 250.155 2 37 -2 4-389.798 242.942 3 37 -2 5 2725.53 425.191 2 37 -2 5 2160.28 328.736 3 37 -2 6 444.918 183.941 3 37 -2 7 1277.92 202.041 3 37 -3 -2 5018.87 471.553 2 37 -3 -1 1223.15 292.682 2 37 -3 0 5021.47 523.224 2 37 -3 1 844.738 316.342 2 37 -3 2 3994.57 498.299 2 37 -3 3 796.295 275.597 3 37 -3 3 769.169 310.072 2 37 -3 4 11196.1 751.107 2 37 -3 4 11475.3 698.959 3 37 -3 5 914.201 238.034 3 37 -3 5 684.320 284.136 2 37 -3 6 1251.37 280.092 2 37 -3 6 1138.20 225.094 3 37 -3 7 824.253 187.346 3 37 -4 -2 838.732 260.778 2 37 -4 -1 7041.48 582.005 2 37 -4 0 322.632 283.008 2 37 -4 1 6908.49 618.369 2 37 -4 2 635.846 285.436 3 37 -4 2 586.825 288.872 2 37 -4 3 5723.75 558.573 2 37 -4 3 6890.50 587.680 3 37 -4 4-22.8103 205.829 3 37 -4 4 203.470 244.834 2 37 -4 5 3272.65 417.731 2 37 -4 5 3452.42 389.814 3 37 -4 6 194.586 176.722 2 37 -4 6 520.059 188.199 3 37 -4 7 3410.39 312.260 3 37 -5 -3 1000.06 240.937 2 37 -5 -2 3163.21 400.549 2 37 -5 -1 1901.62 344.328 2 37 -5 0 1176.66 309.458 2 37 -5 1 1977.37 385.481 2 37 -5 2 3263.10 438.961 3 37 -5 2 3082.96 440.279 2 37 -5 3 819.800 276.376 3 37 -5 3 868.219 292.537 2 37 -5 4 737.227 247.143 3 37 -5 4 1023.68 296.516 2 37 -5 5 823.554 254.448 2 37 -5 5 1245.79 269.781 3 37 -5 6 1625.70 270.641 2 37 -5 6 2058.80 283.588 3 37 -5 7 537.368 163.812 3 37 -6 -3 3003.79 339.671 2 37 -6 -2 204.830 199.038 2 37 -6 -1 679.131 262.706 2 37 -6 0 64.0964 207.410 2 37 -6 1 517.499 246.840 2 37 -6 2 294.587 239.359 3 37 -6 2-92.3561 236.464 2 37 -6 3 2877.76 402.031 2 37 -6 3 2974.53 387.649 3 37 -6 4 946.571 262.609 3 37 -6 4 644.776 220.060 2 37 -6 5 1310.99 263.898 3 37 -6 5 1185.49 260.802 2 37 -6 6 263.570 158.665 2 37 -6 6-201.936 139.803 3 37 -6 7 463.984 137.748 3 37 -7 -3 677.032 200.195 2 37 -7 -2 308.137 196.165 2 37 -7 -1-447.568 235.949 2 37 -7 0 296.068 216.248 2 37 -7 1 433.926 232.607 3 37 -7 1 63.8243 217.053 2 37 -7 2 22.3418 196.891 3 37 -7 2 310.186 214.634 2 37 -7 3 219.097 180.255 3 37 -7 3 310.531 223.653 2 37 -7 4 253.407 177.890 3 37 -7 4 204.384 183.841 2 37 -7 5 448.695 187.247 2 37 -7 5 243.944 164.281 3 37 -7 6 424.051 159.982 3 37 -8 -3-42.3245 135.581 2 37 -8 -2 49.8458 153.638 2 37 -8 -1 597.374 209.563 2 37 -8 0 193.485 174.023 3 37 -8 0 556.268 228.304 2 37 -8 1 351.226 181.934 3 37 -8 1 344.553 209.857 2 37 -8 2-630.276 209.736 3 37 -8 2-149.126 190.144 2 37 -8 3 227.253 152.270 3 37 -8 3 107.844 175.178 2 37 -8 4 236.269 165.163 3 37 -8 4-162.150 162.029 2 37 -8 5 222.239 130.739 2 37 -8 5 345.975 132.333 3 37 -9 -3-359.748 112.886 3 37 -9 -3-263.898 123.034 2 37 -9 -2 216.387 115.227 3 37 -9 -2 660.938 179.027 2 37 -9 -1-99.9528 124.880 3 37 -9 -1 211.002 146.165 2 37 -9 0 1518.11 224.955 3 37 -9 0 2093.02 286.182 2 37 -9 1 0.60961 125.042 3 37 -9 1-89.1849 162.741 2 37 -9 2 432.876 149.200 3 37 -9 2 1184.97 230.570 2 37 -9 3 80.7971 109.830 3 37 -9 3 79.1899 124.177 2 37 -10 -1 1508.99 208.155 2 37 -10 0-212.604 140.458 2 37 -10 1 1653.72 218.887 2 37 -10 2 25.6874 107.770 2 38 0 0 1211.68 297.221 2 38 0 1 6670.51 569.439 2 38 0 2 1256.01 314.241 2 38 0 2 528.582 209.892 3 38 0 3 2715.78 350.014 3 38 0 3 3514.88 465.690 2 38 0 4 514.020 196.917 3 38 0 4 697.280 268.607 2 38 0 5 1368.12 227.573 3 38 -1 -1 744.474 242.788 2 38 -1 0 2177.38 355.337 2 38 -1 1 830.764 287.046 2 38 1 1 571.492 226.337 2 38 -1 2 5506.73 544.428 2 38 -1 2 5059.33 478.366 3 38 1 2 4932.97 495.437 2 38 1 2 5297.12 445.567 3 38 -1 3-38.5122 190.334 3 38 -1 3-130.180 233.646 2 38 -1 4 5117.49 507.477 2 38 -1 4 5021.28 436.622 3 38 -1 5 300.012 167.839 3 38 -1 6 1617.48 225.078 3 38 -2 -1 1955.81 309.964 2 38 -2 0 318.650 207.552 2 38 -2 1 3044.05 424.646 2 38 -2 2 320.039 258.787 2 38 -2 2-8.34935 226.154 3 38 -2 3 1408.44 324.895 2 38 -2 3 1487.63 290.738 3 38 -2 4 339.525 221.249 3 38 -2 4 462.198 263.302 2 38 -2 5 2546.87 316.666 3 38 -2 5 2492.68 368.328 2 38 -2 6 38.3719 143.219 3 38 -3 -2 439.837 206.518 2 38 -3 -1 125.591 197.820 2 38 -3 0 1137.91 296.334 2 38 -3 1 280.113 248.115 2 38 -3 2 234.424 228.965 3 38 -3 2 286.698 256.081 2 38 -3 3 404.399 224.673 3 38 -3 3-149.434 243.464 2 38 -3 4 398.994 232.264 2 38 -3 4 228.004 219.657 3 38 -3 5 86.7307 216.407 2 38 -3 5 53.6474 163.244 3 38 -3 6 304.463 168.323 3 38 -3 7-37.1258 96.2872 3 38 -4 -2 252.387 190.384 2 38 -4 -1 732.657 250.161 2 38 -4 0-89.2693 241.419 2 38 -4 1 860.638 292.828 2 38 -4 2 107.192 223.168 3 38 -4 2 303.729 233.238 2 38 -4 3-238.821 234.325 3 38 -4 3-2.10805 219.690 2 38 -4 4 33.4771 190.091 3 38 -4 4 267.507 237.694 2 38 -4 5 529.200 198.802 3 38 -4 5 696.433 241.743 2 38 -4 6 288.625 158.279 3 38 -4 7 142.837 116.205 3 38 -5 -3 201.980 145.673 2 38 -5 -2 1566.72 282.262 2 38 -5 -1 475.120 218.198 2 38 -5 0 365.043 233.406 2 38 -5 1 641.953 281.268 2 38 -5 2 1230.69 288.465 3 38 -5 2 1065.39 295.005 2 38 -5 3 159.943 200.851 3 38 -5 3 37.6001 210.303 2 38 -5 4 3015.97 379.713 2 38 -5 4 2603.32 332.294 3 38 -5 5 573.562 198.978 3 38 -5 5 256.821 203.825 2 38 -5 6 472.423 146.197 3 38 -6 -3 2117.07 268.836 2 38 -6 -2 325.605 190.115 2 38 -6 -1 2963.95 360.280 2 38 -6 0-282.223 221.265 2 38 -6 1 3589.26 418.773 2 38 -6 1 3734.07 411.619 3 38 -6 2-84.0524 184.425 3 38 -6 2-204.306 223.800 2 38 -6 3 3057.06 375.890 2 38 -6 3 2995.65 354.605 3 38 -6 4 194.135 163.253 3 38 -6 4-4.96527 185.901 2 38 -6 5 1723.73 263.123 2 38 -6 5 1849.72 250.703 3 38 -6 6 232.003 129.093 3 38 -7 -3 438.338 148.410 2 38 -7 -2 1767.16 263.003 2 38 -7 -1 134.968 170.403 2 38 -7 0 1986.83 299.993 3 38 -7 0 1759.65 298.492 2 38 -7 1-47.9686 189.038 3 38 -7 1 387.608 214.882 2 38 -7 2 1915.79 281.928 3 38 -7 2 1972.49 306.234 2 38 -7 3 160.955 176.848 3 38 -7 3 442.520 210.293 2 38 -7 4 2406.88 291.834 2 38 -7 4 2247.02 275.750 3 38 -7 5 229.704 136.474 2 38 -7 5-34.0730 115.761 3 38 -8 -2 220.229 144.088 2 38 -8 -1 3282.90 334.286 2 38 -8 -1 2226.70 273.408 3 38 -8 0 161.361 143.039 3 38 -8 0 351.518 172.464 2 38 -8 1 3509.97 353.586 2 38 -8 1 3237.92 323.666 3 38 -8 2 102.270 126.935 3 38 -8 2-15.1641 149.936 2 38 -8 3 2907.68 307.216 2 38 -8 3 2168.81 250.346 3 38 -8 4 487.967 149.406 2 38 -8 4 182.038 116.540 3 38 -9 -1 110.800 118.321 3 38 -9 -1 86.5740 123.017 2 38 -9 0 1103.50 177.794 3 38 -9 0 1881.95 248.143 2 38 -9 1 94.2234 104.588 3 38 -9 1 217.248 141.463 2 38 -9 2 629.643 138.702 3 38 -9 2 1428.54 216.200 2 39 0 0 131.914 180.332 2 39 0 1-28.9526 223.848 2 39 0 2-131.035 181.844 3 39 0 2 44.1151 198.653 2 39 0 3 99.0637 145.478 3 39 0 3 376.842 236.418 2 39 0 4 191.348 134.260 3 39 -1 0 1414.81 277.781 2 39 1 1 1226.09 249.980 3 39 -1 1 1719.87 320.265 2 39 -1 2 1672.48 327.178 2 39 -1 2 1474.87 282.674 3 39 -1 3 716.526 254.291 2 39 -1 3 409.008 210.356 3 39 -1 4 460.496 176.506 3 39 -1 4 255.618 215.053 2 39 -1 5 568.310 164.378 3 39 -2 -1 1854.00 309.554 2 39 -2 0 406.595 228.419 2 39 -2 1 2344.40 371.404 2 39 -2 2 636.863 262.726 2 39 -2 2 735.415 245.998 3 39 -2 3 245.029 188.850 3 39 -2 3 766.989 279.313 2 39 -2 4 3175.48 398.029 2 39 -2 4 2757.09 324.932 3 39 -2 5 664.672 188.534 3 39 -2 6 127.232 121.371 3 39 -3 -1 1724.97 285.689 2 39 -3 0 2362.62 344.106 2 39 -3 1 2560.28 382.104 2 39 -3 2 3624.19 429.196 2 39 -3 2 2937.05 376.460 3 39 -3 3 1252.39 291.712 2 39 -3 3 1417.09 269.599 3 39 -3 4 956.102 223.417 3 39 -3 4 998.405 273.438 2 39 -3 5 473.945 169.247 3 39 -3 5 337.447 192.726 2 39 -3 6 2856.01 265.160 3 39 -4 -2 1172.05 223.626 2 39 -4 -1 3119.41 363.224 2 39 -4 0 772.920 235.388 2 39 -4 1 3055.22 385.619 2 39 -4 2 735.512 249.627 3 39 -4 2 660.585 245.445 2 39 -4 3 4080.17 428.323 2 39 -4 3 3917.05 398.518 3 39 -4 4 1167.21 244.491 3 39 -4 4 1258.87 286.154 2 39 -4 5 2425.65 319.645 2 39 -4 5 2709.01 292.384 3 39 -4 6 426.033 137.124 3 39 -5 -2 1190.03 227.921 2 39 -5 -1 615.743 200.999 2 39 -5 0 1921.36 311.867 2 39 -5 1 640.238 229.431 3 39 -5 1 812.901 250.315 2 39 -5 2 639.450 226.616 3 39 -5 2 768.770 224.930 2 39 -5 3 1137.94 258.212 2 39 -5 3 1034.66 246.234 3 39 -5 4 1097.73 219.617 3 39 -5 4 1073.27 247.094 2 39 -5 5 318.729 173.600 2 39 -5 5 35.3743 134.923 3 39 -6 -2 270.677 157.410 2 39 -6 -1 1468.09 256.625 2 39 -6 0 68.6946 162.915 2 39 -6 1 1775.73 286.717 3 39 -6 1 1646.87 288.996 2 39 -6 2 637.642 218.076 3 39 -6 2 428.536 209.152 2 39 -6 3 1083.53 232.275 2 39 -6 3 1103.51 227.572 3 39 -6 4 16.0210 137.470 3 39 -6 4 370.038 181.624 2 39 -6 5 711.755 171.364 2 39 -6 5 281.903 127.769 3 39 -7 -2-29.1570 120.183 2 39 -7 -1-74.4392 149.147 2 39 -7 0 79.9583 149.141 3 39 -7 0 120.159 151.055 2 39 -7 1 149.696 160.021 3 39 -7 1 154.083 167.757 2 39 -7 2 98.7268 140.475 3 39 -7 2-63.2353 154.186 2 39 -7 3 277.897 154.652 2 39 -7 3 275.063 147.529 3 39 -7 4 694.919 176.754 2 39 -7 4 485.801 144.878 3 39 -8 -2 26.2692 100.014 3 39 -8 -1 72.7486 119.977 3 39 -8 -1-101.175 124.465 2 39 -8 0 110.059 122.171 3 39 -8 0-42.7481 154.705 2 39 -8 1-144.465 132.049 3 39 -8 1 0.62393 120.650 2 39 -8 2 41.2147 105.366 3 39 -8 2 108.959 131.947 2 39 -8 3 252.061 127.893 2 39 -8 3 163.367 112.248 3 40 0 1 768.364 219.036 3 40 0 1 910.166 234.448 2 40 0 2 3669.60 340.595 3 40 0 3 749.198 166.863 3 40 1 0 2795.54 301.268 3 40 -1 0 3386.49 371.539 2 40 -1 1 2650.52 358.190 2 40 -1 1 2437.96 329.599 3 40 -1 2 982.111 244.375 2 40 -1 2 938.257 216.052 3 40 -1 3 1024.96 215.238 3 40 -1 3 1392.14 279.668 2 40 -1 4 1312.60 202.097 3 40 -2 0 2422.94 326.593 2 40 -2 1-173.905 193.304 3 40 -2 1 344.661 192.054 2 40 -2 2 679.932 220.232 3 40 -2 2 1054.83 268.033 2 40 -2 3 508.176 234.249 2 40 -2 3 156.101 147.381 3 40 -2 4 662.520 183.385 3 40 -2 4 805.431 228.066 2 40 -2 5 293.696 120.534 3 40 -3 -1 437.461 168.414 2 40 -3 0-7.40503 164.259 2 40 -3 1 401.068 203.318 2 40 -3 1-175.395 195.066 3 40 -3 2 842.958 250.020 2 40 -3 2 530.212 208.298 3 40 -3 3 205.969 182.927 3 40 -3 3 147.502 205.567 2 40 -3 4 316.341 143.393 3 40 -3 4 34.5492 184.393 2 40 -3 5 322.044 132.806 3 40 -4 -1 279.883 156.900 2 40 -4 0 63.2565 169.873 2 40 -4 1 259.662 163.177 2 40 -4 1 91.1344 174.605 3 40 -4 2 461.450 207.648 2 40 -4 2-47.7750 170.404 3 40 -4 3 219.652 170.944 3 40 -4 3 231.992 171.534 2 40 -4 4 692.266 220.564 2 40 -4 4 472.821 166.532 3 40 -4 5 159.079 121.889 3 40 -5 -2 568.558 165.652 2 40 -5 -1 1097.94 213.081 2 40 -5 0 734.274 218.177 2 40 -5 1 1121.77 245.252 3 40 -5 1 1307.06 258.944 2 40 -5 2 313.531 167.490 2 40 -5 2-34.0447 172.483 3 40 -5 3 442.351 195.617 2 40 -5 3 409.145 174.075 3 40 -5 4 428.020 159.752 3 40 -5 4 315.922 165.877 2 40 -5 5 297.270 124.695 3 40 -6 -1 294.031 146.212 2 40 -6 0 909.421 211.361 3 40 -6 0 905.253 216.505 2 40 -6 1 82.4413 149.167 3 40 -6 1 94.0185 151.204 2 40 -6 2 846.625 210.316 2 40 -6 2 1023.46 208.340 3 40 -6 3 792.938 201.952 2 40 -6 3 673.617 173.518 3 40 -6 4 1684.91 233.538 2 40 -6 4 1017.95 176.198 3 40 -7 -2 116.131 108.318 3 40 -7 -1 2035.16 231.326 2 40 -7 -1 1286.76 201.013 3 40 -7 0 535.900 166.762 3 40 -7 0 796.859 179.543 2 40 -7 1 1521.70 215.837 3 40 -7 1 1916.23 247.158 2 40 -7 2 45.5290 111.107 3 40 -7 2 300.190 148.098 2 40 -7 3 1681.32 204.310 3 40 -7 3 2338.56 248.205 2 41 0 0 315.816 164.329 3 41 0 1-333.324 151.437 3 41 0 2-37.4188 116.629 3 41 -1 0-76.5993 150.076 3 41 -1 1 738.347 206.447 3 41 -1 1 330.635 146.405 2 41 -1 2 254.194 150.457 3 41 -1 3 14.7249 108.817 3 41 -2 0 1161.09 218.668 2 41 -2 1 413.157 203.459 2 41 -2 1-83.1229 170.341 3 41 -2 2 4199.76 361.034 3 41 -2 2 4762.76 415.012 2 41 -2 3 790.673 185.693 3 41 -2 3 857.561 215.351 2 41 -2 4 1324.39 183.816 3 41 -3 0 412.217 168.102 2 41 -3 1 2466.46 309.744 3 41 -3 1 2551.68 315.698 2 41 -3 2 255.052 178.003 2 41 -3 2-212.741 164.634 3 41 -3 3 1314.63 216.447 3 41 -3 3 1064.78 223.239 2 41 -3 4 299.927 134.162 3 41 -4 -1 130.994 105.309 2 41 -4 0 2300.63 272.056 2 41 -4 0 2180.42 289.619 3 41 -4 1 356.889 172.726 2 41 -4 1 253.219 170.205 3 41 -4 2 1832.86 258.865 3 41 -4 2 2028.92 273.623 2 41 -4 3 249.582 158.125 2 41 -4 3 198.235 147.168 3 41 -4 4 494.205 138.300 3 41 -4 4 784.352 194.805 2 41 -5 0 117.624 143.476 3 41 -5 0 446.670 171.342 2 41 -5 1 1610.36 240.224 2 41 -5 1 1233.66 218.006 3 41 -5 2-167.839 148.883 2 41 -5 2 49.7659 143.718 3 41 -5 3 1802.31 230.250 3 41 -5 3 1962.87 249.044 2 41 -6 -1 1.71134 116.619 3 41 -6 0 492.135 157.258 3 41 -6 0 536.828 149.707 2 41 -6 1-16.6619 115.857 2 41 -6 1 241.308 135.703 3 41 -6 2 454.967 148.256 2 41 -6 2 131.341 115.396 3 42 0 -1 20.7100 117.202 3 42 0 0 2325.85 237.988 3 42 -1 0 302.110 162.041 3 42 -1 1 1102.70 185.475 3 42 -1 2 349.811 128.618 3 42 -2 0 459.397 170.616 3 42 -2 1 238.676 134.057 3 42 -2 1 236.651 126.277 2 42 -2 2 1063.36 184.552 3 42 -3 0 122.571 133.488 3 42 -3 1 543.829 159.979 3 42 -3 1 475.848 156.065 2 42 -3 2 240.989 136.218 3 42 -3 2 245.626 132.243 2 42 -3 3 56.9425 111.123 3 42 -4 -1 172.373 137.289 3 42 -4 0 414.441 154.852 3 42 -4 1 265.990 146.908 2 42 -4 1 242.256 136.448 3 42 -4 2-75.8082 115.056 2 42 -4 2 26.3226 115.349 3 42 -5 -2 89.7136 95.5733 3 42 -5 -1-8.50522 110.580 3 42 -5 0-61.1054 122.555 3 42 -5 1 32.9588 104.920 3 42 -5 2 222.673 117.558 3 43 -3 -1 405.503 134.279 3 43 -3 0 138.692 117.067 3 0 0 0 0.00 0.00 0 TITL MRC2109 in Pna2(1) REM Pna2(1) (#33, found as P2(1)cn in -cba setting) CELL 1.54184 35.346350 15.403868 12.868979 90.0000 90.0000 90.0000 ZERR 4.00 0.000806 0.000343 0.000250 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H N O Mg W UNIT 284.00 368.00 16.00 24.00 8.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 88776 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3e _database_code_depnum_ccdc_archive 'CCDC 2116006' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT220_3e ; PROBLEM: NonSolvent Resd 1 C Ueq(max)/Ueq(min) Range 6.8 Ratio RESPONSE: The crystal was small and weakly diffracting ; _vrf_PLAT230_3e ; PROBLEM: Hirshfeld Test Diff for C01T --C021 . 7.6 s.u. RESPONSE: A consequence of a small crystal sample and a lack of high angle data. This has no significant effect on any aspect of the structure. ; _vrf_PLAT230_3e_2 ; PROBLEM: Hirshfeld Test Diff for C01T --C023 . 17.2 s.u. RESPONSE: A consequence of a small crystal sample and a lack of high angle data. This has no significant effect on any aspect of the structure. ; _vrf_PLAT919_3e ; PROBLEM: Reflection # Likely Affected by the Beamstop ... 1 Check RESPONSE: Reflections affected by position of beam stop ; _vrf_PLAT230_3e_3 ; PROBLEM: Hirshfeld Test Diff for C020 --C022 . 6.6 s.u. RESPONSE: A consequence of a small crystal sample and a lack of high angle data. This has no significant effect on any aspect of the structure. ; # Added during the CSD deposition process: Friday 15 October 2021 05:10 PM # end Validation Reply Form _audit_creation_date 2021-10-15 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _shelx_SHELXL_version_number 2018/3 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C67 H91 Mg2 Mn N4 O3' _chemical_formula_sum 'C67 H91 Mg2 Mn N4 O3' _chemical_formula_weight 1103.99 _chemical_melting_point ? _chemical_oxdiff_formula 'C63 H84 N4 O5 Mg2 Mn' _chemical_oxdiff_usercomment JMP113 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 15.2588(7) _cell_length_b 12.9668(5) _cell_length_c 35.832(3) _cell_angle_alpha 90 _cell_angle_beta 97.903(5) _cell_angle_gamma 90 _cell_volume 7022.3(7) _cell_formula_units_Z 4 _cell_measurement_reflns_used 5535 _cell_measurement_temperature 172.95(10) _cell_measurement_theta_max 26.0450 _cell_measurement_theta_min 2.7560 _shelx_estimated_absorpt_T_max 0.971 _shelx_estimated_absorpt_T_min 0.936 _exptl_absorpt_coefficient_mu 0.248 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.88015 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier . _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.044 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 2376 _exptl_crystal_size_max 0.27 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.12 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0410 _diffrn_reflns_av_unetI/netI 0.0822 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.797 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 41 _diffrn_reflns_limit_l_min -45 _diffrn_reflns_number 24313 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.797 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.429 _diffrn_reflns_theta_min 2.295 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 172.95(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.0382 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.797 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -23.00 84.00 1.00 13.61 -- 14.43 0.00 -30.00 107 2 \w -5.00 53.00 1.00 13.61 -- 14.43 37.00 30.00 58 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0057829000 _diffrn_orient_matrix_UB_12 0.0183410000 _diffrn_orient_matrix_UB_13 0.0181178000 _diffrn_orient_matrix_UB_21 -0.0357743000 _diffrn_orient_matrix_UB_22 0.0313238000 _diffrn_orient_matrix_UB_23 -0.0081565000 _diffrn_orient_matrix_UB_31 -0.0298766000 _diffrn_orient_matrix_UB_32 -0.0409710000 _diffrn_orient_matrix_UB_33 0.0019037000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 8681 _reflns_number_total 14105 _reflns_odcompleteness_completeness 98.76 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 24.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 1.056 _refine_diff_density_min -0.418 _refine_diff_density_rms 0.074 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.028 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 728 _refine_ls_number_reflns 14105 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1240 _refine_ls_R_factor_gt 0.0822 _refine_ls_restrained_S_all 1.028 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1264P)^2^+5.1912P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2192 _refine_ls_wR_factor_ref 0.2545 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Others Sof(C1)=Sof(H1A)=Sof(C2)=1-FVAR(1) Sof(C01N)=Sof(C01X)=Sof(H9)=FVAR(1) 3.a Ternary CH refined with riding coordinates: C00R(H00R), C00S(H00S), C00X(H00X), C00Y(H00Y), C012(H012), C015(H015), C019(H019), C01I(H01U) 3.b Aromatic/amide H refined with riding coordinates: C00G(H00G), C00J(H00J), C00N(H00N), C00Q(H00Q), C00Z(H00Z), C010(H010), C014(H014), C016(H016), C017(H017), C01A(H01G), C01B(H01H), C01D(H01L), C01F(H01P), C01G(H01Q), C01T(H5), C01X(H9), C020(H020), C022(H022), C023(H023), C1(H1A) 3.c Idealised Me refined as rotating group: C00V(H00A,H00B,H00C), C013(H01A,H01B,H01C), C018(H01D,H01E,H01F), C01C(H01I, H01J,H01K), C01E(H01M,H01N,H01O), C01H(H01R,H01S,H01T), C01K(H01V,H01W,H01X), C01L(H01Y,H,HA), C01M(H01Z,HB,HC), C01O(H01,HD,HE), C01P(H1,HF,HG), C01Q(H2,HH, HI), C01R(H3,HJ,HK), C01S(H4,HL,HM), C01U(H6,HN,HO), C01V(H7,HP,HQ), C01W(H8, HR,HS), C01Y(H10,HT,HU), C01Z(H11,HV,HW), C024(H02A,H02B,H02C), C5(H5A,H5B,H5C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mn01 Mn 0.77645(4) 0.58700(4) 0.59309(2) 0.0447(2) Uani 1 1 d . . . . . Mg02 Mg 0.62462(7) 0.33599(8) 0.64740(3) 0.0280(3) Uani 1 1 d . . . . . Mg03 Mg 0.81998(8) 0.24770(9) 0.61558(3) 0.0332(3) Uani 1 1 d . . . . . O004 O 0.63875(17) 0.4624(2) 0.61876(8) 0.0414(6) Uani 1 1 d . . . . . O005 O 0.86059(19) 0.3897(2) 0.61299(9) 0.0478(7) Uani 1 1 d . . . . . N006 N 0.51494(18) 0.2443(2) 0.64413(8) 0.0306(6) Uani 1 1 d . . . . . N007 N 0.60365(18) 0.3982(2) 0.69741(8) 0.0301(6) Uani 1 1 d . . . . . N008 N 0.8918(2) 0.1343(2) 0.64563(9) 0.0370(7) Uani 1 1 d . . . . . N009 N 0.8380(2) 0.1865(2) 0.56496(9) 0.0385(7) Uani 1 1 d . . . . . C00A C 0.4775(2) 0.2217(3) 0.67432(11) 0.0353(8) Uani 1 1 d . . . . . C00B C 0.5852(2) 0.5858(3) 0.69749(11) 0.0382(9) Uani 1 1 d . . . . . C00C C 1.0027(2) 0.2066(3) 0.69407(12) 0.0422(9) Uani 1 1 d . . . . . C00D C 0.9239(2) 0.1510(3) 0.68462(11) 0.0380(9) Uani 1 1 d . . . . . C00E C 0.6371(2) 0.4991(3) 0.70905(10) 0.0330(8) Uani 1 1 d . . . . . C00F C 0.5567(2) 0.3498(3) 0.72061(11) 0.0364(8) Uani 1 1 d . . . . . C00G C 0.6179(3) 0.6822(3) 0.70960(12) 0.0467(10) Uani 1 1 d . . . . . H00G H 0.584766 0.740798 0.702313 0.056 Uiso 1 1 calc R U . . . C00H C 0.8357(3) 0.2514(3) 0.53226(11) 0.0406(9) Uani 1 1 d . . . . . C00I C 0.7206(2) 0.5097(3) 0.73052(11) 0.0375(9) Uani 1 1 d . . . . . C00J C 0.6976(3) 0.6928(3) 0.73194(13) 0.0490(11) Uani 1 1 d . . . . . H00J H 0.717067 0.757743 0.740388 0.059 Uiso 1 1 calc R U . . . C00K C 0.4765(2) 0.2027(3) 0.60847(11) 0.0355(8) Uani 1 1 d . . . . . C00L C 0.7549(3) 0.2725(3) 0.50983(11) 0.0457(10) Uani 1 1 d . . . . . C00M C 0.8756(3) 0.1162(3) 0.71281(12) 0.0445(10) Uani 1 1 d . . . . . C00N C 0.5025(3) 0.2645(3) 0.70995(12) 0.0420(9) Uani 1 1 d . . . . . H00N H 0.479854 0.231360 0.729568 0.050 Uiso 1 1 calc R U . . . C00O C 0.9051(3) 0.0440(3) 0.63042(12) 0.0429(9) Uani 1 1 d . . . . . C00P C 0.4141(2) 0.2623(3) 0.58525(11) 0.0402(9) Uani 1 1 d . . . . . C00Q C 0.7483(3) 0.6081(3) 0.74180(12) 0.0462(10) Uani 1 1 d . . . . . H00Q H 0.802998 0.616466 0.756495 0.055 Uiso 1 1 calc R U . . . C00R C 0.7817(3) 0.4195(3) 0.73904(12) 0.0485(10) Uani 1 1 d . . . . . H00R H 0.745647 0.356709 0.735872 0.058 Uiso 1 1 calc R U . . . C00S C 1.0526(3) 0.2493(3) 0.66392(13) 0.0510(11) Uani 1 1 d . . . . . H00S H 1.008449 0.264710 0.642088 0.061 Uiso 1 1 calc R U . . . C00T C 0.5032(3) 0.1063(3) 0.59631(12) 0.0440(10) Uani 1 1 d . . . . . C00U C 0.8575(3) 0.0871(3) 0.56168(12) 0.0487(10) Uani 1 1 d . . . . . C00V C 0.5583(3) 0.3877(4) 0.76057(12) 0.0567(12) Uani 1 1 d . . . . . H00A H 0.617249 0.382060 0.773755 0.085 Uiso 1 1 calc R U . . . H00B H 0.518813 0.346671 0.773108 0.085 Uiso 1 1 calc R U . . . H00C H 0.539752 0.458497 0.760245 0.085 Uiso 1 1 calc R U . . . O00W O 0.8317(3) 0.6770(4) 0.66469(14) 0.1070(15) Uani 1 1 d . . . . . C00X C 0.6682(3) 0.2283(3) 0.51866(13) 0.0496(11) Uani 1 1 d . . . . . H00X H 0.682061 0.178320 0.539123 0.060 Uiso 1 1 calc R U . . . C00Y C 0.5722(3) 0.0406(3) 0.62006(13) 0.0519(11) Uani 1 1 d . . . . . H00Y H 0.594181 0.079627 0.642868 0.062 Uiso 1 1 calc R U . . . C00Z C 1.0332(3) 0.2211(4) 0.73185(13) 0.0558(12) Uani 1 1 d . . . . . H00Z H 1.085110 0.258106 0.738682 0.067 Uiso 1 1 calc R U . . . C010 C 0.8834(3) 0.0215(3) 0.59219(13) 0.0495(11) Uani 1 1 d . . . . . H010 H 0.886633 -0.047917 0.586039 0.059 Uiso 1 1 calc R U . . . C011 C 0.9137(3) 0.2951(3) 0.52381(12) 0.0491(10) Uani 1 1 d . . . . . C012 C 0.3878(3) 0.3684(3) 0.59680(13) 0.0508(11) Uani 1 1 d . . . . . H012 H 0.420336 0.383240 0.621752 0.061 Uiso 1 1 calc R U . . . C013 C 0.3988(3) 0.1490(4) 0.67132(14) 0.0564(12) Uani 1 1 d . . . . . H01A H 0.346241 0.185334 0.660995 0.085 Uiso 1 1 calc R U . . . H01B H 0.392047 0.123415 0.695907 0.085 Uiso 1 1 calc R U . . . H01C H 0.408473 0.092219 0.655171 0.085 Uiso 1 1 calc R U . . . C014 C 0.7556(3) 0.3356(4) 0.47853(13) 0.0593(12) Uani 1 1 d . . . . . H014 H 0.702868 0.349626 0.463054 0.071 Uiso 1 1 calc R U . . . C015 C 0.4959(3) 0.5758(3) 0.67334(14) 0.0520(11) Uani 1 1 d . . . . . H015 H 0.496084 0.511129 0.659230 0.062 Uiso 1 1 calc R U . . . C016 C 0.9102(3) 0.1320(4) 0.75036(13) 0.0589(12) Uani 1 1 d . . . . . H016 H 0.879671 0.107963 0.769356 0.071 Uiso 1 1 calc R U . . . C017 C 0.3770(3) 0.2204(4) 0.55059(13) 0.0573(12) Uani 1 1 d . . . . . H017 H 0.334345 0.257848 0.535193 0.069 Uiso 1 1 calc R U . . . C018 C 0.9481(3) -0.0437(3) 0.65371(14) 0.0626(13) Uani 1 1 d . . . . . H01D H 0.977835 -0.017449 0.677128 0.094 Uiso 1 1 calc R U . . . H01E H 0.990214 -0.077284 0.640197 0.094 Uiso 1 1 calc R U . . . H01F H 0.903686 -0.092391 0.658629 0.094 Uiso 1 1 calc R U . . . C019 C 0.7863(3) 0.0639(3) 0.70373(14) 0.0542(11) Uani 1 1 d . . . . . H019 H 0.772848 0.058573 0.676253 0.065 Uiso 1 1 calc R U . . . C01A C 0.9115(3) 0.3579(4) 0.49241(13) 0.0611(13) Uani 1 1 d . . . . . H01G H 0.963526 0.386895 0.486380 0.073 Uiso 1 1 calc R U . . . C01B C 0.4019(3) 0.1261(4) 0.53890(14) 0.0623(13) Uani 1 1 d . . . . . H01H H 0.376048 0.099520 0.515889 0.075 Uiso 1 1 calc R U . . . C01C C 0.7136(3) 0.1271(4) 0.71750(14) 0.0599(12) Uani 1 1 d . . . . . H01I H 0.657600 0.093818 0.710339 0.090 Uiso 1 1 calc R U . . . H01J H 0.712297 0.194652 0.706446 0.090 Uiso 1 1 calc R U . . . H01K H 0.724769 0.133009 0.744443 0.090 Uiso 1 1 calc R U . . . C01D C 0.8327(3) 0.3773(4) 0.47026(13) 0.0622(13) Uani 1 1 d . . . . . H01L H 0.831786 0.419581 0.449238 0.075 Uiso 1 1 calc R U . . . C01E C 0.6501(3) 0.0157(4) 0.59988(15) 0.0650(13) Uani 1 1 d . . . . . H01M H 0.630990 -0.027388 0.578531 0.097 Uiso 1 1 calc R U . . . H01N H 0.694400 -0.019773 0.616757 0.097 Uiso 1 1 calc R U . . . H01O H 0.674539 0.078481 0.591517 0.097 Uiso 1 1 calc R U . . . C01F C 0.4654(3) 0.0707(4) 0.56128(14) 0.0612(13) Uani 1 1 d . . . . . H01P H 0.483519 0.007489 0.552723 0.073 Uiso 1 1 calc R U . . . C01G C 0.9886(3) 0.1823(4) 0.75953(13) 0.0651(14) Uani 1 1 d . . . . . H01Q H 1.012103 0.190498 0.784714 0.078 Uiso 1 1 calc R U . . . C01H C 0.6121(3) 0.3112(4) 0.53246(15) 0.0655(13) Uani 1 1 d . . . . . H01R H 0.596063 0.360509 0.512699 0.098 Uiso 1 1 calc R U . . . H01S H 0.644842 0.345217 0.553768 0.098 Uiso 1 1 calc R U . . . H01T H 0.559571 0.281077 0.539734 0.098 Uiso 1 1 calc R U . . . C01I C 1.0022(3) 0.2745(4) 0.54809(14) 0.0641(14) Uani 1 1 d . . . . . H01U H 0.989716 0.237048 0.570526 0.077 Uiso 1 1 calc R U . . . C01J C 0.8070(4) 0.6425(5) 0.63723(16) 0.0746(16) Uani 1 1 d . . . . . C01K C 0.8471(3) 0.4147(4) 0.71117(16) 0.0710(15) Uani 1 1 d . . . . . H01V H 0.886112 0.473007 0.714796 0.106 Uiso 1 1 calc R U . . . H01W H 0.815845 0.415902 0.686011 0.106 Uiso 1 1 calc R U . . . H01X H 0.880887 0.352268 0.714942 0.106 Uiso 1 1 calc R U . . . C01L C 0.8529(4) 0.0392(4) 0.52281(15) 0.0801(17) Uani 1 1 d . . . . . H01Y H 0.896304 0.070707 0.509481 0.120 Uiso 1 1 calc R U . . . H H 0.794981 0.049913 0.509112 0.120 Uiso 1 1 calc R U . . . HA H 0.864398 -0.033489 0.525254 0.120 Uiso 1 1 calc R U . . . C01M C 0.4211(3) 0.5690(5) 0.69787(19) 0.0832(18) Uani 1 1 d . . . . . H01Z H 0.428781 0.508032 0.713190 0.125 Uiso 1 1 calc R U . . . HB H 0.365135 0.565886 0.681984 0.125 Uiso 1 1 calc R U . . . HC H 0.422681 0.628693 0.713785 0.125 Uiso 1 1 calc R U . . . C01N C 0.6991(11) 0.5161(9) 0.6082(3) 0.032(3) Uiso 0.49(4) 1 d . . P A 1 C01O C 0.4770(4) 0.6622(4) 0.64500(17) 0.0803(17) Uani 1 1 d . . . . . H01 H 0.468811 0.725499 0.657965 0.120 Uiso 1 1 calc R U . . . HD H 0.424363 0.646526 0.628052 0.120 Uiso 1 1 calc R U . . . HE H 0.525969 0.669354 0.630980 0.120 Uiso 1 1 calc R U . . . C01P C 0.6161(4) 0.1726(4) 0.48588(18) 0.0822(18) Uani 1 1 d . . . . . H1 H 0.561590 0.147764 0.493125 0.123 Uiso 1 1 calc R U . . . HF H 0.650017 0.115396 0.478662 0.123 Uiso 1 1 calc R U . . . HG H 0.603461 0.219111 0.464989 0.123 Uiso 1 1 calc R U . . . C01Q C 0.8287(5) 0.4206(5) 0.77937(16) 0.092(2) Uani 1 1 d . . . . . H2 H 0.863210 0.358820 0.784037 0.138 Uiso 1 1 calc R U . . . HH H 0.785733 0.424001 0.796524 0.138 Uiso 1 1 calc R U . . . HI H 0.866963 0.479587 0.782962 0.138 Uiso 1 1 calc R U . . . C01R C 1.0475(4) 0.3735(6) 0.5613(2) 0.095(2) Uani 1 1 d . . . . . H3 H 1.070276 0.406165 0.540574 0.143 Uiso 1 1 calc R U . . . HJ H 1.095297 0.359009 0.580918 0.143 Uiso 1 1 calc R U . . . HK H 1.005818 0.418638 0.570779 0.143 Uiso 1 1 calc R U . . . C01S C 0.4118(5) 0.4504(4) 0.56966(18) 0.0888(19) Uani 1 1 d . . . . . H4 H 0.378979 0.438676 0.545191 0.133 Uiso 1 1 calc R U . . . HL H 0.473979 0.447001 0.568056 0.133 Uiso 1 1 calc R U . . . HM H 0.397446 0.517256 0.578596 0.133 Uiso 1 1 calc R U . . . C01T C 0.7385(5) 0.5820(6) 0.5321(2) 0.093(2) Uani 1 1 d . . . . . H5 H 0.712219 0.523521 0.520405 0.112 Uiso 1 1 calc R U . . . C01U C 0.5322(5) -0.0612(5) 0.6323(2) 0.099(2) Uani 1 1 d . . . . . H6 H 0.483640 -0.046263 0.645808 0.149 Uiso 1 1 calc R U . . . HN H 0.576606 -0.099214 0.648203 0.149 Uiso 1 1 calc R U . . . HO H 0.511486 -0.101557 0.610347 0.149 Uiso 1 1 calc R U . . . C01V C 0.7841(4) -0.0462(4) 0.7201(2) 0.098(2) Uani 1 1 d . . . . . H7 H 0.801005 -0.043841 0.746909 0.147 Uiso 1 1 calc R U . . . HP H 0.824594 -0.089437 0.709011 0.147 Uiso 1 1 calc R U . . . HQ H 0.725346 -0.073767 0.714579 0.147 Uiso 1 1 calc R U . . . C01W C 1.1146(4) 0.1724(5) 0.65116(17) 0.0832(17) Uani 1 1 d . . . . . H8 H 1.145389 0.202969 0.632295 0.125 Uiso 1 1 calc R U . . . HR H 1.081877 0.113488 0.640738 0.125 Uiso 1 1 calc R U . . . HS H 1.156570 0.151265 0.672215 0.125 Uiso 1 1 calc R U . . . C01X C 0.8642(16) 0.4828(10) 0.6040(3) 0.047(4) Uiso 0.49(4) 1 d . . P A 1 H9 H 0.921324 0.505620 0.602297 0.057 Uiso 0.49(4) 1 calc R U P A 1 C01Y C 1.0631(5) 0.2074(7) 0.5283(2) 0.125(3) Uani 1 1 d . . . . . H10 H 1.034335 0.143073 0.521305 0.188 Uiso 1 1 calc R U . . . HT H 1.116774 0.194584 0.545040 0.188 Uiso 1 1 calc R U . . . HU H 1.076746 0.242094 0.506180 0.188 Uiso 1 1 calc R U . . . C01Z C 1.1003(4) 0.3488(5) 0.6749(2) 0.099(2) Uani 1 1 d . . . . . H11 H 1.147854 0.335931 0.694816 0.149 Uiso 1 1 calc R U . . . HV H 1.059704 0.397252 0.683393 0.149 Uiso 1 1 calc R U . . . HW H 1.123658 0.376745 0.653502 0.149 Uiso 1 1 calc R U . . . C020 C 0.7621(6) 0.7397(5) 0.5668(2) 0.106(3) Uani 1 1 d . . . . . H020 H 0.753481 0.799082 0.580355 0.127 Uiso 1 1 calc R U . . . C021 C 0.6936(5) 0.6711(8) 0.5470(2) 0.108(3) Uani 1 1 d . . . . . C022 C 0.8393(6) 0.6980(6) 0.5609(3) 0.122(3) Uani 1 1 d . . . . . H022 H 0.895030 0.724747 0.569361 0.147 Uiso 1 1 calc R U . . . C023 C 0.8212(8) 0.6025(7) 0.5387(2) 0.133(4) Uani 1 1 d . . . . . H023 H 0.864932 0.561916 0.530393 0.160 Uiso 1 1 calc R U . . . C024 C 0.2898(5) 0.3742(6) 0.5996(4) 0.167(5) Uani 1 1 d . . . . . H02A H 0.256614 0.356257 0.575758 0.251 Uiso 1 1 calc R U . . . H02B H 0.274846 0.443035 0.606301 0.251 Uiso 1 1 calc R U . . . H02C H 0.275748 0.326931 0.618548 0.251 Uiso 1 1 calc R U . . . HX H 0.719(2) 0.262(3) 0.6356(11) 0.042(10) Uiso 1 1 d . . . . . C1 C 0.6670(17) 0.5345(14) 0.6042(4) 0.058(4) Uani 0.51(4) 1 d . . P A 2 H1A H 0.621313 0.579553 0.595380 0.069 Uiso 0.51(4) 1 calc R U P A 2 C2 C 0.8235(16) 0.4732(8) 0.6023(3) 0.053(4) Uani 0.51(4) 1 d . . P A 2 C5 C 0.5982(6) 0.6941(11) 0.5440(4) 0.217(7) Uani 1 1 d . . . . . H5A H 0.566457 0.632405 0.548475 0.325 Uiso 1 1 calc R U . . . H5B H 0.577478 0.719780 0.519241 0.325 Uiso 1 1 calc R U . . . H5C H 0.588484 0.745268 0.562400 0.325 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Mn01 0.0562(4) 0.0307(3) 0.0517(4) 0.0053(3) 0.0234(3) -0.0023(3) Mg02 0.0268(6) 0.0261(6) 0.0315(6) -0.0002(5) 0.0055(5) -0.0032(5) Mg03 0.0349(6) 0.0333(6) 0.0312(6) 0.0000(5) 0.0043(5) 0.0090(5) O004 0.0483(16) 0.0345(14) 0.0426(16) 0.0059(12) 0.0102(13) -0.0031(13) O005 0.0536(17) 0.0337(15) 0.0573(19) 0.0045(13) 0.0126(14) 0.0009(14) N006 0.0304(15) 0.0270(14) 0.0340(16) 0.0004(13) 0.0026(12) -0.0051(13) N007 0.0315(15) 0.0245(14) 0.0346(16) -0.0016(12) 0.0060(12) -0.0023(12) N008 0.0371(17) 0.0347(16) 0.0387(18) 0.0063(14) 0.0032(14) 0.0090(14) N009 0.0455(18) 0.0368(17) 0.0338(17) 0.0020(14) 0.0076(14) 0.0093(15) C00A 0.0348(19) 0.0272(18) 0.044(2) 0.0014(16) 0.0073(16) -0.0075(16) C00B 0.041(2) 0.036(2) 0.041(2) -0.0079(17) 0.0182(17) -0.0003(17) C00C 0.032(2) 0.046(2) 0.047(2) 0.0016(19) -0.0011(17) 0.0178(18) C00D 0.036(2) 0.036(2) 0.040(2) 0.0051(17) -0.0005(16) 0.0138(17) C00E 0.040(2) 0.0276(18) 0.035(2) -0.0039(15) 0.0154(16) -0.0044(16) C00F 0.041(2) 0.036(2) 0.035(2) 0.0007(16) 0.0117(16) -0.0084(17) C00G 0.059(3) 0.030(2) 0.056(3) -0.0073(18) 0.026(2) 0.0062(19) C00H 0.052(2) 0.040(2) 0.032(2) -0.0023(17) 0.0115(17) 0.0068(19) C00I 0.040(2) 0.0322(19) 0.041(2) -0.0023(16) 0.0090(17) -0.0030(17) C00J 0.057(3) 0.037(2) 0.057(3) -0.015(2) 0.020(2) -0.019(2) C00K 0.0329(19) 0.0332(19) 0.039(2) 0.0016(16) 0.0006(16) -0.0144(16) C00L 0.057(3) 0.044(2) 0.036(2) 0.0007(18) 0.0019(19) 0.002(2) C00M 0.045(2) 0.046(2) 0.041(2) 0.0096(19) 0.0031(18) 0.0130(19) C00N 0.047(2) 0.039(2) 0.042(2) 0.0032(18) 0.0141(18) -0.0108(19) C00O 0.042(2) 0.039(2) 0.048(2) 0.0051(19) 0.0056(18) 0.0088(18) C00P 0.0311(19) 0.043(2) 0.045(2) 0.0030(18) -0.0019(17) -0.0075(17) C00Q 0.048(2) 0.040(2) 0.053(3) -0.0123(19) 0.0123(19) -0.016(2) C00R 0.052(2) 0.043(2) 0.046(2) -0.0067(19) -0.008(2) -0.006(2) C00S 0.033(2) 0.061(3) 0.057(3) 0.007(2) -0.0004(19) 0.008(2) C00T 0.052(2) 0.032(2) 0.046(2) -0.0034(18) -0.0016(19) -0.0093(18) C00U 0.056(3) 0.043(2) 0.047(3) -0.008(2) 0.008(2) 0.009(2) C00V 0.073(3) 0.060(3) 0.042(2) -0.013(2) 0.024(2) -0.027(2) O00W 0.128(4) 0.108(4) 0.084(3) -0.032(3) 0.011(3) -0.022(3) C00X 0.049(2) 0.050(2) 0.048(3) 0.005(2) -0.001(2) -0.001(2) C00Y 0.070(3) 0.034(2) 0.048(3) -0.0058(19) -0.003(2) 0.000(2) C00Z 0.035(2) 0.072(3) 0.057(3) -0.003(2) -0.007(2) 0.015(2) C010 0.061(3) 0.035(2) 0.052(3) -0.0044(19) 0.007(2) 0.013(2) C011 0.048(2) 0.054(2) 0.047(2) -0.002(2) 0.0136(19) 0.006(2) C012 0.037(2) 0.057(3) 0.055(3) 0.005(2) -0.0047(19) 0.007(2) C013 0.052(3) 0.063(3) 0.057(3) -0.004(2) 0.019(2) -0.025(2) C014 0.062(3) 0.062(3) 0.050(3) 0.011(2) -0.003(2) -0.001(2) C015 0.045(2) 0.041(2) 0.070(3) -0.015(2) 0.006(2) 0.013(2) C016 0.056(3) 0.079(3) 0.041(3) 0.017(2) 0.006(2) 0.017(3) C017 0.047(2) 0.063(3) 0.055(3) 0.007(2) -0.018(2) -0.011(2) C018 0.078(3) 0.043(2) 0.065(3) 0.003(2) 0.003(3) 0.026(2) C019 0.059(3) 0.049(2) 0.056(3) 0.012(2) 0.013(2) -0.007(2) C01A 0.063(3) 0.074(3) 0.050(3) 0.011(2) 0.018(2) 0.002(3) C01B 0.073(3) 0.058(3) 0.049(3) -0.011(2) -0.017(2) -0.018(3) C01C 0.047(2) 0.073(3) 0.060(3) 0.004(3) 0.007(2) -0.004(2) C01D 0.079(3) 0.072(3) 0.036(2) 0.014(2) 0.010(2) -0.003(3) C01E 0.072(3) 0.057(3) 0.064(3) 0.003(2) 0.005(3) 0.003(3) C01F 0.078(3) 0.041(2) 0.061(3) -0.012(2) -0.006(3) -0.014(2) C01G 0.056(3) 0.095(4) 0.039(3) -0.002(3) -0.012(2) 0.026(3) C01H 0.064(3) 0.067(3) 0.068(3) -0.023(3) 0.019(2) -0.012(3) C01I 0.048(3) 0.089(4) 0.057(3) 0.019(3) 0.016(2) 0.008(3) C01J 0.090(4) 0.083(4) 0.049(3) 0.016(3) 0.005(3) -0.009(3) C01K 0.066(3) 0.067(3) 0.081(4) 0.000(3) 0.013(3) 0.023(3) C01L 0.126(5) 0.060(3) 0.056(3) -0.013(3) 0.018(3) 0.027(3) C01M 0.039(3) 0.095(4) 0.118(5) 0.009(4) 0.016(3) 0.001(3) C01O 0.074(4) 0.077(4) 0.086(4) 0.012(3) 0.001(3) 0.019(3) C01P 0.076(4) 0.079(4) 0.092(4) -0.047(3) 0.012(3) -0.016(3) C01Q 0.118(5) 0.089(4) 0.059(4) 0.000(3) -0.019(3) 0.022(4) C01R 0.053(3) 0.125(5) 0.103(5) 0.010(4) -0.004(3) -0.016(4) C01S 0.130(5) 0.053(3) 0.082(4) 0.000(3) 0.010(4) 0.006(3) C01T 0.081(4) 0.097(5) 0.107(6) 0.008(4) 0.032(4) -0.027(4) C01U 0.105(5) 0.068(4) 0.127(6) 0.042(4) 0.023(4) 0.006(4) C01V 0.099(4) 0.063(3) 0.136(6) 0.039(4) 0.026(4) -0.002(3) C01W 0.080(4) 0.094(4) 0.082(4) 0.019(3) 0.035(3) 0.023(3) C01Y 0.084(5) 0.156(7) 0.136(7) -0.014(6) 0.012(4) 0.055(5) C01Z 0.096(4) 0.103(5) 0.104(5) -0.019(4) 0.030(4) -0.046(4) C020 0.123(6) 0.067(4) 0.143(7) 0.029(4) 0.075(5) 0.006(4) C021 0.083(4) 0.157(7) 0.084(5) 0.067(5) 0.010(4) 0.010(5) C022 0.123(6) 0.096(5) 0.157(8) 0.038(6) 0.053(6) -0.040(5) C023 0.200(10) 0.110(6) 0.115(6) 0.051(5) 0.115(7) 0.056(7) C024 0.086(5) 0.093(5) 0.344(16) -0.001(7) 0.108(7) 0.024(4) C1 0.046(8) 0.068(8) 0.061(7) 0.008(6) 0.016(6) -0.001(6) C2 0.042(9) 0.058(6) 0.058(6) -0.014(5) 0.007(5) -0.009(5) C5 0.089(6) 0.322(17) 0.235(13) 0.136(13) 0.011(7) 0.013(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Mn01 C01J 1.742(6) . ? Mn01 C01N 1.646(12) . ? Mn01 C01T 2.184(8) . ? Mn01 C01X 1.905(15) . ? Mn01 C020 2.191(6) . ? Mn01 C021 2.222(6) . ? Mn01 C022 2.151(6) . ? Mn01 C023 2.163(6) . ? Mn01 C1 1.895(17) . ? Mn01 C2 1.653(12) . ? Mg02 Mg03 3.5258(16) . ? Mg02 O004 1.962(3) . ? Mg02 N006 2.043(3) . ? Mg02 N007 2.030(3) . ? Mg02 HX 1.83(4) . ? Mg03 O005 1.949(3) . ? Mg03 N008 2.049(3) . ? Mg03 N009 2.033(3) . ? Mg03 HX 1.80(4) . ? O004 C01N 1.253(13) . ? O004 C1 1.181(13) . ? O005 C01X 1.252(13) . ? O005 C2 1.258(13) . ? N006 C00A 1.324(5) . ? N006 C00K 1.436(5) . ? N007 C00E 1.445(4) . ? N007 C00F 1.328(4) . ? N008 C00D 1.432(5) . ? N008 C00O 1.320(5) . ? N009 C00H 1.439(5) . ? N009 C00U 1.332(5) . ? C00A C00N 1.396(5) . ? C00A C013 1.519(5) . ? C00B C00E 1.405(5) . ? C00B C00G 1.393(5) . ? C00B C015 1.516(6) . ? C00C C00D 1.403(6) . ? C00C C00S 1.510(6) . ? C00C C00Z 1.383(6) . ? C00D C00M 1.404(6) . ? C00E C00I 1.402(5) . ? C00F C00N 1.402(5) . ? C00F C00V 1.511(5) . ? C00G H00G 0.9300 . ? C00G C00J 1.367(6) . ? C00H C00L 1.403(6) . ? C00H C011 1.388(6) . ? C00I C00Q 1.387(5) . ? C00I C00R 1.500(6) . ? C00J H00J 0.9300 . ? C00J C00Q 1.362(6) . ? C00K C00P 1.407(5) . ? C00K C00T 1.402(5) . ? C00L C00X 1.515(6) . ? C00L C014 1.390(6) . ? C00M C016 1.392(6) . ? C00M C019 1.517(6) . ? C00N H00N 0.9300 . ? C00O C010 1.395(6) . ? C00O C018 1.507(6) . ? C00P C012 1.507(6) . ? C00P C017 1.401(6) . ? C00Q H00Q 0.9300 . ? C00R H00R 0.9800 . ? C00R C01K 1.507(7) . ? C00R C01Q 1.523(6) . ? C00S H00S 0.9800 . ? C00S C01W 1.489(7) . ? C00S C01Z 1.508(7) . ? C00T C00Y 1.521(6) . ? C00T C01F 1.387(6) . ? C00U C010 1.399(6) . ? C00U C01L 1.518(6) . ? C00V H00A 0.9600 . ? C00V H00B 0.9600 . ? C00V H00C 0.9600 . ? O00W C01J 1.099(6) . ? C00X H00X 0.9800 . ? C00X C01H 1.500(6) . ? C00X C01P 1.509(6) . ? C00Y H00Y 0.9800 . ? C00Y C01E 1.509(7) . ? C00Y C01U 1.543(7) . ? C00Z H00Z 0.9300 . ? C00Z C01G 1.372(7) . ? C010 H010 0.9300 . ? C011 C01A 1.386(6) . ? C011 C01I 1.526(6) . ? C012 H012 0.9800 . ? C012 C01S 1.519(7) . ? C012 C024 1.515(8) . ? C013 H01A 0.9600 . ? C013 H01B 0.9600 . ? C013 H01C 0.9600 . ? C014 H014 0.9300 . ? C014 C01D 1.364(7) . ? C015 H015 0.9800 . ? C015 C01M 1.535(7) . ? C015 C01O 1.512(7) . ? C016 H016 0.9300 . ? C016 C01G 1.363(7) . ? C017 H017 0.9300 . ? C017 C01B 1.363(7) . ? C018 H01D 0.9600 . ? C018 H01E 0.9600 . ? C018 H01F 0.9600 . ? C019 H019 0.9800 . ? C019 C01C 1.516(6) . ? C019 C01V 1.546(7) . ? C01A H01G 0.9300 . ? C01A C01D 1.370(7) . ? C01B H01H 0.9300 . ? C01B C01F 1.373(7) . ? C01C H01I 0.9600 . ? C01C H01J 0.9600 . ? C01C H01K 0.9600 . ? C01D H01L 0.9300 . ? C01E H01M 0.9600 . ? C01E H01N 0.9600 . ? C01E H01O 0.9600 . ? C01F H01P 0.9300 . ? C01G H01Q 0.9300 . ? C01H H01R 0.9600 . ? C01H H01S 0.9600 . ? C01H H01T 0.9600 . ? C01I H01U 0.9800 . ? C01I C01R 1.503(8) . ? C01I C01Y 1.518(8) . ? C01K H01V 0.9600 . ? C01K H01W 0.9600 . ? C01K H01X 0.9600 . ? C01L H01Y 0.9600 . ? C01L H 0.9600 . ? C01L HA 0.9600 . ? C01M H01Z 0.9600 . ? C01M HB 0.9600 . ? C01M HC 0.9600 . ? C01O H01 0.9600 . ? C01O HD 0.9600 . ? C01O HE 0.9600 . ? C01P H1 0.9600 . ? C01P HF 0.9600 . ? C01P HG 0.9600 . ? C01Q H2 0.9600 . ? C01Q HH 0.9600 . ? C01Q HI 0.9600 . ? C01R H3 0.9600 . ? C01R HJ 0.9600 . ? C01R HK 0.9600 . ? C01S H4 0.9600 . ? C01S HL 0.9600 . ? C01S HM 0.9600 . ? C01T H5 0.9300 . ? C01T C021 1.480(11) . ? C01T C023 1.279(12) . ? C01U H6 0.9600 . ? C01U HN 0.9600 . ? C01U HO 0.9600 . ? C01V H7 0.9600 . ? C01V HP 0.9600 . ? C01V HQ 0.9600 . ? C01W H8 0.9600 . ? C01W HR 0.9600 . ? C01W HS 0.9600 . ? C01X H9 0.9300 . ? C01Y H10 0.9600 . ? C01Y HT 0.9600 . ? C01Y HU 0.9600 . ? C01Z H11 0.9600 . ? C01Z HV 0.9600 . ? C01Z HW 0.9600 . ? C020 H020 0.9300 . ? C020 C021 1.477(11) . ? C020 C022 1.338(10) . ? C021 C5 1.476(11) . ? C022 H022 0.9300 . ? C022 C023 1.478(12) . ? C023 H023 0.9300 . ? C024 H02A 0.9600 . ? C024 H02B 0.9600 . ? C024 H02C 0.9600 . ? C1 H1A 0.9300 . ? C5 H5A 0.9600 . ? C5 H5B 0.9600 . ? C5 H5C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C01J Mn01 C01T 157.2(3) . . ? C01J Mn01 C01X 90.8(4) . . ? C01J Mn01 C020 90.9(3) . . ? C01J Mn01 C021 121.7(3) . . ? C01J Mn01 C022 97.3(3) . . ? C01J Mn01 C023 134.6(4) . . ? C01J Mn01 C1 95.3(4) . . ? C01N Mn01 C01J 92.6(4) . . ? C01N Mn01 C01T 102.1(4) . . ? C01N Mn01 C01X 93.0(5) . . ? C01N Mn01 C020 127.8(6) . . ? C01N Mn01 C021 99.1(6) . . ? C01N Mn01 C022 160.6(6) . . ? C01N Mn01 C023 132.8(5) . . ? C01T Mn01 C020 66.4(3) . . ? C01T Mn01 C021 39.3(3) . . ? C01X Mn01 C01T 105.4(4) . . ? C01X Mn01 C020 139.0(7) . . ? C01X Mn01 C021 144.3(4) . . ? C01X Mn01 C022 103.4(7) . . ? C01X Mn01 C023 87.2(5) . . ? C020 Mn01 C021 39.1(3) . . ? C022 Mn01 C01T 63.8(3) . . ? C022 Mn01 C020 35.9(3) . . ? C022 Mn01 C021 61.5(3) . . ? C022 Mn01 C023 40.1(3) . . ? C023 Mn01 C01T 34.2(3) . . ? C023 Mn01 C020 63.4(3) . . ? C023 Mn01 C021 60.2(3) . . ? C1 Mn01 C01T 94.5(5) . . ? C1 Mn01 C020 112.1(8) . . ? C1 Mn01 C021 84.5(8) . . ? C1 Mn01 C022 145.4(8) . . ? C1 Mn01 C023 128.2(6) . . ? C2 Mn01 C01J 97.7(5) . . ? C2 Mn01 C01T 102.7(4) . . ? C2 Mn01 C020 155.0(7) . . ? C2 Mn01 C021 140.5(5) . . ? C2 Mn01 C022 119.4(8) . . ? C2 Mn01 C023 94.6(5) . . ? C2 Mn01 C1 90.5(6) . . ? Mg03 Mg02 HX 13.4(12) . . ? O004 Mg02 Mg03 86.77(9) . . ? O004 Mg02 N006 127.19(12) . . ? O004 Mg02 N007 99.89(12) . . ? O004 Mg02 HX 100.0(12) . . ? N006 Mg02 Mg03 120.99(9) . . ? N006 Mg02 HX 110.1(12) . . ? N007 Mg02 Mg03 131.09(9) . . ? N007 Mg02 N006 93.12(12) . . ? N007 Mg02 HX 129.6(12) . . ? Mg02 Mg03 HX 13.7(12) . . ? O005 Mg03 Mg02 89.83(9) . . ? O005 Mg03 N008 123.53(14) . . ? O005 Mg03 N009 104.07(14) . . ? O005 Mg03 HX 102.7(12) . . ? N008 Mg03 Mg02 118.55(10) . . ? N008 Mg03 HX 106.7(12) . . ? N009 Mg03 Mg02 129.76(10) . . ? N009 Mg03 N008 93.48(13) . . ? N009 Mg03 HX 128.6(12) . . ? C01N O004 Mg02 139.4(8) . . ? C1 O004 Mg02 165.1(14) . . ? C01X O005 Mg03 161.5(10) . . ? C2 O005 Mg03 134.0(10) . . ? C00A N006 Mg02 121.6(2) . . ? C00A N006 C00K 118.3(3) . . ? C00K N006 Mg02 120.1(2) . . ? C00E N007 Mg02 121.5(2) . . ? C00F N007 Mg02 121.9(2) . . ? C00F N007 C00E 116.6(3) . . ? C00D N008 Mg03 119.4(2) . . ? C00O N008 Mg03 121.4(3) . . ? C00O N008 C00D 119.1(3) . . ? C00H N009 Mg03 120.5(2) . . ? C00U N009 Mg03 121.1(3) . . ? C00U N009 C00H 118.3(3) . . ? N006 C00A C00N 124.4(3) . . ? N006 C00A C013 120.4(3) . . ? C00N C00A C013 115.2(4) . . ? C00E C00B C015 121.8(3) . . ? C00G C00B C00E 117.5(4) . . ? C00G C00B C015 120.7(4) . . ? C00D C00C C00S 121.0(4) . . ? C00Z C00C C00D 117.9(4) . . ? C00Z C00C C00S 121.1(4) . . ? C00C C00D N008 118.7(4) . . ? C00C C00D C00M 120.6(4) . . ? C00M C00D N008 120.7(3) . . ? C00B C00E N007 118.5(3) . . ? C00I C00E N007 120.4(3) . . ? C00I C00E C00B 121.1(3) . . ? N007 C00F C00N 123.5(3) . . ? N007 C00F C00V 120.0(3) . . ? C00N C00F C00V 116.6(3) . . ? C00B C00G H00G 119.2 . . ? C00J C00G C00B 121.6(4) . . ? C00J C00G H00G 119.2 . . ? C00L C00H N009 120.1(4) . . ? C011 C00H N009 119.4(4) . . ? C011 C00H C00L 120.5(4) . . ? C00E C00I C00R 121.8(3) . . ? C00Q C00I C00E 117.9(4) . . ? C00Q C00I C00R 120.1(4) . . ? C00G C00J H00J 120.0 . . ? C00Q C00J C00G 119.9(4) . . ? C00Q C00J H00J 120.0 . . ? C00P C00K N006 118.7(3) . . ? C00T C00K N006 120.8(3) . . ? C00T C00K C00P 120.5(4) . . ? C00H C00L C00X 122.1(4) . . ? C014 C00L C00H 118.3(4) . . ? C014 C00L C00X 119.7(4) . . ? C00D C00M C019 122.3(4) . . ? C016 C00M C00D 118.7(4) . . ? C016 C00M C019 119.0(4) . . ? C00A C00N C00F 129.7(4) . . ? C00A C00N H00N 115.1 . . ? C00F C00N H00N 115.1 . . ? N008 C00O C010 124.2(4) . . ? N008 C00O C018 121.4(4) . . ? C010 C00O C018 114.4(4) . . ? C00K C00P C012 121.5(4) . . ? C017 C00P C00K 118.0(4) . . ? C017 C00P C012 120.5(4) . . ? C00I C00Q H00Q 119.1 . . ? C00J C00Q C00I 121.8(4) . . ? C00J C00Q H00Q 119.1 . . ? C00I C00R H00R 107.5 . . ? C00I C00R C01K 110.3(4) . . ? C00I C00R C01Q 112.6(4) . . ? C01K C00R H00R 107.5 . . ? C01K C00R C01Q 111.1(4) . . ? C01Q C00R H00R 107.5 . . ? C00C C00S H00S 106.7 . . ? C01W C00S C00C 112.3(4) . . ? C01W C00S H00S 106.7 . . ? C01W C00S C01Z 110.4(5) . . ? C01Z C00S C00C 113.6(4) . . ? C01Z C00S H00S 106.7 . . ? C00K C00T C00Y 122.2(4) . . ? C01F C00T C00K 118.4(4) . . ? C01F C00T C00Y 119.3(4) . . ? N009 C00U C010 124.2(4) . . ? N009 C00U C01L 119.6(4) . . ? C010 C00U C01L 116.2(4) . . ? C00F C00V H00A 109.5 . . ? C00F C00V H00B 109.5 . . ? C00F C00V H00C 109.5 . . ? H00A C00V H00B 109.5 . . ? H00A C00V H00C 109.5 . . ? H00B C00V H00C 109.5 . . ? C00L C00X H00X 107.6 . . ? C01H C00X C00L 110.6(4) . . ? C01H C00X H00X 107.6 . . ? C01H C00X C01P 109.7(4) . . ? C01P C00X C00L 113.6(4) . . ? C01P C00X H00X 107.6 . . ? C00T C00Y H00Y 108.0 . . ? C00T C00Y C01U 111.5(4) . . ? C01E C00Y C00T 112.5(4) . . ? C01E C00Y H00Y 108.0 . . ? C01E C00Y C01U 108.7(4) . . ? C01U C00Y H00Y 108.0 . . ? C00C C00Z H00Z 119.2 . . ? C01G C00Z C00C 121.6(4) . . ? C01G C00Z H00Z 119.2 . . ? C00O C010 C00U 130.1(4) . . ? C00O C010 H010 115.0 . . ? C00U C010 H010 115.0 . . ? C00H C011 C01I 121.5(4) . . ? C01A C011 C00H 119.4(4) . . ? C01A C011 C01I 119.1(4) . . ? C00P C012 H012 108.1 . . ? C00P C012 C01S 111.5(4) . . ? C00P C012 C024 111.5(5) . . ? C01S C012 H012 108.1 . . ? C024 C012 H012 108.1 . . ? C024 C012 C01S 109.5(5) . . ? C00A C013 H01A 109.5 . . ? C00A C013 H01B 109.5 . . ? C00A C013 H01C 109.5 . . ? H01A C013 H01B 109.5 . . ? H01A C013 H01C 109.5 . . ? H01B C013 H01C 109.5 . . ? C00L C014 H014 119.6 . . ? C01D C014 C00L 120.7(4) . . ? C01D C014 H014 119.6 . . ? C00B C015 H015 107.5 . . ? C00B C015 C01M 111.0(4) . . ? C01M C015 H015 107.5 . . ? C01O C015 C00B 113.1(4) . . ? C01O C015 H015 107.5 . . ? C01O C015 C01M 109.9(4) . . ? C00M C016 H016 119.7 . . ? C01G C016 C00M 120.5(5) . . ? C01G C016 H016 119.7 . . ? C00P C017 H017 119.2 . . ? C01B C017 C00P 121.6(4) . . ? C01B C017 H017 119.2 . . ? C00O C018 H01D 109.5 . . ? C00O C018 H01E 109.5 . . ? C00O C018 H01F 109.5 . . ? H01D C018 H01E 109.5 . . ? H01D C018 H01F 109.5 . . ? H01E C018 H01F 109.5 . . ? C00M C019 H019 107.7 . . ? C00M C019 C01V 113.4(4) . . ? C01C C019 C00M 111.4(4) . . ? C01C C019 H019 107.7 . . ? C01C C019 C01V 108.8(4) . . ? C01V C019 H019 107.7 . . ? C011 C01A H01G 120.0 . . ? C01D C01A C011 120.0(5) . . ? C01D C01A H01G 120.0 . . ? C017 C01B H01H 120.2 . . ? C017 C01B C01F 119.6(4) . . ? C01F C01B H01H 120.2 . . ? C019 C01C H01I 109.5 . . ? C019 C01C H01J 109.5 . . ? C019 C01C H01K 109.5 . . ? H01I C01C H01J 109.5 . . ? H01I C01C H01K 109.5 . . ? H01J C01C H01K 109.5 . . ? C014 C01D C01A 121.1(4) . . ? C014 C01D H01L 119.5 . . ? C01A C01D H01L 119.5 . . ? C00Y C01E H01M 109.5 . . ? C00Y C01E H01N 109.5 . . ? C00Y C01E H01O 109.5 . . ? H01M C01E H01N 109.5 . . ? H01M C01E H01O 109.5 . . ? H01N C01E H01O 109.5 . . ? C00T C01F H01P 119.1 . . ? C01B C01F C00T 121.8(4) . . ? C01B C01F H01P 119.1 . . ? C00Z C01G H01Q 119.8 . . ? C016 C01G C00Z 120.5(4) . . ? C016 C01G H01Q 119.8 . . ? C00X C01H H01R 109.5 . . ? C00X C01H H01S 109.5 . . ? C00X C01H H01T 109.5 . . ? H01R C01H H01S 109.5 . . ? H01R C01H H01T 109.5 . . ? H01S C01H H01T 109.5 . . ? C011 C01I H01U 107.4 . . ? C01R C01I C011 111.3(4) . . ? C01R C01I H01U 107.4 . . ? C01R C01I C01Y 110.6(5) . . ? C01Y C01I C011 112.6(5) . . ? C01Y C01I H01U 107.4 . . ? O00W C01J Mn01 175.5(6) . . ? C00R C01K H01V 109.5 . . ? C00R C01K H01W 109.5 . . ? C00R C01K H01X 109.5 . . ? H01V C01K H01W 109.5 . . ? H01V C01K H01X 109.5 . . ? H01W C01K H01X 109.5 . . ? C00U C01L H01Y 109.5 . . ? C00U C01L H 109.5 . . ? C00U C01L HA 109.5 . . ? H01Y C01L H 109.5 . . ? H01Y C01L HA 109.5 . . ? H C01L HA 109.5 . . ? C015 C01M H01Z 109.5 . . ? C015 C01M HB 109.5 . . ? C015 C01M HC 109.5 . . ? H01Z C01M HB 109.5 . . ? H01Z C01M HC 109.5 . . ? HB C01M HC 109.5 . . ? O004 C01N Mn01 178.2(11) . . ? C015 C01O H01 109.5 . . ? C015 C01O HD 109.5 . . ? C015 C01O HE 109.5 . . ? H01 C01O HD 109.5 . . ? H01 C01O HE 109.5 . . ? HD C01O HE 109.5 . . ? C00X C01P H1 109.5 . . ? C00X C01P HF 109.5 . . ? C00X C01P HG 109.5 . . ? H1 C01P HF 109.5 . . ? H1 C01P HG 109.5 . . ? HF C01P HG 109.5 . . ? C00R C01Q H2 109.5 . . ? C00R C01Q HH 109.5 . . ? C00R C01Q HI 109.5 . . ? H2 C01Q HH 109.5 . . ? H2 C01Q HI 109.5 . . ? HH C01Q HI 109.5 . . ? C01I C01R H3 109.5 . . ? C01I C01R HJ 109.5 . . ? C01I C01R HK 109.5 . . ? H3 C01R HJ 109.5 . . ? H3 C01R HK 109.5 . . ? HJ C01R HK 109.5 . . ? C012 C01S H4 109.5 . . ? C012 C01S HL 109.5 . . ? C012 C01S HM 109.5 . . ? H4 C01S HL 109.5 . . ? H4 C01S HM 109.5 . . ? HL C01S HM 109.5 . . ? Mn01 C01T H5 120.9 . . ? C021 C01T Mn01 71.8(4) . . ? C021 C01T H5 127.3 . . ? C023 C01T Mn01 72.0(5) . . ? C023 C01T H5 127.3 . . ? C023 C01T C021 105.4(7) . . ? C00Y C01U H6 109.5 . . ? C00Y C01U HN 109.5 . . ? C00Y C01U HO 109.5 . . ? H6 C01U HN 109.5 . . ? H6 C01U HO 109.5 . . ? HN C01U HO 109.5 . . ? C019 C01V H7 109.5 . . ? C019 C01V HP 109.5 . . ? C019 C01V HQ 109.5 . . ? H7 C01V HP 109.5 . . ? H7 C01V HQ 109.5 . . ? HP C01V HQ 109.5 . . ? C00S C01W H8 109.5 . . ? C00S C01W HR 109.5 . . ? C00S C01W HS 109.5 . . ? H8 C01W HR 109.5 . . ? H8 C01W HS 109.5 . . ? HR C01W HS 109.5 . . ? Mn01 C01X H9 113.5 . . ? O005 C01X Mn01 133.0(17) . . ? O005 C01X H9 113.5 . . ? C01I C01Y H10 109.5 . . ? C01I C01Y HT 109.5 . . ? C01I C01Y HU 109.5 . . ? H10 C01Y HT 109.5 . . ? H10 C01Y HU 109.5 . . ? HT C01Y HU 109.5 . . ? C00S C01Z H11 109.5 . . ? C00S C01Z HV 109.5 . . ? C00S C01Z HW 109.5 . . ? H11 C01Z HV 109.5 . . ? H11 C01Z HW 109.5 . . ? HV C01Z HW 109.5 . . ? Mn01 C020 H020 122.4 . . ? C021 C020 Mn01 71.6(3) . . ? C021 C020 H020 127.4 . . ? C022 C020 Mn01 70.4(4) . . ? C022 C020 H020 127.4 . . ? C022 C020 C021 105.2(7) . . ? C01T C021 Mn01 69.0(4) . . ? C020 C021 Mn01 69.3(4) . . ? C020 C021 C01T 108.1(6) . . ? C5 C021 Mn01 127.5(6) . . ? C5 C021 C01T 129.3(10) . . ? C5 C021 C020 122.6(10) . . ? Mn01 C022 H022 121.9 . . ? C020 C022 Mn01 73.7(4) . . ? C020 C022 H022 125.7 . . ? C020 C022 C023 108.7(8) . . ? C023 C022 Mn01 70.4(3) . . ? C023 C022 H022 125.7 . . ? Mn01 C023 H023 124.3 . . ? C01T C023 Mn01 73.8(4) . . ? C01T C023 C022 112.3(7) . . ? C01T C023 H023 123.8 . . ? C022 C023 Mn01 69.6(4) . . ? C022 C023 H023 123.8 . . ? C012 C024 H02A 109.5 . . ? C012 C024 H02B 109.5 . . ? C012 C024 H02C 109.5 . . ? H02A C024 H02B 109.5 . . ? H02A C024 H02C 109.5 . . ? H02B C024 H02C 109.5 . . ? Mn01 C1 H1A 110.2 . . ? O004 C1 Mn01 140(2) . . ? O004 C1 H1A 110.2 . . ? O005 C2 Mn01 173.7(8) . . ? C021 C5 H5A 109.5 . . ? C021 C5 H5B 109.5 . . ? C021 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Mn01 C01T C021 C020 58.4(4) . . . . ? Mn01 C01T C021 C5 -121.9(8) . . . . ? Mn01 C01T C023 C022 -59.2(5) . . . . ? Mn01 C020 C021 C01T -58.2(4) . . . . ? Mn01 C020 C021 C5 122.1(7) . . . . ? Mn01 C020 C022 C023 62.1(5) . . . . ? Mn01 C022 C023 C01T 61.6(6) . . . . ? Mg02 O004 C1 Mn01 11(4) . . . . ? Mg02 N006 C00A C00N 6.4(5) . . . . ? Mg02 N006 C00A C013 -176.9(3) . . . . ? Mg02 N006 C00K C00P -86.7(4) . . . . ? Mg02 N006 C00K C00T 90.8(4) . . . . ? Mg02 N007 C00E C00B 86.9(3) . . . . ? Mg02 N007 C00E C00I -91.4(4) . . . . ? Mg02 N007 C00F C00N -14.0(5) . . . . ? Mg02 N007 C00F C00V 167.4(3) . . . . ? Mg03 O005 C01X Mn01 37(3) . . . . ? Mg03 N008 C00D C00C -82.6(4) . . . . ? Mg03 N008 C00D C00M 94.8(4) . . . . ? Mg03 N008 C00O C010 9.1(6) . . . . ? Mg03 N008 C00O C018 -172.4(3) . . . . ? Mg03 N009 C00H C00L -87.3(4) . . . . ? Mg03 N009 C00H C011 90.9(4) . . . . ? Mg03 N009 C00U C010 -12.5(6) . . . . ? Mg03 N009 C00U C01L 168.0(4) . . . . ? N006 C00A C00N C00F 13.2(7) . . . . ? N006 C00K C00P C012 0.7(5) . . . . ? N006 C00K C00P C017 -179.8(4) . . . . ? N006 C00K C00T C00Y 0.9(6) . . . . ? N006 C00K C00T C01F -178.6(4) . . . . ? N007 C00E C00I C00Q -178.2(3) . . . . ? N007 C00E C00I C00R 6.0(5) . . . . ? N007 C00F C00N C00A -8.9(7) . . . . ? N008 C00D C00M C016 178.6(4) . . . . ? N008 C00D C00M C019 -2.7(6) . . . . ? N008 C00O C010 C00U 10.9(8) . . . . ? N009 C00H C00L C00X -0.4(6) . . . . ? N009 C00H C00L C014 179.9(4) . . . . ? N009 C00H C011 C01A -179.7(4) . . . . ? N009 C00H C011 C01I 1.0(6) . . . . ? N009 C00U C010 C00O -9.0(8) . . . . ? C00A N006 C00K C00P 93.3(4) . . . . ? C00A N006 C00K C00T -89.2(4) . . . . ? C00B C00E C00I C00Q 3.6(5) . . . . ? C00B C00E C00I C00R -172.2(4) . . . . ? C00B C00G C00J C00Q 2.2(6) . . . . ? C00C C00D C00M C016 -4.1(6) . . . . ? C00C C00D C00M C019 174.7(4) . . . . ? C00C C00Z C01G C016 -3.0(7) . . . . ? C00D N008 C00O C010 -174.6(4) . . . . ? C00D N008 C00O C018 3.9(6) . . . . ? C00D C00C C00S C01W -86.2(5) . . . . ? C00D C00C C00S C01Z 147.7(4) . . . . ? C00D C00C C00Z C01G 0.3(6) . . . . ? C00D C00M C016 C01G 1.4(7) . . . . ? C00D C00M C019 C01C -116.0(5) . . . . ? C00D C00M C019 C01V 121.0(5) . . . . ? C00E N007 C00F C00N 164.2(4) . . . . ? C00E N007 C00F C00V -14.3(5) . . . . ? C00E C00B C00G C00J 0.0(6) . . . . ? C00E C00B C015 C01M 92.1(5) . . . . ? C00E C00B C015 C01O -143.8(4) . . . . ? C00E C00I C00Q C00J -1.3(6) . . . . ? C00E C00I C00R C01K 96.1(5) . . . . ? C00E C00I C00R C01Q -139.2(5) . . . . ? C00F N007 C00E C00B -91.4(4) . . . . ? C00F N007 C00E C00I 90.4(4) . . . . ? C00G C00B C00E N007 178.8(3) . . . . ? C00G C00B C00E C00I -2.9(5) . . . . ? C00G C00B C015 C01M -86.7(5) . . . . ? C00G C00B C015 C01O 37.4(6) . . . . ? C00G C00J C00Q C00I -1.6(6) . . . . ? C00H N009 C00U C010 163.5(4) . . . . ? C00H N009 C00U C01L -16.0(6) . . . . ? C00H C00L C00X C01H 109.1(5) . . . . ? C00H C00L C00X C01P -127.0(5) . . . . ? C00H C00L C014 C01D -1.1(7) . . . . ? C00H C011 C01A C01D 0.7(7) . . . . ? C00H C011 C01I C01R -125.5(5) . . . . ? C00H C011 C01I C01Y 109.7(6) . . . . ? C00K N006 C00A C00N -173.6(4) . . . . ? C00K N006 C00A C013 3.1(5) . . . . ? C00K C00P C012 C01S 117.7(5) . . . . ? C00K C00P C012 C024 -119.6(6) . . . . ? C00K C00P C017 C01B -1.8(7) . . . . ? C00K C00T C00Y C01E -122.3(4) . . . . ? C00K C00T C00Y C01U 115.3(5) . . . . ? C00K C00T C01F C01B -1.3(7) . . . . ? C00L C00H C011 C01A -1.6(6) . . . . ? C00L C00H C011 C01I 179.1(4) . . . . ? C00L C014 C01D C01A 0.2(8) . . . . ? C00M C016 C01G C00Z 2.1(7) . . . . ? C00O N008 C00D C00C 101.0(4) . . . . ? C00O N008 C00D C00M -81.6(5) . . . . ? C00P C00K C00T C00Y 178.4(4) . . . . ? C00P C00K C00T C01F -1.2(6) . . . . ? C00P C017 C01B C01F -0.6(8) . . . . ? C00Q C00I C00R C01K -79.6(5) . . . . ? C00Q C00I C00R C01Q 45.1(6) . . . . ? C00R C00I C00Q C00J 174.6(4) . . . . ? C00S C00C C00D N008 0.7(5) . . . . ? C00S C00C C00D C00M -176.7(3) . . . . ? C00S C00C C00Z C01G -179.7(4) . . . . ? C00T C00K C00P C012 -176.8(4) . . . . ? C00T C00K C00P C017 2.7(6) . . . . ? C00U N009 C00H C00L 96.7(5) . . . . ? C00U N009 C00H C011 -85.1(5) . . . . ? C00V C00F C00N C00A 169.7(4) . . . . ? C00X C00L C014 C01D 179.2(4) . . . . ? C00Y C00T C01F C01B 179.1(5) . . . . ? C00Z C00C C00D N008 -179.4(3) . . . . ? C00Z C00C C00D C00M 3.2(6) . . . . ? C00Z C00C C00S C01W 93.9(5) . . . . ? C00Z C00C C00S C01Z -32.2(6) . . . . ? C011 C00H C00L C00X -178.5(4) . . . . ? C011 C00H C00L C014 1.7(6) . . . . ? C011 C01A C01D C014 0.0(8) . . . . ? C012 C00P C017 C01B 177.7(4) . . . . ? C013 C00A C00N C00F -163.6(4) . . . . ? C014 C00L C00X C01H -71.1(5) . . . . ? C014 C00L C00X C01P 52.7(6) . . . . ? C015 C00B C00E N007 0.0(5) . . . . ? C015 C00B C00E C00I 178.2(4) . . . . ? C015 C00B C00G C00J 178.8(4) . . . . ? C016 C00M C019 C01C 62.7(5) . . . . ? C016 C00M C019 C01V -60.3(6) . . . . ? C017 C00P C012 C01S -61.8(6) . . . . ? C017 C00P C012 C024 61.0(7) . . . . ? C017 C01B C01F C00T 2.2(8) . . . . ? C018 C00O C010 C00U -167.7(5) . . . . ? C019 C00M C016 C01G -177.4(4) . . . . ? C01A C011 C01I C01R 55.2(6) . . . . ? C01A C011 C01I C01Y -69.6(7) . . . . ? C01F C00T C00Y C01E 57.3(5) . . . . ? C01F C00T C00Y C01U -65.2(6) . . . . ? C01I C011 C01A C01D -180.0(5) . . . . ? C01J Mn01 C1 O004 -83.2(13) . . . . ? C01L C00U C010 C00O 170.6(5) . . . . ? C01T Mn01 C1 O004 117.4(13) . . . . ? C020 Mn01 C1 O004 -176.3(12) . . . . ? C020 C022 C023 Mn01 -64.2(5) . . . . ? C020 C022 C023 C01T -2.5(9) . . . . ? C021 Mn01 C1 O004 155.4(14) . . . . ? C021 C01T C023 Mn01 64.5(5) . . . . ? C021 C01T C023 C022 5.3(8) . . . . ? C021 C020 C022 Mn01 -63.6(4) . . . . ? C021 C020 C022 C023 -1.6(8) . . . . ? C022 Mn01 C1 O004 165.8(10) . . . . ? C022 C020 C021 Mn01 62.9(5) . . . . ? C022 C020 C021 C01T 4.6(8) . . . . ? C022 C020 C021 C5 -175.1(7) . . . . ? C023 Mn01 C1 O004 110.8(14) . . . . ? C023 C01T C021 Mn01 -64.6(5) . . . . ? C023 C01T C021 C020 -6.2(8) . . . . ? C023 C01T C021 C5 173.5(8) . . . . ? C2 Mn01 C1 O004 14.6(14) . . . . ? _smtbx_masks_special_details ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.181 -0.270 0.123 295.1 36.5 '1 pentane' 2 -0.181 0.230 0.377 295.1 36.6 '1 pentane' 3 0.181 -0.230 0.623 295.1 36.5 '1 pentane' 4 -0.181 0.270 0.877 295.1 36.6 '1 pentane' 5 0.500 0.000 1.000 36.8 5.0 ? 6 0.500 0.500 0.500 36.8 5.0 ? _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL mrc2122_a.res in P2(1)/c mrc2122.res created by SHELXL-2018/3 at 12:18:56 on 15-Oct-2021 REM Old TITL MRC2122 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.258, Rweak 0.436, Alpha 0.069 REM 1.192 for 600 systematic absences, Orientation as input REM Formula found by SHELXT: C65 N2 O7 Mg2 Mn CELL 0.71073 15.2588 12.9668 35.832 90 97.903 90 ZERR 4 0.0007 0.0005 0.0026 0 0.005 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Mg Mn N O UNIT 268 364 8 4 16 12 L.S. 6 PLAN 10 SIZE 0.27 0.12 0.14 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta ABIN REM REM REM WGHT 0.126400 5.191200 FVAR 0.33727 0.49295 MN01 4 0.776447 0.587001 0.593095 11.00000 0.05621 0.03074 = 0.05174 0.00528 0.02341 -0.00229 MG02 3 0.624618 0.335992 0.647401 11.00000 0.02685 0.02608 = 0.03148 -0.00022 0.00550 -0.00324 MG03 3 0.819978 0.247702 0.615581 11.00000 0.03494 0.03329 = 0.03118 0.00004 0.00433 0.00904 O004 6 0.638750 0.462420 0.618765 11.00000 0.04832 0.03455 = 0.04257 0.00591 0.01021 -0.00308 O005 6 0.860590 0.389732 0.612989 11.00000 0.05363 0.03373 = 0.05734 0.00455 0.01256 0.00094 N006 5 0.514939 0.244310 0.644131 11.00000 0.03044 0.02696 = 0.03399 0.00035 0.00260 -0.00506 N007 5 0.603647 0.398189 0.697412 11.00000 0.03148 0.02454 = 0.03458 -0.00161 0.00604 -0.00232 N008 5 0.891783 0.134338 0.645633 11.00000 0.03708 0.03468 = 0.03874 0.00627 0.00322 0.00902 N009 5 0.838035 0.186538 0.564960 11.00000 0.04554 0.03676 = 0.03384 0.00203 0.00763 0.00926 C00A 1 0.477528 0.221675 0.674323 11.00000 0.03484 0.02719 = 0.04430 0.00137 0.00730 -0.00750 C00B 1 0.585152 0.585841 0.697489 11.00000 0.04095 0.03626 = 0.04102 -0.00786 0.01816 -0.00026 C00C 1 1.002671 0.206603 0.694069 11.00000 0.03235 0.04570 = 0.04663 0.00164 -0.00113 0.01783 C00D 1 0.923868 0.151017 0.684624 11.00000 0.03622 0.03581 = 0.04026 0.00507 -0.00051 0.01383 C00E 1 0.637100 0.499108 0.709055 11.00000 0.03971 0.02756 = 0.03460 -0.00394 0.01541 -0.00438 C00F 1 0.556657 0.349757 0.720610 11.00000 0.04057 0.03590 = 0.03456 0.00073 0.01174 -0.00838 C00G 1 0.617903 0.682199 0.709601 11.00000 0.05931 0.03024 = 0.05565 -0.00734 0.02639 0.00617 AFIX 43 H00G 2 0.584766 0.740798 0.702313 11.00000 -1.20000 AFIX 0 C00H 1 0.835720 0.251411 0.532256 11.00000 0.05199 0.03960 = 0.03181 -0.00230 0.01150 0.00681 C00I 1 0.720608 0.509691 0.730516 11.00000 0.03998 0.03221 = 0.04119 -0.00229 0.00901 -0.00296 C00J 1 0.697553 0.692791 0.731937 11.00000 0.05668 0.03702 = 0.05650 -0.01479 0.01971 -0.01888 AFIX 43 H00J 2 0.717067 0.757743 0.740388 11.00000 -1.20000 AFIX 0 C00K 1 0.476529 0.202652 0.608471 11.00000 0.03289 0.03323 = 0.03923 0.00156 0.00056 -0.01445 C00L 1 0.754928 0.272495 0.509829 11.00000 0.05662 0.04351 = 0.03569 0.00069 0.00195 0.00242 C00M 1 0.875557 0.116151 0.712807 11.00000 0.04548 0.04590 = 0.04144 0.00959 0.00308 0.01305 C00N 1 0.502529 0.264451 0.709949 11.00000 0.04711 0.03949 = 0.04163 0.00319 0.01410 -0.01079 AFIX 43 H00N 2 0.479854 0.231360 0.729568 11.00000 -1.20000 AFIX 0 C00O 1 0.905133 0.044004 0.630416 11.00000 0.04168 0.03862 = 0.04819 0.00510 0.00555 0.00876 C00P 1 0.414076 0.262252 0.585252 11.00000 0.03113 0.04281 = 0.04453 0.00301 -0.00193 -0.00753 C00Q 1 0.748300 0.608080 0.741798 11.00000 0.04781 0.03960 = 0.05267 -0.01229 0.01233 -0.01629 AFIX 43 H00Q 2 0.802998 0.616466 0.756495 11.00000 -1.20000 AFIX 0 C00R 1 0.781666 0.419486 0.739036 11.00000 0.05236 0.04283 = 0.04608 -0.00674 -0.00813 -0.00638 AFIX 13 H00R 2 0.745647 0.356709 0.735872 11.00000 -1.20000 AFIX 0 C00S 1 1.052564 0.249270 0.663921 11.00000 0.03311 0.06071 = 0.05729 0.00714 -0.00044 0.00789 AFIX 13 H00S 2 1.008449 0.264710 0.642088 11.00000 -1.20000 AFIX 0 C00T 1 0.503207 0.106305 0.596312 11.00000 0.05195 0.03174 = 0.04595 -0.00344 -0.00163 -0.00931 C00U 1 0.857545 0.087111 0.561677 11.00000 0.05584 0.04347 = 0.04700 -0.00772 0.00826 0.00944 C00V 1 0.558265 0.387707 0.760573 11.00000 0.07288 0.06007 = 0.04156 -0.01288 0.02409 -0.02704 AFIX 137 H00A 2 0.617249 0.382060 0.773755 11.00000 -1.50000 H00B 2 0.518813 0.346671 0.773108 11.00000 -1.50000 H00C 2 0.539752 0.458497 0.760245 11.00000 -1.50000 AFIX 0 O00W 6 0.831682 0.676992 0.664695 11.00000 0.12784 0.10836 = 0.08382 -0.03158 0.01124 -0.02182 C00X 1 0.668211 0.228331 0.518656 11.00000 0.04899 0.04950 = 0.04842 0.00515 -0.00054 -0.00145 AFIX 13 H00X 2 0.682061 0.178320 0.539123 11.00000 -1.20000 AFIX 0 C00Y 1 0.572231 0.040628 0.620062 11.00000 0.07036 0.03428 = 0.04774 -0.00579 -0.00332 0.00043 AFIX 13 H00Y 2 0.594181 0.079627 0.642868 11.00000 -1.20000 AFIX 0 C00Z 1 1.033152 0.221135 0.731854 11.00000 0.03488 0.07194 = 0.05671 -0.00253 -0.00747 0.01459 AFIX 43 H00Z 2 1.085110 0.258106 0.738682 11.00000 -1.20000 AFIX 0 C010 1 0.883411 0.021529 0.592192 11.00000 0.06120 0.03519 = 0.05187 -0.00437 0.00684 0.01284 AFIX 43 H010 2 0.886633 -0.047917 0.586039 11.00000 -1.20000 AFIX 0 C011 1 0.913687 0.295080 0.523807 11.00000 0.04822 0.05405 = 0.04698 -0.00219 0.01363 0.00584 C012 1 0.387835 0.368360 0.596804 11.00000 0.03742 0.05722 = 0.05464 0.00466 -0.00467 0.00734 AFIX 13 H012 2 0.420336 0.383240 0.621752 11.00000 -1.20000 AFIX 0 C013 1 0.398834 0.148974 0.671323 11.00000 0.05198 0.06338 = 0.05693 -0.00435 0.01902 -0.02534 AFIX 137 H01A 2 0.346241 0.185334 0.660995 11.00000 -1.50000 H01B 2 0.392047 0.123415 0.695907 11.00000 -1.50000 H01C 2 0.408473 0.092219 0.655171 11.00000 -1.50000 AFIX 0 C014 1 0.755588 0.335633 0.478530 11.00000 0.06219 0.06239 = 0.05013 0.01143 -0.00328 -0.00076 AFIX 43 H014 2 0.702868 0.349626 0.463054 11.00000 -1.20000 AFIX 0 C015 1 0.495865 0.575846 0.673343 11.00000 0.04490 0.04060 = 0.07001 -0.01461 0.00650 0.01330 AFIX 13 H015 2 0.496084 0.511129 0.659230 11.00000 -1.20000 AFIX 0 C016 1 0.910239 0.131969 0.750363 11.00000 0.05606 0.07902 = 0.04134 0.01726 0.00586 0.01690 AFIX 43 H016 2 0.879671 0.107963 0.769356 11.00000 -1.20000 AFIX 0 C017 1 0.376989 0.220397 0.550590 11.00000 0.04711 0.06325 = 0.05455 0.00695 -0.01782 -0.01092 AFIX 43 H017 2 0.334345 0.257848 0.535193 11.00000 -1.20000 AFIX 0 C018 1 0.948117 -0.043741 0.653705 11.00000 0.07772 0.04324 = 0.06498 0.00327 0.00339 0.02564 AFIX 137 H01D 2 0.977835 -0.017449 0.677128 11.00000 -1.50000 H01E 2 0.990214 -0.077284 0.640197 11.00000 -1.50000 H01F 2 0.903686 -0.092391 0.658629 11.00000 -1.50000 AFIX 0 C019 1 0.786253 0.063884 0.703728 11.00000 0.05885 0.04881 = 0.05647 0.01235 0.01307 -0.00679 AFIX 13 H019 2 0.772848 0.058573 0.676253 11.00000 -1.20000 AFIX 0 C01A 1 0.911515 0.357913 0.492409 11.00000 0.06255 0.07404 = 0.04960 0.01115 0.01829 0.00178 AFIX 43 H01G 2 0.963526 0.386895 0.486380 11.00000 -1.20000 AFIX 0 C01B 1 0.401903 0.126122 0.538897 11.00000 0.07270 0.05801 = 0.04912 -0.01084 -0.01710 -0.01761 AFIX 43 H01H 2 0.376048 0.099520 0.515889 11.00000 -1.20000 AFIX 0 C01C 1 0.713569 0.127137 0.717501 11.00000 0.04699 0.07281 = 0.05969 0.00414 0.00693 -0.00397 AFIX 137 H01I 2 0.657600 0.093818 0.710339 11.00000 -1.50000 H01J 2 0.712297 0.194652 0.706446 11.00000 -1.50000 H01K 2 0.724769 0.133009 0.744443 11.00000 -1.50000 AFIX 0 C01D 1 0.832715 0.377312 0.470257 11.00000 0.07931 0.07239 = 0.03553 0.01350 0.01040 -0.00298 AFIX 43 H01L 2 0.831786 0.419581 0.449238 11.00000 -1.20000 AFIX 0 C01E 1 0.650121 0.015723 0.599882 11.00000 0.07222 0.05735 = 0.06418 0.00294 0.00492 0.00314 AFIX 137 H01M 2 0.630990 -0.027388 0.578531 11.00000 -1.50000 H01N 2 0.694400 -0.019773 0.616757 11.00000 -1.50000 H01O 2 0.674539 0.078481 0.591517 11.00000 -1.50000 AFIX 0 C01F 1 0.465393 0.070660 0.561284 11.00000 0.07773 0.04061 = 0.06089 -0.01207 -0.00600 -0.01392 AFIX 43 H01P 2 0.483519 0.007489 0.552723 11.00000 -1.20000 AFIX 0 C01G 1 0.988625 0.182347 0.759530 11.00000 0.05574 0.09523 = 0.03906 -0.00222 -0.01194 0.02592 AFIX 43 H01Q 2 1.012103 0.190498 0.784714 11.00000 -1.20000 AFIX 0 C01H 1 0.612126 0.311243 0.532456 11.00000 0.06350 0.06740 = 0.06849 -0.02317 0.01895 -0.01216 AFIX 137 H01R 2 0.596063 0.360509 0.512699 11.00000 -1.50000 H01S 2 0.644842 0.345217 0.553768 11.00000 -1.50000 H01T 2 0.559571 0.281077 0.539734 11.00000 -1.50000 AFIX 0 C01I 1 1.002165 0.274530 0.548094 11.00000 0.04809 0.08933 = 0.05747 0.01873 0.01599 0.00823 AFIX 13 H01U 2 0.989716 0.237048 0.570526 11.00000 -1.20000 AFIX 0 C01J 1 0.806981 0.642518 0.637228 11.00000 0.09029 0.08287 = 0.04919 0.01569 0.00459 -0.00860 C01K 1 0.847061 0.414735 0.711168 11.00000 0.06574 0.06740 = 0.08057 -0.00048 0.01311 0.02260 AFIX 137 H01V 2 0.886112 0.473007 0.714796 11.00000 -1.50000 H01W 2 0.815845 0.415902 0.686011 11.00000 -1.50000 H01X 2 0.880887 0.352268 0.714942 11.00000 -1.50000 AFIX 0 C01L 1 0.852878 0.039154 0.522809 11.00000 0.12580 0.06034 = 0.05566 -0.01299 0.01814 0.02659 AFIX 137 H01Y 2 0.896304 0.070707 0.509481 11.00000 -1.50000 H 2 0.794981 0.049913 0.509112 11.00000 -1.50000 HA 2 0.864398 -0.033489 0.525254 11.00000 -1.50000 AFIX 0 C01M 1 0.421112 0.568970 0.697874 11.00000 0.03884 0.09458 = 0.11759 0.00910 0.01583 0.00140 AFIX 137 H01Z 2 0.428781 0.508032 0.713190 11.00000 -1.50000 HB 2 0.365135 0.565886 0.681984 11.00000 -1.50000 HC 2 0.422681 0.628693 0.713785 11.00000 -1.50000 AFIX 0 PART 1 C01N 1 0.699103 0.516063 0.608248 21.00000 0.03225 PART 0 C01O 1 0.477032 0.662191 0.644996 11.00000 0.07433 0.07743 = 0.08616 0.01191 0.00061 0.01940 AFIX 137 H01 2 0.468811 0.725499 0.657965 11.00000 -1.50000 HD 2 0.424363 0.646526 0.628052 11.00000 -1.50000 HE 2 0.525969 0.669354 0.630980 11.00000 -1.50000 AFIX 0 C01P 1 0.616075 0.172577 0.485875 11.00000 0.07616 0.07870 = 0.09171 -0.04659 0.01189 -0.01589 AFIX 137 H1 2 0.561590 0.147764 0.493125 11.00000 -1.50000 HF 2 0.650017 0.115396 0.478662 11.00000 -1.50000 HG 2 0.603461 0.219111 0.464989 11.00000 -1.50000 AFIX 0 C01Q 1 0.828743 0.420574 0.779367 11.00000 0.11770 0.08932 = 0.05923 0.00005 -0.01917 0.02221 AFIX 137 H2 2 0.863210 0.358820 0.784037 11.00000 -1.50000 HH 2 0.785733 0.424001 0.796524 11.00000 -1.50000 HI 2 0.866963 0.479587 0.782962 11.00000 -1.50000 AFIX 0 C01R 1 1.047483 0.373529 0.561283 11.00000 0.05331 0.12505 = 0.10327 0.01014 -0.00398 -0.01551 AFIX 137 H3 2 1.070276 0.406165 0.540574 11.00000 -1.50000 HJ 2 1.095297 0.359009 0.580918 11.00000 -1.50000 HK 2 1.005818 0.418638 0.570779 11.00000 -1.50000 AFIX 0 C01S 1 0.411761 0.450368 0.569665 11.00000 0.12996 0.05290 = 0.08207 0.00008 0.00983 0.00562 AFIX 137 H4 2 0.378979 0.438676 0.545191 11.00000 -1.50000 HL 2 0.473979 0.447001 0.568056 11.00000 -1.50000 HM 2 0.397446 0.517256 0.578596 11.00000 -1.50000 AFIX 0 C01T 1 0.738519 0.581988 0.532089 11.00000 0.08125 0.09743 = 0.10655 0.00782 0.03242 -0.02700 AFIX 43 H5 2 0.712219 0.523521 0.520405 11.00000 -1.20000 AFIX 0 C01U 1 0.532210 -0.061224 0.632257 11.00000 0.10492 0.06833 = 0.12687 0.04220 0.02311 0.00556 AFIX 137 H6 2 0.483640 -0.046263 0.645808 11.00000 -1.50000 HN 2 0.576606 -0.099214 0.648203 11.00000 -1.50000 HO 2 0.511486 -0.101557 0.610347 11.00000 -1.50000 AFIX 0 C01V 1 0.784095 -0.046221 0.720108 11.00000 0.09878 0.06291 = 0.13553 0.03901 0.02587 -0.00190 AFIX 137 H7 2 0.801005 -0.043841 0.746909 11.00000 -1.50000 HP 2 0.824594 -0.089437 0.709011 11.00000 -1.50000 HQ 2 0.725346 -0.073767 0.714579 11.00000 -1.50000 AFIX 0 C01W 1 1.114612 0.172421 0.651158 11.00000 0.08038 0.09405 = 0.08181 0.01947 0.03480 0.02346 AFIX 137 H8 2 1.145389 0.202969 0.632295 11.00000 -1.50000 HR 2 1.081877 0.113488 0.640738 11.00000 -1.50000 HS 2 1.156570 0.151265 0.672215 11.00000 -1.50000 AFIX 0 PART 1 C01X 1 0.864236 0.482770 0.603998 21.00000 0.04714 AFIX 43 H9 2 0.921324 0.505620 0.602297 21.00000 -1.20000 AFIX 0 PART 0 C01Y 1 1.063105 0.207401 0.528339 11.00000 0.08385 0.15586 = 0.13580 -0.01372 0.01216 0.05537 AFIX 137 H10 2 1.034335 0.143073 0.521305 11.00000 -1.50000 HT 2 1.116774 0.194584 0.545040 11.00000 -1.50000 HU 2 1.076746 0.242094 0.506180 11.00000 -1.50000 AFIX 0 C01Z 1 1.100278 0.348843 0.674905 11.00000 0.09585 0.10253 = 0.10374 -0.01867 0.02982 -0.04550 AFIX 137 H11 2 1.147854 0.335931 0.694816 11.00000 -1.50000 HV 2 1.059704 0.397252 0.683393 11.00000 -1.50000 HW 2 1.123658 0.376745 0.653502 11.00000 -1.50000 AFIX 0 C020 1 0.762108 0.739701 0.566767 11.00000 0.12257 0.06732 = 0.14280 0.02909 0.07546 0.00570 AFIX 43 H020 2 0.753481 0.799082 0.580355 11.00000 -1.20000 AFIX 0 C021 1 0.693581 0.671051 0.547029 11.00000 0.08337 0.15733 = 0.08381 0.06746 0.01021 0.01017 C022 1 0.839282 0.698030 0.560879 11.00000 0.12332 0.09557 = 0.15736 0.03823 0.05336 -0.04020 AFIX 43 H022 2 0.895030 0.724747 0.569361 11.00000 -1.20000 AFIX 0 C023 1 0.821176 0.602505 0.538660 11.00000 0.20020 0.11004 = 0.11494 0.05111 0.11498 0.05595 AFIX 43 H023 2 0.864932 0.561916 0.530393 11.00000 -1.20000 AFIX 0 C024 1 0.289778 0.374179 0.599610 11.00000 0.08603 0.09338 = 0.34352 -0.00103 0.10775 0.02449 AFIX 137 H02A 2 0.256614 0.356257 0.575758 11.00000 -1.50000 H02B 2 0.274846 0.443035 0.606301 11.00000 -1.50000 H02C 2 0.275748 0.326931 0.618548 11.00000 -1.50000 AFIX 0 HX 2 0.719021 0.261511 0.635598 11.00000 0.04202 PART 2 C1 1 0.666979 0.534547 0.604166 -21.00000 0.04617 0.06785 = 0.06144 0.00849 0.01599 -0.00102 AFIX 43 H1A 2 0.621313 0.579553 0.595380 -21.00000 -1.20000 AFIX 0 C2 1 0.823459 0.473238 0.602257 -21.00000 0.04206 0.05772 = 0.05790 -0.01414 0.00675 -0.00870 PART 0 C5 1 0.598162 0.694144 0.544024 11.00000 0.08915 0.32229 = 0.23484 0.13580 0.01078 0.01346 AFIX 137 H5A 2 0.566457 0.632405 0.548475 11.00000 -1.50000 H5B 2 0.577478 0.719780 0.519241 11.00000 -1.50000 H5C 2 0.588484 0.745268 0.562400 11.00000 -1.50000 AFIX 0 HKLF 4 REM mrc2122_a.res in P2(1)/c REM wR2 = 0.2545, GooF = S = 1.028, Restrained GooF = 1.028 for all data REM R1 = 0.0822 for 8681 Fo > 4sig(Fo) and 0.1240 for all 14105 data REM 728 parameters refined using 0 restraints END WGHT 0.1264 5.1904 REM Highest difference peak 1.056, deepest hole -0.418, 1-sigma level 0.074 Q1 1 0.7462 0.7394 0.6191 11.00000 0.05 1.06 Q2 1 0.8784 0.7180 0.6014 11.00000 0.05 0.96 Q3 1 0.8854 0.6776 0.6353 11.00000 0.05 0.80 Q4 1 0.7579 0.5338 0.5182 11.00000 0.05 0.64 Q5 1 0.7697 0.5520 0.5584 11.00000 0.05 0.62 Q6 1 0.7473 0.8001 0.5457 11.00000 0.05 0.62 Q7 1 0.7926 0.7540 0.5991 11.00000 0.05 0.36 Q8 1 0.3421 0.4373 0.5602 11.00000 0.05 0.29 Q9 1 0.7539 0.4608 0.7377 11.00000 0.05 0.26 Q10 1 0.6959 0.5818 0.5407 11.00000 0.05 0.25 ; _shelx_res_checksum 46338 _shelx_hkl_file ; 0 0 -4 -0.46 0.50 0 0 5 223.99 7.05 0 0 -5 0.41 0.82 0 0 6 2634.40 26.62 0 0 -6 19.43 3.24 0 0 7 63.61 7.44 0 0 -7 62.41 7.04 0 0 -8 1691.83 24.26 0 0 8 1803.30 25.66 0 0 9 20.18 4.70 0 0 -9 54.02 7.15 0 0 -10 159.96 8.50 0 0 10 181.68 9.01 0 0 -11 34.17 9.16 0 0 11 8.29 4.71 0 0 12 1657.16 29.92 0 0 -12 1595.92 29.02 0 0 13 50.53 7.30 0 0 -13 143.74 11.02 0 0 -14 146.87 9.76 0 0 14 162.97 10.34 0 0 -15 190.33 13.65 0 0 15 34.93 7.12 0 0 16 2134.54 40.05 0 0 -16 1908.55 36.33 0 0 -17 74.38 10.21 0 0 17 34.98 7.28 0 0 -18 17.08 3.81 0 0 18 18.67 4.62 0 0 19 3.34 3.11 0 0 -19 1.34 5.05 0 0 20 377.06 18.93 0 0 -20 360.47 18.07 0 0 -21 25.29 6.97 0 0 -22 91.70 10.07 0 0 -23 12.56 5.72 0 0 -24 199.98 15.13 0 0 -25 16.67 6.31 0 0 -26 170.40 14.37 0 0 -27 3.84 3.14 0 0 -28 -8.85 5.94 0 0 -29 -4.12 4.33 0 0 -30 13.05 4.62 0 0 -31 -1.09 3.87 0 0 -32 3.92 4.15 0 0 -33 18.65 9.26 0 0 -34 435.59 27.11 0 0 -35 29.72 8.95 0 0 -36 7.28 5.45 0 0 -37 20.47 8.57 0 0 -38 163.04 18.04 0 0 -39 9.62 6.38 0 0 -40 18.80 8.03 0 0 -41 15.92 7.66 0 0 -42 73.87 13.74 0 0 -43 -1.25 4.59 0 0 -44 -2.87 5.07 0 -1 4 125.02 5.06 0 1 4 122.75 4.82 0 -1 5 35.68 3.22 0 1 -5 36.16 3.16 0 1 5 41.53 3.17 0 1 6 1312.97 18.59 0 1 -6 1327.02 19.21 0 -1 -7 276.08 8.96 0 1 -7 259.93 9.72 0 -1 7 247.20 9.09 0 1 7 267.29 9.16 0 -1 -8 481.60 12.52 0 1 8 460.84 12.75 0 1 -8 487.96 13.98 0 -1 8 480.35 13.68 0 1 -9 232.98 10.53 0 -1 9 239.49 10.27 0 1 9 229.61 9.39 0 -1 -9 239.86 9.48 0 1 10 -1.71 1.91 0 -1 10 -1.00 2.62 0 1 -10 -6.65 2.53 0 1 -11 144.16 9.09 0 -1 11 133.81 8.64 0 -1 -11 148.63 8.69 0 1 11 144.44 8.29 0 -1 -12 197.21 10.69 0 -1 12 171.79 10.42 0 1 -12 162.77 10.56 0 1 12 178.60 9.72 0 1 -13 388.83 15.88 0 -1 13 411.76 15.98 0 -1 -13 413.54 15.13 0 1 13 405.14 15.35 0 -1 14 186.89 11.77 0 1 -14 165.66 11.54 0 1 14 173.27 10.67 0 1 -15 465.93 18.57 0 -1 15 506.17 18.99 0 -1 -15 501.83 18.06 0 1 15 489.18 18.43 0 1 -16 6.00 3.50 0 -1 16 8.35 4.30 0 1 16 6.61 3.23 0 -1 17 57.41 6.84 0 1 17 65.36 7.57 0 -1 -17 59.91 6.96 0 1 -17 56.61 6.86 0 -1 18 24.90 4.88 0 -1 -18 35.80 5.80 0 1 18 26.83 4.95 0 1 -18 23.28 4.49 0 1 -19 1.38 5.50 0 -1 19 4.64 3.63 0 1 19 4.18 3.36 0 1 -20 348.54 18.27 0 -1 -20 362.62 18.32 0 1 21 216.08 14.57 0 -1 -21 193.93 13.92 0 1 -21 183.11 13.84 0 1 -22 3.42 3.82 0 -1 -22 15.87 5.15 0 1 -23 28.37 6.40 0 -1 -23 38.32 6.95 0 1 -24 125.06 12.11 0 -1 -24 121.92 11.88 0 -1 -25 69.95 10.57 0 1 -25 93.88 11.86 0 -1 -26 350.24 20.47 0 1 -26 365.47 21.42 0 1 -27 43.68 9.41 0 -1 -27 61.28 10.20 0 1 -28 176.13 16.42 0 -1 -28 203.34 16.42 0 -1 -29 28.85 7.78 0 1 -29 29.00 8.02 0 -1 -30 46.16 8.83 0 1 -30 42.87 8.12 0 1 -31 -0.37 3.60 0 -1 -31 20.97 7.59 0 -1 -32 96.24 12.73 0 1 -32 83.82 12.04 0 -1 -33 6.87 5.26 0 1 -33 1.17 3.47 0 1 -34 16.46 6.87 0 -1 -34 14.34 6.27 0 -1 -35 34.89 8.42 0 1 -35 42.22 9.81 0 -1 -36 51.64 10.24 0 1 -36 52.01 10.43 0 -1 -37 13.27 5.95 0 1 -37 15.96 7.11 0 -1 -38 -2.58 4.15 0 1 -38 -1.64 5.19 0 1 -39 1.09 3.89 0 -1 -39 -0.62 4.73 0 1 -40 3.20 4.10 0 -1 -40 2.33 3.86 0 -1 -41 10.16 5.99 0 1 -41 6.53 5.49 0 -1 -42 8.54 5.23 0 1 -42 7.96 5.73 0 -1 -43 9.01 6.06 0 1 -43 24.12 9.20 0 -1 -44 6.42 4.77 0 -2 0 2288.42 19.75 0 2 0 2169.75 19.48 0 -2 1 4240.14 27.11 0 2 -1 4327.42 27.09 0 2 1 4341.44 28.20 0 2 -2 1262.18 15.15 0 -2 2 1256.25 15.35 0 -2 3 734.37 12.67 0 2 -3 777.58 12.40 0 -2 4 785.63 13.30 0 2 -4 886.45 14.18 0 -2 5 489.65 11.90 0 2 -5 472.38 11.31 0 -2 6 4382.06 36.88 0 2 -6 4439.16 37.06 0 2 -7 2393.84 29.20 0 -2 7 2458.26 29.53 0 2 7 2473.55 28.83 0 -2 8 7.40 2.32 0 2 8 9.76 3.18 0 2 -8 5.53 2.33 0 2 -9 238.53 10.75 0 -2 -9 230.39 10.22 0 2 9 235.50 9.89 0 -2 9 241.17 10.76 0 -2 -10 4002.62 42.17 0 2 -10 3910.81 46.43 0 2 10 3878.55 41.51 0 -2 10 3944.54 43.73 0 -2 -11 83.21 7.08 0 -2 11 73.05 7.49 0 2 -11 68.92 7.43 0 2 11 85.42 7.58 0 -2 12 67.43 6.71 0 2 -12 60.84 6.29 0 2 12 64.19 5.96 0 -2 -12 69.71 6.78 0 2 -13 424.81 17.19 0 -2 -13 418.20 15.36 0 -2 13 446.12 16.66 0 -2 -14 -0.78 2.19 0 2 -14 -0.45 2.63 0 2 14 -0.32 1.89 0 -2 14 5.70 3.48 0 -2 -15 1.75 2.10 0 -2 15 3.56 2.49 0 2 -15 -3.03 3.19 0 2 15 0.32 2.09 0 -2 -16 53.93 6.15 0 2 -16 49.77 6.64 0 -2 16 54.10 6.55 0 2 16 52.33 6.03 0 2 17 2.67 2.05 0 2 -17 2.97 2.79 0 -2 -17 6.94 3.53 0 -2 17 6.36 3.04 0 2 18 29.65 5.60 0 2 -18 17.99 5.05 0 -2 18 27.34 6.49 0 -2 -19 603.02 21.91 0 2 19 578.85 22.71 0 -2 19 648.65 24.53 0 2 -19 585.00 24.45 0 2 20 40.38 6.63 0 2 -20 48.42 7.77 0 -2 -21 17.64 4.50 0 2 -21 14.83 4.97 0 2 21 11.52 3.93 0 2 -22 46.66 7.76 0 -2 -22 45.62 6.91 0 -2 -23 66.24 8.55 0 2 -23 67.12 9.30 0 -2 -24 64.20 9.85 0 2 -24 40.24 8.64 0 2 -25 346.90 20.91 0 -2 -25 362.75 19.95 0 2 -26 117.37 13.82 0 -2 -26 133.73 13.38 0 2 -27 167.76 15.53 0 -2 -27 184.79 15.00 0 -2 -28 70.34 10.82 0 2 -28 85.15 12.05 0 -2 -29 193.64 16.71 0 2 -29 194.20 17.12 0 2 -30 116.74 13.35 0 -2 -30 125.57 13.69 0 -2 -31 17.15 7.46 0 2 -31 3.38 5.39 0 2 -32 64.09 11.14 0 -2 -32 88.27 11.93 0 -2 -33 41.50 9.72 0 2 -33 28.10 7.34 0 2 -34 25.77 7.37 0 -2 -34 23.39 6.13 0 -2 -35 24.05 6.72 0 2 -35 31.87 8.78 0 2 -36 21.41 7.70 0 -2 -36 24.79 8.17 0 -2 -37 19.35 7.03 0 2 -37 12.34 6.41 0 2 -38 6.44 5.40 0 -2 -38 5.59 4.51 0 -2 -39 2.50 4.29 0 2 -39 -2.11 5.04 0 2 -40 0.29 5.38 0 -2 -40 11.66 6.40 0 2 -41 15.28 6.18 0 -2 -41 16.55 7.09 0 -2 -42 3.82 5.04 0 2 -42 14.45 7.92 0 -2 -43 -6.62 6.06 0 2 -43 -2.29 4.66 0 -2 -44 8.73 5.13 0 -3 0 -1.76 1.69 0 3 0 -1.58 1.59 0 3 -1 2677.30 26.61 0 -3 -1 2730.05 27.04 0 -3 1 2627.17 25.97 0 3 1 2695.56 26.87 0 -3 2 1154.96 17.85 0 3 2 1161.21 18.90 0 3 -2 1160.68 17.41 0 -3 3 5.44 1.89 0 3 3 0.24 2.13 0 3 -3 4.16 1.62 0 -3 4 0.58 1.27 0 3 -4 -0.49 1.50 0 3 -5 23.68 2.99 0 -3 5 27.39 3.24 0 3 -6 172.52 7.82 0 -3 6 173.01 7.95 0 -3 7 537.00 14.68 0 3 -7 545.72 15.11 0 -3 8 800.05 19.44 0 3 -8 741.98 18.07 0 3 -9 7.92 3.08 0 -3 9 7.88 2.54 0 3 10 468.84 15.08 0 3 -10 480.36 15.64 0 -3 10 484.45 15.72 0 3 -11 457.05 16.20 0 -3 11 516.38 17.08 0 3 11 496.79 16.07 0 3 -12 941.62 23.59 0 -3 12 931.61 23.58 0 3 12 924.00 22.37 0 3 -13 324.38 16.15 0 3 13 323.53 14.03 0 3 -13 304.61 14.89 0 -3 13 335.77 15.24 0 -3 14 2171.61 39.28 0 3 -14 2089.43 40.80 0 3 14 2034.79 36.19 0 -3 15 19.19 7.52 0 3 15 22.08 5.62 0 3 -15 20.42 8.57 0 3 -16 6.40 4.32 0 -3 -16 16.48 5.27 0 -3 16 10.91 5.30 0 3 16 3.74 2.16 0 3 17 633.96 22.46 0 -3 -17 646.65 22.10 0 3 -17 620.80 24.46 0 -3 17 664.56 24.29 0 3 18 198.58 13.21 0 -3 -18 233.87 14.17 0 3 -18 214.93 15.05 0 -3 18 221.08 14.85 0 3 -19 28.36 8.22 0 -3 19 28.52 6.76 0 -3 -19 46.74 9.42 0 3 19 21.79 5.00 0 3 20 595.84 23.21 0 -3 -20 584.90 23.11 0 3 -20 550.70 24.38 0 3 21 124.54 11.70 0 3 -21 132.51 13.53 0 -3 -21 137.19 12.02 0 -3 -22 6.30 4.00 0 3 -22 0.72 3.87 0 3 -23 4.02 3.62 0 -3 -23 8.65 4.18 0 -3 -24 27.24 5.98 0 3 -24 24.86 6.35 0 3 -25 1.29 3.53 0 -3 -25 8.98 4.66 0 3 -26 33.11 7.86 0 -3 -26 37.12 7.31 0 3 -27 44.13 9.26 0 -3 -27 50.85 8.71 0 -3 -28 9.80 5.41 0 3 -28 14.59 6.26 0 -3 -29 1.88 3.86 0 3 -29 10.37 5.67 0 3 -30 0.89 3.61 0 -3 -30 4.19 4.95 0 3 -31 6.80 5.07 0 -3 -31 2.82 4.87 0 -3 -32 14.96 6.44 0 3 -32 6.56 5.31 0 -3 -33 26.63 6.83 0 3 -33 21.55 7.22 0 -3 -34 15.54 5.60 0 3 -34 10.09 5.67 0 -3 -35 13.16 6.42 0 3 -35 2.21 5.13 0 -3 -36 34.16 8.40 0 3 -36 33.36 9.82 0 3 -37 7.51 5.26 0 -3 -37 0.39 4.15 0 -3 -38 31.51 8.62 0 3 -38 14.60 6.36 0 3 -39 5.41 4.96 0 -3 -39 2.71 4.61 0 -3 -40 3.76 4.65 0 3 -40 -2.68 4.23 0 3 -41 33.43 9.23 0 -3 -41 30.31 8.75 0 3 -42 -2.87 5.32 0 -3 -42 1.50 4.32 0 -3 -43 -2.05 4.45 0 4 0 993.07 18.60 0 -4 0 988.71 19.32 0 4 -1 1458.66 23.50 0 4 1 1415.42 22.60 0 -4 1 1425.16 22.24 0 4 -2 1013.56 18.87 0 -4 2 1001.74 18.79 0 4 2 1026.79 19.64 0 4 3 1176.97 21.79 0 -4 3 1195.34 21.12 0 4 -3 1140.79 20.04 0 -4 4 318.55 11.03 0 4 -4 323.63 11.19 0 4 4 314.20 11.66 0 4 -5 47.49 4.42 0 -4 5 46.46 4.37 0 -4 6 38.00 4.26 0 4 -6 39.22 4.15 0 -4 7 10.16 2.74 0 4 -7 12.31 2.75 0 4 -8 26.19 3.89 0 -4 8 23.70 4.25 0 4 -9 460.57 15.82 0 -4 9 463.60 15.37 0 -4 10 91.57 7.57 0 4 -10 96.20 7.79 0 4 11 628.94 19.44 0 -4 11 629.52 19.91 0 4 -11 595.11 18.92 0 4 12 238.28 12.11 0 4 -12 217.48 12.18 0 -4 12 233.53 12.82 0 4 -13 725.23 22.27 0 4 13 706.98 21.61 0 -4 14 8.11 3.30 0 4 14 16.10 4.22 0 4 -14 11.11 3.90 0 4 -15 401.04 17.92 0 4 -15 409.82 19.31 0 4 15 389.40 16.84 0 -4 15 380.70 16.92 0 4 -16 102.75 10.29 0 -4 16 104.75 9.31 0 4 16 106.51 9.16 0 4 -17 4.09 4.21 0 4 17 2.20 2.66 0 -4 17 0.36 2.58 0 4 -18 349.16 19.73 0 4 18 379.26 18.16 0 -4 18 383.20 19.04 0 4 19 587.19 23.12 0 -4 19 607.60 24.76 0 4 -19 586.20 25.71 0 4 20 503.19 22.16 0 4 -20 510.51 24.81 0 4 -21 52.21 9.25 0 4 -22 262.78 18.56 0 4 -23 88.48 11.01 0 4 -24 10.41 5.69 0 4 -25 139.93 14.52 0 4 -26 151.90 15.94 0 4 -27 23.38 7.85 0 4 -28 62.80 11.14 0 4 -29 45.34 9.84 0 4 -30 23.31 7.94 0 4 -31 79.53 13.02 0 4 -32 117.37 14.86 0 4 -33 2.72 3.96 0 4 -34 0.74 4.57 0 4 -35 61.48 11.78 0 4 -36 -0.65 5.03 0 4 -37 3.49 5.09 0 4 -38 21.32 7.81 0 4 -39 18.80 8.70 0 4 -40 -1.32 5.10 0 4 -41 -1.97 4.49 0 5 0 -3.38 2.19 0 -5 0 -3.08 1.64 0 5 1 588.79 16.60 0 -5 1 608.43 16.35 0 -5 -1 628.20 16.77 0 5 -1 597.50 16.28 0 5 -2 35.66 3.95 0 5 2 36.38 4.25 0 -5 2 30.11 3.63 0 5 -3 7.41 2.11 0 -5 3 11.29 2.83 0 5 3 9.15 2.69 0 5 -4 949.12 20.86 0 5 4 980.80 22.07 0 5 5 824.16 20.84 0 -5 5 773.28 20.03 0 5 -5 796.66 19.62 0 5 -6 0.94 1.64 0 -5 6 0.29 1.64 0 -5 7 33.88 4.52 0 5 -7 31.61 4.34 0 5 -8 194.59 10.64 0 -5 8 209.77 10.86 0 5 -9 8.07 3.90 0 -5 9 35.40 5.93 0 5 -10 1716.99 32.80 0 -5 10 1744.58 32.77 0 -5 11 2156.29 37.73 0 5 -11 2274.53 38.54 0 -5 12 206.83 12.11 0 5 12 230.75 13.23 0 5 -12 211.08 12.41 0 5 13 523.56 19.19 0 5 -13 517.74 19.53 0 -5 13 492.67 18.53 0 -5 14 161.99 11.30 0 5 14 167.75 11.36 0 5 -14 153.68 11.06 0 5 15 200.11 12.63 0 -5 15 200.11 12.98 0 5 -15 199.74 12.95 0 5 -16 11.08 3.29 0 -5 16 11.71 4.09 0 5 16 6.04 2.61 0 5 -17 20.20 6.08 0 -5 17 21.80 5.74 0 5 17 19.38 4.75 0 5 -18 615.08 26.65 0 5 18 633.46 23.46 0 -5 18 633.75 25.48 0 5 -19 110.37 12.17 0 5 19 103.55 10.28 0 5 -20 188.52 15.55 0 5 -21 145.49 14.21 0 5 -22 39.06 7.95 0 5 -23 4.55 4.55 0 5 -24 125.53 13.55 0 5 -25 18.14 7.23 0 5 -26 273.18 21.42 0 5 -27 63.67 11.93 0 5 -28 7.70 4.14 0 5 -29 17.38 7.14 0 5 -30 66.36 12.10 0 5 -31 118.59 15.49 0 5 -32 6.25 5.42 0 5 -33 -5.60 6.09 0 5 -34 23.26 6.11 0 5 -35 8.69 5.89 0 5 -36 12.74 5.07 0 5 -37 4.17 5.62 0 5 -38 18.31 7.80 0 5 -39 34.73 9.58 0 5 -40 6.34 5.93 0 -6 0 1732.47 31.03 0 6 0 1700.78 30.35 0 -6 -1 201.26 11.15 0 -6 1 212.03 10.87 0 6 1 194.89 10.22 0 6 -1 178.40 10.03 0 6 -2 78.52 6.38 0 -6 2 88.19 6.81 0 6 2 75.29 6.31 0 6 3 40.97 5.05 0 6 -3 46.82 5.05 0 -6 3 40.92 4.61 0 6 -4 51.55 5.53 0 -6 4 53.08 5.49 0 6 4 43.22 5.52 0 -6 5 3.99 4.45 0 6 -5 6.12 3.22 0 6 5 6.39 2.62 0 6 -6 1047.36 23.93 0 -6 6 1082.80 25.09 0 6 6 1132.88 26.81 0 6 -7 61.73 6.41 0 -6 7 61.18 6.38 0 6 7 71.51 7.90 0 6 -8 111.71 8.20 0 6 8 107.04 9.25 0 -6 8 120.32 8.80 0 6 -9 439.04 16.68 0 -6 9 494.55 18.37 0 6 -10 866.52 24.54 0 -6 10 923.94 25.14 0 6 -11 4.46 2.52 0 -6 11 3.40 2.06 0 -6 12 15.43 3.48 0 6 -12 19.05 4.13 0 -6 13 2.54 2.55 0 6 -13 3.79 3.07 0 6 14 213.19 13.17 0 6 -14 226.05 13.74 0 -6 14 209.06 13.59 0 6 15 226.39 13.92 0 6 -15 210.15 13.88 0 -6 15 228.35 14.52 0 -6 16 11.34 3.89 0 6 -16 9.60 3.50 0 6 16 12.35 3.80 0 6 17 -0.65 2.28 0 6 -17 0.01 2.65 0 -6 17 0.11 2.05 0 6 -18 19.41 4.95 0 6 18 19.16 4.68 0 6 -19 154.45 14.14 0 6 -19 146.57 12.72 0 6 -20 11.91 5.44 0 6 -21 77.71 10.71 0 6 -22 -1.67 2.94 0 6 -23 26.51 8.17 0 6 -24 196.49 17.92 0 6 -25 23.21 7.64 0 6 -26 16.94 5.14 0 6 -27 23.07 7.93 0 6 -28 124.83 15.70 0 6 -29 132.89 16.62 0 6 -30 23.70 8.57 0 6 -31 20.35 7.43 0 6 -32 23.57 7.54 0 6 -33 48.64 11.01 0 6 -34 48.83 11.12 0 6 -35 10.43 6.30 0 6 -36 10.88 6.11 0 6 -37 14.74 8.37 0 6 -38 49.28 11.66 0 6 -39 5.78 6.41 0 -7 0 -1.03 1.89 0 7 0 1.76 2.00 0 -7 1 1.43 1.89 0 7 -1 -0.50 2.16 0 7 1 3.66 2.40 0 7 2 37.41 5.30 0 7 -2 45.22 5.50 0 -7 2 42.51 5.43 0 -7 3 65.76 6.73 0 7 3 57.04 6.69 0 7 -3 51.23 6.20 0 7 4 342.93 15.43 0 -7 4 366.58 15.63 0 7 -4 359.25 15.09 0 7 5 35.03 5.84 0 7 -5 31.57 4.73 0 -7 5 38.17 5.92 0 7 -6 245.93 12.77 0 7 6 251.97 13.78 0 -7 6 256.61 13.36 0 7 7 226.41 13.32 0 -7 7 216.88 12.91 0 7 -7 211.98 11.98 0 -7 8 1.65 2.02 0 7 -8 1.95 2.21 0 7 8 6.91 2.95 0 -7 9 12.68 3.91 0 7 -9 4.68 2.55 0 7 9 6.58 2.76 0 -7 10 287.15 15.39 0 7 -10 270.75 14.34 0 7 10 284.91 15.69 0 7 11 613.79 22.99 0 -7 11 611.33 22.11 0 7 -11 572.93 21.26 0 -7 12 36.26 5.72 0 7 -12 41.77 6.26 0 7 -13 4.15 2.92 0 -7 13 1.99 2.10 0 7 -14 13.01 4.30 0 -7 14 13.06 3.81 0 7 -15 130.12 11.26 0 7 15 144.56 11.80 0 -7 15 144.93 11.85 0 7 -16 30.52 5.89 0 7 16 33.41 6.02 0 -7 16 28.78 5.88 0 7 -17 128.50 11.35 0 7 -18 -0.96 2.68 0 7 -19 36.92 7.36 0 7 -20 241.93 16.91 0 7 -21 130.71 14.34 0 7 -22 -0.53 4.55 0 7 -23 74.14 11.45 0 7 -24 7.39 4.88 0 7 -25 10.83 5.60 0 7 -26 32.80 8.54 0 7 -27 55.83 10.82 0 7 -28 48.79 10.24 0 7 -29 8.48 7.07 0 7 -30 67.90 12.14 0 7 -31 17.89 7.08 0 7 -32 4.91 6.19 0 7 -33 51.83 12.12 0 7 -34 78.85 13.93 0 7 -35 8.43 6.38 0 7 -36 17.30 7.68 0 7 -37 0.62 4.35 0 8 0 89.72 8.21 0 -8 0 95.48 8.66 0 8 1 247.52 13.74 0 8 -1 245.78 13.18 0 -8 1 237.57 13.59 0 8 2 6.42 2.48 0 -8 2 6.50 3.05 0 8 -2 13.59 3.74 0 8 -3 389.58 17.14 0 -8 3 390.86 17.05 0 8 3 355.88 16.41 0 -8 4 17.06 3.58 0 8 -4 11.50 3.51 0 8 4 23.22 4.61 0 -8 5 3.86 2.20 0 8 5 4.91 2.35 0 8 -5 3.63 2.00 0 8 -6 29.81 4.70 0 -8 6 44.04 5.96 0 8 6 44.55 6.48 0 8 -7 91.68 8.73 0 -8 7 100.95 9.16 0 8 7 89.93 8.91 0 8 -8 330.54 16.27 0 8 8 339.39 17.36 0 -8 8 343.81 16.42 0 8 9 207.96 14.64 0 8 -9 214.87 13.57 0 -8 9 234.44 14.08 0 8 -10 71.90 7.94 0 -8 10 81.30 8.49 0 8 10 83.59 9.17 0 8 -11 80.45 8.42 0 8 11 76.05 9.18 0 -8 11 87.69 8.90 0 8 12 0.30 3.91 0 -8 12 2.85 1.92 0 8 -12 7.54 3.24 0 8 13 28.38 5.51 0 8 -13 31.24 6.01 0 -8 13 26.26 5.48 0 8 14 107.04 10.47 0 8 -14 102.40 10.28 0 -8 14 107.66 10.17 0 8 -15 50.10 7.26 0 8 -16 31.42 6.21 0 8 -17 156.89 13.32 0 8 -18 20.16 5.23 0 8 -19 70.32 9.27 0 8 -20 -3.38 3.67 0 8 -21 4.07 2.76 0 8 -22 -1.89 4.50 0 8 -23 104.69 13.95 0 8 -24 32.35 9.75 0 8 -25 -2.49 4.56 0 8 -26 14.77 6.52 0 8 -27 10.62 6.07 0 8 -28 62.53 12.17 0 8 -29 18.43 7.43 0 8 -30 5.97 5.20 0 8 -31 16.17 7.48 0 8 -32 14.30 7.46 0 8 -33 3.34 4.73 0 8 -34 8.62 6.90 0 8 -35 38.84 9.94 0 8 -36 12.79 6.94 0 -9 0 -0.45 2.29 0 9 0 -3.47 2.25 0 9 1 18.81 5.55 0 -9 1 31.59 7.80 0 9 -2 1632.80 35.80 0 -9 2 1682.50 37.45 0 9 2 1625.11 37.73 0 -9 3 38.97 6.70 0 9 -3 34.35 6.90 0 9 4 -1.52 3.59 0 9 -4 -1.46 3.03 0 -9 4 -0.55 3.17 0 -9 5 6.75 2.53 0 9 -5 3.08 2.67 0 9 5 3.94 3.00 0 9 6 189.20 13.29 0 9 -6 194.08 12.62 0 -9 6 195.39 13.03 0 -9 7 59.62 7.25 0 9 -7 53.95 6.96 0 9 7 68.02 8.10 0 9 8 209.01 14.40 0 9 -8 217.03 14.11 0 -9 8 227.78 14.48 0 9 9 109.07 11.26 0 9 -9 106.31 10.10 0 -9 9 109.67 10.05 0 9 10 30.73 6.23 0 9 -10 31.78 5.54 0 -9 10 31.31 5.69 0 -9 11 60.59 8.73 0 9 -11 53.55 7.58 0 9 11 58.44 8.17 0 -9 12 212.06 14.79 0 9 -12 202.39 13.99 0 9 12 194.51 15.59 0 9 13 62.28 9.64 0 9 -13 61.20 8.17 0 9 -14 141.49 12.55 0 9 14 155.83 14.01 0 9 15 36.93 7.81 0 9 -15 35.71 7.11 0 9 16 18.02 6.04 0 9 -16 22.73 5.60 0 9 -17 -1.55 2.56 0 9 17 3.74 4.82 0 9 -18 135.12 12.60 0 9 -19 -2.08 2.72 0 9 -20 43.67 7.76 0 9 -21 23.05 6.16 0 9 -22 33.55 7.02 0 9 -23 -6.11 4.41 0 9 -24 88.41 13.31 0 9 -25 10.59 6.56 0 9 -26 14.71 5.46 0 9 -27 12.74 5.45 0 9 -28 -6.38 5.80 0 9 -29 -2.18 4.73 0 9 -30 20.88 7.78 0 9 -31 65.06 12.91 0 9 -32 56.41 12.15 0 9 -33 -0.26 5.92 0 9 -34 8.80 6.37 0 10 0 12.01 3.24 0 10 -1 -3.81 4.08 0 10 1 0.72 2.59 0 -10 1 -3.88 4.45 0 -10 2 -2.60 2.63 0 10 2 0.80 2.46 0 10 -2 -1.74 2.92 0 10 -3 107.93 10.29 0 10 3 117.03 10.99 0 -10 3 113.06 10.76 0 -10 4 211.52 14.54 0 10 -4 182.56 12.96 0 10 4 185.80 14.03 0 -10 5 37.13 7.83 0 10 -5 31.50 6.83 0 10 5 39.50 7.60 0 10 6 580.84 24.13 0 10 -6 564.04 22.53 0 -10 6 580.12 24.07 0 -10 7 17.21 5.60 0 10 -7 17.33 5.46 0 -10 8 135.77 12.08 0 10 -8 149.61 12.64 0 10 8 130.45 12.38 0 -10 9 410.51 20.19 0 10 -9 400.67 20.42 0 10 9 373.84 20.78 0 10 -10 218.87 15.15 0 10 10 196.44 15.29 0 10 -11 1.65 2.38 0 10 11 4.16 5.19 0 10 12 15.60 4.71 0 10 -12 12.64 3.33 0 10 -13 30.46 6.20 0 10 13 32.10 6.88 0 10 -14 142.86 12.97 0 10 14 144.81 14.01 0 10 15 10.54 5.13 0 10 -15 3.41 3.96 0 10 16 53.18 8.87 0 10 -16 58.33 8.35 0 10 17 5.75 4.53 0 10 -17 -1.93 3.72 0 10 18 -1.99 4.04 0 10 -18 0.05 3.31 0 10 -19 1.53 3.43 0 10 19 5.05 4.20 0 10 -20 128.33 13.50 0 10 20 145.35 15.02 0 10 21 13.56 6.09 0 10 -21 16.62 6.25 0 10 22 7.76 3.67 0 10 -22 13.81 5.05 0 10 -23 1.20 3.72 0 10 -23 -1.31 4.65 0 10 -24 -1.39 4.06 0 10 -25 45.19 10.56 0 10 -26 46.74 10.52 0 10 -27 4.48 4.76 0 10 -28 29.76 9.39 0 10 -29 68.56 13.49 0 10 -30 146.91 19.36 0 10 -31 8.31 7.43 0 10 -32 3.40 5.33 0 11 0 8.08 4.04 0 11 1 138.96 12.32 0 11 -1 150.22 12.22 0 11 -2 15.27 5.21 0 11 2 14.18 4.88 0 11 -3 343.08 18.52 0 11 3 345.03 19.94 0 11 4 84.54 10.78 0 11 -4 70.45 8.63 0 11 5 30.44 6.30 0 11 -5 23.95 5.16 0 11 -6 -5.79 4.39 0 11 6 -0.44 2.62 0 11 7 -1.14 3.43 0 11 -7 0.60 2.54 0 11 -8 106.86 10.93 0 11 8 97.94 10.83 0 11 9 43.90 7.73 0 11 -9 49.63 7.89 0 11 10 11.20 4.31 0 11 -10 10.44 4.21 0 11 -11 10.16 6.04 0 11 11 4.62 4.78 0 11 -12 326.33 19.38 0 11 12 313.01 20.48 0 11 -13 9.05 4.83 0 11 13 19.61 7.82 0 11 14 5.07 5.56 0 11 -14 6.48 4.60 0 11 -15 155.41 14.19 0 11 15 152.83 14.94 0 11 -16 8.92 5.68 0 11 16 5.93 5.84 0 11 -17 115.41 12.81 0 11 17 125.60 14.39 0 11 18 16.20 7.04 0 11 -18 8.83 4.39 0 11 19 10.68 3.98 0 11 -19 9.65 3.35 0 11 20 2.85 4.13 0 11 -20 3.13 3.89 0 11 21 73.10 11.14 0 11 -21 68.49 10.21 0 11 22 4.30 4.21 0 11 -22 4.40 3.97 0 11 -23 2.49 4.08 0 11 23 -0.98 3.60 0 11 24 62.01 11.52 0 11 -24 43.93 10.04 0 11 -25 2.88 6.04 0 11 25 8.37 6.76 0 11 -26 32.06 9.19 0 11 26 29.10 8.42 0 11 27 24.53 8.82 0 11 -27 21.74 7.79 0 11 28 19.22 7.36 0 11 -28 22.95 8.66 0 11 -29 0.71 4.47 0 11 -30 2.05 4.39 0 12 0 263.05 17.21 0 12 1 18.86 5.55 0 12 -1 10.39 3.73 0 12 2 8.31 3.92 0 12 -2 0.87 2.86 0 12 3 5.21 3.59 0 12 -3 3.33 3.10 0 12 4 73.27 9.99 0 12 -4 68.48 8.88 0 12 5 81.56 10.34 0 12 -5 66.15 8.98 0 12 -6 6.73 3.80 0 12 6 7.00 4.16 0 12 7 102.62 11.84 0 12 -7 87.09 10.26 0 12 -8 7.03 3.32 0 12 8 10.92 4.49 0 12 -9 9.19 3.61 0 12 9 15.83 5.32 0 12 -10 20.09 5.00 0 12 10 20.68 5.96 0 12 -11 -1.47 3.12 0 12 11 0.22 2.69 0 12 12 42.86 8.29 0 12 -12 52.12 8.52 0 12 13 1.21 3.35 0 12 -13 6.74 4.38 0 12 14 18.11 6.52 0 12 -14 10.02 5.17 0 12 15 79.52 11.94 0 12 -15 82.28 11.15 0 12 -16 112.74 13.01 0 12 16 110.59 13.74 0 12 -17 57.32 9.92 0 12 17 72.73 12.05 0 12 -18 17.89 5.70 0 12 18 21.03 7.22 0 12 19 17.71 6.85 0 12 -19 27.94 7.33 0 12 20 59.02 10.74 0 12 -20 53.57 9.47 0 12 -21 -4.08 4.84 0 12 21 4.59 5.84 0 12 -22 0.48 3.25 0 12 22 0.38 3.73 0 12 23 7.64 5.44 0 12 -23 7.61 4.51 0 12 -24 3.88 4.62 0 12 24 -1.65 4.92 0 12 -25 11.09 5.68 0 12 25 6.82 4.18 0 12 26 5.52 4.68 0 12 -26 6.31 5.69 0 12 27 0.18 4.50 0 12 -27 -3.15 5.74 0 12 28 10.17 5.40 0 12 29 7.97 6.50 0 12 30 7.66 5.35 0 12 31 -1.23 4.66 0 12 32 0.16 4.42 0 13 0 1.53 3.49 0 13 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34.14 8.65 -8 8 -13 22.64 7.32 -8 8 -14 65.58 11.39 -8 8 -15 34.77 9.59 -8 8 -16 27.35 8.05 -8 8 -17 19.50 6.85 -8 8 -18 -1.83 4.01 -8 8 -19 15.64 6.62 -8 8 -20 6.47 5.03 -8 8 -21 -3.36 6.21 -8 8 -22 2.42 4.77 -8 8 -23 6.27 5.26 -8 8 -24 -1.48 6.26 -8 8 -25 -7.32 6.63 -8 8 -26 -4.20 5.49 -8 8 -27 14.77 7.32 -8 8 -28 0.62 4.73 -8 8 -29 -12.78 7.10 -8 8 -30 1.28 5.02 8 9 -34 5.81 5.03 8 9 -33 2.52 4.82 8 9 -32 60.88 11.45 8 9 -31 4.75 4.55 -8 9 31 9.32 6.71 8 9 -30 1.10 4.80 -8 9 30 14.54 7.76 8 9 -29 4.79 5.37 -8 9 29 0.06 5.01 8 9 -28 12.89 6.34 -8 9 28 17.95 8.26 8 9 -27 92.84 13.72 -8 9 27 103.43 17.63 -8 9 26 96.81 19.45 8 9 -26 78.26 12.89 -8 9 25 176.05 20.71 8 9 -25 151.84 17.04 8 9 -24 69.52 11.98 -8 9 24 74.66 15.12 -8 9 23 15.67 8.23 8 9 -23 4.90 5.35 8 9 -22 51.13 9.56 -8 9 22 49.69 11.12 8 9 -21 55.12 10.18 -8 9 21 68.58 12.72 -8 9 20 185.57 20.09 8 9 -20 176.58 16.67 -8 9 19 17.51 8.89 8 9 -19 25.25 8.44 -8 9 18 34.10 9.64 8 9 -18 28.66 7.31 -8 9 17 29.76 9.21 8 9 -17 33.55 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9.01 -19 3 2 13.65 7.83 -19 3 1 -1.39 6.06 -19 3 0 13.25 6.91 -19 3 -1 1.53 4.81 -19 3 -2 0.73 5.65 -19 3 -3 -3.21 4.57 -19 4 10 0.51 5.55 -19 4 9 1.75 5.18 -19 4 8 0.78 4.35 -19 4 7 6.89 5.87 -19 4 6 2.67 6.33 -19 4 5 16.45 7.81 -20 2 7 0.74 4.71 -20 2 6 3.00 4.27 -20 2 5 3.41 4.92 -20 2 4 1.96 5.44 -20 2 3 -5.58 6.18 -20 2 2 2.26 4.27 -20 2 1 0.37 4.66 -20 2 0 -2.36 4.76 0 0 0 0.00 0.00 TITL MRC2122 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 15.258789 12.966789 35.832024 90.0000 97.9033 90.0000 ZERR 5.00 0.000667 0.000496 0.002577 0.0000 0.0047 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Mg Mn UNIT 315.00 420.00 20.00 25.00 10.00 5.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 65385 _shelx_fab_file ; -20 2 1 -0.3642 -0.0497 -20 2 2 -0.6235 0.0253 -20 2 3 -0.8814 0.0458 -20 2 4 -0.5661 0.0062 -20 2 5 0.9141 0.0418 -20 2 6 0.0328 -0.0360 -20 2 7 -1.3091 0.0083 -19 1 1 0.8765 0.0249 -19 1 2 -0.8824 0.0328 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-1.8996 0.0002 0 8 30 -1.2667 -0.0029 0 8 31 -1.0666 -0.0123 0 8 32 -0.0642 0.0024 0 8 33 -1.6849 -0.0099 0 8 34 -0.3735 0.0038 0 8 35 -0.1595 -0.0048 0 8 36 -0.4753 0.0067 0 9 1 2.3187 0.0042 0 9 2 -1.5605 0.0063 0 9 3 0.5855 0.0027 0 9 4 0.3806 -0.0165 0 9 5 0.5793 -0.0016 0 9 6 0.1971 0.0028 0 9 7 0.2783 -0.0069 0 9 8 -1.8650 0.0116 0 9 9 -0.7332 0.0023 0 9 10 -0.5581 0.0011 0 9 11 0.4801 -0.0059 0 9 12 -0.0432 0.0015 0 9 13 0.1378 -0.0037 0 9 14 -0.0467 -0.0033 0 9 15 -1.2689 0.0027 0 9 16 0.0449 0.0064 0 9 17 -1.4870 0.0024 0 9 18 0.9159 -0.0071 0 9 19 0.5473 0.0027 0 9 20 0.5112 0.0006 0 9 21 0.9174 0.0006 0 9 22 -0.4741 -0.0099 0 9 23 -0.5995 0.0113 0 9 24 -1.7726 0.0025 0 9 25 0.1866 0.0093 0 9 26 0.3695 0.0019 0 9 27 1.5170 0.0063 0 9 28 1.1942 0.0011 0 9 29 0.4936 0.0176 0 9 30 -1.2063 0.0098 0 9 31 0.0861 0.0028 0 9 32 -0.0663 0.0184 0 9 33 -0.1901 -0.0102 0 9 34 0.7747 -0.0032 0 10 0 -1.8705 -0.0035 0 10 1 1.0565 0.0065 0 10 2 -0.0166 -0.0036 0 10 3 1.1166 0.0024 0 10 4 1.1727 0.0004 0 10 5 0.3803 -0.0052 0 10 6 0.9133 0.0061 0 10 7 0.3105 -0.0016 0 10 8 1.9441 0.0021 0 10 9 -0.4388 0.0042 0 10 10 0.0477 -0.0001 0 10 11 -0.1835 0.0072 0 10 12 -0.2763 0.0059 0 10 13 1.5775 -0.0099 0 10 14 -0.8500 -0.0056 0 10 15 1.1960 -0.0032 0 10 16 -0.4923 0.0092 0 10 17 -0.4065 -0.0062 0 10 18 0.8353 0.0073 0 10 19 0.2508 0.0075 0 10 20 0.7553 -0.0060 0 10 21 0.0475 0.0087 0 10 22 1.8133 -0.0005 0 10 23 -0.5036 0.0002 0 10 24 -1.2365 -0.0107 0 10 25 0.5152 -0.0145 0 10 26 -1.3414 -0.0179 0 10 27 -0.7951 0.0092 0 10 28 0.3699 -0.0135 0 10 29 -1.1582 0.0049 0 10 30 0.3110 -0.0046 0 10 31 2.3344 0.0068 0 10 32 0.6750 -0.0107 0 11 1 -0.0843 0.0076 0 11 2 -3.1611 -0.0013 0 11 3 -0.1746 -0.0006 0 11 4 0.0760 -0.0071 0 11 5 -0.8216 -0.0020 0 11 6 1.4547 -0.0004 0 11 7 1.4340 -0.0006 0 11 8 1.9689 0.0084 0 11 9 0.4143 -0.0129 0 11 10 0.9357 -0.0054 0 11 11 -2.2967 0.0134 0 11 12 0.6535 0.0027 0 11 13 1.2906 0.0007 0 11 14 0.0852 0.0056 0 11 15 0.7712 0.0045 0 11 16 -0.8123 0.0059 0 11 17 0.1991 -0.0027 0 11 18 -0.6532 0.0071 0 11 19 0.2736 -0.0117 0 11 20 -1.2107 0.0069 0 11 21 -0.0990 -0.0051 0 11 22 1.1954 0.0091 0 11 23 -1.4870 0.0005 0 11 24 1.8006 0.0058 0 11 25 0.4062 -0.0057 0 11 26 -0.6876 -0.0140 0 11 27 1.6168 -0.0038 0 11 28 -2.4870 -0.0078 0 11 29 -1.5570 -0.0100 0 11 30 -1.9894 -0.0014 0 12 0 1.8720 -0.0107 0 12 1 0.6722 0.0039 0 12 2 0.2179 0.0032 0 12 3 1.8655 0.0089 0 12 4 -1.6891 -0.0032 0 12 5 -2.7008 -0.0008 0 12 6 -1.1383 0.0055 0 12 7 -1.5532 0.0104 0 12 8 0.6593 -0.0053 0 12 9 1.3154 -0.0002 0 12 10 0.1482 0.0006 0 12 11 -0.4158 -0.0010 0 12 12 0.5141 -0.0062 0 12 13 0.5045 0.0006 0 12 14 1.1775 -0.0001 0 12 15 0.5492 0.0114 0 12 16 -1.0888 -0.0066 0 12 17 1.6622 0.0218 0 12 18 0.9136 -0.0051 0 12 19 0.5625 -0.0026 0 12 20 1.8623 0.0015 0 12 21 0.5581 0.0066 0 12 22 -1.1096 0.0143 0 12 23 0.7455 -0.0037 0 12 24 0.8702 0.0038 0 12 25 -1.3553 0.0132 0 12 26 1.4881 0.0101 0 12 27 -0.8547 -0.0202 0 12 28 -1.4188 0.0285 0 12 29 -0.6223 -0.0171 0 12 30 -1.1069 -0.0048 0 12 31 -0.1703 -0.0100 0 12 32 -0.9714 -0.0495 0 13 1 -1.8605 0.0047 0 13 2 -0.5761 -0.0075 0 13 3 1.4291 0.0026 0 13 4 -0.0772 -0.0022 0 13 5 1.4820 -0.0045 0 13 6 0.3906 -0.0058 0 13 7 -0.3051 0.0038 0 13 8 2.1793 0.0038 0 13 9 -1.0676 0.0004 0 13 10 0.0850 0.0014 0 13 11 0.0722 -0.0077 0 13 12 -0.5307 0.0106 0 13 13 -1.0258 0.0008 0 13 14 -0.4885 0.0069 0 13 15 -0.5410 -0.0028 0 13 16 1.1255 -0.0098 0 13 17 -0.0211 -0.0015 0 13 18 -0.3060 -0.0141 0 13 19 1.0343 0.0027 0 13 20 -1.1070 -0.0085 0 13 21 0.5945 -0.0023 0 13 22 1.2546 -0.0176 0 13 23 0.8810 0.0193 0 13 24 0.8185 -0.0075 0 13 25 1.7008 -0.0277 0 13 26 1.2661 0.0028 0 13 27 0.0809 -0.0243 0 13 28 0.0864 0.0198 0 13 29 -0.7851 -0.0473 0 13 30 -2.4026 0.1179 0 14 0 0.1351 -0.0002 0 14 1 -0.7427 0.0059 0 14 2 1.5364 -0.0056 0 14 3 -0.0560 0.0018 0 14 4 -1.2512 -0.0046 0 14 5 0.9201 0.0111 0 14 6 -1.4358 -0.0004 0 14 7 0.7340 0.0016 0 14 8 -1.2713 -0.0026 0 14 9 0.3015 0.0095 0 14 10 0.3925 0.0091 0 14 11 -0.1323 -0.0049 0 14 12 2.0352 0.0087 0 14 13 -0.6218 0.0192 0 14 14 1.4902 0.0214 0 14 15 -1.0049 0.0151 0 14 16 2.5808 0.0228 0 14 17 -0.3283 0.0070 0 14 18 -1.2665 0.0079 0 14 19 -0.0758 0.0138 0 14 20 -0.8899 0.0002 0 14 21 0.5177 0.0108 0 14 22 -0.2549 0.0081 0 14 23 0.2559 0.0226 0 14 24 -2.0214 -0.0149 1 0 4 -65.7617 0.0292 1 0 6 53.8891 0.0378 1 0 8 50.9100 0.0415 1 0 10 -20.1449 0.0003 1 0 12 -8.9169 0.0163 1 0 14 9.6203 0.0230 1 0 16 -3.7455 0.0093 1 0 18 -7.3558 -0.0112 1 0 20 -1.0564 0.0286 1 0 22 2.4159 -0.0117 1 0 24 1.0449 -0.0025 1 0 26 -1.2829 -0.0091 1 0 28 -1.4428 -0.0091 1 0 30 -1.0122 -0.0082 1 0 32 2.5677 -0.0026 1 0 34 1.0503 -0.0039 1 0 36 0.6145 -0.0086 1 0 38 -0.0125 -0.0012 1 0 40 0.2164 -0.0042 1 0 42 2.1263 0.0126 1 0 44 0.6969 0.0019 1 1 2 32.4099 0.0089 1 1 3 18.9625 -0.0391 1 1 4 -60.4138 -0.0093 1 1 5 18.9070 -0.0643 1 1 6 -35.3004 0.0176 1 1 7 -10.0235 -0.0154 1 1 8 35.4792 0.0190 1 1 9 -31.9999 -0.0496 1 1 10 20.6482 -0.0033 1 1 11 -3.9028 -0.0068 1 1 12 -19.2487 0.0235 1 1 13 15.6880 -0.0389 1 1 14 -2.8325 -0.0041 1 1 15 6.1668 -0.0001 1 1 16 9.2347 0.0024 1 1 17 0.5166 0.0008 1 1 18 3.1140 0.0078 1 1 19 1.0984 -0.0101 1 1 20 -4.7645 0.0053 1 1 21 1.9152 -0.0011 1 1 22 -2.9430 -0.0002 1 1 23 0.6099 -0.0058 1 1 24 0.1366 0.0044 1 1 25 -2.2084 -0.0054 1 1 26 1.1278 0.0079 1 1 27 2.9916 0.0090 1 1 28 0.0575 -0.0053 1 1 29 2.7015 0.0087 1 1 30 -1.3537 -0.0081 1 1 31 -2.1865 0.0011 1 1 32 -1.3060 -0.0058 1 1 33 -0.5017 0.0103 1 1 34 -0.5579 -0.0034 1 1 35 -1.1113 0.0065 1 1 36 1.8612 -0.0092 1 1 37 -0.0498 -0.0026 1 1 38 -1.1576 0.0060 1 1 39 0.0677 0.0105 1 1 40 1.2242 -0.0009 1 1 41 -0.2517 0.0012 1 1 42 1.1825 0.0044 1 1 43 -1.4820 0.0058 1 1 44 -0.4189 -0.0050 1 2 0 -13.8716 -0.0158 1 2 1 -3.4588 0.0467 1 2 2 12.7356 -0.0114 1 2 3 -1.7391 -0.0430 1 2 4 -7.4440 -0.0157 1 2 5 4.6031 0.0023 1 2 6 -24.4210 -0.0430 1 2 7 16.0159 0.0565 1 2 8 1.7349 0.0105 1 2 9 -7.8948 -0.0366 1 2 10 23.4622 0.0313 1 2 11 -18.7183 -0.0116 1 2 12 3.9504 0.0110 1 2 13 -0.1224 -0.0001 1 2 14 -11.9189 0.0227 1 2 15 6.8297 -0.0105 1 2 16 -5.2168 0.0048 1 2 17 -2.6634 -0.0039 1 2 18 4.0784 0.0063 1 2 19 -4.2168 -0.0002 1 2 20 4.4511 0.0128 1 2 21 2.0996 -0.0087 1 2 22 0.8650 -0.0078 1 2 23 6.2863 -0.0045 1 2 24 -1.1293 0.0014 1 2 25 -2.3429 -0.0082 1 2 26 -2.5120 0.0079 1 2 27 -3.2907 -0.0040 1 2 28 0.0496 0.0016 1 2 29 4.6871 0.0011 1 2 30 -0.9830 0.0080 1 2 31 2.7741 0.0076 1 2 32 -0.1782 -0.0041 1 2 33 -4.5909 0.0002 1 2 34 0.9267 -0.0091 1 2 35 -0.5702 -0.0047 1 2 36 -0.4271 -0.0062 1 2 37 -0.2421 0.0145 1 2 38 0.2038 -0.0125 1 2 39 -1.6434 -0.0066 1 2 40 -1.0008 -0.0091 1 2 41 0.6367 0.0180 1 2 42 2.3943 -0.0008 1 2 43 0.1106 0.0157 1 2 44 2.6197 -0.0247 1 3 0 -1.6245 0.0061 1 3 1 -0.5649 0.0061 1 3 2 5.6073 0.0133 1 3 3 18.4427 -0.0167 1 3 4 -6.0556 0.0025 1 3 5 0.0027 0.0257 1 3 6 -7.8571 0.0034 1 3 7 -6.0202 0.0019 1 3 8 -4.3263 -0.0068 1 3 9 0.9632 -0.0101 1 3 10 0.1516 0.0081 1 3 11 -5.3778 0.0128 1 3 12 2.8020 -0.0280 1 3 13 -2.9170 0.0040 1 3 14 0.0846 0.0092 1 3 15 4.6429 -0.0196 1 3 16 0.0128 -0.0037 1 3 17 6.5935 0.0002 1 3 18 -1.9676 0.0072 1 3 19 -2.4421 -0.0077 1 3 20 1.1858 0.0125 1 3 21 -6.2769 -0.0040 1 3 22 1.2173 0.0013 1 3 23 0.4196 0.0027 1 3 24 -0.5337 -0.0001 1 3 25 2.9399 -0.0054 1 3 26 -0.4733 0.0006 1 3 27 -0.5590 -0.0015 1 3 28 0.5519 -0.0003 1 3 29 1.5310 0.0007 1 3 30 -0.1793 0.0081 1 3 31 5.5329 -0.0032 1 3 32 -2.0104 0.0011 1 3 33 1.5343 -0.0029 1 3 34 -0.9602 -0.0086 1 3 35 -3.7530 -0.0082 1 3 36 1.7018 0.0009 1 3 37 -1.1900 -0.0081 1 3 38 2.4406 -0.0039 1 3 39 0.1635 -0.0007 1 3 40 -1.2973 -0.0003 1 3 41 -2.6246 0.0034 1 3 42 -1.8440 0.0170 1 3 43 -1.1293 0.0047 1 3 44 0.9682 -0.0118 1 4 0 -3.6107 0.0522 1 4 1 -7.7118 -0.0217 1 4 2 -0.8742 0.0148 1 4 3 1.8794 -0.0065 1 4 4 0.1536 -0.0168 1 4 5 2.1658 0.0066 1 4 6 -6.1490 -0.0041 1 4 7 -1.2798 -0.0080 1 4 8 3.1059 -0.0062 1 4 9 -0.5894 -0.0063 1 4 10 4.7919 -0.0000 1 4 11 -0.3238 -0.0057 1 4 12 -1.5351 -0.0129 1 4 13 -3.7725 0.0157 1 4 14 -3.9130 -0.0068 1 4 15 -0.9343 -0.0022 1 4 16 -0.9461 -0.0004 1 4 17 2.1519 0.0069 1 4 18 0.0302 0.0039 1 4 19 1.5346 0.0077 1 4 20 -1.4813 0.0038 1 4 21 0.6642 -0.0112 1 4 22 3.1129 0.0033 1 4 23 -0.8537 0.0035 1 4 24 1.4571 0.0102 1 4 25 -0.3668 -0.0097 1 4 26 -0.6884 0.0036 1 4 27 -0.5487 -0.0034 1 4 28 -2.1927 -0.0143 1 4 29 -0.8502 0.0093 1 4 30 -0.3673 0.0048 1 4 31 0.9939 -0.0066 1 4 32 0.8999 0.0069 1 4 33 1.6551 -0.0051 1 4 34 -0.6583 -0.0069 1 4 35 -1.5806 0.0037 1 4 36 -2.3810 0.0053 1 4 37 -0.4695 -0.0036 1 4 38 -0.4319 -0.0017 1 4 39 0.6423 -0.0002 1 4 40 1.9687 0.0076 1 4 41 0.7658 -0.0112 1 5 0 -0.8343 -0.0003 1 5 1 2.2711 0.0101 1 5 2 -2.3880 -0.0091 1 5 3 4.0141 -0.0089 1 5 4 2.1218 -0.0030 1 5 5 3.9158 -0.0138 1 5 6 0.7591 0.0251 1 5 7 -4.6629 -0.0213 1 5 8 -1.8911 0.0115 1 5 9 -3.3588 0.0026 1 5 10 -0.0156 -0.0097 1 5 11 0.0273 0.0068 1 5 12 2.5318 -0.0040 1 5 13 -1.4790 0.0117 1 5 14 -0.5460 -0.0006 1 5 15 -0.7215 0.0006 1 5 16 -0.8663 0.0064 1 5 17 1.2062 0.0032 1 5 18 0.4952 -0.0051 1 5 19 0.1694 0.0079 1 5 20 -0.8012 -0.0043 1 5 21 -0.0117 0.0018 1 5 22 -0.4121 -0.0102 1 5 23 0.7242 0.0026 1 5 24 0.7285 -0.0031 1 5 25 1.3129 0.0012 1 5 26 0.4197 -0.0011 1 5 27 1.3951 -0.0078 1 5 28 0.1024 0.0035 1 5 29 -0.2092 -0.0004 1 5 30 0.0783 0.0015 1 5 31 2.1859 0.0016 1 5 32 0.8079 0.0001 1 5 33 0.1297 0.0123 1 5 34 2.8691 -0.0071 1 5 35 -0.6907 0.0012 1 5 36 3.6372 0.0015 1 5 37 -0.3430 -0.0186 1 5 38 -2.7129 -0.0042 1 5 39 -1.3374 -0.0066 1 5 40 -3.5623 -0.0062 1 6 0 -0.2589 0.0022 1 6 1 -0.4179 0.0041 1 6 2 -0.0855 0.0074 1 6 3 0.6880 -0.0005 1 6 4 -1.8238 -0.0044 1 6 5 3.5886 0.0178 1 6 6 -1.0713 0.0053 1 6 7 2.6294 0.0129 1 6 8 3.9030 0.0137 1 6 9 -0.9502 -0.0049 1 6 10 4.4520 -0.0028 1 6 11 0.1351 -0.0063 1 6 12 -2.1595 0.0081 1 6 13 -0.5221 -0.0270 1 6 14 -1.6266 -0.0082 1 6 15 -0.5637 -0.0041 1 6 16 -0.0760 -0.0040 1 6 17 0.4138 -0.0037 1 6 18 1.2107 -0.0095 1 6 19 -0.9310 0.0012 1 6 20 -0.3522 -0.0012 1 6 21 0.6356 0.0019 1 6 22 -2.3159 0.0033 1 6 23 0.7429 0.0057 1 6 24 -0.3264 -0.0022 1 6 25 -0.3368 0.0146 1 6 26 0.1430 -0.0072 1 6 27 1.0660 0.0051 1 6 28 -1.7297 -0.0024 1 6 29 1.0674 0.0028 1 6 30 1.0044 0.0014 1 6 31 0.4894 -0.0034 1 6 32 0.5823 0.0017 1 6 33 -2.5933 -0.0089 1 6 34 -2.7051 -0.0104 1 6 35 -1.3189 -0.0035 1 6 36 2.2396 -0.0177 1 6 37 2.7841 0.0064 1 6 38 0.4890 0.0044 1 6 39 0.2172 0.0001 1 7 0 -0.6744 0.0030 1 7 1 0.1535 -0.0058 1 7 2 -0.9302 -0.0108 1 7 3 1.2314 -0.0070 1 7 4 1.8632 -0.0078 1 7 5 -0.3389 -0.0036 1 7 6 -1.0713 -0.0007 1 7 7 -1.7525 0.0019 1 7 8 -1.9431 0.0021 1 7 9 -2.5058 0.0029 1 7 10 2.8961 -0.0111 1 7 11 -0.7436 0.0139 1 7 12 2.4862 -0.0011 1 7 13 0.1800 -0.0082 1 7 14 0.0004 0.0116 1 7 15 0.4317 -0.0022 1 7 16 0.7292 0.0072 1 7 17 1.3003 -0.0040 1 7 18 0.9310 0.0120 1 7 19 -1.1669 -0.0107 1 7 20 1.2932 0.0031 1 7 21 -1.3947 0.0030 1 7 22 -0.8087 -0.0078 1 7 23 2.0785 0.0020 1 7 24 -2.4261 0.0035 1 7 25 1.8293 -0.0054 1 7 26 1.4561 -0.0035 1 7 27 1.6107 0.0036 1 7 28 0.8980 -0.0042 1 7 29 0.5604 0.0080 1 7 30 0.7666 -0.0040 1 7 31 1.0621 -0.0002 1 7 32 4.5185 -0.0024 1 7 33 1.5129 -0.0004 1 7 34 1.1958 0.0001 1 7 35 -1.7964 0.0006 1 7 36 -0.2479 0.0200 1 7 37 -2.4795 0.0009 1 8 0 -1.3213 0.0159 1 8 1 -0.5047 -0.0078 1 8 2 -0.9488 0.0012 1 8 3 0.8633 -0.0064 1 8 4 -1.3050 -0.0041 1 8 5 0.7982 0.0026 1 8 6 1.2032 -0.0060 1 8 7 1.6502 0.0021 1 8 8 2.0548 -0.0056 1 8 9 1.3989 0.0035 1 8 10 0.7804 0.0035 1 8 11 -0.0282 0.0017 1 8 12 -0.9676 -0.0049 1 8 13 0.3737 0.0025 1 8 14 -0.9297 -0.0019 1 8 15 -1.6385 0.0169 1 8 16 0.6862 -0.0079 1 8 17 0.1279 0.0005 1 8 18 1.4885 0.0023 1 8 19 0.5091 -0.0138 1 8 20 0.6941 -0.0066 1 8 21 0.1293 -0.0130 1 8 22 0.5411 -0.0085 1 8 23 -0.2462 -0.0051 1 8 24 -0.9763 0.0031 1 8 25 -1.2101 -0.0065 1 8 26 -3.0441 0.0014 1 8 27 0.4746 -0.0022 1 8 28 -1.8604 -0.0010 1 8 29 0.9630 0.0041 1 8 30 -0.6222 -0.0002 1 8 31 -0.9705 0.0048 1 8 32 0.5836 0.0063 1 8 33 0.5172 -0.0056 1 8 34 2.3079 0.0033 1 8 35 3.6457 0.0026 1 9 0 -2.1436 0.0036 1 9 1 0.3379 0.0020 1 9 2 0.0675 -0.0136 1 9 3 -0.8549 -0.0011 1 9 4 1.0308 0.0005 1 9 5 -1.9869 -0.0100 1 9 6 -0.9335 0.0189 1 9 7 -2.7909 -0.0025 1 9 8 -0.6954 -0.0069 1 9 9 -0.4909 0.0007 1 9 10 0.1616 -0.0044 1 9 11 0.6778 -0.0009 1 9 12 -0.0108 -0.0135 1 9 13 0.0186 -0.0032 1 9 14 -1.3006 0.0003 1 9 15 -0.0575 -0.0042 1 9 16 -0.0324 0.0031 1 9 17 -0.1968 0.0072 1 9 18 0.8371 -0.0043 1 9 19 1.5102 0.0123 1 9 20 0.7057 -0.0065 1 9 21 0.9764 0.0091 1 9 22 0.4186 0.0014 1 9 23 -0.2408 0.0063 1 9 24 -0.0641 0.0042 1 9 25 0.4263 -0.0017 1 9 26 1.8625 -0.0005 1 9 27 -0.3379 0.0058 1 9 28 0.4260 0.0092 1 9 29 0.4733 -0.0001 1 9 30 0.2188 0.0169 1 9 31 2.1147 -0.0073 1 9 32 0.3711 0.0061 1 9 33 -1.0356 -0.0117 1 9 34 -0.1370 -0.0129 1 10 0 -1.3804 -0.0097 1 10 1 1.1451 0.0008 1 10 2 0.0083 -0.0065 1 10 3 -0.3794 -0.0023 1 10 4 0.0826 -0.0014 1 10 5 0.6342 0.0010 1 10 6 1.4129 0.0048 1 10 7 -0.2522 -0.0033 1 10 8 0.0498 0.0017 1 10 9 -1.8341 0.0013 1 10 10 -0.4482 0.0042 1 10 11 0.4222 -0.0018 1 10 12 0.6913 -0.0015 1 10 13 0.5598 -0.0026 1 10 14 -1.0208 -0.0032 1 10 15 -1.3434 -0.0051 1 10 16 0.0275 0.0093 1 10 17 -0.9429 -0.0089 1 10 18 0.1177 -0.0032 1 10 19 -1.2432 0.0069 1 10 20 0.4493 -0.0113 1 10 21 0.5284 0.0031 1 10 22 -0.0899 -0.0076 1 10 23 2.4990 -0.0124 1 10 24 -0.7437 -0.0079 1 10 25 1.0444 -0.0005 1 10 26 -0.3766 -0.0128 1 10 27 -0.4896 0.0103 1 10 28 -0.8070 -0.0010 1 10 29 -0.3430 -0.0106 1 10 30 0.7747 0.0026 1 10 31 0.0265 0.0039 1 10 32 -1.0553 0.0163 1 11 0 -2.6351 0.0044 1 11 1 0.5951 0.0014 1 11 2 -0.6878 -0.0020 1 11 3 -0.5270 -0.0053 1 11 4 0.9927 -0.0090 1 11 5 -0.4454 0.0076 1 11 6 0.5937 0.0008 1 11 7 1.7102 -0.0041 1 11 8 -0.6593 -0.0080 1 11 9 -1.3088 -0.0017 1 11 10 -0.8170 -0.0056 1 11 11 0.1795 -0.0051 1 11 12 -0.0907 0.0020 1 11 13 0.6458 0.0030 1 11 14 -1.0261 0.0047 1 11 15 -0.8117 0.0074 1 11 16 -1.3904 0.0034 1 11 17 -0.3983 -0.0005 1 11 18 -0.7160 0.0054 1 11 19 -1.1115 0.0007 1 11 20 -0.2320 -0.0000 1 11 21 -1.5746 0.0088 1 11 22 0.6256 -0.0054 1 11 23 -0.5418 0.0131 1 11 24 0.2615 -0.0078 1 11 25 1.4307 -0.0037 1 11 26 -0.4477 -0.0064 1 11 27 0.2991 0.0054 1 11 28 -1.3665 -0.0155 1 11 29 0.7699 0.0185 1 12 0 0.6340 -0.0058 1 12 1 0.6902 0.0045 1 12 2 -1.2111 -0.0003 1 12 3 -1.0475 0.0007 1 12 4 -1.0660 0.0018 1 12 5 -2.7194 -0.0013 1 12 6 0.8221 0.0036 1 12 7 -0.0308 0.0065 1 12 8 0.7108 0.0037 1 12 9 -0.4532 -0.0056 1 12 10 -0.7587 -0.0002 1 12 11 -0.3544 -0.0167 1 12 12 1.1236 -0.0029 1 12 13 -0.1424 -0.0146 1 12 14 0.4910 -0.0004 1 12 15 1.0077 0.0131 1 12 16 -0.3337 -0.0046 1 12 17 0.1714 -0.0142 1 12 18 0.6560 0.0164 1 12 19 -0.3771 -0.0062 1 12 20 -1.2188 0.0138 1 12 21 0.9075 -0.0044 1 12 22 -1.6573 0.0136 1 12 23 -0.0375 0.0006 1 12 24 0.2376 0.0048 1 12 25 -0.6540 0.0080 1 12 26 -0.4021 0.0117 1 12 27 -0.5589 -0.0205 1 12 28 -1.8726 -0.0189 1 12 29 -0.3198 -0.0017 1 12 30 -2.1034 -0.0545 1 12 31 0.4563 -0.0046 1 12 32 -0.7311 -0.0174 1 13 0 -0.5175 -0.0058 1 13 1 1.4479 0.0051 1 13 2 0.9023 -0.0084 1 13 3 2.0332 0.0008 1 13 4 0.5131 -0.0133 1 13 5 0.8668 -0.0005 1 13 6 0.7598 -0.0128 1 13 7 -0.8432 -0.0008 1 13 8 0.5611 0.0048 1 13 9 -0.4789 -0.0058 1 13 10 -0.1126 0.0025 1 13 11 -2.1296 -0.0025 1 13 12 -0.8396 -0.0032 1 13 13 -2.4652 -0.0023 1 13 14 1.3525 -0.0092 1 13 15 -0.6526 -0.0154 1 13 16 0.0397 -0.0078 1 13 17 0.3526 0.0079 1 13 18 -3.1785 -0.0078 1 13 19 0.3881 -0.0109 1 13 20 1.0576 0.0059 1 13 21 0.3817 0.0033 1 13 22 0.3917 0.0001 1 13 23 0.3913 -0.0085 1 13 24 -1.2102 0.0262 1 13 25 0.3250 -0.0118 1 13 26 1.9638 0.0147 1 13 27 -0.3833 0.0038 1 13 28 -0.3385 0.0501 1 13 29 -0.8596 0.0528 1 13 30 -1.4722 0.0052 1 14 0 -0.1448 -0.0047 1 14 1 0.4085 -0.0030 1 14 2 -1.3166 -0.0019 1 14 3 0.1593 0.0116 1 14 4 -1.5388 0.0067 1 14 5 0.0363 0.0055 1 14 6 -0.5027 -0.0016 1 14 7 1.0267 0.0048 1 14 8 -1.2136 0.0008 1 14 9 0.2633 0.0021 1 14 10 1.9564 0.0012 1 14 11 -0.7366 -0.0071 2 0 0 -50.0809 0.4653 2 0 2 -74.1752 0.2809 2 0 4 30.9574 -0.0838 2 0 6 69.3037 0.0552 2 0 8 -9.3302 -0.0248 2 0 10 -32.1495 0.0163 2 0 12 2.8925 -0.0032 2 0 14 2.9683 0.0005 2 0 16 -9.3365 -0.0356 2 0 18 -6.0010 0.0008 2 0 20 1.1520 -0.0173 2 0 22 3.7256 -0.0281 2 0 24 -2.4815 -0.0027 2 0 26 -4.8434 -0.0122 2 0 28 1.4749 -0.0009 2 0 30 4.7179 -0.0021 2 0 32 1.2184 0.0001 2 0 34 0.1194 -0.0050 2 0 36 -0.4190 0.0055 2 0 38 -0.5964 0.0033 2 0 40 2.4480 0.0051 2 0 42 0.9489 0.0078 2 0 44 -0.2406 -0.0266 2 1 0 53.1654 -0.0610 2 1 1 33.4176 -0.0797 2 1 2 -27.9623 0.1310 2 1 3 -4.7025 -0.1518 2 1 4 -42.5876 0.0209 2 1 5 -14.1394 0.0011 2 1 6 20.1952 0.0215 2 1 7 -16.7988 -0.0342 2 1 8 35.7039 0.0012 2 1 9 -5.8528 -0.0008 2 1 10 -11.4654 0.0083 2 1 11 9.5052 0.0132 2 1 12 -12.4331 0.0023 2 1 13 5.8871 0.0035 2 1 14 8.5373 -0.0087 2 1 15 -1.5321 0.0310 2 1 16 5.3237 0.0139 2 1 17 -0.9588 -0.0037 2 1 18 -4.3481 0.0049 2 1 19 2.3779 0.0148 2 1 20 -4.7404 -0.0024 2 1 21 1.9004 0.0093 2 1 22 0.8936 -0.0126 2 1 23 -2.1921 0.0014 2 1 24 1.8257 0.0022 2 1 25 -1.4471 0.0011 2 1 26 -0.7199 -0.0078 2 1 27 2.7508 0.0084 2 1 28 -3.2432 -0.0067 2 1 29 -0.8116 0.0044 2 1 30 0.8280 -0.0024 2 1 31 -1.6747 0.0060 2 1 32 -0.3398 0.0005 2 1 33 -1.4182 0.0053 2 1 34 1.4739 -0.0070 2 1 35 0.2040 0.0021 2 1 36 -0.0160 -0.0046 2 1 37 -0.5410 0.0071 2 1 38 0.4246 -0.0062 2 1 39 -1.3610 -0.0004 2 1 40 1.8768 -0.0031 2 1 41 -0.1847 0.0012 2 1 42 -0.7023 0.0011 2 1 43 -0.5626 0.0101 2 1 44 -0.7214 -0.0111 2 2 0 -0.5639 0.0246 2 2 1 30.4798 -0.0084 2 2 2 7.8891 0.0392 2 2 3 13.6418 -0.0175 2 2 4 -6.1411 0.0031 2 2 5 -1.5727 0.0598 2 2 6 -0.1142 0.0205 2 2 7 -1.1970 -0.0368 2 2 8 14.7223 0.0612 2 2 9 -3.2958 -0.0486 2 2 10 4.5626 0.0084 2 2 11 -2.6562 0.0014 2 2 12 -11.2993 -0.0009 2 2 13 2.7038 -0.0092 2 2 14 -6.9118 -0.0102 2 2 15 -0.6150 -0.0048 2 2 16 1.6392 -0.0213 2 2 17 -3.1773 0.0129 2 2 18 2.0812 0.0033 2 2 19 -0.2951 0.0013 2 2 20 0.3075 -0.0011 2 2 21 5.7761 0.0056 2 2 22 0.2775 -0.0063 2 2 23 0.6898 0.0051 2 2 24 -3.0566 0.0010 2 2 25 -4.4013 -0.0006 2 2 26 -0.9257 -0.0116 2 2 27 1.1600 0.0025 2 2 28 0.0274 -0.0001 2 2 29 4.6221 0.0060 2 2 30 0.1172 0.0027 2 2 31 -1.3892 0.0045 2 2 32 1.6071 -0.0089 2 2 33 -2.0962 -0.0077 2 2 34 -0.9461 -0.0007 2 2 35 1.1953 -0.0005 2 2 36 0.6543 0.0000 2 2 37 -0.0262 0.0025 2 2 38 -0.4296 -0.0040 2 2 39 -0.7414 0.0009 2 2 40 1.6413 0.0056 2 2 41 -2.1185 0.0060 2 2 42 3.9828 0.0074 2 2 43 0.5053 -0.0035 2 2 44 -1.4900 -0.0191 2 3 0 1.2919 0.0123 2 3 1 10.0591 -0.0193 2 3 2 2.8941 -0.0067 2 3 3 10.1595 0.0198 2 3 4 -3.1607 0.0157 2 3 5 -8.1968 0.0104 2 3 6 2.0117 -0.0131 2 3 7 -4.3632 -0.0135 2 3 8 4.0432 0.0166 2 3 9 1.3430 0.0095 2 3 10 4.6023 -0.0125 2 3 11 2.9158 0.0114 2 3 12 -0.3010 0.0047 2 3 13 1.8199 -0.0256 2 3 14 0.4276 0.0188 2 3 15 2.5515 -0.0192 2 3 16 -0.4232 -0.0021 2 3 17 -0.4450 -0.0062 2 3 18 -2.3899 0.0066 2 3 19 -5.8618 -0.0075 2 3 20 -2.1823 -0.0085 2 3 21 -0.4867 0.0093 2 3 22 1.1688 -0.0014 2 3 23 3.2571 0.0095 2 3 24 0.8957 0.0037 2 3 25 -0.0382 0.0006 2 3 26 -1.4853 -0.0016 2 3 27 -2.2716 0.0051 2 3 28 -0.2099 -0.0043 2 3 29 2.2679 0.0005 2 3 30 -0.1087 0.0086 2 3 31 3.5828 -0.0062 2 3 32 -0.2707 -0.0038 2 3 33 -1.6077 0.0059 2 3 34 0.2712 -0.0075 2 3 35 -2.2790 0.0016 2 3 36 1.3658 0.0022 2 3 37 1.4478 0.0010 2 3 38 0.0040 0.0011 2 3 39 -0.3006 0.0056 2 3 40 -1.5184 -0.0051 2 3 41 -0.5951 -0.0007 2 3 42 1.3314 0.0071 2 3 43 -1.1480 0.0138 2 3 44 1.1694 -0.0059 2 3 45 0.9925 0.0138 2 4 0 -12.1708 0.0305 2 4 1 0.4113 -0.0147 2 4 2 1.9937 -0.0395 2 4 3 1.6114 0.0126 2 4 4 3.1007 -0.0112 2 4 5 -1.1468 -0.0056 2 4 6 2.3458 -0.0018 2 4 7 1.2911 0.0021 2 4 8 4.0320 0.0027 2 4 9 3.0301 0.0093 2 4 10 1.4518 0.0007 2 4 11 -0.5285 0.0190 2 4 12 -1.0543 -0.0057 2 4 13 -0.4073 0.0191 2 4 14 -3.1158 0.0039 2 4 15 2.5062 -0.0014 2 4 16 2.1556 0.0059 2 4 17 0.9133 0.0027 2 4 18 0.4347 0.0050 2 4 19 -0.0768 -0.0171 2 4 20 0.4722 -0.0014 2 4 21 -1.2771 -0.0067 2 4 22 0.1044 -0.0029 2 4 23 -0.2819 0.0009 2 4 24 -0.2352 -0.0003 2 4 25 -0.4528 -0.0000 2 4 26 -1.7483 -0.0102 2 4 27 -1.7596 0.0064 2 4 28 -2.1911 -0.0036 2 4 29 -0.8353 0.0048 2 4 30 0.5798 0.0125 2 4 31 0.7749 0.0008 2 4 32 0.0109 0.0034 2 4 33 -0.4864 0.0030 2 4 34 -1.2140 0.0052 2 4 35 -0.3241 -0.0029 2 4 36 -0.5829 0.0044 2 4 37 0.8733 0.0037 2 4 38 0.8052 0.0113 2 4 39 1.1801 -0.0165 2 4 40 2.5482 0.0108 2 4 41 0.5960 -0.0184 2 5 0 -3.5328 -0.0091 2 5 1 3.7555 -0.0119 2 5 2 -2.2382 0.0092 2 5 3 3.6222 -0.0088 2 5 4 0.5429 0.0143 2 5 5 -6.4240 -0.0081 2 5 6 0.0518 0.0119 2 5 7 -7.8363 0.0050 2 5 8 -0.4757 -0.0231 2 5 9 3.3399 0.0149 2 5 10 1.6435 -0.0098 2 5 11 3.2932 0.0025 2 5 12 1.1295 -0.0033 2 5 13 -0.5310 -0.0008 2 5 14 -1.2354 0.0056 2 5 15 1.9094 0.0043 2 5 16 -1.2311 -0.0027 2 5 17 2.2927 0.0070 2 5 18 -1.0117 -0.0091 2 5 19 -0.1436 -0.0012 2 5 20 -0.7139 -0.0041 2 5 21 0.4866 -0.0073 2 5 22 0.1528 0.0018 2 5 23 -0.0470 -0.0000 2 5 24 1.0230 0.0007 2 5 25 0.7842 0.0006 2 5 26 0.2409 0.0044 2 5 27 -2.3268 -0.0041 2 5 28 0.3681 0.0049 2 5 29 -0.8518 -0.0005 2 5 30 0.6805 -0.0042 2 5 31 2.3084 0.0109 2 5 32 0.0095 -0.0009 2 5 33 1.7890 0.0085 2 5 34 0.4134 -0.0094 2 5 35 1.7768 -0.0084 2 5 36 -1.7223 0.0074 2 5 37 -2.7054 -0.0006 2 5 38 -4.5925 -0.0060 2 5 39 -0.4990 0.0074 2 6 0 0.0089 0.0078 2 6 1 -1.3660 -0.0025 2 6 2 -0.4518 0.0029 2 6 3 2.5428 0.0019 2 6 4 -0.2070 -0.0040 2 6 5 2.4468 0.0095 2 6 6 1.5575 0.0135 2 6 7 -4.7062 -0.0132 2 6 8 3.7089 -0.0005 2 6 9 -3.8862 -0.0022 2 6 10 -0.4095 0.0014 2 6 11 1.2885 -0.0109 2 6 12 -1.6709 -0.0027 2 6 13 -0.1127 -0.0062 2 6 14 0.2263 -0.0106 2 6 15 -0.4119 0.0128 2 6 16 1.8615 -0.0039 2 6 17 -0.6230 0.0048 2 6 18 0.8519 -0.0031 2 6 19 0.1777 0.0124 2 6 20 -2.9771 -0.0033 2 6 21 1.2426 0.0018 2 6 22 -2.4853 -0.0038 2 6 23 0.7402 0.0028 2 6 24 -0.3012 0.0068 2 6 25 0.1317 -0.0023 2 6 26 0.2535 -0.0052 2 6 27 -0.8634 0.0010 2 6 28 0.3779 0.0053 2 6 29 -3.8093 -0.0071 2 6 30 1.4846 0.0064 2 6 31 -5.3305 -0.0044 2 6 32 -1.5860 0.0041 2 6 33 -1.9377 -0.0090 2 6 34 -0.6265 -0.0050 2 6 35 6.2049 0.0091 2 6 36 -0.8761 0.0110 2 6 37 3.5193 -0.0010 2 6 38 -0.1075 0.0181 2 7 0 -1.3721 -0.0038 2 7 1 0.7095 -0.0034 2 7 2 -0.2160 -0.0089 2 7 3 -1.0103 -0.0023 2 7 4 -0.2978 -0.0063 2 7 5 -0.5059 0.0051 2 7 6 -2.4130 0.0014 2 7 7 -0.7487 -0.0001 2 7 8 -0.7373 -0.0022 2 7 9 -1.5317 0.0073 2 7 10 0.7997 0.0030 2 7 11 0.4727 -0.0008 2 7 12 0.0858 0.0141 2 7 13 1.5774 -0.0047 2 7 14 -0.9296 0.0113 2 7 15 0.7094 0.0043 2 7 16 -0.7365 0.0108 2 7 17 -0.3889 -0.0074 2 7 18 1.9707 0.0066 2 7 19 -1.5575 0.0097 2 7 20 1.1514 -0.0181 2 7 21 -0.2245 0.0106 2 7 22 -2.0152 -0.0186 2 7 23 1.7163 -0.0003 2 7 24 -1.1256 -0.0025 2 7 25 2.1843 -0.0025 2 7 26 -0.0731 -0.0004 2 7 27 0.3456 0.0066 2 7 28 0.3766 -0.0052 2 7 29 -0.9145 -0.0016 2 7 30 2.3322 0.0041 2 7 31 0.3144 -0.0004 2 7 32 -0.1027 0.0081 2 7 33 -2.8222 0.0033 2 7 34 -0.9637 0.0146 2 7 35 -2.8155 0.0075 2 7 36 -1.5243 0.0067 2 7 37 1.8150 0.0109 2 8 0 1.1496 0.0032 2 8 1 0.2462 0.0013 2 8 2 1.0780 -0.0050 2 8 3 -0.6587 0.0059 2 8 4 1.8224 0.0031 2 8 5 -0.4032 0.0022 2 8 6 2.4387 -0.0061 2 8 7 0.9792 0.0027 2 8 8 0.1651 -0.0028 2 8 9 -0.7363 -0.0006 2 8 10 -1.8904 -0.0057 2 8 11 -0.4673 -0.0031 2 8 12 -1.7140 -0.0056 2 8 13 -1.3166 0.0055 2 8 14 0.3886 0.0011 2 8 15 -0.6796 -0.0016 2 8 16 0.1839 0.0020 2 8 17 1.0476 -0.0141 2 8 18 -0.4742 0.0104 2 8 19 1.1269 -0.0062 2 8 20 -0.5491 0.0035 2 8 21 -0.2495 -0.0021 2 8 22 -0.8721 0.0073 2 8 23 -2.4870 -0.0017 2 8 24 -1.6375 -0.0018 2 8 25 -0.7298 0.0062 2 8 26 -0.6615 -0.0074 2 8 27 0.3638 0.0094 2 8 28 -0.2405 -0.0050 2 8 29 -1.9492 0.0065 2 8 30 0.3822 0.0079 2 8 31 -1.4206 -0.0009 2 8 32 0.4786 0.0008 2 8 33 1.7337 -0.0202 2 8 34 0.6809 0.0128 2 8 35 -0.1933 -0.0205 2 9 0 -1.0204 -0.0131 2 9 1 0.1318 0.0035 2 9 2 1.5470 -0.0050 2 9 3 -0.5755 0.0018 2 9 4 0.0262 0.0138 2 9 5 -1.4559 0.0002 2 9 6 -0.4251 0.0007 2 9 7 -0.9946 0.0044 2 9 8 0.1573 -0.0059 2 9 9 1.3450 0.0076 2 9 10 0.5917 -0.0045 2 9 11 0.4259 0.0050 2 9 12 -0.5817 -0.0092 2 9 13 -0.2807 0.0005 2 9 14 -0.2614 0.0085 2 9 15 -0.7878 -0.0022 2 9 16 1.8342 0.0043 2 9 17 -0.3738 0.0090 2 9 18 0.9386 -0.0054 2 9 19 0.8216 0.0126 2 9 20 0.5431 0.0008 2 9 21 0.8383 0.0016 2 9 22 -1.7139 0.0161 2 9 23 0.3147 -0.0166 2 9 24 -1.5614 0.0073 2 9 25 -0.1119 -0.0107 2 9 26 0.5016 0.0082 2 9 27 -0.0711 -0.0057 2 9 28 0.9959 -0.0062 2 9 29 1.9492 -0.0015 2 9 30 0.2212 -0.0004 2 9 31 -1.1820 0.0039 2 9 32 -2.8813 -0.0139 2 9 33 -2.4695 0.0108 2 10 0 -0.4180 -0.0070 2 10 1 -0.6442 -0.0055 2 10 2 0.3090 -0.0025 2 10 3 0.5788 0.0049 2 10 4 1.8100 -0.0008 2 10 5 2.0041 0.0076 2 10 6 0.3905 0.0028 2 10 7 -0.7320 -0.0044 2 10 8 -1.1034 0.0005 2 10 9 -0.2663 -0.0013 2 10 10 1.2621 0.0008 2 10 11 2.0787 0.0012 2 10 12 -0.5968 -0.0019 2 10 13 0.0632 0.0104 2 10 14 -1.3427 -0.0064 2 10 15 -0.3077 0.0018 2 10 16 -0.0245 -0.0080 2 10 17 -0.3604 0.0056 2 10 18 0.1710 -0.0048 2 10 19 -0.7779 0.0050 2 10 20 0.7621 -0.0095 2 10 21 2.6143 0.0065 2 10 22 1.0413 -0.0086 2 10 23 0.9728 0.0012 2 10 24 -0.7248 -0.0058 2 10 25 -1.9024 0.0044 2 10 26 -2.8075 -0.0016 2 10 27 -2.7091 -0.0240 2 10 28 -0.1583 0.0057 2 10 29 -0.6746 -0.0101 2 10 30 1.9090 0.0126 2 10 31 0.4679 0.0017 2 11 0 -0.6661 0.0044 2 11 1 0.2446 0.0001 2 11 2 0.4971 -0.0023 2 11 3 -1.3210 0.0015 2 11 4 0.9211 0.0001 2 11 5 0.7317 0.0068 2 11 6 0.7947 -0.0022 2 11 7 0.4660 0.0019 2 11 8 0.2749 0.0014 2 11 9 -0.9661 -0.0145 2 11 10 0.4649 0.0073 2 11 11 0.0442 -0.0150 2 11 12 1.3347 0.0101 2 11 13 -0.0245 0.0075 2 11 14 -0.3447 0.0091 2 11 15 -0.1369 0.0013 2 11 16 -0.2907 0.0002 2 11 17 -0.2633 0.0023 2 11 18 0.2939 -0.0044 2 11 19 0.2632 -0.0051 2 11 20 -1.1153 0.0008 2 11 21 0.3146 0.0029 2 11 22 -0.2796 -0.0020 2 11 23 2.3588 0.0109 2 11 24 1.0644 0.0017 2 11 25 1.7497 0.0053 2 11 26 -0.5291 -0.0044 2 11 27 -0.1566 0.0057 2 11 28 -0.9051 -0.0100 2 11 29 -0.2823 -0.0129 2 12 0 -1.6138 -0.0034 2 12 1 -0.3107 0.0003 2 12 2 -1.4797 -0.0012 2 12 3 -0.8222 -0.0017 2 12 4 -0.4923 -0.0004 2 12 5 0.4347 0.0050 2 12 6 1.0620 -0.0010 2 12 7 0.0946 0.0022 2 12 8 0.1655 0.0060 2 12 9 0.0568 0.0052 2 12 10 0.7448 -0.0060 2 12 11 -0.2344 -0.0106 2 12 12 1.6234 0.0026 2 12 13 2.0061 0.0036 2 12 14 0.7740 -0.0096 2 12 15 1.5141 -0.0013 2 12 16 0.3675 0.0036 2 12 17 -0.8314 -0.0073 2 12 18 0.3670 0.0044 2 12 19 0.3819 0.0115 2 12 20 -0.0854 -0.0046 2 12 21 0.5012 -0.0105 2 12 22 -0.8717 -0.0043 2 12 23 -0.4926 0.0092 2 12 24 0.1904 -0.0134 2 12 25 -0.7649 0.0061 2 12 26 0.1567 -0.0208 2 12 27 -0.3740 0.0008 2 12 28 -0.8609 -0.0098 2 12 29 -0.7779 0.0096 2 13 0 1.4215 -0.0031 2 13 1 1.1428 0.0022 2 13 2 0.5136 0.0023 2 13 3 -0.1800 -0.0022 2 13 4 -0.4905 0.0013 2 13 5 0.2281 0.0002 2 13 6 -0.0523 0.0039 2 13 7 0.3217 -0.0053 2 13 8 0.3349 0.0099 2 13 9 -1.7703 -0.0083 2 13 10 -0.2428 0.0080 2 13 11 -2.8335 0.0136 2 13 12 1.0075 -0.0003 2 13 13 -0.5288 -0.0049 2 13 14 1.0988 0.0179 2 13 15 2.4930 -0.0039 2 13 16 -3.0386 -0.0004 2 13 17 2.2360 -0.0033 2 13 18 0.1560 0.0005 2 13 19 1.0098 -0.0045 2 13 20 2.2592 0.0049 2 13 21 0.7655 0.0083 2 13 22 -1.0701 0.0012 2 13 23 0.6591 -0.0024 2 13 24 1.0001 0.0095 2 13 25 0.6132 -0.0060 2 13 26 1.1956 -0.0125 2 13 27 -0.8385 0.0213 2 14 0 -0.2881 0.0044 2 14 1 -0.6831 -0.0103 2 14 2 -1.3448 0.0103 2 14 3 -1.8867 0.0102 2 14 4 0.6482 0.0026 2 14 5 -0.0911 -0.0031 2 14 6 -0.1803 -0.0000 2 14 7 1.0356 0.0064 2 14 8 1.9114 0.0006 2 14 9 -0.0808 -0.0114 2 14 10 1.1690 -0.0083 2 14 11 -1.4357 -0.0030 2 14 12 1.2751 0.0064 2 14 13 -1.8988 -0.0083 2 14 14 2.2562 0.0091 2 14 15 1.1651 -0.0056 2 14 16 -2.1698 0.0117 2 14 17 0.3916 -0.0121 2 15 0 -0.4088 0.0098 2 15 1 2.5296 0.0004 3 0 0 -57.1631 0.5283 3 0 2 7.1000 -0.2883 3 0 4 56.0720 -0.0991 3 0 6 9.7406 -0.0334 3 0 8 -27.5899 -0.0335 3 0 10 -2.2877 -0.0086 3 0 12 10.3231 -0.0293 3 0 14 -3.5637 -0.0241 3 0 16 -8.2232 -0.0299 3 0 18 0.6257 0.0064 3 0 20 5.9333 -0.0298 3 0 22 1.2385 0.0144 3 0 24 -4.9114 0.0078 3 0 26 0.0208 0.0035 3 0 28 5.1620 0.0090 3 0 30 1.7474 0.0094 3 0 32 -2.4849 0.0047 3 0 34 -1.4456 0.0089 3 0 36 -0.1073 0.0101 3 0 38 2.5264 -0.0025 3 0 40 1.2811 0.0064 3 0 42 0.2295 0.0007 3 0 44 -0.5397 0.0109 3 1 0 -7.8584 0.1939 3 1 1 -17.7929 -0.1550 3 1 2 -35.7660 0.0858 3 1 3 -27.5251 -0.0008 3 1 4 -2.0594 -0.0345 3 1 5 -2.6312 0.0586 3 1 6 24.7253 0.0080 3 1 7 6.6121 0.0006 3 1 8 -1.2537 -0.0098 3 1 9 6.3352 0.0716 3 1 10 -12.8660 0.0057 3 1 11 4.5692 0.0131 3 1 12 4.8880 -0.0123 3 1 13 1.5601 0.0355 3 1 14 7.2262 0.0071 3 1 15 -0.0898 0.0101 3 1 16 -2.1922 -0.0042 3 1 17 2.4218 0.0062 3 1 18 -6.4615 -0.0086 3 1 19 1.8950 0.0143 3 1 20 1.3334 -0.0124 3 1 21 1.1093 0.0024 3 1 22 2.3488 -0.0055 3 1 23 -0.6794 -0.0032 3 1 24 0.8309 -0.0013 3 1 25 0.1245 -0.0065 3 1 26 -2.7982 -0.0049 3 1 27 -1.2151 -0.0052 3 1 28 0.9428 0.0075 3 1 29 -0.9096 -0.0041 3 1 30 1.0070 0.0012 3 1 31 -0.9955 -0.0019 3 1 32 -0.4345 0.0042 3 1 33 -0.6774 -0.0125 3 1 34 -0.5632 -0.0006 3 1 35 0.9712 -0.0019 3 1 36 -1.3906 0.0030 3 1 37 -0.8045 -0.0018 3 1 38 1.5494 0.0021 3 1 39 -0.4467 -0.0108 3 1 40 0.3086 0.0076 3 1 41 0.2612 0.0098 3 1 42 -0.6499 -0.0014 3 1 43 -0.2672 -0.0109 3 1 44 -0.1374 -0.0012 3 2 0 12.2669 0.0414 3 2 1 18.2613 0.0036 3 2 2 6.7769 0.0039 3 2 3 -17.8882 0.0272 3 2 4 -0.3704 -0.0161 3 2 5 -13.8054 -0.0386 3 2 6 4.4424 0.0332 3 2 7 4.9143 -0.0705 3 2 8 1.3312 -0.0117 3 2 9 1.9035 0.0036 3 2 10 -6.0374 -0.0362 3 2 11 -2.0692 0.0136 3 2 12 -3.9160 -0.0118 3 2 13 -0.2257 -0.0015 3 2 14 1.6251 -0.0187 3 2 15 0.8358 0.0169 3 2 16 3.6151 -0.0067 3 2 17 -0.2070 0.0084 3 2 18 -0.6029 0.0061 3 2 19 1.4256 0.0010 3 2 20 0.2351 -0.0025 3 2 21 0.7028 0.0080 3 2 22 -0.5165 0.0033 3 2 23 -1.2933 0.0037 3 2 24 -1.5607 -0.0043 3 2 25 1.7262 0.0026 3 2 26 0.0636 -0.0098 3 2 27 2.4619 0.0039 3 2 28 0.7054 0.0112 3 2 29 0.6592 -0.0019 3 2 30 3.3664 0.0045 3 2 31 -1.8245 0.0003 3 2 32 -0.7762 -0.0044 3 2 33 -0.5592 -0.0029 3 2 34 -0.6972 -0.0013 3 2 35 -0.2864 -0.0058 3 2 36 -0.2300 0.0077 3 2 37 0.2985 0.0043 3 2 38 -2.2083 -0.0002 3 2 39 -2.0417 -0.0026 3 2 40 2.5837 0.0090 3 2 41 0.6911 -0.0015 3 2 42 0.0182 -0.0012 3 2 43 2.6874 0.0334 3 2 44 -2.1383 -0.0180 3 2 45 -0.2463 -0.0028 3 3 0 -1.6022 -0.0114 3 3 1 7.1127 -0.0050 3 3 2 -1.3711 0.0083 3 3 3 -7.0119 0.0111 3 3 4 -3.0313 -0.0088 3 3 5 -9.9202 -0.0231 3 3 6 -2.1916 -0.0030 3 3 7 -0.4397 -0.0013 3 3 8 1.0226 0.0094 3 3 9 3.8876 0.0117 3 3 10 -0.5674 -0.0139 3 3 11 1.4804 -0.0145 3 3 12 -0.5618 0.0252 3 3 13 -0.4490 -0.0105 3 3 14 -0.7603 -0.0031 3 3 15 2.0355 0.0125 3 3 16 -1.1650 -0.0014 3 3 17 -1.8275 0.0038 3 3 18 -1.0242 -0.0130 3 3 19 -0.4187 0.0112 3 3 20 1.2237 -0.0113 3 3 21 1.1903 0.0098 3 3 22 2.9880 -0.0012 3 3 23 -0.5748 -0.0013 3 3 24 0.2514 0.0046 3 3 25 -1.8385 -0.0003 3 3 26 -0.5061 -0.0081 3 3 27 0.5985 0.0019 3 3 28 -0.6815 -0.0004 3 3 29 3.6086 -0.0096 3 3 30 0.0549 0.0068 3 3 31 1.3047 0.0025 3 3 32 0.4896 0.0017 3 3 33 -2.5713 0.0037 3 3 34 -0.0285 -0.0048 3 3 35 -0.4531 -0.0055 3 3 36 0.8507 0.0022 3 3 37 -0.4641 -0.0037 3 3 38 -0.3689 0.0051 3 3 39 -1.0301 -0.0194 3 3 40 0.6753 0.0009 3 3 41 -1.7850 -0.0129 3 3 42 0.8851 0.0239 3 3 43 0.0911 0.0173 3 3 44 -0.8410 -0.0128 3 3 45 2.3102 0.0007 3 4 0 -1.3314 -0.0254 3 4 1 1.3439 0.0261 3 4 2 9.6695 -0.0304 3 4 3 -3.4284 0.0089 3 4 4 3.5811 0.0142 3 4 5 -1.0238 -0.0029 3 4 6 -1.8166 -0.0012 3 4 7 2.7836 0.0183 3 4 8 -3.1558 0.0019 3 4 9 0.0262 -0.0008 3 4 10 -0.4848 -0.0015 3 4 11 -2.7777 0.0007 3 4 12 -2.8439 0.0050 3 4 13 0.6904 -0.0069 3 4 14 -0.2306 0.0116 3 4 15 1.8769 -0.0016 3 4 16 0.0368 0.0066 3 4 17 1.4154 -0.0053 3 4 18 -0.5134 0.0053 3 4 19 0.1273 -0.0062 3 4 20 -0.1515 -0.0029 3 4 21 0.1000 0.0027 3 4 22 -0.8506 -0.0066 3 4 23 -0.1361 0.0037 3 4 24 0.1101 -0.0053 3 4 25 -1.7808 0.0027 3 4 26 -0.8824 -0.0012 3 4 27 -0.8828 -0.0004 3 4 28 1.1147 0.0035 3 4 29 0.4463 0.0005 3 4 30 0.1055 0.0022 3 4 31 1.2313 0.0079 3 4 32 -1.4709 -0.0054 3 4 33 1.7135 -0.0016 3 4 34 -0.6180 0.0038 3 4 35 1.7530 -0.0098 3 4 36 -1.6316 -0.0068 3 4 37 0.3428 -0.0004 3 4 38 -0.7509 -0.0023 3 4 39 0.2867 -0.0162 3 4 40 2.9585 -0.0102 3 5 0 -2.9438 0.0140 3 5 1 2.8959 -0.0086 3 5 2 0.2650 0.0101 3 5 3 -3.5637 0.0038 3 5 4 2.1337 -0.0005 3 5 5 -9.7492 0.0065 3 5 6 0.6545 -0.0205 3 5 7 0.6716 0.0154 3 5 8 -0.3330 -0.0196 3 5 9 4.6478 0.0017 3 5 10 -0.0867 -0.0079 3 5 11 -0.7874 -0.0116 3 5 12 -0.7920 -0.0074 3 5 13 -2.0962 -0.0026 3 5 14 -0.3247 -0.0003 3 5 15 0.6807 0.0026 3 5 16 -0.5513 -0.0059 3 5 17 0.0419 0.0005 3 5 18 0.4551 0.0066 3 5 19 0.6019 0.0032 3 5 20 0.2955 0.0103 3 5 21 -0.0005 0.0002 3 5 22 1.5672 0.0069 3 5 23 0.7768 -0.0003 3 5 24 0.5932 -0.0007 3 5 25 -0.6356 -0.0002 3 5 26 -0.1236 0.0084 3 5 27 -1.3873 -0.0060 3 5 28 1.5506 -0.0068 3 5 29 2.8207 -0.0031 3 5 30 1.3638 0.0040 3 5 31 1.5685 -0.0032 3 5 32 -0.5651 -0.0034 3 5 33 1.5964 0.0017 3 5 34 -0.6689 -0.0062 3 5 35 -0.3916 -0.0035 3 5 36 -2.1245 0.0131 3 5 37 -2.9520 0.0009 3 5 38 -2.1815 -0.0115 3 5 39 1.2944 -0.0048 3 6 0 0.1498 0.0066 3 6 1 2.9392 -0.0005 3 6 2 0.4516 -0.0098 3 6 3 4.5899 0.0064 3 6 4 0.8005 0.0019 3 6 5 -1.3526 -0.0074 3 6 6 1.4629 0.0110 3 6 7 -4.1260 -0.0031 3 6 8 -0.4669 0.0029 3 6 9 2.2457 0.0100 3 6 10 -1.7552 0.0075 3 6 11 2.6321 -0.0020 3 6 12 -1.2872 -0.0144 3 6 13 -0.1854 0.0183 3 6 14 -0.3587 -0.0107 3 6 15 -1.7001 0.0011 3 6 16 1.2980 -0.0022 3 6 17 0.3299 -0.0014 3 6 18 -1.2164 0.0057 3 6 19 0.8117 -0.0017 3 6 20 -1.6067 -0.0061 3 6 21 0.4127 0.0019 3 6 22 -0.0398 0.0084 3 6 23 -0.0890 -0.0047 3 6 24 2.2605 0.0017 3 6 25 -1.4949 0.0004 3 6 26 1.1181 -0.0058 3 6 27 -2.2302 0.0034 3 6 28 -1.1866 -0.0019 3 6 29 -1.3673 -0.0009 3 6 30 -1.1942 -0.0035 3 6 31 0.6597 -0.0065 3 6 32 -0.7483 0.0100 3 6 33 5.3251 -0.0084 3 6 34 -0.8135 0.0000 3 6 35 6.0482 0.0065 3 6 36 -1.2580 0.0021 3 6 37 0.2673 -0.0093 3 6 38 2.4693 -0.0095 3 7 0 0.4398 -0.0023 3 7 1 -1.5874 -0.0040 3 7 2 0.7271 0.0003 3 7 3 -0.8087 -0.0022 3 7 4 0.5737 0.0020 3 7 5 2.0112 0.0004 3 7 6 0.4994 -0.0001 3 7 7 -0.3603 -0.0013 3 7 8 0.5111 0.0035 3 7 9 -1.1968 0.0012 3 7 10 1.0471 0.0109 3 7 11 1.8975 -0.0056 3 7 12 0.9759 0.0051 3 7 13 1.0490 0.0107 3 7 14 -1.7662 -0.0010 3 7 15 -1.5564 -0.0041 3 7 16 0.0225 -0.0047 3 7 17 -0.1137 0.0009 3 7 18 1.6900 -0.0115 3 7 19 0.7820 0.0079 3 7 20 -0.8178 -0.0114 3 7 21 1.2387 -0.0074 3 7 22 -0.7120 0.0025 3 7 23 1.9594 -0.0047 3 7 24 0.2261 0.0124 3 7 25 0.1498 -0.0029 3 7 26 2.7416 0.0085 3 7 27 -3.1813 -0.0060 3 7 28 3.6818 0.0047 3 7 29 -0.0753 -0.0004 3 7 30 -0.7669 0.0013 3 7 31 0.6652 0.0127 3 7 32 -1.3396 0.0047 3 7 33 -0.8134 -0.0068 3 7 34 1.8765 0.0038 3 7 35 2.8238 -0.0003 3 7 36 -2.8578 -0.0111 3 8 0 1.9840 -0.0127 3 8 1 -0.1558 0.0130 3 8 2 0.4473 -0.0015 3 8 3 -0.7416 -0.0033 3 8 4 0.1861 0.0042 3 8 5 0.9793 -0.0030 3 8 6 -0.7671 -0.0053 3 8 7 1.9313 -0.0055 3 8 8 -0.9849 -0.0022 3 8 9 0.6215 -0.0011 3 8 10 -1.3061 -0.0073 3 8 11 -1.1298 0.0015 3 8 12 1.1708 0.0075 3 8 13 -0.2972 -0.0054 3 8 14 1.8849 0.0063 3 8 15 -0.1916 -0.0107 3 8 16 0.4251 0.0045 3 8 17 -0.4949 0.0004 3 8 18 -0.3740 -0.0025 3 8 19 0.8454 0.0063 3 8 20 -0.3644 -0.0002 3 8 21 -0.9111 -0.0003 3 8 22 -0.6097 -0.0021 3 8 23 -0.3544 0.0068 3 8 24 0.1381 -0.0097 3 8 25 1.3952 0.0166 3 8 26 -0.1777 -0.0057 3 8 27 -0.2696 -0.0033 3 8 28 0.8440 0.0129 3 8 29 -0.4206 -0.0157 3 8 30 0.9724 0.0078 3 8 31 1.3255 -0.0094 3 8 32 -1.4333 -0.0031 3 8 33 0.0524 -0.0194 3 8 34 1.0527 0.0019 3 9 0 1.0678 -0.0037 3 9 1 -0.7765 0.0059 3 9 2 0.8776 -0.0028 3 9 3 -0.1710 0.0031 3 9 4 -0.3378 -0.0019 3 9 5 -1.4300 0.0034 3 9 6 -1.0528 -0.0063 3 9 7 0.3646 0.0051 3 9 8 -0.3832 0.0007 3 9 9 2.0572 0.0012 3 9 10 -0.0469 -0.0067 3 9 11 0.9656 0.0070 3 9 12 -1.2719 -0.0013 3 9 13 0.3646 -0.0003 3 9 14 0.0705 0.0063 3 9 15 0.2583 -0.0091 3 9 16 0.6865 0.0027 3 9 17 -0.3625 0.0004 3 9 18 0.6731 -0.0038 3 9 19 0.6970 0.0010 3 9 20 -0.9867 0.0089 3 9 21 1.2310 -0.0140 3 9 22 -1.3586 0.0020 3 9 23 0.3151 -0.0120 3 9 24 2.1592 -0.0001 3 9 25 -0.2909 0.0032 3 9 26 2.5101 -0.0127 3 9 27 0.1720 0.0101 3 9 28 1.1723 -0.0207 3 9 29 -0.1666 0.0123 3 9 30 -1.1758 0.0156 3 9 31 -1.6812 0.0085 3 9 32 -2.3529 0.0062 3 10 0 -0.0297 0.0039 3 10 1 -0.2764 -0.0004 3 10 2 1.4378 -0.0017 3 10 3 1.5383 0.0095 3 10 4 0.8567 -0.0067 3 10 5 -0.3724 -0.0005 3 10 6 -1.2307 -0.0041 3 10 7 -2.1663 -0.0038 3 10 8 0.5530 -0.0009 3 10 9 -0.5040 -0.0063 3 10 10 0.6625 0.0017 3 10 11 0.0451 0.0071 3 10 12 -0.2163 -0.0001 3 10 13 -1.2592 0.0105 3 10 14 0.0509 -0.0082 3 10 15 -0.5414 0.0098 3 10 16 -0.3843 0.0030 3 10 17 -0.8800 -0.0071 3 10 18 -0.1551 0.0112 3 10 19 1.2629 -0.0120 3 10 20 0.2519 -0.0007 3 10 21 1.6551 -0.0014 3 10 22 -1.1865 0.0006 3 10 23 -0.4970 -0.0071 3 10 24 -2.5165 0.0098 3 10 25 -0.9737 -0.0120 3 10 26 -0.1636 0.0117 3 10 27 0.0887 -0.0092 3 10 28 1.9945 0.0025 3 10 29 3.1556 0.0186 3 10 30 1.4109 -0.0002 3 11 0 -0.5637 0.0039 3 11 1 -0.8763 -0.0009 3 11 2 -0.3441 0.0028 3 11 3 0.0297 0.0041 3 11 4 0.2136 -0.0016 3 11 5 1.2837 0.0002 3 11 6 0.3451 -0.0058 3 11 7 -0.0358 0.0009 3 11 8 -1.6747 -0.0026 3 11 9 -0.3787 -0.0114 3 11 10 -0.8946 -0.0028 3 11 11 0.2991 0.0050 3 11 12 0.5408 -0.0054 3 11 13 0.0133 0.0125 3 11 14 -0.6261 -0.0066 3 11 15 -1.6800 0.0073 3 11 16 0.7921 -0.0114 3 11 17 -0.1592 0.0092 3 11 18 -0.2439 -0.0074 3 11 19 -0.1850 0.0048 3 11 20 -1.1568 0.0076 3 11 21 0.7606 0.0112 3 11 22 1.0628 -0.0019 3 11 23 0.8930 0.0087 3 11 24 1.4154 -0.0008 3 11 25 -0.9028 -0.0118 3 11 26 0.0129 -0.0020 3 11 27 -1.9928 -0.0194 3 11 28 0.5927 -0.0115 3 12 0 -0.2693 0.0019 3 12 1 -1.5021 -0.0032 3 12 2 0.0910 0.0021 3 12 3 0.2771 0.0059 3 12 4 0.7845 -0.0049 3 12 5 -0.4809 -0.0077 3 12 6 0.8290 0.0091 3 12 7 -0.9391 -0.0081 3 12 8 0.0610 0.0051 3 12 9 -1.0957 0.0051 3 12 10 -0.3077 -0.0013 3 12 11 1.1994 -0.0032 3 12 12 -0.2570 0.0002 3 12 13 2.2866 -0.0028 3 12 14 -0.3770 -0.0004 3 12 15 -1.4357 -0.0031 3 12 16 -1.3631 0.0094 3 12 17 -0.9164 0.0114 3 12 18 -0.0002 0.0015 3 12 19 -0.0283 0.0021 3 12 20 -1.2141 -0.0049 3 12 21 -0.4828 0.0062 3 12 22 -2.0055 -0.0027 3 12 23 -0.0673 0.0184 3 12 24 0.0242 -0.0136 3 12 25 0.3505 0.0048 3 12 26 0.3574 0.0251 3 12 27 1.0858 0.0094 3 12 28 0.0564 0.0158 3 13 0 0.1981 0.0083 3 13 1 -0.2004 0.0052 3 13 2 -0.8779 0.0171 3 13 3 -1.2487 0.0127 3 13 4 0.5451 0.0089 3 13 5 1.2189 0.0129 3 13 6 0.1873 -0.0109 3 13 7 -1.1910 -0.0096 3 13 8 -0.3620 -0.0020 3 13 9 -3.1672 -0.0051 3 13 10 0.0264 -0.0030 3 13 11 -1.9926 0.0010 3 13 12 1.0011 0.0034 3 13 13 1.1033 -0.0091 3 13 14 -1.4956 0.0083 3 13 15 2.1552 -0.0024 3 13 16 -0.8836 -0.0114 3 13 17 -0.4498 0.0007 3 13 18 1.4625 0.0114 3 13 19 -0.3195 0.0135 3 13 20 -0.0078 -0.0025 3 13 21 -1.1393 0.0145 3 13 22 0.4618 0.0001 3 13 23 -0.6271 -0.0040 3 13 24 0.8055 -0.0138 3 13 25 -2.3574 -0.0170 3 13 26 -1.0056 -0.0239 3 13 27 0.5276 0.0137 3 13 28 0.1418 0.0014 3 14 0 0.1356 0.0029 3 14 1 1.0462 -0.0150 3 14 2 -0.0230 0.0020 3 14 3 0.4055 0.0016 3 14 4 0.2746 -0.0016 3 14 5 1.3914 0.0121 3 14 6 1.3577 0.0046 3 14 7 1.4262 0.0040 3 14 8 -0.1318 -0.0164 3 14 9 0.1489 0.0069 3 14 10 -1.7840 -0.0100 3 14 11 -2.0940 -0.0064 3 14 12 0.2050 -0.0006 3 14 13 -0.7495 -0.0045 3 14 14 -0.0998 -0.0045 3 14 15 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0.1778 4 1 4 10.7502 -0.0084 4 1 5 9.0610 0.0257 4 1 6 1.4647 -0.0068 4 1 7 0.0904 0.0534 4 1 8 -5.3344 -0.0085 4 1 9 -3.8509 0.0149 4 1 10 2.9212 -0.0056 4 1 11 1.0667 -0.0248 4 1 12 2.3532 -0.0018 4 1 13 0.5557 0.0085 4 1 14 -0.5303 0.0036 4 1 15 0.5558 -0.0156 4 1 16 -5.4088 -0.0169 4 1 17 -0.2597 -0.0015 4 1 18 1.4080 0.0026 4 1 19 0.3899 -0.0099 4 1 20 3.2022 -0.0037 4 1 21 0.5236 -0.0066 4 1 22 0.0166 0.0039 4 1 23 -0.6983 -0.0129 4 1 24 -2.1697 -0.0071 4 1 25 -2.0956 -0.0103 4 1 26 -1.3987 0.0076 4 1 27 -1.1087 -0.0157 4 1 28 0.8166 0.0046 4 1 29 2.3137 -0.0026 4 1 30 -0.6861 0.0021 4 1 31 0.1233 0.0003 4 1 32 0.5354 0.0004 4 1 33 0.0689 -0.0095 4 1 34 -1.1330 -0.0073 4 1 35 1.2846 0.0064 4 1 36 -0.0080 -0.0059 4 1 37 -0.3087 -0.0044 4 1 38 -0.2224 -0.0030 4 1 39 -1.1622 0.0006 4 1 40 -0.5740 -0.0048 4 1 41 -0.4354 -0.0024 4 1 42 -0.3594 -0.0015 4 1 43 -0.4421 -0.0013 4 1 44 1.3002 0.0023 4 2 0 16.0476 -0.0153 4 2 1 -5.2567 0.0056 4 2 2 2.0457 -0.0448 4 2 3 -8.1839 -0.0348 4 2 4 -1.1434 0.0069 4 2 5 9.9345 -0.0466 4 2 6 -2.0793 -0.0072 4 2 7 6.4960 0.0202 4 2 8 -4.3270 -0.0482 4 2 9 -5.8869 0.0389 4 2 10 -0.6532 -0.0142 4 2 11 -3.6255 0.0012 4 2 12 -1.0203 -0.0033 4 2 13 1.9736 0.0066 4 2 14 1.1475 -0.0054 4 2 15 1.2643 0.0087 4 2 16 -0.4532 0.0081 4 2 17 -1.5043 -0.0041 4 2 18 -2.1670 0.0075 4 2 19 -1.1744 0.0069 4 2 20 1.0285 0.0033 4 2 21 -1.7731 0.0050 4 2 22 0.0976 0.0103 4 2 23 1.8147 -0.0021 4 2 24 0.1855 -0.0059 4 2 25 0.0793 0.0002 4 2 26 -0.1201 0.0018 4 2 27 -0.9624 -0.0042 4 2 28 2.4516 0.0121 4 2 29 -0.6549 -0.0112 4 2 30 0.6699 0.0071 4 2 31 0.6566 0.0049 4 2 32 -2.2159 0.0024 4 2 33 -0.2541 -0.0076 4 2 34 0.3791 0.0075 4 2 35 0.7981 -0.0087 4 2 36 -1.6587 0.0052 4 2 37 0.1176 0.0011 4 2 38 0.3926 -0.0022 4 2 39 -0.3872 -0.0122 4 2 40 2.3416 0.0030 4 2 41 1.4202 0.0157 4 2 42 -0.3856 -0.0123 4 2 43 -0.9007 0.0033 4 2 44 -0.0683 -0.0111 4 3 0 8.0756 -0.0103 4 3 1 -5.8824 0.0137 4 3 2 2.1931 0.0143 4 3 3 -5.2601 -0.0185 4 3 4 -2.9155 -0.0115 4 3 5 4.5347 -0.0006 4 3 6 1.0739 0.0332 4 3 7 6.2287 0.0229 4 3 8 1.5322 0.0002 4 3 9 1.4377 -0.0036 4 3 10 0.6216 0.0126 4 3 11 -2.2816 -0.0091 4 3 12 -1.3998 0.0008 4 3 13 1.4007 0.0192 4 3 14 -2.9476 -0.0119 4 3 15 0.3206 0.0005 4 3 16 0.4275 -0.0069 4 3 17 0.4413 -0.0055 4 3 18 1.0089 -0.0078 4 3 19 1.0621 0.0014 4 3 20 0.3965 -0.0040 4 3 21 -0.8245 -0.0065 4 3 22 -0.0567 0.0022 4 3 23 -0.7438 -0.0020 4 3 24 -0.0651 0.0033 4 3 25 -0.2579 0.0032 4 3 26 -1.5312 -0.0026 4 3 27 0.4811 -0.0076 4 3 28 -1.2397 0.0011 4 3 29 0.7156 -0.0012 4 3 30 0.9008 -0.0006 4 3 31 -0.5393 0.0073 4 3 32 0.0494 0.0084 4 3 33 0.1817 -0.0019 4 3 34 0.1715 -0.0042 4 3 35 1.0102 0.0010 4 3 36 -0.3479 0.0053 4 3 37 0.3180 -0.0081 4 3 38 -0.3964 0.0085 4 3 39 -0.7818 -0.0166 4 3 40 0.6507 0.0081 4 3 41 -0.5905 0.0142 4 3 42 0.0669 0.0064 4 4 0 8.6068 -0.0260 4 4 1 -2.4567 0.0252 4 4 2 8.1830 0.0180 4 4 3 -2.8120 -0.0105 4 4 4 -1.4580 0.0125 4 4 5 3.3946 0.0124 4 4 6 -2.2699 -0.0049 4 4 7 3.5156 0.0004 4 4 8 1.8859 0.0070 4 4 9 -1.2429 -0.0163 4 4 10 0.3005 0.0014 4 4 11 -1.2625 -0.0047 4 4 12 0.4454 0.0019 4 4 13 0.9426 0.0005 4 4 14 -0.8060 -0.0065 4 4 15 0.6500 0.0046 4 4 16 -1.7288 -0.0058 4 4 17 -0.2151 -0.0034 4 4 18 2.0913 0.0011 4 4 19 -1.0023 0.0012 4 4 20 -0.5975 0.0020 4 4 21 -0.9477 0.0016 4 4 22 -0.5136 -0.0057 4 4 23 -1.4644 0.0031 4 4 24 -0.4825 0.0026 4 4 25 0.2881 0.0010 4 4 26 0.7299 0.0012 4 4 27 0.0280 0.0000 4 4 28 0.1721 0.0014 4 4 29 -0.4594 -0.0036 4 4 30 -1.8123 -0.0068 4 4 31 0.4189 0.0062 4 4 32 -0.5989 -0.0000 4 4 33 1.6292 -0.0108 4 4 34 0.1321 0.0065 4 4 35 -0.0240 -0.0104 4 4 36 -0.7201 -0.0058 4 4 37 -0.9188 0.0123 4 4 38 2.3142 0.0026 4 4 39 -2.5776 -0.0051 4 4 40 2.7501 0.0083 4 5 0 -3.5613 0.0147 4 5 1 1.0862 -0.0045 4 5 2 -0.1842 -0.0138 4 5 3 -5.8133 0.0035 4 5 4 0.6234 -0.0157 4 5 5 -1.0825 0.0067 4 5 6 -1.3652 -0.0107 4 5 7 5.0947 -0.0011 4 5 8 0.6122 0.0074 4 5 9 1.9581 -0.0123 4 5 10 0.7078 0.0014 4 5 11 -0.2032 -0.0060 4 5 12 0.9591 0.0078 4 5 13 0.6544 0.0010 4 5 14 -1.0738 0.0026 4 5 15 0.3402 -0.0052 4 5 16 -0.7244 0.0065 4 5 17 1.0546 0.0023 4 5 18 -0.0778 0.0017 4 5 19 0.7715 0.0055 4 5 20 1.0762 -0.0009 4 5 21 0.2641 -0.0069 4 5 22 1.0389 -0.0030 4 5 23 0.0330 -0.0039 4 5 24 -0.9375 0.0033 4 5 25 -1.5952 0.0060 4 5 26 -0.0470 0.0005 4 5 27 1.6643 0.0063 4 5 28 0.6792 -0.0078 4 5 29 1.3062 -0.0005 4 5 30 -1.0056 0.0080 4 5 31 0.0983 0.0010 4 5 32 -3.0392 -0.0077 4 5 33 2.8404 0.0185 4 5 34 -2.2304 0.0037 4 5 35 0.0373 -0.0028 4 5 36 -0.3763 0.0046 4 5 37 -1.5859 0.0000 4 5 38 0.8283 -0.0047 4 5 39 -1.1620 0.0003 4 6 0 0.7888 -0.0020 4 6 1 1.0218 0.0053 4 6 2 0.3338 -0.0090 4 6 3 -0.2731 -0.0081 4 6 4 -0.1845 0.0142 4 6 5 -3.7145 -0.0076 4 6 6 -0.6659 -0.0008 4 6 7 0.1227 0.0181 4 6 8 -0.9594 0.0039 4 6 9 0.9700 0.0055 4 6 10 0.7145 -0.0084 4 6 11 -0.3513 0.0168 4 6 12 1.3757 -0.0106 4 6 13 -1.3138 0.0055 4 6 14 1.2808 0.0054 4 6 15 -0.0143 -0.0190 4 6 16 -0.6513 0.0128 4 6 17 0.9643 -0.0109 4 6 18 -0.8151 0.0021 4 6 19 -0.7722 -0.0055 4 6 20 -0.9016 -0.0055 4 6 21 0.1656 -0.0017 4 6 22 0.0851 0.0000 4 6 23 -0.7041 -0.0118 4 6 24 1.4860 -0.0073 4 6 25 -1.3301 0.0000 4 6 26 -2.0800 0.0042 4 6 27 -0.3105 -0.0028 4 6 28 -1.3872 -0.0024 4 6 29 0.2252 0.0019 4 6 30 0.7076 0.0114 4 6 31 -0.4377 -0.0063 4 6 32 -0.1606 0.0159 4 6 33 2.1879 0.0001 4 6 34 -2.4781 -0.0135 4 6 35 4.3771 0.0077 4 6 36 -1.2808 -0.0044 4 6 37 -0.3140 0.0062 4 7 0 -1.0619 0.0033 4 7 1 -0.0612 -0.0046 4 7 2 -0.1602 0.0077 4 7 3 2.0611 -0.0014 4 7 4 -0.8013 -0.0006 4 7 5 0.8564 -0.0072 4 7 6 -1.5434 -0.0033 4 7 7 -1.4622 -0.0056 4 7 8 -0.6379 0.0004 4 7 9 0.1554 -0.0069 4 7 10 0.5749 -0.0068 4 7 11 0.7934 0.0048 4 7 12 -0.1342 -0.0046 4 7 13 -2.4552 0.0070 4 7 14 0.0336 -0.0028 4 7 15 -1.0507 -0.0058 4 7 16 1.2679 -0.0031 4 7 17 1.2649 0.0124 4 7 18 0.3783 0.0016 4 7 19 0.0878 -0.0023 4 7 20 0.8313 0.0104 4 7 21 -0.3815 -0.0078 4 7 22 -0.1895 0.0044 4 7 23 0.3549 0.0017 4 7 24 0.5052 -0.0039 4 7 25 -2.1910 0.0033 4 7 26 1.3900 -0.0000 4 7 27 -0.5556 -0.0010 4 7 28 -2.3697 -0.0013 4 7 29 3.6027 0.0134 4 7 30 -3.1058 -0.0058 4 7 31 0.2815 0.0024 4 7 32 2.0964 0.0090 4 7 33 -0.7849 -0.0173 4 7 34 1.0116 0.0011 4 7 35 0.8708 0.0003 4 7 36 -3.9752 0.0055 4 8 0 0.8629 -0.0042 4 8 1 -0.6061 0.0003 4 8 2 -0.2543 0.0080 4 8 3 0.9063 -0.0008 4 8 4 -1.7525 0.0028 4 8 5 1.2348 -0.0018 4 8 6 -0.7465 0.0035 4 8 7 0.9598 0.0014 4 8 8 -1.0331 -0.0040 4 8 9 -1.2843 0.0080 4 8 10 -0.5569 -0.0015 4 8 11 -0.0794 -0.0036 4 8 12 0.9600 0.0058 4 8 13 1.4654 -0.0083 4 8 14 0.5943 0.0053 4 8 15 -0.9481 0.0002 4 8 16 -1.1025 -0.0014 4 8 17 0.7719 0.0058 4 8 18 -1.7849 -0.0050 4 8 19 0.8053 0.0047 4 8 20 -1.0288 0.0048 4 8 21 -1.5014 -0.0018 4 8 22 0.6619 0.0024 4 8 23 -0.5796 -0.0041 4 8 24 1.1272 -0.0011 4 8 25 -0.9609 -0.0103 4 8 26 0.1849 -0.0014 4 8 27 -1.3752 -0.0167 4 8 28 0.8514 0.0038 4 8 29 -0.0497 -0.0039 4 8 30 -2.8434 -0.0019 4 8 31 -1.0422 0.0177 4 8 32 -2.7100 -0.0044 4 8 33 -0.1554 -0.0029 4 8 34 1.9111 0.0076 4 9 0 -0.5976 -0.0009 4 9 1 -0.0315 -0.0032 4 9 2 0.4681 -0.0082 4 9 3 -0.3913 0.0022 4 9 4 -0.0829 -0.0073 4 9 5 -0.5256 0.0066 4 9 6 -0.6108 0.0034 4 9 7 0.5376 -0.0060 4 9 8 1.2950 0.0075 4 9 9 -0.2825 -0.0041 4 9 10 0.2773 -0.0003 4 9 11 -1.1840 0.0027 4 9 12 -0.5525 -0.0021 4 9 13 -0.7337 -0.0068 4 9 14 0.8515 -0.0000 4 9 15 -0.7451 -0.0019 4 9 16 2.0995 0.0058 4 9 17 -0.2165 -0.0024 4 9 18 -0.1106 0.0065 4 9 19 2.0251 0.0012 4 9 20 -2.5603 -0.0026 4 9 21 1.4122 0.0019 4 9 22 0.1424 -0.0091 4 9 23 0.2402 0.0035 4 9 24 1.0579 0.0014 4 9 25 -1.0833 -0.0046 4 9 26 -1.1060 -0.0082 4 9 27 -0.5055 0.0004 4 9 28 -0.7361 0.0054 4 9 29 -1.0708 -0.0014 4 9 30 -1.0452 0.0254 4 9 31 0.7268 0.0033 4 9 32 -0.3369 0.0055 4 10 0 0.4611 0.0036 4 10 1 1.7626 0.0075 4 10 2 -0.4401 -0.0098 4 10 3 0.7888 0.0009 4 10 4 -1.4054 -0.0109 4 10 5 0.1468 0.0074 4 10 6 -0.5148 -0.0043 4 10 7 0.0162 0.0015 4 10 8 -0.5249 0.0007 4 10 9 0.4675 0.0004 4 10 10 0.2537 0.0020 4 10 11 0.2159 0.0056 4 10 12 0.4273 -0.0007 4 10 13 -0.7672 0.0042 4 10 14 -1.5055 -0.0030 4 10 15 -0.9509 0.0034 4 10 16 -0.1354 0.0023 4 10 17 0.3534 -0.0155 4 10 18 1.2832 0.0083 4 10 19 0.4336 -0.0002 4 10 20 -0.2556 0.0008 4 10 21 -0.8359 0.0128 4 10 22 -0.9930 0.0016 4 10 23 0.2229 0.0066 4 10 24 1.1774 -0.0017 4 10 25 -0.6214 0.0050 4 10 26 0.6903 -0.0043 4 10 27 1.6999 -0.0099 4 10 28 -0.8593 -0.0193 4 10 29 0.6577 -0.0057 4 11 0 0.7303 0.0064 4 11 1 -0.9317 0.0049 4 11 2 0.7115 -0.0017 4 11 3 0.9616 -0.0049 4 11 4 1.7888 -0.0076 4 11 5 0.6871 -0.0027 4 11 6 0.0538 -0.0058 4 11 7 0.4866 0.0081 4 11 8 -1.5971 -0.0036 4 11 9 -0.1149 0.0000 4 11 10 1.5862 -0.0055 4 11 11 0.4721 0.0009 4 11 12 1.5144 -0.0076 4 11 13 -0.7304 -0.0081 4 11 14 0.5828 0.0044 4 11 15 0.0774 -0.0100 4 11 16 0.2329 -0.0035 4 11 17 0.8438 0.0008 4 11 18 -0.7835 0.0045 4 11 19 1.0295 -0.0060 4 11 20 -1.0860 0.0120 4 11 21 0.5673 -0.0008 4 11 22 -0.1003 -0.0009 4 11 23 -0.5835 -0.0098 4 11 24 0.1962 0.0017 4 11 25 0.0006 -0.0028 4 11 26 0.3260 -0.0063 4 11 27 -0.5618 0.0165 4 11 28 -3.5278 -0.0069 4 11 29 2.5162 0.0048 4 12 0 0.7030 0.0030 4 12 1 -1.6541 -0.0041 4 12 2 -0.3083 -0.0035 4 12 3 0.4384 0.0041 4 12 4 0.0803 -0.0083 4 12 5 -0.1842 -0.0080 4 12 6 0.0721 0.0033 4 12 7 -0.0702 0.0101 4 12 8 0.0070 -0.0046 4 12 9 0.5594 0.0246 4 12 10 0.0869 -0.0055 4 12 11 1.5431 0.0051 4 12 12 1.3085 -0.0028 4 12 13 -1.0778 -0.0036 4 12 14 0.1180 -0.0058 4 12 15 -1.3404 0.0046 4 12 16 0.4109 -0.0008 4 12 17 -0.1331 -0.0013 4 12 18 1.7810 -0.0088 4 12 19 -0.8213 0.0010 4 12 20 0.1628 -0.0042 4 12 21 -0.0051 0.0095 4 12 22 0.1286 0.0033 4 12 23 -0.2974 -0.0163 4 12 24 0.9315 0.0140 4 12 25 1.1240 -0.0106 4 12 26 1.9128 0.0176 4 12 27 0.6237 -0.0015 4 12 28 -0.1136 -0.0421 4 12 29 -1.7706 -0.0119 4 13 0 -2.0795 0.0053 4 13 1 -2.9379 0.0039 4 13 2 0.3470 0.0065 4 13 3 0.4637 0.0026 4 13 4 -0.1575 -0.0102 4 13 5 1.7232 -0.0064 4 13 6 -1.4348 -0.0238 4 13 7 -0.6363 -0.0137 4 13 8 -0.3291 -0.0062 4 13 9 -0.3951 -0.0065 4 13 10 1.2095 -0.0022 4 13 11 -0.2627 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-0.0055 5 1 11 3.0799 -0.0139 5 1 12 -1.8543 0.0124 5 1 13 -0.2249 -0.0142 5 1 14 -2.0296 -0.0144 5 1 15 -1.5126 -0.0124 5 1 16 0.8363 -0.0012 5 1 17 -0.3954 -0.0067 5 1 18 3.1208 0.0061 5 1 19 1.7740 -0.0053 5 1 20 -1.1729 0.0075 5 1 21 0.7566 -0.0017 5 1 22 -0.4534 0.0053 5 1 23 0.2017 0.0002 5 1 24 -0.6464 -0.0007 5 1 25 -1.8383 -0.0017 5 1 26 1.2811 0.0089 5 1 27 1.0662 -0.0123 5 1 28 -0.0706 -0.0005 5 1 29 1.2355 0.0112 5 1 30 0.5821 0.0038 5 1 31 -1.5876 0.0038 5 1 32 -0.8324 -0.0012 5 1 33 0.3199 0.0047 5 1 34 -1.5438 -0.0021 5 1 35 1.2958 0.0064 5 1 36 -1.5995 0.0030 5 1 37 -2.2041 0.0025 5 1 38 0.3833 0.0085 5 1 39 -1.6545 0.0022 5 1 40 1.3035 0.0020 5 1 41 -0.0014 0.0046 5 1 42 1.4635 0.0036 5 1 43 -0.2188 0.0315 5 1 44 2.0778 -0.0106 5 2 0 2.6222 -0.0663 5 2 1 -4.8944 -0.0448 5 2 2 -4.0267 -0.0149 5 2 3 3.6696 -0.0225 5 2 4 -2.3364 0.0080 5 2 5 2.1545 0.0258 5 2 6 -3.3310 -0.0247 5 2 7 -6.1080 0.0420 5 2 8 1.3084 0.0046 5 2 9 -1.8000 0.0009 5 2 10 1.2758 0.0238 5 2 11 4.3604 -0.0124 5 2 12 -0.0289 0.0136 5 2 13 3.7511 0.0044 5 2 14 0.6886 0.0166 5 2 15 -1.9134 -0.0177 5 2 16 -2.1923 0.0155 5 2 17 -1.8606 -0.0025 5 2 18 0.6146 -0.0066 5 2 19 -2.3096 0.0060 5 2 20 0.7831 0.0017 5 2 21 1.0962 -0.0027 5 2 22 -0.0440 0.0029 5 2 23 1.9716 -0.0026 5 2 24 0.1444 -0.0038 5 2 25 1.0883 0.0080 5 2 26 0.1988 0.0084 5 2 27 0.7116 -0.0064 5 2 28 0.9067 0.0008 5 2 29 0.8226 -0.0048 5 2 30 -1.1220 0.0035 5 2 31 0.2599 0.0055 5 2 32 -0.9394 -0.0011 5 2 33 -0.4923 -0.0066 5 2 34 -0.9006 -0.0064 5 2 35 1.5255 0.0005 5 2 36 -1.1914 -0.0043 5 2 37 -0.0405 -0.0010 5 2 38 0.3432 0.0085 5 2 39 -0.3769 -0.0001 5 2 40 0.8085 -0.0035 5 2 41 -0.6015 0.0025 5 2 42 0.6668 -0.0031 5 3 0 -0.2627 0.0185 5 3 1 -0.9207 -0.0161 5 3 2 -7.3107 -0.0083 5 3 3 5.2477 -0.0058 5 3 4 -1.4198 0.0114 5 3 5 2.5778 0.0255 5 3 6 3.1737 0.0114 5 3 7 -2.6049 0.0056 5 3 8 1.3962 -0.0103 5 3 9 -3.5597 -0.0094 5 3 10 0.2277 -0.0017 5 3 11 1.5573 0.0181 5 3 12 -2.5110 -0.0173 5 3 13 2.0539 0.0126 5 3 14 0.5050 0.0001 5 3 15 0.6902 -0.0124 5 3 16 2.7635 0.0019 5 3 17 1.3119 -0.0072 5 3 18 0.1749 0.0055 5 3 19 -1.5140 -0.0119 5 3 20 -0.7967 -0.0038 5 3 21 -1.9218 -0.0076 5 3 22 1.1352 0.0040 5 3 23 -1.4326 0.0050 5 3 24 0.3581 -0.0004 5 3 25 -0.3734 0.0037 5 3 26 -0.3376 0.0064 5 3 27 0.4029 0.0011 5 3 28 0.9634 -0.0070 5 3 29 1.5249 0.0052 5 3 30 0.5520 -0.0003 5 3 31 1.5486 -0.0007 5 3 32 0.2520 0.0099 5 3 33 0.2078 -0.0041 5 3 34 -0.4896 -0.0091 5 3 35 -0.8238 -0.0029 5 3 36 -0.5427 0.0012 5 3 37 -1.1348 -0.0023 5 3 38 0.9666 0.0054 5 3 39 -2.4759 0.0012 5 3 40 0.3780 0.0004 5 3 41 1.3058 0.0119 5 4 0 7.2771 0.0111 5 4 1 -4.5715 -0.0244 5 4 2 -3.5484 0.0265 5 4 3 2.5992 -0.0159 5 4 4 -6.9726 -0.0111 5 4 5 3.8913 -0.0061 5 4 6 -0.0354 -0.0011 5 4 7 -1.7155 -0.0295 5 4 8 -0.3467 -0.0011 5 4 9 -3.3856 -0.0061 5 4 10 -0.3851 -0.0081 5 4 11 1.1546 0.0003 5 4 12 0.5020 -0.0075 5 4 13 1.7410 0.0081 5 4 14 -3.6291 -0.0033 5 4 15 1.0368 0.0074 5 4 16 1.1893 0.0025 5 4 17 0.5139 0.0111 5 4 18 0.3521 0.0094 5 4 19 -0.6032 0.0077 5 4 20 -2.2015 -0.0001 5 4 21 -1.2220 -0.0021 5 4 22 -0.9575 -0.0054 5 4 23 0.8385 -0.0084 5 4 24 0.7986 0.0014 5 4 25 0.2431 0.0028 5 4 26 1.1164 -0.0032 5 4 27 -0.9964 0.0004 5 4 28 -0.6831 0.0047 5 4 29 -0.0968 -0.0036 5 4 30 -1.3038 -0.0049 5 4 31 1.5951 0.0066 5 4 32 -0.3589 0.0026 5 4 33 2.8466 -0.0096 5 4 34 -0.2482 -0.0022 5 4 35 -0.6657 -0.0019 5 4 36 0.7920 -0.0014 5 4 37 -2.4303 0.0076 5 4 38 0.9548 0.0028 5 4 39 -3.0760 -0.0144 5 5 0 0.4333 -0.0088 5 5 1 -2.6972 0.0021 5 5 2 3.0330 -0.0134 5 5 3 -4.3527 0.0052 5 5 4 -0.3293 0.0027 5 5 5 2.3766 -0.0013 5 5 6 -0.0083 0.0193 5 5 7 1.2521 -0.0073 5 5 8 1.1847 0.0136 5 5 9 -2.5758 0.0006 5 5 10 0.4402 0.0005 5 5 11 -0.8013 0.0065 5 5 12 -0.9566 0.0003 5 5 13 -0.2752 -0.0053 5 5 14 -0.9261 0.0016 5 5 15 -0.0974 -0.0049 5 5 16 0.6648 0.0033 5 5 17 2.1992 0.0057 5 5 18 1.0060 -0.0076 5 5 19 1.6963 0.0061 5 5 20 0.9082 -0.0001 5 5 21 0.2490 -0.0022 5 5 22 -1.7214 -0.0031 5 5 23 -1.5698 0.0050 5 5 24 -0.6217 0.0033 5 5 25 -0.4739 0.0042 5 5 26 0.3680 -0.0051 5 5 27 0.7899 0.0047 5 5 28 1.4159 0.0011 5 5 29 0.1943 -0.0056 5 5 30 -0.9495 0.0108 5 5 31 2.2598 0.0042 5 5 32 -2.5107 -0.0006 5 5 33 1.7970 0.0067 5 5 34 0.6129 -0.0076 5 5 35 -1.5990 -0.0090 5 5 36 2.5815 -0.0085 5 5 37 -3.1951 -0.0029 5 5 38 0.8898 -0.0109 5 6 0 -0.2838 -0.0081 5 6 1 2.2311 -0.0059 5 6 2 -0.8065 0.0133 5 6 3 -0.4590 -0.0084 5 6 4 -1.6012 0.0035 5 6 5 -0.4582 0.0149 5 6 6 -0.2229 -0.0068 5 6 7 0.1656 0.0100 5 6 8 0.5052 0.0040 5 6 9 -1.2693 -0.0009 5 6 10 1.2041 -0.0041 5 6 11 -0.6736 0.0057 5 6 12 0.6860 0.0113 5 6 13 -0.0037 -0.0237 5 6 14 -2.0072 0.0070 5 6 15 0.2635 -0.0094 5 6 16 -0.5781 -0.0011 5 6 17 -1.9853 -0.0011 5 6 18 1.1283 -0.0080 5 6 19 0.1102 0.0034 5 6 20 -0.6338 -0.0004 5 6 21 1.1146 0.0039 5 6 22 0.8200 -0.0093 5 6 23 0.3882 0.0060 5 6 24 -1.0165 -0.0039 5 6 25 -0.1150 0.0019 5 6 26 -1.6771 0.0006 5 6 27 -0.5151 0.0023 5 6 28 0.6524 -0.0052 5 6 29 -1.0474 0.0119 5 6 30 -0.0506 0.0070 5 6 31 0.3706 -0.0057 5 6 32 -1.2494 -0.0013 5 6 33 5.2772 -0.0050 5 6 34 -2.4423 -0.0040 5 6 35 3.9781 -0.0014 5 6 36 1.1022 0.0010 5 6 37 -5.9711 -0.0036 5 7 0 0.4709 0.0064 5 7 1 2.7744 -0.0073 5 7 2 0.9892 0.0023 5 7 3 1.5068 -0.0026 5 7 4 -0.8284 -0.0077 5 7 5 -0.5348 -0.0086 5 7 6 0.1901 -0.0019 5 7 7 0.1544 0.0022 5 7 8 1.0022 -0.0097 5 7 9 -0.1465 0.0026 5 7 10 -0.6952 -0.0059 5 7 11 -1.7510 0.0097 5 7 12 -0.3209 0.0079 5 7 13 -0.3271 -0.0058 5 7 14 -0.2306 0.0077 5 7 15 1.7920 0.0026 5 7 16 -1.5477 0.0041 5 7 17 1.0912 0.0065 5 7 18 1.0887 0.0125 5 7 19 -0.0741 -0.0117 5 7 20 0.7372 0.0160 5 7 21 0.3457 -0.0059 5 7 22 -0.0045 0.0016 5 7 23 0.1757 0.0063 5 7 24 0.6619 -0.0034 5 7 25 -1.1861 0.0039 5 7 26 -0.7661 0.0051 5 7 27 2.2491 -0.0048 5 7 28 -0.4463 -0.0063 5 7 29 0.8273 0.0047 5 7 30 1.5140 -0.0074 5 7 31 -1.1725 -0.0031 5 7 32 1.2054 -0.0013 5 7 33 0.0826 0.0011 5 7 34 -1.6359 0.0008 5 7 35 2.4637 0.0007 5 8 0 0.4829 0.0019 5 8 1 1.5110 0.0041 5 8 2 -1.0589 -0.0025 5 8 3 1.7067 0.0065 5 8 4 -0.3257 0.0031 5 8 5 -0.1120 0.0005 5 8 6 1.0312 0.0044 5 8 7 -0.7553 0.0068 5 8 8 1.2676 0.0010 5 8 9 -0.2165 -0.0011 5 8 10 1.8521 0.0018 5 8 11 1.0086 -0.0053 5 8 12 1.2962 -0.0014 5 8 13 -1.1863 0.0021 5 8 14 0.1317 0.0013 5 8 15 -1.7628 0.0018 5 8 16 -1.7381 -0.0111 5 8 17 0.0883 0.0023 5 8 18 -1.1887 -0.0080 5 8 19 -0.3945 0.0040 5 8 20 0.2371 -0.0004 5 8 21 0.0998 -0.0050 5 8 22 2.0394 0.0039 5 8 23 1.5339 -0.0164 5 8 24 -0.0196 0.0033 5 8 25 0.4001 -0.0003 5 8 26 -0.6285 -0.0031 5 8 27 -0.4093 0.0083 5 8 28 -1.1792 0.0093 5 8 29 -1.3786 0.0103 5 8 30 -1.6954 0.0064 5 8 31 -0.3631 0.0057 5 8 32 0.7334 0.0046 5 8 33 2.5093 -0.0082 5 9 0 -1.2331 -0.0013 5 9 1 -0.1537 -0.0051 5 9 2 1.0847 -0.0106 5 9 3 0.6346 0.0074 5 9 4 -0.6272 -0.0100 5 9 5 1.4671 0.0002 5 9 6 -0.4613 0.0094 5 9 7 -0.2442 -0.0080 5 9 8 -0.1304 0.0029 5 9 9 0.3565 0.0027 5 9 10 -1.0601 -0.0017 5 9 11 0.8036 -0.0010 5 9 12 -0.4532 -0.0089 5 9 13 0.7644 0.0115 5 9 14 1.8698 -0.0000 5 9 15 0.1868 -0.0029 5 9 16 0.4724 0.0124 5 9 17 0.6182 -0.0104 5 9 18 -2.3332 -0.0022 5 9 19 0.1111 0.0043 5 9 20 -0.6619 -0.0102 5 9 21 -0.0620 0.0073 5 9 22 1.7377 -0.0010 5 9 23 -0.8425 -0.0022 5 9 24 0.6837 0.0072 5 9 25 0.6792 -0.0051 5 9 26 -0.0288 0.0073 5 9 27 0.2111 0.0056 5 9 28 0.7808 0.0003 5 9 29 -0.0985 0.0045 5 9 30 0.5944 0.0044 5 9 31 1.2065 -0.0016 5 10 0 -0.7268 -0.0049 5 10 1 -1.0567 -0.0009 5 10 2 -1.3041 -0.0059 5 10 3 -0.9671 0.0027 5 10 4 1.1242 -0.0017 5 10 5 -0.5484 0.0034 5 10 6 0.9014 0.0011 5 10 7 -1.7303 -0.0025 5 10 8 0.2698 0.0055 5 10 9 -0.3728 -0.0001 5 10 10 1.7272 0.0036 5 10 11 -0.5870 -0.0066 5 10 12 -1.1815 0.0075 5 10 13 -1.2413 0.0010 5 10 14 -0.8858 -0.0028 5 10 15 0.6882 0.0071 5 10 16 1.7661 -0.0007 5 10 17 1.0726 -0.0034 5 10 18 -0.7033 0.0048 5 10 19 -0.4125 0.0053 5 10 20 -2.4875 -0.0015 5 10 21 1.5104 -0.0031 5 10 22 -0.0494 -0.0051 5 10 23 0.8351 -0.0075 5 10 24 0.6214 -0.0094 5 10 25 1.2322 -0.0097 5 10 26 -1.6239 0.0002 5 10 27 2.9106 -0.0172 5 10 28 0.0056 -0.0077 5 10 29 -1.5702 0.0082 5 10 30 2.0364 0.0092 5 11 0 -0.2917 0.0047 5 11 1 2.2272 0.0008 5 11 2 0.0807 -0.0097 5 11 3 1.4688 -0.0057 5 11 4 -0.5818 -0.0049 5 11 5 1.1812 0.0061 5 11 6 -2.2584 -0.0037 5 11 7 -0.8501 0.0075 5 11 8 0.8893 -0.0059 5 11 9 -1.3367 0.0026 5 11 10 2.1616 -0.0061 5 11 11 -0.0396 -0.0021 5 11 12 1.2383 0.0048 5 11 13 -0.3200 -0.0094 5 11 14 0.1103 0.0092 5 11 15 -0.8401 0.0019 5 11 16 0.4749 0.0023 5 11 17 -0.7288 0.0062 5 11 18 0.1669 -0.0009 5 11 19 -0.9425 0.0057 5 11 20 -1.2797 -0.0017 5 11 21 -2.1083 0.0088 5 11 22 -0.3201 -0.0032 5 11 23 1.1564 -0.0083 5 11 24 1.5419 0.0029 5 11 25 -0.1063 0.0203 5 11 26 -1.7025 0.0021 5 11 27 -0.1620 -0.0002 5 11 28 -4.4390 0.0180 5 11 29 2.2921 -0.0221 5 12 0 -0.0809 0.0052 5 12 1 -0.8308 0.0141 5 12 2 -0.5062 -0.0023 5 12 3 0.6198 0.0150 5 12 4 -0.5048 -0.0059 5 12 5 0.5991 0.0068 5 12 6 -0.9002 0.0016 5 12 7 0.2109 0.0049 5 12 8 -0.6036 -0.0037 5 12 9 -0.9104 0.0008 5 12 10 -0.3513 0.0011 5 12 11 -1.2648 -0.0080 5 12 12 -0.3136 -0.0028 5 12 13 0.0837 0.0045 5 12 14 -0.5380 0.0023 5 12 15 0.4832 0.0096 5 12 16 0.6416 0.0158 5 12 17 -0.0896 -0.0008 5 12 18 0.9346 0.0044 5 12 19 0.5248 0.0045 5 12 20 -0.4791 0.0040 5 12 21 -0.3189 -0.0068 5 12 22 -1.6801 -0.0040 5 12 23 0.8466 -0.0192 5 12 24 0.2875 -0.0113 5 12 25 3.8582 0.0034 5 12 26 0.8280 -0.0312 5 12 27 -0.3964 0.0124 5 13 0 0.5661 0.0036 5 13 1 -0.0177 0.0030 5 13 2 0.7753 0.0096 5 13 3 2.1607 0.0115 5 13 4 -0.2776 -0.0016 5 13 5 -0.7373 0.0173 5 13 6 0.3964 -0.0090 5 13 7 -0.5782 0.0024 5 13 8 1.1751 -0.0031 5 13 9 -2.8000 -0.0092 5 13 10 1.1913 0.0005 5 13 11 -1.1787 0.0017 5 13 12 -0.2582 -0.0039 5 13 13 0.6890 -0.0039 5 13 14 -0.9741 -0.0120 5 13 15 0.0898 -0.0017 5 13 16 0.9008 0.0001 5 13 17 0.3669 -0.0057 5 13 18 1.4877 0.0111 5 13 19 -1.4403 0.0150 5 13 20 -0.0995 0.0285 5 13 21 -2.3706 0.0123 5 13 22 -1.5663 0.0187 5 13 23 -3.0983 -0.0090 5 13 24 -1.5083 0.0141 5 13 25 2.8767 -0.0002 5 14 0 0.2998 -0.0156 5 14 1 0.3138 -0.0110 5 14 2 -0.1156 -0.0035 5 14 3 1.5123 0.0090 5 14 4 -0.2328 0.0084 5 14 5 1.6736 0.0182 5 14 6 -0.9497 0.0212 5 14 7 -0.1244 0.0359 5 14 8 0.3293 0.0150 5 14 9 -1.8442 0.0228 5 14 10 0.7082 -0.0229 5 14 11 -1.4681 0.0086 5 14 12 0.9150 -0.0147 5 14 13 -1.9506 0.0103 5 14 14 -2.8488 -0.0071 5 14 15 -0.0321 0.0121 5 14 16 -1.7377 -0.0073 5 14 17 2.1513 -0.0092 5 14 18 1.2254 0.0026 5 14 19 0.4946 -0.0086 5 14 20 0.8421 -0.0039 5 14 21 0.8698 0.0220 5 14 22 -0.2622 -0.0047 5 15 0 -1.0180 -0.0046 5 15 1 -0.4335 -0.0031 5 15 2 0.1155 0.0223 5 15 3 -0.0224 -0.0257 5 15 4 0.9131 0.0194 5 15 5 1.7603 -0.0234 5 15 6 2.2295 -0.0014 5 15 7 -0.2090 -0.0063 5 15 8 0.8725 0.0278 5 15 9 -1.6783 0.0003 5 15 10 1.1347 0.0102 5 15 11 -0.1708 0.0066 5 15 12 0.8676 -0.0168 5 15 13 0.3391 0.0114 5 15 14 -1.7583 -0.0002 5 15 15 -2.0703 -0.0137 5 15 16 -0.9931 0.0068 5 15 17 -0.0150 -0.0026 5 15 18 -0.5786 0.0057 5 16 0 -1.1310 -0.0147 5 16 1 1.8137 0.0029 5 16 2 -2.2594 -0.0165 5 16 3 1.6784 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9 5 24 -0.4271 -0.0136 9 5 25 -0.0440 -0.0010 9 5 26 -1.6867 -0.0070 9 5 27 1.6551 0.0038 9 5 28 2.3647 0.0075 9 5 29 0.7516 0.0044 9 5 30 -1.5211 0.0100 9 5 31 0.4548 -0.0153 9 5 32 -1.5405 0.0050 9 5 33 -0.3307 0.0040 9 5 34 0.5838 -0.0112 9 5 35 -0.4657 0.0044 9 6 0 0.8193 -0.0054 9 6 1 -1.0809 0.0025 9 6 2 -0.3969 -0.0068 9 6 3 1.8128 -0.0015 9 6 4 -0.2444 0.0056 9 6 5 -0.1339 -0.0007 9 6 6 -0.8549 -0.0043 9 6 7 -1.7662 0.0146 9 6 8 -0.8339 -0.0004 9 6 9 0.0389 -0.0003 9 6 10 0.9817 -0.0025 9 6 11 -1.4354 -0.0024 9 6 12 1.2354 -0.0052 9 6 13 -2.8777 -0.0128 9 6 14 -0.7123 0.0089 9 6 15 -0.1925 -0.0067 9 6 16 -1.1334 -0.0012 9 6 17 2.7209 0.0050 9 6 18 -0.0013 -0.0005 9 6 19 0.2705 -0.0147 9 6 20 0.8696 0.0140 9 6 21 -0.0387 -0.0007 9 6 22 2.4141 0.0043 9 6 23 -0.6313 0.0021 9 6 24 -0.5304 -0.0034 9 6 25 -2.0043 -0.0011 9 6 26 -1.7569 -0.0039 9 6 27 0.2594 0.0046 9 6 28 -1.2698 -0.0046 9 6 29 -0.0845 0.0069 9 6 30 0.9531 -0.0124 9 6 31 -0.9816 -0.0007 9 6 32 2.9280 -0.0061 9 6 33 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-0.0031 9 8 15 0.5896 -0.0003 9 8 16 -4.6398 0.0019 9 8 17 -1.2756 -0.0110 9 8 18 -1.3800 0.0014 9 8 19 1.4047 -0.0057 9 8 20 0.7241 -0.0081 9 8 21 -0.3434 0.0072 9 8 22 -1.1117 -0.0036 9 8 23 -0.6542 -0.0052 9 8 24 -0.5672 0.0165 9 8 25 0.6538 -0.0014 9 8 26 0.8083 0.0151 9 8 27 -2.8505 0.0004 9 9 0 0.2554 -0.0039 9 9 1 -1.8413 0.0017 9 9 2 -0.3185 -0.0007 9 9 3 1.1809 -0.0012 9 9 4 -0.5653 -0.0015 9 9 5 -0.2411 -0.0014 9 9 6 0.3559 0.0064 9 9 7 -0.7413 0.0085 9 9 8 0.2353 0.0057 9 9 9 1.8618 0.0020 9 9 10 0.1340 -0.0030 9 9 11 -1.2603 -0.0063 9 9 12 -0.1129 -0.0017 9 9 13 -1.7984 0.0001 9 9 14 1.9809 -0.0033 9 9 15 3.7423 0.0046 9 9 16 -1.3680 -0.0039 9 9 17 -1.7673 -0.0014 9 9 18 -0.3648 0.0097 9 9 19 -1.4327 -0.0117 9 9 20 0.9137 0.0152 9 9 21 2.3388 -0.0024 9 9 22 -1.8680 -0.0070 9 9 23 0.4833 0.0139 9 9 24 -0.9379 -0.0042 9 9 25 1.4709 -0.0000 9 10 0 -0.6980 -0.0025 9 10 1 -0.2079 0.0033 9 10 2 -1.9145 -0.0008 9 10 3 0.2313 -0.0087 9 10 4 1.0002 -0.0044 9 10 5 -0.6862 -0.0165 9 10 6 0.3354 -0.0042 9 10 7 -1.1311 -0.0060 9 10 8 -0.9746 -0.0047 9 10 9 1.6467 0.0078 9 10 10 0.1554 0.0011 9 10 11 -1.2455 0.0082 9 10 12 -0.4860 0.0091 9 10 13 -0.7531 -0.0021 9 10 14 -0.0462 -0.0010 9 10 15 1.3550 -0.0022 9 10 16 -0.6026 -0.0008 9 10 17 0.3737 0.0034 9 10 18 -2.5099 -0.0099 9 10 19 -0.7399 0.0001 9 10 20 1.6821 0.0086 9 10 21 -1.7182 -0.0188 9 10 22 0.2350 0.0119 9 11 0 3.7680 0.0068 9 11 1 0.9549 0.0092 9 11 2 0.3050 0.0060 9 11 3 0.5055 0.0051 9 11 4 -1.6680 -0.0019 9 11 5 0.8898 -0.0156 9 11 6 0.0590 0.0015 9 11 7 -0.0962 -0.0054 9 11 8 0.8634 -0.0051 9 11 9 -0.4960 0.0014 9 11 10 -0.0832 -0.0082 9 11 11 0.0708 0.0017 9 11 12 0.7479 -0.0158 9 11 13 -0.5966 -0.0009 9 11 14 1.4733 0.0106 9 11 15 -0.5258 -0.0057 9 11 16 1.4396 0.0138 9 11 17 1.0035 0.0033 9 11 18 0.8936 -0.0036 9 11 19 -1.4168 0.0054 9 11 20 -2.4873 -0.0103 9 12 0 -1.2819 -0.0039 9 12 1 -1.2250 -0.0044 9 12 2 1.1269 0.0075 9 12 3 0.3713 0.0068 9 12 4 -0.7803 0.0129 9 12 5 -1.1722 0.0091 9 12 6 -0.9759 -0.0086 9 12 7 1.4819 -0.0048 9 12 8 0.4599 0.0095 9 12 9 1.4244 -0.0027 9 12 10 -1.7699 0.0046 9 12 11 0.2761 -0.0008 9 12 12 0.1077 -0.0041 9 12 13 0.5235 -0.0000 9 12 14 -0.5101 0.0002 9 12 15 -1.2884 0.0053 9 12 16 -0.7971 -0.0068 9 13 0 -0.1573 0.0053 9 13 1 0.8667 -0.0036 9 13 2 -0.3412 -0.0108 9 13 3 0.6961 -0.0083 9 13 4 1.9816 -0.0027 9 13 5 -0.8836 -0.0104 9 13 6 0.3472 0.0004 9 13 7 -1.5068 -0.0074 9 13 8 -1.2573 -0.0117 9 13 9 -1.0402 0.0205 9 13 10 -0.2594 -0.0091 9 13 11 0.2035 -0.0118 9 13 12 -0.2631 -0.0018 9 14 0 1.0316 0.0075 9 14 1 3.4785 0.0124 9 14 2 -0.8845 -0.0017 9 14 3 1.3492 -0.0168 9 14 4 -2.2818 0.0209 9 14 5 -0.3671 -0.0178 10 0 0 -5.7279 -0.1143 10 0 2 0.6018 0.2115 10 0 4 4.2664 0.0325 10 0 6 -2.1184 0.0588 10 0 8 -0.8259 -0.0026 10 0 10 2.3821 0.0143 10 0 12 1.7968 0.0140 10 0 14 -0.1476 0.0228 10 0 16 -1.9261 0.0137 10 0 18 -1.0210 -0.0026 10 0 20 0.7127 0.0066 10 0 22 0.1672 -0.0263 10 0 24 1.5647 -0.0013 10 0 26 -0.0263 -0.0049 10 0 28 0.1655 -0.0034 10 1 0 -3.6756 -0.1168 10 1 1 1.7110 0.0717 10 1 2 -2.6246 -0.0118 10 1 3 -1.3767 -0.0716 10 1 4 1.7534 0.0212 10 1 5 -1.5722 -0.0386 10 1 6 1.7020 0.0001 10 1 7 1.5003 -0.0255 10 1 8 -2.5230 0.0052 10 1 9 2.3070 -0.0473 10 1 10 -1.9650 -0.0082 10 1 11 -0.3255 0.0095 10 1 12 1.8577 0.0011 10 1 13 -1.1443 -0.0114 10 1 14 1.5080 -0.0067 10 1 15 0.6686 -0.0020 10 1 16 -0.2882 0.0105 10 1 17 0.0187 -0.0048 10 1 18 -0.9281 -0.0014 10 1 19 -0.2322 -0.0021 10 1 20 -1.3114 0.0011 10 1 21 -1.1946 -0.0123 10 1 22 1.0535 0.0077 10 1 23 -0.1037 0.0017 10 1 24 1.1164 -0.0019 10 1 25 1.4566 0.0081 10 1 26 -0.4410 -0.0002 10 1 27 0.4990 0.0103 10 1 28 -0.0416 0.0032 10 1 29 1.2126 0.0075 10 1 30 0.5586 0.0034 10 1 31 0.7997 0.0068 10 1 32 -1.1037 -0.0016 10 2 0 -1.6962 -0.0146 10 2 1 0.7373 -0.0368 10 2 2 -2.6264 0.0125 10 2 3 -0.8348 0.0148 10 2 4 -1.1187 -0.0148 10 2 5 -4.0125 0.0251 10 2 6 2.2821 -0.0078 10 2 7 -1.5482 0.0209 10 2 8 1.0604 0.0274 10 2 9 1.1595 -0.0106 10 2 10 -0.6290 0.0223 10 2 11 1.5012 -0.0087 10 2 12 -0.7500 0.0110 10 2 13 -1.2399 -0.0037 10 2 14 0.5171 0.0140 10 2 15 -0.3396 -0.0033 10 2 16 0.2375 0.0023 10 2 17 2.1890 0.0041 10 2 18 0.1180 -0.0088 10 2 19 0.2227 0.0049 10 2 20 -0.7327 0.0011 10 2 21 -1.6142 0.0054 10 2 22 -0.8638 -0.0097 10 2 23 -1.7102 -0.0083 10 2 24 -0.2809 -0.0015 10 2 25 -0.7055 -0.0031 10 2 26 0.0559 0.0033 10 2 27 1.1573 -0.0027 10 2 28 0.2597 -0.0047 10 2 29 0.5920 0.0027 10 2 30 0.9216 -0.0120 10 2 31 0.3874 -0.0036 10 2 32 1.4823 -0.0025 10 2 33 -1.5484 0.0027 10 2 34 -0.9685 -0.0049 10 3 0 -1.3341 0.0185 10 3 1 4.2112 -0.0050 10 3 2 -2.6541 0.0025 10 3 3 1.8986 0.0088 10 3 4 0.3705 0.0173 10 3 5 -1.1072 0.0081 10 3 6 1.0872 -0.0061 10 3 7 -1.9092 0.0014 10 3 8 -1.5019 -0.0128 10 3 9 -0.1344 -0.0003 10 3 10 -1.2076 -0.0118 10 3 11 0.4058 0.0060 10 3 12 -0.2942 -0.0070 10 3 13 -0.6371 0.0001 10 3 14 0.3838 0.0049 10 3 15 -1.2951 0.0001 10 3 16 0.8892 0.0144 10 3 17 -0.3609 -0.0065 10 3 18 0.1748 0.0121 10 3 19 -0.3278 -0.0132 10 3 20 -0.3550 0.0117 10 3 21 1.2045 0.0010 10 3 22 0.8949 0.0060 10 3 23 0.5050 0.0007 10 3 24 0.8846 -0.0159 10 3 25 -0.2710 0.0021 10 3 26 -0.3011 -0.0007 10 3 27 1.9628 -0.0055 10 3 28 -1.8498 0.0109 10 3 29 -0.5111 -0.0070 10 3 30 -1.3969 -0.0025 10 3 31 0.4712 -0.0080 10 3 32 0.9950 0.0020 10 3 33 -0.2643 0.0083 10 3 34 0.2526 0.0054 10 3 35 -2.1555 0.0252 10 3 36 -0.3684 -0.0250 10 4 0 0.6513 0.0049 10 4 1 -0.4613 -0.0033 10 4 2 -2.6055 0.0115 10 4 3 -0.0156 0.0079 10 4 4 -0.5097 -0.0162 10 4 5 0.3603 -0.0134 10 4 6 2.9915 0.0005 10 4 7 -2.1383 -0.0153 10 4 8 0.9759 0.0014 10 4 9 0.0309 -0.0052 10 4 10 -3.0974 -0.0045 10 4 11 2.2397 -0.0044 10 4 12 -1.1900 -0.0063 10 4 13 1.8132 0.0113 10 4 14 1.6789 -0.0028 10 4 15 -0.5538 0.0115 10 4 16 -0.1635 0.0002 10 4 17 0.1792 0.0091 10 4 18 -1.9202 -0.0027 10 4 19 -0.5999 0.0069 10 4 20 0.0800 0.0025 10 4 21 -1.0094 0.0023 10 4 22 -0.5806 0.0118 10 4 23 0.1275 -0.0089 10 4 24 -0.8074 -0.0006 10 4 25 -1.9343 -0.0008 10 4 26 1.8568 -0.0143 10 4 27 1.0853 0.0181 10 4 28 -0.4069 0.0020 10 4 29 0.9328 -0.0049 10 4 30 -0.5592 0.0089 10 4 31 1.0832 -0.0061 10 4 32 0.6869 0.0054 10 4 33 1.0211 -0.0076 10 4 34 0.3142 0.0227 10 4 35 -0.9919 -0.0145 10 4 36 0.6715 0.0038 10 5 0 0.5415 -0.0133 10 5 1 1.5515 0.0019 10 5 2 -1.3728 0.0051 10 5 3 -0.1892 0.0015 10 5 4 -1.9852 -0.0023 10 5 5 -0.7005 -0.0008 10 5 6 2.0735 0.0132 10 5 7 -0.1432 0.0049 10 5 8 3.6408 0.0097 10 5 9 -0.7951 0.0155 10 5 10 -1.1070 0.0049 10 5 11 -1.7796 0.0057 10 5 12 -2.7800 0.0064 10 5 13 -0.9576 0.0003 10 5 14 1.4743 -0.0005 10 5 15 1.5395 0.0015 10 5 16 3.3262 0.0019 10 5 17 -0.8175 -0.0108 10 5 18 0.1050 -0.0048 10 5 19 -0.7439 0.0003 10 5 20 -2.4582 -0.0010 10 5 21 0.8181 0.0125 10 5 22 0.5097 0.0027 10 5 23 0.0482 0.0042 10 5 24 -1.1367 0.0037 10 5 25 1.3155 -0.0143 10 5 26 2.2974 0.0103 10 5 27 -1.3548 -0.0000 10 5 28 2.1619 -0.0019 10 5 29 -0.5659 0.0055 10 5 30 -2.4422 -0.0195 10 5 31 0.4458 -0.0041 10 5 32 0.0274 -0.0075 10 5 33 0.0499 0.0180 10 5 34 -1.2260 -0.0104 10 6 0 -1.4992 -0.0134 10 6 1 2.6617 0.0038 10 6 2 -1.2277 0.0104 10 6 3 1.4290 -0.0038 10 6 4 -0.9636 0.0091 10 6 5 -1.3859 0.0004 10 6 6 -1.2860 0.0036 10 6 7 2.0024 -0.0028 10 6 8 0.4103 0.0051 10 6 9 3.2122 -0.0092 10 6 10 0.2590 -0.0127 10 6 11 1.1356 -0.0053 10 6 12 -0.4635 -0.0007 10 6 13 -1.9898 -0.0194 10 6 14 -1.1689 0.0066 10 6 15 0.4475 0.0076 10 6 16 0.7816 -0.0057 10 6 17 1.9777 0.0065 10 6 18 1.4333 0.0006 10 6 19 -0.4308 0.0008 10 6 20 0.8834 0.0056 10 6 21 -0.9596 0.0084 10 6 22 -0.6481 0.0016 10 6 23 -1.4412 0.0066 10 6 24 -1.6216 -0.0023 10 6 25 0.8263 0.0066 10 6 26 -1.2903 0.0011 10 6 27 1.0127 -0.0027 10 6 28 0.8044 0.0172 10 6 29 -2.1012 -0.0071 10 6 30 2.7458 0.0016 10 6 31 1.2571 0.0002 10 6 32 -0.1880 0.0081 10 7 0 -1.0153 -0.0019 10 7 1 -0.9737 0.0054 10 7 2 0.4235 0.0015 10 7 3 0.5933 -0.0006 10 7 4 0.2073 -0.0021 10 7 5 -0.4462 -0.0101 10 7 6 -1.1062 0.0003 10 7 7 -0.8626 -0.0012 10 7 8 0.0859 -0.0020 10 7 9 -0.4252 0.0041 10 7 10 0.3408 -0.0026 10 7 11 2.2136 0.0046 10 7 12 -1.7810 0.0023 10 7 13 1.5549 0.0073 10 7 14 0.6469 0.0137 10 7 15 -1.7978 -0.0045 10 7 16 1.5972 0.0079 10 7 17 1.5607 -0.0083 10 7 18 -0.2529 -0.0023 10 7 19 -0.1739 -0.0066 10 7 20 1.0314 -0.0028 10 7 21 1.0235 -0.0086 10 7 22 -0.5116 0.0009 10 7 23 -0.8872 -0.0110 10 7 24 0.7621 0.0063 10 7 25 -2.1868 0.0054 10 7 26 1.5635 -0.0145 10 8 0 -0.0767 0.0022 10 8 1 0.3186 -0.0006 10 8 2 0.0901 -0.0023 10 8 3 -0.6223 -0.0091 10 8 4 1.0270 -0.0048 10 8 5 0.2218 -0.0005 10 8 6 -1.5569 -0.0024 10 8 7 1.9837 0.0059 10 8 8 -0.2617 0.0138 10 8 9 -0.3856 0.0006 10 8 10 0.4931 0.0128 10 8 11 0.0025 -0.0017 10 8 12 0.4890 -0.0067 10 8 13 3.0040 -0.0014 10 8 14 -2.1705 -0.0110 10 8 15 -0.3592 0.0036 10 8 16 -1.3977 -0.0021 10 8 17 -0.5438 -0.0079 10 8 18 2.7281 0.0079 10 8 19 1.2121 -0.0010 10 8 20 -0.1800 0.0012 10 8 21 -0.6993 -0.0011 10 8 22 0.3295 0.0039 10 8 23 2.6463 -0.0091 10 8 24 -0.9342 0.0065 10 9 0 1.0912 0.0091 10 9 1 -0.6818 0.0055 10 9 2 0.1121 0.0087 10 9 3 -0.2473 -0.0059 10 9 4 1.4023 0.0024 10 9 5 -1.0752 -0.0047 10 9 6 0.5011 -0.0029 10 9 7 1.0391 0.0094 10 9 8 0.0241 -0.0109 10 9 9 -0.1469 0.0059 10 9 10 -0.4674 -0.0012 10 9 11 -3.7070 -0.0077 10 9 12 0.3394 0.0064 10 9 13 4.2128 -0.0096 10 9 14 -0.8790 0.0073 10 9 15 2.7737 0.0060 10 9 16 -1.0894 -0.0003 10 9 17 -2.6383 0.0064 10 9 18 2.1812 -0.0065 10 9 19 2.6881 -0.0131 10 9 20 -0.6673 0.0104 10 9 21 1.5727 -0.0003 10 9 22 -0.5621 -0.0003 10 10 0 -3.4526 0.0032 10 10 1 1.4269 0.0039 10 10 2 -0.4789 -0.0000 10 10 3 -0.9697 0.0024 10 10 4 0.6914 -0.0014 10 10 5 -1.1543 -0.0090 10 10 6 0.0010 -0.0040 10 10 7 0.9484 -0.0085 10 10 8 1.1668 -0.0006 10 10 9 -0.6648 0.0132 10 10 10 1.3359 0.0062 10 10 11 -2.6575 0.0108 10 10 12 0.3122 -0.0029 10 10 13 -1.5555 -0.0068 10 10 14 1.2347 0.0090 10 10 15 -0.2124 -0.0106 10 10 16 -2.0476 0.0066 10 10 17 1.4371 0.0121 10 10 18 -1.0823 -0.0153 10 10 19 -1.5268 0.0103 10 10 20 0.8818 0.0002 10 11 0 1.0400 0.0178 10 11 1 1.3959 0.0048 10 11 2 -2.6904 -0.0019 10 11 3 1.8802 -0.0042 10 11 4 -1.5231 -0.0058 10 11 5 0.4690 0.0028 10 11 6 -0.2277 0.0019 10 11 7 0.5885 -0.0031 10 11 8 0.5698 0.0116 10 11 9 0.3000 -0.0074 10 11 10 0.9398 -0.0065 10 11 11 -0.3580 0.0012 10 11 12 0.9461 -0.0043 10 11 13 -0.5049 -0.0013 10 11 14 0.5404 0.0112 10 11 15 -0.4018 0.0002 10 11 16 2.4007 0.0048 10 12 0 0.9631 0.0136 10 12 1 0.4112 0.0118 10 12 2 0.5726 0.0191 10 12 3 -0.6748 0.0101 10 12 4 -2.1101 -0.0062 10 12 5 0.5007 0.0027 10 12 6 -1.3195 -0.0018 10 12 7 1.3358 0.0036 10 12 8 -0.7845 0.0028 10 12 9 -0.2739 -0.0034 10 12 10 1.6273 0.0016 10 12 11 -1.0025 -0.0105 10 12 12 1.5656 0.0100 10 13 0 -1.7548 -0.0178 10 13 1 0.7046 0.0026 10 13 2 1.4989 -0.0099 10 13 3 -0.0506 -0.0011 10 13 4 0.1379 -0.0001 10 13 5 -0.4387 -0.0294 10 13 6 -3.0551 0.0159 11 0 0 2.1142 0.3294 11 0 2 4.4433 0.1162 11 0 4 -2.9531 -0.0152 11 0 6 -3.4896 -0.0023 11 0 8 0.8559 -0.0333 11 0 10 1.3817 0.0111 11 0 12 -0.5248 -0.0025 11 0 14 -0.9480 0.0101 11 0 16 0.2189 -0.0274 11 0 18 0.9288 -0.0014 11 0 20 -0.2183 -0.0187 11 0 22 -0.0621 -0.0126 11 0 24 0.1220 0.0005 11 1 0 -0.6038 -0.0475 11 1 1 -1.5064 -0.0699 11 1 2 3.3682 0.0656 11 1 3 -0.8304 -0.0896 11 1 4 3.0438 0.0056 11 1 5 0.5566 0.0076 11 1 6 -0.7590 0.0091 11 1 7 0.4466 -0.0331 11 1 8 -2.3560 0.0010 11 1 9 -1.2189 0.0216 11 1 10 1.3124 -0.0045 11 1 11 -1.9016 0.0186 11 1 12 1.3408 -0.0118 11 1 13 0.6465 -0.0047 11 1 14 -0.8889 0.0008 11 1 15 1.6271 0.0054 11 1 16 -0.4607 0.0101 11 1 17 0.1638 0.0073 11 1 18 -0.0906 -0.0101 11 1 19 -0.4857 0.0144 11 1 20 1.5229 0.0005 11 1 21 -0.4363 0.0083 11 1 22 0.2512 0.0002 11 1 23 -0.0735 0.0156 11 1 24 -0.8899 -0.0037 11 1 25 -0.2395 0.0055 11 1 26 0.6603 0.0015 11 1 27 0.8405 0.0158 11 1 28 0.1423 0.0110 11 2 0 -1.5045 0.0349 11 2 1 -0.2502 0.0148 11 2 2 -1.2629 0.0200 11 2 3 -2.1563 0.0288 11 2 4 1.3714 -0.0037 11 2 5 1.7408 0.0073 11 2 6 0.9928 0.0139 11 2 7 2.6389 -0.0105 11 2 8 -1.0025 0.0222 11 2 9 1.0346 -0.0205 11 2 10 -0.9056 0.0037 11 2 11 -0.9506 0.0001 11 2 12 0.6864 -0.0071 11 2 13 -2.2047 -0.0003 11 2 14 1.3578 -0.0090 11 2 15 1.1124 0.0053 11 2 16 0.4708 -0.0138 11 2 17 0.5943 -0.0051 11 2 18 -0.7603 0.0080 11 2 19 -1.2424 -0.0083 11 2 20 0.2203 0.0085 11 2 21 -0.3953 -0.0010 11 2 22 0.7017 -0.0047 11 2 23 -0.5339 0.0043 11 2 24 -1.2794 -0.0001 11 2 25 0.6922 -0.0046 11 2 26 0.8426 -0.0008 11 2 27 0.7095 0.0144 11 2 28 0.3532 -0.0138 11 2 29 1.8249 0.0186 11 2 30 -0.6780 -0.0194 11 3 0 0.0290 -0.0045 11 3 1 1.6230 0.0145 11 3 2 2.0362 0.0031 11 3 3 -2.9434 0.0128 11 3 4 2.3182 0.0120 11 3 5 -1.6815 -0.0097 11 3 6 -0.1295 -0.0132 11 3 7 1.7962 -0.0063 11 3 8 -0.9958 -0.0074 11 3 9 1.5686 -0.0004 11 3 10 -1.0894 -0.0016 11 3 11 0.2075 -0.0054 11 3 12 -0.8218 0.0046 11 3 13 0.3025 -0.0062 11 3 14 -0.2572 0.0022 11 3 15 -0.0020 0.0039 11 3 16 0.4189 -0.0027 11 3 17 -0.2968 0.0000 11 3 18 0.2727 -0.0140 11 3 19 0.8357 0.0054 11 3 20 0.6486 -0.0007 11 3 21 1.4602 0.0035 11 3 22 1.3123 0.0011 11 3 23 -1.2775 0.0019 11 3 24 -0.2731 -0.0121 11 3 25 0.8004 -0.0005 11 3 26 -0.7649 0.0077 11 3 27 -1.6299 -0.0048 11 3 28 -0.2512 0.0269 11 3 29 -1.9584 -0.0038 11 3 30 1.8862 -0.0033 11 3 31 2.4478 -0.0026 11 3 32 1.2572 -0.0016 11 3 33 -0.7067 0.0075 11 4 0 -2.4796 0.0024 11 4 1 -0.3514 0.0046 11 4 2 0.0430 -0.0221 11 4 3 0.8533 0.0021 11 4 4 2.4986 -0.0165 11 4 5 -1.4760 -0.0127 11 4 6 1.1849 0.0050 11 4 7 0.4463 0.0055 11 4 8 -0.9692 -0.0004 11 4 9 2.1988 0.0066 11 4 10 0.6940 -0.0009 11 4 11 -0.0842 0.0075 11 4 12 2.9057 -0.0028 11 4 13 -0.4260 0.0027 11 4 14 1.5564 0.0041 11 4 15 0.3472 -0.0087 11 4 16 -2.1864 0.0061 11 4 17 0.2644 -0.0079 11 4 18 -1.2682 -0.0001 11 4 19 -2.8284 -0.0101 11 4 20 1.0455 0.0007 11 4 21 0.0727 0.0014 11 4 22 -0.2948 0.0080 11 4 23 -0.8072 -0.0030 11 4 24 0.7264 -0.0032 11 4 25 0.3045 0.0034 11 4 26 -0.2966 -0.0102 11 4 27 3.1532 0.0149 11 4 28 -1.6409 0.0036 11 4 29 -0.7965 0.0029 11 4 30 0.1067 -0.0028 11 4 31 0.1777 0.0010 11 4 32 1.2917 -0.0116 11 4 33 -0.0322 0.0115 11 4 34 0.5377 -0.0088 11 4 35 -1.6711 0.0167 11 5 0 -0.6321 0.0021 11 5 1 -0.8763 0.0016 11 5 2 -2.0045 0.0092 11 5 3 -1.5178 -0.0081 11 5 4 0.8911 0.0076 11 5 5 0.0700 0.0004 11 5 6 1.1280 0.0091 11 5 7 1.3973 0.0111 11 5 8 -2.8562 -0.0052 11 5 9 0.0097 0.0080 11 5 10 -3.4744 0.0028 11 5 11 -2.0882 -0.0097 11 5 12 1.2132 -0.0063 11 5 13 1.3638 -0.0029 11 5 14 2.1185 -0.0100 11 5 15 2.4154 -0.0001 11 5 16 0.9217 -0.0101 11 5 17 -0.0593 -0.0013 11 5 18 -2.1531 -0.0078 11 5 19 1.6374 -0.0021 11 5 20 -0.2315 -0.0017 11 5 21 -1.0619 -0.0017 11 5 22 1.9364 0.0009 11 5 23 -0.3502 0.0005 11 5 24 1.3490 -0.0028 11 5 25 -1.9890 -0.0186 11 5 26 2.2487 0.0053 11 5 27 -0.8851 -0.0078 11 5 28 -2.8224 0.0035 11 5 29 2.7575 -0.0070 11 5 30 -2.6178 0.0031 11 5 31 0.8190 -0.0143 11 5 32 -0.8188 0.0113 11 5 33 0.4838 -0.0067 11 6 0 0.1204 0.0087 11 6 1 1.6911 0.0104 11 6 2 0.9273 0.0060 11 6 3 -1.8772 -0.0021 11 6 4 -1.3464 -0.0103 11 6 5 0.7225 -0.0070 11 6 6 1.0942 -0.0026 11 6 7 2.7378 -0.0087 11 6 8 1.0625 -0.0100 11 6 9 0.9711 0.0077 11 6 10 -0.5554 -0.0058 11 6 11 -4.0136 -0.0059 11 6 12 -0.2338 0.0061 11 6 13 -4.3063 -0.0082 11 6 14 1.0964 0.0069 11 6 15 2.1068 0.0074 11 6 16 0.8546 0.0036 11 6 17 2.5571 0.0004 11 6 18 -0.8451 -0.0005 11 6 19 -0.5851 -0.0004 11 6 20 -1.5103 0.0001 11 6 21 -1.2099 -0.0107 11 6 22 -0.3390 0.0099 11 6 23 -0.5741 0.0026 11 6 24 1.2816 -0.0068 11 6 25 -0.1470 0.0097 11 6 26 0.6600 -0.0180 11 6 29 -0.7489 0.0110 11 6 30 0.0119 -0.0191 11 7 0 -0.7323 0.0163 11 7 1 0.6016 0.0006 11 7 2 1.6832 0.0015 11 7 3 0.7503 -0.0025 11 7 4 -2.6268 -0.0089 11 7 5 -0.6257 -0.0118 11 7 6 -2.6661 -0.0019 11 7 7 0.4429 -0.0032 11 7 8 -0.8236 0.0052 11 7 9 2.5546 0.0028 11 7 10 -1.6501 0.0119 11 7 11 3.4074 0.0072 11 7 12 0.1256 0.0032 11 7 13 -3.5948 0.0058 11 7 14 1.4473 -0.0034 11 7 15 -3.2327 -0.0033 11 7 16 -0.0204 0.0034 11 7 17 0.4090 -0.0114 11 7 18 1.7114 -0.0040 11 7 19 1.3751 -0.0002 11 7 20 -1.9281 -0.0188 11 7 21 2.1765 0.0030 11 7 22 -2.0588 0.0120 11 7 23 -2.7620 -0.0108 11 7 24 2.3336 0.0160 11 8 0 -1.5043 0.0041 11 8 1 -1.1065 0.0042 11 8 2 1.4804 0.0065 11 8 3 -0.1740 0.0052 11 8 4 1.2750 -0.0088 11 8 5 2.1461 0.0083 11 8 6 -0.0980 -0.0086 11 8 7 -0.2471 -0.0023 11 8 8 0.4164 0.0083 11 8 9 -1.5090 -0.0035 11 8 10 -1.8333 0.0008 11 8 11 2.4557 -0.0162 11 8 12 -1.8709 -0.0036 11 8 13 1.5414 -0.0080 11 8 14 -2.1413 -0.0037 11 8 15 -3.0768 0.0062 11 8 16 1.3815 0.0082 11 8 17 -0.2773 -0.0013 11 8 18 -0.7093 0.0169 11 8 19 -0.9028 -0.0138 11 8 20 1.2783 0.0027 11 8 21 1.7953 0.0066 11 8 22 0.7808 -0.0188 11 9 0 0.3992 0.0010 11 9 1 -1.0134 0.0120 11 9 2 -0.8774 0.0015 11 9 3 -0.9698 0.0015 11 9 4 0.2156 0.0083 11 9 5 -0.0204 -0.0008 11 9 6 0.3987 -0.0016 11 9 7 0.9459 0.0038 11 9 8 1.0632 -0.0053 11 9 9 -2.9939 0.0036 11 9 10 0.2975 -0.0022 11 9 11 0.7728 -0.0060 11 9 12 -0.2015 -0.0010 11 9 13 4.3126 -0.0114 11 9 14 -0.8257 0.0104 11 9 15 -2.5918 0.0048 11 9 16 0.8031 -0.0150 11 9 17 -0.5476 0.0084 11 9 18 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6 1.5536 -0.0445 12 0 8 1.9038 -0.0024 12 0 10 0.9813 -0.0085 12 0 12 -1.9737 -0.0079 12 0 14 -0.4312 -0.0179 12 0 16 1.2920 -0.0181 12 0 18 -0.4112 0.0013 12 0 20 -1.1147 -0.0133 12 1 0 0.1522 0.0831 12 1 1 0.8288 -0.0769 12 1 2 -0.7001 0.0284 12 1 3 1.6678 0.0453 12 1 4 -0.3005 -0.0345 12 1 5 0.8751 0.0305 12 1 6 -1.3486 -0.0001 12 1 7 -0.5681 0.0117 12 1 8 -0.1626 -0.0032 12 1 9 -0.8977 0.0454 12 1 10 2.1408 -0.0039 12 1 11 0.1465 -0.0027 12 1 12 0.3890 -0.0079 12 1 13 0.8967 0.0106 12 1 14 -1.1171 0.0096 12 1 15 -0.3058 -0.0075 12 1 16 -0.2913 0.0055 12 1 17 -1.5529 0.0025 12 1 18 1.9476 0.0004 12 1 19 -0.9591 0.0020 12 1 20 -0.0124 -0.0013 12 1 21 0.6190 0.0063 12 1 22 -2.2168 0.0018 12 1 23 0.3704 -0.0024 12 1 24 1.0196 -0.0081 12 2 0 -0.3722 0.0263 12 2 1 -3.6051 0.0262 12 2 2 -0.8539 0.0016 12 2 3 -0.2154 -0.0087 12 2 4 -0.0197 -0.0064 12 2 5 1.8258 -0.0199 12 2 6 -0.3067 0.0006 12 2 7 0.0951 -0.0157 12 2 8 -0.8035 -0.0043 12 2 9 -0.5273 0.0044 12 2 10 -0.7491 -0.0121 12 2 11 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12 3 28 0.4798 0.0072 12 3 29 3.4545 0.0063 12 4 0 0.5101 -0.0004 12 4 1 -0.1031 0.0124 12 4 2 1.3236 -0.0123 12 4 3 -0.3540 -0.0070 12 4 4 -0.1750 0.0057 12 4 5 0.0963 0.0002 12 4 6 -2.4310 0.0051 12 4 7 2.9080 0.0114 12 4 8 -0.9306 0.0087 12 4 9 -0.4348 0.0038 12 4 10 1.1321 0.0068 12 4 11 -0.4510 0.0084 12 4 12 0.1864 -0.0007 12 4 13 0.4742 -0.0021 12 4 14 -2.0043 0.0028 12 4 15 1.0910 0.0028 12 4 16 -1.9817 0.0062 12 4 17 -1.3542 0.0064 12 4 18 1.0322 0.0002 12 4 19 -1.7425 -0.0005 12 4 20 1.5711 -0.0062 12 4 21 -0.3108 0.0088 12 4 22 0.2464 0.0060 12 4 23 -1.5010 -0.0057 12 4 24 -1.1648 0.0082 12 4 25 2.7430 -0.0239 12 4 26 -0.4245 0.0006 12 4 27 -0.0817 -0.0047 12 4 28 0.3637 0.0032 12 4 29 -1.7292 -0.0062 12 4 30 0.1034 0.0067 12 4 31 2.0018 -0.0271 12 5 0 -1.3813 0.0079 12 5 1 -1.1113 0.0062 12 5 2 -0.0195 0.0069 12 5 3 -0.9543 0.0039 12 5 4 1.1110 -0.0012 12 5 5 0.5984 0.0025 12 5 6 -0.7594 -0.0191 12 5 7 -0.1120 -0.0010 12 5 8 -1.9922 -0.0107 12 5 9 -2.4502 -0.0049 12 5 10 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6 -0.9519 0.0022 13 4 7 1.1499 0.0037 13 4 8 1.8906 0.0143 13 4 9 -0.6550 -0.0097 13 4 10 2.6952 0.0024 13 4 11 -1.2716 -0.0113 13 4 12 0.2744 -0.0058 13 4 13 -0.4664 -0.0201 13 4 14 -0.6020 -0.0024 13 4 15 2.2894 -0.0016 13 4 16 0.8810 0.0047 13 4 17 -0.5139 0.0040 13 4 18 2.0250 -0.0063 13 4 19 -0.8152 -0.0086 13 4 20 0.5627 -0.0178 13 4 21 -1.1292 0.0159 13 4 22 -3.2145 -0.0060 13 4 23 1.7262 0.0131 13 4 24 -1.4662 -0.0011 13 4 26 1.2587 -0.0175 13 4 27 -2.5515 0.0283 13 5 0 -0.1783 -0.0003 13 5 1 -0.1701 -0.0048 13 5 2 0.6163 -0.0023 13 5 3 1.3159 -0.0027 13 5 4 0.0786 -0.0086 13 5 5 0.7481 -0.0167 13 5 6 -0.1174 -0.0053 13 5 7 -1.1014 0.0071 13 5 8 -1.3353 0.0061 13 5 9 0.8579 0.0071 13 5 10 0.1573 0.0041 13 5 11 2.0903 -0.0009 13 5 12 0.1719 0.0061 13 5 13 -1.5905 -0.0027 13 5 14 2.0815 -0.0068 13 5 15 -0.0123 0.0024 13 5 16 -0.2424 0.0023 13 5 17 1.0652 0.0020 13 5 18 -0.6528 -0.0048 13 5 19 -1.8635 -0.0178 13 5 20 2.3522 0.0034 13 5 21 1.2273 -0.0091 13 5 22 0.6956 0.0179 13 5 28 0.2915 0.0250 13 5 29 -1.6948 -0.0112 13 6 0 -0.4753 -0.0043 13 6 1 1.7148 0.0079 13 6 2 -0.7826 -0.0117 13 6 3 0.5133 0.0013 13 6 4 -0.4719 -0.0098 13 6 5 0.2856 -0.0096 13 6 6 0.4012 -0.0025 13 6 7 -1.8195 0.0014 13 6 8 1.1841 0.0149 13 6 9 -2.5245 0.0059 13 6 10 -0.2596 0.0003 13 6 11 1.1926 0.0100 13 6 12 0.5438 -0.0019 13 6 13 2.2802 -0.0080 13 6 14 -0.5737 0.0035 13 6 15 -1.4132 -0.0189 13 6 16 0.3849 0.0141 13 6 17 -1.3524 0.0039 13 6 18 0.9501 -0.0208 13 6 19 0.4594 -0.0011 13 6 20 0.4766 -0.0210 13 7 0 -0.8503 0.0077 13 7 1 2.2977 -0.0074 13 7 2 0.5829 0.0143 13 7 3 0.4410 -0.0070 13 7 4 0.9488 -0.0004 13 7 5 0.9729 -0.0069 13 7 6 -1.2839 -0.0031 13 7 7 2.5468 -0.0056 13 7 8 1.2793 0.0056 13 7 9 0.3930 0.0015 13 7 10 0.3413 -0.0026 13 7 11 -3.6795 0.0011 13 7 12 -1.4389 -0.0113 13 7 13 -0.1543 0.0140 13 7 14 2.1013 -0.0052 13 7 15 0.5066 0.0127 13 7 16 -0.6122 0.0065 13 7 17 0.3573 -0.0104 13 7 18 -2.0383 0.0066 13 8 0 -0.2210 -0.0003 13 8 1 -0.4539 0.0047 13 8 2 -0.3217 0.0202 13 8 3 2.4366 -0.0081 13 8 4 1.8135 0.0132 13 8 5 -1.1848 -0.0079 13 8 6 -1.5605 -0.0022 13 8 7 -0.9160 -0.0024 13 8 8 -1.8864 -0.0080 13 8 9 0.5527 -0.0061 13 8 10 1.3615 -0.0015 13 8 11 0.2638 -0.0242 13 8 12 -0.5080 0.0065 13 8 13 -0.1715 -0.0151 13 8 14 1.8807 -0.0059 13 8 15 0.1837 0.0323 13 9 0 -1.5616 0.0075 13 9 1 -0.9833 0.0021 13 9 2 -0.5242 0.0146 13 9 3 -0.5959 -0.0064 13 9 4 1.7010 0.0085 13 9 5 1.3386 -0.0163 13 9 6 1.2643 0.0060 13 9 7 0.7607 0.0035 13 9 8 -0.9115 0.0079 13 9 9 1.1694 0.0185 13 9 10 1.1869 0.0050 13 9 11 -2.6844 -0.0020 13 9 12 -0.1005 0.0078 13 10 0 -1.0831 0.0278 13 10 1 1.0443 -0.0112 13 10 2 -2.6968 0.0039 13 10 3 0.1612 0.0012 13 10 4 -0.4791 -0.0043 13 10 5 -1.4039 -0.0011 13 10 6 1.3081 0.0008 13 10 7 -0.1128 0.0006 14 0 0 -1.7476 -0.2014 14 0 2 2.0143 0.0883 14 0 4 0.1775 0.0236 14 0 6 0.2744 0.0382 14 0 8 1.2503 -0.0042 14 0 10 -0.7837 -0.0016 14 0 12 1.0332 0.0157 14 0 14 1.1838 0.0076 14 0 16 -2.0704 0.0166 14 0 18 -2.7817 0.0004 14 0 20 1.3692 0.0091 14 0 22 0.6639 -0.0008 14 1 0 -0.3221 -0.0409 14 1 1 1.1279 0.0767 14 1 2 0.0993 -0.0361 14 1 3 0.0330 -0.0008 14 1 4 -0.4088 0.0103 14 1 5 -1.4222 -0.0102 14 1 6 -0.4248 -0.0066 14 1 7 -0.3325 -0.0021 14 1 8 0.9900 0.0107 14 1 9 0.9658 -0.0476 14 1 10 -0.3571 0.0044 14 1 11 -0.4873 -0.0038 14 1 12 -1.5422 -0.0093 14 1 13 -1.8102 -0.0197 14 1 14 1.5661 -0.0109 14 1 15 -0.3686 -0.0063 14 1 16 1.7452 0.0169 14 1 17 0.7129 -0.0162 14 1 18 -1.9376 0.0030 14 1 19 1.1708 -0.0078 14 1 20 0.0024 -0.0068 14 1 21 0.8783 0.0134 14 1 22 0.9197 -0.0004 14 1 23 1.5664 -0.0068 14 1 24 -2.4762 -0.0231 14 2 0 0.4849 -0.0306 14 2 1 0.4740 -0.0288 14 2 2 -0.0367 0.0054 14 2 3 0.3890 -0.0141 14 2 4 0.3136 0.0073 14 2 5 0.0300 0.0152 14 2 6 -0.5923 -0.0100 14 2 7 -1.6652 0.0264 14 2 8 -0.5758 0.0029 14 2 9 0.2566 0.0126 14 2 10 1.9168 0.0099 14 2 11 3.1522 -0.0020 14 2 12 -1.3289 0.0018 14 2 13 -0.5109 -0.0115 14 2 14 -0.7505 -0.0042 14 2 15 -1.3593 0.0012 14 2 16 1.6509 -0.0039 14 2 17 0.2149 0.0016 14 2 18 -0.2014 -0.0035 14 2 19 -1.2692 -0.0273 14 2 20 -1.9048 0.0153 14 2 21 -1.6626 -0.0018 14 2 22 2.5820 0.0101 14 2 23 -0.7334 -0.0116 14 2 24 0.5789 0.0072 14 3 0 -0.1198 -0.0024 14 3 1 -0.1880 -0.0103 14 3 2 -0.1128 -0.0154 14 3 3 -0.2642 0.0064 14 3 4 -0.5454 0.0079 14 3 5 0.1013 -0.0022 14 3 6 0.7530 0.0144 14 3 7 -2.2196 0.0011 14 3 8 -0.0935 0.0034 14 3 9 -2.5549 0.0068 14 3 10 -0.4666 0.0057 14 3 11 1.0926 -0.0022 14 3 12 -0.9194 -0.0010 14 3 13 2.5760 -0.0013 14 3 14 -1.0909 0.0015 14 3 15 -3.7183 -0.0054 14 3 16 -0.4088 0.0116 14 3 17 -1.8312 -0.0020 14 3 18 -0.1926 -0.0088 14 3 19 3.4423 -0.0042 14 3 20 -0.3958 -0.0089 14 3 21 1.6532 0.0023 14 3 22 1.2753 0.0050 14 3 23 -0.8217 0.0140 14 4 0 -1.3298 0.0036 14 4 1 -0.6195 -0.0037 14 4 2 -0.9755 0.0015 14 4 3 -0.5015 -0.0090 14 4 4 -0.3761 -0.0209 14 4 5 0.9845 -0.0052 14 4 6 -0.1572 -0.0129 14 4 7 0.2580 -0.0110 14 4 8 1.9193 0.0025 14 4 9 -1.6505 0.0009 14 4 10 0.4769 0.0025 14 4 11 -2.9201 0.0078 14 4 12 -1.1250 -0.0009 14 4 13 3.4969 -0.0032 14 4 14 0.2408 -0.0025 14 4 15 2.7435 0.0151 14 4 16 0.9234 0.0029 14 4 17 -2.1744 -0.0017 14 4 18 0.1643 0.0000 14 4 19 -1.9033 -0.0288 14 4 20 -3.6091 -0.0019 14 4 21 -0.6773 0.0013 14 5 0 2.8429 -0.0093 14 5 1 0.6138 0.0185 14 5 2 -1.1469 0.0064 14 5 3 1.5934 -0.0061 14 5 4 0.0189 -0.0021 14 5 5 -3.1736 -0.0177 14 5 6 -0.7354 -0.0009 14 5 7 -0.8601 0.0023 14 5 8 -1.1151 -0.0025 14 5 9 1.8155 -0.0026 14 5 10 0.1145 0.0065 14 5 11 -2.5387 0.0049 14 5 12 1.5331 0.0022 14 5 13 -3.1123 -0.0010 14 5 14 1.2150 0.0116 14 5 15 0.9463 0.0069 14 5 16 -2.1136 0.0184 14 5 17 -0.4153 0.0151 14 5 18 0.0588 -0.0129 14 5 19 2.3442 0.0064 14 6 0 -0.6331 -0.0045 14 6 1 -1.9076 0.0102 14 6 2 0.7232 0.0028 14 6 3 -0.6571 0.0074 14 6 4 -1.7090 -0.0014 14 6 5 0.5474 -0.0051 14 6 6 0.4303 0.0043 14 6 7 -1.3531 -0.0049 14 6 8 0.2349 0.0072 14 6 9 0.3488 -0.0050 14 6 10 0.2359 -0.0065 14 6 11 0.8957 0.0014 14 6 12 -0.3321 -0.0273 14 6 13 -0.5605 -0.0096 14 6 14 -0.3292 0.0028 14 6 15 -1.7610 0.0007 14 6 16 2.6214 0.0185 14 6 17 0.6024 0.0061 14 7 0 -1.7850 0.0068 14 7 1 1.1526 -0.0062 14 7 2 2.6834 0.0099 14 7 3 -0.4885 0.0094 14 7 4 -0.6614 -0.0027 14 7 5 0.3670 0.0015 14 7 6 -0.5295 -0.0096 14 7 7 0.7356 0.0182 14 7 8 -0.1088 -0.0040 14 7 9 -1.7110 0.0022 14 7 10 -1.9934 0.0118 14 7 11 -2.1355 -0.0239 14 7 12 3.2253 0.0056 14 7 13 0.3594 0.0049 14 7 14 0.1233 -0.0267 14 7 15 0.3753 0.0099 14 8 0 -1.5133 0.0091 14 8 1 1.5957 -0.0011 14 8 2 0.0166 0.0158 14 8 3 0.5372 -0.0095 14 8 4 1.0363 0.0056 14 8 5 -1.2283 -0.0156 14 8 6 -2.1945 -0.0081 14 8 7 -1.0004 0.0053 14 8 8 1.8639 -0.0048 14 8 9 -0.0330 0.0267 14 8 10 -1.2745 0.0007 14 8 11 0.5019 -0.0005 14 9 0 -1.1413 0.0033 14 9 1 -1.8665 0.0025 14 9 2 -0.2397 -0.0041 14 9 3 0.6675 -0.0017 14 9 4 1.2753 -0.0066 14 9 5 1.1170 -0.0130 14 9 6 0.5228 0.0117 14 9 7 0.8901 -0.0064 15 0 0 -1.1295 0.1245 15 0 2 1.1573 0.0938 15 0 4 -0.9016 0.0076 15 0 6 -0.3175 0.0212 15 0 8 -0.1530 -0.0139 15 0 10 2.4782 0.0177 15 0 12 1.8041 0.0010 15 0 14 -0.3840 0.0161 15 0 16 -2.1107 0.0006 15 0 18 -0.9251 -0.0130 15 0 20 -0.4181 -0.0130 15 1 0 -0.1083 -0.0466 15 1 1 -0.5700 -0.0180 15 1 2 -1.0659 0.0291 15 1 3 -1.8611 -0.0724 15 1 4 0.1181 -0.0033 15 1 5 -0.9002 -0.0085 15 1 6 0.0392 -0.0062 15 1 7 0.6195 -0.0341 15 1 8 -1.6218 0.0127 15 1 9 1.1134 -0.0073 15 1 10 -1.8583 0.0078 15 1 11 -0.2921 0.0213 15 1 12 1.7498 -0.0104 15 1 13 0.0569 0.0171 15 1 14 2.1729 -0.0102 15 1 15 0.7663 0.0158 15 1 16 0.3512 0.0198 15 1 17 -0.4687 -0.0187 15 1 18 0.6593 0.0062 15 1 19 -1.2136 -0.0059 15 1 20 1.0098 0.0072 15 1 21 -0.4699 0.0096 15 1 22 -1.7695 0.0175 15 1 23 0.2890 0.0095 15 2 0 1.4498 0.0001 15 2 1 0.6550 -0.0003 15 2 2 -0.2322 0.0224 15 2 3 -0.2247 0.0252 15 2 4 0.1204 -0.0029 15 2 5 -0.4728 -0.0038 15 2 6 -0.5910 0.0010 15 2 7 -0.6613 -0.0068 15 2 8 1.8992 0.0060 15 2 9 1.6739 -0.0163 15 2 10 -0.7764 0.0117 15 2 11 0.4458 -0.0217 15 2 12 -0.8335 0.0178 15 2 13 -0.7093 -0.0166 15 2 14 1.0404 0.0131 15 2 15 1.2031 0.0217 15 2 16 -0.9513 -0.0036 15 2 17 0.5276 0.0206 15 2 18 -1.5023 -0.0072 15 2 19 -1.8232 -0.0085 15 2 20 1.5097 0.0041 15 2 21 -0.9906 0.0061 15 3 0 1.3116 0.0104 15 3 1 0.4129 0.0198 15 3 2 0.2086 0.0072 15 3 3 0.5071 0.0271 15 3 4 -0.0400 0.0088 15 3 5 -0.1324 -0.0045 15 3 6 -0.1723 -0.0067 15 3 7 -0.9909 -0.0063 15 3 8 -0.2099 -0.0043 15 3 9 0.5859 -0.0052 15 3 10 -1.0507 -0.0135 15 3 11 1.8938 -0.0002 15 3 12 -0.5177 -0.0150 15 3 13 -1.9360 -0.0087 15 3 14 0.6167 0.0137 15 3 15 -2.0465 0.0006 15 3 16 0.0483 0.0335 15 3 17 4.9503 0.0016 15 3 18 0.0575 0.0093 15 3 19 1.6676 -0.0024 15 3 20 0.8899 -0.0016 15 4 0 -1.2569 -0.0044 15 4 1 -0.7463 0.0029 15 4 2 1.9831 0.0006 15 4 3 0.0537 0.0036 15 4 4 1.5055 -0.0083 15 4 5 1.0896 0.0051 15 4 6 0.2276 0.0012 15 4 7 1.3667 0.0023 15 4 8 0.5224 0.0105 15 4 9 -1.9469 0.0038 15 4 10 0.1203 0.0064 15 4 11 0.7910 -0.0205 15 4 12 1.5631 -0.0125 15 4 13 3.7463 -0.0245 15 4 14 0.8329 -0.0115 15 4 15 -1.1971 0.0046 15 4 16 -1.2168 -0.0045 15 4 17 -0.9206 0.0081 15 4 18 -3.4439 0.0095 15 5 0 1.4050 0.0025 15 5 1 2.7714 0.0088 15 5 2 -1.4200 0.0156 15 5 3 -2.1249 -0.0101 15 5 4 1.5563 0.0066 15 5 5 -3.0025 0.0013 15 5 6 0.4123 0.0119 15 5 7 2.2629 0.0136 15 5 8 -0.1537 0.0071 15 5 9 1.1505 0.0289 15 5 10 -0.7826 -0.0036 15 5 11 -1.5624 0.0126 15 5 12 1.8237 -0.0107 15 5 13 -0.8607 -0.0154 15 5 14 0.2788 0.0061 15 5 15 0.0992 -0.0256 15 5 16 -0.7116 -0.0067 15 6 0 2.5596 -0.0084 15 6 1 -0.6912 0.0052 15 6 2 -0.0879 0.0004 15 6 3 2.3725 -0.0001 15 6 4 -1.2308 -0.0151 15 6 5 0.6222 -0.0088 15 6 6 1.5344 0.0002 15 6 7 -0.8525 -0.0071 15 6 8 2.0338 0.0271 15 6 9 -1.7582 0.0023 15 6 10 0.6120 0.0090 15 6 11 0.7554 0.0079 15 6 12 -1.9056 -0.0057 15 6 13 1.2480 0.0121 15 7 0 1.9655 0.0130 15 7 1 0.8201 0.0112 15 7 2 2.4735 0.0176 15 7 3 -0.1125 -0.0109 15 7 4 0.1630 -0.0140 15 7 5 0.5755 -0.0068 15 7 6 -0.8990 -0.0315 15 7 7 1.5280 0.0088 15 7 8 -2.2405 -0.0129 15 7 9 -1.9152 -0.0149 15 7 10 2.7471 0.0267 15 8 0 -2.5829 -0.0061 15 8 1 1.5457 0.0348 15 8 2 1.0486 0.0112 15 8 3 -0.4926 0.0039 15 8 4 0.9342 0.0019 15 8 5 -1.4126 -0.0118 16 0 0 2.7952 0.1669 16 0 2 0.6021 -0.0341 16 0 4 0.0327 -0.0138 16 0 6 -1.2261 -0.0158 16 0 8 0.8042 -0.0034 16 0 10 1.1158 -0.0096 16 0 12 -0.9791 -0.0133 16 0 14 0.3083 -0.0033 16 0 16 0.3986 -0.0147 16 0 18 0.2978 -0.0038 16 0 20 -0.5001 -0.0122 16 1 0 -1.4632 0.0265 16 1 1 -0.8290 -0.0573 16 1 2 -0.5587 0.0420 16 1 3 0.1404 0.0004 16 1 4 0.8778 -0.0179 16 1 5 0.1506 0.0375 16 1 6 -0.0316 -0.0076 16 1 7 -0.0806 0.0082 16 1 8 -1.3743 -0.0004 16 1 9 0.3325 0.0117 16 1 10 1.2910 0.0092 16 1 11 -0.3149 -0.0179 16 1 12 1.1195 -0.0108 16 1 13 -0.7440 -0.0010 16 1 14 -0.6810 -0.0062 16 1 15 -0.5909 0.0069 16 1 16 0.9703 0.0064 16 1 17 -0.1026 0.0026 16 1 18 -0.1788 -0.0074 16 1 19 1.0568 -0.0038 16 1 20 -0.8585 -0.0305 16 2 0 0.8954 0.0146 16 2 1 -1.3779 0.0273 16 2 2 -0.6244 0.0130 16 2 3 1.2931 -0.0050 16 2 4 -2.5893 0.0204 16 2 5 1.1823 -0.0243 16 2 6 0.3634 0.0219 16 2 7 0.4677 0.0070 16 2 8 0.3175 -0.0084 16 2 9 -0.6394 0.0127 16 2 10 -1.0557 -0.0098 16 2 11 0.2885 -0.0030 16 2 12 1.1727 -0.0101 16 2 13 0.4389 -0.0114 16 2 14 -1.4620 -0.0156 16 2 15 -0.7737 0.0028 16 2 16 0.0100 -0.0145 16 2 17 -2.5521 0.0079 16 2 18 1.5803 0.0001 16 2 19 -1.7522 -0.0538 16 3 0 0.4757 -0.0175 16 3 1 -1.2088 0.0197 16 3 2 0.6554 -0.0115 16 3 3 -0.0121 -0.0048 16 3 4 -0.3030 -0.0180 16 3 5 -0.0187 -0.0186 16 3 6 -0.5889 0.0160 16 3 7 0.6447 -0.0141 16 3 8 -1.1165 0.0355 16 3 9 -0.5855 0.0088 16 3 10 -1.3550 0.0143 16 3 11 -0.6088 0.0016 16 3 12 0.6746 0.0118 16 3 13 0.1049 -0.0057 16 3 14 -0.7030 -0.0042 16 3 15 4.5053 0.0001 16 3 16 -0.3820 0.0067 16 3 17 1.1898 -0.0027 16 4 0 -0.2944 0.0050 16 4 1 -1.3585 0.0033 16 4 2 0.7766 -0.0033 16 4 3 -0.5417 -0.0154 16 4 4 -1.4126 -0.0246 16 4 5 1.8755 -0.0102 16 4 6 -0.6375 -0.0236 16 4 7 0.1924 0.0085 16 4 8 0.7360 0.0077 16 4 9 -2.3670 0.0056 16 4 10 1.6294 0.0110 16 4 11 0.3573 0.0042 16 4 12 -0.1470 0.0149 16 4 13 -0.1761 -0.0075 16 4 14 -3.0801 0.0090 16 4 15 0.5146 0.0075 16 5 0 -1.2826 0.0171 16 5 1 -0.6127 0.0237 16 5 2 -0.2887 0.0062 16 5 3 -3.4896 0.0015 16 5 4 -0.3858 0.0014 16 5 5 0.7054 -0.0226 16 5 6 -0.3678 -0.0088 16 5 7 1.9988 -0.0082 16 5 8 -2.0405 -0.0170 16 5 9 0.7414 -0.0020 16 5 10 0.9058 -0.0141 16 5 11 -2.3859 0.0041 16 5 12 2.3752 -0.0004 16 6 0 1.6082 0.0289 16 6 1 -0.7376 0.0091 16 6 2 -0.9784 0.0126 16 6 3 0.3120 0.0097 16 6 4 -0.6845 -0.0060 16 6 5 -0.3200 -0.0034 16 6 6 0.8681 -0.0041 16 6 7 -3.1789 -0.0052 16 6 8 0.1244 0.0092 16 6 9 -0.8235 -0.0191 16 7 0 0.8188 0.0032 16 7 1 0.3699 -0.0072 16 7 2 1.0896 0.0065 16 7 3 -2.3499 -0.0067 16 7 4 -0.6700 -0.0015 17 0 0 -2.2341 -0.0540 17 0 2 -1.9466 -0.1043 17 0 4 -0.2489 -0.0243 17 0 6 0.0727 -0.0131 17 0 8 2.1440 0.0131 17 0 10 0.7633 -0.0081 17 0 12 0.8935 -0.0097 17 0 14 0.9597 -0.0104 17 0 16 -1.5499 0.0225 17 0 18 -2.8841 -0.0077 17 1 0 -0.8159 0.0541 17 1 1 -0.9178 -0.0122 17 1 2 -1.1345 -0.0050 17 1 3 0.5315 0.0220 17 1 4 -0.3333 -0.0264 17 1 5 -0.3386 0.0003 17 1 6 -0.5821 -0.0182 17 1 7 0.6911 0.0216 17 1 8 -0.1257 0.0021 17 1 9 1.0787 0.0098 17 1 10 1.2501 0.0230 17 1 11 -1.0760 0.0015 17 1 12 -0.6882 0.0041 17 1 13 -1.8815 0.0263 17 1 14 1.5522 -0.0126 17 1 15 0.3597 0.0440 17 1 16 1.1886 0.0100 17 1 17 0.4177 -0.0240 17 1 18 -0.8839 0.0110 17 2 0 0.3724 0.0040 17 2 1 0.6050 0.0418 17 2 2 -2.5272 -0.0172 17 2 3 0.4892 -0.0210 17 2 4 -1.3443 -0.0036 17 2 5 -0.2942 -0.0389 17 2 6 1.7655 -0.0190 17 2 7 -1.8378 -0.0168 17 2 8 -0.8578 -0.0233 17 2 9 0.2193 0.0020 17 2 10 1.2714 -0.0055 17 2 11 2.5553 0.0084 17 2 12 -1.2000 0.0021 17 2 13 -0.4006 -0.0139 17 2 14 -0.8711 0.0138 17 2 15 -1.3751 0.0287 17 3 0 0.0102 0.0289 17 3 1 2.1884 0.0057 17 3 2 0.5155 0.0228 17 3 3 0.7722 0.0030 17 3 4 -0.8009 -0.0127 17 3 5 0.1834 -0.0042 17 3 6 -0.5189 0.0010 17 3 7 -1.3150 -0.0093 17 3 8 -1.5005 -0.0105 17 3 9 -1.2831 -0.0006 17 3 10 1.0865 -0.0028 17 3 11 1.5096 -0.0146 17 3 12 1.1492 -0.0205 17 3 13 3.2771 0.0024 17 4 0 -0.3146 0.0104 17 4 1 -0.5780 0.0088 17 4 2 -1.8591 0.0198 17 4 3 3.0219 0.0005 17 4 4 0.1053 0.0101 17 4 5 2.7637 0.0097 17 4 6 1.4423 0.0111 17 4 7 -2.0883 0.0023 17 4 8 0.8990 0.0103 17 4 9 -1.8326 0.0088 17 4 10 -1.1937 0.0047 17 4 11 0.1279 -0.0089 17 5 0 1.7360 0.0009 17 5 1 -2.7674 0.0157 17 5 2 -0.9248 0.0056 17 5 3 -0.1483 0.0006 17 5 4 0.9575 -0.0028 17 5 5 2.0412 -0.0010 17 5 6 0.5902 -0.0071 17 5 7 2.0635 -0.0004 17 6 0 0.8918 0.0098 17 6 1 0.9684 0.0044 17 6 2 -0.8621 0.0072 18 0 0 -2.6100 -0.1425 18 0 2 0.7753 -0.0075 18 0 4 0.5341 0.0034 18 0 6 0.1901 0.0209 18 0 8 0.3006 0.0269 18 0 10 -0.1669 -0.0143 18 0 12 -0.0050 -0.0230 18 0 14 0.3286 0.0291 18 1 0 -0.7085 0.0128 18 1 1 1.5124 0.0495 18 1 2 -0.5991 -0.0113 18 1 3 0.2021 0.0210 18 1 4 1.6758 -0.0036 18 1 5 -0.4172 0.0292 18 1 6 0.6206 -0.0311 18 1 7 -0.4422 0.0555 18 1 8 0.4252 0.0014 18 1 9 -0.6909 -0.0124 18 1 10 -0.6560 0.0277 18 1 11 -1.7878 -0.0576 18 1 12 -0.8460 -0.0143 18 1 13 0.8845 -0.0167 18 1 14 0.7064 -0.0305 18 2 0 -1.4303 -0.0217 18 2 1 1.1487 0.0137 18 2 2 -2.3664 -0.0109 18 2 3 0.7848 -0.0176 18 2 4 1.1451 0.0149 18 2 5 0.7030 -0.0292 18 2 6 -0.5071 0.0153 18 2 7 -1.1266 0.0204 18 2 8 0.8330 0.0006 18 2 9 1.2976 0.0767 18 2 10 1.1106 -0.0243 18 2 11 0.0202 0.0235 18 2 12 -1.3787 -0.0205 18 3 0 0.4526 0.0218 18 3 1 -0.4669 -0.0177 18 3 2 0.3735 -0.0144 18 3 3 -1.6733 0.0044 18 3 4 0.4187 -0.0438 18 3 5 -0.1232 -0.0093 18 3 6 -1.4510 -0.0020 18 3 7 0.1203 -0.0070 18 3 8 -1.2000 0.0509 18 3 9 1.3249 -0.0021 18 4 0 -3.9914 0.0097 18 4 1 1.9574 0.0252 18 4 2 -0.1097 0.0127 18 4 3 2.6079 -0.0019 18 4 4 2.6235 -0.0088 18 4 5 -2.3726 -0.0210 19 1 0 -0.9375 -0.0361 19 1 1 -0.8081 0.0109 19 1 2 -0.1417 0.0029 19 1 3 -0.1662 -0.0709 19 1 4 0.4799 -0.0269 19 1 5 -0.4516 -0.0011 19 1 6 -1.0083 -0.0418 19 1 7 -0.1269 0.0266 19 1 8 -0.1410 0.0394 19 1 9 0.5154 -0.0330 19 1 10 -0.4097 0.0359 19 2 0 -1.2178 -0.0135 19 2 1 -0.6339 0.0547 19 2 2 0.4664 -0.0333 19 2 3 0.0743 -0.0088 19 2 4 0.1597 -0.0171 19 2 5 -1.1887 -0.0621 19 2 6 -0.3678 0.0048 19 2 7 -0.9865 0.0223 19 3 0 0.0292 0.0603 19 3 1 -1.1228 -0.0154 19 3 2 0.4494 -0.0033 19 3 3 0.6039 0.0202 20 2 0 -0.7034 -0.0153 0 0 0 0.0 0.0 ; _shelx_fab_checksum 70747 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.102 _oxdiff_exptl_absorpt_empirical_full_min 0.914 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3g _database_code_depnum_ccdc_archive 'CCDC 2116008' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT910_3g ; PROBLEM: Missing # of FCF Reflection(s) Below Theta(Min). 14 Note RESPONSE: The crystal was small and weakly diffracting ; # Added during the CSD deposition process: Friday 15 October 2021 05:10 PM # end Validation Reply Form _audit_creation_method SHELXL-2018/3 _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C70 H99 Mg2 N4 O2 Rh, 1.5(C6 H14)' _chemical_formula_sum 'C79 H120 Mg2 N4 O2 Rh' _chemical_formula_weight 1309.31 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 14.0176(4) _cell_length_b 13.9077(5) _cell_length_c 40.2691(10) _cell_angle_alpha 90 _cell_angle_beta 99.749(3) _cell_angle_gamma 90 _cell_volume 7737.2(4) _cell_formula_units_Z 4 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 8575 _cell_measurement_theta_min 2.9310 _cell_measurement_theta_max 27.6320 _exptl_crystal_description blocks _exptl_crystal_colour Yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.124 _exptl_crystal_F_000 2828 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.317 _exptl_crystal_size_mid 0.244 _exptl_crystal_size_min 0.157 _exptl_absorpt_coefficient_mu 0.282 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type analytical _exptl_absorpt_correction_T_min 0.937 _exptl_absorpt_correction_T_max 0.964 _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'Enhance (Mo) X-ray Source' _diffrn_measurement_device_type 'Agilent Xcalibur 3 E' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean 16.0382 _diffrn_reflns_number 31586 _diffrn_reflns_av_unetI/netI 0.0535 _diffrn_reflns_av_R_equivalents 0.0313 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_l_min -52 _diffrn_reflns_limit_l_max 49 _diffrn_reflns_theta_min 2.433 _diffrn_reflns_theta_max 28.390 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.808 _diffrn_measured_fraction_theta_full 0.992 _diffrn_reflns_Laue_measured_fraction_max 0.808 _diffrn_reflns_Laue_measured_fraction_full 0.992 _diffrn_reflns_point_group_measured_fraction_max 0.808 _diffrn_reflns_point_group_measured_fraction_full 0.992 _reflns_number_total 15686 _reflns_number_gt 11939 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro, Rigaku OD' _computing_cell_refinement 'CrysAlisPro, Rigaku OD' _computing_data_reduction 'CrysAlisPro, Rigaku OD' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2017)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2017)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0413P)^2^+2.9689P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 15686 _refine_ls_number_parameters 892 _refine_ls_number_restraints 239 _refine_ls_R_factor_all 0.0652 _refine_ls_R_factor_gt 0.0443 _refine_ls_wR_factor_ref 0.1068 _refine_ls_wR_factor_gt 0.0977 _refine_ls_goodness_of_fit_ref 1.020 _refine_ls_restrained_S_all 1.033 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rh1 Rh 0.33742(2) 0.35067(2) 0.05950(2) 0.03894(7) Uani 1 1 d . . . . . Mg1 Mg 0.59397(5) 0.25194(5) 0.14096(2) 0.02607(16) Uani 1 1 d . . . . . Mg2 Mg 0.43403(5) 0.40912(5) 0.17162(2) 0.02464(16) Uani 1 1 d . . . . . H1 H 0.5361(12) 0.3302(12) 0.1684(4) 0.006(4) Uiso 1 1 d . . . . . N1 N 0.73847(12) 0.25208(13) 0.16020(4) 0.0267(4) Uani 1 1 d . . . . . C1 C 0.78201(16) 0.17276(17) 0.17340(5) 0.0323(5) Uani 1 1 d . . . . . C2 C 0.74005(18) 0.08139(17) 0.17175(6) 0.0365(6) Uani 1 1 d . . . . . H2A H 0.774837 0.034528 0.186139 0.044 Uiso 1 1 calc R U . . . C3 C 0.65407(18) 0.04867(17) 0.15197(6) 0.0349(5) Uani 1 1 d . . . . . N3 N 0.58835(13) 0.10668(13) 0.13451(4) 0.0294(4) Uani 1 1 d . . . . . C4 C 0.88654(18) 0.1761(2) 0.19142(7) 0.0499(7) Uani 1 1 d . . . . . H4A H 0.926897 0.136766 0.179106 0.075 Uiso 1 1 calc R U . . . H4B H 0.890394 0.151003 0.214349 0.075 Uiso 1 1 calc R U . . . H4C H 0.909647 0.242724 0.192413 0.075 Uiso 1 1 calc R U . . . C5 C 0.6405(2) -0.05958(18) 0.15061(8) 0.0558(8) Uani 1 1 d . . . . . H5A H 0.584777 -0.076966 0.161127 0.084 Uiso 1 1 calc R U . . . H5B H 0.698808 -0.090832 0.162752 0.084 Uiso 1 1 calc R U . . . H5C H 0.629206 -0.080862 0.127069 0.084 Uiso 1 1 calc R U . . . C6 C 0.79469(15) 0.33876(16) 0.16024(5) 0.0278(5) Uani 1 1 d . . . . . C7 C 0.84038(16) 0.35843(18) 0.13233(6) 0.0361(6) Uani 1 1 d D . . . . C8 C 0.89474(17) 0.44170(19) 0.13263(6) 0.0410(6) Uani 1 1 d . . . . . H8A H 0.927135 0.454737 0.114225 0.049 Uiso 1 1 calc R U . . . C9 C 0.90296(17) 0.50594(19) 0.15891(7) 0.0407(6) Uani 1 1 d . . . . . H9A H 0.940749 0.562586 0.158726 0.049 Uiso 1 1 calc R U . . . C10 C 0.85546(17) 0.48697(18) 0.18563(6) 0.0377(6) Uani 1 1 d . . . . . H10A H 0.860509 0.531853 0.203629 0.045 Uiso 1 1 calc R U . . . C11 C 0.80076(15) 0.40455(16) 0.18696(5) 0.0288(5) Uani 1 1 d . . . . . C12 C 0.8367(6) 0.2838(7) 0.10411(18) 0.0408(18) Uani 0.610(16) 1 d D U P A 1 H12A H 0.794074 0.229392 0.108721 0.049 Uiso 0.610(16) 1 calc R U P A 1 C13 C 0.7926(7) 0.3305(6) 0.07067(16) 0.068(2) Uani 0.610(16) 1 d D U P A 1 H13A H 0.728363 0.355916 0.072285 0.102 Uiso 0.610(16) 1 calc R U P A 1 H13B H 0.834452 0.383190 0.065656 0.102 Uiso 0.610(16) 1 calc R U P A 1 H13C H 0.786890 0.282530 0.052630 0.102 Uiso 0.610(16) 1 calc R U P A 1 C14 C 0.9370(7) 0.2439(7) 0.10187(16) 0.078(3) Uani 0.610(16) 1 d D U P A 1 H14A H 0.964797 0.214041 0.123379 0.116 Uiso 0.610(16) 1 calc R U P A 1 H14B H 0.931512 0.195751 0.083879 0.116 Uiso 0.610(16) 1 calc R U P A 1 H14C H 0.979075 0.296411 0.096906 0.116 Uiso 0.610(16) 1 calc R U P A 1 C12' C 0.8231(12) 0.3013(9) 0.0995(3) 0.043(4) Uiso 0.390(16) 1 d D U P A 2 H12B H 0.756486 0.273696 0.097550 0.052 Uiso 0.390(16) 1 calc R U P A 2 C13' C 0.8250(9) 0.3565(8) 0.0675(3) 0.057(3) Uiso 0.390(16) 1 d D U P A 2 H13D H 0.813083 0.312489 0.048293 0.085 Uiso 0.390(16) 1 calc R U P A 2 H13E H 0.774729 0.406200 0.064973 0.085 Uiso 0.390(16) 1 calc R U P A 2 H13F H 0.888549 0.386860 0.068530 0.085 Uiso 0.390(16) 1 calc R U P A 2 C14' C 0.8923(10) 0.2159(8) 0.1027(3) 0.062(3) Uiso 0.390(16) 1 d D U P A 2 H14D H 0.889359 0.181498 0.123750 0.093 Uiso 0.390(16) 1 calc R U P A 2 H14E H 0.873545 0.172392 0.083575 0.093 Uiso 0.390(16) 1 calc R U P A 2 H14F H 0.958408 0.238955 0.102832 0.093 Uiso 0.390(16) 1 calc R U P A 2 C15 C 0.75195(17) 0.38756(17) 0.21749(6) 0.0339(5) Uani 1 1 d . . . . . H15A H 0.708952 0.330061 0.212770 0.041 Uiso 1 1 calc R U . . . C16 C 0.8264(2) 0.3665(2) 0.24897(7) 0.0620(9) Uani 1 1 d . . . . . H16A H 0.864057 0.309444 0.245077 0.093 Uiso 1 1 calc R U . . . H16B H 0.792946 0.354723 0.268082 0.093 Uiso 1 1 calc R U . . . H16C H 0.869880 0.421675 0.253961 0.093 Uiso 1 1 calc R U . . . C17 C 0.68971(18) 0.47238(19) 0.22456(7) 0.0435(6) Uani 1 1 d . . . . . H17A H 0.731064 0.528536 0.230851 0.065 Uiso 1 1 calc R U . . . H17B H 0.655368 0.456043 0.243065 0.065 Uiso 1 1 calc R U . . . H17C H 0.642652 0.487163 0.204305 0.065 Uiso 1 1 calc R U . . . C18 C 0.51538(17) 0.06311(16) 0.10921(6) 0.0352(6) Uani 1 1 d . . . . . C19 C 0.42495(19) 0.03972(18) 0.11691(6) 0.0434(6) Uani 1 1 d D . . . . C20 C 0.3572(2) -0.0016(2) 0.09134(8) 0.0633(9) Uani 1 1 d . . . . . H20A H 0.295177 -0.018873 0.095930 0.076 Uiso 1 1 calc R U . . . C21 C 0.3785(3) -0.0177(2) 0.05992(8) 0.0689(9) Uani 1 1 d . . . . . H21A H 0.331652 -0.046171 0.042991 0.083 Uiso 1 1 calc R U . . . C22 C 0.4664(2) 0.0070(3) 0.05290(8) 0.0696(10) Uani 1 1 d . . . . . H22A H 0.480043 -0.004421 0.030926 0.083 Uiso 1 1 calc R U . . . C23 C 0.5373(2) 0.0487(2) 0.07698(7) 0.0517(7) Uani 1 1 d D . . . . C24 C 0.4039(5) 0.0500(5) 0.15246(15) 0.0447(16) Uani 0.693(11) 1 d D U P B 1 H24A H 0.465578 0.065666 0.167939 0.054 Uiso 0.693(11) 1 calc R U P B 1 C25 C 0.3600(5) -0.0405(4) 0.16526(15) 0.075(2) Uani 0.693(11) 1 d D U P B 1 H25A H 0.405201 -0.094296 0.165384 0.112 Uiso 0.693(11) 1 calc R U P B 1 H25B H 0.347598 -0.029371 0.188180 0.112 Uiso 0.693(11) 1 calc R U P B 1 H25C H 0.299013 -0.055842 0.150418 0.112 Uiso 0.693(11) 1 calc R U P B 1 C26 C 0.3347(7) 0.1334(4) 0.15217(15) 0.074(2) Uani 0.693(11) 1 d D U P B 1 H26A H 0.319345 0.142442 0.174815 0.111 Uiso 0.693(11) 1 calc R U P B 1 H26B H 0.364855 0.192009 0.145210 0.111 Uiso 0.693(11) 1 calc R U P B 1 H26C H 0.275157 0.119955 0.136305 0.111 Uiso 0.693(11) 1 calc R U P B 1 C24' C 0.3915(13) 0.0731(13) 0.1495(4) 0.050(5) Uiso 0.307(11) 1 d D U P B 2 H24B H 0.434797 0.127903 0.158074 0.059 Uiso 0.307(11) 1 calc R U P B 2 C25' C 0.4138(12) -0.0074(11) 0.1762(4) 0.082(4) Uiso 0.307(11) 1 d D U P B 2 H25D H 0.480188 -0.030407 0.176856 0.123 Uiso 0.307(11) 1 calc R U P B 2 H25E H 0.406889 0.017973 0.198378 0.123 Uiso 0.307(11) 1 calc R U P B 2 H25F H 0.368476 -0.060847 0.170333 0.123 Uiso 0.307(11) 1 calc R U P B 2 C26' C 0.2899(10) 0.1098(13) 0.1479(4) 0.079(5) Uiso 0.307(11) 1 d D U P B 2 H26D H 0.279821 0.128070 0.170544 0.119 Uiso 0.307(11) 1 calc R U P B 2 H26E H 0.279856 0.165991 0.133025 0.119 Uiso 0.307(11) 1 calc R U P B 2 H26F H 0.243754 0.059246 0.139072 0.119 Uiso 0.307(11) 1 calc R U P B 2 C27 C 0.6349(3) 0.0742(5) 0.06784(13) 0.0714(16) Uani 0.805(18) 1 d D U P C 1 H27A H 0.674503 0.106625 0.087680 0.086 Uiso 0.805(18) 1 calc R U P C 1 C28 C 0.6246(5) 0.1428(5) 0.03801(17) 0.094(2) Uani 0.805(18) 1 d D U P C 1 H28A H 0.688800 0.157696 0.032818 0.140 Uiso 0.805(18) 1 calc R U P C 1 H28B H 0.585002 0.112652 0.018379 0.140 Uiso 0.805(18) 1 calc R U P C 1 H28C H 0.593360 0.202285 0.043627 0.140 Uiso 0.805(18) 1 calc R U P C 1 C29 C 0.6882(7) -0.0173(6) 0.0600(3) 0.120(3) Uani 0.805(18) 1 d D U P C 1 H29A H 0.751007 0.000123 0.054179 0.180 Uiso 0.805(18) 1 calc R U P C 1 H29B H 0.698142 -0.059188 0.079887 0.180 Uiso 0.805(18) 1 calc R U P C 1 H29C H 0.649408 -0.051158 0.041068 0.180 Uiso 0.805(18) 1 calc R U P C 1 C27' C 0.6334(14) 0.080(2) 0.0678(8) 0.092(6) Uiso 0.195(18) 1 d D U P C 2 H27B H 0.653235 0.137757 0.082239 0.110 Uiso 0.195(18) 1 calc R U P C 2 C28' C 0.628(3) 0.116(3) 0.0318(6) 0.083(6) Uiso 0.195(18) 1 d D U P C 2 H28D H 0.692660 0.134596 0.028065 0.124 Uiso 0.195(18) 1 calc R U P C 2 H28E H 0.603035 0.064345 0.016056 0.124 Uiso 0.195(18) 1 calc R U P C 2 H28F H 0.584487 0.171454 0.028018 0.124 Uiso 0.195(18) 1 calc R U P C 2 C29' C 0.7181(18) 0.0103(19) 0.0756(8) 0.085(6) Uiso 0.195(18) 1 d D U P C 2 H29D H 0.775578 0.038528 0.068548 0.127 Uiso 0.195(18) 1 calc R U P C 2 H29E H 0.731533 -0.002686 0.099840 0.127 Uiso 0.195(18) 1 calc R U P C 2 H29F H 0.701641 -0.050019 0.063337 0.127 Uiso 0.195(18) 1 calc R U P C 2 N31 N 0.40357(12) 0.39505(12) 0.21904(4) 0.0214(4) Uani 1 1 d . . . . . C31 C 0.41969(14) 0.46662(15) 0.24129(5) 0.0225(4) Uani 1 1 d . . . . . C32 C 0.44856(14) 0.55926(15) 0.23337(5) 0.0241(5) Uani 1 1 d . . . . . H32A H 0.471707 0.598757 0.252272 0.029 Uiso 1 1 calc R U . . . C33 C 0.44859(14) 0.60259(15) 0.20202(5) 0.0248(5) Uani 1 1 d . . . . . N33 N 0.43486(12) 0.55583(12) 0.17288(4) 0.0230(4) Uani 1 1 d . . . . . C34 C 0.40292(18) 0.45244(17) 0.27715(5) 0.0350(5) Uani 1 1 d . . . . . H34A H 0.333480 0.456626 0.277816 0.052 Uiso 1 1 calc R U . . . H34B H 0.437360 0.502454 0.291605 0.052 Uiso 1 1 calc R U . . . H34C H 0.427079 0.389057 0.285244 0.052 Uiso 1 1 calc R U . . . C35 C 0.46119(18) 0.71100(17) 0.20283(6) 0.0391(6) Uani 1 1 d . . . . . H35A H 0.488765 0.731604 0.183196 0.059 Uiso 1 1 calc R U . . . H35B H 0.504833 0.729536 0.223493 0.059 Uiso 1 1 calc R U . . . H35C H 0.398119 0.741861 0.202341 0.059 Uiso 1 1 calc R U . . . C36 C 0.36916(15) 0.30502(15) 0.23025(5) 0.0244(5) Uani 1 1 d . . . . . C37 C 0.26919(16) 0.28616(16) 0.22492(5) 0.0296(5) Uani 1 1 d . . . . . C38 C 0.23806(18) 0.19916(17) 0.23633(6) 0.0394(6) Uani 1 1 d . . . . . H38A H 0.170707 0.185499 0.232946 0.047 Uiso 1 1 calc R U . . . C39 C 0.30219(19) 0.13231(18) 0.25240(7) 0.0434(6) Uani 1 1 d . . . . . H39A H 0.279114 0.074363 0.260699 0.052 Uiso 1 1 calc R U . . . C40 C 0.40001(19) 0.15012(17) 0.25634(6) 0.0406(6) Uani 1 1 d . . . . . H40A H 0.444105 0.103003 0.266869 0.049 Uiso 1 1 calc R U . . . C41 C 0.43593(16) 0.23547(16) 0.24528(5) 0.0307(5) Uani 1 1 d . . . . . C42 C 0.19450(16) 0.35601(17) 0.20699(6) 0.0344(5) Uani 1 1 d . . . . . H42A H 0.228859 0.416196 0.202255 0.041 Uiso 1 1 calc R U . . . C43 C 0.14396(18) 0.3143(2) 0.17311(7) 0.0488(7) Uani 1 1 d . . . . . H43A H 0.192238 0.301459 0.158687 0.073 Uiso 1 1 calc R U . . . H43B H 0.096356 0.360619 0.161969 0.073 Uiso 1 1 calc R U . . . H43C H 0.111128 0.254251 0.177127 0.073 Uiso 1 1 calc R U . . . C44 C 0.11827(18) 0.3826(2) 0.22842(7) 0.0464(7) Uani 1 1 d . . . . . H44A H 0.080120 0.325444 0.231815 0.070 Uiso 1 1 calc R U . . . H44B H 0.075439 0.432282 0.216867 0.070 Uiso 1 1 calc R U . . . H44C H 0.150353 0.406971 0.250306 0.070 Uiso 1 1 calc R U . . . C45 C 0.54467(16) 0.25068(17) 0.25003(6) 0.0341(5) Uani 1 1 d . . . . . H45A H 0.556864 0.313013 0.239093 0.041 Uiso 1 1 calc R U . . . C46 C 0.59022(19) 0.2571(2) 0.28750(6) 0.0498(7) Uani 1 1 d . . . . . H46A H 0.564546 0.313524 0.297606 0.075 Uiso 1 1 calc R U . . . H46B H 0.660649 0.262978 0.289575 0.075 Uiso 1 1 calc R U . . . H46C H 0.574476 0.198915 0.299186 0.075 Uiso 1 1 calc R U . . . C47 C 0.59298(19) 0.17084(18) 0.23279(6) 0.0437(6) Uani 1 1 d . . . . . H47A H 0.581795 0.108842 0.243036 0.066 Uiso 1 1 calc R U . . . H47B H 0.662720 0.183084 0.235514 0.066 Uiso 1 1 calc R U . . . H47C H 0.565415 0.169370 0.208742 0.066 Uiso 1 1 calc R U . . . C48 C 0.41277(16) 0.61107(16) 0.14218(5) 0.0288(5) Uani 1 1 d . . . . . C49 C 0.48314(17) 0.62194(17) 0.12149(6) 0.0367(6) Uani 1 1 d . . . . . C50 C 0.4587(2) 0.6742(2) 0.09186(7) 0.0553(8) Uani 1 1 d . . . . . H50A H 0.505389 0.682595 0.077543 0.066 Uiso 1 1 calc R U . . . C51 C 0.3685(2) 0.7138(2) 0.08289(7) 0.0624(9) Uani 1 1 d . . . . . H51A H 0.353562 0.749709 0.062611 0.075 Uiso 1 1 calc R U . . . C52 C 0.2998(2) 0.7019(2) 0.10301(7) 0.0535(8) Uani 1 1 d . . . . . H52A H 0.237190 0.728644 0.096244 0.064 Uiso 1 1 calc R U . . . C53 C 0.32014(17) 0.65126(18) 0.13316(6) 0.0374(6) Uani 1 1 d . . . . . C54 C 0.58510(18) 0.58263(19) 0.13146(7) 0.0430(6) Uani 1 1 d . . . . . H54A H 0.582574 0.531334 0.148687 0.052 Uiso 1 1 calc R U . . . C55 C 0.6539(2) 0.6596(3) 0.14779(9) 0.0748(10) Uani 1 1 d . . . . . H55A H 0.656776 0.712027 0.131724 0.112 Uiso 1 1 calc R U . . . H55B H 0.718603 0.631967 0.154471 0.112 Uiso 1 1 calc R U . . . H55C H 0.630813 0.684687 0.167755 0.112 Uiso 1 1 calc R U . . . C56 C 0.6246(2) 0.5369(2) 0.10228(8) 0.0614(8) Uani 1 1 d . . . . . H56A H 0.576604 0.492031 0.090427 0.092 Uiso 1 1 calc R U . . . H56B H 0.684367 0.502002 0.110945 0.092 Uiso 1 1 calc R U . . . H56C H 0.638200 0.587107 0.086670 0.092 Uiso 1 1 calc R U . . . C57 C 0.24135(17) 0.6394(2) 0.15466(7) 0.0468(7) Uani 1 1 d . . . . . H57A H 0.272643 0.613587 0.177053 0.056 Uiso 1 1 calc R U . . . C58 C 0.1666(2) 0.5666(2) 0.13904(10) 0.0735(10) Uani 1 1 d . . . . . H58A H 0.134575 0.589891 0.116981 0.110 Uiso 1 1 calc R U . . . H58B H 0.118320 0.557614 0.153758 0.110 Uiso 1 1 calc R U . . . H58C H 0.198488 0.505086 0.136263 0.110 Uiso 1 1 calc R U . . . C59 C 0.1918(2) 0.7341(2) 0.16094(9) 0.0672(9) Uani 1 1 d . . . . . H59A H 0.240521 0.780217 0.171503 0.101 Uiso 1 1 calc R U . . . H59B H 0.144642 0.722560 0.175895 0.101 Uiso 1 1 calc R U . . . H59C H 0.158580 0.760100 0.139455 0.101 Uiso 1 1 calc R U . . . C60 C 0.4516(4) 0.3216(4) 0.08130(18) 0.0363(14) Uani 0.589(17) 1 d D U P D 1 C61 C 0.2970(7) 0.3733(4) 0.10207(10) 0.0423(17) Uani 0.589(17) 1 d D U P D 1 H61A H 0.229698 0.386075 0.099998 0.051 Uiso 0.589(17) 1 calc R U P D 1 C60' C 0.4709(8) 0.3184(6) 0.0709(3) 0.045(3) Uiso 0.411(17) 1 d D U P D 2 H60B H 0.499484 0.313824 0.051209 0.054 Uiso 0.411(17) 1 calc R U P D 2 C61' C 0.3391(11) 0.3642(7) 0.1021(2) 0.051(3) Uiso 0.411(17) 1 d D U P D 2 O60 O 0.53207(12) 0.30146(13) 0.09654(4) 0.0406(4) Uani 1 1 d D . . . . O61 O 0.34066(12) 0.37497(13) 0.13239(4) 0.0452(4) Uani 1 1 d D . . . . C62 C 0.3189(2) 0.3274(2) 0.00288(6) 0.0502(7) Uani 1 1 d . . . . . C63 C 0.3036(2) 0.4268(2) 0.00790(7) 0.0596(8) Uani 1 1 d . . . . . C64 C 0.2226(2) 0.4361(3) 0.02372(7) 0.0669(9) Uani 1 1 d . . . . . C65 C 0.1865(2) 0.3418(3) 0.02818(7) 0.0652(10) Uani 1 1 d . . . . . C66 C 0.2451(2) 0.2751(2) 0.01457(6) 0.0536(8) Uani 1 1 d . . . . . C67 C 0.3953(2) 0.2851(3) -0.01520(7) 0.0783(11) Uani 1 1 d . . . . . H67A H 0.452184 0.327203 -0.012094 0.117 Uiso 1 1 calc R U . . . H67B H 0.369272 0.279405 -0.039291 0.117 Uiso 1 1 calc R U . . . H67C H 0.413877 0.221372 -0.005946 0.117 Uiso 1 1 calc R U . . . C68 C 0.3606(3) 0.5089(3) -0.00333(10) 0.1052(15) Uani 1 1 d . . . . . H68A H 0.427669 0.488610 -0.003001 0.158 Uiso 1 1 calc R U . . . H68B H 0.359425 0.563586 0.011968 0.158 Uiso 1 1 calc R U . . . H68C H 0.331704 0.528085 -0.026253 0.158 Uiso 1 1 calc R U . . . C69 C 0.1759(3) 0.5289(3) 0.03195(10) 0.1200(18) Uani 1 1 d . . . . . H69A H 0.124966 0.546754 0.013180 0.180 Uiso 1 1 calc R U . . . H69B H 0.224855 0.579926 0.035612 0.180 Uiso 1 1 calc R U . . . H69C H 0.147666 0.520429 0.052413 0.180 Uiso 1 1 calc R U . . . C70 C 0.0956(2) 0.3181(4) 0.04203(10) 0.1152(18) Uani 1 1 d . . . . . H70A H 0.098870 0.251438 0.050030 0.173 Uiso 1 1 calc R U . . . H70B H 0.039137 0.326026 0.024242 0.173 Uiso 1 1 calc R U . . . H70C H 0.090002 0.361421 0.060787 0.173 Uiso 1 1 calc R U . . . C71 C 0.2301(3) 0.1686(3) 0.01128(9) 0.0851(12) Uani 1 1 d . . . . . H71A H 0.198193 0.145438 0.029608 0.128 Uiso 1 1 calc R U . . . H71B H 0.292904 0.136576 0.012514 0.128 Uiso 1 1 calc R U . . . H71C H 0.189476 0.154136 -0.010420 0.128 Uiso 1 1 calc R U . . . C81 C 0.3572(3) 0.3230(3) 0.47851(10) 0.0828(11) Uani 1 1 d . . . . . H81A H 0.330095 0.349905 0.456441 0.124 Uiso 1 1 calc R U . . . H81B H 0.305385 0.292871 0.488443 0.124 Uiso 1 1 calc R U . . . H81C H 0.406152 0.274596 0.475824 0.124 Uiso 1 1 calc R U . . . C82 C 0.4026(3) 0.4012(3) 0.50106(10) 0.0831(11) Uani 1 1 d . . . . . H82A H 0.350359 0.443277 0.506432 0.100 Uiso 1 1 calc R U . . . H82B H 0.434401 0.371563 0.522445 0.100 Uiso 1 1 calc R U . . . C83 C 0.4742(2) 0.4622(2) 0.48844(8) 0.0672(9) Uani 1 1 d . . . . . H83A H 0.441058 0.494889 0.467842 0.081 Uiso 1 1 calc R U . . . H83B H 0.523883 0.419448 0.481565 0.081 Uiso 1 1 calc R U . . . C91 C 1.0458(10) 0.9941(10) 0.1202(5) 0.139(4) Uani 0.649(7) 1 d D U P E 1 H91A H 1.013990 1.033793 0.101421 0.208 Uiso 0.649(7) 1 calc R U P E 1 H91B H 1.103993 0.964628 0.114163 0.208 Uiso 0.649(7) 1 calc R U P E 1 H91C H 1.063827 1.034406 0.140233 0.208 Uiso 0.649(7) 1 calc R U P E 1 C92 C 0.9777(6) 0.9168(6) 0.12747(16) 0.103(3) Uani 0.649(7) 1 d D U P E 1 H92A H 0.918077 0.947241 0.132695 0.124 Uiso 0.649(7) 1 calc R U P E 1 H92B H 1.008175 0.880756 0.147696 0.124 Uiso 0.649(7) 1 calc R U P E 1 C93 C 0.9500(4) 0.8464(4) 0.09845(14) 0.082(2) Uani 0.649(7) 1 d D U P E 1 H93A H 0.912998 0.880911 0.078916 0.098 Uiso 0.649(7) 1 calc R U P E 1 H93B H 1.009630 0.820716 0.091597 0.098 Uiso 0.649(7) 1 calc R U P E 1 C94 C 0.8904(5) 0.7644(5) 0.10776(15) 0.105(3) Uani 0.649(7) 1 d D . P E 1 H94A H 0.834398 0.791365 0.116663 0.126 Uiso 0.649(7) 1 calc R U P E 1 H94B H 0.929959 0.727990 0.126272 0.126 Uiso 0.649(7) 1 calc R U P E 1 C95 C 0.8529(5) 0.6952(6) 0.08001(19) 0.109(3) Uani 0.649(7) 1 d D U P E 1 H95A H 0.815020 0.645417 0.089612 0.131 Uiso 0.649(7) 1 calc R U P E 1 H95B H 0.807071 0.730721 0.062932 0.131 Uiso 0.649(7) 1 calc R U P E 1 C96 C 0.9213(8) 0.6460(8) 0.0625(2) 0.096(3) Uani 0.649(7) 1 d D U P E 1 H96A H 0.970217 0.613477 0.078951 0.144 Uiso 0.649(7) 1 calc R U P E 1 H96B H 0.952858 0.692914 0.049800 0.144 Uiso 0.649(7) 1 calc R U P E 1 H96C H 0.886783 0.598451 0.046958 0.144 Uiso 0.649(7) 1 calc R U P E 1 C91' C 1.0467(18) 0.975(2) 0.1170(12) 0.148(8) Uiso 0.351(7) 1 d D U P E 2 H91F H 1.055592 1.044453 0.118084 0.222 Uiso 0.351(7) 1 calc R U P E 2 H91G H 1.086897 0.944613 0.136513 0.222 Uiso 0.351(7) 1 calc R U P E 2 H91H H 1.065835 0.950050 0.096238 0.222 Uiso 0.351(7) 1 calc R U P E 2 C92' C 0.9450(13) 0.9516(10) 0.1170(5) 0.144(7) Uiso 0.351(7) 1 d D U P E 2 H91D H 0.906807 0.985934 0.097712 0.173 Uiso 0.351(7) 1 calc R U P E 2 H91E H 0.927712 0.980538 0.137686 0.173 Uiso 0.351(7) 1 calc R U P E 2 C93' C 0.9094(11) 0.8510(9) 0.1155(4) 0.111(5) Uiso 0.351(7) 1 d D U P E 2 H93C H 0.929894 0.822781 0.138197 0.134 Uiso 0.351(7) 1 calc R U P E 2 H93D H 0.837834 0.853868 0.111684 0.134 Uiso 0.351(7) 1 calc R U P E 2 C94' C 0.9369(11) 0.7816(9) 0.0908(4) 0.101(5) Uiso 0.351(7) 1 d D U P E 2 H94C H 0.927614 0.816302 0.069058 0.121 Uiso 0.351(7) 1 calc R U P E 2 H94D H 1.007605 0.772319 0.097429 0.121 Uiso 0.351(7) 1 calc R U P E 2 C95' C 0.8981(15) 0.6883(11) 0.0833(6) 0.132(7) Uiso 0.351(7) 1 d D U P E 2 H95C H 0.828170 0.697558 0.074804 0.159 Uiso 0.351(7) 1 calc R U P E 2 H95D H 0.902632 0.654737 0.105207 0.159 Uiso 0.351(7) 1 calc R U P E 2 C96' C 0.933(2) 0.6186(16) 0.0600(7) 0.124(7) Uiso 0.351(7) 1 d D U P E 2 H96D H 0.894365 0.559508 0.059054 0.186 Uiso 0.351(7) 1 calc R U P E 2 H96E H 0.925860 0.646826 0.037391 0.186 Uiso 0.351(7) 1 calc R U P E 2 H96F H 1.001070 0.603574 0.068100 0.186 Uiso 0.351(7) 1 calc R U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh1 0.03640(12) 0.05291(14) 0.02407(10) -0.00162(9) -0.00473(8) -0.00118(10) Mg1 0.0234(4) 0.0254(4) 0.0281(4) -0.0044(3) 0.0006(3) 0.0020(3) Mg2 0.0307(4) 0.0229(4) 0.0214(3) 0.0001(3) 0.0076(3) 0.0015(3) N1 0.0244(9) 0.0288(10) 0.0258(9) -0.0038(8) 0.0014(8) 0.0039(8) C1 0.0302(12) 0.0386(14) 0.0269(11) -0.0041(10) 0.0016(10) 0.0089(11) C2 0.0441(15) 0.0298(13) 0.0337(12) 0.0018(10) 0.0008(11) 0.0128(12) C3 0.0466(15) 0.0271(12) 0.0315(12) -0.0051(10) 0.0076(11) 0.0042(12) N3 0.0340(10) 0.0257(10) 0.0276(9) -0.0064(8) 0.0029(8) -0.0002(9) C4 0.0359(14) 0.0521(17) 0.0546(16) 0.0010(14) -0.0130(12) 0.0135(13) C5 0.071(2) 0.0295(14) 0.0630(18) -0.0027(13) -0.0002(16) 0.0055(14) C6 0.0176(10) 0.0342(13) 0.0298(11) -0.0011(10) -0.0012(9) 0.0033(10) C7 0.0241(12) 0.0474(15) 0.0373(13) -0.0054(12) 0.0067(10) 0.0030(11) C8 0.0295(13) 0.0517(16) 0.0445(14) -0.0005(13) 0.0136(11) -0.0025(12) C9 0.0283(13) 0.0417(15) 0.0524(15) -0.0003(13) 0.0077(12) -0.0050(11) C10 0.0312(13) 0.0392(14) 0.0418(14) -0.0091(12) 0.0031(11) -0.0012(11) C11 0.0209(11) 0.0330(13) 0.0309(11) -0.0024(10) -0.0002(9) 0.0017(10) C12 0.044(4) 0.050(4) 0.031(3) -0.006(3) 0.017(3) 0.000(3) C13 0.086(5) 0.072(4) 0.041(3) -0.010(3) -0.005(3) -0.010(4) C14 0.070(5) 0.096(5) 0.068(4) -0.043(4) 0.017(3) 0.021(4) C15 0.0364(13) 0.0347(13) 0.0299(12) -0.0063(10) 0.0038(10) -0.0030(11) C16 0.0626(19) 0.083(2) 0.0388(15) 0.0078(15) 0.0047(14) 0.0224(17) C17 0.0366(14) 0.0493(16) 0.0453(15) -0.0092(13) 0.0090(12) 0.0012(12) C18 0.0413(14) 0.0257(12) 0.0369(13) -0.0101(10) 0.0018(11) -0.0037(11) C19 0.0490(16) 0.0363(14) 0.0436(14) -0.0063(12) 0.0043(12) -0.0144(13) C20 0.0546(18) 0.065(2) 0.069(2) -0.0110(17) 0.0076(16) -0.0306(16) C21 0.071(2) 0.072(2) 0.060(2) -0.0248(17) -0.0019(17) -0.0330(19) C22 0.079(2) 0.086(2) 0.0431(16) -0.0314(17) 0.0089(16) -0.025(2) C23 0.0535(17) 0.0607(18) 0.0401(14) -0.0262(14) 0.0058(13) -0.0123(15) C24 0.044(3) 0.050(4) 0.040(3) 0.004(3) 0.009(2) -0.009(3) C25 0.096(5) 0.064(3) 0.070(3) 0.018(3) 0.027(3) -0.016(3) C26 0.105(6) 0.055(3) 0.069(3) -0.015(3) 0.033(4) -0.003(3) C27 0.057(2) 0.122(4) 0.039(2) -0.043(2) 0.0190(17) -0.019(2) C28 0.098(4) 0.111(5) 0.084(4) -0.041(3) 0.050(3) -0.041(4) C29 0.095(5) 0.169(6) 0.107(5) -0.004(5) 0.048(4) 0.030(4) N31 0.0213(9) 0.0225(9) 0.0204(8) 0.0007(7) 0.0033(7) 0.0002(7) C31 0.0175(10) 0.0296(12) 0.0201(10) -0.0003(9) 0.0025(8) 0.0040(9) C32 0.0209(10) 0.0267(11) 0.0238(10) -0.0062(9) 0.0012(9) 0.0006(9) C33 0.0164(10) 0.0239(11) 0.0332(11) -0.0017(9) 0.0019(9) 0.0007(9) N33 0.0214(9) 0.0232(9) 0.0242(9) 0.0025(8) 0.0032(7) 0.0016(8) C34 0.0461(14) 0.0361(13) 0.0236(11) -0.0030(10) 0.0084(10) 0.0026(12) C35 0.0454(15) 0.0275(13) 0.0446(14) -0.0027(11) 0.0086(12) -0.0024(11) C36 0.0320(12) 0.0232(11) 0.0193(10) 0.0003(9) 0.0084(9) -0.0012(10) C37 0.0313(12) 0.0286(12) 0.0312(12) -0.0017(10) 0.0115(10) -0.0042(10) C38 0.0344(13) 0.0348(14) 0.0521(15) 0.0026(12) 0.0159(12) -0.0070(12) C39 0.0519(16) 0.0300(13) 0.0531(16) 0.0103(12) 0.0227(13) -0.0060(12) C40 0.0474(15) 0.0311(13) 0.0453(14) 0.0138(12) 0.0133(12) 0.0046(12) C41 0.0353(13) 0.0273(12) 0.0306(12) 0.0044(10) 0.0091(10) 0.0012(10) C42 0.0250(12) 0.0320(13) 0.0464(14) 0.0036(11) 0.0067(10) -0.0035(10) C43 0.0346(14) 0.0590(18) 0.0509(16) 0.0000(14) 0.0021(12) -0.0001(13) C44 0.0374(14) 0.0431(15) 0.0600(17) -0.0029(13) 0.0121(13) 0.0040(12) C45 0.0338(13) 0.0316(13) 0.0365(13) 0.0092(11) 0.0051(10) 0.0049(11) C46 0.0481(16) 0.0532(17) 0.0444(15) -0.0014(13) -0.0028(13) 0.0081(14) C47 0.0424(15) 0.0451(16) 0.0449(14) 0.0105(12) 0.0112(12) 0.0106(12) C48 0.0318(12) 0.0249(11) 0.0291(11) 0.0059(10) 0.0035(10) 0.0012(10) C49 0.0389(14) 0.0358(13) 0.0373(13) 0.0140(11) 0.0118(11) 0.0074(11) C50 0.0570(18) 0.068(2) 0.0467(16) 0.0292(15) 0.0244(14) 0.0147(16) C51 0.065(2) 0.074(2) 0.0482(17) 0.0343(16) 0.0093(15) 0.0204(17) C52 0.0434(16) 0.0634(19) 0.0522(17) 0.0261(15) 0.0036(13) 0.0176(15) C53 0.0312(13) 0.0398(14) 0.0404(13) 0.0117(12) 0.0034(11) 0.0064(11) C54 0.0393(14) 0.0451(15) 0.0494(15) 0.0202(13) 0.0212(12) 0.0114(13) C55 0.0424(17) 0.086(3) 0.092(3) -0.020(2) 0.0024(17) 0.0154(18) C56 0.0570(18) 0.0523(18) 0.081(2) 0.0020(16) 0.0303(17) 0.0092(15) C57 0.0277(13) 0.0584(18) 0.0541(16) 0.0198(14) 0.0062(12) 0.0115(13) C58 0.0408(17) 0.071(2) 0.111(3) 0.007(2) 0.0198(18) -0.0026(16) C59 0.0530(18) 0.076(2) 0.077(2) 0.0094(18) 0.0228(17) 0.0206(17) C60 0.039(3) 0.052(3) 0.020(2) 0.001(2) 0.011(2) -0.003(2) C61 0.037(4) 0.067(4) 0.022(2) -0.016(2) -0.002(2) 0.010(3) O60 0.0389(10) 0.0515(11) 0.0284(8) 0.0026(8) -0.0031(7) 0.0047(9) O61 0.0415(10) 0.0622(12) 0.0291(9) -0.0106(8) -0.0023(8) -0.0009(9) C62 0.0440(16) 0.078(2) 0.0246(12) 0.0011(13) -0.0043(11) -0.0026(15) C63 0.063(2) 0.073(2) 0.0354(15) 0.0113(15) -0.0138(14) -0.0009(18) C64 0.059(2) 0.089(3) 0.0417(16) -0.0097(17) -0.0222(15) 0.019(2) C65 0.0354(16) 0.124(3) 0.0314(14) -0.0086(18) -0.0081(12) -0.0034(19) C66 0.0514(17) 0.076(2) 0.0278(13) -0.0041(14) -0.0090(12) -0.0141(16) C67 0.072(2) 0.129(3) 0.0354(16) -0.0042(19) 0.0114(15) 0.005(2) C68 0.131(4) 0.097(3) 0.077(3) 0.040(2) -0.014(2) -0.026(3) C69 0.120(4) 0.128(4) 0.089(3) -0.027(3) -0.047(3) 0.070(3) C70 0.0415(19) 0.235(6) 0.068(2) -0.022(3) 0.0058(17) -0.017(3) C71 0.102(3) 0.086(3) 0.060(2) -0.0111(19) -0.008(2) -0.035(2) C81 0.071(2) 0.080(3) 0.096(3) -0.017(2) 0.010(2) 0.004(2) C82 0.076(2) 0.093(3) 0.083(3) -0.005(2) 0.021(2) 0.005(2) C83 0.056(2) 0.080(2) 0.066(2) -0.0056(17) 0.0108(16) 0.0156(18) C91 0.163(8) 0.124(8) 0.122(8) -0.020(6) 0.004(6) 0.035(6) C92 0.114(6) 0.127(6) 0.065(4) -0.005(4) 0.001(4) 0.046(5) C93 0.073(4) 0.116(6) 0.057(3) 0.024(4) 0.015(3) 0.026(4) C94 0.071(4) 0.179(9) 0.066(4) 0.029(5) 0.012(3) -0.030(5) C95 0.055(4) 0.174(8) 0.088(5) 0.051(5) -0.015(4) -0.031(4) C96 0.106(6) 0.110(7) 0.059(4) 0.023(5) -0.026(4) -0.018(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh1 C61' 1.721(9) . ? Rh1 C60 1.737(5) . ? Rh1 C60' 1.903(10) . ? Rh1 C61 1.920(6) . ? Rh1 C62 2.274(2) . ? Rh1 C65 2.275(3) . ? Rh1 C66 2.294(3) . ? Rh1 C64 2.301(3) . ? Rh1 C63 2.309(3) . ? Mg1 O60 1.9754(17) . ? Mg1 N3 2.0367(19) . ? Mg1 N1 2.0424(18) . ? Mg1 Mg2 3.5023(10) . ? Mg2 O61 1.9325(17) . ? Mg2 N31 2.0355(17) . ? Mg2 N33 2.0410(18) . ? N1 C1 1.327(3) . ? N1 C6 1.440(3) . ? C1 C2 1.397(3) . ? C1 C4 1.522(3) . ? C2 C3 1.403(3) . ? C3 N3 1.332(3) . ? C3 C5 1.517(3) . ? N3 C18 1.449(3) . ? C6 C11 1.404(3) . ? C6 C7 1.411(3) . ? C7 C8 1.385(3) . ? C7 C12' 1.525(12) . ? C7 C12 1.534(6) . ? C8 C9 1.375(4) . ? C9 C10 1.383(3) . ? C10 C11 1.385(3) . ? C11 C15 1.523(3) . ? C12 C13 1.528(8) . ? C12 C14 1.529(8) . ? C12' C13' 1.504(12) . ? C12' C14' 1.525(11) . ? C15 C17 1.522(3) . ? C15 C16 1.528(3) . ? C18 C19 1.394(3) . ? C18 C23 1.398(3) . ? C19 C20 1.400(4) . ? C19 C24 1.516(5) . ? C19 C24' 1.537(13) . ? C20 C21 1.367(4) . ? C21 C22 1.353(4) . ? C22 C23 1.392(4) . ? C23 C27 1.518(5) . ? C23 C27' 1.522(17) . ? C24 C26 1.511(7) . ? C24 C25 1.529(7) . ? C24' C26' 1.504(13) . ? C24' C25' 1.549(13) . ? C27 C28 1.522(6) . ? C27 C29 1.535(7) . ? C27' C28' 1.521(15) . ? C27' C29' 1.527(16) . ? N31 C31 1.333(3) . ? N31 C36 1.442(3) . ? C31 C32 1.403(3) . ? C31 C34 1.515(3) . ? C32 C33 1.399(3) . ? C33 N33 1.327(3) . ? C33 C35 1.518(3) . ? N33 C48 1.444(3) . ? C36 C37 1.406(3) . ? C36 C41 1.409(3) . ? C37 C38 1.390(3) . ? C37 C42 1.518(3) . ? C38 C39 1.376(4) . ? C39 C40 1.376(3) . ? C40 C41 1.392(3) . ? C41 C45 1.519(3) . ? C42 C44 1.528(3) . ? C42 C43 1.540(3) . ? C45 C47 1.527(3) . ? C45 C46 1.538(3) . ? C48 C49 1.403(3) . ? C48 C53 1.404(3) . ? C49 C50 1.389(3) . ? C49 C54 1.519(3) . ? C50 C51 1.370(4) . ? C51 C52 1.369(4) . ? C52 C53 1.391(3) . ? C53 C57 1.523(3) . ? C54 C55 1.515(4) . ? C54 C56 1.520(4) . ? C57 C58 1.515(4) . ? C57 C59 1.530(4) . ? C60 O60 1.222(5) . ? C61 O61 1.270(5) . ? C60' O60 1.247(9) . ? C61' O61 1.226(9) . ? C62 C66 1.410(4) . ? C62 C63 1.419(4) . ? C62 C67 1.512(4) . ? C63 C64 1.399(4) . ? C63 C68 1.506(5) . ? C64 C65 1.428(5) . ? C64 C69 1.509(5) . ? C65 C66 1.411(4) . ? C65 C70 1.511(4) . ? C66 C71 1.498(4) . ? C81 C82 1.490(5) . ? C82 C83 1.468(5) . ? C83 C83 1.507(6) 3_666 ? C91 C92 1.499(11) . ? C92 C93 1.524(8) . ? C93 C94 1.498(7) . ? C94 C95 1.501(8) . ? C95 C96 1.453(9) . ? C91' C92' 1.462(14) . ? C92' C93' 1.483(12) . ? C93' C94' 1.482(12) . ? C94' C95' 1.420(12) . ? C95' C96' 1.489(13) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C61' Rh1 C60' 86.4(4) . . ? C60 Rh1 C61 88.4(2) . . ? C61' Rh1 C62 174.0(4) . . ? C60 Rh1 C62 114.3(3) . . ? C60' Rh1 C62 98.6(4) . . ? C61 Rh1 C62 156.6(3) . . ? C61' Rh1 C65 114.4(5) . . ? C60 Rh1 C65 163.3(2) . . ? C60' Rh1 C65 154.8(4) . . ? C61 Rh1 C65 96.7(3) . . ? C62 Rh1 C65 59.93(10) . . ? C61' Rh1 C66 138.3(4) . . ? C60 Rh1 C66 129.8(2) . . ? C60' Rh1 C66 118.9(4) . . ? C61 Rh1 C66 124.6(2) . . ? C62 Rh1 C66 35.96(10) . . ? C65 Rh1 C66 35.96(11) . . ? C61' Rh1 C64 117.3(5) . . ? C60 Rh1 C64 157.4(2) . . ? C60' Rh1 C64 145.9(4) . . ? C61 Rh1 C64 101.2(3) . . ? C62 Rh1 C64 59.77(11) . . ? C65 Rh1 C64 36.36(12) . . ? C66 Rh1 C64 60.10(12) . . ? C61' Rh1 C63 144.4(4) . . ? C60 Rh1 C63 126.3(3) . . ? C60' Rh1 C63 111.7(4) . . ? C61 Rh1 C63 133.0(2) . . ? C62 Rh1 C63 36.05(11) . . ? C65 Rh1 C63 59.74(12) . . ? C66 Rh1 C63 59.87(11) . . ? C64 Rh1 C63 35.33(11) . . ? O60 Mg1 N3 103.22(8) . . ? O60 Mg1 N1 126.76(8) . . ? N3 Mg1 N1 93.65(8) . . ? O60 Mg1 Mg2 83.83(6) . . ? N3 Mg1 Mg2 130.61(6) . . ? N1 Mg1 Mg2 121.25(6) . . ? O61 Mg2 N31 121.51(8) . . ? O61 Mg2 N33 105.44(8) . . ? N31 Mg2 N33 94.24(7) . . ? O61 Mg2 Mg1 86.78(6) . . ? N31 Mg2 Mg1 121.28(5) . . ? N33 Mg2 Mg1 129.16(5) . . ? C1 N1 C6 118.74(18) . . ? C1 N1 Mg1 120.69(15) . . ? C6 N1 Mg1 120.57(13) . . ? N1 C1 C2 125.1(2) . . ? N1 C1 C4 120.4(2) . . ? C2 C1 C4 114.5(2) . . ? C1 C2 C3 129.5(2) . . ? N3 C3 C2 123.6(2) . . ? N3 C3 C5 120.7(2) . . ? C2 C3 C5 115.6(2) . . ? C3 N3 C18 117.43(19) . . ? C3 N3 Mg1 121.68(15) . . ? C18 N3 Mg1 120.80(14) . . ? C11 C6 C7 120.5(2) . . ? C11 C6 N1 120.57(19) . . ? C7 C6 N1 118.91(19) . . ? C8 C7 C6 118.6(2) . . ? C8 C7 C12' 116.7(6) . . ? C6 C7 C12' 124.2(7) . . ? C8 C7 C12 121.5(4) . . ? C6 C7 C12 119.7(4) . . ? C9 C8 C7 121.6(2) . . ? C8 C9 C10 119.1(2) . . ? C9 C10 C11 122.0(2) . . ? C10 C11 C6 118.2(2) . . ? C10 C11 C15 119.1(2) . . ? C6 C11 C15 122.7(2) . . ? C13 C12 C14 109.9(5) . . ? C13 C12 C7 108.8(6) . . ? C14 C12 C7 111.9(5) . . ? C13' C12' C7 116.9(10) . . ? C13' C12' C14' 111.4(10) . . ? C7 C12' C14' 109.1(9) . . ? C17 C15 C11 112.4(2) . . ? C17 C15 C16 109.0(2) . . ? C11 C15 C16 111.3(2) . . ? C19 C18 C23 121.6(2) . . ? C19 C18 N3 120.1(2) . . ? C23 C18 N3 118.2(2) . . ? C18 C19 C20 117.5(2) . . ? C18 C19 C24 121.2(3) . . ? C20 C19 C24 121.1(3) . . ? C18 C19 C24' 122.7(8) . . ? C20 C19 C24' 118.9(8) . . ? C21 C20 C19 121.4(3) . . ? C22 C21 C20 120.1(3) . . ? C21 C22 C23 121.8(3) . . ? C22 C23 C18 117.6(3) . . ? C22 C23 C27 119.7(3) . . ? C18 C23 C27 122.7(3) . . ? C22 C23 C27' 120.5(13) . . ? C18 C23 C27' 121.8(13) . . ? C26 C24 C19 107.0(5) . . ? C26 C24 C25 109.9(5) . . ? C19 C24 C25 113.2(5) . . ? C26' C24' C19 119.4(13) . . ? C26' C24' C25' 110.7(11) . . ? C19 C24' C25' 108.7(11) . . ? C23 C27 C28 111.7(5) . . ? C23 C27 C29 110.2(5) . . ? C28 C27 C29 110.0(4) . . ? C23 C27' C28' 115(2) . . ? C23 C27' C29' 117(2) . . ? C28' C27' C29' 108.4(15) . . ? C31 N31 C36 117.76(16) . . ? C31 N31 Mg2 121.35(14) . . ? C36 N31 Mg2 120.78(12) . . ? N31 C31 C32 123.76(18) . . ? N31 C31 C34 120.51(19) . . ? C32 C31 C34 115.68(18) . . ? C33 C32 C31 130.14(19) . . ? N33 C33 C32 124.4(2) . . ? N33 C33 C35 120.34(19) . . ? C32 C33 C35 115.22(19) . . ? C33 N33 C48 118.31(18) . . ? C33 N33 Mg2 120.76(14) . . ? C48 N33 Mg2 120.74(14) . . ? C37 C36 C41 120.7(2) . . ? C37 C36 N31 119.46(18) . . ? C41 C36 N31 119.84(18) . . ? C38 C37 C36 118.2(2) . . ? C38 C37 C42 119.0(2) . . ? C36 C37 C42 122.85(19) . . ? C39 C38 C37 121.8(2) . . ? C40 C39 C38 119.4(2) . . ? C39 C40 C41 121.6(2) . . ? C40 C41 C36 118.2(2) . . ? C40 C41 C45 119.2(2) . . ? C36 C41 C45 122.54(19) . . ? C37 C42 C44 112.2(2) . . ? C37 C42 C43 110.9(2) . . ? C44 C42 C43 109.3(2) . . ? C41 C45 C47 110.7(2) . . ? C41 C45 C46 111.9(2) . . ? C47 C45 C46 110.2(2) . . ? C49 C48 C53 121.1(2) . . ? C49 C48 N33 119.70(19) . . ? C53 C48 N33 119.22(19) . . ? C50 C49 C48 118.1(2) . . ? C50 C49 C54 120.0(2) . . ? C48 C49 C54 121.9(2) . . ? C51 C50 C49 121.3(2) . . ? C52 C51 C50 120.3(2) . . ? C51 C52 C53 121.1(2) . . ? C52 C53 C48 118.1(2) . . ? C52 C53 C57 119.4(2) . . ? C48 C53 C57 122.5(2) . . ? C55 C54 C49 111.2(2) . . ? C55 C54 C56 110.1(2) . . ? C49 C54 C56 113.3(2) . . ? C58 C57 C53 110.7(2) . . ? C58 C57 C59 110.0(2) . . ? C53 C57 C59 113.2(2) . . ? O60 C60 Rh1 179.7(7) . . ? O61 C61 Rh1 134.0(7) . . ? O60 C60' Rh1 139.0(11) . . ? O61 C61' Rh1 179.2(8) . . ? C60 O60 Mg1 139.6(4) . . ? C60' O60 Mg1 161.8(6) . . ? C61' O61 Mg2 137.7(7) . . ? C61 O61 Mg2 160.0(4) . . ? C66 C62 C63 108.6(3) . . ? C66 C62 C67 125.4(3) . . ? C63 C62 C67 125.8(3) . . ? C66 C62 Rh1 72.78(14) . . ? C63 C62 Rh1 73.32(15) . . ? C67 C62 Rh1 124.65(19) . . ? C64 C63 C62 108.0(3) . . ? C64 C63 C68 125.4(4) . . ? C62 C63 C68 126.6(3) . . ? C64 C63 Rh1 72.00(17) . . ? C62 C63 Rh1 70.63(15) . . ? C68 C63 Rh1 125.4(2) . . ? C63 C64 C65 107.7(3) . . ? C63 C64 C69 126.5(4) . . ? C65 C64 C69 125.6(4) . . ? C63 C64 Rh1 72.66(17) . . ? C65 C64 Rh1 70.86(17) . . ? C69 C64 Rh1 126.0(2) . . ? C66 C65 C64 108.3(3) . . ? C66 C65 C70 125.6(4) . . ? C64 C65 C70 125.9(4) . . ? C66 C65 Rh1 72.73(15) . . ? C64 C65 Rh1 72.78(16) . . ? C70 C65 Rh1 124.7(2) . . ? C62 C66 C65 107.3(3) . . ? C62 C66 C71 125.5(3) . . ? C65 C66 C71 127.1(3) . . ? C62 C66 Rh1 71.25(15) . . ? C65 C66 Rh1 71.31(15) . . ? C71 C66 Rh1 125.1(2) . . ? C83 C82 C81 117.2(3) . . ? C82 C83 C83 118.3(4) . 3_666 ? C91 C92 C93 113.5(9) . . ? C94 C93 C92 112.2(6) . . ? C93 C94 C95 116.2(5) . . ? C96 C95 C94 119.1(6) . . ? C91' C92' C93' 121.8(14) . . ? C94' C93' C92' 121.2(12) . . ? C95' C94' C93' 127.1(14) . . ? C94' C95' C96' 125.1(16) . . ? _refine_diff_density_max 0.388 _refine_diff_density_min -0.577 _refine_diff_density_rms 0.049 _shelx_res_file ; TITL MRC2137 in P2(1)/n MRC2137.res created by SHELXL-2018/3 at 13:38:38 on 11-Jun-2021 REM P2(1)/n (#14 in standard setting) REM JMP181 CELL 0.71073 14.017641 13.907675 40.269119 90.0000 99.7488 90.0000 ZERR 4.00 0.000421 0.000454 0.001033 0.0000 0.0028 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H Mg N O Rh UNIT 316 480 8 16 8 4 TEMP -100 L.S. 12 OMIT 1 1 2 OMIT 1 0 3 FMAP 2 PLAN 10 ACTA REM 'C70 H99 Mg2 N4 O2 Rh, 1.5(C6 H14)' REM C79 H120 Mg2 N4 O2 Rh RTAB MG-H MG1 H1 RTAB MG-H MG2 H1 RTAB MHM MG1 H1 MG2 SADI C7 C12 C7 C12' SADI C12 C13 C12 C14 C12' C13' C12' C14' SADI C13 C14 C13' C14' SIMU 0.02 0.02 1 C12 > C14' SADI C19 C24 C19 C24' SADI C24 C25 C24 C26 C24' C25' C24' C26' SADI C25 C26 C25' C26' SIMU 0.02 0.02 1 C24 > C26' SADI C23 C27 C23 C27' SADI C27 C28 C27 C29 C27' C28' C27' C29' SADI C28 C29 C28' C29' SIMU 0.02 0.02 2 C27 > C29' SADI C60 O60 C61' O61 SADI C60' O60 C61 O61 SIMU 0.02 0.02 1 C60 C60' SIMU 0.02 0.02 1 C61 C61' SADI C91 C92 C92 C93 C93 C94 C94 C95 C95 C96 = C91' C92' C92' C93' C93' C94' C94' C95' C95' C96' SADI C91 C93 C92 C94 C93 C95 C94 C96 = C91' C93' C92' C94' C93' C95' C94' C96' SIMU 0.02 0.02 1 C91 > C96' WGHT 0.041300 2.968900 FVAR 2.44621 0.61024 0.69286 0.80468 0.58856 0.64880 RH1 6 0.337419 0.350675 0.059504 11.00000 0.03640 0.05291 = 0.02407 -0.00162 -0.00473 -0.00118 MG1 3 0.593969 0.251944 0.140965 11.00000 0.02338 0.02539 = 0.02813 -0.00443 0.00063 0.00200 MG2 3 0.434033 0.409118 0.171621 11.00000 0.03075 0.02286 = 0.02141 0.00011 0.00760 0.00147 H1 2 0.536144 0.330211 0.168366 11.00000 0.00616 N1 4 0.738468 0.252075 0.160199 11.00000 0.02439 0.02879 = 0.02580 -0.00383 0.00136 0.00388 C1 1 0.782010 0.172757 0.173403 11.00000 0.03016 0.03861 = 0.02694 -0.00414 0.00163 0.00894 C2 1 0.740051 0.081392 0.171753 11.00000 0.04409 0.02979 = 0.03370 0.00176 0.00076 0.01284 AFIX 43 H2A 2 0.774837 0.034528 0.186139 11.00000 -1.20000 AFIX 0 C3 1 0.654068 0.048672 0.151968 11.00000 0.04661 0.02706 = 0.03150 -0.00506 0.00764 0.00422 N3 4 0.588350 0.106682 0.134512 11.00000 0.03398 0.02565 = 0.02763 -0.00638 0.00285 -0.00017 C4 1 0.886540 0.176111 0.191422 11.00000 0.03591 0.05207 = 0.05455 0.00095 -0.01304 0.01354 AFIX 137 H4A 2 0.926897 0.136766 0.179106 11.00000 -1.50000 H4B 2 0.890394 0.151003 0.214349 11.00000 -1.50000 H4C 2 0.909647 0.242724 0.192413 11.00000 -1.50000 AFIX 0 C5 1 0.640515 -0.059581 0.150609 11.00000 0.07090 0.02948 = 0.06304 -0.00268 -0.00017 0.00547 AFIX 137 H5A 2 0.584777 -0.076966 0.161127 11.00000 -1.50000 H5B 2 0.698808 -0.090832 0.162752 11.00000 -1.50000 H5C 2 0.629206 -0.080862 0.127069 11.00000 -1.50000 AFIX 0 C6 1 0.794689 0.338763 0.160240 11.00000 0.01756 0.03416 = 0.02976 -0.00111 -0.00125 0.00332 C7 1 0.840384 0.358428 0.132333 11.00000 0.02413 0.04736 = 0.03731 -0.00537 0.00671 0.00301 C8 1 0.894740 0.441698 0.132632 11.00000 0.02952 0.05167 = 0.04450 -0.00053 0.01360 -0.00245 AFIX 43 H8A 2 0.927135 0.454737 0.114225 11.00000 -1.20000 AFIX 0 C9 1 0.902963 0.505945 0.158914 11.00000 0.02828 0.04166 = 0.05244 -0.00027 0.00775 -0.00499 AFIX 43 H9A 2 0.940749 0.562586 0.158726 11.00000 -1.20000 AFIX 0 C10 1 0.855461 0.486970 0.185632 11.00000 0.03116 0.03920 = 0.04180 -0.00914 0.00310 -0.00116 AFIX 43 H10A 2 0.860509 0.531853 0.203629 11.00000 -1.20000 AFIX 0 C11 1 0.800757 0.404547 0.186959 11.00000 0.02089 0.03300 = 0.03088 -0.00238 -0.00023 0.00169 PART 1 C12 1 0.836650 0.283764 0.104110 21.00000 0.04429 0.05039 = 0.03141 -0.00606 0.01682 0.00045 AFIX 13 H12A 2 0.794074 0.229392 0.108721 21.00000 -1.20000 AFIX 0 C13 1 0.792641 0.330546 0.070671 21.00000 0.08633 0.07206 = 0.04057 -0.00965 -0.00470 -0.01007 AFIX 33 H13A 2 0.728363 0.355916 0.072285 21.00000 -1.50000 H13B 2 0.834452 0.383190 0.065656 21.00000 -1.50000 H13C 2 0.786890 0.282530 0.052630 21.00000 -1.50000 AFIX 0 C14 1 0.937018 0.243915 0.101867 21.00000 0.07001 0.09593 = 0.06843 -0.04303 0.01701 0.02116 AFIX 33 H14A 2 0.964797 0.214041 0.123379 21.00000 -1.50000 H14B 2 0.931512 0.195751 0.083879 21.00000 -1.50000 H14C 2 0.979075 0.296411 0.096906 21.00000 -1.50000 AFIX 0 PART 2 C12' 1 0.823078 0.301321 0.099548 -21.00000 0.04294 AFIX 13 H12B 2 0.756486 0.273696 0.097550 -21.00000 -1.20000 AFIX 0 C13' 1 0.825030 0.356527 0.067548 -21.00000 0.05659 AFIX 33 H13D 2 0.813083 0.312489 0.048293 -21.00000 -1.50000 H13E 2 0.774729 0.406200 0.064973 -21.00000 -1.50000 H13F 2 0.888549 0.386860 0.068530 -21.00000 -1.50000 AFIX 0 C14' 1 0.892283 0.215908 0.102709 -21.00000 0.06227 AFIX 33 H14D 2 0.889359 0.181498 0.123750 -21.00000 -1.50000 H14E 2 0.873545 0.172392 0.083575 -21.00000 -1.50000 H14F 2 0.958408 0.238955 0.102832 -21.00000 -1.50000 AFIX 0 PART 0 C15 1 0.751949 0.387556 0.217492 11.00000 0.03639 0.03467 = 0.02992 -0.00626 0.00375 -0.00298 AFIX 13 H15A 2 0.708952 0.330061 0.212770 11.00000 -1.20000 AFIX 0 C16 1 0.826379 0.366458 0.248975 11.00000 0.06260 0.08331 = 0.03884 0.00776 0.00468 0.02237 AFIX 137 H16A 2 0.864057 0.309444 0.245077 11.00000 -1.50000 H16B 2 0.792946 0.354723 0.268082 11.00000 -1.50000 H16C 2 0.869880 0.421675 0.253961 11.00000 -1.50000 AFIX 0 C17 1 0.689715 0.472380 0.224558 11.00000 0.03658 0.04928 = 0.04535 -0.00919 0.00895 0.00120 AFIX 137 H17A 2 0.731064 0.528536 0.230851 11.00000 -1.50000 H17B 2 0.655368 0.456043 0.243065 11.00000 -1.50000 H17C 2 0.642652 0.487163 0.204305 11.00000 -1.50000 AFIX 0 C18 1 0.515382 0.063114 0.109209 11.00000 0.04134 0.02565 = 0.03687 -0.01005 0.00179 -0.00371 C19 1 0.424947 0.039716 0.116913 11.00000 0.04901 0.03633 = 0.04358 -0.00634 0.00432 -0.01435 C20 1 0.357222 -0.001622 0.091343 11.00000 0.05465 0.06489 = 0.06928 -0.01102 0.00763 -0.03058 AFIX 43 H20A 2 0.295177 -0.018873 0.095930 11.00000 -1.20000 AFIX 0 C21 1 0.378547 -0.017661 0.059924 11.00000 0.07064 0.07154 = 0.06009 -0.02482 -0.00194 -0.03305 AFIX 43 H21A 2 0.331652 -0.046171 0.042991 11.00000 -1.20000 AFIX 0 C22 1 0.466386 0.007020 0.052902 11.00000 0.07911 0.08606 = 0.04306 -0.03143 0.00893 -0.02475 AFIX 43 H22A 2 0.480043 -0.004421 0.030926 11.00000 -1.20000 AFIX 0 C23 1 0.537260 0.048695 0.076983 11.00000 0.05350 0.06070 = 0.04008 -0.02624 0.00585 -0.01227 PART 1 C24 1 0.403940 0.050037 0.152458 31.00000 0.04398 0.05024 = 0.04044 0.00360 0.00903 -0.00925 AFIX 13 H24A 2 0.465578 0.065666 0.167939 31.00000 -1.20000 AFIX 0 C25 1 0.359993 -0.040495 0.165259 31.00000 0.09565 0.06351 = 0.06956 0.01780 0.02702 -0.01591 AFIX 33 H25A 2 0.405201 -0.094296 0.165384 31.00000 -1.50000 H25B 2 0.347598 -0.029371 0.188180 31.00000 -1.50000 H25C 2 0.299013 -0.055842 0.150418 31.00000 -1.50000 AFIX 0 C26 1 0.334747 0.133436 0.152172 31.00000 0.10532 0.05451 = 0.06863 -0.01451 0.03313 -0.00269 AFIX 33 H26A 2 0.319345 0.142442 0.174815 31.00000 -1.50000 H26B 2 0.364855 0.192009 0.145210 31.00000 -1.50000 H26C 2 0.275157 0.119955 0.136305 31.00000 -1.50000 AFIX 0 PART 2 C24' 1 0.391456 0.073053 0.149458 -31.00000 0.04957 AFIX 13 H24B 2 0.434797 0.127903 0.158074 -31.00000 -1.20000 AFIX 0 C25' 1 0.413804 -0.007445 0.176212 -31.00000 0.08193 AFIX 33 H25D 2 0.480188 -0.030407 0.176856 -31.00000 -1.50000 H25E 2 0.406889 0.017973 0.198378 -31.00000 -1.50000 H25F 2 0.368476 -0.060847 0.170333 -31.00000 -1.50000 AFIX 0 C26' 1 0.289873 0.109790 0.147888 -31.00000 0.07913 AFIX 33 H26D 2 0.279821 0.128070 0.170544 -31.00000 -1.50000 H26E 2 0.279856 0.165991 0.133025 -31.00000 -1.50000 H26F 2 0.243754 0.059246 0.139072 -31.00000 -1.50000 AFIX 0 PART 1 C27 1 0.634862 0.074203 0.067841 41.00000 0.05702 0.12213 = 0.03894 -0.04269 0.01896 -0.01892 AFIX 13 H27A 2 0.674503 0.106625 0.087680 41.00000 -1.20000 AFIX 0 C28 1 0.624592 0.142815 0.038011 41.00000 0.09835 0.11079 = 0.08380 -0.04083 0.05042 -0.04149 AFIX 33 H28A 2 0.688800 0.157696 0.032818 41.00000 -1.50000 H28B 2 0.585002 0.112652 0.018379 41.00000 -1.50000 H28C 2 0.593360 0.202285 0.043627 41.00000 -1.50000 AFIX 0 C29 1 0.688171 -0.017270 0.060039 41.00000 0.09507 0.16901 = 0.10656 -0.00357 0.04835 0.03032 AFIX 33 H29A 2 0.751007 0.000123 0.054179 41.00000 -1.50000 H29B 2 0.698142 -0.059188 0.079887 41.00000 -1.50000 H29C 2 0.649408 -0.051158 0.041068 41.00000 -1.50000 AFIX 0 PART 2 C27' 1 0.633371 0.080315 0.067776 -41.00000 0.09188 AFIX 13 H27B 2 0.653235 0.137757 0.082239 -41.00000 -1.20000 AFIX 0 C28' 1 0.627902 0.115837 0.031777 -41.00000 0.08291 AFIX 33 H28D 2 0.692660 0.134596 0.028065 -41.00000 -1.50000 H28E 2 0.603035 0.064345 0.016056 -41.00000 -1.50000 H28F 2 0.584487 0.171454 0.028018 -41.00000 -1.50000 AFIX 0 C29' 1 0.718125 0.010257 0.075574 -41.00000 0.08481 AFIX 33 H29D 2 0.775578 0.038528 0.068548 -41.00000 -1.50000 H29E 2 0.731533 -0.002686 0.099840 -41.00000 -1.50000 H29F 2 0.701641 -0.050019 0.063337 -41.00000 -1.50000 AFIX 0 PART 0 N31 4 0.403569 0.395053 0.219040 11.00000 0.02135 0.02246 = 0.02036 0.00073 0.00335 0.00021 C31 1 0.419689 0.466619 0.241288 11.00000 0.01745 0.02962 = 0.02013 -0.00026 0.00253 0.00399 C32 1 0.448555 0.559260 0.233374 11.00000 0.02089 0.02671 = 0.02382 -0.00619 0.00115 0.00061 AFIX 43 H32A 2 0.471707 0.598757 0.252272 11.00000 -1.20000 AFIX 0 C33 1 0.448592 0.602594 0.202018 11.00000 0.01643 0.02394 = 0.03315 -0.00169 0.00193 0.00069 N33 4 0.434857 0.555830 0.172884 11.00000 0.02142 0.02316 = 0.02424 0.00247 0.00318 0.00155 C34 1 0.402922 0.452437 0.277155 11.00000 0.04606 0.03607 = 0.02361 -0.00300 0.00836 0.00261 AFIX 137 H34A 2 0.333480 0.456626 0.277816 11.00000 -1.50000 H34B 2 0.437360 0.502454 0.291605 11.00000 -1.50000 H34C 2 0.427079 0.389057 0.285244 11.00000 -1.50000 AFIX 0 C35 1 0.461193 0.711001 0.202834 11.00000 0.04541 0.02754 = 0.04462 -0.00268 0.00863 -0.00242 AFIX 137 H35A 2 0.488765 0.731604 0.183196 11.00000 -1.50000 H35B 2 0.504833 0.729536 0.223493 11.00000 -1.50000 H35C 2 0.398119 0.741861 0.202341 11.00000 -1.50000 AFIX 0 C36 1 0.369164 0.305016 0.230253 11.00000 0.03204 0.02325 = 0.01927 0.00034 0.00837 -0.00122 C37 1 0.269190 0.286156 0.224924 11.00000 0.03134 0.02858 = 0.03119 -0.00173 0.01148 -0.00415 C38 1 0.238061 0.199163 0.236332 11.00000 0.03437 0.03482 = 0.05207 0.00260 0.01593 -0.00704 AFIX 43 H38A 2 0.170707 0.185499 0.232946 11.00000 -1.20000 AFIX 0 C39 1 0.302193 0.132312 0.252400 11.00000 0.05188 0.02998 = 0.05315 0.01027 0.02270 -0.00595 AFIX 43 H39A 2 0.279114 0.074363 0.260699 11.00000 -1.20000 AFIX 0 C40 1 0.400008 0.150120 0.256341 11.00000 0.04739 0.03106 = 0.04527 0.01376 0.01334 0.00461 AFIX 43 H40A 2 0.444105 0.103003 0.266869 11.00000 -1.20000 AFIX 0 C41 1 0.435932 0.235467 0.245282 11.00000 0.03533 0.02731 = 0.03062 0.00441 0.00910 0.00120 C42 1 0.194504 0.356008 0.206987 11.00000 0.02499 0.03203 = 0.04636 0.00361 0.00672 -0.00351 AFIX 13 H42A 2 0.228859 0.416196 0.202255 11.00000 -1.20000 AFIX 0 C43 1 0.143961 0.314291 0.173113 11.00000 0.03462 0.05902 = 0.05092 0.00000 0.00212 -0.00012 AFIX 137 H43A 2 0.192238 0.301459 0.158687 11.00000 -1.50000 H43B 2 0.096356 0.360619 0.161969 11.00000 -1.50000 H43C 2 0.111128 0.254251 0.177127 11.00000 -1.50000 AFIX 0 C44 1 0.118267 0.382557 0.228415 11.00000 0.03739 0.04313 = 0.06001 -0.00292 0.01208 0.00399 AFIX 137 H44A 2 0.080120 0.325444 0.231815 11.00000 -1.50000 H44B 2 0.075439 0.432282 0.216867 11.00000 -1.50000 H44C 2 0.150353 0.406971 0.250306 11.00000 -1.50000 AFIX 0 C45 1 0.544675 0.250683 0.250028 11.00000 0.03380 0.03163 = 0.03652 0.00916 0.00512 0.00495 AFIX 13 H45A 2 0.556864 0.313013 0.239093 11.00000 -1.20000 AFIX 0 C46 1 0.590218 0.257108 0.287498 11.00000 0.04815 0.05322 = 0.04441 -0.00145 -0.00279 0.00806 AFIX 137 H46A 2 0.564546 0.313524 0.297606 11.00000 -1.50000 H46B 2 0.660649 0.262978 0.289575 11.00000 -1.50000 H46C 2 0.574476 0.198915 0.299186 11.00000 -1.50000 AFIX 0 C47 1 0.592979 0.170841 0.232785 11.00000 0.04244 0.04514 = 0.04489 0.01055 0.01115 0.01057 AFIX 137 H47A 2 0.581795 0.108842 0.243036 11.00000 -1.50000 H47B 2 0.662720 0.183084 0.235514 11.00000 -1.50000 H47C 2 0.565415 0.169370 0.208742 11.00000 -1.50000 AFIX 0 C48 1 0.412769 0.611071 0.142183 11.00000 0.03182 0.02487 = 0.02915 0.00586 0.00348 0.00121 C49 1 0.483143 0.621945 0.121490 11.00000 0.03886 0.03585 = 0.03725 0.01400 0.01175 0.00742 C50 1 0.458685 0.674181 0.091860 11.00000 0.05698 0.06762 = 0.04675 0.02916 0.02437 0.01468 AFIX 43 H50A 2 0.505389 0.682595 0.077543 11.00000 -1.20000 AFIX 0 C51 1 0.368509 0.713789 0.082892 11.00000 0.06488 0.07392 = 0.04818 0.03431 0.00933 0.02041 AFIX 43 H51A 2 0.353562 0.749709 0.062611 11.00000 -1.20000 AFIX 0 C52 1 0.299818 0.701874 0.103006 11.00000 0.04337 0.06337 = 0.05220 0.02607 0.00356 0.01763 AFIX 43 H52A 2 0.237190 0.728644 0.096244 11.00000 -1.20000 AFIX 0 C53 1 0.320142 0.651259 0.133164 11.00000 0.03117 0.03979 = 0.04039 0.01168 0.00339 0.00637 C54 1 0.585101 0.582635 0.131457 11.00000 0.03933 0.04511 = 0.04944 0.02022 0.02117 0.01139 AFIX 13 H54A 2 0.582574 0.531334 0.148687 11.00000 -1.20000 AFIX 0 C55 1 0.653894 0.659623 0.147793 11.00000 0.04245 0.08649 = 0.09218 -0.01981 0.00239 0.01545 AFIX 137 H55A 2 0.656776 0.712027 0.131724 11.00000 -1.50000 H55B 2 0.718603 0.631967 0.154471 11.00000 -1.50000 H55C 2 0.630813 0.684687 0.167755 11.00000 -1.50000 AFIX 0 C56 1 0.624575 0.536878 0.102282 11.00000 0.05703 0.05234 = 0.08143 0.00200 0.03030 0.00920 AFIX 137 H56A 2 0.576604 0.492031 0.090427 11.00000 -1.50000 H56B 2 0.684367 0.502002 0.110945 11.00000 -1.50000 H56C 2 0.638200 0.587107 0.086670 11.00000 -1.50000 AFIX 0 C57 1 0.241348 0.639370 0.154663 11.00000 0.02775 0.05840 = 0.05410 0.01984 0.00616 0.01147 AFIX 13 H57A 2 0.272643 0.613587 0.177053 11.00000 -1.20000 AFIX 0 C58 1 0.166578 0.566559 0.139036 11.00000 0.04083 0.07144 = 0.11055 0.00654 0.01984 -0.00257 AFIX 137 H58A 2 0.134575 0.589891 0.116981 11.00000 -1.50000 H58B 2 0.118320 0.557614 0.153758 11.00000 -1.50000 H58C 2 0.198488 0.505086 0.136263 11.00000 -1.50000 AFIX 0 C59 1 0.191824 0.734069 0.160943 11.00000 0.05303 0.07586 = 0.07699 0.00944 0.02284 0.02065 AFIX 137 H59A 2 0.240521 0.780217 0.171503 11.00000 -1.50000 H59B 2 0.144642 0.722560 0.175895 11.00000 -1.50000 H59C 2 0.158580 0.760100 0.139455 11.00000 -1.50000 AFIX 0 PART 1 C60 1 0.451572 0.321619 0.081297 51.00000 0.03903 0.05216 = 0.01968 0.00087 0.01054 -0.00306 C61 1 0.297027 0.373320 0.102073 51.00000 0.03652 0.06671 = 0.02152 -0.01589 -0.00165 0.00955 AFIX 43 H61A 2 0.229698 0.386075 0.099998 51.00000 -1.20000 AFIX 0 PART 2 C60' 1 0.470905 0.318398 0.070923 -51.00000 0.04500 AFIX 43 H60B 2 0.499484 0.313824 0.051209 -51.00000 -1.20000 AFIX 0 C61' 1 0.339121 0.364161 0.102096 -51.00000 0.05110 PART 0 O60 5 0.532075 0.301458 0.096536 11.00000 0.03888 0.05152 = 0.02842 0.00261 -0.00309 0.00472 O61 5 0.340658 0.374968 0.132389 11.00000 0.04147 0.06224 = 0.02907 -0.01059 -0.00234 -0.00093 C62 1 0.318935 0.327443 0.002881 11.00000 0.04401 0.07833 = 0.02463 0.00107 -0.00434 -0.00259 C63 1 0.303633 0.426835 0.007899 11.00000 0.06292 0.07269 = 0.03544 0.01127 -0.01384 -0.00088 C64 1 0.222629 0.436127 0.023723 11.00000 0.05915 0.08910 = 0.04175 -0.00972 -0.02223 0.01855 C65 1 0.186520 0.341838 0.028177 11.00000 0.03544 0.12400 = 0.03141 -0.00857 -0.00806 -0.00342 C66 1 0.245115 0.275051 0.014574 11.00000 0.05139 0.07596 = 0.02781 -0.00415 -0.00905 -0.01411 C67 1 0.395282 0.285135 -0.015203 11.00000 0.07175 0.12850 = 0.03540 -0.00417 0.01143 0.00509 AFIX 137 H67A 2 0.452184 0.327203 -0.012094 11.00000 -1.50000 H67B 2 0.369272 0.279405 -0.039291 11.00000 -1.50000 H67C 2 0.413877 0.221372 -0.005946 11.00000 -1.50000 AFIX 0 C68 1 0.360580 0.508949 -0.003327 11.00000 0.13079 0.09686 = 0.07716 0.03993 -0.01353 -0.02621 AFIX 137 H68A 2 0.427669 0.488610 -0.003001 11.00000 -1.50000 H68B 2 0.359425 0.563586 0.011968 11.00000 -1.50000 H68C 2 0.331704 0.528085 -0.026253 11.00000 -1.50000 AFIX 0 C69 1 0.175934 0.528948 0.031953 11.00000 0.11999 0.12832 = 0.08912 -0.02735 -0.04669 0.06952 AFIX 137 H69A 2 0.124966 0.546754 0.013180 11.00000 -1.50000 H69B 2 0.224855 0.579926 0.035612 11.00000 -1.50000 H69C 2 0.147666 0.520429 0.052413 11.00000 -1.50000 AFIX 0 C70 1 0.095648 0.318095 0.042026 11.00000 0.04148 0.23499 = 0.06792 -0.02172 0.00581 -0.01705 AFIX 137 H70A 2 0.098870 0.251438 0.050030 11.00000 -1.50000 H70B 2 0.039137 0.326026 0.024242 11.00000 -1.50000 H70C 2 0.090002 0.361421 0.060787 11.00000 -1.50000 AFIX 0 C71 1 0.230126 0.168596 0.011284 11.00000 0.10152 0.08647 = 0.05990 -0.01111 -0.00774 -0.03465 AFIX 137 H71A 2 0.198193 0.145438 0.029608 11.00000 -1.50000 H71B 2 0.292904 0.136576 0.012514 11.00000 -1.50000 H71C 2 0.189476 0.154136 -0.010420 11.00000 -1.50000 AFIX 0 C81 1 0.357181 0.322952 0.478513 11.00000 0.07052 0.08019 = 0.09627 -0.01669 0.00987 0.00441 AFIX 137 H81A 2 0.330095 0.349905 0.456441 11.00000 -1.50000 H81B 2 0.305385 0.292871 0.488443 11.00000 -1.50000 H81C 2 0.406152 0.274596 0.475824 11.00000 -1.50000 AFIX 0 C82 1 0.402646 0.401209 0.501057 11.00000 0.07591 0.09279 = 0.08324 -0.00462 0.02089 0.00485 AFIX 23 H82A 2 0.350359 0.443277 0.506432 11.00000 -1.20000 H82B 2 0.434401 0.371563 0.522445 11.00000 -1.20000 AFIX 0 C83 1 0.474178 0.462157 0.488435 11.00000 0.05590 0.08046 = 0.06550 -0.00564 0.01077 0.01562 AFIX 23 H83A 2 0.441058 0.494889 0.467842 11.00000 -1.20000 H83B 2 0.523883 0.419448 0.481565 11.00000 -1.20000 AFIX 0 PART 1 C91 1 1.045762 0.994103 0.120192 61.00000 0.16328 0.12424 = 0.12225 -0.02032 0.00362 0.03491 AFIX 137 H91A 2 1.013990 1.033793 0.101421 61.00000 -1.50000 H91B 2 1.103993 0.964628 0.114163 61.00000 -1.50000 H91C 2 1.063827 1.034406 0.140233 61.00000 -1.50000 AFIX 0 C92 1 0.977657 0.916834 0.127471 61.00000 0.11363 0.12673 = 0.06520 -0.00491 0.00132 0.04642 AFIX 23 H92A 2 0.918077 0.947241 0.132695 61.00000 -1.20000 H92B 2 1.008175 0.880756 0.147696 61.00000 -1.20000 AFIX 0 C93 1 0.950008 0.846386 0.098447 61.00000 0.07324 0.11640 = 0.05685 0.02393 0.01480 0.02565 AFIX 23 H93A 2 0.912998 0.880911 0.078916 61.00000 -1.20000 H93B 2 1.009630 0.820716 0.091597 61.00000 -1.20000 AFIX 0 C94 1 0.890395 0.764437 0.107763 61.00000 0.07143 0.17890 = 0.06584 0.02886 0.01199 -0.02972 AFIX 23 H94A 2 0.834398 0.791365 0.116663 61.00000 -1.20000 H94B 2 0.929959 0.727990 0.126272 61.00000 -1.20000 AFIX 0 C95 1 0.852892 0.695201 0.080013 61.00000 0.05546 0.17394 = 0.08765 0.05084 -0.01486 -0.03060 AFIX 23 H95A 2 0.815020 0.645417 0.089612 61.00000 -1.20000 H95B 2 0.807071 0.730721 0.062932 61.00000 -1.20000 AFIX 0 C96 1 0.921254 0.646005 0.062505 61.00000 0.10583 0.10979 = 0.05884 0.02275 -0.02647 -0.01824 AFIX 137 H96A 2 0.970217 0.613477 0.078951 61.00000 -1.50000 H96B 2 0.952858 0.692914 0.049800 61.00000 -1.50000 H96C 2 0.886783 0.598451 0.046958 61.00000 -1.50000 AFIX 0 PART 2 C91' 1 1.046711 0.974564 0.116964 -61.00000 0.14820 AFIX 33 H91F 2 1.055592 1.044453 0.118084 -61.00000 -1.50000 H91G 2 1.086897 0.944613 0.136513 -61.00000 -1.50000 H91H 2 1.065835 0.950050 0.096238 -61.00000 -1.50000 AFIX 0 C92' 1 0.944990 0.951555 0.117046 -61.00000 0.14395 AFIX 23 H91D 2 0.906807 0.985934 0.097712 -61.00000 -1.20000 H91E 2 0.927712 0.980538 0.137686 -61.00000 -1.20000 AFIX 0 C93' 1 0.909427 0.850980 0.115537 -61.00000 0.11128 AFIX 23 H93C 2 0.929894 0.822781 0.138197 -61.00000 -1.20000 H93D 2 0.837834 0.853868 0.111684 -61.00000 -1.20000 AFIX 0 C94' 1 0.936914 0.781649 0.090843 -61.00000 0.10089 AFIX 23 H94C 2 0.927614 0.816302 0.069058 -61.00000 -1.20000 H94D 2 1.007605 0.772319 0.097429 -61.00000 -1.20000 AFIX 0 C95' 1 0.898059 0.688311 0.083316 -61.00000 0.13216 AFIX 23 H95C 2 0.828170 0.697558 0.074804 -61.00000 -1.20000 H95D 2 0.902632 0.654737 0.105207 -61.00000 -1.20000 AFIX 0 C96' 1 0.932807 0.618600 0.059971 -61.00000 0.12419 AFIX 33 H96D 2 0.894365 0.559508 0.059054 -61.00000 -1.50000 H96E 2 0.925860 0.646826 0.037391 -61.00000 -1.50000 H96F 2 1.001070 0.603574 0.068100 -61.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM MRC2137 in P2(1)/n REM wR2 = 0.1068, GooF = S = 1.020, Restrained GooF = 1.033 for all data REM R1 = 0.0443 for 11939 Fo > 4sig(Fo) and 0.0652 for all 15686 data REM 892 parameters refined using 239 restraints END WGHT 0.0414 2.9340 REM Highest difference peak 0.388, deepest hole -0.577, 1-sigma level 0.049 Q1 1 0.3469 0.2802 0.0607 11.00000 0.05 0.39 Q2 1 0.4163 0.4032 0.4741 11.00000 0.05 0.30 Q3 1 0.5830 0.1691 0.1379 11.00000 0.05 0.26 Q4 1 0.9162 0.1193 0.2000 11.00000 0.05 0.25 Q5 1 0.4964 0.2397 0.2450 11.00000 0.05 0.25 Q6 1 0.9417 0.5736 0.0518 11.00000 0.05 0.25 Q7 1 0.3785 0.5134 0.2840 11.00000 0.05 0.25 Q8 1 0.4644 0.4556 0.5120 11.00000 0.05 0.25 Q9 1 0.9364 0.7232 0.0911 11.00000 0.05 0.25 Q10 1 0.3428 0.4445 0.0602 11.00000 0.05 0.23 ; _shelx_res_checksum 21990 _shelx_hkl_file ; 0 0 5 105.500 60.5442 1 0 0 -5 342.756 86.1631 1 0 0 -6 10932.7 353.532 1 0 0 6 9633.14 333.693 1 0 0 -7 509.892 142.527 1 0 0 7 621.669 212.320 1 0 0 -8 128338. 1383.22 1 0 0 8 124146. 1363.74 1 0 0 -9 1168.61 270.334 1 0 0 9 2984.11 444.758 1 0 0 -10 309724. 2405.57 1 0 0 10 310435. 2392.28 1 0 0 -11 2554.68 398.473 1 0 0 11 4824.25 440.989 1 0 0 12 155092. 1890.76 3 0 0 12 152438. 1823.88 1 0 0 -12 151774. 1850.40 1 0 0 13 2862.31 370.961 3 0 0 13 2583.61 307.072 1 0 0 -13 1925.69 315.078 1 0 0 14 79772.3 1493.61 3 0 0 14 80208.6 1434.32 1 0 0 -14 78690.0 1441.86 1 0 0 -15 1277.71 244.719 1 0 0 15 1900.03 435.112 3 0 0 15 1712.19 293.238 1 0 0 16 32861.0 1028.89 3 0 0 16 31316.3 968.276 1 0 0 -16 33846.3 1014.26 1 0 0 -17 1293.35 249.897 1 0 0 17 1879.84 310.963 3 0 0 18 96741.6 1854.67 3 0 0 -18 100670. 1852.09 1 0 0 -19 1883.14 319.826 1 0 0 19 3050.12 489.901 3 0 0 -20 10758.5 655.802 1 0 0 20 10814.2 682.862 3 0 0 -21 578.156 220.278 1 0 0 21 823.961 264.185 3 0 0 -22 681.383 217.564 1 0 0 22 311.505 191.953 3 0 0 -23 972.642 266.577 1 0 0 23 954.997 293.336 3 0 0 -23 467.818 204.749 2 0 0 -24 52409.2 1581.17 1 0 0 24 51977.5 1609.74 3 0 0 -24 52268.5 1342.80 2 0 0 25 9542.26 866.137 3 0 0 -25 5760.11 516.839 2 0 0 26 175845. 3077.74 3 0 0 -26 182058. 2609.25 2 0 0 27 8315.44 735.056 3 0 0 -27 6865.26 557.505 2 0 0 28 1689.65 361.718 3 0 0 -28 1125.85 258.939 2 0 0 29 1085.81 344.712 3 0 0 -29 791.933 253.828 2 0 0 30 27408.7 1337.83 3 0 0 -30 28650.2 1119.50 2 0 0 31 1433.73 396.069 3 0 0 -31 1479.99 312.815 2 0 0 32 11585.4 908.740 3 0 0 -32 12590.7 771.948 2 0 0 33 948.719 331.649 3 0 0 -33 904.472 247.851 2 0 0 34 8733.74 829.324 3 0 0 -34 9222.05 691.299 2 0 0 -35 854.277 260.326 2 0 0 36 20706.5 1291.14 3 0 0 -36 20834.0 1071.49 2 0 0 37 1174.30 386.435 3 0 0 -37 605.432 221.380 2 0 0 38 1172.63 383.404 3 0 0 -38 1046.49 256.578 2 0 0 39 51.2160 250.321 3 0 0 -39-124.580 165.905 2 0 0 40 1900.89 481.051 3 0 0 -40 2794.00 433.157 2 0 0 41 1192.68 436.586 3 0 0 -41 489.909 234.810 2 0 0 42 24821.2 1576.92 3 0 0 -42 26114.7 1302.58 2 0 0 43 1110.60 424.650 3 0 0 -43 1166.60 320.630 2 0 0 -44 8510.60 782.217 2 0 0 44 8110.67 939.695 3 0 0 45 782.256 387.355 3 0 0 46 520.140 330.841 3 0 0 47-624.687 325.080 3 0 -1 4 4708.03 190.572 1 0 1 -4 6829.45 229.924 1 0 -1 -4 4265.18 191.140 3 0 1 4 7354.33 247.026 3 0 1 -5 103540. 958.098 1 0 -1 5 106723. 968.460 1 0 1 5 107401. 1016.33 3 0 -1 -5 100960. 996.248 3 0 -1 6 267140. 1652.67 1 0 1 -6 259767. 1670.70 1 0 -1 -6 261710. 1716.09 3 0 1 6 268020. 1742.94 3 0 -1 7 54695.9 809.029 1 0 1 -7 53836.7 821.454 1 0 1 7 52964.3 854.957 3 0 -1 -7 53316.1 847.000 3 0 -1 8 25474.1 598.113 1 0 1 -8 23456.2 586.078 1 0 1 8 23758.1 619.937 3 0 -1 -8 24750.5 613.553 3 0 1 -9 2028.48 208.982 1 0 -1 9 2080.87 216.741 1 0 1 9 2042.04 217.667 3 0 -1 -9 2035.93 219.005 3 0 -1 -9 1569.88 200.279 1 0 -1 10 283.120 138.594 1 0 1 -10 337.654 127.596 1 0 1 10 366.134 139.460 3 0 -1 -10 461.563 141.672 3 0 -1 -10 513.031 157.654 1 0 1 -11 34091.2 832.023 1 0 1 11 33987.2 858.007 3 0 -1 -11 32460.2 882.827 1 0 -1 11 33773.9 823.036 1 0 1 -12 146183. 1770.38 1 0 1 12 145773. 1828.90 3 0 -1 -12 148294. 1904.93 1 0 -1 12 147934. 1765.83 1 0 1 -13 10861.5 527.436 1 0 1 13 12527.0 647.406 3 0 -1 13 11716.9 543.113 1 0 -1 -13 10828.6 570.666 1 0 1 -14-13.1852 118.954 1 0 1 14 519.038 269.023 3 0 -1 14 263.861 167.555 1 0 -1 -14 74.3690 128.532 1 0 1 -15 4677.99 423.678 1 0 -1 -15 3681.03 351.393 1 0 -1 15 3324.58 322.155 1 0 1 -16 90515.7 1635.68 1 0 1 16 93392.0 1701.57 3 0 -1 -16 89234.8 1711.14 1 0 -1 16 88372.6 1587.40 1 0 1 -17 33449.5 1040.16 1 0 -1 17 28159.5 946.618 1 0 -1 -17 30635.2 1026.52 1 0 1 -18 62166.2 1436.16 1 0 1 18 63800.7 1494.61 3 0 -1 18 58854.4 1382.97 1 0 -1 -18 59806.8 1477.44 1 0 1 -19 3596.71 415.656 1 0 -1 19 2428.23 327.433 1 0 -1 -19 2857.89 382.701 1 0 1 -20 15908.1 777.061 1 0 1 20 16877.8 823.145 3 0 -1 -20 15969.0 819.204 1 0 -1 20 15143.2 764.296 1 0 1 -21 2949.75 397.715 1 0 -1 -21 1709.32 295.361 1 0 1 -21 2163.50 262.232 2 0 -1 21 1557.56 312.263 1 0 1 -22 45583.6 1373.65 1 0 1 22 43586.8 1371.67 3 0 -1 22 41193.9 1365.56 3 0 -1 -22 47000.3 1452.19 1 0 -1 22 41867.9 1311.49 1 0 1 -22 42731.1 1070.92 2 0 -1 -23 1514.96 335.434 1 0 1 -23 2324.61 392.535 1 0 -1 23 1682.66 387.905 3 0 -1 23 1391.67 317.204 1 0 1 -23 2957.30 332.128 2 0 1 -24 33418.0 1241.73 1 0 -1 24 30121.3 1241.58 3 0 1 24 32450.0 1251.03 3 0 -1 24 28915.3 1140.35 1 0 1 -24 31393.6 970.116 2 0 -1 -24 29443.2 1079.35 2 0 1 -25 32738.5 1262.06 1 0 -1 25 30775.7 1291.85 3 0 1 25 32889.2 1293.64 3 0 -1 -25 31726.4 1144.03 2 0 1 -25 31644.2 994.862 2 0 1 26 26964.1 1221.12 3 0 -1 26 22202.5 1119.54 3 0 -1 -26 23836.4 1011.80 2 0 1 -26 24862.7 904.969 2 0 1 27 43003.8 1556.65 3 0 -1 27 38876.1 1502.54 3 0 -1 -27 39870.8 1324.60 2 0 1 -27 39191.4 1153.97 2 0 -1 28 39655.7 1548.53 3 0 1 28 43947.0 1587.60 3 0 1 -28 40666.2 1199.78 2 0 -1 -28 41430.0 1371.93 2 0 -1 29 13627.3 947.687 3 0 1 29 15879.7 1005.78 3 0 -1 -29 14203.2 822.617 2 0 1 -29 15048.6 752.029 2 0 1 30 9268.90 802.992 3 0 -1 30 7669.78 731.074 3 0 -1 -30 7112.18 602.097 2 0 1 -30 7813.74 560.645 2 0 1 31 13391.5 939.289 3 0 -1 31 14042.3 992.240 3 0 1 -31 13707.7 749.793 2 0 -1 -31 13652.8 841.620 2 0 -1 32 2048.56 468.128 3 0 1 32 2823.93 486.846 3 0 1 -32 2610.12 366.253 2 0 -1 -32 2463.74 386.692 2 0 1 33 3815.89 545.037 3 0 -1 33 3849.09 575.749 3 0 -1 -33 4364.29 494.694 2 0 1 -33 4898.05 481.415 2 0 1 34 226.055 291.422 3 0 -1 34 165.703 185.431 3 0 -1 -34 68.2769 169.848 2 0 1 -34 382.824 204.418 2 0 1 35 3784.23 584.206 3 0 -1 35 4611.55 658.263 3 0 1 -35 4883.60 504.599 2 0 -1 -35 4047.72 512.847 2 0 1 36 7190.11 788.938 3 0 -1 36 8368.43 838.780 3 0 -1 -36 7720.87 702.482 2 0 1 -36 7981.43 631.621 2 0 -1 37 5894.16 756.121 3 0 1 37 5180.22 703.904 3 0 -1 -37 4713.62 575.614 2 0 1 -37 5540.25 556.228 2 0 -1 38 18504.8 1287.76 3 0 1 38 18962.0 1288.44 3 0 -1 -38 19455.9 1120.25 2 0 1 -38 19749.0 1012.94 2 0 1 39 1765.09 449.499 3 0 -1 39 1256.11 426.723 3 0 -1 -39 1111.26 342.994 2 0 1 -39 1417.69 314.543 2 0 1 40 4591.43 679.961 3 0 -1 -40 4024.27 544.426 2 0 1 -40 4385.02 509.827 2 0 1 41 2159.77 513.320 3 0 -1 41 2118.77 489.888 3 0 1 -41 2660.13 416.248 2 0 -1 -41 1935.44 382.629 2 0 1 42 662.540 378.993 3 0 -1 42 817.767 387.761 3 0 -1 -42 519.153 241.112 2 0 1 -42 582.631 265.750 2 0 -1 43 3849.88 647.918 3 0 -1 -43 4233.37 574.678 2 0 -1 44 1208.30 411.988 3 0 1 44 782.763 331.755 3 0 -1 -44 815.525 271.720 2 0 1 45 564.348 371.788 3 0 -1 45 771.134 416.837 3 0 -1 -45 399.676 227.194 2 0 -1 46 4000.32 700.349 3 0 1 46 4931.00 769.195 3 0 -1 -46 4548.33 624.690 2 0 -1 47 813.705 359.134 3 0 1 49 4200.42 754.660 3 0 2 -4 24678.5 496.991 1 0 -2 4 26904.3 509.836 1 0 -2 5 369845. 1974.22 1 0 2 -5 366870. 1986.25 1 0 -2 -6 125368. 1268.64 3 0 2 -6 126623. 1231.38 1 0 -2 6 128951. 1224.05 1 0 -2 -7 47103.5 825.522 3 0 2 -7 46288.6 789.509 1 0 -2 7 47971.8 789.575 1 0 -2 -8 777.539 149.462 3 0 2 8 945.403 164.408 3 0 2 -8 713.708 140.716 1 0 -2 8 521.392 145.762 1 0 -2 9 51972.5 925.174 1 0 2 -9 52407.9 929.738 1 0 2 9 54887.3 997.024 3 0 -2 -9 51311.6 952.081 3 0 2 -10 2863.15 244.035 1 0 -2 10 2943.70 252.102 1 0 -2 -10 2761.34 253.237 3 0 2 10 2697.31 264.582 3 0 -2 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2646.74 1 0 -2 19 165980. 2360.81 1 0 2 -19 169727. 1730.51 2 0 2 -20 39691.4 1244.48 1 0 2 20 47529.4 1411.66 3 0 -2 -20 40075.2 1313.49 1 0 2 -20 44656.1 935.569 2 0 -2 20 36626.3 1148.05 1 0 2 -21 17179.5 834.375 1 0 2 21 20116.4 946.379 3 0 2 -21 17701.8 612.634 2 0 -2 21 15382.8 779.061 1 0 -2 -21 16477.4 872.378 1 0 2 -22 2200.95 339.095 1 0 -2 22 1783.48 312.329 1 0 2 -22 2832.40 280.997 2 0 -2 -22 2132.69 345.913 1 0 2 -23 45599.2 1426.75 1 0 2 23 43433.2 1411.74 3 0 -2 23 41958.9 1329.76 1 0 2 -23 41320.4 976.226 2 0 2 -24 5117.04 520.224 1 0 2 -24 6543.25 425.033 2 0 -2 -24 6041.34 540.976 2 0 -2 24 4557.54 473.026 1 0 2 -25 9972.56 711.482 1 0 2 25 11318.6 778.447 3 0 -2 25 9648.66 680.698 1 0 -2 -25 9287.27 667.007 2 0 2 -25 10396.7 527.224 2 0 2 26 24043.2 1144.81 3 0 -2 26 19878.8 987.782 1 0 2 -26 20526.2 755.597 2 0 -2 -26 19849.0 968.714 2 0 2 27 44469.5 1575.40 3 0 -2 27 44271.9 1483.85 1 0 -2 -27 43698.9 1456.42 2 0 2 -27 45957.3 1151.23 2 0 -2 28 1098.84 392.036 3 0 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1356.30 1 -2 -2 17 69213.8 1624.34 3 -2 2 17 65056.5 1562.26 3 2 -2 -17 67279.3 1569.45 3 2 -2 -17 68553.5 1620.67 1 -2 -2 17 67617.1 1551.31 1 2 2 -17 68739.4 1587.26 1 -2 2 16 11900.4 665.494 3 2 -2 -16 12333.8 666.279 3 2 -2 -16 12844.6 695.652 1 -2 -2 16 12674.3 673.223 1 2 2 -16 13151.0 683.485 1 -2 2 15 91616.5 1740.18 3 2 -2 -15 91291.3 1734.01 3 -2 -2 15 92885.1 1715.69 3 2 -2 -15 93130.8 1770.12 1 2 2 -15 91503.4 1723.64 1 -2 -2 15 91669.6 1730.49 1 2 -2 -14 7577.05 518.895 3 2 -2 -14 8508.56 607.549 1 -2 -2 14 6995.78 503.972 1 2 2 -14 7364.71 499.760 1 2 -2 -13 179334. 2291.09 3 -2 -2 13 171872. 2208.28 3 2 -2 -13 174079. 2298.73 1 2 2 -13 178490. 2265.55 1 -2 -2 13 177925. 2283.96 1 -2 -2 12 16891.8 870.590 3 2 -2 -12 516.104 199.998 3 -2 2 12 23248.2 997.080 1 2 2 -12 242.983 143.207 1 2 -2 -12 1555.01 320.367 1 -2 -2 12 699.391 226.596 1 2 -2 -11 177006. 2156.75 3 -2 -2 11 175769. 2052.52 3 2 -2 -11 171237. 2136.98 1 -2 2 11 178666. 2120.25 1 2 2 -11 177231. 2147.42 1 -2 -2 11 180179. 2146.65 1 2 -2 -10 5643.55 394.131 3 2 -2 -10 6328.31 432.321 1 2 2 -10 5177.14 381.144 1 -2 -2 10 5876.23 414.356 1 2 2 -9 13747.0 438.905 2 -2 -2 9 29178.9 858.568 3 2 -2 -9 13717.5 574.337 3 -2 2 9 30767.5 902.723 1 2 -2 -9 15375.1 630.688 1 2 2 -9 13621.6 579.399 1 -2 -2 9 12359.3 558.670 1 -2 -2 8 202500. 1910.11 3 2 -2 -8 207445. 2038.55 1 -2 2 8 210712. 2026.28 1 2 2 -8 204599. 1632.12 2 -2 -2 8 207853. 2135.55 1 2 2 -8 206720. 2107.51 1 -2 -2 7 27711.0 740.057 3 2 -2 -7 17291.8 614.400 1 -2 2 7 24026.2 731.216 1 2 2 -7 16229.9 467.443 2 2 2 -7 15809.0 585.802 1 -2 -2 7 16061.3 593.201 1 -2 -2 6 70210.2 1032.29 3 -2 2 6 64544.6 1043.13 1 2 -2 -6 72142.2 1108.16 1 2 2 -6 62132.7 893.852 2 -2 -2 6 63446.2 904.786 2 -2 -2 6 60919.5 1105.25 1 2 2 -6 62037.4 1099.77 1 -2 -2 5 435105. 2285.00 3 2 -2 -5 439987. 2500.29 1 2 2 -5 432523. 2379.38 2 -2 -2 5 441877. 2370.49 2 2 2 -5 431120. 2829.58 1 -2 -2 5 434374. 2847.92 1 -2 -2 4 64973.6 812.768 3 2 -2 -4 73812.8 977.403 1 -2 -2 4 68454.3 946.849 2 2 2 -4 64987.2 937.376 2 -2 -2 4 64188.0 1089.34 1 2 2 -3 14371.6 447.743 2 -2 -2 3 14774.1 466.010 2 -2 -2 3 14407.7 350.969 3 2 -2 -3 17278.8 446.695 1 -2 -2 2 25880.3 405.234 3 2 -2 -2 27366.8 496.727 1 2 2 -2 24737.0 609.933 2 -2 -2 2 27299.1 625.244 2 2 -2 -1 43343.2 546.586 1 -2 -2 1 41482.6 789.532 2 2 2 -1 42892.9 803.683 2 2 2 0 91615.5 1200.39 2 -2 -2 0 93373.4 1207.52 2 2 2 1 412414. 2591.54 2 -2 -2 -1 413031. 2579.99 2 2 2 2 5367.59 326.413 2 -2 -2 -2 5888.28 345.783 2 -2 -2 -3 18610.3 591.716 2 2 2 3 19306.8 599.425 2 2 -2 4 226798. 1543.43 2 2 2 4 221818. 2090.41 2 -2 -2 -4 227034. 2078.48 2 2 2 5 1149.33 103.971 3 2 2 5 1217.67 197.349 2 -2 -2 -5 1026.00 200.277 2 2 -2 5 1095.52 130.711 2 2 2 6 20441.3 425.571 3 2 -2 6 19746.0 455.681 2 2 2 6 18989.9 645.164 2 -2 -2 -6 18118.2 644.978 2 -2 2 -7 10701.4 293.201 1 2 2 7 14031.9 447.612 3 2 2 7 9840.94 495.481 2 -2 2 -7 10604.4 341.136 2 2 -2 7 10271.2 334.798 2 -2 -2 -7 10806.0 517.922 2 -2 2 -8 329765. 1779.48 1 2 2 8 341285. 2075.23 3 2 2 8 332588. 2808.29 2 -2 2 -8 333949. 1910.37 2 2 -2 8 337572. 1906.95 2 -2 -2 -8 324924. 2790.84 2 -2 2 -9 72272.5 910.110 1 2 2 9 71814.9 1344.08 2 -2 2 -9 74596.8 919.262 2 2 -2 9 73239.5 905.099 2 -2 -2 -9 72619.8 1361.37 2 -2 2 -10 27126.0 608.902 1 2 2 10 26752.4 859.044 2 -2 2 -10 28205.6 583.368 2 2 -2 10 27746.5 573.523 2 -2 -2 -10 28415.1 890.527 2 -2 2 -11 35466.6 741.924 1 2 2 11 39634.4 870.507 3 2 2 11 35182.0 994.575 2 -2 2 -11 35914.4 678.372 2 -2 -2 -11 35017.2 993.833 2 2 -2 11 35234.4 670.321 2 -2 2 -12 18638.7 579.283 1 2 2 12 17957.6 738.105 2 -2 2 -12 17911.8 493.333 2 -2 -2 -12 16307.4 711.543 2 2 -2 12 17840.2 487.600 2 -2 2 -13 39075.5 869.715 1 2 2 13 41213.9 977.656 3 2 -2 13 38644.8 736.694 2 -2 2 -13 37279.0 735.188 2 -2 -2 -13 37140.4 1064.88 2 2 -2 14 11289.3 415.492 2 -2 2 -14 12956.6 543.800 1 -2 -2 -14 11733.5 630.436 2 -2 2 -14 10851.3 420.147 2 2 2 15 30405.1 912.647 3 2 -2 15 30515.9 702.080 2 -2 2 -15 30186.3 714.981 2 -2 -2 -15 29743.4 1007.51 2 -2 2 -15 30027.5 839.970 1 -2 -2 -16 7128.58 732.204 2 -2 2 -16 5267.65 480.224 1 2 2 17 230317. 2682.47 3 -2 2 -17 222701. 2047.66 2 -2 -2 -17 231717. 2837.54 2 -2 2 -17 226027. 2479.15 1 -2 2 -18 102690. 1437.93 2 -2 -2 -18 111312. 2038.85 2 -2 2 -18 106452. 1770.54 1 2 2 19 29709.5 1058.24 3 -2 2 -19 19669.0 651.662 2 -2 -2 -19 29561.8 1088.98 2 -2 2 -19 22828.7 864.210 1 2 2 20 49488.1 1371.77 3 -2 2 -20 47613.9 1267.28 1 -2 -2 -20 50273.4 1410.94 2 -2 2 -20 46383.2 1022.81 2 2 2 21 32330.0 1139.75 3 -2 -2 -21 28850.7 1150.00 1 -2 2 -21 30572.6 1048.47 1 -2 2 -21 29373.8 835.162 2 -2 -2 -21 32910.7 1168.58 2 2 2 22 11030.5 703.815 3 -2 -2 -22 9437.63 675.550 1 -2 2 -22 9659.50 618.942 1 -2 2 -22 10448.1 515.030 2 -2 -2 -22 11480.3 710.536 2 2 2 23 1008.89 275.259 3 -2 -2 -23 821.134 259.888 2 -2 2 -23 174.372 101.806 2 -2 2 -23 693.082 216.640 1 -2 2 -24 2480.79 329.142 2 -2 2 -24 1883.95 330.004 1 2 2 25 62117.2 1742.59 3 -2 -2 -25 64512.5 1742.84 2 -2 2 -25 65554.4 1371.93 2 -2 2 -25 66237.0 1718.48 1 2 2 26 15614.1 931.595 3 -2 2 -26 12976.4 666.767 2 -2 2 -26 13650.5 828.776 1 2 2 27 43410.7 1526.09 3 -2 2 -27 46294.7 1212.18 2 -2 -2 -27 46233.4 1533.60 2 -2 2 -27 47867.1 1539.74 1 2 2 28 9665.75 773.409 3 -2 -2 -28 10088.2 755.721 2 -2 2 -28 8875.33 557.359 2 2 2 29 2704.42 446.760 3 -2 -2 -29 3512.47 494.849 2 -2 2 -29 2804.21 344.041 2 2 2 30 10844.4 822.868 3 -2 -2 -30 12747.3 858.997 2 -2 2 -30 12249.3 664.724 2 2 2 31 2539.44 455.555 3 -2 -2 -31 2925.61 463.081 2 -2 2 -31 2359.05 330.941 2 2 2 32 5218.37 631.865 3 -2 2 -32 5305.78 475.691 2 -2 -2 -32 5102.12 581.495 2 2 2 33 10697.4 870.450 3 -2 2 -33 12228.5 711.192 2 -2 -2 -33 11145.5 839.433 2 2 2 34 809.012 320.197 3 -2 2 -34 498.587 217.253 2 -2 -2 -34 675.797 281.576 2 2 -2 35 1869.88 388.237 3 -2 2 -35 1905.82 306.926 2 -2 -2 -35 2235.10 416.046 2 2 -2 36 342.368 310.919 3 2 2 36 915.120 359.783 3 -2 2 -36 237.867 211.157 2 -2 -2 -36 514.194 284.543 2 2 2 37 14046.1 1078.87 3 2 -2 37 16298.9 1212.79 3 -2 2 -37 16061.8 875.755 2 -2 -2 -37 15668.0 1054.03 2 2 2 38 516.229 290.865 3 2 -2 38 936.025 409.997 3 -2 -2 -38 1367.55 387.784 2 -2 2 -38 765.683 241.558 2 2 -2 39 1605.77 457.356 3 2 2 39 1621.36 443.005 3 -2 -2 -39 1359.53 395.703 2 2 2 40 10033.5 991.763 3 2 -2 40 9098.18 957.662 3 -2 -2 -40 9630.36 882.183 2 2 2 41 8533.75 924.200 3 2 -2 41 9022.60 975.701 3 -2 -2 -41 9541.37 882.798 2 2 -2 42 4102.92 715.711 3 -2 -2 -42 5277.55 698.993 2 2 -2 43 22690.4 1559.91 3 2 2 43 21141.4 1466.28 3 -2 -2 -43 22349.4 1362.12 2 2 2 44 1066.10 407.916 3 2 -2 44 1264.66 487.900 3 -2 -2 -44 941.644 340.483 2 2 2 45 159.696 307.770 3 -2 -2 -45 182.267 239.555 2 2 -2 46 1305.70 418.978 3 2 2 46 1383.57 438.357 3 -2 -2 -46 1249.11 374.176 2 2 2 47 308.584 312.625 3 2 -2 47 65.0828 267.252 3 -2 -2 -47-9.70580 194.971 2 2 2 48 193.577 254.947 3 2 2 49 1246.62 408.645 3 2 -3 -51 2478.82 539.741 2 2 -3 -50-243.767 243.585 2 -2 3 49 97.4182 296.326 3 2 -3 -49 182.036 273.662 2 -2 3 48 220.651 302.237 3 2 -3 -48 413.583 284.799 2 -2 -3 47 3636.54 679.196 3 -2 3 47 3684.13 710.784 3 2 -3 -47 3469.96 608.791 2 -2 3 46 1228.28 436.950 3 -2 -3 46 1901.09 498.050 3 2 -3 -46 957.333 334.868 2 -2 3 45 3036.14 617.030 3 -2 -3 45 3271.17 620.806 3 2 -3 -45 3222.45 568.283 2 -2 -3 44 3902.36 678.360 3 -2 3 44 4611.40 760.350 3 2 -3 -44 4021.47 625.507 2 -2 -3 43 8865.79 993.368 3 -2 3 43 7565.99 904.962 3 2 -3 -43 8420.57 875.244 2 -2 3 42 1381.24 437.449 3 -2 -3 42 1156.09 448.073 3 2 -3 -42 687.578 309.898 2 -2 3 41 39.3316 229.841 3 2 -3 -41-66.8418 211.681 2 -2 -3 41 131.614 233.444 1 -2 3 40 1654.22 461.763 3 2 -3 -40 1745.28 458.127 2 -2 -3 40 1399.24 414.683 1 -2 -3 39 16887.4 1252.86 3 -2 3 39 17873.5 1273.63 3 -2 -3 39 17661.4 1239.57 1 2 3 -39 16822.2 851.731 2 -2 -3 38 2505.52 559.322 3 -2 3 38 3121.64 670.915 3 -2 -3 38 1109.48 425.418 1 2 3 -38 1650.05 313.320 2 -2 -3 37 37089.8 1791.53 3 -2 3 37 42115.5 1886.16 3 -2 -3 37 39935.6 1763.80 1 2 3 -37 42446.7 1308.64 2 -2 3 36 5744.47 815.577 3 2 3 -36 4355.41 436.510 2 -2 -3 36 3831.09 583.668 1 -2 -3 35 1477.09 402.160 3 -2 3 35 870.660 374.953 3 -2 -3 35 1015.04 326.994 1 -2 3 34 273.700 241.708 3 -2 -3 34 71.7088 232.111 3 -2 -3 34-52.5124 193.892 1 -2 3 33 2091.44 455.114 3 -2 -3 33 1922.74 420.313 3 -2 -3 33 2543.28 467.230 1 -2 3 32 4611.64 609.148 3 -2 -3 32 4912.77 596.557 1 -2 3 31 1727.00 393.952 3 -2 -3 31 2237.61 460.715 3 -2 -3 31 1276.31 347.753 1 -2 3 30 1277.24 420.522 3 -2 -3 30 961.507 344.437 3 -2 -3 30 9.51066 188.138 1 -2 -3 29 36876.2 1547.88 3 -2 3 29 37438.2 1562.11 3 -2 -3 29 37994.7 1508.00 1 -2 -3 28 15149.1 982.478 3 -2 3 28 15966.9 1020.32 3 -2 -3 28 14563.0 955.184 1 -2 -3 27 26705.9 1269.93 3 -2 3 27 28200.2 1295.73 3 -2 -3 27 26232.3 1207.80 1 -2 3 26 10506.8 801.908 3 -2 -3 26 10524.7 806.371 3 -2 -3 26 11457.2 800.219 1 -2 -3 25 1854.90 352.192 1 -2 -3 25 1988.68 378.962 3 -2 3 25 2241.97 402.377 3 -2 -3 24 3160.10 418.793 1 -2 3 24 3080.57 435.569 3 -2 -3 24 3433.23 460.803 3 -2 -3 23 10100.7 707.627 1 2 3 -23 11241.6 743.931 1 -2 3 23 10313.7 741.236 3 -2 -3 23 9777.27 727.805 3 2 -3 -22 43.9330 131.777 3 -2 -3 22 407.699 260.323 3 -2 3 22 208.940 211.011 3 -2 -3 22 56.8773 158.271 1 2 3 -22-129.612 149.444 1 -2 -3 21 15456.1 859.570 3 2 -3 -21 16096.2 866.818 3 -2 3 21 16952.1 893.126 3 2 3 -21 16006.1 853.968 1 -2 -3 21 16069.0 849.026 1 2 -3 -20 12156.5 735.642 3 2 -3 -20 12744.3 782.814 1 2 3 -20 12936.7 750.457 1 -2 -3 20 12570.2 742.293 1 2 -3 -19 96965.5 2004.89 3 2 -3 -19 98816.5 2096.63 1 2 3 -19 102883. 2054.34 1 -2 -3 19 97787.3 1983.55 1 2 -3 -18 1770.61 286.640 3 2 -3 -18 1769.35 307.940 1 2 3 -18 1318.12 260.444 1 -2 -3 18 1970.66 316.989 1 2 -3 -17 11244.0 663.761 3 2 -3 -17 11943.3 702.729 1 2 3 -17 11843.8 675.490 1 -2 -3 17 11502.5 663.898 1 2 -3 -16 1093.61 233.127 3 2 -3 -16 1293.45 246.754 1 2 3 -16 1370.08 253.777 1 -2 -3 16 1211.29 259.314 1 2 -3 -15 319.251 139.231 3 2 -3 -15 240.822 163.077 1 2 3 -15 409.516 163.699 1 -2 -3 15 333.789 195.891 1 2 -3 -14 53446.3 1337.13 3 2 -3 -14 54550.1 1358.49 1 2 3 -14 55593.2 1349.11 1 -2 -3 14 54128.8 1330.13 1 2 3 -13 64115.1 1419.67 1 2 -3 -13 63856.1 1424.22 3 2 -3 -13 64332.8 1440.22 1 2 3 -13 63321.5 948.067 2 -2 -3 13 63580.2 1392.58 1 2 3 -12 4622.19 388.814 1 2 -3 -12 4142.05 376.670 3 2 -3 -12 4572.14 395.438 1 2 3 -12 4618.04 261.175 2 -2 -3 12 4729.94 412.149 1 2 3 -11 65255.4 1354.54 1 2 -3 -11 63357.9 1339.45 3 2 -3 -11 62879.5 1330.69 1 2 3 -11 62552.5 923.144 2 -2 -3 11 64064.5 1344.32 1 2 3 -10 15017.8 450.727 2 2 3 -10 16080.1 672.403 1 -2 -3 10 14939.2 665.831 1 2 -3 -10 15384.9 644.506 1 2 3 -9 70786.5 969.410 2 2 3 -9 72625.9 1368.86 1 -2 -3 9 72103.1 1360.58 1 2 -3 -9 69294.8 1306.83 1 -2 -3 8 9123.96 361.641 2 2 3 -8 9071.32 356.844 2 -2 -3 8 8635.70 489.435 1 2 3 -8 8652.18 484.007 1 2 -3 -8 9055.98 464.769 1 2 3 -7 15900.7 471.125 2 -2 -3 7 16450.9 484.143 2 -2 -3 7 16819.4 648.729 1 2 -3 -7 15997.4 584.104 1 -2 -3 6-33.7232 142.305 1 -2 -3 6 259.235 125.645 2 2 3 -6 184.796 91.9478 2 2 -3 -6 274.978 137.113 1 -2 -3 5 200760. 2119.21 1 2 3 -5 194570. 1704.16 2 -2 -3 5 199928. 1700.37 2 2 3 -4 56790.7 936.632 2 -2 -3 4 56675.1 929.644 2 2 3 -3 246088. 1988.13 2 -2 -3 3 251672. 1979.92 2 -2 -3 2 61830.8 1034.24 2 2 3 -2 61823.6 1020.83 2 -2 -3 1 29087.7 724.098 2 2 3 -1 28796.9 719.797 2 2 3 0 231285. 2075.35 2 -2 -3 0 229134. 2068.65 2 -2 -3 -1 5850.62 365.127 2 2 3 1 6036.79 361.641 2 -2 -3 -2 13579.8 545.800 2 2 3 2 12709.3 530.684 2 2 3 3 515931. 3328.49 2 -2 -3 -3 518387. 3330.42 2 2 3 4 17705.2 645.041 2 -2 -3 -4 16634.1 645.388 2 -2 -3 -5 295904. 1414.33 3 2 3 5 296542. 2670.59 2 -2 -3 -5 284679. 2656.99 2 2 -3 6 1129.08 85.0323 1 -2 -3 -6 1583.83 130.581 3 2 3 6 1508.70 234.398 2 2 -3 6 1570.51 146.213 2 -2 -3 -6 1383.29 258.028 2 2 -3 7 185.102 64.8944 1 -2 3 -7 77.5571 55.0596 1 2 3 7 123.174 75.6407 3 2 3 7 69.1736 153.717 2 2 -3 7 240.121 92.8785 2 -2 -3 -7 39.5483 166.705 2 2 -3 8 5938.77 246.272 1 -2 3 -8 4621.76 217.243 1 2 3 8 5095.97 265.148 3 2 3 8 4881.73 401.541 2 2 -3 8 4699.70 220.655 2 -2 -3 -8 4476.99 416.679 2 -2 3 -9 23468.2 510.568 1 2 3 9 23805.9 594.191 3 2 3 9 24545.1 866.174 2 2 -3 9 23733.0 502.279 1 2 -3 9 23080.1 462.247 2 -2 -3 -9 22006.1 834.379 2 2 3 10 3133.49 246.907 3 2 -3 10 3428.27 221.159 1 2 3 10 2954.77 346.897 2 -2 -3 -10 3150.88 353.545 2 -2 3 -10 3012.94 206.741 1 2 -3 10 3396.93 186.756 2 -2 3 -11 129.208 90.9108 1 2 3 11 48.2721 97.8117 3 -2 -3 -11 94.2685 173.180 2 2 -3 11 54.5835 85.6959 1 -2 3 -11 0.73217 60.1911 2 2 -3 11 40.7815 68.6556 2 -2 3 -12 1091.41 158.155 1 2 3 12 1146.93 202.253 3 2 -3 12 1291.46 162.948 1 -2 3 -12 1007.66 118.488 2 2 -3 12 1044.11 116.939 2 -2 -3 -12 1215.74 409.403 2 -2 3 -13 231839. 2052.64 1 2 3 13 236073. 2316.16 3 2 -3 13 236567. 2026.12 1 2 -3 13 231871. 1550.99 2 -2 3 -13 232722. 1593.99 2 -2 -3 -13 235425. 2800.71 2 -2 3 -14 362.977 119.749 1 2 3 14 638.410 184.047 3 2 -3 14 341.558 82.1850 2 2 -3 14 728.186 179.289 1 -2 3 -14 218.243 79.4367 2 -2 3 -15 27571.2 787.778 1 2 3 15 29070.5 889.628 3 2 -3 15 28122.3 773.248 1 -2 3 -15 28262.2 592.908 2 -2 -3 -15 28884.6 1030.72 2 -2 3 -16 19779.3 699.561 1 2 3 16 21077.8 790.351 3 2 -3 16 21635.9 712.212 1 -2 3 -16 20995.4 535.010 2 -2 -3 -16 20964.9 904.942 2 2 3 17 195.525 200.130 3 2 -3 17 99.8681 123.279 1 -2 -3 -17 565.501 275.657 2 -2 3 -17 53.2626 69.6387 2 -2 3 -17 358.860 143.286 1 2 3 18 2969.85 332.719 3 -2 -3 -18 2374.14 354.791 2 2 -3 18 2789.46 283.809 1 -2 3 -18 2723.60 213.019 2 -2 3 -18 2947.45 300.744 1 2 3 19 3217.84 360.994 3 -2 -3 -19 3364.88 408.819 2 2 -3 19 2655.55 291.505 1 -2 3 -19 2952.41 227.978 2 -2 3 -19 3181.77 324.630 1 2 3 20 2291.85 333.280 3 -2 -3 -20 2046.43 376.234 2 -2 3 -20 1375.87 243.467 1 -2 3 -20 1285.86 163.467 2 -2 3 -21 11026.4 631.316 1 -2 3 -21 11110.2 462.016 2 -2 -3 -21 13194.8 796.037 2 2 3 21 13497.3 744.954 3 2 3 22 29593.5 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807.155 2 -2 -4 10 47034.3 814.427 2 -2 -4 9 492.896 214.351 1 2 4 -9 382.041 106.758 2 -2 -4 9 445.678 120.514 2 -2 -4 8 57686.4 1281.46 1 2 4 -8 58238.5 941.245 2 -2 -4 8 57726.2 935.866 2 -2 -4 7 79015.3 1473.02 1 2 4 -7 79774.6 1122.17 2 -2 -4 7 80639.8 1129.15 2 -2 -4 6 13080.8 609.051 1 2 4 -6 12267.6 455.363 2 -2 -4 6 13345.3 478.633 2 -2 -4 5 1432.97 182.931 2 2 4 -5 1746.11 195.858 2 2 4 -4 49665.4 954.398 2 -2 -4 4 51558.5 968.228 2 -2 -4 3 61477.6 1089.19 2 2 4 -3 61185.5 1086.81 2 2 4 -2 85897.4 1317.20 2 -2 -4 2 84376.5 1313.43 2 2 4 -1 65.6724 109.498 2 -2 -4 1 272.639 150.794 2 2 4 0 123673. 1644.19 2 -2 -4 0 125255. 1659.35 2 2 4 1 2707.02 277.801 2 -2 -4 -1 2763.58 295.058 2 2 4 2 76048.1 1372.68 2 -2 -4 -2 75724.9 1361.84 2 2 4 3 18283.1 685.349 2 -2 -4 -3 17849.9 684.915 2 2 4 4 9672.16 528.881 2 -2 -4 -4 9583.36 529.563 2 -2 -4 -5 36540.5 568.083 3 2 4 5 36525.3 1017.99 2 2 -4 5 36698.5 578.765 1 -2 -4 -5 34474.2 1010.62 2 -2 -4 -6 7071.49 276.499 3 2 4 6 7218.25 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1635.87 478.242 2 -2 -6 44 1791.87 489.112 1 -2 -6 43 10302.8 1104.35 3 2 -6 -43 8309.57 944.427 2 -2 -6 43 9190.43 963.260 1 -2 -6 42 12226.2 1192.99 3 2 -6 -42 11660.3 1094.01 2 -2 -6 42 12509.1 1109.06 1 -2 -6 41 328.970 371.135 3 -2 -6 41 388.272 300.622 1 2 -6 -41 600.146 391.741 2 2 -6 -40 4403.16 685.641 2 -2 -6 40 4186.85 633.430 1 -2 -6 39 8719.60 976.929 3 2 -6 -39 9376.70 967.700 2 -2 -6 39 8862.68 895.359 1 -2 -6 38 4905.10 663.488 1 2 -6 -38 4990.77 700.182 2 -2 -6 37 667.085 337.057 3 -2 -6 37 693.827 313.872 1 -2 -6 36 8578.00 892.132 3 -2 -6 36 7771.45 800.861 1 -2 -6 35 325.762 311.379 3 -2 -6 35 151.279 212.158 1 -2 -6 34 3511.07 579.383 3 -2 -6 34 3606.63 519.995 1 -2 -6 33 246.352 236.872 3 -2 -6 33 605.580 262.201 1 -2 -6 32 921.161 315.876 1 -2 -6 31 5327.69 620.159 1 -2 -6 30 7576.22 713.822 1 2 6 -30 6687.27 244.746 2 2 6 -29 3591.88 182.043 2 -2 -6 29 4204.02 533.861 1 2 6 -28 78.6437 38.4159 2 -2 -6 28 334.119 230.262 1 2 6 -27 382.377 70.2846 2 -2 -6 27 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1358.85 2 -2 -6 9 9312.75 430.515 2 -2 -6 9 8712.60 589.938 1 2 6 -9 9238.71 430.987 2 -2 -6 8 15243.6 557.603 2 2 6 -8 15490.4 565.493 2 -2 -6 8 15731.4 765.841 1 -2 -6 7 2282.62 239.922 2 2 6 -7 2163.67 228.020 2 -2 -6 6 13180.5 556.951 2 2 6 -6 12264.5 531.710 2 -2 -6 5 18595.5 676.514 2 2 6 -5 18391.9 668.709 2 -2 -6 4 66142.0 1287.30 2 2 6 -4 65610.0 1280.99 2 -2 -6 3 18438.4 700.630 2 2 6 -3 18816.7 712.375 2 -2 -6 2 43215.6 1089.53 2 2 6 -2 44192.4 1112.49 2 -2 -6 1 19487.4 749.910 2 2 6 -1 20364.7 782.191 2 -2 -6 0 89809.8 1629.99 2 2 6 0 91484.6 1678.33 2 -2 -6 -1 44937.0 1180.76 2 2 6 1 45913.7 1213.20 2 -2 -6 -2 112283. 1905.59 2 2 6 2 116069. 1955.46 2 -2 -6 -3 10863.3 620.509 2 -2 -6 -4 55582.1 1403.66 2 -2 -6 -5 547.561 207.346 2 -2 -6 -6 2088.75 321.649 2 2 -6 7 33121.6 767.812 1 -2 -6 -7 30800.8 1116.41 2 2 -6 8 5795.34 325.357 1 -2 -6 -8 6029.47 519.524 2 -2 -6 -8 5763.64 322.530 3 2 -6 9 20493.5 617.980 1 -2 -6 -9 20103.0 929.057 2 -2 -6 -9 19601.9 612.041 3 2 -6 10 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514.504 2 2 7 -9 11534.4 515.016 2 -2 -7 9 11676.6 714.067 1 2 7 -8 272.400 124.710 2 -2 -7 8 417.455 146.602 2 -2 -7 8 397.088 222.849 1 -2 -7 7 750.955 169.318 2 2 7 -7 956.714 180.337 2 -2 -7 6 7450.20 449.166 2 2 7 -6 7215.23 452.267 2 -2 -7 5 10508.0 552.165 2 2 7 -5 10983.9 559.068 2 -2 -7 4 80.7268 118.103 2 -2 -7 3 15582.3 690.879 2 -2 -7 2 5068.26 420.232 2 -2 -7 1 5989.27 453.703 2 -2 -7 0 14535.4 713.259 2 -2 -7 -1 13978.5 715.375 2 -2 -7 -2 205.679 179.531 2 -2 -7 -3 143017. 2325.62 2 -2 -7 -4 6387.66 524.436 2 -2 -7 -5 2652.02 364.525 2 -2 -7 -6 1107.83 266.340 2 -2 -7 -7 33245.5 1201.53 2 2 -7 7 33303.0 865.581 1 -2 -7 -8 20884.5 969.151 2 2 -7 8 19010.1 655.148 1 -2 -7 -9 51696.1 1051.89 3 -2 -7 -9 50910.3 1523.77 2 2 -7 9 52152.4 1081.70 1 -2 -7 -10 21940.4 709.798 3 2 -7 10 23442.1 734.991 1 -2 -7 -10 22051.2 1046.52 2 -2 -7 -11 138.558 99.2921 3 2 -7 11 224.160 93.7603 1 2 -7 12 30254.7 544.568 2 -2 -7 -12 33188.0 906.758 3 2 -7 12 28997.1 525.481 2 -2 -7 -12 33595.3 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1033.50 2 2 -12 -4 210.912 188.203 2 -2 -12 4 247.902 224.268 2 2 -12 -3 1284.06 306.896 2 -2 -12 3 745.306 240.499 2 2 -12 -2 1521.15 320.647 2 -2 -12 2 1231.62 300.473 2 2 -12 -1 1995.71 366.354 2 -2 -12 1 1208.06 300.623 2 2 -12 0 29.3618 155.012 2 -2 -12 0 509.119 269.495 2 2 -12 1 16544.5 916.884 2 -2 -12 -1 17972.6 1041.39 2 2 -12 2 4410.28 487.545 2 -2 -12 -2 4352.07 539.112 2 2 -12 3 12596.6 772.582 2 -2 -12 -3 12717.5 912.194 2 2 -12 4 812.049 235.996 2 -2 -12 -4 1263.40 333.925 2 2 -12 5 944.726 251.994 2 -2 -12 -5 1079.94 311.968 2 2 -12 6 1461.24 277.073 2 -2 -12 -6 1300.79 345.697 2 2 -12 7 1342.20 248.063 2 -2 -12 -7 1264.78 302.883 2 2 -12 8 1246.70 234.009 2 2 -12 8 1214.96 268.541 1 -2 -12 -8 1234.23 347.360 2 2 -12 9 9371.30 675.634 1 2 -12 9 8605.51 543.914 2 -2 -12 -9 8593.80 810.365 2 2 -12 10 16957.9 896.082 1 -2 -12 -10 17589.7 1154.19 2 2 -12 10 16641.5 727.982 2 2 -12 11 7410.73 592.170 1 2 -12 11 7610.77 476.000 2 -2 -12 -11 7583.59 787.145 2 2 -12 12 625.571 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421.609 1 2 -13 -25 376.825 348.859 2 -2 -13 25 318.929 251.635 1 2 -13 -24 8262.90 944.438 2 -2 -13 24 8267.97 836.954 1 -2 -13 23 1912.85 458.601 1 2 -13 -23 1746.05 474.972 2 -2 -13 22 179.058 234.028 1 2 -13 -22-117.462 242.358 2 -2 -13 21 6822.54 767.019 1 2 -13 -21 7177.58 871.175 2 -2 -13 20 4951.48 658.766 1 2 -13 -20 7121.51 850.497 2 -2 -13 19 16305.4 1145.75 1 2 -13 -19 15143.0 1205.68 2 -2 -13 18 4076.00 616.036 1 2 -13 -18 4561.74 689.351 2 -2 -13 17-23.9409 235.668 1 2 -13 -17 428.320 308.911 2 -2 -13 16 1364.68 369.255 1 2 -13 -16 640.792 295.170 2 -2 -13 15 1284.12 342.669 1 2 -13 -15 1531.96 398.535 2 -2 -13 14 7956.40 790.323 1 2 -13 -14 7118.67 789.083 2 -2 -13 13-85.6406 195.620 1 2 -13 -13 468.776 331.397 2 -2 -13 12 51.0112 226.460 1 2 -13 -12 406.061 335.671 2 -2 -13 11 9136.81 625.823 2 -2 -13 11 9717.81 871.452 1 2 -13 -11 10646.6 930.822 2 -2 -13 10 14916.6 822.142 2 2 -13 -10 13867.6 1053.48 2 -2 -13 10 14869.3 1062.63 1 2 -13 -9 7293.14 762.083 2 -2 -13 9 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5549.32 685.998 2 2 -13 8 5401.97 550.888 1 -2 -13 -9 1154.05 337.285 2 2 -13 9 1349.18 288.418 1 -2 -13 -10 4475.41 623.623 2 2 -13 10 4005.68 467.023 1 -2 -13 -11 371.185 259.023 2 2 -13 11 659.529 206.658 1 -2 -13 -12 10068.9 937.958 2 2 -13 12 10176.3 740.706 1 -2 -13 -13 2722.00 547.017 2 2 -13 13 2069.53 353.770 1 -2 -13 -14 6153.79 779.340 2 2 -13 14 5698.84 551.893 1 -2 -13 -15 9593.65 954.865 2 -2 -13 -16 68.5593 270.975 2 -2 -13 -17 2444.35 506.937 2 -2 -13 -18 598.928 366.095 2 -2 -13 -19 2185.70 520.418 2 -2 -13 -20 2187.44 510.152 2 -2 -13 -21 834.014 390.039 2 -2 -13 -22 784.788 433.802 2 -2 -13 -23 10453.5 1080.80 2 -2 -13 -24 616.488 406.009 2 -2 -13 -25-6.83513 262.888 2 -2 -13 -26 2124.36 557.366 2 -2 -13 -27-220.951 233.937 2 -2 -13 -28 1627.40 526.335 2 2 -14 -26 6203.33 859.491 2 2 -14 -25 1065.53 439.334 2 -2 -14 25 289.025 214.763 1 2 -14 -24 1216.91 428.710 2 -2 -14 24 1676.65 414.702 1 2 -14 -23 1903.20 496.474 2 -2 -14 23 1256.26 398.033 1 2 -14 -22 3844.00 678.592 2 -2 -14 22 3141.19 540.970 1 2 -14 -21 4750.46 728.375 2 -2 -14 21 4687.56 661.116 1 2 -14 -20 1343.56 471.651 2 -2 -14 20 1287.38 391.025 1 2 -14 -19 5591.35 782.388 2 -2 -14 19 4971.30 674.579 1 2 -14 -18 19.4457 215.334 2 -2 -14 18-18.0726 214.014 1 2 -14 -17 1745.12 443.201 2 -2 -14 17 2412.55 485.152 1 2 -14 -16 1313.37 413.126 2 -2 -14 16 926.285 324.605 1 2 -14 -15 1000.43 359.259 2 -2 -14 15 763.450 317.076 1 2 -14 -14 339.330 261.981 2 -2 -14 14-316.387 264.899 1 2 -14 -13 2087.68 464.048 2 -2 -14 13 2091.04 458.619 1 2 -14 -12 6786.70 773.180 2 -2 -14 12 7454.40 813.080 1 2 -14 -11 1160.96 357.990 2 -2 -14 11 826.191 341.963 1 2 -14 -10 2357.16 476.981 2 -2 -14 10 3234.62 544.723 1 2 -14 -9 6487.52 736.288 2 -2 -14 9 6556.74 765.422 1 2 -14 -8 1717.60 396.609 2 -2 -14 8 2200.34 374.240 2 -2 -14 8 2524.82 481.257 1 -2 -14 7 549.918 239.457 2 2 -14 -7 674.460 300.962 2 -2 -14 6 1504.79 326.760 2 2 -14 -6 1987.39 442.273 2 -2 -14 5 1191.67 319.033 2 2 -14 -5 1138.67 327.488 2 -2 -14 4 5376.65 590.720 2 2 -14 -4 6137.95 685.732 2 -2 -14 3 1024.07 301.628 2 2 -14 -3 600.800 268.923 2 -2 -14 2 6785.48 658.924 2 2 -14 -2 7152.96 713.877 2 -2 -14 1 3100.15 478.915 2 2 -14 -1 3179.09 474.260 2 -2 -14 0 8263.15 759.470 2 2 -14 0 7862.97 719.642 2 -2 -14 -1 1957.55 414.307 2 2 -14 1 2586.34 447.204 2 -2 -14 -2 5091.26 630.737 2 2 -14 2 4774.40 548.270 2 -2 -14 -3 1505.29 394.248 2 2 -14 3 1789.20 354.881 2 -2 -14 -4 4304.91 600.167 2 2 -14 4 3580.83 454.865 2 2 -14 5 7496.05 626.282 2 -2 -14 -5 7778.41 794.186 2 -2 -14 -6 1852.96 440.980 2 -2 -14 -7 3464.71 555.270 2 2 -14 7 3382.17 473.101 1 -2 -14 -8 20.4388 223.831 2 2 -14 8 379.558 211.399 1 -2 -14 -9 3938.01 613.322 2 2 -14 9 4254.49 516.388 1 -2 -14 -10 1046.54 369.393 2 -2 -14 -11-49.1282 207.624 2 -2 -14 -12 5348.89 708.637 2 -2 -14 -13 493.969 331.925 2 -2 -14 -14 4039.38 647.796 2 -2 -14 -15 105.602 256.292 2 -2 -14 -16 1867.03 475.258 2 -2 -14 -17 6961.84 866.133 2 -2 -14 -18 1167.09 411.985 2 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246.306 1 2 -15 -7 52.7487 212.333 2 -2 -15 7 549.076 290.046 1 2 -15 -6 1009.27 323.596 2 -2 -15 5 210.742 242.059 2 2 -15 -5 401.205 290.110 2 -2 -15 4 5913.26 651.361 2 2 -15 -4 6953.10 744.735 2 -2 -15 3 145.361 194.561 2 2 -15 -3 686.623 291.445 2 -2 -15 2 17.6388 200.101 2 2 -15 -2-79.5068 190.578 2 -2 -15 1 377.451 272.932 2 2 -15 -1 668.176 282.226 2 -2 -15 0 12491.0 981.929 2 2 -15 0 11992.8 907.416 2 -2 -15 -1-176.263 204.725 2 2 -15 1 59.9229 218.361 2 -2 -15 -2 979.694 331.376 2 2 -15 2 769.810 232.675 2 -2 -15 -3 334.127 256.362 2 -2 -15 -4-272.174 245.727 2 -2 -15 -5 276.208 244.427 2 -2 -15 -6 939.809 342.198 2 -2 -15 -7-73.2922 196.480 2 -2 -15 -8 2345.79 506.624 2 -2 -15 -9 737.611 340.636 2 -2 -15 -10 7143.20 836.584 2 -2 -15 -11 165.025 281.192 2 -2 -15 -12 263.354 270.445 2 -2 -15 -13 450.569 312.023 2 -2 -15 -14 819.635 380.039 2 -2 -15 -15 387.743 260.103 2 -2 -15 -16 6615.28 852.386 2 -2 -15 -17 420.461 365.873 2 -2 -15 -18 422.860 234.032 2 -2 -15 -19 14.2450 244.645 2 -2 -15 -20 775.497 381.434 2 -2 -15 -21 384.087 339.889 2 2 -16 -19 708.557 398.482 2 2 -16 -18 370.823 302.064 2 2 -16 -17 3942.54 699.592 2 2 -16 -16 91.6313 226.581 2 -2 -16 16 477.654 287.051 1 2 -16 -15 305.562 321.602 2 -2 -16 15 457.161 286.680 1 2 -16 -14 47.0256 251.419 2 -2 -16 14 508.900 280.279 1 2 -16 -13 1599.33 474.719 2 -2 -16 13 1553.32 450.058 1 2 -16 -12 2811.71 566.613 2 -2 -16 12 3504.09 607.101 1 2 -16 -11 1372.47 435.947 2 -2 -16 11 725.815 348.293 1 2 -16 -10 2163.79 514.393 2 -2 -16 10 1886.11 470.131 1 2 -16 -9 1059.82 369.845 2 -2 -16 9 468.569 312.585 1 2 -16 -8 627.141 267.888 2 -2 -16 8 1381.90 422.359 1 2 -16 -7 1762.73 416.138 2 -2 -16 7 1712.50 426.793 1 2 -16 -6-278.571 274.138 2 -2 -16 6 55.6717 207.327 1 2 -16 -5 610.118 284.110 2 2 -16 -4 12.7762 235.804 2 2 -16 -3 263.783 267.322 2 2 -16 -2 5874.97 699.860 2 -2 -16 1 3641.36 569.971 2 -2 -16 0 730.604 318.356 2 -2 -16 -1 212.818 243.504 2 -2 -16 -2 1726.60 436.284 2 -2 -16 -3 140.022 224.211 2 -2 -16 -4 544.456 295.034 2 -2 -16 -5 1122.96 386.490 2 -2 -16 -6 776.664 275.906 2 -2 -16 -7-12.9976 218.722 2 -2 -16 -8 1045.85 400.211 2 -2 -16 -9 1952.27 451.283 2 -2 -16 -10-5.36836 256.021 2 -2 -16 -11 205.183 255.050 2 -2 -16 -12 167.541 278.830 2 -2 -16 -13 2408.66 557.141 2 -2 -16 -14 1612.34 498.223 2 -2 -16 -15 283.971 371.688 2 -2 -16 -16 365.591 286.456 2 -2 -16 -17 3631.53 692.192 2 2 -17 -15 394.556 281.375 2 2 -17 -14 288.355 282.119 2 2 -17 -13-74.8435 224.882 2 2 -17 -12 298.374 301.088 2 2 -17 -11 2249.41 529.825 2 -2 -17 11 3350.68 613.461 1 2 -17 -10-103.355 206.138 2 -2 -17 10 62.9321 214.878 1 2 -17 -9 1172.51 398.769 2 -2 -17 9 997.795 381.676 1 2 -17 -8-151.025 213.405 2 -2 -17 8-22.7026 266.927 1 2 -17 -7 480.536 276.375 2 -2 -17 7-9.64398 286.578 1 2 -17 -6 247.932 265.350 2 -2 -17 6-53.3738 235.196 1 -2 -17 5 720.760 374.018 1 -2 -17 -3 17.7197 207.279 2 -2 -17 -4 220.120 230.454 2 -2 -17 -5 2467.12 518.174 2 -2 -17 -6 248.355 294.223 2 -2 -17 -7 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234.281 68.2231 1 5 2 5 333.224 181.083 2 5 -2 5 238.766 148.378 2 -5 -2 -5 405.292 208.703 2 5 2 6 47605.2 1321.39 2 5 -2 6 46083.1 1148.67 2 -5 -2 -6 47923.3 1327.21 2 -5 2 -7 56669.5 1294.13 2 5 -2 7 55851.1 1283.00 2 -5 -2 -7 57890.5 1458.56 2 5 2 7 56111.9 1452.02 2 -5 2 -8 17557.5 726.731 2 -5 -2 -8 18702.2 847.001 2 5 -2 8 17762.4 722.293 2 5 2 8 16871.4 813.635 2 -5 2 -9 259.726 158.635 2 5 -2 9 236.561 123.072 2 5 2 9 116.984 135.010 2 -5 -2 -9 282.352 174.941 2 -5 2 -10 2605.80 297.166 2 5 2 10 2858.28 365.003 2 5 -2 10 2888.53 306.310 2 -5 -2 -10 2331.45 338.344 2 -5 2 -11 48455.9 1216.39 2 -5 -2 -11 48743.1 1413.39 2 5 2 11 50195.0 1434.86 2 5 -2 11 50587.4 1233.82 2 -5 2 -12 95496.9 1714.64 2 -5 -2 -12 92160.6 1971.61 2 5 2 12 96868.0 2024.81 2 5 -2 12 93541.7 1676.26 2 -5 2 -13 23820.5 873.992 2 5 -2 13 23168.0 846.346 2 5 2 13 24822.7 1030.78 2 -5 -2 -13 22790.6 1002.34 2 -5 2 -13 21797.8 641.711 1 -5 2 -14 11007.7 602.777 2 5 -2 14 11253.8 597.491 2 -5 -2 -14 10461.9 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1 5 -2 23 5333.82 462.579 2 -5 -2 -23 5427.89 570.791 2 -5 2 -23 5414.70 489.993 2 5 -2 24 7263.90 539.433 2 -5 2 -24 7482.00 556.966 1 -5 2 -24 8083.21 586.973 2 -5 -2 -24 7567.48 668.861 2 5 2 25 348.874 209.349 3 5 -2 25 195.295 118.572 2 -5 2 -25 575.317 201.046 2 -5 -2 -25 765.824 313.528 2 -5 2 -26 12791.4 763.706 1 -5 2 -26 14414.1 795.931 2 -5 -2 -26 12505.0 878.854 2 5 2 26 12829.1 832.642 3 -5 2 -27 284.686 189.232 1 -5 2 -27 671.915 245.099 2 5 2 27 396.419 251.445 3 -5 2 -28 23799.7 1082.70 1 5 2 28 22869.3 1157.08 3 -5 -2 -28 26345.7 1303.00 2 -5 2 -28 25634.3 1086.76 2 5 2 29 6398.65 644.090 3 -5 -2 -29 8732.60 782.009 2 -5 2 -29 7055.70 597.601 2 5 2 30 1024.88 317.049 3 -5 -2 -30 1616.41 414.597 2 -5 2 -30 1262.82 289.674 2 5 2 31 5345.58 618.455 3 -5 -2 -31 6318.55 718.727 2 -5 2 -31 5039.06 526.428 2 5 2 32 26145.4 1340.96 3 -5 -2 -32 28932.6 1430.56 2 -5 2 -32 28525.6 1202.03 2 -5 -2 -33 12557.9 980.450 2 -5 2 -33 12857.2 838.773 2 5 2 34 18550.4 1178.29 3 -5 -2 -34 20657.2 1241.41 2 -5 2 -34 20953.1 1061.89 2 5 2 35 4659.14 635.181 3 -5 -2 -35 4473.72 657.321 2 -5 2 -35 4541.64 522.421 2 5 2 36 10390.0 924.013 3 -5 -2 -36 11705.8 961.252 2 -5 2 -36 11983.0 831.267 2 5 2 37 464.066 256.992 3 -5 -2 -37 1187.38 386.609 2 5 2 38 1033.42 354.609 3 -5 -2 -38 1295.19 369.803 2 5 2 39 213.867 237.052 3 -5 -2 -39 301.739 231.535 2 5 2 40 512.456 284.410 3 -5 -2 -40 699.820 294.855 2 5 2 41-3.96869 234.008 3 5 -2 41-426.433 327.228 3 -5 -2 -41 206.888 300.340 2 5 2 42 5753.21 762.750 3 5 -2 42 7919.17 947.815 3 -5 -2 -42 7213.98 820.297 2 -5 -2 -43 1484.15 426.086 2 5 2 44 5778.27 803.721 3 5 -2 44 5091.14 755.292 3 -5 -2 -44 5425.56 743.009 2 5 -2 45 336.140 343.385 3 5 2 46 2350.80 542.602 3 5 2 48-169.069 219.611 3 -5 -3 48 985.094 424.544 1 -5 -3 47 1104.07 468.917 1 -5 -3 46 3918.86 721.592 3 -5 -3 46 2709.04 576.145 1 -5 -3 45 1297.90 480.129 3 -5 -3 45 950.024 410.014 1 -5 -3 44 6448.32 881.747 3 -5 -3 44 6443.90 850.268 1 -5 -3 43 2753.66 596.998 1 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1116.38 197.837 3 -5 -3 9 950.032 185.333 3 -5 3 9 1308.50 269.352 1 5 3 -9 1023.60 213.649 2 5 -3 -9 1264.48 233.919 1 -5 -3 8 14522.3 776.571 1 5 3 -8 15677.5 591.642 3 -5 -3 8 14848.7 574.553 3 -5 3 8 15550.1 641.258 1 5 3 -8 16197.8 720.472 2 -5 -3 8 15374.5 713.482 2 5 -3 -8 14940.0 631.361 1 -5 -3 7 876.551 247.141 1 5 3 -7 801.478 151.120 3 -5 3 7 1087.55 216.870 1 -5 -3 7 915.030 230.515 2 5 3 -7 894.634 211.807 2 5 -3 -7 784.505 163.283 1 -5 -3 6 3285.62 376.118 1 5 3 -6 3491.38 259.582 3 -5 3 6 3771.08 316.199 1 5 3 -6 4280.02 398.827 2 -5 -3 6 3555.32 370.267 2 5 -3 -6 3626.52 298.003 1 -5 -3 5 11729.9 668.536 1 5 3 -5 11266.4 434.618 3 -5 3 5 11294.5 502.121 1 -5 -3 5 11496.8 633.564 2 5 3 -5 10486.9 597.018 2 5 -3 -5 10587.7 470.534 1 -5 -3 4 60289.6 1457.67 1 5 3 -4 60984.6 943.326 3 -5 3 4 59695.3 1054.31 1 5 3 -4 61421.6 1415.66 2 -5 -3 4 59898.8 1429.90 2 5 -3 -4 61491.3 1049.27 1 5 3 -3 4332.04 243.166 3 -5 3 3 5092.80 349.174 1 5 3 -3 4157.05 389.789 2 -5 -3 3 3569.36 394.504 2 5 -3 -3 4417.98 273.718 1 5 -3 -2 84799.5 1105.53 1 5 3 -2 85145.9 969.179 3 -5 3 2 85013.2 1117.88 1 -5 -3 2 82756.9 1670.50 2 5 3 -2 86187.2 1702.39 2 -5 3 1 298.783 164.223 1 5 -3 -1-30.0275 72.5088 1 5 3 -1-15.9754 55.7825 3 -5 -3 1 40.2065 181.660 2 5 3 -1-5.17265 138.037 2 5 -3 0 22311.9 496.512 1 5 3 0 21678.5 433.521 3 -5 3 0 22288.5 496.280 1 -5 -3 0 22222.9 898.522 2 5 3 0 23000.7 916.209 2 5 3 1 5982.01 219.119 3 -5 3 -1 6242.72 247.479 1 5 3 1 6591.94 502.827 2 -5 -3 -1 6250.26 508.115 2 -5 3 -2 2171.76 142.964 1 5 3 2 2174.53 313.641 2 -5 -3 -2 2159.75 340.304 2 5 -3 2 2499.10 293.158 2 5 3 3 33468.0 1117.84 2 -5 -3 -3 33804.9 1133.04 2 5 -3 3 34005.5 993.544 2 5 3 4 31795.2 1099.79 2 -5 -3 -4 29273.8 1061.62 2 5 -3 4 31179.3 942.100 2 5 3 5 1545.14 284.218 2 -5 -3 -5 1874.68 337.446 2 5 -3 5 1266.25 219.861 2 5 3 6 257262. 3176.42 2 5 -3 6 251596. 2647.27 2 -5 -3 -6 253070. 3115.35 2 5 3 7 83512.8 1841.90 2 -5 -3 -7 77607.9 1780.35 2 5 -3 7 80939.1 1497.29 2 5 3 8 4551.70 453.070 2 -5 -3 -8 4156.50 437.773 2 5 -3 8 4405.35 364.179 2 5 3 9 34299.8 1208.63 2 -5 -3 -9 33636.5 1196.72 2 5 -3 9 34096.4 978.196 2 -5 3 -10 6469.00 245.246 1 -5 -3 -10 7276.75 581.377 2 5 3 10 8125.83 595.655 2 5 -3 10 7095.24 452.170 2 -5 3 -11 4865.00 237.919 1 5 -3 11 5294.59 391.136 2 5 3 11 4486.15 456.719 2 -5 -3 -11 5084.82 503.107 2 -5 3 -12 24832.2 853.153 2 -5 3 -12 23495.9 541.796 1 5 3 12 24156.9 1042.43 2 -5 -3 -12 22528.3 1015.71 2 5 -3 12 24621.8 840.300 2 -5 3 -13 1334.21 163.971 1 -5 3 -13 1163.29 218.826 2 5 -3 13 1223.01 206.319 2 -5 -3 -13 866.698 257.068 2 5 3 13 940.008 230.747 2 -5 3 -14 13955.5 480.406 1 5 -3 14 14527.3 653.058 2 -5 -3 -14 14309.1 841.676 2 -5 3 -14 14554.1 662.050 2 -5 3 -15 10646.9 451.342 1 5 -3 15 9668.97 535.480 2 -5 -3 -15 9680.06 719.398 2 -5 3 -15 9918.44 549.557 2 -5 3 -16 70764.8 1183.71 1 -5 3 -16 71172.9 1470.23 2 5 -3 16 71119.1 1444.60 2 -5 -3 -16 71729.2 1899.45 2 -5 3 -17 12967.6 541.203 1 -5 3 -17 13327.8 649.469 2 -5 -3 -17 13355.9 848.225 2 5 -3 17 12825.5 629.155 2 5 3 17 13290.9 648.950 3 -5 3 -18 5565.79 372.956 1 5 3 18 6125.04 461.181 3 -5 3 -18 6014.22 445.251 2 -5 -3 -18 5255.40 546.707 2 5 -3 18 5712.24 427.411 2 -5 3 -19 2018.27 246.762 1 5 3 19 1985.58 290.400 3 5 -3 19 1941.72 253.866 2 -5 3 -19 2475.30 306.159 2 -5 -3 -19 1990.90 378.657 2 -5 3 -20 8629.69 496.478 1 5 3 20 8969.36 588.382 3 -5 3 -20 8327.96 535.462 2 -5 -3 -20 8067.19 686.623 2 5 -3 20 7899.72 504.742 2 -5 3 -21 4730.42 395.162 1 5 3 21 4601.44 440.195 3 5 -3 21 4934.59 409.299 2 -5 3 -21 4740.69 414.751 2 -5 -3 -21 5495.17 591.701 2 -5 3 -22 7918.30 518.615 1 5 3 22 7867.08 578.234 3 5 -3 22 7940.46 524.295 2 -5 3 -22 8502.43 549.448 2 -5 -3 -22 8883.86 738.739 2 -5 3 -23 3363.15 368.032 1 5 3 23 3628.94 426.751 3 -5 3 -23 3137.15 362.575 2 -5 -3 -23 4152.47 586.685 2 -5 3 -24 24443.5 955.414 1 5 -3 24 23843.3 919.189 2 -5 3 -24 25032.7 959.902 2 -5 -3 -24 25721.4 1261.80 2 -5 3 -25 2241.27 317.853 1 -5 3 -25 1989.27 279.481 2 -5 -3 -25 2291.87 440.068 2 5 3 25 2220.93 375.875 3 -5 3 -26 1605.62 279.702 1 -5 3 -26 1060.41 222.930 2 -5 -3 -26 1588.35 382.221 2 5 3 26 2009.14 345.174 3 -5 3 -27 6614.60 560.094 1 -5 3 -27 7011.82 546.158 2 -5 -3 -27 7978.59 773.886 2 5 3 27 7469.85 650.639 3 -5 3 -28 26116.7 1100.32 1 -5 3 -28 27400.1 1054.57 2 -5 -3 -28 27796.7 1378.68 2 5 3 28 27615.7 1236.22 3 -5 3 -29 473.350 210.002 1 5 3 29 1001.37 340.757 3 -5 3 -29 384.132 232.367 2 5 3 30 41613.1 1582.69 3 -5 -3 -30 42691.8 1738.10 2 -5 3 -30 43826.7 1365.78 2 5 3 31 3900.50 529.763 3 -5 -3 -31 5422.64 673.222 2 -5 3 -31 4438.82 464.909 2 5 3 32 2421.83 436.112 3 -5 -3 -32 3631.00 579.514 2 -5 3 -32 2932.36 384.488 2 5 3 33 537.235 269.318 3 -5 -3 -33 215.197 220.424 2 -5 3 -33 413.162 206.526 2 5 3 34 1885.73 389.302 3 -5 -3 -34 2089.68 431.834 2 -5 3 -34 2033.78 335.485 2 5 3 35 1261.47 327.634 3 -5 -3 -35 1731.40 452.973 2 -5 -3 -36 3740.97 605.194 2 5 3 37 1804.88 471.444 3 -5 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2875.05 593.704 3 -5 -4 38 3049.20 591.239 1 -5 -4 37 517.402 310.443 1 -5 -4 36 307.352 315.966 3 -5 -4 36 455.390 303.970 1 -5 -4 35 8123.60 881.770 3 -5 -4 35 8477.07 876.892 1 -5 -4 34 8955.60 878.221 1 -5 -4 34 8825.42 883.547 3 -5 -4 33 1969.28 424.865 1 -5 -4 33 3051.97 563.491 3 -5 -4 32 15758.0 1130.04 1 -5 -4 32 16705.4 1153.96 3 -5 -4 31 11917.9 966.699 1 -5 -4 31 11608.2 954.146 3 -5 -4 30 1415.04 393.243 1 -5 -4 30 1907.86 448.038 3 -5 -4 29 6646.87 725.281 1 -5 -4 29 5616.01 643.399 3 -5 -4 28 2282.79 448.713 3 -5 -4 28 2043.93 428.642 1 5 4 -28 1526.44 266.956 2 -5 -4 27 17450.2 1071.11 3 -5 -4 27 16276.7 1081.20 1 5 4 -27 15468.9 778.742 2 -5 -4 26 30598.6 1373.95 3 -5 -4 26 31272.8 1443.06 1 5 4 -26 30564.6 1077.48 2 -5 -4 25 1357.98 348.329 1 5 4 -25 1289.59 246.405 2 -5 -4 24 6995.24 638.867 3 -5 -4 24 6150.22 648.049 1 5 4 -24 6086.14 478.288 2 -5 -4 23 12748.0 841.315 3 -5 -4 23 13247.4 927.937 1 5 4 -23 12250.1 664.175 2 -5 -4 22-196.616 229.947 1 5 4 -22 179.522 115.362 2 -5 -4 21 62611.4 1734.13 3 -5 -4 21 65093.2 1939.86 1 5 4 -21 59225.3 1428.27 2 -5 -4 20 880.623 293.144 1 5 4 -20 916.485 203.439 2 -5 -4 19 39020.7 1306.71 3 5 4 -19 37975.4 1134.80 2 -5 -4 19 39529.7 1451.86 1 -5 -4 18-56.0022 184.070 1 5 4 -18 265.975 129.366 2 -5 -4 17 28541.4 1070.70 3 -5 -4 17 28697.7 1220.14 1 5 -4 -17 28527.8 1133.75 1 5 4 -17 27979.8 965.650 2 -5 -4 16 42824.7 1275.25 3 5 4 -16 41218.0 1165.69 2 5 -4 -16 43165.3 1360.01 1 -5 -4 16 41055.2 1422.46 1 -5 -4 15 1383.16 298.156 3 5 4 -15 823.645 231.267 1 -5 -4 15 955.749 275.455 1 5 4 -15 905.788 207.367 2 5 -4 -15 1197.29 264.924 1 -5 -4 14 1594.05 282.810 3 5 4 -14 1494.69 305.855 1 -5 -4 14 1679.55 334.206 1 5 4 -14 1460.46 239.212 2 5 -4 -14 1734.25 296.214 1 -5 -4 13 35104.6 1058.61 3 5 4 -13 36361.5 1301.13 1 -5 -4 13 37494.7 1313.04 1 5 4 -13 37719.2 1107.31 2 5 -4 -13 37782.8 1176.86 1 -5 -4 12 1787.46 257.446 3 -5 -4 12 2106.06 351.113 1 5 4 -12 2096.58 286.869 2 5 -4 -12 2321.43 322.261 1 -5 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1445.47 2 -5 -4 3 58359.0 1432.70 2 5 -4 -2 32691.5 691.800 1 5 4 -2 32996.7 1106.21 2 -5 -4 2 31548.5 1076.04 2 5 -4 -1 32984.2 636.098 1 5 4 -1 34316.6 1135.16 2 -5 -4 1 34105.8 1127.49 2 5 -4 0 115119. 1088.91 1 5 4 0 120409. 2133.87 2 -5 -4 0 120317. 2122.93 2 5 -4 1 1446.99 115.852 1 -5 -4 -1 1258.59 265.125 2 5 4 1 1139.52 238.542 2 5 4 2 2330.08 324.128 2 -5 -4 -2 1926.25 324.582 2 5 4 3 1301.76 249.367 2 -5 -4 -3 938.294 256.549 2 5 -4 4 10752.8 569.055 2 5 4 4 11481.1 692.409 2 -5 -4 -4 10883.1 672.918 2 5 4 5 141667. 2440.86 2 -5 -4 -5 140550. 2395.74 2 5 -4 5 141635. 2005.56 2 5 4 6 29088.2 1134.32 2 -5 -4 -6 27482.2 1112.40 2 5 -4 6 28143.3 890.381 2 -5 -4 -7 782.262 247.134 2 5 4 7 1334.53 269.883 2 5 -4 7 1260.34 219.913 2 5 4 8 5740.69 228.780 3 5 -4 8 5838.05 409.312 2 5 4 8 5941.53 542.372 2 -5 -4 -8 5472.84 532.680 2 5 4 9 2511.87 172.774 3 5 4 9 2697.86 374.987 2 -5 -4 -9 2484.48 380.782 2 5 -4 9 2984.64 296.648 2 5 4 10 33254.0 654.661 3 5 4 10 36480.7 1309.67 2 -5 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1060.33 2 5 -4 20 17207.3 699.205 2 -5 4 -21 848.828 180.093 1 5 4 21 1157.69 262.130 3 5 -4 21 519.993 153.864 2 -5 4 -21 715.881 162.744 2 -5 -4 -21 448.330 253.513 2 5 -4 22-13.4126 89.7695 2 -5 4 -22 140.811 138.114 2 5 4 23 62750.1 1613.08 3 5 -4 23 61884.6 1349.49 2 -5 4 -23 67454.9 1459.00 2 -5 -4 -23 65085.1 2032.88 2 5 4 24 5905.40 547.917 3 5 -4 24 4063.60 362.818 2 -5 4 -24 4836.24 409.919 2 -5 -4 -24 5610.77 653.705 2 -5 4 -25 1230.31 245.399 1 -5 4 -25 874.213 199.847 2 -5 -4 -25 1470.13 416.775 2 5 4 25 1615.54 327.382 3 -5 4 -26 11439.9 667.919 1 5 4 26 11799.4 763.309 3 -5 -4 -26 12300.5 923.518 2 -5 4 -26 12405.4 650.199 2 5 4 27 968.381 284.893 3 -5 -4 -27 670.717 347.233 2 -5 4 -27 758.186 193.942 2 5 4 28 4168.81 515.458 3 -5 -4 -28 4159.28 594.750 2 -5 4 -28 3345.10 359.800 2 5 4 29 16667.1 978.353 3 -5 -4 -29 17615.7 1148.42 2 -5 4 -29 17579.4 798.299 2 5 4 30 2761.16 439.441 3 -5 -4 -30 3633.21 574.952 2 -5 4 -30 2420.40 326.804 2 5 4 31 5562.55 602.235 3 -5 -4 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6926.89 713.515 1 5 5 -25 6502.95 491.067 2 -5 -5 24-26.0568 181.039 1 -5 -5 24 1955.50 450.879 3 -5 -5 23 49995.7 1633.85 3 -5 -5 23 52122.8 1813.45 1 5 5 -23 48551.8 1293.36 2 -5 -5 22 73.4567 226.598 1 5 5 -22-17.2021 113.408 2 -5 -5 21 8295.91 653.501 3 5 5 -21 8505.95 540.563 2 -5 -5 21 8347.49 721.230 1 5 5 -20 140.859 119.560 2 -5 -5 20 106.873 224.234 1 -5 -5 19 34542.9 1417.32 1 -5 -5 19 33887.7 1233.41 3 -5 -5 18 12721.7 773.172 3 -5 -5 18 10670.4 791.156 1 5 5 -18 9659.62 571.121 2 -5 -5 17 30191.0 1116.31 3 5 5 -17 28375.4 979.870 2 -5 -5 17 28002.8 1236.73 1 5 -5 -17 29961.4 1183.78 1 -5 -5 16 36147.7 1189.70 3 -5 -5 16 32904.1 1340.05 1 5 5 -16 34147.1 1063.47 2 5 -5 -16 34910.2 1251.26 1 -5 -5 15 32412.8 1091.65 3 -5 -5 15 31621.3 1296.89 1 5 5 -15 31578.8 1025.94 2 5 -5 -15 33642.6 1195.76 1 -5 -5 14 1086.08 324.323 3 -5 -5 14 43.5730 172.836 1 5 -5 -14 833.276 258.177 1 5 5 -14 233.747 122.024 2 -5 -5 13 53858.6 1312.88 3 -5 -5 13 54395.2 1644.93 1 5 5 -13 53797.1 1350.23 2 5 -5 -13 54973.1 1455.93 1 -5 -5 12 9746.65 586.696 2 -5 -5 12 10119.7 568.372 3 -5 -5 12 9875.79 714.951 1 5 5 -12 9582.48 576.567 2 5 -5 -12 9925.59 618.577 1 -5 -5 11 7202.10 457.151 3 -5 -5 11 7509.00 616.673 1 -5 -5 11 7660.83 527.125 2 5 5 -11 7433.18 507.732 2 5 -5 -11 7735.87 529.660 1 5 -5 -10 772.594 212.965 1 -5 -5 10 836.072 191.012 3 -5 -5 10 684.471 246.566 1 -5 -5 10 462.114 167.636 2 5 5 -10 612.596 178.853 2 5 -5 -9 29129.5 943.454 1 -5 -5 9 29034.6 827.633 3 -5 -5 9 29578.3 1185.23 1 -5 -5 9 29445.3 1006.28 2 5 5 -9 29820.1 1033.45 2 5 -5 -8 3874.62 353.233 1 -5 -5 8 4010.99 315.741 3 -5 -5 8 3562.17 441.927 1 -5 -5 8 3588.02 375.321 2 5 5 -8 3962.02 391.806 2 5 -5 -7 19382.7 720.003 1 -5 -5 7 20822.6 643.870 3 -5 -5 7 20540.9 981.716 1 -5 -5 7 20252.7 853.344 2 5 5 -7 20269.3 856.394 2 5 -5 -6 1318.35 198.993 1 -5 -5 6 1988.36 215.437 3 -5 -5 6 1579.71 299.811 1 -5 -5 6 1309.70 244.138 2 5 5 -6 1377.48 258.412 2 5 -5 -5 5135.64 344.159 1 -5 -5 5 5806.16 475.331 2 5 5 -5 4887.82 451.457 2 -5 -5 5 5367.29 287.539 3 5 -5 -4 5395.61 332.255 1 -5 -5 4 5245.75 460.224 2 5 5 -4 5543.10 473.466 2 -5 -5 4 5154.56 262.992 3 5 -5 -3 269.683 95.4750 1 -5 -5 3 255.262 158.637 2 5 5 -3 305.783 153.091 2 -5 -5 3 400.237 89.0559 3 5 -5 -2 7472.25 347.174 1 5 5 -2 7126.60 553.713 2 -5 -5 2 7661.23 568.400 2 5 -5 -1 84955.4 1074.44 1 5 5 -1 89047.9 1887.54 2 -5 -5 1 84210.0 1827.98 2 5 -5 0 20725.2 493.638 1 5 5 0 22921.3 967.415 2 -5 -5 0 21233.7 932.152 2 5 -5 1 36932.9 589.519 1 5 5 1 40859.6 1317.22 2 -5 -5 -1 38815.7 1267.89 2 5 5 2 30324.6 1143.08 2 -5 -5 -2 29404.6 1106.57 2 -5 -5 -3 1532.33 291.181 2 5 5 3 2082.24 313.195 2 5 5 4 22724.2 1008.15 2 -5 -5 -4 20845.7 966.132 2 -5 -5 -5 1572.51 302.917 2 5 5 5 1916.42 328.737 2 5 -5 6 4504.37 369.638 2 -5 -5 -6 4169.76 473.427 2 5 5 6 4504.10 472.418 2 5 -5 7 14311.8 639.385 2 5 5 7 14671.4 846.688 2 -5 -5 -7 14669.1 841.079 2 5 -5 8 18156.2 709.703 2 -5 -5 -8 16858.8 919.490 2 5 -5 9 44946.1 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2050.65 330.848 2 -7 -5 9 1984.38 365.485 1 7 -5 -8 6714.43 463.191 1 -7 -5 8 6200.33 565.288 2 7 5 -8 7240.89 607.289 2 -7 -5 8 6115.51 605.401 1 7 -5 -7 3113.20 304.351 1 -7 -5 7 3208.51 411.760 2 7 5 -7 3368.50 413.055 2 -7 -5 7 3256.55 456.583 1 -7 -5 6 1300.68 289.205 2 -7 -5 6 1173.22 303.082 1 7 -5 -6 1482.18 201.733 1 -7 -5 5 25006.4 1120.20 2 7 -5 -5 23913.2 764.323 1 -7 -5 5 25443.2 1166.81 1 -7 -5 4 3476.04 437.438 2 7 -5 -4 3569.58 284.535 1 7 -5 -3 37356.0 860.131 1 -7 -5 3 36406.7 1351.79 2 7 -5 -2 1426.80 172.546 1 -7 -5 2 1040.02 302.848 2 7 -5 -1 111605. 1293.58 1 -7 -5 1 113064. 2397.93 2 7 -5 0 806.593 116.319 1 -7 -5 0 633.165 247.665 2 -7 -5 -1 5816.95 593.115 2 -7 -5 -2 58.6756 212.176 2 7 -5 3 327.741 190.053 2 -7 -5 -3 170.566 188.028 2 -7 -5 -4 115.357 192.490 2 7 -5 4 108.729 139.598 2 -7 -5 -5 4892.25 546.289 2 7 -5 5 5032.62 465.593 2 7 -5 6 3507.29 384.978 2 -7 -5 -6 3686.97 521.931 2 7 -5 7 79985.1 1798.99 2 -7 -5 -7 76732.0 2102.50 2 7 -5 8 5703.13 490.689 2 -7 -5 -8 6192.17 622.531 2 7 -5 9 6318.19 513.496 2 -7 -5 -9 6198.53 640.273 2 -7 -5 -10 6923.81 661.495 2 7 -5 11 9766.58 628.316 2 -7 -5 -11 9123.36 778.496 2 7 -5 12 315.826 159.224 2 -7 -5 -12-186.379 229.747 2 -7 -5 -13 14443.4 978.717 2 7 -5 13 13933.3 735.415 2 7 5 13 14338.2 473.565 3 7 -5 14 4486.60 424.575 2 -7 -5 -14 4190.95 568.916 2 7 5 14 4424.83 287.485 3 7 -5 15 4548.04 426.265 2 -7 -5 -15 4686.90 587.743 2 7 5 15 4775.14 317.438 3 7 -5 16 54.1248 101.673 2 -7 -5 -16-75.3779 208.096 2 7 5 16 148.340 121.001 3 -7 -5 -17 17914.5 1158.35 2 7 5 17 20024.3 703.820 3 -7 -5 -18 1139.50 356.655 2 7 5 18 1941.06 256.693 3 -7 -5 -19 2480.49 470.103 2 7 5 19 2542.38 293.096 3 -7 -5 -20 39.0276 294.758 2 7 -5 20-39.4256 101.842 2 7 5 20 334.784 178.443 3 7 -5 21 15543.1 776.368 2 -7 -5 -21 15724.1 1107.81 2 7 5 21 16300.9 748.335 3 -7 -5 -22 1679.37 524.760 2 7 -5 22 1467.07 255.338 2 -7 -5 -23 45409.7 1903.01 2 7 5 23 43142.3 1299.12 3 -7 -5 -24 1203.41 479.941 2 7 5 24 1255.92 305.433 3 -7 -5 -25 13037.2 1052.65 2 7 5 25 13194.2 767.489 3 -7 -5 -26 62.4780 308.073 2 7 5 26 100.685 168.221 3 -7 -5 -27 111.155 233.831 2 7 5 27-142.295 181.336 3 -7 -5 -28 88.1395 233.491 2 7 5 28 233.890 170.167 3 -7 -5 -29 1704.30 434.973 2 -7 -5 -30 931.066 390.261 2 7 5 30 1653.10 342.981 3 -7 -5 -31 8006.58 883.607 2 -7 -5 -32 2179.16 548.926 2 -7 -5 -33 14346.8 1206.71 2 -7 -5 -34 99.4194 238.314 2 -7 -5 -35 1233.55 446.644 2 -7 -5 -36-332.997 283.572 2 -7 -5 -37 5092.21 747.923 2 -7 -5 -38 369.249 340.939 2 -7 -5 -39 1608.31 447.418 2 -7 -5 -40 211.891 324.225 2 -7 -5 -41 5071.94 797.369 2 -7 -6 44 3246.79 690.816 1 -7 -6 44 3073.39 642.386 3 -7 -6 43 1559.23 516.291 1 -7 -6 42 1017.83 469.579 1 -7 -6 41 3444.21 695.325 1 -7 -6 41 2767.54 561.782 3 -7 -6 40 1436.18 447.928 1 -7 -6 40 2476.44 595.290 3 -7 -6 39 7318.88 897.921 1 -7 -6 39 6878.45 869.923 3 -7 -6 38 1000.14 435.631 1 -7 -6 37 2708.04 573.880 1 -7 -6 37 2735.04 542.279 3 -7 -6 36 57.5938 250.141 1 -7 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762.837 1 -7 -7 28 6639.42 715.779 3 -7 -7 27 2686.83 520.331 1 -7 -7 27 2542.07 469.001 3 -7 -7 26 1085.39 363.894 1 -7 -7 26 1450.57 363.125 3 -7 -7 25 4891.39 586.565 3 -7 -7 25 4092.13 608.198 1 7 7 -25 3677.21 430.160 2 -7 -7 24 20254.6 1113.57 3 7 7 -24 17987.8 928.648 2 -7 -7 24 19692.1 1271.71 1 -7 -7 23 598.641 285.584 1 7 7 -23 686.408 219.730 2 -7 -7 22 17566.1 1182.62 1 -7 -7 22 18693.9 1020.65 3 -7 -7 21 2729.59 478.939 1 7 7 -21 2899.72 376.216 2 -7 -7 20 6396.16 587.680 3 -7 -7 20 7639.75 798.771 1 7 7 -20 7382.73 602.738 2 -7 -7 19 9418.92 686.423 3 -7 -7 19 9506.07 857.752 1 7 7 -19 8667.56 654.625 2 -7 -7 18 16893.3 888.943 3 -7 -7 18 18520.7 1179.04 1 7 7 -18 17139.9 921.858 2 -7 -7 17 2882.16 382.726 3 -7 -7 17 2993.55 503.709 1 7 7 -17 3220.30 415.608 2 -7 -7 16 11136.9 689.633 3 -7 -7 16 11456.0 919.436 1 7 7 -16 11876.4 776.016 2 -7 -7 15 6616.59 523.108 3 -7 -7 15 6518.25 698.962 1 -7 -7 14 26687.8 1159.08 2 -7 -7 14 25383.5 968.406 3 -7 -7 14 26218.7 1354.87 1 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581.320 3 -7 -9 22 4165.07 645.780 1 -7 -9 21 9343.48 735.787 3 -7 -9 21 9142.12 923.486 1 -7 -9 20 105.568 211.150 3 -7 -9 20 151.492 226.985 1 -7 -9 19 25146.8 1127.67 3 -7 -9 19 24745.9 1454.80 1 -7 -9 18 515.906 243.764 3 -7 -9 18 406.002 256.776 1 -7 -9 17 3096.43 397.666 3 -7 -9 17 3992.98 613.547 1 -7 -9 16 54.6034 148.973 2 -7 -9 16 111.498 153.130 3 -7 -9 16-102.063 238.027 1 -7 -9 15 734.386 258.032 2 -7 -9 15 904.836 227.710 3 -7 -9 15 499.858 280.640 1 -7 -9 14 1004.42 268.513 2 -7 -9 14 1196.87 259.799 3 -7 -9 14 881.445 349.620 1 -7 -9 13 150.311 179.684 2 -7 -9 13 328.563 166.608 3 -7 -9 13-115.731 217.473 1 -7 -9 12 853.732 248.859 2 -7 -9 12 1207.71 243.798 3 -7 -9 12 1229.29 390.466 1 -7 -9 11 22253.7 837.801 3 -7 -9 11 21589.7 1295.85 1 -7 -9 11 21681.1 1112.11 2 7 -9 -11 20697.4 972.824 1 -7 -9 10 594.843 179.400 3 -7 -9 10 724.103 338.238 1 -7 -9 10 346.544 211.484 2 7 -9 -10 373.296 199.389 1 -7 -9 9 21684.1 753.672 3 -7 -9 9 23127.4 1167.36 2 7 -9 -9 22436.2 958.332 1 -7 -9 9 23713.5 1372.56 1 -7 -9 8 1831.61 367.062 2 7 -9 -8 1573.41 281.232 1 -7 -9 8 2150.34 456.663 1 -7 -9 7 2199.55 394.795 2 7 -9 -7 2202.20 297.572 1 -7 -9 7 2109.82 458.946 1 7 -9 -6 4874.68 411.261 1 -7 -9 6 5033.22 566.753 2 7 -9 -5 415.949 147.417 1 -7 -9 5 393.358 231.850 2 -7 -9 4 4704.30 561.247 2 7 -9 -3 1014.50 184.518 1 -7 -9 3 742.094 277.548 2 -7 -9 2 2910.29 480.743 2 7 -9 -1 1762.47 205.912 1 -7 -9 1 2157.00 437.551 2 -7 -9 0 3918.51 538.979 2 -7 -9 -1 26744.3 1340.06 2 -7 -9 -2 14784.8 1014.43 2 -7 -9 -3 6716.24 700.233 2 -7 -9 -4 17471.4 1115.65 2 -7 -9 -5 5888.71 672.212 2 -7 -9 -6 681.509 321.427 2 -7 -9 -7 41633.0 1770.58 2 7 -9 8 9976.17 676.450 2 -7 -9 -8 9966.05 901.474 2 -7 -9 -9 114.043 224.929 2 7 -9 10 164.092 105.519 2 -7 -9 -10 52.6470 211.693 2 -7 -9 -11 959.862 351.434 2 -7 -9 -12 14774.5 1113.78 2 -7 -9 -13 3727.67 601.859 2 -7 -9 -14 523.328 338.166 2 -7 -9 -15 4588.20 663.859 2 -7 -9 -16 459.118 299.949 2 -7 -9 -17 2551.52 522.785 2 -7 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282.597 1 -7 -10 27 821.492 298.906 3 -7 -10 26-36.2619 272.724 1 -7 -10 26 138.893 199.419 3 -7 -10 25 5297.32 746.743 1 -7 -10 24 390.184 287.713 1 -7 -10 24 920.649 330.565 3 -7 -10 23 24992.1 1541.85 1 -7 -10 22 146.916 267.055 1 -7 -10 22 699.924 310.312 3 -7 -10 21 2258.91 458.251 1 -7 -10 21 3661.27 486.224 3 -7 -10 20 682.042 338.678 1 -7 -10 20 994.888 304.102 3 -7 -10 19 3296.25 588.616 1 -7 -10 19 3062.88 414.333 3 -7 -10 18-28.4147 255.532 1 -7 -10 18 393.447 198.839 3 -7 -10 17 795.885 330.501 1 -7 -10 17 1855.67 318.704 3 -7 -10 16-72.0180 178.387 2 -7 -10 16-338.360 327.762 1 -7 -10 15 1079.35 288.722 2 -7 -10 15 1651.50 447.780 1 -7 -10 14-44.9887 163.866 2 -7 -10 14 42.0645 249.134 1 -7 -10 14 98.3901 137.387 3 -7 -10 13 11974.8 838.467 2 -7 -10 13 12630.2 1054.24 1 -7 -10 12 305.985 217.407 2 -7 -10 12 258.823 206.624 1 -7 -10 11 691.104 262.743 2 -7 -10 11 356.549 224.209 1 -7 -10 11 839.033 185.936 3 -7 -10 10 961.903 358.134 1 -7 -10 10 924.832 197.568 3 -7 -10 10 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852.441 2 -10 -8 -6 28.6489 245.360 2 -10 -8 -7 11199.7 1031.44 2 -10 -8 -8 815.726 371.547 2 -10 -8 -9 126.964 275.368 2 -10 -8 -10 46.1151 225.717 2 -10 -8 -11 1382.81 441.933 2 -10 -8 -12 10565.5 1035.70 2 -10 -8 -13 10211.8 1036.02 2 -10 -8 -14 3382.92 633.259 2 -10 -8 -15 20067.8 1445.71 2 -10 -8 -16 3561.26 645.678 2 -10 -8 -17 1017.72 412.399 2 -10 -8 -18 1119.64 436.601 2 -10 -8 -19 349.183 320.110 2 -10 -8 -20 559.975 306.002 2 -10 -8 -21-98.9714 292.848 2 -10 -8 -22 669.670 415.004 2 -10 -8 -23 13748.6 1253.41 2 -10 -8 -24 468.399 352.879 2 -10 -8 -25 2130.20 540.625 2 -10 -8 -26 405.311 399.380 2 -10 -9 40 51.0419 222.017 3 -10 -9 39 1494.44 436.943 3 -10 -9 34 5381.09 742.491 3 -10 -9 33 1399.52 419.826 3 -10 -9 33 901.007 418.887 1 -10 -9 32 2163.07 601.666 1 -10 -9 31 1621.58 403.056 3 -10 -9 31 1796.08 542.671 1 -10 -9 30 7333.59 798.460 3 -10 -9 30 7796.07 980.907 1 -10 -9 29 354.194 272.465 3 -10 -9 29 229.322 293.184 1 -10 -9 28 2135.01 431.902 3 -10 -9 28 1306.19 410.766 1 -10 -9 27 300.899 240.750 3 -10 -9 27 557.892 392.505 1 -10 -9 26 1236.74 481.522 1 -10 -9 25 2424.04 420.103 3 -10 -9 25 2755.53 585.771 1 -10 -9 24 1463.61 339.754 3 -10 -9 24 2418.96 560.459 1 -10 -9 23 641.993 349.859 1 -10 -9 22 395.821 220.678 3 -10 -9 22-101.524 319.539 1 -10 -9 21-266.422 274.455 1 -10 -9 20 5043.84 735.294 1 -10 -9 19 906.835 361.981 1 -10 -9 18 3041.20 624.251 1 -10 -9 17 3772.02 638.607 1 -10 -9 16 5139.42 752.548 1 -10 -9 15-352.740 381.013 1 -10 -9 14 2915.43 573.775 1 -10 -9 13 1633.74 417.809 2 -10 -9 13 1794.84 461.680 1 -10 -9 12 1214.87 342.724 2 -10 -9 12 1532.68 440.813 1 -10 -9 11 78.0415 209.491 2 -10 -9 11-13.9163 295.501 1 -10 -9 10 12596.5 1012.84 2 -10 -9 10 11969.5 1076.83 1 -10 -9 9-4.55100 220.736 2 -10 -9 9 60.0630 260.423 1 -10 -9 8 2203.23 448.904 2 -10 -9 8 2342.85 506.441 1 -10 -9 7 6669.75 732.416 2 -10 -9 7 7107.58 855.874 1 -10 -9 6 543.219 347.780 2 -10 -9 6-282.746 331.776 1 -10 -9 5 7671.86 820.915 2 -10 -9 5 7622.36 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552.368 412.078 2 -13 -2 -27 6.79939 252.941 2 -13 -2 -28 853.382 421.469 2 -13 3 37 129.619 356.405 1 -13 3 36 402.507 345.665 1 -13 -3 35 551.462 330.486 1 -13 3 35 347.435 279.833 1 -13 -3 34 682.383 331.170 1 -13 3 34 1272.04 473.131 1 -13 -3 33 234.301 299.289 1 -13 3 33-78.8479 231.704 1 -13 -3 32 3345.23 658.292 1 -13 3 32 4520.65 733.736 1 -13 -3 31 1568.05 494.152 1 -13 3 31 419.552 230.237 1 -13 -3 30 3067.42 640.142 1 -13 3 30 3103.45 603.672 1 -13 -3 29 1594.51 496.944 1 -13 3 29 1861.53 447.653 1 -13 -3 28 0.84257 244.685 1 -13 3 28-54.1333 254.893 1 -13 -3 27 629.781 353.066 1 -13 3 27 914.543 342.188 1 -13 -3 26 643.945 312.926 1 -13 3 26 1377.54 403.546 1 -13 -3 25-112.159 244.574 1 -13 3 25 397.376 300.762 1 -13 -3 24 4489.66 707.357 1 -13 3 24 4409.98 675.181 1 -13 3 23 1972.66 474.126 1 -13 -3 23 2013.24 519.360 1 -13 -3 22 6021.71 802.744 1 -13 3 22 7139.78 790.198 1 -13 -3 21 3713.59 640.494 1 -13 3 21 4303.35 621.764 1 -13 -3 20 5037.33 710.234 1 -13 3 20 5496.28 691.476 1 -13 -3 19 289.728 240.913 1 -13 3 19 457.872 274.902 1 -13 -3 18 1556.50 437.137 1 -13 3 18 1496.13 350.534 1 -13 -3 17 14.8142 240.555 1 -13 3 17-242.120 237.687 1 -13 -3 16 690.964 265.946 1 -13 3 16 1251.81 358.966 1 -13 -3 15 608.910 316.196 1 -13 3 15 962.138 301.269 1 -13 -3 14 5488.04 712.274 1 -13 3 14 5741.19 636.184 1 -13 -3 13 764.586 364.353 1 -13 3 13 930.407 312.328 1 -13 -3 12 8975.74 877.957 1 -13 3 12 9490.56 781.293 1 -13 -3 11 5853.54 703.387 1 -13 3 11 6130.78 639.252 1 -13 -3 10 7104.00 771.933 1 -13 3 10 6546.86 646.417 1 -13 -3 9 2373.06 460.501 1 -13 3 9 2516.52 415.439 1 -13 -3 8 18197.8 1209.10 1 -13 3 8 18990.8 1030.40 1 -13 -3 7 1724.31 424.006 1 -13 3 7 1550.04 322.908 1 -13 -3 6 5125.40 655.667 1 -13 3 6 4984.28 524.753 1 -13 -3 5-336.865 325.646 1 -13 3 5 113.647 143.123 1 -13 -3 4 57.0308 197.814 1 -13 3 4 122.861 131.946 1 -13 -3 3-29.9545 197.133 1 -13 3 3 72.5226 134.570 1 -13 -3 2 738.781 286.182 1 -13 3 2 897.733 244.203 1 -13 -3 1 1719.43 416.973 1 -13 3 1 2369.68 356.342 1 -13 -3 0 8337.10 799.319 1 -13 3 0 7956.18 585.990 1 -13 -3 -1 1673.70 394.935 1 -13 3 -1 2299.01 325.243 1 -13 -3 -2 7906.78 777.986 1 -13 -3 -2 7520.03 864.099 2 -13 -3 -3 683.116 307.512 2 -13 -3 -3 935.059 334.189 1 -13 -3 -4 6029.64 781.409 2 -13 -3 -4 6262.38 703.237 1 -13 -3 -5 156.759 286.413 2 -13 -3 -5 397.308 297.931 1 -13 -3 -6 721.984 353.090 2 -13 -3 -6 1424.16 388.929 1 -13 -3 -7 1508.05 432.970 2 -13 -3 -7 2273.41 460.230 1 -13 -3 -8 384.916 305.043 2 -13 -3 -8 8.27314 197.848 1 -13 -3 -9 1032.14 401.874 2 -13 -3 -10 7641.70 901.619 2 -13 -3 -11-31.3977 291.983 2 -13 -3 -12 20948.4 1467.00 2 -13 -3 -13 509.958 373.676 2 -13 -3 -14 354.267 343.198 2 -13 -3 -15 6395.11 852.940 2 -13 -3 -16 1675.39 492.394 2 -13 -3 -17 294.252 346.192 2 -13 -3 -18 11643.9 1148.19 2 -13 -3 -19 1287.34 525.038 2 -13 -3 -20 5523.84 824.597 2 -13 -3 -21 481.418 329.057 2 -13 -3 -22-117.091 276.024 2 -13 -3 -23 2652.50 606.674 2 -13 -3 -24 4069.13 743.025 2 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529.596 1 -13 -5 12 1001.23 295.078 1 -13 5 12 1765.05 370.279 1 -13 -5 11 5034.05 715.554 1 -13 5 11 6351.38 601.622 1 -13 -5 10 1284.56 411.105 1 -13 5 10 1661.35 342.560 1 -13 -5 9 11790.1 1052.24 1 -13 5 9 13286.0 813.645 1 -13 -5 8 591.618 363.978 1 -13 5 8 382.641 222.391 1 -13 -5 7 4462.97 661.763 1 -13 5 7 4528.98 455.402 1 -13 -5 6 2455.47 506.901 1 -13 -5 5 5664.00 751.875 1 -13 -5 4 1209.97 360.468 1 -13 -5 3 7605.95 845.026 1 -13 -5 3 5371.58 756.280 2 -13 -5 2 1055.23 347.095 1 -13 -5 2 1345.25 413.291 2 -13 -5 1 9605.77 931.018 1 -13 -5 1 10354.7 1017.99 2 -13 -5 0 4082.90 616.449 1 -13 -5 0 3309.30 589.352 2 -13 -5 -1 7214.00 823.820 1 -13 -5 -1 6183.39 815.011 2 -13 -5 -2 211.056 299.299 1 -13 -5 -2-159.407 282.146 2 -13 -5 -3 1620.56 449.865 1 -13 -5 -3 1020.46 368.984 2 -13 -5 -4 1115.81 364.923 1 -13 -5 -4 1433.60 449.109 2 -13 -5 -5 11327.8 1003.28 1 -13 -5 -5 11580.1 1107.08 2 -13 -5 -6 1170.53 387.544 1 -13 -5 -6 864.661 419.071 2 -13 -5 -7 5673.86 784.971 2 -13 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254.910 1 -16 -5 6 58.7525 247.844 1 -16 -5 5 217.111 240.787 1 -16 -5 4 4352.49 703.455 1 -16 -5 3 737.248 330.892 1 -16 -5 2 296.863 313.967 1 -16 -5 1 529.305 362.091 1 -16 -5 0 4328.97 703.534 1 -16 -5 -1 284.069 291.724 1 -16 -5 -2 337.138 240.935 1 -16 -5 -3 94.2732 215.825 1 -16 -5 -4 753.174 324.908 1 -16 -5 -5-214.379 262.058 1 -16 -5 -6 4804.11 739.101 1 -16 -5 -7 646.401 341.092 1 -16 -5 -8 1307.87 412.466 1 -16 -5 -9 409.744 307.983 1 -16 -5 -10 138.284 304.807 1 -16 -5 -11 32.8713 276.361 1 -16 -6 16 527.489 371.386 1 -16 -6 15 995.751 461.204 1 -16 -6 14 1092.25 473.129 1 -16 -6 13 2242.20 581.846 1 -16 -6 12 6613.79 899.828 1 -16 -6 11 2795.13 619.608 1 -16 -6 10-542.478 364.148 1 -16 -6 9 1153.77 447.370 1 -16 -6 8 11290.3 1167.76 1 -16 -6 7 417.051 341.539 1 -16 -6 6 1344.41 434.360 1 -16 -6 5 139.220 253.701 1 -16 -6 4-136.119 304.740 1 -16 -6 3 2020.09 533.344 1 -16 -6 2 343.454 319.127 1 -16 -6 1 146.762 283.585 1 -16 -6 0 2509.05 572.980 1 -16 -6 -1 40.2843 234.253 1 -16 -6 -2 1621.33 480.694 1 -16 -6 -3 768.531 359.149 1 -16 -6 -4 974.532 395.107 1 -16 -6 -5 637.536 315.585 1 -16 -6 -6-69.3791 271.295 1 -16 -6 -7 1368.57 464.502 1 -16 -6 -8 3154.19 656.992 1 -16 -6 -9 432.947 360.920 1 -16 -6 -10 3578.11 660.510 1 -16 -6 -11 478.492 359.960 1 -16 -6 -12 1564.72 462.252 1 -16 -6 -13 2142.74 523.310 1 -16 -6 -14 4126.92 721.485 1 -16 -7 8 550.769 403.969 1 -16 -7 7 1623.69 501.015 1 -16 -7 6 860.591 395.517 1 -16 -7 5 707.043 362.280 1 -16 -7 4-17.3082 280.688 1 -16 -7 3 2168.94 547.445 1 -16 -7 2 654.732 386.017 1 -16 -7 1 2040.75 523.017 1 -16 -7 0 361.761 301.459 1 -16 -7 -1 2321.16 576.081 1 -16 -7 -2 429.691 299.503 1 -16 -7 -3 2909.86 648.590 1 -16 -7 -4 1910.44 535.728 1 -17 0 26-172.631 246.446 1 -17 0 25 161.311 240.019 1 -17 0 24-578.825 325.781 1 -17 0 23 7125.78 930.323 1 -17 0 22-310.916 326.867 1 -17 0 21 54.1685 245.957 1 -17 0 20 301.017 295.182 1 -17 0 19 2815.11 618.482 1 -17 0 18-506.794 319.417 1 -17 0 17 547.970 328.636 1 -17 0 16 277.852 309.304 1 -17 0 15 2923.97 585.506 1 -17 0 14 580.042 297.389 1 -17 0 13 12065.0 1096.98 1 -17 0 12 308.623 303.176 1 -17 0 11 1964.19 468.504 1 -17 1 27 89.8960 257.916 1 -17 1 26 797.448 411.233 1 -17 -1 25 1179.25 457.484 1 -17 1 25 2031.58 547.374 1 -17 1 24 1013.37 419.104 1 -17 -1 24 60.2960 260.249 1 -17 1 23-224.407 299.844 1 -17 -1 23-17.7865 279.215 1 -17 1 22 1115.58 420.538 1 -17 -1 22 902.257 399.465 1 -17 1 21 2192.57 525.019 1 -17 -1 21 2094.06 531.850 1 -17 1 20 232.119 258.396 1 -17 -1 20-238.441 271.288 1 -17 1 19 779.587 338.519 1 -17 -1 19 378.163 292.362 1 -17 -1 18 216.432 297.103 1 -17 1 18 126.119 218.542 1 -17 -1 17 4002.22 744.419 1 -17 1 17 4673.22 702.946 1 -17 -1 16 140.911 285.956 1 -17 1 16 416.211 309.543 1 -17 -1 15 1615.83 491.753 1 -17 -1 14 2369.05 545.172 1 -17 -1 13 185.139 251.443 1 -17 -1 12 426.490 309.393 1 -17 -1 11 573.894 348.496 1 -17 -1 10-222.786 230.689 1 -17 -1 9 1888.60 478.261 1 -17 -1 8 5656.23 759.471 1 -17 -1 7 6290.79 790.669 1 -17 2 28 401.762 324.779 1 -17 2 27-91.5385 300.265 1 -17 2 26 244.567 281.022 1 -17 2 25 2505.67 553.925 1 -17 2 24 2149.23 552.455 1 -17 2 23 151.544 278.889 1 -17 -2 23-75.3609 264.561 1 -17 -2 22 646.312 323.704 1 -17 2 22 757.399 370.098 1 -17 -2 21 311.989 244.617 1 -17 2 21 519.786 311.699 1 -17 -2 20 15.9963 275.968 1 -17 -2 19 986.316 435.968 1 -17 -2 18 2458.38 560.845 1 -17 -2 17 66.7955 292.447 1 -17 -2 16 1557.99 473.911 1 -17 -2 15 134.524 228.324 1 -17 -2 14 1853.75 501.648 1 -17 -2 13-195.518 266.134 1 -17 -2 12-83.5041 220.254 1 -17 -2 11 2324.25 519.970 1 -17 -2 10 1319.40 501.851 1 -17 -2 9 330.454 252.507 1 -17 -2 8 10067.6 1015.48 1 -17 -2 7 879.695 384.205 1 -17 -2 6 448.648 230.645 1 -17 -2 5 254.668 287.609 1 -17 -2 4 254.983 198.759 1 -17 -2 3 1743.23 456.894 1 -17 3 28 2704.18 611.991 1 -17 3 27 1389.17 447.822 1 -17 -3 20 1046.62 434.629 1 -17 -3 19 989.757 400.484 1 -17 -3 18 1298.13 494.235 1 -17 -3 17-77.2751 245.632 1 -17 -3 16 40.9356 306.445 1 -17 -3 15-188.616 258.697 1 -17 -3 14 1317.79 472.029 1 -17 -3 13 205.186 310.508 1 -17 -3 12 3324.87 638.616 1 -17 -3 11-30.1439 241.477 1 -17 -3 10 3677.79 665.079 1 -17 -3 9 329.834 305.210 1 -17 -3 8 45.9790 256.505 1 -17 -3 7 1574.47 469.008 1 -17 -3 6 2316.58 524.830 1 -17 -3 5 2196.38 543.948 1 -17 -3 4 5971.38 804.222 1 -17 -3 3 580.974 321.418 1 -17 -3 2 701.694 317.809 1 -17 -3 1 785.455 360.390 1 -17 -3 0 582.564 352.445 1 -17 -4 17 589.634 399.789 1 -17 -4 16 5017.75 806.093 1 -17 -4 15-82.3816 249.279 1 -17 -4 14 519.778 287.483 1 -17 -4 13 2762.19 637.339 1 -17 -4 12 481.146 303.471 1 -17 -4 11 1617.63 499.086 1 -17 -4 10 3586.83 687.273 1 -17 -4 9 732.333 419.422 1 -17 -4 8 87.1286 244.587 1 -17 -4 7 365.809 315.329 1 -17 -4 6 2064.90 538.513 1 -17 -4 5 2163.09 527.763 1 -17 -4 4-367.237 332.537 1 -17 -4 3 2515.43 568.101 1 -17 -4 2 391.759 278.779 1 -17 -4 1 1711.16 477.847 1 -17 -4 0 2051.09 493.791 1 -17 -4 -1 747.419 345.999 1 -17 -4 -2 248.015 268.483 1 -17 -4 -3 873.668 362.700 1 -17 -5 13 1031.38 378.400 1 -17 -5 12 127.531 370.316 1 -17 -5 11 2401.69 598.302 1 -17 -5 10 1925.13 542.675 1 -17 -5 9 1387.85 485.933 1 -17 -5 8 766.408 388.751 1 -17 -5 7 1261.25 475.894 1 -17 -5 6-166.753 258.518 1 -17 -5 5 467.721 264.303 1 -17 -5 4-121.408 275.580 1 -17 -5 3 712.023 387.491 1 -17 -5 2 199.539 283.973 1 -17 -5 1 2543.17 580.245 1 -17 -5 0 193.296 250.277 1 -17 -5 -1 4679.34 744.119 1 -17 -5 -2 321.122 332.131 1 -17 -5 -3 904.141 363.023 1 -17 -5 -4 48.7218 232.678 1 -17 -5 -5 1964.09 489.601 1 -17 -5 -6 217.796 326.083 1 -18 0 22 600.220 316.644 1 -18 0 21-54.8833 264.601 1 -18 0 20 3168.56 652.839 1 -18 -1 20 1793.88 511.643 1 -18 -1 19 147.704 249.298 1 -18 -1 18 174.636 298.423 1 -18 -1 17 493.612 313.531 1 -18 -1 16 1432.70 481.686 1 -18 -1 15 2479.60 598.582 1 -18 -2 18-91.1005 248.452 1 -18 -2 17 63.1104 235.685 1 -18 -2 16 323.063 290.604 1 -18 -2 15 4950.63 788.721 1 -18 -2 14-148.295 232.008 1 -18 -2 13 3183.80 647.026 1 -18 -2 12-407.280 332.578 1 -18 -2 11-93.9962 264.713 1 -18 -3 14 1215.50 460.383 1 -18 -3 13-92.0265 243.604 1 -18 -3 12 536.085 318.275 1 -18 -3 11 2212.59 533.435 1 -18 -3 10-288.046 303.294 1 -18 -3 9 2033.90 530.288 1 -18 -3 8 360.406 315.831 1 -18 -3 7-77.9408 224.024 1 -18 -4 9-198.305 308.981 1 -18 -4 8 2440.00 570.057 1 -18 -4 7 427.678 346.480 1 -18 -4 6 43.5839 255.494 1 -18 -4 5 1749.50 522.689 1 -18 -4 4 422.316 336.413 1 0 0 0 0.00 0.00 0 TITL MRC2137 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.71073 14.017641 13.907675 40.269119 90.0000 99.7488 90.0000 ZERR 4.00 0.000421 0.000454 0.001033 0.0000 0.0028 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Mg Rh UNIT 316.00 480.00 16.00 8.00 8.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 10177 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_4a _database_code_depnum_ccdc_archive 'CCDC 2116010' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; _audit_creation_method SHELXL-2018/3 _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C92 H126 Cr Mg3 N6 O5, 2(C6 H14)' _chemical_formula_sum 'C104 H154 Cr Mg3 N6 O5' _chemical_formula_weight 1693.25 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr -0.1635 2.4439 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.1719 0.1771 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 19.4330(2) _cell_length_b 17.40489(18) _cell_length_c 30.8931(4) _cell_angle_alpha 90 _cell_angle_beta 96.4115(12) _cell_angle_gamma 90 _cell_volume 10383.6(2) _cell_formula_units_Z 4 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 7336 _cell_measurement_theta_min 3.5850 _cell_measurement_theta_max 73.1110 _exptl_crystal_description 'blocky needles' _exptl_crystal_colour Orange _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.083 _exptl_crystal_F_000 3680 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.282 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.080 _exptl_absorpt_coefficient_mu 1.469 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type analytical _exptl_absorpt_correction_T_min 0.774 _exptl_absorpt_correction_T_max 0.907 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'Enhance Ultra (Cu) X-ray Source' _diffrn_measurement_device_type 'Agilent Xcalibur PX Ultra A' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean 10.4115 _diffrn_reflns_number 34761 _diffrn_reflns_av_unetI/netI 0.0705 _diffrn_reflns_av_R_equivalents 0.0445 _diffrn_reflns_limit_h_min -24 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -38 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_theta_min 3.472 _diffrn_reflns_theta_max 73.465 _diffrn_reflns_theta_full 67.684 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measured_fraction_theta_full 0.987 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_Laue_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_point_group_measured_fraction_full 0.987 _reflns_number_total 19933 _reflns_number_gt 13294 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro, Rigaku OD' _computing_cell_refinement 'CrysAlisPro, Rigaku OD' _computing_data_reduction 'CrysAlisPro, Rigaku OD' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2017)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2017)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0748P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 19933 _refine_ls_number_parameters 1148 _refine_ls_number_restraints 176 _refine_ls_R_factor_all 0.0915 _refine_ls_R_factor_gt 0.0570 _refine_ls_wR_factor_ref 0.1667 _refine_ls_wR_factor_gt 0.1418 _refine_ls_goodness_of_fit_ref 1.022 _refine_ls_restrained_S_all 1.026 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cr1 Cr 0.78459(2) 0.65196(2) 0.39805(2) 0.03964(11) Uani 1 1 d . . . . . Mg1 Mg 0.88763(4) 0.85615(4) 0.33229(3) 0.03564(18) Uani 1 1 d . . . . . Mg2 Mg 0.71029(4) 0.82365(4) 0.29089(3) 0.03424(18) Uani 1 1 d . . . . . Mg3 Mg 0.77955(4) 0.49717(5) 0.44479(3) 0.03883(19) Uani 1 1 d . . . . . H1 H 0.7988(12) 0.8560(13) 0.3040(8) 0.021(5) Uiso 1 1 d . . . . . N1 N 0.95825(10) 0.88041(11) 0.29038(7) 0.0378(4) Uani 1 1 d . . . . . C1 C 0.99611(14) 0.94448(15) 0.29454(10) 0.0456(6) Uani 1 1 d . . . . . C2 C 0.99651(15) 0.99597(16) 0.32953(10) 0.0505(7) Uani 1 1 d . . . . . H2A H 1.017424 1.044330 0.325300 0.061 Uiso 1 1 calc R U . . . C3 C 0.97063(16) 0.98666(15) 0.36984(10) 0.0484(7) Uani 1 1 d . . . . . N3 N 0.93062(12) 0.92909(12) 0.37920(8) 0.0434(5) Uani 1 1 d . . . . . C4 C 1.04327(19) 0.9647(2) 0.26073(13) 0.0675(9) Uani 1 1 d . . . . . H4A H 1.084814 0.932414 0.264809 0.101 Uiso 1 1 calc R U . . . H4B H 1.056634 1.018866 0.263772 0.101 Uiso 1 1 calc R U . . . H4C H 1.019033 0.955896 0.231594 0.101 Uiso 1 1 calc R U . . . C5 C 0.9936(2) 1.0466(2) 0.40443(12) 0.0705(10) Uani 1 1 d . . . . . H5A H 0.959431 1.049531 0.425432 0.106 Uiso 1 1 calc R U . . . H5B H 0.997415 1.096768 0.390531 0.106 Uiso 1 1 calc R U . . . H5C H 1.038691 1.031940 0.419579 0.106 Uiso 1 1 calc R U . . . C6 C 0.96540(13) 0.83023(14) 0.25409(9) 0.0398(6) Uani 1 1 d . . . . . C7 C 1.01029(14) 0.76660(16) 0.25996(12) 0.0509(7) Uani 1 1 d . . . . . C8 C 1.01592(16) 0.71880(17) 0.22410(13) 0.0595(9) Uani 1 1 d . . . . . H8A H 1.046537 0.676118 0.227306 0.071 Uiso 1 1 calc R U . . . C9 C 0.97860(17) 0.73179(18) 0.18455(12) 0.0581(8) Uani 1 1 d . . . . . H9A H 0.983790 0.698951 0.160570 0.070 Uiso 1 1 calc R U . . . C10 C 0.93339(17) 0.79299(17) 0.17988(11) 0.0536(7) Uani 1 1 d . . . . . H10A H 0.906825 0.801268 0.152551 0.064 Uiso 1 1 calc R U . . . C11 C 0.92565(14) 0.84297(15) 0.21414(9) 0.0441(6) Uani 1 1 d . . . . . C12 C 1.05115(18) 0.7490(2) 0.30340(14) 0.0691(10) Uani 1 1 d . . . . . H12A H 1.036547 0.786653 0.325070 0.083 Uiso 1 1 calc R U . . . C13 C 1.0358(3) 0.6690(3) 0.31946(18) 0.1054(17) Uani 1 1 d . . . . . H13A H 1.046670 0.630889 0.297863 0.158 Uiso 1 1 calc R U . . . H13B H 0.986714 0.665282 0.323707 0.158 Uiso 1 1 calc R U . . . H13C H 1.064223 0.659158 0.347153 0.158 Uiso 1 1 calc R U . . . C14 C 1.1279(3) 0.7592(5) 0.3017(3) 0.153(3) Uani 1 1 d . . . . . H14A H 1.143761 0.723258 0.280523 0.230 Uiso 1 1 calc R U . . . H14B H 1.152632 0.749012 0.330564 0.230 Uiso 1 1 calc R U . . . H14C H 1.137236 0.812001 0.292993 0.230 Uiso 1 1 calc R U . . . C15 C 0.87409(16) 0.90889(16) 0.20700(10) 0.0498(7) Uani 1 1 d . . . . . H15A H 0.874168 0.938064 0.234892 0.060 Uiso 1 1 calc R U . . . C16 C 0.8943(2) 0.9637(2) 0.17182(16) 0.0866(13) Uani 1 1 d . . . . . H16A H 0.941808 0.981809 0.179731 0.130 Uiso 1 1 calc R U . . . H16B H 0.862657 1.007663 0.169349 0.130 Uiso 1 1 calc R U . . . H16C H 0.891480 0.936629 0.143856 0.130 Uiso 1 1 calc R U . . . C17 C 0.80156(17) 0.8802(2) 0.19335(12) 0.0604(8) Uani 1 1 d . . . . . H17A H 0.800913 0.850909 0.166224 0.091 Uiso 1 1 calc R U . . . H17B H 0.769960 0.924070 0.188751 0.091 Uiso 1 1 calc R U . . . H17C H 0.786756 0.847070 0.216224 0.091 Uiso 1 1 calc R U . . . C18 C 0.92102(16) 0.91342(15) 0.42392(9) 0.0479(7) Uani 1 1 d . . . . . C19 C 0.85789(18) 0.92946(17) 0.43919(10) 0.0536(7) Uani 1 1 d . . . . . C20 C 0.8483(2) 0.9077(2) 0.48186(11) 0.0635(9) Uani 1 1 d . . . . . H20A H 0.805603 0.918563 0.492813 0.076 Uiso 1 1 calc R U . . . C21 C 0.9001(2) 0.87066(19) 0.50806(11) 0.0658(9) Uani 1 1 d . . . . . H21A H 0.892552 0.855645 0.536726 0.079 Uiso 1 1 calc R U . . . C22 C 0.9622(2) 0.85545(18) 0.49294(11) 0.0635(9) Uani 1 1 d . . . . . H22A H 0.997596 0.830461 0.511516 0.076 Uiso 1 1 calc R U . . . C23 C 0.97491(17) 0.87595(17) 0.45063(11) 0.0550(7) Uani 1 1 d . . . . . C24 C 0.79989(18) 0.97013(19) 0.41130(11) 0.0606(8) Uani 1 1 d . . . . . H24A H 0.810457 0.967226 0.380399 0.073 Uiso 1 1 calc R U . . . C25 C 0.7970(3) 1.0545(2) 0.4234(2) 0.1056(18) Uani 1 1 d . . . . . H25A H 0.782876 1.059392 0.452695 0.158 Uiso 1 1 calc R U . . . H25B H 0.763478 1.080950 0.402455 0.158 Uiso 1 1 calc R U . . . H25C H 0.842902 1.077554 0.422693 0.158 Uiso 1 1 calc R U . . . C26 C 0.7295(2) 0.9341(2) 0.41325(15) 0.0821(12) Uani 1 1 d . . . . . H26A H 0.732467 0.878685 0.408205 0.123 Uiso 1 1 calc R U . . . H26B H 0.696167 0.957023 0.390801 0.123 Uiso 1 1 calc R U . . . H26C H 0.714396 0.943296 0.442019 0.123 Uiso 1 1 calc R U . . . C27 C 1.04419(18) 0.8568(2) 0.43519(13) 0.0667(9) Uani 1 1 d . . . . . H27A H 1.045772 0.881390 0.406052 0.080 Uiso 1 1 calc R U . . . C28 C 1.0535(2) 0.7703(2) 0.42980(16) 0.0782(11) Uani 1 1 d . . . . . H28A H 1.053534 0.744989 0.458154 0.117 Uiso 1 1 calc R U . . . H28B H 1.097595 0.760279 0.418229 0.117 Uiso 1 1 calc R U . . . H28C H 1.015372 0.750020 0.409578 0.117 Uiso 1 1 calc R U . . . C29 C 1.1049(2) 0.8887(3) 0.4661(2) 0.1141(19) Uani 1 1 d . . . . . H29A H 1.098885 0.944167 0.469708 0.171 Uiso 1 1 calc R U . . . H29B H 1.148439 0.878902 0.453904 0.171 Uiso 1 1 calc R U . . . H29C H 1.105972 0.863374 0.494536 0.171 Uiso 1 1 calc R U . . . N31 N 0.64940(11) 0.91349(11) 0.26829(7) 0.0375(4) Uani 1 1 d . . . . . C31 C 0.61803(13) 0.91320(15) 0.22797(9) 0.0403(6) Uani 1 1 d . . . . . C32 C 0.61695(14) 0.85077(16) 0.19881(9) 0.0443(6) Uani 1 1 d . . . . . H32A H 0.601242 0.862421 0.169318 0.053 Uiso 1 1 calc R U . . . C33 C 0.63580(13) 0.77375(15) 0.20715(9) 0.0422(6) Uani 1 1 d . . . . . N33 N 0.66830(10) 0.74855(11) 0.24452(7) 0.0386(5) Uani 1 1 d . . . . . C34 C 0.57848(17) 0.98301(18) 0.20958(11) 0.0567(8) Uani 1 1 d . . . . . H34A H 0.545280 0.998923 0.229504 0.085 Uiso 1 1 calc R U . . . H34B H 0.553583 0.970233 0.181146 0.085 Uiso 1 1 calc R U . . . H34C H 0.610979 1.025072 0.206194 0.085 Uiso 1 1 calc R U . . . C35 C 0.61555(19) 0.71810(19) 0.17013(11) 0.0638(9) Uani 1 1 d . . . . . H35A H 0.657399 0.695962 0.160166 0.096 Uiso 1 1 calc R U . . . H35B H 0.589195 0.745453 0.145976 0.096 Uiso 1 1 calc R U . . . H35C H 0.586973 0.676915 0.180324 0.096 Uiso 1 1 calc R U . . . C36 C 0.63978(14) 0.97947(14) 0.29531(9) 0.0417(6) Uani 1 1 d . . . . . C37 C 0.58853(16) 0.97589(18) 0.32400(10) 0.0511(7) Uani 1 1 d . . . . . C38 C 0.57760(19) 1.0408(2) 0.34878(12) 0.0629(9) Uani 1 1 d . . . . . H38A H 0.541686 1.040165 0.367264 0.076 Uiso 1 1 calc R U . . . C39 C 0.6176(2) 1.1055(2) 0.34707(12) 0.0679(9) Uani 1 1 d . . . . . H39A H 0.609195 1.149060 0.364257 0.081 Uiso 1 1 calc R U . . . C40 C 0.66987(19) 1.10730(17) 0.32042(11) 0.0601(8) Uani 1 1 d . . . . . H40A H 0.698045 1.151832 0.319969 0.072 Uiso 1 1 calc R U . . . C41 C 0.68216(16) 1.04444(15) 0.29395(10) 0.0479(6) Uani 1 1 d . . . . . C42 C 0.54542(17) 0.9036(2) 0.32825(12) 0.0611(8) Uani 1 1 d . . . . . H42A H 0.572017 0.860416 0.316765 0.073 Uiso 1 1 calc R U . . . C43 C 0.5363(3) 0.8831(3) 0.37459(15) 0.0957(14) Uani 1 1 d . . . . . H43A H 0.509753 0.923562 0.387280 0.144 Uiso 1 1 calc R U . . . H43B H 0.581812 0.878177 0.391521 0.144 Uiso 1 1 calc R U . . . H43C H 0.511352 0.834247 0.375127 0.144 Uiso 1 1 calc R U . . . C44 C 0.4776(3) 0.9063(4) 0.3006(2) 0.131(3) Uani 1 1 d . . . . . H44A H 0.451800 0.858887 0.304675 0.197 Uiso 1 1 calc R U . . . H44B H 0.485421 0.911124 0.269947 0.197 Uiso 1 1 calc R U . . . H44C H 0.450843 0.950490 0.309044 0.197 Uiso 1 1 calc R U . . . C45 C 0.73972(18) 1.04984(17) 0.26490(11) 0.0576(8) Uani 1 1 d . . . . . H45A H 0.740869 1.000374 0.248530 0.069 Uiso 1 1 calc R U . . . C46 C 0.81056(19) 1.0613(2) 0.29061(13) 0.0682(9) Uani 1 1 d . . . . . H46A H 0.846241 1.061667 0.270564 0.102 Uiso 1 1 calc R U . . . H46B H 0.819711 1.019269 0.311570 0.102 Uiso 1 1 calc R U . . . H46C H 0.811286 1.110352 0.306236 0.102 Uiso 1 1 calc R U . . . C47 C 0.7271(3) 1.1155(3) 0.23122(16) 0.0990(15) Uani 1 1 d . . . . . H47A H 0.729697 1.165036 0.246368 0.148 Uiso 1 1 calc R U . . . H47B H 0.681166 1.109492 0.214961 0.148 Uiso 1 1 calc R U . . . H47C H 0.762498 1.113480 0.210997 0.148 Uiso 1 1 calc R U . . . C48 C 0.66865(13) 0.66617(14) 0.25118(9) 0.0408(6) Uani 1 1 d . . . . . C49 C 0.72159(14) 0.62074(15) 0.23757(10) 0.0452(6) Uani 1 1 d . . . . . C50 C 0.71736(16) 0.54134(16) 0.24239(11) 0.0535(7) Uani 1 1 d . . . . . H50A H 0.752584 0.509669 0.232939 0.064 Uiso 1 1 calc R U . . . C51 C 0.66325(16) 0.50785(16) 0.26054(12) 0.0570(8) Uani 1 1 d . . . . . H51A H 0.660581 0.453543 0.262916 0.068 Uiso 1 1 calc R U . . . C52 C 0.61314(16) 0.55352(17) 0.27520(12) 0.0585(8) Uani 1 1 d . . . . . H52A H 0.576426 0.530203 0.288315 0.070 Uiso 1 1 calc R U . . . C53 C 0.61480(14) 0.63341(16) 0.27133(11) 0.0491(7) Uani 1 1 d . . . . . C54 C 0.78389(15) 0.65663(16) 0.22003(10) 0.0499(7) Uani 1 1 d . . . . . H54A H 0.771334 0.710674 0.211462 0.060 Uiso 1 1 calc R U . . . C55 C 0.8063(2) 0.6162(2) 0.17991(12) 0.0672(9) Uani 1 1 d . . . . . H55A H 0.823829 0.564808 0.188080 0.101 Uiso 1 1 calc R U . . . H55B H 0.842882 0.646131 0.168383 0.101 Uiso 1 1 calc R U . . . H55C H 0.766523 0.611738 0.157575 0.101 Uiso 1 1 calc R U . . . C56 C 0.84362(16) 0.6601(2) 0.25629(12) 0.0597(8) Uani 1 1 d . . . . . H56A H 0.857732 0.607778 0.265041 0.090 Uiso 1 1 calc R U . . . H56B H 0.828805 0.687562 0.281340 0.090 Uiso 1 1 calc R U . . . H56C H 0.882804 0.687125 0.245839 0.090 Uiso 1 1 calc R U . . . C57 C 0.55883(16) 0.68195(19) 0.28816(14) 0.0634(9) Uani 1 1 d . . . . . H57A H 0.577343 0.735468 0.291642 0.076 Uiso 1 1 calc R U . . . C58 C 0.5414(2) 0.6556(2) 0.33321(15) 0.0810(12) Uani 1 1 d . . . . . H58A H 0.509215 0.692214 0.344195 0.121 Uiso 1 1 calc R U . . . H58B H 0.584023 0.653284 0.353406 0.121 Uiso 1 1 calc R U . . . H58C H 0.520013 0.604620 0.330722 0.121 Uiso 1 1 calc R U . . . C59 C 0.49376(17) 0.6857(2) 0.25567(17) 0.0831(13) Uani 1 1 d . . . . . H59A H 0.478051 0.633433 0.247956 0.125 Uiso 1 1 calc R U . . . H59B H 0.504166 0.712815 0.229374 0.125 Uiso 1 1 calc R U . . . H59C H 0.457271 0.713163 0.268790 0.125 Uiso 1 1 calc R U . . . C60 C 0.84754(14) 0.71523(15) 0.38131(10) 0.0433(6) Uani 1 1 d . . . . . O60 O 0.88541(10) 0.75923(11) 0.36588(7) 0.0522(5) Uani 1 1 d . . . . . C61 C 0.73083(14) 0.71860(15) 0.36786(9) 0.0420(6) Uani 1 1 d . . . . . O61 O 0.69939(10) 0.76766(11) 0.34598(7) 0.0476(4) Uani 1 1 d . . . . . C62 C 0.77337(18) 0.70882(18) 0.44869(11) 0.0549(7) Uani 1 1 d . . . . . O62 O 0.76295(17) 0.74881(15) 0.47680(8) 0.0799(8) Uani 1 1 d . . . . . O63 O 0.84879(10) 0.55189(11) 0.41350(7) 0.0468(4) Uani 1 1 d . . . . . C63 C 0.82154(18) 0.55066(16) 0.37118(11) 0.0538(7) Uani 1 1 d . . . . . H63A H 0.849740 0.549147 0.347976 0.065 Uiso 1 1 calc R U . . . O64 O 0.71820(10) 0.55617(11) 0.40071(7) 0.0488(5) Uani 1 1 d . . . . . C64 C 0.75073(18) 0.55173(16) 0.36400(10) 0.0541(7) Uani 1 1 d . . . . . H64A H 0.726250 0.549546 0.335633 0.065 Uiso 1 1 calc R U . . . N71 N 0.75500(11) 0.38392(12) 0.43609(7) 0.0386(5) Uani 1 1 d . . . . . C71 C 0.76192(13) 0.33435(15) 0.46891(10) 0.0434(6) Uani 1 1 d . . . . . C72 C 0.78638(15) 0.35369(16) 0.51189(10) 0.0471(6) Uani 1 1 d . . . . . H72A H 0.795198 0.311024 0.530871 0.057 Uiso 1 1 calc R U . . . C73 C 0.80006(14) 0.42566(16) 0.53165(10) 0.0466(6) Uani 1 1 d . . . . . N73 N 0.79670(11) 0.49233(12) 0.51049(7) 0.0415(5) Uani 1 1 d . . . . . C74 C 0.74071(17) 0.25126(16) 0.46120(12) 0.0563(8) Uani 1 1 d . . . . . H74A H 0.690860 0.246047 0.462860 0.084 Uiso 1 1 calc R U . . . H74B H 0.766113 0.218784 0.483465 0.084 Uiso 1 1 calc R U . . . H74C H 0.751438 0.235211 0.432298 0.084 Uiso 1 1 calc R U . . . C75 C 0.8178(2) 0.4251(2) 0.58061(11) 0.0647(9) Uani 1 1 d . . . . . H75A H 0.864385 0.446121 0.588048 0.097 Uiso 1 1 calc R U . . . H75B H 0.816203 0.372271 0.591388 0.097 Uiso 1 1 calc R U . . . H75C H 0.784204 0.456631 0.594086 0.097 Uiso 1 1 calc R U . . . C76 C 0.72475(15) 0.35863(14) 0.39380(10) 0.0437(6) Uani 1 1 d . . . . . C77 C 0.65223(16) 0.35569(17) 0.38425(11) 0.0543(7) Uani 1 1 d . . . . . C78 C 0.6250(2) 0.33294(19) 0.34242(13) 0.0667(10) Uani 1 1 d . . . . . H78A H 0.576199 0.330652 0.335463 0.080 Uiso 1 1 calc R U . . . C79 C 0.6666(2) 0.31396(19) 0.31139(13) 0.0696(10) Uani 1 1 d . . . . . H79A H 0.646862 0.297427 0.283410 0.084 Uiso 1 1 calc R U . . . C80 C 0.7375(2) 0.31892(17) 0.32089(11) 0.0632(9) Uani 1 1 d . . . . . H80A H 0.766147 0.306527 0.298904 0.076 Uiso 1 1 calc R U . . . C81 C 0.76837(17) 0.34158(15) 0.36181(10) 0.0503(7) Uani 1 1 d . . . . . C82 C 0.60358(16) 0.3777(2) 0.41758(13) 0.0652(9) Uani 1 1 d . . . . . H82A H 0.632022 0.385507 0.446276 0.078 Uiso 1 1 calc R U . . . C83 C 0.56697(19) 0.4540(2) 0.40446(17) 0.0814(12) Uani 1 1 d . . . . . H83A H 0.601647 0.494469 0.402754 0.122 Uiso 1 1 calc R U . . . H83B H 0.536242 0.468076 0.426281 0.122 Uiso 1 1 calc R U . . . H83C H 0.539698 0.448111 0.376003 0.122 Uiso 1 1 calc R U . . . C84 C 0.5497(2) 0.3156(3) 0.42336(18) 0.0939(14) Uani 1 1 d . . . . . H84A H 0.519565 0.308907 0.395981 0.141 Uiso 1 1 calc R U . . . H84B H 0.521706 0.330976 0.446402 0.141 Uiso 1 1 calc R U . . . H84C H 0.573204 0.266975 0.431390 0.141 Uiso 1 1 calc R U . . . C85 C 0.84675(18) 0.34703(18) 0.37135(12) 0.0588(8) Uani 1 1 d . . . . . H85A H 0.857046 0.386877 0.394491 0.071 Uiso 1 1 calc R U . . . C86 C 0.8783(2) 0.2715(2) 0.38926(15) 0.0780(11) Uani 1 1 d . . . . . H86A H 0.861824 0.260440 0.417453 0.117 Uiso 1 1 calc R U . . . H86B H 0.928879 0.275815 0.392983 0.117 Uiso 1 1 calc R U . . . H86C H 0.864372 0.229808 0.368815 0.117 Uiso 1 1 calc R U . . . C87 C 0.8820(2) 0.3721(2) 0.33219(15) 0.0785(11) Uani 1 1 d . . . . . H87A H 0.880788 0.329879 0.311129 0.118 Uiso 1 1 calc R U . . . H87B H 0.930264 0.385840 0.341677 0.118 Uiso 1 1 calc R U . . . H87C H 0.857781 0.416759 0.318500 0.118 Uiso 1 1 calc R U . . . C88 C 0.80336(14) 0.56337(16) 0.53465(9) 0.0440(6) Uani 1 1 d . . . . . C89 C 0.86692(15) 0.60264(16) 0.54028(10) 0.0466(6) Uani 1 1 d . . . . . C90 C 0.86911(17) 0.67389(17) 0.56100(10) 0.0532(7) Uani 1 1 d . . . . . H90A H 0.911609 0.701320 0.564976 0.064 Uiso 1 1 calc R U . . . C91 C 0.81113(19) 0.70547(19) 0.57584(10) 0.0598(8) Uani 1 1 d . . . . . H91A H 0.813645 0.754382 0.589576 0.072 Uiso 1 1 calc R U . . . C92 C 0.74979(18) 0.6659(2) 0.57068(11) 0.0579(8) Uani 1 1 d . . . . . H92A H 0.710216 0.687810 0.581357 0.069 Uiso 1 1 calc R U . . . C93 C 0.74374(16) 0.59456(19) 0.55029(10) 0.0519(7) Uani 1 1 d . . . . . C94 C 0.93280(16) 0.57051(18) 0.52532(11) 0.0531(7) Uani 1 1 d . . . . . H94A H 0.920508 0.522267 0.508638 0.064 Uiso 1 1 calc R U . . . C95 C 0.98495(19) 0.5496(3) 0.56434(14) 0.0762(10) Uani 1 1 d . . . . . H95A H 0.997670 0.595983 0.581397 0.114 Uiso 1 1 calc R U . . . H95B H 1.026451 0.527395 0.553982 0.114 Uiso 1 1 calc R U . . . H95C H 0.964140 0.512144 0.582657 0.114 Uiso 1 1 calc R U . . . C96 C 0.96610(19) 0.6256(2) 0.49518(14) 0.0682(9) Uani 1 1 d . . . . . H96A H 0.980001 0.672880 0.511055 0.102 Uiso 1 1 calc R U . . . H96B H 0.932677 0.638045 0.470006 0.102 Uiso 1 1 calc R U . . . H96C H 1.006944 0.601265 0.485164 0.102 Uiso 1 1 calc R U . . . C97 C 0.67462(17) 0.5534(2) 0.54385(12) 0.0672(9) Uani 1 1 d . . . . . H97A H 0.683427 0.498605 0.536498 0.081 Uiso 1 1 calc R U . . . C98 C 0.6283(2) 0.5886(3) 0.50576(18) 0.1044(16) Uani 1 1 d . . . . . H98A H 0.615788 0.641147 0.513228 0.157 Uiso 1 1 calc R U . . . H98B H 0.586246 0.557678 0.499706 0.157 Uiso 1 1 calc R U . . . H98C H 0.653296 0.589701 0.479895 0.157 Uiso 1 1 calc R U . . . C99 C 0.6384(3) 0.5545(4) 0.58544(17) 0.1057(17) Uani 1 1 d . . . . . H99A H 0.623242 0.606957 0.590977 0.159 Uiso 1 1 calc R U . . . H99B H 0.670731 0.537001 0.610088 0.159 Uiso 1 1 calc R U . . . H99C H 0.598131 0.520313 0.581849 0.159 Uiso 1 1 calc R U . . . C101 C 0.2679(14) 0.8968(12) 0.3602(8) 0.189(7) Uiso 0.385(3) 1 d D U P A 1 H10B H 0.266585 0.932360 0.335494 0.284 Uiso 0.385(3) 1 calc R U P A 1 H10C H 0.220586 0.881719 0.364553 0.284 Uiso 0.385(3) 1 calc R U P A 1 H10D H 0.289787 0.922177 0.386522 0.284 Uiso 0.385(3) 1 calc R U P A 1 C102 C 0.3090(19) 0.8265(15) 0.3509(7) 0.200(7) Uiso 0.385(3) 1 d D U P A 1 H10E H 0.287454 0.800190 0.324379 0.240 Uiso 0.385(3) 1 calc R U P A 1 H10F H 0.356989 0.840843 0.346454 0.240 Uiso 0.385(3) 1 calc R U P A 1 C103 C 0.3089(13) 0.7750(14) 0.3897(9) 0.178(6) Uiso 0.385(3) 1 d D U P A 1 H10G H 0.263073 0.749950 0.389104 0.214 Uiso 0.385(3) 1 calc R U P A 1 H10H H 0.316605 0.806199 0.416603 0.214 Uiso 0.385(3) 1 calc R U P A 1 C104 C 0.3641(14) 0.7146(14) 0.3904(6) 0.178(6) Uiso 0.385(3) 1 d D U P A 1 H10I H 0.404513 0.734910 0.377214 0.214 Uiso 0.385(3) 1 calc R U P A 1 H10J H 0.346122 0.669242 0.373377 0.214 Uiso 0.385(3) 1 calc R U P A 1 C105 C 0.3853(11) 0.6919(13) 0.4370(6) 0.160(6) Uiso 0.385(3) 1 d D U P A 1 H10K H 0.389282 0.738975 0.455101 0.192 Uiso 0.385(3) 1 calc R U P A 1 H10L H 0.348254 0.659774 0.447134 0.192 Uiso 0.385(3) 1 calc R U P A 1 C106 C 0.4520(14) 0.6489(19) 0.4441(11) 0.169(7) Uiso 0.385(3) 1 d D U P A 1 H10M H 0.462135 0.636308 0.475096 0.253 Uiso 0.385(3) 1 calc R U P A 1 H10N H 0.448276 0.601396 0.426989 0.253 Uiso 0.385(3) 1 calc R U P A 1 H10O H 0.489371 0.680727 0.434969 0.253 Uiso 0.385(3) 1 calc R U P A 1 C111 C 0.2207(13) 0.9047(14) 0.3747(10) 0.176(8) Uiso 0.322(3) 1 d D U P B 2 H11A H 0.219668 0.960585 0.378549 0.264 Uiso 0.322(3) 1 calc R U P B 2 H11B H 0.217150 0.892596 0.343533 0.264 Uiso 0.322(3) 1 calc R U P B 2 H11C H 0.181757 0.881448 0.387464 0.264 Uiso 0.322(3) 1 calc R U P B 2 C112 C 0.2871(13) 0.8736(13) 0.3968(11) 0.206(8) Uiso 0.322(3) 1 d D U P B 2 H11D H 0.326169 0.898393 0.384139 0.247 Uiso 0.322(3) 1 calc R U P B 2 H11E H 0.290806 0.887253 0.428033 0.247 Uiso 0.322(3) 1 calc R U P B 2 C113 C 0.2935(12) 0.7887(13) 0.3926(11) 0.169(6) Uiso 0.322(3) 1 d D U P B 2 H11F H 0.259286 0.763645 0.409451 0.203 Uiso 0.322(3) 1 calc R U P B 2 H11G H 0.282293 0.774140 0.361687 0.203 Uiso 0.322(3) 1 calc R U P B 2 C114 C 0.3637(14) 0.7596(13) 0.4084(12) 0.159(6) Uiso 0.322(3) 1 d D U P B 2 H11H H 0.375551 0.776450 0.438902 0.191 Uiso 0.322(3) 1 calc R U P B 2 H11I H 0.397487 0.783397 0.390743 0.191 Uiso 0.322(3) 1 calc R U P B 2 C115 C 0.3714(17) 0.6739(13) 0.4064(14) 0.168(6) Uiso 0.322(3) 1 d D U P B 2 H11J H 0.376247 0.657124 0.376317 0.202 Uiso 0.322(3) 1 calc R U P B 2 H11K H 0.330476 0.648131 0.416325 0.202 Uiso 0.322(3) 1 calc R U P B 2 C116 C 0.436(2) 0.655(2) 0.4366(15) 0.186(8) Uiso 0.322(3) 1 d D U P B 2 H11L H 0.443821 0.598995 0.436564 0.280 Uiso 0.322(3) 1 calc R U P B 2 H11M H 0.476096 0.680745 0.426376 0.280 Uiso 0.322(3) 1 calc R U P B 2 H11N H 0.430572 0.671801 0.466169 0.280 Uiso 0.322(3) 1 calc R U P B 2 C121 C 0.2834(18) 0.8584(18) 0.3187(9) 0.206(10) Uiso 0.292(3) 1 d D U P C 3 H12J H 0.263765 0.910274 0.315885 0.309 Uiso 0.292(3) 1 calc R U P C 3 H12K H 0.324595 0.855565 0.303200 0.309 Uiso 0.292(3) 1 calc R U P C 3 H12L H 0.248920 0.821123 0.306204 0.309 Uiso 0.292(3) 1 calc R U P C 3 C122 C 0.303(2) 0.8403(17) 0.3661(8) 0.177(7) Uiso 0.292(3) 1 d D U P C 3 H12B H 0.261971 0.842222 0.382399 0.213 Uiso 0.292(3) 1 calc R U P C 3 H12C H 0.338193 0.876913 0.379373 0.213 Uiso 0.292(3) 1 calc R U P C 3 C123 C 0.3322(16) 0.7593(13) 0.3656(7) 0.165(7) Uiso 0.292(3) 1 d D U P C 3 H12D H 0.294567 0.721956 0.357324 0.198 Uiso 0.292(3) 1 calc R U P C 3 H12E H 0.366301 0.755635 0.344102 0.198 Uiso 0.292(3) 1 calc R U P C 3 C124 C 0.367(2) 0.7418(14) 0.4107(9) 0.152(6) Uiso 0.292(3) 1 d D U P C 3 H12F H 0.409208 0.773139 0.416562 0.183 Uiso 0.292(3) 1 calc R U P C 3 H12G H 0.335068 0.755495 0.432456 0.183 Uiso 0.292(3) 1 calc R U P C 3 C125 C 0.385(2) 0.6584(14) 0.4148(11) 0.170(7) Uiso 0.292(3) 1 d D U P C 3 H12H H 0.411190 0.643128 0.390494 0.204 Uiso 0.292(3) 1 calc R U P C 3 H12I H 0.341895 0.627427 0.412765 0.204 Uiso 0.292(3) 1 calc R U P C 3 C126 C 0.4277(17) 0.6426(17) 0.4576(9) 0.163(8) Uiso 0.292(3) 1 d D U P C 3 H12M H 0.439075 0.587738 0.459683 0.244 Uiso 0.292(3) 1 calc R U P C 3 H12N H 0.470550 0.672678 0.459386 0.244 Uiso 0.292(3) 1 calc R U P C 3 H12O H 0.401353 0.657000 0.481626 0.244 Uiso 0.292(3) 1 calc R U P C 3 C131 C 0.4177(7) 0.9106(10) 0.5259(6) 0.131(4) Uiso 0.468(3) 1 d D U P D 1 H13L H 0.380076 0.903283 0.502345 0.196 Uiso 0.468(3) 1 calc R U P D 1 H13M H 0.406932 0.882864 0.551869 0.196 Uiso 0.468(3) 1 calc R U P D 1 H13N H 0.422836 0.965497 0.532559 0.196 Uiso 0.468(3) 1 calc R U P D 1 C132 C 0.4850(8) 0.8799(13) 0.5116(6) 0.153(5) Uiso 0.468(3) 1 d D U P D 1 H13D H 0.478619 0.824850 0.504104 0.184 Uiso 0.468(3) 1 calc R U P D 1 H13E H 0.494495 0.907335 0.484829 0.184 Uiso 0.468(3) 1 calc R U P D 1 C133 C 0.5474(7) 0.8879(15) 0.5452(6) 0.168(5) Uiso 0.468(3) 1 d D U P D 1 H13F H 0.551279 0.941724 0.555588 0.202 Uiso 0.468(3) 1 calc R U P D 1 H13G H 0.541609 0.854534 0.570538 0.202 Uiso 0.468(3) 1 calc R U P D 1 C134 C 0.6124(8) 0.8654(14) 0.5257(7) 0.190(6) Uiso 0.468(3) 1 d D U P D 1 H13H H 0.608331 0.810937 0.516569 0.228 Uiso 0.468(3) 1 calc R U P D 1 H13I H 0.615508 0.896697 0.499238 0.228 Uiso 0.468(3) 1 calc R U P D 1 C135 C 0.6785(8) 0.8751(11) 0.5556(7) 0.161(6) Uiso 0.468(3) 1 d D U P D 1 H13J H 0.669953 0.856250 0.584735 0.193 Uiso 0.468(3) 1 calc R U P D 1 H13K H 0.713608 0.840733 0.544983 0.193 Uiso 0.468(3) 1 calc R U P D 1 C136 C 0.7096(11) 0.9518(13) 0.5613(8) 0.239(9) Uiso 0.468(3) 1 d D U P D 1 H13O H 0.752057 0.948796 0.581569 0.359 Uiso 0.468(3) 1 calc R U P D 1 H13P H 0.720652 0.971171 0.533112 0.359 Uiso 0.468(3) 1 calc R U P D 1 H13Q H 0.676760 0.986772 0.573080 0.359 Uiso 0.468(3) 1 calc R U P D 1 C141 C 0.3820(8) 0.9160(11) 0.5178(6) 0.112(4) Uiso 0.371(3) 1 d D U P E 2 H14L H 0.343778 0.911306 0.494468 0.168 Uiso 0.371(3) 1 calc R U P E 2 H14M H 0.371120 0.886698 0.543283 0.168 Uiso 0.371(3) 1 calc R U P E 2 H14N H 0.388627 0.970225 0.525825 0.168 Uiso 0.371(3) 1 calc R U P E 2 C142 C 0.4466(8) 0.8854(12) 0.5026(5) 0.125(5) Uiso 0.371(3) 1 d D U P E 2 H14D H 0.455687 0.914499 0.476267 0.150 Uiso 0.371(3) 1 calc R U P E 2 H14E H 0.438239 0.831252 0.493666 0.150 Uiso 0.371(3) 1 calc R U P E 2 C143 C 0.5110(9) 0.8882(16) 0.5347(7) 0.153(5) Uiso 0.371(3) 1 d D U P E 2 H14F H 0.502490 0.864594 0.562725 0.183 Uiso 0.371(3) 1 calc R U P E 2 H14G H 0.526510 0.941892 0.539982 0.183 Uiso 0.371(3) 1 calc R U P E 2 C144 C 0.5651(10) 0.8419(15) 0.5128(8) 0.190(6) Uiso 0.371(3) 1 d D U P E 2 H14H H 0.548380 0.788731 0.507183 0.228 Uiso 0.371(3) 1 calc R U P E 2 H14I H 0.572270 0.865708 0.484509 0.228 Uiso 0.371(3) 1 calc R U P E 2 C145 C 0.6313(11) 0.8408(14) 0.5417(9) 0.198(7) Uiso 0.371(3) 1 d D U P E 2 H14J H 0.669550 0.829455 0.523975 0.238 Uiso 0.371(3) 1 calc R U P E 2 H14K H 0.629760 0.798876 0.563194 0.238 Uiso 0.371(3) 1 calc R U P E 2 C146 C 0.6464(13) 0.9152(15) 0.5655(9) 0.192(7) Uiso 0.371(3) 1 d D U P E 2 H14O H 0.690583 0.911148 0.584011 0.287 Uiso 0.371(3) 1 calc R U P E 2 H14P H 0.649098 0.956863 0.544387 0.287 Uiso 0.371(3) 1 calc R U P E 2 H14Q H 0.609287 0.926267 0.583627 0.287 Uiso 0.371(3) 1 calc R U P E 2 C151 C 0.3477(16) 0.922(2) 0.4860(13) 0.119(9) Uiso 0.161(3) 1 d D U P F 3 H15J H 0.310327 0.893849 0.469106 0.179 Uiso 0.161(3) 1 calc R U P F 3 H15K H 0.329098 0.950127 0.509674 0.179 Uiso 0.161(3) 1 calc R U P F 3 H15L H 0.367996 0.958950 0.466936 0.179 Uiso 0.161(3) 1 calc R U P F 3 C152 C 0.4019(17) 0.8676(18) 0.5045(16) 0.150(8) Uiso 0.161(3) 1 d D U P F 3 H15B H 0.419501 0.838850 0.480407 0.180 Uiso 0.161(3) 1 calc R U P F 3 H15C H 0.380647 0.830037 0.523096 0.180 Uiso 0.161(3) 1 calc R U P F 3 C153 C 0.4619(16) 0.905(3) 0.5312(13) 0.146(7) Uiso 0.161(3) 1 d D U P F 3 H15D H 0.459767 0.894536 0.562419 0.175 Uiso 0.161(3) 1 calc R U P F 3 H15E H 0.459138 0.961802 0.526939 0.175 Uiso 0.161(3) 1 calc R U P F 3 C154 C 0.5296(16) 0.876(4) 0.5178(17) 0.175(7) Uiso 0.161(3) 1 d D U P F 3 H15F H 0.528898 0.819392 0.516665 0.210 Uiso 0.161(3) 1 calc R U P F 3 H15G H 0.536048 0.895747 0.488449 0.210 Uiso 0.161(3) 1 calc R U P F 3 C155 C 0.5885(18) 0.903(4) 0.5500(17) 0.180(7) Uiso 0.161(3) 1 d D U P F 3 H15H H 0.587175 0.959416 0.552243 0.217 Uiso 0.161(3) 1 calc R U P F 3 H15I H 0.582599 0.881261 0.579069 0.217 Uiso 0.161(3) 1 calc R U P F 3 C156 C 0.6574(18) 0.879(5) 0.537(2) 0.196(8) Uiso 0.161(3) 1 d D U P F 3 H15M H 0.694137 0.897103 0.559294 0.293 Uiso 0.161(3) 1 calc R U P F 3 H15N H 0.659361 0.822478 0.535796 0.293 Uiso 0.161(3) 1 calc R U P F 3 H15O H 0.663937 0.900627 0.508973 0.293 Uiso 0.161(3) 1 calc R U P F 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cr1 0.0434(2) 0.0329(2) 0.0409(2) 0.00800(18) -0.00308(18) -0.00251(17) Mg1 0.0351(4) 0.0296(4) 0.0403(4) 0.0010(3) -0.0041(3) -0.0048(3) Mg2 0.0332(4) 0.0268(4) 0.0407(4) 0.0031(3) -0.0051(3) 0.0011(3) Mg3 0.0417(4) 0.0325(4) 0.0421(5) 0.0067(3) 0.0037(4) 0.0012(3) N1 0.0343(10) 0.0307(9) 0.0469(12) 0.0019(9) -0.0019(9) -0.0033(8) C1 0.0385(13) 0.0390(13) 0.0576(17) 0.0037(12) -0.0025(12) -0.0102(11) C2 0.0546(16) 0.0344(13) 0.0593(18) -0.0004(13) -0.0077(14) -0.0158(11) C3 0.0589(17) 0.0306(12) 0.0515(16) 0.0000(12) -0.0134(13) -0.0067(11) N3 0.0487(12) 0.0354(11) 0.0430(12) 0.0004(9) -0.0094(10) -0.0043(9) C4 0.064(2) 0.062(2) 0.079(2) -0.0040(18) 0.0202(18) -0.0281(16) C5 0.094(3) 0.0522(18) 0.061(2) -0.0077(16) -0.0080(19) -0.0254(17) C6 0.0360(12) 0.0320(12) 0.0522(15) -0.0010(11) 0.0081(11) -0.0069(9) C7 0.0385(14) 0.0399(14) 0.074(2) -0.0006(14) 0.0047(14) -0.0008(11) C8 0.0461(16) 0.0419(15) 0.093(3) -0.0084(16) 0.0189(17) 0.0049(12) C9 0.0622(19) 0.0492(16) 0.066(2) -0.0112(15) 0.0218(17) -0.0026(14) C10 0.0667(19) 0.0443(15) 0.0515(17) -0.0050(13) 0.0136(15) -0.0038(13) C11 0.0469(14) 0.0391(13) 0.0470(15) 0.0003(12) 0.0084(12) -0.0050(11) C12 0.0575(19) 0.0538(18) 0.091(3) -0.0036(18) -0.0148(18) 0.0160(15) C13 0.138(4) 0.063(2) 0.104(4) 0.017(2) -0.036(3) 0.013(3) C14 0.067(3) 0.178(7) 0.201(8) 0.026(6) -0.046(4) -0.005(4) C15 0.0652(18) 0.0381(13) 0.0443(15) -0.0003(12) -0.0024(14) 0.0026(12) C16 0.096(3) 0.060(2) 0.103(3) 0.035(2) 0.011(3) 0.004(2) C17 0.0564(18) 0.0622(19) 0.062(2) -0.0106(16) 0.0030(15) 0.0079(15) C18 0.0639(18) 0.0329(12) 0.0426(15) -0.0008(11) -0.0135(13) -0.0081(12) C19 0.071(2) 0.0443(15) 0.0423(15) -0.0034(13) -0.0062(14) 0.0011(13) C20 0.089(2) 0.0575(18) 0.0429(17) -0.0043(14) 0.0019(17) 0.0042(17) C21 0.103(3) 0.0502(17) 0.0407(16) 0.0009(14) -0.0065(18) -0.0091(17) C22 0.089(3) 0.0473(16) 0.0473(17) 0.0039(14) -0.0239(17) -0.0057(16) C23 0.0632(18) 0.0421(14) 0.0539(18) 0.0028(13) -0.0185(15) -0.0073(13) C24 0.073(2) 0.0582(18) 0.0491(17) -0.0009(15) 0.0000(16) 0.0126(16) C25 0.106(3) 0.053(2) 0.146(5) 0.001(3) -0.034(3) 0.012(2) C26 0.075(2) 0.077(3) 0.089(3) -0.001(2) -0.017(2) 0.0046(19) C27 0.0592(19) 0.0617(19) 0.073(2) 0.0133(17) -0.0185(17) -0.0041(15) C28 0.060(2) 0.074(2) 0.097(3) 0.000(2) -0.011(2) 0.0064(17) C29 0.075(3) 0.104(4) 0.152(5) -0.004(4) -0.038(3) -0.017(3) N31 0.0364(10) 0.0317(10) 0.0427(12) 0.0028(9) -0.0030(9) 0.0049(8) C31 0.0344(12) 0.0386(12) 0.0466(15) 0.0065(11) -0.0014(11) 0.0065(10) C32 0.0424(14) 0.0443(14) 0.0432(14) 0.0023(12) -0.0081(11) 0.0061(11) C33 0.0382(13) 0.0404(13) 0.0455(15) -0.0023(11) -0.0068(11) -0.0002(10) N33 0.0360(10) 0.0307(10) 0.0468(12) -0.0001(9) -0.0049(9) -0.0010(8) C34 0.0601(18) 0.0492(16) 0.0575(18) 0.0074(14) -0.0086(15) 0.0202(14) C35 0.075(2) 0.0537(17) 0.0559(19) -0.0110(15) -0.0249(16) 0.0103(15) C36 0.0462(14) 0.0322(12) 0.0452(14) 0.0034(11) -0.0012(12) 0.0113(10) C37 0.0502(16) 0.0543(16) 0.0482(16) 0.0037(13) 0.0032(13) 0.0134(13) C38 0.068(2) 0.063(2) 0.058(2) -0.0014(16) 0.0125(16) 0.0221(16) C39 0.092(3) 0.0512(18) 0.060(2) -0.0099(16) 0.0065(19) 0.0224(17) C40 0.083(2) 0.0343(14) 0.063(2) -0.0041(14) 0.0053(17) 0.0061(14) C41 0.0620(17) 0.0315(12) 0.0493(16) 0.0021(11) 0.0023(13) 0.0039(11) C42 0.0570(18) 0.066(2) 0.061(2) 0.0019(16) 0.0109(16) 0.0015(15) C43 0.113(4) 0.101(3) 0.075(3) 0.017(3) 0.018(3) -0.029(3) C44 0.095(4) 0.145(5) 0.140(5) 0.066(4) -0.045(3) -0.045(3) C45 0.069(2) 0.0409(15) 0.063(2) -0.0070(14) 0.0114(16) -0.0121(13) C46 0.069(2) 0.0566(19) 0.080(3) 0.0036(18) 0.0088(19) -0.0022(16) C47 0.097(3) 0.122(4) 0.078(3) 0.034(3) 0.008(2) -0.021(3) C48 0.0381(13) 0.0329(12) 0.0481(15) -0.0036(11) -0.0102(11) -0.0052(10) C49 0.0470(15) 0.0341(12) 0.0519(16) -0.0027(12) -0.0055(12) 0.0007(11) C50 0.0560(17) 0.0347(13) 0.066(2) -0.0032(13) -0.0090(15) 0.0020(12) C51 0.0584(18) 0.0299(13) 0.078(2) -0.0004(14) -0.0125(16) -0.0110(12) C52 0.0494(16) 0.0415(15) 0.082(2) 0.0055(15) -0.0065(16) -0.0158(13) C53 0.0389(14) 0.0383(13) 0.0666(19) 0.0003(13) -0.0088(13) -0.0095(11) C54 0.0537(16) 0.0352(13) 0.0607(18) 0.0004(13) 0.0060(14) 0.0045(11) C55 0.077(2) 0.066(2) 0.060(2) -0.0089(17) 0.0086(17) 0.0039(17) C56 0.0478(16) 0.0622(19) 0.070(2) -0.0132(16) 0.0098(15) -0.0099(14) C57 0.0431(15) 0.0495(16) 0.098(3) -0.0006(17) 0.0120(17) -0.0115(13) C58 0.064(2) 0.077(2) 0.105(3) -0.005(2) 0.026(2) -0.0159(19) C59 0.0428(17) 0.075(2) 0.130(4) 0.020(2) 0.003(2) -0.0007(16) C60 0.0431(14) 0.0342(12) 0.0493(15) 0.0060(11) -0.0088(12) 0.0026(11) O60 0.0474(10) 0.0405(10) 0.0662(14) 0.0151(9) -0.0047(10) -0.0079(8) C61 0.0424(13) 0.0400(13) 0.0426(14) 0.0058(11) 0.0001(11) -0.0059(11) O61 0.0464(10) 0.0455(10) 0.0492(11) 0.0129(9) -0.0030(9) 0.0000(8) C62 0.072(2) 0.0437(15) 0.0461(17) 0.0090(14) -0.0049(15) 0.0028(14) O62 0.130(2) 0.0546(14) 0.0540(14) -0.0014(12) 0.0062(15) 0.0097(14) O63 0.0443(10) 0.0398(9) 0.0564(12) 0.0111(9) 0.0059(9) 0.0014(8) C63 0.070(2) 0.0368(14) 0.0576(19) 0.0045(13) 0.0186(16) 0.0032(13) O64 0.0460(10) 0.0431(10) 0.0553(12) 0.0127(9) -0.0031(9) -0.0065(8) C64 0.073(2) 0.0395(14) 0.0464(16) 0.0048(12) -0.0085(15) -0.0074(13) N71 0.0380(11) 0.0345(10) 0.0433(12) 0.0056(9) 0.0043(9) 0.0034(8) C71 0.0361(13) 0.0372(13) 0.0567(17) 0.0083(12) 0.0044(12) 0.0030(10) C72 0.0503(15) 0.0415(14) 0.0477(16) 0.0144(12) -0.0031(12) 0.0024(11) C73 0.0447(14) 0.0490(15) 0.0450(15) 0.0111(12) -0.0001(12) 0.0052(11) N73 0.0402(11) 0.0403(11) 0.0431(12) 0.0026(10) 0.0007(9) 0.0043(9) C74 0.0624(18) 0.0386(14) 0.066(2) 0.0108(14) -0.0004(16) -0.0035(12) C75 0.083(2) 0.0589(19) 0.0484(18) 0.0113(15) -0.0124(17) 0.0008(16) C76 0.0517(15) 0.0295(11) 0.0488(15) 0.0040(11) 0.0013(12) -0.0021(10) C77 0.0538(17) 0.0422(14) 0.0633(19) 0.0055(14) -0.0083(15) -0.0044(12) C78 0.075(2) 0.0462(16) 0.072(2) 0.0047(16) -0.0206(19) -0.0091(15) C79 0.101(3) 0.0430(16) 0.059(2) -0.0051(15) -0.016(2) -0.0094(17) C80 0.100(3) 0.0370(14) 0.0531(18) -0.0053(13) 0.0111(18) -0.0094(16) C81 0.0665(18) 0.0311(12) 0.0540(17) 0.0004(12) 0.0102(14) -0.0020(12) C82 0.0418(16) 0.072(2) 0.079(2) 0.0059(19) -0.0035(16) 0.0005(14) C83 0.0510(19) 0.070(2) 0.123(4) 0.000(2) 0.007(2) 0.0040(17) C84 0.067(2) 0.092(3) 0.123(4) 0.023(3) 0.012(3) -0.011(2) C85 0.068(2) 0.0463(16) 0.065(2) -0.0081(15) 0.0209(16) -0.0014(14) C86 0.070(2) 0.071(2) 0.095(3) 0.011(2) 0.020(2) 0.0127(18) C87 0.090(3) 0.063(2) 0.090(3) -0.007(2) 0.044(2) -0.0005(19) C88 0.0465(14) 0.0442(14) 0.0408(14) 0.0032(12) 0.0021(12) 0.0068(11) C89 0.0528(16) 0.0416(14) 0.0437(15) 0.0043(12) -0.0020(12) 0.0036(11) C90 0.0631(18) 0.0452(15) 0.0497(17) 0.0035(13) -0.0009(14) 0.0021(13) C91 0.086(2) 0.0497(16) 0.0417(16) -0.0038(13) -0.0008(16) 0.0134(16) C92 0.0624(19) 0.0630(19) 0.0484(17) -0.0041(15) 0.0071(15) 0.0186(15) C93 0.0523(16) 0.0617(18) 0.0415(15) 0.0000(13) 0.0045(13) 0.0119(13) C94 0.0501(16) 0.0481(16) 0.0603(19) -0.0007(14) 0.0028(14) -0.0033(12) C95 0.059(2) 0.089(3) 0.078(3) 0.000(2) -0.0037(19) 0.0167(19) C96 0.063(2) 0.0601(19) 0.083(3) 0.0032(18) 0.0148(18) -0.0082(16) C97 0.0499(17) 0.085(2) 0.069(2) -0.0155(19) 0.0141(16) 0.0067(16) C98 0.066(3) 0.136(4) 0.104(4) -0.008(3) -0.023(2) 0.010(3) C99 0.079(3) 0.145(5) 0.100(4) -0.028(3) 0.042(3) -0.024(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cr1 C61 1.758(3) . ? Cr1 C60 1.766(3) . ? Cr1 C62 1.884(3) . ? Cr1 C64 2.104(3) . ? Cr1 C63 2.109(3) . ? Cr1 O64 2.1154(19) . ? Cr1 O63 2.1645(19) . ? Cr1 Mg3 3.0633(9) . ? Mg1 O60 1.984(2) . ? Mg1 N1 2.034(2) . ? Mg1 N3 2.034(2) . ? Mg1 Mg2 3.5844(11) . ? Mg2 O61 1.993(2) . ? Mg2 N31 2.037(2) . ? Mg2 N33 2.041(2) . ? Mg3 O63 1.986(2) . ? Mg3 O64 1.992(2) . ? Mg3 N73 2.022(2) . ? Mg3 N71 2.039(2) . ? Mg3 C63 2.668(3) . ? Mg3 C64 2.671(3) . ? N1 C1 1.334(3) . ? N1 C6 1.440(3) . ? C1 C2 1.404(4) . ? C1 C4 1.506(4) . ? C2 C3 1.404(4) . ? C3 N3 1.320(4) . ? C3 C5 1.524(4) . ? N3 C18 1.441(4) . ? C6 C11 1.399(4) . ? C6 C7 1.409(4) . ? C7 C8 1.399(5) . ? C7 C12 1.512(5) . ? C8 C9 1.368(5) . ? C9 C10 1.378(5) . ? C10 C11 1.391(4) . ? C11 C15 1.523(4) . ? C12 C14 1.509(6) . ? C12 C13 1.519(6) . ? C15 C17 1.510(5) . ? C15 C16 1.530(5) . ? C18 C19 1.391(5) . ? C18 C23 1.418(4) . ? C19 C20 1.404(5) . ? C19 C24 1.516(5) . ? C20 C21 1.378(5) . ? C21 C22 1.369(5) . ? C22 C23 1.403(5) . ? C23 C27 1.515(5) . ? C24 C26 1.511(5) . ? C24 C25 1.517(5) . ? C27 C28 1.529(5) . ? C27 C29 1.536(6) . ? N31 C31 1.324(3) . ? N31 C36 1.444(3) . ? C31 C32 1.410(4) . ? C31 C34 1.514(4) . ? C32 C33 1.406(4) . ? C33 N33 1.327(3) . ? C33 C35 1.517(4) . ? N33 C48 1.448(3) . ? C36 C41 1.402(4) . ? C36 C37 1.407(4) . ? C37 C38 1.393(5) . ? C37 C42 1.525(5) . ? C38 C39 1.373(5) . ? C39 C40 1.378(5) . ? C40 C41 1.402(4) . ? C41 C45 1.513(4) . ? C42 C44 1.489(6) . ? C42 C43 1.505(5) . ? C45 C46 1.524(5) . ? C45 C47 1.546(6) . ? C48 C53 1.397(4) . ? C48 C49 1.399(4) . ? C49 C50 1.393(4) . ? C49 C54 1.515(4) . ? C50 C51 1.375(5) . ? C51 C52 1.372(5) . ? C52 C53 1.396(4) . ? C53 C57 1.515(5) . ? C54 C56 1.522(5) . ? C54 C55 1.530(4) . ? C57 C59 1.526(5) . ? C57 C58 1.538(6) . ? C60 O60 1.197(3) . ? C61 O61 1.211(3) . ? C62 O62 1.149(4) . ? O63 C63 1.355(4) . ? C63 C64 1.369(5) . ? O64 C64 1.361(4) . ? N71 C71 1.327(3) . ? N71 C76 1.440(4) . ? C71 C72 1.400(4) . ? C71 C74 1.515(4) . ? C72 C73 1.406(4) . ? C73 N73 1.330(4) . ? C73 C75 1.513(4) . ? N73 C88 1.443(4) . ? C76 C81 1.404(4) . ? C76 C77 1.408(4) . ? C77 C78 1.398(5) . ? C77 C82 1.523(5) . ? C78 C79 1.361(6) . ? C79 C80 1.380(6) . ? C80 C81 1.394(5) . ? C81 C85 1.522(5) . ? C82 C84 1.530(5) . ? C82 C83 1.539(5) . ? C85 C87 1.520(5) . ? C85 C86 1.528(5) . ? C88 C89 1.405(4) . ? C88 C93 1.412(4) . ? C89 C90 1.394(4) . ? C89 C94 1.516(4) . ? C90 C91 1.377(5) . ? C91 C92 1.371(5) . ? C92 C93 1.391(5) . ? C93 C97 1.516(5) . ? C94 C95 1.530(5) . ? C94 C96 1.530(5) . ? C97 C98 1.528(6) . ? C97 C99 1.532(5) . ? C101 C102 1.507(10) . ? C102 C103 1.496(10) . ? C103 C104 1.501(10) . ? C104 C105 1.505(10) . ? C105 C106 1.492(10) . ? C111 C112 1.492(10) . ? C112 C113 1.489(10) . ? C113 C114 1.484(10) . ? C114 C115 1.501(10) . ? C115 C116 1.518(10) . ? C121 C122 1.503(10) . ? C122 C123 1.522(10) . ? C123 C124 1.508(10) . ? C124 C125 1.496(10) . ? C125 C126 1.509(10) . ? C131 C132 1.522(9) . ? C132 C133 1.513(9) . ? C133 C134 1.512(9) . ? C134 C135 1.506(9) . ? C135 C136 1.468(10) . ? C141 C142 1.487(9) . ? C142 C143 1.508(10) . ? C143 C144 1.540(10) . ? C144 C145 1.482(10) . ? C145 C146 1.503(10) . ? C151 C152 1.487(10) . ? C152 C153 1.502(10) . ? C153 C154 1.510(10) . ? C154 C155 1.502(10) . ? C155 C156 1.496(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C61 Cr1 C60 79.82(12) . . ? C61 Cr1 C62 88.67(13) . . ? C60 Cr1 C62 93.66(14) . . ? C61 Cr1 C64 98.49(12) . . ? C60 Cr1 C64 123.97(13) . . ? C62 Cr1 C64 142.35(14) . . ? C61 Cr1 C63 123.45(13) . . ? C60 Cr1 C63 97.39(13) . . ? C62 Cr1 C63 147.36(13) . . ? C64 Cr1 C63 37.93(13) . . ? C61 Cr1 O64 102.22(10) . . ? C60 Cr1 O64 161.51(11) . . ? C62 Cr1 O64 104.72(12) . . ? C64 Cr1 O64 37.63(11) . . ? C63 Cr1 O64 65.94(10) . . ? C61 Cr1 O63 160.38(11) . . ? C60 Cr1 O63 99.52(10) . . ? C62 Cr1 O63 110.91(11) . . ? C64 Cr1 O63 65.39(10) . . ? C63 Cr1 O63 36.95(11) . . ? O64 Cr1 O63 72.32(7) . . ? C61 Cr1 Mg3 141.45(9) . . ? C60 Cr1 Mg3 138.26(8) . . ? C62 Cr1 Mg3 93.31(9) . . ? C64 Cr1 Mg3 58.80(8) . . ? C63 Cr1 Mg3 58.70(9) . . ? O64 Cr1 Mg3 40.25(5) . . ? O63 Cr1 Mg3 40.22(5) . . ? O60 Mg1 N1 124.43(9) . . ? O60 Mg1 N3 100.91(10) . . ? N1 Mg1 N3 94.08(10) . . ? O60 Mg1 Mg2 88.64(6) . . ? N1 Mg1 Mg2 119.73(7) . . ? N3 Mg1 Mg2 130.90(8) . . ? O61 Mg2 N31 123.72(9) . . ? O61 Mg2 N33 102.36(9) . . ? N31 Mg2 N33 94.57(9) . . ? O61 Mg2 Mg1 87.83(6) . . ? N31 Mg2 Mg1 119.98(7) . . ? N33 Mg2 Mg1 130.14(7) . . ? O63 Mg3 O64 78.84(8) . . ? O63 Mg3 N73 117.65(10) . . ? O64 Mg3 N73 136.63(10) . . ? O63 Mg3 N71 124.12(9) . . ? O64 Mg3 N71 107.15(9) . . ? N73 Mg3 N71 95.85(10) . . ? O63 Mg3 C63 29.46(9) . . ? O64 Mg3 C63 56.91(9) . . ? N73 Mg3 C63 146.98(11) . . ? N71 Mg3 C63 108.32(10) . . ? O63 Mg3 C64 57.13(9) . . ? O64 Mg3 C64 29.63(10) . . ? N73 Mg3 C64 161.26(10) . . ? N71 Mg3 C64 101.48(10) . . ? C63 Mg3 C64 29.72(10) . . ? O63 Mg3 Cr1 44.74(6) . . ? O64 Mg3 Cr1 43.33(6) . . ? N73 Mg3 Cr1 119.97(7) . . ? N71 Mg3 Cr1 143.85(8) . . ? C63 Mg3 Cr1 42.48(6) . . ? C64 Mg3 Cr1 42.37(6) . . ? C1 N1 C6 118.8(2) . . ? C1 N1 Mg1 121.1(2) . . ? C6 N1 Mg1 120.02(15) . . ? N1 C1 C2 124.3(3) . . ? N1 C1 C4 120.0(3) . . ? C2 C1 C4 115.7(2) . . ? C1 C2 C3 129.6(2) . . ? N3 C3 C2 124.1(3) . . ? N3 C3 C5 120.0(3) . . ? C2 C3 C5 115.9(3) . . ? C3 N3 C18 119.8(2) . . ? C3 N3 Mg1 121.5(2) . . ? C18 N3 Mg1 118.55(17) . . ? C11 C6 C7 120.7(3) . . ? C11 C6 N1 119.9(2) . . ? C7 C6 N1 119.3(3) . . ? C8 C7 C6 117.9(3) . . ? C8 C7 C12 120.2(3) . . ? C6 C7 C12 122.0(3) . . ? C9 C8 C7 121.9(3) . . ? C8 C9 C10 119.3(3) . . ? C9 C10 C11 121.7(3) . . ? C10 C11 C6 118.5(3) . . ? C10 C11 C15 119.1(3) . . ? C6 C11 C15 122.5(3) . . ? C14 C12 C7 111.6(4) . . ? C14 C12 C13 110.5(4) . . ? C7 C12 C13 111.9(3) . . ? C17 C15 C11 111.7(2) . . ? C17 C15 C16 108.3(3) . . ? C11 C15 C16 110.8(3) . . ? C19 C18 C23 121.1(3) . . ? C19 C18 N3 120.1(3) . . ? C23 C18 N3 118.6(3) . . ? C18 C19 C20 118.6(3) . . ? C18 C19 C24 121.9(3) . . ? C20 C19 C24 119.5(3) . . ? C21 C20 C19 120.9(4) . . ? C22 C21 C20 120.2(3) . . ? C21 C22 C23 121.5(3) . . ? C22 C23 C18 117.7(3) . . ? C22 C23 C27 119.5(3) . . ? C18 C23 C27 122.9(3) . . ? C26 C24 C19 113.7(3) . . ? C26 C24 C25 109.5(3) . . ? C19 C24 C25 111.0(3) . . ? C23 C27 C28 111.8(3) . . ? C23 C27 C29 111.8(4) . . ? C28 C27 C29 109.4(3) . . ? C31 N31 C36 118.1(2) . . ? C31 N31 Mg2 120.55(17) . . ? C36 N31 Mg2 121.34(16) . . ? N31 C31 C32 125.2(2) . . ? N31 C31 C34 120.7(2) . . ? C32 C31 C34 114.1(2) . . ? C33 C32 C31 129.3(3) . . ? N33 C33 C32 124.3(2) . . ? N33 C33 C35 120.2(2) . . ? C32 C33 C35 115.5(3) . . ? C33 N33 C48 116.4(2) . . ? C33 N33 Mg2 120.86(17) . . ? C48 N33 Mg2 122.62(17) . . ? C41 C36 C37 120.9(3) . . ? C41 C36 N31 120.6(2) . . ? C37 C36 N31 118.4(2) . . ? C38 C37 C36 118.2(3) . . ? C38 C37 C42 120.1(3) . . ? C36 C37 C42 121.7(3) . . ? C39 C38 C37 121.5(3) . . ? C38 C39 C40 120.0(3) . . ? C39 C40 C41 121.1(3) . . ? C40 C41 C36 118.2(3) . . ? C40 C41 C45 118.9(3) . . ? C36 C41 C45 122.9(3) . . ? C44 C42 C43 111.2(4) . . ? C44 C42 C37 112.7(3) . . ? C43 C42 C37 113.7(3) . . ? C41 C45 C46 112.6(3) . . ? C41 C45 C47 111.9(3) . . ? C46 C45 C47 108.7(3) . . ? C53 C48 C49 121.0(2) . . ? C53 C48 N33 118.4(2) . . ? C49 C48 N33 120.6(2) . . ? C50 C49 C48 118.3(3) . . ? C50 C49 C54 120.4(3) . . ? C48 C49 C54 121.2(2) . . ? C51 C50 C49 121.4(3) . . ? C52 C51 C50 119.5(3) . . ? C51 C52 C53 121.6(3) . . ? C52 C53 C48 118.0(3) . . ? C52 C53 C57 120.1(3) . . ? C48 C53 C57 121.8(3) . . ? C49 C54 C56 109.1(3) . . ? C49 C54 C55 114.3(3) . . ? C56 C54 C55 110.6(3) . . ? C53 C57 C59 111.8(3) . . ? C53 C57 C58 112.5(3) . . ? C59 C57 C58 111.0(3) . . ? O60 C60 Cr1 172.9(2) . . ? C60 O60 Mg1 143.36(19) . . ? O61 C61 Cr1 173.9(2) . . ? C61 O61 Mg2 136.6(2) . . ? O62 C62 Cr1 173.1(3) . . ? C63 O63 Mg3 104.42(17) . . ? C63 O63 Cr1 69.29(14) . . ? Mg3 O63 Cr1 95.05(8) . . ? O63 C63 C64 115.7(3) . . ? O63 C63 Cr1 73.77(16) . . ? C64 C63 Cr1 70.86(18) . . ? O63 C63 Mg3 46.12(12) . . ? C64 C63 Mg3 75.25(19) . . ? Cr1 C63 Mg3 78.82(10) . . ? C64 O64 Mg3 104.02(18) . . ? C64 O64 Cr1 70.75(15) . . ? Mg3 O64 Cr1 96.41(8) . . ? O64 C64 C63 114.7(3) . . ? O64 C64 Cr1 71.63(16) . . ? C63 C64 Cr1 71.21(18) . . ? O64 C64 Mg3 46.36(13) . . ? C63 C64 Mg3 75.03(19) . . ? Cr1 C64 Mg3 78.83(10) . . ? C71 N71 C76 119.4(2) . . ? C71 N71 Mg3 121.73(19) . . ? C76 N71 Mg3 118.73(16) . . ? N71 C71 C72 124.3(2) . . ? N71 C71 C74 119.9(3) . . ? C72 C71 C74 115.8(2) . . ? C71 C72 C73 130.8(2) . . ? N73 C73 C72 124.6(3) . . ? N73 C73 C75 119.3(3) . . ? C72 C73 C75 116.1(3) . . ? C73 N73 C88 119.8(2) . . ? C73 N73 Mg3 121.6(2) . . ? C88 N73 Mg3 118.61(17) . . ? C81 C76 C77 120.9(3) . . ? C81 C76 N71 119.1(3) . . ? C77 C76 N71 119.9(3) . . ? C78 C77 C76 118.1(3) . . ? C78 C77 C82 119.8(3) . . ? C76 C77 C82 122.1(3) . . ? C79 C78 C77 121.8(3) . . ? C78 C79 C80 119.5(3) . . ? C79 C80 C81 122.0(3) . . ? C80 C81 C76 117.7(3) . . ? C80 C81 C85 120.9(3) . . ? C76 C81 C85 121.4(3) . . ? C77 C82 C84 112.7(3) . . ? C77 C82 C83 110.1(3) . . ? C84 C82 C83 109.8(3) . . ? C87 C85 C81 113.2(3) . . ? C87 C85 C86 109.7(3) . . ? C81 C85 C86 111.6(3) . . ? C89 C88 C93 120.9(3) . . ? C89 C88 N73 120.5(2) . . ? C93 C88 N73 118.5(3) . . ? C90 C89 C88 118.1(3) . . ? C90 C89 C94 119.0(3) . . ? C88 C89 C94 122.9(3) . . ? C91 C90 C89 121.6(3) . . ? C92 C91 C90 119.6(3) . . ? C91 C92 C93 122.0(3) . . ? C92 C93 C88 117.8(3) . . ? C92 C93 C97 120.6(3) . . ? C88 C93 C97 121.5(3) . . ? C89 C94 C95 110.8(3) . . ? C89 C94 C96 112.5(3) . . ? C95 C94 C96 109.9(3) . . ? C93 C97 C98 110.4(4) . . ? C93 C97 C99 111.6(3) . . ? C98 C97 C99 110.8(4) . . ? C103 C102 C101 106.6(13) . . ? C102 C103 C104 111.5(14) . . ? C103 C104 C105 108.5(13) . . ? C106 C105 C104 114.4(14) . . ? C113 C112 C111 113.4(14) . . ? C114 C113 C112 113.2(14) . . ? C113 C114 C115 114.7(14) . . ? C114 C115 C116 105.9(14) . . ? C121 C122 C123 103.8(13) . . ? C124 C123 C122 107.8(12) . . ? C125 C124 C123 110.5(13) . . ? C124 C125 C126 110.7(14) . . ? C133 C132 C131 114.6(11) . . ? C134 C133 C132 110.1(11) . . ? C135 C134 C133 114.9(12) . . ? C136 C135 C134 119.2(14) . . ? C141 C142 C143 116.6(12) . . ? C142 C143 C144 104.6(11) . . ? C145 C144 C143 109.4(12) . . ? C144 C145 C146 113.1(13) . . ? C151 C152 C153 113.8(16) . . ? C152 C153 C154 110.5(15) . . ? C155 C154 C153 109.8(15) . . ? C156 C155 C154 112.3(16) . . ? _refine_diff_density_max 0.361 _refine_diff_density_min -0.337 _refine_diff_density_rms 0.046 _shelx_res_file ; TITL MRC2160 in P2(1)/c MRC2160.res created by SHELXL-2018/3 at 14:15:06 on 05-Aug-2021 REM P2(1)/c (#14 in standard setting) REM JMP223 CELL 1.54184 19.433017 17.404892 30.893112 90.0000 96.4115 90.0000 ZERR 4.00 0.000240 0.000178 0.000438 0.0000 0.0012 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H Cr Mg N O UNIT 416 616 4 12 24 20 TEMP -100 L.S. 6 OMIT 20 10 1 FMAP 2 PLAN 10 ACTA REM 'C92 H126 Cr Mg3 N6 O5, 2(C6 H14)' REM C104 H154 Cr Mg3 N6 O5 RTAB MG-H MG1 H1 RTAB MG-H MG2 H1 RTAB MHM MG1 H1 MG2 REM C63 and C64 protons located from delta-F map and then added in idealised REM positions. DFIX 1.50 0.01 C101 C102 C102 C103 C103 C104 C104 C105 C105 C106 = C111 C112 C112 C113 C113 C114 C114 C115 C115 C116 = C121 C122 C122 C123 C123 C124 C124 C125 C125 C126 DFIX 2.46 0.02 C101 C103 C102 C104 C103 C105 C104 C106 = C111 C113 C112 C114 C113 C115 C114 C116 = C121 C123 C122 C124 C123 C125 C124 C126 SIMU 0.02 0.02 2 C101 > C126 SUMP 1 0 1 2 1 3 1 4 DFIX 1.50 0.01 C131 C132 C132 C133 C133 C134 C134 C135 C135 C136 = C141 C142 C142 C143 C143 C144 C144 C145 C145 C146 = C151 C152 C152 C153 C153 C154 C154 C155 C155 C156 DFIX 2.46 0.02 C131 C133 C132 C134 C133 C135 C134 C136 = C141 C143 C142 C144 C143 C145 C144 C146 = C151 C153 C152 C154 C153 C155 C154 C156 SIMU 0.02 0.02 2 C131 > C156 SUMP 1 0 1 5 1 6 1 7 WGHT 0.074800 FVAR 1.24766 0.38518 0.32240 0.29241 0.46786 0.37091 0.16122 CR1 3 0.784593 0.651958 0.398050 11.00000 0.04336 0.03291 = 0.04088 0.00800 -0.00308 -0.00251 MG1 4 0.887626 0.856150 0.332294 11.00000 0.03512 0.02961 = 0.04032 0.00104 -0.00409 -0.00478 MG2 4 0.710287 0.823648 0.290894 11.00000 0.03322 0.02676 = 0.04067 0.00305 -0.00509 0.00112 MG3 4 0.779547 0.497172 0.444790 11.00000 0.04167 0.03249 = 0.04209 0.00674 0.00366 0.00123 H1 2 0.798838 0.856025 0.303973 11.00000 0.02099 N1 5 0.958246 0.880414 0.290381 11.00000 0.03431 0.03071 = 0.04693 0.00188 -0.00194 -0.00329 C1 1 0.996110 0.944478 0.294539 11.00000 0.03846 0.03902 = 0.05761 0.00371 -0.00250 -0.01019 C2 1 0.996514 0.995970 0.329530 11.00000 0.05456 0.03443 = 0.05934 -0.00044 -0.00772 -0.01575 AFIX 43 H2A 2 1.017424 1.044330 0.325300 11.00000 -1.20000 AFIX 0 C3 1 0.970628 0.986662 0.369839 11.00000 0.05885 0.03056 = 0.05150 0.00000 -0.01342 -0.00674 N3 5 0.930625 0.929092 0.379195 11.00000 0.04867 0.03536 = 0.04298 0.00039 -0.00939 -0.00429 C4 1 1.043266 0.964677 0.260726 11.00000 0.06402 0.06236 = 0.07901 -0.00405 0.02020 -0.02809 AFIX 137 H4A 2 1.084814 0.932414 0.264809 11.00000 -1.50000 H4B 2 1.056634 1.018866 0.263772 11.00000 -1.50000 H4C 2 1.019033 0.955896 0.231594 11.00000 -1.50000 AFIX 0 C5 1 0.993590 1.046570 0.404431 11.00000 0.09433 0.05217 = 0.06121 -0.00768 -0.00797 -0.02536 AFIX 137 H5A 2 0.959431 1.049531 0.425432 11.00000 -1.50000 H5B 2 0.997415 1.096768 0.390531 11.00000 -1.50000 H5C 2 1.038691 1.031940 0.419579 11.00000 -1.50000 AFIX 0 C6 1 0.965396 0.830226 0.254091 11.00000 0.03603 0.03202 = 0.05219 -0.00105 0.00812 -0.00685 C7 1 1.010287 0.766596 0.259956 11.00000 0.03846 0.03993 = 0.07383 -0.00064 0.00469 -0.00079 C8 1 1.015921 0.718800 0.224099 11.00000 0.04614 0.04193 = 0.09295 -0.00836 0.01892 0.00486 AFIX 43 H8A 2 1.046537 0.676118 0.227306 11.00000 -1.20000 AFIX 0 C9 1 0.978597 0.731785 0.184555 11.00000 0.06217 0.04920 = 0.06622 -0.01124 0.02179 -0.00261 AFIX 43 H9A 2 0.983790 0.698951 0.160570 11.00000 -1.20000 AFIX 0 C10 1 0.933388 0.792992 0.179876 11.00000 0.06671 0.04427 = 0.05146 -0.00499 0.01358 -0.00375 AFIX 43 H10A 2 0.906825 0.801268 0.152551 11.00000 -1.20000 AFIX 0 C11 1 0.925654 0.842965 0.214138 11.00000 0.04693 0.03907 = 0.04702 0.00033 0.00845 -0.00500 C12 1 1.051147 0.749021 0.303402 11.00000 0.05746 0.05383 = 0.09077 -0.00357 -0.01482 0.01603 AFIX 13 H12A 2 1.036547 0.786653 0.325070 11.00000 -1.20000 AFIX 0 C13 1 1.035829 0.668986 0.319456 11.00000 0.13808 0.06279 = 0.10411 0.01708 -0.03560 0.01294 AFIX 137 H13A 2 1.046670 0.630889 0.297863 11.00000 -1.50000 H13B 2 0.986714 0.665282 0.323707 11.00000 -1.50000 H13C 2 1.064223 0.659158 0.347153 11.00000 -1.50000 AFIX 0 C14 1 1.127924 0.759216 0.301723 11.00000 0.06688 0.17826 = 0.20111 0.02588 -0.04618 -0.00470 AFIX 137 H14A 2 1.143761 0.723258 0.280523 11.00000 -1.50000 H14B 2 1.152632 0.749012 0.330564 11.00000 -1.50000 H14C 2 1.137236 0.812001 0.292993 11.00000 -1.50000 AFIX 0 C15 1 0.874088 0.908895 0.206998 11.00000 0.06517 0.03810 = 0.04426 -0.00034 -0.00239 0.00264 AFIX 13 H15A 2 0.874168 0.938064 0.234892 11.00000 -1.20000 AFIX 0 C16 1 0.894326 0.963670 0.171824 11.00000 0.09627 0.06028 = 0.10322 0.03470 0.01149 0.00375 AFIX 137 H16A 2 0.941808 0.981809 0.179731 11.00000 -1.50000 H16B 2 0.862657 1.007663 0.169349 11.00000 -1.50000 H16C 2 0.891480 0.936629 0.143856 11.00000 -1.50000 AFIX 0 C17 1 0.801565 0.880219 0.193352 11.00000 0.05640 0.06218 = 0.06189 -0.01057 0.00302 0.00787 AFIX 137 H17A 2 0.800913 0.850909 0.166224 11.00000 -1.50000 H17B 2 0.769960 0.924070 0.188751 11.00000 -1.50000 H17C 2 0.786756 0.847070 0.216224 11.00000 -1.50000 AFIX 0 C18 1 0.921019 0.913418 0.423918 11.00000 0.06392 0.03294 = 0.04256 -0.00083 -0.01350 -0.00807 C19 1 0.857893 0.929458 0.439194 11.00000 0.07146 0.04435 = 0.04229 -0.00338 -0.00621 0.00114 C20 1 0.848322 0.907661 0.481856 11.00000 0.08893 0.05749 = 0.04291 -0.00428 0.00185 0.00418 AFIX 43 H20A 2 0.805603 0.918563 0.492813 11.00000 -1.20000 AFIX 0 C21 1 0.900061 0.870656 0.508063 11.00000 0.10317 0.05024 = 0.04067 0.00093 -0.00651 -0.00911 AFIX 43 H21A 2 0.892552 0.855645 0.536726 11.00000 -1.20000 AFIX 0 C22 1 0.962238 0.855451 0.492942 11.00000 0.08871 0.04735 = 0.04733 0.00388 -0.02385 -0.00575 AFIX 43 H22A 2 0.997596 0.830461 0.511516 11.00000 -1.20000 AFIX 0 C23 1 0.974912 0.875945 0.450632 11.00000 0.06322 0.04212 = 0.05388 0.00283 -0.01845 -0.00734 C24 1 0.799891 0.970129 0.411303 11.00000 0.07288 0.05823 = 0.04909 -0.00094 -0.00001 0.01265 AFIX 13 H24A 2 0.810457 0.967226 0.380399 11.00000 -1.20000 AFIX 0 C25 1 0.797034 1.054470 0.423353 11.00000 0.10629 0.05323 = 0.14640 0.00072 -0.03439 0.01161 AFIX 137 H25A 2 0.782876 1.059392 0.452695 11.00000 -1.50000 H25B 2 0.763478 1.080950 0.402455 11.00000 -1.50000 H25C 2 0.842902 1.077554 0.422693 11.00000 -1.50000 AFIX 0 C26 1 0.729549 0.934119 0.413253 11.00000 0.07468 0.07658 = 0.08917 -0.00121 -0.01733 0.00464 AFIX 137 H26A 2 0.732467 0.878685 0.408205 11.00000 -1.50000 H26B 2 0.696167 0.957023 0.390801 11.00000 -1.50000 H26C 2 0.714396 0.943296 0.442019 11.00000 -1.50000 AFIX 0 C27 1 1.044195 0.856836 0.435189 11.00000 0.05922 0.06170 = 0.07327 0.01330 -0.01845 -0.00412 AFIX 13 H27A 2 1.045772 0.881390 0.406052 11.00000 -1.20000 AFIX 0 C28 1 1.053510 0.770260 0.429804 11.00000 0.05994 0.07365 = 0.09676 0.00036 -0.01054 0.00635 AFIX 137 H28A 2 1.053534 0.744989 0.458154 11.00000 -1.50000 H28B 2 1.097595 0.760279 0.418229 11.00000 -1.50000 H28C 2 1.015372 0.750020 0.409578 11.00000 -1.50000 AFIX 0 C29 1 1.104864 0.888704 0.466136 11.00000 0.07460 0.10398 = 0.15235 -0.00439 -0.03767 -0.01731 AFIX 137 H29A 2 1.098885 0.944167 0.469708 11.00000 -1.50000 H29B 2 1.148439 0.878902 0.453904 11.00000 -1.50000 H29C 2 1.105972 0.863374 0.494536 11.00000 -1.50000 AFIX 0 N31 5 0.649397 0.913492 0.268290 11.00000 0.03637 0.03169 = 0.04267 0.00283 -0.00300 0.00489 C31 1 0.618032 0.913202 0.227973 11.00000 0.03443 0.03857 = 0.04663 0.00652 -0.00143 0.00652 C32 1 0.616952 0.850771 0.198814 11.00000 0.04240 0.04427 = 0.04320 0.00233 -0.00812 0.00614 AFIX 43 H32A 2 0.601242 0.862421 0.169318 11.00000 -1.20000 AFIX 0 C33 1 0.635800 0.773755 0.207153 11.00000 0.03823 0.04045 = 0.04547 -0.00227 -0.00677 -0.00015 N33 5 0.668303 0.748546 0.244522 11.00000 0.03601 0.03073 = 0.04680 -0.00006 -0.00492 -0.00098 C34 1 0.578481 0.983014 0.209583 11.00000 0.06013 0.04917 = 0.05748 0.00744 -0.00864 0.02021 AFIX 137 H34A 2 0.545280 0.998923 0.229504 11.00000 -1.50000 H34B 2 0.553583 0.970233 0.181146 11.00000 -1.50000 H34C 2 0.610979 1.025072 0.206194 11.00000 -1.50000 AFIX 0 C35 1 0.615550 0.718096 0.170128 11.00000 0.07460 0.05375 = 0.05586 -0.01099 -0.02488 0.01029 AFIX 137 H35A 2 0.657399 0.695962 0.160166 11.00000 -1.50000 H35B 2 0.589195 0.745453 0.145976 11.00000 -1.50000 H35C 2 0.586973 0.676915 0.180324 11.00000 -1.50000 AFIX 0 C36 1 0.639776 0.979471 0.295313 11.00000 0.04623 0.03223 = 0.04521 0.00341 -0.00121 0.01129 C37 1 0.588530 0.975888 0.324003 11.00000 0.05019 0.05434 = 0.04822 0.00366 0.00319 0.01338 C38 1 0.577602 1.040752 0.348777 11.00000 0.06826 0.06349 = 0.05831 -0.00144 0.01250 0.02213 AFIX 43 H38A 2 0.541686 1.040165 0.367264 11.00000 -1.20000 AFIX 0 C39 1 0.617588 1.105509 0.347068 11.00000 0.09158 0.05122 = 0.06049 -0.00994 0.00647 0.02245 AFIX 43 H39A 2 0.609195 1.149060 0.364257 11.00000 -1.20000 AFIX 0 C40 1 0.669869 1.107298 0.320421 11.00000 0.08260 0.03433 = 0.06262 -0.00412 0.00533 0.00606 AFIX 43 H40A 2 0.698045 1.151832 0.319969 11.00000 -1.20000 AFIX 0 C41 1 0.682163 1.044443 0.293953 11.00000 0.06199 0.03152 = 0.04928 0.00214 0.00233 0.00392 C42 1 0.545421 0.903645 0.328247 11.00000 0.05695 0.06611 = 0.06108 0.00194 0.01095 0.00147 AFIX 13 H42A 2 0.572017 0.860416 0.316765 11.00000 -1.20000 AFIX 0 C43 1 0.536288 0.883118 0.374585 11.00000 0.11258 0.10111 = 0.07533 0.01687 0.01842 -0.02875 AFIX 137 H43A 2 0.509753 0.923562 0.387280 11.00000 -1.50000 H43B 2 0.581812 0.878177 0.391521 11.00000 -1.50000 H43C 2 0.511352 0.834247 0.375127 11.00000 -1.50000 AFIX 0 C44 1 0.477571 0.906260 0.300616 11.00000 0.09532 0.14530 = 0.13961 0.06603 -0.04484 -0.04482 AFIX 137 H44A 2 0.451800 0.858887 0.304675 11.00000 -1.50000 H44B 2 0.485421 0.911124 0.269947 11.00000 -1.50000 H44C 2 0.450843 0.950490 0.309044 11.00000 -1.50000 AFIX 0 C45 1 0.739716 1.049835 0.264904 11.00000 0.06947 0.04091 = 0.06319 -0.00700 0.01143 -0.01208 AFIX 13 H45A 2 0.740869 1.000374 0.248530 11.00000 -1.20000 AFIX 0 C46 1 0.810558 1.061304 0.290612 11.00000 0.06869 0.05655 = 0.07958 0.00364 0.00883 -0.00223 AFIX 137 H46A 2 0.846241 1.061667 0.270564 11.00000 -1.50000 H46B 2 0.819711 1.019269 0.311570 11.00000 -1.50000 H46C 2 0.811286 1.110352 0.306236 11.00000 -1.50000 AFIX 0 C47 1 0.727116 1.115469 0.231224 11.00000 0.09703 0.12162 = 0.07796 0.03424 0.00829 -0.02118 AFIX 137 H47A 2 0.729697 1.165036 0.246368 11.00000 -1.50000 H47B 2 0.681166 1.109492 0.214961 11.00000 -1.50000 H47C 2 0.762498 1.113480 0.210997 11.00000 -1.50000 AFIX 0 C48 1 0.668650 0.666168 0.251185 11.00000 0.03808 0.03292 = 0.04811 -0.00356 -0.01017 -0.00518 C49 1 0.721595 0.620741 0.237570 11.00000 0.04700 0.03411 = 0.05187 -0.00272 -0.00554 0.00070 C50 1 0.717355 0.541342 0.242391 11.00000 0.05598 0.03468 = 0.06638 -0.00324 -0.00904 0.00201 AFIX 43 H50A 2 0.752584 0.509669 0.232939 11.00000 -1.20000 AFIX 0 C51 1 0.663250 0.507855 0.260544 11.00000 0.05842 0.02993 = 0.07815 -0.00039 -0.01249 -0.01099 AFIX 43 H51A 2 0.660581 0.453543 0.262916 11.00000 -1.20000 AFIX 0 C52 1 0.613145 0.553522 0.275204 11.00000 0.04937 0.04151 = 0.08154 0.00552 -0.00646 -0.01580 AFIX 43 H52A 2 0.576426 0.530203 0.288315 11.00000 -1.20000 AFIX 0 C53 1 0.614803 0.633410 0.271326 11.00000 0.03888 0.03833 = 0.06664 0.00027 -0.00878 -0.00947 C54 1 0.783893 0.656630 0.220031 11.00000 0.05365 0.03524 = 0.06070 0.00044 0.00602 0.00448 AFIX 13 H54A 2 0.771334 0.710674 0.211462 11.00000 -1.20000 AFIX 0 C55 1 0.806295 0.616191 0.179911 11.00000 0.07651 0.06554 = 0.05971 -0.00891 0.00858 0.00387 AFIX 137 H55A 2 0.823829 0.564808 0.188080 11.00000 -1.50000 H55B 2 0.842882 0.646131 0.168383 11.00000 -1.50000 H55C 2 0.766523 0.611738 0.157575 11.00000 -1.50000 AFIX 0 C56 1 0.843624 0.660081 0.256289 11.00000 0.04778 0.06218 = 0.06993 -0.01323 0.00978 -0.00991 AFIX 137 H56A 2 0.857732 0.607778 0.265041 11.00000 -1.50000 H56B 2 0.828805 0.687562 0.281340 11.00000 -1.50000 H56C 2 0.882804 0.687125 0.245839 11.00000 -1.50000 AFIX 0 C57 1 0.558830 0.681949 0.288163 11.00000 0.04314 0.04953 = 0.09832 -0.00064 0.01199 -0.01152 AFIX 13 H57A 2 0.577343 0.735468 0.291642 11.00000 -1.20000 AFIX 0 C58 1 0.541443 0.655630 0.333207 11.00000 0.06401 0.07742 = 0.10533 -0.00522 0.02617 -0.01591 AFIX 137 H58A 2 0.509215 0.692214 0.344195 11.00000 -1.50000 H58B 2 0.584023 0.653284 0.353406 11.00000 -1.50000 H58C 2 0.520013 0.604620 0.330722 11.00000 -1.50000 AFIX 0 C59 1 0.493762 0.685673 0.255665 11.00000 0.04284 0.07467 = 0.13035 0.01952 0.00319 -0.00069 AFIX 137 H59A 2 0.478051 0.633433 0.247956 11.00000 -1.50000 H59B 2 0.504166 0.712815 0.229374 11.00000 -1.50000 H59C 2 0.457271 0.713163 0.268790 11.00000 -1.50000 AFIX 0 C60 1 0.847541 0.715227 0.381306 11.00000 0.04314 0.03419 = 0.04934 0.00598 -0.00883 0.00261 O60 6 0.885412 0.759229 0.365884 11.00000 0.04741 0.04051 = 0.06617 0.01510 -0.00474 -0.00787 C61 1 0.730830 0.718603 0.367863 11.00000 0.04236 0.03998 = 0.04262 0.00576 0.00007 -0.00587 O61 6 0.699393 0.767661 0.345981 11.00000 0.04637 0.04546 = 0.04924 0.01294 -0.00301 -0.00004 C62 1 0.773374 0.708817 0.448686 11.00000 0.07227 0.04367 = 0.04613 0.00898 -0.00485 0.00278 O62 6 0.762951 0.748808 0.476804 11.00000 0.13016 0.05456 = 0.05396 -0.00145 0.00623 0.00975 O63 6 0.848795 0.551887 0.413501 11.00000 0.04431 0.03977 = 0.05641 0.01112 0.00592 0.00136 C63 1 0.821537 0.550656 0.371177 11.00000 0.06959 0.03678 = 0.05757 0.00454 0.01865 0.00319 AFIX 43 H63A 2 0.849740 0.549147 0.347976 11.00000 -1.20000 AFIX 0 O64 6 0.718196 0.556166 0.400706 11.00000 0.04602 0.04314 = 0.05530 0.01266 -0.00315 -0.00649 C64 1 0.750730 0.551728 0.363997 11.00000 0.07301 0.03954 = 0.04641 0.00481 -0.00852 -0.00736 AFIX 43 H64A 2 0.726250 0.549546 0.335633 11.00000 -1.20000 AFIX 0 N71 5 0.754998 0.383919 0.436092 11.00000 0.03804 0.03447 = 0.04327 0.00561 0.00426 0.00339 C71 1 0.761923 0.334346 0.468907 11.00000 0.03615 0.03717 = 0.05667 0.00830 0.00445 0.00302 C72 1 0.786376 0.353693 0.511885 11.00000 0.05027 0.04147 = 0.04767 0.01440 -0.00311 0.00238 AFIX 43 H72A 2 0.795198 0.311024 0.530871 11.00000 -1.20000 AFIX 0 C73 1 0.800057 0.425664 0.531646 11.00000 0.04475 0.04904 = 0.04499 0.01111 -0.00010 0.00522 N73 5 0.796701 0.492330 0.510494 11.00000 0.04017 0.04032 = 0.04315 0.00258 0.00067 0.00431 C74 1 0.740710 0.251260 0.461202 11.00000 0.06240 0.03861 = 0.06602 0.01081 -0.00045 -0.00347 AFIX 137 H74A 2 0.690860 0.246047 0.462860 11.00000 -1.50000 H74B 2 0.766113 0.218784 0.483465 11.00000 -1.50000 H74C 2 0.751438 0.235211 0.432298 11.00000 -1.50000 AFIX 0 C75 1 0.817773 0.425124 0.580605 11.00000 0.08253 0.05886 = 0.04838 0.01134 -0.01238 0.00080 AFIX 137 H75A 2 0.864385 0.446121 0.588048 11.00000 -1.50000 H75B 2 0.816203 0.372271 0.591388 11.00000 -1.50000 H75C 2 0.784204 0.456631 0.594086 11.00000 -1.50000 AFIX 0 C76 1 0.724754 0.358634 0.393799 11.00000 0.05167 0.02954 = 0.04883 0.00403 0.00132 -0.00205 C77 1 0.652230 0.355691 0.384248 11.00000 0.05385 0.04222 = 0.06334 0.00555 -0.00830 -0.00439 C78 1 0.625024 0.332935 0.342423 11.00000 0.07539 0.04617 = 0.07205 0.00466 -0.02056 -0.00908 AFIX 43 H78A 2 0.576199 0.330652 0.335463 11.00000 -1.20000 AFIX 0 C79 1 0.666558 0.313956 0.311389 11.00000 0.10095 0.04297 = 0.05925 -0.00512 -0.01596 -0.00942 AFIX 43 H79A 2 0.646862 0.297427 0.283410 11.00000 -1.20000 AFIX 0 C80 1 0.737491 0.318916 0.320892 11.00000 0.09996 0.03700 = 0.05307 -0.00527 0.01106 -0.00938 AFIX 43 H80A 2 0.766147 0.306527 0.298904 11.00000 -1.20000 AFIX 0 C81 1 0.768368 0.341575 0.361810 11.00000 0.06654 0.03114 = 0.05404 0.00036 0.01021 -0.00201 C82 1 0.603582 0.377733 0.417585 11.00000 0.04179 0.07214 = 0.07925 0.00589 -0.00346 0.00048 AFIX 13 H82A 2 0.632022 0.385507 0.446276 11.00000 -1.20000 AFIX 0 C83 1 0.566966 0.454028 0.404464 11.00000 0.05104 0.06960 = 0.12285 -0.00041 0.00675 0.00397 AFIX 137 H83A 2 0.601647 0.494469 0.402754 11.00000 -1.50000 H83B 2 0.536242 0.468076 0.426281 11.00000 -1.50000 H83C 2 0.539698 0.448111 0.376003 11.00000 -1.50000 AFIX 0 C84 1 0.549666 0.315557 0.423359 11.00000 0.06736 0.09167 = 0.12290 0.02294 0.01210 -0.01129 AFIX 137 H84A 2 0.519565 0.308907 0.395981 11.00000 -1.50000 H84B 2 0.521706 0.330976 0.446402 11.00000 -1.50000 H84C 2 0.573204 0.266975 0.431390 11.00000 -1.50000 AFIX 0 C85 1 0.846748 0.347029 0.371354 11.00000 0.06791 0.04630 = 0.06512 -0.00813 0.02087 -0.00140 AFIX 13 H85A 2 0.857046 0.386877 0.394491 11.00000 -1.20000 AFIX 0 C86 1 0.878282 0.271505 0.389256 11.00000 0.07013 0.07100 = 0.09530 0.01096 0.01954 0.01270 AFIX 137 H86A 2 0.861824 0.260440 0.417453 11.00000 -1.50000 H86B 2 0.928879 0.275815 0.392983 11.00000 -1.50000 H86C 2 0.864372 0.229808 0.368815 11.00000 -1.50000 AFIX 0 C87 1 0.882028 0.372103 0.332187 11.00000 0.09016 0.06266 = 0.09022 -0.00696 0.04394 -0.00046 AFIX 137 H87A 2 0.880788 0.329879 0.311129 11.00000 -1.50000 H87B 2 0.930264 0.385840 0.341677 11.00000 -1.50000 H87C 2 0.857781 0.416759 0.318500 11.00000 -1.50000 AFIX 0 C88 1 0.803360 0.563371 0.534651 11.00000 0.04654 0.04419 = 0.04078 0.00315 0.00206 0.00678 C89 1 0.866925 0.602642 0.540279 11.00000 0.05279 0.04161 = 0.04369 0.00431 -0.00202 0.00356 C90 1 0.869110 0.673886 0.560999 11.00000 0.06306 0.04523 = 0.04974 0.00351 -0.00087 0.00210 AFIX 43 H90A 2 0.911609 0.701320 0.564976 11.00000 -1.20000 AFIX 0 C91 1 0.811132 0.705468 0.575845 11.00000 0.08621 0.04970 = 0.04167 -0.00376 -0.00077 0.01341 AFIX 43 H91A 2 0.813645 0.754382 0.589576 11.00000 -1.20000 AFIX 0 C92 1 0.749792 0.665884 0.570684 11.00000 0.06235 0.06300 = 0.04842 -0.00409 0.00710 0.01855 AFIX 43 H92A 2 0.710216 0.687810 0.581357 11.00000 -1.20000 AFIX 0 C93 1 0.743744 0.594563 0.550285 11.00000 0.05230 0.06173 = 0.04149 -0.00001 0.00446 0.01186 C94 1 0.932796 0.570507 0.525317 11.00000 0.05007 0.04814 = 0.06025 -0.00068 0.00279 -0.00334 AFIX 13 H94A 2 0.920508 0.522267 0.508638 11.00000 -1.20000 AFIX 0 C95 1 0.984950 0.549632 0.564344 11.00000 0.05939 0.08859 = 0.07803 -0.00046 -0.00368 0.01671 AFIX 137 H95A 2 0.997670 0.595983 0.581397 11.00000 -1.50000 H95B 2 1.026451 0.527395 0.553982 11.00000 -1.50000 H95C 2 0.964140 0.512144 0.582657 11.00000 -1.50000 AFIX 0 C96 1 0.966097 0.625628 0.495177 11.00000 0.06318 0.06006 = 0.08278 0.00319 0.01480 -0.00817 AFIX 137 H96A 2 0.980001 0.672880 0.511055 11.00000 -1.50000 H96B 2 0.932677 0.638045 0.470006 11.00000 -1.50000 H96C 2 1.006944 0.601265 0.485164 11.00000 -1.50000 AFIX 0 C97 1 0.674616 0.553424 0.543855 11.00000 0.04990 0.08458 = 0.06868 -0.01553 0.01410 0.00673 AFIX 13 H97A 2 0.683427 0.498605 0.536498 11.00000 -1.20000 AFIX 0 C98 1 0.628340 0.588644 0.505757 11.00000 0.06584 0.13603 = 0.10396 -0.00821 -0.02296 0.00980 AFIX 137 H98A 2 0.615788 0.641147 0.513228 11.00000 -1.50000 H98B 2 0.586246 0.557678 0.499706 11.00000 -1.50000 H98C 2 0.653296 0.589701 0.479895 11.00000 -1.50000 AFIX 0 C99 1 0.638419 0.554522 0.585438 11.00000 0.07932 0.14517 = 0.09995 -0.02796 0.04194 -0.02424 AFIX 137 H99A 2 0.623242 0.606957 0.590977 11.00000 -1.50000 H99B 2 0.670731 0.537001 0.610088 11.00000 -1.50000 H99C 2 0.598131 0.520313 0.581849 11.00000 -1.50000 AFIX 0 PART 1 C101 1 0.267896 0.896832 0.360182 21.00000 0.18940 AFIX 33 H10B 2 0.266585 0.932360 0.335494 21.00000 -1.50000 H10C 2 0.220586 0.881719 0.364553 21.00000 -1.50000 H10D 2 0.289787 0.922177 0.386522 21.00000 -1.50000 AFIX 0 C102 1 0.309000 0.826464 0.350921 21.00000 0.19968 AFIX 23 H10E 2 0.287454 0.800190 0.324379 21.00000 -1.20000 H10F 2 0.356989 0.840843 0.346454 21.00000 -1.20000 AFIX 0 C103 1 0.308893 0.775030 0.389692 21.00000 0.17812 AFIX 23 H10G 2 0.263073 0.749950 0.389104 21.00000 -1.20000 H10H 2 0.316605 0.806199 0.416603 21.00000 -1.20000 AFIX 0 C104 1 0.364082 0.714577 0.390404 21.00000 0.17850 AFIX 23 H10I 2 0.404513 0.734910 0.377214 21.00000 -1.20000 H10J 2 0.346122 0.669242 0.373377 21.00000 -1.20000 AFIX 0 C105 1 0.385295 0.691928 0.436983 21.00000 0.16006 AFIX 23 H10K 2 0.389282 0.738975 0.455101 21.00000 -1.20000 H10L 2 0.348254 0.659774 0.447134 21.00000 -1.20000 AFIX 0 C106 1 0.451990 0.648899 0.444121 21.00000 0.16860 AFIX 33 H10M 2 0.462135 0.636308 0.475096 21.00000 -1.50000 H10N 2 0.448276 0.601396 0.426989 21.00000 -1.50000 H10O 2 0.489371 0.680727 0.434969 21.00000 -1.50000 AFIX 0 PART 2 C111 1 0.220726 0.904728 0.374680 31.00000 0.17616 AFIX 33 H11A 2 0.219668 0.960585 0.378549 31.00000 -1.50000 H11B 2 0.217150 0.892596 0.343533 31.00000 -1.50000 H11C 2 0.181757 0.881448 0.387464 31.00000 -1.50000 AFIX 0 C112 1 0.287113 0.873599 0.396751 31.00000 0.20595 AFIX 23 H11D 2 0.326169 0.898393 0.384139 31.00000 -1.20000 H11E 2 0.290806 0.887253 0.428033 31.00000 -1.20000 AFIX 0 C113 1 0.293544 0.788702 0.392646 31.00000 0.16913 AFIX 23 H11F 2 0.259286 0.763645 0.409451 31.00000 -1.20000 H11G 2 0.282293 0.774140 0.361687 31.00000 -1.20000 AFIX 0 C114 1 0.363672 0.759596 0.408376 31.00000 0.15924 AFIX 23 H11H 2 0.375551 0.776450 0.438902 31.00000 -1.20000 H11I 2 0.397487 0.783397 0.390743 31.00000 -1.20000 AFIX 0 C115 1 0.371368 0.673902 0.406442 31.00000 0.16820 AFIX 23 H11J 2 0.376247 0.657124 0.376317 31.00000 -1.20000 H11K 2 0.330476 0.648131 0.416325 31.00000 -1.20000 AFIX 0 C116 1 0.436207 0.654656 0.436555 31.00000 0.18640 AFIX 33 H11L 2 0.443821 0.598995 0.436564 31.00000 -1.50000 H11M 2 0.476096 0.680745 0.426376 31.00000 -1.50000 H11N 2 0.430572 0.671801 0.466169 31.00000 -1.50000 AFIX 0 PART 3 C121 1 0.283355 0.858398 0.318721 41.00000 0.20572 AFIX 33 H12J 2 0.263765 0.910274 0.315885 41.00000 -1.50000 H12K 2 0.324595 0.855565 0.303200 41.00000 -1.50000 H12L 2 0.248920 0.821123 0.306204 41.00000 -1.50000 AFIX 0 C122 1 0.302958 0.840350 0.366059 41.00000 0.17732 AFIX 23 H12B 2 0.261971 0.842222 0.382399 41.00000 -1.20000 H12C 2 0.338193 0.876913 0.379373 41.00000 -1.20000 AFIX 0 C123 1 0.332218 0.759262 0.365559 41.00000 0.16509 AFIX 23 H12D 2 0.294567 0.721956 0.357324 41.00000 -1.20000 H12E 2 0.366301 0.755635 0.344102 41.00000 -1.20000 AFIX 0 C124 1 0.366681 0.741800 0.410658 41.00000 0.15211 AFIX 23 H12F 2 0.409208 0.773139 0.416562 41.00000 -1.20000 H12G 2 0.335068 0.755495 0.432456 41.00000 -1.20000 AFIX 0 C125 1 0.384853 0.658415 0.414754 41.00000 0.17020 AFIX 23 H12H 2 0.411190 0.643128 0.390494 41.00000 -1.20000 H12I 2 0.341895 0.627427 0.412765 41.00000 -1.20000 AFIX 0 C126 1 0.427714 0.642569 0.457619 41.00000 0.16256 AFIX 33 H12M 2 0.439075 0.587738 0.459683 41.00000 -1.50000 H12N 2 0.470550 0.672678 0.459386 41.00000 -1.50000 H12O 2 0.401353 0.657000 0.481626 41.00000 -1.50000 AFIX 0 PART 1 C131 1 0.417714 0.910620 0.525862 51.00000 0.13062 AFIX 33 H13L 2 0.380076 0.903283 0.502345 51.00000 -1.50000 H13M 2 0.406932 0.882864 0.551869 51.00000 -1.50000 H13N 2 0.422836 0.965497 0.532559 51.00000 -1.50000 AFIX 0 C132 1 0.484965 0.879892 0.511590 51.00000 0.15310 AFIX 23 H13D 2 0.478619 0.824850 0.504104 51.00000 -1.20000 H13E 2 0.494495 0.907335 0.484829 51.00000 -1.20000 AFIX 0 C133 1 0.547351 0.887903 0.545239 51.00000 0.16846 AFIX 23 H13F 2 0.551279 0.941724 0.555588 51.00000 -1.20000 H13G 2 0.541609 0.854534 0.570538 51.00000 -1.20000 AFIX 0 C134 1 0.612404 0.865414 0.525713 51.00000 0.18972 AFIX 23 H13H 2 0.608331 0.810937 0.516569 51.00000 -1.20000 H13I 2 0.615508 0.896697 0.499238 51.00000 -1.20000 AFIX 0 C135 1 0.678540 0.875132 0.555589 51.00000 0.16065 AFIX 23 H13J 2 0.669953 0.856250 0.584735 51.00000 -1.20000 H13K 2 0.713608 0.840733 0.544983 51.00000 -1.20000 AFIX 0 C136 1 0.709580 0.951839 0.561313 51.00000 0.23920 AFIX 33 H13O 2 0.752057 0.948796 0.581569 51.00000 -1.50000 H13P 2 0.720652 0.971171 0.533112 51.00000 -1.50000 H13Q 2 0.676760 0.986772 0.573080 51.00000 -1.50000 AFIX 0 PART 2 C141 1 0.382019 0.916019 0.517838 61.00000 0.11215 AFIX 33 H14L 2 0.343778 0.911306 0.494468 61.00000 -1.50000 H14M 2 0.371120 0.886698 0.543283 61.00000 -1.50000 H14N 2 0.388627 0.970225 0.525825 61.00000 -1.50000 AFIX 0 C142 1 0.446573 0.885401 0.502566 61.00000 0.12514 AFIX 23 H14D 2 0.455687 0.914499 0.476267 61.00000 -1.20000 H14E 2 0.438239 0.831252 0.493666 61.00000 -1.20000 AFIX 0 C143 1 0.510951 0.888219 0.534652 61.00000 0.15250 AFIX 23 H14F 2 0.502490 0.864594 0.562725 61.00000 -1.20000 H14G 2 0.526510 0.941892 0.539982 61.00000 -1.20000 AFIX 0 C144 1 0.565106 0.841926 0.512770 61.00000 0.19010 AFIX 23 H14H 2 0.548380 0.788731 0.507183 61.00000 -1.20000 H14I 2 0.572270 0.865708 0.484509 61.00000 -1.20000 AFIX 0 C145 1 0.631315 0.840788 0.541659 61.00000 0.19812 AFIX 23 H14J 2 0.669550 0.829455 0.523975 61.00000 -1.20000 H14K 2 0.629760 0.798876 0.563194 61.00000 -1.20000 AFIX 0 C146 1 0.646382 0.915244 0.565495 61.00000 0.19161 AFIX 33 H14O 2 0.690583 0.911148 0.584011 61.00000 -1.50000 H14P 2 0.649098 0.956863 0.544387 61.00000 -1.50000 H14Q 2 0.609287 0.926267 0.583627 61.00000 -1.50000 AFIX 0 PART 3 C151 1 0.347721 0.922292 0.485985 71.00000 0.11904 AFIX 33 H15J 2 0.310327 0.893849 0.469106 71.00000 -1.50000 H15K 2 0.329098 0.950127 0.509674 71.00000 -1.50000 H15L 2 0.367996 0.958950 0.466936 71.00000 -1.50000 AFIX 0 C152 1 0.401939 0.867609 0.504549 71.00000 0.15030 AFIX 23 H15B 2 0.419501 0.838850 0.480407 71.00000 -1.20000 H15C 2 0.380647 0.830037 0.523096 71.00000 -1.20000 AFIX 0 C153 1 0.461939 0.905456 0.531151 71.00000 0.14586 AFIX 23 H15D 2 0.459767 0.894536 0.562419 71.00000 -1.20000 H15E 2 0.459138 0.961802 0.526939 71.00000 -1.20000 AFIX 0 C154 1 0.529625 0.876233 0.517830 71.00000 0.17474 AFIX 23 H15F 2 0.528898 0.819392 0.516665 71.00000 -1.20000 H15G 2 0.536048 0.895747 0.488449 71.00000 -1.20000 AFIX 0 C155 1 0.588495 0.902702 0.550030 71.00000 0.18043 AFIX 23 H15H 2 0.587175 0.959416 0.552243 71.00000 -1.20000 H15I 2 0.582599 0.881261 0.579069 71.00000 -1.20000 AFIX 0 C156 1 0.657424 0.878655 0.537438 71.00000 0.19558 AFIX 33 H15M 2 0.694137 0.897103 0.559294 71.00000 -1.50000 H15N 2 0.659361 0.822478 0.535796 71.00000 -1.50000 H15O 2 0.663937 0.900627 0.508973 71.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM MRC2160 in P2(1)/c REM wR2 = 0.1667, GooF = S = 1.022, Restrained GooF = 1.026 for all data REM R1 = 0.0570 for 13294 Fo > 4sig(Fo) and 0.0915 for all 19933 data REM 1148 parameters refined using 176 restraints END WGHT 0.0748 0.0000 REM Highest difference peak 0.361, deepest hole -0.337, 1-sigma level 0.046 Q1 1 0.8985 0.9882 0.2021 11.00000 0.05 0.36 Q2 1 0.7102 0.8957 0.5574 11.00000 0.05 0.35 Q3 1 0.7269 0.5976 0.4385 11.00000 0.05 0.32 Q4 1 0.8008 0.5228 0.3176 11.00000 0.05 0.30 Q5 1 0.4603 0.9556 0.3242 11.00000 0.05 0.28 Q6 1 0.2889 0.8584 0.3606 11.00000 0.05 0.28 Q7 1 0.8644 0.5907 0.4422 11.00000 0.05 0.28 Q8 1 0.8253 0.6583 0.4546 11.00000 0.05 0.26 Q9 1 0.4186 0.7109 0.4283 11.00000 0.05 0.26 Q10 1 0.7356 1.0673 0.2243 11.00000 0.05 0.26 ; _shelx_res_checksum 39506 _shelx_hkl_file ; 0 0 -3 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56150.7 882.725 1 -2 2 -5 79771.8 681.990 6 2 -2 5 78815.5 1116.87 1 2 -2 6 1233.63 163.990 1 2 -2 7 311.451 108.808 1 2 -2 8 8457.91 443.387 1 2 -2 9 378.452 132.605 1 2 -2 10 23963.5 815.878 1 2 -2 11 5570.70 409.365 1 2 -2 12 26.0506 103.880 1 2 -2 13 19245.8 833.701 1 2 2 14 2734.58 323.941 1 2 -2 14 2646.71 334.339 1 2 -2 15 101.706 124.955 1 2 2 15 317.868 141.331 1 2 2 16 16409.0 835.275 1 2 -2 16 16269.2 856.055 1 2 2 17 94.6102 96.9927 1 2 -2 17-27.0416 137.754 1 2 -2 18 62.8964 126.076 1 2 2 18-105.686 121.546 1 2 2 19 117.558 99.7787 1 2 -2 19-46.1906 124.750 1 2 2 20 2011.86 351.846 1 2 -2 20 1265.17 284.228 1 2 -2 21 1.42009 162.474 1 -2 -2 -21 44.4923 57.7060 2 2 2 21 28.3400 144.857 1 2 2 22 1229.61 293.006 1 2 -2 22 1905.49 348.605 1 -2 -2 -22 1697.37 170.549 2 -2 -2 -23 1982.99 190.342 2 2 2 23 2030.25 389.778 1 2 -2 23 1604.62 355.132 1 2 -2 24 149.717 142.626 1 -2 -2 -24 63.4662 63.7972 2 2 2 24 106.136 125.419 1 2 -2 25 663.769 249.093 1 -2 -2 -25 580.459 121.299 2 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2 -3 -25 104.076 75.8321 2 -2 -3 25 1100.99 282.963 1 2 -3 -24 771.927 132.308 2 -2 -3 24 774.470 255.501 1 -2 -3 23 5463.15 580.919 1 2 -3 -23 5322.23 313.287 2 2 -3 -22 2370.31 207.062 2 -2 -3 22 2356.09 383.436 1 -2 3 21 183.964 118.522 1 -2 -3 21 237.339 112.106 1 2 -3 -21 328.766 85.8387 2 -2 -3 20-131.535 115.951 1 -2 3 20 168.913 112.034 1 -2 3 19 104.553 83.7119 1 -2 -3 19 120.720 100.075 1 -2 3 18 1909.40 277.291 1 -2 -3 18 2503.48 352.098 1 -2 3 17 125.197 108.220 1 2 3 -17 29.2433 91.4109 6 -2 -3 17-22.3680 125.974 1 2 3 -16 720.173 188.662 6 -2 3 16 408.294 129.632 1 -2 -3 16 707.072 182.193 1 2 3 -15 403.543 147.156 6 -2 3 15 400.205 124.511 1 -2 -3 15 304.939 128.294 1 -2 3 14 11953.7 562.637 1 2 3 -14 13358.1 687.005 6 -2 -3 14 12313.0 638.502 1 -2 -3 13 2144.63 268.940 1 -2 3 13 2175.57 235.272 1 2 3 -13 2358.01 279.105 6 -2 -3 12 1805.73 233.406 1 2 3 -12 2106.02 259.646 6 2 3 -11 1363.02 202.022 6 -2 -3 11 1282.72 196.879 1 2 3 -10 1555.08 214.006 6 -2 -3 10 1451.47 193.677 1 -2 -3 9 5439.67 350.870 1 2 3 -9 5002.54 349.825 6 -2 -3 8 13794.7 533.820 1 2 3 -8 13332.3 542.160 6 2 3 -7 5998.34 351.988 6 -2 -3 7 6757.00 358.490 1 -2 -3 6 23.2816 71.6038 1 2 3 -6 98.4184 90.9973 6 2 3 -5 27444.1 670.548 6 -2 -3 5 26968.8 654.000 1 -2 -3 4 28982.0 659.334 1 2 3 -4 29950.7 673.941 6 -2 -3 3 3037.74 213.323 1 2 3 -3 3207.07 217.051 6 2 3 -2 8306.47 339.492 6 2 -3 -2 9218.35 287.674 1 -2 -3 2 8694.98 347.037 1 -2 -3 1 50323.5 824.630 1 2 3 -1 52976.6 836.555 6 2 -3 -1 52052.3 703.013 1 2 3 0 20389.3 524.788 6 2 -3 0 20684.6 463.612 1 2 -3 1 3565.02 208.048 1 -2 3 -2 1842.67 96.6806 6 2 -3 2 1901.29 165.213 1 2 -3 3 30921.1 661.285 1 -2 3 -3 30294.6 386.657 6 -2 3 -4 59290.1 577.030 6 2 -3 4 58070.6 969.781 1 2 -3 5 12742.8 487.921 1 -2 3 -5 13372.2 304.086 6 -2 3 -6 77288.2 808.911 6 2 -3 6 78595.7 1262.72 1 2 -3 7 44209.3 992.277 1 -2 3 -7 43810.0 664.701 6 2 -3 8 987.394 172.362 1 -2 3 -8 970.278 111.707 6 2 -3 9 18700.9 718.942 1 -2 3 -9 19225.4 520.127 6 2 -3 10 3601.86 330.233 1 2 -3 11 18468.7 771.915 1 2 -3 12 1631.99 265.156 1 2 -3 13 4.18733 99.5271 1 2 -3 14 14198.8 763.791 1 2 -3 15 608.359 200.573 1 2 3 16 1964.93 297.622 1 2 -3 16 2091.97 329.449 1 2 3 17 632.322 194.111 1 2 -3 17 598.127 194.725 1 2 3 18 562.547 181.500 1 2 -3 18 163.919 152.017 1 2 -3 19 1301.98 288.526 1 2 3 19 956.820 236.141 1 2 3 20 7100.87 644.246 1 -2 -3 -20 6634.32 320.079 2 2 -3 20 7031.95 661.658 1 2 -3 21 1258.46 303.811 1 2 3 21 1217.03 277.465 1 -2 -3 -21 1295.81 151.978 2 -2 -3 -22 6033.60 323.522 2 2 -3 22 5411.14 608.814 1 2 3 22 6782.51 663.563 1 2 -3 23 874.128 260.666 1 2 3 23 511.519 232.970 1 -2 -3 -23 626.666 118.296 2 2 3 24 640.059 232.620 1 2 -3 24 495.664 251.692 1 -2 -3 -24 869.352 141.982 2 -2 -3 -25 1233.76 166.213 2 2 3 25 1234.95 309.328 1 2 -3 25 761.948 245.082 1 -2 -3 -26 146.379 97.7920 2 -2 -3 -27 46.8519 77.4141 2 -2 -3 -28 228.197 92.1015 2 -2 -3 -29 390.055 104.091 2 -2 -3 -30-95.9958 92.9920 2 -2 -3 -31 746.828 130.591 2 -2 -3 -32 325.555 95.4066 2 -2 -3 -33 3.58175 56.6005 2 -2 -3 -34-153.269 65.9772 2 -2 -3 -35 3.25806 38.9966 3 -2 3 -35-28.9187 49.0813 3 -2 -3 -35 48.5619 42.1562 2 -2 3 -36-14.6822 38.9519 3 -2 -3 -36-45.7803 32.0832 3 -2 3 -37 151.130 47.4342 3 2 4 -37-10.4734 31.5660 3 2 4 -36 127.020 54.3702 3 2 -4 -35-11.3607 26.4819 3 2 4 -35 772.806 103.787 3 2 -4 -34-45.5372 54.6135 3 2 4 -34-42.6784 69.1643 3 2 -4 -33 747.892 102.375 3 2 -4 -33 1221.39 147.147 2 2 4 -33 1167.39 139.920 3 2 -4 -32 606.851 99.4442 3 2 4 -32 759.714 129.135 3 2 -4 -32 886.641 141.158 2 2 -4 -31 430.892 118.369 2 2 4 -31 257.861 103.795 3 2 -4 -31 135.050 73.2966 3 2 4 -30 494.380 122.340 3 2 -4 -30 363.116 99.6490 2 2 -4 -29 316.912 97.2941 2 2 -4 -28 3309.71 265.296 2 2 -4 -27 1462.58 190.592 2 2 -4 -26 45.0986 94.0852 2 -2 -4 25 369.520 189.892 1 2 -4 -25 319.611 110.493 2 -2 -4 24 2478.73 401.899 1 2 -4 -24 2491.94 224.752 2 2 -4 -23 659.526 126.777 2 -2 -4 23 411.849 194.971 1 2 -4 -22-6.64387 60.8542 2 -2 -4 22-242.542 161.701 1 2 -4 -21 695.032 127.161 2 -2 -4 21 618.388 231.786 1 -2 -4 20 1787.59 329.080 1 2 -4 -20 1422.98 155.819 2 -2 4 20 1294.55 247.294 1 -2 -4 19 171.014 85.4275 1 -2 4 19 274.151 146.078 1 -2 4 18 339.641 136.987 1 -2 -4 18 106.097 135.094 1 -2 4 17 1444.83 232.694 1 -2 -4 17 1481.27 274.382 1 2 4 -17 1923.74 306.829 6 -2 -4 16-126.484 141.125 1 2 4 -16 38.2815 115.597 6 -2 4 16 33.6119 71.9636 1 -2 4 15 494.194 139.342 1 -2 -4 15 617.231 170.981 1 2 4 -15 304.139 132.995 6 2 4 -14 13287.9 697.236 6 -2 -4 14 14516.6 732.401 1 2 4 -13 8323.20 529.174 6 -2 -4 13 7413.48 511.145 1 -2 -4 12 76.5225 94.9732 1 2 4 -12 198.473 130.170 6 -2 -4 11 234.047 115.528 1 2 4 -11 82.6104 91.7978 6 2 4 -10 30082.4 904.515 6 -2 -4 10 29711.8 908.485 1 -2 -4 9 2663.96 272.474 1 2 4 -9 2846.42 277.708 6 2 4 -8 2761.95 265.048 6 -2 -4 8 2831.49 266.119 1 -2 -4 7 13783.6 559.952 1 2 4 -7 13180.4 540.941 6 2 4 -6 29374.3 779.657 6 -2 -4 6 28322.9 775.336 1 2 4 -5 69.2684 64.5291 6 -2 -4 5 57.0997 93.8442 1 2 4 -4 6489.24 345.463 6 -2 -4 4 5859.63 339.824 1 -2 -4 3 24100.2 670.529 1 2 4 -3 25175.5 660.773 6 -2 -4 2 31570.2 750.239 1 2 4 -2 32216.1 737.224 6 2 -4 -2 32668.8 652.945 1 -2 -4 1 17194.6 554.226 1 2 -4 -1 17033.3 478.916 1 2 4 -1 18041.5 548.508 6 2 -4 0 837.172 121.836 1 2 -4 1 213610. 1789.70 1 -2 4 -2 77822.7 808.876 6 2 -4 2 79963.4 1139.46 1 -2 4 -3 7336.27 243.507 6 2 -4 3 7514.95 371.277 1 2 -4 4 46339.6 941.155 1 -2 4 -4 45283.9 612.430 6 -2 4 -5 8241.64 274.652 6 2 -4 5 8564.16 432.869 1 2 -4 6 3163.64 283.695 1 -2 4 -6 2813.65 171.417 6 2 -4 7 372.720 123.879 1 -2 4 -7 394.480 73.7424 6 -2 4 -8 304.805 68.6111 6 2 -4 8 263.367 132.236 1 -2 4 -9 5303.68 275.777 6 2 -4 9 5800.44 425.161 1 -2 4 -10 66.4710 62.0573 6 2 -4 10 113.813 105.340 1 2 -4 11 3229.43 351.144 1 -2 4 -11 3182.71 245.488 6 2 -4 12 2415.34 320.941 1 2 -4 13 575.599 182.625 1 2 -4 14 584.542 172.272 1 2 -4 15 4676.42 469.015 1 2 -4 16 680.041 189.022 1 2 -4 17 6229.01 585.281 1 2 4 17 5923.84 542.537 1 2 4 18 161.348 121.502 1 2 -4 18 24.2779 146.019 1 -2 -4 -19 3011.97 216.691 2 2 -4 19 3317.18 464.336 1 2 4 19 3075.22 422.103 1 2 -4 20 76.8541 143.005 1 -2 -4 -20 226.056 84.7478 2 2 4 20 86.2103 102.556 1 2 -4 21 1994.15 385.721 1 -2 -4 -21 1760.78 179.791 2 2 4 21 1806.74 349.295 1 -2 -4 -22 1018.75 149.876 2 2 -4 22 825.930 261.983 1 2 4 22 1176.89 308.726 1 2 4 23 7948.52 738.269 1 -2 -4 -23 7876.18 383.910 2 2 -4 23 7754.57 775.707 1 2 -4 24 5178.74 649.964 1 2 4 24 5423.91 624.432 1 -2 -4 -24 5167.16 321.162 2 2 -4 25 420.260 216.680 1 -2 -4 -25 433.152 114.029 2 2 4 25 873.437 260.058 1 -2 -4 -26-0.87569 81.6168 2 -2 -4 -27 193.203 90.0173 2 -2 -4 -28 104.000 92.7283 2 -2 -4 -29 170.874 91.8854 2 -2 -4 -30 1469.11 176.515 2 -2 -4 -31-94.7548 75.2618 2 -2 -4 -32 406.535 101.032 2 -2 -4 -33-32.3930 64.8269 2 -2 -4 -34 626.769 95.0176 2 -2 4 -34 604.613 98.4700 3 -2 -4 -34 312.840 64.0665 3 -2 -4 -35-11.5828 38.5211 3 -2 4 -35 88.1377 50.9075 3 -2 -4 -35 28.0137 38.7051 2 -2 4 -36 269.502 53.2830 3 2 5 -37 163.725 42.3823 3 2 5 -36 22.4540 38.6624 3 2 5 -35 14.6611 45.6252 3 2 5 -34-103.314 63.1362 3 2 -5 -33 98.4577 75.0020 2 2 5 -33 116.295 69.1900 3 2 5 -32 33.5555 69.9491 3 2 -5 -32-25.9162 68.9694 2 2 -5 -31-15.9706 81.8130 2 2 5 -31 55.8259 88.7854 3 2 -5 -31 99.3004 59.9164 3 2 -5 -30 1876.20 163.037 3 2 5 -30 2171.56 204.855 3 2 -5 -30 2037.18 210.154 2 2 5 -29-79.6355 89.6773 3 2 -5 -29 147.452 96.4892 2 2 -5 -28 158.264 101.519 2 2 -5 -27 190.772 106.581 2 2 -5 -26 504.934 128.247 2 2 -5 -25 1440.54 179.544 2 -2 -5 25 2033.96 378.904 1 2 -5 -24 713.275 133.438 2 -2 -5 24 993.170 292.485 1 -2 -5 23 2393.43 415.794 1 2 -5 -23 2411.37 225.632 2 -2 -5 22 612.903 229.497 1 2 -5 -22 272.263 87.2310 2 2 -5 -21-55.2039 78.8021 2 -2 -5 21-32.0969 92.6876 1 2 -5 -20 3427.75 244.633 2 -2 -5 20 3377.00 452.376 1 2 -5 -19 391.203 90.7733 2 -2 -5 19 306.827 155.736 1 2 5 -19 177.389 88.0989 6 -2 5 19 332.453 131.372 1 2 5 -18 803.610 215.383 6 -2 5 18 924.497 196.725 1 -2 -5 18 940.101 241.972 1 2 5 -17 11750.4 734.848 6 -2 -5 17 11356.5 750.078 1 -2 5 17 10955.8 635.677 1 2 5 -16 4869.44 467.636 6 -2 5 16 5027.13 420.284 1 -2 -5 16 5246.80 490.616 1 2 5 -15 872.064 210.017 6 -2 -5 15 785.838 196.471 1 -2 -5 14 4738.25 448.752 1 2 5 -14 4981.65 448.403 6 -2 -5 13 23917.6 957.450 1 2 5 -13 23785.8 915.580 6 -2 -5 12 13621.3 696.568 1 2 5 -12 13173.5 667.894 6 2 5 -11 11091.7 589.326 6 -2 -5 11 10521.5 599.232 1 2 5 -10 11463.1 587.725 6 -2 -5 10 10363.3 577.689 1 2 5 -9 24.4357 95.5542 6 -2 -5 9 175.567 94.0246 1 2 5 -8 29700.8 884.340 6 -2 -5 8 30675.8 928.493 1 -2 -5 7 11211.1 550.831 1 2 5 -7 11388.1 528.755 6 2 5 -6 261.620 109.790 6 -2 -5 6 202.290 107.929 1 2 5 -5 18061.9 632.337 6 -2 -5 5 17417.1 654.247 1 2 5 -4 2710.98 244.926 6 -2 -5 4 2566.31 252.410 1 2 5 -3 1464.48 184.832 6 -2 -5 3 1246.51 174.538 1 2 5 -2 92251.1 1365.71 6 -2 -5 2 89069.1 1402.91 1 2 -5 -1 667.302 123.003 1 2 5 -1 719.246 139.859 6 2 5 0 32966.1 823.664 6 2 -5 0 31988.1 763.442 1 2 -5 1 250.460 104.937 1 2 -5 2 5587.69 337.976 1 -2 5 -2 5060.38 245.287 6 -2 5 -3 11029.7 354.081 6 2 -5 3 10725.6 483.334 1 -2 5 -4 13433.0 394.849 6 2 -5 4 13920.2 566.810 1 -2 5 -5 7250.23 293.385 6 2 -5 5 7230.49 436.598 1 2 -5 6 19252.8 717.220 1 -2 5 -6 18756.2 481.028 6 -2 5 -7 7333.94 312.612 6 2 -5 7 7191.25 460.157 1 2 -5 8 8559.00 519.482 1 -2 5 -8 8224.98 344.069 6 2 -5 9 12644.2 654.006 1 -2 5 -9 12272.8 437.126 6 2 -5 10 722.834 181.171 1 -2 5 -10 919.032 128.843 6 2 -5 11 13158.6 715.554 1 -2 5 -11 11852.4 472.635 6 2 -5 12 7147.68 549.762 1 -2 5 -12 7061.88 383.434 6 2 -5 13 4486.84 450.318 1 2 -5 14 865.564 228.650 1 2 -5 15 199.723 124.734 1 2 -5 16-25.1629 119.645 1 2 -5 17 4211.36 492.620 1 2 5 18 20025.3 1044.63 1 2 -5 18 19122.6 1086.99 1 2 5 19 7844.93 680.393 1 2 -5 19 8547.10 745.392 1 -2 -5 -19 6957.01 335.264 2 2 -5 20 790.681 236.144 1 -2 -5 -20 879.503 134.015 2 2 5 20 551.417 203.296 1 -2 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435.481 108.001 3 2 6 -29 245.721 83.0833 3 2 -6 -29 404.001 117.624 2 2 6 -28 823.440 134.252 3 2 -6 -28 1265.48 175.817 2 2 6 -27 25.8815 76.2984 3 2 -6 -27 66.6486 96.6638 2 2 -6 -26 386.106 116.870 2 2 -6 -25 203.152 89.4229 2 2 -6 -24 633.560 134.011 2 -2 -6 24 678.990 219.203 1 2 -6 -23 350.804 111.741 2 -2 -6 23 132.519 222.780 1 2 -6 -22 179.795 92.9918 2 -2 -6 22 82.4327 132.037 1 2 -6 -21 1544.44 175.831 2 -2 -6 21 1491.41 329.363 1 -2 -6 20 8691.73 746.530 1 2 -6 -20 8438.53 383.070 2 2 6 -20 8305.24 679.948 6 -2 -6 19 447.280 207.269 1 2 -6 -19 382.712 91.2141 2 2 6 -19 336.576 154.497 6 -2 6 18 6966.46 539.552 1 -2 -6 18 7790.98 671.809 1 2 -6 -18 7341.76 334.152 2 2 6 -18 7961.74 640.002 6 -2 6 17 14426.4 754.195 1 -2 -6 17 15018.4 904.063 1 2 6 -17 14288.3 825.447 6 -2 -6 16 3511.02 431.149 1 2 6 -16 3487.67 394.870 6 2 6 -15 2508.48 336.152 6 -2 -6 15 2701.97 367.971 1 2 6 -14 132.462 114.979 6 -2 -6 14 453.604 146.905 1 -2 -6 13 1525.65 279.618 1 2 6 -13 1437.19 251.914 6 -2 -6 12 11988.7 705.586 1 2 6 -12 11949.2 660.014 6 -2 -6 11 6130.42 487.253 1 2 6 -11 5928.59 453.292 6 -2 -6 10 23104.0 921.383 1 2 6 -10 23153.2 863.619 6 2 6 -9 1590.55 229.151 6 -2 -6 9 1680.03 256.389 1 -2 -6 8 3812.23 364.543 1 2 6 -8 4270.58 358.855 6 -2 -6 7 897.254 184.374 1 2 6 -7 1109.64 194.000 6 2 6 -6 7105.78 439.205 6 -2 -6 6 7604.20 482.250 1 -2 -6 5 19739.6 764.068 1 2 6 -5 19256.3 702.586 6 -2 -6 4 2924.66 295.320 1 2 6 -4 2787.82 272.309 6 2 6 -3 3656.12 303.721 6 -2 -6 3 3012.46 294.996 1 2 6 -2 118.298 81.9568 6 -2 -6 2 207.722 117.074 1 2 6 -1 4329.01 338.767 6 2 -6 -1 4582.76 320.675 1 2 6 0 1410.86 204.697 6 2 -6 0 983.883 163.183 1 2 -6 1 2583.19 261.237 1 2 -6 2 1699.42 218.458 1 -2 6 -2 1532.55 157.717 6 2 -6 3 36010.4 961.394 1 -2 6 -3 35509.8 727.746 6 2 -6 4 526.732 148.652 1 -2 6 -4 505.477 95.1610 6 2 -6 5 11904.7 588.699 1 -2 6 -5 12208.0 424.824 6 -2 6 -6 2556.35 201.430 6 2 -6 6 2464.17 290.708 1 -2 6 -7 5752.01 302.962 6 2 -6 7 6425.03 462.863 1 -2 6 -8 4487.76 275.892 6 2 -6 8 4224.05 392.945 1 -2 6 -9 28422.1 709.970 6 2 -6 9 27622.1 1021.87 1 -2 6 -10 9207.62 412.059 6 2 -6 10 8383.51 591.734 1 2 -6 11 9651.32 660.265 1 -2 6 -11 9497.92 435.943 6 2 -6 12 97.3735 155.779 1 2 -6 13 11900.5 768.132 1 2 -6 14 681.445 230.498 1 2 -6 15 267.796 180.920 1 2 -6 16 1179.16 267.155 1 2 -6 17 936.116 258.445 1 2 -6 18 233.835 219.930 1 -2 -6 -18 251.399 77.5090 2 -2 -6 -19 798.683 123.990 2 2 6 19 761.290 210.576 1 2 -6 19 939.536 294.736 1 2 6 20 90.1551 167.136 1 2 -6 20 332.631 122.121 1 -2 -6 -20 121.937 66.9571 2 2 6 21 956.679 269.472 1 -2 -6 -21 1092.35 154.610 2 2 -6 21 1357.69 345.125 1 2 -6 22 114.066 154.549 1 -2 -6 -22 42.2898 69.9024 2 2 6 22 102.111 124.695 1 -2 -6 -23 1488.24 183.963 2 2 6 23 1356.35 325.405 1 2 -6 23 1241.10 320.224 1 2 -6 24 1261.63 328.806 1 2 6 24 793.036 270.092 1 -2 -6 -24 1544.51 188.363 2 -2 -6 -25-69.2835 86.1125 2 -2 -6 -26 976.800 162.022 2 -2 -6 -27 367.456 114.371 2 -2 -6 -28 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210.452 3 -2 8 -29-76.7302 71.5405 3 -2 -8 -29-74.7644 83.1079 2 -2 -8 -30 41.7985 76.8723 2 -2 8 -30-12.3228 51.1203 3 -2 -8 -31 279.596 84.6006 2 -2 8 -31 403.164 78.4650 3 -2 -8 -32-11.9578 53.8259 2 -2 8 -32 6.45611 40.5568 3 -2 -8 -33 274.545 73.3220 2 -2 8 -33 193.303 45.6730 3 -2 -8 -34 67.6858 39.8192 2 2 -9 -34 9.07210 29.7366 4 2 9 -33 30.6498 31.2734 3 2 9 -32 101.294 46.3393 3 2 -9 -31-117.323 79.0294 2 2 9 -31-18.6347 45.6876 3 2 -9 -30 274.259 91.0755 2 2 9 -30 366.625 77.4789 3 2 9 -29 787.035 109.470 3 2 -9 -29 800.635 129.475 2 2 9 -28 152.555 76.7811 3 2 -9 -28 160.981 87.2929 2 2 9 -27 811.432 126.957 3 2 -9 -27 653.060 130.410 2 2 -9 -26 219.359 103.975 2 2 9 -26 474.602 109.418 3 2 9 -25 432.081 96.5765 3 2 -9 -25 610.582 132.063 2 2 9 -24 287.384 77.8145 3 2 -9 -24 353.897 115.839 2 2 9 -23 550.460 112.718 3 2 -9 -23 542.035 129.350 2 2 9 -22 2765.89 212.247 3 2 -9 -22 2705.26 238.895 2 2 -9 -21 4536.11 301.533 2 2 9 -21 4174.77 260.593 3 -2 -9 21 4715.78 613.125 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9 -1 771.897 190.269 6 -2 9 0 205.265 109.485 6 2 9 0 210.509 115.398 6 2 9 1 6174.16 507.583 6 2 -9 1 5753.29 475.659 1 -2 9 -1 5751.83 407.605 6 2 -9 2 7.20490 89.0640 1 -2 9 -2 198.278 93.4291 6 2 9 2 35.8805 102.747 6 2 -9 3 12.0671 123.168 1 -2 9 -3-46.7344 87.3841 6 -2 9 -4 5029.93 368.566 6 2 -9 4 5290.12 478.403 1 -2 9 -5 11620.8 548.401 6 2 -9 5 11682.2 730.819 1 2 -9 6 6495.07 550.013 1 2 -9 7 4986.16 499.765 1 2 -9 8 3113.48 411.335 1 2 -9 9 897.934 219.561 1 2 -9 10 4291.76 503.618 1 2 -9 11 15253.6 967.154 1 2 -9 12 2715.39 433.695 1 2 -9 13 887.148 260.342 1 2 -9 14 1629.99 345.232 1 -2 -9 -14 1663.69 156.967 2 -2 -9 -15 2797.56 184.560 5 -2 -9 -15 2646.42 203.563 2 2 -9 15 2747.68 445.123 1 -2 -9 -16 3141.86 231.208 2 2 -9 16 3918.88 547.146 1 -2 -9 -17 422.424 105.512 2 2 -9 17 555.952 240.150 1 -2 -9 -18 4904.27 301.620 2 2 -9 18 4335.27 596.215 1 -2 -9 -19 5155.81 308.309 2 2 -9 19 5291.12 657.751 1 -2 -9 -20 32.2137 81.4446 2 2 -9 20-280.998 181.208 1 -2 -9 -21 324.809 100.113 2 2 -9 21 47.3653 150.140 1 2 9 21 1.61882 117.414 1 -2 -9 -22 328.019 103.310 2 -2 -9 -23 219.424 98.7609 2 -2 -9 -24-60.3529 85.8013 2 -2 -9 -25 78.7898 83.8121 2 -2 9 -26 180.602 88.0785 3 -2 -9 -26 131.352 90.3558 2 -2 9 -27 973.897 121.015 3 -2 -9 -27 1096.42 159.826 2 -2 -9 -28-16.2144 75.3647 2 -2 9 -28-10.9400 50.9551 3 -2 9 -29 267.344 70.0533 3 -2 -9 -29 411.997 102.421 2 -2 9 -30 261.285 60.4934 3 -2 -9 -30 347.543 90.2932 2 -2 -9 -31 1887.21 163.870 2 -2 9 -31 1696.75 122.122 3 -2 -9 -32 267.181 67.0878 2 -2 -9 -33 25.7715 40.6351 2 2 -10 -33 295.126 55.1315 4 2 10 -30 163.703 59.4983 3 2 -10 -30 176.861 68.8298 2 2 -10 -29 45.1747 71.8713 2 2 10 -29-21.7986 49.4687 3 2 -10 -28 2772.09 220.736 2 2 10 -28 2751.99 182.847 3 2 10 -27 125.593 70.2569 3 2 -10 -27 84.2930 69.7599 2 2 10 -26 698.490 106.714 3 2 -10 -26 567.610 125.382 2 2 10 -25 1638.09 157.955 3 2 -10 -25 1551.57 183.559 2 2 10 -24 23.6212 51.0122 3 2 -10 -24 91.5763 80.8195 2 2 -10 -23 181.069 86.2286 2 2 -10 -22-73.1909 65.4674 2 2 -10 -21 262.740 102.175 2 2 -10 -20 1209.30 162.429 2 -2 -10 20 784.595 279.494 1 2 -10 -19 560.274 111.932 2 -2 -10 19 251.783 170.839 1 2 -10 -18 1565.46 168.765 2 -2 -10 18 1245.48 329.751 1 2 -10 -17 789.547 131.291 2 -2 -10 17 1097.24 306.234 1 -2 -10 16 6091.87 685.350 1 2 -10 -16 5456.60 300.801 2 2 -10 -16 5340.36 266.068 5 2 -10 -15 931.032 118.153 5 2 -10 -15 913.761 127.921 2 -2 -10 15 990.199 272.767 1 2 -10 -14 5452.40 266.884 5 -2 -10 14 5374.28 624.663 1 2 -10 -14 5272.02 277.076 2 2 10 -13 1425.23 268.684 6 2 -10 -13 1716.80 152.691 5 -2 -10 13 2088.59 393.218 1 2 10 -12 615.540 188.275 6 -2 -10 12 661.917 203.116 1 2 -10 -12 813.935 107.271 5 2 10 -11 142.577 115.439 6 -2 -10 11 560.945 220.023 1 -2 -10 10 7562.70 683.115 1 2 10 -10 7916.77 613.507 6 2 10 -9-51.0651 83.9905 6 -2 -10 9-11.9301 130.180 1 2 10 -8 7344.97 584.067 6 -2 -10 8 9032.62 732.048 1 -2 -10 7 2942.17 411.791 1 2 10 -7 3004.32 370.754 6 2 10 -6 166.324 82.0613 6 -2 -10 6 151.573 140.979 1 2 10 -5 1336.87 259.462 6 2 10 -4 2948.99 372.234 6 2 10 -3 328.745 170.358 6 -2 10 2 7389.72 525.131 6 2 10 -2 6962.79 556.030 6 2 10 -1 5244.76 485.862 6 -2 10 1 5477.57 448.843 6 -2 10 0 7515.87 513.160 6 2 10 0 8279.77 614.191 6 2 10 1 4630.78 470.635 6 -2 10 -1 4207.16 378.539 6 2 -10 2 4847.69 481.792 1 -2 10 -2 4380.19 383.862 6 2 10 2 4577.61 466.181 6 2 10 3 9178.48 669.334 6 -2 10 -3 9023.28 534.453 6 2 -10 3 9097.66 663.944 1 2 10 4 6100.70 552.634 6 2 -10 4 5730.73 536.545 1 2 -10 5 3595.20 446.332 1 2 -10 6 4747.79 503.947 1 2 -10 7 902.091 252.374 1 2 -10 8 13897.0 907.385 1 2 -10 9 1130.18 281.724 1 2 -10 10 561.105 190.179 1 2 -10 11 266.570 183.167 1 -2 -10 -11 58.6197 54.5617 5 2 -10 12 1550.85 338.463 1 -2 -10 -12 1325.57 132.284 5 -2 -10 -13 462.254 85.3252 2 -2 -10 -13 398.422 87.6217 5 -2 -10 -14 1730.39 154.785 5 2 -10 14 1803.07 359.502 1 -2 -10 -14 2018.19 179.453 2 2 -10 15 178.002 168.000 1 -2 -10 -15 294.950 70.8862 5 -2 -10 -15 370.559 99.2382 2 -2 -10 -16 6624.63 298.998 5 2 -10 16 7102.35 749.588 1 -2 -10 -16 7002.95 347.038 2 -2 -10 -17 186.734 78.3627 2 2 -10 17 630.622 257.222 1 -2 -10 -18 551.171 122.006 2 2 -10 18 930.150 303.765 1 2 -10 19 2085.62 443.704 1 -2 -10 -19 2567.54 222.668 2 -2 -10 -20 1551.60 184.940 2 -2 -10 -21 239.025 91.6838 2 -2 -10 -22 197.334 89.6307 2 -2 -10 -23 38.7703 77.1320 2 -2 -10 -24-44.8856 76.8198 2 -2 -10 -25 272.344 95.5125 2 -2 -10 -26 79.6882 76.8314 2 -2 -10 -27 803.995 137.855 2 -2 -10 -28 66.6208 70.8619 2 -2 -10 -29 309.556 83.4685 2 -2 -10 -30 1849.55 160.943 2 -2 -10 -31 234.050 65.7418 2 -2 -10 -32 26.3209 39.4710 2 2 -11 -33 240.054 45.4526 4 2 -11 -32 27.1082 36.6497 4 2 -11 -31 35.4110 44.0434 4 2 -11 -29-31.0684 60.3520 2 2 -11 -28 647.602 107.414 2 2 -11 -27 55.3986 67.2154 2 2 -11 -26 1632.98 171.530 2 2 -11 -25 75.6844 67.6379 2 2 -11 -24-57.0433 79.5732 2 2 -11 -23 165.746 90.4414 2 2 -11 -22 363.669 104.885 2 2 -11 -21 844.595 139.430 2 2 -11 -20 225.359 92.0098 2 2 -11 -19 2955.32 235.776 2 2 -11 -18 529.933 113.440 2 -2 -11 18 206.248 146.964 1 2 -11 -17 6940.30 310.813 5 2 -11 -17 6370.16 332.583 2 -2 -11 17 6059.85 705.834 1 2 -11 -16 325.845 86.9912 2 2 -11 -16 606.118 100.834 5 -2 -11 15-38.8056 186.175 1 2 -11 -15 24.8545 55.9359 5 2 -11 -14-81.4620 65.5091 5 -2 -11 14-419.033 208.239 1 2 -11 -13 275.957 74.8945 5 -2 -11 13 397.398 177.504 1 2 -11 -12 1118.32 130.510 5 -2 -11 12 860.492 264.525 1 -2 -11 11 181.720 183.189 1 2 -11 -11 71.4704 47.2880 5 2 11 -11 275.852 140.624 6 2 -11 -10 827.025 115.553 5 2 11 -10 1184.18 254.068 6 -2 -11 10 786.835 251.000 1 2 -11 -9 13232.9 423.988 5 2 11 -9 13118.1 821.410 6 -2 -11 9 13868.6 969.051 1 2 11 -8 289.126 90.2321 6 2 -11 -8 419.213 90.3943 5 2 -11 -7-63.1369 62.0024 5 2 11 -7 219.518 158.817 6 2 11 -6 263.694 107.712 6 2 11 -5 762.638 194.981 6 2 11 -4 167.873 113.557 6 2 11 -3 10214.8 706.291 6 -2 11 3 10417.5 688.494 6 -2 11 2 2434.94 336.315 6 2 11 -2 2656.32 376.170 6 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230.309 2 -2 -11 -19 63.1958 74.4108 2 -2 -11 -20 466.140 114.820 2 -2 -11 -21 545.773 124.951 2 -2 -11 -22 1941.18 195.862 2 -2 -11 -23 16.0804 70.8876 2 -2 -11 -24 243.744 94.9914 2 -2 -11 -25 627.242 122.495 2 -2 -11 -26 174.435 86.2970 2 -2 -11 -27-48.0063 64.8786 2 -2 -11 -28 915.012 123.984 2 -2 -11 -29 1765.94 154.673 2 -2 -11 -30 541.918 89.0603 2 -2 -11 -31 101.227 48.0636 2 2 -12 -31 27.4829 32.2088 4 2 -12 -30 40.6132 44.6556 4 2 -12 -29 410.472 74.5756 4 2 -12 -28-59.2888 59.1572 4 2 -12 -27-58.2940 61.5104 2 2 -12 -26-38.2020 69.6125 2 2 -12 -25 17.4943 61.8186 2 2 -12 -24 138.740 79.6881 2 2 -12 -23 12.0716 55.6942 2 2 -12 -22 428.485 102.410 2 2 -12 -21 2138.52 204.011 2 2 -12 -20 2167.42 200.371 2 2 -12 -19 19.3221 58.8721 2 2 -12 -18 73.6175 55.5661 5 2 -12 -18 145.378 74.9464 2 2 -12 -17 846.138 119.667 5 2 -12 -16 1067.50 135.425 5 -2 -12 16 625.920 246.803 1 -2 -12 15 45.5883 182.594 1 2 -12 -15 63.8993 55.8708 5 2 -12 -14 138.408 79.2663 5 -2 -12 14 54.0974 120.599 1 -2 -12 13 593.343 279.449 1 2 -12 -13 222.730 77.4007 5 2 -12 -12 478.133 96.5275 5 -2 -12 12 550.287 253.313 1 2 -12 -11 2088.45 184.187 5 -2 -12 11 1776.93 395.662 1 2 -12 -10 158.741 74.8902 5 2 -12 -10 163.991 79.7720 4 -2 -12 10 105.088 190.686 1 2 -12 -9-83.1124 67.7692 5 2 -12 -9 66.7828 58.2632 4 2 -12 -8 219.234 69.1291 5 2 -12 -8 207.735 67.1185 4 2 12 -8 6.25355 103.380 6 2 -12 -7 832.138 116.286 5 2 -12 -7 531.297 91.6949 4 2 12 -7 1131.56 264.233 6 2 -12 -6 676.582 96.1008 4 2 -12 -6 719.692 113.379 5 2 12 -6 899.757 235.357 6 2 12 -5 412.034 195.127 6 -2 -12 5 264.901 74.0173 5 -2 12 5 499.775 185.892 6 2 -12 -5 223.166 80.3375 5 -2 -12 4 690.871 99.4572 5 -2 12 4 630.335 193.743 6 2 12 -4 774.368 240.842 6 2 -12 -4 640.472 107.252 5 2 -12 -3 6964.54 311.882 5 -2 -12 3 6941.36 302.055 5 2 12 -3 6806.56 617.992 6 -2 12 3 6805.86 590.657 6 -2 -12 2 2539.31 185.691 5 -2 12 2 2696.04 368.455 6 2 -12 -2 2561.13 193.125 5 2 12 -2 2544.23 382.413 6 2 12 -1 2357.72 374.720 6 2 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267.996 84.2703 5 -2 -12 -14-148.144 74.3688 5 2 -12 14 49.1331 251.658 1 -2 -12 -15 600.827 111.906 5 2 -12 15 548.478 223.520 1 -2 -12 -16 931.766 129.585 5 -2 -12 -16 1028.19 136.974 2 -2 -12 -17 76.6048 67.1680 5 -2 -12 -17 27.2567 63.4142 2 -2 -12 -18 2137.15 203.488 2 -2 -12 -18 2097.76 174.472 5 -2 -12 -19 118.363 76.4748 2 -2 -12 -20 216.542 80.1330 2 -2 -12 -21 551.711 117.879 2 -2 -12 -22 434.104 102.972 2 -2 -12 -23 1070.50 145.111 2 -2 -12 -24-29.9505 61.9012 2 -2 -12 -25 733.081 123.422 2 -2 -12 -26 907.296 123.827 2 -2 -12 -27 1207.65 130.513 2 -2 -12 -28 46.0795 50.7222 2 -2 -12 -29 25.0090 41.5148 2 -2 -12 -30 23.0108 32.3114 2 2 -13 -30 161.316 45.6970 4 2 -13 -29 795.285 85.9107 4 2 -13 -28 39.8608 43.0024 4 2 -13 -27 198.854 64.3106 4 2 -13 -26 220.102 72.3163 4 2 -13 -25 168.672 70.8085 4 2 -13 -24 1782.35 170.270 4 2 -13 -24 1609.37 154.619 2 2 -13 -23 927.113 123.332 2 2 -13 -22 135.144 64.9384 2 2 -13 -21 135.574 67.2520 2 2 -13 -20 934.239 127.329 2 2 -13 -19 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145.657 5 2 13 11 1275.41 337.579 6 2 -13 11 636.978 259.542 1 -2 -13 -12 53.6854 73.1322 5 2 13 12 305.832 150.954 6 -2 -13 -13 356.624 92.2884 5 2 -13 13 823.226 281.492 1 -2 -13 -14 115.388 81.6469 5 -2 -13 -15 1404.20 154.882 5 -2 -13 -16 2444.63 196.848 5 -2 -13 -17 335.445 92.5279 5 -2 -13 -18 72.6363 64.8291 5 -2 -13 -18-31.2787 70.6800 2 -2 -13 -19 233.580 77.0208 2 -2 -13 -19 325.954 75.8729 5 -2 -13 -20 1004.99 138.053 2 -2 -13 -21 477.557 106.116 2 -2 -13 -22 460.666 93.9970 2 -2 -13 -23 323.337 84.0430 2 -2 -13 -24-53.7625 54.2101 2 -2 -13 -25 989.911 119.040 2 -2 -13 -26 78.1703 53.5462 2 -2 -13 -27 141.457 50.2348 2 -2 -13 -28-32.4864 39.4201 2 -2 -13 -28 89.0968 40.8715 4 -2 -13 -29 244.716 44.5406 4 2 -14 -29 189.215 41.1948 4 2 -14 -28 119.766 44.0602 4 2 -14 -27 49.7132 42.6941 4 2 -14 -26 38.9624 45.8629 4 2 -14 -25 73.3576 48.7544 4 2 -14 -24 442.759 86.3093 4 2 -14 -23-17.5550 62.6618 4 2 -14 -22 338.270 92.1393 4 2 -14 -21 203.598 73.9886 4 2 -14 -20-38.7674 63.8336 4 2 -14 -19 2459.85 180.617 5 2 -14 -19 2552.18 208.967 4 2 -14 -18 1188.01 148.887 4 2 -14 -18 1034.16 132.264 5 2 -14 -17 4.36469 69.0948 4 2 -14 -17 48.4317 59.1978 5 2 -14 -16 631.896 115.960 5 2 -14 -16 560.742 114.675 4 2 -14 -15 1010.88 137.222 5 2 -14 -15 777.364 124.492 4 2 -14 -14 3.33567 66.2596 4 2 -14 -14 105.908 76.2649 5 2 -14 -13 2119.49 193.987 5 2 -14 -13 1965.24 190.508 4 2 -14 -12 156.021 77.1578 4 2 -14 -12-10.3777 69.9138 5 2 -14 -11 8.22762 64.0272 4 2 -14 -11-90.0673 86.2747 5 2 -14 -10 2222.67 197.822 5 2 -14 -10 2160.04 185.883 4 2 -14 -9 73.9905 66.0921 4 2 -14 -9 169.884 89.9087 5 2 -14 -8 73.5964 74.1780 5 2 -14 -8 130.314 68.1328 4 2 -14 -7 2431.39 210.629 5 2 -14 -7 2491.06 194.929 4 -2 -14 6 4864.39 269.329 5 2 -14 -6 5457.98 307.990 5 2 -14 -6 4655.25 260.488 4 -2 -14 5 1302.60 144.449 5 2 -14 -5 910.083 137.138 5 2 -14 -4 128.006 82.9966 5 -2 -14 4 56.4749 66.3276 5 2 -14 -3 121.930 75.5197 5 -2 -14 3 126.402 58.1821 5 2 -14 -2 935.619 134.379 5 -2 -14 2 848.069 128.086 5 2 14 -2 660.304 228.979 6 -2 -14 1 1231.12 148.988 5 2 -14 -1 1335.40 153.818 5 2 14 -1 1638.76 338.615 6 2 -14 0 533.496 104.869 5 -2 -14 0 602.470 114.043 5 2 14 0 312.378 173.836 6 -2 -14 -1 16.5822 57.1302 5 2 -14 1 86.1511 67.6098 5 -2 -14 -2 15550.1 505.660 5 2 -14 2 15055.1 486.490 5 2 14 2 14979.2 1029.26 6 -2 -14 -3 622.698 118.545 5 2 -14 3 583.447 109.048 5 2 14 3 403.341 192.054 6 2 -14 4 8120.05 352.290 5 2 14 4 7959.14 764.728 6 -2 -14 -4 8680.73 380.805 5 2 -14 5 224.121 69.7924 5 2 14 5 221.060 151.730 6 -2 -14 -5 308.487 103.726 5 -2 -14 -6 216.845 77.6285 5 2 14 6 337.059 108.290 6 2 -14 6 464.820 90.6491 5 -2 -14 -7 840.743 133.456 5 2 14 7 398.050 214.044 6 -2 -14 -8 1395.78 169.688 5 2 14 8 1564.44 380.031 6 -2 -14 -9 99.7953 77.9966 5 2 14 9-56.6759 132.858 6 -2 -14 -10 1064.63 150.194 5 2 14 10 813.819 282.560 6 -2 -14 -11 147.727 76.3071 5 -2 -14 -12 12.9932 65.2236 5 -2 -14 -13 2472.48 210.905 5 -2 -14 -14 1500.82 163.901 5 -2 -14 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303.515 6 4 -7 3 2171.93 266.624 1 4 -7 4-10.9986 87.6461 1 4 -7 5 903.774 203.139 1 4 -7 6 14.0532 104.910 1 4 -7 7 1109.20 240.295 1 4 -7 8 10.3790 119.097 1 4 -7 9-6.06491 113.505 1 4 -7 10 191.520 109.946 1 4 -7 11 5802.34 551.979 1 4 -7 12 398.790 158.075 1 4 -7 13 131.900 155.000 1 4 -7 14 3246.48 457.012 1 -4 -7 -15 1917.00 174.689 2 4 -7 15 1218.36 303.138 1 4 -7 16-637.375 237.018 1 -4 -7 -16-11.7767 58.3585 2 4 -7 17 3620.61 520.470 1 -4 -7 -17 3551.69 245.413 2 4 -7 18 524.705 211.154 1 -4 -7 -18 575.855 114.257 2 -4 -7 -19 1290.20 163.430 2 4 -7 19 1624.62 363.735 1 4 7 20-87.3726 140.771 1 4 -7 20-68.7326 155.920 1 -4 -7 -20 30.1142 71.5587 2 -4 -7 -21 60.4377 75.8077 2 4 -7 21-3.84867 115.337 1 4 7 21 50.7032 117.094 1 -4 -7 -22 35.7268 75.6835 2 4 -7 22 108.675 141.924 1 -4 -7 -23-10.1714 72.7598 2 -4 -7 -24 494.652 120.807 2 -4 -7 -25 18.1042 90.1135 2 -4 -7 -26 216.401 95.4282 2 -4 -7 -27 1723.74 194.670 2 -4 -7 -28-110.068 96.6905 2 -4 -7 -29-31.4922 80.1475 2 -4 -7 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269.012 6 -4 -8 19 1353.67 298.685 1 4 -8 -19 1320.69 162.711 2 4 8 -19 1260.92 146.571 3 -4 -8 18 825.964 216.575 1 4 8 -18 776.242 117.822 3 4 -8 -18 1018.29 139.033 2 4 8 -18 875.031 239.570 6 4 -8 -17 3493.27 240.814 2 4 8 -17 3652.34 230.649 3 -4 -8 17 3734.55 490.760 1 4 8 -17 3779.40 473.195 6 -4 -8 16 3081.52 437.829 1 4 -8 -16 3163.38 225.705 2 4 8 -16 3270.99 431.613 6 -4 -8 15 7001.07 643.693 1 4 8 -15 6639.97 617.003 6 -4 -8 14 760.802 231.315 1 4 8 -14 1195.56 253.719 6 -4 -8 13 1609.94 300.131 1 4 8 -13 990.999 230.804 6 -4 -8 12-15.0616 126.445 1 4 8 -12 80.6306 93.1325 6 -4 -8 11 632.557 204.414 1 4 8 -11 869.353 227.509 6 -4 -8 10 2143.39 325.882 1 4 8 -10 2135.99 317.371 6 4 8 -9 2392.78 335.952 6 -4 -8 9 2830.58 372.434 1 -4 -8 8 2044.25 317.839 1 4 8 -8 2058.28 304.720 6 -4 -8 7 1598.29 282.766 1 4 8 -7 1297.17 243.573 6 4 8 -6 2099.43 309.798 6 -4 -8 6 1622.95 293.753 1 4 8 -5 21341.8 922.726 6 4 8 -4 34.0596 105.910 6 4 8 -3 84.7151 108.236 6 4 8 -2 15483.0 777.035 6 4 -8 -1 1334.48 213.457 1 4 8 -1 1127.14 209.548 6 -4 8 0 2.34100 63.1682 6 4 -8 0 8.43949 83.8590 1 4 8 0-35.4091 113.980 6 -4 8 -1 265.685 71.4524 6 4 8 1 52.3511 115.029 6 4 -8 1-22.6651 76.5749 1 4 -8 2 8589.60 545.037 1 4 8 2 9427.81 619.679 6 4 -8 3 8460.43 551.152 1 4 8 3 9751.99 645.329 6 4 -8 4 9176.12 594.863 1 4 -8 5 16555.1 818.210 1 4 -8 6 65.1437 122.512 1 4 -8 7-52.8759 100.106 1 4 -8 8 5714.61 524.642 1 4 -8 9 5274.08 511.867 1 4 -8 10 1342.19 271.929 1 4 -8 11 7656.99 664.524 1 4 -8 12 108.256 119.995 1 4 -8 13 15476.2 985.301 1 4 -8 14 67.2781 171.050 1 -4 -8 -14 155.062 59.9267 2 -4 -8 -15 76.6521 48.6977 2 4 -8 15 7.85957 93.9131 1 -4 -8 -16 266.900 85.5198 2 4 -8 16 333.118 167.068 1 4 -8 17 2808.67 466.430 1 -4 -8 -17 2879.41 225.490 2 -4 -8 -18 1249.02 155.826 2 4 -8 18 1406.60 347.860 1 4 -8 19-44.8082 134.054 1 -4 -8 -19 347.008 109.923 2 4 -8 20-15.4317 173.246 1 4 8 20 15.3393 123.347 1 -4 -8 -20 78.8656 81.2617 2 4 8 21 938.076 291.233 1 4 -8 21 1088.77 311.318 1 -4 -8 -21 1096.91 163.122 2 -4 -8 -22 47.3863 77.2888 2 -4 -8 -23 13.2510 74.3894 2 -4 -8 -24 4075.90 293.745 2 -4 -8 -25 1315.19 178.935 2 -4 -8 -26-82.2102 87.4606 2 -4 -8 -27 23.8366 89.2551 2 -4 -8 -28 1333.37 167.609 2 -4 8 -29 1894.82 154.936 3 -4 -8 -29 1874.75 187.358 2 -4 8 -30 115.289 45.6269 3 -4 -8 -30 113.826 66.7928 2 -4 8 -31-8.64785 40.3050 3 -4 -8 -31-16.2669 55.7511 2 -4 8 -32 9.23493 30.6597 3 -4 -8 -32 59.5776 54.8581 2 -4 -8 -33 108.596 44.7693 2 -4 -8 -34 52.9599 34.8002 2 4 -9 -34 32.8762 30.2150 4 4 9 -33 448.958 64.6761 3 4 -9 -33 614.057 78.9884 4 4 -9 -32 112.195 55.6763 4 4 9 -32-37.8143 43.9709 3 4 9 -31 244.246 69.1083 3 4 9 -30 231.126 68.5456 3 4 9 -29 1247.16 134.704 3 4 -9 -28 530.160 116.620 2 4 9 -28 564.395 100.234 3 4 9 -27 1709.30 169.587 3 4 -9 -27 1368.70 174.303 2 4 -9 -26 61.4794 75.8450 2 4 9 -26-24.7435 65.4593 3 4 -9 -25 1056.08 157.693 2 4 9 -25 1092.43 141.823 3 4 9 -24 319.586 100.973 3 4 -9 -24 219.398 91.8010 2 4 -9 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161.951 6 5 6 -2 12025.1 628.702 6 5 -6 -2 11228.6 462.393 1 5 -6 -1 28.1691 59.1218 1 5 6 -1-24.1640 122.079 6 5 6 0 19096.8 784.763 6 5 -6 0 18809.1 642.315 1 5 -6 1 119.924 73.1028 1 -5 6 -1 157.980 43.3731 6 5 6 1 47.0439 90.6566 6 5 -6 2 5357.21 367.690 1 5 6 2 5597.45 435.774 6 5 -6 3 73.2050 69.0551 1 5 6 3-53.8013 124.923 6 5 -6 4 21662.7 792.687 1 5 -6 5 8532.52 520.334 1 5 -6 6 93.9001 98.7484 1 5 -6 7 1286.30 220.076 1 5 -6 8 202.854 125.143 1 5 -6 9 553.910 193.068 1 5 -6 10 418.135 178.702 1 5 -6 11 6284.03 561.574 1 5 -6 12 195.882 147.049 1 5 -6 13 1298.17 281.398 1 5 -6 14 223.130 143.647 1 5 -6 15 952.693 266.138 1 -5 -6 -16 897.834 123.031 2 5 -6 16 1002.48 274.860 1 5 -6 17 1916.47 379.885 1 -5 -6 -17 2153.25 194.691 2 -5 -6 -18 1189.16 148.692 2 5 -6 18 879.741 271.303 1 5 6 19 109.716 154.691 1 -5 -6 -19 45.6857 62.4499 2 5 -6 19 49.0296 109.594 1 5 6 20 1941.71 382.482 1 -5 -6 -20 1671.40 184.270 2 5 -6 20 1915.66 404.529 1 5 6 21 348.471 171.140 1 5 -6 21 440.562 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143.353 1 5 -7 17 3529.57 517.806 1 -5 -7 -17 4297.02 274.050 2 -5 -7 -18 1625.73 174.963 2 5 -7 18 1530.43 364.105 1 -5 -7 -19 3370.33 253.605 2 5 -7 19 3030.67 514.708 1 5 7 20 63.9416 135.401 1 5 -7 20-72.9929 149.129 1 -5 -7 -20 82.7686 68.0532 2 -5 -7 -21 373.198 107.411 2 5 7 21 444.297 180.054 1 5 -7 21 29.6981 129.457 1 -5 -7 -22 46.9493 73.9597 2 -5 -7 -23 565.457 133.782 2 -5 -7 -24 64.9131 80.3923 2 -5 -7 -25 159.528 96.3984 2 -5 -7 -26 81.8968 78.3800 2 -5 -7 -27 635.725 131.059 2 -5 -7 -28 234.829 100.587 2 -5 -7 -29 1056.11 139.094 2 -5 -7 -30-29.3457 62.3675 2 -5 7 -31 92.0231 51.3352 3 -5 -7 -31 153.763 69.2690 2 -5 7 -32 208.173 54.1408 3 -5 -7 -32 245.308 73.4597 2 -5 -7 -33 282.922 63.5196 2 -5 7 -33 156.195 40.5917 3 -5 -7 -34 250.307 49.6311 2 5 8 -34 11.5155 32.9219 3 5 -8 -34-19.9313 32.8670 4 5 8 -33 285.415 61.0143 3 5 -8 -33 189.845 52.1330 4 5 8 -32 96.4047 47.5249 3 5 8 -31 482.947 92.4745 3 5 8 -30 1347.24 142.549 3 5 8 -29 632.566 113.079 3 5 8 -28 109.247 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473.503 1 5 -8 12 1421.68 314.305 1 5 -8 13 298.092 180.978 1 -5 -8 -13 525.587 94.8368 2 -5 -8 -14 939.381 126.186 2 5 -8 14 932.822 277.406 1 5 -8 14 875.052 113.505 4 5 -8 15 36.6179 42.6643 4 5 -8 15 204.890 172.276 1 -5 -8 -15 85.3410 59.5305 2 -5 -8 -16 956.624 134.126 2 5 -8 16 1103.96 307.546 1 5 -8 17 5336.09 667.314 1 -5 -8 -17 5361.76 311.857 2 5 -8 18 630.645 274.105 1 -5 -8 -18 627.695 125.739 2 -5 -8 -19 6481.93 351.938 2 5 -8 19 6026.65 717.648 1 5 8 20 71.2876 192.363 1 -5 -8 -20 27.3422 71.3645 2 -5 -8 -21 647.218 135.647 2 -5 -8 -22 157.320 92.0891 2 -5 -8 -23 796.763 144.013 2 -5 -8 -24 751.672 147.346 2 -5 -8 -25 406.002 130.320 2 -5 -8 -26 390.082 109.115 2 -5 -8 -27 174.401 93.3320 2 -5 -8 -28 36.5349 69.4243 2 -5 -8 -29 118.536 71.0669 2 -5 -8 -30 20.5397 59.3785 2 -5 8 -30 20.1674 47.0571 3 -5 -8 -31 992.663 117.122 2 -5 8 -31 772.677 82.8074 3 -5 -8 -32-14.2889 48.2517 2 -5 -8 -33 178.206 47.7714 2 5 -9 -34 110.213 35.4783 4 5 9 -33 45.4367 35.1249 3 5 -9 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871.427 116.044 2 -5 -9 -31 45.7466 52.3335 2 -5 -9 -32 116.802 47.0152 2 5 -10 -33 105.823 37.7265 4 5 -10 -32 256.919 56.8966 4 5 10 -31 19.6418 32.9135 3 5 -10 -31 81.7329 53.2614 4 5 -10 -30 355.999 81.0161 4 5 10 -30 344.739 65.3023 3 5 10 -29 110.646 62.2330 3 5 -10 -29 91.9195 58.7694 4 5 10 -28 188.566 61.4099 3 5 10 -27 55.9773 56.1585 3 5 10 -26 55.9233 51.6647 3 5 10 -25 1183.19 142.813 3 5 -10 -25 1140.96 159.247 2 5 -10 -24 1279.26 170.931 2 5 10 -24 1241.71 148.662 3 5 -10 -23-66.4058 75.7187 2 5 10 -23 130.557 75.2998 3 5 -10 -22 2273.04 212.735 2 5 10 -22 2577.78 202.662 3 5 10 -21 30.8395 52.4912 3 5 -10 -21 55.5259 71.7207 2 5 10 -20 267.220 77.0494 3 5 -10 -20 200.193 80.2983 2 5 -10 -19 244.699 85.0223 2 5 10 -19 294.193 86.0008 3 -5 -10 19 218.587 174.534 1 -5 -10 18 3020.62 486.810 1 5 -10 -18 3416.34 249.591 2 5 10 -18 3580.54 494.755 6 5 -10 -17 1002.73 129.599 5 5 -10 -17 986.505 142.677 2 -5 -10 17 933.992 278.806 1 5 10 -16 3740.35 517.282 6 5 -10 -16 3090.54 228.679 2 -5 -10 16 3656.63 533.820 1 5 -10 -16 3276.63 216.120 5 5 -10 -15 567.107 109.339 2 5 10 -15 436.730 172.030 6 5 -10 -15 507.481 98.7125 5 -5 -10 15 713.554 251.999 1 5 10 -14 1066.86 278.661 6 5 -10 -14 1584.70 154.013 5 5 10 -13 1823.56 349.615 6 5 -10 -13 2170.81 175.981 5 -5 -10 13 2374.51 406.948 1 5 -10 -12 1266.68 140.147 5 5 10 -12 1166.62 280.281 6 5 -10 -11 3521.80 222.505 5 5 10 -11 3825.09 487.396 6 5 -10 -10 15358.9 451.657 5 5 -10 -10 15516.3 468.108 4 5 10 -10 15578.0 968.532 6 5 -10 -9 5265.75 264.233 5 5 -10 -9 5032.81 267.426 4 5 10 -9 5483.16 561.225 6 5 10 -8 876.203 234.500 6 5 10 -7 641.561 225.087 6 5 10 -6 8539.52 690.474 6 5 10 -5 7097.55 622.781 6 5 10 -4-59.0079 114.763 6 5 10 -3 230.908 146.923 6 5 10 -2 16.7121 123.194 6 5 10 -1 2008.94 336.791 6 5 10 0 92.6833 90.7904 6 5 10 1 1489.70 302.107 6 5 -10 1 1308.28 251.072 1 5 -10 2 59.0712 92.5542 1 5 10 2 65.0298 97.9191 6 5 -10 3 255.160 150.963 1 5 10 3-101.999 156.957 6 5 10 4 332.236 204.019 6 5 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144.841 2 -5 -10 -23 1130.42 159.733 2 -5 -10 -24 422.722 108.455 2 -5 -10 -25 207.759 92.0394 2 -5 -10 -26 368.972 89.8966 2 -5 -10 -27 57.9703 63.1615 2 -5 -10 -28 379.652 91.4041 2 -5 -10 -29 38.4292 54.6399 2 -5 -10 -30 30.6256 50.6190 2 -5 -10 -31-21.1726 40.0180 2 5 -11 -32 45.9850 33.1508 4 5 -11 -31 856.504 91.8766 4 5 -11 -30 53.6605 45.4407 4 5 -11 -29 54.0506 52.9417 4 5 -11 -28 45.8401 55.7708 4 5 -11 -27 618.265 112.665 4 5 -11 -26 984.493 141.729 4 5 -11 -22 2757.48 230.009 2 5 -11 -21 297.743 85.2042 2 5 -11 -20 47.5564 64.2562 2 5 -11 -19 1609.95 177.718 2 5 -11 -18 1060.33 128.628 5 5 -11 -18 1009.84 140.397 2 5 -11 -17 583.172 114.517 2 5 -11 -17 640.770 104.027 5 -5 -11 17 797.930 272.581 1 5 -11 -16 471.623 100.823 5 5 -11 -16 361.469 89.2547 2 5 -11 -15 1474.33 158.444 5 5 11 -15 2029.38 372.100 6 5 11 -14 341.840 183.276 6 5 -11 -14 52.7579 53.2766 5 5 -11 -13 1335.46 153.035 5 5 -11 -13 1204.64 151.564 4 5 11 -13 886.152 259.919 6 5 -11 -12 418.631 92.7177 5 5 11 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181.272 6 5 -11 3 227.292 68.5814 5 5 11 3 299.269 151.804 6 5 -11 3 314.104 169.682 1 5 -11 4 337.895 77.5135 5 5 11 4 339.396 221.001 6 5 -11 4 350.098 159.239 1 5 11 5 628.202 223.124 6 5 -11 5 565.439 93.9079 5 5 -11 5 688.980 214.391 1 5 -11 5 583.543 93.8144 4 5 -11 6 1140.24 131.285 5 5 -11 6 936.473 240.244 1 5 -11 6 1052.97 119.960 4 5 11 6 1192.94 319.274 6 5 -11 7 6562.18 644.208 1 5 11 7 5517.68 616.630 6 5 -11 7 5511.78 266.156 4 5 -11 8 378.411 80.5824 4 5 11 8 498.742 231.352 6 5 -11 8 680.703 231.663 1 5 -11 9-8.01891 45.1212 4 5 11 9-63.8492 207.011 6 5 -11 9 154.005 204.397 1 5 -11 10 3854.19 224.811 4 5 11 10 3949.68 549.545 6 5 -11 10 3790.86 531.228 1 5 -11 11 403.835 232.786 1 5 11 11 538.956 229.372 6 -5 -11 -12 477.057 98.1255 2 5 -11 12 1200.24 319.249 1 5 11 12 920.365 307.605 6 5 -11 13 360.968 212.257 1 -5 -11 -13 129.616 67.9775 2 5 -11 14 720.501 268.625 1 -5 -11 -14 528.206 107.484 2 5 -11 15 224.500 194.138 1 -5 -11 -15 60.6443 59.1594 5 -5 -11 -15 28.9936 61.8131 2 -5 -11 -16 1398.34 148.343 5 -5 -11 -16 1381.84 164.397 2 -5 -11 -17 94.0703 78.7096 2 -5 -11 -17-22.2125 50.8991 5 -5 -11 -18 29.5952 48.4190 5 -5 -11 -18 65.0285 61.0666 2 -5 -11 -19 110.938 71.7138 2 -5 -11 -20 15.8085 69.5015 2 -5 -11 -21 42.8362 73.2763 2 -5 -11 -22 14.8834 68.1228 2 -5 -11 -23-20.8660 71.9510 2 -5 -11 -24 458.558 105.125 2 -5 -11 -25 35.1770 68.3912 2 -5 -11 -26 591.854 111.775 2 -5 -11 -27 538.590 96.0398 2 -5 -11 -28 104.027 60.7191 2 -5 -11 -29 70.5980 45.7121 2 -5 -11 -30 34.5607 35.2810 2 5 -12 -31 56.1553 33.2748 4 5 -12 -30 201.695 49.1530 4 5 -12 -29 766.451 93.0477 4 5 -12 -28 162.887 56.0169 4 5 -12 -27-29.2078 66.1807 4 5 -12 -26 16.0939 60.7390 4 5 -12 -25 295.752 84.9486 4 5 -12 -24 867.941 132.299 4 5 -12 -23 164.505 90.2273 4 5 -12 -22-21.5548 78.4518 4 5 -12 -21 122.610 90.3623 4 5 -12 -20-33.3947 86.1148 4 5 -12 -19 938.266 147.841 4 5 -12 -18 764.974 122.170 5 5 -12 -18 759.997 139.473 4 5 -12 -17 5716.37 325.636 4 5 -12 -17 5527.73 292.344 5 5 -12 -16 525.421 103.279 5 5 -12 -16 693.093 128.774 4 5 -12 -15 164.318 70.1984 5 5 -12 -15 193.139 81.4682 4 5 -12 -14 1271.05 153.982 5 5 -12 -14 1149.58 154.598 4 5 -12 -13 1913.10 187.238 5 5 12 -13 1924.03 378.017 6 5 -12 -13 2273.21 205.474 4 5 12 -12 1893.91 372.197 6 5 -12 -12 2172.78 192.307 5 5 -12 -12 2348.70 208.071 4 5 -12 -11 77.3584 59.9214 5 5 -12 -11 43.6111 69.8191 4 5 12 -11 201.954 156.121 6 5 -12 -10 149.571 63.5781 4 5 -12 -10 205.595 85.2570 5 5 12 -10 284.640 158.971 6 5 -12 -9 1380.07 153.085 5 5 -12 -9 1194.23 142.995 4 5 12 -9 1469.76 328.198 6 5 -12 -8 1133.15 143.335 5 5 -12 -8 910.982 130.378 4 5 -12 -7 1926.63 182.036 5 5 12 -7 2035.73 380.309 6 5 -12 -7 2099.83 180.904 4 5 12 -6 783.328 245.791 6 5 -12 -6 799.654 110.677 4 5 -12 -6 558.177 105.911 5 5 -12 -5 155.087 70.0901 5 5 12 -5 172.303 161.482 6 5 -12 -5 137.852 65.2840 4 5 -12 -4 455.583 95.8629 5 5 12 -4 718.378 241.606 6 5 -12 -4 502.904 99.1614 4 5 -12 -3 6021.36 293.226 4 5 12 -3 5951.22 633.549 6 5 -12 -3 6399.32 309.593 5 5 -12 -2 2712.40 209.555 5 5 -12 -2 2422.97 189.232 4 5 12 -2 2787.01 434.579 6 5 -12 -1 632.744 109.395 5 5 -12 -1 484.214 88.8952 4 5 12 -1 438.683 163.681 6 5 -12 0 33.8727 48.7932 4 5 12 0 42.0708 116.075 6 5 -12 0 70.4768 72.6625 5 5 -12 1 14056.9 436.261 4 5 12 1 14611.8 996.310 6 5 -12 1 14264.3 454.746 5 5 -12 2 306.074 82.0882 5 5 12 2 497.166 232.052 6 5 -12 2 390.952 74.9621 4 5 12 3 428.977 190.966 6 5 -12 3 551.465 96.9731 4 5 -12 3 582.931 100.397 5 5 12 4-56.7774 202.689 6 5 -12 4 106.710 58.1650 4 5 -12 4 11.7496 51.7534 5 5 -12 5 3841.12 230.033 4 5 12 5 3933.94 528.624 6 5 -12 5 3785.95 502.848 1 5 -12 5 4293.93 248.418 5 5 -12 6 639.632 98.7622 5 5 -12 6 738.937 104.211 4 5 -12 6 582.833 224.917 1 5 12 6 587.245 202.168 6 5 -12 7 1881.64 379.961 1 5 -12 7 1575.60 151.833 4 5 12 7 1881.85 374.754 6 5 -12 7 1731.27 154.133 5 5 -12 8 1228.52 307.490 1 5 12 8 1078.12 296.151 6 5 12 9 1944.35 407.499 6 5 -12 9 1606.68 348.982 1 5 -12 10 98.8447 147.881 1 5 12 10 117.555 137.157 6 5 -12 11 1019.94 293.926 1 5 12 11 993.677 312.464 6 5 12 12-53.7885 143.576 6 5 -12 12 29.9031 174.078 1 -5 -12 -13 3221.64 233.648 5 5 -12 13 3635.71 564.096 1 5 12 13 3814.02 570.455 6 -5 -12 -14 2496.85 204.337 2 -5 -12 -14 2845.36 217.641 5 -5 -12 -15 1011.50 134.155 5 -5 -12 -15 1043.43 139.541 2 -5 -12 -16 94.4646 72.6603 5 -5 -12 -16 111.963 68.8776 2 -5 -12 -17 97.8523 69.8303 2 -5 -12 -17 142.734 69.3240 5 -5 -12 -18 705.307 105.764 5 -5 -12 -18 758.638 129.347 2 -5 -12 -19 659.369 122.761 2 -5 -12 -20 43.9739 77.5108 2 -5 -12 -21 419.422 106.087 2 -5 -12 -22 529.477 113.737 2 -5 -12 -23 233.212 81.7155 2 -5 -12 -24 300.353 79.5049 2 -5 -12 -25 613.779 101.496 2 -5 -12 -26 18.9071 51.4596 2 -5 -12 -27 211.489 63.5252 2 -5 -12 -28 63.2080 40.3124 2 -5 -12 -29 128.969 41.5046 2 5 -13 -30 71.0095 30.7404 4 5 -13 -29 175.785 49.7570 4 5 -13 -28 22.5475 41.6767 4 5 -13 -27 127.954 58.9558 4 5 -13 -26 6.13718 53.4288 4 5 -13 -25 280.743 80.9412 4 5 -13 -24-38.3076 68.7595 4 5 -13 -23 375.686 99.9364 4 5 -13 -22 58.2376 74.9854 4 5 -13 -21 351.468 95.3587 4 5 -13 -20 12.4167 78.5775 4 5 -13 -19 1002.59 149.766 4 5 -13 -19 928.399 123.913 5 5 -13 -18 160.945 66.0691 5 5 -13 -18 49.9537 72.5372 4 5 -13 -17 734.220 117.249 5 5 -13 -17 842.634 148.538 4 5 -13 -16 152.846 78.1023 5 5 -13 -16 165.010 82.7605 4 5 -13 -15 469.484 100.944 5 5 -13 -15 513.455 113.888 4 5 -13 -14 28.5617 69.3321 5 5 -13 -14 24.0654 69.1962 4 5 -13 -13 460.876 105.193 5 5 -13 -13 510.350 115.778 4 5 -13 -12 12.8972 74.5300 5 5 -13 -12 47.9720 81.9185 4 5 -13 -11 1703.06 178.588 4 5 -13 -11 1621.76 176.060 5 5 13 -11 1767.05 369.767 6 5 -13 -10 3966.95 266.392 4 5 13 -10 4523.09 589.050 6 5 -13 -10 3879.66 262.887 5 5 13 -9 3028.37 471.957 6 5 -13 -9 3493.07 243.598 4 5 -13 -9 3582.77 249.747 5 5 -13 -8 2361.16 200.764 4 5 -13 -8 2074.70 194.218 5 5 -13 -7 1649.54 172.725 5 5 -13 -7 1481.31 157.449 4 5 13 -7 1476.25 330.658 6 -5 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899.250 86.7915 4 6 5 -34 1191.84 124.573 3 6 5 -33 203.130 79.8518 3 6 5 -32 103.013 73.4092 3 6 5 -31 263.388 90.4963 3 6 5 -30 66.3779 80.5335 3 6 5 -29 784.471 144.794 3 6 5 -28 442.489 111.676 3 6 5 -27-12.3550 74.3972 3 6 -5 -27 22.0245 90.7749 2 6 5 -26 48.5771 81.7666 3 6 -5 -26 220.819 95.1737 2 6 5 -25 269.396 94.7105 3 6 -5 -25 420.024 120.190 2 6 5 -24 3493.72 261.680 3 6 -5 -24 3286.83 267.253 2 6 5 -23 63.1310 68.7006 3 6 -5 -23 225.679 106.207 2 6 5 -22 742.309 126.298 3 6 5 -22 736.362 288.865 6 6 -5 -22 1160.84 161.428 2 6 -5 -21 1963.64 195.326 2 6 5 -21 1832.79 365.394 6 6 5 -21 1946.80 190.919 3 6 5 -20 8352.57 367.477 3 6 -5 -20 7870.24 374.995 2 6 5 -19 1048.78 296.113 6 6 5 -19 1294.14 146.644 3 6 -5 -19 1288.46 154.695 2 6 5 -18 89.3476 115.108 6 6 5 -18 169.889 66.7670 3 6 -5 -18 227.709 80.7761 2 6 5 -17 381.874 165.317 6 -6 -5 17 338.212 143.641 1 6 5 -16 1998.22 345.164 6 -6 -5 16 1870.95 291.160 1 6 5 -15 86.2290 127.046 6 -6 -5 15 37.9648 91.0981 1 6 5 -14 249.827 179.488 6 -6 -5 14 261.569 133.657 1 6 5 -13 1935.54 323.470 6 -6 -5 13 2083.85 277.991 1 6 5 -12 2061.68 324.550 6 -6 -5 12 2135.54 277.130 1 6 5 -11 1558.73 272.051 6 -6 -5 11 1736.62 254.029 1 -6 -5 10 2278.14 270.611 1 6 5 -10 2033.96 305.658 6 6 5 -9 1775.51 285.743 6 -6 -5 9 1600.23 230.857 1 -6 -5 8 6626.91 445.465 1 6 5 -8 6087.76 488.846 6 6 5 -7 765.311 194.767 6 6 5 -6 34997.8 1115.35 6 6 5 -5 6306.61 469.030 6 6 5 -4 3141.95 336.329 6 6 5 -3 0.70478 111.949 6 6 5 -2 269.573 148.734 6 6 -5 -2 266.747 72.7245 1 6 5 -1 179.329 126.525 6 6 -5 -1 189.552 68.2821 1 6 5 0 6891.08 472.022 6 6 -5 0 6780.05 349.842 1 6 5 1 5250.66 405.920 6 6 -5 1 5095.91 324.487 1 6 -5 2 223.810 98.8400 1 6 5 2 131.480 95.1801 6 6 -5 3 1980.98 227.474 1 6 5 3 1912.08 257.368 6 6 5 4 111.658 102.319 6 6 -5 4 167.487 70.4296 1 6 -5 5 1823.98 238.659 1 6 5 5 1777.62 245.010 6 6 -5 6 4265.57 375.994 1 6 -5 7 5012.80 432.268 1 6 -5 8 1846.05 269.540 1 6 -5 9 384.264 130.953 1 6 -5 10 5530.48 505.850 1 6 -5 11 152.305 136.233 1 6 -5 12 16.1771 122.810 1 6 -5 13 3394.73 438.304 1 6 -5 14 3849.06 487.161 1 6 -5 15 223.933 162.142 1 -6 -5 -15 283.197 80.0532 2 -6 -5 -16 602.206 103.025 2 6 -5 16 620.366 205.214 1 -6 -5 -17 6675.31 331.783 2 6 -5 17 6599.68 684.065 1 -6 -5 -18 245.439 78.5576 2 6 5 18-67.6135 133.592 1 6 -5 18 180.736 128.842 1 6 -5 19-59.1949 151.869 1 -6 -5 -19-130.365 87.5755 2 6 5 19-469.336 202.918 1 6 -5 20 5179.41 657.472 1 -6 -5 -20 4513.19 291.804 2 6 5 20 4349.28 569.130 1 6 5 21 946.350 286.512 1 6 -5 21 978.228 303.853 1 -6 -5 -21 548.565 125.044 2 -6 -5 -22 386.896 107.715 2 6 5 22 587.644 241.669 1 6 -5 22 225.015 169.104 1 -6 -5 -23 1248.64 173.232 2 -6 -5 -24 1495.85 191.773 2 -6 -5 -25-211.720 106.664 2 -6 -5 -26 258.706 97.6043 2 -6 -5 -27 26.6546 72.2776 2 -6 -5 -28 178.902 90.7268 2 -6 -5 -29 2.54889 72.7435 2 -6 -5 -30 656.442 114.995 2 -6 -5 -31 205.946 74.2001 2 -6 -5 -32 8.24410 52.2854 2 -6 -5 -33-35.8771 43.1768 2 -6 5 -34 121.812 38.3060 3 -6 -5 -34 383.398 57.7747 2 6 6 -36 31.4329 30.3891 3 6 6 -35 281.853 59.0325 3 6 6 -34 154.210 55.5672 3 6 -6 -34 37.2199 29.6700 4 6 -6 -33 474.959 73.9137 4 6 6 -33 517.567 98.4432 3 6 6 -32 193.460 76.4417 3 6 6 -31 372.819 96.5318 3 6 6 -30 852.562 142.099 3 6 6 -29 47.4764 74.5223 3 6 6 -28 1536.66 176.484 3 6 6 -27 34.5132 73.7081 3 6 -6 -27-121.126 105.424 2 6 6 -26 441.333 114.830 3 6 -6 -26 383.013 120.048 2 6 6 -25 43.3658 70.5300 3 6 -6 -25-4.99081 84.0115 2 6 6 -24 518.286 113.530 3 6 -6 -24 657.205 135.146 2 6 6 -23-38.1675 117.951 6 6 6 -23-19.6018 79.0422 3 6 -6 -23 21.2600 69.7182 2 6 6 -22 2936.82 233.540 3 6 6 -22 2768.28 475.072 6 6 -6 -22 3278.17 262.011 2 6 6 -21 67.5262 62.6916 3 6 -6 -21 143.207 94.3035 2 6 -6 -20 2819.24 231.541 2 6 6 -20 2646.36 433.611 6 6 6 -20 2544.70 208.979 3 6 6 -19 1023.68 247.043 6 -6 -6 19 1404.83 286.173 1 6 6 -19 1375.41 160.108 3 6 -6 -19 1314.19 163.162 2 6 6 -18 1519.72 309.519 6 -6 -6 18 1331.24 261.006 1 6 -6 -18 1491.54 164.188 2 6 6 -18 1393.39 152.299 3 6 6 -17 1101.72 303.684 6 -6 -6 17 1328.44 274.037 1 6 -6 -17 976.440 133.515 2 6 6 -17 1077.57 131.638 3 6 6 -16 107.383 145.943 6 -6 -6 16 369.189 156.314 1 6 6 -15 3033.58 419.448 6 -6 -6 15 3330.43 395.278 1 -6 -6 14 499.451 177.128 1 6 6 -14 516.646 200.844 6 6 6 -13 501.594 156.105 6 -6 -6 13 368.873 146.802 1 -6 -6 12 147.465 107.060 1 6 6 -12 377.958 158.374 6 6 6 -11 21265.8 1000.13 6 -6 -6 11 22266.1 921.659 1 6 6 -10 5031.02 488.162 6 -6 -6 10 5836.97 463.340 1 6 6 -9 128.818 132.737 6 -6 -6 9-15.3226 84.7578 1 6 6 -8 12333.1 717.457 6 6 6 -7 481.437 180.596 6 6 6 -6 12539.4 698.155 6 6 6 -5 2030.81 304.555 6 6 6 -4 15506.2 752.989 6 6 6 -3 11544.2 651.663 6 6 6 -2 28597.4 1004.46 6 6 -6 -2 28099.6 719.553 1 6 -6 -1 345.319 101.291 1 6 6 -1 500.571 164.382 6 6 6 0 4553.25 409.352 6 6 -6 0 4773.06 324.292 1 6 -6 1 426.162 120.670 1 6 6 1 627.741 175.744 6 6 6 2 7524.21 517.766 6 6 -6 2 7686.63 444.809 1 6 -6 3 8416.97 485.483 1 6 6 3 8706.09 559.212 6 6 6 4 28558.0 1031.07 6 6 -6 4 29299.5 935.665 1 6 -6 5 607.150 170.016 1 6 6 5 535.972 169.939 6 6 -6 6 9813.23 591.773 1 6 -6 7 16564.3 795.685 1 6 -6 8 2716.39 338.686 1 6 -6 9 2021.28 313.093 1 6 -6 10 868.081 221.441 1 6 -6 11-110.671 101.603 1 6 -6 12 87.9217 141.570 1 6 -6 13 3370.02 451.647 1 6 -6 14 538.822 194.884 1 -6 -6 -14 773.567 111.483 2 6 -6 15 3269.44 209.771 4 -6 -6 -15 3382.37 231.581 2 6 -6 15 3175.93 465.288 1 6 -6 16 6107.47 669.381 1 -6 -6 -16 6782.41 331.602 2 -6 -6 -17 1479.63 166.504 2 6 -6 17 1089.58 300.092 1 -6 -6 -18 684.276 120.800 2 6 -6 18 819.866 280.372 1 6 6 19 128.956 153.902 1 -6 -6 -19 175.636 64.2485 2 6 -6 19 129.395 209.973 1 6 6 20 801.452 275.836 1 -6 -6 -20 782.357 139.483 2 6 -6 20 249.988 130.177 1 -6 -6 -21 398.863 103.144 2 6 6 21 562.732 231.819 1 6 -6 21 777.369 273.159 1 -6 -6 -22 3769.23 278.362 2 -6 -6 -23 49.7859 83.0504 2 -6 -6 -24 29.4387 89.8834 2 -6 -6 -25 344.514 111.992 2 -6 -6 -26 1458.84 181.848 2 -6 -6 -27 1079.05 159.152 2 -6 -6 -28-31.3157 74.7022 2 -6 -6 -29 61.6678 68.6481 2 -6 -6 -30 676.466 116.627 2 -6 -6 -31 1444.12 144.252 2 -6 -6 -32-2.70527 49.4882 2 -6 6 -33 201.824 48.6934 3 -6 -6 -33 343.098 63.5258 2 -6 -6 -34 46.4400 28.5542 2 6 7 -35 20.5247 32.0812 3 6 7 -34 301.983 62.2866 3 6 -7 -34 209.087 44.3412 4 6 7 -33-28.1909 51.4772 3 6 -7 -33 37.4027 46.5329 4 6 7 -32 502.304 94.9433 3 6 -7 -32 332.203 72.4873 4 6 7 -31 17.4257 60.4046 3 6 7 -30 16.7112 60.9484 3 6 7 -29 381.471 97.6862 3 6 7 -28 30.0001 69.5333 3 6 7 -27 2366.68 211.916 3 6 -7 -26 172.308 101.146 2 6 7 -26 225.567 95.8615 3 6 -7 -25 1481.79 188.881 2 6 7 -25 1509.44 177.100 3 6 -7 -24 142.676 91.8651 2 6 7 -24 81.1497 77.3221 3 6 7 -23 79.6790 78.1118 3 6 -7 -23 20.9482 68.6884 2 6 -7 -22 1217.15 166.000 2 6 7 -22 1155.00 155.741 3 6 7 -22 862.299 269.817 6 6 7 -21-9.90179 70.4474 3 6 -7 -21 94.6536 86.6706 2 6 7 -20 1056.24 148.537 3 6 -7 -20 972.555 144.898 2 6 7 -19 95.0981 63.2633 3 6 -7 -19 34.6614 71.3216 2 6 7 -18 3397.10 477.704 6 6 7 -18 3571.15 237.410 3 6 -7 -18 3811.15 262.678 2 -6 -7 18 3824.88 478.148 1 6 7 -17 2158.77 373.176 6 6 -7 -17 2128.43 193.050 2 6 7 -17 2281.51 187.417 3 -6 -7 17 2360.37 360.686 1 6 7 -16 70.0452 95.5257 6 6 -7 -16 98.1779 53.9708 2 6 7 -16 101.590 67.1240 3 -6 -7 16 57.3472 105.075 1 -6 -7 15 1265.68 244.877 1 6 7 -15 1218.16 283.274 6 6 7 -14 873.713 244.608 6 -6 -7 14 1331.63 267.738 1 6 7 -13 1955.76 333.304 6 -6 -7 13 2234.22 330.597 1 -6 -7 12-5.12161 88.9877 1 6 7 -12-46.1010 110.996 6 -6 -7 11 58.5312 121.723 1 6 7 -11 24.9832 98.7905 6 6 7 -10 1423.30 278.988 6 -6 -7 10 1533.67 277.769 1 6 7 -9 34.7452 94.3468 6 -6 -7 9 240.732 137.073 1 6 7 -8 1031.28 245.561 6 6 7 -7 1333.63 268.702 6 6 7 -6 999.459 241.000 6 6 7 -5 24409.0 1013.69 6 6 7 -4 1408.20 251.282 6 6 7 -3 12208.9 713.225 6 6 7 -2 189.928 104.188 6 6 7 -1 93.3020 138.064 6 6 -7 -1 18.4196 59.3582 1 6 -7 0 313.993 98.1833 1 6 7 0 356.274 168.024 6 6 7 1 17552.6 848.615 6 6 -7 1 17313.0 696.057 1 6 -7 2 3290.08 312.203 1 6 7 2 4051.72 413.718 6 6 -7 3 23004.9 857.778 1 6 7 3 22880.9 978.205 6 6 -7 4 25338.6 930.267 1 6 7 4 26948.0 1066.32 6 6 -7 5 1195.52 216.773 1 6 7 5 1121.42 233.743 6 6 -7 6 1004.76 218.044 1 6 7 6 1197.01 253.732 6 6 -7 7 15702.0 817.155 1 6 -7 8 1733.11 295.882 1 6 -7 9 4711.26 483.384 1 6 -7 10 761.378 230.302 1 6 -7 11 1004.85 265.836 1 6 -7 12 658.360 211.246 1 -6 -7 -13 442.983 95.7468 2 6 -7 13 132.002 121.482 1 -6 -7 -14 68.8539 65.9454 2 6 -7 14-0.88454 54.9956 4 -6 -7 -15 130.800 70.4294 2 6 -7 15 117.883 57.7393 4 6 -7 15 82.7841 129.193 1 -6 -7 -16 390.123 91.4288 2 6 -7 16 202.986 165.750 1 6 -7 17 9451.33 868.692 1 -6 -7 -17 10303.6 425.981 2 -6 -7 -18-63.6191 83.2473 2 6 -7 18 64.1461 136.925 1 6 7 19 124.789 244.534 1 -6 -7 -19 202.567 80.8440 2 6 7 20 441.181 161.528 1 -6 -7 -20 641.150 130.184 2 -6 -7 -21 1273.98 175.629 2 -6 -7 -22 50.6545 84.0174 2 -6 -7 -23 82.4047 79.0040 2 -6 -7 -24 528.153 127.250 2 -6 -7 -25 240.793 88.3514 2 -6 -7 -26-10.3045 84.4972 2 -6 -7 -27 457.863 119.744 2 -6 -7 -28 182.981 78.3457 2 -6 -7 -29 528.477 111.931 2 -6 -7 -30 308.477 86.1059 2 -6 7 -31-0.20300 36.4818 3 -6 -7 -31-20.0460 52.1149 2 -6 7 -32 55.9834 32.5909 3 -6 -7 -32 48.7218 44.1242 2 -6 -7 -33 24.2161 36.5863 2 6 8 -34 19.6678 29.3282 3 6 -8 -34-26.7860 30.9327 4 6 8 -33 42.1574 45.3881 3 6 -8 -33 1.42748 39.1771 4 6 8 -32 440.428 74.0875 3 6 -8 -32 507.261 77.7147 4 6 8 -31 50.9865 49.4634 3 6 -8 -31 34.3698 49.0708 4 6 8 -30 69.7864 55.7987 3 6 8 -29 2220.45 185.425 3 6 8 -28-52.8405 68.6462 3 6 8 -27-59.8849 70.3364 3 6 8 -26-86.3795 76.4721 3 6 8 -25 930.597 144.711 3 6 -8 -25 722.114 138.458 2 6 8 -24 35.9847 69.1253 3 6 -8 -24-77.1714 88.3393 2 6 8 -23 207.231 88.1375 3 6 -8 -23 231.547 102.109 2 6 8 -22 260.109 82.5470 3 6 8 -22 111.038 124.430 6 6 -8 -22 284.250 104.030 2 6 -8 -21 96.7502 68.0468 2 6 8 -21 96.8114 77.6258 3 6 8 -20-16.7297 129.920 6 6 8 -20 228.186 81.4268 3 6 -8 -20 130.759 68.5075 2 6 -8 -19 1420.14 169.153 2 -6 -8 19 1387.19 320.267 1 6 8 -19 1832.82 359.081 6 6 8 -19 1527.63 162.569 3 6 -8 -18 2213.09 207.770 2 6 8 -18 2193.09 191.522 3 6 8 -18 1633.61 344.324 6 -6 -8 18 2030.71 362.561 1 6 8 -17 262.778 183.189 6 6 -8 -17 196.505 88.2230 2 6 8 -17 99.3024 69.8727 3 -6 -8 17-146.544 127.337 1 6 8 -16 356.741 83.1998 3 6 8 -16 526.153 206.517 6 6 -8 -16 321.596 92.6031 2 -6 -8 16 339.730 179.927 1 6 8 -15 4598.90 253.754 3 6 -8 -15 4643.99 266.565 2 -6 -8 15 4452.59 509.092 1 6 8 -15 5575.13 602.692 6 6 8 -14 1180.34 279.383 6 -6 -8 14 1305.69 283.494 1 6 8 -13 7334.43 656.729 6 -6 -8 13 7521.34 634.240 1 6 8 -12-43.4833 121.627 6 -6 -8 12 382.591 175.639 1 6 8 -11 2312.31 386.047 6 -6 -8 11 2299.90 346.268 1 6 8 -10 802.094 240.276 6 6 8 -9 659.145 210.781 6 6 8 -8 573.000 207.255 6 6 8 -7 7100.57 600.423 6 6 8 -6 18810.4 953.555 6 6 8 -5 6017.15 533.377 6 6 8 -4 4573.02 464.750 6 6 8 -3 1469.86 276.603 6 6 8 -2 283.345 150.588 6 6 8 -1 1151.44 255.233 6 6 -8 -1 772.289 145.535 1 6 -8 0 2423.78 278.114 1 6 8 0 2726.34 368.563 6 6 -8 1 312.678 127.494 1 6 8 1 326.678 170.743 6 6 -8 2 9701.75 576.713 1 6 8 2 9629.38 668.363 6 6 -8 3 7571.73 531.842 1 6 8 3 7974.85 616.250 6 6 8 4 12379.8 778.700 6 6 -8 4 11806.9 677.428 1 6 -8 5 2416.70 328.123 1 6 8 5 2127.53 332.933 6 6 8 6 3613.69 428.661 6 6 -8 6 3402.91 393.292 1 6 -8 7 1686.17 295.314 1 6 8 7 1249.23 260.498 6 6 -8 8 12509.7 785.771 1 6 -8 9 1454.01 286.962 1 6 -8 10 1491.61 300.611 1 6 -8 11 131.622 134.133 1 -6 -8 -12 341.868 87.9565 2 6 -8 12 262.371 62.7407 4 6 -8 12 108.542 113.809 1 -6 -8 -13 1588.29 164.453 2 6 -8 13 1198.66 133.928 4 6 -8 13 1603.80 343.719 1 -6 -8 -14 599.862 110.794 2 6 -8 14 530.131 96.1703 4 6 -8 14 651.595 220.860 1 6 -8 15 1156.72 137.337 4 -6 -8 -15 1100.16 143.638 2 6 -8 15 1159.45 325.194 1 -6 -8 -16 80.5814 57.1075 2 6 -8 16 263.343 172.341 1 -6 -8 -17 20.3832 58.9196 2 6 -8 17-685.407 267.551 1 6 -8 18 1554.16 367.524 1 -6 -8 -18 1622.63 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77.4373 2 -7 -5 -27 203.460 84.9399 2 -7 -5 -28 1258.84 160.828 2 -7 -5 -29 16.7483 67.7906 2 -7 -5 -30 241.055 85.3671 2 -7 -5 -31 328.869 74.8829 2 -7 -5 -32 813.513 102.013 2 -7 -5 -33-20.2006 36.7242 2 7 6 -36 70.8742 31.0980 3 7 6 -35-59.0570 40.5486 3 7 6 -34 1258.32 119.986 3 7 6 -33 10.1826 51.8993 3 7 -6 -33-37.3478 35.3058 4 7 6 -32-1.43550 68.1480 3 7 -6 -32-72.9461 45.9766 4 7 6 -31 384.468 102.871 3 7 -6 -31 260.790 64.6757 4 7 6 -30-37.1030 76.4101 3 7 6 -29-39.5360 80.4190 3 7 6 -28 64.1405 83.9689 3 7 6 -27 279.275 106.599 3 7 6 -26 526.810 126.107 3 7 6 -25 43.7813 73.2778 3 7 6 -24 241.013 96.8134 3 7 6 -23 314.891 185.462 6 7 -6 -23 253.865 98.5700 2 7 6 -23 107.484 71.0738 3 7 6 -22 322.870 100.700 3 7 6 -22 451.765 209.641 6 7 -6 -22 335.289 115.335 2 7 6 -21 66.9146 64.9315 3 7 6 -21 179.830 196.683 6 7 -6 -21 46.9693 74.0068 2 7 6 -20 14807.0 498.916 3 7 6 -20 13975.3 1019.03 6 7 -6 -20 14618.7 523.945 2 7 6 -19 351.234 95.1802 3 7 -6 -19 183.505 74.4057 2 7 6 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146.192 3 7 -7 -19 1070.27 153.511 2 7 7 -19 1331.43 318.564 6 7 7 -18 63.6208 67.9091 3 7 7 -18 28.7990 98.9542 6 7 -7 -18-22.0171 53.3253 2 7 -7 -17 4722.03 287.495 2 -7 -7 17 4996.17 521.274 1 7 7 -17 4685.20 276.827 3 7 7 -17 4790.63 576.685 6 7 7 -16 1858.36 373.767 6 7 -7 -16 1561.01 166.281 2 -7 -7 16 1470.80 273.920 1 7 7 -16 1587.34 155.737 3 7 7 -15 154.796 62.9974 3 7 7 -15 204.209 181.792 6 7 -7 -15 32.3050 56.9833 2 7 7 -14 755.502 212.728 6 -7 -7 14 453.444 163.714 1 7 7 -13 2557.32 404.836 6 -7 -7 13 1963.05 313.504 1 7 7 -12 652.802 234.869 6 7 7 -11 6395.24 600.130 6 7 7 -10 1735.30 324.754 6 7 7 -9 3616.69 434.030 6 7 7 -8 8916.68 672.748 6 7 7 -7 1220.76 269.962 6 7 7 -6 7861.47 612.948 6 7 7 -5 9014.94 648.754 6 7 7 -4 1880.28 306.147 6 7 7 -3-16.7215 108.194 6 7 7 -2 50.5464 99.4678 6 7 -7 -1 3827.00 293.717 1 7 7 -1 4036.33 426.908 6 7 -7 0 1297.16 187.407 1 7 7 0 1008.99 226.365 6 7 7 1 13164.2 759.446 6 7 -7 1 13388.9 611.402 1 7 -7 2 183.393 102.666 1 7 7 2 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2 -7 -7 -21-46.4680 83.3389 2 -7 -7 -22 2123.39 220.641 2 -7 -7 -23 2422.49 226.959 2 -7 -7 -24 12.8373 87.4239 2 -7 -7 -25 2.90092 87.6443 2 -7 -7 -26-36.0484 83.9439 2 -7 -7 -27 1127.59 154.252 2 -7 -7 -28-66.3290 79.9543 2 -7 -7 -29 34.5687 61.8035 2 -7 -7 -30 166.219 65.9442 2 -7 7 -31 133.505 39.2779 3 -7 -7 -31 363.551 75.4532 2 -7 -7 -32 68.6304 40.7451 2 7 8 -34-0.46671 28.5371 3 7 8 -33 238.096 56.8047 3 7 -8 -33 165.382 43.1928 4 7 8 -32-92.4707 50.9821 3 7 -8 -32-12.6638 35.8567 4 7 8 -31 345.535 75.7727 3 7 -8 -31 295.086 67.7234 4 7 8 -30 330.329 87.2582 3 7 -8 -30 200.134 68.2627 4 7 8 -29 23.1581 64.2922 3 7 -8 -29 42.5542 59.0769 4 7 8 -28 877.596 126.216 3 7 8 -27 1608.10 171.380 3 7 8 -26 1724.71 178.019 3 7 8 -25 88.1884 71.5809 3 7 8 -24 435.600 106.768 3 7 8 -23 1336.47 160.899 3 7 8 -22 234.544 87.4296 3 7 8 -21 452.813 201.918 6 7 8 -21-106.662 67.5514 3 7 -8 -20 6889.91 363.733 2 7 8 -20 6420.11 702.606 6 7 8 -20 7000.27 348.312 3 7 8 -19 3253.01 505.280 6 7 -8 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7 -8 3 1264.87 222.786 1 7 8 3 1109.36 251.999 6 7 -8 4 136.297 97.0675 1 7 8 4 257.185 136.244 6 7 -8 5 2447.98 325.765 1 7 8 5 2469.65 358.554 6 7 8 6 3751.90 454.749 6 7 -8 6 3410.73 396.100 1 7 8 7 8917.51 699.667 6 7 -8 7 8755.31 649.533 1 7 -8 8 364.152 141.045 1 7 8 8 238.416 112.467 6 7 -8 9-280.556 151.213 1 7 8 9 50.1249 118.480 6 7 -8 10 14783.0 436.822 4 7 8 10 15949.6 979.700 6 7 -8 10 15726.6 951.704 1 7 8 11 7733.44 694.804 6 7 -8 11 7337.01 663.793 1 -7 -8 -11 7555.99 333.737 2 7 -8 11 7442.21 319.841 4 -7 -8 -12 83.6445 56.7552 2 7 -8 12-11.3828 50.7928 4 7 -8 12 35.2126 113.437 1 -7 -8 -13 76.4156 67.0911 2 7 -8 13 132.911 59.2870 4 7 -8 13 97.9909 150.500 1 7 -8 14 3243.54 223.669 4 7 -8 14 2833.03 470.273 1 -7 -8 -14 3416.60 240.035 2 7 -8 15 1607.42 160.832 4 7 -8 15 1661.32 347.310 1 -7 -8 -15 1687.52 181.408 2 -7 -8 -16 155.373 77.7771 2 7 -8 16 116.845 158.394 1 -7 -8 -17-20.9310 82.7213 2 7 -8 17 241.435 195.021 1 7 -8 18 11.7553 134.045 1 -7 -8 -18 53.0313 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593.140 1 8 -3 18 5183.21 631.382 1 -8 -3 -18 5139.87 300.542 2 8 3 19 3241.54 504.929 1 8 -3 19 3010.95 506.697 1 -8 -3 -19 3095.85 239.763 2 8 -3 20 1638.31 393.713 1 8 3 20 1158.64 327.917 1 -8 -3 -20 1484.11 171.937 2 8 -3 21 1967.96 423.924 1 -8 -3 -21 1856.91 193.302 2 8 3 21 1650.33 420.348 1 -8 -3 -22 107.049 66.8135 2 -8 -3 -23 307.534 109.502 2 -8 -3 -24-149.256 90.0685 2 -8 -3 -25 86.9503 81.3631 2 -8 -3 -26 1663.81 178.923 2 -8 -3 -27 764.463 134.500 2 -8 -3 -28 90.3642 70.0182 2 -8 -3 -29 1110.99 134.667 2 -8 -3 -30 199.138 70.0851 2 -8 -3 -31 251.031 69.2222 2 -8 -3 -32-2.39414 39.7125 2 8 4 -36 22.8571 32.5317 3 8 4 -35 198.187 57.1220 3 8 4 -34 3.40734 50.3580 3 8 4 -33-28.5845 65.7455 3 8 4 -32 1390.41 153.755 3 8 4 -31 17.2470 71.8044 3 8 4 -30 24.3272 81.1203 3 8 4 -29 961.709 149.360 3 8 -4 -28-92.3063 63.4526 3 8 4 -28 6.39055 79.0780 3 8 -4 -27-11.9258 58.6665 3 8 4 -27 83.6352 87.3032 3 8 4 -26 1688.13 191.514 3 8 -4 -26 1601.76 165.950 3 8 -4 -25 32.0185 52.8680 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4 183.311 100.721 1 8 4 4 13.3523 81.3960 6 8 4 5 7377.21 495.606 6 8 -4 5 6887.52 458.643 1 8 -4 6 27240.4 947.996 1 8 4 6 27876.8 983.718 6 8 -4 7 5965.08 464.721 1 8 4 7 5979.41 463.564 6 8 -4 8 182.163 113.661 1 8 4 8 154.230 106.411 6 8 -4 9 13197.8 761.402 1 8 4 9 14126.2 733.791 6 8 -4 10 7573.57 598.638 1 8 4 10 7091.35 524.845 6 8 -4 11 1765.12 304.421 1 8 -4 12 6046.75 580.594 1 8 -4 13 3295.66 446.024 1 8 -4 14 5174.76 268.517 4 8 -4 14 5192.81 585.056 1 -8 -4 -14 5488.82 286.750 2 8 4 15 4175.50 529.589 1 8 -4 15 4989.01 584.345 1 -8 -4 -15 3881.36 249.974 2 8 -4 16 7180.29 715.563 1 8 4 16 7108.82 705.618 1 -8 -4 -16 7411.25 351.731 2 8 4 17 1896.91 378.561 1 8 -4 17 2506.68 445.960 1 -8 -4 -17 2387.83 202.807 2 -8 -4 -18 550.645 113.033 2 8 -4 18 959.805 290.208 1 8 4 18 630.870 216.996 1 8 -4 19 3052.92 482.714 1 8 4 19 3010.05 494.246 1 -8 -4 -19 2971.33 236.561 2 -8 -4 -20 97.1338 68.7054 2 8 4 20-267.951 184.549 1 8 -4 20-194.051 161.781 1 -8 -4 -21 135.010 78.7161 2 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738.342 6 8 5 -18 7761.88 353.161 3 8 5 -17 1194.77 290.422 6 8 5 -17 964.215 130.963 3 8 5 -16 11065.3 401.556 3 8 5 -16 10965.3 845.084 6 8 5 -15-54.9667 176.495 6 8 5 -14 161.367 159.961 6 8 5 -13 22.7294 141.063 6 8 5 -12 1563.29 312.214 6 8 5 -11 198.617 146.890 6 8 5 -10 565.999 204.609 6 8 5 -9 68.1913 147.406 6 8 5 -8 1542.85 295.471 6 8 5 -7 5607.74 503.291 6 8 5 -6 8349.70 599.886 6 8 5 -5 9646.98 634.203 6 8 5 -4 56044.0 1492.62 6 8 5 -3 2526.84 330.061 6 8 5 -2 608.346 178.506 6 8 5 -1 11378.3 653.856 6 8 5 0 3029.27 354.624 6 8 -5 0 3047.83 233.219 1 8 5 1 2062.22 296.809 6 8 -5 1 2521.40 233.210 1 8 -5 2 7688.93 427.612 1 8 5 2 7490.29 534.057 6 8 -5 3 567.961 119.286 1 8 5 3 700.137 198.032 6 8 -5 4 28479.7 910.049 1 8 5 4 29872.0 1063.06 6 8 5 5 516.238 167.251 6 8 -5 5 650.484 160.298 1 8 -5 6 39.6519 79.7031 1 8 5 6-14.0703 110.677 6 8 -5 7 2054.50 286.722 1 8 5 7 1633.96 280.665 6 8 -5 8 1090.31 220.153 1 8 5 8 1062.10 215.495 6 8 -5 9 1396.07 274.051 1 8 5 9 1642.42 280.272 6 8 -5 10 14658.6 841.809 1 8 5 10 14593.2 814.632 6 8 -5 11 4606.89 497.453 1 8 5 11 4610.93 469.281 6 8 -5 12 2338.45 370.755 1 8 -5 13 995.142 259.390 1 -8 -5 -13 1051.42 134.274 2 8 -5 13 976.964 124.589 4 8 -5 14 7734.75 706.109 1 8 -5 14 8016.84 338.479 4 -8 -5 -14 7867.08 352.318 2 8 -5 15 978.935 252.418 1 -8 -5 -15 1159.45 145.391 2 8 -5 16 879.288 301.973 1 -8 -5 -16 1278.00 156.315 2 8 5 16 1601.59 372.095 1 8 5 17 3660.86 528.487 1 -8 -5 -17 3255.87 244.632 2 8 -5 17 3104.63 494.101 1 8 -5 18 755.543 217.626 1 -8 -5 -18 456.005 99.8354 2 8 5 18 500.990 207.784 1 -8 -5 -19 93.9373 84.0352 2 8 -5 19 283.580 190.311 1 -8 -5 -20 58.2381 65.9783 2 8 5 20-168.495 167.148 1 -8 -5 -21-27.6348 85.7578 2 -8 -5 -22 1228.21 170.224 2 -8 -5 -23 520.843 126.827 2 -8 -5 -24 1291.55 168.464 2 -8 -5 -25-0.41408 80.3047 2 -8 -5 -26 1272.14 164.778 2 -8 -5 -27 139.118 84.4089 2 -8 -5 -28 211.976 82.5432 2 -8 -5 -29 204.857 74.2938 2 -8 -5 -30 1429.27 148.370 2 -8 -5 -31-53.0518 44.0939 2 -8 -5 -32 24.5838 39.9115 2 8 6 -35-3.90787 33.4471 3 8 6 -34 182.020 58.9949 3 8 6 -33 6.27240 47.4770 3 8 6 -32-16.4333 56.9524 3 8 -6 -32 114.286 40.7305 4 8 6 -31 88.5301 77.3798 3 8 -6 -31 25.0314 46.0005 4 8 6 -30 1038.96 137.337 3 8 -6 -30 1017.58 114.812 4 8 6 -29-45.1665 78.5194 3 8 -6 -29 26.8214 53.0132 4 8 6 -28 929.946 143.606 3 8 6 -27-69.9473 79.5617 3 8 6 -26 840.792 140.450 3 8 6 -25 229.869 93.4464 3 8 6 -24 88.4555 74.7208 3 8 6 -23 1590.59 177.620 3 8 6 -22 5332.47 680.013 6 8 6 -22 4962.76 308.904 3 8 6 -21 3632.16 259.806 3 8 6 -21 4116.84 581.357 6 8 6 -20 979.141 286.763 6 8 6 -20 971.133 141.070 3 8 6 -19 57.3370 126.290 6 8 6 -19 163.282 82.3845 3 8 6 -18 2522.10 441.887 6 8 6 -18 2610.59 212.186 3 8 6 -17-31.0774 57.9035 3 8 6 -17 131.286 185.172 6 8 6 -16 2789.39 209.183 3 8 6 -16 3412.76 484.528 6 8 6 -15 47.3247 53.1832 3 8 6 -15 69.9811 138.619 6 8 6 -14 3535.63 482.702 6 8 6 -13 5593.95 592.849 6 8 6 -12-37.0057 131.144 6 8 6 -11 2875.93 405.408 6 8 6 -10-66.0246 133.118 6 8 6 -9 10717.6 738.205 6 8 6 -8 1836.20 310.755 6 8 6 -7 5424.54 523.908 6 8 6 -6 3441.82 410.687 6 8 6 -5 12074.5 744.122 6 8 6 -4 34747.6 1242.20 6 8 6 -3 12172.5 725.781 6 8 6 -2 4239.34 439.582 6 8 6 -1 1087.56 240.640 6 8 6 0 2630.81 348.375 6 8 6 1 8100.41 591.209 6 8 -6 1 7937.47 433.215 1 8 -6 2 13368.6 593.417 1 8 6 2 12693.2 736.878 6 8 6 3 6129.22 517.485 6 8 -6 3 5239.74 390.241 1 8 6 4 1200.47 244.278 6 8 -6 4 727.559 168.817 1 8 6 5 6872.27 554.925 6 8 -6 5 6156.16 468.943 1 8 -6 6 1137.11 215.362 1 8 6 6 1145.13 248.926 6 8 -6 7 474.438 176.715 1 8 6 7 548.187 184.481 6 8 6 8 932.001 247.016 6 8 -6 8 1433.32 264.381 1 8 -6 9 11811.6 761.477 1 8 6 9 12710.1 794.378 6 8 -6 10 9296.96 702.488 1 8 6 10 9736.57 702.420 6 8 6 11 881.578 224.640 6 8 -6 11 1086.47 245.060 1 8 -6 12 5794.49 588.070 1 8 -6 12 6541.56 299.823 4 8 6 12 5862.61 557.815 6 -8 -6 -12 6092.95 301.325 2 8 -6 13 1777.79 163.335 4 -8 -6 -13 1749.85 176.387 2 8 -6 13 1574.22 338.751 1 8 -6 14 1859.90 169.197 4 -8 -6 -14 1804.11 176.288 2 8 -6 14 1599.28 325.223 1 8 -6 15 3048.28 220.017 4 -8 -6 -15 3056.20 234.734 2 8 -6 15 2515.00 442.271 1 -8 -6 -16 1392.93 164.995 2 8 -6 16 1676.29 383.121 1 -8 -6 -17 2112.41 206.987 2 8 6 17 1933.58 401.200 1 8 -6 17 2529.39 465.553 1 8 -6 18 3957.43 579.135 1 -8 -6 -18 4170.78 287.186 2 8 6 18 3679.75 545.130 1 8 6 19 462.805 156.557 1 -8 -6 -19 372.440 103.884 2 8 -6 19 554.741 309.054 1 -8 -6 -20 1087.30 160.361 2 -8 -6 -21 6.55349 75.4762 2 -8 -6 -22 457.687 112.692 2 -8 -6 -23 124.231 96.4413 2 -8 -6 -24-4.65825 83.5772 2 -8 -6 -25 67.4760 82.6752 2 -8 -6 -26 20.2531 79.5378 2 -8 -6 -27 53.6426 75.3625 2 -8 -6 -28 1056.43 141.626 2 -8 -6 -29-83.1289 65.8709 2 -8 -6 -30 173.554 70.6139 2 -8 -6 -31 184.143 58.6572 2 -8 -6 -32 80.1209 45.6937 2 8 7 -34 75.1201 42.7623 3 8 7 -33 67.4173 45.2834 3 8 -7 -33 28.8037 27.5395 4 8 7 -32 0.74156 48.3589 3 8 -7 -32 103.640 45.8017 4 8 7 -31 168.306 76.1136 3 8 -7 -31 36.3789 44.4346 4 8 7 -30 126.352 74.7178 3 8 -7 -30 62.8553 47.9406 4 8 7 -29 111.612 76.1330 3 8 -7 -29-1.93077 51.7530 4 8 7 -28 295.313 100.723 3 8 -7 -28 298.985 76.8416 4 8 -7 -27 1655.93 162.440 4 8 7 -27 2153.96 199.615 3 8 7 -26 80.6206 72.4376 3 8 7 -25-117.341 83.4555 3 8 7 -24 960.240 146.602 3 8 7 -23 812.801 136.115 3 8 7 -22-26.7406 72.7579 3 8 7 -21 452.765 206.893 6 8 7 -21 217.079 85.8918 3 8 7 -20 565.647 238.737 6 8 7 -20 1478.14 173.306 3 8 7 -19 1335.45 350.418 6 8 7 -19 1411.07 163.465 3 8 7 -18 315.745 175.393 6 8 7 -18 192.629 83.6591 3 8 7 -17 708.213 238.384 6 8 7 -17 559.018 104.761 3 8 7 -16 82.9772 51.2185 3 8 7 -16 360.042 204.245 6 8 7 -15 2464.33 436.186 6 8 7 -15 2231.58 186.689 3 8 7 -14 2532.57 420.014 6 8 7 -14 2614.27 199.552 3 8 7 -13 731.852 248.734 6 8 -7 -13 740.167 110.408 4 8 7 -12-168.314 187.915 6 8 7 -11 1650.77 319.982 6 8 7 -10 328.739 197.725 6 8 7 -9-170.938 152.730 6 8 7 -8 134.156 141.687 6 8 7 -7 223.076 151.408 6 8 7 -6 4400.84 484.609 6 8 7 -5 904.938 237.989 6 8 7 -4-11.9850 124.548 6 8 7 -3 1180.42 260.584 6 8 7 -2 2418.99 358.089 6 8 7 -1 10094.5 696.716 6 8 7 0 2997.69 386.963 6 8 7 1 9488.74 677.698 6 8 -7 2 9.53377 68.0389 1 8 7 2-33.9389 136.434 6 8 7 3 14661.3 846.246 6 8 -7 3 13321.5 662.284 1 8 -7 4 921.846 188.783 1 8 7 4 938.798 246.919 6 8 -7 5 45.9777 81.3905 1 8 7 5 96.9186 131.351 6 8 -7 6 218.805 136.632 1 8 7 6 37.0548 118.654 6 8 -7 7 7296.91 569.095 1 8 7 7 7627.93 633.266 6 8 -7 8 95.8554 100.244 1 8 7 8-52.0618 129.141 6 8 -7 9 672.243 210.700 1 8 7 9 761.992 235.426 6 8 7 10 10.0356 86.5361 6 -8 -7 -10 137.269 69.0906 2 8 -7 10 59.0638 44.5973 4 8 -7 10 106.528 98.2047 1 8 -7 11 1865.95 163.899 4 8 -7 11 1476.42 306.875 1 8 7 11 1473.09 302.616 6 -8 -7 -11 1901.20 177.319 2 -8 -7 -12 461.911 94.5213 2 8 -7 12 578.544 100.374 4 8 -7 12 466.647 178.098 1 8 7 12 432.660 193.929 6 -8 -7 -13 56.8116 62.6301 2 8 -7 13 54.8725 57.7186 4 8 -7 13 39.2185 139.844 1 -8 -7 -14 590.926 109.967 2 8 -7 14 417.513 95.5933 4 8 -7 14 265.520 162.982 1 8 7 14 516.262 182.930 6 8 -7 15 1971.94 178.809 4 8 -7 15 1587.42 338.670 1 -8 -7 -15 1903.96 190.048 2 8 7 15 1287.80 298.393 6 8 -7 16 2302.14 450.991 1 -8 -7 -16 2025.95 200.381 2 8 7 16 1317.68 299.971 6 8 -7 17 1974.47 406.268 1 -8 -7 -17 2383.72 216.837 2 8 7 17 2410.55 424.721 6 -8 -7 -18 5898.98 340.772 2 8 7 18 5556.43 679.572 1 8 -7 18 5643.48 696.041 1 8 7 18 5837.19 644.136 6 -8 -7 -19 3871.18 281.737 2 -8 -7 -20 238.824 106.124 2 -8 -7 -21 474.578 122.865 2 -8 -7 -22 1046.18 166.644 2 -8 -7 -23 84.6202 85.1948 2 -8 -7 -24 199.143 89.0520 2 -8 -7 -25 36.5603 81.9049 2 -8 -7 -26-77.3750 80.2654 2 -8 -7 -27 222.625 84.0967 2 -8 -7 -28 419.255 95.0346 2 -8 -7 -29 3.15426 57.1336 2 -8 -7 -30 99.9489 56.3794 2 -8 -7 -31 349.246 67.9761 2 -8 -7 -32 66.9539 36.1886 2 8 8 -34-13.4029 27.4749 3 8 8 -33 158.786 49.7683 3 8 -8 -33 72.1000 26.6512 4 8 8 -32 127.274 54.3017 3 8 -8 -32 66.5976 35.3990 4 8 8 -31 3.68402 52.0008 3 8 -8 -31 35.3384 42.4481 4 8 8 -30 260.609 80.6179 3 8 -8 -30 118.414 56.5955 4 8 -8 -29 1132.91 123.686 4 8 8 -29 1066.61 131.602 3 8 8 -28 1122.17 138.328 3 8 -8 -28 1202.70 134.852 4 8 -8 -27-9.73699 57.4736 4 8 8 -27 20.7781 64.8990 3 8 8 -26 47.5410 71.0011 3 8 -8 -26 14.9684 60.4964 4 8 8 -25 15.7717 70.4333 3 8 -8 -25 126.805 71.5736 4 8 8 -24 766.926 132.548 3 8 -8 -24 971.365 139.561 4 8 8 -23 536.431 120.908 3 8 8 -22 491.768 113.434 3 8 8 -21 45.4032 63.7451 3 8 8 -20 1481.07 343.465 6 8 8 -20 841.913 132.615 3 8 8 -19-143.282 147.524 6 8 8 -19 179.025 75.9282 3 8 8 -18 514.630 214.891 6 8 8 -18 170.009 83.2499 3 8 8 -17 413.751 165.799 6 8 8 -17 74.4218 63.6020 3 8 8 -16 214.170 212.962 6 8 8 -16 35.6677 53.8196 3 8 -8 -16 148.238 83.8604 4 8 -8 -15 1977.00 170.733 5 8 8 -15 2657.06 444.603 6 8 8 -15 2176.41 186.252 3 8 -8 -15 2184.24 185.420 4 8 8 -14 344.341 221.434 6 8 -8 -14 198.471 72.7200 5 8 8 -14 191.038 71.9943 3 8 -8 -14 141.925 66.9262 4 8 8 -13 2633.10 431.293 6 8 -8 -13 3240.62 209.760 5 8 -8 -13 2686.42 199.473 4 8 8 -13 3398.22 223.506 3 8 8 -12 651.207 231.655 6 8 -8 -12 714.140 110.188 5 8 8 -12 586.317 100.830 3 8 -8 -12 701.359 108.718 4 8 8 -11 2529.09 418.646 6 8 -8 -11 2303.79 178.806 5 8 -8 -11 2123.89 174.366 4 8 8 -10 55.4984 143.953 6 8 -8 -10 73.6626 54.0286 4 8 8 -9 4472.49 516.438 6 8 8 -8 337.424 176.693 6 8 8 -7 4441.20 504.763 6 8 8 -6 219.869 155.768 6 8 8 -5 420.844 192.745 6 8 8 -4 261.441 180.146 6 8 8 -3 6929.02 614.910 6 8 8 -2 1978.16 333.912 6 8 8 -1 1037.82 279.769 6 8 8 0 5125.05 526.150 6 8 8 1 2832.47 409.734 6 8 8 2 8211.49 664.247 6 8 -8 3 95.8734 82.2201 1 8 8 3 34.8937 111.187 6 8 -8 4 15.2297 62.2779 1 8 8 4-103.520 132.502 6 8 8 5 23817.4 1160.95 6 8 -8 5 23266.2 1001.03 1 8 -8 6 1389.96 266.104 1 8 8 6 1238.89 279.765 6 8 -8 7 1487.20 282.567 1 8 8 7 2004.88 353.874 6 8 -8 8 2217.42 174.285 4 8 -8 8 1911.17 316.759 1 8 8 8 1939.44 359.893 6 8 -8 9 5415.02 275.971 4 8 8 9 5184.83 566.206 6 -8 -8 -9 4877.00 263.820 2 8 -8 9 5228.34 541.742 1 -8 -8 -10 73.0328 50.6595 2 8 -8 10 54.1642 50.9054 4 8 -8 10 57.0853 122.633 1 8 8 10 235.583 228.060 6 8 -8 11 1423.58 147.782 4 8 -8 11 1159.14 288.262 1 -8 -8 -11 1525.89 158.682 2 8 8 11 1450.71 302.564 6 8 8 12 2255.10 395.613 6 8 -8 12 2181.56 186.156 4 8 -8 12 1727.38 343.486 1 -8 -8 -12 2482.31 209.622 2 -8 -8 -13-3.74606 60.2994 2 8 -8 13-5.39221 57.2606 4 8 -8 13-31.6480 105.391 1 8 8 13-105.845 179.771 6 -8 -8 -14 367.976 96.5711 2 8 -8 14 622.568 113.606 4 8 -8 14 617.383 227.492 1 8 8 14 636.536 215.811 6 8 -8 15 1630.97 170.702 4 8 -8 15 1325.53 342.816 1 -8 -8 -15 1797.81 189.395 2 8 8 15 1710.57 354.585 6 8 -8 16 3363.50 520.420 1 -8 -8 -16 3089.80 245.262 2 8 8 16 3560.22 512.603 6 -8 -8 -17 396.290 103.388 2 8 -8 17 479.435 273.984 1 8 8 17 31.4952 123.882 6 -8 -8 -18 944.697 149.659 2 -8 -8 -19 871.157 151.016 2 -8 -8 -20 362.519 111.643 2 -8 -8 -21 778.376 145.203 2 -8 -8 -22 14.9124 83.7042 2 -8 -8 -23 504.277 123.429 2 -8 -8 -24 1019.52 149.862 2 -8 -8 -25 219.863 100.701 2 -8 -8 -26 26.2680 70.2660 2 -8 -8 -27 58.9213 63.5697 2 -8 -8 -28 861.527 120.684 2 -8 -8 -29 500.215 88.4356 2 -8 -8 -30 14.6608 47.5760 2 -8 -8 -31 174.474 47.7599 2 8 9 -32 5.16846 33.2056 3 8 -9 -32 20.0379 31.3035 4 8 9 -31 367.829 65.8107 3 8 -9 -31 331.439 64.2461 4 8 9 -30 422.365 81.8406 3 8 -9 -30 311.844 68.7981 4 8 9 -29 56.6186 48.1724 3 8 -9 -29 88.0696 57.2240 4 8 9 -28-55.1513 56.2883 3 8 -9 -28-15.8439 52.4162 4 8 9 -27 675.876 109.902 3 8 -9 -27 811.227 121.215 4 8 9 -26 29.2353 59.5035 3 8 -9 -26 179.082 73.9738 4 8 9 -25 161.119 73.1276 3 8 -9 -25 164.727 79.2414 4 8 9 -24 108.390 72.2891 3 8 -9 -24-35.1753 75.5537 4 8 9 -23 11.7919 62.0121 3 8 -9 -23 82.3448 82.1714 4 8 -9 -22 1567.27 175.759 4 8 9 -22 1696.18 183.150 3 8 9 -21 121.564 71.2341 3 8 -9 -21 220.121 81.1451 4 8 9 -20 1534.03 168.371 3 8 -9 -20 1512.62 168.534 4 8 9 -19 296.725 140.492 6 8 9 -19 368.907 98.0177 3 8 -9 -19 154.252 77.5433 4 8 9 -18 249.286 81.3639 3 8 -9 -18 297.146 79.0161 4 8 9 -17 331.538 89.2144 3 8 9 -17 598.641 209.193 6 8 -9 -17 549.866 114.956 4 8 9 -16 1373.86 327.710 6 8 -9 -16 1226.57 136.757 5 8 -9 -16 1159.57 145.118 4 8 9 -16 1539.63 160.796 3 8 9 -15 275.692 190.297 6 8 -9 -15 439.077 95.0781 5 8 9 -15 433.633 95.2647 3 8 -9 -15 324.595 92.9928 4 8 9 -14 1011.45 296.475 6 8 -9 -14 979.881 128.000 5 8 9 -14 1085.15 137.446 3 8 -9 -14 1078.48 142.390 4 8 -9 -13-74.2148 49.5590 5 8 9 -13-9.44510 52.2490 3 8 -9 -13 63.5672 62.4993 4 8 9 -13-61.4599 128.546 6 8 -9 -12 1056.00 135.540 5 8 9 -12 882.306 120.907 3 8 -9 -12 1241.73 147.011 4 8 9 -12 1048.23 301.121 6 8 -9 -11 1372.36 147.469 5 8 9 -11 1176.30 291.992 6 8 -9 -11 1447.63 153.167 4 8 9 -11 1411.01 143.333 3 8 -9 -10 2958.13 205.770 5 8 -9 -10 3123.01 220.047 4 8 9 -10 3222.54 479.221 6 8 -9 -9 1584.40 158.860 4 8 9 -9 1199.31 292.413 6 8 -9 -9 1428.40 150.369 5 8 -9 -8 18.9553 52.0718 5 8 -9 -8-41.1504 63.9414 4 8 9 -8 121.992 183.598 6 8 -9 -7 3729.14 227.706 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840.910 6 9 8 1 25.4789 99.3255 6 9 8 2 662.186 233.134 6 9 8 3 3013.87 423.182 6 9 -8 4 280.764 76.0553 4 9 8 4 125.382 127.019 6 9 -8 5 382.377 87.4324 4 9 8 5 76.7774 120.438 6 -9 -8 -6 139.036 55.2353 2 9 -8 6 148.245 52.5430 4 -9 -8 -7 9385.75 366.479 2 9 -8 7 9634.38 367.351 4 9 -8 7 9488.39 681.517 1 9 8 7 9947.86 785.294 6 9 -8 8 2981.23 210.109 4 9 -8 8 2646.49 377.022 1 9 8 8 3400.11 475.660 6 -9 -8 -8 3068.45 214.908 2 9 -8 9 1719.61 164.333 4 9 -8 9 1435.69 298.325 1 9 8 9 1135.97 279.585 6 -9 -8 -9 1557.62 158.333 2 -9 -8 -10 3224.04 229.452 2 9 -8 10 3171.85 223.776 4 9 8 10 3620.58 489.973 6 9 -8 10 2830.96 408.910 1 9 -8 11 7243.51 335.770 4 9 8 11 7432.86 703.623 6 -9 -8 -11 6909.18 340.703 2 9 -8 11 7100.93 673.131 1 -9 -8 -12 477.676 113.391 2 9 -8 12 395.521 93.8539 4 9 -8 12 122.694 124.468 1 9 8 12 475.496 204.139 6 9 -8 13 1720.80 174.255 4 9 -8 13 1281.99 316.764 1 -9 -8 -13 1635.40 175.035 2 9 8 13 1343.69 334.889 6 -9 -8 -14 111.148 67.3099 2 9 -8 14 17.0626 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100.108 4 9 9 -24 143.243 74.4941 3 9 -9 -24 237.455 83.7980 4 9 9 -23 569.007 118.655 3 9 -9 -23 748.966 127.385 4 9 9 -22 50.2146 72.7661 3 9 -9 -22 40.0074 73.5843 4 9 9 -21 502.278 107.214 3 9 -9 -21 555.087 112.868 4 9 9 -20 189.209 84.1048 3 9 -9 -20 292.187 95.3870 4 9 -9 -19 2409.09 205.420 4 9 9 -19 2225.43 196.831 3 9 9 -18-76.9802 69.6202 3 9 9 -18 30.0300 135.933 6 9 -9 -18 108.950 68.9267 4 9 9 -17 804.692 125.841 3 9 -9 -17 848.229 120.450 5 9 -9 -17 786.985 133.264 4 9 -9 -16 48.2938 59.8947 5 9 9 -16 34.5032 59.2642 3 9 -9 -16 39.5987 59.2668 4 9 9 -15 221.105 82.9155 3 9 -9 -15 109.581 59.6710 5 9 -9 -15 173.313 89.5746 4 9 9 -14 593.725 287.554 6 9 -9 -14 590.200 107.296 5 9 9 -14 556.909 102.393 3 9 -9 -14 813.493 133.101 4 9 9 -13 3392.20 514.906 6 9 -9 -13 3376.37 227.055 5 9 -9 -13 3937.01 253.191 4 9 9 -13 3391.06 228.691 3 9 9 -12 2090.07 402.876 6 9 -9 -12 2212.10 186.176 5 9 -9 -12 2242.19 197.202 4 9 9 -12 2163.41 182.278 3 9 -9 -11 4431.39 261.362 5 9 -9 -11 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386.202 94.0471 4 9 9 1 373.322 142.070 6 9 -9 2 3666.55 234.379 4 9 -9 2 3914.97 236.850 5 9 9 2 3792.66 501.235 6 9 -9 3-11.2393 48.2976 4 9 9 3 32.9283 144.569 6 9 -9 3 33.3359 51.8661 5 9 -9 4 201.532 64.9102 5 9 -9 4 261.863 81.9003 4 9 9 4 94.2194 109.104 6 9 -9 5 108.280 59.6147 5 -9 -9 -5 84.7655 49.0162 2 9 -9 5 173.382 71.3228 4 9 -9 6 270.892 79.6299 5 -9 -9 -6 161.752 62.5351 2 9 -9 6 87.9877 57.6592 4 9 9 6 141.359 133.961 6 -9 -9 -7 518.830 98.7027 2 9 -9 7 555.498 101.694 4 9 -9 7 430.502 86.2287 5 9 9 7 530.191 227.595 6 9 -9 8 163.270 64.9966 5 -9 -9 -8 172.247 72.7150 2 9 -9 8 251.576 76.5495 4 9 9 8 118.301 178.663 6 9 -9 9 457.808 187.284 1 -9 -9 -9 488.819 98.2552 2 9 -9 9 541.432 98.1440 4 9 9 9 362.829 170.160 6 9 9 10 144.857 184.447 6 -9 -9 -10 209.643 72.8638 2 9 -9 10 173.136 177.292 1 9 -9 10 179.674 68.0956 4 9 -9 11 1264.20 304.788 1 9 -9 11 1481.90 159.143 4 9 9 11 1322.24 355.881 6 -9 -9 -11 1596.13 168.038 2 9 -9 12 1919.03 364.147 1 9 -9 12 2100.62 189.191 4 -9 -9 -12 2053.27 201.051 2 9 9 12 2137.50 410.090 6 -9 -9 -13 369.596 102.290 2 9 -9 13 337.354 170.958 1 9 -9 13 338.027 93.3587 4 9 9 13 469.371 235.843 6 9 -9 14 1816.22 182.969 4 9 -9 14 1528.94 317.648 1 -9 -9 -14 1950.57 200.399 2 9 9 14 1959.40 387.210 6 -9 -9 -15 1232.16 164.419 2 9 -9 15 1619.57 175.489 4 9 -9 15 1286.32 339.499 1 9 9 15 1818.30 380.534 6 -9 -9 -16 44.9770 72.0286 2 -9 -9 -17 545.783 126.989 2 -9 -9 -18 1408.08 180.583 2 -9 -9 -19-12.2368 79.9406 2 -9 -9 -20 25.8095 83.7197 2 -9 -9 -21 973.139 155.719 2 -9 -9 -22 115.614 78.3164 2 -9 -9 -23 1416.00 167.081 2 -9 -9 -24 95.0836 83.6648 2 -9 -9 -25 911.644 128.210 2 -9 -9 -26 45.4380 65.8500 2 -9 -9 -27 142.431 57.2057 2 -9 -9 -28 269.125 66.2485 2 -9 -9 -29 239.938 55.1611 2 -9 -9 -30 4.15476 32.4111 2 9 -10 -31-50.7817 32.8308 4 9 10 -30 185.875 49.9586 3 9 -10 -30 287.525 58.6907 4 9 10 -29 334.770 64.5948 3 9 -10 -29 536.988 80.9887 4 9 10 -28 594.513 88.9359 3 9 -10 -28 674.178 95.4746 4 9 10 -27 107.768 58.0582 3 9 -10 -27-33.2591 61.3238 4 9 10 -26 31.8071 50.9918 3 9 -10 -26 26.2259 59.4386 4 9 10 -25 148.705 64.7733 3 9 -10 -25 97.6084 63.3115 4 9 10 -24-48.1675 66.3417 3 9 -10 -24-39.4445 72.2676 4 9 10 -23 90.2155 69.7375 3 9 -10 -23 177.641 81.2806 4 9 10 -22 893.277 129.807 3 9 -10 -22 960.594 136.367 4 9 10 -21 540.287 105.035 3 9 -10 -21 682.361 129.692 4 9 10 -20 297.848 81.5727 3 9 -10 -20 408.011 104.083 4 9 10 -19 67.9828 61.2093 3 9 -10 -19 81.4424 80.1813 4 9 10 -18 70.9881 76.2852 3 9 -10 -18 203.561 104.272 4 9 -10 -17 79.8851 60.1204 5 9 10 -17 63.1889 60.7190 3 9 -10 -17 89.4692 68.7052 4 9 10 -16 2447.87 463.571 6 9 -10 -16 2050.52 184.963 5 9 -10 -16 2155.25 200.740 4 9 10 -16 2045.68 188.137 3 9 10 -15 3424.13 539.175 6 9 -10 -15 3300.66 231.545 5 9 -10 -15 3045.34 235.043 4 9 10 -15 3259.21 231.664 3 9 10 -14 438.292 235.673 6 9 10 -14 558.713 96.1984 3 9 -10 -14 520.733 102.618 5 9 -10 -14 577.073 116.660 4 9 10 -13 978.205 282.905 6 9 10 -13 1017.96 126.142 3 9 -10 -13 1117.43 145.336 5 9 -10 -13 1002.86 149.339 4 9 10 -12 21.2777 111.066 6 9 10 -12 101.808 50.6158 3 9 -10 -12 171.364 76.1847 5 9 -10 -12 68.6869 67.0806 4 9 -10 -11 150.903 78.8098 5 9 -10 -11 113.129 73.5573 4 9 -10 -10 4842.57 279.946 5 9 -10 -10 4687.65 281.625 4 9 10 -10 4745.40 614.687 6 9 10 -9 900.761 266.215 6 9 -10 -9 988.475 133.888 5 9 -10 -9 948.463 131.657 4 9 -10 -8 5058.50 289.059 5 9 -10 -8 5198.97 290.639 4 9 10 -8 4739.74 598.172 6 9 -10 -7 718.553 111.262 5 9 -10 -7 597.450 110.000 4 9 10 -7 673.659 258.653 6 9 -10 -6 1681.99 169.163 5 9 -10 -6 1556.30 163.571 4 9 10 -6 1891.43 383.967 6 9 -10 -5 52.9917 56.1904 5 9 -10 -5 29.0856 71.5714 4 9 10 -5-54.4093 140.099 6 9 -10 -4 1002.60 137.169 5 9 -10 -4 1101.73 135.419 4 9 10 -4 1345.39 328.928 6 9 -10 -3 13.8217 55.8560 5 9 -10 -3 10.2772 65.0321 4 9 -10 -2 1471.23 157.231 4 9 -10 -2 1452.32 159.864 5 9 10 -2 1092.82 265.600 6 9 -10 -1 2379.33 197.862 5 9 -10 -1 2321.00 194.028 4 9 10 -1 2040.36 398.838 6 9 -10 0 867.160 122.614 5 9 10 0 1188.02 302.886 6 9 -10 0 988.203 134.751 4 9 -10 1 2441.96 197.501 5 9 -10 1 2606.87 206.486 4 9 10 1 2522.59 430.380 6 9 -10 2 677.209 118.677 4 9 10 2 413.417 208.348 6 9 -10 2 670.403 117.553 5 9 -10 3 1313.02 147.493 5 9 -10 3 1349.82 156.089 4 9 10 3 1144.45 307.277 6 9 -10 4 4479.37 265.033 5 9 -10 4 4584.70 269.685 4 9 10 4 4605.21 585.086 6 9 -10 5 465.927 100.040 5 9 -10 5 712.524 111.303 4 9 10 5 222.506 186.253 6 -9 -10 -6 154.227 72.5640 2 9 -10 6 104.428 53.8144 5 9 -10 6 17.5896 60.2203 4 9 -10 7 2359.16 192.479 5 9 -10 7 2467.60 202.626 4 9 10 7 1857.39 408.755 6 -9 -10 -7 2464.04 195.070 2 -9 -10 -8 129.112 70.1339 2 9 -10 8 105.489 64.1972 4 9 10 8 36.8848 133.354 6 9 -10 8 95.9919 62.8080 5 -9 -10 -9 674.465 111.740 2 9 -10 9 523.278 109.678 4 9 10 9 717.600 219.314 6 -9 -10 -10 57.1037 60.3854 2 9 -10 10 170.170 84.4128 4 9 10 10 262.203 206.287 6 -9 -10 -11-11.4168 56.8333 2 9 -10 11-120.065 76.0855 4 9 -10 12 1448.70 170.048 4 -9 -10 -12 1349.33 161.965 2 9 10 12 1409.71 360.162 6 -9 -10 -13 675.228 121.075 2 9 -10 13 712.001 117.197 4 9 10 13 488.496 279.023 6 -9 -10 -14 890.747 138.980 2 9 -10 14 747.745 127.378 4 9 -10 15 1605.26 173.536 4 -9 -10 -15 1582.63 179.961 2 -9 -10 -16 1232.14 161.206 2 -9 -10 -17 925.427 147.997 2 -9 -10 -18 253.174 96.0362 2 -9 -10 -19 667.924 123.770 2 -9 -10 -20 277.166 85.3951 2 -9 -10 -21 665.838 129.271 2 -9 -10 -22 9.78430 69.2453 2 -9 -10 -23 312.744 97.8590 2 -9 -10 -24-20.6816 64.7981 2 -9 -10 -25 671.571 105.294 2 -9 -10 -26 1059.31 120.199 2 -9 -10 -27 103.695 56.1776 2 -9 -10 -28 116.023 44.6040 2 -9 -10 -29 17.6804 25.7462 2 9 -11 -30 82.7912 38.9271 4 9 -11 -29-83.3850 41.1396 4 9 -11 -28 352.482 71.6391 4 9 11 -28 247.232 55.1518 3 9 -11 -27 1027.25 113.501 4 9 11 -27 885.129 95.8977 3 9 11 -26 98.9095 55.1367 3 9 -11 -26 66.3038 57.0509 4 9 11 -25 170.405 58.4086 3 9 -11 -25-0.86612 62.6910 4 9 11 -24 709.030 105.114 3 9 -11 -24 816.985 122.954 4 9 11 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1764.05 185.645 4 9 11 -8 1732.18 374.403 6 9 -11 -7 1970.05 192.841 4 9 -11 -7 1453.55 167.254 5 9 11 -7 1672.74 383.490 6 9 -11 -6 1.86349 57.5274 5 9 -11 -6-109.818 77.7263 4 9 -11 -5 932.434 135.636 5 9 -11 -5 1440.18 164.571 4 9 11 -5 1188.02 342.779 6 9 -11 -4 1496.05 173.329 5 9 -11 -4 1331.90 154.653 4 9 11 -4 1098.09 304.078 6 9 -11 -3 1453.64 168.802 5 9 11 -3 1066.92 312.504 6 9 -11 -3 1472.13 165.538 4 9 -11 -2 1834.69 181.751 4 9 -11 -2 1955.46 189.827 5 9 11 -2 1815.22 379.718 6 9 -11 -1 384.997 95.1846 4 9 11 -1 406.935 213.327 6 9 -11 -1 398.684 97.4197 5 9 -11 0 573.115 110.052 5 9 11 0 490.937 240.688 6 9 -11 0 810.093 129.358 4 9 -11 1 3855.98 254.207 4 9 -11 1 4247.21 264.806 5 9 11 1 4239.05 576.446 6 9 -11 2 709.688 119.895 4 9 -11 2 657.828 116.379 5 9 -11 3 94.5479 58.2221 5 9 -11 3 157.493 78.0403 4 9 11 3 147.796 162.690 6 9 -11 4 62.2183 76.5843 4 9 11 4 24.2692 170.440 6 9 -11 4 11.3338 58.0671 5 9 -11 5 397.463 99.7734 5 9 -11 5 424.503 96.2346 4 9 -11 6 414.865 102.143 5 9 -11 6 550.388 110.732 4 9 11 6 620.842 236.791 6 9 -11 7 945.409 126.943 5 9 11 7 1005.80 299.191 6 9 -11 7 906.191 126.678 4 9 -11 8 1638.80 172.422 4 9 -11 8 1647.37 161.684 5 -9 -11 -8 1439.81 157.947 2 9 11 8 1502.04 363.031 6 9 -11 9 2282.59 198.294 4 -9 -11 -9 2354.01 195.382 2 9 11 9 2021.87 423.769 6 -9 -11 -10 135.581 72.7119 2 9 -11 10-50.3008 69.9653 4 9 -11 11 3132.20 230.099 4 -9 -11 -11 3011.38 226.733 2 9 -11 12 8569.46 373.686 4 -9 -11 -12 8158.81 375.862 2 9 -11 13 99.2584 75.8974 4 -9 -11 -13 157.876 76.9429 2 9 -11 14 636.643 116.777 4 -9 -11 -14 469.378 105.494 2 -9 -11 -15 559.367 113.121 2 -9 -11 -16 203.962 81.2427 2 -9 -11 -17 609.973 119.084 2 -9 -11 -18 816.036 130.825 2 -9 -11 -18 747.129 102.796 5 -9 -11 -19 224.524 89.2059 2 -9 -11 -20 42.0814 75.1382 2 -9 -11 -21 214.480 87.9317 2 -9 -11 -22 271.007 83.4951 2 -9 -11 -23 543.132 104.381 2 -9 -11 -24 72.6792 57.1343 2 -9 -11 -25 39.3197 43.9161 2 -9 -11 -26 240.723 57.5616 2 -9 -11 -27 288.864 57.9450 2 9 -12 -29 133.055 40.8611 4 9 -12 -28 20.6063 41.2663 4 9 -12 -27 2.71819 43.6392 4 9 -12 -26 197.831 62.8056 4 9 -12 -25 1605.51 145.140 4 9 -12 -24 658.388 109.064 4 9 -12 -23 801.948 122.325 4 9 -12 -22 146.050 78.3476 4 9 -12 -21 1157.18 149.330 4 9 -12 -20 115.967 91.6663 4 9 -12 -19 44.5791 75.8649 4 9 -12 -19-53.6843 55.3573 5 9 -12 -18 80.9786 53.7978 5 9 -12 -18 57.3695 88.1928 4 9 -12 -17-5.62905 61.2170 5 9 -12 -17 33.6855 74.2036 4 9 -12 -16 303.340 89.6390 5 9 -12 -16 279.942 96.6878 4 9 -12 -15 416.217 104.530 5 9 -12 -15 531.669 112.270 4 9 -12 -14 25.0758 67.7782 5 9 -12 -14-5.92563 74.5381 4 9 -12 -13 111.065 83.5298 5 9 -12 -13 124.380 88.2745 4 9 -12 -12 924.922 138.302 5 9 -12 -12 1012.47 155.846 4 9 -12 -11 446.105 103.215 5 9 -12 -11 472.089 117.901 4 9 12 -10 95.0848 124.502 6 9 -12 -10 25.2804 76.0781 5 9 -12 -10 20.1304 71.5832 4 9 12 -9 83.3174 140.707 6 9 -12 -9 103.127 78.3300 5 9 -12 -9 187.609 89.3677 4 9 -12 -8 6286.01 341.013 5 9 -12 -8 6057.77 332.032 4 9 12 -8 5305.94 664.736 6 9 -12 -7 429.952 114.809 5 9 -12 -7 359.040 106.723 4 9 12 -7 384.266 228.590 6 9 -12 -6 3550.81 260.337 5 9 -12 -6 3477.56 255.261 4 9 12 -6 3836.61 566.397 6 9 -12 -5 347.342 106.066 5 9 -12 -5 364.276 106.134 4 9 12 -5 647.414 278.266 6 9 -12 -4 116.323 86.1162 5 9 -12 -4 95.2766 71.4709 4 9 12 -4 211.936 220.439 6 9 -12 -3 3931.68 268.393 5 9 -12 -3 3784.79 259.393 4 9 12 -3 3425.93 534.287 6 9 -12 -2 1501.17 175.618 5 9 -12 -2 1634.43 178.008 4 9 12 -2 1602.82 377.979 6 9 -12 -1 55.6519 69.2330 5 9 -12 -1-11.7178 66.7654 4 9 12 -1-109.450 166.315 6 9 -12 0 3353.73 245.200 5 9 -12 0 3306.39 241.107 4 9 12 0 2780.92 481.504 6 9 -12 1 1294.71 158.647 4 9 -12 1 1294.72 161.884 5 9 -12 2 176.007 83.8566 5 9 -12 2 146.531 80.5289 4 9 12 2 62.5485 204.490 6 9 -12 3 1136.57 153.235 5 9 -12 3 1387.54 160.114 4 9 -12 4 80.7836 68.7975 5 9 -12 4 53.2402 65.3066 4 9 12 4 154.114 177.404 6 9 -12 5 700.753 120.074 5 9 -12 5 878.893 134.060 4 9 12 5 835.376 304.448 6 9 -12 6 1034.73 140.290 5 9 -12 6 838.679 127.985 4 9 -12 7 347.728 94.1382 4 9 -12 7 243.124 89.3402 5 9 -12 8 114.878 58.3898 5 9 -12 8 33.6424 63.5923 4 9 -12 9 482.593 98.3255 4 9 -12 10 2629.06 211.627 4 -9 -12 -11 15.8009 58.4996 2 9 -12 11-9.57762 73.1035 4 -9 -12 -12 144.477 64.8678 2 9 -12 12 203.985 70.6929 4 -9 -12 -13 977.339 137.239 2 9 -12 13 1098.02 139.045 4 9 -12 14 2393.90 196.365 4 -9 -12 -14 2157.15 193.150 2 -9 -12 -15 41.6942 61.2698 2 -9 -12 -16 67.0161 64.3873 5 -9 -12 -16 98.6799 64.8537 2 -9 -12 -17-39.2788 64.9733 5 -9 -12 -17 35.0684 56.4783 2 -9 -12 -18 20.5545 50.8439 5 -9 -12 -18-68.1459 69.5520 2 -9 -12 -19 980.595 133.124 2 -9 -12 -20 178.750 71.4339 2 -9 -12 -21 619.752 98.2048 2 -9 -12 -22 321.026 78.6498 2 -9 -12 -23 292.916 70.0777 2 -9 -12 -24 90.2504 47.6244 2 -9 -12 -25 188.084 51.8974 2 -9 -12 -26 121.291 37.4885 2 9 -13 -28 413.033 56.6109 4 9 -13 -27 113.028 40.5423 4 9 -13 -26 27.5650 40.1234 4 9 -13 -25 718.711 94.5076 4 9 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112.017 6 10 -2 -11 240.381 92.9598 6 10 2 -10-71.9239 116.179 6 10 -2 -10 27.3124 133.536 6 10 2 -9 119.775 119.678 6 10 -2 -9 58.4170 92.5860 6 10 2 -8 109.681 95.1835 6 10 -2 -8 277.553 123.241 6 10 2 -7-79.6040 112.612 6 10 -2 -7-49.9182 108.323 6 10 -2 -6 5041.86 414.466 6 10 2 -6 4460.68 426.702 6 10 -2 -5 38113.1 1070.91 6 10 2 -5 39292.0 1227.82 6 10 2 -4 192.086 105.005 6 10 -2 -4 164.337 82.1496 6 10 2 -3 5451.72 442.050 6 10 -2 -3 5484.46 370.989 6 10 -2 -2 666.994 134.599 6 10 2 -2 749.130 177.935 6 10 2 -1 879.646 185.216 6 10 2 0 2639.73 296.846 6 10 2 1 2292.13 267.293 6 10 2 2 8387.67 511.541 6 10 -2 3 7636.72 445.713 1 10 2 3 8364.27 504.729 6 10 -2 4 1009.02 179.735 1 10 2 4 1160.27 188.988 6 10 -2 5 810.201 183.329 1 10 2 5 1103.42 193.875 6 10 2 6 122.079 67.4347 6 10 -2 6 52.2227 79.7676 1 10 -2 7 6334.34 495.863 1 10 -2 8 8096.81 590.974 1 10 2 9 2426.21 351.303 1 10 -2 9 2571.63 356.246 1 10 2 10 1383.38 276.857 1 10 -2 10 2142.55 335.026 1 10 -2 11 2336.55 364.672 1 10 2 11 2425.73 380.358 1 10 2 12 465.857 185.107 1 -10 -2 -12 627.705 101.319 2 10 -2 12 671.719 220.553 1 -10 -2 -13 283.786 77.4843 2 10 -2 13 180.949 141.416 1 10 2 13-29.3318 139.386 1 10 -2 14-85.4286 131.632 1 10 2 14-164.282 146.300 1 -10 2 -14 56.6098 54.7421 2 -10 -2 -14 142.139 76.2919 2 10 2 15 1025.70 272.141 1 -10 2 -15 1030.38 126.099 2 -10 -2 -15 1284.58 149.806 2 10 -2 15 1218.61 301.883 1 -10 -2 -16 1108.88 149.604 2 10 2 16 731.334 262.551 1 10 -2 16 1471.51 359.660 1 -10 2 -16 1163.67 133.102 2 -10 -2 -17 123.330 81.5145 2 10 -2 17-87.8643 126.230 1 10 2 17 100.353 126.986 1 -10 -2 -18 631.359 125.383 2 10 -2 18 795.480 265.062 1 10 2 18 807.816 278.268 1 10 2 19 2965.54 508.948 1 10 -2 19 1672.11 381.250 1 -10 -2 -19 2436.36 217.889 2 -10 -2 -20 138.690 81.7108 2 -10 -2 -21 1053.67 152.883 2 -10 -2 -22 839.014 144.183 2 -10 -2 -23 787.079 137.770 2 -10 -2 -24 18.8548 76.0215 2 -10 -2 -25 519.887 115.977 2 -10 -2 -26 19.5729 61.2258 2 -10 -2 -27-13.5701 55.0017 2 -10 -2 -28 150.909 57.1999 2 -10 -2 -29 431.264 78.2507 2 -10 -2 -30 26.9429 36.2915 2 10 3 -35 47.5651 41.0356 3 10 3 -34 42.4070 41.6308 3 10 3 -33 42.9275 54.1920 3 10 3 -32 386.098 87.4748 3 10 -3 -31 182.694 56.3660 3 10 3 -31 295.345 83.6887 3 10 -3 -30 171.825 64.4046 3 10 3 -30 272.324 94.8064 3 10 -3 -29-12.1098 57.4290 3 10 3 -29 77.4641 84.9281 3 10 -3 -28 56.4688 54.2851 3 10 3 -28 257.633 106.334 3 10 -3 -27 907.028 127.431 3 10 3 -27 754.412 144.124 3 10 -3 -26 353.622 89.4859 3 10 3 -26 364.036 110.860 3 10 -3 -25 322.121 97.2213 3 10 3 -25 498.899 124.136 3 10 -3 -24-28.7467 55.8364 3 10 3 -24 141.750 88.5150 3 10 -3 -23 214.233 83.8682 3 10 3 -23 191.589 101.269 3 10 -3 -22 32.2330 58.8586 3 10 3 -22 95.4005 81.3489 3 10 3 -21 2307.15 447.233 6 10 -3 -21 2402.27 195.627 3 10 3 -21 2565.80 220.233 3 10 3 -20 71.3111 127.560 6 10 -3 -20 147.510 72.2193 3 10 3 -20 75.4508 86.5238 3 10 3 -19 1625.14 361.109 6 10 -3 -19 1551.31 152.227 3 10 3 -19 1731.88 181.284 3 10 3 -18 1148.74 276.838 6 10 -3 -18 1433.72 147.043 3 10 3 -18 1646.16 173.170 3 10 3 -17 2608.25 438.176 6 10 -3 -17 2480.11 186.640 3 10 3 -17 2412.02 198.974 3 10 3 -16 19.5503 132.342 6 10 3 -16 25.3690 55.4595 3 10 3 -15-50.2292 120.952 6 10 3 -15-17.2219 49.0927 3 10 3 -14 2101.14 367.235 6 10 3 -14 1797.48 168.705 3 10 3 -13-40.5696 144.843 6 10 3 -12 4294.58 496.769 6 10 3 -11 25855.6 1191.50 6 10 3 -10 517.136 190.121 6 10 3 -9 569.628 202.800 6 10 3 -8 1592.93 286.972 6 10 3 -7 5462.98 499.719 6 10 3 -6 1084.76 233.640 6 10 3 -5 16562.9 827.169 6 10 3 -4 3892.15 405.670 6 10 3 -3 1000.95 214.381 6 10 3 -2-97.8867 103.073 6 10 3 -1 218.230 104.985 6 10 3 0 1534.63 239.580 6 10 3 1 12002.1 646.990 6 10 3 2 2072.37 276.423 6 10 -3 3 366.210 108.067 1 10 3 3 37.4522 87.3621 6 10 -3 4 2045.25 243.049 1 10 3 4 1714.08 246.212 6 10 -3 5 5752.72 431.911 1 10 3 5 5791.21 454.112 6 10 3 6 181.069 118.267 6 10 -3 6 245.420 118.170 1 10 -3 7 2141.63 296.445 1 10 3 7 1326.57 217.628 6 10 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3996.94 224.651 4 10 4 -16 4562.41 271.403 3 10 4 -16 3897.50 527.984 6 10 4 -15 487.619 200.037 6 10 4 -15 754.089 120.465 3 10 4 -14-4.28394 57.5339 3 10 4 -14-187.588 210.639 6 10 4 -13 208.410 147.505 6 10 4 -12 2306.22 381.851 6 10 4 -11 309.640 162.720 6 10 4 -10 3087.11 420.153 6 10 4 -9 3861.27 453.482 6 10 4 -8 1730.73 313.578 6 10 4 -7-165.652 160.509 6 10 4 -6 21.8550 102.738 6 10 4 -5 1648.25 285.923 6 10 4 -4 1839.51 298.996 6 10 4 -3 169.801 103.213 6 10 4 -2 1688.98 267.904 6 10 4 -1 2670.29 337.010 6 10 4 0 262.043 119.967 6 10 4 1 1158.83 220.719 6 10 4 2 951.002 211.952 6 10 4 3 4089.50 408.490 6 10 4 4 3486.27 376.140 6 10 -4 5 193.919 98.8711 1 10 4 5 1195.51 238.549 6 10 -4 6 143.158 116.757 1 10 4 6-26.2946 82.9000 6 10 -4 7 1044.62 211.915 1 10 4 7 909.601 195.998 6 10 -4 8 1425.04 253.566 1 10 4 8 1263.53 247.624 6 10 -4 9 993.468 232.967 1 10 4 9 511.547 165.359 6 -10 -4 -10 4363.26 257.036 2 10 -4 10 4094.24 235.980 4 10 -4 10 4654.84 501.768 1 10 4 10 4064.89 249.054 3 10 4 10 3348.07 391.329 6 10 -4 11-17.4364 98.5975 1 10 -4 11 220.908 70.0814 4 -10 -4 -11 102.510 67.3653 2 -10 -4 -12 3996.08 253.203 2 10 -4 12 3622.68 233.295 4 10 -4 12 3933.91 489.799 1 10 4 13 566.859 215.547 1 10 -4 13 648.213 246.746 1 10 -4 13 508.020 105.176 4 -10 -4 -13 504.092 101.558 2 10 -4 14 4220.89 542.582 1 10 4 14 4510.72 561.109 1 -10 -4 -14 4599.42 282.381 2 10 -4 15 2482.14 430.169 1 10 4 15 1944.34 387.560 1 -10 -4 -15 2542.01 220.854 2 10 -4 16 541.221 252.761 1 -10 -4 -16 225.617 99.2469 2 10 -4 17 579.967 230.233 1 -10 -4 -17 233.415 86.5410 2 10 4 17 611.762 271.154 1 -10 -4 -18 363.197 106.509 2 10 -4 18 492.075 219.508 1 -10 -4 -19 2260.87 213.267 2 -10 -4 -20 238.752 102.931 2 -10 -4 -21-26.3792 91.7447 2 -10 -4 -22 411.772 109.295 2 -10 -4 -23 22.2018 75.6884 2 -10 -4 -24-68.6100 83.1344 2 -10 -4 -25 3652.42 258.663 2 -10 -4 -26 57.4610 66.1319 2 -10 -4 -27 377.357 91.7059 2 -10 -4 -28 205.381 74.8548 2 -10 -4 -29 11.0156 47.1056 2 -10 -4 -30 43.1115 44.4393 2 -10 -4 -31 654.638 76.3325 2 10 5 -35-36.0076 30.4904 3 10 5 -34 49.5674 35.8726 3 10 5 -33 457.428 78.0235 3 10 5 -32 110.219 63.4913 3 10 5 -31-2.32176 62.7317 3 10 5 -30 279.581 88.3071 3 10 5 -29 6.53116 70.5072 3 10 5 -28 656.077 121.735 3 10 5 -27 157.160 84.3677 3 10 5 -26 61.9312 88.8943 3 10 -5 -26 52.7113 55.4003 4 10 5 -25 333.208 105.018 3 10 -5 -25 226.594 72.8672 4 10 5 -24 223.135 98.5419 3 10 -5 -24 75.3968 55.9764 4 10 5 -23 88.0053 80.2821 3 10 -5 -23 78.8215 46.9434 4 10 5 -22 93.7840 84.0168 3 10 -5 -22 98.2053 65.7739 4 10 -5 -21 3310.37 223.702 4 10 5 -21 2694.76 494.216 6 10 5 -21 3510.74 255.803 3 10 5 -20 421.390 199.677 6 10 5 -20 177.141 91.1055 3 10 -5 -20 165.518 69.6329 4 10 5 -19 119.237 124.425 6 10 5 -19 127.580 80.7010 3 10 -5 -19 154.484 64.7934 4 10 5 -18 2120.46 423.940 6 10 -5 -18 2003.46 173.669 4 10 5 -18 2252.93 206.923 3 10 5 -17 383.148 200.525 6 10 5 -17 262.815 87.0541 3 10 -5 -17 199.967 64.4250 4 10 5 -16 1194.32 313.192 6 10 5 -16 945.787 134.798 3 10 -5 -16 835.727 113.278 4 10 5 -15 122.058 58.0606 3 10 -5 -15 135.725 52.0138 4 10 5 -14 1097.80 293.106 6 10 -5 -14 1238.03 130.741 4 10 5 -14 1175.75 143.372 3 10 5 -13 555.627 101.300 3 10 5 -13 542.139 201.201 6 10 5 -12 1283.89 143.447 3 10 5 -12 1400.95 324.805 6 10 5 -11 151.831 166.479 6 10 5 -10 2937.14 411.700 6 10 5 -9 4905.21 532.207 6 10 5 -8 7139.05 620.805 6 10 5 -7 3743.79 449.052 6 10 5 -6 3413.30 420.402 6 10 5 -5 1430.55 285.072 6 10 5 -4 13445.3 797.898 6 10 5 -3 5389.77 510.563 6 10 5 -2 3943.95 433.185 6 10 5 -1 309.473 177.308 6 10 5 0 11202.0 707.497 6 10 5 1 3538.92 401.432 6 10 5 2 6534.02 551.181 6 10 5 3 17256.7 881.616 6 10 5 4 2165.23 324.891 6 10 5 5 10690.4 700.543 6 10 -5 6 6453.29 496.688 1 10 5 6 6440.39 545.730 6 10 5 7 46.0136 119.426 6 10 -5 7 56.7967 84.9804 1 10 5 8 723.418 199.387 6 10 -5 8 805.682 202.720 1 10 -5 9 212.673 139.474 1 10 -5 9 138.234 74.9075 4 -10 -5 -9 136.611 58.4027 2 10 5 9 139.705 59.7522 3 10 5 9 305.600 145.211 6 10 -5 10 1654.48 309.643 1 -10 -5 -10 1661.90 167.192 2 10 -5 10 1934.41 172.156 4 10 5 10 1591.66 312.500 6 10 -5 11 266.497 174.640 1 10 -5 11 386.868 83.2365 4 -10 -5 -11 272.216 84.9142 2 10 5 11 522.608 176.649 6 10 -5 12 5288.86 572.709 1 10 -5 12 5586.19 293.703 4 -10 -5 -12 5371.94 298.588 2 10 -5 13 451.808 200.553 1 -10 -5 -13 537.610 106.197 2 10 -5 13 512.599 102.603 4 10 -5 14 2273.65 397.182 1 10 -5 14 2744.97 215.718 4 -10 -5 -14 2957.30 235.999 2 10 -5 15 3418.84 500.567 1 10 5 15 4244.97 576.380 1 -10 -5 -15 4078.51 279.472 2 10 -5 16 2780.53 461.847 1 10 5 16 2581.09 452.516 1 -10 -5 -16 2714.40 231.848 2 10 -5 17 1255.01 306.871 1 -10 -5 -17 1370.42 181.133 2 10 5 17 886.232 275.005 1 10 5 18 2067.39 411.876 1 -10 -5 -18 2275.74 223.158 2 10 -5 18 2677.36 475.834 1 -10 -5 -19 2801.87 242.817 2 -10 -5 -20 3504.05 264.836 2 -10 -5 -21 138.158 88.8550 2 -10 -5 -22 177.418 95.0646 2 -10 -5 -23 506.173 125.557 2 -10 -5 -24 110.938 93.8220 2 -10 -5 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1055.83 145.932 3 10 -6 -18 955.550 126.884 4 10 6 -17 177.845 148.624 6 10 6 -17 236.211 90.0391 3 10 -6 -17 198.737 73.7484 4 10 -6 -16 4234.17 251.190 4 10 6 -16 4332.31 274.738 3 10 6 -16 4454.89 583.526 6 10 6 -15 269.981 176.685 6 10 6 -15 179.258 68.5533 3 10 -6 -15 383.015 88.2960 4 10 6 -14 878.269 125.624 3 10 -6 -14 749.213 102.951 5 10 6 -14 535.364 247.503 6 10 -6 -14 807.784 111.040 4 10 6 -13 12.3440 147.528 6 10 -6 -13 116.354 56.6278 5 10 6 -13 2.37583 59.7099 3 10 -6 -13 21.3770 43.1815 4 10 6 -12 422.752 185.033 6 10 -6 -12 373.501 85.0559 5 10 6 -12 400.064 90.4914 3 10 -6 -12 268.553 73.7924 4 10 6 -11 266.520 82.2377 3 10 -6 -11 114.175 66.5718 4 10 6 -10 2301.46 402.128 6 10 6 -9 958.134 262.491 6 10 6 -8 980.681 257.596 6 10 6 -7 2723.04 412.220 6 10 6 -6 429.497 179.846 6 10 6 -5 5087.53 539.952 6 10 6 -4 2271.31 366.758 6 10 6 -3 3120.16 404.604 6 10 6 -2 6862.27 593.553 6 10 6 -1 17.9721 118.800 6 10 6 0 2831.66 386.324 6 10 6 1 1913.36 310.534 6 10 6 2 1749.37 304.454 6 10 6 3 2687.10 363.606 6 10 6 4 521.485 176.676 6 10 6 5 7462.37 622.305 6 10 6 6 1630.44 297.416 6 10 -6 7 197.847 58.5420 4 -10 -6 -7 125.351 60.4067 2 10 -6 7 259.913 122.535 1 10 6 7 129.194 130.736 6 10 6 8 272.548 136.146 6 10 -6 8 525.557 94.4706 4 -10 -6 -8 370.588 82.6436 2 10 6 8 423.797 91.2453 3 10 -6 9 5753.19 549.873 1 10 -6 9 5942.76 293.512 4 10 6 9 5700.38 294.083 3 10 6 9 6201.31 586.647 6 -10 -6 -9 5851.20 298.314 2 -10 -6 -10 4854.01 278.203 2 10 -6 10 4490.33 516.682 1 10 -6 10 4552.33 261.587 4 10 6 10 4894.43 524.055 6 10 -6 11 3898.46 486.548 1 10 -6 11 3770.82 242.893 4 10 6 11 3778.96 475.959 6 -10 -6 -11 3823.45 255.180 2 -10 -6 -12 61.3900 71.3764 2 10 -6 12 209.788 85.1577 4 10 -6 12 459.964 177.949 1 10 6 12 115.672 165.513 6 10 -6 13 4031.45 257.621 4 10 -6 13 3065.17 471.053 1 10 6 13 3086.43 435.327 6 -10 -6 -13 3666.46 255.539 2 -10 -6 -14 71.6788 77.2089 2 10 -6 14-18.6719 76.1472 4 -10 -6 -15 218.914 101.224 2 10 -6 15-444.281 195.584 1 -10 -6 -16 794.636 138.549 2 10 6 16 464.513 168.414 1 -10 -6 -17 54.6991 78.8952 2 10 6 17 334.053 204.897 1 10 -6 17 97.0828 144.406 1 -10 -6 -18 3067.71 254.851 2 -10 -6 -19 464.299 119.249 2 -10 -6 -20 1229.89 172.797 2 -10 -6 -21 1371.91 176.119 2 -10 -6 -22 480.684 126.704 2 -10 -6 -23-41.7576 81.2918 2 -10 -6 -24 83.2097 93.6120 2 -10 -6 -25 529.859 121.463 2 -10 -6 -26 1439.59 159.103 2 -10 -6 -27 161.725 76.1426 2 -10 -6 -28 30.2055 50.2975 2 -10 -6 -29 437.325 80.2090 2 -10 -6 -30 22.9717 36.8061 2 10 7 -34-29.6178 29.0475 3 10 7 -33 166.595 48.4642 3 10 7 -32-52.9039 45.8744 3 10 7 -31 82.3042 50.5738 3 10 7 -30 30.4914 58.7362 3 10 -7 -30-50.6495 42.2347 4 10 7 -29 970.518 126.913 3 10 -7 -29 846.255 97.8815 4 10 7 -28-23.8526 70.5826 3 10 -7 -28 19.1837 48.9580 4 10 7 -27 1086.00 148.422 3 10 -7 -27 914.262 116.746 4 10 7 -26 116.924 83.5899 3 10 -7 -26 27.0561 51.7436 4 10 7 -25 80.3650 69.9409 3 10 -7 -25 6.60589 58.0237 4 10 7 -24 864.110 137.975 3 10 -7 -24 603.571 110.760 4 10 7 -23 425.137 109.183 3 10 -7 -23 527.696 106.570 4 10 7 -22 143.495 89.4021 3 10 -7 -22 218.819 86.8135 4 10 -7 -21 3979.44 251.986 4 10 7 -21 4007.94 273.415 3 10 7 -20 1126.37 157.837 3 10 -7 -20 1162.80 144.810 4 10 7 -19 10.6858 70.4572 3 10 7 -19-28.3912 101.389 6 10 -7 -19 62.0323 62.5205 4 10 7 -18 179.615 173.186 6 10 7 -18 329.659 95.0145 3 10 -7 -18 478.834 101.014 4 10 -7 -17 4906.34 278.166 4 10 7 -17 4788.40 286.761 3 10 7 -16 125.802 74.6220 3 10 -7 -16 101.163 67.0137 4 10 7 -16 199.592 152.924 6 10 7 -15 651.142 263.354 6 10 -7 -15 475.214 87.5735 5 10 7 -15 537.476 109.539 3 10 -7 -15 584.312 109.114 4 10 7 -14 1806.01 397.194 6 10 -7 -14 1538.62 151.254 5 10 -7 -14 1653.45 165.781 4 10 7 -14 1673.13 167.673 3 10 -7 -13 3861.77 236.997 5 10 -7 -13 4085.67 248.723 4 10 7 -13 4504.35 268.872 3 10 7 -13 3746.78 534.825 6 10 -7 -12 112.765 67.9355 5 10 7 -12 140.622 73.6461 3 10 7 -12 258.124 176.866 6 10 -7 -12 119.452 66.3775 4 10 7 -11 2067.57 386.199 6 10 -7 -11 2093.80 177.028 4 10 -7 -11 2083.66 173.937 5 10 7 -11 1952.99 176.759 3 10 7 -10 279.772 153.614 6 10 -7 -10 354.671 80.8212 5 10 7 -10 274.640 71.9616 3 10 -7 -10 172.366 71.1708 4 10 7 -9 2844.25 431.457 6 10 -7 -9 3450.69 224.157 5 10 -7 -9 3197.84 215.275 4 10 7 -9 3014.61 211.910 3 10 7 -8 1461.34 322.174 6 10 -7 -8 1333.26 147.419 5 10 -7 -8 1304.80 139.357 4 10 7 -7 4469.84 532.825 6 10 7 -6 2790.23 424.019 6 10 7 -5 81.5797 114.420 6 10 7 -4 543.347 206.508 6 10 7 -3 386.654 205.116 6 10 7 -2 719.171 221.083 6 10 7 -1 573.792 220.947 6 10 7 0 744.500 206.849 6 10 7 1 473.090 196.487 6 10 7 2 849.250 251.045 6 10 7 3 1143.84 271.907 6 10 -7 4 2298.44 181.654 4 10 7 4 2273.72 370.281 6 -10 -7 -5 1102.62 131.775 2 10 -7 5 1254.31 140.947 4 10 7 5 921.553 242.923 6 10 -7 6 183.597 67.3746 4 -10 -7 -6 40.1848 50.3199 2 10 7 6-35.7406 54.3543 3 10 7 6-172.645 164.160 6 10 -7 7 606.622 109.764 4 -10 -7 -7 584.855 104.782 2 10 7 7 704.933 109.217 3 10 7 7 514.013 213.987 6 -10 -7 -8 1532.44 160.832 2 10 -7 8 1468.93 156.195 4 10 7 8 1314.86 146.700 3 10 7 8 1142.62 283.486 6 -10 -7 -9 4390.05 266.191 2 10 -7 9 3808.18 453.972 1 10 -7 9 4298.03 256.285 4 10 7 9 4024.85 494.710 6 -10 -7 -10 183.711 73.4323 2 10 -7 10 197.727 72.7566 4 10 7 10 6.90160 89.6614 6 -10 -7 -11 8.67203 56.9494 2 10 -7 11 15.7852 53.8217 4 10 -7 11-25.1079 104.943 1 10 7 11 105.538 112.860 6 10 -7 12 6506.17 654.038 1 10 -7 12 7299.73 343.826 4 10 7 12 6841.67 658.896 6 -10 -7 -12 7811.01 369.753 2 -10 -7 -13 123.043 84.3909 2 10 -7 13 260.101 85.7879 4 10 7 13 16.0557 92.2998 6 -10 -7 -14 323.057 110.794 2 10 -7 14 154.900 80.9374 4 10 -7 14 204.040 168.061 1 10 -7 15 3159.19 236.215 4 10 -7 15 2718.07 465.585 1 -10 -7 -15 3123.67 250.221 2 -10 -7 -16 1190.45 168.532 2 10 7 16 1625.03 396.586 1 10 -7 16 1220.92 322.533 1 -10 -7 -17 190.523 98.5487 2 -10 -7 -18 1070.74 159.147 2 -10 -7 -19 5375.76 327.175 2 -10 -7 -20 49.8108 76.7331 2 -10 -7 -21 92.4006 86.2067 2 -10 -7 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85.0581 4 10 8 -8 154.245 54.6746 3 10 -8 -8 17.6890 61.0418 5 10 -8 -8 22.0476 46.8561 4 10 -8 -7 5277.60 279.941 5 10 -8 -7 5344.90 279.211 4 10 8 -7 5095.30 273.429 3 10 8 -7 5004.98 589.773 6 10 8 -6 806.927 114.628 3 10 -8 -6 1083.47 136.894 5 10 -8 -6 930.360 125.877 4 10 8 -6 1161.07 313.375 6 10 8 -5 2367.68 398.822 6 10 -8 -5 2683.80 200.071 5 10 -8 -5 2629.98 196.759 4 10 -8 -4 2013.07 175.972 5 10 8 -4 1827.01 344.008 6 10 -8 -4 2217.10 186.513 4 10 -8 -3 4480.25 257.723 5 10 -8 -3 4583.51 257.869 4 10 8 -3 4923.32 559.887 6 10 -8 -2 5229.66 273.133 4 10 -8 -2 5886.27 293.672 5 10 8 -2 6141.79 628.459 6 10 -8 -1 1158.75 137.739 5 10 -8 -1 1287.23 142.888 4 10 8 -1 1028.32 263.919 6 10 8 0 197.363 159.789 6 10 -8 0 339.632 81.3379 5 10 -8 0 401.905 91.8124 4 10 -8 1 119.060 59.5122 5 10 -8 1 103.911 51.4346 4 10 8 1 48.0183 121.517 6 10 -8 2 4126.01 245.128 5 10 -8 2 4088.49 246.091 4 10 8 2 4593.01 543.000 6 -10 -8 -3 1994.11 171.451 2 10 -8 3 1785.29 168.254 5 10 -8 3 2130.52 182.994 4 10 8 3 1680.37 314.728 6 10 -8 4 1795.36 167.154 4 -10 -8 -4 2048.24 172.980 2 10 -8 4 2025.83 172.853 5 10 8 4 1705.06 158.811 3 10 8 4 1703.75 336.232 6 -10 -8 -5 2021.23 176.739 2 10 -8 5 1896.03 169.190 5 10 -8 5 1913.07 171.621 4 10 8 5 1815.14 164.519 3 10 8 5 1860.07 347.263 6 10 -8 6 1091.24 135.727 4 10 -8 6 1191.00 137.253 5 -10 -8 -6 1086.60 128.892 2 10 8 6 1207.97 135.644 3 10 8 6 1007.29 265.298 6 -10 -8 -7 10639.4 406.444 2 10 -8 7 10775.4 402.466 4 10 8 7 9690.42 380.733 3 10 8 7 10879.5 852.722 6 -10 -8 -8 217.723 76.0322 2 10 -8 8 245.714 84.3771 4 10 8 8 240.288 78.5711 3 10 -8 9 3014.67 220.563 4 10 8 9 2974.52 450.354 6 -10 -8 -9 2920.17 222.391 2 -10 -8 -10 272.472 84.1455 2 10 -8 10 227.534 87.8444 4 10 8 10 306.226 172.798 6 10 -8 11 2344.36 203.601 4 -10 -8 -11 2326.30 207.266 2 10 8 11 1751.89 349.990 6 10 -8 12 6991.31 342.518 4 10 8 12 6918.95 689.175 6 -10 -8 -12 7249.27 362.942 2 -10 -8 -13 410.527 109.738 2 10 -8 13 351.891 95.7862 4 -10 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167.765 4 10 9 -23 1461.47 160.898 3 10 9 -22 220.131 84.9811 3 10 -9 -22 11.5738 67.7034 4 10 9 -21 260.285 88.2418 3 10 -9 -21 21.6230 66.1496 4 10 9 -20 366.185 98.5584 3 10 -9 -20 253.786 84.7724 4 10 9 -19 289.038 86.5339 3 10 -9 -19 236.002 79.5390 4 10 -9 -18 151.783 84.7883 4 10 9 -18-17.8656 64.8420 3 10 -9 -17 1009.27 126.753 5 10 9 -17 942.511 130.824 3 10 -9 -17 1028.58 137.873 4 10 9 -16 1207.14 349.858 6 10 -9 -16 1031.09 135.873 5 10 9 -16 1085.73 143.829 3 10 -9 -16 934.324 139.199 4 10 9 -15 364.643 243.684 6 10 -9 -15 109.887 74.2971 5 10 9 -15 136.033 71.2081 3 10 -9 -15 124.846 63.6296 4 10 -9 -14 4674.07 273.351 5 10 -9 -14 5027.81 290.766 4 10 9 -14 4689.12 277.490 3 10 9 -14 5226.66 658.130 6 10 -9 -13 95.4479 73.1238 5 10 9 -13 93.9614 70.9732 3 10 9 -13-16.3111 108.735 6 10 -9 -13 152.013 80.1367 4 10 9 -12 510.810 172.758 6 10 9 -12 613.828 103.796 3 10 -9 -12 464.035 108.020 5 10 -9 -12 455.823 92.5737 4 10 -9 -11 3628.86 241.899 5 10 9 -11 3321.58 511.954 6 10 -9 -11 3362.42 235.640 4 10 9 -11 3892.35 247.348 3 10 9 -10 283.881 189.073 6 10 9 -10 33.3971 49.1030 3 10 -9 -10 26.6398 61.0160 5 10 -9 -10 195.222 77.8450 4 10 9 -9 533.039 240.557 6 10 9 -9 453.817 87.9609 3 10 -9 -9 449.924 95.8872 4 10 -9 -9 535.346 111.933 5 10 9 -8 120.511 68.3164 3 10 -9 -8 130.142 72.6156 5 10 9 -8 14.7729 101.593 6 10 -9 -8 63.9104 63.4511 4 10 -9 -7 155.075 65.4853 5 10 -9 -7 64.0976 67.9389 4 10 9 -7-16.0957 159.553 6 10 9 -7 138.371 60.7315 3 10 -9 -6 4547.52 264.738 5 10 -9 -6 4390.35 263.182 4 10 9 -6 3924.23 238.978 3 10 9 -6 4913.89 602.080 6 10 -9 -5 1490.77 162.283 5 10 -9 -5 1319.94 144.132 4 10 9 -5 1339.39 134.512 3 10 -9 -4 2146.55 186.128 5 10 -9 -4 2133.64 185.172 4 10 9 -4 2087.93 169.637 3 10 9 -4 2204.51 396.006 6 10 -9 -3 50.3726 58.2714 5 10 -9 -3-12.1910 60.2701 4 10 9 -3-158.330 194.185 6 10 -9 -2 218.669 72.5196 5 10 -9 -2 211.093 76.1703 4 10 9 -2 97.3700 155.181 6 10 -9 -1 66.1294 60.6060 5 10 -9 -1 33.8371 60.7270 4 10 9 -1 71.0515 124.281 6 10 -9 0 4909.52 274.602 5 10 -9 0 5011.54 279.854 4 10 9 0 4844.67 584.237 6 10 -9 1 589.940 111.656 5 10 -9 1 686.511 116.942 4 10 9 1 878.110 272.783 6 10 -9 2 2352.33 196.527 4 10 -9 2 2336.01 194.231 5 10 9 2 2210.70 405.346 6 -10 -9 -3 1379.81 143.461 2 10 -9 3 1685.72 170.017 4 10 -9 3 1582.66 160.125 5 10 9 3 1672.19 357.564 6 -10 -9 -4 1551.72 153.671 2 10 -9 4 1558.52 167.564 4 10 9 4 1682.78 345.749 6 10 -9 4 1494.54 155.269 5 -10 -9 -5 10.3605 50.5721 2 10 -9 5 100.252 58.9678 4 10 9 5 185.618 186.816 6 10 -9 5-45.9903 61.3713 5 10 -9 6 2619.33 198.477 5 10 -9 6 2503.88 200.130 4 10 9 6 3065.06 468.076 6 -10 -9 -6 2419.22 194.486 2 10 -9 7 5873.96 305.482 4 10 9 7 5913.90 640.674 6 -10 -9 -7 5741.65 304.408 2 -10 -9 -8 803.295 127.337 2 10 -9 8 953.662 134.475 4 10 9 8 701.655 266.636 6 -10 -9 -9 58.2807 67.2655 2 10 -9 9-46.6418 77.3682 4 -10 -9 -10 1461.89 162.839 2 10 -9 10 1587.83 170.282 4 10 9 10 1373.21 330.230 6 10 -9 11 7495.82 356.251 4 10 9 11 7114.78 728.611 6 -10 -9 -11 7354.64 364.568 2 -10 -9 -12 134.041 76.9999 2 10 -9 12 131.223 88.3498 4 10 9 12-21.9339 105.773 6 -10 -9 -13 9.81554 67.0808 2 10 -9 13 153.766 93.7396 4 10 9 13 109.034 116.504 6 -10 -9 -14-33.1867 69.0933 2 10 -9 14 33.6433 69.0615 4 10 -9 15 6966.58 348.826 4 -10 -9 -15 6968.65 363.033 2 -10 -9 -16 3542.74 267.843 2 -10 -9 -17 1897.70 196.167 2 -10 -9 -18 873.181 148.822 2 -10 -9 -19 513.177 117.229 2 -10 -9 -20 103.842 92.2025 2 -10 -9 -21 2170.07 205.381 2 -10 -9 -22 138.032 89.4900 2 -10 -9 -23 18.0934 69.7971 2 -10 -9 -24 15.8642 60.2364 2 -10 -9 -25 91.9505 63.6472 2 -10 -9 -26 228.894 60.8070 2 -10 -9 -27 812.611 102.250 2 -10 -9 -28 193.241 54.7472 2 -10 -9 -29 16.0779 28.3174 2 10 -10 -30 599.655 66.9711 4 10 10 -30 638.725 72.0314 3 10 -10 -29 117.239 43.2185 4 10 10 -29 54.6241 41.8533 3 10 10 -28 207.352 60.6528 3 10 -10 -28 216.935 60.9567 4 10 10 -27 287.270 72.0743 3 10 -10 -27 213.420 68.1334 4 10 10 -26 383.239 75.7638 3 10 -10 -26 602.372 99.6399 4 10 10 -25 166.452 71.9456 3 10 -10 -25 108.126 60.9029 4 10 10 -24 319.293 82.1092 3 10 -10 -24 360.286 90.2473 4 10 10 -23 70.8537 64.6238 3 10 -10 -23 135.808 75.2183 4 10 10 -22 114.867 75.8513 3 10 -10 -22 72.8373 65.3179 4 10 10 -21-44.1064 61.2141 3 10 -10 -21-102.153 78.4055 4 10 10 -20 657.767 113.742 3 10 -10 -20 550.461 116.564 4 10 10 -19 278.710 83.0815 3 10 -10 -19 112.806 73.4948 4 10 -10 -18 41.4481 51.0277 5 10 10 -18 214.655 84.7545 3 10 -10 -18 88.7304 72.2800 4 10 -10 -17 32.1903 59.8282 5 10 10 -17-18.9281 58.8284 3 10 -10 -17 91.7741 82.9246 4 10 -10 -16 128.228 70.8040 5 10 10 -16 216.216 76.3482 3 10 -10 -16 19.9611 72.4205 4 10 -10 -15 2286.95 209.265 4 10 10 -15 2118.57 192.449 3 10 -10 -15 2042.71 181.131 5 10 10 -14 533.892 233.959 6 10 10 -14 299.824 86.4991 3 10 -10 -14 359.668 104.437 5 10 -10 -14 161.517 88.9793 4 10 10 -13 2852.08 485.820 6 10 -10 -13 3230.07 233.677 5 10 -10 -13 3043.95 234.703 4 10 10 -13 3039.31 221.329 3 10 10 -12 1504.90 359.430 6 10 -10 -12 1705.44 172.497 5 10 -10 -12 1688.82 185.429 4 10 10 -12 1670.34 164.410 3 10 10 -11 2942.99 487.616 6 10 -10 -11 2655.64 219.685 5 10 -10 -11 2763.68 220.193 4 10 10 -11 2659.40 207.864 3 10 -10 -10 641.843 119.553 5 10 10 -10 1227.98 336.552 6 10 10 -10 1034.71 126.523 3 10 -10 -10 1029.49 147.041 4 10 10 -9 2460.37 454.712 6 10 -10 -9 2408.98 205.508 4 10 -10 -9 2141.56 198.779 5 10 10 -9 2497.64 199.280 3 10 -10 -8 257.487 75.0135 5 10 -10 -8 306.953 92.3176 4 10 10 -8 332.542 165.509 6 10 -10 -7 54.1996 66.1350 5 10 10 -7-182.008 205.831 6 10 -10 -7-6.97382 60.7357 4 10 -10 -6 1511.36 164.507 5 10 -10 -6 1738.11 178.931 4 10 10 -6 1604.07 341.042 6 10 -10 -5 113.642 72.3757 5 10 -10 -5 72.6248 64.4292 4 10 10 -5 137.545 123.542 6 10 -10 -4 1610.86 174.077 5 10 -10 -4 1786.99 175.534 4 10 10 -4 1239.31 331.540 6 10 -10 -3 6779.56 334.386 4 10 -10 -3 6899.54 337.139 5 10 10 -3 7163.20 740.981 6 10 -10 -2 112.105 71.7920 5 10 -10 -2 33.8543 62.2518 4 10 10 -2 14.9476 148.957 6 10 -10 -1 340.190 89.8551 5 10 -10 -1 521.565 110.979 4 10 10 -1 514.526 233.169 6 10 -10 0 632.297 109.335 5 10 -10 0 942.931 135.900 4 10 10 0 668.704 250.526 6 10 -10 1 1263.62 149.224 4 10 -10 1 1286.98 154.015 5 10 10 1 1104.27 298.731 6 10 -10 2 2025.11 189.048 4 10 -10 2 1902.66 185.307 5 10 -10 3 105.107 66.7132 5 10 -10 3 197.236 85.7372 4 10 -10 4 70.8288 61.5375 5 10 -10 4 30.9868 62.5195 4 10 10 4 122.007 165.291 6 10 -10 5 1776.87 182.183 4 10 -10 5 1401.71 158.062 5 -10 -10 -5 1738.61 168.571 2 10 -10 6 2869.62 216.807 5 10 -10 6 3567.96 244.085 4 -10 -10 -6 3222.64 226.331 2 10 10 6 3437.45 520.334 6 10 -10 7 62.7333 64.1379 5 -10 -10 -7 93.9912 71.6688 2 10 -10 7 8.04009 81.9618 4 10 10 7 36.0312 159.223 6 -10 -10 -8 66.0012 54.0478 2 10 -10 8 43.7830 63.9284 4 -10 -10 -9 263.653 61.2027 2 10 -10 9 89.2827 71.0193 4 10 10 9-33.2945 112.197 6 -10 -10 -10 510.031 110.364 2 10 -10 10 515.466 105.154 4 10 10 10 267.028 177.794 6 -10 -10 -11 728.409 130.300 2 10 -10 11 525.526 113.954 4 10 10 11 973.292 298.697 6 10 -10 12 3289.25 244.863 4 -10 -10 -12 3348.58 250.036 2 -10 -10 -13 1101.39 155.189 2 10 -10 13 1215.11 155.076 4 10 -10 14 1808.38 183.801 4 -10 -10 -14 1782.79 186.720 2 -10 -10 -15 187.345 90.4881 2 -10 -10 -16 4129.12 280.043 2 -10 -10 -17 22.2166 70.4655 2 -10 -10 -18 6020.03 335.070 2 -10 -10 -19 102.197 75.3839 2 -10 -10 -20-0.74754 69.4227 2 -10 -10 -21 2330.74 203.637 2 -10 -10 -22 171.056 76.3557 2 -10 -10 -23 566.855 111.749 2 -10 -10 -24-5.76200 60.2409 2 -10 -10 -25 288.556 71.8604 2 -10 -10 -26 8.74007 43.0438 2 -10 -10 -27 47.6841 36.6690 2 -10 -10 -28 192.697 41.6087 2 10 -11 -29 412.336 57.5097 4 10 11 -28 324.634 49.8746 3 10 -11 -28 441.078 69.1871 4 10 11 -27 32.2965 35.7717 3 10 -11 -27 81.9604 45.6684 4 10 11 -26 152.958 52.8853 3 10 -11 -26 337.183 77.1288 4 10 11 -25 522.838 86.5449 3 10 -11 -25 537.545 96.4094 4 10 -11 -24 216.151 73.3703 4 10 11 -24 184.385 59.9995 3 10 11 -23 83.4706 55.7386 3 10 -11 -23 107.242 69.7585 4 10 11 -22-23.2671 53.9982 3 10 -11 -22 158.646 80.0674 4 10 11 -21 65.3322 64.0561 3 10 -11 -21 11.3336 66.3029 4 10 11 -20 101.516 55.8291 3 10 -11 -20 9.27245 68.4810 4 10 11 -19 103.261 81.2500 3 10 -11 -19-2.93924 66.8228 4 10 -11 -18 421.623 92.7190 5 10 -11 -18 466.849 115.856 4 10 11 -18 432.965 94.8718 3 10 -11 -17 79.6770 65.4473 5 10 11 -17 9.47990 60.7545 3 10 -11 -17 58.9196 83.7267 4 10 -11 -16 144.771 78.3274 5 10 -11 -16 113.417 82.5578 4 10 11 -16 133.057 67.9945 3 10 11 -15 111.537 64.7667 3 10 -11 -15 29.7087 62.4281 5 10 -11 -15-39.8141 86.7073 4 10 -11 -14 1757.38 181.347 5 10 -11 -14 1846.01 193.566 4 10 -11 -13 133.736 84.5359 5 10 -11 -13 200.560 87.4327 4 10 -11 -12 808.392 131.370 5 10 -11 -12 976.471 151.025 4 10 11 -11 233.531 189.390 6 10 -11 -11 167.753 91.5156 4 10 -11 -11 267.603 87.4788 5 10 -11 -10 1177.71 158.837 5 10 -11 -10 1045.90 152.038 4 10 11 -9 655.298 275.181 6 10 -11 -9 534.565 109.792 4 10 -11 -9 714.879 130.646 5 10 -11 -8 742.428 134.338 5 10 -11 -8 875.750 138.380 4 10 -11 -7 2795.92 225.421 5 10 -11 -7 2669.80 222.981 4 10 11 -7 2180.84 417.236 6 10 -11 -6 209.099 87.9555 5 10 -11 -6 98.7644 80.8305 4 10 11 -6-3.66329 130.871 6 10 -11 -5 59.0151 72.7883 5 10 -11 -5 250.728 97.7281 4 10 -11 -4-58.3858 79.7824 4 10 -11 -4 36.5409 69.7630 5 10 -11 -3 48.6822 72.8065 5 10 11 -3 59.4269 167.750 6 10 -11 -3-74.1189 74.0974 4 10 -11 -2 3910.68 264.930 5 10 11 -2 3580.26 545.131 6 10 -11 -2 3980.93 263.724 4 10 -11 -1 4120.60 269.838 5 10 -11 -1 3978.46 264.853 4 10 11 -1 4507.21 602.450 6 10 -11 0 1405.58 171.597 5 10 -11 0 1530.11 172.872 4 10 11 0 1892.16 424.485 6 10 -11 1 807.819 136.311 5 10 -11 1 1045.40 147.625 4 10 -11 2 514.137 109.956 4 10 -11 2 443.478 106.252 5 10 11 2 335.974 168.424 6 10 -11 3 377.154 95.1075 5 10 -11 3 284.194 91.7290 4 10 11 3 89.6960 205.658 6 10 -11 4 477.347 108.754 5 10 -11 4 706.174 127.672 4 10 11 4 534.795 238.822 6 10 -11 5 1111.15 148.969 4 10 -11 5 1075.29 142.212 5 10 11 5 1137.03 331.054 6 10 -11 6 2196.26 199.176 4 10 -11 6 1953.97 183.927 5 10 -11 7 779.162 122.188 5 -10 -11 -7 842.392 121.925 2 10 -11 7 779.528 130.026 4 10 11 7 831.115 310.554 6 -10 -11 -8 143.101 64.6233 2 10 -11 8 42.9469 74.8526 4 10 11 8 208.459 161.795 6 -10 -11 -9 318.045 84.5712 2 10 -11 9 316.292 93.0363 4 -10 -11 -10 253.105 87.5998 2 10 -11 10 117.450 78.7160 4 -10 -11 -11 418.912 100.462 2 10 -11 11 393.607 96.5303 4 10 -11 12 3777.13 257.513 4 -10 -11 -12 3674.24 255.010 2 10 -11 13 1234.22 157.575 4 -10 -11 -13 1337.79 164.986 2 10 -11 14 741.533 127.554 4 -10 -11 -14 842.889 137.106 2 -10 -11 -15 41.0445 66.5842 2 -10 -11 -16 81.5848 69.5151 2 -10 -11 -17 92.1191 72.6075 2 -10 -11 -18 168.260 80.2608 2 -10 -11 -18-13.6748 45.7584 5 -10 -11 -19 1070.48 142.927 2 -10 -11 -20 349.562 96.2008 2 -10 -11 -21-84.0941 75.6155 2 -10 -11 -22 147.856 69.6163 2 -10 -11 -23-13.0228 52.3996 2 -10 -11 -24 443.138 83.1183 2 -10 -11 -25 124.347 51.2906 2 -10 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218.881 4 10 -12 -6 576.654 120.211 5 10 -12 -6 514.574 113.398 4 10 12 -6 269.632 190.875 6 10 -12 -5 8265.62 390.447 5 10 -12 -5 7736.70 376.502 4 10 12 -5 8486.04 856.981 6 10 -12 -4 629.756 137.049 5 10 -12 -4 620.869 125.162 4 10 12 -4 612.918 311.642 6 10 -12 -3 143.120 84.6817 5 10 -12 -3 207.149 102.623 4 10 -12 -2 207.040 92.3677 5 10 -12 -2 191.248 84.2127 4 10 12 -2 240.188 229.471 6 10 -12 -1 99.2388 73.7131 4 10 -12 -1 115.738 80.9413 5 10 12 -1 236.156 208.501 6 10 -12 0 311.334 97.8932 5 10 -12 0 348.344 99.4143 4 10 12 0 447.774 191.441 6 10 -12 1 95.7763 81.4555 4 10 -12 1 46.5809 73.8606 5 10 12 1-70.1314 216.112 6 10 -12 2 123.939 86.7616 5 10 -12 2 48.6247 62.7293 4 10 -12 3 1772.36 181.633 5 10 -12 3 1833.85 188.493 4 10 12 3 2074.02 419.096 6 10 -12 4 5155.38 297.374 5 10 -12 4 5118.15 298.959 4 10 -12 5 2592.06 213.620 5 10 -12 5 2843.01 224.505 4 10 -12 6 1345.61 157.124 5 10 -12 6 1368.39 162.629 4 10 -12 7 560.336 112.641 4 10 -12 7 601.088 103.263 5 10 -12 8-53.0299 65.6589 4 10 -12 9 805.512 135.787 4 10 -12 10 129.909 71.7994 4 -10 -12 -10 81.2202 64.2461 2 10 -12 11 3715.45 251.092 4 -10 -12 -11 3850.62 250.566 2 -10 -12 -12 374.335 94.7113 2 10 -12 12 533.542 108.799 4 10 -12 13 66.1649 69.5775 4 -10 -12 -13 363.165 93.2964 2 -10 -12 -14 758.611 127.144 2 10 -12 14 757.115 121.981 4 -10 -12 -15-74.8389 76.4939 2 -10 -12 -16 27.6454 59.0278 2 -10 -12 -16 8.24178 59.3068 5 -10 -12 -17-33.7939 56.0815 5 -10 -12 -17 101.951 68.5414 2 -10 -12 -18 171.965 60.3795 5 -10 -12 -18 134.554 67.0035 2 -10 -12 -19 52.5129 54.2779 2 -10 -12 -20 412.237 87.9153 2 -10 -12 -21 722.766 100.656 2 -10 -12 -22 208.863 61.7926 2 -10 -12 -23-4.17568 39.2914 2 -10 -12 -24 95.1547 40.0236 2 -10 -12 -25 216.633 45.6072 2 10 -13 -27 112.634 39.2249 4 10 -13 -26 125.423 46.8277 4 10 -13 -25 810.365 91.5374 4 10 -13 -24-27.2683 52.3836 4 10 -13 -23 119.755 57.6324 4 10 -13 -22 425.128 87.9939 4 10 -13 -21 1322.22 141.395 4 10 -13 -20 8.02370 68.2935 4 10 -13 -19 30.4073 46.6662 5 10 -13 -19 25.6477 70.1319 4 10 -13 -18 551.612 116.386 4 10 -13 -18 528.389 98.6116 5 10 -13 -17 799.227 115.312 5 10 -13 -17 937.087 138.098 4 10 -13 -16 283.600 101.350 4 10 -13 -16 269.557 78.9395 5 10 -13 -15 161.451 80.2380 5 10 -13 -15 8.15847 72.4268 4 10 -13 -14 116.935 77.9388 5 10 -13 -14 143.284 78.9276 4 10 -13 -13 50.4687 72.3509 5 10 -13 -13 178.606 91.8610 4 10 -13 -12 188.698 80.2781 5 10 -13 -12 272.602 102.360 4 10 -13 -11 1587.33 178.011 5 10 -13 -11 1558.01 175.132 4 10 -13 -10-43.9600 82.0667 5 10 -13 -10-73.5321 82.0239 4 10 -13 -9 1.58926 86.6024 5 10 -13 -9 111.269 78.5020 4 10 -13 -8 421.305 110.573 5 10 -13 -8 428.853 115.240 4 10 -13 -7 3206.31 249.252 4 10 -13 -7 3145.21 245.240 5 10 -13 -6 868.632 151.944 5 10 -13 -6 952.470 143.106 4 10 -13 -5 692.574 136.702 5 10 -13 -5 538.737 123.513 4 10 -13 -4 1367.61 178.811 5 10 -13 -4 1267.78 168.739 4 10 -13 -3 4555.59 296.712 5 10 -13 -3 4256.39 283.072 4 10 -13 -2 2359.31 221.641 5 10 -13 -2 1991.14 201.939 4 10 -13 -1 6305.67 342.454 5 10 -13 -1 6524.31 343.539 4 10 -13 0 865.875 144.640 5 10 -13 0 884.716 141.790 4 10 -13 1 152.479 82.4243 5 10 -13 1 205.580 81.3036 4 10 -13 2 81.6356 86.9128 5 10 -13 2-22.1400 68.0033 4 10 -13 3 388.979 103.875 5 10 -13 3 215.835 88.6497 4 10 -13 4 609.085 120.656 5 10 -13 4 794.238 127.663 4 10 -13 5 5386.56 303.543 4 10 -13 5 5621.51 304.750 5 10 -13 6 105.017 72.5860 5 10 -13 6 137.875 84.1227 4 10 -13 7 30.8049 67.8091 4 10 -13 8 1485.47 166.040 4 10 -13 9 1308.87 154.955 4 10 -13 10 595.096 115.795 4 10 -13 11 6.37931 63.5425 4 10 -13 12-58.3117 69.8525 4 10 -13 13 1.87945 54.8548 4 -10 -13 -14 614.734 111.006 5 -10 -13 -14 639.489 103.336 2 -10 -13 -15 324.818 80.1121 5 -10 -13 -15 433.094 81.3923 2 -10 -13 -16 869.036 112.344 5 -10 -13 -16 789.203 109.524 2 -10 -13 -17 142.964 60.1095 5 -10 -13 -17 64.2266 51.7986 2 -10 -13 -18 1115.21 108.588 5 -10 -13 -18 991.771 114.177 2 -10 -13 -19 1020.48 113.112 2 -10 -13 -20 71.8500 47.9609 2 -10 -13 -21 70.2258 39.5494 2 -10 -13 -22 243.232 55.3377 2 10 -14 -26-1.48655 28.3091 4 10 -14 -25 38.5754 38.9531 4 10 -14 -24-3.36589 39.6747 4 10 -14 -23 59.3030 48.2899 4 10 -14 -22 126.284 61.4610 4 10 -14 -21-53.0667 57.6062 4 10 -14 -20 412.109 88.7408 4 10 -14 -19 636.608 109.016 4 10 -14 -18 95.0919 59.4153 5 10 -14 -18 218.242 85.0243 4 10 -14 -17 370.441 99.1394 4 10 -14 -17 299.870 83.5940 5 10 -14 -16 1837.34 167.719 5 10 -14 -16 2102.85 188.470 4 10 -14 -15 1103.50 142.431 4 10 -14 -15 1205.28 146.974 5 10 -14 -14 622.363 117.757 5 10 -14 -14 519.866 107.537 4 10 -14 -13-60.4013 75.6192 5 10 -14 -13-89.7503 91.6376 4 10 -14 -12 142.647 86.3868 5 10 -14 -12-35.7961 79.2860 4 10 -14 -11 14.1036 74.6609 5 10 -14 -11-51.7540 85.8216 4 10 -14 -10 562.569 120.575 5 10 -14 -10 400.931 113.206 4 10 -14 -9 141.729 90.9364 5 10 -14 -9 213.565 99.1402 4 10 -14 -8 202.334 92.7104 5 10 -14 -8 152.170 79.8892 4 10 -14 -7 525.864 121.706 5 -10 -14 7 704.957 109.418 5 10 -14 -7 558.598 122.172 4 10 -14 -6 1397.23 182.645 5 10 -14 -6 1478.29 176.644 4 10 -14 -5 1106.83 163.477 5 10 -14 -5 1174.58 161.486 4 10 -14 -4 616.928 140.786 5 10 -14 -4 453.166 112.014 4 10 -14 -3 1571.87 184.392 5 10 -14 -3 1607.04 182.472 4 10 -14 -2 2692.13 231.826 5 10 -14 -2 2588.05 224.650 4 10 -14 -1 152.889 93.2376 5 10 -14 -1 154.183 83.0659 4 10 -14 0 1710.73 182.478 5 10 -14 0 2116.58 196.550 4 10 -14 1 31.8664 72.7765 5 10 -14 1 43.9312 76.0869 4 10 -14 2 600.907 118.971 5 10 -14 2 611.967 114.759 4 10 -14 3 150.379 86.6910 5 10 -14 3 215.222 86.7684 4 10 -14 4 85.9340 70.9401 5 10 -14 4 15.3771 70.7082 4 10 -14 5 105.231 68.8544 4 10 -14 5 198.142 76.4960 5 10 -14 6 375.662 87.9210 5 10 -14 6 606.732 109.852 4 10 -14 7 675.976 117.341 4 10 -14 8 579.131 110.594 4 10 -14 9 122.971 65.8230 4 10 -14 10 330.812 83.7987 4 -10 -14 -11 2006.83 179.916 5 10 -14 11 1940.33 166.704 4 -10 -14 -12 597.394 107.203 5 10 -14 12 734.675 107.360 4 -10 -14 -13-17.3697 61.0495 5 -10 -14 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49.2152 3 11 -5 -11 18.4451 54.7606 4 11 -5 -11 42.1374 54.1175 5 11 5 -10 6692.24 312.628 3 11 5 -10 6902.90 655.538 6 11 5 -9 64.5573 127.543 6 11 5 -8 1366.50 283.691 6 11 5 -7 4584.07 516.275 6 11 5 -6 3849.54 468.896 6 11 5 -5 564.196 191.294 6 11 5 -4-58.5027 118.959 6 11 5 -3 233.446 157.402 6 11 5 -2 1042.17 245.275 6 11 5 -1 4463.38 482.376 6 11 5 0 10748.3 736.226 6 11 5 1 956.855 225.724 6 11 5 2 333.619 167.065 6 11 5 3 1861.84 312.032 6 11 5 4 709.545 210.114 6 11 5 5 199.763 146.447 6 11 -5 6 1109.68 127.227 4 11 5 6 1151.21 137.959 3 11 5 6 1249.14 269.431 6 11 -5 7 77.3631 71.1522 4 -11 -5 -7 104.725 63.4307 2 11 5 7-64.2972 53.1010 3 11 5 7 80.1096 117.076 6 -11 -5 -8 2952.44 218.606 2 11 -5 8 2654.13 199.250 4 11 5 8 2672.63 207.958 3 11 5 8 3192.36 403.985 6 11 -5 9 754.979 117.724 4 -11 -5 -9 801.994 120.435 2 11 5 9 753.705 111.937 3 11 5 9 646.239 221.037 6 -11 -5 -10 2179.33 195.924 2 11 -5 10 2336.26 194.404 4 11 -5 10 2098.17 358.235 1 -11 -5 -11 1588.93 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419.779 120.455 2 -11 -6 -19 31.8539 87.3180 2 -11 -6 -20 1463.66 183.282 2 -11 -6 -21 208.513 83.2646 2 -11 -6 -22-65.7008 88.8716 2 -11 -6 -23 2450.82 213.188 2 -11 -6 -24 141.698 83.4100 2 -11 -6 -25 179.047 88.6258 2 -11 -6 -26 393.210 94.9899 2 -11 -6 -27 273.144 78.2166 2 -11 -6 -28 445.204 81.7176 2 -11 -6 -29 317.647 62.6782 2 -11 -6 -30 132.874 40.3523 2 11 7 -33 128.156 41.9028 3 11 7 -32-24.1666 37.1033 3 11 7 -31 221.375 62.4987 3 11 7 -30 99.8957 59.3434 3 11 7 -29 114.901 66.9676 3 11 7 -28 62.5682 64.1386 3 11 -7 -28 98.0809 54.3822 4 11 7 -27 32.4782 70.2169 3 11 -7 -27-59.0252 52.9645 4 11 7 -26 137.575 83.3610 3 11 -7 -26 60.4899 51.0776 4 11 7 -25-86.6518 70.5338 3 11 -7 -25 4.09559 55.6687 4 11 7 -24 13.3834 72.8471 3 11 -7 -24-37.7178 52.8302 4 11 7 -23 267.571 94.9954 3 11 -7 -23 248.212 73.5563 4 11 7 -22 211.939 91.9267 3 11 -7 -22 243.268 77.9281 4 11 7 -21 106.345 79.5678 3 11 -7 -21 100.358 68.4966 4 11 7 -20 887.820 143.876 3 11 -7 -20 817.120 121.156 4 11 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2933.20 210.390 5 11 -7 1 2848.53 204.894 4 11 7 1 2625.36 198.639 3 11 7 1 2661.44 407.778 6 11 -7 2 217.644 76.5547 4 11 -7 2 149.516 69.8176 5 11 7 2 42.1422 50.4167 3 11 7 2 107.989 133.441 6 11 -7 3 3192.04 217.230 4 11 7 3 2656.32 202.221 3 11 7 3 2798.05 424.452 6 11 -7 4 993.591 125.547 4 11 7 4 823.304 114.196 3 11 7 4 824.720 247.841 6 11 -7 5 35.7499 49.2460 4 -11 -7 -5 275.150 77.1361 2 11 7 5 97.0805 63.6640 3 11 7 5 43.2638 123.634 6 11 -7 6 397.466 101.069 4 -11 -7 -6 457.725 99.8358 2 11 7 6 264.016 78.0894 3 11 7 6 304.312 169.308 6 -11 -7 -7 1206.18 149.619 2 11 -7 7 1378.08 153.340 4 11 7 7 1289.58 151.962 3 11 7 7 1167.41 286.162 6 11 -7 8 135.442 72.8200 4 -11 -7 -8 304.121 88.1393 2 11 7 8 201.377 81.7819 3 11 7 8 341.839 183.950 6 11 -7 9 1194.34 145.137 4 -11 -7 -9 1105.70 143.442 2 11 7 9 1265.21 288.179 6 11 -7 10 3539.82 245.435 4 11 7 10 3473.56 476.731 6 -11 -7 -10 3105.71 239.271 2 -11 -7 -11 796.257 133.044 2 11 -7 11 864.244 135.226 4 -11 -7 -12-44.2770 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85.9601 53.7311 3 11 -9 -28 153.355 54.1653 4 11 -9 -27 189.855 62.4940 4 11 9 -27 24.8755 50.3592 3 11 9 -26 77.7221 71.5115 3 11 -9 -26 47.2704 51.6884 4 11 9 -25 706.362 113.668 3 11 -9 -25 655.768 99.4670 4 11 9 -24 138.225 68.4721 3 11 -9 -24 183.020 75.5878 4 11 9 -23 555.556 107.103 3 11 -9 -23 297.859 84.7051 4 11 9 -22 116.596 72.1587 3 11 -9 -22 359.659 94.7333 4 11 9 -21-9.58331 61.3322 3 11 -9 -21-14.5511 68.1902 4 11 9 -20-13.5365 64.1939 3 11 -9 -20-21.0237 65.7512 4 11 9 -19 299.873 80.2191 3 11 -9 -19 436.829 104.781 4 11 9 -18-140.496 85.1788 3 11 -9 -18 40.6178 64.0902 4 11 -9 -17 461.306 84.7849 5 11 9 -17 198.247 78.8589 3 11 -9 -17 466.290 108.060 4 11 9 -16 213.403 75.0728 3 11 -9 -16 68.4883 66.6295 4 11 -9 -16 337.589 93.6751 5 11 -9 -15 217.635 79.1363 5 11 9 -15 145.165 69.1635 3 11 -9 -15 252.718 87.9628 4 11 9 -14 25.1969 137.500 6 11 -9 -14 119.735 77.1196 5 11 9 -14 63.2870 58.4269 3 11 -9 -14 122.252 68.9827 4 11 -9 -13 16.2160 58.5078 5 11 9 -13-25.7212 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186.053 6 11 10 -5 410.398 81.8303 3 11 -10 -4 440.579 103.626 5 11 -10 -4 408.083 101.148 4 11 10 -4 189.985 214.845 6 11 -10 -3 1637.79 179.666 5 11 -10 -3 1808.49 186.327 4 11 10 -3 2084.90 422.962 6 11 -10 -2 1507.86 169.130 4 11 -10 -2 1459.40 169.285 5 11 10 -2 1617.21 374.024 6 11 -10 -1 5673.48 314.428 5 11 -10 -1 5579.44 309.094 4 11 10 -1 5847.03 675.766 6 11 -10 0 200.173 92.4847 5 11 -10 0 106.063 68.5990 4 11 10 0 403.004 233.856 6 11 -10 1 84.3532 69.0421 5 11 -10 1 82.4445 83.6517 4 11 -10 2 690.917 127.384 5 11 -10 2 792.331 128.388 4 11 -10 3 239.217 79.2335 5 11 -10 3 316.804 95.4965 4 11 10 3 285.123 170.527 6 11 -10 4 225.798 79.8928 5 -11 -10 -4 332.882 89.3650 2 11 -10 4 417.261 95.3217 4 11 10 4 411.657 164.375 6 11 -10 5 1029.95 137.239 4 -11 -10 -5 1198.10 146.221 2 -11 -10 -6 51.0924 66.3649 2 11 -10 6-5.67787 60.6246 4 11 10 6 54.4891 122.318 6 11 -10 7 2345.67 207.745 4 -11 -10 -7 2492.06 208.951 2 11 10 7 2044.88 407.448 6 -11 -10 -8 69.9921 72.0158 2 11 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131.560 1 12 2 9 140.696 78.6145 3 12 -2 9-77.8656 103.132 1 12 -2 10 613.013 108.064 4 12 2 10 448.870 145.462 1 -12 -2 -10 677.337 109.386 2 -12 2 -10 746.563 114.757 2 12 -2 10 297.625 183.517 1 -12 -2 -11 2195.48 197.468 2 -12 2 -11 2174.98 181.930 2 12 2 11 1817.45 341.084 1 12 -2 11 2517.78 376.908 1 -12 -2 -12 2315.55 203.538 2 12 2 12 1902.86 363.577 1 12 -2 12 2016.11 343.636 1 -12 2 -12 2313.82 188.659 2 -12 -2 -13 1862.69 187.281 2 12 -2 13 1071.40 272.401 1 12 2 13 1634.76 346.174 1 -12 2 -13 1624.22 161.134 2 -12 2 -14 102.715 61.0981 2 -12 -2 -14 34.9504 68.4555 2 12 2 14 93.6081 127.110 1 12 2 15 6461.86 700.577 1 12 -2 15 5614.92 635.526 1 -12 2 -15 5539.35 297.639 2 -12 -2 -15 6073.04 333.458 2 -12 2 -16 945.664 131.170 2 -12 -2 -16 1052.55 147.808 2 12 -2 16 843.335 249.456 1 12 2 16 1230.40 320.104 1 -12 2 -17 166.205 72.8685 2 -12 -2 -17 103.502 80.1128 2 -12 -2 -18 1440.51 177.457 2 -12 -2 -19 907.870 143.180 2 -12 -2 -20 399.487 109.198 2 -12 -2 -21 180.878 91.0747 2 -12 -2 -22 665.418 123.596 2 -12 -2 -23 1670.44 174.063 2 -12 -2 -24 397.177 102.220 2 -12 -2 -25 1489.35 154.903 2 -12 -2 -26 130.147 52.3694 2 -12 -2 -27 307.154 73.3791 2 -12 -2 -28 52.2882 40.4945 2 12 3 -34 93.3847 41.0596 3 12 3 -33 140.865 52.3694 3 12 3 -32 71.8411 56.2793 3 12 3 -31 1210.92 130.892 3 12 3 -30-71.8972 67.5089 3 12 3 -29 102.511 74.2181 3 12 -3 -28 236.920 63.7961 3 12 3 -28 276.401 91.6334 3 12 -3 -27 58.1785 50.1209 3 12 3 -27-16.4429 74.5117 3 12 -3 -26 43.8607 53.5381 3 12 3 -26 93.5937 75.2634 3 12 -3 -25 120.771 68.6360 3 12 3 -25 56.0809 78.3759 3 12 -3 -24 367.792 88.8979 3 12 3 -24 315.354 106.100 3 12 -3 -23 1009.43 132.581 3 12 3 -23 1216.92 166.213 3 12 -3 -22 298.747 80.3112 3 12 3 -22 241.815 93.5001 3 12 3 -21 1246.77 161.393 3 12 -3 -21 1437.92 157.346 3 12 3 -20 1213.69 330.284 6 12 3 -20 1517.61 177.512 3 12 -3 -20 1586.57 159.409 3 12 3 -19-65.0291 158.769 6 12 -3 -19 57.2306 64.8313 3 12 3 -19 90.8642 85.8059 3 12 3 -18 9.04867 110.093 6 12 3 -18 103.180 72.3800 3 12 3 -17 929.353 292.097 6 12 -3 -17 962.804 128.604 3 12 3 -17 1100.46 148.211 3 12 3 -16 376.235 229.835 6 12 -3 -16 651.586 110.230 3 12 3 -16 459.684 104.884 3 12 3 -15 1730.30 372.774 6 12 -3 -15 1367.09 141.849 3 12 3 -15 1560.82 172.336 3 12 3 -14-63.7621 114.694 6 12 -3 -14-15.0867 53.2827 3 12 3 -14 65.6716 72.2899 3 12 3 -13 342.505 208.665 6 12 3 -13 188.349 74.9981 3 12 3 -12 3374.79 471.349 6 12 3 -12 4065.75 254.290 3 12 3 -11 1567.48 316.740 6 12 3 -11 1941.22 179.075 3 12 3 -10 581.780 175.663 6 12 3 -10 625.454 103.964 3 12 3 -9 4626.66 260.742 3 12 3 -9 3829.37 475.115 6 12 3 -8 296.169 180.356 6 12 3 -7 281.073 174.496 6 12 3 -6 117.189 103.691 6 12 3 -5 7680.43 624.073 6 12 3 -4 2246.40 340.546 6 12 3 -3 727.965 205.011 6 12 3 -2 165.338 140.661 6 12 3 -1 97.6583 103.677 6 12 3 0 5.84042 78.0166 6 12 3 1 178.664 100.577 6 12 3 2 181.707 102.167 6 12 3 3 181.991 95.0476 6 12 3 5 4501.42 263.943 3 12 -3 6 1089.68 124.570 4 12 3 6 1104.35 136.007 3 12 -3 7 1715.71 160.304 4 12 3 7 1832.80 179.896 3 12 -3 8 12.7325 58.5134 4 12 3 8 117.641 150.660 1 12 3 8 101.874 72.6111 3 12 -3 9 1353.43 144.385 4 -12 -3 -9 1323.80 147.409 2 12 3 9 1268.01 151.085 3 12 3 9 1475.43 307.068 1 12 -3 10 242.791 83.4842 4 12 3 10 8.31508 128.595 1 -12 -3 -10 219.699 77.7408 2 -12 3 -10 229.190 73.6199 2 12 3 11 1322.60 284.125 1 12 -3 11 1563.14 164.279 4 12 -3 11 2036.03 362.133 1 -12 -3 -11 1763.55 183.800 2 12 -3 12-5.59101 133.246 1 -12 -3 -12 93.9258 67.4560 2 12 3 12-127.687 130.193 1 12 -3 13 2412.97 417.864 1 12 3 13 1799.87 367.756 1 -12 -3 -13 1977.74 192.527 2 12 3 14 404.439 159.669 1 -12 -3 -14 833.120 140.072 2 12 3 15 547.406 252.840 1 -12 -3 -15 481.342 112.806 2 12 -3 16 1723.18 370.181 1 12 3 16 1502.62 346.524 1 -12 -3 -16 1832.91 197.015 2 -12 -3 -17 179.860 81.5931 2 -12 -3 -18 780.550 147.241 2 -12 -3 -19 32.4704 79.2827 2 -12 -3 -20 333.496 100.096 2 -12 -3 -21 2115.88 202.403 2 -12 -3 -22 75.7632 67.2830 2 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1512.48 337.783 6 12 4 -12 1088.22 135.952 3 12 4 -11 262.238 134.875 6 12 4 -11 456.927 96.9478 3 12 4 -10 6149.98 309.154 3 12 4 -10 5914.42 620.968 6 12 4 -9 422.221 206.308 6 12 4 -9 447.186 98.1521 3 12 4 -8 7.91522 127.504 6 12 4 -8-37.9622 57.9822 3 12 4 -7 408.944 86.9278 3 12 4 -7 373.289 161.240 6 12 4 -6 599.575 223.490 6 12 4 -5-85.3523 157.830 6 12 4 -4 1188.14 262.194 6 12 4 -3 1855.27 316.890 6 12 4 -2 2085.63 320.797 6 12 4 -1 2325.02 341.809 6 12 4 0 10048.5 701.400 6 12 4 1 69.4010 89.2286 6 12 4 2 5498.13 513.077 6 12 4 3 243.150 70.5159 3 12 4 3 159.617 109.233 6 12 -4 4 247.288 64.8442 4 12 4 4 21.9002 86.0356 6 12 4 4 152.544 64.0674 3 12 -4 5 6373.25 293.564 4 12 4 5 5455.61 497.359 6 12 4 5 5919.28 303.215 3 12 -4 6 2619.89 192.533 4 12 4 6 2896.15 218.793 3 12 -4 7 11.5535 42.5073 4 12 4 7 70.7807 64.7321 3 12 -4 8 2366.12 190.616 4 -12 -4 -8 2172.00 194.024 2 12 4 8 2279.48 197.914 3 -12 -4 -9 1449.09 162.393 2 12 -4 9 1254.46 144.776 4 12 4 9 1082.14 140.524 3 12 -4 10 102.703 72.3323 4 -12 -4 -10 74.2868 67.2893 2 -12 -4 -11 2392.06 210.478 2 12 4 11 2461.92 408.327 1 12 -4 11 2115.17 189.898 4 12 -4 12 257.972 84.9107 4 -12 -4 -12 225.102 84.8130 2 12 4 12 112.450 127.658 1 12 4 13 114.705 142.491 1 -12 -4 -13 193.983 94.0923 2 12 4 14 2276.63 422.286 1 -12 -4 -14 2380.94 221.578 2 -12 -4 -15 156.211 89.2318 2 12 4 15 77.8008 175.612 1 -12 -4 -16 4458.66 299.438 2 -12 -4 -17 825.720 143.176 2 -12 -4 -18 244.085 97.3545 2 -12 -4 -19 1077.14 159.525 2 -12 -4 -20 3988.54 281.546 2 -12 -4 -21 1851.63 196.101 2 -12 -4 -22-11.9807 79.2590 2 -12 -4 -23 1036.28 143.984 2 -12 -4 -24 117.784 75.5906 2 -12 -4 -25 947.451 132.704 2 -12 -4 -26 61.5054 58.8200 2 -12 -4 -27 2.75572 46.7951 2 -12 -4 -28 561.184 83.5650 2 -12 -4 -29 24.4163 32.0345 2 12 5 -34 65.2224 29.3051 3 12 5 -33 2.86222 35.5815 3 12 5 -32 88.4629 47.5608 3 12 5 -31 25.4148 51.8912 3 12 5 -30 52.9119 58.2559 3 12 5 -29 187.857 79.1184 3 12 5 -28 1076.85 145.902 3 12 5 -27 160.498 79.7276 3 12 5 -26 8.85804 79.0035 3 12 5 -25 13.8506 83.4567 3 12 5 -24 1290.81 168.703 3 12 5 -23-43.8032 85.8162 3 12 5 -22 150.827 95.0019 3 12 5 -21 868.759 146.099 3 12 5 -20 214.855 95.7617 3 12 -5 -20 224.259 79.0084 4 12 5 -19 1288.14 331.245 6 12 -5 -19 1448.34 146.122 4 12 5 -19 1529.49 182.781 3 12 5 -18 7.55674 121.741 6 12 5 -18 213.678 93.6373 3 12 -5 -18-21.4994 54.4507 4 12 5 -17 875.179 298.259 6 12 5 -17 766.711 137.689 3 12 -5 -17 776.099 111.563 4 12 5 -16 91.3499 140.532 6 12 5 -16 69.4289 70.9450 3 12 -5 -16 83.6710 63.9830 4 12 5 -15-29.8443 67.4141 3 12 -5 -15 77.8889 50.8351 4 12 5 -14 184.466 75.3170 3 12 -5 -14 128.797 54.8935 4 12 5 -13 56.1283 123.901 6 12 5 -13 40.2890 63.3050 3 12 -5 -13 117.210 62.7509 4 12 -5 -12 5372.70 269.259 4 12 5 -12 5450.13 303.144 3 12 5 -12 5027.00 606.333 6 12 5 -11 791.788 260.331 6 12 5 -11 858.709 128.208 3 12 -5 -11 878.639 113.001 4 12 5 -10 2045.97 379.858 6 12 -5 -10 1807.57 155.187 4 12 5 -10 1665.59 169.746 3 12 5 -9 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317.550 6 12 6 -13 872.760 133.083 3 12 -6 -13 868.046 123.157 4 12 6 -12 117.201 146.623 6 12 6 -12 80.1876 65.8305 3 12 -6 -12-55.7139 62.2605 4 12 6 -11 362.877 201.793 6 12 6 -11 176.584 72.8876 3 12 -6 -11 224.117 74.0722 4 12 -6 -10 2941.94 210.000 4 12 6 -10 2711.81 214.093 3 12 6 -10 2905.70 466.369 6 12 6 -9 274.928 197.335 6 12 6 -9 362.313 98.0217 3 12 -6 -9 274.977 81.0997 4 12 6 -8 90.3684 135.614 6 12 6 -8 387.348 93.6553 3 12 -6 -8 221.906 81.8357 5 12 -6 -8 269.290 71.2196 4 12 -6 -7 5620.34 289.397 5 12 -6 -7 6000.28 288.650 4 12 6 -7 5655.06 300.072 3 12 6 -7 4991.05 581.535 6 12 6 -6 3221.37 462.118 6 12 -6 -6 3299.91 223.919 5 12 -6 -6 3181.51 212.148 4 12 6 -6 3383.38 235.423 3 12 6 -5-91.7317 73.6953 3 12 -6 -5-24.2925 57.3396 5 12 -6 -5 13.0529 50.7381 4 12 6 -5-48.0160 155.317 6 12 -6 -4 1318.19 138.198 4 12 6 -4 1457.34 153.580 3 12 6 -4 1275.64 308.791 6 12 -6 -3 6091.48 295.699 4 12 6 -3 6229.56 309.449 3 12 6 -3 6453.48 640.794 6 12 6 -2 670.896 107.828 3 12 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131.994 6 12 -7 2 214.978 85.8622 4 12 7 2 186.844 77.4551 3 12 7 2 62.7565 108.641 6 12 -7 3 880.958 125.786 4 12 7 3 693.826 117.213 3 12 7 3 718.616 250.918 6 12 -7 4 1494.39 161.437 4 12 7 4 1730.13 173.269 3 12 7 4 1537.81 317.172 6 12 -7 5 262.155 84.6607 4 -12 -7 -5 266.348 86.5852 2 12 7 5 137.142 68.2569 3 12 7 5 254.566 152.505 6 12 -7 6 135.880 64.7147 4 -12 -7 -6 283.129 86.8464 2 12 7 6 247.734 74.5758 3 12 7 6 334.719 167.103 6 12 -7 7 424.534 91.5431 4 -12 -7 -7 512.851 102.370 2 12 7 7 355.323 82.6201 3 -12 -7 -8 4474.69 284.294 2 12 -7 8 4628.73 283.553 4 12 7 8 4394.87 280.937 3 12 7 8 4120.42 527.412 6 -12 -7 -9 2752.89 226.570 2 12 -7 9 2803.37 222.947 4 12 -7 10 2085.87 195.838 4 -12 -7 -10 2334.20 217.328 2 12 -7 11 3540.78 255.708 4 -12 -7 -11 3733.12 265.716 2 12 -7 12 3645.45 258.480 4 -12 -7 -12 3657.01 271.065 2 -12 -7 -13 720.801 135.660 2 12 -7 13 684.338 127.100 4 -12 -7 -14 203.798 91.0948 2 12 -7 14 376.315 111.273 4 -12 -7 -15 330.225 112.336 2 -12 -7 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67.8611 4 12 -8 -6 4824.31 285.830 5 12 -8 -6 4243.79 264.167 4 12 8 -6 4475.66 273.814 3 12 8 -6 4650.56 588.309 6 12 8 -5 46.7900 61.1282 3 12 -8 -5 73.0731 60.1150 5 12 -8 -5 87.9828 55.3252 4 12 8 -5 88.6651 178.755 6 12 -8 -4 1480.38 165.203 5 12 -8 -4 1729.87 172.726 4 12 8 -4 1875.28 175.581 3 12 8 -4 1752.80 373.967 6 12 -8 -3 3086.26 232.195 5 12 -8 -3 3068.16 223.807 4 12 8 -3 2996.08 224.387 3 12 8 -3 3068.72 484.537 6 12 -8 -2 257.713 89.0620 5 12 -8 -2 208.495 79.8326 4 12 8 -2 192.053 69.7704 3 12 8 -2 255.982 170.422 6 12 -8 -1 157.230 75.5151 5 12 -8 -1 140.511 79.4510 4 12 8 -1 161.240 67.3183 3 12 8 -1 99.4742 132.913 6 12 -8 0 3403.35 241.720 5 12 -8 0 3337.97 234.922 4 12 8 0 3061.12 226.377 3 12 8 0 3041.37 465.811 6 12 -8 1 1411.87 161.493 4 12 8 1 1196.57 145.677 3 12 8 1 1476.90 337.106 6 12 -8 2 307.702 91.9655 4 12 8 2 98.8175 72.3479 3 12 8 2 20.2345 127.152 6 12 -8 3-11.5284 54.4034 4 -12 -8 -3 38.1662 63.3384 2 12 8 3 52.7657 59.7210 3 12 -8 4 828.663 130.218 4 -12 -8 -4 966.093 132.318 2 12 8 4 970.687 139.515 3 12 8 4 677.870 190.096 6 12 -8 5 1092.88 141.673 4 -12 -8 -5 989.750 137.628 2 12 8 5 1141.44 142.028 3 12 8 5 668.196 237.483 6 12 -8 6 64.8812 66.6015 4 -12 -8 -6 22.8486 66.2674 2 12 8 6 53.3507 60.5225 3 12 8 6 76.7937 124.895 6 12 -8 7 1047.97 148.980 4 -12 -8 -7 1208.13 155.544 2 12 8 7 1102.94 148.291 3 12 8 7 1244.32 308.152 6 -12 -8 -8 991.363 144.665 2 12 -8 8 949.837 142.303 4 -12 -8 -9-94.1947 86.0264 2 12 -8 9 5.75633 73.0667 4 12 8 9-274.307 162.610 6 -12 -8 -10 4.09803 76.3455 2 12 -8 10 76.2975 73.6136 4 12 -8 11 7589.53 370.568 4 -12 -8 -11 7435.33 378.370 2 -12 -8 -12 62.6315 74.5927 2 12 -8 12 0.39258 67.4080 4 -12 -8 -13 226.958 90.5635 2 12 -8 13 103.229 86.3232 4 -12 -8 -14 203.240 92.9360 2 12 -8 14 208.397 106.459 4 -12 -8 -15 47.9284 75.3960 2 -12 -8 -16 903.962 151.739 2 -12 -8 -17 1636.11 185.543 2 -12 -8 -18 99.7291 92.9225 2 -12 -8 -19 1384.05 168.737 2 -12 -8 -20 202.744 92.2036 2 -12 -8 -21 238.821 104.986 2 -12 -8 -22 384.036 104.766 2 -12 -8 -23 367.983 89.2160 2 -12 -8 -24 192.910 71.4112 2 -12 -8 -25 133.040 69.9418 2 -12 -8 -26 143.316 51.1369 2 -12 -8 -27 932.264 95.8376 2 12 9 -30 90.0212 33.8605 3 12 9 -29-43.9491 42.4334 3 12 9 -28 72.6384 46.4547 3 12 -9 -28 37.2451 35.9763 4 12 9 -27 12.2430 51.0643 3 12 -9 -27 111.119 48.1193 4 12 -9 -26 78.9473 49.2280 4 12 9 -26 87.5865 58.6987 3 12 9 -25 192.425 77.1401 3 12 -9 -25 325.490 74.6347 4 12 9 -24 332.341 89.2280 3 12 -9 -24 332.361 78.4780 4 12 9 -23 611.853 113.836 3 12 -9 -23 636.006 101.925 4 12 9 -22 260.973 88.3884 3 12 -9 -22 371.150 98.4235 4 12 9 -21 226.469 89.9737 3 12 -9 -21 152.582 80.5317 4 12 9 -20 228.144 81.7885 3 12 -9 -20 109.004 75.7685 4 12 9 -19-34.5441 72.8781 3 12 -9 -19 31.1521 60.1616 4 12 9 -18-65.1023 75.6845 3 12 -9 -18-26.1485 81.0964 4 12 9 -17 120.644 64.8752 3 12 -9 -17 95.4760 88.2912 4 12 9 -16 934.266 132.466 3 12 -9 -16 985.442 136.375 4 12 9 -15 22.4116 62.1095 3 12 -9 -15 12.2694 67.3817 4 12 -9 -14 2034.41 185.212 5 12 -9 -14 2188.16 199.879 4 12 9 -14 2000.49 191.347 3 12 -9 -13 3451.24 242.720 5 12 -9 -13 3539.22 250.360 4 12 9 -13 3272.20 248.322 3 12 9 -12 226.487 85.0950 3 12 -9 -12 214.396 88.1986 5 12 -9 -12 175.689 94.4171 4 12 9 -11 257.090 240.828 6 12 9 -11 16.2934 57.5814 3 12 -9 -11 243.157 90.1414 5 12 -9 -11 47.1700 69.9116 4 12 9 -10 257.633 89.6437 3 12 -9 -10 209.703 89.3613 5 12 -9 -10 163.449 77.1925 4 12 -9 -9 297.103 91.7459 5 12 9 -9 92.3685 187.596 6 12 9 -9 261.106 80.7910 3 12 -9 -9 282.268 87.8097 4 12 -9 -8 3745.80 254.804 4 12 -9 -8 3534.01 250.682 5 12 9 -8 3539.21 245.226 3 12 9 -7 171.276 179.633 6 12 9 -7 185.455 78.7840 3 12 -9 -7 76.3572 74.8131 5 12 -9 -7 22.3649 65.2865 4 12 9 -6 762.344 119.221 3 12 -9 -6 529.729 113.181 5 12 -9 -6 665.061 115.896 4 12 9 -6 785.638 262.487 6 12 -9 -5 4820.39 294.359 5 12 -9 -5 5048.76 292.067 4 12 9 -5 4013.55 261.165 3 12 9 -5 4485.11 604.867 6 12 -9 -4 417.301 114.155 5 12 -9 -4 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72.2716 34.6468 4 12 10 -27-9.38462 41.2898 3 12 -10 -27-9.11552 39.1629 4 12 10 -26 259.460 68.5452 3 12 -10 -26 237.650 60.2541 4 12 10 -25 102.167 59.1133 3 12 -10 -25 21.7015 44.8749 4 12 10 -24 612.447 97.8350 3 12 -10 -24 765.474 101.549 4 12 -10 -23 11.9976 52.2705 4 12 10 -23 69.9222 57.3063 3 12 10 -22 4.93690 57.2888 3 12 -10 -22-34.6528 57.1896 4 12 10 -21 145.620 75.9875 3 12 -10 -21 183.337 72.0254 4 12 10 -20 500.023 106.433 3 12 -10 -20 534.649 106.757 4 12 -10 -19-28.2214 62.5084 4 12 10 -19-22.5448 60.5878 3 12 10 -18 415.678 97.6381 3 12 -10 -18 361.651 100.760 4 12 10 -17 24.9306 71.9515 3 12 -10 -17-57.8175 80.4320 4 12 10 -16 36.9433 61.3438 3 12 -10 -16 207.178 84.6469 4 12 10 -15 114.213 66.5557 3 12 -10 -15 123.056 68.3059 5 12 -10 -15 120.651 80.4583 4 12 10 -14 217.787 77.0378 3 12 -10 -14 52.3246 62.9372 5 12 -10 -14 133.383 68.2052 4 12 10 -13 1081.64 138.529 3 12 -10 -13 1141.54 153.477 5 12 -10 -13 968.431 138.058 4 12 -10 -12 2239.18 207.652 5 12 -10 -12 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670.657 111.163 3 12 10 -2 623.999 253.680 6 12 -10 -1 10.4461 63.9313 4 12 -10 -1 74.7602 74.2346 5 12 10 -1 165.772 70.9227 3 12 10 -1 16.3841 152.530 6 12 -10 0 900.739 141.985 5 12 -10 0 1067.50 150.883 4 12 10 0 1138.54 141.113 3 12 10 0 695.301 254.873 6 12 -10 1 55.2134 70.2617 5 12 -10 1 64.9794 70.1219 4 12 10 1 72.2738 55.4323 3 12 10 1 117.734 148.293 6 12 -10 2 164.616 92.3232 5 -12 -10 -2-2.80240 56.6107 2 12 -10 2-41.3499 71.4337 4 12 10 2-77.7996 63.7389 3 12 10 2-61.3445 133.048 6 12 -10 3 2187.31 203.529 4 12 10 3 2238.16 415.465 6 -12 -10 -3 1922.33 178.721 2 -12 -10 -4 638.320 114.325 2 12 -10 4 409.366 107.894 4 12 10 4 545.932 226.967 6 -12 -10 -5 270.695 84.3881 2 12 -10 5 233.285 90.5815 4 12 10 5 285.462 186.921 6 -12 -10 -6 81.1349 66.2565 2 12 -10 6 104.983 86.2400 4 -12 -10 -7 24.5366 59.1668 2 12 -10 7 17.5310 68.1748 4 -12 -10 -8 206.822 81.5461 2 12 -10 8 54.5717 73.4603 4 -12 -10 -9 201.291 80.8149 2 12 -10 9 230.730 91.6825 4 -12 -10 -10 536.467 117.459 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157.444 82.5998 5 12 -11 -5 233.334 98.1086 4 12 -11 -4 6.89549 83.3475 5 12 -11 -4-56.6216 90.5914 4 12 -11 -3 306.884 91.0748 5 12 -11 -3 417.412 116.416 4 12 -11 -2 681.306 130.468 5 12 -11 -2 975.391 152.681 4 12 -11 -1 120.789 78.3817 5 12 -11 -1 100.144 75.3797 4 12 -11 0 1796.50 191.823 5 12 -11 0 2027.62 201.206 4 12 -11 1 1118.68 159.257 5 12 -11 1 1415.57 172.216 4 12 -11 2 1004.33 150.664 5 12 -11 2 1117.13 160.705 4 12 -11 3 341.749 102.023 4 12 -11 4 236.932 98.0492 4 -12 -11 -5 265.321 78.2713 2 12 -11 5 228.815 94.1007 4 12 -11 6 3638.02 264.565 4 -12 -11 -6 3486.56 237.578 2 -12 -11 -7 751.935 126.796 2 12 -11 7 755.708 140.653 4 -12 -11 -8-43.3803 71.6308 2 12 -11 8-49.5964 76.9893 4 12 -11 9 6289.50 333.113 4 -12 -11 -9 5722.77 314.063 2 -12 -11 -10 312.986 95.2920 2 12 -11 10 410.991 112.457 4 -12 -11 -11 477.899 112.749 2 12 -11 11 288.434 94.5858 4 -12 -11 -12 492.564 106.283 2 12 -11 12 571.106 122.579 4 -12 -11 -13 1208.87 148.314 2 12 -11 13 1185.70 154.785 4 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82.0288 5 12 -14 -6-4.36180 73.4218 4 12 -14 -5 248.261 107.101 5 12 -14 -5 39.4123 71.9519 4 12 -14 -4 777.153 136.392 5 12 -14 -4 775.779 140.014 4 12 -14 -3 1411.13 176.029 5 12 -14 -3 1313.23 166.131 4 12 -14 -2 1693.01 180.580 5 12 -14 -2 1796.27 183.283 4 12 -14 -1 91.3121 87.2112 5 12 -14 -1 94.1532 83.0406 4 12 -14 0 761.442 134.812 4 12 -14 0 690.573 132.843 5 12 -14 1 32.2614 72.1415 4 12 -14 2 934.789 138.467 4 12 -14 3 449.529 106.184 4 12 -14 4 1529.63 166.273 4 12 -14 5 840.997 125.180 4 12 -14 6 39.4613 63.3598 4 12 -14 7 28.2681 66.9103 4 12 -14 8 219.690 81.1413 4 12 -14 9 62.3527 63.1866 4 12 -14 10 222.015 72.7664 4 -12 -14 -11 1246.15 138.893 5 12 -14 11 1182.56 128.753 4 -12 -14 -12 1179.26 130.350 5 -12 -14 -13 19.3560 52.8400 5 -12 -14 -14-1.14475 45.4054 5 -12 -14 -15 79.7090 49.1063 5 -12 -14 -16-43.1950 37.7483 5 -12 -14 -17 140.323 38.0158 5 12 -15 -21 67.2299 38.8788 4 12 -15 -20 112.123 42.6222 4 12 -15 -19 50.1356 44.3689 4 12 -15 -18 163.224 53.9197 4 12 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65.7992 4 12 -15 4 774.639 116.914 4 12 -15 5 101.326 61.7848 4 -12 -15 -6 3162.42 218.236 5 12 -15 6 2807.43 196.340 4 -12 -15 -7 562.955 104.942 5 12 -15 7 462.909 92.3099 4 -12 -15 -8 645.396 105.899 5 12 -15 8 688.184 102.818 4 -12 -15 -9 148.470 62.2538 5 12 -15 9 98.3654 55.9123 4 -12 -15 -10 252.869 72.1082 5 12 -15 10 418.452 78.9911 4 -12 -15 -11 88.6224 56.6693 5 -12 -15 -12 148.138 59.1792 5 -12 -15 -13 7.31449 41.9595 5 -12 -15 -14-18.5609 40.0912 5 -12 -15 -15-35.5079 36.2004 5 12 -16 -19 243.634 44.4562 4 12 -16 -18 189.969 50.4238 4 12 -16 -17 51.1351 42.6812 4 12 -16 -16 3.84414 41.0917 4 12 -16 -15 384.180 69.1572 4 12 -16 -14 695.375 93.3655 4 12 -16 -13-12.4417 49.1817 4 12 -16 -12 1244.40 124.152 4 12 -16 -11 334.750 72.0872 4 12 -16 -10 89.1497 58.2879 4 12 -16 -9-10.0466 53.3848 4 12 -16 -8 134.738 61.7839 4 12 -16 -7 513.537 94.0021 4 -12 -16 6 480.269 76.5264 5 12 -16 -6 619.768 100.882 4 -12 -16 5 35.6494 44.4073 5 12 -16 -5-35.2507 67.6059 4 -12 -16 4 11.1454 46.0632 5 12 -16 -4-25.8475 60.0524 4 -12 -16 3 27.0303 56.8504 5 12 -16 -3-46.5316 53.9239 4 -12 -16 2 4.04757 65.5868 5 12 -16 -2-35.1049 57.5851 4 -12 -16 1 66.9006 56.5357 5 12 -16 -1 61.8092 54.3017 4 -12 -16 0 141.648 65.7557 5 12 -16 0 81.9859 57.0875 4 -12 -16 -1 1253.13 139.643 5 12 -16 1 1184.83 128.489 4 -12 -16 -2 424.898 94.4367 5 12 -16 2 319.193 73.2620 4 -12 -16 -3 140.348 72.9448 5 12 -16 3 73.7724 53.6629 4 -12 -16 -4 57.7475 55.6891 5 12 -16 4 298.078 73.7905 4 -12 -16 -5 21.0314 63.8436 5 12 -16 5 85.9277 50.8100 4 -12 -16 -6 197.174 71.2860 5 12 -16 6 204.297 59.4449 4 -12 -16 -7-43.7240 53.8204 5 12 -16 7-40.7703 46.6864 4 -12 -16 -8 179.080 63.6791 5 12 -16 8 137.712 49.5666 4 -12 -16 -9 120.960 55.3097 5 -12 -16 -10 56.7188 54.7187 5 -12 -16 -11 404.605 73.4067 5 -12 -16 -12 13.0740 38.2036 5 -12 -16 -13-22.6851 34.9199 5 12 -17 -16 53.8157 28.3534 4 12 -17 -15 10.6647 27.7390 4 12 -17 -14 81.8814 43.4543 4 12 -17 -13 255.891 52.7970 4 12 -17 -12 53.5408 43.7638 4 12 -17 -11 68.8772 43.6034 4 12 -17 -10 480.732 76.3384 4 12 -17 -9 676.521 88.0689 4 12 -17 -8 100.966 50.6815 4 12 -17 -7 157.594 55.8875 4 12 -17 -6 27.1141 45.5488 4 -12 -17 5-1.71948 19.6387 5 12 -17 -5 518.357 80.4703 4 -12 -17 4 141.437 44.8851 5 12 -17 -4 122.100 51.6833 4 -12 -17 3 142.052 49.7471 5 12 -17 -3 157.519 55.0998 4 -12 -17 2 62.5480 46.9919 5 12 -17 -2 109.532 55.6070 4 -12 -17 1 439.636 75.4306 5 12 -17 -1 353.254 69.6030 4 -12 -17 0 50.1743 47.1232 5 12 -17 0-21.1970 45.7821 4 -12 -17 -1 33.0757 44.6593 5 12 -17 1-36.7567 44.1182 4 -12 -17 -2-4.62445 44.4998 5 12 -17 2 20.2162 37.3610 4 -12 -17 -3 116.931 51.4142 5 12 -17 3 53.9583 40.7111 4 -12 -17 -4 123.099 51.4487 5 12 -17 4 151.977 43.9594 4 -12 -17 -5 148.891 57.0832 5 12 -17 5 83.9508 38.9579 4 -12 -17 -6 483.948 81.7063 5 12 -17 6 341.491 58.2797 4 -12 -17 -7 73.8598 42.8319 5 -12 -17 -8 154.216 51.0671 5 -12 -17 -9 394.236 67.5754 5 -12 -17 -10 51.6221 38.9744 5 -12 -17 -11 18.2176 28.6976 5 12 -18 -10 42.3876 30.6595 4 12 -18 -9 193.734 43.1886 4 12 -18 -8 60.3035 33.7046 4 12 -18 -7 4.83401 26.7652 4 12 -18 -6 116.251 39.5895 4 12 -18 -5 110.192 37.4133 4 12 -18 -4-39.6174 33.3927 4 12 -18 -3 460.545 62.1243 4 -12 -18 2 387.050 56.0106 5 12 -18 -2 392.748 58.4373 4 -12 -18 1 30.3392 30.6989 5 12 -18 -1 107.919 35.7043 4 -12 -18 0 62.3987 36.1562 5 12 -18 0 0.57444 26.9844 4 -12 -18 -1 405.936 60.9796 5 -12 -18 -2 89.2590 37.3004 5 -12 -18 -3 7.50843 34.1418 5 -12 -18 -4 30.4082 31.2963 5 -12 -18 -5 78.0308 38.1144 5 -12 -18 -6 106.840 37.8429 5 -12 -18 -7 659.453 68.6694 5 13 0 -33-27.2675 30.5661 3 13 0 -32 162.035 52.0115 3 13 0 -31-8.03069 42.9852 3 13 0 -30 296.141 74.5028 3 13 0 -29-76.0961 58.2229 3 13 0 -28 96.6911 64.7469 3 13 0 -27-3.94704 64.1599 3 13 0 -26 42.7298 68.0210 3 13 0 -25-52.5179 64.9085 3 13 0 -24 1458.18 166.154 3 13 0 -23-61.8372 71.5204 3 13 0 -22 1818.31 188.190 3 13 0 -21 40.3825 65.2972 3 13 0 -20 1735.00 183.208 3 13 0 -19-37.7200 75.5826 3 13 0 -18 7853.58 369.504 3 13 0 -17 204.004 96.5484 3 13 0 -16 26.2265 63.9064 3 13 0 -15-528.785 213.275 6 13 0 -15 31.2075 60.9340 3 13 0 -14 1729.22 346.600 6 13 0 -14 2485.85 201.784 3 13 0 -13-161.673 122.983 6 13 0 -13-65.0994 80.7001 3 13 0 -12 2185.64 363.079 6 13 0 -12 2922.40 216.375 3 13 0 -11-50.9996 88.0095 6 13 0 -11 18.2483 56.9224 3 13 0 -10 707.851 220.983 6 13 0 -10 844.548 119.471 3 13 0 -9-41.3357 93.5537 6 13 0 -9 20.3767 47.7461 3 13 0 -8 1923.43 322.204 6 13 0 -8 1979.29 178.002 3 13 0 -7 328.910 136.240 6 13 0 -7-23.1518 58.4841 3 13 0 -6 1563.06 260.068 6 13 0 2 8842.50 365.166 3 13 0 3 14.2419 63.1125 3 13 0 4 242.642 76.8946 3 13 0 5 7.04336 53.6541 3 13 0 6 3884.36 223.277 4 13 0 6 3689.87 247.556 3 13 0 7 25.0656 59.4865 3 13 0 8 7447.43 358.567 3 -13 0 -10 734.555 119.992 2 -13 0 -11 54.1918 64.6455 2 13 0 12 165.765 123.983 1 -13 0 -12 194.425 82.6522 2 13 0 13 127.966 192.868 1 -13 0 -13 86.4809 78.6597 2 13 0 14 1282.21 317.180 1 -13 0 -14 782.562 132.379 2 -13 0 -15 6.94921 70.3509 2 -13 0 -16 3065.49 236.413 2 -13 0 -17 27.6977 79.3660 2 -13 0 -18 1702.55 182.092 2 -13 0 -19 4.07503 59.1932 2 -13 0 -20 1438.17 164.323 2 -13 0 -21 72.4753 59.6204 2 -13 0 -22 372.608 95.3676 2 -13 0 -23 27.3372 48.3808 2 -13 0 -24 694.152 95.3995 2 13 1 -33-29.9560 36.2208 3 13 -1 -32 89.7057 35.8794 3 13 1 -32 229.930 60.9122 3 13 -1 -31 71.2444 41.8998 3 13 1 -31 75.6483 59.2420 3 13 -1 -30 220.194 58.4883 3 13 1 -30 173.162 67.3113 3 13 -1 -29 38.1398 54.1304 3 13 1 -29 6.42740 54.5115 3 13 -1 -28 671.592 105.043 3 13 1 -28 683.290 113.533 3 13 -1 -27-17.8303 53.3881 3 13 1 -27-63.4159 67.6883 3 13 -1 -26 260.767 80.9328 3 13 1 -26 342.519 98.5596 3 13 -1 -25 103.434 70.7045 3 13 1 -25 169.948 86.5755 3 13 -1 -24 731.043 123.499 3 13 1 -24 685.985 122.727 3 13 -1 -23 959.647 136.893 3 13 1 -23 877.434 143.033 3 13 -1 -22 530.105 110.594 3 13 1 -22 600.880 126.968 3 13 -1 -21 19.5072 68.6897 3 13 1 -21 41.4354 67.5709 3 13 -1 -20 686.619 115.397 3 13 1 -20 502.281 112.913 3 13 -1 -19 41.7532 68.4261 3 13 1 -19 124.892 78.1652 3 13 1 -18-62.2484 120.174 6 13 -1 -18 104.870 76.1905 3 13 1 -18 282.914 95.5634 3 13 -1 -17 5461.59 300.038 3 13 1 -17 4870.34 294.612 3 13 1 -16 8878.57 817.732 6 13 -1 -16 9095.00 382.612 3 13 1 -16 9369.14 400.325 3 13 1 -15 714.893 240.438 6 13 -1 -15 618.455 108.528 3 13 1 -15 896.788 136.159 3 13 -1 -14 142.514 55.5710 3 13 1 -14 139.370 73.4305 3 13 1 -13 734.229 243.028 6 13 -1 -13 866.443 123.305 3 13 1 -13 631.196 113.029 3 13 1 -12 265.995 162.851 6 13 -1 -12-17.2075 81.0258 6 13 -1 -12 379.271 90.7353 3 13 1 -12 157.287 66.4485 3 13 1 -11-66.0579 113.321 6 13 -1 -11-42.8259 110.737 6 13 -1 -11 60.2701 61.3348 3 13 1 -11 31.5355 57.5973 3 13 1 -10 2456.56 380.425 6 13 -1 -10 2613.61 376.619 6 13 -1 -10 3087.27 213.717 3 13 1 -10 3327.12 228.692 3 13 -1 -9 316.388 138.919 6 13 1 -9 16.0235 88.6451 6 13 -1 -9 370.007 85.8549 3 13 1 -9 301.822 85.8854 3 13 1 -8 1341.92 253.698 6 13 -1 -8 1109.37 249.126 6 13 -1 -8 1573.84 154.294 3 13 1 -8 1627.60 161.079 3 13 1 -7 270.422 113.226 6 13 1 -7 192.903 79.0024 3 13 1 -6 1630.14 281.874 6 13 1 -6 2240.83 183.178 3 13 1 -5 321.556 144.396 6 13 1 -4 877.620 190.173 6 13 1 0 5708.93 293.633 3 13 1 1 1972.98 176.311 3 13 1 2 1175.37 139.128 3 13 -1 3 1194.53 140.403 3 13 1 3 1213.61 143.498 3 13 -1 4 958.737 128.760 3 13 1 4 985.559 133.885 3 13 -1 5 27.1487 41.5219 4 13 -1 5-114.191 61.1440 3 13 1 5-25.0374 68.1211 3 13 -1 6 79.1029 59.2621 4 13 -1 6 120.035 64.3694 3 13 1 6 74.1372 65.3638 3 13 -1 7 5271.45 271.494 4 13 -1 7 6049.81 313.277 3 13 1 7 6046.81 318.000 3 13 -1 8 182.720 57.7886 4 13 -1 8 265.568 83.8284 3 13 1 8 127.399 72.4491 3 13 1 9 1275.74 157.063 3 -13 -1 -10 3265.45 236.767 2 -13 1 -10 2989.34 222.694 2 13 1 10 3375.98 455.823 1 -13 -1 -11 4163.07 271.052 2 -13 1 -11 4008.09 258.687 2 13 1 11 4355.75 530.544 1 -13 -1 -12 4697.70 290.796 2 -13 1 -12 4610.92 277.720 2 13 1 12 4434.41 550.061 1 -13 -1 -13 4352.05 281.398 2 13 1 13 3838.75 524.663 1 -13 1 -13 4274.25 268.201 2 -13 1 -14-43.9138 57.8465 2 -13 -1 -14 13.8573 61.6436 2 13 1 15 2778.68 464.402 1 -13 1 -15 3199.56 236.850 2 -13 -1 -15 3032.94 236.310 2 -13 1 -16 697.425 120.263 2 -13 -1 -16 640.994 122.915 2 -13 1 -17 753.232 122.833 2 -13 -1 -17 615.612 123.749 2 -13 1 -18 563.055 98.2280 2 -13 -1 -18 734.393 131.173 2 -13 1 -19-47.6694 62.9462 2 -13 -1 -19 50.2054 67.5660 2 -13 1 -20 272.386 79.7341 2 -13 -1 -20 158.016 79.5542 2 -13 1 -21 915.391 119.657 2 -13 -1 -21 645.695 111.914 2 -13 -1 -22 424.698 94.0105 2 -13 -1 -23 874.261 120.418 2 -13 -1 -24 195.495 66.8022 2 -13 -1 -25 62.1532 43.9478 2 -13 -1 -26 59.2722 48.8141 2 13 2 -33-12.2062 36.0870 3 13 2 -32-32.8253 42.1909 3 13 2 -31 607.192 90.1209 3 13 -2 -30 266.400 57.4350 3 13 2 -30 277.137 75.6849 3 13 -2 -29-5.52971 42.5711 3 13 2 -29 70.0076 67.1281 3 13 -2 -28 98.3150 52.1993 3 13 2 -28 173.502 85.7568 3 13 -2 -27 25.2712 53.5005 3 13 2 -27 7.57013 66.0649 3 13 -2 -26 175.920 72.2410 3 13 2 -26 55.5224 79.1423 3 13 -2 -25 2.28517 52.9820 3 13 2 -25 88.1890 74.6030 3 13 -2 -24 165.284 74.6881 3 13 2 -24 115.874 80.8268 3 13 -2 -23 195.947 77.2078 3 13 2 -23 153.079 90.2213 3 13 -2 -22 254.143 87.0404 3 13 2 -22 99.7495 84.4341 3 13 -2 -21 1171.42 144.987 3 13 2 -21 1305.92 167.265 3 13 -2 -20 398.613 101.895 3 13 2 -20 203.671 90.0211 3 13 -2 -19 281.541 80.9460 3 13 2 -19 282.117 95.2487 3 13 2 -18 201.864 164.284 6 13 -2 -18 400.790 90.8082 3 13 2 -18 494.072 118.893 3 13 2 -17 4479.40 590.009 6 13 -2 -17 4248.95 261.192 3 13 2 -17 3907.26 271.047 3 13 2 -16 1980.32 379.661 6 13 -2 -16 2419.78 197.513 3 13 2 -16 2172.74 201.356 3 13 2 -15 1926.32 388.682 6 13 -2 -15 2130.69 182.165 3 13 2 -15 2314.00 206.321 3 13 2 -14 1506.00 349.779 6 13 -2 -14 1857.09 173.505 3 13 2 -14 1975.11 191.117 3 13 2 -13 399.188 176.846 6 13 -2 -13 525.000 96.1301 3 13 2 -13 474.570 98.4693 3 13 2 -12 93.6791 133.845 6 13 -2 -12 12.3661 57.0038 3 13 2 -12-121.548 83.3948 3 13 2 -11 1338.78 292.420 6 13 2 -11 1128.89 141.838 3 13 -2 -11 1292.17 140.358 3 13 2 -10 600.939 214.925 6 13 -2 -10 624.254 99.2430 3 13 2 -10 468.357 102.830 3 13 2 -9 805.208 219.260 6 13 -2 -9 1023.23 124.542 3 13 2 -9 1068.45 137.908 3 13 2 -8 1341.70 279.877 6 13 2 -8 1503.15 151.672 3 13 2 -7-299.609 154.313 6 13 2 -7 44.2429 63.2959 3 13 2 -6 2211.68 336.367 6 13 2 -6 2721.34 204.991 3 13 2 -5 4631.27 262.326 3 13 2 -5 4112.06 463.772 6 13 2 -4 3507.68 231.792 3 13 2 -4 3025.50 388.127 6 13 2 -3 397.008 157.086 6 13 2 -3 309.281 83.2684 3 13 2 -2 383.597 90.4651 3 13 2 -2 246.328 127.882 6 13 2 -1 4096.13 247.901 3 13 2 0 398.467 96.0631 3 13 2 1-12.6850 54.7218 3 13 2 2 218.472 79.9652 3 13 -2 3 11.8297 50.5322 3 13 2 3-1.05502 48.9870 3 13 -2 4 633.034 98.8988 4 13 -2 4 909.976 125.020 3 13 2 4 801.514 123.439 3 13 -2 5 3033.23 202.171 4 13 -2 5 2739.45 205.724 3 13 2 5 2850.17 219.180 3 13 -2 6 1274.47 137.843 4 13 -2 6 1319.96 148.609 3 13 2 6 1425.80 163.212 3 13 -2 7-51.6081 46.7175 4 13 -2 7-17.9376 59.1972 3 13 2 7-15.1586 60.7762 3 13 2 8 230.392 105.674 1 13 -2 8 316.491 79.2626 4 13 2 8 271.822 88.9664 3 13 -2 9 302.964 77.8359 4 -13 -2 -9 343.231 91.4761 2 13 2 9 336.664 89.8238 3 13 2 10 2101.27 366.120 1 -13 -2 -10 2080.68 194.308 2 -13 2 -10 1782.17 170.233 2 -13 -2 -11 4576.04 286.563 2 -13 2 -11 4180.69 260.287 2 13 2 11 4264.28 535.823 1 -13 -2 -12 202.935 90.7426 2 -13 2 -12 219.841 78.8237 2 13 2 12 98.5800 180.231 1 13 2 13 2424.32 412.606 1 -13 2 -13 2388.60 197.983 2 -13 -2 -13 2559.92 222.747 2 -13 2 -14 464.425 98.5834 2 -13 -2 -14 833.759 137.243 2 13 2 14 458.790 197.058 1 -13 2 -15 258.130 94.4631 2 -13 -2 -15 284.568 87.9760 2 -13 -2 -16 1385.80 170.454 2 -13 2 -16 1465.61 158.333 2 -13 2 -17 3058.10 219.228 2 -13 -2 -17 2920.43 237.292 2 -13 -2 -18-85.2605 83.9292 2 -13 -2 -19 78.7277 68.6760 2 -13 -2 -20-35.1191 71.4566 2 -13 -2 -21 103.700 66.4221 2 -13 -2 -22 75.1056 70.3206 2 -13 -2 -23-16.7310 70.8696 2 -13 -2 -24 2.10399 59.1057 2 -13 -2 -25 915.744 112.978 2 -13 -2 -26 39.2135 43.6498 2 -13 -2 -27 81.6903 42.9665 2 13 3 -33 391.686 62.7376 3 13 3 -32 12.0924 38.9167 3 13 3 -31 58.8112 53.3261 3 13 3 -30 121.418 58.0133 3 13 3 -29 765.624 117.275 3 13 3 -28-112.957 79.4040 3 13 3 -27 51.8909 68.9527 3 13 -3 -26 74.8570 52.5633 3 13 3 -26-2.90783 79.3803 3 13 -3 -25 501.778 90.6004 3 13 3 -25 511.250 120.828 3 13 -3 -24-54.8809 61.7769 3 13 3 -24-10.9886 74.1202 3 13 -3 -23 51.9412 53.2278 3 13 3 -23 22.1037 77.0514 3 13 -3 -22 451.472 90.6637 3 13 3 -22 620.843 134.141 3 13 -3 -21 35.0854 53.8306 3 13 3 -21 164.047 91.0484 3 13 -3 -20 80.1717 53.0570 3 13 3 -20 115.667 89.7326 3 13 -3 -19 86.6759 55.6374 3 13 3 -19-22.9536 87.1121 3 13 -3 -18 187.928 70.0104 3 13 3 -18 320.105 96.7952 3 13 3 -17 277.938 109.886 6 13 -3 -17 317.381 68.4607 3 13 3 -17 387.375 111.902 3 13 -3 -16 41.1935 51.9377 3 13 3 -16 49.9307 65.5452 3 13 3 -15 1411.30 353.794 6 13 -3 -15 1251.19 140.499 3 13 3 -15 1387.39 165.959 3 13 3 -14 2315.20 428.311 6 13 -3 -14 2121.97 178.317 3 13 3 -14 2301.66 206.680 3 13 3 -13 2651.01 439.429 6 13 -3 -13 1840.50 163.587 3 13 3 -13 2332.84 206.213 3 13 3 -12 1816.55 358.227 6 13 -3 -12 1363.30 137.678 3 13 3 -12 1630.67 171.181 3 13 3 -11-64.9740 114.811 6 13 -3 -11 90.6612 64.9658 3 13 3 -11 17.5035 65.0168 3 13 3 -10 1377.78 316.441 6 13 3 -10 915.119 131.998 3 13 3 -9 92.9753 135.220 6 13 3 -9 17.3841 60.9813 3 13 3 -8-103.469 111.793 6 13 3 -8 169.372 69.0543 3 13 3 -7 5344.06 293.240 3 13 3 -7 5452.93 579.185 6 13 3 -6 3308.12 229.229 3 13 3 -6 2997.10 419.813 6 13 3 -5 3898.34 244.622 3 13 3 -5 3576.08 447.194 6 13 3 -4 886.719 130.497 3 13 3 -4 963.598 219.238 6 13 3 -3 4664.98 266.344 3 13 3 -3 4519.03 482.193 6 13 3 -2-74.7646 68.0433 3 13 3 -2 6.61701 87.5461 6 13 3 -1 1861.60 300.937 6 13 3 -1 2567.72 201.240 3 13 3 0 3679.82 243.231 3 13 3 0 3088.12 387.652 6 13 3 1 475.448 101.012 3 13 -3 2 310.044 73.1309 4 13 3 2 414.908 95.3848 3 13 -3 3 399.317 86.9074 4 13 -3 3 413.536 88.0791 3 13 3 3 489.236 99.8625 3 13 -3 4 958.653 117.226 4 13 -3 4 881.305 121.669 3 13 3 4 994.899 136.129 3 13 -3 5 72.7325 53.4293 4 13 -3 5-7.07975 59.6794 3 13 3 5 7.77698 62.1882 3 13 -3 6 828.044 121.103 4 13 -3 6 644.120 113.739 3 13 3 6 707.660 115.359 3 13 -3 7 4350.25 257.113 4 13 3 7 4668.89 285.676 3 13 3 7 3897.06 459.395 1 13 -3 8 142.745 73.5983 4 13 3 8 53.4469 73.5801 3 13 -3 9 19.8515 51.6702 4 -13 -3 -9 51.6847 67.0986 2 13 3 9 152.648 86.2727 3 13 3 9-68.0280 136.754 1 -13 -3 -10 2609.72 220.544 2 -13 3 -10 2220.65 183.794 2 13 -3 10 2367.12 203.338 4 13 3 10 2284.45 373.511 1 -13 -3 -11 197.392 88.1089 2 -13 3 -11 259.920 75.3137 2 13 3 12-629.131 224.271 1 -13 -3 -12 42.6266 63.4715 2 13 3 13 2683.52 447.908 1 -13 -3 -13 2414.38 219.485 2 -13 -3 -14 231.020 100.204 2 13 3 14 58.3456 114.049 1 -13 -3 -15 384.813 112.696 2 -13 -3 -16 175.779 99.8965 2 -13 -3 -17 870.281 138.880 2 -13 -3 -18 1085.87 156.155 2 -13 -3 -19 229.504 95.0098 2 -13 -3 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325.864 3 13 4 -12 5836.35 646.476 6 13 4 -11 168.718 152.581 6 13 4 -11 29.9087 58.0087 3 13 4 -10 77.4960 136.389 6 13 4 -10 188.494 69.7848 3 13 4 -9 319.316 173.432 6 13 4 -9 220.389 81.9372 3 13 -4 -9 132.080 45.0331 4 13 -4 -8 7615.64 310.465 4 13 4 -8 7780.32 356.117 3 13 4 -8 8340.73 731.783 6 13 4 -7 209.692 177.820 6 13 4 -7 122.967 69.3870 3 13 -4 -7 122.037 52.0768 4 13 4 -6 140.027 136.640 6 13 4 -6 166.875 72.9752 3 13 -4 -6 139.803 65.5344 4 13 4 -5 328.409 165.592 6 13 4 -5 423.339 100.000 3 13 -4 -5 462.918 86.6245 4 13 4 -4 37.9563 143.015 6 13 4 -4 31.6146 56.3677 3 13 -4 -4 53.4377 47.8505 4 13 4 -3 164.567 160.345 6 13 4 -3-7.02237 67.6141 3 13 -4 -3 138.143 53.2633 4 13 4 -2 579.016 107.840 3 13 4 -2 382.917 174.899 6 13 -4 -2 587.905 96.1434 4 13 -4 -1 2532.48 184.330 4 13 4 -1 2290.13 195.253 3 13 4 -1 2002.17 337.085 6 13 -4 0 24.9305 48.7284 4 13 4 0 44.4757 64.2517 3 13 4 0 57.1515 112.373 6 13 -4 1 136.028 59.6892 4 13 4 1 226.734 68.7609 3 13 -4 2 82.6094 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77.2133 2 -13 -4 -22 128.408 74.5340 2 -13 -4 -23 92.8165 70.7451 2 -13 -4 -24 97.8023 61.8211 2 -13 -4 -25 186.997 70.4678 2 -13 -4 -26 102.799 47.9208 2 -13 -4 -27 33.9714 41.1392 2 -13 -4 -28 13.5613 30.6063 2 13 5 -33 27.6487 32.3063 3 13 5 -32 162.612 47.5644 3 13 5 -31-1.73105 44.8292 3 13 5 -30 59.4889 52.9641 3 13 5 -29 55.4200 64.6077 3 13 5 -28 218.495 82.8690 3 13 5 -27 89.2038 69.3149 3 13 5 -26 1290.39 156.807 3 13 5 -25 71.1756 81.2277 3 13 5 -24 24.1007 90.2725 3 13 5 -23-43.4468 72.0941 3 13 5 -22 905.405 146.983 3 13 5 -21 80.0296 77.7047 3 13 5 -20 268.601 109.645 3 13 5 -19 7.46853 76.2789 3 13 5 -18 415.875 112.890 3 13 5 -17 944.425 291.465 6 13 5 -17 145.292 91.6848 3 13 5 -16 223.099 123.560 6 13 5 -16 481.550 113.284 3 13 -5 -16 467.517 86.1251 4 13 5 -15 223.353 173.234 6 13 5 -15 279.310 86.6736 3 13 -5 -15 354.440 76.7706 4 13 5 -14 915.412 137.855 3 13 -5 -14 767.182 111.266 4 13 5 -13 89.8367 136.520 6 13 5 -13 88.8149 76.4631 3 13 -5 -13 151.033 51.5802 4 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3729.52 487.239 6 13 -6 0 137.809 66.3866 4 13 6 0-57.0098 81.0675 3 13 6 0 272.792 147.669 6 13 -6 1 198.188 78.0806 4 13 6 1 254.900 87.0774 3 13 6 1 171.352 140.023 6 13 -6 2 2715.87 208.300 4 13 6 2 2657.71 217.631 3 13 6 2 3089.48 435.040 6 13 -6 3 185.896 80.6494 4 13 6 3 191.564 72.0933 3 13 6 3 89.5040 119.497 6 13 -6 4 24.4360 57.0156 4 13 6 4-18.4215 61.7357 3 13 6 4 6.85992 123.708 6 13 -6 5 219.515 81.7102 4 13 6 5 171.155 78.2410 3 13 -6 6 89.0890 62.7598 4 -13 -6 -6 157.514 74.5764 2 13 6 6 204.200 90.1552 3 13 -6 7 794.143 124.118 4 -13 -6 -7 742.771 125.059 2 13 6 7 935.190 148.547 3 -13 -6 -8 4617.93 293.279 2 13 -6 8 4661.68 283.842 4 13 6 8 4297.56 283.264 3 13 -6 9 109.526 79.7056 4 -13 -6 -9 45.9342 78.4075 2 13 -6 10 88.5255 67.8558 4 -13 -6 -10 74.9097 68.0475 2 13 -6 11 51.0738 80.9992 4 -13 -6 -11 44.2712 74.8519 2 13 -6 12 769.021 135.819 4 -13 -6 -12 809.487 144.839 2 -13 -6 -13 1.71873 76.4005 2 13 -6 13 323.597 115.779 4 -13 -6 -14 328.787 111.332 2 -13 -6 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13 7 -16 336.397 92.7581 3 13 -7 -16 319.606 85.7209 4 13 7 -15 1152.96 160.876 3 13 -7 -15 1061.12 137.317 4 13 7 -14 24.6545 67.6840 3 13 -7 -14-42.9055 56.7741 4 13 7 -13 334.958 222.193 6 13 7 -13 335.416 105.527 3 13 -7 -13 228.476 82.8760 4 13 7 -12 1951.20 412.287 6 13 -7 -12 2197.77 191.678 4 13 7 -12 2179.02 205.911 3 13 7 -11 349.759 230.084 6 13 7 -11 551.314 127.096 3 13 -7 -11 583.358 122.270 4 13 7 -10 3119.77 497.463 6 13 -7 -10 2489.63 202.413 4 13 7 -10 2783.18 225.687 3 13 7 -9 604.568 236.233 6 13 7 -9 827.188 127.981 3 13 -7 -9 957.368 131.047 4 13 7 -8 651.697 112.809 3 13 -7 -8 693.915 110.429 4 13 7 -7 28.2780 70.7251 3 13 -7 -7 59.5996 56.1652 4 13 7 -6 365.919 98.4532 3 13 -7 -6 356.853 93.0021 4 13 7 -6 447.917 216.272 6 13 7 -5 913.049 135.927 3 13 7 -5 1023.30 262.433 6 13 -7 -5 941.024 129.763 4 13 7 -4 82.3869 55.2317 3 13 -7 -4 94.5797 61.5159 4 13 7 -4-59.1435 131.096 6 13 -7 -3 4762.15 276.704 4 13 7 -3 5341.53 300.984 3 13 7 -3 5611.20 629.191 6 13 -7 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54.2545 79.5323 2 13 -7 11 80.4572 88.7898 4 -13 -7 -12-32.0063 79.1708 2 13 -7 12-23.3330 76.9003 4 -13 -7 -13 28.7191 72.6127 2 13 -7 13 56.4221 68.7228 4 -13 -7 -14-7.27366 78.6998 2 -13 -7 -15 1006.23 158.025 2 -13 -7 -16 1121.70 163.604 2 -13 -7 -17 1863.02 205.447 2 -13 -7 -18 213.497 94.3504 2 -13 -7 -19 365.348 104.039 2 -13 -7 -20 286.740 102.502 2 -13 -7 -21 137.492 85.2077 2 -13 -7 -22-47.9072 73.3747 2 -13 -7 -23 190.876 76.1918 2 -13 -7 -24 47.5227 53.7471 2 -13 -7 -25 72.2002 54.6532 2 -13 -7 -26 126.840 47.8244 2 -13 -7 -27 1620.61 112.852 2 13 8 -30 1.53381 32.6701 3 13 8 -29-20.0795 41.6328 3 13 8 -28-7.79359 45.6359 3 13 8 -27 49.3717 56.6006 3 13 8 -26 49.6386 50.4313 3 13 -8 -26 81.6074 40.3074 4 13 8 -25 305.970 88.2084 3 13 -8 -25 73.5431 49.3518 4 13 8 -24 189.211 76.7857 3 13 -8 -24 141.579 57.9044 4 13 8 -23 204.056 92.0993 3 13 -8 -23 90.2535 70.7300 4 13 8 -22 219.368 94.0107 3 13 -8 -22 128.619 53.9721 4 13 8 -21 92.7583 77.5437 3 13 -8 -21 99.7283 66.7018 4 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737.240 134.449 2 -14 -4 -14 569.890 128.348 2 -14 -4 -15 70.8885 82.1957 2 -14 -4 -16 93.8039 88.6398 2 -14 -4 -17 335.493 108.982 2 -14 -4 -18 661.171 123.843 2 -14 -4 -19 876.628 135.562 2 -14 -4 -20 941.814 135.568 2 -14 -4 -21 75.5554 69.3713 2 -14 -4 -22 214.934 85.0173 2 -14 -4 -23 5.58266 51.8222 2 -14 -4 -24 740.911 101.646 2 -14 -4 -25 37.5844 45.5312 2 -14 -4 -26 62.4707 40.7202 2 14 5 -32 64.2837 34.6202 3 14 5 -31-30.6895 36.7952 3 14 5 -30-21.3797 41.9160 3 14 5 -29 89.9779 58.9083 3 14 5 -28 171.836 69.7139 3 14 5 -27 21.4891 60.0351 3 14 5 -26 396.700 102.969 3 14 5 -25 8.92530 73.3268 3 14 5 -24-37.9825 80.9317 3 14 5 -23 135.525 86.6131 3 14 5 -22 243.994 99.8640 3 14 5 -21 744.413 133.569 3 14 5 -20 369.054 116.454 3 14 5 -19 139.958 86.6636 3 14 5 -18 426.790 112.360 3 14 5 -17 2372.20 217.829 3 14 5 -16 965.874 150.710 3 14 5 -15 123.386 128.831 6 14 5 -15-7.46022 76.0633 3 14 5 -14 489.117 219.232 6 14 5 -14 553.455 122.361 3 14 5 -13 985.414 293.487 6 14 5 -13 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14 -5 1 496.809 100.039 4 14 5 1 819.531 135.947 3 14 -5 2 155.594 61.6390 4 14 5 2 70.8746 73.0483 3 14 -5 3 69.6830 54.5313 4 14 5 3 36.1315 74.5368 3 14 -5 4 2388.82 200.371 4 14 5 4 2204.53 206.570 3 14 -5 5 1159.60 143.047 4 14 5 5 1298.54 163.536 3 14 -5 6 4637.56 279.620 4 -14 -5 -6 5023.63 307.224 2 14 5 6 5225.59 314.428 3 14 -5 7 569.348 117.890 4 -14 -5 -7 534.110 123.279 2 14 5 7 450.977 106.507 3 14 -5 8 9.38060 68.1099 4 -14 -5 -8 112.239 71.5778 2 14 5 8 92.8477 69.9949 3 14 -5 9 75.0433 78.1810 4 -14 -5 -9 113.941 87.5904 2 14 -5 10 931.909 141.486 4 -14 -5 -10 955.758 145.626 2 14 -5 11 185.551 82.6262 4 -14 -5 -11 159.853 81.6571 2 -14 -5 -12 247.714 101.342 2 -14 -5 -13 55.4862 72.0583 2 -14 -5 -14 544.612 129.687 2 -14 -5 -15 351.450 123.168 2 -14 -5 -16 1405.74 175.384 2 -14 -5 -17 2014.95 204.172 2 -14 -5 -18 403.552 110.573 2 -14 -5 -19 630.331 122.960 2 -14 -5 -20 15.8657 72.4052 2 -14 -5 -21 168.716 90.2276 2 -14 -5 -22 1842.92 172.242 2 -14 -5 -23 243.505 76.7817 2 -14 -5 -24 43.6019 57.4333 2 -14 -5 -25 48.1381 46.5195 2 -14 -5 -26 1225.21 106.578 2 14 6 -31 56.9411 34.9671 3 14 6 -30-47.8582 46.6339 3 14 6 -29 816.319 103.171 3 14 6 -28 86.0128 60.6561 3 14 6 -27 442.009 89.3324 3 14 6 -26 538.567 101.744 3 14 6 -25 38.2625 70.9413 3 14 6 -24 15.2500 77.0404 3 14 6 -23-42.5648 84.5535 3 14 6 -22 239.097 78.7730 3 14 6 -21 288.309 89.2528 3 14 6 -20 1824.57 196.781 3 14 6 -19 38.9845 78.2353 3 14 -6 -18 1655.30 152.901 4 14 6 -18 1886.16 196.160 3 14 6 -17 19.4355 78.1645 3 14 -6 -17 14.9981 55.7238 4 14 6 -16 60.9857 71.7867 3 14 -6 -16 142.392 62.7803 4 14 6 -15 713.932 133.168 3 14 -6 -15 898.644 123.897 4 14 6 -14 55.0218 73.7656 3 14 -6 -14 69.2340 56.3096 4 14 6 -13 1283.78 329.876 6 14 6 -13 1064.06 158.005 3 14 -6 -13 678.690 115.324 4 14 -6 -12 6972.69 323.406 4 14 6 -12 6973.68 363.057 3 14 6 -12 6801.42 748.545 6 14 6 -11 314.965 147.245 6 14 6 -11 367.198 117.119 3 14 -6 -11 321.950 87.5842 4 14 6 -10 3060.92 505.866 6 14 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732.898 130.439 3 14 -6 4 407.354 97.3672 4 14 6 4 274.973 90.4787 3 14 -6 5 233.032 84.5154 4 -14 -6 -5 460.752 121.028 2 14 6 5 434.919 112.634 3 14 -6 6 46.4363 68.9698 4 -14 -6 -6 64.0815 68.7172 2 14 6 6 40.9998 76.7233 3 14 -6 7 1172.96 150.797 4 -14 -6 -7 1280.54 168.027 2 14 6 7 1289.20 166.196 3 14 -6 8 6.91143 78.3038 4 -14 -6 -8 37.7681 73.0042 2 14 6 8 46.6080 67.7487 3 14 -6 9 858.204 134.728 4 -14 -6 -9 872.956 146.068 2 14 -6 10 296.298 99.5090 4 -14 -6 -10 345.984 109.460 2 14 -6 11 408.362 103.308 4 -14 -6 -11 418.442 113.143 2 14 -6 12 161.046 94.1646 4 -14 -6 -12 396.410 110.399 2 -14 -6 -13 30.0112 85.1013 2 -14 -6 -14 517.278 122.333 2 -14 -6 -15 3.77991 76.4532 2 -14 -6 -16 785.172 142.949 2 -14 -6 -17 356.858 109.510 2 -14 -6 -18 366.036 111.962 2 -14 -6 -19 104.109 82.1267 2 -14 -6 -20 886.238 135.118 2 -14 -6 -21 144.754 81.7968 2 -14 -6 -22 0.30152 57.2819 2 -14 -6 -23 306.918 84.4012 2 -14 -6 -24 953.153 111.075 2 -14 -6 -25 634.147 87.0138 2 -14 -6 -26 684.446 78.1584 2 14 7 -30 266.509 54.4028 3 14 7 -29 13.7099 39.3906 3 14 7 -28 88.7389 54.9922 3 14 7 -27 200.367 70.2917 3 14 7 -26 143.244 69.1107 3 14 7 -25 44.1587 61.6572 3 14 7 -24-16.2622 66.9882 3 14 7 -23 19.2574 69.9029 3 14 7 -22-24.1246 73.0206 3 14 -7 -22 0.25744 45.7462 4 14 7 -21 696.291 130.763 3 14 -7 -21 411.928 82.7463 4 14 7 -20 116.253 84.4225 3 14 -7 -20 26.7607 49.2341 4 14 -7 -19 2667.92 193.311 4 14 7 -19 2671.64 226.755 3 14 -7 -18 1618.24 161.152 4 14 7 -18 1656.09 190.545 3 14 7 -17 1252.82 167.100 3 14 -7 -17 915.623 123.468 4 14 7 -16 88.6377 79.7270 3 14 -7 -16 91.6788 66.0410 4 14 7 -15 56.6009 70.3547 3 14 -7 -15 68.3688 62.7161 4 14 7 -14 975.974 150.466 3 14 -7 -14 1277.06 148.724 4 14 7 -13 90.2176 83.3097 3 14 -7 -13 262.667 86.5253 4 14 -7 -12 3042.60 223.076 4 14 7 -12 2992.14 246.427 3 14 7 -11 585.903 196.492 6 14 7 -11 964.671 149.903 3 14 -7 -11 1028.20 128.688 4 14 7 -10 80.1656 78.6378 3 14 -7 -10 39.6912 65.2603 4 14 7 -9 452.243 215.152 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130.014 59.8494 3 14 8 -25 116.751 63.8917 3 14 8 -24 103.123 65.9423 3 14 -8 -24 55.1544 41.1467 4 14 8 -23 34.8828 66.2341 3 14 -8 -23 58.6721 49.8281 4 14 8 -22 1276.31 151.517 3 14 -8 -22 1225.27 124.970 4 14 8 -21 350.809 99.5801 3 14 -8 -21 261.974 75.0818 4 14 8 -20 266.105 97.2986 3 14 -8 -20 202.069 72.6587 4 14 8 -19 79.3861 73.1688 3 14 -8 -19 158.797 63.3231 4 14 8 -18 617.023 122.492 3 14 -8 -18 480.025 93.7932 4 14 8 -17 88.1966 77.1464 3 14 -8 -17 112.313 65.2037 4 14 8 -16 55.3631 67.6667 3 14 -8 -16 120.071 67.7066 4 14 8 -15 39.5403 74.2127 3 14 -8 -15 24.8581 68.2279 4 14 8 -14 667.378 132.450 3 14 -8 -14 554.957 106.951 4 14 -8 -13 6981.30 335.563 4 14 8 -13 6966.16 356.508 3 14 8 -12 592.722 122.829 3 14 -8 -12 957.079 134.517 4 14 -8 -11 5072.59 288.497 4 14 8 -11 5269.64 311.976 3 14 8 -10 1141.75 151.962 3 14 -8 -10 1123.75 147.663 4 14 8 -9 1217.14 163.198 3 14 -8 -9 1132.01 145.169 4 14 8 -8 115.666 74.7841 3 14 -8 -8 148.926 79.6324 4 14 8 -7 298.653 89.1716 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4 -17 406.009 60.5962 3 22 4 -16-20.6432 33.0156 3 22 4 -15-24.5904 37.7977 3 22 4 -14 267.291 62.2004 3 22 4 -13 55.2573 45.1480 3 22 4 -12 272.164 67.3131 3 22 4 -11 21.9044 46.1906 3 22 4 -10-40.3522 57.6965 3 22 4 -9-29.2449 54.3344 3 22 4 -8 1455.01 135.496 3 22 4 -7 80.9847 61.8650 3 22 4 -6 324.393 78.2529 3 -22 -4 5 196.035 64.9151 2 22 4 -5 154.998 62.5032 3 -22 -4 4 48.2933 56.2150 2 22 4 -4 9.24701 53.3685 3 -22 -4 3 255.761 70.5104 2 22 4 -3 328.480 82.6172 3 -22 -4 2 105.682 59.6927 2 -22 4 2 217.522 54.9272 2 -22 -4 1 798.436 104.705 2 -22 4 1 762.735 86.5051 2 -22 -4 0 307.492 77.0081 2 -22 4 0 303.185 56.2273 2 -22 -4 -1 138.723 58.0731 2 -22 4 -1 12.7543 32.0634 2 -22 -4 -2 87.0131 53.4484 2 -22 -4 -3-0.23404 43.5117 2 -22 -4 -4-15.6246 45.5004 2 -22 -4 -5 36.5261 40.9942 2 -22 -4 -6 422.474 75.9506 2 -22 -4 -7 645.511 82.4294 2 -22 -4 -8 111.726 46.1130 2 -22 -4 -9 198.345 46.7081 2 22 5 -16 69.6350 35.6040 3 22 5 -15 28.0087 31.8601 3 22 5 -14 525.980 74.9183 3 22 5 -13 367.227 66.7589 3 22 5 -12 95.9764 50.8377 3 22 5 -11 353.824 73.4799 3 22 5 -10 217.516 60.0868 3 22 5 -9 144.259 54.7639 3 -22 -5 8 15.3761 41.1908 2 22 5 -8 237.424 69.0795 3 -22 -5 7 398.002 75.1726 2 22 5 -7 539.700 89.5512 3 -22 -5 6 671.074 91.6315 2 22 5 -6 815.687 105.515 3 -22 -5 5 68.1371 51.9731 2 22 5 -5 92.8915 60.6818 3 -22 -5 4-31.3465 50.6870 2 22 5 -4 55.5142 53.3261 3 -22 -5 3 97.2477 52.4014 2 22 5 -3 1.24968 48.3376 3 -22 -5 2-13.5757 47.6465 2 -22 -5 1 73.0410 49.7113 2 -22 -5 0 595.109 93.4065 2 -22 -5 -1 183.253 60.1448 2 -22 -5 -2 559.061 85.1996 2 -22 -5 -3-96.9046 51.7018 2 -22 -5 -4 221.818 62.7552 2 -22 -5 -5 199.958 58.0607 2 -22 -5 -6 59.8967 39.4105 2 -22 -5 -7 58.5678 39.9821 2 -22 -5 -8 79.2279 36.2873 2 -22 -5 -9 232.620 46.7922 2 22 6 -15 72.9920 32.4533 3 22 6 -14 41.6483 33.8988 3 22 6 -13 0.53842 34.4148 3 22 6 -12 279.775 60.6389 3 -22 -6 11 42.3248 30.5127 2 22 6 -11 151.272 51.7690 3 -22 -6 10 20.5581 36.1820 2 22 6 -10 19.6299 42.0720 3 -22 -6 9 19.8208 34.0253 2 22 6 -9 8.74712 43.5028 3 -22 -6 8 167.439 47.4242 2 22 6 -8 263.617 64.6878 3 -22 -6 7 144.262 47.4402 2 22 6 -7 110.007 47.4897 3 -22 -6 6 116.724 49.6205 2 22 6 -6 206.932 59.1959 3 -22 -6 5 117.807 45.2717 2 22 6 -5 212.404 64.8472 3 -22 -6 4 673.219 86.3870 2 22 6 -4 682.905 94.0402 3 -22 -6 3 12.0457 41.1005 2 -22 -6 2 110.316 50.7120 2 -22 -6 1 589.450 82.7132 2 -22 -6 0-15.0946 38.2745 2 -22 -6 -1 83.4700 43.8982 2 -22 -6 -2 253.715 56.4202 2 -22 -6 -3 38.0710 41.5740 2 -22 -6 -4 17.4279 37.6618 2 -22 -6 -5 244.481 55.6611 2 -22 -6 -6 345.243 58.0059 2 -22 -6 -7 175.219 44.0675 2 22 7 -13 150.439 38.1321 3 22 7 -12 6.06552 29.3773 3 22 7 -11 35.6677 35.1927 3 22 7 -10 28.0411 34.1133 3 22 7 -9 20.8201 41.0242 3 -22 -7 8 205.775 37.9998 2 22 7 -8 386.147 67.8367 3 -22 -7 7 219.389 47.4555 2 22 7 -7 298.702 58.5745 3 -22 -7 6 39.6368 29.6617 2 22 7 -6-4.60847 42.4773 3 -22 -7 5 46.9863 31.4649 2 22 7 -5-0.40424 41.5394 3 -22 -7 4 17.9232 29.4875 2 -22 -7 3 147.653 46.2513 2 -22 -7 2-5.44738 31.3282 2 -22 -7 1 101.390 43.4507 2 -22 -7 0 55.7466 37.9979 2 -22 -7 -1 26.2997 31.9945 2 -22 -7 -2 21.5023 31.4880 2 -22 -7 -3 376.145 57.2503 2 -22 -7 -4 132.822 39.1436 2 -22 -7 -5 48.4276 26.0329 2 22 8 -9-17.8586 27.2407 3 22 8 -8 34.0951 31.4284 3 23 0 -11 12.5483 22.6819 3 23 0 -10 173.149 42.4727 3 -23 0 4-34.6706 44.5097 2 -23 0 3-55.3263 51.0021 2 -23 0 2 41.4843 38.7855 2 -23 0 1 53.0357 41.9358 2 -23 0 0 219.772 57.1066 2 -23 0 -1 41.7102 39.6786 2 -23 0 -2 155.198 49.2212 2 -23 0 -3 44.0122 38.2425 2 -23 0 -4 81.6239 34.3764 2 -23 0 -5-34.4770 27.9570 2 23 1 -12 92.7797 38.9348 3 23 1 -11-9.95848 31.7119 3 23 1 -10 74.5891 37.1168 3 23 1 -9-23.3018 36.7066 3 23 1 -8 11.0491 35.5737 3 -23 -1 4 174.126 60.2128 2 -23 1 4 184.541 56.8160 2 -23 -1 3 24.9004 44.5458 2 -23 1 3-18.2193 38.0086 2 -23 -1 2 228.054 65.6398 2 -23 1 2 243.770 55.9686 2 -23 -1 1 43.9965 46.6289 2 -23 1 1 64.8697 38.2465 2 -23 -1 0 1139.03 107.960 2 -23 1 0 1293.70 110.400 2 -23 1 -1-64.7357 44.5213 2 -23 -1 -1 36.9171 44.3658 2 -23 1 -2 844.598 83.5881 2 -23 -1 -2 881.672 93.5327 2 -23 1 -3 209.334 45.0926 2 -23 -1 -3 219.039 51.1726 2 -23 1 -4 73.1126 35.4205 2 -23 -1 -4 75.7102 38.4998 2 -23 -1 -5 6.10956 27.1995 2 23 2 -13 102.047 32.4872 3 23 2 -12-25.7535 32.5436 3 23 2 -11 159.189 47.3118 3 23 2 -10 48.8745 36.0756 3 23 2 -9 40.0214 34.8757 3 23 2 -8 39.4115 38.3660 3 23 2 -7 94.6011 40.0711 3 -23 -2 5 261.161 64.9538 2 -23 -2 4 62.3413 47.3329 2 -23 2 4 20.2193 35.5497 2 -23 -2 3 396.488 75.3735 2 -23 2 3 349.294 63.0705 2 -23 -2 2 90.4834 49.9413 2 -23 2 2 27.1476 35.0884 2 -23 -2 1-16.3019 43.4803 2 -23 2 1 57.7460 40.6448 2 -23 -2 0 16.7863 40.6495 2 -23 2 0-11.4816 33.5243 2 -23 2 -1-6.32034 30.8802 2 -23 -2 -1-4.57750 41.1059 2 -23 2 -2 458.749 61.6828 2 -23 -2 -2 479.767 73.8294 2 -23 -2 -3 251.138 51.8286 2 -23 -2 -4 235.624 52.6532 2 -23 -2 -5 90.8097 41.0209 2 -23 -2 -6 364.148 54.9469 2 23 3 -13 58.0224 30.6367 3 23 3 -12 227.809 47.9039 3 23 3 -11 509.432 67.2178 3 23 3 -10 736.579 82.7922 3 23 3 -9-9.77141 34.3560 3 23 3 -8 24.8206 35.8085 3 -23 -3 7 103.319 49.9133 2 23 3 -7 5.56272 38.9250 3 -23 -3 6 99.6496 50.5524 2 23 3 -6 64.1046 45.9925 3 -23 -3 5-59.5082 44.3243 2 -23 -3 4-4.92135 42.4599 2 -23 3 4 1.19495 31.1503 2 -23 -3 3 313.396 66.5482 2 -23 3 3 346.992 55.8955 2 -23 -3 2 36.9273 43.1724 2 -23 3 2 43.0139 31.4857 2 -23 -3 1 817.787 93.0600 2 -23 3 1 505.518 61.8252 2 -23 -3 0 20.7643 37.3664 2 -23 -3 -1 35.6778 34.1497 2 -23 -3 -2-14.3708 34.6462 2 -23 -3 -3 56.0303 40.0871 2 -23 -3 -4 33.6192 30.1956 2 -23 -3 -5-30.0877 30.3828 2 23 4 -12-1.71575 32.9192 3 -23 -4 11 508.120 62.3748 2 23 4 -11 528.042 68.5565 3 -23 -4 10 709.259 75.1578 2 23 4 -10 657.491 77.6624 3 -23 -4 9 518.536 70.1769 2 23 4 -9 525.626 72.2154 3 -23 -4 8 18.5240 30.6654 2 23 4 -8 89.2219 45.4816 3 -23 -4 7 12.6366 34.2105 2 23 4 -7-2.10760 38.7997 3 -23 -4 6 597.485 76.6169 2 -23 4 6 553.822 64.0751 2 -23 -4 5 247.274 53.9908 2 -23 4 5 252.255 46.6550 2 -23 -4 4 35.3551 42.0688 2 -23 -4 3 178.516 52.9983 2 -23 -4 2 10.0787 35.6803 2 -23 -4 1 136.141 46.5443 2 -23 -4 0 15.3587 36.5856 2 -23 -4 -1 238.133 53.7964 2 -23 -4 -2-48.4589 34.7854 2 -23 -4 -3 146.210 43.1319 2 -23 -4 -4-61.5738 33.1394 2 -23 -4 -5 305.849 50.8253 2 23 5 -11-8.25294 28.1337 3 23 5 -10 201.646 45.9098 3 -23 -5 9-16.8166 28.4906 2 23 5 -9-22.5108 32.6435 3 -23 -5 8 372.755 58.1630 2 23 5 -8 366.356 62.2558 3 -23 -5 7 68.4517 36.6843 2 23 5 -7 48.4222 40.2397 3 -23 -5 6 760.334 79.6924 2 -23 -5 5 22.7612 32.5136 2 -23 -5 4 556.731 68.8571 2 -23 -5 3 106.129 39.7202 2 -23 -5 2-7.65171 30.9846 2 -23 -5 1 14.1845 36.0981 2 -23 -5 0 367.174 61.0105 2 -23 -5 -1-6.16361 27.8305 2 -23 -5 -2 131.217 40.4401 2 -23 -5 -3 14.5334 29.6402 2 23 6 -9 107.209 37.9528 3 -24 0 8 16.3141 26.4327 2 -24 0 7 27.5440 28.7330 2 -24 0 6 37.6966 30.8647 2 -24 0 5 61.3492 33.5691 2 -24 0 4 535.535 62.2456 2 -24 0 3 18.1265 24.2613 2 -24 -1 8 96.2258 34.4057 2 -24 -1 7 155.295 40.3504 2 -24 -1 6 106.312 38.3821 2 -24 -1 5 46.8103 33.6780 2 -24 -1 4 90.3645 33.5623 2 -24 -1 3 220.484 43.1669 2 -24 -1 2 0.57850 26.0795 2 -24 -2 6 450.960 58.5531 2 -24 -2 5 33.9662 27.0618 2 -24 -2 4-14.1792 28.2295 2 -24 -2 3 538.774 61.8917 2 0 0 0 0.00 0.00 0 TITL MRC2160 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 19.433017 17.404892 30.893112 90.0000 96.4115 90.0000 ZERR 4.00 0.000240 0.000178 0.000438 0.0000 0.0012 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Mg Cr UNIT 392.00 560.00 24.00 20.00 12.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 70405 #===END ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3h _database_code_depnum_ccdc_archive 'CCDC 2116009' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT342_3h ; PROBLEM: Low Bond Precision on C-C Bonds ............... 0.0315 Ang. RESPONSE: The crystal was small and weakly diffracting. Bond precision on solvate molecule made no significant effect on key atomic metrics. ; _vrf_PLAT910_3h ; PROBLEM: Missing # of FCF Reflection(s) Below Theta(Min). 12 Note RESPONSE: The crystal was small and weakly diffracting ; # Added during the CSD deposition process: Friday 15 October 2021 05:10 PM # end Validation Reply Form _audit_creation_method SHELXL-2018/3 _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C70 H99 Ir Mg2 N4 O2, 1.5(C6 H14)' _chemical_formula_sum 'C79 H120 Ir Mg2 N4 O2' _chemical_formula_weight 1398.60 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -1.4442 7.9887 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 14.0273(6) _cell_length_b 13.9062(6) _cell_length_c 40.2048(14) _cell_angle_alpha 90 _cell_angle_beta 99.779(4) _cell_angle_gamma 90 _cell_volume 7728.7(5) _cell_formula_units_Z 4 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 7032 _cell_measurement_theta_min 2.9280 _cell_measurement_theta_max 27.4090 _exptl_crystal_description tablets _exptl_crystal_colour 'Pale yellow' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.202 _exptl_crystal_F_000 2956 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.542 _exptl_crystal_size_mid 0.418 _exptl_crystal_size_min 0.174 _exptl_absorpt_coefficient_mu 1.788 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type analytical _exptl_absorpt_correction_T_min 0.476 _exptl_absorpt_correction_T_max 0.759 _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'Enhance (Mo) X-ray Source' _diffrn_measurement_device_type 'Agilent Xcalibur 3 E' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean 16.0382 _diffrn_reflns_number 16394 _diffrn_reflns_av_unetI/netI 0.1238 _diffrn_reflns_av_R_equivalents 0.0663 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -52 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_theta_min 2.307 _diffrn_reflns_theta_max 28.165 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.810 _diffrn_measured_fraction_theta_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.810 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.810 _diffrn_reflns_point_group_measured_fraction_full 0.991 _reflns_number_total 16394 _reflns_number_gt 11538 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. Completness statistics refer to single and composite reflections containing twin component 1 only. ; _computing_data_collection 'CrysAlisPro, Rigaku OD' _computing_cell_refinement 'CrysAlisPro, Rigaku OD' _computing_data_reduction 'CrysAlisPro, Rigaku OD' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2017)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2017)' _refine_special_details ; Refined as a 2-component twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0465P)^2^+289.9742P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 16394 _refine_ls_number_parameters 890 _refine_ls_number_restraints 1091 _refine_ls_R_factor_all 0.1545 _refine_ls_R_factor_gt 0.1271 _refine_ls_wR_factor_ref 0.3310 _refine_ls_wR_factor_gt 0.3227 _refine_ls_goodness_of_fit_ref 1.266 _refine_ls_restrained_S_all 1.232 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ir1 Ir 0.33857(6) 0.35154(7) 0.05978(2) 0.0327(2) Uani 1 1 d . . . . . Mg1 Mg 0.5932(4) 0.2534(4) 0.14042(14) 0.0155(13) Uani 1 1 d . . . . . Mg2 Mg 0.4342(4) 0.4102(4) 0.17156(14) 0.0149(12) Uani 1 1 d . . . . . H1 H 0.538(12) 0.333(13) 0.168(4) 0.022 Uiso 1 1 d . U . . . N1 N 0.7385(9) 0.2526(10) 0.1598(3) 0.010(3) Uani 1 1 d . U . . . C1 C 0.7815(13) 0.1746(13) 0.1736(4) 0.023(4) Uani 1 1 d . . . . . C2 C 0.7391(14) 0.0817(15) 0.1724(5) 0.024(4) Uani 1 1 d . U . . . H2A H 0.773810 0.034410 0.186607 0.029 Uiso 1 1 calc R U . . . C3 C 0.6501(16) 0.0508(15) 0.1523(5) 0.027(4) Uani 1 1 d . U . . . N3 N 0.5887(10) 0.1078(11) 0.1346(4) 0.019(3) Uani 1 1 d . . . . . C4 C 0.8848(15) 0.1754(17) 0.1925(6) 0.045(6) Uani 1 1 d . . . . . H4A H 0.927360 0.145349 0.178549 0.067 Uiso 1 1 calc R U . . . H4B H 0.888287 0.139317 0.213645 0.067 Uiso 1 1 calc R U . . . H4C H 0.905435 0.241856 0.197580 0.067 Uiso 1 1 calc R U . . . C5 C 0.6412(19) -0.0586(15) 0.1508(6) 0.047(6) Uani 1 1 d . . . . . H5A H 0.592728 -0.079389 0.164259 0.070 Uiso 1 1 calc R U . . . H5B H 0.703807 -0.087600 0.159992 0.070 Uiso 1 1 calc R U . . . H5C H 0.621210 -0.078990 0.127366 0.070 Uiso 1 1 calc R U . . . C6 C 0.7946(11) 0.3389(15) 0.1602(4) 0.023(4) Uani 1 1 d . . . . . C7 C 0.8393(11) 0.3603(17) 0.1318(5) 0.029(5) Uani 1 1 d D . . . . C8 C 0.8935(13) 0.4435(17) 0.1321(5) 0.030(5) Uani 1 1 d . . . . . H8A H 0.924426 0.456956 0.113381 0.036 Uiso 1 1 calc R U . . . C9 C 0.9042(14) 0.5077(16) 0.1587(5) 0.032(5) Uani 1 1 d . . . . . H9A H 0.943824 0.563139 0.158706 0.039 Uiso 1 1 calc R U . . . C10 C 0.8562(14) 0.4895(15) 0.1851(5) 0.030(5) Uani 1 1 d . . . . . H10A H 0.860698 0.535134 0.202841 0.036 Uiso 1 1 calc R U . . . C11 C 0.8003(11) 0.4055(14) 0.1868(4) 0.019(4) Uani 1 1 d . . . . . C12 C 0.834(2) 0.290(2) 0.1029(7) 0.041(8) Uani 0.59(4) 1 d D U P A 1 H12A H 0.791267 0.236420 0.107951 0.049 Uiso 0.59(4) 1 calc R U P A 1 C13 C 0.784(3) 0.335(3) 0.0700(7) 0.030(8) Uani 0.59(4) 1 d D U P A 1 H13A H 0.781287 0.288028 0.051721 0.045 Uiso 0.59(4) 1 calc R U P A 1 H13B H 0.717960 0.353923 0.072275 0.045 Uiso 0.59(4) 1 calc R U P A 1 H13C H 0.820091 0.391775 0.064914 0.045 Uiso 0.59(4) 1 calc R U P A 1 C14 C 0.932(3) 0.246(4) 0.1009(12) 0.053(11) Uani 0.59(4) 1 d D U P A 1 H14A H 0.924844 0.200817 0.081852 0.080 Uiso 0.59(4) 1 calc R U P A 1 H14B H 0.977533 0.296497 0.097663 0.080 Uiso 0.59(4) 1 calc R U P A 1 H14C H 0.955301 0.211066 0.121895 0.080 Uiso 0.59(4) 1 calc R U P A 1 C12' C 0.826(4) 0.294(3) 0.1018(8) 0.044(10) Uiso 0.41(4) 1 d D U P A 2 H12B H 0.758090 0.268118 0.098407 0.053 Uiso 0.41(4) 1 calc R U P A 2 C13' C 0.835(4) 0.359(3) 0.0723(10) 0.023(9) Uiso 0.41(4) 1 d D U P A 2 H13D H 0.827422 0.321191 0.051460 0.034 Uiso 0.41(4) 1 calc R U P A 2 H13E H 0.785423 0.408987 0.070272 0.034 Uiso 0.41(4) 1 calc R U P A 2 H13F H 0.899437 0.389175 0.076182 0.034 Uiso 0.41(4) 1 calc R U P A 2 C14' C 0.895(5) 0.209(4) 0.1054(17) 0.051(13) Uiso 0.41(4) 1 d D U P A 2 H14D H 0.881795 0.168770 0.085002 0.077 Uiso 0.41(4) 1 calc R U P A 2 H14E H 0.961728 0.232220 0.108379 0.077 Uiso 0.41(4) 1 calc R U P A 2 H14F H 0.886053 0.170161 0.125029 0.077 Uiso 0.41(4) 1 calc R U P A 2 C15 C 0.7519(14) 0.3891(15) 0.2178(4) 0.025(4) Uani 1 1 d . . . . . H15A H 0.708802 0.331596 0.213169 0.030 Uiso 1 1 calc R U . . . C16 C 0.8255(18) 0.368(2) 0.2486(5) 0.055(7) Uani 1 1 d . . . . . H16A H 0.859155 0.308096 0.245308 0.082 Uiso 1 1 calc R U . . . H16B H 0.792918 0.361887 0.268208 0.082 Uiso 1 1 calc R U . . . H16C H 0.872349 0.420963 0.252397 0.082 Uiso 1 1 calc R U . . . C17 C 0.6903(13) 0.4732(17) 0.2249(5) 0.035(5) Uani 1 1 d . . . . . H17A H 0.731760 0.529338 0.231182 0.053 Uiso 1 1 calc R U . . . H17B H 0.656105 0.456848 0.243405 0.053 Uiso 1 1 calc R U . . . H17C H 0.643241 0.488172 0.204597 0.053 Uiso 1 1 calc R U . . . C18 C 0.5158(14) 0.0656(14) 0.1091(5) 0.025(4) Uani 1 1 d . U . . . C19 C 0.4239(15) 0.0416(16) 0.1167(5) 0.032(5) Uani 1 1 d D . . . . C20 C 0.351(2) 0.003(2) 0.0902(6) 0.057(8) Uani 1 1 d . . . . . H20A H 0.287095 -0.009485 0.093632 0.069 Uiso 1 1 calc R U . . . C21 C 0.3809(14) -0.0155(16) 0.0584(6) 0.033(5) Uani 1 1 d . U . . . H21A H 0.336337 -0.044639 0.040879 0.040 Uiso 1 1 calc R U . . . C22 C 0.4669(19) 0.006(2) 0.0528(7) 0.067(9) Uani 1 1 d . . . . . H22A H 0.482465 -0.006768 0.031164 0.080 Uiso 1 1 calc R U . . . C23 C 0.5364(16) 0.0476(18) 0.0768(5) 0.039(5) Uani 1 1 d D U . . . C24 C 0.400(3) 0.053(2) 0.1526(6) 0.028(7) Uani 0.62(4) 1 d D U P B 1 H24A H 0.461470 0.069055 0.168319 0.034 Uiso 0.62(4) 1 calc R U P B 1 C25 C 0.359(3) -0.038(3) 0.1651(9) 0.044(9) Uani 0.62(4) 1 d D U P B 1 H25A H 0.405883 -0.090503 0.165659 0.066 Uiso 0.62(4) 1 calc R U P B 1 H25B H 0.344783 -0.027331 0.187838 0.066 Uiso 0.62(4) 1 calc R U P B 1 H25C H 0.299182 -0.055274 0.149848 0.066 Uiso 0.62(4) 1 calc R U P B 1 C26 C 0.332(4) 0.137(3) 0.1510(13) 0.067(13) Uani 0.62(4) 1 d D U P B 1 H26A H 0.362223 0.193807 0.142807 0.101 Uiso 0.62(4) 1 calc R U P B 1 H26B H 0.271967 0.121936 0.135605 0.101 Uiso 0.62(4) 1 calc R U P B 1 H26C H 0.317568 0.149879 0.173595 0.101 Uiso 0.62(4) 1 calc R U P B 1 C24' C 0.388(4) 0.078(4) 0.1487(10) 0.032(10) Uiso 0.38(4) 1 d D U P B 2 H24B H 0.432563 0.133103 0.156978 0.038 Uiso 0.38(4) 1 calc R U P B 2 C25' C 0.412(5) 0.001(5) 0.1751(16) 0.050(12) Uiso 0.38(4) 1 d D U P B 2 H25D H 0.478370 -0.022296 0.175167 0.074 Uiso 0.38(4) 1 calc R U P B 2 H25E H 0.407161 0.026857 0.197328 0.074 Uiso 0.38(4) 1 calc R U P B 2 H25F H 0.366795 -0.052789 0.169779 0.074 Uiso 0.38(4) 1 calc R U P B 2 C26' C 0.288(5) 0.118(6) 0.147(2) 0.069(15) Uiso 0.38(4) 1 d D U P B 2 H26D H 0.276303 0.168053 0.129423 0.103 Uiso 0.38(4) 1 calc R U P B 2 H26E H 0.240510 0.066222 0.141172 0.103 Uiso 0.38(4) 1 calc R U P B 2 H26F H 0.280875 0.145868 0.168721 0.103 Uiso 0.38(4) 1 calc R U P B 2 C27 C 0.639(2) 0.054(4) 0.0693(13) 0.053(7) Uani 0.51(7) 1 d D U P C 1 H27A H 0.683062 0.076574 0.090153 0.063 Uiso 0.51(7) 1 calc R U P C 1 C28 C 0.638(5) 0.129(4) 0.0420(15) 0.058(8) Uani 0.51(7) 1 d D U P C 1 H28A H 0.613546 0.189665 0.049387 0.087 Uiso 0.51(7) 1 calc R U P C 1 H28B H 0.704404 0.138343 0.037643 0.087 Uiso 0.51(7) 1 calc R U P C 1 H28C H 0.596847 0.106894 0.021346 0.087 Uiso 0.51(7) 1 calc R U P C 1 C29 C 0.678(4) -0.040(5) 0.0579(15) 0.057(8) Uani 0.51(7) 1 d D U P C 1 H29A H 0.678333 -0.088315 0.075613 0.086 Uiso 0.51(7) 1 calc R U P C 1 H29B H 0.636142 -0.061611 0.037215 0.086 Uiso 0.51(7) 1 calc R U P C 1 H29C H 0.743700 -0.030161 0.053512 0.086 Uiso 0.51(7) 1 calc R U P C 1 C27' C 0.630(3) 0.087(4) 0.0672(12) 0.050(8) Uiso 0.49(7) 1 d D U P C 2 H27B H 0.659773 0.131148 0.085798 0.060 Uiso 0.49(7) 1 calc R U P C 2 C28' C 0.613(5) 0.144(4) 0.0348(15) 0.061(9) Uiso 0.49(7) 1 d D U P C 2 H28D H 0.567872 0.196905 0.036556 0.091 Uiso 0.49(7) 1 calc R U P C 2 H28E H 0.675173 0.171336 0.030869 0.091 Uiso 0.49(7) 1 calc R U P C 2 H28F H 0.586902 0.102309 0.015980 0.091 Uiso 0.49(7) 1 calc R U P C 2 C29' C 0.700(4) 0.006(5) 0.0647(15) 0.058(9) Uiso 0.49(7) 1 d D U P C 2 H29D H 0.710056 -0.030497 0.085799 0.086 Uiso 0.49(7) 1 calc R U P C 2 H29E H 0.673351 -0.035953 0.045920 0.086 Uiso 0.49(7) 1 calc R U P C 2 H29F H 0.761621 0.033074 0.060809 0.086 Uiso 0.49(7) 1 calc R U P C 2 N31 N 0.4043(10) 0.3962(10) 0.2191(3) 0.016(2) Uani 1 1 d . U . . . C31 C 0.4176(11) 0.4674(12) 0.2415(4) 0.012(3) Uani 1 1 d . U . . . C32 C 0.4478(11) 0.5596(12) 0.2337(4) 0.014(3) Uani 1 1 d . U . . . H32A H 0.473025 0.598368 0.252583 0.017 Uiso 1 1 calc R U . . . C33 C 0.4464(12) 0.6044(13) 0.2014(4) 0.017(3) Uani 1 1 d . U . . . N33 N 0.4353(10) 0.5569(11) 0.1727(4) 0.018(2) Uani 1 1 d . U . . . C34 C 0.4033(13) 0.4551(14) 0.2779(4) 0.019(3) Uani 1 1 d . U . . . H34A H 0.334087 0.458100 0.279014 0.029 Uiso 1 1 calc R U . . . H34B H 0.437268 0.506676 0.291726 0.029 Uiso 1 1 calc R U . . . H34C H 0.429232 0.392733 0.286400 0.029 Uiso 1 1 calc R U . . . C35 C 0.4651(13) 0.7120(14) 0.2041(5) 0.024(3) Uani 1 1 d . U . . . H35A H 0.471570 0.737551 0.181873 0.036 Uiso 1 1 calc R U . . . H35B H 0.524820 0.724058 0.220063 0.036 Uiso 1 1 calc R U . . . H35C H 0.410816 0.743767 0.212087 0.036 Uiso 1 1 calc R U . . . C36 C 0.3694(12) 0.3058(13) 0.2301(4) 0.019(3) Uani 1 1 d . U . . . C37 C 0.2695(13) 0.2871(15) 0.2244(5) 0.025(3) Uani 1 1 d . U . . . C38 C 0.2388(15) 0.2001(15) 0.2358(5) 0.030(4) Uani 1 1 d . U . . . H38A H 0.171375 0.186788 0.232146 0.036 Uiso 1 1 calc R U . . . C39 C 0.3013(15) 0.1324(15) 0.2521(5) 0.032(4) Uani 1 1 d . U . . . H39A H 0.277782 0.074908 0.260617 0.039 Uiso 1 1 calc R U . . . C40 C 0.3998(14) 0.1505(17) 0.2558(5) 0.033(3) Uani 1 1 d . U . . . H40A H 0.443749 0.102805 0.265994 0.040 Uiso 1 1 calc R U . . . C41 C 0.4369(14) 0.2362(14) 0.2450(5) 0.026(3) Uani 1 1 d . U . . . C42 C 0.1945(12) 0.3576(16) 0.2069(5) 0.027(3) Uani 1 1 d . U . . . H42A H 0.228968 0.417721 0.202082 0.032 Uiso 1 1 calc R U . . . C43 C 0.1452(15) 0.3160(16) 0.1733(5) 0.035(4) Uani 1 1 d . U . . . H43A H 0.192477 0.309370 0.158145 0.053 Uiso 1 1 calc R U . . . H43B H 0.092949 0.358981 0.163151 0.053 Uiso 1 1 calc R U . . . H43C H 0.118232 0.252657 0.177154 0.053 Uiso 1 1 calc R U . . . C44 C 0.1190(14) 0.3847(16) 0.2296(6) 0.032(4) Uani 1 1 d . U . . . H44A H 0.076609 0.329603 0.231343 0.049 Uiso 1 1 calc R U . . . H44B H 0.080219 0.439380 0.219677 0.049 Uiso 1 1 calc R U . . . H44C H 0.152819 0.402223 0.252196 0.049 Uiso 1 1 calc R U . . . C45 C 0.5439(13) 0.2507(15) 0.2495(5) 0.026(3) Uani 1 1 d . U . . . H45A H 0.555514 0.312762 0.238311 0.032 Uiso 1 1 calc R U . . . C46 C 0.5923(16) 0.2589(16) 0.2876(5) 0.035(4) Uani 1 1 d . U . . . H46A H 0.566675 0.315485 0.297638 0.053 Uiso 1 1 calc R U . . . H46B H 0.662453 0.265495 0.289138 0.053 Uiso 1 1 calc R U . . . H46C H 0.577917 0.201019 0.299692 0.053 Uiso 1 1 calc R U . . . C47 C 0.5921(14) 0.1715(15) 0.2322(5) 0.033(4) Uani 1 1 d . U . . . H47A H 0.580945 0.109363 0.242364 0.050 Uiso 1 1 calc R U . . . H47B H 0.661762 0.183898 0.235003 0.050 Uiso 1 1 calc R U . . . H47C H 0.564592 0.170380 0.208118 0.050 Uiso 1 1 calc R U . . . C48 C 0.4136(13) 0.6122(15) 0.1417(5) 0.027(3) Uani 1 1 d . U . . . C49 C 0.4836(15) 0.6220(15) 0.1212(5) 0.033(3) Uani 1 1 d . U . . . C50 C 0.4577(16) 0.6746(16) 0.0918(6) 0.041(4) Uani 1 1 d . U . . . H50A H 0.505084 0.684463 0.077833 0.049 Uiso 1 1 calc R U . . . C51 C 0.3675(16) 0.7132(17) 0.0818(6) 0.038(4) Uani 1 1 d . U . . . H51A H 0.351851 0.746783 0.060960 0.046 Uiso 1 1 calc R U . . . C52 C 0.3010(16) 0.7019(17) 0.1026(6) 0.038(4) Uani 1 1 d . U . . . H52A H 0.238778 0.730092 0.096392 0.045 Uiso 1 1 calc R U . . . C53 C 0.3213(14) 0.6503(18) 0.1327(5) 0.037(3) Uani 1 1 d . U . . . C54 C 0.5836(15) 0.5827(17) 0.1308(6) 0.037(4) Uani 1 1 d . U . . . H54A H 0.581565 0.531185 0.148025 0.044 Uiso 1 1 calc R U . . . C55 C 0.6538(17) 0.659(2) 0.1465(6) 0.053(5) Uani 1 1 d . U . . . H55A H 0.650239 0.714443 0.131425 0.080 Uiso 1 1 calc R U . . . H55B H 0.719623 0.632563 0.150137 0.080 Uiso 1 1 calc R U . . . H55C H 0.637211 0.678654 0.168217 0.080 Uiso 1 1 calc R U . . . C56 C 0.6244(17) 0.5388(18) 0.1015(6) 0.047(4) Uani 1 1 d . U . . . H56A H 0.577710 0.493027 0.089548 0.070 Uiso 1 1 calc R U . . . H56B H 0.685028 0.505344 0.110216 0.070 Uiso 1 1 calc R U . . . H56C H 0.636844 0.589847 0.086015 0.070 Uiso 1 1 calc R U . . . C57 C 0.2420(13) 0.6395(17) 0.1553(5) 0.035(4) Uani 1 1 d . U . . . H57A H 0.273741 0.614302 0.177770 0.042 Uiso 1 1 calc R U . . . C58 C 0.1695(16) 0.5681(19) 0.1401(7) 0.049(5) Uani 1 1 d . U . . . H58A H 0.143667 0.586772 0.116850 0.073 Uiso 1 1 calc R U . . . H58B H 0.116731 0.565435 0.153256 0.073 Uiso 1 1 calc R U . . . H58C H 0.200049 0.504674 0.140247 0.073 Uiso 1 1 calc R U . . . C59 C 0.1895(17) 0.7335(19) 0.1613(6) 0.048(5) Uani 1 1 d . U . . . H59A H 0.236562 0.780397 0.172389 0.073 Uiso 1 1 calc R U . . . H59B H 0.141177 0.720535 0.175687 0.073 Uiso 1 1 calc R U . . . H59C H 0.157334 0.759405 0.139594 0.073 Uiso 1 1 calc R U . . . C60 C 0.463(2) 0.318(2) 0.0790(9) 0.041(8) Uani 0.74(4) 1 d D U P D 1 C61 C 0.313(3) 0.372(3) 0.1016(7) 0.051(9) Uani 0.74(4) 1 d D U P D 1 H61A H 0.246669 0.388937 0.098178 0.061 Uiso 0.74(4) 1 calc R U P D 1 C60' C 0.507(7) 0.324(6) 0.0654(11) 0.041(12) Uiso 0.26(4) 1 d D U P D 2 H60B H 0.546042 0.328986 0.048190 0.049 Uiso 0.26(4) 1 calc R U P D 2 C61' C 0.358(8) 0.355(9) 0.1077(17) 0.050(13) Uiso 0.26(4) 1 d D U P D 2 O60 O 0.5352(9) 0.3023(10) 0.0962(3) 0.026(3) Uani 1 1 d D U . . . O61 O 0.3400(10) 0.3755(11) 0.1333(3) 0.038(4) Uani 1 1 d D . . . . C62 C 0.3199(17) 0.3254(19) 0.0029(5) 0.047(4) Uani 1 1 d . U . . . C63 C 0.3047(19) 0.428(2) 0.0080(6) 0.050(4) Uani 1 1 d . U . . . C64 C 0.2201(19) 0.439(2) 0.0233(6) 0.056(4) Uani 1 1 d . U . . . C65 C 0.1870(17) 0.344(2) 0.0282(6) 0.054(4) Uani 1 1 d . U . . . C66 C 0.2470(18) 0.273(2) 0.0149(6) 0.048(4) Uani 1 1 d . U . . . C67 C 0.3978(18) 0.282(2) -0.0153(6) 0.056(5) Uani 1 1 d . U . . . H67A H 0.456059 0.321660 -0.011111 0.084 Uiso 1 1 calc R U . . . H67B H 0.373408 0.278571 -0.039562 0.084 Uiso 1 1 calc R U . . . H67C H 0.413520 0.216568 -0.006619 0.084 Uiso 1 1 calc R U . . . C68 C 0.357(2) 0.514(2) -0.0018(7) 0.064(6) Uani 1 1 d . U . . . H68A H 0.423655 0.514208 0.010725 0.097 Uiso 1 1 calc R U . . . H68B H 0.324049 0.572712 0.003383 0.097 Uiso 1 1 calc R U . . . H68C H 0.358963 0.511775 -0.026108 0.097 Uiso 1 1 calc R U . . . C69 C 0.179(2) 0.539(2) 0.0298(7) 0.068(6) Uani 1 1 d . U . . . H69A H 0.126905 0.556076 0.011146 0.103 Uiso 1 1 calc R U . . . H69B H 0.230282 0.587665 0.031473 0.103 Uiso 1 1 calc R U . . . H69C H 0.152848 0.537955 0.050966 0.103 Uiso 1 1 calc R U . . . C70 C 0.0944(18) 0.316(2) 0.0426(7) 0.066(6) Uani 1 1 d . U . . . H70A H 0.102409 0.251927 0.052688 0.099 Uiso 1 1 calc R U . . . H70B H 0.038357 0.316557 0.024404 0.099 Uiso 1 1 calc R U . . . H70C H 0.084250 0.362999 0.059947 0.099 Uiso 1 1 calc R U . . . C71 C 0.2338(19) 0.165(2) 0.0130(6) 0.060(5) Uani 1 1 d . U . . . H71A H 0.191106 0.145112 0.028606 0.089 Uiso 1 1 calc R U . . . H71B H 0.296745 0.133679 0.019070 0.089 Uiso 1 1 calc R U . . . H71C H 0.204773 0.147120 -0.010104 0.089 Uiso 1 1 calc R U . . . C81 C 0.358(2) 0.320(2) 0.4787(7) 0.069(9) Uani 1 1 d . . . . . H81A H 0.337820 0.342922 0.455543 0.103 Uiso 1 1 calc R U . . . H81B H 0.302063 0.294790 0.487426 0.103 Uiso 1 1 calc R U . . . H81C H 0.406599 0.269203 0.478984 0.103 Uiso 1 1 calc R U . . . C82 C 0.402(2) 0.403(3) 0.5008(8) 0.074(9) Uani 1 1 d . . . . . H82A H 0.348252 0.445711 0.504723 0.088 Uiso 1 1 calc R U . . . H82B H 0.431355 0.376371 0.522987 0.088 Uiso 1 1 calc R U . . . C83 C 0.4734(19) 0.462(2) 0.4890(8) 0.063(8) Uani 1 1 d . . . . . H83A H 0.441191 0.494149 0.468064 0.076 Uiso 1 1 calc R U . . . H83B H 0.522515 0.418105 0.482358 0.076 Uiso 1 1 calc R U . . . C91 C 1.048(6) 0.997(4) 0.118(2) 0.112(17) Uani 0.66(4) 1 d D U P E 1 H91A H 1.062683 1.039698 0.137815 0.169 Uiso 0.66(4) 1 calc R U P E 1 H91B H 1.107944 0.966639 0.113971 0.169 Uiso 0.66(4) 1 calc R U P E 1 H91C H 1.019248 1.034307 0.098391 0.169 Uiso 0.66(4) 1 calc R U P E 1 C92 C 0.979(4) 0.922(3) 0.1251(12) 0.089(16) Uani 0.66(4) 1 d D U P E 1 H92A H 1.009062 0.887143 0.145788 0.107 Uiso 0.66(4) 1 calc R U P E 1 H92B H 0.920847 0.954444 0.130293 0.107 Uiso 0.66(4) 1 calc R U P E 1 C93 C 0.946(3) 0.848(3) 0.0989(8) 0.065(11) Uani 0.66(4) 1 d D U P E 1 H93A H 0.907425 0.881760 0.079465 0.078 Uiso 0.66(4) 1 calc R U P E 1 H93B H 1.004681 0.822916 0.090994 0.078 Uiso 0.66(4) 1 calc R U P E 1 C94 C 0.889(3) 0.765(3) 0.1070(9) 0.084(19) Uani 0.66(4) 1 d D . P E 1 H94A H 0.929452 0.729704 0.125855 0.101 Uiso 0.66(4) 1 calc R U P E 1 H94B H 0.832480 0.789952 0.115726 0.101 Uiso 0.66(4) 1 calc R U P E 1 C95 C 0.854(3) 0.693(3) 0.0807(12) 0.086(15) Uani 0.66(4) 1 d D U P E 1 H95A H 0.818146 0.643402 0.091276 0.104 Uiso 0.66(4) 1 calc R U P E 1 H95B H 0.805742 0.725991 0.063525 0.104 Uiso 0.66(4) 1 calc R U P E 1 C96 C 0.922(4) 0.642(4) 0.0625(16) 0.091(14) Uani 0.66(4) 1 d D U P E 1 H96A H 0.885736 0.597996 0.046058 0.136 Uiso 0.66(4) 1 calc R U P E 1 H96B H 0.956013 0.689436 0.050716 0.136 Uiso 0.66(4) 1 calc R U P E 1 H96C H 0.968498 0.606311 0.078646 0.136 Uiso 0.66(4) 1 calc R U P E 1 C91' C 1.027(9) 0.981(8) 0.115(5) 0.112(19) Uiso 0.34(4) 1 d D U P E 2 H91F H 1.030764 1.050841 0.118324 0.167 Uiso 0.34(4) 1 calc R U P E 2 H91G H 1.079079 0.950308 0.131152 0.167 Uiso 0.34(4) 1 calc R U P E 2 H91H H 1.034135 0.964721 0.092147 0.167 Uiso 0.34(4) 1 calc R U P E 2 C92' C 0.933(7) 0.946(5) 0.122(3) 0.091(19) Uiso 0.34(4) 1 d D U P E 2 H91D H 0.881821 0.980750 0.106284 0.109 Uiso 0.34(4) 1 calc R U P E 2 H91E H 0.926486 0.966426 0.145048 0.109 Uiso 0.34(4) 1 calc R U P E 2 C93' C 0.909(7) 0.843(5) 0.119(2) 0.10(4) Uiso 0.34(4) 1 d D . P E 2 H93C H 0.837629 0.836748 0.116861 0.121 Uiso 0.34(4) 1 calc R U P E 2 H93D H 0.937045 0.812127 0.140748 0.121 Uiso 0.34(4) 1 calc R U P E 2 C94' C 0.939(6) 0.784(4) 0.0918(19) 0.060(14) Uiso 0.34(4) 1 d D U P E 2 H94C H 0.924054 0.822457 0.070779 0.072 Uiso 0.34(4) 1 calc R U P E 2 H94D H 1.009753 0.777299 0.097124 0.072 Uiso 0.34(4) 1 calc R U P E 2 C95' C 0.898(7) 0.687(5) 0.084(3) 0.088(18) Uiso 0.34(4) 1 d D U P E 2 H95C H 0.828752 0.695608 0.074136 0.106 Uiso 0.34(4) 1 calc R U P E 2 H95D H 0.899230 0.653902 0.106050 0.106 Uiso 0.34(4) 1 calc R U P E 2 C96' C 0.941(10) 0.622(7) 0.062(3) 0.089(16) Uiso 0.34(4) 1 d D U P E 2 H96D H 0.905242 0.560915 0.059668 0.133 Uiso 0.34(4) 1 calc R U P E 2 H96E H 0.937831 0.651399 0.039706 0.133 Uiso 0.34(4) 1 calc R U P E 2 H96F H 1.008752 0.609430 0.071820 0.133 Uiso 0.34(4) 1 calc R U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir1 0.0308(4) 0.0462(5) 0.0177(3) -0.0053(5) -0.0055(3) -0.0014(5) Mg1 0.012(3) 0.020(3) 0.012(3) -0.007(3) -0.005(2) 0.005(3) Mg2 0.021(3) 0.015(3) 0.010(3) 0.000(2) 0.006(2) 0.000(3) N1 0.011(4) 0.014(5) 0.006(4) -0.001(4) 0.000(4) 0.000(4) C1 0.021(9) 0.027(11) 0.020(9) -0.013(8) 0.000(7) 0.010(8) C2 0.032(8) 0.027(8) 0.015(7) -0.007(6) 0.011(6) 0.005(7) C3 0.043(8) 0.023(8) 0.015(7) -0.004(6) 0.003(7) 0.002(7) N3 0.020(8) 0.018(8) 0.020(8) 0.004(7) 0.004(6) 0.004(7) C4 0.036(12) 0.041(15) 0.049(14) 0.009(11) -0.018(10) 0.012(11) C5 0.055(14) 0.017(11) 0.062(16) -0.008(11) -0.005(13) 0.009(12) C6 0.014(8) 0.030(11) 0.022(9) -0.007(9) 0.000(6) 0.000(9) C7 0.007(7) 0.046(13) 0.034(10) -0.014(11) 0.006(7) -0.004(10) C8 0.015(9) 0.053(14) 0.025(10) 0.001(10) 0.010(7) -0.002(10) C9 0.025(10) 0.041(13) 0.030(11) -0.003(10) 0.002(8) -0.005(10) C10 0.035(11) 0.028(12) 0.027(11) -0.016(9) 0.004(9) -0.001(10) C11 0.007(8) 0.033(11) 0.018(9) 0.000(8) 0.003(6) 0.002(8) C12 0.047(16) 0.045(16) 0.034(14) -0.017(14) 0.017(13) -0.014(15) C13 0.037(15) 0.041(16) 0.016(12) -0.011(12) 0.018(11) -0.025(14) C14 0.062(19) 0.049(19) 0.046(17) -0.015(16) 0.003(15) 0.006(16) C15 0.028(10) 0.028(11) 0.017(9) -0.003(8) -0.001(8) 0.000(9) C16 0.058(15) 0.08(2) 0.026(11) 0.007(13) 0.005(10) 0.019(16) C17 0.016(9) 0.054(15) 0.037(12) -0.009(11) 0.010(8) 0.005(10) C18 0.029(8) 0.021(8) 0.023(7) -0.014(6) 0.002(6) -0.001(7) C19 0.043(12) 0.033(12) 0.018(10) -0.001(9) 0.001(9) -0.013(11) C20 0.071(18) 0.062(18) 0.050(16) -0.006(14) 0.039(14) -0.032(16) C21 0.028(6) 0.038(6) 0.034(6) -0.002(5) 0.003(5) -0.009(5) C22 0.050(15) 0.09(2) 0.053(16) -0.049(16) -0.013(13) -0.014(16) C23 0.041(9) 0.045(9) 0.030(8) -0.016(8) 0.004(7) 0.000(8) C24 0.033(10) 0.029(11) 0.023(10) 0.004(8) 0.004(8) 0.000(8) C25 0.054(17) 0.050(17) 0.032(15) 0.011(14) 0.019(13) -0.016(15) C26 0.08(2) 0.06(2) 0.065(18) -0.013(17) 0.010(17) 0.003(18) C27 0.053(11) 0.057(11) 0.049(11) -0.004(10) 0.009(9) 0.003(10) C28 0.054(13) 0.061(13) 0.059(13) -0.001(12) 0.007(12) 0.003(12) C29 0.056(13) 0.057(14) 0.058(13) -0.005(12) 0.007(12) 0.004(12) N31 0.016(5) 0.017(5) 0.017(5) -0.001(5) 0.003(4) 0.002(5) C31 0.010(4) 0.015(4) 0.010(4) -0.002(4) 0.002(4) 0.003(4) C32 0.012(5) 0.018(6) 0.011(5) -0.004(5) -0.001(5) 0.003(5) C33 0.013(6) 0.020(6) 0.020(6) 0.003(6) 0.006(5) 0.006(6) N33 0.014(5) 0.022(5) 0.020(5) 0.004(5) 0.008(4) 0.003(5) C34 0.022(6) 0.022(6) 0.013(6) -0.001(6) 0.002(5) 0.002(6) C35 0.021(6) 0.019(6) 0.030(6) 0.000(6) 0.004(6) -0.001(6) C36 0.022(4) 0.019(4) 0.017(4) 0.000(4) 0.008(4) -0.001(4) C37 0.026(6) 0.025(6) 0.026(6) 0.000(6) 0.009(5) -0.002(6) C38 0.034(7) 0.022(7) 0.037(7) -0.003(7) 0.012(6) -0.004(7) C39 0.041(7) 0.022(8) 0.036(7) 0.005(7) 0.014(7) -0.001(7) C40 0.039(7) 0.027(7) 0.034(7) 0.005(7) 0.007(6) 0.002(7) C41 0.027(6) 0.025(6) 0.026(6) 0.004(6) 0.003(6) 0.003(6) C42 0.022(6) 0.026(7) 0.034(7) 0.002(7) 0.009(6) -0.003(7) C43 0.023(8) 0.044(9) 0.037(9) -0.001(8) 0.002(7) -0.005(8) C44 0.020(7) 0.031(8) 0.045(9) -0.004(7) 0.001(7) -0.004(7) C45 0.030(7) 0.026(7) 0.023(7) 0.010(6) 0.005(6) 0.004(6) C46 0.040(9) 0.037(9) 0.026(8) 0.004(8) -0.003(8) 0.011(8) C47 0.031(8) 0.033(9) 0.036(9) 0.009(8) 0.008(7) 0.014(8) C48 0.025(6) 0.029(6) 0.029(6) 0.009(6) 0.011(5) 0.005(6) C49 0.032(6) 0.036(7) 0.034(6) 0.014(6) 0.012(6) 0.005(6) C50 0.041(7) 0.042(8) 0.043(7) 0.014(7) 0.015(6) 0.005(7) C51 0.039(7) 0.040(7) 0.038(7) 0.017(6) 0.011(6) 0.008(6) C52 0.035(7) 0.040(8) 0.040(7) 0.016(7) 0.010(7) 0.012(7) C53 0.035(6) 0.038(7) 0.038(6) 0.014(6) 0.007(6) 0.006(6) C54 0.036(6) 0.040(7) 0.038(6) 0.010(6) 0.018(6) 0.004(6) C55 0.045(9) 0.056(10) 0.058(10) -0.001(10) 0.007(8) 0.011(10) C56 0.044(8) 0.048(9) 0.052(9) 0.005(8) 0.016(8) 0.003(8) C57 0.030(7) 0.039(8) 0.038(7) 0.017(7) 0.014(6) 0.010(7) C58 0.035(9) 0.054(11) 0.057(10) 0.009(9) 0.008(9) 0.006(9) C59 0.041(9) 0.054(10) 0.048(10) 0.015(9) 0.001(9) 0.010(9) C60 0.044(15) 0.032(14) 0.049(15) 0.011(12) 0.014(13) -0.018(12) C61 0.077(18) 0.048(16) 0.017(11) 0.007(12) -0.025(12) -0.004(15) O60 0.023(6) 0.041(7) 0.010(5) 0.003(5) -0.009(5) 0.003(5) O61 0.038(8) 0.053(11) 0.019(7) -0.009(7) 0.000(6) 0.000(7) C62 0.045(6) 0.063(7) 0.029(6) -0.001(6) -0.005(6) -0.003(6) C63 0.049(7) 0.064(7) 0.032(6) 0.003(6) -0.006(6) -0.002(6) C64 0.049(8) 0.075(8) 0.037(7) 0.001(8) -0.015(7) 0.003(8) C65 0.042(7) 0.077(8) 0.037(7) -0.004(8) -0.009(7) -0.001(8) C66 0.043(6) 0.065(7) 0.031(6) -0.004(6) -0.007(6) -0.004(6) C67 0.052(10) 0.079(11) 0.032(9) -0.006(9) -0.007(8) -0.002(10) C68 0.064(10) 0.077(11) 0.043(10) 0.015(10) -0.015(9) -0.006(10) C69 0.065(10) 0.078(10) 0.054(9) -0.005(9) -0.013(9) 0.010(9) C70 0.045(9) 0.091(11) 0.056(9) -0.002(9) -0.007(8) -0.008(9) C71 0.060(10) 0.075(11) 0.038(9) -0.008(10) -0.006(8) -0.014(10) C81 0.057(16) 0.10(3) 0.046(16) -0.014(16) 0.004(13) -0.006(17) C82 0.053(17) 0.10(3) 0.07(2) -0.01(2) 0.021(15) 0.003(18) C83 0.052(17) 0.07(2) 0.07(2) 0.005(16) 0.014(14) 0.012(15) C91 0.12(2) 0.11(2) 0.11(2) -0.004(19) 0.01(2) 0.006(19) C92 0.09(2) 0.10(2) 0.08(2) -0.003(18) 0.015(18) 0.010(18) C93 0.065(17) 0.07(2) 0.057(17) 0.013(17) 0.006(15) 0.003(17) C94 0.03(2) 0.16(6) 0.06(3) 0.01(3) 0.00(2) -0.02(3) C95 0.08(2) 0.10(2) 0.08(2) 0.018(18) 0.007(18) -0.008(18) C96 0.08(2) 0.09(2) 0.09(2) 0.004(19) -0.018(18) -0.008(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir1 C61 1.80(3) . ? Ir1 C60 1.85(3) . ? Ir1 C61' 1.90(7) . ? Ir1 C65 2.29(2) . ? Ir1 C62 2.29(2) . ? Ir1 C66 2.31(2) . ? Ir1 C63 2.32(2) . ? Ir1 C64 2.36(2) . ? Ir1 C60' 2.37(10) . ? Mg1 O60 1.949(13) . ? Mg1 N3 2.039(17) . ? Mg1 N1 2.056(13) . ? Mg1 Mg2 3.498(8) . ? Mg2 O61 1.911(14) . ? Mg2 N31 2.033(15) . ? Mg2 N33 2.041(17) . ? Mg2 C61' 2.72(8) . ? N1 C1 1.32(2) . ? N1 C6 1.43(2) . ? C1 C2 1.42(3) . ? C1 C4 1.52(3) . ? C2 C3 1.43(3) . ? C3 N3 1.29(2) . ? C3 C5 1.53(3) . ? N3 C18 1.44(2) . ? C6 C11 1.41(3) . ? C6 C7 1.42(3) . ? C7 C8 1.38(3) . ? C7 C12' 1.51(3) . ? C7 C12 1.51(3) . ? C8 C9 1.38(3) . ? C9 C10 1.37(3) . ? C10 C11 1.42(3) . ? C11 C15 1.53(2) . ? C12 C14 1.52(3) . ? C12 C13 1.52(3) . ? C12' C13' 1.52(3) . ? C12' C14' 1.52(3) . ? C15 C16 1.50(3) . ? C15 C17 1.51(3) . ? C18 C23 1.40(3) . ? C18 C19 1.42(3) . ? C19 C20 1.45(3) . ? C19 C24 1.54(3) . ? C19 C24' 1.54(3) . ? C20 C21 1.43(3) . ? C21 C22 1.30(3) . ? C22 C23 1.37(3) . ? C23 C27 1.53(4) . ? C23 C27' 1.53(4) . ? C24 C25 1.51(3) . ? C24 C26 1.51(3) . ? C24' C26' 1.51(3) . ? C24' C25' 1.51(3) . ? C27 C28 1.51(3) . ? C27 C29 1.51(3) . ? C27' C29' 1.51(3) . ? C27' C28' 1.51(3) . ? N31 C31 1.33(2) . ? N31 C36 1.45(2) . ? C31 C32 1.40(2) . ? C31 C34 1.52(2) . ? C32 C33 1.44(2) . ? C33 N33 1.31(2) . ? C33 C35 1.52(3) . ? N33 C48 1.45(2) . ? C36 C37 1.41(3) . ? C36 C41 1.41(3) . ? C37 C38 1.39(3) . ? C37 C42 1.52(3) . ? C38 C39 1.38(3) . ? C39 C40 1.39(3) . ? C40 C41 1.40(3) . ? C41 C45 1.49(3) . ? C42 C43 1.52(3) . ? C42 C44 1.56(3) . ? C45 C47 1.52(3) . ? C45 C46 1.57(3) . ? C48 C53 1.39(3) . ? C48 C49 1.39(3) . ? C49 C50 1.38(3) . ? C49 C54 1.49(3) . ? C50 C51 1.37(3) . ? C51 C52 1.37(3) . ? C52 C53 1.40(3) . ? C53 C57 1.56(3) . ? C54 C55 1.51(3) . ? C54 C56 1.52(3) . ? C57 C58 1.48(3) . ? C57 C59 1.54(3) . ? C60 O60 1.14(3) . ? C61 O61 1.27(3) . ? C60' O60 1.27(3) . ? C61' O61 1.14(4) . ? C62 C66 1.41(4) . ? C62 C63 1.46(4) . ? C62 C67 1.54(4) . ? C63 C64 1.44(4) . ? C63 C68 1.49(4) . ? C64 C65 1.43(4) . ? C64 C69 1.55(4) . ? C65 C66 1.46(4) . ? C65 C70 1.56(4) . ? C66 C71 1.51(4) . ? C81 C82 1.52(4) . ? C82 C83 1.44(4) . ? C83 C83 1.50(6) 3_666 ? C91 C92 1.48(2) . ? C92 C93 1.48(2) . ? C93 C94 1.48(2) . ? C94 C95 1.48(2) . ? C95 C96 1.47(2) . ? C91' C92' 1.48(2) . ? C92' C93' 1.48(2) . ? C93' C94' 1.48(2) . ? C94' C95' 1.48(2) . ? C95' C96' 1.48(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C61 Ir1 C60 88.4(17) . . ? C61 Ir1 C65 102.4(15) . . ? C60 Ir1 C65 161.0(13) . . ? C61' Ir1 C65 122(3) . . ? C61 Ir1 C62 162.3(15) . . ? C60 Ir1 C62 108.5(13) . . ? C61' Ir1 C62 172(4) . . ? C65 Ir1 C62 59.9(9) . . ? C61 Ir1 C66 129.4(14) . . ? C60 Ir1 C66 124.7(13) . . ? C61' Ir1 C66 140(4) . . ? C65 Ir1 C66 37.0(9) . . ? C62 Ir1 C66 35.7(9) . . ? C61 Ir1 C63 136.4(14) . . ? C60 Ir1 C63 121.8(12) . . ? C61' Ir1 C63 151(4) . . ? C65 Ir1 C63 59.5(9) . . ? C62 Ir1 C63 37.1(9) . . ? C66 Ir1 C63 60.9(9) . . ? C61 Ir1 C64 105.5(15) . . ? C60 Ir1 C64 154.9(12) . . ? C61' Ir1 C64 126(4) . . ? C65 Ir1 C64 35.9(10) . . ? C62 Ir1 C64 60.8(9) . . ? C66 Ir1 C64 61.4(9) . . ? C63 Ir1 C64 35.7(9) . . ? C61' Ir1 C60' 86(4) . . ? C65 Ir1 C60' 149.8(16) . . ? C62 Ir1 C60' 90.7(14) . . ? C66 Ir1 C60' 114.4(19) . . ? C63 Ir1 C60' 102.0(14) . . ? C64 Ir1 C60' 136.7(15) . . ? O60 Mg1 N3 104.0(6) . . ? O60 Mg1 N1 125.6(6) . . ? N3 Mg1 N1 92.7(6) . . ? O60 Mg1 Mg2 85.2(5) . . ? N3 Mg1 Mg2 130.6(5) . . ? N1 Mg1 Mg2 121.3(4) . . ? O61 Mg2 N31 120.5(7) . . ? O61 Mg2 N33 105.8(7) . . ? N31 Mg2 N33 94.4(6) . . ? O61 Mg2 C61' 20(2) . . ? N31 Mg2 C61' 139(2) . . ? N33 Mg2 C61' 108(3) . . ? O61 Mg2 Mg1 87.2(5) . . ? N31 Mg2 Mg1 121.5(5) . . ? N33 Mg2 Mg1 128.9(5) . . ? C61' Mg2 Mg1 70(2) . . ? C1 N1 C6 118.3(13) . . ? C1 N1 Mg1 121.2(12) . . ? C6 N1 Mg1 120.4(11) . . ? N1 C1 C2 125.1(16) . . ? N1 C1 C4 122.4(17) . . ? C2 C1 C4 112.5(17) . . ? C1 C2 C3 127.8(18) . . ? N3 C3 C2 124.1(19) . . ? N3 C3 C5 123.2(19) . . ? C2 C3 C5 112.3(18) . . ? C3 N3 C18 117.8(16) . . ? C3 N3 Mg1 122.9(13) . . ? C18 N3 Mg1 119.3(12) . . ? C11 C6 C7 119.8(18) . . ? C11 C6 N1 121.1(16) . . ? C7 C6 N1 118.9(16) . . ? C8 C7 C6 118.9(18) . . ? C8 C7 C12' 121(2) . . ? C6 C7 C12' 120(2) . . ? C8 C7 C12 120(2) . . ? C6 C7 C12 121(2) . . ? C9 C8 C7 122.4(18) . . ? C10 C9 C8 118(2) . . ? C9 C10 C11 122.7(18) . . ? C6 C11 C10 117.7(16) . . ? C6 C11 C15 123.0(17) . . ? C10 C11 C15 119.3(17) . . ? C7 C12 C14 112(3) . . ? C7 C12 C13 111(2) . . ? C14 C12 C13 114(3) . . ? C7 C12' C13' 104(3) . . ? C7 C12' C14' 114(4) . . ? C13' C12' C14' 114(3) . . ? C16 C15 C17 109.2(17) . . ? C16 C15 C11 111.3(17) . . ? C17 C15 C11 112.6(17) . . ? C23 C18 C19 119.9(18) . . ? C23 C18 N3 119.9(18) . . ? C19 C18 N3 120.2(17) . . ? C18 C19 C20 118.7(19) . . ? C18 C19 C24 122(2) . . ? C20 C19 C24 119(2) . . ? C18 C19 C24' 122(3) . . ? C20 C19 C24' 117(3) . . ? C21 C20 C19 117(2) . . ? C22 C21 C20 122(2) . . ? C21 C22 C23 123(3) . . ? C22 C23 C18 119(2) . . ? C22 C23 C27 118(3) . . ? C18 C23 C27 121(3) . . ? C22 C23 C27' 121(3) . . ? C18 C23 C27' 119(3) . . ? C25 C24 C26 113(3) . . ? C25 C24 C19 113(2) . . ? C26 C24 C19 106(3) . . ? C26' C24' C25' 113(3) . . ? C26' C24' C19 121(5) . . ? C25' C24' C19 106(4) . . ? C28 C27 C29 109(3) . . ? C28 C27 C23 107(4) . . ? C29 C27 C23 114(4) . . ? C29' C27' C28' 110(3) . . ? C29' C27' C23 110(3) . . ? C28' C27' C23 113(4) . . ? C31 N31 C36 116.9(14) . . ? C31 N31 Mg2 122.6(12) . . ? C36 N31 Mg2 120.5(11) . . ? N31 C31 C32 122.6(15) . . ? N31 C31 C34 122.9(16) . . ? C32 C31 C34 114.4(15) . . ? C31 C32 C33 129.9(16) . . ? N33 C33 C32 123.8(17) . . ? N33 C33 C35 123.4(17) . . ? C32 C33 C35 112.7(17) . . ? C33 N33 C48 117.6(16) . . ? C33 N33 Mg2 121.4(12) . . ? C48 N33 Mg2 120.7(12) . . ? C37 C36 C41 121.3(18) . . ? C37 C36 N31 119.4(16) . . ? C41 C36 N31 119.2(15) . . ? C38 C37 C36 117.7(18) . . ? C38 C37 C42 119.0(17) . . ? C36 C37 C42 123.2(18) . . ? C39 C38 C37 123.0(19) . . ? C38 C39 C40 118(2) . . ? C39 C40 C41 123(2) . . ? C40 C41 C36 117.2(18) . . ? C40 C41 C45 119.7(18) . . ? C36 C41 C45 123.1(18) . . ? C37 C42 C43 109.9(18) . . ? C37 C42 C44 111.6(16) . . ? C43 C42 C44 111.1(15) . . ? C41 C45 C47 111.3(17) . . ? C41 C45 C46 112.8(17) . . ? C47 C45 C46 110.3(16) . . ? C53 C48 C49 122.0(18) . . ? C53 C48 N33 118.3(16) . . ? C49 C48 N33 119.6(16) . . ? C50 C49 C48 116.6(19) . . ? C50 C49 C54 120.9(19) . . ? C48 C49 C54 122.5(18) . . ? C51 C50 C49 124(2) . . ? C52 C51 C50 118(2) . . ? C51 C52 C53 122(2) . . ? C48 C53 C52 117.7(19) . . ? C48 C53 C57 122.6(17) . . ? C52 C53 C57 119.6(18) . . ? C49 C54 C55 112(2) . . ? C49 C54 C56 114(2) . . ? C55 C54 C56 107.5(19) . . ? C58 C57 C59 108.7(17) . . ? C58 C57 C53 109.6(19) . . ? C59 C57 C53 114.6(19) . . ? O60 C60 Ir1 168(3) . . ? O61 C61 Ir1 151(4) . . ? O60 C60' Ir1 105(5) . . ? O61 C61' Ir1 155(10) . . ? O61 C61' Mg2 36(4) . . ? Ir1 C61' Mg2 159(6) . . ? C60 O60 Mg1 144(2) . . ? C60' O60 Mg1 170(4) . . ? C61' O61 Mg2 124(6) . . ? C61 O61 Mg2 150(2) . . ? C66 C62 C63 109(2) . . ? C66 C62 C67 125(2) . . ? C63 C62 C67 126(2) . . ? C66 C62 Ir1 72.8(13) . . ? C63 C62 Ir1 72.5(14) . . ? C67 C62 Ir1 124.5(15) . . ? C64 C63 C62 108(2) . . ? C64 C63 C68 121(3) . . ? C62 C63 C68 131(3) . . ? C64 C63 Ir1 73.9(14) . . ? C62 C63 Ir1 70.4(14) . . ? C68 C63 Ir1 124.9(16) . . ? C65 C64 C63 106(2) . . ? C65 C64 C69 132(3) . . ? C63 C64 C69 122(3) . . ? C65 C64 Ir1 69.2(14) . . ? C63 C64 Ir1 70.4(14) . . ? C69 C64 Ir1 127.2(17) . . ? C64 C65 C66 111(2) . . ? C64 C65 C70 126(3) . . ? C66 C65 C70 123(3) . . ? C64 C65 Ir1 74.9(14) . . ? C66 C65 Ir1 72.2(13) . . ? C70 C65 Ir1 124.0(16) . . ? C62 C66 C65 106(2) . . ? C62 C66 C71 126(3) . . ? C65 C66 C71 128(3) . . ? C62 C66 Ir1 71.5(13) . . ? C65 C66 Ir1 70.8(13) . . ? C71 C66 Ir1 124.1(17) . . ? C83 C82 C81 118(3) . . ? C82 C83 C83 121(3) . 3_666 ? C93 C92 C91 119(3) . . ? C94 C93 C92 120(3) . . ? C95 C94 C93 120(2) . . ? C96 C95 C94 121(2) . . ? C91' C92' C93' 120(3) . . ? C92' C93' C94' 120(3) . . ? C95' C94' C93' 120(3) . . ? C94' C95' C96' 120(3) . . ? _refine_diff_density_max 2.013 _refine_diff_density_min -2.187 _refine_diff_density_rms 0.270 _shelx_res_file ; TITL MRC2138 in P2(1)/n MRC2138.res created by SHELXL-2018/3 at 13:02:11 on 29-Jun-2021 REM P2(1)/n (#14 in standard setting) REM JMP183 CELL 0.71073 14.027301 13.906250 40.204757 90.0000 99.7793 90.0000 ZERR 4.00 0.000567 0.000552 0.001389 0.0000 0.0035 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H Mg N O Ir UNIT 316 480 8 16 8 4 TEMP -100 L.S. 12 OMIT 2 0 8 OMIT 0 1 6 OMIT 1 -1 -3 FMAP 2 PLAN 10 ACTA REM Modelled as a 2 component twin using an hklf5 file and a BASF parameter REM The crystal was modelled as a two component twin in a ca. 77:23 ratio, REM with the two major lattices related by the approximate twin law REM [-1.00 0.00 0.00 0.00 -1.00 0.00 0.98 0.00 1.01] REM Unit cell from original, no-twin, data processing REM 'C70 H99 Ir Mg2 N4 O2, 1.5(C6 H14)' REM C79 H120 Ir Mg2 N4 O2 RTAB MG-H MG1 H1 RTAB MG-H MG2 H1 RTAB MHM MG1 H1 MG2 SADI C7 C12 C7 C12' SADI C12 C13 C12 C14 C12' C13' C12' C14' SADI C13 C14 C13' C14' SIMU 0.02 0.02 1 C12 > C14' SADI C19 C24 C19 C24' SADI C24 C25 C24 C26 C24' C25' C24' C26' SADI C25 C26 C25' C26' SIMU 0.02 0.02 1 C24 > C26' SADI C23 C27 C23 C27' SADI C27 C28 C27 C29 C27' C28' C27' C29' SADI C28 C29 C28' C29' SIMU 0.02 0.02 2 C27 > C29' SADI C60 O60 C61' O61 SADI C60' O60 C61 O61 SIMU 0.02 0.02 1 C60 C60' SIMU 0.02 0.02 1 C61 C61' SADI C91 C92 C92 C93 C93 C94 C94 C95 C95 C96 = C91' C92' C92' C93' C93' C94' C94' C95' C95' C96' SADI C91 C93 C92 C94 C93 C95 C94 C96 = C91' C93' C92' C94' C93' C95' C94' C96' SIMU 0.02 0.02 1 C91 > C96' ISOR 0.01 C2 C3 C18 C21 C23 C24 C31 C32 C34 C36 C69 ISOR 0.01 C44 C51 C54 O60 C62 C63 C66 C70 ISOR 0.005 N1 C21 C31 C36 SIMU 0.02 0.02 5 N31 > C35 SIMU 0.02 0.02 3 N31 > C59 SIMU 0.02 0.02 3 C62 > C71 WGHT 0.046500 289.974213 BASF 0.22953 FVAR 1.78378 0.59306 0.62284 0.50531 0.73725 0.65909 IR1 6 0.338566 0.351539 0.059778 11.00000 0.03079 0.04619 = 0.01774 -0.00527 -0.00550 -0.00137 MG1 3 0.593159 0.253439 0.140422 11.00000 0.01172 0.02006 = 0.01246 -0.00750 -0.00452 0.00466 MG2 3 0.434194 0.410152 0.171557 11.00000 0.02104 0.01523 = 0.00977 0.00011 0.00636 0.00033 H1 2 0.538422 0.333102 0.167729 11.00000 -1.50000 N1 4 0.738516 0.252616 0.159831 11.00000 0.01068 0.01407 = 0.00608 -0.00070 0.00003 0.00005 C1 1 0.781548 0.174647 0.173646 11.00000 0.02092 0.02725 = 0.01953 -0.01316 -0.00022 0.00980 C2 1 0.739059 0.081736 0.172398 11.00000 0.03161 0.02743 = 0.01511 -0.00720 0.01074 0.00479 AFIX 43 H2A 2 0.773810 0.034410 0.186607 11.00000 -1.20000 AFIX 0 C3 1 0.650097 0.050752 0.152293 11.00000 0.04274 0.02339 = 0.01459 -0.00426 0.00274 0.00240 N3 4 0.588702 0.107793 0.134617 11.00000 0.02003 0.01750 = 0.01983 0.00421 0.00350 0.00392 C4 1 0.884790 0.175355 0.192525 11.00000 0.03621 0.04092 = 0.04890 0.00859 -0.01750 0.01162 AFIX 137 H4A 2 0.927360 0.145349 0.178549 11.00000 -1.50000 H4B 2 0.888287 0.139317 0.213645 11.00000 -1.50000 H4C 2 0.905435 0.241856 0.197580 11.00000 -1.50000 AFIX 0 C5 1 0.641162 -0.058587 0.150848 11.00000 0.05537 0.01727 = 0.06223 -0.00755 -0.00473 0.00875 AFIX 137 H5A 2 0.592728 -0.079389 0.164259 11.00000 -1.50000 H5B 2 0.703807 -0.087600 0.159992 11.00000 -1.50000 H5C 2 0.621210 -0.078990 0.127366 11.00000 -1.50000 AFIX 0 C6 1 0.794623 0.338932 0.160153 11.00000 0.01424 0.02990 = 0.02226 -0.00664 -0.00028 -0.00044 C7 1 0.839301 0.360310 0.131784 11.00000 0.00708 0.04589 = 0.03428 -0.01365 0.00557 -0.00404 C8 1 0.893460 0.443500 0.132121 11.00000 0.01516 0.05299 = 0.02476 0.00127 0.01011 -0.00155 AFIX 43 H8A 2 0.924426 0.456956 0.113381 11.00000 -1.20000 AFIX 0 C9 1 0.904200 0.507728 0.158682 11.00000 0.02537 0.04088 = 0.02976 -0.00323 0.00179 -0.00466 AFIX 43 H9A 2 0.943824 0.563139 0.158706 11.00000 -1.20000 AFIX 0 C10 1 0.856194 0.489521 0.185052 11.00000 0.03466 0.02814 = 0.02731 -0.01564 0.00379 -0.00115 AFIX 43 H10A 2 0.860698 0.535134 0.202841 11.00000 -1.20000 AFIX 0 C11 1 0.800252 0.405539 0.186815 11.00000 0.00736 0.03255 = 0.01814 -0.00016 0.00271 0.00218 PART 1 C12 1 0.833819 0.290270 0.102878 21.00000 0.04702 0.04498 = 0.03431 -0.01728 0.01660 -0.01391 AFIX 13 H12A 2 0.791267 0.236420 0.107951 21.00000 -1.20000 AFIX 0 C13 1 0.783859 0.334963 0.070034 21.00000 0.03658 0.04078 = 0.01643 -0.01132 0.01784 -0.02493 AFIX 33 H13A 2 0.781287 0.288028 0.051721 21.00000 -1.50000 H13B 2 0.717960 0.353923 0.072275 21.00000 -1.50000 H13C 2 0.820091 0.391775 0.064914 21.00000 -1.50000 AFIX 0 C14 1 0.931540 0.245711 0.100896 21.00000 0.06160 0.04944 = 0.04631 -0.01457 0.00325 0.00607 AFIX 33 H14A 2 0.924844 0.200817 0.081852 21.00000 -1.50000 H14B 2 0.977533 0.296497 0.097663 21.00000 -1.50000 H14C 2 0.955301 0.211066 0.121895 21.00000 -1.50000 AFIX 0 PART 2 C12' 1 0.825729 0.293556 0.101784 -21.00000 0.04383 AFIX 13 H12B 2 0.758090 0.268118 0.098407 -21.00000 -1.20000 AFIX 0 C13' 1 0.835356 0.359032 0.072312 -21.00000 0.02291 AFIX 33 H13D 2 0.827422 0.321191 0.051460 -21.00000 -1.50000 H13E 2 0.785423 0.408987 0.070272 -21.00000 -1.50000 H13F 2 0.899437 0.389175 0.076182 -21.00000 -1.50000 AFIX 0 C14' 1 0.894980 0.208630 0.105367 -21.00000 0.05107 AFIX 33 H14D 2 0.881795 0.168770 0.085002 -21.00000 -1.50000 H14E 2 0.961728 0.232220 0.108379 -21.00000 -1.50000 H14F 2 0.886053 0.170161 0.125029 -21.00000 -1.50000 AFIX 0 PART 0 C15 1 0.751897 0.389055 0.217753 11.00000 0.02815 0.02754 = 0.01687 -0.00252 -0.00092 -0.00010 AFIX 13 H15A 2 0.708802 0.331596 0.213169 11.00000 -1.20000 AFIX 0 C16 1 0.825459 0.368191 0.248591 11.00000 0.05784 0.07914 = 0.02613 0.00654 0.00455 0.01889 AFIX 137 H16A 2 0.859155 0.308096 0.245308 11.00000 -1.50000 H16B 2 0.792918 0.361887 0.268208 11.00000 -1.50000 H16C 2 0.872349 0.420963 0.252397 11.00000 -1.50000 AFIX 0 C17 1 0.690347 0.473245 0.224858 11.00000 0.01554 0.05442 = 0.03731 -0.00919 0.01016 0.00542 AFIX 137 H17A 2 0.731760 0.529338 0.231182 11.00000 -1.50000 H17B 2 0.656105 0.456848 0.243405 11.00000 -1.50000 H17C 2 0.643241 0.488172 0.204597 11.00000 -1.50000 AFIX 0 C18 1 0.515798 0.065591 0.109098 11.00000 0.02937 0.02110 = 0.02273 -0.01351 0.00182 -0.00086 C19 1 0.423875 0.041640 0.116735 11.00000 0.04340 0.03343 = 0.01794 -0.00146 0.00051 -0.01326 C20 1 0.351263 0.002990 0.090158 11.00000 0.07102 0.06151 = 0.04957 -0.00624 0.03947 -0.03155 AFIX 43 H20A 2 0.287095 -0.009485 0.093632 11.00000 -1.20000 AFIX 0 C21 1 0.380906 -0.015485 0.058414 11.00000 0.02779 0.03795 = 0.03366 -0.00235 0.00332 -0.00916 AFIX 43 H21A 2 0.336337 -0.044639 0.040879 11.00000 -1.20000 AFIX 0 C22 1 0.466947 0.006377 0.052809 11.00000 0.05025 0.08899 = 0.05339 -0.04932 -0.01270 -0.01406 AFIX 43 H22A 2 0.482465 -0.006768 0.031164 11.00000 -1.20000 AFIX 0 C23 1 0.536369 0.047606 0.076772 11.00000 0.04138 0.04536 = 0.02996 -0.01606 0.00442 0.00041 PART 1 C24 1 0.400466 0.052593 0.152609 31.00000 0.03267 0.02913 = 0.02275 0.00409 0.00424 0.00015 AFIX 13 H24A 2 0.461470 0.069055 0.168319 31.00000 -1.20000 AFIX 0 C25 1 0.358934 -0.038086 0.165083 31.00000 0.05437 0.04960 = 0.03204 0.01060 0.01858 -0.01621 AFIX 33 H25A 2 0.405883 -0.090503 0.165659 31.00000 -1.50000 H25B 2 0.344783 -0.027331 0.187838 31.00000 -1.50000 H25C 2 0.299182 -0.055274 0.149848 31.00000 -1.50000 AFIX 0 C26 1 0.332052 0.136958 0.151014 31.00000 0.07680 0.06005 = 0.06488 -0.01272 0.01028 0.00272 AFIX 33 H26A 2 0.362223 0.193807 0.142807 31.00000 -1.50000 H26B 2 0.271967 0.121936 0.135605 31.00000 -1.50000 H26C 2 0.317568 0.149879 0.173595 31.00000 -1.50000 AFIX 0 PART 2 C24' 1 0.388479 0.078471 0.148724 -31.00000 0.03157 AFIX 13 H24B 2 0.432563 0.133103 0.156978 -31.00000 -1.20000 AFIX 0 C25' 1 0.412292 0.000736 0.175062 -31.00000 0.04966 AFIX 33 H25D 2 0.478370 -0.022296 0.175167 -31.00000 -1.50000 H25E 2 0.407161 0.026857 0.197328 -31.00000 -1.50000 H25F 2 0.366795 -0.052789 0.169779 -31.00000 -1.50000 AFIX 0 C26' 1 0.287736 0.118119 0.146846 -31.00000 0.06890 AFIX 33 H26D 2 0.276303 0.168053 0.129423 -31.00000 -1.50000 H26E 2 0.240510 0.066222 0.141172 -31.00000 -1.50000 H26F 2 0.280875 0.145868 0.168721 -31.00000 -1.50000 AFIX 0 PART 1 C27 1 0.639251 0.054191 0.069341 41.00000 0.05252 0.05666 = 0.04936 -0.00413 0.00893 0.00265 AFIX 13 H27A 2 0.683062 0.076574 0.090153 41.00000 -1.20000 AFIX 0 C28 1 0.638441 0.128816 0.042035 41.00000 0.05372 0.06132 = 0.05886 -0.00069 0.00668 0.00328 AFIX 33 H28A 2 0.613546 0.189665 0.049387 41.00000 -1.50000 H28B 2 0.704404 0.138343 0.037643 41.00000 -1.50000 H28C 2 0.596847 0.106894 0.021346 41.00000 -1.50000 AFIX 0 C29 1 0.677754 -0.039766 0.057911 41.00000 0.05596 0.05740 = 0.05787 -0.00548 0.00659 0.00407 AFIX 33 H29A 2 0.678333 -0.088315 0.075613 41.00000 -1.50000 H29B 2 0.636142 -0.061611 0.037215 41.00000 -1.50000 H29C 2 0.743700 -0.030161 0.053512 41.00000 -1.50000 AFIX 0 PART 2 C27' 1 0.629569 0.087332 0.067241 -41.00000 0.05029 AFIX 13 H27B 2 0.659773 0.131148 0.085798 -41.00000 -1.20000 AFIX 0 C28' 1 0.613464 0.144491 0.034813 -41.00000 0.06077 AFIX 33 H28D 2 0.567872 0.196905 0.036556 -41.00000 -1.50000 H28E 2 0.675173 0.171336 0.030869 -41.00000 -1.50000 H28F 2 0.586902 0.102309 0.015980 -41.00000 -1.50000 AFIX 0 C29' 1 0.699820 0.006378 0.064721 -41.00000 0.05751 AFIX 33 H29D 2 0.710056 -0.030497 0.085799 -41.00000 -1.50000 H29E 2 0.673351 -0.035953 0.045920 -41.00000 -1.50000 H29F 2 0.761621 0.033074 0.060809 -41.00000 -1.50000 AFIX 0 PART 0 N31 4 0.404305 0.396153 0.219052 11.00000 0.01558 0.01709 = 0.01669 -0.00061 0.00350 0.00235 C31 1 0.417561 0.467378 0.241534 11.00000 0.01046 0.01488 = 0.01028 -0.00150 0.00203 0.00258 C32 1 0.447784 0.559623 0.233668 11.00000 0.01249 0.01759 = 0.01115 -0.00423 -0.00104 0.00263 AFIX 43 H32A 2 0.473025 0.598368 0.252583 11.00000 -1.20000 AFIX 0 C33 1 0.446369 0.604372 0.201383 11.00000 0.01340 0.02021 = 0.02009 0.00338 0.00640 0.00650 N33 4 0.435270 0.556863 0.172707 11.00000 0.01447 0.02178 = 0.01965 0.00359 0.00829 0.00315 C34 1 0.403270 0.455136 0.277891 11.00000 0.02212 0.02213 = 0.01269 -0.00132 0.00158 0.00224 AFIX 137 H34A 2 0.334087 0.458100 0.279014 11.00000 -1.50000 H34B 2 0.437268 0.506676 0.291726 11.00000 -1.50000 H34C 2 0.429232 0.392733 0.286400 11.00000 -1.50000 AFIX 0 C35 1 0.465053 0.711998 0.204092 11.00000 0.02146 0.01935 = 0.03044 -0.00032 0.00356 -0.00079 AFIX 137 H35A 2 0.471570 0.737551 0.181873 11.00000 -1.50000 H35B 2 0.524820 0.724058 0.220063 11.00000 -1.50000 H35C 2 0.410816 0.743767 0.212087 11.00000 -1.50000 AFIX 0 C36 1 0.369446 0.305846 0.230134 11.00000 0.02164 0.01916 = 0.01660 -0.00008 0.00758 -0.00088 C37 1 0.269542 0.287087 0.224421 11.00000 0.02588 0.02534 = 0.02616 -0.00022 0.00852 -0.00157 C38 1 0.238764 0.200150 0.235794 11.00000 0.03387 0.02207 = 0.03651 -0.00303 0.01204 -0.00408 AFIX 43 H38A 2 0.171375 0.186788 0.232146 11.00000 -1.20000 AFIX 0 C39 1 0.301318 0.132363 0.252116 11.00000 0.04123 0.02197 = 0.03592 0.00455 0.01371 -0.00125 AFIX 43 H39A 2 0.277782 0.074908 0.260617 11.00000 -1.20000 AFIX 0 C40 1 0.399796 0.150488 0.255777 11.00000 0.03911 0.02671 = 0.03409 0.00485 0.00713 0.00151 AFIX 43 H40A 2 0.443749 0.102805 0.265994 11.00000 -1.20000 AFIX 0 C41 1 0.436909 0.236242 0.245012 11.00000 0.02678 0.02499 = 0.02618 0.00368 0.00315 0.00294 C42 1 0.194545 0.357638 0.206876 11.00000 0.02155 0.02618 = 0.03424 0.00227 0.00881 -0.00281 AFIX 13 H42A 2 0.228968 0.417721 0.202082 11.00000 -1.20000 AFIX 0 C43 1 0.145155 0.315951 0.173347 11.00000 0.02347 0.04402 = 0.03728 -0.00136 0.00217 -0.00511 AFIX 137 H43A 2 0.192477 0.309370 0.158145 11.00000 -1.50000 H43B 2 0.092949 0.358981 0.163151 11.00000 -1.50000 H43C 2 0.118232 0.252657 0.177154 11.00000 -1.50000 AFIX 0 C44 1 0.119038 0.384726 0.229636 11.00000 0.01950 0.03147 = 0.04476 -0.00375 0.00128 -0.00440 AFIX 137 H44A 2 0.076609 0.329603 0.231343 11.00000 -1.50000 H44B 2 0.080219 0.439380 0.219677 11.00000 -1.50000 H44C 2 0.152819 0.402223 0.252196 11.00000 -1.50000 AFIX 0 C45 1 0.543855 0.250682 0.249516 11.00000 0.03019 0.02586 = 0.02316 0.00973 0.00458 0.00391 AFIX 13 H45A 2 0.555514 0.312762 0.238311 11.00000 -1.20000 AFIX 0 C46 1 0.592269 0.258946 0.287567 11.00000 0.04042 0.03679 = 0.02624 0.00424 -0.00296 0.01098 AFIX 137 H46A 2 0.566675 0.315485 0.297638 11.00000 -1.50000 H46B 2 0.662453 0.265495 0.289138 11.00000 -1.50000 H46C 2 0.577917 0.201019 0.299692 11.00000 -1.50000 AFIX 0 C47 1 0.592074 0.171547 0.232212 11.00000 0.03106 0.03344 = 0.03552 0.00871 0.00772 0.01436 AFIX 137 H47A 2 0.580945 0.109363 0.242364 11.00000 -1.50000 H47B 2 0.661762 0.183898 0.235003 11.00000 -1.50000 H47C 2 0.564592 0.170380 0.208118 11.00000 -1.50000 AFIX 0 C48 1 0.413552 0.612228 0.141670 11.00000 0.02501 0.02881 = 0.02880 0.00870 0.01118 0.00502 C49 1 0.483618 0.622002 0.121184 11.00000 0.03244 0.03597 = 0.03435 0.01357 0.01235 0.00483 C50 1 0.457719 0.674600 0.091804 11.00000 0.04077 0.04221 = 0.04278 0.01378 0.01459 0.00548 AFIX 43 H50A 2 0.505084 0.684463 0.077833 11.00000 -1.20000 AFIX 0 C51 1 0.367542 0.713232 0.081754 11.00000 0.03878 0.03991 = 0.03828 0.01749 0.01107 0.00777 AFIX 43 H51A 2 0.351851 0.746783 0.060960 11.00000 -1.20000 AFIX 0 C52 1 0.300954 0.701925 0.102608 11.00000 0.03473 0.03970 = 0.03955 0.01624 0.00971 0.01160 AFIX 43 H52A 2 0.238778 0.730092 0.096392 11.00000 -1.20000 AFIX 0 C53 1 0.321325 0.650343 0.132742 11.00000 0.03470 0.03798 = 0.03836 0.01416 0.00737 0.00554 C54 1 0.583578 0.582739 0.130818 11.00000 0.03646 0.03992 = 0.03750 0.00972 0.01797 0.00445 AFIX 13 H54A 2 0.581565 0.531185 0.148025 11.00000 -1.20000 AFIX 0 C55 1 0.653815 0.658758 0.146525 11.00000 0.04499 0.05636 = 0.05754 -0.00143 0.00670 0.01093 AFIX 137 H55A 2 0.650239 0.714443 0.131425 11.00000 -1.50000 H55B 2 0.719623 0.632563 0.150137 11.00000 -1.50000 H55C 2 0.637211 0.678654 0.168217 11.00000 -1.50000 AFIX 0 C56 1 0.624425 0.538832 0.101544 11.00000 0.04382 0.04781 = 0.05159 0.00512 0.01621 0.00296 AFIX 137 H56A 2 0.577710 0.493027 0.089548 11.00000 -1.50000 H56B 2 0.685028 0.505344 0.110216 11.00000 -1.50000 H56C 2 0.636844 0.589847 0.086015 11.00000 -1.50000 AFIX 0 C57 1 0.241999 0.639464 0.155303 11.00000 0.02996 0.03904 = 0.03849 0.01696 0.01370 0.01009 AFIX 13 H57A 2 0.273741 0.614302 0.177770 11.00000 -1.20000 AFIX 0 C58 1 0.169518 0.568086 0.140139 11.00000 0.03495 0.05449 = 0.05683 0.00922 0.00794 0.00648 AFIX 137 H58A 2 0.143667 0.586772 0.116850 11.00000 -1.50000 H58B 2 0.116731 0.565435 0.153256 11.00000 -1.50000 H58C 2 0.200049 0.504674 0.140247 11.00000 -1.50000 AFIX 0 C59 1 0.189497 0.733494 0.161287 11.00000 0.04084 0.05393 = 0.04793 0.01453 0.00075 0.01027 AFIX 137 H59A 2 0.236562 0.780397 0.172389 11.00000 -1.50000 H59B 2 0.141177 0.720535 0.175687 11.00000 -1.50000 H59C 2 0.157334 0.759405 0.139594 11.00000 -1.50000 AFIX 0 PART 1 C60 1 0.463462 0.318116 0.079018 51.00000 0.04379 0.03171 = 0.04939 0.01138 0.01419 -0.01802 C61 1 0.313275 0.372189 0.101558 51.00000 0.07677 0.04804 = 0.01746 0.00651 -0.02469 -0.00361 AFIX 43 H61A 2 0.246669 0.388937 0.098178 51.00000 -1.20000 AFIX 0 PART 2 C60' 1 0.507341 0.324365 0.065357 -51.00000 0.04069 AFIX 43 H60B 2 0.546042 0.328986 0.048190 -51.00000 -1.20000 AFIX 0 C61' 1 0.358417 0.354762 0.107748 -51.00000 0.04966 PART 0 O60 5 0.535161 0.302310 0.096152 11.00000 0.02283 0.04068 = 0.01029 0.00314 -0.00892 0.00252 O61 5 0.340035 0.375540 0.133290 11.00000 0.03842 0.05347 = 0.01884 -0.00861 -0.00027 0.00019 C62 1 0.319853 0.325426 0.002862 11.00000 0.04467 0.06310 = 0.02893 -0.00145 -0.00450 -0.00301 C63 1 0.304747 0.428235 0.007987 11.00000 0.04917 0.06439 = 0.03185 0.00309 -0.00566 -0.00207 C64 1 0.220077 0.439500 0.023295 11.00000 0.04873 0.07500 = 0.03716 0.00117 -0.01476 0.00333 C65 1 0.187010 0.343731 0.028178 11.00000 0.04239 0.07706 = 0.03651 -0.00354 -0.00867 -0.00121 C66 1 0.247035 0.272699 0.014937 11.00000 0.04348 0.06455 = 0.03142 -0.00422 -0.00749 -0.00360 C67 1 0.397785 0.281576 -0.015252 11.00000 0.05173 0.07902 = 0.03239 -0.00603 -0.00665 -0.00170 AFIX 137 H67A 2 0.456059 0.321660 -0.011111 11.00000 -1.50000 H67B 2 0.373408 0.278571 -0.039562 11.00000 -1.50000 H67C 2 0.413520 0.216568 -0.006619 11.00000 -1.50000 AFIX 0 C68 1 0.357368 0.514099 -0.001847 11.00000 0.06437 0.07725 = 0.04294 0.01518 -0.01519 -0.00577 AFIX 137 H68A 2 0.423655 0.514208 0.010725 11.00000 -1.50000 H68B 2 0.324049 0.572712 0.003383 11.00000 -1.50000 H68C 2 0.358963 0.511775 -0.026108 11.00000 -1.50000 AFIX 0 C69 1 0.178748 0.539439 0.029816 11.00000 0.06536 0.07810 = 0.05372 -0.00466 -0.01319 0.01018 AFIX 137 H69A 2 0.126905 0.556076 0.011146 11.00000 -1.50000 H69B 2 0.230282 0.587665 0.031473 11.00000 -1.50000 H69C 2 0.152848 0.537955 0.050966 11.00000 -1.50000 AFIX 0 C70 1 0.094417 0.316255 0.042646 11.00000 0.04534 0.09072 = 0.05642 -0.00215 -0.00747 -0.00826 AFIX 137 H70A 2 0.102409 0.251927 0.052688 11.00000 -1.50000 H70B 2 0.038357 0.316557 0.024404 11.00000 -1.50000 H70C 2 0.084250 0.362999 0.059947 11.00000 -1.50000 AFIX 0 C71 1 0.233755 0.165274 0.012954 11.00000 0.06000 0.07518 = 0.03834 -0.00787 -0.00619 -0.01448 AFIX 137 H71A 2 0.191106 0.145112 0.028606 11.00000 -1.50000 H71B 2 0.296745 0.133679 0.019070 11.00000 -1.50000 H71C 2 0.204773 0.147120 -0.010104 11.00000 -1.50000 AFIX 0 C81 1 0.358207 0.320146 0.478728 11.00000 0.05656 0.10208 = 0.04557 -0.01407 0.00375 -0.00593 AFIX 137 H81A 2 0.337820 0.342922 0.455543 11.00000 -1.50000 H81B 2 0.302063 0.294790 0.487426 11.00000 -1.50000 H81C 2 0.406599 0.269203 0.478984 11.00000 -1.50000 AFIX 0 C82 1 0.401868 0.403198 0.500808 11.00000 0.05252 0.10287 = 0.06887 -0.01282 0.02097 0.00330 AFIX 23 H82A 2 0.348252 0.445711 0.504723 11.00000 -1.20000 H82B 2 0.431355 0.376371 0.522987 11.00000 -1.20000 AFIX 0 C83 1 0.473387 0.462014 0.488952 11.00000 0.05231 0.06726 = 0.07152 0.00461 0.01447 0.01210 AFIX 23 H83A 2 0.441191 0.494149 0.468064 11.00000 -1.20000 H83B 2 0.522515 0.418105 0.482358 11.00000 -1.20000 AFIX 0 PART 1 C91 1 1.048106 0.996949 0.118232 61.00000 0.11599 0.11214 = 0.10558 -0.00390 0.00859 0.00646 AFIX 33 H91A 2 1.062683 1.039698 0.137815 61.00000 -1.50000 H91B 2 1.107944 0.966639 0.113971 61.00000 -1.50000 H91C 2 1.019248 1.034307 0.098391 61.00000 -1.50000 AFIX 0 C92 1 0.979145 0.921566 0.125074 61.00000 0.08826 0.09791 = 0.08104 -0.00327 0.01504 0.00990 AFIX 23 H92A 2 1.009062 0.887143 0.145788 61.00000 -1.20000 H92B 2 0.920847 0.954444 0.130293 61.00000 -1.20000 AFIX 0 C93 1 0.946391 0.848195 0.098864 61.00000 0.06482 0.07168 = 0.05694 0.01298 0.00569 0.00304 AFIX 23 H93A 2 0.907425 0.881760 0.079465 61.00000 -1.20000 H93B 2 1.004681 0.822916 0.090994 61.00000 -1.20000 AFIX 0 C94 1 0.889431 0.764612 0.107015 61.00000 0.02884 0.15671 = 0.06390 0.00686 0.00132 -0.01628 AFIX 23 H94A 2 0.929452 0.729704 0.125855 61.00000 -1.20000 H94B 2 0.832480 0.789952 0.115726 61.00000 -1.20000 AFIX 0 C95 1 0.853716 0.693083 0.080676 61.00000 0.08087 0.10081 = 0.07557 0.01834 0.00725 -0.00759 AFIX 23 H95A 2 0.818146 0.643402 0.091276 61.00000 -1.20000 H95B 2 0.805742 0.725991 0.063525 61.00000 -1.20000 AFIX 0 C96 1 0.921694 0.642459 0.062499 61.00000 0.08413 0.08924 = 0.08707 0.00411 -0.01773 -0.00762 AFIX 33 H96A 2 0.885736 0.597996 0.046058 61.00000 -1.50000 H96B 2 0.956013 0.689436 0.050716 61.00000 -1.50000 H96C 2 0.968498 0.606311 0.078646 61.00000 -1.50000 AFIX 0 PART 2 C91' 1 1.027084 0.980924 0.115327 -61.00000 0.11156 AFIX 33 H91F 2 1.030764 1.050841 0.118324 -61.00000 -1.50000 H91G 2 1.079079 0.950308 0.131152 -61.00000 -1.50000 H91H 2 1.034135 0.964721 0.092147 -61.00000 -1.50000 AFIX 0 C92' 1 0.932504 0.946096 0.121897 -61.00000 0.09054 AFIX 23 H91D 2 0.881821 0.980750 0.106284 -61.00000 -1.20000 H91E 2 0.926486 0.966426 0.145048 -61.00000 -1.20000 AFIX 0 C93' 1 0.908763 0.842564 0.119048 -61.00000 0.10061 AFIX 23 H93C 2 0.837629 0.836748 0.116861 -61.00000 -1.20000 H93D 2 0.937045 0.812127 0.140748 -61.00000 -1.20000 AFIX 0 C94' 1 0.938554 0.784314 0.091823 -61.00000 0.05967 AFIX 23 H94C 2 0.924054 0.822457 0.070779 -61.00000 -1.20000 H94D 2 1.009753 0.777299 0.097124 -61.00000 -1.20000 AFIX 0 C95' 1 0.897706 0.687360 0.084231 -61.00000 0.08831 AFIX 23 H95C 2 0.828752 0.695608 0.074136 -61.00000 -1.20000 H95D 2 0.899230 0.653902 0.106050 -61.00000 -1.20000 AFIX 0 C96' 1 0.941037 0.621742 0.061980 -61.00000 0.08882 AFIX 33 H96D 2 0.905242 0.560915 0.059668 -61.00000 -1.50000 H96E 2 0.937831 0.651399 0.039706 -61.00000 -1.50000 H96F 2 1.008752 0.609430 0.071820 -61.00000 -1.50000 PART 0 AFIX 0 HKLF 5 REM MRC2138 in P2(1)/n REM wR2 = 0.3310, GooF = S = 1.266, Restrained GooF = 1.232 for all data REM R1 = 0.1271 for 11538 Fo > 4sig(Fo) and 0.1545 for all 16394 data REM 890 parameters refined using 1091 restraints END WGHT 0.0462 290.3135 REM Highest difference peak 2.013, deepest hole -2.187, 1-sigma level 0.270 Q1 1 0.4272 0.3554 0.0599 11.00000 0.05 2.01 Q2 1 0.3445 0.2931 0.0606 11.00000 0.05 1.90 Q3 1 0.4875 0.1448 0.3043 11.00000 0.05 1.61 Q4 1 0.5013 0.5562 0.3184 11.00000 0.05 1.57 Q5 1 0.3634 -0.0601 0.0734 11.00000 0.05 1.46 Q6 1 0.3387 0.7832 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1412.08 1473.65 -2 -2 -13 -25 1412.08 1473.65 1 2 13 -28 1613.69 1418.50 -2 -2 -13 -26 1613.69 1418.50 1 2 13 -29 2783.60 2135.18 -2 -2 -13 -27 2783.60 2135.18 1 2 13 -30 4865.07 2244.78 -2 -2 -13 -28 4865.07 2244.78 1 2 13 -31 7091.66 2315.79 -2 -2 -13 -29 7091.66 2315.79 1 2 13 -32 3394.58 2292.87 -2 -2 -13 -30 3394.58 2292.87 1 2 13 -33 7053.82 2416.38 -2 -2 -13 -31 7053.82 2416.38 1 2 13 -34 4460.75 3308.88 -2 -2 -13 -32 4460.75 3308.88 1 -2 14 -29 237.968 1714.71 -2 2 -14 -31 237.968 1714.71 1 -2 14 -28 8097.74 3178.49 -2 2 -14 -30 8097.74 3178.49 1 -2 14 -27 1096.09 2933.15 -2 2 -14 -29 1096.09 2933.15 1 -2 14 -26 3816.76 2936.44 -2 2 -14 -28 3816.76 2936.44 1 -2 14 -25 2017.25 2819.52 -2 2 -14 -27 2017.25 2819.52 1 -2 14 -24 8505.89 2240.08 -2 2 -14 -26 8505.89 2240.08 1 -2 14 -23 1877.53 2138.36 -2 2 -14 -25 1877.53 2138.36 1 -2 14 -22 3635.84 2089.61 -2 2 -14 -24 3635.84 2089.61 1 -2 14 -21 4001.98 2098.61 -2 2 -14 -23 4001.98 2098.61 1 -2 14 -20 5482.41 2767.03 -2 2 -14 -22 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179.430 1857.27 2 10 6 -22 30797.9 2628.73 2 10 6 -21 958.149 2281.86 2 10 6 -18 4733.71 2051.50 2 10 6 -16 1768.28 1827.54 2 10 6 -15 18457.0 2194.47 2 10 7 -31 13774.9 2776.76 2 10 7 -22 780.911 2308.34 2 10 7 -21 41299.5 2906.34 2 10 7 -17 2850.15 1991.68 2 10 7 -16 4354.31 2261.02 2 10 7 -14 1777.99 1844.25 2 10 8 -17 27336.4 2614.02 2 10 8 -13 1571.39 1903.35 2 10 8 -12 4700.88 1943.28 2 10 9 -22 375.175 2315.85 2 10 9 -17 1103.08 2136.21 2 10 9 -16 34198.0 2718.27 2 10 9 -15 1026.82 2153.51 2 10 9 -11 2997.77 2207.99 2 10 10 -10 4150.33 2362.21 2 10 10 -9 578.714 2236.21 2 10 11 -8 699.166 2246.46 2 10 11 -7 1704.45 2453.63 2 10 12 -7 1612.22 2265.23 2 10 12 -6 2542.80 2649.70 2 10 13 -6 385.933 2628.71 2 10 13 -5 7197.45 2684.40 2 10 13 -4 190.256 2557.33 2 11 0 -25 352.085 1723.51 2 11 0 -19 1106.87 1467.25 2 11 0 -17 404.326 1420.54 2 11 0 -15 342.898 1323.79 2 11 0 -13 890.487 1076.08 2 11 0 -11 2013.67 1130.58 2 11 0 -9-167.837 1017.37 2 11 0 -7 1021.86 1121.96 2 11 0 -5 2099.05 1117.77 2 11 0 -3 8688.88 545.990 2 11 0 -1 4205.11 570.870 2 11 0 1 1687.47 586.276 2 -11 0 -3 8203.25 755.232 2 -11 0 -5 6905.04 812.268 2 -11 0 -7 1006.13 835.709 2 -11 0 -9 1584.82 904.151 2 -11 0 -11 4800.69 997.024 2 -11 0 -13 6700.00 1156.42 2 -11 0 -15 19393.8 1251.89 2 -11 0 -17 1628.11 1175.92 2 -11 0 -19 9274.62 1281.19 2 -11 0 -21 5492.49 1285.23 2 -11 0 -23 7730.21 1444.58 2 -11 0 -25 3342.66 1464.01 2 -11 0 -27 4958.41 1621.82 2 -11 0 -29 8531.54 1685.64 2 -11 0 -31 1661.36 1693.69 2 -11 0 -33 974.311 1885.73 2 11 -1 -24 1811.22 1262.44 2 11 -1 -22 7565.37 1185.38 2 11 -1 -20 30351.7 1375.57 2 11 -1 -19 13313.9 1183.39 2 11 -1 -18 16562.0 1170.73 2 11 -1 -17 14564.1 492.370 2 11 1 -15 5494.55 1505.75 2 11 1 -14 1027.86 1315.23 2 11 2 -25 3761.51 1966.11 2 11 -2 -23 822.766 1626.86 2 11 2 -22 2883.26 1915.14 2 11 -2 -21 61233.3 2179.64 2 11 2 -20 1446.22 948.248 2 11 -2 -19 44526.7 1025.65 2 -11 2 18 1583.24 824.953 2 11 2 -17 590.025 1615.66 2 11 2 -16 16132.3 1821.75 2 11 2 -15-467.797 1496.12 2 11 2 -14 1864.90 1440.39 2 11 2 -13 15862.8 1617.49 2 11 2 -12 1429.75 1418.65 2 11 3 -34 866.561 2788.04 2 11 3 -26 3602.88 2116.73 2 11 -3 -21 19208.8 1709.90 2 11 -3 -20 12194.3 1290.64 2 11 3 -18 4954.76 1912.72 2 11 3 -17 10352.3 1843.46 2 11 3 -15 52867.7 2351.08 2 11 3 -14 2328.31 1647.23 2 11 3 -12 7808.71 1662.85 2 11 3 -11 818.736 1493.85 2 11 4 -25 90.8378 2101.64 2 11 -4 -22 18466.4 1702.00 2 11 -4 -21 9401.40 1284.17 2 11 4 -16 9056.12 1997.63 2 11 4 -15 364.794 1785.59 2 11 4 -13 13870.7 1932.20 2 11 4 -11 9853.38 1882.38 2 11 4 -10 6283.97 1700.51 2 11 4 -9 2107.19 1675.17 2 11 5 -30 29042.6 2928.25 2 11 5 -21 2913.03 2161.63 2 11 5 -20 70936.6 3133.66 2 11 5 -17 620.168 2072.75 2 11 5 -15 10110.4 2036.43 2 11 5 -13 2642.04 1838.20 2 11 5 -11 513.908 1644.55 2 11 5 -9 3878.61 1789.65 2 11 5 -8 2191.13 1816.68 2 11 6 -23 769.457 2285.18 2 11 6 -22 21994.3 2661.09 2 11 6 -17 67.8626 2208.11 2 11 6 -14 15890.2 2183.92 2 11 6 -11 14409.2 2013.23 2 11 6 -8 11264.8 1896.69 2 11 6 -7 446.240 1908.17 2 11 6 -6 14786.7 2149.61 2 11 7 -23 20011.6 2713.97 2 11 7 -22 10903.5 2625.01 2 11 7 -21 4774.72 2425.20 2 11 7 -15 43660.2 2698.16 2 11 7 -14 1671.49 2258.34 2 11 7 -10 2388.45 1828.24 2 11 7 -9 6209.20 1942.91 2 11 7 -6 920.899 2009.02 2 11 7 -5 609.929 1809.02 2 11 8 -15 6876.99 2232.08 2 11 8 -14 9892.04 2272.14 2 11 8 -13 13995.5 2391.62 2 11 8 -5 8557.76 2261.47 2 11 8 -4 736.471 2207.39 2 11 8 -3 4711.61 2193.18 2 11 9 -23 11532.5 2846.25 2 11 9 -3 1161.25 2115.95 2 11 9 -2 1999.57 2167.85 2 11 9 -1 1824.08 2235.56 2 11 10 -2 218.796 2191.39 2 11 10 -1 218.837 2362.35 2 11 10 0 5371.10 2407.80 2 11 11 -1 3463.17 2626.29 2 11 11 0 1437.37 2329.02 2 11 11 1 1164.81 2262.94 2 11 11 2 1382.17 2529.61 2 11 12 1-410.276 2678.85 2 11 12 2 1385.91 2392.32 2 11 12 3 3123.06 2686.48 2 12 0 -40 7347.64 2396.73 2 12 0 -38 27311.6 2473.58 2 12 0 -36 45850.8 2557.95 2 12 0 -34 8248.26 2165.22 2 12 0 -32 2600.85 2097.05 2 12 0 -30 7945.09 2430.91 2 12 0 -28 58607.1 2968.84 2 12 0 -26 42230.1 1978.17 2 12 0 -24 1712.83 1524.84 2 12 0 -22 40382.7 1827.99 2 12 0 -20 4500.76 1521.69 2 12 0 -18 22879.1 1714.41 2 12 0 -16 9951.71 1571.17 2 12 0 -14 1967.78 1444.22 2 12 0 -12 59333.2 1708.01 2 12 0 -10 34393.1 1895.73 2 12 0 -8 68.2044 1228.41 2 12 0 -6 4054.37 1334.18 2 12 1 -33 763.762 2616.92 2 12 1 -28 1734.09 2110.97 2 12 1 -27 24682.9 2308.09 2 12 -1 -24 45033.6 2289.05 2 12 1 -23 1598.46 1920.42 2 12 1 -21 15404.6 1960.61 2 12 -1 -20 403.456 1448.40 2 12 1 -19 14350.9 1959.81 2 12 1 -18 3167.83 1659.25 2 12 -1 -15 509.448 967.414 2 12 -1 -14 20291.6 1172.13 2 12 -1 -13 3062.88 988.318 2 12 -1 -12 3872.75 969.765 2 12 -1 -11 25506.9 1206.28 2 12 1 -10 4286.53 966.713 2 12 -1 -9 1836.57 950.856 2 12 -1 -8 18002.4 1089.10 2 12 1 -7-388.252 1444.00 2 12 1 -6 18447.6 1706.83 2 12 1 -5-101.341 1438.10 2 12 2 -34 2562.12 2911.17 2 12 2 -26 7909.65 2183.48 2 12 -2 -23 35552.8 2168.87 2 12 2 -19 3214.00 1758.05 2 12 -2 -17 31486.7 1674.74 2 12 2 -15 11114.8 1817.22 2 12 -2 -14 1529.80 976.076 2 12 2 -13 23320.0 1867.14 2 12 -2 -12 2550.49 1189.48 2 12 -2 -11 976.295 1118.70 2 12 -2 -10 5146.10 917.880 2 12 -2 -9 15011.7 1025.14 2 12 2 -8 2286.86 1514.54 2 12 2 -7 58342.3 2149.70 2 12 2 -6 580.981 1585.99 2 12 2 -5 8507.73 1721.73 2 12 2 -4 110.443 1541.44 2 12 2 -3 2663.94 346.715 2 12 3 -23 7638.05 2156.32 2 12 3 -20 5140.99 2067.95 2 12 3 -16 1008.66 1835.91 2 12 -3 -14 1722.49 908.790 2 12 -3 -13 15574.9 1024.48 2 12 -3 -12 271.476 1045.12 2 12 -3 -11 33135.9 1170.48 2 12 3 -8 7057.55 1708.57 2 12 3 -6 2506.71 1695.17 2 12 3 -4 818.998 1591.52 2 12 3 -3 27007.7 1957.42 2 12 3 -2 111.125 456.451 2 12 4 -32 2816.51 2454.65 2 12 4 -21-295.226 2166.45 2 12 4 -18 27210.5 2319.59 2 12 4 -15 16234.5 2191.79 2 12 -4 -14 7234.02 1095.57 2 12 -4 -13 3796.01 835.848 2 12 -4 -12 18470.7 1038.11 2 12 4 -11 537.041 1808.57 2 12 4 -9 12569.2 1864.50 2 12 4 -7 5153.46 1830.65 2 12 4 -3 2051.06 1681.52 2 12 4 -2 30632.3 2096.27 2 12 4 -1 850.607 1788.97 2 12 4 0 4722.60 741.621 2 12 5 -19 1671.92 2135.82 2 12 5 -16 34899.2 2502.29 2 12 5 -13 443.980 1911.35 2 12 5 -10-294.095 1753.42 2 12 5 -7 3625.56 1858.30 2 12 5 -2-386.939 1819.30 2 12 5 -1 2845.79 1909.35 2 12 5 0 8105.06 2005.77 2 12 5 1 1657.19 1915.32 2 12 5 2 25746.6 2269.21 2 12 6 -15 11149.4 2177.90 2 12 6 -14 4559.37 2162.43 2 12 6 -9 3580.28 1922.44 2 12 6 -2 10571.5 2046.02 2 12 6 -1 6208.87 2024.25 2 12 6 0 3226.74 1949.68 2 12 6 1 4126.64 1876.94 2 12 6 2 693.779 1826.31 2 12 6 3 4027.11 1908.33 2 12 7 -18-951.935 2240.97 2 12 7 -16 10293.1 2530.41 2 12 7 2 965.649 2071.40 2 12 7 3 871.838 1861.96 2 12 7 4 954.039 1944.48 2 12 7 5 23739.7 2508.06 2 12 8 3 20895.6 2440.46 2 12 8 4 2028.47 2307.03 2 12 8 5 4971.45 2386.18 2 12 8 6-261.752 2035.53 2 12 9 4 1558.44 2353.97 2 12 9 5 2674.40 2277.58 2 12 9 6 1155.23 2315.76 2 12 9 7 1516.74 2281.54 2 12 9 8 144.341 2399.96 2 12 10 6 6475.46 2612.35 2 12 10 7 332.955 2380.80 2 12 10 8 4573.08 2389.00 2 12 10 9 51.3771 2579.50 2 13 0 -17 494.374 1544.71 2 13 0 -7 1070.88 1392.97 2 13 0 -5 332.842 1450.22 2 13 0 -3 954.663 1423.77 2 13 0 -1 934.204 1483.32 2 13 0 1 1583.84 815.118 2 -13 0 -3 1452.05 877.677 2 -13 0 -5 1931.83 921.447 2 -13 0 -7 224.737 927.687 2 -13 0 -9 8964.42 1112.28 2 -13 0 -11 8524.73 1149.83 2 -13 0 -13 1764.70 1124.99 2 -13 0 -15-188.729 1238.38 2 -13 0 -17 6564.34 1342.89 2 -13 0 -19 8608.56 1467.94 2 -13 0 -21 3296.48 1503.63 2 -13 0 -23 648.465 1503.73 2 -13 0 -25 4051.84 1590.81 2 -13 0 -27 4951.14 1688.45 2 -13 0 -29 2454.39 1836.05 2 13 1 -32 2615.69 2642.33 2 13 1 -31 8433.78 2603.44 2 13 1 -17 9378.10 1806.24 2 13 1 -14 499.782 1565.98 2 13 1 -13 7789.64 1710.71 2 13 1 -12 17941.9 1746.44 2 13 -1 -11 199.964 1357.48 2 13 -1 -9 3521.35 1380.71 2 13 -1 -8 7126.54 1082.96 2 13 1 -7 1747.90 1500.05 2 13 -1 -6 482.507 960.604 2 13 -1 -4 7570.89 1407.69 2 13 -1 -3 3427.54 1381.41 2 13 -1 -2 3495.60 1054.42 2 13 -1 -1 3860.18 800.304 2 -13 1 0 9144.00 875.715 2 13 -1 1 7660.05 802.020 2 13 1 2 422.245 1536.49 2 13 1 3 5101.65 1673.82 2 13 1 4 3928.66 889.314 2 13 2 -27 27980.6 2609.07 2 13 2 -20 3793.33 2038.98 2 13 2 -14 752.106 1729.60 2 13 -2 -13 7345.58 1363.89 2 13 2 -12 1095.91 1679.54 2 13 -2 -11 32090.4 1255.22 2 13 -2 -8 915.357 1207.74 2 13 -2 -7 5520.31 1253.00 2 13 2 -6 2773.22 1712.01 2 13 -2 -4 2744.12 1267.07 2 13 -2 -3 8872.97 1375.65 2 13 -2 -2 5316.55 1352.69 2 -13 2 1 12857.7 928.304 2 13 -2 0 831.100 800.568 2 13 2 2 6239.94 1688.30 2 13 2 3 978.523 1691.11 2 13 2 4 1332.07 1765.36 2 13 2 5 3276.41 1813.69 2 13 2 6 5518.56 1968.88 2 13 3 -22 3189.53 2251.85 2 13 3 -19 325.485 1913.75 2 13 3 -16 1537.94 1932.85 2 13 3 -14 2364.69 1859.29 2 13 3 -12 3590.94 1862.35 2 13 3 -10 1315.48 1718.49 2 13 -3 -8 864.300 1088.60 2 13 -3 -7 13370.9 1228.38 2 13 -3 -6 897.203 1118.46 2 13 -3 -5 24455.8 1311.76 2 13 -3 -4 3777.78 1099.72 2 13 3 -3 4925.33 962.054 2 13 -3 -2 6029.99 1210.26 2 13 3 0 3599.86 1753.11 2 13 3 4 2423.81 1857.59 2 13 3 5 2333.69 1878.98 2 13 3 6 1582.85 1844.55 2 13 4 -24 20608.9 2638.75 2 13 4 -15-112.387 2047.89 2 13 4 -12 2304.66 1987.49 2 13 4 -6 20378.4 2152.15 2 13 4 -2 4929.75 1928.24 2 13 4 5 1198.83 1812.83 2 13 4 6 1307.20 1849.34 2 13 4 7 3354.37 2046.21 2 13 5 -23 1509.64 2383.59 2 13 5 -22 3474.69 2415.03 2 13 5 -16 3555.28 2143.56 2 13 5 -11 4595.16 2067.32 2 13 5 -6 319.120 1897.99 2 13 5 7 3370.76 2099.52 2 13 5 8 3607.18 2210.59 2 13 6 -13 3230.35 2186.74 2 13 6 8 1276.63 2242.33 2 13 6 9 2307.43 2043.86 2 13 7 9 9811.13 2316.84 2 13 7 10 6137.97 2551.80 2 13 7 11 1154.33 2334.22 2 13 8 11 1790.48 2599.69 2 13 8 12 1633.32 2485.29 2 13 8 13 1323.19 2415.50 2 14 0 -32 5377.20 2202.35 2 14 0 -30 2310.59 2201.96 2 14 0 -28 61055.9 2318.13 2 14 0 -26 13853.3 1825.24 2 14 0 -24 3374.40 1673.01 2 14 0 -22 2111.19 1707.03 2 14 0 -20 30729.3 1884.49 2 14 0 -18 20219.4 1854.34 2 14 0 -16 2033.75 1615.84 2 14 0 -14 2256.00 1560.87 2 14 0 -12 8339.79 1636.60 2 14 0 -10 47270.0 1834.40 2 14 0 -8 7459.32 1601.81 2 14 0 -6 665.381 1523.14 2 14 0 -4 6357.13 1653.16 2 14 0 -2 5308.97 1652.25 2 14 0 0 6558.84 1651.61 2 14 0 2 2681.66 1607.36 2 14 0 4 5104.23 1648.22 2 14 0 6 29271.7 1951.22 2 14 1 -17 2671.84 1805.79 2 14 1 -12 4058.44 1709.19 2 14 -1 -8 11849.9 1605.72 2 14 -1 -7 10.1638 1413.88 2 14 1 -5 2260.81 1641.70 2 14 -1 6 2039.88 1712.18 2 14 2 -15 19600.7 2138.10 2 14 2 -11 232.970 1817.26 2 14 2 -9 5963.45 1805.88 2 14 -2 -8 5156.98 1344.69 2 14 -2 -6-193.128 1298.70 2 14 -2 4-16.3715 1474.93 2 14 -2 5 39.3717 1506.00 2 14 -2 6 6289.78 1657.26 2 14 -2 7 3684.24 1658.17 2 -14 4 -6 3688.96 1720.09 2 -14 5 -3 150.750 1596.60 2 -14 5 -4 1335.47 1654.96 2 15 0 -9 456.569 1636.29 2 ; _shelx_hkl_checksum 5835 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3d _database_code_depnum_ccdc_archive 'CCDC 2116005' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT230_3d ; PROBLEM: Hirshfeld Test Diff for C01Y --C022 . 9.0 s.u. RESPONSE: A consequence of a small crystal sample and a lack of high angle data. This has no significant effect on any aspect of the structure. ; # Added during the CSD deposition process: Friday 15 October 2021 05:10 PM # end Validation Reply Form _audit_creation_date 2021-10-15 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _shelx_SHELXL_version_number 2018/3 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C67 H90 Cr Mg2 N4 O3' _chemical_formula_sum 'C67 H90 Cr Mg2 N4 O3' _chemical_formula_weight 1100.04 _chemical_melting_point ? _chemical_oxdiff_formula 'C67 H91 Cr1 Mg2 N4 O3' _chemical_oxdiff_usercomment JMP-084 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr -0.1635 2.4439 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.1719 0.1771 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 15.3628(2) _cell_length_b 12.9497(2) _cell_length_c 35.8850(6) _cell_angle_alpha 90 _cell_angle_beta 99.436(2) _cell_angle_gamma 90 _cell_volume 7042.50(19) _cell_formula_units_Z 4 _cell_measurement_reflns_used 6270 _cell_measurement_temperature 173.00(14) _cell_measurement_theta_max 72.7450 _cell_measurement_theta_min 4.4730 _shelx_estimated_absorpt_T_max 0.810 _shelx_estimated_absorpt_T_min 0.771 _exptl_absorpt_coefficient_mu 1.829 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.97620 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear orange' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier . _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.038 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 2368 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.12 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0362 _diffrn_reflns_av_unetI/netI 0.0515 _diffrn_reflns_Laue_measured_fraction_full 0.985 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 43 _diffrn_reflns_limit_l_min -43 _diffrn_reflns_number 23388 _diffrn_reflns_point_group_measured_fraction_full 0.985 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.375 _diffrn_reflns_theta_min 3.515 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 173.00(14) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.4115 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.985 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 18.00 104.00 1.00 15.20 -- 42.36 38.00 30.00 86 2 \w 86.00 133.00 1.00 73.92 -- 105.13 -30.00 -30.00 47 3 \w 86.00 174.00 1.00 73.92 -- 105.13 30.00 -60.00 88 4 \w 73.00 178.00 1.00 73.92 -- 105.13 77.00 -30.00 105 5 \w 28.00 109.00 1.00 73.92 -- 105.13 -95.00 -90.00 81 6 \w 29.00 64.00 1.00 73.92 -- 105.13 -30.00 -30.00 35 7 \w 6.00 98.00 1.00 15.20 -- 42.36-125.00-120.00 92 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Atlas, Ultra' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0708528000 _diffrn_orient_matrix_UB_12 0.0482582000 _diffrn_orient_matrix_UB_13 0.0204516000 _diffrn_orient_matrix_UB_21 -0.0628274000 _diffrn_orient_matrix_UB_22 -0.0901498000 _diffrn_orient_matrix_UB_23 -0.0133587000 _diffrn_orient_matrix_UB_31 0.0369898000 _diffrn_orient_matrix_UB_32 -0.0607422000 _diffrn_orient_matrix_UB_33 0.0360194000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance Ultra (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 9836 _reflns_number_total 13503 _reflns_odcompleteness_completeness 98.48 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.49 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.343 _refine_diff_density_min -0.517 _refine_diff_density_rms 0.045 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 727 _refine_ls_number_reflns 13503 _refine_ls_number_restraints 12 _refine_ls_R_factor_all 0.0724 _refine_ls_R_factor_gt 0.0517 _refine_ls_restrained_S_all 1.030 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0844P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1388 _refine_ls_wR_factor_ref 0.1558 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints C1 \\sim C01U \\sim C2 \\sim C01S: within 1A with sigma of 0.01 and sigma for terminal atoms of 0.01 within 1A 3. Others Sof(C1)=Sof(H1A)=Sof(C2)=1-FVAR(1) Sof(C01S)=Sof(H6)=Sof(C01U)=FVAR(1) 4.a Ternary CH refined with riding coordinates: C00U(H00U), C00V(H00V), C00W(H00W), C00Z(H00Z), C010(H010), C015(H015), C01B(H01H), C01J(H01W) 4.b Aromatic/amide H refined with riding coordinates: C00I(H00I), C00M(H00M), C00N(H00N), C00S(H00S), C00X(H00X), C00Y(H00Y), C011(H011), C014(H014), C017(H017), C018(H018), C019(H019), C01A(H01G), C01E(H01L), C01F(H01M), C01M(H01), C01S(H6), C01T(H7), C01V(H8), C01X(H10), C01Y(H11), C022(H022), C1(H1A) 4.c Idealised Me refined as rotating group: C013(H01A,H01B,H01C), C016(H01D,H01E,H01F), C01D(H01I,H01J,H01K), C01G(H01N, H01O,H01P), C01H(H01Q,H01R,H01S), C01I(H01T,H01U,H01V), C01K(H01X,H01Y,H), C01L(H01Z,HA,HB), C01N(H1,HC,HD), C01O(H2,HE,HF), C01P(H3,HG,HH), C01Q(H4,HI, HJ), C01R(H5,HK,HL), C01W(H9,HM,HN), C01Z(H12,HO,HP), C020(H02A,H02B,H02C), C021(H02D,H02E,H02F), C023(H02G,H02H,H02I), C024(H02J,H02K,H02L), C025(H02M, H02N,H02O) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cr01 Cr 0.76128(3) 0.40338(3) 0.58906(2) 0.04274(12) Uani 1 1 d . . . . . Mg02 Mg 0.62090(5) 0.66209(5) 0.64732(2) 0.03353(16) Uani 1 1 d . . . . . Mg03 Mg 0.81180(5) 0.74841(6) 0.61426(2) 0.03599(16) Uani 1 1 d . . . . . O004 O 0.63041(12) 0.53646(13) 0.61800(5) 0.0459(4) Uani 1 1 d . . . . . O005 O 0.84946(12) 0.60389(13) 0.61164(5) 0.0485(4) Uani 1 1 d . . . . . N006 N 0.51337(11) 0.75720(14) 0.64397(5) 0.0344(4) Uani 1 1 d . . . . . N007 N 0.88623(13) 0.86160(15) 0.64423(5) 0.0394(4) Uani 1 1 d . . . . . N008 N 0.82572(13) 0.80971(15) 0.56303(5) 0.0388(4) Uani 1 1 d . . . . . N009 N 0.60174(12) 0.59981(14) 0.69771(5) 0.0358(4) Uani 1 1 d . . . . . C00A C 0.47626(15) 0.77927(18) 0.67420(7) 0.0397(5) Uani 1 1 d . . . . . C00B C 0.47370(14) 0.79781(18) 0.60802(6) 0.0374(5) Uani 1 1 d . . . . . C00C C 0.58423(16) 0.41180(18) 0.69781(7) 0.0425(5) Uani 1 1 d . . . . . C00D C 0.63601(15) 0.49940(17) 0.70952(6) 0.0369(5) Uani 1 1 d . . . . . C00E C 0.74149(17) 0.72542(19) 0.50614(7) 0.0456(5) Uani 1 1 d . . . . . C00F C 0.92074(15) 0.84642(19) 0.68387(7) 0.0421(5) Uani 1 1 d . . . . . C00G C 0.55618(16) 0.64948(18) 0.72067(6) 0.0414(5) Uani 1 1 d . . . . . C00H C 0.40802(15) 0.7401(2) 0.58524(7) 0.0438(5) Uani 1 1 d . . . . . C00I C 0.50286(17) 0.73546(19) 0.71008(7) 0.0445(5) Uani 1 1 d . . . . . H00I H 0.481780 0.768729 0.729770 0.053 Uiso 1 1 calc R U . . . C00J C 0.71988(16) 0.48930(19) 0.73161(6) 0.0417(5) Uani 1 1 d . . . . . C00K C 0.50312(16) 0.89200(18) 0.59493(7) 0.0436(5) Uani 1 1 d . . . . . C00L C 0.82188(16) 0.74560(18) 0.53001(6) 0.0410(5) Uani 1 1 d . . . . . C00M C 0.61742(19) 0.3154(2) 0.71038(8) 0.0506(6) Uani 1 1 d . . . . . H00M H 0.584589 0.256479 0.702823 0.061 Uiso 1 1 calc R U . . . C00N C 0.7430(2) 0.6647(2) 0.47424(7) 0.0524(6) Uani 1 1 d . . . . . H00N H 0.690334 0.651758 0.458065 0.063 Uiso 1 1 calc R U . . . C00O C 0.84689(17) 0.90871(19) 0.55950(7) 0.0440(5) Uani 1 1 d . . . . . C00P C 0.87382(17) 0.8837(2) 0.71183(7) 0.0482(6) Uani 1 1 d . . . . . C00Q C 0.89975(16) 0.95232(18) 0.62875(7) 0.0446(5) Uani 1 1 d . . . . . O00R O 0.8234(2) 0.3217(3) 0.66671(7) 0.0969(9) Uani 1 1 d . . . . . C00S C 0.74812(18) 0.3907(2) 0.74390(7) 0.0494(6) Uani 1 1 d . . . . . H00S H 0.802525 0.383080 0.759384 0.059 Uiso 1 1 calc R U . . . C00T C 0.99940(16) 0.7903(2) 0.69361(7) 0.0479(6) Uani 1 1 d . . . . . C00U C 0.57329(19) 0.9576(2) 0.61851(8) 0.0518(6) Uani 1 1 d . . . . . H00U H 0.597529 0.918064 0.641120 0.062 Uiso 1 1 calc R U . . . C00V C 0.78067(18) 0.5802(2) 0.74042(8) 0.0521(6) Uani 1 1 d . . . . . H00V H 0.744468 0.642947 0.737604 0.063 Uiso 1 1 calc R U . . . C00W C 0.49484(18) 0.4208(2) 0.67269(8) 0.0539(6) Uani 1 1 d . . . . . H00W H 0.496122 0.483455 0.657492 0.065 Uiso 1 1 calc R U . . . C00X C 0.87527(17) 0.97449(19) 0.59000(8) 0.0478(6) Uani 1 1 d . . . . . H00X H 0.878496 1.043891 0.583699 0.057 Uiso 1 1 calc R U . . . C00Y C 0.69764(19) 0.3053(2) 0.73370(8) 0.0534(6) Uani 1 1 d . . . . . H00Y H 0.717386 0.240474 0.742486 0.064 Uiso 1 1 calc R U . . . C00Z C 0.37778(18) 0.6365(2) 0.59799(8) 0.0543(6) Uani 1 1 d . . . . . H00Z H 0.405493 0.625667 0.624296 0.065 Uiso 1 1 calc R U . . . C010 C 0.65486(17) 0.7664(2) 0.51502(7) 0.0494(6) Uani 1 1 d . . . . . H010 H 0.668552 0.819395 0.534613 0.059 Uiso 1 1 calc R U . . . C011 C 0.37138(18) 0.7789(2) 0.54969(8) 0.0550(7) Uani 1 1 d . . . . . H011 H 0.327357 0.741564 0.534566 0.066 Uiso 1 1 calc R U . . . C012 C 0.90092(18) 0.7024(2) 0.52206(7) 0.0492(6) Uani 1 1 d . . . . . C013 C 0.3982(2) 0.8517(2) 0.67084(9) 0.0600(7) Uani 1 1 d . . . . . H01A H 0.412840 0.915818 0.659989 0.090 Uiso 1 1 calc R U . . . H01B H 0.383573 0.864132 0.695456 0.090 Uiso 1 1 calc R U . . . H01C H 0.348558 0.820982 0.654955 0.090 Uiso 1 1 calc R U . . . C014 C 0.4652(2) 0.9265(2) 0.55888(8) 0.0565(7) Uani 1 1 d . . . . . H014 H 0.484743 0.988028 0.549722 0.068 Uiso 1 1 calc R U . . . C015 C 1.04692(17) 0.7447(2) 0.66328(8) 0.0539(6) Uani 1 1 d . . . . . H015 H 1.001554 0.726951 0.641727 0.065 Uiso 1 1 calc R U . . . C016 C 0.5587(2) 0.6111(2) 0.76080(8) 0.0613(8) Uani 1 1 d . . . . . H01D H 0.545211 0.538740 0.760401 0.092 Uiso 1 1 calc R U . . . H01E H 0.516077 0.648215 0.772370 0.092 Uiso 1 1 calc R U . . . H01F H 0.616572 0.622231 0.775026 0.092 Uiso 1 1 calc R U . . . C017 C 0.8980(2) 0.6416(2) 0.48983(8) 0.0577(7) Uani 1 1 d . . . . . H017 H 0.949882 0.612721 0.484382 0.069 Uiso 1 1 calc R U . . . C018 C 0.8201(2) 0.6233(2) 0.46591(8) 0.0588(7) Uani 1 1 d . . . . . H018 H 0.819417 0.583339 0.444331 0.071 Uiso 1 1 calc R U . . . C019 C 1.03270(18) 0.7774(2) 0.73190(8) 0.0575(7) Uani 1 1 d . . . . . H019 H 1.085003 0.741051 0.738975 0.069 Uiso 1 1 calc R U . . . C01A C 0.9115(2) 0.8686(3) 0.74946(8) 0.0603(7) Uani 1 1 d . . . . . H01G H 0.882633 0.893932 0.768396 0.072 Uiso 1 1 calc R U . . . C01B C 0.78477(19) 0.9357(2) 0.70253(8) 0.0542(6) Uani 1 1 d . . . . . H01H H 0.769112 0.939007 0.674965 0.065 Uiso 1 1 calc R U . . . C01C C 0.7975(2) 0.3532(3) 0.63726(8) 0.0613(7) Uani 1 1 d . . . . . C01D C 0.8404(2) 0.9562(2) 0.52046(8) 0.0621(7) Uani 1 1 d . . . . . H01I H 0.879944 0.921095 0.506635 0.093 Uiso 1 1 calc R U . . . H01J H 0.855978 1.027964 0.522806 0.093 Uiso 1 1 calc R U . . . H01K H 0.781010 0.949585 0.507245 0.093 Uiso 1 1 calc R U . . . C01E C 0.3993(2) 0.8712(2) 0.53670(8) 0.0624(8) Uani 1 1 d . . . . . H01L H 0.373918 0.896103 0.513103 0.075 Uiso 1 1 calc R U . . . C01F C 0.9898(2) 0.8174(3) 0.75933(8) 0.0648(8) Uani 1 1 d . . . . . H01M H 1.013934 0.809608 0.784686 0.078 Uiso 1 1 calc R U . . . C01G C 0.9461(2) 1.0400(2) 0.65215(9) 0.0616(7) Uani 1 1 d . . . . . H01N H 0.961240 1.018364 0.677987 0.092 Uiso 1 1 calc R U . . . H01O H 0.907535 1.098727 0.650700 0.092 Uiso 1 1 calc R U . . . H01P H 0.998777 1.058371 0.642559 0.092 Uiso 1 1 calc R U . . . C01H C 0.6487(2) 0.9842(3) 0.59777(10) 0.0693(8) Uani 1 1 d . . . . . H01Q H 0.673060 0.921776 0.589320 0.104 Uiso 1 1 calc R U . . . H01R H 0.693597 1.020563 0.614476 0.104 Uiso 1 1 calc R U . . . H01S H 0.627250 1.026919 0.576381 0.104 Uiso 1 1 calc R U . . . C01I C 0.4064(2) 0.5496(2) 0.57438(10) 0.0701(8) Uani 1 1 d . . . . . H01T H 0.377815 0.557047 0.548657 0.105 Uiso 1 1 calc R U . . . H01U H 0.390288 0.484475 0.584099 0.105 Uiso 1 1 calc R U . . . H01V H 0.469213 0.552142 0.575454 0.105 Uiso 1 1 calc R U . . . C01J C 0.98891(19) 0.7205(3) 0.54747(9) 0.0598(7) Uani 1 1 d . . . . . H01W H 0.976670 0.756543 0.570060 0.072 Uiso 1 1 calc R U . . . C01K C 0.7139(2) 0.8739(3) 0.71736(9) 0.0655(8) Uani 1 1 d . . . . . H01X H 0.710468 0.806063 0.706403 0.098 Uiso 1 1 calc R U . . . H01Y H 0.658019 0.908031 0.710712 0.098 Uiso 1 1 calc R U . . . H H 0.728242 0.868364 0.744347 0.098 Uiso 1 1 calc R U . . . C01L C 0.5980(3) 0.8165(3) 0.48104(11) 0.0856(12) Uani 1 1 d . . . . . H01Z H 0.632575 0.865938 0.469887 0.128 Uiso 1 1 calc R U . . . HA H 0.548800 0.850795 0.489045 0.128 Uiso 1 1 calc R U . . . HB H 0.576745 0.764413 0.462767 0.128 Uiso 1 1 calc R U . . . C01M C 0.7590(3) 0.2416(2) 0.56757(10) 0.0709(9) Uani 1 1 d . . . . . H01 H 0.762648 0.179819 0.580930 0.085 Uiso 1 1 calc R U . . . C01N C 0.4202(2) 0.4334(3) 0.69540(13) 0.0830(11) Uani 1 1 d . . . . . H1 H 0.420280 0.375986 0.712322 0.124 Uiso 1 1 calc R U . . . HC H 0.364896 0.435903 0.678537 0.124 Uiso 1 1 calc R U . . . HD H 0.428443 0.496340 0.709691 0.124 Uiso 1 1 calc R U . . . C01O C 0.4755(3) 0.3312(3) 0.64546(11) 0.0832(11) Uani 1 1 d . . . . . H2 H 0.522372 0.324550 0.630941 0.125 Uiso 1 1 calc R U . . . HE H 0.420896 0.343569 0.628799 0.125 Uiso 1 1 calc R U . . . HF H 0.470829 0.268699 0.659393 0.125 Uiso 1 1 calc R U . . . C01P C 0.8430(2) 0.5852(3) 0.71159(11) 0.0762(9) Uani 1 1 d . . . . . H3 H 0.881178 0.526065 0.714518 0.114 Uiso 1 1 calc R U . . . HG H 0.877772 0.647012 0.715487 0.114 Uiso 1 1 calc R U . . . HH H 0.809287 0.585634 0.686568 0.114 Uiso 1 1 calc R U . . . C01Q C 1.0346(2) 0.6196(3) 0.56047(12) 0.0804(10) Uani 1 1 d . . . . . H4 H 0.994538 0.576119 0.571179 0.121 Uiso 1 1 calc R U . . . HI H 1.085445 0.633715 0.579157 0.121 Uiso 1 1 calc R U . . . HJ H 1.052660 0.585365 0.539275 0.121 Uiso 1 1 calc R U . . . C01R C 0.6029(2) 0.6821(3) 0.53063(11) 0.0737(9) Uani 1 1 d . . . . . H5 H 0.585746 0.630873 0.511505 0.111 Uiso 1 1 calc R U . . . HK H 0.551081 0.711336 0.538244 0.111 Uiso 1 1 calc R U . . . HL H 0.638757 0.650694 0.552051 0.111 Uiso 1 1 calc R U . . . C01S C 0.8493(10) 0.5108(7) 0.6043(2) 0.058(2) Uiso 0.449(16) 1 d . U P A 1 H6 H 0.906386 0.484814 0.606662 0.070 Uiso 0.449(16) 1 calc R U P A 1 C01T C 0.6787(3) 0.2839(3) 0.55505(10) 0.0763(9) Uani 1 1 d . . . . . H7 H 0.627742 0.250088 0.559244 0.092 Uiso 1 1 calc R U . . . C01U C 0.6866(7) 0.4813(6) 0.6080(2) 0.0455(18) Uiso 0.449(16) 1 d . U P A 1 C01V C 0.8360(3) 0.2891(3) 0.56077(12) 0.0825(11) Uani 1 1 d . . . . . H8 H 0.890847 0.259851 0.569437 0.099 Uiso 1 1 calc R U . . . C01W C 0.8330(3) 0.5794(3) 0.78061(10) 0.0941(13) Uani 1 1 d . . . . . H9 H 0.793424 0.568471 0.798340 0.141 Uiso 1 1 calc R U . . . HM H 0.862633 0.644339 0.785745 0.141 Uiso 1 1 calc R U . . . HN H 0.875788 0.524712 0.782927 0.141 Uiso 1 1 calc R U . . . C01X C 0.6725(3) 0.3793(3) 0.53564(10) 0.0887(13) Uani 1 1 d . . . . . H10 H 0.617486 0.409521 0.528179 0.106 Uiso 1 1 calc R U . . . C01Y C 0.7458(4) 0.4272(3) 0.52777(10) 0.0887(13) Uani 1 1 d . . . . . H11 H 0.741212 0.488580 0.514161 0.106 Uiso 1 1 calc R U . . . C01Z C 0.7843(3) 1.0465(3) 0.71782(14) 0.0932(12) Uani 1 1 d . . . . . H12 H 0.798535 1.045327 0.744883 0.140 Uiso 1 1 calc R U . . . HO H 0.726766 1.076147 0.710416 0.140 Uiso 1 1 calc R U . . . HP H 0.827164 1.087131 0.707717 0.140 Uiso 1 1 calc R U . . . C020 C 1.1076(2) 0.8237(3) 0.64931(11) 0.0781(10) Uani 1 1 d . . . . . H02A H 1.074448 0.884540 0.640848 0.117 Uiso 1 1 calc R U . . . H02B H 1.132436 0.794861 0.628750 0.117 Uiso 1 1 calc R U . . . H02C H 1.154212 0.841517 0.669526 0.117 Uiso 1 1 calc R U . . . C021 C 1.0501(3) 0.7890(3) 0.52908(13) 0.0903(12) Uani 1 1 d . . . . . H02D H 1.060896 0.757540 0.506036 0.135 Uiso 1 1 calc R U . . . H02E H 1.104971 0.797301 0.545955 0.135 Uiso 1 1 calc R U . . . H02F H 1.023103 0.855287 0.523619 0.135 Uiso 1 1 calc R U . . . C022 C 0.8290(4) 0.3828(3) 0.54042(12) 0.0984(16) Uani 1 1 d . . . . . H022 H 0.879732 0.415475 0.535353 0.118 Uiso 1 1 calc R U . . . C023 C 0.5350(3) 1.0577(3) 0.63133(14) 0.0980(14) Uani 1 1 d . . . . . H02G H 0.511327 1.098218 0.609623 0.147 Uiso 1 1 calc R U . . . H02H H 0.580725 1.096018 0.646880 0.147 Uiso 1 1 calc R U . . . H02I H 0.488986 1.041910 0.645560 0.147 Uiso 1 1 calc R U . . . C024 C 1.0961(3) 0.6471(4) 0.67556(14) 0.1013(14) Uani 1 1 d . . . . . H02J H 1.143820 0.662233 0.695624 0.152 Uiso 1 1 calc R U . . . H02K H 1.119185 0.617977 0.654586 0.152 Uiso 1 1 calc R U . . . H02L H 1.056712 0.598553 0.684307 0.152 Uiso 1 1 calc R U . . . C025 C 0.2774(3) 0.6325(4) 0.59614(17) 0.1086(16) Uani 1 1 d . . . . . H02M H 0.259022 0.688387 0.610612 0.163 Uiso 1 1 calc R U . . . H02N H 0.261271 0.567986 0.606322 0.163 Uiso 1 1 calc R U . . . H02O H 0.248998 0.638499 0.570330 0.163 Uiso 1 1 calc R U . . . HQ H 0.7116(12) 0.7380(15) 0.6334(5) 0.012(4) Uiso 1 1 d . . . . . C1 C 0.6523(7) 0.4598(6) 0.60205(19) 0.0512(18) Uani 0.551(16) 1 d . U P A 2 H1A H 0.604365 0.416852 0.593943 0.061 Uiso 0.551(16) 1 calc R U P A 2 C2 C 0.8108(6) 0.5219(4) 0.60149(14) 0.0439(15) Uani 0.551(16) 1 d . U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cr01 0.0566(2) 0.0314(2) 0.0435(2) -0.00075(16) 0.01809(17) 0.00316(16) Mg02 0.0327(3) 0.0340(4) 0.0341(3) 0.0024(3) 0.0060(3) 0.0048(3) Mg03 0.0381(4) 0.0346(4) 0.0347(3) -0.0006(3) 0.0043(3) -0.0058(3) O004 0.0523(10) 0.0400(9) 0.0471(9) -0.0075(7) 0.0134(7) 0.0018(7) O005 0.0531(10) 0.0366(9) 0.0566(10) -0.0007(8) 0.0111(8) 0.0001(7) N006 0.0335(9) 0.0318(9) 0.0371(9) -0.0011(7) 0.0031(7) 0.0034(7) N007 0.0397(10) 0.0377(10) 0.0397(10) -0.0043(8) 0.0031(7) -0.0047(8) N008 0.0420(10) 0.0372(10) 0.0376(9) -0.0017(8) 0.0077(7) -0.0024(8) N009 0.0399(10) 0.0311(9) 0.0371(9) 0.0019(7) 0.0088(7) 0.0053(7) C00A 0.0401(12) 0.0357(11) 0.0440(12) -0.0025(9) 0.0089(9) 0.0081(9) C00B 0.0322(10) 0.0402(12) 0.0380(11) -0.0023(9) 0.0004(8) 0.0094(9) C00C 0.0467(13) 0.0387(12) 0.0453(12) 0.0059(10) 0.0173(10) -0.0001(10) C00D 0.0462(12) 0.0318(11) 0.0351(10) 0.0035(8) 0.0136(9) 0.0056(9) C00E 0.0557(14) 0.0381(12) 0.0413(12) 0.0048(10) 0.0031(10) -0.0016(10) C00F 0.0407(12) 0.0409(12) 0.0420(12) -0.0028(10) -0.0011(9) -0.0118(9) C00G 0.0502(13) 0.0399(12) 0.0359(11) 0.0004(9) 0.0122(9) 0.0058(10) C00H 0.0350(11) 0.0471(13) 0.0475(13) -0.0053(10) 0.0016(9) 0.0046(10) C00I 0.0526(14) 0.0420(12) 0.0412(12) -0.0031(10) 0.0145(10) 0.0132(10) C00J 0.0484(13) 0.0394(12) 0.0381(11) 0.0037(9) 0.0100(9) 0.0093(10) C00K 0.0493(13) 0.0338(11) 0.0457(12) 0.0022(10) 0.0024(10) 0.0083(10) C00L 0.0524(13) 0.0376(12) 0.0336(11) 0.0061(9) 0.0086(9) -0.0015(10) C00M 0.0609(16) 0.0355(12) 0.0595(15) 0.0063(11) 0.0220(12) -0.0021(11) C00N 0.0684(17) 0.0453(14) 0.0406(12) 0.0001(11) 0.0006(11) -0.0045(12) C00O 0.0494(13) 0.0389(12) 0.0443(12) 0.0047(10) 0.0096(10) -0.0007(10) C00P 0.0513(14) 0.0480(14) 0.0433(12) -0.0082(11) 0.0018(10) -0.0117(11) C00Q 0.0429(12) 0.0355(12) 0.0538(14) -0.0017(10) 0.0035(10) -0.0068(9) O00R 0.101(2) 0.123(2) 0.0626(15) 0.0214(15) 0.0024(13) 0.0212(18) C00S 0.0518(14) 0.0453(14) 0.0518(14) 0.0094(11) 0.0109(11) 0.0141(11) C00T 0.0380(12) 0.0520(14) 0.0514(14) 0.0022(11) 0.0001(10) -0.0094(10) C00U 0.0606(16) 0.0382(13) 0.0533(14) 0.0030(11) 0.0001(12) -0.0035(11) C00V 0.0540(15) 0.0447(14) 0.0526(14) 0.0036(11) -0.0061(11) 0.0039(11) C00W 0.0549(15) 0.0423(13) 0.0631(16) 0.0121(12) 0.0050(12) -0.0066(11) C00X 0.0526(14) 0.0345(12) 0.0558(14) 0.0050(10) 0.0078(11) -0.0070(10) C00Y 0.0647(17) 0.0373(13) 0.0618(16) 0.0130(11) 0.0206(13) 0.0142(11) C00Z 0.0467(14) 0.0576(16) 0.0556(15) -0.0049(12) -0.0007(11) -0.0121(12) C010 0.0495(14) 0.0466(13) 0.0490(13) 0.0018(11) -0.0009(10) 0.0042(11) C011 0.0481(14) 0.0621(17) 0.0489(14) -0.0051(12) -0.0102(11) 0.0067(12) C012 0.0523(14) 0.0559(15) 0.0417(12) -0.0020(11) 0.0149(10) -0.0014(12) C013 0.0613(17) 0.0614(17) 0.0600(16) 0.0029(13) 0.0182(13) 0.0283(14) C014 0.0671(17) 0.0452(14) 0.0534(15) 0.0130(12) -0.0015(12) 0.0117(12) C015 0.0409(13) 0.0594(16) 0.0591(15) 0.0003(13) 0.0009(11) -0.0018(11) C016 0.083(2) 0.0641(17) 0.0417(13) 0.0085(12) 0.0250(13) 0.0287(15) C017 0.0648(17) 0.0614(17) 0.0506(15) -0.0047(13) 0.0209(13) 0.0008(14) C018 0.081(2) 0.0557(16) 0.0408(13) -0.0082(12) 0.0145(13) 0.0004(14) C019 0.0416(13) 0.0695(18) 0.0559(15) 0.0093(13) -0.0085(11) -0.0134(12) C01A 0.0622(17) 0.0740(19) 0.0416(13) -0.0123(13) -0.0005(12) -0.0154(14) C01B 0.0602(16) 0.0518(15) 0.0501(14) -0.0149(12) 0.0075(12) -0.0012(12) C01C 0.0646(18) 0.0677(19) 0.0520(16) -0.0002(14) 0.0112(13) 0.0050(14) C01D 0.086(2) 0.0502(16) 0.0520(15) 0.0096(12) 0.0156(14) -0.0096(14) C01E 0.0686(18) 0.0635(18) 0.0481(14) 0.0064(13) -0.0111(13) 0.0185(14) C01F 0.0561(16) 0.089(2) 0.0439(14) 0.0008(14) -0.0092(12) -0.0190(15) C01G 0.0691(18) 0.0460(15) 0.0670(18) -0.0044(13) 0.0028(14) -0.0181(13) C01H 0.0674(19) 0.0606(18) 0.079(2) 0.0045(16) 0.0089(16) -0.0091(15) C01I 0.083(2) 0.0505(17) 0.071(2) -0.0037(15) -0.0049(16) -0.0049(15) C01J 0.0500(15) 0.0726(19) 0.0590(16) -0.0144(14) 0.0159(12) -0.0014(13) C01K 0.0538(16) 0.080(2) 0.0618(17) -0.0082(15) 0.0066(13) -0.0004(15) C01L 0.077(2) 0.097(3) 0.084(2) 0.046(2) 0.0156(18) 0.029(2) C01M 0.107(3) 0.0359(14) 0.072(2) -0.0019(13) 0.0185(18) 0.0044(15) C01N 0.0477(17) 0.087(2) 0.114(3) 0.011(2) 0.0142(17) 0.0019(17) C01O 0.087(2) 0.066(2) 0.088(2) 0.0012(18) -0.0097(19) -0.0156(18) C01P 0.072(2) 0.071(2) 0.087(2) 0.0029(18) 0.0174(18) -0.0202(17) C01Q 0.0519(17) 0.091(3) 0.095(3) 0.001(2) 0.0000(16) 0.0039(17) C01R 0.073(2) 0.070(2) 0.085(2) 0.0313(18) 0.0315(17) 0.0170(16) C01T 0.090(2) 0.061(2) 0.076(2) -0.0238(17) 0.0097(18) -0.0113(18) C01V 0.091(3) 0.062(2) 0.104(3) -0.026(2) 0.045(2) 0.0105(18) C01W 0.118(3) 0.087(3) 0.064(2) 0.0065(19) -0.026(2) -0.020(2) C01X 0.109(3) 0.082(3) 0.062(2) -0.0207(19) -0.023(2) 0.017(2) C01Y 0.157(4) 0.062(2) 0.0495(18) 0.0011(15) 0.025(2) 0.004(3) C01Z 0.104(3) 0.060(2) 0.115(3) -0.030(2) 0.018(2) 0.001(2) C020 0.072(2) 0.086(2) 0.082(2) -0.0150(19) 0.0298(18) -0.0210(18) C021 0.070(2) 0.093(3) 0.110(3) -0.010(2) 0.021(2) -0.020(2) C022 0.143(4) 0.083(3) 0.091(3) -0.027(2) 0.083(3) -0.024(3) C023 0.083(3) 0.082(3) 0.128(4) -0.052(3) 0.014(2) -0.007(2) C024 0.107(3) 0.096(3) 0.106(3) 0.021(3) 0.034(3) 0.045(3) C025 0.065(2) 0.103(3) 0.164(5) -0.013(3) 0.035(3) -0.019(2) C1 0.058(4) 0.053(3) 0.047(3) 0.002(2) 0.021(3) 0.013(3) C2 0.042(4) 0.041(2) 0.049(2) 0.0047(18) 0.009(2) 0.008(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cr01 C01C 1.846(3) . ? Cr01 C01M 2.230(3) . ? Cr01 C01S 1.955(10) . ? Cr01 C01T 2.233(3) . ? Cr01 C01U 1.747(8) . ? Cr01 C01V 2.218(3) . ? Cr01 C01X 2.185(3) . ? Cr01 C01Y 2.195(3) . ? Cr01 C022 2.190(3) . ? Cr01 C1 1.952(7) . ? Cr01 C2 1.738(6) . ? Mg02 Mg03 3.5212(10) . ? Mg02 O004 1.9560(17) . ? Mg02 N006 2.0482(18) . ? Mg02 N009 2.0446(19) . ? Mg02 HQ 1.839(19) . ? Mg03 O005 1.9658(18) . ? Mg03 N007 2.052(2) . ? Mg03 N008 2.046(2) . ? Mg03 HQ 1.792(18) . ? O004 C01U 1.219(8) . ? O004 C1 1.221(6) . ? O005 C01S 1.233(9) . ? O005 C2 1.242(6) . ? N006 C00A 1.336(3) . ? N006 C00B 1.433(3) . ? N007 C00F 1.448(3) . ? N007 C00Q 1.330(3) . ? N008 C00L 1.440(3) . ? N008 C00O 1.334(3) . ? N009 C00D 1.440(3) . ? N009 C00G 1.331(3) . ? C00A C00I 1.405(3) . ? C00A C013 1.511(3) . ? C00B C00H 1.406(3) . ? C00B C00K 1.408(4) . ? C00C C00D 1.409(3) . ? C00C C00M 1.395(3) . ? C00C C00W 1.519(4) . ? C00D C00J 1.404(3) . ? C00E C00L 1.407(3) . ? C00E C00N 1.392(4) . ? C00E C010 1.515(4) . ? C00F C00P 1.413(4) . ? C00F C00T 1.405(4) . ? C00G C00I 1.397(3) . ? C00G C016 1.518(3) . ? C00H C00Z 1.514(4) . ? C00H C011 1.400(4) . ? C00I H00I 0.9300 . ? C00J C00S 1.396(3) . ? C00J C00V 1.504(4) . ? C00K C00U 1.517(4) . ? C00K C014 1.402(4) . ? C00L C012 1.408(4) . ? C00M H00M 0.9300 . ? C00M C00Y 1.378(4) . ? C00N H00N 0.9300 . ? C00N C018 1.377(4) . ? C00O C00X 1.399(4) . ? C00O C01D 1.518(4) . ? C00P C01A 1.393(4) . ? C00P C01B 1.512(4) . ? C00Q C00X 1.409(4) . ? C00Q C01G 1.518(4) . ? O00R C01C 1.142(4) . ? C00S H00S 0.9300 . ? C00S C00Y 1.366(4) . ? C00T C015 1.525(4) . ? C00T C019 1.395(4) . ? C00U H00U 0.9800 . ? C00U C01H 1.516(4) . ? C00U C023 1.525(5) . ? C00V H00V 0.9800 . ? C00V C01P 1.522(5) . ? C00V C01W 1.532(4) . ? C00W H00W 0.9800 . ? C00W C01N 1.520(5) . ? C00W C01O 1.514(5) . ? C00X H00X 0.9300 . ? C00Y H00Y 0.9300 . ? C00Z H00Z 0.9800 . ? C00Z C01I 1.517(5) . ? C00Z C025 1.534(5) . ? C010 H010 0.9800 . ? C010 C01L 1.524(4) . ? C010 C01R 1.513(4) . ? C011 H011 0.9300 . ? C011 C01E 1.377(5) . ? C012 C017 1.394(4) . ? C012 C01J 1.520(4) . ? C013 H01A 0.9600 . ? C013 H01B 0.9600 . ? C013 H01C 0.9600 . ? C014 H014 0.9300 . ? C014 C01E 1.381(4) . ? C015 H015 0.9800 . ? C015 C020 1.523(4) . ? C015 C024 1.502(5) . ? C016 H01D 0.9600 . ? C016 H01E 0.9600 . ? C016 H01F 0.9600 . ? C017 H017 0.9300 . ? C017 C018 1.374(4) . ? C018 H018 0.9300 . ? C019 H019 0.9300 . ? C019 C01F 1.373(5) . ? C01A H01G 0.9300 . ? C01A C01F 1.368(5) . ? C01B H01H 0.9800 . ? C01B C01K 1.517(4) . ? C01B C01Z 1.536(4) . ? C01D H01I 0.9600 . ? C01D H01J 0.9600 . ? C01D H01K 0.9600 . ? C01E H01L 0.9300 . ? C01F H01M 0.9300 . ? C01G H01N 0.9600 . ? C01G H01O 0.9600 . ? C01G H01P 0.9600 . ? C01H H01Q 0.9600 . ? C01H H01R 0.9600 . ? C01H H01S 0.9600 . ? C01I H01T 0.9600 . ? C01I H01U 0.9600 . ? C01I H01V 0.9600 . ? C01J H01W 0.9800 . ? C01J C01Q 1.519(5) . ? C01J C021 1.520(5) . ? C01K H01X 0.9600 . ? C01K H01Y 0.9600 . ? C01K H 0.9600 . ? C01L H01Z 0.9600 . ? C01L HA 0.9600 . ? C01L HB 0.9600 . ? C01M H01 0.9300 . ? C01M C01T 1.358(5) . ? C01M C01V 1.389(5) . ? C01N H1 0.9600 . ? C01N HC 0.9600 . ? C01N HD 0.9600 . ? C01O H2 0.9600 . ? C01O HE 0.9600 . ? C01O HF 0.9600 . ? C01P H3 0.9600 . ? C01P HG 0.9600 . ? C01P HH 0.9600 . ? C01Q H4 0.9600 . ? C01Q HI 0.9600 . ? C01Q HJ 0.9600 . ? C01R H5 0.9600 . ? C01R HK 0.9600 . ? C01R HL 0.9600 . ? C01S H6 0.9300 . ? C01T H7 0.9300 . ? C01T C01X 1.414(6) . ? C01V H8 0.9300 . ? C01V C022 1.411(6) . ? C01W H9 0.9600 . ? C01W HM 0.9600 . ? C01W HN 0.9600 . ? C01X H10 0.9300 . ? C01X C01Y 1.356(7) . ? C01Y H11 0.9300 . ? C01Y C022 1.407(7) . ? C01Z H12 0.9600 . ? C01Z HO 0.9600 . ? C01Z HP 0.9600 . ? C020 H02A 0.9600 . ? C020 H02B 0.9600 . ? C020 H02C 0.9600 . ? C021 H02D 0.9600 . ? C021 H02E 0.9600 . ? C021 H02F 0.9600 . ? C022 H022 0.9300 . ? C023 H02G 0.9600 . ? C023 H02H 0.9600 . ? C023 H02I 0.9600 . ? C024 H02J 0.9600 . ? C024 H02K 0.9600 . ? C024 H02L 0.9600 . ? C025 H02M 0.9600 . ? C025 H02N 0.9600 . ? C025 H02O 0.9600 . ? C1 H1A 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C01C Cr01 C01M 88.78(14) . . ? C01C Cr01 C01S 84.2(3) . . ? C01C Cr01 C01T 108.98(15) . . ? C01C Cr01 C01V 95.45(16) . . ? C01C Cr01 C01X 145.14(18) . . ? C01C Cr01 C01Y 162.70(16) . . ? C01C Cr01 C022 126.47(19) . . ? C01C Cr01 C1 92.7(2) . . ? C01M Cr01 C01T 35.42(14) . . ? C01S Cr01 C01M 137.4(4) . . ? C01S Cr01 C01T 162.0(3) . . ? C01S Cr01 C01V 102.5(4) . . ? C01S Cr01 C01X 130.6(3) . . ? C01S Cr01 C01Y 97.9(3) . . ? C01S Cr01 C022 85.0(3) . . ? C01U Cr01 C01C 87.4(3) . . ? C01U Cr01 C01M 134.7(4) . . ? C01U Cr01 C01S 87.0(4) . . ? C01U Cr01 C01T 105.2(4) . . ? C01U Cr01 C01V 170.2(4) . . ? C01U Cr01 C01X 93.9(3) . . ? C01U Cr01 C01Y 109.8(3) . . ? C01U Cr01 C022 144.0(3) . . ? C01V Cr01 C01M 36.40(14) . . ? C01V Cr01 C01T 65.04(15) . . ? C01X Cr01 C01M 65.83(14) . . ? C01X Cr01 C01T 37.30(15) . . ? C01X Cr01 C01V 78.39(17) . . ? C01X Cr01 C01Y 36.07(18) . . ? C01X Cr01 C022 66.0(2) . . ? C01Y Cr01 C01M 78.01(14) . . ? C01Y Cr01 C01T 65.87(16) . . ? C01Y Cr01 C01V 67.29(17) . . ? C022 Cr01 C01M 65.97(14) . . ? C022 Cr01 C01T 77.41(16) . . ? C022 Cr01 C01V 37.34(16) . . ? C022 Cr01 C01Y 37.42(18) . . ? C1 Cr01 C01M 117.9(4) . . ? C1 Cr01 C01T 87.5(4) . . ? C1 Cr01 C01V 152.5(4) . . ? C1 Cr01 C01X 80.0(3) . . ? C1 Cr01 C01Y 103.3(2) . . ? C1 Cr01 C022 140.7(2) . . ? C2 Cr01 C01C 91.0(2) . . ? C2 Cr01 C01M 154.0(3) . . ? C2 Cr01 C01T 159.7(2) . . ? C2 Cr01 C01V 118.0(3) . . ? C2 Cr01 C01X 122.4(2) . . ? C2 Cr01 C01Y 96.0(2) . . ? C2 Cr01 C022 93.8(2) . . ? C2 Cr01 C1 88.0(3) . . ? Mg03 Mg02 HQ 13.9(6) . . ? O004 Mg02 Mg03 86.73(6) . . ? O004 Mg02 N006 126.81(8) . . ? O004 Mg02 N009 100.48(8) . . ? O004 Mg02 HQ 99.9(6) . . ? N006 Mg02 Mg03 119.84(6) . . ? N006 Mg02 HQ 107.6(6) . . ? N009 Mg02 Mg03 132.21(6) . . ? N009 Mg02 N006 93.30(8) . . ? N009 Mg02 HQ 132.5(6) . . ? Mg02 Mg03 HQ 14.3(6) . . ? O005 Mg03 Mg02 88.96(6) . . ? O005 Mg03 N007 124.21(9) . . ? O005 Mg03 N008 104.57(8) . . ? O005 Mg03 HQ 103.0(6) . . ? N007 Mg03 Mg02 118.27(6) . . ? N007 Mg03 HQ 107.0(6) . . ? N008 Mg03 Mg02 129.91(6) . . ? N008 Mg03 N007 93.58(8) . . ? N008 Mg03 HQ 126.7(6) . . ? C01U O004 Mg02 139.9(5) . . ? C1 O004 Mg02 168.4(6) . . ? C01S O005 Mg03 161.8(7) . . ? C2 O005 Mg03 134.3(4) . . ? C00A N006 Mg02 121.88(15) . . ? C00A N006 C00B 118.49(18) . . ? C00B N006 Mg02 119.56(14) . . ? C00F N007 Mg03 120.05(15) . . ? C00Q N007 Mg03 121.59(16) . . ? C00Q N007 C00F 118.2(2) . . ? C00L N008 Mg03 121.30(15) . . ? C00O N008 Mg03 121.42(16) . . ? C00O N008 C00L 116.99(19) . . ? C00D N009 Mg02 121.19(13) . . ? C00G N009 Mg02 121.56(15) . . ? C00G N009 C00D 117.25(18) . . ? N006 C00A C00I 124.0(2) . . ? N006 C00A C013 120.4(2) . . ? C00I C00A C013 115.5(2) . . ? C00H C00B N006 119.2(2) . . ? C00H C00B C00K 120.4(2) . . ? C00K C00B N006 120.4(2) . . ? C00D C00C C00W 121.8(2) . . ? C00M C00C C00D 117.7(2) . . ? C00M C00C C00W 120.5(2) . . ? C00C C00D N009 118.5(2) . . ? C00J C00D N009 120.5(2) . . ? C00J C00D C00C 121.0(2) . . ? C00L C00E C010 121.4(2) . . ? C00N C00E C00L 118.3(2) . . ? C00N C00E C010 120.3(2) . . ? C00P C00F N007 120.3(2) . . ? C00T C00F N007 118.4(2) . . ? C00T C00F C00P 121.2(2) . . ? N009 C00G C00I 124.1(2) . . ? N009 C00G C016 119.7(2) . . ? C00I C00G C016 116.2(2) . . ? C00B C00H C00Z 121.5(2) . . ? C011 C00H C00B 118.8(2) . . ? C011 C00H C00Z 119.7(2) . . ? C00A C00I H00I 115.1 . . ? C00G C00I C00A 129.8(2) . . ? C00G C00I H00I 115.1 . . ? C00D C00J C00V 121.8(2) . . ? C00S C00J C00D 118.2(2) . . ? C00S C00J C00V 120.0(2) . . ? C00B C00K C00U 122.5(2) . . ? C014 C00K C00B 118.5(2) . . ? C014 C00K C00U 119.1(2) . . ? C00E C00L N008 121.4(2) . . ? C00E C00L C012 120.2(2) . . ? C012 C00L N008 118.4(2) . . ? C00C C00M H00M 119.2 . . ? C00Y C00M C00C 121.6(3) . . ? C00Y C00M H00M 119.2 . . ? C00E C00N H00N 119.0 . . ? C018 C00N C00E 121.9(3) . . ? C018 C00N H00N 119.0 . . ? N008 C00O C00X 124.1(2) . . ? N008 C00O C01D 119.8(2) . . ? C00X C00O C01D 116.1(2) . . ? C00F C00P C01B 123.0(2) . . ? C01A C00P C00F 117.4(3) . . ? C01A C00P C01B 119.6(3) . . ? N007 C00Q C00X 123.9(2) . . ? N007 C00Q C01G 121.4(2) . . ? C00X C00Q C01G 114.7(2) . . ? C00J C00S H00S 119.3 . . ? C00Y C00S C00J 121.5(2) . . ? C00Y C00S H00S 119.3 . . ? C00F C00T C015 121.1(2) . . ? C019 C00T C00F 117.9(3) . . ? C019 C00T C015 121.0(3) . . ? C00K C00U H00U 107.9 . . ? C00K C00U C023 111.8(3) . . ? C01H C00U C00K 112.6(2) . . ? C01H C00U H00U 107.9 . . ? C01H C00U C023 108.6(3) . . ? C023 C00U H00U 107.9 . . ? C00J C00V H00V 107.7 . . ? C00J C00V C01P 109.2(2) . . ? C00J C00V C01W 113.8(3) . . ? C01P C00V H00V 107.7 . . ? C01P C00V C01W 110.4(3) . . ? C01W C00V H00V 107.7 . . ? C00C C00W H00W 107.2 . . ? C00C C00W C01N 112.2(3) . . ? C01N C00W H00W 107.2 . . ? C01O C00W C00C 112.8(3) . . ? C01O C00W H00W 107.2 . . ? C01O C00W C01N 110.0(3) . . ? C00O C00X C00Q 130.3(2) . . ? C00O C00X H00X 114.9 . . ? C00Q C00X H00X 114.9 . . ? C00M C00Y H00Y 120.1 . . ? C00S C00Y C00M 119.9(2) . . ? C00S C00Y H00Y 120.1 . . ? C00H C00Z H00Z 108.2 . . ? C00H C00Z C01I 110.9(2) . . ? C00H C00Z C025 111.9(3) . . ? C01I C00Z H00Z 108.2 . . ? C01I C00Z C025 109.4(3) . . ? C025 C00Z H00Z 108.2 . . ? C00E C010 H010 107.7 . . ? C00E C010 C01L 112.9(2) . . ? C01L C010 H010 107.7 . . ? C01R C010 C00E 111.1(2) . . ? C01R C010 H010 107.7 . . ? C01R C010 C01L 109.6(3) . . ? C00H C011 H011 119.4 . . ? C01E C011 C00H 121.3(3) . . ? C01E C011 H011 119.4 . . ? C00L C012 C01J 121.9(2) . . ? C017 C012 C00L 118.7(3) . . ? C017 C012 C01J 119.3(2) . . ? C00A C013 H01A 109.5 . . ? C00A C013 H01B 109.5 . . ? C00A C013 H01C 109.5 . . ? H01A C013 H01B 109.5 . . ? H01A C013 H01C 109.5 . . ? H01B C013 H01C 109.5 . . ? C00K C014 H014 119.3 . . ? C01E C014 C00K 121.4(3) . . ? C01E C014 H014 119.3 . . ? C00T C015 H015 107.0 . . ? C020 C015 C00T 111.5(3) . . ? C020 C015 H015 107.0 . . ? C024 C015 C00T 113.1(3) . . ? C024 C015 H015 107.0 . . ? C024 C015 C020 110.9(3) . . ? C00G C016 H01D 109.5 . . ? C00G C016 H01E 109.5 . . ? C00G C016 H01F 109.5 . . ? H01D C016 H01E 109.5 . . ? H01D C016 H01F 109.5 . . ? H01E C016 H01F 109.5 . . ? C012 C017 H017 119.3 . . ? C018 C017 C012 121.5(3) . . ? C018 C017 H017 119.3 . . ? C00N C018 H018 120.3 . . ? C017 C018 C00N 119.3(3) . . ? C017 C018 H018 120.3 . . ? C00T C019 H019 119.4 . . ? C01F C019 C00T 121.3(3) . . ? C01F C019 H019 119.4 . . ? C00P C01A H01G 119.1 . . ? C01F C01A C00P 121.8(3) . . ? C01F C01A H01G 119.1 . . ? C00P C01B H01H 107.8 . . ? C00P C01B C01K 111.3(3) . . ? C00P C01B C01Z 113.2(3) . . ? C01K C01B H01H 107.8 . . ? C01K C01B C01Z 108.8(3) . . ? C01Z C01B H01H 107.8 . . ? O00R C01C Cr01 177.1(3) . . ? C00O C01D H01I 109.5 . . ? C00O C01D H01J 109.5 . . ? C00O C01D H01K 109.5 . . ? H01I C01D H01J 109.5 . . ? H01I C01D H01K 109.5 . . ? H01J C01D H01K 109.5 . . ? C011 C01E C014 119.7(3) . . ? C011 C01E H01L 120.2 . . ? C014 C01E H01L 120.2 . . ? C019 C01F H01M 119.9 . . ? C01A C01F C019 120.1(3) . . ? C01A C01F H01M 119.9 . . ? C00Q C01G H01N 109.5 . . ? C00Q C01G H01O 109.5 . . ? C00Q C01G H01P 109.5 . . ? H01N C01G H01O 109.5 . . ? H01N C01G H01P 109.5 . . ? H01O C01G H01P 109.5 . . ? C00U C01H H01Q 109.5 . . ? C00U C01H H01R 109.5 . . ? C00U C01H H01S 109.5 . . ? H01Q C01H H01R 109.5 . . ? H01Q C01H H01S 109.5 . . ? H01R C01H H01S 109.5 . . ? C00Z C01I H01T 109.5 . . ? C00Z C01I H01U 109.5 . . ? C00Z C01I H01V 109.5 . . ? H01T C01I H01U 109.5 . . ? H01T C01I H01V 109.5 . . ? H01U C01I H01V 109.5 . . ? C012 C01J H01W 107.3 . . ? C01Q C01J C012 111.8(3) . . ? C01Q C01J H01W 107.3 . . ? C01Q C01J C021 110.3(3) . . ? C021 C01J C012 112.5(3) . . ? C021 C01J H01W 107.3 . . ? C01B C01K H01X 109.5 . . ? C01B C01K H01Y 109.5 . . ? C01B C01K H 109.5 . . ? H01X C01K H01Y 109.5 . . ? H01X C01K H 109.5 . . ? H01Y C01K H 109.5 . . ? C010 C01L H01Z 109.5 . . ? C010 C01L HA 109.5 . . ? C010 C01L HB 109.5 . . ? H01Z C01L HA 109.5 . . ? H01Z C01L HB 109.5 . . ? HA C01L HB 109.5 . . ? Cr01 C01M H01 129.3 . . ? C01T C01M Cr01 72.40(19) . . ? C01T C01M H01 119.4 . . ? C01T C01M C01V 121.1(3) . . ? C01V C01M Cr01 71.31(18) . . ? C01V C01M H01 119.4 . . ? C00W C01N H1 109.5 . . ? C00W C01N HC 109.5 . . ? C00W C01N HD 109.5 . . ? H1 C01N HC 109.5 . . ? H1 C01N HD 109.5 . . ? HC C01N HD 109.5 . . ? C00W C01O H2 109.5 . . ? C00W C01O HE 109.5 . . ? C00W C01O HF 109.5 . . ? H2 C01O HE 109.5 . . ? H2 C01O HF 109.5 . . ? HE C01O HF 109.5 . . ? C00V C01P H3 109.5 . . ? C00V C01P HG 109.5 . . ? C00V C01P HH 109.5 . . ? H3 C01P HG 109.5 . . ? H3 C01P HH 109.5 . . ? HG C01P HH 109.5 . . ? C01J C01Q H4 109.5 . . ? C01J C01Q HI 109.5 . . ? C01J C01Q HJ 109.5 . . ? H4 C01Q HI 109.5 . . ? H4 C01Q HJ 109.5 . . ? HI C01Q HJ 109.5 . . ? C010 C01R H5 109.5 . . ? C010 C01R HK 109.5 . . ? C010 C01R HL 109.5 . . ? H5 C01R HK 109.5 . . ? H5 C01R HL 109.5 . . ? HK C01R HL 109.5 . . ? Cr01 C01S H6 111.5 . . ? O005 C01S Cr01 137.1(11) . . ? O005 C01S H6 111.5 . . ? Cr01 C01T H7 131.0 . . ? C01M C01T Cr01 72.2(2) . . ? C01M C01T H7 120.0 . . ? C01M C01T C01X 119.9(4) . . ? C01X C01T Cr01 69.5(2) . . ? C01X C01T H7 120.0 . . ? O004 C01U Cr01 174.2(7) . . ? Cr01 C01V H8 128.9 . . ? C01M C01V Cr01 72.30(18) . . ? C01M C01V H8 120.7 . . ? C01M C01V C022 118.5(4) . . ? C022 C01V Cr01 70.26(19) . . ? C022 C01V H8 120.7 . . ? C00V C01W H9 109.5 . . ? C00V C01W HM 109.5 . . ? C00V C01W HN 109.5 . . ? H9 C01W HM 109.5 . . ? H9 C01W HN 109.5 . . ? HM C01W HN 109.5 . . ? Cr01 C01X H10 126.8 . . ? C01T C01X Cr01 73.2(2) . . ? C01T C01X H10 119.6 . . ? C01Y C01X Cr01 72.3(2) . . ? C01Y C01X C01T 120.7(4) . . ? C01Y C01X H10 119.6 . . ? Cr01 C01Y H11 129.2 . . ? C01X C01Y Cr01 71.6(2) . . ? C01X C01Y H11 120.4 . . ? C01X C01Y C022 119.2(4) . . ? C022 C01Y Cr01 71.1(2) . . ? C022 C01Y H11 120.4 . . ? C01B C01Z H12 109.5 . . ? C01B C01Z HO 109.5 . . ? C01B C01Z HP 109.5 . . ? H12 C01Z HO 109.5 . . ? H12 C01Z HP 109.5 . . ? HO C01Z HP 109.5 . . ? C015 C020 H02A 109.5 . . ? C015 C020 H02B 109.5 . . ? C015 C020 H02C 109.5 . . ? H02A C020 H02B 109.5 . . ? H02A C020 H02C 109.5 . . ? H02B C020 H02C 109.5 . . ? C01J C021 H02D 109.5 . . ? C01J C021 H02E 109.5 . . ? C01J C021 H02F 109.5 . . ? H02D C021 H02E 109.5 . . ? H02D C021 H02F 109.5 . . ? H02E C021 H02F 109.5 . . ? Cr01 C022 H022 128.6 . . ? C01V C022 Cr01 72.40(19) . . ? C01V C022 H022 119.8 . . ? C01Y C022 Cr01 71.5(2) . . ? C01Y C022 C01V 120.4(4) . . ? C01Y C022 H022 119.8 . . ? C00U C023 H02G 109.5 . . ? C00U C023 H02H 109.5 . . ? C00U C023 H02I 109.5 . . ? H02G C023 H02H 109.5 . . ? H02G C023 H02I 109.5 . . ? H02H C023 H02I 109.5 . . ? C015 C024 H02J 109.5 . . ? C015 C024 H02K 109.5 . . ? C015 C024 H02L 109.5 . . ? H02J C024 H02K 109.5 . . ? H02J C024 H02L 109.5 . . ? H02K C024 H02L 109.5 . . ? C00Z C025 H02M 109.5 . . ? C00Z C025 H02N 109.5 . . ? C00Z C025 H02O 109.5 . . ? H02M C025 H02N 109.5 . . ? H02M C025 H02O 109.5 . . ? H02N C025 H02O 109.5 . . ? Cr01 C1 H1A 111.6 . . ? O004 C1 Cr01 136.8(9) . . ? O004 C1 H1A 111.6 . . ? O005 C2 Cr01 176.7(6) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cr01 C01M C01T C01X 52.5(3) . . . . ? Cr01 C01M C01V C022 -54.8(3) . . . . ? Cr01 C01T C01X C01Y 56.7(3) . . . . ? Cr01 C01V C022 C01Y -55.1(3) . . . . ? Cr01 C01X C01Y C022 54.7(3) . . . . ? Cr01 C01Y C022 C01V 55.5(3) . . . . ? Mg02 O004 C1 Cr01 -16.2(18) . . . . ? Mg02 N006 C00A C00I -4.2(3) . . . . ? Mg02 N006 C00A C013 178.6(2) . . . . ? Mg02 N006 C00B C00H 87.7(2) . . . . ? Mg02 N006 C00B C00K -89.3(2) . . . . ? Mg02 N009 C00D C00C -87.1(2) . . . . ? Mg02 N009 C00D C00J 91.7(2) . . . . ? Mg02 N009 C00G C00I 13.7(3) . . . . ? Mg02 N009 C00G C016 -167.9(2) . . . . ? Mg03 O005 C01S Cr01 -20(2) . . . . ? Mg03 N007 C00F C00P -94.5(2) . . . . ? Mg03 N007 C00F C00T 82.8(2) . . . . ? Mg03 N007 C00Q C00X -8.7(3) . . . . ? Mg03 N007 C00Q C01G 173.1(2) . . . . ? Mg03 N008 C00L C00E 89.5(2) . . . . ? Mg03 N008 C00L C012 -90.1(2) . . . . ? Mg03 N008 C00O C00X 10.9(3) . . . . ? Mg03 N008 C00O C01D -168.9(2) . . . . ? N006 C00A C00I C00G -14.6(4) . . . . ? N006 C00B C00H C00Z 0.6(3) . . . . ? N006 C00B C00H C011 -178.2(2) . . . . ? N006 C00B C00K C00U -3.5(3) . . . . ? N006 C00B C00K C014 177.2(2) . . . . ? N007 C00F C00P C01A -178.7(2) . . . . ? N007 C00F C00P C01B 3.1(4) . . . . ? N007 C00F C00T C015 -0.9(3) . . . . ? N007 C00F C00T C019 179.1(2) . . . . ? N007 C00Q C00X C00O -11.3(5) . . . . ? N008 C00L C012 C017 -179.0(2) . . . . ? N008 C00L C012 C01J 0.8(4) . . . . ? N008 C00O C00X C00Q 10.1(5) . . . . ? N009 C00D C00J C00S 176.8(2) . . . . ? N009 C00D C00J C00V -6.4(3) . . . . ? N009 C00G C00I C00A 9.1(5) . . . . ? C00A N006 C00B C00H -89.4(3) . . . . ? C00A N006 C00B C00K 93.6(3) . . . . ? C00B N006 C00A C00I 172.9(2) . . . . ? C00B N006 C00A C013 -4.3(3) . . . . ? C00B C00H C00Z C01I -111.1(3) . . . . ? C00B C00H C00Z C025 126.4(3) . . . . ? C00B C00H C011 C01E 0.8(4) . . . . ? C00B C00K C00U C01H 126.9(3) . . . . ? C00B C00K C00U C023 -110.6(3) . . . . ? C00B C00K C014 C01E 1.1(4) . . . . ? C00C C00D C00J C00S -4.4(3) . . . . ? C00C C00D C00J C00V 172.4(2) . . . . ? C00C C00M C00Y C00S -2.4(4) . . . . ? C00D N009 C00G C00I -165.4(2) . . . . ? C00D N009 C00G C016 13.0(3) . . . . ? C00D C00C C00M C00Y 0.5(4) . . . . ? C00D C00C C00W C01N -89.5(3) . . . . ? C00D C00C C00W C01O 145.6(3) . . . . ? C00D C00J C00S C00Y 2.5(4) . . . . ? C00D C00J C00V C01P -94.3(3) . . . . ? C00D C00J C00V C01W 141.8(3) . . . . ? C00E C00L C012 C017 1.4(4) . . . . ? C00E C00L C012 C01J -178.8(3) . . . . ? C00E C00N C018 C017 0.4(4) . . . . ? C00F N007 C00Q C00X 175.3(2) . . . . ? C00F N007 C00Q C01G -3.0(4) . . . . ? C00F C00P C01A C01F -1.6(4) . . . . ? C00F C00P C01B C01K 116.6(3) . . . . ? C00F C00P C01B C01Z -120.5(3) . . . . ? C00F C00T C015 C020 85.0(3) . . . . ? C00F C00T C015 C024 -149.3(3) . . . . ? C00F C00T C019 C01F 0.6(4) . . . . ? C00G N009 C00D C00C 91.9(3) . . . . ? C00G N009 C00D C00J -89.3(3) . . . . ? C00H C00B C00K C00U 179.5(2) . . . . ? C00H C00B C00K C014 0.2(4) . . . . ? C00H C011 C01E C014 0.5(5) . . . . ? C00J C00S C00Y C00M 0.8(4) . . . . ? C00K C00B C00H C00Z 177.5(2) . . . . ? C00K C00B C00H C011 -1.2(3) . . . . ? C00K C014 C01E C011 -1.5(5) . . . . ? C00L N008 C00O C00X -163.0(2) . . . . ? C00L N008 C00O C01D 17.2(3) . . . . ? C00L C00E C00N C018 1.0(4) . . . . ? C00L C00E C010 C01L 133.0(3) . . . . ? C00L C00E C010 C01R -103.4(3) . . . . ? C00L C012 C017 C018 0.0(4) . . . . ? C00L C012 C01J C01Q 125.1(3) . . . . ? C00L C012 C01J C021 -110.1(3) . . . . ? C00M C00C C00D N009 -178.3(2) . . . . ? C00M C00C C00D C00J 2.9(3) . . . . ? C00M C00C C00W C01N 89.9(3) . . . . ? C00M C00C C00W C01O -35.0(4) . . . . ? C00N C00E C00L N008 178.5(2) . . . . ? C00N C00E C00L C012 -1.9(4) . . . . ? C00N C00E C010 C01L -48.3(4) . . . . ? C00N C00E C010 C01R 75.3(3) . . . . ? C00O N008 C00L C00E -96.6(3) . . . . ? C00O N008 C00L C012 83.8(3) . . . . ? C00P C00F C00T C015 176.4(2) . . . . ? C00P C00F C00T C019 -3.6(4) . . . . ? C00P C01A C01F C019 -1.3(5) . . . . ? C00Q N007 C00F C00P 81.6(3) . . . . ? C00Q N007 C00F C00T -101.1(3) . . . . ? C00S C00J C00V C01P 82.4(3) . . . . ? C00S C00J C00V C01W -41.5(4) . . . . ? C00T C00F C00P C01A 4.1(4) . . . . ? C00T C00F C00P C01B -174.1(2) . . . . ? C00T C019 C01F C01A 1.8(5) . . . . ? C00U C00K C014 C01E -178.2(3) . . . . ? C00V C00J C00S C00Y -174.3(2) . . . . ? C00W C00C C00D N009 1.1(3) . . . . ? C00W C00C C00D C00J -177.7(2) . . . . ? C00W C00C C00M C00Y -178.9(2) . . . . ? C00Z C00H C011 C01E -177.9(3) . . . . ? C010 C00E C00L N008 -2.7(3) . . . . ? C010 C00E C00L C012 176.9(2) . . . . ? C010 C00E C00N C018 -177.8(3) . . . . ? C011 C00H C00Z C01I 67.6(3) . . . . ? C011 C00H C00Z C025 -54.9(4) . . . . ? C012 C017 C018 C00N -0.9(5) . . . . ? C013 C00A C00I C00G 162.7(3) . . . . ? C014 C00K C00U C01H -53.9(3) . . . . ? C014 C00K C00U C023 68.6(4) . . . . ? C015 C00T C019 C01F -179.4(3) . . . . ? C016 C00G C00I C00A -169.4(3) . . . . ? C017 C012 C01J C01Q -55.1(4) . . . . ? C017 C012 C01J C021 69.7(4) . . . . ? C019 C00T C015 C020 -95.1(3) . . . . ? C019 C00T C015 C024 30.7(4) . . . . ? C01A C00P C01B C01K -61.6(3) . . . . ? C01A C00P C01B C01Z 61.3(4) . . . . ? C01B C00P C01A C01F 176.7(3) . . . . ? C01D C00O C00X C00Q -170.2(3) . . . . ? C01G C00Q C00X C00O 167.0(3) . . . . ? C01J C012 C017 C018 -179.8(3) . . . . ? C01M C01T C01X Cr01 -53.7(3) . . . . ? C01M C01T C01X C01Y 3.1(5) . . . . ? C01M C01V C022 Cr01 55.8(3) . . . . ? C01M C01V C022 C01Y 0.7(5) . . . . ? C01T C01M C01V Cr01 54.7(3) . . . . ? C01T C01M C01V C022 0.0(5) . . . . ? C01T C01X C01Y Cr01 -57.1(3) . . . . ? C01T C01X C01Y C022 -2.4(6) . . . . ? C01V C01M C01T Cr01 -54.2(3) . . . . ? C01V C01M C01T C01X -1.8(5) . . . . ? C01X C01Y C022 Cr01 -55.0(3) . . . . ? C01X C01Y C022 C01V 0.6(6) . . . . ? _smtbx_masks_special_details ; A solvent mask was calculated and 198 electrons were found in a volume of 1230\%A^3^ in 1 void per unit cell. This is consistent with the presence of 0.8[C6H14] per Asymmetric Unit which account for 200 electrons per unit cell. ; loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.500 0.000 615.3 99.4 '2 hexane' 2 0.000 0.000 0.500 615.3 99.4 '2 hexane' _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL mrc2116_a.res in P2(1)/c mrc2116.res created by SHELXL-2018/3 at 12:28:03 on 15-Oct-2021 REM Old TITL MRC2116 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.181, Rweak 0.032, Alpha 0.059 REM 0.451 for 609 systematic absences, Orientation as input REM Formula found by SHELXT: C67 N4 O5 Mg2 Cr CELL 1.54184 15.3628 12.9497 35.885 90 99.436 90 ZERR 4 0.0002 0.0002 0.0006 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cr Mg N O UNIT 268 360 4 8 16 12 SIMU 0.01 0.01 1 C1 C01U C2 C01S L.S. 6 PLAN 20 SIZE 0.12 0.15 0.14 CONF BOND list 4 MORE -1 BOND $H ABIN fmap 2 53 acta REM REM REM WGHT 0.084400 FVAR 0.30857 0.44949 CR01 3 0.761282 0.403376 0.589058 11.00000 0.05658 0.03145 = 0.04354 -0.00075 0.01809 0.00316 MG02 4 0.620901 0.662093 0.647325 11.00000 0.03267 0.03405 = 0.03405 0.00237 0.00598 0.00481 MG03 4 0.811798 0.748412 0.614260 11.00000 0.03812 0.03455 = 0.03474 -0.00055 0.00432 -0.00580 O004 6 0.630406 0.536461 0.617999 11.00000 0.05230 0.03996 = 0.04708 -0.00747 0.01336 0.00179 O005 6 0.849456 0.603885 0.611638 11.00000 0.05310 0.03662 = 0.05662 -0.00075 0.01111 0.00011 N006 5 0.513368 0.757201 0.643971 11.00000 0.03346 0.03178 = 0.03705 -0.00109 0.00308 0.00336 N007 5 0.886232 0.861602 0.644227 11.00000 0.03966 0.03767 = 0.03971 -0.00434 0.00305 -0.00471 N008 5 0.825718 0.809714 0.563030 11.00000 0.04195 0.03716 = 0.03760 -0.00168 0.00767 -0.00241 N009 5 0.601741 0.599806 0.697705 11.00000 0.03991 0.03107 = 0.03713 0.00191 0.00883 0.00533 C00A 1 0.476257 0.779266 0.674199 11.00000 0.04014 0.03570 = 0.04396 -0.00250 0.00892 0.00813 C00B 1 0.473700 0.797808 0.608024 11.00000 0.03220 0.04023 = 0.03804 -0.00225 0.00039 0.00943 C00C 1 0.584232 0.411799 0.697811 11.00000 0.04666 0.03867 = 0.04534 0.00589 0.01726 -0.00011 C00D 1 0.636009 0.499398 0.709522 11.00000 0.04623 0.03180 = 0.03505 0.00348 0.01362 0.00560 C00E 1 0.741486 0.725423 0.506141 11.00000 0.05573 0.03812 = 0.04132 0.00484 0.00313 -0.00160 C00F 1 0.920740 0.846419 0.683873 11.00000 0.04071 0.04094 = 0.04202 -0.00280 -0.00109 -0.01180 C00G 1 0.556182 0.649483 0.720672 11.00000 0.05023 0.03991 = 0.03586 0.00037 0.01220 0.00583 C00H 1 0.408021 0.740061 0.585235 11.00000 0.03504 0.04711 = 0.04753 -0.00530 0.00159 0.00457 C00I 1 0.502860 0.735457 0.710078 11.00000 0.05260 0.04200 = 0.04125 -0.00307 0.01446 0.01323 AFIX 43 H00I 2 0.481780 0.768729 0.729770 11.00000 -1.20000 AFIX 0 C00J 1 0.719875 0.489304 0.731610 11.00000 0.04842 0.03943 = 0.03810 0.00371 0.00999 0.00932 C00K 1 0.503123 0.892000 0.594932 11.00000 0.04934 0.03382 = 0.04570 0.00219 0.00242 0.00830 C00L 1 0.821881 0.745595 0.530011 11.00000 0.05238 0.03763 = 0.03355 0.00605 0.00858 -0.00153 C00M 1 0.617420 0.315383 0.710377 11.00000 0.06092 0.03546 = 0.05954 0.00635 0.02199 -0.00207 AFIX 43 H00M 2 0.584589 0.256479 0.702823 11.00000 -1.20000 AFIX 0 C00N 1 0.742970 0.664713 0.474235 11.00000 0.06842 0.04530 = 0.04059 0.00006 0.00056 -0.00450 AFIX 43 H00N 2 0.690334 0.651758 0.458065 11.00000 -1.20000 AFIX 0 C00O 1 0.846886 0.908712 0.559502 11.00000 0.04939 0.03888 = 0.04427 0.00472 0.00961 -0.00068 C00P 1 0.873818 0.883724 0.711832 11.00000 0.05130 0.04802 = 0.04334 -0.00820 0.00179 -0.01174 C00Q 1 0.899754 0.952316 0.628746 11.00000 0.04291 0.03550 = 0.05378 -0.00165 0.00352 -0.00681 O00R 6 0.823386 0.321713 0.666707 11.00000 0.10119 0.12319 = 0.06257 0.02143 0.00241 0.02124 C00S 1 0.748118 0.390747 0.743902 11.00000 0.05183 0.04532 = 0.05176 0.00939 0.01090 0.01409 AFIX 43 H00S 2 0.802525 0.383080 0.759384 11.00000 -1.20000 AFIX 0 C00T 1 0.999398 0.790259 0.693607 11.00000 0.03802 0.05200 = 0.05136 0.00219 0.00008 -0.00943 C00U 1 0.573287 0.957635 0.618512 11.00000 0.06060 0.03823 = 0.05333 0.00304 0.00015 -0.00348 AFIX 13 H00U 2 0.597529 0.918064 0.641120 11.00000 -1.20000 AFIX 0 C00V 1 0.780671 0.580246 0.740418 11.00000 0.05399 0.04469 = 0.05261 0.00364 -0.00607 0.00395 AFIX 13 H00V 2 0.744468 0.642947 0.737604 11.00000 -1.20000 AFIX 0 C00W 1 0.494837 0.420774 0.672694 11.00000 0.05489 0.04226 = 0.06305 0.01209 0.00501 -0.00655 AFIX 13 H00W 2 0.496122 0.483455 0.657492 11.00000 -1.20000 AFIX 0 C00X 1 0.875271 0.974491 0.589998 11.00000 0.05262 0.03448 = 0.05579 0.00504 0.00779 -0.00699 AFIX 43 H00X 2 0.878496 1.043891 0.583699 11.00000 -1.20000 AFIX 0 C00Y 1 0.697639 0.305306 0.733702 11.00000 0.06468 0.03727 = 0.06179 0.01305 0.02055 0.01415 AFIX 43 H00Y 2 0.717386 0.240474 0.742486 11.00000 -1.20000 AFIX 0 C00Z 1 0.377783 0.636512 0.597989 11.00000 0.04670 0.05762 = 0.05558 -0.00494 -0.00075 -0.01208 AFIX 13 H00Z 2 0.405493 0.625667 0.624296 11.00000 -1.20000 AFIX 0 C010 1 0.654857 0.766429 0.515023 11.00000 0.04949 0.04664 = 0.04904 0.00175 -0.00087 0.00420 AFIX 13 H010 2 0.668552 0.819395 0.534613 11.00000 -1.20000 AFIX 0 C011 1 0.371384 0.778863 0.549688 11.00000 0.04810 0.06208 = 0.04887 -0.00506 -0.01016 0.00668 AFIX 43 H011 2 0.327357 0.741564 0.534566 11.00000 -1.20000 AFIX 0 C012 1 0.900920 0.702360 0.522064 11.00000 0.05234 0.05593 = 0.04168 -0.00201 0.01489 -0.00143 C013 1 0.398186 0.851651 0.670844 11.00000 0.06132 0.06141 = 0.06003 0.00287 0.01820 0.02827 AFIX 137 H01A 2 0.412840 0.915818 0.659989 11.00000 -1.50000 H01B 2 0.383573 0.864132 0.695456 11.00000 -1.50000 H01C 2 0.348558 0.820982 0.654955 11.00000 -1.50000 AFIX 0 C014 1 0.465162 0.926546 0.558884 11.00000 0.06706 0.04519 = 0.05344 0.01302 -0.00151 0.01166 AFIX 43 H014 2 0.484743 0.988028 0.549722 11.00000 -1.20000 AFIX 0 C015 1 1.046923 0.744718 0.663284 11.00000 0.04091 0.05938 = 0.05911 0.00034 0.00095 -0.00179 AFIX 13 H015 2 1.001554 0.726951 0.641727 11.00000 -1.20000 AFIX 0 C016 1 0.558746 0.611145 0.760804 11.00000 0.08324 0.06407 = 0.04166 0.00851 0.02503 0.02874 AFIX 137 H01D 2 0.545211 0.538740 0.760401 11.00000 -1.50000 H01E 2 0.516077 0.648215 0.772370 11.00000 -1.50000 H01F 2 0.616572 0.622231 0.775026 11.00000 -1.50000 AFIX 0 C017 1 0.897964 0.641560 0.489826 11.00000 0.06477 0.06145 = 0.05061 -0.00470 0.02090 0.00083 AFIX 43 H017 2 0.949882 0.612721 0.484382 11.00000 -1.20000 AFIX 0 C018 1 0.820064 0.623280 0.465913 11.00000 0.08140 0.05573 = 0.04077 -0.00817 0.01454 0.00038 AFIX 43 H018 2 0.819417 0.583339 0.444331 11.00000 -1.20000 AFIX 0 C019 1 1.032697 0.777401 0.731898 11.00000 0.04158 0.06948 = 0.05588 0.00932 -0.00847 -0.01342 AFIX 43 H019 2 1.085003 0.741051 0.738975 11.00000 -1.20000 AFIX 0 C01A 1 0.911493 0.868553 0.749464 11.00000 0.06222 0.07403 = 0.04157 -0.01230 -0.00048 -0.01541 AFIX 43 H01G 2 0.882633 0.893932 0.768396 11.00000 -1.20000 AFIX 0 C01B 1 0.784767 0.935732 0.702535 11.00000 0.06020 0.05179 = 0.05008 -0.01489 0.00752 -0.00125 AFIX 13 H01H 2 0.769112 0.939007 0.674965 11.00000 -1.20000 AFIX 0 C01C 1 0.797501 0.353221 0.637259 11.00000 0.06455 0.06774 = 0.05203 -0.00017 0.01121 0.00497 C01D 1 0.840354 0.956205 0.520457 11.00000 0.08557 0.05023 = 0.05204 0.00955 0.01555 -0.00958 AFIX 137 H01I 2 0.879944 0.921095 0.506635 11.00000 -1.50000 H01J 2 0.855978 1.027964 0.522806 11.00000 -1.50000 H01K 2 0.781010 0.949585 0.507245 11.00000 -1.50000 AFIX 0 C01E 1 0.399289 0.871163 0.536698 11.00000 0.06862 0.06351 = 0.04811 0.00636 -0.01107 0.01847 AFIX 43 H01L 2 0.373918 0.896103 0.513103 11.00000 -1.20000 AFIX 0 C01F 1 0.989753 0.817364 0.759335 11.00000 0.05606 0.08858 = 0.04391 0.00082 -0.00920 -0.01896 AFIX 43 H01M 2 1.013934 0.809608 0.784686 11.00000 -1.20000 AFIX 0 C01G 1 0.946086 1.040006 0.652149 11.00000 0.06909 0.04600 = 0.06695 -0.00438 0.00276 -0.01814 AFIX 137 H01N 2 0.961240 1.018364 0.677987 11.00000 -1.50000 H01O 2 0.907535 1.098727 0.650700 11.00000 -1.50000 H01P 2 0.998777 1.058371 0.642559 11.00000 -1.50000 AFIX 0 C01H 1 0.648712 0.984154 0.597771 11.00000 0.06744 0.06059 = 0.07882 0.00448 0.00889 -0.00910 AFIX 137 H01Q 2 0.673060 0.921776 0.589320 11.00000 -1.50000 H01R 2 0.693597 1.020563 0.614476 11.00000 -1.50000 H01S 2 0.627250 1.026919 0.576381 11.00000 -1.50000 AFIX 0 C01I 1 0.406401 0.549565 0.574383 11.00000 0.08265 0.05052 = 0.07114 -0.00374 -0.00494 -0.00486 AFIX 137 H01T 2 0.377815 0.557047 0.548657 11.00000 -1.50000 H01U 2 0.390288 0.484475 0.584099 11.00000 -1.50000 H01V 2 0.469213 0.552142 0.575454 11.00000 -1.50000 AFIX 0 C01J 1 0.988908 0.720477 0.547473 11.00000 0.05003 0.07265 = 0.05899 -0.01438 0.01586 -0.00143 AFIX 13 H01W 2 0.976670 0.756543 0.570060 11.00000 -1.20000 AFIX 0 C01K 1 0.713866 0.873869 0.717360 11.00000 0.05377 0.08002 = 0.06177 -0.00816 0.00663 -0.00041 AFIX 137 H01X 2 0.710468 0.806063 0.706403 11.00000 -1.50000 H01Y 2 0.658019 0.908031 0.710712 11.00000 -1.50000 H 2 0.728242 0.868364 0.744347 11.00000 -1.50000 AFIX 0 C01L 1 0.597982 0.816529 0.481036 11.00000 0.07672 0.09661 = 0.08434 0.04593 0.01558 0.02934 AFIX 137 H01Z 2 0.632575 0.865938 0.469887 11.00000 -1.50000 HA 2 0.548800 0.850795 0.489045 11.00000 -1.50000 HB 2 0.576745 0.764413 0.462767 11.00000 -1.50000 AFIX 0 C01M 1 0.759048 0.241632 0.567572 11.00000 0.10658 0.03592 = 0.07163 -0.00186 0.01850 0.00437 AFIX 43 H01 2 0.762648 0.179819 0.580930 11.00000 -1.20000 AFIX 0 C01N 1 0.420244 0.433415 0.695403 11.00000 0.04773 0.08743 = 0.11403 0.01124 0.01424 0.00193 AFIX 137 H1 2 0.420280 0.375986 0.712322 11.00000 -1.50000 HC 2 0.364896 0.435903 0.678537 11.00000 -1.50000 HD 2 0.428443 0.496340 0.709691 11.00000 -1.50000 AFIX 0 C01O 1 0.475460 0.331200 0.645464 11.00000 0.08719 0.06599 = 0.08826 0.00123 -0.00971 -0.01561 AFIX 137 H2 2 0.522372 0.324550 0.630941 11.00000 -1.50000 HE 2 0.420896 0.343569 0.628799 11.00000 -1.50000 HF 2 0.470829 0.268699 0.659393 11.00000 -1.50000 AFIX 0 C01P 1 0.842976 0.585196 0.711587 11.00000 0.07230 0.07117 = 0.08665 0.00291 0.01744 -0.02019 AFIX 137 H3 2 0.881178 0.526065 0.714518 11.00000 -1.50000 HG 2 0.877772 0.647012 0.715487 11.00000 -1.50000 HH 2 0.809287 0.585634 0.686568 11.00000 -1.50000 AFIX 0 C01Q 1 1.034591 0.619641 0.560466 11.00000 0.05192 0.09054 = 0.09457 0.00137 -0.00003 0.00390 AFIX 137 H4 2 0.994538 0.576119 0.571179 11.00000 -1.50000 HI 2 1.085445 0.633715 0.579157 11.00000 -1.50000 HJ 2 1.052660 0.585365 0.539275 11.00000 -1.50000 AFIX 0 C01R 1 0.602856 0.682126 0.530633 11.00000 0.07280 0.06998 = 0.08456 0.03133 0.03146 0.01698 AFIX 137 H5 2 0.585746 0.630873 0.511505 11.00000 -1.50000 HK 2 0.551081 0.711336 0.538244 11.00000 -1.50000 HL 2 0.638757 0.650694 0.552051 11.00000 -1.50000 AFIX 0 PART 1 C01S 1 0.849323 0.510836 0.604306 21.00000 0.05811 AFIX 43 H6 2 0.906386 0.484814 0.606662 21.00000 -1.20000 AFIX 0 PART 0 C01T 1 0.678673 0.283877 0.555051 11.00000 0.08968 0.06140 = 0.07644 -0.02383 0.00969 -0.01134 AFIX 43 H7 2 0.627742 0.250088 0.559244 11.00000 -1.20000 AFIX 0 PART 1 C01U 1 0.686605 0.481251 0.608013 21.00000 0.04551 PART 0 C01V 1 0.835987 0.289138 0.560773 11.00000 0.09106 0.06183 = 0.10420 -0.02554 0.04477 0.01051 AFIX 43 H8 2 0.890847 0.259851 0.569437 11.00000 -1.20000 AFIX 0 C01W 1 0.833014 0.579359 0.780608 11.00000 0.11829 0.08673 = 0.06366 0.00649 -0.02593 -0.01988 AFIX 137 H9 2 0.793424 0.568471 0.798340 11.00000 -1.50000 HM 2 0.862633 0.644339 0.785745 11.00000 -1.50000 HN 2 0.875788 0.524712 0.782927 11.00000 -1.50000 AFIX 0 C01X 1 0.672486 0.379269 0.535637 11.00000 0.10940 0.08203 = 0.06211 -0.02070 -0.02280 0.01733 AFIX 43 H10 2 0.617486 0.409521 0.528179 11.00000 -1.20000 AFIX 0 C01Y 1 0.745846 0.427151 0.527769 11.00000 0.15742 0.06175 = 0.04945 0.00107 0.02457 0.00365 AFIX 43 H11 2 0.741212 0.488580 0.514161 11.00000 -1.20000 AFIX 0 C01Z 1 0.784261 1.046462 0.717821 11.00000 0.10414 0.06004 = 0.11525 -0.02968 0.01785 0.00136 AFIX 137 H12 2 0.798535 1.045327 0.744883 11.00000 -1.50000 HO 2 0.726766 1.076147 0.710416 11.00000 -1.50000 HP 2 0.827164 1.087131 0.707717 11.00000 -1.50000 AFIX 0 C020 1 1.107616 0.823712 0.649310 11.00000 0.07206 0.08572 = 0.08227 -0.01497 0.02977 -0.02101 AFIX 137 H02A 2 1.074448 0.884540 0.640848 11.00000 -1.50000 H02B 2 1.132436 0.794861 0.628750 11.00000 -1.50000 H02C 2 1.154212 0.841517 0.669526 11.00000 -1.50000 AFIX 0 C021 1 1.050104 0.788957 0.529077 11.00000 0.07005 0.09281 = 0.11007 -0.00955 0.02053 -0.02032 AFIX 137 H02D 2 1.060896 0.757540 0.506036 11.00000 -1.50000 H02E 2 1.104971 0.797301 0.545955 11.00000 -1.50000 H02F 2 1.023103 0.855287 0.523619 11.00000 -1.50000 AFIX 0 C022 1 0.829031 0.382839 0.540424 11.00000 0.14335 0.08261 = 0.09081 -0.02676 0.08328 -0.02437 AFIX 43 H022 2 0.879732 0.415475 0.535353 11.00000 -1.20000 AFIX 0 C023 1 0.535039 1.057713 0.631331 11.00000 0.08318 0.08165 = 0.12782 -0.05224 0.01357 -0.00652 AFIX 137 H02G 2 0.511327 1.098218 0.609623 11.00000 -1.50000 H02H 2 0.580725 1.096018 0.646880 11.00000 -1.50000 H02I 2 0.488986 1.041910 0.645560 11.00000 -1.50000 AFIX 0 C024 1 1.096094 0.647066 0.675557 11.00000 0.10734 0.09597 = 0.10634 0.02139 0.03428 0.04505 AFIX 137 H02J 2 1.143820 0.662233 0.695624 11.00000 -1.50000 H02K 2 1.119185 0.617977 0.654586 11.00000 -1.50000 H02L 2 1.056712 0.598553 0.684307 11.00000 -1.50000 AFIX 0 C025 1 0.277376 0.632468 0.596140 11.00000 0.06504 0.10253 = 0.16361 -0.01266 0.03478 -0.01878 AFIX 137 H02M 2 0.259022 0.688387 0.610612 11.00000 -1.50000 H02N 2 0.261271 0.567986 0.606322 11.00000 -1.50000 H02O 2 0.248998 0.638499 0.570330 11.00000 -1.50000 AFIX 0 HQ 2 0.711566 0.737958 0.633435 11.00000 0.01238 PART 2 C1 1 0.652283 0.459751 0.602046 -21.00000 0.05758 0.05304 = 0.04699 0.00167 0.02085 0.01289 AFIX 43 H1A 2 0.604365 0.416852 0.593943 -21.00000 -1.20000 AFIX 0 C2 1 0.810815 0.521873 0.601489 -21.00000 0.04217 0.04054 = 0.04942 0.00468 0.00873 0.00848 HKLF 4 REM mrc2116_a.res in P2(1)/c REM wR2 = 0.1558, GooF = S = 1.025, Restrained GooF = 1.030 for all data REM R1 = 0.0517 for 9836 Fo > 4sig(Fo) and 0.0724 for all 13503 data REM 727 parameters refined using 12 restraints END WGHT 0.0844 0.0000 REM Highest difference peak 0.343, deepest hole -0.517, 1-sigma level 0.045 Q1 1 0.7450 0.4943 0.6019 11.00000 0.05 0.34 Q2 1 0.3039 0.6557 0.6250 11.00000 0.05 0.27 Q3 1 0.8210 0.4063 0.6030 11.00000 0.05 0.26 Q4 1 0.7398 0.2592 0.6202 11.00000 0.05 0.26 Q5 1 0.9008 0.2949 0.6002 11.00000 0.05 0.24 Q6 1 0.8981 0.8798 0.7025 11.00000 0.05 0.23 Q7 1 0.5435 1.0116 0.6607 11.00000 0.05 0.22 Q8 1 0.8879 0.3234 0.6376 11.00000 0.05 0.22 Q9 1 0.7583 0.4555 0.5554 11.00000 0.05 0.21 Q10 1 0.9600 1.1059 0.6369 11.00000 0.05 0.20 Q11 1 0.3627 0.8774 0.6408 11.00000 0.05 0.20 Q12 1 0.6035 0.4396 0.7018 11.00000 0.05 0.19 Q13 1 0.6498 0.7345 0.6380 11.00000 0.05 0.19 Q14 1 0.6133 0.6193 0.6855 11.00000 0.05 0.19 Q15 1 0.4401 0.7964 0.6013 11.00000 0.05 0.18 Q16 1 1.1572 0.7778 0.6685 11.00000 0.05 0.18 Q17 1 0.5978 0.3777 0.7019 11.00000 0.05 0.18 Q18 1 0.8752 0.8097 0.6384 11.00000 0.05 0.18 Q19 1 0.8248 0.3648 0.6199 11.00000 0.05 0.18 Q20 1 0.5130 0.7787 0.6517 11.00000 0.05 0.18 ; _shelx_res_checksum 18660 _shelx_hkl_file ; 0 0 3 1.37 0.81 0 0 4 1459.11 16.01 0 0 5 0.20 1.15 0 0 6 2019.66 23.19 0 0 7 -0.11 1.94 0 0 8 939.73 18.49 0 0 9 2.08 2.50 0 0 10 104.76 7.07 0 0 11 -0.77 2.31 0 0 12 849.24 22.05 0 0 13 -1.23 2.30 0 0 14 65.43 7.25 0 0 15 0.41 3.17 0 0 16 1646.40 36.83 0 0 17 2.27 3.52 0 0 -18 167.66 12.13 0 0 -19 0.32 3.07 0 0 -20 199.55 14.23 0 0 -21 4.58 3.93 0 0 -22 91.23 10.55 0 0 -23 2.22 3.52 0 0 -24 53.89 8.73 0 0 25 -1.21 1.76 0 0 -25 0.60 3.32 0 0 26 113.59 6.39 0 0 -26 135.82 14.62 0 0 27 1.62 1.61 0 0 -27 0.10 4.05 0 0 28 1.93 2.15 0 0 -28 15.37 6.38 0 0 -29 -13.71 5.85 0 0 29 0.36 2.20 0 0 30 61.45 5.29 0 0 31 -0.36 2.19 0 0 32 -0.08 2.34 0 0 33 -0.24 2.48 0 0 34 520.61 14.40 0 0 35 -1.63 2.24 0 0 36 28.89 3.77 0 0 37 2.44 2.39 0 0 38 84.33 5.46 0 0 39 -0.45 1.76 0 0 40 44.64 3.73 0 0 41 0.86 1.47 0 0 42 9.05 1.68 0 0 43 -0.97 0.92 0 -1 0 1.06 0.43 0 -1 1 998.13 9.91 0 -1 2 3715.43 22.29 0 -1 3 0.51 0.88 0 1 -3 2.85 0.66 0 -1 4 192.87 6.55 0 1 -4 180.11 4.58 0 -1 5 87.38 5.02 0 1 -5 82.82 3.73 0 -1 6 654.19 14.30 0 -1 7 233.67 9.34 0 1 8 269.82 9.53 0 -1 8 258.62 10.26 0 1 9 60.81 5.10 0 -1 9 50.30 5.36 0 -1 10 31.48 4.49 0 -1 11 125.10 8.51 0 -1 12 281.80 13.36 0 1 -12 276.28 11.56 0 -1 13 180.41 11.35 0 1 -13 164.69 9.43 0 1 -14 85.15 7.20 0 -1 14 83.49 8.29 0 -1 15 360.08 17.22 0 1 -15 410.38 15.84 0 -1 16 21.18 5.48 0 1 -16 18.38 4.33 0 -1 17 120.57 10.96 0 1 -17 107.39 9.28 0 -1 18 88.52 10.26 0 1 -18 77.05 8.02 0 -1 19 31.08 6.48 0 1 -19 36.91 6.28 0 -1 -20 373.99 20.07 0 1 -20 376.16 18.94 0 -1 20 414.43 22.01 0 1 -21 66.51 8.52 0 -1 -21 70.60 9.60 0 1 -22 136.09 12.49 0 -1 -22 111.26 12.38 0 1 -23 17.95 5.21 0 -1 -23 21.19 5.84 0 -1 -24 21.84 7.00 0 -1 24 14.78 2.63 0 1 -24 5.21 3.60 0 1 -25 144.39 14.04 0 -1 -25 142.21 15.01 0 -1 25 133.21 6.83 0 1 25 128.07 6.54 0 1 26 286.20 9.88 0 1 -26 296.29 20.33 0 -1 -26 304.41 22.31 0 -1 26 288.36 10.27 0 -1 27 3.33 2.22 0 -1 -27 -0.92 3.12 0 1 27 -0.37 1.56 0 -1 28 147.29 7.69 0 -1 -28 131.39 15.41 0 1 28 142.86 7.34 0 -1 -29 16.95 7.52 0 1 29 14.30 2.88 0 -1 29 12.51 3.00 0 1 30 55.48 4.95 0 -1 30 53.36 5.12 0 -1 -30 60.87 11.45 0 -1 31 4.21 2.38 0 1 31 7.30 2.55 0 1 32 41.21 4.41 0 -1 32 42.11 4.73 0 -1 33 3.74 2.85 0 1 33 1.84 2.39 0 -1 34 19.42 3.66 0 1 34 19.84 3.49 0 1 35 37.78 4.25 0 -1 35 38.82 4.46 0 1 36 21.17 3.14 0 -1 36 21.21 3.55 0 -1 37 1.70 2.25 0 1 37 0.58 2.00 0 1 38 1.23 2.03 0 -1 38 3.10 2.39 0 1 39 4.97 1.84 0 -1 39 4.02 2.02 0 1 40 1.36 1.40 0 -1 40 2.41 1.91 0 1 41 0.14 1.21 0 -1 41 2.47 1.51 0 -1 42 2.37 1.43 0 1 42 2.39 1.03 0 -1 43 1.20 1.01 0 -2 0 2155.30 17.27 0 -2 -1 3433.79 20.01 0 -2 1 3337.37 23.49 0 -2 2 1113.31 14.90 0 -2 3 617.31 12.12 0 -2 4 593.16 12.79 0 2 -4 611.20 7.11 0 2 -5 589.18 8.27 0 -2 5 573.11 13.37 0 2 -6 3478.40 23.25 0 -2 6 3476.95 35.18 0 2 -7 2545.56 22.38 0 -2 7 2768.63 33.09 0 -2 8 10.92 2.85 0 2 -8 10.63 1.90 0 2 -9 283.22 8.99 0 -2 9 293.38 12.38 0 -2 10 3352.29 43.07 0 2 -10 3283.63 32.70 0 -2 11 145.78 9.82 0 2 -11 142.82 7.45 0 2 -12 35.45 4.09 0 -2 12 33.67 5.62 0 -2 13 333.09 15.83 0 2 -13 313.88 12.20 0 -2 14 3.31 3.82 0 2 -14 0.70 1.76 0 2 -15 8.93 2.85 0 -2 15 6.97 3.51 0 -2 16 75.60 9.06 0 2 -16 71.59 7.09 0 2 -17 43.60 5.77 0 -2 17 47.53 8.10 0 -2 18 76.23 9.61 0 2 -18 79.87 8.08 0 -2 19 519.61 24.57 0 2 -19 562.52 21.41 0 -2 20 16.37 6.48 0 2 -20 8.38 3.77 0 -2 21 147.55 14.25 0 2 -21 158.19 12.29 0 -2 -22 54.98 8.82 0 2 -22 47.31 7.07 0 -2 -23 5.53 4.94 0 2 -23 -3.06 2.41 0 -2 24 107.62 6.17 0 -2 -24 106.72 13.17 0 2 25 372.84 10.83 0 -2 -25 380.06 24.84 0 -2 25 378.44 11.52 0 -2 -26 19.33 5.97 0 2 26 22.24 2.90 0 -2 26 27.74 3.53 0 2 27 42.08 3.96 0 -2 -27 38.09 8.97 0 -2 27 38.88 4.26 0 -2 -28 68.66 11.87 0 2 28 72.26 5.26 0 -2 28 79.45 5.91 0 2 29 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47.24 4.58 7 -7 -14 54.91 10.03 7 -7 -14 52.02 5.17 -7 -7 13 53.43 5.05 7 -7 -13 58.97 5.08 7 -7 -13 53.57 10.06 7 -7 -13 49.77 5.14 7 -7 -12 9.71 2.97 7 -7 -12 7.57 4.66 7 -7 -12 9.99 2.73 -7 -7 12 6.57 2.57 7 -7 -11 3.75 2.25 7 -7 -11 2.65 2.23 -7 -7 11 2.34 2.30 7 -7 -11 6.69 5.13 7 -7 -10 5.38 2.36 -7 -7 10 3.88 2.35 7 -7 -10 3.85 2.04 7 -7 -10 10.31 5.21 7 -7 -9 28.83 3.96 7 -7 -9 23.90 3.34 7 -7 -9 30.40 7.70 -7 -7 9 29.77 3.79 7 -7 -8 120.17 6.65 7 -7 -8 118.42 13.70 -7 -7 8 137.16 7.59 7 -7 -8 123.66 7.18 7 -7 -7 4.33 4.81 7 -7 -7 5.77 2.11 -7 -7 7 5.92 2.25 7 -7 -7 9.09 2.52 7 -7 -6 106.70 12.81 7 -7 -6 101.89 6.07 -7 -7 6 101.87 6.53 7 -7 -6 105.38 6.66 7 -7 -5 26.12 3.27 7 -7 -5 30.54 7.28 7 -7 -5 32.13 4.02 7 -7 -4 110.13 6.21 7 -7 -4 126.00 13.78 7 -7 -4 118.13 6.95 7 -7 -3 2.97 3.88 7 -7 -3 2.38 1.85 7 -7 -3 3.84 2.38 7 -7 -2 208.64 8.31 7 -7 -2 236.99 18.97 7 -7 -2 211.68 9.00 7 -7 -1 7.30 2.00 7 -7 -1 7.41 5.23 7 -7 -1 6.23 2.00 7 -7 0 661.70 31.88 7 -7 0 638.24 14.29 7 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14.58 2.85 8 6 21 14.50 2.73 -8 -6 -21 12.61 3.35 -8 -6 -22 71.64 5.80 8 6 22 76.44 5.24 8 6 23 4.02 2.06 -8 -6 -23 1.65 2.26 8 6 24 12.46 2.52 -8 -6 -24 21.69 3.69 8 6 25 11.76 2.21 -8 -6 -25 6.09 2.42 -8 -6 -26 70.65 5.04 8 6 26 81.37 4.78 -8 -6 -27 11.44 2.52 8 6 27 8.27 1.82 -8 -6 -28 22.39 2.67 8 -7 -38 4.88 1.31 8 -7 -37 3.00 1.43 8 -7 -36 28.04 2.87 8 -7 -35 5.46 1.99 8 -7 -34 34.43 3.58 8 -7 -33 2.28 2.32 8 -7 -32 79.88 5.58 8 -7 -31 -1.86 2.74 8 -7 -30 21.23 3.92 8 -7 -30 25.21 3.04 8 -7 -29 1.62 2.74 -8 -7 29 1.85 1.85 8 -7 -29 6.34 2.16 8 -7 -28 104.91 6.90 -8 -7 28 86.55 5.68 8 -7 -28 110.80 6.60 8 -7 -27 5.87 3.40 -8 -7 27 1.55 1.91 8 -7 -27 2.72 2.22 8 -7 -26 16.47 3.46 -8 -7 26 11.65 2.80 8 -7 -26 13.36 3.16 8 -7 -25 2.30 2.76 -8 -7 25 1.76 2.33 8 -7 -25 6.52 2.95 8 -7 -24 52.12 5.50 -8 -7 24 50.91 5.14 8 -7 -24 49.26 5.30 -8 -7 23 189.57 9.16 8 -7 -23 208.96 10.00 -8 -7 22 21.84 3.79 8 -7 -22 28.23 4.26 8 -7 -22 25.32 4.24 8 -7 -21 6.65 2.93 -8 -7 21 5.36 2.32 8 -7 -21 4.93 2.87 8 -7 -20 2.25 2.68 -8 -7 20 2.05 2.39 8 -7 -20 1.09 2.75 8 -7 -19 -3.22 2.73 -8 -7 19 1.15 2.46 8 -7 -19 1.89 2.55 8 -7 -18 6.59 2.83 8 -7 -18 10.03 5.14 -8 -7 18 4.02 2.61 8 -7 -18 1.86 2.57 8 -7 -17 18.32 3.89 8 -7 -17 25.54 7.84 -8 -7 17 9.67 2.77 8 -7 -17 17.55 3.86 8 -7 -16 31.29 4.36 -8 -7 16 24.02 3.93 8 -7 -16 23.71 3.99 8 -7 -15 89.00 6.56 8 -7 -15 73.11 11.39 -8 -7 15 85.24 6.48 8 -7 -15 86.99 6.73 8 -7 -14 93.77 6.52 8 -7 -14 73.09 11.90 -8 -7 14 85.04 6.39 8 -7 -14 91.04 6.87 8 -7 -13 221.43 9.73 8 -7 -13 208.71 19.08 -8 -7 13 235.70 10.39 8 -7 -13 227.53 10.39 8 -7 -12 3.10 3.60 8 -7 -12 14.01 3.12 -8 -7 12 13.64 3.31 8 -7 -12 11.25 3.26 8 -7 -11 82.65 12.31 -8 -7 11 86.90 6.50 8 -7 -11 84.72 6.07 8 -7 -11 89.31 6.67 8 -7 -10 127.38 7.18 8 -7 -10 125.64 14.96 -8 -7 10 145.96 8.17 8 -7 -10 133.70 7.84 8 -7 -9 11.68 2.65 8 -7 -9 17.00 6.44 -8 -7 9 12.23 2.81 8 -7 -9 9.94 3.31 8 -7 -8 2.53 1.92 8 -7 -8 10.79 5.78 -8 -7 8 6.34 2.57 8 -7 -8 7.35 2.79 8 -7 -7 5.06 2.26 8 -7 -7 12.22 5.78 -8 -7 7 8.57 2.76 8 -7 -7 6.66 2.77 8 -7 -6 144.84 7.61 -8 -7 6 147.45 7.98 8 -7 -6 147.81 16.06 8 -7 -6 163.23 8.51 8 -7 -5 6.25 2.15 8 -7 -5 -0.21 4.21 8 -7 -5 7.80 2.55 8 -7 -4 76.06 5.54 8 -7 -4 66.48 10.91 8 -7 -4 79.11 6.10 8 -7 -3 130.52 7.04 8 -7 -3 124.52 14.58 8 -7 -3 143.99 7.79 8 -7 -2 252.68 9.72 8 -7 -2 249.84 20.57 8 -7 -2 267.42 10.40 8 -7 -1 42.82 4.19 8 -7 -1 57.42 10.47 8 -7 -1 48.32 4.80 8 -7 0 5.42 2.46 8 -7 0 5.85 4.89 8 -7 0 1.00 1.96 8 -7 1 3.60 1.82 8 -7 1 2.33 2.08 8 -7 2 185.02 8.18 8 -7 2 192.00 8.65 8 -7 2 187.85 18.19 8 -7 3 2.28 1.83 8 -7 3 -2.80 4.57 8 -7 4 0.82 1.84 8 -7 4 -2.64 4.85 8 -7 5 3.33 1.94 8 -7 5 6.85 6.01 8 -7 6 352.73 11.25 8 -7 6 346.25 25.56 -8 -7 -6 346.43 11.61 8 -7 7 7.05 2.44 8 -7 7 10.37 5.95 -8 -7 -7 5.71 2.40 8 -7 8 37.38 4.15 8 -7 8 30.04 8.55 -8 -7 -8 31.30 3.74 8 -7 9 17.80 3.15 -8 -7 -9 13.07 2.68 8 -7 9 10.60 5.61 -8 -7 -10 5.15 1.98 8 -7 10 0.55 1.85 8 -7 10 4.22 4.62 8 -7 11 136.24 7.29 8 -7 11 130.74 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4.60 -8 -8 21 35.20 4.47 8 -8 -21 34.40 4.76 8 -8 -20 77.06 6.36 -8 -8 20 75.19 6.15 8 -8 -20 82.46 6.86 -8 -8 19 63.70 5.84 8 -8 -19 61.93 6.06 8 -8 -18 40.32 4.78 -8 -8 18 36.28 4.74 8 -8 -18 43.58 5.29 8 -8 -17 55.22 5.29 -8 -8 17 44.51 5.07 8 -8 -17 49.53 5.55 8 -8 -16 -0.01 2.33 -8 -8 16 -2.07 2.58 8 -8 -16 -0.55 2.90 8 -8 -15 8.84 2.89 -8 -8 15 7.47 2.63 8 -8 -15 10.75 3.63 8 -8 -14 124.49 7.54 -8 -8 14 128.53 8.15 8 -8 -14 127.42 8.18 8 -8 -13 17.25 3.37 -8 -8 13 18.12 3.66 8 -8 -13 20.79 4.09 8 -8 -12 3.61 2.45 8 -8 -12 4.27 2.95 8 -8 -11 33.89 4.13 8 -8 -11 38.68 9.08 8 -8 -11 40.85 5.05 8 -8 -10 12.98 3.08 8 -8 -10 12.05 5.53 8 -8 -10 12.73 3.82 8 -8 -9 237.14 9.74 8 -8 -9 214.47 19.33 8 -8 -9 213.86 10.31 8 -8 -8 12.93 2.76 8 -8 -8 10.94 4.95 8 -8 -8 12.99 3.12 8 -8 -7 16.31 6.14 8 -8 -7 20.99 3.32 8 -8 -7 21.72 3.80 8 -8 -6 27.14 3.69 8 -8 -6 35.99 4.45 8 -8 -6 37.35 8.85 8 -8 -5 36.17 4.23 8 -8 -5 23.90 7.25 8 -8 -5 36.21 4.62 8 -8 -4 31.23 3.72 8 -8 -4 30.08 7.74 8 -8 -4 36.96 4.62 8 -8 -3 26.38 7.59 8 -8 -3 14.93 2.93 8 -8 -3 20.12 3.48 8 -8 -2 17.66 3.09 8 -8 -2 24.87 7.78 8 -8 -2 17.16 3.30 8 -8 -1 62.63 5.04 8 -8 -1 50.19 5.10 8 -8 -1 54.45 9.95 8 -8 0 1.64 1.97 8 -8 0 3.35 4.11 8 -8 0 3.84 2.41 8 -8 1 119.07 6.63 8 -8 1 110.98 14.66 8 -8 1 111.41 6.98 8 -8 2 58.67 4.68 8 -8 2 59.77 11.06 8 -8 2 65.61 5.31 8 -8 3 89.20 5.83 8 -8 3 99.99 14.12 8 -8 4 7.64 2.62 8 -8 4 3.44 4.84 8 -8 5 45.87 4.19 8 -8 5 58.48 10.75 -8 -8 -5 52.79 5.04 8 -8 6 10.20 2.30 -8 -8 -6 14.20 3.11 8 -8 6 10.98 6.14 -8 -8 -7 98.56 6.59 8 -8 7 106.76 14.44 8 -8 8 95.24 13.93 -8 -8 -8 84.89 6.17 -8 -8 -9 48.21 4.81 -8 -8 -10 51.11 4.93 -8 -8 -11 2.56 1.97 -8 -8 -12 42.90 4.46 -8 -8 -13 72.38 5.50 -8 -8 -14 81.32 6.54 -8 -8 -15 0.87 3.00 -8 -8 -16 -2.32 2.75 -8 -8 -17 4.38 2.86 -8 -8 -18 2.89 2.72 -8 -8 -19 27.81 4.25 -8 -8 -20 13.55 3.35 -8 -8 -21 1.27 2.38 -8 -8 -22 8.62 2.88 -8 -8 -23 5.40 2.17 -8 -8 -24 1.08 1.94 -8 -8 -25 26.65 3.26 -8 -8 -26 7.13 2.16 -8 -8 -27 2.28 1.53 -8 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98.13 14.00 10 -5 -18 20.92 4.18 -10 -5 18 20.34 4.13 10 -5 -18 14.84 6.54 10 -5 -18 23.07 3.91 10 -5 -17 141.29 8.20 10 -5 -17 154.36 17.14 -10 -5 17 139.32 8.30 10 -5 -17 139.17 8.31 10 -5 -16 47.12 5.22 -10 -5 16 53.58 5.38 10 -5 -16 47.05 10.13 10 -5 -16 41.38 4.91 10 -5 -15 133.23 8.08 10 -5 -15 118.05 14.59 -10 -5 15 129.75 7.96 10 -5 -15 122.77 7.83 10 -5 -14 8.19 3.12 10 -5 -14 9.61 4.12 -10 -5 14 8.84 3.20 10 -5 -14 6.08 2.72 10 -5 -13 334.47 12.17 10 -5 -13 309.75 22.66 -10 -5 13 351.01 12.55 10 -5 -13 338.32 12.45 10 -5 -12 1.79 2.64 10 -5 -12 1.97 4.49 10 -5 -12 0.64 4.38 -10 -5 12 5.71 3.00 10 -5 -12 -1.06 2.45 10 -5 -11 8.71 2.76 10 -5 -11 14.02 5.68 10 -5 -11 20.27 7.58 -10 -5 11 10.36 2.70 10 -5 -11 13.63 3.37 10 -5 -10 40.74 4.63 10 -5 -10 43.08 9.63 -10 -5 10 39.23 4.62 10 -5 -10 36.46 4.44 10 -5 -9 13.79 3.33 10 -5 -9 6.83 5.40 -10 -5 9 10.62 2.78 10 -5 -9 9.90 2.91 10 -5 -8 273.31 10.67 10 -5 -8 270.33 22.30 -10 -5 8 274.25 10.87 10 -5 -8 274.46 10.97 -10 -5 7 148.03 7.96 10 -5 -7 168.27 8.42 10 -5 -7 167.60 8.66 10 -5 -6 -0.22 2.02 10 -5 -6 -3.54 5.37 -10 -5 6 -1.15 1.94 10 -5 -6 5.05 2.52 10 -5 -5 144.59 7.77 10 -5 -5 142.25 8.17 10 -5 -5 128.60 15.61 -10 -5 5 143.89 7.74 10 -5 -4 44.44 4.81 10 -5 -4 35.05 8.07 -10 -5 4 47.98 4.69 10 -5 -3 64.76 5.40 10 -5 -3 66.90 11.73 -10 -5 3 66.02 5.38 10 -5 -2 0.90 2.10 10 -5 -2 5.76 5.27 -10 -5 2 3.36 1.89 10 -5 -1 404.66 27.16 10 -5 -1 416.96 12.95 10 -5 0 4.21 2.43 10 -5 0 8.28 5.73 10 -5 1 -0.83 2.01 10 -5 1 1.60 4.33 10 -5 2 18.65 3.42 10 -5 2 21.50 6.84 10 -5 3 20.07 3.46 10 -5 3 22.17 7.98 10 -5 4 2.67 2.63 10 -5 4 0.32 4.49 10 -5 5 93.30 6.43 10 -5 5 99.08 14.30 10 -5 6 169.04 8.51 10 -5 6 168.37 18.24 10 -5 7 8.75 2.94 10 -5 7 6.90 5.22 10 -5 8 22.04 3.63 10 -5 8 33.20 8.09 10 -5 9 83.80 6.19 10 -5 9 103.80 14.91 10 -5 10 162.71 8.48 10 -5 10 156.36 18.31 10 -5 11 4.61 2.63 10 -5 11 6.17 5.82 10 -5 12 6.10 2.92 10 -5 13 40.79 4.72 10 -5 14 77.01 6.13 10 -5 15 143.34 8.12 10 -5 16 5.50 2.97 10 5 17 7.39 2.52 10 -5 17 11.35 3.32 10 5 18 26.43 3.67 10 5 19 4.08 2.41 10 5 20 10.78 2.61 10 5 21 25.42 3.54 10 5 22 9.45 2.61 -10 -5 -22 4.56 2.33 10 -5 22 3.89 1.58 10 5 23 24.63 3.21 -10 -5 -23 17.10 2.92 10 -5 23 18.63 2.48 10 5 24 -0.72 1.67 10 -5 24 -1.72 1.48 10 5 25 6.85 1.99 -10 -5 -25 6.07 1.95 10 -5 25 7.02 1.82 10 5 26 2.02 1.44 -10 -5 -26 2.63 1.56 10 -5 26 -0.51 0.62 10 5 27 14.86 2.18 10 5 28 1.65 1.24 10 5 29 4.29 1.22 10 -6 -37 1.26 1.24 10 -6 -36 4.91 1.72 10 -6 -35 5.54 1.86 10 -6 -34 29.94 3.28 10 -6 -33 6.15 2.39 10 -6 -32 7.32 2.67 -10 -6 32 2.02 1.50 10 -6 -31 2.24 2.51 -10 -6 31 3.73 1.93 10 -6 -30 1.44 2.77 -10 -6 30 1.18 1.81 10 -6 -29 9.69 3.33 -10 -6 29 8.78 2.60 10 -6 -28 35.07 4.64 -10 -6 28 18.57 3.32 10 -6 -27 100.49 7.25 -10 -6 27 78.17 5.91 10 -6 -27 88.20 5.90 10 -6 -26 -0.24 2.83 -10 -6 26 0.07 2.49 10 -6 -26 -2.40 1.94 10 -6 -25 9.94 3.58 -10 -6 25 0.72 2.45 10 -6 -25 9.52 2.72 10 -6 -24 15.38 3.99 -10 -6 24 8.90 2.76 10 -6 -24 7.50 2.31 10 -6 -23 5.21 3.18 -10 -6 23 -2.78 2.84 10 -6 -23 -0.82 2.53 10 -6 -22 67.88 6.40 -10 -6 22 74.22 6.31 10 -6 -22 69.46 5.87 10 -6 -21 22.47 4.41 -10 -6 21 15.29 3.75 10 -6 -21 15.95 3.63 10 -6 -20 20.12 4.19 -10 -6 20 23.88 4.03 10 -6 -20 20.12 3.83 10 -6 -19 7.25 3.11 -10 -6 19 7.19 3.13 10 -6 -19 8.80 3.14 10 -6 -18 19.15 3.97 -10 -6 18 26.64 4.28 10 -6 -18 24.34 4.33 10 -6 -17 136.52 8.25 -10 -6 17 115.55 7.80 10 -6 -17 119.91 7.90 10 -6 -16 5.10 2.98 -10 -6 16 1.80 2.70 10 -6 -16 0.50 2.60 10 -6 -15 55.60 5.40 10 -6 -15 51.42 10.78 -10 -6 15 49.21 5.41 10 -6 -15 49.71 5.39 10 -6 -14 38.66 4.86 10 -6 -14 39.27 9.71 -10 -6 14 43.07 5.11 10 -6 -14 40.61 5.16 10 -6 -13 136.73 8.10 10 -6 -13 134.54 16.48 -10 -6 13 135.25 8.25 10 -6 -13 137.56 8.30 10 -6 -12 22.16 3.88 10 -6 -12 26.17 6.82 -10 -6 12 27.56 4.37 10 -6 -12 17.68 3.80 10 -6 -11 4.83 2.99 10 -6 -11 3.33 4.59 -10 -6 11 6.83 3.04 10 -6 -11 7.29 2.95 10 -6 -10 194.52 9.37 10 -6 -10 182.25 19.53 -10 -6 10 202.70 9.65 10 -6 -10 201.36 9.81 10 -6 -9 0.37 2.24 10 -6 -9 0.33 3.90 -10 -6 9 0.39 2.45 10 -6 -9 3.44 2.64 10 -6 -8 1.39 2.36 10 -6 -8 -3.89 5.52 -10 -6 8 3.39 2.63 10 -6 -8 6.40 2.77 10 -6 -7 -1.17 2.44 10 -6 -7 7.00 5.43 -10 -6 7 1.35 2.36 10 -6 -7 -0.92 2.29 10 -6 -6 44.20 4.74 10 -6 -6 38.80 9.94 -10 -6 6 44.71 4.74 10 -6 -6 40.93 4.81 10 -6 -5 203.24 9.32 -10 -6 5 198.03 9.40 10 -6 -5 224.34 10.20 10 -6 -4 -1.86 2.85 10 -6 -4 3.29 4.80 -10 -6 4 1.77 2.25 10 -6 -4 10.09 3.14 10 -6 -3 35.99 4.37 10 -6 -3 35.83 8.77 10 -6 -2 109.06 6.85 10 -6 -2 112.50 14.99 10 -6 -1 31.90 4.11 10 -6 -1 30.00 8.70 10 -6 0 51.44 5.02 10 -6 0 63.69 11.74 10 -6 1 1.41 2.20 10 -6 1 6.67 5.81 10 -6 2 0.94 2.15 10 -6 2 -0.04 4.21 10 -6 3 5.68 2.33 10 -6 3 -4.23 5.28 10 -6 4 50.19 4.93 10 -6 4 63.12 11.58 10 -6 5 4.23 2.28 10 -6 5 -2.73 3.96 10 -6 6 52.07 5.05 10 -6 6 58.59 11.01 10 -6 7 47.87 4.89 10 -6 7 51.27 10.82 10 -6 8 13.16 3.32 10 -6 8 13.47 6.39 10 -6 9 67.47 5.66 10 -6 10 0.09 2.32 10 -6 11 92.76 6.56 10 -6 12 254.42 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setting) CELL 1.54184 15.362797 12.949697 35.884974 90.0000 99.4357 90.0000 ZERR 5.00 0.000244 0.000194 0.000562 0.0000 0.0015 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Mg Cr UNIT 335.00 455.00 20.00 15.00 10.00 5.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 13598 _shelx_fab_file ; -18 1 1 0.0161 0.1107 -18 1 2 -0.8224 -0.0400 -18 1 3 0.1876 0.1258 -18 1 4 -2.0327 -0.0720 -18 1 5 1.8495 -0.1609 -18 2 1 -0.1953 0.3259 -18 2 2 -2.3869 0.1665 -18 2 3 0.7970 0.0790 -18 2 4 0.0468 0.1634 -18 2 5 0.3998 -0.2314 -18 2 6 0.8425 0.0948 -18 2 7 -1.1843 -0.3125 -18 2 8 0.2060 -0.0870 -18 2 9 -0.6456 -0.0123 -18 2 10 -0.0502 -0.1272 -18 2 11 0.3319 0.2182 -18 2 12 -0.1304 -0.0308 -18 3 1 -0.3947 -0.0232 -18 3 2 -0.3041 0.2914 -18 3 3 0.7445 -0.1468 -18 3 4 0.7163 -0.0580 -18 3 5 -0.6362 -0.0411 -18 3 6 -1.0333 -0.3366 -18 3 7 -0.2059 0.0478 -18 3 8 -0.0886 -0.1526 -18 3 9 0.5881 0.0870 -18 3 10 1.4931 0.0914 -18 3 11 -0.2251 0.0497 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-0.0335 16 7 1 0.7906 -0.0652 16 7 2 0.7659 -0.1491 16 7 3 -0.5337 -0.0957 16 7 4 1.5444 0.2526 16 7 5 -0.3875 0.2021 16 7 6 -0.6065 0.3005 16 7 7 0.1137 -0.0009 16 8 0 0.5835 -0.1639 16 8 1 0.2535 -0.2324 17 0 0 0.3858 -0.5153 17 0 2 -0.6472 0.0682 17 0 4 -0.1571 -0.0436 17 0 6 1.0984 0.1389 17 0 8 -0.7688 0.0958 17 0 10 -1.5066 -0.2540 17 1 0 -0.3797 -0.0544 17 1 1 0.9985 0.0777 17 1 2 -1.0114 0.0609 17 1 3 0.4295 -0.0943 17 1 4 0.4695 0.1493 17 1 5 -0.9495 -0.0672 17 1 6 0.4361 0.0633 17 1 7 -0.0007 0.1787 17 1 8 -0.9871 -0.1860 17 1 9 0.7311 0.0003 17 1 10 0.0019 -0.0253 17 1 11 0.1253 -0.2152 17 2 0 -3.0345 -0.0807 17 2 1 -0.7397 -0.1869 17 2 2 -0.7775 -0.1249 17 2 3 -0.7231 0.1858 17 2 4 1.8530 0.0395 17 2 5 0.3908 0.1604 17 2 6 -0.0690 0.0438 17 2 7 0.5668 -0.0503 17 2 8 -0.5877 0.0171 17 2 9 0.0345 -0.2359 17 2 10 0.2177 -0.1510 17 2 11 -0.6792 0.2354 17 2 12 0.4406 -0.0330 17 3 0 0.2262 -0.2305 17 3 1 -0.3622 -0.0091 17 3 2 0.4001 0.0021 17 3 3 2.2834 -0.0082 17 3 4 0.6121 0.2701 17 3 5 -0.0043 0.0889 17 3 6 -0.8253 0.0665 17 3 7 -1.1893 -0.0021 17 3 8 0.1859 -0.4081 17 3 9 -0.3714 -0.0342 17 3 10 0.3043 0.0448 17 3 11 -0.1970 0.0637 17 4 0 -0.9275 0.0734 17 4 1 0.8780 0.0073 17 4 2 0.0153 0.1039 17 4 3 1.3572 0.2232 17 4 4 0.2539 0.0613 17 4 5 -0.6996 0.1588 17 4 6 0.2478 -0.1756 17 4 7 -0.2624 -0.3007 17 4 8 0.6363 0.0435 17 4 9 0.1299 -0.1144 17 4 10 -0.1586 0.2810 17 5 0 -0.4839 0.0205 17 5 1 1.4889 0.3154 17 5 2 0.2402 0.1298 17 5 3 0.0785 -0.1158 17 5 4 -1.0134 -0.0183 17 5 5 -1.4614 -0.3454 17 5 6 -0.2474 -0.0654 17 5 7 -0.6981 -0.0417 17 5 8 0.4512 0.1046 17 6 0 -0.5201 0.3398 17 6 1 -0.0790 -0.1168 17 6 2 0.5701 -0.1412 17 6 3 -0.0789 -0.2778 17 6 4 0.6289 -0.2100 18 1 0 -1.2850 -0.0519 18 1 1 0.2641 -0.2136 18 1 2 -0.7918 0.0009 18 1 3 -0.5273 -0.2923 18 2 0 -1.1029 -0.1460 18 2 1 -0.5872 -0.0989 18 2 2 1.8686 -0.0746 18 2 3 0.2673 0.2978 18 2 4 0.6508 0.0488 18 3 0 0.2581 -0.3509 18 3 1 0.5118 0.0476 18 3 2 0.2827 0.2000 18 3 3 0.5537 0.1311 18 3 4 -0.4633 0.3845 18 4 0 -0.3182 0.2097 18 4 1 0.7940 0.1256 18 4 2 0.4290 0.2654 0 0 0 0.0 0.0 ; _shelx_fab_checksum 87442 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.142 _oxdiff_exptl_absorpt_empirical_full_min 0.908 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3c _database_code_depnum_ccdc_archive 'CCDC 2116004' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT332_3c ; PROBLEM: Large Phenyl C-C Range C1A -C10 . 0.41 Ang. RESPONSE: Bond length range due to restrictions on the disorder of the split mod solvate. This has no significant effect on any aspect of the structure. ; _vrf_PLAT910_3c ; PROBLEM: Missing # of FCF Reflection(s) Below Theta(Min). 13 Note RESPONSE: The crystal was small and weakly diffracting at high angle ; _vrf_PLAT919_3c ; PROBLEM: Reflection # Likely Affected by the Beamstop ... 1 Check RESPONSE: reflection affected by position of beam stop ; _vrf_PLAT930_3c ; PROBLEM: FCF-based Twin Law ( 1-1 0) Est.d BASF 0.14 Check RESPONSE: crystal was slightly twinned but minor component had no significant effect on key atomic metrics ; _vrf_PLAT934_3c ; PROBLEM: Number of (Iobs-Icalc)/Sigma(W) > 10 Outliers .. 9 Check RESPONSE: The crystal was small and weakly diffracting ; _vrf_PLAT939_3c ; PROBLEM: Large Value of Not (SHELXL) Weight Optimized S . 108.07 Check RESPONSE: The crystal was small and weakly diffracting ; # Added during the CSD deposition process: Friday 15 October 2021 05:10 PM # end Validation Reply Form _audit_creation_date 2021-10-15 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _shelx_SHELXL_version_number 2018/3 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C63 H84 Fe Mg2 N4 O5, 2(C7 H8)' _chemical_formula_sum 'C77 H100 Fe Mg2 N4 O5' _chemical_formula_weight 1266.07 _chemical_melting_point ? _chemical_oxdiff_formula 'C63 H84 N4 Fe1 Mg2' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.3957(10) _cell_length_b 13.4353(8) _cell_length_c 22.6744(8) _cell_angle_alpha 99.136(4) _cell_angle_beta 97.078(4) _cell_angle_gamma 112.627(6) _cell_volume 3642.1(4) _cell_formula_units_Z 2 _cell_measurement_reflns_used 6849 _cell_measurement_temperature 173.00(14) _cell_measurement_theta_max 28.1240 _cell_measurement_theta_min 2.7200 _shelx_estimated_absorpt_T_max 0.978 _shelx_estimated_absorpt_T_min 0.952 _exptl_absorpt_coefficient_mu 0.275 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.85621 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear green' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier . _exptl_crystal_colour_primary green _exptl_crystal_density_diffrn 1.154 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1360 _exptl_crystal_preparation ? _exptl_crystal_recrystallization_method ? _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.08 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0288 _diffrn_reflns_av_unetI/netI 0.0624 _diffrn_reflns_Laue_measured_fraction_full 0.985 _diffrn_reflns_Laue_measured_fraction_max 0.799 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 20927 _diffrn_reflns_point_group_measured_fraction_full 0.985 _diffrn_reflns_point_group_measured_fraction_max 0.799 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.221 _diffrn_reflns_theta_min 2.576 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 173.00(14) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.0382 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.985 _diffrn_measured_fraction_theta_max 0.799 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -2.00 82.00 1.00 42.50 -- 14.43 57.00-180.00 84 2 \w -53.00 40.00 1.00 42.50 -- 14.43 -77.00 -90.00 93 3 \w -11.00 82.00 1.00 42.50 -- 14.43 77.00 30.00 93 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0199965000 _diffrn_orient_matrix_UB_12 0.0211332000 _diffrn_orient_matrix_UB_13 0.0318674000 _diffrn_orient_matrix_UB_21 -0.0400238000 _diffrn_orient_matrix_UB_22 0.0223407000 _diffrn_orient_matrix_UB_23 0.0011948000 _diffrn_orient_matrix_UB_31 -0.0378070000 _diffrn_orient_matrix_UB_32 -0.0500030000 _diffrn_orient_matrix_UB_33 0.0054524000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 10076 _reflns_number_total 14369 _reflns_odcompleteness_completeness 98.96 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 24.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 1.167 _refine_diff_density_min -0.599 _refine_diff_density_rms 0.116 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.116 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 922 _refine_ls_number_reflns 14369 _refine_ls_number_restraints 180 _refine_ls_R_factor_all 0.1270 _refine_ls_R_factor_gt 0.0980 _refine_ls_restrained_S_all 1.111 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1080P)^2^+19.3278P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3006 _refine_ls_wR_factor_ref 0.3168 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Rigid body (RIGU) restrains C3, C1, C027, C7, C02A, C026, C6, C9, H9A, C3A, C1A, C6A, C10, C02B, C7A with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 C029, C2, C025, C028, C0AA, C1AA, C024, C0, C2A, C4, C8, C0AB, C1AB, C5 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 3. Others Sof(C0)=Sof(H0A)=Sof(H0B)=Sof(H0C)=Sof(C2A)=Sof(C4)=Sof(H4A)=Sof(C8)=Sof(H8A)= Sof(C0AB)=Sof(H0AB)=Sof(C1AB)=Sof(H1AB)=Sof(C5)=Sof(H5A)=1-FVAR(1) Sof(C029)=Sof(H02J)=Sof(H02K)=Sof(H02L)=Sof(C2)=Sof(C025)=Sof(H025)=Sof(C028)= Sof(H028)=Sof(C0AA)=Sof(H0AA)=Sof(C1AA)=Sof(H1AA)=Sof(C024)=Sof(H024)=FVAR(1) Sof(C9)=Sof(H9A)=Sof(C3A)=Sof(C1A)=Sof(H1AC)=Sof(C6A)=Sof(H6AA)=Sof(H6AB)= Sof(H6AC)=Sof(C10)=Sof(H10A)=Sof(C02B)=Sof(H02N)=Sof(C7A)=Sof(H7AA)=1-FVAR(2) Sof(C3)=Sof(C1)=Sof(H1A)=Sof(C027)=Sof(H027)=Sof(C7)=Sof(H7A)=Sof(C02A)= Sof(H02M)=Sof(C026)=Sof(H026)=Sof(C6)=Sof(H6A)=Sof(H6B)=Sof(H6C)=FVAR(2) 4.a Ternary CH refined with riding coordinates: C00H(H00H), C00I(H00I), C00M(H00M), C00Y(H00Y), C018(H018), C019(H019), C01F(H01Q), C01I(H01V) 4.b Aromatic/amide H refined with riding coordinates: C00C(H00C), C00J(H00J), C00O(H00O), C00W(H00W), C00Z(H00Z), C010(H010), C011(H011), C012(H012), C015(H015), C01D(H01M), C01H(H01U), C01J(H01W), C01M(H01), C01N(H1), C01P(H3), C1(H1A), C027(H027), C7(H7A), C02A(H02M), C026(H026), C025(H025), C028(H028), C0AA(H0AA), C1AA(H1AA), C024(H024), C4(H4A), C8(H8A), C0AB(H0AB), C1AB(H1AB), C5(H5A), C9(H9A), C1A(H1AC), C10(H10A), C02B(H02N), C7A(H7AA) 4.c Fitted hexagon refined as free rotating group: C3(C1,C027,C7,C02A,C026), C2(C025,C028,C0AA,C1AA,C024), C2A(C4,C8,C0AB,C1AB,C5) 4.d Idealised Me refined as rotating group: C014(H01A,H01B,H01C), C016(H01D,H01E,H01F), C01B(H01G,H01H,H01I), C01C(H01J, H01K,H01L), C01E(H01N,H01O,H01P), C01G(H01R,H01S,H01T), C01K(H01X,H01Y,H), C01L(H01Z,HA,HB), C01O(H2,HC,HD), C01Q(H4,HE,HF), C01R(H5,HG,HH), C01S(H6,HI, HJ), C01T(H7,HK,HL), C01U(H8,HM,HN), C01V(H9,HO,HP), C01W(H10,HQ,HR), C01Y(H11, HS,HT), C021(H02A,H02B,H02C), C022(H02D,H02E,H02F), C023(H02G,H02H,H02I), C029(H02J,H02K,H02L), C6(H6A,H6B,H6C), C0(H0A,H0B,H0C), C6A(H6AA,H6AB,H6AC) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe01 Fe 0.16204(8) 0.88738(8) 0.27323(5) 0.0436(3) Uani 1 1 d . . . . . Mg02 Mg 0.41371(14) 0.75791(14) 0.21082(8) 0.0238(4) Uani 1 1 d . . . . . Mg03 Mg 0.23609(14) 0.58313(14) 0.28892(8) 0.0240(4) Uani 1 1 d . . . . . N004 N 0.2998(4) 0.5023(4) 0.34021(19) 0.0254(9) Uani 1 1 d . . . . . O005 O 0.2922(3) 0.8140(3) 0.19795(19) 0.0365(9) Uani 1 1 d . . . . . O006 O 0.1884(3) 0.7031(3) 0.30973(19) 0.0374(9) Uani 1 1 d . . . . . N007 N 0.5490(4) 0.9020(3) 0.2448(2) 0.0251(9) Uani 1 1 d . . . . . N008 N 0.4752(4) 0.7041(4) 0.14131(19) 0.0253(9) Uani 1 1 d . . . . . N009 N 0.0920(3) 0.4481(4) 0.2525(2) 0.0266(9) Uani 1 1 d . . . . . C00A C 0.6462(4) 0.9076(4) 0.2350(3) 0.0289(11) Uani 1 1 d . . . . . C00B C 0.3929(4) 0.5652(4) 0.3899(2) 0.0271(11) Uani 1 1 d . . . . . C00C C 0.6606(4) 0.8299(5) 0.1918(3) 0.0302(12) Uani 1 1 d . . . . . H00C H 0.733391 0.838688 0.194068 0.036 Uiso 1 1 calc R U . . . C00D C 0.5019(5) 0.5984(5) 0.3792(3) 0.0303(12) Uani 1 1 d . . . . . C00E C 0.3754(4) 0.5079(4) 0.0858(2) 0.0274(11) Uani 1 1 d . . . . . C00F C 0.4035(4) 0.6205(4) 0.0885(2) 0.0267(11) Uani 1 1 d . . . . . C00G C 0.2582(5) 0.3926(4) 0.3290(2) 0.0280(11) Uani 1 1 d . . . . . C00H C 0.4189(5) 0.4657(5) 0.1369(3) 0.0334(13) Uani 1 1 d . . . . . H00H H 0.470498 0.529747 0.168648 0.040 Uiso 1 1 calc R U . . . C00I C 0.5254(5) 0.5662(5) 0.3172(3) 0.0336(13) Uani 1 1 d . . . . . H00I H 0.455972 0.539656 0.287402 0.040 Uiso 1 1 calc R U . . . C00J C 0.3043(5) 0.4304(5) 0.0340(3) 0.0347(13) Uani 1 1 d . . . . . H00J H 0.285975 0.355514 0.031562 0.042 Uiso 1 1 calc R U . . . C00K C 0.5835(5) 0.7408(5) 0.1457(3) 0.0290(12) Uani 1 1 d . . . . . C00L C 0.5409(5) 1.0131(5) 0.3408(3) 0.0323(12) Uani 1 1 d . . . . . C00M C 0.5578(5) 0.9328(5) 0.3778(3) 0.0353(13) Uani 1 1 d . . . . . H00M H 0.573936 0.878569 0.350907 0.042 Uiso 1 1 calc R U . . . C00N C 0.5398(4) 0.9974(4) 0.2779(3) 0.0280(11) Uani 1 1 d . . . . . C00O C 0.2609(5) 0.4635(5) -0.0137(3) 0.0360(13) Uani 1 1 d . . . . . H00O H 0.214027 0.411025 -0.048187 0.043 Uiso 1 1 calc R U . . . C00P C -0.0038(4) 0.4672(5) 0.2317(3) 0.0318(12) Uani 1 1 d . . . . . C00Q C 0.0815(4) 0.3458(5) 0.2536(3) 0.0304(12) Uani 1 1 d . . . . . O00R O 0.2109(6) 1.0909(5) 0.2274(4) 0.090(2) Uani 1 1 d . . . . . C00S C -0.0125(5) 0.5049(5) 0.1781(3) 0.0375(14) Uani 1 1 d . . . . . C00T C 0.3572(5) 0.6540(5) 0.0404(2) 0.0316(12) Uani 1 1 d . . . . . C00U C 0.5236(5) 1.0725(5) 0.2453(3) 0.0343(13) Uani 1 1 d . . . . . C00V C 0.3743(5) 0.5955(5) 0.4478(3) 0.0333(12) Uani 1 1 d . . . . . C00W C 0.2868(5) 0.5736(5) -0.0103(3) 0.0371(13) Uani 1 1 d . . . . . H00W H 0.256705 0.594953 -0.042623 0.045 Uiso 1 1 calc R U . . . C00X C -0.0834(5) 0.4572(6) 0.2683(3) 0.0397(14) Uani 1 1 d . . . . . C00Y C 0.2584(5) 0.5627(6) 0.4610(3) 0.0404(14) Uani 1 1 d . . . . . H00Y H 0.205264 0.520574 0.422826 0.048 Uiso 1 1 calc R U . . . C00Z C 0.1619(5) 0.3231(5) 0.2853(3) 0.0327(12) Uani 1 1 d . . . . . H00Z H 0.150667 0.249124 0.276152 0.039 Uiso 1 1 calc R U . . . C010 C 0.5709(5) 0.6930(6) 0.4854(3) 0.0430(15) Uani 1 1 d . . . . . H010 H 0.630497 0.735975 0.517389 0.052 Uiso 1 1 calc R U . . . C011 C 0.5247(5) 1.1011(5) 0.3699(3) 0.0381(14) Uani 1 1 d . . . . . H011 H 0.525326 1.111533 0.411526 0.046 Uiso 1 1 calc R U . . . C012 C 0.5084(6) 1.1600(5) 0.2764(3) 0.0407(15) Uani 1 1 d . . . . . H012 H 0.498776 1.210534 0.255180 0.049 Uiso 1 1 calc R U . . . O013 O 0.2628(6) 0.9991(6) 0.4014(3) 0.084(2) Uani 1 1 d . . . . . C014 C 0.3247(6) 0.3960(6) 0.1653(3) 0.0442(15) Uani 1 1 d . . . . . H01A H 0.288088 0.440170 0.181069 0.066 Uiso 1 1 calc R U . . . H01B H 0.354526 0.371209 0.197818 0.066 Uiso 1 1 calc R U . . . H01C H 0.272802 0.333051 0.134718 0.066 Uiso 1 1 calc R U . . . C015 C 0.5885(5) 0.6622(5) 0.4281(3) 0.0399(14) Uani 1 1 d . . . . . H015 H 0.660618 0.684865 0.421941 0.048 Uiso 1 1 calc R U . . . C016 C 0.6082(7) 0.6593(6) 0.2979(3) 0.0534(18) Uani 1 1 d . . . . . H01D H 0.587164 0.720439 0.301720 0.080 Uiso 1 1 calc R U . . . H01E H 0.611439 0.635770 0.256249 0.080 Uiso 1 1 calc R U . . . H01F H 0.679370 0.681962 0.323435 0.080 Uiso 1 1 calc R U . . . C017 C 0.2405(5) 0.8461(5) 0.2279(3) 0.0356(13) Uani 1 1 d . . . . . C018 C -0.0760(5) 0.4207(6) 0.3287(3) 0.0463(16) Uani 1 1 d . . . . . H018 H -0.022210 0.387773 0.330358 0.056 Uiso 1 1 calc R U . . . C019 C 0.3829(6) 0.7756(5) 0.0428(3) 0.0420(15) Uani 1 1 d . . . . . H019 H 0.399481 0.812405 0.086020 0.050 Uiso 1 1 calc R U . . . O01A O -0.0772(6) 0.8240(7) 0.2416(4) 0.104(3) Uani 1 1 d . . . . . C01B C 0.3099(6) 0.3352(5) 0.3663(3) 0.0458(16) Uani 1 1 d . . . . . H01G H 0.382439 0.386789 0.387942 0.069 Uiso 1 1 calc R U . . . H01H H 0.315247 0.274965 0.339736 0.069 Uiso 1 1 calc R U . . . H01I H 0.265166 0.307172 0.394856 0.069 Uiso 1 1 calc R U . . . C01C C 0.6318(5) 0.6877(6) 0.0997(3) 0.0422(15) Uani 1 1 d . . . . . H01J H 0.642405 0.627587 0.113194 0.063 Uiso 1 1 calc R U . . . H01K H 0.701454 0.741689 0.096087 0.063 Uiso 1 1 calc R U . . . H01L H 0.581999 0.660170 0.060818 0.063 Uiso 1 1 calc R U . . . C01D C 0.1269(6) 0.7478(6) 0.2972(3) 0.0475(16) Uani 1 1 d . . . . . H01M H 0.053551 0.709587 0.299507 0.057 Uiso 1 1 calc R U . . . C01E C 0.4811(6) 0.3968(6) 0.1149(4) 0.0507(17) Uani 1 1 d . . . . . H01N H 0.429678 0.327987 0.088441 0.076 Uiso 1 1 calc R U . . . H01O H 0.517930 0.382296 0.149475 0.076 Uiso 1 1 calc R U . . . H01P H 0.534586 0.436884 0.093195 0.076 Uiso 1 1 calc R U . . . C01F C 0.0708(5) 0.5114(6) 0.1367(3) 0.0463(16) Uani 1 1 d . . . . . H01Q H 0.143466 0.535924 0.163025 0.056 Uiso 1 1 calc R U . . . C01G C 0.7515(5) 1.0044(5) 0.2719(3) 0.0467(16) Uani 1 1 d . . . . . H01R H 0.749765 1.072695 0.265593 0.070 Uiso 1 1 calc R U . . . H01S H 0.814542 0.997412 0.259003 0.070 Uiso 1 1 calc R U . . . H01T H 0.756244 1.003747 0.314463 0.070 Uiso 1 1 calc R U . . . C01H C 0.5069(6) 1.1762(5) 0.3378(3) 0.0426(15) Uani 1 1 d . . . . . H01U H 0.494559 1.235353 0.357534 0.051 Uiso 1 1 calc R U . . . C01I C 0.5237(6) 1.0586(6) 0.1772(3) 0.0462(16) Uani 1 1 d . . . . . H01V H 0.523131 0.985967 0.161748 0.055 Uiso 1 1 calc R U . . . C01J C 0.4639(6) 0.6596(6) 0.4953(3) 0.0417(15) Uani 1 1 d . . . . . H01W H 0.451891 0.680189 0.533994 0.050 Uiso 1 1 calc R U . . . C01K C 0.2358(6) 0.6612(7) 0.4846(4) 0.0563(19) Uani 1 1 d . . . . . H01X H 0.280488 0.698388 0.524590 0.084 Uiso 1 1 calc R U . . . H01Y H 0.159188 0.637083 0.486727 0.084 Uiso 1 1 calc R U . . . H H 0.253245 0.710977 0.457657 0.084 Uiso 1 1 calc R U . . . C01L C 0.4243(7) 1.0653(7) 0.1412(3) 0.059(2) Uani 1 1 d . . . . . H01Z H 0.358003 1.008025 0.146290 0.089 Uiso 1 1 calc R U . . . HA H 0.428097 1.055887 0.098825 0.089 Uiso 1 1 calc R U . . . HB H 0.423902 1.136219 0.155778 0.089 Uiso 1 1 calc R U . . . C01M C -0.0990(6) 0.5336(7) 0.1623(3) 0.0544(19) Uani 1 1 d . . . . . H01 H -0.104539 0.560532 0.127317 0.065 Uiso 1 1 calc R U . . . C01N C -0.1771(6) 0.5229(8) 0.1978(4) 0.064(2) Uani 1 1 d . . . . . H1 H -0.235839 0.540955 0.185954 0.077 Uiso 1 1 calc R U . . . C01O C 0.2874(7) 0.7956(7) 0.0119(4) 0.065(2) Uani 1 1 d . . . . . H2 H 0.268767 0.761070 -0.030713 0.097 Uiso 1 1 calc R U . . . HC H 0.308348 0.873693 0.016859 0.097 Uiso 1 1 calc R U . . . HD H 0.224578 0.764532 0.030126 0.097 Uiso 1 1 calc R U . . . C01P C -0.1695(6) 0.4867(7) 0.2492(4) 0.0558(19) Uani 1 1 d . . . . . H3 H -0.222727 0.481151 0.272766 0.067 Uiso 1 1 calc R U . . . C01Q C -0.0221(5) 0.2463(5) 0.2200(3) 0.0461(16) Uani 1 1 d . . . . . H4 H -0.063934 0.214192 0.248821 0.069 Uiso 1 1 calc R U . . . HE H -0.002437 0.192674 0.196985 0.069 Uiso 1 1 calc R U . . . HF H -0.065859 0.268826 0.192767 0.069 Uiso 1 1 calc R U . . . C01R C -0.1863(6) 0.3351(7) 0.3356(4) 0.060(2) Uani 1 1 d . . . . . H5 H -0.237875 0.368370 0.338283 0.089 Uiso 1 1 calc R U . . . HG H -0.175527 0.309215 0.371932 0.089 Uiso 1 1 calc R U . . . HH H -0.214631 0.273870 0.300813 0.089 Uiso 1 1 calc R U . . . C01S C 0.4530(6) 0.8704(6) 0.3997(4) 0.0555(19) Uani 1 1 d . . . . . H6 H 0.438288 0.921410 0.428235 0.083 Uiso 1 1 calc R U . . . HI H 0.462511 0.815340 0.419149 0.083 Uiso 1 1 calc R U . . . HJ H 0.392092 0.835238 0.365461 0.083 Uiso 1 1 calc R U . . . C01T C 0.0800(7) 0.5935(8) 0.0964(4) 0.065(2) Uani 1 1 d . . . . . H7 H 0.012048 0.567724 0.067248 0.098 Uiso 1 1 calc R U . . . HK H 0.139367 0.600226 0.075326 0.098 Uiso 1 1 calc R U . . . HL H 0.094300 0.664317 0.121187 0.098 Uiso 1 1 calc R U . . . C01U C 0.6546(6) 0.9917(7) 0.4319(4) 0.060(2) Uani 1 1 d . . . . . H8 H 0.717187 1.040369 0.418678 0.091 Uiso 1 1 calc R U . . . HM H 0.673132 0.937923 0.448244 0.091 Uiso 1 1 calc R U . . . HN H 0.634516 1.033868 0.462730 0.091 Uiso 1 1 calc R U . . . C01V C 0.0439(7) 0.3988(8) 0.0972(4) 0.065(2) Uani 1 1 d . . . . . H9 H 0.044542 0.348386 0.122762 0.098 Uiso 1 1 calc R U . . . HO H 0.098068 0.404887 0.072318 0.098 Uiso 1 1 calc R U . . . HP H -0.027893 0.371655 0.071571 0.098 Uiso 1 1 calc R U . . . C01W C -0.0348(6) 0.5213(7) 0.3814(3) 0.063(2) Uani 1 1 d . . . . . H10 H 0.038330 0.571073 0.379678 0.095 Uiso 1 1 calc R U . . . HQ H -0.033279 0.498064 0.419299 0.095 Uiso 1 1 calc R U . . . HR H -0.083316 0.558219 0.378547 0.095 Uiso 1 1 calc R U . . . C01X C 0.2260(7) 0.9583(8) 0.3520(4) 0.062(2) Uani 1 1 d . . . . . C01Y C 0.6282(8) 1.1480(9) 0.1661(4) 0.080(3) Uani 1 1 d . . . . . H11 H 0.637084 1.219477 0.187445 0.120 Uiso 1 1 calc R U . . . HS H 0.621634 1.145645 0.123202 0.120 Uiso 1 1 calc R U . . . HT H 0.691368 1.134737 0.180662 0.120 Uiso 1 1 calc R U . . . C01Z C 0.1918(7) 1.0142(7) 0.2455(4) 0.061(2) Uani 1 1 d . . . . . C020 C 0.0155(7) 0.8491(8) 0.2549(4) 0.065(2) Uani 1 1 d . . . . . C021 C 0.2391(9) 0.4888(8) 0.5069(5) 0.080(3) Uani 1 1 d . . . . . H02A H 0.255339 0.426510 0.492710 0.120 Uiso 1 1 calc R U . . . H02B H 0.163449 0.463040 0.511160 0.120 Uiso 1 1 calc R U . . . H02C H 0.286489 0.530237 0.545712 0.120 Uiso 1 1 calc R U . . . C022 C 0.5617(9) 0.4728(8) 0.3133(4) 0.076(3) Uani 1 1 d . . . . . H02D H 0.628382 0.495205 0.342979 0.114 Uiso 1 1 calc R U . . . H02E H 0.574925 0.454307 0.273238 0.114 Uiso 1 1 calc R U . . . H02F H 0.504946 0.409397 0.321331 0.114 Uiso 1 1 calc R U . . . C023 C 0.4857(7) 0.8309(7) 0.0177(5) 0.070(2) Uani 1 1 d . . . . . H02G H 0.546102 0.820041 0.038728 0.105 Uiso 1 1 calc R U . . . H02H H 0.503885 0.908720 0.023590 0.105 Uiso 1 1 calc R U . . . H02I H 0.471920 0.798894 -0.025050 0.105 Uiso 1 1 calc R U . . . C029 C -0.088(2) 0.848(3) 0.4076(11) 0.119(8) Uani 0.598(16) 1 d . . P A 1 H02J H -0.151965 0.864882 0.403509 0.178 Uiso 0.598(16) 1 calc R U P A 1 H02K H -0.103959 0.780417 0.379092 0.178 Uiso 0.598(16) 1 calc R U P A 1 H02L H -0.026999 0.907159 0.399377 0.178 Uiso 0.598(16) 1 calc R U P A 1 C3 C 0.9397(8) 0.8771(9) 0.0508(6) 0.091(4) Uani 0.706(16) 1 d G . P B 1 C1 C 0.8973(10) 0.8620(9) -0.0107(5) 0.090(4) Uani 0.706(16) 1 d G . P B 1 H1A H 0.921079 0.825016 -0.040220 0.108 Uiso 0.706(16) 1 calc R U P B 1 C027 C 0.8195(11) 0.9021(10) -0.0280(5) 0.114(5) Uani 0.706(16) 1 d G . P B 1 H027 H 0.791136 0.892039 -0.069110 0.137 Uiso 0.706(16) 1 calc R U P B 1 C7 C 0.7840(9) 0.9574(10) 0.0162(7) 0.115(5) Uani 0.706(16) 1 d G . P B 1 H7A H 0.731883 0.984232 0.004582 0.138 Uiso 0.706(16) 1 calc R U P B 1 C02A C 0.8263(11) 0.9724(11) 0.0776(6) 0.108(5) Uani 0.706(16) 1 d G . P B 1 H02M H 0.802573 1.009402 0.107165 0.130 Uiso 0.706(16) 1 calc R U P B 1 C026 C 0.9042(11) 0.9323(11) 0.0949(5) 0.095(4) Uani 0.706(16) 1 d G . P B 1 H026 H 0.932517 0.942380 0.136056 0.114 Uiso 0.706(16) 1 calc R U P B 1 C6 C 1.026(2) 0.837(2) 0.0722(12) 0.134(7) Uani 0.706(16) 1 d . . P B 1 H6A H 0.990079 0.764308 0.078870 0.201 Uiso 0.706(16) 1 calc R U P B 1 H6B H 1.072503 0.886693 0.109579 0.201 Uiso 0.706(16) 1 calc R U P B 1 H6C H 1.069304 0.836212 0.041747 0.201 Uiso 0.706(16) 1 calc R U P B 1 C2 C -0.0597(9) 0.8352(9) 0.4724(4) 0.075(4) Uani 0.598(16) 1 d G . P A 1 C025 C -0.1128(8) 0.8673(10) 0.5157(6) 0.076(6) Uani 0.598(16) 1 d G . P A 1 H025 H -0.165254 0.893971 0.504623 0.091 Uiso 0.598(16) 1 calc R U P A 1 C028 C -0.0874(10) 0.8597(10) 0.5757(5) 0.082(4) Uani 0.598(16) 1 d G . P A 1 H028 H -0.122907 0.881187 0.604703 0.098 Uiso 0.598(16) 1 calc R U P A 1 C0AA C -0.0089(10) 0.8198(11) 0.5923(5) 0.080(4) Uani 0.598(16) 1 d G . P A 1 H0AA H 0.008053 0.814725 0.632447 0.096 Uiso 0.598(16) 1 calc R U P A 1 C1AA C 0.0442(10) 0.7877(11) 0.5490(6) 0.092(5) Uani 0.598(16) 1 d G . P A 1 H1AA H 0.096666 0.761046 0.560110 0.110 Uiso 0.598(16) 1 calc R U P A 1 C024 C 0.0188(9) 0.7953(10) 0.4890(5) 0.076(4) Uani 0.598(16) 1 d G . P A 1 H024 H 0.054322 0.773829 0.460029 0.092 Uiso 0.598(16) 1 calc R U P A 1 C0 C -0.024(4) 0.865(4) 0.6094(17) 0.130(12) Uani 0.402(16) 1 d . . P A 2 H0A H -0.071286 0.799788 0.621240 0.195 Uiso 0.402(16) 1 calc R U P A 2 H0B H -0.042887 0.925049 0.623265 0.195 Uiso 0.402(16) 1 calc R U P A 2 H0C H 0.051510 0.883229 0.627330 0.195 Uiso 0.402(16) 1 calc R U P A 2 C2A C -0.0390(17) 0.8410(18) 0.5389(8) 0.099(7) Uani 0.402(16) 1 d G . P A 2 C4 C 0.0293(18) 0.806(2) 0.5081(12) 0.140(14) Uani 0.402(16) 1 d G . P A 2 H4A H 0.080613 0.786462 0.529230 0.168 Uiso 0.402(16) 1 calc R U P A 2 C8 C 0.021(2) 0.800(2) 0.4459(12) 0.128(11) Uani 0.402(16) 1 d G . P A 2 H8A H 0.066750 0.776356 0.425252 0.153 Uiso 0.402(16) 1 calc R U P A 2 C0AB C -0.056(2) 0.829(2) 0.4143(8) 0.099(8) Uani 0.402(16) 1 d G . P A 2 H0AB H -0.061141 0.824818 0.372661 0.119 Uiso 0.402(16) 1 calc R U P A 2 C1AB C -0.1239(16) 0.8640(18) 0.4451(10) 0.097(7) Uani 0.402(16) 1 d G . P A 2 H1AB H -0.175169 0.883388 0.424047 0.116 Uiso 0.402(16) 1 calc R U P A 2 C5 C -0.1156(15) 0.8700(18) 0.5074(10) 0.102(12) Uani 0.402(16) 1 d G . P A 2 H5A H -0.161308 0.893495 0.528025 0.122 Uiso 0.402(16) 1 calc R U P A 2 HU H 0.345(4) 0.661(4) 0.249(2) 0.005(11) Uiso 1 1 d . . . . . C9 C 0.853(2) 0.905(2) 0.0043(15) 0.060(6) Uani 0.294(16) 1 d . . P B 2 H9A H 0.811174 0.916740 -0.027492 0.072 Uiso 0.294(16) 1 calc R U P B 2 C3A C 0.859(3) 0.947(3) 0.0602(15) 0.062(6) Uani 0.294(16) 1 d . . P B 2 C1A C 0.937(4) 0.935(4) 0.1087(17) 0.070(8) Uani 0.294(16) 1 d . . P B 2 H1AC H 0.953167 0.976387 0.148464 0.084 Uiso 0.294(16) 1 calc R U P B 2 C6A C 0.790(3) 1.014(4) 0.0816(18) 0.091(10) Uani 0.294(16) 1 d . . P B 2 H6AA H 0.769849 1.044748 0.049062 0.137 Uiso 0.294(16) 1 calc R U P B 2 H6AB H 0.833592 1.072482 0.116484 0.137 Uiso 0.294(16) 1 calc R U P B 2 H6AC H 0.724237 0.964894 0.092207 0.137 Uiso 0.294(16) 1 calc R U P B 2 C10 C 0.983(3) 0.863(3) 0.0941(16) 0.073(8) Uani 0.294(16) 1 d . . P B 2 H10A H 1.014899 0.839936 0.124515 0.088 Uiso 0.294(16) 1 calc R U P B 2 C02B C 0.922(3) 0.832(3) -0.0085(17) 0.070(8) Uani 0.294(16) 1 d . . P B 2 H02N H 0.915642 0.795101 -0.048078 0.084 Uiso 0.294(16) 1 calc R U P B 2 C7A C 0.981(3) 0.825(2) 0.0326(15) 0.063(7) Uani 0.294(16) 1 d . . P B 2 H7AA H 1.028456 0.791570 0.023612 0.076 Uiso 0.294(16) 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe01 0.0454(6) 0.0462(6) 0.0545(6) 0.0126(4) 0.0158(4) 0.0329(5) Mg02 0.0229(9) 0.0213(8) 0.0268(9) 0.0034(7) 0.0080(7) 0.0086(7) Mg03 0.0204(8) 0.0249(9) 0.0267(9) 0.0071(7) 0.0052(7) 0.0087(7) N004 0.026(2) 0.028(2) 0.024(2) 0.0084(18) 0.0078(18) 0.0117(19) O005 0.032(2) 0.039(2) 0.046(2) 0.0142(19) 0.0114(19) 0.0191(19) O006 0.033(2) 0.035(2) 0.046(2) 0.0042(19) 0.0070(18) 0.0178(18) N007 0.027(2) 0.018(2) 0.029(2) 0.0048(17) 0.0065(18) 0.0077(18) N008 0.024(2) 0.024(2) 0.026(2) 0.0039(18) 0.0073(18) 0.0089(18) N009 0.021(2) 0.028(2) 0.029(2) 0.0052(19) 0.0068(18) 0.0077(18) C00A 0.023(3) 0.023(3) 0.036(3) 0.007(2) 0.006(2) 0.004(2) C00B 0.028(3) 0.025(3) 0.028(3) 0.009(2) 0.002(2) 0.010(2) C00C 0.023(3) 0.031(3) 0.037(3) 0.009(2) 0.010(2) 0.011(2) C00D 0.029(3) 0.031(3) 0.032(3) 0.009(2) 0.003(2) 0.015(2) C00E 0.025(3) 0.029(3) 0.029(3) 0.003(2) 0.008(2) 0.012(2) C00F 0.027(3) 0.026(3) 0.027(3) 0.002(2) 0.011(2) 0.011(2) C00G 0.033(3) 0.025(3) 0.032(3) 0.010(2) 0.013(2) 0.014(2) C00H 0.034(3) 0.025(3) 0.036(3) 0.004(2) 0.003(2) 0.010(2) C00I 0.027(3) 0.039(3) 0.039(3) 0.008(3) 0.008(2) 0.018(2) C00J 0.035(3) 0.033(3) 0.035(3) 0.002(2) 0.010(2) 0.014(3) C00K 0.031(3) 0.031(3) 0.034(3) 0.012(2) 0.015(2) 0.018(2) C00L 0.037(3) 0.026(3) 0.033(3) 0.007(2) 0.008(2) 0.012(2) C00M 0.050(4) 0.032(3) 0.031(3) 0.008(2) 0.007(3) 0.024(3) C00N 0.026(3) 0.023(3) 0.033(3) 0.005(2) 0.006(2) 0.008(2) C00O 0.036(3) 0.038(3) 0.027(3) -0.003(2) 0.004(2) 0.012(3) C00P 0.018(3) 0.033(3) 0.034(3) 0.000(2) 0.002(2) 0.003(2) C00Q 0.026(3) 0.028(3) 0.031(3) 0.001(2) 0.010(2) 0.006(2) O00R 0.117(6) 0.059(4) 0.128(6) 0.038(4) 0.040(5) 0.062(4) C00S 0.022(3) 0.050(4) 0.032(3) 0.004(3) -0.001(2) 0.011(3) C00T 0.038(3) 0.033(3) 0.026(3) 0.007(2) 0.011(2) 0.015(3) C00U 0.037(3) 0.028(3) 0.035(3) 0.006(2) 0.006(3) 0.011(2) C00V 0.038(3) 0.034(3) 0.032(3) 0.011(2) 0.008(2) 0.016(3) C00W 0.045(3) 0.043(3) 0.027(3) 0.007(3) 0.007(3) 0.022(3) C00X 0.024(3) 0.048(4) 0.043(4) 0.004(3) 0.007(3) 0.013(3) C00Y 0.039(3) 0.047(4) 0.033(3) 0.005(3) 0.013(3) 0.015(3) C00Z 0.036(3) 0.022(3) 0.040(3) 0.004(2) 0.011(3) 0.012(2) C010 0.039(4) 0.044(4) 0.033(3) 0.002(3) -0.009(3) 0.011(3) C011 0.046(4) 0.032(3) 0.032(3) 0.001(2) 0.005(3) 0.015(3) C012 0.053(4) 0.027(3) 0.042(4) 0.009(3) 0.003(3) 0.019(3) O013 0.076(4) 0.106(5) 0.061(4) -0.010(4) 0.006(3) 0.040(4) C014 0.049(4) 0.045(4) 0.037(3) 0.011(3) 0.011(3) 0.016(3) C015 0.024(3) 0.047(4) 0.047(4) 0.014(3) 0.002(3) 0.014(3) C016 0.061(5) 0.049(4) 0.045(4) 0.012(3) 0.017(3) 0.015(4) C017 0.035(3) 0.032(3) 0.044(3) 0.011(3) 0.007(3) 0.016(3) C018 0.036(3) 0.063(4) 0.042(4) 0.014(3) 0.018(3) 0.020(3) C019 0.058(4) 0.040(3) 0.031(3) 0.012(3) 0.009(3) 0.022(3) O01A 0.056(4) 0.140(7) 0.145(7) 0.047(6) 0.020(4) 0.064(4) C01B 0.049(4) 0.031(3) 0.063(4) 0.019(3) 0.010(3) 0.020(3) C01C 0.034(3) 0.048(4) 0.045(4) 0.003(3) 0.019(3) 0.017(3) C01D 0.044(4) 0.050(4) 0.067(5) 0.021(3) 0.023(3) 0.032(3) C01E 0.051(4) 0.043(4) 0.066(5) 0.012(3) 0.011(3) 0.028(3) C01F 0.032(3) 0.073(5) 0.035(3) 0.019(3) 0.007(3) 0.020(3) C01G 0.027(3) 0.039(3) 0.060(4) -0.001(3) 0.006(3) 0.005(3) C01H 0.055(4) 0.031(3) 0.043(4) -0.001(3) 0.005(3) 0.024(3) C01I 0.070(5) 0.036(3) 0.034(3) 0.008(3) 0.007(3) 0.025(3) C01J 0.050(4) 0.051(4) 0.022(3) 0.005(3) 0.003(3) 0.021(3) C01K 0.045(4) 0.063(5) 0.063(5) 0.003(4) 0.013(3) 0.029(4) C01L 0.076(5) 0.060(5) 0.039(4) 0.020(3) 0.003(4) 0.025(4) C01M 0.040(4) 0.087(6) 0.042(4) 0.019(4) 0.001(3) 0.033(4) C01N 0.035(4) 0.102(7) 0.060(5) 0.015(5) 0.001(3) 0.037(4) C01O 0.077(6) 0.052(5) 0.081(6) 0.026(4) 0.014(5) 0.039(4) C01P 0.033(4) 0.079(5) 0.057(4) 0.008(4) 0.012(3) 0.026(4) C01Q 0.030(3) 0.038(3) 0.056(4) 0.002(3) 0.003(3) 0.005(3) C01R 0.044(4) 0.062(5) 0.065(5) 0.015(4) 0.021(4) 0.011(4) C01S 0.058(5) 0.046(4) 0.062(5) 0.025(4) 0.008(4) 0.016(3) C01T 0.053(5) 0.090(6) 0.050(4) 0.032(4) 0.013(4) 0.018(4) C01U 0.049(4) 0.064(5) 0.061(5) 0.018(4) -0.005(4) 0.019(4) C01V 0.061(5) 0.084(6) 0.056(5) 0.011(4) 0.032(4) 0.031(4) C01W 0.045(4) 0.086(6) 0.044(4) 0.013(4) 0.013(3) 0.010(4) C01X 0.056(5) 0.077(6) 0.069(6) 0.017(5) 0.023(4) 0.041(4) C01Y 0.073(6) 0.121(8) 0.044(4) 0.025(5) 0.023(4) 0.032(6) C01Z 0.073(5) 0.058(5) 0.073(5) 0.013(4) 0.022(4) 0.048(4) C020 0.062(5) 0.079(6) 0.084(6) 0.030(5) 0.022(4) 0.054(5) C021 0.097(7) 0.080(6) 0.088(7) 0.047(5) 0.060(6) 0.040(6) C022 0.118(8) 0.077(6) 0.088(6) 0.046(5) 0.070(6) 0.074(6) C023 0.057(5) 0.050(5) 0.107(7) 0.039(5) 0.025(5) 0.016(4) C029 0.101(18) 0.14(2) 0.111(8) 0.026(11) 0.012(9) 0.047(16) C3 0.065(8) 0.069(8) 0.128(8) 0.031(7) 0.021(6) 0.012(6) C1 0.073(10) 0.035(7) 0.130(7) 0.021(6) 0.006(6) -0.009(5) C027 0.085(10) 0.080(10) 0.155(9) 0.033(9) 0.001(9) 0.014(8) C7 0.091(11) 0.079(10) 0.173(10) 0.055(9) 0.025(8) 0.024(8) C02A 0.073(10) 0.092(12) 0.167(9) 0.057(9) 0.041(8) 0.027(8) C026 0.066(10) 0.076(9) 0.138(8) 0.037(8) 0.032(8) 0.016(8) C6 0.130(14) 0.17(2) 0.145(14) 0.056(15) 0.038(12) 0.093(15) C2 0.055(7) 0.046(7) 0.108(7) 0.011(6) 0.016(6) 0.006(5) C025 0.046(11) 0.050(14) 0.118(8) 0.015(8) 0.019(7) 0.005(11) C028 0.063(8) 0.060(9) 0.118(8) 0.020(8) 0.028(7) 0.018(7) C0AA 0.067(8) 0.061(10) 0.107(8) 0.015(8) 0.024(7) 0.020(7) C1AA 0.087(11) 0.090(12) 0.108(8) 0.019(8) 0.027(7) 0.045(9) C024 0.070(9) 0.046(8) 0.105(8) 0.008(7) 0.023(6) 0.018(7) C0 0.12(3) 0.12(3) 0.126(12) 0.017(14) 0.031(12) 0.04(2) C2A 0.049(11) 0.076(15) 0.126(12) 0.007(11) 0.022(9) -0.018(9) C4 0.10(2) 0.19(4) 0.130(13) 0.029(16) 0.034(14) 0.06(3) C8 0.109(19) 0.15(3) 0.129(14) 0.022(16) 0.034(14) 0.054(19) C0AB 0.071(15) 0.078(18) 0.118(14) 0.002(13) 0.023(12) 0.005(12) C1AB 0.067(13) 0.066(14) 0.122(12) 0.001(12) 0.025(10) -0.004(10) C5 0.056(18) 0.09(3) 0.124(12) 0.007(13) 0.028(11) -0.01(2) C9 0.046(13) 0.042(12) 0.071(9) 0.018(8) 0.008(8) -0.003(9) C3A 0.049(13) 0.056(13) 0.072(9) 0.018(8) 0.008(8) 0.012(10) C1A 0.065(17) 0.070(16) 0.069(9) 0.008(10) 0.003(9) 0.028(14) C6A 0.09(2) 0.11(2) 0.091(15) 0.021(16) 0.013(16) 0.058(19) C10 0.076(17) 0.077(16) 0.066(10) 0.009(9) 0.004(9) 0.037(14) C02B 0.068(15) 0.060(17) 0.067(10) 0.010(10) 0.005(9) 0.016(13) C7A 0.064(14) 0.042(13) 0.067(10) 0.007(9) 0.004(9) 0.008(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe01 C017 1.733(6) . ? Fe01 C01D 1.934(7) . ? Fe01 C01X 1.813(10) . ? Fe01 C01Z 1.826(9) . ? Fe01 C020 1.802(8) . ? Mg02 Mg03 3.517(2) . ? Mg02 O005 2.048(4) . ? Mg02 N007 2.026(5) . ? Mg02 N008 2.025(5) . ? Mg02 HU 1.72(4) . ? Mg03 N004 2.032(5) . ? Mg03 O006 1.964(4) . ? Mg03 N009 2.034(5) . ? Mg03 HU 1.86(5) . ? N004 C00B 1.442(7) . ? N004 C00G 1.328(7) . ? O005 C017 1.175(7) . ? O006 C01D 1.223(7) . ? N007 C00A 1.324(7) . ? N007 C00N 1.435(7) . ? N008 C00F 1.441(7) . ? N008 C00K 1.325(7) . ? N009 C00P 1.442(7) . ? N009 C00Q 1.331(7) . ? C00A C00C 1.400(8) . ? C00A C01G 1.527(8) . ? C00B C00D 1.418(8) . ? C00B C00V 1.392(8) . ? C00C H00C 0.9300 . ? C00C C00K 1.407(8) . ? C00D C00I 1.512(8) . ? C00D C015 1.387(8) . ? C00E C00F 1.400(8) . ? C00E C00H 1.516(8) . ? C00E C00J 1.395(8) . ? C00F C00T 1.407(8) . ? C00G C00Z 1.408(8) . ? C00G C01B 1.504(8) . ? C00H H00H 0.9800 . ? C00H C014 1.539(9) . ? C00H C01E 1.531(9) . ? C00I H00I 0.9800 . ? C00I C016 1.487(9) . ? C00I C022 1.505(9) . ? C00J H00J 0.9300 . ? C00J C00O 1.379(9) . ? C00K C01C 1.517(8) . ? C00L C00M 1.532(8) . ? C00L C00N 1.405(8) . ? C00L C011 1.367(8) . ? C00M H00M 0.9800 . ? C00M C01S 1.523(10) . ? C00M C01U 1.524(9) . ? C00N C00U 1.407(8) . ? C00O H00O 0.9300 . ? C00O C00W 1.370(9) . ? C00P C00S 1.397(9) . ? C00P C00X 1.411(8) . ? C00Q C00Z 1.380(8) . ? C00Q C01Q 1.511(8) . ? O00R C01Z 1.120(10) . ? C00S C01F 1.531(9) . ? C00S C01M 1.380(9) . ? C00T C00W 1.391(8) . ? C00T C019 1.524(8) . ? C00U C012 1.370(8) . ? C00U C01I 1.524(9) . ? C00V C00Y 1.525(8) . ? C00V C01J 1.390(9) . ? C00W H00W 0.9300 . ? C00X C018 1.529(9) . ? C00X C01P 1.400(9) . ? C00Y H00Y 0.9800 . ? C00Y C01K 1.500(10) . ? C00Y C021 1.527(10) . ? C00Z H00Z 0.9300 . ? C010 H010 0.9300 . ? C010 C015 1.378(9) . ? C010 C01J 1.387(10) . ? C011 H011 0.9300 . ? C011 C01H 1.407(9) . ? C012 H012 0.9300 . ? C012 C01H 1.380(9) . ? O013 C01X 1.121(10) . ? C014 H01A 0.9600 . ? C014 H01B 0.9600 . ? C014 H01C 0.9600 . ? C015 H015 0.9300 . ? C016 H01D 0.9600 . ? C016 H01E 0.9600 . ? C016 H01F 0.9600 . ? C018 H018 0.9800 . ? C018 C01R 1.529(10) . ? C018 C01W 1.520(11) . ? C019 H019 0.9800 . ? C019 C01O 1.518(10) . ? C019 C023 1.521(10) . ? O01A C020 1.139(10) . ? C01B H01G 0.9600 . ? C01B H01H 0.9600 . ? C01B H01I 0.9600 . ? C01C H01J 0.9600 . ? C01C H01K 0.9600 . ? C01C H01L 0.9600 . ? C01D H01M 0.9300 . ? C01E H01N 0.9600 . ? C01E H01O 0.9600 . ? C01E H01P 0.9600 . ? C01F H01Q 0.9800 . ? C01F C01T 1.519(10) . ? C01F C01V 1.514(11) . ? C01G H01R 0.9600 . ? C01G H01S 0.9600 . ? C01G H01T 0.9600 . ? C01H H01U 0.9300 . ? C01I H01V 0.9800 . ? C01I C01L 1.515(10) . ? C01I C01Y 1.535(12) . ? C01J H01W 0.9300 . ? C01K H01X 0.9600 . ? C01K H01Y 0.9600 . ? C01K H 0.9600 . ? C01L H01Z 0.9600 . ? C01L HA 0.9600 . ? C01L HB 0.9600 . ? C01M H01 0.9300 . ? C01M C01N 1.375(11) . ? C01N H1 0.9300 . ? C01N C01P 1.339(11) . ? C01O H2 0.9600 . ? C01O HC 0.9600 . ? C01O HD 0.9600 . ? C01P H3 0.9300 . ? C01Q H4 0.9600 . ? C01Q HE 0.9600 . ? C01Q HF 0.9600 . ? C01R H5 0.9600 . ? C01R HG 0.9600 . ? C01R HH 0.9600 . ? C01S H6 0.9600 . ? C01S HI 0.9600 . ? C01S HJ 0.9600 . ? C01T H7 0.9600 . ? C01T HK 0.9600 . ? C01T HL 0.9600 . ? C01U H8 0.9600 . ? C01U HM 0.9600 . ? C01U HN 0.9600 . ? C01V H9 0.9600 . ? C01V HO 0.9600 . ? C01V HP 0.9600 . ? C01W H10 0.9600 . ? C01W HQ 0.9600 . ? C01W HR 0.9600 . ? C01Y H11 0.9600 . ? C01Y HS 0.9600 . ? C01Y HT 0.9600 . ? C021 H02A 0.9600 . ? C021 H02B 0.9600 . ? C021 H02C 0.9600 . ? C022 H02D 0.9600 . ? C022 H02E 0.9600 . ? C022 H02F 0.9600 . ? C023 H02G 0.9600 . ? C023 H02H 0.9600 . ? C023 H02I 0.9600 . ? C029 H02J 0.9600 . ? C029 H02K 0.9600 . ? C029 H02L 0.9600 . ? C029 C2 1.53(3) . ? C3 C1 1.3900 . ? C3 C026 1.3900 . ? C3 C6 1.50(3) . ? C1 H1A 0.9300 . ? C1 C027 1.3900 . ? C027 H027 0.9300 . ? C027 C7 1.3900 . ? C7 H7A 0.9300 . ? C7 C02A 1.3900 . ? C02A H02M 0.9300 . ? C02A C026 1.3900 . ? C026 H026 0.9300 . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C2 C025 1.3900 . ? C2 C024 1.3900 . ? C025 H025 0.9300 . ? C025 C028 1.3900 . ? C028 H028 0.9300 . ? C028 C0AA 1.3900 . ? C0AA H0AA 0.9300 . ? C0AA C1AA 1.3900 . ? C1AA H1AA 0.9300 . ? C1AA C024 1.3900 . ? C024 H024 0.9300 . ? C0 H0A 0.9600 . ? C0 H0B 0.9600 . ? C0 H0C 0.9600 . ? C0 C2A 1.55(4) . ? C2A C4 1.3900 . ? C2A C5 1.3900 . ? C4 H4A 0.9300 . ? C4 C8 1.3900 . ? C8 H8A 0.9300 . ? C8 C0AB 1.3900 . ? C0AB H0AB 0.9300 . ? C0AB C1AB 1.3900 . ? C1AB H1AB 0.9300 . ? C1AB C5 1.3900 . ? C5 H5A 0.9300 . ? C9 H9A 0.9300 . ? C9 C3A 1.28(5) . ? C9 C02B 1.60(5) . ? C3A C1A 1.49(4) . ? C3A C6A 1.58(5) . ? C1A H1AC 0.9300 . ? C1A C10 1.35(5) . ? C6A H6AA 0.9600 . ? C6A H6AB 0.9600 . ? C6A H6AC 0.9600 . ? C10 H10A 0.9300 . ? C10 C7A 1.40(5) . ? C02B H02N 0.9300 . ? C02B C7A 1.19(5) . ? C7A H7AA 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C017 Fe01 C01D 85.6(3) . . ? C017 Fe01 C01X 118.1(3) . . ? C017 Fe01 C01Z 92.3(3) . . ? C017 Fe01 C020 126.9(4) . . ? C01X Fe01 C01D 88.9(4) . . ? C01X Fe01 C01Z 94.8(4) . . ? C01Z Fe01 C01D 176.3(4) . . ? C020 Fe01 C01D 87.1(3) . . ? C020 Fe01 C01X 114.2(4) . . ? C020 Fe01 C01Z 91.8(4) . . ? Mg03 Mg02 HU 11.2(15) . . ? O005 Mg02 Mg03 83.99(13) . . ? O005 Mg02 HU 95.1(15) . . ? N007 Mg02 Mg03 129.28(14) . . ? N007 Mg02 O005 101.27(19) . . ? N007 Mg02 HU 128.0(15) . . ? N008 Mg02 Mg03 124.13(14) . . ? N008 Mg02 O005 122.79(19) . . ? N008 Mg02 N007 95.35(19) . . ? N008 Mg02 HU 116.1(15) . . ? Mg02 Mg03 HU 10.3(14) . . ? N004 Mg03 Mg02 117.03(14) . . ? N004 Mg03 N009 94.09(19) . . ? N004 Mg03 HU 107.3(14) . . ? O006 Mg03 Mg02 85.59(14) . . ? O006 Mg03 N004 132.9(2) . . ? O006 Mg03 N009 103.55(19) . . ? O006 Mg03 HU 95.1(14) . . ? N009 Mg03 Mg02 127.60(15) . . ? N009 Mg03 HU 128.5(14) . . ? C00B N004 Mg03 119.5(3) . . ? C00G N004 Mg03 121.7(4) . . ? C00G N004 C00B 118.8(4) . . ? C017 O005 Mg02 137.6(4) . . ? C01D O006 Mg03 149.6(5) . . ? C00A N007 Mg02 118.9(4) . . ? C00A N007 C00N 120.2(4) . . ? C00N N007 Mg02 120.8(3) . . ? C00F N008 Mg02 121.2(3) . . ? C00K N008 Mg02 119.8(4) . . ? C00K N008 C00F 118.8(4) . . ? C00P N009 Mg03 117.5(3) . . ? C00Q N009 Mg03 122.2(4) . . ? C00Q N009 C00P 119.9(4) . . ? N007 C00A C00C 124.3(5) . . ? N007 C00A C01G 119.5(5) . . ? C00C C00A C01G 116.2(5) . . ? C00D C00B N004 120.0(5) . . ? C00V C00B N004 119.3(5) . . ? C00V C00B C00D 120.7(5) . . ? C00A C00C H00C 114.6 . . ? C00A C00C C00K 130.9(5) . . ? C00K C00C H00C 114.6 . . ? C00B C00D C00I 122.2(5) . . ? C015 C00D C00B 117.8(5) . . ? C015 C00D C00I 120.1(5) . . ? C00F C00E C00H 123.0(5) . . ? C00J C00E C00F 119.0(5) . . ? C00J C00E C00H 118.0(5) . . ? C00E C00F N008 121.4(5) . . ? C00E C00F C00T 120.1(5) . . ? C00T C00F N008 118.4(5) . . ? N004 C00G C00Z 123.7(5) . . ? N004 C00G C01B 120.4(5) . . ? C00Z C00G C01B 115.8(5) . . ? C00E C00H H00H 108.1 . . ? C00E C00H C014 111.1(5) . . ? C00E C00H C01E 112.0(5) . . ? C014 C00H H00H 108.1 . . ? C01E C00H H00H 108.1 . . ? C01E C00H C014 109.2(5) . . ? C00D C00I H00I 107.2 . . ? C016 C00I C00D 113.9(5) . . ? C016 C00I H00I 107.2 . . ? C016 C00I C022 108.8(6) . . ? C022 C00I C00D 112.0(5) . . ? C022 C00I H00I 107.2 . . ? C00E C00J H00J 119.6 . . ? C00O C00J C00E 120.8(6) . . ? C00O C00J H00J 119.6 . . ? N008 C00K C00C 123.5(5) . . ? N008 C00K C01C 120.8(5) . . ? C00C C00K C01C 115.7(5) . . ? C00N C00L C00M 121.8(5) . . ? C011 C00L C00M 118.7(5) . . ? C011 C00L C00N 119.6(5) . . ? C00L C00M H00M 108.0 . . ? C01S C00M C00L 110.6(5) . . ? C01S C00M H00M 108.0 . . ? C01S C00M C01U 110.0(6) . . ? C01U C00M C00L 112.0(5) . . ? C01U C00M H00M 108.0 . . ? C00L C00N N007 121.3(5) . . ? C00L C00N C00U 120.3(5) . . ? C00U C00N N007 118.3(5) . . ? C00J C00O H00O 120.0 . . ? C00W C00O C00J 120.0(5) . . ? C00W C00O H00O 120.0 . . ? C00S C00P N009 119.8(5) . . ? C00S C00P C00X 120.3(5) . . ? C00X C00P N009 119.7(5) . . ? N009 C00Q C00Z 123.2(5) . . ? N009 C00Q C01Q 121.1(5) . . ? C00Z C00Q C01Q 115.7(5) . . ? C00P C00S C01F 120.6(5) . . ? C01M C00S C00P 118.9(6) . . ? C01M C00S C01F 120.6(6) . . ? C00F C00T C019 121.5(5) . . ? C00W C00T C00F 118.7(5) . . ? C00W C00T C019 119.8(5) . . ? C00N C00U C01I 121.5(5) . . ? C012 C00U C00N 118.2(5) . . ? C012 C00U C01I 120.3(5) . . ? C00B C00V C00Y 122.4(5) . . ? C01J C00V C00B 119.3(6) . . ? C01J C00V C00Y 118.3(5) . . ? C00O C00W C00T 121.4(6) . . ? C00O C00W H00W 119.3 . . ? C00T C00W H00W 119.3 . . ? C00P C00X C018 122.7(5) . . ? C01P C00X C00P 117.7(6) . . ? C01P C00X C018 119.5(6) . . ? C00V C00Y H00Y 108.0 . . ? C00V C00Y C021 111.3(6) . . ? C01K C00Y C00V 112.5(6) . . ? C01K C00Y H00Y 108.0 . . ? C01K C00Y C021 108.9(6) . . ? C021 C00Y H00Y 108.0 . . ? C00G C00Z H00Z 114.4 . . ? C00Q C00Z C00G 131.1(5) . . ? C00Q C00Z H00Z 114.4 . . ? C015 C010 H010 120.2 . . ? C015 C010 C01J 119.6(6) . . ? C01J C010 H010 120.2 . . ? C00L C011 H011 119.6 . . ? C00L C011 C01H 120.9(6) . . ? C01H C011 H011 119.6 . . ? C00U C012 H012 118.6 . . ? C00U C012 C01H 122.7(6) . . ? C01H C012 H012 118.6 . . ? C00H C014 H01A 109.5 . . ? C00H C014 H01B 109.5 . . ? C00H C014 H01C 109.5 . . ? H01A C014 H01B 109.5 . . ? H01A C014 H01C 109.5 . . ? H01B C014 H01C 109.5 . . ? C00D C015 H015 119.0 . . ? C010 C015 C00D 122.0(6) . . ? C010 C015 H015 119.0 . . ? C00I C016 H01D 109.5 . . ? C00I C016 H01E 109.5 . . ? C00I C016 H01F 109.5 . . ? H01D C016 H01E 109.5 . . ? H01D C016 H01F 109.5 . . ? H01E C016 H01F 109.5 . . ? O005 C017 Fe01 177.1(5) . . ? C00X C018 H018 108.3 . . ? C01R C018 C00X 112.8(6) . . ? C01R C018 H018 108.3 . . ? C01W C018 C00X 109.4(6) . . ? C01W C018 H018 108.3 . . ? C01W C018 C01R 109.6(6) . . ? C00T C019 H019 106.8 . . ? C01O C019 C00T 114.1(6) . . ? C01O C019 H019 106.8 . . ? C01O C019 C023 110.4(6) . . ? C023 C019 C00T 111.5(6) . . ? C023 C019 H019 106.8 . . ? C00G C01B H01G 109.5 . . ? C00G C01B H01H 109.5 . . ? C00G C01B H01I 109.5 . . ? H01G C01B H01H 109.5 . . ? H01G C01B H01I 109.5 . . ? H01H C01B H01I 109.5 . . ? C00K C01C H01J 109.5 . . ? C00K C01C H01K 109.5 . . ? C00K C01C H01L 109.5 . . ? H01J C01C H01K 109.5 . . ? H01J C01C H01L 109.5 . . ? H01K C01C H01L 109.5 . . ? Fe01 C01D H01M 115.7 . . ? O006 C01D Fe01 128.6(5) . . ? O006 C01D H01M 115.7 . . ? C00H C01E H01N 109.5 . . ? C00H C01E H01O 109.5 . . ? C00H C01E H01P 109.5 . . ? H01N C01E H01O 109.5 . . ? H01N C01E H01P 109.5 . . ? H01O C01E H01P 109.5 . . ? C00S C01F H01Q 107.5 . . ? C01T C01F C00S 113.6(6) . . ? C01T C01F H01Q 107.5 . . ? C01V C01F C00S 111.1(6) . . ? C01V C01F H01Q 107.5 . . ? C01V C01F C01T 109.3(6) . . ? C00A C01G H01R 109.5 . . ? C00A C01G H01S 109.5 . . ? C00A C01G H01T 109.5 . . ? H01R C01G H01S 109.5 . . ? H01R C01G H01T 109.5 . . ? H01S C01G H01T 109.5 . . ? C011 C01H H01U 120.9 . . ? C012 C01H C011 118.3(6) . . ? C012 C01H H01U 120.9 . . ? C00U C01I H01V 108.5 . . ? C00U C01I C01Y 110.5(6) . . ? C01L C01I C00U 112.7(6) . . ? C01L C01I H01V 108.5 . . ? C01L C01I C01Y 108.2(6) . . ? C01Y C01I H01V 108.5 . . ? C00V C01J H01W 119.7 . . ? C010 C01J C00V 120.6(6) . . ? C010 C01J H01W 119.7 . . ? C00Y C01K H01X 109.5 . . ? C00Y C01K H01Y 109.5 . . ? C00Y C01K H 109.5 . . ? H01X C01K H01Y 109.5 . . ? H01X C01K H 109.5 . . ? H01Y C01K H 109.5 . . ? C01I C01L H01Z 109.5 . . ? C01I C01L HA 109.5 . . ? C01I C01L HB 109.5 . . ? H01Z C01L HA 109.5 . . ? H01Z C01L HB 109.5 . . ? HA C01L HB 109.5 . . ? C00S C01M H01 119.6 . . ? C01N C01M C00S 120.9(7) . . ? C01N C01M H01 119.6 . . ? C01M C01N H1 119.7 . . ? C01P C01N C01M 120.7(7) . . ? C01P C01N H1 119.7 . . ? C019 C01O H2 109.5 . . ? C019 C01O HC 109.5 . . ? C019 C01O HD 109.5 . . ? H2 C01O HC 109.5 . . ? H2 C01O HD 109.5 . . ? HC C01O HD 109.5 . . ? C00X C01P H3 119.2 . . ? C01N C01P C00X 121.6(7) . . ? C01N C01P H3 119.2 . . ? C00Q C01Q H4 109.5 . . ? C00Q C01Q HE 109.5 . . ? C00Q C01Q HF 109.5 . . ? H4 C01Q HE 109.5 . . ? H4 C01Q HF 109.5 . . ? HE C01Q HF 109.5 . . ? C018 C01R H5 109.5 . . ? C018 C01R HG 109.5 . . ? C018 C01R HH 109.5 . . ? H5 C01R HG 109.5 . . ? H5 C01R HH 109.5 . . ? HG C01R HH 109.5 . . ? C00M C01S H6 109.5 . . ? C00M C01S HI 109.5 . . ? C00M C01S HJ 109.5 . . ? H6 C01S HI 109.5 . . ? H6 C01S HJ 109.5 . . ? HI C01S HJ 109.5 . . ? C01F C01T H7 109.5 . . ? C01F C01T HK 109.5 . . ? C01F C01T HL 109.5 . . ? H7 C01T HK 109.5 . . ? H7 C01T HL 109.5 . . ? HK C01T HL 109.5 . . ? C00M C01U H8 109.5 . . ? C00M C01U HM 109.5 . . ? C00M C01U HN 109.5 . . ? H8 C01U HM 109.5 . . ? H8 C01U HN 109.5 . . ? HM C01U HN 109.5 . . ? C01F C01V H9 109.5 . . ? C01F C01V HO 109.5 . . ? C01F C01V HP 109.5 . . ? H9 C01V HO 109.5 . . ? H9 C01V HP 109.5 . . ? HO C01V HP 109.5 . . ? C018 C01W H10 109.5 . . ? C018 C01W HQ 109.5 . . ? C018 C01W HR 109.5 . . ? H10 C01W HQ 109.5 . . ? H10 C01W HR 109.5 . . ? HQ C01W HR 109.5 . . ? O013 C01X Fe01 177.5(9) . . ? C01I C01Y H11 109.5 . . ? C01I C01Y HS 109.5 . . ? C01I C01Y HT 109.5 . . ? H11 C01Y HS 109.5 . . ? H11 C01Y HT 109.5 . . ? HS C01Y HT 109.5 . . ? O00R C01Z Fe01 178.3(8) . . ? O01A C020 Fe01 178.1(9) . . ? C00Y C021 H02A 109.5 . . ? C00Y C021 H02B 109.5 . . ? C00Y C021 H02C 109.5 . . ? H02A C021 H02B 109.5 . . ? H02A C021 H02C 109.5 . . ? H02B C021 H02C 109.5 . . ? C00I C022 H02D 109.5 . . ? C00I C022 H02E 109.5 . . ? C00I C022 H02F 109.5 . . ? H02D C022 H02E 109.5 . . ? H02D C022 H02F 109.5 . . ? H02E C022 H02F 109.5 . . ? C019 C023 H02G 109.5 . . ? C019 C023 H02H 109.5 . . ? C019 C023 H02I 109.5 . . ? H02G C023 H02H 109.5 . . ? H02G C023 H02I 109.5 . . ? H02H C023 H02I 109.5 . . ? H02J C029 H02K 109.5 . . ? H02J C029 H02L 109.5 . . ? H02K C029 H02L 109.5 . . ? C2 C029 H02J 109.5 . . ? C2 C029 H02K 109.5 . . ? C2 C029 H02L 109.5 . . ? C1 C3 C026 120.0 . . ? C1 C3 C6 122.4(14) . . ? C026 C3 C6 117.6(14) . . ? C3 C1 H1A 120.0 . . ? C3 C1 C027 120.0 . . ? C027 C1 H1A 120.0 . . ? C1 C027 H027 120.0 . . ? C1 C027 C7 120.0 . . ? C7 C027 H027 120.0 . . ? C027 C7 H7A 120.0 . . ? C027 C7 C02A 120.0 . . ? C02A C7 H7A 120.0 . . ? C7 C02A H02M 120.0 . . ? C026 C02A C7 120.0 . . ? C026 C02A H02M 120.0 . . ? C3 C026 H026 120.0 . . ? C02A C026 C3 120.0 . . ? C02A C026 H026 120.0 . . ? C3 C6 H6A 109.5 . . ? C3 C6 H6B 109.5 . . ? C3 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C025 C2 C029 117.9(13) . . ? C025 C2 C024 120.0 . . ? C024 C2 C029 122.1(13) . . ? C2 C025 H025 120.0 . . ? C028 C025 C2 120.0 . . ? C028 C025 H025 120.0 . . ? C025 C028 H028 120.0 . . ? C0AA C028 C025 120.0 . . ? C0AA C028 H028 120.0 . . ? C028 C0AA H0AA 120.0 . . ? C1AA C0AA C028 120.0 . . ? C1AA C0AA H0AA 120.0 . . ? C0AA C1AA H1AA 120.0 . . ? C0AA C1AA C024 120.0 . . ? C024 C1AA H1AA 120.0 . . ? C2 C024 H024 120.0 . . ? C1AA C024 C2 120.0 . . ? C1AA C024 H024 120.0 . . ? H0A C0 H0B 109.5 . . ? H0A C0 H0C 109.5 . . ? H0B C0 H0C 109.5 . . ? C2A C0 H0A 109.5 . . ? C2A C0 H0B 109.5 . . ? C2A C0 H0C 109.5 . . ? C4 C2A C0 123(2) . . ? C4 C2A C5 120.0 . . ? C5 C2A C0 117(2) . . ? C2A C4 H4A 120.0 . . ? C8 C4 C2A 120.0 . . ? C8 C4 H4A 120.0 . . ? C4 C8 H8A 120.0 . . ? C4 C8 C0AB 120.0 . . ? C0AB C8 H8A 120.0 . . ? C8 C0AB H0AB 120.0 . . ? C8 C0AB C1AB 120.0 . . ? C1AB C0AB H0AB 120.0 . . ? C0AB C1AB H1AB 120.0 . . ? C5 C1AB C0AB 120.0 . . ? C5 C1AB H1AB 120.0 . . ? C2A C5 H5A 120.0 . . ? C1AB C5 C2A 120.0 . . ? C1AB C5 H5A 120.0 . . ? C3A C9 H9A 121.4 . . ? C3A C9 C02B 117(3) . . ? C02B C9 H9A 121.4 . . ? C9 C3A C1A 119(3) . . ? C9 C3A C6A 124(3) . . ? C1A C3A C6A 117(3) . . ? C3A C1A H1AC 120.5 . . ? C10 C1A C3A 119(3) . . ? C10 C1A H1AC 120.5 . . ? C3A C6A H6AA 109.5 . . ? C3A C6A H6AB 109.5 . . ? C3A C6A H6AC 109.5 . . ? H6AA C6A H6AB 109.5 . . ? H6AA C6A H6AC 109.5 . . ? H6AB C6A H6AC 109.5 . . ? C1A C10 H10A 120.3 . . ? C1A C10 C7A 119(4) . . ? C7A C10 H10A 120.3 . . ? C9 C02B H02N 120.0 . . ? C7A C02B C9 120(4) . . ? C7A C02B H02N 120.0 . . ? C10 C7A H7AA 118.4 . . ? C02B C7A C10 123(4) . . ? C02B C7A H7AA 118.4 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Mg02 N007 C00A C00C 14.7(7) . . . . ? Mg02 N007 C00A C01G -165.7(4) . . . . ? Mg02 N007 C00N C00L 85.4(6) . . . . ? Mg02 N007 C00N C00U -91.2(5) . . . . ? Mg02 N008 C00F C00E -91.0(5) . . . . ? Mg02 N008 C00F C00T 85.8(5) . . . . ? Mg02 N008 C00K C00C -11.1(7) . . . . ? Mg02 N008 C00K C01C 169.3(4) . . . . ? Mg03 N004 C00B C00D -88.0(5) . . . . ? Mg03 N004 C00B C00V 90.0(5) . . . . ? Mg03 N004 C00G C00Z -5.9(7) . . . . ? Mg03 N004 C00G C01B 177.6(4) . . . . ? Mg03 O006 C01D Fe01 -110.3(9) . . . . ? Mg03 N009 C00P C00S 73.2(6) . . . . ? Mg03 N009 C00P C00X -101.1(5) . . . . ? Mg03 N009 C00Q C00Z 7.7(7) . . . . ? Mg03 N009 C00Q C01Q -173.0(4) . . . . ? N004 C00B C00D C00I -2.6(8) . . . . ? N004 C00B C00D C015 177.7(5) . . . . ? N004 C00B C00V C00Y 1.3(8) . . . . ? N004 C00B C00V C01J -177.7(5) . . . . ? N004 C00G C00Z C00Q -12.7(10) . . . . ? N007 C00A C00C C00K 8.8(10) . . . . ? N007 C00N C00U C012 176.3(5) . . . . ? N007 C00N C00U C01I -4.3(8) . . . . ? N008 C00F C00T C00W -179.2(5) . . . . ? N008 C00F C00T C019 1.0(8) . . . . ? N009 C00P C00S C01F 8.2(9) . . . . ? N009 C00P C00S C01M -173.3(6) . . . . ? N009 C00P C00X C018 -3.2(9) . . . . ? N009 C00P C00X C01P 174.0(6) . . . . ? N009 C00Q C00Z C00G 11.7(10) . . . . ? C00A N007 C00N C00L -95.9(7) . . . . ? C00A N007 C00N C00U 87.6(7) . . . . ? C00A C00C C00K N008 -11.0(10) . . . . ? C00A C00C C00K C01C 168.6(6) . . . . ? C00B N004 C00G C00Z 174.3(5) . . . . ? C00B N004 C00G C01B -2.1(8) . . . . ? C00B C00D C00I C016 133.7(6) . . . . ? C00B C00D C00I C022 -102.2(7) . . . . ? C00B C00D C015 C010 0.0(9) . . . . ? C00B C00V C00Y C01K -120.2(7) . . . . ? C00B C00V C00Y C021 117.4(7) . . . . ? C00B C00V C01J C010 -0.1(9) . . . . ? C00D C00B C00V C00Y 179.2(5) . . . . ? C00D C00B C00V C01J 0.3(8) . . . . ? C00E C00F C00T C00W -2.3(8) . . . . ? C00E C00F C00T C019 177.9(5) . . . . ? C00E C00J C00O C00W -0.5(9) . . . . ? C00F N008 C00K C00C 173.2(5) . . . . ? C00F N008 C00K C01C -6.5(8) . . . . ? C00F C00E C00H C014 115.5(6) . . . . ? C00F C00E C00H C01E -122.1(6) . . . . ? C00F C00E C00J C00O -0.8(8) . . . . ? C00F C00T C00W C00O 1.0(9) . . . . ? C00F C00T C019 C01O -146.1(6) . . . . ? C00F C00T C019 C023 88.1(7) . . . . ? C00G N004 C00B C00D 91.7(6) . . . . ? C00G N004 C00B C00V -90.3(6) . . . . ? C00H C00E C00F N008 -1.1(8) . . . . ? C00H C00E C00F C00T -177.8(5) . . . . ? C00H C00E C00J C00O 179.3(5) . . . . ? C00I C00D C015 C010 -179.7(6) . . . . ? C00J C00E C00F N008 179.0(5) . . . . ? C00J C00E C00F C00T 2.3(8) . . . . ? C00J C00E C00H C014 -64.6(7) . . . . ? C00J C00E C00H C01E 57.8(7) . . . . ? C00J C00O C00W C00T 0.4(9) . . . . ? C00K N008 C00F C00E 84.7(6) . . . . ? C00K N008 C00F C00T -98.5(6) . . . . ? C00L C00N C00U C012 -0.3(9) . . . . ? C00L C00N C00U C01I 179.1(6) . . . . ? C00L C011 C01H C012 -1.2(10) . . . . ? C00M C00L C00N N007 3.2(8) . . . . ? C00M C00L C00N C00U 179.7(5) . . . . ? C00M C00L C011 C01H -179.0(6) . . . . ? C00N N007 C00A C00C -164.1(5) . . . . ? C00N N007 C00A C01G 15.5(8) . . . . ? C00N C00L C00M C01S -112.5(7) . . . . ? C00N C00L C00M C01U 124.3(6) . . . . ? C00N C00L C011 C01H 0.0(9) . . . . ? C00N C00U C012 C01H -1.0(10) . . . . ? C00N C00U C01I C01L 130.0(6) . . . . ? C00N C00U C01I C01Y -108.8(7) . . . . ? C00P N009 C00Q C00Z -164.6(5) . . . . ? C00P N009 C00Q C01Q 14.7(8) . . . . ? C00P C00S C01F C01T -156.7(6) . . . . ? C00P C00S C01F C01V 79.5(8) . . . . ? C00P C00S C01M C01N -1.6(11) . . . . ? C00P C00X C018 C01R -135.2(7) . . . . ? C00P C00X C018 C01W 102.5(7) . . . . ? C00P C00X C01P C01N 0.3(11) . . . . ? C00Q N009 C00P C00S -114.1(6) . . . . ? C00Q N009 C00P C00X 71.5(7) . . . . ? C00S C00P C00X C018 -177.6(6) . . . . ? C00S C00P C00X C01P -0.4(9) . . . . ? C00S C01M C01N C01P 1.6(13) . . . . ? C00U C012 C01H C011 1.7(10) . . . . ? C00V C00B C00D C00I 179.4(5) . . . . ? C00V C00B C00D C015 -0.3(8) . . . . ? C00W C00T C019 C01O 34.1(9) . . . . ? C00W C00T C019 C023 -91.7(8) . . . . ? C00X C00P C00S C01F -177.5(6) . . . . ? C00X C00P C00S C01M 1.0(9) . . . . ? C00Y C00V C01J C010 -179.1(6) . . . . ? C011 C00L C00M C01S 66.4(7) . . . . ? C011 C00L C00M C01U -56.8(8) . . . . ? C011 C00L C00N N007 -175.7(5) . . . . ? C011 C00L C00N C00U 0.8(9) . . . . ? C012 C00U C01I C01L -50.6(9) . . . . ? C012 C00U C01I C01Y 70.5(9) . . . . ? C015 C00D C00I C016 -46.6(8) . . . . ? C015 C00D C00I C022 77.5(8) . . . . ? C015 C010 C01J C00V -0.1(10) . . . . ? C018 C00X C01P C01N 177.6(8) . . . . ? C019 C00T C00W C00O -179.2(6) . . . . ? C01B C00G C00Z C00Q 163.9(6) . . . . ? C01F C00S C01M C01N 176.9(7) . . . . ? C01G C00A C00C C00K -170.8(6) . . . . ? C01I C00U C012 C01H 179.6(6) . . . . ? C01J C00V C00Y C01K 58.8(8) . . . . ? C01J C00V C00Y C021 -63.7(8) . . . . ? C01J C010 C015 C00D 0.2(10) . . . . ? C01M C00S C01F C01T 24.8(10) . . . . ? C01M C00S C01F C01V -99.0(8) . . . . ? C01M C01N C01P C00X -0.9(14) . . . . ? C01P C00X C018 C01R 47.6(9) . . . . ? C01P C00X C018 C01W -74.6(8) . . . . ? C01Q C00Q C00Z C00G -167.7(6) . . . . ? C029 C2 C025 C028 -178.4(17) . . . . ? C029 C2 C024 C1AA 178.3(17) . . . . ? C3 C1 C027 C7 0.0 . . . . ? C1 C3 C026 C02A 0.0 . . . . ? C1 C027 C7 C02A 0.0 . . . . ? C027 C7 C02A C026 0.0 . . . . ? C7 C02A C026 C3 0.0 . . . . ? C026 C3 C1 C027 0.0 . . . . ? C6 C3 C1 C027 -178.7(15) . . . . ? C6 C3 C026 C02A 178.8(14) . . . . ? C2 C025 C028 C0AA 0.0 . . . . ? C025 C2 C024 C1AA 0.0 . . . . ? C025 C028 C0AA C1AA 0.0 . . . . ? C028 C0AA C1AA C024 0.0 . . . . ? C0AA C1AA C024 C2 0.0 . . . . ? C024 C2 C025 C028 0.0 . . . . ? C0 C2A C4 C8 -172(2) . . . . ? C0 C2A C5 C1AB 172(2) . . . . ? C2A C4 C8 C0AB 0.0 . . . . ? C4 C2A C5 C1AB 0.0 . . . . ? C4 C8 C0AB C1AB 0.0 . . . . ? C8 C0AB C1AB C5 0.0 . . . . ? C0AB C1AB C5 C2A 0.0 . . . . ? C5 C2A C4 C8 0.0 . . . . ? C9 C3A C1A C10 -13(6) . . . . ? C9 C02B C7A C10 10(6) . . . . ? C3A C9 C02B C7A -5(5) . . . . ? C3A C1A C10 C7A 17(6) . . . . ? C1A C10 C7A C02B -17(6) . . . . ? C6A C3A C1A C10 168(4) . . . . ? C02B C9 C3A C1A 6(4) . . . . ? C02B C9 C3A C6A -175(3) . . . . ? _shelx_res_file ; TITL mrc2111_a.res in P-1 mrc2111.res created by SHELXL-2018/3 at 12:24:18 on 15-Oct-2021 REM Old TITL MRC2111 in P-1 REM SHELXT solution in P-1 REM R1 0.252, Rweak 0.033, Alpha 0.130, Orientation as input REM Formula found by SHELXT: C69 N10 Mg2 Fe CELL 0.71073 13.3957 13.4353 22.6744 99.136 97.078 112.627 ZERR 2 0.001 0.0008 0.0008 0.004 0.004 0.006 LATT 1 SFAC C H Fe Mg N O UNIT 154 200 2 4 8 10 RIGU 0.001 0.001 C3 C1 C027 C7 C02A C026 C6 C9 H9a C3A C1A C6A C10 C02B C7A RIGU 0.001 0.001 C029 C2 C025 C028 C0AA C1AA C024 C0 C2A C4 C8 C0AB C1AB C5 L.S. 99 0 0 PLAN 20 SIZE 0.08 0.16 0.18 CONF list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.108000 19.327799 FVAR 0.48991 0.59836 0.70613 FE01 3 0.162045 0.887380 0.273233 11.00000 0.04535 0.04621 = 0.05446 0.01261 0.01578 0.03293 MG02 4 0.413710 0.757912 0.210825 11.00000 0.02287 0.02126 = 0.02675 0.00344 0.00796 0.00858 MG03 4 0.236089 0.583127 0.288918 11.00000 0.02040 0.02490 = 0.02671 0.00707 0.00515 0.00869 N004 5 0.299839 0.502330 0.340210 11.00000 0.02635 0.02797 = 0.02407 0.00837 0.00784 0.01172 O005 6 0.292243 0.813963 0.197953 11.00000 0.03158 0.03873 = 0.04630 0.01419 0.01141 0.01911 O006 6 0.188384 0.703147 0.309734 11.00000 0.03326 0.03487 = 0.04564 0.00424 0.00701 0.01779 N007 5 0.548979 0.901979 0.244756 11.00000 0.02666 0.01805 = 0.02912 0.00475 0.00653 0.00770 N008 5 0.475165 0.704115 0.141312 11.00000 0.02444 0.02434 = 0.02592 0.00393 0.00732 0.00890 N009 5 0.092006 0.448101 0.252450 11.00000 0.02058 0.02815 = 0.02894 0.00516 0.00678 0.00770 C00A 1 0.646228 0.907619 0.234952 11.00000 0.02257 0.02251 = 0.03640 0.00688 0.00609 0.00381 C00B 1 0.392938 0.565209 0.389933 11.00000 0.02789 0.02468 = 0.02796 0.00876 0.00241 0.00977 C00C 1 0.660598 0.829924 0.191845 11.00000 0.02330 0.03134 = 0.03728 0.00855 0.00964 0.01115 AFIX 43 H00C 2 0.733391 0.838688 0.194068 11.00000 -1.20000 AFIX 0 C00D 1 0.501929 0.598446 0.379203 11.00000 0.02894 0.03138 = 0.03220 0.00890 0.00265 0.01460 C00E 1 0.375414 0.507938 0.085824 11.00000 0.02475 0.02940 = 0.02855 0.00308 0.00826 0.01212 C00F 1 0.403500 0.620530 0.088519 11.00000 0.02671 0.02643 = 0.02702 0.00156 0.01120 0.01112 C00G 1 0.258193 0.392576 0.329027 11.00000 0.03251 0.02520 = 0.03161 0.00960 0.01312 0.01443 C00H 1 0.418941 0.465686 0.136851 11.00000 0.03417 0.02509 = 0.03645 0.00404 0.00347 0.00978 AFIX 13 H00H 2 0.470498 0.529747 0.168648 11.00000 -1.20000 AFIX 0 C00I 1 0.525359 0.566201 0.317161 11.00000 0.02657 0.03925 = 0.03942 0.00836 0.00791 0.01799 AFIX 13 H00I 2 0.455972 0.539656 0.287402 11.00000 -1.20000 AFIX 0 C00J 1 0.304317 0.430414 0.033983 11.00000 0.03497 0.03286 = 0.03485 0.00178 0.01040 0.01372 AFIX 43 H00J 2 0.285975 0.355514 0.031562 11.00000 -1.20000 AFIX 0 C00K 1 0.583480 0.740826 0.145731 11.00000 0.03143 0.03056 = 0.03388 0.01202 0.01504 0.01792 C00L 1 0.540880 1.013094 0.340760 11.00000 0.03706 0.02599 = 0.03310 0.00698 0.00820 0.01187 C00M 1 0.557797 0.932771 0.377754 11.00000 0.04964 0.03241 = 0.03071 0.00779 0.00721 0.02426 AFIX 13 H00M 2 0.573936 0.878569 0.350907 11.00000 -1.20000 AFIX 0 C00N 1 0.539824 0.997365 0.277908 11.00000 0.02551 0.02318 = 0.03317 0.00477 0.00647 0.00829 C00O 1 0.260886 0.463457 -0.013726 11.00000 0.03581 0.03835 = 0.02677 -0.00290 0.00384 0.01235 AFIX 43 H00O 2 0.214027 0.411025 -0.048187 11.00000 -1.20000 AFIX 0 C00P 1 -0.003817 0.467177 0.231652 11.00000 0.01838 0.03286 = 0.03372 0.00004 0.00214 0.00338 C00Q 1 0.081452 0.345847 0.253563 11.00000 0.02591 0.02831 = 0.03141 0.00119 0.01004 0.00629 O00R 6 0.210886 1.090888 0.227360 11.00000 0.11740 0.05872 = 0.12799 0.03842 0.03974 0.06212 C00S 1 -0.012526 0.504854 0.178059 11.00000 0.02244 0.04979 = 0.03242 0.00387 -0.00066 0.01068 C00T 1 0.357192 0.654011 0.040410 11.00000 0.03796 0.03288 = 0.02586 0.00672 0.01059 0.01539 C00U 1 0.523555 1.072456 0.245258 11.00000 0.03715 0.02756 = 0.03535 0.00593 0.00557 0.01145 C00V 1 0.374296 0.595537 0.447776 11.00000 0.03762 0.03362 = 0.03182 0.01096 0.00807 0.01631 C00W 1 0.286807 0.573553 -0.010324 11.00000 0.04461 0.04310 = 0.02718 0.00673 0.00720 0.02238 AFIX 43 H00W 2 0.256705 0.594953 -0.042623 11.00000 -1.20000 AFIX 0 C00X 1 -0.083414 0.457158 0.268334 11.00000 0.02406 0.04779 = 0.04350 0.00398 0.00691 0.01333 C00Y 1 0.258423 0.562692 0.461044 11.00000 0.03874 0.04715 = 0.03271 0.00469 0.01293 0.01501 AFIX 13 H00Y 2 0.205264 0.520574 0.422826 11.00000 -1.20000 AFIX 0 C00Z 1 0.161945 0.323101 0.285266 11.00000 0.03552 0.02234 = 0.04047 0.00418 0.01116 0.01233 AFIX 43 H00Z 2 0.150667 0.249124 0.276152 11.00000 -1.20000 AFIX 0 C010 1 0.570927 0.693016 0.485446 11.00000 0.03919 0.04434 = 0.03286 0.00212 -0.00911 0.01136 AFIX 43 H010 2 0.630497 0.735975 0.517389 11.00000 -1.20000 AFIX 0 C011 1 0.524652 1.101146 0.369915 11.00000 0.04646 0.03200 = 0.03208 0.00145 0.00509 0.01528 AFIX 43 H011 2 0.525326 1.111533 0.411526 11.00000 -1.20000 AFIX 0 C012 1 0.508438 1.159975 0.276367 11.00000 0.05291 0.02736 = 0.04235 0.00910 0.00291 0.01877 AFIX 43 H012 2 0.498776 1.210534 0.255180 11.00000 -1.20000 AFIX 0 O013 6 0.262808 0.999093 0.401358 11.00000 0.07632 0.10588 = 0.06080 -0.00984 0.00584 0.03998 C014 1 0.324728 0.395972 0.165289 11.00000 0.04860 0.04519 = 0.03749 0.01135 0.01073 0.01643 AFIX 137 H01A 2 0.288088 0.440170 0.181069 11.00000 -1.50000 H01B 2 0.354526 0.371209 0.197818 11.00000 -1.50000 H01C 2 0.272802 0.333051 0.134718 11.00000 -1.50000 AFIX 0 C015 1 0.588534 0.662224 0.428082 11.00000 0.02444 0.04735 = 0.04679 0.01357 0.00190 0.01415 AFIX 43 H015 2 0.660618 0.684865 0.421941 11.00000 -1.20000 AFIX 0 C016 1 0.608169 0.659344 0.297938 11.00000 0.06134 0.04937 = 0.04467 0.01186 0.01733 0.01542 AFIX 137 H01D 2 0.587164 0.720439 0.301720 11.00000 -1.50000 H01E 2 0.611439 0.635770 0.256249 11.00000 -1.50000 H01F 2 0.679370 0.681962 0.323435 11.00000 -1.50000 AFIX 0 C017 1 0.240508 0.846123 0.227879 11.00000 0.03451 0.03171 = 0.04382 0.01093 0.00691 0.01637 C018 1 -0.075990 0.420720 0.328670 11.00000 0.03633 0.06338 = 0.04203 0.01395 0.01768 0.01991 AFIX 13 H018 2 -0.022210 0.387773 0.330358 11.00000 -1.20000 AFIX 0 C019 1 0.382894 0.775589 0.042846 11.00000 0.05816 0.03969 = 0.03090 0.01188 0.00909 0.02153 AFIX 13 H019 2 0.399481 0.812405 0.086020 11.00000 -1.20000 AFIX 0 O01A 6 -0.077163 0.824024 0.241604 11.00000 0.05587 0.13954 = 0.14453 0.04652 0.02004 0.06422 C01B 1 0.309939 0.335187 0.366256 11.00000 0.04925 0.03077 = 0.06343 0.01881 0.01037 0.01997 AFIX 137 H01G 2 0.382439 0.386789 0.387942 11.00000 -1.50000 H01H 2 0.315247 0.274965 0.339736 11.00000 -1.50000 H01I 2 0.265166 0.307172 0.394856 11.00000 -1.50000 AFIX 0 C01C 1 0.631766 0.687692 0.099737 11.00000 0.03374 0.04846 = 0.04464 0.00283 0.01895 0.01685 AFIX 137 H01J 2 0.642405 0.627587 0.113194 11.00000 -1.50000 H01K 2 0.701454 0.741689 0.096087 11.00000 -1.50000 H01L 2 0.581999 0.660170 0.060818 11.00000 -1.50000 AFIX 0 C01D 1 0.126909 0.747798 0.297205 11.00000 0.04367 0.05000 = 0.06678 0.02074 0.02261 0.03201 AFIX 43 H01M 2 0.053551 0.709587 0.299507 11.00000 -1.20000 AFIX 0 C01E 1 0.481080 0.396786 0.114947 11.00000 0.05060 0.04289 = 0.06649 0.01218 0.01111 0.02788 AFIX 137 H01N 2 0.429678 0.327987 0.088441 11.00000 -1.50000 H01O 2 0.517930 0.382296 0.149475 11.00000 -1.50000 H01P 2 0.534586 0.436884 0.093195 11.00000 -1.50000 AFIX 0 C01F 1 0.070808 0.511433 0.136675 11.00000 0.03240 0.07282 = 0.03466 0.01864 0.00699 0.02007 AFIX 13 H01Q 2 0.143466 0.535924 0.163025 11.00000 -1.20000 AFIX 0 C01G 1 0.751467 1.004350 0.271937 11.00000 0.02744 0.03875 = 0.06047 -0.00084 0.00626 0.00485 AFIX 137 H01R 2 0.749765 1.072695 0.265593 11.00000 -1.50000 H01S 2 0.814542 0.997412 0.259003 11.00000 -1.50000 H01T 2 0.756244 1.003747 0.314463 11.00000 -1.50000 AFIX 0 C01H 1 0.506950 1.176244 0.337828 11.00000 0.05466 0.03127 = 0.04269 -0.00058 0.00453 0.02355 AFIX 43 H01U 2 0.494559 1.235353 0.357534 11.00000 -1.20000 AFIX 0 C01I 1 0.523707 1.058598 0.177243 11.00000 0.07031 0.03572 = 0.03418 0.00769 0.00744 0.02456 AFIX 13 H01V 2 0.523131 0.985967 0.161748 11.00000 -1.20000 AFIX 0 C01J 1 0.463877 0.659584 0.495276 11.00000 0.04972 0.05119 = 0.02165 0.00513 0.00292 0.02064 AFIX 43 H01W 2 0.451891 0.680189 0.533994 11.00000 -1.20000 AFIX 0 C01K 1 0.235799 0.661152 0.484629 11.00000 0.04523 0.06321 = 0.06302 0.00329 0.01314 0.02856 AFIX 137 H01X 2 0.280488 0.698388 0.524590 11.00000 -1.50000 H01Y 2 0.159188 0.637083 0.486727 11.00000 -1.50000 H 2 0.253245 0.710977 0.457657 11.00000 -1.50000 AFIX 0 C01L 1 0.424328 1.065295 0.141237 11.00000 0.07576 0.06034 = 0.03907 0.02022 0.00279 0.02499 AFIX 137 H01Z 2 0.358003 1.008025 0.146290 11.00000 -1.50000 HA 2 0.428097 1.055887 0.098825 11.00000 -1.50000 HB 2 0.423902 1.136219 0.155778 11.00000 -1.50000 AFIX 0 C01M 1 -0.099022 0.533585 0.162348 11.00000 0.03956 0.08718 = 0.04226 0.01898 0.00146 0.03276 AFIX 43 H01 2 -0.104539 0.560532 0.127317 11.00000 -1.20000 AFIX 0 C01N 1 -0.177126 0.522900 0.197789 11.00000 0.03506 0.10190 = 0.06022 0.01477 0.00138 0.03737 AFIX 43 H1 2 -0.235839 0.540955 0.185954 11.00000 -1.20000 AFIX 0 C01O 1 0.287372 0.795555 0.011940 11.00000 0.07735 0.05207 = 0.08066 0.02602 0.01393 0.03948 AFIX 137 H2 2 0.268767 0.761070 -0.030713 11.00000 -1.50000 HC 2 0.308348 0.873693 0.016859 11.00000 -1.50000 HD 2 0.224578 0.764532 0.030126 11.00000 -1.50000 AFIX 0 C01P 1 -0.169511 0.486746 0.249195 11.00000 0.03294 0.07894 = 0.05664 0.00849 0.01248 0.02573 AFIX 43 H3 2 -0.222727 0.481151 0.272766 11.00000 -1.20000 AFIX 0 C01Q 1 -0.022134 0.246314 0.219973 11.00000 0.03011 0.03819 = 0.05627 0.00231 0.00292 0.00462 AFIX 137 H4 2 -0.063934 0.214192 0.248821 11.00000 -1.50000 HE 2 -0.002437 0.192674 0.196985 11.00000 -1.50000 HF 2 -0.065859 0.268826 0.192767 11.00000 -1.50000 AFIX 0 C01R 1 -0.186260 0.335080 0.335566 11.00000 0.04447 0.06232 = 0.06506 0.01517 0.02131 0.01139 AFIX 137 H5 2 -0.237875 0.368370 0.338283 11.00000 -1.50000 HG 2 -0.175527 0.309215 0.371932 11.00000 -1.50000 HH 2 -0.214631 0.273870 0.300813 11.00000 -1.50000 AFIX 0 C01S 1 0.452987 0.870429 0.399676 11.00000 0.05789 0.04607 = 0.06153 0.02524 0.00844 0.01647 AFIX 137 H6 2 0.438288 0.921410 0.428235 11.00000 -1.50000 HI 2 0.462511 0.815340 0.419149 11.00000 -1.50000 HJ 2 0.392092 0.835238 0.365461 11.00000 -1.50000 AFIX 0 C01T 1 0.079974 0.593471 0.096405 11.00000 0.05284 0.08958 = 0.05007 0.03187 0.01266 0.01836 AFIX 137 H7 2 0.012048 0.567724 0.067248 11.00000 -1.50000 HK 2 0.139367 0.600226 0.075326 11.00000 -1.50000 HL 2 0.094300 0.664317 0.121187 11.00000 -1.50000 AFIX 0 C01U 1 0.654618 0.991685 0.431859 11.00000 0.04852 0.06413 = 0.06120 0.01845 -0.00455 0.01858 AFIX 137 H8 2 0.717187 1.040369 0.418678 11.00000 -1.50000 HM 2 0.673132 0.937923 0.448244 11.00000 -1.50000 HN 2 0.634516 1.033868 0.462730 11.00000 -1.50000 AFIX 0 C01V 1 0.043922 0.398788 0.097223 11.00000 0.06061 0.08424 = 0.05605 0.01133 0.03231 0.03089 AFIX 137 H9 2 0.044542 0.348386 0.122762 11.00000 -1.50000 HO 2 0.098068 0.404887 0.072318 11.00000 -1.50000 HP 2 -0.027893 0.371655 0.071571 11.00000 -1.50000 AFIX 0 C01W 1 -0.034767 0.521281 0.381406 11.00000 0.04529 0.08572 = 0.04388 0.01255 0.01323 0.01044 AFIX 137 H10 2 0.038330 0.571073 0.379678 11.00000 -1.50000 HQ 2 -0.033279 0.498064 0.419299 11.00000 -1.50000 HR 2 -0.083316 0.558219 0.378547 11.00000 -1.50000 AFIX 0 C01X 1 0.226002 0.958325 0.352019 11.00000 0.05608 0.07661 = 0.06873 0.01698 0.02310 0.04081 C01Y 1 0.628239 1.147987 0.166094 11.00000 0.07282 0.12055 = 0.04432 0.02461 0.02325 0.03209 AFIX 137 H11 2 0.637084 1.219477 0.187445 11.00000 -1.50000 HS 2 0.621634 1.145645 0.123202 11.00000 -1.50000 HT 2 0.691368 1.134737 0.180662 11.00000 -1.50000 AFIX 0 C01Z 1 0.191811 1.014170 0.245527 11.00000 0.07324 0.05803 = 0.07347 0.01259 0.02180 0.04835 C020 1 0.015470 0.849138 0.254862 11.00000 0.06194 0.07894 = 0.08369 0.02962 0.02188 0.05382 C021 1 0.239134 0.488755 0.506916 11.00000 0.09701 0.08016 = 0.08833 0.04674 0.06044 0.04009 AFIX 137 H02A 2 0.255339 0.426510 0.492710 11.00000 -1.50000 H02B 2 0.163449 0.463040 0.511160 11.00000 -1.50000 H02C 2 0.286489 0.530237 0.545712 11.00000 -1.50000 AFIX 0 C022 1 0.561691 0.472828 0.313331 11.00000 0.11788 0.07715 = 0.08828 0.04610 0.06976 0.07430 AFIX 137 H02D 2 0.628382 0.495205 0.342979 11.00000 -1.50000 H02E 2 0.574925 0.454307 0.273238 11.00000 -1.50000 H02F 2 0.504946 0.409397 0.321331 11.00000 -1.50000 AFIX 0 C023 1 0.485678 0.830912 0.017711 11.00000 0.05712 0.05009 = 0.10702 0.03863 0.02458 0.01598 AFIX 137 H02G 2 0.546102 0.820041 0.038728 11.00000 -1.50000 H02H 2 0.503885 0.908720 0.023590 11.00000 -1.50000 H02I 2 0.471920 0.798894 -0.025050 11.00000 -1.50000 AFIX 0 PART 1 C029 1 -0.088306 0.848108 0.407578 21.00000 0.10147 0.13838 = 0.11075 0.02641 0.01215 0.04658 AFIX 137 H02J 2 -0.151965 0.864882 0.403509 21.00000 -1.50000 H02K 2 -0.103959 0.780417 0.379092 21.00000 -1.50000 H02L 2 -0.026999 0.907159 0.399377 21.00000 -1.50000 AFIX 66 C3 1 0.939682 0.877052 0.050782 31.00000 0.06475 0.06875 = 0.12768 0.03054 0.02052 0.01236 C1 1 0.897327 0.861973 -0.010679 31.00000 0.07269 0.03503 = 0.12977 0.02149 0.00644 -0.00930 AFIX 43 H1A 2 0.921079 0.825016 -0.040220 31.00000 -1.20000 AFIX 65 C027 1 0.819473 0.902129 -0.027988 31.00000 0.08541 0.08000 = 0.15463 0.03309 0.00122 0.01397 AFIX 43 H027 2 0.791136 0.892039 -0.069110 31.00000 -1.20000 AFIX 65 C7 1 0.783972 0.957365 0.016164 31.00000 0.09070 0.07893 = 0.17306 0.05462 0.02477 0.02379 AFIX 43 H7A 2 0.731883 0.984232 0.004582 31.00000 -1.20000 AFIX 65 C02A 1 0.826326 0.972445 0.077625 31.00000 0.07343 0.09218 = 0.16700 0.05675 0.04102 0.02687 AFIX 43 H02M 2 0.802573 1.009402 0.107165 31.00000 -1.20000 AFIX 65 C026 1 0.904180 0.932290 0.094935 31.00000 0.06583 0.07600 = 0.13753 0.03686 0.03214 0.01550 AFIX 43 H026 2 0.932517 0.942380 0.136056 31.00000 -1.20000 AFIX 0 C6 1 1.025659 0.837493 0.072177 31.00000 0.13036 0.16627 = 0.14519 0.05556 0.03837 0.09297 AFIX 137 H6A 2 0.990079 0.764308 0.078870 31.00000 -1.50000 H6B 2 1.072503 0.886693 0.109579 31.00000 -1.50000 H6C 2 1.069304 0.836212 0.041747 31.00000 -1.50000 AFIX 66 C2 1 -0.059665 0.835168 0.472403 21.00000 0.05521 0.04566 = 0.10827 0.01068 0.01571 0.00585 C025 1 -0.112757 0.867329 0.515744 21.00000 0.04591 0.04991 = 0.11777 0.01489 0.01944 0.00516 AFIX 43 H025 2 -0.165254 0.893971 0.504623 21.00000 -1.20000 AFIX 65 C028 1 -0.087385 0.859669 0.575706 21.00000 0.06330 0.06016 = 0.11772 0.01994 0.02774 0.01803 AFIX 43 H028 2 -0.122907 0.881187 0.604703 21.00000 -1.20000 AFIX 65 C0AA 1 -0.008922 0.819850 0.592328 21.00000 0.06736 0.06134 = 0.10680 0.01474 0.02415 0.02039 AFIX 43 H0AA 2 0.008053 0.814725 0.632447 21.00000 -1.20000 AFIX 65 C1AA 1 0.044169 0.787689 0.548988 21.00000 0.08655 0.08968 = 0.10819 0.01876 0.02717 0.04463 AFIX 43 H1AA 2 0.096666 0.761046 0.560110 21.00000 -1.20000 AFIX 65 C024 1 0.018799 0.795347 0.489026 21.00000 0.07038 0.04567 = 0.10546 0.00841 0.02309 0.01764 AFIX 43 H024 2 0.054322 0.773829 0.460029 21.00000 -1.20000 AFIX 0 PART 2 C0 1 -0.023981 0.864502 0.609404 -21.00000 0.12424 0.12299 = 0.12606 0.01667 0.03092 0.03579 AFIX 137 H0A 2 -0.071286 0.799788 0.621240 -21.00000 -1.50000 H0B 2 -0.042887 0.925049 0.623265 -21.00000 -1.50000 H0C 2 0.051510 0.883229 0.627330 -21.00000 -1.50000 AFIX 66 C2A 1 -0.038972 0.840980 0.538936 -21.00000 0.04914 0.07588 = 0.12558 0.00741 0.02209 -0.01844 C4 1 0.029346 0.805889 0.508148 -21.00000 0.10423 0.18859 = 0.13023 0.02939 0.03426 0.06369 AFIX 43 H4A 2 0.080613 0.786462 0.529230 -21.00000 -1.20000 AFIX 65 C8 1 0.021040 0.799834 0.445851 -21.00000 0.10946 0.14584 = 0.12929 0.02195 0.03414 0.05435 AFIX 43 H8A 2 0.066750 0.776356 0.425252 -21.00000 -1.20000 AFIX 65 C0AB 1 -0.055584 0.828870 0.414342 -21.00000 0.07127 0.07753 = 0.11847 0.00158 0.02340 0.00490 AFIX 43 H0AB 2 -0.061141 0.824818 0.372661 -21.00000 -1.20000 AFIX 65 C1AB 1 -0.123902 0.863961 0.445129 -21.00000 0.06713 0.06553 = 0.12223 0.00117 0.02545 -0.00350 AFIX 43 H1AB 2 -0.175169 0.883388 0.424047 -21.00000 -1.20000 AFIX 65 C5 1 -0.115598 0.870017 0.507426 -21.00000 0.05638 0.08819 = 0.12355 0.00659 0.02754 -0.00552 AFIX 43 H5A 2 -0.161308 0.893495 0.528025 -21.00000 -1.20000 AFIX 0 PART 0 HU 2 0.344943 0.660739 0.249349 11.00000 0.00530 PART 2 C9 1 0.853356 0.905193 0.004278 -31.00000 0.04587 0.04246 = 0.07116 0.01767 0.00763 -0.00303 AFIX 43 H9A 2 0.811174 0.916740 -0.027492 -31.00000 -1.20000 AFIX 0 C3A 1 0.859055 0.947279 0.060205 -31.00000 0.04914 0.05610 = 0.07197 0.01831 0.00781 0.01158 C1A 1 0.936650 0.935175 0.108745 -31.00000 0.06479 0.06998 = 0.06927 0.00805 0.00271 0.02781 AFIX 43 H1AC 2 0.953167 0.976387 0.148464 -31.00000 -1.20000 AFIX 0 C6A 1 0.789875 1.013908 0.081594 -31.00000 0.08871 0.10886 = 0.09085 0.02142 0.01293 0.05790 AFIX 137 H6AA 2 0.769849 1.044748 0.049062 -31.00000 -1.50000 H6AB 2 0.833592 1.072482 0.116484 -31.00000 -1.50000 H6AC 2 0.724237 0.964894 0.092207 -31.00000 -1.50000 AFIX 0 C10 1 0.982501 0.863467 0.094102 -31.00000 0.07613 0.07658 = 0.06636 0.00947 0.00410 0.03669 AFIX 43 H10A 2 1.014899 0.839936 0.124515 -31.00000 -1.20000 AFIX 0 C02B 1 0.922011 0.831889 -0.008496 -31.00000 0.06843 0.06011 = 0.06697 0.00984 0.00460 0.01620 AFIX 43 H02N 2 0.915642 0.795101 -0.048078 -31.00000 -1.20000 AFIX 0 C7A 1 0.980932 0.824633 0.032593 -31.00000 0.06359 0.04184 = 0.06653 0.00693 0.00422 0.00818 AFIX 43 H7AA 2 1.028456 0.791570 0.023612 -31.00000 -1.20000 AFIX 0 HKLF 4 REM mrc2111_a.res in P-1 REM wR2 = 0.3168, GooF = S = 1.116, Restrained GooF = 1.111 for all data REM R1 = 0.0980 for 10076 Fo > 4sig(Fo) and 0.1270 for all 14369 data REM 922 parameters refined using 180 restraints END WGHT 0.1080 19.3361 REM Highest difference peak 1.167, deepest hole -0.599, 1-sigma level 0.116 Q1 1 0.1131 0.8378 0.2238 11.00000 0.05 1.17 Q2 1 1.0470 0.7761 0.1519 11.00000 0.05 0.62 Q3 1 0.2604 0.5951 0.3386 11.00000 0.05 0.54 Q4 1 0.0157 0.7784 0.5899 11.00000 0.05 0.51 Q5 1 0.7774 0.9696 -0.0450 11.00000 0.05 0.43 Q6 1 0.2243 0.6126 0.4516 11.00000 0.05 0.41 Q7 1 -0.0281 0.3465 0.0167 11.00000 0.05 0.40 Q8 1 0.0931 0.2420 0.3141 11.00000 0.05 0.40 Q9 1 0.1827 0.3451 0.3236 11.00000 0.05 0.39 Q10 1 0.4128 0.9093 0.4471 11.00000 0.05 0.39 Q11 1 0.1854 1.0724 0.2639 11.00000 0.05 0.38 Q12 1 0.1546 0.5019 0.4837 11.00000 0.05 0.38 Q13 1 1.0638 0.6997 0.0197 11.00000 0.05 0.38 Q14 1 0.2565 0.6402 0.5423 11.00000 0.05 0.37 Q15 1 0.3043 0.6196 0.4181 11.00000 0.05 0.37 Q16 1 0.4338 0.4864 0.1834 11.00000 0.05 0.37 Q17 1 0.6613 0.8420 0.3516 11.00000 0.05 0.37 Q18 1 0.2644 1.0974 0.1711 11.00000 0.05 0.36 Q19 1 1.0520 0.7189 0.0523 11.00000 0.05 0.36 Q20 1 0.3498 0.7777 -0.0625 11.00000 0.05 0.36 ; _shelx_res_checksum 69591 _shelx_hkl_file ; 0 0 3 661.56 7.91 0 0 -3 680.31 8.44 0 0 4 3404.12 20.48 0 0 -4 1166.69 13.00 0 0 4 1022.70 11.87 0 0 -4 3441.95 21.82 0 0 -5 236.92 6.74 0 0 5 244.81 6.46 0 0 -5 240.59 6.78 0 0 5 273.10 7.17 0 0 6 160.80 5.63 0 0 6 160.85 6.31 0 0 -6 156.38 6.03 0 0 -6 155.60 6.02 0 0 7 216.72 6.97 0 0 -7 227.99 7.63 0 0 7 203.20 7.52 0 0 -7 220.81 7.71 0 0 8 1405.66 19.70 0 0 8 1436.89 18.56 0 0 -8 1484.09 20.57 0 0 -8 1469.99 19.45 0 0 9 281.26 8.94 0 0 9 288.32 9.86 0 0 -9 271.17 9.26 0 0 -9 283.83 9.56 0 0 10 21.28 4.05 0 0 10 15.73 3.06 0 0 -10 16.16 3.56 0 0 -10 17.67 3.25 0 0 11 103.98 7.05 0 0 11 108.99 6.50 0 0 -11 104.36 6.48 0 0 -11 96.07 6.23 0 0 -12 120.68 7.14 0 0 12 121.32 6.96 0 0 12 121.42 7.70 0 0 -12 112.24 7.13 0 0 13 44.88 4.81 0 0 -13 44.10 5.02 0 0 13 42.15 5.34 0 0 -14 5.48 3.25 0 0 14 3.16 3.54 0 0 14 4.80 2.58 0 0 -15 4.66 3.36 0 0 15 4.52 3.82 0 0 16 113.00 9.20 0 0 -16 124.14 8.69 0 0 -17 239.76 11.95 0 0 -18 38.49 5.46 0 0 -19 23.92 5.03 0 0 -20 -5.07 4.85 0 0 -21 150.79 10.94 0 0 -22 20.72 5.22 0 0 -23 -2.77 4.44 0 0 -24 28.57 6.41 0 0 -25 2.28 4.59 0 0 -26 14.67 6.15 0 0 -27 6.48 4.95 0 0 -28 1.97 4.50 0 1 -29 1.30 4.98 0 1 -28 2.26 4.77 0 1 -27 13.12 6.11 0 1 -26 9.50 5.61 0 1 -25 41.32 7.55 0 1 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137.07 5.89 0 6 1 1154.68 19.00 0 -6 -1 1144.29 18.65 0 -6 -1 1174.57 17.75 0 6 1 1202.42 17.71 0 6 2 223.64 8.44 0 -6 -2 245.50 8.98 0 6 2 245.90 8.91 0 -6 -2 246.89 8.85 0 6 3 31.43 4.17 0 -6 -3 32.21 4.25 0 -6 -3 37.44 4.14 0 6 3 46.58 4.27 0 -6 -4 24.21 3.72 0 6 4 30.32 3.80 0 6 4 24.66 3.98 0 6 4 32.52 3.70 0 -6 -4 27.19 3.70 0 -6 -5 11.23 2.77 0 -6 -5 11.47 3.07 0 6 5 14.41 2.93 0 6 5 12.04 3.66 0 6 6 567.07 15.88 0 -6 -6 589.28 16.08 0 6 6 525.16 13.49 0 -6 -6 530.39 13.31 0 6 7 1.72 2.18 0 -6 -7 -1.31 2.76 0 6 7 -0.21 3.47 0 6 8 101.61 7.92 0 6 8 88.61 6.17 0 -6 -8 99.95 6.19 0 6 9 16.45 5.11 0 6 9 12.87 2.93 0 -6 -9 17.13 3.42 0 -6 -10 5.31 2.65 0 6 10 10.35 4.65 0 6 10 2.88 2.55 0 6 11 15.99 5.87 0 -6 -11 11.72 3.67 0 6 12 321.61 14.95 0 -6 -12 313.61 11.90 0 -6 -13 385.92 13.48 0 6 13 400.19 16.86 0 -6 -14 11.45 3.98 0 6 14 26.36 7.34 0 -6 -15 17.23 4.11 0 6 15 20.51 6.65 0 -6 -16 9.72 3.84 0 6 16 10.46 5.42 0 6 17 36.66 7.52 0 -6 -17 32.02 5.12 0 6 18 36.77 8.03 0 -6 -18 25.68 4.78 0 6 19 76.00 9.97 0 6 20 2.41 5.74 0 6 21 12.92 6.79 0 7 -26 -3.67 5.30 0 7 -25 20.00 6.57 0 7 -24 39.30 7.99 0 7 -23 6.33 5.33 0 7 -22 -3.53 4.77 0 7 -21 25.14 6.21 0 7 -20 23.82 5.97 0 7 -19 3.39 5.00 0 7 -18 43.10 4.88 0 7 -18 51.27 7.56 0 7 -17 126.46 7.65 0 7 -17 134.02 10.64 0 7 -16 0.62 2.46 0 7 -16 -1.75 4.70 0 7 -15 148.93 7.34 0 7 -15 150.53 11.33 0 7 -14 50.63 6.46 0 7 -14 53.29 4.43 0 7 -13 99.11 5.30 0 7 -13 89.46 8.11 0 7 -12 5.62 2.14 0 -7 11 -1.09 3.89 0 7 -11 2.10 1.76 0 -7 10 34.18 5.29 0 -7 9 9.64 3.57 0 -7 8 174.90 10.52 0 7 -7 36.67 2.45 0 -7 7 39.94 5.51 0 7 -6 534.26 8.68 0 -7 6 548.34 15.87 0 -7 5 18.28 4.05 0 7 -5 18.04 3.60 0 7 -5 14.37 2.14 0 -7 4 360.82 12.74 0 7 -4 371.74 12.75 0 7 -4 360.12 7.90 0 7 -3 217.59 6.60 0 -7 3 213.32 9.63 0 7 -3 221.59 9.72 0 7 -2 274.49 7.82 0 -7 2 269.53 10.57 0 7 -2 280.72 10.68 0 7 -1 95.45 6.59 0 -7 1 89.55 4.97 0 -7 1 91.04 6.40 0 7 -1 104.62 5.49 0 -7 0 128.64 7.33 0 7 0 128.07 7.35 0 -7 0 125.84 6.09 0 7 0 119.39 5.86 0 7 1 670.08 15.89 0 7 1 674.22 14.46 0 -7 -1 686.69 14.57 0 -7 -1 675.09 16.05 0 7 2 29.14 4.20 0 -7 -2 38.74 4.87 0 -7 -2 39.45 4.67 0 7 2 37.66 4.37 0 7 3 1471.55 23.53 0 -7 -3 1428.58 23.09 0 -7 -3 1517.35 23.77 0 7 3 1440.08 22.97 0 -7 -4 76.07 5.98 0 7 4 70.60 5.38 0 7 4 72.37 5.79 0 7 4 71.14 6.45 0 -7 -4 74.07 6.27 0 -7 -5 667.15 17.49 0 7 5 647.80 17.48 0 -7 -5 624.84 15.51 0 7 5 612.90 15.55 0 7 6 130.74 8.19 0 -7 -6 110.97 7.41 0 7 6 118.90 9.09 0 7 7 1436.43 27.52 0 7 7 1381.07 23.97 0 -7 -7 1462.74 24.03 0 7 8 151.81 8.67 0 -7 -8 151.16 8.51 0 7 8 156.80 10.81 0 7 9 115.71 9.06 0 -7 -9 121.37 7.52 0 -7 -10 160.30 8.84 0 7 10 160.51 10.73 0 7 11 91.32 9.14 0 -7 -11 78.94 6.51 0 -7 -12 74.49 6.53 0 7 12 86.24 8.91 0 7 13 118.47 10.39 0 -7 -13 113.05 7.91 0 -7 -14 37.22 5.21 0 7 14 46.77 8.08 0 -7 -15 5.38 3.40 0 7 15 1.90 5.05 0 -7 -16 148.06 9.46 0 7 16 168.37 12.77 0 7 17 58.23 9.23 0 7 18 14.25 6.71 0 7 19 2.33 5.50 0 7 20 1.08 5.75 0 8 -25 0.30 5.22 0 8 -24 -5.60 6.19 0 8 -23 5.96 5.59 0 8 -22 -1.50 5.18 0 8 -21 21.09 6.39 0 8 -20 1.00 4.89 0 8 -19 167.29 12.75 0 8 -18 11.38 4.93 0 8 -17 201.87 13.24 0 8 -16 145.71 11.29 0 8 -16 142.00 7.12 0 8 -15 91.38 5.50 0 8 -15 86.00 8.77 0 8 -14 3.06 2.19 0 8 -14 -0.41 3.90 0 8 -13 5.02 2.08 0 8 -12 106.94 4.68 0 -8 12 114.85 9.33 0 -8 11 -3.59 4.29 0 8 -11 3.64 1.57 0 -8 10 6.00 3.48 0 -8 9 55.00 6.50 0 8 -9 49.50 3.03 0 8 -8 19.31 2.06 0 -8 8 18.72 4.35 0 -8 7 45.69 5.99 0 8 -7 42.58 2.86 0 8 -6 137.49 4.90 0 -8 6 127.40 8.42 0 8 -5 0.43 1.51 0 -8 5 5.01 3.38 0 8 -4 9.67 2.06 0 -8 4 15.97 3.95 0 8 -3 28.18 2.98 0 -8 3 39.38 5.24 0 -8 2 47.84 5.24 0 8 -2 49.10 3.97 0 -8 1 102.84 7.39 0 8 -1 101.37 5.63 0 -8 1 103.48 5.85 0 8 0 13.96 3.32 0 -8 0 13.50 2.64 0 8 0 6.65 2.64 0 -8 0 15.46 3.70 0 8 1 125.70 7.24 0 -8 -1 115.52 7.20 0 8 1 118.95 8.09 0 -8 -1 123.00 8.35 0 -8 -2 308.60 11.12 0 8 2 300.18 11.52 0 -8 -2 303.80 11.82 0 8 2 291.39 11.06 0 8 3 16.71 4.31 0 -8 -3 20.03 4.25 0 -8 -3 24.46 4.35 0 8 3 30.01 4.48 0 8 4 1.08 2.35 0 8 4 0.47 3.16 0 -8 -4 -3.48 3.38 0 -8 -5 11.42 3.08 0 8 5 10.30 4.21 0 8 6 201.14 10.87 0 -8 -6 202.68 9.75 0 8 7 82.63 7.84 0 -8 -7 80.18 6.51 0 8 8 11.95 5.04 0 -8 -8 8.25 3.15 0 -8 -9 -0.31 2.87 0 8 9 2.69 4.18 0 -8 -10 13.62 4.04 0 8 10 12.67 5.86 0 8 11 14.45 5.87 0 -8 -11 9.52 3.61 0 8 12 16.62 6.09 0 -8 -12 14.64 4.05 0 -8 -13 159.91 9.72 0 8 13 161.83 12.15 0 8 14 164.73 12.32 0 -8 -14 158.18 9.93 0 8 15 6.56 5.73 0 -8 -15 4.01 3.85 0 8 16 62.99 9.33 0 8 17 6.40 5.86 0 8 18 75.44 10.19 0 8 19 20.22 7.63 0 9 -24 3.46 5.03 0 9 -23 2.54 5.00 0 9 -22 32.94 7.09 0 9 -21 3.97 5.31 0 9 -20 35.89 7.08 0 9 -19 28.10 6.31 0 9 -18 78.37 9.13 0 9 -17 3.05 4.60 0 9 -16 33.93 6.37 0 9 -15 13.79 5.03 0 9 -13 91.35 4.39 0 -9 13 95.49 9.19 0 9 -12 59.40 3.42 0 -9 12 64.33 7.58 0 9 -11 6.93 1.60 0 -9 11 19.62 5.35 0 9 -10 49.79 2.97 0 -9 10 65.39 7.38 0 9 -9 103.32 4.04 0 -9 9 117.55 9.61 0 -9 8 134.74 9.83 0 9 -8 104.15 4.16 0 9 -7 34.71 2.75 0 -9 7 46.67 6.58 0 9 -6 716.80 11.45 0 -9 6 730.14 20.45 0 9 -5 11.66 2.49 0 -9 5 25.40 5.61 0 -9 4 793.92 20.62 0 9 -4 806.88 13.70 0 -9 3 71.61 7.02 0 9 -3 53.54 4.11 0 -9 2 184.70 9.98 0 9 -2 173.38 7.26 0 -9 1 76.16 7.11 0 9 -1 67.72 5.37 0 9 0 183.93 8.51 0 -9 0 183.95 8.32 0 -9 0 186.92 9.94 0 -9 -1 158.37 8.39 0 9 1 160.88 8.43 0 -9 -1 163.60 9.20 0 -9 -2 8.21 4.06 0 -9 -2 5.47 2.97 0 9 2 -0.37 3.14 0 -9 -3 312.24 12.84 0 9 3 300.28 12.49 0 9 4 372.28 14.32 0 -9 -4 367.03 13.49 0 -9 -5 24.13 4.36 0 9 5 27.00 5.40 0 -9 -6 25.71 5.10 0 9 6 25.91 6.42 0 -9 -7 140.42 8.88 0 9 7 139.82 10.27 0 9 8 66.25 7.95 0 -9 -8 65.80 6.60 0 9 9 120.62 9.98 0 -9 -9 107.16 7.87 0 -9 -10 -0.32 2.92 0 9 10 5.09 5.58 0 -9 -11 2.47 3.08 0 9 11 8.86 5.87 0 9 12 12.15 5.71 0 -9 -12 3.54 3.09 0 9 13 56.05 8.50 0 -9 -13 36.24 5.22 0 9 14 7.55 6.20 0 9 15 31.39 7.72 0 9 16 5.45 6.17 0 9 17 22.01 7.43 0 10 -23 40.32 8.33 0 10 -22 39.13 8.58 0 10 -21 80.99 10.31 0 10 -20 10.10 5.71 0 10 -19 53.35 8.23 0 10 -18 43.52 7.88 0 10 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32.65 6.90 0 11 10 121.44 11.02 0 11 11 39.26 8.11 0 11 12 103.50 11.01 0 11 13 18.15 7.06 0 11 14 15.97 6.90 0 11 15 27.98 8.03 0 12 -20 -1.52 5.48 0 12 -19 56.05 9.11 0 12 -18 0.95 5.23 0 12 -17 9.03 5.24 0 12 -16 8.21 5.19 0 -12 14 67.67 9.23 0 -12 13 -4.36 4.81 0 -12 12 36.36 6.94 0 -12 11 3.14 4.85 0 -12 10 31.81 6.42 0 -12 9 29.84 6.69 0 -12 8 132.52 11.35 0 -12 7 61.23 8.54 0 -12 6 102.87 9.88 0 -12 5 1.99 3.84 0 -12 4 47.91 7.06 0 12 -3 96.83 6.73 0 -12 3 84.78 8.76 0 12 -2 198.50 9.81 0 -12 2 200.05 12.55 0 -12 1 88.26 9.08 0 12 -1 89.05 7.29 0 12 0 301.57 12.59 0 -12 0 282.57 14.81 0 12 1 22.99 5.47 0 -12 -1 13.78 5.33 0 -12 -2 67.29 7.88 0 12 2 77.64 7.86 0 -12 -3 20.42 5.25 0 12 3 42.51 6.57 0 -12 -4 20.66 5.22 0 12 4 36.12 6.48 0 12 5 34.55 6.53 0 -12 -5 17.30 4.82 0 -12 -6 65.65 7.54 0 12 6 77.27 8.43 0 12 7 20.64 6.04 0 -12 -7 10.85 4.59 0 12 8 19.24 5.97 0 12 9 6.60 5.44 0 12 10 0.68 5.17 0 12 11 9.94 5.95 0 12 12 7.80 6.48 0 12 13 7.28 6.38 0 13 -17 8.51 5.19 0 13 -16 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6.30 1 -14 10 2.24 4.80 1 -14 11 6.26 4.79 1 -14 12 18.99 6.81 1 -14 13 18.30 6.87 1 -14 14 5.92 5.77 1 -14 15 0.50 5.16 -1 13 11 32.37 7.54 -1 13 10 8.96 5.75 -1 13 9 15.51 6.20 1 -13 -8 5.78 4.44 -1 13 8 7.53 5.52 1 -13 -7 -2.02 4.26 -1 13 7 4.27 4.79 1 -13 -6 1.79 3.92 -1 13 6 6.90 4.86 -1 13 5 24.81 5.71 1 -13 -5 22.40 5.49 1 -13 -4 9.22 4.76 -1 13 4 14.10 5.02 -1 13 3 74.70 7.40 1 -13 -3 54.18 7.43 1 -13 -2 17.65 5.26 1 -13 -1 62.89 7.97 1 -13 0 34.47 6.47 1 -13 1 44.64 7.19 1 -13 2 53.59 7.84 1 -13 3 52.63 7.91 1 -13 4 23.93 6.25 1 -13 5 278.35 15.84 1 -13 6 5.90 4.63 1 -13 7 15.17 5.61 1 -13 8 8.77 5.19 1 -13 9 7.35 5.14 1 -13 10 44.27 7.91 1 -13 11 2.33 4.95 1 -13 12 215.57 14.93 1 -13 13 4.95 4.78 1 -13 14 36.86 7.68 1 -13 15 -0.42 5.27 -1 13 -18 3.28 4.79 -1 12 13 3.71 5.94 -1 12 12 8.66 6.08 -1 12 11 6.27 5.55 -1 12 10 20.01 6.12 1 -12 -10 13.26 4.43 -1 12 9 9.27 5.30 1 -12 -9 7.56 3.85 -1 12 8 42.12 7.17 1 -12 -8 44.07 6.65 -1 12 7 5.11 4.96 1 -12 -7 2.13 4.31 -1 12 6 27.60 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167.92 9.73 2 -9 4 31.31 4.94 2 -9 5 169.66 10.15 2 -9 6 992.57 23.97 2 -9 7 216.86 11.86 2 -9 8 539.36 18.55 2 -9 9 424.18 16.80 2 -9 10 381.50 16.00 2 -9 11 71.13 7.52 2 -9 12 58.04 8.14 2 -9 13 3.99 3.99 -2 9 -14 0.51 1.03 2 -9 14 78.91 9.56 2 -9 15 157.32 11.78 -2 9 -17 -0.76 4.41 -2 9 -18 3.64 4.38 -2 9 -19 25.54 6.39 -2 9 -20 44.55 8.20 -2 9 -21 45.22 7.70 -2 9 -22 67.81 9.44 -2 9 -23 21.10 6.42 -2 9 -24 84.13 10.34 -2 9 -25 -0.62 5.24 2 -8 -19 0.96 4.04 2 -8 -18 10.41 4.69 2 -8 -17 51.16 7.16 2 -8 -16 36.96 6.20 2 -8 -15 1.50 3.59 2 -8 -14 19.91 4.95 2 -8 -13 27.13 5.18 -2 8 13 37.14 7.36 -2 8 12 67.61 8.13 2 -8 -12 62.31 6.91 2 -8 -11 12.58 4.33 -2 8 11 14.82 6.20 2 -8 -10 -0.08 3.24 -2 8 10 11.02 5.32 2 -8 -9 607.52 18.21 -2 8 9 624.87 19.20 -2 8 8 414.18 15.06 2 -8 -8 413.17 15.04 2 -8 -7 10.40 4.39 -2 8 7 12.71 4.60 -2 8 6 192.57 9.83 2 -8 -6 185.36 9.95 2 -8 -5 115.88 7.74 2 -8 -5 123.43 8.87 -2 8 5 124.36 7.96 2 -8 -4 36.98 5.49 2 -8 -4 31.47 4.69 -2 8 4 44.97 5.44 -2 8 3 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22.83 -2 -3 -7 268.04 13.11 2 3 7 240.04 12.28 2 3 8 24.35 5.28 2 3 8 15.33 2.87 -2 -3 -9 19.54 2.57 2 3 9 13.06 2.42 2 3 10 14.64 3.99 2 3 10 20.88 3.07 -2 -3 -10 25.36 2.95 -2 -3 -10 19.89 2.85 2 3 11 4.69 2.26 2 3 11 0.48 4.51 -2 -3 -11 4.87 2.22 -2 -3 -12 174.58 7.61 2 3 12 170.94 7.52 2 3 12 178.93 11.04 -2 -3 -13 50.53 4.79 2 3 13 47.26 7.14 2 3 13 43.19 4.47 -2 -3 -14 333.69 11.29 2 3 14 319.46 15.67 -2 -3 -15 11.80 3.67 2 3 15 13.04 3.30 2 3 15 22.10 6.39 2 3 16 9.48 5.46 2 3 16 2.58 2.66 -2 -3 -16 4.45 3.07 -2 -3 -17 28.15 4.41 2 3 17 31.96 7.08 2 3 18 13.88 6.63 -2 -3 -18 -0.45 2.97 2 3 19 26.55 7.00 -2 -3 -19 14.65 4.10 -2 -3 -20 -0.41 3.14 2 3 20 8.91 6.43 2 3 21 0.98 5.03 2 3 22 4.32 6.08 2 3 23 10.10 6.36 2 4 -27 9.32 6.34 2 4 -26 1.06 4.91 2 4 -25 -1.00 5.24 2 4 -24 1.36 4.91 2 4 -23 25.45 6.91 2 4 -22 37.07 7.31 2 4 -21 3.00 4.42 2 4 -20 21.80 5.82 2 4 -19 5.88 4.52 2 4 -18 45.78 6.79 2 4 -17 24.96 5.56 2 4 -16 181.21 11.46 2 4 -15 353.30 12.47 2 4 -15 358.93 15.35 2 4 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37.82 6.05 -2 -4 -6 28.90 2.79 2 4 6 40.50 3.56 -2 -4 -7 89.85 4.22 2 4 7 82.39 6.40 2 4 7 88.49 4.65 -2 -4 -8 66.69 3.85 2 4 8 62.87 4.27 2 4 9 0.30 1.85 -2 -4 -9 0.03 1.77 2 4 10 44.41 3.98 2 4 10 40.44 5.91 -2 -4 -10 50.36 3.85 -2 -4 -11 97.29 5.25 2 4 11 92.82 5.69 2 4 11 89.09 8.18 2 4 12 -0.87 4.18 2 4 12 0.06 2.19 -2 -4 -12 1.18 1.99 2 4 13 27.59 6.15 -2 -4 -13 29.91 3.75 2 4 13 26.82 3.82 2 4 14 1.96 2.24 -2 -4 -14 1.39 2.26 2 4 14 1.41 5.08 -2 -4 -15 156.85 8.67 -2 -4 -15 166.07 7.86 2 4 15 165.95 12.14 2 4 15 156.86 8.38 2 4 16 12.79 5.90 -2 -4 -16 6.43 3.32 -2 -4 -16 4.80 2.69 -2 -4 -17 38.86 4.65 2 4 17 48.55 8.64 -2 -4 -17 38.58 5.18 -2 -4 -18 51.39 6.03 2 4 18 65.20 9.24 2 4 19 36.62 7.90 2 4 20 36.49 7.92 2 4 21 9.36 6.40 2 4 22 42.96 8.85 2 5 -27 5.65 5.19 2 5 -26 4.28 5.77 2 5 -25 3.41 5.28 2 5 -24 -1.45 5.52 2 5 -23 6.87 5.47 2 5 -22 54.58 8.36 2 5 -21 23.01 6.33 2 5 -20 54.59 7.98 2 5 -19 81.52 10.60 2 5 -18 288.89 15.56 2 5 -17 12.01 5.01 2 5 -16 170.69 11.42 2 5 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-6 3.81 1.82 2 5 7 23.63 5.64 2 5 7 11.27 3.30 -2 -5 -7 18.16 3.03 2 5 8 129.32 6.29 2 5 8 119.21 8.23 -2 -5 -8 135.97 5.82 -2 -5 -9 62.36 4.48 2 5 9 51.04 4.80 2 5 9 62.85 7.53 2 5 10 73.54 5.32 -2 -5 -10 77.45 4.80 2 5 10 68.56 7.35 2 5 11 49.64 4.54 -2 -5 -11 56.30 4.38 2 5 11 50.69 6.92 -2 -5 -12 18.74 3.28 2 5 12 13.40 5.58 2 5 12 15.80 3.15 2 5 13 32.99 7.05 2 5 13 35.37 4.41 -2 -5 -13 33.87 3.77 -2 -5 -14 7.85 2.64 2 5 14 12.69 5.76 -2 -5 -15 1.90 2.39 2 5 15 2.77 5.39 2 5 16 12.16 7.25 2 5 17 44.16 8.06 2 5 18 77.65 10.29 2 5 19 22.89 6.91 2 5 20 3.22 6.07 2 5 21 11.89 6.57 2 6 -26 6.01 5.74 2 6 -25 -0.28 5.19 2 6 -24 39.05 8.11 2 6 -23 27.36 7.27 2 6 -22 140.73 12.15 2 6 -21 78.94 9.57 2 6 -20 4.39 4.81 2 6 -19 143.51 12.00 2 6 -18 30.34 6.32 2 6 -17 167.24 11.86 2 6 -16 17.33 3.96 2 6 -16 18.42 5.85 2 6 -15 52.92 8.20 2 6 -14 17.40 5.60 2 6 -13 19.31 5.00 2 6 -12 0.61 3.36 2 6 -11 18.05 4.70 2 6 -10 168.66 9.84 2 6 -7 1391.33 25.15 -2 -6 7 1400.73 25.40 -2 -6 6 366.36 12.76 2 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44.97 8.36 4 -15 -2 9.54 6.27 4 -15 -1 121.82 11.57 4 -15 0 10.49 6.07 4 -15 1 164.34 13.41 4 -15 2 18.56 6.73 4 -15 3 33.37 7.28 4 -15 4 3.26 4.53 4 -15 5 6.29 4.94 4 -15 6 1.31 4.89 4 -15 7 29.15 7.10 4 -15 8 3.44 4.65 4 -15 9 24.27 6.87 4 -15 10 107.53 11.85 4 -15 11 57.85 9.36 4 -15 12 6.66 5.86 4 -15 13 28.94 8.44 4 -14 -12 -1.31 4.85 4 -14 -11 -0.58 4.43 4 -14 -10 3.27 4.74 4 -14 -9 7.53 5.39 4 -14 -8 -4.67 5.17 4 -14 -7 23.45 6.13 4 -14 -6 4.02 4.44 4 -14 -5 16.14 5.63 4 -14 -4 21.14 6.26 4 -14 -3 89.43 10.25 4 -14 -2 26.55 6.68 4 -14 -1 53.76 8.18 4 -14 0 51.08 7.89 4 -14 1 24.24 6.50 4 -14 2 62.15 8.53 4 -14 3 23.01 6.41 4 -14 4 0.56 4.37 4 -14 5 104.54 10.89 4 -14 6 36.66 7.62 4 -14 7 64.03 9.22 4 -14 8 85.10 10.08 4 -14 9 17.03 6.16 4 -14 10 17.26 6.57 4 -14 11 32.80 7.31 4 -14 12 104.74 11.45 4 -14 13 12.17 6.72 4 -14 14 104.64 11.77 4 -14 15 9.08 5.81 4 -14 16 48.77 9.03 4 -13 -14 -0.63 4.43 4 -13 -13 3.25 4.63 4 -13 -12 1.61 4.54 4 -13 -11 26.06 6.50 4 -13 -10 171.14 13.34 4 -13 -9 9.10 5.60 4 -13 -8 158.14 12.68 4 -13 -7 8.80 4.68 4 -13 -6 22.50 6.04 4 -13 -5 8.61 4.89 4 -13 -4 58.49 8.00 4 -13 -3 2.70 4.15 4 -13 -2 119.23 10.67 4 -13 -1 154.60 12.17 4 -13 0 57.60 8.51 4 -13 1 80.76 9.60 4 -13 2 21.10 6.14 4 -13 3 84.48 9.27 4 -13 4 51.39 7.87 4 -13 5 22.07 5.76 4 -13 6 22.77 5.90 4 -13 7 16.12 5.60 4 -13 8 110.11 10.96 4 -13 9 5.86 4.97 4 -13 10 153.31 12.64 4 -13 11 -2.18 4.82 4 -13 12 6.09 4.53 4 -13 13 17.69 5.80 4 -13 14 15.66 5.81 4 -13 15 46.54 8.14 4 -13 16 0.25 4.76 4 -13 17 -1.13 5.13 4 -13 18 4.33 5.35 4 -13 19 31.12 7.82 4 -12 -16 3.15 5.05 4 -12 -15 2.77 4.74 4 -12 -14 2.89 4.83 4 -12 -13 33.68 6.67 4 -12 -12 -1.93 5.12 4 -12 -11 -3.96 4.90 4 -12 -10 0.64 4.22 4 -12 -9 160.69 12.06 4 -12 -8 43.32 7.20 4 -12 -7 29.62 6.44 4 -12 -6 139.25 11.18 4 -12 -5 176.49 12.36 4 -12 -4 129.65 10.65 4 -12 -3 237.72 14.16 4 -12 -2 26.40 6.04 4 -12 -1 6.42 4.29 4 -12 0 57.60 7.50 4 -12 1 102.53 9.53 4 -12 2 60.39 7.89 4 -12 3 152.73 11.58 4 -12 4 6.63 4.82 4 -12 5 153.47 11.52 4 -12 6 14.80 5.40 4 -12 7 83.21 9.44 4 -12 8 216.70 13.85 4 -12 9 316.43 16.17 4 -12 10 16.22 6.13 4 -12 11 329.91 17.05 4 -12 12 36.95 7.23 4 -12 13 227.80 14.84 4 -12 14 75.64 9.39 4 -12 15 91.13 10.07 4 -12 16 43.62 8.03 4 -12 17 0.10 4.49 4 -12 18 101.37 10.98 -4 12 -20 44.99 8.29 -4 12 -21 31.18 7.19 4 -11 -18 18.75 6.20 4 -11 -17 10.87 5.70 4 -11 -16 9.83 5.23 4 -11 -15 2.63 4.54 4 -11 -14 -4.95 5.07 4 -11 -13 6.14 4.26 4 -11 -12 -1.55 4.92 4 -11 -11 85.16 9.03 4 -11 -10 7.98 4.57 4 -11 -9 4.81 4.38 4 -11 -8 7.27 5.04 4 -11 -7 122.10 10.43 4 -11 -6 55.99 7.39 4 -11 -5 105.83 9.52 4 -11 -4 113.81 9.84 4 -11 -3 88.02 6.67 4 -11 -3 97.47 9.20 4 -11 -2 31.21 6.18 4 -11 -2 20.71 3.75 4 -11 -1 15.59 3.04 4 -11 -1 26.54 5.64 4 -11 0 20.38 2.74 4 -11 0 22.50 5.08 4 -11 1 92.21 9.02 4 -11 1 87.98 4.69 4 -11 2 6.22 4.25 4 -11 2 4.38 1.42 4 -11 3 147.26 10.69 4 -11 4 101.31 9.50 4 -11 5 48.06 7.05 4 -11 6 205.15 12.63 4 -11 7 45.27 7.03 4 -11 8 172.81 11.74 4 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1.70 4 6 5 12.28 2.71 -4 -6 -5 2.78 1.84 4 6 5 10.82 4.92 -4 -6 -6 3.70 1.59 4 6 6 1.62 3.81 4 6 6 7.08 2.15 -4 -6 -7 12.21 2.03 4 6 7 14.87 2.82 -4 -6 -8 101.48 4.25 4 6 8 106.16 9.47 4 6 9 16.28 4.78 4 6 10 72.81 8.02 4 6 11 -8.71 6.49 4 6 12 6.40 5.30 4 6 13 -3.63 5.82 4 6 14 34.50 7.28 4 6 15 5.15 5.67 4 6 16 69.97 10.37 4 6 17 4.39 6.40 4 7 -24 2.91 5.51 4 7 -23 5.06 5.21 4 7 -22 6.78 5.65 4 7 -21 6.81 5.42 4 7 -20 49.12 7.98 4 7 -19 5.47 5.66 4 7 -18 6.13 5.28 4 7 -17 92.96 10.24 4 7 -16 647.60 23.36 4 7 -15 86.82 9.74 4 7 -14 296.65 15.64 4 7 -13 18.73 5.95 4 7 -12 488.10 19.07 4 7 -11 35.60 6.42 4 7 -10 32.58 5.96 4 7 -9 333.09 14.42 4 7 -8 158.67 10.44 4 7 -8 158.93 9.03 4 7 -7 92.89 6.64 4 7 -7 81.79 7.05 4 7 -6 156.02 9.26 4 7 -6 159.72 8.72 4 7 -5 213.71 10.15 4 7 -4 35.46 5.00 4 7 -3 230.85 10.95 4 7 -3 217.35 9.95 4 7 -2 77.49 6.87 4 7 -2 69.86 5.87 4 7 -1 78.72 6.91 4 7 -1 81.93 5.96 -4 -7 0 286.48 11.00 4 7 0 271.99 12.89 4 7 0 280.29 10.49 -4 -7 -1 546.47 13.90 4 7 1 511.58 13.33 4 7 1 528.59 17.36 -4 -7 -2 261.35 9.53 4 7 2 251.74 12.65 4 7 2 242.48 9.12 4 7 3 6.25 2.29 -4 -7 -3 6.19 2.63 4 7 3 6.71 3.96 4 7 4 71.56 4.52 -4 -7 -4 74.02 5.02 4 7 4 83.07 8.19 4 7 4 64.96 4.84 -4 -7 -5 39.86 3.85 4 7 5 42.41 6.58 4 7 5 39.19 4.03 -4 -7 -6 109.96 5.54 4 7 6 100.53 9.10 4 7 7 25.34 6.07 -4 -7 -7 30.98 3.09 4 7 8 -2.66 5.15 4 7 9 -7.77 5.80 4 7 10 36.75 6.54 4 7 11 -2.88 5.76 4 7 12 92.46 10.45 4 7 13 18.25 6.56 4 7 14 71.63 10.14 4 7 15 11.04 6.33 4 7 16 19.44 7.37 4 8 -23 12.44 6.72 4 8 -22 7.32 5.48 4 8 -21 22.36 7.10 4 8 -20 22.29 6.55 4 8 -19 8.84 5.77 4 8 -18 149.72 12.59 4 8 -17 2.88 5.10 4 8 -16 127.23 11.44 4 8 -15 0.79 4.63 4 8 -14 136.99 11.07 4 8 -13 40.65 6.66 4 8 -12 22.14 5.56 4 8 -11 89.93 8.86 4 8 -10 5.33 4.16 4 8 -9 15.73 4.48 4 8 -9 13.06 3.67 4 8 -8 12.23 4.02 4 8 -8 14.70 3.67 4 8 -7 88.33 7.94 4 8 -7 84.44 6.92 4 8 -6 404.61 14.24 4 8 -5 248.22 11.45 4 8 -4 34.79 5.37 4 8 -3 177.53 10.04 4 8 -2 26.57 4.84 -4 -8 1 226.58 10.49 4 8 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10.83 -4 -9 -1 5.72 3.46 4 9 1 3.00 3.85 4 9 2 54.16 7.15 -4 -9 -2 51.97 5.53 -4 -9 -3 6.94 2.90 4 9 3 8.14 4.36 4 9 4 68.53 8.16 4 9 5 16.60 5.48 4 9 6 -0.50 5.25 4 9 7 -5.75 5.56 4 9 8 -4.74 6.14 4 9 9 4.60 5.43 4 9 10 2.01 5.08 4 9 11 1.61 5.76 4 9 12 2.31 5.63 4 9 13 84.93 11.07 4 10 -20 36.40 8.10 4 10 -19 9.34 5.86 4 10 -18 54.63 8.96 4 10 -17 1.42 5.38 4 10 -16 92.38 10.53 4 10 -15 -0.89 4.88 4 10 -14 72.93 9.28 4 10 -13 4.82 4.58 4 10 -12 17.86 5.66 4 10 -12 21.59 4.38 4 10 -11 3.46 4.21 4 10 -11 5.18 3.03 4 10 -10 33.56 6.27 4 10 -10 40.96 5.20 4 10 -9 -4.57 4.81 4 10 -9 -3.34 3.66 4 10 -8 52.29 6.74 4 10 -8 51.55 5.84 4 10 -7 7.28 3.09 4 10 -6 177.00 10.20 4 10 -5 10.44 3.72 4 10 -4 89.49 7.87 4 10 -3 40.98 6.13 4 10 -2 9.97 4.23 -4 -10 1 13.49 4.20 4 10 -1 17.53 4.90 -4 -10 0 3.79 3.09 4 10 0 5.65 4.08 -4 -10 -1 7.04 3.27 4 10 1 4.62 4.09 -4 -10 -2 22.98 4.29 4 10 2 27.67 5.89 4 10 3 9.81 4.95 4 10 4 2.07 4.70 4 10 5 -6.86 6.29 4 10 6 24.62 5.66 4 10 7 -5.88 6.07 4 10 8 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5.63 4 13 -12 12.61 5.76 4 13 -11 8.34 4.55 4 13 -10 20.89 5.48 4 13 -9 -10.95 6.02 4 13 -8 -0.68 4.78 4 14 -11 60.99 9.29 4 14 -10 2.76 5.00 4 14 -9 36.97 7.40 4 14 -8 0.10 4.27 4 14 -7 16.07 5.65 5 -16 -5 8.39 6.03 5 -16 -4 161.64 14.26 5 -16 -3 23.29 7.39 5 -16 -2 13.38 6.14 5 -16 -1 33.19 7.41 5 -16 0 5.81 5.48 5 -16 1 113.76 12.18 5 -16 2 10.91 6.33 5 -16 3 99.45 11.51 5 -16 4 7.75 5.85 5 -16 5 39.07 8.03 5 -16 6 6.72 5.41 5 -16 7 8.71 6.04 5 -15 -10 11.23 5.83 5 -15 -9 -1.67 5.22 5 -15 -8 2.40 4.76 5 -15 -7 0.61 4.72 5 -15 -6 -1.79 5.47 5 -15 -5 24.11 6.87 5 -15 -4 -1.62 4.94 5 -15 -3 -2.81 5.15 5 -15 -2 8.71 4.99 5 -15 -1 -1.00 5.64 5 -15 0 72.76 9.56 5 -15 1 18.85 6.02 5 -15 2 123.10 11.92 5 -15 3 35.90 7.56 5 -15 4 80.08 9.85 5 -15 5 17.67 6.66 5 -15 6 49.78 8.69 5 -15 7 13.67 6.39 5 -15 8 43.71 8.43 5 -15 9 54.31 8.72 5 -15 10 19.39 6.54 5 -15 11 47.65 8.62 5 -15 12 1.98 4.96 5 -15 13 1.01 5.24 5 -14 -14 9.56 5.57 5 -14 -13 -0.67 5.16 5 -14 -12 1.34 4.93 5 -14 -11 5.66 5.02 5 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8 16.84 5.63 5 -13 9 85.58 9.55 5 -13 10 38.85 6.98 5 -13 11 -0.35 4.20 5 -13 12 0.84 5.01 5 -13 13 98.70 10.46 5 -13 14 -3.07 5.21 5 -13 15 1.01 4.75 5 -13 16 15.19 5.92 5 -13 17 7.56 5.44 5 -13 18 16.62 6.11 5 -13 19 5.49 6.09 5 -12 -18 7.63 5.92 5 -12 -17 2.23 5.12 5 -12 -16 5.66 5.23 5 -12 -15 8.69 5.64 5 -12 -14 7.97 5.47 5 -12 -13 -0.03 4.77 5 -12 -12 1.33 4.26 5 -12 -11 -0.95 4.34 5 -12 -10 8.27 4.97 5 -12 -9 3.75 4.80 5 -12 -8 42.91 7.33 5 -12 -7 20.62 6.31 5 -12 -6 169.43 12.42 5 -12 -5 53.40 8.24 5 -12 -4 245.60 14.61 5 -12 -3 178.95 12.81 5 -12 -2 366.43 17.30 5 -12 -1 67.86 8.28 5 -12 0 8.18 4.16 5 -12 1 6.70 4.21 5 -12 2 97.47 9.42 5 -12 3 17.87 5.73 5 -12 4 133.77 11.54 5 -12 5 3.79 4.40 5 -12 6 41.24 6.93 5 -12 7 134.81 11.15 5 -12 8 146.08 11.40 5 -12 9 87.17 9.44 5 -12 10 20.46 5.65 5 -12 11 25.98 6.06 5 -12 12 25.00 5.96 5 -12 13 30.04 6.55 5 -12 14 32.23 7.29 5 -12 15 7.83 5.43 5 -12 16 37.90 7.71 5 -12 17 7.85 5.18 5 -12 18 7.31 5.33 5 -12 19 0.26 4.75 -5 12 -20 2.98 4.75 -5 12 -21 12.36 6.00 5 -11 -19 1.56 4.96 5 -11 -18 20.47 6.31 5 -11 -17 1.70 4.70 5 -11 -16 9.29 4.97 5 -11 -15 5.88 4.68 5 -11 -14 2.41 4.51 5 -11 -13 4.18 4.26 5 -11 -12 -0.33 4.21 5 -11 -11 -0.46 4.22 5 -11 -10 8.15 4.71 5 -11 -9 107.79 10.06 5 -11 -8 4.53 4.79 5 -11 -7 60.80 7.82 5 -11 -6 83.97 8.90 5 -11 -5 64.55 7.82 5 -11 -4 53.26 5.57 5 -11 -4 65.00 7.81 5 -11 -3 61.40 7.50 5 -11 -3 60.96 5.38 5 -11 -2 18.78 3.48 5 -11 -2 18.79 5.27 5 -11 -1 246.07 8.85 5 -11 -1 254.60 13.84 5 -11 0 55.63 4.28 5 -11 0 62.28 7.68 5 -11 1 152.25 5.90 5 -11 1 169.87 11.44 5 -11 2 71.24 3.55 5 -11 2 87.93 8.63 5 -11 3 31.94 1.79 5 -11 3 60.81 7.46 5 -11 4 164.54 11.33 5 -11 5 44.09 6.83 5 -11 6 -0.29 3.94 5 -11 7 54.92 7.42 5 -11 8 208.19 12.74 5 -11 9 36.60 6.54 5 -11 10 59.15 8.31 5 -11 11 22.05 5.48 5 -11 12 24.72 6.72 5 -11 13 35.72 6.33 5 -11 14 19.09 5.94 5 -11 15 55.60 7.77 5 -11 16 -0.29 4.35 5 -11 17 -0.27 4.34 5 -11 18 89.24 10.05 -5 11 -19 11.48 5.55 -5 11 -20 66.96 9.29 -5 11 -21 34.22 7.60 -5 11 -22 80.14 9.91 -5 11 -23 64.62 9.54 5 -10 -21 -0.82 5.03 5 -10 -20 7.08 5.08 5 -10 -19 1.89 4.83 5 -10 -18 2.78 4.91 5 -10 -17 -2.38 5.19 5 -10 -16 1.74 4.54 5 -10 -15 -1.05 4.39 5 -10 -14 29.21 6.27 5 -10 -13 80.54 9.00 5 -10 -12 23.81 6.11 5 -10 -11 323.64 16.60 5 -10 -10 53.64 7.63 5 -10 -9 129.90 10.53 5 -10 -8 5.63 4.55 5 -10 -7 130.62 10.21 5 -10 -6 12.55 4.87 5 -10 -5 176.52 11.52 5 -10 -4 228.03 10.03 5 -10 -4 262.05 13.87 5 -10 -3 100.88 6.44 5 -10 -3 113.46 9.29 5 -10 -2 9.01 2.39 5 -10 -2 27.46 5.45 5 -10 -1 6.52 2.12 5 -10 -1 9.83 4.04 5 -10 0 9.67 2.05 5 -10 0 14.23 4.46 5 -10 1 128.13 10.13 5 -10 1 120.13 5.23 5 -10 2 157.03 10.36 5 -10 2 142.00 4.87 5 -10 3 51.33 2.41 5 -10 3 74.49 7.67 5 -10 4 523.28 18.31 5 -10 5 46.62 6.65 5 -10 6 347.16 15.30 5 -10 7 27.62 5.57 5 -10 8 265.92 14.66 5 -10 9 103.23 9.38 5 -10 10 446.08 18.14 5 -10 11 -0.40 4.21 5 -10 12 104.84 9.23 5 -10 13 16.18 4.95 5 -10 14 253.04 14.67 5 -10 15 17.06 6.13 5 -10 16 89.96 9.72 5 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8.28 5 -8 1 348.62 13.47 5 -8 2 86.37 4.25 5 -8 2 83.46 7.51 5 -8 3 924.22 11.19 5 -8 3 963.30 22.21 5 -8 4 208.37 10.72 5 -8 5 649.04 18.52 5 -8 5 450.96 5.97 5 -8 6 1.75 0.68 5 -8 6 9.57 4.18 5 -8 7 769.60 20.30 5 -8 7 518.32 6.26 5 -8 8 44.47 5.68 5 -8 8 42.93 2.10 5 -8 9 361.44 6.44 5 -8 9 417.73 15.33 5 -8 10 369.35 7.04 5 -8 10 371.90 14.85 5 -8 11 26.99 2.84 5 -8 11 24.91 5.30 5 -8 12 289.77 13.48 5 -8 12 303.68 7.79 5 -8 13 52.71 6.75 5 -8 13 61.99 4.20 5 -8 14 169.19 11.06 5 -8 14 194.59 7.44 5 -8 15 27.63 5.64 5 -8 16 48.22 6.83 -5 8 -17 76.52 8.05 -5 8 -18 127.44 10.40 -5 8 -19 3.23 3.97 -5 8 -20 -2.94 4.36 -5 8 -21 160.19 12.34 -5 8 -22 47.90 7.49 -5 8 -23 1.18 4.31 -5 8 -24 4.87 4.29 -5 8 -25 -3.08 5.28 -5 8 -26 3.67 4.79 -5 8 -27 -2.88 5.04 5 -7 -25 2.30 4.92 5 -7 -24 58.40 9.81 5 -7 -23 17.79 6.80 5 -7 -22 56.29 8.92 5 -7 -21 -0.70 4.89 5 -7 -20 3.07 5.25 5 -7 -19 21.39 6.00 5 -7 -18 2.00 4.51 5 -7 -17 64.90 8.63 5 -7 -16 36.50 6.94 5 -7 -16 32.94 6.00 5 -7 -15 237.54 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32.82 4.13 6 -6 12 299.55 12.43 -6 6 -12 290.05 11.24 6 -6 12 260.06 10.11 6 -6 13 1.74 3.15 -6 6 -13 -0.12 2.64 6 -6 14 2.31 3.24 6 -6 14 -3.17 3.50 -6 6 -15 -0.02 3.23 6 -6 15 -3.33 3.73 6 -6 15 -0.07 3.46 -6 6 -16 17.10 4.21 6 -6 16 15.64 4.36 -6 6 -17 1.78 3.28 6 -6 17 1.91 3.80 -6 6 -18 33.22 5.42 6 -6 18 38.21 6.13 -6 6 -19 13.14 4.31 6 -6 19 20.51 5.11 -6 6 -20 68.27 7.76 6 -6 20 74.80 7.73 -6 6 -21 32.09 6.15 6 -6 21 36.33 6.51 -6 6 -22 37.84 6.27 6 -6 22 46.14 7.13 -6 6 -23 -0.87 3.56 6 -6 23 8.34 5.22 6 -6 24 61.61 8.19 6 -5 -25 3.84 5.33 6 -5 -24 18.68 6.67 6 -5 -23 79.93 10.50 6 -5 -22 13.66 5.98 6 -5 -21 3.47 4.85 6 -5 -20 41.72 7.77 6 -5 -19 32.15 7.05 6 -5 -18 5.70 4.79 6 -5 -17 -0.60 4.67 6 -5 -16 133.50 11.13 6 -5 -15 23.73 6.03 6 -5 -14 108.06 9.86 6 -5 -13 48.78 6.72 6 -5 -12 120.89 9.47 6 -5 -11 506.36 17.63 6 -5 -10 183.04 10.75 6 -5 -9 63.04 6.42 6 -5 -8 6.82 3.75 6 -5 -7 124.18 8.35 6 -5 -6 12.69 4.23 6 -5 -5 38.70 4.90 6 -5 -5 36.37 4.82 -6 5 5 32.84 4.26 6 -5 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1.44 6 5 5 26.59 5.72 6 5 6 3.45 4.23 6 5 7 18.41 5.75 6 5 8 -0.79 4.51 6 5 9 5.75 4.55 6 5 10 2.33 4.88 6 5 11 162.75 12.55 6 5 12 16.89 5.66 6 5 13 16.68 5.73 6 5 14 -10.59 7.02 6 5 15 35.38 7.50 6 5 16 1.87 5.74 6 6 -23 0.95 5.20 6 6 -22 40.43 8.51 6 6 -21 6.65 5.49 6 6 -20 80.48 10.22 6 6 -19 6.74 5.17 6 6 -18 5.75 4.93 6 6 -17 66.87 8.85 6 6 -16 25.05 6.10 6 6 -15 73.05 8.52 6 6 -14 23.26 5.40 6 6 -13 6.14 4.19 6 6 -12 43.56 6.76 6 6 -11 5.09 4.22 6 6 -10 3.79 3.90 6 6 -9 3.57 3.62 6 6 -8 17.01 3.97 6 6 -7 132.85 8.65 6 6 -7 125.56 9.20 6 6 -6 132.06 9.34 6 6 -6 148.62 8.96 6 6 -5 5.72 3.08 6 6 -5 6.54 3.83 6 6 -4 7.22 3.18 6 6 -4 9.12 3.94 6 6 -4 3.92 2.62 6 6 -3 80.37 6.19 6 6 -3 70.85 5.67 6 6 -3 76.41 7.40 6 6 -2 10.49 3.06 6 6 -2 5.49 3.80 6 6 -2 6.11 2.53 6 6 -1 41.62 6.12 6 6 -1 39.83 4.34 6 6 -1 35.86 3.93 6 6 0 77.97 5.55 6 6 0 73.24 5.14 6 6 0 82.04 7.95 6 6 1 6.02 2.41 6 6 1 4.11 4.19 6 6 1 0.66 2.00 6 6 2 106.85 5.57 6 6 2 120.66 9.91 6 6 3 99.88 5.07 6 6 3 107.83 9.87 6 6 4 179.01 6.19 6 6 4 212.97 13.06 6 6 5 16.21 5.43 6 6 6 80.26 9.05 6 6 7 -2.54 4.92 6 6 8 54.07 7.77 6 6 9 8.48 4.96 6 6 10 8.04 5.00 6 6 11 15.56 5.23 6 6 12 99.44 10.68 6 6 13 -4.85 6.51 6 6 14 62.74 9.39 6 7 -22 86.58 11.48 6 7 -21 24.25 7.62 6 7 -20 42.26 8.21 6 7 -19 447.78 21.35 6 7 -18 21.75 7.02 6 7 -17 120.72 11.12 6 7 -16 -2.33 4.62 6 7 -15 6.24 4.29 6 7 -14 -2.44 4.64 6 7 -13 -1.66 4.74 6 7 -12 10.91 4.25 6 7 -11 22.57 5.45 6 7 -10 57.03 7.09 6 7 -9 4.59 3.96 6 7 -9 1.34 3.84 6 7 -8 11.93 4.14 6 7 -8 7.88 3.93 6 7 -7 12.75 3.99 6 7 -7 9.01 4.06 6 7 -6 134.66 9.12 6 7 -6 142.20 10.18 6 7 -5 15.32 4.48 6 7 -5 22.04 4.57 6 7 -4 2.40 2.88 6 7 -4 2.15 3.68 6 7 -3 46.04 5.55 6 7 -3 45.40 6.56 6 7 -2 450.34 14.15 6 7 -2 430.07 13.57 6 7 -2 448.69 17.23 6 7 -1 37.41 4.79 6 7 -1 43.69 6.92 6 7 0 68.36 5.78 6 7 0 80.71 8.25 6 7 1 40.58 4.95 6 7 1 49.48 8.14 6 7 2 433.22 12.08 6 7 2 445.44 18.35 6 7 3 90.65 9.25 6 7 4 154.55 11.71 6 7 5 4.40 5.13 6 7 6 32.61 6.71 6 7 7 1.02 4.25 6 7 8 6.92 5.25 6 7 9 5.84 4.78 6 7 10 -16.03 7.04 6 7 11 -17.16 7.91 6 7 12 -1.13 6.02 6 7 13 -11.40 6.74 6 8 -21 43.42 8.95 6 8 -20 56.11 9.21 6 8 -19 67.43 9.65 6 8 -18 31.27 7.67 6 8 -17 3.25 5.93 6 8 -16 9.24 5.08 6 8 -15 1.54 4.54 6 8 -14 14.45 5.52 6 8 -13 -0.29 4.20 6 8 -12 31.18 6.46 6 8 -11 51.21 7.65 6 8 -11 47.77 6.26 6 8 -10 29.25 6.00 6 8 -10 19.49 4.60 6 8 -9 17.82 4.74 6 8 -9 16.08 4.18 6 8 -8 34.89 5.69 6 8 -8 36.98 5.73 6 8 -7 2.54 3.59 6 8 -7 -0.69 3.29 6 8 -6 185.34 10.84 6 8 -6 188.92 11.57 6 8 -5 1.67 3.95 6 8 -5 3.89 3.56 6 8 -4 40.07 5.44 6 8 -4 39.23 6.12 6 8 -3 12.40 4.12 6 8 -3 15.90 5.16 6 8 -2 30.54 5.00 6 8 -2 22.40 5.52 6 8 -1 48.43 5.47 6 8 -1 44.13 6.86 6 8 0 -4.25 5.09 6 8 0 2.63 2.74 6 8 1 122.99 10.70 6 8 2 111.05 10.16 6 8 3 40.65 7.12 6 8 4 9.73 5.64 6 8 5 105.10 10.53 6 8 6 26.34 6.80 6 8 7 100.49 10.54 6 8 8 5.51 5.40 6 8 9 41.25 7.37 6 8 10 17.86 5.84 6 8 11 31.46 7.25 6 9 -20 -0.33 5.57 6 9 -19 30.18 8.04 6 9 -18 10.17 5.99 6 9 -17 14.65 6.13 6 9 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6 10 -6 5.48 4.05 6 10 -6 -9.47 5.13 6 10 -5 90.34 8.57 6 10 -5 77.45 8.41 6 10 -4 19.67 5.09 6 10 -4 32.26 5.94 6 10 -3 20.83 5.63 6 10 -2 74.77 8.76 6 10 -1 40.94 7.56 6 10 0 156.47 12.24 6 10 1 19.34 6.37 6 10 2 10.77 5.52 6 10 3 4.01 5.25 6 10 4 9.28 5.55 6 10 5 6.52 4.81 6 10 6 -15.40 6.83 6 10 7 -22.59 8.07 6 11 -17 43.05 8.45 6 11 -16 11.04 5.89 6 11 -15 45.54 8.37 6 11 -14 17.95 6.92 6 11 -13 119.83 12.16 6 11 -12 6.81 5.34 6 11 -11 62.20 8.71 6 11 -10 51.97 7.71 6 11 -9 77.45 9.13 6 11 -8 32.37 6.62 6 11 -7 0.81 3.94 6 11 -6 25.05 5.85 6 11 -5 25.07 5.97 6 11 -4 63.85 8.17 6 11 -3 2.64 4.62 6 11 -2 19.60 6.12 6 11 -1 60.02 8.84 6 11 0 17.48 6.11 6 11 1 19.67 6.25 6 11 2 8.76 5.45 6 11 3 22.88 6.90 6 11 4 -0.30 5.25 6 11 5 -19.30 7.39 6 12 -14 49.27 8.82 6 12 -13 10.86 5.88 6 12 -12 3.54 4.72 6 12 -11 -2.97 4.75 6 12 -10 -1.16 4.52 6 12 -9 -8.09 5.19 6 12 3 -3.93 6.35 6 13 -12 -0.49 4.74 7 -16 -1 5.98 5.06 7 -16 0 77.75 10.79 7 -16 1 3.50 5.58 7 -16 2 58.43 9.32 7 -16 3 2.88 5.06 7 -16 4 -1.11 5.14 7 -16 5 16.26 6.52 7 -15 -8 2.71 4.98 7 -15 -7 1.08 4.99 7 -15 -6 11.98 5.76 7 -15 -5 13.29 5.63 7 -15 -4 17.72 6.39 7 -15 -3 51.09 8.76 7 -15 -2 16.72 6.07 7 -15 -1 31.42 7.37 7 -15 0 45.65 8.35 7 -15 1 33.43 7.24 7 -15 2 40.92 8.19 7 -15 3 2.13 5.09 7 -15 4 28.92 6.67 7 -15 5 -0.03 5.18 7 -15 6 51.77 8.60 7 -15 7 100.51 11.65 7 -15 8 61.22 9.56 7 -15 9 12.83 6.17 7 -15 10 9.76 5.46 7 -15 11 6.70 5.21 7 -15 12 5.66 5.24 7 -14 -12 3.14 5.20 7 -14 -11 3.96 5.71 7 -14 -10 20.33 6.63 7 -14 -9 7.69 5.91 7 -14 -8 38.63 7.57 7 -14 -7 12.94 6.07 7 -14 -6 52.01 8.64 7 -14 -5 33.73 7.83 7 -14 -4 2.02 4.73 7 -14 -3 6.97 5.36 7 -14 -2 50.08 8.48 7 -14 -1 9.39 5.10 7 -14 0 4.76 4.48 7 -14 1 -2.87 5.01 7 -14 2 60.41 8.49 7 -14 3 5.34 4.91 7 -14 4 0.21 4.67 7 -14 5 64.47 8.75 7 -14 6 16.08 5.97 7 -14 7 44.58 7.95 7 -14 8 230.45 16.12 7 -14 9 9.89 5.69 7 -14 10 50.36 8.28 7 -14 11 10.55 5.83 7 -14 12 136.76 12.74 7 -14 13 3.37 5.40 7 -14 14 48.05 8.43 7 -14 15 -3.75 5.43 7 -14 16 4.15 5.00 7 -13 -15 12.44 6.62 7 -13 -14 11.88 6.60 7 -13 -13 21.67 6.83 7 -13 -12 17.44 6.78 7 -13 -11 12.35 5.89 7 -13 -10 30.73 7.30 7 -13 -9 0.82 4.93 7 -13 -8 4.91 4.93 7 -13 -7 2.00 4.72 7 -13 -6 9.19 5.40 7 -13 -5 39.44 7.79 7 -13 -4 15.29 6.14 7 -13 -3 23.71 6.34 7 -13 -2 67.01 9.96 7 -13 -1 0.17 4.54 7 -13 0 22.70 6.01 7 -13 1 25.97 6.37 7 -13 2 54.55 7.98 7 -13 3 44.88 7.48 7 -13 4 -2.59 4.98 7 -13 5 27.82 6.12 7 -13 6 1.86 4.12 7 -13 7 48.24 7.86 7 -13 8 11.46 5.65 7 -13 9 24.95 6.42 7 -13 10 14.16 6.05 7 -13 11 26.84 6.80 7 -13 12 13.46 6.96 7 -13 13 39.55 7.57 7 -13 14 0.00 4.50 7 -13 15 22.91 6.70 7 -13 16 16.87 6.57 7 -13 17 -2.06 5.00 7 -13 18 40.22 8.40 7 -13 19 -2.37 4.85 7 -12 -17 6.66 6.19 7 -12 -16 16.51 6.89 7 -12 -15 13.09 6.46 7 -12 -14 22.72 6.87 7 -12 -13 34.34 7.73 7 -12 -12 15.51 6.90 7 -12 -11 225.42 15.84 7 -12 -10 12.33 6.46 7 -12 -9 96.12 10.67 7 -12 -8 51.35 8.62 7 -12 -7 38.35 7.56 7 -12 -6 16.54 6.09 7 -12 -5 44.89 7.74 7 -12 -4 17.00 5.48 7 -12 -3 27.69 6.77 7 -12 -2 45.21 7.45 7 -12 -1 33.93 6.73 7 -12 0 95.36 9.39 7 -12 1 22.47 5.98 7 -12 2 14.90 4.93 7 -12 3 49.50 7.38 7 -12 4 103.53 9.88 7 -12 5 102.46 9.99 7 -12 6 94.33 9.62 7 -12 7 22.94 6.01 7 -12 8 8.09 5.44 7 -12 9 0.88 4.10 7 -12 10 6.79 4.88 7 -12 11 7.16 4.68 7 -12 12 10.13 5.35 7 -12 13 28.11 6.65 7 -12 14 33.10 6.90 7 -12 15 2.51 4.94 7 -12 16 6.25 4.98 7 -12 17 0.38 4.37 7 -12 18 8.42 5.31 7 -12 19 34.37 7.81 7 -12 20 35.79 7.65 -7 12 -21 4.28 5.12 7 -11 -19 -0.32 5.71 7 -11 -18 4.87 5.48 7 -11 -17 2.06 5.46 7 -11 -16 3.22 5.15 7 -11 -15 1.51 4.81 7 -11 -14 13.14 5.71 7 -11 -13 5.53 5.40 7 -11 -12 167.50 13.55 7 -11 -11 80.10 9.76 7 -11 -10 33.44 7.05 7 -11 -9 16.67 6.18 7 -11 -8 53.18 8.06 7 -11 -7 20.84 5.96 7 -11 -6 33.48 6.93 7 -11 -5 115.36 10.61 7 -11 -4 30.53 6.52 7 -11 -3 150.22 8.63 7 -11 -3 158.25 11.95 7 -11 -2 245.91 10.19 7 -11 -2 264.33 14.65 7 -11 -1 69.60 5.60 7 -11 -1 82.72 8.68 7 -11 0 157.08 7.39 7 -11 0 161.35 11.61 7 -11 1 123.97 6.20 7 -11 1 131.95 10.56 7 -11 2 143.06 6.02 7 -11 2 168.92 11.82 7 -11 3 17.41 5.15 7 -11 4 194.46 5.14 7 -11 4 270.00 14.50 7 -11 5 78.64 2.48 7 -11 5 155.34 11.41 7 -11 6 17.68 5.36 7 -11 7 20.65 5.44 7 -11 8 125.18 10.05 7 -11 9 8.90 4.80 7 -11 10 50.77 7.29 7 -11 11 44.84 6.79 7 -11 12 11.16 4.45 7 -11 13 -1.03 4.30 7 -11 14 1.54 4.04 7 -11 15 171.77 12.89 7 -11 16 22.79 6.26 7 -11 17 29.49 6.60 7 -11 18 46.41 7.52 7 -11 19 47.62 8.00 -7 11 -20 25.18 6.79 -7 11 -21 27.60 6.85 -7 11 -22 1.96 5.12 -7 11 -23 24.76 6.52 7 -10 -20 37.18 8.33 7 -10 -19 2.35 5.32 7 -10 -18 15.20 5.93 7 -10 -17 12.31 5.83 7 -10 -16 20.14 6.35 7 -10 -15 11.46 5.46 7 -10 -14 150.54 12.91 7 -10 -13 58.51 8.50 7 -10 -12 -1.64 5.02 7 -10 -11 -1.78 4.58 7 -10 -10 16.06 5.37 7 -10 -9 32.61 6.42 7 -10 -8 7.51 4.93 7 -10 -7 0.22 4.07 7 -10 -6 28.20 6.72 7 -10 -5 5.01 4.27 7 -10 -4 69.07 6.53 7 -10 -4 79.62 8.95 7 -10 -3 34.87 4.76 7 -10 -3 29.80 6.04 7 -10 -2 41.85 5.03 7 -10 -2 43.62 7.15 7 -10 -1 175.84 7.90 7 -10 -1 174.00 11.46 7 -10 0 21.53 3.55 7 -10 0 21.29 5.31 7 -10 1 161.94 6.81 7 -10 1 160.43 10.88 7 -10 2 76.03 4.82 7 -10 2 65.92 7.87 7 -10 3 621.47 20.51 7 -10 4 358.60 15.73 7 -10 5 49.04 2.91 7 -10 5 57.67 7.45 7 -10 6 290.21 14.38 7 -10 6 234.32 5.59 7 -10 7 79.50 3.34 7 -10 7 124.37 9.77 7 -10 8 54.21 7.65 7 -10 8 17.74 1.85 7 -10 9 104.19 8.88 7 -10 9 92.33 3.34 7 -10 10 53.24 6.98 7 -10 10 54.81 2.74 7 -10 11 18.68 6.12 7 -10 12 119.95 9.77 7 -10 13 51.17 6.90 7 -10 14 -1.23 4.08 7 -10 15 0.71 3.84 7 -10 16 65.92 8.19 7 -10 17 38.46 7.00 7 -10 18 23.83 5.91 -7 10 -19 9.54 5.23 7 -10 19 5.90 4.30 -7 10 -20 20.05 5.83 -7 10 -21 11.73 5.38 -7 10 -22 2.27 4.22 -7 10 -23 24.87 6.55 -7 10 -24 5.53 5.23 -7 10 -25 103.97 11.25 7 -9 -21 23.88 7.40 7 -9 -20 6.12 4.95 7 -9 -19 31.04 7.45 7 -9 -18 0.94 4.84 7 -9 -17 28.35 6.72 7 -9 -16 -3.79 5.29 7 -9 -15 152.55 12.68 7 -9 -14 84.36 9.67 7 -9 -13 44.39 7.51 7 -9 -12 87.70 9.71 7 -9 -11 115.67 10.59 7 -9 -10 44.90 7.68 7 -9 -9 26.69 6.80 7 -9 -8 226.38 13.73 7 -9 -7 98.35 9.58 7 -9 -6 149.15 10.72 7 -9 -5 147.37 10.81 7 -9 -4 69.73 5.97 7 -9 -4 66.54 7.55 7 -9 -3 266.85 10.62 7 -9 -3 283.21 14.32 7 -9 -2 33.27 5.67 7 -9 -1 274.17 13.59 7 -9 0 81.44 8.03 7 -9 1 146.27 9.99 7 -9 2 16.23 4.49 7 -9 3 100.98 8.36 7 -9 4 20.64 4.67 7 -9 5 78.86 7.33 7 -9 5 77.29 4.18 7 -9 6 56.27 6.43 7 -9 6 58.20 3.55 7 -9 7 54.44 3.38 7 -9 7 58.16 6.95 7 -9 8 123.39 4.95 7 -9 8 132.42 9.44 7 -9 9 125.63 9.34 7 -9 9 134.38 5.40 7 -9 10 455.42 17.12 7 -9 10 454.41 10.03 7 -9 11 19.52 5.22 7 -9 11 10.05 2.23 7 -9 12 341.34 15.20 7 -9 12 352.77 9.78 7 -9 13 16.44 5.33 7 -9 13 14.84 3.22 7 -9 14 10.23 4.25 7 -9 14 15.80 3.29 7 -9 15 5.36 4.21 7 -9 15 7.82 3.05 7 -9 16 35.78 6.41 7 -9 17 -0.69 3.58 -7 9 -18 0.46 4.00 7 -9 18 1.03 3.96 -7 9 -19 -2.80 4.56 -7 9 -20 16.69 5.27 -7 9 -21 -0.27 4.31 -7 9 -22 11.40 5.11 -7 9 -23 6.58 4.44 -7 9 -24 12.42 5.57 7 -8 -22 1.71 5.13 7 -8 -22 5.60 5.91 7 -8 -21 19.90 6.83 7 -8 -21 25.75 7.26 7 -8 -20 3.92 5.00 7 -8 -20 5.32 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138.60 4.69 7 5 4 10.58 5.14 7 5 5 86.56 9.25 7 5 6 5.51 4.98 7 5 7 -2.14 4.42 7 5 8 15.21 5.59 7 5 9 4.31 4.81 7 5 10 21.45 6.47 7 5 11 4.33 5.23 7 5 12 24.03 6.63 7 5 13 -11.25 7.69 7 5 14 14.83 5.61 7 6 -23 55.21 9.69 7 6 -22 24.85 7.93 7 6 -21 77.32 10.62 7 6 -20 9.85 6.64 7 6 -19 80.68 11.69 7 6 -18 17.02 6.32 7 6 -17 49.32 8.50 7 6 -16 11.67 5.21 7 6 -15 22.02 6.00 7 6 -14 43.49 6.84 7 6 -13 -0.09 4.60 7 6 -12 -1.67 4.71 7 6 -11 -3.92 4.49 7 6 -10 30.10 5.74 7 6 -9 26.70 5.14 7 6 -8 1.06 3.28 7 6 -7 76.11 7.08 7 6 -7 77.25 7.92 7 6 -6 25.33 4.95 7 6 -6 21.83 5.50 7 6 -5 51.47 5.71 7 6 -5 50.04 6.74 7 6 -4 11.99 3.41 7 6 -4 6.96 3.90 7 6 -3 14.29 3.36 7 6 -3 16.76 3.63 7 6 -3 10.51 4.51 7 6 -2 215.52 9.62 7 6 -2 221.64 13.10 7 6 -2 194.72 9.35 7 6 -1 10.13 3.12 7 6 -1 16.67 5.43 7 6 0 134.81 6.86 7 6 0 141.32 10.87 7 6 1 241.53 8.46 7 6 1 241.61 13.84 7 6 2 216.05 13.74 7 6 3 79.00 9.45 7 6 4 63.03 8.47 7 6 5 24.81 6.25 7 6 6 26.73 6.33 7 6 7 16.92 5.89 7 6 8 49.71 7.73 7 6 9 2.13 5.25 7 6 10 22.71 6.58 7 6 11 8.97 5.35 7 6 12 -19.29 7.75 7 6 13 -0.04 5.95 7 7 -22 48.94 9.49 7 7 -21 77.65 11.06 7 7 -20 167.46 15.14 7 7 -19 82.57 11.00 7 7 -18 111.85 12.10 7 7 -17 14.57 5.78 7 7 -16 18.97 5.56 7 7 -15 20.97 5.83 7 7 -14 5.51 4.45 7 7 -13 -2.81 4.71 7 7 -12 4.86 4.03 7 7 -11 47.19 7.40 7 7 -10 6.69 4.54 7 7 -9 65.31 7.55 7 7 -9 58.12 7.31 7 7 -8 26.14 5.03 7 7 -8 23.99 5.44 7 7 -7 55.89 6.26 7 7 -7 60.48 7.54 7 7 -6 2.00 3.09 7 7 -6 1.22 4.07 7 7 -5 0.09 3.49 7 7 -5 1.02 3.96 7 7 -4 -3.56 3.54 7 7 -4 -2.74 4.29 7 7 -3 25.61 4.23 7 7 -3 40.88 7.02 7 7 -2 319.00 12.19 7 7 -2 316.43 15.63 7 7 -1 305.27 11.43 7 7 -1 315.16 15.95 7 7 0 1.62 4.47 7 7 1 -3.41 4.77 7 7 2 31.13 6.39 7 7 3 4.63 4.58 7 7 4 24.63 6.20 7 7 5 -2.20 4.90 7 7 6 5.50 5.23 7 7 7 7.91 5.26 7 7 8 2.19 4.78 7 7 9 3.72 4.86 7 7 10 3.95 5.58 7 7 11 -6.62 7.07 7 8 -20 7.54 5.86 7 8 -19 31.52 7.86 7 8 -18 12.83 6.10 7 8 -17 13.49 5.92 7 8 -16 1.69 4.82 7 8 -15 10.99 5.78 7 8 -14 30.75 6.92 7 8 -13 3.23 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3.31 8 -9 12 21.92 5.47 8 -9 13 26.42 3.55 8 -9 13 26.60 5.04 8 -9 14 4.07 4.17 8 -9 14 3.18 2.73 8 -9 15 2.33 3.96 8 -9 15 1.44 2.76 8 -9 16 1.32 3.71 8 -9 17 8.04 4.17 -8 9 -18 -0.44 4.02 8 -9 18 0.27 3.93 -8 9 -19 21.37 5.41 -8 9 -20 -2.60 4.24 -8 9 -21 34.20 6.57 8 -8 -21 0.57 5.05 8 -8 -21 -0.76 5.26 8 -8 -20 2.63 5.02 8 -8 -20 7.66 6.06 8 -8 -19 21.61 6.73 8 -8 -19 26.00 7.23 8 -8 -18 -2.64 5.11 8 -8 -18 -2.44 5.04 8 -8 -17 93.56 10.58 8 -8 -17 95.66 10.86 8 -8 -16 -0.19 4.72 8 -8 -16 -2.06 5.00 8 -8 -15 125.98 11.81 8 -8 -15 122.73 11.73 8 -8 -14 2.95 4.83 8 -8 -14 1.83 5.01 8 -8 -13 105.10 10.53 8 -8 -12 123.12 10.99 8 -8 -11 0.85 4.27 8 -8 -10 33.30 6.26 8 -8 -9 -1.16 4.49 8 -8 -8 13.39 4.99 8 -8 -7 209.65 12.72 8 -8 -6 56.98 7.26 8 -8 -5 109.74 9.69 8 -8 -4 81.68 8.03 8 -8 -3 154.23 10.56 8 -8 -2 401.56 15.95 8 -8 -1 73.10 7.54 8 -8 0 138.87 9.56 8 -8 1 89.53 7.71 8 -8 2 92.81 8.13 8 -8 3 262.36 12.34 8 -8 4 35.57 5.50 8 -8 5 338.45 10.50 8 -8 5 334.45 13.85 8 -8 6 13.34 4.12 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27.28 6.11 8 4 1 22.23 2.27 8 4 2 27.93 6.04 8 4 3 6.83 4.80 8 4 4 13.05 5.21 8 4 5 71.02 9.23 8 4 6 63.51 8.58 8 4 7 29.54 6.85 8 4 8 12.58 5.33 8 4 9 1.95 5.01 8 4 10 1.33 4.43 8 4 11 4.93 5.41 8 4 12 8.35 5.84 8 4 13 8.99 6.27 8 4 14 13.71 5.90 8 5 -22 26.73 7.40 8 5 -21 0.75 5.84 8 5 -20 -3.50 6.33 8 5 -19 5.25 5.27 8 5 -18 2.85 5.76 8 5 -17 18.39 6.41 8 5 -16 4.37 5.14 8 5 -15 4.73 4.76 8 5 -14 5.84 4.83 8 5 -13 2.66 4.21 8 5 -12 267.96 14.81 8 5 -11 118.36 10.01 8 5 -10 132.61 10.13 8 5 -9 4.16 3.93 8 5 -8 210.19 11.45 8 5 -7 10.70 3.68 8 5 -6 170.00 11.57 8 5 -6 180.68 10.02 8 5 -5 7.11 4.07 8 5 -5 28.10 4.89 8 5 -4 17.99 4.85 8 5 -4 39.16 4.97 8 5 -3 183.02 8.81 8 5 -3 179.53 12.08 8 5 -2 83.22 8.95 8 5 -2 90.71 6.71 8 5 -1 198.93 12.98 8 5 -1 207.72 8.70 8 5 0 180.87 12.64 8 5 0 178.67 7.24 8 5 1 138.36 11.21 8 5 2 47.24 7.71 8 5 3 4.96 4.82 8 5 4 178.47 13.27 8 5 5 32.55 7.31 8 5 6 128.37 11.92 8 5 7 7.43 5.11 8 5 8 70.40 9.43 8 5 9 11.46 5.69 8 5 10 24.65 6.93 8 5 11 35.94 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123.25 13.29 9 8 -16 23.31 7.40 9 8 -15 81.36 10.29 9 8 -14 42.20 8.03 9 8 -13 139.00 12.37 9 8 -13 143.76 12.17 9 8 -12 12.95 5.17 9 8 -12 26.03 6.82 9 8 -11 29.48 5.65 9 8 -11 32.69 7.16 9 8 -10 -5.32 4.81 9 8 -10 8.67 5.55 9 8 -9 9.69 3.76 9 8 -9 19.45 6.08 9 8 -8 -2.28 4.87 9 8 -7 5.24 4.55 9 8 -6 39.57 7.43 9 8 -5 3.96 4.74 9 8 -4 2.95 4.88 9 8 -3 29.15 6.63 9 8 -2 -0.43 4.75 9 8 -1 43.81 8.04 9 8 0 -3.05 5.11 9 8 1 31.13 7.39 9 8 2 4.04 4.95 9 8 3 18.07 6.38 9 8 4 6.91 6.02 9 9 -17 1.29 5.37 9 9 -16 0.23 5.29 9 9 -15 2.95 5.35 9 9 -14 55.61 8.67 9 9 -13 2.77 4.69 9 9 -13 9.43 5.64 9 9 -12 76.09 9.75 9 9 -12 67.86 8.69 9 9 -11 13.12 6.01 9 9 -10 24.71 6.48 9 9 -9 15.04 5.71 9 9 -8 3.56 4.92 9 9 -7 0.20 4.78 9 9 -6 8.79 5.03 9 9 -5 -2.34 5.24 9 9 -4 -4.06 5.78 9 9 -3 0.36 5.25 9 9 -2 -1.91 5.56 9 9 -1 -0.83 5.43 9 9 0 -4.45 5.58 9 9 1 -1.14 5.40 9 10 -15 25.52 7.08 9 10 -8 5.83 5.06 9 10 -7 3.54 4.75 9 10 -6 -1.88 5.42 9 10 -5 3.56 5.01 9 10 -4 -3.88 5.75 9 10 -3 -3.83 6.03 9 10 -2 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2 79.59 9.80 10 -13 3 2.36 4.76 10 -13 4 89.40 10.34 10 -13 5 95.11 10.53 10 -13 6 109.31 11.22 10 -13 7 35.72 6.94 10 -13 8 13.00 6.15 10 -13 9 62.99 8.41 10 -13 10 8.08 5.30 10 -13 11 29.49 6.69 10 -13 12 4.47 4.72 10 -13 13 8.31 4.94 10 -13 14 17.82 5.80 10 -13 15 3.92 4.45 10 -13 16 83.42 10.56 10 -13 17 2.08 4.92 10 -13 18 15.53 6.11 10 -12 -13 127.93 13.52 10 -12 -12 77.84 11.08 10 -12 -11 108.37 12.34 10 -12 -10 13.40 6.24 10 -12 -9 9.53 6.37 10 -12 -8 4.98 5.03 10 -12 -7 -0.06 4.97 10 -12 -6 -0.91 4.61 10 -12 -5 10.00 5.67 10 -12 -4 -0.31 4.57 10 -12 -3 28.57 6.88 10 -12 -2 97.20 10.29 10 -12 -1 30.40 7.09 10 -12 0 25.37 6.01 10 -12 1 5.04 4.61 10 -12 2 30.36 6.58 10 -12 3 114.15 10.61 10 -12 4 5.76 4.42 10 -12 5 113.69 10.64 10 -12 6 0.96 4.23 10 -12 7 6.85 5.03 10 -12 8 -0.29 4.05 10 -12 9 53.13 8.24 10 -12 10 2.33 4.36 10 -12 11 1.74 4.06 10 -12 12 -2.12 4.76 10 -12 13 11.30 4.90 10 -12 14 1.51 4.46 10 -12 15 36.09 6.63 10 -12 16 17.11 5.79 10 -12 17 7.18 4.83 10 -12 18 4.19 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10 -10 -10 36.05 7.66 10 -10 -9 42.64 7.87 10 -10 -8 86.45 10.11 10 -10 -7 126.77 11.77 10 -10 -6 414.98 19.25 10 -10 -5 7.13 5.19 10 -10 -4 146.91 11.56 10 -10 -3 75.42 8.72 10 -10 -2 282.01 15.79 10 -10 -1 268.95 15.05 10 -10 0 203.38 13.43 10 -10 1 228.32 13.81 10 -10 2 394.78 17.60 10 -10 3 11.15 4.84 10 -10 4 27.96 4.70 10 -10 4 34.22 6.30 10 -10 5 97.99 8.92 10 -10 5 96.10 6.56 10 -10 6 76.96 6.20 10 -10 6 73.12 8.83 10 -10 7 53.72 7.38 10 -10 7 53.95 5.11 10 -10 8 10.89 3.37 10 -10 8 16.24 5.04 10 -10 9 9.43 4.46 10 -10 9 5.45 2.69 10 -10 10 14.20 4.54 10 -10 10 16.84 3.43 10 -10 11 3.33 3.94 10 -10 12 51.19 7.11 10 -10 13 -2.78 4.13 10 -10 14 108.83 10.00 10 -10 15 8.88 4.77 10 -10 16 48.91 7.27 10 -10 17 -0.55 3.97 10 -10 18 -4.45 4.41 10 -9 -18 4.45 5.41 10 -9 -17 17.09 6.08 10 -9 -16 25.27 7.15 10 -9 -15 15.39 6.09 10 -9 -14 9.39 5.67 10 -9 -13 -4.53 5.78 10 -9 -12 23.17 6.51 10 -9 -11 3.12 5.12 10 -9 -10 59.16 8.61 10 -9 -9 65.55 9.21 10 -9 -8 102.41 10.44 10 -9 -7 57.99 8.22 10 -9 -6 13.78 5.31 10 -9 -5 159.13 11.87 10 -9 -4 86.13 8.81 10 -9 -3 19.14 5.54 10 -9 -2 212.63 12.94 10 -9 -1 25.66 5.88 10 -9 0 379.37 16.52 10 -9 1 10.68 4.78 10 -9 2 26.06 5.82 10 -9 3 105.51 9.08 10 -9 4 117.57 9.68 10 -9 4 113.49 7.71 10 -9 5 143.36 8.12 10 -9 5 139.66 10.03 10 -9 6 2.16 3.45 10 -9 6 1.52 2.71 10 -9 7 72.33 6.07 10 -9 7 70.29 7.38 10 -9 8 90.72 8.55 10 -9 8 93.60 6.73 10 -9 9 3.12 2.64 10 -9 9 6.51 3.95 10 -9 10 42.17 5.11 10 -9 10 35.04 5.83 10 -9 11 102.38 7.32 10 -9 11 103.11 8.86 10 -9 12 -0.25 3.42 10 -9 12 1.55 2.84 10 -9 13 56.53 7.01 10 -9 13 67.64 6.42 10 -9 14 33.78 4.96 10 -9 14 34.74 5.74 10 -9 15 67.15 7.99 10 -9 16 4.22 4.10 10 -9 17 -5.40 4.57 10 -8 -19 -5.21 6.38 10 -8 -19 3.33 6.10 10 -8 -18 72.18 10.31 10 -8 -18 79.37 10.86 10 -8 -17 18.20 6.75 10 -8 -17 23.62 7.31 10 -8 -16 12.32 6.33 10 -8 -16 5.91 5.21 10 -8 -15 50.99 8.52 10 -8 -15 54.65 8.79 10 -8 -14 -0.27 4.88 10 -8 -14 -3.10 5.61 10 -8 -13 141.34 12.41 10 -8 -13 137.89 12.39 10 -8 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3.36 5.66 10 -6 -19 0.15 5.54 10 -6 -18 11.18 6.06 10 -6 -17 -1.02 4.77 10 -6 -16 133.79 12.26 10 -6 -15 5.55 5.13 10 -6 -14 212.55 14.22 10 -6 -13 19.85 6.21 10 -6 -12 291.03 15.80 10 -6 -11 4.33 5.25 10 -6 -10 89.79 9.14 10 -6 -9 475.90 19.01 10 -6 -8 219.26 13.33 10 -6 -8 232.22 13.53 10 -6 -7 135.25 10.75 10 -6 -7 139.83 10.95 10 -6 -6 15.05 4.83 10 -6 -5 327.66 14.80 10 -6 -4 30.05 5.63 10 -6 -3 11.60 4.01 10 -6 -2 16.18 4.21 10 -6 -1 92.30 7.72 10 -6 0 115.21 8.47 10 -6 1 26.02 4.56 10 -6 2 27.08 4.78 10 -6 3 168.04 9.93 10 -6 3 159.35 9.42 10 -6 4 6.82 3.62 -10 6 -4 3.25 2.67 10 -6 4 10.00 3.71 -10 6 -5 139.04 8.15 10 -6 5 149.27 8.82 10 -6 5 142.10 9.40 10 -6 6 58.66 6.85 10 -6 6 51.19 6.00 10 -6 7 139.23 9.05 10 -6 7 129.84 8.06 -10 6 -7 135.46 7.95 10 -6 8 41.98 5.30 -10 6 -8 37.23 4.71 10 -6 8 40.26 6.02 10 -6 9 42.21 5.63 10 -6 9 40.76 4.93 10 -6 10 1.50 3.50 10 -6 10 4.19 3.11 10 -6 11 57.70 5.65 10 -6 11 65.12 6.92 10 -6 12 -1.42 2.90 10 -6 12 0.41 3.53 10 -6 13 3.68 3.08 10 -6 13 3.27 3.70 10 -6 14 1.23 3.99 10 -6 15 43.78 6.65 10 -6 16 11.32 4.38 10 -6 17 201.19 12.88 10 -6 18 -9.50 5.93 10 -6 19 13.02 4.82 10 -6 20 3.38 5.04 10 -6 21 26.18 7.13 10 -6 22 25.46 7.29 10 -5 -21 -0.90 5.52 10 -5 -20 3.09 5.31 10 -5 -19 48.02 8.74 10 -5 -18 127.81 12.50 10 -5 -17 188.90 14.43 10 -5 -16 132.17 12.26 10 -5 -15 224.32 14.91 10 -5 -14 380.85 18.62 10 -5 -13 2.71 4.72 10 -5 -12 15.10 5.55 10 -5 -11 9.36 5.19 10 -5 -10 378.51 16.93 10 -5 -9 164.50 11.26 10 -5 -8 987.68 25.28 10 -5 -7 50.63 6.94 10 -5 -6 533.02 18.25 10 -5 -6 548.66 18.33 10 -5 -5 13.98 4.93 10 -5 -4 288.41 13.56 10 -5 -3 167.69 10.17 10 -5 -2 36.19 5.62 10 -5 -1 640.79 18.27 10 -5 0 12.85 3.46 -10 5 0 13.28 3.24 10 -5 1 18.16 3.59 -10 5 -1 18.22 3.49 -10 5 -2 68.23 5.64 10 -5 2 70.53 6.10 -10 5 -3 45.73 4.87 10 -5 3 52.00 6.28 10 -5 3 54.15 5.68 10 -5 4 35.89 6.21 -10 5 -4 22.56 4.40 10 -5 4 42.25 5.39 10 -5 5 61.25 6.03 -10 5 -5 49.78 4.93 10 -5 5 61.38 6.96 10 -5 6 22.13 4.61 10 -5 6 19.62 3.52 -10 5 -6 21.41 3.46 10 -5 7 20.57 5.36 10 -5 7 17.26 4.02 -10 5 -7 10.37 3.13 10 -5 8 86.93 6.38 10 -5 8 112.35 8.68 10 -5 9 27.07 5.84 10 -5 9 29.83 4.52 10 -5 10 0.89 3.80 10 -5 10 3.01 2.58 10 -5 11 18.46 4.06 10 -5 11 17.97 6.08 10 -5 12 35.06 4.42 10 -5 12 33.30 5.77 10 -5 13 75.48 8.42 10 -5 14 2.22 4.06 10 -5 15 36.84 6.33 10 -5 16 10.97 4.97 10 -5 17 -1.14 5.96 10 -5 18 -6.38 6.15 10 -5 19 21.28 5.76 10 -5 20 -1.70 5.15 10 -5 21 32.39 7.69 10 -5 22 48.07 8.96 10 -4 -22 -0.51 5.27 10 -4 -21 3.45 5.14 10 -4 -20 5.69 5.75 10 -4 -19 6.66 5.61 10 -4 -18 70.80 9.77 10 -4 -17 6.85 5.61 10 -4 -16 15.28 6.25 10 -4 -15 53.03 8.47 10 -4 -14 18.85 6.10 10 -4 -13 88.38 9.62 10 -4 -12 114.01 10.19 10 -4 -11 24.63 5.57 10 -4 -10 -5.03 4.73 10 -4 -9 114.79 9.36 10 -4 -8 110.34 9.68 10 -4 -7 17.94 4.59 10 -4 -6 187.02 10.58 10 -4 -5 94.54 7.76 10 -4 -4 484.28 16.29 10 -4 -4 479.58 15.60 10 -4 -3 232.49 11.30 10 -4 -2 926.81 21.45 -10 4 2 952.78 21.03 10 -4 -1 5.84 3.45 -10 4 1 7.85 3.40 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11 -13 -1 7.13 5.23 11 -13 0 11.56 5.48 11 -13 1 37.14 7.22 11 -13 2 22.18 6.53 11 -13 3 106.49 11.10 11 -13 4 73.85 9.46 11 -13 5 158.67 13.19 11 -13 6 55.77 8.82 11 -13 7 164.92 13.75 11 -13 8 9.26 4.84 11 -13 9 85.25 9.87 11 -13 10 48.32 7.96 11 -13 11 17.63 5.55 11 -13 12 103.18 10.97 11 -13 13 3.36 4.33 11 -13 14 0.70 4.40 11 -13 15 0.89 4.57 11 -13 16 2.88 5.01 11 -13 17 4.40 5.12 11 -12 -12 43.30 8.69 11 -12 -11 5.46 6.17 11 -12 -10 86.14 11.19 11 -12 -9 11.29 6.10 11 -12 -8 1.31 5.42 11 -12 -7 10.12 6.08 11 -12 -6 1.92 5.23 11 -12 -5 10.15 5.89 11 -12 -4 21.19 7.44 11 -12 -3 15.87 6.09 11 -12 -2 37.71 7.61 11 -12 -1 13.35 5.39 11 -12 0 1.58 4.51 11 -12 1 34.53 6.93 11 -12 2 18.90 6.00 11 -12 3 58.67 8.25 11 -12 4 36.10 7.42 11 -12 5 163.85 12.67 11 -12 6 78.24 9.74 11 -12 7 25.16 6.27 11 -12 8 17.60 5.97 11 -12 9 37.11 7.20 11 -12 10 107.57 10.87 11 -12 11 39.73 7.47 11 -12 12 13.96 5.76 11 -12 13 8.88 4.98 11 -12 14 4.75 4.21 11 -12 15 9.10 4.91 11 -12 16 3.66 4.74 11 -12 17 0.84 4.32 11 -12 18 5.03 4.77 11 -11 -14 8.39 6.14 11 -11 -13 92.27 11.60 11 -11 -12 -3.64 5.41 11 -11 -11 214.54 16.30 11 -11 -10 4.73 6.04 11 -11 -9 394.59 20.84 11 -11 -8 244.99 16.82 11 -11 -7 66.19 9.70 11 -11 -6 233.39 15.77 11 -11 -5 24.93 6.94 11 -11 -4 87.23 10.94 11 -11 -3 101.11 10.89 11 -11 -2 289.03 16.84 11 -11 -1 154.75 12.60 11 -11 0 216.08 14.50 11 -11 1 278.00 15.98 11 -11 2 668.25 23.88 11 -11 3 230.76 14.70 11 -11 4 387.49 13.27 11 -11 4 404.89 18.51 11 -11 5 21.70 3.93 11 -11 5 24.57 6.03 11 -11 6 91.94 9.72 11 -11 7 33.00 6.92 11 -11 8 54.87 8.14 11 -11 9 71.56 9.07 11 -11 10 17.38 5.24 11 -11 11 16.31 6.07 11 -11 12 2.62 4.04 11 -11 13 4.29 4.31 11 -11 14 3.59 4.33 11 -11 15 4.88 4.57 11 -11 16 4.09 4.76 11 -11 17 -0.23 4.13 11 -10 -16 43.78 8.63 11 -10 -15 1.24 5.39 11 -10 -14 86.91 11.29 11 -10 -13 -1.21 5.31 11 -10 -12 77.18 10.27 11 -10 -11 0.28 5.12 11 -10 -10 104.62 11.56 11 -10 -9 11.79 6.52 11 -10 -8 163.66 13.36 11 -10 -7 6.26 5.22 11 -10 -6 3.12 4.78 11 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9.95 11 -9 4 92.95 7.63 11 -9 4 96.23 9.00 11 -9 5 113.32 9.86 11 -9 5 104.03 8.17 11 -9 6 23.34 5.02 11 -9 6 18.69 4.21 11 -9 7 22.35 4.35 11 -9 7 23.45 5.24 11 -9 8 4.18 3.27 11 -9 8 9.34 4.35 11 -9 9 -1.26 3.26 11 -9 9 4.46 3.67 11 -9 10 16.37 4.06 11 -9 10 18.06 4.74 11 -9 11 0.31 3.41 11 -9 11 -2.44 3.26 11 -9 12 53.12 6.04 11 -9 12 46.80 6.56 11 -9 13 -0.16 3.87 11 -9 13 0.79 3.33 11 -9 14 4.27 3.69 11 -9 15 29.40 5.93 11 -8 -18 3.27 6.27 11 -8 -18 -0.94 5.20 11 -8 -17 98.08 11.65 11 -8 -17 104.19 11.95 11 -8 -16 13.69 6.20 11 -8 -16 8.95 5.77 11 -8 -15 67.94 9.68 11 -8 -15 68.56 9.94 11 -8 -14 12.07 5.65 11 -8 -14 9.48 5.47 11 -8 -13 8.38 5.15 11 -8 -12 -3.73 6.07 11 -8 -11 81.12 9.56 11 -8 -10 10.41 5.63 11 -8 -9 54.89 8.64 11 -8 -8 44.33 7.46 11 -8 -7 5.74 5.03 11 -8 -6 102.19 10.18 11 -8 -5 57.39 8.77 11 -8 -4 6.97 4.71 11 -8 -3 96.65 9.27 11 -8 -2 99.46 9.04 11 -8 -1 174.29 11.42 11 -8 0 86.05 8.71 11 -8 1 63.02 7.40 11 -8 2 64.39 7.46 11 -8 3 12.13 4.58 11 -8 4 84.65 8.11 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36.51 6.11 11 -3 -6 11.55 4.28 11 -3 -5 595.84 18.08 11 -3 -4 23.24 4.55 11 -3 -3 165.48 9.90 11 -3 -2 14.67 3.94 -11 3 2 7.82 3.13 11 -3 -1 49.20 5.77 -11 3 1 41.31 4.85 11 -3 0 85.84 6.63 -11 3 0 84.59 6.28 11 -3 1 39.17 6.79 -11 3 -1 38.05 4.45 11 -3 1 41.80 4.94 11 -3 2 184.74 11.76 -11 3 -2 192.54 8.22 11 -3 2 185.37 8.75 11 -3 3 59.16 7.61 11 -3 3 60.05 5.15 11 -3 4 309.46 10.31 11 -3 4 321.78 15.66 11 -3 5 218.76 12.91 11 -3 5 208.67 8.10 11 -3 6 55.65 7.27 11 -3 6 55.68 4.44 11 -3 7 110.09 9.74 11 -3 8 21.85 5.92 11 -3 9 58.80 7.92 11 -3 10 6.75 5.54 11 -3 11 0.60 4.28 11 -3 12 23.17 5.93 11 -3 13 -2.80 4.48 11 -3 14 4.01 4.92 11 -3 15 1.08 4.72 11 -3 16 63.95 9.46 11 -3 17 4.31 6.08 11 -2 -21 3.62 5.74 11 -2 -20 77.18 10.66 11 -2 -19 78.97 10.62 11 -2 -18 48.05 9.05 11 -2 -17 114.03 11.90 11 -2 -16 18.03 6.28 11 -2 -15 159.16 12.60 11 -2 -14 54.16 8.05 11 -2 -13 9.47 5.05 11 -2 -12 47.61 7.28 11 -2 -11 6.44 4.67 11 -2 -10 9.89 4.26 11 -2 -9 -1.67 4.00 11 -2 -8 -1.12 3.91 11 -2 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6.10 11 0 0 53.43 7.82 11 0 0 52.03 4.49 11 0 1 70.15 4.71 11 0 1 68.84 8.56 11 0 2 25.08 5.81 11 0 3 62.46 8.12 11 0 4 118.67 11.04 11 0 5 5.86 5.23 11 0 6 124.53 11.15 11 0 7 2.30 4.83 11 0 8 88.53 10.74 11 0 9 -1.16 4.92 11 0 10 77.64 10.03 11 0 11 3.05 5.31 11 0 12 111.16 11.85 11 0 13 15.33 6.34 11 1 -21 131.24 13.86 11 1 -20 13.15 6.67 11 1 -19 44.31 8.28 11 1 -18 -3.84 5.47 11 1 -17 22.65 6.15 11 1 -16 -4.79 5.64 11 1 -15 -5.28 5.36 11 1 -14 43.96 7.13 11 1 -13 15.86 5.01 11 1 -12 58.39 7.56 11 1 -11 2.12 3.87 11 1 -10 44.72 6.29 11 1 -9 110.69 8.90 11 1 -8 -0.32 3.31 11 1 -7 48.97 5.91 11 1 -6 15.44 4.08 11 1 -5 14.10 3.87 11 1 -4 154.93 8.40 11 1 -3 19.54 5.76 11 1 -3 29.26 4.11 11 1 -2 12.12 2.88 11 1 -2 9.52 5.05 11 1 -1 30.59 7.00 11 1 0 55.37 8.06 11 1 1 72.06 8.73 11 1 2 6.25 4.84 11 1 3 3.32 5.06 11 1 4 -4.34 5.11 11 1 5 4.88 4.69 11 1 6 3.48 5.03 11 1 7 5.77 4.89 11 1 8 6.13 5.23 11 1 9 0.96 4.83 11 1 10 -1.01 5.52 11 1 11 36.93 7.89 11 1 12 -0.95 5.30 11 2 -21 7.32 6.11 11 2 -20 79.97 10.96 11 2 -19 8.62 5.72 11 2 -18 102.84 11.46 11 2 -17 8.84 5.33 11 2 -16 -6.06 5.58 11 2 -15 -6.25 5.62 11 2 -14 -4.88 5.06 11 2 -13 19.43 5.68 11 2 -12 4.20 4.22 11 2 -11 -0.77 4.20 11 2 -10 29.13 5.87 11 2 -9 25.92 5.49 11 2 -8 149.40 9.88 11 2 -7 26.93 5.12 11 2 -6 44.16 5.46 11 2 -5 68.99 6.37 11 2 -4 30.56 6.44 11 2 -4 42.06 5.02 11 2 -3 3.78 5.04 11 2 -3 12.95 3.38 11 2 -2 51.88 7.86 11 2 -1 40.11 7.58 11 2 0 124.29 11.19 11 2 1 132.46 11.78 11 2 2 94.66 10.54 11 2 3 77.70 9.53 11 2 4 17.38 6.95 11 2 5 42.54 8.01 11 2 6 44.53 8.53 11 2 7 66.45 9.31 11 2 8 7.20 5.71 11 2 9 33.46 7.59 11 2 10 33.69 7.94 11 3 -20 -3.69 6.08 11 3 -19 2.47 5.33 11 3 -18 3.29 5.32 11 3 -17 -2.63 5.54 11 3 -16 -2.67 5.23 11 3 -15 -1.40 4.54 11 3 -14 -3.48 4.77 11 3 -13 3.05 4.24 11 3 -12 4.17 4.52 11 3 -11 58.28 7.53 11 3 -10 47.80 6.93 11 3 -9 86.18 8.15 11 3 -8 78.46 7.85 11 3 -7 160.64 10.17 11 3 -6 39.61 5.61 11 3 -6 39.60 7.94 11 3 -5 1.35 4.57 11 3 -5 1.25 2.77 11 3 -4 2.72 4.82 11 3 -3 14.84 5.99 11 3 -2 0.48 4.80 11 3 -1 4.93 4.97 11 3 0 52.83 8.07 11 3 1 12.88 6.18 11 3 2 93.11 10.41 11 3 3 7.55 5.66 11 3 4 83.73 10.39 11 3 5 31.36 7.69 11 3 6 56.56 8.89 11 3 7 6.25 5.74 11 3 8 14.15 6.80 11 4 -20 12.79 6.35 11 4 -19 -0.12 5.89 11 4 -18 4.62 4.88 11 4 -17 -1.74 5.11 11 4 -16 3.99 4.72 11 4 -15 2.39 4.63 11 4 -14 50.45 7.77 11 4 -13 46.16 7.71 11 4 -12 69.81 8.60 11 4 -11 28.51 6.01 11 4 -10 33.58 6.09 11 4 -9 10.91 4.87 11 4 -8 9.23 3.71 11 4 -7 79.34 7.25 11 4 -7 78.91 9.86 11 4 -6 65.46 9.25 11 4 -5 65.61 9.31 11 4 -4 33.66 7.05 11 4 -3 22.52 6.69 11 4 -2 20.28 6.56 11 4 -1 4.73 4.93 11 4 0 4.93 5.32 11 4 1 -3.17 5.63 11 4 2 -2.09 5.06 11 4 3 0.41 5.48 11 4 4 34.66 7.92 11 4 5 46.29 8.58 11 4 6 14.50 6.16 11 5 -19 -17.36 6.82 11 5 -18 -6.26 6.13 11 5 -17 2.44 5.15 11 5 -16 22.31 6.55 11 5 -15 -1.65 5.10 11 5 -14 0.71 4.52 11 5 -13 46.81 7.88 11 5 -12 45.84 7.77 11 5 -11 21.11 6.16 11 5 -10 81.18 9.08 11 5 -9 7.37 5.52 11 5 -8 49.17 7.73 11 5 -7 10.73 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140.64 10.52 13 -9 3 153.83 11.36 13 -9 4 8.52 4.51 13 -9 4 6.23 4.17 13 -9 5 145.60 10.85 13 -9 5 141.76 10.32 13 -9 6 -0.86 3.58 13 -9 6 0.96 3.69 13 -9 7 55.40 7.25 13 -9 7 65.81 7.69 13 -9 8 32.14 6.16 13 -9 8 29.21 5.91 13 -9 9 215.99 12.81 13 -9 9 318.65 15.16 13 -9 10 37.12 6.47 13 -9 10 29.04 5.55 13 -9 11 13.16 4.66 13 -8 -16 -4.81 6.19 13 -8 -15 58.35 9.89 13 -8 -15 53.71 9.56 13 -8 -14 0.42 5.26 13 -8 -13 65.22 9.83 13 -8 -12 86.82 10.82 13 -8 -11 35.94 7.69 13 -8 -10 -1.88 5.58 13 -8 -9 21.41 6.29 13 -8 -8 -3.85 5.57 13 -8 -7 2.58 4.49 13 -8 -6 9.79 5.26 13 -8 -5 1.33 4.39 13 -8 -4 2.56 4.29 13 -8 -3 80.31 9.02 13 -8 -2 13.27 5.30 13 -8 -1 3.29 4.27 13 -8 0 -0.11 3.68 13 -8 1 94.89 9.07 13 -8 2 19.42 5.56 13 -8 2 24.47 5.89 13 -8 3 117.17 9.99 13 -8 3 126.45 10.24 13 -8 4 3.25 3.94 13 -8 4 10.06 4.30 13 -8 5 136.90 10.08 13 -8 5 133.07 10.27 13 -8 6 20.55 5.10 13 -8 6 21.32 4.93 13 -8 7 2.97 3.89 13 -8 7 7.57 4.03 13 -8 8 38.21 5.76 13 -8 8 41.42 6.65 13 -8 9 0.89 3.96 13 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4.84 4.46 13 -5 -9 4.67 4.87 13 -5 -8 15.61 5.30 13 -5 -8 12.57 4.90 13 -5 -7 38.43 7.03 13 -5 -6 120.31 10.37 13 -5 -5 293.52 15.16 13 -5 -4 6.05 4.40 13 -5 -3 290.23 14.43 13 -5 -2 19.20 4.99 13 -5 -1 14.98 4.32 13 -5 0 7.99 3.46 13 -5 1 60.26 6.78 13 -5 1 61.51 8.23 13 -5 2 16.67 5.69 13 -5 2 17.95 4.50 13 -5 3 40.74 7.00 13 -5 3 44.81 5.38 13 -5 4 -2.22 4.47 13 -5 4 -0.36 2.96 13 -5 5 0.40 3.97 13 -5 6 9.73 4.79 13 -5 7 4.37 4.79 13 -5 8 7.68 4.74 13 -5 9 16.71 5.98 13 -5 10 -2.26 5.04 13 -5 11 -2.25 4.77 13 -5 12 1.18 4.57 13 -5 13 1.52 4.51 13 -5 14 11.92 5.61 13 -5 15 -0.36 4.90 13 -4 -19 60.69 9.88 13 -4 -18 1.52 5.27 13 -4 -17 35.74 7.84 13 -4 -16 -3.87 6.12 13 -4 -15 17.25 5.83 13 -4 -14 7.22 4.73 13 -4 -13 28.01 6.82 13 -4 -12 -0.29 4.44 13 -4 -11 2.81 4.40 13 -4 -10 9.69 5.57 13 -4 -9 6.32 4.23 13 -4 -8 98.03 9.18 13 -4 -7 21.60 5.48 13 -4 -6 119.52 9.92 13 -4 -6 126.95 9.76 13 -4 -5 62.84 7.54 13 -4 -4 179.21 11.45 13 -4 -3 102.68 8.83 13 -4 -2 118.03 9.06 13 -4 -1 249.35 12.45 13 -4 0 241.22 15.22 13 -4 0 224.56 11.37 13 -4 1 168.01 12.87 13 -4 1 156.65 9.59 13 -4 2 73.41 9.23 13 -4 2 81.57 7.01 13 -4 3 0.94 5.02 13 -4 3 5.57 2.99 13 -4 4 6.75 5.15 13 -4 5 3.60 4.75 13 -4 6 48.65 7.89 13 -4 7 50.10 7.73 13 -4 8 16.39 6.82 13 -4 9 4.00 5.15 13 -4 10 76.70 10.10 13 -4 11 8.03 5.26 13 -4 12 -1.44 5.14 13 -4 13 -2.23 5.21 13 -4 14 0.12 4.72 13 -3 -19 -3.18 5.98 13 -3 -18 2.87 5.72 13 -3 -17 4.66 5.60 13 -3 -16 42.78 7.90 13 -3 -15 83.20 10.22 13 -3 -14 0.72 4.67 13 -3 -13 4.39 4.93 13 -3 -12 0.02 4.24 13 -3 -11 27.59 6.12 13 -3 -10 8.12 4.83 13 -3 -9 1.79 4.14 13 -3 -8 11.20 4.57 13 -3 -7 23.48 5.38 13 -3 -6 46.13 6.36 13 -3 -5 4.37 3.54 13 -3 -5 11.69 4.25 13 -3 -4 7.79 4.04 13 -3 -3 94.57 7.95 13 -3 -2 101.34 8.10 13 -3 -1 186.98 10.52 13 -3 -1 191.74 14.01 13 -3 0 50.93 8.13 13 -3 0 51.42 5.91 13 -3 1 112.42 10.89 13 -3 1 118.29 7.89 13 -3 2 6.75 4.94 13 -3 3 8.38 5.20 13 -3 4 43.33 7.30 13 -3 5 73.97 9.33 13 -3 6 288.18 17.10 13 -3 7 43.83 8.91 13 -3 8 8.79 5.43 13 -3 9 160.28 13.60 13 -3 10 46.94 8.14 13 -3 11 27.31 7.07 13 -3 12 0.99 4.98 13 -3 13 -1.66 5.10 13 -2 -19 6.66 5.66 13 -2 -18 2.87 5.60 13 -2 -17 4.84 5.55 13 -2 -16 35.63 7.40 13 -2 -15 9.90 6.28 13 -2 -14 5.34 5.38 13 -2 -13 14.29 6.08 13 -2 -12 4.03 4.52 13 -2 -11 2.03 4.41 13 -2 -10 23.00 5.56 13 -2 -9 107.28 9.39 13 -2 -8 4.59 4.24 13 -2 -7 93.08 8.33 13 -2 -6 31.45 5.41 13 -2 -5 9.85 3.83 13 -2 -4 12.91 4.13 13 -2 -3 25.24 4.61 13 -2 -2 73.48 6.76 13 -2 -1 -0.82 2.99 13 -2 -1 0.40 4.85 13 -2 0 6.89 5.05 13 -2 1 1.53 5.06 13 -2 2 19.11 6.13 13 -2 3 10.92 5.37 13 -2 4 26.92 6.79 13 -2 5 114.83 11.21 13 -2 6 10.24 5.54 13 -2 7 3.96 4.98 13 -2 8 96.87 10.67 13 -2 9 25.99 6.99 13 -2 10 47.34 8.22 13 -2 11 -3.03 5.00 13 -1 -19 86.32 11.21 13 -1 -18 5.03 5.64 13 -1 -17 6.72 5.45 13 -1 -16 23.66 6.93 13 -1 -15 23.48 6.68 13 -1 -14 48.31 8.16 13 -1 -13 3.32 4.70 13 -1 -12 29.65 6.90 13 -1 -11 0.62 4.07 13 -1 -10 29.14 6.10 13 -1 -9 8.77 4.46 13 -1 -8 0.47 3.43 13 -1 -7 15.23 4.52 13 -1 -6 5.37 3.86 13 -1 -5 153.03 9.52 13 -1 -4 6.80 3.57 13 -1 -3 7.07 3.25 13 -1 -2 18.29 6.36 13 -1 -1 20.12 6.29 13 -1 0 70.07 9.67 13 -1 1 20.63 6.40 13 -1 2 30.04 7.05 13 -1 3 33.12 7.47 13 -1 4 42.87 7.88 13 -1 5 2.56 5.32 13 -1 6 40.40 7.70 13 -1 7 13.62 6.15 13 -1 8 11.48 5.61 13 -1 9 -4.32 6.51 13 0 -19 8.73 5.93 13 0 -18 5.98 5.29 13 0 -17 4.12 5.57 13 0 -16 6.56 5.37 13 0 -15 7.91 5.65 13 0 -14 0.97 4.66 13 0 -13 46.63 7.81 13 0 -12 9.23 5.02 13 0 -11 84.83 9.00 13 0 -10 32.30 6.17 13 0 -9 29.26 5.69 13 0 -8 29.78 5.61 13 0 -7 0.51 3.40 13 0 -6 127.25 8.62 13 0 -4 77.63 10.07 13 0 -3 15.25 5.99 13 0 -2 86.03 10.31 13 0 -1 5.59 5.67 13 0 0 82.83 10.19 13 0 1 6.36 5.47 13 0 2 65.31 9.11 13 0 3 78.42 10.71 13 0 4 26.40 7.76 13 0 5 132.78 12.82 13 0 6 -6.55 6.13 13 0 7 55.36 9.02 13 1 -19 41.07 8.40 13 1 -18 5.42 5.35 13 1 -17 2.07 5.06 13 1 -16 8.84 5.04 13 1 -15 4.81 5.04 13 1 -14 14.72 5.78 13 1 -13 4.24 4.75 13 1 -12 15.57 5.72 13 1 -11 3.83 4.47 13 1 -10 24.82 6.22 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16 -11 0 21.89 6.62 16 -11 1 -1.37 4.48 16 -11 2 -0.13 4.52 16 -11 3 4.93 5.07 16 -11 4 12.93 5.87 16 -10 -6 34.08 7.89 16 -10 -5 10.16 5.82 16 -10 -4 16.61 6.36 16 -10 -3 7.84 5.52 16 -10 -2 5.08 4.99 16 -10 -1 28.12 6.81 16 -10 0 2.85 4.91 16 -10 1 48.76 7.97 16 -10 1 44.79 7.77 16 -10 2 31.51 6.65 16 -10 2 31.34 6.75 16 -10 3 56.41 8.23 16 -10 3 56.48 8.50 16 -9 -8 16.60 6.99 16 -9 -7 55.57 9.50 16 -9 -6 35.11 7.88 16 -9 -5 2.06 4.97 16 -9 -4 36.42 7.72 16 -9 -3 14.75 6.52 16 -9 -2 110.69 11.22 16 -9 -1 4.87 5.25 16 -9 0 118.98 12.06 16 -9 0 128.33 11.53 16 -9 1 70.89 9.48 16 -9 1 72.26 8.97 16 -9 2 50.73 8.55 16 -9 3 45.85 7.76 16 -9 4 2.07 4.59 16 -9 5 37.30 7.15 16 -9 6 1.54 4.71 16 -9 7 60.35 8.67 16 -8 -10 -1.31 5.59 16 -8 -9 -3.92 5.96 16 -8 -8 -2.42 5.51 16 -8 -7 -2.53 5.46 16 -8 -6 12.09 5.60 16 -8 -5 14.52 5.63 16 -8 -4 3.60 4.62 16 -8 -3 4.18 4.40 16 -8 -2 2.72 4.26 16 -8 -1 23.77 6.34 16 -8 0 0.98 5.14 16 -8 0 -0.48 3.96 16 -8 1 11.90 6.25 16 -8 2 14.93 6.02 16 -8 3 8.73 5.34 16 -8 4 -0.45 4.55 16 -8 5 -3.06 5.30 16 -8 6 22.26 6.57 16 -8 7 10.72 5.52 16 -8 8 41.37 7.96 16 -8 9 -4.53 5.73 16 -7 -11 2.23 5.51 16 -7 -10 4.21 5.07 16 -7 -9 16.59 6.64 16 -7 -8 -1.60 4.92 16 -7 -7 28.66 7.04 16 -7 -6 -4.55 5.49 16 -7 -5 26.13 6.37 16 -7 -4 -3.15 4.82 16 -7 -3 0.43 5.05 16 -7 -2 47.60 7.46 16 -7 -1 6.51 5.92 16 -7 0 14.91 6.01 16 -7 1 -0.09 5.08 16 -7 2 9.40 5.45 16 -7 3 -2.76 4.62 16 -7 4 -6.38 5.29 16 -7 5 2.79 4.95 16 -7 6 1.33 4.68 16 -7 7 2.62 5.17 16 -6 -13 5.94 5.54 16 -6 -12 12.06 6.88 16 -6 -11 7.32 5.67 16 -6 -10 2.19 4.98 16 -6 -9 24.38 6.89 16 -6 -8 73.29 9.68 16 -6 -7 128.81 12.07 16 -6 -6 23.51 6.48 16 -6 -5 24.99 6.04 16 -6 -4 8.09 4.70 16 -6 -3 58.73 7.87 16 -6 -1 20.69 6.80 16 -6 0 39.06 7.96 16 -6 1 3.25 5.68 16 -6 2 14.89 6.41 16 -6 3 6.06 5.17 16 -6 4 -3.99 5.39 16 -6 5 11.32 6.45 16 -5 -14 -3.76 5.52 16 -5 -13 1.55 4.90 16 -5 -12 0.10 4.82 16 -5 -12 2.28 5.24 16 -5 -11 11.67 6.39 16 -5 -11 2.21 5.04 16 -5 -10 85.69 10.64 16 -5 -9 8.53 5.73 16 -5 -8 69.16 9.52 16 -5 -7 27.57 6.93 16 -5 -6 46.60 7.84 16 -5 -5 1.73 4.26 16 -5 -2 23.91 7.60 16 -5 -1 24.70 7.98 16 -5 0 -5.24 5.57 16 -5 1 22.42 7.33 16 -5 2 0.27 5.58 16 -4 -14 8.73 5.59 16 -4 -13 -0.25 4.73 16 -4 -12 2.21 4.94 16 -4 -11 43.78 7.97 16 -4 -10 15.83 6.20 16 -4 -10 17.30 6.01 16 -4 -9 64.63 9.18 16 -4 -8 30.21 6.82 16 -4 -7 13.98 5.47 16 -3 -15 -1.12 5.39 16 -3 -14 3.56 4.87 16 -3 -13 0.64 4.81 16 -3 -12 -2.66 4.99 16 -3 -9 28.27 6.73 16 -2 -15 -0.18 5.00 17 -11 0 13.59 6.26 17 -11 1 24.52 6.79 17 -10 -3 34.55 7.98 17 -10 -2 44.46 8.25 17 -10 -1 -2.06 5.12 17 -10 0 18.73 6.52 17 -10 1 4.70 5.06 17 -10 2 8.89 5.67 17 -9 -6 79.84 10.61 17 -9 -5 -0.07 4.86 17 -9 -4 66.39 9.89 17 -9 -3 55.87 9.00 17 -9 -2 20.50 6.33 17 -9 -1 46.53 8.69 17 -9 0 4.81 5.15 17 -9 1 2.12 4.85 17 -9 2 1.78 5.03 17 -9 3 5.23 4.97 17 -9 4 10.55 5.37 17 -8 -7 30.27 7.40 17 -8 -6 0.01 4.87 17 -8 -5 4.23 5.32 17 -8 -4 -4.08 4.89 17 -8 -3 11.72 5.67 17 -7 -9 12.73 6.36 17 -7 -8 3.54 5.31 17 -7 -7 -0.95 5.07 17 -7 -6 15.62 6.06 17 -7 -5 -3.79 4.79 17 -6 -10 34.11 7.98 17 -6 -9 21.27 6.93 17 -6 -8 -1.48 4.87 17 -6 -7 51.97 8.64 17 -5 -10 5.66 5.46 17 -5 -9 16.81 6.30 17 -4 -11 -1.31 5.56 0 0 0 0.00 0.00 TITL MRC2111 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 13.395717 13.435330 22.674365 99.1364 97.0781 112.6273 ZERR 3.00 0.000982 0.000789 0.000840 0.0039 0.0043 0.0062 LATT 1 SFAC C H N Mg Fe UNIT 189.00 252.00 12.00 6.00 3.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 60133 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.136 _oxdiff_exptl_absorpt_empirical_full_min 0.892 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_3f _database_code_depnum_ccdc_archive 'CCDC 2116007' loop_ _audit_author_name _audit_author_address 'Andrew White' ;Imperial College London United Kingdom ; _audit_update_record ; 2021-10-15 deposited with the CCDC. 2022-05-16 downloaded from the CCDC. ; _audit_creation_method SHELXL-2018/3 _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C70 H99 Co Mg2 N4 O2, 2(C7 H8)' _chemical_formula_sum 'C84 H115 Co Mg2 N4 O2' _chemical_formula_weight 1320.34 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.1719 0.1771 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.9878(4) _cell_length_b 13.5935(8) _cell_length_c 41.687(3) _cell_angle_alpha 90 _cell_angle_beta 92.375(5) _cell_angle_gamma 90 _cell_volume 7919.7(7) _cell_formula_units_Z 4 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 3008 _cell_measurement_theta_min 4.2540 _cell_measurement_theta_max 57.2730 _exptl_crystal_description 'tabular needles' _exptl_crystal_colour Orange _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.107 _exptl_crystal_F_000 2856 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.356 _exptl_crystal_size_mid 0.174 _exptl_crystal_size_min 0.039 _exptl_absorpt_coefficient_mu 2.199 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type analytical _exptl_absorpt_correction_T_min 0.625 _exptl_absorpt_correction_T_max 0.932 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'Enhance Ultra (Cu) X-ray Source' _diffrn_measurement_device_type 'Agilent Xcalibur PX Ultra A' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean 10.4115 _diffrn_reflns_number 27095 _diffrn_reflns_av_unetI/netI 0.1164 _diffrn_reflns_av_R_equivalents 0.0786 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -51 _diffrn_reflns_limit_l_max 50 _diffrn_reflns_theta_min 3.420 _diffrn_reflns_theta_max 73.718 _diffrn_reflns_theta_full 67.684 _diffrn_measured_fraction_theta_max 0.947 _diffrn_measured_fraction_theta_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.947 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.947 _diffrn_reflns_point_group_measured_fraction_full 0.988 _reflns_number_total 15158 _reflns_number_gt 8175 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro, Rigaku OD' _computing_cell_refinement 'CrysAlisPro, Rigaku OD' _computing_data_reduction 'CrysAlisPro, Rigaku OD' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2017)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2017)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0841P)^2^+10.3103P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 15158 _refine_ls_number_parameters 917 _refine_ls_number_restraints 362 _refine_ls_R_factor_all 0.1655 _refine_ls_R_factor_gt 0.1004 _refine_ls_wR_factor_ref 0.2711 _refine_ls_wR_factor_gt 0.2251 _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_restrained_S_all 1.035 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.19838(6) 0.28026(8) 0.71795(2) 0.0476(3) Uani 1 1 d . . . . . Mg1 Mg 0.20758(11) 0.43328(13) 0.62004(4) 0.0375(4) Uani 1 1 d . . . . . Mg2 Mg 0.38913(11) 0.25939(13) 0.63754(4) 0.0404(4) Uani 1 1 d . . . . . H1 H 0.305(3) 0.352(4) 0.6220(12) 0.043(14) Uiso 1 1 d . . . . . N1 N 0.2019(3) 0.5797(3) 0.63061(10) 0.0405(10) Uani 1 1 d . . . . . C1 C 0.1936(3) 0.6456(4) 0.60697(13) 0.0405(12) Uani 1 1 d . . . . . C2 C 0.1716(4) 0.6229(4) 0.57503(13) 0.0437(13) Uani 1 1 d . . . . . H2A H 0.180191 0.675283 0.560350 0.052 Uiso 1 1 calc R U . . . C3 C 0.1387(3) 0.5347(4) 0.56105(13) 0.0406(12) Uani 1 1 d . . . . . N3 N 0.1410(3) 0.4481(3) 0.57587(10) 0.0384(10) Uani 1 1 d . . . . . C4 C 0.2049(5) 0.7542(4) 0.61451(15) 0.0546(15) Uani 1 1 d . . . . . H4A H 0.142303 0.782380 0.618986 0.082 Uiso 1 1 calc R U . . . H4B H 0.231158 0.788047 0.596078 0.082 Uiso 1 1 calc R U . . . H4C H 0.248422 0.762474 0.633341 0.082 Uiso 1 1 calc R U . . . C5 C 0.0960(5) 0.5428(5) 0.52723(15) 0.0616(17) Uani 1 1 d . . . . . H5A H 0.111359 0.483455 0.515123 0.092 Uiso 1 1 calc R U . . . H5B H 0.122586 0.600534 0.516704 0.092 Uiso 1 1 calc R U . . . H5C H 0.026380 0.549656 0.527944 0.092 Uiso 1 1 calc R U . . . C6 C 0.2009(3) 0.6131(4) 0.66310(12) 0.0374(11) Uani 1 1 d . . . . . C7 C 0.1123(3) 0.6436(4) 0.67613(13) 0.0421(12) Uani 1 1 d . . . . . C8 C 0.1129(4) 0.6701(5) 0.70775(13) 0.0493(14) Uani 1 1 d . . . . . H8A H 0.054411 0.689582 0.716635 0.059 Uiso 1 1 calc R U . . . C9 C 0.1952(4) 0.6699(5) 0.72740(14) 0.0514(14) Uani 1 1 d . . . . . H9A H 0.193102 0.689586 0.749227 0.062 Uiso 1 1 calc R U . . . C10 C 0.2808(4) 0.6403(5) 0.71463(14) 0.0512(14) Uani 1 1 d . . . . . H10A H 0.337471 0.639174 0.728011 0.061 Uiso 1 1 calc R U . . . C11 C 0.2851(3) 0.6125(4) 0.68283(13) 0.0423(13) Uani 1 1 d . . . . . C12 C 0.0191(4) 0.6447(5) 0.65578(14) 0.0478(14) Uani 1 1 d . . . . . H12A H 0.034965 0.637128 0.632742 0.057 Uiso 1 1 calc R U . . . C13 C -0.0428(4) 0.5577(6) 0.66501(19) 0.072(2) Uani 1 1 d . . . . . H13A H -0.008293 0.496261 0.661366 0.108 Uiso 1 1 calc R U . . . H13B H -0.102548 0.558218 0.651869 0.108 Uiso 1 1 calc R U . . . H13C H -0.057415 0.562751 0.687747 0.108 Uiso 1 1 calc R U . . . C14 C -0.0350(5) 0.7412(6) 0.65938(18) 0.073(2) Uani 1 1 d . . . . . H14A H -0.055689 0.747458 0.681472 0.109 Uiso 1 1 calc R U . . . H14B H -0.091207 0.741886 0.644528 0.109 Uiso 1 1 calc R U . . . H14C H 0.006997 0.796424 0.654467 0.109 Uiso 1 1 calc R U . . . C15 C 0.3804(4) 0.5840(5) 0.66949(14) 0.0531(15) Uani 1 1 d . . . . . H15A H 0.366817 0.546427 0.649188 0.064 Uiso 1 1 calc R U . . . C16 C 0.4365(5) 0.6739(7) 0.6611(3) 0.111(4) Uani 1 1 d . . . . . H16A H 0.451483 0.712015 0.680639 0.167 Uiso 1 1 calc R U . . . H16B H 0.398560 0.714367 0.645868 0.167 Uiso 1 1 calc R U . . . H16C H 0.496072 0.653987 0.651388 0.167 Uiso 1 1 calc R U . . . C17 C 0.4394(5) 0.5191(6) 0.6917(2) 0.086(2) Uani 1 1 d . . . . . H17A H 0.491485 0.489544 0.680016 0.129 Uiso 1 1 calc R U . . . H17B H 0.398907 0.466899 0.700081 0.129 Uiso 1 1 calc R U . . . H17C H 0.466268 0.558349 0.709647 0.129 Uiso 1 1 calc R U . . . C18 C 0.0980(3) 0.3647(4) 0.55915(12) 0.0390(12) Uani 1 1 d . . . . . C19 C 0.1553(3) 0.3050(4) 0.53983(13) 0.0421(12) Uani 1 1 d . . . . . C20 C 0.1116(4) 0.2272(5) 0.52339(14) 0.0553(15) Uani 1 1 d . . . . . H20A H 0.148947 0.187410 0.509944 0.066 Uiso 1 1 calc R U . . . C21 C 0.0163(4) 0.2057(5) 0.52591(16) 0.0616(17) Uani 1 1 d . . . . . H21A H -0.012115 0.152412 0.514266 0.074 Uiso 1 1 calc R U . . . C22 C -0.0376(4) 0.2633(5) 0.54574(16) 0.0568(16) Uani 1 1 d . . . . . H22A H -0.103060 0.247390 0.548043 0.068 Uiso 1 1 calc R U . . . C23 C 0.0008(3) 0.3434(4) 0.56236(13) 0.0437(13) Uani 1 1 d . . . . . C24 C 0.2618(4) 0.3248(5) 0.53632(14) 0.0519(15) Uani 1 1 d . . . . . H24A H 0.281835 0.376628 0.552237 0.062 Uiso 1 1 calc R U . . . C25 C 0.2825(5) 0.3623(8) 0.5034(2) 0.108(4) Uani 1 1 d . . . . . H25A H 0.351861 0.366205 0.501132 0.162 Uiso 1 1 calc R U . . . H25B H 0.254306 0.427823 0.500345 0.162 Uiso 1 1 calc R U . . . H25C H 0.254781 0.317302 0.487127 0.162 Uiso 1 1 calc R U . . . C26 C 0.3211(4) 0.2334(5) 0.54360(18) 0.0691(19) Uani 1 1 d . . . . . H26A H 0.304406 0.182270 0.527789 0.104 Uiso 1 1 calc R U . . . H26B H 0.307988 0.209563 0.565163 0.104 Uiso 1 1 calc R U . . . H26C H 0.389202 0.249499 0.542568 0.104 Uiso 1 1 calc R U . . . C27 C -0.0618(4) 0.4031(5) 0.58410(15) 0.0508(14) Uani 1 1 d . . . . . H27A H -0.022297 0.458760 0.593066 0.061 Uiso 1 1 calc R U . . . C28 C -0.0948(4) 0.3421(5) 0.61230(16) 0.0644(18) Uani 1 1 d . . . . . H28A H -0.126862 0.282464 0.604204 0.097 Uiso 1 1 calc R U . . . H28B H -0.139427 0.380868 0.624678 0.097 Uiso 1 1 calc R U . . . H28C H -0.039241 0.323860 0.626125 0.097 Uiso 1 1 calc R U . . . C29 C -0.1488(5) 0.4478(6) 0.56545(18) 0.080(2) Uani 1 1 d . . . . . H29A H -0.126668 0.490796 0.548419 0.120 Uiso 1 1 calc R U . . . H29B H -0.187038 0.486117 0.580165 0.120 Uiso 1 1 calc R U . . . H29C H -0.188142 0.394828 0.555912 0.120 Uiso 1 1 calc R U . . . N31 N 0.3844(3) 0.1124(3) 0.62741(11) 0.0442(11) Uani 1 1 d . . . . . C31 C 0.4384(4) 0.0711(4) 0.60517(15) 0.0489(14) Uani 1 1 d . . . . . C32 C 0.5138(4) 0.1219(4) 0.59078(15) 0.0513(14) Uani 1 1 d . . . . . H32A H 0.539741 0.089452 0.572920 0.062 Uiso 1 1 calc R U . . . C33 C 0.5565(3) 0.2128(5) 0.59875(14) 0.0455(13) Uani 1 1 d . . . . . N33 N 0.5210(3) 0.2786(3) 0.61840(10) 0.0392(10) Uani 1 1 d . . . . . C34 C 0.4211(5) -0.0326(5) 0.5939(2) 0.073(2) Uani 1 1 d . . . . . H34A H 0.373920 -0.063923 0.607374 0.109 Uiso 1 1 calc R U . . . H34B H 0.481230 -0.069631 0.595600 0.109 Uiso 1 1 calc R U . . . H34C H 0.396869 -0.032003 0.571551 0.109 Uiso 1 1 calc R U . . . C35 C 0.6507(4) 0.2316(5) 0.58306(17) 0.0627(18) Uani 1 1 d . . . . . H35A H 0.657629 0.302200 0.578963 0.094 Uiso 1 1 calc R U . . . H35B H 0.651756 0.195604 0.562707 0.094 Uiso 1 1 calc R U . . . H35C H 0.703683 0.209174 0.597357 0.094 Uiso 1 1 calc R U . . . C36 C 0.3293(4) 0.0463(4) 0.64629(14) 0.0456(13) Uani 1 1 d . . . . . C37 C 0.3754(4) -0.0025(4) 0.67254(15) 0.0511(14) Uani 1 1 d . . . . . C38 C 0.3238(5) -0.0716(5) 0.68937(16) 0.0579(16) Uani 1 1 d . . . . . H38A H 0.355240 -0.108551 0.706014 0.070 Uiso 1 1 calc R U . . . C39 C 0.2271(5) -0.0874(5) 0.68227(16) 0.0574(16) Uani 1 1 d . . . . . H39A H 0.192794 -0.135152 0.693799 0.069 Uiso 1 1 calc R U . . . C40 C 0.1821(4) -0.0335(4) 0.65854(16) 0.0553(16) Uani 1 1 d . . . . . H40A H 0.115160 -0.041782 0.654639 0.066 Uiso 1 1 calc R U . . . C41 C 0.2310(4) 0.0337(4) 0.63972(15) 0.0497(14) Uani 1 1 d . . . . . C42 C 0.4805(4) 0.0185(5) 0.68197(18) 0.0672(19) Uani 1 1 d . . . . . H42A H 0.498676 0.080526 0.670860 0.081 Uiso 1 1 calc R U . . . C43 C 0.4962(6) 0.0347(9) 0.7164(2) 0.124(4) Uani 1 1 d . . . . . H43A H 0.483718 -0.026431 0.727978 0.186 Uiso 1 1 calc R U . . . H43B H 0.452842 0.086242 0.723465 0.186 Uiso 1 1 calc R U . . . H43C H 0.562605 0.055139 0.720903 0.186 Uiso 1 1 calc R U . . . C44 C 0.5457(6) -0.0614(9) 0.6708(3) 0.145(5) Uani 1 1 d . . . . . H44A H 0.611822 -0.037439 0.671649 0.218 Uiso 1 1 calc R U . . . H44B H 0.526909 -0.079902 0.648752 0.218 Uiso 1 1 calc R U . . . H44C H 0.540787 -0.118842 0.684874 0.218 Uiso 1 1 calc R U . . . C45 C 0.1790(4) 0.0882(5) 0.61270(16) 0.0559(16) Uani 1 1 d . . . . . H45A H 0.221678 0.142350 0.605654 0.067 Uiso 1 1 calc R U . . . C46 C 0.1574(6) 0.0220(7) 0.58390(19) 0.092(3) Uani 1 1 d . . . . . H46A H 0.216018 -0.011961 0.578095 0.138 Uiso 1 1 calc R U . . . H46B H 0.133415 0.061945 0.565720 0.138 Uiso 1 1 calc R U . . . H46C H 0.108909 -0.026581 0.589316 0.138 Uiso 1 1 calc R U . . . C47 C 0.0855(5) 0.1352(6) 0.6234(2) 0.080(2) Uani 1 1 d . . . . . H47A H 0.039012 0.083385 0.627742 0.121 Uiso 1 1 calc R U . . . H47B H 0.059390 0.178315 0.606373 0.121 Uiso 1 1 calc R U . . . H47C H 0.098480 0.173781 0.642970 0.121 Uiso 1 1 calc R U . . . C48 C 0.5759(3) 0.3649(4) 0.62575(13) 0.0422(13) Uani 1 1 d . . . . . C49 C 0.5685(3) 0.4487(4) 0.60605(14) 0.0449(13) Uani 1 1 d . . . . . C50 C 0.6226(4) 0.5311(5) 0.61454(15) 0.0515(14) Uani 1 1 d . . . . . H50A H 0.618369 0.587850 0.601258 0.062 Uiso 1 1 calc R U . . . C51 C 0.6817(4) 0.5327(5) 0.64150(16) 0.0563(16) Uani 1 1 d . . . . . H51A H 0.718153 0.589915 0.646710 0.068 Uiso 1 1 calc R U . . . C52 C 0.6881(4) 0.4511(5) 0.66107(16) 0.0588(17) Uani 1 1 d . . . . . H52A H 0.729461 0.452764 0.679733 0.071 Uiso 1 1 calc R U . . . C53 C 0.6355(4) 0.3662(5) 0.65414(14) 0.0483(14) Uani 1 1 d . . . . . C54 C 0.5042(4) 0.4497(5) 0.57566(15) 0.0524(15) Uani 1 1 d . . . . . H54A H 0.469749 0.385359 0.574005 0.063 Uiso 1 1 calc R U . . . C55 C 0.5622(5) 0.4630(7) 0.54551(17) 0.089(3) Uani 1 1 d . . . . . H55A H 0.518636 0.464482 0.526489 0.133 Uiso 1 1 calc R U . . . H55B H 0.607037 0.408056 0.543744 0.133 Uiso 1 1 calc R U . . . H55C H 0.597940 0.524942 0.547038 0.133 Uiso 1 1 calc R U . . . C56 C 0.4299(4) 0.5322(5) 0.57648(17) 0.0641(18) Uani 1 1 d . . . . . H56A H 0.462509 0.596066 0.577079 0.096 Uiso 1 1 calc R U . . . H56B H 0.392214 0.525019 0.595637 0.096 Uiso 1 1 calc R U . . . H56C H 0.387374 0.528483 0.557231 0.096 Uiso 1 1 calc R U . . . C57 C 0.6418(4) 0.2797(5) 0.67683(15) 0.0601(17) Uani 1 1 d . . . . . H57A H 0.590681 0.232227 0.669617 0.072 Uiso 1 1 calc R U . . . C58 C 0.6242(6) 0.3052(7) 0.71123(18) 0.097(3) Uani 1 1 d . . . . . H58A H 0.623647 0.244818 0.724078 0.146 Uiso 1 1 calc R U . . . H58B H 0.562372 0.338560 0.712393 0.146 Uiso 1 1 calc R U . . . H58C H 0.675204 0.348726 0.719605 0.146 Uiso 1 1 calc R U . . . C59 C 0.7374(7) 0.2257(7) 0.6750(2) 0.103(3) Uani 1 1 d . . . . . H59A H 0.789763 0.270522 0.681362 0.154 Uiso 1 1 calc R U . . . H59B H 0.745628 0.202958 0.653010 0.154 Uiso 1 1 calc R U . . . H59C H 0.738185 0.169051 0.689585 0.154 Uiso 1 1 calc R U . . . C60 C 0.1705(4) 0.3325(6) 0.68371(17) 0.0673(19) Uani 1 1 d . . . . . O60 O 0.1505(3) 0.3700(4) 0.65762(10) 0.0596(12) Uani 1 1 d . . . . . C61 C 0.3204(6) 0.2594(6) 0.70728(18) 0.080(2) Uani 1 1 d . . . . . H61A H 0.358687 0.234652 0.724818 0.096 Uiso 1 1 calc R U . . . O61 O 0.3672(3) 0.2693(3) 0.68244(10) 0.0594(11) Uani 1 1 d . . . . . C62 C 0.0749(4) 0.3026(5) 0.74435(15) 0.0549(16) Uani 1 1 d . . . . . C63 C 0.1571(4) 0.3311(5) 0.76367(14) 0.0529(15) Uani 1 1 d . . . . . C64 C 0.2156(4) 0.2468(5) 0.76724(14) 0.0527(15) Uani 1 1 d . . . . . C65 C 0.1709(4) 0.1656(4) 0.75083(13) 0.0465(13) Uani 1 1 d . . . . . C66 C 0.0838(4) 0.2017(5) 0.73621(14) 0.0503(14) Uani 1 1 d . . . . . C67 C -0.0074(5) 0.3694(6) 0.73515(19) 0.075(2) Uani 1 1 d . . . . . H67A H 0.016656 0.435962 0.731381 0.112 Uiso 1 1 calc R U . . . H67B H -0.052405 0.371061 0.752552 0.112 Uiso 1 1 calc R U . . . H67C H -0.040186 0.344804 0.715524 0.112 Uiso 1 1 calc R U . . . C68 C 0.1753(6) 0.4308(5) 0.77872(19) 0.079(2) Uani 1 1 d . . . . . H68A H 0.244105 0.444538 0.779527 0.118 Uiso 1 1 calc R U . . . H68B H 0.151803 0.431206 0.800543 0.118 Uiso 1 1 calc R U . . . H68C H 0.141686 0.481384 0.765840 0.118 Uiso 1 1 calc R U . . . C69 C 0.3079(5) 0.2395(6) 0.78734(17) 0.077(2) Uani 1 1 d . . . . . H69A H 0.344053 0.181764 0.780639 0.116 Uiso 1 1 calc R U . . . H69B H 0.293328 0.232973 0.810028 0.116 Uiso 1 1 calc R U . . . H69C H 0.346178 0.298927 0.784357 0.116 Uiso 1 1 calc R U . . . C70 C 0.2066(5) 0.0622(5) 0.75127(17) 0.0654(18) Uani 1 1 d . . . . . H70A H 0.178856 0.026676 0.732653 0.098 Uiso 1 1 calc R U . . . H70B H 0.187805 0.029742 0.771037 0.098 Uiso 1 1 calc R U . . . H70C H 0.276479 0.062163 0.750402 0.098 Uiso 1 1 calc R U . . . C71 C 0.0144(4) 0.1400(6) 0.71691(17) 0.0683(19) Uani 1 1 d . . . . . H71A H -0.018279 0.180840 0.700463 0.102 Uiso 1 1 calc R U . . . H71B H -0.032862 0.112104 0.731042 0.102 Uiso 1 1 calc R U . . . H71C H 0.048725 0.086688 0.706546 0.102 Uiso 1 1 calc R U . . . C80 C 0.4806(12) 0.7842(13) 0.5204(4) 0.124(6) Uani 0.527(3) 1 d D U P A 1 H80A H 0.485700 0.774644 0.543749 0.185 Uiso 0.527(3) 1 calc R U P A 1 H80B H 0.536133 0.821477 0.513553 0.185 Uiso 0.527(3) 1 calc R U P A 1 H80C H 0.478661 0.720079 0.509716 0.185 Uiso 0.527(3) 1 calc R U P A 1 C81 C 0.3889(6) 0.8413(8) 0.5115(3) 0.094(4) Uani 0.527(3) 1 d DG U P A 1 C82 C 0.3030(7) 0.8066(8) 0.5227(3) 0.091(4) Uani 0.527(3) 1 d DG U P A 1 H82A H 0.302072 0.748498 0.535379 0.109 Uiso 0.527(3) 1 calc R U P A 1 C83 C 0.2183(6) 0.8569(10) 0.5154(3) 0.091(4) Uani 0.527(3) 1 d G U P A 1 H83A H 0.159602 0.833201 0.523074 0.109 Uiso 0.527(3) 1 calc R U P A 1 C84 C 0.2197(7) 0.9419(9) 0.4969(3) 0.094(5) Uani 0.527(3) 1 d G U P A 1 H84A H 0.161822 0.976337 0.491931 0.113 Uiso 0.527(3) 1 calc R U P A 1 C85 C 0.3056(9) 0.9767(8) 0.4857(3) 0.101(4) Uani 0.527(3) 1 d G U P A 1 H85A H 0.306512 1.034772 0.473094 0.121 Uiso 0.527(3) 1 calc R U P A 1 C86 C 0.3902(7) 0.9263(9) 0.4930(3) 0.083(4) Uani 0.527(3) 1 d DG U P A 1 H86A H 0.448983 0.950071 0.485398 0.099 Uiso 0.527(3) 1 calc R U P A 1 C80' C 0.189(2) 0.976(3) 0.4912(10) 0.108(9) Uiso 0.261(3) 1 d D U P B 2 H80D H 0.154488 0.989497 0.510823 0.162 Uiso 0.261(3) 1 calc R U P B 2 H80E H 0.145240 0.943711 0.475463 0.162 Uiso 0.261(3) 1 calc R U P B 2 H80F H 0.211512 1.037978 0.482319 0.162 Uiso 0.261(3) 1 calc R U P B 2 C81' C 0.2732(15) 0.9092(17) 0.4992(6) 0.091(6) Uiso 0.261(3) 1 d DG U P B 2 C82' C 0.3629(17) 0.9339(18) 0.4885(6) 0.083(6) Uiso 0.261(3) 1 d DG U P B 2 H82B H 0.370950 0.992134 0.476333 0.099 Uiso 0.261(3) 1 calc R U P B 2 C83' C 0.4410(14) 0.873(2) 0.4957(7) 0.087(6) Uiso 0.261(3) 1 d G U P B 2 H83B H 0.502307 0.890138 0.488420 0.105 Uiso 0.261(3) 1 calc R U P B 2 C84' C 0.4292(17) 0.788(2) 0.5135(7) 0.113(7) Uiso 0.261(3) 1 d G U P B 2 H84B H 0.482542 0.746613 0.518421 0.136 Uiso 0.261(3) 1 calc R U P B 2 C85' C 0.339(2) 0.7634(18) 0.5242(7) 0.096(8) Uiso 0.261(3) 1 d G U P B 2 H85B H 0.331420 0.705084 0.536334 0.115 Uiso 0.261(3) 1 calc R U P B 2 C86' C 0.2614(16) 0.8239(19) 0.5170(7) 0.088(7) Uiso 0.261(3) 1 d DG U P B 2 H86B H 0.200062 0.807078 0.524246 0.106 Uiso 0.261(3) 1 calc R U P B 2 C80" C 0.230(2) 0.984(3) 0.4877(11) 0.098(7) Uiso 0.212(3) 1 d D U P C 3 H80G H 0.164167 0.962464 0.489812 0.146 Uiso 0.212(3) 1 calc R U P C 3 H80H H 0.243088 1.041264 0.501559 0.146 Uiso 0.212(3) 1 calc R U P C 3 H80I H 0.240547 1.001995 0.465343 0.146 Uiso 0.212(3) 1 calc R U P C 3 C81" C 0.2982(17) 0.9008(19) 0.4977(7) 0.094(7) Uiso 0.212(3) 1 d DG U P C 3 C82" C 0.3964(18) 0.916(2) 0.4966(9) 0.084(7) Uiso 0.212(3) 1 d DG U P C 3 H82C H 0.420458 0.976992 0.489737 0.101 Uiso 0.212(3) 1 calc R U P C 3 C83" C 0.4592(16) 0.840(3) 0.5056(10) 0.103(7) Uiso 0.212(3) 1 d G U P C 3 H83C H 0.526321 0.850347 0.504839 0.123 Uiso 0.212(3) 1 calc R U P C 3 C84" C 0.424(2) 0.750(2) 0.5157(8) 0.119(9) Uiso 0.212(3) 1 d G U P C 3 H84C H 0.466964 0.698920 0.521809 0.143 Uiso 0.212(3) 1 calc R U P C 3 C85" C 0.326(2) 0.7356(19) 0.5168(8) 0.091(9) Uiso 0.212(3) 1 d G U P C 3 H85C H 0.301744 0.674136 0.523676 0.109 Uiso 0.212(3) 1 calc R U P C 3 C86" C 0.2630(17) 0.811(2) 0.5078(7) 0.086(7) Uiso 0.212(3) 1 d DG U P C 3 H86C H 0.195879 0.800780 0.508573 0.103 Uiso 0.212(3) 1 calc R U P C 3 C90 C 0.9309(11) 0.7476(13) 0.5654(4) 0.111(5) Uani 0.551(3) 1 d D U P D 1 H90A H 0.930672 0.758236 0.542113 0.167 Uiso 0.551(3) 1 calc R U P D 1 H90B H 0.913993 0.679122 0.569755 0.167 Uiso 0.551(3) 1 calc R U P D 1 H90C H 0.994774 0.761692 0.574795 0.167 Uiso 0.551(3) 1 calc R U P D 1 C91 C 0.8607(7) 0.8135(9) 0.5795(3) 0.094(4) Uani 0.551(3) 1 d DG U P D 1 C92 C 0.7714(9) 0.7778(10) 0.5873(3) 0.108(5) Uani 0.551(3) 1 d DG U P D 1 H92A H 0.755020 0.711203 0.582951 0.130 Uiso 0.551(3) 1 calc R U P D 1 C93 C 0.7061(8) 0.8397(14) 0.6014(4) 0.130(6) Uani 0.551(3) 1 d G U P D 1 H93A H 0.645107 0.815331 0.606723 0.156 Uiso 0.551(3) 1 calc R U P D 1 C94 C 0.7301(11) 0.9372(13) 0.6078(4) 0.150(8) Uani 0.551(3) 1 d G U P D 1 H94A H 0.685477 0.979467 0.617436 0.180 Uiso 0.551(3) 1 calc R U P D 1 C95 C 0.8194(12) 0.9728(9) 0.6000(5) 0.155(7) Uani 0.551(3) 1 d G U P D 1 H95A H 0.835760 1.039475 0.604378 0.186 Uiso 0.551(3) 1 calc R U P D 1 C96 C 0.8847(9) 0.9110(10) 0.5859(4) 0.121(5) Uani 0.551(3) 1 d DG U P D 1 H96A H 0.945674 0.935348 0.580606 0.146 Uiso 0.551(3) 1 calc R U P D 1 C90' C 0.783(2) 1.002(2) 0.6098(9) 0.167(9) Uiso 0.332(3) 1 d D U P E 2 H90D H 0.719803 1.018454 0.600315 0.251 Uiso 0.332(3) 1 calc R U P E 2 H90E H 0.827865 1.055645 0.605579 0.251 Uiso 0.332(3) 1 calc R U P E 2 H90F H 0.778805 0.993267 0.632995 0.251 Uiso 0.332(3) 1 calc R U P E 2 C91' C 0.8175(15) 0.9106(13) 0.5954(5) 0.130(7) Uiso 0.332(3) 1 d DG U P E 2 C92' C 0.9053(15) 0.9103(14) 0.5809(6) 0.128(7) Uiso 0.332(3) 1 d DG U P E 2 H92B H 0.942048 0.968960 0.580201 0.153 Uiso 0.332(3) 1 calc R U P E 2 C93' C 0.9394(13) 0.8241(17) 0.5676(6) 0.097(6) Uiso 0.332(3) 1 d G U P E 2 H93B H 0.999445 0.823872 0.557713 0.116 Uiso 0.332(3) 1 calc R U P E 2 C94' C 0.8857(16) 0.7382(14) 0.5687(6) 0.108(7) Uiso 0.332(3) 1 d G U P E 2 H94B H 0.909039 0.679292 0.559541 0.130 Uiso 0.332(3) 1 calc R U P E 2 C95' C 0.7979(16) 0.7385(13) 0.5831(6) 0.108(8) Uiso 0.332(3) 1 d G U P E 2 H95B H 0.761235 0.679799 0.583857 0.130 Uiso 0.332(3) 1 calc R U P E 2 C96' C 0.7638(13) 0.8247(16) 0.5965(6) 0.113(7) Uiso 0.332(3) 1 d DG U P E 2 H96B H 0.703837 0.824886 0.606345 0.136 Uiso 0.332(3) 1 calc R U P E 2 C90" C 0.977(4) 0.896(5) 0.5634(18) 0.126(14) Uiso 0.118(3) 1 d D U P F 3 H90G H 0.991375 0.964781 0.568315 0.189 Uiso 0.118(3) 1 calc R U P F 3 H90H H 1.021912 0.853469 0.575912 0.189 Uiso 0.118(3) 1 calc R U P F 3 H90I H 0.984440 0.883706 0.540481 0.189 Uiso 0.118(3) 1 calc R U P F 3 C91" C 0.879(3) 0.873(4) 0.5719(11) 0.103(8) Uiso 0.118(3) 1 d DG U P F 3 C92" C 0.843(4) 0.779(4) 0.5671(14) 0.095(9) Uiso 0.118(3) 1 d DG U P F 3 H92C H 0.881672 0.728946 0.558358 0.114 Uiso 0.118(3) 1 calc R U P F 3 C93" C 0.749(4) 0.757(5) 0.5749(16) 0.111(10) Uiso 0.118(3) 1 d G U P F 3 H93C H 0.724649 0.692625 0.571643 0.133 Uiso 0.118(3) 1 calc R U P F 3 C94" C 0.692(4) 0.830(6) 0.5877(16) 0.127(11) Uiso 0.118(3) 1 d G U P F 3 H94C H 0.628520 0.815093 0.593053 0.153 Uiso 0.118(3) 1 calc R U P F 3 C95" C 0.728(4) 0.924(5) 0.5925(18) 0.139(9) Uiso 0.118(3) 1 d G U P F 3 H95C H 0.689413 0.973885 0.601177 0.166 Uiso 0.118(3) 1 calc R U P F 3 C96" C 0.822(4) 0.946(4) 0.5846(16) 0.135(8) Uiso 0.118(3) 1 d DG U P F 3 H96C H 0.846437 1.010208 0.587892 0.162 Uiso 0.118(3) 1 calc R U P F 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0404(5) 0.0547(6) 0.0481(5) 0.0072(5) 0.0080(4) -0.0002(4) Mg1 0.0300(8) 0.0419(10) 0.0405(9) 0.0011(7) -0.0005(6) 0.0009(7) Mg2 0.0244(8) 0.0425(11) 0.0544(10) 0.0008(8) 0.0032(7) 0.0005(7) N1 0.0249(19) 0.055(3) 0.042(2) 0.003(2) 0.0008(16) -0.0015(19) C1 0.024(2) 0.046(3) 0.051(3) 0.003(3) 0.006(2) 0.002(2) C2 0.039(3) 0.049(3) 0.043(3) 0.010(3) 0.009(2) 0.000(2) C3 0.034(3) 0.043(3) 0.045(3) 0.007(2) 0.004(2) 0.001(2) N3 0.0237(19) 0.048(3) 0.044(2) -0.002(2) -0.0014(16) 0.0011(18) C4 0.066(4) 0.040(3) 0.058(4) 0.001(3) 0.004(3) -0.002(3) C5 0.068(4) 0.065(4) 0.051(4) 0.007(3) -0.010(3) -0.006(3) C6 0.028(2) 0.041(3) 0.043(3) 0.003(2) 0.0015(19) 0.001(2) C7 0.032(3) 0.045(3) 0.048(3) 0.004(2) 0.001(2) -0.003(2) C8 0.037(3) 0.065(4) 0.046(3) -0.002(3) 0.005(2) 0.001(3) C9 0.053(3) 0.059(4) 0.042(3) -0.005(3) -0.002(2) 0.001(3) C10 0.035(3) 0.063(4) 0.056(4) -0.001(3) -0.003(2) 0.005(3) C11 0.026(2) 0.049(3) 0.051(3) -0.004(3) 0.000(2) 0.005(2) C12 0.033(3) 0.061(4) 0.049(3) -0.002(3) 0.005(2) 0.006(3) C13 0.035(3) 0.080(5) 0.100(6) 0.004(4) -0.005(3) -0.008(3) C14 0.058(4) 0.083(6) 0.076(5) -0.001(4) -0.004(3) 0.019(4) C15 0.036(3) 0.070(4) 0.053(3) -0.011(3) -0.003(2) 0.008(3) C16 0.064(5) 0.085(6) 0.190(10) 0.031(6) 0.064(6) 0.019(4) C17 0.057(4) 0.091(6) 0.109(6) 0.009(5) 0.007(4) 0.032(4) C18 0.036(3) 0.045(3) 0.036(3) -0.001(2) -0.002(2) 0.001(2) C19 0.034(3) 0.048(3) 0.045(3) -0.001(2) -0.001(2) -0.002(2) C20 0.048(3) 0.064(4) 0.054(3) -0.012(3) 0.001(3) 0.002(3) C21 0.048(3) 0.070(5) 0.066(4) -0.015(3) -0.007(3) -0.011(3) C22 0.032(3) 0.065(4) 0.073(4) -0.005(3) 0.002(3) -0.011(3) C23 0.032(3) 0.046(3) 0.053(3) 0.000(3) -0.001(2) 0.000(2) C24 0.036(3) 0.063(4) 0.056(4) -0.009(3) 0.004(2) 0.004(3) C25 0.044(4) 0.169(10) 0.111(7) 0.069(7) 0.017(4) 0.010(5) C26 0.036(3) 0.080(5) 0.092(5) -0.002(4) 0.007(3) 0.002(3) C27 0.026(2) 0.056(4) 0.071(4) -0.002(3) 0.002(2) 0.003(2) C28 0.048(3) 0.080(5) 0.066(4) 0.003(4) 0.013(3) 0.009(3) C29 0.052(4) 0.105(7) 0.084(5) 0.014(5) 0.007(3) 0.023(4) N31 0.029(2) 0.040(3) 0.064(3) 0.004(2) 0.0026(19) 0.0005(19) C31 0.034(3) 0.048(4) 0.065(4) -0.006(3) 0.002(2) 0.008(2) C32 0.037(3) 0.050(4) 0.068(4) -0.008(3) 0.012(3) 0.002(3) C33 0.024(2) 0.057(4) 0.056(3) 0.001(3) 0.004(2) 0.000(2) N33 0.0220(19) 0.046(3) 0.050(3) 0.003(2) -0.0007(16) -0.0009(18) C34 0.062(4) 0.049(4) 0.109(6) -0.019(4) 0.020(4) 0.000(3) C35 0.032(3) 0.073(5) 0.084(5) -0.012(4) 0.014(3) -0.004(3) C36 0.043(3) 0.031(3) 0.063(4) -0.002(3) 0.007(2) -0.002(2) C37 0.049(3) 0.044(3) 0.061(4) 0.001(3) -0.001(3) 0.005(3) C38 0.068(4) 0.044(4) 0.062(4) 0.001(3) 0.002(3) 0.002(3) C39 0.067(4) 0.040(4) 0.066(4) 0.000(3) 0.012(3) -0.011(3) C40 0.041(3) 0.044(4) 0.082(5) -0.001(3) 0.010(3) -0.011(3) C41 0.040(3) 0.045(3) 0.064(4) 0.001(3) 0.003(3) -0.007(3) C42 0.050(4) 0.065(5) 0.084(5) 0.014(4) -0.016(3) -0.001(3) C43 0.082(6) 0.187(12) 0.101(7) -0.014(7) -0.030(5) -0.027(7) C44 0.041(4) 0.172(12) 0.222(14) -0.047(10) -0.016(6) 0.024(6) C45 0.032(3) 0.051(4) 0.084(5) 0.016(3) 0.001(3) -0.008(3) C46 0.096(6) 0.109(7) 0.070(5) -0.003(5) -0.012(4) 0.033(5) C47 0.059(4) 0.075(5) 0.107(6) -0.009(4) -0.003(4) 0.027(4) C48 0.020(2) 0.056(4) 0.051(3) -0.001(3) 0.0036(19) -0.001(2) C49 0.030(2) 0.052(4) 0.053(3) 0.000(3) 0.002(2) -0.001(2) C50 0.034(3) 0.051(4) 0.070(4) 0.001(3) 0.004(3) -0.005(3) C51 0.032(3) 0.057(4) 0.081(5) -0.013(3) 0.005(3) -0.010(3) C52 0.030(3) 0.080(5) 0.066(4) -0.008(4) -0.005(3) -0.003(3) C53 0.029(3) 0.062(4) 0.054(3) -0.004(3) 0.001(2) -0.002(2) C54 0.042(3) 0.053(4) 0.061(4) 0.006(3) -0.004(3) -0.006(3) C55 0.069(5) 0.145(8) 0.053(4) 0.012(5) 0.009(3) 0.019(5) C56 0.048(3) 0.070(5) 0.074(4) 0.013(4) -0.004(3) 0.005(3) C57 0.045(3) 0.074(5) 0.060(4) 0.008(3) -0.014(3) -0.009(3) C58 0.082(5) 0.140(9) 0.070(5) 0.034(5) 0.011(4) 0.032(5) C59 0.118(7) 0.108(7) 0.083(6) 0.021(5) 0.016(5) 0.056(6) C60 0.047(3) 0.093(6) 0.064(4) -0.008(4) 0.022(3) -0.012(3) O60 0.041(2) 0.086(3) 0.052(2) 0.023(2) 0.0066(17) 0.003(2) C61 0.081(5) 0.099(7) 0.062(4) 0.004(4) 0.015(4) 0.005(4) O61 0.047(2) 0.079(3) 0.053(2) 0.000(2) 0.0109(18) 0.000(2) C62 0.040(3) 0.065(4) 0.060(4) 0.011(3) 0.013(3) 0.011(3) C63 0.061(4) 0.055(4) 0.044(3) -0.004(3) 0.012(3) 0.003(3) C64 0.055(3) 0.055(4) 0.049(3) 0.008(3) 0.004(3) 0.000(3) C65 0.047(3) 0.049(4) 0.045(3) 0.011(3) 0.016(2) 0.004(3) C66 0.043(3) 0.056(4) 0.052(3) 0.006(3) 0.009(2) -0.006(3) C67 0.061(4) 0.075(5) 0.090(5) 0.028(4) 0.019(4) 0.013(4) C68 0.089(5) 0.061(5) 0.087(5) -0.006(4) 0.010(4) -0.006(4) C69 0.071(5) 0.090(6) 0.068(5) 0.011(4) -0.013(4) 0.002(4) C70 0.064(4) 0.062(5) 0.071(4) 0.009(4) 0.016(3) 0.009(3) C71 0.051(4) 0.077(5) 0.078(5) 0.001(4) 0.013(3) -0.012(3) C80 0.114(10) 0.119(10) 0.139(10) -0.013(9) 0.016(9) 0.007(9) C81 0.094(8) 0.097(8) 0.093(8) -0.014(7) 0.026(7) -0.013(7) C82 0.087(8) 0.094(8) 0.093(8) 0.002(7) 0.011(7) -0.017(7) C83 0.080(8) 0.098(9) 0.094(8) 0.014(8) 0.000(7) -0.003(8) C84 0.081(8) 0.099(9) 0.101(8) -0.005(8) -0.010(7) -0.007(8) C85 0.114(8) 0.096(8) 0.092(8) -0.007(7) -0.001(7) -0.018(8) C86 0.079(8) 0.096(9) 0.075(8) -0.019(7) 0.027(7) -0.027(8) C90 0.088(9) 0.138(12) 0.107(10) 0.002(9) 0.003(8) 0.024(9) C91 0.087(7) 0.114(9) 0.082(8) 0.012(7) 0.000(7) 0.021(7) C92 0.087(8) 0.121(10) 0.116(10) -0.001(9) -0.009(8) -0.006(8) C93 0.117(10) 0.140(11) 0.134(11) 0.002(9) 0.021(9) 0.021(9) C94 0.137(12) 0.148(13) 0.166(13) 0.000(12) 0.007(11) 0.019(11) C95 0.142(11) 0.163(12) 0.159(11) -0.012(10) -0.004(10) 0.020(10) C96 0.102(9) 0.130(9) 0.132(9) 0.012(8) 0.000(8) 0.000(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 C60 1.627(8) . ? Co1 C61 1.804(8) . ? Co1 C66 2.095(6) . ? Co1 C62 2.108(6) . ? Co1 C64 2.108(6) . ? Co1 C65 2.121(5) . ? Co1 C63 2.129(6) . ? Mg1 O60 1.984(4) . ? Mg1 N3 2.039(4) . ? Mg1 N1 2.041(5) . ? Mg1 Mg2 3.523(2) . ? Mg2 O61 1.914(4) . ? Mg2 N31 2.043(5) . ? Mg2 N33 2.056(4) . ? N1 C1 1.334(7) . ? N1 C6 1.429(7) . ? C1 C2 1.389(7) . ? C1 C4 1.517(8) . ? C2 C3 1.402(8) . ? C3 N3 1.329(7) . ? C3 C5 1.513(7) . ? N3 C18 1.448(7) . ? C6 C11 1.407(7) . ? C6 C7 1.436(7) . ? C7 C8 1.366(8) . ? C7 C12 1.526(7) . ? C8 C9 1.384(7) . ? C9 C10 1.391(8) . ? C10 C11 1.382(8) . ? C11 C15 1.515(7) . ? C12 C13 1.524(9) . ? C12 C14 1.526(9) . ? C15 C16 1.501(10) . ? C15 C17 1.503(9) . ? C18 C23 1.402(7) . ? C18 C19 1.415(7) . ? C19 C20 1.389(8) . ? C19 C24 1.527(7) . ? C20 C21 1.373(8) . ? C21 C22 1.384(9) . ? C22 C23 1.387(8) . ? C23 C27 1.521(8) . ? C24 C25 1.505(9) . ? C24 C26 1.517(9) . ? C27 C28 1.525(9) . ? C27 C29 1.542(8) . ? N31 C31 1.342(7) . ? N31 C36 1.439(7) . ? C31 C32 1.415(8) . ? C31 C34 1.502(8) . ? C32 C33 1.407(8) . ? C33 N33 1.323(7) . ? C33 C35 1.517(7) . ? N33 C48 1.429(7) . ? C36 C41 1.402(7) . ? C36 C37 1.412(8) . ? C37 C38 1.392(9) . ? C37 C42 1.533(8) . ? C38 C39 1.389(9) . ? C39 C40 1.364(9) . ? C40 C41 1.400(8) . ? C41 C45 1.510(8) . ? C42 C43 1.460(11) . ? C42 C44 1.503(12) . ? C45 C46 1.520(10) . ? C45 C47 1.538(8) . ? C48 C49 1.406(8) . ? C48 C53 1.420(7) . ? C49 C50 1.389(8) . ? C49 C54 1.523(8) . ? C50 C51 1.368(8) . ? C51 C52 1.378(9) . ? C52 C53 1.392(8) . ? C53 C57 1.510(9) . ? C54 C56 1.531(8) . ? C54 C55 1.534(9) . ? C57 C58 1.505(10) . ? C57 C59 1.530(10) . ? C60 O60 1.223(8) . ? C61 O61 1.256(8) . ? C62 C66 1.420(9) . ? C62 C63 1.429(9) . ? C62 C67 1.504(8) . ? C63 C64 1.413(8) . ? C63 C68 1.511(9) . ? C64 C65 1.429(8) . ? C64 C69 1.513(9) . ? C65 C66 1.426(8) . ? C65 C70 1.492(8) . ? C66 C71 1.493(9) . ? C80 C81 1.531(17) . ? C81 C82 1.3900 . ? C81 C86 1.3900 . ? C82 C83 1.3900 . ? C83 C84 1.3900 . ? C84 C85 1.3900 . ? C85 C86 1.3900 . ? C80' C81' 1.516(19) . ? C81' C82' 1.3900 . ? C81' C86' 1.3900 . ? C82' C83' 1.3900 . ? C83' C84' 1.3900 . ? C84' C85' 1.3900 . ? C85' C86' 1.3900 . ? C80" C81" 1.523(19) . ? C81" C82" 1.3900 . ? C81" C86" 1.3900 . ? C82" C83" 1.3900 . ? C83" C84" 1.3900 . ? C84" C85" 1.3900 . ? C85" C86" 1.3900 . ? C90 C91 1.471(17) . ? C91 C92 1.3900 . ? C91 C96 1.3900 . ? C92 C93 1.3900 . ? C93 C94 1.3900 . ? C94 C95 1.3900 . ? C95 C96 1.3900 . ? C90' C91' 1.47(2) . ? C91' C92' 1.3900 . ? C91' C96' 1.3900 . ? C92' C93' 1.3900 . ? C93' C94' 1.3900 . ? C94' C95' 1.3900 . ? C95' C96' 1.3900 . ? C90" C91" 1.47(2) . ? C91" C92" 1.3900 . ? C91" C96" 1.3900 . ? C92" C93" 1.3900 . ? C93" C94" 1.3900 . ? C94" C95" 1.3900(11) . ? C95" C96" 1.3900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C60 Co1 C61 92.7(3) . . ? C60 Co1 C66 112.5(3) . . ? C61 Co1 C66 139.0(3) . . ? C60 Co1 C62 102.9(3) . . ? C61 Co1 C62 162.8(3) . . ? C66 Co1 C62 39.5(2) . . ? C60 Co1 C64 164.3(3) . . ? C61 Co1 C64 97.8(3) . . ? C66 Co1 C64 66.1(2) . . ? C62 Co1 C64 65.5(2) . . ? C60 Co1 C65 147.6(3) . . ? C61 Co1 C65 104.0(3) . . ? C66 Co1 C65 39.5(2) . . ? C62 Co1 C65 66.1(2) . . ? C64 Co1 C65 39.5(2) . . ? C60 Co1 C63 125.4(3) . . ? C61 Co1 C63 124.5(3) . . ? C66 Co1 C63 66.4(2) . . ? C62 Co1 C63 39.4(2) . . ? C64 Co1 C63 38.9(2) . . ? C65 Co1 C63 66.2(2) . . ? O60 Mg1 N3 124.90(18) . . ? O60 Mg1 N1 103.4(2) . . ? N3 Mg1 N1 94.50(19) . . ? O60 Mg1 Mg2 81.72(13) . . ? N3 Mg1 Mg2 123.47(14) . . ? N1 Mg1 Mg2 130.07(13) . . ? O61 Mg2 N31 105.4(2) . . ? O61 Mg2 N33 123.57(19) . . ? N31 Mg2 N33 93.75(19) . . ? O61 Mg2 Mg1 90.69(14) . . ? N31 Mg2 Mg1 126.63(13) . . ? N33 Mg2 Mg1 119.01(14) . . ? C1 N1 C6 118.9(5) . . ? C1 N1 Mg1 119.9(4) . . ? C6 N1 Mg1 121.1(3) . . ? N1 C1 C2 124.6(5) . . ? N1 C1 C4 119.7(5) . . ? C2 C1 C4 115.6(5) . . ? C1 C2 C3 130.1(5) . . ? N3 C3 C2 124.3(5) . . ? N3 C3 C5 119.9(5) . . ? C2 C3 C5 115.8(5) . . ? C3 N3 C18 117.9(4) . . ? C3 N3 Mg1 120.5(4) . . ? C18 N3 Mg1 121.5(3) . . ? C11 C6 N1 120.8(4) . . ? C11 C6 C7 119.7(5) . . ? N1 C6 C7 119.5(4) . . ? C8 C7 C6 118.0(5) . . ? C8 C7 C12 120.4(5) . . ? C6 C7 C12 121.6(5) . . ? C7 C8 C9 122.9(5) . . ? C8 C9 C10 118.8(5) . . ? C11 C10 C9 121.2(5) . . ? C10 C11 C6 119.4(5) . . ? C10 C11 C15 119.7(5) . . ? C6 C11 C15 120.9(5) . . ? C13 C12 C14 110.7(5) . . ? C13 C12 C7 109.5(5) . . ? C14 C12 C7 111.7(5) . . ? C16 C15 C17 110.0(6) . . ? C16 C15 C11 110.7(5) . . ? C17 C15 C11 113.1(5) . . ? C23 C18 C19 120.7(5) . . ? C23 C18 N3 120.0(5) . . ? C19 C18 N3 119.3(4) . . ? C20 C19 C18 118.0(5) . . ? C20 C19 C24 119.9(5) . . ? C18 C19 C24 122.1(5) . . ? C21 C20 C19 122.2(6) . . ? C20 C21 C22 118.7(6) . . ? C21 C22 C23 122.2(5) . . ? C22 C23 C18 118.1(5) . . ? C22 C23 C27 119.7(5) . . ? C18 C23 C27 122.1(5) . . ? C25 C24 C26 109.6(6) . . ? C25 C24 C19 111.9(5) . . ? C26 C24 C19 111.3(5) . . ? C23 C27 C28 111.6(5) . . ? C23 C27 C29 111.8(5) . . ? C28 C27 C29 110.2(5) . . ? C31 N31 C36 116.5(5) . . ? C31 N31 Mg2 122.5(4) . . ? C36 N31 Mg2 120.7(4) . . ? N31 C31 C32 122.7(5) . . ? N31 C31 C34 121.3(5) . . ? C32 C31 C34 116.1(5) . . ? C33 C32 C31 130.2(5) . . ? N33 C33 C32 125.0(5) . . ? N33 C33 C35 120.6(5) . . ? C32 C33 C35 114.4(5) . . ? C33 N33 C48 118.4(4) . . ? C33 N33 Mg2 121.4(4) . . ? C48 N33 Mg2 120.3(3) . . ? C41 C36 C37 120.4(5) . . ? C41 C36 N31 120.9(5) . . ? C37 C36 N31 118.6(5) . . ? C38 C37 C36 118.6(5) . . ? C38 C37 C42 120.5(6) . . ? C36 C37 C42 120.9(6) . . ? C39 C38 C37 121.2(6) . . ? C40 C39 C38 119.2(6) . . ? C39 C40 C41 122.3(6) . . ? C40 C41 C36 118.0(6) . . ? C40 C41 C45 120.4(5) . . ? C36 C41 C45 121.6(5) . . ? C43 C42 C44 110.1(8) . . ? C43 C42 C37 112.6(7) . . ? C44 C42 C37 112.0(6) . . ? C41 C45 C46 111.9(6) . . ? C41 C45 C47 112.1(6) . . ? C46 C45 C47 109.4(6) . . ? C49 C48 C53 120.2(5) . . ? C49 C48 N33 121.0(5) . . ? C53 C48 N33 118.8(5) . . ? C50 C49 C48 118.6(5) . . ? C50 C49 C54 120.1(5) . . ? C48 C49 C54 121.3(5) . . ? C51 C50 C49 121.8(6) . . ? C50 C51 C52 119.7(6) . . ? C51 C52 C53 121.5(6) . . ? C52 C53 C48 118.1(6) . . ? C52 C53 C57 119.9(5) . . ? C48 C53 C57 122.0(5) . . ? C49 C54 C56 111.5(5) . . ? C49 C54 C55 111.7(5) . . ? C56 C54 C55 108.3(6) . . ? C58 C57 C53 114.2(6) . . ? C58 C57 C59 109.6(6) . . ? C53 C57 C59 111.8(6) . . ? O60 C60 Co1 178.6(7) . . ? C60 O60 Mg1 142.9(4) . . ? O61 C61 Co1 135.9(6) . . ? C61 O61 Mg2 155.4(5) . . ? C66 C62 C63 108.7(5) . . ? C66 C62 C67 126.6(6) . . ? C63 C62 C67 124.7(6) . . ? C66 C62 Co1 69.8(3) . . ? C63 C62 Co1 71.1(3) . . ? C67 C62 Co1 126.1(4) . . ? C64 C63 C62 106.8(6) . . ? C64 C63 C68 126.7(6) . . ? C62 C63 C68 126.5(6) . . ? C64 C63 Co1 69.7(3) . . ? C62 C63 Co1 69.5(3) . . ? C68 C63 Co1 128.0(5) . . ? C63 C64 C65 109.6(5) . . ? C63 C64 C69 126.1(6) . . ? C65 C64 C69 124.1(6) . . ? C63 C64 Co1 71.3(3) . . ? C65 C64 Co1 70.7(3) . . ? C69 C64 Co1 127.9(5) . . ? C66 C65 C64 106.7(5) . . ? C66 C65 C70 127.5(6) . . ? C64 C65 C70 125.6(5) . . ? C66 C65 Co1 69.3(3) . . ? C64 C65 Co1 69.8(3) . . ? C70 C65 Co1 129.1(4) . . ? C62 C66 C65 108.2(5) . . ? C62 C66 C71 127.6(6) . . ? C65 C66 C71 124.2(6) . . ? C62 C66 Co1 70.7(3) . . ? C65 C66 Co1 71.2(3) . . ? C71 C66 Co1 125.5(4) . . ? C82 C81 C86 120.0 . . ? C82 C81 C80 118.3(7) . . ? C86 C81 C80 121.7(7) . . ? C83 C82 C81 120.0 . . ? C82 C83 C84 120.0 . . ? C83 C84 C85 120.0 . . ? C86 C85 C84 120.0 . . ? C85 C86 C81 120.0 . . ? C82' C81' C86' 120.0 . . ? C82' C81' C80' 119.5(8) . . ? C86' C81' C80' 120.5(8) . . ? C81' C82' C83' 120.0 . . ? C84' C83' C82' 120.0 . . ? C83' C84' C85' 120.0 . . ? C84' C85' C86' 120.0 . . ? C85' C86' C81' 120.0 . . ? C82" C81" C86" 120.0 . . ? C82" C81" C80" 119.2(8) . . ? C86" C81" C80" 120.8(8) . . ? C83" C82" C81" 120.0 . . ? C84" C83" C82" 120.0 . . ? C85" C84" C83" 120.0 . . ? C84" C85" C86" 120.0 . . ? C85" C86" C81" 120.0 . . ? C92 C91 C96 120.0 . . ? C92 C91 C90 120.2(7) . . ? C96 C91 C90 119.8(7) . . ? C91 C92 C93 120.0 . . ? C94 C93 C92 120.0 . . ? C93 C94 C95 120.0 . . ? C96 C95 C94 120.0 . . ? C95 C96 C91 120.0 . . ? C92' C91' C96' 120.0 . . ? C92' C91' C90' 119.3(8) . . ? C96' C91' C90' 120.7(8) . . ? C91' C92' C93' 120.0 . . ? C92' C93' C94' 120.0 . . ? C95' C94' C93' 120.0 . . ? C96' C95' C94' 120.0 . . ? C95' C96' C91' 120.0 . . ? C92" C91" C96" 120.00(5) . . ? C92" C91" C90" 119.9(8) . . ? C96" C91" C90" 120.1(8) . . ? C91" C92" C93" 120.0 . . ? C94" C93" C92" 120.00(7) . . ? C93" C94" C95" 120.00(6) . . ? C94" C95" C96" 120.0 . . ? C95" C96" C91" 120.00(6) . . ? _refine_diff_density_max 1.086 _refine_diff_density_min -0.613 _refine_diff_density_rms 0.067 _shelx_res_file ; TITL MRC2141 in P2(1)/c MRC2141.res created by SHELXL-2018/3 at 13:15:25 on 17-Jun-2021 REM P2(1)/c (#14 in standard setting) REM JMP179 CELL 1.54184 13.987842 13.593524 41.686731 90.0000 92.3748 90.0000 ZERR 4.00 0.000448 0.000822 0.002656 0.0000 0.0050 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H Co Mg N O UNIT 336 460 4 8 16 8 TEMP -100 L.S. 6 OMIT -4 1 3 OMIT 2 1 5 FMAP 2 PLAN 10 ACTA REM 'C70 H99 Co Mg2 N4 O2, 2(C7 H8)' REM C84 H115 Co Mg2 N4 O2 RTAB MG-H MG1 H1 RTAB MG-H MG2 H1 RTAB MHM MG1 H1 MG2 SADI C80 C81 C80' C81' C80" C81" SADI C80 C82 C80 C86 C80' C82' C80' C86' C80" C82" C80" C86" FLAT C80 C82 C85 C81 C83 C84 C86 FLAT C80' C82' C85' C81' C83' C84' C86' FLAT C80" C82" C85" C81" C83" C84" C86" SIMU 0.02 0.02 1.3 C80 > C86" SUMP 1 0 1 2 1 3 1 4 SADI C90 C91 C90' C91' C90" C91" SADI C90 C92 C90 C96 C90' C92' C90' C96' C90" C92" C90" C96" FLAT C90 C92 C95 C91 C93 C94 C96 FLAT C90' C92' C95' C91' C93' C94' C96' FLAT C90" C92" C95" C91" C93" C94" C96" SIMU 0.02 0.02 1.3 C90 > C96" SUMP 1 0 1 5 1 6 1 7 WGHT 0.084100 10.310301 FVAR 1.63942 0.52689 0.26069 0.21243 0.55053 0.33157 0.11790 CO1 3 0.198376 0.280263 0.717954 11.00000 0.04044 0.05469 = 0.04806 0.00723 0.00803 -0.00022 MG1 4 0.207583 0.433277 0.620041 11.00000 0.03004 0.04185 = 0.04052 0.00105 -0.00055 0.00088 MG2 4 0.389129 0.259389 0.637542 11.00000 0.02436 0.04254 = 0.05438 0.00083 0.00317 0.00053 H1 2 0.305124 0.352279 0.622041 11.00000 0.04321 N1 5 0.201909 0.579694 0.630614 11.00000 0.02490 0.05474 = 0.04192 0.00302 0.00079 -0.00151 C1 1 0.193559 0.645605 0.606967 11.00000 0.02426 0.04639 = 0.05110 0.00291 0.00638 0.00212 C2 1 0.171598 0.622873 0.575028 11.00000 0.03935 0.04883 = 0.04338 0.01037 0.00866 0.00038 AFIX 43 H2A 2 0.180191 0.675283 0.560350 11.00000 -1.20000 AFIX 0 C3 1 0.138723 0.534658 0.561054 11.00000 0.03416 0.04317 = 0.04469 0.00701 0.00398 0.00075 N3 5 0.140988 0.448069 0.575867 11.00000 0.02373 0.04775 = 0.04352 -0.00167 -0.00144 0.00111 C4 1 0.204860 0.754237 0.614510 11.00000 0.06579 0.04047 = 0.05767 0.00116 0.00442 -0.00200 AFIX 137 H4A 2 0.142303 0.782380 0.618986 11.00000 -1.50000 H4B 2 0.231158 0.788047 0.596078 11.00000 -1.50000 H4C 2 0.248422 0.762474 0.633341 11.00000 -1.50000 AFIX 0 C5 1 0.096002 0.542792 0.527229 11.00000 0.06805 0.06521 = 0.05063 0.00696 -0.00969 -0.00555 AFIX 137 H5A 2 0.111359 0.483455 0.515123 11.00000 -1.50000 H5B 2 0.122586 0.600534 0.516704 11.00000 -1.50000 H5C 2 0.026380 0.549656 0.527944 11.00000 -1.50000 AFIX 0 C6 1 0.200948 0.613059 0.663105 11.00000 0.02814 0.04110 = 0.04298 0.00322 0.00151 0.00085 C7 1 0.112273 0.643641 0.676126 11.00000 0.03242 0.04545 = 0.04841 0.00390 0.00133 -0.00309 C8 1 0.112938 0.670136 0.707747 11.00000 0.03686 0.06536 = 0.04586 -0.00211 0.00468 0.00060 AFIX 43 H8A 2 0.054411 0.689582 0.716635 11.00000 -1.20000 AFIX 0 C9 1 0.195156 0.669888 0.727402 11.00000 0.05272 0.05921 = 0.04186 -0.00508 -0.00204 0.00092 AFIX 43 H9A 2 0.193102 0.689586 0.749227 11.00000 -1.20000 AFIX 0 C10 1 0.280827 0.640288 0.714631 11.00000 0.03481 0.06259 = 0.05578 -0.00076 -0.00342 0.00454 AFIX 43 H10A 2 0.337471 0.639174 0.728011 11.00000 -1.20000 AFIX 0 C11 1 0.285078 0.612456 0.682826 11.00000 0.02646 0.04925 = 0.05094 -0.00377 -0.00018 0.00504 C12 1 0.019068 0.644693 0.655779 11.00000 0.03306 0.06133 = 0.04933 -0.00177 0.00531 0.00582 AFIX 13 H12A 2 0.034965 0.637128 0.632742 11.00000 -1.20000 AFIX 0 C13 1 -0.042821 0.557718 0.665015 11.00000 0.03484 0.08026 = 0.09952 0.00400 -0.00473 -0.00800 AFIX 137 H13A 2 -0.008293 0.496261 0.661366 11.00000 -1.50000 H13B 2 -0.102548 0.558218 0.651869 11.00000 -1.50000 H13C 2 -0.057415 0.562751 0.687747 11.00000 -1.50000 AFIX 0 C14 1 -0.035047 0.741249 0.659384 11.00000 0.05807 0.08288 = 0.07606 -0.00077 -0.00368 0.01869 AFIX 137 H14A 2 -0.055689 0.747458 0.681472 11.00000 -1.50000 H14B 2 -0.091207 0.741886 0.644528 11.00000 -1.50000 H14C 2 0.006997 0.796424 0.654467 11.00000 -1.50000 AFIX 0 C15 1 0.380371 0.584030 0.669487 11.00000 0.03592 0.07045 = 0.05264 -0.01085 -0.00334 0.00767 AFIX 13 H15A 2 0.366817 0.546427 0.649188 11.00000 -1.20000 AFIX 0 C16 1 0.436491 0.673898 0.661120 11.00000 0.06434 0.08487 = 0.18975 0.03108 0.06433 0.01882 AFIX 137 H16A 2 0.451483 0.712015 0.680639 11.00000 -1.50000 H16B 2 0.398560 0.714367 0.645868 11.00000 -1.50000 H16C 2 0.496072 0.653987 0.651388 11.00000 -1.50000 AFIX 0 C17 1 0.439392 0.519052 0.691744 11.00000 0.05740 0.09111 = 0.10883 0.00863 0.00661 0.03185 AFIX 137 H17A 2 0.491485 0.489544 0.680016 11.00000 -1.50000 H17B 2 0.398907 0.466899 0.700081 11.00000 -1.50000 H17C 2 0.466268 0.558349 0.709647 11.00000 -1.50000 AFIX 0 C18 1 0.098013 0.364681 0.559146 11.00000 0.03579 0.04483 = 0.03609 -0.00121 -0.00243 0.00084 C19 1 0.155311 0.305004 0.539833 11.00000 0.03381 0.04769 = 0.04456 -0.00090 -0.00117 -0.00217 C20 1 0.111636 0.227155 0.523386 11.00000 0.04777 0.06385 = 0.05430 -0.01213 0.00080 0.00162 AFIX 43 H20A 2 0.148947 0.187410 0.509944 11.00000 -1.20000 AFIX 0 C21 1 0.016300 0.205715 0.525908 11.00000 0.04800 0.06957 = 0.06638 -0.01523 -0.00705 -0.01111 AFIX 43 H21A 2 -0.012115 0.152412 0.514266 11.00000 -1.20000 AFIX 0 C22 1 -0.037565 0.263280 0.545738 11.00000 0.03238 0.06451 = 0.07349 -0.00511 0.00172 -0.01088 AFIX 43 H22A 2 -0.103060 0.247390 0.548043 11.00000 -1.20000 AFIX 0 C23 1 0.000828 0.343385 0.562363 11.00000 0.03205 0.04561 = 0.05318 -0.00039 -0.00101 -0.00036 C24 1 0.261807 0.324794 0.536317 11.00000 0.03644 0.06323 = 0.05617 -0.00866 0.00447 0.00366 AFIX 13 H24A 2 0.281835 0.376628 0.552237 11.00000 -1.20000 AFIX 0 C25 1 0.282492 0.362301 0.503356 11.00000 0.04370 0.16921 = 0.11138 0.06910 0.01738 0.01030 AFIX 137 H25A 2 0.351861 0.366205 0.501132 11.00000 -1.50000 H25B 2 0.254306 0.427823 0.500345 11.00000 -1.50000 H25C 2 0.254781 0.317302 0.487127 11.00000 -1.50000 AFIX 0 C26 1 0.321097 0.233448 0.543604 11.00000 0.03612 0.07963 = 0.09195 -0.00155 0.00655 0.00166 AFIX 137 H26A 2 0.304406 0.182270 0.527789 11.00000 -1.50000 H26B 2 0.307988 0.209563 0.565163 11.00000 -1.50000 H26C 2 0.389202 0.249499 0.542568 11.00000 -1.50000 AFIX 0 C27 1 -0.061809 0.403121 0.584102 11.00000 0.02582 0.05559 = 0.07091 -0.00243 0.00200 0.00276 AFIX 13 H27A 2 -0.022297 0.458760 0.593066 11.00000 -1.20000 AFIX 0 C28 1 -0.094782 0.342127 0.612297 11.00000 0.04778 0.08041 = 0.06584 0.00255 0.01315 0.00880 AFIX 137 H28A 2 -0.126862 0.282464 0.604204 11.00000 -1.50000 H28B 2 -0.139427 0.380868 0.624678 11.00000 -1.50000 H28C 2 -0.039241 0.323860 0.626125 11.00000 -1.50000 AFIX 0 C29 1 -0.148841 0.447783 0.565451 11.00000 0.05180 0.10452 = 0.08354 0.01419 0.00738 0.02336 AFIX 137 H29A 2 -0.126668 0.490796 0.548419 11.00000 -1.50000 H29B 2 -0.187038 0.486117 0.580165 11.00000 -1.50000 H29C 2 -0.188142 0.394828 0.555912 11.00000 -1.50000 AFIX 0 N31 5 0.384441 0.112378 0.627408 11.00000 0.02851 0.04039 = 0.06385 0.00409 0.00256 0.00049 C31 1 0.438396 0.071130 0.605167 11.00000 0.03404 0.04777 = 0.06495 -0.00605 0.00241 0.00810 C32 1 0.513831 0.121895 0.590780 11.00000 0.03695 0.04999 = 0.06780 -0.00840 0.01153 0.00185 AFIX 43 H32A 2 0.539741 0.089452 0.572920 11.00000 -1.20000 AFIX 0 C33 1 0.556509 0.212832 0.598754 11.00000 0.02422 0.05676 = 0.05566 0.00132 0.00412 -0.00012 N33 5 0.520985 0.278572 0.618405 11.00000 0.02200 0.04573 = 0.04972 0.00304 -0.00072 -0.00085 C34 1 0.421101 -0.032626 0.593948 11.00000 0.06160 0.04918 = 0.10942 -0.01895 0.01973 0.00002 AFIX 137 H34A 2 0.373920 -0.063923 0.607374 11.00000 -1.50000 H34B 2 0.481230 -0.069631 0.595600 11.00000 -1.50000 H34C 2 0.396869 -0.032003 0.571551 11.00000 -1.50000 AFIX 0 C35 1 0.650736 0.231615 0.583055 11.00000 0.03193 0.07341 = 0.08362 -0.01204 0.01405 -0.00434 AFIX 137 H35A 2 0.657629 0.302200 0.578963 11.00000 -1.50000 H35B 2 0.651756 0.195604 0.562707 11.00000 -1.50000 H35C 2 0.703683 0.209174 0.597357 11.00000 -1.50000 AFIX 0 C36 1 0.329309 0.046316 0.646287 11.00000 0.04283 0.03123 = 0.06310 -0.00176 0.00673 -0.00177 C37 1 0.375381 -0.002493 0.672542 11.00000 0.04882 0.04354 = 0.06063 0.00067 -0.00142 0.00515 C38 1 0.323784 -0.071560 0.689371 11.00000 0.06794 0.04383 = 0.06203 0.00080 0.00244 0.00181 AFIX 43 H38A 2 0.355240 -0.108551 0.706014 11.00000 -1.20000 AFIX 0 C39 1 0.227124 -0.087376 0.682269 11.00000 0.06742 0.04005 = 0.06560 0.00010 0.01197 -0.01137 AFIX 43 H39A 2 0.192794 -0.135152 0.693799 11.00000 -1.20000 AFIX 0 C40 1 0.182069 -0.033473 0.658537 11.00000 0.04062 0.04396 = 0.08204 -0.00111 0.01007 -0.01144 AFIX 43 H40A 2 0.115160 -0.041782 0.654639 11.00000 -1.20000 AFIX 0 C41 1 0.230978 0.033670 0.639721 11.00000 0.04015 0.04455 = 0.06449 0.00130 0.00331 -0.00668 C42 1 0.480525 0.018481 0.681969 11.00000 0.05024 0.06535 = 0.08449 0.01380 -0.01569 -0.00078 AFIX 13 H42A 2 0.498676 0.080526 0.670860 11.00000 -1.20000 AFIX 0 C43 1 0.496212 0.034690 0.716410 11.00000 0.08161 0.18708 = 0.10053 -0.01390 -0.02974 -0.02658 AFIX 137 H43A 2 0.483718 -0.026431 0.727978 11.00000 -1.50000 H43B 2 0.452842 0.086242 0.723465 11.00000 -1.50000 H43C 2 0.562605 0.055139 0.720903 11.00000 -1.50000 AFIX 0 C44 1 0.545678 -0.061372 0.670843 11.00000 0.04053 0.17205 = 0.22173 -0.04701 -0.01632 0.02350 AFIX 137 H44A 2 0.611822 -0.037439 0.671649 11.00000 -1.50000 H44B 2 0.526909 -0.079902 0.648752 11.00000 -1.50000 H44C 2 0.540787 -0.118842 0.684874 11.00000 -1.50000 AFIX 0 C45 1 0.178955 0.088185 0.612698 11.00000 0.03218 0.05090 = 0.08435 0.01646 0.00087 -0.00780 AFIX 13 H45A 2 0.221678 0.142350 0.605654 11.00000 -1.20000 AFIX 0 C46 1 0.157410 0.022019 0.583899 11.00000 0.09560 0.10944 = 0.06952 -0.00264 -0.01238 0.03255 AFIX 137 H46A 2 0.216018 -0.011961 0.578095 11.00000 -1.50000 H46B 2 0.133415 0.061945 0.565720 11.00000 -1.50000 H46C 2 0.108909 -0.026581 0.589316 11.00000 -1.50000 AFIX 0 C47 1 0.085480 0.135180 0.623418 11.00000 0.05871 0.07507 = 0.10672 -0.00932 -0.00259 0.02685 AFIX 137 H47A 2 0.039012 0.083385 0.627742 11.00000 -1.50000 H47B 2 0.059390 0.178315 0.606373 11.00000 -1.50000 H47C 2 0.098480 0.173781 0.642970 11.00000 -1.50000 AFIX 0 C48 1 0.575882 0.364890 0.625749 11.00000 0.02004 0.05602 = 0.05073 -0.00138 0.00365 -0.00101 C49 1 0.568476 0.448735 0.606053 11.00000 0.02956 0.05187 = 0.05333 0.00011 0.00152 -0.00090 C50 1 0.622559 0.531098 0.614541 11.00000 0.03383 0.05082 = 0.06986 0.00117 0.00405 -0.00514 AFIX 43 H50A 2 0.618369 0.587850 0.601258 11.00000 -1.20000 AFIX 0 C51 1 0.681680 0.532734 0.641497 11.00000 0.03153 0.05689 = 0.08058 -0.01301 0.00482 -0.00982 AFIX 43 H51A 2 0.718153 0.589915 0.646710 11.00000 -1.20000 AFIX 0 C52 1 0.688140 0.451089 0.661072 11.00000 0.03034 0.08007 = 0.06551 -0.00845 -0.00506 -0.00321 AFIX 43 H52A 2 0.729461 0.452764 0.679733 11.00000 -1.20000 AFIX 0 C53 1 0.635529 0.366217 0.654140 11.00000 0.02900 0.06191 = 0.05403 -0.00418 0.00070 -0.00238 C54 1 0.504245 0.449708 0.575661 11.00000 0.04196 0.05338 = 0.06141 0.00553 -0.00368 -0.00593 AFIX 13 H54A 2 0.469749 0.385359 0.574005 11.00000 -1.20000 AFIX 0 C55 1 0.562199 0.462997 0.545510 11.00000 0.06861 0.14501 = 0.05270 0.01235 0.00909 0.01935 AFIX 137 H55A 2 0.518636 0.464482 0.526489 11.00000 -1.50000 H55B 2 0.607037 0.408056 0.543744 11.00000 -1.50000 H55C 2 0.597940 0.524942 0.547038 11.00000 -1.50000 AFIX 0 C56 1 0.429895 0.532247 0.576475 11.00000 0.04771 0.07047 = 0.07370 0.01276 -0.00416 0.00467 AFIX 137 H56A 2 0.462509 0.596066 0.577079 11.00000 -1.50000 H56B 2 0.392214 0.525019 0.595637 11.00000 -1.50000 H56C 2 0.387374 0.528483 0.557231 11.00000 -1.50000 AFIX 0 C57 1 0.641809 0.279671 0.676830 11.00000 0.04494 0.07371 = 0.06042 0.00814 -0.01388 -0.00867 AFIX 13 H57A 2 0.590681 0.232227 0.669617 11.00000 -1.20000 AFIX 0 C58 1 0.624224 0.305168 0.711227 11.00000 0.08193 0.14008 = 0.06970 0.03378 0.01089 0.03210 AFIX 137 H58A 2 0.623647 0.244818 0.724078 11.00000 -1.50000 H58B 2 0.562372 0.338560 0.712393 11.00000 -1.50000 H58C 2 0.675204 0.348726 0.719605 11.00000 -1.50000 AFIX 0 C59 1 0.737443 0.225699 0.675035 11.00000 0.11763 0.10754 = 0.08343 0.02146 0.01556 0.05624 AFIX 137 H59A 2 0.789763 0.270522 0.681362 11.00000 -1.50000 H59B 2 0.745628 0.202958 0.653010 11.00000 -1.50000 H59C 2 0.738185 0.169051 0.689585 11.00000 -1.50000 AFIX 0 C60 1 0.170521 0.332493 0.683713 11.00000 0.04741 0.09260 = 0.06357 -0.00809 0.02176 -0.01232 O60 6 0.150491 0.370016 0.657620 11.00000 0.04064 0.08634 = 0.05209 0.02282 0.00664 0.00323 C61 1 0.320351 0.259354 0.707277 11.00000 0.08068 0.09878 = 0.06155 0.00419 0.01471 0.00520 AFIX 43 H61A 2 0.358687 0.234652 0.724818 11.00000 -1.20000 AFIX 0 O61 6 0.367241 0.269305 0.682438 11.00000 0.04732 0.07897 = 0.05275 0.00041 0.01092 -0.00048 C62 1 0.074925 0.302636 0.744349 11.00000 0.04009 0.06504 = 0.06044 0.01114 0.01267 0.01129 C63 1 0.157090 0.331098 0.763667 11.00000 0.06078 0.05467 = 0.04416 -0.00405 0.01181 0.00281 C64 1 0.215627 0.246813 0.767239 11.00000 0.05451 0.05512 = 0.04877 0.00779 0.00409 -0.00046 C65 1 0.170913 0.165627 0.750828 11.00000 0.04651 0.04896 = 0.04530 0.01129 0.01562 0.00365 C66 1 0.083818 0.201704 0.736213 11.00000 0.04335 0.05629 = 0.05187 0.00572 0.00920 -0.00637 C67 1 -0.007425 0.369433 0.735151 11.00000 0.06093 0.07496 = 0.09018 0.02787 0.01918 0.01283 AFIX 137 H67A 2 0.016656 0.435962 0.731381 11.00000 -1.50000 H67B 2 -0.052405 0.371061 0.752552 11.00000 -1.50000 H67C 2 -0.040186 0.344804 0.715524 11.00000 -1.50000 AFIX 0 C68 1 0.175267 0.430814 0.778716 11.00000 0.08938 0.06076 = 0.08674 -0.00554 0.01019 -0.00552 AFIX 137 H68A 2 0.244105 0.444538 0.779527 11.00000 -1.50000 H68B 2 0.151803 0.431206 0.800543 11.00000 -1.50000 H68C 2 0.141686 0.481384 0.765840 11.00000 -1.50000 AFIX 0 C69 1 0.307925 0.239473 0.787336 11.00000 0.07133 0.09033 = 0.06826 0.01077 -0.01253 0.00169 AFIX 137 H69A 2 0.344053 0.181764 0.780639 11.00000 -1.50000 H69B 2 0.293328 0.232973 0.810028 11.00000 -1.50000 H69C 2 0.346178 0.298927 0.784357 11.00000 -1.50000 AFIX 0 C70 1 0.206572 0.062178 0.751268 11.00000 0.06397 0.06206 = 0.07116 0.00918 0.01555 0.00914 AFIX 137 H70A 2 0.178856 0.026676 0.732653 11.00000 -1.50000 H70B 2 0.187805 0.029742 0.771037 11.00000 -1.50000 H70C 2 0.276479 0.062163 0.750402 11.00000 -1.50000 AFIX 0 C71 1 0.014387 0.140038 0.716908 11.00000 0.05107 0.07719 = 0.07755 0.00122 0.01271 -0.01192 AFIX 137 H71A 2 -0.018279 0.180840 0.700463 11.00000 -1.50000 H71B 2 -0.032862 0.112104 0.731042 11.00000 -1.50000 H71C 2 0.048725 0.086688 0.706546 11.00000 -1.50000 AFIX 0 PART 1 C80 1 0.480606 0.784243 0.520441 21.00000 0.11364 0.11935 = 0.13894 -0.01264 0.01643 0.00732 AFIX 137 H80A 2 0.485700 0.774644 0.543749 21.00000 -1.50000 H80B 2 0.536133 0.821477 0.513553 21.00000 -1.50000 H80C 2 0.478661 0.720079 0.509716 21.00000 -1.50000 AFIX 66 C81 1 0.388922 0.841320 0.511545 21.00000 0.09418 0.09743 = 0.09275 -0.01388 0.02565 -0.01300 C82 1 0.302973 0.806609 0.522735 21.00000 0.08724 0.09387 = 0.09277 0.00209 0.01122 -0.01694 AFIX 43 H82A 2 0.302072 0.748498 0.535379 21.00000 -1.20000 AFIX 65 C83 1 0.218344 0.856924 0.515426 21.00000 0.07967 0.09823 = 0.09412 0.01411 0.00027 -0.00338 AFIX 43 H83A 2 0.159602 0.833201 0.523074 21.00000 -1.20000 AFIX 65 C84 1 0.219663 0.941949 0.496927 21.00000 0.08120 0.09873 = 0.10124 -0.00514 -0.01038 -0.00704 AFIX 43 H84A 2 0.161822 0.976337 0.491931 21.00000 -1.20000 AFIX 65 C85 1 0.305611 0.976661 0.485737 21.00000 0.11426 0.09569 = 0.09204 -0.00671 -0.00134 -0.01828 AFIX 43 H85A 2 0.306512 1.034772 0.473094 21.00000 -1.20000 AFIX 65 C86 1 0.390241 0.926347 0.493046 21.00000 0.07897 0.09621 = 0.07453 -0.01866 0.02723 -0.02688 AFIX 43 H86A 2 0.448983 0.950071 0.485398 21.00000 -1.20000 AFIX 0 PART 2 C80' 1 0.188624 0.976003 0.491240 31.00000 0.10829 AFIX 137 H80D 2 0.154488 0.989497 0.510823 31.00000 -1.50000 H80E 2 0.145240 0.943711 0.475463 31.00000 -1.50000 H80F 2 0.211512 1.037978 0.482319 31.00000 -1.50000 AFIX 66 C81' 1 0.273156 0.909197 0.499153 31.00000 0.09090 C82' 1 0.362925 0.933865 0.488512 31.00000 0.08275 AFIX 43 H82B 2 0.370950 0.992134 0.476333 31.00000 -1.20000 AFIX 65 C83' 1 0.440953 0.873278 0.495693 31.00000 0.08745 AFIX 43 H83B 2 0.502307 0.890138 0.488420 31.00000 -1.20000 AFIX 65 C84' 1 0.429213 0.788022 0.513513 31.00000 0.11340 AFIX 43 H84B 2 0.482542 0.746613 0.518421 31.00000 -1.20000 AFIX 65 C85' 1 0.339444 0.763352 0.524154 31.00000 0.09602 AFIX 43 H85B 2 0.331420 0.705084 0.536334 31.00000 -1.20000 AFIX 65 C86' 1 0.261415 0.823939 0.516974 31.00000 0.08799 AFIX 43 H86B 2 0.200062 0.807078 0.524246 31.00000 -1.20000 AFIX 0 PART 3 C80" 1 0.230463 0.984054 0.487719 41.00000 0.09753 AFIX 33 H80G 2 0.164167 0.962464 0.489812 41.00000 -1.50000 H80H 2 0.243088 1.041264 0.501559 41.00000 -1.50000 H80I 2 0.240547 1.001995 0.465343 41.00000 -1.50000 AFIX 66 C81" 1 0.298216 0.900794 0.497735 41.00000 0.09427 C82" 1 0.396360 0.915515 0.496626 41.00000 0.08382 AFIX 43 H82C 2 0.420458 0.976992 0.489737 41.00000 -1.20000 AFIX 65 C83" 1 0.459244 0.840286 0.505597 41.00000 0.10281 AFIX 43 H83C 2 0.526321 0.850347 0.504839 41.00000 -1.20000 AFIX 65 C84" 1 0.423985 0.750336 0.515677 41.00000 0.11930 AFIX 43 H84C 2 0.466964 0.698920 0.521809 41.00000 -1.20000 AFIX 65 C85" 1 0.325841 0.735613 0.516786 41.00000 0.09081 AFIX 43 H85C 2 0.301744 0.674136 0.523676 41.00000 -1.20000 AFIX 65 C86" 1 0.262956 0.810842 0.507815 41.00000 0.08559 AFIX 43 H86C 2 0.195879 0.800780 0.508573 41.00000 -1.20000 AFIX 0 PART 1 C90 1 0.930885 0.747642 0.565369 51.00000 0.08848 0.13827 = 0.10684 0.00218 0.00306 0.02361 AFIX 137 H90A 2 0.930672 0.758236 0.542113 51.00000 -1.50000 H90B 2 0.913993 0.679122 0.569755 51.00000 -1.50000 H90C 2 0.994774 0.761692 0.574795 51.00000 -1.50000 AFIX 66 C91 1 0.860681 0.813484 0.579543 51.00000 0.08670 0.11363 = 0.08230 0.01153 0.00017 0.02112 C92 1 0.771410 0.777840 0.587301 51.00000 0.08665 0.12070 = 0.11643 -0.00121 -0.00898 -0.00567 AFIX 43 H92A 2 0.755020 0.711203 0.582951 51.00000 -1.20000 AFIX 65 C93 1 0.706120 0.839693 0.601422 51.00000 0.11677 0.13960 = 0.13388 0.00154 0.02065 0.02142 AFIX 43 H93A 2 0.645107 0.815331 0.606723 51.00000 -1.20000 AFIX 65 C94 1 0.730100 0.937193 0.607785 51.00000 0.13736 0.14775 = 0.16598 0.00009 0.00717 0.01881 AFIX 43 H94A 2 0.685477 0.979467 0.617436 51.00000 -1.20000 AFIX 65 C95 1 0.819371 0.972838 0.600028 51.00000 0.14231 0.16317 = 0.15914 -0.01209 -0.00440 0.01967 AFIX 43 H95A 2 0.835760 1.039475 0.604378 51.00000 -1.20000 AFIX 65 C96 1 0.884662 0.910986 0.585907 51.00000 0.10179 0.13005 = 0.13160 0.01249 0.00021 -0.00039 AFIX 43 H96A 2 0.945674 0.935348 0.580606 51.00000 -1.20000 AFIX 0 PART 2 C90' 1 0.783133 1.002124 0.609769 61.00000 0.16734 AFIX 137 H90D 2 0.719803 1.018454 0.600315 61.00000 -1.50000 H90E 2 0.827865 1.055645 0.605579 61.00000 -1.50000 H90F 2 0.778805 0.993267 0.632995 61.00000 -1.50000 AFIX 66 C91' 1 0.817546 0.910565 0.595388 61.00000 0.13019 C92' 1 0.905344 0.910263 0.580943 61.00000 0.12759 AFIX 43 H92B 2 0.942048 0.968960 0.580201 61.00000 -1.20000 AFIX 65 C93' 1 0.939439 0.824078 0.567585 61.00000 0.09689 AFIX 43 H93B 2 0.999445 0.823872 0.557713 61.00000 -1.20000 AFIX 65 C94' 1 0.885736 0.738195 0.568671 61.00000 0.10804 AFIX 43 H94B 2 0.909039 0.679292 0.559541 61.00000 -1.20000 AFIX 65 C95' 1 0.797938 0.738496 0.583115 61.00000 0.10841 AFIX 43 H95B 2 0.761235 0.679799 0.583857 61.00000 -1.20000 AFIX 65 C96' 1 0.763842 0.824680 0.596473 61.00000 0.11349 AFIX 43 H96B 2 0.703837 0.824886 0.606345 61.00000 -1.20000 AFIX 0 PART 3 C90" 1 0.977332 0.895619 0.563445 71.00000 0.12623 AFIX 33 H90G 2 0.991375 0.964781 0.568315 71.00000 -1.50000 H90H 2 1.021912 0.853469 0.575912 71.00000 -1.50000 H90I 2 0.984440 0.883706 0.540481 71.00000 -1.50000 AFIX 66 C91" 1 0.878819 0.872991 0.571876 71.00000 0.10317 C92" 1 0.842646 0.778667 0.567050 71.00000 0.09471 AFIX 43 H92C 2 0.881672 0.728946 0.558358 71.00000 -1.20000 AFIX 65 C93" 1 0.749371 0.757091 0.574942 71.00000 0.11108 AFIX 43 H93C 2 0.724649 0.692625 0.571643 71.00000 -1.20000 AFIX 65 C94" 1 0.692269 0.829840 0.587659 71.00000 0.12736 AFIX 43 H94C 2 0.628520 0.815093 0.593053 71.00000 -1.20000 AFIX 65 C95" 1 0.728440 0.924164 0.592485 71.00000 0.13871 AFIX 43 H95C 2 0.689413 0.973885 0.601177 71.00000 -1.20000 AFIX 65 C96" 1 0.821715 0.945741 0.584594 71.00000 0.13512 AFIX 43 H96C 2 0.846437 1.010208 0.587892 71.00000 -1.20000 PART 0 AFIX 0 HKLF 4 REM MRC2141 in P2(1)/c REM wR2 = 0.2711, GooF = S = 1.042, Restrained GooF = 1.035 for all data REM R1 = 0.1004 for 8175 Fo > 4sig(Fo) and 0.1655 for all 15158 data REM 917 parameters refined using 362 restraints END WGHT 0.0843 10.2834 REM Highest difference peak 1.086, deepest hole -0.613, 1-sigma level 0.067 Q1 1 0.2047 0.2760 0.7438 11.00000 0.05 1.09 Q2 1 0.1941 0.2687 0.6930 11.00000 0.05 0.75 Q3 1 0.3814 0.2559 0.6124 11.00000 0.05 0.70 Q4 1 0.1979 0.4355 0.5949 11.00000 0.05 0.67 Q5 1 0.2139 0.4327 0.6443 11.00000 0.05 0.65 Q6 1 0.3865 0.2636 0.6629 11.00000 0.05 0.57 Q7 1 0.1365 0.4394 0.5529 11.00000 0.05 0.37 Q8 1 0.1210 0.3135 0.6801 11.00000 0.05 0.37 Q9 1 0.1480 0.5365 0.5842 11.00000 0.05 0.35 Q10 1 0.1876 0.5206 0.6141 11.00000 0.05 0.34 ; _shelx_res_checksum 82636 _shelx_hkl_file ; 0 0 -4 84620.9 1279.98 7 0 0 -5 50.7857 79.3901 7 0 0 -6 2554.47 306.567 7 0 0 -7 12.5663 84.3687 7 0 0 -8 752.740 214.652 7 0 0 -9 57.3194 137.378 7 0 0 -10 27403.8 1236.35 7 0 0 -11 211.510 185.243 7 0 0 -12 24079.2 1278.23 7 0 0 -13 161.029 179.364 7 0 0 -14 4781.86 617.955 7 0 0 -15-18.1223 175.719 7 0 0 -16 7460.25 825.982 7 0 0 -17 330.962 281.464 7 0 0 -18 40128.6 1998.13 7 0 0 -19 336.924 263.022 7 0 0 -20 65280.1 2646.79 7 0 0 -21-32.9931 221.732 7 0 0 -22 455.008 287.895 7 0 0 -28 11613.0 1373.59 1 0 0 -29-12.2861 205.282 4 0 0 -29 70.1521 216.105 1 0 0 -30 16731.9 1678.59 1 0 0 -30 17085.7 1156.13 4 0 0 -31 91.2872 290.905 1 0 0 -31 196.790 201.995 4 0 0 -32 4610.53 906.933 1 0 0 -32 4117.95 604.522 4 0 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239.453 138.004 5 -4 4 46 244.127 179.205 5 -4 4 45 309.578 195.905 5 -4 4 44 139.490 202.616 5 -4 4 43 599.272 275.082 5 -4 4 42 219.294 217.598 5 -4 4 41-244.952 246.138 5 -4 4 40 2619.79 474.550 5 -4 4 39 818.139 333.474 5 -4 4 38 2112.95 467.928 5 -4 4 37 1330.45 376.449 5 -4 4 36 116.080 243.362 5 -4 4 35 3851.70 612.228 5 -4 4 34 1851.40 429.885 5 -4 4 33 901.236 348.188 5 4 4 -33 391.721 189.507 4 -4 4 32 1276.63 399.201 5 4 -4 -32 1042.68 547.250 7 -4 -4 32 954.368 269.805 6 4 -4 -32 1372.37 566.810 1 4 4 -32 976.845 254.686 4 4 -4 -31 142.051 298.867 7 -4 4 31 331.937 278.848 5 -4 -4 31-209.129 201.291 6 4 4 -31 36.3391 155.959 4 4 -4 -31-212.213 289.550 1 -4 4 30 478.737 295.933 5 4 -4 -30-303.369 250.191 7 4 -4 -30-44.0884 189.072 1 -4 -4 30-78.9943 150.543 6 -4 4 29 48.1898 201.733 5 -4 -4 29 346.628 230.160 6 4 -4 -29 310.515 451.131 7 4 -4 -29 504.436 309.181 1 -4 4 28 2099.66 473.042 5 -4 -4 28 1809.92 370.988 6 4 -4 -28 1840.11 631.018 7 4 -4 -28 1933.23 626.178 1 4 -4 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635.468 7 4 -4 -5 25362.5 1457.10 7 -4 -4 5 23312.1 1307.89 1 4 -4 -4 5619.51 711.314 7 -4 -4 4 5639.07 660.051 1 -4 -4 3 9783.83 851.465 1 4 -4 -3 10891.3 961.886 7 -4 -4 2 13403.3 973.147 1 4 -4 -2 14645.0 1062.67 7 -4 -4 1 2556.29 454.852 1 -4 -4 0 5946.98 664.991 1 -4 -4 -1 12320.7 929.295 1 -4 -4 -2 407.208 236.574 1 -4 -4 -3 944.591 366.872 1 -4 -4 -4 20044.5 1134.96 1 -4 -4 -5 760.466 288.806 1 -4 -4 -6 12375.0 963.007 1 -4 -4 -7 6118.27 717.241 1 -4 -4 -8 1297.95 363.561 1 -4 -4 -9 6276.46 723.461 1 -4 -4 -10 367.486 213.445 1 -4 -4 -11 1003.87 354.182 1 -4 -4 -12 11367.0 1045.89 1 -4 -4 -13 532.833 291.522 1 -4 -4 -14 3990.20 659.495 1 -4 -4 -15 4322.52 701.484 1 -4 -4 -16 2788.57 588.412 1 -4 -4 -17 701.910 316.043 1 -4 -4 -18 2959.51 672.278 1 -4 -4 -19 5382.09 905.788 1 -4 -4 -20 423.498 316.218 1 -4 -4 -21-180.081 337.455 1 -4 -4 -22 11005.9 1422.92 1 -4 -4 -23 1718.63 643.548 1 -4 -4 -24 16274.5 1807.58 1 -4 -4 -25 12841.8 1645.19 1 -4 4 -25 11755.2 942.132 4 -4 4 -26 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3937.83 980.903 7 4 -5 -30 4472.41 883.459 1 -4 -5 30 4022.58 560.003 6 -4 5 30 4287.49 671.603 5 -4 5 29 2602.41 560.166 5 4 -5 -29 2618.24 681.483 1 -4 -5 29 2720.35 482.535 6 4 -5 -29 2451.02 800.948 7 -4 5 28 1142.63 392.802 5 -4 -5 28 967.706 316.452 6 4 -5 -28 451.525 286.814 1 4 -5 -28 661.744 472.663 7 -4 -5 27 2582.17 478.344 6 -4 5 27 2654.44 527.592 5 4 -5 -27 2532.03 755.909 7 4 -5 -27 3503.95 761.225 1 -4 5 26-99.5858 201.368 5 -4 -5 26-92.4969 228.523 6 4 -5 -26 252.687 332.042 7 4 -5 -26 28.3541 212.772 1 -4 5 25 2552.38 496.754 5 4 -5 -25 2080.91 549.262 1 -4 -5 25 2380.90 432.441 6 4 -5 -25 1414.77 544.545 7 -4 5 24 683.016 298.164 5 4 -5 -24-75.8326 276.526 7 4 -5 -24 349.914 263.891 1 -4 -5 24 319.265 194.957 6 -4 -5 23 5175.00 626.792 6 4 -5 -23 4526.19 971.573 7 4 -5 -23 4825.16 776.474 1 -4 5 23 5491.83 679.812 5 4 -5 -22 678.727 263.636 1 -4 5 22 191.242 179.560 5 4 -5 -22-113.438 308.327 7 -4 -5 22 175.002 166.292 6 4 -5 -21 164.552 233.075 7 4 -5 -21 134.855 166.020 1 4 -5 -20 379.806 263.750 1 4 -5 -20 98.5562 300.782 7 4 -5 -19 82.4718 123.284 1 4 -5 -19 632.321 374.460 7 4 -5 -18 328.539 343.752 7 4 -5 -18 119.863 130.496 1 4 -5 -17 5339.68 912.043 7 4 -5 -17 3964.38 577.964 1 4 -5 -16 1652.29 370.372 1 4 -5 -16 2894.68 694.184 7 4 -5 -15 8365.76 1071.57 7 4 -5 -15 6655.67 715.596 1 4 -5 -14 456.341 192.852 1 4 -5 -14 465.476 355.779 7 4 -5 -13 13213.1 925.111 1 4 -5 -13 15368.5 1383.49 7 4 -5 -12 747.162 370.134 7 4 -5 -12 414.083 172.129 1 4 -5 -11 2765.33 643.202 7 4 -5 -10 9451.86 1050.45 7 4 -5 -9 2389.80 584.937 7 4 -5 -8 8677.36 957.557 7 -4 -5 7 4321.85 650.352 1 4 -5 -7 3863.00 690.075 7 -4 -5 6 30935.4 1588.34 1 4 -5 -6 28609.7 1670.38 7 -4 -5 5 9346.51 886.096 1 4 -5 -5 9821.93 1067.27 7 4 -5 -4 373.998 386.677 7 -4 -5 4 103.531 233.544 1 -4 -5 3 8341.99 827.480 1 4 -5 -3 8401.49 930.431 7 4 -5 -2 2488.38 608.608 7 -4 -5 2 1905.79 404.486 1 4 -5 -1 10552.0 967.763 7 -4 -5 1 9473.29 886.746 1 -4 -5 0 743.554 301.125 1 -4 -5 -1 721.479 274.100 1 -4 -5 -2 656.532 270.148 1 -4 -5 -3 1803.66 401.409 1 -4 -5 -4 1791.02 405.698 1 -4 -5 -5 3739.57 552.652 1 -4 -5 -6 193.669 135.679 1 -4 -5 -7 210.077 173.439 1 -4 -5 -8 716.749 293.823 1 -4 -5 -9 1062.58 330.886 1 -4 -5 -10 146.658 234.834 1 -4 -5 -11 9547.19 975.019 1 -4 -5 -12 3381.47 608.732 1 -4 -5 -13 249.942 223.884 1 -4 -5 -14 2394.65 559.727 1 -4 -5 -15 2796.41 620.695 1 -4 -5 -16 1771.26 548.855 1 -4 -5 -17 8042.44 1040.93 1 -4 -5 -18 5078.87 853.052 1 -4 -5 -19 2548.51 686.536 1 -4 5 -20 28502.9 1359.70 3 -4 -5 -20 28405.0 2110.93 1 -4 -5 -21 1047.37 497.560 1 -4 -5 -21 1093.89 282.502 2 -4 -5 -22 1574.24 511.358 1 -4 -5 -22 1300.15 311.836 2 -4 -5 -23 4240.40 616.096 2 -4 -5 -23 5378.68 1010.82 1 -4 -5 -24 1933.42 624.571 1 -4 -5 -24 1896.37 392.962 2 -4 -5 -25 117.685 126.734 2 -4 -5 -25 92.5889 280.371 1 -4 5 -26 62.9189 182.650 4 -4 -5 -26 168.700 430.427 1 -4 -5 -26-2.53904 139.430 2 -4 -5 -27 2920.45 800.333 1 -4 5 -27 2889.56 504.120 4 -4 -5 -27 2271.24 445.881 2 -4 -5 -28 2156.89 670.199 1 -4 5 -28 3572.40 575.045 4 -4 -5 -28 2877.18 500.438 2 -4 5 -29-5.80094 219.401 4 -4 -5 -29 667.081 468.849 1 -4 -5 -29 174.512 208.529 2 -4 -5 -30 2785.09 819.597 1 -4 5 -30 2359.11 487.713 4 -4 -5 -30 2192.41 429.923 2 -4 5 -31 18.6298 198.933 4 -4 -5 -31 283.666 238.173 2 -4 -5 -32 1809.62 400.097 2 -4 5 -32 2315.40 493.652 4 -4 5 -33 557.105 307.040 4 -4 -5 -33 358.212 235.201 2 -4 5 -34 1913.36 433.354 4 -4 -5 -34 1280.27 376.320 2 -4 5 -35 250.847 239.991 4 -4 -5 -35 83.8979 160.791 2 -4 5 -36 1747.59 410.046 4 -4 -5 -36 1124.45 335.250 2 -4 -5 -37-30.0131 156.014 2 -4 5 -37 79.7860 189.180 4 -4 5 -38 25.2769 217.271 4 -4 -5 -38 152.130 194.996 2 -4 5 -39 235.010 281.441 4 -4 -5 -39 36.0590 142.767 2 -4 -5 -40 802.821 270.301 2 -4 5 -40 883.128 308.858 4 -4 5 -40 728.794 212.839 2 -4 5 -41-18.9181 155.393 4 -4 -5 -41 331.509 188.087 2 -4 5 -42 115.954 155.849 4 -4 -5 -42-231.765 150.062 2 -4 -5 -43 17.6361 111.659 2 -4 5 -43 194.519 189.967 4 -4 -5 -44 143.670 130.410 2 4 5 44 94.7470 175.131 5 -4 5 -44 207.005 142.201 4 4 5 45 246.097 160.252 5 -4 5 -45 243.045 145.529 4 -4 -5 -45 289.156 147.605 2 4 5 46 84.2417 114.657 5 -4 -5 -46 11.3902 64.2204 2 4 5 47 475.863 155.857 5 -4 6 47-23.6244 82.4286 5 -4 6 46-127.467 117.157 5 -4 6 45 192.251 144.174 5 -4 6 44 14.8445 146.167 5 -4 6 43 198.976 170.365 5 -4 6 42 364.611 222.239 5 -4 6 41 712.303 299.752 5 -4 6 40 593.940 327.539 5 -4 6 39-41.4645 215.535 5 -4 6 38 224.646 230.452 5 -4 6 37 478.996 204.067 5 -4 6 36-243.980 343.931 5 -4 -6 36-58.1522 160.365 6 -4 -6 35 313.387 221.594 6 -4 6 35-208.657 252.802 5 -4 6 34-172.501 290.111 5 -4 -6 34 370.986 191.149 6 -4 6 33-73.3796 249.290 5 -4 -6 33 411.840 236.163 6 -4 6 32 475.500 319.799 5 -4 -6 32 1019.71 313.813 6 -4 -6 31 1055.72 324.797 6 -4 6 31 1290.42 370.414 5 -4 6 30 807.047 406.486 5 -4 -6 30 1399.82 375.823 6 -4 6 29 73.0441 220.720 5 -4 -6 29 147.689 195.415 6 4 -6 -29-125.568 405.263 7 -4 6 28-87.8241 285.637 5 4 -6 -28 334.686 356.284 7 -4 -6 28-30.7081 176.474 6 -4 6 27 2883.28 544.995 5 -4 -6 27 3286.71 548.865 6 4 -6 -27 2755.94 825.115 7 -4 6 26 51.3001 199.492 5 4 -6 -26 180.096 326.474 7 -4 -6 26 133.054 179.260 6 -4 6 25 614.628 249.461 5 4 -6 -25 490.971 308.586 7 -4 -6 25 534.389 253.705 6 -4 6 24 693.778 273.174 5 4 -6 -24 799.203 401.434 7 -4 -6 24 1100.61 327.623 6 4 -6 -23-66.5621 338.184 7 -4 6 23 194.717 242.329 5 -4 -6 23-196.083 254.261 6 -4 6 22 1071.40 275.207 5 -4 -6 22 1206.45 314.204 6 4 -6 -22 791.637 454.906 7 -4 6 21 166.507 174.040 5 -4 -6 21 200.130 195.576 6 4 -6 -21 140.469 279.059 7 -4 6 20 1571.97 395.909 5 4 -6 -20 1659.58 614.391 7 -4 -6 20 1635.88 393.562 6 4 -6 -19 3667.72 853.277 7 -4 -6 19 3879.27 570.174 6 4 -6 -18 2202.29 664.937 7 4 -6 -17 5729.01 971.957 7 4 -6 -16 604.404 359.598 7 4 -6 -15 328.677 295.323 7 4 -6 -14 1643.69 523.042 7 4 -6 -13-46.9201 178.444 7 4 -6 -12 2462.32 607.084 7 4 -6 -11 4408.77 783.165 7 4 -6 -10 5132.98 824.098 7 4 -6 -9 8570.61 1067.73 7 4 -6 -8 1419.77 492.927 7 4 -6 -7 2172.46 551.786 7 4 -6 -6 1111.83 411.764 7 -4 -6 6 1588.08 413.009 1 -4 -6 5 1403.42 395.448 1 4 -6 -5 1092.66 428.101 7 4 -6 -4 175.999 252.409 7 -4 -6 4 776.321 307.275 1 4 -6 -3 9400.74 1026.33 7 -4 -6 3 12168.0 1081.94 1 4 -6 -2 26682.0 1727.85 7 -4 -6 2 25906.0 1562.48 1 4 -6 -1 8662.30 1172.60 7 -4 -6 1 3728.50 640.562 1 -4 -6 0 713.688 292.302 1 4 -6 0 1084.26 502.476 7 -4 -6 -1 604.535 227.268 1 -4 -6 -2 225.312 237.344 1 -4 -6 -3 1548.16 392.495 1 -4 -6 -4 130.469 209.397 1 -4 -6 -5 800.366 437.442 1 -4 -6 -6 14851.0 1149.87 1 -4 -6 -7 765.541 302.674 1 -4 -6 -8 65.9079 190.181 1 -4 -6 -9 3487.67 586.908 1 -4 -6 -10 7794.64 902.203 1 -4 -6 -11 12242.8 1148.43 1 -4 -6 -12 1021.30 397.383 1 -4 -6 -13 1523.93 455.842 1 -4 -6 -14 9276.15 1085.71 1 -4 -6 -15 7077.98 979.680 1 -4 -6 -16 412.957 357.119 1 -4 6 -17 4439.64 528.004 3 -4 -6 -17 3706.47 744.818 1 -4 6 -18 2958.56 466.977 3 -4 -6 -18 2843.05 651.063 1 -4 -6 -19 271.217 149.883 2 -4 6 -19 215.871 154.605 3 -4 -6 -19 407.158 274.342 1 -4 6 -20 1804.00 373.391 3 -4 -6 -20 2369.61 683.293 1 -4 -6 -20 2006.01 390.115 2 -4 6 -21 9107.72 831.889 3 -4 -6 -21 9304.60 1290.12 1 -4 -6 -21 8162.88 740.235 2 -4 -6 -22 12127.7 1495.09 1 -4 -6 -22 11104.1 892.527 2 -4 -6 -23 2283.41 430.096 2 -4 -6 -23 3093.84 824.164 1 -4 -6 -24 1729.85 617.539 1 -4 -6 -24 1639.22 365.308 2 -4 -6 -25 50.1789 417.948 1 -4 -6 -25 218.869 188.316 2 -4 -6 -26 3415.08 518.664 2 -4 -6 -26 3486.49 901.984 1 -4 -6 -27 1708.65 654.905 1 -4 6 -27 1490.56 381.266 4 -4 -6 -27 1309.10 350.092 2 -4 6 -28 1199.61 363.563 4 -4 -6 -28 559.354 233.680 2 -4 -6 -28 935.415 537.435 1 -4 6 -29 347.696 242.516 4 -4 -6 -29 157.754 196.010 2 -4 6 -30 912.296 343.512 4 -4 -6 -30 891.981 305.440 2 -4 -6 -31 6220.63 686.895 2 -4 6 -31 7141.60 805.129 4 -4 6 -32 386.830 230.107 4 -4 -6 -32 18.2210 174.975 2 -4 -6 -33 134.045 174.748 2 -4 6 -33 205.326 235.513 4 -4 -6 -34 939.941 289.678 2 -4 6 -34 1552.12 403.251 4 -4 6 -35 115.849 202.916 4 -4 -6 -35 235.035 183.234 2 -4 6 -36 1574.29 396.941 4 -4 -6 -36 1035.78 290.430 2 -4 -6 -37-4.89187 147.771 2 -4 6 -37 285.446 189.019 4 -4 6 -38 586.224 278.047 4 -4 -6 -38 220.190 169.432 2 -4 6 -39 519.683 246.395 4 -4 -6 -39-28.1270 141.427 2 -4 6 -40 162.800 196.802 4 -4 -6 -40 388.714 169.109 2 -4 6 -41 1442.32 325.856 4 -4 -6 -41 1462.77 284.466 2 -4 6 -42 111.077 151.595 4 4 6 42 270.939 209.652 5 -4 -6 -42 355.367 139.382 2 -4 6 -43 96.9027 138.079 4 -4 -6 -43-50.6370 100.268 2 4 6 43 130.008 188.186 5 4 6 44 131.320 127.892 5 -4 -6 -44 24.6365 71.0910 2 4 6 45 234.868 145.198 5 -4 6 -45 88.4625 122.501 4 4 6 46-74.7627 92.7936 5 -4 7 45 231.980 130.043 5 -4 7 44-1.16971 110.306 5 -4 7 43 858.464 267.673 5 -4 7 42 511.496 227.594 5 -4 7 41 1096.94 284.107 5 -4 7 40 989.766 320.208 5 -4 7 39 227.921 239.117 5 -4 7 38 423.740 261.263 5 -4 7 37 575.019 312.893 5 -4 -7 37-43.9174 151.828 6 -4 7 36-199.015 196.283 5 -4 -7 36 12.4418 182.287 6 -4 -7 35 170.042 150.707 6 -4 7 35-50.3739 258.205 5 -4 7 34-822.618 317.451 5 -4 -7 34-60.0572 182.759 6 -4 7 33 79.5706 229.553 5 -4 -7 33 554.345 207.352 6 -4 7 32-378.571 256.133 5 -4 -7 32-24.6323 200.354 6 -4 7 31 2203.14 477.851 5 -4 -7 31 2361.14 455.728 6 -4 7 30-132.289 251.234 5 -4 -7 30 76.1261 214.395 6 -4 7 29 2700.79 552.730 5 -4 -7 29 4415.58 600.972 6 -4 7 28 705.702 277.105 5 -4 -7 28 903.859 340.373 6 4 -7 -27 116.188 346.037 7 -4 -7 27 83.1157 210.383 6 -4 7 27 237.694 216.661 5 -4 7 26 367.131 196.638 5 -4 -7 26 311.026 195.166 6 4 -7 -26 219.629 296.083 7 -4 7 25 781.760 294.904 5 4 -7 -25 967.825 464.283 7 -4 -7 25 1157.79 367.063 6 -4 7 24 1991.42 476.276 5 4 -7 -24 2061.18 729.822 7 -4 -7 24 2237.11 471.154 6 -4 7 23-400.818 267.266 5 -4 -7 23-412.155 240.283 6 -4 7 22 2040.51 471.381 5 4 -7 -22 1508.08 530.823 7 -4 -7 22 2486.13 476.199 6 -4 7 21 1406.85 342.331 5 4 -7 -21 1460.60 594.725 7 -4 -7 21 1807.87 417.098 6 -4 -7 20 2485.54 497.300 6 -4 7 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-7 2 18485.3 1628.49 7 -4 -7 -3 1841.38 528.571 1 -4 -7 -4 3393.65 630.717 1 -4 -7 -5 273.749 227.328 1 -4 -7 -6 2531.99 511.691 1 -4 -7 -7 1446.24 410.420 1 -4 -7 -8 3016.49 565.621 1 -4 -7 -9 7469.65 915.401 1 -4 -7 -10 1358.43 449.604 1 -4 -7 -11-95.7295 147.028 1 -4 -7 -12 234.492 256.354 1 -4 -7 -13 8953.22 1052.97 1 -4 -7 -14 317.785 274.470 1 -4 7 -14 146.327 150.589 3 -4 -7 -15 5039.92 831.255 1 -4 7 -15 5352.32 609.700 3 -4 -7 -16 356.862 274.098 1 -4 7 -16 169.760 116.398 3 -4 -7 -17 860.786 390.725 1 -4 7 -17 757.586 261.070 3 -4 7 -18 778.839 264.222 3 -4 -7 -18 512.974 173.129 2 -4 -7 -18 572.756 350.858 1 4 -7 19 5863.98 607.890 6 -4 7 -19 5723.08 665.675 3 -4 -7 -19 5482.49 571.231 2 -4 -7 -19 5763.49 1001.50 1 -4 7 -20 4.79519 142.682 3 -4 -7 -20 304.138 186.094 2 4 -7 20 43.2192 188.687 6 4 -7 21 7780.61 723.307 6 -4 7 -21 8065.17 787.180 3 -4 -7 -21 9181.66 786.085 2 -4 -7 -21 8233.35 1261.47 1 -4 -7 -22 1282.85 323.870 2 4 -7 22 1416.59 338.743 6 -4 -7 -22 1526.86 550.457 1 4 -7 23-14.4056 178.968 6 -4 -7 -23 148.428 182.646 2 -4 -7 -23 119.828 264.132 1 -4 -7 -24 1327.12 634.777 1 -4 -7 -24 1128.02 304.541 2 -4 -7 -25 5588.79 1138.22 1 -4 -7 -25 5709.32 672.122 2 -4 -7 -26 270.935 453.174 1 -4 -7 -26 252.434 212.264 2 -4 7 -27 221.941 233.499 4 -4 -7 -27 37.3054 125.805 2 -4 -7 -28 319.792 215.120 2 -4 7 -28 586.065 298.679 4 -4 -7 -29 2464.34 442.714 2 -4 7 -29 2621.00 487.119 4 -4 -7 -30 80.8081 179.018 2 -4 7 -30 73.2093 168.674 4 -4 7 -31 3210.49 552.886 4 -4 -7 -31 2808.62 470.561 2 -4 -7 -32 176.054 161.950 2 -4 7 -32 502.884 320.382 4 -4 7 -33 2667.85 500.486 4 -4 -7 -33 2637.27 427.153 2 -4 -7 -34 139.473 155.860 2 -4 7 -34-84.6745 193.027 4 -4 7 -35 121.920 193.241 4 -4 -7 -35 117.867 137.801 2 -4 -7 -36-31.1732 139.047 2 -4 7 -36 205.582 203.876 4 -4 7 -37 457.025 219.046 4 -4 -7 -37-25.3589 128.419 2 -4 7 -38 328.952 226.699 4 -4 -7 -38 66.6289 126.920 2 -4 7 -39 664.527 237.196 4 -4 -7 -39 312.400 141.769 2 4 7 40 723.591 277.769 5 -4 7 -40 690.199 267.707 4 -4 -7 -40 611.471 168.203 2 -4 7 -41 349.352 193.571 4 4 7 41 249.525 192.086 5 -4 -7 -41-155.543 109.043 2 -4 7 -42 517.938 197.412 4 4 7 42 814.040 218.509 5 4 7 43 541.100 195.471 5 -4 7 -43 442.977 171.794 4 4 7 44 38.0152 86.9108 5 -4 7 -44-62.8196 95.0720 4 -4 8 43-194.322 118.513 5 -4 8 42 263.484 156.932 5 -4 8 41 325.146 155.566 5 -4 8 40 182.882 162.765 5 -4 8 39 404.450 219.079 5 -4 8 38 238.202 203.567 5 -4 8 37 376.920 233.771 5 -4 -8 37 207.811 147.117 6 -4 8 36 314.614 247.164 5 -4 -8 36 293.995 194.105 6 -4 8 35 645.603 318.456 5 -4 -8 35-30.7129 181.166 6 -4 8 34 516.605 296.021 5 -4 -8 34 247.083 224.774 6 -4 8 33 198.034 258.196 5 -4 -8 33 201.622 194.358 6 -4 8 32 579.457 306.740 5 -4 -8 32-222.654 188.494 6 -4 8 31 928.998 319.295 5 -4 -8 31 527.777 231.272 6 -4 8 30 732.770 288.714 5 -4 -8 30 866.137 325.596 6 -4 8 29 21.5688 194.549 5 -4 -8 29-98.9514 218.186 6 -4 8 28 6.17486 261.997 5 -4 -8 28 1190.18 391.521 6 -4 8 27 3572.26 564.840 5 -4 -8 27 3857.57 579.170 6 -4 8 26 655.360 215.907 5 -4 -8 26 1391.13 389.090 6 -4 8 25 1855.68 451.662 5 -4 -8 25 1999.37 449.156 6 -4 8 24-193.393 293.524 5 4 -8 -24 152.652 391.078 7 -4 -8 24 269.473 255.803 6 -4 8 23 1134.96 349.827 5 4 -8 -23 509.628 435.754 7 -4 8 22 1405.95 337.160 5 -4 -8 22 1837.88 430.048 6 4 -8 -22 951.500 561.529 7 -4 8 21 278.353 214.023 5 4 -8 -21 16.6807 287.628 7 -4 -8 21 372.777 281.611 6 4 -8 -20 2100.71 786.764 7 -4 8 20 1429.26 376.025 5 -4 -8 20 2263.26 469.025 6 -4 -8 19 463.854 307.139 6 4 -8 -19-143.879 290.321 7 -4 8 19 449.754 287.332 5 4 -8 -18 3783.90 910.011 7 -4 -8 18 3769.46 559.786 6 -4 -8 17 1034.69 354.292 6 4 -8 -17 1022.27 503.453 7 4 -8 -16 4368.24 987.324 7 -4 -8 16 3686.07 579.732 6 -4 -8 15 261.443 226.470 6 4 -8 -15 329.331 287.550 7 -4 -8 14 2493.57 457.086 6 4 -8 -14 2008.64 609.207 7 4 -8 -13-28.1978 217.402 7 -4 -8 13 195.986 200.903 6 4 -8 -12 1690.44 560.051 7 -4 -8 12 2377.39 448.913 6 4 -8 -11 1038.18 447.816 7 -4 -8 11 1483.44 359.950 6 4 -8 -10 4999.93 902.116 7 -4 -8 10 4135.88 567.290 6 4 -8 -9 3699.71 820.212 7 -4 -8 9 3628.65 547.631 6 4 -8 -8 1743.06 598.788 7 4 -8 -7 17151.3 1623.78 7 4 -8 -6 10960.3 1310.53 7 4 -8 -5 1913.18 689.609 7 -4 -8 4 8585.63 987.093 1 4 -8 -4 7875.06 1038.48 7 4 -8 -3 1512.13 604.676 7 -4 -8 3 162.773 259.092 1 4 -8 -2-553.322 454.657 7 -4 -8 2 1022.70 402.651 1 4 -8 -1 2642.34 612.244 7 -4 -8 1 3680.84 676.697 1 -4 -8 0 1189.79 392.430 1 4 -8 0 1399.49 561.003 7 4 -8 1 101.691 193.205 7 -4 -8 -1 648.199 270.279 1 4 -8 2 1343.35 512.776 7 -4 -8 -2 2321.61 506.781 1 -4 -8 -3 2601.24 607.229 1 4 -8 3 1782.30 601.195 7 4 -8 4 6219.71 1004.35 7 -4 -8 -4 5818.51 834.649 1 -4 -8 -5 1462.72 454.980 1 -4 -8 -6 335.461 340.970 1 -4 -8 -7 2960.78 617.546 1 -4 8 -7 2634.00 408.055 3 -4 -8 -8 867.548 408.889 1 -4 8 -8 1073.97 296.463 3 -4 8 -9 1238.12 322.490 3 -4 -8 -9 1482.19 450.317 1 -4 8 -10 121.148 131.442 3 -4 -8 -10 451.132 337.587 1 -4 8 -11 4659.59 561.339 3 -4 -8 -11 4237.16 725.727 1 -4 8 -12 288.799 226.184 3 -4 -8 -12 198.061 165.412 1 -4 8 -13 565.012 227.473 3 -4 -8 -13 905.053 384.733 1 -4 -8 -14 1764.41 515.233 1 -4 8 -14 1575.01 337.369 3 -4 -8 -15 918.809 418.532 1 -4 8 -15 1033.53 315.332 3 -4 -8 -16 98.8353 216.602 1 -4 8 -16 179.136 208.333 3 -4 -8 -17 935.035 451.272 1 -4 8 -17 887.671 313.562 3 -4 8 -18 40.1349 115.466 3 -4 -8 -18 239.050 292.434 1 4 -8 18-280.700 236.571 6 -4 -8 -19 969.122 411.803 1 -4 8 -19 936.176 310.217 3 4 -8 19 888.142 272.703 6 4 -8 20 15.7678 158.301 6 -4 -8 -20 128.865 240.553 1 -4 8 -20-143.637 231.607 3 -4 -8 -21 515.074 382.463 1 -4 8 -21-295.082 265.641 3 4 -8 21-29.9646 202.120 6 -4 -8 -22 628.149 345.402 1 4 -8 22 874.570 323.057 6 -4 -8 -23 1823.00 646.260 1 4 -8 23 2273.04 408.048 6 4 -8 24 689.519 280.889 6 4 -8 25 1464.58 328.303 6 4 -8 26 81.8501 164.636 6 -4 8 -27 102.233 202.484 4 -4 8 -28 52.3458 206.745 4 -4 8 -29 489.399 254.419 4 -4 8 -30 9.20195 211.168 4 -4 8 -31 153.063 208.120 4 -4 8 -32 81.8649 240.295 4 -4 8 -33 586.302 255.810 4 -4 8 -34-70.9394 161.671 4 -4 8 -35 348.928 247.586 4 -4 8 -36 1666.76 392.614 4 4 8 37 77.5010 184.234 5 -4 8 -37 431.234 222.322 4 4 8 38 1048.29 286.298 5 -4 8 -38 1056.25 307.968 4 4 8 39-195.049 145.169 5 -4 8 -39 400.055 196.968 4 4 8 40 443.318 213.000 5 -4 8 -40 170.929 135.336 4 4 8 41 427.541 170.067 5 -4 8 -41 340.297 138.922 4 4 8 42-17.2089 101.459 5 -4 8 -42 96.8129 106.860 4 -4 8 -43 666.935 177.805 4 -4 9 41 66.1360 86.6207 5 -4 9 40-26.9962 97.4110 5 -4 9 39 73.6419 122.402 5 -4 9 38 162.732 155.565 5 -4 -9 38 243.317 109.833 6 -4 -9 37 224.985 154.578 6 -4 9 37 31.2985 134.166 5 -4 -9 36 16.2961 123.992 6 -4 9 36-87.9572 151.557 5 -4 9 35 1186.48 298.782 5 -4 -9 35 1725.46 326.122 6 -4 9 34 660.566 262.805 5 -4 -9 34 71.9836 165.266 6 -4 9 33 1920.95 386.453 5 -4 -9 33 1469.75 336.998 6 -4 9 32 656.445 281.939 5 -4 -9 32 516.163 259.132 6 -4 9 31 174.210 194.973 5 -4 -9 31 238.892 174.562 6 -4 9 30 1500.08 375.827 5 -4 -9 30 1720.78 394.147 6 -4 9 29 852.636 294.358 5 -4 -9 29 412.859 267.724 6 -4 9 28 128.964 199.274 5 -4 -9 28 495.357 310.652 6 -4 -9 27 3149.02 526.644 6 -4 9 27 3487.24 544.939 5 -4 9 26 1189.69 346.409 5 -4 -9 26 1097.29 367.957 6 -4 9 25 858.504 314.986 5 -4 -9 25 420.563 278.090 6 -4 9 24 155.255 227.022 5 -4 -9 24 201.656 190.090 6 -4 -9 23 42.7411 210.009 6 -4 -9 22 1038.96 341.199 6 -4 -9 21 2299.63 465.008 6 4 -9 -21 2272.27 699.722 7 4 -9 -20 556.148 412.881 7 -4 -9 20 150.428 202.505 6 4 -9 -19 1632.83 630.558 7 -4 -9 19 1332.69 368.685 6 -4 -9 18 230.416 189.218 6 4 -9 -18-386.946 367.440 7 4 -9 -17 2858.85 824.724 7 -4 -9 17 3006.47 547.663 6 4 -9 -16 811.435 486.426 7 -4 -9 16 1056.28 352.992 6 4 -9 -15 4943.47 1035.04 7 -4 -9 15 3949.73 590.066 6 4 -9 -14 60.3610 285.610 7 -4 -9 14 61.7824 207.617 6 4 -9 -13-112.919 312.488 7 -4 -9 13 24.3142 226.416 6 -4 -9 12 4087.36 618.971 6 4 -9 -12 4150.09 899.952 7 -4 -9 11 1254.34 381.098 6 4 -9 -11 179.998 260.652 7 4 -9 -10 6419.18 1041.74 7 -4 -9 10 5851.44 706.994 6 -4 -9 9 1303.09 384.863 6 4 -9 -9 1837.96 616.769 7 4 -9 -8 529.651 443.712 7 -4 -9 8 844.655 331.174 6 -4 -9 7 2271.09 502.457 6 4 -9 -7 824.325 409.213 7 4 -9 -6 6793.54 1081.50 7 -4 -9 6 7247.89 797.394 6 4 -9 -5 7203.02 1143.28 7 -4 -9 5 8238.97 845.367 6 4 -9 -4 4704.15 916.543 7 -4 -9 4 4900.40 661.176 6 -4 -9 3 3148.70 551.555 6 4 -9 -3 3217.95 795.076 7 -4 -9 2 4510.53 752.390 1 4 -9 -2 4601.84 934.789 7 -4 -9 2 5142.42 656.493 6 4 -9 -1 2615.70 798.885 7 -4 -9 1 1675.14 520.479 1 4 -9 0 5454.93 949.383 7 -4 -9 0 5600.63 817.155 1 -4 -9 -1 775.640 336.382 1 4 -9 1 2634.46 700.387 7 -4 9 -2 268.620 185.246 3 4 -9 2-119.384 242.792 7 -4 -9 -2 114.475 185.964 1 4 -9 3 380.943 320.626 7 -4 9 -3 708.643 264.982 3 -4 -9 -3 520.879 209.866 1 4 -9 4 861.398 459.958 7 -4 9 -4 900.017 305.259 3 4 -9 5 7217.08 1119.90 7 -4 9 -5 8063.39 740.669 3 -4 -9 -5 7447.47 986.461 1 4 -9 6 2136.77 812.818 7 -4 -9 -6 382.872 275.431 1 -4 9 -6 1553.04 399.934 3 4 -9 7 673.869 404.405 7 -4 -9 -7 1175.70 440.341 1 -4 9 -7 790.621 282.687 3 -4 -9 -8 497.547 342.838 1 -4 9 -8 641.183 262.517 3 -4 -9 -9 772.507 410.109 1 -4 9 -9 340.931 205.748 3 -4 -9 -10 385.395 308.520 1 -4 9 -10 809.801 277.822 3 -4 9 -11 162.902 190.958 3 -4 -9 -11 79.0220 204.254 1 -4 -9 -12 296.854 191.170 1 -4 9 -12-223.318 192.571 3 -4 -9 -13 448.107 322.013 1 -4 9 -13 288.115 183.415 3 -4 9 -14 44.5056 174.363 3 -4 -9 -14 128.176 196.512 1 -4 9 -15 3549.45 556.666 3 -4 -9 -15 3637.08 758.208 1 -4 -9 -16 706.185 382.550 1 -4 9 -16 358.711 218.638 3 4 -9 16 560.126 276.056 6 4 -9 17 2651.80 471.838 6 -4 9 -17 2748.31 491.117 3 -4 -9 -17 2836.20 697.535 1 -4 9 -18 2962.05 509.542 3 -4 -9 -18 2120.27 631.155 1 4 -9 18 3217.44 515.504 6 4 -9 19-18.8327 172.180 6 -4 9 -19 201.776 171.331 3 -4 -9 -19-347.862 324.990 1 4 -9 20-8.66730 221.937 6 -4 -9 -20 174.661 201.184 1 4 -9 21 343.812 268.155 6 4 -9 22 242.268 179.865 6 4 -9 23-76.1323 186.222 6 4 -9 24 465.866 219.942 6 4 -9 25 1053.33 303.533 6 4 -9 26 260.673 241.019 6 -4 9 -27 3123.62 514.859 4 4 -9 27 2815.24 467.835 6 -4 9 -28 120.688 199.884 4 4 -9 28 297.973 210.609 6 -4 9 -29 102.040 215.380 4 -4 9 -30-1.85960 210.439 4 -4 9 -31 278.220 204.298 4 -4 9 -32 136.633 194.035 4 4 9 33 1393.93 353.478 5 -4 9 -33 1226.26 324.899 4 -4 9 -34-11.1955 162.019 4 4 9 34 134.851 161.761 5 4 9 35 1848.47 347.101 5 -4 9 -35 1687.97 343.302 4 4 9 36 156.652 157.148 5 -4 9 -36 258.886 191.487 4 4 9 37-64.3600 128.158 5 -4 9 -37 29.0939 130.649 4 4 9 38 155.367 144.174 5 -4 9 -38 266.730 173.471 4 4 9 39 32.0220 95.0616 5 -4 9 -39 39.9675 125.049 4 -4 9 -40 14.5501 115.022 4 -4 9 -41-76.4105 99.0867 4 -4 -10 37 254.456 122.078 6 -4 -10 36-96.7385 116.366 6 -4 -10 35 1132.91 252.050 6 -4 -10 34 151.584 135.041 6 -4 -10 33 83.5938 143.258 6 -4 -10 32 108.132 183.508 6 -4 -10 31 128.177 172.909 6 -4 -10 30 167.014 173.849 6 -4 -10 29 171.169 232.849 6 -4 -10 28 126.529 241.447 6 -4 -10 27 755.373 289.278 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285.434 5 -5 -7 27-20.1785 174.722 6 -5 7 26 2603.40 556.249 5 5 -7 -26 2131.91 714.635 7 -5 -7 26 3246.44 538.285 6 -5 7 25 3238.56 575.788 5 5 -7 -25 4275.00 1095.74 7 -5 -7 25 3143.79 544.670 6 -5 -7 24 661.570 277.309 6 -5 7 24 28.4428 241.918 5 5 -7 -24 450.967 429.874 7 5 -7 -23 9169.94 1480.99 7 -5 7 23 7789.83 852.081 5 -5 -7 23 8693.86 851.532 6 -5 7 22-79.7709 184.338 5 -5 -7 22 73.0681 196.823 6 -5 -7 21 1590.19 397.456 6 -5 7 21 1354.16 351.719 5 5 -7 -21 1504.00 612.022 7 -5 7 20 665.844 256.353 5 5 -7 -20 1077.92 603.204 7 -5 -7 20 577.045 259.787 6 -5 7 19-100.227 238.165 5 5 -7 -19 161.148 379.507 7 -5 -7 19 136.077 183.248 6 5 -7 -18 1503.40 607.499 7 -5 7 18 911.599 290.319 5 -5 -7 18 707.541 262.743 6 -5 7 17 473.929 226.924 5 5 -7 -17 813.178 494.581 7 -5 -7 17 320.958 199.295 6 -5 7 16 446.699 259.410 5 -5 -7 16 739.960 282.411 6 5 -7 -16 516.754 335.176 7 -5 -7 15-72.5830 153.165 6 5 -7 -15 249.509 352.216 7 5 -7 -14-74.6937 224.517 7 -5 -7 14 71.7868 180.894 6 5 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156.669 5 -5 7 -43 141.428 107.991 4 -5 7 -44 323.669 120.260 4 -5 8 43-5.89263 78.7754 5 -5 8 42 367.647 144.751 5 -5 8 41 235.882 143.053 5 -5 8 40 473.260 192.934 5 -5 8 39-14.8332 136.585 5 -5 8 38 845.089 282.824 5 -5 -8 38 725.246 182.555 6 -5 8 37 146.137 164.133 5 -5 -8 37-23.2905 124.562 6 -5 8 36 367.658 260.884 5 -5 -8 36-37.1819 141.117 6 -5 8 35 444.374 261.518 5 -5 -8 35 301.389 218.947 6 -5 8 34 1114.72 339.089 5 -5 -8 34 339.445 197.875 6 -5 8 33 1673.03 408.077 5 -5 -8 33 1568.64 357.086 6 -5 8 32 1763.64 426.940 5 -5 -8 32 1136.12 345.919 6 -5 8 31 583.454 310.682 5 -5 -8 31 291.942 213.147 6 -5 8 30 1440.56 393.896 5 -5 -8 30 1055.10 325.211 6 -5 8 29 2915.96 533.369 5 -5 -8 29 2744.61 480.018 6 -5 8 28 461.761 283.717 5 -5 -8 28 490.710 295.397 6 -5 8 27 1067.34 370.723 5 -5 -8 27 997.843 333.687 6 -5 8 26-5.44411 205.328 5 -5 -8 26 102.748 235.982 6 -5 8 25 40.6682 218.714 5 -5 -8 25 78.2358 185.839 6 -5 8 24-126.176 182.496 5 -5 -8 24 417.187 306.823 6 -5 8 23 349.768 272.366 5 5 -8 -23 523.850 426.052 7 -5 -8 23-24.7231 221.688 6 -5 8 22-499.491 328.568 5 -5 -8 22-266.608 196.720 6 5 -8 -22-896.420 557.371 7 -5 8 21-20.4897 230.381 5 -5 -8 21 209.594 223.293 6 5 -8 -21 64.2004 273.437 7 -5 8 20-225.822 240.394 5 -5 -8 20 59.6876 187.089 6 5 -8 -20 360.282 477.887 7 -5 8 19 522.593 257.079 5 -5 -8 19 685.229 316.262 6 5 -8 -19 66.0409 290.815 7 -5 -8 18 4373.10 611.257 6 5 -8 -18 3811.26 937.491 7 -5 8 18 3652.80 561.684 5 5 -8 -17 5084.25 1045.23 7 -5 -8 17 4794.06 646.241 6 -5 -8 16-192.351 257.052 6 5 -8 -16 322.512 356.865 7 5 -8 -15 2408.30 741.535 7 -5 -8 15 2029.30 436.167 6 -5 -8 14 611.676 294.033 6 5 -8 -14 412.734 416.875 7 -5 -8 13 907.010 287.409 6 5 -8 -13 1030.43 493.538 7 5 -8 -12 2017.17 614.382 7 -5 -8 12 2146.83 455.948 6 5 -8 -11 163.961 273.310 7 -5 -8 11 699.780 330.706 6 5 -8 -10 9875.53 1351.66 7 -5 -8 10 8082.79 819.640 6 5 -8 -9 451.750 463.987 7 -5 -8 9 294.741 261.350 6 5 -8 -8 57.4267 216.785 7 -5 -8 8 1176.49 412.076 6 5 -8 -7 3921.33 850.750 7 -5 -8 7 4324.87 602.367 6 5 -8 -6 921.747 533.340 7 -5 -8 6 1836.03 477.392 6 5 -8 -5 2364.84 662.786 7 -5 -8 4 535.062 289.491 1 5 -8 -4 384.864 411.701 7 -5 -8 3 218.118 189.449 1 5 -8 -3-850.290 415.008 7 -5 -8 2 2796.86 620.462 1 5 -8 -2 1621.16 547.255 7 -5 -8 1 1260.02 362.292 1 5 -8 -1 2631.94 692.733 7 -5 -8 0 1148.75 456.733 1 5 -8 0 980.827 496.049 7 5 -8 1 3827.52 807.375 7 -5 -8 -1 3794.39 711.763 1 -5 -8 -2 2524.28 738.395 1 5 -8 2 1917.09 623.615 7 -5 -8 -3 10942.4 1211.63 1 5 -8 3 9537.58 1245.59 7 -5 8 -3 9706.74 804.334 3 5 -8 4 3823.62 962.729 7 -5 8 -4 2773.09 480.702 3 5 -8 5 2706.81 710.748 7 -5 8 -5 3225.35 467.413 3 -5 -8 -5 2824.65 663.427 1 -5 -8 -6 462.082 311.383 1 -5 8 -6 716.534 296.142 3 -5 -8 -7 2.08641 174.342 1 -5 8 -7 73.9307 137.768 3 -5 -8 -8-344.782 282.014 1 -5 8 -8-73.6748 130.984 3 -5 8 -9 662.135 253.599 3 -5 -8 -9 636.045 355.262 1 -5 8 -10 222.019 168.062 3 -5 -8 -10 176.147 237.307 1 -5 -8 -11 724.437 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168.215 143.295 5 -5 -9 35 539.230 220.114 6 -5 9 34 188.284 152.196 5 -5 -9 34-169.489 167.092 6 -5 9 33 801.022 253.240 5 -5 -9 33 441.413 209.948 6 -5 9 32-117.062 159.977 5 -5 -9 32-191.542 203.354 6 -5 9 31 694.114 275.511 5 -5 -9 31 461.069 245.303 6 -5 9 30 312.295 207.582 5 -5 -9 30 34.0357 188.612 6 -5 9 29 442.152 291.922 5 -5 -9 29 114.791 203.120 6 -5 9 28 2978.94 496.656 5 -5 -9 28 2322.15 470.414 6 -5 9 27 163.498 184.753 5 -5 -9 27-182.696 269.517 6 -5 9 26 619.307 278.524 5 -5 -9 26 371.138 243.703 6 -5 9 25 1028.96 305.589 5 -5 -9 25 936.506 338.276 6 -5 -9 24 3821.10 607.864 6 -5 9 24 4031.42 584.860 5 -5 -9 23 4895.22 665.999 6 -5 9 23 5842.06 692.787 5 -5 -9 22 269.850 246.242 6 -5 -9 21 68.1467 238.729 6 -5 -9 20 3159.00 563.680 6 -5 -9 19 1060.73 346.263 6 5 -9 -19 1850.45 738.759 7 5 -9 -18 105.316 357.353 7 -5 -9 18-172.949 246.097 6 5 -9 -17 5588.96 1096.42 7 -5 -9 17 4883.59 660.964 6 5 -9 -16 794.541 517.906 7 -5 -9 16 947.243 288.059 6 5 -9 -15 950.149 507.387 7 -5 -9 15 744.680 325.056 6 5 -9 -14 364.900 408.140 7 -5 -9 14 661.740 351.461 6 5 -9 -13 8981.30 1379.97 7 -5 -9 13 9275.62 902.680 6 5 -9 -12 7318.09 1273.01 7 -5 -9 12 7136.49 796.454 6 5 -9 -11 469.543 448.885 7 -5 -9 11 252.756 256.991 6 5 -9 -10 138.093 452.668 7 -5 -9 10 331.227 276.551 6 5 -9 -9 991.454 539.407 7 -5 -9 9 1164.87 370.862 6 -5 -9 8 4401.25 651.627 6 5 -9 -8 3020.97 773.227 7 5 -9 -7 4126.85 945.022 7 -5 -9 7 4204.82 620.226 6 5 -9 -6 256.363 403.078 7 -5 -9 6 3348.19 635.954 6 5 -9 -5 6826.94 1173.91 7 -5 -9 5 8882.68 904.056 6 5 -9 -4 5114.26 1040.51 7 -5 -9 4 3856.69 582.464 6 5 -9 -3 1339.94 591.936 7 -5 -9 3 1038.69 361.972 6 -5 -9 2 1791.76 507.246 1 5 -9 -2 938.292 435.781 7 -5 -9 1 808.440 407.943 1 5 -9 -1 682.827 494.820 7 5 -9 0 554.402 452.532 7 -5 -9 0 1068.00 469.775 1 5 -9 1 743.985 509.038 7 -5 -9 -1 218.511 257.786 1 5 -9 2-213.431 250.359 7 -5 -9 -2 131.671 220.889 1 -5 9 -2 143.322 127.088 3 -5 -9 -3 458.105 337.409 1 5 -9 3-178.598 295.803 7 -5 9 -3 156.392 149.188 3 5 -9 4 1558.30 611.690 7 -5 -9 -4 3207.41 720.969 1 -5 9 -4 1911.71 395.285 3 -5 -9 -5 4067.21 798.997 1 5 -9 5 5751.27 1075.90 7 -5 9 -5 4179.13 584.974 3 -5 -9 -6 144.980 295.222 1 -5 9 -6 470.691 241.372 3 5 -9 7 2015.03 668.785 7 -5 -9 -7 1615.63 527.531 1 -5 9 -7 1871.19 400.595 3 -5 9 -8 542.034 278.938 3 -5 -9 -8-21.5177 174.957 1 5 -9 8 400.390 449.091 7 -5 9 -9 1547.41 371.656 3 -5 -9 -9 1260.94 459.872 1 -5 9 -10-141.252 158.339 3 -5 -9 -10 24.8715 195.100 1 -5 -9 -11 718.187 399.932 1 -5 9 -11 944.248 313.178 3 -5 9 -12 597.658 276.542 3 -5 -9 -12 1473.07 517.508 1 -5 9 -13 1411.32 384.528 3 -5 -9 -13 1911.61 566.035 1 -5 9 -14-98.8033 164.271 3 -5 -9 -14 188.316 292.384 1 -5 9 -15 46.4957 160.320 3 -5 -9 -15 26.2600 247.930 1 -5 9 -16 478.721 261.034 3 -5 -9 -16 749.432 395.204 1 -5 9 -17 2447.23 493.052 3 5 -9 17 2041.49 435.159 6 -5 -9 -17 2147.59 596.054 1 -5 9 -18 575.996 253.791 3 5 -9 18 488.363 247.680 6 -5 9 -19-236.536 245.885 3 5 -9 19 206.038 187.232 6 5 -9 20 3820.14 571.936 6 -5 9 -20 4528.88 623.344 3 5 -9 21 206.994 208.626 6 5 -9 22-226.004 217.109 6 5 -9 23 482.398 271.270 6 5 -9 24 1469.81 325.796 6 5 -9 25 796.992 282.932 6 5 -9 26 434.763 243.595 6 -5 9 -27 506.077 251.207 4 -5 9 -28 3129.43 492.855 4 -5 9 -29 744.054 271.062 4 -5 9 -30 669.026 281.993 4 -5 9 -31 628.287 257.259 4 -5 9 -32 210.834 193.838 4 -5 9 -33-167.214 187.123 4 5 9 34-109.129 165.224 5 -5 9 -34-395.189 242.039 4 5 9 35 373.202 191.312 5 -5 9 -35 514.076 223.599 4 5 9 36 453.500 186.675 5 -5 9 -36 345.328 172.244 4 -5 9 -37 2509.98 368.361 4 5 9 37 2338.10 313.758 5 -5 9 -38 194.780 156.259 4 -5 9 -39 188.532 124.507 4 -5 9 -40 62.5697 83.7386 4 -5 -10 37-42.3086 101.227 6 -5 -10 36-41.0933 101.944 6 -5 -10 35 699.547 185.539 6 -5 -10 34 116.647 136.661 6 -5 -10 33 870.580 232.488 6 -5 -10 32 297.463 190.999 6 -5 -10 31 325.264 181.854 6 -5 -10 30 322.509 221.079 6 -5 -10 29-29.0300 172.341 6 -5 -10 28 76.2515 196.434 6 -5 -10 27 1566.10 368.834 6 -5 -10 26 799.841 300.875 6 -5 -10 25 1353.20 354.032 6 -5 -10 24 298.371 257.769 6 -5 -10 23 1813.86 390.973 6 -5 -10 22 109.705 210.459 6 -5 -10 21 1993.14 439.121 6 -5 -10 20 759.857 325.879 6 -5 -10 19 840.855 353.157 6 -5 -10 18 645.118 301.098 6 -5 -10 17 448.482 259.699 6 -5 -10 16 1360.76 395.220 6 -5 -10 15 2352.01 491.695 6 -5 -10 14-81.2000 241.519 6 5 -10 -13 415.135 377.704 7 -5 -10 13 494.578 309.457 6 5 -10 -12 157.884 239.085 7 -5 -10 12 212.696 282.736 6 5 -10 -11 1047.70 559.899 7 -5 -10 11 431.935 272.667 6 5 -10 -10-137.578 321.968 7 -5 -10 10 194.255 223.576 6 5 -10 -9 606.671 356.025 7 -5 -10 9 1373.76 383.661 6 5 -10 -8 2048.25 714.400 7 -5 -10 8 1927.34 452.984 6 5 -10 -7 169.885 313.091 7 -5 -10 7 993.186 391.358 6 5 -10 -6 1219.38 562.063 7 -5 -10 6 3572.42 595.116 6 5 -10 -5 931.673 584.655 7 -5 -10 5 1877.57 498.527 6 5 -10 -4 363.958 359.922 7 -5 -10 4 4533.91 703.320 6 5 -10 -3 6322.68 1152.55 7 -5 -10 3 7206.92 803.317 6 5 -10 -2 4378.71 1001.98 7 5 -10 -1 9196.91 1323.89 7 5 -10 0 4998.05 1088.20 7 -5 10 0 4101.08 629.722 3 -5 -10 -1 3259.58 721.980 1 -5 10 -1 3553.44 553.773 3 5 -10 1 2760.63 785.131 7 -5 -10 -2 322.551 312.191 1 -5 10 -2 1334.75 458.529 3 5 -10 3 185.374 261.685 7 -5 -10 -3 390.172 300.228 1 -5 10 -3 154.195 229.395 3 -5 -10 -4 2196.19 604.902 1 -5 10 -4 1960.10 448.506 3 5 -10 4 1551.59 590.928 7 -5 -10 -5-119.061 191.779 1 -5 10 -5 492.854 294.417 3 5 -10 6 7.94230 266.445 7 -5 -10 -6 76.7820 186.203 1 -5 10 -6 264.439 194.176 3 5 -10 7 244.153 390.772 7 -5 -10 -7 426.459 407.358 1 -5 10 -7 156.499 192.072 3 5 -10 8 4125.54 1021.33 7 -5 10 -8 4828.27 657.289 3 -5 -10 -8 4031.14 777.575 1 5 -10 9 850.684 722.224 7 -5 -10 -9-220.862 167.436 1 -5 10 -9 444.437 282.171 3 5 -10 10 579.925 388.425 7 -5 10 -10 590.685 268.529 3 -5 -10 -10 701.580 425.323 1 5 -10 11 1603.63 614.388 7 -5 -10 -11 891.917 392.981 1 -5 10 -11 1465.94 357.934 3 5 -10 12-18.3440 304.669 7 -5 10 -12 196.798 153.346 3 -5 10 -13 25.2875 189.337 3 -5 10 -14 366.487 221.529 3 -5 10 -15 1021.29 326.169 3 5 -10 15 920.738 321.363 6 -5 10 -16 860.051 311.054 3 5 -10 16 937.224 375.400 6 -5 10 -17 1003.09 284.305 3 5 -10 17 710.874 272.168 6 -5 10 -18-85.5891 224.827 3 5 -10 18-354.901 268.335 6 -5 10 -19-104.353 218.894 3 5 -10 19-84.2699 214.358 6 5 -10 20-81.9186 189.123 6 5 -10 21 500.120 250.983 6 5 -10 22 131.271 195.387 6 5 -10 23 386.999 258.410 6 5 -10 24 330.266 173.761 6 5 -10 25 374.961 237.423 6 5 -10 26 242.455 232.755 6 -5 10 -26 76.1033 202.525 4 5 -10 27 2159.50 376.478 6 -5 10 -27 2444.68 446.724 4 -5 10 -28 309.233 230.410 4 -5 10 -29 479.894 226.101 4 -5 10 -30 176.727 157.595 4 -5 10 -31 106.445 178.218 4 -5 10 -32-19.9524 149.759 4 -5 10 -33 482.640 213.534 4 -5 10 -34 18.9751 129.115 4 -5 10 -35 652.248 214.283 4 -5 10 -36 97.1474 109.108 4 -5 10 -37 134.061 101.439 4 -5 -11 35 51.6884 91.5984 6 -5 -11 34 12.7839 107.909 6 -5 -11 33 81.1422 117.128 6 -5 -11 32 308.690 150.096 6 -5 -11 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157.626 3 -5 11 -5 323.827 233.621 3 -5 11 -6 1008.89 321.354 3 -5 11 -7 248.092 262.033 3 -5 11 -8-7.87799 156.484 3 -5 11 -9 992.198 344.726 3 -5 11 -10 196.096 192.678 3 -5 11 -11 763.136 292.269 3 -5 11 -12 294.224 224.248 3 5 -11 12 525.933 273.586 6 -5 11 -13 602.821 261.883 3 5 -11 13 137.547 232.499 6 5 -11 14 1709.91 409.190 6 -5 11 -14 893.970 340.274 3 -5 11 -15 214.935 233.826 3 5 -11 15-351.937 253.985 6 5 -11 16 75.3549 190.245 6 -5 11 -16-22.2514 237.811 3 -5 11 -17-589.552 257.440 3 5 -11 17 184.860 225.989 6 5 -11 18 201.670 210.482 6 -5 11 -18-17.3690 238.005 3 5 -11 19 65.8734 192.485 6 5 -11 20-241.463 209.198 6 5 -11 21-102.202 202.271 6 5 -11 22-197.050 214.648 6 5 -11 23 95.7733 216.460 6 5 -11 24-105.092 162.430 6 -5 11 -25 39.4826 144.225 4 5 -11 25 358.613 216.169 6 -5 11 -26 1177.81 321.936 4 5 -11 26 1231.88 301.069 6 -5 11 -27 44.1712 143.788 4 5 -11 27 160.745 143.658 6 -5 11 -28 146.462 157.482 4 5 -11 28-37.5939 144.534 6 -5 11 -29-50.5059 136.233 4 -5 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21 980.386 297.727 6 5 -12 22 294.610 217.764 6 -5 12 -23 39.9705 137.704 4 5 -12 23 411.763 222.075 6 -5 12 -24-4.23850 132.102 4 5 -12 24 201.001 175.539 6 5 -12 25 314.070 175.565 6 -5 12 -25 114.726 142.421 4 5 -12 26-409.036 156.809 6 -5 12 -26 28.0822 135.879 4 5 -12 27 355.457 190.058 6 -5 12 -27 72.2535 137.102 4 -5 12 -28 226.306 149.831 4 5 -12 28 178.915 110.912 6 -5 12 -29 176.223 135.239 4 -5 12 -30 386.112 172.648 4 -5 12 -31 146.456 109.400 4 -5 -13 30-14.6299 75.9826 6 -5 -13 29 281.094 132.628 6 -5 -13 28 383.170 156.421 6 -5 13 28 329.396 149.720 3 -5 -13 27 122.735 126.385 6 -5 -13 26-72.1007 114.910 6 -5 -13 25 477.628 189.766 6 -5 -13 24 104.391 122.033 6 -5 -13 23-76.8192 130.288 6 -5 -13 22 442.217 211.860 6 -5 -13 21-85.7585 173.765 6 -5 -13 20 186.593 192.140 6 -5 -13 19 446.694 243.354 6 -5 -13 18 75.9983 167.675 6 -5 -13 17 35.0502 199.856 6 -5 -13 16 2664.72 455.246 6 -5 -13 15 207.832 274.211 6 -5 13 15 434.934 233.646 3 -5 -13 14 872.478 318.367 6 -5 13 14 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422.649 7 -7 -6 4 1209.47 472.160 1 7 -6 -3 385.367 288.797 7 -7 -6 3 119.878 216.130 1 -7 -6 2 376.153 361.871 1 7 -6 -2 346.953 292.287 7 -7 -6 1 9582.87 1224.01 1 7 -6 -1 4843.36 956.652 7 -7 -6 0 31876.8 2061.90 1 7 -6 0 31592.1 2152.09 7 -7 -6 -1 8029.92 1113.70 1 7 -6 1 14855.6 1594.09 7 -7 -6 -2 4092.84 758.234 1 7 -6 2 3971.88 822.976 7 7 -6 3 304.638 289.904 7 -7 -6 -3 223.484 234.924 1 -7 -6 -4 218.349 398.346 1 -7 -6 -5 4418.66 797.368 1 -7 6 -5 4798.27 539.249 3 -7 -6 -6 1102.35 244.220 2 -7 -6 -6 1562.11 518.847 1 -7 6 -6 1406.45 349.213 3 -7 -6 -7 550.104 226.352 2 -7 -6 -7 651.821 355.171 1 -7 6 -7 240.651 215.114 3 -7 -6 -8 1688.25 531.462 1 -7 6 -8 1244.20 317.434 3 -7 -6 -8 1927.15 340.055 2 -7 6 -9 1354.00 309.438 3 -7 -6 -9 1269.51 494.385 1 -7 -6 -9 878.515 240.547 2 -7 -6 -10 393.634 206.061 2 -7 6 -10 65.9465 146.081 3 -7 -6 -10 572.727 401.093 1 -7 6 -11 3192.40 506.155 3 -7 -6 -11 3657.64 737.769 1 -7 -6 -11 4185.99 524.023 2 -7 -6 -12 57.9771 95.7328 2 -7 6 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319.918 272.890 4 -7 -6 -28 234.922 192.370 2 -7 6 -29 92.3082 189.577 4 -7 -6 -29 475.511 203.753 2 -7 -6 -30-65.8383 183.487 2 -7 6 -30-48.3237 189.689 4 -7 -6 -31 1001.92 352.843 2 -7 6 -31 1732.98 412.339 4 -7 6 -32 184.243 189.802 4 -7 -6 -32-92.9723 198.943 2 -7 6 -33 204.153 189.072 4 -7 -6 -33-257.383 188.153 2 -7 6 -34 1292.08 354.849 4 -7 -6 -34 1118.13 318.599 2 -7 6 -35 294.263 228.253 4 -7 -6 -35 565.933 229.658 2 -7 6 -36 40.0779 163.233 4 -7 -6 -36 307.764 172.814 2 -7 6 -37-113.050 158.510 4 -7 -6 -37 105.201 133.093 2 -7 6 -38-110.037 175.218 4 -7 -6 -38 127.019 141.768 2 -7 6 -39 289.339 165.372 4 -7 -6 -39 75.1726 123.008 2 -7 6 -40 481.851 186.074 4 -7 -6 -40 356.470 154.334 2 -7 6 -41-60.5464 112.842 4 -7 -6 -41 46.2674 81.5477 2 -7 6 -42 463.766 152.131 4 7 6 42 528.639 161.781 5 -7 7 42-9.64130 91.5652 5 -7 7 41 476.243 156.031 5 -7 7 40 24.6441 108.646 5 -7 7 39 231.365 133.668 5 -7 7 38-148.212 172.295 5 -7 7 37 72.6299 172.527 5 -7 -7 37 33.0743 124.618 6 -7 7 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7 -7 -7 19 452.697 298.984 6 -7 7 18 2254.17 484.415 5 7 -7 -18 2419.87 803.362 7 -7 -7 18 2062.64 457.820 6 7 -7 -17 4014.07 986.211 7 -7 -7 17 3527.67 562.986 6 -7 7 17 3986.68 600.364 5 -7 7 16 1042.51 327.544 5 7 -7 -16 1094.09 579.545 7 -7 -7 16 849.459 289.092 6 -7 7 15 587.657 292.207 5 7 -7 -15 539.193 454.491 7 -7 -7 15 1037.28 304.012 6 -7 7 14 1135.47 351.613 5 7 -7 -14 1524.35 638.066 7 -7 -7 14 1246.58 341.964 6 -7 7 13 991.709 303.921 5 7 -7 -13 1220.62 526.731 7 -7 -7 13 1558.69 394.684 6 -7 -7 13 1362.72 337.538 2 -7 -7 12 1406.39 338.896 2 -7 7 12 765.094 241.130 5 7 -7 -12 1669.37 568.934 7 -7 -7 12 917.546 339.206 6 7 -7 -11 3944.31 915.334 7 -7 -7 11 2783.24 476.969 6 -7 7 11 2732.35 454.599 5 -7 -7 11 3882.10 495.849 2 -7 -7 10 1213.24 427.699 6 -7 7 10 621.615 292.026 5 -7 -7 10 437.760 198.038 2 7 -7 -10 149.903 347.136 7 7 -7 -9 7765.45 1199.19 7 -7 -7 9 7307.63 792.611 6 -7 -7 9 6887.85 646.318 2 -7 -7 8 1923.29 356.289 2 7 -7 -8 2341.66 793.313 7 -7 -7 8 2496.26 464.587 6 -7 -7 7 318.109 178.041 2 7 -7 -7 632.900 455.996 7 -7 -7 7 269.832 229.697 6 -7 -7 6 2029.78 477.723 6 -7 -7 6 1405.61 307.850 2 7 -7 -6 797.929 440.957 7 7 -7 -5 2031.99 699.360 7 -7 -7 5 2950.32 535.487 6 -7 -7 5 2017.93 368.090 2 -7 -7 4 4357.65 810.864 1 7 -7 -4 3457.51 826.507 7 -7 -7 4 4544.24 560.570 6 -7 -7 4 4601.05 500.607 2 -7 -7 3 145.893 128.778 2 -7 -7 3-30.6499 265.359 1 -7 -7 2 2149.71 636.552 1 -7 -7 2 1863.40 390.449 2 -7 -7 1 9346.59 1204.21 1 7 -7 -1 8692.00 1237.80 7 -7 -7 1 10767.4 767.437 2 -7 -7 0 3407.16 768.993 1 -7 -7 0 4579.06 526.941 2 -7 -7 -1 5566.02 974.923 1 7 -7 1 7343.69 1210.67 7 -7 -7 -1 6853.72 611.012 2 -7 -7 -2 8811.75 1392.83 1 7 -7 2 8098.06 1396.46 7 -7 -7 -2 6567.27 714.703 2 -7 -7 -3 38644.2 2411.70 1 7 -7 3 39785.6 2556.95 7 -7 7 -3 37369.1 1603.88 3 -7 -7 -3 32778.6 1336.22 2 -7 -7 -4 2574.58 906.582 1 -7 -7 -4 2267.66 455.464 2 -7 -7 -5 10426.4 1233.75 1 7 -7 5 11207.7 1420.73 7 -7 7 -5 11354.4 882.392 3 -7 -7 -5 11864.8 836.986 2 -7 -7 -6 193.817 169.629 2 -7 -7 -6-184.798 249.067 1 -7 -7 -7 84.8917 89.6720 2 -7 -7 -7 273.946 298.367 1 -7 7 -7 196.310 210.116 3 -7 -7 -8 400.312 202.042 2 -7 -7 -8 870.546 427.240 1 -7 7 -8 232.140 191.492 3 -7 -7 -9 529.846 192.259 2 -7 -7 -9 497.836 334.481 1 -7 7 -9 425.845 224.902 3 -7 -7 -10 1580.00 331.736 2 -7 -7 -10 1584.09 539.407 1 -7 7 -10 1266.15 326.512 3 -7 -7 -11 171.913 148.377 2 -7 7 -11 192.508 179.733 3 -7 -7 -11 155.982 286.641 1 -7 -7 -12 98.5710 105.393 2 -7 7 -12 126.740 163.321 3 -7 -7 -12 279.447 262.101 1 -7 7 -13 5012.00 629.575 3 -7 -7 -13 3630.10 784.463 1 -7 -7 -13 4205.73 529.312 2 -7 -7 -14 185.566 131.124 2 -7 7 -14 430.886 265.003 3 -7 -7 -14 317.543 226.142 1 -7 -7 -15 1127.56 286.482 2 -7 7 -15 833.715 310.797 3 -7 -7 -15 1103.76 514.630 1 -7 -7 -16 1215.89 305.468 2 -7 7 -16 1026.37 295.076 3 -7 -7 -16 969.901 397.234 1 -7 7 -17 300.523 172.758 3 -7 -7 -17 713.583 277.212 2 -7 -7 -17 388.716 292.239 1 -7 -7 -18 5909.42 1061.80 1 -7 7 -18 7072.95 821.675 3 -7 -7 -18 7539.57 759.197 2 -7 7 -19 84.0772 164.594 3 -7 -7 -19 303.224 360.975 1 -7 -7 -19 185.472 145.753 2 -7 -7 -20 302.873 206.986 2 -7 7 -20 233.999 199.293 3 -7 -7 -21 5624.05 685.273 2 -7 -7 -22-12.5682 158.269 2 -7 -7 -23 2435.04 463.684 2 -7 -7 -24-89.9153 215.095 2 -7 -7 -25 55.9091 176.545 2 -7 -7 -26 2299.14 435.116 2 -7 7 -27 1818.28 429.853 4 -7 -7 -27 1123.86 330.105 2 -7 7 -28 275.990 230.338 4 -7 -7 -28 382.257 199.354 2 -7 -7 -29-144.478 199.573 2 -7 7 -29 220.797 248.615 4 -7 7 -30-133.830 212.109 4 -7 -7 -30-76.5664 145.777 2 -7 7 -31 888.955 294.815 4 -7 -7 -31 434.422 190.283 2 -7 7 -32 230.810 224.867 4 -7 -7 -32 411.684 214.422 2 -7 7 -33 2520.65 459.294 4 -7 -7 -33 2160.72 369.294 2 -7 7 -34-15.2030 159.426 4 -7 -7 -34 35.1720 117.222 2 -7 7 -35 117.056 141.922 4 -7 -7 -35 134.723 137.279 2 -7 7 -36 109.845 183.022 4 -7 -7 -36 93.5321 112.878 2 -7 7 -37 166.758 164.898 4 -7 -7 -37 117.584 116.554 2 -7 7 -38-6.63620 127.439 4 -7 -7 -38-5.59408 87.2578 2 -7 7 -39 180.466 145.446 4 -7 -7 -39-98.4354 100.774 2 7 7 40 143.308 106.727 5 -7 7 -40 170.661 139.334 4 -7 7 -41 973.608 194.674 4 -7 8 40 213.531 124.451 5 -7 8 39 239.128 130.001 5 -7 8 38 74.4455 112.571 5 -7 8 37-168.351 147.975 5 -7 -8 37 294.156 148.431 6 -7 8 36 328.786 147.920 5 -7 -8 36 293.424 154.854 6 -7 8 35 244.817 170.880 5 -7 -8 35 175.056 135.411 6 -7 8 34-31.4728 162.404 5 -7 -8 34 306.139 177.811 6 -7 8 33 216.248 192.081 5 -7 -8 33 200.799 181.289 6 -7 8 32 956.484 271.687 5 -7 -8 32 923.258 254.491 6 -7 8 31 236.144 213.125 5 -7 -8 31-37.6307 160.898 6 -7 8 30-146.295 179.695 5 -7 -8 30-58.6566 169.529 6 -7 8 29 165.350 183.090 5 -7 -8 29 49.6529 192.026 6 -7 8 28 46.5073 187.791 5 -7 -8 28 110.965 174.915 6 -7 8 27 222.518 207.849 5 -7 -8 27 501.797 254.067 6 -7 8 26 211.534 228.096 5 -7 -8 26 110.252 214.533 6 -7 8 25 488.977 303.533 5 -7 -8 25 919.559 337.015 6 -7 8 24-14.1055 190.510 5 -7 -8 24-229.841 259.588 6 -7 8 23 769.523 275.192 5 -7 -8 23 961.547 311.126 6 -7 8 22 279.475 234.759 5 -7 -8 22 181.687 192.278 6 -7 8 21 2346.42 512.846 5 -7 -8 21 3038.89 509.053 6 -7 8 20 1067.67 359.584 5 -7 -8 20 726.658 308.853 6 -7 8 19 1843.91 408.843 5 -7 -8 19 2360.46 487.388 6 -7 8 18 1341.46 388.327 5 -7 -8 18 568.082 310.103 6 -7 8 17 2581.94 481.322 5 7 -8 -17 2614.40 833.238 7 -7 -8 17 2271.06 488.947 6 -7 8 16 667.852 294.385 5 7 -8 -16 841.995 528.330 7 -7 -8 16 1017.07 345.237 6 -7 8 15 2408.65 424.454 5 7 -8 -15 1898.17 667.389 7 -7 -8 15 2307.08 494.765 6 7 -8 -14 3404.25 903.825 7 -7 -8 14 3394.45 584.307 6 7 -8 -13 814.688 444.012 7 -7 -8 13 1091.03 356.382 6 7 -8 -12 358.575 425.373 7 -7 -8 12 811.814 338.273 6 7 -8 -11 2103.57 670.642 7 -7 -8 11 2058.97 485.579 6 -7 -8 11 2112.88 366.663 2 -7 -8 10 1300.20 303.792 2 7 -8 -10 987.570 492.252 7 -7 -8 10 1551.61 378.692 6 -7 -8 9 910.255 283.590 2 7 -8 -9 891.844 555.856 7 -7 -8 9 993.034 351.021 6 -7 -8 8 1014.47 284.080 2 7 -8 -8 821.277 583.384 7 7 -8 -7 8110.69 1313.81 7 -7 -8 7 8065.73 863.252 6 -7 -8 7 8329.80 720.470 2 -7 -8 6 3600.05 609.311 6 -7 -8 6 3748.25 479.760 2 -7 -8 5 1371.43 285.414 2 7 -8 -5 2358.06 755.981 7 -7 -8 5 1535.55 357.451 6 -7 -8 4 400.489 199.298 2 -7 -8 4 655.798 242.100 6 7 -8 -4 783.737 524.510 7 -7 -8 3 1868.53 332.873 2 -7 -8 3 1659.09 563.105 1 7 -8 -3 846.897 654.698 7 -7 -8 2 7862.55 1124.41 1 7 -8 -2 5983.86 1134.32 7 -7 -8 2 9087.75 711.534 2 -7 -8 1 4248.22 844.482 1 7 -8 -1 6182.73 1179.68 7 -7 -8 1 5043.99 526.994 2 7 -8 0 2035.27 868.816 7 -7 -8 0 2919.85 789.396 1 -7 -8 0 2143.24 419.990 2 -7 -8 -1 8686.30 1189.41 1 7 -8 1 7409.99 1244.96 7 -7 8 -1 8287.45 771.724 3 -7 -8 -1 8347.15 690.199 2 7 -8 2 2293.44 875.283 7 -7 -8 -2 276.456 363.188 1 -7 8 -2 3511.83 524.113 3 7 -8 3 247.112 379.180 7 -7 -8 -3 300.268 291.987 1 -7 8 -3 160.222 203.985 3 -7 -8 -3-104.366 141.447 2 7 -8 4 457.271 413.533 7 -7 -8 -4 1162.94 510.764 1 -7 8 -4 297.546 193.936 3 -7 -8 -4 304.798 180.116 2 7 -8 5 196.296 290.349 7 -7 -8 -5 627.057 218.014 2 -7 -8 -5 1089.38 476.359 1 -7 8 -5 428.703 244.125 3 7 -8 6 1227.83 581.789 7 -7 -8 -6 894.800 276.691 2 -7 -8 -6 700.453 427.512 1 -7 8 -6 865.714 287.834 3 7 -8 7 2725.91 832.328 7 -7 -8 -7 2526.01 658.063 1 -7 8 -7 2108.11 458.971 3 -7 -8 -7 2841.99 456.965 2 7 -8 8 2821.39 875.863 7 -7 -8 -8 3564.28 803.879 1 -7 8 -8 3534.40 580.227 3 -7 -8 -8 3549.42 484.550 2 -7 -8 -9 2243.30 395.541 2 -7 -8 -9 1930.90 608.327 1 -7 8 -9 2445.20 481.907 3 -7 -8 -10 1193.84 313.887 2 -7 -8 -10 612.272 399.501 1 -7 8 -10 1260.58 351.054 3 -7 8 -11 4560.04 627.579 3 -7 -8 -11 3605.75 821.503 1 -7 -8 -11 3109.14 443.581 2 -7 -8 -12 599.555 226.224 2 -7 -8 -12 481.218 375.444 1 -7 8 -12 325.373 237.236 3 -7 -8 -13 902.424 292.036 2 -7 8 -13 460.862 265.453 3 -7 -8 -13 728.919 232.532 1 -7 -8 -14 525.351 226.126 2 -7 8 -14 360.572 231.833 3 -7 -8 -14-190.334 292.744 1 -7 -8 -15 470.113 207.427 2 -7 8 -15 652.914 293.406 3 -7 -8 -15 497.290 220.943 1 -7 8 -16 2289.69 505.279 3 -7 -8 -16 2423.08 437.152 2 -7 -8 -17 162.495 184.322 2 -7 8 -17-76.0223 224.089 3 -7 -8 -18 341.932 221.799 2 -7 8 -18-62.3759 232.177 3 -7 -8 -19-28.0059 167.276 2 -7 8 -19-2.97182 203.125 3 -7 -8 -20 1526.75 382.777 2 -7 8 -20 1336.50 375.982 3 7 -8 20 2032.16 413.763 6 -7 -8 -21 69.9255 161.584 2 7 -8 21 119.853 193.310 6 7 -8 22 211.043 195.608 6 -7 -8 -22-110.548 156.886 2 -7 -8 -23 671.386 257.377 2 -7 -8 -24 4084.46 560.786 2 -7 -8 -25 38.7143 130.752 2 -7 -8 -26-135.822 172.715 2 -7 8 -26 242.229 227.658 4 -7 -8 -27 1273.21 276.199 2 -7 8 -27 941.400 336.437 4 -7 -8 -28-55.2368 138.689 2 -7 8 -28 172.009 188.641 4 -7 8 -29 2278.49 452.629 4 -7 -8 -29 2737.20 417.435 2 -7 -8 -30 1190.59 273.335 2 -7 8 -30 1199.86 323.486 4 -7 -8 -31 2075.24 346.247 2 -7 8 -31 1469.75 337.115 4 -7 -8 -32 327.561 174.425 2 -7 8 -32 134.527 180.837 4 -7 8 -33-13.3742 150.054 4 -7 -8 -33 49.5650 107.018 2 -7 8 -34 89.5582 134.575 4 -7 -8 -34 44.4552 108.025 2 -7 8 -35 211.569 176.856 4 -7 -8 -35 126.858 101.724 2 -7 8 -36-99.0064 139.169 4 -7 -8 -36 23.5929 70.2235 2 7 8 37 60.3084 101.752 5 -7 8 -37 285.000 155.576 4 -7 8 -38 64.5572 121.460 4 -7 8 -39-23.5595 100.549 4 -7 -9 37 226.714 138.835 6 -7 9 37 469.937 147.533 5 -7 9 36 638.673 193.060 5 -7 -9 36 709.027 177.960 6 -7 9 35 151.335 127.223 5 -7 -9 35 40.3867 115.309 6 -7 9 34 42.8448 112.248 5 -7 -9 34 329.420 131.248 6 -7 9 33 531.377 187.945 5 -7 -9 33 535.561 198.906 6 -7 9 32 258.673 188.899 5 -7 -9 32 543.451 242.133 6 -7 9 31 161.896 151.694 5 -7 -9 31 60.6576 148.489 6 -7 9 30-230.830 195.937 5 -7 -9 30 164.394 171.898 6 -7 9 29-78.7400 177.732 5 -7 -9 29 602.433 273.299 6 -7 9 28-373.617 199.266 5 -7 -9 28 415.977 206.934 6 -7 9 27 2236.52 414.948 5 -7 -9 27 2264.74 431.747 6 -7 9 26 498.834 247.795 5 -7 -9 26 1004.35 324.470 6 -7 9 25 2706.52 458.724 5 -7 -9 25 2799.28 475.933 6 -7 9 24 1355.20 347.368 5 -7 -9 24 1461.71 385.421 6 -7 9 23 1649.02 378.874 5 -7 -9 23 1524.58 413.476 6 -7 9 22-59.4502 176.406 5 -7 -9 22-35.4953 209.144 6 -7 9 21 504.968 242.811 5 -7 -9 21 804.649 320.814 6 -7 -9 20 24.1659 192.783 6 -7 -9 19 1570.30 410.646 6 -7 -9 18 1542.14 400.579 6 -7 -9 17 583.003 318.292 6 -7 -9 16 497.949 265.142 6 -7 -9 15 1452.17 449.340 6 -7 -9 14 522.891 294.698 6 -7 -9 13 1336.22 385.048 6 7 -9 -12 647.821 377.374 7 -7 -9 12 888.249 341.672 6 7 -9 -11-138.203 301.389 7 -7 -9 11 969.309 376.703 6 7 -9 -10 1539.68 603.724 7 -7 -9 10 1506.92 409.287 6 7 -9 -9 286.026 374.642 7 -7 -9 9-228.730 282.234 6 -7 -9 9 264.267 179.652 2 7 -9 -8-47.4694 279.450 7 -7 -9 8 822.182 337.345 6 -7 -9 8 289.215 206.131 2 -7 -9 7 1985.51 364.988 2 -7 -9 7 1525.94 390.762 6 7 -9 -7 2054.00 675.813 7 -7 -9 6 16.3807 106.308 2 7 -9 -6 40.0443 256.772 7 -7 -9 6 283.904 216.634 6 -7 -9 5 340.226 176.658 2 7 -9 -5 456.606 453.719 7 -7 -9 5-36.6703 202.804 6 -7 -9 4 378.209 166.352 2 7 -9 -4 1027.19 530.340 7 -7 -9 4 469.660 183.628 6 -7 -9 3 797.852 241.056 2 7 -9 -3 1320.97 648.232 7 -7 -9 2 33.3543 109.083 2 7 -9 -2 271.803 388.049 7 -7 -9 1 722.926 238.317 2 -7 -9 1 518.251 347.455 1 7 -9 -1-183.053 294.604 7 7 -9 0 1297.83 653.472 7 -7 9 0 1884.64 467.512 3 -7 -9 0 2827.66 725.448 1 -7 -9 0 3634.94 453.736 2 7 -9 1 3315.69 922.000 7 -7 -9 -1 3385.53 808.147 1 -7 9 -1 4360.98 617.900 3 -7 -9 -1 3079.07 427.981 2 -7 -9 -2 1547.81 308.849 2 7 -9 2 1937.36 692.700 7 -7 -9 -2 1504.80 553.290 1 -7 9 -2 2191.42 459.856 3 -7 -9 -3 628.845 218.377 2 7 -9 3 627.683 433.826 7 -7 -9 -3 319.249 305.459 1 -7 9 -3 487.944 318.796 3 7 -9 4 769.746 420.878 7 -7 -9 -4 1954.48 371.113 2 -7 -9 -4 2269.56 683.183 1 -7 9 -4 526.931 312.733 3 -7 -9 -5 4490.23 928.382 1 7 -9 5 4567.39 1094.98 7 -7 9 -5 3807.36 607.576 3 -7 -9 -5 3257.90 440.627 2 -7 -9 -6 548.536 232.756 2 7 -9 6 704.080 693.223 7 -7 -9 -6 597.593 488.337 1 -7 9 -6 1122.64 389.543 3 -7 -9 -7 600.716 239.074 2 7 -9 7 420.331 415.776 7 -7 -9 -7 619.311 467.487 1 -7 9 -7 304.088 233.084 3 7 -9 8 3535.63 904.585 7 -7 9 -8 4010.18 608.922 3 -7 -9 -8 4002.46 516.173 2 -7 -9 -8 3974.10 840.628 1 7 -9 9 1911.87 788.669 7 -7 -9 -9 1280.09 299.320 2 -7 -9 -9 1656.68 610.983 1 -7 9 -9 1478.53 417.434 3 7 -9 10 1024.23 649.900 7 -7 -9 -10 2004.73 383.672 2 -7 9 -10 1935.86 446.395 3 -7 -9 -10 2087.27 660.342 1 -7 -9 -11 259.461 228.447 2 -7 9 -11 304.726 202.139 3 -7 -9 -12 659.676 261.225 2 -7 9 -12 226.812 229.256 3 -7 -9 -13 2237.55 411.340 2 -7 9 -13 1627.78 438.326 3 -7 -9 -14 151.892 169.318 2 -7 9 -14 55.2410 178.320 3 -7 -9 -15 2154.91 403.736 2 -7 9 -15 1738.05 452.910 3 -7 -9 -16 1824.49 392.253 2 -7 9 -16 984.141 356.628 3 -7 -9 -17 1505.20 346.508 2 -7 9 -17 1434.27 399.911 3 -7 -9 -18 78.6265 130.562 2 -7 9 -18-717.345 292.601 3 -7 -9 -19 1257.77 318.720 2 -7 9 -19 540.377 232.286 3 7 -9 19 781.118 296.649 6 -7 -9 -20 526.757 229.909 2 7 -9 20 100.223 164.652 6 -7 -9 -21 30.7200 135.366 2 7 -9 21 142.419 186.785 6 -7 -9 -22 99.7323 167.862 2 7 -9 22-40.7684 161.092 6 -7 -9 -23 26.4971 135.985 2 7 -9 23-69.8455 181.104 6 -7 -9 -24 427.033 212.689 2 -7 -9 -25 494.724 196.714 2 -7 -9 -26 392.609 184.346 2 -7 9 -26 699.349 279.104 4 -7 -9 -27 96.4814 141.525 2 -7 9 -27 49.3808 203.938 4 -7 -9 -28 235.226 141.737 2 -7 9 -28 52.6036 182.526 4 -7 -9 -29-89.5262 131.690 2 -7 9 -29-101.756 180.370 4 -7 9 -30 136.497 169.864 4 -7 9 -31-24.0584 172.625 4 -7 9 -32-116.431 184.133 4 -7 9 -33 464.573 201.846 4 -7 9 -34 179.992 141.277 4 -7 9 -35 402.564 186.272 4 -7 9 -36 65.1585 100.481 4 -7 9 -37 141.948 120.615 4 -7 -10 35 498.538 152.928 6 -7 -10 34 55.1023 101.869 6 -7 -10 33 99.7118 119.249 6 -7 -10 32 49.5958 126.801 6 -7 -10 31 129.302 140.518 6 -7 -10 30-220.382 150.458 6 -7 -10 29 302.815 178.663 6 -7 -10 28 385.338 222.184 6 -7 -10 27 1892.37 359.426 6 -7 -10 26 118.361 196.392 6 -7 -10 25 509.683 253.662 6 -7 -10 24 386.066 222.275 6 -7 -10 23 851.837 306.401 6 -7 -10 22 167.514 211.740 6 -7 -10 21 1469.09 379.344 6 -7 -10 20 186.258 191.468 6 -7 -10 19 840.332 286.381 6 -7 -10 18-150.263 216.637 6 -7 -10 17 1060.98 358.517 6 -7 -10 16 1274.74 394.802 6 -7 -10 15 488.555 328.516 6 -7 -10 14 981.390 360.125 6 -7 -10 13 397.008 320.317 6 -7 -10 12 2006.81 476.029 6 -7 -10 11 972.103 356.306 6 -7 -10 10 225.194 258.944 6 -7 -10 9 2162.30 507.883 6 -7 -10 8 3464.70 594.604 6 -7 -10 7 2227.70 479.506 6 -7 -10 6 3040.58 542.762 6 -7 -10 5 5321.23 659.093 6 -7 10 3 1038.66 401.713 3 -7 10 2 2737.29 545.220 3 -7 10 1 1368.49 439.346 3 -7 10 0 1015.38 372.791 3 -7 10 -1 297.415 283.137 3 -7 10 -2 125.166 182.806 3 -7 10 -3 2150.70 470.298 3 -7 10 -4 351.038 339.227 3 -7 10 -5 362.104 259.446 3 -7 10 -6 123.412 205.176 3 -7 10 -7 1781.28 443.736 3 -7 10 -8 174.230 297.133 3 -7 10 -9 3676.53 628.275 3 -7 10 -10 110.546 240.938 3 -7 10 -11-19.0001 181.428 3 -7 10 -12 277.599 251.129 3 -7 10 -13 2935.32 542.057 3 -7 10 -14 1045.38 354.219 3 -7 10 -15 1451.36 419.258 3 -7 10 -16-20.8400 175.599 3 7 -10 16 286.328 252.448 6 -7 10 -17-66.2501 210.048 3 7 -10 17 392.384 266.916 6 -7 10 -18-35.0807 245.923 3 7 -10 18 381.326 271.094 6 7 -10 19 180.425 170.463 6 7 -10 20 53.8438 187.643 6 7 -10 21 149.716 202.633 6 7 -10 22-4.03108 175.516 6 7 -10 23 198.105 181.197 6 7 -10 24 629.407 236.228 6 -7 10 -25 542.335 236.165 4 -7 10 -26 1265.92 299.513 4 -7 10 -27 1152.17 312.194 4 -7 10 -28 11.4219 149.478 4 -7 10 -29 239.947 174.625 4 -7 10 -30 331.354 191.155 4 -7 10 -31 473.923 197.084 4 -7 10 -32 355.407 162.480 4 -7 10 -33 226.069 141.728 4 -7 10 -34 457.911 156.987 4 -7 10 -35 12.2322 82.1885 4 -7 -11 33 119.214 103.534 6 -7 -11 32 13.4834 112.212 6 -7 -11 31 223.565 136.656 6 -7 -11 30-94.9052 109.711 6 -7 -11 29 110.124 117.488 6 -7 -11 28 107.692 130.114 6 -7 -11 27 378.379 200.311 6 -7 -11 26 698.263 242.854 6 -7 -11 25 768.826 265.780 6 -7 -11 24 77.7462 168.391 6 -7 -11 23 1543.33 350.429 6 -7 -11 22 2126.46 410.371 6 -7 -11 21 871.668 279.585 6 -7 -11 20 414.278 258.111 6 -7 -11 19 67.3827 190.851 6 -7 -11 18 21.9557 186.505 6 -7 -11 17 658.833 289.534 6 -7 -11 16 655.248 297.505 6 -7 -11 15 2255.16 461.235 6 -7 -11 14 974.957 331.425 6 -7 -11 13 1456.43 397.353 6 -7 -11 12 2016.33 448.646 6 -7 -11 11 1719.22 429.665 6 -7 -11 10 873.380 328.926 6 -7 -11 9 1213.83 380.453 6 -7 -11 8 1768.02 413.596 6 -7 -11 7 1466.80 413.910 6 -7 -11 6 1344.85 356.727 6 -7 11 6 895.144 343.963 3 -7 -11 5 172.560 206.344 6 -7 11 5 316.016 233.379 3 -7 11 4-835.119 305.860 3 -7 11 3-98.2794 251.224 3 -7 11 2 847.186 347.074 3 -7 11 1 104.237 244.236 3 -7 11 0 552.714 324.206 3 -7 11 -1 446.444 323.361 3 -7 11 -2 250.300 260.988 3 -7 11 -3 406.665 285.646 3 -7 11 -4 392.448 255.113 3 -7 11 -5 3475.86 574.651 3 -7 11 -6 1058.08 447.905 3 -7 11 -7 1849.21 459.546 3 -7 11 -8 1045.06 373.197 3 -7 11 -9 129.289 224.479 3 -7 11 -10 165.777 248.325 3 -7 11 -11 1230.58 397.253 3 -7 11 -12 302.433 252.702 3 -7 11 -13 481.875 237.943 3 -7 11 -14 154.043 202.917 3 7 -11 14 653.052 298.183 6 -7 11 -15-35.6315 225.112 3 7 -11 15 246.566 244.465 6 -7 11 -16 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492.752 287.136 2 -8 6 -32 639.087 305.334 4 -8 -6 -32 788.441 257.247 2 -8 6 -33 295.423 206.376 4 -8 -6 -33 293.252 210.218 2 -8 6 -34 789.770 270.625 4 -8 -6 -34 293.775 204.446 2 -8 6 -35 231.945 200.082 4 -8 -6 -35 388.244 191.373 2 -8 6 -36 264.710 167.027 4 -8 -6 -36 62.8380 134.136 2 -8 6 -37 309.098 188.807 4 -8 -6 -37 345.403 182.926 2 -8 6 -38 78.4901 141.748 4 -8 -6 -38 16.3976 94.0647 2 -8 6 -39-63.2394 112.640 4 -8 -6 -39-45.9738 88.3900 2 -8 6 -40 38.7642 98.9353 4 -8 -6 -40-38.3794 70.4608 2 -8 7 41 212.217 112.020 5 -8 7 40 452.371 151.669 5 -8 7 39 217.171 152.672 5 -8 7 38-126.414 152.669 5 -8 7 37-29.0899 150.181 5 -8 7 36 232.320 156.408 5 -8 7 35-140.332 185.477 5 -8 -7 35 320.877 171.825 6 -8 7 34-172.516 215.478 5 -8 -7 34 238.949 169.755 6 -8 7 33 2480.82 456.579 5 -8 -7 33 2594.51 398.320 6 -8 7 32-5.42764 172.771 5 -8 -7 32 241.270 191.858 6 -8 7 31 223.927 219.287 5 -8 -7 31 475.578 219.078 6 -8 7 30-406.243 283.576 5 -8 -7 30 226.555 169.656 6 -8 7 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192.123 5 8 -7 -13 580.667 509.774 7 -8 -7 13 47.3957 232.825 6 -8 -7 13-16.1200 143.895 2 -8 -7 12 178.124 192.333 2 8 -7 -12-60.3616 239.492 7 -8 -7 12 137.430 212.698 6 -8 7 12 182.751 195.934 5 -8 -7 11 825.732 300.259 2 8 -7 -11 901.169 419.400 7 -8 -7 11 884.201 350.515 6 -8 7 11 684.867 241.591 5 8 -7 -10 2879.31 771.038 7 -8 -7 10 2833.04 536.056 6 -8 -7 10 3686.50 515.838 2 -8 7 10 2148.66 380.224 5 -8 -7 9 703.359 255.206 2 8 -7 -9 1009.31 527.383 7 -8 -7 9 828.632 341.499 6 -8 7 9 454.909 304.969 5 -8 -7 8 564.992 227.788 2 8 -7 -8-51.1019 280.734 7 -8 -7 8 341.293 295.905 6 -8 7 8 233.356 171.865 5 -8 -7 7 746.657 251.750 2 8 -7 -7 708.614 421.676 7 8 -7 -6 6906.17 1146.99 7 -8 -7 6 6155.83 714.330 6 -8 -7 6 7439.59 672.174 2 -8 -7 5 879.280 271.879 2 8 -7 -5 1575.46 632.328 7 8 -7 -4 7259.57 1186.97 7 -8 -7 4 6118.15 651.290 6 -8 -7 4 7114.53 665.476 2 -8 -7 3 477.474 214.994 2 -8 -7 3 1716.12 645.805 1 8 -7 -3 997.175 789.192 7 -8 -7 2 944.910 250.332 2 -8 -7 2 1345.89 529.515 1 8 -7 -2 807.201 456.586 7 -8 -7 1 588.490 198.983 2 8 -7 -1 24.0545 311.074 7 -8 -7 0 517.948 209.552 2 8 -7 0 160.492 275.647 7 -8 -7 0 606.134 448.982 1 -8 -7 -1 1460.67 302.398 2 8 -7 1 1261.32 523.674 7 -8 -7 -1 1494.88 533.787 1 -8 7 -1 1368.50 365.714 3 -8 -7 -2-50.3722 137.587 2 -8 -7 -2 433.988 409.201 1 -8 7 -2 869.789 307.427 3 8 -7 2-126.736 396.981 7 8 -7 3-20.4240 339.429 7 -8 -7 -3 2129.60 419.487 2 -8 -7 -3 2740.87 836.392 1 -8 7 -3 505.371 253.056 3 -8 -7 -4 12195.2 1445.93 1 8 -7 4 15307.8 1684.19 7 -8 7 -4 13283.2 996.397 3 -8 -7 -4 13434.0 948.767 2 -8 -7 -5 6003.66 1077.08 1 8 -7 5 7330.25 1387.56 7 -8 7 -5 7551.03 775.629 3 -8 -7 -5 5304.21 587.843 2 8 -7 6 948.506 639.090 7 -8 -7 -6 705.397 273.855 2 -8 -7 -6 181.825 271.351 1 -8 7 -6 1033.18 333.849 3 8 -7 7 221.155 340.409 7 -8 -7 -7 297.658 206.291 2 -8 -7 -7 123.166 259.116 1 -8 7 -7 38.8942 150.605 3 8 -7 8 4025.42 907.940 7 -8 7 -8 4618.32 600.415 3 -8 -7 -8 3188.91 720.263 1 -8 -7 -8 4290.41 563.880 2 -8 -7 -9 399.269 229.868 2 -8 7 -9 611.610 294.813 3 -8 -7 -10 293.568 196.401 2 -8 7 -10-7.74574 153.285 3 -8 -7 -11 8757.15 1265.83 1 -8 7 -11 8769.07 828.936 3 -8 -7 -11 8579.93 770.889 2 -8 -7 -12 495.924 254.551 2 -8 -7 -12 319.928 375.616 1 -8 7 -12 461.688 265.862 3 -8 7 -13 2536.97 476.460 3 -8 -7 -13 1991.56 626.394 1 -8 -7 -13 2739.80 459.035 2 -8 -7 -14-26.0080 140.905 2 -8 7 -14 195.960 204.217 3 -8 -7 -15 855.057 288.946 2 -8 7 -15 446.336 229.239 3 -8 -7 -15 649.700 384.408 1 -8 7 -16 13.5739 153.686 3 -8 -7 -16-43.9530 124.531 2 -8 -7 -17 61.3397 162.571 2 -8 7 -17 38.2251 150.258 3 -8 -7 -18-56.4217 185.754 2 -8 7 -18-169.032 279.524 3 -8 7 -19-926.224 314.192 3 -8 -7 -19-171.610 220.526 2 -8 -7 -20 52.4980 171.446 2 -8 -7 -21 1831.76 405.013 2 -8 -7 -22 178.818 171.759 2 -8 -7 -23 799.349 309.672 2 -8 -7 -24-203.375 221.603 2 -8 -7 -25-17.4063 177.784 2 -8 -7 -26 85.2921 168.029 2 -8 7 -26 275.983 174.176 4 -8 -7 -27 477.341 244.137 2 -8 7 -27 828.272 303.432 4 -8 7 -28 1101.75 328.088 4 -8 -7 -28 594.263 275.995 2 -8 7 -29 960.225 294.989 4 -8 -7 -29 1443.12 333.696 2 -8 -7 -30 174.144 178.466 2 -8 7 -30-309.309 287.448 4 -8 -7 -31 1860.10 350.141 2 -8 7 -31 1938.86 388.159 4 -8 7 -32-333.816 223.058 4 -8 -7 -32 329.641 200.568 2 -8 7 -33-11.9485 148.163 4 -8 -7 -33 336.665 180.649 2 -8 7 -34 281.929 189.083 4 -8 -7 -34-115.515 112.354 2 -8 7 -35 202.957 172.354 4 -8 -7 -35-111.057 122.838 2 -8 7 -36 160.938 133.109 4 -8 -7 -36 37.7045 103.591 2 -8 7 -37 649.406 204.111 4 -8 -7 -37 145.990 101.892 2 -8 7 -38 94.1421 111.175 4 -8 -7 -38 78.8158 98.6241 2 -8 7 -39 295.530 141.216 4 -8 8 38 119.434 113.592 5 -8 8 37 387.274 175.316 5 -8 8 36 344.586 182.466 5 -8 8 35 263.205 164.592 5 -8 -8 35 274.680 161.214 6 -8 8 34-39.7668 138.929 5 -8 -8 34-11.8301 129.862 6 -8 8 33 113.955 173.066 5 -8 -8 33 143.009 144.358 6 -8 8 32-332.967 223.960 5 -8 -8 32 39.6780 151.642 6 -8 8 31-96.6919 202.179 5 -8 -8 31 85.1970 154.875 6 -8 8 30-568.658 238.739 5 -8 -8 30 320.699 192.532 6 -8 8 29 521.420 247.118 5 -8 -8 29 1202.09 324.821 6 -8 8 28-184.822 238.006 5 -8 -8 28 7.03481 172.992 6 -8 8 27 1052.09 317.652 5 -8 -8 27 1072.65 300.543 6 -8 8 26-37.9807 235.369 5 -8 -8 26-3.62502 183.360 6 -8 8 25-394.506 286.967 5 -8 -8 25-22.4817 181.490 6 -8 8 24 184.945 186.112 5 -8 -8 24 745.785 279.462 6 -8 8 23 382.736 227.959 5 -8 -8 23 633.039 267.603 6 -8 8 22 433.591 200.099 5 -8 -8 22 387.040 276.154 6 -8 8 21 149.435 199.970 5 -8 -8 21 188.223 181.373 6 -8 8 20 27.5085 206.088 5 -8 -8 20 419.387 268.358 6 -8 8 19 525.549 264.972 5 -8 -8 19 346.989 228.160 6 -8 8 18 446.391 225.479 5 -8 -8 18 694.138 299.848 6 -8 8 17-447.441 301.811 5 -8 -8 17-63.0500 229.574 6 -8 -8 16 316.642 257.655 6 -8 8 16-165.229 226.441 5 -8 -8 15 5524.51 727.035 6 -8 8 15 5189.71 636.812 5 -8 -8 14 445.937 229.636 6 -8 8 14 976.446 316.961 5 8 -8 -13 51.7882 321.932 7 -8 -8 13 211.823 219.426 6 -8 8 13-124.242 181.966 5 8 -8 -12-179.821 457.969 7 -8 -8 12 66.7806 222.143 6 -8 -8 12 430.050 236.455 2 8 -8 -11 12.3545 241.005 7 -8 -8 11-105.473 260.203 6 -8 -8 11 563.334 243.277 2 -8 -8 10 56.6770 141.703 2 8 -8 -10 354.119 253.302 7 -8 -8 10 131.799 248.887 6 -8 -8 9 424.407 217.939 2 8 -8 -9 676.454 508.675 7 -8 -8 9 775.174 356.831 6 -8 -8 8 688.893 246.165 2 8 -8 -8 744.480 468.948 7 -8 -8 8 364.580 281.586 6 -8 -8 7 455.835 193.727 2 8 -8 -7 565.539 362.414 7 -8 -8 7 244.547 224.991 6 -8 -8 6 670.275 260.156 2 8 -8 -6 159.086 321.551 7 -8 -8 6 1165.46 383.557 6 8 -8 -5 3193.86 905.615 7 -8 -8 5 3424.68 484.154 2 8 -8 -4 8737.54 1375.98 7 -8 -8 4 8656.51 795.156 6 -8 -8 4 9995.27 818.837 2 -8 -8 3 34.6427 169.647 2 8 -8 -3 2529.46 914.607 7 -8 -8 2-130.458 180.783 2 -8 -8 2-9.34273 221.784 1 8 -8 -2-48.6015 281.982 7 -8 -8 1 946.496 360.377 2 8 -8 -1 366.741 455.911 7 -8 8 1 95.0378 221.679 3 -8 -8 0 5705.27 998.536 1 8 -8 0 4506.97 990.366 7 -8 8 0 4543.79 615.336 3 -8 -8 0 5156.72 587.920 2 8 -8 1 2995.64 935.930 7 -8 -8 -1 2371.27 717.951 1 -8 8 -1 3947.56 635.439 3 -8 -8 -1 4052.98 533.620 2 -8 -8 -2 12471.4 1558.97 1 8 -8 2 10628.1 1536.19 7 -8 8 -2 10822.7 945.572 3 -8 -8 -2 11389.9 878.501 2 8 -8 3 7577.07 1350.07 7 -8 -8 -3 4334.27 878.209 1 -8 8 -3 7236.94 819.161 3 -8 -8 -3 4147.78 550.320 2 -8 -8 -4 2086.86 447.273 2 8 -8 4 1116.42 695.395 7 -8 -8 -4 2073.90 881.607 1 -8 8 -4 893.552 381.649 3 -8 -8 -5 9912.57 1355.85 1 8 -8 5 8545.44 1391.74 7 -8 8 -5 6991.36 787.740 3 -8 -8 -5 8194.58 743.294 2 8 -8 6 4263.48 1186.50 7 -8 -8 -6 3745.76 894.002 1 -8 8 -6 3957.32 658.213 3 -8 -8 -6 4747.38 574.239 2 8 -8 7 1662.53 703.361 7 -8 -8 -7 1052.19 325.719 2 -8 -8 -7 853.290 492.796 1 -8 8 -7 963.761 343.309 3 -8 -8 -8 5946.08 1038.38 1 8 -8 8 5552.69 1124.43 7 -8 8 -8 5136.63 661.609 3 -8 -8 -8 5546.16 637.332 2 8 -8 9 1121.72 647.343 7 -8 -8 -9 1024.02 341.994 2 -8 -8 -9 352.020 440.704 1 -8 8 -9 685.649 348.188 3 8 -8 10 1711.96 730.758 7 -8 -8 -10 2508.35 746.331 1 -8 8 -10 2620.85 497.575 3 -8 -8 -10 2875.55 483.691 2 8 -8 11 236.257 470.276 7 -8 -8 -11 227.000 203.704 2 -8 -8 -11 232.682 297.455 1 -8 8 -11 149.423 202.245 3 -8 -8 -12 2227.31 403.498 2 -8 8 -12 1436.76 406.008 3 -8 -8 -13 1359.24 325.155 2 -8 8 -13 1430.97 446.538 3 -8 -8 -14 1094.07 309.161 2 -8 8 -14 1074.51 390.325 3 -8 -8 -15 2189.63 421.274 2 -8 8 -15 1440.44 441.594 3 -8 -8 -16 0.35548 147.186 2 -8 8 -16-90.6877 223.456 3 -8 -8 -17 399.465 259.790 2 -8 8 -17-55.6113 263.259 3 -8 -8 -18 394.428 233.937 2 -8 8 -18-12.2477 224.117 3 -8 -8 -19 51.3877 159.158 2 -8 8 -19-935.110 321.834 3 -8 -8 -20 293.152 224.019 2 8 -8 20-149.180 157.340 6 -8 -8 -21 602.636 266.897 2 -8 -8 -22 930.287 326.516 2 -8 -8 -23 167.896 190.598 2 -8 -8 -24-29.1225 197.479 2 -8 -8 -25 209.185 187.691 2 -8 -8 -26 437.732 204.662 2 -8 8 -26 570.006 251.074 4 -8 -8 -27 1007.40 286.431 2 -8 8 -27 663.623 267.309 4 -8 -8 -28 467.226 212.432 2 -8 8 -28 390.156 236.083 4 -8 -8 -29-50.5445 129.008 2 -8 8 -29 276.023 200.302 4 -8 -8 -30-75.3608 139.208 2 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157.098 206.644 2 -9 2 -21 164.102 181.552 2 -9 -2 -21 321.848 244.411 1 -9 -2 -22 2609.71 482.386 2 -9 2 -22 2597.70 426.749 2 -9 -2 -22 2358.09 675.367 1 -9 -2 -23 189.104 199.331 2 -9 2 -23 324.572 204.909 2 -9 -2 -23-156.313 188.215 1 -9 -2 -24 2139.91 425.657 2 -9 2 -24 2251.62 433.100 2 -9 -2 -25 1341.33 372.580 2 -9 2 -25 1110.53 294.367 2 -9 -2 -26 667.739 243.335 2 -9 2 -26 638.735 226.094 2 -9 -2 -27 22.7352 209.910 2 -9 2 -27 7.07845 144.513 2 -9 -2 -28-242.360 274.121 2 -9 2 -28-228.905 207.142 2 -9 -2 -29-74.8734 236.306 2 -9 2 -29-272.261 241.344 2 -9 -2 -30 141.083 218.728 2 -9 2 -30-298.696 250.069 2 -9 -2 -31-37.1223 202.229 2 -9 2 -31 143.566 149.415 2 -9 -2 -32-597.785 257.069 2 -9 2 -32-59.5818 161.836 2 -9 -2 -33 1278.06 320.972 2 -9 2 -33 1256.13 297.302 2 -9 2 -34 36.0361 117.309 2 -9 -2 -34-524.188 230.744 2 -9 2 -35-114.093 140.102 2 -9 -2 -35-2.14906 149.947 2 -9 2 -36 815.164 224.303 2 -9 -2 -36 396.819 213.428 2 -9 2 -37 726.814 201.902 2 -9 -2 -37 773.710 226.316 2 -9 2 -38 580.598 166.157 2 -9 -2 -38 808.601 230.367 2 -9 2 -39 33.9333 50.8629 2 -9 -2 -39 369.871 173.697 2 -9 -2 -40 180.094 112.770 2 -9 -2 -41 632.067 188.683 2 -9 -2 -42 30.4208 74.1230 2 -9 3 43 190.700 112.284 5 -9 3 42 874.137 192.623 5 -9 3 41 251.356 152.210 5 -9 3 40 206.546 124.334 5 -9 3 39-244.789 199.803 5 -9 3 38 501.636 220.358 5 -9 3 37 256.000 190.121 5 -9 3 36-261.797 232.081 5 -9 3 35 2615.29 445.188 5 -9 3 34 211.558 183.116 5 -9 3 33 170.712 192.019 5 -9 3 32-96.2885 295.570 5 -9 3 31-126.654 256.556 5 -9 3 30 1301.61 406.155 5 -9 3 29 146.943 232.701 5 -9 3 28 856.642 344.444 5 -9 -3 28 717.024 289.912 6 -9 3 27-301.999 388.088 5 -9 -3 27 285.724 242.528 6 -9 3 26-221.109 342.313 5 -9 -3 26-220.618 197.780 6 -9 3 25 179.660 275.196 5 -9 -3 25 17.8399 183.614 6 -9 3 24 2336.26 580.705 5 9 -3 -24 1658.57 628.766 7 -9 -3 24 1573.46 394.508 6 -9 3 23 2381.57 536.287 5 9 -3 -23 1697.44 648.516 7 -9 -3 23 2602.42 491.724 6 -9 3 22 302.594 271.724 5 9 -3 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430.806 7 -9 -3 12 534.815 252.526 6 -9 -3 11 548.719 243.400 2 9 -3 -11 531.262 408.442 7 -9 -3 11 169.803 216.981 6 -9 3 11 79.7495 137.479 5 9 -3 -10 2013.97 528.317 7 -9 -3 10 2368.57 386.437 2 -9 -3 10 2735.04 473.683 6 -9 3 10 2651.15 462.424 5 -9 -3 9 29.8680 98.0673 2 9 -3 -9 227.619 256.357 7 -9 -3 9-57.3979 184.097 6 -9 3 9 257.981 201.114 5 -9 -3 8 1876.65 355.125 2 9 -3 -8 1655.95 521.649 7 -9 -3 8 1863.09 396.473 6 -9 3 8 1853.12 394.097 5 -9 -3 7 148.668 146.520 2 9 -3 -7 635.621 336.802 7 -9 -3 7 123.079 177.592 6 -9 3 7 192.571 192.303 5 9 -3 -6 2813.95 645.170 7 -9 3 6 3710.68 508.632 5 -9 -3 6 3308.61 462.619 2 9 -3 -5 4028.32 778.103 7 -9 3 5 3845.65 535.860 5 -9 -3 5 3274.25 433.521 2 -9 -3 4 4654.54 794.689 1 9 -3 -4 4006.34 732.450 7 -9 3 4 5200.81 608.489 5 -9 -3 4 4439.14 502.148 2 -9 -3 3 2023.79 675.497 1 9 -3 -3 977.324 466.565 7 -9 -3 3 2010.12 376.087 2 -9 3 3 1634.62 364.716 5 -9 -3 2 14018.3 1390.41 1 9 -3 -2 13310.9 1317.01 7 -9 3 2 11190.0 858.616 5 -9 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157.215 5 -9 -4 9 1050.32 308.363 2 9 -4 -9 715.107 364.863 7 -9 -4 9 824.166 329.757 6 -9 4 9 724.714 256.665 5 -9 -4 8 2465.56 396.773 2 9 -4 -8 1983.67 569.439 7 -9 -4 8 3116.22 532.812 6 -9 4 8 1831.16 380.474 5 -9 -4 7 7535.22 746.286 6 9 -4 -7 7357.60 1057.08 7 -9 4 7 8139.62 762.776 5 -9 -4 7 9140.11 745.047 2 9 -4 -6 2667.62 758.663 7 -9 -4 6 3472.36 512.582 6 -9 4 6 3113.61 492.627 5 -9 -4 6 3530.00 490.452 2 9 -4 -5 5647.54 938.027 7 -9 4 5 4343.89 557.253 5 -9 -4 5 5313.59 560.405 2 -9 -4 5 5735.26 628.241 6 -9 -4 4 3672.93 760.586 1 9 -4 -4 3771.57 844.505 7 -9 4 4 3812.33 606.468 5 -9 -4 4 3706.87 504.568 6 -9 -4 4 3292.45 439.242 2 -9 -4 3 1595.37 306.072 2 -9 -4 3 1614.89 545.748 1 9 -4 -3 1125.70 489.794 7 -9 4 3 1912.27 395.896 5 -9 -4 2 177.909 89.5455 2 9 -4 -2 146.862 258.348 7 -9 -4 2 420.664 419.480 1 -9 4 2 270.296 228.767 5 9 -4 -1 2580.47 651.387 7 -9 -4 1 2940.68 727.791 1 -9 4 1 2818.35 402.586 5 -9 -4 1 2571.27 373.186 2 9 -4 0 1279.31 463.024 7 -9 -4 0 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337.871 5 9 -5 -20 711.739 479.084 7 -9 -5 20 365.925 267.307 6 -9 5 19 366.062 275.760 5 9 -5 -19 683.588 460.918 7 -9 -5 19 276.502 209.837 6 -9 5 18 143.074 233.976 5 9 -5 -18 886.807 579.489 7 -9 -5 18 394.793 229.244 6 -9 5 17 607.649 358.165 5 9 -5 -17 619.921 390.357 7 -9 -5 17 525.532 210.675 6 -9 5 16 2851.29 568.977 5 9 -5 -16 3309.36 891.146 7 -9 -5 16 2618.71 508.688 6 -9 5 15 1683.34 426.822 5 9 -5 -15 1603.52 629.492 7 -9 -5 15 1593.02 387.309 6 -9 -5 15 1882.54 405.068 2 -9 -5 14 2625.93 443.277 2 -9 5 14 2282.50 470.757 5 9 -5 -14 2044.01 687.453 7 -9 -5 14 2579.42 483.158 6 9 -5 -13 2804.90 761.731 7 -9 -5 13 2725.54 482.676 6 -9 -5 13 3547.67 503.104 2 -9 5 13 2944.09 519.187 5 -9 -5 12 1058.68 292.992 2 9 -5 -12 1782.66 575.647 7 -9 -5 12 1085.64 362.472 6 -9 5 12 809.229 331.049 5 -9 -5 11 779.765 249.285 2 9 -5 -11 577.788 388.446 7 -9 -5 11 622.691 269.737 6 -9 5 11 865.906 275.048 5 -9 -5 10 428.806 203.498 2 9 -5 -10 186.419 244.428 7 -9 -5 10 519.066 269.245 6 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874.093 1 9 -5 0 4878.11 978.411 7 -9 5 0 4331.51 545.038 3 -9 5 0 4134.94 535.123 5 -9 -5 0 3790.94 504.888 2 9 -5 1 1005.48 470.123 7 -9 -5 -1 455.031 189.617 2 -9 -5 -1 564.640 423.744 1 -9 5 -1 991.557 305.870 3 -9 5 -1 587.617 204.273 5 9 -5 2 535.055 319.017 7 -9 -5 -2 1287.24 374.379 2 -9 5 -2 1127.45 305.859 3 -9 5 -2 810.927 231.789 5 -9 -5 -3 5951.27 1008.91 1 9 -5 3 6627.32 1077.93 7 -9 5 -3 4696.17 565.095 3 -9 5 -3 4714.68 553.791 5 -9 -5 -3 6288.19 658.768 2 -9 -5 -4 3298.00 908.593 1 9 -5 4 4427.52 988.080 7 -9 5 -4 2890.82 440.884 3 -9 5 -4 3498.65 457.174 5 -9 -5 -4 4757.11 598.807 2 -9 -5 -5 5308.31 914.636 1 9 -5 5 4270.17 924.378 7 -9 5 -5 4385.72 582.816 3 -9 5 -5 3242.53 439.713 5 -9 -5 -5 4615.78 536.912 2 9 -5 6 1294.15 589.552 7 -9 -5 -6 1123.80 336.569 2 -9 -5 -6 1381.89 614.894 1 -9 5 -6 833.365 272.119 3 -9 5 -6 1013.03 296.528 5 9 -5 7 2920.31 801.696 7 -9 -5 -7 3697.30 777.292 1 -9 5 -7 4095.61 543.872 3 -9 5 -7 3184.78 437.406 5 -9 -5 -7 3743.87 489.401 2 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1270.67 394.730 2 -9 -5 -20 3924.39 593.078 2 -9 -5 -21 86.5531 182.105 2 -9 -5 -22 38.0654 178.999 2 -9 -5 -23-85.5659 212.011 2 -9 5 -24 661.325 274.547 4 -9 -5 -24 39.8993 206.407 2 -9 5 -25 411.674 269.661 4 -9 -5 -25-9.38410 176.933 2 -9 5 -26 1169.63 358.695 4 -9 -5 -26 1157.50 348.445 2 -9 5 -27-176.195 244.052 4 -9 -5 -27-3.60865 183.570 2 -9 5 -28-20.8391 220.681 4 -9 -5 -28-177.878 252.761 2 -9 5 -29 616.714 245.619 4 -9 -5 -29 505.225 258.560 2 -9 5 -30-20.0336 173.086 4 -9 -5 -30-60.7187 214.482 2 -9 5 -31 1135.58 303.781 4 -9 -5 -31 930.624 269.967 2 -9 5 -32 143.379 152.827 4 -9 -5 -32 14.7025 144.163 2 -9 5 -33 269.675 187.887 4 -9 -5 -33 139.952 167.107 2 -9 5 -34 130.767 182.739 4 -9 -5 -34 22.5226 138.161 2 -9 5 -35 459.871 210.573 4 -9 -5 -35 262.161 176.938 2 -9 5 -36 5.23542 136.063 4 -9 -5 -36-11.7085 118.402 2 -9 5 -37 236.040 115.250 4 -9 -5 -37 238.211 162.570 2 -9 5 -38 21.4731 97.1264 4 -9 -5 -38-28.4212 88.6534 2 -9 -5 -39 4.85917 76.5106 2 -9 -5 -40-31.9367 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282.533 196.186 4 -9 7 -31 2017.09 355.066 4 -9 -7 -31 2352.59 366.976 2 -9 -7 -32-11.3593 101.787 2 -9 7 -32-63.9711 147.369 4 -9 7 -33 762.646 217.953 4 -9 -7 -33 791.093 224.830 2 -9 7 -34 339.706 164.847 4 -9 -7 -34-0.19672 89.0714 2 -9 7 -35 71.5556 115.626 4 -9 -7 -35 98.0507 104.911 2 -9 7 -36-18.9841 88.6020 4 -9 -7 -36 16.7937 75.8570 2 -9 8 36-172.889 101.140 5 -9 8 35 91.2330 104.424 5 -9 8 34 279.906 159.025 5 -9 -8 33 138.345 134.301 6 -9 8 33 201.358 166.869 5 -9 -8 32 90.6106 148.336 6 -9 8 32 76.6780 145.375 5 -9 -8 31 150.666 149.547 6 -9 8 31 207.820 165.937 5 -9 -8 30 40.2086 140.765 6 -9 8 30 370.758 210.203 5 -9 -8 29-164.688 179.661 6 -9 8 29 184.240 169.372 5 -9 -8 28 12.0028 156.648 6 -9 8 28-26.0683 161.579 5 -9 -8 27 1320.36 330.483 6 -9 8 27 938.291 315.860 5 -9 -8 26 176.786 184.031 6 -9 8 26 201.490 193.963 5 -9 -8 25 262.483 232.038 6 -9 8 25 269.664 182.997 5 -9 -8 24 18.8386 202.788 6 -9 8 24-325.505 275.232 5 -9 -8 23 499.831 264.014 6 -9 8 23 166.849 197.478 5 -9 -8 22 221.721 224.410 6 -9 8 22 58.6990 217.133 5 -9 -8 21 4816.74 629.927 6 -9 8 21 5062.04 657.912 5 -9 -8 20 135.231 204.119 6 -9 8 20-316.166 246.933 5 -9 -8 19 1828.67 411.821 6 -9 8 19 1886.01 417.154 5 -9 -8 18 2354.96 463.313 6 -9 8 18 3285.72 520.804 5 -9 -8 17-5.81869 200.419 6 -9 8 17 35.8566 191.004 5 -9 -8 16 330.513 246.704 6 -9 8 16-158.995 237.128 5 -9 -8 15-100.905 211.554 6 -9 8 15-255.443 237.351 5 -9 -8 14-138.114 270.621 6 -9 8 14 83.5143 164.222 5 -9 -8 13 3.18084 257.040 6 -9 8 13 376.162 206.438 5 -9 -8 12 791.334 315.909 6 -9 8 12-50.2164 149.630 5 -9 -8 11 1280.40 395.914 6 -9 8 11 1359.15 333.549 5 -9 -8 11 1561.36 352.993 2 -9 -8 10 632.652 392.264 6 -9 -8 10 433.304 261.806 2 -9 -8 9 3923.66 625.404 6 -9 -8 9 3499.06 551.609 2 -9 -8 8 1948.18 401.629 2 -9 -8 8 1946.78 415.315 6 -9 -8 7 354.306 200.188 2 -9 -8 7 1152.63 379.026 6 -9 -8 6 2491.83 447.792 2 -9 -8 6 2462.68 448.227 6 -9 -8 5 1253.70 329.439 2 -9 -8 5 1447.87 372.304 6 -9 -8 4 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743.923 2 -10 0 1 395.873 195.901 2 -10 0 1 1017.28 345.740 5 -10 0 0 35863.5 1516.08 5 -10 0 0 31721.0 1283.38 2 -10 0 -1 526.225 217.709 2 -10 0 -1 888.807 316.197 5 -10 0 -2 7318.96 887.954 1 -10 0 -2 7871.82 722.478 5 -10 0 -2 7091.58 607.533 2 -10 0 -3 112.201 217.921 1 -10 0 -3 80.0740 107.032 2 -10 0 -3-250.053 192.750 5 -10 0 -4 1466.07 297.100 2 -10 0 -4 1259.11 319.188 5 -10 0 -5 216.992 198.880 2 -10 0 -5-112.673 164.773 5 -10 0 -6 192.544 142.556 2 -10 0 -6 20.2751 117.803 5 -10 0 -7 315.046 192.858 2 -10 0 -7 12.9487 137.167 5 -10 0 -8 27101.8 1360.14 5 -10 0 -8 26685.2 1250.58 2 -10 0 -9 103.012 135.148 2 -10 0 -9 437.867 237.803 5 -10 0 -10 1660.79 334.990 2 -10 0 -10 1680.62 385.388 5 -10 0 -11 259.553 155.474 2 -10 0 -11 173.372 230.071 5 -10 0 -12 24343.4 1335.71 5 -10 0 -12 24913.8 1216.71 2 -10 0 -13 312.922 212.498 2 -10 0 -14 4689.47 540.474 2 -10 0 -15 65.4055 152.181 2 -10 0 -16 1213.14 270.322 2 -10 0 -17-82.1933 176.257 2 -10 0 -18 4972.37 596.749 2 -10 0 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328.987 5 -11 6 24-110.750 271.619 5 -11 -6 23-27.3973 174.010 6 -11 6 23 249.821 262.925 5 -11 -6 22 214.319 164.697 6 -11 6 22 631.730 306.699 5 -11 -6 21 388.684 243.301 6 -11 6 21 393.139 295.633 5 -11 -6 20 856.334 291.422 6 -11 6 20 577.191 272.815 5 -11 -6 19 320.845 229.088 6 -11 6 19 103.916 217.728 5 -11 -6 18 168.400 200.729 6 -11 6 18-25.5166 219.220 5 -11 -6 17 1331.71 387.724 6 -11 6 17 1009.27 399.433 5 -11 -6 16-2.04571 216.999 6 -11 6 16 248.898 275.073 5 -11 -6 15 45.0673 198.447 6 -11 6 15 178.275 219.943 5 -11 -6 14 710.034 299.762 6 -11 6 14 545.154 262.578 5 -11 -6 13 3112.29 565.501 6 -11 -6 13 2206.49 538.677 2 -11 6 13 2677.82 490.714 5 -11 -6 12-3.20746 223.253 6 -11 6 12 544.904 303.388 5 -11 -6 12 40.0793 217.577 2 -11 -6 11 1979.35 422.290 2 -11 -6 11 2832.47 560.768 6 -11 6 11 1835.54 417.204 5 -11 -6 10 2268.85 455.163 2 -11 -6 10 2173.36 462.018 6 -11 6 10 2807.59 521.671 5 -11 -6 9 383.297 238.501 2 -11 -6 9 187.810 267.539 6 -11 6 9 547.981 356.153 5 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260.708 5 -11 -7 21 335.340 222.589 6 -11 7 21 624.841 303.723 5 -11 -7 20 848.377 291.771 6 -11 7 20 727.313 275.032 5 -11 -7 19 320.967 240.047 6 -11 7 19 250.865 215.074 5 -11 -7 18 2803.73 480.972 6 -11 7 18 2878.86 520.141 5 -11 -7 17 199.256 204.413 6 -11 7 17 799.649 320.487 5 -11 -7 16 184.623 210.093 6 -11 7 16-218.835 251.374 5 -11 -7 15 494.492 310.198 6 -11 7 15 969.302 336.996 5 -11 -7 14 1105.70 348.311 6 -11 7 14 844.859 322.456 5 -11 -7 13 3497.13 574.117 6 -11 7 13 3669.82 537.513 5 -11 -7 12 433.984 304.484 6 -11 7 12 688.101 329.561 5 -11 -7 11 634.190 276.441 6 -11 7 11 697.134 314.311 5 -11 -7 11 268.868 264.717 2 -11 -7 10 693.742 341.485 6 -11 7 10 373.390 242.986 5 -11 -7 10 400.985 261.254 2 -11 -7 9 277.543 226.110 2 -11 -7 9 355.669 260.035 6 -11 7 9 88.4258 168.342 3 -11 7 9 111.539 168.151 5 -11 -7 8 555.076 311.790 2 -11 -7 8 662.535 266.307 6 -11 7 8 196.953 194.110 3 -11 7 8 497.869 205.198 5 -11 -7 7 120.479 184.381 2 -11 -7 7 84.8347 200.505 6 -11 7 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588.875 183.818 4 -11 -7 -29 155.139 127.118 2 -11 7 -29 90.8008 92.2067 4 -11 -7 -30-60.6155 95.3111 2 -11 -7 -31-20.9093 79.3974 2 -11 8 31 91.7275 92.7082 5 -11 8 30 244.180 130.312 5 -11 8 29 255.093 148.462 5 -11 8 28 137.977 123.350 5 -11 8 27 292.289 167.801 5 -11 8 26 16.0567 113.683 5 -11 8 25 2142.70 334.250 5 -11 8 24-123.673 161.130 5 -11 -8 23 1534.72 331.487 6 -11 8 23 1346.51 319.570 5 -11 -8 22-51.4511 168.734 6 -11 8 22-86.1413 187.352 5 -11 -8 21-91.8712 186.442 6 -11 8 21 5.22777 150.448 5 -11 -8 20 554.554 232.661 6 -11 8 20 681.759 255.691 5 -11 -8 19 169.534 214.051 6 -11 8 19 131.680 156.562 5 -11 -8 18-592.523 256.663 6 -11 8 18-16.0649 153.010 5 -11 -8 17 8.79711 163.623 6 -11 8 17 146.611 223.331 5 -11 -8 16 307.380 214.552 6 -11 8 16 660.167 238.766 5 -11 -8 15 264.564 229.704 6 -11 8 15 773.223 303.851 5 -11 -8 14 422.033 250.512 6 -11 8 14 687.506 273.913 5 -11 -8 13 164.472 198.977 6 -11 8 13 456.280 247.927 5 -11 -8 12 577.378 295.841 6 -11 8 12 390.813 236.131 5 -11 -8 11 992.268 321.941 6 -11 8 11 1130.94 342.355 3 -11 8 11 1432.33 301.718 5 -11 -8 10 202.883 269.912 6 -11 8 10 119.172 180.392 3 -11 8 10 135.268 152.442 5 -11 -8 9 1290.74 337.840 6 -11 8 9 1952.42 411.131 3 -11 8 9 726.697 216.553 5 -11 -8 9 2042.07 435.574 2 -11 -8 8 346.152 223.553 6 -11 8 8 635.244 278.165 3 -11 -8 8 72.9533 207.317 2 -11 -8 7 803.660 282.335 2 -11 -8 7 443.667 225.973 6 -11 8 7 311.155 218.092 3 -11 -8 6 144.936 202.585 2 -11 8 6-66.3388 159.084 3 -11 -8 5 426.392 238.935 2 -11 8 5-90.4831 171.989 3 -11 -8 4 1496.81 370.937 2 -11 8 4 1485.45 385.392 3 -11 -8 3 593.009 348.414 2 -11 8 3 946.432 359.515 3 -11 -8 2 954.473 312.080 2 -11 8 2 868.946 324.782 3 -11 -8 1 3.67436 175.603 2 -11 8 1 285.422 238.478 3 -11 -8 0 208.871 200.392 2 -11 8 0-274.175 228.440 3 -11 -8 -1 118.796 172.370 2 -11 8 -1-12.1439 170.965 3 -11 -8 -2 1424.30 421.800 2 -11 8 -2 74.9295 284.949 3 -11 8 -3 4003.77 586.624 3 -11 -8 -3 4715.56 603.595 2 -11 -8 -4 1491.75 417.089 2 -11 8 -4 1002.98 326.341 3 -11 8 -5 2452.26 446.626 3 -11 -8 -5 2674.92 497.604 2 -11 -8 -6 451.191 317.870 2 -11 8 -6 664.462 327.166 3 -11 8 -7 2042.88 452.855 3 -11 -8 -7 2454.56 477.672 2 -11 8 -8 3705.44 550.386 3 -11 -8 -8 2625.79 504.864 2 -11 -8 -9 102.378 240.392 2 -11 8 -9 600.082 296.168 3 -11 -8 -10 200.537 226.966 2 -11 8 -10 168.655 153.323 3 -11 -8 -11 13.7904 153.741 2 -11 8 -11-72.4120 198.504 3 -11 -8 -12 3.68127 168.325 2 -11 8 -12 267.591 180.471 3 -11 -8 -13 295.408 163.962 2 -11 8 -13 17.2828 149.119 3 -11 -8 -14 189.379 220.491 2 -11 8 -14-71.2968 186.667 3 -11 -8 -15-283.272 228.254 2 -11 -8 -16 17.7439 168.361 2 -11 -8 -17 417.323 211.770 2 -11 -8 -18 22.4385 159.058 2 -11 -8 -19 306.108 205.473 2 -11 -8 -20-511.522 217.131 2 -11 8 -20-180.155 134.146 4 -11 -8 -21 159.538 126.618 2 -11 8 -21 114.723 126.988 4 -11 -8 -22 52.8565 122.791 2 -11 8 -22 180.909 162.221 4 -11 -8 -23 20.9031 124.385 2 -11 8 -23 146.287 148.193 4 -11 -8 -24 412.033 186.290 2 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197.880 2 -11 10 -4 249.156 228.213 3 -11 -10 -5 602.623 217.494 2 -11 10 -5 395.132 256.386 3 -11 -10 -6 731.682 250.651 2 -11 10 -6 652.199 281.569 3 -11 -10 -7 795.160 237.273 2 -11 10 -7 389.092 231.283 3 -11 -10 -8-5.75973 146.833 2 -11 10 -8 227.820 175.318 3 -11 -10 -9-83.2195 130.208 2 -11 10 -9 24.1601 148.991 3 -11 -10 -10 382.369 187.850 2 -11 10 -10 49.6547 141.886 3 -11 -10 -11 1471.79 280.986 2 -11 10 -11 767.126 267.316 3 -11 -10 -12 359.144 196.369 2 -11 10 -12 38.3487 124.101 3 -11 -10 -13 240.076 142.037 2 -11 -10 -14 145.245 136.236 2 11 -10 14-16.9669 123.654 6 -11 -10 -15 505.582 178.248 2 11 -10 15 405.718 189.317 6 -11 -10 -16 135.767 128.417 2 11 -10 16 4.59228 115.912 6 -11 -10 -17 419.198 149.199 2 -11 -10 -18 77.6685 103.071 2 -11 -10 -19 179.420 117.593 2 -11 10 -19 57.0333 113.093 4 -11 10 -20 99.3078 126.564 4 -11 10 -21-163.830 117.114 4 -11 10 -22 0.34865 93.2735 4 -11 10 -23 1453.68 239.949 4 -11 11 22 6.53453 66.6340 3 -11 11 21 84.2977 99.4670 3 -11 11 20 68.1794 98.1363 3 -11 11 19 98.4390 120.044 3 -11 11 18 102.371 132.473 3 -11 11 17 297.537 181.303 3 -11 11 16 159.969 177.274 3 -11 11 15 64.3538 132.214 3 -11 11 14 61.2946 152.594 3 -11 11 13 299.201 175.429 3 -11 11 12 157.774 191.006 3 -11 11 11 90.9244 154.395 3 -11 11 10 348.453 186.932 3 -11 11 9 558.494 209.364 3 -11 11 8 100.552 159.092 3 -11 11 7-36.4723 163.674 3 -11 11 6 149.901 183.435 3 -11 11 5 13.2072 122.540 3 -11 11 4-52.8857 143.122 3 -11 11 3-27.0205 134.929 3 -11 11 2 210.891 177.991 3 -11 11 1 137.129 182.306 3 -11 11 0 199.719 218.554 3 -11 11 -1 628.282 241.667 3 -11 11 -2 90.9115 147.153 3 -11 11 -3 148.246 161.846 3 -11 11 -4 714.374 255.259 3 -11 11 -5 304.133 217.191 3 -11 11 -6 66.9661 148.667 3 -11 11 -7 81.1693 112.305 3 -11 11 -8 291.293 191.788 3 -11 11 -9-221.043 150.347 3 -11 11 -10 424.697 179.248 3 11 -11 10 608.077 228.905 6 11 -11 11-61.4589 158.880 6 11 -11 12 225.009 159.898 6 11 -11 13-25.7197 132.356 6 11 -11 14 183.682 134.275 6 11 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370.298 134.496 2 -16 -5 -10-4.79505 77.5416 2 -16 -6 -6 160.298 104.509 2 0 0 0 0.00 0.00 0 TITL MRC2141 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 13.987842 13.593524 41.686731 90.0000 92.3748 90.0000 ZERR 6.00 0.000448 0.000822 0.002656 0.0000 0.0050 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Mg Co UNIT 420.00 720.00 24.00 12.00 12.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 97492