# Electronic Supplementary Material (ESI) for Chemical Science. # This journal is © The Royal Society of Chemistry 2022 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p-1_a _database_code_depnum_ccdc_archive 'CCDC 2150901' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universitaet Freiburg Germany ; _audit_update_record ; 2022-02-08 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C58 H4 Al2 F80 O22 Ru3' _chemical_formula_moiety '2(C16 Al F36 O4), C14 O14 Ru3, 2(C6 H2 F4)' _chemical_formula_weight 2929.78 _chemical_melting_point ? _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.298(4) _cell_length_b 14.164(6) _cell_length_c 15.698(5) _cell_angle_alpha 71.621(10) _cell_angle_beta 71.685(18) _cell_angle_gamma 73.388(12) _cell_volume 2213.9(14) _cell_formula_units_Z 1 _cell_measurement_temperature 106(2) _cell_measurement_reflns_used 9785 _cell_measurement_theta_min 2.339 _cell_measurement_theta_max 28.3115 _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.197 _exptl_crystal_F_000 1406 _exptl_crystal_size_max 0.12 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.07 _exptl_absorpt_coefficient_mu 0.763 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.7036 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 106(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 201036 _diffrn_reflns_av_unetI/netI 0.0155 _diffrn_reflns_av_R_equivalents 0.0544 _diffrn_reflns_theta_min 1.410 _diffrn_reflns_theta_max 28.364 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 11068 _reflns_number_gt 10225 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS V6.2.14 Patch 4/2020-11-09' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0181P)^2^+1.5466P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_number_reflns 11068 _refine_ls_number_parameters 745 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0217 _refine_ls_R_factor_gt 0.0192 _refine_ls_wR_factor_ref 0.0463 _refine_ls_wR_factor_gt 0.0453 _refine_ls_goodness_of_fit_ref 1.017 _refine_ls_restrained_S_all 1.017 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.491 _refine_diff_density_min -0.550 _refine_diff_density_rms 0.055 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.53312(2) 0.14503(2) 0.32111(2) 0.01088(3) Uani 1 1 d . . . . . Ru2 Ru 0.500000 0.000000 0.500000 0.01056(3) Uani 1 2 d S . P . . Al6 Al 0.73017(4) 0.29555(3) 0.77696(3) 0.01077(7) Uani 1 1 d . . . . . F1 F -0.18992(8) 0.25005(8) 0.19537(7) 0.0285(2) Uani 1 1 d . . . . . F6 F 0.88693(10) 0.40818(7) 0.50087(6) 0.0300(2) Uani 1 1 d . . . . . F7 F 1.00790(8) 0.28357(8) 0.44332(6) 0.0283(2) Uani 1 1 d . . . . . F8 F 0.95084(9) 0.10035(8) 0.53844(7) 0.0302(2) Uani 1 1 d . . . . . F9 F 0.75908(9) 0.13867(8) 0.61990(8) 0.0365(3) Uani 1 1 d . . . . . F10 F 0.80384(9) 0.30355(9) 0.47685(6) 0.0324(2) Uani 1 1 d . . . . . F11 F 0.91315(10) 0.06916(7) 0.68692(7) 0.0336(2) Uani 1 1 d . . . . . F12 F 1.12187(8) 0.16493(7) 0.58787(6) 0.02280(18) Uani 1 1 d . . . . . F13 F 1.06586(8) 0.32124(7) 0.59595(7) 0.02567(19) Uani 1 1 d . . . . . F14 F 1.01692(9) 0.20299(7) 0.71744(6) 0.02575(19) Uani 1 1 d . . . . . F15 F 0.84149(9) 0.50509(7) 0.66161(6) 0.02229(18) Uani 1 1 d . . . . . F16 F 0.66786(8) 0.56712(6) 0.74958(6) 0.02056(17) Uani 1 1 d . . . . . F17 F 0.84194(9) 0.61300(6) 0.73245(6) 0.02157(18) Uani 1 1 d . . . . . F18 F 1.04000(8) 0.43661(7) 0.74170(6) 0.02536(19) Uani 1 1 d . . . . . F19 F 0.97766(8) 0.50209(7) 0.85952(7) 0.02541(19) Uani 1 1 d . . . . . F20 F 1.00316(8) 0.34056(7) 0.87960(6) 0.02366(18) Uani 1 1 d . . . . . F21 F 0.71401(8) 0.56725(6) 0.91461(6) 0.02069(17) Uani 1 1 d . . . . . F22 F 0.77576(9) 0.41281(6) 0.98886(6) 0.02138(17) Uani 1 1 d . . . . . F23 F 0.61696(8) 0.45071(7) 0.92816(6) 0.02102(17) Uani 1 1 d . . . . . F24 F 0.94216(8) 0.13527(7) 0.91469(6) 0.02226(18) Uani 1 1 d . . . . . F25 F 0.78838(9) 0.20941(6) 1.00887(6) 0.02249(18) Uani 1 1 d . . . . . F26 F 0.85543(9) 0.04728(7) 1.04781(6) 0.02558(19) Uani 1 1 d . . . . . F27 F 0.55617(8) 0.23585(6) 0.98283(6) 0.02091(17) Uani 1 1 d . . . . . F28 F 0.59329(9) 0.09505(7) 1.08498(6) 0.0276(2) Uani 1 1 d . . . . . F29 F 0.51639(8) 0.10080(7) 0.97315(7) 0.02582(19) Uani 1 1 d . . . . . F30 F 0.73512(9) -0.06528(6) 1.00698(6) 0.02566(19) Uani 1 1 d . . . . . F31 F 0.89177(9) -0.02937(6) 0.88943(6) 0.02471(19) Uani 1 1 d . . . . . F32 F 0.70596(9) -0.01023(6) 0.86914(6) 0.02366(18) Uani 1 1 d . . . . . F33 F 0.37118(9) 0.45092(8) 0.88422(7) 0.0325(2) Uani 1 1 d . . . . . F34 F 0.41199(10) 0.56282(7) 0.75603(8) 0.0341(2) Uani 1 1 d . . . . . F35 F 0.25660(8) 0.48802(8) 0.78705(8) 0.0325(2) Uani 1 1 d . . . . . F36 F 0.58453(10) 0.49091(9) 0.61375(7) 0.0390(3) Uani 1 1 d . . . . . F37 F 0.39636(10) 0.48659(9) 0.61223(7) 0.0388(3) Uani 1 1 d . . . . . F38 F 0.54979(10) 0.35622(9) 0.59900(7) 0.0380(3) Uani 1 1 d . . . . . F39 F 0.32026(9) 0.31067(8) 0.73033(8) 0.0345(2) Uani 1 1 d . . . . . F40 F 0.49644(10) 0.21434(7) 0.75917(8) 0.0355(2) Uani 1 1 d . . . . . F2 F -0.09000(9) 0.14988(7) 0.34181(6) 0.0280(2) Uani 1 1 d . . . . . C1 C 0.54550(12) 0.24990(10) 0.20033(9) 0.0143(2) Uani 1 1 d . . . . . C2 C 0.46200(13) 0.05479(10) 0.28466(9) 0.0158(3) Uani 1 1 d . . . . . O1 O 0.55098(10) 0.31026(7) 0.13422(7) 0.0189(2) Uani 1 1 d . . . . . O2 O 0.42477(10) 0.00108(8) 0.26535(7) 0.0213(2) Uani 1 1 d . . . . . F3 F 0.16301(9) 0.13225(7) 0.32621(6) 0.02601(19) Uani 1 1 d . . . . . F4 F 0.31292(8) 0.21258(7) 0.16381(7) 0.02421(19) Uani 1 1 d . . . . . F5 F 0.35180(10) 0.27406(8) 0.86660(7) 0.0348(2) Uani 1 1 d . . . . . O3 O 0.26742(10) 0.25583(8) 0.41234(7) 0.0241(2) Uani 1 1 d . . . . . O4 O 0.63523(11) 0.26356(9) 0.40888(8) 0.0262(2) Uani 1 1 d . . . . . O5 O 0.80451(10) 0.01822(9) 0.25804(8) 0.0270(2) Uani 1 1 d . . . . . O6 O 0.39200(11) 0.17448(8) 0.59921(8) 0.0256(2) Uani 1 1 d . . . . . O7 O 0.22848(10) -0.00441(8) 0.49891(7) 0.0204(2) Uani 1 1 d . . . . . O8 O 0.80832(9) 0.35540(7) 0.81638(7) 0.01442(18) Uani 1 1 d . . . . . O9 O 0.57649(9) 0.36448(7) 0.78046(7) 0.01581(19) Uani 1 1 d . . . . . O10 O 0.79988(9) 0.29000(7) 0.66317(6) 0.01505(18) Uani 1 1 d . . . . . O11 O 0.74064(9) 0.17227(7) 0.84513(6) 0.01435(18) Uani 1 1 d . . . . . C3 C 0.36200(13) 0.21411(10) 0.37779(9) 0.0158(3) Uani 1 1 d . . . . . C22 C 0.83234(14) 0.12574(10) 0.97616(10) 0.0177(3) Uani 1 1 d . . . . . C23 C 0.76712(14) -0.00044(10) 0.92485(10) 0.0182(3) Uani 1 1 d . . . . . C24 C 0.40804(15) 0.29616(12) 0.77627(12) 0.0240(3) Uani 1 1 d . . . . . C25 C 0.50043(15) 0.43146(13) 0.64153(11) 0.0265(3) Uani 1 1 d . . . . . C26 C 0.37489(14) 0.47355(11) 0.79514(11) 0.0214(3) Uani 1 1 d . . . . . C27 C 0.88088(15) 0.13631(12) 0.61214(11) 0.0238(3) Uani 1 1 d . . . . . C28 C 0.89977(13) 0.31125(12) 0.50476(10) 0.0208(3) Uani 1 1 d . . . . . C29 C 1.02744(13) 0.23350(11) 0.62678(10) 0.0180(3) Uani 1 1 d . . . . . C4 C 0.60109(13) 0.21992(10) 0.37607(10) 0.0170(3) Uani 1 1 d . . . . . C5 C 0.70658(13) 0.06375(10) 0.28132(9) 0.0171(3) Uani 1 1 d . . . . . C6 C 0.43084(13) 0.11086(10) 0.56318(9) 0.0162(3) Uani 1 1 d . . . . . C7 C 0.32734(13) -0.00215(10) 0.49902(9) 0.0143(2) Uani 1 1 d . . . . . C8 C 0.14010(14) 0.27234(11) 0.09259(10) 0.0190(3) Uani 1 1 d . . . . . H1 H 0.193874 0.299541 0.035067 0.023 Uiso 1 1 calc R U . . . C9 C 0.01112(14) 0.28217(11) 0.10102(10) 0.0202(3) Uani 1 1 d . . . . . H2 H -0.024591 0.316524 0.049330 0.024 Uiso 1 1 calc R U . . . C10 C -0.06375(13) 0.24170(11) 0.18480(10) 0.0188(3) Uani 1 1 d . . . . . C11 C -0.01487(13) 0.19055(11) 0.26118(10) 0.0181(3) Uani 1 1 d . . . . . C12 C 0.11277(14) 0.18129(10) 0.25306(10) 0.0174(3) Uani 1 1 d . . . . . C13 C 0.18829(13) 0.22266(10) 0.16883(10) 0.0171(3) Uani 1 1 d . . . . . C14 C 0.73472(13) 0.11191(10) 0.93175(9) 0.0139(2) Uani 1 1 d . . . . . C15 C 0.89837(12) 0.24403(10) 0.60491(9) 0.0146(2) Uani 1 1 d . . . . . C16 C 0.47035(12) 0.38951(10) 0.74884(9) 0.0154(2) Uani 1 1 d . . . . . C17 C 0.82222(12) 0.44367(9) 0.82408(9) 0.0127(2) Uani 1 1 d . . . . . C18 C 0.96338(13) 0.43071(11) 0.82621(10) 0.0178(3) Uani 1 1 d . . . . . C19 C 0.79410(13) 0.53329(10) 0.74048(9) 0.0159(3) Uani 1 1 d . . . . . C20 C 0.73058(13) 0.46942(10) 0.91529(9) 0.0151(2) Uani 1 1 d . . . . . C21 C 0.59823(14) 0.13581(10) 0.99397(10) 0.0180(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.01085(5) 0.01187(5) 0.00950(5) -0.00143(4) -0.00300(4) -0.00255(4) Ru2 0.01154(7) 0.01098(6) 0.00885(6) -0.00190(5) -0.00313(5) -0.00177(5) Al6 0.01087(17) 0.01102(17) 0.01017(17) -0.00318(14) -0.00211(14) -0.00180(13) F1 0.0146(4) 0.0369(5) 0.0337(5) -0.0038(4) -0.0095(4) -0.0066(4) F6 0.0340(5) 0.0274(5) 0.0204(5) 0.0031(4) -0.0058(4) -0.0054(4) F7 0.0168(4) 0.0499(6) 0.0131(4) -0.0086(4) 0.0023(3) -0.0053(4) F8 0.0258(5) 0.0371(5) 0.0333(5) -0.0270(4) 0.0036(4) -0.0069(4) F9 0.0213(5) 0.0408(6) 0.0551(7) -0.0304(5) 0.0072(4) -0.0159(4) F10 0.0184(4) 0.0638(7) 0.0197(5) -0.0155(4) -0.0068(4) -0.0072(4) F11 0.0435(6) 0.0185(4) 0.0304(5) -0.0067(4) 0.0033(4) -0.0069(4) F12 0.0149(4) 0.0294(5) 0.0201(4) -0.0098(4) -0.0010(3) 0.0019(3) F13 0.0210(4) 0.0279(5) 0.0328(5) -0.0084(4) -0.0076(4) -0.0102(4) F14 0.0222(4) 0.0381(5) 0.0143(4) -0.0080(4) -0.0069(3) 0.0021(4) F15 0.0306(5) 0.0225(4) 0.0134(4) -0.0047(3) -0.0052(3) -0.0048(4) F16 0.0180(4) 0.0173(4) 0.0247(4) -0.0011(3) -0.0094(3) -0.0011(3) F17 0.0285(5) 0.0163(4) 0.0216(4) -0.0006(3) -0.0063(4) -0.0117(3) F18 0.0147(4) 0.0365(5) 0.0241(5) -0.0106(4) 0.0005(3) -0.0064(4) F19 0.0221(4) 0.0289(5) 0.0351(5) -0.0154(4) -0.0103(4) -0.0082(4) F20 0.0207(4) 0.0241(4) 0.0279(5) -0.0063(4) -0.0136(4) 0.0012(3) F21 0.0270(4) 0.0141(4) 0.0208(4) -0.0081(3) -0.0027(3) -0.0032(3) F22 0.0291(5) 0.0203(4) 0.0138(4) -0.0041(3) -0.0068(3) -0.0022(3) F23 0.0157(4) 0.0255(4) 0.0212(4) -0.0079(3) 0.0015(3) -0.0076(3) F24 0.0178(4) 0.0242(4) 0.0247(4) -0.0039(3) -0.0062(3) -0.0055(3) F25 0.0307(5) 0.0199(4) 0.0219(4) -0.0090(3) -0.0098(4) -0.0051(3) F26 0.0337(5) 0.0214(4) 0.0213(4) 0.0031(3) -0.0157(4) -0.0049(4) F27 0.0221(4) 0.0164(4) 0.0205(4) -0.0067(3) -0.0019(3) 0.0003(3) F28 0.0317(5) 0.0280(5) 0.0131(4) -0.0001(3) 0.0018(4) -0.0047(4) F29 0.0198(4) 0.0256(5) 0.0326(5) -0.0068(4) -0.0019(4) -0.0110(4) F30 0.0360(5) 0.0139(4) 0.0238(5) 0.0025(3) -0.0076(4) -0.0080(4) F31 0.0229(4) 0.0177(4) 0.0306(5) -0.0098(4) -0.0045(4) 0.0022(3) F32 0.0325(5) 0.0172(4) 0.0268(5) -0.0080(3) -0.0117(4) -0.0058(4) F33 0.0254(5) 0.0456(6) 0.0284(5) -0.0251(5) -0.0038(4) 0.0042(4) F34 0.0295(5) 0.0180(4) 0.0590(7) -0.0124(4) -0.0194(5) 0.0015(4) F35 0.0126(4) 0.0393(6) 0.0509(6) -0.0251(5) -0.0111(4) 0.0058(4) F36 0.0332(6) 0.0520(7) 0.0245(5) 0.0092(5) -0.0078(4) -0.0176(5) F37 0.0297(5) 0.0533(7) 0.0291(5) -0.0026(5) -0.0197(4) 0.0030(5) F38 0.0285(5) 0.0649(7) 0.0239(5) -0.0254(5) -0.0073(4) 0.0023(5) F39 0.0258(5) 0.0382(6) 0.0530(7) -0.0222(5) -0.0179(5) -0.0056(4) F40 0.0320(5) 0.0222(5) 0.0587(7) -0.0204(5) -0.0160(5) 0.0019(4) F2 0.0230(5) 0.0364(5) 0.0177(4) -0.0016(4) 0.0014(4) -0.0086(4) C1 0.0124(6) 0.0160(6) 0.0152(6) -0.0057(5) -0.0030(5) -0.0023(5) C2 0.0165(6) 0.0169(6) 0.0111(6) -0.0006(5) -0.0035(5) -0.0023(5) O1 0.0223(5) 0.0170(5) 0.0148(5) -0.0010(4) -0.0034(4) -0.0045(4) O2 0.0269(5) 0.0213(5) 0.0194(5) -0.0038(4) -0.0083(4) -0.0092(4) F3 0.0263(5) 0.0323(5) 0.0195(4) -0.0033(4) -0.0134(4) -0.0011(4) F4 0.0139(4) 0.0239(4) 0.0351(5) -0.0047(4) -0.0089(4) -0.0040(3) F5 0.0313(5) 0.0356(5) 0.0340(6) -0.0019(4) -0.0010(4) -0.0169(4) O3 0.0161(5) 0.0259(5) 0.0195(5) 0.0007(4) -0.0010(4) 0.0012(4) O4 0.0294(6) 0.0272(6) 0.0294(6) -0.0088(5) -0.0124(5) -0.0094(5) O5 0.0208(5) 0.0273(6) 0.0243(6) -0.0053(5) -0.0026(4) 0.0036(4) O6 0.0313(6) 0.0227(5) 0.0256(6) -0.0129(4) -0.0089(5) 0.0002(4) O7 0.0166(5) 0.0245(5) 0.0214(5) -0.0059(4) -0.0058(4) -0.0046(4) O8 0.0164(5) 0.0120(4) 0.0173(5) -0.0050(4) -0.0066(4) -0.0024(3) O9 0.0115(4) 0.0203(5) 0.0155(5) -0.0064(4) -0.0050(4) 0.0009(4) O10 0.0140(4) 0.0179(5) 0.0117(4) -0.0061(4) -0.0007(3) -0.0009(4) O11 0.0176(5) 0.0130(4) 0.0116(4) -0.0020(3) -0.0029(4) -0.0037(3) C3 0.0168(6) 0.0167(6) 0.0122(6) 0.0023(5) -0.0058(5) -0.0049(5) C22 0.0224(7) 0.0145(6) 0.0159(6) -0.0014(5) -0.0077(5) -0.0029(5) C23 0.0220(7) 0.0128(6) 0.0189(7) -0.0030(5) -0.0055(5) -0.0027(5) C24 0.0201(7) 0.0239(7) 0.0322(8) -0.0124(6) -0.0079(6) -0.0030(6) C25 0.0209(7) 0.0384(9) 0.0186(7) -0.0050(6) -0.0089(6) -0.0015(6) C26 0.0141(6) 0.0220(7) 0.0302(8) -0.0124(6) -0.0074(6) 0.0020(5) C27 0.0209(7) 0.0255(7) 0.0266(8) -0.0153(6) 0.0039(6) -0.0078(6) C28 0.0144(6) 0.0347(8) 0.0126(6) -0.0069(6) -0.0017(5) -0.0046(6) C29 0.0162(6) 0.0226(7) 0.0145(6) -0.0063(5) -0.0029(5) -0.0021(5) C4 0.0149(6) 0.0178(6) 0.0160(6) -0.0018(5) -0.0040(5) -0.0024(5) C5 0.0194(7) 0.0172(6) 0.0133(6) -0.0011(5) -0.0049(5) -0.0036(5) C6 0.0166(6) 0.0178(6) 0.0137(6) -0.0013(5) -0.0061(5) -0.0030(5) C7 0.0186(6) 0.0129(6) 0.0103(6) -0.0021(5) -0.0037(5) -0.0022(5) C8 0.0207(7) 0.0173(6) 0.0183(7) -0.0023(5) -0.0039(5) -0.0060(5) C9 0.0221(7) 0.0199(7) 0.0200(7) -0.0018(5) -0.0104(6) -0.0043(5) C10 0.0146(6) 0.0208(7) 0.0239(7) -0.0062(6) -0.0075(5) -0.0040(5) C11 0.0179(7) 0.0199(6) 0.0152(6) -0.0052(5) -0.0012(5) -0.0043(5) C12 0.0193(7) 0.0167(6) 0.0181(7) -0.0059(5) -0.0091(5) 0.0002(5) C13 0.0136(6) 0.0156(6) 0.0241(7) -0.0075(5) -0.0057(5) -0.0021(5) C14 0.0172(6) 0.0110(6) 0.0131(6) -0.0029(5) -0.0032(5) -0.0029(5) C15 0.0126(6) 0.0194(6) 0.0127(6) -0.0064(5) -0.0008(5) -0.0043(5) C16 0.0119(6) 0.0183(6) 0.0161(6) -0.0068(5) -0.0041(5) 0.0003(5) C17 0.0135(6) 0.0120(6) 0.0132(6) -0.0032(5) -0.0041(5) -0.0027(4) C18 0.0167(6) 0.0201(6) 0.0196(7) -0.0073(5) -0.0058(5) -0.0041(5) C19 0.0177(6) 0.0151(6) 0.0155(6) -0.0032(5) -0.0046(5) -0.0046(5) C20 0.0172(6) 0.0137(6) 0.0147(6) -0.0039(5) -0.0039(5) -0.0034(5) C21 0.0200(7) 0.0159(6) 0.0149(6) -0.0021(5) -0.0010(5) -0.0045(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 C3 1.9681(15) . ? Ru1 C4 1.9795(15) . ? Ru1 C2 1.9861(15) . ? Ru1 C5 1.9875(15) . ? Ru1 C1 1.9992(15) . ? Ru1 Ru2 2.8960(8) . ? Ru2 C6 1.9630(15) . ? Ru2 C6 1.9630(15) 2_656 ? Ru2 C7 1.9646(15) . ? Ru2 C7 1.9647(15) 2_656 ? Al6 O9 1.7249(11) . ? Al6 O8 1.7272(11) . ? Al6 O10 1.7280(11) . ? Al6 O11 1.7296(12) . ? F1 C10 1.3568(16) . ? F6 C28 1.3222(19) . ? F7 C28 1.3419(17) . ? F8 C27 1.3376(17) . ? F9 C27 1.3344(19) . ? F10 C28 1.3322(17) . ? F11 C27 1.335(2) . ? F12 C29 1.3515(16) . ? F13 C29 1.3283(18) . ? F14 C29 1.3272(17) . ? F15 C19 1.3236(16) . ? F16 C19 1.3449(16) . ? F17 C19 1.3414(16) . ? F18 C18 1.3289(17) . ? F19 C18 1.3421(16) . ? F20 C18 1.3299(17) . ? F21 C20 1.3412(16) . ? F22 C20 1.3378(16) . ? F23 C20 1.3254(16) . ? F24 C22 1.3229(17) . ? F25 C22 1.3423(17) . ? F26 C22 1.3411(16) . ? F27 C21 1.3323(17) . ? F28 C21 1.3510(17) . ? F29 C21 1.3274(17) . ? F30 C23 1.3366(17) . ? F31 C23 1.3349(17) . ? F32 C23 1.3313(17) . ? F33 C26 1.3221(19) . ? F34 C26 1.3428(19) . ? F35 C26 1.3334(17) . ? F36 C25 1.329(2) . ? F37 C25 1.3388(18) . ? F38 C25 1.329(2) . ? F39 C24 1.3362(18) . ? F40 C24 1.3335(18) . ? F2 C11 1.3412(17) . ? C1 O1 1.1145(17) . ? C2 O2 1.1208(17) . ? F3 C12 1.3433(16) . ? F4 C13 1.3534(16) . ? F5 C24 1.334(2) . ? O3 C3 1.1234(18) . ? O4 C4 1.1215(18) . ? O5 C5 1.1225(18) . ? O6 C6 1.1241(18) . ? O7 C7 1.1270(17) . ? O8 C17 1.3498(16) . ? O9 C16 1.3529(16) . ? O10 C15 1.3492(16) . ? O11 C14 1.3515(16) . ? C22 C14 1.5601(19) . ? C23 C14 1.5585(19) . ? C24 C16 1.553(2) . ? C25 C16 1.559(2) . ? C26 C16 1.5580(19) . ? C27 C15 1.558(2) . ? C28 C15 1.558(2) . ? C29 C15 1.557(2) . ? C8 C13 1.372(2) . ? C8 C9 1.391(2) . ? C8 H1 0.9500 . ? C9 C10 1.370(2) . ? C9 H2 0.9500 . ? C10 C11 1.381(2) . ? C11 C12 1.378(2) . ? C12 C13 1.381(2) . ? C14 C21 1.552(2) . ? C17 C19 1.5542(19) . ? C17 C20 1.5610(19) . ? C17 C18 1.5622(19) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 Ru1 C4 87.01(6) . . ? C3 Ru1 C2 92.00(6) . . ? C4 Ru1 C2 171.27(5) . . ? C3 Ru1 C5 172.15(5) . . ? C4 Ru1 C5 90.81(6) . . ? C2 Ru1 C5 89.02(6) . . ? C3 Ru1 C1 93.83(6) . . ? C4 Ru1 C1 93.39(6) . . ? C2 Ru1 C1 95.33(6) . . ? C5 Ru1 C1 93.82(6) . . ? C3 Ru1 Ru2 82.72(4) . . ? C4 Ru1 Ru2 86.52(5) . . ? C2 Ru1 Ru2 84.76(5) . . ? C5 Ru1 Ru2 89.63(5) . . ? C1 Ru1 Ru2 176.55(4) . . ? C6 Ru2 C6 180.0 . 2_656 ? C6 Ru2 C7 90.43(6) . . ? C6 Ru2 C7 89.57(6) 2_656 . ? C6 Ru2 C7 89.57(6) . 2_656 ? C6 Ru2 C7 90.43(6) 2_656 2_656 ? C7 Ru2 C7 180.0 . 2_656 ? C6 Ru2 Ru1 89.15(5) . 2_656 ? C6 Ru2 Ru1 90.85(5) 2_656 2_656 ? C7 Ru2 Ru1 88.37(4) . 2_656 ? C7 Ru2 Ru1 91.63(4) 2_656 2_656 ? C6 Ru2 Ru1 90.85(5) . . ? C6 Ru2 Ru1 89.15(5) 2_656 . ? C7 Ru2 Ru1 91.63(4) . . ? C7 Ru2 Ru1 88.37(4) 2_656 . ? Ru1 Ru2 Ru1 180.0 2_656 . ? O9 Al6 O8 108.86(6) . . ? O9 Al6 O10 106.50(5) . . ? O8 Al6 O10 112.47(5) . . ? O9 Al6 O11 114.43(5) . . ? O8 Al6 O11 106.74(5) . . ? O10 Al6 O11 107.96(5) . . ? O1 C1 Ru1 178.19(12) . . ? O2 C2 Ru1 177.60(12) . . ? C17 O8 Al6 147.54(9) . . ? C16 O9 Al6 148.69(9) . . ? C15 O10 Al6 145.79(9) . . ? C14 O11 Al6 145.89(9) . . ? O3 C3 Ru1 176.19(13) . . ? F24 C22 F26 108.07(11) . . ? F24 C22 F25 107.66(11) . . ? F26 C22 F25 106.66(11) . . ? F24 C22 C14 111.07(11) . . ? F26 C22 C14 112.20(11) . . ? F25 C22 C14 110.97(11) . . ? F32 C23 F31 107.48(12) . . ? F32 C23 F30 107.61(12) . . ? F31 C23 F30 107.92(11) . . ? F32 C23 C14 110.56(11) . . ? F31 C23 C14 110.40(11) . . ? F30 C23 C14 112.67(12) . . ? F40 C24 F5 107.14(13) . . ? F40 C24 F39 107.79(12) . . ? F5 C24 F39 107.63(13) . . ? F40 C24 C16 110.30(13) . . ? F5 C24 C16 110.98(12) . . ? F39 C24 C16 112.78(13) . . ? F36 C25 F38 107.72(14) . . ? F36 C25 F37 107.52(14) . . ? F38 C25 F37 107.72(13) . . ? F36 C25 C16 110.41(13) . . ? F38 C25 C16 111.11(13) . . ? F37 C25 C16 112.17(13) . . ? F33 C26 F35 108.17(13) . . ? F33 C26 F34 107.14(12) . . ? F35 C26 F34 107.25(12) . . ? F33 C26 C16 110.83(12) . . ? F35 C26 C16 113.01(12) . . ? F34 C26 C16 110.21(12) . . ? F9 C27 F11 107.33(13) . . ? F9 C27 F8 107.58(13) . . ? F11 C27 F8 107.47(13) . . ? F9 C27 C15 110.23(12) . . ? F11 C27 C15 111.08(12) . . ? F8 C27 C15 112.92(12) . . ? F6 C28 F10 107.63(13) . . ? F6 C28 F7 108.07(12) . . ? F10 C28 F7 107.17(12) . . ? F6 C28 C15 111.06(12) . . ? F10 C28 C15 110.54(12) . . ? F7 C28 C15 112.19(12) . . ? F14 C29 F13 107.74(12) . . ? F14 C29 F12 107.11(11) . . ? F13 C29 F12 107.05(12) . . ? F14 C29 C15 110.70(11) . . ? F13 C29 C15 111.66(11) . . ? F12 C29 C15 112.33(11) . . ? O4 C4 Ru1 177.50(13) . . ? O5 C5 Ru1 179.38(14) . . ? O6 C6 Ru2 179.55(12) . . ? O7 C7 Ru2 179.29(13) . . ? C13 C8 C9 118.83(13) . . ? C13 C8 H1 120.6 . . ? C9 C8 H1 120.6 . . ? C10 C9 C8 119.16(13) . . ? C10 C9 H2 120.4 . . ? C8 C9 H2 120.4 . . ? F1 C10 C9 120.64(13) . . ? F1 C10 C11 117.37(13) . . ? C9 C10 C11 121.99(13) . . ? F2 C11 C12 120.45(13) . . ? F2 C11 C10 120.65(13) . . ? C12 C11 C10 118.90(13) . . ? F3 C12 C11 120.28(13) . . ? F3 C12 C13 120.49(13) . . ? C11 C12 C13 119.22(13) . . ? F4 C13 C8 120.66(13) . . ? F4 C13 C12 117.46(13) . . ? C8 C13 C12 121.89(13) . . ? O11 C14 C21 109.92(11) . . ? O11 C14 C23 107.55(11) . . ? C21 C14 C23 109.53(11) . . ? O11 C14 C22 111.89(11) . . ? C21 C14 C22 109.24(11) . . ? C23 C14 C22 108.68(11) . . ? O10 C15 C29 111.22(11) . . ? O10 C15 C28 107.42(11) . . ? C29 C15 C28 109.36(11) . . ? O10 C15 C27 110.44(11) . . ? C29 C15 C27 108.98(12) . . ? C28 C15 C27 109.40(12) . . ? O9 C16 C24 110.80(12) . . ? O9 C16 C26 107.29(11) . . ? C24 C16 C26 108.85(12) . . ? O9 C16 C25 111.42(12) . . ? C24 C16 C25 109.22(12) . . ? C26 C16 C25 109.20(12) . . ? O8 C17 C19 111.71(11) . . ? O8 C17 C20 110.05(11) . . ? C19 C17 C20 109.00(11) . . ? O8 C17 C18 108.10(10) . . ? C19 C17 C18 108.24(11) . . ? C20 C17 C18 109.71(11) . . ? F18 C18 F20 107.72(12) . . ? F18 C18 F19 107.95(12) . . ? F20 C18 F19 107.49(12) . . ? F18 C18 C17 110.75(11) . . ? F20 C18 C17 110.75(11) . . ? F19 C18 C17 112.01(11) . . ? F15 C19 F17 108.07(11) . . ? F15 C19 F16 107.05(11) . . ? F17 C19 F16 106.81(11) . . ? F15 C19 C17 111.41(11) . . ? F17 C19 C17 112.34(11) . . ? F16 C19 C17 110.90(11) . . ? F23 C20 F22 107.56(11) . . ? F23 C20 F21 107.75(11) . . ? F22 C20 F21 107.39(11) . . ? F23 C20 C17 110.56(11) . . ? F22 C20 C17 110.98(11) . . ? F21 C20 C17 112.40(11) . . ? F29 C21 F27 107.52(12) . . ? F29 C21 F28 107.59(11) . . ? F27 C21 F28 106.98(11) . . ? F29 C21 C14 111.49(12) . . ? F27 C21 C14 110.59(11) . . ? F28 C21 C14 112.43(12) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O9 Al6 O8 C17 -31.47(18) . . . . ? O10 Al6 O8 C17 86.31(17) . . . . ? O11 Al6 O8 C17 -155.47(16) . . . . ? O8 Al6 O9 C16 156.75(17) . . . . ? O10 Al6 O9 C16 35.24(19) . . . . ? O11 Al6 O9 C16 -83.95(19) . . . . ? O9 Al6 O10 C15 -165.07(15) . . . . ? O8 Al6 O10 C15 75.76(17) . . . . ? O11 Al6 O10 C15 -41.74(17) . . . . ? O9 Al6 O11 C14 -79.30(17) . . . . ? O8 Al6 O11 C14 41.19(17) . . . . ? O10 Al6 O11 C14 162.33(15) . . . . ? C13 C8 C9 C10 -0.3(2) . . . . ? C8 C9 C10 F1 179.94(13) . . . . ? C8 C9 C10 C11 -0.6(2) . . . . ? F1 C10 C11 F2 0.9(2) . . . . ? C9 C10 C11 F2 -178.60(13) . . . . ? F1 C10 C11 C12 -179.54(13) . . . . ? C9 C10 C11 C12 0.9(2) . . . . ? F2 C11 C12 F3 -0.7(2) . . . . ? C10 C11 C12 F3 179.78(13) . . . . ? F2 C11 C12 C13 179.09(12) . . . . ? C10 C11 C12 C13 -0.5(2) . . . . ? C9 C8 C13 F4 -179.18(13) . . . . ? C9 C8 C13 C12 0.8(2) . . . . ? F3 C12 C13 F4 -0.67(19) . . . . ? C11 C12 C13 F4 179.56(12) . . . . ? F3 C12 C13 C8 179.37(13) . . . . ? C11 C12 C13 C8 -0.4(2) . . . . ? Al6 O11 C14 C21 64.48(19) . . . . ? Al6 O11 C14 C23 -176.34(12) . . . . ? Al6 O11 C14 C22 -57.1(2) . . . . ? F32 C23 C14 O11 -44.58(15) . . . . ? F31 C23 C14 O11 74.22(14) . . . . ? F30 C23 C14 O11 -165.04(11) . . . . ? F32 C23 C14 C21 74.84(14) . . . . ? F31 C23 C14 C21 -166.35(11) . . . . ? F30 C23 C14 C21 -45.61(15) . . . . ? F32 C23 C14 C22 -165.89(11) . . . . ? F31 C23 C14 C22 -47.09(15) . . . . ? F30 C23 C14 C22 73.65(14) . . . . ? F24 C22 C14 O11 -39.92(15) . . . . ? F26 C22 C14 O11 -160.99(11) . . . . ? F25 C22 C14 O11 79.80(14) . . . . ? F24 C22 C14 C21 -161.86(11) . . . . ? F26 C22 C14 C21 77.07(14) . . . . ? F25 C22 C14 C21 -42.14(14) . . . . ? F24 C22 C14 C23 78.70(13) . . . . ? F26 C22 C14 C23 -42.38(15) . . . . ? F25 C22 C14 C23 -161.58(11) . . . . ? Al6 O10 C15 C29 -45.8(2) . . . . ? Al6 O10 C15 C28 -165.45(13) . . . . ? Al6 O10 C15 C27 75.32(19) . . . . ? F14 C29 C15 O10 43.50(16) . . . . ? F13 C29 C15 O10 -76.54(14) . . . . ? F12 C29 C15 O10 163.19(11) . . . . ? F14 C29 C15 C28 161.98(11) . . . . ? F13 C29 C15 C28 41.94(15) . . . . ? F12 C29 C15 C28 -78.34(14) . . . . ? F14 C29 C15 C27 -78.48(14) . . . . ? F13 C29 C15 C27 161.48(11) . . . . ? F12 C29 C15 C27 41.20(15) . . . . ? F6 C28 C15 O10 46.64(15) . . . . ? F10 C28 C15 O10 -72.74(15) . . . . ? F7 C28 C15 O10 167.70(11) . . . . ? F6 C28 C15 C29 -74.18(14) . . . . ? F10 C28 C15 C29 166.43(12) . . . . ? F7 C28 C15 C29 46.88(16) . . . . ? F6 C28 C15 C27 166.54(11) . . . . ? F10 C28 C15 C27 47.15(15) . . . . ? F7 C28 C15 C27 -72.40(15) . . . . ? F9 C27 C15 O10 40.05(16) . . . . ? F11 C27 C15 O10 -78.79(15) . . . . ? F8 C27 C15 O10 160.40(12) . . . . ? F9 C27 C15 C29 162.50(12) . . . . ? F11 C27 C15 C29 43.67(15) . . . . ? F8 C27 C15 C29 -77.14(16) . . . . ? F9 C27 C15 C28 -77.98(15) . . . . ? F11 C27 C15 C28 163.19(11) . . . . ? F8 C27 C15 C28 42.37(17) . . . . ? Al6 O9 C16 C24 65.7(2) . . . . ? Al6 O9 C16 C26 -175.59(14) . . . . ? Al6 O9 C16 C25 -56.1(2) . . . . ? F40 C24 C16 O9 -45.82(16) . . . . ? F5 C24 C16 O9 72.76(15) . . . . ? F39 C24 C16 O9 -166.39(12) . . . . ? F40 C24 C16 C26 -163.58(12) . . . . ? F5 C24 C16 C26 -45.00(16) . . . . ? F39 C24 C16 C26 75.85(16) . . . . ? F40 C24 C16 C25 77.28(15) . . . . ? F5 C24 C16 C25 -164.14(12) . . . . ? F39 C24 C16 C25 -43.29(16) . . . . ? F33 C26 C16 O9 -43.66(16) . . . . ? F35 C26 C16 O9 -165.26(12) . . . . ? F34 C26 C16 O9 74.76(15) . . . . ? F33 C26 C16 C24 76.30(15) . . . . ? F35 C26 C16 C24 -45.31(17) . . . . ? F34 C26 C16 C24 -165.28(12) . . . . ? F33 C26 C16 C25 -164.55(12) . . . . ? F35 C26 C16 C25 73.84(16) . . . . ? F34 C26 C16 C25 -46.13(16) . . . . ? F36 C25 C16 O9 -39.53(17) . . . . ? F38 C25 C16 O9 79.93(15) . . . . ? F37 C25 C16 O9 -159.43(13) . . . . ? F36 C25 C16 C24 -162.27(13) . . . . ? F38 C25 C16 C24 -42.81(16) . . . . ? F37 C25 C16 C24 77.83(16) . . . . ? F36 C25 C16 C26 78.81(15) . . . . ? F38 C25 C16 C26 -161.73(12) . . . . ? F37 C25 C16 C26 -41.10(17) . . . . ? Al6 O8 C17 C19 -31.6(2) . . . . ? Al6 O8 C17 C20 89.66(18) . . . . ? Al6 O8 C17 C18 -150.54(14) . . . . ? O8 C17 C18 F18 77.08(14) . . . . ? C19 C17 C18 F18 -44.09(14) . . . . ? C20 C17 C18 F18 -162.91(11) . . . . ? O8 C17 C18 F20 -42.37(15) . . . . ? C19 C17 C18 F20 -163.54(11) . . . . ? C20 C17 C18 F20 77.64(13) . . . . ? O8 C17 C18 F19 -162.35(11) . . . . ? C19 C17 C18 F19 76.48(14) . . . . ? C20 C17 C18 F19 -42.34(15) . . . . ? O8 C17 C19 F15 -40.41(15) . . . . ? C20 C17 C19 F15 -162.24(11) . . . . ? C18 C17 C19 F15 78.49(13) . . . . ? O8 C17 C19 F17 -161.83(11) . . . . ? C20 C17 C19 F17 76.34(14) . . . . ? C18 C17 C19 F17 -42.93(14) . . . . ? O8 C17 C19 F16 78.72(14) . . . . ? C20 C17 C19 F16 -43.10(14) . . . . ? C18 C17 C19 F16 -162.37(10) . . . . ? O8 C17 C20 F23 -42.30(14) . . . . ? C19 C17 C20 F23 80.53(13) . . . . ? C18 C17 C20 F23 -161.11(11) . . . . ? O8 C17 C20 F22 76.98(13) . . . . ? C19 C17 C20 F22 -160.19(10) . . . . ? C18 C17 C20 F22 -41.84(14) . . . . ? O8 C17 C20 F21 -162.74(11) . . . . ? C19 C17 C20 F21 -39.91(14) . . . . ? C18 C17 C20 F21 78.44(13) . . . . ? O11 C14 C21 F29 72.96(14) . . . . ? C23 C14 C21 F29 -45.00(15) . . . . ? C22 C14 C21 F29 -163.92(11) . . . . ? O11 C14 C21 F27 -46.60(15) . . . . ? C23 C14 C21 F27 -164.56(11) . . . . ? C22 C14 C21 F27 76.52(14) . . . . ? O11 C14 C21 F28 -166.12(11) . . . . ? C23 C14 C21 F28 75.92(14) . . . . ? C22 C14 C21 F28 -43.00(15) . . . . ? _shelx_res_file ; TITL p-1_a.res in P-1 p-1_a.res created by SHELXL-2018/3 at 14:12:44 on 08-Feb-2022 REM Old TITL p-1 in P-1 REM SHELXT solution in P-1: R1 0.074, Rweak 0.004, Alpha 0.058 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C62 O18 F80 Al2 Ru3 CELL 0.71073 11.2982 14.1638 15.6975 71.621 71.685 73.388 ZERR 1.000 0.0037 0.0059 0.0051 0.010 0.018 0.012 LATT 1 SFAC C O F AL RU H UNIT 58 22 80 2 3 4 TEMP -167.150 L.S. 10 BOND $H CONF MORE -1 LIST 4 HTAB ACTA OMIT 1 -1 1 FMAP 2 PLAN 20 WGHT 0.018100 1.546600 FVAR 0.30557 RU1 5 0.533124 0.145030 0.321113 11.00000 0.01085 0.01187 = 0.00950 -0.00143 -0.00300 -0.00255 RU2 5 0.500000 0.000000 0.500000 10.50000 0.01154 0.01098 = 0.00885 -0.00190 -0.00313 -0.00177 AL6 4 0.730173 0.295554 0.776958 11.00000 0.01087 0.01102 = 0.01017 -0.00318 -0.00211 -0.00180 F1 3 -0.189918 0.250046 0.195373 11.00000 0.01462 0.03687 = 0.03373 -0.00380 -0.00949 -0.00662 F6 3 0.886934 0.408179 0.500867 11.00000 0.03402 0.02743 = 0.02041 0.00314 -0.00578 -0.00545 F7 3 1.007898 0.283568 0.443318 11.00000 0.01684 0.04988 = 0.01306 -0.00855 0.00235 -0.00525 F8 3 0.950839 0.100353 0.538441 11.00000 0.02583 0.03710 = 0.03330 -0.02701 0.00361 -0.00685 F9 3 0.759077 0.138672 0.619904 11.00000 0.02130 0.04076 = 0.05507 -0.03037 0.00725 -0.01590 F10 3 0.803840 0.303553 0.476847 11.00000 0.01835 0.06380 = 0.01965 -0.01549 -0.00683 -0.00715 F11 3 0.913155 0.069158 0.686919 11.00000 0.04350 0.01855 = 0.03045 -0.00671 0.00326 -0.00689 F12 3 1.121874 0.164935 0.587873 11.00000 0.01488 0.02938 = 0.02009 -0.00981 -0.00100 0.00195 F13 3 1.065859 0.321239 0.595954 11.00000 0.02100 0.02794 = 0.03278 -0.00840 -0.00755 -0.01016 F14 3 1.016922 0.202990 0.717440 11.00000 0.02216 0.03807 = 0.01433 -0.00798 -0.00690 0.00212 F15 3 0.841494 0.505093 0.661608 11.00000 0.03057 0.02246 = 0.01337 -0.00465 -0.00517 -0.00483 F16 3 0.667858 0.567120 0.749576 11.00000 0.01802 0.01726 = 0.02472 -0.00114 -0.00935 -0.00111 F17 3 0.841942 0.613001 0.732452 11.00000 0.02853 0.01626 = 0.02164 -0.00062 -0.00627 -0.01168 F18 3 1.040001 0.436606 0.741697 11.00000 0.01468 0.03648 = 0.02405 -0.01055 0.00050 -0.00644 F19 3 0.977661 0.502088 0.859517 11.00000 0.02207 0.02889 = 0.03510 -0.01541 -0.01028 -0.00816 F20 3 1.003156 0.340556 0.879596 11.00000 0.02071 0.02405 = 0.02787 -0.00631 -0.01364 0.00124 F21 3 0.714010 0.567248 0.914610 11.00000 0.02698 0.01407 = 0.02080 -0.00812 -0.00272 -0.00324 F22 3 0.775762 0.412811 0.988863 11.00000 0.02909 0.02030 = 0.01380 -0.00409 -0.00678 -0.00217 F23 3 0.616960 0.450709 0.928160 11.00000 0.01575 0.02551 = 0.02120 -0.00794 0.00146 -0.00764 F24 3 0.942164 0.135269 0.914688 11.00000 0.01777 0.02424 = 0.02467 -0.00392 -0.00619 -0.00552 F25 3 0.788378 0.209415 1.008874 11.00000 0.03073 0.01988 = 0.02194 -0.00896 -0.00979 -0.00505 F26 3 0.855429 0.047278 1.047808 11.00000 0.03374 0.02140 = 0.02134 0.00315 -0.01570 -0.00485 F27 3 0.556170 0.235848 0.982827 11.00000 0.02208 0.01644 = 0.02046 -0.00674 -0.00189 0.00034 F28 3 0.593295 0.095047 1.084975 11.00000 0.03171 0.02799 = 0.01313 -0.00010 0.00181 -0.00468 F29 3 0.516395 0.100799 0.973147 11.00000 0.01982 0.02556 = 0.03261 -0.00679 -0.00195 -0.01097 F30 3 0.735117 -0.065281 1.006981 11.00000 0.03597 0.01393 = 0.02384 0.00248 -0.00764 -0.00797 F31 3 0.891769 -0.029371 0.889430 11.00000 0.02291 0.01767 = 0.03059 -0.00977 -0.00453 0.00222 F32 3 0.705964 -0.010227 0.869138 11.00000 0.03248 0.01717 = 0.02685 -0.00796 -0.01167 -0.00583 F33 3 0.371176 0.450923 0.884225 11.00000 0.02535 0.04561 = 0.02844 -0.02511 -0.00382 0.00423 F34 3 0.411988 0.562824 0.756034 11.00000 0.02953 0.01802 = 0.05900 -0.01240 -0.01942 0.00147 F35 3 0.256600 0.488019 0.787046 11.00000 0.01262 0.03928 = 0.05090 -0.02513 -0.01113 0.00577 F36 3 0.584531 0.490909 0.613754 11.00000 0.03317 0.05197 = 0.02449 0.00916 -0.00778 -0.01756 F37 3 0.396358 0.486587 0.612229 11.00000 0.02973 0.05334 = 0.02906 -0.00263 -0.01965 0.00300 F38 3 0.549794 0.356222 0.598996 11.00000 0.02852 0.06488 = 0.02389 -0.02541 -0.00731 0.00231 F39 3 0.320258 0.310667 0.730333 11.00000 0.02577 0.03816 = 0.05301 -0.02223 -0.01792 -0.00557 F40 3 0.496437 0.214339 0.759172 11.00000 0.03205 0.02218 = 0.05867 -0.02041 -0.01602 0.00190 F2 3 -0.089996 0.149884 0.341814 11.00000 0.02296 0.03638 = 0.01768 -0.00165 0.00142 -0.00860 C1 1 0.545501 0.249901 0.200332 11.00000 0.01235 0.01604 = 0.01519 -0.00573 -0.00295 -0.00233 C2 1 0.461996 0.054789 0.284662 11.00000 0.01646 0.01694 = 0.01108 -0.00056 -0.00347 -0.00234 O1 2 0.550980 0.310262 0.134223 11.00000 0.02228 0.01698 = 0.01476 -0.00097 -0.00344 -0.00450 O2 2 0.424772 0.001075 0.265347 11.00000 0.02693 0.02126 = 0.01935 -0.00375 -0.00828 -0.00923 F3 3 0.163010 0.132252 0.326209 11.00000 0.02627 0.03234 = 0.01952 -0.00327 -0.01339 -0.00114 F4 3 0.312924 0.212585 0.163810 11.00000 0.01387 0.02387 = 0.03506 -0.00468 -0.00886 -0.00397 F5 3 0.351798 0.274062 0.866595 11.00000 0.03128 0.03564 = 0.03395 -0.00188 -0.00104 -0.01687 O3 2 0.267415 0.255826 0.412344 11.00000 0.01614 0.02588 = 0.01951 0.00072 -0.00101 0.00122 O4 2 0.635228 0.263565 0.408876 11.00000 0.02940 0.02725 = 0.02944 -0.00883 -0.01243 -0.00937 O5 2 0.804507 0.018218 0.258039 11.00000 0.02080 0.02729 = 0.02428 -0.00529 -0.00265 0.00356 O6 2 0.391999 0.174483 0.599209 11.00000 0.03129 0.02266 = 0.02563 -0.01292 -0.00893 0.00025 O7 2 0.228481 -0.004412 0.498908 11.00000 0.01662 0.02445 = 0.02139 -0.00594 -0.00581 -0.00456 O8 2 0.808321 0.355398 0.816384 11.00000 0.01638 0.01201 = 0.01731 -0.00500 -0.00660 -0.00236 O9 2 0.576493 0.364476 0.780464 11.00000 0.01155 0.02030 = 0.01548 -0.00642 -0.00495 0.00088 O10 2 0.799878 0.290001 0.663170 11.00000 0.01404 0.01788 = 0.01166 -0.00615 -0.00073 -0.00087 O11 2 0.740636 0.172270 0.845130 11.00000 0.01756 0.01297 = 0.01164 -0.00202 -0.00295 -0.00372 C3 1 0.361995 0.214112 0.377786 11.00000 0.01685 0.01675 = 0.01216 0.00227 -0.00579 -0.00494 C22 1 0.832342 0.125744 0.976158 11.00000 0.02244 0.01447 = 0.01592 -0.00135 -0.00767 -0.00291 C23 1 0.767120 -0.000442 0.924852 11.00000 0.02202 0.01279 = 0.01888 -0.00304 -0.00552 -0.00267 C24 1 0.408043 0.296157 0.776273 11.00000 0.02012 0.02388 = 0.03222 -0.01240 -0.00791 -0.00305 C25 1 0.500433 0.431463 0.641533 11.00000 0.02094 0.03844 = 0.01859 -0.00503 -0.00888 -0.00147 C26 1 0.374891 0.473552 0.795143 11.00000 0.01407 0.02203 = 0.03017 -0.01238 -0.00742 0.00196 C27 1 0.880879 0.136309 0.612138 11.00000 0.02086 0.02547 = 0.02657 -0.01532 0.00393 -0.00784 C28 1 0.899769 0.311252 0.504763 11.00000 0.01438 0.03472 = 0.01258 -0.00687 -0.00174 -0.00460 C29 1 1.027436 0.233496 0.626781 11.00000 0.01620 0.02261 = 0.01450 -0.00628 -0.00286 -0.00211 C4 1 0.601087 0.219923 0.376075 11.00000 0.01495 0.01780 = 0.01599 -0.00176 -0.00401 -0.00242 C5 1 0.706578 0.063747 0.281316 11.00000 0.01935 0.01716 = 0.01333 -0.00108 -0.00490 -0.00355 C6 1 0.430836 0.110863 0.563183 11.00000 0.01663 0.01776 = 0.01370 -0.00126 -0.00613 -0.00300 C7 1 0.327338 -0.002148 0.499017 11.00000 0.01857 0.01291 = 0.01029 -0.00215 -0.00373 -0.00215 C8 1 0.140097 0.272344 0.092587 11.00000 0.02068 0.01734 = 0.01825 -0.00233 -0.00393 -0.00601 AFIX 43 H1 6 0.193874 0.299541 0.035067 11.00000 -1.20000 AFIX 0 C9 1 0.011124 0.282173 0.101020 11.00000 0.02212 0.01989 = 0.02002 -0.00181 -0.01040 -0.00432 AFIX 43 H2 6 -0.024591 0.316524 0.049330 11.00000 -1.20000 AFIX 0 C10 1 -0.063750 0.241696 0.184802 11.00000 0.01456 0.02082 = 0.02392 -0.00625 -0.00749 -0.00401 C11 1 -0.014873 0.190549 0.261177 11.00000 0.01795 0.01985 = 0.01520 -0.00516 -0.00124 -0.00432 C12 1 0.112771 0.181289 0.253057 11.00000 0.01930 0.01666 = 0.01814 -0.00594 -0.00914 0.00019 C13 1 0.188292 0.222661 0.168831 11.00000 0.01359 0.01559 = 0.02407 -0.00753 -0.00569 -0.00210 C14 1 0.734717 0.111914 0.931750 11.00000 0.01721 0.01095 = 0.01309 -0.00288 -0.00319 -0.00294 C15 1 0.898373 0.244028 0.604910 11.00000 0.01258 0.01944 = 0.01271 -0.00644 -0.00085 -0.00430 C16 1 0.470346 0.389508 0.748843 11.00000 0.01187 0.01831 = 0.01610 -0.00684 -0.00414 0.00035 C17 1 0.822222 0.443671 0.824083 11.00000 0.01353 0.01197 = 0.01318 -0.00319 -0.00406 -0.00265 C18 1 0.963382 0.430709 0.826208 11.00000 0.01673 0.02010 = 0.01961 -0.00732 -0.00582 -0.00407 C19 1 0.794098 0.533289 0.740476 11.00000 0.01773 0.01511 = 0.01554 -0.00322 -0.00462 -0.00457 C20 1 0.730578 0.469419 0.915294 11.00000 0.01716 0.01371 = 0.01474 -0.00386 -0.00394 -0.00343 C21 1 0.598231 0.135807 0.993973 11.00000 0.02002 0.01590 = 0.01494 -0.00215 -0.00098 -0.00451 REM ##### HKLF 4 REM p-1_a.res in P-1 REM wR2 = 0.0463, GooF = S = 1.017, Restrained GooF = 1.017 for all data REM R1 = 0.0192 for 10225 Fo > 4sig(Fo) and 0.0217 for all 11068 data REM 745 parameters refined using 0 restraints END WGHT 0.0183 1.5293 REM Instructions for potential hydrogen bonds EQIV $2 x-1, y, z-1 HTAB C9 F20_$2 HTAB C9 F22_$2 REM Highest difference peak 0.491, deepest hole -0.550, 1-sigma level 0.055 Q1 1 0.7454 0.0575 0.9330 11.00000 0.05 0.49 Q2 1 0.7762 0.4587 0.8674 11.00000 0.05 0.46 Q3 1 0.8964 0.1926 0.6016 11.00000 0.05 0.44 Q4 1 0.4173 0.4283 0.7689 11.00000 0.05 0.44 Q5 1 0.7758 0.1170 0.9558 11.00000 0.05 0.44 Q6 1 0.4336 0.3435 0.7650 11.00000 0.05 0.43 Q7 1 0.9602 0.2404 0.6125 11.00000 0.05 0.42 Q8 1 0.8018 0.4895 0.7877 11.00000 0.05 0.42 Q9 1 0.8886 0.4400 0.8329 11.00000 0.05 0.40 Q10 1 0.9030 0.2744 0.5572 11.00000 0.05 0.39 Q11 1 0.4812 0.4094 0.6990 11.00000 0.05 0.38 Q12 1 -0.0368 0.2202 0.2239 11.00000 0.05 0.35 Q13 1 0.6717 0.1199 0.9614 11.00000 0.05 0.35 Q14 1 0.0475 0.1965 0.2623 11.00000 0.05 0.34 Q15 1 0.1632 0.2405 0.1301 11.00000 0.05 0.33 Q16 1 0.1501 0.2049 0.2113 11.00000 0.05 0.32 Q17 1 0.0789 0.2738 0.1011 11.00000 0.05 0.30 Q18 1 -0.0240 0.2679 0.1484 11.00000 0.05 0.30 Q19 1 0.4021 0.4325 0.6085 11.00000 0.05 0.27 Q20 1 0.6032 0.1701 0.3635 11.00000 0.05 0.27 ; _shelx_res_checksum 89335 _shelx_hkl_file ; -1 0 0 819.82 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0 443.86 22.30 7 -2 0 468.15 19.70 7 -2 0 460.35 21.70 7 -2 0 480.55 16.90 7 -2 0 473.75 17.20 7 -2 0 479.65 21.10 7 -2 0 491.45 15.80 -7 2 0 475.05 18.70 -7 2 0 480.95 20.60 -7 2 0 504.85 22.30 -7 2 0 415.66 20.00 -7 2 0 472.45 21.60 -7 2 0 472.45 17.70 -7 2 0 498.55 18.50 -7 2 0 477.65 20.20 6 -2 0 1.60 1.50 6 -2 0 -0.50 0.70 6 -2 0 -0.60 2.10 6 -2 0 -0.70 2.30 6 -2 0 0.60 1.30 6 -2 0 1.60 1.20 6 -2 0 1.00 2.10 6 -2 0 0.30 2.10 6 -2 0 3.20 2.80 6 -2 0 1.90 1.40 -6 2 0 0.70 1.20 -6 2 0 1.60 2.30 -6 2 0 4.50 2.90 -6 2 0 1.80 1.50 -6 2 0 1.20 1.20 -6 2 0 0.80 2.70 -6 2 0 -1.00 0.60 -6 2 0 0.80 2.30 5 -2 0 770.52 23.70 5 -2 0 761.22 24.80 5 -2 0 744.03 22.00 5 -2 0 711.03 23.20 5 -2 0 711.03 24.10 5 -2 0 766.62 24.90 5 -2 0 739.03 23.50 5 -2 0 733.63 25.40 5 -2 0 715.93 25.90 5 -2 0 758.62 22.50 -5 2 0 708.33 24.00 -5 2 0 763.72 22.30 -5 2 0 734.13 21.80 -5 2 0 711.73 25.00 -5 2 0 765.92 24.80 -5 2 0 776.32 25.80 4 -2 0 428.26 15.10 4 -2 0 398.86 16.30 4 -2 0 435.56 13.30 4 -2 0 418.56 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1100.59 28.00 1 -2 0 1219.78 28.00 1 -2 0 1248.38 27.10 1 -2 0 1209.78 28.00 -1 2 0 1149.58 27.80 -1 2 0 1224.78 27.10 -1 2 0 1197.98 27.80 -1 2 0 1177.48 29.20 -1 2 0 1206.68 27.90 0 -2 0 0.90 0.50 0 -2 0 1.00 0.50 0 -2 0 0.10 0.50 0 -2 0 1.40 0.70 0 -2 0 1.70 0.70 0 -2 0 0.70 0.40 0 -2 0 1.00 0.60 0 -2 0 1.50 0.90 0 -2 0 1.30 0.50 0 -2 0 0.70 0.60 0 -2 0 1.70 0.60 0 -2 0 1.50 0.50 0 -2 0 1.70 0.50 0 -2 0 0.30 0.30 0 -2 0 1.60 0.70 0 -2 0 0.60 0.50 0 2 0 1.40 0.50 0 2 0 1.10 0.50 0 2 0 1.00 0.50 0 2 0 0.80 0.60 0 2 0 0.60 0.40 0 2 0 0.30 0.40 0 2 0 0.70 0.40 0 2 0 1.00 0.80 0 2 0 0.80 0.60 0 2 0 1.10 0.70 0 2 0 0.50 0.60 0 2 0 0.50 0.30 0 2 0 0.80 0.50 0 2 0 1.40 0.60 -1 -2 0 106.69 3.80 -1 -2 0 96.49 4.10 -1 -2 0 99.89 4.10 -1 -2 0 104.79 4.30 -1 -2 0 103.09 4.00 -1 -2 0 105.69 4.20 -1 -2 0 92.39 4.20 -1 -2 0 104.59 4.50 -1 -2 0 108.09 4.40 -1 -2 0 106.79 3.70 -1 -2 0 101.49 3.90 -1 -2 0 102.99 3.80 1 2 0 109.79 4.60 1 2 0 102.99 4.10 1 2 0 99.19 4.20 1 2 0 106.99 3.10 1 2 0 97.69 3.60 1 2 0 103.59 4.00 1 2 0 101.69 4.40 1 2 0 101.59 4.60 1 2 0 100.89 4.10 1 2 0 102.99 4.10 1 2 0 105.49 4.30 1 2 0 101.79 3.30 -2 -2 0 245.18 7.50 -2 -2 0 280.77 9.80 -2 -2 0 262.17 8.10 -2 -2 0 277.67 8.70 -2 -2 0 281.87 7.40 2 2 0 275.57 9.80 2 2 0 292.07 9.30 2 2 0 263.87 8.70 2 2 0 286.07 9.30 2 2 0 269.97 8.30 2 2 0 269.97 9.30 2 2 0 278.17 7.80 2 2 0 275.67 10.00 -3 -2 0 50.99 3.60 -3 -2 0 46.20 3.10 -3 -2 0 48.90 4.40 -3 -2 0 44.00 3.00 -3 -2 0 47.90 3.80 -3 -2 0 46.70 3.20 -3 -2 0 44.20 2.70 3 2 0 47.60 3.70 3 2 0 44.70 3.10 3 2 0 48.20 2.90 3 2 0 45.20 3.10 3 2 0 43.20 4.00 3 2 0 52.09 4.00 3 2 0 46.10 4.50 3 2 0 49.00 3.90 3 2 0 47.60 3.10 -4 -2 0 182.08 7.00 -4 -2 0 189.78 7.90 -4 -2 0 166.08 8.80 -4 -2 0 180.38 8.80 -4 -2 0 183.88 7.60 -4 -2 0 197.98 6.60 4 2 0 187.88 7.80 4 2 0 183.08 7.10 4 2 0 178.28 9.40 4 2 0 196.68 8.90 4 2 0 163.98 9.20 4 2 0 197.48 7.90 4 2 0 167.78 8.80 4 2 0 187.38 6.60 -5 -2 0 213.68 10.50 -5 -2 0 197.98 9.00 -5 -2 0 231.18 11.10 -5 -2 0 206.58 7.80 -5 -2 0 217.18 9.10 -5 -2 0 210.98 7.30 5 2 0 206.08 9.30 5 2 0 184.98 10.90 5 2 0 206.28 7.80 5 2 0 215.28 11.40 5 2 0 213.88 7.30 5 2 0 205.28 10.30 5 2 0 207.08 10.50 5 2 0 206.38 8.90 -6 -2 0 196.48 7.00 -6 -2 0 191.08 7.60 -6 -2 0 172.88 10.20 -6 -2 0 189.58 10.20 -6 -2 0 192.78 12.10 -6 -2 0 174.88 8.90 -6 -2 0 190.78 11.00 -6 -2 0 197.38 9.60 6 2 0 204.88 10.00 6 2 0 192.88 10.70 6 2 0 190.68 9.00 6 2 0 191.68 11.90 6 2 0 201.28 7.00 6 2 0 176.58 7.30 6 2 0 193.68 11.10 6 2 0 174.18 11.20 -7 -2 0 258.07 15.30 -7 -2 0 244.38 9.00 -7 -2 0 234.08 8.20 -7 -2 0 253.97 11.80 -7 -2 0 231.18 13.30 -7 -2 0 234.08 13.60 -7 -2 0 263.77 13.00 -7 -2 0 240.68 11.30 7 2 0 253.07 13.40 7 2 0 247.48 8.20 7 2 0 233.08 12.90 7 2 0 231.08 14.10 7 2 0 252.37 12.30 7 2 0 240.28 13.80 7 2 0 235.88 11.00 7 2 0 260.37 15.00 7 2 0 245.38 8.90 7 2 0 254.47 11.20 -8 -2 0 7.30 3.50 -8 -2 0 -0.10 1.00 -8 -2 0 0.70 0.80 -8 -2 0 3.70 3.40 -8 -2 0 5.70 3.70 -8 -2 0 0.80 1.30 -8 -2 0 1.90 1.50 -8 -2 0 0.60 1.50 8 2 0 -0.70 3.10 8 2 0 0.40 1.30 8 2 0 -2.00 3.20 8 2 0 2.20 0.90 8 2 0 0.80 1.50 8 2 0 0.30 3.00 8 2 0 2.60 2.50 8 2 0 1.30 2.00 8 2 0 0.50 1.20 8 2 0 0.80 1.30 -9 -2 0 -0.50 0.80 -9 -2 0 -0.90 1.00 -9 -2 0 -2.60 2.90 -9 -2 0 -0.90 0.70 -9 -2 0 2.30 4.70 -9 -2 0 -2.00 3.70 9 2 0 -6.60 3.60 9 2 0 0.70 2.10 9 2 0 1.70 3.90 9 2 0 1.20 1.20 9 2 0 3.90 3.80 9 2 0 0.40 1.10 -10 -2 0 83.09 10.70 -10 -2 0 71.99 8.40 -10 -2 0 101.19 14.20 -10 -2 0 75.99 8.90 -10 -2 0 101.79 12.10 -10 -2 0 77.09 11.50 10 2 0 89.39 8.80 10 2 0 104.29 12.20 10 2 0 71.59 8.10 10 2 0 86.29 15.60 10 2 0 108.59 14.60 10 2 0 72.89 11.50 10 2 0 80.99 12.50 -11 -2 0 194.88 13.70 -11 -2 0 192.18 17.40 -11 -2 0 197.98 16.40 -11 -2 0 198.18 12.80 -11 -2 0 191.78 17.20 -11 -2 0 196.68 12.60 11 2 0 166.58 11.10 11 2 0 193.58 16.30 11 2 0 168.48 13.20 11 2 0 192.38 15.50 11 2 0 190.38 14.70 11 2 0 198.48 11.70 11 2 0 190.58 16.20 11 2 0 156.28 15.40 -12 -2 0 70.29 12.70 -12 -2 0 83.09 10.10 -12 -2 0 47.30 11.50 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28.60 -13 3 0 224.18 16.00 -13 3 0 215.78 14.70 -13 3 0 188.98 22.10 -13 3 0 212.48 18.00 12 -3 0 250.07 21.20 12 -3 0 265.37 15.60 12 -3 0 290.87 20.70 12 -3 0 280.77 19.10 12 -3 0 293.37 21.50 12 -3 0 241.88 13.80 12 -3 0 207.68 14.50 12 -3 0 247.98 12.10 12 -3 0 256.87 18.80 12 -3 0 256.07 22.30 -12 3 0 255.37 15.50 -12 3 0 251.27 21.00 -12 3 0 264.47 22.20 -12 3 0 236.48 16.00 -12 3 0 235.18 24.20 -12 3 0 248.78 18.70 -12 3 0 239.38 16.40 -12 3 0 277.37 22.20 11 -3 0 100.89 11.60 11 -3 0 88.09 13.90 11 -3 0 75.89 8.60 11 -3 0 76.99 9.50 11 -3 0 91.19 14.10 11 -3 0 89.79 7.00 11 -3 0 84.69 13.50 11 -3 0 70.29 11.50 11 -3 0 102.59 12.30 11 -3 0 64.19 12.00 -11 3 0 102.79 16.80 -11 3 0 81.79 12.80 -11 3 0 86.49 10.70 -11 3 0 95.79 14.10 -11 3 0 68.39 12.10 -11 3 0 77.29 9.40 -11 3 0 74.29 10.00 -11 3 0 80.79 14.30 10 -3 0 72.69 9.50 10 -3 0 69.99 10.40 10 -3 0 40.40 7.00 10 -3 0 62.39 10.50 10 -3 0 49.40 8.80 10 -3 0 78.59 9.30 10 -3 0 65.19 5.90 10 -3 0 52.39 9.00 10 -3 0 57.69 10.30 10 -3 0 69.69 8.00 -10 3 0 62.19 8.60 -10 3 0 90.09 13.30 -10 3 0 74.19 11.30 -10 3 0 76.99 9.30 -10 3 0 52.39 7.50 -10 3 0 58.09 10.10 -10 3 0 49.30 9.40 9 -3 0 -0.60 3.10 9 -3 0 4.20 2.10 9 -3 0 2.50 2.30 9 -3 0 7.00 4.30 9 -3 0 2.50 1.70 9 -3 0 3.80 3.10 9 -3 0 6.20 4.90 9 -3 0 5.90 3.90 -9 3 0 4.70 2.30 -9 3 0 0.00 5.10 -9 3 0 4.60 5.90 -9 3 0 4.70 3.30 -9 3 0 1.60 3.40 -9 3 0 4.40 2.20 -9 3 0 4.50 2.70 -9 3 0 0.20 4.80 8 -3 0 39.90 6.80 8 -3 0 55.49 8.40 8 -3 0 49.30 8.80 8 -3 0 45.00 4.60 8 -3 0 43.30 9.60 8 -3 0 52.69 9.20 8 -3 0 35.70 7.10 8 -3 0 48.20 7.60 8 -3 0 50.39 7.70 8 -3 0 42.90 5.60 -8 3 0 46.00 8.10 -8 3 0 39.50 7.40 -8 3 0 35.90 5.80 -8 3 0 46.20 7.80 -8 3 0 29.10 5.20 -8 3 0 37.90 6.70 -8 3 0 38.70 5.80 -8 3 0 44.20 8.40 7 -3 0 8.40 2.70 7 -3 0 17.30 4.30 7 -3 0 17.30 4.10 7 -3 0 14.40 3.20 7 -3 0 14.00 3.20 7 -3 0 16.00 4.90 7 -3 0 17.50 5.40 7 -3 0 18.20 4.40 7 -3 0 10.30 4.80 7 -3 0 15.80 4.80 7 -3 0 20.50 5.00 7 -3 0 19.40 5.70 -7 3 0 18.40 3.90 -7 3 0 12.50 3.00 -7 3 0 19.20 5.10 -7 3 0 11.50 2.80 -7 3 0 12.60 4.40 -7 3 0 14.80 5.20 -7 3 0 12.90 3.80 -7 3 0 13.20 3.90 6 -3 0 111.49 10.30 6 -3 0 77.49 6.60 6 -3 0 69.39 8.50 6 -3 0 71.99 5.40 6 -3 0 82.99 12.30 6 -3 0 76.19 5.60 6 -3 0 70.29 6.50 6 -3 0 71.99 7.10 6 -3 0 76.89 6.20 6 -3 0 84.79 9.10 6 -3 0 68.89 7.40 6 -3 0 71.09 6.90 -6 3 0 80.69 8.00 -6 3 0 68.89 8.80 -6 3 0 67.89 5.60 -6 3 0 81.79 8.10 -6 3 0 66.49 6.00 -6 3 0 75.09 6.20 -6 3 0 77.89 7.00 -6 3 0 75.79 7.50 5 -3 0 172.68 10.30 5 -3 0 186.08 10.20 5 -3 0 189.78 12.20 5 -3 0 167.78 9.70 5 -3 0 187.88 9.40 5 -3 0 180.88 9.70 5 -3 0 179.58 10.90 5 -3 0 170.88 8.40 5 -3 0 183.88 10.50 5 -3 0 170.68 11.20 5 -3 0 203.38 8.90 5 -3 0 181.28 9.90 -5 3 0 202.48 10.60 -5 3 0 180.78 9.30 -5 3 0 174.88 10.60 -5 3 0 169.98 8.60 -5 3 0 196.78 10.80 -5 3 0 165.48 10.70 -5 3 0 190.78 11.30 -5 3 0 183.78 9.20 4 -3 0 28.50 4.20 4 -3 0 28.00 3.60 4 -3 0 29.50 3.50 4 -3 0 28.70 4.60 4 -3 0 19.40 3.80 4 -3 0 25.40 4.00 4 -3 0 27.80 1.90 4 -3 0 36.00 4.50 4 -3 0 29.20 4.80 4 -3 0 30.30 2.40 4 -3 0 22.50 4.20 4 -3 0 23.60 4.30 4 -3 0 20.40 3.30 4 -3 0 28.60 4.50 -4 3 0 27.20 3.80 -4 3 0 30.00 4.70 -4 3 0 31.00 2.50 -4 3 0 29.40 4.40 -4 3 0 21.50 3.10 -4 3 0 24.50 3.80 -4 3 0 30.50 2.10 -4 3 0 23.60 3.30 -4 3 0 25.10 4.20 -4 3 0 28.20 4.80 3 -3 0 505.05 17.50 3 -3 0 519.95 16.90 3 -3 0 513.15 17.30 3 -3 0 501.95 13.70 3 -3 0 545.35 18.90 3 -3 0 530.05 15.70 3 -3 0 487.95 17.90 -3 3 0 503.15 13.90 -3 3 0 501.55 17.40 -3 3 0 530.15 17.30 -3 3 0 487.65 16.60 -3 3 0 472.15 16.80 -3 3 0 510.35 16.20 2 -3 0 349.17 10.50 2 -3 0 326.67 11.70 2 -3 0 361.06 11.50 2 -3 0 357.36 11.50 2 -3 0 312.57 11.90 2 -3 0 345.27 12.30 2 -3 0 345.37 10.90 2 -3 0 368.66 12.70 -2 3 0 333.67 10.50 -2 3 0 334.27 10.70 -2 3 0 333.57 11.90 -2 3 0 336.47 12.00 -2 3 0 348.77 12.20 -2 3 0 347.67 10.70 -2 3 0 359.36 11.50 1 -3 0 0.30 0.60 1 -3 0 3.70 1.00 1 -3 0 0.10 0.70 1 -3 0 0.00 0.90 1 -3 0 1.00 0.90 1 -3 0 3.50 1.30 1 -3 0 0.90 0.60 1 -3 0 4.80 2.00 1 -3 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207.68 26.00 14 3 0 205.68 19.80 14 3 0 190.08 18.60 14 3 0 189.08 20.30 14 3 0 194.98 12.80 14 3 0 212.58 17.00 14 3 0 252.27 21.70 13 -4 0 29.50 10.00 13 -4 0 21.00 8.50 -13 4 0 23.30 8.10 -13 4 0 34.60 6.90 -13 4 0 37.20 11.30 12 -4 0 1.60 1.40 12 -4 0 0.50 2.60 12 -4 0 0.20 7.20 12 -4 0 1.90 1.70 12 -4 0 5.60 4.10 12 -4 0 2.20 5.90 12 -4 0 3.70 6.90 12 -4 0 -7.60 10.00 12 -4 0 0.00 0.70 12 -4 0 -0.20 5.80 -12 4 0 3.70 2.40 -12 4 0 2.90 5.10 -12 4 0 4.50 10.20 -12 4 0 -3.40 13.30 -12 4 0 6.00 3.40 -12 4 0 1.20 8.20 -12 4 0 1.40 2.60 -12 4 0 4.20 2.80 11 -4 0 47.80 10.00 11 -4 0 42.90 6.90 11 -4 0 45.70 6.70 11 -4 0 43.70 11.30 11 -4 0 57.39 11.10 11 -4 0 25.70 7.90 11 -4 0 51.29 9.60 11 -4 0 44.30 7.50 11 -4 0 56.59 13.20 11 -4 0 51.69 10.60 -11 4 0 42.00 7.60 -11 4 0 41.20 9.80 -11 4 0 17.40 10.90 -11 4 0 38.40 8.80 -11 4 0 50.29 11.60 -11 4 0 39.20 10.30 -11 4 0 42.20 7.70 -11 4 0 36.80 6.50 10 -4 0 154.58 15.50 10 -4 0 154.38 10.00 10 -4 0 146.99 10.00 10 -4 0 182.08 15.20 10 -4 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41.00 7.00 7 -4 0 47.50 7.30 7 -4 0 38.20 6.80 7 -4 0 60.09 8.20 -7 4 0 33.70 5.30 -7 4 0 55.29 8.60 -7 4 0 47.60 6.00 -7 4 0 50.99 7.80 -7 4 0 31.50 5.00 -7 4 0 45.30 8.80 -7 4 0 31.60 5.80 -7 4 0 45.90 7.60 6 -4 0 11.20 2.70 6 -4 0 10.30 3.80 6 -4 0 9.90 2.80 6 -4 0 10.40 3.00 6 -4 0 13.60 4.00 6 -4 0 18.10 4.50 6 -4 0 10.60 4.40 6 -4 0 13.00 3.30 6 -4 0 14.10 4.40 6 -4 0 22.70 5.30 6 -4 0 8.70 3.70 6 -4 0 25.20 5.50 -6 4 0 10.50 3.20 -6 4 0 13.20 4.30 -6 4 0 10.90 3.40 -6 4 0 11.00 3.00 -6 4 0 11.50 4.20 -6 4 0 8.40 2.60 -6 4 0 14.10 4.40 -6 4 0 12.70 3.00 5 -4 0 647.24 20.00 5 -4 0 625.54 25.10 5 -4 0 661.43 22.60 5 -4 0 663.03 20.90 5 -4 0 655.33 21.30 5 -4 0 646.64 22.30 5 -4 0 649.83 22.40 5 -4 0 669.53 17.30 5 -4 0 647.64 23.90 5 -4 0 659.83 24.60 5 -4 0 660.43 22.80 -5 4 0 674.43 21.40 -5 4 0 654.93 21.20 -5 4 0 662.13 24.10 -5 4 0 651.43 23.80 -5 4 0 635.14 20.20 -5 4 0 689.23 24.40 -5 4 0 647.14 22.90 -5 4 0 603.24 21.90 -5 4 0 624.14 17.40 4 -4 0 2.60 1.30 4 -4 0 7.00 2.50 4 -4 0 5.00 2.60 4 -4 0 4.60 1.50 4 -4 0 3.80 1.40 4 -4 0 2.50 2.20 4 -4 0 5.10 2.00 4 -4 0 4.40 2.20 4 -4 0 1.30 2.60 4 -4 0 2.40 1.50 4 -4 0 3.80 1.70 4 -4 0 3.90 1.10 -4 4 0 3.20 2.50 -4 4 0 2.80 1.40 -4 4 0 2.30 2.20 -4 4 0 4.30 1.70 -4 4 0 3.80 1.20 -4 4 0 2.10 2.20 -4 4 0 5.30 1.70 -4 4 0 3.50 2.30 -4 4 0 3.30 1.90 -4 4 0 3.40 1.50 3 -4 0 605.94 17.40 3 -4 0 586.84 18.50 3 -4 0 626.14 20.30 3 -4 0 582.04 19.90 3 -4 0 606.94 18.20 3 -4 0 598.84 20.30 3 -4 0 616.94 17.10 3 -4 0 624.34 19.50 -3 4 0 588.04 20.00 -3 4 0 591.44 19.40 -3 4 0 587.24 17.50 -3 4 0 591.44 17.20 -3 4 0 587.44 19.70 -3 4 0 597.54 18.80 -3 4 0 623.74 20.30 -3 4 0 600.24 18.00 2 -4 0 842.32 24.00 2 -4 0 824.22 24.60 2 -4 0 784.12 24.50 2 -4 0 835.12 23.50 2 -4 0 826.02 24.10 2 -4 0 863.61 22.40 -2 4 0 844.62 24.10 -2 4 0 863.81 23.90 -2 4 0 814.12 23.60 -2 4 0 878.61 22.70 1 -4 0 322.47 10.30 1 -4 0 288.47 11.70 1 -4 0 299.57 10.90 1 -4 0 298.37 10.00 1 -4 0 293.27 10.70 1 -4 0 318.77 12.20 1 -4 0 294.57 10.70 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100.49 5.90 4 4 0 86.89 5.20 4 4 0 79.29 6.40 4 4 0 87.09 6.30 4 4 0 98.49 6.20 4 4 0 79.99 6.90 4 4 0 81.69 5.10 4 4 0 78.79 7.00 -5 -4 0 4.80 1.00 -5 -4 0 5.80 1.90 -5 -4 0 4.80 1.90 -5 -4 0 0.80 2.20 -5 -4 0 5.50 2.60 -5 -4 0 4.70 1.70 -5 -4 0 6.70 2.90 -5 -4 0 8.60 1.70 -5 -4 0 3.80 2.00 5 4 0 6.70 2.40 5 4 0 3.10 2.80 5 4 0 5.70 1.90 5 4 0 2.70 2.00 5 4 0 5.10 2.60 5 4 0 6.50 1.90 5 4 0 2.00 2.60 5 4 0 3.10 2.00 5 4 0 4.40 2.10 5 4 0 5.30 1.80 -6 -4 0 205.58 11.40 -6 -4 0 203.38 9.70 -6 -4 0 189.48 9.80 -6 -4 0 209.28 12.00 -6 -4 0 193.38 12.40 -6 -4 0 199.98 9.50 -6 -4 0 206.48 8.80 -6 -4 0 199.08 10.50 6 4 0 201.38 9.70 6 4 0 203.58 11.70 6 4 0 199.48 12.40 6 4 0 194.08 9.50 6 4 0 212.48 13.30 6 4 0 197.28 12.30 6 4 0 213.88 11.20 6 4 0 208.48 11.90 6 4 0 212.78 9.80 6 4 0 207.28 8.80 -7 -4 0 1.50 1.20 -7 -4 0 0.00 0.80 -7 -4 0 4.00 3.70 -7 -4 0 4.40 2.60 -7 -4 0 0.80 1.70 -7 -4 0 1.00 2.90 -7 -4 0 0.50 1.50 -7 -4 0 -0.20 1.10 7 4 0 -0.10 0.70 7 4 0 2.70 2.40 7 4 0 -0.10 3.30 7 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0 237.68 19.10 -10 -4 0 225.28 13.50 -10 -4 0 242.68 10.70 -10 -4 0 248.18 18.80 10 4 0 248.48 12.80 10 4 0 240.58 15.60 10 4 0 253.57 14.60 10 4 0 267.47 17.30 10 4 0 259.77 18.60 10 4 0 235.48 17.60 10 4 0 242.18 11.10 10 4 0 246.08 10.00 10 4 0 230.98 16.00 10 4 0 231.68 14.10 -11 -4 0 12.90 3.90 -11 -4 0 20.10 7.60 -11 -4 0 21.30 8.80 -11 -4 0 19.10 4.70 -11 -4 0 18.70 3.00 -11 -4 0 14.20 6.30 -11 -4 0 16.70 4.90 -11 -4 0 23.60 6.10 -11 -4 0 21.30 9.30 -11 -4 0 19.40 4.20 11 4 0 17.50 3.00 11 4 0 15.40 6.80 11 4 0 15.70 6.90 11 4 0 7.70 6.50 11 4 0 22.50 4.60 11 4 0 19.30 7.10 11 4 0 21.60 4.60 11 4 0 15.50 5.50 11 4 0 22.90 6.20 11 4 0 11.10 3.40 -12 -4 0 246.18 14.60 -12 -4 0 194.28 19.40 -12 -4 0 209.48 15.30 -12 -4 0 206.58 21.60 -12 -4 0 207.38 15.10 -12 -4 0 217.48 19.20 12 4 0 226.28 13.10 12 4 0 229.98 17.20 12 4 0 212.58 12.70 12 4 0 247.98 16.20 12 4 0 211.68 18.60 12 4 0 182.28 16.60 12 4 0 189.48 16.90 12 4 0 173.38 16.80 -13 -4 0 307.27 19.50 -13 -4 0 299.77 24.90 -13 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41.70 7.90 -11 5 0 34.30 6.90 -11 5 0 30.40 11.80 -11 5 0 34.40 7.90 -11 5 0 40.00 7.00 -11 5 0 24.60 8.40 10 -5 0 2.10 2.20 10 -5 0 0.70 2.00 10 -5 0 -7.90 7.50 10 -5 0 1.30 5.30 10 -5 0 2.50 2.30 10 -5 0 3.40 2.10 10 -5 0 2.90 6.20 10 -5 0 8.20 5.20 -10 5 0 12.20 7.30 -10 5 0 8.60 4.60 -10 5 0 3.50 2.90 -10 5 0 -2.40 7.90 -10 5 0 3.30 2.40 -10 5 0 1.20 1.90 -10 5 0 5.40 5.60 -10 5 0 3.00 2.10 9 -5 0 369.06 20.30 9 -5 0 353.06 24.90 9 -5 0 388.96 16.80 9 -5 0 308.97 21.20 9 -5 0 382.26 20.50 9 -5 0 421.96 24.40 9 -5 0 345.97 17.80 9 -5 0 383.46 19.80 9 -5 0 372.46 17.10 9 -5 0 376.66 19.60 -9 5 0 372.56 20.20 -9 5 0 365.96 18.10 -9 5 0 386.66 17.50 -9 5 0 370.86 22.00 -9 5 0 398.76 22.50 -9 5 0 367.86 20.50 8 -5 0 39.60 8.40 8 -5 0 42.60 5.80 8 -5 0 45.00 8.20 8 -5 0 44.30 9.40 8 -5 0 48.40 7.30 8 -5 0 49.80 8.60 8 -5 0 45.90 7.10 8 -5 0 29.50 7.90 8 -5 0 39.00 7.20 8 -5 0 41.10 6.50 -8 5 0 39.00 6.90 -8 5 0 47.00 6.50 -8 5 0 39.80 8.90 -8 5 0 38.50 7.10 -8 5 0 37.00 7.20 -8 5 0 46.30 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8.50 -5 5 0 117.59 7.70 4 -5 0 65.99 6.90 4 -5 0 66.79 5.00 4 -5 0 61.59 5.60 4 -5 0 77.69 6.20 4 -5 0 60.09 5.10 4 -5 0 61.59 6.90 4 -5 0 54.39 4.50 4 -5 0 69.39 4.20 4 -5 0 67.09 5.70 4 -5 0 61.89 7.70 4 -5 0 58.19 6.20 4 -5 0 67.89 6.80 -4 5 0 62.99 6.40 -4 5 0 58.69 6.30 -4 5 0 56.99 4.80 -4 5 0 67.89 4.40 -4 5 0 69.79 5.50 -4 5 0 71.59 5.90 -4 5 0 60.49 6.40 -4 5 0 66.39 5.00 -4 5 0 73.19 6.60 -4 5 0 60.69 5.10 3 -5 0 285.57 12.50 3 -5 0 297.07 12.20 3 -5 0 303.97 11.80 3 -5 0 288.47 13.40 3 -5 0 283.77 13.80 3 -5 0 284.07 11.00 3 -5 0 302.67 13.70 3 -5 0 266.57 12.90 3 -5 0 285.37 10.80 3 -5 0 263.77 11.50 3 -5 0 284.27 10.10 3 -5 0 281.17 12.20 -3 5 0 305.97 13.30 -3 5 0 278.67 11.80 -3 5 0 333.47 12.60 -3 5 0 270.57 11.10 -3 5 0 289.37 12.80 -3 5 0 291.77 13.00 -3 5 0 287.27 11.40 -3 5 0 282.57 10.90 -3 5 0 294.67 13.30 -3 5 0 269.87 12.80 2 -5 0 327.67 12.80 2 -5 0 332.37 14.20 2 -5 0 320.87 11.10 2 -5 0 330.87 14.00 2 -5 0 325.57 11.70 2 -5 0 315.87 11.60 2 -5 0 324.17 13.30 2 -5 0 337.17 12.30 2 -5 0 341.57 13.20 2 -5 0 321.67 12.10 -2 5 0 319.57 12.90 -2 5 0 310.87 11.20 -2 5 0 317.17 11.50 -2 5 0 317.27 12.90 -2 5 0 318.67 13.20 -2 5 0 315.57 12.40 -2 5 0 326.57 12.10 -2 5 0 321.17 11.60 -2 5 0 328.37 11.70 -2 5 0 318.87 13.30 1 -5 0 7.30 1.60 1 -5 0 12.10 2.60 1 -5 0 5.80 1.70 1 -5 0 6.20 2.10 1 -5 0 13.80 3.20 1 -5 0 3.90 1.60 1 -5 0 9.00 2.20 1 -5 0 11.10 2.20 1 -5 0 10.40 2.10 1 -5 0 6.10 1.60 1 -5 0 7.40 2.30 1 -5 0 8.00 2.40 -1 5 0 9.60 1.90 -1 5 0 9.40 2.10 -1 5 0 5.90 2.10 -1 5 0 13.00 2.30 -1 5 0 9.70 2.30 -1 5 0 8.40 2.50 -1 5 0 14.80 2.90 -1 5 0 7.40 1.80 -1 5 0 11.50 2.20 -1 5 0 5.50 1.50 -1 5 0 8.90 2.70 -1 5 0 13.30 2.70 0 -5 0 6.70 1.80 0 -5 0 10.90 2.00 0 -5 0 6.70 1.50 0 -5 0 11.80 2.30 0 -5 0 3.20 1.30 0 -5 0 9.50 2.30 0 -5 0 11.90 1.90 0 -5 0 5.10 2.30 0 -5 0 5.70 1.90 0 5 0 10.80 2.20 0 5 0 6.30 1.80 0 5 0 7.00 1.60 0 5 0 4.40 1.60 0 5 0 6.00 1.60 0 5 0 6.40 1.50 0 5 0 10.20 2.70 0 5 0 9.40 2.50 0 5 0 6.90 1.90 0 5 0 8.20 1.80 0 5 0 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31.10 6 5 0 876.61 29.80 6 5 0 884.31 27.20 6 5 0 940.31 27.00 6 5 0 945.71 30.00 -7 -5 0 684.43 22.80 -7 -5 0 705.53 22.50 -7 -5 0 695.53 25.20 -7 -5 0 714.93 23.50 -7 -5 0 680.93 24.00 -7 -5 0 688.83 27.40 -7 -5 0 697.73 26.60 -7 -5 0 698.83 21.40 7 5 0 771.92 28.70 7 5 0 724.93 22.80 7 5 0 712.43 22.90 7 5 0 701.03 23.00 7 5 0 720.03 28.30 7 5 0 683.93 24.40 7 5 0 697.53 25.80 7 5 0 704.93 21.60 -8 -5 0 448.76 15.60 -8 -5 0 429.46 17.80 -8 -5 0 427.06 16.80 -8 -5 0 416.46 20.90 -8 -5 0 415.66 19.40 -8 -5 0 414.96 21.70 -8 -5 0 427.26 18.50 -8 -5 0 457.15 17.20 8 5 0 438.96 16.40 8 5 0 423.86 16.70 8 5 0 410.86 19.70 8 5 0 419.06 22.00 8 5 0 415.96 19.10 8 5 0 443.66 19.00 8 5 0 394.76 16.80 8 5 0 434.06 15.60 8 5 0 388.16 16.50 8 5 0 453.45 22.60 -9 -5 0 170.58 8.80 -9 -5 0 170.48 10.20 -9 -5 0 158.58 13.00 -9 -5 0 143.39 10.10 -9 -5 0 184.58 10.70 -9 -5 0 175.88 14.70 -9 -5 0 194.98 13.60 -9 -5 0 152.78 11.00 9 5 0 163.48 9.60 9 5 0 151.48 13.40 9 5 0 160.38 10.10 9 5 0 160.18 14.30 9 5 0 166.28 10.00 9 5 0 156.68 12.80 9 5 0 168.08 12.50 9 5 0 157.78 8.60 9 5 0 157.08 11.90 9 5 0 152.98 10.40 -10 -5 0 347.47 13.70 -10 -5 0 346.57 20.70 -10 -5 0 357.46 15.30 -10 -5 0 381.16 17.90 -10 -5 0 323.97 17.70 -10 -5 0 351.86 22.50 -10 -5 0 374.66 17.20 -10 -5 0 360.56 19.70 -10 -5 0 309.47 20.20 -10 -5 0 355.16 23.50 10 5 0 358.06 22.50 10 5 0 350.86 13.70 10 5 0 358.36 19.70 10 5 0 359.26 16.40 10 5 0 323.17 18.20 10 5 0 355.86 15.20 10 5 0 345.37 17.30 10 5 0 357.76 22.20 10 5 0 322.37 15.00 10 5 0 362.06 20.00 -11 -5 0 405.66 25.70 -11 -5 0 404.46 16.80 -11 -5 0 404.46 18.80 -11 -5 0 447.56 24.20 -11 -5 0 399.06 14.90 -11 -5 0 432.76 20.20 -11 -5 0 395.96 20.60 -11 -5 0 385.66 25.20 -11 -5 0 393.76 24.00 -11 -5 0 402.86 21.10 11 5 0 411.66 16.40 11 5 0 402.56 14.80 11 5 0 362.56 19.00 11 5 0 433.16 18.00 11 5 0 411.96 22.80 11 5 0 373.76 24.40 11 5 0 416.56 18.50 11 5 0 453.45 23.10 11 5 0 383.16 20.90 11 5 0 418.86 25.40 -12 -5 0 10.80 2.50 -12 -5 0 16.30 8.30 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2.50 -12 6 0 4.20 3.10 -12 6 0 14.40 10.70 -12 6 0 -0.70 16.40 -12 6 0 -0.30 5.30 -12 6 0 7.40 4.00 -12 6 0 3.40 2.30 11 -6 0 36.20 9.60 11 -6 0 51.79 10.70 11 -6 0 29.00 8.70 11 -6 0 34.40 7.50 11 -6 0 52.99 7.40 11 -6 0 48.10 8.00 -11 6 0 40.60 10.20 -11 6 0 48.10 8.50 -11 6 0 38.70 6.80 -11 6 0 45.80 9.90 -11 6 0 47.00 9.40 -11 6 0 59.69 15.20 -11 6 0 37.10 6.80 -11 6 0 25.50 9.30 10 -6 0 78.09 14.90 10 -6 0 81.69 10.80 10 -6 0 72.19 11.20 10 -6 0 65.89 11.00 10 -6 0 59.19 10.00 10 -6 0 94.59 13.80 10 -6 0 63.09 11.00 10 -6 0 61.49 14.20 10 -6 0 60.69 13.00 10 -6 0 70.09 8.30 -10 6 0 66.39 8.60 -10 6 0 55.69 8.50 -10 6 0 63.39 9.00 -10 6 0 59.29 14.40 -10 6 0 69.29 12.70 -10 6 0 60.79 12.10 -10 6 0 56.99 11.00 -10 6 0 67.79 11.40 9 -6 0 116.59 14.90 9 -6 0 126.29 9.10 9 -6 0 117.59 11.80 9 -6 0 118.59 13.40 9 -6 0 117.79 17.00 9 -6 0 137.79 12.20 9 -6 0 140.99 14.40 9 -6 0 111.39 11.90 -9 6 0 138.19 10.10 -9 6 0 121.29 11.40 -9 6 0 133.89 10.90 -9 6 0 107.59 9.50 -9 6 0 115.09 12.70 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58.79 8.40 4 8 0 61.39 4.90 4 8 0 57.19 7.30 4 8 0 63.89 5.00 4 8 0 58.59 5.80 4 8 0 45.10 6.40 4 8 0 59.39 6.20 4 8 0 56.19 8.30 4 8 0 55.39 7.70 4 8 0 52.59 7.30 4 8 0 64.09 7.10 4 8 0 55.49 3.80 -5 -8 0 141.79 10.00 -5 -8 0 136.79 9.00 -5 -8 0 141.89 10.80 -5 -8 0 137.19 9.00 -5 -8 0 151.88 8.40 -5 -8 0 132.59 8.30 -5 -8 0 144.09 8.00 -5 -8 0 159.58 11.00 -5 -8 0 160.78 9.30 -5 -8 0 149.88 10.60 5 8 0 151.38 6.80 5 8 0 167.48 10.00 5 8 0 154.28 8.20 5 8 0 144.29 11.00 5 8 0 154.68 9.90 5 8 0 162.48 10.60 5 8 0 144.69 9.60 5 8 0 143.59 10.90 5 8 0 162.78 9.20 5 8 0 153.98 7.90 5 8 0 174.88 12.80 5 8 0 166.68 11.80 5 8 0 141.19 10.50 -6 -8 0 15.60 3.40 -6 -8 0 25.20 4.60 -6 -8 0 18.40 5.20 -6 -8 0 26.20 4.80 -6 -8 0 15.30 4.00 -6 -8 0 25.80 3.90 -6 -8 0 23.70 5.30 -6 -8 0 16.60 3.30 -6 -8 0 22.20 5.40 -6 -8 0 25.40 4.60 6 8 0 22.60 4.30 6 8 0 25.00 6.50 6 8 0 28.90 6.00 6 8 0 27.00 3.80 6 8 0 16.10 4.00 6 8 0 23.70 5.50 6 8 0 17.80 5.00 6 8 0 12.70 5.10 6 8 0 30.20 8.90 6 8 0 22.20 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60.39 10.30 9 8 0 52.59 6.80 9 8 0 45.20 7.80 9 8 0 48.20 10.40 9 8 0 66.69 8.90 9 8 0 47.70 10.80 9 8 0 45.70 8.70 9 8 0 44.70 6.60 9 8 0 47.60 8.00 9 8 0 50.89 6.90 9 8 0 57.59 11.50 -10 -8 0 159.58 14.70 -10 -8 0 149.49 12.30 -10 -8 0 155.28 16.10 -10 -8 0 170.18 11.00 -10 -8 0 141.39 15.00 -10 -8 0 158.68 10.40 -10 -8 0 129.49 10.70 -10 -8 0 176.28 12.30 10 8 0 171.68 13.20 10 8 0 159.18 11.10 10 8 0 174.78 16.80 10 8 0 169.48 15.40 10 8 0 167.28 10.80 10 8 0 169.78 15.80 10 8 0 144.99 10.20 10 8 0 161.98 10.10 10 8 0 161.38 13.30 10 8 0 153.28 12.60 -11 -8 0 7.40 3.00 -11 -8 0 15.60 7.80 -11 -8 0 4.20 2.20 -11 -8 0 -3.00 7.80 -11 -8 0 12.40 5.50 -11 -8 0 8.10 7.10 -11 -8 0 2.80 2.20 -11 -8 0 9.60 3.70 11 8 0 5.10 4.90 11 8 0 6.10 5.10 11 8 0 4.80 2.60 11 8 0 0.50 5.80 11 8 0 5.70 4.30 11 8 0 9.70 7.60 11 8 0 6.40 7.20 11 8 0 3.50 2.10 11 8 0 7.90 3.30 11 8 0 2.80 2.30 -12 -8 0 7.90 3.40 -12 -8 0 11.10 4.10 -12 -8 0 12.40 6.30 -12 -8 0 3.40 8.60 -12 -8 0 9.50 3.50 -12 -8 0 9.90 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100.39 14.90 -9 9 0 92.99 11.80 -9 9 0 72.89 11.70 -9 9 0 76.39 10.60 -9 9 0 81.39 10.60 -9 9 0 87.69 13.80 -9 9 0 78.19 9.70 8 -9 0 40.30 9.30 8 -9 0 32.20 7.30 8 -9 0 12.70 10.00 8 -9 0 36.90 4.50 8 -9 0 36.40 8.30 8 -9 0 36.70 7.50 8 -9 0 36.60 5.80 8 -9 0 28.10 5.30 8 -9 0 36.40 10.00 8 -9 0 30.80 6.50 8 -9 0 29.60 7.00 8 -9 0 26.00 8.40 -8 9 0 27.80 6.80 -8 9 0 36.60 6.20 -8 9 0 43.30 10.00 -8 9 0 20.90 10.80 -8 9 0 31.20 6.10 -8 9 0 48.50 9.30 -8 9 0 33.70 9.00 -8 9 0 41.00 7.50 7 -9 0 701.63 35.40 7 -9 0 710.63 32.60 7 -9 0 702.73 33.20 7 -9 0 728.93 28.50 7 -9 0 746.53 26.00 7 -9 0 759.02 30.20 7 -9 0 736.23 29.60 7 -9 0 776.42 30.40 7 -9 0 696.93 22.30 7 -9 0 673.53 31.90 7 -9 0 723.73 30.20 7 -9 0 743.43 24.60 -7 9 0 753.82 29.80 -7 9 0 763.82 27.70 -7 9 0 731.83 25.10 -7 9 0 732.43 29.20 -7 9 0 743.33 31.90 -7 9 0 747.23 26.60 -7 9 0 710.13 34.20 -7 9 0 702.73 31.30 -7 9 0 710.43 23.20 -7 9 0 668.43 29.60 6 -9 0 252.17 13.10 6 -9 0 270.97 16.20 6 -9 0 271.37 18.00 6 -9 0 243.78 14.60 6 -9 0 260.27 11.80 6 -9 0 249.68 19.80 6 -9 0 287.77 16.10 6 -9 0 265.17 13.60 6 -9 0 242.88 18.80 6 -9 0 255.47 18.20 6 -9 0 245.08 16.10 6 -9 0 274.57 16.50 -6 9 0 268.17 17.20 -6 9 0 255.57 18.60 -6 9 0 244.98 12.20 -6 9 0 272.77 15.70 -6 9 0 252.97 13.90 -6 9 0 253.17 14.70 -6 9 0 272.57 17.60 -6 9 0 272.77 14.20 -6 9 0 287.67 17.70 -6 9 0 252.17 13.50 5 -9 0 46.90 7.10 5 -9 0 51.59 9.70 5 -9 0 30.60 6.80 5 -9 0 61.69 9.60 5 -9 0 55.49 6.40 5 -9 0 47.20 6.70 5 -9 0 51.39 8.20 5 -9 0 53.99 10.70 5 -9 0 42.20 8.80 5 -9 0 59.89 8.80 5 -9 0 50.09 6.30 5 -9 0 35.30 6.00 -5 9 0 39.80 5.50 -5 9 0 51.69 8.10 -5 9 0 63.79 8.80 -5 9 0 43.10 7.50 -5 9 0 62.59 7.20 -5 9 0 53.39 7.60 -5 9 0 50.09 9.10 -5 9 0 52.79 8.30 -5 9 0 35.20 8.20 -5 9 0 51.29 7.30 4 -9 0 242.58 16.70 4 -9 0 277.07 13.90 4 -9 0 271.27 15.30 4 -9 0 246.78 13.40 4 -9 0 243.08 18.90 4 -9 0 243.68 11.90 4 -9 0 250.67 12.40 4 -9 0 278.27 16.00 4 -9 0 217.18 14.50 4 -9 0 284.27 15.70 -4 9 0 259.87 13.90 -4 9 0 299.77 16.20 -4 9 0 258.97 14.00 -4 9 0 249.78 12.50 -4 9 0 230.48 14.50 -4 9 0 253.87 12.60 -4 9 0 235.18 13.60 -4 9 0 258.97 14.00 -4 9 0 275.17 16.90 -4 9 0 261.07 15.70 -4 9 0 258.67 13.50 -4 9 0 257.67 13.10 3 -9 0 110.59 10.40 3 -9 0 126.89 10.50 3 -9 0 139.49 8.60 3 -9 0 125.09 8.50 3 -9 0 114.19 11.10 3 -9 0 131.39 9.80 3 -9 0 127.49 8.30 3 -9 0 117.29 11.10 3 -9 0 128.59 9.20 3 -9 0 114.59 13.00 3 -9 0 134.59 10.40 3 -9 0 118.19 8.50 -3 9 0 126.89 10.50 -3 9 0 133.79 9.30 -3 9 0 127.19 10.20 -3 9 0 144.89 11.70 -3 9 0 110.09 9.50 -3 9 0 125.49 8.20 -3 9 0 135.09 10.50 -3 9 0 135.99 9.00 -3 9 0 122.79 8.90 -3 9 0 132.99 8.80 -3 9 0 121.79 9.20 -3 9 0 121.49 8.30 2 -9 0 308.27 16.30 2 -9 0 340.97 17.50 2 -9 0 347.17 15.40 2 -9 0 373.66 16.40 2 -9 0 331.67 16.50 2 -9 0 367.46 15.30 2 -9 0 368.76 14.50 2 -9 0 357.86 18.30 2 -9 0 401.86 15.20 2 -9 0 334.47 18.80 2 -9 0 359.56 15.10 2 -9 0 348.87 16.60 -2 9 0 363.76 15.80 -2 9 0 354.46 15.40 -2 9 0 360.86 17.60 -2 9 0 368.66 17.30 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142.09 8.60 -5 -9 0 139.69 8.30 -5 -9 0 157.78 10.30 5 9 0 157.88 9.40 5 9 0 155.88 10.80 5 9 0 138.09 12.30 5 9 0 159.08 7.80 5 9 0 137.49 8.10 5 9 0 147.39 11.60 5 9 0 143.59 6.50 5 9 0 132.79 9.60 5 9 0 139.49 9.80 5 9 0 153.78 11.60 5 9 0 147.59 11.50 5 9 0 156.88 10.20 5 9 0 138.29 11.80 5 9 0 139.79 10.90 -6 -9 0 13.40 4.20 -6 -9 0 10.50 2.80 -6 -9 0 7.60 3.90 -6 -9 0 10.60 3.00 -6 -9 0 11.80 3.70 -6 -9 0 8.30 3.80 -6 -9 0 8.90 3.00 -6 -9 0 12.50 5.40 -6 -9 0 14.60 4.40 -6 -9 0 11.20 3.20 6 9 0 5.20 3.80 6 9 0 9.00 4.50 6 9 0 10.40 2.40 6 9 0 11.80 3.30 6 9 0 13.50 4.10 6 9 0 9.90 3.70 6 9 0 3.20 3.60 6 9 0 18.80 4.70 6 9 0 6.40 4.80 6 9 0 5.40 2.30 6 9 0 5.70 2.50 6 9 0 4.70 4.00 6 9 0 10.10 2.70 6 9 0 5.30 3.00 -7 -9 0 8.00 4.30 -7 -9 0 0.50 4.10 -7 -9 0 1.30 1.50 -7 -9 0 3.40 1.90 -7 -9 0 0.80 2.90 -7 -9 0 0.80 1.40 -7 -9 0 -0.50 4.10 -7 -9 0 4.50 2.00 -7 -9 0 3.60 2.10 -7 -9 0 3.50 3.50 7 9 0 4.00 1.70 7 9 0 3.10 3.60 7 9 0 10.40 4.80 7 9 0 -2.00 3.60 7 9 0 1.80 2.40 7 9 0 2.30 1.80 7 9 0 4.30 2.10 7 9 0 1.90 3.70 7 9 0 1.50 1.60 7 9 0 3.40 2.10 7 9 0 4.40 2.90 7 9 0 2.20 3.10 7 9 0 -1.30 3.50 7 9 0 4.40 4.90 -8 -9 0 382.16 21.70 -8 -9 0 351.86 17.50 -8 -9 0 399.46 20.00 -8 -9 0 402.16 18.00 -8 -9 0 374.16 18.60 -8 -9 0 400.76 17.80 -8 -9 0 430.56 22.10 -8 -9 0 403.76 23.40 -8 -9 0 402.96 15.70 -8 -9 0 374.36 13.60 8 9 0 368.26 21.70 8 9 0 403.26 17.20 8 9 0 402.36 23.20 8 9 0 376.36 15.00 8 9 0 397.96 20.10 8 9 0 411.66 21.50 8 9 0 449.06 24.20 8 9 0 374.96 25.80 8 9 0 441.76 24.00 8 9 0 370.66 20.50 8 9 0 393.16 17.80 8 9 0 387.76 17.90 -9 -9 0 12.10 7.10 -9 -9 0 4.90 4.80 -9 -9 0 4.50 2.70 -9 -9 0 -1.70 4.90 -9 -9 0 7.60 3.30 -9 -9 0 6.20 2.50 9 9 0 -0.10 1.90 9 9 0 1.70 5.60 9 9 0 8.80 4.80 9 9 0 7.70 3.10 9 9 0 6.60 2.60 9 9 0 5.50 2.90 9 9 0 7.40 5.10 9 9 0 1.70 4.10 9 9 0 3.20 2.70 9 9 0 9.30 5.40 -10 -9 0 14.50 6.70 -10 -9 0 12.10 6.80 -10 -9 0 24.50 4.90 -10 -9 0 13.20 3.90 -10 -9 0 13.50 5.40 -10 -9 0 8.30 7.90 -10 -9 0 14.30 3.80 -10 -9 0 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0 -0.50 6.30 7 -10 0 0.80 2.20 7 -10 0 -0.50 1.50 7 -10 0 3.00 4.30 7 -10 0 -2.40 4.20 7 -10 0 -1.30 8.20 7 -10 0 -3.30 4.00 7 -10 0 3.00 1.80 7 -10 0 1.80 2.50 -7 10 0 3.60 5.50 -7 10 0 1.20 1.80 -7 10 0 9.90 4.80 -7 10 0 3.40 4.20 -7 10 0 -0.60 8.30 -7 10 0 -0.10 4.10 -7 10 0 -0.90 1.40 -7 10 0 1.60 1.20 -7 10 0 -2.30 6.70 -7 10 0 -1.20 1.10 -7 10 0 1.10 2.10 6 -10 0 2.70 4.90 6 -10 0 11.50 4.40 6 -10 0 7.60 4.90 6 -10 0 8.20 2.80 6 -10 0 12.50 5.20 6 -10 0 -2.00 5.50 6 -10 0 6.50 4.20 6 -10 0 12.40 3.70 6 -10 0 5.70 2.70 6 -10 0 1.20 5.60 -6 10 0 5.50 2.40 -6 10 0 4.80 2.90 -6 10 0 2.10 6.60 -6 10 0 3.40 2.70 -6 10 0 10.70 5.10 -6 10 0 18.20 5.20 -6 10 0 6.80 3.00 -6 10 0 4.10 4.00 -6 10 0 12.10 3.80 -6 10 0 9.20 3.00 -6 10 0 7.50 5.40 -6 10 0 -4.80 8.20 5 -10 0 6.50 4.30 5 -10 0 -0.40 5.50 5 -10 0 2.90 2.10 5 -10 0 4.10 2.80 5 -10 0 4.90 4.00 5 -10 0 3.80 3.70 5 -10 0 0.50 4.40 5 -10 0 2.90 1.80 5 -10 0 0.60 1.40 5 -10 0 -3.70 5.50 5 -10 0 1.00 2.10 5 -10 0 1.00 2.00 -5 10 0 0.70 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0 419.66 20.40 8 11 0 383.36 20.50 8 11 0 379.06 24.80 8 11 0 379.86 22.40 8 11 0 389.26 21.80 8 11 0 356.16 23.40 8 11 0 377.96 16.50 8 11 0 374.16 23.80 8 11 0 430.66 25.00 8 11 0 379.16 16.30 -9 -11 0 82.29 12.00 -9 -11 0 72.29 11.90 -9 -11 0 76.79 8.80 -9 -11 0 87.29 10.80 -9 -11 0 94.79 8.60 -9 -11 0 79.29 6.00 -9 -11 0 60.39 8.70 -9 -11 0 60.69 7.70 -9 -11 0 70.69 11.20 -9 -11 0 47.00 9.30 9 11 0 67.19 10.80 9 11 0 76.09 12.80 9 11 0 87.09 15.40 9 11 0 99.29 16.20 9 11 0 73.19 9.50 9 11 0 80.29 9.80 9 11 0 87.69 13.20 9 11 0 70.69 5.90 9 11 0 76.49 12.60 9 11 0 62.59 8.80 9 11 0 90.69 14.80 9 11 0 53.19 7.90 -10 -11 0 167.38 12.50 -10 -11 0 212.48 18.30 -10 -11 0 183.88 17.10 -10 -11 0 200.38 16.80 -10 -11 0 192.48 19.70 -10 -11 0 197.68 14.10 -10 -11 0 185.88 12.10 -10 -11 0 185.58 12.80 10 11 0 199.18 18.80 10 11 0 193.68 16.30 10 11 0 189.18 13.20 10 11 0 196.48 19.00 10 11 0 172.88 17.10 10 11 0 185.88 10.60 10 11 0 195.98 13.70 10 11 0 185.38 16.60 10 11 0 228.98 14.10 10 11 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227.98 23.70 -6 12 0 238.38 18.70 5 -12 0 0.80 1.30 5 -12 0 1.40 7.70 5 -12 0 -1.60 1.30 5 -12 0 1.30 1.50 5 -12 0 5.00 4.90 5 -12 0 -4.70 4.00 5 -12 0 -0.60 1.10 5 -12 0 0.40 6.00 5 -12 0 -1.30 1.10 5 -12 0 2.50 2.20 5 -12 0 8.70 8.10 5 -12 0 -2.20 4.80 -5 12 0 2.40 2.20 -5 12 0 2.80 3.80 -5 12 0 -0.90 1.10 -5 12 0 -0.10 1.20 -5 12 0 9.20 6.90 -5 12 0 -0.80 5.50 -5 12 0 1.60 2.00 -5 12 0 6.50 5.60 -5 12 0 -1.20 3.70 -5 12 0 -1.10 0.80 -5 12 0 -3.40 8.10 -5 12 0 2.50 2.00 4 -12 0 53.89 10.20 4 -12 0 47.50 7.40 4 -12 0 58.39 9.00 4 -12 0 49.50 9.10 4 -12 0 26.80 7.70 4 -12 0 47.00 7.10 4 -12 0 47.30 7.70 4 -12 0 58.19 12.20 4 -12 0 63.09 9.20 4 -12 0 49.80 10.90 4 -12 0 45.30 8.80 -4 12 0 43.00 7.90 -4 12 0 42.60 8.70 -4 12 0 59.29 12.10 -4 12 0 48.10 7.30 -4 12 0 56.39 10.40 -4 12 0 31.80 7.30 -4 12 0 44.40 8.20 -4 12 0 37.50 6.20 -4 12 0 44.40 7.40 -4 12 0 50.09 8.80 -4 12 0 31.20 5.40 -4 12 0 37.10 6.60 3 -12 0 50.49 8.00 3 -12 0 58.79 9.70 3 -12 0 62.59 11.00 3 -12 0 53.79 10.50 3 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6.40 1 12 0 30.80 6.40 1 12 0 44.00 8.70 1 12 0 29.50 5.10 1 12 0 37.80 7.20 1 12 0 42.10 8.10 1 12 0 24.70 5.80 1 12 0 34.30 7.20 -2 -12 0 111.49 11.20 -2 -12 0 131.39 10.20 -2 -12 0 110.09 10.60 -2 -12 0 106.99 11.30 -2 -12 0 119.59 11.30 -2 -12 0 105.89 8.10 -2 -12 0 95.59 9.10 -2 -12 0 128.89 9.20 -2 -12 0 116.39 8.60 -2 -12 0 103.29 11.50 2 12 0 123.19 11.40 2 12 0 99.79 8.80 2 12 0 118.09 8.70 2 12 0 101.79 9.40 2 12 0 124.49 11.40 2 12 0 106.39 10.20 2 12 0 96.49 9.30 2 12 0 117.99 8.60 2 12 0 97.59 8.50 2 12 0 85.89 9.80 2 12 0 116.09 11.60 2 12 0 113.79 12.10 -3 -12 0 194.78 13.70 -3 -12 0 201.28 13.10 -3 -12 0 187.48 11.50 -3 -12 0 191.78 14.70 -3 -12 0 179.18 10.70 -3 -12 0 165.98 13.80 -3 -12 0 184.98 13.90 -3 -12 0 170.98 10.40 -3 -12 0 179.08 13.10 -3 -12 0 190.08 12.60 3 12 0 180.88 14.90 3 12 0 178.58 13.50 3 12 0 204.38 13.60 3 12 0 170.98 11.60 3 12 0 169.08 10.80 3 12 0 180.68 14.00 3 12 0 179.68 13.20 3 12 0 171.98 12.50 3 12 0 174.48 7.30 3 12 0 173.98 8.70 3 12 0 191.88 10.90 3 12 0 192.88 12.70 3 12 0 182.58 15.10 3 12 0 175.98 13.40 -4 -12 0 30.70 5.90 -4 -12 0 17.70 5.40 -4 -12 0 27.10 6.90 -4 -12 0 24.00 4.80 -4 -12 0 24.00 7.30 -4 -12 0 35.80 5.60 4 12 0 21.70 7.00 4 12 0 34.40 7.10 4 12 0 42.10 9.00 4 12 0 24.50 6.20 4 12 0 30.70 7.40 4 12 0 27.60 5.30 4 12 0 19.70 4.10 4 12 0 12.30 6.40 4 12 0 14.40 5.80 4 12 0 33.90 6.70 4 12 0 17.80 5.50 4 12 0 19.50 7.60 -5 -12 0 421.46 19.00 -5 -12 0 417.16 18.90 -5 -12 0 383.06 19.90 -5 -12 0 445.06 21.70 -5 -12 0 405.76 17.20 -5 -12 0 399.96 22.00 -5 -12 0 431.16 19.10 -5 -12 0 414.86 19.80 -5 -12 0 393.36 22.20 -5 -12 0 431.66 22.80 5 12 0 340.17 26.90 5 12 0 407.66 22.30 5 12 0 497.35 32.90 5 12 0 389.56 22.30 5 12 0 407.16 22.20 5 12 0 374.86 16.60 5 12 0 399.76 18.20 5 12 0 396.86 20.30 5 12 0 398.56 20.50 5 12 0 398.66 22.00 -6 -12 0 295.77 17.60 -6 -12 0 272.97 19.50 -6 -12 0 304.17 18.10 -6 -12 0 307.47 15.20 -6 -12 0 324.47 20.80 -6 -12 0 308.77 16.70 -6 -12 0 320.77 16.90 -6 -12 0 356.66 20.60 -6 -12 0 314.07 15.50 -6 -12 0 296.27 16.60 6 12 0 321.27 21.80 6 12 0 293.57 18.90 6 12 0 275.67 18.90 6 12 0 306.17 18.00 6 12 0 282.87 15.40 6 12 0 263.37 18.60 6 12 0 292.77 17.00 6 12 0 293.37 17.10 6 12 0 328.97 20.80 6 12 0 293.97 10.10 6 12 0 284.07 19.10 6 12 0 294.27 11.50 6 12 0 333.07 17.90 6 12 0 306.27 14.50 -7 -12 0 80.69 12.10 -7 -12 0 92.99 12.10 -7 -12 0 86.09 9.70 -7 -12 0 64.39 9.60 -7 -12 0 72.39 9.90 -7 -12 0 64.49 8.50 -7 -12 0 85.39 12.60 -7 -12 0 80.59 11.70 -7 -12 0 73.99 7.10 -7 -12 0 74.49 8.20 7 12 0 64.59 9.90 7 12 0 72.09 10.60 7 12 0 72.69 12.60 7 12 0 94.19 13.90 7 12 0 69.49 8.60 7 12 0 58.09 10.10 7 12 0 73.79 8.10 7 12 0 61.69 11.80 7 12 0 64.39 8.50 7 12 0 64.09 9.60 7 12 0 62.39 9.10 7 12 0 66.09 4.50 7 12 0 70.09 11.70 7 12 0 71.29 6.60 -8 -12 0 289.87 15.30 -8 -12 0 296.27 19.30 -8 -12 0 261.97 16.00 -8 -12 0 252.27 15.60 -8 -12 0 276.07 14.50 -8 -12 0 277.77 20.30 -8 -12 0 291.57 16.50 -8 -12 0 298.47 19.10 -8 -12 0 280.47 19.30 -8 -12 0 283.67 14.00 8 12 0 262.47 15.40 8 12 0 305.07 21.70 8 12 0 269.17 19.30 8 12 0 253.87 17.80 8 12 0 290.77 23.10 8 12 0 238.58 16.50 8 12 0 307.87 21.40 8 12 0 278.77 16.90 8 12 0 281.17 13.00 8 12 0 271.77 13.90 8 12 0 277.27 19.90 8 12 0 246.38 16.70 8 12 0 249.08 20.40 8 12 0 265.27 10.80 -9 -12 0 39.50 7.40 -9 -12 0 57.89 8.70 -9 -12 0 48.70 9.90 -9 -12 0 45.40 8.60 -9 -12 0 43.50 11.10 -9 -12 0 41.80 6.20 -9 -12 0 43.80 6.70 -9 -12 0 36.70 9.00 -9 -12 0 37.60 7.40 -9 -12 0 43.40 9.80 9 12 0 41.80 11.20 9 12 0 45.70 7.70 9 12 0 38.70 10.80 9 12 0 37.10 10.60 9 12 0 40.20 9.30 9 12 0 23.70 7.10 9 12 0 30.00 8.60 9 12 0 41.40 7.30 9 12 0 45.60 4.40 9 12 0 43.30 6.60 9 12 0 35.40 8.90 9 12 0 33.50 6.80 -10 -12 0 41.90 4.30 -10 -12 0 42.90 8.00 -10 -12 0 42.30 7.80 -10 -12 0 59.29 12.90 -10 -12 0 39.50 10.90 -10 -12 0 50.69 7.50 -10 -12 0 43.30 7.40 -10 -12 0 60.89 11.70 -10 -12 0 39.20 9.80 -10 -12 0 40.70 7.10 10 12 0 45.70 10.30 10 12 0 45.50 8.30 10 12 0 36.30 11.10 10 12 0 43.70 7.70 10 12 0 34.60 8.90 10 12 0 33.60 9.30 10 12 0 47.80 7.80 10 12 0 31.50 9.60 10 12 0 51.79 11.50 10 12 0 52.49 6.50 -11 -12 0 160.48 12.50 -11 -12 0 152.78 17.30 -11 -12 0 135.99 16.20 -11 -12 0 166.38 22.20 -11 -12 0 164.28 12.90 -11 -12 0 162.38 13.50 11 12 0 170.38 18.60 11 12 0 172.48 20.00 11 12 0 192.98 20.20 11 12 0 159.58 13.00 11 12 0 161.38 10.00 11 12 0 130.89 18.10 11 12 0 156.18 13.00 11 12 0 141.39 12.00 -12 -12 0 38.10 15.60 -12 -12 0 42.50 8.60 -12 -12 0 84.29 14.70 -12 -12 0 35.70 13.40 -12 -12 0 58.59 13.00 -12 -12 0 59.79 9.50 -12 -12 0 50.19 7.90 -12 -12 0 48.90 9.40 12 12 0 58.69 8.20 12 12 0 58.29 10.60 12 12 0 66.09 17.00 12 12 0 48.10 13.60 12 12 0 57.89 8.90 12 12 0 56.99 9.60 12 12 0 47.40 12.60 12 12 0 56.69 14.70 7 -13 0 91.69 15.00 7 -13 0 62.59 8.10 7 -13 0 64.49 9.90 7 -13 0 57.29 11.70 7 -13 0 69.19 12.50 7 -13 0 88.59 11.90 7 -13 0 52.39 13.70 7 -13 0 59.69 8.70 -7 13 0 65.39 10.50 -7 13 0 89.89 14.50 -7 13 0 71.89 20.20 -7 13 0 68.19 9.20 -7 13 0 86.39 14.40 -7 13 0 62.79 9.20 -7 13 0 56.59 10.20 -7 13 0 81.49 10.20 -7 13 0 64.89 9.80 -7 13 0 62.49 10.80 -7 13 0 64.19 13.00 -7 13 0 84.09 14.80 6 -13 0 6.10 3.60 6 -13 0 25.50 6.50 6 -13 0 15.30 8.90 6 -13 0 27.30 8.80 6 -13 0 17.90 10.90 6 -13 0 19.50 5.00 6 -13 0 19.60 5.50 6 -13 0 20.80 5.00 6 -13 0 24.20 6.30 6 -13 0 16.80 7.60 6 -13 0 10.60 6.50 6 -13 0 9.10 11.40 -6 13 0 -3.00 8.20 -6 13 0 18.20 5.70 -6 13 0 12.90 4.10 -6 13 0 30.90 9.50 -6 13 0 19.50 5.80 -6 13 0 14.10 4.70 -6 13 0 5.70 12.00 -6 13 0 21.50 7.10 -6 13 0 14.50 8.80 -6 13 0 18.30 4.80 -6 13 0 11.40 6.20 -6 13 0 24.50 5.80 5 -13 0 13.20 10.20 5 -13 0 35.30 9.20 5 -13 0 23.40 10.90 5 -13 0 31.10 5.90 5 -13 0 37.40 7.20 5 -13 0 53.99 13.00 5 -13 0 51.59 11.40 5 -13 0 39.20 7.50 5 -13 0 41.70 8.30 5 -13 0 24.80 8.70 5 -13 0 45.40 10.40 5 -13 0 36.60 7.40 -5 13 0 21.30 12.20 -5 13 0 26.80 5.50 -5 13 0 47.80 10.60 -5 13 0 40.50 8.10 -5 13 0 46.90 10.60 -5 13 0 41.70 7.40 -5 13 0 37.50 8.50 -5 13 0 30.20 6.60 -5 13 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0 128.19 11.30 -4 -14 0 111.69 12.70 4 14 0 114.19 13.30 4 14 0 102.49 13.40 4 14 0 124.19 11.50 4 14 0 108.69 11.60 4 14 0 90.99 10.70 4 14 0 106.19 14.70 4 14 0 95.29 13.20 4 14 0 109.69 12.50 4 14 0 114.89 9.10 4 14 0 103.19 10.20 -5 -14 0 4.50 6.00 -5 -14 0 3.50 2.30 -5 -14 0 1.30 7.20 -5 -14 0 7.50 6.20 -5 -14 0 3.80 2.50 -5 -14 0 4.30 2.40 -5 -14 0 8.40 3.70 -5 -14 0 -1.00 4.20 -5 -14 0 1.20 1.90 -5 -14 0 -1.70 6.30 5 14 0 4.30 2.70 5 14 0 1.10 2.50 5 14 0 -3.50 7.30 5 14 0 1.70 2.00 5 14 0 -1.70 5.70 5 14 0 0.30 1.30 5 14 0 7.30 5.40 5 14 0 0.20 1.80 5 14 0 0.80 5.70 5 14 0 4.10 5.40 5 14 0 5.00 5.80 5 14 0 2.00 1.80 -6 -14 0 45.50 10.10 -6 -14 0 49.00 7.00 -6 -14 0 40.70 10.50 -6 -14 0 35.60 8.50 -6 -14 0 46.80 9.60 -6 -14 0 52.69 7.80 -6 -14 0 59.19 9.20 -6 -14 0 60.19 8.80 -6 -14 0 49.20 8.20 -6 -14 0 44.40 9.10 6 14 0 52.99 7.90 6 14 0 69.99 11.70 6 14 0 47.20 10.70 6 14 0 46.20 8.20 6 14 0 53.59 12.00 6 14 0 31.80 9.30 6 14 0 57.39 10.30 6 14 0 62.99 11.30 6 14 0 32.50 8.90 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87.69 13.80 3 -15 0 104.59 12.80 3 -15 0 87.69 8.30 3 -15 0 65.19 11.10 3 -15 0 78.59 14.60 3 -15 0 68.99 12.40 3 -15 0 81.99 11.20 3 -15 0 101.49 13.20 -3 15 0 110.39 14.10 -3 15 0 57.79 12.20 -3 15 0 115.99 16.60 -3 15 0 85.09 14.40 -3 15 0 86.39 10.40 -3 15 0 89.49 11.50 -3 15 0 76.79 10.20 -3 15 0 85.59 13.80 -3 15 0 108.79 10.90 -3 15 0 101.29 13.40 2 -15 0 33.90 11.10 2 -15 0 38.40 6.80 2 -15 0 37.80 8.80 2 -15 0 39.60 9.80 2 -15 0 39.50 7.30 2 -15 0 31.90 7.00 2 -15 0 26.20 5.80 2 -15 0 21.00 10.00 2 -15 0 20.80 8.50 2 -15 0 39.50 7.30 2 -15 0 64.59 12.20 2 -15 0 30.90 10.70 -2 15 0 41.70 10.00 -2 15 0 36.60 10.10 -2 15 0 40.30 8.80 -2 15 0 20.30 5.20 -2 15 0 29.30 6.60 -2 15 0 31.80 9.70 -2 15 0 27.80 5.70 -2 15 0 35.00 7.50 -2 15 0 30.20 7.00 -2 15 0 23.80 7.90 1 -15 0 43.60 7.40 1 -15 0 58.79 13.30 1 -15 0 49.80 9.00 1 -15 0 63.09 9.10 1 -15 0 57.39 13.50 1 -15 0 54.09 11.10 1 -15 0 45.70 10.70 1 -15 0 57.69 11.10 1 -15 0 51.29 7.80 1 -15 0 54.39 10.40 1 -15 0 62.09 7.90 1 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15 0 9.50 6.80 1 15 0 14.70 4.20 1 15 0 14.70 6.70 1 15 0 12.70 8.40 1 15 0 14.20 4.40 1 15 0 19.60 5.60 -2 -15 0 7.30 7.30 -2 -15 0 5.00 4.60 -2 -15 0 5.70 3.40 -2 -15 0 8.90 3.30 -2 -15 0 20.10 8.80 -2 -15 0 9.60 4.20 -2 -15 0 13.80 7.20 -2 -15 0 8.10 3.30 -2 -15 0 4.80 2.70 -2 -15 0 3.20 7.40 2 15 0 13.00 7.50 2 15 0 8.00 3.70 2 15 0 5.50 7.30 2 15 0 9.10 3.70 2 15 0 14.90 5.90 2 15 0 4.00 4.80 2 15 0 6.20 5.60 2 15 0 8.90 3.80 2 15 0 11.70 3.80 2 15 0 9.50 7.70 -3 -15 0 9.90 4.00 -3 -15 0 9.50 3.40 -3 -15 0 9.80 6.20 -3 -15 0 8.50 3.10 -3 -15 0 19.50 8.60 -3 -15 0 8.30 7.20 -3 -15 0 9.10 5.70 -3 -15 0 21.90 8.00 -3 -15 0 8.70 3.80 -3 -15 0 10.90 3.90 3 15 0 8.80 3.20 3 15 0 6.50 3.30 3 15 0 10.80 3.60 3 15 0 16.90 6.10 3 15 0 13.30 6.70 3 15 0 5.70 3.00 3 15 0 15.10 5.50 3 15 0 18.80 8.90 3 15 0 17.80 6.80 3 15 0 19.10 7.60 3 15 0 9.40 4.10 3 15 0 12.70 8.10 3 15 0 20.30 8.60 -4 -15 0 -2.40 6.10 -4 -15 0 0.10 1.30 -4 -15 0 2.60 5.30 -4 -15 0 -0.80 1.00 -4 -15 0 0.40 5.90 -4 -15 0 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4 -10 2.90 1.70 -2 4 -10 1.50 2.30 -2 4 -10 5.00 2.50 2 -4 10 5.70 3.90 2 -4 10 2.80 2.40 2 -4 10 2.70 3.20 2 -4 10 0.80 4.40 2 -4 10 4.70 1.80 2 -4 10 3.50 1.90 2 -4 10 1.20 1.10 2 -4 10 8.30 4.40 2 -4 10 -0.40 1.30 2 -4 10 -2.30 4.60 -3 4 -10 21.80 3.60 -3 4 -10 27.80 4.70 -3 4 -10 14.40 4.40 -3 4 -10 32.00 6.00 -3 4 -10 36.80 6.00 -3 4 -10 18.10 4.10 -3 4 -10 24.30 3.40 -3 4 -10 28.90 6.10 -3 4 -10 28.30 5.10 -3 4 -10 29.70 4.70 3 -4 10 28.60 7.70 3 -4 10 36.30 8.60 3 -4 10 25.20 4.80 3 -4 10 25.10 4.30 3 -4 10 13.30 4.50 3 -4 10 34.40 6.40 3 -4 10 36.30 8.50 3 -4 10 24.80 5.90 3 -4 10 27.90 6.40 3 -4 10 23.50 4.10 3 -4 10 23.20 3.60 3 -4 10 26.40 5.40 -4 4 -10 27.10 5.80 -4 4 -10 32.60 6.30 -4 4 -10 33.40 5.90 -4 4 -10 27.80 5.00 -4 4 -10 47.80 5.60 -4 4 -10 29.80 5.10 -4 4 -10 43.00 6.60 -4 4 -10 46.20 5.50 4 -4 10 34.40 6.60 4 -4 10 38.60 5.00 4 -4 10 34.30 5.10 4 -4 10 40.70 8.50 4 -4 10 27.00 5.10 4 -4 10 38.70 7.10 4 -4 10 32.30 6.10 4 -4 10 41.20 9.50 4 -4 10 40.30 4.60 4 -4 10 29.80 7.00 4 -4 10 41.60 6.90 4 -4 10 37.20 7.40 -5 4 -10 461.55 19.60 -5 4 -10 457.85 19.30 -5 4 -10 482.35 21.00 -5 4 -10 496.45 20.00 -5 4 -10 458.75 16.40 -5 4 -10 454.15 16.70 -5 4 -10 469.65 17.10 -5 4 -10 458.45 13.90 -5 4 -10 494.05 15.10 -5 4 -10 491.15 19.30 -5 4 -10 475.55 20.90 -5 4 -10 435.26 21.20 5 -4 10 481.95 16.80 5 -4 10 472.15 19.40 5 -4 10 454.15 24.30 5 -4 10 456.75 21.40 5 -4 10 451.35 24.10 5 -4 10 454.75 21.80 5 -4 10 485.35 28.10 5 -4 10 483.65 19.30 5 -4 10 455.75 24.00 5 -4 10 444.36 22.00 -6 4 -10 103.09 7.50 -6 4 -10 114.29 10.80 -6 4 -10 102.79 9.00 -6 4 -10 90.99 8.90 -6 4 -10 95.39 7.30 -6 4 -10 106.29 10.00 -6 4 -10 102.59 6.20 -6 4 -10 106.89 7.10 -6 4 -10 108.29 7.10 -6 4 -10 103.49 8.40 6 -4 10 115.19 9.60 6 -4 10 101.89 9.70 6 -4 10 97.59 6.40 6 -4 10 104.09 6.70 6 -4 10 99.79 9.50 6 -4 10 91.39 13.10 6 -4 10 114.69 12.10 6 -4 10 102.19 8.70 6 -4 10 79.79 11.60 6 -4 10 109.49 12.10 6 -4 10 109.89 8.90 6 -4 10 124.89 14.70 -7 4 -10 143.29 12.00 -7 4 -10 154.68 8.90 -7 4 -10 150.88 10.00 -7 4 -10 156.88 11.10 -7 4 -10 144.99 8.60 -7 4 -10 167.38 13.00 -7 4 -10 153.08 10.20 -7 4 -10 180.48 10.70 -7 4 -10 159.68 9.00 -7 4 -10 162.08 11.50 7 -4 10 154.78 10.60 7 -4 10 163.58 14.50 7 -4 10 157.88 8.40 7 -4 10 161.38 12.70 7 -4 10 158.88 8.30 7 -4 10 161.48 15.00 7 -4 10 157.38 14.30 7 -4 10 137.09 15.10 7 -4 10 154.28 11.70 7 -4 10 139.29 11.20 7 -4 10 173.98 11.00 7 -4 10 181.78 17.80 -8 4 -10 64.69 8.60 -8 4 -10 47.20 6.30 -8 4 -10 46.50 7.50 -8 4 -10 47.90 6.80 -8 4 -10 44.70 8.00 -8 4 -10 58.09 8.70 -8 4 -10 58.69 6.60 -8 4 -10 36.20 6.00 -8 4 -10 53.29 10.10 -8 4 -10 40.20 5.20 8 -4 10 40.40 6.10 8 -4 10 44.20 8.70 8 -4 10 47.80 5.10 8 -4 10 56.99 12.20 8 -4 10 49.50 8.30 8 -4 10 53.99 11.30 8 -4 10 64.19 10.80 8 -4 10 45.90 10.00 8 -4 10 41.60 5.10 8 -4 10 41.00 7.00 8 -4 10 50.09 8.10 8 -4 10 51.29 11.20 -9 4 -10 67.39 10.00 -9 4 -10 65.99 6.90 -9 4 -10 51.79 7.70 -9 4 -10 65.99 8.90 -9 4 -10 74.89 7.80 -9 4 -10 60.09 7.30 -9 4 -10 58.09 9.70 -9 4 -10 61.49 7.80 9 -4 10 63.19 5.00 9 -4 10 43.70 9.40 9 -4 10 63.59 5.30 9 -4 10 49.99 8.60 9 -4 10 46.00 8.50 9 -4 10 68.99 12.30 9 -4 10 64.09 13.10 9 -4 10 54.29 8.30 9 -4 10 70.19 8.00 9 -4 10 70.79 12.40 -10 4 -10 163.48 9.50 -10 4 -10 173.78 12.10 -10 4 -10 158.38 11.90 -10 4 -10 169.68 25.30 -10 4 -10 187.68 19.60 -10 4 -10 155.08 16.60 -10 4 -10 165.88 12.20 -10 4 -10 187.58 14.60 -10 4 -10 157.88 13.10 -10 4 -10 168.08 9.70 10 -4 10 197.88 16.50 10 -4 10 165.78 11.30 10 -4 10 205.48 20.40 10 -4 10 165.18 14.50 10 -4 10 184.48 17.90 10 -4 10 175.18 9.20 10 -4 10 186.68 13.50 10 -4 10 177.88 8.50 -11 4 -10 203.78 12.30 -11 4 -10 236.78 15.30 -11 4 -10 221.88 14.70 -11 4 -10 202.98 12.40 -11 4 -10 222.48 11.70 -11 4 -10 213.78 19.10 -11 4 -10 222.68 15.90 -11 4 -10 214.48 10.50 -11 4 -10 193.98 19.60 -11 4 -10 234.78 17.30 11 -4 10 216.28 9.40 11 -4 10 233.68 21.10 11 -4 10 214.58 17.70 11 -4 10 256.67 18.60 11 -4 10 259.97 23.60 11 -4 10 204.58 12.40 -12 4 -10 52.19 13.10 -12 4 -10 32.70 5.80 -12 4 -10 47.40 9.00 -12 4 -10 39.60 7.10 -12 4 -10 41.80 10.10 -12 4 -10 43.50 8.20 -12 4 -10 53.99 11.40 -12 4 -10 39.00 3.90 -12 4 -10 34.90 3.40 -12 4 -10 33.90 5.40 12 -4 10 39.30 12.80 12 -4 10 39.90 9.80 12 -4 10 45.10 5.00 12 -4 10 43.50 10.50 12 -4 10 47.50 13.30 12 -4 10 33.80 8.30 12 -4 10 47.80 3.90 12 -4 10 42.80 7.00 10 3 -10 18.10 5.60 10 3 -10 24.10 10.20 10 3 -10 28.20 5.80 10 3 -10 12.90 17.80 10 3 -10 23.20 9.50 10 3 -10 22.80 6.30 10 3 -10 18.90 6.30 10 3 -10 47.70 17.40 10 3 -10 16.40 8.00 10 3 -10 28.20 8.60 -10 -3 10 39.70 8.50 -10 -3 10 25.00 6.40 -10 -3 10 27.00 9.10 -10 -3 10 46.80 11.80 -10 -3 10 27.60 7.30 -10 -3 10 37.50 12.40 -10 -3 10 25.10 16.20 -10 -3 10 23.70 7.00 -10 -3 10 25.60 5.80 -10 -3 10 -1.30 17.00 9 3 -10 12.40 12.00 9 3 -10 0.50 1.50 9 3 -10 3.30 3.60 9 3 -10 5.90 5.90 9 3 -10 2.10 11.90 9 3 -10 0.60 2.60 9 3 -10 4.60 7.20 9 3 -10 5.90 7.10 9 3 -10 1.20 1.90 9 3 -10 2.30 1.80 -9 -3 10 -5.20 15.40 -9 -3 10 1.10 1.50 -9 -3 10 0.70 6.10 -9 -3 10 17.10 12.20 -9 -3 10 6.20 5.40 -9 -3 10 4.70 4.30 -9 -3 10 3.20 1.70 -9 -3 10 -5.20 6.30 -9 -3 10 4.60 9.00 -9 -3 10 2.80 1.90 -9 -3 10 4.50 3.20 -9 -3 10 0.70 1.70 8 3 -10 32.40 6.90 8 3 -10 28.70 10.60 8 3 -10 36.70 8.30 8 3 -10 11.50 18.50 8 3 -10 36.10 6.20 8 3 -10 33.20 7.90 8 3 -10 33.60 12.10 8 3 -10 24.70 7.80 8 3 -10 35.10 9.40 8 3 -10 15.80 5.60 -8 -3 10 34.60 4.90 -8 -3 10 42.80 8.40 -8 -3 10 35.10 7.10 -8 -3 10 49.90 8.50 -8 -3 10 38.50 8.00 -8 -3 10 47.60 8.60 -8 -3 10 42.10 11.50 -8 -3 10 26.40 12.80 -8 -3 10 39.50 14.10 -8 -3 10 40.90 5.80 -8 -3 10 33.50 7.20 -8 -3 10 36.50 8.20 7 3 -10 14.70 10.50 7 3 -10 32.30 9.30 7 3 -10 20.60 6.10 7 3 -10 33.90 10.90 7 3 -10 35.10 7.70 7 3 -10 34.40 8.20 7 3 -10 28.80 6.40 7 3 -10 28.60 9.10 7 3 -10 21.70 5.80 7 3 -10 37.50 9.80 -7 -3 10 27.80 5.80 -7 -3 10 20.90 3.50 -7 -3 10 28.90 9.90 -7 -3 10 35.50 6.40 -7 -3 10 33.30 6.50 -7 -3 10 28.10 6.70 -7 -3 10 30.00 6.90 -7 -3 10 40.80 11.80 -7 -3 10 30.40 4.70 -7 -3 10 29.70 7.10 6 3 -10 42.60 9.20 6 3 -10 26.50 6.30 6 3 -10 30.60 7.30 6 3 -10 42.00 7.40 6 3 -10 41.20 7.80 6 3 -10 34.70 11.10 6 3 -10 42.30 8.70 6 3 -10 28.20 9.80 6 3 -10 38.60 7.60 6 3 -10 28.70 5.30 -6 -3 10 37.70 4.90 -6 -3 10 39.40 4.50 -6 -3 10 47.50 6.90 -6 -3 10 41.30 7.40 -6 -3 10 33.40 6.30 -6 -3 10 36.40 5.70 -6 -3 10 32.20 6.80 -6 -3 10 36.70 9.60 -6 -3 10 32.80 10.00 -6 -3 10 31.20 6.80 -6 -3 10 40.20 9.80 -6 -3 10 38.70 6.80 -6 -3 10 31.40 8.50 -6 -3 10 53.89 9.40 5 3 -10 5.90 2.90 5 3 -10 0.00 4.20 5 3 -10 6.90 6.60 5 3 -10 2.40 2.50 5 3 -10 0.20 6.30 5 3 -10 3.30 2.60 5 3 -10 0.10 4.50 5 3 -10 5.00 3.10 5 3 -10 12.10 5.60 -5 -3 10 3.10 2.30 -5 -3 10 5.70 2.60 -5 -3 10 1.80 2.40 -5 -3 10 6.40 3.20 -5 -3 10 5.10 1.50 -5 -3 10 1.10 3.20 -5 -3 10 2.60 5.10 -5 -3 10 2.80 2.70 -5 -3 10 4.60 3.80 -5 -3 10 5.30 2.50 -5 -3 10 4.30 1.60 -5 -3 10 -0.20 6.40 -5 -3 10 -0.60 5.60 -5 -3 10 9.90 6.60 4 3 -10 49.50 7.90 4 3 -10 31.60 6.50 4 3 -10 52.79 9.90 4 3 -10 38.70 7.20 4 3 -10 28.00 8.10 4 3 -10 30.20 5.90 4 3 -10 38.00 11.10 4 3 -10 40.60 7.30 4 3 -10 26.20 8.30 -4 -3 10 42.10 5.40 -4 -3 10 37.20 2.90 -4 -3 10 43.40 9.30 -4 -3 10 48.50 8.00 -4 -3 10 43.60 8.50 -4 -3 10 31.10 7.90 -4 -3 10 26.80 6.30 -4 -3 10 39.50 7.00 -4 -3 10 34.60 5.90 -4 -3 10 58.29 7.70 -4 -3 10 35.30 4.30 -4 -3 10 41.90 4.50 -4 -3 10 31.70 8.00 -4 -3 10 44.80 5.50 3 3 -10 23.30 6.60 3 3 -10 45.30 7.40 3 3 -10 31.50 5.80 3 3 -10 30.60 5.70 3 3 -10 38.30 7.00 3 3 -10 32.30 6.00 3 3 -10 31.10 6.20 3 3 -10 28.00 7.40 3 3 -10 25.10 5.80 3 3 -10 32.50 5.70 -3 -3 10 44.80 8.40 -3 -3 10 38.10 2.60 -3 -3 10 36.80 9.20 -3 -3 10 39.40 7.40 -3 -3 10 33.50 8.10 -3 -3 10 49.60 8.40 -3 -3 10 35.30 3.30 -3 -3 10 34.00 6.20 -3 -3 10 36.20 5.60 -3 -3 10 36.30 5.10 -3 -3 10 36.00 3.60 -3 -3 10 36.60 8.40 2 3 -10 3.10 3.20 2 3 -10 1.10 1.70 2 3 -10 5.50 2.70 2 3 -10 5.70 2.50 2 3 -10 1.80 3.50 2 3 -10 1.80 1.80 2 3 -10 2.10 4.10 2 3 -10 7.40 3.10 2 3 -10 2.10 3.50 2 3 -10 8.00 4.60 -2 -3 10 4.60 1.20 -2 -3 10 3.30 2.90 -2 -3 10 7.70 1.40 -2 -3 10 5.60 2.30 -2 -3 10 -3.20 4.10 -2 -3 10 8.70 4.70 -2 -3 10 0.50 1.50 -2 -3 10 3.80 2.60 -2 -3 10 4.20 3.70 -2 -3 10 0.60 1.20 -2 -3 10 6.40 5.10 -2 -3 10 7.10 2.00 1 3 -10 155.58 9.80 1 3 -10 154.68 12.00 1 3 -10 148.49 12.30 1 3 -10 162.48 10.30 1 3 -10 146.09 9.80 1 3 -10 144.49 7.40 1 3 -10 150.98 10.80 1 3 -10 147.79 9.40 1 3 -10 159.88 6.40 1 3 -10 165.48 12.90 -1 -3 10 147.99 14.00 -1 -3 10 148.09 5.70 -1 -3 10 145.29 6.70 -1 -3 10 156.38 9.10 -1 -3 10 139.09 11.60 -1 -3 10 137.79 12.40 -1 -3 10 152.98 10.20 -1 -3 10 166.28 11.30 -1 -3 10 143.49 11.90 -1 -3 10 168.08 14.50 0 3 -10 274.87 13.30 0 3 -10 279.87 15.00 0 3 -10 283.47 15.40 0 3 -10 272.07 13.30 0 3 -10 260.37 15.90 0 3 -10 284.77 13.00 0 3 -10 272.97 10.60 0 3 -10 277.07 9.20 0 3 -10 304.47 13.80 0 3 -10 244.48 15.80 0 -3 10 287.27 10.60 0 -3 10 268.07 15.80 0 -3 10 283.47 13.60 0 -3 10 277.57 19.30 0 -3 10 278.27 16.50 0 -3 10 254.57 16.30 0 -3 10 273.07 18.30 0 -3 10 283.87 9.20 -1 3 -10 111.19 7.90 -1 3 -10 127.59 6.80 -1 3 -10 108.69 10.00 -1 3 -10 121.29 8.60 -1 3 -10 104.89 8.90 -1 3 -10 115.09 7.50 -1 3 -10 112.79 10.90 -1 3 -10 106.39 7.70 -1 3 -10 124.09 9.90 -1 3 -10 107.89 5.30 1 -3 10 124.99 10.50 1 -3 10 115.99 10.80 1 -3 10 119.99 12.10 1 -3 10 118.29 7.10 1 -3 10 108.69 12.30 1 -3 10 123.49 10.60 1 -3 10 115.19 8.00 1 -3 10 114.29 8.70 -2 3 -10 170.68 10.40 -2 3 -10 182.38 13.50 -2 3 -10 201.18 11.00 -2 3 -10 190.28 11.40 -2 3 -10 192.38 10.00 -2 3 -10 186.68 7.50 -2 3 -10 176.98 11.50 -2 3 -10 174.58 11.70 -2 3 -10 176.98 8.80 -2 3 -10 177.18 9.10 2 -3 10 174.18 14.20 2 -3 10 173.58 15.60 2 -3 10 171.28 9.80 2 -3 10 171.68 13.40 2 -3 10 168.78 8.30 2 -3 10 192.68 10.00 2 -3 10 178.98 10.30 2 -3 10 166.18 12.30 2 -3 10 178.28 8.30 2 -3 10 181.88 11.80 -3 3 -10 90.59 6.70 -3 3 -10 84.29 7.80 -3 3 -10 103.19 5.80 -3 3 -10 96.49 8.50 -3 3 -10 98.19 10.30 -3 3 -10 100.69 7.90 -3 3 -10 89.19 6.40 -3 3 -10 92.99 8.00 -3 3 -10 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6 -6 14 32.50 9.00 6 -6 14 67.89 15.00 -7 6 -14 55.39 11.60 -7 6 -14 66.09 12.60 -7 6 -14 56.49 9.80 -7 6 -14 75.59 11.80 -7 6 -14 83.99 9.40 -7 6 -14 83.69 7.50 -7 6 -14 69.99 10.90 -7 6 -14 61.59 8.90 7 -6 14 72.59 11.80 7 -6 14 83.79 19.20 7 -6 14 85.79 7.30 7 -6 14 48.20 13.40 7 -6 14 98.79 16.70 7 -6 14 88.59 11.60 7 -6 14 74.39 12.50 7 -6 14 92.89 7.00 7 -6 14 70.99 14.80 7 -6 14 61.19 12.50 7 -6 14 76.69 11.30 7 -6 14 75.29 10.10 -8 6 -14 67.09 11.90 -8 6 -14 41.00 8.20 -8 6 -14 57.39 8.10 -8 6 -14 45.70 10.40 -8 6 -14 71.39 9.90 -8 6 -14 53.79 12.50 -8 6 -14 51.19 7.30 -8 6 -14 42.80 11.60 8 -6 14 77.59 18.10 8 -6 14 64.49 6.80 8 -6 14 72.09 10.40 8 -6 14 64.59 14.60 8 -6 14 48.40 14.40 8 -6 14 63.19 10.90 8 -6 14 26.60 14.40 8 -6 14 78.59 13.20 8 -6 14 58.09 10.30 8 -6 14 77.39 14.00 8 -6 14 61.69 8.70 8 -6 14 53.89 12.40 6 5 -14 9.40 4.70 6 5 -14 5.60 3.10 6 5 -14 -2.50 15.30 6 5 -14 2.00 3.00 6 5 -14 6.20 4.00 6 5 -14 5.40 3.70 6 5 -14 20.10 9.30 6 5 -14 1.90 16.30 6 5 -14 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-7 -9 -20 155.38 16.70 -7 -9 -20 156.58 7.50 -7 -9 -20 141.59 8.50 7 9 20 170.28 13.90 7 9 20 147.29 16.30 -8 -9 -20 52.89 6.80 -8 -9 -20 50.69 5.80 -8 -9 -20 38.30 8.10 -8 -9 -20 44.20 2.80 -8 -9 -20 55.29 9.40 -8 -9 -20 43.80 4.50 -8 -9 -20 36.60 6.70 -8 -9 -20 43.40 10.20 -8 -9 -20 33.80 8.30 -8 -9 -20 47.60 5.70 -8 -9 -20 27.50 11.00 8 9 20 45.80 12.40 8 9 20 59.39 10.70 -3 -10 -20 104.29 13.50 -3 -10 -20 94.19 10.10 -3 -10 -20 106.49 15.50 -3 -10 -20 112.99 15.50 -3 -10 -20 110.09 16.80 -3 -10 -20 80.49 16.30 3 10 20 141.89 18.80 3 10 20 102.59 13.90 3 10 20 119.79 12.10 3 10 20 104.79 6.80 -4 -10 -20 140.49 22.70 -4 -10 -20 116.39 14.60 -4 -10 -20 141.19 18.20 -4 -10 -20 126.89 9.30 -4 -10 -20 144.29 18.80 -4 -10 -20 143.89 12.70 4 10 20 135.99 6.40 4 10 20 143.39 9.90 4 10 20 152.38 13.40 4 10 20 145.89 6.90 4 10 20 141.79 16.10 4 10 20 151.38 11.00 -5 -10 -20 104.09 7.70 -5 -10 -20 113.19 11.10 -5 -10 -20 104.49 15.70 -5 -10 -20 98.19 13.00 -5 -10 -20 126.29 20.70 -5 -10 -20 87.89 14.80 5 10 20 70.69 13.30 5 10 20 106.19 13.60 -6 -10 -20 185.58 17.40 -6 -10 -20 215.68 15.10 -6 -10 -20 223.88 25.30 -6 -10 -20 212.68 22.00 -6 -10 -20 207.38 14.80 -6 -10 -20 198.98 12.10 -6 -10 -20 199.78 9.80 -6 -10 -20 204.18 18.10 -6 -10 -20 194.78 8.50 -6 -10 -20 176.18 13.60 6 10 20 183.88 14.90 6 10 20 206.48 19.00 -7 -10 -20 209.28 13.20 -7 -10 -20 201.18 17.90 -7 -10 -20 171.08 16.20 -7 -10 -20 197.58 17.80 -7 -10 -20 213.48 9.10 -7 -10 -20 211.88 11.20 -7 -10 -20 206.88 9.60 -7 -10 -20 208.38 24.90 -7 -10 -20 195.68 14.30 -7 -10 -20 180.98 13.50 7 10 20 176.98 15.00 7 10 20 183.68 18.40 -5 -11 -20 133.49 14.40 -5 -11 -20 112.69 11.70 -5 -11 -20 88.99 9.80 -5 -11 -20 117.19 8.40 -5 -11 -20 114.09 7.10 -5 -11 -20 165.78 16.70 -5 -11 -20 124.29 20.90 -5 -11 -20 134.49 18.00 -5 -11 -20 142.99 12.10 -5 -11 -20 114.99 6.20 -6 -11 -20 127.69 14.80 -6 -11 -20 120.29 11.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 35091 _chemical_properties_physical Moisture-sensitive ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p-1_a_CCDC1 _database_code_depnum_ccdc_archive 'CCDC 2150925' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-08 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C2.76 H0.19 Al0.10 F3.81 O1.05 Os0.14' _chemical_formula_moiety '2(C16 Al F36 O4), C14 O14 Os3, 2(C6 H2 F4)' _chemical_formula_weight 152.25 _chemical_melting_point ? _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.283(3) _cell_length_b 14.143(3) _cell_length_c 15.714(3) _cell_angle_alpha 71.674(9) _cell_angle_beta 71.730(7) _cell_angle_gamma 73.486(9) _cell_volume 2211.8(8) _cell_formula_units_Z 21 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 3311 _cell_measurement_theta_min 2.666 _cell_measurement_theta_max 28.4575 _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.400 _exptl_crystal_F_000 1502 _exptl_crystal_size_max 0.252 _exptl_crystal_size_mid 0.081 _exptl_crystal_size_min 0.029 _exptl_absorpt_coefficient_mu 4.556 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.558513 _exptl_absorpt_correction_T_max 0.74607 _exptl_absorpt_process_details ; TWINABS - Bruker AXS scaling for twinned crystals - Version 2012/1: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min 0.393 _shelx_estimated_absorpt_T_max 0.879 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 13532 _diffrn_reflns_av_unetI/netI 0.0526 _diffrn_reflns_av_R_equivalents 0.0544 _diffrn_reflns_theta_min 1.408 _diffrn_reflns_theta_max 30.650 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 22 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 13532 _reflns_number_gt 10982 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS V6.2.14 Patch 4/2020-11-09' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+16.6006P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_number_reflns 13532 _refine_ls_number_parameters 745 _refine_ls_number_restraints 3053 _refine_ls_R_factor_all 0.0604 _refine_ls_R_factor_gt 0.0411 _refine_ls_wR_factor_ref 0.0713 _refine_ls_wR_factor_gt 0.0665 _refine_ls_goodness_of_fit_ref 1.000 _refine_ls_restrained_S_all 0.915 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 1.193 _refine_diff_density_min -2.394 _refine_diff_density_rms 0.189 _refine_ls_extinction_method none _refine_ls_extinction_coef . _twin_special_details 'The data was integrated as a 2-component twin.' _twin_individual_id 2 _twin_individual_twin_matrix_11 6e-05 _twin_individual_twin_matrix_12 0.00047 _twin_individual_twin_matrix_13 -1.00023 _twin_individual_twin_matrix_21 0.99952 _twin_individual_twin_matrix_22 -0.45124 _twin_individual_twin_matrix_23 -0.51557 _twin_individual_twin_matrix_31 -0.00218 _twin_individual_twin_matrix_32 -0.9993 _twin_individual_twin_matrix_33 -0.00038 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Os1 Os 1.03273(2) 0.14629(2) 0.32050(2) 0.01178(4) Uani 1 1 d . . . . . Os2 Os 1.000000 0.000000 0.500000 0.01148(5) Uani 1 2 d S . P . . Al1 Al 0.23056(11) 0.29558(9) 0.77718(8) 0.0116(2) Uani 1 1 d . . . . . O1 O 1.0501(3) 0.3104(2) 0.1347(2) 0.0212(7) Uani 1 1 d . . . . . O2 O 0.9240(3) 0.0016(2) 0.2651(2) 0.0216(6) Uani 1 1 d . . . . . O3 O 1.3039(3) 0.0188(3) 0.2583(2) 0.0295(8) Uani 1 1 d . . . . . O4 O 1.1365(3) 0.2642(3) 0.4084(2) 0.0272(7) Uani 1 1 d . . . . . O5 O 0.7664(3) 0.2565(3) 0.4123(2) 0.0251(7) Uani 1 1 d . . . . . O6 O 1.2719(3) 0.0041(2) 0.5013(2) 0.0212(6) Uani 1 1 d . . . . . O7 O 0.8929(3) 0.1745(3) 0.5987(2) 0.0271(7) Uani 1 1 d . . . . . C1 C 1.0456(4) 0.2500(3) 0.2009(3) 0.0131(7) Uani 1 1 d . . . . . C2 C 0.9611(4) 0.0560(3) 0.2835(3) 0.0152(8) Uani 1 1 d . . . . . C3 C 1.2062(4) 0.0656(3) 0.2806(3) 0.0174(8) Uani 1 1 d . . . . . C4 C 1.1016(4) 0.2214(3) 0.3749(3) 0.0174(8) Uani 1 1 d . . . . . C5 C 0.8605(4) 0.2158(3) 0.3767(3) 0.0163(8) Uani 1 1 d . . . . . C6 C 1.1726(4) 0.0021(3) 0.5012(3) 0.0143(8) Uani 1 1 d . . . . . C7 C 0.9315(4) 0.1105(3) 0.5626(3) 0.0172(8) Uani 1 1 d . . . . . O1_1 O 0.3089(3) 0.3557(2) 0.8162(2) 0.0159(6) Uani 1 1 d D U . . . C1_1 C 0.3224(3) 0.4440(3) 0.8245(3) 0.0139(7) Uani 1 1 d D U . . . C2_1 C 0.4639(4) 0.4315(3) 0.8264(3) 0.0174(8) Uani 1 1 d D U . . . F1_1 F 0.5402(2) 0.4373(2) 0.74189(19) 0.0263(6) Uani 1 1 d D U . . . F2_1 F 0.4780(3) 0.5027(2) 0.8594(2) 0.0259(6) Uani 1 1 d D U . . . F3_1 F 0.5036(3) 0.3414(2) 0.87945(19) 0.0248(6) Uani 1 1 d D U . . . C3_1 C 0.2312(4) 0.4696(3) 0.9154(3) 0.0163(8) Uani 1 1 d D U . . . F4_1 F 0.1172(2) 0.4507(2) 0.92832(18) 0.0218(5) Uani 1 1 d D U . . . F5_1 F 0.2761(3) 0.4131(2) 0.98893(17) 0.0223(5) Uani 1 1 d D U . . . F6_1 F 0.2143(3) 0.56734(18) 0.91498(18) 0.0218(5) Uani 1 1 d D U . . . C4_1 C 0.2936(4) 0.5340(3) 0.7414(3) 0.0165(8) Uani 1 1 d D U . . . F7_1 F 0.1676(2) 0.56742(19) 0.75041(18) 0.0221(5) Uani 1 1 d D U . . . F8_1 F 0.3420(3) 0.61349(19) 0.73273(18) 0.0225(5) Uani 1 1 d D U . . . F9_1 F 0.3412(3) 0.5056(2) 0.66230(17) 0.0228(6) Uani 1 1 d D U . . . O1_2 O 0.2402(3) 0.1725(2) 0.84547(19) 0.0144(6) Uani 1 1 d D U . . . C1_2 C 0.2350(4) 0.1123(3) 0.9318(3) 0.0149(7) Uani 1 1 d D U . . . C2_2 C 0.0980(4) 0.1368(3) 0.9942(3) 0.0190(8) Uani 1 1 d D U . . . F1_2 F 0.0160(2) 0.1011(2) 0.9739(2) 0.0262(6) Uani 1 1 d D U . . . F2_2 F 0.0935(3) 0.0956(2) 1.08480(18) 0.0281(6) Uani 1 1 d D U . . . F3_2 F 0.0562(2) 0.23619(19) 0.98280(18) 0.0218(5) Uani 1 1 d D U . . . C3_2 C 0.3322(4) 0.1263(3) 0.9764(3) 0.0188(8) Uani 1 1 d D U . . . F4_2 F 0.4424(2) 0.1357(2) 0.91451(18) 0.0224(5) Uani 1 1 d D U . . . F5_2 F 0.2888(3) 0.2100(2) 1.00864(18) 0.0238(6) Uani 1 1 d D U . . . F6_2 F 0.3554(3) 0.0479(2) 1.04751(18) 0.0263(6) Uani 1 1 d D U . . . C4_2 C 0.2667(4) -0.0003(3) 0.9255(3) 0.0216(9) Uani 1 1 d D U . . . F7_2 F 0.3918(3) -0.0289(2) 0.8893(2) 0.0265(6) Uani 1 1 d D U . . . F8_2 F 0.2351(3) -0.0651(2) 1.00710(19) 0.0269(6) Uani 1 1 d D U . . . F9_2 F 0.2060(3) -0.0100(2) 0.86933(19) 0.0242(6) Uani 1 1 d D U . . . O1_3 O 0.0768(3) 0.3647(2) 0.7806(2) 0.0169(6) Uani 1 1 d D U . . . C1_3 C -0.0290(4) 0.3895(3) 0.7492(3) 0.0181(8) Uani 1 1 d D U . . . C2_3 C -0.1246(4) 0.4735(3) 0.7954(3) 0.0232(9) Uani 1 1 d D U . . . F1_3 F -0.0879(3) 0.5629(2) 0.7563(2) 0.0350(7) Uani 1 1 d D U . . . F2_3 F -0.2429(3) 0.4876(2) 0.7873(2) 0.0336(7) Uani 1 1 d D U . . . F3_3 F -0.1285(3) 0.4508(2) 0.8844(2) 0.0329(7) Uani 1 1 d D U . . . C3_3 C -0.0910(4) 0.2969(3) 0.7757(3) 0.0248(9) Uani 1 1 d D U . . . F4_3 F -0.0033(3) 0.2148(2) 0.7590(2) 0.0370(7) Uani 1 1 d D U . . . F5_3 F -0.1479(3) 0.2741(2) 0.8663(2) 0.0356(7) Uani 1 1 d D U . . . F6_3 F -0.1796(3) 0.3110(2) 0.7303(2) 0.0346(7) Uani 1 1 d D U . . . C4_3 C 0.0008(4) 0.4321(4) 0.6420(3) 0.0272(10) Uani 1 1 d D U . . . F7_3 F 0.0504(3) 0.3561(3) 0.5996(2) 0.0403(8) Uani 1 1 d D U . . . F8_3 F -0.1037(3) 0.4867(3) 0.6127(2) 0.0398(8) Uani 1 1 d D U . . . F9_3 F 0.0847(3) 0.4914(3) 0.6141(2) 0.0403(8) Uani 1 1 d D U . . . O1_4 O 0.3006(3) 0.2901(2) 0.66343(19) 0.0164(6) Uani 1 1 d D U . . . C1_4 C 0.3990(4) 0.2439(3) 0.6050(3) 0.0161(8) Uani 1 1 d D U . . . C2_4 C 0.5281(4) 0.2338(3) 0.6267(3) 0.0197(8) Uani 1 1 d D U . . . F1_4 F 0.5662(3) 0.3213(2) 0.5965(2) 0.0272(6) Uani 1 1 d D U . . . F2_4 F 0.6221(2) 0.1653(2) 0.58781(18) 0.0248(6) Uani 1 1 d D U . . . F3_4 F 0.5178(3) 0.2022(2) 0.71749(17) 0.0265(6) Uani 1 1 d D U . . . C3_4 C 0.3808(4) 0.1366(3) 0.6121(3) 0.0252(9) Uani 1 1 d D U . . . F4_4 F 0.2584(3) 0.1391(2) 0.6198(2) 0.0372(8) Uani 1 1 d D U . . . F5_4 F 0.4130(3) 0.0693(2) 0.6866(2) 0.0356(7) Uani 1 1 d D U . . . F6_4 F 0.4507(3) 0.1005(2) 0.5386(2) 0.0315(7) Uani 1 1 d D U . . . C4_4 C 0.4001(4) 0.3115(4) 0.5053(3) 0.0226(9) Uani 1 1 d D U . . . F7_4 F 0.3036(3) 0.3041(3) 0.47744(19) 0.0346(7) Uani 1 1 d D U . . . F8_4 F 0.5078(3) 0.2840(2) 0.44394(17) 0.0295(6) Uani 1 1 d D U . . . F9_4 F 0.3871(3) 0.4086(2) 0.50163(19) 0.0318(7) Uani 1 1 d D U . . . F1_5 F 0.3105(2) 0.2501(2) 0.1948(2) 0.0290(6) Uani 1 1 d D U . . . F2_5 F 0.4101(3) 0.1514(2) 0.34138(18) 0.0294(6) Uani 1 1 d D U . . . F3_5 F 0.6633(3) 0.1330(2) 0.32529(18) 0.0277(6) Uani 1 1 d D U . . . F4_5 F 0.8137(2) 0.2126(2) 0.1627(2) 0.0259(6) Uani 1 1 d D U . . . C1_5 C 0.4369(4) 0.2416(3) 0.1841(3) 0.0199(8) Uani 1 1 d D U . . . C2_5 C 0.4858(4) 0.1914(3) 0.2604(3) 0.0196(8) Uani 1 1 d D U . . . C3_5 C 0.6134(4) 0.1821(3) 0.2520(3) 0.0178(8) Uani 1 1 d D U . . . C4_5 C 0.6889(4) 0.2222(3) 0.1682(3) 0.0168(8) Uani 1 1 d D U . . . C5_5 C 0.6406(4) 0.2722(3) 0.0920(3) 0.0190(8) Uani 1 1 d D U . . . H5_5 H 0.694348 0.299671 0.034619 0.023 Uiso 1 1 calc R U . . . C6_5 C 0.5120(4) 0.2820(3) 0.1006(3) 0.0218(9) Uani 1 1 d D U . . . H6_5 H 0.476297 0.316306 0.048972 0.026 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Os1 0.01149(7) 0.01206(7) 0.01110(7) -0.00190(6) -0.00320(5) -0.00200(5) Os2 0.01235(10) 0.01123(10) 0.01045(10) -0.00246(8) -0.00337(8) -0.00143(8) Al1 0.0114(5) 0.0109(5) 0.0119(5) -0.0037(4) -0.0024(4) -0.0011(4) O1 0.0262(17) 0.0164(16) 0.0178(16) 0.0008(13) -0.0045(13) -0.0061(13) O2 0.0290(17) 0.0208(16) 0.0188(15) -0.0037(13) -0.0091(13) -0.0088(13) O3 0.0248(18) 0.0283(19) 0.0271(18) -0.0043(15) -0.0048(14) 0.0026(14) O4 0.0304(18) 0.0267(18) 0.0318(19) -0.0085(15) -0.0142(15) -0.0085(14) O5 0.0162(15) 0.0268(18) 0.0214(16) 0.0002(14) -0.0007(13) 0.0008(13) O6 0.0175(15) 0.0226(16) 0.0241(16) -0.0066(13) -0.0052(12) -0.0040(12) O7 0.0310(18) 0.0263(18) 0.0262(17) -0.0142(14) -0.0086(14) 0.0007(14) C1 0.0182(19) 0.0085(17) 0.0118(18) -0.0020(15) -0.0028(14) -0.0032(14) C2 0.0165(19) 0.017(2) 0.0104(17) -0.0016(15) -0.0045(14) -0.0023(15) C3 0.021(2) 0.017(2) 0.0153(19) -0.0029(16) -0.0053(16) -0.0041(16) C4 0.0159(19) 0.016(2) 0.018(2) 0.0002(16) -0.0065(16) -0.0017(15) C5 0.0156(19) 0.020(2) 0.0126(18) 0.0001(16) -0.0052(15) -0.0045(16) C6 0.0171(19) 0.0117(18) 0.0107(17) -0.0015(14) 0.0002(14) -0.0031(14) C7 0.022(2) 0.016(2) 0.0115(18) -0.0016(15) -0.0038(15) -0.0031(16) O1_1 0.0180(14) 0.0130(14) 0.0182(15) -0.0052(11) -0.0056(11) -0.0026(11) C1_1 0.0129(17) 0.0120(17) 0.0170(18) -0.0051(14) -0.0033(14) -0.0015(13) C2_1 0.0157(18) 0.020(2) 0.0188(19) -0.0057(16) -0.0062(15) -0.0033(15) F1_1 0.0153(12) 0.0368(16) 0.0262(14) -0.0113(12) -0.0002(10) -0.0061(11) F2_1 0.0216(13) 0.0283(15) 0.0372(16) -0.0166(13) -0.0099(12) -0.0070(11) F3_1 0.0229(13) 0.0231(14) 0.0295(15) -0.0060(11) -0.0146(11) 0.0022(11) C3_1 0.0187(19) 0.0121(18) 0.0189(19) -0.0041(15) -0.0048(15) -0.0038(15) F4_1 0.0168(12) 0.0243(14) 0.0232(14) -0.0078(11) 0.0004(10) -0.0064(10) F5_1 0.0298(14) 0.0214(13) 0.0147(12) -0.0035(10) -0.0078(10) -0.0021(11) F6_1 0.0277(14) 0.0139(12) 0.0222(13) -0.0068(10) -0.0025(11) -0.0034(10) C4_1 0.0190(19) 0.0106(18) 0.0180(19) -0.0010(15) -0.0039(15) -0.0039(14) F7_1 0.0203(13) 0.0173(13) 0.0262(14) -0.0002(11) -0.0100(11) -0.0015(10) F8_1 0.0290(14) 0.0161(12) 0.0232(13) -0.0008(10) -0.0062(11) -0.0110(11) F9_1 0.0310(14) 0.0219(13) 0.0139(12) -0.0036(10) -0.0047(10) -0.0048(11) O1_2 0.0160(14) 0.0129(14) 0.0126(13) -0.0016(11) -0.0021(11) -0.0036(11) C1_2 0.0161(18) 0.0115(17) 0.0147(18) -0.0030(14) -0.0017(14) -0.0015(14) C2_2 0.020(2) 0.0173(19) 0.0171(19) -0.0043(16) 0.0014(15) -0.0070(15) F1_2 0.0196(13) 0.0257(14) 0.0332(15) -0.0063(12) -0.0021(11) -0.0104(11) F2_2 0.0322(15) 0.0265(15) 0.0160(12) -0.0024(11) 0.0012(11) -0.0023(12) F3_2 0.0226(13) 0.0160(12) 0.0214(13) -0.0050(10) -0.0017(10) 0.0005(10) C3_2 0.024(2) 0.0160(19) 0.0164(19) -0.0029(15) -0.0074(15) -0.0025(16) F4_2 0.0151(12) 0.0239(14) 0.0257(14) -0.0020(11) -0.0035(10) -0.0066(10) F5_2 0.0320(15) 0.0202(13) 0.0238(14) -0.0093(11) -0.0094(11) -0.0050(11) F6_2 0.0354(16) 0.0215(14) 0.0227(14) 0.0022(11) -0.0158(12) -0.0056(12) C4_2 0.026(2) 0.0155(19) 0.023(2) -0.0036(16) -0.0052(17) -0.0041(16) F7_2 0.0249(14) 0.0178(13) 0.0336(15) -0.0110(12) -0.0030(11) 0.0010(11) F8_2 0.0361(16) 0.0149(13) 0.0266(14) 0.0017(11) -0.0080(12) -0.0076(11) F9_2 0.0310(15) 0.0172(13) 0.0294(14) -0.0078(11) -0.0120(12) -0.0054(11) O1_3 0.0134(13) 0.0208(15) 0.0165(14) -0.0065(12) -0.0046(11) -0.0002(11) C1_3 0.0133(18) 0.022(2) 0.0190(19) -0.0075(16) -0.0044(15) 0.0003(15) C2_3 0.0140(19) 0.023(2) 0.034(2) -0.0126(19) -0.0078(17) 0.0026(16) F1_3 0.0292(16) 0.0196(14) 0.059(2) -0.0130(14) -0.0185(15) 0.0018(12) F2_3 0.0150(13) 0.0390(17) 0.0525(19) -0.0270(15) -0.0114(13) 0.0069(12) F3_3 0.0250(15) 0.0456(19) 0.0294(15) -0.0237(14) -0.0045(12) 0.0042(13) C3_3 0.021(2) 0.026(2) 0.031(2) -0.0134(19) -0.0066(18) -0.0039(17) F4_3 0.0306(16) 0.0232(15) 0.064(2) -0.0209(15) -0.0179(15) 0.0032(12) F5_3 0.0310(16) 0.0349(17) 0.0381(17) -0.0043(14) -0.0013(13) -0.0158(13) F6_3 0.0256(15) 0.0374(17) 0.053(2) -0.0221(15) -0.0176(14) -0.0035(13) C4_3 0.021(2) 0.037(3) 0.022(2) -0.0050(19) -0.0095(17) -0.0013(18) F7_3 0.0306(17) 0.065(2) 0.0286(16) -0.0264(16) -0.0098(13) 0.0052(15) F8_3 0.0302(16) 0.054(2) 0.0287(16) -0.0012(15) -0.0187(13) 0.0029(14) F9_3 0.0342(17) 0.052(2) 0.0259(16) 0.0099(14) -0.0091(13) -0.0156(15) O1_4 0.0136(13) 0.0197(15) 0.0129(13) -0.0063(12) -0.0010(11) 0.0013(11) C1_4 0.0147(18) 0.0196(19) 0.0157(18) -0.0081(15) -0.0025(14) -0.0033(15) C2_4 0.0179(19) 0.023(2) 0.0162(19) -0.0079(16) -0.0033(15) 0.0004(16) F1_4 0.0241(14) 0.0255(14) 0.0362(16) -0.0087(12) -0.0086(12) -0.0089(11) F2_4 0.0156(12) 0.0306(15) 0.0251(14) -0.0125(12) -0.0019(10) 0.0026(11) F3_4 0.0250(14) 0.0373(16) 0.0138(12) -0.0062(11) -0.0073(10) 0.0013(12) C3_4 0.021(2) 0.027(2) 0.026(2) -0.0162(18) 0.0065(17) -0.0067(18) F4_4 0.0219(14) 0.0414(18) 0.056(2) -0.0308(16) 0.0078(13) -0.0160(13) F5_4 0.0452(19) 0.0197(14) 0.0326(16) -0.0069(12) 0.0050(14) -0.0084(13) F6_4 0.0258(15) 0.0379(17) 0.0369(16) -0.0290(14) 0.0029(12) -0.0057(12) C4_4 0.0167(19) 0.038(2) 0.0131(18) -0.0084(18) -0.0009(15) -0.0060(18) F7_4 0.0190(14) 0.068(2) 0.0219(14) -0.0166(14) -0.0074(11) -0.0075(14) F8_4 0.0202(13) 0.0509(19) 0.0127(12) -0.0089(12) 0.0023(10) -0.0063(12) F9_4 0.0362(17) 0.0295(15) 0.0214(14) 0.0039(12) -0.0067(12) -0.0060(13) F1_5 0.0154(13) 0.0389(17) 0.0339(16) -0.0040(13) -0.0109(11) -0.0075(11) F2_5 0.0252(14) 0.0369(17) 0.0186(13) -0.0006(12) 0.0001(11) -0.0081(12) F3_5 0.0262(14) 0.0342(16) 0.0225(14) -0.0035(12) -0.0146(11) -0.0003(12) F4_5 0.0147(12) 0.0261(14) 0.0371(16) -0.0055(12) -0.0086(11) -0.0048(10) C1_5 0.0152(18) 0.021(2) 0.025(2) -0.0056(17) -0.0083(16) -0.0036(16) C2_5 0.0200(19) 0.024(2) 0.0134(18) -0.0034(16) -0.0031(15) -0.0050(17) C3_5 0.0209(19) 0.018(2) 0.0164(18) -0.0062(16) -0.0077(15) -0.0020(16) C4_5 0.0118(17) 0.0139(19) 0.025(2) -0.0062(16) -0.0047(15) -0.0009(14) C5_5 0.022(2) 0.017(2) 0.0165(19) -0.0035(16) -0.0023(16) -0.0059(16) C6_5 0.026(2) 0.020(2) 0.021(2) -0.0002(17) -0.0122(17) -0.0031(17) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Os1 C5 1.977(4) . ? Os1 C1 1.980(4) . ? Os1 C4 1.981(4) . ? Os1 C3 1.984(4) . ? Os1 C2 1.993(4) . ? Os1 Os2 2.9128(6) . ? Os2 C7 1.952(4) . ? Os2 C7 1.952(4) 2_756 ? Os2 C6 1.962(4) . ? Os2 C6 1.962(4) 2_756 ? Al1 O1_1 1.725(3) . ? Al1 O1_3 1.726(3) . ? Al1 O1_2 1.728(3) . ? Al1 O1_4 1.730(3) . ? O1 C1 1.117(5) . ? O2 C2 1.117(5) . ? O3 C3 1.125(5) . ? O4 C4 1.123(5) . ? O5 C5 1.119(5) . ? O6 C6 1.129(5) . ? O7 C7 1.129(5) . ? O1_1 C1_1 1.350(4) . ? C1_1 C4_1 1.554(5) . ? C1_1 C3_1 1.556(5) . ? C1_1 C2_1 1.564(5) . ? C2_1 F3_1 1.328(5) . ? C2_1 F1_1 1.329(5) . ? C2_1 F2_1 1.335(5) . ? C3_1 F4_1 1.328(4) . ? C3_1 F5_1 1.336(4) . ? C3_1 F6_1 1.339(4) . ? C4_1 F9_1 1.330(5) . ? C4_1 F8_1 1.337(4) . ? C4_1 F7_1 1.341(5) . ? O1_2 C1_2 1.349(5) . ? C1_2 C3_2 1.557(5) . ? C1_2 C4_2 1.558(5) . ? C1_2 C2_2 1.558(5) . ? C2_2 F3_2 1.323(5) . ? C2_2 F1_2 1.329(5) . ? C2_2 F2_2 1.348(5) . ? C3_2 F4_2 1.328(5) . ? C3_2 F6_2 1.337(5) . ? C3_2 F5_2 1.338(5) . ? C4_2 F8_2 1.331(5) . ? C4_2 F9_2 1.332(5) . ? C4_2 F7_2 1.340(5) . ? O1_3 C1_3 1.346(5) . ? C1_3 C3_3 1.541(6) . ? C1_3 C2_3 1.558(5) . ? C1_3 C4_3 1.560(6) . ? C2_3 F3_3 1.321(5) . ? C2_3 F2_3 1.333(5) . ? C2_3 F1_3 1.340(5) . ? C3_3 F4_3 1.331(5) . ? C3_3 F6_3 1.340(5) . ? C3_3 F5_3 1.341(5) . ? C4_3 F9_3 1.323(5) . ? C4_3 F7_3 1.337(5) . ? C4_3 F8_3 1.341(5) . ? O1_4 C1_4 1.353(5) . ? C1_4 C3_4 1.553(6) . ? C1_4 C4_4 1.555(5) . ? C1_4 C2_4 1.556(5) . ? C2_4 F1_4 1.322(5) . ? C2_4 F3_4 1.332(5) . ? C2_4 F2_4 1.348(5) . ? C3_4 F5_4 1.334(5) . ? C3_4 F6_4 1.338(5) . ? C3_4 F4_4 1.339(5) . ? C4_4 F9_4 1.323(5) . ? C4_4 F7_4 1.334(5) . ? C4_4 F8_4 1.338(5) . ? F1_5 C1_5 1.357(5) . ? F2_5 C2_5 1.345(5) . ? F3_5 C3_5 1.344(5) . ? F4_5 C4_5 1.353(4) . ? C1_5 C6_5 1.369(6) . ? C1_5 C2_5 1.378(5) . ? C2_5 C3_5 1.376(5) . ? C3_5 C4_5 1.373(5) . ? C4_5 C5_5 1.374(5) . ? C5_5 C6_5 1.385(6) . ? C5_5 H5_5 0.9500 . ? C6_5 H6_5 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C5 Os1 C1 93.78(16) . . ? C5 Os1 C4 87.42(17) . . ? C1 Os1 C4 93.24(16) . . ? C5 Os1 C3 172.55(17) . . ? C1 Os1 C3 93.49(17) . . ? C4 Os1 C3 90.51(17) . . ? C5 Os1 C2 91.81(17) . . ? C1 Os1 C2 95.09(16) . . ? C4 Os1 C2 171.66(17) . . ? C3 Os1 C2 89.21(17) . . ? C5 Os1 Os2 83.11(12) . . ? C1 Os1 Os2 176.88(12) . . ? C4 Os1 Os2 86.70(12) . . ? C3 Os1 Os2 89.63(12) . . ? C2 Os1 Os2 84.97(11) . . ? C7 Os2 C7 180.0 . 2_756 ? C7 Os2 C6 89.51(17) . . ? C7 Os2 C6 90.49(17) 2_756 . ? C7 Os2 C6 90.49(17) . 2_756 ? C7 Os2 C6 89.51(17) 2_756 2_756 ? C6 Os2 C6 180.0 . 2_756 ? C7 Os2 Os1 89.33(12) . 2_756 ? C7 Os2 Os1 90.67(12) 2_756 2_756 ? C6 Os2 Os1 91.41(11) . 2_756 ? C6 Os2 Os1 88.59(11) 2_756 2_756 ? C7 Os2 Os1 90.67(12) . . ? C7 Os2 Os1 89.33(12) 2_756 . ? C6 Os2 Os1 88.59(11) . . ? C6 Os2 Os1 91.41(11) 2_756 . ? Os1 Os2 Os1 180.0 2_756 . ? O1_1 Al1 O1_3 108.80(15) . . ? O1_1 Al1 O1_2 106.92(15) . . ? O1_3 Al1 O1_2 114.27(15) . . ? O1_1 Al1 O1_4 112.23(16) . . ? O1_3 Al1 O1_4 106.52(15) . . ? O1_2 Al1 O1_4 108.21(15) . . ? O1 C1 Os1 178.0(4) . . ? O2 C2 Os1 176.8(4) . . ? O3 C3 Os1 179.2(4) . . ? O4 C4 Os1 177.4(4) . . ? O5 C5 Os1 175.5(4) . . ? O6 C6 Os2 179.3(4) . . ? O7 C7 Os2 179.4(4) . . ? C1_1 O1_1 Al1 147.7(3) . . ? O1_1 C1_1 C4_1 111.7(3) . . ? O1_1 C1_1 C3_1 110.4(3) . . ? C4_1 C1_1 C3_1 108.7(3) . . ? O1_1 C1_1 C2_1 108.1(3) . . ? C4_1 C1_1 C2_1 108.2(3) . . ? C3_1 C1_1 C2_1 109.6(3) . . ? F3_1 C2_1 F1_1 107.6(3) . . ? F3_1 C2_1 F2_1 107.7(3) . . ? F1_1 C2_1 F2_1 108.1(3) . . ? F3_1 C2_1 C1_1 110.5(3) . . ? F1_1 C2_1 C1_1 110.6(3) . . ? F2_1 C2_1 C1_1 112.1(3) . . ? F4_1 C3_1 F5_1 107.4(3) . . ? F4_1 C3_1 F6_1 107.5(3) . . ? F5_1 C3_1 F6_1 107.3(3) . . ? F4_1 C3_1 C1_1 110.5(3) . . ? F5_1 C3_1 C1_1 111.2(3) . . ? F6_1 C3_1 C1_1 112.6(3) . . ? F9_1 C4_1 F8_1 107.6(3) . . ? F9_1 C4_1 F7_1 106.9(3) . . ? F8_1 C4_1 F7_1 107.2(3) . . ? F9_1 C4_1 C1_1 111.1(3) . . ? F8_1 C4_1 C1_1 112.7(3) . . ? F7_1 C4_1 C1_1 111.1(3) . . ? C1_2 O1_2 Al1 145.9(3) . . ? O1_2 C1_2 C3_2 112.3(3) . . ? O1_2 C1_2 C4_2 107.7(3) . . ? C3_2 C1_2 C4_2 108.8(3) . . ? O1_2 C1_2 C2_2 109.6(3) . . ? C3_2 C1_2 C2_2 108.9(3) . . ? C4_2 C1_2 C2_2 109.5(3) . . ? F3_2 C2_2 F1_2 107.6(3) . . ? F3_2 C2_2 F2_2 107.5(3) . . ? F1_2 C2_2 F2_2 107.2(3) . . ? F3_2 C2_2 C1_2 110.8(3) . . ? F1_2 C2_2 C1_2 111.3(3) . . ? F2_2 C2_2 C1_2 112.2(3) . . ? F4_2 C3_2 F6_2 108.0(3) . . ? F4_2 C3_2 F5_2 107.6(3) . . ? F6_2 C3_2 F5_2 107.0(3) . . ? F4_2 C3_2 C1_2 110.7(3) . . ? F6_2 C3_2 C1_2 112.2(3) . . ? F5_2 C3_2 C1_2 111.2(3) . . ? F8_2 C4_2 F9_2 108.0(3) . . ? F8_2 C4_2 F7_2 108.2(3) . . ? F9_2 C4_2 F7_2 106.9(3) . . ? F8_2 C4_2 C1_2 113.1(3) . . ? F9_2 C4_2 C1_2 110.4(3) . . ? F7_2 C4_2 C1_2 110.1(3) . . ? C1_3 O1_3 Al1 148.7(3) . . ? O1_3 C1_3 C3_3 111.1(3) . . ? O1_3 C1_3 C2_3 107.4(3) . . ? C3_3 C1_3 C2_3 108.9(3) . . ? O1_3 C1_3 C4_3 111.4(3) . . ? C3_3 C1_3 C4_3 109.1(3) . . ? C2_3 C1_3 C4_3 108.9(3) . . ? F3_3 C2_3 F2_3 108.1(4) . . ? F3_3 C2_3 F1_3 107.5(4) . . ? F2_3 C2_3 F1_3 107.2(4) . . ? F3_3 C2_3 C1_3 110.8(3) . . ? F2_3 C2_3 C1_3 112.9(3) . . ? F1_3 C2_3 C1_3 110.3(4) . . ? F4_3 C3_3 F6_3 107.7(4) . . ? F4_3 C3_3 F5_3 106.7(4) . . ? F6_3 C3_3 F5_3 106.9(4) . . ? F4_3 C3_3 C1_3 110.7(4) . . ? F6_3 C3_3 C1_3 113.4(4) . . ? F5_3 C3_3 C1_3 111.1(3) . . ? F9_3 C4_3 F7_3 107.7(4) . . ? F9_3 C4_3 F8_3 107.8(4) . . ? F7_3 C4_3 F8_3 107.5(4) . . ? F9_3 C4_3 C1_3 110.8(4) . . ? F7_3 C4_3 C1_3 110.6(4) . . ? F8_3 C4_3 C1_3 112.3(4) . . ? C1_4 O1_4 Al1 146.0(3) . . ? O1_4 C1_4 C3_4 110.4(3) . . ? O1_4 C1_4 C4_4 107.3(3) . . ? C3_4 C1_4 C4_4 109.5(3) . . ? O1_4 C1_4 C2_4 111.0(3) . . ? C3_4 C1_4 C2_4 109.3(3) . . ? C4_4 C1_4 C2_4 109.3(3) . . ? F1_4 C2_4 F3_4 107.9(3) . . ? F1_4 C2_4 F2_4 107.4(3) . . ? F3_4 C2_4 F2_4 106.7(3) . . ? F1_4 C2_4 C1_4 111.9(3) . . ? F3_4 C2_4 C1_4 110.6(3) . . ? F2_4 C2_4 C1_4 112.1(3) . . ? F5_4 C3_4 F6_4 107.3(4) . . ? F5_4 C3_4 F4_4 107.4(4) . . ? F6_4 C3_4 F4_4 107.6(4) . . ? F5_4 C3_4 C1_4 111.1(4) . . ? F6_4 C3_4 C1_4 112.9(3) . . ? F4_4 C3_4 C1_4 110.3(4) . . ? F9_4 C4_4 F7_4 107.4(4) . . ? F9_4 C4_4 F8_4 108.2(4) . . ? F7_4 C4_4 F8_4 107.2(3) . . ? F9_4 C4_4 C1_4 111.2(3) . . ? F7_4 C4_4 C1_4 110.6(3) . . ? F8_4 C4_4 C1_4 112.1(4) . . ? F1_5 C1_5 C6_5 120.8(4) . . ? F1_5 C1_5 C2_5 117.4(4) . . ? C6_5 C1_5 C2_5 121.8(4) . . ? F2_5 C2_5 C3_5 120.6(4) . . ? F2_5 C2_5 C1_5 120.5(4) . . ? C3_5 C2_5 C1_5 118.9(4) . . ? F3_5 C3_5 C4_5 120.6(4) . . ? F3_5 C3_5 C2_5 120.0(4) . . ? C4_5 C3_5 C2_5 119.4(4) . . ? F4_5 C4_5 C3_5 117.8(4) . . ? F4_5 C4_5 C5_5 120.3(4) . . ? C3_5 C4_5 C5_5 121.9(4) . . ? C4_5 C5_5 C6_5 118.7(4) . . ? C4_5 C5_5 H5_5 120.7 . . ? C6_5 C5_5 H5_5 120.7 . . ? C1_5 C6_5 C5_5 119.4(4) . . ? C1_5 C6_5 H6_5 120.3 . . ? C5_5 C6_5 H6_5 120.3 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_3 Al1 O1_1 C1_1 -30.5(5) . . . . ? O1_2 Al1 O1_1 C1_1 -154.3(5) . . . . ? O1_4 Al1 O1_1 C1_1 87.2(5) . . . . ? Al1 O1_1 C1_1 C4_1 -32.2(6) . . . . ? Al1 O1_1 C1_1 C3_1 88.9(5) . . . . ? Al1 O1_1 C1_1 C2_1 -151.1(4) . . . . ? O1_1 C1_1 C2_1 F3_1 -42.7(4) . . . . ? C4_1 C1_1 C2_1 F3_1 -163.8(3) . . . . ? C3_1 C1_1 C2_1 F3_1 77.8(4) . . . . ? O1_1 C1_1 C2_1 F1_1 76.5(4) . . . . ? C4_1 C1_1 C2_1 F1_1 -44.6(4) . . . . ? C3_1 C1_1 C2_1 F1_1 -163.1(3) . . . . ? O1_1 C1_1 C2_1 F2_1 -162.8(3) . . . . ? C4_1 C1_1 C2_1 F2_1 76.1(4) . . . . ? C3_1 C1_1 C2_1 F2_1 -42.3(4) . . . . ? O1_1 C1_1 C3_1 F4_1 -42.3(4) . . . . ? C4_1 C1_1 C3_1 F4_1 80.6(4) . . . . ? C2_1 C1_1 C3_1 F4_1 -161.4(3) . . . . ? O1_1 C1_1 C3_1 F5_1 76.9(4) . . . . ? C4_1 C1_1 C3_1 F5_1 -160.2(3) . . . . ? C2_1 C1_1 C3_1 F5_1 -42.2(4) . . . . ? O1_1 C1_1 C3_1 F6_1 -162.5(3) . . . . ? C4_1 C1_1 C3_1 F6_1 -39.7(4) . . . . ? C2_1 C1_1 C3_1 F6_1 78.4(4) . . . . ? O1_1 C1_1 C4_1 F9_1 -40.2(4) . . . . ? C3_1 C1_1 C4_1 F9_1 -162.3(3) . . . . ? C2_1 C1_1 C4_1 F9_1 78.6(4) . . . . ? O1_1 C1_1 C4_1 F8_1 -161.1(3) . . . . ? C3_1 C1_1 C4_1 F8_1 76.8(4) . . . . ? C2_1 C1_1 C4_1 F8_1 -42.2(4) . . . . ? O1_1 C1_1 C4_1 F7_1 78.6(4) . . . . ? C3_1 C1_1 C4_1 F7_1 -43.5(4) . . . . ? C2_1 C1_1 C4_1 F7_1 -162.5(3) . . . . ? O1_1 Al1 O1_2 C1_2 40.3(5) . . . . ? O1_3 Al1 O1_2 C1_2 -80.2(5) . . . . ? O1_4 Al1 O1_2 C1_2 161.3(4) . . . . ? Al1 O1_2 C1_2 C3_2 -56.0(6) . . . . ? Al1 O1_2 C1_2 C4_2 -175.7(4) . . . . ? Al1 O1_2 C1_2 C2_2 65.2(6) . . . . ? O1_2 C1_2 C2_2 F3_2 -46.4(4) . . . . ? C3_2 C1_2 C2_2 F3_2 76.8(4) . . . . ? C4_2 C1_2 C2_2 F3_2 -164.4(3) . . . . ? O1_2 C1_2 C2_2 F1_2 73.3(4) . . . . ? C3_2 C1_2 C2_2 F1_2 -163.5(3) . . . . ? C4_2 C1_2 C2_2 F1_2 -44.7(4) . . . . ? O1_2 C1_2 C2_2 F2_2 -166.6(3) . . . . ? C3_2 C1_2 C2_2 F2_2 -43.4(4) . . . . ? C4_2 C1_2 C2_2 F2_2 75.4(4) . . . . ? O1_2 C1_2 C3_2 F4_2 -40.2(4) . . . . ? C4_2 C1_2 C3_2 F4_2 79.0(4) . . . . ? C2_2 C1_2 C3_2 F4_2 -161.8(3) . . . . ? O1_2 C1_2 C3_2 F6_2 -160.9(3) . . . . ? C4_2 C1_2 C3_2 F6_2 -41.7(4) . . . . ? C2_2 C1_2 C3_2 F6_2 77.5(4) . . . . ? O1_2 C1_2 C3_2 F5_2 79.3(4) . . . . ? C4_2 C1_2 C3_2 F5_2 -161.5(3) . . . . ? C2_2 C1_2 C3_2 F5_2 -42.2(4) . . . . ? O1_2 C1_2 C4_2 F8_2 -164.8(3) . . . . ? C3_2 C1_2 C4_2 F8_2 73.2(4) . . . . ? C2_2 C1_2 C4_2 F8_2 -45.7(5) . . . . ? O1_2 C1_2 C4_2 F9_2 -43.7(4) . . . . ? C3_2 C1_2 C4_2 F9_2 -165.7(3) . . . . ? C2_2 C1_2 C4_2 F9_2 75.5(4) . . . . ? O1_2 C1_2 C4_2 F7_2 74.1(4) . . . . ? C3_2 C1_2 C4_2 F7_2 -47.9(4) . . . . ? C2_2 C1_2 C4_2 F7_2 -166.8(3) . . . . ? O1_1 Al1 O1_3 C1_3 156.8(5) . . . . ? O1_2 Al1 O1_3 C1_3 -83.8(6) . . . . ? O1_4 Al1 O1_3 C1_3 35.6(6) . . . . ? Al1 O1_3 C1_3 C3_3 65.1(6) . . . . ? Al1 O1_3 C1_3 C2_3 -175.9(4) . . . . ? Al1 O1_3 C1_3 C4_3 -56.7(7) . . . . ? O1_3 C1_3 C2_3 F3_3 -43.9(5) . . . . ? C3_3 C1_3 C2_3 F3_3 76.5(4) . . . . ? C4_3 C1_3 C2_3 F3_3 -164.6(4) . . . . ? O1_3 C1_3 C2_3 F2_3 -165.2(4) . . . . ? C3_3 C1_3 C2_3 F2_3 -44.9(5) . . . . ? C4_3 C1_3 C2_3 F2_3 74.0(5) . . . . ? O1_3 C1_3 C2_3 F1_3 74.9(4) . . . . ? C3_3 C1_3 C2_3 F1_3 -164.7(3) . . . . ? C4_3 C1_3 C2_3 F1_3 -45.8(5) . . . . ? O1_3 C1_3 C3_3 F4_3 -45.5(5) . . . . ? C2_3 C1_3 C3_3 F4_3 -163.5(4) . . . . ? C4_3 C1_3 C3_3 F4_3 77.8(4) . . . . ? O1_3 C1_3 C3_3 F6_3 -166.6(3) . . . . ? C2_3 C1_3 C3_3 F6_3 75.3(4) . . . . ? C4_3 C1_3 C3_3 F6_3 -43.4(5) . . . . ? O1_3 C1_3 C3_3 F5_3 72.9(4) . . . . ? C2_3 C1_3 C3_3 F5_3 -45.1(5) . . . . ? C4_3 C1_3 C3_3 F5_3 -163.9(3) . . . . ? O1_3 C1_3 C4_3 F9_3 -39.2(5) . . . . ? C3_3 C1_3 C4_3 F9_3 -162.2(4) . . . . ? C2_3 C1_3 C4_3 F9_3 79.0(4) . . . . ? O1_3 C1_3 C4_3 F7_3 80.1(4) . . . . ? C3_3 C1_3 C4_3 F7_3 -42.9(5) . . . . ? C2_3 C1_3 C4_3 F7_3 -161.7(3) . . . . ? O1_3 C1_3 C4_3 F8_3 -159.9(4) . . . . ? C3_3 C1_3 C4_3 F8_3 77.2(5) . . . . ? C2_3 C1_3 C4_3 F8_3 -41.6(5) . . . . ? O1_1 Al1 O1_4 C1_4 76.4(5) . . . . ? O1_3 Al1 O1_4 C1_4 -164.7(5) . . . . ? O1_2 Al1 O1_4 C1_4 -41.4(5) . . . . ? Al1 O1_4 C1_4 C3_4 74.9(6) . . . . ? Al1 O1_4 C1_4 C4_4 -165.8(4) . . . . ? Al1 O1_4 C1_4 C2_4 -46.5(6) . . . . ? O1_4 C1_4 C2_4 F1_4 -76.1(4) . . . . ? C3_4 C1_4 C2_4 F1_4 161.9(3) . . . . ? C4_4 C1_4 C2_4 F1_4 42.0(4) . . . . ? O1_4 C1_4 C2_4 F3_4 44.2(5) . . . . ? C3_4 C1_4 C2_4 F3_4 -77.8(4) . . . . ? C4_4 C1_4 C2_4 F3_4 162.3(3) . . . . ? O1_4 C1_4 C2_4 F2_4 163.2(3) . . . . ? C3_4 C1_4 C2_4 F2_4 41.2(4) . . . . ? C4_4 C1_4 C2_4 F2_4 -78.7(4) . . . . ? O1_4 C1_4 C3_4 F5_4 -78.8(4) . . . . ? C4_4 C1_4 C3_4 F5_4 163.3(3) . . . . ? C2_4 C1_4 C3_4 F5_4 43.6(4) . . . . ? O1_4 C1_4 C3_4 F6_4 160.6(4) . . . . ? C4_4 C1_4 C3_4 F6_4 42.7(5) . . . . ? C2_4 C1_4 C3_4 F6_4 -77.0(4) . . . . ? O1_4 C1_4 C3_4 F4_4 40.2(5) . . . . ? C4_4 C1_4 C3_4 F4_4 -77.7(4) . . . . ? C2_4 C1_4 C3_4 F4_4 162.6(3) . . . . ? O1_4 C1_4 C4_4 F9_4 46.3(4) . . . . ? C3_4 C1_4 C4_4 F9_4 166.2(3) . . . . ? C2_4 C1_4 C4_4 F9_4 -74.0(4) . . . . ? O1_4 C1_4 C4_4 F7_4 -72.9(4) . . . . ? C3_4 C1_4 C4_4 F7_4 47.0(5) . . . . ? C2_4 C1_4 C4_4 F7_4 166.8(3) . . . . ? O1_4 C1_4 C4_4 F8_4 167.6(3) . . . . ? C3_4 C1_4 C4_4 F8_4 -72.6(4) . . . . ? C2_4 C1_4 C4_4 F8_4 47.2(5) . . . . ? F1_5 C1_5 C2_5 F2_5 1.0(6) . . . . ? C6_5 C1_5 C2_5 F2_5 -179.2(4) . . . . ? F1_5 C1_5 C2_5 C3_5 -179.6(4) . . . . ? C6_5 C1_5 C2_5 C3_5 0.2(7) . . . . ? F2_5 C2_5 C3_5 F3_5 -0.3(6) . . . . ? C1_5 C2_5 C3_5 F3_5 -179.7(4) . . . . ? F2_5 C2_5 C3_5 C4_5 178.9(4) . . . . ? C1_5 C2_5 C3_5 C4_5 -0.5(6) . . . . ? F3_5 C3_5 C4_5 F4_5 -1.5(6) . . . . ? C2_5 C3_5 C4_5 F4_5 179.3(4) . . . . ? F3_5 C3_5 C4_5 C5_5 179.7(4) . . . . ? C2_5 C3_5 C4_5 C5_5 0.5(6) . . . . ? F4_5 C4_5 C5_5 C6_5 -179.0(4) . . . . ? C3_5 C4_5 C5_5 C6_5 -0.2(6) . . . . ? F1_5 C1_5 C6_5 C5_5 179.8(4) . . . . ? C2_5 C1_5 C6_5 C5_5 0.0(7) . . . . ? C4_5 C5_5 C6_5 C1_5 -0.1(6) . . . . ? _shelx_res_file ; TITL p-1_a.res in P-1 p-1_a.res created by SHELXL-2018/3 at 16:38:01 on 08-Feb-2022 REM Old TITL p-1 in P-1 REM SHELXT solution in P-1: R1 0.065, Rweak 0.008, Alpha 0.056 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C62 O18 F80 Al2 Os3 CELL 0.71073 11.2827 14.1432 15.7136 71.674 71.730 73.486 ZERR 21.000 0.0029 0.0027 0.0031 0.009 0.007 0.009 LATT 1 SFAC C O F AL OS H UNIT 58 22 80 2 3 4 REM Restraints for Fragment tetfluorbenz, 1,2,3,4-Tetrafluorobenzene, REM C6H2F4 from: CCDC ZELDOJ, http://dx.doi.org/10.1002/anie.199515171. REM Please cite https://doi.org/10.1107/S1600576718004508 REM HFIX_TFB 43 C5 C6 SIMU_TFB F1 > C6 RIGU_TFB F1 > C6 FLAT_TFB F1 > C6 SADI_TFB 0.02 C1 C2 C2 C3 C3 C4 C4 C5 C5 C6 C6 C1 SADI_TFB 0.02 C1 F1 C2 F2 C3 F3 C4 F4 SADI_TFB 0.04 C1 C3 C3 C5 C5 C1 C2 C6 C6 C4 C2 C4 SADI_TFB 0.05 C2 F1 C6 F1 C1 F2 C3 F2 C2 F3 C4 F3 C3 F4 C5 F4 SAME_TFB F1 > C6 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 TEMP -173.150 SIZE 0.029 0.081 0.252 L.S. 10 BOND $H CONF MORE -1 OMIT -3 7 16 OMIT 2 13 17 OMIT -3 -1 16 OMIT -3 8 16 LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.000000 16.600609 FVAR 0.24224 OS1 5 1.032734 0.146285 0.320501 11.00000 0.01149 0.01206 = 0.01110 -0.00190 -0.00320 -0.00200 OS2 5 1.000000 0.000000 0.500000 10.50000 0.01235 0.01123 = 0.01045 -0.00246 -0.00337 -0.00143 AL1 4 0.230556 0.295577 0.777181 11.00000 0.01141 0.01091 = 0.01195 -0.00368 -0.00245 -0.00108 O1 2 1.050141 0.310397 0.134682 11.00000 0.02622 0.01638 = 0.01779 0.00082 -0.00449 -0.00607 O2 2 0.924036 0.001613 0.265131 11.00000 0.02901 0.02082 = 0.01880 -0.00366 -0.00908 -0.00882 O3 2 1.303936 0.018844 0.258325 11.00000 0.02481 0.02830 = 0.02713 -0.00427 -0.00478 0.00258 O4 2 1.136453 0.264224 0.408374 11.00000 0.03041 0.02672 = 0.03180 -0.00849 -0.01416 -0.00846 O5 2 0.766419 0.256455 0.412276 11.00000 0.01623 0.02679 = 0.02141 0.00017 -0.00074 0.00082 O6 2 1.271875 0.004136 0.501296 11.00000 0.01749 0.02263 = 0.02406 -0.00662 -0.00523 -0.00398 O7 2 0.892892 0.174491 0.598680 11.00000 0.03102 0.02635 = 0.02625 -0.01421 -0.00855 0.00071 C1 1 1.045574 0.249979 0.200874 11.00000 0.01816 0.00853 = 0.01184 -0.00195 -0.00278 -0.00325 C2 1 0.961088 0.055966 0.283505 11.00000 0.01654 0.01745 = 0.01036 -0.00156 -0.00452 -0.00230 C3 1 1.206189 0.065592 0.280589 11.00000 0.02063 0.01652 = 0.01526 -0.00289 -0.00527 -0.00414 C4 1 1.101580 0.221450 0.374949 11.00000 0.01593 0.01616 = 0.01761 0.00025 -0.00647 -0.00172 C5 1 0.860502 0.215840 0.376732 11.00000 0.01558 0.01965 = 0.01259 0.00013 -0.00521 -0.00453 C6 1 1.172560 0.002100 0.501248 11.00000 0.01709 0.01170 = 0.01067 -0.00151 0.00016 -0.00309 C7 1 0.931459 0.110474 0.562603 11.00000 0.02209 0.01605 = 0.01147 -0.00157 -0.00381 -0.00310 RESI CCF3 1 O1 2 0.308860 0.355671 0.816230 11.00000 0.01800 0.01296 = 0.01823 -0.00521 -0.00564 -0.00257 C1 1 0.322390 0.443957 0.824508 11.00000 0.01293 0.01197 = 0.01703 -0.00513 -0.00327 -0.00152 C2 1 0.463868 0.431517 0.826378 11.00000 0.01571 0.01967 = 0.01883 -0.00566 -0.00620 -0.00331 F1 3 0.540163 0.437302 0.741888 11.00000 0.01533 0.03678 = 0.02623 -0.01133 -0.00025 -0.00607 F2 3 0.478043 0.502749 0.859363 11.00000 0.02163 0.02826 = 0.03718 -0.01658 -0.00988 -0.00700 F3 3 0.503639 0.341382 0.879453 11.00000 0.02287 0.02305 = 0.02949 -0.00597 -0.01465 0.00220 C3 1 0.231239 0.469564 0.915393 11.00000 0.01868 0.01212 = 0.01886 -0.00409 -0.00476 -0.00380 F4 3 0.117248 0.450721 0.928320 11.00000 0.01678 0.02429 = 0.02318 -0.00776 0.00037 -0.00645 F5 3 0.276067 0.413080 0.988926 11.00000 0.02976 0.02136 = 0.01468 -0.00349 -0.00777 -0.00211 F6 3 0.214280 0.567343 0.914979 11.00000 0.02771 0.01387 = 0.02220 -0.00679 -0.00250 -0.00342 C4 1 0.293633 0.533969 0.741439 11.00000 0.01898 0.01062 = 0.01805 -0.00097 -0.00387 -0.00394 F7 3 0.167647 0.567416 0.750410 11.00000 0.02034 0.01734 = 0.02624 -0.00017 -0.00998 -0.00155 F8 3 0.341997 0.613491 0.732726 11.00000 0.02901 0.01614 = 0.02317 -0.00076 -0.00619 -0.01098 F9 3 0.341219 0.505569 0.662296 11.00000 0.03099 0.02187 = 0.01389 -0.00357 -0.00470 -0.00477 RESI 0 RESI CCF3 2 O1 2 0.240200 0.172460 0.845474 11.00000 0.01595 0.01292 = 0.01258 -0.00158 -0.00211 -0.00362 C1 1 0.234959 0.112284 0.931820 11.00000 0.01611 0.01148 = 0.01468 -0.00304 -0.00171 -0.00149 C2 1 0.097981 0.136751 0.994216 11.00000 0.02007 0.01731 = 0.01715 -0.00427 0.00143 -0.00697 F1 3 0.015987 0.101064 0.973875 11.00000 0.01962 0.02569 = 0.03317 -0.00627 -0.00207 -0.01038 F2 3 0.093527 0.095633 1.084796 11.00000 0.03219 0.02647 = 0.01601 -0.00244 0.00125 -0.00232 F3 3 0.056182 0.236192 0.982803 11.00000 0.02261 0.01603 = 0.02137 -0.00498 -0.00169 0.00054 C3 1 0.332193 0.126283 0.976355 11.00000 0.02401 0.01597 = 0.01642 -0.00295 -0.00737 -0.00249 F4 3 0.442438 0.135682 0.914511 11.00000 0.01510 0.02389 = 0.02575 -0.00199 -0.00352 -0.00658 F5 3 0.288808 0.209975 1.008642 11.00000 0.03203 0.02015 = 0.02378 -0.00932 -0.00941 -0.00497 F6 3 0.355410 0.047860 1.047508 11.00000 0.03538 0.02150 = 0.02268 0.00215 -0.01577 -0.00560 C4 1 0.266721 -0.000315 0.925453 11.00000 0.02550 0.01548 = 0.02255 -0.00364 -0.00523 -0.00407 F7 3 0.391782 -0.028943 0.889329 11.00000 0.02485 0.01777 = 0.03358 -0.01096 -0.00303 0.00099 F8 3 0.235056 -0.065069 1.007103 11.00000 0.03609 0.01486 = 0.02660 0.00171 -0.00798 -0.00765 F9 3 0.205983 -0.009973 0.869326 11.00000 0.03099 0.01723 = 0.02945 -0.00776 -0.01198 -0.00543 RESI 0 RESI CCF3 3 O1 2 0.076786 0.364684 0.780580 11.00000 0.01338 0.02081 = 0.01647 -0.00652 -0.00464 -0.00025 C1 1 -0.029014 0.389491 0.749220 11.00000 0.01325 0.02154 = 0.01903 -0.00747 -0.00443 0.00030 C2 1 -0.124599 0.473548 0.795449 11.00000 0.01396 0.02315 = 0.03366 -0.01262 -0.00781 0.00262 F1 3 -0.087887 0.562901 0.756325 11.00000 0.02919 0.01964 = 0.05944 -0.01301 -0.01847 0.00179 F2 3 -0.242879 0.487631 0.787338 11.00000 0.01498 0.03905 = 0.05249 -0.02703 -0.01144 0.00692 F3 3 -0.128502 0.450754 0.884385 11.00000 0.02504 0.04557 = 0.02936 -0.02367 -0.00446 0.00418 C3 1 -0.090958 0.296852 0.775743 11.00000 0.02083 0.02628 = 0.03144 -0.01338 -0.00657 -0.00388 F4 3 -0.003278 0.214804 0.759009 11.00000 0.03060 0.02317 = 0.06358 -0.02090 -0.01791 0.00315 F5 3 -0.147925 0.274129 0.866306 11.00000 0.03095 0.03494 = 0.03810 -0.00434 -0.00131 -0.01579 F6 3 -0.179606 0.310993 0.730303 11.00000 0.02564 0.03745 = 0.05269 -0.02208 -0.01762 -0.00352 C4 1 0.000797 0.432131 0.642040 11.00000 0.02122 0.03708 = 0.02163 -0.00505 -0.00950 -0.00128 F7 3 0.050367 0.356102 0.599617 11.00000 0.03060 0.06464 = 0.02863 -0.02638 -0.00983 0.00518 F8 3 -0.103721 0.486694 0.612718 11.00000 0.03019 0.05441 = 0.02874 -0.00117 -0.01870 0.00286 F9 3 0.084699 0.491422 0.614051 11.00000 0.03424 0.05207 = 0.02593 0.00988 -0.00907 -0.01557 RESI 0 RESI CCF3 4 O1 2 0.300557 0.290130 0.663430 11.00000 0.01355 0.01967 = 0.01290 -0.00635 -0.00103 0.00129 C1 1 0.398960 0.243936 0.604955 11.00000 0.01472 0.01961 = 0.01571 -0.00813 -0.00251 -0.00334 C2 1 0.528104 0.233773 0.626656 11.00000 0.01791 0.02345 = 0.01624 -0.00787 -0.00335 0.00038 F1 3 0.566247 0.321315 0.596540 11.00000 0.02410 0.02550 = 0.03622 -0.00874 -0.00861 -0.00895 F2 3 0.622114 0.165291 0.587812 11.00000 0.01563 0.03062 = 0.02509 -0.01248 -0.00187 0.00264 F3 3 0.517838 0.202208 0.717489 11.00000 0.02501 0.03728 = 0.01384 -0.00617 -0.00729 0.00129 C3 1 0.380785 0.136617 0.612142 11.00000 0.02095 0.02731 = 0.02643 -0.01615 0.00647 -0.00674 F4 3 0.258396 0.139148 0.619825 11.00000 0.02193 0.04142 = 0.05558 -0.03079 0.00777 -0.01601 F5 3 0.413016 0.069287 0.686639 11.00000 0.04524 0.01971 = 0.03262 -0.00691 0.00498 -0.00837 F6 3 0.450669 0.100513 0.538583 11.00000 0.02581 0.03788 = 0.03692 -0.02901 0.00285 -0.00572 C4 1 0.400059 0.311497 0.505301 11.00000 0.01665 0.03774 = 0.01307 -0.00836 -0.00089 -0.00600 F7 3 0.303627 0.304071 0.477436 11.00000 0.01903 0.06763 = 0.02194 -0.01663 -0.00738 -0.00752 F8 3 0.507772 0.284013 0.443943 11.00000 0.02020 0.05087 = 0.01275 -0.00886 0.00226 -0.00626 F9 3 0.387119 0.408565 0.501634 11.00000 0.03619 0.02947 = 0.02137 0.00385 -0.00668 -0.00602 RESI 0 RESI TFB 5 F1 3 0.310492 0.250081 0.194820 11.00000 0.01535 0.03892 = 0.03390 -0.00402 -0.01089 -0.00753 F2 3 0.410123 0.151370 0.341377 11.00000 0.02523 0.03692 = 0.01861 -0.00065 0.00012 -0.00805 F3 3 0.663339 0.133019 0.325287 11.00000 0.02621 0.03418 = 0.02252 -0.00346 -0.01458 -0.00028 F4 3 0.813673 0.212561 0.162738 11.00000 0.01474 0.02607 = 0.03713 -0.00547 -0.00862 -0.00479 C1 1 0.436921 0.241614 0.184142 11.00000 0.01520 0.02127 = 0.02535 -0.00558 -0.00832 -0.00357 C2 1 0.485752 0.191412 0.260387 11.00000 0.01996 0.02406 = 0.01344 -0.00339 -0.00311 -0.00503 C3 1 0.613414 0.182091 0.252025 11.00000 0.02094 0.01832 = 0.01638 -0.00620 -0.00774 -0.00203 C4 1 0.688936 0.222182 0.168163 11.00000 0.01179 0.01393 = 0.02471 -0.00617 -0.00472 -0.00093 C5 1 0.640612 0.272248 0.092026 11.00000 0.02198 0.01744 = 0.01653 -0.00347 -0.00230 -0.00595 AFIX 43 H5 6 0.694348 0.299671 0.034619 11.00000 -1.20000 AFIX 0 C6 1 0.512040 0.281962 0.100593 11.00000 0.02561 0.01950 = 0.02056 -0.00017 -0.01225 -0.00305 AFIX 43 H6 6 0.476297 0.316306 0.048972 11.00000 -1.20000 RESI 0 REM ##### AFIX 0 HKLF 4 REM p-1_a.res in P-1 REM wR2 = 0.0713, GooF = S = 1.000, Restrained GooF = 0.915 for all data REM R1 = 0.0411 for 10982 Fo > 4sig(Fo) and 0.0604 for all 13532 data REM 745 parameters refined using 3053 restraints END WGHT 0.0000 14.3220 REM Highest difference peak 1.193, deepest hole -2.394, 1-sigma level 0.189 Q1 1 1.0351 0.0275 0.4197 11.00000 0.05 1.19 Q2 1 1.0583 0.0506 0.4508 11.00000 0.05 0.94 Q3 1 1.0221 0.2255 0.2624 11.00000 0.05 0.92 Q4 1 1.0510 0.1530 0.2608 11.00000 0.05 0.90 Q5 1 1.0047 -0.0313 0.4407 11.00000 0.05 0.89 Q6 1 0.9750 0.0949 0.3727 11.00000 0.05 0.89 Q7 1 0.7221 0.0143 0.3358 11.00000 0.05 0.84 Q8 1 0.9375 0.0272 0.6206 11.00000 0.05 0.83 Q9 1 0.5435 0.2974 0.6531 11.00000 0.05 0.82 Q10 1 1.0471 0.1873 0.2391 11.00000 0.05 0.81 Q11 1 0.9587 0.1656 0.3978 11.00000 0.05 0.81 Q12 1 0.9386 0.2918 0.3305 11.00000 0.05 0.80 Q13 1 0.9738 0.0169 0.4216 11.00000 0.05 0.79 Q14 1 -0.0820 0.2100 0.7590 11.00000 0.05 0.78 Q15 1 1.0802 0.0324 0.5936 11.00000 0.05 0.76 Q16 1 1.0193 0.0835 0.3185 11.00000 0.05 0.76 Q17 1 0.4738 0.1227 0.7698 11.00000 0.05 0.76 Q18 1 1.1007 0.0121 0.4968 11.00000 0.05 0.75 Q19 1 1.1041 -0.0261 0.4620 11.00000 0.05 0.74 Q20 1 0.5410 0.2216 0.7549 11.00000 0.05 0.73 ; _shelx_res_checksum 74220 _shelx_hkl_file ; 1 0 0 2149.88 16.90 2 0 0 2228.88 22.60 3 0 0 1924.11 13.30 4 0 0 1715.43 13.90 5 0 0 87.09 2.60 6 0 0 184.18 3.90 7 0 0 44.80 2.60 8 0 0 133.49 6.20 9 0 0 51.99 3.60 10 0 0 0.00 8.50 11 0 0 55.29 6.60 12 0 0 24.10 8.00 13 0 0 17.70 12.50 14 0 0 89.49 17.60 15 0 0 37.00 47.30 -14 1 0 58.39 49.60 -13 1 0 20.90 14.00 -12 1 0 31.10 9.10 -11 1 0 180.68 9.70 -10 1 0 428.96 12.10 -9 1 0 116.09 4.60 -8 1 0 964.00 16.10 -7 1 0 747.33 9.60 -6 1 0 647.94 9.00 -5 1 0 7034.60 58.49 -4 1 0 5144.89 43.30 -3 1 0 3859.01 29.50 -2 1 0 781.82 7.30 -1 1 0 2711.13 22.90 0 1 0 837.72 25.50 1 1 0 18.50 0.60 2 1 0 851.11 12.70 3 1 0 810.02 6.60 4 1 0 173.88 3.70 5 1 0 2.20 1.00 6 1 0 30.10 3.40 7 1 0 13.20 1.60 8 1 0 241.28 5.10 9 1 0 29.90 2.40 10 1 0 175.18 7.90 11 1 0 26.60 6.10 12 1 0 0.00 8.30 13 1 0 28.70 11.30 14 1 0 24.40 14.80 15 1 0 19.50 41.90 -14 2 0 144.59 28.40 -13 2 0 201.38 17.90 -12 2 0 599.54 17.60 -11 2 0 683.13 17.30 -10 2 0 697.63 14.50 -9 2 0 1370.56 16.30 -8 2 0 1044.50 16.40 -7 2 0 1063.99 12.60 -6 2 0 271.07 10.00 -5 2 0 1342.27 12.90 -4 2 0 27.90 2.20 -3 2 0 862.71 7.10 -2 2 0 22.30 2.30 -1 2 0 1179.48 8.90 0 2 0 15.30 0.90 1 2 0 73.19 1.40 2 2 0 228.28 4.80 3 2 0 103.19 2.20 4 2 0 31.20 6.40 5 2 0 310.07 4.50 6 2 0 313.77 5.40 7 2 0 332.47 5.30 8 2 0 31.10 3.00 9 2 0 23.10 2.30 10 2 0 85.89 5.20 11 2 0 94.19 8.20 12 2 0 33.10 12.30 13 2 0 0.00 8.40 14 2 0 23.20 17.20 15 2 0 120.09 47.40 -14 3 0 525.25 49.40 -13 3 0 410.66 22.00 -12 3 0 534.75 17.20 -11 3 0 320.67 12.00 -10 3 0 286.17 12.10 -9 3 0 136.89 5.70 -8 3 0 25.80 4.50 -7 3 0 129.59 4.30 -6 3 0 156.18 6.40 -5 3 0 204.38 3.90 -4 3 0 29.70 3.10 -3 3 0 291.37 4.50 -2 3 0 340.87 5.40 -1 3 0 29.80 1.30 0 3 0 894.51 10.30 1 3 0 419.16 4.00 2 3 0 376.86 4.10 3 3 0 432.46 4.50 4 3 0 85.29 15.40 5 3 0 10.30 1.40 6 3 0 40.50 3.30 7 3 0 9.30 1.60 8 3 0 12.10 4.10 9 3 0 14.50 2.20 10 3 0 284.17 7.60 11 3 0 74.99 7.00 12 3 0 127.09 9.20 13 3 0 149.88 17.60 14 3 0 454.15 25.60 15 3 0 173.78 32.40 -14 4 0 62.59 153.88 -13 4 0 143.29 24.40 -12 4 0 76.69 17.10 -11 4 0 72.99 9.50 -10 4 0 164.58 8.30 -9 4 0 12.90 3.00 -8 4 0 4.00 5.40 -7 4 0 15.70 2.30 -6 4 0 5.00 2.70 -5 4 0 655.43 8.30 -4 4 0 80.49 6.90 -3 4 0 695.03 7.40 -2 4 0 892.41 11.70 -1 4 0 68.69 2.10 0 4 0 403.96 5.30 1 4 0 131.39 2.20 2 4 0 269.77 4.80 3 4 0 223.78 3.50 4 4 0 119.29 3.20 5 4 0 73.59 3.00 6 4 0 389.06 8.50 7 4 0 133.49 4.10 8 4 0 726.03 11.10 9 4 0 451.25 7.90 10 4 0 647.14 13.80 11 4 0 254.67 7.40 12 4 0 522.05 13.40 13 4 0 564.14 16.70 14 4 0 272.17 22.90 15 4 0 196.18 33.90 -13 5 0 14.80 14.20 -12 5 0 0.00 11.00 -11 5 0 13.20 4.20 -10 5 0 6.40 6.70 -9 5 0 366.46 9.70 -8 5 0 117.19 9.70 -7 5 0 41.30 3.00 -6 5 0 31.40 3.00 -5 5 0 178.38 4.40 -4 5 0 9.80 3.80 -3 5 0 155.98 4.20 -2 5 0 195.98 7.10 -1 5 0 1.90 0.90 0 5 0 15.50 1.30 1 5 0 759.42 6.80 2 5 0 701.33 10.80 3 5 0 619.44 6.60 4 5 0 273.07 4.90 5 5 0 2568.34 19.20 6 5 0 1659.93 18.50 7 5 0 1362.16 14.00 8 5 0 1018.30 16.00 9 5 0 606.84 9.50 10 5 0 832.52 14.60 11 5 0 706.63 12.10 12 5 0 155.98 9.10 13 5 0 201.38 10.00 14 5 0 123.59 16.90 15 5 0 105.19 119.59 -13 6 0 56.99 34.80 -12 6 0 1.90 11.30 -11 6 0 91.09 9.20 -10 6 0 87.09 8.70 -9 6 0 138.89 7.50 -8 6 0 6.20 4.40 -7 6 0 14.50 2.30 -6 6 0 39.50 3.50 -5 6 0 32.30 2.80 -4 6 0 206.28 6.00 -3 6 0 344.67 6.00 -2 6 0 451.45 11.30 -1 6 0 242.18 4.20 0 6 0 1249.97 17.20 1 6 0 1203.98 9.90 2 6 0 926.51 12.70 3 6 0 1508.05 12.80 4 6 0 1210.68 14.10 5 6 0 1439.16 13.60 6 6 0 892.61 11.30 7 6 0 343.47 6.30 8 6 0 537.65 13.00 9 6 0 254.07 7.00 10 6 0 549.25 15.20 11 6 0 151.48 6.90 12 6 0 30.10 8.70 13 6 0 14.80 6.30 14 6 0 15.40 10.30 15 6 0 0.00 174.88 -12 7 0 17.20 17.10 -11 7 0 3.90 5.10 -10 7 0 10.60 6.70 -9 7 0 63.29 5.90 -8 7 0 78.39 7.80 -7 7 0 371.56 9.80 -6 7 0 324.17 7.80 -5 7 0 646.64 10.20 -4 7 0 986.10 12.90 -3 7 0 222.68 5.40 -2 7 0 373.76 8.10 -1 7 0 703.63 8.40 0 7 0 2956.90 36.30 1 7 0 1675.03 13.80 2 7 0 465.65 7.90 3 7 0 1854.91 16.10 4 7 0 192.18 4.60 5 7 0 800.52 9.00 6 7 0 64.89 3.40 7 7 0 177.38 5.30 8 7 0 162.28 5.40 9 7 0 3.70 2.00 10 7 0 39.90 8.60 11 7 0 5.20 2.60 12 7 0 8.50 5.00 13 7 0 14.60 4.90 14 7 0 31.80 10.90 15 7 0 95.89 154.48 -12 8 0 50.09 14.90 -11 8 0 128.59 12.20 -10 8 0 115.09 11.10 -9 8 0 327.97 10.60 -8 8 0 420.46 15.20 -7 8 0 536.25 12.90 -6 8 0 442.56 12.10 -5 8 0 616.84 10.40 -4 8 0 683.53 10.80 -3 8 0 1035.40 13.00 -2 8 0 625.24 9.00 -1 8 0 1077.59 12.10 0 8 0 663.33 9.60 1 8 0 330.17 5.10 2 8 0 366.86 6.20 3 8 0 1198.08 12.80 4 8 0 54.99 3.90 5 8 0 121.39 4.10 6 8 0 3.70 2.70 7 8 0 47.10 3.30 8 8 0 197.38 6.20 9 8 0 99.69 5.30 10 8 0 208.88 10.10 11 8 0 37.40 5.20 12 8 0 0.00 8.50 13 8 0 20.90 7.20 14 8 0 0.60 13.40 -11 9 0 346.97 19.90 -10 9 0 402.66 14.50 -9 9 0 321.47 12.50 -8 9 0 284.17 15.40 -7 9 0 1054.69 17.60 -6 9 0 560.84 15.70 -5 9 0 267.17 8.70 -4 9 0 435.86 10.20 -3 9 0 260.87 7.10 -2 9 0 348.77 7.50 -1 9 0 252.57 6.00 0 9 0 120.29 3.90 1 9 0 81.99 3.10 2 9 0 43.20 4.60 3 9 0 439.46 6.70 4 9 0 0.00 6.70 5 9 0 237.48 6.20 6 9 0 56.39 4.30 7 9 0 30.10 2.90 8 9 0 369.06 11.60 9 9 0 3.00 2.50 10 9 0 0.00 6.40 11 9 0 89.79 6.60 12 9 0 0.00 8.90 13 9 0 33.60 11.00 14 9 0 27.00 14.00 -11 10 0 322.97 21.40 -10 10 0 230.08 23.10 -9 10 0 237.88 18.00 -8 10 0 173.28 8.60 -7 10 0 19.90 4.20 -6 10 0 25.70 6.30 -5 10 0 8.90 3.10 -4 10 0 271.27 10.10 -3 10 0 2.30 1.80 -2 10 0 134.39 5.50 -1 10 0 12.70 2.30 0 10 0 15.80 2.40 1 10 0 133.99 4.40 2 10 0 87.59 4.50 3 10 0 213.68 5.50 4 10 0 66.29 6.00 5 10 0 27.60 2.50 6 10 0 23.30 5.60 7 10 0 18.50 3.00 8 10 0 34.00 5.40 9 10 0 8.40 2.90 10 10 0 241.88 10.60 11 10 0 294.37 10.20 12 10 0 229.58 11.40 13 10 0 237.68 13.00 14 10 0 239.68 25.50 -10 11 0 18.50 11.50 -9 11 0 7.80 5.50 -8 11 0 6.50 6.50 -7 11 0 21.10 5.50 -6 11 0 21.80 7.40 -5 11 0 74.89 6.40 -4 11 0 132.89 12.80 -3 11 0 594.24 13.00 -2 11 0 97.19 7.30 -1 11 0 2.10 1.80 0 11 0 51.69 3.70 1 11 0 25.20 2.70 2 11 0 10.40 4.10 3 11 0 89.49 4.50 4 11 0 151.08 8.00 5 11 0 15.60 2.70 6 11 0 221.08 10.00 7 11 0 436.86 9.60 8 11 0 637.84 15.40 9 11 0 317.77 9.60 10 11 0 474.95 13.70 11 11 0 364.36 12.10 12 11 0 416.56 17.90 13 11 0 394.46 19.20 14 11 0 184.18 21.10 -9 12 0 68.49 14.20 -8 12 0 61.79 9.80 -7 12 0 3.10 3.90 -6 12 0 233.08 11.00 -5 12 0 6.40 3.70 -4 12 0 10.40 7.00 -3 12 0 29.40 4.30 -2 12 0 39.00 8.70 -1 12 0 12.20 4.40 0 12 0 89.69 5.80 1 12 0 167.38 6.30 2 12 0 310.87 8.20 3 12 0 480.65 9.90 4 12 0 273.37 10.40 5 12 0 889.51 14.40 6 12 0 710.13 18.10 7 12 0 405.76 12.00 8 12 0 582.94 18.20 9 12 0 252.57 10.10 10 12 0 241.08 10.40 11 12 0 289.67 11.70 12 12 0 175.08 11.40 13 12 0 46.70 9.00 -8 13 0 0.00 10.10 -7 13 0 50.09 8.40 -6 13 0 0.00 6.10 -5 13 0 69.69 6.90 -4 13 0 75.69 9.60 -3 13 0 190.28 9.20 -2 13 0 243.68 11.20 -1 13 0 418.66 12.30 0 13 0 591.94 23.50 1 13 0 1026.10 18.30 2 13 0 350.46 9.60 3 13 0 897.61 15.70 4 13 0 731.33 17.20 5 13 0 735.13 14.90 6 13 0 187.28 8.20 7 13 0 261.47 9.60 8 13 0 39.10 8.00 9 13 0 87.99 7.30 10 13 0 94.49 10.50 11 13 0 17.10 6.40 12 13 0 18.70 11.80 13 13 0 9.40 7.90 -7 14 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1 257.07 10.20 4 -14 1 288.27 11.40 5 -14 1 356.46 13.30 6 -14 1 348.77 14.60 7 -14 1 168.78 14.80 -12 -13 1 26.10 10.80 -11 -13 1 29.50 9.70 -10 -13 1 1.40 4.80 -9 -13 1 30.10 8.00 -8 -13 1 0.30 4.60 -7 -13 1 0.00 6.80 -6 -13 1 90.09 6.80 -5 -13 1 268.77 11.60 -4 -13 1 159.18 7.70 -3 -13 1 51.99 5.90 -2 -13 1 466.45 10.80 -1 -13 1 389.36 11.00 0 -13 1 467.45 11.40 1 -13 1 359.46 12.60 2 -13 1 372.76 12.60 3 -13 1 587.14 16.40 4 -13 1 305.17 9.90 5 -13 1 306.67 12.20 6 -13 1 328.17 14.50 7 -13 1 260.07 12.80 8 -13 1 200.68 14.40 -13 -12 1 20.30 18.60 -12 -12 1 2.90 9.10 -11 -12 1 18.70 8.50 -10 -12 1 2.60 4.70 -9 -12 1 144.99 8.60 -8 -12 1 103.39 8.20 -7 -12 1 168.58 13.40 -6 -12 1 549.65 14.20 -5 -12 1 480.75 15.30 -4 -12 1 383.96 9.50 -3 -12 1 1055.59 22.10 -2 -12 1 898.71 14.80 -1 -12 1 380.56 12.40 0 -12 1 918.31 19.10 1 -12 1 682.33 17.40 2 -12 1 355.06 12.20 3 -12 1 429.66 16.20 4 -12 1 78.59 6.00 5 -12 1 82.59 8.70 6 -12 1 64.09 6.70 7 -12 1 63.69 8.40 8 -12 1 6.60 5.00 9 -12 1 11.40 10.10 -13 -11 1 68.19 19.30 -12 -11 1 87.19 17.20 -11 -11 1 182.88 12.10 -10 -11 1 312.47 14.90 -9 -11 1 362.56 11.80 -8 -11 1 380.66 11.40 -7 -11 1 439.86 12.40 -6 -11 1 814.32 15.30 -5 -11 1 1159.58 25.00 -4 -11 1 1193.28 16.20 -3 -11 1 323.07 8.10 -2 -11 1 509.75 8.50 -1 -11 1 882.31 13.30 0 -11 1 259.47 6.80 1 -11 1 252.87 7.80 2 -11 1 5.30 2.50 3 -11 1 33.30 7.40 4 -11 1 36.40 4.50 5 -11 1 52.69 9.10 6 -11 1 141.89 8.30 7 -11 1 48.70 7.20 8 -11 1 55.69 7.70 9 -11 1 21.80 10.40 10 -11 1 95.99 14.60 -14 -10 1 219.68 24.20 -13 -10 1 107.19 13.20 -12 -10 1 280.07 14.60 -11 -10 1 386.56 13.20 -10 -10 1 492.65 11.90 -9 -10 1 704.13 15.00 -8 -10 1 358.66 10.10 -7 -10 1 630.14 12.30 -6 -10 1 461.55 8.90 -5 -10 1 190.18 7.70 -4 -10 1 128.99 4.80 -3 -10 1 112.79 7.30 -2 -10 1 179.98 4.60 -1 -10 1 46.80 4.20 0 -10 1 10.40 1.70 1 -10 1 370.16 9.00 2 -10 1 6.70 2.20 3 -10 1 116.09 8.50 4 -10 1 79.29 5.70 5 -10 1 167.68 10.70 6 -10 1 7.70 3.00 7 -10 1 68.09 8.30 8 -10 1 5.10 3.00 9 -10 1 7.80 8.60 10 -10 1 1.80 4.70 11 -10 1 46.90 16.10 -14 -9 1 312.57 22.30 -13 -9 1 252.87 13.80 -12 -9 1 319.97 12.90 -11 -9 1 411.26 16.80 -10 -9 1 148.79 9.10 -9 -9 1 2.20 5.10 -8 -9 1 124.39 6.80 -7 -9 1 65.09 5.60 -6 -9 1 9.90 2.00 -5 -9 1 65.39 5.30 -4 -9 1 79.89 3.70 -3 -9 1 330.37 10.80 -2 -9 1 13.60 1.70 -1 -9 1 26.90 3.30 0 -9 1 599.04 7.80 1 -9 1 129.59 4.70 2 -9 1 81.39 4.20 3 -9 1 69.69 4.30 4 -9 1 3.10 2.00 5 -9 1 24.90 5.20 6 -9 1 2.00 2.20 7 -9 1 28.70 9.10 8 -9 1 137.69 8.80 9 -9 1 105.49 11.70 10 -9 1 36.20 7.70 11 -9 1 280.57 16.40 -14 -8 1 31.60 16.70 -13 -8 1 85.59 10.30 -12 -8 1 98.99 7.90 -11 -8 1 0.00 7.50 -10 -8 1 105.89 7.70 -9 -8 1 3.50 8.70 -8 -8 1 233.68 7.20 -7 -8 1 36.30 4.50 -6 -8 1 280.17 5.90 -5 -8 1 112.59 4.50 -4 -8 1 73.79 3.20 -3 -8 1 76.79 3.10 -2 -8 1 854.91 8.60 -1 -8 1 5.80 7.70 0 -8 1 25.80 1.80 1 -8 1 205.58 4.50 2 -8 1 99.49 4.00 3 -8 1 1.40 2.40 4 -8 1 186.38 5.80 5 -8 1 285.47 9.60 6 -8 1 282.07 8.80 7 -8 1 306.07 9.50 8 -8 1 961.60 17.80 9 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6.90 5 -6 1 574.14 10.40 6 -6 1 943.71 12.00 7 -6 1 287.07 7.20 8 -6 1 97.99 6.00 9 -6 1 6.30 5.00 10 -6 1 109.99 7.70 11 -6 1 39.70 13.90 12 -6 1 13.50 5.60 13 -6 1 0.00 69.29 -15 -5 1 0.00 21.90 -14 -5 1 64.19 19.20 -13 -5 1 4.80 9.20 -12 -5 1 39.80 6.70 -11 -5 1 6.40 5.00 -10 -5 1 7.30 3.60 -9 -5 1 325.37 9.70 -8 -5 1 1649.33 17.30 -7 -5 1 824.72 16.60 -6 -5 1 1626.74 15.10 -5 -5 1 1620.34 26.90 -4 -5 1 1492.25 13.20 -3 -5 1 1232.68 13.00 -2 -5 1 6522.65 48.10 -1 -5 1 1986.60 18.70 0 -5 1 287.27 4.00 1 -5 1 1293.47 13.50 2 -5 1 900.71 9.00 3 -5 1 555.14 23.10 4 -5 1 56.29 3.00 5 -5 1 368.36 8.10 6 -5 1 17.30 2.10 7 -5 1 17.00 3.00 8 -5 1 40.80 3.70 9 -5 1 19.10 5.50 10 -5 1 25.70 4.10 11 -5 1 0.00 5.90 12 -5 1 35.20 6.20 13 -5 1 72.99 20.60 -15 -4 1 12.30 22.20 -14 -4 1 102.59 18.60 -13 -4 1 210.88 14.80 -12 -4 1 594.54 16.70 -11 -4 1 415.06 10.40 -10 -4 1 772.42 12.10 -9 -4 1 645.04 10.80 -8 -4 1 506.25 8.20 -7 -4 1 1219.68 13.00 -6 -4 1 3018.80 23.10 -5 -4 1 1004.30 15.60 -4 -4 1 455.45 5.90 -3 -4 1 574.74 9.50 -2 -4 1 438.06 4.60 -1 -4 1 90.49 2.40 0 -4 1 374.76 4.30 1 -4 1 1362.96 12.00 2 -4 1 251.87 4.10 3 -4 1 245.48 6.00 4 -4 1 17.80 1.80 5 -4 1 169.78 6.60 6 -4 1 719.63 10.00 7 -4 1 56.99 4.30 8 -4 1 197.68 7.10 9 -4 1 29.10 4.50 10 -4 1 3.20 2.40 11 -4 1 23.90 5.40 12 -4 1 9.40 6.20 13 -4 1 15.90 20.50 14 -4 1 34.90 11.30 -15 -3 1 236.38 34.60 -14 -3 1 237.48 31.90 -13 -3 1 478.05 23.60 -12 -3 1 413.16 18.70 -11 -3 1 582.94 19.90 -10 -3 1 623.74 13.20 -9 -3 1 765.12 11.40 -8 -3 1 238.88 5.30 -7 -3 1 1014.20 10.70 -6 -3 1 220.68 4.80 -5 -3 1 28.90 2.90 -4 -3 1 2112.59 15.60 -3 -3 1 237.98 13.10 -2 -3 1 354.86 3.90 -1 -3 1 33.90 3.00 0 -3 1 23.60 1.00 1 -3 1 294.27 3.70 2 -3 1 314.57 4.00 3 -3 1 949.60 9.30 4 -3 1 241.38 4.20 5 -3 1 230.98 5.50 6 -3 1 42.20 2.70 7 -3 1 262.47 9.30 8 -3 1 19.20 2.70 9 -3 1 19.50 6.10 10 -3 1 3.00 2.70 11 -3 1 20.40 6.80 12 -3 1 29.90 4.40 13 -3 1 86.49 12.40 14 -3 1 86.99 32.70 -15 -2 1 319.87 35.50 -14 -2 1 406.26 36.10 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189.18 10.60 -1 -15 2 19.70 7.00 0 -15 2 15.30 9.10 1 -15 2 79.89 8.10 2 -15 2 143.39 9.80 3 -15 2 70.49 7.80 4 -15 2 8.60 6.00 5 -15 2 6.20 5.00 6 -15 2 17.00 7.40 -11 -14 2 36.90 12.00 -10 -14 2 29.60 13.60 -9 -14 2 0.00 9.70 -8 -14 2 14.40 12.30 -7 -14 2 48.70 10.20 -6 -14 2 1.20 7.60 -5 -14 2 72.69 7.60 -4 -14 2 6.00 4.70 -3 -14 2 79.49 7.20 -2 -14 2 152.08 9.20 -1 -14 2 48.70 6.70 0 -14 2 39.20 10.60 1 -14 2 72.99 6.80 2 -14 2 6.00 8.10 3 -14 2 4.50 3.70 4 -14 2 14.70 7.00 5 -14 2 39.00 5.90 6 -14 2 105.19 9.40 7 -14 2 233.58 19.00 -12 -13 2 4.10 11.50 -11 -13 2 6.30 8.50 -10 -13 2 22.50 12.80 -9 -13 2 41.30 7.60 -8 -13 2 50.79 7.80 -7 -13 2 13.00 10.00 -6 -13 2 149.19 9.70 -5 -13 2 159.78 10.20 -4 -13 2 57.59 6.20 -3 -13 2 7.80 2.40 -2 -13 2 28.20 5.50 -1 -13 2 0.70 3.30 0 -13 2 72.99 5.60 1 -13 2 179.88 6.40 2 -13 2 344.47 12.40 3 -13 2 74.79 7.20 4 -13 2 120.79 9.40 5 -13 2 308.17 12.20 6 -13 2 443.66 18.30 7 -13 2 285.17 13.60 8 -13 2 138.39 20.20 -12 -12 2 57.39 15.30 -11 -12 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17.80 -12 -8 2 246.08 10.70 -11 -8 2 493.45 12.90 -10 -8 2 538.95 14.90 -9 -8 2 237.88 9.20 -8 -8 2 264.47 11.80 -7 -8 2 38.50 5.10 -6 -8 2 93.49 5.10 -5 -8 2 177.28 5.40 -4 -8 2 3.30 2.40 -3 -8 2 382.36 5.90 -2 -8 2 25.50 3.50 -1 -8 2 20.20 1.60 0 -8 2 4.90 7.50 1 -8 2 373.06 6.20 2 -8 2 95.49 6.60 3 -8 2 63.79 3.50 4 -8 2 14.50 2.90 5 -8 2 23.60 3.00 6 -8 2 0.20 3.30 7 -8 2 3.00 2.40 8 -8 2 238.58 9.30 9 -8 2 28.10 6.10 10 -8 2 82.29 11.70 11 -8 2 142.69 12.50 12 -8 2 183.68 25.30 -14 -7 2 204.68 24.20 -13 -7 2 98.59 11.40 -12 -7 2 84.49 12.30 -11 -7 2 112.99 10.60 -10 -7 2 29.90 6.40 -9 -7 2 0.00 5.00 -8 -7 2 0.00 8.10 -7 -7 2 2.80 2.20 -6 -7 2 47.80 4.40 -5 -7 2 19.50 2.30 -4 -7 2 71.89 3.50 -3 -7 2 163.48 4.00 -2 -7 2 37.90 2.30 -1 -7 2 311.87 4.60 0 -7 2 0.00 3.70 1 -7 2 17.50 1.60 2 -7 2 15.80 4.70 3 -7 2 141.29 4.10 4 -7 2 3.00 2.80 5 -7 2 415.46 6.90 6 -7 2 516.95 10.10 7 -7 2 356.26 7.80 8 -7 2 599.24 13.60 9 -7 2 318.27 12.50 10 -7 2 523.65 16.80 11 -7 2 400.96 15.40 12 -7 2 312.77 18.10 -14 -6 2 37.80 13.70 -13 -6 2 22.20 9.20 -12 -6 2 8.50 5.90 -11 -6 2 46.30 5.90 -10 -6 2 91.49 9.10 -9 -6 2 37.50 5.30 -8 -6 2 258.67 10.30 -7 -6 2 5.50 2.40 -6 -6 2 30.20 11.90 -5 -6 2 43.20 2.70 -4 -6 2 70.99 4.00 -3 -6 2 114.19 3.30 -2 -6 2 234.58 4.80 -1 -6 2 14.00 1.30 0 -6 2 307.57 5.40 1 -6 2 378.36 5.00 2 -6 2 258.07 10.90 3 -6 2 626.74 7.80 4 -6 2 368.66 11.00 5 -6 2 1637.84 17.10 6 -6 2 1697.53 17.90 7 -6 2 949.90 13.50 8 -6 2 632.54 12.50 9 -6 2 732.03 14.90 10 -6 2 388.56 12.10 11 -6 2 331.17 11.90 12 -6 2 156.28 14.20 13 -6 2 78.59 14.60 -14 -5 2 0.00 16.20 -13 -5 2 75.29 14.30 -12 -5 2 55.09 7.60 -11 -5 2 81.79 8.60 -10 -5 2 14.20 5.70 -9 -5 2 51.69 4.30 -8 -5 2 101.69 5.70 -7 -5 2 5.30 2.10 -6 -5 2 0.00 8.50 -5 -5 2 484.15 7.50 -4 -5 2 170.08 11.00 -3 -5 2 616.74 7.20 -2 -5 2 9.10 3.60 -1 -5 2 24.60 1.40 0 -5 2 1030.60 14.90 1 -5 2 1365.76 11.20 2 -5 2 723.73 10.40 3 -5 2 2555.24 19.30 4 -5 2 2015.50 24.60 5 -5 2 1499.45 14.30 6 -5 2 546.65 9.00 7 -5 2 464.15 9.70 8 -5 2 300.57 9.50 9 -5 2 115.39 6.60 10 -5 2 29.90 5.60 11 -5 2 50.49 5.70 12 -5 2 1.20 6.80 13 -5 2 8.00 6.60 -14 -4 2 3.20 9.00 -13 -4 2 84.99 14.10 -12 -4 2 35.00 6.80 -11 -4 2 16.80 10.90 -10 -4 2 40.80 4.70 -9 -4 2 46.30 3.60 -8 -4 2 330.37 7.10 -7 -4 2 495.75 7.90 -6 -4 2 325.77 6.40 -5 -4 2 1436.16 13.00 -4 -4 2 327.07 11.20 -3 -4 2 1517.35 12.40 -2 -4 2 1145.39 13.00 -1 -4 2 3359.06 22.50 0 -4 2 1652.43 17.00 1 -4 2 374.46 4.30 2 -4 2 2024.70 15.50 3 -4 2 1726.73 14.90 4 -4 2 147.29 5.40 5 -4 2 105.69 3.80 6 -4 2 123.09 7.70 7 -4 2 115.09 5.30 8 -4 2 27.10 5.20 9 -4 2 27.40 3.80 10 -4 2 190.28 7.70 11 -4 2 10.00 3.20 12 -4 2 6.80 6.20 13 -4 2 37.30 6.30 14 -4 2 65.19 45.00 -14 -3 2 37.20 27.80 -13 -3 2 90.49 15.20 -12 -3 2 107.89 10.00 -11 -3 2 430.46 16.50 -10 -3 2 242.48 12.50 -9 -3 2 143.39 7.60 -8 -3 2 1772.62 20.90 -7 -3 2 1100.79 12.40 -6 -3 2 1390.86 15.00 -5 -3 2 2697.43 22.90 -4 -3 2 1700.83 23.40 -3 -3 2 1230.08 10.30 -2 -3 2 3040.30 28.20 -1 -3 2 177.08 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2 2 693.13 8.20 8 2 2 786.62 10.40 9 2 2 431.56 7.90 10 2 2 9.40 4.00 11 2 2 82.99 5.20 12 2 2 6.10 4.70 13 2 2 12.70 3.50 14 2 2 89.39 21.80 15 2 2 55.49 15.90 -13 3 2 0.00 16.20 -12 3 2 2.30 12.80 -11 3 2 37.50 10.30 -10 3 2 122.59 10.70 -9 3 2 331.67 10.90 -8 3 2 254.17 9.30 -7 3 2 1188.98 14.10 -6 3 2 1593.44 14.90 -5 3 2 1386.06 13.20 -4 3 2 2220.08 21.80 -3 3 2 3554.44 27.30 -2 3 2 1896.41 25.70 -1 3 2 305.87 3.70 0 3 2 3075.29 30.80 1 3 2 90.39 1.70 2 3 2 1805.52 14.40 3 3 2 342.47 4.20 4 3 2 1254.17 11.80 5 3 2 9.60 1.40 6 3 2 831.52 17.20 7 3 2 6.90 1.50 8 3 2 23.60 5.60 9 3 2 416.26 7.10 10 3 2 76.49 4.60 11 3 2 146.49 7.60 12 3 2 96.69 8.80 13 3 2 175.28 8.90 14 3 2 193.28 22.60 15 3 2 9.10 10.10 -13 4 2 15.60 57.99 -12 4 2 237.78 22.80 -11 4 2 209.48 15.40 -10 4 2 674.83 19.70 -9 4 2 192.38 8.10 -8 4 2 1089.09 14.60 -7 4 2 590.94 8.40 -6 4 2 1860.11 19.60 -5 4 2 865.31 9.50 -4 4 2 2107.89 19.80 -3 4 2 1401.86 12.70 -2 4 2 617.54 11.20 -1 4 2 193.38 3.10 0 4 2 16.40 3.50 1 4 2 1121.29 8.60 2 4 2 47.80 2.80 3 4 2 429.16 4.60 4 4 2 39.70 2.10 5 4 2 1.80 1.20 6 4 2 4.30 2.80 7 4 2 445.16 6.80 8 4 2 136.09 8.60 9 4 2 172.58 5.60 10 4 2 90.49 4.80 11 4 2 2.10 2.00 12 4 2 12.10 5.20 13 4 2 9.70 3.80 14 4 2 6.00 13.10 15 4 2 7.60 9.00 -13 5 2 73.79 71.29 -12 5 2 225.98 15.60 -11 5 2 356.16 18.90 -10 5 2 212.98 12.90 -9 5 2 607.54 11.80 -8 5 2 1239.58 17.60 -7 5 2 679.53 10.70 -6 5 2 42.30 3.60 -5 5 2 297.07 5.40 -4 5 2 21.90 3.30 -3 5 2 51.89 2.70 -2 5 2 496.25 7.10 -1 5 2 13.40 1.40 0 5 2 599.04 12.30 1 5 2 1445.86 11.10 2 5 2 2861.01 20.60 3 5 2 883.61 7.80 4 5 2 320.97 5.50 5 5 2 141.49 4.50 6 5 2 294.87 5.80 7 5 2 2.20 1.40 8 5 2 14.90 6.50 9 5 2 162.98 5.40 10 5 2 20.40 5.30 11 5 2 37.00 3.80 12 5 2 8.10 4.30 13 5 2 116.59 6.70 14 5 2 162.68 22.20 15 5 2 96.39 15.40 -12 6 2 149.69 18.80 -11 6 2 330.07 22.30 -10 6 2 134.49 10.50 -9 6 2 151.98 7.90 -8 6 2 13.00 10.40 -7 6 2 199.68 8.10 -6 6 2 153.48 6.00 -5 6 2 30.50 2.70 -4 6 2 61.39 3.90 -3 6 2 186.78 4.30 -2 6 2 24.50 4.30 -1 6 2 528.85 7.10 0 6 2 1205.68 19.20 1 6 2 58.09 2.20 2 6 2 17.80 7.00 3 6 2 87.99 2.70 4 6 2 338.37 5.60 5 6 2 2.00 1.40 6 6 2 54.39 3.70 7 6 2 102.69 4.00 8 6 2 89.09 4.30 9 6 2 49.00 3.30 10 6 2 557.94 13.40 11 6 2 799.42 13.20 12 6 2 407.76 10.50 13 6 2 372.66 9.60 14 6 2 472.65 17.60 15 6 2 178.68 19.10 -12 7 2 0.00 56.39 -11 7 2 21.90 8.60 -10 7 2 11.40 8.00 -9 7 2 54.09 5.80 -8 7 2 3.90 7.10 -7 7 2 6.70 11.10 -6 7 2 155.28 8.50 -5 7 2 435.36 8.40 -4 7 2 2.90 3.10 -3 7 2 260.47 5.70 -2 7 2 4.40 3.30 -1 7 2 489.75 6.60 0 7 2 31.90 5.10 1 7 2 5.20 1.30 2 7 2 3.70 4.70 3 7 2 679.13 7.90 4 7 2 483.25 7.90 5 7 2 644.94 8.10 6 7 2 1641.84 16.10 7 7 2 736.73 10.10 8 7 2 884.51 11.20 9 7 2 842.22 11.90 10 7 2 1513.25 21.90 11 7 2 367.06 9.40 12 7 2 514.75 12.50 13 7 2 141.19 7.10 14 7 2 206.88 11.70 15 7 2 154.48 49.80 -12 8 2 15.80 21.50 -11 8 2 42.50 10.90 -10 8 2 96.29 10.20 -9 8 2 85.09 6.90 -8 8 2 189.68 9.50 -7 8 2 74.09 6.60 -6 8 2 18.30 6.60 -5 8 2 8.40 2.70 -4 8 2 79.39 6.60 -3 8 2 117.29 4.70 -2 8 2 248.08 6.10 -1 8 2 551.34 7.60 0 8 2 758.32 9.60 1 8 2 785.32 9.10 2 8 2 2487.05 22.30 3 8 2 174.48 4.00 4 8 2 1475.25 20.80 5 8 2 2506.95 21.20 6 8 2 642.94 9.10 7 8 2 1366.66 14.60 8 8 2 424.36 8.20 9 8 2 611.54 9.90 10 8 2 273.17 8.90 11 8 2 622.24 12.80 12 8 2 133.59 9.70 13 8 2 41.70 4.80 14 8 2 0.00 9.30 15 8 2 58.99 42.60 -11 9 2 28.00 19.20 -10 9 2 15.60 7.30 -9 9 2 81.89 9.10 -8 9 2 26.90 6.00 -7 9 2 9.30 6.20 -6 9 2 89.79 9.20 -5 9 2 247.98 9.10 -4 9 2 410.96 13.50 -3 9 2 675.83 10.40 -2 9 2 895.31 12.50 -1 9 2 756.92 9.90 0 9 2 2157.68 19.70 1 9 2 2281.87 19.90 2 9 2 669.63 8.60 3 9 2 981.70 10.30 4 9 2 1259.87 15.70 5 9 2 700.83 8.80 6 9 2 260.37 7.30 7 9 2 1137.89 13.90 8 9 2 242.08 7.00 9 9 2 25.10 3.00 10 9 2 5.00 4.00 11 9 2 3.50 2.60 12 9 2 7.80 5.00 13 9 2 21.40 4.30 14 9 2 0.00 9.40 15 9 2 82.99 36.00 -10 10 2 63.39 14.70 -9 10 2 47.00 9.20 -8 10 2 86.89 8.10 -7 10 2 681.53 15.80 -6 10 2 490.65 12.20 -5 10 2 250.87 10.00 -4 10 2 596.44 14.20 -3 10 2 1433.26 17.10 -2 10 2 1316.77 23.30 -1 10 2 973.40 11.80 0 10 2 521.05 9.40 1 10 2 218.88 5.60 2 10 2 1030.80 13.60 3 10 2 463.25 7.70 4 10 2 57.79 3.60 5 10 2 13.20 2.00 6 10 2 61.69 8.90 7 10 2 107.29 4.70 8 10 2 80.69 6.40 9 10 2 31.20 3.90 10 10 2 9.30 6.10 11 10 2 3.20 2.60 12 10 2 67.19 7.10 13 10 2 54.49 6.20 14 10 2 70.89 15.20 -10 11 2 227.28 31.30 -9 11 2 428.16 27.90 -8 11 2 534.05 17.00 -7 11 2 643.04 18.60 -6 11 2 454.95 13.80 -5 11 2 1032.10 20.70 -4 11 2 485.15 15.10 -3 11 2 573.44 13.20 -2 11 2 232.28 15.50 -1 11 2 497.95 10.00 0 11 2 37.60 6.40 1 11 2 44.80 3.10 2 11 2 8.40 3.10 3 11 2 60.49 3.40 4 11 2 5.10 2.40 5 11 2 3.60 1.80 6 11 2 5.40 5.70 7 11 2 99.79 5.00 8 11 2 25.20 7.10 9 11 2 11.00 3.30 10 11 2 140.59 8.40 11 11 2 46.50 5.50 12 11 2 8.60 6.60 13 11 2 8.30 4.60 14 11 2 6.00 8.90 -9 12 2 189.18 19.10 -8 12 2 233.98 15.10 -7 12 2 220.88 12.70 -6 12 2 197.98 14.20 -5 12 2 116.39 10.50 -4 12 2 18.00 8.50 -3 12 2 2.40 3.50 -2 12 2 0.00 6.60 -1 12 2 41.80 4.50 0 12 2 29.90 9.00 1 12 2 3.80 2.40 2 12 2 116.59 5.40 3 12 2 116.79 5.20 4 12 2 29.50 4.00 5 12 2 187.78 6.70 6 12 2 40.10 4.10 7 12 2 8.10 2.50 8 12 2 3.40 8.60 9 12 2 2.20 3.10 10 12 2 15.00 8.80 11 12 2 65.79 6.10 12 12 2 108.59 10.00 13 12 2 113.99 8.20 14 12 2 80.09 12.20 -8 13 2 38.60 13.70 -7 13 2 0.00 15.40 -6 13 2 29.30 8.20 -5 13 2 0.00 8.20 -4 13 2 4.40 6.20 -3 13 2 71.49 7.30 -2 13 2 97.69 9.10 -1 13 2 70.09 6.40 0 13 2 263.77 17.10 1 13 2 112.39 6.30 2 13 2 83.69 9.10 3 13 2 16.50 3.10 4 13 2 80.29 6.30 5 13 2 1.50 2.30 6 13 2 44.40 5.00 7 13 2 234.68 8.80 8 13 2 278.07 10.60 9 13 2 46.30 5.20 10 13 2 223.38 12.90 11 13 2 289.37 12.30 12 13 2 479.45 16.20 13 13 2 323.27 17.80 -7 14 2 0.00 13.60 -6 14 2 26.70 11.90 -5 14 2 96.29 14.40 -4 14 2 56.79 9.30 -3 14 2 0.90 3.50 -2 14 2 58.69 8.30 -1 14 2 32.10 5.40 0 14 2 49.90 6.80 1 14 2 100.59 6.70 2 14 2 8.00 7.30 3 14 2 156.38 7.30 4 14 2 226.08 11.20 5 14 2 249.48 8.50 6 14 2 404.86 10.10 7 14 2 594.34 12.10 8 14 2 394.36 11.70 9 14 2 271.77 10.20 10 14 2 416.26 14.00 11 14 2 490.45 13.70 12 14 2 194.48 15.50 13 14 2 46.10 8.60 -6 15 2 44.90 15.20 -5 15 2 0.00 12.90 -4 15 2 27.50 12.90 -3 15 2 27.00 10.90 -2 15 2 78.69 9.60 -1 15 2 155.08 10.00 0 15 2 363.36 14.90 1 15 2 226.78 10.20 2 15 2 260.27 11.40 3 15 2 440.36 12.30 4 15 2 498.05 14.10 5 15 2 329.47 10.50 6 15 2 407.56 14.60 7 15 2 615.54 13.30 8 15 2 281.87 9.50 9 15 2 235.28 10.70 10 15 2 134.59 10.10 11 15 2 62.79 7.50 12 15 2 143.59 22.10 -5 16 2 63.49 12.50 -4 16 2 188.98 39.80 -3 16 2 282.07 19.90 -2 16 2 223.48 12.40 -1 16 2 563.44 18.60 0 16 2 349.07 13.80 1 16 2 433.56 13.90 2 16 2 465.05 12.80 3 16 2 347.47 11.50 4 16 2 171.68 8.80 5 16 2 168.18 8.50 6 16 2 100.29 8.10 7 16 2 257.27 10.80 8 16 2 75.49 8.60 9 16 2 32.20 6.00 10 16 2 0.20 9.50 11 16 2 2.80 5.10 -4 17 2 245.68 20.60 -3 17 2 503.75 61.59 -2 17 2 257.97 15.00 -1 17 2 121.29 11.50 0 17 2 231.08 14.20 1 17 2 185.78 14.10 2 17 2 183.88 11.00 3 17 2 40.10 5.70 4 17 2 83.09 8.70 5 17 2 34.10 6.40 6 17 2 29.90 10.80 7 17 2 18.20 4.60 8 17 2 71.09 9.60 9 17 2 12.30 5.20 10 17 2 36.60 9.90 -2 18 2 49.60 16.10 -1 18 2 35.90 12.60 0 18 2 64.69 12.20 1 18 2 35.90 6.70 2 18 2 5.70 6.10 3 18 2 34.00 5.20 4 18 2 11.10 5.50 5 18 2 10.00 4.10 6 18 2 31.40 7.50 7 18 2 48.50 7.50 8 18 2 78.39 20.10 9 18 2 5.90 7.40 1 19 2 79.19 56.39 2 19 2 59.69 21.50 3 19 2 14.00 13.40 4 19 2 146.69 51.09 5 19 2 5.50 9.70 6 19 2 15.20 13.70 7 19 2 10.30 7.00 -4 -18 3 0.00 92.29 -3 -18 3 46.40 19.80 -2 -18 3 0.00 110.69 -1 -18 3 106.89 51.19 -7 -17 3 22.30 17.30 -6 -17 3 86.19 44.30 -5 -17 3 35.10 20.80 -4 -17 3 126.29 72.89 -3 -17 3 192.98 28.60 -2 -17 3 291.97 47.80 -1 -17 3 180.98 31.20 0 -17 3 362.86 25.50 1 -17 3 304.37 36.40 2 -17 3 276.97 37.50 -8 -16 3 61.89 16.90 -7 -16 3 186.68 16.90 -6 -16 3 247.88 23.50 -5 -16 3 297.07 17.80 -4 -16 3 323.87 25.20 -3 -16 3 309.57 16.50 -2 -16 3 332.17 29.40 -1 -16 3 390.66 26.30 0 -16 3 226.38 17.90 1 -16 3 115.19 14.90 2 -16 3 68.89 9.40 3 -16 3 107.59 61.89 4 -16 3 84.19 17.80 -10 -15 3 196.18 128.49 -9 -15 3 142.29 26.10 -8 -15 3 277.47 19.20 -7 -15 3 462.05 34.40 -6 -15 3 562.04 23.70 -5 -15 3 476.05 20.20 -4 -15 3 202.18 12.00 -3 -15 3 164.58 10.90 -2 -15 3 160.48 10.90 -1 -15 3 250.47 12.50 0 -15 3 16.40 5.50 1 -15 3 53.19 11.00 2 -15 3 6.50 5.70 3 -15 3 0.30 12.20 4 -15 3 7.60 4.90 5 -15 3 36.40 12.50 6 -15 3 8.70 9.20 -11 -14 3 311.37 27.20 -10 -14 3 176.38 15.20 -9 -14 3 176.38 12.60 -8 -14 3 181.18 13.70 -7 -14 3 198.48 14.20 -6 -14 3 257.27 13.90 -5 -14 3 9.00 6.30 -4 -14 3 35.70 8.90 -3 -14 3 3.20 6.40 -2 -14 3 6.20 5.70 -1 -14 3 49.99 7.20 0 -14 3 76.59 7.40 1 -14 3 43.10 9.00 2 -14 3 27.10 5.90 3 -14 3 126.59 9.70 4 -14 3 71.59 9.30 5 -14 3 7.50 6.10 6 -14 3 3.60 3.50 7 -14 3 1.10 8.70 -11 -13 3 81.79 12.20 -10 -13 3 78.69 13.00 -9 -13 3 107.49 12.30 -8 -13 3 33.40 6.90 -7 -13 3 0.00 7.60 -6 -13 3 0.00 8.90 -5 -13 3 37.90 8.80 -4 -13 3 1.80 8.90 -3 -13 3 13.40 7.80 -2 -13 3 22.80 6.60 -1 -13 3 184.18 9.50 0 -13 3 3.60 3.80 1 -13 3 20.20 7.20 2 -13 3 105.39 7.10 3 -13 3 23.40 8.40 4 -13 3 29.90 5.90 5 -13 3 42.90 12.20 6 -13 3 50.69 6.90 7 -13 3 57.59 9.30 8 -13 3 103.79 12.90 -12 -12 3 24.90 18.60 -11 -12 3 6.50 7.40 -10 -12 3 3.90 10.60 -9 -12 3 35.00 7.10 -8 -12 3 35.30 6.80 -7 -12 3 21.10 6.50 -6 -12 3 8.30 7.00 -5 -12 3 84.59 8.70 -4 -12 3 22.60 4.50 -3 -12 3 134.09 10.90 -2 -12 3 2.00 6.10 -1 -12 3 32.80 7.30 0 -12 3 34.10 6.00 1 -12 3 75.79 7.80 2 -12 3 107.99 5.50 3 -12 3 401.16 10.80 4 -12 3 254.27 9.60 5 -12 3 154.58 11.40 6 -12 3 288.47 12.70 7 -12 3 393.46 17.70 8 -12 3 332.37 14.80 9 -12 3 173.08 20.90 -12 -11 3 16.80 13.70 -11 -11 3 0.00 10.10 -10 -11 3 75.29 11.60 -9 -11 3 0.00 7.30 -8 -11 3 125.59 7.90 -7 -11 3 9.30 6.90 -6 -11 3 13.90 5.50 -5 -11 3 0.00 6.40 -4 -11 3 25.40 5.60 -3 -11 3 39.10 8.90 -2 -11 3 19.10 5.80 -1 -11 3 346.57 15.90 0 -11 3 525.65 15.90 1 -11 3 372.86 15.20 2 -11 3 318.87 8.40 3 -11 3 1172.88 20.80 4 -11 3 444.76 12.50 5 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7.00 5 -9 3 5.40 4.30 6 -9 3 24.40 3.50 7 -9 3 6.10 3.70 8 -9 3 95.19 7.00 9 -9 3 112.39 11.50 10 -9 3 53.09 8.60 11 -9 3 68.19 12.50 -13 -8 3 142.19 13.90 -12 -8 3 231.48 15.30 -11 -8 3 508.35 12.70 -10 -8 3 649.24 15.90 -9 -8 3 591.24 15.20 -8 -8 3 857.31 19.10 -7 -8 3 1258.67 20.00 -6 -8 3 712.13 12.20 -5 -8 3 827.32 12.20 -4 -8 3 373.26 7.70 -3 -8 3 267.77 9.30 -2 -8 3 15.60 2.30 -1 -8 3 326.57 7.00 0 -8 3 2.40 1.50 1 -8 3 23.80 9.50 2 -8 3 40.30 2.60 3 -8 3 34.50 4.20 4 -8 3 24.50 2.50 5 -8 3 117.79 5.90 6 -8 3 62.79 4.90 7 -8 3 3.00 3.60 8 -8 3 207.58 9.00 9 -8 3 83.49 12.10 10 -8 3 5.20 4.30 11 -8 3 37.10 8.90 12 -8 3 4.40 5.80 -14 -7 3 262.27 25.20 -13 -7 3 281.67 19.10 -12 -7 3 482.15 18.00 -11 -7 3 477.65 14.70 -10 -7 3 318.57 12.00 -9 -7 3 242.58 8.20 -8 -7 3 338.77 10.60 -7 -7 3 143.49 7.70 -6 -7 3 0.40 5.20 -5 -7 3 0.00 5.00 -4 -7 3 17.80 2.80 -3 -7 3 10.50 2.70 -2 -7 3 255.77 4.50 -1 -7 3 11.10 2.80 0 -7 3 3.30 1.50 1 -7 3 32.40 2.50 2 -7 3 6.40 1.50 3 -7 3 574.04 11.30 4 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7.40 1.70 1 -5 3 906.51 15.50 2 -5 3 10.20 1.20 3 -5 3 1141.29 10.90 4 -5 3 206.98 4.90 5 -5 3 1145.59 22.50 6 -5 3 1138.69 12.90 7 -5 3 1280.77 17.20 8 -5 3 223.28 9.40 9 -5 3 743.33 16.10 10 -5 3 578.44 14.30 11 -5 3 365.66 10.50 12 -5 3 373.86 15.40 13 -5 3 242.38 14.40 -14 -4 3 0.00 530.75 -13 -4 3 37.70 9.30 -12 -4 3 97.09 10.90 -11 -4 3 74.39 8.20 -10 -4 3 175.58 13.00 -9 -4 3 13.60 3.80 -8 -4 3 262.07 6.50 -7 -4 3 49.00 3.90 -6 -4 3 185.08 5.20 -5 -4 3 116.09 4.00 -4 -4 3 1185.48 11.40 -3 -4 3 693.63 10.40 -2 -4 3 94.49 2.80 -1 -4 3 733.53 10.10 0 -4 3 838.92 9.90 1 -4 3 893.51 10.40 2 -4 3 2761.62 20.10 3 -4 3 1043.30 11.10 4 -4 3 3653.23 26.90 5 -4 3 3113.99 25.80 6 -4 3 1263.07 14.00 7 -4 3 1368.66 19.00 8 -4 3 638.64 11.90 9 -4 3 411.56 10.30 10 -4 3 197.08 8.80 11 -4 3 44.70 6.10 12 -4 3 62.19 6.00 13 -4 3 13.80 6.00 14 -4 3 8.10 16.20 -14 -3 3 20.00 18.00 -13 -3 3 6.90 6.60 -12 -3 3 31.00 6.50 -11 -3 3 21.70 6.50 -10 -3 3 7.80 8.80 -9 -3 3 23.70 6.80 -8 -3 3 776.42 14.30 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0 3 15.00 1.70 7 0 3 30.00 4.10 8 0 3 54.49 3.90 9 0 3 20.10 4.60 10 0 3 226.38 7.30 11 0 3 51.89 5.60 12 0 3 239.68 8.00 13 0 3 361.26 11.00 14 0 3 254.17 13.40 15 0 3 67.09 76.59 -14 1 3 192.68 49.50 -13 1 3 86.79 11.50 -12 1 3 65.59 13.10 -11 1 3 79.69 8.00 -10 1 3 130.29 7.50 -9 1 3 28.80 4.70 -8 1 3 13.70 5.30 -7 1 3 3.40 3.70 -6 1 3 86.19 4.90 -5 1 3 178.38 7.10 -4 1 3 158.38 4.40 -3 1 3 1618.24 15.80 -2 1 3 2679.03 18.20 -1 1 3 132.29 2.50 0 1 3 1369.76 10.30 1 1 3 270.57 3.50 2 1 3 205.48 2.70 3 1 3 181.28 5.60 4 1 3 1376.96 11.30 5 1 3 439.16 17.60 6 1 3 1222.68 12.50 7 1 3 183.08 5.40 8 1 3 592.34 9.10 9 1 3 729.43 12.40 10 1 3 535.25 10.70 11 1 3 1034.90 17.50 12 1 3 801.92 14.20 13 1 3 469.75 12.40 14 1 3 351.56 19.00 15 1 3 139.59 116.29 -13 2 3 59.99 16.10 -12 2 3 28.80 18.80 -11 2 3 5.20 5.30 -10 2 3 0.90 5.60 -9 2 3 45.90 6.60 -8 2 3 151.88 7.70 -7 2 3 121.79 5.30 -6 2 3 236.28 6.30 -5 2 3 119.89 4.50 -4 2 3 640.84 9.50 -3 2 3 728.83 9.20 -2 2 3 507.75 5.00 -1 2 3 111.09 2.10 0 2 3 57.49 1.30 1 2 3 806.32 8.80 2 2 3 510.85 4.90 3 2 3 1676.43 13.20 4 2 3 1347.27 10.80 5 2 3 435.86 7.20 6 2 3 2620.44 20.80 7 2 3 2819.52 28.40 8 2 3 2082.49 19.50 9 2 3 241.18 7.10 10 2 3 550.94 10.50 11 2 3 520.65 11.00 12 2 3 305.17 9.10 13 2 3 141.79 7.30 14 2 3 72.09 10.80 15 2 3 142.99 33.90 -13 3 3 59.49 21.60 -12 3 3 18.70 13.90 -11 3 3 7.60 7.30 -10 3 3 63.79 7.80 -9 3 3 250.87 9.10 -8 3 3 9.50 5.40 -7 3 3 5.00 3.70 -6 3 3 16.50 3.20 -5 3 3 53.99 3.00 -4 3 3 142.79 3.30 -3 3 3 1368.56 16.00 -2 3 3 1303.27 10.80 -1 3 3 384.86 6.20 0 3 3 1591.34 11.60 1 3 3 1165.28 10.30 2 3 3 2946.81 20.00 3 3 3 4308.77 32.90 4 3 3 556.54 6.30 5 3 3 3643.64 31.20 6 3 3 613.54 7.80 7 3 3 558.74 14.90 8 3 3 124.89 4.20 9 3 3 331.27 8.40 10 3 3 725.63 12.80 11 3 3 1.80 4.30 12 3 3 3.60 2.70 13 3 3 7.50 4.30 14 3 3 4.20 5.00 15 3 3 16.20 21.60 -13 4 3 8.80 26.90 -12 4 3 0.00 8.30 -11 4 3 30.40 12.00 -10 4 3 56.99 13.60 -9 4 3 10.50 4.60 -8 4 3 428.16 12.90 -7 4 3 176.88 7.30 -6 4 3 607.14 9.50 -5 4 3 1169.28 12.90 -4 4 3 897.11 10.20 -3 4 3 910.71 12.30 -2 4 3 634.84 6.90 -1 4 3 4826.32 53.99 0 4 3 8222.08 87.99 1 4 3 694.83 6.90 2 4 3 272.77 3.50 3 4 3 1622.14 13.00 4 4 3 13.60 1.40 5 4 3 289.37 8.10 6 4 3 140.59 4.00 7 4 3 89.59 4.20 8 4 3 182.88 5.10 9 4 3 33.40 4.40 10 4 3 7.00 2.10 11 4 3 38.70 4.40 12 4 3 5.20 2.90 13 4 3 78.69 6.30 14 4 3 52.49 6.90 15 4 3 71.29 15.70 -13 5 3 35.80 15.00 -12 5 3 82.99 15.50 -11 5 3 277.77 16.60 -10 5 3 349.37 13.30 -9 5 3 645.44 19.40 -8 5 3 817.42 16.60 -7 5 3 604.34 10.30 -6 5 3 973.00 11.90 -5 5 3 3780.52 32.90 -4 5 3 932.21 11.40 -3 5 3 1405.86 16.40 -2 5 3 629.64 7.60 -1 5 3 27.60 4.90 0 5 3 1962.40 17.10 1 5 3 85.19 10.60 2 5 3 29.60 1.40 3 5 3 405.76 5.70 4 5 3 1.10 1.00 5 5 3 36.80 2.60 6 5 3 7.50 1.60 7 5 3 299.27 6.30 8 5 3 79.59 3.80 9 5 3 51.29 6.60 10 5 3 299.07 7.30 11 5 3 37.20 7.40 12 5 3 4.20 2.20 13 5 3 23.60 4.70 14 5 3 7.30 4.70 15 5 3 0.00 10.80 -12 6 3 289.27 31.20 -11 6 3 362.06 22.20 -10 6 3 488.25 17.10 -9 6 3 664.63 15.90 -8 6 3 985.30 18.50 -7 6 3 791.42 21.70 -6 6 3 160.08 9.70 -5 6 3 403.56 9.00 -4 6 3 491.25 8.40 -3 6 3 148.59 7.70 -2 6 3 460.05 6.50 -1 6 3 185.38 9.20 0 6 3 292.77 5.00 1 6 3 123.19 5.90 2 6 3 750.62 7.70 3 6 3 29.70 6.20 4 6 3 5.00 1.30 5 6 3 5.90 2.50 6 6 3 112.89 4.00 7 6 3 53.29 3.10 8 6 3 5.40 1.70 9 6 3 182.58 5.90 10 6 3 11.40 2.50 11 6 3 119.69 10.40 12 6 3 51.49 4.40 13 6 3 39.20 6.80 14 6 3 177.18 11.00 15 6 3 87.49 17.40 -12 7 3 240.08 68.79 -11 7 3 220.18 13.60 -10 7 3 56.39 7.60 -9 7 3 86.19 7.30 -8 7 3 56.39 7.10 -7 7 3 24.70 8.50 -6 7 3 13.50 9.60 -5 7 3 221.58 11.50 -4 7 3 72.49 5.10 -3 7 3 53.69 4.10 -2 7 3 164.18 5.30 -1 7 3 80.09 5.00 0 7 3 23.90 2.00 1 7 3 766.22 14.40 2 7 3 180.28 3.70 3 7 3 0.70 5.80 4 7 3 123.69 3.70 5 7 3 2.00 4.50 6 7 3 28.80 2.50 7 7 3 9.00 2.40 8 7 3 79.29 4.00 9 7 3 209.08 6.00 10 7 3 116.69 5.50 11 7 3 178.48 7.10 12 7 3 175.98 7.60 13 7 3 326.67 11.90 14 7 3 297.17 11.70 15 7 3 372.46 28.50 -11 8 3 15.60 10.90 -10 8 3 53.19 11.20 -9 8 3 6.80 8.30 -8 8 3 13.60 5.50 -7 8 3 74.79 6.40 -6 8 3 8.70 4.70 -5 8 3 13.10 7.00 -4 8 3 8.80 4.00 -3 8 3 682.53 11.50 -2 8 3 192.78 5.00 -1 8 3 21.60 4.20 0 8 3 27.80 2.40 1 8 3 389.36 6.90 2 8 3 148.99 3.60 3 8 3 0.00 5.40 4 8 3 826.82 9.40 5 8 3 144.39 12.50 6 8 3 83.89 3.90 7 8 3 654.53 9.90 8 8 3 361.36 7.20 9 8 3 359.96 7.90 10 8 3 490.15 10.80 11 8 3 433.16 10.50 12 8 3 353.56 10.40 13 8 3 299.07 11.20 14 8 3 272.97 11.50 15 8 3 237.58 31.50 -11 9 3 8.20 18.00 -10 9 3 36.80 10.40 -9 9 3 80.09 7.60 -8 9 3 84.99 6.80 -7 9 3 11.00 5.00 -6 9 3 37.30 5.70 -5 9 3 40.30 7.00 -4 9 3 50.89 5.70 -3 9 3 38.40 8.90 -2 9 3 13.90 2.60 -1 9 3 135.49 6.90 0 9 3 107.09 4.80 1 9 3 73.89 3.70 2 9 3 593.14 7.80 3 9 3 1301.07 13.70 4 9 3 231.68 4.90 5 9 3 2068.29 24.60 6 9 3 1451.95 14.70 7 9 3 729.83 15.80 8 9 3 553.44 10.30 9 9 3 638.64 10.70 10 9 3 363.76 9.00 11 9 3 340.07 10.00 12 9 3 119.19 7.10 13 9 3 105.89 7.40 14 9 3 32.50 5.30 15 9 3 46.20 20.80 -10 10 3 31.60 16.40 -9 10 3 1.90 4.60 -8 10 3 34.40 6.80 -7 10 3 14.40 6.90 -6 10 3 3.90 6.30 -5 10 3 258.47 10.70 -4 10 3 33.20 5.40 -3 10 3 403.36 11.10 -2 10 3 304.47 10.90 -1 10 3 497.05 15.30 0 10 3 1224.18 15.00 1 10 3 1898.41 22.30 2 10 3 1187.08 12.50 3 10 3 572.44 12.60 4 10 3 1602.84 16.50 5 10 3 2729.73 27.80 6 10 3 803.72 10.20 7 10 3 33.90 8.20 8 10 3 205.38 7.10 9 10 3 46.40 6.90 10 10 3 175.28 8.10 11 10 3 21.00 5.70 12 10 3 6.70 3.40 13 10 3 6.60 8.30 14 10 3 7.10 4.10 15 10 3 37.30 15.50 -10 11 3 50.09 34.80 -9 11 3 82.29 9.90 -8 11 3 170.88 13.50 -7 11 3 143.29 9.20 -6 11 3 468.85 15.10 -5 11 3 518.55 15.90 -4 11 3 434.36 11.50 -3 11 3 673.83 13.70 -2 11 3 601.24 12.30 -1 11 3 738.83 16.50 0 11 3 2500.05 27.00 1 11 3 1552.04 18.90 2 11 3 709.63 9.60 3 11 3 260.87 5.80 4 11 3 388.56 6.60 5 11 3 61.69 4.20 6 11 3 18.10 2.70 7 11 3 0.10 3.00 8 11 3 31.20 3.90 9 11 3 107.89 9.70 10 11 3 59.09 6.00 11 11 3 23.60 7.10 12 11 3 30.10 4.80 13 11 3 52.79 7.30 14 11 3 13.40 6.00 -9 12 3 263.37 32.40 -8 12 3 259.77 19.40 -7 12 3 358.96 17.80 -6 12 3 460.85 19.30 -5 12 3 646.54 17.00 -4 12 3 789.52 23.50 -3 12 3 250.17 11.40 -2 12 3 236.68 10.40 -1 12 3 82.29 10.60 0 12 3 289.47 11.20 1 12 3 50.69 8.00 2 12 3 28.90 3.30 3 12 3 112.19 5.70 4 12 3 4.40 2.00 5 12 3 145.29 6.10 6 12 3 34.50 3.30 7 12 3 111.29 5.70 8 12 3 46.40 4.40 9 12 3 0.00 7.20 10 12 3 73.09 7.00 11 12 3 0.00 7.00 12 12 3 37.40 5.70 13 12 3 11.70 5.70 14 12 3 1.20 4.20 -8 13 3 312.67 24.40 -7 13 3 304.17 22.50 -6 13 3 176.58 16.90 -5 13 3 97.69 11.30 -4 13 3 30.70 8.70 -3 13 3 134.59 19.70 -2 13 3 5.00 7.50 -1 13 3 69.09 11.00 0 13 3 89.89 8.70 1 13 3 6.50 9.30 2 13 3 315.27 9.60 3 13 3 66.49 9.50 4 13 3 113.89 5.90 5 13 3 10.20 5.70 6 13 3 5.20 2.50 7 13 3 7.30 3.40 8 13 3 139.99 7.00 9 13 3 7.60 4.80 10 13 3 2.10 3.10 11 13 3 46.80 8.50 12 13 3 4.10 3.60 13 13 3 23.50 9.70 14 13 3 69.29 7.80 -7 14 3 45.40 12.10 -6 14 3 1.70 11.40 -5 14 3 26.80 11.20 -4 14 3 9.10 10.60 -3 14 3 92.09 8.50 -2 14 3 89.59 9.40 -1 14 3 0.00 8.00 0 14 3 77.39 7.50 1 14 3 79.99 7.70 2 14 3 20.70 3.90 3 14 3 116.09 10.80 4 14 3 24.20 3.30 5 14 3 0.10 7.40 6 14 3 140.09 6.40 7 14 3 6.20 4.10 8 14 3 101.29 6.20 9 14 3 89.29 9.30 10 14 3 393.26 13.80 11 14 3 273.67 11.70 12 14 3 162.58 10.90 13 14 3 383.16 18.70 -6 15 3 0.00 13.50 -5 15 3 43.00 13.30 -4 15 3 116.69 13.00 -3 15 3 67.99 9.80 -2 15 3 9.30 8.90 -1 15 3 2.90 7.30 0 15 3 8.70 5.10 1 15 3 65.99 7.70 2 15 3 61.49 5.70 3 15 3 123.99 9.00 4 15 3 85.89 5.80 5 15 3 365.56 12.00 6 15 3 279.27 9.50 7 15 3 448.66 13.20 8 15 3 698.03 16.80 9 15 3 202.18 11.20 10 15 3 455.65 14.50 11 15 3 359.46 12.40 12 15 3 207.88 12.10 -5 16 3 35.40 12.10 -4 16 3 30.10 19.70 -3 16 3 29.00 12.50 -2 16 3 76.09 12.60 -1 16 3 132.39 11.60 0 16 3 107.89 9.50 1 16 3 327.87 14.40 2 16 3 398.66 13.00 3 16 3 474.25 14.50 4 16 3 398.26 13.20 5 16 3 422.06 14.30 6 16 3 509.45 14.40 7 16 3 512.55 15.90 8 16 3 363.56 11.90 9 16 3 164.88 9.40 10 16 3 232.28 13.70 11 16 3 104.69 10.00 12 16 3 26.20 7.40 -4 17 3 177.18 25.00 -3 17 3 112.69 15.90 -2 17 3 0.00 76.19 -1 17 3 352.86 20.80 0 17 3 347.87 20.40 1 17 3 361.86 16.40 2 17 3 220.38 13.50 3 17 3 327.67 12.70 4 17 3 303.37 12.30 5 17 3 367.46 15.20 6 17 3 217.48 13.20 7 17 3 86.89 15.90 8 17 3 60.09 7.30 9 17 3 80.39 9.90 10 17 3 1.90 4.00 11 17 3 0.00 15.00 -2 18 3 276.67 30.00 -1 18 3 252.17 22.30 0 18 3 134.39 12.80 1 18 3 175.18 13.40 2 18 3 103.39 10.20 3 18 3 221.58 10.70 4 18 3 114.49 8.00 5 18 3 18.50 5.60 6 18 3 14.00 5.60 7 18 3 9.40 7.60 8 18 3 10.90 5.20 9 18 3 32.40 13.80 0 19 3 32.90 10.00 1 19 3 47.20 16.80 2 19 3 19.90 17.10 3 19 3 47.80 16.80 4 19 3 13.40 8.00 5 19 3 19.60 10.60 6 19 3 19.00 10.20 7 19 3 16.70 14.60 8 19 3 28.80 9.10 -6 -17 4 14.70 13.50 -5 -17 4 0.00 59.49 -4 -17 4 2.10 46.70 -3 -17 4 43.70 60.79 -2 -17 4 0.00 87.49 -1 -17 4 0.00 65.69 0 -17 4 119.39 221.88 2 -17 4 90.29 22.40 -8 -16 4 9.10 9.10 -7 -16 4 58.89 24.80 -6 -16 4 79.49 24.20 -5 -16 4 67.39 15.30 -4 -16 4 86.79 17.20 -3 -16 4 130.39 14.70 -2 -16 4 234.48 16.00 -1 -16 4 203.78 21.10 0 -16 4 289.77 24.90 1 -16 4 440.26 45.50 2 -16 4 326.97 32.00 3 -16 4 220.28 39.40 4 -16 4 158.58 158.98 -9 -15 4 51.29 23.30 -8 -15 4 144.59 44.00 -7 -15 4 160.18 19.70 -6 -15 4 247.78 26.10 -5 -15 4 167.58 28.00 -4 -15 4 441.86 29.20 -3 -15 4 524.75 21.90 -2 -15 4 499.25 25.90 -1 -15 4 194.88 16.00 0 -15 4 501.05 29.90 1 -15 4 501.65 25.80 2 -15 4 111.69 13.10 3 -15 4 116.89 12.40 4 -15 4 129.69 25.20 5 -15 4 7.50 9.60 -10 -14 4 174.88 44.60 -9 -14 4 313.37 14.90 -8 -14 4 355.56 17.20 -7 -14 4 461.85 22.00 -6 -14 4 133.99 18.60 -5 -14 4 347.87 17.00 -4 -14 4 510.05 18.70 -3 -14 4 198.58 11.90 -2 -14 4 128.99 9.80 -1 -14 4 228.88 12.10 0 -14 4 98.59 10.00 1 -14 4 36.90 7.70 2 -14 4 5.60 7.70 3 -14 4 26.80 8.60 4 -14 4 0.00 16.80 5 -14 4 3.20 4.70 6 -14 4 64.29 16.10 7 -14 4 46.00 9.20 -11 -13 4 237.98 21.60 -10 -13 4 480.45 24.40 -9 -13 4 251.77 15.70 -8 -13 4 207.48 13.30 -7 -13 4 154.88 9.00 -6 -13 4 224.88 10.60 -5 -13 4 36.90 7.80 -4 -13 4 33.50 11.80 -3 -13 4 53.59 12.90 -2 -13 4 49.50 8.30 -1 -13 4 10.40 6.80 0 -13 4 0.00 7.00 1 -13 4 55.49 7.80 2 -13 4 100.19 9.40 3 -13 4 28.00 6.90 4 -13 4 69.89 8.10 5 -13 4 30.30 6.00 6 -13 4 105.99 15.40 7 -13 4 2.20 5.30 8 -13 4 0.00 17.20 -11 -12 4 177.78 14.90 -10 -12 4 82.89 12.40 -9 -12 4 20.90 6.50 -8 -12 4 10.30 5.30 -7 -12 4 23.00 6.70 -6 -12 4 20.80 7.40 -5 -12 4 33.70 6.10 -4 -12 4 85.69 9.80 -3 -12 4 49.10 10.40 -2 -12 4 69.09 9.30 -1 -12 4 155.08 12.80 0 -12 4 106.49 8.70 1 -12 4 9.20 5.40 2 -12 4 35.40 6.90 3 -12 4 9.30 3.90 4 -12 4 3.50 4.90 5 -12 4 8.00 4.00 6 -12 4 61.29 10.60 7 -12 4 81.69 8.20 8 -12 4 21.60 9.90 9 -12 4 29.60 8.70 -12 -11 4 40.60 9.00 -11 -11 4 0.00 13.00 -10 -11 4 7.10 7.20 -9 -11 4 29.90 9.00 -8 -11 4 134.29 9.30 -7 -11 4 19.20 6.50 -6 -11 4 168.68 12.80 -5 -11 4 89.39 7.80 -4 -11 4 20.50 5.80 -3 -11 4 27.10 11.60 -2 -11 4 36.70 21.60 -1 -11 4 23.30 27.00 0 -11 4 0.00 17.40 1 -11 4 42.50 10.10 2 -11 4 179.78 9.10 3 -11 4 32.90 3.60 4 -11 4 29.20 6.70 5 -11 4 84.89 6.80 6 -11 4 203.58 9.70 7 -11 4 273.07 11.30 8 -11 4 416.36 17.90 9 -11 4 364.66 17.20 10 -11 4 207.58 20.40 -12 -10 4 8.20 6.20 -11 -10 4 56.49 9.50 -10 -10 4 40.00 7.00 -9 -10 4 51.89 8.80 -8 -10 4 13.40 4.80 -7 -10 4 5.20 5.40 -6 -10 4 41.00 6.80 -5 -10 4 0.00 7.60 -4 -10 4 8.00 3.70 -3 -10 4 180.28 8.10 -2 -10 4 298.37 11.90 -1 -10 4 10.30 6.30 0 -10 4 563.74 15.50 1 -10 4 387.76 12.50 2 -10 4 213.78 11.20 3 -10 4 338.17 10.40 4 -10 4 1410.26 21.10 5 -10 4 892.31 15.90 6 -10 4 607.74 14.00 7 -10 4 535.55 13.60 8 -10 4 645.74 17.40 9 -10 4 168.28 12.40 10 -10 4 226.98 13.60 -13 -9 4 6.70 11.10 -12 -9 4 13.90 5.50 -11 -9 4 6.70 6.10 -10 -9 4 3.80 3.60 -9 -9 4 93.29 8.20 -8 -9 4 39.90 6.90 -7 -9 4 111.49 7.90 -6 -9 4 142.99 7.50 -5 -9 4 53.39 5.00 -4 -9 4 170.38 5.60 -3 -9 4 886.31 11.20 -2 -9 4 495.65 10.00 -1 -9 4 1015.90 13.90 0 -9 4 1205.68 18.60 1 -9 4 866.01 14.00 2 -9 4 1780.92 24.20 3 -9 4 1213.58 18.00 4 -9 4 413.36 12.00 5 -9 4 346.57 9.70 6 -9 4 667.53 15.60 7 -9 4 314.07 9.50 8 -9 4 18.20 4.30 9 -9 4 11.90 4.20 10 -9 4 46.20 9.10 11 -9 4 8.30 5.40 -13 -8 4 6.00 8.40 -12 -8 4 34.60 7.30 -11 -8 4 56.89 7.30 -10 -8 4 60.59 5.60 -9 -8 4 184.58 8.00 -8 -8 4 624.94 14.80 -7 -8 4 531.45 14.50 -6 -8 4 571.44 13.90 -5 -8 4 1343.87 16.90 -4 -8 4 656.83 10.30 -3 -8 4 2120.99 21.20 -2 -8 4 1450.25 18.90 -1 -8 4 642.64 12.80 0 -8 4 522.95 14.50 1 -8 4 1630.84 20.60 2 -8 4 238.68 10.60 3 -8 4 306.17 6.40 4 -8 4 114.29 6.00 5 -8 4 103.79 5.60 6 -8 4 46.20 4.30 7 -8 4 10.10 2.80 8 -8 4 54.39 6.40 9 -8 4 5.70 3.80 10 -8 4 89.49 14.60 11 -8 4 67.89 9.50 12 -8 4 42.90 15.20 -13 -7 4 185.08 17.90 -12 -7 4 224.68 12.50 -11 -7 4 229.68 9.10 -10 -7 4 555.04 12.60 -9 -7 4 913.21 16.90 -8 -7 4 724.13 13.40 -7 -7 4 748.63 14.10 -6 -7 4 955.20 16.30 -5 -7 4 863.71 15.90 -4 -7 4 364.56 7.50 -3 -7 4 335.97 6.20 -2 -7 4 329.57 6.90 -1 -7 4 54.89 3.60 0 -7 4 568.34 8.50 1 -7 4 180.48 4.90 2 -7 4 2.40 3.00 3 -7 4 1.40 1.30 4 -7 4 29.30 9.00 5 -7 4 458.95 8.80 6 -7 4 266.77 8.00 7 -7 4 112.29 6.40 8 -7 4 146.49 7.70 9 -7 4 129.69 8.40 10 -7 4 31.10 7.50 11 -7 4 3.80 4.10 12 -7 4 30.00 10.80 -13 -6 4 436.66 23.20 -12 -6 4 285.37 14.70 -11 -6 4 423.76 19.40 -10 -6 4 1033.40 17.80 -9 -6 4 519.85 12.30 -8 -6 4 498.85 10.20 -7 -6 4 652.93 13.30 -6 -6 4 746.03 11.60 -5 -6 4 41.20 4.50 -4 -6 4 55.59 5.30 -3 -6 4 31.50 3.30 -2 -6 4 9.50 2.10 -1 -6 4 8.60 1.80 0 -6 4 509.05 10.70 1 -6 4 3.20 1.50 2 -6 4 527.65 7.20 3 -6 4 119.89 3.50 4 -6 4 282.67 11.30 5 -6 4 235.38 5.70 6 -6 4 67.59 9.30 7 -6 4 6.60 2.00 8 -6 4 17.30 4.50 9 -6 4 2.40 3.20 10 -6 4 1.80 5.30 11 -6 4 73.39 7.60 12 -6 4 121.89 10.20 13 -6 4 140.09 13.90 -14 -5 4 251.57 22.30 -13 -5 4 240.58 19.60 -12 -5 4 252.57 14.80 -11 -5 4 353.26 15.20 -10 -5 4 84.39 7.30 -9 -5 4 10.20 3.70 -8 -5 4 12.50 2.60 -7 -5 4 41.10 5.60 -6 -5 4 18.40 2.80 -5 -5 4 333.67 6.70 -4 -5 4 59.69 4.80 -3 -5 4 46.90 3.70 -2 -5 4 26.60 3.30 -1 -5 4 384.46 8.00 0 -5 4 83.09 4.60 1 -5 4 188.38 5.00 2 -5 4 75.19 2.80 3 -5 4 1.10 0.90 4 -5 4 0.00 2.40 5 -5 4 3.50 1.50 6 -5 4 556.14 11.60 7 -5 4 50.39 3.40 8 -5 4 366.56 12.60 9 -5 4 199.78 9.40 10 -5 4 248.98 11.40 11 -5 4 682.73 17.70 12 -5 4 344.47 14.70 13 -5 4 149.29 12.50 -14 -4 4 33.80 12.40 -13 -4 4 16.20 8.60 -12 -4 4 11.00 5.50 -11 -4 4 7.70 8.90 -10 -4 4 84.29 6.90 -9 -4 4 87.29 10.30 -8 -4 4 192.48 5.50 -7 -4 4 84.69 6.50 -6 -4 4 168.88 5.40 -5 -4 4 312.67 7.00 -4 -4 4 20.40 2.40 -3 -4 4 105.59 3.90 -2 -4 4 56.99 4.90 -1 -4 4 11.70 1.60 0 -4 4 4.80 3.10 1 -4 4 441.46 7.20 2 -4 4 64.79 3.20 3 -4 4 753.92 7.90 4 -4 4 994.50 11.20 5 -4 4 828.52 9.20 6 -4 4 375.06 7.70 7 -4 4 861.81 11.40 8 -4 4 762.92 18.60 9 -4 4 624.14 16.80 10 -4 4 529.85 14.10 11 -4 4 459.55 12.70 12 -4 4 256.57 12.50 13 -4 4 203.78 12.40 14 -4 4 69.89 42.60 -14 -3 4 20.60 10.70 -13 -3 4 26.60 8.60 -12 -3 4 69.99 7.00 -11 -3 4 116.29 8.50 -10 -3 4 25.00 5.50 -9 -3 4 0.00 7.60 -8 -3 4 424.86 10.60 -7 -3 4 84.39 5.10 -6 -3 4 0.70 1.40 -5 -3 4 68.89 3.90 -4 -3 4 3.50 1.50 -3 -3 4 88.99 3.00 -2 -3 4 61.89 2.60 -1 -3 4 2038.90 15.90 0 -3 4 5671.43 67.09 1 -3 4 556.64 7.40 2 -3 4 259.17 4.20 3 -3 4 2791.22 20.30 4 -3 4 748.93 10.00 5 -3 4 531.25 6.70 6 -3 4 825.12 10.00 7 -3 4 323.47 6.60 8 -3 4 562.94 12.70 9 -3 4 281.77 8.60 10 -3 4 135.49 9.80 11 -3 4 302.67 10.10 12 -3 4 132.09 7.00 13 -3 4 49.50 7.10 14 -3 4 11.20 15.70 -14 -2 4 25.80 13.80 -13 -2 4 89.39 11.20 -12 -2 4 39.40 6.70 -11 -2 4 6.20 5.50 -10 -2 4 42.80 5.30 -9 -2 4 48.10 8.20 -8 -2 4 137.59 7.00 -7 -2 4 104.19 9.70 -6 -2 4 122.69 5.50 -5 -2 4 466.95 7.80 -4 -2 4 470.35 6.50 -3 -2 4 1570.34 14.60 -2 -2 4 450.25 5.30 -1 -2 4 1481.95 11.60 0 -2 4 3395.06 25.00 1 -2 4 2552.84 17.20 2 -2 4 2313.77 29.90 3 -2 4 810.02 8.00 4 -2 4 506.95 7.50 5 -2 4 419.26 6.30 6 -2 4 845.62 12.30 7 -2 4 820.02 11.80 8 -2 4 141.79 5.30 9 -2 4 6.40 2.60 10 -2 4 24.70 7.90 11 -2 4 12.30 3.40 12 -2 4 25.40 8.80 13 -2 4 8.40 5.00 14 -2 4 47.90 10.80 -14 -1 4 13.70 20.40 -13 -1 4 21.30 13.50 -12 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39.00 6.10 4 14 8 45.40 7.00 5 14 8 87.29 6.00 6 14 8 46.50 6.60 7 14 8 330.97 12.60 8 14 8 425.46 15.20 9 14 8 290.37 10.80 10 14 8 241.88 11.20 11 14 8 530.65 18.20 12 14 8 503.55 16.80 13 14 8 424.26 26.00 14 14 8 177.58 15.20 -5 15 8 23.80 6.00 -4 15 8 3.00 3.60 -3 15 8 21.50 7.20 -2 15 8 1.10 3.20 -1 15 8 38.60 8.60 0 15 8 55.79 8.00 1 15 8 40.00 12.10 2 15 8 195.18 11.00 3 15 8 401.46 16.20 4 15 8 308.27 14.50 5 15 8 351.16 14.60 6 15 8 859.81 18.60 7 15 8 388.96 14.20 8 15 8 563.34 14.20 9 15 8 229.98 9.30 10 15 8 246.58 14.70 11 15 8 206.58 17.50 12 15 8 89.79 11.30 13 15 8 18.30 16.50 -4 16 8 30.40 7.30 -3 16 8 43.90 8.60 -2 16 8 132.99 10.70 -1 16 8 231.58 12.60 0 16 8 361.06 14.40 1 16 8 373.76 16.60 2 16 8 462.05 13.00 3 16 8 477.95 15.20 4 16 8 583.14 17.40 5 16 8 428.06 13.20 6 16 8 357.36 11.10 7 16 8 106.49 6.80 8 16 8 158.78 8.50 9 16 8 142.29 11.40 10 16 8 86.49 13.30 11 16 8 47.00 11.40 12 16 8 15.10 17.80 13 16 8 5.60 5.80 -3 17 8 156.48 16.10 -2 17 8 242.08 14.70 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23.40 21.80 3 -14 9 36.00 15.10 -7 -13 9 0.00 139.09 -6 -13 9 10.40 12.30 -5 -13 9 15.00 7.30 -4 -13 9 21.60 12.00 -3 -13 9 4.90 5.10 -2 -13 9 10.80 8.90 -1 -13 9 31.70 6.60 0 -13 9 12.70 11.50 1 -13 9 16.50 7.40 2 -13 9 24.90 12.10 3 -13 9 10.90 6.50 4 -13 9 59.49 22.70 5 -13 9 0.40 8.30 -8 -12 9 41.30 10.30 -7 -12 9 17.00 7.80 -6 -12 9 44.50 17.90 -5 -12 9 12.70 5.30 -4 -12 9 21.60 6.90 -3 -12 9 24.00 6.80 -2 -12 9 7.90 8.30 -1 -12 9 9.00 4.70 0 -12 9 0.00 8.80 1 -12 9 2.60 4.10 2 -12 9 9.60 29.70 3 -12 9 3.80 5.50 4 -12 9 76.69 11.90 5 -12 9 67.79 13.50 6 -12 9 23.60 18.90 7 -12 9 169.28 26.50 -8 -11 9 56.69 14.80 -7 -11 9 7.20 4.80 -6 -11 9 16.00 9.20 -5 -11 9 13.00 5.60 -4 -11 9 27.20 7.30 -3 -11 9 2.20 3.90 -2 -11 9 16.70 5.20 -1 -11 9 103.89 7.90 0 -11 9 33.80 6.30 1 -11 9 103.49 9.00 2 -11 9 229.68 11.90 3 -11 9 525.55 20.90 4 -11 9 322.47 21.90 5 -11 9 315.47 18.20 6 -11 9 371.96 17.30 7 -11 9 421.16 32.90 8 -11 9 398.46 177.18 -9 -10 9 24.80 7.80 -8 -10 9 17.60 7.70 -7 -10 9 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7.40 2 -8 9 71.19 8.60 3 -8 9 2.40 3.90 4 -8 9 23.50 7.70 5 -8 9 101.29 9.00 6 -8 9 102.29 5.90 7 -8 9 15.30 5.00 8 -8 9 0.00 8.80 9 -8 9 20.10 9.30 10 -8 9 81.49 36.10 11 -8 9 26.70 18.00 -11 -7 9 374.36 19.30 -10 -7 9 199.08 17.20 -9 -7 9 195.48 9.70 -8 -7 9 475.55 13.90 -7 -7 9 279.27 9.70 -6 -7 9 285.17 8.40 -5 -7 9 310.37 8.30 -4 -7 9 107.29 5.40 -3 -7 9 34.70 3.70 -2 -7 9 12.50 5.60 -1 -7 9 17.30 3.50 0 -7 9 562.34 19.10 1 -7 9 23.40 3.90 2 -7 9 120.89 9.60 3 -7 9 55.19 5.90 4 -7 9 31.80 6.70 5 -7 9 11.30 3.00 6 -7 9 136.49 7.40 7 -7 9 6.30 4.40 8 -7 9 17.20 6.50 9 -7 9 2.60 13.80 10 -7 9 0.00 11.20 11 -7 9 30.40 18.50 -11 -6 9 141.79 14.50 -10 -6 9 57.79 10.10 -9 -6 9 91.49 7.60 -8 -6 9 10.80 6.50 -7 -6 9 30.50 4.00 -6 -6 9 21.60 4.60 -5 -6 9 35.70 3.30 -4 -6 9 0.00 2.50 -3 -6 9 9.10 2.20 -2 -6 9 42.30 3.80 -1 -6 9 5.70 2.40 0 -6 9 127.39 7.10 1 -6 9 8.10 2.50 2 -6 9 83.69 7.00 3 -6 9 126.39 7.00 4 -6 9 26.60 4.20 5 -6 9 1.60 2.30 6 -6 9 7.70 5.00 7 -6 9 158.78 8.40 8 -6 9 173.58 7.80 9 -6 9 29.10 5.80 10 -6 9 257.57 20.90 11 -6 9 254.97 16.50 12 -6 9 267.47 31.70 -11 -5 9 5.60 5.90 -10 -5 9 17.90 6.60 -9 -5 9 1.90 3.50 -8 -5 9 7.90 6.70 -7 -5 9 63.99 4.50 -6 -5 9 30.20 7.40 -5 -5 9 77.69 4.20 -4 -5 9 13.40 3.70 -3 -5 9 287.67 6.70 -2 -5 9 14.20 2.00 -1 -5 9 137.39 3.90 0 -5 9 392.26 8.40 1 -5 9 8.90 2.00 2 -5 9 93.99 9.80 3 -5 9 338.97 8.20 4 -5 9 349.27 10.80 5 -5 9 253.47 8.30 6 -5 9 284.17 13.40 7 -5 9 191.48 8.50 8 -5 9 391.56 11.90 9 -5 9 544.35 13.90 10 -5 9 368.66 13.90 11 -5 9 382.76 23.00 12 -5 9 371.96 21.60 13 -5 9 470.85 37.10 -11 -4 9 14.60 6.20 -10 -4 9 0.00 6.80 -9 -4 9 80.79 6.70 -8 -4 9 54.29 6.50 -7 -4 9 7.40 2.60 -6 -4 9 54.79 8.10 -5 -4 9 40.20 3.40 -4 -4 9 100.99 5.10 -3 -4 9 20.00 2.50 -2 -4 9 239.68 5.50 -1 -4 9 220.08 4.80 0 -4 9 609.24 9.30 1 -4 9 930.41 10.90 2 -4 9 683.43 9.30 3 -4 9 234.58 5.60 4 -4 9 458.55 9.90 5 -4 9 254.77 8.10 6 -4 9 718.13 14.80 7 -4 9 542.05 12.90 8 -4 9 611.74 14.70 9 -4 9 336.67 11.00 10 -4 9 274.77 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17.40 5 3 20 368.16 15.00 6 3 20 404.36 17.70 7 3 20 431.06 19.90 8 3 20 310.37 19.60 9 3 20 259.07 21.10 10 3 20 85.09 17.40 -2 4 20 293.77 20.20 -1 4 20 207.78 12.40 0 4 20 389.86 17.30 1 4 20 186.88 12.00 2 4 20 301.67 12.90 3 4 20 184.08 10.20 4 4 20 295.47 16.10 5 4 20 212.98 12.00 6 4 20 258.87 13.20 7 4 20 26.90 8.90 8 4 20 32.50 11.10 9 4 20 11.90 8.60 10 4 20 0.00 13.70 11 4 20 0.00 18.30 -2 5 20 202.48 14.30 -1 5 20 217.48 13.30 0 5 20 318.87 22.30 1 5 20 200.38 11.60 2 5 20 35.50 7.10 3 5 20 82.09 8.50 4 5 20 36.80 8.30 5 5 20 16.90 6.10 6 5 20 7.20 7.80 7 5 20 13.00 6.40 8 5 20 51.09 10.00 9 5 20 13.80 11.80 10 5 20 44.70 16.10 11 5 20 81.49 21.00 -2 6 20 21.80 9.20 -1 6 20 142.99 10.60 0 6 20 43.70 10.50 1 6 20 12.00 5.50 2 6 20 18.60 9.10 3 6 20 2.70 3.90 4 6 20 43.30 11.60 5 6 20 39.10 8.60 6 6 20 44.90 10.50 7 6 20 59.09 7.30 8 6 20 5.80 10.30 9 6 20 25.80 10.40 10 6 20 20.30 15.90 11 6 20 6.00 9.80 -2 7 20 0.00 51.89 -1 7 20 7.90 6.60 0 7 20 1.80 7.70 1 7 20 7.20 4.80 2 7 20 33.20 9.70 3 7 20 82.69 10.20 4 7 20 20.80 12.10 5 7 20 9.30 6.00 6 7 20 0.00 8.00 7 7 20 12.70 6.50 8 7 20 34.20 9.70 9 7 20 10.40 8.10 10 7 20 77.19 14.70 11 7 20 81.49 19.90 -1 8 20 10.70 8.10 0 8 20 8.10 8.90 1 8 20 4.50 5.90 2 8 20 19.00 9.30 3 8 20 11.30 6.70 4 8 20 21.60 13.10 5 8 20 39.90 9.10 6 8 20 111.49 20.00 7 8 20 124.29 11.70 8 8 20 138.49 13.40 9 8 20 155.18 15.60 10 8 20 356.56 20.90 11 8 20 225.38 23.00 -1 9 20 19.30 8.20 0 9 20 9.10 9.40 1 9 20 29.30 8.50 2 9 20 104.79 12.60 3 9 20 193.48 15.40 4 9 20 299.17 19.10 5 9 20 253.57 17.20 6 9 20 262.77 21.90 7 9 20 359.16 16.70 8 9 20 203.58 15.20 9 9 20 232.18 19.70 10 9 20 179.28 20.50 11 9 20 266.97 27.20 0 10 20 116.19 16.00 1 10 20 136.79 17.30 2 10 20 309.37 18.50 3 10 20 285.27 15.60 4 10 20 343.37 23.50 5 10 20 277.17 20.90 6 10 20 441.96 23.90 7 10 20 325.27 17.20 8 10 20 127.79 15.80 9 10 20 171.38 17.90 10 10 20 156.48 21.20 11 10 20 16.40 19.50 0 11 20 177.88 28.70 1 11 20 249.88 18.30 2 11 20 188.58 21.40 3 11 20 140.49 14.70 4 11 20 86.09 20.50 5 11 20 151.68 15.30 6 11 20 181.78 17.20 7 11 20 6.50 8.60 8 11 20 0.00 14.30 9 11 20 12.90 15.90 10 11 20 9.30 15.30 1 12 20 60.89 12.80 2 12 20 0.00 21.30 3 12 20 18.00 14.70 4 12 20 0.00 14.30 5 12 20 3.60 8.40 6 12 20 23.20 14.80 7 12 20 2.00 7.30 8 12 20 0.00 11.60 9 12 20 28.60 37.80 10 12 20 50.99 17.10 2 13 20 271.57 1024.60 3 13 20 1.70 13.20 4 13 20 0.00 12.30 5 13 20 42.40 14.80 6 13 20 38.10 38.20 7 13 20 4.90 31.40 8 13 20 41.90 23.90 9 13 20 38.50 26.20 4 14 20 22.30 19.50 5 14 20 6.20 16.50 6 14 20 0.00 19.30 7 14 20 30.70 25.30 8 14 20 66.29 64.79 2 0 21 9.40 5.80 3 0 21 22.10 11.70 4 0 21 3.10 5.90 5 0 21 0.00 14.00 6 0 21 20.30 8.00 1 1 21 29.60 8.10 2 1 21 33.20 7.40 3 1 21 58.99 10.50 4 1 21 5.60 5.80 5 1 21 88.49 16.60 6 1 21 32.00 7.70 7 1 21 22.50 10.00 0 2 21 21.70 6.60 1 2 21 36.00 9.80 2 2 21 9.20 5.60 3 2 21 16.90 7.50 4 2 21 10.70 5.50 5 2 21 37.90 11.70 6 2 21 32.30 6.50 7 2 21 125.19 13.60 8 2 21 36.50 7.90 0 3 21 2.00 4.70 1 3 21 2.70 6.50 2 3 21 32.50 7.70 3 3 21 32.70 8.30 4 3 21 14.70 5.70 5 3 21 136.79 13.40 6 3 21 168.88 12.70 7 3 21 176.28 20.50 8 3 21 139.69 13.30 9 3 21 383.66 29.10 0 4 21 65.59 8.80 1 4 21 192.78 14.60 2 4 21 128.39 10.70 3 4 21 78.09 15.50 4 4 21 344.97 16.10 5 4 21 279.77 14.40 6 4 21 199.88 11.80 7 4 21 295.07 22.70 8 4 21 231.58 16.10 9 4 21 268.47 36.20 0 5 21 325.17 18.30 1 5 21 252.67 18.00 2 5 21 299.07 21.00 3 5 21 406.86 19.10 4 5 21 315.77 14.90 5 5 21 89.69 12.00 6 5 21 202.78 13.30 7 5 21 92.89 12.20 8 5 21 19.60 7.70 9 5 21 16.80 14.40 0 6 21 169.88 15.10 1 6 21 159.78 15.70 2 6 21 134.49 14.30 3 6 21 37.40 19.80 4 6 21 9.40 6.20 5 6 21 5.70 8.50 6 6 21 2.40 4.70 7 6 21 14.70 9.10 8 6 21 21.20 9.20 9 6 21 52.49 13.80 10 6 21 6.70 7.20 0 7 21 109.69 13.50 1 7 21 44.20 9.70 2 7 21 6.70 6.70 3 7 21 0.00 12.80 4 7 21 25.70 7.50 5 7 21 5.50 10.10 6 7 21 12.70 6.70 7 7 21 11.50 11.60 8 7 21 26.80 8.00 9 7 21 19.40 10.30 10 7 21 5.70 9.50 0 8 21 12.90 15.10 1 8 21 13.20 10.10 2 8 21 17.00 7.30 3 8 21 10.60 10.20 4 8 21 18.90 10.50 5 8 21 44.40 14.50 6 8 21 19.60 6.60 7 8 21 28.00 13.40 8 8 21 7.10 6.40 9 8 21 15.80 13.70 10 8 21 3.70 8.40 1 9 21 17.80 13.70 2 9 21 26.20 8.20 3 9 21 3.00 8.20 4 9 21 8.30 8.30 5 9 21 1.00 13.90 6 9 21 23.30 9.00 7 9 21 116.99 23.50 8 9 21 20.90 9.80 9 9 21 116.19 27.00 10 9 21 136.99 34.40 2 10 21 25.60 12.80 3 10 21 106.09 14.70 4 10 21 84.59 12.80 5 10 21 254.37 19.40 6 10 21 201.78 18.70 7 10 21 221.68 28.40 8 10 21 190.08 19.20 9 10 21 398.46 133.79 2 11 21 175.28 79.09 3 11 21 149.59 17.30 4 11 21 421.06 28.20 5 11 21 143.79 61.29 6 11 21 127.69 20.20 7 11 21 196.08 31.20 8 11 21 329.67 26.70 9 11 21 88.29 26.40 4 12 21 136.29 21.60 5 12 21 121.99 25.30 6 12 21 111.19 17.70 7 12 21 107.09 22.90 8 12 21 32.90 15.80 3 3 22 32.00 7.80 4 3 22 27.10 10.90 5 3 22 9.00 8.10 6 3 22 28.40 13.20 3 4 22 2.10 6.20 4 4 22 41.30 11.30 5 4 22 50.89 13.70 6 4 22 121.09 19.40 7 4 22 254.17 24.70 2 5 22 156.98 18.30 3 5 22 127.39 21.60 4 5 22 157.98 16.60 5 5 22 182.88 20.80 6 5 22 330.87 27.50 7 5 22 197.48 22.60 2 6 22 302.57 20.20 3 6 22 176.28 16.40 4 6 22 224.78 22.70 5 6 22 260.57 24.90 6 6 22 185.88 23.30 7 6 22 83.29 18.30 3 7 22 95.29 12.70 4 7 22 81.49 14.80 5 7 22 86.09 17.30 6 7 22 26.30 17.80 7 7 22 3.90 8.80 8 7 22 5.70 16.40 3 8 22 2.40 6.30 4 8 22 13.40 10.30 5 8 22 52.19 14.30 6 8 22 7.60 19.40 7 8 22 6.70 13.60 4 9 22 49.99 40.30 5 9 22 11.50 12.60 6 9 22 0.00 16.00 7 9 22 11.30 15.00 5 10 22 26.10 19.00 6 10 22 0.00 10.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 45007 _chemical_properties_physical Moisture-sensitive ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p21c_a _database_code_depnum_ccdc_archive 'CCDC 2151474' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-11 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C29 Al F36 N O17 Ru4' _chemical_formula_moiety 'C16 Al F36 O4, C13 N O13 Ru4' _chemical_formula_weight 1749.56 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 15.639(14) _cell_length_b 15.156(14) _cell_length_c 41.36(4) _cell_angle_alpha 90 _cell_angle_beta 95.87(2) _cell_angle_gamma 90 _cell_volume 9752(15) _cell_formula_units_Z 8 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9931 _cell_measurement_theta_min 2.2595 _cell_measurement_theta_max 24.2605 _exptl_crystal_description plate _exptl_crystal_colour red _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: 1,2,3,4-Tetrafluorobenzene, n-pentane' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.383 _exptl_crystal_F_000 6640 _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 1.440 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.5889 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment ? _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _olex2_diffrn_ambient_temperature_device 'Bruker Kryoflex II' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'sealed X-ray tube' _diffrn_source_type ? _diffrn_source_voltage 50.0 _diffrn_source_current 0.6 _diffrn_detector 'Image Plate' _diffrn_detector_type 'Rigaku Image Plate' _diffrn_detector_area_resol_mean ? _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Rigaku R-AXIS SPIDER' _diffrn_measurement_method '\w scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 135688 _diffrn_reflns_av_unetI/netI 0.0867 _diffrn_reflns_av_R_equivalents 0.1000 _diffrn_reflns_theta_min 0.990 _diffrn_reflns_theta_max 28.022 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -54 _diffrn_reflns_limit_l_max 54 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 23163 _reflns_number_gt 15319 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS 2018.9.0.3/05-Dec-2018 && APEX3_2019.1-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0306P)^2^+3.5066P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_number_reflns 23163 _refine_ls_number_parameters 1966 _refine_ls_number_restraints 19111 _refine_ls_R_factor_all 0.0889 _refine_ls_R_factor_gt 0.0436 _refine_ls_wR_factor_ref 0.0867 _refine_ls_wR_factor_gt 0.0740 _refine_ls_goodness_of_fit_ref 1.005 _refine_ls_restrained_S_all 0.832 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.807 _refine_diff_density_min -1.028 _refine_diff_density_rms 0.157 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru2 Ru 0.71154(2) 0.73078(3) 0.24042(2) 0.01755(9) Uani 1 1 d . . . . . Ru3 Ru 0.73086(2) 0.80388(2) 0.30215(2) 0.01551(9) Uani 1 1 d . . . . . Ru4 Ru 0.69386(2) 0.91248(2) 0.24771(2) 0.01676(9) Uani 1 1 d . . . . . Ru5 Ru 0.34458(2) 0.26179(3) 0.49871(2) 0.01687(9) Uani 1 1 d . . . . . Ru6 Ru 0.25543(2) 0.13070(3) 0.52792(2) 0.01577(9) Uani 1 1 d . . . . . Ru7 Ru 0.12301(2) 0.24783(3) 0.53253(2) 0.01696(9) Uani 1 1 d . . . . . Ru8 Ru 0.17863(2) 0.21484(3) 0.47134(2) 0.01697(9) Uani 1 1 d . . . . . Al1 Al 0.71183(9) 0.33930(9) 0.39687(3) 0.0136(3) Uani 1 1 d . . . . . Al2 Al 0.78539(8) 0.32872(9) 0.14863(3) 0.0130(3) Uani 1 1 d . . . . . Ru1 Ru 0.84169(2) 0.84108(3) 0.22410(2) 0.01836(10) Uani 1 1 d . . . . . O1 O 0.8218(2) 0.8480(3) 0.14924(8) 0.0372(10) Uani 1 1 d . . . . . O2 O 0.9675(2) 0.9956(3) 0.23185(8) 0.0348(10) Uani 1 1 d . . . . . O3 O 0.9909(2) 0.7120(3) 0.22824(9) 0.0404(10) Uani 1 1 d . . . . . O4 O 0.6652(2) 1.0086(2) 0.18156(8) 0.0347(10) Uani 1 1 d . . . . . O5 O 0.8106(2) 1.0618(2) 0.27749(8) 0.0312(9) Uani 1 1 d . . . . . O6 O 0.5486(2) 0.9802(2) 0.28658(8) 0.0318(9) Uani 1 1 d . . . . . O7 O 0.7933(2) 0.9296(2) 0.35696(8) 0.0301(9) Uani 1 1 d . . . . . O8 O 0.5626(2) 0.7753(2) 0.33350(8) 0.0295(9) Uani 1 1 d . . . . . O9 O 0.8309(2) 0.6497(2) 0.33392(8) 0.0346(10) Uani 1 1 d . . . . . O10 O 0.5592(2) 0.6201(2) 0.25964(8) 0.0322(9) Uani 1 1 d . . . . . O11 O 0.8331(2) 0.5800(2) 0.25947(9) 0.0365(10) Uani 1 1 d . . . . . O12 O 0.6946(2) 0.6868(2) 0.16692(8) 0.0289(9) Uani 1 1 d . . . . . O13 O 0.5316(2) 0.8187(2) 0.21578(8) 0.0272(8) Uani 1 1 d . . . . . O14 O 0.4801(2) 0.3205(2) 0.55214(8) 0.0282(9) Uani 1 1 d . . . . . O15 O 0.4806(2) 0.1584(2) 0.46514(8) 0.0299(9) Uani 1 1 d . . . . . O16 O 0.3682(3) 0.4318(3) 0.46138(9) 0.0402(10) Uani 1 1 d . . . . . O17 O 0.2686(2) 0.2109(2) 0.40793(8) 0.0364(10) Uani 1 1 d . . . . . O18 O 0.1378(2) 0.4114(2) 0.45740(9) 0.0360(10) Uani 1 1 d . . . . . O19 O -0.0095(2) 0.1599(2) 0.45075(9) 0.0318(9) Uani 1 1 d . . . . . O20 O 0.4075(2) 0.0086(2) 0.51511(8) 0.0273(8) Uani 1 1 d . . . . . O21 O 0.3343(2) 0.1597(2) 0.59678(8) 0.0250(8) Uani 1 1 d . . . . . O22 O 0.1308(2) -0.0068(2) 0.55209(9) 0.0364(10) Uani 1 1 d . . . . . O23 O 0.1496(2) 0.2521(3) 0.60606(8) 0.0343(10) Uani 1 1 d . . . . . O24 O -0.0451(2) 0.1415(2) 0.53026(8) 0.0344(9) Uani 1 1 d . . . . . O25 O 0.0324(2) 0.4269(2) 0.52755(8) 0.0295(9) Uani 1 1 d . . . . . O26 O 0.1832(2) 0.0115(2) 0.46676(7) 0.0252(8) Uani 1 1 d . . . . . N1 N 0.2360(2) 0.2627(2) 0.51722(8) 0.0165(9) Uani 1 1 d . . . . . N2 N 0.7921(2) 0.8236(2) 0.26455(8) 0.0172(9) Uani 1 1 d . . . . . C1 C 0.8317(3) 0.8470(3) 0.17677(12) 0.0259(12) Uani 1 1 d . . . . . C2 C 0.9204(3) 0.9385(4) 0.22849(11) 0.0224(12) Uani 1 1 d . . . . . C3 C 0.9354(3) 0.7602(4) 0.22583(12) 0.0281(13) Uani 1 1 d . . . . . C4 C 0.6777(3) 0.9745(3) 0.20577(12) 0.0241(12) Uani 1 1 d . . . . . C5 C 0.7682(3) 1.0081(3) 0.26646(11) 0.0222(12) Uani 1 1 d . . . . . C6 C 0.6023(3) 0.9538(3) 0.27312(11) 0.0223(11) Uani 1 1 d . . . . . C7 C 0.7699(3) 0.8837(3) 0.33643(12) 0.0209(12) Uani 1 1 d . . . . . C8 C 0.6253(3) 0.7837(3) 0.32260(10) 0.0192(11) Uani 1 1 d . . . . . C9 C 0.7912(3) 0.7071(3) 0.32326(11) 0.0213(12) Uani 1 1 d . . . . . C10 C 0.6154(3) 0.6618(3) 0.25342(11) 0.0221(12) Uani 1 1 d . . . . . C11 C 0.7869(4) 0.6342(3) 0.25177(12) 0.0254(12) Uani 1 1 d . . . . . C12 C 0.7018(3) 0.7026(3) 0.19364(12) 0.0227(12) Uani 1 1 d . . . . . C13 C 0.5992(3) 0.8307(3) 0.22704(11) 0.0217(12) Uani 1 1 d . . . . . C14 C 0.4302(3) 0.2969(3) 0.53238(11) 0.0191(11) Uani 1 1 d . . . . . C15 C 0.4309(3) 0.1991(3) 0.47679(11) 0.0211(11) Uani 1 1 d . . . . . C16 C 0.3602(3) 0.3682(4) 0.47518(12) 0.0260(12) Uani 1 1 d . . . . . C17 C 0.2388(3) 0.2095(3) 0.43162(11) 0.0241(12) Uani 1 1 d . . . . . C18 C 0.1517(3) 0.3404(4) 0.46223(11) 0.0241(12) Uani 1 1 d . . . . . C19 C 0.0582(4) 0.1831(3) 0.45816(11) 0.0224(12) Uani 1 1 d . . . . . C20 C 0.3522(3) 0.0544(3) 0.51917(11) 0.0235(12) Uani 1 1 d . . . . . C21 C 0.3056(3) 0.1479(3) 0.57099(12) 0.0220(12) Uani 1 1 d . . . . . C22 C 0.1764(3) 0.0433(3) 0.54321(11) 0.0224(11) Uani 1 1 d . . . . . C23 C 0.1375(3) 0.2535(3) 0.57880(12) 0.0260(12) Uani 1 1 d . . . . . C24 C 0.0170(3) 0.1827(3) 0.53251(11) 0.0251(12) Uani 1 1 d . . . . . C25 C 0.0649(3) 0.3599(4) 0.52900(11) 0.0245(12) Uani 1 1 d . . . . . C26 C 0.1921(3) 0.0830(4) 0.47484(11) 0.0220(12) Uani 1 1 d . . . . . O1_1 O 0.7639(6) 0.2992(6) 0.18744(17) 0.0177(12) Uani 0.828(5) 1 d D U P A 1 C1_1 C 0.7175(4) 0.3142(4) 0.21270(14) 0.0179(10) Uani 0.828(5) 1 d D U P A 1 C2_1 C 0.6722(4) 0.4053(4) 0.21028(13) 0.0250(11) Uani 0.828(5) 1 d D U P A 1 F1_1 F 0.6027(3) 0.4041(3) 0.18879(12) 0.0314(12) Uani 0.828(5) 1 d D U P A 1 F2_1 F 0.6464(3) 0.4329(3) 0.23847(10) 0.0351(12) Uani 0.828(5) 1 d D U P A 1 F3_1 F 0.7237(5) 0.4673(5) 0.20011(17) 0.0320(15) Uani 0.828(5) 1 d D U P A 1 C3_1 C 0.7789(4) 0.3110(4) 0.24412(12) 0.0248(11) Uani 0.828(5) 1 d D U P A 1 F4_1 F 0.8334(3) 0.2435(5) 0.2441(2) 0.0345(14) Uani 0.828(5) 1 d D U P A 1 F5_1 F 0.8261(3) 0.3838(4) 0.24770(16) 0.0360(14) Uani 0.828(5) 1 d D U P A 1 F6_1 F 0.7366(3) 0.3008(3) 0.27055(9) 0.0370(12) Uani 0.828(5) 1 d D U P A 1 C4_1 C 0.6477(4) 0.2412(4) 0.21341(13) 0.0258(11) Uani 0.828(5) 1 d D U P A 1 F7_1 F 0.6818(3) 0.1659(3) 0.22595(15) 0.0340(12) Uani 0.828(5) 1 d D U P A 1 F8_1 F 0.5856(4) 0.2633(4) 0.23197(16) 0.0372(15) Uani 0.828(5) 1 d D U P A 1 F9_1 F 0.6113(6) 0.2235(5) 0.1838(2) 0.0319(14) Uani 0.828(5) 1 d D U P A 1 O1_2 O 0.765(3) 0.301(3) 0.1870(8) 0.019(4) Uani 0.172(5) 1 d D U P A 2 C1_2 C 0.7209(12) 0.3124(11) 0.2133(5) 0.021(2) Uani 0.172(5) 1 d D U P A 2 C2_2 C 0.7504(12) 0.2404(12) 0.2387(4) 0.027(3) Uani 0.172(5) 1 d D U P A 2 F1_2 F 0.8350(13) 0.230(2) 0.2412(10) 0.031(4) Uani 0.172(5) 1 d D U P A 2 F2_2 F 0.7252(16) 0.2590(14) 0.2677(4) 0.033(4) Uani 0.172(5) 1 d D U P A 2 F3_2 F 0.7145(14) 0.1627(12) 0.2299(6) 0.027(4) Uani 0.172(5) 1 d D U P A 2 C3_2 C 0.6233(11) 0.3018(13) 0.2033(4) 0.023(3) Uani 0.172(5) 1 d D U P A 2 F4_2 F 0.5911(15) 0.3719(13) 0.1866(6) 0.026(4) Uani 0.172(5) 1 d D U P A 2 F5_2 F 0.608(3) 0.231(2) 0.1842(9) 0.025(4) Uani 0.172(5) 1 d D U P A 2 F6_2 F 0.5770(19) 0.2908(19) 0.2285(7) 0.027(4) Uani 0.172(5) 1 d D U P A 2 C4_2 C 0.7400(12) 0.4046(11) 0.2282(4) 0.027(3) Uani 0.172(5) 1 d D U P A 2 F7_2 F 0.739(2) 0.466(2) 0.2051(7) 0.026(4) Uani 0.172(5) 1 d D U P A 2 F8_2 F 0.6844(13) 0.4286(16) 0.2491(5) 0.031(4) Uani 0.172(5) 1 d D U P A 2 F9_2 F 0.8187(14) 0.4077(18) 0.2442(8) 0.034(4) Uani 0.172(5) 1 d D U P A 2 O1_3 O 0.8480(2) 0.4227(3) 0.14772(9) 0.0159(7) Uani 0.956(3) 1 d D U P A 1 C1_3 C 0.9277(3) 0.4576(3) 0.15266(11) 0.0184(9) Uani 0.956(3) 1 d D U P A 1 C2_3 C 0.9923(3) 0.3957(3) 0.17237(12) 0.0247(10) Uani 0.956(3) 1 d D U P A 1 F1_3 F 1.02376(19) 0.3335(2) 0.15296(8) 0.0350(8) Uani 0.956(3) 1 d D U P A 1 F2_3 F 1.06091(19) 0.4384(2) 0.18699(7) 0.0282(8) Uani 0.956(3) 1 d D U P A 1 F3_3 F 0.95590(19) 0.3519(2) 0.19462(7) 0.0331(8) Uani 0.956(3) 1 d D U P A 1 C3_3 C 0.9219(3) 0.5445(3) 0.17157(12) 0.0294(11) Uani 0.956(3) 1 d D U P A 1 F4_3 F 0.8542(2) 0.5923(2) 0.16114(9) 0.0412(9) Uani 0.956(3) 1 d D U P A 1 F5_3 F 0.9127(2) 0.5252(2) 0.20336(7) 0.0408(9) Uani 0.956(3) 1 d D U P A 1 F6_3 F 0.9914(2) 0.5959(2) 0.17128(8) 0.0368(9) Uani 0.956(3) 1 d D U P A 1 C4_3 C 0.9610(3) 0.4771(4) 0.11916(11) 0.0266(10) Uani 0.956(3) 1 d D U P A 1 F7_3 F 0.9182(2) 0.5485(2) 0.10506(7) 0.0394(9) Uani 0.956(3) 1 d D U P A 1 F8_3 F 1.04408(18) 0.4983(2) 0.12169(7) 0.0328(8) Uani 0.956(3) 1 d D U P A 1 F9_3 F 0.9468(2) 0.4116(2) 0.09890(7) 0.0418(9) Uani 0.956(3) 1 d D U P A 1 O1_4 O 0.841(3) 0.420(4) 0.1460(15) 0.022(5) Uani 0.044(3) 1 d D U P A 2 C1_4 C 0.917(2) 0.461(2) 0.1512(7) 0.024(3) Uani 0.044(3) 1 d D U P A 2 C2_4 C 0.935(2) 0.519(3) 0.1219(7) 0.030(3) Uani 0.044(3) 1 d D U P A 2 F1_4 F 0.889(3) 0.593(3) 0.1234(12) 0.029(5) Uani 0.044(3) 1 d D U P A 2 F2_4 F 1.019(2) 0.539(4) 0.1229(13) 0.033(4) Uani 0.044(3) 1 d D U P A 2 F3_4 F 0.915(4) 0.476(4) 0.0940(8) 0.031(4) Uani 0.044(3) 1 d D U P A 2 C3_4 C 0.992(2) 0.394(2) 0.1579(9) 0.028(3) Uani 0.044(3) 1 d D U P A 2 F4_4 F 0.972(3) 0.332(3) 0.1787(13) 0.031(4) Uani 0.044(3) 1 d D U P A 2 F5_4 F 1.012(3) 0.360(3) 0.1297(11) 0.030(4) Uani 0.044(3) 1 d D U P A 2 F6_4 F 1.061(3) 0.434(4) 0.1732(13) 0.029(5) Uani 0.044(3) 1 d D U P A 2 C4_4 C 0.920(3) 0.522(2) 0.1816(8) 0.030(3) Uani 0.044(3) 1 d D U P A 2 F7_4 F 0.935(4) 0.470(3) 0.2077(8) 0.028(4) Uani 0.044(3) 1 d D U P A 2 F8_4 F 0.984(4) 0.580(4) 0.1811(14) 0.033(5) Uani 0.044(3) 1 d D U P A 2 F9_4 F 0.847(3) 0.567(3) 0.1814(14) 0.034(4) Uani 0.044(3) 1 d D U P A 2 O1_5 O 0.68858(18) 0.3493(2) 0.12625(7) 0.0152(7) Uani 1 1 d D U . . . C1_5 C 0.6464(3) 0.3919(3) 0.10067(10) 0.0155(10) Uani 1 1 d D U . . . C2_5 C 0.6619(3) 0.4928(3) 0.10296(11) 0.0216(11) Uani 1 1 d D U . . . F1_5 F 0.73866(16) 0.51462(17) 0.09310(6) 0.0252(7) Uani 1 1 d D U . . . F2_5 F 0.60253(17) 0.53916(18) 0.08462(6) 0.0290(7) Uani 1 1 d D U . . . F3_5 F 0.66226(17) 0.52025(17) 0.13354(6) 0.0263(7) Uani 1 1 d D U . . . C3_5 C 0.5494(3) 0.3723(3) 0.10083(10) 0.0199(10) Uani 1 1 d D U . . . F4_5 F 0.53566(16) 0.28831(17) 0.10754(6) 0.0234(6) Uani 1 1 d D U . . . F5_5 F 0.51611(16) 0.42067(18) 0.12361(6) 0.0258(7) Uani 1 1 d D U . . . F6_5 F 0.50424(17) 0.39165(19) 0.07231(6) 0.0274(7) Uani 1 1 d D U . . . C4_5 C 0.6769(3) 0.3575(3) 0.06824(10) 0.0191(10) Uani 1 1 d D U . . . F7_5 F 0.64336(17) 0.27909(17) 0.06044(6) 0.0249(7) Uani 1 1 d D U . . . F8_5 F 0.65418(18) 0.41272(19) 0.04324(6) 0.0279(7) Uani 1 1 d D U . . . F9_5 F 0.76178(16) 0.34989(17) 0.07074(6) 0.0225(6) Uani 1 1 d D U . . . O1_6 O 0.84445(19) 0.24508(19) 0.13332(7) 0.0174(7) Uani 1 1 d D U . . . C1_6 C 0.8497(3) 0.1571(3) 0.12827(10) 0.0187(10) Uani 1 1 d D U . . . C2_6 C 0.8883(3) 0.1107(3) 0.15995(10) 0.0203(10) Uani 1 1 d D U . . . F1_6 F 0.82889(17) 0.10385(18) 0.18105(6) 0.0261(7) Uani 1 1 d D U . . . F2_6 F 0.91532(18) 0.02866(18) 0.15475(7) 0.0304(7) Uani 1 1 d D U . . . F3_6 F 0.95352(18) 0.15542(19) 0.17464(7) 0.0301(7) Uani 1 1 d D U . . . C3_6 C 0.9108(3) 0.1424(3) 0.10122(11) 0.0232(11) Uani 1 1 d D U . . . F4_6 F 0.89604(18) 0.20167(18) 0.07766(6) 0.0317(8) Uani 1 1 d D U . . . F5_6 F 0.99340(18) 0.1516(2) 0.11310(7) 0.0365(8) Uani 1 1 d D U . . . F6_6 F 0.90239(19) 0.06286(18) 0.08771(7) 0.0329(8) Uani 1 1 d D U . . . C4_6 C 0.7604(3) 0.1169(3) 0.11687(10) 0.0214(11) Uani 1 1 d D U . . . F7_6 F 0.73683(19) 0.13609(19) 0.08583(6) 0.0328(7) Uani 1 1 d D U . . . F8_6 F 0.75921(18) 0.02876(17) 0.11952(7) 0.0296(7) Uani 1 1 d D U . . . F9_6 F 0.70108(16) 0.14900(18) 0.13437(6) 0.0262(7) Uani 1 1 d D U . . . O1_8 O 0.79924(18) 0.3577(2) 0.37567(7) 0.0181(7) Uani 1 1 d D U . . . C1_8 C 0.8844(3) 0.3480(3) 0.37315(10) 0.0183(10) Uani 1 1 d D U . . . C2_8 C 0.9393(3) 0.3901(3) 0.40228(11) 0.0243(11) Uani 1 1 d D U . . . F1_8 F 0.94176(18) 0.3389(2) 0.42865(6) 0.0321(7) Uani 1 1 d D U . . . F2_8 F 1.02068(17) 0.40329(19) 0.39604(7) 0.0309(7) Uani 1 1 d D U . . . F3_8 F 0.90749(19) 0.46745(19) 0.41004(7) 0.0347(8) Uani 1 1 d D U . . . C3_8 C 0.9036(3) 0.3961(3) 0.34126(11) 0.0269(12) Uani 1 1 d D U . . . F4_8 F 0.84423(19) 0.3778(2) 0.31735(6) 0.0427(9) Uani 1 1 d D U . . . F5_8 F 0.90582(18) 0.4830(2) 0.34538(7) 0.0363(8) Uani 1 1 d D U . . . F6_8 F 0.97995(17) 0.3713(2) 0.33168(7) 0.0377(8) Uani 1 1 d D U . . . C4_8 C 0.9093(3) 0.2494(3) 0.37087(12) 0.0291(12) Uani 1 1 d D U . . . F7_8 F 0.88513(19) 0.2170(2) 0.34139(8) 0.0427(9) Uani 1 1 d D U . . . F8_8 F 0.99390(17) 0.2357(2) 0.37736(8) 0.0390(8) Uani 1 1 d D U . . . F9_8 F 0.87025(19) 0.20197(19) 0.39223(8) 0.0388(8) Uani 1 1 d D U . . . O1_9 O 0.7458(2) 0.3531(2) 0.43756(7) 0.0221(8) Uani 1 1 d D U . . . C1_9 C 0.7312(3) 0.3337(3) 0.46858(10) 0.0244(11) Uani 1 1 d D U . . . C2_9 C 0.7462(3) 0.2342(4) 0.47554(12) 0.0357(13) Uani 1 1 d D U . . . F1_9 F 0.6780(2) 0.1862(2) 0.46429(7) 0.0413(8) Uani 1 1 d D U . . . F2_9 F 0.7624(2) 0.2170(2) 0.50725(7) 0.0548(10) Uani 1 1 d D U . . . F3_9 F 0.8124(2) 0.2044(2) 0.46103(8) 0.0552(11) Uani 1 1 d D U . . . C3_9 C 0.7952(4) 0.3879(4) 0.49142(12) 0.0515(17) Uani 1 1 d D U . . . F4_9 F 0.7999(2) 0.4711(3) 0.48097(7) 0.0650(12) Uani 1 1 d D U . . . F5_9 F 0.8738(2) 0.3541(3) 0.49255(8) 0.0748(13) Uani 1 1 d D U . . . F6_9 F 0.7730(2) 0.3918(3) 0.52184(7) 0.0662(12) Uani 1 1 d D U . . . C4_9 C 0.6379(3) 0.3588(3) 0.47490(11) 0.0291(12) Uani 1 1 d D U . . . F7_9 F 0.6290(2) 0.4457(2) 0.47775(7) 0.0447(9) Uani 1 1 d D U . . . F8_9 F 0.61462(19) 0.3216(2) 0.50203(6) 0.0414(9) Uani 1 1 d D U . . . F9_9 F 0.58200(17) 0.3322(2) 0.45026(7) 0.0307(7) Uani 1 1 d D U . . . O1_10 O 0.66970(19) 0.2346(2) 0.39145(7) 0.0177(7) Uani 1 1 d D U . . . C1_10 C 0.6239(3) 0.1789(3) 0.37104(10) 0.0170(10) Uani 1 1 d D U . . . C2_10 C 0.6422(3) 0.0837(3) 0.38351(12) 0.0275(12) Uani 1 1 d D U . . . F1_10 F 0.59897(19) 0.06481(19) 0.40875(7) 0.0356(8) Uani 1 1 d D U . . . F2_10 F 0.61982(18) 0.02319(19) 0.36026(7) 0.0340(7) Uani 1 1 d D U . . . F3_10 F 0.72508(18) 0.07249(19) 0.39297(7) 0.0371(8) Uani 1 1 d D U . . . C3_10 C 0.6497(3) 0.1875(3) 0.33576(11) 0.0272(12) Uani 1 1 d D U . . . F4_10 F 0.65998(19) 0.27226(19) 0.32842(6) 0.0335(8) Uani 1 1 d D U . . . F5_10 F 0.72366(19) 0.1464(2) 0.33269(7) 0.0406(8) Uani 1 1 d D U . . . F6_10 F 0.59101(19) 0.15418(19) 0.31322(6) 0.0348(8) Uani 1 1 d D U . . . C4_10 C 0.5261(3) 0.1976(3) 0.37015(11) 0.0246(11) Uani 1 1 d D U . . . F7_10 F 0.50311(18) 0.26842(18) 0.35218(7) 0.0300(7) Uani 1 1 d D U . . . F8_10 F 0.47857(18) 0.13010(19) 0.35803(7) 0.0340(7) Uani 1 1 d D U . . . F9_10 F 0.50433(18) 0.2139(2) 0.39997(6) 0.0346(8) Uani 1 1 d D U . . . O1_11 O 0.6317(14) 0.4104(10) 0.3833(5) 0.021(4) Uani 0.58(3) 1 d D U P B 1 C1_11 C 0.6090(8) 0.4944(8) 0.3750(3) 0.025(2) Uani 0.58(3) 1 d D U P B 1 C2_11 C 0.6687(8) 0.5628(8) 0.3937(3) 0.028(3) Uani 0.58(3) 1 d D U P B 1 F1_11 F 0.7466(8) 0.5621(12) 0.3834(4) 0.034(3) Uani 0.58(3) 1 d D U P B 1 F2_11 F 0.6391(7) 0.6464(6) 0.3908(3) 0.034(2) Uani 0.58(3) 1 d D U P B 1 F3_11 F 0.6803(11) 0.5463(10) 0.4254(3) 0.038(3) Uani 0.58(3) 1 d D U P B 1 C3_11 C 0.5148(8) 0.5090(9) 0.3830(4) 0.035(3) Uani 0.58(3) 1 d D U P B 1 F4_11 F 0.4656(10) 0.4412(9) 0.3726(5) 0.043(3) Uani 0.58(3) 1 d D U P B 1 F5_11 F 0.5134(12) 0.5147(13) 0.4151(3) 0.048(4) Uani 0.58(3) 1 d D U P B 1 F6_11 F 0.4810(10) 0.5828(8) 0.3699(5) 0.063(4) Uani 0.58(3) 1 d D U P B 1 C4_11 C 0.6143(8) 0.5060(7) 0.3380(3) 0.034(3) Uani 0.58(3) 1 d D U P B 1 F7_11 F 0.5496(9) 0.4662(9) 0.3201(4) 0.047(3) Uani 0.58(3) 1 d D U P B 1 F8_11 F 0.6138(11) 0.5906(5) 0.3287(2) 0.047(3) Uani 0.58(3) 1 d D U P B 1 F9_11 F 0.6867(6) 0.4710(10) 0.3295(2) 0.043(3) Uani 0.58(3) 1 d D U P B 1 O1_12 O 0.6315(18) 0.4164(12) 0.3849(7) 0.016(5) Uani 0.42(3) 1 d D U P B 2 C1_12 C 0.6077(10) 0.4994(10) 0.3760(3) 0.020(3) Uani 0.42(3) 1 d D U P B 2 C2_12 C 0.6705(10) 0.5677(10) 0.3933(4) 0.023(3) Uani 0.42(3) 1 d D U P B 2 F1_12 F 0.6591(13) 0.5716(14) 0.4248(3) 0.034(4) Uani 0.42(3) 1 d D U P B 2 F2_12 F 0.6612(11) 0.6489(7) 0.3805(4) 0.029(3) Uani 0.42(3) 1 d D U P B 2 F3_12 F 0.7521(11) 0.5447(15) 0.3922(6) 0.034(4) Uani 0.42(3) 1 d D U P B 2 C3_12 C 0.6072(10) 0.5110(10) 0.3387(4) 0.033(3) Uani 0.42(3) 1 d D U P B 2 F4_12 F 0.5706(15) 0.4408(10) 0.3232(5) 0.048(5) Uani 0.42(3) 1 d D U P B 2 F5_12 F 0.6867(8) 0.5174(15) 0.3298(3) 0.048(4) Uani 0.42(3) 1 d D U P B 2 F6_12 F 0.5631(16) 0.5832(8) 0.3279(3) 0.048(4) Uani 0.42(3) 1 d D U P B 2 C4_12 C 0.5152(10) 0.5146(12) 0.3856(4) 0.025(3) Uani 0.42(3) 1 d D U P B 2 F7_12 F 0.4588(13) 0.4660(12) 0.3670(6) 0.035(4) Uani 0.42(3) 1 d D U P B 2 F8_12 F 0.4925(13) 0.5985(10) 0.3824(5) 0.043(4) Uani 0.42(3) 1 d D U P B 2 F9_12 F 0.5085(17) 0.4899(17) 0.4162(4) 0.042(5) Uani 0.42(3) 1 d D U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru2 0.0192(2) 0.0176(2) 0.0158(2) -0.00255(16) 0.00195(17) -0.00147(17) Ru3 0.0166(2) 0.0173(2) 0.01256(19) -0.00006(16) 0.00125(16) -0.00085(16) Ru4 0.0195(2) 0.0163(2) 0.01450(19) 0.00059(16) 0.00181(17) -0.00011(17) Ru5 0.0162(2) 0.0203(2) 0.01431(19) -0.00027(16) 0.00236(17) -0.00238(17) Ru6 0.0156(2) 0.0182(2) 0.01346(19) 0.00148(16) 0.00081(16) 0.00009(16) Ru7 0.0147(2) 0.0223(2) 0.01379(19) -0.00030(16) 0.00092(16) 0.00063(17) Ru8 0.0183(2) 0.0199(2) 0.01223(19) 0.00090(16) -0.00039(17) -0.00088(17) Al1 0.0139(7) 0.0168(8) 0.0100(7) 0.0014(6) 0.0004(6) -0.0014(6) Al2 0.0123(7) 0.0153(7) 0.0114(7) -0.0002(6) 0.0007(6) 0.0010(6) Ru1 0.0164(2) 0.0235(2) 0.0155(2) -0.00180(17) 0.00330(17) -0.00239(17) O1 0.040(2) 0.053(3) 0.020(2) -0.0032(18) 0.0062(18) -0.011(2) O2 0.034(2) 0.037(2) 0.034(2) 0.0025(18) 0.0071(19) -0.0131(19) O3 0.025(2) 0.037(2) 0.058(3) -0.018(2) -0.001(2) 0.0077(19) O4 0.035(2) 0.037(2) 0.029(2) 0.0138(19) -0.0055(18) -0.0109(19) O5 0.026(2) 0.029(2) 0.037(2) -0.0088(18) -0.0056(18) -0.0038(18) O6 0.025(2) 0.030(2) 0.042(2) -0.0037(18) 0.0113(19) 0.0014(17) O7 0.023(2) 0.040(2) 0.028(2) -0.0140(18) 0.0027(17) -0.0031(17) O8 0.020(2) 0.039(2) 0.030(2) 0.0004(17) 0.0075(17) -0.0022(17) O9 0.045(3) 0.034(2) 0.023(2) 0.0050(18) -0.0036(19) 0.010(2) O10 0.035(2) 0.031(2) 0.032(2) 0.0021(17) 0.0062(18) -0.0085(18) O11 0.043(3) 0.027(2) 0.038(2) -0.0041(18) -0.002(2) 0.013(2) O12 0.030(2) 0.038(2) 0.0184(19) -0.0130(17) 0.0001(17) -0.0015(17) O13 0.023(2) 0.028(2) 0.030(2) -0.0015(17) -0.0047(17) -0.0027(17) O14 0.024(2) 0.033(2) 0.027(2) -0.0077(17) -0.0020(17) -0.0032(17) O15 0.030(2) 0.031(2) 0.030(2) -0.0070(17) 0.0095(18) -0.0036(17) O16 0.051(3) 0.033(2) 0.038(2) 0.0085(19) 0.009(2) -0.006(2) O17 0.057(3) 0.034(2) 0.0208(19) 0.0005(17) 0.0184(19) 0.001(2) O18 0.048(3) 0.023(2) 0.033(2) 0.0029(18) -0.0128(19) 0.0034(19) O19 0.024(2) 0.031(2) 0.038(2) 0.0049(18) -0.0100(18) -0.0038(18) O20 0.024(2) 0.029(2) 0.028(2) -0.0061(16) -0.0002(17) 0.0079(17) O21 0.023(2) 0.035(2) 0.0165(19) 0.0001(16) -0.0016(16) 0.0025(16) O22 0.033(2) 0.035(2) 0.042(2) 0.0091(19) 0.0053(19) -0.0086(19) O23 0.034(2) 0.055(3) 0.0141(19) -0.0013(18) 0.0007(17) 0.0100(19) O24 0.025(2) 0.045(3) 0.033(2) 0.0047(19) 0.0014(18) -0.0076(19) O25 0.024(2) 0.029(2) 0.034(2) -0.0026(17) -0.0053(17) 0.0048(17) O26 0.028(2) 0.027(2) 0.0205(18) -0.0008(16) 0.0000(16) 0.0006(17) N1 0.018(2) 0.019(2) 0.0108(19) -0.0004(16) -0.0056(17) -0.0011(17) N2 0.017(2) 0.016(2) 0.018(2) -0.0051(17) -0.0032(18) -0.0009(17) C1 0.017(3) 0.031(3) 0.030(3) -0.006(2) 0.003(2) -0.009(2) C2 0.021(3) 0.035(3) 0.012(2) 0.002(2) 0.003(2) 0.000(2) C3 0.026(3) 0.028(3) 0.030(3) -0.011(2) 0.005(3) -0.011(3) C4 0.025(3) 0.021(3) 0.025(3) -0.001(2) 0.002(2) -0.005(2) C5 0.019(3) 0.025(3) 0.022(3) 0.002(2) -0.002(2) 0.007(2) C6 0.020(3) 0.024(3) 0.021(3) 0.003(2) -0.005(2) -0.005(2) C7 0.017(3) 0.023(3) 0.024(3) 0.001(2) 0.006(2) 0.002(2) C8 0.022(3) 0.021(3) 0.013(2) 0.004(2) -0.003(2) 0.002(2) C9 0.024(3) 0.028(3) 0.012(2) -0.003(2) 0.001(2) -0.003(2) C10 0.025(3) 0.024(3) 0.017(3) -0.002(2) 0.001(2) 0.003(2) C11 0.036(3) 0.021(3) 0.019(3) -0.010(2) 0.001(2) -0.002(3) C12 0.021(3) 0.019(3) 0.028(3) -0.001(2) 0.002(2) -0.001(2) C13 0.026(3) 0.025(3) 0.015(3) -0.002(2) 0.004(2) -0.003(2) C14 0.021(3) 0.020(3) 0.018(3) -0.002(2) 0.006(2) 0.000(2) C15 0.023(3) 0.026(3) 0.015(2) -0.002(2) 0.002(2) -0.007(2) C16 0.025(3) 0.028(3) 0.025(3) -0.002(2) 0.002(2) -0.004(2) C17 0.034(3) 0.021(3) 0.016(3) 0.001(2) -0.002(2) 0.003(2) C18 0.028(3) 0.028(3) 0.015(3) -0.005(2) -0.005(2) -0.005(2) C19 0.031(3) 0.020(3) 0.016(3) 0.004(2) -0.001(2) 0.004(2) C20 0.030(3) 0.024(3) 0.016(3) 0.001(2) 0.000(2) -0.005(2) C21 0.019(3) 0.023(3) 0.026(3) 0.001(2) 0.009(2) 0.004(2) C22 0.021(3) 0.026(3) 0.018(3) 0.002(2) -0.008(2) 0.006(2) C23 0.018(3) 0.033(3) 0.028(3) 0.006(2) 0.006(2) 0.010(2) C24 0.025(3) 0.035(3) 0.015(3) 0.006(2) 0.003(2) 0.002(3) C25 0.017(3) 0.034(3) 0.022(3) 0.001(2) -0.001(2) -0.001(2) C26 0.016(3) 0.030(3) 0.021(3) 0.000(2) 0.004(2) 0.002(2) O1_1 0.016(2) 0.025(3) 0.012(2) 0.0009(19) 0.004(2) 0.003(2) C1_1 0.018(2) 0.026(2) 0.010(2) -0.0018(19) 0.0033(16) -0.0025(17) C2_1 0.031(3) 0.027(2) 0.019(2) -0.005(2) 0.0100(19) 0.002(2) F1_1 0.027(2) 0.038(3) 0.029(2) -0.003(2) 0.0043(16) 0.012(2) F2_1 0.042(3) 0.040(2) 0.025(2) -0.014(2) 0.013(2) 0.004(2) F3_1 0.038(3) 0.027(2) 0.032(3) 0.002(2) 0.006(2) -0.001(2) C3_1 0.028(3) 0.034(3) 0.012(2) -0.001(2) -0.0004(18) -0.0087(18) F4_1 0.032(2) 0.046(3) 0.023(3) 0.008(2) -0.0083(18) 0.0034(19) F5_1 0.041(3) 0.044(3) 0.021(2) -0.003(2) -0.0057(19) -0.019(2) F6_1 0.045(3) 0.058(3) 0.0076(17) 0.000(2) 0.0034(17) -0.016(3) C4_1 0.021(3) 0.031(3) 0.026(2) -0.005(2) 0.0043(19) -0.005(2) F7_1 0.034(3) 0.030(2) 0.038(3) 0.0047(17) 0.004(2) -0.0069(19) F8_1 0.028(2) 0.043(4) 0.044(3) -0.010(2) 0.021(2) -0.011(2) F9_1 0.020(3) 0.044(3) 0.030(2) -0.012(2) -0.003(2) -0.004(2) O1_2 0.020(7) 0.023(9) 0.015(6) -0.004(6) 0.002(7) 0.001(8) C1_2 0.022(4) 0.026(4) 0.014(5) -0.004(4) 0.002(4) 0.001(4) C2_2 0.030(5) 0.033(4) 0.018(5) 0.001(4) -0.006(4) -0.003(4) F1_2 0.030(5) 0.036(9) 0.023(9) 0.011(8) -0.007(5) -0.002(5) F2_2 0.043(8) 0.037(9) 0.016(5) 0.001(5) -0.003(6) -0.005(8) F3_2 0.029(8) 0.027(5) 0.023(7) 0.004(5) -0.005(8) 0.000(6) C3_2 0.022(4) 0.027(5) 0.019(5) -0.004(4) 0.004(4) 0.001(4) F4_2 0.020(7) 0.029(6) 0.029(8) -0.001(6) -0.001(6) 0.001(6) F5_2 0.018(9) 0.032(6) 0.025(7) -0.010(6) 0.003(7) 0.000(6) F6_2 0.029(7) 0.028(9) 0.025(6) -0.007(6) 0.010(6) -0.006(7) C4_2 0.032(5) 0.030(4) 0.018(5) -0.010(4) 0.005(4) -0.002(4) F7_2 0.037(9) 0.026(6) 0.017(7) -0.012(6) 0.008(6) -0.001(7) F8_2 0.044(7) 0.033(7) 0.019(7) -0.009(6) 0.011(6) 0.002(7) F9_2 0.037(5) 0.037(9) 0.026(8) -0.005(7) -0.002(5) -0.010(6) O1_3 0.0132(16) 0.0163(18) 0.0176(17) 0.0012(14) -0.0011(14) -0.0018(13) C1_3 0.0142(19) 0.023(2) 0.018(2) -0.0010(15) 0.0022(17) -0.0049(16) C2_3 0.018(2) 0.032(3) 0.024(2) 0.0017(17) -0.0007(17) -0.0050(17) F1_3 0.0223(17) 0.0357(19) 0.047(2) -0.0045(15) 0.0046(16) 0.0047(14) F2_3 0.0180(15) 0.046(2) 0.0189(16) 0.0019(15) -0.0058(13) -0.0068(14) F3_3 0.0233(17) 0.045(2) 0.0308(18) 0.0188(15) 0.0005(14) 0.0003(15) C3_3 0.026(2) 0.029(2) 0.034(2) -0.0087(19) 0.006(2) -0.0084(17) F4_3 0.0362(18) 0.0236(18) 0.063(2) -0.0086(17) 0.0011(17) 0.0040(14) F5_3 0.047(2) 0.052(2) 0.0249(16) -0.0174(15) 0.0098(16) -0.0155(18) F6_3 0.0372(18) 0.034(2) 0.040(2) -0.0080(16) 0.0061(17) -0.0204(15) C4_3 0.019(2) 0.042(3) 0.019(2) 0.0013(17) 0.0022(19) -0.0046(19) F7_3 0.0310(18) 0.051(2) 0.0353(19) 0.0222(16) 0.0003(16) -0.0030(16) F8_3 0.0160(15) 0.056(2) 0.0267(16) 0.0072(16) 0.0065(13) -0.0045(14) F9_3 0.045(2) 0.058(2) 0.0242(17) -0.0129(15) 0.0110(16) -0.0081(18) O1_4 0.018(6) 0.027(9) 0.022(11) -0.001(8) 0.003(7) -0.003(6) C1_4 0.019(5) 0.031(5) 0.023(5) -0.001(4) 0.004(4) -0.005(4) C2_4 0.023(6) 0.041(6) 0.028(5) 0.005(5) 0.004(5) -0.006(5) F1_4 0.020(9) 0.036(7) 0.033(10) 0.006(6) 0.005(9) -0.011(7) F2_4 0.022(6) 0.049(9) 0.027(9) 0.010(8) 0.005(6) -0.006(6) F3_4 0.024(9) 0.044(9) 0.025(5) 0.005(7) 0.007(7) -0.005(8) C3_4 0.020(5) 0.036(5) 0.027(6) -0.001(5) 0.002(5) -0.002(5) F4_4 0.022(9) 0.038(8) 0.032(8) 0.003(7) 0.003(8) -0.001(7) F5_4 0.021(8) 0.039(8) 0.030(6) -0.004(6) 0.004(6) -0.003(7) F6_4 0.020(6) 0.037(8) 0.030(9) -0.002(8) 0.001(7) -0.001(7) C4_4 0.028(6) 0.034(6) 0.029(5) -0.007(5) 0.007(5) -0.009(5) F7_4 0.024(9) 0.036(9) 0.024(5) -0.009(7) 0.005(7) -0.012(8) F8_4 0.032(7) 0.037(8) 0.033(10) -0.007(7) 0.008(8) -0.013(7) F9_4 0.031(6) 0.034(8) 0.038(9) -0.008(8) 0.010(7) -0.006(6) O1_5 0.0134(17) 0.0187(18) 0.0127(16) 0.0026(13) -0.0023(13) 0.0028(14) C1_5 0.014(2) 0.022(2) 0.011(2) 0.0029(18) -0.0001(18) 0.0010(19) C2_5 0.019(3) 0.021(3) 0.023(2) 0.004(2) -0.003(2) 0.004(2) F1_5 0.0238(15) 0.0220(16) 0.0302(16) 0.0023(13) 0.0051(13) -0.0042(13) F2_5 0.0262(17) 0.0240(17) 0.0347(17) 0.0089(13) -0.0063(14) 0.0077(13) F3_5 0.0302(17) 0.0228(16) 0.0260(15) -0.0056(13) 0.0031(13) 0.0036(13) C3_5 0.015(2) 0.026(3) 0.018(2) 0.001(2) -0.0014(19) 0.001(2) F4_5 0.0195(15) 0.0263(16) 0.0242(15) 0.0018(12) 0.0009(13) -0.0039(12) F5_5 0.0188(15) 0.0314(17) 0.0279(15) -0.0037(13) 0.0054(13) 0.0059(13) F6_5 0.0169(15) 0.0415(19) 0.0218(15) 0.0068(13) -0.0074(12) 0.0018(13) C4_5 0.017(2) 0.025(3) 0.015(2) 0.0004(19) -0.001(2) 0.000(2) F7_5 0.0300(16) 0.0246(16) 0.0201(15) -0.0086(12) 0.0021(13) -0.0036(13) F8_5 0.0316(17) 0.0386(18) 0.0131(14) 0.0109(13) 0.0003(13) 0.0033(14) F9_5 0.0166(14) 0.0311(17) 0.0204(14) -0.0004(12) 0.0045(12) 0.0022(12) O1_6 0.0199(18) 0.0126(17) 0.0202(17) 0.0001(14) 0.0044(15) -0.0006(14) C1_6 0.020(2) 0.018(2) 0.019(2) 0.0007(19) 0.0053(19) 0.0000(19) C2_6 0.018(3) 0.020(3) 0.023(2) 0.004(2) 0.003(2) 0.002(2) F1_6 0.0257(16) 0.0306(17) 0.0223(15) 0.0062(13) 0.0036(13) 0.0015(13) F2_6 0.0304(17) 0.0227(16) 0.0380(17) 0.0070(14) 0.0028(15) 0.0115(13) F3_6 0.0242(16) 0.0296(18) 0.0339(17) 0.0078(14) -0.0100(14) -0.0011(13) C3_6 0.026(3) 0.023(3) 0.022(3) 0.001(2) 0.008(2) 0.004(2) F4_6 0.0426(19) 0.0307(17) 0.0244(15) 0.0068(13) 0.0159(14) 0.0065(14) F5_6 0.0229(16) 0.041(2) 0.0473(19) 0.0011(15) 0.0130(15) 0.0048(14) F6_6 0.0439(19) 0.0213(16) 0.0364(17) -0.0073(13) 0.0178(15) 0.0028(14) C4_6 0.027(3) 0.016(2) 0.021(2) 0.003(2) 0.003(2) -0.001(2) F7_6 0.0374(18) 0.0385(19) 0.0213(15) 0.0030(14) -0.0025(14) -0.0030(15) F8_6 0.0328(18) 0.0172(15) 0.0387(17) -0.0003(13) 0.0031(15) -0.0057(13) F9_6 0.0189(15) 0.0294(17) 0.0311(16) -0.0004(13) 0.0066(13) 0.0011(13) O1_8 0.0133(16) 0.0244(19) 0.0168(16) 0.0018(14) 0.0029(14) -0.0002(14) C1_8 0.012(2) 0.023(2) 0.020(2) 0.0019(19) 0.0022(19) -0.0022(19) C2_8 0.021(3) 0.023(3) 0.028(3) -0.002(2) 0.002(2) -0.004(2) F1_8 0.0282(17) 0.045(2) 0.0217(15) 0.0060(14) -0.0065(14) -0.0035(15) F2_8 0.0162(15) 0.0386(19) 0.0364(17) 0.0025(15) -0.0040(14) -0.0073(13) F3_8 0.0365(19) 0.0291(18) 0.0364(17) -0.0134(14) -0.0060(15) 0.0001(14) C3_8 0.017(3) 0.043(3) 0.020(2) 0.004(2) 0.002(2) -0.001(2) F4_8 0.0323(18) 0.083(3) 0.0131(15) 0.0042(16) 0.0030(14) -0.0093(18) F5_8 0.0322(18) 0.0327(18) 0.0452(19) 0.0179(15) 0.0090(15) -0.0007(15) F6_8 0.0218(16) 0.057(2) 0.0370(17) -0.0013(16) 0.0159(14) -0.0031(15) C4_8 0.017(3) 0.028(3) 0.043(3) -0.006(2) 0.001(2) -0.001(2) F7_8 0.0304(18) 0.041(2) 0.056(2) -0.0287(17) 0.0033(16) 0.0016(15) F8_8 0.0166(16) 0.0335(19) 0.065(2) -0.0080(16) -0.0028(16) 0.0045(14) F9_8 0.0294(18) 0.0242(18) 0.062(2) 0.0118(16) 0.0004(17) -0.0026(14) O1_9 0.0247(19) 0.031(2) 0.0098(15) 0.0018(14) -0.0008(14) -0.0086(16) C1_9 0.022(3) 0.041(3) 0.009(2) 0.005(2) -0.001(2) -0.007(2) C2_9 0.028(3) 0.054(3) 0.027(3) 0.019(3) 0.011(2) 0.008(2) F1_9 0.048(2) 0.0350(19) 0.0419(19) 0.0126(16) 0.0113(17) 0.0002(16) F2_9 0.048(2) 0.087(3) 0.0299(17) 0.0358(18) 0.0068(17) 0.016(2) F3_9 0.043(2) 0.069(3) 0.058(2) 0.0301(19) 0.0243(18) 0.0305(19) C3_9 0.042(3) 0.096(5) 0.015(3) -0.008(3) 0.000(3) -0.032(3) F4_9 0.083(3) 0.088(3) 0.0239(18) -0.0147(18) 0.0056(19) -0.057(2) F5_9 0.028(2) 0.165(4) 0.0294(19) 0.005(2) -0.0097(17) -0.025(2) F6_9 0.067(3) 0.121(4) 0.0101(16) -0.0080(19) -0.0002(17) -0.028(2) C4_9 0.036(3) 0.037(3) 0.015(2) 0.005(2) 0.009(2) 0.001(2) F7_9 0.065(2) 0.0352(19) 0.0366(18) -0.0062(15) 0.0195(18) 0.0028(17) F8_9 0.0398(19) 0.064(2) 0.0232(16) 0.0140(15) 0.0166(15) 0.0031(17) F9_9 0.0179(16) 0.047(2) 0.0264(16) 0.0065(14) -0.0014(13) 0.0014(14) O1_10 0.0180(17) 0.0182(18) 0.0163(16) -0.0010(14) -0.0016(14) -0.0040(14) C1_10 0.020(2) 0.016(2) 0.015(2) 0.0011(18) -0.0011(19) -0.0032(19) C2_10 0.025(3) 0.021(3) 0.035(3) 0.001(2) -0.003(2) -0.007(2) F1_10 0.0404(19) 0.0296(18) 0.0358(17) 0.0131(14) -0.0001(15) -0.0082(15) F2_10 0.0306(18) 0.0235(17) 0.0458(19) -0.0060(14) -0.0068(15) -0.0074(14) F3_10 0.0273(17) 0.0227(17) 0.058(2) -0.0039(15) -0.0109(16) 0.0014(14) C3_10 0.031(3) 0.030(3) 0.021(2) -0.002(2) 0.006(2) -0.008(2) F4_10 0.049(2) 0.0331(18) 0.0194(15) 0.0010(13) 0.0076(15) -0.0204(15) F5_10 0.0333(18) 0.050(2) 0.0407(18) -0.0145(16) 0.0158(16) -0.0040(16) F6_10 0.0436(19) 0.0362(19) 0.0237(16) -0.0098(14) -0.0014(14) -0.0170(15) C4_10 0.024(3) 0.026(3) 0.022(3) 0.004(2) -0.002(2) -0.006(2) F7_10 0.0292(17) 0.0280(17) 0.0309(16) 0.0073(13) -0.0067(14) 0.0019(14) F8_10 0.0212(16) 0.0336(18) 0.0455(19) 0.0044(15) -0.0056(15) -0.0103(14) F9_10 0.0236(17) 0.055(2) 0.0261(16) 0.0017(15) 0.0053(14) 0.0017(15) O1_11 0.021(8) 0.022(5) 0.017(7) -0.002(5) -0.008(6) 0.003(5) C1_11 0.028(5) 0.018(5) 0.027(5) 0.000(4) 0.001(4) 0.000(4) C2_11 0.028(5) 0.022(5) 0.032(5) 0.003(5) 0.000(5) 0.002(4) F1_11 0.026(4) 0.033(7) 0.043(7) -0.005(5) 0.006(4) -0.008(3) F2_11 0.042(5) 0.016(3) 0.044(6) -0.003(3) 0.005(4) -0.002(3) F3_11 0.046(7) 0.040(7) 0.024(4) 0.001(4) -0.008(4) -0.009(5) C3_11 0.030(6) 0.019(5) 0.054(6) -0.001(5) -0.001(5) 0.007(4) F4_11 0.019(4) 0.021(6) 0.086(8) -0.005(5) -0.011(4) 0.009(4) F5_11 0.031(5) 0.051(9) 0.068(6) -0.015(4) 0.028(4) -0.003(5) F6_11 0.042(5) 0.021(5) 0.122(11) -0.001(6) -0.018(7) 0.012(4) C4_11 0.045(6) 0.024(5) 0.030(5) 0.003(5) -0.005(4) 0.001(5) F7_11 0.066(6) 0.034(6) 0.036(5) 0.005(5) -0.019(4) -0.006(5) F8_11 0.075(9) 0.026(3) 0.037(4) 0.014(3) -0.010(5) -0.002(4) F9_11 0.065(4) 0.037(6) 0.028(4) 0.013(4) 0.012(3) 0.015(4) O1_12 0.011(10) 0.010(6) 0.029(10) -0.003(6) 0.009(8) 0.000(6) C1_12 0.026(6) 0.012(6) 0.021(5) -0.002(5) -0.002(5) 0.002(5) C2_12 0.025(6) 0.018(6) 0.026(6) -0.004(5) 0.002(5) -0.002(5) F1_12 0.038(8) 0.046(10) 0.016(5) -0.007(4) -0.005(4) 0.006(6) F2_12 0.035(7) 0.019(4) 0.033(7) -0.001(4) -0.003(5) -0.003(4) F3_12 0.023(5) 0.028(8) 0.051(11) -0.008(6) 0.005(5) 0.001(4) C3_12 0.050(7) 0.025(7) 0.023(6) -0.001(5) -0.003(6) -0.012(5) F4_12 0.098(12) 0.027(6) 0.014(5) 0.006(5) -0.024(7) -0.020(7) F5_12 0.073(6) 0.049(10) 0.025(5) 0.003(6) 0.022(5) -0.010(6) F6_12 0.079(11) 0.036(5) 0.024(5) 0.005(4) -0.016(7) 0.002(6) C4_12 0.020(6) 0.023(6) 0.030(7) -0.001(6) -0.010(5) 0.008(5) F7_12 0.021(5) 0.020(7) 0.057(7) -0.003(7) -0.025(5) 0.009(6) F8_12 0.037(8) 0.024(6) 0.066(9) -0.006(5) -0.003(7) 0.015(5) F9_12 0.026(7) 0.063(13) 0.039(6) 0.007(6) 0.003(5) -0.001(7) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru2 C11 1.907(6) . ? Ru2 C10 1.951(5) . ? Ru2 C12 1.972(5) . ? Ru2 N2 2.075(4) . ? Ru2 C13 2.342(6) . ? Ru2 Ru1 2.7702(18) . ? Ru2 Ru3 2.771(2) . ? Ru2 Ru4 2.787(2) . ? Ru3 C9 1.906(6) . ? Ru3 C7 1.915(5) . ? Ru3 N2 1.931(4) . ? Ru3 C8 1.954(5) . ? Ru3 Ru4 2.801(2) . ? Ru4 C6 1.963(5) . ? Ru4 C4 1.966(5) . ? Ru4 C5 1.968(6) . ? Ru4 C13 2.049(6) . ? Ru4 N2 2.107(4) . ? Ru4 Ru1 2.8161(19) . ? Ru5 C14 1.906(6) . ? Ru5 C16 1.912(5) . ? Ru5 N1 1.933(4) . ? Ru5 C15 1.949(5) . ? Ru5 Ru6 2.7740(16) . ? Ru5 Ru8 2.815(2) . ? Ru6 C21 1.889(6) . ? Ru6 C22 1.960(5) . ? Ru6 C20 1.968(5) . ? Ru6 N1 2.065(4) . ? Ru6 C26 2.425(5) . ? Ru6 Ru7 2.7490(18) . ? Ru6 Ru8 2.823(2) . ? Ru7 C23 1.906(5) . ? Ru7 C25 1.925(6) . ? Ru7 C24 1.929(6) . ? Ru7 N1 1.950(4) . ? Ru7 Ru8 2.804(2) . ? Ru8 C19 1.966(6) . ? Ru8 C17 1.976(5) . ? Ru8 C18 1.977(6) . ? Ru8 C26 2.013(6) . ? Ru8 N1 2.142(4) . ? Al1 O1_11 1.703(16) . ? Al1 O1_8 1.721(3) . ? Al1 O1_10 1.724(4) . ? Al1 O1_9 1.725(4) . ? Al1 O1_12 1.75(2) . ? Al2 O1_4 1.64(4) . ? Al2 O1_2 1.70(3) . ? Al2 O1_5 1.720(4) . ? Al2 O1_6 1.726(3) . ? Al2 O1_3 1.731(4) . ? Al2 O1_1 1.732(6) . ? Ru1 C3 1.906(6) . ? Ru1 C2 1.919(6) . ? Ru1 N2 1.933(4) . ? Ru1 C1 1.950(5) . ? O1 C1 1.133(6) . ? O2 C2 1.136(6) . ? O3 C3 1.131(6) . ? O4 C4 1.126(5) . ? O5 C5 1.116(6) . ? O6 C6 1.128(5) . ? O7 C7 1.130(5) . ? O8 C8 1.129(5) . ? O9 C9 1.131(6) . ? O10 C10 1.134(5) . ? O11 C11 1.119(6) . ? O12 C12 1.125(5) . ? O13 C13 1.127(6) . ? O14 C14 1.128(5) . ? O15 C15 1.137(5) . ? O16 C16 1.134(6) . ? O17 C17 1.128(5) . ? O18 C18 1.112(6) . ? O19 C19 1.129(6) . ? O20 C20 1.135(5) . ? O21 C21 1.129(6) . ? O22 C22 1.129(5) . ? O23 C23 1.124(6) . ? O24 C24 1.151(6) . ? O25 C25 1.135(6) . ? O26 C26 1.138(6) . ? O1_1 C1_1 1.351(5) . ? C1_1 C3_1 1.535(7) . ? C1_1 C2_1 1.551(7) . ? C1_1 C4_1 1.556(7) . ? C2_1 F3_1 1.332(7) . ? C2_1 F1_1 1.333(7) . ? C2_1 F2_1 1.339(5) . ? C3_1 F5_1 1.328(7) . ? C3_1 F4_1 1.331(8) . ? C3_1 F6_1 1.343(5) . ? C4_1 F9_1 1.323(8) . ? C4_1 F8_1 1.340(6) . ? C4_1 F7_1 1.342(7) . ? O1_2 C1_2 1.355(14) . ? C1_2 C4_2 1.545(12) . ? C1_2 C3_2 1.547(12) . ? C1_2 C2_2 1.551(12) . ? C2_2 F1_2 1.325(13) . ? C2_2 F2_2 1.330(13) . ? C2_2 F3_2 1.338(13) . ? C3_2 F5_2 1.337(13) . ? C3_2 F6_2 1.337(13) . ? C3_2 F4_2 1.339(13) . ? C4_2 F9_2 1.336(13) . ? C4_2 F7_2 1.336(13) . ? C4_2 F8_2 1.337(13) . ? O1_3 C1_3 1.350(5) . ? C1_3 C3_3 1.539(6) . ? C1_3 C2_3 1.549(6) . ? C1_3 C4_3 1.557(5) . ? C2_3 F3_3 1.311(5) . ? C2_3 F2_3 1.343(5) . ? C2_3 F1_3 1.362(5) . ? C3_3 F4_3 1.318(6) . ? C3_3 F6_3 1.338(5) . ? C3_3 F5_3 1.369(5) . ? C4_3 F9_3 1.303(5) . ? C4_3 F8_3 1.333(5) . ? C4_3 F7_3 1.371(6) . ? O1_4 C1_4 1.342(14) . ? C1_4 C2_4 1.552(13) . ? C1_4 C3_4 1.552(13) . ? C1_4 C4_4 1.558(13) . ? C2_4 F3_4 1.333(14) . ? C2_4 F1_4 1.340(14) . ? C2_4 F2_4 1.341(14) . ? C3_4 F4_4 1.333(14) . ? C3_4 F5_4 1.336(14) . ? C3_4 F6_4 1.342(14) . ? C4_4 F9_4 1.331(14) . ? C4_4 F7_4 1.336(14) . ? C4_4 F8_4 1.339(14) . ? O1_5 C1_5 1.353(5) . ? C1_5 C3_5 1.547(6) . ? C1_5 C2_5 1.550(6) . ? C1_5 C4_5 1.558(5) . ? C2_5 F3_5 1.331(5) . ? C2_5 F2_5 1.337(5) . ? C2_5 F1_5 1.347(5) . ? C3_5 F4_5 1.325(5) . ? C3_5 F5_5 1.340(5) . ? C3_5 F6_5 1.344(5) . ? C4_5 F7_5 1.326(5) . ? C4_5 F9_5 1.327(5) . ? C4_5 F8_5 1.349(5) . ? O1_6 C1_6 1.353(5) . ? C1_6 C4_6 1.552(6) . ? C1_6 C2_6 1.554(6) . ? C1_6 C3_6 1.559(5) . ? C2_6 F3_6 1.320(5) . ? C2_6 F2_6 1.338(5) . ? C2_6 F1_6 1.342(4) . ? C3_6 F4_6 1.328(5) . ? C3_6 F6_6 1.330(5) . ? C3_6 F5_6 1.342(5) . ? C4_6 F9_6 1.326(5) . ? C4_6 F7_6 1.331(5) . ? C4_6 F8_6 1.341(5) . ? O1_8 C1_8 1.354(5) . ? C1_8 C2_8 1.544(6) . ? C1_8 C4_8 1.550(6) . ? C1_8 C3_8 1.563(6) . ? C2_8 F3_8 1.326(5) . ? C2_8 F1_8 1.336(5) . ? C2_8 F2_8 1.339(5) . ? C3_8 F4_8 1.315(5) . ? C3_8 F5_8 1.328(6) . ? C3_8 F6_8 1.349(5) . ? C4_8 F7_8 1.333(5) . ? C4_8 F9_8 1.334(5) . ? C4_8 F8_8 1.339(5) . ? O1_9 C1_9 1.358(5) . ? C1_9 C3_9 1.542(7) . ? C1_9 C2_9 1.548(6) . ? C1_9 C4_9 1.556(6) . ? C2_9 F3_9 1.328(5) . ? C2_9 F1_9 1.335(6) . ? C2_9 F2_9 1.335(5) . ? C3_9 F5_9 1.328(7) . ? C3_9 F4_9 1.337(7) . ? C3_9 F6_9 1.340(5) . ? C4_9 F7_9 1.330(5) . ? C4_9 F9_9 1.335(5) . ? C4_9 F8_9 1.339(5) . ? O1_10 C1_10 1.348(5) . ? C1_10 C2_10 1.548(6) . ? C1_10 C4_10 1.552(6) . ? C1_10 C3_10 1.559(5) . ? C2_10 F3_10 1.326(5) . ? C2_10 F1_10 1.332(5) . ? C2_10 F2_10 1.349(5) . ? C3_10 F5_10 1.331(5) . ? C3_10 F4_10 1.333(5) . ? C3_10 F6_10 1.339(5) . ? C4_10 F8_10 1.333(5) . ? C4_10 F7_10 1.333(5) . ? C4_10 F9_10 1.336(5) . ? O1_11 C1_11 1.357(10) . ? C1_11 C2_11 1.549(10) . ? C1_11 C4_11 1.550(10) . ? C1_11 C3_11 1.557(10) . ? C2_11 F3_11 1.330(10) . ? C2_11 F1_11 1.332(10) . ? C2_11 F2_11 1.350(10) . ? C3_11 F6_11 1.327(10) . ? C3_11 F4_11 1.329(10) . ? C3_11 F5_11 1.333(11) . ? C4_11 F9_11 1.332(10) . ? C4_11 F7_11 1.336(10) . ? C4_11 F8_11 1.338(10) . ? O1_12 C1_12 1.352(11) . ? C1_12 C2_12 1.551(11) . ? C1_12 C3_12 1.552(11) . ? C1_12 C4_12 1.557(11) . ? C2_12 F3_12 1.329(12) . ? C2_12 F1_12 1.335(11) . ? C2_12 F2_12 1.341(12) . ? C3_12 F5_12 1.335(12) . ? C3_12 F4_12 1.340(12) . ? C3_12 F6_12 1.343(12) . ? C4_12 F8_12 1.323(12) . ? C4_12 F7_12 1.332(12) . ? C4_12 F9_12 1.336(12) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C11 Ru2 C10 89.7(2) . . ? C11 Ru2 C12 93.4(2) . . ? C10 Ru2 C12 99.8(2) . . ? C11 Ru2 N2 94.2(2) . . ? C10 Ru2 N2 132.66(17) . . ? C12 Ru2 N2 126.94(17) . . ? C11 Ru2 C13 169.7(2) . . ? C10 Ru2 C13 80.3(2) . . ? C12 Ru2 C13 85.82(18) . . ? N2 Ru2 C13 94.52(18) . . ? C11 Ru2 Ru1 94.13(16) . . ? C10 Ru2 Ru1 175.16(14) . . ? C12 Ru2 Ru1 82.91(14) . . ? N2 Ru2 Ru1 44.19(10) . . ? C13 Ru2 Ru1 95.97(14) . . ? C11 Ru2 Ru3 94.22(15) . . ? C10 Ru2 Ru3 88.55(14) . . ? C12 Ru2 Ru3 168.72(14) . . ? N2 Ru2 Ru3 44.12(9) . . ? C13 Ru2 Ru3 88.14(12) . . ? Ru1 Ru2 Ru3 88.26(4) . . ? C11 Ru2 Ru4 142.86(16) . . ? C10 Ru2 Ru4 114.31(14) . . ? C12 Ru2 Ru4 108.74(14) . . ? N2 Ru2 Ru4 48.71(11) . . ? C13 Ru2 Ru4 46.08(13) . . ? Ru1 Ru2 Ru4 60.89(4) . . ? Ru3 Ru2 Ru4 60.53(2) . . ? C9 Ru3 C7 92.4(2) . . ? C9 Ru3 N2 103.00(17) . . ? C7 Ru3 N2 110.59(18) . . ? C9 Ru3 C8 94.69(19) . . ? C7 Ru3 C8 89.88(19) . . ? N2 Ru3 C8 152.00(18) . . ? C9 Ru3 Ru2 96.69(14) . . ? C7 Ru3 Ru2 158.57(13) . . ? N2 Ru3 Ru2 48.41(12) . . ? C8 Ru3 Ru2 108.59(15) . . ? C9 Ru3 Ru4 150.68(12) . . ? C7 Ru3 Ru4 104.35(16) . . ? N2 Ru3 Ru4 48.73(12) . . ? C8 Ru3 Ru4 108.99(14) . . ? Ru2 Ru3 Ru4 60.02(6) . . ? C6 Ru4 C4 106.6(2) . . ? C6 Ru4 C5 89.3(2) . . ? C4 Ru4 C5 90.7(2) . . ? C6 Ru4 C13 83.2(2) . . ? C4 Ru4 C13 84.2(2) . . ? C5 Ru4 C13 169.3(2) . . ? C6 Ru4 N2 125.02(17) . . ? C4 Ru4 N2 128.36(17) . . ? C5 Ru4 N2 87.67(19) . . ? C13 Ru4 N2 102.84(19) . . ? C6 Ru4 Ru2 117.32(14) . . ? C4 Ru4 Ru2 112.46(15) . . ? C5 Ru4 Ru2 135.20(15) . . ? C13 Ru4 Ru2 55.44(15) . . ? N2 Ru4 Ru2 47.71(11) . . ? C6 Ru4 Ru3 81.90(15) . . ? C4 Ru4 Ru3 170.84(14) . . ? C5 Ru4 Ru3 92.92(15) . . ? C13 Ru4 Ru3 93.50(15) . . ? N2 Ru4 Ru3 43.53(9) . . ? Ru2 Ru4 Ru3 59.45(4) . . ? C6 Ru4 Ru1 167.86(14) . . ? C4 Ru4 Ru1 85.05(14) . . ? C5 Ru4 Ru1 86.95(14) . . ? C13 Ru4 Ru1 101.92(14) . . ? N2 Ru4 Ru1 43.32(10) . . ? Ru2 Ru4 Ru1 59.26(2) . . ? Ru3 Ru4 Ru1 86.76(5) . . ? C14 Ru5 C16 91.1(2) . . ? C14 Ru5 N1 106.77(17) . . ? C16 Ru5 N1 111.02(18) . . ? C14 Ru5 C15 90.4(2) . . ? C16 Ru5 C15 92.5(2) . . ? N1 Ru5 C15 150.06(18) . . ? C14 Ru5 Ru6 103.20(14) . . ? C16 Ru5 Ru6 157.20(15) . . ? N1 Ru5 Ru6 48.07(11) . . ? C15 Ru5 Ru6 104.87(15) . . ? C14 Ru5 Ru8 156.11(12) . . ? C16 Ru5 Ru8 99.74(16) . . ? N1 Ru5 Ru8 49.46(12) . . ? C15 Ru5 Ru8 110.12(16) . . ? Ru6 Ru5 Ru8 60.68(4) . . ? C21 Ru6 C22 90.2(2) . . ? C21 Ru6 C20 90.1(2) . . ? C22 Ru6 C20 100.6(2) . . ? C21 Ru6 N1 96.11(18) . . ? C22 Ru6 N1 129.80(17) . . ? C20 Ru6 N1 128.98(17) . . ? C21 Ru6 C26 170.55(19) . . ? C22 Ru6 C26 82.99(19) . . ? C20 Ru6 C26 84.78(19) . . ? N1 Ru6 C26 93.29(16) . . ? C21 Ru6 Ru7 95.11(14) . . ? C22 Ru6 Ru7 84.81(15) . . ? C20 Ru6 Ru7 172.49(13) . . ? N1 Ru6 Ru7 45.08(10) . . ? C26 Ru6 Ru7 90.82(12) . . ? C21 Ru6 Ru5 97.65(15) . . ? C22 Ru6 Ru5 170.43(14) . . ? C20 Ru6 Ru5 84.86(15) . . ? N1 Ru6 Ru5 44.12(10) . . ? C26 Ru6 Ru5 89.78(13) . . ? Ru7 Ru6 Ru5 89.05(6) . . ? C21 Ru6 Ru8 145.06(15) . . ? C22 Ru6 Ru8 110.10(15) . . ? C20 Ru6 Ru8 112.52(14) . . ? N1 Ru6 Ru8 49.00(10) . . ? C26 Ru6 Ru8 44.30(13) . . ? Ru7 Ru6 Ru8 60.40(4) . . ? Ru5 Ru6 Ru8 60.37(5) . . ? C23 Ru7 C25 92.5(2) . . ? C23 Ru7 C24 92.2(2) . . ? C25 Ru7 C24 93.0(2) . . ? C23 Ru7 N1 107.55(18) . . ? C25 Ru7 N1 108.03(18) . . ? C24 Ru7 N1 150.04(18) . . ? C23 Ru7 Ru6 94.90(14) . . ? C25 Ru7 Ru6 156.59(14) . . ? C24 Ru7 Ru6 108.86(17) . . ? N1 Ru7 Ru6 48.57(12) . . ? C23 Ru7 Ru8 153.93(14) . . ? C25 Ru7 Ru8 106.05(14) . . ? C24 Ru7 Ru8 104.74(14) . . ? N1 Ru7 Ru8 49.66(11) . . ? Ru6 Ru7 Ru8 61.11(3) . . ? C19 Ru8 C17 106.5(2) . . ? C19 Ru8 C18 90.2(2) . . ? C17 Ru8 C18 89.49(19) . . ? C19 Ru8 C26 82.3(2) . . ? C17 Ru8 C26 87.94(18) . . ? C18 Ru8 C26 171.1(2) . . ? C19 Ru8 N1 129.16(16) . . ? C17 Ru8 N1 123.95(19) . . ? C18 Ru8 N1 84.51(18) . . ? C26 Ru8 N1 103.98(18) . . ? C19 Ru8 Ru7 85.25(13) . . ? C17 Ru8 Ru7 167.28(15) . . ? C18 Ru8 Ru7 85.46(13) . . ? C26 Ru8 Ru7 98.74(12) . . ? N1 Ru8 Ru7 43.96(10) . . ? C19 Ru8 Ru5 172.33(13) . . ? C17 Ru8 Ru5 81.20(17) . . ? C18 Ru8 Ru5 90.16(16) . . ? C26 Ru8 Ru5 97.86(15) . . ? N1 Ru8 Ru5 43.30(9) . . ? Ru7 Ru8 Ru5 87.15(5) . . ? C19 Ru8 Ru6 115.68(14) . . ? C17 Ru8 Ru6 118.18(16) . . ? C18 Ru8 Ru6 131.07(14) . . ? C26 Ru8 Ru6 57.29(14) . . ? N1 Ru8 Ru6 46.71(11) . . ? Ru7 Ru8 Ru6 58.49(6) . . ? Ru5 Ru8 Ru6 58.95(3) . . ? O1_11 Al1 O1_8 109.0(7) . . ? O1_11 Al1 O1_10 106.3(7) . . ? O1_8 Al1 O1_10 113.32(15) . . ? O1_11 Al1 O1_9 112.8(8) . . ? O1_8 Al1 O1_9 107.24(17) . . ? O1_10 Al1 O1_9 108.27(16) . . ? O1_8 Al1 O1_12 109.4(8) . . ? O1_10 Al1 O1_12 108.9(9) . . ? O1_9 Al1 O1_12 109.6(10) . . ? O1_4 Al2 O1_2 115(3) . . ? O1_4 Al2 O1_5 105(2) . . ? O1_2 Al2 O1_5 107.7(14) . . ? O1_4 Al2 O1_6 106(2) . . ? O1_2 Al2 O1_6 108.8(14) . . ? O1_5 Al2 O1_6 114.21(16) . . ? O1_5 Al2 O1_3 107.95(18) . . ? O1_6 Al2 O1_3 105.73(18) . . ? O1_5 Al2 O1_1 107.6(3) . . ? O1_6 Al2 O1_1 108.2(3) . . ? O1_3 Al2 O1_1 113.3(4) . . ? C3 Ru1 C2 90.5(2) . . ? C3 Ru1 N2 104.74(19) . . ? C2 Ru1 N2 109.50(17) . . ? C3 Ru1 C1 92.9(2) . . ? C2 Ru1 C1 92.55(19) . . ? N2 Ru1 C1 151.29(18) . . ? C3 Ru1 Ru2 100.60(16) . . ? C2 Ru1 Ru2 157.12(12) . . ? N2 Ru1 Ru2 48.43(11) . . ? C1 Ru1 Ru2 106.67(14) . . ? C3 Ru1 Ru4 152.78(15) . . ? C2 Ru1 Ru4 102.27(15) . . ? N2 Ru1 Ru4 48.41(11) . . ? C1 Ru1 Ru4 110.23(15) . . ? Ru2 Ru1 Ru4 59.85(6) . . ? Ru5 N1 Ru7 171.8(2) . . ? Ru5 N1 Ru6 87.81(15) . . ? Ru7 N1 Ru6 86.36(14) . . ? Ru5 N1 Ru8 87.24(14) . . ? Ru7 N1 Ru8 86.37(15) . . ? Ru6 N1 Ru8 84.29(14) . . ? Ru3 N2 Ru1 173.8(2) . . ? Ru3 N2 Ru2 87.47(15) . . ? Ru1 N2 Ru2 87.38(15) . . ? Ru3 N2 Ru4 87.73(14) . . ? Ru1 N2 Ru4 88.26(15) . . ? Ru2 N2 Ru4 83.58(16) . . ? O1 C1 Ru1 176.3(4) . . ? O2 C2 Ru1 178.3(5) . . ? O3 C3 Ru1 177.1(5) . . ? O4 C4 Ru4 177.2(5) . . ? O5 C5 Ru4 179.1(5) . . ? O6 C6 Ru4 176.8(4) . . ? O7 C7 Ru3 178.9(5) . . ? O8 C8 Ru3 176.6(4) . . ? O9 C9 Ru3 174.8(4) . . ? O10 C10 Ru2 176.9(4) . . ? O11 C11 Ru2 176.8(5) . . ? O12 C12 Ru2 178.8(4) . . ? O13 C13 Ru4 151.4(4) . . ? O13 C13 Ru2 130.0(4) . . ? Ru4 C13 Ru2 78.5(2) . . ? O14 C14 Ru5 177.7(5) . . ? O15 C15 Ru5 175.9(4) . . ? O16 C16 Ru5 178.8(5) . . ? O17 C17 Ru8 174.8(5) . . ? O18 C18 Ru8 178.8(5) . . ? O19 C19 Ru8 176.0(4) . . ? O20 C20 Ru6 177.4(4) . . ? O21 C21 Ru6 178.4(4) . . ? O22 C22 Ru6 179.8(5) . . ? O23 C23 Ru7 175.4(4) . . ? O24 C24 Ru7 174.9(4) . . ? O25 C25 Ru7 178.1(5) . . ? O26 C26 Ru8 156.3(4) . . ? O26 C26 Ru6 125.1(4) . . ? Ru8 C26 Ru6 78.42(18) . . ? C1_1 O1_1 Al2 147.6(7) . . ? O1_1 C1_1 C3_1 108.1(5) . . ? O1_1 C1_1 C2_1 112.2(5) . . ? C3_1 C1_1 C2_1 108.9(5) . . ? O1_1 C1_1 C4_1 109.2(5) . . ? C3_1 C1_1 C4_1 109.9(5) . . ? C2_1 C1_1 C4_1 108.5(5) . . ? F3_1 C2_1 F1_1 106.1(5) . . ? F3_1 C2_1 F2_1 107.5(6) . . ? F1_1 C2_1 F2_1 106.7(5) . . ? F3_1 C2_1 C1_1 111.2(5) . . ? F1_1 C2_1 C1_1 111.5(5) . . ? F2_1 C2_1 C1_1 113.5(5) . . ? F5_1 C3_1 F4_1 106.9(6) . . ? F5_1 C3_1 F6_1 108.6(5) . . ? F4_1 C3_1 F6_1 106.4(5) . . ? F5_1 C3_1 C1_1 111.1(5) . . ? F4_1 C3_1 C1_1 111.6(5) . . ? F6_1 C3_1 C1_1 112.0(5) . . ? F9_1 C4_1 F8_1 108.2(6) . . ? F9_1 C4_1 F7_1 107.5(6) . . ? F8_1 C4_1 F7_1 105.9(5) . . ? F9_1 C4_1 C1_1 111.3(6) . . ? F8_1 C4_1 C1_1 112.6(5) . . ? F7_1 C4_1 C1_1 111.1(5) . . ? C1_2 O1_2 Al2 152(3) . . ? O1_2 C1_2 C4_2 109.8(19) . . ? O1_2 C1_2 C3_2 109.8(19) . . ? C4_2 C1_2 C3_2 110.2(12) . . ? O1_2 C1_2 C2_2 108.5(18) . . ? C4_2 C1_2 C2_2 109.5(12) . . ? C3_2 C1_2 C2_2 108.9(12) . . ? F1_2 C2_2 F2_2 109.9(19) . . ? F1_2 C2_2 F3_2 107.9(18) . . ? F2_2 C2_2 F3_2 106.0(16) . . ? F1_2 C2_2 C1_2 111.1(17) . . ? F2_2 C2_2 C1_2 111.4(14) . . ? F3_2 C2_2 C1_2 110.3(14) . . ? F5_2 C3_2 F6_2 106.4(19) . . ? F5_2 C3_2 F4_2 106.8(19) . . ? F6_2 C3_2 F4_2 107.2(16) . . ? F5_2 C3_2 C1_2 110.9(19) . . ? F6_2 C3_2 C1_2 113.8(16) . . ? F4_2 C3_2 C1_2 111.4(14) . . ? F9_2 C4_2 F7_2 105.9(18) . . ? F9_2 C4_2 F8_2 107.4(17) . . ? F7_2 C4_2 F8_2 108.1(18) . . ? F9_2 C4_2 C1_2 111.1(15) . . ? F7_2 C4_2 C1_2 111.0(17) . . ? F8_2 C4_2 C1_2 113.0(14) . . ? C1_3 O1_3 Al2 146.6(3) . . ? O1_3 C1_3 C3_3 108.2(4) . . ? O1_3 C1_3 C2_3 112.6(4) . . ? C3_3 C1_3 C2_3 108.7(4) . . ? O1_3 C1_3 C4_3 109.1(4) . . ? C3_3 C1_3 C4_3 109.4(4) . . ? C2_3 C1_3 C4_3 108.9(4) . . ? F3_3 C2_3 F2_3 108.2(4) . . ? F3_3 C2_3 F1_3 105.8(4) . . ? F2_3 C2_3 F1_3 106.2(4) . . ? F3_3 C2_3 C1_3 111.7(4) . . ? F2_3 C2_3 C1_3 113.2(4) . . ? F1_3 C2_3 C1_3 111.4(4) . . ? F4_3 C3_3 F6_3 107.7(4) . . ? F4_3 C3_3 F5_3 105.8(4) . . ? F6_3 C3_3 F5_3 107.3(4) . . ? F4_3 C3_3 C1_3 113.0(4) . . ? F6_3 C3_3 C1_3 113.8(4) . . ? F5_3 C3_3 C1_3 108.8(4) . . ? F9_3 C4_3 F8_3 109.6(4) . . ? F9_3 C4_3 F7_3 106.5(4) . . ? F8_3 C4_3 F7_3 105.7(4) . . ? F9_3 C4_3 C1_3 112.2(4) . . ? F8_3 C4_3 C1_3 112.9(4) . . ? F7_3 C4_3 C1_3 109.6(4) . . ? C1_4 O1_4 Al2 148(4) . . ? O1_4 C1_4 C2_4 111(2) . . ? O1_4 C1_4 C3_4 111(2) . . ? C2_4 C1_4 C3_4 108.9(15) . . ? O1_4 C1_4 C4_4 111(2) . . ? C2_4 C1_4 C4_4 107.2(15) . . ? C3_4 C1_4 C4_4 106.7(15) . . ? F3_4 C2_4 F1_4 112(2) . . ? F3_4 C2_4 F2_4 106(2) . . ? F1_4 C2_4 F2_4 110(2) . . ? F3_4 C2_4 C1_4 110.5(19) . . ? F1_4 C2_4 C1_4 107.6(18) . . ? F2_4 C2_4 C1_4 110.8(19) . . ? F4_4 C3_4 F5_4 113(2) . . ? F4_4 C3_4 F6_4 105(2) . . ? F5_4 C3_4 F6_4 110(2) . . ? F4_4 C3_4 C1_4 110.5(19) . . ? F5_4 C3_4 C1_4 109.2(18) . . ? F6_4 C3_4 C1_4 109.8(19) . . ? F9_4 C4_4 F7_4 113(2) . . ? F9_4 C4_4 F8_4 108(2) . . ? F7_4 C4_4 F8_4 109(2) . . ? F9_4 C4_4 C1_4 110.4(19) . . ? F7_4 C4_4 C1_4 106.8(18) . . ? F8_4 C4_4 C1_4 110.0(19) . . ? C1_5 O1_5 Al2 147.1(3) . . ? O1_5 C1_5 C3_5 107.7(3) . . ? O1_5 C1_5 C2_5 111.3(4) . . ? C3_5 C1_5 C2_5 109.7(3) . . ? O1_5 C1_5 C4_5 110.2(3) . . ? C3_5 C1_5 C4_5 109.0(3) . . ? C2_5 C1_5 C4_5 108.8(3) . . ? F3_5 C2_5 F2_5 108.1(3) . . ? F3_5 C2_5 F1_5 107.1(4) . . ? F2_5 C2_5 F1_5 106.7(3) . . ? F3_5 C2_5 C1_5 110.6(3) . . ? F2_5 C2_5 C1_5 112.8(4) . . ? F1_5 C2_5 C1_5 111.2(3) . . ? F4_5 C3_5 F5_5 107.2(3) . . ? F4_5 C3_5 F6_5 108.2(4) . . ? F5_5 C3_5 F6_5 106.9(4) . . ? F4_5 C3_5 C1_5 111.5(4) . . ? F5_5 C3_5 C1_5 110.4(4) . . ? F6_5 C3_5 C1_5 112.4(3) . . ? F7_5 C4_5 F9_5 107.9(4) . . ? F7_5 C4_5 F8_5 107.6(4) . . ? F9_5 C4_5 F8_5 107.2(3) . . ? F7_5 C4_5 C1_5 111.2(3) . . ? F9_5 C4_5 C1_5 110.7(4) . . ? F8_5 C4_5 C1_5 111.9(4) . . ? C1_6 O1_6 Al2 145.4(3) . . ? O1_6 C1_6 C4_6 111.5(4) . . ? O1_6 C1_6 C2_6 109.9(4) . . ? C4_6 C1_6 C2_6 109.8(3) . . ? O1_6 C1_6 C3_6 107.6(3) . . ? C4_6 C1_6 C3_6 108.9(4) . . ? C2_6 C1_6 C3_6 109.1(3) . . ? F3_6 C2_6 F2_6 108.0(4) . . ? F3_6 C2_6 F1_6 107.1(4) . . ? F2_6 C2_6 F1_6 106.5(3) . . ? F3_6 C2_6 C1_6 111.8(4) . . ? F2_6 C2_6 C1_6 112.8(4) . . ? F1_6 C2_6 C1_6 110.4(3) . . ? F4_6 C3_6 F6_6 107.6(4) . . ? F4_6 C3_6 F5_6 106.7(4) . . ? F6_6 C3_6 F5_6 107.3(4) . . ? F4_6 C3_6 C1_6 110.9(4) . . ? F6_6 C3_6 C1_6 112.9(4) . . ? F5_6 C3_6 C1_6 111.1(4) . . ? F9_6 C4_6 F7_6 107.8(4) . . ? F9_6 C4_6 F8_6 107.7(3) . . ? F7_6 C4_6 F8_6 107.0(4) . . ? F9_6 C4_6 C1_6 110.4(4) . . ? F7_6 C4_6 C1_6 111.0(3) . . ? F8_6 C4_6 C1_6 112.7(4) . . ? C1_8 O1_8 Al1 149.4(3) . . ? O1_8 C1_8 C2_8 111.6(3) . . ? O1_8 C1_8 C4_8 111.3(3) . . ? C2_8 C1_8 C4_8 108.8(4) . . ? O1_8 C1_8 C3_8 106.9(4) . . ? C2_8 C1_8 C3_8 109.0(4) . . ? C4_8 C1_8 C3_8 109.1(3) . . ? F3_8 C2_8 F1_8 107.2(4) . . ? F3_8 C2_8 F2_8 107.6(4) . . ? F1_8 C2_8 F2_8 107.2(4) . . ? F3_8 C2_8 C1_8 111.2(4) . . ? F1_8 C2_8 C1_8 111.4(4) . . ? F2_8 C2_8 C1_8 112.0(3) . . ? F4_8 C3_8 F5_8 108.3(4) . . ? F4_8 C3_8 F6_8 107.3(4) . . ? F5_8 C3_8 F6_8 107.6(4) . . ? F4_8 C3_8 C1_8 110.7(4) . . ? F5_8 C3_8 C1_8 111.0(4) . . ? F6_8 C3_8 C1_8 111.7(4) . . ? F7_8 C4_8 F9_8 107.5(4) . . ? F7_8 C4_8 F8_8 107.9(4) . . ? F9_8 C4_8 F8_8 107.1(4) . . ? F7_8 C4_8 C1_8 111.2(4) . . ? F9_8 C4_8 C1_8 110.2(4) . . ? F8_8 C4_8 C1_8 112.7(4) . . ? C1_9 O1_9 Al1 146.2(3) . . ? O1_9 C1_9 C3_9 107.6(4) . . ? O1_9 C1_9 C2_9 110.5(4) . . ? C3_9 C1_9 C2_9 109.2(4) . . ? O1_9 C1_9 C4_9 110.9(4) . . ? C3_9 C1_9 C4_9 109.2(4) . . ? C2_9 C1_9 C4_9 109.5(4) . . ? F3_9 C2_9 F1_9 106.8(4) . . ? F3_9 C2_9 F2_9 107.4(4) . . ? F1_9 C2_9 F2_9 107.5(4) . . ? F3_9 C2_9 C1_9 110.9(4) . . ? F1_9 C2_9 C1_9 111.4(4) . . ? F2_9 C2_9 C1_9 112.5(4) . . ? F5_9 C3_9 F4_9 107.1(5) . . ? F5_9 C3_9 F6_9 108.2(5) . . ? F4_9 C3_9 F6_9 106.9(5) . . ? F5_9 C3_9 C1_9 110.9(5) . . ? F4_9 C3_9 C1_9 111.0(5) . . ? F6_9 C3_9 C1_9 112.6(4) . . ? F7_9 C4_9 F9_9 107.6(4) . . ? F7_9 C4_9 F8_9 107.6(4) . . ? F9_9 C4_9 F8_9 107.4(4) . . ? F7_9 C4_9 C1_9 111.4(4) . . ? F9_9 C4_9 C1_9 110.4(4) . . ? F8_9 C4_9 C1_9 112.1(4) . . ? C1_10 O1_10 Al1 146.1(3) . . ? O1_10 C1_10 C2_10 107.9(4) . . ? O1_10 C1_10 C4_10 111.1(3) . . ? C2_10 C1_10 C4_10 109.1(3) . . ? O1_10 C1_10 C3_10 111.2(3) . . ? C2_10 C1_10 C3_10 109.5(4) . . ? C4_10 C1_10 C3_10 108.1(4) . . ? F3_10 C2_10 F1_10 107.5(4) . . ? F3_10 C2_10 F2_10 107.3(4) . . ? F1_10 C2_10 F2_10 107.3(4) . . ? F3_10 C2_10 C1_10 111.1(4) . . ? F1_10 C2_10 C1_10 111.7(4) . . ? F2_10 C2_10 C1_10 111.7(4) . . ? F5_10 C3_10 F4_10 107.7(4) . . ? F5_10 C3_10 F6_10 107.3(4) . . ? F4_10 C3_10 F6_10 107.2(4) . . ? F5_10 C3_10 C1_10 111.1(4) . . ? F4_10 C3_10 C1_10 110.1(4) . . ? F6_10 C3_10 C1_10 113.3(4) . . ? F8_10 C4_10 F7_10 107.4(4) . . ? F8_10 C4_10 F9_10 107.7(4) . . ? F7_10 C4_10 F9_10 106.6(4) . . ? F8_10 C4_10 C1_10 112.3(4) . . ? F7_10 C4_10 C1_10 111.7(3) . . ? F9_10 C4_10 C1_10 110.8(4) . . ? C1_11 O1_11 Al1 147.4(16) . . ? O1_11 C1_11 C2_11 111.8(11) . . ? O1_11 C1_11 C4_11 108.5(11) . . ? C2_11 C1_11 C4_11 109.1(8) . . ? O1_11 C1_11 C3_11 108.0(10) . . ? C2_11 C1_11 C3_11 109.6(8) . . ? C4_11 C1_11 C3_11 109.8(9) . . ? F3_11 C2_11 F1_11 106.2(10) . . ? F3_11 C2_11 F2_11 106.1(9) . . ? F1_11 C2_11 F2_11 107.1(10) . . ? F3_11 C2_11 C1_11 112.5(10) . . ? F1_11 C2_11 C1_11 111.0(11) . . ? F2_11 C2_11 C1_11 113.5(9) . . ? F6_11 C3_11 F4_11 109.1(10) . . ? F6_11 C3_11 F5_11 107.6(11) . . ? F4_11 C3_11 F5_11 107.7(12) . . ? F6_11 C3_11 C1_11 112.3(10) . . ? F4_11 C3_11 C1_11 110.6(10) . . ? F5_11 C3_11 C1_11 109.4(11) . . ? F9_11 C4_11 F7_11 106.8(10) . . ? F9_11 C4_11 F8_11 106.6(9) . . ? F7_11 C4_11 F8_11 106.9(9) . . ? F9_11 C4_11 C1_11 110.5(9) . . ? F7_11 C4_11 C1_11 112.5(10) . . ? F8_11 C4_11 C1_11 113.1(9) . . ? C1_12 O1_12 Al1 150.2(19) . . ? O1_12 C1_12 C2_12 110.6(14) . . ? O1_12 C1_12 C3_12 110.6(14) . . ? C2_12 C1_12 C3_12 108.8(10) . . ? O1_12 C1_12 C4_12 107.7(12) . . ? C2_12 C1_12 C4_12 110.1(10) . . ? C3_12 C1_12 C4_12 109.1(10) . . ? F3_12 C2_12 F1_12 105.5(13) . . ? F3_12 C2_12 F2_12 107.1(12) . . ? F1_12 C2_12 F2_12 108.9(12) . . ? F3_12 C2_12 C1_12 112.0(14) . . ? F1_12 C2_12 C1_12 109.8(13) . . ? F2_12 C2_12 C1_12 113.2(11) . . ? F5_12 C3_12 F4_12 106.9(13) . . ? F5_12 C3_12 F6_12 108.1(11) . . ? F4_12 C3_12 F6_12 108.0(12) . . ? F5_12 C3_12 C1_12 111.7(11) . . ? F4_12 C3_12 C1_12 110.1(12) . . ? F6_12 C3_12 C1_12 111.8(11) . . ? F8_12 C4_12 F7_12 108.7(12) . . ? F8_12 C4_12 F9_12 108.6(13) . . ? F7_12 C4_12 F9_12 106.3(14) . . ? F8_12 C4_12 C1_12 111.3(12) . . ? F7_12 C4_12 C1_12 110.3(13) . . ? F9_12 C4_12 C1_12 111.5(13) . . ? _shelx_res_file ; TITL p21c_a.res in P2(1)/c p21c_a.res created by SHELXL-2018/3 at 10:55:05 on 11-Feb-2022 REM Old TITL p21c in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.113, Rweak 0.006, Alpha 0.054 REM 0.541 for 768 systematic absences, Orientation as input REM Formula found by SHELXT: C58 N3 O31 F74 Al2 Ru8 CELL 0.71073 15.6388 15.1560 41.3591 90.000 95.868 90.000 ZERR 8.000 0.0141 0.0135 0.0394 0.000 0.021 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C N O F AL RU UNIT 232 8 136 288 8 32 SIMU 0.04 0.08 2 O1_11 C1_11 C2_11 F1_11 F2_11 F3_11 C3_11 F4_11 F5_11 = F6_11 C4_11 F7_11 F8_11 F9_11 O1_12 C1_12 C2_12 F1_12 F2_12 F3_12 C3_12 = F4_12 F5_12 F6_12 C4_12 F7_12 F8_12 F9_12 RIGU 0.004 0.004 O1_11 C1_11 C2_11 F1_11 F2_11 F3_11 C3_11 F4_11 F5_11 = F6_11 C4_11 F7_11 F8_11 F9_11 O1_12 C1_12 C2_12 F1_12 F2_12 F3_12 C3_12 = F4_12 F5_12 F6_12 C4_12 F7_12 F8_12 F9_12 SIMU 0.02 0.02 2 O1_1 C1_1 C2_1 F1_1 F2_1 F3_1 C3_1 F4_1 F5_1 F6_1 = C4_1 F7_1 F8_1 F9_1 O1_2 C1_2 C2_2 F1_2 F2_2 F3_2 C3_2 F4_2 F5_2 F6_2 = C4_2 F7_2 F8_2 F9_2 RIGU 0.002 0.002 O1_1 C1_1 C2_1 F1_1 F2_1 F3_1 C3_1 F4_1 F5_1 F6_1 = C4_1 F7_1 F8_1 F9_1 O1_2 C1_2 C2_2 F1_2 F2_2 F3_2 C3_2 F4_2 F5_2 F6_2 = C4_2 F7_2 F8_2 F9_2 SIMU 0.02 0.02 2 O1_3 C1_3 C2_3 F1_3 F2_3 F3_3 C3_3 F4_3 F5_3 F6_3 = C4_3 F7_3 F8_3 F9_3 O1_4 C1_4 C2_4 F1_4 F2_4 F3_4 C3_4 F4_4 F5_4 F6_4 = C4_4 F7_4 F8_4 F9_4 RIGU 0.002 0.002 O1_3 C1_3 C2_3 F1_3 F2_3 F3_3 C3_3 F4_3 F5_3 F6_3 = C4_3 F7_3 F8_3 F9_3 O1_4 C1_4 C2_4 F1_4 F2_4 F3_4 C3_4 F4_4 F5_4 F6_4 = C4_4 F7_4 F8_4 F9_4 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 TEMP -173.150 L.S. 10 BOND LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.030600 3.506600 FVAR 0.09275 0.82799 0.95609 0.57974 RU2 6 0.711538 0.730781 0.240424 11.00000 0.01923 0.01763 = 0.01583 -0.00255 0.00195 -0.00147 RU3 6 0.730863 0.803879 0.302154 11.00000 0.01660 0.01733 = 0.01256 -0.00006 0.00125 -0.00085 RU4 6 0.693860 0.912477 0.247710 11.00000 0.01946 0.01633 = 0.01450 0.00059 0.00181 -0.00011 RU5 6 0.344582 0.261789 0.498711 11.00000 0.01616 0.02030 = 0.01431 -0.00027 0.00236 -0.00238 RU6 6 0.255435 0.130701 0.527922 11.00000 0.01557 0.01815 = 0.01346 0.00148 0.00081 0.00009 RU7 6 0.123012 0.247833 0.532528 11.00000 0.01469 0.02229 = 0.01379 -0.00030 0.00092 0.00063 RU8 6 0.178632 0.214838 0.471337 11.00000 0.01833 0.01993 = 0.01223 0.00090 -0.00039 -0.00088 AL1 5 0.711827 0.339300 0.396869 11.00000 0.01389 0.01684 = 0.01003 0.00136 0.00044 -0.00140 AL2 5 0.785393 0.328719 0.148626 11.00000 0.01230 0.01530 = 0.01135 -0.00025 0.00066 0.00100 RU1 6 0.841686 0.841078 0.224101 11.00000 0.01644 0.02350 = 0.01547 -0.00180 0.00330 -0.00239 O1 3 0.821814 0.848046 0.149245 11.00000 0.03996 0.05273 = 0.01971 -0.00324 0.00625 -0.01142 O2 3 0.967511 0.995578 0.231851 11.00000 0.03407 0.03705 = 0.03405 0.00247 0.00708 -0.01313 O3 3 0.990886 0.711983 0.228242 11.00000 0.02503 0.03725 = 0.05777 -0.01763 -0.00103 0.00774 O4 3 0.665201 1.008567 0.181556 11.00000 0.03542 0.03735 = 0.02946 0.01381 -0.00547 -0.01085 O5 3 0.810574 1.061804 0.277488 11.00000 0.02571 0.02926 = 0.03687 -0.00876 -0.00555 -0.00380 O6 3 0.548590 0.980179 0.286583 11.00000 0.02524 0.02999 = 0.04186 -0.00369 0.01134 0.00143 O7 3 0.793315 0.929626 0.356959 11.00000 0.02298 0.03956 = 0.02792 -0.01402 0.00272 -0.00305 O8 3 0.562554 0.775283 0.333498 11.00000 0.02042 0.03926 = 0.02997 0.00044 0.00752 -0.00224 O9 3 0.830878 0.649740 0.333920 11.00000 0.04533 0.03361 = 0.02343 0.00499 -0.00356 0.00973 O10 3 0.559228 0.620072 0.259643 11.00000 0.03451 0.03096 = 0.03161 0.00210 0.00624 -0.00846 O11 3 0.833138 0.580017 0.259469 11.00000 0.04341 0.02737 = 0.03764 -0.00409 -0.00178 0.01255 O12 3 0.694644 0.686778 0.166921 11.00000 0.02970 0.03821 = 0.01841 -0.01302 0.00008 -0.00148 O13 3 0.531562 0.818694 0.215785 11.00000 0.02254 0.02757 = 0.03007 -0.00152 -0.00465 -0.00272 O14 3 0.480051 0.320462 0.552138 11.00000 0.02373 0.03276 = 0.02727 -0.00771 -0.00204 -0.00318 O15 3 0.480576 0.158414 0.465144 11.00000 0.03004 0.03096 = 0.02995 -0.00696 0.00951 -0.00357 O16 3 0.368181 0.431774 0.461382 11.00000 0.05082 0.03320 = 0.03768 0.00849 0.00936 -0.00630 O17 3 0.268639 0.210852 0.407930 11.00000 0.05741 0.03410 = 0.02081 0.00048 0.01836 0.00122 O18 3 0.137837 0.411396 0.457401 11.00000 0.04788 0.02317 = 0.03345 0.00290 -0.01280 0.00344 O19 3 -0.009544 0.159851 0.450754 11.00000 0.02364 0.03066 = 0.03836 0.00488 -0.01004 -0.00382 O20 3 0.407519 0.008601 0.515115 11.00000 0.02434 0.02934 = 0.02763 -0.00609 -0.00019 0.00794 O21 3 0.334333 0.159703 0.596779 11.00000 0.02257 0.03506 = 0.01651 0.00012 -0.00156 0.00247 O22 3 0.130803 -0.006776 0.552092 11.00000 0.03311 0.03458 = 0.04185 0.00914 0.00527 -0.00859 O23 3 0.149581 0.252145 0.606059 11.00000 0.03381 0.05463 = 0.01413 -0.00130 0.00074 0.01003 O24 3 -0.045128 0.141530 0.530259 11.00000 0.02482 0.04464 = 0.03333 0.00468 0.00140 -0.00764 O25 3 0.032408 0.426902 0.527554 11.00000 0.02397 0.02860 = 0.03415 -0.00258 -0.00527 0.00476 O26 3 0.183249 0.011519 0.466765 11.00000 0.02802 0.02653 = 0.02048 -0.00081 0.00004 0.00062 N1 2 0.236021 0.262738 0.517224 11.00000 0.01844 0.01877 = 0.01081 -0.00043 -0.00557 -0.00106 N2 2 0.792081 0.823589 0.264552 11.00000 0.01742 0.01555 = 0.01756 -0.00506 -0.00320 -0.00091 C1 1 0.831663 0.847018 0.176774 11.00000 0.01682 0.03065 = 0.03030 -0.00560 0.00340 -0.00879 C2 1 0.920363 0.938532 0.228495 11.00000 0.02113 0.03472 = 0.01168 0.00204 0.00271 0.00042 C3 1 0.935377 0.760199 0.225827 11.00000 0.02625 0.02818 = 0.03018 -0.01147 0.00474 -0.01074 C4 1 0.677726 0.974478 0.205775 11.00000 0.02545 0.02147 = 0.02520 -0.00131 0.00181 -0.00537 C5 1 0.768228 1.008148 0.266463 11.00000 0.01867 0.02475 = 0.02221 0.00194 -0.00201 0.00651 C6 1 0.602331 0.953799 0.273117 11.00000 0.02031 0.02367 = 0.02140 0.00250 -0.00518 -0.00543 C7 1 0.769903 0.883685 0.336430 11.00000 0.01702 0.02302 = 0.02354 0.00056 0.00607 0.00195 C8 1 0.625318 0.783711 0.322596 11.00000 0.02235 0.02085 = 0.01346 0.00433 -0.00303 0.00222 C9 1 0.791171 0.707114 0.323258 11.00000 0.02398 0.02840 = 0.01157 -0.00325 0.00143 -0.00303 C10 1 0.615430 0.661844 0.253422 11.00000 0.02517 0.02403 = 0.01693 -0.00176 0.00061 0.00284 C11 1 0.786879 0.634239 0.251767 11.00000 0.03602 0.02065 = 0.01930 -0.01007 0.00114 -0.00176 C12 1 0.701772 0.702627 0.193642 11.00000 0.02091 0.01935 = 0.02787 -0.00106 0.00221 -0.00113 C13 1 0.599239 0.830726 0.227045 11.00000 0.02633 0.02460 = 0.01467 -0.00217 0.00412 -0.00315 C14 1 0.430213 0.296870 0.532380 11.00000 0.02054 0.01984 = 0.01760 -0.00171 0.00584 -0.00045 C15 1 0.430920 0.199139 0.476789 11.00000 0.02291 0.02558 = 0.01464 -0.00169 0.00155 -0.00707 C16 1 0.360226 0.368165 0.475185 11.00000 0.02497 0.02817 = 0.02475 -0.00219 0.00243 -0.00436 C17 1 0.238782 0.209503 0.431622 11.00000 0.03420 0.02121 = 0.01590 0.00111 -0.00240 0.00258 C18 1 0.151732 0.340383 0.462225 11.00000 0.02776 0.02770 = 0.01523 -0.00511 -0.00506 -0.00501 C19 1 0.058237 0.183062 0.458162 11.00000 0.03075 0.01990 = 0.01586 0.00403 -0.00050 0.00355 C20 1 0.352231 0.054401 0.519168 11.00000 0.03004 0.02366 = 0.01626 0.00083 0.00011 -0.00451 C21 1 0.305610 0.147860 0.570987 11.00000 0.01914 0.02274 = 0.02554 0.00080 0.00896 0.00400 C22 1 0.176400 0.043339 0.543207 11.00000 0.02108 0.02574 = 0.01843 0.00158 -0.00780 0.00561 C23 1 0.137546 0.253532 0.578797 11.00000 0.01802 0.03286 = 0.02775 0.00628 0.00556 0.00971 C24 1 0.016985 0.182744 0.532510 11.00000 0.02488 0.03530 = 0.01527 0.00623 0.00252 0.00192 C25 1 0.064921 0.359891 0.528998 11.00000 0.01745 0.03376 = 0.02172 0.00087 -0.00059 -0.00121 C26 1 0.192083 0.083011 0.474836 11.00000 0.01560 0.02969 = 0.02114 -0.00033 0.00353 0.00241 RESI CCF3 1 PART 1 21 O1 3 0.763950 0.299220 0.187438 21.00000 0.01633 0.02517 = 0.01223 0.00095 0.00383 0.00299 C1 1 0.717522 0.314153 0.212696 21.00000 0.01837 0.02607 = 0.00954 -0.00184 0.00334 -0.00249 C2 1 0.672241 0.405304 0.210280 21.00000 0.03073 0.02721 = 0.01856 -0.00515 0.01003 0.00182 F1 4 0.602680 0.404055 0.188789 21.00000 0.02740 0.03776 = 0.02941 -0.00304 0.00432 0.01214 F2 4 0.646400 0.432923 0.238466 21.00000 0.04226 0.03974 = 0.02532 -0.01391 0.01270 0.00350 F3 4 0.723651 0.467262 0.200111 21.00000 0.03781 0.02699 = 0.03163 0.00171 0.00633 -0.00082 C3 1 0.778904 0.310958 0.244117 21.00000 0.02850 0.03365 = 0.01187 -0.00106 -0.00043 -0.00870 F4 4 0.833359 0.243524 0.244057 21.00000 0.03161 0.04638 = 0.02327 0.00835 -0.00830 0.00337 F5 4 0.826129 0.383806 0.247698 21.00000 0.04109 0.04439 = 0.02063 -0.00281 -0.00574 -0.01932 F6 4 0.736607 0.300753 0.270553 21.00000 0.04537 0.05834 = 0.00758 -0.00029 0.00338 -0.01634 C4 1 0.647687 0.241238 0.213409 21.00000 0.02146 0.03053 = 0.02578 -0.00528 0.00427 -0.00545 F7 4 0.681812 0.165932 0.225953 21.00000 0.03421 0.02994 = 0.03786 0.00473 0.00398 -0.00686 F8 4 0.585602 0.263333 0.231968 21.00000 0.02814 0.04348 = 0.04350 -0.00974 0.02111 -0.01112 F9 4 0.611283 0.223452 0.183843 21.00000 0.02027 0.04371 = 0.03047 -0.01243 -0.00272 -0.00406 PART 0 RESI 0 RESI CCF3 2 PART 2 -21 O1 3 0.764625 0.301387 0.186961 -21.00000 0.02017 0.02272 = 0.01528 -0.00351 0.00165 0.00121 C1 1 0.720862 0.312357 0.213308 -21.00000 0.02233 0.02567 = 0.01437 -0.00366 0.00192 0.00068 C2 1 0.750429 0.240385 0.238682 -21.00000 0.03042 0.03260 = 0.01753 0.00097 -0.00581 -0.00338 F1 4 0.835002 0.230257 0.241158 -21.00000 0.03024 0.03636 = 0.02306 0.01095 -0.00746 -0.00177 F2 4 0.725173 0.258997 0.267655 -21.00000 0.04331 0.03664 = 0.01639 0.00077 -0.00345 -0.00525 F3 4 0.714473 0.162739 0.229892 -21.00000 0.02893 0.02740 = 0.02263 0.00368 -0.00494 0.00008 C3 1 0.623336 0.301756 0.203347 -21.00000 0.02217 0.02734 = 0.01887 -0.00412 0.00390 0.00062 F4 4 0.591110 0.371882 0.186588 -21.00000 0.02036 0.02942 = 0.02870 -0.00054 -0.00083 0.00086 F5 4 0.607721 0.231402 0.184155 -21.00000 0.01841 0.03191 = 0.02483 -0.00952 0.00271 0.00013 F6 4 0.577026 0.290836 0.228505 -21.00000 0.02893 0.02838 = 0.02476 -0.00723 0.01025 -0.00612 C4 1 0.740009 0.404642 0.228218 -21.00000 0.03238 0.03019 = 0.01808 -0.00958 0.00455 -0.00248 F7 4 0.738843 0.466250 0.205076 -21.00000 0.03691 0.02568 = 0.01706 -0.01188 0.00757 -0.00056 F8 4 0.684412 0.428569 0.249124 -21.00000 0.04401 0.03315 = 0.01861 -0.00860 0.01075 0.00243 F9 4 0.818670 0.407743 0.244154 -21.00000 0.03685 0.03742 = 0.02602 -0.00546 -0.00240 -0.01044 PART 0 RESI 0 RESI CCF3 3 PART 1 31 O1 3 0.848000 0.422676 0.147717 31.00000 0.01317 0.01632 = 0.01764 0.00122 -0.00108 -0.00180 C1 1 0.927667 0.457612 0.152658 31.00000 0.01416 0.02270 = 0.01840 -0.00099 0.00222 -0.00492 C2 1 0.992285 0.395691 0.172368 31.00000 0.01772 0.03193 = 0.02395 0.00171 -0.00071 -0.00496 F1 4 1.023756 0.333479 0.152960 31.00000 0.02233 0.03566 = 0.04717 -0.00447 0.00457 0.00470 F2 4 1.060913 0.438403 0.186991 31.00000 0.01804 0.04622 = 0.01887 0.00186 -0.00576 -0.00680 F3 4 0.955898 0.351936 0.194618 31.00000 0.02327 0.04466 = 0.03076 0.01876 0.00049 0.00026 C3 1 0.921931 0.544530 0.171566 31.00000 0.02570 0.02933 = 0.03375 -0.00866 0.00562 -0.00842 F4 4 0.854248 0.592337 0.161140 31.00000 0.03619 0.02363 = 0.06284 -0.00861 0.00113 0.00401 F5 4 0.912746 0.525245 0.203357 31.00000 0.04704 0.05156 = 0.02492 -0.01741 0.00975 -0.01554 F6 4 0.991416 0.595872 0.171283 31.00000 0.03721 0.03351 = 0.04025 -0.00803 0.00612 -0.02044 C4 1 0.960990 0.477052 0.119161 31.00000 0.01890 0.04162 = 0.01930 0.00125 0.00221 -0.00457 F7 4 0.918237 0.548467 0.105061 31.00000 0.03105 0.05132 = 0.03531 0.02217 0.00027 -0.00301 F8 4 1.044081 0.498347 0.121686 31.00000 0.01604 0.05646 = 0.02675 0.00717 0.00650 -0.00448 F9 4 0.946771 0.411603 0.098904 31.00000 0.04520 0.05761 = 0.02420 -0.01292 0.01100 -0.00813 PART 0 RESI 0 RESI CCF3 4 PART 2 -31 O1 3 0.841248 0.419638 0.145960 -31.00000 0.01823 0.02666 = 0.02166 -0.00097 0.00325 -0.00274 C1 1 0.917459 0.460642 0.151215 -31.00000 0.01900 0.03111 = 0.02349 -0.00118 0.00356 -0.00511 C2 1 0.935082 0.519353 0.121885 -31.00000 0.02271 0.04100 = 0.02765 0.00539 0.00425 -0.00611 F1 4 0.888675 0.593315 0.123437 -31.00000 0.01975 0.03572 = 0.03324 0.00603 0.00487 -0.01053 F2 4 1.018885 0.539099 0.122900 -31.00000 0.02208 0.04905 = 0.02742 0.01038 0.00460 -0.00607 F3 4 0.915311 0.476193 0.094030 -31.00000 0.02409 0.04436 = 0.02520 0.00529 0.00731 -0.00534 C3 1 0.992221 0.393663 0.157920 -31.00000 0.01993 0.03588 = 0.02739 -0.00080 0.00203 -0.00221 F4 4 0.971842 0.331812 0.178724 -31.00000 0.02215 0.03757 = 0.03232 0.00320 0.00294 -0.00056 F5 4 1.011579 0.359859 0.129726 -31.00000 0.02101 0.03943 = 0.03022 -0.00445 0.00377 -0.00254 F6 4 1.061180 0.434244 0.173198 -31.00000 0.01992 0.03653 = 0.03004 -0.00240 0.00080 -0.00092 C4 1 0.920254 0.521866 0.181580 -31.00000 0.02768 0.03415 = 0.02947 -0.00684 0.00689 -0.00934 F7 4 0.935337 0.470087 0.207675 -31.00000 0.02429 0.03638 = 0.02445 -0.00927 0.00532 -0.01185 F8 4 0.984307 0.580302 0.181103 -31.00000 0.03154 0.03711 = 0.03267 -0.00714 0.00759 -0.01287 F9 4 0.847234 0.567089 0.181375 -31.00000 0.03090 0.03421 = 0.03775 -0.00812 0.01026 -0.00645 PART 0 RESI 0 RESI CCF3 5 O1 3 0.688578 0.349253 0.126248 11.00000 0.01345 0.01871 = 0.01268 0.00256 -0.00232 0.00282 C1 1 0.646409 0.391928 0.100669 11.00000 0.01383 0.02189 = 0.01056 0.00292 -0.00010 0.00100 C2 1 0.661920 0.492838 0.102960 11.00000 0.01913 0.02143 = 0.02336 0.00363 -0.00280 0.00433 F1 4 0.738658 0.514621 0.093099 11.00000 0.02380 0.02202 = 0.03025 0.00227 0.00507 -0.00415 F2 4 0.602533 0.539156 0.084615 11.00000 0.02618 0.02399 = 0.03473 0.00889 -0.00633 0.00767 F3 4 0.662255 0.520247 0.133543 11.00000 0.03022 0.02283 = 0.02603 -0.00564 0.00314 0.00364 C3 1 0.549374 0.372269 0.100829 11.00000 0.01542 0.02584 = 0.01787 0.00086 -0.00140 0.00139 F4 4 0.535664 0.288306 0.107538 11.00000 0.01950 0.02628 = 0.02422 0.00178 0.00088 -0.00393 F5 4 0.516108 0.420674 0.123610 11.00000 0.01884 0.03137 = 0.02788 -0.00369 0.00536 0.00590 F6 4 0.504239 0.391647 0.072312 11.00000 0.01686 0.04155 = 0.02176 0.00676 -0.00738 0.00176 C4 1 0.676854 0.357548 0.068245 11.00000 0.01719 0.02477 = 0.01463 0.00039 -0.00149 -0.00041 F7 4 0.643364 0.279093 0.060439 11.00000 0.03004 0.02460 = 0.02006 -0.00855 0.00214 -0.00362 F8 4 0.654182 0.412718 0.043241 11.00000 0.03160 0.03857 = 0.01312 0.01092 0.00028 0.00334 F9 4 0.761780 0.349893 0.070739 11.00000 0.01660 0.03108 = 0.02036 -0.00042 0.00453 0.00223 RESI 0 RESI CCF3 6 O1 3 0.844451 0.245080 0.133324 11.00000 0.01990 0.01264 = 0.02017 0.00012 0.00442 -0.00059 C1 1 0.849718 0.157109 0.128265 11.00000 0.01971 0.01797 = 0.01908 0.00067 0.00530 0.00003 C2 1 0.888294 0.110695 0.159953 11.00000 0.01819 0.01954 = 0.02342 0.00443 0.00312 0.00170 F1 4 0.828891 0.103853 0.181051 11.00000 0.02574 0.03060 = 0.02232 0.00623 0.00356 0.00154 F2 4 0.915317 0.028661 0.154753 11.00000 0.03041 0.02266 = 0.03801 0.00698 0.00276 0.01154 F3 4 0.953525 0.155420 0.174638 11.00000 0.02417 0.02963 = 0.03386 0.00781 -0.00997 -0.00112 C3 1 0.910757 0.142431 0.101223 11.00000 0.02593 0.02254 = 0.02226 0.00062 0.00816 0.00424 F4 4 0.896042 0.201671 0.077660 11.00000 0.04256 0.03070 = 0.02440 0.00679 0.01588 0.00654 F5 4 0.993402 0.151551 0.113098 11.00000 0.02294 0.04131 = 0.04733 0.00110 0.01300 0.00478 F6 4 0.902394 0.062860 0.087710 11.00000 0.04392 0.02131 = 0.03642 -0.00735 0.01781 0.00283 C4 1 0.760413 0.116907 0.116874 11.00000 0.02714 0.01586 = 0.02150 0.00322 0.00343 -0.00124 F7 4 0.736830 0.136089 0.085831 11.00000 0.03740 0.03846 = 0.02132 0.00298 -0.00247 -0.00302 F8 4 0.759206 0.028757 0.119522 11.00000 0.03278 0.01720 = 0.03872 -0.00032 0.00314 -0.00570 F9 4 0.701079 0.149005 0.134372 11.00000 0.01891 0.02942 = 0.03110 -0.00042 0.00660 0.00114 RESI 0 RESI CCF3 7 RESI 0 RESI CCF3 8 O1 3 0.799240 0.357678 0.375668 11.00000 0.01334 0.02438 = 0.01679 0.00180 0.00294 -0.00016 C1 1 0.884381 0.348019 0.373148 11.00000 0.01163 0.02330 = 0.02020 0.00189 0.00225 -0.00223 C2 1 0.939309 0.390065 0.402281 11.00000 0.02137 0.02335 = 0.02803 -0.00206 0.00194 -0.00435 F1 4 0.941764 0.338872 0.428648 11.00000 0.02817 0.04470 = 0.02170 0.00603 -0.00654 -0.00353 F2 4 1.020683 0.403287 0.396040 11.00000 0.01622 0.03860 = 0.03645 0.00247 -0.00396 -0.00728 F3 4 0.907486 0.467452 0.410045 11.00000 0.03651 0.02911 = 0.03642 -0.01341 -0.00603 0.00012 C3 1 0.903603 0.396124 0.341259 11.00000 0.01739 0.04305 = 0.02023 0.00422 0.00196 -0.00106 F4 4 0.844235 0.377795 0.317346 11.00000 0.03230 0.08279 = 0.01311 0.00421 0.00302 -0.00933 F5 4 0.905822 0.482997 0.345380 11.00000 0.03216 0.03273 = 0.04521 0.01788 0.00902 -0.00070 F6 4 0.979950 0.371318 0.331678 11.00000 0.02181 0.05713 = 0.03696 -0.00132 0.01593 -0.00308 C4 1 0.909269 0.249397 0.370873 11.00000 0.01661 0.02752 = 0.04267 -0.00588 0.00052 -0.00112 F7 4 0.885131 0.217017 0.341392 11.00000 0.03042 0.04128 = 0.05607 -0.02867 0.00335 0.00155 F8 4 0.993904 0.235747 0.377356 11.00000 0.01659 0.03354 = 0.06543 -0.00804 -0.00281 0.00447 F9 4 0.870251 0.201972 0.392226 11.00000 0.02937 0.02416 = 0.06207 0.01176 0.00037 -0.00261 RESI 0 RESI CCF3 9 O1 3 0.745771 0.353067 0.437563 11.00000 0.02466 0.03127 = 0.00978 0.00176 -0.00078 -0.00856 C1 1 0.731187 0.333678 0.468583 11.00000 0.02250 0.04130 = 0.00888 0.00485 -0.00113 -0.00683 C2 1 0.746187 0.234211 0.475545 11.00000 0.02756 0.05379 = 0.02734 0.01870 0.01114 0.00779 F1 4 0.677993 0.186243 0.464292 11.00000 0.04833 0.03498 = 0.04191 0.01261 0.01128 0.00022 F2 4 0.762386 0.217013 0.507247 11.00000 0.04813 0.08704 = 0.02990 0.03584 0.00681 0.01625 F3 4 0.812407 0.204415 0.461029 11.00000 0.04299 0.06872 = 0.05779 0.03011 0.02432 0.03053 C3 1 0.795241 0.387893 0.491421 11.00000 0.04223 0.09629 = 0.01544 -0.00837 0.00017 -0.03219 F4 4 0.799920 0.471073 0.480971 11.00000 0.08288 0.08816 = 0.02386 -0.01474 0.00559 -0.05739 F5 4 0.873844 0.354064 0.492546 11.00000 0.02774 0.16459 = 0.02943 0.00484 -0.00972 -0.02482 F6 4 0.773028 0.391764 0.521845 11.00000 0.06654 0.12097 = 0.01012 -0.00801 -0.00021 -0.02847 C4 1 0.637852 0.358848 0.474897 11.00000 0.03636 0.03741 = 0.01495 0.00537 0.00886 0.00101 F7 4 0.628990 0.445673 0.477750 11.00000 0.06540 0.03519 = 0.03657 -0.00620 0.01947 0.00278 F8 4 0.614620 0.321629 0.502032 11.00000 0.03981 0.06404 = 0.02318 0.01399 0.01656 0.00312 F9 4 0.582003 0.332152 0.450261 11.00000 0.01789 0.04696 = 0.02645 0.00649 -0.00136 0.00136 RESI 0 RESI CCF3 10 O1 3 0.669702 0.234617 0.391455 11.00000 0.01802 0.01820 = 0.01625 -0.00102 -0.00159 -0.00399 C1 1 0.623893 0.178876 0.371039 11.00000 0.01954 0.01610 = 0.01489 0.00106 -0.00109 -0.00317 C2 1 0.642200 0.083735 0.383506 11.00000 0.02542 0.02137 = 0.03459 0.00071 -0.00295 -0.00721 F1 4 0.598971 0.064807 0.408745 11.00000 0.04045 0.02964 = 0.03583 0.01312 -0.00008 -0.00819 F2 4 0.619823 0.023191 0.360261 11.00000 0.03056 0.02351 = 0.04579 -0.00604 -0.00679 -0.00736 F3 4 0.725075 0.072486 0.392973 11.00000 0.02734 0.02267 = 0.05803 -0.00386 -0.01086 0.00142 C3 1 0.649727 0.187535 0.335756 11.00000 0.03116 0.03032 = 0.02081 -0.00180 0.00635 -0.00803 F4 4 0.659978 0.272263 0.328417 11.00000 0.04879 0.03314 = 0.01944 0.00100 0.00764 -0.02044 F5 4 0.723661 0.146433 0.332686 11.00000 0.03326 0.05044 = 0.04072 -0.01450 0.01584 -0.00401 F6 4 0.591013 0.154176 0.313222 11.00000 0.04361 0.03618 = 0.02372 -0.00982 -0.00138 -0.01696 C4 1 0.526140 0.197637 0.370147 11.00000 0.02402 0.02645 = 0.02246 0.00367 -0.00197 -0.00562 F7 4 0.503114 0.268416 0.352182 11.00000 0.02915 0.02797 = 0.03092 0.00729 -0.00669 0.00189 F8 4 0.478574 0.130096 0.358030 11.00000 0.02118 0.03364 = 0.04546 0.00442 -0.00560 -0.01030 F9 4 0.504332 0.213920 0.399973 11.00000 0.02356 0.05472 = 0.02611 0.00171 0.00534 0.00165 RESI 0 RESI CCF3 11 PART 1 41 O1 3 0.631711 0.410396 0.383339 41.00000 0.02133 0.02166 = 0.01739 -0.00227 -0.00819 0.00343 C1 1 0.608959 0.494417 0.375001 41.00000 0.02771 0.01802 = 0.02742 -0.00035 0.00087 -0.00049 C2 1 0.668727 0.562802 0.393724 41.00000 0.02821 0.02215 = 0.03213 0.00296 -0.00002 0.00187 F1 4 0.746602 0.562115 0.383365 41.00000 0.02583 0.03320 = 0.04329 -0.00526 0.00566 -0.00762 F2 4 0.639106 0.646408 0.390766 41.00000 0.04195 0.01628 = 0.04394 -0.00301 0.00505 -0.00187 F3 4 0.680307 0.546328 0.425444 41.00000 0.04631 0.04032 = 0.02420 0.00116 -0.00824 -0.00949 C3 1 0.514786 0.508984 0.382952 41.00000 0.02984 0.01942 = 0.05374 -0.00083 -0.00063 0.00739 F4 4 0.465565 0.441170 0.372565 41.00000 0.01905 0.02085 = 0.08596 -0.00512 -0.01054 0.00873 F5 4 0.513385 0.514738 0.415056 41.00000 0.03083 0.05106 = 0.06776 -0.01504 0.02805 -0.00327 F6 4 0.481033 0.582776 0.369913 41.00000 0.04152 0.02129 = 0.12225 -0.00112 -0.01757 0.01170 C4 1 0.614262 0.505988 0.338028 41.00000 0.04539 0.02389 = 0.02963 0.00286 -0.00489 0.00056 F7 4 0.549564 0.466155 0.320074 41.00000 0.06571 0.03367 = 0.03605 0.00534 -0.01877 -0.00558 F8 4 0.613771 0.590559 0.328714 41.00000 0.07464 0.02590 = 0.03702 0.01376 -0.01036 -0.00184 F9 4 0.686723 0.470953 0.329454 41.00000 0.06507 0.03747 = 0.02756 0.01297 0.01211 0.01471 PART 0 RESI 0 RESI CCF3 12 PART 2 -41 O1 3 0.631491 0.416386 0.384905 -41.00000 0.01131 0.00965 = 0.02907 -0.00282 0.00867 -0.00040 C1 1 0.607712 0.499370 0.375954 -41.00000 0.02630 0.01229 = 0.02066 -0.00187 -0.00199 0.00206 C2 1 0.670451 0.567735 0.393254 -41.00000 0.02548 0.01805 = 0.02610 -0.00359 0.00190 -0.00193 F1 4 0.659101 0.571637 0.424781 -41.00000 0.03849 0.04615 = 0.01587 -0.00672 -0.00500 0.00552 F2 4 0.661248 0.648890 0.380485 -41.00000 0.03547 0.01865 = 0.03293 -0.00133 -0.00347 -0.00274 F3 4 0.752128 0.544661 0.392221 -41.00000 0.02316 0.02805 = 0.05059 -0.00840 0.00521 0.00078 C3 1 0.607168 0.511034 0.338664 -41.00000 0.05044 0.02543 = 0.02252 -0.00065 -0.00258 -0.01161 F4 4 0.570574 0.440823 0.323182 -41.00000 0.09821 0.02695 = 0.01404 0.00561 -0.02351 -0.01952 F5 4 0.686708 0.517438 0.329828 -41.00000 0.07324 0.04913 = 0.02504 0.00258 0.02199 -0.01025 F6 4 0.563098 0.583165 0.327932 -41.00000 0.07888 0.03574 = 0.02433 0.00545 -0.01628 0.00221 C4 1 0.515173 0.514630 0.385610 -41.00000 0.02022 0.02250 = 0.02951 -0.00062 -0.00979 0.00820 F7 4 0.458817 0.465953 0.367022 -41.00000 0.02086 0.01985 = 0.05735 -0.00336 -0.02487 0.00875 F8 4 0.492522 0.598538 0.382421 -41.00000 0.03658 0.02431 = 0.06645 -0.00599 -0.00300 0.01518 F9 4 0.508477 0.489869 0.416243 -41.00000 0.02560 0.06266 = 0.03904 0.00713 0.00328 -0.00081 PART 0 RESI 0 HKLF 4 REM p21c_a.res in P2(1)/c REM wR2 = 0.0867, GooF = S = 1.005, Restrained GooF = 0.832 for all data REM R1 = 0.0436 for 15319 Fo > 4sig(Fo) and 0.0889 for all 23163 data REM 1966 parameters refined using 19111 restraints END WGHT 0.0306 3.5063 REM Highest difference peak 0.807, deepest hole -1.028, 1-sigma level 0.157 Q1 1 0.4079 0.2990 0.4818 11.00000 0.05 0.81 Q2 1 1.0003 0.3747 0.1193 11.00000 0.05 0.78 Q3 1 0.4207 0.2980 0.5128 11.00000 0.05 0.73 Q4 1 0.3198 0.1936 0.5301 11.00000 0.05 0.70 Q5 1 0.6635 0.7482 0.2670 11.00000 0.05 0.68 Q6 1 0.2750 0.1995 0.4859 11.00000 0.05 0.67 Q7 1 0.7766 0.7833 0.2126 11.00000 0.05 0.67 Q8 1 0.6873 0.8863 0.2216 11.00000 0.05 0.65 Q9 1 0.2564 0.2565 0.4792 11.00000 0.05 0.64 Q10 1 0.6593 0.7602 0.3110 11.00000 0.05 0.64 Q11 1 0.8758 0.6050 0.1331 11.00000 0.05 0.64 Q12 1 0.1817 0.1863 0.5233 11.00000 0.05 0.62 Q13 1 0.7380 -0.0269 0.0850 11.00000 0.05 0.62 Q14 1 0.8063 0.8639 0.3148 11.00000 0.05 0.62 Q15 1 0.9600 0.3765 0.2902 11.00000 0.05 0.62 Q16 1 0.8862 0.7643 0.2347 11.00000 0.05 0.62 Q17 1 0.9406 0.4420 0.2063 11.00000 0.05 0.62 Q18 1 0.3245 0.1814 0.5124 11.00000 0.05 0.62 Q19 1 0.5447 0.8043 0.2890 11.00000 0.05 0.62 Q20 1 0.7970 0.6796 0.2935 11.00000 0.05 0.61 ; _shelx_res_checksum 89383 _shelx_hkl_file ; 1 0 0 11.50 2.60 -1 0 0 20.70 2.50 -1 0 0 15.00 2.00 -2 0 0 7389.96 249.58 -2 0 0 7201.58 250.47 2 0 0 6954.70 251.67 2 0 0 7117.99 249.38 2 0 0 7142.79 249.58 -3 0 0 534.15 22.10 -3 0 0 527.65 23.50 3 0 0 549.45 21.90 3 0 0 550.44 25.40 3 0 0 521.25 22.10 -4 0 0 -1.10 4.80 4 0 0 -7.50 5.30 4 0 0 1.70 3.90 -4 0 0 1.90 3.60 5 0 0 681.43 29.50 -5 0 0 731.03 30.20 -5 0 0 733.03 32.80 5 0 0 694.43 34.60 -6 0 0 1365.86 56.39 6 0 0 1379.86 52.49 -6 0 0 1272.47 52.59 6 0 0 1350.56 58.39 7 0 0 233.78 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121.49 15.30 6 -5 0 112.09 9.30 -6 -5 0 103.79 14.00 -6 -5 0 143.19 14.70 6 -5 0 116.29 23.40 -6 -5 0 97.99 14.90 -6 5 0 108.19 10.80 6 5 0 128.69 10.90 -7 -5 0 35.90 8.90 -7 -5 0 42.30 12.40 7 -5 0 53.79 7.30 7 -5 0 44.20 18.60 -7 -5 0 49.99 10.70 7 -5 0 31.10 9.70 -7 5 0 54.19 7.60 7 5 0 53.29 8.40 -7 5 0 30.50 7.50 8 -5 0 12.40 5.00 8 -5 0 -3.30 14.40 -8 -5 0 8.80 10.10 -8 -5 0 -0.10 7.10 -8 -5 0 5.50 7.60 8 -5 0 7.10 7.50 -8 5 0 7.30 6.10 8 5 0 20.40 7.10 -8 5 0 7.90 5.30 9 -5 0 233.48 22.40 -9 -5 0 197.98 20.00 -9 -5 0 221.18 21.80 9 -5 0 237.88 15.60 -9 -5 0 189.78 23.90 9 -5 0 225.28 33.80 -9 5 0 230.58 15.90 -9 5 0 227.68 20.90 9 5 0 219.98 17.60 9 5 0 268.57 18.00 -10 -5 0 482.15 28.50 10 -5 0 444.46 24.80 10 -5 0 509.85 31.00 10 -5 0 429.66 46.80 -10 -5 0 501.35 31.50 -10 -5 0 548.85 36.80 10 5 0 454.75 27.00 -10 5 0 447.36 24.80 10 5 0 444.56 27.00 -10 5 0 468.85 29.40 -11 -5 0 326.27 27.40 -11 -5 0 384.16 26.40 -11 -5 0 308.37 33.20 11 -5 0 333.97 42.80 11 -5 0 400.96 28.40 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83.99 12.50 -8 -7 0 53.49 13.70 8 -7 0 85.79 24.90 -8 -7 0 60.49 13.50 8 -7 0 66.29 9.20 -8 7 0 61.89 10.60 8 7 0 61.79 10.20 -9 -7 0 17.90 12.10 -9 -7 0 7.00 7.40 9 -7 0 14.90 10.10 9 -7 0 4.50 5.10 -9 -7 0 3.20 8.70 -9 -7 0 6.90 8.50 9 -7 0 -0.40 17.70 -9 7 0 8.00 7.10 -9 7 0 -7.70 5.00 9 7 0 14.20 7.30 10 -7 0 346.97 46.80 10 -7 0 439.36 32.20 -10 -7 0 484.15 31.10 -10 -7 0 362.46 34.90 -10 -7 0 495.35 32.70 10 -7 0 446.36 24.70 10 7 0 449.66 26.80 -10 7 0 455.45 28.60 11 -7 0 237.08 26.30 -11 -7 0 220.58 23.70 11 -7 0 124.19 33.00 -11 -7 0 149.59 23.80 -11 -7 0 215.08 24.30 -11 7 0 192.38 21.50 11 7 0 233.98 19.40 -12 -7 0 4.00 9.90 -12 -7 0 18.70 12.00 12 -7 0 -5.30 11.10 -12 -7 0 3.60 13.20 12 -7 0 35.70 24.30 12 7 0 5.50 8.10 -12 7 0 -5.60 9.00 13 -7 0 355.26 48.90 -13 -7 0 303.17 30.90 13 -7 0 347.17 33.50 -13 -7 0 289.17 35.40 -13 7 0 352.96 32.20 13 7 0 292.77 24.10 -14 -7 0 8.00 14.90 14 -7 0 45.90 18.00 -14 -7 0 26.80 14.40 14 -7 0 12.20 22.20 -14 7 0 13.20 12.00 -15 -7 0 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56.39 19.20 -12 -10 4 78.19 18.60 -12 -10 4 47.80 18.90 12 -10 -4 51.09 19.80 12 -10 -4 72.09 30.90 12 10 -4 79.09 16.80 -11 -10 4 71.89 16.90 11 -10 -4 28.20 17.10 11 -10 -4 81.09 32.20 -11 -10 4 74.99 18.40 -11 -10 4 38.50 14.70 -11 -10 4 62.49 17.70 11 10 -4 62.09 15.20 10 -10 -4 459.55 59.39 -10 -10 4 602.94 39.90 -10 -10 4 567.94 40.30 -10 -10 4 586.84 40.00 10 -10 -4 576.24 43.20 -10 -10 4 649.74 41.90 10 10 -4 592.04 36.40 9 -10 -4 117.39 32.40 -9 -10 4 84.79 18.10 -9 -10 4 74.09 15.50 -9 -10 4 41.60 13.80 9 -10 -4 78.89 12.40 9 -10 -4 44.70 16.20 -9 -10 4 69.49 17.80 -9 10 4 74.59 16.00 9 10 -4 53.69 13.70 -8 -10 4 714.43 43.20 8 -10 -4 812.62 66.69 -8 -10 4 762.32 45.50 -8 -10 4 790.72 46.70 -8 -10 4 772.02 44.90 8 -10 -4 778.72 38.30 8 -10 -4 809.12 48.60 -8 10 4 765.62 36.50 8 10 -4 845.82 43.20 7 -10 -4 200.98 18.40 -7 -10 4 182.58 22.80 7 -10 -4 149.39 23.10 -7 -10 4 181.58 20.80 -7 -10 4 197.68 24.30 -7 -10 4 227.08 26.20 7 -10 -4 183.78 36.90 7 10 -4 186.38 21.10 -7 10 4 189.88 14.20 6 -10 -4 46.60 23.60 6 -10 -4 20.00 12.20 -6 -10 4 13.60 9.20 -6 -10 4 13.90 10.70 6 -10 -4 6.00 6.60 -6 -10 4 30.80 13.50 6 -10 -4 6.70 5.20 -6 -10 4 4.20 8.70 6 10 -4 7.40 8.50 -6 10 4 12.40 5.40 -5 -10 4 -6.60 8.50 5 -10 -4 8.20 10.10 -5 -10 4 25.20 12.20 5 -10 -4 3.00 6.00 -5 -10 4 -9.80 7.20 5 -10 -4 18.20 19.70 -5 -10 4 0.90 8.00 5 -10 -4 11.20 5.30 -5 10 4 4.80 4.40 5 10 -4 2.90 8.10 -4 -10 4 107.89 18.20 4 -10 -4 131.29 20.00 -4 -10 4 158.78 22.60 -4 -10 4 144.69 14.50 4 -10 -4 141.19 15.70 4 -10 -4 131.49 10.70 -4 -10 4 106.29 15.70 4 -10 -4 113.09 28.30 -4 10 4 143.59 10.90 -3 -10 4 97.89 10.60 -3 -10 4 62.89 12.40 3 -10 -4 74.99 11.90 -3 -10 4 62.79 14.60 3 -10 -4 93.99 17.70 -3 -10 4 69.09 17.80 3 -10 -4 52.09 21.80 3 -10 -4 92.49 9.20 -3 10 4 102.99 10.00 -2 -10 4 392.76 19.70 -2 -10 4 375.36 28.70 2 -10 -4 401.36 24.60 -2 -10 4 386.36 25.00 2 -10 -4 372.16 28.90 2 -10 -4 392.16 19.60 -2 -10 4 389.66 38.20 2 -10 -4 296.27 39.80 1 -10 -4 570.14 35.40 1 -10 -4 564.14 45.60 1 -10 -4 558.54 31.20 -1 -10 4 527.95 30.70 -1 -10 4 662.03 45.60 -1 -10 4 552.34 24.30 -1 -10 4 540.75 34.60 1 -10 -4 563.24 26.00 0 -10 -4 19.10 8.70 0 -10 -4 14.80 5.80 0 -10 -4 30.30 16.70 0 -10 4 18.20 4.20 0 -10 4 27.40 8.50 0 -10 -4 23.50 10.70 0 -10 4 0.70 13.50 0 -10 4 18.90 10.20 1 -10 4 767.62 42.50 -1 -10 -4 751.62 49.80 -1 -10 -4 758.72 39.20 -1 -10 -4 774.22 42.70 -1 -10 -4 782.42 34.20 1 -10 4 714.83 52.79 1 -10 4 680.43 35.60 -2 -10 -4 11.70 10.10 -2 -10 -4 -1.50 5.50 -2 -10 -4 12.40 12.80 -2 -10 -4 6.20 7.60 2 -10 4 14.90 10.00 2 -10 4 -7.70 5.30 2 -10 4 1.40 16.00 3 -10 4 -6.40 17.20 3 -10 4 -14.00 7.20 -3 -10 -4 -5.40 6.10 -3 -10 -4 11.10 12.50 -3 -10 -4 -3.80 6.20 3 -10 4 -0.20 5.40 -3 -10 -4 -8.70 7.90 4 -10 4 434.76 30.60 -4 -10 -4 355.66 29.00 4 -10 4 454.15 23.70 -4 -10 -4 406.46 32.70 -4 -10 -4 385.06 24.70 4 -10 4 423.66 51.39 -4 -10 -4 475.45 30.00 5 -10 4 -16.50 16.70 -5 -10 -4 -5.80 7.00 5 -10 4 6.00 9.60 -5 -10 -4 13.80 11.90 -5 -10 -4 6.80 10.50 5 -10 4 5.30 5.50 -5 -10 -4 9.70 7.70 -6 -10 -4 86.99 14.80 -6 -10 -4 134.79 18.70 -6 -10 -4 109.39 18.70 -6 -10 -4 127.69 19.80 6 -10 4 152.58 34.10 6 -10 4 175.38 22.80 -7 -10 -4 4.20 9.90 7 -10 4 -2.40 9.60 7 -10 4 -7.00 19.40 -7 -10 -4 1.40 10.20 -7 -10 -4 10.30 10.70 7 10 4 -7.40 7.20 -8 -10 -4 149.69 21.10 8 -10 4 126.19 35.30 -8 -10 -4 151.78 21.40 -8 -10 -4 146.39 22.20 8 -10 4 138.29 21.70 9 -10 4 79.69 32.40 -9 -10 -4 77.29 17.30 -9 -10 -4 92.39 18.40 9 -10 4 87.19 19.10 -9 -10 -4 62.09 16.60 -10 -10 -4 31.40 13.90 10 -10 4 40.70 15.70 -10 -10 -4 25.80 14.30 -10 -10 -4 30.00 13.90 10 -10 4 -0.70 27.40 11 -10 4 -9.60 10.90 -11 -10 -4 7.20 11.80 11 -10 4 -4.60 24.40 -11 -10 -4 -3.70 13.80 12 -10 4 72.09 37.10 -12 -10 -4 79.09 20.00 12 -10 4 119.79 23.30 -12 -10 -4 103.59 19.60 -13 -10 -4 49.40 19.70 13 -10 4 70.29 35.70 -13 -10 -4 35.50 16.70 -14 -10 -4 115.39 26.60 -14 -10 -4 129.39 24.70 14 -10 4 132.29 41.00 -15 -10 -4 17.20 19.40 15 -10 4 48.80 37.50 -15 -10 -4 27.00 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93.89 17.10 -8 -11 4 32.00 14.40 8 -11 -4 -7.50 22.20 8 -11 -4 26.10 14.60 -8 -11 4 -8.00 11.70 -8 -11 4 0.00 9.40 -8 -11 4 -6.70 9.90 8 -11 -4 -0.90 6.50 8 11 -4 -0.70 9.20 -7 -11 4 39.50 14.50 7 -11 -4 20.90 14.70 -7 -11 4 42.10 12.80 7 -11 -4 15.10 24.50 -7 -11 4 14.20 11.00 -7 -11 4 24.10 14.70 7 -11 -4 66.29 11.90 7 11 -4 40.10 12.80 6 -11 -4 41.30 25.00 -6 -11 4 95.19 20.20 6 -11 -4 59.29 9.40 -6 -11 4 74.69 14.90 6 -11 -4 88.29 18.90 6 -11 -4 69.59 12.50 -6 -11 4 61.39 16.80 -6 -11 4 66.89 12.70 6 11 -4 78.39 15.50 5 -11 -4 120.89 15.30 -5 -11 4 134.79 22.90 5 -11 -4 133.79 12.20 -5 -11 4 106.99 17.00 -5 -11 4 91.09 18.90 -5 -11 4 119.59 15.00 5 -11 -4 132.19 31.70 5 -11 -4 119.29 21.20 4 -11 -4 152.48 11.80 4 -11 -4 188.68 24.80 -4 -11 4 132.69 14.30 -4 -11 4 230.88 26.90 -4 -11 4 130.59 18.00 4 -11 -4 160.08 17.30 -4 -11 4 181.08 27.20 4 -11 -4 142.29 32.70 -3 -11 4 129.99 13.90 -3 -11 4 129.59 25.20 3 -11 -4 146.59 11.10 3 -11 -4 108.09 29.00 3 -11 -4 108.79 19.10 3 -11 -4 148.89 16.90 -3 -11 4 127.19 17.10 -3 -11 4 139.39 19.60 -3 11 4 135.79 12.20 -2 -11 4 291.47 22.10 2 -11 -4 229.18 37.10 -2 -11 4 293.77 28.50 2 -11 -4 246.38 21.10 -2 -11 4 312.77 36.90 2 -11 -4 304.67 30.00 2 -11 -4 316.57 17.00 -1 -11 4 37.50 10.10 1 -11 -4 10.20 10.20 -1 -11 4 24.80 18.20 -1 -11 4 38.00 12.70 1 -11 -4 19.70 18.00 1 -11 -4 19.60 8.70 1 -11 -4 23.60 6.00 0 -11 4 272.47 20.80 0 -11 -4 236.18 22.60 0 -11 4 294.27 39.40 0 -11 -4 250.47 16.20 0 -11 -4 271.67 28.40 0 -11 -4 311.77 38.80 0 -11 4 262.37 28.10 -1 -11 -4 313.87 30.60 1 -11 4 350.76 23.10 1 -11 4 459.25 49.60 1 -11 4 381.86 29.80 -1 -11 -4 365.66 20.60 -1 -11 -4 337.47 40.00 -1 -11 -4 359.96 25.40 -2 -11 -4 216.58 24.80 2 -11 4 232.18 25.70 -2 -11 -4 153.88 27.10 -2 -11 -4 185.28 16.50 2 -11 4 194.98 34.80 2 -11 4 219.88 19.30 -2 -11 -4 190.48 20.50 -3 -11 -4 251.27 23.90 -3 -11 -4 266.67 33.70 3 -11 4 180.38 36.90 3 -11 4 237.28 17.80 -3 -11 -4 205.58 17.00 -3 -11 -4 230.78 26.20 3 -11 4 254.57 26.90 -4 -11 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34.90 21.00 -11 -11 21 62.19 21.30 11 -11 -21 26.30 14.20 11 -11 -21 38.50 13.50 -11 -11 21 54.59 17.30 11 -11 -21 33.90 23.20 -11 -11 21 67.29 20.60 11 11 -21 41.40 17.20 -11 11 21 47.20 12.70 -10 -11 21 307.37 37.80 10 -11 -21 217.18 25.40 -10 -11 21 272.77 35.60 -10 -11 21 210.38 27.60 10 -11 -21 285.17 37.80 10 -11 -21 311.97 42.60 10 -11 -21 306.27 28.30 -10 11 21 287.17 26.30 10 11 -21 207.08 29.60 -9 -11 21 36.80 14.20 -9 -11 21 98.19 23.40 9 -11 -21 40.70 14.00 9 -11 -21 38.80 11.80 -9 -11 21 53.29 18.20 9 -11 -21 53.69 25.10 9 -11 -21 48.40 19.80 9 11 -21 29.30 14.60 -9 11 21 51.89 12.00 8 -11 -21 276.67 38.60 -8 -11 21 262.27 35.40 8 -11 -21 274.47 24.90 8 -11 -21 353.06 40.90 -8 -11 21 225.98 29.80 -8 -11 21 196.38 24.40 8 -11 -21 287.87 28.80 -8 11 21 250.47 23.50 8 11 -21 248.38 30.70 7 -11 -21 237.98 26.70 7 -11 -21 186.18 33.70 -7 -11 21 303.37 29.50 7 -11 -21 235.08 34.20 -7 -11 21 175.48 30.20 7 -11 -21 275.07 22.10 -7 -11 21 225.88 30.00 7 11 -21 240.58 29.90 -7 11 21 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33.30 -1 -13 -21 117.59 20.10 2 -13 21 64.39 18.60 -2 -13 -21 107.99 20.00 2 -13 21 36.80 26.10 -2 -13 -21 81.59 20.00 -2 -13 -21 84.99 15.90 -3 -13 -21 4.10 11.60 3 -13 21 -4.00 12.30 -3 -13 -21 -11.80 9.00 -3 -13 -21 -9.00 8.20 3 -13 21 8.80 26.30 -4 -13 -21 16.60 11.00 4 -13 21 -10.30 12.00 -4 -13 -21 10.00 10.30 4 -13 21 26.10 28.40 -4 -13 -21 6.50 13.20 -5 -13 -21 -13.50 9.90 5 -13 21 -9.50 12.30 5 -13 21 -8.10 25.30 -5 -13 -21 3.80 11.10 6 -13 21 15.00 18.00 -6 -13 -21 46.40 15.80 -6 -13 -21 30.90 15.20 6 -13 21 55.49 35.10 -7 -13 -21 12.90 11.20 -7 -13 -21 -17.40 10.20 7 -13 21 -6.50 29.20 8 -13 21 88.49 42.00 -8 -13 -21 82.29 20.20 -8 -13 -21 55.09 17.10 -9 -13 -21 0.40 12.30 -9 -13 -21 -2.30 13.30 9 -13 21 -23.60 29.40 10 -13 21 -1.30 38.10 -10 -13 -21 22.40 17.00 -10 -13 -21 11.50 13.00 -11 -13 -21 21.20 18.00 -11 -13 -21 55.19 18.30 -12 -13 -21 8.20 17.10 -12 -13 -21 8.10 17.30 -13 -14 21 11.70 19.90 -13 -14 21 14.70 26.30 -12 -14 21 -13.50 20.90 -12 -14 21 1.50 16.50 12 -14 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143.49 22.90 11 -11 -22 102.99 30.30 -11 11 22 116.19 18.00 11 11 -22 116.39 23.10 10 -11 -22 72.09 25.30 10 -11 -22 78.79 17.80 10 -11 -22 61.79 14.90 -10 -11 22 60.09 17.50 -10 -11 22 26.40 17.20 10 -11 -22 50.89 21.40 -10 -11 22 51.39 19.80 10 11 -22 39.50 15.80 -10 11 22 50.79 13.10 9 -11 -22 50.09 15.10 -9 -11 22 22.00 13.40 -9 -11 22 32.00 18.10 9 -11 -22 16.90 16.20 9 -11 -22 37.40 22.10 -9 -11 22 33.90 17.80 9 -11 -22 29.80 11.70 -9 11 22 25.90 10.20 9 11 -22 54.49 17.40 8 -11 -22 28.30 19.40 8 -11 -22 23.20 13.10 8 -11 -22 1.90 8.50 -8 -11 22 16.30 16.40 -8 -11 22 3.20 11.40 -8 -11 22 11.20 13.90 8 -11 -22 29.60 17.50 -8 11 22 3.20 7.60 8 11 -22 22.40 13.40 7 -11 -22 253.27 27.80 -7 -11 22 243.18 34.30 7 -11 -22 255.77 23.30 7 -11 -22 232.78 33.80 -7 -11 22 160.58 22.60 7 -11 -22 257.07 35.50 -7 -11 22 231.08 29.80 7 11 -22 251.27 30.20 -7 11 22 219.08 21.50 -6 -11 22 20.80 11.60 6 -11 -22 4.00 9.40 6 -11 -22 4.00 8.10 6 -11 -22 -1.80 17.90 6 -11 -22 10.00 15.20 -6 -11 22 1.40 12.00 -6 -11 22 20.60 16.20 6 11 -22 -12.40 10.60 -6 11 22 10.80 8.60 -5 -11 22 141.39 23.40 5 -11 -22 224.58 31.50 -5 -11 22 185.78 21.70 -5 -11 22 270.87 36.50 5 -11 -22 227.48 26.30 5 -11 -22 211.18 20.70 -5 11 22 151.98 18.40 5 11 -22 214.88 27.80 4 -11 -22 87.59 22.20 4 -11 -22 91.19 17.70 -4 -11 22 63.09 21.80 -4 -11 22 69.19 14.20 4 -11 -22 53.69 12.30 -4 -11 22 70.39 18.30 4 11 -22 60.09 16.90 -4 11 22 72.79 13.50 3 -11 -22 8.40 10.00 3 -11 -22 4.40 7.30 -3 -11 22 19.70 12.90 -3 -11 22 11.80 8.80 3 -11 -22 13.90 14.30 -3 -11 22 -14.00 13.60 -2 -11 22 50.19 21.50 -2 -11 22 76.09 17.70 2 -11 -22 25.20 10.20 -2 -11 22 50.39 14.70 2 -11 -22 50.09 17.00 2 -11 -22 28.00 11.40 -1 -11 22 147.09 31.50 1 -11 -22 121.09 20.10 1 -11 -22 129.69 16.80 1 -11 -22 150.98 23.90 -1 -11 22 83.09 18.40 0 -11 22 60.19 16.10 0 -11 -22 79.09 15.80 0 -11 -22 99.39 20.20 0 -11 -22 60.59 13.10 0 -11 22 57.39 24.90 -1 -11 -22 175.48 20.20 -1 -11 -22 157.48 23.30 1 -11 22 239.18 40.90 1 -11 22 193.28 25.00 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12 22 90.19 21.80 14 -12 -22 23.60 15.10 14 -12 -22 66.29 28.90 -14 -12 22 20.20 21.40 -14 -12 22 16.30 18.50 -14 12 22 18.00 14.90 -13 -12 22 -4.80 20.30 -13 -12 22 16.50 19.80 13 -12 -22 25.60 28.50 13 -12 -22 -0.50 12.90 13 -12 -22 1.40 23.20 -13 -12 22 -4.40 13.90 13 12 -22 -2.40 14.20 -13 12 22 6.00 11.30 12 -12 -22 36.50 15.70 12 -12 -22 30.00 25.20 12 -12 -22 54.49 28.30 -12 -12 22 41.20 18.20 -12 -12 22 93.89 26.70 -12 -12 22 33.20 21.00 -12 12 22 62.39 14.90 12 12 -22 48.50 19.70 -11 -12 22 6.50 19.80 -11 -12 22 8.40 13.10 11 -12 -22 3.30 10.90 -11 -12 22 10.20 17.00 11 -12 -22 32.80 13.00 11 -12 -22 7.30 18.70 11 -12 -22 16.00 19.30 -11 12 22 -3.30 8.40 11 12 -22 10.50 14.50 10 -12 -22 500.35 52.69 -10 -12 22 325.27 41.70 10 -12 -22 385.26 35.20 10 -12 -22 273.87 42.90 -10 -12 22 338.67 36.20 10 -12 -22 345.37 28.10 -10 -12 22 422.86 44.90 -10 12 22 361.56 27.40 10 12 -22 340.47 38.50 9 -12 -22 5.10 19.30 9 -12 -22 22.10 10.40 9 -12 -22 -4.00 16.20 -9 -12 22 2.80 17.60 -9 -12 22 11.30 12.80 9 -12 -22 -3.20 10.70 -9 -12 22 -9.50 15.90 -9 12 22 -7.60 7.40 9 12 -22 5.00 13.50 8 -12 -22 11.90 19.10 -8 -12 22 -3.20 16.40 8 -12 -22 -3.70 8.50 8 -12 -22 -6.80 9.70 -8 -12 22 37.80 16.30 -8 -12 22 4.40 12.90 8 -12 -22 13.50 16.70 8 12 -22 -9.60 12.10 -8 12 22 10.20 9.10 7 -12 -22 -6.00 10.00 -7 -12 22 17.60 17.40 -7 -12 22 4.50 13.50 -7 -12 22 0.80 10.90 7 -12 -22 -2.90 7.40 7 -12 -22 12.80 17.10 7 12 -22 -3.10 12.40 -7 12 22 -3.60 6.70 -6 -12 22 9.80 16.60 6 -12 -22 -4.70 12.60 6 -12 -22 19.10 11.50 -6 -12 22 5.90 10.00 -6 -12 22 -10.40 12.50 6 -12 -22 21.00 9.80 -6 12 22 1.00 7.40 6 12 -22 10.60 13.70 5 -12 -22 145.89 17.60 -5 -12 22 141.49 24.70 -5 -12 22 119.39 18.80 -5 -12 22 70.49 24.60 5 -12 -22 123.89 26.00 5 -12 -22 182.08 22.80 5 12 -22 92.79 21.30 -5 12 22 153.78 18.50 4 -12 -22 8.20 10.10 -4 -12 22 9.60 9.90 4 -12 -22 4.00 15.30 4 -12 -22 19.60 9.50 -4 -12 22 30.50 18.80 -4 -12 22 21.80 13.80 -4 12 22 8.80 9.10 -3 -12 22 62.09 25.50 3 -12 -22 75.99 13.70 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62.39 17.00 -6 -15 -22 20.00 14.20 -6 -15 -22 6.40 13.40 6 -15 22 0.20 42.70 -7 -15 -22 64.39 19.10 -7 -15 -22 44.80 17.10 -8 -15 -22 21.00 16.60 -8 -15 -22 19.70 15.30 -9 -15 -22 68.09 21.20 -9 -15 -22 88.89 25.10 9 -16 -22 5.30 15.20 -9 -16 22 5.00 15.70 9 -16 -22 16.80 24.40 -9 -16 22 24.30 23.20 8 -16 -22 88.39 31.70 -8 -16 22 90.59 21.70 -8 -16 22 97.79 28.90 8 -16 -22 162.18 27.20 7 -16 -22 52.09 27.40 -7 -16 22 14.70 21.00 7 -16 -22 44.20 18.20 -7 -16 22 46.10 17.90 6 -16 -22 12.20 22.30 -6 -16 22 8.50 25.90 -6 -16 22 55.19 23.80 6 -16 -22 32.40 15.60 5 -16 -22 25.70 14.60 5 -16 -22 45.20 24.80 -5 -16 22 -19.40 21.90 -5 -16 22 -22.20 16.10 4 -16 -22 17.00 22.00 -4 -16 22 18.30 28.50 -4 -16 22 24.30 18.70 4 -16 -22 60.29 19.80 -3 -16 22 9.50 17.00 -3 -16 22 0.80 26.00 3 -16 -22 -6.40 18.00 3 -16 -22 -11.90 12.90 -2 -16 22 29.40 31.30 2 -16 -22 37.50 23.20 -2 -16 22 69.79 23.90 2 -16 -22 37.50 15.90 1 -16 -22 41.60 17.90 -1 -16 22 5.10 17.00 1 -16 -22 19.10 13.10 -1 -16 22 22.50 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23 70.99 14.30 7 14 -23 76.79 21.20 6 -14 -23 6.00 9.70 6 -14 -23 -1.90 11.40 -6 -14 23 5.10 17.40 -6 -14 23 9.40 21.00 -6 -14 23 5.70 11.70 6 -14 -23 -3.30 16.90 -6 14 23 7.70 8.60 -5 -14 23 20.30 23.60 -5 -14 23 7.30 15.80 5 -14 -23 20.30 18.90 5 -14 -23 15.50 12.10 5 -14 -23 27.90 11.50 -5 14 23 22.10 10.00 4 -14 -23 45.10 20.80 4 -14 -23 42.20 11.50 -4 -14 23 53.39 19.80 -4 -14 23 37.70 26.60 4 -14 -23 43.70 16.40 -4 14 23 16.80 9.30 3 -14 -23 13.60 18.20 3 -14 -23 4.90 8.70 -3 -14 23 -1.60 21.70 3 -14 -23 -16.50 8.80 -3 -14 23 15.60 15.40 -3 14 23 -1.00 7.90 -2 -14 23 -2.40 13.80 2 -14 -23 -6.80 11.10 -2 -14 23 -10.20 20.70 2 -14 -23 -12.90 8.10 2 -14 -23 13.90 17.50 -1 -14 23 14.00 25.00 1 -14 -23 17.10 13.40 1 -14 -23 26.30 17.40 1 -14 -23 21.40 11.40 -1 -14 23 50.09 18.30 0 -14 -23 18.60 10.70 0 -14 23 13.40 15.60 0 -14 -23 21.10 18.90 0 -14 23 36.60 30.10 0 -14 -23 22.40 13.40 -1 -14 -23 3.20 15.70 -1 -14 -23 16.70 11.30 1 -14 23 -2.20 25.80 1 -14 23 12.10 15.00 -1 -14 -23 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25 44.30 11.70 -3 -10 25 60.09 20.80 3 -10 -25 16.40 14.20 3 -10 -25 54.89 14.50 3 -10 -25 17.70 9.20 -3 -10 25 17.10 13.00 3 10 -25 46.10 14.60 2 -10 -25 86.19 14.80 2 -10 -25 81.39 16.70 2 -10 -25 90.39 21.00 -2 -10 25 58.59 16.10 -2 -10 25 92.69 24.00 -1 -10 25 40.10 13.50 1 -10 -25 72.39 15.60 1 -10 -25 57.99 12.40 1 -10 -25 57.09 16.60 -1 -10 25 44.50 20.10 0 -10 -25 22.70 13.40 0 -10 25 -5.50 15.80 0 -10 25 30.30 12.10 0 -10 -25 24.90 10.60 0 -10 -25 14.80 10.50 -1 -10 -25 79.59 15.50 -1 -10 -25 77.89 14.50 1 -10 25 91.19 18.30 1 -10 25 87.69 26.30 -1 -10 -25 34.40 15.10 -2 -10 -25 -6.50 8.60 2 -10 25 5.70 10.20 -2 -10 -25 -2.00 8.40 2 -10 25 -1.30 17.60 -2 -10 -25 0.30 8.30 3 -10 25 167.18 36.50 -3 -10 -25 192.18 23.30 -3 -10 -25 177.88 22.30 3 -10 25 250.37 26.60 -4 -10 -25 -2.90 9.30 4 -10 25 4.50 10.70 4 -10 25 -9.60 20.30 -4 -10 -25 -3.70 10.00 -5 -10 -25 309.37 30.70 -5 -10 -25 330.37 32.20 5 -10 25 229.98 42.70 -6 -10 -25 14.40 12.10 6 -10 25 18.20 23.00 -6 -10 -25 10.40 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28.30 22.10 12 -11 -25 9.90 13.10 12 -11 -25 8.30 12.50 -12 -11 25 -0.50 17.00 12 -11 -25 1.30 22.10 12 11 -25 9.40 14.90 -12 11 25 5.50 10.90 -11 -11 25 10.70 13.70 11 -11 -25 28.30 14.60 11 -11 -25 0.70 10.80 11 -11 -25 42.40 25.80 -11 -11 25 34.30 21.20 -11 -11 25 7.00 15.60 11 -11 -25 43.00 23.20 11 11 -25 20.30 15.80 -11 11 25 39.90 12.60 10 -11 -25 51.89 14.50 -10 -11 25 55.29 17.00 -10 -11 25 48.40 18.70 10 -11 -25 65.99 24.70 10 -11 -25 103.39 19.80 10 -11 -25 77.39 23.50 -10 -11 25 53.39 21.80 -10 11 25 83.19 15.50 10 11 -25 40.50 17.60 -9 -11 25 25.00 15.50 9 -11 -25 2.10 18.10 9 -11 -25 19.40 18.50 9 -11 -25 17.90 10.30 9 -11 -25 20.20 11.60 -9 -11 25 24.70 18.10 -9 -11 25 14.10 13.00 9 11 -25 32.60 16.10 -9 11 25 23.50 10.40 -8 -11 25 26.00 13.20 -8 -11 25 8.20 13.60 8 -11 -25 9.70 11.40 -8 -11 25 8.10 15.90 8 -11 -25 -1.20 7.60 8 -11 -25 8.20 16.80 8 11 -25 -9.10 11.40 -8 11 25 8.70 8.50 7 -11 -25 282.97 38.30 -7 -11 25 228.48 26.30 -7 -11 25 282.97 37.40 -7 -11 25 263.47 32.60 7 -11 -25 285.47 29.80 7 -11 -25 248.38 24.30 7 11 -25 237.18 30.70 -7 11 25 291.17 26.30 -6 -11 25 11.60 14.20 6 -11 -25 5.60 10.60 6 -11 -25 -8.00 6.80 -6 -11 25 -16.10 8.10 -6 -11 25 9.80 16.30 6 -11 -25 -9.50 13.80 -6 11 25 5.70 8.00 6 11 -25 -3.70 11.00 -5 -11 25 31.80 11.90 -5 -11 25 44.80 16.10 5 -11 -25 66.59 16.50 -5 -11 25 55.59 21.50 5 -11 -25 40.00 11.40 5 -11 -25 36.00 19.20 5 11 -25 56.29 17.10 -5 11 25 45.40 11.80 4 -11 -25 37.30 13.70 -4 -11 25 62.69 14.00 4 -11 -25 35.30 11.20 -4 -11 25 64.69 17.70 4 -11 -25 7.10 15.90 -4 -11 25 50.09 21.50 4 11 -25 26.00 14.30 -4 11 25 40.10 11.40 3 -11 -25 74.49 21.90 3 -11 -25 66.09 13.50 -3 -11 25 89.19 19.10 -3 -11 25 57.29 23.20 3 -11 -25 84.29 17.60 -2 -11 25 18.70 13.00 2 -11 -25 9.90 11.10 2 -11 -25 8.20 14.10 2 -11 -25 21.30 9.90 -2 -11 25 -15.10 14.40 1 -11 -25 67.89 19.00 1 -11 -25 30.20 10.90 -1 -11 25 37.30 21.20 -1 -11 25 19.00 13.50 1 -11 -25 21.00 10.90 0 -11 -25 4.20 9.10 0 -11 25 16.70 20.60 0 -11 -25 9.30 9.70 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149.49 19.40 10 -2 -28 202.48 22.70 -10 -2 28 232.28 25.90 10 -2 -28 228.38 26.20 10 -2 -28 187.98 23.20 10 2 -28 191.58 24.80 -10 2 28 159.28 21.90 -10 2 28 199.28 20.90 10 2 -28 163.68 21.60 10 2 -28 174.78 23.60 9 -2 -28 2.80 8.50 9 -2 -28 -6.20 6.60 9 -2 -28 3.10 9.30 -9 -2 28 11.60 7.30 9 -2 -28 11.70 9.50 -9 -2 28 7.10 9.60 -9 -2 28 5.60 10.10 9 2 -28 0.00 9.40 -9 2 28 4.20 7.40 9 2 -28 8.40 8.70 -9 2 28 -6.80 8.30 9 2 -28 3.60 9.10 -8 -2 28 528.55 34.90 -8 -2 28 594.94 35.20 8 -2 -28 547.25 34.20 -8 -2 28 539.25 30.50 8 -2 -28 528.45 31.40 8 -2 -28 510.75 33.30 8 -2 -28 511.65 36.10 8 2 -28 524.75 35.10 -8 2 28 581.64 35.10 8 2 -28 551.94 34.70 -8 2 28 548.15 30.70 8 2 -28 496.05 33.30 -7 -2 28 55.09 13.40 -7 -2 28 72.19 11.00 7 -2 -28 68.89 12.20 7 -2 -28 79.79 14.30 7 -2 -28 49.70 11.80 -7 -2 28 70.09 13.50 7 -2 -28 33.20 13.70 -7 2 28 58.69 11.00 -7 2 28 49.20 12.40 7 2 -28 61.19 14.50 7 2 -28 47.60 10.40 7 2 -28 54.59 12.70 7 2 -28 73.79 13.80 6 -2 -28 81.89 12.10 6 -2 -28 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283.57 20.10 3 2 -28 293.07 21.80 2 -2 -28 27.10 8.30 -2 -2 28 34.50 10.20 -2 -2 28 37.70 7.30 -2 -2 28 34.20 8.20 -2 -2 28 42.30 9.10 2 -2 -28 39.30 9.00 2 -2 -28 42.50 11.00 2 -2 -28 33.50 7.80 2 2 -28 23.60 7.50 2 2 -28 45.00 10.50 2 2 -28 34.40 7.50 2 2 -28 34.50 7.90 1 -2 -28 2.00 6.00 -1 -2 28 0.70 4.30 1 -2 -28 -0.30 4.20 -1 -2 28 5.70 5.60 1 -2 -28 0.80 5.40 1 -2 -28 11.70 6.70 -1 -2 28 10.40 7.70 1 2 -28 8.40 5.60 1 2 -28 -4.20 6.30 1 2 -28 4.70 4.70 -1 2 28 6.80 5.10 1 2 -28 -0.20 4.20 0 -2 -28 383.36 20.40 0 -2 -28 363.66 22.20 0 -2 28 329.87 20.30 0 -2 28 331.17 20.00 0 -2 -28 342.77 22.40 0 -2 -28 342.17 22.80 0 -2 28 370.86 27.20 0 2 -28 369.66 21.00 0 2 -28 355.16 20.00 0 2 -28 341.67 20.40 0 2 -28 369.96 24.20 0 2 28 337.37 21.10 -1 -2 -28 66.59 11.50 -1 -2 -28 59.89 10.80 1 -2 28 55.69 14.40 -1 -2 -28 62.29 10.00 1 -2 28 47.00 8.10 1 -2 28 45.80 8.60 -1 2 -28 63.09 9.00 1 2 28 54.59 10.40 -1 2 -28 82.19 10.40 -1 2 -28 61.69 11.80 -1 2 -28 80.79 9.90 2 -2 28 58.69 15.40 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-17 -3 28 26.10 19.50 17 -3 -28 29.80 16.60 -17 3 28 40.40 17.70 17 3 -28 9.20 16.60 -17 3 28 11.80 16.60 -16 -3 28 -2.20 14.90 16 -3 -28 0.20 16.10 16 -3 -28 14.80 14.70 -16 -3 28 1.90 15.80 16 -3 -28 3.90 15.40 -16 -3 28 18.30 14.80 16 3 -28 -3.90 13.70 -16 3 28 -6.90 13.30 -16 3 28 11.10 14.60 16 3 -28 -4.40 14.30 -15 -3 28 88.59 22.40 15 -3 -28 35.00 16.30 15 -3 -28 64.19 20.70 -15 -3 28 106.59 23.00 15 -3 -28 62.09 21.10 -15 -3 28 81.09 19.70 -15 3 28 77.09 18.30 15 3 -28 65.79 19.60 -15 3 28 67.89 19.40 15 3 -28 33.40 16.10 14 -3 -28 75.09 21.00 -14 -3 28 81.79 20.10 -14 -3 28 104.29 22.10 14 -3 -28 57.79 20.60 14 -3 -28 47.40 17.20 -14 -3 28 56.69 17.70 -14 3 28 59.69 17.00 14 3 -28 45.10 16.10 -14 3 28 29.10 14.10 14 3 -28 53.09 17.00 13 -3 -28 -1.90 12.90 13 -3 -28 -2.10 9.50 -13 -3 28 9.00 11.70 13 -3 -28 5.00 12.60 -13 -3 28 -12.20 10.00 -13 -3 28 -20.40 11.00 13 3 -28 -5.60 10.10 -13 3 28 -2.60 10.10 13 3 -28 -3.80 10.70 -13 3 28 -9.10 9.00 13 3 -28 8.70 13.90 12 -3 -28 28.40 13.90 -12 -3 28 26.80 13.20 -12 -3 28 17.10 12.50 12 -3 -28 40.20 17.20 12 -3 -28 48.30 15.00 -12 -3 28 28.60 13.70 -12 3 28 52.39 13.30 12 3 -28 35.00 14.00 12 3 -28 25.00 12.50 -12 3 28 47.40 15.20 12 3 -28 48.40 16.40 11 -3 -28 353.96 29.00 11 -3 -28 355.56 37.30 -11 -3 28 401.36 35.40 11 -3 -28 413.16 33.90 -11 -3 28 383.56 31.40 -11 -3 28 384.56 29.30 11 -3 -28 438.16 31.80 -11 3 28 360.46 30.30 11 3 -28 303.57 33.10 -11 3 28 341.97 27.00 11 3 -28 387.96 35.00 11 3 -28 354.86 29.90 10 -3 -28 67.69 16.40 -10 -3 28 106.49 18.90 10 -3 -28 67.99 14.90 -10 -3 28 99.79 15.50 10 -3 -28 57.29 13.00 -10 -3 28 84.59 16.60 10 -3 -28 98.89 20.20 10 3 -28 50.69 15.60 -10 3 28 65.49 14.70 -10 3 28 85.79 14.60 10 3 -28 71.99 16.40 10 3 -28 77.49 16.30 9 -3 -28 560.54 33.80 9 -3 -28 512.15 34.90 9 -3 -28 529.25 34.50 -9 -3 28 518.65 35.20 9 -3 -28 597.84 40.00 -9 -3 28 576.84 33.10 -9 -3 28 534.85 35.60 -9 3 28 547.45 32.60 9 3 -28 528.95 34.70 -9 3 28 533.95 35.30 9 3 -28 600.34 36.70 9 3 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16.20 5.70 1 3 -28 1.50 4.70 1 3 -28 3.00 7.20 1 3 -28 3.30 5.50 0 -3 -28 68.69 11.50 0 -3 28 90.69 11.50 0 -3 -28 90.09 13.40 0 -3 28 57.09 14.00 0 -3 -28 71.69 12.00 0 -3 28 76.69 10.20 0 3 -28 48.70 11.70 0 3 -28 62.29 9.00 0 3 28 62.99 9.30 0 3 -28 86.99 10.50 0 3 -28 73.09 10.30 1 -3 28 56.09 8.40 -1 -3 -28 53.49 10.50 1 -3 28 30.60 12.30 -1 -3 -28 42.60 9.80 1 -3 28 34.10 7.80 -1 -3 -28 51.99 10.40 -1 3 -28 46.60 7.70 -1 3 -28 55.59 8.60 -1 3 -28 50.29 8.90 2 -3 28 41.20 8.00 -2 -3 -28 39.30 10.80 -2 -3 -28 46.40 9.80 2 -3 28 51.19 16.10 -2 3 -28 46.00 8.30 -3 -3 -28 83.89 13.50 -3 -3 -28 77.59 12.60 3 -3 28 62.99 17.30 -3 3 -28 105.09 12.20 -4 -3 -28 -5.30 5.30 -4 -3 -28 7.20 7.40 4 -3 28 23.00 14.50 -4 3 -28 0.00 5.70 5 -3 28 183.68 29.60 -5 -3 -28 193.58 19.30 -5 -3 -28 206.78 22.60 -5 3 -28 230.18 20.50 -6 -3 -28 -2.70 6.30 -6 -3 -28 5.60 9.30 6 -3 28 -11.50 15.20 -6 3 -28 3.90 6.90 -7 -3 -28 15.30 9.70 7 -3 28 -6.40 16.70 -7 3 -28 4.70 7.60 -8 -3 -28 95.99 16.60 -9 -3 -28 2.40 10.90 -10 -3 -28 13.90 10.80 -11 -3 -28 -3.20 10.40 -12 -3 -28 31.10 15.50 -13 -3 -28 -4.50 12.40 -14 -3 -28 135.19 25.70 -15 -3 -28 2.80 15.10 -16 -3 -28 -6.80 16.70 -18 -4 28 17.70 20.80 -18 -4 28 16.10 21.30 18 -4 -28 -0.70 19.90 18 -4 -28 13.40 18.90 18 4 -28 -18.90 16.00 -18 4 28 16.50 17.10 -17 -4 28 -7.30 17.50 17 -4 -28 -3.60 18.00 17 -4 -28 -20.20 13.10 -17 -4 28 12.10 16.30 -17 -4 28 -16.00 16.60 -17 4 28 14.60 17.50 -17 4 28 0.30 14.90 17 4 -28 10.90 17.80 16 -4 -28 -1.50 17.70 -16 -4 28 13.60 17.00 -16 -4 28 -8.30 15.20 16 -4 -28 18.70 18.30 -16 -4 28 12.20 14.40 16 -4 -28 -24.00 12.40 16 4 -28 2.20 16.60 -16 4 28 -2.80 12.60 -16 4 28 24.90 16.70 16 4 -28 3.20 15.30 15 -4 -28 90.69 24.30 -15 -4 28 49.60 20.00 15 -4 -28 87.69 25.60 -15 -4 28 97.69 21.40 -15 -4 28 43.50 18.80 15 -4 -28 42.60 16.60 15 4 -28 76.69 20.60 15 4 -28 107.49 23.10 -15 4 28 84.99 19.20 -15 4 28 59.29 17.70 14 -4 -28 4.50 15.90 -14 -4 28 3.20 14.00 14 -4 -28 24.10 14.50 -14 -4 28 11.10 13.20 14 -4 -28 12.30 15.50 -14 -4 28 -14.30 11.60 -14 4 28 4.60 13.10 14 4 -28 25.50 16.10 -14 4 28 -17.00 10.60 14 4 -28 27.90 15.80 13 -4 -28 12.10 16.70 -13 -4 28 11.20 12.30 13 -4 -28 1.40 12.00 -13 -4 28 26.20 15.40 13 -4 -28 11.30 14.60 -13 -4 28 2.70 12.20 13 4 -28 5.90 12.50 13 4 -28 10.40 12.10 -13 4 28 26.70 14.70 -13 4 28 25.70 11.40 12 -4 -28 10.90 11.10 12 -4 -28 -11.30 12.00 -12 -4 28 29.50 14.80 -12 -4 28 -2.80 11.70 12 -4 -28 21.10 14.30 -12 -4 28 -1.60 11.40 12 4 -28 -1.30 9.10 -12 4 28 23.50 12.50 -12 4 28 5.90 9.10 12 4 -28 10.40 11.80 11 -4 -28 93.49 21.20 -11 -4 28 55.79 14.90 11 -4 -28 78.89 19.40 -11 -4 28 61.29 16.30 11 -4 -28 63.89 15.00 11 -4 -28 65.29 14.80 -11 -4 28 36.00 15.10 -11 4 28 55.39 15.40 -11 4 28 105.19 16.10 11 4 -28 78.49 16.80 11 4 -28 70.29 16.60 10 -4 -28 756.62 42.80 10 -4 -28 839.02 45.90 -10 -4 28 782.32 46.20 -10 -4 28 782.02 43.00 10 -4 -28 770.52 47.80 10 -4 -28 687.03 47.80 -10 -4 28 855.81 47.70 10 4 -28 883.61 49.30 -10 4 28 722.73 40.70 10 4 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37.40 9.80 6 4 -28 66.19 13.80 6 4 -28 49.40 12.00 6 4 -28 71.69 13.50 -5 -4 28 31.00 11.20 -5 -4 28 19.50 10.20 -5 -4 28 23.30 6.40 5 -4 -28 50.19 14.10 5 -4 -28 26.10 8.40 5 -4 -28 31.60 9.10 -5 -4 28 29.70 9.90 5 -4 -28 32.60 10.00 5 4 -28 26.30 10.50 5 4 -28 42.70 11.60 5 4 -28 33.60 8.20 -5 4 28 42.60 9.70 5 4 -28 6.80 8.00 4 -4 -28 873.51 41.40 -4 -4 28 881.71 42.80 -4 -4 28 897.21 44.80 4 -4 -28 828.42 44.00 4 -4 -28 870.61 42.40 -4 -4 28 853.61 38.10 4 -4 -28 889.91 47.60 -4 -4 28 853.01 47.00 4 4 -28 890.31 43.70 4 4 -28 863.81 43.50 -4 4 28 889.41 43.20 4 4 -28 857.01 45.00 4 4 -28 927.61 39.60 -3 -4 28 613.84 34.50 3 -4 -28 663.93 34.10 3 -4 -28 677.83 38.50 3 -4 -28 688.33 32.20 -3 -4 28 578.94 38.00 -3 -4 28 601.84 32.60 3 -4 -28 575.84 34.40 -3 -4 28 607.64 29.00 3 4 -28 663.33 33.60 3 4 -28 619.04 36.40 3 4 -28 635.84 34.10 3 4 -28 665.73 30.10 2 -4 -28 41.50 9.30 -2 -4 28 41.20 12.70 2 -4 -28 23.90 10.20 -2 -4 28 42.30 7.30 -2 -4 28 49.30 10.30 2 -4 -28 33.30 7.50 2 -4 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13.20 15.60 -6 -4 -28 261.67 26.50 6 -4 28 288.67 40.50 -6 -4 -28 323.57 23.10 -7 -4 -28 84.69 16.20 -7 -4 -28 108.99 15.90 7 -4 28 81.49 25.10 -8 -4 -28 184.78 23.50 8 -4 28 137.09 30.80 -9 -4 -28 185.88 24.90 -10 -4 -28 107.89 20.60 -11 -4 -28 43.80 16.40 -12 -4 -28 23.60 14.50 -13 -4 -28 257.67 32.70 -14 -4 -28 -11.60 14.80 -15 -4 -28 -12.40 16.00 -17 -5 28 9.30 19.50 -17 -5 28 36.70 21.20 17 -5 -28 -3.00 14.00 17 -5 -28 -6.50 19.10 -17 -5 28 12.40 17.10 -17 5 28 23.00 17.40 17 5 -28 -6.80 15.90 -17 5 28 11.00 15.60 -16 -5 28 -4.50 16.90 -16 -5 28 -3.60 16.70 -16 -5 28 10.00 14.30 16 -5 -28 -1.80 16.90 16 -5 -28 -19.00 13.90 16 5 -28 8.90 15.20 -16 5 28 3.70 13.70 -16 5 28 -10.90 11.70 15 -5 -28 19.80 17.00 15 -5 -28 35.80 18.10 -15 -5 28 26.60 15.90 -15 -5 28 37.00 20.60 15 -5 -28 18.50 19.40 -15 -5 28 48.50 20.00 15 5 -28 31.50 15.70 -15 5 28 15.80 13.40 -15 5 28 28.90 15.90 15 5 -28 49.20 18.50 -14 -5 28 13.10 15.00 -14 -5 28 -13.40 13.50 14 -5 -28 3.40 12.60 14 -5 -28 1.80 13.80 -14 -5 28 2.60 13.20 14 -5 -28 -0.10 17.60 -14 5 28 -26.90 11.10 -14 5 28 -16.20 9.10 14 5 -28 -14.40 12.20 14 5 -28 13.30 14.00 -13 -5 28 124.69 22.60 -13 -5 28 179.68 27.80 13 -5 -28 83.59 23.30 13 -5 -28 208.18 30.80 -13 -5 28 130.79 24.70 13 -5 -28 126.29 22.40 -13 5 28 118.39 20.00 13 5 -28 170.88 25.50 -13 5 28 149.09 23.50 13 5 -28 120.49 23.10 -12 -5 28 71.29 18.90 12 -5 -28 79.89 22.40 -12 -5 28 61.39 18.00 12 -5 -28 79.09 21.20 -12 -5 28 72.89 18.30 12 -5 -28 68.69 17.50 12 5 -28 77.89 17.80 -12 5 28 98.29 19.30 12 5 -28 75.19 18.70 -12 5 28 71.89 15.40 -11 -5 28 18.50 12.30 11 -5 -28 2.80 8.90 11 -5 -28 6.60 12.50 -11 -5 28 17.40 11.60 11 -5 -28 0.50 12.10 -11 -5 28 1.10 11.00 11 -5 -28 21.60 11.50 11 5 -28 -14.30 9.40 11 5 -28 13.60 10.80 -11 5 28 12.20 9.80 -11 5 28 31.60 10.10 -10 -5 28 135.69 20.60 10 -5 -28 105.89 16.50 -10 -5 28 122.99 22.00 -10 -5 28 117.09 19.90 10 -5 -28 70.69 17.40 10 -5 -28 77.99 16.30 -10 -5 28 149.19 20.20 10 -5 -28 157.28 25.80 -10 5 28 120.79 19.70 10 5 -28 107.39 18.70 -10 5 28 104.89 15.20 10 5 -28 95.99 19.30 9 -5 -28 383.76 26.80 9 -5 -28 354.46 37.60 9 -5 -28 326.07 27.60 -9 -5 28 358.56 29.00 9 -5 -28 362.96 30.00 -9 -5 28 315.37 31.90 -9 -5 28 330.27 25.70 -9 -5 28 319.37 30.80 9 5 -28 408.56 30.10 -9 5 28 331.17 24.50 9 5 -28 332.67 27.90 -8 -5 28 -1.00 8.90 8 -5 -28 28.10 11.10 -8 -5 28 -0.30 8.50 -8 -5 28 3.40 8.00 8 -5 -28 2.30 11.00 -8 -5 28 11.80 11.00 8 -5 -28 -5.90 6.80 8 -5 -28 6.90 9.20 8 5 -28 16.80 10.90 8 5 -28 -0.30 10.10 -8 5 28 3.90 6.90 7 -5 -28 106.49 14.40 -7 -5 28 106.39 17.30 -7 -5 28 99.79 18.10 -7 -5 28 108.29 18.50 7 -5 -28 139.89 19.00 -7 -5 28 109.39 14.20 7 -5 -28 94.79 16.90 7 -5 -28 90.29 19.70 -7 5 28 122.19 15.40 7 5 -28 86.49 16.40 7 5 -28 119.39 18.20 7 5 -28 115.59 18.50 6 -5 -28 2.20 7.40 -6 -5 28 -4.90 7.70 -6 -5 28 2.10 8.50 -6 -5 28 2.80 5.50 6 -5 -28 6.70 6.40 6 -5 -28 0.50 7.20 -6 -5 28 -13.80 6.90 6 -5 -28 -16.90 10.10 -6 5 28 -4.80 5.10 6 5 -28 -1.10 8.70 6 5 -28 -13.00 6.60 6 5 -28 -5.80 7.80 5 -5 -28 87.09 13.20 5 -5 -28 74.39 14.60 5 -5 -28 97.09 14.70 -5 -5 28 73.09 10.20 5 -5 -28 104.39 18.50 -5 -5 28 107.59 16.90 -5 -5 28 71.99 15.90 -5 -5 28 73.69 13.50 5 5 -28 83.39 14.80 -5 5 28 103.69 14.70 5 5 -28 70.89 14.10 5 5 -28 83.99 15.20 -4 -5 28 18.40 12.20 -4 -5 28 10.30 8.70 -4 -5 28 26.60 6.60 -4 -5 28 31.90 9.50 4 -5 -28 13.00 7.00 4 -5 -28 22.60 8.10 4 -5 -28 14.70 11.00 4 -5 -28 37.00 11.30 4 5 -28 13.40 9.40 -4 5 28 36.40 9.80 4 5 -28 21.20 9.40 4 5 -28 16.00 6.30 4 5 -28 28.70 10.00 -3 -5 28 158.98 22.90 -3 -5 28 140.79 16.20 3 -5 -28 160.88 17.90 3 -5 -28 217.88 22.00 -3 -5 28 165.08 19.70 -3 -5 28 175.18 12.70 3 -5 -28 184.38 17.00 3 -5 -28 195.38 23.20 3 5 -28 162.98 18.60 3 5 -28 168.58 13.20 3 5 -28 155.08 17.10 3 5 -28 163.58 20.60 2 -5 -28 488.75 30.60 2 -5 -28 418.16 27.90 2 -5 -28 462.15 32.00 -2 -5 28 516.45 36.30 -2 -5 28 523.35 23.80 -2 -5 28 501.75 27.40 -2 -5 28 483.15 29.50 2 5 -28 515.65 28.70 2 5 -28 498.85 29.10 2 5 -28 500.15 32.20 -1 -5 28 244.58 19.30 1 -5 -28 268.97 25.60 -1 -5 28 246.88 17.50 -1 -5 28 283.17 30.50 1 -5 -28 255.17 23.80 -1 -5 28 258.37 15.00 1 -5 -28 197.38 20.00 1 5 -28 266.17 18.50 1 5 -28 279.37 19.80 1 5 -28 276.37 25.90 0 -5 -28 615.44 35.80 0 -5 28 634.84 44.00 0 -5 -28 641.54 35.90 0 -5 -28 686.03 35.90 0 -5 28 665.33 30.90 0 -5 28 640.34 33.50 0 5 -28 571.74 36.40 -1 -5 -28 393.66 27.10 1 -5 28 400.96 24.50 1 -5 28 376.56 39.00 -1 -5 -28 424.36 27.20 -1 -5 -28 394.76 26.30 -2 -5 -28 82.99 14.30 -2 -5 -28 100.09 14.50 2 -5 28 80.19 12.00 2 -5 28 77.99 21.50 -3 -5 -28 0.30 7.60 3 -5 28 11.70 14.10 -3 -5 -28 0.10 7.50 -4 -5 -28 153.58 18.50 -4 -5 -28 157.08 20.20 4 -5 28 163.28 30.30 -5 -5 -28 145.59 19.90 5 -5 28 118.89 28.30 -5 -5 -28 181.58 19.70 -6 -5 -28 15.80 9.00 6 -5 28 14.80 18.90 -6 -5 -28 29.80 11.60 -7 -5 -28 54.79 13.20 7 -5 28 95.59 28.40 -7 -5 -28 50.39 15.00 -8 -5 -28 206.28 22.80 -8 -5 -28 218.48 26.10 8 -5 28 191.68 36.90 9 -5 28 170.98 35.30 -9 -5 -28 216.78 26.60 -10 -5 -28 16.70 13.50 -11 -5 -28 6.50 13.20 -12 -5 -28 200.48 28.70 -13 -5 -28 10.00 15.20 -14 -5 -28 108.19 25.90 -15 -5 -28 15.40 17.60 -17 -6 28 28.30 22.00 -17 -6 28 3.90 19.90 -17 -6 28 -12.10 15.40 17 -6 -28 31.20 22.80 17 -6 -28 29.50 16.60 -17 6 28 12.80 14.40 -17 6 28 4.60 16.00 17 6 -28 24.80 18.20 16 -6 -28 -32.90 14.30 16 -6 -28 20.90 16.60 -16 -6 28 -11.30 14.00 -16 -6 28 9.90 19.40 -16 -6 28 -21.20 16.60 16 6 -28 14.10 17.30 -16 6 28 5.20 13.30 -16 6 28 -16.30 11.80 -15 -6 28 109.39 27.70 -15 -6 28 28.60 18.10 15 -6 -28 40.30 17.10 15 -6 -28 44.80 20.50 15 -6 -28 40.70 23.00 -15 -6 28 48.60 18.60 15 6 -28 45.80 18.30 -15 6 28 79.19 20.70 -15 6 28 55.59 19.00 15 6 -28 49.99 19.20 -14 -6 28 95.89 22.10 -14 -6 28 151.68 26.90 14 -6 -28 112.29 29.30 14 -6 -28 128.69 24.10 14 -6 -28 101.79 25.90 -14 -6 28 130.59 24.90 -14 6 28 116.09 22.60 14 6 -28 41.80 17.90 14 6 -28 97.69 21.30 -14 6 28 86.79 18.70 -13 -6 28 157.28 27.70 13 -6 -28 123.69 27.00 -13 -6 28 140.69 24.10 -13 -6 28 118.89 24.50 -13 -6 28 116.39 22.40 13 -6 -28 156.88 29.20 13 -6 -28 132.39 22.70 -13 6 28 142.19 23.90 13 6 -28 108.59 22.10 -13 6 28 129.79 20.50 13 6 -28 125.19 23.90 12 -6 -28 34.60 17.20 -12 -6 28 4.80 12.80 -12 -6 28 24.90 14.00 -12 -6 28 -6.90 12.50 12 -6 -28 8.00 15.50 12 -6 -28 17.20 11.60 12 -6 -28 4.60 12.00 -12 -6 28 18.40 14.00 -12 6 28 -8.90 9.80 -12 6 28 9.60 10.00 12 6 -28 15.50 13.20 12 6 -28 12.60 13.30 -11 -6 28 50.09 17.00 -11 -6 28 75.49 19.00 -11 -6 28 57.49 17.00 -11 -6 28 38.20 14.60 11 -6 -28 63.59 17.10 11 -6 -28 67.49 15.80 11 -6 -28 42.50 13.80 11 -6 -28 39.30 17.40 11 6 -28 13.20 11.20 -11 6 28 47.30 15.50 11 6 -28 36.00 16.10 -11 6 28 42.50 12.30 -10 -6 28 257.97 28.70 -10 -6 28 255.37 26.60 -10 -6 28 232.98 29.90 10 -6 -28 240.98 25.20 -10 -6 28 259.27 29.70 10 -6 -28 244.08 26.40 10 -6 -28 265.37 33.70 10 -6 -28 255.87 30.70 -10 6 28 236.78 27.40 10 6 -28 203.18 25.80 10 6 -28 258.57 28.10 -10 6 28 190.18 21.90 -9 -6 28 21.00 11.40 -9 -6 28 17.50 11.40 9 -6 -28 -12.30 12.30 -9 -6 28 4.00 10.10 9 -6 -28 -9.50 6.40 9 -6 -28 7.70 10.00 -9 -6 28 -3.50 10.00 9 -6 -28 7.20 9.20 9 6 -28 -6.00 9.70 9 6 -28 0.50 9.00 -9 6 28 -4.60 6.50 -8 -6 28 237.38 23.10 8 -6 -28 211.78 30.60 8 -6 -28 234.68 25.60 -8 -6 28 205.18 27.30 8 -6 -28 231.28 22.90 8 -6 -28 286.07 29.50 -8 -6 28 185.48 24.50 -8 -6 28 212.88 24.30 8 6 -28 263.97 27.50 8 6 -28 247.88 25.90 -8 6 28 263.37 21.20 7 -6 -28 301.27 33.70 7 -6 -28 246.18 25.80 -7 -6 28 295.57 27.00 -7 -6 28 251.77 26.70 -7 -6 28 279.07 29.50 7 -6 -28 273.27 21.90 -7 -6 28 298.07 21.30 7 -6 -28 228.28 24.60 -7 6 28 280.87 21.60 7 6 -28 242.38 27.00 7 6 -28 234.88 25.30 6 -6 -28 116.99 16.10 -6 -6 28 170.48 16.20 6 -6 -28 148.69 19.50 -6 -6 28 137.09 21.00 6 -6 -28 144.49 18.70 6 -6 -28 139.99 23.10 -6 -6 28 160.28 20.70 -6 -6 28 152.78 18.80 6 6 -28 114.59 18.50 -6 6 28 131.99 16.50 6 6 -28 167.58 21.30 5 -6 -28 127.99 18.10 -5 -6 28 126.99 17.10 5 -6 -28 118.49 21.50 5 -6 -28 123.49 16.60 5 -6 -28 119.29 15.50 -5 -6 28 120.09 20.00 -5 -6 28 129.39 18.90 -5 -6 28 123.39 13.00 -5 6 28 120.79 15.50 5 6 -28 85.19 16.00 5 6 -28 140.29 19.40 4 -6 -28 139.79 18.30 4 -6 -28 135.09 16.40 -4 -6 28 122.09 20.50 4 -6 -28 122.69 15.60 4 -6 -28 114.29 20.50 -4 -6 28 145.59 17.20 -4 -6 28 139.19 19.10 4 6 -28 166.58 20.50 -4 6 28 117.79 15.90 4 6 -28 129.19 17.20 3 -6 -28 112.69 19.30 -3 -6 28 63.89 16.40 -3 -6 28 114.69 14.20 3 -6 -28 109.79 16.80 -3 -6 28 94.49 15.60 3 -6 -28 105.09 14.70 3 6 -28 86.59 14.70 3 6 -28 52.89 14.00 -2 -6 28 99.09 12.60 2 -6 -28 80.09 15.80 2 -6 -28 97.49 15.80 2 -6 -28 56.69 11.50 -2 -6 28 98.59 19.60 -2 -6 28 80.59 14.20 2 6 -28 72.19 15.50 2 6 -28 93.49 14.10 -1 -6 28 332.57 23.30 -1 -6 28 317.47 20.10 -1 -6 28 281.07 32.90 1 -6 -28 298.77 22.70 1 -6 -28 304.77 24.20 1 -6 -28 347.37 26.70 1 6 -28 340.07 27.20 0 -6 -28 668.43 37.00 0 -6 28 603.64 34.00 0 -6 28 580.64 44.10 0 -6 -28 635.34 36.80 0 -6 -28 584.24 34.40 1 -6 28 473.85 45.80 1 -6 28 334.37 23.30 -1 -6 -28 291.27 24.30 -1 -6 -28 357.06 25.00 -1 -6 -28 339.77 25.60 -2 -6 -28 127.99 18.30 -2 -6 -28 156.08 19.70 2 -6 28 169.08 17.50 2 -6 28 110.09 24.10 3 -6 28 596.34 49.99 -3 -6 -28 663.53 37.30 -3 -6 -28 631.24 37.30 -4 -6 -28 115.59 17.20 4 -6 28 134.19 27.40 -4 -6 -28 89.69 15.80 -5 -6 -28 53.39 12.60 -5 -6 -28 11.60 10.50 5 -6 28 75.09 25.10 -6 -6 -28 166.68 20.20 -6 -6 -28 172.48 23.00 6 -6 28 171.08 35.30 7 -6 28 5.30 19.60 -7 -6 -28 3.00 10.10 -7 -6 -28 11.50 9.30 -8 -6 -28 80.89 16.00 8 -6 28 24.30 23.60 -8 -6 -28 100.99 18.60 -9 -6 -28 38.90 16.40 9 -6 28 48.30 27.40 -9 -6 -28 85.99 18.50 -10 -6 -28 119.19 21.30 10 -6 28 145.29 36.50 -11 -6 -28 23.80 14.60 -12 -6 -28 7.40 13.50 -13 -6 -28 39.40 18.40 -14 -6 -28 47.70 19.30 -15 -6 -28 -15.60 16.00 -17 -7 28 6.20 22.30 17 -7 -28 5.10 15.50 -17 -7 28 2.30 20.40 17 -7 -28 0.90 21.20 17 7 -28 2.50 17.40 -17 7 28 20.40 18.10 -16 -7 28 122.99 28.70 -16 -7 28 86.69 23.10 -16 -7 28 49.50 23.30 16 -7 -28 104.39 29.50 16 -7 -28 32.50 16.30 -16 7 28 54.09 19.00 16 7 -28 23.80 19.10 -16 7 28 98.79 22.50 15 -7 -28 27.80 16.00 -15 -7 28 23.10 21.40 -15 -7 28 -11.30 18.00 15 -7 -28 21.80 18.20 -15 -7 28 34.20 21.50 15 -7 -28 -1.90 20.00 -15 -7 28 21.80 16.60 -15 7 28 21.20 15.80 15 7 -28 10.80 18.10 -15 7 28 29.90 15.90 15 7 -28 26.60 20.90 -14 -7 28 199.28 31.30 14 -7 -28 195.28 26.70 -14 -7 28 200.88 29.60 14 -7 -28 195.28 36.70 14 -7 -28 137.19 30.10 -14 -7 28 167.98 27.90 -14 -7 28 174.88 29.40 -14 7 28 170.18 25.60 14 7 -28 189.68 28.30 -14 7 28 158.38 25.40 14 7 -28 210.28 29.80 -13 -7 28 51.79 17.40 -13 -7 28 105.09 24.10 13 -7 -28 81.19 23.90 -13 -7 28 39.50 17.80 -13 -7 28 45.00 18.70 13 -7 -28 44.10 22.40 13 -7 -28 53.69 16.80 13 7 -28 65.49 18.30 -13 7 28 74.79 16.00 -13 7 28 71.79 18.00 13 7 -28 33.90 15.70 12 -7 -28 38.80 20.60 -12 -7 28 19.60 15.00 12 -7 -28 -5.30 13.20 -12 -7 28 17.10 15.30 12 -7 -28 26.60 13.10 -12 -7 28 10.50 12.90 12 -7 -28 10.30 13.00 -12 -7 28 15.60 14.90 -12 7 28 8.90 9.50 12 7 -28 35.40 16.30 -12 7 28 41.30 14.80 12 7 -28 20.10 13.00 11 -7 -28 7.30 13.00 -11 -7 28 30.30 14.70 -11 -7 28 12.10 12.90 11 -7 -28 28.30 12.80 11 -7 -28 5.30 14.90 -11 -7 28 25.40 13.80 -11 -7 28 15.70 12.80 11 -7 -28 32.40 13.30 11 7 -28 25.50 14.00 11 7 -28 28.30 14.20 -11 7 28 35.80 11.90 -11 7 28 13.30 11.60 10 -7 -28 13.60 11.80 -10 -7 28 23.40 13.30 -10 -7 28 -1.00 11.20 -10 -7 28 6.60 11.60 10 -7 -28 -8.90 13.90 10 -7 -28 -1.00 8.80 10 -7 -28 10.10 10.50 -10 -7 28 -0.40 10.90 -10 7 28 5.70 8.30 10 7 -28 -3.50 10.60 10 7 -28 -10.40 8.30 -9 -7 28 234.68 29.30 9 -7 -28 293.47 27.80 -9 -7 28 268.87 27.30 9 -7 -28 285.67 28.30 9 -7 -28 235.18 28.70 -9 -7 28 236.08 26.90 -9 -7 28 218.58 27.00 9 -7 -28 222.78 30.50 -9 7 28 227.38 23.00 9 7 -28 236.68 27.20 9 7 -28 266.47 28.30 -8 -7 28 56.39 17.10 8 -7 -28 81.99 16.00 8 -7 -28 64.19 13.00 8 -7 -28 73.79 20.40 8 -7 -28 65.59 16.40 -8 -7 28 88.39 18.30 -8 -7 28 71.69 15.30 -8 7 28 89.59 14.20 8 7 -28 55.69 15.20 8 7 -28 58.99 16.20 -7 -7 28 345.77 26.50 7 -7 -28 285.47 23.10 -7 -7 28 280.17 31.40 7 -7 -28 301.37 29.30 -7 -7 28 316.97 30.70 7 -7 -28 234.38 30.60 7 -7 -28 325.27 26.70 7 7 -28 347.87 28.20 7 7 -28 276.67 28.00 -7 7 28 294.37 23.40 -6 -7 28 241.18 24.00 6 -7 -28 242.58 26.10 6 -7 -28 257.17 23.40 -6 -7 28 284.27 28.80 -6 -7 28 300.57 33.70 6 -7 -28 263.47 27.00 6 -7 -28 291.77 33.30 -6 7 28 211.08 21.60 6 7 -28 205.88 24.60 6 7 -28 285.67 27.80 -5 -7 28 13.90 8.90 5 -7 -28 4.10 7.40 5 -7 -28 -8.00 10.80 -5 -7 28 4.80 10.50 5 -7 -28 -2.90 8.60 -5 -7 28 -15.60 7.00 5 -7 -28 21.70 10.10 5 7 -28 3.30 9.20 -5 7 28 2.10 6.10 5 7 -28 6.90 10.10 4 -7 -28 106.69 20.20 4 -7 -28 104.89 17.30 -4 -7 28 79.49 15.50 -4 -7 28 106.69 15.10 -4 -7 28 94.19 20.00 4 -7 -28 69.79 12.50 4 7 -28 95.79 18.10 -4 7 28 82.19 14.00 4 7 -28 94.99 15.80 -3 -7 28 4.60 11.90 3 -7 -28 48.00 14.60 3 -7 -28 24.50 8.70 -3 -7 28 20.70 8.50 -3 -7 28 21.00 10.00 3 -7 -28 22.50 11.00 3 7 -28 26.50 12.00 2 -7 -28 6.60 7.80 -2 -7 28 7.70 12.40 2 -7 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2 -9 28 191.48 22.50 -3 -9 -28 86.29 16.30 -3 -9 -28 64.99 15.10 3 -9 28 79.69 15.50 3 -9 28 60.19 25.90 -4 -9 -28 13.70 10.60 -4 -9 -28 8.00 9.20 4 -9 28 45.50 24.70 -5 -9 -28 -10.20 8.00 -5 -9 -28 -7.00 9.40 5 -9 28 12.30 21.50 6 -9 28 66.79 30.40 -6 -9 -28 98.29 18.50 -6 -9 -28 95.09 19.40 -7 -9 -28 221.38 28.40 -7 -9 -28 179.78 25.30 7 -9 28 231.48 46.50 8 -9 28 -11.10 25.00 -8 -9 -28 1.70 10.10 -8 -9 -28 26.50 14.00 -9 -9 -28 83.29 20.10 9 -9 28 82.79 36.00 -9 -9 -28 107.09 18.70 -10 -9 -28 3.40 12.40 -10 -9 -28 21.30 14.40 10 -9 28 32.80 32.00 -11 -9 -28 -1.90 12.30 11 -9 28 25.10 30.80 -11 -9 -28 -19.80 12.20 -12 -9 -28 8.20 15.60 12 -9 28 0.10 29.70 13 -9 28 -23.20 36.40 -13 -9 -28 -3.80 15.60 -15 -10 28 134.69 33.10 15 -10 -28 138.79 38.40 -15 -10 28 115.19 27.50 15 -10 -28 112.39 23.30 -15 10 28 205.58 30.40 -15 10 28 99.89 22.20 14 -10 -28 -20.30 20.00 14 -10 -28 20.70 15.20 -14 -10 28 28.50 17.10 -14 -10 28 -28.60 16.80 -14 10 28 7.10 13.90 -14 10 28 25.80 13.90 -13 -10 28 236.48 33.20 13 -10 -28 297.87 34.10 -13 -10 28 318.27 50.89 13 -10 -28 267.17 44.00 13 -10 -28 249.38 40.60 -13 -10 28 218.88 34.50 -13 10 28 269.27 32.00 -13 10 28 267.47 29.90 12 -10 -28 1.60 12.00 -12 -10 28 1.30 17.20 12 -10 -28 15.70 14.80 12 -10 -28 40.10 21.60 12 -10 -28 8.40 20.10 -12 -10 28 20.20 19.60 -12 -10 28 9.90 14.20 -12 10 28 10.40 10.30 12 10 -28 19.20 16.00 -11 -10 28 20.80 18.50 -11 -10 28 8.40 12.90 11 -10 -28 -7.40 16.70 11 -10 -28 9.60 11.80 11 -10 -28 30.50 14.00 11 -10 -28 7.00 17.50 -11 -10 28 50.19 19.60 11 10 -28 5.40 14.40 -11 10 28 47.10 13.30 -10 -10 28 62.69 20.70 10 -10 -28 57.79 21.90 10 -10 -28 58.39 14.50 -10 -10 28 61.09 17.30 10 -10 -28 65.99 22.10 10 -10 -28 35.70 15.00 -10 -10 28 31.90 17.40 -10 10 28 65.29 14.40 10 10 -28 74.79 19.00 9 -10 -28 15.10 17.00 -9 -10 28 18.20 12.10 9 -10 -28 18.70 10.80 9 -10 -28 -7.40 14.40 -9 -10 28 -1.80 13.00 -9 -10 28 5.10 14.30 9 -10 -28 30.90 14.20 -9 10 28 3.10 8.70 9 10 -28 0.10 11.80 -8 -10 28 103.39 24.30 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11.00 -4 1 53 17.70 12.70 -3 1 53 22.30 12.40 -2 1 53 43.70 14.40 -1 1 53 13.70 10.50 6 -2 -53 -10.30 14.60 6 -2 -53 21.30 14.10 -6 2 53 27.10 13.70 -6 2 53 40.20 19.20 5 -2 -53 24.30 14.30 -5 2 53 9.50 11.30 -5 2 53 25.60 16.30 4 -2 -53 -2.10 12.00 -4 2 53 12.00 11.90 3 -2 -53 -6.30 11.60 -3 2 53 10.90 10.60 2 -2 -53 -16.70 10.40 -2 2 53 -1.60 9.80 1 -2 -53 250.37 31.00 -1 2 53 155.78 25.50 0 -2 -53 4.90 13.10 0 2 53 20.00 12.20 -1 -2 -53 533.95 57.19 -6 3 53 32.40 17.00 -6 3 53 14.00 13.70 5 -3 -53 9.10 13.90 5 -3 -53 35.70 18.80 -5 3 53 12.20 14.40 -5 3 53 -14.30 11.50 4 -3 -53 -19.20 11.80 -4 3 53 -6.10 8.80 -4 3 53 -13.90 12.70 3 -3 -53 7.20 11.50 -3 3 53 5.20 11.00 2 -3 -53 8.40 12.40 -2 3 53 34.20 13.40 1 -3 -53 2.60 13.70 -1 3 53 -5.00 9.80 0 -3 -53 165.28 25.90 -1 -3 -53 26.40 16.10 -5 4 53 -12.10 9.90 4 -4 -53 5.90 13.10 4 -4 -53 -1.40 16.10 -4 4 53 0.00 12.40 -4 4 53 7.80 11.90 3 -4 -53 15.40 13.80 -3 4 53 17.40 11.10 2 -4 -53 6.40 14.10 -2 4 53 -0.10 10.70 1 -4 -53 51.89 18.00 -1 4 53 49.70 16.80 0 -4 -53 6.50 13.70 -5 1 54 131.29 21.80 -4 1 54 29.70 15.40 -3 1 54 12.70 12.00 -2 1 54 43.40 13.80 -4 2 54 9.20 11.60 3 -2 -54 37.30 17.50 -3 2 54 6.00 10.20 2 -2 -54 4.40 14.60 -2 2 54 24.90 13.20 1 -2 -54 134.19 25.10 -1 2 54 142.29 23.60 0 2 54 36.20 15.20 -3 3 54 29.20 14.30 -2 3 54 61.99 17.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 81175 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p21n_neu_a _database_code_depnum_ccdc_archive 'CCDC 2151155' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-09 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C38 Al2 Cl2 F63 O6' _chemical_formula_moiety 'C24 Al2 F55 O6, C14 Cl2 F8' _chemical_formula_weight 1874.24 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 14.514(9) _cell_length_b 10.566(6) _cell_length_c 18.161(11) _cell_angle_alpha 90 _cell_angle_beta 98.81(3) _cell_angle_gamma 90 _cell_volume 2752(3) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9931 _cell_measurement_theta_min 2.2365 _cell_measurement_theta_max 26.9895 _exptl_crystal_description block _exptl_crystal_colour blue _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.262 _exptl_crystal_F_000 1806 _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.12 _exptl_absorpt_coefficient_mu 0.414 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.7102 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 0.6 _diffrn_detector CCD _diffrn_detector_type 'Bruker APEXII' _diffrn_detector_area_resol_mean 8.3 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker APEX2 QUAZAR' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 28399 _diffrn_reflns_av_unetI/netI 0.0225 _diffrn_reflns_av_R_equivalents 0.0272 _diffrn_reflns_theta_min 1.676 _diffrn_reflns_theta_max 27.102 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_limit_l_max 23 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 6071 _reflns_number_gt 4993 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS 2018.9.0.3/05-Dec-2018 && APEX3_2019.1-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0388P)^2^+4.7880P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_number_reflns 6071 _refine_ls_number_parameters 757 _refine_ls_number_restraints 4354 _refine_ls_R_factor_all 0.0542 _refine_ls_R_factor_gt 0.0421 _refine_ls_wR_factor_ref 0.1061 _refine_ls_wR_factor_gt 0.0993 _refine_ls_goodness_of_fit_ref 1.072 _refine_ls_restrained_S_all 0.866 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 1.022 _refine_diff_density_min -0.540 _refine_diff_density_rms 0.068 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl2 Cl 0.98999(6) 0.47034(7) 0.32841(4) 0.03780(19) Uani 1 1 d . . . . . Al1 Al 0.45857(4) 0.42836(6) 0.57707(4) 0.01167(14) Uani 1 1 d . . . . . F1 F 0.500000 0.500000 0.500000 0.0144(4) Uani 1 2 d S . P A . F2 F 0.91686(11) 0.04463(14) 0.44376(10) 0.0307(4) Uani 1 1 d . . . . . F3 F 0.96013(12) 0.23119(15) 0.36283(9) 0.0319(4) Uani 1 1 d . . . . . F4 F 1.05206(10) 0.70755(15) 0.34351(8) 0.0264(3) Uani 1 1 d . . . . . F5 F 1.08763(11) 0.92643(15) 0.40833(10) 0.0307(4) Uani 1 1 d . . . . . C1 C 0.93657(17) 0.1569(2) 0.47619(15) 0.0238(5) Uani 1 1 d . . . . . C2 C 0.95917(17) 0.2572(2) 0.43408(14) 0.0221(5) Uani 1 1 d . . . . . C3 C 0.97908(16) 0.3793(2) 0.46510(13) 0.0179(5) Uani 1 1 d . . . . . C4 C 0.99881(16) 0.4859(2) 0.42246(13) 0.0197(5) Uani 1 1 d . . . . . C5 C 1.02210(16) 0.6054(2) 0.45568(13) 0.0179(5) Uani 1 1 d . . . . . C6 C 1.04650(16) 0.7119(2) 0.41533(14) 0.0208(5) Uani 1 1 d . . . . . C7 C 1.06611(17) 0.8282(2) 0.44861(15) 0.0227(5) Uani 1 1 d . . . . . O1_1 O 0.39168(11) 0.30710(15) 0.53497(9) 0.0162(3) Uani 1 1 d D U . . . C1_1 C 0.32891(16) 0.2171(2) 0.54722(13) 0.0174(5) Uani 1 1 d D U . . . C2_1 C 0.3619(2) 0.1470(3) 0.62166(17) 0.0360(7) Uani 1 1 d D U . . . F1_1 F 0.43415(14) 0.0719(2) 0.61489(17) 0.0759(8) Uani 1 1 d D U . . . F2_1 F 0.29638(12) 0.07463(18) 0.64329(11) 0.0442(5) Uani 1 1 d D U . . . F3_1 F 0.39334(16) 0.2279(3) 0.67495(10) 0.0682(8) Uani 1 1 d D U . . . C3_1 C 0.23227(19) 0.2766(3) 0.55154(19) 0.0355(7) Uani 1 1 d D U . . . F4_1 F 0.21194(13) 0.3662(2) 0.50182(16) 0.0720(8) Uani 1 1 d D U . . . F5_1 F 0.23130(15) 0.3312(2) 0.61812(14) 0.0622(7) Uani 1 1 d D U . . . F6_1 F 0.16314(11) 0.19177(16) 0.54344(11) 0.0403(4) Uani 1 1 d D U . . . C4_1 C 0.3209(2) 0.1204(3) 0.48261(18) 0.0428(8) Uani 1 1 d D U . . . F7_1 F 0.2699(2) 0.1718(3) 0.42191(11) 0.0860(10) Uani 1 1 d D U . . . F8_1 F 0.27587(14) 0.01528(17) 0.49658(12) 0.0479(5) Uani 1 1 d D U . . . F9_1 F 0.40207(18) 0.0913(2) 0.46594(17) 0.0864(10) Uani 1 1 d D U . . . O1_2 O 0.3884(7) 0.5363(7) 0.6118(4) 0.0154(15) Uani 0.810(3) 1 d D U P A 1 C1_2 C 0.3803(3) 0.6282(5) 0.6628(3) 0.0160(9) Uani 0.810(3) 1 d D U P A 1 C2_2 C 0.2855(3) 0.6958(4) 0.6379(3) 0.0277(9) Uani 0.810(3) 1 d D U P A 1 F1_2 F 0.28977(19) 0.7727(2) 0.58028(13) 0.0407(6) Uani 0.810(3) 1 d D U P A 1 F2_2 F 0.2568(5) 0.7632(5) 0.6921(4) 0.0396(11) Uani 0.810(3) 1 d D U P A 1 F3_2 F 0.21893(14) 0.6108(2) 0.61506(15) 0.0382(6) Uani 0.810(3) 1 d D U P A 1 C3_2 C 0.3804(3) 0.5671(4) 0.7406(2) 0.0229(9) Uani 0.810(3) 1 d D U P A 1 F4_2 F 0.45070(18) 0.4863(2) 0.75643(11) 0.0360(6) Uani 0.810(3) 1 d D U P A 1 F5_2 F 0.30177(18) 0.5033(2) 0.74222(12) 0.0369(6) Uani 0.810(3) 1 d D U P A 1 F6_2 F 0.3882(5) 0.6535(7) 0.7959(4) 0.0274(14) Uani 0.810(3) 1 d D U P A 1 C4_2 C 0.4601(3) 0.7265(4) 0.6658(2) 0.0237(9) Uani 0.810(3) 1 d D U P A 1 F7_2 F 0.53927(13) 0.6813(2) 0.70424(11) 0.0321(5) Uani 0.810(3) 1 d D U P A 1 F8_2 F 0.4400(5) 0.8347(7) 0.6980(4) 0.0330(13) Uani 0.810(3) 1 d D U P A 1 F9_2 F 0.47717(19) 0.7519(2) 0.59751(12) 0.0402(7) Uani 0.810(3) 1 d D U P A 1 O1_3 O 0.5536(4) 0.3879(8) 0.6399(5) 0.0170(16) Uani 0.809(4) 1 d D U P A 1 C1_3 C 0.6448(3) 0.3547(4) 0.6554(2) 0.0165(9) Uani 0.809(4) 1 d D U P A 1 C2_3 C 0.6748(2) 0.3570(3) 0.74146(16) 0.0239(7) Uani 0.809(4) 1 d D U P A 1 F1_3 F 0.6834(5) 0.4750(5) 0.7663(2) 0.0346(11) Uani 0.809(4) 1 d D U P A 1 F2_3 F 0.75638(18) 0.2981(3) 0.76168(16) 0.0349(6) Uani 0.809(4) 1 d D U P A 1 F3_3 F 0.6109(4) 0.3012(7) 0.7754(3) 0.0338(10) Uani 0.809(4) 1 d D U P A 1 C3_3 C 0.6591(2) 0.2192(3) 0.62574(18) 0.0242(7) Uani 0.809(4) 1 d D U P A 1 F4_3 F 0.6095(5) 0.2047(7) 0.5581(4) 0.0308(12) Uani 0.809(4) 1 d D U P A 1 F5_3 F 0.6307(2) 0.1312(2) 0.66951(17) 0.0334(6) Uani 0.809(4) 1 d D U P A 1 F6_3 F 0.7482(5) 0.1951(7) 0.6206(5) 0.0350(14) Uani 0.809(4) 1 d D U P A 1 C4_3 C 0.7057(2) 0.4503(3) 0.61861(17) 0.0210(7) Uani 0.809(4) 1 d D U P A 1 F7_3 F 0.6992(2) 0.4255(3) 0.54549(17) 0.0278(7) Uani 0.809(4) 1 d D U P A 1 F8_3 F 0.79545(14) 0.4466(2) 0.64782(15) 0.0316(6) Uani 0.809(4) 1 d D U P A 1 F9_3 F 0.6749(4) 0.5670(5) 0.6247(3) 0.0275(8) Uani 0.809(4) 1 d D U P A 1 O1_4 O 0.5544(15) 0.395(4) 0.639(2) 0.020(7) Uani 0.191(4) 1 d D U P A 2 C1_4 C 0.6430(11) 0.3525(13) 0.6609(7) 0.019(3) Uani 0.191(4) 1 d D U P A 2 C2_4 C 0.7058(7) 0.4669(11) 0.6887(7) 0.033(3) Uani 0.191(4) 1 d D U P A 2 F1_4 F 0.691(2) 0.505(2) 0.7554(10) 0.042(5) Uani 0.191(4) 1 d D U P A 2 F2_4 F 0.7953(6) 0.4386(13) 0.6919(9) 0.054(4) Uani 0.191(4) 1 d D U P A 2 F3_4 F 0.688(2) 0.564(2) 0.6422(12) 0.045(5) Uani 0.191(4) 1 d D U P A 2 C3_4 C 0.6783(8) 0.2888(11) 0.5934(6) 0.024(3) Uani 0.191(4) 1 d D U P A 2 F4_4 F 0.6102(19) 0.222(3) 0.5536(16) 0.033(6) Uani 0.191(4) 1 d D U P A 2 F5_4 F 0.7048(12) 0.3754(13) 0.5477(9) 0.044(4) Uani 0.191(4) 1 d D U P A 2 F6_4 F 0.7511(17) 0.213(3) 0.6122(17) 0.026(4) Uani 0.191(4) 1 d D U P A 2 C4_4 C 0.6444(8) 0.2544(12) 0.7244(6) 0.033(3) Uani 0.191(4) 1 d D U P A 2 F7_4 F 0.6094(11) 0.1437(11) 0.6985(8) 0.048(3) Uani 0.191(4) 1 d D U P A 2 F8_4 F 0.7311(8) 0.2365(14) 0.7594(7) 0.048(3) Uani 0.191(4) 1 d D U P A 2 F9_4 F 0.5939(18) 0.294(3) 0.7751(13) 0.052(7) Uani 0.191(4) 1 d D U P A 2 O1_5 O 0.392(3) 0.538(3) 0.6100(19) 0.022(8) Uani 0.190(3) 1 d D U P A 2 C1_5 C 0.3839(10) 0.6301(19) 0.6610(10) 0.022(4) Uani 0.190(3) 1 d D U P A 2 C2_5 C 0.4112(9) 0.5776(14) 0.7411(9) 0.027(4) Uani 0.190(3) 1 d D U P A 2 F1_5 F 0.5033(6) 0.5691(8) 0.7586(4) 0.031(2) Uani 0.190(3) 1 d D U P A 2 F2_5 F 0.381(2) 0.653(3) 0.7915(19) 0.037(7) Uani 0.190(3) 1 d D U P A 2 F3_5 F 0.3753(10) 0.4642(9) 0.7481(5) 0.048(4) Uani 0.190(3) 1 d D U P A 2 C3_5 C 0.2815(11) 0.6774(17) 0.6510(9) 0.039(4) Uani 0.190(3) 1 d D U P A 2 F4_5 F 0.2481(8) 0.6943(13) 0.5793(6) 0.055(4) Uani 0.190(3) 1 d D U P A 2 F5_5 F 0.2259(7) 0.5946(11) 0.6780(8) 0.057(3) Uani 0.190(3) 1 d D U P A 2 F6_5 F 0.276(2) 0.787(2) 0.6867(18) 0.044(6) Uani 0.190(3) 1 d D U P A 2 C4_5 C 0.4481(10) 0.7420(16) 0.6472(8) 0.029(4) Uani 0.190(3) 1 d D U P A 2 F7_5 F 0.4114(9) 0.8075(9) 0.5875(5) 0.044(3) Uani 0.190(3) 1 d D U P A 2 F8_5 F 0.461(2) 0.824(3) 0.7034(13) 0.030(5) Uani 0.190(3) 1 d D U P A 2 F9_5 F 0.5306(7) 0.6997(9) 0.6357(6) 0.040(3) Uani 0.190(3) 1 d D U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl2 0.0571(5) 0.0358(4) 0.0201(3) -0.0006(3) 0.0043(3) -0.0160(3) Al1 0.0108(3) 0.0120(3) 0.0124(3) 0.0002(2) 0.0025(2) -0.0002(2) F1 0.0150(9) 0.0143(9) 0.0145(8) 0.0013(7) 0.0043(7) -0.0007(7) F2 0.0290(8) 0.0150(7) 0.0489(10) -0.0050(7) 0.0084(7) -0.0029(6) F3 0.0410(10) 0.0269(8) 0.0287(8) -0.0076(7) 0.0086(7) -0.0031(7) F4 0.0278(8) 0.0273(8) 0.0251(7) 0.0081(6) 0.0066(6) 0.0023(6) F5 0.0248(8) 0.0231(8) 0.0461(10) 0.0084(7) 0.0114(7) 0.0011(6) C1 0.0150(12) 0.0168(12) 0.0393(15) 0.0000(11) 0.0036(10) 0.0008(9) C2 0.0138(11) 0.0241(13) 0.0280(13) -0.0017(10) 0.0020(9) 0.0022(10) C3 0.0106(10) 0.0178(11) 0.0246(12) 0.0009(9) 0.0009(9) 0.0011(9) C4 0.0146(11) 0.0244(13) 0.0197(11) 0.0011(10) 0.0016(9) -0.0003(9) C5 0.0106(10) 0.0199(12) 0.0230(12) 0.0030(9) 0.0017(9) 0.0031(9) C6 0.0131(11) 0.0241(13) 0.0252(12) 0.0058(10) 0.0029(9) 0.0043(9) C7 0.0138(11) 0.0188(12) 0.0361(14) 0.0075(11) 0.0059(10) 0.0029(9) O1_1 0.0158(8) 0.0148(8) 0.0183(8) -0.0007(6) 0.0038(6) -0.0042(6) C1_1 0.0148(11) 0.0146(11) 0.0233(11) 0.0011(9) 0.0045(9) -0.0034(9) C2_1 0.0300(15) 0.0393(17) 0.0372(15) 0.0181(13) 0.0000(12) -0.0127(13) F1_1 0.0303(11) 0.0630(15) 0.134(2) 0.0659(15) 0.0124(12) 0.0102(10) F2_1 0.0360(10) 0.0484(11) 0.0487(11) 0.0255(9) 0.0079(8) -0.0148(8) F3_1 0.0736(15) 0.0981(18) 0.0276(10) 0.0192(11) -0.0092(9) -0.0520(14) C3_1 0.0192(13) 0.0207(14) 0.068(2) 0.0079(13) 0.0110(13) -0.0021(10) F4_1 0.0224(9) 0.0514(13) 0.140(2) 0.0563(14) 0.0057(11) 0.0059(9) F5_1 0.0561(13) 0.0403(11) 0.1032(18) -0.0320(12) 0.0536(13) -0.0162(10) F6_1 0.0175(8) 0.0318(9) 0.0715(13) 0.0090(9) 0.0062(8) -0.0081(7) C4_1 0.060(2) 0.0330(16) 0.0409(17) -0.0189(13) 0.0254(15) -0.0287(15) F7_1 0.139(2) 0.0861(18) 0.0268(10) -0.0043(11) -0.0075(12) -0.0718(18) F8_1 0.0563(12) 0.0270(9) 0.0679(13) -0.0212(9) 0.0327(10) -0.0251(9) F9_1 0.0923(18) 0.0510(14) 0.140(2) -0.0616(15) 0.0943(18) -0.0429(13) O1_2 0.016(3) 0.018(3) 0.014(2) -0.002(2) 0.005(3) 0.003(2) C1_2 0.0170(17) 0.015(2) 0.016(2) -0.0033(16) 0.0053(16) 0.0005(16) C2_2 0.025(2) 0.025(2) 0.033(2) -0.0067(16) 0.0017(17) 0.0088(16) F1_2 0.0524(16) 0.0303(13) 0.0364(12) 0.0044(10) -0.0024(10) 0.0188(12) F2_2 0.029(2) 0.042(2) 0.0492(19) -0.0192(18) 0.0104(15) 0.0161(17) F3_2 0.0155(10) 0.0387(13) 0.0580(17) -0.0171(12) -0.0016(10) 0.0056(9) C3_2 0.030(2) 0.022(2) 0.0194(17) -0.0033(14) 0.0123(16) -0.0004(15) F4_2 0.0519(15) 0.0364(14) 0.0213(10) 0.0085(9) 0.0104(10) 0.0189(13) F5_2 0.0471(15) 0.0350(12) 0.0346(11) -0.0078(9) 0.0256(11) -0.0185(11) F6_2 0.033(2) 0.033(3) 0.019(2) -0.010(2) 0.0116(17) -0.0069(19) C4_2 0.0282(18) 0.024(2) 0.0201(19) -0.0028(15) 0.0077(14) -0.0067(15) F7_2 0.0214(10) 0.0395(12) 0.0350(12) -0.0139(9) 0.0033(8) -0.0038(8) F8_2 0.045(3) 0.0188(17) 0.0342(18) -0.0076(13) 0.0033(15) -0.0047(16) F9_2 0.0560(17) 0.0429(15) 0.0249(11) -0.0017(10) 0.0166(11) -0.0246(14) O1_3 0.013(2) 0.022(3) 0.016(3) 0.003(2) 0.000(2) 0.0040(18) C1_3 0.014(2) 0.019(2) 0.0148(17) 0.0018(14) -0.0020(15) 0.0017(16) C2_3 0.0197(15) 0.0313(18) 0.0191(14) 0.0021(13) -0.0015(11) 0.0031(13) F1_3 0.037(2) 0.040(2) 0.0249(13) -0.0116(12) -0.0026(11) -0.0012(17) F2_3 0.0246(12) 0.0497(17) 0.0266(11) 0.0083(13) -0.0080(9) 0.0111(11) F3_3 0.0318(16) 0.052(2) 0.0184(17) 0.0111(14) 0.0049(11) 0.0000(14) C3_3 0.0194(15) 0.0229(16) 0.0301(16) -0.0003(13) 0.0031(12) 0.0028(12) F4_3 0.033(2) 0.0273(17) 0.030(2) -0.0090(13) -0.0016(16) 0.0020(14) F5_3 0.0354(14) 0.0196(11) 0.0447(17) 0.0084(11) 0.0042(12) -0.0001(10) F6_3 0.0240(19) 0.031(2) 0.050(3) -0.0033(16) 0.0074(15) 0.0128(17) C4_3 0.0153(14) 0.0248(16) 0.0227(14) 0.0011(12) 0.0021(11) 0.0012(12) F7_3 0.0281(12) 0.0356(17) 0.0216(11) 0.0041(12) 0.0095(9) 0.0004(13) F8_3 0.0137(10) 0.0387(13) 0.0413(14) 0.0045(12) 0.0005(10) -0.0030(8) F9_3 0.0284(18) 0.0193(14) 0.0354(16) 0.0034(11) 0.0062(13) -0.0008(11) O1_4 0.010(8) 0.028(14) 0.021(16) -0.005(11) 0.003(8) 0.003(8) C1_4 0.010(7) 0.018(7) 0.029(7) -0.004(5) 0.008(6) 0.004(5) C2_4 0.015(5) 0.031(6) 0.052(7) -0.013(5) 0.004(5) -0.003(4) F1_4 0.028(7) 0.039(10) 0.055(8) -0.027(7) -0.004(7) -0.004(8) F2_4 0.017(4) 0.066(8) 0.077(9) -0.040(8) 0.000(5) -0.005(4) F3_4 0.040(10) 0.022(6) 0.076(12) -0.010(6) 0.021(9) -0.006(5) C3_4 0.017(5) 0.027(6) 0.029(6) -0.007(4) 0.006(4) -0.001(4) F4_4 0.024(8) 0.047(13) 0.028(9) -0.025(9) 0.006(6) -0.002(7) F5_4 0.051(7) 0.046(8) 0.041(6) 0.008(6) 0.031(5) 0.013(6) F6_4 0.015(6) 0.023(7) 0.039(9) -0.018(6) 0.005(6) 0.001(4) C4_4 0.031(6) 0.040(6) 0.028(6) 0.006(5) 0.000(5) 0.009(5) F7_4 0.062(9) 0.033(5) 0.052(9) 0.014(5) 0.015(6) 0.001(5) F8_4 0.040(6) 0.064(9) 0.034(6) 0.010(7) -0.010(5) 0.022(6) F9_4 0.066(13) 0.050(11) 0.048(10) 0.024(7) 0.034(10) 0.024(10) O1_5 0.020(16) 0.022(12) 0.022(11) -0.009(12) -0.003(12) 0.003(10) C1_5 0.028(6) 0.022(8) 0.018(8) -0.003(6) 0.005(6) 0.007(6) C2_5 0.040(6) 0.021(7) 0.022(6) -0.003(5) 0.006(6) -0.007(6) F1_5 0.042(5) 0.029(5) 0.019(4) -0.003(3) -0.003(3) 0.010(4) F2_5 0.056(15) 0.035(12) 0.023(10) -0.002(9) 0.013(10) 0.006(11) F3_5 0.092(11) 0.030(5) 0.023(5) -0.003(4) 0.016(6) -0.032(6) C3_5 0.028(7) 0.039(8) 0.049(8) -0.020(6) -0.001(6) 0.008(6) F4_5 0.044(7) 0.060(9) 0.054(6) -0.023(5) -0.015(5) 0.035(7) F5_5 0.029(5) 0.059(7) 0.088(9) -0.032(6) 0.021(6) -0.008(5) F6_5 0.040(14) 0.039(8) 0.053(9) -0.022(7) 0.007(8) 0.012(7) C4_5 0.045(7) 0.022(7) 0.021(7) -0.004(5) 0.008(6) -0.002(5) F7_5 0.084(8) 0.026(5) 0.023(4) 0.002(3) 0.005(4) 0.003(5) F8_5 0.049(14) 0.022(7) 0.023(6) -0.006(5) 0.014(7) -0.004(7) F9_5 0.043(5) 0.031(5) 0.051(7) -0.008(4) 0.023(5) -0.007(4) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl2 C4 1.701(3) . ? Al1 O1_5 1.68(3) . ? Al1 O1_4 1.69(2) . ? Al1 O1_3 1.705(5) . ? Al1 O1_2 1.712(7) . ? Al1 O1_1 1.7150(18) . ? Al1 F1 1.7752(10) . ? F2 C1 1.336(3) . ? F3 C2 1.325(3) . ? F4 C6 1.320(3) . ? F5 C7 1.335(3) . ? C1 C2 1.376(4) . ? C1 C7 1.381(4) 3_766 ? C2 C3 1.420(4) . ? C3 C4 1.420(3) . ? C3 C5 1.451(3) 3_766 ? C4 C5 1.418(4) . ? C5 C6 1.417(3) . ? C6 C7 1.380(4) . ? O1_1 C1_1 1.359(3) . ? C1_1 C4_1 1.547(4) . ? C1_1 C3_1 1.550(4) . ? C1_1 C2_1 1.552(4) . ? C2_1 F3_1 1.319(4) . ? C2_1 F2_1 1.326(3) . ? C2_1 F1_1 1.335(4) . ? C3_1 F4_1 1.310(4) . ? C3_1 F6_1 1.337(3) . ? C3_1 F5_1 1.342(4) . ? C4_1 F9_1 1.298(4) . ? C4_1 F8_1 1.332(3) . ? C4_1 F7_1 1.345(4) . ? O1_2 C1_2 1.360(4) . ? C1_2 C4_2 1.551(5) . ? C1_2 C2_2 1.554(5) . ? C1_2 C3_2 1.554(5) . ? C2_2 F2_2 1.332(6) . ? C2_2 F1_2 1.333(5) . ? C2_2 F3_2 1.338(5) . ? C3_2 F4_2 1.327(4) . ? C3_2 F5_2 1.330(4) . ? C3_2 F6_2 1.350(5) . ? C4_2 F9_2 1.328(4) . ? C4_2 F8_2 1.337(6) . ? C4_2 F7_2 1.338(5) . ? O1_3 C1_3 1.356(5) . ? C1_3 C3_3 1.554(5) . ? C1_3 C2_3 1.557(5) . ? C1_3 C4_3 1.559(5) . ? C2_3 F1_3 1.325(6) . ? C2_3 F3_3 1.328(6) . ? C2_3 F2_3 1.338(4) . ? C3_3 F5_3 1.329(4) . ? C3_3 F4_3 1.334(7) . ? C3_3 F6_3 1.335(6) . ? C4_3 F9_3 1.322(6) . ? C4_3 F8_3 1.330(4) . ? C4_3 F7_3 1.343(4) . ? O1_4 C1_4 1.362(14) . ? C1_4 C4_4 1.549(12) . ? C1_4 C2_4 1.551(12) . ? C1_4 C3_4 1.553(12) . ? C2_4 F2_4 1.325(11) . ? C2_4 F1_4 1.326(13) . ? C2_4 F3_4 1.331(13) . ? C3_4 F6_4 1.329(13) . ? C3_4 F5_4 1.332(12) . ? C3_4 F4_4 1.335(13) . ? C4_4 F9_4 1.329(13) . ? C4_4 F7_4 1.332(12) . ? C4_4 F8_4 1.333(11) . ? O1_5 C1_5 1.362(14) . ? C1_5 C4_5 1.549(13) . ? C1_5 C2_5 1.551(12) . ? C1_5 C3_5 1.552(13) . ? C2_5 F3_5 1.321(12) . ? C2_5 F1_5 1.330(12) . ? C2_5 F2_5 1.334(13) . ? C3_5 F4_5 1.331(13) . ? C3_5 F6_5 1.331(14) . ? C3_5 F5_5 1.333(13) . ? C4_5 F9_5 1.325(13) . ? C4_5 F7_5 1.327(12) . ? C4_5 F8_5 1.331(13) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1_5 Al1 O1_4 111.5(18) . . ? O1_3 Al1 O1_2 112.7(4) . . ? O1_5 Al1 O1_1 110.9(13) . . ? O1_4 Al1 O1_1 119.6(13) . . ? O1_3 Al1 O1_1 117.1(3) . . ? O1_2 Al1 O1_1 109.5(3) . . ? O1_5 Al1 F1 105.7(14) . . ? O1_4 Al1 F1 105.7(12) . . ? O1_3 Al1 F1 107.3(3) . . ? O1_2 Al1 F1 107.4(3) . . ? O1_1 Al1 F1 101.77(7) . . ? Al1 F1 Al1 180.0 3_666 . ? F2 C1 C2 119.5(2) . . ? F2 C1 C7 120.0(2) . 3_766 ? C2 C1 C7 120.5(2) . 3_766 ? F3 C2 C1 115.0(2) . . ? F3 C2 C3 123.0(2) . . ? C1 C2 C3 122.1(2) . . ? C2 C3 C4 123.4(2) . . ? C2 C3 C5 117.5(2) . 3_766 ? C4 C3 C5 119.1(2) . 3_766 ? C5 C4 C3 121.9(2) . . ? C5 C4 Cl2 119.30(19) . . ? C3 C4 Cl2 118.73(19) . . ? C6 C5 C4 123.3(2) . . ? C6 C5 C3 117.8(2) . 3_766 ? C4 C5 C3 118.9(2) . 3_766 ? F4 C6 C7 115.1(2) . . ? F4 C6 C5 122.8(2) . . ? C7 C6 C5 122.1(2) . . ? F5 C7 C6 120.2(2) . . ? F5 C7 C1 119.8(2) . 3_766 ? C6 C7 C1 120.0(2) . 3_766 ? C1_1 O1_1 Al1 142.93(15) . . ? O1_1 C1_1 C4_1 108.2(2) . . ? O1_1 C1_1 C3_1 111.1(2) . . ? C4_1 C1_1 C3_1 110.0(2) . . ? O1_1 C1_1 C2_1 110.58(19) . . ? C4_1 C1_1 C2_1 108.8(2) . . ? C3_1 C1_1 C2_1 108.1(2) . . ? F3_1 C2_1 F2_1 109.9(3) . . ? F3_1 C2_1 F1_1 105.3(3) . . ? F2_1 C2_1 F1_1 107.1(3) . . ? F3_1 C2_1 C1_1 110.8(2) . . ? F2_1 C2_1 C1_1 113.2(2) . . ? F1_1 C2_1 C1_1 110.2(3) . . ? F4_1 C3_1 F6_1 108.8(2) . . ? F4_1 C3_1 F5_1 106.1(3) . . ? F6_1 C3_1 F5_1 106.0(2) . . ? F4_1 C3_1 C1_1 111.6(2) . . ? F6_1 C3_1 C1_1 113.1(2) . . ? F5_1 C3_1 C1_1 110.8(2) . . ? F9_1 C4_1 F8_1 109.7(3) . . ? F9_1 C4_1 F7_1 108.0(3) . . ? F8_1 C4_1 F7_1 105.6(3) . . ? F9_1 C4_1 C1_1 111.6(3) . . ? F8_1 C4_1 C1_1 112.9(2) . . ? F7_1 C4_1 C1_1 108.8(3) . . ? C1_2 O1_2 Al1 147.7(7) . . ? O1_2 C1_2 C4_2 111.1(5) . . ? O1_2 C1_2 C2_2 107.2(5) . . ? C4_2 C1_2 C2_2 109.0(3) . . ? O1_2 C1_2 C3_2 109.5(4) . . ? C4_2 C1_2 C3_2 110.5(3) . . ? C2_2 C1_2 C3_2 109.5(3) . . ? F2_2 C2_2 F1_2 108.1(5) . . ? F2_2 C2_2 F3_2 107.2(4) . . ? F1_2 C2_2 F3_2 106.5(4) . . ? F2_2 C2_2 C1_2 113.2(5) . . ? F1_2 C2_2 C1_2 111.3(3) . . ? F3_2 C2_2 C1_2 110.3(3) . . ? F4_2 C3_2 F5_2 107.6(3) . . ? F4_2 C3_2 F6_2 107.4(5) . . ? F5_2 C3_2 F6_2 107.6(4) . . ? F4_2 C3_2 C1_2 111.0(3) . . ? F5_2 C3_2 C1_2 110.4(3) . . ? F6_2 C3_2 C1_2 112.6(5) . . ? F9_2 C4_2 F8_2 108.7(5) . . ? F9_2 C4_2 F7_2 107.0(3) . . ? F8_2 C4_2 F7_2 107.7(4) . . ? F9_2 C4_2 C1_2 110.3(3) . . ? F8_2 C4_2 C1_2 112.1(5) . . ? F7_2 C4_2 C1_2 110.9(3) . . ? C1_3 O1_3 Al1 150.2(7) . . ? O1_3 C1_3 C3_3 110.2(5) . . ? O1_3 C1_3 C2_3 108.6(5) . . ? C3_3 C1_3 C2_3 109.3(3) . . ? O1_3 C1_3 C4_3 110.0(5) . . ? C3_3 C1_3 C4_3 109.5(3) . . ? C2_3 C1_3 C4_3 109.2(3) . . ? F1_3 C2_3 F3_3 107.2(4) . . ? F1_3 C2_3 F2_3 108.1(4) . . ? F3_3 C2_3 F2_3 108.5(4) . . ? F1_3 C2_3 C1_3 110.7(3) . . ? F3_3 C2_3 C1_3 110.5(3) . . ? F2_3 C2_3 C1_3 111.6(3) . . ? F5_3 C3_3 F4_3 107.3(4) . . ? F5_3 C3_3 F6_3 107.4(4) . . ? F4_3 C3_3 F6_3 107.8(5) . . ? F5_3 C3_3 C1_3 111.6(3) . . ? F4_3 C3_3 C1_3 110.1(5) . . ? F6_3 C3_3 C1_3 112.5(5) . . ? F9_3 C4_3 F8_3 108.5(4) . . ? F9_3 C4_3 F7_3 107.0(3) . . ? F8_3 C4_3 F7_3 107.7(3) . . ? F9_3 C4_3 C1_3 110.4(3) . . ? F8_3 C4_3 C1_3 113.3(3) . . ? F7_3 C4_3 C1_3 109.8(3) . . ? C1_4 O1_4 Al1 155(3) . . ? O1_4 C1_4 C4_4 110.0(17) . . ? O1_4 C1_4 C2_4 108.6(18) . . ? C4_4 C1_4 C2_4 109.8(10) . . ? O1_4 C1_4 C3_4 108.9(18) . . ? C4_4 C1_4 C3_4 109.2(10) . . ? C2_4 C1_4 C3_4 110.2(10) . . ? F2_4 C2_4 F1_4 109.1(16) . . ? F2_4 C2_4 F3_4 107.2(15) . . ? F1_4 C2_4 F3_4 107.8(16) . . ? F2_4 C2_4 C1_4 111.2(10) . . ? F1_4 C2_4 C1_4 111.0(14) . . ? F3_4 C2_4 C1_4 110.5(14) . . ? F6_4 C3_4 F5_4 106.3(16) . . ? F6_4 C3_4 F4_4 108.2(17) . . ? F5_4 C3_4 F4_4 106.7(17) . . ? F6_4 C3_4 C1_4 113.9(15) . . ? F5_4 C3_4 C1_4 110.9(11) . . ? F4_4 C3_4 C1_4 110.5(15) . . ? F9_4 C4_4 F7_4 107.4(15) . . ? F9_4 C4_4 F8_4 107.2(15) . . ? F7_4 C4_4 F8_4 109.0(12) . . ? F9_4 C4_4 C1_4 111.1(15) . . ? F7_4 C4_4 C1_4 111.3(10) . . ? F8_4 C4_4 C1_4 110.7(11) . . ? C1_5 O1_5 Al1 148(3) . . ? O1_5 C1_5 C4_5 108.7(18) . . ? O1_5 C1_5 C2_5 110.2(18) . . ? C4_5 C1_5 C2_5 110.5(11) . . ? O1_5 C1_5 C3_5 109.4(18) . . ? C4_5 C1_5 C3_5 108.9(11) . . ? C2_5 C1_5 C3_5 109.1(11) . . ? F3_5 C2_5 F1_5 108.2(12) . . ? F3_5 C2_5 F2_5 107.4(18) . . ? F1_5 C2_5 F2_5 107.4(18) . . ? F3_5 C2_5 C1_5 111.5(12) . . ? F1_5 C2_5 C1_5 110.5(11) . . ? F2_5 C2_5 C1_5 111.6(18) . . ? F4_5 C3_5 F6_5 108.7(18) . . ? F4_5 C3_5 F5_5 107.4(13) . . ? F6_5 C3_5 F5_5 107.9(15) . . ? F4_5 C3_5 C1_5 110.8(12) . . ? F6_5 C3_5 C1_5 110.3(16) . . ? F5_5 C3_5 C1_5 111.6(12) . . ? F9_5 C4_5 F7_5 107.8(13) . . ? F9_5 C4_5 F8_5 108.2(16) . . ? F7_5 C4_5 F8_5 106.2(16) . . ? F9_5 C4_5 C1_5 110.4(12) . . ? F7_5 C4_5 C1_5 110.7(11) . . ? F8_5 C4_5 C1_5 113.3(17) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag F2 C1 C2 F3 -0.7(3) . . . . ? C7 C1 C2 F3 179.5(2) 3_766 . . . ? F2 C1 C2 C3 178.8(2) . . . . ? C7 C1 C2 C3 -1.0(4) 3_766 . . . ? F3 C2 C3 C4 2.2(4) . . . . ? C1 C2 C3 C4 -177.3(2) . . . . ? F3 C2 C3 C5 -178.5(2) . . . 3_766 ? C1 C2 C3 C5 2.0(3) . . . 3_766 ? C2 C3 C4 C5 -177.4(2) . . . . ? C5 C3 C4 C5 3.3(4) 3_766 . . . ? C2 C3 C4 Cl2 5.0(3) . . . . ? C5 C3 C4 Cl2 -174.30(17) 3_766 . . . ? C3 C4 C5 C6 176.9(2) . . . . ? Cl2 C4 C5 C6 -5.6(3) . . . . ? C3 C4 C5 C3 -3.3(4) . . . 3_766 ? Cl2 C4 C5 C3 174.29(17) . . . 3_766 ? C4 C5 C6 F4 -1.9(4) . . . . ? C3 C5 C6 F4 178.2(2) 3_766 . . . ? C4 C5 C6 C7 178.0(2) . . . . ? C3 C5 C6 C7 -1.9(3) 3_766 . . . ? F4 C6 C7 F5 0.8(3) . . . . ? C5 C6 C7 F5 -179.1(2) . . . . ? F4 C6 C7 C1 -179.3(2) . . . 3_766 ? C5 C6 C7 C1 0.8(4) . . . 3_766 ? O1_5 Al1 O1_1 C1_1 -58.0(15) . . . . ? O1_4 Al1 O1_1 C1_1 74.0(14) . . . . ? O1_3 Al1 O1_1 C1_1 73.3(4) . . . . ? O1_2 Al1 O1_1 C1_1 -56.7(4) . . . . ? F1 Al1 O1_1 C1_1 -170.1(2) . . . . ? Al1 O1_1 C1_1 C4_1 -165.3(2) . . . . ? Al1 O1_1 C1_1 C3_1 73.8(3) . . . . ? Al1 O1_1 C1_1 C2_1 -46.2(3) . . . . ? O1_1 C1_1 C2_1 F3_1 44.5(3) . . . . ? C4_1 C1_1 C2_1 F3_1 163.3(2) . . . . ? C3_1 C1_1 C2_1 F3_1 -77.2(3) . . . . ? O1_1 C1_1 C2_1 F2_1 168.5(2) . . . . ? C4_1 C1_1 C2_1 F2_1 -72.8(3) . . . . ? C3_1 C1_1 C2_1 F2_1 46.7(3) . . . . ? O1_1 C1_1 C2_1 F1_1 -71.7(3) . . . . ? C4_1 C1_1 C2_1 F1_1 47.1(3) . . . . ? C3_1 C1_1 C2_1 F1_1 166.6(2) . . . . ? O1_1 C1_1 C3_1 F4_1 40.0(3) . . . . ? C4_1 C1_1 C3_1 F4_1 -79.8(3) . . . . ? C2_1 C1_1 C3_1 F4_1 161.5(3) . . . . ? O1_1 C1_1 C3_1 F6_1 163.1(2) . . . . ? C4_1 C1_1 C3_1 F6_1 43.3(3) . . . . ? C2_1 C1_1 C3_1 F6_1 -75.5(3) . . . . ? O1_1 C1_1 C3_1 F5_1 -78.0(3) . . . . ? C4_1 C1_1 C3_1 F5_1 162.2(2) . . . . ? C2_1 C1_1 C3_1 F5_1 43.4(3) . . . . ? O1_1 C1_1 C4_1 F9_1 43.3(3) . . . . ? C3_1 C1_1 C4_1 F9_1 164.8(3) . . . . ? C2_1 C1_1 C4_1 F9_1 -77.0(3) . . . . ? O1_1 C1_1 C4_1 F8_1 167.3(3) . . . . ? C3_1 C1_1 C4_1 F8_1 -71.2(3) . . . . ? C2_1 C1_1 C4_1 F8_1 47.1(3) . . . . ? O1_1 C1_1 C4_1 F7_1 -75.8(3) . . . . ? C3_1 C1_1 C4_1 F7_1 45.7(3) . . . . ? C2_1 C1_1 C4_1 F7_1 163.9(2) . . . . ? O1_3 Al1 O1_2 C1_2 21.8(13) . . . . ? O1_1 Al1 O1_2 C1_2 154.1(10) . . . . ? F1 Al1 O1_2 C1_2 -96.2(11) . . . . ? Al1 O1_2 C1_2 C4_2 48.7(12) . . . . ? Al1 O1_2 C1_2 C2_2 167.8(10) . . . . ? Al1 O1_2 C1_2 C3_2 -73.6(12) . . . . ? O1_2 C1_2 C2_2 F2_2 162.7(5) . . . . ? C4_2 C1_2 C2_2 F2_2 -77.0(5) . . . . ? C3_2 C1_2 C2_2 F2_2 43.9(5) . . . . ? O1_2 C1_2 C2_2 F1_2 -75.3(5) . . . . ? C4_2 C1_2 C2_2 F1_2 45.0(5) . . . . ? C3_2 C1_2 C2_2 F1_2 166.0(4) . . . . ? O1_2 C1_2 C2_2 F3_2 42.6(5) . . . . ? C4_2 C1_2 C2_2 F3_2 163.0(4) . . . . ? C3_2 C1_2 C2_2 F3_2 -76.1(4) . . . . ? O1_2 C1_2 C3_2 F4_2 49.1(6) . . . . ? C4_2 C1_2 C3_2 F4_2 -73.6(4) . . . . ? C2_2 C1_2 C3_2 F4_2 166.4(4) . . . . ? O1_2 C1_2 C3_2 F5_2 -70.2(5) . . . . ? C4_2 C1_2 C3_2 F5_2 167.2(4) . . . . ? C2_2 C1_2 C3_2 F5_2 47.1(4) . . . . ? O1_2 C1_2 C3_2 F6_2 169.6(6) . . . . ? C4_2 C1_2 C3_2 F6_2 46.9(5) . . . . ? C2_2 C1_2 C3_2 F6_2 -73.1(5) . . . . ? O1_2 C1_2 C4_2 F9_2 40.6(6) . . . . ? C2_2 C1_2 C4_2 F9_2 -77.4(4) . . . . ? C3_2 C1_2 C4_2 F9_2 162.3(4) . . . . ? O1_2 C1_2 C4_2 F8_2 161.9(6) . . . . ? C2_2 C1_2 C4_2 F8_2 43.9(5) . . . . ? C3_2 C1_2 C4_2 F8_2 -76.4(5) . . . . ? O1_2 C1_2 C4_2 F7_2 -77.7(5) . . . . ? C2_2 C1_2 C4_2 F7_2 164.3(4) . . . . ? C3_2 C1_2 C4_2 F7_2 44.0(4) . . . . ? O1_2 Al1 O1_3 C1_3 -145.3(13) . . . . ? O1_1 Al1 O1_3 C1_3 86.3(13) . . . . ? F1 Al1 O1_3 C1_3 -27.3(14) . . . . ? Al1 O1_3 C1_3 C3_3 -69.6(14) . . . . ? Al1 O1_3 C1_3 C2_3 170.7(12) . . . . ? Al1 O1_3 C1_3 C4_3 51.2(14) . . . . ? O1_3 C1_3 C2_3 F1_3 -73.8(6) . . . . ? C3_3 C1_3 C2_3 F1_3 166.0(4) . . . . ? C4_3 C1_3 C2_3 F1_3 46.2(5) . . . . ? O1_3 C1_3 C2_3 F3_3 44.9(6) . . . . ? C3_3 C1_3 C2_3 F3_3 -75.3(5) . . . . ? C4_3 C1_3 C2_3 F3_3 164.9(4) . . . . ? O1_3 C1_3 C2_3 F2_3 165.7(5) . . . . ? C3_3 C1_3 C2_3 F2_3 45.5(4) . . . . ? C4_3 C1_3 C2_3 F2_3 -74.3(4) . . . . ? O1_3 C1_3 C3_3 F5_3 -76.6(5) . . . . ? C2_3 C1_3 C3_3 F5_3 42.6(4) . . . . ? C4_3 C1_3 C3_3 F5_3 162.3(3) . . . . ? O1_3 C1_3 C3_3 F4_3 42.4(6) . . . . ? C2_3 C1_3 C3_3 F4_3 161.7(5) . . . . ? C4_3 C1_3 C3_3 F4_3 -78.7(5) . . . . ? O1_3 C1_3 C3_3 F6_3 162.6(6) . . . . ? C2_3 C1_3 C3_3 F6_3 -78.2(5) . . . . ? C4_3 C1_3 C3_3 F6_3 41.5(5) . . . . ? O1_3 C1_3 C4_3 F9_3 40.0(6) . . . . ? C3_3 C1_3 C4_3 F9_3 161.2(3) . . . . ? C2_3 C1_3 C4_3 F9_3 -79.1(4) . . . . ? O1_3 C1_3 C4_3 F8_3 161.8(5) . . . . ? C3_3 C1_3 C4_3 F8_3 -76.9(4) . . . . ? C2_3 C1_3 C4_3 F8_3 42.7(4) . . . . ? O1_3 C1_3 C4_3 F7_3 -77.7(5) . . . . ? C3_3 C1_3 C4_3 F7_3 43.5(4) . . . . ? C2_3 C1_3 C4_3 F7_3 163.2(3) . . . . ? O1_5 Al1 O1_4 C1_4 -158(6) . . . . ? O1_1 Al1 O1_4 C1_4 71(7) . . . . ? F1 Al1 O1_4 C1_4 -43(7) . . . . ? Al1 O1_4 C1_4 C4_4 -128(6) . . . . ? Al1 O1_4 C1_4 C2_4 112(6) . . . . ? Al1 O1_4 C1_4 C3_4 -8(7) . . . . ? O1_4 C1_4 C2_4 F2_4 -163(2) . . . . ? C4_4 C1_4 C2_4 F2_4 76.3(14) . . . . ? C3_4 C1_4 C2_4 F2_4 -44.1(15) . . . . ? O1_4 C1_4 C2_4 F1_4 75(2) . . . . ? C4_4 C1_4 C2_4 F1_4 -45.4(18) . . . . ? C3_4 C1_4 C2_4 F1_4 -165.8(16) . . . . ? O1_4 C1_4 C2_4 F3_4 -45(2) . . . . ? C4_4 C1_4 C2_4 F3_4 -164.9(15) . . . . ? C3_4 C1_4 C2_4 F3_4 74.7(17) . . . . ? O1_4 C1_4 C3_4 F6_4 -162(2) . . . . ? C4_4 C1_4 C3_4 F6_4 -41.4(19) . . . . ? C2_4 C1_4 C3_4 F6_4 79.4(19) . . . . ? O1_4 C1_4 C3_4 F5_4 79(2) . . . . ? C4_4 C1_4 C3_4 F5_4 -161.2(13) . . . . ? C2_4 C1_4 C3_4 F5_4 -40.4(16) . . . . ? O1_4 C1_4 C3_4 F4_4 -39(3) . . . . ? C4_4 C1_4 C3_4 F4_4 81(2) . . . . ? C2_4 C1_4 C3_4 F4_4 -158.5(19) . . . . ? O1_4 C1_4 C4_4 F9_4 -45(2) . . . . ? C2_4 C1_4 C4_4 F9_4 74.7(18) . . . . ? C3_4 C1_4 C4_4 F9_4 -164.3(16) . . . . ? O1_4 C1_4 C4_4 F7_4 75(2) . . . . ? C2_4 C1_4 C4_4 F7_4 -165.7(12) . . . . ? C3_4 C1_4 C4_4 F7_4 -44.7(15) . . . . ? O1_4 C1_4 C4_4 F8_4 -164(2) . . . . ? C2_4 C1_4 C4_4 F8_4 -44.3(14) . . . . ? C3_4 C1_4 C4_4 F8_4 76.7(13) . . . . ? O1_4 Al1 O1_5 C1_5 16(6) . . . . ? O1_1 Al1 O1_5 C1_5 152(5) . . . . ? F1 Al1 O1_5 C1_5 -99(5) . . . . ? Al1 O1_5 C1_5 C4_5 67(5) . . . . ? Al1 O1_5 C1_5 C2_5 -55(6) . . . . ? Al1 O1_5 C1_5 C3_5 -175(5) . . . . ? O1_5 C1_5 C2_5 F3_5 -43(2) . . . . ? C4_5 C1_5 C2_5 F3_5 -163.5(14) . . . . ? C3_5 C1_5 C2_5 F3_5 76.8(16) . . . . ? O1_5 C1_5 C2_5 F1_5 77(2) . . . . ? C4_5 C1_5 C2_5 F1_5 -43.0(16) . . . . ? C3_5 C1_5 C2_5 F1_5 -162.8(13) . . . . ? O1_5 C1_5 C2_5 F2_5 -163(2) . . . . ? C4_5 C1_5 C2_5 F2_5 76(2) . . . . ? C3_5 C1_5 C2_5 F2_5 -43(2) . . . . ? O1_5 C1_5 C3_5 F4_5 -44(2) . . . . ? C4_5 C1_5 C3_5 F4_5 74.4(16) . . . . ? C2_5 C1_5 C3_5 F4_5 -164.9(15) . . . . ? O1_5 C1_5 C3_5 F6_5 -165(2) . . . . ? C4_5 C1_5 C3_5 F6_5 -46(2) . . . . ? C2_5 C1_5 C3_5 F6_5 75(2) . . . . ? O1_5 C1_5 C3_5 F5_5 75(2) . . . . ? C4_5 C1_5 C3_5 F5_5 -166.0(14) . . . . ? C2_5 C1_5 C3_5 F5_5 -45.3(17) . . . . ? O1_5 C1_5 C4_5 F9_5 -44(2) . . . . ? C2_5 C1_5 C4_5 F9_5 76.7(15) . . . . ? C3_5 C1_5 C4_5 F9_5 -163.5(14) . . . . ? O1_5 C1_5 C4_5 F7_5 75(2) . . . . ? C2_5 C1_5 C4_5 F7_5 -164.0(14) . . . . ? C3_5 C1_5 C4_5 F7_5 -44.2(16) . . . . ? O1_5 C1_5 C4_5 F8_5 -166(2) . . . . ? C2_5 C1_5 C4_5 F8_5 -45(2) . . . . ? C3_5 C1_5 C4_5 F8_5 75.0(19) . . . . ? _shelx_res_file ; TITL p21n_neu_a.res in P2(1)/n p21n_neu_a.res created by SHELXL-2018/3 at 17:26:28 on 09-Feb-2022 REM Old TITL p21n_neu in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.217, Rweak 0.012, Alpha 0.051 REM 0.868 for 326 systematic absences, Orientation as input REM Formula found by SHELXT: C40 O8 F60 Al Cl4 CELL 0.71073 14.5135 10.5663 18.1610 90.000 98.811 90.000 ZERR 2.000 0.0088 0.0056 0.0110 0.000 0.030 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C O F AL CL UNIT 76 12 126 4 4 RIGU 0.004 0.004 O1_1 C1_1 C2_1 F1_1 F2_1 F3_1 C3_1 F4_1 F5_1 F6_1 = C4_1 F7_1 F8_1 F9_1 SIMU 0.04 0.08 2 O1_1 C1_1 C2_1 F1_1 F2_1 F3_1 C3_1 F4_1 F5_1 F6_1 = C4_1 F7_1 F8_1 F9_1 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 TEMP -173.150 L.S. 10 BOND $H CONF MORE -1 LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.038800 4.788000 FVAR 0.34304 1.00269 0.81025 0.80942 CL2 5 0.989992 0.470339 0.328410 11.00000 0.05706 0.03578 = 0.02008 -0.00059 0.00432 -0.01600 AL1 4 0.458569 0.428362 0.577066 11.00000 0.01085 0.01204 = 0.01235 0.00025 0.00251 -0.00022 F1 3 0.500000 0.500000 0.500000 10.50000 0.01503 0.01432 = 0.01455 0.00133 0.00433 -0.00072 F2 3 0.916860 0.044626 0.443757 11.00000 0.02904 0.01503 = 0.04888 -0.00502 0.00835 -0.00290 F3 3 0.960127 0.231190 0.362827 11.00000 0.04103 0.02691 = 0.02866 -0.00755 0.00864 -0.00307 F4 3 1.052065 0.707545 0.343512 11.00000 0.02775 0.02731 = 0.02507 0.00808 0.00665 0.00235 F5 3 1.087629 0.926429 0.408328 11.00000 0.02479 0.02307 = 0.04614 0.00836 0.01142 0.00108 C1 1 0.936569 0.156928 0.476192 11.00000 0.01497 0.01684 = 0.03933 -0.00003 0.00358 0.00082 C2 1 0.959166 0.257218 0.434079 11.00000 0.01379 0.02409 = 0.02796 -0.00169 0.00203 0.00223 C3 1 0.979083 0.379310 0.465097 11.00000 0.01065 0.01782 = 0.02456 0.00090 0.00087 0.00112 C4 1 0.998809 0.485851 0.422456 11.00000 0.01459 0.02437 = 0.01970 0.00113 0.00160 -0.00031 C5 1 1.022100 0.605405 0.455676 11.00000 0.01059 0.01990 = 0.02302 0.00297 0.00167 0.00314 C6 1 1.046504 0.711876 0.415327 11.00000 0.01306 0.02414 = 0.02520 0.00584 0.00288 0.00427 C7 1 1.066105 0.828158 0.448608 11.00000 0.01376 0.01880 = 0.03611 0.00753 0.00590 0.00287 RESI CCF3 1 PART 0 11 O1 2 0.391680 0.307102 0.534968 11.00000 0.01584 0.01476 = 0.01829 -0.00070 0.00379 -0.00419 C1 1 0.328907 0.217114 0.547217 11.00000 0.01481 0.01464 = 0.02327 0.00108 0.00450 -0.00344 C2 1 0.361911 0.147022 0.621664 11.00000 0.03003 0.03929 = 0.03719 0.01807 -0.00005 -0.01266 F1 3 0.434150 0.071936 0.614894 11.00000 0.03026 0.06298 = 0.13430 0.06586 0.01235 0.01022 F2 3 0.296375 0.074626 0.643286 11.00000 0.03602 0.04838 = 0.04868 0.02549 0.00789 -0.01480 F3 3 0.393336 0.227936 0.674947 11.00000 0.07364 0.09809 = 0.02761 0.01917 -0.00920 -0.05202 C3 1 0.232273 0.276583 0.551545 11.00000 0.01916 0.02066 = 0.06808 0.00791 0.01101 -0.00215 F4 3 0.211936 0.366162 0.501824 11.00000 0.02237 0.05136 = 0.14021 0.05632 0.00567 0.00586 F5 3 0.231295 0.331215 0.618120 11.00000 0.05613 0.04032 = 0.10321 -0.03197 0.05358 -0.01617 F6 3 0.163139 0.191768 0.543439 11.00000 0.01747 0.03180 = 0.07149 0.00903 0.00616 -0.00812 C4 1 0.320883 0.120350 0.482608 11.00000 0.05992 0.03303 = 0.04091 -0.01890 0.02544 -0.02866 F7 3 0.269949 0.171828 0.421906 11.00000 0.13890 0.08605 = 0.02676 -0.00435 -0.00750 -0.07177 F8 3 0.275865 0.015283 0.496578 11.00000 0.05626 0.02696 = 0.06786 -0.02124 0.03272 -0.02506 F9 3 0.402072 0.091253 0.465936 11.00000 0.09231 0.05099 = 0.13999 -0.06157 0.09430 -0.04285 PART 0 RESI 0 RESI CCF3 2 PART 1 31 O1 2 0.388436 0.536277 0.611776 31.00000 0.01564 0.01782 = 0.01353 -0.00151 0.00475 0.00318 C1 1 0.380271 0.628227 0.662756 31.00000 0.01696 0.01542 = 0.01647 -0.00333 0.00530 0.00045 C2 1 0.285547 0.695815 0.637890 31.00000 0.02478 0.02475 = 0.03266 -0.00670 0.00174 0.00876 F1 3 0.289767 0.772680 0.580281 31.00000 0.05239 0.03034 = 0.03642 0.00443 -0.00239 0.01878 F2 3 0.256847 0.763213 0.692081 31.00000 0.02896 0.04202 = 0.04919 -0.01917 0.01036 0.01605 F3 3 0.218934 0.610833 0.615055 31.00000 0.01554 0.03875 = 0.05796 -0.01712 -0.00155 0.00561 C3 1 0.380398 0.567098 0.740627 31.00000 0.02988 0.02201 = 0.01936 -0.00330 0.01235 -0.00043 F4 3 0.450695 0.486331 0.756428 31.00000 0.05188 0.03639 = 0.02126 0.00847 0.01042 0.01890 F5 3 0.301767 0.503297 0.742222 31.00000 0.04709 0.03500 = 0.03458 -0.00776 0.02556 -0.01849 F6 3 0.388245 0.653540 0.795939 31.00000 0.03297 0.03318 = 0.01852 -0.00997 0.01155 -0.00689 C4 1 0.460113 0.726506 0.665762 31.00000 0.02822 0.02399 = 0.02011 -0.00281 0.00773 -0.00667 F7 3 0.539273 0.681310 0.704239 31.00000 0.02144 0.03947 = 0.03502 -0.01385 0.00327 -0.00376 F8 3 0.440049 0.834706 0.698012 31.00000 0.04522 0.01876 = 0.03422 -0.00757 0.00334 -0.00466 F9 3 0.477165 0.751879 0.597509 31.00000 0.05597 0.04288 = 0.02493 -0.00173 0.01663 -0.02461 PART 0 RESI 0 RESI CCF3 3 PART 1 41 O1 2 0.553615 0.387897 0.639892 41.00000 0.01310 0.02154 = 0.01557 0.00304 0.00007 0.00402 C1 1 0.644758 0.354661 0.655383 41.00000 0.01440 0.01897 = 0.01485 0.00178 -0.00196 0.00173 C2 1 0.674834 0.357033 0.741456 41.00000 0.01975 0.03132 = 0.01909 0.00214 -0.00152 0.00311 F1 3 0.683434 0.474994 0.766294 41.00000 0.03704 0.03950 = 0.02494 -0.01155 -0.00258 -0.00117 F2 3 0.756376 0.298096 0.761685 41.00000 0.02459 0.04969 = 0.02659 0.00829 -0.00796 0.01114 F3 3 0.610947 0.301161 0.775380 41.00000 0.03182 0.05168 = 0.01836 0.01111 0.00493 -0.00002 C3 1 0.659076 0.219221 0.625743 41.00000 0.01941 0.02293 = 0.03014 -0.00029 0.00311 0.00285 F4 3 0.609521 0.204717 0.558090 41.00000 0.03254 0.02733 = 0.03046 -0.00897 -0.00163 0.00199 F5 3 0.630742 0.131185 0.669511 41.00000 0.03542 0.01964 = 0.04467 0.00839 0.00415 -0.00012 F6 3 0.748158 0.195076 0.620602 41.00000 0.02397 0.03129 = 0.05018 -0.00330 0.00739 0.01285 C4 1 0.705662 0.450329 0.618605 41.00000 0.01533 0.02477 = 0.02266 0.00113 0.00208 0.00118 F7 3 0.699209 0.425483 0.545492 41.00000 0.02808 0.03561 = 0.02157 0.00406 0.00945 0.00042 F8 3 0.795450 0.446633 0.647817 41.00000 0.01368 0.03866 = 0.04127 0.00451 0.00045 -0.00303 F9 3 0.674888 0.567029 0.624720 41.00000 0.02835 0.01928 = 0.03542 0.00341 0.00616 -0.00085 PART 0 RESI 0 RESI CCF3 4 PART 2 -41 O1 2 0.554421 0.395018 0.639119 -41.00000 0.00954 0.02787 = 0.02150 -0.00533 0.00288 0.00289 C1 1 0.642989 0.352523 0.660922 -41.00000 0.01046 0.01792 = 0.02883 -0.00408 0.00758 0.00429 C2 1 0.705837 0.466933 0.688684 -41.00000 0.01506 0.03056 = 0.05228 -0.01335 0.00435 -0.00271 F1 3 0.690591 0.504553 0.755402 -41.00000 0.02786 0.03876 = 0.05525 -0.02697 -0.00427 -0.00447 F2 3 0.795296 0.438587 0.691911 -41.00000 0.01653 0.06571 = 0.07712 -0.03993 -0.00028 -0.00453 F3 3 0.688151 0.564298 0.642192 -41.00000 0.03999 0.02188 = 0.07578 -0.00995 0.02128 -0.00584 C3 1 0.678307 0.288814 0.593412 -41.00000 0.01744 0.02703 = 0.02932 -0.00668 0.00611 -0.00092 F4 3 0.610176 0.221770 0.553597 -41.00000 0.02419 0.04721 = 0.02797 -0.02484 0.00648 -0.00159 F5 3 0.704805 0.375418 0.547680 -41.00000 0.05124 0.04600 = 0.04147 0.00829 0.03136 0.01279 F6 3 0.751129 0.212943 0.612207 -41.00000 0.01481 0.02336 = 0.03911 -0.01793 0.00529 0.00077 C4 1 0.644445 0.254409 0.724447 -41.00000 0.03092 0.04009 = 0.02798 0.00633 0.00013 0.00945 F7 3 0.609429 0.143717 0.698531 -41.00000 0.06178 0.03259 = 0.05201 0.01391 0.01460 0.00109 F8 3 0.731077 0.236538 0.759437 -41.00000 0.04004 0.06423 = 0.03372 0.01033 -0.01034 0.02229 F9 3 0.593856 0.293814 0.775119 -41.00000 0.06590 0.04973 = 0.04771 0.02356 0.03440 0.02368 PART 0 RESI 0 RESI CCF3 5 PART 2 -31 O1 2 0.391976 0.537803 0.610015 -31.00000 0.02019 0.02237 = 0.02232 -0.00872 -0.00343 0.00274 C1 1 0.383877 0.630118 0.660992 -31.00000 0.02766 0.02173 = 0.01809 -0.00261 0.00547 0.00655 C2 1 0.411154 0.577620 0.741126 -31.00000 0.03965 0.02084 = 0.02162 -0.00320 0.00647 -0.00687 F1 3 0.503330 0.569130 0.758564 -31.00000 0.04204 0.02915 = 0.01950 -0.00269 -0.00347 0.01002 F2 3 0.381097 0.652681 0.791520 -31.00000 0.05641 0.03509 = 0.02258 -0.00195 0.01347 0.00569 F3 3 0.375277 0.464174 0.748095 -31.00000 0.09216 0.03022 = 0.02340 -0.00332 0.01642 -0.03241 C3 1 0.281464 0.677410 0.651048 -31.00000 0.02817 0.03932 = 0.04867 -0.02023 -0.00058 0.00806 F4 3 0.248139 0.694327 0.579297 -31.00000 0.04386 0.05951 = 0.05409 -0.02326 -0.01548 0.03504 F5 3 0.225856 0.594626 0.678039 -31.00000 0.02855 0.05944 = 0.08759 -0.03198 0.02108 -0.00767 F6 3 0.276238 0.786685 0.686675 -31.00000 0.04039 0.03940 = 0.05251 -0.02232 0.00731 0.01214 C4 1 0.448050 0.741981 0.647248 -31.00000 0.04480 0.02160 = 0.02102 -0.00408 0.00774 -0.00173 F7 3 0.411398 0.807458 0.587514 -31.00000 0.08371 0.02560 = 0.02290 0.00169 0.00506 0.00300 F8 3 0.461433 0.824195 0.703426 -31.00000 0.04870 0.02189 = 0.02299 -0.00557 0.01381 -0.00363 F9 3 0.530599 0.699686 0.635721 -31.00000 0.04320 0.03137 = 0.05087 -0.00790 0.02319 -0.00725 PART 0 RESI 0 PART 0 RESI 0 PART 0 RESI 0 HKLF 4 REM p21n_neu_a.res in P2(1)/n REM wR2 = 0.1061, GooF = S = 1.072, Restrained GooF = 0.866 for all data REM R1 = 0.0421 for 4993 Fo > 4sig(Fo) and 0.0542 for all 6071 data REM 757 parameters refined using 4354 restraints END WGHT 0.0388 4.7881 REM Highest difference peak 1.022, deepest hole -0.540, 1-sigma level 0.068 Q1 1 0.2017 0.2782 0.4464 11.00000 0.05 1.02 Q2 1 0.3036 0.2553 0.6664 11.00000 0.05 0.87 Q3 1 0.3541 0.1525 0.4272 11.00000 0.05 0.84 Q4 1 0.4141 0.0357 0.5274 11.00000 0.05 0.81 Q5 1 0.4225 0.1622 0.6483 11.00000 0.05 0.74 Q6 1 0.2205 0.3725 0.5604 11.00000 0.05 0.62 Q7 1 1.0550 0.4621 0.3437 11.00000 0.05 0.53 Q8 1 0.3394 0.1778 0.5781 11.00000 0.05 0.33 Q9 1 0.3246 0.1665 0.5208 11.00000 0.05 0.33 Q10 1 0.3356 0.6546 0.6547 11.00000 0.05 0.33 Q11 1 0.3543 0.8042 0.5982 11.00000 0.05 0.31 Q12 1 1.0418 0.6575 0.4375 11.00000 0.05 0.29 Q13 1 1.0174 0.6186 0.4930 11.00000 0.05 0.28 Q14 1 0.6558 0.3476 0.6979 11.00000 0.05 0.28 Q15 1 0.9765 0.3210 0.4486 11.00000 0.05 0.28 Q16 1 0.3830 0.5989 0.6972 11.00000 0.05 0.28 Q17 1 0.6508 0.2874 0.6482 11.00000 0.05 0.28 Q18 1 0.4248 0.6683 0.6645 11.00000 0.05 0.27 Q19 1 1.0694 0.7648 0.4380 11.00000 0.05 0.27 Q20 1 0.1701 0.2032 0.4994 11.00000 0.05 0.26 ; _shelx_res_checksum 93924 _shelx_hkl_file ; 1 0 0 0.20 0.30 -1 0 0 0.20 0.20 1 0 0 -0.20 0.20 -1 0 0 0.50 0.30 2 0 0 0.80 0.40 -2 0 0 -0.50 0.40 -2 0 0 0.90 0.50 2 0 0 0.60 0.50 2 0 0 1.70 0.60 -3 0 0 0.00 0.70 3 0 0 -1.00 0.60 -4 0 0 3024.20 32.20 4 0 0 3066.49 33.00 5 0 0 -0.90 0.90 -5 0 0 1.90 0.90 5 0 0 0.60 0.60 -6 0 0 1451.25 18.10 6 0 0 1428.16 18.90 -7 0 0 0.30 1.20 7 0 0 0.30 1.40 -8 0 0 68.39 3.50 8 0 0 68.79 4.00 -9 0 0 3.10 1.60 9 0 0 -2.40 1.40 10 0 0 39.40 4.00 -10 0 0 47.40 3.50 -11 0 0 10.40 2.40 11 0 0 8.00 2.50 12 0 0 558.34 13.70 -12 0 0 549.35 11.70 13 0 0 15.00 3.60 -13 0 0 14.20 2.80 -14 0 0 140.99 6.60 14 0 0 143.89 8.30 15 0 0 -4.70 2.50 16 0 0 2.40 3.20 17 0 0 2.50 3.50 18 0 0 104.39 9.60 0 -1 0 -0.40 0.40 0 -1 0 0.00 0.30 0 -1 0 0.70 0.40 0 1 0 0.30 0.40 0 1 0 0.30 0.40 0 1 0 0.10 0.30 1 -1 0 746.13 9.00 -1 -1 0 747.13 8.90 -1 -1 0 751.22 8.30 -1 -1 0 737.13 8.50 1 -1 0 739.83 8.70 1 -1 0 746.03 8.60 -1 1 0 742.03 8.60 1 1 0 746.23 8.80 1 1 0 743.03 8.50 1 1 0 759.92 8.30 -1 1 0 722.33 8.70 2 -1 0 96.49 2.50 -2 -1 0 96.89 2.60 2 -1 0 96.39 2.50 -2 -1 0 93.19 2.40 2 1 0 94.19 2.90 -2 1 0 97.39 2.50 -2 1 0 98.59 2.50 2 1 0 101.39 2.40 3 -1 0 615.94 8.50 -3 -1 0 612.54 8.90 3 -1 0 639.04 7.30 3 -1 0 647.54 8.90 -3 1 0 622.64 7.20 3 1 0 648.84 8.60 -3 1 0 621.14 8.50 -4 -1 0 3782.52 40.30 4 -1 0 3777.12 40.30 4 -1 0 3746.73 39.30 4 -1 0 3808.82 38.20 -4 1 0 3730.93 38.10 4 1 0 3742.53 40.00 -5 -1 0 1980.70 23.70 5 -1 0 1974.80 23.90 5 -1 0 1986.20 22.60 5 1 0 2036.30 23.70 -5 1 0 1989.90 21.80 -6 -1 0 1250.97 16.90 6 -1 0 1234.08 17.20 6 -1 0 1246.18 15.50 -6 1 0 1205.38 15.00 6 1 0 1248.18 17.00 7 -1 0 1.30 1.50 7 -1 0 1.70 1.10 -7 -1 0 0.70 1.40 -7 1 0 1.20 1.10 7 1 0 1.70 1.50 8 -1 0 416.66 9.60 -8 -1 0 437.16 9.30 8 -1 0 433.86 7.60 8 1 0 440.36 9.60 -8 1 0 439.16 7.90 -9 -1 0 1061.09 16.70 9 -1 0 1029.40 14.10 9 -1 0 1019.20 17.30 9 1 0 1029.20 17.20 -9 1 0 1035.30 14.70 10 -1 0 132.59 6.10 -10 -1 0 128.79 5.50 10 -1 0 126.19 4.00 -10 1 0 134.09 4.70 10 1 0 128.99 5.90 11 -1 0 93.29 4.50 11 -1 0 88.39 5.70 -11 -1 0 97.39 5.20 11 1 0 84.39 5.40 -11 1 0 92.49 4.30 -12 -1 0 12.20 3.00 12 -1 0 13.30 3.30 -12 1 0 12.40 2.40 12 1 0 13.70 3.20 -13 -1 0 477.55 11.90 13 -1 0 469.35 13.40 13 1 0 497.75 13.40 -13 1 0 467.45 10.40 -14 -1 0 12.80 3.10 14 -1 0 16.90 3.90 14 1 0 9.50 3.40 -15 -1 0 53.49 5.30 15 -1 0 44.50 5.90 15 1 0 47.30 6.20 16 -1 0 2.30 3.30 16 1 0 1.30 3.20 17 -1 0 8.90 4.00 17 1 0 4.00 3.80 18 -1 0 4.60 4.10 18 1 0 -1.00 3.70 0 -2 0 1591.74 17.50 0 -2 0 1610.74 18.40 0 -2 0 1591.54 17.70 0 2 0 1583.24 17.70 0 2 0 1626.34 17.50 1 -2 0 2660.03 27.70 1 -2 0 2773.62 29.80 1 -2 0 2742.83 27.70 -1 -2 0 2734.63 29.00 -1 -2 0 2702.53 29.10 1 2 0 2802.52 29.00 -1 2 0 2723.13 27.60 1 2 0 2734.43 28.70 -1 2 0 2703.83 28.80 2 -2 0 411.76 7.10 2 -2 0 419.96 6.80 -2 -2 0 418.86 6.90 -2 -2 0 413.86 6.10 2 2 0 415.06 5.90 -2 2 0 415.36 6.50 2 2 0 410.06 6.40 -3 -2 0 181.98 3.40 3 -2 0 181.38 4.60 -3 -2 0 179.08 4.50 3 -2 0 185.78 4.50 3 2 0 182.48 3.20 3 2 0 187.28 4.20 -3 2 0 184.98 4.30 -4 -2 0 12.20 1.70 4 -2 0 12.50 1.80 4 -2 0 13.30 1.70 4 2 0 14.80 1.70 5 -2 0 570.74 10.00 -5 -2 0 577.74 10.20 5 -2 0 574.64 7.00 5 -2 0 591.54 9.70 -5 2 0 571.94 6.90 5 2 0 576.74 9.50 -6 -2 0 1502.15 20.60 6 -2 0 1562.14 19.90 6 -2 0 1546.85 17.00 6 -2 0 1502.85 20.60 -6 2 0 1523.45 16.80 6 2 0 1546.65 20.10 -7 -2 0 39.50 3.40 7 -2 0 34.80 3.40 7 -2 0 39.30 3.10 -7 2 0 43.70 2.00 7 2 0 37.40 3.20 8 -2 0 598.34 10.60 -8 -2 0 613.14 12.00 -8 2 0 605.84 8.90 8 2 0 582.14 11.50 9 -2 0 14.70 2.20 -9 -2 0 13.80 2.60 9 -2 0 11.90 2.60 9 2 0 10.60 2.30 -9 2 0 14.60 1.70 10 -2 0 2147.69 26.50 -10 -2 0 2098.19 29.10 10 -2 0 2056.79 29.70 -10 2 0 2086.59 24.70 10 2 0 2041.10 28.90 -11 -2 0 199.08 7.50 11 -2 0 188.08 7.80 11 -2 0 192.38 5.90 -11 2 0 183.38 5.30 11 2 0 192.18 7.60 12 -2 0 1.60 2.50 -12 -2 0 4.10 2.50 12 2 0 6.50 2.80 -12 2 0 4.20 2.50 13 -2 0 2.30 2.70 -13 -2 0 1.70 2.50 13 2 0 4.30 2.70 14 -2 0 351.66 12.30 -14 -2 0 357.56 11.20 14 2 0 372.36 12.10 15 -2 0 11.90 4.00 -15 -2 0 14.90 3.70 15 2 0 16.00 4.10 16 -2 0 26.20 5.30 -16 -2 0 13.90 3.60 16 2 0 25.30 4.90 17 -2 0 11.60 4.40 17 2 0 4.80 4.10 18 -2 0 27.50 6.00 18 2 0 22.20 5.70 0 -3 0 -0.90 0.60 0 -3 0 0.30 1.00 0 3 0 0.60 0.90 1 -3 0 84.69 2.50 -1 -3 0 88.59 3.20 -1 -3 0 91.79 3.10 1 -3 0 90.09 2.50 1 -3 0 92.99 3.50 -1 3 0 92.69 3.10 -1 3 0 90.69 2.50 1 3 0 87.69 2.90 2 -3 0 783.72 9.30 2 -3 0 813.62 12.30 2 -3 0 789.22 9.20 -2 -3 0 795.02 11.10 -2 -3 0 798.12 11.70 2 3 0 791.92 11.00 -2 3 0 792.92 11.20 -3 -3 0 879.21 11.70 3 -3 0 880.71 13.50 -3 -3 0 892.31 13.20 3 -3 0 898.31 12.90 -3 3 0 899.51 12.60 3 3 0 869.11 12.20 4 -3 0 38.10 3.00 -4 -3 0 49.30 3.10 -4 -3 0 43.90 2.20 4 -3 0 42.00 2.90 -4 3 0 41.60 2.80 4 3 0 34.20 2.50 -5 -3 0 170.68 5.70 5 -3 0 179.18 5.60 5 -3 0 173.98 5.60 -5 3 0 175.08 5.30 5 3 0 178.18 5.20 6 -3 0 887.41 14.30 6 -3 0 874.41 14.50 -6 -3 0 862.91 14.60 6 3 0 870.41 13.70 -6 3 0 868.01 14.10 -7 -3 0 794.02 14.30 7 -3 0 808.52 13.80 7 -3 0 785.12 14.10 7 3 0 788.12 13.30 8 -3 0 136.09 6.00 8 -3 0 147.59 5.50 -8 -3 0 154.88 6.20 8 3 0 144.49 5.60 -9 -3 0 7.70 2.40 9 -3 0 8.10 2.40 9 -3 0 13.60 2.40 9 3 0 9.80 2.30 -9 3 0 11.10 1.30 10 -3 0 0.30 1.50 -10 -3 0 2.20 2.10 10 -3 0 6.40 2.50 -10 3 0 1.60 1.00 10 3 0 3.50 2.10 11 -3 0 71.59 5.60 -11 -3 0 76.09 5.50 11 -3 0 67.09 4.40 11 3 0 72.49 5.20 12 -3 0 13.20 2.90 12 -3 0 13.80 3.40 -12 -3 0 13.90 3.30 12 3 0 8.90 2.90 -13 -3 0 4.20 3.00 13 -3 0 4.70 3.10 13 3 0 3.60 2.70 -14 -3 0 343.27 11.50 14 -3 0 352.46 12.60 14 3 0 323.87 11.40 -15 -3 0 16.30 4.00 15 -3 0 10.10 3.90 15 3 0 12.70 3.70 -16 -3 0 44.60 5.80 16 -3 0 44.30 6.50 16 3 0 36.80 5.70 17 -3 0 1.00 3.70 -17 -3 0 4.10 3.60 17 3 0 8.70 4.50 0 -4 0 1166.38 16.90 0 -4 0 1178.88 15.30 0 4 0 1207.28 15.70 -1 -4 0 942.71 14.20 -1 -4 0 962.00 13.60 1 -4 0 977.80 12.40 1 -4 0 949.51 14.80 1 4 0 943.21 13.30 -1 4 0 956.00 13.50 -2 -4 0 128.59 4.40 2 -4 0 124.49 4.90 2 -4 0 125.19 3.10 -2 -4 0 123.99 4.40 2 4 0 128.59 4.10 -2 4 0 139.79 4.40 3 -4 0 427.26 5.80 -3 -4 0 419.76 8.70 3 -4 0 421.96 9.30 3 -4 0 411.56 5.70 -3 -4 0 417.56 8.00 3 4 0 425.16 8.00 -3 4 0 417.56 8.20 -4 -4 0 1744.93 21.10 -4 -4 0 1695.43 23.10 4 -4 0 1698.73 23.60 -4 4 0 1728.63 22.30 4 4 0 1712.43 21.80 5 -4 0 658.33 12.60 5 -4 0 648.14 12.00 -5 -4 0 624.94 12.10 -5 -4 0 662.33 10.10 -5 4 0 639.34 11.60 5 4 0 629.44 11.10 -6 -4 0 38.20 3.60 -6 -4 0 41.60 2.40 6 -4 0 45.40 3.60 6 -4 0 38.60 3.80 -6 4 0 44.20 3.80 6 4 0 42.70 3.30 7 -4 0 79.29 4.70 -7 -4 0 103.49 5.30 7 -4 0 102.29 5.10 7 4 0 93.89 4.50 -7 4 0 99.39 4.90 8 -4 0 60.49 4.30 8 -4 0 66.59 4.60 -8 -4 0 70.09 4.70 -8 4 0 58.29 4.20 8 4 0 67.69 4.20 9 -4 0 78.09 4.90 -9 -4 0 75.49 5.30 9 -4 0 82.59 5.40 9 4 0 79.49 4.80 -9 4 0 76.19 5.00 10 -4 0 17.00 3.40 10 -4 0 11.50 2.70 -10 -4 0 7.10 2.90 10 4 0 11.00 2.70 -10 4 0 11.10 2.90 11 -4 0 354.86 9.90 -11 -4 0 343.97 11.00 11 -4 0 375.06 11.50 -11 4 0 360.66 10.90 11 4 0 376.26 10.70 -12 -4 0 115.89 6.90 12 -4 0 109.99 5.90 12 -4 0 112.39 7.20 -12 4 0 107.89 6.80 12 4 0 106.69 6.50 13 -4 0 100.39 7.50 -13 -4 0 111.29 7.30 -13 4 0 101.69 7.00 13 4 0 101.29 6.80 -14 -4 0 88.49 7.20 14 -4 0 95.49 7.60 14 4 0 85.49 6.90 -14 4 0 88.39 7.00 15 -4 0 13.30 4.00 -15 -4 0 10.60 4.00 15 4 0 12.20 3.90 -15 4 0 7.10 3.70 16 -4 0 2.00 3.50 -16 -4 0 5.50 3.30 16 4 0 2.30 3.00 -16 4 0 2.80 3.10 -17 -4 0 82.99 7.90 17 -4 0 87.49 9.00 -17 4 0 76.59 8.10 17 4 0 69.99 7.70 0 -5 0 0.40 1.20 0 -5 0 3.50 1.70 0 5 0 2.30 1.50 1 -5 0 10.60 2.40 1 -5 0 11.50 1.60 -1 -5 0 12.80 2.40 -1 -5 0 15.00 2.10 1 5 0 13.40 2.10 -1 5 0 15.90 2.30 -2 -5 0 1669.53 22.30 2 -5 0 1653.93 23.60 2 -5 0 1658.13 19.50 -2 -5 0 1657.53 22.50 2 5 0 1659.63 21.50 -2 5 0 1654.53 21.80 -3 -5 0 209.68 6.50 -3 -5 0 205.38 6.10 3 -5 0 208.58 4.20 3 -5 0 202.28 7.00 3 5 0 214.68 6.00 -3 5 0 212.08 6.20 -4 -5 0 423.56 8.70 4 -5 0 414.06 10.20 -4 -5 0 417.66 9.70 4 5 0 421.76 8.80 -4 5 0 423.26 9.20 -5 -5 0 -0.30 1.70 -5 -5 0 2.50 1.30 5 -5 0 2.10 1.90 5 5 0 3.40 1.60 -5 5 0 3.20 1.80 -6 -5 0 117.59 4.20 -6 -5 0 109.59 5.40 6 -5 0 124.19 5.90 6 5 0 105.49 4.80 -6 5 0 126.49 5.40 7 -5 0 36.90 3.90 7 -5 0 44.70 4.60 -7 -5 0 34.20 3.80 -7 -5 0 37.00 2.70 7 5 0 35.40 3.50 -7 5 0 43.70 4.00 8 -5 0 4.70 2.30 -8 -5 0 2.30 2.30 8 -5 0 15.70 3.00 -8 5 0 4.90 2.40 8 5 0 7.90 2.20 9 -5 0 21.20 3.50 9 -5 0 22.40 3.70 -9 -5 0 17.60 3.40 9 5 0 17.40 3.00 -9 5 0 17.40 3.30 -10 -5 0 22.00 3.80 10 -5 0 19.50 3.80 10 -5 0 20.40 3.60 -10 5 0 20.30 3.60 10 5 0 18.20 3.50 11 -5 0 53.89 5.20 -11 -5 0 50.29 5.60 11 -5 0 41.70 5.20 11 5 0 51.89 5.20 -11 5 0 40.60 4.90 12 -5 0 0.10 2.80 -12 -5 0 1.10 2.70 12 -5 0 -2.60 1.80 12 5 0 1.70 2.50 -12 5 0 0.60 2.60 -13 -5 0 22.50 4.60 13 -5 0 12.00 3.80 13 5 0 36.70 5.00 -13 5 0 18.40 3.90 14 -5 0 10.60 4.00 -14 -5 0 7.30 3.60 14 5 0 6.10 3.40 -14 5 0 5.90 3.60 -15 -5 0 27.10 5.00 15 -5 0 14.30 4.40 -15 5 0 19.50 4.60 15 5 0 20.40 4.50 -16 -5 0 13.40 4.30 16 -5 0 18.80 5.00 -16 5 0 11.90 4.30 16 5 0 16.50 4.50 17 -5 0 47.70 7.30 -17 -5 0 36.20 5.90 -17 5 0 25.30 5.60 17 5 0 41.70 6.60 0 -6 0 10.20 1.80 0 -6 0 11.00 2.40 0 6 0 6.90 1.80 -1 -6 0 1.90 1.50 -1 -6 0 -0.60 1.50 1 -6 0 1.40 1.20 1 -6 0 -1.20 1.60 1 6 0 2.20 1.60 -1 6 0 0.10 1.50 -2 -6 0 58.49 4.10 2 -6 0 72.39 4.80 2 -6 0 65.69 3.00 -2 -6 0 71.89 4.10 -2 6 0 67.69 4.00 2 6 0 63.59 3.80 -3 -6 0 279.47 8.00 3 -6 0 279.27 5.60 -3 -6 0 279.67 7.80 3 -6 0 288.47 8.90 -3 6 0 279.87 7.70 3 6 0 282.57 7.40 -4 -6 0 16.30 2.70 4 -6 0 14.80 2.90 -4 -6 0 12.20 2.40 4 -6 0 16.20 1.40 4 6 0 14.40 2.50 -4 6 0 22.00 3.00 -5 -6 0 49.40 4.60 5 -6 0 54.09 5.10 -5 -6 0 62.69 3.80 5 6 0 56.09 3.90 -5 6 0 58.49 4.10 -6 -6 0 18.90 2.50 6 -6 0 17.50 3.30 -6 -6 0 21.00 3.30 -6 6 0 20.80 3.10 6 6 0 24.90 3.10 7 -6 0 17.10 3.50 -7 -6 0 19.30 3.50 -7 -6 0 11.70 2.20 -7 6 0 14.90 2.90 7 6 0 17.60 3.00 -8 -6 0 213.28 8.50 -8 -6 0 208.68 5.90 8 -6 0 194.48 8.20 -8 6 0 201.18 7.90 8 6 0 194.28 7.20 9 -6 0 78.09 5.80 9 -6 0 87.79 6.10 -9 -6 0 73.19 6.10 -9 6 0 85.99 6.00 9 6 0 81.59 5.40 10 -6 0 3.70 2.60 10 -6 0 5.80 2.70 -10 -6 0 0.90 2.50 10 6 0 2.90 2.50 -10 6 0 -0.70 2.60 -11 -6 0 3.60 2.90 11 -6 0 2.00 2.70 11 -6 0 -2.00 2.50 11 6 0 4.80 2.70 -11 6 0 1.20 2.60 12 -6 0 55.69 5.70 12 -6 0 79.29 7.60 -12 -6 0 58.59 6.20 -12 6 0 63.09 6.40 12 6 0 66.09 6.10 13 -6 0 45.20 5.40 13 -6 0 49.00 6.60 -13 -6 0 40.10 5.70 -13 6 0 39.60 5.50 13 6 0 37.00 5.10 14 -6 0 92.29 9.00 -14 -6 0 77.99 7.70 -14 6 0 80.39 7.50 14 6 0 81.09 7.30 -15 -6 0 4.40 3.80 15 -6 0 8.30 4.20 -15 6 0 9.10 4.00 15 6 0 1.90 2.80 16 -6 0 58.69 7.60 -16 -6 0 67.79 7.30 16 6 0 70.29 7.80 -16 6 0 52.29 7.40 0 -7 0 6.40 2.30 0 -7 0 3.00 1.50 0 7 0 4.50 1.80 -1 -7 0 51.79 3.70 1 -7 0 43.50 4.40 1 -7 0 51.79 3.30 -1 -7 0 51.79 4.60 -1 7 0 50.89 3.90 1 7 0 56.09 3.90 2 -7 0 4.60 1.40 -2 -7 0 5.30 2.00 -2 -7 0 4.60 2.20 2 -7 0 4.90 2.30 2 7 0 6.50 2.10 -2 7 0 5.30 2.10 3 -7 0 54.89 5.20 -3 -7 0 46.60 4.20 -3 -7 0 48.50 4.30 3 -7 0 46.30 2.70 -3 7 0 50.09 4.00 3 7 0 53.49 3.90 4 -7 0 148.89 7.30 4 -7 0 162.48 4.10 -4 -7 0 172.68 6.70 -4 -7 0 169.18 6.90 -4 7 0 162.18 6.50 4 7 0 164.88 6.30 -5 -7 0 28.00 3.50 -5 -7 0 29.00 3.80 5 -7 0 30.10 4.40 -5 7 0 25.00 3.60 5 7 0 27.80 3.40 6 -7 0 85.79 6.10 -6 -7 0 81.89 5.70 -6 -7 0 86.89 4.90 -6 7 0 94.99 5.50 6 7 0 77.19 4.90 7 -7 0 27.10 4.30 -7 -7 0 33.90 3.60 -7 -7 0 47.80 5.30 -7 7 0 34.40 4.20 7 7 0 37.90 4.30 8 -7 0 -0.20 2.30 -8 -7 0 2.30 2.50 -8 -7 0 0.70 1.80 8 7 0 1.20 2.20 -8 7 0 1.00 2.30 -9 -7 0 30.30 4.70 9 -7 0 31.80 4.80 9 7 0 30.60 4.30 -9 7 0 26.40 4.20 10 -7 0 5.70 2.90 -10 -7 0 6.90 3.20 -10 7 0 5.60 2.90 10 7 0 5.80 2.60 11 -7 0 10.30 3.30 -11 -7 0 6.60 3.20 11 7 0 10.10 3.00 -11 7 0 11.40 3.60 12 -7 0 57.29 6.20 12 -7 0 66.99 7.00 -12 -7 0 67.79 6.80 12 7 0 61.09 6.20 -12 7 0 53.79 6.20 -13 -7 0 14.10 4.40 13 -7 0 10.30 4.00 13 -7 0 13.00 3.50 -13 7 0 9.30 3.60 13 7 0 8.90 3.30 -14 -7 0 10.10 4.00 14 -7 0 7.90 4.20 14 7 0 1.80 3.00 -14 7 0 0.90 3.10 -15 -7 0 11.70 4.30 15 -7 0 28.50 5.50 -15 7 0 13.40 4.60 15 7 0 13.70 4.50 0 -8 0 338.97 10.60 0 -8 0 317.17 8.50 0 8 0 292.07 8.70 -1 -8 0 42.50 4.00 -1 -8 0 47.90 5.10 1 -8 0 46.20 3.90 1 -8 0 43.70 4.90 1 8 0 47.70 4.30 -1 8 0 41.40 4.10 -2 -8 0 0.50 1.80 -2 -8 0 1.80 2.10 2 -8 0 -0.60 1.50 2 -8 0 0.20 2.30 -2 8 0 9.30 2.50 2 8 0 0.60 1.90 3 -8 0 218.38 9.20 3 -8 0 235.18 6.00 -3 -8 0 238.28 8.30 -3 -8 0 238.68 8.60 -3 8 0 231.78 8.10 3 8 0 213.98 7.50 -4 -8 0 80.09 5.40 -4 -8 0 83.69 5.70 4 -8 0 69.29 6.70 4 8 0 70.29 4.90 -4 8 0 88.09 5.50 -5 -8 0 164.48 7.10 5 -8 0 147.19 8.00 -5 -8 0 158.58 7.50 -5 8 0 154.78 7.20 5 8 0 159.38 6.80 -6 -8 0 346.57 11.20 6 -8 0 349.87 12.00 -6 -8 0 339.27 9.80 -6 8 0 348.87 10.60 6 8 0 349.96 10.00 -7 -8 0 58.09 4.70 -7 -8 0 57.19 5.80 7 -8 0 57.69 6.20 -7 8 0 60.69 5.70 7 8 0 55.99 5.00 -8 -8 0 148.29 8.20 8 -8 0 146.49 8.30 8 8 0 140.79 6.90 -8 8 0 143.59 7.60 -9 -8 0 64.39 6.50 9 -8 0 85.89 6.90 9 8 0 69.79 5.50 -9 8 0 75.79 6.70 10 -8 0 2.50 2.90 -10 -8 0 2.20 3.20 -10 8 0 5.10 3.10 10 8 0 1.10 2.60 -11 -8 0 113.29 8.10 11 -8 0 100.79 7.70 11 8 0 112.89 7.00 -11 8 0 111.19 7.70 -12 -8 0 19.90 4.50 12 -8 0 11.00 3.80 12 8 0 18.50 3.90 -12 8 0 25.40 4.80 -13 -8 0 52.29 6.80 13 -8 0 56.09 6.80 -13 8 0 51.19 6.60 13 8 0 53.99 6.20 -14 -8 0 41.10 6.60 -14 8 0 51.29 6.70 14 8 0 54.99 6.60 0 -9 0 -3.10 2.10 0 -9 0 -0.90 1.90 0 9 0 4.00 2.40 1 -9 0 285.37 8.30 1 -9 0 279.07 10.70 -1 -9 0 285.77 9.00 -1 -9 0 303.47 10.70 -1 9 0 283.57 9.30 1 9 0 285.37 9.10 2 -9 0 198.38 9.20 2 -9 0 181.18 6.20 -2 -9 0 179.98 7.60 -2 -9 0 193.98 8.60 -2 9 0 183.18 7.60 2 9 0 184.68 7.50 -3 -9 0 117.99 6.90 -3 -9 0 119.29 6.70 3 -9 0 96.89 7.10 -3 9 0 110.09 6.40 3 9 0 107.89 6.00 -4 -9 0 29.60 4.50 -4 -9 0 35.80 4.60 4 -9 0 31.20 4.80 -4 9 0 25.60 4.10 4 9 0 30.80 4.00 5 -9 0 8.90 3.40 -5 -9 0 6.00 2.90 -5 -9 0 8.10 3.00 5 9 0 12.00 3.00 -5 9 0 6.40 2.80 -6 -9 0 16.60 3.50 -6 -9 0 15.60 3.70 6 -9 0 16.50 4.40 -6 9 0 13.20 3.50 6 9 0 13.40 3.20 7 -9 0 7.10 3.40 -7 -9 0 4.80 2.90 -7 -9 0 15.00 3.30 7 9 0 8.60 3.00 -7 9 0 1.00 2.90 -8 -9 0 3.70 3.10 8 -9 0 1.50 3.10 -8 9 0 3.50 3.10 8 9 0 2.70 2.90 -9 -9 0 9.00 3.70 9 -9 0 8.10 3.60 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2.60 -9 -4 -9 156.18 8.10 -9 -4 -9 146.39 5.90 9 -4 9 148.19 7.30 9 4 9 165.88 6.90 -9 4 -9 139.39 7.70 10 -4 9 134.19 8.30 -10 -4 -9 134.09 7.80 10 -4 9 133.39 7.20 10 4 9 133.19 6.80 -10 4 -9 127.89 8.00 11 -4 9 41.20 5.00 -11 -4 -9 51.59 6.00 11 -4 9 45.10 5.90 11 4 9 40.90 4.90 -11 4 -9 45.80 5.90 12 -4 9 83.79 6.10 -12 -4 -9 68.79 7.00 12 -4 9 74.49 7.90 -12 4 -9 64.89 6.90 12 4 9 71.39 6.50 -13 -4 -9 -1.30 3.10 13 -4 9 4.10 3.60 -13 4 -9 6.40 3.70 13 4 9 2.30 3.00 14 -4 9 104.69 9.80 -14 -4 -9 102.19 8.20 -14 4 -9 115.79 8.70 14 4 9 109.29 7.80 -16 -5 9 10.10 4.30 16 -5 -9 11.60 4.20 16 5 -9 7.90 4.20 -15 -5 9 -1.70 3.10 15 -5 -9 5.00 3.40 15 5 -9 -3.30 2.80 14 -5 -9 41.70 5.30 -14 -5 9 38.50 5.80 14 5 -9 33.60 5.30 -13 -5 9 90.99 8.10 13 -5 -9 82.39 6.30 13 5 -9 75.59 7.00 12 -5 -9 46.80 4.90 -12 -5 9 62.99 6.50 12 -5 -9 60.69 5.80 12 5 -9 59.79 6.20 11 -5 -9 3.80 2.30 11 -5 -9 4.60 2.50 -11 -5 9 3.30 3.00 -11 5 9 1.90 2.00 11 5 -9 0.50 2.80 10 -5 -9 13.60 3.30 -10 -5 9 14.40 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-1 -3 22 21.00 5.90 1 3 -22 29.40 5.60 -1 3 22 16.80 5.00 0 -3 22 2.90 4.20 0 -3 -22 2.80 4.00 0 -3 22 8.60 4.50 0 3 -22 8.70 4.40 0 3 22 5.90 3.80 -1 -3 -22 4.90 4.40 1 -3 22 8.00 4.60 1 -3 22 9.50 4.30 -1 3 -22 2.10 3.60 1 3 22 1.00 4.40 5 -4 -22 48.30 7.40 -5 -4 22 49.00 6.80 -5 -4 22 40.10 6.90 -5 4 22 53.49 7.70 5 4 -22 49.90 6.60 -4 -4 22 -3.50 3.40 -4 -4 22 -0.70 3.60 4 -4 -22 0.80 4.00 -4 4 22 3.10 4.40 4 4 -22 -3.50 4.00 -3 -4 22 26.20 5.50 -3 -4 22 29.00 6.10 3 -4 -22 29.40 6.00 -3 4 22 27.00 6.10 3 4 -22 28.90 5.60 2 -4 -22 5.40 3.70 -2 -4 22 15.60 5.50 -2 -4 22 6.10 4.70 -2 4 22 0.10 4.40 2 4 -22 5.40 4.20 -1 -4 22 103.89 9.70 -1 -4 22 84.99 8.80 1 -4 -22 105.89 9.70 -1 4 22 92.69 9.60 1 4 -22 77.19 7.50 -5 0 23 4.00 4.70 5 0 -23 9.00 4.20 -4 0 23 5.40 4.80 4 0 -23 2.20 3.80 3 0 -23 57.89 7.20 -3 0 23 68.49 8.60 2 0 -23 -1.40 3.80 -2 0 23 -3.80 4.00 -1 0 23 3.40 4.10 1 0 -23 0.30 4.10 0 0 -23 2.50 3.60 0 0 23 2.60 4.30 -5 -1 23 33.10 7.10 5 -1 -23 51.19 6.70 -5 1 23 46.50 7.50 5 1 -23 36.10 5.70 4 -1 -23 258.87 11.90 -4 -1 23 279.97 13.60 4 1 -23 264.97 11.50 -4 1 23 261.67 13.60 3 -1 -23 16.00 5.00 -3 -1 23 6.00 4.80 3 1 -23 11.00 4.20 -3 1 23 12.40 4.80 -2 -1 23 204.98 12.00 2 -1 -23 188.58 10.30 -2 1 23 181.28 12.20 2 1 -23 176.18 10.10 -1 -1 23 18.00 5.40 1 -1 -23 8.10 4.70 -1 1 23 23.60 6.20 1 1 -23 27.50 5.40 -3 -2 23 -1.20 4.20 3 -2 -23 -1.60 4.20 -3 2 23 -0.40 4.50 3 2 -23 -1.20 3.70 -2 -2 23 6.70 4.70 2 -2 -23 7.10 4.80 2 2 -23 4.70 3.90 -2 2 23 23.40 5.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 24141 _chemical_properties_physical Moisture-sensitive ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p-1_a_CCDC2 _database_code_depnum_ccdc_archive 'CCDC 2151836' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-14 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C68 H2 Al4 F114 O26 Os3' _chemical_formula_moiety '2(C24 Al2 F55 O6), C14 O14 Os3, C6 H2 F4' _chemical_formula_weight 4079.22 _chemical_melting_point ? _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.810(4) _cell_length_b 12.939(2) _cell_length_c 19.507(5) _cell_angle_alpha 102.689(9) _cell_angle_beta 103.941(14) _cell_angle_gamma 92.667(9) _cell_volume 2806.9(13) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9171 _cell_measurement_theta_min 2.1715 _cell_measurement_theta_max 29.506 _exptl_crystal_description block _exptl_crystal_colour white _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.413 _exptl_crystal_F_000 1924 _exptl_crystal_size_max 0.103 _exptl_crystal_size_mid 0.080 _exptl_crystal_size_min 0.071 _exptl_absorpt_coefficient_mu 3.677 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.7042 _exptl_absorpt_correction_T_max 0.7463 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min 0.703 _shelx_estimated_absorpt_T_max 0.780 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 86130 _diffrn_reflns_av_unetI/netI 0.0590 _diffrn_reflns_av_R_equivalents 0.0673 _diffrn_reflns_theta_min 1.622 _diffrn_reflns_theta_max 32.091 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_limit_l_max 28 _diffrn_measured_fraction_theta_max 0.976 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.976 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.976 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 19196 _reflns_number_gt 14185 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0434P)^2^+6.9523P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_number_reflns 19196 _refine_ls_number_parameters 1142 _refine_ls_number_restraints 8318 _refine_ls_R_factor_all 0.0672 _refine_ls_R_factor_gt 0.0415 _refine_ls_wR_factor_ref 0.1020 _refine_ls_wR_factor_gt 0.0901 _refine_ls_goodness_of_fit_ref 1.003 _refine_ls_restrained_S_all 0.919 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 2.002 _refine_diff_density_min -2.129 _refine_diff_density_rms 0.177 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Os1 Os 0.04961(2) 0.58252(2) 0.65669(2) 0.01601(4) Uani 1 1 d . . . . . Os2 Os 0.000000 0.500000 0.500000 0.01458(5) Uani 1 2 d S . P . . Al1 Al 0.59105(11) 0.30458(10) 0.78386(6) 0.0168(2) Uani 1 1 d . . . . . Al2 Al 0.66638(11) 0.04984(9) 0.80380(6) 0.0166(2) Uani 1 1 d . . . . . F1 F 0.6239(2) 0.17591(19) 0.79368(13) 0.0206(5) Uani 1 1 d . . . . . O2 O -0.0074(3) 0.3518(3) 0.67127(18) 0.0287(7) Uani 1 1 d . . . . . C1 C 0.0857(4) 0.6443(3) 0.7632(2) 0.0181(7) Uani 1 1 d . . . . . C2 C 0.0126(4) 0.4349(3) 0.6659(2) 0.0202(8) Uani 1 1 d . . . . . O1 O 0.1069(3) 0.6788(3) 0.82246(17) 0.0295(7) Uani 1 1 d . . . . . O3 O 0.3034(3) 0.5302(3) 0.65470(17) 0.0255(6) Uani 1 1 d . . . . . O4 O 0.0964(3) 0.8015(2) 0.62236(18) 0.0257(6) Uani 1 1 d . . . . . O5 O -0.2164(3) 0.6137(3) 0.62427(18) 0.0283(7) Uani 1 1 d . . . . . O6 O -0.2307(3) 0.3759(3) 0.49838(18) 0.0283(7) Uani 1 1 d . . . . . O7 O 0.1382(3) 0.3076(3) 0.52173(19) 0.0287(7) Uani 1 1 d . . . . . C3 C 0.2131(4) 0.5507(3) 0.6575(2) 0.0198(8) Uani 1 1 d . . . . . C4 C 0.0812(4) 0.7226(3) 0.6359(2) 0.0198(8) Uani 1 1 d . . . . . C5 C -0.1208(4) 0.6029(3) 0.6376(2) 0.0209(8) Uani 1 1 d . . . . . C6 C -0.1456(3) 0.4197(3) 0.4997(2) 0.0178(7) Uani 1 1 d . . . . . C7 C 0.0873(3) 0.3779(3) 0.5147(2) 0.0179(7) Uani 1 1 d . . . . . O1_1 O 0.5476(3) -0.0368(3) 0.75331(17) 0.0305(7) Uani 1 1 d D U . . . C1_1 C 0.4667(4) -0.1174(3) 0.7487(2) 0.0224(8) Uani 1 1 d D U . . . C2_1 C 0.5110(4) -0.1840(4) 0.8051(3) 0.0337(10) Uani 1 1 d D U . . . F1_1 F 0.5019(3) -0.1357(3) 0.87066(16) 0.0392(7) Uani 1 1 d D U . . . F2_1 F 0.4481(3) -0.2800(2) 0.78583(19) 0.0517(9) Uani 1 1 d D U . . . F3_1 F 0.6222(3) -0.1985(3) 0.80965(19) 0.0460(8) Uani 1 1 d D U . . . C3_1 C 0.4390(4) -0.1893(3) 0.6702(2) 0.0285(9) Uani 1 1 d D U . . . F4_1 F 0.4311(3) -0.1314(2) 0.62118(15) 0.0366(7) Uani 1 1 d D U . . . F5_1 F 0.5239(3) -0.2517(3) 0.66333(18) 0.0455(8) Uani 1 1 d D U . . . F6_1 F 0.3379(2) -0.2518(2) 0.65248(16) 0.0338(6) Uani 1 1 d D U . . . C4_1 C 0.3527(4) -0.0704(4) 0.7623(2) 0.0305(9) Uani 1 1 d D U . . . F7_1 F 0.2964(3) -0.0352(2) 0.70510(16) 0.0384(7) Uani 1 1 d D U . . . F8_1 F 0.2777(3) -0.1427(3) 0.77194(18) 0.0419(7) Uani 1 1 d D U . . . F9_1 F 0.3780(3) 0.0110(3) 0.81981(17) 0.0465(8) Uani 1 1 d D U . . . O1_2 O 0.6919(3) 0.0454(2) 0.89246(15) 0.0230(6) Uani 1 1 d D U . . . C1_2 C 0.7430(4) 0.0956(3) 0.9632(2) 0.0221(8) Uani 1 1 d D U . . . C2_2 C 0.8639(4) 0.1551(4) 0.9699(2) 0.0264(9) Uani 1 1 d D U . . . F1_2 F 0.9455(2) 0.0882(3) 0.96627(17) 0.0386(7) Uani 1 1 d D U . . . F2_2 F 0.9011(3) 0.2307(3) 1.03094(15) 0.0397(7) Uani 1 1 d D U . . . F3_2 F 0.8552(3) 0.2015(2) 0.91394(15) 0.0345(6) Uani 1 1 d D U . . . C3_2 C 0.6613(4) 0.1771(4) 0.9902(2) 0.0331(10) Uani 1 1 d D U . . . F4_2 F 0.5510(3) 0.1328(3) 0.96988(19) 0.0471(9) Uani 1 1 d D U . . . F5_2 F 0.6652(3) 0.2612(3) 0.96203(19) 0.0465(8) Uani 1 1 d D U . . . F6_2 F 0.6906(3) 0.2115(3) 1.06239(16) 0.0511(9) Uani 1 1 d D U . . . C4_2 C 0.7601(4) 0.0114(4) 1.0093(3) 0.0367(11) Uani 1 1 d D U . . . F7_2 F 0.6584(3) -0.0217(3) 1.01937(18) 0.0517(9) Uani 1 1 d D U . . . F8_2 F 0.8342(3) 0.0511(3) 1.07448(18) 0.0550(10) Uani 1 1 d D U . . . F9_2 F 0.8015(3) -0.0733(3) 0.9756(2) 0.0508(9) Uani 1 1 d D U . . . O1_3 O 0.7817(3) 0.0414(2) 0.76457(16) 0.0215(6) Uani 1 1 d D U . . . C1_3 C 0.8595(4) -0.0150(3) 0.7357(2) 0.0228(8) Uani 1 1 d D U . . . C2_3 C 0.9740(4) 0.0604(4) 0.7508(3) 0.0289(9) Uani 1 1 d D U . . . F1_3 F 1.0333(3) 0.0770(3) 0.82064(17) 0.0439(8) Uani 1 1 d D U . . . F2_3 F 1.0455(3) 0.0194(3) 0.71102(18) 0.0421(8) Uani 1 1 d D U . . . F3_3 F 0.9497(3) 0.1539(2) 0.7381(2) 0.0432(8) Uani 1 1 d D U . . . C3_3 C 0.8074(4) -0.0582(4) 0.6521(2) 0.0291(9) Uani 1 1 d D U . . . F4_3 F 0.6976(3) -0.0976(3) 0.63718(16) 0.0416(8) Uani 1 1 d D U . . . F5_3 F 0.8126(3) 0.0201(3) 0.61786(16) 0.0425(8) Uani 1 1 d D U . . . F6_3 F 0.8684(3) -0.1333(3) 0.62330(16) 0.0419(8) Uani 1 1 d D U . . . C4_3 C 0.8896(4) -0.1103(4) 0.7711(2) 0.0293(9) Uani 1 1 d D U . . . F7_3 F 0.8040(3) -0.1917(2) 0.74135(19) 0.0462(8) Uani 1 1 d D U . . . F8_3 F 0.9870(3) -0.1501(3) 0.75891(19) 0.0469(8) Uani 1 1 d D U . . . F9_3 F 0.8996(3) -0.0855(3) 0.84133(16) 0.0431(8) Uani 1 1 d D U . . . O1_5 O 0.4895(3) 0.3366(3) 0.83162(17) 0.0283(7) Uani 1 1 d D U . . . C1_5 C 0.3770(4) 0.3512(3) 0.8311(2) 0.0208(7) Uani 1 1 d D U . . . C2_5 C 0.3608(5) 0.4713(4) 0.8373(3) 0.0363(11) Uani 1 1 d D U . . . F1_5 F 0.4049(3) 0.5287(2) 0.90493(17) 0.0496(9) Uani 1 1 d D U . . . F2_5 F 0.2485(3) 0.4877(3) 0.8164(2) 0.0586(11) Uani 1 1 d D U . . . F3_5 F 0.4167(4) 0.5086(3) 0.79467(18) 0.0529(10) Uani 1 1 d D U . . . C3_5 C 0.2893(4) 0.2848(3) 0.7604(2) 0.0233(8) Uani 1 1 d D U . . . F4_5 F 0.3256(3) 0.1893(2) 0.74115(15) 0.0374(7) Uani 1 1 d D U . . . F5_5 F 0.2838(2) 0.3309(2) 0.70453(14) 0.0275(6) Uani 1 1 d D U . . . F6_5 F 0.1815(3) 0.2711(3) 0.76738(17) 0.0419(8) Uani 1 1 d D U . . . C4_5 C 0.3497(4) 0.3177(4) 0.8977(2) 0.0308(10) Uani 1 1 d D U . . . F7_5 F 0.3374(4) 0.2123(3) 0.88602(18) 0.0516(9) Uani 1 1 d D U . . . F8_5 F 0.2514(3) 0.3540(3) 0.91084(18) 0.0513(9) Uani 1 1 d D U . . . F9_5 F 0.4361(3) 0.3551(3) 0.95720(14) 0.0375(7) Uani 1 1 d D U . . . O1_6 O 0.5334(3) 0.2962(2) 0.69302(15) 0.0206(6) Uani 1 1 d D U . . . C1_6 C 0.5463(3) 0.2634(3) 0.6243(2) 0.0218(8) Uani 1 1 d D U . . . C2_6 C 0.4954(4) 0.3444(4) 0.5799(2) 0.0268(9) Uani 1 1 d D U . . . F1_6 F 0.3783(3) 0.3339(3) 0.56365(16) 0.0422(8) Uani 1 1 d D U . . . F2_6 F 0.5269(3) 0.3320(3) 0.51766(15) 0.0391(7) Uani 1 1 d D U . . . F3_6 F 0.5298(3) 0.4441(2) 0.61768(17) 0.0393(7) Uani 1 1 d D U . . . C3_6 C 0.6781(4) 0.2593(4) 0.6253(2) 0.0282(9) Uani 1 1 d D U . . . F4_6 F 0.7326(3) 0.2200(3) 0.67997(15) 0.0365(7) Uani 1 1 d D U . . . F5_6 F 0.7312(2) 0.3580(2) 0.63569(16) 0.0347(6) Uani 1 1 d D U . . . F6_6 F 0.6930(3) 0.2003(3) 0.56376(15) 0.0367(7) Uani 1 1 d D U . . . C4_6 C 0.4783(4) 0.1520(4) 0.5885(2) 0.0316(10) Uani 1 1 d D U . . . F7_6 F 0.5380(3) 0.0788(2) 0.61716(18) 0.0482(9) Uani 1 1 d D U . . . F8_6 F 0.4645(3) 0.1245(3) 0.51692(15) 0.0448(8) Uani 1 1 d D U . . . F9_6 F 0.3735(3) 0.1471(3) 0.60101(18) 0.0489(9) Uani 1 1 d D U . . . F1_7 F -0.0608(13) 0.1960(13) 0.5450(8) 0.036(3) Uani 0.5 1 d D U P A -1 F2_7 F -0.2015(5) 0.0422(5) 0.4379(3) 0.0359(14) Uani 0.5 1 d D U P A -1 F3_7 F -0.1261(5) -0.1527(4) 0.3983(3) 0.0329(13) Uani 0.5 1 d D U P A -1 F4_7 F 0.0878(13) -0.1934(13) 0.4686(8) 0.031(3) Uani 0.5 1 d D U P A -1 C1_7 C -0.0217(10) 0.1003(11) 0.5255(7) 0.023(2) Uani 0.5 1 d D U P A -1 C2_7 C -0.0951(10) 0.0227(10) 0.4715(7) 0.023(2) Uani 0.5 1 d D U P A -1 C3_7 C -0.0567(10) -0.0770(10) 0.4516(7) 0.021(2) Uani 0.5 1 d D U P A -1 C4_7 C 0.0535(10) -0.0952(12) 0.4876(8) 0.023(2) Uani 0.5 1 d D U P A -1 C5_7 C 0.1272(11) -0.0173(12) 0.5416(8) 0.028(3) Uani 0.5 1 d D U P A -1 H5_7 H 0.203334 -0.031526 0.564812 0.033 Uiso 0.5 1 calc R U P A -1 C6_7 C 0.0894(11) 0.0821(11) 0.5618(8) 0.026(2) Uani 0.5 1 d D U P A -1 H6_7 H 0.138347 0.136566 0.599588 0.031 Uiso 0.5 1 calc R U P A -1 O1_8 O 0.7252(5) 0.3777(5) 0.8215(4) 0.0232(11) Uani 0.828(11) 1 d D U P B 1 C1_8 C 0.7920(5) 0.4721(5) 0.8547(3) 0.0232(9) Uani 0.828(11) 1 d D U P B 1 C2_8 C 0.9225(5) 0.4486(5) 0.8720(4) 0.0335(12) Uani 0.828(11) 1 d D U P B 1 F1_8 F 0.9462(5) 0.4074(4) 0.9310(3) 0.0550(16) Uani 0.828(11) 1 d D U P B 1 F2_8 F 0.9966(5) 0.5363(5) 0.8878(4) 0.0397(13) Uani 0.828(11) 1 d D U P B 1 F3_8 F 0.9436(5) 0.3783(5) 0.8195(4) 0.0537(15) Uani 0.828(11) 1 d D U P B 1 C3_8 C 0.7751(6) 0.5496(5) 0.8031(4) 0.0329(12) Uani 0.828(11) 1 d D U P B 1 F4_8 F 0.6640(5) 0.5434(6) 0.7668(3) 0.0463(14) Uani 0.828(11) 1 d D U P B 1 F5_8 F 0.8361(5) 0.5193(5) 0.7518(3) 0.0481(13) Uani 0.828(11) 1 d D U P B 1 F6_8 F 0.8147(8) 0.6497(5) 0.8371(5) 0.0436(17) Uani 0.828(11) 1 d D U P B 1 C4_8 C 0.7604(6) 0.5252(6) 0.9261(4) 0.0422(14) Uani 0.828(11) 1 d D U P B 1 F7_8 F 0.6569(4) 0.5686(5) 0.9079(4) 0.0611(17) Uani 0.828(11) 1 d D U P B 1 F8_8 F 0.8422(6) 0.6023(6) 0.9681(4) 0.0471(17) Uani 0.828(11) 1 d D U P B 1 F9_8 F 0.7431(8) 0.4563(5) 0.9626(3) 0.070(2) Uani 0.828(11) 1 d D U P B 1 O1_9 O 0.710(3) 0.385(2) 0.820(2) 0.031(5) Uani 0.172(11) 1 d D U P B 2 C1_9 C 0.7824(17) 0.4742(19) 0.8544(10) 0.031(3) Uani 0.172(11) 1 d D U P B 2 C2_9 C 0.9052(18) 0.4494(18) 0.8929(12) 0.042(3) Uani 0.172(11) 1 d D U P B 2 F1_9 F 0.895(2) 0.4275(18) 0.9556(11) 0.051(5) Uani 0.172(11) 1 d D U P B 2 F2_9 F 0.984(3) 0.534(2) 0.9060(18) 0.046(6) Uani 0.172(11) 1 d D U P B 2 F3_9 F 0.943(2) 0.370(2) 0.8518(15) 0.049(5) Uani 0.172(11) 1 d D U P B 2 C3_9 C 0.799(2) 0.541(2) 0.7997(12) 0.041(3) Uani 0.172(11) 1 d D U P B 2 F4_9 F 0.697(2) 0.542(3) 0.7543(15) 0.047(5) Uani 0.172(11) 1 d D U P B 2 F5_9 F 0.878(2) 0.495(2) 0.7665(16) 0.059(5) Uani 0.172(11) 1 d D U P B 2 F6_9 F 0.839(4) 0.642(2) 0.833(2) 0.039(5) Uani 0.172(11) 1 d D U P B 2 C4_9 C 0.7300(19) 0.5441(18) 0.9124(12) 0.040(3) Uani 0.172(11) 1 d D U P B 2 F7_9 F 0.647(2) 0.594(2) 0.8757(16) 0.069(6) Uani 0.172(11) 1 d D U P B 2 F8_9 F 0.811(3) 0.617(2) 0.9598(17) 0.044(6) Uani 0.172(11) 1 d D U P B 2 F9_9 F 0.689(2) 0.4850(17) 0.9499(13) 0.039(4) Uani 0.172(11) 1 d D U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Os1 0.01618(7) 0.01732(7) 0.01442(7) 0.00262(5) 0.00478(5) 0.00172(5) Os2 0.01433(10) 0.01519(9) 0.01424(9) 0.00287(7) 0.00443(7) 0.00095(7) Al1 0.0168(5) 0.0183(5) 0.0164(5) 0.0046(4) 0.0057(4) 0.0032(5) Al2 0.0162(5) 0.0168(5) 0.0165(5) 0.0043(4) 0.0036(4) 0.0015(4) F1 0.0228(12) 0.0187(11) 0.0218(11) 0.0065(9) 0.0067(10) 0.0047(9) O2 0.0304(17) 0.0242(15) 0.0339(17) 0.0103(13) 0.0097(14) 0.0026(13) C1 0.0229(19) 0.0180(17) 0.0129(16) 0.0018(13) 0.0048(14) 0.0038(15) C2 0.0214(19) 0.0212(18) 0.0189(17) 0.0049(14) 0.0074(15) -0.0005(16) O1 0.0359(19) 0.0300(17) 0.0193(15) 0.0037(12) 0.0033(13) -0.0001(15) O3 0.0188(14) 0.0299(16) 0.0290(16) 0.0096(13) 0.0056(12) 0.0043(13) O4 0.0249(16) 0.0208(14) 0.0313(16) 0.0061(12) 0.0075(13) 0.0014(12) O5 0.0197(15) 0.0344(17) 0.0313(17) 0.0065(14) 0.0084(13) 0.0051(13) O6 0.0232(16) 0.0332(17) 0.0283(16) 0.0063(13) 0.0086(13) -0.0053(13) O7 0.0244(16) 0.0259(16) 0.0378(18) 0.0100(14) 0.0087(14) 0.0073(13) C3 0.0214(19) 0.0212(18) 0.0151(16) 0.0031(14) 0.0029(15) -0.0007(15) C4 0.0228(19) 0.0171(17) 0.0183(17) 0.0001(14) 0.0067(15) 0.0024(15) C5 0.0189(19) 0.0245(19) 0.0187(18) 0.0021(15) 0.0060(15) 0.0050(16) C6 0.0175(18) 0.0189(17) 0.0174(17) 0.0046(14) 0.0057(14) 0.0002(14) C7 0.0162(17) 0.0173(17) 0.0206(18) 0.0055(14) 0.0047(14) 0.0012(14) O1_1 0.0334(18) 0.0327(17) 0.0215(15) 0.0088(13) 0.0006(13) -0.0128(14) C1_1 0.0213(19) 0.0211(18) 0.0228(18) 0.0038(14) 0.0043(15) -0.0030(15) C2_1 0.034(2) 0.028(2) 0.037(2) 0.0135(19) 0.001(2) 0.0006(19) F1_1 0.0451(18) 0.0446(17) 0.0291(14) 0.0163(13) 0.0069(13) -0.0071(14) F2_1 0.066(2) 0.0283(15) 0.055(2) 0.0200(15) -0.0020(18) -0.0109(15) F3_1 0.0384(17) 0.0454(19) 0.053(2) 0.0177(16) 0.0015(15) 0.0147(15) C3_1 0.028(2) 0.024(2) 0.030(2) 0.0003(16) 0.0080(18) -0.0018(17) F4_1 0.0380(17) 0.0430(17) 0.0246(13) 0.0056(12) 0.0052(12) -0.0108(13) F5_1 0.0377(17) 0.0485(19) 0.0436(18) -0.0064(15) 0.0120(15) 0.0142(15) F6_1 0.0284(14) 0.0263(13) 0.0378(15) -0.0048(11) 0.0052(12) -0.0088(11) C4_1 0.030(2) 0.029(2) 0.027(2) 0.0002(17) 0.0029(18) 0.0007(18) F7_1 0.0369(17) 0.0316(15) 0.0368(15) 0.0016(12) -0.0046(13) 0.0093(13) F8_1 0.0290(15) 0.055(2) 0.0429(17) 0.0093(15) 0.0156(14) -0.0028(14) F9_1 0.051(2) 0.0411(17) 0.0355(16) -0.0084(13) 0.0040(15) 0.0133(16) O1_2 0.0236(15) 0.0265(15) 0.0157(13) 0.0048(11) 0.0000(11) -0.0014(12) C1_2 0.0212(18) 0.032(2) 0.0142(16) 0.0077(15) 0.0038(14) 0.0032(16) C2_2 0.0216(19) 0.033(2) 0.0213(18) 0.0018(16) 0.0039(16) -0.0002(17) F1_2 0.0204(13) 0.0494(18) 0.0454(17) 0.0083(14) 0.0089(13) 0.0098(13) F2_2 0.0281(15) 0.0537(19) 0.0274(14) -0.0076(13) 0.0069(12) -0.0093(14) F3_2 0.0412(17) 0.0335(15) 0.0296(14) 0.0065(12) 0.0134(13) -0.0075(13) C3_2 0.024(2) 0.044(3) 0.028(2) 0.0010(19) 0.0056(18) 0.004(2) F4_2 0.0195(14) 0.066(2) 0.0491(19) -0.0019(17) 0.0103(13) 0.0080(14) F5_2 0.048(2) 0.0389(17) 0.0508(19) 0.0051(14) 0.0127(16) 0.0190(15) F6_2 0.0410(18) 0.075(3) 0.0289(15) -0.0108(15) 0.0154(14) 0.0015(18) C4_2 0.030(2) 0.051(3) 0.031(2) 0.023(2) 0.0021(19) 0.001(2) F7_2 0.0453(19) 0.074(3) 0.0412(18) 0.0315(18) 0.0091(15) -0.0114(18) F8_2 0.048(2) 0.080(3) 0.0342(17) 0.0319(17) -0.0092(15) -0.0015(19) F9_2 0.052(2) 0.0459(19) 0.059(2) 0.0316(16) 0.0025(17) 0.0139(16) O1_3 0.0211(14) 0.0228(14) 0.0242(14) 0.0063(11) 0.0108(12) 0.0071(12) C1_3 0.0229(19) 0.0246(19) 0.0234(18) 0.0055(15) 0.0099(16) 0.0081(16) C2_3 0.023(2) 0.032(2) 0.036(2) 0.0108(19) 0.0124(18) 0.0074(17) F1_3 0.0289(16) 0.052(2) 0.0421(17) 0.0024(15) -0.0001(13) 0.0036(14) F2_3 0.0269(15) 0.0506(19) 0.0548(19) 0.0117(16) 0.0213(14) 0.0098(14) F3_3 0.0309(16) 0.0362(16) 0.070(2) 0.0242(16) 0.0168(16) 0.0040(13) C3_3 0.030(2) 0.035(2) 0.025(2) 0.0085(17) 0.0108(18) 0.0101(19) F4_3 0.0332(16) 0.055(2) 0.0294(15) -0.0008(14) 0.0059(13) -0.0029(14) F5_3 0.053(2) 0.0527(19) 0.0299(15) 0.0190(14) 0.0158(14) 0.0151(16) F6_3 0.0426(18) 0.0512(19) 0.0299(15) -0.0027(13) 0.0143(13) 0.0194(15) C4_3 0.038(2) 0.027(2) 0.028(2) 0.0076(17) 0.0138(19) 0.0139(18) F7_3 0.061(2) 0.0273(15) 0.052(2) 0.0110(14) 0.0163(17) 0.0046(15) F8_3 0.059(2) 0.0480(19) 0.0504(19) 0.0226(15) 0.0293(17) 0.0378(17) F9_3 0.063(2) 0.0438(18) 0.0304(15) 0.0165(13) 0.0158(15) 0.0286(16) O1_5 0.0223(15) 0.0441(19) 0.0219(14) 0.0095(13) 0.0092(12) 0.0119(14) C1_5 0.0209(18) 0.0254(18) 0.0172(16) 0.0062(14) 0.0054(14) 0.0069(15) C2_5 0.042(3) 0.025(2) 0.033(2) 0.0023(18) -0.003(2) 0.010(2) F1_5 0.067(2) 0.0296(15) 0.0377(17) -0.0051(13) -0.0030(16) 0.0094(16) F2_5 0.055(2) 0.046(2) 0.058(2) -0.0011(16) -0.0091(18) 0.0339(18) F3_5 0.072(3) 0.0349(17) 0.0428(18) 0.0183(14) -0.0067(17) -0.0112(17) C3_5 0.0238(19) 0.0219(18) 0.0252(19) 0.0055(15) 0.0086(16) 0.0007(16) F4_5 0.061(2) 0.0212(13) 0.0281(14) 0.0025(11) 0.0113(14) 0.0067(13) F5_5 0.0285(14) 0.0296(13) 0.0246(12) 0.0110(10) 0.0031(11) 0.0023(11) F6_5 0.0243(14) 0.061(2) 0.0354(16) 0.0040(15) 0.0086(12) -0.0106(14) C4_5 0.032(2) 0.041(2) 0.0214(19) 0.0052(18) 0.0125(17) 0.005(2) F7_5 0.086(3) 0.0390(17) 0.0346(17) 0.0164(14) 0.0204(18) -0.0032(18) F8_5 0.0317(16) 0.088(3) 0.0358(17) 0.0036(17) 0.0224(14) 0.0077(17) F9_5 0.0388(16) 0.0564(19) 0.0187(12) 0.0079(12) 0.0100(12) 0.0108(15) O1_6 0.0230(14) 0.0263(15) 0.0142(12) 0.0053(11) 0.0070(11) 0.0042(12) C1_6 0.0211(18) 0.030(2) 0.0148(16) 0.0041(14) 0.0061(14) 0.0052(16) C2_6 0.0199(19) 0.041(2) 0.0228(19) 0.0139(17) 0.0060(16) 0.0066(18) F1_6 0.0225(14) 0.072(2) 0.0342(16) 0.0178(15) 0.0048(12) 0.0177(15) F2_6 0.0392(17) 0.065(2) 0.0256(14) 0.0259(14) 0.0157(13) 0.0206(15) F3_6 0.0446(18) 0.0361(15) 0.0412(17) 0.0174(13) 0.0098(14) 0.0118(14) C3_6 0.026(2) 0.039(2) 0.0231(19) 0.0095(17) 0.0098(17) 0.0087(18) F4_6 0.0316(15) 0.0566(19) 0.0291(14) 0.0207(13) 0.0096(12) 0.0219(14) F5_6 0.0246(14) 0.0454(17) 0.0357(15) 0.0126(13) 0.0090(12) -0.0004(12) F6_6 0.0368(16) 0.0508(18) 0.0298(14) 0.0113(13) 0.0184(13) 0.0185(14) C4_6 0.040(3) 0.033(2) 0.0211(19) 0.0005(17) 0.0127(19) -0.0017(19) F7_6 0.073(3) 0.0278(15) 0.0439(18) 0.0068(13) 0.0170(17) 0.0035(16) F8_6 0.052(2) 0.0519(19) 0.0210(13) -0.0062(13) 0.0070(13) -0.0029(16) F9_6 0.0373(17) 0.057(2) 0.0437(18) -0.0076(16) 0.0162(15) -0.0224(15) F1_7 0.028(7) 0.024(4) 0.052(7) 0.001(4) 0.010(6) 0.004(4) F2_7 0.022(3) 0.036(3) 0.053(4) 0.024(3) 0.001(3) 0.002(2) F3_7 0.033(3) 0.030(3) 0.026(3) 0.002(2) -0.005(2) -0.007(2) F4_7 0.026(6) 0.028(4) 0.041(5) 0.012(4) 0.010(5) 0.010(4) C1_7 0.029(6) 0.016(4) 0.027(5) 0.007(4) 0.012(4) 0.000(4) C2_7 0.019(5) 0.024(4) 0.029(6) 0.015(4) 0.005(4) 0.001(4) C3_7 0.020(5) 0.021(4) 0.019(5) 0.006(3) 0.001(4) -0.003(4) C4_7 0.016(5) 0.024(4) 0.029(6) 0.007(4) 0.006(4) 0.003(4) C5_7 0.023(6) 0.035(5) 0.023(5) 0.010(4) 0.001(4) 0.000(5) C6_7 0.030(6) 0.030(5) 0.017(5) 0.008(4) 0.007(4) -0.004(5) O1_8 0.016(2) 0.0259(19) 0.024(2) 0.0020(16) 0.0026(18) -0.0021(16) C1_8 0.024(2) 0.023(2) 0.0215(19) 0.0045(15) 0.0061(16) -0.0035(16) C2_8 0.025(2) 0.031(2) 0.040(3) 0.009(2) 0.001(2) -0.0028(18) F1_8 0.055(3) 0.043(3) 0.057(3) 0.028(2) -0.016(2) -0.008(2) F2_8 0.0228(19) 0.039(2) 0.056(4) 0.015(2) 0.007(2) -0.0068(16) F3_8 0.029(2) 0.056(3) 0.065(3) -0.004(3) 0.007(3) 0.013(2) C3_8 0.030(3) 0.034(2) 0.037(3) 0.015(2) 0.006(2) 0.002(2) F4_8 0.037(2) 0.048(3) 0.051(3) 0.020(2) -0.003(2) 0.009(2) F5_8 0.054(3) 0.065(3) 0.037(2) 0.026(2) 0.021(2) 0.009(2) F6_8 0.045(4) 0.0286(19) 0.057(3) 0.0175(18) 0.007(3) 0.0035(19) C4_8 0.044(3) 0.044(3) 0.033(3) -0.008(2) 0.021(2) -0.019(2) F7_8 0.042(2) 0.066(3) 0.067(4) -0.022(3) 0.033(2) -0.004(2) F8_8 0.051(3) 0.044(3) 0.035(3) -0.010(2) 0.010(2) -0.015(2) F9_8 0.111(6) 0.067(4) 0.029(2) -0.001(2) 0.031(3) -0.040(3) O1_9 0.033(8) 0.031(6) 0.025(8) 0.003(6) 0.002(7) -0.010(7) C1_9 0.030(5) 0.031(5) 0.029(5) 0.002(4) 0.009(4) -0.011(4) C2_9 0.032(5) 0.040(6) 0.045(7) 0.009(5) 0.000(5) -0.010(5) F1_9 0.058(11) 0.040(9) 0.043(7) 0.011(6) -0.005(6) -0.018(8) F2_9 0.036(8) 0.051(8) 0.039(12) 0.015(7) -0.010(8) -0.020(8) F3_9 0.029(8) 0.053(8) 0.056(10) 0.005(8) 0.001(9) -0.003(6) C3_9 0.044(7) 0.043(6) 0.038(6) 0.012(5) 0.018(5) -0.008(5) F4_9 0.052(8) 0.053(11) 0.036(8) 0.017(8) 0.011(6) -0.015(8) F5_9 0.061(10) 0.059(11) 0.060(11) -0.001(8) 0.041(9) -0.016(8) F6_9 0.033(12) 0.039(6) 0.050(10) 0.017(6) 0.017(8) -0.005(7) C4_9 0.043(7) 0.036(6) 0.038(6) 0.000(4) 0.018(5) -0.008(5) F7_9 0.078(10) 0.057(11) 0.066(12) 0.006(9) 0.014(8) 0.023(8) F8_9 0.063(11) 0.036(9) 0.032(8) -0.004(6) 0.026(7) -0.019(8) F9_9 0.046(10) 0.027(8) 0.040(9) -0.009(6) 0.025(8) -0.010(7) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Os1 C4 1.980(4) . ? Os1 C1 1.986(4) . ? Os1 C3 1.990(4) . ? Os1 C2 1.996(4) . ? Os1 C5 1.997(4) . ? Os1 Os2 2.9106(7) . ? Os2 C7 1.962(4) . ? Os2 C7 1.962(4) 2_566 ? Os2 C6 1.965(4) 2_566 ? Os2 C6 1.965(4) . ? Al1 O1_9 1.61(3) . ? Al1 O1_5 1.701(3) . ? Al1 O1_8 1.715(6) . ? Al1 O1_6 1.716(3) . ? Al1 F1 1.767(3) . ? Al2 O1_2 1.697(3) . ? Al2 O1_1 1.702(3) . ? Al2 O1_3 1.712(3) . ? Al2 F1 1.767(3) . ? O2 C2 1.123(5) . ? C1 O1 1.106(5) . ? O3 C3 1.122(5) . ? O4 C4 1.127(5) . ? O5 C5 1.119(5) . ? O6 C6 1.123(5) . ? O7 C7 1.128(5) . ? O1_1 C1_1 1.355(5) . ? C1_1 C2_1 1.551(6) . ? C1_1 C3_1 1.556(5) . ? C1_1 C4_1 1.559(6) . ? C2_1 F3_1 1.320(6) . ? C2_1 F1_1 1.327(6) . ? C2_1 F2_1 1.345(5) . ? C3_1 F4_1 1.327(5) . ? C3_1 F5_1 1.330(5) . ? C3_1 F6_1 1.337(5) . ? C4_1 F9_1 1.322(5) . ? C4_1 F8_1 1.332(5) . ? C4_1 F7_1 1.337(5) . ? O1_2 C1_2 1.363(5) . ? C1_2 C4_2 1.549(6) . ? C1_2 C2_2 1.552(6) . ? C1_2 C3_2 1.554(6) . ? C2_2 F2_2 1.328(5) . ? C2_2 F1_2 1.329(5) . ? C2_2 F3_2 1.343(5) . ? C3_2 F5_2 1.326(6) . ? C3_2 F4_2 1.328(5) . ? C3_2 F6_2 1.333(5) . ? C4_2 F9_2 1.327(6) . ? C4_2 F7_2 1.329(6) . ? C4_2 F8_2 1.335(5) . ? O1_3 C1_3 1.352(5) . ? C1_3 C4_3 1.556(6) . ? C1_3 C2_3 1.558(6) . ? C1_3 C3_3 1.560(6) . ? C2_3 F3_3 1.318(5) . ? C2_3 F2_3 1.331(5) . ? C2_3 F1_3 1.338(5) . ? C3_3 F4_3 1.310(5) . ? C3_3 F5_3 1.337(5) . ? C3_3 F6_3 1.342(5) . ? C4_3 F9_3 1.311(5) . ? C4_3 F8_3 1.334(5) . ? C4_3 F7_3 1.348(6) . ? O1_5 C1_5 1.349(5) . ? C1_5 C4_5 1.553(6) . ? C1_5 C3_5 1.556(5) . ? C1_5 C2_5 1.557(6) . ? C2_5 F1_5 1.328(5) . ? C2_5 F3_5 1.332(6) . ? C2_5 F2_5 1.332(6) . ? C3_5 F6_5 1.320(5) . ? C3_5 F4_5 1.332(5) . ? C3_5 F5_5 1.343(5) . ? C4_5 F9_5 1.327(5) . ? C4_5 F7_5 1.327(6) . ? C4_5 F8_5 1.334(5) . ? O1_6 C1_6 1.361(4) . ? C1_6 C4_6 1.546(6) . ? C1_6 C2_6 1.555(6) . ? C1_6 C3_6 1.555(6) . ? C2_6 F3_6 1.327(5) . ? C2_6 F2_6 1.333(5) . ? C2_6 F1_6 1.335(5) . ? C3_6 F4_6 1.323(5) . ? C3_6 F6_6 1.329(5) . ? C3_6 F5_6 1.347(5) . ? C4_6 F9_6 1.319(5) . ? C4_6 F8_6 1.331(5) . ? C4_6 F7_6 1.345(6) . ? F1_7 C1_7 1.350(11) . ? F2_7 C2_7 1.334(10) . ? F3_7 C3_7 1.334(10) . ? F4_7 C4_7 1.352(11) . ? C1_7 C2_7 1.372(10) . ? C1_7 C6_7 1.390(11) . ? C2_7 C3_7 1.393(10) . ? C3_7 C4_7 1.380(10) . ? C4_7 C5_7 1.375(10) . ? C5_7 C6_7 1.388(11) . ? C5_7 H5_7 0.9500 . ? C6_7 H6_7 0.9500 . ? O1_8 C1_8 1.360(6) . ? C1_8 C4_8 1.551(7) . ? C1_8 C2_8 1.555(7) . ? C1_8 C3_8 1.558(7) . ? C2_8 F3_8 1.293(7) . ? C2_8 F2_8 1.331(6) . ? C2_8 F1_8 1.349(7) . ? C3_8 F4_8 1.322(7) . ? C3_8 F6_8 1.324(7) . ? C3_8 F5_8 1.370(7) . ? C4_8 F9_8 1.294(7) . ? C4_8 F8_8 1.331(7) . ? C4_8 F7_8 1.370(8) . ? O1_9 C1_9 1.351(14) . ? C1_9 C2_9 1.548(12) . ? C1_9 C4_9 1.556(12) . ? C1_9 C3_9 1.558(13) . ? C2_9 F3_9 1.326(13) . ? C2_9 F1_9 1.345(13) . ? C2_9 F2_9 1.347(13) . ? C3_9 F4_9 1.318(13) . ? C3_9 F6_9 1.330(13) . ? C3_9 F5_9 1.346(13) . ? C4_9 F9_9 1.319(13) . ? C4_9 F8_9 1.329(13) . ? C4_9 F7_9 1.343(13) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 Os1 C1 92.69(16) . . ? C4 Os1 C3 90.63(17) . . ? C1 Os1 C3 94.67(16) . . ? C4 Os1 C2 173.74(16) . . ? C1 Os1 C2 93.56(16) . . ? C3 Os1 C2 89.28(17) . . ? C4 Os1 C5 89.25(18) . . ? C1 Os1 C5 95.19(17) . . ? C3 Os1 C5 170.14(16) . . ? C2 Os1 C5 89.77(18) . . ? C4 Os1 Os2 85.11(11) . . ? C1 Os1 Os2 177.78(12) . . ? C3 Os1 Os2 85.07(11) . . ? C2 Os1 Os2 88.64(12) . . ? C5 Os1 Os2 85.10(12) . . ? C7 Os2 C7 180.0 . 2_566 ? C7 Os2 C6 89.62(17) . 2_566 ? C7 Os2 C6 90.38(17) 2_566 2_566 ? C7 Os2 C6 90.38(17) . . ? C7 Os2 C6 89.62(17) 2_566 . ? C6 Os2 C6 180.0 2_566 . ? C7 Os2 Os1 89.80(12) . 2_566 ? C7 Os2 Os1 90.20(12) 2_566 2_566 ? C6 Os2 Os1 90.58(11) 2_566 2_566 ? C6 Os2 Os1 89.42(11) . 2_566 ? C7 Os2 Os1 90.20(12) . . ? C7 Os2 Os1 89.80(12) 2_566 . ? C6 Os2 Os1 89.42(11) 2_566 . ? C6 Os2 Os1 90.58(11) . . ? Os1 Os2 Os1 180.0 2_566 . ? O1_9 Al1 O1_5 110.3(14) . . ? O1_5 Al1 O1_8 114.4(3) . . ? O1_9 Al1 O1_6 114.3(16) . . ? O1_5 Al1 O1_6 111.05(16) . . ? O1_8 Al1 O1_6 115.4(3) . . ? O1_9 Al1 F1 107.8(14) . . ? O1_5 Al1 F1 105.14(16) . . ? O1_8 Al1 F1 102.0(3) . . ? O1_6 Al1 F1 107.69(14) . . ? O1_2 Al2 O1_1 109.86(16) . . ? O1_2 Al2 O1_3 118.39(16) . . ? O1_1 Al2 O1_3 112.57(17) . . ? O1_2 Al2 F1 109.68(14) . . ? O1_1 Al2 F1 104.06(16) . . ? O1_3 Al2 F1 100.93(14) . . ? Al2 F1 Al1 176.26(17) . . ? O1 C1 Os1 179.3(4) . . ? O2 C2 Os1 179.5(4) . . ? O3 C3 Os1 176.8(4) . . ? O4 C4 Os1 177.9(4) . . ? O5 C5 Os1 177.4(4) . . ? O6 C6 Os2 177.8(4) . . ? O7 C7 Os2 178.4(4) . . ? C1_1 O1_1 Al2 149.0(3) . . ? O1_1 C1_1 C2_1 112.0(3) . . ? O1_1 C1_1 C3_1 107.5(3) . . ? C2_1 C1_1 C3_1 110.1(3) . . ? O1_1 C1_1 C4_1 109.2(4) . . ? C2_1 C1_1 C4_1 108.9(4) . . ? C3_1 C1_1 C4_1 109.2(3) . . ? F3_1 C2_1 F1_1 108.1(4) . . ? F3_1 C2_1 F2_1 108.5(4) . . ? F1_1 C2_1 F2_1 107.7(4) . . ? F3_1 C2_1 C1_1 110.2(4) . . ? F1_1 C2_1 C1_1 111.4(4) . . ? F2_1 C2_1 C1_1 110.8(4) . . ? F4_1 C3_1 F5_1 107.4(4) . . ? F4_1 C3_1 F6_1 107.1(4) . . ? F5_1 C3_1 F6_1 107.9(4) . . ? F4_1 C3_1 C1_1 111.4(3) . . ? F5_1 C3_1 C1_1 110.3(4) . . ? F6_1 C3_1 C1_1 112.5(4) . . ? F9_1 C4_1 F8_1 108.8(4) . . ? F9_1 C4_1 F7_1 107.8(4) . . ? F8_1 C4_1 F7_1 106.8(4) . . ? F9_1 C4_1 C1_1 110.7(4) . . ? F8_1 C4_1 C1_1 112.2(4) . . ? F7_1 C4_1 C1_1 110.5(4) . . ? C1_2 O1_2 Al2 147.1(3) . . ? O1_2 C1_2 C4_2 108.9(4) . . ? O1_2 C1_2 C2_2 110.2(3) . . ? C4_2 C1_2 C2_2 109.5(3) . . ? O1_2 C1_2 C3_2 108.7(3) . . ? C4_2 C1_2 C3_2 110.1(4) . . ? C2_2 C1_2 C3_2 109.4(4) . . ? F2_2 C2_2 F1_2 108.5(4) . . ? F2_2 C2_2 F3_2 107.7(4) . . ? F1_2 C2_2 F3_2 106.8(4) . . ? F2_2 C2_2 C1_2 112.9(3) . . ? F1_2 C2_2 C1_2 111.5(4) . . ? F3_2 C2_2 C1_2 109.1(3) . . ? F5_2 C3_2 F4_2 107.9(4) . . ? F5_2 C3_2 F6_2 108.0(4) . . ? F4_2 C3_2 F6_2 107.6(4) . . ? F5_2 C3_2 C1_2 110.7(4) . . ? F4_2 C3_2 C1_2 110.2(4) . . ? F6_2 C3_2 C1_2 112.3(4) . . ? F9_2 C4_2 F7_2 107.4(4) . . ? F9_2 C4_2 F8_2 108.7(4) . . ? F7_2 C4_2 F8_2 108.1(4) . . ? F9_2 C4_2 C1_2 110.5(4) . . ? F7_2 C4_2 C1_2 110.7(4) . . ? F8_2 C4_2 C1_2 111.3(4) . . ? C1_3 O1_3 Al2 151.4(3) . . ? O1_3 C1_3 C4_3 111.1(3) . . ? O1_3 C1_3 C2_3 108.1(3) . . ? C4_3 C1_3 C2_3 108.7(3) . . ? O1_3 C1_3 C3_3 109.7(3) . . ? C4_3 C1_3 C3_3 109.2(3) . . ? C2_3 C1_3 C3_3 110.1(3) . . ? F3_3 C2_3 F2_3 109.0(4) . . ? F3_3 C2_3 F1_3 107.4(4) . . ? F2_3 C2_3 F1_3 107.1(4) . . ? F3_3 C2_3 C1_3 110.8(4) . . ? F2_3 C2_3 C1_3 112.3(4) . . ? F1_3 C2_3 C1_3 110.0(4) . . ? F4_3 C3_3 F5_3 108.5(4) . . ? F4_3 C3_3 F6_3 108.8(4) . . ? F5_3 C3_3 F6_3 105.8(4) . . ? F4_3 C3_3 C1_3 111.2(4) . . ? F5_3 C3_3 C1_3 110.2(4) . . ? F6_3 C3_3 C1_3 112.1(4) . . ? F9_3 C4_3 F8_3 109.0(4) . . ? F9_3 C4_3 F7_3 107.3(4) . . ? F8_3 C4_3 F7_3 105.1(4) . . ? F9_3 C4_3 C1_3 112.5(3) . . ? F8_3 C4_3 C1_3 112.6(4) . . ? F7_3 C4_3 C1_3 110.0(4) . . ? C1_5 O1_5 Al1 148.5(3) . . ? O1_5 C1_5 C4_5 108.6(3) . . ? O1_5 C1_5 C3_5 112.3(3) . . ? C4_5 C1_5 C3_5 109.0(3) . . ? O1_5 C1_5 C2_5 108.9(4) . . ? C4_5 C1_5 C2_5 109.2(4) . . ? C3_5 C1_5 C2_5 108.7(3) . . ? F1_5 C2_5 F3_5 107.7(4) . . ? F1_5 C2_5 F2_5 108.3(4) . . ? F3_5 C2_5 F2_5 107.3(4) . . ? F1_5 C2_5 C1_5 111.5(4) . . ? F3_5 C2_5 C1_5 109.5(4) . . ? F2_5 C2_5 C1_5 112.3(4) . . ? F6_5 C3_5 F4_5 108.4(4) . . ? F6_5 C3_5 F5_5 107.3(4) . . ? F4_5 C3_5 F5_5 106.6(3) . . ? F6_5 C3_5 C1_5 113.1(3) . . ? F4_5 C3_5 C1_5 109.6(3) . . ? F5_5 C3_5 C1_5 111.5(3) . . ? F9_5 C4_5 F7_5 107.8(4) . . ? F9_5 C4_5 F8_5 107.8(4) . . ? F7_5 C4_5 F8_5 108.3(4) . . ? F9_5 C4_5 C1_5 111.1(4) . . ? F7_5 C4_5 C1_5 110.3(3) . . ? F8_5 C4_5 C1_5 111.6(4) . . ? C1_6 O1_6 Al1 146.7(3) . . ? O1_6 C1_6 C4_6 109.3(3) . . ? O1_6 C1_6 C2_6 108.4(3) . . ? C4_6 C1_6 C2_6 109.6(3) . . ? O1_6 C1_6 C3_6 110.9(3) . . ? C4_6 C1_6 C3_6 110.0(3) . . ? C2_6 C1_6 C3_6 108.6(3) . . ? F3_6 C2_6 F2_6 108.0(4) . . ? F3_6 C2_6 F1_6 106.3(4) . . ? F2_6 C2_6 F1_6 107.6(3) . . ? F3_6 C2_6 C1_6 111.4(3) . . ? F2_6 C2_6 C1_6 112.3(4) . . ? F1_6 C2_6 C1_6 110.9(4) . . ? F4_6 C3_6 F6_6 108.8(4) . . ? F4_6 C3_6 F5_6 107.0(4) . . ? F6_6 C3_6 F5_6 108.0(4) . . ? F4_6 C3_6 C1_6 109.9(3) . . ? F6_6 C3_6 C1_6 112.4(4) . . ? F5_6 C3_6 C1_6 110.7(4) . . ? F9_6 C4_6 F8_6 108.0(4) . . ? F9_6 C4_6 F7_6 107.9(4) . . ? F8_6 C4_6 F7_6 107.6(4) . . ? F9_6 C4_6 C1_6 111.1(4) . . ? F8_6 C4_6 C1_6 112.9(4) . . ? F7_6 C4_6 C1_6 109.0(4) . . ? F1_7 C1_7 C2_7 118.5(10) . . ? F1_7 C1_7 C6_7 119.4(10) . . ? C2_7 C1_7 C6_7 122.1(9) . . ? F2_7 C2_7 C1_7 120.8(9) . . ? F2_7 C2_7 C3_7 120.1(10) . . ? C1_7 C2_7 C3_7 119.1(8) . . ? F3_7 C3_7 C4_7 121.3(8) . . ? F3_7 C3_7 C2_7 119.9(9) . . ? C4_7 C3_7 C2_7 118.9(8) . . ? F4_7 C4_7 C5_7 120.2(10) . . ? F4_7 C4_7 C3_7 117.8(10) . . ? C5_7 C4_7 C3_7 122.0(9) . . ? C4_7 C5_7 C6_7 119.4(9) . . ? C4_7 C5_7 H5_7 120.3 . . ? C6_7 C5_7 H5_7 120.3 . . ? C5_7 C6_7 C1_7 118.5(9) . . ? C5_7 C6_7 H6_7 120.8 . . ? C1_7 C6_7 H6_7 120.8 . . ? C1_8 O1_8 Al1 151.0(5) . . ? O1_8 C1_8 C4_8 111.2(5) . . ? O1_8 C1_8 C2_8 107.5(5) . . ? C4_8 C1_8 C2_8 109.8(5) . . ? O1_8 C1_8 C3_8 110.4(5) . . ? C4_8 C1_8 C3_8 109.1(5) . . ? C2_8 C1_8 C3_8 108.7(5) . . ? F3_8 C2_8 F2_8 110.2(6) . . ? F3_8 C2_8 F1_8 106.5(5) . . ? F2_8 C2_8 F1_8 106.5(5) . . ? F3_8 C2_8 C1_8 111.7(5) . . ? F2_8 C2_8 C1_8 112.5(5) . . ? F1_8 C2_8 C1_8 109.1(5) . . ? F4_8 C3_8 F6_8 110.2(6) . . ? F4_8 C3_8 F5_8 105.9(5) . . ? F6_8 C3_8 F5_8 107.0(6) . . ? F4_8 C3_8 C1_8 111.2(5) . . ? F6_8 C3_8 C1_8 113.3(6) . . ? F5_8 C3_8 C1_8 108.9(5) . . ? F9_8 C4_8 F8_8 109.5(6) . . ? F9_8 C4_8 F7_8 106.9(6) . . ? F8_8 C4_8 F7_8 108.5(6) . . ? F9_8 C4_8 C1_8 111.8(5) . . ? F8_8 C4_8 C1_8 112.0(5) . . ? F7_8 C4_8 C1_8 108.0(5) . . ? C1_9 O1_9 Al1 161(3) . . ? O1_9 C1_9 C2_9 111.9(17) . . ? O1_9 C1_9 C4_9 110.0(17) . . ? C2_9 C1_9 C4_9 108.4(12) . . ? O1_9 C1_9 C3_9 110.9(18) . . ? C2_9 C1_9 C3_9 107.5(13) . . ? C4_9 C1_9 C3_9 108.0(13) . . ? F3_9 C2_9 F1_9 112.1(16) . . ? F3_9 C2_9 F2_9 106.0(17) . . ? F1_9 C2_9 F2_9 110.6(17) . . ? F3_9 C2_9 C1_9 111.9(15) . . ? F1_9 C2_9 C1_9 106.3(14) . . ? F2_9 C2_9 C1_9 110.0(16) . . ? F4_9 C3_9 F6_9 106.7(18) . . ? F4_9 C3_9 F5_9 113.2(18) . . ? F6_9 C3_9 F5_9 110.5(18) . . ? F4_9 C3_9 C1_9 109.0(16) . . ? F6_9 C3_9 C1_9 111.6(18) . . ? F5_9 C3_9 C1_9 105.9(15) . . ? F9_9 C4_9 F8_9 107.1(17) . . ? F9_9 C4_9 F7_9 113.2(18) . . ? F8_9 C4_9 F7_9 108.5(18) . . ? F9_9 C4_9 C1_9 110.6(15) . . ? F8_9 C4_9 C1_9 111.5(17) . . ? F7_9 C4_9 C1_9 106.0(14) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_2 Al2 O1_1 C1_1 -10.1(7) . . . . ? O1_3 Al2 O1_1 C1_1 124.1(6) . . . . ? F1 Al2 O1_1 C1_1 -127.5(6) . . . . ? Al2 O1_1 C1_1 C2_1 -24.6(8) . . . . ? Al2 O1_1 C1_1 C3_1 -145.7(5) . . . . ? Al2 O1_1 C1_1 C4_1 96.0(7) . . . . ? O1_1 C1_1 C2_1 F3_1 -40.8(5) . . . . ? C3_1 C1_1 C2_1 F3_1 78.7(5) . . . . ? C4_1 C1_1 C2_1 F3_1 -161.6(4) . . . . ? O1_1 C1_1 C2_1 F1_1 79.2(5) . . . . ? C3_1 C1_1 C2_1 F1_1 -161.2(4) . . . . ? C4_1 C1_1 C2_1 F1_1 -41.6(5) . . . . ? O1_1 C1_1 C2_1 F2_1 -160.9(4) . . . . ? C3_1 C1_1 C2_1 F2_1 -41.3(5) . . . . ? C4_1 C1_1 C2_1 F2_1 78.3(5) . . . . ? O1_1 C1_1 C3_1 F4_1 -41.2(5) . . . . ? C2_1 C1_1 C3_1 F4_1 -163.5(4) . . . . ? C4_1 C1_1 C3_1 F4_1 77.1(4) . . . . ? O1_1 C1_1 C3_1 F5_1 78.0(5) . . . . ? C2_1 C1_1 C3_1 F5_1 -44.3(5) . . . . ? C4_1 C1_1 C3_1 F5_1 -163.7(4) . . . . ? O1_1 C1_1 C3_1 F6_1 -161.5(4) . . . . ? C2_1 C1_1 C3_1 F6_1 76.2(5) . . . . ? C4_1 C1_1 C3_1 F6_1 -43.2(5) . . . . ? O1_1 C1_1 C4_1 F9_1 -46.6(5) . . . . ? C2_1 C1_1 C4_1 F9_1 75.9(5) . . . . ? C3_1 C1_1 C4_1 F9_1 -163.8(4) . . . . ? O1_1 C1_1 C4_1 F8_1 -168.3(3) . . . . ? C2_1 C1_1 C4_1 F8_1 -45.8(5) . . . . ? C3_1 C1_1 C4_1 F8_1 74.5(4) . . . . ? O1_1 C1_1 C4_1 F7_1 72.7(4) . . . . ? C2_1 C1_1 C4_1 F7_1 -164.8(3) . . . . ? C3_1 C1_1 C4_1 F7_1 -44.6(5) . . . . ? O1_1 Al2 O1_2 C1_2 -159.2(5) . . . . ? O1_3 Al2 O1_2 C1_2 69.6(6) . . . . ? F1 Al2 O1_2 C1_2 -45.4(6) . . . . ? Al2 O1_2 C1_2 C4_2 -158.5(4) . . . . ? Al2 O1_2 C1_2 C2_2 -38.3(7) . . . . ? Al2 O1_2 C1_2 C3_2 81.6(6) . . . . ? O1_2 C1_2 C2_2 F2_2 160.3(4) . . . . ? C4_2 C1_2 C2_2 F2_2 -79.9(5) . . . . ? C3_2 C1_2 C2_2 F2_2 40.8(5) . . . . ? O1_2 C1_2 C2_2 F1_2 -77.2(4) . . . . ? C4_2 C1_2 C2_2 F1_2 42.6(5) . . . . ? C3_2 C1_2 C2_2 F1_2 163.3(3) . . . . ? O1_2 C1_2 C2_2 F3_2 40.6(5) . . . . ? C4_2 C1_2 C2_2 F3_2 160.4(4) . . . . ? C3_2 C1_2 C2_2 F3_2 -78.9(4) . . . . ? O1_2 C1_2 C3_2 F5_2 -73.8(5) . . . . ? C4_2 C1_2 C3_2 F5_2 167.0(4) . . . . ? C2_2 C1_2 C3_2 F5_2 46.6(5) . . . . ? O1_2 C1_2 C3_2 F4_2 45.5(5) . . . . ? C4_2 C1_2 C3_2 F4_2 -73.7(5) . . . . ? C2_2 C1_2 C3_2 F4_2 165.9(4) . . . . ? O1_2 C1_2 C3_2 F6_2 165.5(4) . . . . ? C4_2 C1_2 C3_2 F6_2 46.3(5) . . . . ? C2_2 C1_2 C3_2 F6_2 -74.1(5) . . . . ? O1_2 C1_2 C4_2 F9_2 43.9(5) . . . . ? C2_2 C1_2 C4_2 F9_2 -76.7(5) . . . . ? C3_2 C1_2 C4_2 F9_2 163.0(4) . . . . ? O1_2 C1_2 C4_2 F7_2 -74.9(5) . . . . ? C2_2 C1_2 C4_2 F7_2 164.5(4) . . . . ? C3_2 C1_2 C4_2 F7_2 44.2(5) . . . . ? O1_2 C1_2 C4_2 F8_2 164.8(4) . . . . ? C2_2 C1_2 C4_2 F8_2 44.2(5) . . . . ? C3_2 C1_2 C4_2 F8_2 -76.1(5) . . . . ? O1_2 Al2 O1_3 C1_3 75.4(6) . . . . ? O1_1 Al2 O1_3 C1_3 -54.6(6) . . . . ? F1 Al2 O1_3 C1_3 -165.0(6) . . . . ? Al2 O1_3 C1_3 C4_3 -30.7(7) . . . . ? Al2 O1_3 C1_3 C2_3 -149.9(5) . . . . ? Al2 O1_3 C1_3 C3_3 90.1(6) . . . . ? O1_3 C1_3 C2_3 F3_3 -43.8(5) . . . . ? C4_3 C1_3 C2_3 F3_3 -164.5(4) . . . . ? C3_3 C1_3 C2_3 F3_3 76.0(4) . . . . ? O1_3 C1_3 C2_3 F2_3 -166.0(4) . . . . ? C4_3 C1_3 C2_3 F2_3 73.3(5) . . . . ? C3_3 C1_3 C2_3 F2_3 -46.2(5) . . . . ? O1_3 C1_3 C2_3 F1_3 74.9(4) . . . . ? C4_3 C1_3 C2_3 F1_3 -45.8(4) . . . . ? C3_3 C1_3 C2_3 F1_3 -165.3(3) . . . . ? O1_3 C1_3 C3_3 F4_3 -44.2(5) . . . . ? C4_3 C1_3 C3_3 F4_3 77.7(5) . . . . ? C2_3 C1_3 C3_3 F4_3 -163.1(4) . . . . ? O1_3 C1_3 C3_3 F5_3 76.1(4) . . . . ? C4_3 C1_3 C3_3 F5_3 -162.0(4) . . . . ? C2_3 C1_3 C3_3 F5_3 -42.8(5) . . . . ? O1_3 C1_3 C3_3 F6_3 -166.3(4) . . . . ? C4_3 C1_3 C3_3 F6_3 -44.4(5) . . . . ? C2_3 C1_3 C3_3 F6_3 74.8(5) . . . . ? O1_3 C1_3 C4_3 F9_3 -39.6(5) . . . . ? C2_3 C1_3 C4_3 F9_3 79.3(5) . . . . ? C3_3 C1_3 C4_3 F9_3 -160.7(4) . . . . ? O1_3 C1_3 C4_3 F8_3 -163.2(4) . . . . ? C2_3 C1_3 C4_3 F8_3 -44.3(5) . . . . ? C3_3 C1_3 C4_3 F8_3 75.7(5) . . . . ? O1_3 C1_3 C4_3 F7_3 79.9(4) . . . . ? C2_3 C1_3 C4_3 F7_3 -161.2(4) . . . . ? C3_3 C1_3 C4_3 F7_3 -41.2(5) . . . . ? O1_9 Al1 O1_5 C1_5 136.8(17) . . . . ? O1_8 Al1 O1_5 C1_5 141.7(6) . . . . ? O1_6 Al1 O1_5 C1_5 8.9(7) . . . . ? F1 Al1 O1_5 C1_5 -107.2(6) . . . . ? Al1 O1_5 C1_5 C4_5 147.0(5) . . . . ? Al1 O1_5 C1_5 C3_5 26.4(8) . . . . ? Al1 O1_5 C1_5 C2_5 -94.1(6) . . . . ? O1_5 C1_5 C2_5 F1_5 -76.5(5) . . . . ? C4_5 C1_5 C2_5 F1_5 42.0(6) . . . . ? C3_5 C1_5 C2_5 F1_5 160.9(4) . . . . ? O1_5 C1_5 C2_5 F3_5 42.7(5) . . . . ? C4_5 C1_5 C2_5 F3_5 161.2(4) . . . . ? C3_5 C1_5 C2_5 F3_5 -80.0(4) . . . . ? O1_5 C1_5 C2_5 F2_5 161.8(4) . . . . ? C4_5 C1_5 C2_5 F2_5 -79.7(5) . . . . ? C3_5 C1_5 C2_5 F2_5 39.2(5) . . . . ? O1_5 C1_5 C3_5 F6_5 160.2(4) . . . . ? C4_5 C1_5 C3_5 F6_5 39.8(5) . . . . ? C2_5 C1_5 C3_5 F6_5 -79.2(5) . . . . ? O1_5 C1_5 C3_5 F4_5 39.1(5) . . . . ? C4_5 C1_5 C3_5 F4_5 -81.3(4) . . . . ? C2_5 C1_5 C3_5 F4_5 159.7(4) . . . . ? O1_5 C1_5 C3_5 F5_5 -78.7(4) . . . . ? C4_5 C1_5 C3_5 F5_5 160.9(3) . . . . ? C2_5 C1_5 C3_5 F5_5 41.9(5) . . . . ? O1_5 C1_5 C4_5 F9_5 44.3(5) . . . . ? C3_5 C1_5 C4_5 F9_5 166.9(4) . . . . ? C2_5 C1_5 C4_5 F9_5 -74.4(5) . . . . ? O1_5 C1_5 C4_5 F7_5 -75.1(5) . . . . ? C3_5 C1_5 C4_5 F7_5 47.5(5) . . . . ? C2_5 C1_5 C4_5 F7_5 166.2(4) . . . . ? O1_5 C1_5 C4_5 F8_5 164.5(4) . . . . ? C3_5 C1_5 C4_5 F8_5 -72.8(5) . . . . ? C2_5 C1_5 C4_5 F8_5 45.8(5) . . . . ? O1_9 Al1 O1_6 C1_6 68.4(16) . . . . ? O1_5 Al1 O1_6 C1_6 -166.0(5) . . . . ? O1_8 Al1 O1_6 C1_6 61.7(6) . . . . ? F1 Al1 O1_6 C1_6 -51.3(5) . . . . ? Al1 O1_6 C1_6 C4_6 95.0(5) . . . . ? Al1 O1_6 C1_6 C2_6 -145.5(4) . . . . ? Al1 O1_6 C1_6 C3_6 -26.3(7) . . . . ? O1_6 C1_6 C2_6 F3_6 44.9(5) . . . . ? C4_6 C1_6 C2_6 F3_6 164.2(4) . . . . ? C3_6 C1_6 C2_6 F3_6 -75.6(4) . . . . ? O1_6 C1_6 C2_6 F2_6 166.3(4) . . . . ? C4_6 C1_6 C2_6 F2_6 -74.4(4) . . . . ? C3_6 C1_6 C2_6 F2_6 45.7(5) . . . . ? O1_6 C1_6 C2_6 F1_6 -73.3(4) . . . . ? C4_6 C1_6 C2_6 F1_6 46.0(5) . . . . ? C3_6 C1_6 C2_6 F1_6 166.1(3) . . . . ? O1_6 C1_6 C3_6 F4_6 40.8(5) . . . . ? C4_6 C1_6 C3_6 F4_6 -80.2(4) . . . . ? C2_6 C1_6 C3_6 F4_6 159.8(4) . . . . ? O1_6 C1_6 C3_6 F6_6 162.0(4) . . . . ? C4_6 C1_6 C3_6 F6_6 41.0(5) . . . . ? C2_6 C1_6 C3_6 F6_6 -78.9(4) . . . . ? O1_6 C1_6 C3_6 F5_6 -77.2(4) . . . . ? C4_6 C1_6 C3_6 F5_6 161.8(3) . . . . ? C2_6 C1_6 C3_6 F5_6 41.9(4) . . . . ? O1_6 C1_6 C4_6 F9_6 44.3(5) . . . . ? C2_6 C1_6 C4_6 F9_6 -74.4(5) . . . . ? C3_6 C1_6 C4_6 F9_6 166.2(4) . . . . ? O1_6 C1_6 C4_6 F8_6 165.9(4) . . . . ? C2_6 C1_6 C4_6 F8_6 47.2(5) . . . . ? C3_6 C1_6 C4_6 F8_6 -72.1(5) . . . . ? O1_6 C1_6 C4_6 F7_6 -74.6(4) . . . . ? C2_6 C1_6 C4_6 F7_6 166.7(3) . . . . ? C3_6 C1_6 C4_6 F7_6 47.4(5) . . . . ? F1_7 C1_7 C2_7 F2_7 1.6(15) . . . . ? C6_7 C1_7 C2_7 F2_7 179.6(10) . . . . ? F1_7 C1_7 C2_7 C3_7 -178.9(9) . . . . ? C6_7 C1_7 C2_7 C3_7 -0.9(15) . . . . ? F2_7 C2_7 C3_7 F3_7 0.7(15) . . . . ? C1_7 C2_7 C3_7 F3_7 -178.8(10) . . . . ? F2_7 C2_7 C3_7 C4_7 -179.6(10) . . . . ? C1_7 C2_7 C3_7 C4_7 0.9(15) . . . . ? F3_7 C3_7 C4_7 F4_7 -1.8(16) . . . . ? C2_7 C3_7 C4_7 F4_7 178.4(10) . . . . ? F3_7 C3_7 C4_7 C5_7 178.6(11) . . . . ? C2_7 C3_7 C4_7 C5_7 -1.2(16) . . . . ? F4_7 C4_7 C5_7 C6_7 -178.2(10) . . . . ? C3_7 C4_7 C5_7 C6_7 1.3(16) . . . . ? C4_7 C5_7 C6_7 C1_7 -1.2(16) . . . . ? F1_7 C1_7 C6_7 C5_7 179.1(10) . . . . ? C2_7 C1_7 C6_7 C5_7 1.1(15) . . . . ? O1_5 Al1 O1_8 C1_8 -42.6(14) . . . . ? O1_6 Al1 O1_8 C1_8 88.1(13) . . . . ? F1 Al1 O1_8 C1_8 -155.5(13) . . . . ? Al1 O1_8 C1_8 C4_8 56.6(14) . . . . ? Al1 O1_8 C1_8 C2_8 176.9(12) . . . . ? Al1 O1_8 C1_8 C3_8 -64.7(14) . . . . ? O1_8 C1_8 C2_8 F3_8 40.0(7) . . . . ? C4_8 C1_8 C2_8 F3_8 161.1(6) . . . . ? C3_8 C1_8 C2_8 F3_8 -79.6(6) . . . . ? O1_8 C1_8 C2_8 F2_8 164.5(6) . . . . ? C4_8 C1_8 C2_8 F2_8 -74.4(6) . . . . ? C3_8 C1_8 C2_8 F2_8 44.9(7) . . . . ? O1_8 C1_8 C2_8 F1_8 -77.5(6) . . . . ? C4_8 C1_8 C2_8 F1_8 43.6(6) . . . . ? C3_8 C1_8 C2_8 F1_8 162.9(5) . . . . ? O1_8 C1_8 C3_8 F4_8 40.1(7) . . . . ? C4_8 C1_8 C3_8 F4_8 -82.4(6) . . . . ? C2_8 C1_8 C3_8 F4_8 157.9(5) . . . . ? O1_8 C1_8 C3_8 F6_8 164.9(6) . . . . ? C4_8 C1_8 C3_8 F6_8 42.3(7) . . . . ? C2_8 C1_8 C3_8 F6_8 -77.4(7) . . . . ? O1_8 C1_8 C3_8 F5_8 -76.2(6) . . . . ? C4_8 C1_8 C3_8 F5_8 161.2(5) . . . . ? C2_8 C1_8 C3_8 F5_8 41.5(6) . . . . ? O1_8 C1_8 C4_8 F9_8 41.1(8) . . . . ? C2_8 C1_8 C4_8 F9_8 -77.7(7) . . . . ? C3_8 C1_8 C4_8 F9_8 163.2(6) . . . . ? O1_8 C1_8 C4_8 F8_8 164.4(6) . . . . ? C2_8 C1_8 C4_8 F8_8 45.5(7) . . . . ? C3_8 C1_8 C4_8 F8_8 -73.5(7) . . . . ? O1_8 C1_8 C4_8 F7_8 -76.1(7) . . . . ? C2_8 C1_8 C4_8 F7_8 165.0(5) . . . . ? C3_8 C1_8 C4_8 F7_8 45.9(6) . . . . ? O1_5 Al1 O1_9 C1_9 -35(10) . . . . ? O1_6 Al1 O1_9 C1_9 91(10) . . . . ? F1 Al1 O1_9 C1_9 -149(9) . . . . ? Al1 O1_9 C1_9 C2_9 154(9) . . . . ? Al1 O1_9 C1_9 C4_9 33(10) . . . . ? Al1 O1_9 C1_9 C3_9 -86(10) . . . . ? O1_9 C1_9 C2_9 F3_9 43(2) . . . . ? C4_9 C1_9 C2_9 F3_9 164.2(18) . . . . ? C3_9 C1_9 C2_9 F3_9 -79.2(19) . . . . ? O1_9 C1_9 C2_9 F1_9 -80(2) . . . . ? C4_9 C1_9 C2_9 F1_9 41.6(19) . . . . ? C3_9 C1_9 C2_9 F1_9 158.1(17) . . . . ? O1_9 C1_9 C2_9 F2_9 160(2) . . . . ? C4_9 C1_9 C2_9 F2_9 -78(2) . . . . ? C3_9 C1_9 C2_9 F2_9 38(2) . . . . ? O1_9 C1_9 C3_9 F4_9 43(2) . . . . ? C2_9 C1_9 C3_9 F4_9 165(2) . . . . ? C4_9 C1_9 C3_9 F4_9 -78(2) . . . . ? O1_9 C1_9 C3_9 F6_9 160(2) . . . . ? C2_9 C1_9 C3_9 F6_9 -77(2) . . . . ? C4_9 C1_9 C3_9 F6_9 40(2) . . . . ? O1_9 C1_9 C3_9 F5_9 -79(2) . . . . ? C2_9 C1_9 C3_9 F5_9 43(2) . . . . ? C4_9 C1_9 C3_9 F5_9 160.1(19) . . . . ? O1_9 C1_9 C4_9 F9_9 44(2) . . . . ? C2_9 C1_9 C4_9 F9_9 -78.2(19) . . . . ? C3_9 C1_9 C4_9 F9_9 165.6(18) . . . . ? O1_9 C1_9 C4_9 F8_9 164(2) . . . . ? C2_9 C1_9 C4_9 F8_9 41(2) . . . . ? C3_9 C1_9 C4_9 F8_9 -75(2) . . . . ? O1_9 C1_9 C4_9 F7_9 -79(2) . . . . ? C2_9 C1_9 C4_9 F7_9 158.8(19) . . . . ? C3_9 C1_9 C4_9 F7_9 43(2) . . . . ? _shelx_res_file ; TITL p-1_a.res in P-1 p-1_a.res created by SHELXL-2018/3 at 08:56:41 on 14-Feb-2022 REM Old TITL p-1 in P-1 REM SHELXT solution in P-1: R1 0.080, Rweak 0.005, Alpha 0.058 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C74 O20 F116 Al4 Os3 CELL 0.71073 11.8104 12.9390 19.5072 102.689 103.941 92.667 ZERR 1.000 0.0039 0.0024 0.0047 0.009 0.014 0.009 LATT 1 SFAC C O F AL OS H UNIT 68 26 114 4 3 2 SIMU 0.02 0.04 2 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 RIGU 0.002 0.002 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 REM Restraints for Fragment tetfluorbenz, 1,2,3,4-Tetrafluorobenzene, REM C6H2F4 from: CCDC ZELDOJ, http://dx.doi.org/10.1002/anie.199515171. REM Please cite https://doi.org/10.1107/S1600576718004508 REM HFIX_TFB 43 C5 C6 SIMU_TFB F1 > C6 RIGU_TFB F1 > C6 FLAT_TFB F1 > C6 SADI_TFB 0.02 C1 C2 C2 C3 C3 C4 C4 C5 C5 C6 C6 C1 SADI_TFB 0.02 C1 F1 C2 F2 C3 F3 C4 F4 SADI_TFB 0.04 C1 C3 C3 C5 C5 C1 C2 C6 C6 C4 C2 C4 SADI_TFB 0.05 C2 F1 C6 F1 C1 F2 C3 F2 C2 F3 C4 F3 C3 F4 C5 F4 SAME_TFB F1 > C6 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 TEMP -173.150 SIZE 0.071 0.08 0.103 L.S. 10 OMIT 11 4 14 BOND $H CONF MORE -1 LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.043400 6.952300 FVAR 0.22054 0.82759 OS1 5 0.049613 0.582520 0.656695 11.00000 0.01618 0.01732 = 0.01442 0.00262 0.00478 0.00172 OS2 5 0.000000 0.500000 0.500000 10.50000 0.01433 0.01519 = 0.01424 0.00287 0.00443 0.00095 AL1 4 0.591046 0.304583 0.783862 11.00000 0.01681 0.01830 = 0.01643 0.00458 0.00573 0.00323 AL2 4 0.666385 0.049839 0.803800 11.00000 0.01620 0.01682 = 0.01646 0.00427 0.00356 0.00152 F1 3 0.623904 0.175907 0.793685 11.00000 0.02285 0.01870 = 0.02185 0.00646 0.00670 0.00468 O2 2 -0.007373 0.351752 0.671268 11.00000 0.03037 0.02419 = 0.03394 0.01031 0.00971 0.00264 C1 1 0.085657 0.644270 0.763154 11.00000 0.02288 0.01804 = 0.01285 0.00184 0.00481 0.00383 C2 1 0.012579 0.434879 0.665872 11.00000 0.02144 0.02123 = 0.01894 0.00488 0.00742 -0.00048 O1 2 0.106857 0.678770 0.822462 11.00000 0.03586 0.03000 = 0.01931 0.00369 0.00334 -0.00008 O3 2 0.303409 0.530193 0.654699 11.00000 0.01881 0.02994 = 0.02901 0.00962 0.00560 0.00434 O4 2 0.096367 0.801470 0.622363 11.00000 0.02494 0.02077 = 0.03129 0.00607 0.00751 0.00138 O5 2 -0.216412 0.613718 0.624268 11.00000 0.01973 0.03442 = 0.03125 0.00653 0.00836 0.00513 O6 2 -0.230746 0.375902 0.498376 11.00000 0.02317 0.03324 = 0.02825 0.00635 0.00856 -0.00526 O7 2 0.138185 0.307586 0.521727 11.00000 0.02441 0.02587 = 0.03784 0.01000 0.00870 0.00729 C3 1 0.213070 0.550672 0.657469 11.00000 0.02141 0.02120 = 0.01507 0.00310 0.00292 -0.00071 C4 1 0.081236 0.722559 0.635944 11.00000 0.02277 0.01709 = 0.01834 0.00006 0.00665 0.00239 C5 1 -0.120757 0.602944 0.637627 11.00000 0.01895 0.02453 = 0.01871 0.00213 0.00605 0.00499 C6 1 -0.145564 0.419651 0.499657 11.00000 0.01753 0.01892 = 0.01743 0.00457 0.00569 0.00016 C7 1 0.087343 0.377903 0.514720 11.00000 0.01622 0.01727 = 0.02064 0.00550 0.00467 0.00120 RESI CCF3 1 O1 2 0.547614 -0.036753 0.753314 11.00000 0.03339 0.03272 = 0.02146 0.00882 0.00060 -0.01275 C1 1 0.466670 -0.117438 0.748718 11.00000 0.02130 0.02115 = 0.02282 0.00383 0.00428 -0.00296 C2 1 0.510964 -0.184008 0.805081 11.00000 0.03433 0.02760 = 0.03741 0.01348 0.00131 0.00064 F1 3 0.501897 -0.135665 0.870661 11.00000 0.04507 0.04461 = 0.02907 0.01633 0.00691 -0.00715 F2 3 0.448123 -0.279995 0.785833 11.00000 0.06596 0.02835 = 0.05468 0.01998 -0.00201 -0.01087 F3 3 0.622180 -0.198480 0.809649 11.00000 0.03837 0.04540 = 0.05265 0.01769 0.00149 0.01474 C3 1 0.438995 -0.189266 0.670188 11.00000 0.02827 0.02402 = 0.03016 0.00029 0.00795 -0.00180 F4 3 0.431068 -0.131359 0.621184 11.00000 0.03804 0.04299 = 0.02457 0.00557 0.00516 -0.01076 F5 3 0.523948 -0.251681 0.663334 11.00000 0.03771 0.04849 = 0.04361 -0.00644 0.01200 0.01415 F6 3 0.337880 -0.251806 0.652481 11.00000 0.02838 0.02627 = 0.03776 -0.00477 0.00521 -0.00879 C4 1 0.352690 -0.070369 0.762255 11.00000 0.02971 0.02948 = 0.02659 0.00017 0.00292 0.00069 F7 3 0.296386 -0.035187 0.705098 11.00000 0.03686 0.03162 = 0.03675 0.00158 -0.00465 0.00929 F8 3 0.277750 -0.142665 0.771936 11.00000 0.02902 0.05511 = 0.04294 0.00926 0.01558 -0.00278 F9 3 0.377965 0.010993 0.819806 11.00000 0.05137 0.04115 = 0.03551 -0.00844 0.00400 0.01326 RESI 0 RESI CCF3 2 O1 2 0.691947 0.045404 0.892455 11.00000 0.02356 0.02654 = 0.01573 0.00476 -0.00002 -0.00143 C1 1 0.742989 0.095608 0.963186 11.00000 0.02125 0.03153 = 0.01415 0.00771 0.00383 0.00322 C2 1 0.863868 0.155064 0.969922 11.00000 0.02159 0.03289 = 0.02132 0.00182 0.00395 -0.00016 F1 3 0.945518 0.088199 0.966266 11.00000 0.02041 0.04936 = 0.04538 0.00833 0.00889 0.00976 F2 3 0.901059 0.230662 1.030939 11.00000 0.02814 0.05367 = 0.02744 -0.00755 0.00694 -0.00928 F3 3 0.855245 0.201493 0.913941 11.00000 0.04116 0.03345 = 0.02955 0.00652 0.01344 -0.00755 C3 1 0.661278 0.177081 0.990187 11.00000 0.02377 0.04406 = 0.02754 0.00103 0.00560 0.00447 F4 3 0.551021 0.132767 0.969883 11.00000 0.01945 0.06646 = 0.04908 -0.00186 0.01027 0.00800 F5 3 0.665182 0.261155 0.962030 11.00000 0.04831 0.03894 = 0.05085 0.00510 0.01266 0.01896 F6 3 0.690575 0.211468 1.062388 11.00000 0.04096 0.07524 = 0.02890 -0.01077 0.01542 0.00151 C4 1 0.760084 0.011419 1.009315 11.00000 0.03049 0.05132 = 0.03114 0.02326 0.00206 0.00075 F7 3 0.658432 -0.021680 1.019368 11.00000 0.04526 0.07441 = 0.04120 0.03150 0.00914 -0.01143 F8 3 0.834236 0.051060 1.074483 11.00000 0.04798 0.08038 = 0.03415 0.03186 -0.00924 -0.00153 F9 3 0.801539 -0.073270 0.975601 11.00000 0.05168 0.04593 = 0.05869 0.03162 0.00248 0.01394 RESI 0 RESI CCF3 3 O1 2 0.781680 0.041446 0.764566 11.00000 0.02105 0.02279 = 0.02422 0.00633 0.01083 0.00706 C1 1 0.859482 -0.015023 0.735687 11.00000 0.02291 0.02462 = 0.02337 0.00551 0.00989 0.00813 C2 1 0.974034 0.060366 0.750787 11.00000 0.02341 0.03178 = 0.03584 0.01085 0.01238 0.00739 F1 3 1.033252 0.077050 0.820639 11.00000 0.02887 0.05170 = 0.04209 0.00235 -0.00005 0.00361 F2 3 1.045506 0.019443 0.711021 11.00000 0.02692 0.05056 = 0.05479 0.01175 0.02128 0.00975 F3 3 0.949681 0.153875 0.738096 11.00000 0.03095 0.03617 = 0.07013 0.02416 0.01684 0.00399 C3 1 0.807363 -0.058203 0.652095 11.00000 0.03048 0.03507 = 0.02498 0.00847 0.01080 0.01014 F4 3 0.697604 -0.097617 0.637178 11.00000 0.03319 0.05504 = 0.02941 -0.00077 0.00588 -0.00290 F5 3 0.812650 0.020105 0.617857 11.00000 0.05291 0.05268 = 0.02993 0.01898 0.01582 0.01506 F6 3 0.868410 -0.133309 0.623299 11.00000 0.04265 0.05119 = 0.02991 -0.00274 0.01434 0.01937 C4 1 0.889556 -0.110328 0.771084 11.00000 0.03768 0.02664 = 0.02800 0.00755 0.01378 0.01392 F7 3 0.803978 -0.191707 0.741353 11.00000 0.06128 0.02728 = 0.05182 0.01095 0.01631 0.00457 F8 3 0.986996 -0.150145 0.758907 11.00000 0.05874 0.04797 = 0.05040 0.02263 0.02934 0.03775 F9 3 0.899647 -0.085500 0.841334 11.00000 0.06296 0.04378 = 0.03042 0.01649 0.01578 0.02857 RESI 0 RESI CCF3 4 RESI 0 RESI CCF3 5 O1 2 0.489493 0.336592 0.831622 11.00000 0.02231 0.04414 = 0.02186 0.00947 0.00922 0.01191 C1 1 0.376993 0.351171 0.831103 11.00000 0.02089 0.02541 = 0.01718 0.00618 0.00536 0.00689 C2 1 0.360784 0.471316 0.837346 11.00000 0.04230 0.02547 = 0.03288 0.00231 -0.00298 0.00999 F1 3 0.404947 0.528652 0.904928 11.00000 0.06700 0.02957 = 0.03772 -0.00510 -0.00302 0.00942 F2 3 0.248493 0.487701 0.816417 11.00000 0.05540 0.04559 = 0.05844 -0.00109 -0.00914 0.03393 F3 3 0.416674 0.508641 0.794673 11.00000 0.07225 0.03486 = 0.04283 0.01834 -0.00673 -0.01123 C3 1 0.289286 0.284751 0.760422 11.00000 0.02377 0.02186 = 0.02525 0.00548 0.00861 0.00069 F4 3 0.325627 0.189305 0.741148 11.00000 0.06137 0.02122 = 0.02806 0.00247 0.01132 0.00667 F5 3 0.283768 0.330884 0.704526 11.00000 0.02854 0.02955 = 0.02462 0.01097 0.00306 0.00225 F6 3 0.181483 0.271066 0.767380 11.00000 0.02434 0.06118 = 0.03538 0.00395 0.00858 -0.01056 C4 1 0.349740 0.317679 0.897664 11.00000 0.03243 0.04055 = 0.02140 0.00524 0.01254 0.00459 F7 3 0.337371 0.212304 0.886017 11.00000 0.08643 0.03900 = 0.03460 0.01637 0.02044 -0.00323 F8 3 0.251373 0.354040 0.910841 11.00000 0.03172 0.08848 = 0.03578 0.00359 0.02235 0.00769 F9 3 0.436120 0.355139 0.957204 11.00000 0.03885 0.05645 = 0.01874 0.00787 0.01004 0.01084 RESI 0 RESI CCF3 6 O1 2 0.533412 0.296237 0.693017 11.00000 0.02296 0.02632 = 0.01417 0.00530 0.00698 0.00416 C1 1 0.546309 0.263413 0.624338 11.00000 0.02109 0.03002 = 0.01485 0.00408 0.00614 0.00517 C2 1 0.495383 0.344415 0.579933 11.00000 0.01987 0.04148 = 0.02277 0.01387 0.00599 0.00658 F1 3 0.378314 0.333856 0.563647 11.00000 0.02251 0.07223 = 0.03417 0.01776 0.00481 0.01770 F2 3 0.526870 0.331990 0.517662 11.00000 0.03920 0.06512 = 0.02560 0.02591 0.01571 0.02058 F3 3 0.529812 0.444086 0.617680 11.00000 0.04464 0.03610 = 0.04117 0.01739 0.00977 0.01181 C3 1 0.678067 0.259326 0.625271 11.00000 0.02590 0.03901 = 0.02306 0.00946 0.00976 0.00867 F4 3 0.732626 0.220031 0.679974 11.00000 0.03158 0.05661 = 0.02905 0.02069 0.00956 0.02188 F5 3 0.731183 0.357983 0.635689 11.00000 0.02462 0.04543 = 0.03568 0.01261 0.00903 -0.00044 F6 3 0.693021 0.200320 0.563756 11.00000 0.03678 0.05084 = 0.02976 0.01135 0.01838 0.01845 C4 1 0.478307 0.151976 0.588532 11.00000 0.03952 0.03326 = 0.02112 0.00051 0.01271 -0.00168 F7 3 0.538045 0.078825 0.617156 11.00000 0.07307 0.02780 = 0.04388 0.00683 0.01697 0.00348 F8 3 0.464484 0.124456 0.516916 11.00000 0.05210 0.05191 = 0.02104 -0.00617 0.00701 -0.00288 F9 3 0.373524 0.147111 0.601009 11.00000 0.03732 0.05654 = 0.04371 -0.00762 0.01624 -0.02241 RESI 0 RESI TFB 7 PART -1 10.5 F1 3 -0.060750 0.195970 0.545010 10.50000 0.02843 0.02447 = 0.05218 0.00081 0.00966 0.00354 F2 3 -0.201503 0.042189 0.437859 10.50000 0.02162 0.03550 = 0.05255 0.02394 0.00140 0.00187 F3 3 -0.126138 -0.152711 0.398299 10.50000 0.03339 0.02965 = 0.02560 0.00201 -0.00507 -0.00688 F4 3 0.087760 -0.193359 0.468564 10.50000 0.02626 0.02762 = 0.04126 0.01159 0.00987 0.01047 C1 1 -0.021675 0.100256 0.525464 10.50000 0.02889 0.01649 = 0.02650 0.00733 0.01176 -0.00002 C2 1 -0.095061 0.022701 0.471466 10.50000 0.01927 0.02405 = 0.02927 0.01477 0.00451 0.00115 C3 1 -0.056662 -0.077015 0.451580 10.50000 0.02044 0.02140 = 0.01860 0.00563 0.00114 -0.00349 C4 1 0.053542 -0.095187 0.487600 10.50000 0.01597 0.02393 = 0.02898 0.00680 0.00590 0.00319 C5 1 0.127234 -0.017347 0.541574 10.50000 0.02306 0.03513 = 0.02341 0.01003 0.00051 -0.00003 AFIX 43 H5 6 0.203334 -0.031526 0.564812 10.50000 -1.20000 AFIX 0 C6 1 0.089419 0.082121 0.561788 10.50000 0.03041 0.02982 = 0.01716 0.00821 0.00667 -0.00408 AFIX 43 H6 6 0.138347 0.136566 0.599588 10.50000 -1.20000 PART 0 RESI 0 AFIX 0 RESI CCF3 8 PART 1 21 O1 2 0.725208 0.377750 0.821526 21.00000 0.01639 0.02591 = 0.02375 0.00199 0.00259 -0.00214 C1 1 0.792036 0.472062 0.854737 21.00000 0.02403 0.02322 = 0.02154 0.00451 0.00607 -0.00349 C2 1 0.922534 0.448639 0.871951 21.00000 0.02495 0.03143 = 0.03974 0.00920 0.00050 -0.00284 F1 3 0.946220 0.407391 0.931039 21.00000 0.05527 0.04338 = 0.05665 0.02758 -0.01592 -0.00756 F2 3 0.996642 0.536283 0.887836 21.00000 0.02281 0.03923 = 0.05599 0.01494 0.00657 -0.00679 F3 3 0.943636 0.378316 0.819515 21.00000 0.02890 0.05599 = 0.06526 -0.00422 0.00684 0.01308 C3 1 0.775054 0.549636 0.803130 21.00000 0.03044 0.03380 = 0.03662 0.01545 0.00635 0.00197 F4 3 0.663956 0.543409 0.766751 21.00000 0.03706 0.04752 = 0.05106 0.02034 -0.00349 0.00891 F5 3 0.836085 0.519263 0.751837 21.00000 0.05390 0.06547 = 0.03668 0.02593 0.02071 0.00880 F6 3 0.814667 0.649710 0.837099 21.00000 0.04513 0.02859 = 0.05714 0.01750 0.00686 0.00355 C4 1 0.760351 0.525194 0.926125 21.00000 0.04415 0.04447 = 0.03317 -0.00805 0.02124 -0.01942 F7 3 0.656891 0.568597 0.907927 21.00000 0.04205 0.06568 = 0.06658 -0.02175 0.03271 -0.00391 F8 3 0.842194 0.602287 0.968148 21.00000 0.05104 0.04381 = 0.03461 -0.01013 0.01027 -0.01542 F9 3 0.743052 0.456325 0.962650 21.00000 0.11056 0.06668 = 0.02890 -0.00127 0.03114 -0.03991 PART 0 RESI 0 RESI CCF3 9 PART 2 -21 O1 2 0.709527 0.384510 0.819926 -21.00000 0.03251 0.03056 = 0.02504 0.00274 0.00243 -0.00978 C1 1 0.782416 0.474200 0.854411 -21.00000 0.02969 0.03132 = 0.02898 0.00234 0.00856 -0.01090 C2 1 0.905236 0.449374 0.892916 -21.00000 0.03242 0.03984 = 0.04490 0.00860 0.00003 -0.01039 F1 3 0.895371 0.427497 0.955627 -21.00000 0.05802 0.03958 = 0.04302 0.01071 -0.00491 -0.01771 F2 3 0.984367 0.534337 0.906009 -21.00000 0.03564 0.05124 = 0.03904 0.01537 -0.01015 -0.01950 F3 3 0.943139 0.369753 0.851756 -21.00000 0.02886 0.05254 = 0.05633 0.00538 0.00135 -0.00318 C3 1 0.799488 0.541322 0.799706 -21.00000 0.04449 0.04252 = 0.03793 0.01154 0.01756 -0.00835 F4 3 0.697100 0.542497 0.754315 -21.00000 0.05246 0.05257 = 0.03640 0.01705 0.01132 -0.01481 F5 3 0.878022 0.494858 0.766536 -21.00000 0.06135 0.05877 = 0.06006 -0.00073 0.04062 -0.01575 F6 3 0.838602 0.642197 0.833327 -21.00000 0.03250 0.03884 = 0.05011 0.01696 0.01748 -0.00490 C4 1 0.729994 0.544064 0.912448 -21.00000 0.04329 0.03585 = 0.03821 -0.00028 0.01768 -0.00787 F7 3 0.647369 0.593792 0.875678 -21.00000 0.07763 0.05677 = 0.06648 0.00632 0.01369 0.02344 F8 3 0.810629 0.617294 0.959802 -21.00000 0.06307 0.03622 = 0.03247 -0.00430 0.02594 -0.01861 F9 3 0.688758 0.484958 0.949924 -21.00000 0.04598 0.02742 = 0.03979 -0.00901 0.02477 -0.01042 PART 0 RESI 0 HKLF 4 REM p-1_a.res in P-1 REM wR2 = 0.1020, GooF = S = 1.003, Restrained GooF = 0.919 for all data REM R1 = 0.0415 for 14185 Fo > 4sig(Fo) and 0.0672 for all 19196 data REM 1142 parameters refined using 8318 restraints END WGHT 0.0439 5.8686 REM Highest difference peak 2.002, deepest hole -2.129, 1-sigma level 0.177 Q1 1 -0.0116 0.4426 0.4636 11.00000 0.05 2.00 Q2 1 0.0573 0.6397 0.7033 11.00000 0.05 1.85 Q3 1 -0.1016 0.5072 0.4904 11.00000 0.05 1.83 Q4 1 -0.0624 0.4293 0.4793 11.00000 0.05 1.79 Q5 1 -0.0472 0.5701 0.6631 11.00000 0.05 1.77 Q6 1 0.1572 0.5790 0.6653 11.00000 0.05 1.56 Q7 1 -0.0187 0.5084 0.6320 11.00000 0.05 1.56 Q8 1 0.0393 0.5226 0.6108 11.00000 0.05 1.53 Q9 1 0.1138 0.6501 0.6714 11.00000 0.05 1.47 Q10 1 0.1404 0.6009 0.6524 11.00000 0.05 1.43 Q11 1 -0.0822 0.4709 0.5123 11.00000 0.05 1.32 Q12 1 0.0398 0.4796 0.4500 11.00000 0.05 1.28 Q13 1 0.7994 -0.1403 0.7913 11.00000 0.05 1.11 Q14 1 0.9319 0.4590 0.7874 11.00000 0.05 1.07 Q15 1 0.0793 0.5531 0.6014 11.00000 0.05 1.07 Q16 1 -0.0214 0.5163 0.4401 11.00000 0.05 1.05 Q17 1 -0.0437 0.5998 0.6186 11.00000 0.05 1.01 Q18 1 0.9789 -0.0606 0.8327 11.00000 0.05 1.00 Q19 1 0.6595 0.6006 0.8396 11.00000 0.05 0.99 Q20 1 0.0582 0.4292 0.4843 11.00000 0.05 0.99 ; _shelx_res_checksum 89467 _shelx_hkl_file ; -1 0 0 752.32 29.70 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485.75 34.30 3 -9 9 522.85 28.30 -4 9 -9 124.59 15.20 -4 9 -9 147.49 14.60 -4 9 -9 154.58 20.00 4 -9 9 166.18 16.10 4 -9 9 106.19 14.80 4 -9 9 122.09 14.70 4 -9 9 154.68 16.70 4 -9 9 139.19 17.70 -5 9 -9 480.55 27.60 -5 9 -9 433.76 24.80 -5 9 -9 424.86 31.80 5 -9 9 449.76 28.30 5 -9 9 429.86 29.50 5 -9 9 470.85 31.80 5 -9 9 488.85 27.70 5 -9 9 471.65 25.80 -6 9 -9 584.64 37.70 -6 9 -9 561.24 31.10 -6 9 -9 585.34 29.70 6 -9 9 621.44 37.70 6 -9 9 515.25 34.40 6 -9 9 580.74 31.30 6 -9 9 557.44 33.70 6 -9 9 582.14 29.60 -7 9 -9 412.76 33.60 -7 9 -9 463.35 25.80 -7 9 -9 462.25 27.00 7 -9 9 498.95 27.30 7 -9 9 453.45 31.80 7 -9 9 455.45 31.10 7 -9 9 475.05 25.80 7 -9 9 493.55 34.90 -8 9 -9 824.62 38.10 -8 9 -9 764.62 47.30 8 -9 9 769.12 43.60 8 -9 9 780.92 48.70 8 -9 9 713.63 43.50 8 -9 9 731.43 36.40 8 -9 9 753.72 37.10 -9 9 -9 155.28 21.60 9 -9 9 179.48 21.90 9 -9 9 204.08 25.10 9 -9 9 160.98 24.40 -10 9 -9 143.09 21.80 10 -9 9 187.58 27.60 10 -9 9 176.88 23.60 10 -9 9 155.18 25.80 -11 9 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10.50 6.90 3 8 -9 11.10 7.40 -3 -8 9 9.40 6.50 -3 -8 9 12.00 8.30 2 8 -9 10.00 6.70 2 8 -9 22.50 7.70 2 8 -9 21.50 9.70 -2 -8 9 26.30 7.50 -2 -8 9 35.30 12.00 1 8 -9 -3.70 6.10 1 8 -9 3.80 6.50 1 8 -9 17.40 9.00 -1 -8 9 7.90 7.20 -1 -8 9 2.60 6.00 0 8 -9 284.77 20.10 0 8 -9 277.17 20.80 0 8 -9 324.97 22.30 0 -8 9 306.97 22.00 0 -8 9 290.37 21.00 0 -8 9 306.37 20.70 -1 8 -9 462.75 25.20 -1 8 -9 450.05 27.10 -1 8 -9 430.56 26.50 1 -8 9 399.36 25.70 1 -8 9 434.86 25.70 1 -8 9 427.36 26.70 -2 8 -9 40.00 9.20 -2 8 -9 15.30 7.10 -2 8 -9 33.70 9.80 2 -8 9 43.40 8.90 2 -8 9 40.20 10.90 2 -8 9 37.00 9.00 2 -8 9 24.00 8.40 2 -8 9 38.80 10.20 -3 8 -9 1057.39 48.30 -3 8 -9 1047.00 47.00 -3 8 -9 1050.19 51.59 3 -8 9 1018.70 47.60 3 -8 9 956.10 49.00 3 -8 9 1021.80 47.70 3 -8 9 1076.89 49.00 3 -8 9 1085.29 50.89 -4 8 -9 581.74 34.30 -4 8 -9 517.35 27.70 -4 8 -9 504.85 28.70 4 -8 9 538.55 29.20 4 -8 9 541.95 28.70 4 -8 9 530.45 32.20 4 -8 9 517.55 31.60 4 -8 9 511.05 29.50 -5 8 -9 511.75 28.10 -5 8 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17.30 15 7 -9 96.29 17.00 15 7 -9 109.19 24.60 14 7 -9 108.89 24.70 14 7 -9 65.39 13.80 14 7 -9 115.39 20.50 13 7 -9 38.90 11.50 13 7 -9 67.29 15.80 13 7 -9 54.19 10.70 13 7 -9 79.79 20.00 12 7 -9 38.50 14.20 12 7 -9 19.40 12.30 12 7 -9 30.30 10.50 12 7 -9 39.20 16.40 12 7 -9 34.00 9.10 11 7 -9 13.30 7.90 11 7 -9 15.30 12.10 11 7 -9 28.20 8.70 11 7 -9 36.60 13.70 11 7 -9 13.70 12.20 11 7 -9 27.20 8.90 10 7 -9 32.90 13.60 10 7 -9 28.00 11.10 10 7 -9 35.00 8.90 10 7 -9 31.40 7.70 10 7 -9 40.40 12.10 9 7 -9 29.50 11.50 9 7 -9 28.80 11.00 9 7 -9 27.50 12.10 9 7 -9 29.60 7.70 8 7 -9 55.99 12.20 8 7 -9 49.10 12.30 8 7 -9 87.79 11.10 7 7 -9 66.19 10.00 7 7 -9 70.69 15.50 7 7 -9 89.19 16.00 6 7 -9 100.69 11.40 6 7 -9 71.69 13.40 -6 -7 9 97.69 12.00 5 7 -9 43.00 10.20 5 7 -9 65.49 9.70 5 7 -9 34.80 10.00 -5 -7 9 58.99 13.90 -5 -7 9 71.49 10.30 4 7 -9 53.09 9.10 4 7 -9 59.99 12.00 4 7 -9 76.79 12.50 -4 -7 9 76.39 13.40 -4 -7 9 66.19 10.60 3 7 -9 139.09 15.90 3 7 -9 165.78 13.90 3 7 -9 139.29 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12.80 3 12 -22 46.40 16.10 2 12 -22 19.30 13.00 2 12 -22 11.20 12.30 -2 -12 22 -7.00 10.00 1 12 -22 14.10 11.60 1 12 -22 42.70 14.40 -1 -12 22 29.90 12.50 0 12 -22 22.80 13.50 0 12 -22 13.70 25.50 0 -12 22 -10.70 11.50 -1 12 -22 24.80 13.10 -1 12 -22 -12.90 9.30 1 -12 22 -18.70 9.50 -2 12 -22 39.60 15.70 -2 12 -22 10.60 11.60 2 -12 22 35.00 16.30 -3 12 -22 0.30 9.70 -3 12 -22 50.29 18.20 3 -12 22 3.30 12.10 -4 12 -22 -9.00 9.40 4 -12 22 -7.60 13.90 -5 12 -22 -3.70 5.80 5 -12 22 -0.40 8.40 5 -12 22 4.30 12.80 11 11 -22 128.39 20.10 10 11 -22 148.49 21.80 9 11 -22 103.29 18.90 9 11 -22 47.50 17.90 8 11 -22 146.49 23.10 8 11 -22 177.08 23.10 7 11 -22 11.60 12.40 7 11 -22 6.00 11.40 6 11 -22 21.40 12.30 6 11 -22 29.60 12.70 5 11 -22 -3.00 10.00 5 11 -22 -1.70 8.60 4 11 -22 -7.70 10.30 4 11 -22 -8.10 9.40 3 11 -22 48.10 14.60 3 11 -22 29.30 13.70 -3 -11 22 52.49 15.70 2 11 -22 5.00 11.50 2 11 -22 -0.10 10.10 -2 -11 22 10.10 12.30 1 11 -22 -2.20 10.50 1 11 -22 11.60 11.40 -1 -11 22 -6.60 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16.80 2 10 -22 30.10 12.30 2 10 -22 17.40 12.10 2 10 -22 26.70 16.80 -2 -10 22 9.00 12.60 1 10 -22 85.49 20.20 1 10 -22 86.89 18.90 1 10 -22 79.59 15.80 -1 -10 22 99.09 21.00 0 10 -22 23.80 12.60 0 10 -22 1.00 9.20 0 10 -22 22.10 12.60 0 -10 22 1.40 11.70 -1 10 -22 33.60 15.40 -1 10 -22 3.50 12.70 -1 10 -22 10.40 10.60 1 -10 22 13.80 12.40 -2 10 -22 11.20 15.70 -2 10 -22 29.20 22.60 -2 10 -22 -8.20 17.80 2 -10 22 -21.40 8.40 -3 10 -22 29.60 15.70 -3 10 -22 17.20 10.40 -3 10 -22 28.70 11.80 3 -10 22 11.60 12.90 -4 10 -22 30.50 16.60 -4 10 -22 51.69 11.90 4 -10 22 62.39 17.80 5 -10 22 82.29 16.10 5 -10 22 99.19 19.50 5 -10 22 72.59 18.60 6 -10 22 83.69 17.40 6 -10 22 107.59 21.90 6 -10 22 96.49 20.80 12 9 -22 93.49 18.80 11 9 -22 20.00 13.20 10 9 -22 151.78 23.20 10 9 -22 135.09 23.30 9 9 -22 10.30 14.40 9 9 -22 9.20 11.40 8 9 -22 -3.40 9.50 8 9 -22 10.10 13.10 -8 -9 22 -11.60 11.70 7 9 -22 17.80 12.70 7 9 -22 -3.60 9.30 -7 -9 22 21.60 15.00 6 9 -22 -3.00 9.10 6 9 -22 0.20 11.00 -6 -9 22 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20.70 -1 8 -22 177.78 23.70 -1 8 -22 171.48 24.40 -1 8 -22 217.18 23.00 -1 8 -22 204.48 23.40 1 -8 22 236.88 30.00 -2 8 -22 194.18 21.10 -2 8 -22 167.48 25.30 -2 8 -22 194.58 28.30 2 -8 22 144.29 22.90 -3 8 -22 111.19 21.80 -3 8 -22 134.19 16.70 -3 8 -22 103.69 29.50 3 -8 22 99.59 20.90 -4 8 -22 270.07 31.40 4 -8 22 255.67 29.80 4 -8 22 313.87 24.30 -5 8 -22 135.19 21.70 5 -8 22 96.69 16.90 5 -8 22 118.39 22.30 -6 8 -22 114.99 24.40 6 -8 22 111.89 19.00 6 -8 22 108.09 21.00 7 -8 22 54.89 17.30 13 7 -22 20.20 14.80 12 7 -22 15.40 11.10 11 7 -22 -14.30 9.80 11 7 -22 -1.80 10.30 10 7 -22 19.00 12.10 10 7 -22 32.30 14.90 9 7 -22 5.00 11.00 9 7 -22 -6.60 9.50 8 7 -22 22.50 14.30 8 7 -22 24.60 12.10 -8 -7 22 44.00 17.30 7 7 -22 60.09 26.40 7 7 -22 48.50 16.00 7 7 -22 39.80 13.40 -7 -7 22 27.80 15.60 -7 -7 22 42.60 16.10 6 7 -22 36.50 13.20 6 7 -22 13.40 14.80 6 7 -22 20.60 11.60 6 7 -22 25.60 14.60 -6 -7 22 38.00 15.70 -6 -7 22 41.50 16.30 5 7 -22 4.50 9.50 5 7 -22 0.60 9.00 5 7 -22 -0.10 9.30 5 7 -22 15.10 10.90 -5 -7 22 -5.60 9.60 -5 -7 22 11.40 12.20 4 7 -22 16.10 12.30 4 7 -22 38.70 14.30 4 7 -22 22.30 11.50 4 7 -22 12.90 10.80 -4 -7 22 23.80 14.00 -4 -7 22 26.60 12.70 3 7 -22 8.80 11.70 3 7 -22 43.60 15.40 3 7 -22 14.80 10.80 3 7 -22 38.30 12.90 -3 -7 22 8.00 13.20 -3 -7 22 12.60 11.60 2 7 -22 3.40 9.40 2 7 -22 11.70 11.40 2 7 -22 -5.80 8.70 2 7 -22 -8.60 10.00 -2 -7 22 26.10 12.90 -2 -7 22 -16.40 9.30 1 7 -22 285.97 26.00 1 7 -22 196.58 25.80 1 7 -22 295.67 30.30 -1 -7 22 344.27 31.70 -1 -7 22 270.47 31.00 0 7 -22 146.69 24.10 0 7 -22 127.79 21.60 0 7 -22 159.98 20.70 0 7 -22 185.78 22.10 0 -7 22 86.59 19.50 0 -7 22 127.59 22.70 -1 7 -22 251.67 27.60 -1 7 -22 270.67 24.30 -1 7 -22 301.47 33.40 -1 7 -22 284.57 24.50 1 -7 22 268.67 29.70 -2 7 -22 168.98 26.20 -2 7 -22 204.78 25.30 -2 7 -22 210.48 20.50 -2 7 -22 238.98 21.20 2 -7 22 218.78 28.00 -3 7 -22 228.58 27.00 -3 7 -22 207.58 35.30 -3 7 -22 244.68 20.60 -3 7 -22 265.27 20.90 3 -7 22 302.67 31.40 -4 7 -22 223.98 37.20 4 -7 22 265.97 30.70 4 -7 22 251.27 23.20 -5 7 -22 167.28 26.60 5 -7 22 87.49 18.80 5 -7 22 125.89 22.30 -6 7 -22 58.99 17.30 6 -7 22 30.30 16.20 6 -7 22 54.49 15.80 7 -7 22 48.70 18.70 13 6 -22 4.40 12.00 12 6 -22 -15.20 9.90 12 6 -22 6.40 11.90 11 6 -22 3.60 12.80 11 6 -22 12.50 11.40 10 6 -22 38.50 17.00 10 6 -22 16.90 11.50 9 6 -22 15.40 11.50 9 6 -22 -0.80 10.10 8 6 -22 11.40 13.00 8 6 -22 21.90 11.00 -8 -6 22 4.80 11.80 -8 -6 22 4.50 12.10 7 6 -22 21.50 19.30 7 6 -22 6.00 9.70 7 6 -22 36.60 16.40 7 6 -22 25.60 12.90 -7 -6 22 16.00 11.60 -7 -6 22 21.60 13.00 6 6 -22 -10.00 7.90 6 6 -22 -12.00 8.00 6 6 -22 -12.20 9.30 6 6 -22 2.60 10.50 -6 -6 22 3.60 11.70 -6 -6 22 1.50 12.70 5 6 -22 17.90 11.10 5 6 -22 0.70 8.70 5 6 -22 8.50 10.30 -5 -6 22 0.60 10.50 -5 -6 22 -5.10 10.40 4 6 -22 89.29 18.40 4 6 -22 53.79 14.90 4 6 -22 61.29 14.50 4 6 -22 61.49 16.10 -4 -6 22 79.39 18.00 -4 -6 22 70.79 16.80 3 6 -22 53.89 15.70 3 6 -22 29.30 11.70 3 6 -22 30.70 12.00 3 6 -22 59.99 16.40 -3 -6 22 47.60 14.70 -3 -6 22 41.80 14.50 2 6 -22 226.28 26.30 2 6 -22 211.68 25.80 2 6 -22 223.18 24.50 2 6 -22 207.08 25.10 -2 -6 22 252.77 29.40 -2 -6 22 211.08 27.60 1 6 -22 255.57 26.10 1 6 -22 234.88 26.90 1 6 -22 254.77 24.50 1 6 -22 240.88 28.40 -1 -6 22 229.58 27.50 -1 -6 22 247.78 28.70 0 6 -22 181.08 20.70 0 6 -22 226.88 28.90 0 6 -22 140.89 19.40 0 6 -22 127.59 21.70 0 -6 22 139.79 23.70 0 -6 22 151.88 23.50 -1 6 -22 337.77 34.30 -1 6 -22 318.17 40.30 -1 6 -22 325.97 30.50 -1 6 -22 369.26 26.40 1 -6 22 263.07 29.40 1 -6 22 370.86 46.50 -2 6 -22 324.27 34.30 -2 6 -22 271.87 31.10 -2 6 -22 336.07 24.00 2 -6 22 312.57 23.40 2 -6 22 304.67 32.80 -3 6 -22 224.18 19.00 -3 6 -22 195.98 25.40 -3 6 -22 269.57 20.10 3 -6 22 203.78 26.50 3 -6 22 243.58 22.10 -4 6 -22 185.48 25.80 4 -6 22 215.08 27.60 4 -6 22 194.28 22.30 -5 6 -22 34.40 14.90 5 -6 22 23.50 15.60 5 -6 22 15.40 12.80 -6 6 -22 19.70 13.40 6 -6 22 0.00 15.70 -7 6 -22 1.80 13.00 7 -6 22 -6.40 10.90 14 5 -22 -1.80 12.50 13 5 -22 -0.60 11.40 12 5 -22 1.50 10.50 12 5 -22 29.30 14.60 11 5 -22 17.10 13.70 11 5 -22 -4.00 9.70 10 5 -22 14.70 12.90 10 5 -22 -7.40 10.90 9 5 -22 5.90 11.10 9 5 -22 -9.60 12.40 -9 -5 22 3.60 11.80 8 5 -22 29.60 15.80 8 5 -22 23.50 13.00 -8 -5 22 12.20 12.60 -8 -5 22 12.00 12.60 7 5 -22 3.90 9.90 7 5 -22 -2.40 10.00 7 5 -22 1.10 8.90 7 5 -22 -1.70 8.90 -7 -5 22 -1.80 10.40 -7 -5 22 7.00 12.80 6 5 -22 38.90 14.50 6 5 -22 20.60 13.10 6 5 -22 22.30 14.50 6 5 -22 31.70 12.20 -6 -5 22 36.70 14.30 -6 -5 22 27.80 14.70 5 5 -22 12.50 10.70 5 5 -22 41.00 14.10 5 5 -22 29.80 11.40 5 5 -22 30.60 14.40 -5 -5 22 52.79 17.30 -5 -5 22 41.20 15.40 4 5 -22 188.18 25.00 4 5 -22 165.48 22.90 4 5 -22 190.18 24.30 4 5 -22 180.08 23.10 -4 -5 22 165.78 22.90 -4 -5 22 165.28 22.80 3 5 -22 282.37 30.00 3 5 -22 212.58 24.70 3 5 -22 275.97 26.10 3 5 -22 226.08 26.40 -3 -5 22 276.57 30.40 -3 -5 22 230.18 27.20 2 5 -22 447.96 31.90 2 5 -22 428.86 33.90 2 5 -22 372.26 32.30 2 5 -22 400.96 52.39 -2 -5 22 429.76 35.90 -2 -5 22 380.16 33.80 1 5 -22 346.07 27.10 1 5 -22 318.37 29.90 1 5 -22 295.07 32.30 1 5 -22 308.37 26.60 -1 -5 22 273.87 29.80 -1 -5 22 368.66 32.50 0 5 -22 587.84 41.00 0 5 -22 613.64 37.10 0 5 -22 652.03 38.00 0 5 -22 554.84 41.80 0 -5 22 539.05 41.60 0 -5 22 720.73 45.70 -1 5 -22 163.18 21.90 -1 5 -22 189.88 20.80 -1 5 -22 198.18 26.20 -1 5 -22 224.08 21.00 1 -5 22 233.48 30.50 1 -5 22 213.28 26.80 -2 5 -22 88.29 13.80 -2 5 -22 53.39 11.50 -2 5 -22 79.59 19.30 -2 5 -22 85.79 18.40 2 -5 22 98.49 21.10 2 -5 22 62.69 13.20 -3 5 -22 217.28 17.60 -3 5 -22 173.38 26.10 -3 5 -22 215.98 18.10 3 -5 22 183.78 28.20 3 -5 22 193.68 21.50 -4 5 -22 9.90 11.20 4 -5 22 13.40 14.00 4 -5 22 10.00 10.40 -5 5 -22 30.40 21.30 5 -5 22 11.20 14.10 5 -5 22 -4.20 9.80 -6 5 -22 34.00 15.20 6 -5 22 10.90 22.40 -7 5 -22 20.00 14.60 7 -5 22 9.10 12.90 14 4 -22 -2.20 11.20 13 4 -22 8.80 12.20 12 4 -22 4.40 13.10 12 4 -22 16.30 13.50 11 4 -22 14.50 16.10 11 4 -22 20.60 12.80 10 4 -22 -7.80 11.10 10 4 -22 -14.30 9.30 9 4 -22 39.60 15.20 9 4 -22 35.70 14.20 -9 -4 22 15.20 12.80 8 4 -22 0.30 11.80 8 4 -22 14.30 11.90 8 4 -22 3.40 9.90 8 4 -22 16.70 14.30 -8 -4 22 -8.20 9.50 7 4 -22 24.70 12.40 7 4 -22 38.50 12.30 7 4 -22 46.50 14.90 7 4 -22 46.00 14.50 -7 -4 22 26.00 13.50 -7 -4 22 26.90 13.20 6 4 -22 51.49 18.10 6 4 -22 24.80 11.30 6 4 -22 27.70 13.00 6 4 -22 27.80 11.50 -6 -4 22 18.00 12.30 -6 -4 22 26.90 15.30 5 4 -22 356.26 30.60 5 4 -22 344.07 30.60 5 4 -22 374.26 30.80 5 4 -22 367.56 32.50 -5 -4 22 349.57 32.70 -5 -4 22 355.76 32.50 4 4 -22 355.86 30.70 4 4 -22 278.27 29.80 4 4 -22 249.97 28.80 4 4 -22 316.27 28.00 -4 -4 22 243.28 28.00 -4 -4 22 360.16 32.10 3 4 -22 233.28 27.20 3 4 -22 305.87 26.80 3 4 -22 229.28 26.50 3 4 -22 289.07 30.20 -3 -4 22 262.67 28.80 -3 -4 22 326.67 30.50 2 4 -22 515.85 40.00 2 4 -22 595.94 38.40 2 4 -22 594.94 40.10 2 4 -22 636.54 41.20 -2 -4 22 586.04 41.50 -2 -4 22 661.43 43.80 1 4 -22 344.57 27.10 1 4 -22 289.27 30.20 1 4 -22 363.06 28.40 1 4 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400.66 35.30 1 7 -23 237.58 43.10 1 7 -23 128.79 20.00 1 7 -23 129.09 20.80 1 7 -23 173.18 21.80 -1 -7 23 102.09 20.20 0 7 -23 365.96 28.80 0 7 -23 331.17 31.80 0 7 -23 367.36 48.40 0 -7 23 327.57 34.90 -1 7 -23 225.18 27.60 -1 7 -23 287.47 24.50 -1 7 -23 284.67 24.30 1 -7 23 302.77 32.90 -2 7 -23 130.99 22.90 -2 7 -23 149.79 18.60 2 -7 23 175.08 25.80 -3 7 -23 44.70 10.90 -3 7 -23 25.60 22.50 -3 7 -23 54.69 11.50 3 -7 23 58.49 16.30 3 -7 23 32.90 11.60 -4 7 -23 53.89 17.80 4 -7 23 7.30 12.20 4 -7 23 22.90 11.30 -5 7 -23 16.50 13.70 5 -7 23 -2.90 19.30 5 -7 23 -0.20 11.40 6 -7 23 3.40 11.90 13 6 -23 0.40 11.30 12 6 -23 3.70 10.90 11 6 -23 -9.30 9.30 11 6 -23 -9.00 9.80 10 6 -23 -19.50 9.80 10 6 -23 3.50 11.20 9 6 -23 -8.70 10.20 9 6 -23 14.10 14.00 8 6 -23 16.00 12.90 8 6 -23 15.30 11.90 -8 -6 23 7.70 11.20 7 6 -23 22.60 13.10 7 6 -23 31.70 13.30 -7 -6 23 18.90 12.70 6 6 -23 90.89 19.70 6 6 -23 70.39 18.80 6 6 -23 90.49 17.00 -6 -6 23 96.39 20.80 -6 -6 23 76.19 24.00 5 6 -23 101.39 18.10 5 6 -23 90.79 17.20 5 6 -23 76.59 17.40 -5 -6 23 78.19 19.30 -5 -6 23 143.29 23.30 4 6 -23 346.57 30.90 4 6 -23 405.86 31.80 4 6 -23 344.67 37.30 -4 -6 23 248.18 31.20 -4 -6 23 325.67 35.70 3 6 -23 353.86 32.50 3 6 -23 363.06 30.90 3 6 -23 330.97 31.10 3 6 -23 357.56 30.40 -3 -6 23 361.26 39.20 -3 -6 23 429.46 35.30 2 6 -23 231.98 26.20 2 6 -23 224.48 27.50 2 6 -23 233.18 25.60 2 6 -23 230.68 27.80 -2 -6 23 265.57 48.30 -2 -6 23 264.77 31.20 1 6 -23 578.84 41.30 1 6 -23 626.94 39.10 1 6 -23 592.44 38.70 1 6 -23 628.44 43.60 -1 -6 23 553.14 42.70 0 6 -23 139.59 23.50 0 6 -23 182.18 38.70 0 6 -23 130.09 19.00 0 6 -23 137.79 18.90 0 -6 23 90.89 19.30 -1 6 -23 87.59 15.20 -1 6 -23 85.39 20.70 -1 6 -23 68.89 13.60 1 -6 23 37.20 15.40 -2 6 -23 78.49 13.20 -2 6 -23 71.99 19.10 -2 6 -23 83.19 13.80 2 -6 23 79.29 13.60 2 -6 23 78.29 18.40 -3 6 -23 22.80 8.50 -3 6 -23 34.00 9.50 -3 6 -23 39.60 15.50 3 -6 23 27.40 14.80 3 -6 23 40.20 11.50 -4 6 -23 -0.10 10.30 4 -6 23 -4.80 10.80 4 -6 23 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4 -27 -9.30 9.60 -6 -4 27 -5.60 11.20 5 4 -27 16.00 13.70 5 4 -27 14.50 12.60 -5 -4 27 22.50 14.50 4 4 -27 26.00 14.20 4 4 -27 18.80 12.80 -4 -4 27 -6.60 10.90 3 4 -27 -8.70 10.80 3 4 -27 -6.40 10.90 -3 -4 27 3.50 12.70 2 4 -27 43.20 16.80 2 4 -27 49.10 15.20 2 4 -27 67.29 16.70 -2 -4 27 46.60 16.80 1 4 -27 48.10 14.10 1 4 -27 22.90 12.60 1 4 -27 36.30 15.40 -1 -4 27 41.80 19.40 0 4 -27 178.08 27.20 0 4 -27 201.78 24.30 -1 4 -27 175.88 21.30 -1 4 -27 165.28 20.90 1 -4 27 189.98 24.40 2 -4 27 92.59 19.50 8 3 -27 16.60 13.40 7 3 -27 10.80 12.80 7 3 -27 -15.20 10.90 -7 -3 27 1.40 12.50 6 3 -27 1.60 9.90 6 3 -27 -8.60 11.80 -6 -3 27 11.40 13.70 5 3 -27 21.50 14.60 5 3 -27 2.70 10.70 -5 -3 27 10.60 13.50 4 3 -27 36.30 15.70 4 3 -27 32.40 15.20 -4 -3 27 24.60 16.00 3 3 -27 76.79 17.70 3 3 -27 19.90 12.90 -3 -3 27 22.60 15.40 2 3 -27 122.69 22.30 2 3 -27 124.49 21.40 2 3 -27 146.09 25.40 -2 -3 27 124.69 23.90 1 3 -27 193.08 27.10 1 3 -27 236.88 27.10 1 3 -27 193.18 23.80 -1 -3 27 184.88 32.40 0 3 -27 166.78 21.10 0 3 -27 165.68 22.50 0 -3 27 168.18 21.50 -1 3 -27 146.99 20.40 -1 3 -27 110.69 18.70 1 -3 27 86.79 18.50 -2 3 -27 119.69 19.50 8 2 -27 7.00 14.90 -8 -2 27 28.60 25.50 7 2 -27 10.30 13.70 -7 -2 27 5.60 11.90 6 2 -27 43.30 18.10 6 2 -27 28.20 16.00 -6 -2 27 45.30 15.90 5 2 -27 97.49 22.80 5 2 -27 100.59 21.20 -5 -2 27 90.69 22.10 4 2 -27 84.19 19.40 4 2 -27 126.99 21.50 -4 -2 27 99.29 22.40 3 2 -27 204.68 27.60 3 2 -27 214.58 26.60 -3 -2 27 174.48 27.70 2 2 -27 134.59 22.00 2 2 -27 105.69 15.80 2 2 -27 87.29 19.80 -2 -2 27 85.99 22.00 -2 -2 27 83.09 16.10 1 2 -27 65.09 15.30 1 2 -27 83.29 18.20 1 2 -27 75.89 14.60 1 2 -27 87.79 18.90 -1 -2 27 83.29 16.80 0 2 -27 159.78 20.70 0 2 -27 145.79 21.20 0 2 -27 182.38 26.90 0 -2 27 138.09 21.40 -1 2 -27 30.10 14.00 -1 2 -27 41.50 13.20 -1 2 -27 12.60 7.30 -2 2 -27 79.59 17.70 -8 -1 27 -4.50 18.60 7 1 -27 52.39 16.60 -7 -1 27 46.10 18.10 6 1 -27 70.19 18.20 -6 -1 27 58.19 19.70 5 1 -27 114.29 22.90 -5 -1 27 117.69 23.40 4 1 -27 72.49 17.70 4 1 -27 113.29 21.90 -4 -1 27 136.59 27.50 3 1 -27 259.57 33.10 3 1 -27 240.38 23.50 3 1 -27 167.28 25.60 -3 -1 27 210.38 24.60 -3 -1 27 223.98 33.80 2 1 -27 158.28 20.40 2 1 -27 153.18 24.10 2 1 -27 173.38 26.10 -2 -1 27 127.39 21.00 1 1 -27 155.58 23.10 1 1 -27 168.38 20.90 1 1 -27 146.39 21.10 1 1 -27 156.68 34.90 -1 -1 27 128.19 21.90 0 1 -27 146.99 20.80 0 1 -27 89.89 18.20 0 1 -27 128.99 19.40 -1 1 -27 8.90 7.80 -1 1 -27 26.60 12.30 -1 1 -27 18.50 12.70 -7 0 27 65.69 23.70 -6 0 27 177.68 29.50 -5 0 27 282.57 36.00 -5 0 27 213.78 25.50 4 0 -27 146.89 19.30 4 0 -27 128.49 26.20 -4 0 27 71.29 17.50 -4 0 27 128.79 26.40 3 0 -27 57.09 17.80 3 0 -27 90.89 21.10 3 0 -27 96.49 16.50 -3 0 27 90.49 19.20 2 0 -27 91.09 16.10 2 0 -27 110.59 28.70 2 0 -27 121.69 22.40 -2 0 27 44.90 16.10 1 0 -27 40.30 12.80 1 0 -27 47.40 15.60 0 0 -27 -6.40 10.30 0 0 -27 14.30 11.40 0 0 -27 18.50 11.00 -1 0 -27 27.20 22.80 7 -1 -27 164.78 20.20 -6 1 27 127.89 21.70 5 -1 -27 39.80 12.90 -5 1 27 27.20 14.80 4 -1 -27 106.09 17.20 -4 1 27 82.09 18.70 3 -1 -27 46.10 14.10 -3 1 27 18.90 17.20 2 -1 -27 67.29 15.90 1 -1 -27 18.20 12.10 1 -1 -27 43.10 14.70 0 -1 -27 -2.20 9.90 0 -1 -27 10.00 13.30 0 -1 -27 4.50 12.00 7 -2 -27 140.59 20.00 6 -2 -27 56.39 13.60 5 -2 -27 84.59 16.90 4 -2 -27 23.10 11.90 3 -2 -27 0.10 10.00 2 -2 -27 53.49 17.90 1 -2 -27 16.10 12.30 6 -3 -27 56.29 14.90 5 -3 -27 50.29 16.30 4 9 -28 6.90 12.70 3 9 -28 13.90 12.90 5 8 -28 30.90 17.20 4 8 -28 13.20 15.00 3 8 -28 -12.00 10.60 2 8 -28 3.50 11.90 1 8 -28 5.10 12.20 6 7 -28 6.40 15.10 5 7 -28 -3.40 11.30 4 7 -28 -12.00 9.60 3 7 -28 13.40 24.80 2 7 -28 -1.30 11.00 1 7 -28 29.40 13.90 0 7 -28 38.90 14.30 0 7 -28 60.69 16.90 6 6 -28 0.90 11.80 5 6 -28 13.40 12.60 4 6 -28 0.70 11.50 3 6 -28 2.90 11.90 2 6 -28 21.80 13.40 1 6 -28 16.80 12.30 0 6 -28 118.29 19.70 0 6 -28 75.79 16.80 6 5 -28 4.80 12.40 5 5 -28 9.70 13.30 4 5 -28 -1.20 20.80 3 5 -28 75.09 18.60 2 5 -28 43.30 14.90 1 5 -28 150.58 22.40 0 5 -28 95.09 17.90 0 5 -28 100.09 18.00 7 4 -28 12.60 23.10 6 4 -28 37.20 16.60 5 4 -28 -3.00 12.50 3 4 -28 124.39 22.80 2 4 -28 214.08 28.70 1 4 -28 154.88 22.40 0 4 -28 135.69 21.00 0 4 -28 137.89 20.00 7 3 -28 21.30 27.30 6 3 -28 140.29 28.10 5 3 -28 142.79 24.80 3 3 -28 123.69 22.20 2 3 -28 113.79 21.50 1 3 -28 133.69 21.70 0 3 -28 55.49 15.70 0 3 -28 71.99 16.00 0 3 -28 104.59 17.30 0 -3 28 31.30 15.30 6 2 -28 85.09 19.60 5 2 -28 233.48 30.50 4 2 -28 203.98 32.90 3 2 -28 151.08 25.60 2 2 -28 123.59 23.00 1 2 -28 36.90 12.90 1 2 -28 27.50 13.90 -1 -2 28 28.20 14.80 0 2 -28 37.60 13.90 0 2 -28 41.70 13.20 0 2 -28 37.10 13.90 6 1 -28 213.48 29.80 5 1 -28 124.09 24.50 4 1 -28 70.59 18.90 3 1 -28 83.69 15.60 3 1 -28 111.09 26.20 -3 -1 28 78.79 21.80 2 1 -28 22.60 11.10 2 1 -28 3.00 11.50 -2 -1 28 6.20 12.70 1 1 -28 24.60 11.10 1 1 -28 10.20 11.80 6 0 -28 60.59 28.20 5 0 -28 93.89 24.00 4 0 -28 69.79 14.70 4 0 -28 107.29 21.20 -4 0 28 50.89 17.20 3 0 -28 34.60 12.90 3 0 -28 21.40 15.10 -3 0 28 27.40 14.70 2 0 -28 5.80 10.00 2 0 -28 6.30 11.80 5 -1 -28 54.99 14.00 -5 1 28 37.30 19.40 4 -1 -28 2.00 9.80 5 5 -29 125.29 22.80 4 5 -29 129.39 24.50 3 5 -29 84.79 19.00 5 4 -29 95.29 21.20 4 4 -29 134.69 25.80 3 4 -29 64.09 18.20 5 3 -29 160.58 29.30 4 3 -29 99.79 21.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 79099 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_065_xm _database_code_depnum_ccdc_archive 'CCDC 2153977' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-22 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _vrf_PLAT088_065_xm ; PROBLEM: Poor Data / Parameter Ratio .................... 7.66 Note RESPONSE: to encounter this probem, we measured until a resolution of 0.65 angstrom. However all the -OC(CF3)3 groups of the [Al(OC(CF3)3)4]- are disordered over multiple positions, consideration of the restraints however leads to a brilliant data/paramater ratio of 18.8 ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C22 Al F36 I3 O10 Ru2' _chemical_formula_moiety 'C22 Al F36 I3 O10 Ru2' _chemical_formula_weight 1718.04 _chemical_melting_point ? _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_H-M_alt 'P n m a' _space_group_name_Hall '-P 2ac 2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' _cell_length_a 18.581(3) _cell_length_b 13.756(2) _cell_length_c 16.816(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4298.3(13) _cell_formula_units_Z 4 _cell_measurement_temperature 109(2) _cell_measurement_reflns_used 9620 _cell_measurement_theta_min 2.2045 _cell_measurement_theta_max 32.2625 _exptl_crystal_description block _exptl_crystal_colour yellow _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.655 _exptl_crystal_F_000 3184 _exptl_crystal_size_max 0.11 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.07 _exptl_absorpt_coefficient_mu 3.083 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6944 _exptl_absorpt_correction_T_max 0.7465 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 109(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 182411 _diffrn_reflns_av_unetI/netI 0.0179 _diffrn_reflns_av_R_equivalents 0.0509 _diffrn_reflns_theta_min 1.633 _diffrn_reflns_theta_max 33.198 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_h_max 28 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_limit_l_max 25 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 8508 _reflns_number_gt 7398 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS V6.2.15 Patch 4/2021-03-15 && APEX4 2021.10-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXS (G. Sheldrick)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details 'The disorders of the Nonaperfluorotertbutoxy-groups where treated with DSR' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+46.9395P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_number_reflns 8508 _refine_ls_number_parameters 1110 _refine_ls_number_restraints 12323 _refine_ls_R_factor_all 0.0604 _refine_ls_R_factor_gt 0.0528 _refine_ls_wR_factor_ref 0.1107 _refine_ls_wR_factor_gt 0.1077 _refine_ls_goodness_of_fit_ref 1.193 _refine_ls_restrained_S_all 1.035 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 1.513 _refine_diff_density_min -1.507 _refine_diff_density_rms 0.186 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.96832(3) 0.250000 0.06034(3) 0.03108(11) Uani 1 2 d S T P . . I2 I 0.93153(2) 0.38580(2) -0.12653(2) 0.02997(8) Uani 1 1 d . . . . . Ru1 Ru 1.03243(3) 0.250000 -0.08533(3) 0.02181(10) Uani 1 2 d S T P . . Ru2 Ru 0.85449(3) 0.250000 -0.04274(4) 0.02581(11) Uani 1 2 d S T P . . Al1 Al 0.90083(11) 0.250000 0.40110(14) 0.0230(4) Uani 1 2 d S T P . . O1 O 1.1294(2) 0.0861(4) -0.0290(3) 0.0490(12) Uani 1 1 d . . . . . O2 O 1.0924(4) 0.250000 -0.2536(4) 0.0480(16) Uani 1 2 d S T P . . O3 O 0.7812(2) 0.0907(3) 0.0533(3) 0.0475(11) Uani 1 1 d . . . . . O4 O 0.7369(4) 0.250000 -0.1683(6) 0.067(2) Uani 1 2 d S T P . . C1 C 1.0944(3) 0.1478(4) -0.0507(4) 0.0334(11) Uani 1 1 d . . . . . C2 C 1.0706(4) 0.250000 -0.1918(5) 0.0309(15) Uani 1 2 d S T P . . C3 C 0.8083(3) 0.1490(4) 0.0169(4) 0.0356(12) Uani 1 1 d . . . . . C4 C 0.7804(5) 0.250000 -0.1220(7) 0.044(2) Uani 1 2 d S T P . . O1_3 O 0.8920(5) 0.2636(14) 0.5061(6) 0.032(3) Uani 0.325(3) 1 d D U P A -2 C1_3 C 0.8547(5) 0.2498(10) 0.5737(6) 0.0282(15) Uani 0.325(3) 1 d D U P A -2 C2_3 C 0.7782(6) 0.2928(10) 0.5620(7) 0.034(2) Uani 0.325(3) 1 d D U P A -2 F1_3 F 0.7802(8) 0.3888(10) 0.5593(16) 0.067(5) Uani 0.325(3) 1 d D U P A -2 F2_3 F 0.7330(5) 0.2715(13) 0.6209(6) 0.055(4) Uani 0.325(3) 1 d D U P A -2 F3_3 F 0.7480(4) 0.260(2) 0.4956(5) 0.041(3) Uani 0.325(3) 1 d D U P A -2 C3_3 C 0.8512(8) 0.1407(10) 0.5972(9) 0.049(3) Uani 0.325(3) 1 d D U P A -2 F4_3 F 0.9161(8) 0.1008(12) 0.5813(12) 0.061(4) Uani 0.325(3) 1 d D U P A -2 F5_3 F 0.8026(9) 0.0953(13) 0.5522(13) 0.066(4) Uani 0.325(3) 1 d D U P A -2 F6_3 F 0.8380(10) 0.1235(13) 0.6729(9) 0.078(4) Uani 0.325(3) 1 d D U P A -2 C4_3 C 0.8924(7) 0.3080(11) 0.6408(7) 0.046(3) Uani 0.325(3) 1 d D U P A -2 F7_3 F 0.9506(6) 0.2629(17) 0.6667(7) 0.062(4) Uani 0.325(3) 1 d D U P A -2 F8_3 F 0.8455(8) 0.3178(13) 0.7015(7) 0.070(4) Uani 0.325(3) 1 d D U P A -2 F9_3 F 0.9106(10) 0.3964(11) 0.6195(9) 0.062(4) Uani 0.325(3) 1 d D U P A -2 O1_6 O 0.862(2) 0.359(2) 0.3753(17) 0.031(3) Uani 0.163(3) 1 d D U P A -1 C1_6 C 0.8370(10) 0.4167(13) 0.3181(12) 0.038(2) Uani 0.163(3) 1 d D U P A -1 C2_6 C 0.8959(11) 0.4474(15) 0.2578(13) 0.043(3) Uani 0.163(3) 1 d D U P A -1 F1_6 F 0.9394(13) 0.5175(17) 0.2845(15) 0.042(4) Uani 0.163(3) 1 d D U P A -1 F2_6 F 0.8638(15) 0.477(2) 0.1907(13) 0.048(4) Uani 0.163(3) 1 d D U P A -1 F3_6 F 0.9389(13) 0.3745(16) 0.2378(17) 0.042(4) Uani 0.163(3) 1 d D U P A -1 C3_6 C 0.7761(11) 0.3627(17) 0.2710(13) 0.042(3) Uani 0.163(3) 1 d D U P A -1 F4_6 F 0.7351(16) 0.311(2) 0.3201(15) 0.042(4) Uani 0.163(3) 1 d D U P A -1 F5_6 F 0.8030(15) 0.304(2) 0.2159(18) 0.051(5) Uani 0.163(3) 1 d D U P A -1 F6_6 F 0.7335(17) 0.425(3) 0.233(2) 0.052(5) Uani 0.163(3) 1 d D U P A -1 C4_6 C 0.8020(12) 0.5103(14) 0.3529(12) 0.046(3) Uani 0.163(3) 1 d D U P A -1 F7_6 F 0.7376(13) 0.493(2) 0.3827(17) 0.051(4) Uani 0.163(3) 1 d D U P A -1 F8_6 F 0.7971(16) 0.5782(17) 0.2966(16) 0.057(5) Uani 0.163(3) 1 d D U P A -1 F9_6 F 0.8425(15) 0.548(2) 0.4092(16) 0.055(5) Uani 0.163(3) 1 d D U P A -1 O1_7 O 0.8547(7) 0.3409(7) 0.3521(8) 0.037(2) Uani 0.442(3) 1 d D U P A -2 C1_7 C 0.8479(5) 0.4329(7) 0.3284(5) 0.0288(14) Uani 0.442(3) 1 d D U P A -2 C2_7 C 0.7690(6) 0.4550(8) 0.3045(7) 0.0461(19) Uani 0.442(3) 1 d D U P A -2 F1_7 F 0.7548(7) 0.4086(9) 0.2360(7) 0.059(3) Uani 0.442(3) 1 d D U P A -2 F2_7 F 0.7573(6) 0.5503(7) 0.2936(8) 0.068(3) Uani 0.442(3) 1 d D U P A -2 F3_7 F 0.7240(5) 0.4220(10) 0.3597(7) 0.069(3) Uani 0.442(3) 1 d D U P A -2 C3_7 C 0.8705(6) 0.5058(8) 0.3944(7) 0.0455(19) Uani 0.442(3) 1 d D U P A -2 F4_7 F 0.9323(5) 0.4741(6) 0.4270(6) 0.061(2) Uani 0.442(3) 1 d D U P A -2 F5_7 F 0.8186(8) 0.5025(12) 0.4514(7) 0.088(4) Uani 0.442(3) 1 d D U P A -2 F6_7 F 0.8841(5) 0.5933(5) 0.3672(5) 0.048(2) Uani 0.442(3) 1 d D U P A -2 C4_7 C 0.8979(6) 0.4498(9) 0.2553(7) 0.0458(19) Uani 0.442(3) 1 d D U P A -2 F7_7 F 0.9654(5) 0.4650(11) 0.2792(7) 0.073(3) Uani 0.442(3) 1 d D U P A -2 F8_7 F 0.8797(8) 0.5277(9) 0.2120(7) 0.073(3) Uani 0.442(3) 1 d D U P A -2 F9_7 F 0.8917(8) 0.3776(9) 0.2044(7) 0.075(3) Uani 0.442(3) 1 d D U P A -2 O1_5 O 0.9897(6) 0.2301(11) 0.3826(9) 0.035(3) Uani 0.323(4) 1 d D U P A -2 C1_5 C 1.0581(5) 0.2526(9) 0.4000(6) 0.0394(18) Uani 0.323(4) 1 d D U P A -2 C2_5 C 1.0776(7) 0.2175(10) 0.4851(8) 0.051(3) Uani 0.323(4) 1 d D U P A -2 F1_5 F 1.0505(7) 0.1295(9) 0.4973(10) 0.064(3) Uani 0.323(4) 1 d D U P A -2 F2_5 F 1.1488(6) 0.2127(13) 0.4955(10) 0.062(4) Uani 0.323(4) 1 d D U P A -2 F3_5 F 1.0512(6) 0.2779(9) 0.5393(7) 0.060(3) Uani 0.323(4) 1 d D U P A -2 C3_5 C 1.0707(7) 0.3638(9) 0.3951(9) 0.044(2) Uani 0.323(4) 1 d D U P A -2 F4_5 F 1.0722(9) 0.3953(10) 0.3202(8) 0.051(3) Uani 0.323(4) 1 d D U P A -2 F5_5 F 1.0173(6) 0.4115(11) 0.4311(10) 0.054(3) Uani 0.323(4) 1 d D U P A -2 F6_5 F 1.1323(6) 0.3927(10) 0.4284(9) 0.050(3) Uani 0.323(4) 1 d D U P A -2 C4_5 C 1.1074(6) 0.1991(9) 0.3392(8) 0.046(2) Uani 0.323(4) 1 d D U P A -2 F7_5 F 1.0827(7) 0.2093(10) 0.2652(7) 0.059(3) Uani 0.323(4) 1 d D U P A -2 F8_5 F 1.1747(5) 0.2327(13) 0.3409(9) 0.063(4) Uani 0.323(4) 1 d D U P A -2 F9_5 F 1.1098(7) 0.1047(8) 0.3535(11) 0.060(3) Uani 0.323(4) 1 d D U P A -2 O1_8 O 0.8644(8) 0.245(3) 0.4883(8) 0.026(3) Uani 0.175(3) 1 d D U P A -1 C1_8 C 0.8716(7) 0.2561(12) 0.5674(9) 0.031(2) Uani 0.175(3) 1 d D U P A -1 C2_8 C 0.8040(9) 0.2165(15) 0.6101(10) 0.041(3) Uani 0.175(3) 1 d D U P A -1 F1_8 F 0.8001(16) 0.1205(15) 0.6098(16) 0.056(5) Uani 0.175(3) 1 d D U P A -1 F2_8 F 0.7996(9) 0.246(3) 0.6853(8) 0.050(4) Uani 0.175(3) 1 d D U P A -1 F3_8 F 0.7452(8) 0.249(3) 0.5724(11) 0.057(4) Uani 0.175(3) 1 d D U P A -1 C3_8 C 0.8792(10) 0.3666(13) 0.5873(11) 0.040(3) Uani 0.175(3) 1 d D U P A -1 F4_8 F 0.9205(12) 0.4088(16) 0.5334(11) 0.044(4) Uani 0.175(3) 1 d D U P A -1 F5_8 F 0.8148(11) 0.4091(18) 0.5900(16) 0.045(4) Uani 0.175(3) 1 d D U P A -1 F6_8 F 0.9097(13) 0.3794(18) 0.6579(11) 0.049(5) Uani 0.175(3) 1 d D U P A -1 C4_8 C 0.9406(9) 0.2044(14) 0.5978(11) 0.038(3) Uani 0.175(3) 1 d D U P A -1 F7_8 F 0.9992(8) 0.258(2) 0.5837(10) 0.053(5) Uani 0.175(3) 1 d D U P A -1 F8_8 F 0.9389(13) 0.1880(18) 0.6755(10) 0.048(5) Uani 0.175(3) 1 d D U P A -1 F9_8 F 0.9475(12) 0.1194(14) 0.5619(14) 0.043(4) Uani 0.175(3) 1 d D U P A -1 O1_9 O 0.9936(9) 0.248(3) 0.4011(14) 0.034(4) Uani 0.177(4) 1 d D U P A -1 C1_9 C 1.0578(8) 0.2677(12) 0.3695(9) 0.035(2) Uani 0.177(4) 1 d D U P A -1 C2_9 C 1.0633(9) 0.2227(15) 0.2849(10) 0.045(3) Uani 0.177(4) 1 d D U P A -1 F1_9 F 1.0776(15) 0.1282(14) 0.2907(14) 0.056(5) Uani 0.177(4) 1 d D U P A -1 F2_9 F 1.1139(9) 0.265(2) 0.2417(11) 0.055(5) Uani 0.177(4) 1 d D U P A -1 F3_9 F 1.0012(8) 0.2276(19) 0.2462(9) 0.051(6) Uani 0.177(4) 1 d D U P A -1 C3_9 C 1.0685(10) 0.3797(13) 0.3640(13) 0.046(3) Uani 0.177(4) 1 d D U P A -1 F4_9 F 1.0404(13) 0.4233(19) 0.4272(15) 0.055(5) Uani 0.177(4) 1 d D U P A -1 F5_9 F 1.0353(11) 0.4162(18) 0.3011(13) 0.058(5) Uani 0.177(4) 1 d D U P A -1 F6_9 F 1.1384(9) 0.4008(18) 0.3603(19) 0.058(5) Uani 0.177(4) 1 d D U P A -1 C4_9 C 1.1193(8) 0.2264(13) 0.4221(10) 0.040(3) Uani 0.177(4) 1 d D U P A -1 F7_9 F 1.1268(11) 0.2787(18) 0.4883(12) 0.047(4) Uani 0.177(4) 1 d D U P A -1 F8_9 F 1.1821(8) 0.2269(19) 0.3833(12) 0.046(5) Uani 0.177(4) 1 d D U P A -1 F9_9 F 1.1049(11) 0.1354(13) 0.4440(15) 0.051(4) Uani 0.177(4) 1 d D U P A -1 O1_10 O 0.8821(9) 0.3542(14) 0.3435(12) 0.036(3) Uani 0.238(3) 1 d D U P A -3 C1_10 C 0.8342(8) 0.4166(10) 0.3136(8) 0.0373(19) Uani 0.238(3) 1 d D U P A -3 C2_10 C 0.7856(10) 0.3590(13) 0.2527(10) 0.045(3) Uani 0.238(3) 1 d D U P A -3 F1_10 F 0.8278(13) 0.3104(18) 0.2027(13) 0.059(5) Uani 0.238(3) 1 d D U P A -3 F2_10 F 0.7464(14) 0.4175(17) 0.2085(12) 0.055(4) Uani 0.238(3) 1 d D U P A -3 F3_10 F 0.7416(11) 0.3006(16) 0.2923(13) 0.057(4) Uani 0.238(3) 1 d D U P A -3 C3_10 C 0.7830(9) 0.4596(11) 0.3774(10) 0.044(2) Uani 0.238(3) 1 d D U P A -3 F4_10 F 0.8128(13) 0.5290(14) 0.4212(13) 0.063(4) Uani 0.238(3) 1 d D U P A -3 F5_10 F 0.7510(9) 0.3862(11) 0.4134(12) 0.061(4) Uani 0.238(3) 1 d D U P A -3 F6_10 F 0.7291(9) 0.5121(14) 0.3456(12) 0.060(4) Uani 0.238(3) 1 d D U P A -3 C4_10 C 0.8710(8) 0.4984(12) 0.2651(9) 0.044(2) Uani 0.238(3) 1 d D U P A -3 F7_10 F 0.9185(11) 0.5438(15) 0.3121(13) 0.066(4) Uani 0.238(3) 1 d D U P A -3 F8_10 F 0.8220(8) 0.5562(12) 0.2314(10) 0.054(4) Uani 0.238(3) 1 d D U P A -3 F9_10 F 0.9052(12) 0.4633(16) 0.2013(11) 0.068(4) Uani 0.238(3) 1 d D U P A -3 O1_11 O 0.8633(19) 0.353(2) 0.3822(17) 0.033(3) Uani 0.157(3) 1 d D U P A -4 C1_11 C 0.8404(10) 0.4151(14) 0.3254(11) 0.037(2) Uani 0.157(3) 1 d D U P A -4 C2_11 C 0.8651(12) 0.3748(16) 0.2441(12) 0.044(3) Uani 0.157(3) 1 d D U P A -4 F1_11 F 0.9338(12) 0.346(2) 0.2476(17) 0.048(4) Uani 0.157(3) 1 d D U P A -4 F2_11 F 0.8618(16) 0.439(2) 0.1858(13) 0.047(4) Uani 0.157(3) 1 d D U P A -4 F3_11 F 0.8253(18) 0.300(2) 0.218(2) 0.056(5) Uani 0.157(3) 1 d D U P A -4 C3_11 C 0.7570(10) 0.4185(16) 0.3314(13) 0.044(3) Uani 0.157(3) 1 d D U P A -4 F4_11 F 0.7367(16) 0.471(2) 0.3943(15) 0.051(4) Uani 0.157(3) 1 d D U P A -4 F5_11 F 0.7323(15) 0.3298(16) 0.346(2) 0.058(5) Uani 0.157(3) 1 d D U P A -4 F6_11 F 0.7235(14) 0.453(2) 0.2682(15) 0.059(5) Uani 0.157(3) 1 d D U P A -4 C4_11 C 0.8724(12) 0.5171(14) 0.3418(13) 0.048(3) Uani 0.157(3) 1 d D U P A -4 F7_11 F 0.8702(19) 0.538(2) 0.4186(13) 0.069(5) Uani 0.157(3) 1 d D U P A -4 F8_11 F 0.8354(16) 0.5862(18) 0.3039(18) 0.066(5) Uani 0.157(3) 1 d D U P A -4 F9_11 F 0.9408(11) 0.521(2) 0.3194(19) 0.053(4) Uani 0.157(3) 1 d D U P A -4 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.0295(2) 0.0412(3) 0.02246(19) 0.000 0.00153(16) 0.000 I2 0.02748(14) 0.02608(14) 0.03636(16) 0.00780(13) 0.00288(12) 0.00440(12) Ru1 0.0179(2) 0.0212(2) 0.0263(2) 0.000 0.00258(18) 0.000 Ru2 0.0168(2) 0.0242(2) 0.0364(3) 0.000 0.0017(2) 0.000 Al1 0.0166(8) 0.0208(9) 0.0316(10) 0.000 -0.0020(7) 0.000 O1 0.038(2) 0.041(2) 0.068(3) 0.013(2) -0.001(2) 0.012(2) O2 0.046(4) 0.057(4) 0.041(3) 0.000 0.021(3) 0.000 O3 0.035(2) 0.037(2) 0.071(3) 0.003(2) 0.015(2) -0.0054(18) O4 0.035(4) 0.076(6) 0.091(6) 0.000 -0.030(4) 0.000 C1 0.024(2) 0.032(3) 0.045(3) 0.002(2) 0.001(2) 0.0027(19) C2 0.027(3) 0.028(3) 0.038(4) 0.000 0.013(3) 0.000 C3 0.026(2) 0.026(2) 0.055(3) 0.000(2) 0.011(2) 0.0010(19) C4 0.027(4) 0.045(5) 0.060(6) 0.000 -0.013(4) 0.000 O1_3 0.025(4) 0.040(8) 0.030(3) -0.002(4) -0.001(3) -0.012(5) C1_3 0.027(3) 0.032(3) 0.025(3) 0.001(4) -0.005(2) -0.003(4) C2_3 0.026(4) 0.038(5) 0.036(4) 0.002(4) -0.002(3) 0.000(4) F1_3 0.028(6) 0.037(5) 0.136(13) 0.000(6) -0.008(7) 0.004(4) F2_3 0.032(4) 0.096(12) 0.036(4) 0.011(6) 0.004(3) 0.006(6) F3_3 0.026(3) 0.060(9) 0.035(3) 0.007(6) -0.008(3) 0.000(7) C3_3 0.047(6) 0.037(4) 0.064(6) 0.017(4) -0.006(5) -0.005(4) F4_3 0.056(6) 0.051(7) 0.077(10) 0.039(8) 0.000(7) 0.012(5) F5_3 0.061(8) 0.040(7) 0.097(9) 0.004(8) -0.009(8) -0.019(6) F6_3 0.094(10) 0.068(9) 0.071(6) 0.035(6) 0.010(6) -0.009(8) C4_3 0.045(5) 0.059(5) 0.034(4) -0.010(4) -0.012(4) -0.009(5) F7_3 0.046(5) 0.090(10) 0.051(6) 0.004(8) -0.025(4) -0.011(7) F8_3 0.089(8) 0.087(10) 0.035(5) -0.019(6) 0.005(5) -0.001(8) F9_3 0.082(9) 0.059(5) 0.047(7) -0.016(6) -0.022(7) -0.026(5) O1_6 0.039(7) 0.024(6) 0.031(6) -0.002(5) 0.003(5) 0.010(5) C1_6 0.042(4) 0.032(4) 0.040(4) 0.007(3) 0.001(3) 0.008(3) C2_6 0.051(5) 0.038(5) 0.039(5) 0.003(4) 0.005(4) -0.001(4) F1_6 0.047(8) 0.033(7) 0.044(9) 0.004(7) 0.006(7) 0.001(6) F2_6 0.065(9) 0.038(10) 0.040(6) 0.003(7) -0.002(6) -0.004(8) F3_6 0.048(8) 0.041(7) 0.036(9) 0.000(7) 0.007(6) -0.003(6) C3_6 0.043(5) 0.041(5) 0.043(6) 0.009(4) -0.003(4) 0.006(4) F4_6 0.040(8) 0.043(9) 0.044(10) 0.008(7) -0.004(7) 0.005(6) F5_6 0.052(11) 0.052(8) 0.048(8) -0.003(6) -0.004(7) 0.003(8) F6_6 0.050(9) 0.055(10) 0.051(10) 0.017(8) -0.007(7) 0.011(7) C4_6 0.051(5) 0.038(4) 0.049(5) 0.003(4) -0.003(4) 0.017(4) F7_6 0.053(6) 0.061(10) 0.039(9) -0.001(8) 0.001(6) 0.021(6) F8_6 0.057(10) 0.039(8) 0.074(8) 0.016(7) -0.009(8) 0.013(8) F9_6 0.064(9) 0.038(9) 0.063(8) -0.007(7) -0.010(7) 0.017(8) O1_7 0.038(4) 0.024(3) 0.048(5) 0.015(3) -0.010(4) 0.001(3) C1_7 0.036(3) 0.022(3) 0.028(3) 0.009(2) -0.003(2) 0.003(3) C2_7 0.041(3) 0.043(4) 0.054(4) 0.007(3) -0.008(3) 0.011(3) F1_7 0.057(6) 0.055(5) 0.066(5) 0.001(4) -0.031(4) 0.013(5) F2_7 0.062(6) 0.044(4) 0.097(7) 0.014(4) -0.011(6) 0.022(4) F3_7 0.043(4) 0.076(6) 0.089(6) 0.018(5) 0.011(5) 0.008(5) C3_7 0.063(4) 0.032(3) 0.041(4) -0.001(3) -0.012(3) 0.005(4) F4_7 0.078(5) 0.026(4) 0.078(6) -0.002(4) -0.050(4) -0.008(4) F5_7 0.110(7) 0.105(9) 0.048(5) -0.016(5) 0.016(5) 0.009(7) F6_7 0.070(5) 0.024(3) 0.050(4) -0.005(3) -0.027(4) 0.000(3) C4_7 0.057(4) 0.040(4) 0.041(4) 0.006(3) 0.011(3) -0.005(4) F7_7 0.053(4) 0.092(8) 0.073(6) 0.016(6) 0.013(4) -0.018(5) F8_7 0.103(7) 0.060(5) 0.057(6) 0.030(4) 0.020(5) 0.004(6) F9_7 0.104(7) 0.065(5) 0.055(5) -0.016(4) 0.037(5) -0.023(5) O1_5 0.017(3) 0.029(7) 0.058(7) -0.002(5) 0.008(3) 0.001(3) C1_5 0.018(3) 0.035(3) 0.066(4) -0.008(4) 0.005(3) 0.002(3) C2_5 0.026(5) 0.059(6) 0.068(5) 0.003(5) 0.001(4) -0.001(4) F1_5 0.042(6) 0.061(6) 0.088(9) 0.015(6) 0.001(7) -0.003(5) F2_5 0.029(4) 0.073(9) 0.084(8) -0.003(7) -0.007(5) 0.001(4) F3_5 0.030(5) 0.082(8) 0.066(5) -0.012(6) -0.007(4) -0.003(5) C3_5 0.021(4) 0.035(4) 0.076(6) -0.010(4) 0.004(4) -0.002(3) F4_5 0.041(7) 0.035(6) 0.079(6) -0.007(5) 0.002(5) -0.002(5) F5_5 0.024(5) 0.042(6) 0.096(8) -0.029(6) 0.005(5) -0.003(5) F6_5 0.022(4) 0.046(6) 0.082(7) -0.012(6) 0.003(5) -0.006(4) C4_5 0.024(4) 0.039(4) 0.076(5) -0.011(5) 0.014(4) 0.002(4) F7_5 0.039(6) 0.067(8) 0.072(5) -0.012(5) 0.016(4) -0.002(5) F8_5 0.023(4) 0.054(10) 0.110(9) -0.016(9) 0.019(4) -0.002(5) F9_5 0.031(6) 0.036(4) 0.114(10) -0.011(6) 0.013(7) 0.008(4) O1_8 0.019(6) 0.036(8) 0.024(4) -0.002(6) 0.002(4) -0.006(10) C1_8 0.031(4) 0.038(4) 0.025(4) -0.001(5) 0.000(3) -0.003(4) C2_8 0.036(5) 0.051(6) 0.034(5) 0.008(6) 0.007(4) -0.002(5) F1_8 0.069(12) 0.052(6) 0.046(11) 0.011(7) 0.041(10) -0.003(6) F2_8 0.051(8) 0.067(10) 0.034(5) 0.006(8) 0.015(5) -0.010(15) F3_8 0.033(5) 0.092(11) 0.045(7) 0.027(12) 0.010(5) -0.001(10) C3_8 0.045(6) 0.040(5) 0.034(6) -0.006(5) -0.008(5) -0.005(5) F4_8 0.053(9) 0.041(8) 0.037(7) -0.006(7) -0.008(7) -0.013(8) F5_8 0.055(7) 0.040(9) 0.041(11) -0.015(8) -0.006(7) 0.004(7) F6_8 0.061(10) 0.051(10) 0.035(6) -0.006(7) -0.013(7) -0.011(9) C4_8 0.033(5) 0.048(6) 0.033(5) 0.003(5) -0.006(5) -0.002(5) F7_8 0.038(5) 0.073(10) 0.047(8) 0.017(11) -0.022(6) -0.017(9) F8_8 0.049(10) 0.061(12) 0.034(6) 0.007(6) -0.005(6) 0.011(10) F9_8 0.040(9) 0.049(7) 0.042(9) 0.002(7) -0.012(8) 0.009(6) O1_9 0.018(4) 0.037(9) 0.048(8) -0.005(10) 0.001(5) 0.005(7) C1_9 0.017(4) 0.041(5) 0.049(5) -0.009(4) -0.001(4) 0.002(4) C2_9 0.032(6) 0.056(7) 0.047(5) -0.010(5) 0.003(4) 0.000(6) F1_9 0.058(11) 0.055(7) 0.054(11) -0.018(7) 0.014(10) 0.002(7) F2_9 0.039(7) 0.073(13) 0.054(8) -0.003(10) 0.009(6) -0.003(9) F3_9 0.037(6) 0.092(17) 0.025(6) -0.002(8) 0.005(5) -0.008(7) C3_9 0.025(6) 0.039(5) 0.073(8) -0.003(5) 0.001(6) 0.002(5) F4_9 0.039(10) 0.040(8) 0.086(8) -0.015(8) 0.007(8) -0.007(9) F5_9 0.027(8) 0.064(11) 0.084(8) 0.022(9) 0.006(8) 0.004(8) F6_9 0.025(6) 0.050(10) 0.098(14) 0.008(11) 0.001(7) -0.001(6) C4_9 0.020(4) 0.046(6) 0.055(6) -0.007(5) -0.003(4) 0.006(5) F7_9 0.028(8) 0.057(9) 0.057(7) -0.012(7) -0.011(6) 0.009(8) F8_9 0.019(5) 0.058(12) 0.061(9) -0.004(9) -0.003(6) 0.010(6) F9_9 0.030(8) 0.047(6) 0.075(11) 0.000(6) -0.003(8) 0.007(6) O1_10 0.036(5) 0.035(5) 0.035(5) 0.014(4) 0.008(4) 0.009(4) C1_10 0.040(4) 0.032(4) 0.039(4) 0.009(3) 0.003(3) 0.011(3) C2_10 0.050(5) 0.039(5) 0.047(5) 0.004(4) -0.005(4) 0.010(4) F1_10 0.075(10) 0.064(9) 0.038(7) -0.004(6) -0.011(6) 0.027(7) F2_10 0.065(9) 0.043(8) 0.058(9) 0.002(7) -0.018(7) 0.013(6) F3_10 0.047(7) 0.051(8) 0.072(10) 0.012(7) -0.016(6) -0.002(5) C3_10 0.047(5) 0.038(5) 0.047(5) 0.003(4) 0.008(4) 0.014(4) F4_10 0.088(9) 0.037(7) 0.065(8) -0.004(6) -0.006(7) 0.016(6) F5_10 0.054(7) 0.046(6) 0.082(10) 0.018(6) 0.036(7) 0.024(5) F6_10 0.050(6) 0.065(8) 0.063(8) 0.022(7) 0.019(5) 0.029(6) C4_10 0.048(5) 0.037(4) 0.047(5) 0.014(4) 0.002(4) 0.008(4) F7_10 0.061(8) 0.054(8) 0.081(8) 0.015(7) -0.017(7) -0.008(6) F8_10 0.046(6) 0.062(8) 0.053(8) 0.037(6) 0.009(5) 0.014(6) F9_10 0.078(9) 0.066(8) 0.061(6) 0.015(6) 0.029(6) 0.014(7) O1_11 0.039(6) 0.028(6) 0.033(5) 0.001(5) 0.002(6) 0.011(6) C1_11 0.041(4) 0.034(4) 0.036(4) 0.007(3) 0.001(4) 0.008(3) C2_11 0.050(5) 0.044(5) 0.037(4) 0.003(4) 0.003(4) 0.006(4) F1_11 0.053(6) 0.057(11) 0.033(9) 0.005(8) 0.009(6) 0.013(6) F2_11 0.060(9) 0.055(8) 0.027(6) 0.001(6) -0.006(7) 0.005(7) F3_11 0.069(10) 0.053(7) 0.045(11) -0.003(7) -0.009(9) 0.001(8) C3_11 0.041(4) 0.042(5) 0.049(5) 0.011(5) 0.001(4) 0.011(4) F4_11 0.048(9) 0.051(9) 0.054(7) 0.009(7) 0.004(7) 0.022(8) F5_11 0.042(8) 0.046(6) 0.086(12) 0.014(6) 0.013(10) 0.008(6) F6_11 0.053(8) 0.065(10) 0.059(7) 0.012(7) -0.013(7) 0.013(9) C4_11 0.058(5) 0.034(4) 0.052(5) 0.004(4) -0.004(5) 0.004(4) F7_11 0.102(12) 0.045(10) 0.061(6) -0.013(6) -0.008(7) 0.008(10) F8_11 0.070(9) 0.041(6) 0.086(9) 0.016(8) -0.007(9) 0.011(7) F9_11 0.054(5) 0.033(9) 0.073(10) 0.004(9) -0.013(7) -0.005(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 Ru1 2.7239(8) . ? I1 Ru2 2.7347(8) . ? I2 Ru1 2.7358(6) . ? I2 Ru2 2.7431(6) . ? Ru1 C1 1.908(6) 7_565 ? Ru1 C1 1.908(6) . ? Ru1 C2 1.925(8) . ? Ru2 C4 1.916(9) . ? Ru2 C3 1.916(6) . ? Ru2 C3 1.916(6) 7_565 ? Al1 O1_11 1.62(3) . ? Al1 O1_8 1.617(13) . ? Al1 O1_5 1.702(11) . ? Al1 O1_6 1.72(2) . ? Al1 O1_9 1.723(17) . ? Al1 O1_7 1.726(9) . ? Al1 O1_10 1.765(15) . ? Al1 O1_3 1.783(10) . ? O1 C1 1.130(7) . ? O2 C2 1.116(10) . ? O3 C3 1.127(7) . ? O4 C4 1.123(11) . ? O1_3 C1_3 1.345(11) . ? C1_3 C4_3 1.551(12) . ? C1_3 C2_3 1.552(12) . ? C1_3 C3_3 1.554(13) . ? C2_3 F1_3 1.322(12) . ? C2_3 F3_3 1.329(12) . ? C2_3 F2_3 1.330(12) . ? C3_3 F6_3 1.318(13) . ? C3_3 F5_3 1.333(13) . ? C3_3 F4_3 1.352(13) . ? C4_3 F9_3 1.313(13) . ? C4_3 F7_3 1.319(13) . ? C4_3 F8_3 1.349(12) . ? O1_6 C1_6 1.330(14) . ? C1_6 C2_6 1.552(13) . ? C1_6 C4_6 1.557(13) . ? C1_6 C3_6 1.569(14) . ? C2_6 F3_6 1.325(14) . ? C2_6 F1_6 1.337(14) . ? C2_6 F2_6 1.338(14) . ? C3_6 F6_6 1.325(14) . ? C3_6 F5_6 1.328(14) . ? C3_6 F4_6 1.331(14) . ? C4_6 F9_6 1.316(14) . ? C4_6 F7_6 1.319(14) . ? C4_6 F8_6 1.332(14) . ? O1_7 C1_7 1.333(10) . ? C1_7 C2_7 1.551(11) . ? C1_7 C3_7 1.553(11) . ? C1_7 C4_7 1.557(11) . ? C2_7 F3_7 1.328(11) . ? C2_7 F2_7 1.342(11) . ? C2_7 F1_7 1.343(12) . ? C3_7 F6_7 1.312(11) . ? C3_7 F4_7 1.345(11) . ? C3_7 F5_7 1.361(12) . ? C4_7 F9_7 1.316(12) . ? C4_7 F7_7 1.333(12) . ? C4_7 F8_7 1.340(12) . ? O1_5 C1_5 1.341(12) . ? C1_5 C3_5 1.550(13) . ? C1_5 C2_5 1.554(12) . ? C1_5 C4_5 1.558(12) . ? C2_5 F1_5 1.327(12) . ? C2_5 F3_5 1.328(12) . ? C2_5 F2_5 1.337(12) . ? C3_5 F4_5 1.333(13) . ? C3_5 F5_5 1.334(12) . ? C3_5 F6_5 1.335(12) . ? C4_5 F9_5 1.321(12) . ? C4_5 F7_5 1.332(13) . ? C4_5 F8_5 1.334(12) . ? O1_8 C1_8 1.345(13) . ? C1_8 C2_8 1.546(13) . ? C1_8 C4_8 1.553(13) . ? C1_8 C3_8 1.562(13) . ? C2_8 F1_8 1.323(13) . ? C2_8 F2_8 1.331(13) . ? C2_8 F3_8 1.338(13) . ? C3_8 F4_8 1.322(14) . ? C3_8 F6_8 1.326(14) . ? C3_8 F5_8 1.332(14) . ? C4_8 F9_8 1.322(13) . ? C4_8 F8_8 1.325(13) . ? C4_8 F7_8 1.340(13) . ? O1_9 C1_9 1.335(14) . ? C1_9 C4_9 1.552(13) . ? C1_9 C2_9 1.555(13) . ? C1_9 C3_9 1.556(13) . ? C2_9 F2_9 1.325(14) . ? C2_9 F3_9 1.327(13) . ? C2_9 F1_9 1.330(14) . ? C3_9 F5_9 1.323(14) . ? C3_9 F4_9 1.329(14) . ? C3_9 F6_9 1.332(14) . ? C4_9 F9_9 1.331(13) . ? C4_9 F7_9 1.334(13) . ? C4_9 F8_9 1.337(13) . ? O1_10 C1_10 1.334(13) . ? C1_10 C4_10 1.550(13) . ? C1_10 C3_10 1.550(13) . ? C1_10 C2_10 1.579(13) . ? C2_10 F2_10 1.316(13) . ? C2_10 F3_10 1.326(13) . ? C2_10 F1_10 1.329(13) . ? C3_10 F5_10 1.319(13) . ? C3_10 F4_10 1.326(13) . ? C3_10 F6_10 1.346(13) . ? C4_10 F8_10 1.335(13) . ? C4_10 F9_10 1.337(13) . ? C4_10 F7_10 1.339(13) . ? O1_11 C1_11 1.346(15) . ? C1_11 C2_11 1.545(13) . ? C1_11 C4_11 1.548(13) . ? C1_11 C3_11 1.553(13) . ? C2_11 F2_11 1.317(14) . ? C2_11 F3_11 1.337(14) . ? C2_11 F1_11 1.339(14) . ? C3_11 F6_11 1.319(14) . ? C3_11 F5_11 1.328(14) . ? C3_11 F4_11 1.336(14) . ? C4_11 F7_11 1.325(14) . ? C4_11 F9_11 1.327(14) . ? C4_11 F8_11 1.334(14) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Ru1 I1 Ru2 76.60(2) . . ? Ru1 I2 Ru2 76.27(2) . . ? C1 Ru1 C1 94.9(3) 7_565 . ? C1 Ru1 C2 93.5(2) 7_565 . ? C1 Ru1 C2 93.5(2) . . ? C1 Ru1 I1 89.37(18) 7_565 . ? C1 Ru1 I1 89.37(18) . . ? C2 Ru1 I1 175.7(2) . . ? C1 Ru1 I2 89.31(17) 7_565 . ? C1 Ru1 I2 173.63(17) . . ? C2 Ru1 I2 90.97(18) . . ? I1 Ru1 I2 85.873(18) . . ? C1 Ru1 I2 173.63(17) 7_565 7_565 ? C1 Ru1 I2 89.31(17) . 7_565 ? C2 Ru1 I2 90.97(18) . 7_565 ? I1 Ru1 I2 85.872(18) . 7_565 ? I2 Ru1 I2 86.13(2) . 7_565 ? C4 Ru2 C3 92.4(3) . . ? C4 Ru2 C3 92.4(3) . 7_565 ? C3 Ru2 C3 93.0(3) . 7_565 ? C4 Ru2 I1 175.3(3) . . ? C3 Ru2 I1 90.83(19) . . ? C3 Ru2 I1 90.83(19) 7_565 . ? C4 Ru2 I2 91.0(2) . 7_565 ? C3 Ru2 I2 90.48(17) . 7_565 ? C3 Ru2 I2 175.01(17) 7_565 7_565 ? I1 Ru2 I2 85.52(2) . 7_565 ? C4 Ru2 I2 91.0(2) . . ? C3 Ru2 I2 175.01(17) . . ? C3 Ru2 I2 90.48(17) 7_565 . ? I1 Ru2 I2 85.52(2) . . ? I2 Ru2 I2 85.85(2) 7_565 . ? O1_8 Al1 O1_6 95.2(18) . . ? O1_8 Al1 O1_9 114.7(10) . . ? O1_6 Al1 O1_9 115.4(19) . . ? O1_5 Al1 O1_7 120.7(7) . . ? O1_5 Al1 O1_3 106.7(6) . . ? O1_7 Al1 O1_3 110.5(7) . . ? O1 C1 Ru1 177.9(5) . . ? O2 C2 Ru1 179.6(8) . . ? O3 C3 Ru2 178.6(6) . . ? O4 C4 Ru2 179.9(10) . . ? C1_3 O1_3 Al1 150.5(10) . . ? O1_3 C1_3 C4_3 108.0(10) . . ? O1_3 C1_3 C2_3 108.1(9) . . ? C4_3 C1_3 C2_3 108.1(9) . . ? O1_3 C1_3 C3_3 111.9(11) . . ? C4_3 C1_3 C3_3 109.4(9) . . ? C2_3 C1_3 C3_3 111.2(9) . . ? F1_3 C2_3 F3_3 109.0(16) . . ? F1_3 C2_3 F2_3 105.4(14) . . ? F3_3 C2_3 F2_3 106.5(10) . . ? F1_3 C2_3 C1_3 111.0(11) . . ? F3_3 C2_3 C1_3 111.2(10) . . ? F2_3 C2_3 C1_3 113.5(10) . . ? F6_3 C3_3 F5_3 109.8(15) . . ? F6_3 C3_3 F4_3 106.6(14) . . ? F5_3 C3_3 F4_3 107.5(15) . . ? F6_3 C3_3 C1_3 115.2(12) . . ? F5_3 C3_3 C1_3 109.6(12) . . ? F4_3 C3_3 C1_3 107.7(11) . . ? F9_3 C4_3 F7_3 108.3(14) . . ? F9_3 C4_3 F8_3 106.3(14) . . ? F7_3 C4_3 F8_3 109.1(13) . . ? F9_3 C4_3 C1_3 113.3(11) . . ? F7_3 C4_3 C1_3 111.6(11) . . ? F8_3 C4_3 C1_3 108.0(11) . . ? C1_6 O1_6 Al1 148(2) . . ? O1_6 C1_6 C2_6 112.6(17) . . ? O1_6 C1_6 C4_6 111.6(16) . . ? C2_6 C1_6 C4_6 108.3(12) . . ? O1_6 C1_6 C3_6 109.9(17) . . ? C2_6 C1_6 C3_6 107.8(12) . . ? C4_6 C1_6 C3_6 106.3(13) . . ? F3_6 C2_6 F1_6 105.4(17) . . ? F3_6 C2_6 F2_6 106.5(17) . . ? F1_6 C2_6 F2_6 109.6(18) . . ? F3_6 C2_6 C1_6 112.7(16) . . ? F1_6 C2_6 C1_6 113.8(15) . . ? F2_6 C2_6 C1_6 108.7(15) . . ? F6_6 C3_6 F5_6 106.6(18) . . ? F6_6 C3_6 F4_6 107.5(18) . . ? F5_6 C3_6 F4_6 108.6(18) . . ? F6_6 C3_6 C1_6 111.4(17) . . ? F5_6 C3_6 C1_6 111.8(16) . . ? F4_6 C3_6 C1_6 110.7(16) . . ? F9_6 C4_6 F7_6 108.4(18) . . ? F9_6 C4_6 F8_6 106.0(18) . . ? F7_6 C4_6 F8_6 109.5(18) . . ? F9_6 C4_6 C1_6 110.8(16) . . ? F7_6 C4_6 C1_6 111.9(16) . . ? F8_6 C4_6 C1_6 110.0(15) . . ? C1_7 O1_7 Al1 151.4(9) . . ? O1_7 C1_7 C2_7 110.6(9) . . ? O1_7 C1_7 C3_7 111.9(9) . . ? C2_7 C1_7 C3_7 108.3(8) . . ? O1_7 C1_7 C4_7 108.8(9) . . ? C2_7 C1_7 C4_7 109.3(8) . . ? C3_7 C1_7 C4_7 107.9(8) . . ? F3_7 C2_7 F2_7 109.1(11) . . ? F3_7 C2_7 F1_7 108.3(12) . . ? F2_7 C2_7 F1_7 108.4(11) . . ? F3_7 C2_7 C1_7 110.4(9) . . ? F2_7 C2_7 C1_7 112.3(10) . . ? F1_7 C2_7 C1_7 108.3(9) . . ? F6_7 C3_7 F4_7 106.0(9) . . ? F6_7 C3_7 F5_7 114.3(12) . . ? F4_7 C3_7 F5_7 107.9(11) . . ? F6_7 C3_7 C1_7 113.3(9) . . ? F4_7 C3_7 C1_7 108.3(9) . . ? F5_7 C3_7 C1_7 106.9(9) . . ? F9_7 C4_7 F7_7 113.4(12) . . ? F9_7 C4_7 F8_7 103.2(11) . . ? F7_7 C4_7 F8_7 106.0(11) . . ? F9_7 C4_7 C1_7 110.4(9) . . ? F7_7 C4_7 C1_7 110.3(9) . . ? F8_7 C4_7 C1_7 113.4(10) . . ? C1_5 O1_5 Al1 147.5(11) . . ? O1_5 C1_5 C3_5 111.1(10) . . ? O1_5 C1_5 C2_5 110.4(11) . . ? C3_5 C1_5 C2_5 108.7(10) . . ? O1_5 C1_5 C4_5 107.8(10) . . ? C3_5 C1_5 C4_5 110.1(9) . . ? C2_5 C1_5 C4_5 108.7(9) . . ? F1_5 C2_5 F3_5 108.9(12) . . ? F1_5 C2_5 F2_5 108.1(12) . . ? F3_5 C2_5 F2_5 107.8(12) . . ? F1_5 C2_5 C1_5 109.8(11) . . ? F3_5 C2_5 C1_5 110.6(11) . . ? F2_5 C2_5 C1_5 111.5(12) . . ? F4_5 C3_5 F5_5 106.5(13) . . ? F4_5 C3_5 F6_5 106.4(13) . . ? F5_5 C3_5 F6_5 107.6(12) . . ? F4_5 C3_5 C1_5 111.9(11) . . ? F5_5 C3_5 C1_5 110.5(11) . . ? F6_5 C3_5 C1_5 113.6(11) . . ? F9_5 C4_5 F7_5 106.6(13) . . ? F9_5 C4_5 F8_5 107.7(13) . . ? F7_5 C4_5 F8_5 107.9(12) . . ? F9_5 C4_5 C1_5 111.4(11) . . ? F7_5 C4_5 C1_5 111.1(10) . . ? F8_5 C4_5 C1_5 111.9(11) . . ? C1_8 O1_8 Al1 148.3(15) . . ? O1_8 C1_8 C2_8 109.8(13) . . ? O1_8 C1_8 C4_8 110.9(14) . . ? C2_8 C1_8 C4_8 110.9(11) . . ? O1_8 C1_8 C3_8 109.2(18) . . ? C2_8 C1_8 C3_8 108.5(12) . . ? C4_8 C1_8 C3_8 107.5(12) . . ? F1_8 C2_8 F2_8 107.7(19) . . ? F1_8 C2_8 F3_8 106(2) . . ? F2_8 C2_8 F3_8 107.4(16) . . ? F1_8 C2_8 C1_8 113.2(14) . . ? F2_8 C2_8 C1_8 112.6(13) . . ? F3_8 C2_8 C1_8 109.1(13) . . ? F4_8 C3_8 F6_8 107.9(16) . . ? F4_8 C3_8 F5_8 110.6(18) . . ? F6_8 C3_8 F5_8 107.2(17) . . ? F4_8 C3_8 C1_8 109.4(14) . . ? F6_8 C3_8 C1_8 111.0(15) . . ? F5_8 C3_8 C1_8 110.7(15) . . ? F9_8 C4_8 F8_8 107.6(16) . . ? F9_8 C4_8 F7_8 109.3(18) . . ? F8_8 C4_8 F7_8 106.7(15) . . ? F9_8 C4_8 C1_8 109.6(14) . . ? F8_8 C4_8 C1_8 112.5(14) . . ? F7_8 C4_8 C1_8 111.0(13) . . ? C1_9 O1_9 Al1 153(2) . . ? O1_9 C1_9 C4_9 110.9(15) . . ? O1_9 C1_9 C2_9 110.0(15) . . ? C4_9 C1_9 C2_9 109.1(11) . . ? O1_9 C1_9 C3_9 109.9(19) . . ? C4_9 C1_9 C3_9 107.6(11) . . ? C2_9 C1_9 C3_9 109.4(12) . . ? F2_9 C2_9 F3_9 109.0(15) . . ? F2_9 C2_9 F1_9 109.4(17) . . ? F3_9 C2_9 F1_9 105.0(17) . . ? F2_9 C2_9 C1_9 111.9(14) . . ? F3_9 C2_9 C1_9 111.8(13) . . ? F1_9 C2_9 C1_9 109.5(14) . . ? F5_9 C3_9 F4_9 106.5(17) . . ? F5_9 C3_9 F6_9 109.6(18) . . ? F4_9 C3_9 F6_9 108.8(17) . . ? F5_9 C3_9 C1_9 111.3(15) . . ? F4_9 C3_9 C1_9 110.5(16) . . ? F6_9 C3_9 C1_9 110.1(15) . . ? F9_9 C4_9 F7_9 107.3(17) . . ? F9_9 C4_9 F8_9 108.3(16) . . ? F7_9 C4_9 F8_9 108.2(15) . . ? F9_9 C4_9 C1_9 110.8(14) . . ? F7_9 C4_9 C1_9 110.8(14) . . ? F8_9 C4_9 C1_9 111.2(14) . . ? C1_10 O1_10 Al1 149.4(14) . . ? O1_10 C1_10 C4_10 111.7(12) . . ? O1_10 C1_10 C3_10 113.2(12) . . ? C4_10 C1_10 C3_10 111.0(11) . . ? O1_10 C1_10 C2_10 107.6(13) . . ? C4_10 C1_10 C2_10 106.0(11) . . ? C3_10 C1_10 C2_10 106.9(11) . . ? F2_10 C2_10 F3_10 108.2(16) . . ? F2_10 C2_10 F1_10 106.1(16) . . ? F3_10 C2_10 F1_10 112.2(16) . . ? F2_10 C2_10 C1_10 112.1(14) . . ? F3_10 C2_10 C1_10 109.3(13) . . ? F1_10 C2_10 C1_10 109.0(14) . . ? F5_10 C3_10 F4_10 119.0(17) . . ? F5_10 C3_10 F6_10 104.9(14) . . ? F4_10 C3_10 F6_10 98.4(14) . . ? F5_10 C3_10 C1_10 107.5(12) . . ? F4_10 C3_10 C1_10 113.8(14) . . ? F6_10 C3_10 C1_10 112.7(13) . . ? F8_10 C4_10 F9_10 101.4(14) . . ? F8_10 C4_10 F7_10 115.0(15) . . ? F9_10 C4_10 F7_10 109.2(16) . . ? F8_10 C4_10 C1_10 110.8(12) . . ? F9_10 C4_10 C1_10 111.7(13) . . ? F7_10 C4_10 C1_10 108.6(13) . . ? C1_11 O1_11 Al1 146(2) . . ? O1_11 C1_11 C2_11 107.9(16) . . ? O1_11 C1_11 C4_11 108.9(17) . . ? C2_11 C1_11 C4_11 111.6(13) . . ? O1_11 C1_11 C3_11 106.7(16) . . ? C2_11 C1_11 C3_11 111.3(13) . . ? C4_11 C1_11 C3_11 110.1(13) . . ? F2_11 C2_11 F3_11 104.1(18) . . ? F2_11 C2_11 F1_11 105.9(17) . . ? F3_11 C2_11 F1_11 108.3(19) . . ? F2_11 C2_11 C1_11 114.0(16) . . ? F3_11 C2_11 C1_11 113.6(17) . . ? F1_11 C2_11 C1_11 110.5(15) . . ? F6_11 C3_11 F5_11 108.5(18) . . ? F6_11 C3_11 F4_11 108.0(18) . . ? F5_11 C3_11 F4_11 104.5(18) . . ? F6_11 C3_11 C1_11 115.4(16) . . ? F5_11 C3_11 C1_11 109.3(15) . . ? F4_11 C3_11 C1_11 110.5(16) . . ? F7_11 C4_11 F9_11 107.4(19) . . ? F7_11 C4_11 F8_11 107.1(18) . . ? F9_11 C4_11 F8_11 109.3(18) . . ? F7_11 C4_11 C1_11 111.1(16) . . ? F9_11 C4_11 C1_11 110.5(15) . . ? F8_11 C4_11 C1_11 111.3(16) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_5 Al1 O1_3 C1_3 -144(3) . . . . ? O1_7 Al1 O1_3 C1_3 83(3) . . . . ? Al1 O1_3 C1_3 C4_3 -171(2) . . . . ? Al1 O1_3 C1_3 C2_3 -55(3) . . . . ? Al1 O1_3 C1_3 C3_3 68(3) . . . . ? O1_3 C1_3 C2_3 F1_3 -70.5(17) . . . . ? C4_3 C1_3 C2_3 F1_3 46.2(16) . . . . ? C3_3 C1_3 C2_3 F1_3 166.3(14) . . . . ? O1_3 C1_3 C2_3 F3_3 51.0(16) . . . . ? C4_3 C1_3 C2_3 F3_3 167.7(13) . . . . ? C3_3 C1_3 C2_3 F3_3 -72.2(15) . . . . ? O1_3 C1_3 C2_3 F2_3 171.1(14) . . . . ? C4_3 C1_3 C2_3 F2_3 -72.2(14) . . . . ? C3_3 C1_3 C2_3 F2_3 47.9(15) . . . . ? O1_3 C1_3 C3_3 F6_3 158.1(13) . . . . ? C4_3 C1_3 C3_3 F6_3 38.5(16) . . . . ? C2_3 C1_3 C3_3 F6_3 -80.8(15) . . . . ? O1_3 C1_3 C3_3 F5_3 -77.4(15) . . . . ? C4_3 C1_3 C3_3 F5_3 162.9(14) . . . . ? C2_3 C1_3 C3_3 F5_3 43.6(16) . . . . ? O1_3 C1_3 C3_3 F4_3 39.3(15) . . . . ? C4_3 C1_3 C3_3 F4_3 -80.3(14) . . . . ? C2_3 C1_3 C3_3 F4_3 160.4(13) . . . . ? O1_3 C1_3 C4_3 F9_3 45.1(17) . . . . ? C2_3 C1_3 C4_3 F9_3 -71.7(15) . . . . ? C3_3 C1_3 C4_3 F9_3 167.1(13) . . . . ? O1_3 C1_3 C4_3 F7_3 -77.5(15) . . . . ? C2_3 C1_3 C4_3 F7_3 165.7(12) . . . . ? C3_3 C1_3 C4_3 F7_3 44.5(15) . . . . ? O1_3 C1_3 C4_3 F8_3 162.6(14) . . . . ? C2_3 C1_3 C4_3 F8_3 45.8(14) . . . . ? C3_3 C1_3 C4_3 F8_3 -75.5(14) . . . . ? O1_8 Al1 O1_6 C1_6 -149(5) . . . . ? O1_9 Al1 O1_6 C1_6 90(5) . . . . ? Al1 O1_6 C1_6 C2_6 -64(5) . . . . ? Al1 O1_6 C1_6 C4_6 174(4) . . . . ? Al1 O1_6 C1_6 C3_6 56(5) . . . . ? O1_6 C1_6 C2_6 F3_6 42(2) . . . . ? C4_6 C1_6 C2_6 F3_6 166.4(18) . . . . ? C3_6 C1_6 C2_6 F3_6 -79(2) . . . . ? O1_6 C1_6 C2_6 F1_6 -77(2) . . . . ? C4_6 C1_6 C2_6 F1_6 47(2) . . . . ? C3_6 C1_6 C2_6 F1_6 161.2(19) . . . . ? O1_6 C1_6 C2_6 F2_6 160(2) . . . . ? C4_6 C1_6 C2_6 F2_6 -76(2) . . . . ? C3_6 C1_6 C2_6 F2_6 39(2) . . . . ? O1_6 C1_6 C3_6 F6_6 159(2) . . . . ? C2_6 C1_6 C3_6 F6_6 -78(2) . . . . ? C4_6 C1_6 C3_6 F6_6 38(2) . . . . ? O1_6 C1_6 C3_6 F5_6 -82(2) . . . . ? C2_6 C1_6 C3_6 F5_6 41(2) . . . . ? C4_6 C1_6 C3_6 F5_6 157(2) . . . . ? O1_6 C1_6 C3_6 F4_6 39(2) . . . . ? C2_6 C1_6 C3_6 F4_6 162.1(19) . . . . ? C4_6 C1_6 C3_6 F4_6 -82(2) . . . . ? O1_6 C1_6 C4_6 F9_6 44(3) . . . . ? C2_6 C1_6 C4_6 F9_6 -80(2) . . . . ? C3_6 C1_6 C4_6 F9_6 164.1(19) . . . . ? O1_6 C1_6 C4_6 F7_6 -77(2) . . . . ? C2_6 C1_6 C4_6 F7_6 158.6(19) . . . . ? C3_6 C1_6 C4_6 F7_6 43(2) . . . . ? O1_6 C1_6 C4_6 F8_6 161(2) . . . . ? C2_6 C1_6 C4_6 F8_6 37(2) . . . . ? C3_6 C1_6 C4_6 F8_6 -79(2) . . . . ? O1_5 Al1 O1_7 C1_7 -51(3) . . . . ? O1_3 Al1 O1_7 C1_7 75(2) . . . . ? Al1 O1_7 C1_7 C2_7 -162(2) . . . . ? Al1 O1_7 C1_7 C3_7 -41(3) . . . . ? Al1 O1_7 C1_7 C4_7 78(2) . . . . ? O1_7 C1_7 C2_7 F3_7 47.2(14) . . . . ? C3_7 C1_7 C2_7 F3_7 -75.8(12) . . . . ? C4_7 C1_7 C2_7 F3_7 166.9(10) . . . . ? O1_7 C1_7 C2_7 F2_7 169.1(12) . . . . ? C3_7 C1_7 C2_7 F2_7 46.2(12) . . . . ? C4_7 C1_7 C2_7 F2_7 -71.1(12) . . . . ? O1_7 C1_7 C2_7 F1_7 -71.2(13) . . . . ? C3_7 C1_7 C2_7 F1_7 165.8(10) . . . . ? C4_7 C1_7 C2_7 F1_7 48.5(12) . . . . ? O1_7 C1_7 C3_7 F6_7 161.9(11) . . . . ? C2_7 C1_7 C3_7 F6_7 -75.9(12) . . . . ? C4_7 C1_7 C3_7 F6_7 42.4(12) . . . . ? O1_7 C1_7 C3_7 F4_7 44.7(13) . . . . ? C2_7 C1_7 C3_7 F4_7 166.8(9) . . . . ? C4_7 C1_7 C3_7 F4_7 -74.9(11) . . . . ? O1_7 C1_7 C3_7 F5_7 -71.3(13) . . . . ? C2_7 C1_7 C3_7 F5_7 50.9(12) . . . . ? C4_7 C1_7 C3_7 F5_7 169.1(10) . . . . ? O1_7 C1_7 C4_7 F9_7 45.3(14) . . . . ? C2_7 C1_7 C4_7 F9_7 -75.6(13) . . . . ? C3_7 C1_7 C4_7 F9_7 166.8(11) . . . . ? O1_7 C1_7 C4_7 F7_7 -80.9(13) . . . . ? C2_7 C1_7 C4_7 F7_7 158.3(11) . . . . ? C3_7 C1_7 C4_7 F7_7 40.7(13) . . . . ? O1_7 C1_7 C4_7 F8_7 160.5(11) . . . . ? C2_7 C1_7 C4_7 F8_7 39.6(13) . . . . ? C3_7 C1_7 C4_7 F8_7 -78.0(12) . . . . ? O1_7 Al1 O1_5 C1_5 87(2) . . . . ? O1_3 Al1 O1_5 C1_5 -40(3) . . . . ? Al1 O1_5 C1_5 C3_5 -52(3) . . . . ? Al1 O1_5 C1_5 C2_5 68(3) . . . . ? Al1 O1_5 C1_5 C4_5 -173(2) . . . . ? O1_5 C1_5 C2_5 F1_5 42.0(15) . . . . ? C3_5 C1_5 C2_5 F1_5 164.1(11) . . . . ? C4_5 C1_5 C2_5 F1_5 -76.0(13) . . . . ? O1_5 C1_5 C2_5 F3_5 -78.2(14) . . . . ? C3_5 C1_5 C2_5 F3_5 43.9(13) . . . . ? C4_5 C1_5 C2_5 F3_5 163.7(11) . . . . ? O1_5 C1_5 C2_5 F2_5 161.8(13) . . . . ? C3_5 C1_5 C2_5 F2_5 -76.1(14) . . . . ? C4_5 C1_5 C2_5 F2_5 43.7(15) . . . . ? O1_5 C1_5 C3_5 F4_5 -73.6(14) . . . . ? C2_5 C1_5 C3_5 F4_5 164.7(11) . . . . ? C4_5 C1_5 C3_5 F4_5 45.8(14) . . . . ? O1_5 C1_5 C3_5 F5_5 45.0(16) . . . . ? C2_5 C1_5 C3_5 F5_5 -76.8(14) . . . . ? C4_5 C1_5 C3_5 F5_5 164.3(12) . . . . ? O1_5 C1_5 C3_5 F6_5 165.9(13) . . . . ? C2_5 C1_5 C3_5 F6_5 44.2(14) . . . . ? C4_5 C1_5 C3_5 F6_5 -74.7(14) . . . . ? O1_5 C1_5 C4_5 F9_5 -72.5(15) . . . . ? C3_5 C1_5 C4_5 F9_5 166.2(12) . . . . ? C2_5 C1_5 C4_5 F9_5 47.2(15) . . . . ? O1_5 C1_5 C4_5 F7_5 46.2(15) . . . . ? C3_5 C1_5 C4_5 F7_5 -75.1(13) . . . . ? C2_5 C1_5 C4_5 F7_5 165.9(11) . . . . ? O1_5 C1_5 C4_5 F8_5 166.8(14) . . . . ? C3_5 C1_5 C4_5 F8_5 45.5(15) . . . . ? C2_5 C1_5 C4_5 F8_5 -73.4(14) . . . . ? O1_6 Al1 O1_8 C1_8 -103(6) . . . . ? O1_9 Al1 O1_8 C1_8 18(6) . . . . ? Al1 O1_8 C1_8 C2_8 -170(5) . . . . ? Al1 O1_8 C1_8 C4_8 -47(6) . . . . ? Al1 O1_8 C1_8 C3_8 71(6) . . . . ? O1_8 C1_8 C2_8 F1_8 73(2) . . . . ? C4_8 C1_8 C2_8 F1_8 -50(2) . . . . ? C3_8 C1_8 C2_8 F1_8 -167.8(18) . . . . ? O1_8 C1_8 C2_8 F2_8 -165(2) . . . . ? C4_8 C1_8 C2_8 F2_8 73(2) . . . . ? C3_8 C1_8 C2_8 F2_8 -45(2) . . . . ? O1_8 C1_8 C2_8 F3_8 -45(3) . . . . ? C4_8 C1_8 C2_8 F3_8 -168(2) . . . . ? C3_8 C1_8 C2_8 F3_8 74(2) . . . . ? O1_8 C1_8 C3_8 F4_8 -40.2(18) . . . . ? C2_8 C1_8 C3_8 F4_8 -159.8(16) . . . . ? C4_8 C1_8 C3_8 F4_8 80.2(17) . . . . ? O1_8 C1_8 C3_8 F6_8 -159.1(16) . . . . ? C2_8 C1_8 C3_8 F6_8 81.2(18) . . . . ? C4_8 C1_8 C3_8 F6_8 -38.7(18) . . . . ? O1_8 C1_8 C3_8 F5_8 82.0(19) . . . . ? C2_8 C1_8 C3_8 F5_8 -38(2) . . . . ? C4_8 C1_8 C3_8 F5_8 -157.6(17) . . . . ? O1_8 C1_8 C4_8 F9_8 -41(2) . . . . ? C2_8 C1_8 C4_8 F9_8 80.8(18) . . . . ? C3_8 C1_8 C4_8 F9_8 -160.8(16) . . . . ? O1_8 C1_8 C4_8 F8_8 -161(2) . . . . ? C2_8 C1_8 C4_8 F8_8 -39(2) . . . . ? C3_8 C1_8 C4_8 F8_8 79.6(18) . . . . ? O1_8 C1_8 C4_8 F7_8 79(2) . . . . ? C2_8 C1_8 C4_8 F7_8 -158.4(16) . . . . ? C3_8 C1_8 C4_8 F7_8 -40.0(18) . . . . ? O1_8 Al1 O1_9 C1_9 -154(6) . . . . ? O1_6 Al1 O1_9 C1_9 -45(7) . . . . ? Al1 O1_9 C1_9 C4_9 -178(6) . . . . ? Al1 O1_9 C1_9 C2_9 -57(7) . . . . ? Al1 O1_9 C1_9 C3_9 63(6) . . . . ? O1_9 C1_9 C2_9 F2_9 159(2) . . . . ? C4_9 C1_9 C2_9 F2_9 -78.9(18) . . . . ? C3_9 C1_9 C2_9 F2_9 38.5(19) . . . . ? O1_9 C1_9 C2_9 F3_9 37(2) . . . . ? C4_9 C1_9 C2_9 F3_9 158.5(17) . . . . ? C3_9 C1_9 C2_9 F3_9 -84.0(18) . . . . ? O1_9 C1_9 C2_9 F1_9 -79(2) . . . . ? C4_9 C1_9 C2_9 F1_9 42.5(19) . . . . ? C3_9 C1_9 C2_9 F1_9 160.0(17) . . . . ? O1_9 C1_9 C3_9 F5_9 -80(2) . . . . ? C4_9 C1_9 C3_9 F5_9 158.7(16) . . . . ? C2_9 C1_9 C3_9 F5_9 40.3(18) . . . . ? O1_9 C1_9 C3_9 F4_9 38(2) . . . . ? C4_9 C1_9 C3_9 F4_9 -83.1(18) . . . . ? C2_9 C1_9 C3_9 F4_9 158.5(17) . . . . ? O1_9 C1_9 C3_9 F6_9 158(2) . . . . ? C4_9 C1_9 C3_9 F6_9 37(2) . . . . ? C2_9 C1_9 C3_9 F6_9 -81.4(19) . . . . ? O1_9 C1_9 C4_9 F9_9 46(2) . . . . ? C2_9 C1_9 C4_9 F9_9 -75.3(18) . . . . ? C3_9 C1_9 C4_9 F9_9 166.1(16) . . . . ? O1_9 C1_9 C4_9 F7_9 -73(2) . . . . ? C2_9 C1_9 C4_9 F7_9 165.7(16) . . . . ? C3_9 C1_9 C4_9 F7_9 47.1(18) . . . . ? O1_9 C1_9 C4_9 F8_9 167(2) . . . . ? C2_9 C1_9 C4_9 F8_9 45.3(18) . . . . ? C3_9 C1_9 C4_9 F8_9 -73.3(18) . . . . ? Al1 O1_10 C1_10 C4_10 178(3) . . . . ? Al1 O1_10 C1_10 C3_10 52(4) . . . . ? Al1 O1_10 C1_10 C2_10 -66(3) . . . . ? O1_10 C1_10 C2_10 F2_10 -167.3(17) . . . . ? C4_10 C1_10 C2_10 F2_10 -47.7(18) . . . . ? C3_10 C1_10 C2_10 F2_10 70.8(17) . . . . ? O1_10 C1_10 C2_10 F3_10 72.7(17) . . . . ? C4_10 C1_10 C2_10 F3_10 -167.6(15) . . . . ? C3_10 C1_10 C2_10 F3_10 -49.1(17) . . . . ? O1_10 C1_10 C2_10 F1_10 -50.2(18) . . . . ? C4_10 C1_10 C2_10 F1_10 69.5(17) . . . . ? C3_10 C1_10 C2_10 F1_10 -172.0(15) . . . . ? O1_10 C1_10 C3_10 F5_10 -56.5(19) . . . . ? C4_10 C1_10 C3_10 F5_10 176.9(15) . . . . ? C2_10 C1_10 C3_10 F5_10 61.7(17) . . . . ? O1_10 C1_10 C3_10 F4_10 77.4(19) . . . . ? C4_10 C1_10 C3_10 F4_10 -49.2(18) . . . . ? C2_10 C1_10 C3_10 F4_10 -164.3(15) . . . . ? O1_10 C1_10 C3_10 F6_10 -171.7(17) . . . . ? C4_10 C1_10 C3_10 F6_10 61.7(17) . . . . ? C2_10 C1_10 C3_10 F6_10 -53.4(17) . . . . ? O1_10 C1_10 C4_10 F8_10 175.8(17) . . . . ? C3_10 C1_10 C4_10 F8_10 -56.8(17) . . . . ? C2_10 C1_10 C4_10 F8_10 58.9(16) . . . . ? O1_10 C1_10 C4_10 F9_10 63.5(19) . . . . ? C3_10 C1_10 C4_10 F9_10 -169.1(15) . . . . ? C2_10 C1_10 C4_10 F9_10 -53.4(17) . . . . ? O1_10 C1_10 C4_10 F7_10 -57.0(19) . . . . ? C3_10 C1_10 C4_10 F7_10 70.4(17) . . . . ? C2_10 C1_10 C4_10 F7_10 -173.9(15) . . . . ? Al1 O1_11 C1_11 C2_11 -7(5) . . . . ? Al1 O1_11 C1_11 C4_11 -129(4) . . . . ? Al1 O1_11 C1_11 C3_11 113(4) . . . . ? O1_11 C1_11 C2_11 F2_11 -164(2) . . . . ? C4_11 C1_11 C2_11 F2_11 -45(2) . . . . ? C3_11 C1_11 C2_11 F2_11 79(2) . . . . ? O1_11 C1_11 C2_11 F3_11 77(3) . . . . ? C4_11 C1_11 C2_11 F3_11 -164(2) . . . . ? C3_11 C1_11 C2_11 F3_11 -40(2) . . . . ? O1_11 C1_11 C2_11 F1_11 -45(2) . . . . ? C4_11 C1_11 C2_11 F1_11 74(2) . . . . ? C3_11 C1_11 C2_11 F1_11 -162.1(19) . . . . ? O1_11 C1_11 C3_11 F6_11 -162(2) . . . . ? C2_11 C1_11 C3_11 F6_11 -44(2) . . . . ? C4_11 C1_11 C3_11 F6_11 80(2) . . . . ? O1_11 C1_11 C3_11 F5_11 -39(2) . . . . ? C2_11 C1_11 C3_11 F5_11 78(2) . . . . ? C4_11 C1_11 C3_11 F5_11 -157(2) . . . . ? O1_11 C1_11 C3_11 F4_11 75(2) . . . . ? C2_11 C1_11 C3_11 F4_11 -167.3(19) . . . . ? C4_11 C1_11 C3_11 F4_11 -43(2) . . . . ? O1_11 C1_11 C4_11 F7_11 -42(2) . . . . ? C2_11 C1_11 C4_11 F7_11 -161(2) . . . . ? C3_11 C1_11 C4_11 F7_11 75(2) . . . . ? O1_11 C1_11 C4_11 F9_11 78(2) . . . . ? C2_11 C1_11 C4_11 F9_11 -42(2) . . . . ? C3_11 C1_11 C4_11 F9_11 -165.7(19) . . . . ? O1_11 C1_11 C4_11 F8_11 -161(2) . . . . ? C2_11 C1_11 C4_11 F8_11 80(2) . . . . ? C3_11 C1_11 C4_11 F8_11 -44(2) . . . . ? _shelx_res_file ; REM Best SHELXD solution FINAL CC 77.99 REM Fragments: 14 1 1 1 1 1 REM TITL pnma2 in Pnma 065_xm.res created by SHELXL-2018/3 at 15:04:37 on 22-Feb-2022 CELL 0.71073 18.58120 13.75590 16.81650 90.0000 90.0000 90.0000 ZERR 4.00 0.00340 0.00200 0.00320 0.0000 0.0000 0.0000 LATT 1 SYMM 0.5-X, -Y, 0.5+Z SYMM -X, 0.5+Y, -Z SYMM 0.5+X, 0.5-Y, 0.5-Z SFAC C O F AL RU I UNIT 88 40 144 4 8 12 SIMU 0.02 0.04 2 O1_3 C1_3 C2_3 F1_3 F2_3 F3_3 C3_3 F4_3 F5_3 F6_3 = C4_3 F7_3 F8_3 F9_3 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 RIGU 0.002 0.002 O1_3 C1_3 C2_3 F1_3 F2_3 F3_3 C3_3 F4_3 F5_3 F6_3 = C4_3 F7_3 F8_3 F9_3 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 SIMU 0.02 0.04 2 O1_5 C1_5 C2_5 F1_5 F2_5 F3_5 C3_5 F4_5 F5_5 F6_5 = C4_5 F7_5 F8_5 F9_5 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 RIGU 0.002 0.002 O1_5 C1_5 C2_5 F1_5 F2_5 F3_5 C3_5 F4_5 F5_5 F6_5 = C4_5 F7_5 F8_5 F9_5 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 SIMU 0.02 0.04 2 O1_6 C1_6 C2_6 F1_6 F2_6 F3_6 C3_6 F4_6 F5_6 F6_6 = C4_6 F7_6 F8_6 F9_6 O1_7 C1_7 C2_7 F1_7 F2_7 F3_7 C3_7 F4_7 F5_7 F6_7 = C4_7 F7_7 F8_7 F9_7 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 F4_10 = F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_11 C1_11 C2_11 F1_11 F2_11 F3_11 = C3_11 F4_11 F5_11 F6_11 C4_11 F7_11 F8_11 F9_11 RIGU 0.002 0.002 O1_6 C1_6 C2_6 F1_6 F2_6 F3_6 C3_6 F4_6 F5_6 F6_6 = C4_6 F7_6 F8_6 F9_6 O1_7 C1_7 C2_7 F1_7 F2_7 F3_7 C3_7 F4_7 F5_7 F6_7 = C4_7 F7_7 F8_7 F9_7 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 F4_10 = F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_11 C1_11 C2_11 F1_11 F2_11 F3_11 = C3_11 F4_11 F5_11 F6_11 C4_11 F7_11 F8_11 F9_11 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 OMIT 7 7 5 OMIT 4 4 2 OMIT 26 7 0 BOND $H CONF MORE -1 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -164.150 L.S. 10 PLAN 20 LIST 4 ACTA SUMP 1 0.00001 1 6 1 7 1 8 1 9 WGHT 0.000000 46.939499 FVAR 0.03814 0.00000 0.00000 0.65024 0.64555 0.16253 0.44231 FVAR 0.23814 0.15701 I1 6 0.968322 0.250000 0.060337 10.50000 0.02954 0.04125 = 0.02246 0.00000 0.00153 0.00000 I2 6 0.931535 0.385802 -0.126529 11.00000 0.02748 0.02608 = 0.03636 0.00780 0.00288 0.00440 RU1 5 1.032435 0.250000 -0.085329 10.50000 0.01792 0.02125 = 0.02628 0.00000 0.00258 0.00000 RU2 5 0.854487 0.250000 -0.042742 10.50000 0.01684 0.02415 = 0.03643 0.00000 0.00167 0.00000 AL1 4 0.900830 0.250000 0.401098 10.50000 0.01657 0.02080 = 0.03165 0.00000 -0.00202 0.00000 O1 2 1.129403 0.086114 -0.028957 11.00000 0.03762 0.04103 = 0.06835 0.01305 -0.00138 0.01245 O2 2 1.092362 0.250000 -0.253642 10.50000 0.04620 0.05731 = 0.04057 0.00000 0.02078 0.00000 O3 2 0.781230 0.090690 0.053265 11.00000 0.03488 0.03665 = 0.07110 0.00316 0.01536 -0.00545 O4 2 0.736908 0.250000 -0.168311 10.50000 0.03505 0.07567 = 0.09083 0.00000 -0.03025 0.00000 C1 1 1.094394 0.147835 -0.050657 11.00000 0.02385 0.03170 = 0.04457 0.00240 0.00105 0.00273 C2 1 1.070604 0.250000 -0.191775 10.50000 0.02676 0.02830 = 0.03765 0.00000 0.01253 0.00000 C3 1 0.808337 0.148955 0.016882 11.00000 0.02566 0.02630 = 0.05480 -0.00045 0.01064 0.00104 C4 1 0.780381 0.250000 -0.121954 10.50000 0.02720 0.04523 = 0.05989 0.00000 -0.01311 0.00000 RESI CCF3 1 PART 1 11 PART 0 RESI 0 RESI CCF3 2 RESI 0 RESI CCF3 3 PART -2 40.5 O1 2 0.891975 0.263582 0.506102 40.50000 0.02489 0.03968 = 0.03033 -0.00164 -0.00104 -0.01183 C1 1 0.854668 0.249837 0.573730 40.50000 0.02746 0.03178 = 0.02549 0.00114 -0.00491 -0.00330 C2 1 0.778157 0.292808 0.562023 40.50000 0.02648 0.03763 = 0.03647 0.00198 -0.00198 -0.00016 F1 3 0.780222 0.388785 0.559293 40.50000 0.02830 0.03688 = 0.13627 -0.00021 -0.00767 0.00401 F2 3 0.733045 0.271454 0.620878 40.50000 0.03233 0.09552 = 0.03629 0.01064 0.00366 0.00576 F3 3 0.748048 0.259746 0.495636 40.50000 0.02614 0.06039 = 0.03526 0.00746 -0.00819 -0.00040 C3 1 0.851180 0.140659 0.597243 40.50000 0.04683 0.03675 = 0.06366 0.01698 -0.00567 -0.00535 F4 3 0.916100 0.100758 0.581271 40.50000 0.05619 0.05096 = 0.07707 0.03941 -0.00047 0.01228 F5 3 0.802573 0.095296 0.552231 40.50000 0.06055 0.03962 = 0.09670 0.00435 -0.00894 -0.01858 F6 3 0.837954 0.123516 0.672929 40.50000 0.09358 0.06783 = 0.07111 0.03500 0.01029 -0.00875 C4 1 0.892437 0.307968 0.640847 40.50000 0.04452 0.05864 = 0.03419 -0.00952 -0.01185 -0.00874 F7 3 0.950579 0.262895 0.666730 40.50000 0.04640 0.08978 = 0.05079 0.00370 -0.02467 -0.01117 F8 3 0.845496 0.317800 0.701500 40.50000 0.08898 0.08694 = 0.03491 -0.01926 0.00543 -0.00056 F9 3 0.910645 0.396423 0.619490 40.50000 0.08175 0.05852 = 0.04688 -0.01567 -0.02208 -0.02576 PART 0 RESI 0 RESI CCF3 4 PART 0 RESI 0 RESI CCF3 6 PART -1 61 O1 2 0.862391 0.359316 0.375266 61.00000 0.03899 0.02432 = 0.03114 -0.00172 0.00337 0.01046 C1 1 0.836977 0.416660 0.318149 61.00000 0.04177 0.03239 = 0.03954 0.00710 0.00145 0.00775 C2 1 0.895866 0.447376 0.257758 61.00000 0.05101 0.03821 = 0.03939 0.00334 0.00451 -0.00086 F1 3 0.939432 0.517464 0.284500 61.00000 0.04687 0.03325 = 0.04443 0.00362 0.00570 0.00064 F2 3 0.863843 0.476782 0.190695 61.00000 0.06464 0.03801 = 0.04014 0.00298 -0.00195 -0.00368 F3 3 0.938931 0.374528 0.237823 61.00000 0.04757 0.04054 = 0.03642 0.00014 0.00736 -0.00345 C3 1 0.776113 0.362652 0.270962 61.00000 0.04342 0.04054 = 0.04341 0.00877 -0.00322 0.00631 F4 3 0.735139 0.310698 0.320052 61.00000 0.04026 0.04260 = 0.04409 0.00838 -0.00423 0.00479 F5 3 0.802951 0.303709 0.215890 61.00000 0.05202 0.05233 = 0.04750 -0.00284 -0.00412 0.00266 F6 3 0.733539 0.424827 0.233442 61.00000 0.05031 0.05517 = 0.05081 0.01667 -0.00722 0.01062 C4 1 0.801980 0.510346 0.352890 61.00000 0.05064 0.03813 = 0.04894 0.00325 -0.00297 0.01745 F7 3 0.737560 0.493154 0.382702 61.00000 0.05310 0.06147 = 0.03947 -0.00070 0.00068 0.02137 F8 3 0.797058 0.578200 0.296647 61.00000 0.05676 0.03880 = 0.07420 0.01558 -0.00930 0.01268 F9 3 0.842521 0.547864 0.409248 61.00000 0.06439 0.03801 = 0.06261 -0.00719 -0.01009 0.01710 PART 0 RESI 0 RESI CCF3 7 PART -2 71 O1 2 0.854702 0.340948 0.352127 71.00000 0.03846 0.02394 = 0.04815 0.01521 -0.00961 0.00079 C1 1 0.847942 0.432940 0.328351 71.00000 0.03592 0.02236 = 0.02821 0.00932 -0.00333 0.00348 C2 1 0.768987 0.454982 0.304528 71.00000 0.04120 0.04293 = 0.05424 0.00700 -0.00804 0.01136 F1 3 0.754810 0.408596 0.235997 71.00000 0.05709 0.05544 = 0.06595 0.00050 -0.03065 0.01346 F2 3 0.757347 0.550318 0.293643 71.00000 0.06177 0.04400 = 0.09675 0.01390 -0.01099 0.02211 F3 3 0.724012 0.422042 0.359690 71.00000 0.04283 0.07585 = 0.08947 0.01765 0.01126 0.00789 C3 1 0.870547 0.505755 0.394365 71.00000 0.06303 0.03233 = 0.04129 -0.00056 -0.01238 0.00506 F4 3 0.932325 0.474123 0.426973 71.00000 0.07756 0.02638 = 0.07804 -0.00164 -0.05008 -0.00838 F5 3 0.818634 0.502464 0.451430 71.00000 0.10965 0.10499 = 0.04807 -0.01625 0.01640 0.00888 F6 3 0.884061 0.593282 0.367242 71.00000 0.06989 0.02441 = 0.04998 -0.00513 -0.02664 0.00044 C4 1 0.897921 0.449768 0.255294 71.00000 0.05690 0.03960 = 0.04089 0.00644 0.01150 -0.00489 F7 3 0.965364 0.464989 0.279198 71.00000 0.05298 0.09216 = 0.07338 0.01619 0.01341 -0.01772 F8 3 0.879727 0.527749 0.212010 71.00000 0.10251 0.05994 = 0.05686 0.03019 0.01961 0.00354 F9 3 0.891690 0.377619 0.204392 71.00000 0.10386 0.06532 = 0.05475 -0.01637 0.03737 -0.02305 PART 0 RESI 0 RESI CCF3 5 PART -2 50.5 O1 2 0.989654 0.230129 0.382618 50.50000 0.01703 0.02886 = 0.05783 -0.00192 0.00831 0.00123 C1 1 1.058107 0.252639 0.399966 50.50000 0.01798 0.03461 = 0.06558 -0.00788 0.00484 0.00168 C2 1 1.077575 0.217474 0.485080 50.50000 0.02606 0.05926 = 0.06819 0.00342 0.00107 -0.00103 F1 3 1.050489 0.129474 0.497279 50.50000 0.04151 0.06138 = 0.08771 0.01520 0.00102 -0.00315 F2 3 1.148822 0.212703 0.495513 50.50000 0.02855 0.07343 = 0.08421 -0.00318 -0.00688 0.00132 F3 3 1.051188 0.277873 0.539338 50.50000 0.03030 0.08231 = 0.06595 -0.01235 -0.00705 -0.00304 C3 1 1.070677 0.363840 0.395138 50.50000 0.02143 0.03534 = 0.07557 -0.00990 0.00383 -0.00163 F4 3 1.072184 0.395317 0.320162 50.50000 0.04078 0.03454 = 0.07873 -0.00667 0.00203 -0.00219 F5 3 1.017280 0.411526 0.431103 50.50000 0.02365 0.04171 = 0.09579 -0.02912 0.00529 -0.00324 F6 3 1.132322 0.392713 0.428422 50.50000 0.02250 0.04603 = 0.08224 -0.01245 0.00284 -0.00649 C4 1 1.107379 0.199081 0.339167 50.50000 0.02448 0.03906 = 0.07571 -0.01095 0.01357 0.00235 F7 3 1.082705 0.209274 0.265239 50.50000 0.03938 0.06685 = 0.07190 -0.01176 0.01620 -0.00171 F8 3 1.174694 0.232660 0.340928 50.50000 0.02334 0.05420 = 0.11029 -0.01569 0.01897 -0.00201 F9 3 1.109809 0.104710 0.353454 50.50000 0.03084 0.03647 = 0.11369 -0.01083 0.01317 0.00765 PART 0 RESI 0 RESI CCF3 8 PART -1 -40.5 O1 2 0.864389 0.245294 0.488326 -40.50000 0.01917 0.03563 = 0.02446 -0.00200 0.00202 -0.00565 C1 1 0.871592 0.256146 0.567391 -40.50000 0.03103 0.03758 = 0.02489 -0.00068 -0.00035 -0.00258 C2 1 0.803980 0.216498 0.610089 -40.50000 0.03626 0.05129 = 0.03417 0.00772 0.00742 -0.00247 F1 3 0.800109 0.120463 0.609765 -40.50000 0.06854 0.05190 = 0.04635 0.01094 0.04109 -0.00253 F2 3 0.799569 0.245975 0.685347 -40.50000 0.05060 0.06714 = 0.03362 0.00553 0.01491 -0.00961 F3 3 0.745177 0.248543 0.572409 -40.50000 0.03253 0.09199 = 0.04546 0.02658 0.00954 -0.00051 C3 1 0.879175 0.366599 0.587312 -40.50000 0.04542 0.04014 = 0.03391 -0.00578 -0.00767 -0.00538 F4 3 0.920491 0.408751 0.533422 -40.50000 0.05260 0.04074 = 0.03744 -0.00553 -0.00812 -0.01344 F5 3 0.814791 0.409122 0.590003 -40.50000 0.05492 0.04037 = 0.04109 -0.01474 -0.00638 0.00356 F6 3 0.909657 0.379361 0.657852 -40.50000 0.06061 0.05124 = 0.03481 -0.00553 -0.01330 -0.01120 C4 1 0.940598 0.204379 0.597812 -40.50000 0.03349 0.04754 = 0.03327 0.00284 -0.00636 -0.00183 F7 3 0.999234 0.258385 0.583655 -40.50000 0.03849 0.07347 = 0.04717 0.01679 -0.02225 -0.01722 F8 3 0.938936 0.188032 0.675450 -40.50000 0.04936 0.06123 = 0.03432 0.00718 -0.00514 0.01054 F9 3 0.947462 0.119363 0.561943 -40.50000 0.03968 0.04897 = 0.04154 0.00215 -0.01155 0.00868 PART 0 RESI 0 RESI CCF3 9 PART -1 -50.5 O1 2 0.993565 0.247926 0.401052 -50.50000 0.01786 0.03651 = 0.04763 -0.00520 0.00080 0.00537 C1 1 1.057842 0.267711 0.369460 -50.50000 0.01700 0.04087 = 0.04855 -0.00873 -0.00124 0.00185 C2 1 1.063339 0.222726 0.284878 -50.50000 0.03214 0.05613 = 0.04726 -0.01049 0.00326 0.00011 F1 3 1.077644 0.128230 0.290718 -50.50000 0.05796 0.05503 = 0.05429 -0.01799 0.01398 0.00153 F2 3 1.113916 0.265391 0.241654 -50.50000 0.03910 0.07276 = 0.05444 -0.00280 0.00923 -0.00285 F3 3 1.001189 0.227589 0.246150 -50.50000 0.03707 0.09201 = 0.02471 -0.00155 0.00488 -0.00821 C3 1 1.068547 0.379696 0.363996 -50.50000 0.02492 0.03939 = 0.07343 -0.00286 0.00084 0.00162 F4 3 1.040368 0.423340 0.427237 -50.50000 0.03873 0.03987 = 0.08582 -0.01479 0.00706 -0.00726 F5 3 1.035325 0.416186 0.301120 -50.50000 0.02746 0.06366 = 0.08428 0.02156 0.00611 0.00365 F6 3 1.138406 0.400784 0.360348 -50.50000 0.02543 0.05007 = 0.09819 0.00763 0.00133 -0.00135 C4 1 1.119262 0.226352 0.422066 -50.50000 0.01956 0.04587 = 0.05540 -0.00733 -0.00347 0.00638 F7 3 1.126831 0.278718 0.488272 -50.50000 0.02788 0.05707 = 0.05718 -0.01173 -0.01087 0.00859 F8 3 1.182089 0.226875 0.383273 -50.50000 0.01901 0.05838 = 0.06130 -0.00387 -0.00258 0.00987 F9 3 1.104938 0.135433 0.443950 -50.50000 0.03002 0.04723 = 0.07470 -0.00050 -0.00260 0.00730 PART 0 RESI 0 RESI CCF3 10 PART -3 81 O1 2 0.882051 0.354199 0.343477 81.00000 0.03615 0.03492 = 0.03547 0.01436 0.00756 0.00915 C1 1 0.834164 0.416606 0.313621 81.00000 0.04015 0.03229 = 0.03931 0.00903 0.00287 0.01055 C2 1 0.785614 0.358953 0.252660 81.00000 0.04993 0.03880 = 0.04733 0.00396 -0.00550 0.01011 F1 3 0.827845 0.310394 0.202741 81.00000 0.07521 0.06401 = 0.03835 -0.00383 -0.01087 0.02720 F2 3 0.746371 0.417456 0.208489 81.00000 0.06544 0.04253 = 0.05780 0.00248 -0.01804 0.01302 F3 3 0.741579 0.300567 0.292322 81.00000 0.04740 0.05072 = 0.07216 0.01225 -0.01556 -0.00236 C3 1 0.783037 0.459593 0.377417 81.00000 0.04743 0.03795 = 0.04745 0.00339 0.00801 0.01409 F4 3 0.812806 0.528954 0.421237 81.00000 0.08772 0.03747 = 0.06493 -0.00386 -0.00552 0.01627 F5 3 0.751050 0.386159 0.413373 81.00000 0.05400 0.04569 = 0.08231 0.01812 0.03557 0.02360 F6 3 0.729088 0.512095 0.345615 81.00000 0.05010 0.06528 = 0.06313 0.02157 0.01905 0.02854 C4 1 0.871032 0.498387 0.265085 81.00000 0.04776 0.03712 = 0.04661 0.01426 0.00215 0.00758 F7 3 0.918502 0.543817 0.312118 81.00000 0.06140 0.05402 = 0.08117 0.01467 -0.01663 -0.00781 F8 3 0.822049 0.556151 0.231381 81.00000 0.04643 0.06154 = 0.05284 0.03726 0.00949 0.01386 F9 3 0.905228 0.463265 0.201272 81.00000 0.07760 0.06626 = 0.06107 0.01501 0.02854 0.01351 PART 0 RESI 0 RESI CCF3 11 PART -4 91 O1 2 0.863305 0.353472 0.382230 91.00000 0.03869 0.02792 = 0.03280 0.00147 0.00184 0.01101 C1 1 0.840401 0.415135 0.325441 91.00000 0.04107 0.03377 = 0.03569 0.00673 0.00073 0.00804 C2 1 0.865052 0.374826 0.244111 91.00000 0.05028 0.04399 = 0.03665 0.00330 0.00265 0.00649 F1 3 0.933837 0.346025 0.247619 91.00000 0.05269 0.05729 = 0.03255 0.00473 0.00872 0.01255 F2 3 0.861827 0.438615 0.185826 91.00000 0.06024 0.05453 = 0.02705 0.00074 -0.00629 0.00539 F3 3 0.825329 0.300258 0.218136 91.00000 0.06934 0.05298 = 0.04548 -0.00294 -0.00864 0.00143 C3 1 0.757040 0.418511 0.331432 91.00000 0.04096 0.04163 = 0.04925 0.01130 0.00091 0.01143 F4 3 0.736696 0.471240 0.394267 91.00000 0.04848 0.05125 = 0.05378 0.00925 0.00444 0.02162 F5 3 0.732296 0.329808 0.346390 91.00000 0.04223 0.04592 = 0.08630 0.01437 0.01283 0.00841 F6 3 0.723503 0.452755 0.268216 91.00000 0.05270 0.06484 = 0.05894 0.01153 -0.01316 0.01341 C4 1 0.872359 0.517144 0.341817 91.00000 0.05797 0.03380 = 0.05204 0.00427 -0.00395 0.00408 F7 3 0.870183 0.538252 0.418629 91.00000 0.10193 0.04534 = 0.06066 -0.01277 -0.00805 0.00843 F8 3 0.835428 0.586162 0.303880 91.00000 0.07035 0.04136 = 0.08638 0.01639 -0.00667 0.01109 F9 3 0.940779 0.520651 0.319354 91.00000 0.05419 0.03338 = 0.07251 0.00439 -0.01272 -0.00450 PART 0 RESI 0 HKLF 4 REM pnma2 in Pnma REM wR2 = 0.1107, GooF = S = 1.193, Restrained GooF = 1.035 for all data REM R1 = 0.0528 for 7398 Fo > 4sig(Fo) and 0.0604 for all 8508 data REM 1110 parameters refined using 12323 restraints END WGHT 0.0001 44.4328 REM Highest difference peak 1.513, deepest hole -1.507, 1-sigma level 0.186 Q1 1 1.0083 0.2500 -0.2066 10.50000 0.05 1.51 Q2 1 0.9081 0.4992 0.3557 11.00000 0.05 1.32 Q3 1 0.7966 0.4544 0.4606 11.00000 0.05 1.32 Q4 1 0.8217 0.4543 0.2416 11.00000 0.05 1.16 Q5 1 0.9423 0.3655 -0.1560 11.00000 0.05 1.07 Q6 1 0.7800 0.2500 0.2021 10.50000 0.05 1.04 Q7 1 0.7364 0.3714 0.3824 11.00000 0.05 1.01 Q8 1 0.8354 0.2500 -0.1608 10.50000 0.05 0.98 Q9 1 0.8528 0.2500 -0.0766 10.50000 0.05 0.97 Q10 1 0.9104 0.3887 -0.1245 11.00000 0.05 0.92 Q11 1 0.8474 0.3922 0.1879 11.00000 0.05 0.90 Q12 1 0.9560 0.2500 -0.0201 10.50000 0.05 0.88 Q13 1 0.8112 0.3330 0.6952 11.00000 0.05 0.86 Q14 1 0.8370 0.1539 0.6276 11.00000 0.05 0.85 Q15 1 0.9694 0.2500 -0.1805 10.50000 0.05 0.85 Q16 1 1.0182 0.2500 0.1012 10.50000 0.05 0.85 Q17 1 1.0540 0.2500 0.4187 10.50000 0.05 0.84 Q18 1 0.8692 0.3318 0.3206 11.00000 0.05 0.84 Q19 1 0.9864 0.4808 0.2114 11.00000 0.05 0.82 Q20 1 0.8923 0.5966 0.3208 11.00000 0.05 0.80 ; _shelx_res_checksum 81822 _shelx_hkl_file ; 0 1 0 -0.01 0.03 0 1 0 0.02 0.04 0 1 0 0.00 0.03 0 -1 0 0.01 0.02 0 -1 0 -0.01 0.02 0 2 0 405.75 14.31 0 -2 0 407.45 14.00 0 2 0 416.36 13.34 0 2 0 422.28 14.02 0 2 0 410.09 14.37 0 -2 0 400.99 14.31 0 -3 0 -0.02 0.06 0 3 0 0.14 0.10 0 3 0 -0.04 0.08 0 -3 0 0.01 0.08 0 3 0 -0.03 0.06 0 3 0 0.01 0.03 0 4 0 38.12 1.32 0 -4 0 35.31 1.26 0 -4 0 36.07 1.35 0 4 0 34.29 1.34 0 4 0 34.92 1.33 0 4 0 35.78 1.19 0 5 0 0.14 0.05 0 -5 0 0.15 0.09 0 -5 0 0.24 0.13 0 5 0 0.20 0.09 0 5 0 0.02 0.09 0 5 0 0.10 0.12 0 5 0 0.13 0.14 0 6 0 1000.00 33.71 0 -6 0 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0.03 0.07 0 -2 3 0.04 0.07 0 2 3 0.04 0.07 0 -2 3 0.17 0.11 0 -2 -3 0.09 0.08 0 2 3 -0.06 0.14 0 2 -3 0.13 0.09 0 2 -3 0.07 0.08 0 -2 -3 0.04 0.08 0 -3 3 63.50 2.12 0 -3 -3 59.98 2.12 0 3 3 59.64 2.07 0 3 -3 63.12 2.12 0 -3 3 60.63 2.10 0 3 -3 64.29 2.12 0 -3 3 64.81 2.23 0 -3 3 63.58 2.12 0 -3 3 64.43 2.15 0 3 3 58.78 2.06 0 3 -3 64.59 2.23 0 3 3 61.48 2.23 0 -3 -3 65.28 2.18 0 3 3 61.00 2.17 0 3 3 62.09 2.12 0 3 3 59.40 2.09 0 3 -3 65.88 2.14 0 4 -3 0.50 0.13 0 4 -3 0.70 0.07 0 -4 3 0.41 0.11 0 -4 3 1.18 0.14 0 -4 -3 1.08 0.15 0 4 3 0.68 0.15 0 -4 -3 0.72 0.16 0 4 3 0.98 0.13 0 5 -3 4.35 0.39 0 5 3 3.88 0.23 0 -5 3 5.07 0.25 0 5 3 3.87 0.27 0 5 -3 4.52 0.21 0 -5 3 4.59 0.35 0 5 -3 4.60 0.28 0 -5 -3 4.16 0.29 0 -5 3 4.15 0.28 0 5 -3 4.51 0.32 0 5 3 4.00 0.33 0 -5 -3 4.51 0.34 0 5 3 4.02 0.29 0 -5 3 4.67 0.25 0 5 -3 4.06 0.26 0 6 3 0.20 0.14 0 6 3 0.59 0.11 0 -6 3 0.26 0.16 0 6 -3 0.53 0.13 0 6 3 0.63 0.15 0 6 -3 0.25 0.14 0 6 -3 0.50 0.11 0 -6 3 0.54 0.10 0 -6 -3 0.17 0.13 0 6 -3 0.76 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8 1.41 0.47 27 0 8 0.55 0.33 27 0 -8 0.21 0.40 27 0 8 0.56 0.40 27 1 -8 0.08 0.26 27 -1 8 0.09 0.30 27 -1 8 -0.19 0.25 27 1 -8 -0.28 0.54 27 1 8 0.27 0.30 27 1 8 0.21 0.36 27 1 8 -0.11 0.25 27 -1 -8 0.15 0.40 27 -1 -8 -0.06 0.24 27 -2 8 1.28 0.41 27 2 -8 0.92 0.38 27 -2 8 1.25 0.52 27 2 -8 0.86 0.46 27 -2 8 0.81 0.41 27 2 8 0.81 0.35 27 2 8 1.29 0.42 27 -2 -8 1.08 0.54 27 2 8 1.18 0.52 27 -2 -8 0.76 0.33 28 0 0 18.75 1.19 28 1 0 0.54 0.41 28 -1 0 -0.15 0.34 28 -1 0 0.05 0.24 28 1 0 0.03 0.34 28 2 0 6.64 0.79 28 -2 0 7.71 0.99 28 -2 0 7.02 0.68 28 2 0 7.99 0.98 28 -3 0 1.68 0.38 28 -3 0 1.95 0.57 28 3 0 1.07 0.47 28 3 0 1.14 0.42 28 -4 0 0.74 0.47 28 4 0 0.99 0.66 28 0 -1 -0.10 0.31 28 0 1 -0.09 0.25 28 0 1 0.28 0.55 28 0 -1 -0.04 0.26 28 -1 1 1.21 0.36 28 1 -1 0.90 0.45 28 -1 1 0.71 0.46 28 1 -1 0.77 0.38 28 1 1 1.17 0.50 28 -1 -1 0.93 0.35 28 -1 -1 1.85 0.56 28 -2 1 0.65 0.30 28 -2 1 0.41 0.43 28 2 -1 0.82 0.45 28 2 -1 0.05 0.26 28 2 1 0.69 0.34 28 -2 -1 0.67 0.32 28 -2 -1 0.87 0.49 28 2 1 1.30 0.47 28 3 -1 0.25 0.36 28 3 -1 0.08 0.30 28 -3 1 0.01 0.38 28 -3 1 0.07 0.23 28 -3 -1 0.36 0.42 28 -3 -1 -0.10 0.22 28 3 1 0.01 0.27 28 3 1 0.18 0.35 28 -4 1 1.40 0.57 28 -4 -1 1.68 0.57 28 0 2 2.06 0.46 28 0 -2 2.72 0.64 28 0 -2 2.26 0.48 28 -1 2 0.13 0.38 28 -1 2 0.13 0.27 28 -1 2 0.05 0.23 28 1 -2 0.31 0.36 28 -1 -2 -0.03 0.25 28 -1 -2 0.02 0.32 28 1 2 0.21 0.34 28 2 -2 2.53 0.52 28 -2 2 4.26 0.77 28 -2 2 3.25 0.54 28 -2 2 3.30 0.51 28 2 -2 3.61 0.71 28 -2 -2 4.47 0.78 28 2 2 3.52 0.70 28 -2 -2 3.71 0.54 28 2 2 3.28 0.60 28 -3 2 -0.01 0.34 28 3 -2 0.03 0.34 28 -3 2 -0.03 0.26 28 3 -2 0.04 0.28 28 -3 2 -0.10 0.21 28 3 2 0.12 0.34 28 -3 -2 0.08 0.40 28 3 2 0.13 0.30 28 -3 -2 0.18 0.24 28 -4 2 3.31 0.60 28 0 3 0.90 0.37 28 0 -3 1.13 0.39 28 0 3 0.84 0.32 28 0 -3 1.03 0.56 28 0 3 1.02 0.54 28 -1 3 2.75 0.49 28 -1 3 3.19 0.69 28 1 -3 2.94 0.64 28 -1 -3 2.84 0.65 28 -1 -3 3.31 0.53 28 1 3 3.14 0.56 28 2 -3 3.65 0.63 28 -2 3 3.44 0.52 28 -2 3 3.12 0.57 28 -2 3 3.43 0.71 28 2 -3 3.32 0.70 28 2 3 3.14 0.67 28 -2 -3 3.26 0.51 28 2 3 3.52 0.61 28 -2 -3 3.76 0.74 28 3 -3 -0.01 0.36 28 3 -3 0.08 0.28 28 -3 3 0.10 0.24 28 -3 3 -0.02 0.27 28 -3 3 -0.17 0.37 28 -3 -3 0.53 0.44 28 -3 -3 0.08 0.24 28 3 3 0.24 0.30 28 0 4 1.77 0.56 28 0 -4 1.76 0.45 28 0 4 2.53 0.58 28 1 -4 0.17 0.31 28 -1 4 0.26 0.60 28 -1 4 0.32 0.29 28 -1 4 0.04 0.28 28 1 -4 -0.07 0.36 28 1 4 0.48 0.38 28 1 4 -0.01 0.25 28 1 4 0.06 0.31 28 -1 -4 0.25 0.38 28 -1 -4 0.04 0.26 28 2 -4 -0.21 0.24 28 2 -4 0.05 0.36 28 -2 4 -0.04 0.38 28 -2 4 0.14 0.27 28 -2 4 -0.16 0.26 28 2 4 0.29 0.37 28 2 4 0.09 0.27 28 -2 -4 0.24 0.43 28 -2 -4 -0.11 0.23 28 0 5 3.66 0.58 28 0 5 3.09 0.72 28 0 5 4.06 0.73 28 0 -5 3.37 0.60 28 -1 5 -0.06 0.26 28 -1 5 -0.01 0.25 28 1 -5 0.38 0.41 28 1 -5 0.06 0.28 28 1 5 0.10 0.27 28 1 5 0.08 0.29 28 -1 -5 -0.04 0.34 28 -1 -5 0.16 0.28 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 88820 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p21c_b _database_code_depnum_ccdc_archive 'CCDC 2151840' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-14 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C57 H3 Ag Al2 F61 O30 Os6' _chemical_formula_moiety 'C24 Al2 F55 O6, C24 Ag O24 Os6, 1.5(C6 H2 F4)' _chemical_formula_weight 3629.62 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 20.504(4) _cell_length_b 17.810(3) _cell_length_c 25.217(8) _cell_angle_alpha 90 _cell_angle_beta 107.09(2) _cell_angle_gamma 90 _cell_volume 8802(4) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9519 _cell_measurement_theta_min 2.2285 _cell_measurement_theta_max 27.096 _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.739 _exptl_crystal_F_000 6652 _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 9.070 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.5549 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 158056 _diffrn_reflns_av_unetI/netI 0.0323 _diffrn_reflns_av_R_equivalents 0.0589 _diffrn_reflns_theta_min 1.422 _diffrn_reflns_theta_max 27.144 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_limit_l_max 31 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 19471 _reflns_number_gt 15614 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS V6.2.15 Patch 4/2021-03-15 && APEX4 2021.10-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0240P)^2^+125.0107P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_number_reflns 19471 _refine_ls_number_parameters 2368 _refine_ls_number_restraints 27525 _refine_ls_R_factor_all 0.0587 _refine_ls_R_factor_gt 0.0420 _refine_ls_wR_factor_ref 0.0965 _refine_ls_wR_factor_gt 0.0881 _refine_ls_goodness_of_fit_ref 1.124 _refine_ls_restrained_S_all 1.001 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 1.518 _refine_diff_density_min -1.927 _refine_diff_density_rms 0.195 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Os2 Os 0.32015(2) 0.09290(2) 0.98916(2) 0.02347(8) Uani 1 1 d . . . . . Os3 Os 0.23455(2) 0.14964(2) 0.88407(2) 0.02429(8) Uani 1 1 d . . . . . Os4 Os 0.29137(2) 0.14802(2) 0.68418(2) 0.02260(7) Uani 1 1 d . . . . . Os5 Os 0.20172(2) 0.09982(2) 0.57772(2) 0.02592(8) Uani 1 1 d . . . . . Os6 Os 0.17039(2) 0.04970(2) 0.67697(2) 0.02318(8) Uani 1 1 d . . . . . Os1 Os 0.34748(2) 0.03947(2) 0.88933(2) 0.02229(7) Uani 1 1 d . . . . . Ag1 Ag 0.26194(3) 0.09566(3) 0.78358(3) 0.02268(12) Uani 1 1 d . . . . . Al1 Al 0.6649(5) 0.1077(6) 0.7395(3) 0.0178(16) Uani 0.516(2) 1 d D U P A 1 Al2 Al 0.6678(5) 0.1164(7) 0.7599(3) 0.024(2) Uani 0.484(2) 1 d D U P A 2 Al08 Al 0.84167(12) 0.09244(14) 0.76674(10) 0.0239(5) Uani 1 1 d D . . . . O1 O 0.2371(4) -0.0834(4) 0.8607(3) 0.0452(18) Uani 1 1 d . . . . . F1 F 0.7528(6) 0.102(3) 0.7467(17) 0.024(6) Uani 0.516(2) 1 d D U P A 1 F1B F 0.7536(7) 0.108(3) 0.7591(18) 0.030(8) Uani 0.484(2) 1 d D U P A 2 C2 C 0.4093(5) -0.0258(5) 0.9415(4) 0.032(2) Uani 1 1 d . . . . . C11 C 0.1756(5) 0.1864(6) 0.8151(4) 0.037(2) Uani 1 1 d . . . . . C12 C 0.3010(5) 0.2292(5) 0.8827(4) 0.034(2) Uani 1 1 d . . . . . C13 C 0.2354(5) -0.0344(5) 0.6915(4) 0.032(2) Uani 1 1 d . . . . . C14 C 0.1403(4) 0.0207(5) 0.7389(4) 0.0289(19) Uani 1 1 d . . . . . C15 C 0.1009(5) -0.0068(6) 0.6251(4) 0.037(2) Uani 1 1 d . . . . . C16 C 0.1099(5) 0.1359(5) 0.6652(4) 0.031(2) Uani 1 1 d . . . . . C17 C 0.2468(5) 0.0023(5) 0.5809(4) 0.035(2) Uani 1 1 d . . . . . C18 C 0.1221(5) 0.0627(5) 0.5207(4) 0.032(2) Uani 1 1 d . . . . . C19 C 0.2505(5) 0.1387(6) 0.5279(4) 0.038(2) Uani 1 1 d . . . . . C20 C 0.1551(5) 0.1961(5) 0.5763(4) 0.0289(19) Uani 1 1 d . . . . . C21 C 0.3451(4) 0.0603(5) 0.6771(4) 0.0292(19) Uani 1 1 d . . . . . C22 C 0.3579(4) 0.1756(5) 0.7534(4) 0.0298(19) Uani 1 1 d . . . . . C23 C 0.3345(5) 0.2060(6) 0.6399(4) 0.036(2) Uani 1 1 d . . . . . C24 C 0.2323(5) 0.2324(5) 0.6908(4) 0.0285(19) Uani 1 1 d . . . . . C3 C 0.3766(5) 0.0088(5) 0.8271(4) 0.031(2) Uani 1 1 d . . . . . O4 O 0.4561(4) 0.1656(4) 0.9122(3) 0.0423(17) Uani 1 1 d . . . . . O5 O 0.2350(4) -0.0523(4) 0.9813(3) 0.0438(18) Uani 1 1 d . . . . . O2 O 0.4445(4) -0.0670(4) 0.9703(3) 0.0406(16) Uani 1 1 d . . . . . O3 O 0.4012(4) -0.0133(4) 0.7943(3) 0.0468(19) Uani 1 1 d . . . . . C4 C 0.4158(5) 0.1212(6) 0.9038(4) 0.034(2) Uani 1 1 d . . . . . C5 C 0.2656(5) 0.0007(5) 0.9837(4) 0.033(2) Uani 1 1 d . . . . . C6 C 0.2742(5) 0.1368(5) 1.0366(4) 0.035(2) Uani 1 1 d . . . . . C7 C 0.3955(5) 0.0477(5) 1.0434(4) 0.033(2) Uani 1 1 d . . . . . C8 C 0.3749(5) 0.1849(5) 0.9930(4) 0.030(2) Uani 1 1 d . . . . . C9 C 0.1723(5) 0.0656(6) 0.8858(4) 0.038(2) Uani 1 1 d . . . . . C10 C 0.1896(5) 0.2075(6) 0.9265(4) 0.042(2) Uani 1 1 d . . . . . O6 O 0.2457(4) 0.1634(4) 1.0657(3) 0.0443(17) Uani 1 1 d . . . . . O7 O 0.4410(4) 0.0242(4) 1.0771(3) 0.0419(17) Uani 1 1 d . . . . . O8 O 0.4069(4) 0.2373(4) 0.9988(3) 0.0409(17) Uani 1 1 d . . . . . O9 O 0.1352(4) 0.0207(5) 0.8886(3) 0.050(2) Uani 1 1 d . . . . . O10 O 0.1603(4) 0.2419(5) 0.9504(3) 0.052(2) Uani 1 1 d . . . . . O11 O 0.1359(4) 0.2131(4) 0.7782(3) 0.0473(19) Uani 1 1 d . . . . . O12 O 0.3353(4) 0.2768(4) 0.8801(3) 0.0420(17) Uani 1 1 d . . . . . O13 O 0.2707(4) -0.0841(4) 0.7013(3) 0.0413(17) Uani 1 1 d . . . . . O14 O 0.1145(3) 0.0002(4) 0.7717(3) 0.0371(15) Uani 1 1 d . . . . . O15 O 0.0591(4) -0.0422(4) 0.5955(3) 0.0440(18) Uani 1 1 d . . . . . O16 O 0.0713(4) 0.1840(4) 0.6582(3) 0.0412(17) Uani 1 1 d . . . . . O17 O 0.2735(4) -0.0540(4) 0.5795(3) 0.052(2) Uani 1 1 d . . . . . O18 O 0.0764(4) 0.0434(5) 0.4877(3) 0.052(2) Uani 1 1 d . . . . . O19 O 0.2792(4) 0.1612(4) 0.5006(3) 0.0498(19) Uani 1 1 d . . . . . O20 O 0.1266(3) 0.2512(4) 0.5725(3) 0.0343(15) Uani 1 1 d . . . . . O21 O 0.3777(3) 0.0105(4) 0.6725(3) 0.0412(17) Uani 1 1 d . . . . . O22 O 0.4009(3) 0.1954(4) 0.7899(3) 0.0391(16) Uani 1 1 d . . . . . O23 O 0.3619(4) 0.2400(4) 0.6150(3) 0.0458(18) Uani 1 1 d . . . . . O24 O 0.2005(4) 0.2818(4) 0.6957(3) 0.0414(17) Uani 1 1 d . . . . . C1 C 0.2750(5) -0.0376(5) 0.8716(4) 0.031(2) Uani 1 1 d . . . . . O1_7 O 0.6416(7) 0.1757(8) 0.6907(6) 0.039(3) Uani 0.516(2) 1 d D U P A 1 C1_7 C 0.5971(6) 0.2052(6) 0.6435(5) 0.030(3) Uani 0.516(2) 1 d D U P A 1 C2_7 C 0.5347(6) 0.1515(7) 0.6246(6) 0.037(3) Uani 0.516(2) 1 d D U P A 1 F1_7 F 0.5518(7) 0.0899(6) 0.6025(5) 0.061(4) Uani 0.516(2) 1 d D U P A 1 F2_7 F 0.4828(7) 0.1823(9) 0.5859(5) 0.058(4) Uani 0.516(2) 1 d D U P A 1 F3_7 F 0.5123(6) 0.1341(7) 0.6679(5) 0.052(3) Uani 0.516(2) 1 d D U P A 1 C3_7 C 0.5737(7) 0.2834(7) 0.6563(5) 0.046(3) Uani 0.516(2) 1 d D U P A 1 F4_7 F 0.6281(7) 0.3249(7) 0.6841(7) 0.071(4) Uani 0.516(2) 1 d D U P A 1 F5_7 F 0.5311(7) 0.2795(8) 0.6869(5) 0.064(4) Uani 0.516(2) 1 d D U P A 1 F6_7 F 0.5414(8) 0.3213(7) 0.6098(5) 0.068(4) Uani 0.516(2) 1 d D U P A 1 C4_7 C 0.6320(7) 0.2121(8) 0.5963(6) 0.049(4) Uani 0.516(2) 1 d D U P A 1 F7_7 F 0.6747(7) 0.2702(9) 0.6072(6) 0.078(4) Uani 0.516(2) 1 d D U P A 1 F8_7 F 0.5839(8) 0.2247(13) 0.5484(6) 0.064(5) Uani 0.516(2) 1 d D U P A 1 F9_7 F 0.6649(10) 0.1479(10) 0.5940(8) 0.091(5) Uani 0.516(2) 1 d D U P A 1 O1_8 O 0.6185(7) 0.1516(8) 0.6974(6) 0.033(3) Uani 0.484(2) 1 d D U P A 2 C1_8 C 0.6018(6) 0.2089(7) 0.6594(6) 0.034(3) Uani 0.484(2) 1 d D U P A 2 C2_8 C 0.6333(9) 0.1910(10) 0.6122(7) 0.076(5) Uani 0.484(2) 1 d D U P A 2 F1_8 F 0.7004(8) 0.2091(13) 0.6307(9) 0.113(6) Uani 0.484(2) 1 d D U P A 2 F2_8 F 0.6023(14) 0.2312(15) 0.5661(8) 0.107(8) Uani 0.484(2) 1 d D U P A 2 F3_8 F 0.6225(11) 0.1189(9) 0.5974(8) 0.091(6) Uani 0.484(2) 1 d D U P A 2 C3_8 C 0.5228(7) 0.2117(8) 0.6368(6) 0.053(4) Uani 0.484(2) 1 d D U P A 2 F4_8 F 0.4957(6) 0.2060(8) 0.6789(5) 0.058(3) Uani 0.484(2) 1 d D U P A 2 F5_8 F 0.5028(10) 0.1554(8) 0.5995(6) 0.084(6) Uani 0.484(2) 1 d D U P A 2 F6_8 F 0.5041(8) 0.2794(8) 0.6136(7) 0.079(5) Uani 0.484(2) 1 d D U P A 2 C4_8 C 0.6290(7) 0.2853(8) 0.6864(6) 0.050(4) Uani 0.484(2) 1 d D U P A 2 F7_8 F 0.5856(8) 0.3106(8) 0.7136(6) 0.063(4) Uani 0.484(2) 1 d D U P A 2 F8_8 F 0.6380(8) 0.3326(7) 0.6472(6) 0.058(4) Uani 0.484(2) 1 d D U P A 2 F9_8 F 0.6915(6) 0.2757(7) 0.7221(6) 0.058(4) Uani 0.484(2) 1 d D U P A 2 O1_9 O 0.8775(5) 0.1773(5) 0.7836(4) 0.030(2) Uani 0.657(5) 1 d D U P A 1 C1_9 C 0.9046(5) 0.2383(6) 0.7648(4) 0.0308(17) Uani 0.657(5) 1 d D U P A 1 C2_9 C 0.8491(5) 0.2821(6) 0.7204(5) 0.039(2) Uani 0.657(5) 1 d D U P A 1 F1_9 F 0.8086(7) 0.3204(8) 0.7441(5) 0.056(4) Uani 0.657(5) 1 d D U P A 1 F2_9 F 0.8779(5) 0.3284(5) 0.6924(4) 0.050(2) Uani 0.657(5) 1 d D U P A 1 F3_9 F 0.8092(5) 0.2342(5) 0.6848(4) 0.052(2) Uani 0.657(5) 1 d D U P A 1 C3_9 C 0.9616(5) 0.2135(6) 0.7392(5) 0.038(2) Uani 0.657(5) 1 d D U P A 1 F4_9 F 1.0004(5) 0.1599(5) 0.7694(5) 0.053(2) Uani 0.657(5) 1 d D U P A 1 F5_9 F 0.9341(5) 0.1882(5) 0.6870(4) 0.050(2) Uani 0.657(5) 1 d D U P A 1 F6_9 F 1.0030(5) 0.2720(5) 0.7384(5) 0.053(3) Uani 0.657(5) 1 d D U P A 1 C4_9 C 0.9346(6) 0.2902(6) 0.8156(5) 0.046(2) Uani 0.657(5) 1 d D U P A 1 F7_9 F 0.9945(5) 0.2621(6) 0.8476(5) 0.069(3) Uani 0.657(5) 1 d D U P A 1 F8_9 F 0.9457(5) 0.3593(4) 0.8001(4) 0.055(2) Uani 0.657(5) 1 d D U P A 1 F9_9 F 0.8928(5) 0.2938(5) 0.8470(4) 0.057(2) Uani 0.657(5) 1 d D U P A 1 O1_12 O 0.6332(6) 0.0214(6) 0.7182(6) 0.037(3) Uani 0.516(2) 1 d D U P A 1 C1_12 C 0.6039(6) -0.0444(7) 0.7273(5) 0.033(3) Uani 0.516(2) 1 d D U P A 1 C2_12 C 0.5620(6) -0.0765(7) 0.6705(5) 0.037(3) Uani 0.516(2) 1 d D U P A 1 F1_12 F 0.5027(5) -0.0388(7) 0.6516(5) 0.054(3) Uani 0.516(2) 1 d D U P A 1 F2_12 F 0.5485(7) -0.1489(6) 0.6735(6) 0.052(3) Uani 0.516(2) 1 d D U P A 1 F3_12 F 0.5963(6) -0.0692(6) 0.6334(5) 0.047(3) Uani 0.516(2) 1 d D U P A 1 C3_12 C 0.6610(7) -0.1008(7) 0.7565(6) 0.044(3) Uani 0.516(2) 1 d D U P A 1 F4_12 F 0.7119(6) -0.0639(6) 0.7933(5) 0.055(3) Uani 0.516(2) 1 d D U P A 1 F5_12 F 0.6862(8) -0.1351(9) 0.7191(7) 0.050(4) Uani 0.516(2) 1 d D U P A 1 F6_12 F 0.6367(7) -0.1546(7) 0.7818(6) 0.060(3) Uani 0.516(2) 1 d D U P A 1 C4_12 C 0.5556(6) -0.0304(7) 0.7639(5) 0.033(3) Uani 0.516(2) 1 d D U P A 1 F7_12 F 0.5932(7) -0.0252(7) 0.8175(4) 0.054(3) Uani 0.516(2) 1 d D U P A 1 F8_12 F 0.5103(6) -0.0859(6) 0.7574(7) 0.059(4) Uani 0.516(2) 1 d D U P A 1 F9_12 F 0.5200(12) 0.0330(9) 0.7493(8) 0.035(4) Uani 0.516(2) 1 d D U P A 1 O1_13 O 0.6451(6) 0.0263(6) 0.7674(5) 0.035(3) Uani 0.484(2) 1 d D U P A 2 C1_13 C 0.6069(6) -0.0350(7) 0.7455(5) 0.026(3) Uani 0.484(2) 1 d D U P A 2 C2_13 C 0.5327(6) -0.0114(7) 0.7133(5) 0.035(3) Uani 0.484(2) 1 d D U P A 2 F1_13 F 0.5135(14) 0.0422(12) 0.7432(10) 0.047(6) Uani 0.484(2) 1 d D U P A 2 F2_13 F 0.4908(5) -0.0696(6) 0.7106(7) 0.060(4) Uani 0.484(2) 1 d D U P A 2 F3_13 F 0.5304(6) 0.0135(7) 0.6626(4) 0.047(3) Uani 0.484(2) 1 d D U P A 2 C3_13 C 0.6393(8) -0.0729(9) 0.7040(6) 0.060(4) Uani 0.484(2) 1 d D U P A 2 F4_13 F 0.6957(10) -0.1113(13) 0.7319(8) 0.089(8) Uani 0.484(2) 1 d D U P A 2 F5_13 F 0.6580(8) -0.0220(10) 0.6725(6) 0.095(6) Uani 0.484(2) 1 d D U P A 2 F6_13 F 0.5947(9) -0.1193(9) 0.6706(6) 0.089(5) Uani 0.484(2) 1 d D U P A 2 C4_13 C 0.6077(7) -0.0900(7) 0.7931(5) 0.039(3) Uani 0.484(2) 1 d D U P A 2 F7_13 F 0.6696(5) -0.0943(6) 0.8293(4) 0.039(3) Uani 0.484(2) 1 d D U P A 2 F8_13 F 0.5895(6) -0.1596(5) 0.7740(5) 0.036(3) Uani 0.484(2) 1 d D U P A 2 F9_13 F 0.5623(7) -0.0643(8) 0.8189(6) 0.058(3) Uani 0.484(2) 1 d D U P A 2 O1_14 O 0.8711(9) 0.1812(7) 0.7516(8) 0.031(3) Uani 0.343(5) 1 d D U P A 2 C1_14 C 0.9081(7) 0.2457(8) 0.7690(6) 0.033(2) Uani 0.343(5) 1 d D U P A 2 C2_14 C 0.8634(8) 0.3033(8) 0.7890(7) 0.036(3) Uani 0.343(5) 1 d D U P A 2 F1_14 F 0.8218(11) 0.3399(12) 0.7455(8) 0.040(4) Uani 0.343(5) 1 d D U P A 2 F2_14 F 0.9019(8) 0.3546(8) 0.8230(7) 0.050(4) Uani 0.343(5) 1 d D U P A 2 F3_14 F 0.8266(9) 0.2677(9) 0.8171(7) 0.049(4) Uani 0.343(5) 1 d D U P A 2 C3_14 C 0.9729(8) 0.2282(9) 0.8180(6) 0.041(3) Uani 0.343(5) 1 d D U P A 2 F4_14 F 1.0016(8) 0.1645(8) 0.8084(8) 0.042(3) Uani 0.343(5) 1 d D U P A 2 F5_14 F 0.9557(9) 0.2218(10) 0.8655(6) 0.056(4) Uani 0.343(5) 1 d D U P A 2 F6_14 F 1.0202(8) 0.2829(9) 0.8248(9) 0.056(4) Uani 0.343(5) 1 d D U P A 2 C4_14 C 0.9296(8) 0.2823(8) 0.7206(6) 0.039(3) Uani 0.343(5) 1 d D U P A 2 F7_14 F 0.9819(9) 0.2448(10) 0.7118(8) 0.048(4) Uani 0.343(5) 1 d D U P A 2 F8_14 F 0.9479(8) 0.3544(7) 0.7318(7) 0.047(4) Uani 0.343(5) 1 d D U P A 2 F9_14 F 0.8768(8) 0.2815(11) 0.6742(6) 0.051(4) Uani 0.343(5) 1 d D U P A 2 O1_15 O 0.8579(5) 0.0363(6) 0.8259(3) 0.034(2) Uani 0.687(8) 1 d D U P A 1 C1_15 C 0.9024(5) 0.0142(6) 0.8748(4) 0.0414(19) Uani 0.687(8) 1 d D U P A 1 C2_15 C 0.9620(6) -0.0343(7) 0.8659(5) 0.050(2) Uani 0.687(8) 1 d D U P A 1 F1_15 F 0.9389(6) -0.1029(6) 0.8478(5) 0.066(3) Uani 0.687(8) 1 d D U P A 1 F2_15 F 1.0121(7) -0.0390(8) 0.9140(5) 0.077(4) Uani 0.687(8) 1 d D U P A 1 F3_15 F 0.9895(7) 0.0015(11) 0.8316(6) 0.082(5) Uani 0.687(8) 1 d D U P A 1 C3_15 C 0.9349(7) 0.0834(7) 0.9094(5) 0.070(3) Uani 0.687(8) 1 d D U P A 1 F4_15 F 0.8856(8) 0.1347(7) 0.9066(5) 0.096(4) Uani 0.687(8) 1 d D U P A 1 F5_15 F 0.9849(6) 0.1100(6) 0.8907(5) 0.090(3) Uani 0.687(8) 1 d D U P A 1 F6_15 F 0.9619(8) 0.0648(7) 0.9637(4) 0.105(4) Uani 0.687(8) 1 d D U P A 1 C4_15 C 0.8641(6) -0.0360(7) 0.9065(5) 0.051(2) Uani 0.687(8) 1 d D U P A 1 F7_15 F 0.8275(8) 0.0096(9) 0.9285(5) 0.093(4) Uani 0.687(8) 1 d D U P A 1 F8_15 F 0.9074(5) -0.0731(6) 0.9484(4) 0.061(3) Uani 0.687(8) 1 d D U P A 1 F9_15 F 0.8263(6) -0.0875(6) 0.8722(4) 0.067(3) Uani 0.687(8) 1 d D U P A 1 O1_16 O 0.8779(10) 0.0725(10) 0.8340(6) 0.031(4) Uani 0.313(8) 1 d D U P A 2 C1_16 C 0.9013(9) 0.0178(9) 0.8715(7) 0.051(3) Uani 0.313(8) 1 d D U P A 2 C2_16 C 0.9489(10) -0.0365(12) 0.8522(9) 0.058(4) Uani 0.313(8) 1 d D U P A 2 F1_16 F 0.9061(12) -0.0913(13) 0.8254(12) 0.076(6) Uani 0.313(8) 1 d D U P A 2 F2_16 F 1.0013(12) -0.0594(18) 0.8947(11) 0.067(6) Uani 0.313(8) 1 d D U P A 2 F3_16 F 0.9747(15) -0.005(2) 0.8148(11) 0.061(6) Uani 0.313(8) 1 d D U P A 2 C3_16 C 0.9340(11) 0.0568(12) 0.9279(7) 0.078(4) Uani 0.313(8) 1 d D U P A 2 F4_16 F 0.8935(16) 0.1171(15) 0.9294(11) 0.101(6) Uani 0.313(8) 1 d D U P A 2 F5_16 F 0.9975(10) 0.0787(14) 0.9302(12) 0.098(6) Uani 0.313(8) 1 d D U P A 2 F6_16 F 0.9236(16) 0.0103(16) 0.9668(9) 0.110(6) Uani 0.313(8) 1 d D U P A 2 C4_16 C 0.8396(9) -0.0315(11) 0.8754(8) 0.064(4) Uani 0.313(8) 1 d D U P A 2 F7_16 F 0.8052(12) 0.0071(16) 0.9041(10) 0.079(6) Uani 0.313(8) 1 d D U P A 2 F8_16 F 0.8649(12) -0.0963(11) 0.9002(11) 0.081(6) Uani 0.313(8) 1 d D U P A 2 F9_16 F 0.8009(8) -0.0459(10) 0.8234(7) 0.048(5) Uani 0.313(8) 1 d D U P A 2 O1_17 O 0.8319(11) 0.0308(11) 0.7137(8) 0.039(4) Uani 0.289(7) 1 d D U P A 2 C1_17 C 0.8546(8) 0.0075(9) 0.6709(8) 0.048(3) Uani 0.289(7) 1 d D U P A 2 C2_17 C 0.7911(10) 0.0197(14) 0.6196(8) 0.067(4) Uani 0.289(7) 1 d D U P A 2 F1_17 F 0.7370(12) 0.0109(15) 0.6391(12) 0.066(5) Uani 0.289(7) 1 d D U P A 2 F2_17 F 0.7892(17) -0.0292(19) 0.5795(12) 0.071(6) Uani 0.289(7) 1 d D U P A 2 F3_17 F 0.7956(19) 0.0895(14) 0.6024(12) 0.069(6) Uani 0.289(7) 1 d D U P A 2 C3_17 C 0.9169(9) 0.0527(10) 0.6659(8) 0.051(3) Uani 0.289(7) 1 d D U P A 2 F4_17 F 0.9615(9) 0.0629(12) 0.7161(7) 0.054(5) Uani 0.289(7) 1 d D U P A 2 F5_17 F 0.8962(12) 0.1194(11) 0.6422(9) 0.066(5) Uani 0.289(7) 1 d D U P A 2 F6_17 F 0.9487(11) 0.0141(14) 0.6351(10) 0.065(5) Uani 0.289(7) 1 d D U P A 2 C4_17 C 0.8728(11) -0.0768(10) 0.6791(9) 0.066(4) Uani 0.289(7) 1 d D U P A 2 F7_17 F 0.9348(11) -0.0822(14) 0.7170(11) 0.078(6) Uani 0.289(7) 1 d D U P A 2 F8_17 F 0.8717(15) -0.1070(14) 0.6302(10) 0.092(6) Uani 0.289(7) 1 d D U P A 2 F9_17 F 0.8260(14) -0.1105(12) 0.6986(12) 0.083(5) Uani 0.289(7) 1 d D U P A 2 O1_18 O 0.8624(5) 0.0504(5) 0.7128(4) 0.039(2) Uani 0.711(7) 1 d D U P A 1 C1_18 C 0.8547(5) -0.0033(6) 0.6728(4) 0.0418(18) Uani 0.711(7) 1 d D U P A 1 C2_18 C 0.8452(7) -0.0815(6) 0.6960(5) 0.058(2) Uani 0.711(7) 1 d D U P A 1 F1_18 F 0.9052(6) -0.1098(6) 0.7259(5) 0.075(3) Uani 0.711(7) 1 d D U P A 1 F2_18 F 0.8160(7) -0.1303(6) 0.6562(5) 0.086(3) Uani 0.711(7) 1 d D U P A 1 F3_18 F 0.8067(6) -0.0756(6) 0.7301(5) 0.082(3) Uani 0.711(7) 1 d D U P A 1 C3_18 C 0.7937(7) 0.0163(9) 0.6220(6) 0.072(3) Uani 0.711(7) 1 d D U P A 1 F4_18 F 0.7861(9) 0.0901(7) 0.6178(5) 0.084(4) Uani 0.711(7) 1 d D U P A 1 F5_18 F 0.7371(7) -0.0170(11) 0.6261(9) 0.145(6) Uani 0.711(7) 1 d D U P A 1 F6_18 F 0.8044(11) -0.0085(12) 0.5752(6) 0.126(6) Uani 0.711(7) 1 d D U P A 1 C4_18 C 0.9199(6) -0.0043(6) 0.6537(5) 0.045(2) Uani 0.711(7) 1 d D U P A 1 F7_18 F 0.9204(5) 0.0538(5) 0.6196(4) 0.057(2) Uani 0.711(7) 1 d D U P A 1 F8_18 F 0.9234(5) -0.0675(5) 0.6259(4) 0.056(2) Uani 0.711(7) 1 d D U P A 1 F9_18 F 0.9756(4) 0.0007(6) 0.6956(4) 0.059(2) Uani 0.711(7) 1 d D U P A 1 O1_19 O 0.6604(10) 0.1259(10) 0.8039(7) 0.034(3) Uani 0.360(3) 1 d D U P A 1 C1_19 C 0.6507(7) 0.1737(8) 0.8438(6) 0.040(2) Uani 0.360(3) 1 d D U P A 1 C2_19 C 0.6873(8) 0.1391(10) 0.9014(6) 0.046(2) Uani 0.360(3) 1 d D U P A 1 F1_19 F 0.6773(13) 0.0647(9) 0.8994(13) 0.047(3) Uani 0.360(3) 1 d D U P A 1 F2_19 F 0.6616(10) 0.1666(11) 0.9404(7) 0.053(3) Uani 0.360(3) 1 d D U P A 1 F3_19 F 0.7550(7) 0.1500(9) 0.9131(7) 0.049(3) Uani 0.360(3) 1 d D U P A 1 C3_19 C 0.6803(8) 0.2513(8) 0.8365(7) 0.046(2) Uani 0.360(3) 1 d D U P A 1 F4_19 F 0.6374(8) 0.2901(9) 0.7950(7) 0.045(3) Uani 0.360(3) 1 d D U P A 1 F5_19 F 0.7405(8) 0.2445(10) 0.8263(8) 0.052(3) Uani 0.360(3) 1 d D U P A 1 F6_19 F 0.6918(10) 0.2929(9) 0.8826(6) 0.056(3) Uani 0.360(3) 1 d D U P A 1 C4_19 C 0.5726(7) 0.1796(9) 0.8347(7) 0.040(2) Uani 0.360(3) 1 d D U P A 1 F7_19 F 0.5393(8) 0.1865(9) 0.7802(6) 0.039(3) Uani 0.360(3) 1 d D U P A 1 F8_19 F 0.5537(10) 0.2399(9) 0.8571(8) 0.051(3) Uani 0.360(3) 1 d D U P A 1 F9_19 F 0.5491(10) 0.1180(11) 0.8530(10) 0.040(4) Uani 0.360(3) 1 d D U P A 1 F1_21 F 0.6022(10) -0.0890(15) 0.5227(10) 0.144(11) Uani 0.5 1 d D U P B -1 F2_21 F 0.5623(15) 0.0510(15) 0.4815(10) 0.192(12) Uani 0.5 1 d D U P B -1 F3_21 F 0.4379(16) 0.1039(11) 0.4814(8) 0.170(12) Uani 0.5 1 d D U P B -1 F4_21 F 0.3573(11) 0.0189(13) 0.5207(8) 0.150(9) Uani 0.5 1 d D U P B -1 C1_21 C 0.5417(10) -0.0617(11) 0.5227(9) 0.097(8) Uani 0.5 1 d D U P B -1 C2_21 C 0.5221(11) 0.0090(11) 0.5016(9) 0.121(8) Uani 0.5 1 d D U P B -1 C3_21 C 0.4585(11) 0.0360(11) 0.5012(8) 0.106(7) Uani 0.5 1 d D U P B -1 C4_21 C 0.4167(11) -0.0080(12) 0.5219(8) 0.112(8) Uani 0.5 1 d D U P B -1 C5_21 C 0.4357(12) -0.0789(12) 0.5431(9) 0.096(8) Uani 0.5 1 d D U P B -1 H5_21 H 0.406217 -0.108353 0.557576 0.116 Uiso 0.5 1 calc R U P B -1 C6_21 C 0.4979(11) -0.1052(12) 0.5427(8) 0.089(7) Uani 0.5 1 d D U P B -1 H6_21 H 0.511617 -0.154185 0.556314 0.107 Uiso 0.5 1 calc R U P B -1 O1_10 O 0.6732(7) 0.1705(8) 0.8158(6) 0.043(2) Uani 0.484(2) 1 d D U P A 2 C1_10 C 0.6521(6) 0.1927(7) 0.8594(5) 0.045(2) Uani 0.484(2) 1 d D U P A 2 C2_10 C 0.7089(8) 0.2332(8) 0.9047(6) 0.059(2) Uani 0.484(2) 1 d D U P A 2 F1_10 F 0.7455(10) 0.2798(8) 0.8829(8) 0.062(3) Uani 0.484(2) 1 d D U P A 2 F2_10 F 0.6803(8) 0.2762(8) 0.9366(6) 0.079(3) Uani 0.484(2) 1 d D U P A 2 F3_10 F 0.7470(8) 0.1807(8) 0.9370(7) 0.073(3) Uani 0.484(2) 1 d D U P A 2 C3_10 C 0.6245(8) 0.1249(8) 0.8846(6) 0.046(2) Uani 0.484(2) 1 d D U P A 2 F4_10 F 0.5627(7) 0.1059(9) 0.8508(7) 0.044(3) Uani 0.484(2) 1 d D U P A 2 F5_10 F 0.6693(10) 0.0680(8) 0.8935(10) 0.048(3) Uani 0.484(2) 1 d D U P A 2 F6_10 F 0.6163(8) 0.1409(8) 0.9342(5) 0.059(3) Uani 0.484(2) 1 d D U P A 2 C4_10 C 0.5933(7) 0.2515(7) 0.8375(6) 0.051(2) Uani 0.484(2) 1 d D U P A 2 F7_10 F 0.5486(7) 0.2230(8) 0.7918(5) 0.050(3) Uani 0.484(2) 1 d D U P A 2 F8_10 F 0.5617(9) 0.2561(10) 0.8770(6) 0.067(3) Uani 0.484(2) 1 d D U P A 2 F9_10 F 0.6216(7) 0.3174(6) 0.8302(6) 0.051(3) Uani 0.484(2) 1 d D U P A 2 O1_20 O 0.653(2) 0.143(2) 0.8000(14) 0.041(4) Uani 0.155(3) 1 d D U P C 3 C1_20 C 0.6642(11) 0.1900(13) 0.8447(11) 0.045(2) Uani 0.155(3) 1 d D U P C 3 C2_20 C 0.6650(13) 0.1429(14) 0.8967(11) 0.049(3) Uani 0.155(3) 1 d D U P C 3 F1_20 F 0.6009(14) 0.1231(19) 0.8938(15) 0.048(3) Uani 0.155(3) 1 d D U P C 3 F2_20 F 0.692(2) 0.182(2) 0.9432(12) 0.055(4) Uani 0.155(3) 1 d D U P C 3 F3_20 F 0.7016(18) 0.0804(16) 0.8974(17) 0.050(4) Uani 0.155(3) 1 d D U P C 3 C3_20 C 0.7345(12) 0.2292(15) 0.8538(12) 0.048(3) Uani 0.155(3) 1 d D U P C 3 F4_20 F 0.7400(18) 0.252(2) 0.8045(13) 0.044(4) Uani 0.155(3) 1 d D U P C 3 F5_20 F 0.7824(14) 0.1776(17) 0.8764(14) 0.050(4) Uani 0.155(3) 1 d D U P C 3 F6_20 F 0.740(2) 0.2893(19) 0.8866(19) 0.049(4) Uani 0.155(3) 1 d D U P C 3 C4_20 C 0.6073(12) 0.2502(14) 0.8343(11) 0.049(3) Uani 0.155(3) 1 d D U P C 3 F7_20 F 0.616(2) 0.302(2) 0.7982(16) 0.051(4) Uani 0.155(3) 1 d D U P C 3 F8_20 F 0.6089(19) 0.2835(19) 0.8825(13) 0.054(4) Uani 0.155(3) 1 d D U P C 3 F9_20 F 0.5460(14) 0.218(2) 0.8136(16) 0.050(4) Uani 0.155(3) 1 d D U P C 3 F1_22 F 0.7779(4) 0.2033(4) 1.0633(3) 0.076(2) Uani 1 1 d D U . . . F2_22 F 0.7650(5) 0.3348(4) 1.0093(3) 0.098(3) Uani 1 1 d D U . . . F3_22 F 0.8703(5) 0.3917(5) 0.9783(4) 0.146(5) Uani 1 1 d D U . . . F4_22 F 0.9898(5) 0.3170(6) 1.0016(5) 0.143(5) Uani 1 1 d D U . . . C1_22 C 0.8312(5) 0.2306(5) 1.0489(4) 0.054(3) Uani 1 1 d D U . . . C2_22 C 0.8235(6) 0.2981(5) 1.0209(4) 0.063(3) Uani 1 1 d D U . . . C3_22 C 0.8778(5) 0.3263(6) 1.0056(5) 0.075(4) Uani 1 1 d D U . . . C4_22 C 0.9383(6) 0.2879(6) 1.0169(5) 0.080(4) Uani 1 1 d D U . . . C5_22 C 0.9458(6) 0.2205(6) 1.0448(5) 0.068(4) Uani 1 1 d D U . . . H5_22 H 0.987784 0.193915 1.053131 0.082 Uiso 1 1 calc R U . . . C6_22 C 0.8915(5) 0.1920(5) 1.0604(4) 0.054(3) Uani 1 1 d D U . . . H6_22 H 0.896065 0.145234 1.079259 0.065 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Os2 0.02505(17) 0.02463(16) 0.02270(17) -0.00351(12) 0.01006(13) -0.00415(13) Os3 0.02176(16) 0.02806(17) 0.02376(17) -0.00603(13) 0.00782(13) 0.00110(13) Os4 0.02105(16) 0.02043(15) 0.02711(17) -0.00053(12) 0.00832(13) -0.00096(12) Os5 0.03238(19) 0.02259(16) 0.02441(17) -0.00372(13) 0.01083(14) -0.00219(14) Os6 0.02219(16) 0.02426(16) 0.02381(17) -0.00413(13) 0.00784(13) -0.00329(13) Os1 0.02512(17) 0.02039(15) 0.02488(17) 0.00039(12) 0.01282(13) 0.00026(12) Ag1 0.0213(3) 0.0239(3) 0.0240(3) -0.0043(2) 0.0084(2) -0.0013(2) Al1 0.013(3) 0.021(3) 0.015(4) 0.002(3) -0.002(3) 0.000(2) Al2 0.015(3) 0.036(5) 0.016(5) 0.009(4) -0.004(4) -0.001(3) Al08 0.0183(12) 0.0299(13) 0.0241(13) -0.0035(10) 0.0068(10) -0.0019(10) O1 0.064(5) 0.032(4) 0.039(4) -0.005(3) 0.016(4) -0.019(4) F1 0.012(7) 0.031(8) 0.027(17) 0.013(11) 0.000(5) 0.004(5) F1B 0.014(8) 0.056(16) 0.019(15) 0.013(11) 0.004(5) -0.004(7) C2 0.038(5) 0.031(5) 0.033(5) 0.005(4) 0.019(4) 0.003(4) C11 0.027(5) 0.050(6) 0.034(5) -0.006(4) 0.010(4) 0.011(4) C12 0.039(5) 0.034(5) 0.028(5) 0.009(4) 0.010(4) 0.016(4) C13 0.030(5) 0.028(5) 0.038(5) -0.004(4) 0.012(4) -0.006(4) C14 0.027(4) 0.026(4) 0.031(5) -0.008(4) 0.003(4) -0.005(4) C15 0.037(5) 0.041(5) 0.038(6) 0.003(4) 0.018(5) -0.003(4) C16 0.028(5) 0.038(5) 0.032(5) 0.003(4) 0.019(4) -0.007(4) C17 0.040(5) 0.034(5) 0.032(5) -0.004(4) 0.009(4) -0.003(4) C18 0.044(6) 0.033(5) 0.024(5) 0.011(4) 0.017(4) 0.001(4) C19 0.051(6) 0.039(5) 0.031(5) -0.005(4) 0.025(5) 0.001(5) C20 0.037(5) 0.028(5) 0.022(4) -0.001(3) 0.008(4) -0.007(4) C21 0.025(4) 0.032(5) 0.035(5) 0.000(4) 0.015(4) -0.005(4) C22 0.023(4) 0.029(5) 0.036(5) 0.009(4) 0.008(4) 0.000(4) C23 0.029(5) 0.036(5) 0.044(6) 0.008(4) 0.013(4) 0.001(4) C24 0.030(5) 0.023(4) 0.030(5) -0.001(3) 0.004(4) -0.006(4) C3 0.037(5) 0.024(4) 0.035(5) 0.007(4) 0.017(4) 0.005(4) O4 0.034(4) 0.050(4) 0.043(4) 0.007(3) 0.011(3) -0.013(3) O5 0.060(5) 0.042(4) 0.033(4) -0.010(3) 0.020(3) -0.029(4) O2 0.043(4) 0.035(4) 0.048(4) 0.009(3) 0.018(3) 0.010(3) O3 0.060(5) 0.046(4) 0.046(4) 0.011(3) 0.035(4) 0.023(4) C4 0.029(5) 0.044(6) 0.031(5) 0.009(4) 0.011(4) 0.009(4) C5 0.040(5) 0.040(5) 0.023(5) -0.005(4) 0.014(4) -0.005(4) C6 0.028(5) 0.036(5) 0.038(5) -0.007(4) 0.004(4) -0.007(4) C7 0.026(5) 0.034(5) 0.045(6) 0.013(4) 0.020(4) 0.005(4) C8 0.037(5) 0.028(5) 0.026(5) -0.002(4) 0.009(4) -0.008(4) C9 0.038(6) 0.052(6) 0.027(5) -0.014(4) 0.014(4) -0.005(5) C10 0.036(5) 0.049(6) 0.036(6) -0.009(5) 0.006(4) 0.008(5) O6 0.050(4) 0.048(4) 0.044(4) -0.010(3) 0.027(4) 0.002(3) O7 0.039(4) 0.057(5) 0.032(4) 0.008(3) 0.012(3) 0.004(3) O8 0.049(4) 0.040(4) 0.032(4) -0.004(3) 0.009(3) -0.023(3) O9 0.038(4) 0.076(6) 0.041(4) -0.008(4) 0.018(3) -0.025(4) O10 0.050(5) 0.060(5) 0.051(5) -0.017(4) 0.022(4) 0.019(4) O11 0.042(4) 0.065(5) 0.031(4) -0.005(3) 0.005(3) 0.028(4) O12 0.050(4) 0.034(4) 0.038(4) 0.005(3) 0.006(3) -0.011(3) O13 0.045(4) 0.026(3) 0.057(5) -0.001(3) 0.021(4) 0.000(3) O14 0.036(4) 0.049(4) 0.030(4) 0.000(3) 0.015(3) -0.010(3) O15 0.040(4) 0.057(5) 0.032(4) -0.010(3) 0.005(3) -0.023(4) O16 0.038(4) 0.049(4) 0.040(4) 0.001(3) 0.016(3) 0.010(3) O17 0.085(6) 0.026(4) 0.048(5) -0.006(3) 0.024(4) 0.017(4) O18 0.053(5) 0.062(5) 0.032(4) -0.022(4) 0.001(4) -0.020(4) O19 0.060(5) 0.046(4) 0.057(5) 0.005(4) 0.039(4) 0.003(4) O20 0.035(4) 0.029(3) 0.039(4) 0.004(3) 0.011(3) 0.002(3) O21 0.038(4) 0.031(4) 0.060(5) -0.002(3) 0.023(4) 0.007(3) O22 0.026(3) 0.043(4) 0.040(4) 0.010(3) -0.004(3) -0.010(3) O23 0.047(4) 0.042(4) 0.057(5) 0.016(4) 0.029(4) 0.002(3) O24 0.044(4) 0.030(4) 0.046(4) -0.010(3) 0.006(3) 0.008(3) C1 0.043(5) 0.027(4) 0.026(5) -0.003(4) 0.017(4) -0.001(4) O1_7 0.030(8) 0.042(8) 0.036(7) 0.013(6) -0.005(6) 0.006(6) C1_7 0.024(6) 0.029(6) 0.032(7) 0.010(5) 0.002(5) 0.008(5) C2_7 0.028(7) 0.037(7) 0.038(8) 0.011(6) -0.005(5) 0.004(6) F1_7 0.085(10) 0.046(6) 0.037(7) -0.007(5) -0.007(6) 0.008(6) F2_7 0.038(7) 0.088(11) 0.030(7) 0.010(6) -0.016(5) 0.013(6) F3_7 0.044(7) 0.057(8) 0.050(7) 0.023(5) 0.006(5) -0.007(6) C3_7 0.057(9) 0.030(7) 0.042(8) 0.002(6) 0.000(6) 0.012(6) F4_7 0.095(10) 0.027(6) 0.067(10) -0.001(7) -0.013(8) -0.006(7) F5_7 0.079(9) 0.061(9) 0.051(8) 0.014(6) 0.019(7) 0.036(7) F6_7 0.084(10) 0.048(8) 0.059(8) 0.028(6) 0.002(7) 0.024(7) C4_7 0.041(8) 0.068(9) 0.037(8) 0.018(8) 0.011(6) 0.013(6) F7_7 0.052(8) 0.109(10) 0.076(10) 0.029(9) 0.021(7) -0.026(8) F8_7 0.056(8) 0.090(12) 0.037(8) 0.022(8) -0.002(6) -0.010(7) F9_7 0.093(13) 0.098(11) 0.100(13) 0.007(10) 0.054(11) 0.050(9) O1_8 0.018(7) 0.035(7) 0.042(8) 0.017(6) 0.000(6) 0.000(6) C1_8 0.032(7) 0.031(7) 0.037(8) 0.013(5) 0.008(6) 0.009(5) C2_8 0.106(11) 0.071(11) 0.066(11) 0.016(8) 0.049(10) 0.030(10) F1_8 0.088(10) 0.131(16) 0.154(18) 0.049(14) 0.089(11) 0.032(10) F2_8 0.18(2) 0.098(14) 0.048(12) 0.022(11) 0.039(12) 0.015(17) F3_8 0.134(17) 0.076(9) 0.096(14) -0.006(8) 0.084(13) 0.019(10) C3_8 0.040(7) 0.049(9) 0.057(10) 0.015(6) -0.006(6) 0.007(7) F4_8 0.019(6) 0.066(9) 0.085(9) 0.015(7) 0.009(6) 0.008(6) F5_8 0.094(14) 0.060(9) 0.052(9) 0.011(7) -0.048(8) 0.000(9) F6_8 0.052(9) 0.066(8) 0.096(12) 0.045(8) -0.014(8) 0.021(7) C4_8 0.053(8) 0.043(8) 0.048(9) 0.010(6) 0.006(6) -0.003(7) F7_8 0.095(10) 0.052(8) 0.043(8) -0.015(6) 0.023(7) 0.001(8) F8_8 0.080(10) 0.034(7) 0.064(9) 0.016(7) 0.024(7) -0.002(6) F9_8 0.039(6) 0.042(7) 0.081(9) 0.017(6) -0.002(6) -0.018(5) O1_9 0.031(5) 0.029(4) 0.034(5) -0.008(3) 0.013(4) -0.009(3) C1_9 0.024(4) 0.024(4) 0.045(4) -0.002(3) 0.011(3) -0.003(3) C2_9 0.031(4) 0.043(5) 0.046(4) 0.004(3) 0.016(3) 0.009(3) F1_9 0.042(7) 0.064(8) 0.068(6) 0.006(5) 0.027(5) 0.025(6) F2_9 0.058(6) 0.047(5) 0.051(5) 0.009(4) 0.025(4) 0.008(4) F3_9 0.043(5) 0.067(5) 0.043(5) 0.002(4) 0.006(3) 0.001(4) C3_9 0.034(4) 0.019(4) 0.069(5) 0.002(3) 0.027(4) 0.000(3) F4_9 0.036(5) 0.029(4) 0.099(7) 0.015(5) 0.027(5) 0.007(3) F5_9 0.056(5) 0.036(5) 0.071(5) -0.007(4) 0.040(4) -0.004(4) F6_9 0.042(5) 0.025(4) 0.104(9) 0.001(4) 0.040(5) -0.005(3) C4_9 0.053(5) 0.031(4) 0.049(4) -0.005(3) 0.009(3) -0.010(4) F7_9 0.057(5) 0.052(6) 0.074(7) -0.010(5) -0.017(4) -0.019(4) F8_9 0.068(6) 0.027(4) 0.069(6) -0.011(3) 0.019(5) -0.012(4) F9_9 0.077(6) 0.047(5) 0.049(5) -0.015(4) 0.022(4) -0.015(5) O1_12 0.027(6) 0.031(6) 0.056(9) -0.005(5) 0.017(6) -0.009(5) C1_12 0.029(6) 0.031(6) 0.038(6) 0.005(5) 0.009(5) -0.003(5) C2_12 0.035(7) 0.041(7) 0.034(7) 0.000(6) 0.010(5) 0.005(5) F1_12 0.036(6) 0.058(7) 0.058(8) -0.002(6) -0.001(5) 0.007(5) F2_12 0.049(8) 0.041(5) 0.068(9) -0.010(5) 0.018(7) -0.006(5) F3_12 0.066(8) 0.036(6) 0.048(6) -0.007(5) 0.030(6) 0.004(5) C3_12 0.050(8) 0.033(7) 0.045(8) -0.003(5) 0.005(6) 0.002(5) F4_12 0.050(7) 0.039(6) 0.059(7) -0.004(5) -0.011(5) 0.012(5) F5_12 0.042(8) 0.039(7) 0.062(8) -0.017(6) 0.007(6) 0.011(6) F6_12 0.070(9) 0.043(7) 0.066(9) 0.024(6) 0.018(7) 0.016(6) C4_12 0.044(7) 0.020(6) 0.035(6) 0.000(5) 0.013(5) -0.010(5) F7_12 0.074(9) 0.053(8) 0.037(5) -0.008(5) 0.017(5) 0.003(6) F8_12 0.057(8) 0.038(6) 0.102(11) -0.009(7) 0.053(8) -0.021(6) F9_12 0.041(11) 0.029(6) 0.042(8) -0.005(6) 0.021(7) -0.005(6) O1_13 0.025(6) 0.036(6) 0.033(7) 0.012(5) -0.009(5) -0.013(5) C1_13 0.017(6) 0.029(6) 0.030(7) 0.000(5) 0.005(5) 0.001(5) C2_13 0.026(6) 0.027(7) 0.043(7) -0.010(6) -0.003(6) 0.001(5) F1_13 0.035(11) 0.043(9) 0.063(11) -0.009(9) 0.016(9) 0.008(8) F2_13 0.020(6) 0.037(6) 0.097(11) 0.010(6) -0.024(6) -0.005(5) F3_13 0.040(7) 0.047(7) 0.039(6) 0.004(5) -0.013(5) -0.001(6) C3_13 0.057(10) 0.093(11) 0.032(9) 0.008(6) 0.015(7) 0.047(8) F4_13 0.072(12) 0.121(19) 0.069(12) -0.001(10) 0.015(9) 0.073(13) F5_13 0.070(10) 0.169(14) 0.062(10) 0.056(10) 0.047(8) 0.068(9) F6_13 0.123(13) 0.092(11) 0.033(8) -0.018(7) -0.005(8) 0.057(9) C4_13 0.049(7) 0.034(7) 0.026(7) 0.001(5) 0.000(5) -0.011(6) F7_13 0.044(6) 0.034(6) 0.028(5) 0.015(4) -0.005(4) -0.013(5) F8_13 0.023(6) 0.024(5) 0.052(7) 0.002(4) -0.002(5) -0.001(4) F9_13 0.075(8) 0.058(8) 0.052(8) -0.003(6) 0.037(7) -0.025(7) O1_14 0.029(6) 0.027(5) 0.040(8) -0.008(5) 0.014(6) -0.002(5) C1_14 0.030(5) 0.025(5) 0.047(5) -0.004(4) 0.014(3) -0.002(4) C2_14 0.042(6) 0.025(5) 0.046(6) -0.005(4) 0.018(4) 0.000(4) F1_14 0.031(8) 0.036(10) 0.056(7) 0.004(6) 0.019(5) 0.002(6) F2_14 0.049(8) 0.034(7) 0.064(9) -0.017(6) 0.010(6) 0.003(6) F3_14 0.062(9) 0.039(8) 0.057(9) 0.000(6) 0.036(8) 0.004(6) C3_14 0.032(5) 0.035(6) 0.053(5) 0.002(5) 0.007(4) -0.007(4) F4_14 0.032(7) 0.036(6) 0.062(10) 0.019(6) 0.019(7) 0.002(5) F5_14 0.062(10) 0.055(9) 0.048(6) -0.004(7) 0.012(6) -0.013(8) F6_14 0.028(7) 0.042(7) 0.088(12) 0.008(8) 0.003(6) -0.009(6) C4_14 0.035(6) 0.033(5) 0.055(5) 0.004(5) 0.021(4) 0.004(4) F7_14 0.044(7) 0.041(8) 0.072(11) 0.012(8) 0.035(7) 0.011(7) F8_14 0.046(8) 0.031(5) 0.068(10) 0.008(6) 0.022(7) 0.003(5) F9_14 0.043(6) 0.056(10) 0.055(6) 0.008(7) 0.016(5) -0.001(7) O1_15 0.025(5) 0.044(6) 0.028(5) 0.004(4) -0.001(4) 0.007(4) C1_15 0.040(4) 0.041(4) 0.035(4) 0.013(3) -0.002(3) 0.001(3) C2_15 0.033(5) 0.060(5) 0.050(6) 0.018(4) 0.000(4) 0.007(4) F1_15 0.073(8) 0.055(5) 0.065(7) 0.005(5) 0.014(5) 0.009(5) F2_15 0.054(6) 0.075(8) 0.072(7) 0.025(6) -0.027(5) 0.012(5) F3_15 0.042(8) 0.104(8) 0.105(10) 0.064(8) 0.031(7) 0.028(6) C3_15 0.094(7) 0.042(5) 0.045(5) 0.015(4) -0.027(5) 0.000(4) F4_15 0.154(9) 0.058(6) 0.047(7) -0.003(5) -0.015(7) 0.037(6) F5_15 0.093(6) 0.057(6) 0.084(7) 0.010(6) -0.033(5) -0.039(5) F6_15 0.168(11) 0.062(7) 0.041(5) 0.009(5) -0.038(5) 0.002(7) C4_15 0.056(5) 0.061(5) 0.038(5) 0.013(4) 0.015(4) 0.004(4) F7_15 0.105(10) 0.132(8) 0.052(7) 0.016(6) 0.038(7) 0.051(7) F8_15 0.061(6) 0.078(7) 0.048(5) 0.035(5) 0.024(4) 0.008(5) F9_15 0.071(7) 0.068(6) 0.062(6) 0.013(4) 0.022(5) -0.025(5) O1_16 0.020(10) 0.028(9) 0.037(9) 0.000(7) -0.003(8) -0.002(7) C1_16 0.047(6) 0.045(6) 0.049(6) 0.015(5) -0.003(5) 0.003(4) C2_16 0.048(7) 0.052(7) 0.063(8) 0.015(6) 0.000(6) 0.006(5) F1_16 0.055(11) 0.057(9) 0.105(15) -0.008(9) 0.005(9) 0.002(9) F2_16 0.048(9) 0.080(14) 0.066(11) 0.029(10) 0.008(7) 0.019(8) F3_16 0.028(10) 0.081(12) 0.063(11) 0.027(10) -0.004(8) 0.019(9) C3_16 0.098(8) 0.058(8) 0.054(7) 0.009(6) -0.016(6) -0.005(6) F4_16 0.138(13) 0.080(10) 0.051(13) -0.014(8) -0.027(11) 0.019(10) F5_16 0.093(8) 0.065(12) 0.092(14) 0.029(11) -0.041(8) -0.018(8) F6_16 0.151(14) 0.099(12) 0.053(8) 0.024(9) -0.010(10) -0.017(11) C4_16 0.061(7) 0.068(8) 0.056(8) 0.019(6) 0.006(6) -0.009(6) F7_16 0.054(11) 0.110(12) 0.067(12) -0.005(11) 0.008(9) -0.016(9) F8_16 0.065(12) 0.068(9) 0.092(13) 0.032(9) -0.002(10) -0.018(8) F9_16 0.032(9) 0.043(11) 0.066(9) 0.002(8) 0.007(7) -0.003(7) O1_17 0.042(9) 0.032(8) 0.048(6) -0.020(7) 0.019(6) -0.012(7) C1_17 0.048(5) 0.051(5) 0.049(5) -0.018(5) 0.020(4) 0.001(5) C2_17 0.058(6) 0.084(7) 0.055(6) -0.026(6) 0.010(5) 0.003(6) F1_17 0.048(6) 0.068(11) 0.076(11) -0.058(9) 0.010(7) -0.014(8) F2_17 0.053(12) 0.094(11) 0.060(9) -0.038(10) 0.010(8) -0.016(11) F3_17 0.071(12) 0.088(8) 0.047(12) -0.013(7) 0.015(10) 0.020(8) C3_17 0.052(6) 0.057(6) 0.048(7) -0.011(6) 0.024(5) 0.000(5) F4_17 0.044(8) 0.068(12) 0.055(7) -0.018(7) 0.021(6) 0.000(7) F5_17 0.084(13) 0.067(8) 0.061(11) 0.004(9) 0.041(10) 0.010(8) F6_17 0.058(10) 0.079(11) 0.067(9) -0.028(9) 0.033(8) -0.003(9) C4_17 0.079(7) 0.047(5) 0.081(7) -0.019(5) 0.038(6) 0.004(5) F7_17 0.081(8) 0.053(12) 0.105(11) -0.007(10) 0.035(8) 0.027(8) F8_17 0.113(14) 0.074(11) 0.104(9) -0.044(9) 0.057(9) -0.003(12) F9_17 0.107(10) 0.046(9) 0.116(13) -0.036(10) 0.063(10) -0.017(9) O1_18 0.052(6) 0.030(4) 0.039(4) -0.006(3) 0.018(4) 0.002(4) C1_18 0.047(4) 0.041(4) 0.045(4) -0.013(3) 0.024(3) -0.007(3) C2_18 0.083(6) 0.038(4) 0.067(6) -0.017(4) 0.044(4) -0.018(4) F1_18 0.106(6) 0.046(6) 0.081(7) 0.010(5) 0.039(5) -0.001(5) F2_18 0.131(9) 0.059(6) 0.080(6) -0.029(5) 0.050(6) -0.048(6) F3_18 0.124(8) 0.054(6) 0.100(7) -0.013(5) 0.082(7) -0.029(6) C3_18 0.057(5) 0.094(6) 0.057(5) -0.020(5) 0.007(4) -0.003(5) F4_18 0.102(9) 0.103(6) 0.040(7) 0.010(5) 0.013(6) 0.027(5) F5_18 0.062(6) 0.179(12) 0.173(13) -0.001(12) 0.004(7) -0.043(8) F6_18 0.135(12) 0.171(13) 0.056(5) -0.043(8) 0.000(6) 0.038(10) C4_18 0.049(4) 0.047(4) 0.047(5) -0.002(3) 0.024(3) 0.000(4) F7_18 0.077(7) 0.048(4) 0.056(5) 0.001(4) 0.035(4) -0.005(4) F8_18 0.071(6) 0.051(4) 0.056(5) -0.002(4) 0.036(4) 0.012(4) F9_18 0.043(4) 0.070(6) 0.064(5) -0.001(4) 0.015(3) 0.005(4) O1_19 0.034(7) 0.029(6) 0.044(5) 0.004(5) 0.019(5) -0.005(5) C1_19 0.045(4) 0.031(4) 0.047(4) 0.003(3) 0.020(4) -0.006(4) C2_19 0.054(4) 0.039(4) 0.045(4) 0.001(4) 0.014(4) -0.011(4) F1_19 0.055(7) 0.037(4) 0.046(7) 0.009(4) 0.012(7) -0.008(5) F2_19 0.060(6) 0.055(6) 0.046(5) -0.008(5) 0.017(5) -0.016(5) F3_19 0.051(4) 0.035(6) 0.056(7) -0.008(6) 0.009(4) -0.006(5) C3_19 0.049(4) 0.033(4) 0.057(5) 0.001(3) 0.018(4) -0.010(4) F4_19 0.053(6) 0.033(6) 0.057(5) 0.006(5) 0.027(5) -0.004(5) F5_19 0.045(5) 0.041(6) 0.069(7) 0.000(6) 0.017(5) -0.013(4) F6_19 0.069(6) 0.040(5) 0.058(5) -0.003(4) 0.018(5) -0.010(5) C4_19 0.046(4) 0.034(5) 0.048(5) -0.001(4) 0.026(4) -0.004(4) F7_19 0.044(6) 0.031(7) 0.050(5) 0.000(5) 0.024(4) 0.001(6) F8_19 0.052(6) 0.042(5) 0.064(7) -0.019(5) 0.024(6) -0.011(5) F9_19 0.045(7) 0.038(5) 0.042(6) -0.004(5) 0.023(6) -0.009(6) F1_21 0.108(16) 0.16(2) 0.17(3) -0.081(18) 0.043(15) 0.020(13) F2_21 0.26(3) 0.21(3) 0.12(2) -0.05(2) 0.08(2) -0.09(2) F3_21 0.30(3) 0.100(16) 0.088(19) 0.011(14) 0.02(2) 0.056(18) F4_21 0.19(2) 0.14(2) 0.135(19) 0.035(16) 0.068(18) 0.068(16) C1_21 0.104(15) 0.094(16) 0.09(2) -0.056(13) 0.020(14) 0.011(12) C2_21 0.16(2) 0.102(17) 0.100(19) -0.038(15) 0.035(18) 0.002(14) C3_21 0.186(19) 0.085(15) 0.045(15) -0.018(12) 0.033(15) 0.041(13) C4_21 0.173(19) 0.097(16) 0.069(18) -0.017(13) 0.038(16) 0.043(13) C5_21 0.129(17) 0.111(17) 0.051(16) -0.003(14) 0.029(15) 0.033(14) C6_21 0.103(16) 0.100(16) 0.051(15) -0.040(12) 0.002(13) 0.013(12) O1_10 0.040(6) 0.035(5) 0.055(5) 0.006(4) 0.018(4) -0.014(4) C1_10 0.049(4) 0.035(4) 0.050(4) 0.005(3) 0.015(3) -0.011(3) C2_10 0.066(5) 0.046(5) 0.058(5) 0.003(3) 0.007(4) -0.017(4) F1_10 0.060(6) 0.044(5) 0.069(6) 0.001(5) 0.002(5) -0.023(5) F2_10 0.106(7) 0.061(6) 0.067(6) -0.015(5) 0.018(5) -0.017(5) F3_10 0.074(6) 0.056(6) 0.068(6) 0.010(5) -0.011(5) -0.018(5) C3_10 0.055(5) 0.038(4) 0.046(4) 0.005(4) 0.019(4) -0.010(3) F4_10 0.052(5) 0.035(6) 0.048(5) 0.003(5) 0.022(5) -0.012(4) F5_10 0.056(6) 0.036(4) 0.052(7) 0.012(4) 0.016(5) -0.010(4) F6_10 0.081(7) 0.054(6) 0.046(4) 0.002(4) 0.025(4) -0.010(5) C4_10 0.057(4) 0.038(4) 0.060(5) 0.003(4) 0.020(4) -0.005(3) F7_10 0.046(5) 0.044(6) 0.061(5) 0.004(5) 0.017(4) 0.000(5) F8_10 0.075(6) 0.065(7) 0.070(6) -0.001(5) 0.034(5) -0.005(5) F9_10 0.073(6) 0.031(4) 0.053(6) 0.000(4) 0.023(5) -0.005(4) O1_20 0.043(9) 0.035(8) 0.049(6) 0.003(6) 0.019(7) -0.011(7) C1_20 0.049(4) 0.037(5) 0.050(5) 0.001(4) 0.016(4) -0.009(4) C2_20 0.057(5) 0.041(5) 0.048(5) 0.001(4) 0.015(4) -0.010(4) F1_20 0.057(5) 0.040(6) 0.048(6) 0.003(6) 0.017(5) -0.009(5) F2_20 0.069(7) 0.045(6) 0.050(5) 0.000(5) 0.014(6) -0.014(6) F3_20 0.055(7) 0.042(6) 0.051(8) 0.004(5) 0.013(7) -0.008(6) C3_20 0.049(4) 0.037(5) 0.056(6) -0.001(5) 0.014(5) -0.010(4) F4_20 0.038(9) 0.035(10) 0.057(7) -0.002(6) 0.013(7) -0.010(8) F5_20 0.049(6) 0.037(7) 0.055(8) -0.009(7) 0.002(7) -0.011(6) F6_20 0.053(8) 0.038(6) 0.058(7) -0.003(6) 0.018(7) -0.011(6) C4_20 0.053(4) 0.038(5) 0.059(5) 0.002(4) 0.022(5) -0.006(4) F7_20 0.056(8) 0.038(7) 0.061(7) 0.004(6) 0.022(7) -0.006(6) F8_20 0.063(8) 0.042(7) 0.063(6) -0.002(5) 0.027(6) -0.008(7) F9_20 0.050(5) 0.047(7) 0.059(8) 0.002(7) 0.025(6) -0.006(5) F1_22 0.102(6) 0.067(5) 0.078(5) 0.027(4) 0.057(5) 0.024(4) F2_22 0.126(7) 0.069(5) 0.119(7) 0.044(5) 0.067(6) 0.048(5) F3_22 0.127(9) 0.090(7) 0.235(14) 0.112(8) 0.075(9) 0.030(6) F4_22 0.078(6) 0.109(8) 0.236(13) 0.108(9) 0.037(7) -0.004(6) C1_22 0.091(7) 0.037(5) 0.043(6) 0.004(4) 0.033(6) 0.011(5) C2_22 0.094(7) 0.039(6) 0.066(8) 0.011(5) 0.039(7) 0.013(5) C3_22 0.086(7) 0.039(6) 0.096(10) 0.030(6) 0.022(7) 0.003(5) C4_22 0.071(7) 0.058(7) 0.104(11) 0.038(7) 0.014(7) -0.005(5) C5_22 0.065(7) 0.053(7) 0.080(9) 0.026(6) 0.010(7) 0.004(6) C6_22 0.079(7) 0.032(5) 0.051(7) 0.010(5) 0.017(6) 0.002(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Os2 C6 1.896(10) . ? Os2 C7 1.914(10) . ? Os2 C5 1.969(10) . ? Os2 C8 1.972(9) . ? Os2 Os1 2.8958(9) . ? Os2 Os3 2.8968(10) . ? Os3 C10 1.906(10) . ? Os3 C11 1.917(10) . ? Os3 C12 1.973(11) . ? Os3 C9 1.976(11) . ? Os3 Ag1 2.9152(10) . ? Os3 Os1 3.0081(6) . ? Os4 C23 1.918(10) . ? Os4 C22 1.937(10) . ? Os4 C21 1.951(9) . ? Os4 C24 1.968(9) . ? Os4 Ag1 2.8991(10) . ? Os4 Os5 2.9023(11) . ? Os4 Os6 2.9980(7) . ? Os5 C18 1.946(10) . ? Os5 C19 1.948(9) . ? Os5 C17 1.958(10) . ? Os5 C20 1.959(9) . ? Os5 Os6 2.9015(9) . ? Os6 C14 1.912(9) . ? Os6 C15 1.913(10) . ? Os6 C16 1.940(10) . ? Os6 C13 1.967(10) . ? Os6 Ag1 2.9078(12) . ? Os1 C3 1.916(9) . ? Os1 C2 1.925(10) . ? Os1 C1 1.975(10) . ? Os1 C4 1.979(11) . ? Os1 Ag1 2.9053(12) . ? Ag1 C11 2.684(9) . ? Al1 O1_19 1.686(17) . ? Al1 O1_7 1.692(16) . ? Al1 O1_12 1.694(14) . ? Al1 F1 1.760(12) . ? Al2 O1_10 1.685(16) . ? Al2 O1_13 1.695(16) . ? Al2 O1_8 1.720(16) . ? Al2 F1B 1.772(11) . ? Al08 O1_16 1.677(12) . ? Al08 O1_9 1.680(8) . ? Al08 O1_17 1.697(12) . ? Al08 O1_18 1.712(8) . ? Al08 O1_15 1.746(8) . ? Al08 F1 1.750(10) . ? Al08 O1_14 1.772(11) . ? Al08 F1B 1.781(10) . ? O1 C1 1.105(11) . ? C2 O2 1.132(11) . ? C11 O11 1.146(11) . ? C12 O12 1.116(12) . ? C13 O13 1.123(11) . ? C14 O14 1.163(11) . ? C15 O15 1.146(12) . ? C16 O16 1.145(11) . ? C17 O17 1.149(11) . ? C18 O18 1.110(11) . ? C19 O19 1.103(11) . ? C20 O20 1.131(11) . ? C21 O21 1.136(11) . ? C22 O22 1.128(11) . ? C23 O23 1.134(11) . ? C24 O24 1.123(11) . ? C3 O3 1.156(11) . ? O4 C4 1.117(12) . ? O5 C5 1.124(11) . ? C6 O6 1.164(11) . ? C7 O7 1.141(11) . ? C8 O8 1.125(10) . ? C9 O9 1.121(12) . ? C10 O10 1.147(12) . ? O1_7 C1_7 1.373(12) . ? C1_7 C3_7 1.538(12) . ? C1_7 C2_7 1.555(12) . ? C1_7 C4_7 1.564(12) . ? C2_7 F1_7 1.324(12) . ? C2_7 F2_7 1.333(12) . ? C2_7 F3_7 1.339(12) . ? C3_7 F5_7 1.326(12) . ? C3_7 F6_7 1.346(12) . ? C3_7 F4_7 1.349(12) . ? C4_7 F7_7 1.331(12) . ? C4_7 F8_7 1.335(12) . ? C4_7 F9_7 1.338(12) . ? O1_8 C1_8 1.373(13) . ? C1_8 C2_8 1.545(12) . ? C1_8 C4_8 1.551(13) . ? C1_8 C3_8 1.553(12) . ? C2_8 F3_8 1.338(13) . ? C2_8 F2_8 1.353(13) . ? C2_8 F1_8 1.355(13) . ? C3_8 F4_8 1.340(12) . ? C3_8 F6_8 1.346(12) . ? C3_8 F5_8 1.352(13) . ? C4_8 F9_8 1.343(12) . ? C4_8 F7_8 1.348(13) . ? C4_8 F8_8 1.354(12) . ? O1_9 C1_9 1.366(11) . ? C1_9 C2_9 1.551(11) . ? C1_9 C4_9 1.555(11) . ? C1_9 C3_9 1.557(11) . ? C2_9 F2_9 1.331(11) . ? C2_9 F3_9 1.331(11) . ? C2_9 F1_9 1.343(12) . ? C3_9 F4_9 1.329(11) . ? C3_9 F6_9 1.346(11) . ? C3_9 F5_9 1.347(11) . ? C4_9 F9_9 1.328(11) . ? C4_9 F8_9 1.331(11) . ? C4_9 F7_9 1.353(11) . ? O1_12 C1_12 1.368(12) . ? C1_12 C2_12 1.549(12) . ? C1_12 C3_12 1.553(12) . ? C1_12 C4_12 1.559(12) . ? C2_12 F2_12 1.326(12) . ? C2_12 F3_12 1.330(12) . ? C2_12 F1_12 1.347(12) . ? C3_12 F6_12 1.328(12) . ? C3_12 F4_12 1.346(12) . ? C3_12 F5_12 1.348(12) . ? C4_12 F8_12 1.333(11) . ? C4_12 F9_12 1.337(13) . ? C4_12 F7_12 1.347(12) . ? O1_13 C1_13 1.363(12) . ? C1_13 C4_13 1.546(12) . ? C1_13 C3_13 1.548(12) . ? C1_13 C2_13 1.558(12) . ? C2_13 F2_13 1.335(12) . ? C2_13 F3_13 1.341(12) . ? C2_13 F1_13 1.345(13) . ? C3_13 F5_13 1.333(13) . ? C3_13 F6_13 1.333(13) . ? C3_13 F4_13 1.349(13) . ? C4_13 F7_13 1.331(12) . ? C4_13 F8_13 1.343(12) . ? C4_13 F9_13 1.363(12) . ? O1_14 C1_14 1.375(13) . ? C1_14 C2_14 1.555(13) . ? C1_14 C3_14 1.557(13) . ? C1_14 C4_14 1.558(13) . ? C2_14 F3_14 1.337(13) . ? C2_14 F2_14 1.339(13) . ? C2_14 F1_14 1.345(13) . ? C3_14 F4_14 1.333(13) . ? C3_14 F6_14 1.349(13) . ? C3_14 F5_14 1.350(13) . ? C4_14 F7_14 1.336(13) . ? C4_14 F9_14 1.339(13) . ? C4_14 F8_14 1.346(13) . ? O1_15 C1_15 1.358(11) . ? C1_15 C3_15 1.544(12) . ? C1_15 C4_15 1.556(11) . ? C1_15 C2_15 1.567(11) . ? C2_15 F3_15 1.326(11) . ? C2_15 F1_15 1.340(11) . ? C2_15 F2_15 1.342(11) . ? C3_15 F5_15 1.335(12) . ? C3_15 F4_15 1.349(12) . ? C3_15 F6_15 1.359(11) . ? C4_15 F7_15 1.333(11) . ? C4_15 F8_15 1.338(11) . ? C4_15 F9_15 1.340(11) . ? O1_16 C1_16 1.344(14) . ? C1_16 C3_16 1.549(13) . ? C1_16 C2_16 1.549(13) . ? C1_16 C4_16 1.565(13) . ? C2_16 F3_16 1.332(14) . ? C2_16 F2_16 1.339(13) . ? C2_16 F1_16 1.353(14) . ? C3_16 F6_16 1.345(13) . ? C3_16 F5_16 1.346(13) . ? C3_16 F4_16 1.364(14) . ? C4_16 F7_16 1.340(13) . ? C4_16 F8_16 1.341(13) . ? C4_16 F9_16 1.344(13) . ? O1_17 C1_17 1.360(14) . ? C1_17 C4_17 1.545(13) . ? C1_17 C3_17 1.546(13) . ? C1_17 C2_17 1.558(13) . ? C2_17 F2_17 1.327(13) . ? C2_17 F3_17 1.328(14) . ? C2_17 F1_17 1.347(14) . ? C3_17 F6_17 1.340(13) . ? C3_17 F4_17 1.340(13) . ? C3_17 F5_17 1.341(13) . ? C4_17 F8_17 1.338(13) . ? C4_17 F9_17 1.342(14) . ? C4_17 F7_17 1.351(14) . ? O1_18 C1_18 1.366(11) . ? C1_18 C3_18 1.544(12) . ? C1_18 C4_18 1.546(11) . ? C1_18 C2_18 1.546(11) . ? C2_18 F3_18 1.330(11) . ? C2_18 F2_18 1.331(11) . ? C2_18 F1_18 1.339(12) . ? C3_18 F4_18 1.324(12) . ? C3_18 F5_18 1.335(12) . ? C3_18 F6_18 1.339(12) . ? C4_18 F9_18 1.312(11) . ? C4_18 F8_18 1.339(11) . ? C4_18 F7_18 1.348(11) . ? O1_19 C1_19 1.375(14) . ? C1_19 C3_19 1.543(13) . ? C1_19 C4_19 1.552(13) . ? C1_19 C2_19 1.555(13) . ? C2_19 F2_19 1.339(13) . ? C2_19 F1_19 1.340(13) . ? C2_19 F3_19 1.345(13) . ? C3_19 F5_19 1.339(13) . ? C3_19 F6_19 1.339(13) . ? C3_19 F4_19 1.343(13) . ? C4_19 F8_19 1.325(13) . ? C4_19 F9_19 1.334(13) . ? C4_19 F7_19 1.348(13) . ? F1_21 C1_21 1.332(15) . ? F2_21 C2_21 1.320(15) . ? F3_21 C3_21 1.328(15) . ? F4_21 C4_21 1.300(15) . ? C1_21 C2_21 1.379(14) . ? C1_21 C6_21 1.387(14) . ? C2_21 C3_21 1.386(13) . ? C3_21 C4_21 1.374(14) . ? C4_21 C5_21 1.381(14) . ? C5_21 C6_21 1.363(15) . ? C5_21 H5_21 0.9500 . ? C6_21 H6_21 0.9500 . ? O1_10 C1_10 1.352(13) . ? C1_10 C3_10 1.547(12) . ? C1_10 C2_10 1.549(12) . ? C1_10 C4_10 1.570(12) . ? C2_10 F3_10 1.333(12) . ? C2_10 F1_10 1.341(13) . ? C2_10 F2_10 1.361(13) . ? C3_10 F6_10 1.339(12) . ? C3_10 F5_10 1.343(13) . ? C3_10 F4_10 1.345(13) . ? C4_10 F8_10 1.340(13) . ? C4_10 F7_10 1.345(12) . ? C4_10 F9_10 1.345(12) . ? O1_20 C1_20 1.369(15) . ? C1_20 C4_20 1.549(13) . ? C1_20 C2_20 1.553(13) . ? C1_20 C3_20 1.558(14) . ? C2_20 F2_20 1.339(14) . ? C2_20 F3_20 1.339(14) . ? C2_20 F1_20 1.343(14) . ? C3_20 F6_20 1.337(14) . ? C3_20 F5_20 1.344(14) . ? C3_20 F4_20 1.344(14) . ? C4_20 F7_20 1.340(14) . ? C4_20 F9_20 1.343(14) . ? C4_20 F8_20 1.344(14) . ? F1_22 C1_22 1.339(11) . ? F2_22 C2_22 1.322(11) . ? F3_22 C3_22 1.338(10) . ? F4_22 C4_22 1.331(11) . ? C1_22 C6_22 1.369(11) . ? C1_22 C2_22 1.381(10) . ? C2_22 C3_22 1.375(11) . ? C3_22 C4_22 1.371(11) . ? C4_22 C5_22 1.377(11) . ? C5_22 C6_22 1.383(11) . ? C5_22 H5_22 0.9500 . ? C6_22 H6_22 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 Os2 C7 99.7(4) . . ? C6 Os2 C5 90.6(4) . . ? C7 Os2 C5 91.3(4) . . ? C6 Os2 C8 90.4(4) . . ? C7 Os2 C8 89.2(4) . . ? C5 Os2 C8 178.8(4) . . ? C6 Os2 Os1 160.6(3) . . ? C7 Os2 Os1 99.3(3) . . ? C5 Os2 Os1 85.2(2) . . ? C8 Os2 Os1 93.6(3) . . ? C6 Os2 Os3 98.8(3) . . ? C7 Os2 Os3 160.9(3) . . ? C5 Os2 Os3 92.7(3) . . ? C8 Os2 Os3 86.4(3) . . ? Os1 Os2 Os3 62.57(2) . . ? C10 Os3 C11 92.5(4) . . ? C10 Os3 C12 94.1(4) . . ? C11 Os3 C12 89.6(4) . . ? C10 Os3 C9 88.6(4) . . ? C11 Os3 C9 92.3(4) . . ? C12 Os3 C9 176.6(4) . . ? C10 Os3 Os2 86.5(3) . . ? C11 Os3 Os2 178.4(3) . . ? C12 Os3 Os2 91.7(3) . . ? C9 Os3 Os2 86.4(3) . . ? C10 Os3 Ag1 156.1(3) . . ? C11 Os3 Ag1 63.6(3) . . ? C12 Os3 Ag1 84.9(3) . . ? C9 Os3 Ag1 93.5(3) . . ? Os2 Os3 Ag1 117.42(3) . . ? C10 Os3 Os1 145.2(3) . . ? C11 Os3 Os1 122.3(3) . . ? C12 Os3 Os1 86.7(3) . . ? C9 Os3 Os1 89.9(3) . . ? Os2 Os3 Os1 58.697(19) . . ? Ag1 Os3 Os1 58.72(2) . . ? C23 Os4 C22 93.8(4) . . ? C23 Os4 C21 90.5(4) . . ? C22 Os4 C21 91.1(4) . . ? C23 Os4 C24 92.2(4) . . ? C22 Os4 C24 91.0(4) . . ? C21 Os4 C24 176.5(4) . . ? C23 Os4 Ag1 157.8(3) . . ? C22 Os4 Ag1 64.7(3) . . ? C21 Os4 Ag1 95.1(3) . . ? C24 Os4 Ag1 83.3(3) . . ? C23 Os4 Os5 84.0(3) . . ? C22 Os4 Os5 174.8(3) . . ? C21 Os4 Os5 84.2(3) . . ? C24 Os4 Os5 93.8(3) . . ? Ag1 Os4 Os5 117.93(3) . . ? C23 Os4 Os6 142.6(3) . . ? C22 Os4 Os6 123.6(3) . . ? C21 Os4 Os6 90.4(2) . . ? C24 Os4 Os6 86.1(2) . . ? Ag1 Os4 Os6 59.06(2) . . ? Os5 Os4 Os6 58.89(2) . . ? C18 Os5 C19 97.0(4) . . ? C18 Os5 C17 90.7(4) . . ? C19 Os5 C17 90.9(4) . . ? C18 Os5 C20 89.1(4) . . ? C19 Os5 C20 91.0(4) . . ? C17 Os5 C20 178.1(4) . . ? C18 Os5 Os6 100.5(2) . . ? C19 Os5 Os6 162.0(3) . . ? C17 Os5 Os6 85.1(3) . . ? C20 Os5 Os6 93.1(2) . . ? C18 Os5 Os4 161.7(3) . . ? C19 Os5 Os4 100.7(3) . . ? C17 Os5 Os4 93.5(3) . . ? C20 Os5 Os4 86.0(3) . . ? Os6 Os5 Os4 62.20(2) . . ? C14 Os6 C15 93.5(4) . . ? C14 Os6 C16 89.6(4) . . ? C15 Os6 C16 89.9(4) . . ? C14 Os6 C13 90.4(4) . . ? C15 Os6 C13 93.1(4) . . ? C16 Os6 C13 177.0(4) . . ? C14 Os6 Os5 174.0(3) . . ? C15 Os6 Os5 83.2(3) . . ? C16 Os6 Os5 85.3(2) . . ? C13 Os6 Os5 94.9(3) . . ? C14 Os6 Ag1 66.2(3) . . ? C15 Os6 Ag1 158.3(3) . . ? C16 Os6 Ag1 97.4(3) . . ? C13 Os6 Ag1 79.9(3) . . ? Os5 Os6 Ag1 117.68(3) . . ? C14 Os6 Os4 124.6(3) . . ? C15 Os6 Os4 141.8(3) . . ? C16 Os6 Os4 91.6(3) . . ? C13 Os6 Os4 86.0(3) . . ? Os5 Os6 Os4 58.91(2) . . ? Ag1 Os6 Os4 58.78(2) . . ? C3 Os1 C2 94.9(4) . . ? C3 Os1 C1 90.7(4) . . ? C2 Os1 C1 92.0(4) . . ? C3 Os1 C4 89.2(4) . . ? C2 Os1 C4 91.7(4) . . ? C1 Os1 C4 176.3(4) . . ? C3 Os1 Os2 173.0(3) . . ? C2 Os1 Os2 82.0(3) . . ? C1 Os1 Os2 95.8(2) . . ? C4 Os1 Os2 84.5(3) . . ? C3 Os1 Ag1 66.2(3) . . ? C2 Os1 Ag1 159.0(3) . . ? C1 Os1 Ag1 79.7(3) . . ? C4 Os1 Ag1 96.9(3) . . ? Os2 Os1 Ag1 117.77(3) . . ? C3 Os1 Os3 124.8(3) . . ? C2 Os1 Os3 140.2(3) . . ? C1 Os1 Os3 85.7(3) . . ? C4 Os1 Os3 91.3(3) . . ? Os2 Os1 Os3 58.73(2) . . ? Ag1 Os1 Os3 59.04(2) . . ? C11 Ag1 Os4 112.7(2) . . ? C11 Ag1 Os1 102.0(2) . . ? Os4 Ag1 Os1 132.96(3) . . ? C11 Ag1 Os6 98.1(2) . . ? Os4 Ag1 Os6 62.17(2) . . ? Os1 Ag1 Os6 143.44(3) . . ? C11 Ag1 Os3 39.8(2) . . ? Os4 Ag1 Os3 141.97(3) . . ? Os1 Ag1 Os3 62.24(2) . . ? Os6 Ag1 Os3 131.27(3) . . ? O1_19 Al1 O1_7 118.7(10) . . ? O1_19 Al1 O1_12 110.8(9) . . ? O1_7 Al1 O1_12 114.8(8) . . ? O1_19 Al1 F1 104.8(16) . . ? O1_7 Al1 F1 100.4(16) . . ? O1_12 Al1 F1 105.3(17) . . ? O1_10 Al2 O1_13 113.6(8) . . ? O1_10 Al2 O1_8 115.7(10) . . ? O1_13 Al2 O1_8 109.9(8) . . ? O1_10 Al2 F1B 103.5(18) . . ? O1_13 Al2 F1B 103(2) . . ? O1_8 Al2 F1B 109.7(16) . . ? O1_16 Al08 O1_17 125.0(11) . . ? O1_9 Al08 O1_18 113.7(5) . . ? O1_9 Al08 O1_15 109.9(5) . . ? O1_18 Al08 O1_15 113.6(5) . . ? O1_9 Al08 F1 109.2(16) . . ? O1_18 Al08 F1 107.0(14) . . ? O1_15 Al08 F1 102.8(15) . . ? O1_16 Al08 O1_14 109.2(9) . . ? O1_17 Al08 O1_14 112.1(10) . . ? O1_16 Al08 F1B 106.1(16) . . ? O1_17 Al08 F1B 97.9(18) . . ? O1_14 Al08 F1B 103(2) . . ? Al08 F1 Al1 169(3) . . ? Al2 F1B Al08 172(3) . . ? O2 C2 Os1 176.7(9) . . ? O11 C11 Os3 170.9(8) . . ? O11 C11 Ag1 112.5(7) . . ? Os3 C11 Ag1 76.6(3) . . ? O12 C12 Os3 175.7(8) . . ? O13 C13 Os6 176.5(8) . . ? O14 C14 Os6 171.4(8) . . ? O15 C15 Os6 177.7(9) . . ? O16 C16 Os6 176.1(8) . . ? O17 C17 Os5 175.8(9) . . ? O18 C18 Os5 178.3(9) . . ? O19 C19 Os5 178.5(10) . . ? O20 C20 Os5 176.3(8) . . ? O21 C21 Os4 178.0(8) . . ? O22 C22 Os4 171.7(8) . . ? O23 C23 Os4 177.8(9) . . ? O24 C24 Os4 177.6(8) . . ? O3 C3 Os1 171.6(8) . . ? O4 C4 Os1 177.7(8) . . ? O5 C5 Os2 179.0(10) . . ? O6 C6 Os2 179.6(9) . . ? O7 C7 Os2 176.5(9) . . ? O8 C8 Os2 175.6(8) . . ? O9 C9 Os3 175.9(9) . . ? O10 C10 Os3 177.4(9) . . ? O1 C1 Os1 175.8(8) . . ? C1_7 O1_7 Al1 151.3(12) . . ? O1_7 C1_7 C3_7 109.5(10) . . ? O1_7 C1_7 C2_7 107.9(10) . . ? C3_7 C1_7 C2_7 110.0(9) . . ? O1_7 C1_7 C4_7 110.7(10) . . ? C3_7 C1_7 C4_7 109.2(10) . . ? C2_7 C1_7 C4_7 109.5(9) . . ? F1_7 C2_7 F2_7 106.7(12) . . ? F1_7 C2_7 F3_7 110.3(12) . . ? F2_7 C2_7 F3_7 107.5(12) . . ? F1_7 C2_7 C1_7 110.1(11) . . ? F2_7 C2_7 C1_7 112.3(11) . . ? F3_7 C2_7 C1_7 109.9(10) . . ? F5_7 C3_7 F6_7 107.2(12) . . ? F5_7 C3_7 F4_7 108.2(13) . . ? F6_7 C3_7 F4_7 107.3(12) . . ? F5_7 C3_7 C1_7 111.9(11) . . ? F6_7 C3_7 C1_7 112.0(11) . . ? F4_7 C3_7 C1_7 110.1(11) . . ? F7_7 C4_7 F8_7 108.8(13) . . ? F7_7 C4_7 F9_7 111.3(14) . . ? F8_7 C4_7 F9_7 110.7(15) . . ? F7_7 C4_7 C1_7 109.0(11) . . ? F8_7 C4_7 C1_7 108.7(12) . . ? F9_7 C4_7 C1_7 108.3(12) . . ? C1_8 O1_8 Al2 150.4(12) . . ? O1_8 C1_8 C2_8 108.1(11) . . ? O1_8 C1_8 C4_8 111.2(11) . . ? C2_8 C1_8 C4_8 110.0(10) . . ? O1_8 C1_8 C3_8 107.5(10) . . ? C2_8 C1_8 C3_8 110.5(11) . . ? C4_8 C1_8 C3_8 109.6(10) . . ? F3_8 C2_8 F2_8 105.7(16) . . ? F3_8 C2_8 F1_8 113.1(16) . . ? F2_8 C2_8 F1_8 110.0(16) . . ? F3_8 C2_8 C1_8 109.8(12) . . ? F2_8 C2_8 C1_8 110.9(14) . . ? F1_8 C2_8 C1_8 107.3(12) . . ? F4_8 C3_8 F6_8 106.3(13) . . ? F4_8 C3_8 F5_8 112.6(14) . . ? F6_8 C3_8 F5_8 111.9(13) . . ? F4_8 C3_8 C1_8 109.7(11) . . ? F6_8 C3_8 C1_8 108.8(11) . . ? F5_8 C3_8 C1_8 107.6(12) . . ? F9_8 C4_8 F7_8 110.1(13) . . ? F9_8 C4_8 F8_8 105.1(12) . . ? F7_8 C4_8 F8_8 114.6(13) . . ? F9_8 C4_8 C1_8 109.4(11) . . ? F7_8 C4_8 C1_8 108.1(11) . . ? F8_8 C4_8 C1_8 109.5(11) . . ? C1_9 O1_9 Al08 145.0(8) . . ? O1_9 C1_9 C2_9 111.4(9) . . ? O1_9 C1_9 C4_9 106.8(8) . . ? C2_9 C1_9 C4_9 108.9(8) . . ? O1_9 C1_9 C3_9 110.5(8) . . ? C2_9 C1_9 C3_9 108.9(8) . . ? C4_9 C1_9 C3_9 110.3(8) . . ? F2_9 C2_9 F3_9 108.6(10) . . ? F2_9 C2_9 F1_9 110.5(10) . . ? F3_9 C2_9 F1_9 106.7(10) . . ? F2_9 C2_9 C1_9 110.5(9) . . ? F3_9 C2_9 C1_9 109.8(9) . . ? F1_9 C2_9 C1_9 110.6(9) . . ? F4_9 C3_9 F6_9 106.9(9) . . ? F4_9 C3_9 F5_9 109.1(10) . . ? F6_9 C3_9 F5_9 109.2(10) . . ? F4_9 C3_9 C1_9 111.2(9) . . ? F6_9 C3_9 C1_9 109.9(8) . . ? F5_9 C3_9 C1_9 110.4(8) . . ? F9_9 C4_9 F8_9 109.1(10) . . ? F9_9 C4_9 F7_9 107.2(11) . . ? F8_9 C4_9 F7_9 108.3(10) . . ? F9_9 C4_9 C1_9 110.5(9) . . ? F8_9 C4_9 C1_9 111.6(9) . . ? F7_9 C4_9 C1_9 110.0(9) . . ? C1_12 O1_12 Al1 150.6(11) . . ? O1_12 C1_12 C2_12 108.1(10) . . ? O1_12 C1_12 C3_12 109.1(10) . . ? C2_12 C1_12 C3_12 109.6(9) . . ? O1_12 C1_12 C4_12 110.4(10) . . ? C2_12 C1_12 C4_12 109.3(9) . . ? C3_12 C1_12 C4_12 110.2(9) . . ? F2_12 C2_12 F3_12 107.3(11) . . ? F2_12 C2_12 F1_12 108.8(11) . . ? F3_12 C2_12 F1_12 108.2(11) . . ? F2_12 C2_12 C1_12 111.9(10) . . ? F3_12 C2_12 C1_12 110.5(10) . . ? F1_12 C2_12 C1_12 110.0(10) . . ? F6_12 C3_12 F4_12 110.2(12) . . ? F6_12 C3_12 F5_12 106.5(13) . . ? F4_12 C3_12 F5_12 108.9(12) . . ? F6_12 C3_12 C1_12 110.9(11) . . ? F4_12 C3_12 C1_12 109.6(10) . . ? F5_12 C3_12 C1_12 110.7(11) . . ? F8_12 C4_12 F9_12 106.7(14) . . ? F8_12 C4_12 F7_12 110.4(12) . . ? F9_12 C4_12 F7_12 108.9(13) . . ? F8_12 C4_12 C1_12 110.4(10) . . ? F9_12 C4_12 C1_12 111.2(12) . . ? F7_12 C4_12 C1_12 109.1(10) . . ? C1_13 O1_13 Al2 148.9(10) . . ? O1_13 C1_13 C4_13 108.6(9) . . ? O1_13 C1_13 C3_13 108.3(11) . . ? C4_13 C1_13 C3_13 109.9(10) . . ? O1_13 C1_13 C2_13 110.6(10) . . ? C4_13 C1_13 C2_13 111.2(9) . . ? C3_13 C1_13 C2_13 108.2(9) . . ? F2_13 C2_13 F3_13 111.5(12) . . ? F2_13 C2_13 F1_13 106.8(15) . . ? F3_13 C2_13 F1_13 111.5(14) . . ? F2_13 C2_13 C1_13 109.4(10) . . ? F3_13 C2_13 C1_13 110.0(10) . . ? F1_13 C2_13 C1_13 107.6(13) . . ? F5_13 C3_13 F6_13 108.1(14) . . ? F5_13 C3_13 F4_13 107.6(15) . . ? F6_13 C3_13 F4_13 109.7(14) . . ? F5_13 C3_13 C1_13 111.2(11) . . ? F6_13 C3_13 C1_13 110.2(11) . . ? F4_13 C3_13 C1_13 109.9(12) . . ? F7_13 C4_13 F8_13 107.5(11) . . ? F7_13 C4_13 F9_13 109.8(12) . . ? F8_13 C4_13 F9_13 108.9(12) . . ? F7_13 C4_13 C1_13 111.0(10) . . ? F8_13 C4_13 C1_13 111.7(10) . . ? F9_13 C4_13 C1_13 107.8(10) . . ? C1_14 O1_14 Al08 150.1(14) . . ? O1_14 C1_14 C2_14 109.4(11) . . ? O1_14 C1_14 C3_14 110.4(12) . . ? C2_14 C1_14 C3_14 108.7(11) . . ? O1_14 C1_14 C4_14 110.9(11) . . ? C2_14 C1_14 C4_14 107.9(10) . . ? C3_14 C1_14 C4_14 109.5(11) . . ? F3_14 C2_14 F2_14 107.6(14) . . ? F3_14 C2_14 F1_14 110.0(15) . . ? F2_14 C2_14 F1_14 107.7(15) . . ? F3_14 C2_14 C1_14 109.8(12) . . ? F2_14 C2_14 C1_14 111.5(12) . . ? F1_14 C2_14 C1_14 110.4(13) . . ? F4_14 C3_14 F6_14 107.3(14) . . ? F4_14 C3_14 F5_14 109.5(14) . . ? F6_14 C3_14 F5_14 108.3(15) . . ? F4_14 C3_14 C1_14 110.1(12) . . ? F6_14 C3_14 C1_14 111.8(12) . . ? F5_14 C3_14 C1_14 109.7(12) . . ? F7_14 C4_14 F9_14 109.5(15) . . ? F7_14 C4_14 F8_14 108.9(14) . . ? F9_14 C4_14 F8_14 107.3(14) . . ? F7_14 C4_14 C1_14 110.3(12) . . ? F9_14 C4_14 C1_14 109.6(12) . . ? F8_14 C4_14 C1_14 111.1(12) . . ? C1_15 O1_15 Al08 148.3(9) . . ? O1_15 C1_15 C3_15 110.1(9) . . ? O1_15 C1_15 C4_15 109.1(9) . . ? C3_15 C1_15 C4_15 111.6(9) . . ? O1_15 C1_15 C2_15 112.0(9) . . ? C3_15 C1_15 C2_15 107.2(9) . . ? C4_15 C1_15 C2_15 106.9(8) . . ? F3_15 C2_15 F1_15 113.1(13) . . ? F3_15 C2_15 F2_15 105.1(11) . . ? F1_15 C2_15 F2_15 110.6(11) . . ? F3_15 C2_15 C1_15 109.1(11) . . ? F1_15 C2_15 C1_15 109.7(10) . . ? F2_15 C2_15 C1_15 109.1(10) . . ? F5_15 C3_15 F4_15 112.4(12) . . ? F5_15 C3_15 F6_15 108.3(12) . . ? F4_15 C3_15 F6_15 107.2(11) . . ? F5_15 C3_15 C1_15 109.5(10) . . ? F4_15 C3_15 C1_15 108.6(10) . . ? F6_15 C3_15 C1_15 110.8(10) . . ? F7_15 C4_15 F8_15 107.2(10) . . ? F7_15 C4_15 F9_15 113.4(12) . . ? F8_15 C4_15 F9_15 107.2(11) . . ? F7_15 C4_15 C1_15 107.2(10) . . ? F8_15 C4_15 C1_15 111.7(9) . . ? F9_15 C4_15 C1_15 110.2(9) . . ? C1_16 O1_16 Al08 145.6(15) . . ? O1_16 C1_16 C3_16 106.9(12) . . ? O1_16 C1_16 C2_16 111.0(14) . . ? C3_16 C1_16 C2_16 115.2(13) . . ? O1_16 C1_16 C4_16 108.9(13) . . ? C3_16 C1_16 C4_16 109.4(12) . . ? C2_16 C1_16 C4_16 105.3(12) . . ? F3_16 C2_16 F2_16 107.5(16) . . ? F3_16 C2_16 F1_16 106.4(18) . . ? F2_16 C2_16 F1_16 115.5(18) . . ? F3_16 C2_16 C1_16 112.3(18) . . ? F2_16 C2_16 C1_16 111.8(16) . . ? F1_16 C2_16 C1_16 103.3(14) . . ? F6_16 C3_16 F5_16 120.4(19) . . ? F6_16 C3_16 F4_16 103.8(17) . . ? F5_16 C3_16 F4_16 111.0(18) . . ? F6_16 C3_16 C1_16 106.0(15) . . ? F5_16 C3_16 C1_16 108.8(15) . . ? F4_16 C3_16 C1_16 106.0(15) . . ? F7_16 C4_16 F8_16 112.5(18) . . ? F7_16 C4_16 F9_16 111.8(16) . . ? F8_16 C4_16 F9_16 109.2(16) . . ? F7_16 C4_16 C1_16 108.0(15) . . ? F8_16 C4_16 C1_16 107.6(14) . . ? F9_16 C4_16 C1_16 107.5(13) . . ? C1_17 O1_17 Al08 146.6(16) . . ? O1_17 C1_17 C4_17 108.4(13) . . ? O1_17 C1_17 C3_17 112.9(14) . . ? C4_17 C1_17 C3_17 110.1(12) . . ? O1_17 C1_17 C2_17 102.6(13) . . ? C4_17 C1_17 C2_17 110.9(13) . . ? C3_17 C1_17 C2_17 111.6(13) . . ? F2_17 C2_17 F3_17 110.8(18) . . ? F2_17 C2_17 F1_17 111.0(17) . . ? F3_17 C2_17 F1_17 111.9(19) . . ? F2_17 C2_17 C1_17 111.7(17) . . ? F3_17 C2_17 C1_17 106.3(17) . . ? F1_17 C2_17 C1_17 104.9(15) . . ? F6_17 C3_17 F4_17 107.7(16) . . ? F6_17 C3_17 F5_17 110.0(17) . . ? F4_17 C3_17 F5_17 109.8(16) . . ? F6_17 C3_17 C1_17 109.6(15) . . ? F4_17 C3_17 C1_17 110.1(14) . . ? F5_17 C3_17 C1_17 109.7(14) . . ? F8_17 C4_17 F9_17 109.7(17) . . ? F8_17 C4_17 F7_17 112.4(18) . . ? F9_17 C4_17 F7_17 109.4(18) . . ? F8_17 C4_17 C1_17 109.3(15) . . ? F9_17 C4_17 C1_17 108.3(15) . . ? F7_17 C4_17 C1_17 107.7(14) . . ? C1_18 O1_18 Al08 153.1(9) . . ? O1_18 C1_18 C3_18 110.1(9) . . ? O1_18 C1_18 C4_18 108.4(9) . . ? C3_18 C1_18 C4_18 108.0(9) . . ? O1_18 C1_18 C2_18 110.5(9) . . ? C3_18 C1_18 C2_18 110.9(9) . . ? C4_18 C1_18 C2_18 108.9(8) . . ? F3_18 C2_18 F2_18 108.7(11) . . ? F3_18 C2_18 F1_18 106.8(11) . . ? F2_18 C2_18 F1_18 108.3(11) . . ? F3_18 C2_18 C1_18 109.8(9) . . ? F2_18 C2_18 C1_18 112.4(10) . . ? F1_18 C2_18 C1_18 110.7(10) . . ? F4_18 C3_18 F5_18 111.3(14) . . ? F4_18 C3_18 F6_18 107.7(13) . . ? F5_18 C3_18 F6_18 107.0(14) . . ? F4_18 C3_18 C1_18 109.8(11) . . ? F5_18 C3_18 C1_18 110.3(12) . . ? F6_18 C3_18 C1_18 110.7(12) . . ? F9_18 C4_18 F8_18 108.1(10) . . ? F9_18 C4_18 F7_18 107.0(10) . . ? F8_18 C4_18 F7_18 107.4(9) . . ? F9_18 C4_18 C1_18 112.1(9) . . ? F8_18 C4_18 C1_18 111.0(9) . . ? F7_18 C4_18 C1_18 111.0(9) . . ? C1_19 O1_19 Al1 152.1(14) . . ? O1_19 C1_19 C3_19 108.7(12) . . ? O1_19 C1_19 C4_19 107.4(12) . . ? C3_19 C1_19 C4_19 110.3(11) . . ? O1_19 C1_19 C2_19 107.7(12) . . ? C3_19 C1_19 C2_19 111.6(11) . . ? C4_19 C1_19 C2_19 111.0(11) . . ? F2_19 C2_19 F1_19 107.5(16) . . ? F2_19 C2_19 F3_19 113.0(15) . . ? F1_19 C2_19 F3_19 106.8(16) . . ? F2_19 C2_19 C1_19 110.8(13) . . ? F1_19 C2_19 C1_19 109.3(15) . . ? F3_19 C2_19 C1_19 109.3(12) . . ? F5_19 C3_19 F6_19 106.2(14) . . ? F5_19 C3_19 F4_19 109.1(14) . . ? F6_19 C3_19 F4_19 107.4(14) . . ? F5_19 C3_19 C1_19 111.1(12) . . ? F6_19 C3_19 C1_19 111.5(13) . . ? F4_19 C3_19 C1_19 111.3(12) . . ? F8_19 C4_19 F9_19 109.8(15) . . ? F8_19 C4_19 F7_19 103.6(14) . . ? F9_19 C4_19 F7_19 107.5(15) . . ? F8_19 C4_19 C1_19 114.2(13) . . ? F9_19 C4_19 C1_19 110.8(13) . . ? F7_19 C4_19 C1_19 110.4(12) . . ? F1_21 C1_21 C2_21 120.0(16) . . ? F1_21 C1_21 C6_21 119.8(16) . . ? C2_21 C1_21 C6_21 120.2(14) . . ? F2_21 C2_21 C1_21 121.4(17) . . ? F2_21 C2_21 C3_21 119.5(17) . . ? C1_21 C2_21 C3_21 119.1(14) . . ? F3_21 C3_21 C4_21 119.8(16) . . ? F3_21 C3_21 C2_21 120.9(17) . . ? C4_21 C3_21 C2_21 119.3(14) . . ? F4_21 C4_21 C3_21 117.8(16) . . ? F4_21 C4_21 C5_21 120.0(16) . . ? C3_21 C4_21 C5_21 122.2(14) . . ? C6_21 C5_21 C4_21 117.9(16) . . ? C6_21 C5_21 H5_21 121.0 . . ? C4_21 C5_21 H5_21 121.0 . . ? C5_21 C6_21 C1_21 121.2(16) . . ? C5_21 C6_21 H6_21 119.4 . . ? C1_21 C6_21 H6_21 119.4 . . ? C1_10 O1_10 Al2 152.7(12) . . ? O1_10 C1_10 C3_10 110.5(10) . . ? O1_10 C1_10 C2_10 112.7(11) . . ? C3_10 C1_10 C2_10 110.3(10) . . ? O1_10 C1_10 C4_10 107.8(11) . . ? C3_10 C1_10 C4_10 109.2(10) . . ? C2_10 C1_10 C4_10 106.3(10) . . ? F3_10 C2_10 F1_10 112.8(14) . . ? F3_10 C2_10 F2_10 108.1(14) . . ? F1_10 C2_10 F2_10 106.5(13) . . ? F3_10 C2_10 C1_10 107.6(11) . . ? F1_10 C2_10 C1_10 112.1(12) . . ? F2_10 C2_10 C1_10 109.7(12) . . ? F6_10 C3_10 F5_10 105.8(14) . . ? F6_10 C3_10 F4_10 107.1(14) . . ? F5_10 C3_10 F4_10 112.7(14) . . ? F6_10 C3_10 C1_10 112.3(12) . . ? F5_10 C3_10 C1_10 110.0(12) . . ? F4_10 C3_10 C1_10 109.0(11) . . ? F8_10 C4_10 F7_10 107.6(13) . . ? F8_10 C4_10 F9_10 111.8(13) . . ? F7_10 C4_10 F9_10 115.2(13) . . ? F8_10 C4_10 C1_10 105.6(12) . . ? F7_10 C4_10 C1_10 107.9(11) . . ? F9_10 C4_10 C1_10 108.2(11) . . ? O1_20 C1_20 C4_20 110.6(18) . . ? O1_20 C1_20 C2_20 108.8(17) . . ? C4_20 C1_20 C2_20 109.7(14) . . ? O1_20 C1_20 C3_20 108.5(18) . . ? C4_20 C1_20 C3_20 109.5(14) . . ? C2_20 C1_20 C3_20 109.7(14) . . ? F2_20 C2_20 F3_20 109(2) . . ? F2_20 C2_20 F1_20 110(2) . . ? F3_20 C2_20 F1_20 108.5(19) . . ? F2_20 C2_20 C1_20 110.8(17) . . ? F3_20 C2_20 C1_20 109.2(18) . . ? F1_20 C2_20 C1_20 109.2(17) . . ? F6_20 C3_20 F5_20 111(2) . . ? F6_20 C3_20 F4_20 108(2) . . ? F5_20 C3_20 F4_20 110.6(19) . . ? F6_20 C3_20 C1_20 111.2(19) . . ? F5_20 C3_20 C1_20 106.6(16) . . ? F4_20 C3_20 C1_20 108.9(17) . . ? F7_20 C4_20 F9_20 109(2) . . ? F7_20 C4_20 F8_20 110(2) . . ? F9_20 C4_20 F8_20 108.2(19) . . ? F7_20 C4_20 C1_20 110.3(18) . . ? F9_20 C4_20 C1_20 109.9(18) . . ? F8_20 C4_20 C1_20 109.7(17) . . ? F1_22 C1_22 C6_22 121.2(8) . . ? F1_22 C1_22 C2_22 118.4(8) . . ? C6_22 C1_22 C2_22 120.4(9) . . ? F2_22 C2_22 C3_22 121.0(8) . . ? F2_22 C2_22 C1_22 120.2(9) . . ? C3_22 C2_22 C1_22 118.8(9) . . ? F3_22 C3_22 C4_22 120.1(9) . . ? F3_22 C3_22 C2_22 118.8(9) . . ? C4_22 C3_22 C2_22 121.1(8) . . ? F4_22 C4_22 C3_22 119.5(9) . . ? F4_22 C4_22 C5_22 120.5(10) . . ? C3_22 C4_22 C5_22 120.0(9) . . ? C4_22 C5_22 C6_22 119.1(10) . . ? C4_22 C5_22 H5_22 120.4 . . ? C6_22 C5_22 H5_22 120.4 . . ? C1_22 C6_22 C5_22 120.6(9) . . ? C1_22 C6_22 H6_22 119.7 . . ? C5_22 C6_22 H6_22 119.7 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_9 Al08 F1 Al1 -92(17) . . . . ? O1_18 Al08 F1 Al1 145(17) . . . . ? O1_15 Al08 F1 Al1 25(17) . . . . ? O1_19 Al1 F1 Al08 21(18) . . . . ? O1_7 Al1 F1 Al08 145(17) . . . . ? O1_12 Al1 F1 Al08 -96(17) . . . . ? O1_19 Al1 O1_7 C1_7 -108(3) . . . . ? O1_12 Al1 O1_7 C1_7 26(3) . . . . ? F1 Al1 O1_7 C1_7 139(3) . . . . ? Al1 O1_7 C1_7 C3_7 122(2) . . . . ? Al1 O1_7 C1_7 C2_7 3(3) . . . . ? Al1 O1_7 C1_7 C4_7 -117(2) . . . . ? O1_7 C1_7 C2_7 F1_7 -73.8(13) . . . . ? C3_7 C1_7 C2_7 F1_7 166.8(11) . . . . ? C4_7 C1_7 C2_7 F1_7 46.8(13) . . . . ? O1_7 C1_7 C2_7 F2_7 167.5(13) . . . . ? C3_7 C1_7 C2_7 F2_7 48.2(15) . . . . ? C4_7 C1_7 C2_7 F2_7 -71.9(14) . . . . ? O1_7 C1_7 C2_7 F3_7 47.9(14) . . . . ? C3_7 C1_7 C2_7 F3_7 -71.5(13) . . . . ? C4_7 C1_7 C2_7 F3_7 168.5(11) . . . . ? O1_7 C1_7 C3_7 F5_7 -72.4(14) . . . . ? C2_7 C1_7 C3_7 F5_7 46.1(14) . . . . ? C4_7 C1_7 C3_7 F5_7 166.3(11) . . . . ? O1_7 C1_7 C3_7 F6_7 167.3(13) . . . . ? C2_7 C1_7 C3_7 F6_7 -74.3(14) . . . . ? C4_7 C1_7 C3_7 F6_7 45.9(15) . . . . ? O1_7 C1_7 C3_7 F4_7 48.0(15) . . . . ? C2_7 C1_7 C3_7 F4_7 166.4(12) . . . . ? C4_7 C1_7 C3_7 F4_7 -73.4(14) . . . . ? O1_7 C1_7 C4_7 F7_7 -75.2(15) . . . . ? C3_7 C1_7 C4_7 F7_7 45.4(14) . . . . ? C2_7 C1_7 C4_7 F7_7 165.9(12) . . . . ? O1_7 C1_7 C4_7 F8_7 166.4(14) . . . . ? C3_7 C1_7 C4_7 F8_7 -73.0(15) . . . . ? C2_7 C1_7 C4_7 F8_7 47.5(16) . . . . ? O1_7 C1_7 C4_7 F9_7 46.1(16) . . . . ? C3_7 C1_7 C4_7 F9_7 166.7(14) . . . . ? C2_7 C1_7 C4_7 F9_7 -72.8(15) . . . . ? O1_10 Al2 O1_8 C1_8 51(3) . . . . ? O1_13 Al2 O1_8 C1_8 -178(2) . . . . ? F1B Al2 O1_8 C1_8 -65(3) . . . . ? Al2 O1_8 C1_8 C2_8 102(3) . . . . ? Al2 O1_8 C1_8 C4_8 -19(3) . . . . ? Al2 O1_8 C1_8 C3_8 -139(2) . . . . ? O1_8 C1_8 C2_8 F3_8 44.5(17) . . . . ? C4_8 C1_8 C2_8 F3_8 166.1(15) . . . . ? C3_8 C1_8 C2_8 F3_8 -72.8(17) . . . . ? O1_8 C1_8 C2_8 F2_8 161.0(16) . . . . ? C4_8 C1_8 C2_8 F2_8 -77.4(18) . . . . ? C3_8 C1_8 C2_8 F2_8 43.6(18) . . . . ? O1_8 C1_8 C2_8 F1_8 -78.8(16) . . . . ? C4_8 C1_8 C2_8 F1_8 42.8(16) . . . . ? C3_8 C1_8 C2_8 F1_8 163.9(14) . . . . ? O1_8 C1_8 C3_8 F4_8 45.1(15) . . . . ? C2_8 C1_8 C3_8 F4_8 162.8(12) . . . . ? C4_8 C1_8 C3_8 F4_8 -75.9(14) . . . . ? O1_8 C1_8 C3_8 F6_8 160.9(14) . . . . ? C2_8 C1_8 C3_8 F6_8 -81.4(15) . . . . ? C4_8 C1_8 C3_8 F6_8 39.9(15) . . . . ? O1_8 C1_8 C3_8 F5_8 -77.7(15) . . . . ? C2_8 C1_8 C3_8 F5_8 40.0(15) . . . . ? C4_8 C1_8 C3_8 F5_8 161.3(13) . . . . ? O1_8 C1_8 C4_8 F9_8 39.8(15) . . . . ? C2_8 C1_8 C4_8 F9_8 -79.9(14) . . . . ? C3_8 C1_8 C4_8 F9_8 158.5(12) . . . . ? O1_8 C1_8 C4_8 F7_8 -80.1(14) . . . . ? C2_8 C1_8 C4_8 F7_8 160.2(12) . . . . ? C3_8 C1_8 C4_8 F7_8 38.5(15) . . . . ? O1_8 C1_8 C4_8 F8_8 154.4(13) . . . . ? C2_8 C1_8 C4_8 F8_8 34.8(15) . . . . ? C3_8 C1_8 C4_8 F8_8 -86.9(14) . . . . ? O1_18 Al08 O1_9 C1_9 24.2(16) . . . . ? O1_15 Al08 O1_9 C1_9 152.7(14) . . . . ? F1 Al08 O1_9 C1_9 -95(2) . . . . ? Al08 O1_9 C1_9 C2_9 67.8(16) . . . . ? Al08 O1_9 C1_9 C4_9 -173.4(12) . . . . ? Al08 O1_9 C1_9 C3_9 -53.4(17) . . . . ? O1_9 C1_9 C2_9 F2_9 -163.8(10) . . . . ? C4_9 C1_9 C2_9 F2_9 78.7(11) . . . . ? C3_9 C1_9 C2_9 F2_9 -41.6(12) . . . . ? O1_9 C1_9 C2_9 F3_9 -44.0(12) . . . . ? C4_9 C1_9 C2_9 F3_9 -161.5(9) . . . . ? C3_9 C1_9 C2_9 F3_9 78.2(10) . . . . ? O1_9 C1_9 C2_9 F1_9 73.5(13) . . . . ? C4_9 C1_9 C2_9 F1_9 -44.0(13) . . . . ? C3_9 C1_9 C2_9 F1_9 -164.3(10) . . . . ? O1_9 C1_9 C3_9 F4_9 -40.7(12) . . . . ? C2_9 C1_9 C3_9 F4_9 -163.4(9) . . . . ? C4_9 C1_9 C3_9 F4_9 77.2(11) . . . . ? O1_9 C1_9 C3_9 F6_9 -158.9(10) . . . . ? C2_9 C1_9 C3_9 F6_9 78.4(11) . . . . ? C4_9 C1_9 C3_9 F6_9 -41.0(12) . . . . ? O1_9 C1_9 C3_9 F5_9 80.5(11) . . . . ? C2_9 C1_9 C3_9 F5_9 -42.2(11) . . . . ? C4_9 C1_9 C3_9 F5_9 -161.6(9) . . . . ? O1_9 C1_9 C4_9 F9_9 -41.6(12) . . . . ? C2_9 C1_9 C4_9 F9_9 78.8(11) . . . . ? C3_9 C1_9 C4_9 F9_9 -161.8(9) . . . . ? O1_9 C1_9 C4_9 F8_9 -163.3(10) . . . . ? C2_9 C1_9 C4_9 F8_9 -42.9(12) . . . . ? C3_9 C1_9 C4_9 F8_9 76.6(11) . . . . ? O1_9 C1_9 C4_9 F7_9 76.5(12) . . . . ? C2_9 C1_9 C4_9 F7_9 -163.1(10) . . . . ? C3_9 C1_9 C4_9 F7_9 -43.6(12) . . . . ? O1_19 Al1 O1_12 C1_12 1(2) . . . . ? O1_7 Al1 O1_12 C1_12 -137(2) . . . . ? F1 Al1 O1_12 C1_12 113(2) . . . . ? Al1 O1_12 C1_12 C2_12 152.5(19) . . . . ? Al1 O1_12 C1_12 C3_12 -88(2) . . . . ? Al1 O1_12 C1_12 C4_12 33(2) . . . . ? O1_12 C1_12 C2_12 F2_12 161.7(11) . . . . ? C3_12 C1_12 C2_12 F2_12 42.9(14) . . . . ? C4_12 C1_12 C2_12 F2_12 -78.0(13) . . . . ? O1_12 C1_12 C2_12 F3_12 42.2(13) . . . . ? C3_12 C1_12 C2_12 F3_12 -76.6(13) . . . . ? C4_12 C1_12 C2_12 F3_12 162.5(10) . . . . ? O1_12 C1_12 C2_12 F1_12 -77.2(13) . . . . ? C3_12 C1_12 C2_12 F1_12 164.0(11) . . . . ? C4_12 C1_12 C2_12 F1_12 43.0(13) . . . . ? O1_12 C1_12 C3_12 F6_12 159.9(12) . . . . ? C2_12 C1_12 C3_12 F6_12 -81.9(13) . . . . ? C4_12 C1_12 C3_12 F6_12 38.5(14) . . . . ? O1_12 C1_12 C3_12 F4_12 38.0(14) . . . . ? C2_12 C1_12 C3_12 F4_12 156.3(11) . . . . ? C4_12 C1_12 C3_12 F4_12 -83.4(13) . . . . ? O1_12 C1_12 C3_12 F5_12 -82.1(14) . . . . ? C2_12 C1_12 C3_12 F5_12 36.2(14) . . . . ? C4_12 C1_12 C3_12 F5_12 156.6(12) . . . . ? O1_12 C1_12 C4_12 F8_12 158.6(12) . . . . ? C2_12 C1_12 C4_12 F8_12 39.7(14) . . . . ? C3_12 C1_12 C4_12 F8_12 -80.9(13) . . . . ? O1_12 C1_12 C4_12 F9_12 40.3(16) . . . . ? C2_12 C1_12 C4_12 F9_12 -78.5(15) . . . . ? C3_12 C1_12 C4_12 F9_12 160.9(14) . . . . ? O1_12 C1_12 C4_12 F7_12 -79.9(13) . . . . ? C2_12 C1_12 C4_12 F7_12 161.2(10) . . . . ? C3_12 C1_12 C4_12 F7_12 40.7(13) . . . . ? O1_10 Al2 O1_13 C1_13 137(2) . . . . ? O1_8 Al2 O1_13 C1_13 5(3) . . . . ? F1B Al2 O1_13 C1_13 -112(3) . . . . ? Al2 O1_13 C1_13 C4_13 -164.7(19) . . . . ? Al2 O1_13 C1_13 C3_13 76(2) . . . . ? Al2 O1_13 C1_13 C2_13 -42(3) . . . . ? O1_13 C1_13 C2_13 F2_13 -156.6(13) . . . . ? C4_13 C1_13 C2_13 F2_13 -35.8(15) . . . . ? C3_13 C1_13 C2_13 F2_13 84.9(14) . . . . ? O1_13 C1_13 C2_13 F3_13 80.6(13) . . . . ? C4_13 C1_13 C2_13 F3_13 -158.6(11) . . . . ? C3_13 C1_13 C2_13 F3_13 -37.9(14) . . . . ? O1_13 C1_13 C2_13 F1_13 -41.0(18) . . . . ? C4_13 C1_13 C2_13 F1_13 79.8(16) . . . . ? C3_13 C1_13 C2_13 F1_13 -159.5(16) . . . . ? O1_13 C1_13 C3_13 F5_13 -42.9(15) . . . . ? C4_13 C1_13 C3_13 F5_13 -161.4(12) . . . . ? C2_13 C1_13 C3_13 F5_13 77.0(14) . . . . ? O1_13 C1_13 C3_13 F6_13 -162.8(12) . . . . ? C4_13 C1_13 C3_13 F6_13 78.7(14) . . . . ? C2_13 C1_13 C3_13 F6_13 -42.8(14) . . . . ? O1_13 C1_13 C3_13 F4_13 76.1(17) . . . . ? C4_13 C1_13 C3_13 F4_13 -42.4(17) . . . . ? C2_13 C1_13 C3_13 F4_13 -163.9(15) . . . . ? O1_13 C1_13 C4_13 F7_13 -41.2(14) . . . . ? C3_13 C1_13 C4_13 F7_13 77.2(13) . . . . ? C2_13 C1_13 C4_13 F7_13 -163.1(11) . . . . ? O1_13 C1_13 C4_13 F8_13 -161.2(11) . . . . ? C3_13 C1_13 C4_13 F8_13 -42.8(14) . . . . ? C2_13 C1_13 C4_13 F8_13 76.9(13) . . . . ? O1_13 C1_13 C4_13 F9_13 79.2(13) . . . . ? C3_13 C1_13 C4_13 F9_13 -162.5(11) . . . . ? C2_13 C1_13 C4_13 F9_13 -42.8(13) . . . . ? O1_16 Al08 O1_14 C1_14 -5(3) . . . . ? O1_17 Al08 O1_14 C1_14 -148(3) . . . . ? F1B Al08 O1_14 C1_14 107(3) . . . . ? Al08 O1_14 C1_14 C2_14 -85(3) . . . . ? Al08 O1_14 C1_14 C3_14 34(3) . . . . ? Al08 O1_14 C1_14 C4_14 156(2) . . . . ? O1_14 C1_14 C2_14 F3_14 39.7(17) . . . . ? C3_14 C1_14 C2_14 F3_14 -80.9(15) . . . . ? C4_14 C1_14 C2_14 F3_14 160.5(14) . . . . ? O1_14 C1_14 C2_14 F2_14 158.7(15) . . . . ? C3_14 C1_14 C2_14 F2_14 38.1(16) . . . . ? C4_14 C1_14 C2_14 F2_14 -80.5(16) . . . . ? O1_14 C1_14 C2_14 F1_14 -81.7(17) . . . . ? C3_14 C1_14 C2_14 F1_14 157.7(15) . . . . ? C4_14 C1_14 C2_14 F1_14 39.1(17) . . . . ? O1_14 C1_14 C3_14 F4_14 41.7(17) . . . . ? C2_14 C1_14 C3_14 F4_14 161.7(13) . . . . ? C4_14 C1_14 C3_14 F4_14 -80.7(15) . . . . ? O1_14 C1_14 C3_14 F6_14 160.9(15) . . . . ? C2_14 C1_14 C3_14 F6_14 -79.1(16) . . . . ? C4_14 C1_14 C3_14 F6_14 38.5(17) . . . . ? O1_14 C1_14 C3_14 F5_14 -78.9(16) . . . . ? C2_14 C1_14 C3_14 F5_14 41.1(16) . . . . ? C4_14 C1_14 C3_14 F5_14 158.7(13) . . . . ? O1_14 C1_14 C4_14 F7_14 -76.9(17) . . . . ? C2_14 C1_14 C4_14 F7_14 163.3(14) . . . . ? C3_14 C1_14 C4_14 F7_14 45.2(17) . . . . ? O1_14 C1_14 C4_14 F9_14 43.8(17) . . . . ? C2_14 C1_14 C4_14 F9_14 -76.1(15) . . . . ? C3_14 C1_14 C4_14 F9_14 165.8(14) . . . . ? O1_14 C1_14 C4_14 F8_14 162.3(14) . . . . ? C2_14 C1_14 C4_14 F8_14 42.4(15) . . . . ? C3_14 C1_14 C4_14 F8_14 -75.7(15) . . . . ? O1_9 Al08 O1_15 C1_15 -38.9(17) . . . . ? O1_18 Al08 O1_15 C1_15 89.7(17) . . . . ? F1 Al08 O1_15 C1_15 -155(2) . . . . ? Al08 O1_15 C1_15 C3_15 49(2) . . . . ? Al08 O1_15 C1_15 C4_15 171.6(13) . . . . ? Al08 O1_15 C1_15 C2_15 -70.3(18) . . . . ? O1_15 C1_15 C2_15 F3_15 50.9(14) . . . . ? C3_15 C1_15 C2_15 F3_15 -70.0(13) . . . . ? C4_15 C1_15 C2_15 F3_15 170.2(11) . . . . ? O1_15 C1_15 C2_15 F1_15 -73.5(12) . . . . ? C3_15 C1_15 C2_15 F1_15 165.6(10) . . . . ? C4_15 C1_15 C2_15 F1_15 45.8(12) . . . . ? O1_15 C1_15 C2_15 F2_15 165.1(11) . . . . ? C3_15 C1_15 C2_15 F2_15 44.2(12) . . . . ? C4_15 C1_15 C2_15 F2_15 -75.5(12) . . . . ? O1_15 C1_15 C3_15 F5_15 -79.7(12) . . . . ? C4_15 C1_15 C3_15 F5_15 159.0(10) . . . . ? C2_15 C1_15 C3_15 F5_15 42.3(12) . . . . ? O1_15 C1_15 C3_15 F4_15 43.4(13) . . . . ? C4_15 C1_15 C3_15 F4_15 -77.9(12) . . . . ? C2_15 C1_15 C3_15 F4_15 165.4(10) . . . . ? O1_15 C1_15 C3_15 F6_15 160.9(12) . . . . ? C4_15 C1_15 C3_15 F6_15 39.6(15) . . . . ? C2_15 C1_15 C3_15 F6_15 -77.1(13) . . . . ? O1_15 C1_15 C4_15 F7_15 -76.9(12) . . . . ? C3_15 C1_15 C4_15 F7_15 45.0(13) . . . . ? C2_15 C1_15 C4_15 F7_15 161.9(10) . . . . ? O1_15 C1_15 C4_15 F8_15 165.9(10) . . . . ? C3_15 C1_15 C4_15 F8_15 -72.2(12) . . . . ? C2_15 C1_15 C4_15 F8_15 44.7(12) . . . . ? O1_15 C1_15 C4_15 F9_15 46.9(13) . . . . ? C3_15 C1_15 C4_15 F9_15 168.8(10) . . . . ? C2_15 C1_15 C4_15 F9_15 -74.3(12) . . . . ? O1_17 Al08 O1_16 C1_16 -11(3) . . . . ? O1_14 Al08 O1_16 C1_16 -148(3) . . . . ? F1B Al08 O1_16 C1_16 101(3) . . . . ? Al08 O1_16 C1_16 C3_16 175(2) . . . . ? Al08 O1_16 C1_16 C2_16 49(3) . . . . ? Al08 O1_16 C1_16 C4_16 -67(3) . . . . ? O1_16 C1_16 C2_16 F3_16 21(2) . . . . ? C3_16 C1_16 C2_16 F3_16 -100(2) . . . . ? C4_16 C1_16 C2_16 F3_16 139.2(18) . . . . ? O1_16 C1_16 C2_16 F2_16 142.4(19) . . . . ? C3_16 C1_16 C2_16 F2_16 21(2) . . . . ? C4_16 C1_16 C2_16 F2_16 -99.9(18) . . . . ? O1_16 C1_16 C2_16 F1_16 -92.8(19) . . . . ? C3_16 C1_16 C2_16 F1_16 145.6(18) . . . . ? C4_16 C1_16 C2_16 F1_16 25.0(18) . . . . ? O1_16 C1_16 C3_16 F6_16 147.8(19) . . . . ? C2_16 C1_16 C3_16 F6_16 -88(2) . . . . ? C4_16 C1_16 C3_16 F6_16 30(2) . . . . ? O1_16 C1_16 C3_16 F5_16 -81.5(19) . . . . ? C2_16 C1_16 C3_16 F5_16 42(2) . . . . ? C4_16 C1_16 C3_16 F5_16 160.8(16) . . . . ? O1_16 C1_16 C3_16 F4_16 38(2) . . . . ? C2_16 C1_16 C3_16 F4_16 161.7(19) . . . . ? C4_16 C1_16 C3_16 F4_16 -80(2) . . . . ? O1_16 C1_16 C4_16 F7_16 -75.3(19) . . . . ? C3_16 C1_16 C4_16 F7_16 41.2(19) . . . . ? C2_16 C1_16 C4_16 F7_16 165.5(17) . . . . ? O1_16 C1_16 C4_16 F8_16 163.0(18) . . . . ? C3_16 C1_16 C4_16 F8_16 -80.5(19) . . . . ? C2_16 C1_16 C4_16 F8_16 43.8(19) . . . . ? O1_16 C1_16 C4_16 F9_16 45.5(18) . . . . ? C3_16 C1_16 C4_16 F9_16 162.0(16) . . . . ? C2_16 C1_16 C4_16 F9_16 -73.7(16) . . . . ? O1_16 Al08 O1_17 C1_17 -104(3) . . . . ? O1_14 Al08 O1_17 C1_17 32(4) . . . . ? F1B Al08 O1_17 C1_17 140(4) . . . . ? Al08 O1_17 C1_17 C4_17 124(3) . . . . ? Al08 O1_17 C1_17 C3_17 2(4) . . . . ? Al08 O1_17 C1_17 C2_17 -119(3) . . . . ? O1_17 C1_17 C2_17 F2_17 -150(2) . . . . ? C4_17 C1_17 C2_17 F2_17 -34(2) . . . . ? C3_17 C1_17 C2_17 F2_17 88.9(19) . . . . ? O1_17 C1_17 C2_17 F3_17 89(2) . . . . ? C4_17 C1_17 C2_17 F3_17 -155.3(18) . . . . ? C3_17 C1_17 C2_17 F3_17 -32(2) . . . . ? O1_17 C1_17 C2_17 F1_17 -29.5(19) . . . . ? C4_17 C1_17 C2_17 F1_17 86.0(18) . . . . ? C3_17 C1_17 C2_17 F1_17 -150.8(16) . . . . ? O1_17 C1_17 C3_17 F6_17 161.6(19) . . . . ? C4_17 C1_17 C3_17 F6_17 40(2) . . . . ? C2_17 C1_17 C3_17 F6_17 -83.4(19) . . . . ? O1_17 C1_17 C3_17 F4_17 43(2) . . . . ? C4_17 C1_17 C3_17 F4_17 -78.0(18) . . . . ? C2_17 C1_17 C3_17 F4_17 158.4(16) . . . . ? O1_17 C1_17 C3_17 F5_17 -78(2) . . . . ? C4_17 C1_17 C3_17 F5_17 161.1(16) . . . . ? C2_17 C1_17 C3_17 F5_17 37.4(19) . . . . ? O1_17 C1_17 C4_17 F8_17 158.3(19) . . . . ? C3_17 C1_17 C4_17 F8_17 -77.7(19) . . . . ? C2_17 C1_17 C4_17 F8_17 46(2) . . . . ? O1_17 C1_17 C4_17 F9_17 39(2) . . . . ? C3_17 C1_17 C4_17 F9_17 162.8(18) . . . . ? C2_17 C1_17 C4_17 F9_17 -73(2) . . . . ? O1_17 C1_17 C4_17 F7_17 -79(2) . . . . ? C3_17 C1_17 C4_17 F7_17 45(2) . . . . ? C2_17 C1_17 C4_17 F7_17 168.7(18) . . . . ? O1_9 Al08 O1_18 C1_18 -168.2(18) . . . . ? O1_15 Al08 O1_18 C1_18 65(2) . . . . ? F1 Al08 O1_18 C1_18 -48(3) . . . . ? Al08 O1_18 C1_18 C3_18 80(2) . . . . ? Al08 O1_18 C1_18 C4_18 -162.5(16) . . . . ? Al08 O1_18 C1_18 C2_18 -43(2) . . . . ? O1_18 C1_18 C2_18 F3_18 38.4(14) . . . . ? C3_18 C1_18 C2_18 F3_18 -83.9(13) . . . . ? C4_18 C1_18 C2_18 F3_18 157.4(11) . . . . ? O1_18 C1_18 C2_18 F2_18 159.5(11) . . . . ? C3_18 C1_18 C2_18 F2_18 37.2(14) . . . . ? C4_18 C1_18 C2_18 F2_18 -81.5(13) . . . . ? O1_18 C1_18 C2_18 F1_18 -79.3(12) . . . . ? C3_18 C1_18 C2_18 F1_18 158.4(10) . . . . ? C4_18 C1_18 C2_18 F1_18 39.7(13) . . . . ? O1_18 C1_18 C3_18 F4_18 29.8(15) . . . . ? C4_18 C1_18 C3_18 F4_18 -88.4(13) . . . . ? C2_18 C1_18 C3_18 F4_18 152.3(12) . . . . ? O1_18 C1_18 C3_18 F5_18 -93.2(15) . . . . ? C4_18 C1_18 C3_18 F5_18 148.6(13) . . . . ? C2_18 C1_18 C3_18 F5_18 29.3(16) . . . . ? O1_18 C1_18 C3_18 F6_18 148.5(13) . . . . ? C4_18 C1_18 C3_18 F6_18 30.3(15) . . . . ? C2_18 C1_18 C3_18 F6_18 -88.9(14) . . . . ? O1_18 C1_18 C4_18 F9_18 42.7(12) . . . . ? C3_18 C1_18 C4_18 F9_18 161.9(10) . . . . ? C2_18 C1_18 C4_18 F9_18 -77.6(11) . . . . ? O1_18 C1_18 C4_18 F8_18 163.7(10) . . . . ? C3_18 C1_18 C4_18 F8_18 -77.1(11) . . . . ? C2_18 C1_18 C4_18 F8_18 43.4(12) . . . . ? O1_18 C1_18 C4_18 F7_18 -77.0(11) . . . . ? C3_18 C1_18 C4_18 F7_18 42.3(12) . . . . ? C2_18 C1_18 C4_18 F7_18 162.7(9) . . . . ? O1_7 Al1 O1_19 C1_19 -8(4) . . . . ? O1_12 Al1 O1_19 C1_19 -144(3) . . . . ? F1 Al1 O1_19 C1_19 103(4) . . . . ? Al1 O1_19 C1_19 C3_19 -35(4) . . . . ? Al1 O1_19 C1_19 C4_19 84(3) . . . . ? Al1 O1_19 C1_19 C2_19 -156(3) . . . . ? O1_19 C1_19 C2_19 F2_19 -158.6(16) . . . . ? C3_19 C1_19 C2_19 F2_19 82.2(16) . . . . ? C4_19 C1_19 C2_19 F2_19 -41.3(17) . . . . ? O1_19 C1_19 C2_19 F1_19 -40.3(19) . . . . ? C3_19 C1_19 C2_19 F1_19 -159.5(17) . . . . ? C4_19 C1_19 C2_19 F1_19 77.0(18) . . . . ? O1_19 C1_19 C2_19 F3_19 76.3(16) . . . . ? C3_19 C1_19 C2_19 F3_19 -42.9(17) . . . . ? C4_19 C1_19 C2_19 F3_19 -166.4(13) . . . . ? O1_19 C1_19 C3_19 F5_19 -42.6(17) . . . . ? C4_19 C1_19 C3_19 F5_19 -160.0(14) . . . . ? C2_19 C1_19 C3_19 F5_19 76.1(16) . . . . ? O1_19 C1_19 C3_19 F6_19 -160.8(15) . . . . ? C4_19 C1_19 C3_19 F6_19 81.7(16) . . . . ? C2_19 C1_19 C3_19 F6_19 -42.2(17) . . . . ? O1_19 C1_19 C3_19 F4_19 79.2(16) . . . . ? C4_19 C1_19 C3_19 F4_19 -38.2(17) . . . . ? C2_19 C1_19 C3_19 F4_19 -162.1(14) . . . . ? O1_19 C1_19 C4_19 F8_19 -159.4(16) . . . . ? C3_19 C1_19 C4_19 F8_19 -41.2(18) . . . . ? C2_19 C1_19 C4_19 F8_19 83.1(17) . . . . ? O1_19 C1_19 C4_19 F9_19 75.9(18) . . . . ? C3_19 C1_19 C4_19 F9_19 -165.8(16) . . . . ? C2_19 C1_19 C4_19 F9_19 -41.6(18) . . . . ? O1_19 C1_19 C4_19 F7_19 -43.1(16) . . . . ? C3_19 C1_19 C4_19 F7_19 75.1(15) . . . . ? C2_19 C1_19 C4_19 F7_19 -160.6(13) . . . . ? F1_21 C1_21 C2_21 F2_21 0(2) . . . . ? C6_21 C1_21 C2_21 F2_21 -178.9(13) . . . . ? F1_21 C1_21 C2_21 C3_21 179.1(13) . . . . ? C6_21 C1_21 C2_21 C3_21 1(2) . . . . ? F2_21 C2_21 C3_21 F3_21 -1(2) . . . . ? C1_21 C2_21 C3_21 F3_21 179.8(13) . . . . ? F2_21 C2_21 C3_21 C4_21 179.7(13) . . . . ? C1_21 C2_21 C3_21 C4_21 0(2) . . . . ? F3_21 C3_21 C4_21 F4_21 1(2) . . . . ? C2_21 C3_21 C4_21 F4_21 -179.7(15) . . . . ? F3_21 C3_21 C4_21 C5_21 -179.8(13) . . . . ? C2_21 C3_21 C4_21 C5_21 0(2) . . . . ? F4_21 C4_21 C5_21 C6_21 178.9(15) . . . . ? C3_21 C4_21 C5_21 C6_21 -1(2) . . . . ? C4_21 C5_21 C6_21 C1_21 1(2) . . . . ? F1_21 C1_21 C6_21 C5_21 -180.0(13) . . . . ? C2_21 C1_21 C6_21 C5_21 -1(2) . . . . ? O1_13 Al2 O1_10 C1_10 -37(3) . . . . ? O1_8 Al2 O1_10 C1_10 91(3) . . . . ? F1B Al2 O1_10 C1_10 -149(3) . . . . ? Al2 O1_10 C1_10 C3_10 34(3) . . . . ? Al2 O1_10 C1_10 C2_10 158(2) . . . . ? Al2 O1_10 C1_10 C4_10 -85(3) . . . . ? O1_10 C1_10 C2_10 F3_10 -83.8(16) . . . . ? C3_10 C1_10 C2_10 F3_10 40.1(16) . . . . ? C4_10 C1_10 C2_10 F3_10 158.3(13) . . . . ? O1_10 C1_10 C2_10 F1_10 40.7(17) . . . . ? C3_10 C1_10 C2_10 F1_10 164.7(14) . . . . ? C4_10 C1_10 C2_10 F1_10 -77.1(15) . . . . ? O1_10 C1_10 C2_10 F2_10 158.8(13) . . . . ? C3_10 C1_10 C2_10 F2_10 -77.3(14) . . . . ? C4_10 C1_10 C2_10 F2_10 40.9(14) . . . . ? O1_10 C1_10 C3_10 F6_10 167.0(13) . . . . ? C2_10 C1_10 C3_10 F6_10 41.8(16) . . . . ? C4_10 C1_10 C3_10 F6_10 -74.6(14) . . . . ? O1_10 C1_10 C3_10 F5_10 49.5(17) . . . . ? C2_10 C1_10 C3_10 F5_10 -75.7(16) . . . . ? C4_10 C1_10 C3_10 F5_10 167.9(14) . . . . ? O1_10 C1_10 C3_10 F4_10 -74.5(16) . . . . ? C2_10 C1_10 C3_10 F4_10 160.3(13) . . . . ? C4_10 C1_10 C3_10 F4_10 43.9(15) . . . . ? O1_10 C1_10 C4_10 F8_10 163.3(13) . . . . ? C3_10 C1_10 C4_10 F8_10 43.3(14) . . . . ? C2_10 C1_10 C4_10 F8_10 -75.7(14) . . . . ? O1_10 C1_10 C4_10 F7_10 48.4(14) . . . . ? C3_10 C1_10 C4_10 F7_10 -71.6(14) . . . . ? C2_10 C1_10 C4_10 F7_10 169.4(12) . . . . ? O1_10 C1_10 C4_10 F9_10 -76.8(14) . . . . ? C3_10 C1_10 C4_10 F9_10 163.1(12) . . . . ? C2_10 C1_10 C4_10 F9_10 44.2(14) . . . . ? O1_20 C1_20 C2_20 F2_20 164(3) . . . . ? C4_20 C1_20 C2_20 F2_20 -75(2) . . . . ? C3_20 C1_20 C2_20 F2_20 46(2) . . . . ? O1_20 C1_20 C2_20 F3_20 44(3) . . . . ? C4_20 C1_20 C2_20 F3_20 165(2) . . . . ? C3_20 C1_20 C2_20 F3_20 -75(2) . . . . ? O1_20 C1_20 C2_20 F1_20 -75(3) . . . . ? C4_20 C1_20 C2_20 F1_20 46(2) . . . . ? C3_20 C1_20 C2_20 F1_20 166(2) . . . . ? O1_20 C1_20 C3_20 F6_20 164(3) . . . . ? C4_20 C1_20 C3_20 F6_20 43(3) . . . . ? C2_20 C1_20 C3_20 F6_20 -78(3) . . . . ? O1_20 C1_20 C3_20 F5_20 -75(3) . . . . ? C4_20 C1_20 C3_20 F5_20 164(2) . . . . ? C2_20 C1_20 C3_20 F5_20 44(2) . . . . ? O1_20 C1_20 C3_20 F4_20 45(3) . . . . ? C4_20 C1_20 C3_20 F4_20 -76(2) . . . . ? C2_20 C1_20 C3_20 F4_20 163(2) . . . . ? O1_20 C1_20 C4_20 F7_20 -74(3) . . . . ? C2_20 C1_20 C4_20 F7_20 166(2) . . . . ? C3_20 C1_20 C4_20 F7_20 45(2) . . . . ? O1_20 C1_20 C4_20 F9_20 46(3) . . . . ? C2_20 C1_20 C4_20 F9_20 -74(2) . . . . ? C3_20 C1_20 C4_20 F9_20 165(2) . . . . ? O1_20 C1_20 C4_20 F8_20 165(3) . . . . ? C2_20 C1_20 C4_20 F8_20 45(2) . . . . ? C3_20 C1_20 C4_20 F8_20 -76(2) . . . . ? F1_22 C1_22 C2_22 F2_22 0.6(14) . . . . ? C6_22 C1_22 C2_22 F2_22 179.2(9) . . . . ? F1_22 C1_22 C2_22 C3_22 -179.5(9) . . . . ? C6_22 C1_22 C2_22 C3_22 -1.0(16) . . . . ? F2_22 C2_22 C3_22 F3_22 -0.3(16) . . . . ? C1_22 C2_22 C3_22 F3_22 179.9(9) . . . . ? F2_22 C2_22 C3_22 C4_22 -179.1(10) . . . . ? C1_22 C2_22 C3_22 C4_22 1.1(18) . . . . ? F3_22 C3_22 C4_22 F4_22 1.3(18) . . . . ? C2_22 C3_22 C4_22 F4_22 -179.9(11) . . . . ? F3_22 C3_22 C4_22 C5_22 -179.8(10) . . . . ? C2_22 C3_22 C4_22 C5_22 -1.0(19) . . . . ? F4_22 C4_22 C5_22 C6_22 179.7(11) . . . . ? C3_22 C4_22 C5_22 C6_22 0.8(18) . . . . ? F1_22 C1_22 C6_22 C5_22 179.3(9) . . . . ? C2_22 C1_22 C6_22 C5_22 0.8(16) . . . . ? C4_22 C5_22 C6_22 C1_22 -0.7(16) . . . . ? _shelx_res_file ; TITL p21c_b.res in P2(1)/c p21c_b.res created by SHELXL-2018/3 at 10:35:49 on 14-Feb-2022 REM Old TITL p21c in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.207, Rweak 0.005, Alpha 0.070 REM 0.897 for 618 systematic absences, Orientation as input REM Formula found by SHELXT: C84 O17 F35 Al3 Ag Os6 CELL 0.71073 20.5041 17.8097 25.2173 90.000 107.088 90.000 ZERR 4.000 0.0044 0.0034 0.0082 0.000 0.024 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C O F AL AG OS H UNIT 228 120 244 8 4 24 12 SIMU 0.04 0.08 2 O1_10 O1_20 O1_19 RIGU 0.004 0.004 O1_10 O1_20 O1_19 SIMU 0.02 0.04 2 C1_15 C2_15 F1_15 F2_15 F3_15 C3_15 F4_15 F5_15 F6_15 = C4_15 F7_15 F8_15 F9_15 C1_16 C2_16 F1_16 F2_16 F3_16 C3_16 F4_16 F5_16 = F6_16 C4_16 F7_16 F8_16 RIGU 0.002 0.002 C1_15 C2_15 F1_15 F2_15 F3_15 C3_15 F4_15 F5_15 F6_15 = C4_15 F7_15 F8_15 F9_15 C1_16 C2_16 F1_16 F2_16 F3_16 C3_16 F4_16 F5_16 = F6_16 C4_16 F7_16 F8_16 SIMU 0.02 0.02 2 O1_19 C1_19 C2_19 F1_19 F2_19 F3_19 C3_19 F4_19 F5_19 = F6_19 C4_19 F7_19 F8_19 F9_19 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 = F4_10 F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_20 C1_20 C2_20 F1_20 F2_20 = F3_20 C3_20 F4_20 F5_20 F6_20 C4_20 F7_20 F8_20 F9_20 RIGU 0.002 0.002 O1_19 C1_19 C2_19 F1_19 F2_19 F3_19 C3_19 F4_19 F5_19 = F6_19 C4_19 F7_19 F8_19 F9_19 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 = F4_10 F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_20 C1_20 C2_20 F1_20 F2_20 = F3_20 C3_20 F4_20 F5_20 F6_20 C4_20 F7_20 F8_20 F9_20 SIMU 0.04 0.08 2 O1_17 C1_17 C2_17 F1_17 F2_17 F3_17 C3_17 F4_17 F5_17 = F6_17 C4_17 F7_17 F8_17 F9_17 O1_18 C1_18 C2_18 F1_18 F2_18 F3_18 C3_18 = F4_18 F5_18 F6_18 C4_18 F7_18 F8_18 F9_18 RIGU 0.004 0.004 O1_17 C1_17 C2_17 F1_17 F2_17 F3_17 C3_17 F4_17 F5_17 = F6_17 C4_17 F7_17 F8_17 F9_17 O1_18 C1_18 C2_18 F1_18 F2_18 F3_18 C3_18 = F4_18 F5_18 F6_18 C4_18 F7_18 F8_18 F9_18 SADI 0.02 AL08 F1 AL08 F1B AL08 O1_9 AL08 O1_14 AL08 O1_15 AL08 O1_16 = AL08 O1_17 AL08 O1_18 SIMU 0.04 0.08 2 F1 F1B RIGU 0.004 0.004 F1 F1B SADI 0.02 F1B AL2 F1B AL08 SIMU 0.02 0.04 2 O1_19 C1_19 C2_19 F1_19 F2_19 F3_19 C3_19 F4_19 F5_19 = F6_19 C4_19 F7_19 F8_19 F9_19 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 = F4_10 F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_20 C1_20 C2_20 F1_20 F2_20 = F3_20 C3_20 F4_20 F5_20 F6_20 C4_20 F7_20 F8_20 F9_20 RIGU 0.002 0.002 O1_19 C1_19 C2_19 F1_19 F2_19 F3_19 C3_19 F4_19 F5_19 = F6_19 C4_19 F7_19 F8_19 F9_19 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 = F4_10 F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_20 C1_20 C2_20 F1_20 F2_20 = F3_20 C3_20 F4_20 F5_20 F6_20 C4_20 F7_20 F8_20 F9_20 RIGU 0.004 0.004 O1_19 C1_19 C2_19 F1_19 F2_19 F3_19 C3_19 F4_19 F5_19 = F6_19 C4_19 F7_19 F8_19 F9_19 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 = F4_10 F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_20 C1_20 C2_20 F1_20 F2_20 = F3_20 C3_20 F4_20 F5_20 F6_20 C4_20 F7_20 F8_20 F9_20 SIMU 0.04 0.08 2 O1_19 C1_19 C2_19 F1_19 F2_19 F3_19 C3_19 F4_19 F5_19 = F6_19 C4_19 F7_19 F8_19 F9_19 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 = F4_10 F5_10 F6_10 C4_10 F7_10 F8_10 F9_10 O1_20 C1_20 C2_20 F1_20 F2_20 = F3_20 C3_20 F4_20 F5_20 F6_20 C4_20 F7_20 F8_20 F9_20 RIGU 0.002 0.002 O1_17 C1_17 C2_17 F1_17 F2_17 F3_17 C3_17 F4_17 F5_17 = F6_17 C4_17 F7_17 F8_17 F9_17 O1_18 C1_18 C2_18 F1_18 F2_18 F3_18 C3_18 = F4_18 F5_18 F6_18 C4_18 F7_18 F8_18 F9_18 SIMU 0.02 0.04 2 O1_17 C1_17 C2_17 F1_17 F2_17 F3_17 C3_17 F4_17 F5_17 = F6_17 C4_17 F7_17 F8_17 F9_17 O1_18 C1_18 C2_18 F1_18 F2_18 F3_18 C3_18 = F4_18 F5_18 F6_18 C4_18 F7_18 F8_18 F9_18 SIMU 0.02 0.04 2 O1_17 C1_17 C2_17 F1_17 F2_17 F3_17 C3_17 F4_17 F5_17 = F6_17 C4_17 F7_17 F8_17 F9_17 O1_18 C1_18 C2_18 F1_18 F2_18 F3_18 C3_18 = F4_18 F5_18 F6_18 C4_18 F7_18 F8_18 F9_18 RIGU 0.002 0.002 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 O1_14 C1_14 C2_14 F1_14 F2_14 F3_14 C3_14 F4_14 = F5_14 F6_14 C4_14 F7_14 F8_14 F9_14 SIMU 0.02 0.04 2 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 O1_14 C1_14 C2_14 F1_14 F2_14 F3_14 C3_14 F4_14 = F5_14 F6_14 C4_14 F7_14 F8_14 F9_14 REM Restraints for Fragment tetfluorbenz, 1,2,3,4-Tetrafluorobenzene, REM C6H2F4 from: CCDC ZELDOJ, http://dx.doi.org/10.1002/anie.199515171. REM Please cite https://doi.org/10.1107/S1600576718004508 REM HFIX_TFB 43 C5 C6 SIMU_TFB F1 > C6 RIGU_TFB F1 > C6 FLAT_TFB F1 > C6 SADI_TFB 0.02 C1 C2 C2 C3 C3 C4 C4 C5 C5 C6 C6 C1 SADI_TFB 0.02 C1 F1 C2 F2 C3 F3 C4 F4 SADI_TFB 0.04 C1 C3 C3 C5 C5 C1 C2 C6 C6 C4 C2 C4 SADI_TFB 0.05 C2 F1 C6 F1 C1 F2 C3 F2 C2 F3 C4 F3 C3 F4 C5 F4 SAME_TFB F1 > C6 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SADI 0.04 F1 AL08 F1 AL1 F1B AL08 F1B AL2 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 BIND AL1 O1_20 TEMP -173.150 L.S. 10 BOND $H CONF MORE -1 LIST 4 ACTA FMAP 2 PLAN 20 SUMP 1.0 0.000001 1 6 1 7 1 2 WGHT 0.024000 125.010704 FVAR 0.05909 0.48437 0.68653 0.65693 0.71118 0.36040 0.15524 FVAR 0.29112 0.35943 0.15556 OS2 6 0.320153 0.092898 0.989158 11.00000 0.02505 0.02463 = 0.02270 -0.00351 0.01006 -0.00415 OS3 6 0.234550 0.149645 0.884068 11.00000 0.02176 0.02806 = 0.02376 -0.00603 0.00782 0.00110 OS4 6 0.291373 0.148017 0.684180 11.00000 0.02105 0.02043 = 0.02711 -0.00053 0.00832 -0.00096 OS5 6 0.201721 0.099817 0.577717 11.00000 0.03238 0.02259 = 0.02441 -0.00372 0.01083 -0.00219 OS6 6 0.170386 0.049704 0.676970 11.00000 0.02219 0.02426 = 0.02381 -0.00413 0.00784 -0.00329 OS1 6 0.347478 0.039466 0.889330 11.00000 0.02512 0.02039 = 0.02488 0.00039 0.01282 0.00026 AG1 5 0.261943 0.095660 0.783576 11.00000 0.02130 0.02387 = 0.02398 -0.00429 0.00838 -0.00132 PART 1 -21 AL1 4 0.664917 0.107744 0.739486 -21.00000 0.01300 0.02085 = 0.01528 0.00181 -0.00238 0.00031 PART 2 21 AL2 4 0.667790 0.116372 0.759875 21.00000 0.01512 0.03553 = 0.01583 0.00868 -0.00369 -0.00070 PART 0 AL08 4 0.841669 0.092443 0.766742 11.00000 0.01826 0.02985 = 0.02408 -0.00349 0.00680 -0.00187 O1 2 0.237080 -0.083403 0.860684 11.00000 0.06400 0.03244 = 0.03938 -0.00504 0.01561 -0.01868 PART 1 -21 F1 3 0.752799 0.101701 0.746708 -21.00000 0.01165 0.03059 = 0.02654 0.01268 -0.00017 0.00386 PART 2 21 F1B 3 0.753646 0.108349 0.759135 21.00000 0.01439 0.05630 = 0.01884 0.01345 0.00371 -0.00448 PART 0 C2 1 0.409296 -0.025811 0.941456 11.00000 0.03755 0.03095 = 0.03265 0.00522 0.01945 0.00325 C11 1 0.175646 0.186373 0.815142 11.00000 0.02733 0.04986 = 0.03435 -0.00579 0.01026 0.01076 C12 1 0.301026 0.229172 0.882696 11.00000 0.03888 0.03427 = 0.02788 0.00926 0.01033 0.01639 C13 1 0.235428 -0.034413 0.691478 11.00000 0.02975 0.02839 = 0.03826 -0.00387 0.01230 -0.00584 C14 1 0.140287 0.020722 0.738914 11.00000 0.02662 0.02556 = 0.03088 -0.00816 0.00291 -0.00505 C15 1 0.100862 -0.006789 0.625123 11.00000 0.03652 0.04095 = 0.03841 0.00291 0.01818 -0.00340 C16 1 0.109948 0.135906 0.665244 11.00000 0.02830 0.03819 = 0.03245 0.00325 0.01867 -0.00719 C17 1 0.246776 0.002315 0.580851 11.00000 0.03961 0.03365 = 0.03244 -0.00409 0.00950 -0.00267 C18 1 0.122120 0.062745 0.520709 11.00000 0.04448 0.03267 = 0.02377 0.01093 0.01680 0.00051 C19 1 0.250506 0.138697 0.527906 11.00000 0.05138 0.03913 = 0.03067 -0.00481 0.02477 0.00128 C20 1 0.155113 0.196122 0.576281 11.00000 0.03698 0.02753 = 0.02181 -0.00135 0.00827 -0.00711 C21 1 0.345122 0.060275 0.677074 11.00000 0.02506 0.03160 = 0.03471 -0.00040 0.01469 -0.00529 C22 1 0.357875 0.175622 0.753432 11.00000 0.02319 0.02942 = 0.03642 0.00873 0.00841 0.00039 C23 1 0.334490 0.205971 0.639857 11.00000 0.02891 0.03639 = 0.04421 0.00753 0.01326 0.00082 C24 1 0.232263 0.232402 0.690772 11.00000 0.02970 0.02285 = 0.02989 -0.00131 0.00418 -0.00617 C3 1 0.376635 0.008789 0.827096 11.00000 0.03683 0.02436 = 0.03477 0.00698 0.01670 0.00533 O4 2 0.456054 0.165638 0.912244 11.00000 0.03362 0.04965 = 0.04338 0.00737 0.01104 -0.01273 O5 2 0.235020 -0.052260 0.981269 11.00000 0.06046 0.04167 = 0.03340 -0.01006 0.02040 -0.02871 O2 2 0.444550 -0.066954 0.970332 11.00000 0.04253 0.03458 = 0.04757 0.00860 0.01769 0.01001 O3 2 0.401191 -0.013329 0.794337 11.00000 0.06038 0.04588 = 0.04649 0.01096 0.03500 0.02264 C4 1 0.415827 0.121245 0.903831 11.00000 0.02860 0.04409 = 0.03075 0.00857 0.01052 0.00935 C5 1 0.265553 0.000696 0.983653 11.00000 0.03970 0.03953 = 0.02291 -0.00476 0.01439 -0.00517 C6 1 0.274173 0.136815 1.036627 11.00000 0.02802 0.03607 = 0.03798 -0.00712 0.00352 -0.00706 C7 1 0.395533 0.047709 1.043380 11.00000 0.02558 0.03432 = 0.04522 0.01276 0.01978 0.00490 C8 1 0.374866 0.184923 0.993000 11.00000 0.03725 0.02760 = 0.02599 -0.00212 0.00858 -0.00754 C9 1 0.172287 0.065637 0.885813 11.00000 0.03823 0.05173 = 0.02687 -0.01358 0.01372 -0.00451 C10 1 0.189617 0.207493 0.926455 11.00000 0.03643 0.04871 = 0.03641 -0.00945 0.00610 0.00833 O6 2 0.245703 0.163443 1.065712 11.00000 0.04951 0.04819 = 0.04382 -0.01033 0.02715 0.00243 O7 2 0.440957 0.024154 1.077111 11.00000 0.03874 0.05667 = 0.03151 0.00835 0.01241 0.00368 O8 2 0.406941 0.237256 0.998794 11.00000 0.04899 0.04006 = 0.03164 -0.00440 0.00878 -0.02342 O9 2 0.135188 0.020670 0.888553 11.00000 0.03755 0.07572 = 0.04073 -0.00839 0.01836 -0.02486 O10 2 0.160275 0.241942 0.950382 11.00000 0.04988 0.06035 = 0.05113 -0.01691 0.02199 0.01853 O11 2 0.135914 0.213139 0.778199 11.00000 0.04175 0.06521 = 0.03112 -0.00496 0.00494 0.02847 O12 2 0.335303 0.276831 0.880109 11.00000 0.04951 0.03352 = 0.03832 0.00519 0.00579 -0.01085 O13 2 0.270654 -0.084112 0.701277 11.00000 0.04507 0.02556 = 0.05750 -0.00070 0.02142 -0.00033 O14 2 0.114522 0.000158 0.771673 11.00000 0.03565 0.04886 = 0.03018 0.00007 0.01497 -0.00980 O15 2 0.059077 -0.042180 0.595464 11.00000 0.03998 0.05659 = 0.03184 -0.01017 0.00504 -0.02292 O16 2 0.071292 0.184012 0.658158 11.00000 0.03823 0.04907 = 0.03966 0.00070 0.01646 0.01020 O17 2 0.273539 -0.054038 0.579534 11.00000 0.08495 0.02616 = 0.04826 -0.00601 0.02445 0.01736 O18 2 0.076436 0.043372 0.487698 11.00000 0.05344 0.06233 = 0.03166 -0.02192 0.00128 -0.02027 O19 2 0.279189 0.161155 0.500632 11.00000 0.06046 0.04590 = 0.05713 0.00511 0.03896 0.00272 O20 2 0.126608 0.251157 0.572482 11.00000 0.03536 0.02905 = 0.03880 0.00411 0.01139 0.00243 O21 2 0.377748 0.010545 0.672504 11.00000 0.03814 0.03078 = 0.05993 -0.00175 0.02251 0.00677 O22 2 0.400919 0.195393 0.789928 11.00000 0.02587 0.04294 = 0.03969 0.00975 -0.00412 -0.00957 O23 2 0.361912 0.240021 0.614971 11.00000 0.04724 0.04194 = 0.05685 0.01586 0.02871 0.00225 O24 2 0.200502 0.281785 0.695719 11.00000 0.04359 0.02959 = 0.04618 -0.01045 0.00565 0.00787 C1 1 0.275024 -0.037603 0.871606 11.00000 0.04281 0.02711 = 0.02616 -0.00279 0.01660 -0.00060 RESI CCF3 1 RESI 0 RESI CCF3 2 RESI 0 RESI CCF3 3 RESI 0 RESI CCF3 4 RESI 0 RESI CCF3 5 RESI 0 RESI CCF3 6 RESI 0 RESI CCF3 7 PART 1 -21 O1 2 0.641598 0.175722 0.690687 -21.00000 0.02980 0.04206 = 0.03580 0.01277 -0.00517 0.00606 C1 1 0.597078 0.205182 0.643526 -21.00000 0.02444 0.02888 = 0.03156 0.01040 0.00189 0.00803 C2 1 0.534712 0.151519 0.624630 -21.00000 0.02817 0.03670 = 0.03776 0.01105 -0.00543 0.00360 F1 3 0.551803 0.089881 0.602534 -21.00000 0.08514 0.04608 = 0.03708 -0.00705 -0.00697 0.00773 F2 3 0.482812 0.182349 0.585938 -21.00000 0.03757 0.08834 = 0.03029 0.00955 -0.01624 0.01339 F3 3 0.512313 0.134116 0.667892 -21.00000 0.04384 0.05660 = 0.04998 0.02317 0.00558 -0.00692 C3 1 0.573668 0.283409 0.656340 -21.00000 0.05699 0.02965 = 0.04159 0.00200 0.00012 0.01247 F4 3 0.628062 0.324871 0.684125 -21.00000 0.09475 0.02703 = 0.06714 -0.00137 -0.01258 -0.00555 F5 3 0.531097 0.279456 0.686944 -21.00000 0.07919 0.06124 = 0.05137 0.01401 0.01894 0.03601 F6 3 0.541420 0.321260 0.609814 -21.00000 0.08406 0.04796 = 0.05891 0.02770 0.00173 0.02439 C4 1 0.631964 0.212108 0.596306 -21.00000 0.04061 0.06764 = 0.03748 0.01759 0.01053 0.01291 F7 3 0.674697 0.270194 0.607151 -21.00000 0.05170 0.10891 = 0.07641 0.02876 0.02127 -0.02636 F8 3 0.583876 0.224732 0.548402 -21.00000 0.05628 0.08953 = 0.03671 0.02222 -0.00197 -0.01029 F9 3 0.664856 0.147872 0.594022 -21.00000 0.09264 0.09808 = 0.09964 0.00686 0.05438 0.05040 PART 0 RESI 0 RESI CCF3 8 PART 2 21 O1 2 0.618538 0.151555 0.697413 21.00000 0.01776 0.03536 = 0.04151 0.01713 -0.00002 -0.00035 C1 1 0.601794 0.208868 0.659398 21.00000 0.03248 0.03100 = 0.03685 0.01301 0.00781 0.00905 C2 1 0.633266 0.191048 0.612164 21.00000 0.10565 0.07090 = 0.06630 0.01598 0.04866 0.03025 F1 3 0.700359 0.209107 0.630672 21.00000 0.08845 0.13091 = 0.15399 0.04908 0.08929 0.03158 F2 3 0.602342 0.231173 0.566082 21.00000 0.18015 0.09764 = 0.04775 0.02163 0.03871 0.01490 F3 3 0.622452 0.118920 0.597396 21.00000 0.13450 0.07573 = 0.09616 -0.00625 0.08426 0.01886 C3 1 0.522767 0.211672 0.636755 21.00000 0.04001 0.04938 = 0.05674 0.01480 -0.00636 0.00674 F4 3 0.495671 0.205987 0.678914 21.00000 0.01871 0.06565 = 0.08505 0.01513 0.00872 0.00826 F5 3 0.502810 0.155414 0.599491 21.00000 0.09406 0.06010 = 0.05238 0.01071 -0.04821 0.00036 F6 3 0.504096 0.279419 0.613618 21.00000 0.05233 0.06636 = 0.09590 0.04461 -0.01360 0.02139 C4 1 0.628987 0.285304 0.686433 21.00000 0.05282 0.04296 = 0.04819 0.01025 0.00560 -0.00346 F7 3 0.585634 0.310553 0.713565 21.00000 0.09517 0.05179 = 0.04331 -0.01468 0.02252 0.00074 F8 3 0.638020 0.332629 0.647167 21.00000 0.07958 0.03354 = 0.06367 0.01594 0.02448 -0.00200 F9 3 0.691510 0.275748 0.722134 21.00000 0.03948 0.04166 = 0.08064 0.01744 -0.00216 -0.01778 PART 0 RESI 0 RESI CCF3 9 PART 1 41 O1 2 0.877527 0.177309 0.783612 41.00000 0.03090 0.02907 = 0.03388 -0.00818 0.01333 -0.00879 C1 1 0.904559 0.238262 0.764755 41.00000 0.02429 0.02424 = 0.04454 -0.00199 0.01138 -0.00282 C2 1 0.849146 0.282116 0.720399 41.00000 0.03137 0.04323 = 0.04636 0.00408 0.01597 0.00900 F1 3 0.808613 0.320356 0.744086 41.00000 0.04173 0.06440 = 0.06773 0.00637 0.02727 0.02469 F2 3 0.877861 0.328426 0.692357 41.00000 0.05777 0.04678 = 0.05083 0.00920 0.02535 0.00802 F3 3 0.809218 0.234228 0.684775 41.00000 0.04256 0.06684 = 0.04283 0.00172 0.00594 0.00118 C3 1 0.961643 0.213539 0.739180 41.00000 0.03438 0.01879 = 0.06937 0.00234 0.02684 0.00013 F4 3 1.000352 0.159878 0.769351 41.00000 0.03568 0.02889 = 0.09922 0.01486 0.02730 0.00678 F5 3 0.934149 0.188241 0.687043 41.00000 0.05550 0.03630 = 0.07080 -0.00745 0.04019 -0.00400 F6 3 1.003029 0.271972 0.738423 41.00000 0.04170 0.02544 = 0.10390 0.00125 0.03985 -0.00455 C4 1 0.934585 0.290242 0.815620 41.00000 0.05314 0.03068 = 0.04903 -0.00538 0.00886 -0.01013 F7 3 0.994535 0.262124 0.847617 41.00000 0.05703 0.05208 = 0.07378 -0.00961 -0.01722 -0.01913 F8 3 0.945664 0.359341 0.800089 41.00000 0.06775 0.02682 = 0.06915 -0.01071 0.01949 -0.01163 F9 3 0.892761 0.293756 0.846968 41.00000 0.07727 0.04663 = 0.04915 -0.01521 0.02182 -0.01513 PART 0 RESI 0 PART 0 RESI 0 RESI CCF3 11 PART 0 RESI 0 RESI CCF3 12 PART 1 -21 O1 2 0.633186 0.021434 0.718203 -21.00000 0.02685 0.03141 = 0.05574 -0.00469 0.01725 -0.00938 C1 1 0.603884 -0.044421 0.727349 -21.00000 0.02869 0.03087 = 0.03758 0.00529 0.00868 -0.00270 C2 1 0.561967 -0.076464 0.670453 -21.00000 0.03485 0.04075 = 0.03448 0.00036 0.00957 0.00543 F1 3 0.502685 -0.038810 0.651599 -21.00000 0.03568 0.05760 = 0.05801 -0.00173 -0.00121 0.00713 F2 3 0.548453 -0.148887 0.673549 -21.00000 0.04926 0.04058 = 0.06751 -0.00958 0.01780 -0.00554 F3 3 0.596265 -0.069239 0.633412 -21.00000 0.06618 0.03616 = 0.04754 -0.00698 0.03028 0.00372 C3 1 0.660995 -0.100788 0.756485 -21.00000 0.04961 0.03297 = 0.04456 -0.00336 0.00450 0.00247 F4 3 0.711916 -0.063914 0.793254 -21.00000 0.05049 0.03928 = 0.05892 -0.00353 -0.01059 0.01247 F5 3 0.686237 -0.135133 0.719117 -21.00000 0.04206 0.03942 = 0.06179 -0.01664 0.00669 0.01150 F6 3 0.636677 -0.154606 0.781833 -21.00000 0.06960 0.04338 = 0.06592 0.02443 0.01848 0.01588 C4 1 0.555587 -0.030395 0.763930 -21.00000 0.04362 0.02008 = 0.03533 -0.00019 0.01336 -0.01050 F7 3 0.593243 -0.025156 0.817466 -21.00000 0.07447 0.05252 = 0.03664 -0.00787 0.01721 0.00266 F8 3 0.510291 -0.085919 0.757357 -21.00000 0.05687 0.03834 = 0.10209 -0.00944 0.05297 -0.02130 F9 3 0.519951 0.032990 0.749254 -21.00000 0.04054 0.02898 = 0.04225 -0.00458 0.02104 -0.00538 PART 0 RESI 0 RESI CCF3 13 PART 2 21 O1 2 0.645139 0.026337 0.767398 21.00000 0.02485 0.03575 = 0.03272 0.01221 -0.00914 -0.01307 C1 1 0.606945 -0.034983 0.745471 21.00000 0.01692 0.02888 = 0.03023 -0.00004 0.00491 0.00051 C2 1 0.532710 -0.011395 0.713266 21.00000 0.02572 0.02676 = 0.04287 -0.00951 -0.00306 0.00103 F1 3 0.513461 0.042155 0.743184 21.00000 0.03509 0.04250 = 0.06285 -0.00901 0.01556 0.00828 F2 3 0.490824 -0.069566 0.710582 21.00000 0.01969 0.03729 = 0.09677 0.00998 -0.02439 -0.00505 F3 3 0.530415 0.013522 0.662588 21.00000 0.04045 0.04660 = 0.03915 0.00358 -0.01265 -0.00103 C3 1 0.639301 -0.072875 0.703986 21.00000 0.05678 0.09337 = 0.03222 0.00827 0.01538 0.04712 F4 3 0.695666 -0.111284 0.731860 21.00000 0.07238 0.12075 = 0.06945 -0.00128 0.01481 0.07333 F5 3 0.657977 -0.021998 0.672523 21.00000 0.07017 0.16897 = 0.06249 0.05627 0.04652 0.06783 F6 3 0.594681 -0.119348 0.670636 21.00000 0.12311 0.09239 = 0.03298 -0.01756 -0.00514 0.05695 C4 1 0.607698 -0.090008 0.793070 21.00000 0.04901 0.03382 = 0.02646 0.00114 0.00047 -0.01095 F7 3 0.669633 -0.094280 0.829277 21.00000 0.04419 0.03395 = 0.02823 0.01546 -0.00497 -0.01274 F8 3 0.589522 -0.159649 0.774007 21.00000 0.02319 0.02433 = 0.05196 0.00239 -0.00245 -0.00083 F9 3 0.562304 -0.064318 0.818932 21.00000 0.07470 0.05847 = 0.05227 -0.00342 0.03741 -0.02524 PART 0 RESI 0 RESI CCF3 14 PART 2 -41 O1 2 0.871097 0.181159 0.751599 -41.00000 0.02852 0.02735 = 0.03982 -0.00788 0.01386 -0.00202 C1 1 0.908059 0.245662 0.768962 -41.00000 0.02971 0.02487 = 0.04680 -0.00356 0.01387 -0.00223 C2 1 0.863420 0.303265 0.789005 -41.00000 0.04175 0.02527 = 0.04559 -0.00477 0.01768 0.00015 F1 3 0.821834 0.339922 0.745486 -41.00000 0.03077 0.03636 = 0.05578 0.00431 0.01949 0.00215 F2 3 0.901853 0.354597 0.822955 -41.00000 0.04880 0.03372 = 0.06397 -0.01701 0.01037 0.00254 F3 3 0.826604 0.267740 0.817146 -41.00000 0.06211 0.03946 = 0.05748 0.00038 0.03610 0.00354 C3 1 0.972878 0.228246 0.817992 -41.00000 0.03202 0.03466 = 0.05308 0.00153 0.00732 -0.00741 F4 3 1.001608 0.164531 0.808353 -41.00000 0.03227 0.03588 = 0.06219 0.01906 0.01880 0.00189 F5 3 0.955687 0.221785 0.865532 -41.00000 0.06225 0.05506 = 0.04779 -0.00441 0.01224 -0.01282 F6 3 1.020170 0.282908 0.824759 -41.00000 0.02776 0.04207 = 0.08758 0.00816 0.00275 -0.00935 C4 1 0.929582 0.282272 0.720551 -41.00000 0.03467 0.03253 = 0.05465 0.00435 0.02138 0.00438 F7 3 0.981918 0.244803 0.711812 -41.00000 0.04407 0.04063 = 0.07202 0.01210 0.03470 0.01121 F8 3 0.947870 0.354445 0.731808 -41.00000 0.04601 0.03131 = 0.06817 0.00781 0.02182 0.00280 F9 3 0.876752 0.281485 0.674248 -41.00000 0.04307 0.05636 = 0.05497 0.00794 0.01646 -0.00091 PART 0 RESI 0 RESI CCF3 15 PART 1 31 O1 2 0.857895 0.036274 0.825943 31.00000 0.02494 0.04353 = 0.02805 0.00388 -0.00053 0.00678 C1 1 0.902371 0.014156 0.874819 31.00000 0.04010 0.04065 = 0.03522 0.01267 -0.00151 0.00143 C2 1 0.962036 -0.034347 0.865898 31.00000 0.03309 0.05978 = 0.04956 0.01829 -0.00026 0.00659 F1 3 0.938892 -0.102870 0.847803 31.00000 0.07319 0.05497 = 0.06522 0.00474 0.01424 0.00919 F2 3 1.012146 -0.038984 0.913988 31.00000 0.05403 0.07483 = 0.07221 0.02530 -0.02665 0.01227 F3 3 0.989486 0.001521 0.831629 31.00000 0.04212 0.10386 = 0.10455 0.06365 0.03080 0.02845 C3 1 0.934879 0.083407 0.909395 31.00000 0.09380 0.04177 = 0.04475 0.01480 -0.02680 -0.00042 F4 3 0.885565 0.134730 0.906563 31.00000 0.15394 0.05789 = 0.04666 -0.00260 -0.01529 0.03701 F5 3 0.984874 0.110049 0.890699 31.00000 0.09260 0.05710 = 0.08361 0.01013 -0.03282 -0.03860 F6 3 0.961944 0.064798 0.963713 31.00000 0.16800 0.06216 = 0.04101 0.00891 -0.03850 0.00227 C4 1 0.864055 -0.036008 0.906472 31.00000 0.05594 0.06094 = 0.03784 0.01324 0.01470 0.00413 F7 3 0.827463 0.009577 0.928541 31.00000 0.10470 0.13151 = 0.05224 0.01556 0.03839 0.05128 F8 3 0.907382 -0.073128 0.948362 31.00000 0.06134 0.07826 = 0.04814 0.03536 0.02422 0.00796 F9 3 0.826252 -0.087524 0.872185 31.00000 0.07131 0.06813 = 0.06173 0.01298 0.02156 -0.02498 PART 0 RESI 0 RESI CCF3 16 PART 2 -31 O1 2 0.877919 0.072470 0.833979 -31.00000 0.02022 0.02781 = 0.03724 -0.00016 -0.00267 -0.00154 C1 1 0.901252 0.017754 0.871468 -31.00000 0.04720 0.04512 = 0.04941 0.01510 -0.00291 0.00255 C2 1 0.948855 -0.036527 0.852240 -31.00000 0.04759 0.05198 = 0.06270 0.01497 -0.00034 0.00557 F1 3 0.906058 -0.091315 0.825413 -31.00000 0.05470 0.05706 = 0.10524 -0.00780 0.00486 0.00206 F2 3 1.001308 -0.059448 0.894727 -31.00000 0.04757 0.08007 = 0.06648 0.02937 0.00771 0.01902 F3 3 0.974681 -0.005236 0.814829 -31.00000 0.02786 0.08115 = 0.06284 0.02739 -0.00373 0.01943 C3 1 0.933955 0.056754 0.927948 -31.00000 0.09809 0.05825 = 0.05430 0.00908 -0.01624 -0.00495 F4 3 0.893542 0.117097 0.929384 -31.00000 0.13789 0.08047 = 0.05063 -0.01428 -0.02675 0.01864 F5 3 0.997546 0.078742 0.930210 -31.00000 0.09305 0.06468 = 0.09201 0.02877 -0.04057 -0.01846 F6 3 0.923628 0.010270 0.966759 -31.00000 0.15149 0.09950 = 0.05336 0.02400 -0.01033 -0.01658 C4 1 0.839626 -0.031529 0.875404 -31.00000 0.06077 0.06832 = 0.05559 0.01877 0.00647 -0.00893 F7 3 0.805206 0.007090 0.904088 -31.00000 0.05443 0.11024 = 0.06668 -0.00490 0.00826 -0.01604 F8 3 0.864936 -0.096255 0.900237 -31.00000 0.06541 0.06835 = 0.09235 0.03200 -0.00194 -0.01802 F9 3 0.800920 -0.045867 0.823362 -31.00000 0.03186 0.04285 = 0.06556 0.00152 0.00702 -0.00331 PART 0 RESI 0 RESI CCF3 17 PART 2 -51 O1 2 0.831937 0.030754 0.713707 -51.00000 0.04184 0.03209 = 0.04818 -0.01958 0.01888 -0.01217 C1 1 0.854630 0.007460 0.670887 -51.00000 0.04839 0.05104 = 0.04889 -0.01811 0.02001 0.00079 C2 1 0.791092 0.019713 0.619603 -51.00000 0.05767 0.08423 = 0.05528 -0.02607 0.00965 0.00337 F1 3 0.737045 0.010868 0.639121 -51.00000 0.04764 0.06837 = 0.07613 -0.05750 0.00979 -0.01416 F2 3 0.789245 -0.029244 0.579521 -51.00000 0.05280 0.09425 = 0.06027 -0.03782 0.00983 -0.01620 F3 3 0.795624 0.089503 0.602426 -51.00000 0.07087 0.08833 = 0.04684 -0.01328 0.01461 0.01965 C3 1 0.916895 0.052661 0.665852 -51.00000 0.05224 0.05711 = 0.04835 -0.01054 0.02393 0.00019 F4 3 0.961461 0.062860 0.716133 -51.00000 0.04378 0.06823 = 0.05547 -0.01775 0.02124 0.00027 F5 3 0.896205 0.119384 0.642242 -51.00000 0.08357 0.06706 = 0.06128 0.00437 0.04068 0.01035 F6 3 0.948737 0.014114 0.635146 -51.00000 0.05811 0.07884 = 0.06732 -0.02765 0.03280 -0.00278 C4 1 0.872772 -0.076771 0.679050 -51.00000 0.07877 0.04740 = 0.08129 -0.01945 0.03769 0.00387 F7 3 0.934756 -0.082233 0.717023 -51.00000 0.08091 0.05304 = 0.10525 -0.00747 0.03504 0.02739 F8 3 0.871688 -0.107000 0.630219 -51.00000 0.11259 0.07423 = 0.10432 -0.04442 0.05667 -0.00311 F9 3 0.826008 -0.110486 0.698594 -51.00000 0.10686 0.04564 = 0.11624 -0.03594 0.06266 -0.01697 PART 0 RESI 0 RESI CCF3 18 PART 1 51 O1 2 0.862394 0.050435 0.712802 51.00000 0.05194 0.03003 = 0.03865 -0.00555 0.01764 0.00154 C1 1 0.854737 -0.003277 0.672766 51.00000 0.04700 0.04055 = 0.04452 -0.01305 0.02375 -0.00739 C2 1 0.845167 -0.081494 0.696037 51.00000 0.08264 0.03839 = 0.06727 -0.01655 0.04415 -0.01789 F1 3 0.905248 -0.109779 0.725859 51.00000 0.10624 0.04553 = 0.08081 0.00952 0.03907 -0.00084 F2 3 0.816026 -0.130300 0.656151 51.00000 0.13136 0.05879 = 0.08046 -0.02898 0.04979 -0.04796 F3 3 0.806712 -0.075553 0.730081 51.00000 0.12432 0.05435 = 0.10013 -0.01332 0.08227 -0.02910 C3 1 0.793720 0.016337 0.622035 51.00000 0.05685 0.09389 = 0.05741 -0.01965 0.00664 -0.00293 F4 3 0.786078 0.090149 0.617818 51.00000 0.10189 0.10343 = 0.04029 0.00973 0.01262 0.02656 F5 3 0.737070 -0.017046 0.626108 51.00000 0.06213 0.17881 = 0.17303 -0.00124 0.00355 -0.04271 F6 3 0.804446 -0.008516 0.575188 51.00000 0.13467 0.17108 = 0.05582 -0.04305 0.00020 0.03751 C4 1 0.919854 -0.004335 0.653709 51.00000 0.04873 0.04678 = 0.04676 -0.00206 0.02355 -0.00004 F7 3 0.920392 0.053778 0.619580 51.00000 0.07697 0.04815 = 0.05634 0.00076 0.03489 -0.00476 F8 3 0.923395 -0.067524 0.625895 51.00000 0.07137 0.05106 = 0.05616 -0.00230 0.03573 0.01200 F9 3 0.975616 0.000719 0.695605 51.00000 0.04344 0.06969 = 0.06356 -0.00137 0.01453 0.00522 PART 0 RESI 0 RESI CCF3 19 PART 1 61 O1 2 0.660421 0.125938 0.803932 61.00000 0.03417 0.02850 = 0.04375 0.00427 0.01891 -0.00482 C1 1 0.650691 0.173690 0.843789 61.00000 0.04496 0.03148 = 0.04689 0.00253 0.02045 -0.00614 C2 1 0.687335 0.139051 0.901450 61.00000 0.05420 0.03856 = 0.04475 0.00118 0.01449 -0.01095 F1 3 0.677306 0.064656 0.899441 61.00000 0.05541 0.03706 = 0.04612 0.00932 0.01184 -0.00807 F2 3 0.661566 0.166635 0.940428 61.00000 0.06019 0.05470 = 0.04620 -0.00781 0.01671 -0.01601 F3 3 0.754966 0.150041 0.913123 61.00000 0.05104 0.03499 = 0.05556 -0.00794 0.00903 -0.00607 C3 1 0.680287 0.251326 0.836458 61.00000 0.04908 0.03280 = 0.05687 0.00143 0.01768 -0.01002 F4 3 0.637398 0.290140 0.794990 61.00000 0.05264 0.03278 = 0.05697 0.00638 0.02659 -0.00441 F5 3 0.740516 0.244535 0.826281 61.00000 0.04454 0.04105 = 0.06946 0.00002 0.01708 -0.01322 F6 3 0.691780 0.292894 0.882552 61.00000 0.06943 0.04006 = 0.05826 -0.00265 0.01823 -0.01035 C4 1 0.572635 0.179563 0.834704 61.00000 0.04587 0.03436 = 0.04836 -0.00079 0.02584 -0.00446 F7 3 0.539312 0.186520 0.780249 61.00000 0.04361 0.03133 = 0.04965 0.00012 0.02357 0.00060 F8 3 0.553690 0.239945 0.857124 61.00000 0.05191 0.04248 = 0.06389 -0.01944 0.02426 -0.01060 F9 3 0.549086 0.118002 0.852989 61.00000 0.04485 0.03827 = 0.04249 -0.00366 0.02287 -0.00944 PART 0 RESI 0 PART 0 RESI 0 RESI TFB 21 PART -1 10.5 F1 3 0.602173 -0.089026 0.522745 10.50000 0.10823 0.15905 = 0.16652 -0.08066 0.04325 0.01986 F2 3 0.562319 0.050973 0.481529 10.50000 0.26060 0.20714 = 0.12130 -0.05128 0.07867 -0.09129 F3 3 0.437897 0.103885 0.481400 10.50000 0.29704 0.09957 = 0.08789 0.01090 0.01892 0.05567 F4 3 0.357329 0.018877 0.520732 10.50000 0.18558 0.14257 = 0.13462 0.03527 0.06830 0.06765 C1 1 0.541673 -0.061697 0.522661 10.50000 0.10424 0.09421 = 0.08683 -0.05640 0.01961 0.01137 C2 1 0.522072 0.008980 0.501606 10.50000 0.16026 0.10167 = 0.09966 -0.03754 0.03547 0.00232 C3 1 0.458546 0.036030 0.501201 10.50000 0.18602 0.08490 = 0.04536 -0.01805 0.03347 0.04060 C4 1 0.416714 -0.007998 0.521926 10.50000 0.17256 0.09696 = 0.06856 -0.01659 0.03769 0.04318 C5 1 0.435663 -0.078859 0.543126 10.50000 0.12926 0.11051 = 0.05105 -0.00349 0.02859 0.03311 AFIX 43 H5 7 0.406217 -0.108353 0.557576 10.50000 -1.20000 AFIX 0 C6 1 0.497926 -0.105167 0.542672 10.50000 0.10330 0.09975 = 0.05127 -0.04038 0.00172 0.01320 AFIX 43 H6 7 0.511617 -0.154185 0.556314 10.50000 -1.20000 AFIX 0 PART 0 RESI 0 RESI CCF3 10 PART 2 21.0 O1 2 0.673202 0.170520 0.815784 21.00000 0.04035 0.03506 = 0.05505 0.00552 0.01752 -0.01425 C1 1 0.652112 0.192668 0.859354 21.00000 0.04917 0.03485 = 0.05005 0.00532 0.01462 -0.01080 C2 1 0.708859 0.233195 0.904691 21.00000 0.06574 0.04558 = 0.05759 0.00328 0.00696 -0.01674 F1 3 0.745469 0.279831 0.882882 21.00000 0.06041 0.04446 = 0.06928 0.00107 0.00240 -0.02324 F2 3 0.680271 0.276208 0.936565 21.00000 0.10610 0.06069 = 0.06655 -0.01457 0.01807 -0.01700 F3 3 0.746975 0.180653 0.936999 21.00000 0.07409 0.05579 = 0.06845 0.01031 -0.01065 -0.01810 C3 1 0.624457 0.124921 0.884594 21.00000 0.05507 0.03790 = 0.04613 0.00545 0.01887 -0.01012 F4 3 0.562740 0.105900 0.850769 21.00000 0.05187 0.03531 = 0.04834 0.00322 0.02156 -0.01151 F5 3 0.669314 0.067952 0.893465 21.00000 0.05615 0.03631 = 0.05169 0.01161 0.01641 -0.00951 F6 3 0.616324 0.140883 0.934161 21.00000 0.08052 0.05394 = 0.04619 0.00204 0.02457 -0.01022 C4 1 0.593334 0.251521 0.837530 21.00000 0.05674 0.03779 = 0.05987 0.00321 0.01954 -0.00479 F7 3 0.548622 0.222986 0.791789 21.00000 0.04551 0.04386 = 0.06149 0.00411 0.01687 -0.00030 F8 3 0.561708 0.256071 0.876954 21.00000 0.07495 0.06471 = 0.07049 -0.00138 0.03406 -0.00481 F9 3 0.621638 0.317382 0.830242 21.00000 0.07300 0.03142 = 0.05307 -0.00040 0.02329 -0.00512 PART 0 RESI 0 RESI CCF3 20 PART 3 71.0 O1 2 0.653186 0.142844 0.800003 71.00000 0.04255 0.03486 = 0.04879 0.00315 0.01878 -0.01084 C1 1 0.664186 0.189989 0.844652 71.00000 0.04901 0.03714 = 0.05042 0.00116 0.01590 -0.00852 C2 1 0.665033 0.142909 0.896668 71.00000 0.05705 0.04067 = 0.04849 0.00146 0.01510 -0.01028 F1 3 0.600890 0.123140 0.893803 71.00000 0.05715 0.04049 = 0.04829 0.00289 0.01705 -0.00877 F2 3 0.692425 0.182147 0.943166 71.00000 0.06886 0.04458 = 0.04962 -0.00016 0.01444 -0.01406 F3 3 0.701601 0.080384 0.897442 71.00000 0.05513 0.04202 = 0.05078 0.00395 0.01319 -0.00820 C3 1 0.734543 0.229206 0.853781 71.00000 0.04920 0.03682 = 0.05631 -0.00139 0.01432 -0.00980 F4 3 0.739987 0.252137 0.804493 71.00000 0.03841 0.03521 = 0.05651 -0.00247 0.01270 -0.00954 F5 3 0.782430 0.177599 0.876404 71.00000 0.04883 0.03707 = 0.05528 -0.00863 0.00223 -0.01068 F6 3 0.740445 0.289291 0.886623 71.00000 0.05276 0.03846 = 0.05819 -0.00335 0.01777 -0.01138 C4 1 0.607315 0.250187 0.834328 71.00000 0.05326 0.03819 = 0.05862 0.00206 0.02202 -0.00583 F7 3 0.615818 0.301768 0.798240 71.00000 0.05553 0.03844 = 0.06144 0.00443 0.02223 -0.00567 F8 3 0.608890 0.283460 0.882506 71.00000 0.06341 0.04192 = 0.06320 -0.00184 0.02715 -0.00841 F9 3 0.545990 0.217702 0.813648 71.00000 0.05036 0.04674 = 0.05941 0.00193 0.02500 -0.00641 PART 0 RESI TFB 22 F1 3 0.777940 0.203252 1.063313 11.00000 0.10239 0.06722 = 0.07803 0.02742 0.05733 0.02439 F2 3 0.764977 0.334768 1.009262 11.00000 0.12568 0.06906 = 0.11933 0.04431 0.06724 0.04770 F3 3 0.870287 0.391695 0.978347 11.00000 0.12689 0.08954 = 0.23505 0.11179 0.07519 0.02993 F4 3 0.989811 0.316961 1.001567 11.00000 0.07759 0.10916 = 0.23630 0.10758 0.03669 -0.00386 C1 1 0.831197 0.230551 1.048907 11.00000 0.09081 0.03655 = 0.04255 0.00435 0.03265 0.01106 C2 1 0.823530 0.298119 1.020875 11.00000 0.09367 0.03878 = 0.06559 0.01066 0.03874 0.01313 C3 1 0.877786 0.326295 1.005579 11.00000 0.08601 0.03936 = 0.09570 0.02956 0.02213 0.00347 C4 1 0.938278 0.287939 1.016890 11.00000 0.07091 0.05752 = 0.10445 0.03766 0.01369 -0.00520 C5 1 0.945815 0.220499 1.044757 11.00000 0.06507 0.05308 = 0.07994 0.02564 0.01027 0.00408 AFIX 43 H5 7 0.987784 0.193915 1.053131 11.00000 -1.20000 AFIX 0 C6 1 0.891498 0.191991 1.060387 11.00000 0.07949 0.03160 = 0.05110 0.00990 0.01744 0.00233 AFIX 43 H6 7 0.896065 0.145234 1.079259 11.00000 -1.20000 RESI 0 REM ##### AFIX 0 HKLF 4 REM p21c_b.res in P2(1)/c REM wR2 = 0.0965, GooF = S = 1.124, Restrained GooF = 1.001 for all data REM R1 = 0.0420 for 15614 Fo > 4sig(Fo) and 0.0587 for all 19471 data REM 2368 parameters refined using 27525 restraints END WGHT 0.0240 125.0001 REM Highest difference peak 1.518, deepest hole -1.927, 1-sigma level 0.195 Q1 1 0.1620 0.0955 0.5806 11.00000 0.05 1.52 Q2 1 0.3650 0.1035 0.9854 11.00000 0.05 1.51 Q3 1 0.2912 0.0476 0.7805 11.00000 0.05 1.49 Q4 1 0.2492 0.1434 0.6810 11.00000 0.05 1.47 Q5 1 0.2437 0.0925 0.5941 11.00000 0.05 1.43 Q6 1 0.1641 0.0846 0.6681 11.00000 0.05 1.42 Q7 1 0.9283 0.1627 0.9022 11.00000 0.05 1.38 Q8 1 0.1299 0.0306 0.6726 11.00000 0.05 1.30 Q9 1 0.1874 0.1509 0.8739 11.00000 0.05 1.29 Q10 1 0.8008 0.0521 0.9070 11.00000 0.05 1.29 Q11 1 0.2524 0.1197 0.5668 11.00000 0.05 1.29 Q12 1 0.2164 0.0477 0.6893 11.00000 0.05 1.28 Q13 1 0.8570 0.0626 0.9406 11.00000 0.05 1.28 Q14 1 0.2556 0.1043 0.7094 11.00000 0.05 1.26 Q15 1 0.7636 -0.0668 0.6214 11.00000 0.05 1.24 Q16 1 0.2001 0.0868 0.5495 11.00000 0.05 1.24 Q17 1 0.2392 0.1551 0.5789 11.00000 0.05 1.23 Q18 1 0.2737 0.1634 0.8776 11.00000 0.05 1.21 Q19 1 0.8689 -0.0522 0.8583 11.00000 0.05 1.20 Q20 1 0.2015 0.1357 0.5677 11.00000 0.05 1.16 ; _shelx_res_checksum 82814 _shelx_hkl_file ; 2 0 0 6101.39 174.58 2 0 0 5895.51 173.58 2 0 0 5737.23 173.48 -2 0 0 6033.00 173.78 -2 0 0 6004.20 173.78 -2 0 0 6036.70 174.38 -3 0 0 58.69 3.70 -3 0 0 52.39 3.40 -3 0 0 59.89 3.40 3 0 0 59.39 3.80 3 0 0 55.59 3.40 3 0 0 56.69 3.30 4 0 0 23.20 2.80 4 0 0 22.00 2.60 4 0 0 31.80 3.90 -4 0 0 26.20 2.90 -4 0 0 23.00 2.80 -4 0 0 29.20 3.00 5 0 0 29.50 4.00 5 0 0 30.80 3.60 5 0 0 33.30 3.50 -5 0 0 31.60 3.70 -5 0 0 27.70 3.30 -5 0 0 24.50 3.40 6 0 0 657.33 22.90 -6 0 0 656.63 23.00 -6 0 0 633.64 21.80 -6 0 0 622.64 22.10 6 0 0 638.74 21.80 6 0 0 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224.48 7.80 3 3 0 222.78 9.30 -4 -3 0 3.80 1.80 -4 -3 0 2.40 1.20 4 -3 0 4.90 2.00 4 -3 0 1.80 1.60 -4 -3 0 4.10 1.90 -4 3 0 1.60 1.50 4 3 0 3.50 1.40 4 3 0 2.20 1.50 -4 3 0 2.60 1.10 -4 3 0 2.80 1.10 4 3 0 3.40 1.90 -4 3 0 2.00 1.60 5 -3 0 115.79 6.80 -5 -3 0 125.09 7.20 5 -3 0 121.69 5.40 -5 -3 0 131.59 6.00 5 -3 0 116.39 6.80 -5 -3 0 106.39 6.70 5 3 0 124.59 7.20 5 3 0 117.99 5.80 -5 3 0 122.39 6.80 -5 3 0 111.29 6.60 5 3 0 121.29 6.80 -5 3 0 118.79 5.30 -6 -3 0 40.50 5.00 -6 -3 0 50.89 5.50 -6 -3 0 45.00 4.30 6 -3 0 43.50 3.40 6 -3 0 38.80 4.80 6 -3 0 53.69 5.20 -6 3 0 53.39 5.80 6 3 0 39.30 4.00 -6 3 0 50.79 5.10 6 3 0 40.90 4.80 -6 3 0 35.00 3.10 6 3 0 47.00 5.40 -7 -3 0 651.23 22.90 7 -3 0 668.73 24.40 7 -3 0 636.34 24.10 -7 -3 0 715.43 24.90 7 -3 0 684.13 22.30 -7 -3 0 674.53 24.50 -7 3 0 665.53 22.10 -7 3 0 645.74 24.10 7 3 0 703.73 23.00 -7 3 0 693.93 24.40 7 3 0 672.63 24.40 8 -3 0 42.00 5.70 -8 -3 0 38.30 5.60 8 -3 0 33.40 3.90 -8 -3 0 39.40 4.80 -8 -3 0 44.90 7.00 8 -3 0 25.80 4.50 -8 3 0 38.40 6.20 -8 3 0 45.40 4.40 8 3 0 36.90 5.60 8 3 0 27.40 4.80 8 3 0 40.00 4.80 -9 -3 0 468.45 19.70 -9 -3 0 430.76 18.70 -9 -3 0 415.76 17.30 9 -3 0 422.86 18.80 9 -3 0 443.66 16.70 9 -3 0 469.55 19.20 9 3 0 450.55 17.40 9 3 0 393.26 18.70 9 3 0 447.86 19.00 -9 3 0 474.45 19.30 -9 3 0 473.85 16.90 -9 3 0 453.45 18.90 -10 -3 0 22.60 4.40 -10 -3 0 15.20 5.30 -10 -3 0 17.20 4.40 10 -3 0 22.40 5.30 10 -3 0 24.10 4.20 10 -3 0 16.70 4.70 10 3 0 17.20 4.00 -10 3 0 24.60 4.20 -10 3 0 17.00 4.80 10 3 0 19.80 4.70 10 3 0 16.20 4.50 -10 3 0 22.40 5.80 11 -3 0 10.00 3.40 -11 -3 0 12.30 4.20 -11 -3 0 14.80 5.70 11 -3 0 15.40 4.80 -11 -3 0 9.20 3.30 -11 3 0 14.50 5.00 11 3 0 10.70 4.30 -11 3 0 12.10 4.30 11 3 0 10.10 4.90 12 -3 0 81.59 9.10 12 -3 0 94.99 7.60 -12 -3 0 92.49 9.60 -12 -3 0 82.79 10.80 12 -3 0 72.59 9.00 12 3 0 90.39 9.60 -12 3 0 84.19 9.70 12 3 0 76.19 9.30 -12 3 0 91.29 7.50 12 3 0 83.69 8.50 13 -3 0 89.59 10.10 -13 -3 0 97.09 9.20 -13 -3 0 100.49 10.80 13 -3 0 113.99 13.10 13 -3 0 89.99 7.90 -13 -3 0 105.19 10.90 -13 3 0 102.09 10.50 13 3 0 102.79 10.60 -13 3 0 109.59 8.20 13 3 0 107.39 10.10 13 3 0 110.59 11.60 -13 3 0 89.29 10.30 -14 -3 0 40.30 7.10 14 -3 0 33.50 8.10 -14 -3 0 31.00 6.00 14 -3 0 34.90 7.10 14 -3 0 32.00 6.00 -14 -3 0 43.60 8.00 14 3 0 37.40 7.20 -14 3 0 47.50 6.40 14 3 0 32.60 6.10 -14 3 0 24.20 6.60 -14 3 0 33.10 6.60 14 3 0 37.70 7.50 -15 -3 0 34.60 7.30 15 -3 0 64.09 10.90 -15 -3 0 55.89 7.70 15 -3 0 54.79 7.30 -15 -3 0 43.40 8.80 15 -3 0 37.40 7.80 -15 3 0 47.20 8.30 -15 3 0 47.70 6.80 -15 3 0 42.90 8.50 15 3 0 38.30 7.50 15 3 0 39.50 6.90 15 3 0 46.80 8.80 -16 -3 0 8.00 4.20 16 -3 0 0.70 4.80 16 -3 0 3.40 4.10 -16 -3 0 -2.20 2.90 -16 -3 0 6.60 5.60 16 -3 0 3.20 4.40 -16 3 0 10.00 6.00 16 3 0 7.70 4.80 -16 3 0 6.70 4.30 16 3 0 7.70 5.20 16 3 0 7.30 5.00 -16 3 0 7.50 3.90 17 -3 0 -3.90 4.20 -17 -3 0 1.40 5.80 17 -3 0 -2.10 3.90 -17 -3 0 0.30 3.50 -17 -3 0 -8.40 4.70 17 -3 0 -1.20 3.80 -17 3 0 -1.80 5.10 17 3 0 -4.40 3.90 17 3 0 2.70 4.20 17 3 0 0.10 3.80 -17 3 0 0.60 3.30 -18 -3 0 2.70 5.30 -18 -3 0 0.30 3.70 18 -3 0 0.80 4.00 18 -3 0 -0.60 4.00 18 -3 0 0.40 4.80 18 3 0 7.60 8.70 18 3 0 -1.00 3.90 -18 3 0 7.70 4.50 -18 3 0 9.40 6.90 18 3 0 4.40 5.00 19 -3 0 -2.10 4.70 19 -3 0 -1.20 4.60 -19 -3 0 4.50 7.10 19 -3 0 -4.30 4.40 -19 3 0 0.30 3.70 -19 3 0 2.40 6.20 19 3 0 -2.80 3.80 19 3 0 4.00 5.40 -20 -3 0 59.09 14.40 20 -3 0 46.40 8.60 20 -3 0 48.20 9.70 20 3 0 43.00 9.00 20 3 0 45.10 8.70 -20 3 0 54.79 10.90 21 -3 0 -1.20 4.60 -21 -3 0 13.90 7.20 21 -3 0 -2.60 5.00 -21 3 0 5.60 7.60 21 3 0 1.70 5.10 21 3 0 6.10 6.20 -22 -3 0 43.00 10.00 22 -3 0 41.20 10.00 22 -3 0 26.40 8.00 -22 3 0 51.69 11.40 22 3 0 39.10 8.80 22 3 0 41.00 9.20 -23 -3 0 -5.60 5.30 23 -3 0 -0.20 5.70 23 -3 0 1.50 6.80 23 3 0 -4.00 5.20 23 3 0 9.30 6.60 -23 3 0 11.50 8.80 24 -3 0 -2.60 7.50 24 -3 0 -11.90 4.30 -24 -3 0 0.60 6.20 24 3 0 -7.30 4.50 -24 3 0 -3.20 5.90 24 3 0 -1.90 5.50 0 -4 0 394.96 12.70 0 -4 0 418.76 13.40 0 -4 0 415.36 14.30 0 4 0 428.96 13.50 0 4 0 402.86 12.80 -1 -4 0 37.60 1.80 1 -4 0 40.60 2.50 1 -4 0 40.10 2.50 -1 -4 0 43.30 2.90 1 -4 0 45.20 3.30 -1 -4 0 43.10 3.40 -1 4 0 41.60 2.70 -1 4 0 44.70 3.30 1 4 0 36.20 2.90 -1 4 0 42.30 2.50 1 4 0 40.90 3.20 1 4 0 38.00 1.80 2 -4 0 2489.85 77.09 -2 -4 0 2530.55 79.39 2 -4 0 2366.26 78.19 -2 -4 0 2484.65 78.59 2 -4 0 2538.95 74.99 -2 4 0 2451.25 74.89 2 4 0 2478.05 79.59 -2 4 0 2433.76 78.49 -2 4 0 2418.06 77.29 2 4 0 2407.16 78.19 -3 -4 0 39.30 1.90 -3 -4 0 45.00 4.30 3 -4 0 41.30 3.60 -3 -4 0 41.80 3.70 3 -4 0 42.30 3.50 3 -4 0 37.70 2.50 3 4 0 46.20 3.70 -3 4 0 41.50 4.10 -3 4 0 37.20 2.50 3 4 0 34.70 2.20 -3 4 0 41.70 3.50 3 4 0 45.60 4.40 -4 -4 0 1360.06 40.60 -4 -4 0 1476.55 43.10 4 -4 0 1464.15 43.10 4 -4 0 1412.86 43.00 -4 -4 0 1399.06 43.30 4 4 0 1373.26 42.80 -4 4 0 1360.76 40.90 -4 4 0 1390.26 41.10 -4 4 0 1320.97 42.80 4 4 0 1394.06 43.50 4 4 0 1316.37 40.90 -4 4 0 1367.16 42.90 -5 -4 0 250.97 9.30 -5 -4 0 276.97 11.50 5 -4 0 263.27 11.30 -5 4 0 263.97 11.20 5 4 0 260.87 9.60 5 4 0 254.97 11.10 -5 4 0 251.77 9.40 5 4 0 263.37 11.80 -5 4 0 251.57 9.30 -5 4 0 268.57 11.30 -6 -4 0 271.17 12.30 -6 -4 0 262.77 12.40 -6 -4 0 259.37 10.40 6 -4 0 276.27 10.20 6 -4 0 283.37 12.50 6 -4 0 263.77 12.10 6 4 0 273.37 12.70 6 4 0 279.27 10.60 -6 4 0 273.27 10.10 -6 4 0 275.37 12.10 -6 4 0 277.47 10.30 -6 4 0 289.47 12.40 6 4 0 267.07 12.00 7 -4 0 -0.10 1.40 -7 -4 0 -0.80 2.00 -7 -4 0 -0.50 1.60 -7 -4 0 -0.70 2.20 7 -4 0 3.10 2.60 7 -4 0 -1.90 2.00 7 4 0 -0.50 2.00 7 4 0 -2.90 2.10 -7 4 0 2.00 1.60 7 4 0 0.80 1.80 -7 4 0 1.30 2.10 -7 4 0 2.00 2.10 -8 -4 0 112.39 8.10 8 -4 0 105.39 6.20 -8 -4 0 90.99 7.90 -8 -4 0 102.99 6.60 8 -4 0 112.19 8.10 -8 4 0 116.69 8.00 -8 4 0 119.99 6.30 8 4 0 100.49 7.90 8 4 0 117.29 6.80 -8 4 0 107.99 7.90 9 -4 0 102.39 8.30 -9 -4 0 89.69 8.10 -9 -4 0 88.89 6.50 9 -4 0 116.69 6.40 9 -4 0 94.99 8.00 9 4 0 99.99 8.30 9 4 0 81.89 6.40 9 4 0 78.39 8.40 -9 4 0 100.09 6.10 -9 4 0 94.79 7.90 -10 -4 0 207.28 13.00 -10 -4 0 236.58 12.90 10 -4 0 239.38 13.20 -10 -4 0 214.88 11.00 10 -4 0 234.68 13.10 10 -4 0 234.88 10.70 -10 4 0 225.28 12.70 -10 4 0 213.68 10.30 10 4 0 221.88 13.00 10 4 0 226.58 13.30 10 4 0 214.68 11.00 -10 4 0 223.28 12.60 11 -4 0 187.98 12.20 -11 -4 0 162.18 11.30 11 -4 0 181.88 9.80 -11 -4 0 177.08 12.40 11 4 0 189.78 10.60 11 4 0 188.28 12.20 -11 4 0 182.28 12.00 -11 4 0 189.88 9.80 -11 4 0 176.58 11.70 11 4 0 167.28 11.80 12 -4 0 80.49 10.60 12 -4 0 74.79 9.20 -12 -4 0 60.49 8.70 -12 -4 0 56.99 7.80 12 -4 0 58.09 6.60 -12 -4 0 83.09 7.10 12 4 0 76.39 7.90 12 4 0 89.39 10.70 -12 4 0 76.49 6.50 -12 4 0 89.09 10.00 12 4 0 54.09 7.80 13 -4 0 107.49 11.90 -13 -4 0 104.69 12.80 13 -4 0 84.19 10.10 -13 -4 0 90.99 10.30 -13 -4 0 102.99 8.40 13 -4 0 106.79 8.30 -13 4 0 84.69 7.60 -13 4 0 104.19 10.60 13 4 0 117.49 12.90 13 4 0 116.49 11.60 13 4 0 84.79 8.80 -13 4 0 109.89 11.70 -14 -4 0 1.10 3.50 14 -4 0 2.80 4.40 14 -4 0 -1.10 4.80 -14 -4 0 4.50 4.70 -14 -4 0 7.00 4.60 14 -4 0 9.40 4.10 14 4 0 3.00 4.20 -14 4 0 5.30 3.40 14 4 0 11.60 4.70 -14 4 0 12.80 5.70 -14 4 0 7.10 4.60 14 4 0 12.10 5.50 -15 -4 0 1.20 4.50 15 -4 0 1.70 3.90 15 -4 0 -2.70 4.20 -15 -4 0 -1.60 3.40 -15 -4 0 2.50 3.50 15 -4 0 0.30 3.30 15 4 0 0.70 3.60 15 4 0 3.00 4.20 15 4 0 -4.20 3.90 -15 4 0 -2.20 3.20 -15 4 0 4.50 3.30 -15 4 0 -0.10 4.90 16 -4 0 55.69 9.10 16 -4 0 31.20 7.70 -16 -4 0 57.39 9.40 -16 -4 0 65.79 9.00 -16 -4 0 66.49 8.10 16 -4 0 42.00 7.20 -16 4 0 62.69 9.10 -16 4 0 56.09 7.70 -16 4 0 51.59 9.60 16 4 0 52.89 7.90 16 4 0 48.80 9.50 16 4 0 58.99 9.10 17 -4 0 13.70 5.40 17 -4 0 26.90 7.30 -17 -4 0 21.50 5.50 -17 -4 0 22.40 7.40 -17 4 0 15.70 4.90 17 4 0 23.50 6.80 17 4 0 17.10 5.40 -17 4 0 14.10 6.80 17 4 0 13.10 6.60 18 -4 0 -0.10 4.80 18 -4 0 8.90 5.20 18 -4 0 -2.80 3.60 -18 -4 0 2.10 6.00 -18 -4 0 0.60 3.60 -18 4 0 4.70 4.50 18 4 0 0.80 4.00 18 4 0 -1.20 4.60 18 4 0 0.50 6.20 -18 4 0 -3.00 5.40 19 -4 0 -12.20 4.00 -19 -4 0 -1.40 3.80 19 -4 0 -1.10 4.00 -19 -4 0 9.50 7.40 19 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528.05 22.90 8 -5 0 98.69 7.70 8 -5 0 76.79 7.20 -8 -5 0 82.49 5.50 -8 -5 0 91.09 7.60 -8 -5 0 81.29 7.50 -8 5 0 92.19 7.40 8 5 0 82.89 5.60 8 5 0 92.89 8.50 -8 5 0 92.29 5.40 -8 5 0 93.39 7.40 -8 5 0 83.59 5.30 8 5 0 87.49 8.70 9 -5 0 42.80 6.40 -9 -5 0 51.89 7.60 9 -5 0 42.80 4.60 -9 -5 0 53.59 5.30 9 -5 0 46.00 6.10 -9 -5 0 39.50 6.10 9 5 0 46.50 5.10 -9 5 0 34.60 5.60 -9 5 0 52.59 7.00 9 5 0 37.80 6.10 -9 5 0 38.00 4.40 9 5 0 46.50 6.90 -9 5 0 48.00 4.80 -10 -5 0 40.60 6.50 -10 -5 0 58.59 8.60 10 -5 0 57.89 7.80 -10 -5 0 55.79 5.90 10 -5 0 61.09 5.30 10 -5 0 69.39 8.40 -10 5 0 41.40 6.40 10 5 0 54.89 6.00 -10 5 0 58.09 7.50 10 5 0 44.00 6.50 10 5 0 48.40 7.30 -10 5 0 60.89 5.10 11 -5 0 472.55 20.90 -11 -5 0 438.06 17.70 11 -5 0 441.66 17.20 -11 -5 0 433.56 20.60 -11 -5 0 417.66 19.80 11 5 0 441.56 20.10 11 5 0 446.36 17.90 -11 5 0 420.36 19.80 -11 5 0 445.06 17.10 11 5 0 440.76 20.60 -11 5 0 460.15 20.40 12 -5 0 336.97 18.10 -12 -5 0 329.57 15.40 -12 -5 0 328.97 17.50 12 -5 0 352.76 18.40 12 -5 0 388.76 21.60 -12 -5 0 337.87 18.40 -12 5 0 350.16 17.80 -12 5 0 357.56 15.00 12 5 0 378.16 18.70 12 5 0 355.36 18.00 12 5 0 345.47 17.50 13 -5 0 230.48 12.20 13 -5 0 249.18 15.40 -13 -5 0 248.58 15.90 13 -5 0 228.38 15.00 -13 -5 0 237.68 12.90 -13 -5 0 232.48 14.30 -13 5 0 261.97 15.50 13 5 0 249.68 15.00 13 5 0 230.78 12.70 -13 5 0 228.48 14.30 13 5 0 211.68 14.50 -14 -5 0 252.07 13.50 14 -5 0 257.57 13.30 14 -5 0 254.57 16.40 -14 -5 0 261.07 16.80 14 -5 0 260.57 16.30 14 5 0 230.98 15.40 -14 5 0 254.27 16.20 -14 5 0 211.88 14.50 -14 5 0 246.58 12.90 14 5 0 238.98 15.50 14 5 0 269.77 13.90 15 -5 0 14.30 4.60 -15 -5 0 13.40 4.60 15 -5 0 6.60 5.60 -15 -5 0 19.80 7.20 15 -5 0 2.10 4.60 -15 -5 0 16.10 5.20 -15 5 0 15.00 6.10 15 5 0 17.70 5.10 -15 5 0 12.80 4.40 15 5 0 11.50 5.10 -15 5 0 15.60 5.70 15 5 0 14.60 6.00 16 -5 0 37.80 8.10 -16 -5 0 50.39 7.20 16 -5 0 51.29 8.90 -16 -5 0 58.89 10.70 16 -5 0 53.49 7.50 -16 -5 0 64.89 9.00 16 5 0 62.09 8.00 -16 5 0 55.99 9.50 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5.00 -4 6 0 38.00 3.00 -5 -6 0 15.30 3.40 -5 -6 0 7.40 3.10 5 -6 0 15.50 3.50 -5 -6 0 13.10 1.60 5 -6 0 10.60 3.00 5 -6 0 9.50 2.00 5 6 0 11.30 3.30 5 6 0 9.20 2.80 -5 6 0 12.70 2.00 -5 6 0 13.80 3.40 5 6 0 9.40 1.70 -5 6 0 11.60 2.00 -5 6 0 14.00 3.10 -6 -6 0 465.35 18.30 6 -6 0 450.65 18.20 -6 -6 0 439.26 14.80 -6 -6 0 496.65 20.80 6 -6 0 466.35 18.30 -6 6 0 486.25 18.40 6 6 0 458.75 18.00 -6 6 0 477.55 15.80 6 6 0 451.35 15.30 -6 6 0 437.46 18.10 -6 6 0 447.26 15.50 6 6 0 465.85 19.10 7 -6 0 1.80 3.20 -7 -6 0 0.10 1.40 -7 -6 0 0.00 2.50 -7 -6 0 2.90 2.70 -7 6 0 2.10 1.70 -7 6 0 4.50 2.80 7 6 0 0.20 2.80 7 6 0 2.90 3.20 -7 6 0 1.90 2.40 -7 6 0 4.10 1.70 7 6 0 4.10 1.90 8 -6 0 732.13 27.30 8 -6 0 760.92 27.70 -8 -6 0 772.02 30.20 -8 -6 0 713.03 23.80 -8 -6 0 689.03 27.20 -8 6 0 725.73 27.00 8 6 0 695.03 23.90 8 6 0 719.53 26.80 -8 6 0 762.52 24.20 -8 6 0 746.73 24.00 8 6 0 720.43 27.90 -9 -6 0 14.60 5.10 9 -6 0 8.30 3.90 -9 -6 0 9.70 2.60 -9 -6 0 13.80 4.20 9 -6 0 4.00 2.80 -9 6 0 10.10 2.60 -9 6 0 8.10 4.10 -9 6 0 8.60 2.60 9 6 0 8.80 2.80 -9 6 0 2.50 3.00 9 6 0 7.40 3.20 9 6 0 11.00 4.60 10 -6 0 19.40 5.20 -10 -6 0 20.20 5.40 -10 -6 0 19.20 4.80 10 -6 0 28.40 5.70 -10 -6 0 28.20 4.10 -10 6 0 25.50 3.80 10 6 0 17.60 4.90 10 6 0 32.50 6.60 -10 6 0 23.00 4.90 10 6 0 26.30 4.40 -10 6 0 26.80 5.70 -10 6 0 25.40 3.70 11 -6 0 13.50 5.20 -11 -6 0 8.30 3.90 -11 -6 0 0.40 2.70 -11 -6 0 5.70 3.60 11 -6 0 6.00 4.30 -11 6 0 7.80 2.90 11 6 0 9.30 4.60 -11 6 0 7.50 2.80 11 6 0 5.40 3.10 11 6 0 7.70 3.30 -11 6 0 2.30 4.10 -11 6 0 7.00 4.20 12 -6 0 154.68 13.30 -12 -6 0 180.68 13.20 -12 -6 0 187.38 12.60 12 -6 0 179.18 12.90 -12 -6 0 200.08 12.10 12 -6 0 171.68 12.70 12 6 0 188.98 12.70 12 6 0 194.98 13.40 -12 6 0 180.28 9.80 -12 6 0 198.08 12.90 12 6 0 193.08 10.60 -13 -6 0 93.99 10.90 13 -6 0 113.09 12.50 13 -6 0 111.79 8.20 13 -6 0 126.39 11.40 -13 -6 0 98.69 10.60 -13 -6 0 87.49 10.10 -13 6 0 114.99 8.20 13 6 0 104.89 11.50 -13 6 0 128.39 11.20 -13 6 0 121.29 8.40 -13 6 0 127.59 11.40 13 6 0 106.89 11.30 13 6 0 90.59 8.20 -14 -6 0 160.18 13.70 -14 -6 0 138.19 11.80 -14 -6 0 152.28 10.20 14 -6 0 173.68 13.30 14 -6 0 171.68 10.40 14 -6 0 172.98 13.30 14 6 0 131.19 13.40 -14 6 0 161.98 12.40 -14 6 0 158.48 13.00 14 6 0 165.58 10.60 -14 6 0 162.08 10.00 14 6 0 158.88 12.50 15 -6 0 391.66 21.50 -15 -6 0 361.86 17.20 -15 -6 0 341.37 19.30 -15 -6 0 383.56 21.60 15 -6 0 372.36 17.10 15 -6 0 377.56 20.80 15 6 0 370.76 17.50 15 6 0 322.77 20.00 -15 6 0 402.66 21.40 -15 6 0 369.06 17.00 -15 6 0 408.16 20.50 15 6 0 389.46 20.80 -16 -6 0 109.69 8.90 16 -6 0 104.69 18.80 16 -6 0 74.69 10.90 16 -6 0 91.19 9.30 -16 -6 0 77.69 10.80 16 6 0 100.99 12.00 -16 6 0 85.59 8.90 16 6 0 70.89 10.60 16 6 0 89.89 9.60 -16 6 0 92.19 11.70 17 -6 0 660.13 31.10 -17 -6 0 670.73 32.40 17 -6 0 665.63 26.90 -17 -6 0 657.03 26.80 17 -6 0 683.93 32.20 17 6 0 703.23 31.00 -17 6 0 664.53 31.50 17 6 0 671.33 27.40 -17 6 0 669.83 26.90 17 6 0 698.83 37.30 18 -6 0 1.70 5.10 18 -6 0 3.80 4.50 18 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-0.80 1.70 0 7 0 0.80 1.50 0 7 0 -0.20 1.10 1 -7 0 38.60 3.60 -1 -7 0 34.40 3.80 -1 -7 0 29.30 4.60 1 -7 0 37.40 4.40 1 -7 0 34.90 2.90 -1 -7 0 34.00 2.30 1 -7 0 38.80 4.30 -1 7 0 39.80 3.70 -1 7 0 40.00 3.40 1 7 0 38.80 2.50 1 7 0 34.70 3.90 2 -7 0 54.69 3.90 -2 -7 0 50.79 4.40 -2 -7 0 64.39 5.40 2 -7 0 55.59 4.90 2 -7 0 59.89 3.80 -2 7 0 58.09 5.10 -2 7 0 58.59 3.90 -2 7 0 57.19 4.40 2 7 0 68.69 5.30 2 7 0 64.69 5.10 3 -7 0 169.48 8.80 -3 -7 0 151.98 8.10 3 -7 0 138.19 7.40 -3 -7 0 162.88 8.90 3 -7 0 158.78 6.80 3 7 0 173.58 8.80 3 7 0 160.88 8.60 -3 7 0 163.98 6.90 -3 7 0 165.98 8.70 -3 7 0 147.19 7.90 4 -7 0 23.10 4.00 4 -7 0 29.50 4.00 -4 -7 0 29.70 4.70 -4 -7 0 30.20 4.10 4 -7 0 22.70 2.80 -4 7 0 29.20 3.00 -4 7 0 36.30 4.70 4 7 0 27.80 4.70 -4 7 0 24.40 4.10 4 7 0 29.90 4.30 -5 -7 0 189.58 10.10 5 -7 0 171.68 7.50 5 -7 0 191.48 9.60 -5 -7 0 189.28 11.20 5 -7 0 175.38 9.70 -5 7 0 189.88 9.80 -5 7 0 173.68 7.50 5 7 0 171.18 9.50 5 7 0 191.78 10.40 5 7 0 173.58 6.40 -6 -7 0 2.70 1.20 6 -7 0 1.10 2.50 -6 -7 0 7.60 3.30 -6 -7 0 5.70 2.90 6 -7 0 4.30 2.90 -6 7 0 5.00 1.90 -6 7 0 1.90 2.50 -6 7 0 2.20 1.60 6 7 0 5.00 1.60 6 7 0 -0.40 2.90 6 7 0 4.70 2.80 7 -7 0 33.90 5.40 -7 -7 0 26.50 2.70 -7 -7 0 22.40 4.60 -7 -7 0 29.90 5.00 7 -7 0 27.00 4.70 -7 7 0 27.00 4.70 7 7 0 21.80 4.90 -7 7 0 23.40 3.20 -7 7 0 28.20 5.00 -7 7 0 23.50 3.10 7 7 0 23.60 4.60 7 7 0 24.90 2.90 -8 -7 0 28.30 5.80 -8 -7 0 28.70 5.20 -8 -7 0 26.50 3.10 8 -7 0 24.90 5.70 8 -7 0 21.50 4.90 -8 7 0 20.30 4.20 8 7 0 21.20 5.60 8 7 0 27.80 5.40 8 7 0 31.20 3.60 -8 7 0 26.60 3.50 -8 7 0 32.10 3.70 -8 7 0 14.50 4.50 9 -7 0 303.17 15.30 -9 -7 0 305.77 11.70 -9 -7 0 325.57 15.80 -9 -7 0 287.37 15.00 9 -7 0 314.87 15.50 9 7 0 266.97 14.20 -9 7 0 303.87 11.90 -9 7 0 275.37 14.80 9 7 0 289.07 15.60 -9 7 0 286.37 11.90 -9 7 0 299.77 14.90 9 7 0 292.47 11.90 -10 -7 0 143.89 10.90 10 -7 0 160.48 11.40 10 -7 0 156.28 11.00 -10 -7 0 144.89 7.80 -10 -7 0 137.29 10.40 -10 7 0 153.28 8.10 10 7 0 153.68 10.60 10 7 0 139.59 11.20 -10 7 0 152.48 10.70 10 7 0 137.59 7.90 -10 7 0 144.39 10.70 -10 7 0 154.48 7.90 11 -7 0 496.25 22.70 -11 -7 0 512.35 18.70 -11 -7 0 483.25 22.20 -11 -7 0 489.55 22.70 11 -7 0 524.45 23.00 11 7 0 494.45 22.00 -11 7 0 504.05 18.60 -11 7 0 493.85 18.70 -11 7 0 475.35 22.10 11 7 0 498.85 23.10 -11 7 0 489.85 22.00 11 7 0 501.95 18.90 -12 -7 0 68.69 9.00 12 -7 0 69.69 9.60 12 -7 0 86.79 12.40 -12 -7 0 91.39 11.40 -12 -7 0 66.89 6.80 12 7 0 72.69 9.60 -12 7 0 75.59 8.10 12 7 0 78.29 7.40 -12 7 0 85.29 6.90 -12 7 0 65.19 11.20 12 7 0 95.59 11.30 -12 7 0 73.69 9.50 -13 -7 0 11.70 5.30 13 -7 0 5.20 4.70 -13 -7 0 7.60 3.60 -13 -7 0 10.90 4.30 13 -7 0 14.30 5.90 -13 7 0 2.60 4.50 13 7 0 8.30 4.00 13 7 0 5.50 4.40 13 7 0 13.00 5.90 -13 7 0 9.20 5.20 -13 7 0 14.50 3.90 -13 7 0 13.80 3.90 14 -7 0 153.78 13.20 -14 -7 0 163.48 13.80 14 -7 0 148.79 13.00 -14 -7 0 167.38 10.20 -14 -7 0 161.38 12.30 14 7 0 155.78 10.20 14 7 0 197.88 22.80 -14 7 0 152.08 9.90 -14 7 0 171.58 10.00 14 7 0 169.28 13.20 -14 7 0 140.89 12.00 -14 7 0 159.08 13.20 15 -7 0 148.19 13.30 -15 -7 0 142.29 9.80 -15 -7 0 128.69 13.80 15 -7 0 142.49 15.30 -15 -7 0 169.18 14.20 -15 7 0 144.19 13.20 15 7 0 137.19 10.00 -15 7 0 128.69 9.30 15 7 0 135.09 12.40 -15 7 0 158.58 10.10 15 7 0 133.89 14.20 -15 7 0 154.88 20.80 -16 -7 0 491.45 21.20 -16 -7 0 504.95 26.70 16 -7 0 498.15 25.90 16 -7 0 500.95 26.30 16 7 0 497.85 25.60 -16 7 0 507.95 21.30 -16 7 0 519.75 21.70 -16 7 0 532.05 26.30 16 7 0 448.96 24.40 16 7 0 534.85 22.00 17 -7 0 260.87 18.20 17 -7 0 243.98 18.30 -17 -7 0 251.57 14.10 -17 -7 0 206.48 18.00 -17 7 0 228.48 17.70 17 7 0 210.88 16.60 17 7 0 262.17 14.60 -17 7 0 246.38 13.90 -17 7 0 267.07 14.40 -18 -7 0 563.64 42.40 18 -7 0 484.85 28.10 18 -7 0 592.04 29.20 -18 -7 0 537.75 23.40 -18 7 0 556.54 23.90 -18 7 0 545.35 28.40 18 7 0 501.45 26.90 18 7 0 525.35 23.80 -18 7 0 563.04 23.80 -19 -7 0 14.40 5.30 19 -7 0 14.00 7.20 19 -7 0 14.30 6.60 -19 -7 0 35.50 10.80 -19 7 0 25.30 8.50 -19 7 0 10.90 5.10 19 7 0 20.00 6.10 19 7 0 27.80 8.40 -19 7 0 28.50 10.50 20 -7 0 109.49 15.00 -20 -7 0 100.39 10.90 -20 -7 0 121.59 16.60 -20 7 0 98.29 10.60 -20 7 0 105.19 11.50 -20 7 0 99.39 14.50 20 7 0 102.69 11.50 20 7 0 86.29 12.90 -21 -7 0 9.90 7.90 21 -7 0 22.30 8.80 -21 7 0 10.30 6.20 -21 7 0 21.30 9.40 21 7 0 17.00 8.10 -21 7 0 15.60 5.90 -22 -7 0 46.30 11.00 22 -7 0 36.70 10.00 -22 7 0 45.90 11.20 22 7 0 32.80 9.60 22 7 0 38.00 7.90 -22 7 0 39.50 8.10 -23 -7 0 15.10 8.40 23 -7 0 16.30 8.40 23 7 0 21.60 6.90 -23 7 0 19.10 9.80 23 7 0 23.30 8.70 -23 7 0 17.70 6.30 0 -8 0 31.10 3.50 0 -8 0 27.60 4.00 0 -8 0 28.00 2.80 0 -8 0 20.70 3.80 0 8 0 25.90 3.00 0 8 0 34.30 3.90 1 -8 0 3.80 1.60 1 -8 0 3.20 2.50 1 -8 0 5.30 2.70 -1 -8 0 3.70 2.40 -1 -8 0 3.30 1.20 -1 -8 0 2.90 1.90 1 -8 0 3.00 1.80 1 8 0 4.00 2.10 -1 8 0 4.00 2.00 1 8 0 4.40 1.40 -1 8 0 2.60 1.80 2 -8 0 55.69 4.00 2 -8 0 52.19 6.30 2 -8 0 49.20 4.20 -2 -8 0 65.29 5.00 -2 -8 0 51.69 6.00 2 8 0 58.99 5.80 -2 8 0 54.49 4.20 2 8 0 64.19 5.60 -2 8 0 54.89 4.70 3 -8 0 48.50 4.30 3 -8 0 47.10 3.80 -3 -8 0 49.70 5.20 3 -8 0 48.80 5.40 -3 -8 0 60.99 6.50 -3 8 0 44.50 5.60 -3 8 0 51.69 4.50 -3 8 0 51.29 5.40 3 8 0 46.50 5.20 3 8 0 54.79 5.90 -4 -8 0 202.18 11.60 -4 -8 0 207.98 11.00 4 -8 0 192.78 8.40 4 -8 0 194.58 9.60 4 -8 0 205.78 10.80 -4 8 0 209.48 10.80 4 8 0 203.48 10.80 4 8 0 193.78 12.00 -4 8 0 226.18 8.70 -4 8 0 200.28 10.20 -5 -8 0 16.70 3.80 -5 -8 0 36.20 8.30 5 -8 0 13.90 3.40 5 -8 0 12.10 3.70 5 -8 0 12.20 2.50 5 8 0 16.80 3.80 -5 8 0 15.30 4.20 -5 8 0 16.10 3.90 -5 8 0 17.50 2.80 5 8 0 11.80 3.90 6 -8 0 265.57 13.00 -6 -8 0 253.87 12.70 -6 -8 0 267.37 13.10 6 -8 0 243.48 10.00 -6 8 0 262.07 10.10 6 8 0 261.67 12.90 -6 8 0 246.08 12.70 -6 8 0 253.77 12.70 6 8 0 262.77 13.40 -6 8 0 239.18 9.80 6 8 0 238.28 8.50 -7 -8 0 29.90 5.70 7 -8 0 37.10 5.70 -7 -8 0 29.30 2.60 7 -8 0 39.80 6.20 -7 -8 0 37.10 6.10 7 8 0 39.50 5.40 -7 8 0 35.10 3.90 -7 8 0 32.10 3.50 -7 8 0 34.70 5.40 7 8 0 29.30 5.60 7 8 0 32.90 2.90 8 -8 0 33.70 5.30 -8 -8 0 25.60 2.90 8 -8 0 30.70 5.40 -8 -8 0 31.30 5.90 -8 -8 0 30.90 6.00 -8 8 0 30.50 3.80 8 8 0 29.90 3.30 8 8 0 32.20 5.20 -8 8 0 33.60 5.70 8 8 0 24.30 5.70 -8 8 0 25.60 4.70 -8 8 0 34.30 3.80 9 -8 0 59.19 7.60 -9 -8 0 63.99 8.00 9 -8 0 61.59 8.20 -9 -8 0 52.59 4.30 -9 -8 0 61.69 7.60 -9 8 0 58.09 4.70 9 8 0 66.69 8.90 -9 8 0 44.80 6.40 9 8 0 54.89 7.00 -9 8 0 58.89 4.90 -9 8 0 61.49 7.90 9 8 0 58.89 4.70 -10 -8 0 132.89 7.30 -10 -8 0 139.89 10.60 -10 -8 0 141.09 11.10 10 -8 0 152.38 11.20 10 -8 0 156.38 11.10 10 8 0 138.09 7.60 -10 8 0 132.29 10.50 -10 8 0 142.59 7.90 -10 8 0 164.18 8.00 10 8 0 130.19 11.20 10 8 0 147.09 10.50 -10 8 0 161.78 11.20 -11 -8 0 53.39 5.30 11 -8 0 44.30 7.70 -11 -8 0 38.30 7.00 -11 -8 0 61.89 8.60 11 -8 0 46.60 7.50 11 8 0 56.79 5.80 11 8 0 43.40 7.80 -11 8 0 45.60 7.80 -11 8 0 58.59 5.90 -11 8 0 50.59 5.40 -11 8 0 60.99 9.10 11 8 0 57.29 7.90 -12 -8 0 175.28 13.20 12 -8 0 166.08 12.90 -12 -8 0 182.78 9.40 -12 -8 0 187.78 19.70 12 8 0 173.08 9.50 -12 8 0 177.08 13.20 12 8 0 158.08 12.10 12 8 0 216.08 14.40 -12 8 0 169.28 12.80 -12 8 0 184.18 10.70 -12 8 0 163.28 9.80 -13 -8 0 3.80 4.50 -13 -8 0 3.80 3.40 13 -8 0 6.80 5.40 13 -8 0 5.10 3.70 -13 -8 0 9.20 4.60 -13 8 0 2.40 3.20 -13 8 0 8.40 3.40 -13 8 0 6.30 5.30 -13 8 0 15.60 5.80 13 8 0 13.20 6.20 13 8 0 8.00 4.80 13 8 0 3.70 3.20 14 -8 0 6.90 5.50 14 -8 0 -2.40 4.30 -14 -8 0 10.20 4.50 -14 -8 0 16.10 5.00 -14 -8 0 7.30 5.60 -14 8 0 0.70 2.90 14 8 0 7.20 4.50 -14 8 0 2.80 3.00 -14 8 0 4.40 4.10 14 8 0 -6.20 3.80 14 8 0 10.80 3.90 -14 8 0 5.30 4.70 -15 -8 0 9.50 3.80 15 -8 0 7.90 7.10 15 -8 0 16.20 6.20 -15 -8 0 11.30 5.70 15 8 0 10.00 4.20 -15 8 0 5.70 3.30 -15 8 0 -0.60 4.40 15 8 0 6.20 4.90 -15 8 0 6.40 3.70 16 -8 0 19.30 7.00 16 -8 0 3.10 5.20 -16 -8 0 6.60 6.30 -16 -8 0 9.40 3.80 -16 8 0 8.50 4.10 -16 8 0 1.80 3.70 -16 8 0 1.80 5.00 16 8 0 10.30 6.50 16 8 0 12.50 4.60 -17 -8 0 40.10 8.80 17 -8 0 38.70 9.30 17 -8 0 56.79 11.20 -17 -8 0 33.40 6.20 -17 8 0 23.20 6.00 -17 8 0 34.20 6.40 -17 8 0 46.60 10.40 17 8 0 35.40 6.50 17 8 0 46.60 9.60 -18 -8 0 66.49 8.20 -18 -8 0 63.79 11.80 18 -8 0 71.29 11.30 18 -8 0 50.59 10.20 -18 8 0 39.50 8.90 18 8 0 62.79 8.60 -18 8 0 60.89 8.30 18 8 0 48.00 10.00 -18 8 0 59.89 8.20 -19 -8 0 8.60 5.40 19 -8 0 -1.50 4.40 19 -8 0 12.00 7.20 -19 -8 0 -3.80 6.40 -19 8 0 -4.20 4.10 -19 8 0 9.00 7.20 19 8 0 1.80 6.10 19 8 0 -4.20 4.40 -19 8 0 5.10 4.70 20 -8 0 24.40 8.40 -20 -8 0 19.40 5.60 -20 -8 0 28.10 9.70 20 8 0 17.30 5.90 -20 8 0 28.90 6.90 20 8 0 20.70 8.00 -20 8 0 28.40 9.80 -20 8 0 18.30 5.50 21 -8 0 87.19 13.80 -21 -8 0 79.69 15.20 -21 8 0 78.59 10.30 21 8 0 68.99 10.10 21 8 0 60.59 10.90 -21 8 0 56.89 14.70 -21 8 0 81.19 9.80 22 -8 0 0.40 7.90 -22 -8 0 20.10 8.70 22 8 0 3.10 4.50 -22 8 0 19.10 8.50 -22 8 0 9.80 6.00 22 8 0 -3.30 4.90 23 -8 0 61.99 12.30 -23 -8 0 53.49 12.80 23 8 0 43.70 8.70 23 8 0 48.80 11.00 -23 8 0 62.79 9.30 -23 8 0 58.99 12.20 0 -9 0 -0.20 1.30 0 -9 0 -1.20 2.30 0 -9 0 -2.20 1.90 0 -9 0 0.40 1.70 0 9 0 -1.80 1.80 0 9 0 1.60 1.70 1 -9 0 223.08 11.60 -1 -9 0 223.08 11.60 -1 -9 0 212.68 10.00 1 -9 0 223.68 8.90 -1 -9 0 211.98 7.90 -1 -9 0 205.98 11.00 1 -9 0 234.98 9.60 1 -9 0 218.58 11.20 -1 9 0 216.68 9.50 1 9 0 221.88 10.40 1 9 0 207.88 8.30 -1 9 0 236.78 9.90 -2 -9 0 39.30 2.50 2 -9 0 51.79 4.70 2 -9 0 66.59 7.80 -2 -9 0 37.20 4.60 2 -9 0 41.80 5.10 -2 -9 0 47.10 6.20 2 -9 0 44.00 3.90 -2 9 0 41.50 4.70 -2 9 0 49.10 4.20 2 9 0 41.70 5.30 2 9 0 49.40 5.60 -3 -9 0 30.10 4.30 3 -9 0 29.50 3.50 3 -9 0 28.40 3.80 3 -9 0 36.10 5.30 3 9 0 26.90 4.90 -3 9 0 28.30 4.40 3 9 0 36.50 5.30 -3 9 0 35.40 3.90 -3 9 0 33.70 5.50 -4 -9 0 -3.80 2.30 4 -9 0 0.60 2.30 4 -9 0 3.70 2.40 -4 -9 0 -0.20 2.00 4 -9 0 1.80 1.70 -4 9 0 -0.20 2.10 4 9 0 -0.60 2.70 -4 9 0 -1.20 2.50 4 9 0 -2.30 2.10 -4 9 0 -0.50 1.60 5 -9 0 1.40 1.70 5 -9 0 -2.20 2.10 -5 -9 0 4.90 2.70 5 -9 0 0.80 2.30 -5 -9 0 2.10 2.70 -5 9 0 -0.90 2.20 -5 9 0 5.20 2.00 5 9 0 2.50 3.20 5 9 0 -3.40 2.20 6 -9 0 14.10 2.70 6 -9 0 4.70 3.30 -6 -9 0 7.60 3.40 6 -9 0 11.80 3.90 -6 -9 0 13.00 4.10 -6 9 0 10.20 2.60 -6 9 0 6.90 3.70 6 9 0 10.40 3.40 -6 9 0 8.30 3.80 6 9 0 14.80 4.50 -7 -9 0 78.89 8.70 7 -9 0 76.49 8.20 -7 -9 0 89.29 8.10 7 -9 0 85.19 9.10 -7 9 0 63.79 6.80 7 9 0 105.79 10.50 -7 9 0 82.59 8.70 -7 9 0 71.39 4.90 -7 9 0 62.59 4.80 7 9 0 72.79 8.40 -8 -9 0 5.50 3.50 -8 -9 0 7.30 1.70 8 -9 0 7.20 4.00 -8 -9 0 10.60 4.30 8 -9 0 7.20 4.20 -8 9 0 8.10 3.50 8 9 0 12.10 4.30 8 9 0 6.50 4.30 8 9 0 7.60 1.90 -8 9 0 10.10 2.70 -8 9 0 11.20 2.70 -8 9 0 3.30 3.70 -9 -9 0 213.38 8.70 -9 -9 0 223.78 13.40 -9 -9 0 235.28 13.90 9 -9 0 241.98 13.80 9 -9 0 229.98 13.60 -9 9 0 224.28 9.90 -9 9 0 238.38 13.60 -9 9 0 226.48 10.00 9 9 0 212.58 9.00 9 9 0 229.68 14.30 -9 9 0 214.98 13.30 9 9 0 236.08 13.30 10 -9 0 9.50 5.30 10 -9 0 4.90 4.60 -10 -9 0 6.00 4.10 -10 -9 0 4.40 2.10 -10 -9 0 7.40 4.60 -10 9 0 4.10 3.60 -10 9 0 7.00 2.60 10 9 0 6.30 3.90 10 9 0 0.10 4.10 10 9 0 5.30 2.50 -10 9 0 5.20 4.30 -10 9 0 6.20 2.70 11 -9 0 44.00 6.80 -11 -9 0 55.69 9.50 -11 -9 0 55.29 5.20 11 -9 0 43.40 8.00 11 9 0 40.00 7.00 11 9 0 53.69 9.00 -11 9 0 58.29 5.90 -11 9 0 56.49 5.60 -11 9 0 42.10 7.50 -11 9 0 52.19 8.60 11 9 0 42.30 4.80 12 -9 0 15.10 6.00 -12 -9 0 6.30 2.90 -12 -9 0 5.40 4.60 12 -9 0 1.40 4.00 -12 -9 0 9.30 4.40 12 9 0 4.40 2.90 12 9 0 12.60 5.60 -12 9 0 11.70 5.30 -12 9 0 10.30 3.60 -12 9 0 9.30 3.60 12 9 0 1.40 4.70 -12 9 0 20.10 5.50 -13 -9 0 142.19 12.80 13 -9 0 148.09 12.80 13 -9 0 134.29 12.00 -13 -9 0 124.09 11.00 -13 -9 0 122.69 7.80 -13 9 0 135.49 8.50 13 9 0 107.69 7.90 13 9 0 125.79 13.40 -13 9 0 134.59 8.30 -13 9 0 116.89 12.20 13 9 0 143.19 14.70 -13 9 0 140.19 12.10 14 -9 0 179.68 14.20 -14 -9 0 181.58 10.20 -14 -9 0 192.38 15.30 14 -9 0 144.79 15.10 14 9 0 183.98 13.90 -14 9 0 185.88 10.30 -14 9 0 177.08 10.40 14 9 0 179.68 14.60 14 9 0 166.38 12.80 -14 9 0 173.08 14.00 -15 -9 0 202.48 11.20 15 -9 0 216.98 16.10 15 -9 0 213.98 16.00 -15 -9 0 172.68 15.60 -15 9 0 179.28 10.80 -15 9 0 180.78 14.70 -15 9 0 181.38 11.10 15 9 0 191.98 15.40 15 9 0 215.08 19.20 15 9 0 207.48 11.50 -16 -9 0 650.13 31.30 16 -9 0 662.43 31.20 16 -9 0 580.94 30.00 -16 -9 0 614.44 24.30 16 9 0 639.74 24.70 -16 9 0 606.34 29.60 -16 9 0 608.54 24.40 -16 9 0 625.34 24.60 16 9 0 659.93 30.40 -17 -9 0 101.79 13.60 17 -9 0 117.89 22.10 -17 -9 0 109.89 9.20 17 -9 0 88.59 12.80 -17 9 0 126.89 9.80 -17 9 0 93.69 12.50 17 9 0 122.79 9.90 17 9 0 91.39 12.50 -17 9 0 112.19 9.70 -18 -9 0 674.53 26.90 -18 -9 0 690.53 34.40 18 -9 0 685.13 33.50 18 -9 0 669.33 34.10 18 9 0 667.33 27.30 -18 9 0 636.94 32.50 -18 9 0 687.23 27.40 -18 9 0 695.33 27.60 18 9 0 735.03 33.50 19 -9 0 11.80 7.40 -19 -9 0 0.00 3.50 -19 -9 0 16.10 7.20 19 -9 0 17.00 7.90 -19 9 0 8.50 5.10 -19 9 0 -0.40 5.30 -19 9 0 8.90 5.10 19 9 0 6.50 4.60 19 9 0 13.90 7.70 -20 -9 0 180.28 19.40 -20 -9 0 195.48 12.90 20 -9 0 176.98 19.50 -20 9 0 188.08 13.20 -20 9 0 215.48 18.20 20 9 0 186.18 13.00 20 9 0 199.18 17.00 -20 9 0 159.68 12.30 21 -9 0 43.00 10.80 -21 -9 0 33.50 11.50 -21 -9 0 38.50 7.10 21 9 0 26.80 6.40 21 9 0 28.60 9.30 -21 9 0 36.80 7.10 -21 9 0 30.20 15.40 -21 9 0 41.80 7.60 -22 -9 0 2.20 6.60 22 -9 0 -10.60 5.40 -22 9 0 -2.10 4.60 22 9 0 -2.10 5.70 22 9 0 -1.20 5.00 -23 -9 0 23.70 9.10 23 -9 0 26.30 9.30 23 9 0 35.00 9.40 -23 9 0 28.10 9.70 -23 9 0 29.60 7.20 23 9 0 11.60 5.80 0 -10 0 132.89 8.80 0 -10 0 133.89 6.20 0 -10 0 139.49 9.60 0 -10 0 149.49 7.70 0 10 0 131.99 6.80 0 10 0 135.09 7.80 1 -10 0 6.40 2.40 -1 -10 0 7.00 3.30 -1 -10 0 3.70 2.80 -1 -10 0 5.80 1.60 1 -10 0 6.80 2.00 -1 -10 0 4.70 3.70 1 -10 0 9.20 3.30 1 10 0 4.60 1.90 -1 10 0 8.40 2.50 1 10 0 6.80 2.80 -1 10 0 7.70 2.60 -2 -10 0 57.49 7.40 2 -10 0 53.69 6.70 2 -10 0 52.89 4.40 2 -10 0 60.09 4.70 -2 -10 0 44.10 2.80 -2 -10 0 44.60 5.30 2 -10 0 56.29 10.20 -2 10 0 64.89 4.90 -2 10 0 55.39 5.50 -3 -10 0 7.10 3.00 3 -10 0 7.30 2.30 3 -10 0 10.80 3.90 -3 -10 0 7.90 4.00 3 -10 0 6.90 2.70 3 10 0 7.40 3.40 -3 10 0 8.60 2.60 -3 10 0 7.40 3.20 3 10 0 5.90 3.30 -4 -10 0 7.20 3.00 -4 -10 0 3.00 3.40 4 -10 0 3.80 2.50 4 -10 0 5.90 2.10 4 -10 0 4.60 3.30 4 10 0 4.30 3.30 4 10 0 9.60 3.80 -4 10 0 9.70 3.30 -4 10 0 5.30 2.10 -4 10 0 6.40 3.30 5 -10 0 7.10 3.60 5 -10 0 6.60 2.20 -5 -10 0 2.20 2.70 -5 -10 0 9.00 3.70 5 -10 0 -0.60 3.20 5 10 0 2.40 3.40 5 10 0 5.60 3.10 -5 10 0 4.50 2.20 -5 10 0 5.10 3.00 -5 10 0 0.60 3.20 -6 -10 0 10.60 3.50 6 -10 0 0.80 2.90 -6 -10 0 7.40 4.20 6 -10 0 1.60 1.90 6 -10 0 5.80 3.60 -6 10 0 5.40 3.20 -6 10 0 3.40 2.10 6 10 0 7.30 4.10 6 10 0 4.20 2.80 7 -10 0 26.80 5.50 -7 -10 0 30.40 5.70 -7 -10 0 25.30 5.80 7 -10 0 26.90 5.20 -7 10 0 36.90 6.40 -7 10 0 32.70 4.00 7 10 0 29.70 5.50 -7 10 0 31.30 3.90 7 10 0 28.30 6.10 -7 10 0 30.30 6.00 8 -10 0 71.09 8.10 -8 -10 0 87.59 9.80 8 -10 0 78.29 8.60 -8 -10 0 82.59 9.30 -8 10 0 66.39 5.10 8 10 0 78.89 9.00 -8 10 0 75.89 8.90 -8 10 0 66.19 8.80 8 10 0 69.39 9.40 -8 10 0 74.59 5.40 9 -10 0 119.99 10.10 9 -10 0 115.89 11.40 -9 -10 0 105.09 5.00 -9 -10 0 109.69 10.10 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97.29 12.20 -13 10 0 110.69 7.60 13 10 0 86.49 10.50 13 10 0 102.59 7.00 -13 10 0 98.79 10.80 -13 10 0 101.49 7.30 -14 -10 0 109.59 13.70 14 -10 0 102.29 12.40 -14 -10 0 99.39 11.30 14 -10 0 109.89 19.10 14 10 0 113.49 7.80 -14 10 0 110.09 8.10 14 10 0 88.99 11.20 14 10 0 103.39 12.40 -14 10 0 97.69 7.70 -14 10 0 111.19 13.20 -15 -10 0 809.12 28.90 -15 -10 0 816.62 36.40 15 -10 0 861.91 36.40 15 -10 0 765.92 35.30 15 10 0 845.62 29.40 -15 10 0 844.62 35.50 -15 10 0 826.22 29.60 -15 10 0 860.61 29.80 15 10 0 750.02 35.00 16 -10 0 226.18 17.60 -16 -10 0 231.88 19.60 16 -10 0 228.38 17.90 -16 -10 0 239.78 12.40 -16 10 0 224.88 12.70 16 10 0 224.48 12.60 -16 10 0 237.98 12.80 -16 10 0 242.78 17.70 16 10 0 190.18 16.50 -17 -10 0 1297.07 53.29 17 -10 0 1396.36 53.59 17 -10 0 1352.06 55.89 -17 -10 0 1267.77 44.80 17 10 0 1359.06 52.39 -17 10 0 1263.07 51.69 -17 10 0 1343.07 45.70 17 10 0 1357.76 45.30 -17 10 0 1450.25 46.10 18 -10 0 110.79 15.00 18 -10 0 117.09 14.80 -18 -10 0 136.19 10.20 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12.90 6 12 0 181.48 13.00 -6 12 0 191.38 9.50 -7 -12 0 79.09 9.20 7 -12 0 79.39 5.90 7 -12 0 66.29 9.20 7 -12 0 69.29 8.20 -7 -12 0 84.69 10.20 7 12 0 71.69 9.80 -7 12 0 91.89 11.10 -7 12 0 66.49 8.70 7 12 0 84.29 10.00 -7 12 0 84.19 6.20 -8 -12 0 6.70 4.70 8 -12 0 5.60 3.90 -8 -12 0 5.10 4.30 8 -12 0 2.50 3.80 8 12 0 2.50 3.60 -8 12 0 10.80 4.80 -8 12 0 4.80 2.50 -8 12 0 7.70 2.60 8 12 0 1.60 4.70 -8 12 0 7.40 4.10 9 -12 0 55.49 9.50 -9 -12 0 66.39 9.00 -9 -12 0 55.69 9.20 9 -12 0 67.39 8.70 -9 12 0 55.79 8.50 -9 12 0 60.39 5.70 9 12 0 55.39 9.50 -9 12 0 61.39 9.00 9 12 0 54.29 9.20 -9 12 0 56.59 5.00 10 -12 0 109.89 11.30 10 -12 0 105.79 12.90 -10 -12 0 114.99 13.20 -10 -12 0 85.89 10.20 10 12 0 87.19 11.50 -10 12 0 96.79 10.50 -10 12 0 94.09 14.50 10 12 0 117.59 10.40 -10 12 0 102.19 6.60 -10 12 0 106.19 7.00 -11 -12 0 65.09 9.70 11 -12 0 90.29 11.10 -11 -12 0 98.19 15.90 11 -12 0 60.99 9.30 -11 12 0 85.59 7.10 -11 12 0 72.99 10.10 -11 12 0 62.99 9.60 11 12 0 74.59 11.20 11 12 0 70.49 9.50 12 -12 0 27.10 6.30 -12 -12 0 40.10 8.30 12 -12 0 32.00 7.30 -12 12 0 34.40 7.30 12 12 0 41.90 9.10 -12 12 0 34.70 6.60 -12 12 0 52.89 5.80 12 12 0 37.50 8.80 -12 12 0 41.10 5.10 13 -12 0 71.09 10.90 -13 -12 0 66.19 10.90 -13 -12 0 63.49 4.90 13 12 0 58.99 10.30 -13 12 0 83.59 7.00 13 12 0 69.29 5.20 -13 12 0 64.99 9.30 -13 12 0 79.19 6.90 14 -12 0 34.30 8.80 14 -12 0 13.60 7.00 -14 -12 0 28.70 10.80 -14 -12 0 29.30 3.80 14 12 0 17.80 7.50 14 12 0 29.80 4.10 -14 12 0 27.30 8.10 -14 12 0 19.20 4.50 -14 12 0 27.60 4.90 15 -12 0 19.70 8.00 -15 -12 0 18.10 8.80 15 -12 0 27.50 7.90 -15 -12 0 26.70 4.40 15 12 0 20.00 4.30 -15 12 0 27.90 5.10 -15 12 0 25.30 8.20 -15 12 0 27.10 5.20 15 12 0 21.40 8.30 16 -12 0 80.79 12.90 16 -12 0 76.09 13.10 -16 -12 0 82.19 14.40 -16 12 0 89.09 8.60 16 12 0 104.69 7.70 16 12 0 91.49 12.70 -16 12 0 85.59 11.90 -16 12 0 100.09 8.40 17 -12 0 169.08 18.70 -17 -12 0 145.99 16.50 17 -12 0 157.68 17.00 17 12 0 156.88 10.00 -17 12 0 169.18 10.80 -17 12 0 158.38 10.80 17 12 0 146.39 16.60 -17 12 0 185.78 19.70 18 -12 0 25.60 9.10 18 -12 0 19.40 8.60 -18 -12 0 32.30 10.20 -18 -12 0 13.50 4.00 -18 12 0 20.20 5.30 18 12 0 24.40 8.60 -18 12 0 17.30 4.80 18 12 0 12.20 4.30 -18 12 0 14.60 6.80 19 -12 0 61.69 12.00 -19 -12 0 94.99 8.70 -19 -12 0 64.59 11.90 19 12 0 87.09 8.60 -19 12 0 81.19 8.80 -19 12 0 74.49 8.60 -19 12 0 74.79 13.20 19 12 0 73.09 12.40 20 -12 0 -2.50 6.30 -20 -12 0 14.60 4.70 -20 -12 0 5.10 6.70 -20 12 0 7.70 4.40 20 12 0 10.20 4.40 20 12 0 -2.20 5.90 -20 12 0 11.80 7.30 -20 12 0 11.30 7.00 21 -12 0 21.10 9.40 -21 -12 0 10.80 7.60 21 12 0 12.80 4.90 21 12 0 -0.90 6.80 -21 12 0 22.20 8.60 -21 12 0 24.80 5.70 0 -13 0 -3.60 1.80 0 -13 0 -0.60 3.30 0 -13 0 -2.80 2.20 0 -13 0 0.70 4.10 0 13 0 -4.00 2.10 0 13 0 3.10 3.10 -1 -13 0 48.00 7.70 -1 -13 0 39.90 5.70 1 -13 0 61.89 9.40 -1 -13 0 45.10 3.60 -1 -13 0 42.50 7.70 1 -13 0 48.80 7.50 1 -13 0 44.20 4.60 1 13 0 43.20 6.60 1 13 0 41.50 4.20 -1 13 0 46.60 6.10 -1 13 0 41.80 5.10 2 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28.00 9.60 20 -13 0 28.30 9.70 -20 13 0 41.50 6.60 20 13 0 40.90 10.70 -20 13 0 32.80 7.30 20 13 0 33.20 5.80 0 -14 0 79.49 5.30 0 -14 0 91.19 9.80 0 -14 0 70.49 7.30 0 -14 0 75.09 8.60 0 14 0 77.09 8.50 0 14 0 80.29 6.10 1 -14 0 9.00 5.70 -1 -14 0 7.60 5.10 -1 -14 0 11.20 4.70 1 -14 0 3.10 2.50 1 -14 0 10.00 3.50 -1 -14 0 5.60 3.30 -1 -14 0 3.50 2.10 1 -14 0 8.10 4.40 -1 14 0 12.90 3.80 1 14 0 0.40 2.30 1 14 0 8.30 4.30 -1 14 0 8.30 4.00 2 -14 0 0.60 2.40 2 -14 0 -0.60 5.00 -2 -14 0 0.20 4.30 -2 -14 0 -0.20 3.20 -2 -14 0 -1.10 2.80 2 -14 0 3.40 3.90 2 -14 0 -1.40 2.30 -2 14 0 1.10 3.00 -2 14 0 1.60 2.90 2 14 0 -1.40 3.80 3 -14 0 7.80 5.20 -3 -14 0 0.80 4.70 -3 -14 0 2.00 3.10 3 -14 0 0.30 3.70 3 -14 0 3.80 4.10 -3 -14 0 -0.80 2.70 -3 14 0 -1.60 2.60 -3 14 0 -3.20 2.90 3 14 0 -3.90 3.70 4 -14 0 284.17 16.60 4 -14 0 242.58 12.30 -4 -14 0 283.67 16.30 4 -14 0 261.57 12.70 4 -14 0 257.17 15.40 -4 -14 0 237.78 13.60 -4 14 0 238.78 12.20 4 14 0 265.37 15.30 5 -14 0 114.79 8.90 5 -14 0 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47.40 7.70 -12 11 3 49.50 8.10 12 11 -3 54.09 11.50 12 11 -3 59.09 9.70 -12 11 3 59.69 4.70 12 11 -3 54.49 5.60 -12 11 3 50.09 4.40 -11 -11 3 1031.20 38.40 -11 -11 3 916.31 36.30 11 -11 -3 990.50 37.10 11 -11 -3 941.81 36.90 11 11 -3 920.21 30.60 11 11 -3 960.30 37.40 11 11 -3 904.51 36.40 11 11 -3 871.81 29.80 -11 11 3 1002.80 36.70 -11 11 3 935.41 29.50 -11 11 3 942.51 36.20 -11 11 3 911.71 29.50 10 -11 -3 29.70 6.40 10 -11 -3 23.00 6.50 -10 -11 3 19.40 6.40 -10 -11 3 22.10 5.30 -10 11 3 27.10 6.40 10 11 -3 22.10 3.70 10 11 -3 25.30 6.90 -10 11 3 20.70 5.40 -10 11 3 22.10 3.00 -10 11 3 19.00 3.00 10 11 -3 23.80 6.00 10 11 -3 20.40 3.10 -9 -11 3 1889.01 62.09 9 -11 -3 1828.22 60.49 9 -11 -3 1861.11 61.29 -9 -11 3 1801.32 61.19 9 11 -3 1749.82 60.89 9 11 -3 1805.32 54.79 9 11 -3 1777.92 54.19 9 11 -3 1865.91 61.69 -9 11 3 1860.31 60.89 -9 11 3 1797.62 54.19 -9 11 3 1764.02 60.29 -9 11 3 1856.71 54.19 8 -11 -3 36.10 6.20 -8 -11 3 28.30 5.70 8 -11 -3 44.00 8.00 -8 -11 3 38.40 7.40 8 11 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2.20 5.00 -10 -16 3 4.20 7.20 -10 16 3 4.30 2.40 -10 16 3 7.70 4.80 -10 16 3 5.80 4.60 -10 16 3 11.60 3.10 10 16 -3 -0.10 5.40 -9 -16 3 23.10 8.00 9 -16 -3 17.20 5.80 9 -16 -3 38.30 8.30 -9 16 3 14.10 5.40 -9 16 3 30.20 4.40 9 16 -3 25.50 7.90 -9 16 3 23.50 7.30 -9 16 3 26.40 3.70 8 -16 -3 18.00 5.60 8 -16 -3 19.60 7.30 -8 -16 3 12.10 6.30 -8 16 3 5.60 4.10 -8 16 3 12.60 3.50 -8 16 3 8.60 2.70 8 16 -3 19.40 7.50 7 -16 -3 2.10 3.90 7 -16 -3 14.10 6.20 7 -16 -3 19.90 3.70 -7 -16 3 13.00 5.70 -7 16 3 11.40 3.60 7 16 -3 12.80 5.20 -7 16 3 11.60 4.80 6 -16 -3 135.69 12.60 -6 -16 3 154.58 14.20 6 -16 -3 152.08 13.70 6 -16 -3 152.48 10.40 6 16 -3 119.69 12.70 -6 16 3 140.79 10.40 -6 16 3 139.49 9.00 -5 -16 3 7.40 5.90 -5 -16 3 -1.20 3.50 5 -16 -3 1.80 3.40 5 -16 -3 0.50 4.90 5 -16 -3 9.90 5.40 5 -16 -3 8.70 2.90 -5 16 3 -0.50 3.00 5 16 -3 1.90 4.60 -4 -16 3 406.26 21.20 4 -16 -3 368.76 16.90 -4 -16 3 382.56 21.60 4 -16 -3 398.66 21.40 -4 -16 3 375.26 18.70 4 -16 -3 385.76 16.10 4 -16 -3 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1 -16 3 11.40 3.70 1 -16 3 3.80 5.00 -1 -16 -3 16.60 4.40 -1 -16 -3 27.40 6.90 1 -16 3 18.70 4.90 -1 16 -3 13.30 5.00 1 16 3 15.20 5.60 -1 16 -3 17.90 5.00 2 -16 3 129.79 9.30 2 -16 3 149.88 12.50 -2 -16 -3 130.29 9.70 -2 -16 -3 134.09 12.30 2 -16 3 98.79 12.10 -2 -16 -3 133.29 11.40 2 -16 3 129.59 8.80 -2 16 -3 125.99 9.60 -2 16 -3 129.69 10.00 2 16 3 142.69 13.30 3 -16 3 13.50 6.10 -3 -16 -3 8.20 5.00 3 -16 3 3.90 3.70 -3 -16 -3 1.20 3.40 3 -16 3 5.00 3.50 -3 -16 -3 6.40 5.00 3 -16 3 14.30 6.30 -3 16 -3 5.20 3.90 3 16 3 5.10 4.60 -3 16 -3 4.30 4.10 4 -16 3 76.49 8.10 -4 -16 -3 84.99 9.60 4 -16 3 92.99 13.50 4 -16 3 75.69 10.60 -4 -16 -3 57.79 10.50 -4 -16 -3 75.39 10.00 4 -16 3 85.69 8.50 -4 16 -3 77.99 8.50 4 16 3 63.19 9.60 -4 16 -3 93.19 10.10 5 -16 3 1.40 3.70 5 -16 3 8.20 6.10 5 -16 3 2.40 3.20 5 -16 3 4.10 4.10 -5 -16 -3 10.40 4.80 -5 -16 -3 21.40 7.10 -5 16 -3 8.90 4.90 -5 16 -3 18.00 4.70 5 16 3 -2.00 4.30 6 -16 3 5.60 3.50 6 -16 3 -2.70 4.50 -6 -16 -3 3.50 5.60 -6 -16 -3 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60.69 9.30 10 9 -4 37.30 6.50 -10 9 4 42.10 3.30 10 9 -4 39.90 5.10 -10 9 4 43.80 3.50 10 9 -4 36.80 6.80 -10 9 4 48.10 7.80 -10 9 4 50.69 7.40 9 -9 -4 479.15 20.50 9 -9 -4 432.46 19.70 -9 -9 4 388.96 15.20 -9 -9 4 429.36 20.30 -9 -9 4 388.86 18.80 -9 9 4 413.66 18.90 9 9 -4 393.36 15.50 -9 9 4 416.46 13.70 -9 9 4 431.66 19.30 -9 9 4 407.26 13.50 9 9 -4 419.56 19.70 8 -9 -4 209.78 12.50 8 -9 -4 206.38 12.40 -8 -9 4 210.68 13.20 -8 -9 4 237.18 12.60 8 9 -4 204.38 8.80 8 9 -4 215.18 9.10 -8 9 4 194.38 11.60 8 9 -4 197.78 12.20 -8 9 4 201.78 12.00 -8 9 4 215.78 7.60 -7 -9 4 16.30 5.20 -7 -9 4 13.90 3.90 7 9 -4 16.50 2.60 -7 9 4 17.80 4.50 7 9 -4 12.50 2.50 7 9 -4 13.60 4.40 7 9 -4 10.50 3.70 6 -9 -4 15.70 3.70 -6 -9 4 10.40 4.20 -6 -9 4 8.90 3.40 6 -9 -4 6.60 3.50 6 -9 -4 9.50 1.60 6 9 -4 6.70 3.40 6 9 -4 7.60 2.10 6 9 -4 5.00 3.50 -6 9 4 7.50 1.80 -6 9 4 2.80 3.00 6 9 -4 10.20 2.10 -6 9 4 7.60 3.40 5 -9 -4 82.69 6.80 -5 -9 4 71.69 7.40 5 -9 -4 64.79 6.80 -5 -9 4 68.29 8.50 5 -9 -4 63.19 3.50 5 9 -4 63.69 7.40 5 9 -4 70.09 4.20 -5 9 4 66.29 3.90 -5 9 4 62.99 6.30 5 9 -4 65.59 7.10 5 9 -4 65.09 4.20 -5 9 4 60.29 6.50 -4 -9 4 78.69 6.80 -4 -9 4 82.59 7.50 4 -9 -4 83.39 6.50 4 -9 -4 85.19 4.30 4 -9 -4 78.19 6.70 4 9 -4 93.99 5.00 4 9 -4 94.39 7.60 -4 9 4 81.69 4.90 -4 9 4 87.79 6.70 4 9 -4 98.79 5.10 4 9 -4 80.99 7.70 -4 9 4 75.19 5.80 -3 -9 4 32.80 3.50 3 -9 -4 42.50 4.70 3 -9 -4 33.70 3.30 -3 -9 4 37.10 5.90 -3 -9 4 32.60 5.30 3 -9 -4 32.40 4.60 3 9 -4 28.20 4.80 3 9 -4 35.90 3.60 -3 9 4 40.00 4.10 3 9 -4 24.30 4.50 -3 9 4 40.10 4.30 2 -9 -4 11.30 2.30 2 -9 -4 10.80 2.70 -2 -9 4 11.50 3.40 -2 -9 4 11.60 2.50 -2 -9 4 11.70 3.70 -2 9 4 7.20 2.30 2 9 -4 12.70 2.50 2 9 -4 8.30 3.20 2 9 -4 12.00 3.70 -2 9 4 9.70 2.70 -1 -9 4 631.24 21.80 -1 -9 4 650.63 24.70 1 -9 -4 626.64 23.50 1 -9 -4 691.23 24.20 1 -9 -4 654.03 21.70 1 -9 -4 673.03 21.20 -1 -9 4 634.64 23.20 -1 -9 4 663.23 25.20 1 9 -4 632.14 21.70 -1 9 4 639.24 20.70 -1 9 4 691.83 23.00 0 -9 -4 864.11 29.70 0 -9 4 844.12 29.00 0 -9 -4 823.22 25.90 0 -9 -4 835.22 27.80 0 -9 4 836.72 30.90 0 -9 4 853.91 30.50 0 -9 4 888.51 28.10 0 -9 -4 830.92 29.20 0 9 4 875.51 29.20 0 9 4 859.41 25.70 0 9 -4 865.21 28.90 0 9 -4 840.32 27.80 -1 -9 -4 764.32 27.00 -1 -9 -4 723.63 25.60 1 -9 4 725.53 27.70 1 -9 4 785.22 25.80 1 -9 4 741.83 28.30 -1 9 -4 775.82 25.60 -1 9 -4 780.62 26.20 1 9 4 760.92 27.10 2 -9 4 1870.81 60.79 -2 -9 -4 1823.92 58.49 -2 -9 -4 1900.91 59.29 2 -9 4 1952.00 58.39 2 9 4 1840.22 59.79 -2 9 -4 1932.81 58.29 -2 9 -4 1920.11 58.39 3 -9 4 308.77 16.00 -3 -9 -4 345.47 15.00 3 -9 4 352.76 16.00 -3 -9 -4 369.96 15.20 3 -9 4 323.77 14.20 -3 9 -4 336.87 15.80 -3 9 -4 348.17 15.90 3 9 4 328.27 14.40 -3 9 -4 351.26 14.10 4 -9 4 402.36 16.40 4 -9 4 376.36 17.30 -4 -9 -4 396.46 16.70 -4 9 -4 390.16 16.30 4 9 4 403.36 18.10 -4 9 -4 404.46 15.70 -4 9 -4 395.06 17.70 4 9 4 381.66 16.10 -5 -9 -4 20.90 4.30 5 -9 4 16.70 3.50 -5 -9 -4 17.40 4.20 5 -9 4 18.20 4.80 5 -9 4 16.50 4.10 -5 9 -4 17.30 4.70 -5 9 -4 17.20 4.00 -5 9 -4 17.10 3.60 5 9 4 23.90 4.20 5 9 4 15.60 4.80 6 -9 4 17.70 3.50 6 -9 4 17.80 4.90 -6 -9 -4 18.80 4.60 6 -9 4 17.90 4.30 -6 -9 -4 23.10 4.80 6 9 4 16.00 5.20 -6 9 -4 19.90 5.10 -6 9 -4 17.60 4.20 -6 9 -4 13.60 4.00 6 9 4 20.70 4.20 7 -9 4 16.40 4.60 7 -9 4 25.00 5.00 -7 -9 -4 27.30 5.50 -7 -9 -4 16.30 4.50 -7 9 -4 24.80 4.20 -7 9 -4 21.10 4.80 -7 9 -4 19.50 3.70 7 9 4 20.00 4.40 7 9 4 30.10 6.20 8 -9 4 308.57 15.60 -8 -9 -4 325.97 15.90 -8 -9 -4 284.07 10.50 -8 -9 -4 296.17 15.90 8 -9 4 292.67 15.70 -8 9 -4 308.67 15.20 -8 9 -4 302.37 13.60 -8 9 -4 323.57 16.20 8 9 4 289.77 14.40 8 9 4 287.57 10.40 8 9 4 294.67 16.80 9 -9 4 3.90 4.00 9 -9 4 0.80 3.60 -9 -9 -4 3.00 3.70 -9 -9 -4 16.00 4.80 -9 9 -4 -2.50 2.90 -9 9 -4 1.70 3.40 -9 9 -4 -0.50 2.60 9 9 4 5.00 4.40 9 9 4 10.00 3.70 -9 9 -4 1.50 2.50 9 9 4 11.60 2.20 10 -9 4 344.57 18.10 -10 -9 -4 313.67 12.50 10 -9 4 331.77 17.50 -10 -9 -4 290.57 16.80 -10 9 -4 321.27 17.40 10 9 4 316.07 18.40 -10 9 -4 330.17 14.50 10 9 4 326.27 12.40 -10 9 -4 310.47 16.90 -10 9 -4 336.87 15.00 10 9 4 307.47 19.80 -11 -9 -4 11.40 3.10 -11 -9 -4 14.20 5.70 11 -9 4 14.10 5.50 11 -9 4 7.90 5.10 -11 -9 -4 2.20 3.80 -11 9 -4 6.70 3.30 -11 9 -4 12.20 5.80 11 9 4 9.30 5.70 -11 9 -4 18.50 5.10 -11 9 -4 14.30 4.20 11 9 4 8.30 3.90 11 9 4 9.80 2.90 -12 -9 -4 152.48 12.80 -12 -9 -4 178.38 9.30 12 -9 4 164.58 13.20 12 -9 4 161.28 13.50 -12 -9 -4 173.78 13.60 -12 9 -4 164.08 13.30 -12 9 -4 165.68 10.30 12 9 4 178.58 14.10 12 9 4 161.08 11.80 12 9 4 176.68 9.30 -12 9 -4 192.28 11.30 -12 9 -4 178.08 12.80 13 -9 4 10.00 5.80 -13 -9 -4 12.30 6.40 13 -9 4 1.70 4.00 -13 9 -4 11.60 4.00 -13 9 -4 14.50 4.60 13 9 4 16.90 4.00 13 9 4 17.40 9.50 -13 9 -4 13.60 6.50 14 -9 4 57.29 9.70 14 -9 4 79.99 15.70 -14 -9 -4 56.39 7.10 -14 9 -4 82.29 8.90 -14 9 -4 65.79 7.90 14 9 4 83.19 12.10 14 9 4 57.49 6.90 -14 9 -4 69.79 11.40 -15 -9 -4 45.60 6.20 15 -9 4 34.30 7.80 -15 -9 -4 41.10 9.90 15 -9 4 34.00 8.70 -15 9 -4 48.60 7.10 15 9 4 34.70 8.90 -15 9 -4 36.70 6.60 15 9 4 33.10 5.70 -15 9 -4 36.30 8.20 -16 -9 -4 109.19 8.90 -16 -9 -4 132.59 14.60 16 -9 4 113.89 14.70 16 -9 4 116.59 15.20 -16 9 -4 149.09 17.10 -16 9 -4 110.89 9.70 16 9 4 108.69 9.20 -16 9 -4 133.19 11.00 16 9 4 102.99 13.50 -17 -9 -4 37.60 9.00 -17 -9 -4 35.40 6.40 17 -9 4 43.80 10.20 17 9 4 30.80 9.10 -17 9 -4 45.90 8.00 -17 9 -4 39.50 7.00 17 9 4 30.80 6.30 -17 9 -4 52.29 11.20 -18 -9 -4 7.60 6.40 -18 -9 -4 10.80 4.50 18 -9 4 8.80 7.70 -18 9 -4 12.00 7.80 18 9 4 27.90 9.70 -18 9 -4 8.10 5.00 18 9 4 14.10 5.20 -18 9 -4 8.80 5.40 -19 -9 -4 4.50 4.40 19 -9 4 7.50 6.70 -19 -9 -4 6.00 6.70 19 9 4 4.20 6.10 -19 9 -4 21.80 9.40 -19 9 -4 -0.60 4.30 19 9 4 5.70 4.50 20 -9 4 -8.30 6.10 -20 -9 -4 -4.90 5.80 -20 -9 -4 8.10 4.50 -20 9 -4 2.90 6.40 20 9 4 4.20 6.50 -20 9 -4 -3.20 4.30 20 9 4 0.20 4.30 -21 -9 -4 18.20 8.50 21 -9 4 23.40 8.80 -21 9 -4 11.70 6.00 -21 9 -4 13.00 8.00 21 9 4 4.30 5.30 21 9 4 7.00 6.80 -23 -10 4 65.09 13.30 23 -10 -4 66.69 12.30 23 10 -4 83.09 13.60 -23 10 4 75.99 8.70 -23 10 4 51.59 11.60 23 10 -4 59.99 9.20 22 -10 -4 0.10 6.70 -22 -10 4 7.80 7.80 -22 10 4 -2.20 6.70 22 10 -4 -3.40 4.40 -22 10 4 2.60 3.60 22 10 -4 -6.90 6.30 -22 10 4 7.60 3.60 -21 -10 4 40.40 10.30 21 -10 -4 43.40 10.70 -21 -10 4 53.99 8.40 21 -10 -4 38.70 10.20 21 10 -4 34.50 7.10 21 10 -4 38.30 10.10 -21 10 4 45.40 6.70 -21 10 4 51.19 11.70 -21 10 4 48.10 6.60 -20 -10 4 22.40 5.70 20 -10 -4 36.50 10.40 -20 -10 4 32.90 10.10 20 -10 -4 38.40 9.60 -20 10 4 27.20 8.60 20 10 -4 41.90 9.70 -20 10 4 38.80 6.00 20 10 -4 30.50 6.60 -20 10 4 40.30 5.80 19 -10 -4 41.90 10.00 -19 -10 4 39.40 10.60 19 -10 -4 39.20 10.50 -19 -10 4 43.40 7.20 19 10 -4 46.70 10.10 19 10 -4 49.60 7.70 -19 10 4 47.10 6.00 -19 10 4 39.40 5.60 -19 10 4 45.20 10.30 18 -10 -4 117.49 14.40 -18 -10 4 140.79 17.70 18 -10 -4 122.29 14.70 -18 -10 4 132.29 10.00 -18 10 4 110.89 13.10 -18 10 4 151.68 8.90 18 10 -4 130.79 15.30 18 10 -4 117.19 10.00 -18 10 4 142.39 8.90 17 -10 -4 1.90 5.80 -17 -10 4 4.30 3.70 17 -10 -4 11.10 6.40 -17 -10 4 12.50 6.30 17 10 -4 3.20 3.80 -17 10 4 0.10 4.80 -17 10 4 9.70 3.30 17 10 -4 3.90 5.70 16 -10 -4 64.19 11.00 16 -10 -4 60.99 10.50 -16 -10 4 88.59 8.50 -16 -10 4 91.89 13.80 -16 10 4 79.39 11.50 -16 10 4 79.99 6.40 16 10 -4 92.99 8.90 16 10 -4 87.09 11.80 -16 10 4 88.29 6.30 16 10 -4 66.69 10.70 -15 -10 4 6.20 5.60 -15 -10 4 5.10 2.90 15 -10 -4 11.70 7.60 15 10 -4 -1.60 3.90 15 10 -4 3.40 5.30 -15 10 4 6.80 2.50 15 10 -4 -0.80 3.10 -15 10 4 3.80 4.80 -15 10 4 1.50 2.30 14 -10 -4 52.99 9.50 -14 -10 4 58.79 6.40 -14 -10 4 53.39 10.50 14 -10 -4 56.99 9.70 -14 10 4 53.29 8.60 14 10 -4 52.49 6.50 14 10 -4 44.20 10.40 -14 10 4 60.89 9.20 -14 10 4 57.49 5.30 -14 10 4 50.29 4.80 -13 -10 4 -0.20 4.00 13 -10 -4 12.00 5.90 -13 -10 4 2.60 3.70 13 -10 -4 8.00 5.10 13 10 -4 2.30 5.00 -13 10 4 0.80 4.20 -13 10 4 5.60 4.00 13 10 -4 5.80 3.50 -13 10 4 5.90 2.40 13 10 -4 8.20 5.40 -13 10 4 8.40 2.30 -12 -10 4 737.93 31.90 -12 -10 4 668.33 29.90 12 -10 -4 769.72 31.70 12 -10 -4 759.72 31.40 -12 -10 4 728.83 25.30 -12 10 4 714.03 30.10 -12 10 4 763.52 24.00 -12 10 4 750.22 23.40 12 10 -4 730.23 31.10 12 10 -4 715.53 30.60 12 10 -4 732.43 26.20 -11 -10 4 47.20 9.80 -11 -10 4 30.40 6.20 11 -10 -4 49.00 9.10 -11 -10 4 37.20 4.40 11 -10 -4 28.90 6.90 -11 10 4 35.20 7.00 11 10 -4 32.80 4.90 11 10 -4 30.30 7.00 -11 10 4 35.40 6.60 11 10 -4 30.30 6.70 -11 10 4 23.10 3.00 -11 10 4 30.90 3.10 10 -10 -4 1116.99 39.20 -10 -10 4 1012.80 32.80 -10 -10 4 999.10 37.90 10 -10 -4 1012.40 38.40 -10 -10 4 1097.09 39.80 10 10 -4 1014.50 38.40 10 10 -4 1031.30 38.50 10 10 -4 1050.69 33.50 -10 10 4 1035.50 31.10 -10 10 4 1040.20 31.30 10 10 -4 980.70 32.60 -10 10 4 1048.00 38.00 -10 10 4 941.41 37.20 -9 -10 4 19.80 5.70 -9 -10 4 11.30 4.00 9 -10 -4 5.60 4.20 9 -10 -4 4.10 4.10 -9 10 4 6.30 4.00 9 10 -4 13.70 4.70 -9 10 4 9.40 1.90 9 10 -4 7.80 4.30 -9 10 4 12.90 2.10 9 10 -4 7.70 2.70 -9 10 4 8.20 3.90 9 10 -4 11.60 2.60 -8 -10 4 193.78 12.00 -8 -10 4 206.18 13.20 8 -10 -4 201.78 12.50 8 -10 -4 193.68 12.10 -8 10 4 191.88 7.30 8 10 -4 211.98 12.90 -8 10 4 185.38 12.00 -8 10 4 186.38 7.10 8 10 -4 183.38 8.50 8 10 -4 177.38 12.10 8 10 -4 179.58 8.20 -8 10 4 193.48 11.80 7 -10 -4 41.40 6.20 -7 -10 4 37.60 5.80 7 -10 -4 46.70 6.50 -7 -10 4 35.90 7.00 7 10 -4 42.20 3.70 -7 10 4 38.20 3.20 7 10 -4 44.20 3.80 -7 10 4 40.50 6.10 -7 10 4 39.90 6.40 7 10 -4 40.30 6.40 7 10 -4 34.60 6.40 -7 10 4 33.70 2.90 -6 -10 4 90.69 10.10 6 -10 -4 119.19 8.80 6 -10 -4 100.39 8.10 -6 -10 4 96.49 9.40 6 -10 -4 103.89 4.90 6 10 -4 113.39 5.70 -6 10 4 108.19 7.80 -6 10 4 110.89 5.30 6 10 -4 106.99 5.50 6 10 -4 98.49 8.50 -6 10 4 107.59 8.40 6 10 -4 116.19 10.50 -5 -10 4 121.69 9.80 5 -10 -4 104.29 8.20 5 -10 -4 107.99 5.30 5 -10 -4 124.79 8.20 -5 -10 4 111.99 8.20 5 10 -4 112.79 8.90 5 10 -4 115.99 8.60 -5 10 4 111.69 8.30 -5 10 4 119.69 7.60 -5 10 4 106.99 5.70 5 10 -4 112.59 5.60 5 10 -4 121.49 5.80 4 -10 -4 129.69 7.90 -4 -10 4 130.69 8.70 4 -10 -4 117.69 5.80 -4 -10 4 134.59 9.80 4 -10 -4 118.49 8.50 -4 10 4 121.19 7.40 -4 10 4 133.39 8.60 4 10 -4 137.89 9.10 -4 10 4 122.09 6.50 4 10 -4 118.99 6.00 4 10 -4 127.89 6.30 4 10 -4 134.99 9.50 3 -10 -4 15.40 4.00 -3 -10 4 7.30 3.00 3 -10 -4 9.30 2.20 -3 -10 4 11.20 2.30 -3 -10 4 6.40 3.50 3 -10 -4 7.80 2.80 3 10 -4 2.20 3.10 -3 10 4 14.40 3.10 -3 10 4 9.60 2.60 3 10 -4 8.70 2.20 3 10 -4 12.90 5.10 -2 -10 4 214.48 12.60 -2 -10 4 211.38 11.00 -2 -10 4 215.38 9.30 2 -10 -4 208.18 11.70 2 -10 -4 227.48 9.50 2 -10 -4 234.88 9.30 2 -10 -4 216.18 11.50 -2 10 4 213.88 9.10 2 10 -4 231.98 11.40 -2 10 4 214.68 10.10 2 10 -4 204.38 9.10 -1 -10 4 839.72 30.40 1 -10 -4 784.02 31.10 1 -10 -4 851.61 29.90 -1 -10 4 808.42 30.60 1 -10 -4 809.12 25.90 1 -10 -4 794.52 26.90 -1 -10 4 816.22 27.00 1 10 -4 829.52 27.00 -1 10 4 851.41 25.80 -1 10 4 844.72 28.30 1 10 -4 846.32 28.90 0 -10 -4 1071.79 37.00 0 -10 -4 1097.89 37.50 0 -10 4 1066.99 36.10 0 -10 4 1176.68 39.30 0 -10 4 1136.49 35.40 0 -10 -4 1092.19 35.20 0 -10 4 1079.99 38.20 0 -10 -4 1067.99 32.80 0 10 -4 1087.29 36.30 0 10 4 1092.19 36.60 0 10 4 1099.49 32.80 0 10 -4 1134.19 35.20 1 -10 4 2015.50 65.69 1 -10 4 1978.00 63.49 -1 -10 -4 2089.79 64.99 -1 -10 -4 2025.80 63.19 1 -10 4 2112.69 63.19 1 -10 4 2168.58 66.89 -1 -10 -4 2050.19 64.59 -1 10 -4 2136.49 63.89 1 10 4 2009.30 64.69 -1 10 -4 2097.99 63.09 -2 -10 -4 1033.50 35.10 2 -10 4 1100.99 38.10 2 -10 4 1082.69 37.30 -2 -10 -4 1077.49 36.50 2 -10 4 1085.99 34.90 2 -10 4 1036.80 34.90 -2 10 -4 1070.89 35.10 2 10 4 961.40 38.80 -2 10 -4 1068.29 35.10 3 -10 4 1137.79 37.80 3 -10 4 1154.58 39.90 3 -10 4 1225.18 41.00 -3 -10 -4 1121.69 38.70 -3 -10 -4 1099.49 38.50 3 -10 4 1125.99 37.40 -3 10 -4 1168.88 37.80 3 10 4 1123.09 39.70 -3 10 -4 1156.48 37.90 4 -10 4 136.49 8.00 -4 -10 -4 145.79 9.50 4 -10 4 125.99 8.40 4 -10 4 129.99 9.60 -4 -10 -4 134.89 9.00 -4 10 -4 128.99 9.80 4 10 4 117.99 8.20 4 10 4 127.59 9.90 -4 10 -4 135.59 8.00 -4 10 -4 137.89 9.90 -5 -10 -4 110.19 8.40 5 -10 4 92.79 10.20 5 -10 4 102.69 7.10 -5 -10 -4 107.09 8.40 5 -10 4 103.59 8.00 5 10 4 98.89 7.60 5 10 4 96.59 10.30 -5 10 -4 101.69 8.90 -5 10 -4 105.39 7.90 -5 10 -4 103.59 7.00 6 -10 4 34.70 4.80 -6 -10 -4 42.20 6.60 -6 -10 -4 44.00 6.40 6 -10 4 39.50 7.00 6 -10 4 25.70 5.20 6 10 4 34.30 5.50 -6 10 -4 34.30 4.80 -6 10 -4 27.70 5.20 6 10 4 40.40 7.00 -6 10 -4 26.40 5.20 7 -10 4 227.58 13.10 -7 -10 -4 228.18 13.10 -7 -10 -4 197.18 12.80 -7 10 -4 243.28 11.50 7 10 4 237.68 12.60 -7 10 -4 246.28 13.90 -7 10 -4 214.08 12.60 7 10 4 221.58 14.40 8 -10 4 37.70 6.60 -8 -10 -4 28.90 6.00 8 -10 4 42.10 7.70 -8 -10 -4 46.70 7.50 -8 10 -4 32.30 6.20 -8 10 -4 36.00 5.00 8 10 4 40.60 6.60 8 10 4 32.90 7.10 -8 10 -4 24.50 5.70 -8 10 -4 34.20 5.10 9 -10 4 372.56 18.80 -9 -10 -4 357.26 19.30 -9 -10 -4 359.76 18.70 9 -10 4 363.66 19.10 -9 10 -4 394.26 18.80 -9 10 -4 360.66 15.70 9 10 4 398.46 20.60 9 10 4 388.06 18.40 -9 10 -4 403.46 19.60 -9 10 -4 391.06 16.50 -10 -10 -4 15.30 5.30 -10 -10 -4 20.70 5.40 10 -10 4 7.50 4.80 -10 -10 -4 18.40 2.70 10 -10 4 12.00 4.50 -10 10 -4 11.20 5.00 10 10 4 19.00 5.20 10 10 4 16.90 2.70 -10 10 -4 9.00 3.60 10 10 4 21.40 6.40 -10 10 -4 11.10 5.40 -10 10 -4 9.80 3.50 -11 -10 -4 149.88 12.10 11 -10 4 158.28 12.80 -11 -10 -4 153.88 7.60 11 -10 4 138.79 12.10 -11 -10 -4 149.29 12.50 11 10 4 147.79 11.30 -11 10 -4 144.89 12.60 11 10 4 143.49 7.40 -11 10 -4 154.78 9.60 11 10 4 171.38 13.90 -11 10 -4 157.58 12.20 -11 10 -4 170.38 10.30 12 -10 4 34.90 7.10 -12 -10 -4 32.00 4.30 -12 -10 -4 25.30 6.90 12 -10 4 45.00 8.70 -12 10 -4 31.40 7.60 12 10 4 31.60 4.20 -12 10 -4 42.60 9.40 -12 10 -4 37.90 6.00 -12 10 -4 42.30 5.90 12 10 4 47.80 9.20 -13 -10 -4 63.59 6.10 13 -10 4 59.59 10.00 -13 -10 -4 62.19 15.80 13 -10 4 36.70 6.80 -13 10 -4 60.79 7.70 -13 10 -4 46.30 8.90 13 10 4 46.60 9.50 13 10 4 68.89 6.00 -13 10 -4 51.29 6.70 -14 -10 -4 85.19 12.30 -14 -10 -4 68.69 10.00 14 -10 4 65.29 11.20 14 -10 4 59.99 10.40 -14 10 -4 61.59 8.00 -14 10 -4 60.59 7.60 14 10 4 61.19 6.60 -14 10 -4 51.49 9.90 14 10 4 54.89 10.70 -15 -10 -4 158.48 17.60 15 -10 4 149.88 13.70 15 -10 4 142.99 15.60 15 10 4 162.48 16.40 15 10 4 132.49 9.30 -15 10 -4 121.39 13.40 -15 10 -4 153.78 11.20 -15 10 -4 149.79 10.50 -16 -10 -4 61.99 7.20 16 -10 4 62.99 12.00 -16 -10 -4 61.49 10.80 -16 10 -4 72.39 8.70 16 10 4 71.89 7.80 16 10 4 60.69 11.30 -16 10 -4 71.59 9.00 -16 10 -4 52.19 10.90 -17 -10 -4 146.89 18.50 17 -10 4 112.99 14.80 -17 -10 -4 106.09 8.80 17 10 4 101.19 9.90 17 10 4 90.49 13.10 -17 10 -4 118.39 15.90 -17 10 -4 137.19 11.20 -17 10 -4 118.79 10.50 -18 -10 -4 14.80 4.80 18 -10 4 18.10 8.10 -18 -10 -4 14.00 7.60 -18 10 -4 19.90 6.10 18 10 4 -6.00 5.20 -18 10 -4 16.30 5.90 18 10 4 14.20 5.20 -18 10 -4 23.80 8.90 -19 -10 -4 5.40 7.40 -19 -10 -4 1.20 3.40 19 -10 4 -3.80 5.90 19 10 4 0.90 4.20 19 10 4 -12.60 4.30 -19 10 -4 -3.40 4.90 -19 10 -4 -3.00 3.90 -20 -10 -4 2.10 6.70 -20 -10 -4 14.50 4.50 20 -10 4 14.40 7.90 -20 10 -4 6.00 4.90 20 10 4 -1.90 5.60 20 10 4 2.70 4.30 -20 10 -4 2.50 6.40 21 -10 4 48.50 11.50 -21 -10 -4 28.10 11.30 -21 10 -4 55.99 13.20 -21 10 -4 49.00 9.00 21 10 4 36.10 10.30 21 10 4 37.20 7.40 -22 -11 4 45.70 8.80 22 -11 -4 62.49 12.50 -22 -11 4 30.00 10.00 -22 11 4 55.09 12.00 22 11 -4 52.99 11.80 22 11 -4 49.30 8.10 -22 11 4 44.40 6.70 -22 11 4 47.80 8.50 -21 -11 4 56.69 13.80 -21 -11 4 40.60 7.10 21 -11 -4 35.50 10.50 21 -11 -4 38.50 13.00 -21 11 4 38.70 5.40 21 11 -4 29.50 6.70 -21 11 4 53.29 6.50 -21 11 4 61.39 12.60 21 11 -4 72.89 19.40 -20 -11 4 12.90 6.30 20 -11 -4 23.20 8.50 20 -11 -4 23.80 9.50 -20 -11 4 14.40 9.00 -20 11 4 29.50 5.00 -20 11 4 17.80 7.70 -20 11 4 25.60 4.80 20 11 -4 16.50 7.60 20 11 -4 16.10 5.30 -19 -11 4 28.30 9.30 -19 -11 4 40.00 6.50 19 -11 -4 42.60 9.80 19 -11 -4 23.90 9.00 -19 11 4 41.00 10.80 19 11 -4 29.50 6.10 19 11 -4 28.20 8.80 -19 11 4 22.40 7.00 -19 11 4 38.70 5.20 -18 -11 4 3.50 3.50 18 -11 -4 -1.00 5.50 18 -11 -4 1.40 6.30 -18 -11 4 -4.30 6.20 18 11 -4 7.00 4.20 18 11 -4 3.40 5.90 -18 11 4 8.10 6.50 -17 -11 4 7.80 3.70 17 -11 -4 -1.80 5.50 17 -11 -4 -0.40 4.50 -17 -11 4 -2.30 5.50 -17 11 4 2.40 2.60 17 11 -4 2.40 3.80 17 11 -4 5.40 6.20 -17 11 4 10.60 3.20 -17 11 4 -1.70 6.30 -16 -11 4 9.10 6.80 -16 -11 4 8.00 3.60 16 -11 -4 10.50 6.20 16 -11 -4 21.80 7.60 -16 11 4 13.30 3.30 16 11 -4 12.90 6.60 -16 11 4 12.90 5.70 16 11 -4 12.00 4.30 -16 11 4 13.90 3.10 15 -11 -4 1.70 5.00 15 -11 -4 0.50 5.60 -15 -11 4 0.40 4.90 15 11 -4 -0.10 3.00 -15 11 4 1.00 2.10 15 11 -4 0.40 4.40 15 11 -4 -8.20 4.40 -15 11 4 1.00 4.90 -15 11 4 0.70 2.00 -14 -11 4 60.69 10.50 -14 -11 4 65.59 6.50 14 -11 -4 50.39 8.50 14 -11 -4 48.50 9.40 14 11 -4 64.89 10.80 14 11 -4 68.79 9.20 -14 11 4 57.49 4.90 -14 11 4 67.29 4.70 14 11 -4 65.09 9.90 -14 11 4 56.59 8.70 13 -11 -4 8.80 6.00 -13 -11 4 2.60 5.00 13 -11 -4 9.10 5.70 -13 -11 4 9.20 3.10 -13 11 4 11.90 2.60 -13 11 4 9.20 2.30 13 11 -4 6.30 4.70 13 11 -4 3.10 3.30 13 11 -4 8.90 8.80 -13 11 4 11.70 5.30 -13 11 4 10.40 5.90 -12 -11 4 -0.20 2.10 12 -11 -4 4.70 5.00 -12 -11 4 5.20 4.80 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5.10 8 11 -4 101.19 10.30 -8 11 4 82.49 8.90 -8 11 4 114.89 8.90 8 11 -4 91.09 5.70 -8 11 4 97.49 4.80 7 -11 -4 195.18 11.80 -7 -11 4 175.68 12.70 -7 -11 4 182.68 11.70 7 -11 -4 185.68 12.00 -7 11 4 170.48 7.10 -7 11 4 175.68 11.10 7 11 -4 180.98 7.90 -7 11 4 181.88 7.60 -7 11 4 199.08 12.10 7 11 -4 185.88 12.50 7 11 -4 184.58 12.40 7 11 -4 180.08 7.80 -6 -11 4 11.80 3.80 6 -11 -4 6.70 2.20 6 -11 -4 12.30 4.20 -6 -11 4 5.70 4.10 6 -11 -4 9.80 3.70 6 11 -4 13.70 2.40 -6 11 4 7.90 2.80 6 11 -4 12.70 4.60 6 11 -4 10.00 2.30 6 11 -4 10.40 4.30 -6 11 4 10.00 3.70 -6 11 4 18.80 5.00 -5 -11 4 133.99 10.70 5 -11 -4 144.99 9.00 5 -11 -4 130.79 6.20 -5 -11 4 121.09 9.10 5 -11 -4 133.19 9.60 -5 11 4 125.79 9.20 5 11 -4 141.29 6.50 5 11 -4 130.89 9.50 5 11 -4 131.59 10.20 -5 11 4 132.79 6.80 5 11 -4 129.29 6.20 4 -11 -4 109.89 8.40 4 -11 -4 113.79 7.30 -4 -11 4 98.49 9.20 -4 -11 4 103.09 8.10 4 -11 -4 98.69 5.50 4 11 -4 95.09 8.00 4 11 -4 105.89 5.60 4 11 -4 111.19 5.80 -4 11 4 102.59 6.50 -4 11 4 113.89 7.20 3 -11 -4 25.40 4.70 -3 -11 4 24.20 3.30 -3 -11 4 24.80 5.00 3 -11 -4 25.00 3.30 3 -11 -4 29.90 4.00 3 11 -4 21.50 3.10 -3 11 4 23.80 3.90 -3 11 4 33.10 4.20 3 11 -4 35.00 6.60 3 11 -4 23.40 5.00 2 -11 -4 545.85 18.70 -2 -11 4 556.84 23.30 2 -11 -4 552.14 18.90 2 -11 -4 532.35 21.70 -2 -11 4 526.15 21.00 -2 -11 4 547.55 18.80 -2 -11 4 562.44 22.80 2 -11 -4 512.15 21.80 -2 11 4 554.94 20.10 2 11 -4 540.65 21.30 2 11 -4 538.15 18.80 -2 11 4 539.45 18.60 -1 -11 4 4.40 2.90 -1 -11 4 8.40 2.70 -1 -11 4 2.80 3.60 1 -11 -4 5.30 2.10 1 -11 -4 1.60 3.20 1 -11 -4 8.50 2.60 1 -11 -4 -1.60 2.90 -1 -11 4 6.60 3.90 1 11 -4 9.20 2.80 -1 11 4 7.90 2.20 -1 11 4 12.70 3.50 1 11 -4 3.00 3.20 0 -11 4 283.17 14.90 0 -11 -4 306.27 14.80 0 -11 -4 283.77 12.30 0 -11 4 295.47 12.40 0 -11 -4 295.97 14.40 0 -11 4 275.07 13.10 0 -11 4 296.87 15.80 0 -11 -4 285.97 10.00 0 11 4 283.67 10.00 0 11 -4 301.67 12.40 0 11 -4 289.37 13.40 0 11 4 286.57 13.70 -1 -11 -4 40.60 7.00 1 -11 4 32.10 4.90 1 -11 4 38.90 6.70 -1 -11 -4 54.89 5.60 1 -11 4 24.80 4.40 -1 -11 -4 38.10 5.90 1 -11 4 27.20 6.30 -1 11 -4 34.50 5.00 -1 11 -4 33.40 4.90 1 11 4 50.79 7.50 2 -11 4 112.39 9.80 2 -11 4 117.99 12.20 -2 -11 -4 103.19 10.20 -2 -11 -4 99.89 7.50 2 -11 4 96.99 10.70 -2 11 -4 89.19 7.10 -2 11 -4 100.89 7.40 2 11 4 93.29 9.30 3 -11 4 97.89 9.10 -3 -11 -4 109.39 9.00 3 -11 4 87.29 7.40 -3 -11 -4 130.09 8.40 3 -11 4 102.69 11.20 -3 11 -4 100.89 7.30 -3 11 -4 92.59 7.60 3 11 4 131.39 9.70 -4 -11 -4 8.60 4.10 4 -11 4 13.10 4.10 4 -11 4 12.00 5.30 -4 -11 -4 12.50 3.90 4 11 4 8.50 4.40 -4 11 -4 10.20 3.30 -4 11 -4 6.60 3.60 5 -11 4 203.18 12.00 5 -11 4 194.78 12.60 -5 -11 -4 190.18 11.70 -5 -11 -4 217.08 12.50 5 -11 4 204.38 11.60 5 11 4 211.38 11.60 -5 11 -4 206.28 12.90 -5 11 -4 221.18 10.80 -5 11 -4 182.38 11.10 5 11 4 210.08 13.40 6 -11 4 13.80 4.50 -6 -11 -4 7.20 4.00 -6 -11 -4 8.80 3.90 6 -11 4 14.20 3.60 6 -11 4 8.60 4.20 6 11 4 13.70 5.20 6 11 4 5.60 3.30 -6 11 -4 7.70 3.20 -6 11 -4 13.80 4.10 7 -11 4 13.00 4.70 -7 -11 -4 20.50 5.20 7 -11 4 17.10 3.80 -7 -11 -4 18.20 5.50 7 -11 4 31.00 6.90 7 11 4 24.90 5.70 -7 11 -4 18.80 5.10 -7 11 -4 16.90 5.30 -7 11 -4 16.90 4.00 -7 11 -4 21.30 4.20 7 11 4 9.30 5.10 8 -11 4 32.70 6.30 -8 -11 -4 22.10 5.50 -8 -11 -4 30.70 6.40 8 -11 4 22.40 5.50 -8 11 -4 25.00 5.50 -8 11 -4 23.70 6.10 8 11 4 28.00 6.80 -8 11 -4 37.10 5.30 8 11 4 26.80 5.40 -8 11 -4 32.20 4.80 9 -11 4 11.30 5.10 -9 -11 -4 7.20 4.20 -9 -11 -4 11.20 5.00 9 -11 4 10.40 4.70 -9 11 -4 14.10 3.90 9 11 4 16.70 6.30 -9 11 -4 16.30 4.30 -9 11 -4 14.60 5.40 9 11 4 15.40 4.90 -10 -11 -4 59.19 8.70 -10 -11 -4 77.59 10.20 10 -11 4 63.09 8.90 10 -11 4 74.89 10.00 -10 11 -4 76.29 9.60 10 11 4 65.19 10.20 10 11 4 96.49 10.50 -10 11 -4 84.49 7.10 -10 11 -4 72.29 7.60 -10 11 -4 79.49 9.90 11 -11 4 25.20 6.70 -11 -11 -4 13.60 5.30 11 -11 4 12.10 5.70 11 11 4 20.60 6.70 -11 11 -4 17.60 4.50 -11 11 -4 29.10 8.30 -11 11 -4 20.10 4.40 -11 11 -4 19.90 5.90 12 -11 4 214.68 26.90 -12 -11 -4 181.28 8.20 -12 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17 11 4 25.30 5.30 -18 -11 -4 0.80 3.20 18 -11 4 6.40 6.80 -18 -11 -4 6.40 7.40 18 11 4 -2.70 5.50 -18 11 -4 3.20 4.40 18 11 4 4.90 4.00 -18 11 -4 1.30 5.60 -18 11 -4 -2.80 3.40 -19 -11 -4 -2.60 2.80 -19 -11 -4 -6.10 5.70 19 -11 4 -9.00 6.20 -19 11 -4 3.20 4.40 -19 11 -4 -7.00 4.90 19 11 4 0.10 3.50 -20 -11 -4 -5.70 8.40 20 -11 4 -2.10 6.20 20 11 4 2.50 5.90 -20 11 -4 -1.90 4.20 -20 11 -4 -4.90 4.70 20 11 4 -4.40 2.90 -22 -12 4 23.40 8.70 22 -12 -4 30.50 9.90 22 12 -4 28.10 6.70 22 12 -4 30.20 9.40 -22 12 4 32.70 8.70 -21 -12 4 17.10 5.90 -21 -12 4 13.50 9.00 21 -12 -4 19.20 8.20 21 12 -4 19.20 8.20 -21 12 4 26.50 9.40 -21 12 4 26.20 4.90 21 12 -4 20.70 5.60 -21 12 4 12.40 3.90 20 -12 -4 24.50 9.30 -20 -12 4 7.60 4.20 -20 -12 4 23.90 10.10 20 -12 -4 10.30 6.70 -20 12 4 5.40 6.00 20 12 -4 5.30 7.40 -20 12 4 15.00 3.80 20 12 -4 16.00 4.90 19 -12 -4 16.00 7.90 19 -12 -4 4.60 6.00 -19 -12 4 1.60 7.30 -19 -12 4 6.20 3.70 19 12 -4 9.00 7.20 -19 12 4 2.00 6.40 19 12 -4 11.40 4.40 18 -12 -4 16.20 8.60 -18 -12 4 21.30 4.80 -18 -12 4 29.60 9.10 18 -12 -4 23.90 8.50 -18 12 4 22.70 8.30 18 12 -4 27.80 5.50 18 12 -4 4.90 6.40 -18 12 4 28.40 4.20 -18 12 4 22.70 4.10 -17 -12 4 1.00 3.10 17 -12 -4 10.10 6.80 17 -12 -4 -5.20 3.90 -17 -12 4 -4.50 5.30 -17 12 4 0.00 2.30 17 12 -4 5.20 3.60 -17 12 4 1.90 2.60 -17 12 4 1.00 4.90 17 12 -4 -2.50 5.50 16 -12 -4 41.30 9.80 -16 -12 4 35.90 9.70 16 -12 -4 47.60 9.00 -16 12 4 50.29 11.20 16 12 -4 36.70 9.20 -16 12 4 42.90 4.50 16 12 -4 55.39 6.50 -16 12 4 56.59 5.40 15 -12 -4 11.70 5.90 -15 -12 4 25.50 8.40 -15 -12 4 19.40 3.90 15 -12 -4 19.70 8.00 -15 12 4 18.10 3.10 -15 12 4 22.20 3.60 -15 12 4 35.50 10.80 15 12 -4 19.60 7.20 -14 -12 4 13.30 7.00 14 -12 -4 15.10 5.60 14 -12 -4 19.00 7.80 -14 -12 4 15.70 3.70 14 12 -4 23.60 7.80 14 12 -4 22.40 4.40 14 12 -4 19.20 6.20 -14 12 4 23.00 3.10 -14 12 4 28.20 3.60 -14 12 4 14.80 5.80 -13 -12 4 24.40 7.00 13 -12 -4 34.70 8.20 -13 12 4 39.50 3.90 -13 12 4 35.00 8.30 13 12 -4 28.30 7.70 -13 12 4 35.10 3.50 13 12 -4 38.20 8.00 13 12 -4 30.30 4.60 -13 12 4 27.40 6.60 13 12 -4 29.70 4.10 -12 -12 4 371.26 20.90 12 -12 -4 361.26 19.90 12 -12 -4 351.06 19.80 12 12 -4 337.57 19.50 -12 12 4 331.77 12.00 12 12 -4 332.37 14.00 -12 12 4 394.66 19.80 -12 12 4 311.57 18.00 12 12 -4 329.67 13.30 -11 -12 4 30.40 6.70 -11 -12 4 18.30 6.80 11 -12 -4 20.70 6.20 11 -12 -4 32.90 7.00 11 12 -4 25.10 4.00 11 12 -4 38.30 8.30 -11 12 4 22.90 2.80 -11 12 4 27.40 7.00 11 12 -4 23.30 3.30 11 12 -4 31.00 7.70 10 -12 -4 157.88 12.50 -10 -12 4 133.89 11.30 10 -12 -4 168.68 12.70 -10 -12 4 179.98 13.70 10 12 -4 145.69 7.20 -10 12 4 137.19 11.70 -10 12 4 143.19 11.20 -10 12 4 134.39 6.40 10 12 -4 134.39 7.80 10 12 -4 148.19 12.60 10 12 -4 170.48 12.80 9 -12 -4 28.60 6.40 -9 -12 4 32.20 7.30 9 -12 -4 27.60 6.50 -9 -12 4 29.00 6.40 9 12 -4 35.40 7.70 9 12 -4 36.40 8.00 -9 12 4 26.70 2.90 -9 12 4 39.30 8.00 9 12 -4 29.60 3.90 9 12 -4 27.30 3.30 -9 12 4 31.90 6.20 -9 12 4 24.40 3.10 8 -12 -4 46.40 7.40 8 -12 -4 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130.49 6.40 1 14 -4 132.29 8.10 0 -14 -4 15.90 5.60 0 -14 4 15.80 3.80 0 -14 -4 18.00 4.00 0 -14 4 27.10 6.50 0 -14 4 26.80 6.30 0 -14 4 9.90 3.90 0 -14 -4 20.40 5.60 0 14 -4 16.70 4.70 0 14 4 19.80 5.40 1 -14 4 79.99 11.20 -1 -14 -4 81.09 10.40 1 -14 4 89.99 11.70 -1 -14 -4 76.99 9.10 -1 -14 -4 94.19 7.40 1 -14 4 82.59 7.00 1 -14 4 84.29 8.30 1 14 4 95.79 9.80 -1 14 -4 84.69 8.80 -1 14 -4 82.49 8.10 -2 -14 -4 86.69 7.40 -2 -14 -4 105.89 11.70 -2 -14 -4 79.99 9.10 2 -14 4 88.49 10.40 2 -14 4 57.59 8.40 2 -14 4 79.59 8.10 2 -14 4 89.09 8.20 2 14 4 80.39 9.40 -2 14 -4 84.79 8.30 -2 14 -4 80.49 8.20 3 -14 4 83.59 9.90 3 -14 4 93.29 8.70 3 -14 4 85.99 7.50 -3 -14 -4 108.59 12.10 -3 -14 -4 93.09 8.00 3 -14 4 117.69 12.70 3 14 4 96.99 10.70 -3 14 -4 87.39 8.80 -3 14 -4 77.49 8.00 4 -14 4 79.69 14.90 -4 -14 -4 68.79 8.20 4 -14 4 99.39 12.40 4 -14 4 81.79 7.10 -4 -14 -4 85.89 10.60 4 -14 4 72.19 8.00 -4 14 -4 69.19 7.70 4 14 4 66.39 9.50 -4 14 -4 81.49 8.90 -5 -14 -4 188.48 13.30 5 -14 4 190.08 14.50 -5 -14 -4 165.98 11.50 5 -14 4 182.38 11.60 5 -14 4 181.48 10.50 5 -14 4 167.28 13.10 5 14 4 176.88 13.30 -5 14 -4 166.78 11.80 -5 14 -4 178.28 10.60 6 -14 4 78.99 11.20 -6 -14 -4 62.19 8.40 6 -14 4 77.19 10.20 6 -14 4 76.39 8.90 -6 -14 -4 86.89 11.20 6 -14 4 73.79 7.80 6 14 4 95.89 11.90 -6 14 -4 78.79 7.90 -6 14 -4 88.09 9.90 7 -14 4 41.70 7.00 7 -14 4 35.50 5.80 -7 -14 -4 31.30 6.80 7 -14 4 43.80 8.90 -7 -14 -4 42.20 7.30 -7 14 -4 45.50 8.60 -7 14 -4 30.00 5.30 7 14 4 39.80 8.20 -7 14 -4 40.80 8.50 8 -14 4 14.30 5.60 -8 -14 -4 7.70 4.40 8 -14 4 12.50 5.40 -8 14 -4 12.70 4.20 -8 14 -4 11.10 3.70 -8 14 -4 15.10 5.70 -8 14 -4 8.70 4.80 8 14 4 10.60 6.40 9 -14 4 88.19 12.40 9 -14 4 79.59 10.20 -9 -14 -4 110.29 13.60 -9 14 -4 81.49 11.20 -9 14 -4 89.19 7.50 -9 14 -4 113.69 12.20 -9 14 -4 90.49 8.90 10 -14 4 26.70 7.40 -10 -14 -4 27.90 7.20 10 -14 4 17.70 7.40 -10 14 -4 20.40 5.10 -10 14 -4 27.20 5.00 -10 14 -4 22.50 6.20 10 14 4 12.10 6.60 11 -14 4 450.95 23.70 -11 -14 -4 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5.40 18 14 4 -7.50 5.60 -19 -15 4 33.80 11.10 19 -15 -4 20.00 14.00 19 15 -4 18.20 8.60 -19 15 4 30.60 8.20 18 -15 -4 91.29 13.90 18 -15 -4 79.29 19.20 -18 -15 4 81.39 15.00 18 15 -4 70.29 12.50 -18 15 4 60.19 11.50 18 15 -4 81.89 6.10 17 -15 -4 7.60 6.40 17 -15 -4 2.30 6.30 -17 -15 4 1.60 6.10 17 15 -4 13.00 8.10 -17 15 4 -0.80 4.60 17 15 -4 1.40 2.30 -16 -15 4 24.70 9.70 16 -15 -4 26.00 8.00 16 -15 -4 30.60 8.90 -16 15 4 40.60 9.10 16 15 -4 27.50 8.60 -15 -15 4 -3.70 5.40 15 -15 -4 4.10 4.60 15 -15 -4 11.90 6.30 15 15 -4 -4.00 5.80 -15 15 4 3.90 5.70 14 -15 -4 14.50 5.90 14 -15 -4 24.60 7.80 -14 -15 4 2.90 5.30 14 15 -4 22.00 7.80 -14 15 4 14.30 7.10 13 -15 -4 80.99 13.40 13 -15 -4 77.19 11.50 -13 -15 4 74.19 11.70 -13 15 4 88.99 13.00 13 15 -4 75.89 11.90 12 -15 -4 40.10 9.70 12 -15 -4 36.00 9.00 -12 -15 4 21.10 7.80 12 15 -4 36.00 9.30 -12 15 4 46.00 8.70 11 -15 -4 114.29 14.00 11 -15 -4 114.19 12.40 -11 -15 4 114.89 14.90 11 15 -4 104.39 13.40 -11 15 4 97.29 11.40 -11 15 4 127.09 15.10 -10 -15 4 97.29 12.50 10 -15 -4 127.59 13.80 10 -15 -4 138.49 11.80 -10 15 4 131.59 14.30 10 15 -4 117.69 13.60 -10 15 4 132.19 12.60 10 15 -4 146.79 19.10 9 -15 -4 10.80 5.10 -9 -15 4 24.90 8.20 9 -15 -4 8.20 4.40 -9 15 4 5.80 2.40 9 15 -4 6.10 4.50 9 15 -4 12.60 6.30 -9 15 4 8.00 4.40 -9 15 4 10.20 2.30 -9 15 4 6.10 4.10 8 -15 -4 -4.70 3.40 -8 -15 4 2.80 5.70 8 -15 -4 1.10 4.00 -8 15 4 -0.90 1.80 8 15 -4 -3.00 4.00 -8 15 4 1.30 3.70 -8 15 4 3.30 2.60 8 15 -4 4.70 5.70 -8 15 4 7.00 3.90 7 -15 -4 246.48 13.70 -7 -15 4 265.47 16.50 7 -15 -4 256.57 10.50 7 -15 -4 252.87 16.10 -7 -15 4 256.77 17.30 7 15 -4 257.27 16.50 -7 15 4 258.37 14.00 -7 15 4 247.98 11.30 7 15 -4 227.88 15.90 -6 -15 4 170.78 14.30 -6 -15 4 160.78 11.80 6 -15 -4 149.19 7.90 6 -15 -4 164.38 10.30 6 -15 -4 162.58 12.80 -6 15 4 143.39 8.90 6 15 -4 213.98 24.80 6 15 -4 145.29 12.30 -6 15 4 154.38 10.10 -5 -15 4 529.85 23.30 5 -15 -4 555.14 25.50 5 -15 -4 539.85 24.60 5 -15 -4 553.74 20.90 -5 -15 4 558.04 26.30 5 -15 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8.60 11 -15 4 16.10 6.60 -11 15 -4 13.50 6.10 -11 15 -4 19.90 5.00 11 15 4 24.10 7.60 -11 15 -4 18.40 4.60 12 -15 4 298.37 19.50 -12 -15 -4 283.67 19.80 12 -15 4 328.57 20.70 12 15 4 307.27 20.80 -12 15 -4 310.57 15.60 -12 15 -4 288.37 19.90 -12 15 -4 291.87 14.90 -13 -15 -4 2.20 5.20 13 -15 4 10.30 5.80 13 -15 4 6.50 5.80 13 15 4 12.70 7.60 -13 15 -4 6.60 3.90 -13 15 -4 1.70 4.00 -13 15 -4 17.20 7.30 -14 -15 -4 189.28 16.90 14 -15 4 207.08 17.30 -14 15 -4 202.28 12.50 14 15 4 188.58 19.40 -14 15 -4 183.18 16.30 15 -15 4 -8.20 4.10 -15 -15 -4 -0.40 5.70 -15 15 -4 4.40 5.70 -15 15 -4 -0.90 3.40 -15 15 -4 -2.70 3.30 15 15 4 -8.00 4.70 -16 -15 -4 32.80 10.00 16 -15 4 28.60 9.10 -16 15 -4 33.60 9.20 -16 15 -4 32.70 6.20 16 15 4 38.40 16.60 -16 15 -4 23.40 5.80 17 -15 4 4.30 6.70 -17 -15 -4 2.40 6.80 -17 15 -4 -0.70 6.80 17 15 4 4.90 6.20 -17 15 -4 -1.90 3.80 -17 15 -4 8.30 4.60 18 -16 -4 48.70 11.90 -18 -16 4 72.99 15.50 18 16 -4 45.10 10.70 -18 16 4 43.50 10.40 17 -16 -4 59.59 11.50 17 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5 4.30 6.50 -12 14 -5 9.40 4.20 -12 14 -5 5.80 3.80 -12 14 -5 8.60 6.00 13 -14 5 128.79 15.30 -13 -14 -5 137.29 16.60 13 -14 5 202.48 26.40 -13 14 -5 126.79 14.80 -13 14 -5 123.19 10.20 13 14 5 124.89 15.30 -13 14 -5 131.69 10.40 -14 -14 -5 4.90 5.50 14 -14 5 5.60 6.20 -14 14 -5 14.60 5.30 -14 14 -5 5.70 4.10 14 14 5 10.80 7.30 -14 14 -5 -3.90 4.70 15 -14 5 59.29 11.80 -15 -14 -5 43.20 9.80 15 14 5 32.00 9.10 -15 14 -5 58.49 8.10 -15 14 -5 54.09 7.70 -15 14 -5 59.69 10.90 16 -14 5 50.79 11.10 -16 -14 -5 34.50 9.50 16 14 5 31.60 9.10 -16 14 -5 56.59 8.30 -16 14 -5 43.00 10.40 -16 14 -5 45.00 7.70 -17 -14 -5 -2.10 9.00 -17 14 -5 16.40 7.80 17 14 5 -0.60 6.50 -18 -14 -5 59.19 12.90 18 -14 5 88.49 14.90 -18 14 -5 98.59 15.30 18 14 5 120.99 16.00 -18 14 -5 87.99 10.60 -19 -15 5 105.89 16.90 19 15 -5 125.19 8.60 19 15 -5 97.99 14.50 -19 15 5 125.69 17.70 18 -15 -5 27.10 9.00 18 -15 -5 15.90 6.80 -18 -15 5 16.60 7.50 18 15 -5 17.80 7.50 -18 15 5 1.20 5.20 -17 -15 5 144.09 18.50 17 -15 -5 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125.29 5.70 -5 8 -7 141.09 8.70 -5 8 -7 118.09 9.10 -6 -8 -7 54.19 7.70 6 -8 7 64.39 7.50 6 -8 7 51.39 6.40 -6 -8 -7 55.29 6.80 -6 -8 -7 45.40 4.00 -6 8 -7 50.89 6.60 -6 8 -7 49.90 6.40 6 8 7 49.99 7.50 -6 8 -7 42.30 6.80 6 8 7 48.90 5.50 -6 8 -7 51.19 6.00 6 8 7 45.20 3.70 -7 -8 -7 1910.11 64.49 7 -8 7 1982.70 63.89 7 -8 7 1977.60 63.79 -7 -8 -7 1866.71 58.69 -7 -8 -7 2074.09 62.89 -7 8 -7 1961.60 63.09 -7 8 -7 1965.20 61.69 7 8 7 1850.51 64.79 7 8 7 2036.60 58.79 7 8 7 1889.01 60.89 -7 8 -7 2061.09 64.29 -7 8 -7 1986.40 62.29 -8 -8 -7 553.04 22.60 8 -8 7 529.25 23.20 -8 -8 -7 507.85 18.80 -8 -8 -7 527.05 23.70 8 -8 7 591.04 23.80 -8 8 -7 540.75 21.80 8 8 7 506.05 20.70 -8 8 -7 535.75 22.50 -8 8 -7 562.54 23.60 8 8 7 512.95 24.40 8 8 7 560.14 18.90 -8 8 -7 511.25 21.00 9 -8 7 1950.10 64.09 9 -8 7 1829.82 63.69 -9 -8 -7 1903.71 58.99 -9 -8 -7 1842.02 64.39 -9 -8 -7 1958.00 63.29 -9 8 -7 1980.80 61.99 9 8 7 1967.40 65.69 -9 8 -7 1902.71 61.19 9 8 7 1900.91 64.29 9 8 7 1944.31 58.79 -9 8 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13.90 4.20 0 -12 -8 23.00 5.30 0 -12 8 15.20 5.10 0 -12 -8 18.30 2.80 0 -12 -8 19.20 2.50 0 -12 -8 14.80 4.70 0 -12 8 17.80 4.50 0 12 -8 20.50 4.80 0 12 8 26.40 5.20 0 12 -8 12.70 3.80 1 -12 8 296.47 17.00 1 -12 8 298.17 16.20 -1 -12 -8 278.27 14.00 1 -12 8 297.57 14.60 -1 -12 -8 282.17 14.50 1 -12 8 299.47 14.40 -1 -12 -8 278.07 13.70 -1 12 -8 301.57 14.80 -1 12 -8 290.37 13.90 1 12 8 289.97 14.70 -2 -12 -8 86.39 8.40 -2 -12 -8 67.59 7.90 2 -12 8 83.49 10.30 2 -12 8 70.99 7.90 2 -12 8 70.99 8.00 -2 -12 -8 75.39 8.00 2 -12 8 58.79 8.50 -2 12 -8 89.59 8.90 -2 12 -8 77.99 7.80 2 12 8 83.59 9.20 -3 -12 -8 70.69 8.30 3 -12 8 79.39 9.70 -3 -12 -8 76.69 8.70 3 -12 8 102.79 11.50 3 -12 8 76.39 8.30 3 -12 8 68.29 8.10 -3 12 -8 72.59 8.20 -3 12 -8 81.79 8.70 3 12 8 82.29 9.90 4 -12 8 -0.70 3.50 4 -12 8 0.50 3.30 4 -12 8 -3.10 3.20 -4 -12 -8 2.90 3.90 -4 -12 -8 3.10 3.60 4 -12 8 2.70 3.60 -4 12 -8 4.10 3.90 -4 12 -8 -1.70 3.00 4 12 8 2.00 4.20 -5 -12 -8 133.79 10.40 5 -12 8 139.19 12.30 5 -12 8 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77.39 10.90 -12 -12 9 113.99 13.90 12 12 -9 88.99 7.30 12 12 -9 80.99 10.60 12 12 -9 95.89 11.80 12 12 -9 111.29 8.00 -12 12 9 88.49 10.70 -12 12 9 92.99 10.70 -11 -12 9 0.70 5.10 11 -12 -9 -2.00 4.60 11 -12 -9 2.10 3.90 -11 12 9 6.20 3.60 11 12 -9 2.70 3.00 -11 12 9 -2.60 3.60 11 12 -9 5.20 4.30 11 12 -9 4.00 8.20 -10 -12 9 9.60 5.90 10 -12 -9 13.30 5.80 10 -12 -9 12.00 5.30 -10 -12 9 23.90 6.90 10 12 -9 11.80 3.50 -10 12 9 9.30 4.10 10 12 -9 4.20 3.90 10 12 -9 11.00 5.10 10 12 -9 10.00 3.40 9 -12 -9 82.09 10.20 -9 -12 9 76.09 9.70 9 -12 -9 84.29 9.90 -9 -12 9 83.09 11.10 9 12 -9 84.29 6.70 -9 12 9 79.29 9.80 9 12 -9 81.19 6.70 9 12 -9 112.59 11.50 9 12 -9 92.99 11.40 -9 12 9 94.59 9.60 8 -12 -9 112.09 14.50 -8 -12 9 73.09 9.20 8 -12 -9 89.59 10.20 -8 -12 9 94.09 12.50 8 12 -9 98.09 7.10 8 12 -9 86.39 6.90 -8 12 9 102.19 9.50 8 12 -9 90.89 10.40 8 12 -9 100.79 10.90 -8 12 9 98.19 8.70 -7 -12 9 337.77 19.00 -7 -12 9 323.77 17.20 7 -12 -9 328.77 16.80 7 -12 -9 358.86 17.50 7 12 -9 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42.40 7.20 -2 -12 -9 48.10 6.90 2 -12 9 42.40 6.60 2 12 9 54.19 7.80 -2 12 -9 60.99 7.30 -2 12 -9 56.69 7.40 3 -12 9 95.59 9.40 3 -12 9 86.19 10.00 -3 -12 -9 99.79 9.80 3 -12 9 83.69 8.90 -3 -12 -9 90.79 9.60 3 -12 9 91.79 10.60 -3 12 -9 96.69 9.50 3 12 9 99.29 10.60 -3 12 -9 101.49 8.50 -4 -12 -9 158.48 10.90 4 -12 9 161.48 11.00 4 -12 9 187.98 13.70 4 -12 9 168.58 12.50 4 -12 9 172.78 11.60 -4 -12 -9 154.28 11.20 -4 12 -9 164.88 11.10 -4 12 -9 159.28 11.10 4 12 9 181.78 12.60 5 -12 9 78.59 9.40 -5 -12 -9 64.49 8.50 5 -12 9 66.69 9.80 5 -12 9 64.39 8.10 5 -12 9 55.79 8.20 -5 -12 -9 74.29 8.50 -5 12 -9 54.19 7.70 5 12 9 58.39 9.30 6 -12 9 31.90 7.30 -6 -12 -9 31.60 6.20 6 -12 9 38.40 6.50 -6 -12 -9 32.70 10.10 6 -12 9 37.60 7.20 6 -12 9 39.00 8.70 6 12 9 47.50 8.70 -6 12 -9 43.70 6.80 -6 12 -9 33.50 6.70 -6 12 -9 32.40 6.60 7 -12 9 132.19 12.90 -7 -12 -9 106.99 14.00 -7 -12 -9 133.79 11.60 7 -12 9 138.89 12.70 -7 12 -9 131.59 14.30 -7 12 -9 143.09 10.40 7 12 9 117.89 13.20 -7 12 -9 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12 -0.50 3.70 18 -10 -12 5.10 7.00 18 -10 -12 7.60 7.40 18 10 -12 4.50 4.80 18 10 -12 -5.30 9.10 -18 10 12 -1.10 5.60 18 10 -12 -6.10 4.70 -17 -10 12 19.50 5.50 17 -10 -12 24.80 8.20 -17 -10 12 40.50 11.20 17 -10 -12 31.20 8.50 -17 10 12 22.70 6.50 17 10 -12 22.80 8.30 17 10 -12 24.40 6.40 17 10 -12 34.50 8.70 -16 -10 12 24.70 8.80 16 -10 -12 12.10 6.00 16 -10 -12 26.00 8.20 16 10 -12 19.40 6.80 16 10 -12 20.40 6.20 -16 10 12 13.70 6.10 16 10 -12 21.00 8.00 15 -10 -12 63.39 9.70 15 -10 -12 85.39 12.10 -15 -10 12 58.59 9.80 -15 -10 12 83.89 9.70 15 10 -12 81.89 8.90 15 10 -12 92.49 9.50 -15 10 12 78.09 10.20 15 10 -12 73.39 10.50 15 10 -12 82.19 11.70 14 -10 -12 8.80 6.10 14 -10 -12 6.50 4.60 -14 -10 12 14.90 8.00 14 10 -12 13.60 5.10 14 10 -12 13.00 6.00 14 10 -12 13.80 6.10 14 10 -12 5.80 3.80 -13 -10 12 43.10 9.30 13 -10 -12 35.90 8.30 13 -10 -12 24.00 7.30 13 10 -12 25.80 5.60 -13 10 12 27.40 6.10 13 10 -12 34.60 10.30 13 10 -12 29.30 5.70 13 10 -12 22.20 7.00 12 -10 -12 11.40 4.80 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-11 -15 147.99 11.70 -9 -11 15 155.48 13.60 9 11 -15 125.09 9.90 -9 11 15 163.58 11.00 -9 11 15 150.38 9.90 9 11 -15 144.39 12.10 9 11 -15 152.78 12.70 9 11 -15 165.98 10.90 8 -11 -15 51.29 8.10 8 -11 -15 30.10 6.30 -8 -11 15 38.00 7.70 -8 11 15 31.60 5.80 8 11 -15 26.90 7.20 8 11 -15 42.00 6.60 -8 11 15 27.60 4.90 8 11 -15 33.50 6.10 -7 -11 15 274.87 16.80 7 -11 -15 240.88 13.90 7 -11 -15 276.67 14.90 7 11 -15 236.38 15.70 7 11 -15 237.98 13.60 -7 11 15 242.48 13.20 7 11 -15 244.18 13.80 7 11 -15 263.67 15.50 6 -11 -15 6.30 3.70 6 -11 -15 8.50 4.50 6 -11 -15 4.80 1.90 6 -11 -15 2.00 1.80 -6 -11 15 8.00 5.30 -6 11 15 7.70 3.40 6 11 -15 4.30 4.00 6 11 -15 14.20 4.80 6 11 -15 3.20 3.80 6 11 -15 0.90 3.30 -5 -11 15 10.90 4.90 5 -11 -15 6.00 4.30 5 -11 -15 10.80 4.50 5 -11 -15 10.00 2.70 -5 -11 15 12.80 5.00 -5 -11 15 14.10 6.60 5 -11 -15 11.70 2.90 5 11 -15 11.20 5.40 5 11 -15 7.90 4.80 5 11 -15 10.50 4.30 5 11 -15 14.50 4.70 -5 11 15 14.30 4.20 -4 -11 15 80.09 10.30 4 -11 -15 70.49 8.00 -4 -11 15 74.89 10.30 -4 -11 15 41.90 7.80 4 -11 -15 59.69 7.10 -4 -11 15 60.89 8.10 4 -11 -15 74.79 7.90 4 -11 -15 67.49 5.70 4 -11 -15 71.79 6.20 4 11 -15 69.19 10.10 4 11 -15 61.89 7.90 4 11 -15 49.70 8.00 4 11 -15 53.89 7.60 -3 -11 15 1132.89 42.70 -3 -11 15 1177.68 42.10 3 -11 -15 1156.78 37.50 -3 -11 15 1147.49 42.10 3 -11 -15 1164.78 38.10 3 -11 -15 1107.19 38.50 3 -11 -15 1104.79 38.60 3 -11 -15 1172.38 38.50 -3 -11 15 1103.79 40.60 3 11 -15 1098.69 43.00 3 11 -15 1131.39 41.50 -3 11 15 1184.18 37.10 -2 -11 15 25.70 6.30 -2 -11 15 21.60 6.00 2 -11 -15 12.90 4.40 2 -11 -15 10.30 4.30 2 -11 -15 20.60 5.70 2 -11 -15 5.90 4.00 -2 -11 15 8.40 5.00 2 11 -15 22.10 6.00 -2 11 15 21.30 4.30 2 11 -15 24.60 6.60 -1 -11 15 1978.50 66.49 1 -11 -15 1958.60 62.19 -1 -11 15 2013.30 67.59 1 -11 -15 2061.29 62.19 1 -11 -15 2034.00 62.49 -1 -11 15 1973.60 66.89 1 -11 -15 1986.50 64.29 -1 -11 15 2041.80 66.29 1 -11 -15 1946.81 61.59 1 11 -15 2007.60 65.59 -1 11 15 1997.40 62.89 1 11 -15 2083.29 66.79 0 -11 15 25.40 6.50 0 -11 -15 8.90 5.00 0 -11 -15 6.20 3.50 0 -11 15 11.80 6.30 0 -11 -15 11.80 3.90 0 -11 -15 14.40 4.30 0 -11 15 27.60 6.30 0 -11 -15 12.70 5.00 0 11 -15 25.60 6.00 0 11 15 20.20 4.80 -1 -11 -15 873.31 29.10 -1 -11 -15 850.01 32.60 1 -11 15 829.92 34.20 1 -11 15 848.62 33.50 -1 -11 -15 866.11 31.10 -1 -11 -15 872.91 29.20 -1 -11 -15 826.82 28.60 1 -11 15 881.21 33.80 1 11 15 836.92 31.30 -1 11 -15 836.42 32.70 -1 11 -15 850.91 33.40 -2 -11 -15 27.30 4.40 -2 -11 -15 28.90 6.60 -2 -11 -15 31.10 5.60 -2 -11 -15 27.70 4.50 2 -11 15 19.60 6.00 2 -11 15 24.20 5.70 2 -11 15 36.60 7.40 -2 11 -15 30.70 6.50 -2 11 -15 32.70 6.40 2 11 15 19.50 5.20 -3 -11 -15 6.60 4.60 -3 -11 -15 11.70 3.40 -3 -11 -15 5.60 3.40 3 -11 15 8.50 5.40 3 -11 15 9.30 4.60 -3 -11 -15 5.00 2.90 3 11 15 0.70 3.60 -3 11 -15 9.30 7.30 -4 -11 -15 7.00 4.70 -4 -11 -15 10.00 3.20 4 -11 15 -1.10 3.90 -4 -11 -15 6.40 3.20 -4 -11 -15 6.10 3.70 4 -11 15 5.20 4.50 4 11 15 9.30 4.70 -4 11 -15 9.00 4.70 -5 -11 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2.10 5 -14 -15 -4.00 3.80 -5 -14 15 -2.70 3.50 5 14 -15 -1.60 4.30 -5 14 15 0.60 2.70 5 14 -15 2.40 4.00 5 14 -15 -1.70 3.20 4 -14 -15 11.20 3.60 4 -14 -15 18.20 5.70 4 -14 -15 19.00 5.60 4 -14 -15 16.10 4.70 -4 -14 15 24.20 7.60 -4 -14 15 13.80 5.40 4 -14 -15 16.80 3.20 4 14 -15 17.00 6.10 4 14 -15 23.60 5.90 -4 14 15 22.00 3.60 4 14 -15 25.40 5.70 -3 -14 15 -3.60 3.90 3 -14 -15 -1.10 2.20 3 -14 -15 2.20 3.00 3 -14 -15 2.20 3.90 -3 -14 15 0.40 3.90 3 -14 -15 -0.10 4.00 3 -14 -15 2.20 3.80 3 14 -15 4.50 3.70 3 14 -15 -2.10 3.50 3 14 -15 4.40 4.70 -3 14 15 -0.40 2.90 -2 -14 15 159.08 14.10 2 -14 -15 172.28 9.90 2 -14 -15 144.89 11.30 2 -14 -15 157.28 8.90 2 -14 -15 178.88 11.60 -2 -14 15 161.28 12.00 2 -14 -15 148.49 12.10 2 14 -15 154.08 12.70 2 14 -15 145.69 11.20 -2 14 15 169.48 9.60 1 -14 -15 -3.00 3.30 1 -14 -15 6.60 4.40 1 -14 -15 7.30 3.60 1 -14 -15 -0.80 3.30 -1 -14 15 4.30 6.00 -1 -14 15 4.90 4.80 1 14 -15 6.80 4.90 1 14 -15 0.90 3.30 -1 14 15 -0.10 3.10 0 -14 -15 154.28 10.50 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16 -15 -15 29.60 8.90 -16 -15 15 28.30 9.10 16 15 -15 10.00 11.80 -16 15 15 21.00 6.70 16 15 -15 23.90 5.90 16 15 -15 20.10 5.80 15 -15 -15 25.60 9.00 -15 -15 15 22.60 9.30 15 15 -15 14.80 5.60 15 15 -15 17.50 8.60 15 15 -15 23.40 6.20 15 15 -15 17.40 7.70 -15 15 15 22.30 7.00 -14 -15 15 34.70 9.80 14 -15 -15 15.70 6.60 14 -15 -15 14.30 7.70 14 15 -15 14.40 7.80 14 15 -15 17.70 7.50 -14 15 15 8.30 5.30 14 15 -15 15.10 5.00 14 15 -15 9.50 4.70 13 -15 -15 24.80 8.00 -13 -15 15 11.40 7.50 13 -15 -15 11.40 6.10 13 15 -15 13.10 7.10 -13 15 15 20.20 6.50 13 15 -15 27.40 15.90 13 15 -15 6.80 3.80 13 15 -15 15.40 5.30 12 -15 -15 37.30 8.80 -12 -15 15 33.80 9.10 12 -15 -15 33.50 8.10 12 15 -15 40.20 6.60 12 15 -15 32.90 6.30 -12 15 15 42.20 8.30 12 15 -15 41.50 9.10 12 15 -15 23.90 7.50 11 -15 -15 189.78 15.80 -11 -15 15 210.18 17.80 11 -15 -15 187.78 15.10 11 15 -15 180.98 12.00 11 15 -15 201.88 15.60 11 15 -15 191.08 12.50 11 15 -15 208.68 17.10 10 -15 -15 2.30 4.60 10 -15 -15 0.90 5.60 -10 -15 15 -4.20 5.10 10 15 -15 0.50 3.70 -10 15 15 4.70 3.60 10 15 -15 -2.50 2.90 10 15 -15 6.00 5.50 10 15 -15 -4.80 4.20 9 -15 -15 91.89 11.30 9 -15 -15 84.29 11.40 -9 -15 15 67.99 11.70 -9 15 15 65.09 8.20 9 15 -15 70.09 11.70 9 15 -15 81.99 9.20 9 15 -15 76.39 8.70 9 15 -15 79.29 11.20 8 -15 -15 6.50 5.50 8 -15 -15 1.80 5.00 -8 -15 15 9.00 5.40 8 15 -15 4.00 4.90 8 15 -15 0.80 4.50 8 15 -15 -0.70 3.50 -8 15 15 0.50 3.30 8 15 -15 3.10 4.00 7 -15 -15 -4.60 4.40 -7 -15 15 2.10 4.80 7 -15 -15 -2.50 3.80 7 15 -15 0.80 4.50 -7 15 15 2.50 3.50 7 15 -15 -1.70 3.80 7 15 -15 2.00 3.40 7 15 -15 3.10 4.10 -6 -15 15 8.60 6.00 6 -15 -15 3.00 4.10 6 -15 -15 -1.70 4.40 6 -15 -15 4.50 4.50 6 15 -15 8.40 5.50 6 15 -15 2.90 3.70 6 15 -15 5.60 4.20 -6 15 15 4.60 3.60 5 -15 -15 114.79 10.20 5 -15 -15 118.89 10.30 5 -15 -15 112.69 6.30 5 -15 -15 103.69 6.00 5 -15 -15 134.99 11.00 -5 -15 15 110.49 13.50 5 -15 -15 130.69 8.90 5 15 -15 124.69 10.00 -5 15 15 110.59 8.50 5 15 -15 115.09 11.10 5 15 -15 92.29 11.20 4 -15 -15 20.10 5.40 4 -15 -15 13.60 5.40 4 -15 -15 12.30 3.10 -4 -15 15 26.90 7.50 4 -15 -15 18.50 4.10 4 -15 -15 12.20 4.80 4 15 -15 21.10 6.30 -4 15 15 16.50 3.50 4 15 -15 17.40 5.40 4 15 -15 7.00 4.50 -3 -15 15 198.28 13.10 3 -15 -15 197.68 11.90 3 -15 -15 189.58 12.30 3 -15 -15 158.18 9.70 3 -15 -15 193.58 12.70 -3 -15 15 195.58 16.00 3 15 -15 175.48 12.30 3 15 -15 211.88 14.70 3 15 -15 192.78 12.80 -3 15 15 185.58 9.80 2 -15 -15 1.20 2.50 2 -15 -15 -2.80 5.00 2 -15 -15 3.10 4.90 2 -15 -15 2.50 2.80 -2 -15 15 -3.40 5.40 2 -15 -15 -5.00 3.30 -2 -15 15 6.80 4.50 2 15 -15 -2.50 3.00 2 15 -15 0.60 4.60 -2 15 15 5.40 3.20 1 -15 -15 83.59 8.40 1 -15 -15 96.29 7.60 -1 -15 15 78.79 10.00 1 -15 -15 75.09 8.60 -1 -15 15 94.89 12.80 1 -15 -15 109.79 10.70 1 -15 -15 72.79 5.60 -1 15 15 74.09 7.80 1 15 -15 80.09 10.40 0 -15 -15 14.70 4.80 0 -15 -15 13.70 4.30 0 -15 15 10.40 6.50 0 -15 -15 5.60 3.30 0 -15 -15 13.40 5.00 0 -15 -15 14.90 3.00 0 -15 15 10.40 5.00 0 15 15 10.10 4.20 0 15 -15 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-8 -15 -15 5.70 5.00 -8 15 -15 4.50 5.50 8 15 15 -3.90 4.80 -9 -15 -15 36.20 9.10 9 -15 15 51.09 10.50 9 -15 15 36.80 9.20 -9 15 -15 53.19 9.50 9 15 15 75.49 12.50 10 -15 15 5.00 6.10 -10 -15 -15 12.90 6.40 10 15 15 11.00 7.20 -10 15 -15 6.10 5.50 11 -15 15 6.90 6.30 11 -15 15 -0.80 2.20 -11 -15 -15 1.20 4.60 -11 15 -15 6.00 5.60 11 15 15 1.40 6.90 17 -16 -15 11.90 7.30 -17 -16 15 7.80 8.50 17 16 -15 9.40 4.90 17 16 -15 10.70 7.20 -16 -16 15 6.50 8.10 16 -16 -15 -6.60 5.40 16 16 -15 0.70 4.20 -16 16 15 0.70 2.20 16 16 -15 6.00 4.30 16 16 -15 9.10 7.50 15 -16 -15 17.70 10.00 -15 -16 15 4.20 7.50 15 -16 -15 -0.60 7.00 15 16 -15 4.30 6.20 -15 16 15 -1.30 1.90 15 16 -15 10.40 4.90 15 16 -15 0.90 3.90 14 -16 -15 115.59 13.90 -14 -16 15 123.19 17.10 14 -16 -15 112.79 15.20 14 16 -15 91.19 10.20 -14 16 15 125.89 13.80 14 16 -15 142.69 10.70 14 16 -15 122.39 17.40 13 -16 -15 75.19 12.10 -13 -16 15 89.99 14.30 13 -16 -15 80.39 11.80 13 16 -15 81.49 9.40 -13 16 15 50.49 8.60 13 16 -15 78.69 8.90 13 16 -15 98.79 15.00 13 16 -15 81.09 12.30 12 -16 -15 247.48 17.80 -12 -16 15 219.18 19.70 12 -16 -15 224.98 17.20 12 16 -15 239.78 14.00 12 16 -15 257.57 14.00 12 16 -15 220.78 18.60 12 16 -15 205.68 16.80 11 -16 -15 43.80 9.20 11 -16 -15 62.49 17.10 -11 -16 15 31.70 9.80 11 16 -15 41.20 6.90 11 16 -15 39.00 6.50 11 16 -15 36.60 8.90 11 16 -15 38.80 11.70 -10 -16 15 50.69 11.50 10 -16 -15 62.69 10.60 10 -16 -15 49.99 9.00 -10 16 15 37.80 7.10 10 16 -15 34.50 6.30 10 16 -15 36.20 9.20 10 16 -15 35.70 6.40 10 16 -15 61.39 10.40 9 -16 -15 10.90 5.40 9 -16 -15 13.00 6.10 -9 -16 15 5.60 6.70 -9 16 15 -1.00 3.20 9 16 -15 5.90 4.10 9 16 -15 3.40 5.20 9 16 -15 6.10 6.00 9 16 -15 -1.20 3.40 8 -16 -15 57.39 9.00 8 -16 -15 69.09 10.80 -8 -16 15 47.90 10.90 8 16 -15 59.89 12.30 -8 16 15 51.39 7.60 8 16 -15 47.80 7.40 8 16 -15 51.69 9.40 8 16 -15 63.69 8.10 7 -16 -15 20.20 6.10 7 -16 -15 12.00 6.00 -7 -16 15 5.90 6.30 7 -16 -15 11.50 5.30 -7 16 15 8.50 3.70 7 16 -15 7.80 4.30 7 16 -15 5.20 3.90 7 16 -15 -4.90 4.40 6 -16 -15 162.98 12.20 -6 -16 15 186.88 16.40 6 -16 -15 155.88 12.80 6 -16 -15 156.38 12.70 6 16 -15 152.98 11.20 -6 16 15 157.48 10.40 6 16 -15 132.69 10.80 6 16 -15 154.08 13.30 5 -16 -15 4.80 4.30 5 -16 -15 -1.70 3.50 5 -16 -15 0.60 3.00 5 -16 -15 8.80 4.60 -5 -16 15 1.90 5.40 5 16 -15 6.90 4.10 5 16 -15 2.00 5.00 5 16 -15 6.60 4.40 4 -16 -15 67.69 6.90 -4 -16 15 66.39 11.60 4 -16 -15 76.09 9.60 4 -16 -15 77.59 8.50 4 -16 -15 88.69 10.50 4 -16 -15 58.19 5.70 4 16 -15 77.59 10.70 4 16 -15 80.19 9.40 -4 16 15 66.19 5.60 4 16 -15 76.39 9.30 3 -16 -15 6.80 3.70 3 -16 -15 8.00 4.70 3 -16 -15 9.80 3.30 -3 -16 15 7.60 4.70 -3 -16 15 12.00 7.50 3 -16 -15 2.30 3.90 3 16 -15 5.60 5.20 3 16 -15 2.70 3.70 3 16 -15 2.30 4.20 -3 16 15 11.00 3.40 2 -16 -15 -2.40 2.50 2 -16 -15 -2.80 3.90 -2 -16 15 2.50 4.70 2 -16 -15 -6.10 3.70 2 -16 -15 0.90 2.90 2 -16 -15 2.30 2.60 -2 -16 15 3.50 5.70 -2 16 15 0.10 2.80 2 16 -15 3.00 4.90 1 -16 -15 5.90 2.30 1 -16 -15 9.20 4.70 -1 -16 15 -2.30 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12 14 -20 37.50 9.20 11 -14 -20 2.10 6.50 -11 -14 20 8.30 7.20 11 -14 -20 8.60 5.70 11 14 -20 23.80 6.90 11 14 -20 10.50 6.30 10 -14 -20 21.80 7.50 10 -14 -20 18.40 6.10 -10 -14 20 23.00 8.60 10 14 -20 24.00 6.30 10 14 -20 20.10 7.20 10 14 -20 11.10 6.90 9 -14 -20 6.50 6.50 9 -14 -20 0.60 3.70 -9 -14 20 0.70 5.00 9 14 -20 -0.40 5.20 9 14 -20 0.00 4.30 9 14 -20 0.30 6.70 8 -14 -20 119.19 11.90 8 -14 -20 118.29 12.20 -8 -14 20 90.59 12.60 8 -14 -20 119.69 12.80 8 14 -20 138.89 14.70 8 14 -20 127.69 12.80 8 14 -20 90.19 12.60 -8 14 20 106.29 11.00 7 -14 -20 16.80 5.20 7 -14 -20 14.70 5.30 -7 -14 20 7.30 6.10 7 -14 -20 24.10 6.90 7 -14 -20 12.30 5.50 7 14 -20 15.40 6.60 7 14 -20 25.50 6.60 6 -14 -20 51.19 4.90 -6 -14 20 49.10 10.20 6 -14 -20 52.99 7.70 6 -14 -20 55.69 4.80 6 -14 -20 48.50 7.30 6 -14 -20 44.70 6.90 6 -14 -20 39.80 7.90 6 14 -20 54.79 8.80 6 14 -20 48.40 9.20 5 -14 -20 31.50 6.00 5 -14 -20 20.50 5.40 -5 -14 20 32.10 9.00 5 -14 -20 20.20 4.00 5 -14 -20 17.90 5.90 5 14 -20 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17 -13 -21 40.70 10.30 17 -13 -21 44.10 11.00 17 13 -21 30.40 7.60 17 13 -21 41.70 9.30 16 -13 -21 9.40 6.40 -16 -13 21 23.20 9.40 16 -13 -21 27.40 9.30 -16 13 21 13.10 5.70 16 13 -21 6.20 6.10 16 13 -21 17.60 6.90 -15 -13 21 225.38 19.90 15 -13 -21 196.68 17.40 15 -13 -21 206.78 18.20 15 13 -21 226.48 15.60 -15 13 21 207.88 13.80 15 13 -21 183.78 21.70 15 13 -21 132.99 17.50 -14 -13 21 22.90 8.10 14 -13 -21 19.60 8.30 14 -13 -21 29.50 8.90 14 13 -21 27.30 8.60 -14 13 21 20.70 5.70 14 13 -21 13.00 6.80 14 13 -21 21.40 6.90 13 -13 -21 251.87 18.50 13 -13 -21 213.28 17.20 -13 -13 21 193.78 17.90 13 13 -21 200.38 18.50 13 13 -21 179.18 16.10 -13 13 21 198.08 12.50 13 13 -21 216.48 15.20 12 -13 -21 90.69 12.80 12 -13 -21 89.69 12.60 -12 -13 21 64.39 11.70 12 13 -21 91.39 11.00 12 13 -21 79.69 12.20 12 13 -21 53.39 10.10 -11 -13 21 21.90 7.70 11 -13 -21 33.70 8.10 11 -13 -21 23.10 7.80 11 13 -21 16.10 6.80 11 13 -21 26.50 8.00 11 13 -21 35.60 7.70 -10 -13 21 6.90 6.10 10 -13 -21 6.50 5.10 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4.20 4.90 -3 -13 21 29.50 7.40 3 -13 -21 32.60 6.60 3 -13 -21 34.40 6.20 3 -13 -21 29.80 5.70 3 -13 -21 35.60 6.50 3 13 -21 47.10 9.10 3 13 -21 27.00 7.30 2 -13 -21 -3.90 2.80 2 -13 -21 0.40 3.50 2 -13 -21 -4.50 2.80 2 -13 -21 2.30 3.10 -2 -13 21 2.80 5.00 2 13 -21 6.80 5.30 2 13 -21 -0.90 4.40 1 -13 -21 0.20 3.50 1 -13 -21 0.90 3.10 1 -13 -21 -1.70 3.30 -1 -13 21 -3.10 4.10 1 -13 -21 4.70 3.70 1 13 -21 3.50 5.00 0 -13 21 38.20 8.50 0 -13 -21 41.90 6.50 0 -13 -21 31.70 5.50 0 -13 -21 43.50 7.30 0 -13 -21 63.19 9.20 0 13 -21 31.70 8.10 -1 -13 -21 5.20 3.40 1 -13 21 -6.30 3.50 1 -13 21 5.70 5.70 -1 -13 -21 1.90 4.50 -1 -13 -21 4.90 3.70 1 13 21 6.00 4.70 -1 13 -21 -0.80 4.90 2 -13 21 273.37 18.70 -2 -13 -21 240.18 13.40 -2 -13 -21 252.27 13.30 -2 -13 -21 295.07 17.50 2 -13 21 237.18 17.40 -2 13 -21 262.17 18.20 2 13 21 276.37 16.20 -3 -13 -21 1.60 3.40 3 -13 21 1.20 4.20 3 -13 21 8.00 6.00 -3 -13 -21 3.20 3.30 3 13 21 4.90 4.80 -3 13 -21 7.50 5.70 -4 -13 -21 226.48 12.20 -4 -13 -21 234.78 12.80 4 -13 21 278.17 19.30 4 -13 21 210.18 16.40 -4 13 -21 257.27 18.00 4 13 21 267.37 16.90 -5 -13 -21 0.40 2.50 5 -13 21 -3.90 5.20 5 -13 21 0.70 2.40 -5 -13 -21 0.60 3.10 5 13 21 4.80 5.10 -5 13 -21 -0.70 5.20 -6 -13 -21 39.50 5.80 6 -13 21 42.10 9.90 6 13 21 33.30 8.10 -6 13 -21 27.50 10.00 -7 -13 -21 -1.20 2.90 7 -13 21 -1.20 4.90 7 13 21 -5.10 4.10 -7 13 -21 0.00 4.60 16 -14 -21 113.89 15.80 16 -14 -21 132.19 16.20 -16 -14 21 118.69 16.60 16 14 -21 114.99 14.50 16 14 -21 102.29 11.90 15 -14 -21 38.20 10.20 15 14 -21 30.40 7.60 15 14 -21 40.90 9.60 14 -14 -21 248.58 19.50 -14 -14 21 231.68 20.90 14 -14 -21 262.47 20.20 14 14 -21 270.87 19.00 -14 14 21 244.98 15.00 14 14 -21 319.67 38.30 14 14 -21 268.07 17.00 -13 -14 21 27.60 9.60 13 -14 -21 30.90 13.60 13 -14 -21 36.40 9.30 13 14 -21 28.50 8.40 13 14 -21 23.40 7.10 13 14 -21 19.50 7.70 -12 -14 21 131.39 17.10 12 -14 -21 135.79 15.40 12 -14 -21 127.19 14.30 12 14 -21 144.29 22.90 12 14 -21 117.19 16.30 12 14 -21 114.19 12.30 -11 -14 21 1.60 5.40 11 -14 -21 -3.10 4.10 11 -14 -21 3.90 6.50 11 14 -21 -3.10 5.10 11 14 -21 -3.60 5.10 11 14 -21 -2.40 4.50 -10 -14 21 -7.10 4.60 10 -14 -21 -3.20 4.30 10 -14 -21 -9.00 4.60 10 14 -21 0.50 5.30 10 14 -21 -2.30 4.60 10 14 -21 -0.10 4.10 9 -14 -21 12.40 6.10 -9 -14 21 15.90 7.50 9 -14 -21 22.80 6.70 9 14 -21 16.90 7.10 9 14 -21 22.80 6.90 9 14 -21 26.60 8.10 -8 -14 21 72.99 11.40 8 -14 -21 97.39 11.20 8 -14 -21 102.59 12.40 8 14 -21 104.19 13.00 8 14 -21 101.19 11.60 8 14 -21 85.29 11.90 7 -14 -21 82.19 9.20 7 -14 -21 67.99 9.00 -7 -14 21 59.49 10.80 7 -14 -21 80.89 10.70 7 -14 -21 79.09 9.70 7 14 -21 66.69 10.40 7 14 -21 85.69 11.00 6 -14 -21 118.79 9.50 6 -14 -21 101.39 6.70 6 -14 -21 110.89 9.90 6 -14 -21 86.49 9.90 6 -14 -21 113.59 12.20 -6 -14 21 92.19 14.00 6 -14 -21 115.29 6.80 6 14 -21 94.79 12.30 6 14 -21 82.59 10.90 -5 -14 21 58.89 10.80 5 -14 -21 63.79 8.80 5 -14 -21 60.69 8.00 5 -14 -21 54.99 7.80 5 -14 -21 61.29 6.20 5 -14 -21 55.99 7.20 5 14 -21 74.99 11.20 5 14 -21 43.80 8.40 4 -14 -21 15.10 4.10 4 -14 -21 5.70 4.90 4 -14 -21 8.30 3.60 4 -14 -21 10.20 4.00 -4 -14 21 9.70 6.00 4 -14 -21 16.60 5.70 4 14 -21 15.60 6.30 4 14 -21 -4.20 4.70 3 -14 -21 3.40 4.20 3 -14 -21 14.00 4.60 3 -14 -21 14.10 4.50 -3 -14 21 6.50 6.60 3 -14 -21 12.80 4.10 3 14 -21 11.80 6.40 3 14 -21 14.80 6.30 2 -14 -21 8.90 4.40 -2 -14 21 5.70 4.70 2 -14 -21 6.20 4.20 -2 -14 21 5.80 5.10 2 -14 -21 13.30 4.90 2 -14 -21 4.70 3.40 2 14 -21 4.60 5.50 2 14 -21 -2.10 4.70 -1 -14 21 30.40 8.30 1 -14 -21 24.60 5.00 1 -14 -21 23.30 5.80 -1 -14 21 11.80 6.40 1 -14 -21 12.10 5.10 1 -14 -21 19.60 5.60 1 14 -21 18.30 7.00 0 -14 -21 13.20 5.20 0 -14 -21 14.90 5.50 0 -14 -21 9.20 4.70 0 -14 21 19.50 6.70 0 -14 21 14.50 5.90 0 -14 -21 13.00 4.20 0 14 -21 19.90 7.20 1 -14 21 35.00 8.90 -1 -14 -21 43.20 14.00 -1 -14 -21 40.20 5.80 -1 -14 -21 41.70 6.50 -1 14 -21 32.30 8.20 -2 -14 -21 3.30 3.60 -2 -14 -21 2.40 5.10 2 -14 21 2.40 5.10 -2 -14 -21 9.00 3.50 -2 14 -21 11.30 6.10 2 14 21 13.10 5.10 -3 -14 -21 36.90 5.30 3 -14 21 27.00 7.90 -3 -14 -21 27.50 5.20 3 14 21 27.80 7.20 -3 14 -21 32.70 8.60 -4 -14 -21 13.70 3.90 4 -14 21 16.70 8.10 4 14 21 16.70 6.00 5 -14 21 -1.00 2.10 5 -14 21 3.10 5.90 -5 -14 -21 4.30 3.20 5 14 21 5.00 4.70 -5 14 -21 10.30 6.40 6 -14 21 24.30 7.90 -6 -14 -21 16.80 4.00 -6 14 -21 6.20 5.60 6 14 21 15.10 6.10 -14 -15 21 -0.60 6.30 14 -15 -21 8.80 6.90 14 -15 -21 18.80 8.10 14 15 -21 10.50 6.30 14 15 -21 -0.60 4.90 -13 -15 21 -3.90 6.60 13 -15 -21 3.30 7.20 13 -15 -21 0.30 6.40 13 15 -21 10.80 6.50 13 15 -21 7.30 5.30 -12 -15 21 7.90 7.00 12 -15 -21 30.50 8.40 12 -15 -21 26.90 8.60 12 15 -21 28.10 7.90 12 15 -21 24.40 6.70 11 -15 -21 27.00 7.90 -11 -15 21 36.10 11.00 11 -15 -21 18.60 7.30 11 15 -21 17.90 8.50 11 15 -21 26.80 8.10 11 15 -21 28.60 7.00 -10 -15 21 10.20 6.70 10 -15 -21 18.50 7.10 10 -15 -21 17.80 7.30 10 15 -21 11.50 8.00 10 15 -21 -3.00 5.10 10 15 -21 9.30 5.50 9 -15 -21 0.20 4.60 -9 -15 21 -2.80 5.40 9 -15 -21 -8.60 4.70 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4 -22 190.58 14.20 -13 -4 22 23.20 7.10 13 -4 -22 27.20 4.70 13 -4 -22 22.10 6.40 13 -4 -22 19.80 6.60 -13 4 22 16.30 5.10 -13 4 22 19.90 4.60 13 4 -22 22.00 6.70 13 4 -22 16.80 6.00 13 4 -22 32.70 6.60 12 -4 -22 11.50 5.40 -12 -4 22 11.70 5.20 12 -4 -22 -1.30 4.10 12 -4 -22 6.80 3.20 12 -4 -22 3.40 3.30 -12 4 22 6.10 3.30 12 4 -22 2.00 4.20 12 4 -22 -1.70 3.40 12 4 -22 8.00 4.90 11 -4 -22 0.30 3.90 -11 -4 22 7.50 4.40 -11 -4 22 14.50 5.60 11 -4 -22 5.70 3.20 11 -4 -22 9.00 3.70 11 -4 -22 -0.50 4.00 11 4 -22 10.30 5.40 -11 4 22 7.60 3.30 11 4 -22 2.30 3.70 11 4 -22 6.50 4.30 10 -4 -22 18.90 5.70 10 -4 -22 20.50 5.60 -10 -4 22 25.60 6.10 10 -4 -22 17.10 4.30 10 -4 -22 24.00 4.60 -10 -4 22 30.40 7.00 10 4 -22 18.40 5.00 10 4 -22 23.70 5.80 10 4 -22 21.40 6.20 -10 4 22 20.30 3.80 9 -4 -22 71.69 8.30 9 -4 -22 63.49 7.00 -9 -4 22 77.79 10.50 9 -4 -22 67.39 7.30 -9 -4 22 52.59 8.10 9 4 -22 58.29 8.00 9 4 -22 59.29 8.50 9 4 -22 53.39 8.20 8 -4 -22 26.30 5.00 8 -4 -22 23.00 4.70 -8 -4 22 25.00 5.90 -8 -4 22 23.20 5.90 8 -4 -22 21.20 5.80 8 -4 -22 22.70 4.70 8 4 -22 23.40 5.90 8 4 -22 20.30 5.40 8 4 -22 24.80 6.20 7 -4 -22 2.70 3.10 7 -4 -22 4.90 4.40 7 -4 -22 2.30 3.10 7 -4 -22 3.90 4.80 -7 -4 22 6.60 3.80 -7 -4 22 3.50 3.50 7 -4 -22 0.50 2.50 7 4 -22 5.40 4.20 7 4 -22 2.50 3.50 7 4 -22 5.50 4.20 6 -4 -22 -2.70 2.20 6 -4 -22 -0.70 3.60 -6 -4 22 4.40 3.50 -6 -4 22 -0.90 2.90 6 -4 -22 4.50 3.40 6 -4 -22 3.70 3.40 6 4 -22 4.10 3.10 6 4 -22 0.60 3.50 6 4 -22 -2.80 3.50 5 -4 -22 44.50 7.00 -5 -4 22 52.19 10.20 5 -4 -22 36.40 6.00 5 -4 -22 53.19 7.00 5 -4 -22 40.40 7.20 5 4 -22 30.80 6.30 5 4 -22 28.90 6.60 5 4 -22 46.00 6.80 -4 -4 22 16.50 4.70 4 -4 -22 13.80 5.00 4 -4 -22 14.00 4.20 4 -4 -22 9.90 4.00 4 -4 -22 15.10 4.50 4 4 -22 5.00 4.50 4 4 -22 15.40 4.50 4 4 -22 9.00 4.50 3 -4 -22 199.68 12.00 -3 -4 22 192.88 11.50 3 -4 -22 187.58 12.00 3 -4 -22 176.38 12.20 3 -4 -22 203.68 13.20 3 4 -22 175.78 13.30 3 4 -22 211.18 15.50 -2 -4 22 2.00 4.10 2 -4 -22 7.00 3.90 -2 -4 22 1.40 4.50 2 -4 -22 3.40 4.00 2 -4 -22 1.70 3.40 2 -4 -22 1.40 2.90 2 4 -22 -5.70 3.50 2 4 -22 5.00 5.40 1 -4 -22 69.49 8.60 1 -4 -22 71.49 9.20 -1 -4 22 62.59 9.70 1 -4 -22 76.79 9.70 1 -4 -22 70.49 8.90 -1 -4 22 84.89 8.00 1 4 -22 62.79 9.50 1 4 -22 63.29 9.30 0 -4 -22 -3.90 3.30 0 -4 -22 1.90 3.40 0 -4 -22 0.70 4.10 0 -4 -22 -3.80 2.40 0 -4 22 -0.30 2.70 0 -4 22 10.00 5.20 0 4 -22 3.00 4.20 -1 -4 -22 37.40 7.40 1 -4 22 25.10 4.80 1 -4 22 19.60 6.70 -1 -4 -22 27.60 6.50 -1 -4 -22 34.90 6.50 -1 4 -22 12.70 5.60 2 -4 22 3.40 2.80 2 -4 22 4.80 5.00 -2 -4 -22 10.30 5.00 -2 4 -22 13.50 5.60 3 -4 22 99.79 12.50 -3 -4 -22 91.99 11.40 -3 -4 -22 98.69 10.80 3 -4 22 92.89 7.40 -3 4 -22 105.59 11.80 4 -4 22 35.10 5.20 -4 -4 -22 35.40 7.90 4 -4 22 33.50 7.80 -4 4 -22 39.10 8.30 5 -4 22 219.98 16.40 5 -4 22 215.48 11.70 -5 -4 -22 240.98 16.70 -5 4 -22 226.18 16.20 5 4 22 224.98 15.30 6 -4 22 83.29 8.20 6 -4 22 75.09 11.20 -6 -4 -22 80.99 11.50 -6 4 -22 59.09 10.20 6 4 22 69.79 10.10 7 -4 22 157.28 10.00 -7 -4 -22 156.68 16.40 7 -4 22 143.99 15.20 7 4 22 156.68 13.60 -7 4 -22 159.98 16.40 8 -4 22 62.49 11.10 -8 -4 -22 77.39 12.00 8 -4 22 75.39 8.10 8 4 22 91.59 12.00 -8 4 -22 78.19 11.70 9 -4 22 86.79 8.20 -9 -4 -22 155.38 17.00 9 -4 22 98.79 13.70 9 4 22 122.59 13.70 -9 4 -22 110.09 14.20 -9 4 -22 112.29 11.80 -10 -4 -22 57.09 11.20 10 -4 22 74.19 11.80 -10 4 -22 59.49 11.10 -10 4 -22 76.59 10.10 10 4 22 74.29 10.90 11 -4 22 79.99 10.60 -11 -4 -22 71.29 13.60 -11 4 -22 64.59 9.50 11 4 22 84.79 12.10 -11 4 -22 73.69 12.10 12 -4 22 28.30 6.00 -12 -4 -22 20.80 9.10 -12 -4 -22 32.10 6.10 12 -4 22 31.30 8.60 -12 4 -22 32.30 7.30 -12 4 -22 24.30 8.40 12 4 22 24.10 7.50 22 -5 -22 -8.30 6.30 22 -5 -22 -0.60 2.90 -22 -5 22 6.60 5.40 22 5 -22 7.60 6.10 -22 5 22 4.00 3.10 21 -5 -22 145.49 17.70 21 -5 -22 144.29 9.20 -21 -5 22 127.79 17.70 21 -5 -22 174.28 21.70 21 5 -22 150.78 16.10 21 5 -22 123.19 13.80 21 5 -22 139.19 18.60 20 -5 -22 7.20 13.70 20 -5 -22 3.00 6.60 20 -5 -22 3.90 3.30 -20 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15.10 6.50 -6 5 -22 7.20 5.80 6 5 22 3.40 4.80 7 -5 22 11.70 6.00 -7 -5 -22 0.50 5.10 7 -5 22 4.70 3.50 7 5 22 9.60 5.70 -7 5 -22 11.10 6.30 8 -5 22 4.10 3.60 -8 -5 -22 7.50 6.30 8 -5 22 -2.10 5.60 8 5 22 0.50 5.00 -8 5 -22 -1.10 5.20 9 -5 22 4.70 3.70 9 -5 22 13.60 6.50 -9 -5 -22 1.40 5.60 -9 5 -22 11.70 6.60 9 5 22 22.60 7.00 10 -5 22 19.90 5.30 -10 -5 -22 37.80 9.80 10 -5 22 33.70 9.60 10 5 22 18.40 7.00 -10 5 -22 35.00 14.80 11 -5 22 28.50 6.30 -11 -5 -22 36.20 10.20 11 -5 22 59.19 11.00 -11 5 -22 43.50 9.80 -11 5 -22 39.40 8.00 11 5 22 51.09 9.50 12 -5 22 76.09 12.40 -12 -5 -22 76.79 13.70 -12 -5 -22 78.19 8.20 -12 5 -22 63.59 11.50 -12 5 -22 49.99 8.90 12 5 22 89.09 12.20 -22 -6 22 2.40 3.10 22 -6 -22 -2.80 6.20 22 6 -22 2.90 5.90 21 -6 -22 1.80 6.70 -21 -6 22 6.20 7.20 21 -6 -22 -3.10 6.10 21 6 -22 -2.20 5.50 -21 6 22 1.90 2.40 21 6 -22 6.10 6.00 -20 -6 22 10.80 6.20 20 -6 -22 9.40 3.00 20 -6 -22 3.00 6.60 20 -6 -22 12.00 8.00 20 6 -22 19.10 7.10 20 6 -22 10.20 7.10 -20 6 22 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6 22 66.39 8.30 14 6 -22 49.20 8.80 14 6 -22 61.79 10.30 13 -6 -22 33.50 8.30 -13 -6 22 42.20 9.00 13 -6 -22 33.30 4.70 13 -6 -22 36.60 7.70 -13 6 22 46.00 6.90 13 6 -22 30.70 7.70 13 6 -22 39.30 8.30 13 6 -22 23.40 6.60 -12 -6 22 406.36 22.60 12 -6 -22 464.05 22.30 12 -6 -22 370.86 16.10 12 -6 -22 367.36 20.70 -12 6 22 414.56 17.20 12 6 -22 393.66 21.20 12 6 -22 446.86 21.30 12 6 -22 431.66 26.80 11 -6 -22 170.38 23.60 -11 -6 22 147.59 15.00 11 -6 -22 141.49 8.60 11 -6 -22 157.18 12.90 11 -6 -22 127.89 8.60 11 6 -22 166.98 13.00 -11 6 22 140.19 8.50 11 6 -22 131.69 12.00 11 6 -22 141.29 11.90 10 -6 -22 334.17 14.50 10 -6 -22 322.57 18.30 10 -6 -22 358.36 18.00 -10 -6 22 314.57 19.00 10 6 -22 397.86 19.80 10 6 -22 340.27 18.90 10 6 -22 348.77 18.70 9 -6 -22 324.57 13.90 -9 -6 22 282.67 17.30 9 -6 -22 297.57 13.90 9 -6 -22 284.37 15.40 9 6 -22 321.17 17.30 9 6 -22 296.17 17.30 9 6 -22 318.97 17.50 -8 -6 22 122.49 11.10 8 -6 -22 124.89 10.90 8 -6 -22 129.79 9.30 8 -6 -22 137.29 8.80 8 -6 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9.40 1 -6 -22 63.49 8.40 -1 -6 22 92.79 11.20 1 -6 -22 74.19 8.90 1 -6 -22 68.49 9.00 -1 -6 22 85.39 9.30 1 6 -22 87.49 10.90 0 -6 22 1.10 4.50 0 -6 22 0.30 4.50 0 -6 -22 1.60 3.40 0 -6 -22 3.10 4.20 0 -6 -22 0.70 3.80 0 -6 -22 1.80 3.60 0 6 -22 3.20 4.70 -1 -6 -22 160.68 11.60 -1 -6 -22 154.28 12.30 -1 -6 -22 157.08 11.80 1 -6 22 161.68 13.70 1 -6 22 152.78 10.60 -1 -6 -22 196.58 22.90 -1 6 -22 170.58 13.20 2 -6 22 2.60 5.00 2 -6 22 6.80 3.80 -2 -6 -22 16.40 5.40 -2 -6 -22 1.60 3.40 -2 6 -22 10.10 5.50 -3 -6 -22 125.39 13.30 -3 -6 -22 124.59 10.80 3 -6 22 99.49 12.40 -3 -6 -22 114.69 11.50 -3 6 -22 113.29 12.60 -4 -6 -22 -6.30 4.50 4 -6 22 -1.30 3.30 4 -6 22 2.20 5.20 -4 -6 -22 2.20 4.20 -4 6 -22 0.50 4.30 5 -6 22 -3.40 2.90 -5 -6 -22 4.00 5.00 5 -6 22 1.00 5.10 -5 -6 -22 -3.10 4.30 -5 6 -22 2.40 5.10 6 -6 22 -1.40 3.00 -6 -6 -22 -2.50 4.90 -6 -6 -22 -7.00 3.20 6 -6 22 1.70 4.90 6 6 22 5.90 4.90 -6 6 -22 5.10 5.20 -7 -6 -22 40.40 7.70 -7 -6 -22 21.40 7.80 7 -6 22 30.30 6.20 7 -6 22 22.40 7.60 -7 6 -22 20.20 7.20 7 6 22 31.40 7.40 -8 -6 -22 8.40 6.00 8 -6 22 0.50 3.20 8 -6 22 -4.80 4.50 8 6 22 -1.20 4.60 -8 6 -22 -1.20 4.90 9 -6 22 16.90 5.30 9 -6 22 25.90 7.90 -9 -6 -22 27.20 8.60 -9 6 -22 20.20 7.50 9 6 22 12.70 5.70 10 -6 22 0.80 6.60 10 -6 22 3.50 3.70 -10 -6 -22 -0.40 6.30 10 6 22 -3.40 4.30 -10 6 -22 0.10 4.20 -10 6 -22 -5.80 5.30 11 -6 22 2.20 5.80 -11 -6 -22 10.80 7.70 11 -6 22 -1.70 3.20 -11 6 -22 -3.60 4.90 11 6 22 -5.60 4.00 -11 6 -22 1.80 4.80 22 7 -22 0.30 5.70 21 -7 -22 71.89 13.30 -21 -7 22 70.19 12.80 21 7 -22 61.69 10.60 21 7 -22 79.19 11.60 20 -7 -22 3.20 6.80 -20 -7 22 3.80 6.20 20 7 -22 1.40 4.90 20 7 -22 3.90 5.80 20 7 -22 10.80 7.60 -20 7 22 4.40 5.50 19 -7 -22 9.90 7.10 19 -7 -22 -3.10 5.80 -19 -7 22 1.30 5.50 19 7 -22 2.00 4.70 19 7 -22 -2.00 5.00 19 7 -22 -2.50 5.00 -19 7 22 -5.10 4.10 -18 -7 22 0.30 5.40 18 -7 -22 -4.60 5.40 18 -7 -22 -3.20 5.00 18 7 -22 -0.60 5.20 -18 7 22 -4.60 4.40 18 7 -22 -2.10 4.70 18 7 -22 7.70 5.70 17 -7 -22 97.09 13.80 -17 -7 22 72.89 12.10 17 -7 -22 68.39 12.00 17 7 -22 70.29 10.30 17 7 -22 70.79 10.20 17 7 -22 71.19 11.90 -17 7 22 65.99 9.50 16 -7 -22 42.80 9.30 -16 -7 22 43.50 9.80 16 -7 -22 43.20 10.40 16 7 -22 36.10 8.20 16 7 -22 58.79 10.90 -16 7 22 30.30 8.40 16 7 -22 50.99 9.20 15 -7 -22 101.69 13.10 15 -7 -22 117.49 6.20 -15 -7 22 131.59 15.90 15 -7 -22 116.69 14.60 15 7 -22 104.59 11.80 15 7 -22 101.69 12.20 15 7 -22 113.29 14.00 -15 7 22 117.59 9.90 14 -7 -22 44.20 4.60 14 -7 -22 49.50 9.40 14 -7 -22 51.69 5.00 14 -7 -22 49.30 9.30 14 7 -22 63.39 10.30 14 7 -22 56.59 9.10 14 7 -22 34.70 8.50 13 -7 -22 4.90 6.00 13 -7 -22 2.00 2.70 13 -7 -22 -0.80 2.40 13 -7 -22 12.60 5.40 -13 -7 22 -3.60 4.20 13 7 -22 -1.40 4.90 13 7 -22 4.10 5.40 13 7 -22 1.50 5.00 -13 7 22 1.40 3.30 12 -7 -22 52.69 9.20 12 -7 -22 57.29 5.40 12 -7 -22 58.09 9.60 -12 -7 22 45.60 9.30 12 -7 -22 51.99 5.40 12 7 -22 49.99 8.50 -12 7 22 53.49 6.50 12 7 -22 47.90 8.50 12 7 -22 52.09 9.10 -11 -7 22 396.56 22.10 11 -7 -22 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22 12.40 6.30 -2 -7 -22 33.70 11.40 -2 -7 -22 33.00 6.70 2 -7 22 17.40 8.20 -2 -7 -22 30.60 6.70 -2 7 -22 36.00 8.20 -3 -7 -22 11.40 4.80 -3 -7 -22 9.50 5.40 -3 -7 -22 5.50 4.10 3 -7 22 3.00 3.80 3 -7 22 9.00 5.50 -3 7 -22 2.10 4.80 -4 -7 -22 31.10 7.80 4 -7 22 49.60 7.70 -4 -7 -22 44.40 7.20 -4 -7 -22 46.10 7.70 4 -7 22 61.89 10.30 -4 7 -22 28.00 7.60 5 -7 22 -5.00 4.70 5 -7 22 -3.30 4.30 -5 -7 -22 4.50 4.20 -5 -7 -22 -7.70 4.10 -5 7 -22 1.50 4.60 6 -7 22 0.30 5.00 -6 -7 -22 2.80 5.60 -6 7 -22 -8.60 3.40 -7 -7 -22 1.00 5.00 7 -7 22 -2.10 4.60 -7 -7 -22 4.10 4.20 7 -7 22 -2.10 2.80 -7 7 -22 -5.80 4.30 7 7 22 -0.10 3.90 -8 -7 -22 0.00 5.50 8 -7 22 2.70 3.40 8 -7 22 0.60 5.10 -8 -7 -22 5.10 4.20 -8 7 -22 -2.40 4.30 8 7 22 -1.10 3.90 9 -7 22 3.50 3.60 -9 -7 -22 9.90 6.90 -9 7 -22 3.90 5.70 9 7 22 -0.50 5.20 9 7 22 1.50 4.40 10 -7 22 14.60 7.00 10 -7 22 6.00 4.60 10 7 22 13.10 5.90 -10 7 -22 14.70 6.70 11 -7 22 4.90 6.20 -11 -7 -22 10.70 7.90 -11 7 -22 13.40 7.30 -11 7 -22 3.10 5.20 11 7 22 7.90 6.30 11 7 22 5.40 5.40 -21 -8 22 15.50 7.90 21 -8 -22 0.50 6.90 21 8 -22 -8.80 4.20 21 8 -22 6.00 5.70 20 -8 -22 22.20 8.70 -20 -8 22 30.40 9.10 20 -8 -22 31.50 10.30 20 8 -22 27.50 8.00 20 8 -22 24.30 7.80 -19 -8 22 6.10 6.70 19 -8 -22 -6.80 4.70 19 -8 -22 -4.50 6.00 -19 8 22 6.70 5.50 19 8 -22 4.00 5.70 19 8 -22 -5.80 5.00 19 8 -22 4.70 6.10 18 -8 -22 -2.60 6.30 18 -8 -22 -10.80 4.30 -18 -8 22 -1.20 5.20 18 8 -22 -2.60 4.70 18 8 -22 -3.70 4.60 18 8 -22 2.10 5.10 -18 8 22 -4.30 3.90 17 -8 -22 5.40 7.00 17 -8 -22 4.30 6.50 -17 -8 22 20.30 7.90 -17 8 22 9.30 5.20 17 8 -22 6.70 5.20 17 8 -22 9.40 6.50 17 8 -22 15.30 6.50 -16 -8 22 45.50 9.90 16 -8 -22 56.49 10.70 16 -8 -22 46.90 10.00 16 8 -22 61.79 11.70 16 8 -22 58.69 9.50 16 8 -22 59.49 9.80 -16 8 22 73.39 9.80 15 -8 -22 17.50 7.00 -15 -8 22 9.20 6.60 15 -8 -22 9.10 6.50 15 8 -22 3.50 5.40 15 8 -22 6.20 5.60 15 8 -22 11.60 6.00 14 -8 -22 98.09 12.80 -14 -8 22 75.19 12.00 14 -8 -22 75.39 11.00 14 8 -22 106.09 13.70 14 8 -22 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30.20 5.00 7 8 -22 43.20 8.00 7 8 -22 40.00 7.80 7 8 -22 24.80 6.80 6 -8 -22 10.70 5.00 6 -8 -22 3.40 3.20 6 -8 -22 6.70 4.60 -6 -8 22 2.10 4.30 6 -8 -22 3.70 3.50 6 8 -22 6.20 5.00 6 8 -22 2.50 4.40 6 8 -22 -2.30 4.40 5 -8 -22 141.89 11.30 5 -8 -22 186.08 10.90 -5 -8 22 153.08 12.30 5 -8 -22 168.48 10.20 5 -8 -22 148.59 11.60 5 8 -22 165.28 12.60 5 8 -22 160.48 12.80 5 8 -22 168.08 13.30 4 -8 -22 6.10 4.00 4 -8 -22 6.10 3.70 -4 -8 22 0.00 3.80 4 -8 -22 3.60 4.20 4 -8 -22 12.20 4.30 4 8 -22 11.00 5.50 4 8 -22 11.70 5.40 3 -8 -22 77.99 8.70 3 -8 -22 69.19 8.20 3 -8 -22 66.49 8.50 3 -8 -22 68.69 8.70 -3 -8 22 69.89 9.90 3 8 -22 63.39 9.80 3 8 -22 72.29 9.80 2 -8 -22 2.20 3.40 -2 -8 22 2.00 4.30 2 -8 -22 -4.60 3.00 2 -8 -22 0.30 3.70 2 -8 -22 -1.20 3.10 -2 -8 22 -0.50 3.50 2 8 -22 7.20 4.90 2 8 -22 1.70 4.40 1 -8 -22 2.30 3.50 -1 -8 22 1.90 3.50 1 -8 -22 -3.00 3.20 1 -8 -22 -2.00 2.70 1 -8 -22 -2.90 3.20 -1 -8 22 -4.40 3.60 1 8 -22 2.90 4.90 0 -8 22 9.00 5.90 0 -8 -22 5.20 4.00 0 -8 -22 -0.50 3.20 0 -8 22 9.50 4.30 0 -8 -22 8.20 4.60 0 -8 -22 1.40 4.00 0 8 -22 4.30 4.90 1 -8 22 53.79 8.00 -1 -8 -22 30.30 6.50 -1 -8 -22 45.80 7.30 1 -8 22 39.60 8.60 -1 -8 -22 43.10 7.10 -1 8 -22 51.59 8.60 2 -8 22 -5.60 4.60 2 -8 22 4.00 4.00 -2 -8 -22 0.50 3.70 -2 -8 -22 0.30 3.50 -2 -8 -22 6.90 5.00 -2 8 -22 3.50 4.80 -3 -8 -22 58.49 9.00 -3 -8 -22 55.69 7.60 3 -8 22 59.59 8.50 3 -8 22 54.09 9.90 -3 -8 -22 63.99 8.50 -3 8 -22 63.09 9.80 -4 -8 -22 0.50 3.10 4 -8 22 -1.40 5.20 -4 -8 -22 2.60 5.10 4 -8 22 -1.30 3.60 -4 -8 -22 1.20 3.90 -4 8 -22 9.10 5.50 -5 -8 -22 7.50 4.00 5 -8 22 -3.20 4.50 -5 -8 -22 5.80 4.40 -5 -8 -22 7.60 5.50 -5 8 -22 0.60 4.60 -6 -8 -22 -2.00 4.60 -6 -8 -22 -0.90 3.80 6 -8 22 -5.80 4.10 6 -8 22 -2.50 3.30 -6 8 -22 5.40 5.50 7 -8 22 -0.70 4.80 -7 -8 -22 3.20 6.00 7 -8 22 5.20 4.10 7 8 22 1.90 4.60 -7 8 -22 7.50 5.80 -8 -8 -22 2.30 3.90 8 -8 22 6.30 6.40 -8 -8 -22 10.90 6.60 -8 8 -22 -2.00 4.80 8 8 22 -1.70 4.30 9 -8 22 4.10 5.50 -9 -8 -22 6.60 6.20 -9 -8 -22 7.50 4.50 9 -8 22 0.00 3.50 9 8 22 -0.80 3.80 -9 8 -22 5.70 7.00 9 8 22 -2.30 4.10 -10 -8 -22 10.50 7.30 -10 -8 -22 12.30 4.80 10 -8 22 12.00 7.20 10 8 22 18.20 7.90 10 8 22 7.20 5.40 -10 8 -22 22.40 8.10 -20 -9 22 15.50 8.40 20 -9 -22 10.00 7.80 20 9 -22 14.60 6.90 20 9 -22 28.80 10.20 19 -9 -22 7.00 9.30 -19 -9 22 10.40 6.50 19 -9 -22 6.00 7.50 -19 9 22 -1.90 4.20 19 9 -22 2.50 6.10 19 9 -22 -3.20 5.50 18 -9 -22 10.00 7.30 18 -9 -22 5.90 7.10 -18 -9 22 7.10 6.40 18 9 -22 3.80 5.20 18 9 -22 9.30 6.40 18 9 -22 10.60 7.80 -18 9 22 6.80 5.00 -17 -9 22 11.40 6.30 17 -9 -22 37.40 9.90 17 -9 -22 29.70 9.60 -17 9 22 12.10 7.50 17 9 -22 18.00 6.50 17 9 -22 18.10 7.10 17 9 -22 20.70 8.00 16 -9 -22 -0.40 5.20 -16 -9 22 3.10 5.80 16 -9 -22 1.10 5.60 16 9 -22 0.40 5.00 16 9 -22 0.00 5.20 -16 9 22 5.40 4.70 16 9 -22 -1.20 5.00 15 -9 -22 -6.80 4.50 -15 -9 22 6.60 5.60 15 -9 -22 -2.20 5.30 -15 9 22 -0.30 3.10 15 9 -22 -0.50 5.30 15 9 -22 -2.50 4.10 15 9 -22 -1.50 4.40 14 -9 -22 3.20 6.00 14 -9 -22 11.90 6.50 -14 -9 22 20.70 8.20 14 9 -22 13.50 6.60 -14 9 22 8.80 3.80 14 9 -22 5.30 5.80 14 9 -22 14.60 6.30 13 -9 -22 103.39 13.00 13 -9 -22 117.09 14.00 -13 -9 22 100.39 13.20 13 9 -22 109.99 12.60 13 9 -22 106.09 14.20 -13 9 22 103.49 8.40 13 9 -22 123.89 12.70 12 -9 -22 14.60 7.00 12 -9 -22 4.80 5.30 -12 9 22 21.80 4.40 12 9 -22 16.60 6.70 12 9 -22 12.10 6.20 12 9 -22 11.20 6.50 11 -9 -22 374.86 20.50 11 -9 -22 415.16 21.90 11 -9 -22 376.26 13.80 11 9 -22 420.86 21.70 11 9 -22 417.06 21.70 11 9 -22 370.36 21.90 -11 9 22 387.26 15.90 10 -9 -22 402.96 16.10 10 -9 -22 421.46 21.10 10 -9 -22 443.06 22.20 -10 -9 22 417.66 23.60 10 -9 -22 404.06 15.30 10 9 -22 452.35 22.30 10 9 -22 412.36 22.80 10 9 -22 455.75 22.70 9 -9 -22 287.07 16.40 -9 -9 22 309.97 19.30 9 -9 -22 285.97 13.10 9 -9 -22 303.07 17.70 9 -9 -22 279.97 12.20 9 9 -22 292.87 18.60 9 9 -22 290.37 18.20 9 9 -22 311.17 18.30 8 -9 -22 740.53 33.00 8 -9 -22 699.43 25.40 -8 -9 22 643.84 30.60 8 -9 -22 677.83 27.40 8 9 -22 725.63 31.40 8 9 -22 707.13 30.60 8 9 -22 748.53 30.70 -7 -9 22 36.90 7.80 7 -9 -22 36.50 5.20 7 -9 -22 30.90 5.80 7 -9 -22 43.60 7.50 7 9 -22 58.09 9.10 7 9 -22 40.40 8.10 7 9 -22 30.70 11.10 6 -9 -22 228.48 14.10 6 -9 -22 217.18 14.00 6 -9 -22 221.98 11.50 6 -9 -22 220.88 12.20 -6 -9 22 199.48 14.70 6 9 -22 224.58 15.30 6 9 -22 225.58 15.30 6 9 -22 202.88 14.90 5 -9 -22 3.50 3.70 5 -9 -22 7.30 3.70 -5 -9 22 9.80 5.00 5 -9 -22 3.30 4.20 5 -9 -22 7.60 3.60 5 9 -22 3.70 4.60 5 9 -22 7.40 5.20 4 -9 -22 4.70 3.40 4 -9 -22 5.60 3.50 -4 -9 22 -0.10 4.10 4 -9 -22 -1.40 3.70 4 -9 -22 3.90 3.80 4 9 -22 0.30 4.50 4 9 -22 -2.60 4.20 3 -9 -22 5.50 3.60 3 -9 -22 1.40 3.90 3 -9 -22 -0.80 3.20 -3 -9 22 -1.00 3.70 3 -9 -22 8.90 4.00 3 9 -22 1.00 4.40 3 9 -22 0.80 4.30 2 -9 -22 78.69 9.30 2 -9 -22 80.09 9.10 2 -9 -22 82.19 9.10 -2 -9 22 86.39 10.20 2 -9 -22 61.19 8.40 -2 -9 22 66.29 10.00 2 9 -22 57.09 9.50 2 9 -22 78.89 10.60 1 -9 -22 -1.30 2.70 1 -9 -22 1.70 3.30 -1 -9 22 4.30 5.00 1 -9 -22 3.30 4.00 1 -9 -22 4.10 4.10 -1 -9 22 -0.40 3.80 1 9 -22 0.90 4.70 0 -9 22 19.10 6.50 0 -9 -22 37.70 6.90 0 -9 -22 20.70 5.40 0 -9 -22 24.80 5.50 0 -9 22 28.60 6.40 0 -9 -22 16.50 5.00 0 9 -22 30.00 7.30 -1 -9 -22 2.80 3.80 -1 -9 -22 6.80 3.90 -1 -9 -22 -4.90 3.50 1 -9 22 9.60 4.50 1 -9 22 2.30 5.20 -1 9 -22 8.60 5.10 -2 -9 -22 15.90 4.60 -2 -9 -22 7.40 4.60 2 -9 22 11.90 6.10 -2 -9 -22 3.00 4.70 2 -9 22 18.70 6.00 -2 9 -22 14.90 6.40 -3 -9 -22 1.30 3.80 3 -9 22 0.50 3.80 -3 -9 -22 4.70 5.30 3 -9 22 -1.40 4.70 -3 -9 -22 -5.80 2.30 -3 9 -22 13.10 6.20 4 -9 22 -8.80 3.00 4 -9 22 -6.70 3.90 -4 -9 -22 7.80 5.10 -4 -9 -22 -2.80 3.70 -4 -9 -22 4.50 3.70 -4 9 -22 -0.90 4.30 5 -9 22 -3.90 4.70 -5 -9 -22 -2.80 4.40 5 -9 22 -3.60 3.40 -5 -9 -22 -7.20 3.10 -5 -9 -22 1.50 3.10 -5 9 -22 6.30 5.30 -6 -9 -22 3.10 4.10 6 -9 22 0.90 3.60 -6 -9 -22 7.90 5.80 -6 -9 -22 2.80 3.60 6 -9 22 1.10 5.40 6 9 22 0.80 4.50 -6 9 -22 14.00 6.50 -7 -9 -22 11.80 4.80 -7 -9 -22 8.30 5.90 7 -9 22 6.10 5.50 7 9 22 19.70 6.80 -7 9 -22 12.30 5.80 8 -9 22 2.30 5.40 8 -9 22 6.40 4.60 -8 -9 -22 15.00 7.10 8 9 22 4.20 5.60 -8 9 -22 3.00 8.30 9 -9 22 24.60 7.50 -9 -9 -22 6.90 4.50 9 -9 22 16.00 7.00 -9 -9 -22 15.20 7.80 9 9 22 14.90 7.20 -9 9 -22 6.50 6.30 10 -9 22 3.30 6.30 -10 -9 -22 7.90 4.80 -10 -9 -22 -1.40 5.20 -10 9 -22 -9.10 4.00 10 9 22 1.00 4.70 20 -10 -22 8.80 8.30 -20 -10 22 16.70 7.70 20 10 -22 20.40 8.00 20 10 -22 7.40 6.20 -19 -10 22 -6.00 5.70 19 -10 -22 -2.00 7.50 19 -10 -22 -10.50 4.70 19 10 -22 8.90 9.90 19 10 -22 0.00 5.30 18 -10 -22 14.40 7.90 -18 -10 22 6.70 7.60 18 -10 -22 10.20 7.00 18 10 -22 15.20 6.10 -18 10 22 7.30 9.70 18 10 -22 15.10 7.00 -17 -10 22 16.80 8.60 17 -10 -22 5.60 6.90 17 -10 -22 13.20 7.30 17 10 -22 6.60 6.20 17 10 -22 33.00 8.40 -17 10 22 9.00 4.90 17 10 -22 13.00 6.40 -16 -10 22 46.80 11.30 16 -10 -22 39.20 9.00 16 -10 -22 31.40 8.70 16 10 -22 45.00 9.10 16 10 -22 15.10 7.00 -16 10 22 40.00 7.80 16 10 -22 33.40 7.90 15 -10 -22 16.20 7.40 15 -10 -22 21.60 8.20 -15 -10 22 8.90 6.20 15 10 -22 11.50 6.40 15 10 -22 10.70 6.20 -15 10 22 6.60 4.00 15 10 -22 18.80 7.00 14 -10 -22 -1.30 5.50 -14 -10 22 1.00 5.90 14 -10 -22 3.10 5.80 14 10 -22 6.30 5.60 -14 10 22 0.90 3.40 14 10 -22 4.70 5.70 14 10 -22 -4.70 4.40 13 -10 -22 20.40 7.70 -13 -10 22 23.40 7.20 13 -10 -22 20.30 7.50 13 10 -22 19.50 8.00 13 10 -22 14.70 6.30 13 10 -22 14.30 6.50 -13 10 22 23.50 5.00 -12 -10 22 214.58 17.20 12 -10 -22 233.68 16.90 12 -10 -22 235.08 16.30 12 10 -22 229.78 15.90 12 10 -22 233.78 17.30 12 10 -22 237.48 16.50 -12 10 22 231.28 12.00 11 -10 -22 431.86 22.10 -11 -10 22 405.46 23.80 11 -10 -22 452.85 23.20 11 10 -22 384.66 22.90 11 10 -22 402.46 21.80 11 10 -22 467.25 23.30 -11 10 22 435.66 17.30 10 -10 -22 665.03 29.60 10 -10 -22 625.24 28.20 10 10 -22 682.43 29.60 10 10 -22 665.73 31.20 10 10 -22 697.53 30.50 9 -10 -22 875.41 34.90 9 -10 -22 847.02 27.70 9 -10 -22 843.32 28.80 9 -10 -22 876.61 33.70 9 10 -22 855.71 34.90 9 10 -22 888.51 35.90 9 10 -22 822.72 36.40 -8 -10 22 435.76 24.80 8 -10 -22 560.64 34.50 8 -10 -22 509.95 24.00 8 -10 -22 506.05 22.20 8 -10 -22 489.45 18.20 8 10 -22 493.85 25.80 8 10 -22 495.15 24.50 8 10 -22 516.85 25.00 7 -10 -22 427.96 17.20 7 -10 -22 449.36 19.60 7 -10 -22 446.16 20.70 7 -10 -22 451.05 21.70 -7 -10 22 436.66 23.20 7 10 -22 460.95 23.00 7 10 -22 436.16 23.10 7 10 -22 438.76 23.50 6 -10 -22 41.60 6.20 -6 -10 22 40.80 8.60 6 -10 -22 39.60 7.20 6 -10 -22 54.29 7.80 6 -10 -22 59.09 6.40 6 10 -22 49.30 8.80 6 10 -22 37.40 8.40 6 10 -22 56.49 9.60 5 -10 -22 2.20 3.40 5 -10 -22 -0.20 2.90 5 -10 -22 -3.20 2.60 5 -10 -22 3.40 4.20 -5 -10 22 -0.70 4.80 5 10 -22 1.10 4.90 5 10 -22 3.00 5.10 4 -10 -22 17.70 4.90 4 -10 -22 7.40 4.00 4 -10 -22 14.80 4.40 -4 -10 22 4.90 4.90 4 -10 -22 6.40 4.10 4 10 -22 16.70 6.10 4 10 -22 7.50 5.10 3 -10 -22 95.09 9.50 3 -10 -22 88.39 9.50 3 -10 -22 91.69 9.60 3 -10 -22 76.29 9.10 -3 -10 22 84.39 10.80 3 10 -22 91.49 11.30 3 10 -22 68.89 10.00 2 -10 -22 21.40 6.60 2 -10 -22 16.60 5.00 -2 -10 22 15.90 6.00 2 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4.80 8 -11 -22 49.20 5.60 8 -11 -22 49.70 8.10 8 11 -22 54.99 9.80 8 11 -22 39.50 8.70 8 11 -22 43.30 8.40 7 -11 -22 151.48 10.90 7 -11 -22 128.29 12.50 7 -11 -22 137.49 9.20 7 11 -22 159.88 15.40 7 11 -22 162.18 13.40 7 11 -22 139.89 15.50 -6 -11 22 13.30 6.10 6 -11 -22 11.90 5.50 6 -11 -22 11.80 3.60 6 -11 -22 13.50 4.10 6 -11 -22 10.60 4.40 6 11 -22 15.50 6.40 6 11 -22 4.20 5.40 5 -11 -22 41.50 7.50 5 -11 -22 53.29 6.30 5 -11 -22 52.09 7.10 -5 -11 22 32.00 7.80 5 -11 -22 43.20 7.50 5 11 -22 49.99 9.00 5 11 -22 54.99 9.10 4 -11 -22 1.10 2.90 4 -11 -22 1.90 4.10 -4 -11 22 -4.20 3.50 4 -11 -22 4.00 3.50 4 -11 -22 2.80 3.60 4 11 -22 -3.20 3.90 4 11 -22 -4.30 4.50 3 -11 -22 8.60 3.90 3 -11 -22 9.00 3.70 3 -11 -22 -3.00 3.20 3 -11 -22 3.50 3.30 -3 -11 22 -3.40 3.80 3 11 -22 3.80 5.00 3 11 -22 5.60 5.10 -2 -11 22 3.00 4.90 2 -11 -22 -0.70 3.20 2 -11 -22 -1.50 3.20 2 -11 -22 3.60 3.20 2 -11 -22 -2.50 3.00 -2 -11 22 -1.70 4.10 2 11 -22 2.20 4.70 2 11 -22 -1.30 4.50 1 -11 -22 14.50 4.90 1 -11 -22 22.90 5.50 -1 -11 22 11.80 5.70 1 -11 -22 11.00 4.20 -1 -11 22 22.50 6.90 1 -11 -22 13.70 4.90 1 11 -22 7.10 5.40 0 -11 -22 29.10 5.70 0 -11 22 28.70 8.40 0 -11 -22 23.10 5.70 0 -11 -22 31.00 6.70 0 -11 -22 39.10 7.50 0 -11 22 32.60 7.60 0 11 -22 25.40 7.20 1 -11 22 -1.90 4.70 -1 -11 -22 0.40 3.20 1 -11 22 2.50 4.10 -1 -11 -22 -2.20 4.60 -1 -11 -22 6.10 4.30 -1 11 -22 10.30 5.80 -2 -11 -22 64.69 9.70 -2 -11 -22 56.19 7.50 -2 -11 -22 60.39 7.80 2 -11 22 61.89 10.50 2 -11 22 52.89 9.00 -2 11 -22 84.49 11.60 -3 -11 -22 2.60 4.00 -3 -11 -22 8.80 3.90 -3 -11 -22 -5.60 4.80 3 -11 22 0.10 5.30 3 -11 22 -4.40 3.90 -3 11 -22 4.70 5.50 -4 -11 -22 33.70 8.50 -4 -11 -22 34.30 6.00 -4 -11 -22 37.70 6.30 4 -11 22 30.80 7.40 4 -11 22 40.90 9.40 4 11 22 34.00 7.60 -4 11 -22 39.30 8.50 -5 -11 -22 10.60 3.90 5 -11 22 12.50 7.10 -5 -11 -22 3.00 5.20 5 -11 22 2.60 4.20 -5 -11 -22 6.30 4.10 5 11 22 8.60 5.20 -5 11 -22 11.20 5.90 6 -11 22 10.40 5.40 -6 -11 -22 12.30 6.60 -6 -11 -22 17.70 4.90 -6 -11 -22 10.90 3.70 -6 11 -22 21.10 9.00 6 11 22 12.50 5.70 -7 -11 -22 4.50 3.70 7 -11 22 8.70 6.10 -7 -11 -22 -0.60 2.80 7 -11 22 -1.90 1.80 7 11 22 18.90 6.60 -7 11 -22 5.40 5.50 -8 -11 -22 6.30 4.00 8 -11 22 10.10 6.70 8 11 22 0.70 5.00 -8 11 -22 3.60 5.30 18 -12 -22 -2.30 7.30 -18 -12 22 30.00 11.30 18 12 -22 19.80 7.70 18 12 -22 17.00 7.00 17 -12 -22 22.70 8.70 17 -12 -22 7.20 7.10 -17 -12 22 12.70 8.20 17 12 -22 17.70 6.70 17 12 -22 33.20 8.30 16 -12 -22 137.29 16.80 -16 -12 22 121.29 16.50 16 -12 -22 156.08 17.40 16 12 -22 130.29 16.20 16 12 -22 121.69 13.20 16 12 -22 138.89 23.50 -16 12 22 116.59 12.00 15 -12 -22 78.49 12.30 15 -12 -22 67.39 11.70 -15 -12 22 133.09 18.70 -15 12 22 81.99 9.70 15 12 -22 67.39 10.20 15 12 -22 86.29 12.70 15 12 -22 71.59 11.50 14 -12 -22 45.60 9.70 14 -12 -22 74.09 11.60 -14 -12 22 53.89 10.80 14 12 -22 52.79 9.70 14 12 -22 46.20 8.70 -14 12 22 53.59 7.50 -13 -12 22 35.30 10.60 13 -12 -22 2.90 6.00 13 -12 -22 30.80 8.20 13 12 -22 18.90 6.30 -13 12 22 24.40 5.10 13 12 -22 18.30 6.80 13 12 -22 11.00 5.70 -12 -12 22 13.10 6.10 12 -12 -22 13.30 7.40 12 -12 -22 9.90 5.80 12 12 -22 13.00 6.40 12 12 -22 9.90 6.70 12 12 -22 14.00 5.60 -11 -12 22 22.30 7.60 11 -12 -22 46.70 9.00 11 -12 -22 30.10 8.10 11 12 -22 32.90 7.40 11 12 -22 36.40 9.30 11 12 -22 32.50 8.20 -10 -12 22 63.59 11.80 10 -12 -22 99.09 11.90 10 -12 -22 78.79 11.10 10 12 -22 115.09 15.30 10 12 -22 109.89 12.40 10 12 -22 108.89 13.40 -9 -12 22 161.88 15.20 9 -12 -22 195.88 13.80 9 -12 -22 192.08 14.70 9 12 -22 190.68 16.10 9 12 -22 186.28 15.00 9 12 -22 189.18 14.50 -8 -12 22 28.90 8.40 8 -12 -22 42.30 7.60 8 -12 -22 37.30 9.10 8 -12 -22 32.00 3.70 8 -12 -22 28.80 3.80 8 12 -22 39.00 9.30 8 12 -22 16.50 6.70 8 12 -22 24.20 7.00 7 -12 -22 77.19 8.90 7 -12 -22 84.79 9.70 -7 -12 22 71.69 11.80 7 -12 -22 99.09 11.50 7 -12 -22 80.39 6.00 7 12 -22 77.39 11.50 7 12 -22 74.09 10.90 7 12 -22 94.79 11.60 6 -12 -22 21.90 4.10 6 -12 -22 26.20 6.70 6 -12 -22 12.80 5.00 6 -12 -22 23.30 4.70 6 12 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6.30 -2 -12 -22 -0.50 3.60 -2 -12 -22 3.40 5.70 -2 12 -22 18.30 6.40 -3 -12 -22 87.79 11.70 -3 -12 -22 69.59 8.10 -3 -12 -22 70.69 10.30 3 -12 22 63.19 10.10 3 -12 22 59.09 11.00 3 12 22 90.99 11.10 -3 12 -22 70.29 10.90 -4 -12 -22 2.70 5.20 4 -12 22 -5.10 3.20 4 -12 22 -1.00 4.90 -4 -12 -22 5.60 3.80 -4 12 -22 2.90 5.20 4 12 22 -4.60 3.60 -5 -12 -22 27.70 5.70 -5 -12 -22 16.20 6.70 5 12 22 20.70 6.60 -6 -12 -22 -2.10 3.70 -6 -12 -22 -0.30 2.90 6 -12 22 -2.10 4.50 6 -12 22 -0.90 1.80 6 12 22 -1.50 4.30 -6 12 -22 2.20 4.90 -7 -12 -22 -3.90 2.60 7 -12 22 -2.90 4.00 -7 12 -22 4.80 5.10 7 12 22 -3.30 4.40 16 -13 -22 21.60 8.70 -16 -13 22 19.10 8.80 16 -13 -22 15.30 7.20 16 13 -22 23.60 6.80 16 13 -22 24.40 8.00 15 -13 -22 3.00 6.70 15 -13 -22 5.60 7.00 -15 -13 22 24.10 8.50 -15 13 22 3.00 4.50 15 13 -22 0.20 4.90 15 13 -22 22.70 7.00 14 -13 -22 -2.50 5.70 -14 -13 22 2.00 6.50 14 13 -22 5.20 5.60 14 13 -22 -1.20 4.50 -14 13 22 5.90 4.10 13 -13 -22 20.00 7.90 13 -13 -22 18.10 6.70 -13 -13 22 20.60 7.20 13 13 -22 14.60 8.20 13 13 -22 24.60 6.90 13 13 -22 24.00 9.80 12 -13 -22 63.69 11.10 12 -13 -22 75.29 11.70 -12 -13 22 61.99 11.80 12 13 -22 66.29 12.80 12 13 -22 68.29 11.20 12 13 -22 89.49 11.10 -11 -13 22 71.59 12.60 11 -13 -22 65.39 10.50 11 -13 -22 75.49 11.20 11 13 -22 74.09 11.70 11 13 -22 88.19 11.30 11 13 -22 85.69 13.80 10 -13 -22 242.08 17.20 10 -13 -22 208.58 15.30 -10 -13 22 215.28 17.90 10 13 -22 211.78 16.60 10 13 -22 249.08 16.20 10 13 -22 210.68 17.70 -9 -13 22 120.19 15.10 9 -13 -22 156.08 15.00 9 -13 -22 137.29 12.30 9 13 -22 174.78 18.80 9 13 -22 116.29 13.80 9 13 -22 163.18 13.60 8 -13 -22 256.47 16.30 8 -13 -22 221.58 14.50 -8 -13 22 217.28 17.40 8 13 -22 231.98 15.90 8 13 -22 223.48 17.70 8 13 -22 213.58 17.00 7 -13 -22 93.19 10.50 -7 -13 22 83.69 12.40 7 -13 -22 97.59 6.60 7 -13 -22 97.29 9.40 7 -13 -22 101.89 6.30 7 -13 -22 92.09 11.20 7 13 -22 85.99 11.60 7 13 -22 94.09 11.40 6 -13 -22 69.09 9.20 -6 -13 22 51.49 9.40 6 -13 -22 74.89 9.20 6 -13 -22 65.29 6.80 6 -13 -22 64.49 9.30 6 -13 -22 67.39 7.40 6 13 -22 66.09 10.60 6 13 -22 75.29 10.60 5 -13 -22 19.60 5.20 -5 -13 22 7.40 5.60 5 -13 -22 21.70 4.40 5 -13 -22 23.10 5.90 5 -13 -22 22.00 4.60 5 13 -22 22.70 6.90 5 13 -22 19.70 7.30 4 -13 -22 3.30 3.70 4 -13 -22 3.20 3.40 4 -13 -22 4.20 3.50 4 -13 -22 1.30 4.40 4 13 -22 0.40 4.90 4 13 -22 5.50 5.40 3 -13 -22 11.50 5.00 3 -13 -22 17.60 4.80 3 -13 -22 9.60 4.10 3 -13 -22 7.80 4.00 3 13 -22 16.00 6.40 3 13 -22 17.10 6.60 2 -13 -22 40.90 6.80 -2 -13 22 42.80 10.20 2 -13 -22 50.49 7.00 2 -13 -22 35.00 6.20 -2 -13 22 56.79 9.70 2 13 -22 48.00 9.00 2 13 -22 46.50 9.30 1 -13 -22 28.70 5.90 -1 -13 22 34.40 8.50 1 -13 -22 30.40 6.60 1 -13 -22 33.50 7.10 -1 -13 22 18.50 6.80 1 13 -22 30.20 8.20 0 -13 22 12.00 6.00 0 -13 -22 32.20 6.00 0 -13 -22 20.20 6.20 0 -13 -22 15.90 4.60 0 -13 22 14.50 6.90 0 13 -22 23.70 7.60 -1 -13 -22 1.00 3.20 -1 -13 -22 2.20 4.90 1 -13 22 3.50 5.60 -1 -13 -22 4.90 3.50 1 -13 22 6.70 4.90 -1 13 -22 8.10 5.50 -2 -13 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23 8.70 5.80 -8 -5 -23 19.80 7.40 8 -5 23 12.20 6.70 8 -5 23 7.30 3.90 -8 5 -23 18.70 7.20 8 5 23 15.30 6.20 9 -5 23 2.40 9.10 -9 -5 -23 4.50 6.50 9 5 23 -2.10 4.40 -10 -5 -23 1.00 6.50 10 -5 23 1.50 3.40 10 -5 23 0.70 5.70 10 5 23 7.70 5.50 -10 5 -23 9.30 6.30 11 -5 23 0.20 5.30 -11 -5 -23 5.40 6.20 -11 5 -23 3.70 5.10 -11 5 -23 6.00 6.30 11 5 23 -8.00 4.40 21 -6 -23 15.40 8.30 21 6 -23 19.30 7.50 20 -6 -23 4.10 7.20 20 -6 -23 25.90 9.30 -20 -6 23 30.10 9.00 20 6 -23 33.90 8.50 20 6 -23 36.50 8.30 20 6 -23 21.40 10.10 19 -6 -23 -1.60 5.50 19 -6 -23 -1.50 1.80 -19 -6 23 0.30 4.60 19 -6 -23 -0.20 2.50 19 -6 -23 -3.50 5.60 19 6 -23 1.70 5.00 19 6 -23 0.60 5.60 -19 6 23 2.70 5.00 19 6 -23 3.30 5.50 18 -6 -23 13.50 3.40 18 -6 -23 10.00 6.60 -18 -6 23 6.50 5.90 18 -6 -23 6.90 7.00 18 -6 -23 10.10 2.80 18 6 -23 2.10 5.70 18 6 -23 9.30 5.90 18 6 -23 19.30 6.80 -18 6 23 5.30 4.80 17 -6 -23 17.80 7.70 17 -6 -23 19.10 3.90 17 -6 -23 13.40 3.30 17 -6 -23 1.80 5.00 17 6 -23 7.70 6.00 -17 6 23 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47.70 9.00 -11 -7 23 56.29 10.20 11 7 -23 56.69 8.90 11 7 -23 48.20 8.90 11 7 -23 62.19 10.80 10 -7 -23 178.38 9.80 10 -7 -23 156.28 12.40 -10 -7 23 177.58 14.60 10 -7 -23 205.38 14.60 10 7 -23 231.58 15.10 10 7 -23 181.08 13.90 10 7 -23 155.58 13.40 9 -7 -23 24.90 6.70 9 -7 -23 21.60 4.30 9 -7 -23 14.80 5.70 -9 -7 23 16.50 6.10 9 -7 -23 23.00 4.70 9 7 -23 14.10 5.90 9 7 -23 19.90 5.90 9 7 -23 27.70 6.70 8 -7 -23 289.17 13.60 8 -7 -23 270.07 13.80 -8 -7 23 303.27 17.80 8 -7 -23 301.17 17.10 8 7 -23 285.67 17.40 8 7 -23 314.47 18.20 8 7 -23 289.97 17.20 7 -7 -23 6.70 3.50 7 -7 -23 1.70 8.00 -7 -7 23 13.70 5.60 7 -7 -23 7.80 3.60 7 7 -23 15.60 6.10 7 7 -23 11.40 5.80 7 7 -23 13.10 5.40 6 -7 -23 253.27 12.90 6 -7 -23 236.68 12.90 6 -7 -23 260.17 17.20 -6 -7 23 239.18 15.10 6 7 -23 234.88 15.60 6 7 -23 251.57 15.90 6 7 -23 225.68 14.70 5 -7 -23 15.90 4.50 -5 -7 23 11.40 4.80 5 -7 -23 12.30 3.90 5 -7 -23 1.40 4.40 5 7 -23 16.10 5.80 5 7 -23 15.90 5.70 5 7 -23 14.50 5.50 4 -7 -23 62.59 7.70 4 -7 -23 51.09 7.10 -4 -7 23 48.00 7.60 4 -7 -23 45.80 7.70 4 7 -23 38.20 8.00 4 7 -23 54.69 8.80 3 -7 -23 14.80 5.20 -3 -7 23 18.00 5.30 3 -7 -23 22.30 7.30 3 -7 -23 14.70 4.90 3 7 -23 19.90 6.20 3 7 -23 18.10 5.80 -2 -7 23 22.00 6.60 2 -7 -23 24.90 5.80 -2 -7 23 12.80 4.80 2 -7 -23 18.10 5.00 2 -7 -23 15.20 5.60 2 -7 -23 16.30 5.50 2 7 -23 23.90 6.90 2 7 -23 22.20 6.50 -1 -7 23 2.40 5.10 1 -7 -23 19.10 5.70 -1 -7 23 11.40 5.30 1 -7 -23 8.50 4.40 1 -7 -23 3.00 4.10 1 -7 -23 2.70 4.00 1 7 -23 6.80 5.30 1 7 -23 12.00 5.50 0 -7 -23 8.40 4.90 0 -7 23 4.60 4.40 0 -7 -23 9.10 4.70 0 -7 -23 2.80 4.10 0 -7 23 5.20 5.10 0 7 -23 -1.80 4.60 -1 -7 -23 6.00 5.80 -1 -7 -23 8.00 4.90 1 -7 23 -0.90 4.50 1 -7 23 -4.30 3.30 -1 7 -23 3.40 5.00 -2 -7 -23 9.00 5.50 -2 -7 -23 17.10 5.40 2 -7 23 7.00 5.40 2 -7 23 7.90 6.00 -2 7 -23 3.70 5.70 -3 -7 -23 14.50 6.20 3 -7 23 20.50 7.20 3 -7 23 5.90 5.90 -3 -7 -23 0.00 4.50 -3 7 -23 1.80 5.10 -4 -7 -23 22.00 6.60 4 -7 23 18.90 6.90 4 -7 23 8.00 4.80 -4 -7 -23 22.20 7.60 -4 7 -23 18.90 7.10 5 -7 23 21.40 7.60 -5 -7 -23 6.90 6.00 5 -7 23 3.90 4.30 -5 -7 -23 11.70 5.50 -5 7 -23 0.10 4.80 -6 -7 -23 -2.60 3.60 6 -7 23 1.00 3.40 -6 -7 -23 4.90 6.10 6 -7 23 2.60 4.50 -6 7 -23 2.70 4.60 -7 -7 -23 -4.70 4.90 -7 -7 -23 8.40 4.80 7 -7 23 3.00 3.40 7 -7 23 5.60 5.60 -7 7 -23 0.50 5.20 -8 -7 -23 12.00 6.40 8 -7 23 1.50 3.50 -8 -7 -23 4.00 4.00 8 7 23 6.80 5.00 -9 -7 -23 44.80 14.90 9 -7 23 52.59 8.30 -9 -7 -23 52.79 8.40 9 -7 23 55.89 11.00 9 7 23 60.69 9.50 -9 7 -23 60.39 10.90 -10 -7 -23 45.60 10.60 10 -7 23 46.60 10.30 -10 7 -23 31.80 8.60 10 7 23 48.70 9.10 20 -8 -23 79.79 16.10 20 -8 -23 63.19 12.70 20 8 -23 75.59 11.30 20 8 -23 79.09 12.10 -19 -8 23 9.00 6.80 19 -8 -23 3.30 6.10 19 8 -23 3.50 8.10 19 8 -23 4.70 5.60 19 8 -23 16.80 7.00 -19 8 23 13.50 5.80 18 -8 -23 85.89 13.60 18 -8 -23 81.19 13.40 -18 -8 23 85.59 14.50 18 8 -23 82.19 11.40 -18 8 23 83.79 12.00 18 8 -23 84.39 11.50 18 8 -23 97.89 14.90 -17 -8 23 23.40 7.90 17 -8 -23 23.20 8.10 17 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16.40 5.90 10 -5 -25 102.29 8.90 10 -5 -25 85.09 10.80 -10 -5 25 83.79 10.80 10 -5 -25 94.19 8.20 10 -5 -25 93.39 8.00 10 5 -25 99.89 11.40 10 5 -25 108.49 12.50 10 5 -25 94.99 11.10 9 -5 -25 3.80 3.50 9 -5 -25 10.90 4.00 -9 -5 25 12.70 6.40 9 -5 -25 -0.40 4.70 9 -5 -25 1.80 3.20 9 5 -25 3.90 4.60 9 5 -25 7.20 4.60 9 5 -25 12.80 5.70 -8 -5 25 43.30 8.10 8 -5 -25 38.50 7.80 8 -5 -25 46.60 6.70 8 -5 -25 40.60 6.50 8 5 -25 51.09 8.60 8 5 -25 64.39 9.50 8 5 -25 31.10 7.30 7 -5 -25 5.80 3.80 7 -5 -25 5.50 4.30 -7 -5 25 0.00 3.90 7 -5 -25 8.60 5.10 7 5 -25 -0.20 3.80 7 5 -25 10.00 4.90 7 5 -25 6.90 5.20 -6 -5 25 43.20 7.50 6 -5 -25 38.70 6.60 6 -5 -25 45.50 6.70 6 -5 -25 57.29 8.80 6 5 -25 46.50 8.50 6 5 -25 53.99 8.20 6 5 -25 40.80 7.90 5 -5 -25 1.30 3.60 -5 -5 25 3.00 3.40 5 -5 -25 4.70 4.60 5 -5 -25 -2.70 2.70 5 5 -25 0.40 4.60 5 5 -25 1.60 4.10 4 -5 -25 188.48 13.90 4 -5 -25 181.48 12.40 -4 -5 25 190.38 12.20 4 -5 -25 187.98 12.70 4 5 -25 211.58 15.70 4 5 -25 217.28 14.80 -3 -5 25 22.60 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106.49 13.50 15 6 -25 104.59 12.60 -15 6 25 100.19 8.80 15 6 -25 108.99 14.40 15 6 -25 103.79 12.30 14 -6 -25 33.50 5.00 14 -6 -25 34.80 5.10 -14 -6 25 48.90 9.50 14 -6 -25 35.30 8.70 14 -6 -25 25.00 7.20 14 6 -25 32.10 7.90 14 6 -25 41.10 8.40 -14 6 25 36.10 5.70 14 6 -25 44.00 9.30 -13 -6 25 219.98 17.00 13 -6 -25 240.28 12.10 13 -6 -25 237.68 15.90 13 -6 -25 245.68 17.00 13 -6 -25 225.48 11.40 13 6 -25 255.87 16.80 13 6 -25 218.58 16.50 13 6 -25 211.78 15.40 -13 6 25 201.08 12.20 12 -6 -25 -2.10 4.50 12 -6 -25 -0.90 2.80 12 -6 -25 -0.10 4.10 -12 -6 25 6.80 5.30 12 -6 -25 1.30 3.00 12 6 -25 -1.50 4.80 12 6 -25 5.70 4.90 12 6 -25 2.00 5.10 11 -6 -25 16.60 4.30 11 -6 -25 15.90 4.20 11 -6 -25 10.60 5.90 -11 -6 25 10.80 6.20 11 -6 -25 12.80 5.50 11 6 -25 10.40 5.40 11 6 -25 18.40 6.80 11 6 -25 19.70 6.00 10 -6 -25 2.80 3.10 10 -6 -25 3.00 3.00 -10 -6 25 3.90 4.90 10 -6 -25 2.20 3.80 10 -6 -25 6.50 5.10 10 6 -25 -1.40 4.60 10 6 -25 -0.20 3.80 10 6 -25 6.30 5.40 9 -6 -25 87.19 8.50 -9 -6 25 103.09 12.30 9 -6 -25 86.89 7.60 9 -6 -25 102.49 11.90 9 -6 -25 86.49 8.60 9 6 -25 71.69 9.90 9 6 -25 79.19 10.80 9 6 -25 86.69 11.50 8 -6 -25 9.00 5.20 8 -6 -25 0.90 3.00 -8 -6 25 1.30 4.30 8 -6 -25 4.60 3.20 8 6 -25 -0.90 4.60 8 6 -25 5.20 4.20 8 6 -25 2.50 4.60 7 -6 -25 157.18 10.60 7 -6 -25 163.18 10.60 7 -6 -25 154.28 12.90 7 6 -25 155.38 13.00 7 6 -25 156.68 12.20 7 6 -25 155.38 13.20 6 -6 -25 3.70 4.50 6 -6 -25 4.00 3.40 -6 -6 25 1.40 3.80 6 6 -25 4.60 5.00 6 6 -25 3.10 3.80 6 6 -25 8.10 5.00 5 -6 -25 3.90 5.00 5 -6 -25 6.60 3.90 5 -6 -25 4.00 3.80 5 6 -25 7.00 5.20 5 6 -25 5.60 4.90 4 -6 -25 3.90 3.80 4 -6 -25 -4.00 3.00 4 -6 -25 -0.10 4.40 -4 -6 25 -3.00 3.10 4 6 -25 -1.80 4.70 4 6 -25 -1.90 4.90 3 -6 -25 123.69 10.60 3 -6 -25 111.29 12.00 3 -6 -25 116.69 11.30 -3 -6 25 115.59 11.40 3 6 -25 111.99 13.60 3 6 -25 93.59 11.70 2 -6 -25 14.10 5.80 -2 -6 25 4.80 3.90 2 -6 -25 9.40 4.90 2 6 -25 12.20 5.80 2 6 -25 12.80 6.20 -1 -6 25 99.89 12.90 1 -6 -25 83.49 10.60 1 -6 -25 75.09 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51.99 8.90 13 7 -25 19.00 7.40 13 7 -25 43.90 9.10 12 -7 -25 149.59 9.10 12 -7 -25 123.29 13.80 -12 -7 25 124.89 14.60 12 -7 -25 162.48 8.90 12 -7 -25 134.79 11.90 12 7 -25 166.48 13.60 12 7 -25 164.68 13.80 12 7 -25 144.39 13.30 11 -7 -25 25.00 6.60 11 -7 -25 32.00 7.80 -11 -7 25 27.80 7.80 11 -7 -25 25.10 4.90 11 -7 -25 20.80 4.30 11 7 -25 22.20 6.70 11 7 -25 17.90 6.70 11 7 -25 11.40 6.10 10 -7 -25 19.00 4.70 10 -7 -25 22.10 5.50 -10 -7 25 33.70 8.10 10 -7 -25 25.50 7.00 10 -7 -25 18.80 4.40 10 7 -25 30.10 7.40 10 7 -25 16.00 6.10 10 7 -25 24.40 6.80 9 -7 -25 15.90 4.40 9 -7 -25 13.10 5.90 -9 -7 25 2.00 4.30 9 -7 -25 14.90 4.00 9 7 -25 15.40 6.10 9 7 -25 10.00 5.60 9 7 -25 9.50 5.80 8 -7 -25 30.50 5.50 8 -7 -25 36.10 7.50 -8 -7 25 24.30 7.00 8 -7 -25 35.60 5.70 8 7 -25 32.30 7.00 8 7 -25 34.10 8.00 8 7 -25 36.90 7.50 -7 -7 25 8.30 5.10 7 -7 -25 11.30 4.00 7 -7 -25 4.40 3.30 7 -7 -25 -1.00 4.40 7 7 -25 5.40 5.00 7 7 -25 9.10 5.50 -6 -7 25 139.39 12.00 6 -7 -25 169.28 10.70 6 -7 -25 141.79 12.40 6 -7 -25 147.59 10.50 6 7 -25 127.49 11.40 6 7 -25 142.59 12.60 6 7 -25 121.99 13.50 5 -7 -25 5.80 4.00 5 -7 -25 3.90 3.80 -5 -7 25 11.60 5.70 5 -7 -25 7.40 5.40 5 7 -25 8.40 5.40 5 7 -25 0.50 5.30 4 -7 -25 181.28 12.10 4 -7 -25 163.88 12.00 -4 -7 25 165.18 12.40 4 -7 -25 165.88 13.10 4 7 -25 182.68 14.20 4 7 -25 177.98 14.70 3 -7 -25 20.50 5.70 3 -7 -25 13.40 5.70 3 -7 -25 26.40 6.20 3 7 -25 22.40 7.60 3 7 -25 21.30 6.90 -2 -7 25 116.39 10.50 2 -7 -25 126.79 12.90 2 -7 -25 119.79 12.00 2 7 -25 115.29 13.30 2 7 -25 127.89 14.40 -1 -7 25 55.39 8.70 1 -7 -25 73.69 9.90 1 -7 -25 85.89 10.70 -1 -7 25 70.49 11.20 1 7 -25 90.39 12.20 1 7 -25 79.49 11.60 0 -7 25 52.19 10.40 0 -7 -25 75.59 10.00 0 -7 25 66.59 8.80 0 -7 -25 70.29 9.70 0 7 -25 68.69 10.90 0 7 -25 80.79 11.50 1 -7 25 124.59 10.50 -1 -7 -25 128.79 13.20 1 -7 25 126.99 14.70 -1 -7 -25 122.49 12.60 -1 7 -25 117.99 13.70 2 -7 25 58.59 8.40 2 -7 25 55.39 10.00 -2 -7 -25 84.99 10.30 -2 -7 -25 72.19 10.20 -2 7 -25 65.39 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10 -25 8.30 6.10 -6 -10 25 35.30 8.10 6 -10 -25 31.40 7.20 6 -10 -25 25.00 5.30 6 -10 -25 37.00 5.80 6 10 -25 19.00 7.40 6 10 -25 26.30 7.80 5 -10 -25 6.70 5.40 5 -10 -25 13.80 4.40 -5 -10 25 7.40 4.80 5 -10 -25 12.80 4.20 5 10 -25 3.50 5.50 5 10 -25 10.10 6.20 4 -10 -25 5.40 5.20 4 -10 -25 14.10 5.00 4 -10 -25 6.20 4.30 -4 -10 25 10.40 5.30 4 10 -25 3.40 5.70 4 10 -25 9.90 6.60 -3 -10 25 33.40 7.80 3 -10 -25 52.49 7.80 3 -10 -25 37.80 6.80 3 -10 -25 30.60 7.20 3 10 -25 50.49 9.60 3 10 -25 44.00 10.00 2 -10 -25 29.20 6.80 2 -10 -25 29.60 6.90 -2 -10 25 24.40 6.90 2 10 -25 34.90 9.00 2 10 -25 41.50 9.60 1 -10 -25 21.10 6.20 1 -10 -25 20.40 6.20 -1 -10 25 20.30 6.80 -1 -10 25 24.70 8.10 1 10 -25 18.00 7.70 1 10 -25 32.80 8.30 0 -10 25 58.89 10.40 0 -10 -25 66.79 9.10 0 -10 -25 76.19 10.50 0 -10 25 49.40 10.10 0 10 -25 57.29 10.40 -1 -10 -25 5.50 5.30 1 -10 25 0.70 4.80 -1 -10 -25 9.40 4.70 1 -10 25 6.70 6.00 -1 10 -25 8.50 6.20 -2 -10 -25 15.80 5.10 -2 -10 -25 22.60 7.20 2 -10 25 10.00 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77.59 11.90 3 11 -25 74.39 11.70 -2 -11 25 549.95 27.90 2 -11 -25 644.04 26.60 2 -11 -25 574.24 26.10 2 11 -25 608.04 29.70 2 11 -25 637.94 30.70 -1 -11 25 236.88 18.40 1 -11 -25 235.98 15.50 -1 -11 25 193.28 15.90 1 -11 -25 214.78 14.60 1 11 -25 217.28 18.20 1 11 -25 260.97 22.40 0 -11 -25 267.77 17.00 0 -11 25 282.17 20.20 0 -11 -25 292.77 16.30 0 -11 25 257.87 17.70 -1 -11 -25 74.69 10.60 -1 -11 -25 93.49 10.20 1 -11 25 66.29 10.70 -1 11 -25 67.69 11.20 2 -11 25 0.70 4.20 -2 -11 -25 -3.00 3.40 2 -11 25 -4.20 4.80 -2 -11 -25 2.20 4.50 -2 11 -25 -1.20 5.00 -3 -11 -25 5.00 4.80 3 -11 25 12.70 6.60 -3 -11 -25 1.30 4.00 -3 11 -25 3.60 5.00 -4 -11 -25 40.90 6.70 -4 -11 -25 41.70 9.00 4 -11 25 45.50 9.70 -4 11 -25 41.30 9.20 14 -12 -25 17.10 8.10 14 -12 -25 3.80 5.60 14 12 -25 20.70 6.80 14 12 -25 11.30 6.60 13 -12 -25 48.80 9.50 13 -12 -25 50.69 9.80 13 12 -25 63.29 10.10 13 12 -25 50.39 9.50 12 -12 -25 0.60 5.20 12 -12 -25 4.80 4.60 -12 -12 25 -1.70 2.40 12 12 -25 8.70 6.00 12 12 -25 -1.30 4.50 11 -12 -25 83.09 11.20 11 -12 -25 78.79 11.10 11 12 -25 58.69 10.00 11 12 -25 93.29 12.70 11 12 -25 76.79 13.00 10 -12 -25 9.40 5.00 -10 -12 25 3.90 4.50 10 -12 -25 6.80 5.60 10 12 -25 12.30 8.10 10 12 -25 15.20 6.80 10 12 -25 10.30 5.60 9 -12 -25 45.00 8.90 9 -12 -25 40.00 7.10 9 -12 -25 38.30 4.10 -9 -12 25 32.60 8.80 9 12 -25 30.70 7.80 9 12 -25 29.20 7.90 8 -12 -25 -0.80 2.40 8 -12 -25 0.50 4.70 -8 -12 25 -3.40 3.60 8 12 -25 3.50 4.80 7 -12 -25 2.10 3.00 -7 -12 25 1.10 4.30 7 -12 -25 4.30 4.80 7 -12 -25 -2.70 2.60 7 12 -25 -4.00 4.90 7 12 -25 -11.00 8.10 6 -12 -25 62.69 7.00 -6 -12 25 41.80 8.80 6 -12 -25 38.70 8.20 6 -12 -25 35.30 6.10 6 12 -25 41.60 8.90 6 12 -25 40.60 13.40 -5 -12 25 101.89 14.00 5 -12 -25 112.59 9.80 5 -12 -25 114.79 12.60 5 -12 -25 125.39 9.30 5 12 -25 108.09 13.30 5 12 -25 139.99 19.00 -4 -12 25 92.39 12.20 4 -12 -25 58.89 9.10 4 -12 -25 68.39 9.30 4 -12 -25 105.09 9.10 4 12 -25 78.49 11.60 3 -12 -25 286.77 17.20 -3 -12 25 283.17 19.10 3 -12 -25 315.47 17.50 3 -12 -25 322.07 16.60 3 12 -25 285.27 25.10 3 12 -25 324.57 20.90 -2 -12 25 68.19 10.60 2 -12 -25 71.39 9.30 2 12 -25 94.49 13.20 2 12 -25 90.29 13.50 -1 -12 25 370.06 26.00 1 -12 -25 287.67 17.90 1 -12 -25 322.47 18.10 1 12 -25 319.87 22.50 1 12 -25 383.76 22.40 0 -12 -25 41.60 8.00 0 -12 25 53.69 11.90 0 12 -25 47.30 15.30 0 12 -25 48.70 10.30 1 -12 25 129.59 15.50 -1 -12 -25 145.09 14.30 -1 12 -25 118.99 13.90 -2 -12 -25 12.10 5.80 2 -12 25 9.40 6.10 -2 12 -25 7.20 6.40 13 -13 -25 6.40 4.90 13 13 -25 11.70 6.40 12 -13 -25 120.89 14.20 12 -13 -25 102.39 13.00 12 13 -25 100.59 13.30 12 13 -25 120.39 13.40 11 -13 -25 -5.40 3.60 11 -13 -25 -0.80 4.70 -11 -13 25 -1.80 2.50 11 13 -25 -11.50 3.80 11 13 -25 -2.40 4.20 10 -13 -25 8.80 5.70 10 -13 -25 1.10 4.30 10 13 -25 7.70 5.80 10 13 -25 8.00 5.90 9 -13 -25 -1.60 4.20 9 -13 -25 6.70 5.20 9 13 -25 -2.90 4.10 9 13 -25 1.50 4.60 8 -13 -25 56.99 9.40 8 -13 -25 71.89 5.30 8 13 -25 62.99 10.60 8 13 -25 73.39 11.00 7 -13 -25 15.30 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-28 7.00 4.00 16 -3 -28 2.60 6.90 -16 3 28 -0.70 3.10 -16 3 28 4.10 3.80 16 3 -28 -4.30 3.40 16 3 -28 1.70 5.80 16 3 -28 -3.10 4.50 15 -3 -28 -0.50 4.30 15 -3 -28 -5.00 2.80 15 -3 -28 -0.60 4.90 15 -3 -28 1.90 3.80 15 3 -28 -2.90 7.00 15 3 -28 -5.40 4.20 -15 3 28 5.90 4.00 15 3 -28 -1.20 4.20 14 -3 -28 118.09 10.10 14 -3 -28 125.19 10.00 14 -3 -28 132.99 12.20 14 -3 -28 112.99 13.40 -14 -3 28 145.89 12.80 -14 3 28 121.99 8.90 14 3 -28 112.79 13.50 14 3 -28 142.59 12.40 14 3 -28 131.79 14.80 13 -3 -28 29.80 7.10 -13 -3 28 31.80 7.70 13 -3 -28 25.30 6.20 13 -3 -28 36.10 6.50 13 -3 -28 29.20 7.90 13 3 -28 25.40 7.00 13 3 -28 38.00 8.60 13 3 -28 42.20 8.80 12 -3 -28 419.56 19.20 12 -3 -28 418.36 19.90 12 -3 -28 411.26 19.90 12 -3 -28 405.16 22.70 -12 -3 28 391.26 20.70 12 3 -28 399.86 22.80 12 3 -28 397.86 21.10 12 3 -28 392.76 21.50 11 -3 -28 116.69 11.60 11 -3 -28 126.49 10.20 -11 -3 28 117.99 12.40 11 -3 -28 123.69 10.10 11 -3 -28 118.39 13.70 11 3 -28 133.69 13.70 11 3 -28 110.89 12.00 11 3 -28 94.89 13.00 -10 -3 28 253.77 15.60 10 -3 -28 293.57 18.90 10 -3 -28 301.97 15.90 10 -3 -28 297.97 14.70 10 3 -28 279.67 17.30 10 3 -28 253.77 18.50 10 3 -28 261.27 23.00 9 -3 -28 56.19 10.10 -9 -3 28 60.49 8.40 9 -3 -28 55.09 7.90 9 -3 -28 60.49 7.20 9 3 -28 60.99 10.20 9 3 -28 61.09 9.30 9 3 -28 47.50 8.20 8 -3 -28 12.40 6.40 -8 -3 28 6.20 6.10 8 -3 -28 7.30 6.00 8 3 -28 14.80 5.50 8 3 -28 5.80 6.00 8 3 -28 5.00 5.30 7 -3 -28 22.80 6.30 7 -3 -28 10.90 6.50 7 3 -28 16.80 6.00 7 3 -28 16.20 5.40 7 3 -28 11.40 6.30 6 -3 -28 81.79 11.00 6 -3 -28 80.09 9.90 6 3 -28 75.19 11.70 6 3 -28 72.59 10.60 5 -3 -28 88.79 10.90 5 -3 -28 106.89 12.40 5 3 -28 97.29 11.90 5 3 -28 91.29 12.40 4 -3 -28 60.19 9.90 4 -3 -28 64.89 9.40 4 3 -28 44.60 8.60 4 3 -28 36.30 8.50 3 -3 -28 5.80 5.00 3 -3 -28 6.10 5.30 3 3 -28 9.80 6.60 3 3 -28 5.60 5.30 2 -3 -28 7.70 5.40 2 -3 -28 3.40 4.50 2 3 -28 -3.80 4.10 2 3 -28 -3.60 4.20 1 -3 -28 33.90 7.80 1 -3 -28 46.50 9.10 1 3 -28 50.89 9.70 1 3 -28 31.50 8.70 0 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116.49 17.10 -15 4 28 100.79 8.40 15 4 -28 114.99 12.40 15 4 -28 126.79 14.40 14 -4 -28 21.50 6.40 14 -4 -28 14.50 4.70 14 -4 -28 35.20 9.00 14 -4 -28 21.70 5.30 14 4 -28 27.20 7.00 14 4 -28 19.40 7.30 14 4 -28 21.30 6.80 13 -4 -28 143.19 10.70 13 -4 -28 142.49 10.90 13 -4 -28 158.58 12.40 -13 -4 28 155.78 13.60 13 -4 -28 164.08 14.50 13 4 -28 191.68 14.20 13 4 -28 195.08 14.80 13 4 -28 160.78 14.30 12 -4 -28 21.20 5.10 12 -4 -28 10.20 4.60 -12 -4 28 19.80 6.10 12 -4 -28 30.10 8.00 12 -4 -28 16.50 5.00 12 4 -28 17.50 6.90 12 4 -28 15.20 5.90 12 4 -28 26.00 7.30 11 -4 -28 84.99 11.50 -11 -4 28 125.29 13.20 11 -4 -28 103.59 10.50 11 -4 -28 94.19 8.80 11 -4 -28 101.39 8.90 11 4 -28 92.59 11.30 11 4 -28 128.09 13.30 11 4 -28 78.19 11.80 10 -4 -28 13.20 6.20 10 -4 -28 4.20 4.30 -10 -4 28 9.40 5.10 10 -4 -28 12.20 4.80 10 -4 -28 7.50 3.70 10 4 -28 3.00 5.00 10 4 -28 10.30 6.10 10 4 -28 -2.00 3.90 9 -4 -28 76.89 10.70 -9 -4 28 78.59 10.10 9 -4 -28 74.49 8.80 9 -4 -28 74.59 10.90 9 4 -28 69.49 12.60 9 4 -28 64.59 10.80 9 4 -28 100.59 11.60 8 -4 -28 32.90 6.60 -8 -4 28 17.90 6.20 8 -4 -28 22.30 7.10 8 4 -28 36.80 7.70 8 4 -28 10.40 6.40 8 4 -28 26.00 7.20 7 -4 -28 79.89 11.10 7 -4 -28 73.09 11.20 7 4 -28 82.99 10.80 7 4 -28 71.29 11.40 7 4 -28 72.19 9.60 6 -4 -28 70.59 9.50 6 -4 -28 88.29 11.90 6 4 -28 86.49 11.30 6 4 -28 71.49 11.30 5 -4 -28 24.20 7.30 5 -4 -28 22.90 6.30 5 4 -28 31.00 7.40 5 4 -28 21.40 7.50 4 -4 -28 42.10 8.70 4 -4 -28 43.10 7.70 4 4 -28 35.80 8.10 4 4 -28 30.00 8.30 3 -4 -28 0.50 4.30 3 -4 -28 8.50 5.60 3 4 -28 -0.70 5.00 3 4 -28 1.90 4.80 2 -4 -28 2.70 5.30 2 -4 -28 3.30 4.60 2 4 -28 -8.10 3.90 2 4 -28 2.50 5.50 1 -4 -28 -3.80 4.20 1 -4 -28 -4.70 3.40 1 4 -28 2.90 5.70 1 4 -28 8.40 5.60 0 -4 -28 5.80 5.10 0 -4 -28 -0.20 4.40 0 4 -28 -5.30 4.70 0 4 -28 0.00 4.70 -1 -4 -28 5.30 5.20 1 -4 28 0.40 5.10 -1 -4 -28 5.30 5.50 -1 4 -28 1.30 6.60 -1 4 -28 1.90 4.90 -2 -4 -28 16.60 6.90 -2 -4 -28 38.20 8.70 2 -4 28 37.70 12.00 -2 4 -28 16.60 10.00 3 -4 28 19.70 7.40 -3 -4 -28 10.20 6.00 -3 -4 -28 -0.30 4.40 -3 4 -28 -5.10 5.40 -3 4 -28 12.70 6.10 -4 -4 -28 61.29 10.00 -4 -4 -28 73.39 17.00 4 -4 28 59.89 11.50 -4 4 -28 54.29 10.20 -5 -4 -28 8.60 6.40 -5 -4 -28 5.30 5.40 5 -4 28 7.60 5.90 -5 4 -28 6.10 5.60 18 -5 -28 27.20 5.20 18 5 -28 29.90 7.50 17 -5 -28 6.60 6.50 17 -5 -28 13.00 7.10 17 -5 -28 12.30 4.20 17 5 -28 13.40 5.80 17 5 -28 7.90 6.60 -17 5 28 8.50 4.60 16 -5 -28 63.39 10.80 16 -5 -28 70.09 11.70 -16 -5 28 48.60 9.50 16 5 -28 55.49 9.50 16 5 -28 74.79 12.20 16 5 -28 57.49 10.70 15 -5 -28 11.20 4.20 15 -5 -28 1.20 5.00 15 -5 -28 10.70 4.20 -15 -5 28 10.40 5.10 15 5 -28 10.00 11.10 15 5 -28 6.30 5.90 15 5 -28 20.70 6.90 -14 -5 28 17.60 6.40 14 -5 -28 17.00 4.50 14 -5 -28 10.20 5.70 14 -5 -28 14.30 4.70 14 -5 -28 5.90 6.30 14 5 -28 17.30 6.50 14 5 -28 27.40 7.50 14 5 -28 13.30 7.10 13 -5 -28 -1.50 4.20 13 -5 -28 -0.10 3.80 13 -5 -28 -1.00 2.60 -13 -5 28 4.30 6.90 13 -5 -28 6.90 5.70 13 5 -28 -1.80 3.90 13 5 -28 5.30 5.00 13 5 -28 -2.60 4.20 -12 -5 28 6.20 4.80 12 -5 -28 12.30 6.40 12 -5 -28 7.10 3.90 12 -5 -28 9.60 3.90 12 -5 -28 7.10 3.90 12 5 -28 16.40 5.90 12 5 -28 13.30 6.40 12 5 -28 5.90 4.90 11 -5 -28 12.50 4.10 -11 -5 28 12.00 5.40 11 -5 -28 20.60 7.10 11 -5 -28 15.90 4.70 11 -5 -28 11.50 4.50 11 5 -28 5.70 5.40 11 5 -28 13.50 6.40 11 5 -28 13.10 5.90 -10 -5 28 -2.70 3.80 10 -5 -28 3.80 3.50 10 -5 -28 0.50 4.80 10 -5 -28 -4.30 2.70 10 -5 -28 -5.20 2.50 10 5 -28 0.90 5.40 10 5 -28 -2.50 4.30 10 5 -28 -7.90 3.40 -9 -5 28 0.20 3.70 9 -5 -28 3.10 3.70 9 -5 -28 6.70 4.00 9 -5 -28 1.00 5.00 9 5 -28 -4.10 4.60 9 5 -28 3.00 4.30 9 5 -28 3.50 5.00 8 -5 -28 93.49 11.40 -8 -5 28 72.59 10.00 8 -5 -28 78.69 10.90 8 -5 -28 78.99 8.90 8 5 -28 90.79 11.30 8 5 -28 77.49 11.50 8 5 -28 82.29 11.20 7 -5 -28 98.39 12.40 -7 -5 28 116.39 11.70 7 -5 -28 116.59 10.10 7 5 -28 117.99 13.30 7 5 -28 122.19 14.10 7 5 -28 121.79 14.10 6 -5 -28 222.28 14.50 -6 -5 28 209.38 14.00 6 -5 -28 235.18 16.60 6 5 -28 216.18 15.70 6 5 -28 237.08 17.40 5 -5 -28 269.17 15.80 5 -5 -28 226.68 16.70 5 5 -28 223.68 17.00 5 5 -28 234.38 16.60 4 -5 -28 120.69 12.20 -4 -5 28 107.79 9.60 4 -5 -28 113.89 12.80 4 5 -28 114.39 13.80 4 5 -28 118.29 13.50 3 -5 -28 116.79 12.90 3 -5 -28 107.79 12.00 3 5 -28 104.19 13.50 3 5 -28 120.29 14.00 2 -5 -28 2.00 4.70 2 -5 -28 5.30 4.70 2 5 -28 4.40 5.30 2 5 -28 -6.90 4.10 1 -5 -28 1.80 4.70 1 -5 -28 -2.90 4.10 1 5 -28 7.40 5.80 1 5 -28 -0.90 5.00 0 -5 -28 27.00 7.40 0 -5 -28 12.80 6.10 0 5 -28 26.00 9.00 0 5 -28 19.10 7.20 -1 -5 -28 59.39 9.80 -1 -5 -28 37.60 8.00 1 -5 28 47.00 13.30 -1 5 -28 36.10 12.50 2 -5 28 0.50 5.20 -2 -5 -28 8.90 5.90 -2 -5 -28 7.60 5.40 -2 5 -28 5.00 5.60 -2 5 -28 1.90 5.70 3 -5 28 7.50 6.40 -3 -5 -28 9.50 5.90 -3 -5 -28 24.60 7.80 -3 5 -28 22.70 7.80 -4 -5 -28 18.20 8.70 -4 -5 -28 7.50 5.20 4 -5 28 8.00 6.10 -4 5 -28 6.30 5.50 17 -6 -28 3.20 5.40 17 -6 -28 5.00 3.20 17 -6 -28 -10.50 5.00 17 6 -28 -0.80 5.40 17 6 -28 -2.40 4.60 16 -6 -28 0.00 2.80 16 -6 -28 -0.70 5.70 16 -6 -28 0.80 4.30 16 6 -28 -6.70 4.40 16 6 -28 -8.30 4.90 16 6 -28 -1.30 5.30 -15 -6 28 35.20 8.90 15 -6 -28 37.20 5.40 15 -6 -28 34.50 8.30 15 6 -28 35.50 8.00 15 6 -28 27.60 8.30 15 6 -28 39.10 9.40 14 -6 -28 13.40 5.40 -14 -6 28 5.80 5.00 14 -6 -28 8.50 3.50 14 -6 -28 3.40 3.50 14 -6 -28 8.70 6.30 14 6 -28 9.30 6.80 14 6 -28 2.40 5.00 13 -6 -28 76.09 9.70 13 -6 -28 55.59 10.20 13 -6 -28 104.59 7.90 13 -6 -28 85.79 8.50 -13 -6 28 63.69 14.90 13 6 -28 76.59 11.40 13 6 -28 78.59 11.40 13 6 -28 80.99 10.80 12 -6 -28 11.90 4.10 12 -6 -28 14.20 4.90 -12 -6 28 19.90 6.90 12 -6 -28 9.60 6.40 12 -6 -28 9.10 4.20 12 6 -28 11.10 6.00 12 6 -28 13.70 6.10 12 6 -28 15.40 6.50 -11 -6 28 -1.00 7.70 11 -6 -28 14.70 6.50 11 -6 -28 10.80 3.90 11 -6 -28 8.70 4.00 11 -6 -28 5.90 5.00 11 6 -28 3.30 4.40 11 6 -28 11.20 6.00 11 6 -28 8.50 5.50 10 -6 -28 1.00 3.10 -10 -6 28 1.10 4.40 10 -6 -28 5.00 3.20 10 -6 -28 -6.40 4.10 10 -6 -28 2.00 3.10 10 6 -28 1.10 4.30 10 6 -28 3.70 4.90 10 6 -28 -0.70 4.80 9 -6 -28 23.30 5.00 -9 -6 28 31.60 7.30 9 -6 -28 9.70 4.40 9 -6 -28 22.60 7.10 9 6 -28 25.00 7.20 9 6 -28 14.80 5.80 9 6 -28 21.30 7.00 8 -6 -28 38.60 8.30 -8 -6 28 40.90 8.30 8 -6 -28 32.10 6.40 8 -6 -28 45.90 6.80 8 6 -28 50.59 9.40 8 6 -28 51.79 8.90 8 6 -28 27.90 7.40 7 -6 -28 78.69 11.40 -7 -6 28 89.49 11.00 7 -6 -28 94.39 9.60 7 6 -28 75.69 11.50 7 6 -28 106.89 12.50 6 -6 -28 113.69 18.10 -6 -6 28 81.19 10.40 6 -6 -28 96.29 11.90 6 6 -28 82.89 11.40 6 6 -28 84.49 12.00 5 -6 -28 127.09 10.80 -5 -6 28 89.79 10.70 5 -6 -28 111.49 12.80 5 6 -28 105.09 13.30 5 6 -28 123.99 13.70 4 -6 -28 82.49 9.90 -4 -6 28 84.69 11.20 4 -6 -28 61.19 10.00 4 6 -28 66.29 10.90 4 6 -28 77.99 11.20 3 -6 -28 45.70 8.10 3 -6 -28 40.90 8.80 -3 -6 28 39.10 8.60 3 6 -28 28.00 8.20 3 6 -28 36.00 8.10 -2 -6 28 47.70 7.40 2 -6 -28 44.40 8.20 2 -6 -28 48.80 9.20 2 6 -28 53.89 9.50 2 6 -28 36.10 9.20 1 -6 -28 0.70 4.50 1 -6 -28 0.90 4.20 -1 -6 28 2.80 3.70 1 6 -28 11.10 10.20 1 6 -28 5.30 5.30 0 -6 -28 -0.40 4.00 0 -6 -28 -5.10 3.50 0 6 -28 -3.40 5.80 -1 -6 -28 6.50 4.90 -1 -6 -28 9.60 5.50 1 -6 28 5.30 5.50 -1 6 -28 -0.40 5.00 -1 6 -28 3.00 5.90 -2 -6 -28 53.79 9.90 2 -6 28 54.69 10.40 -2 -6 -28 31.60 8.10 -2 6 -28 46.40 9.30 -2 6 -28 50.79 9.70 -3 -6 -28 0.60 5.10 -3 -6 -28 4.70 4.90 3 -6 28 9.80 6.50 -3 6 -28 7.60 5.90 16 -7 -28 183.18 15.60 16 -7 -28 196.48 17.30 16 -7 -28 185.18 9.90 16 7 -28 194.78 16.20 16 7 -28 185.98 15.60 15 -7 -28 14.80 3.60 15 -7 -28 18.10 8.20 15 -7 -28 5.10 4.60 15 7 -28 11.50 6.40 15 7 -28 6.00 5.60 15 7 -28 9.60 8.20 14 -7 -28 75.39 10.20 14 -7 -28 89.59 13.40 -14 -7 28 51.69 11.00 14 -7 -28 102.69 7.30 14 7 -28 78.49 11.30 14 7 -28 87.79 15.90 14 7 -28 87.49 12.20 13 -7 -28 5.80 4.40 13 -7 -28 19.50 7.00 13 -7 -28 10.40 3.60 -13 -7 28 3.40 5.00 13 -7 -28 7.40 3.30 13 7 -28 7.10 5.70 13 7 -28 4.30 5.30 12 -7 -28 4.40 3.10 -12 -7 28 6.10 7.20 12 -7 -28 -1.10 2.70 12 -7 -28 1.50 5.00 12 -7 -28 3.90 3.80 12 7 -28 2.10 5.10 12 7 -28 1.70 4.70 12 7 -28 -9.60 3.80 11 -7 -28 12.50 6.40 11 -7 -28 5.70 3.60 11 -7 -28 12.50 4.50 11 -7 -28 9.80 3.60 -11 -7 28 10.00 5.90 11 7 -28 7.70 6.00 11 7 -28 5.30 4.70 11 7 -28 7.00 5.60 -10 -7 28 0.20 6.10 10 -7 -28 10.40 4.50 10 -7 -28 1.30 2.90 10 -7 -28 3.60 5.50 10 7 -28 9.40 6.00 10 7 -28 4.20 4.90 10 7 -28 2.90 5.20 9 -7 -28 5.10 5.70 9 -7 -28 5.40 3.70 -9 -7 28 3.90 5.30 9 -7 -28 1.80 3.40 9 7 -28 9.40 5.80 9 7 -28 1.10 4.10 9 7 -28 15.20 6.20 8 -7 -28 -7.60 3.60 -8 -7 28 -2.00 3.60 8 -7 -28 -0.40 3.40 8 -7 -28 -5.70 2.90 8 7 -28 5.10 4.50 8 7 -28 2.00 5.10 8 7 -28 -2.60 4.30 -7 -7 28 4.10 4.60 7 -7 -28 -3.60 3.50 7 -7 -28 -5.60 4.10 7 -7 -28 -1.30 3.20 7 7 -28 2.40 4.80 7 7 -28 3.50 5.50 6 -7 -28 3.90 5.00 -6 -7 28 1.00 4.10 6 -7 -28 1.70 3.70 6 7 -28 -0.10 4.80 6 7 -28 12.70 6.90 5 -7 -28 -0.60 4.60 -5 -7 28 2.90 4.30 5 -7 -28 -3.60 3.50 5 7 -28 2.70 5.10 5 7 -28 -5.30 4.80 -4 -7 28 11.10 5.00 4 -7 -28 8.80 6.00 4 -7 -28 7.20 5.00 4 7 -28 16.30 6.50 4 7 -28 16.90 6.80 -3 -7 28 19.30 5.90 3 -7 -28 19.30 6.40 3 -7 -28 35.10 7.50 3 7 -28 22.80 7.10 3 7 -28 19.40 7.40 2 -7 -28 41.50 7.80 2 -7 -28 30.40 7.60 2 7 -28 35.40 9.00 1 -7 -28 54.39 9.10 1 -7 -28 48.40 9.10 -1 -7 28 43.60 8.50 1 7 -28 58.69 11.30 0 -7 28 5.30 4.40 0 -7 28 15.90 6.90 0 -7 -28 25.40 7.20 0 -7 -28 23.20 6.80 0 7 -28 20.70 7.50 0 7 -28 17.40 7.00 1 -7 28 1.50 3.70 -1 -7 -28 7.70 4.80 1 -7 28 2.20 4.60 -1 -7 -28 5.40 4.90 -1 7 -28 -2.10 4.50 -1 7 -28 -1.00 4.20 -2 -7 -28 -4.40 3.60 2 -7 28 4.20 5.50 -2 -7 -28 0.90 4.70 -2 7 -28 -6.30 3.60 -2 7 -28 -4.30 4.50 -3 -7 -28 82.39 11.90 3 -7 28 73.99 12.40 -3 -7 -28 81.99 11.10 -3 7 -28 63.99 11.10 15 -8 -28 15.50 7.60 15 -8 -28 19.70 6.90 15 8 -28 15.90 9.20 15 8 -28 19.60 7.10 14 -8 -28 -2.20 2.30 14 -8 -28 -1.30 3.80 14 8 -28 3.10 5.30 13 -8 -28 4.40 5.40 13 -8 -28 -1.60 2.20 -13 -8 28 -0.10 3.10 13 -8 -28 -5.30 2.70 13 8 -28 -0.40 4.60 13 8 -28 -0.50 4.20 13 8 -28 0.10 7.10 12 -8 -28 9.60 3.40 -12 -8 28 10.60 6.40 12 -8 -28 9.80 4.40 12 -8 -28 6.20 3.50 12 -8 -28 16.70 6.90 12 8 -28 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14.30 9 5 -29 41.50 9.30 9 5 -29 38.70 8.40 -8 -5 29 23.20 6.70 8 -5 -29 23.10 7.10 8 -5 -29 22.70 7.40 8 5 -29 18.30 5.80 8 5 -29 31.70 7.90 8 5 -29 17.30 7.10 7 -5 -29 16.00 6.60 -7 -5 29 10.20 5.20 7 -5 -29 15.40 5.30 7 5 -29 14.20 6.90 7 5 -29 17.90 6.90 6 -5 -29 15.70 6.60 6 -5 -29 13.20 5.20 -6 -5 29 5.40 4.20 6 5 -29 10.00 6.20 6 5 -29 -0.30 5.20 5 -5 -29 3.30 4.30 5 -5 -29 5.20 5.30 -5 -5 29 -2.80 3.30 5 5 -29 -1.50 4.60 5 5 -29 0.50 5.60 4 -5 -29 6.10 5.30 4 -5 -29 2.30 4.20 4 5 -29 8.40 6.10 4 5 -29 -1.50 5.10 3 -5 -29 9.90 5.60 3 -5 -29 15.50 6.20 3 5 -29 12.80 6.50 2 -5 -29 -4.20 3.80 2 -5 -29 1.10 4.60 2 5 -29 1.60 6.50 2 5 -29 -4.80 4.20 1 -5 -29 82.59 11.50 1 -5 -29 76.79 10.90 1 5 -29 82.29 12.10 0 -5 -29 10.60 5.90 0 -5 -29 9.30 5.40 0 5 -29 -7.70 4.20 0 5 -29 8.40 5.80 -1 -5 -29 92.29 12.00 -1 -5 -29 105.69 12.90 -1 5 -29 119.39 14.90 -1 5 -29 111.79 13.70 -2 -5 -29 0.80 4.80 -2 -5 -29 4.40 5.20 2 -5 29 -4.40 4.50 -2 5 -29 -5.60 4.30 -2 5 -29 12.80 6.50 15 -6 -29 7.20 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30.60 7.20 7 -6 -29 35.30 6.90 -7 -6 29 25.50 6.80 7 -6 -29 28.40 7.70 7 6 -29 53.99 10.90 7 6 -29 36.80 8.40 6 -6 -29 180.08 12.90 6 -6 -29 184.78 14.90 6 6 -29 166.98 14.80 6 6 -29 172.88 20.60 -5 -6 29 16.20 5.40 5 -6 -29 11.50 5.20 5 -6 -29 15.50 6.40 5 6 -29 27.90 8.00 -4 -6 29 76.09 9.50 4 -6 -29 78.59 10.00 4 -6 -29 87.89 11.50 4 6 -29 48.40 13.50 4 6 -29 72.79 11.20 -3 -6 29 -4.00 4.50 3 -6 -29 -3.20 4.00 3 -6 -29 3.20 4.40 3 6 -29 3.60 5.20 3 6 -29 -7.80 5.40 2 -6 -29 -3.00 3.80 2 -6 -29 -2.70 3.80 2 6 -29 5.90 5.10 2 6 -29 -4.80 8.10 1 -6 -29 1.30 4.40 1 -6 -29 1.40 4.40 1 6 -29 3.20 5.20 1 6 -29 2.60 5.60 0 -6 -29 -6.20 3.40 0 -6 -29 -6.70 3.70 0 6 -29 5.60 5.80 0 6 -29 2.90 5.70 -1 -6 -29 3.20 4.80 -1 -6 -29 2.50 4.80 1 -6 29 0.90 4.70 -1 6 -29 -5.20 4.40 -1 6 -29 -1.30 4.70 2 -6 29 40.10 9.40 15 -7 -29 33.50 4.90 15 7 -29 25.60 12.30 14 -7 -29 21.20 6.20 14 -7 -29 40.90 5.70 14 -7 -29 60.49 10.40 14 7 -29 55.39 14.50 14 7 -29 41.50 9.20 13 -7 -29 31.60 6.60 13 -7 -29 43.60 5.90 13 7 -29 48.80 9.80 13 7 -29 52.09 10.10 13 7 -29 35.10 8.90 12 -7 -29 8.30 4.10 12 -7 -29 9.90 6.10 12 -7 -29 12.20 4.10 12 7 -29 15.20 6.30 12 7 -29 13.20 6.50 12 7 -29 9.60 6.40 -11 -7 29 5.50 5.10 11 -7 -29 -0.50 2.60 11 -7 -29 7.20 5.60 11 7 -29 0.30 4.80 11 7 -29 -1.00 5.20 11 7 -29 3.70 5.00 -10 -7 29 -1.40 4.10 10 -7 -29 2.10 3.50 10 -7 -29 2.30 3.30 10 -7 -29 -1.50 4.90 10 7 -29 5.70 5.80 10 7 -29 6.80 4.90 10 7 -29 8.20 5.70 9 -7 -29 64.99 10.40 9 -7 -29 74.29 8.30 9 -7 -29 63.09 8.10 -9 -7 29 66.19 10.60 9 7 -29 87.89 15.60 9 7 -29 72.79 10.90 9 7 -29 74.39 11.10 8 -7 -29 34.90 7.70 8 -7 -29 37.90 6.60 8 -7 -29 38.30 8.50 -8 -7 29 44.40 8.70 8 7 -29 30.60 13.00 8 7 -29 40.90 8.80 7 -7 -29 146.99 14.70 7 -7 -29 148.49 12.70 -7 -7 29 146.19 14.60 7 7 -29 133.19 14.70 7 7 -29 111.79 17.70 -6 -7 29 51.29 8.80 6 -7 -29 52.19 8.00 6 -7 -29 58.79 9.70 6 7 -29 56.99 10.70 6 7 -29 48.60 12.00 5 -7 -29 113.69 11.30 5 -7 -29 101.49 12.60 -5 -7 29 105.09 11.90 5 7 -29 128.59 18.10 5 7 -29 128.19 14.90 4 -7 -29 24.70 6.30 4 -7 -29 26.80 7.50 -4 -7 29 12.70 6.10 4 7 -29 14.10 7.00 4 7 -29 11.80 10.30 3 -7 -29 29.10 7.20 -3 -7 29 23.30 6.30 3 -7 -29 29.10 6.80 3 7 -29 28.00 8.30 3 7 -29 12.00 5.90 -2 -7 29 -1.60 3.50 2 -7 -29 3.60 4.70 2 -7 -29 7.20 5.00 2 7 -29 1.10 4.90 2 7 -29 5.00 5.40 1 -7 -29 -0.90 4.20 1 -7 -29 3.10 5.00 1 7 -29 6.80 5.40 1 7 -29 -2.30 5.10 0 -7 -29 5.90 5.00 0 -7 -29 7.00 4.80 0 7 -29 5.60 5.40 0 7 -29 8.70 5.50 1 -7 29 1.00 5.50 -1 -7 -29 2.70 5.10 -1 -7 -29 10.40 5.90 -1 7 -29 7.40 5.60 -1 7 -29 -5.00 4.00 13 -8 -29 -4.00 3.30 13 -8 -29 -1.80 6.20 13 -8 -29 5.80 3.00 13 8 -29 11.90 5.90 13 8 -29 -6.20 4.40 12 -8 -29 17.90 7.60 12 -8 -29 18.90 4.10 12 8 -29 15.70 6.90 12 8 -29 13.30 6.20 12 8 -29 13.80 6.80 11 -8 -29 34.60 5.50 11 -8 -29 45.30 9.10 11 8 -29 28.60 7.90 11 8 -29 27.50 7.70 11 8 -29 36.40 9.10 10 -8 -29 91.19 7.90 10 -8 -29 73.59 11.10 -10 -8 29 58.19 14.60 10 8 -29 97.59 12.30 10 8 -29 92.89 17.20 10 8 -29 82.59 11.30 9 -8 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10 -9 -29 21.00 7.00 10 -9 -29 24.50 4.80 10 9 -29 27.40 7.80 10 9 -29 22.30 9.00 10 9 -29 25.50 7.90 9 -9 -29 18.60 4.70 9 -9 -29 15.90 6.40 9 9 -29 14.80 6.80 9 9 -29 3.10 4.20 9 9 -29 19.30 7.10 8 -9 -29 11.10 6.00 8 -9 -29 11.60 4.40 8 9 -29 14.40 6.60 8 9 -29 10.90 6.00 7 -9 -29 -2.80 2.80 7 -9 -29 -0.20 4.10 7 9 -29 0.30 4.70 7 9 -29 5.50 5.20 6 -9 -29 9.40 5.60 6 -9 -29 3.70 4.80 6 9 -29 -4.90 4.70 6 9 -29 1.50 4.80 5 -9 -29 14.70 5.30 5 -9 -29 2.80 4.30 5 9 -29 9.50 6.40 5 9 -29 5.80 5.40 4 -9 -29 1.90 3.80 4 -9 -29 0.80 4.30 4 9 -29 3.90 5.50 4 9 -29 -0.50 4.90 3 -9 -29 21.00 6.00 3 -9 -29 13.20 5.60 3 9 -29 17.90 6.90 3 9 -29 18.70 7.30 2 -9 -29 13.00 5.90 2 -9 -29 -1.40 4.20 2 9 -29 4.40 5.50 2 9 -29 6.90 6.10 8 -10 -29 -2.70 2.70 8 -10 -29 -3.90 3.20 8 10 -29 -1.50 4.60 8 10 -29 2.50 5.70 7 -10 -29 8.60 4.80 7 -10 -29 0.80 3.00 7 10 -29 -3.80 5.00 7 10 -29 -4.00 4.20 6 -10 -29 8.30 5.20 6 -10 -29 -1.00 2.90 6 10 -29 -5.40 4.30 6 10 -29 -2.40 4.30 16 0 -30 2.70 5.70 16 0 -30 3.20 4.10 16 0 -30 -2.90 4.90 -15 0 30 14.20 4.60 15 0 -30 2.40 4.80 15 0 -30 0.80 4.10 15 0 -30 3.80 5.40 14 0 -30 -2.00 3.80 14 0 -30 -2.70 4.20 14 0 -30 -1.40 3.90 13 0 -30 -3.60 5.10 13 0 -30 11.20 5.40 13 0 -30 15.00 5.90 12 0 -30 12.80 5.10 12 0 -30 15.20 7.10 12 0 -30 3.20 4.40 11 0 -30 32.90 6.50 11 0 -30 29.80 6.70 10 0 -30 68.89 8.50 10 0 -30 62.49 11.10 10 0 -30 75.19 10.10 9 0 -30 37.70 6.30 9 0 -30 36.30 9.00 9 0 -30 50.39 8.50 8 0 -30 91.59 8.10 8 0 -30 97.39 12.80 8 0 -30 94.59 11.20 7 0 -30 -2.20 4.20 7 0 -30 -7.70 4.80 6 0 -30 13.90 6.10 6 0 -30 6.30 6.80 5 0 -30 7.60 7.30 5 0 -30 19.60 7.00 4 0 -30 609.84 28.20 4 0 -30 539.25 28.80 3 0 -30 19.20 8.70 3 0 -30 25.80 8.10 2 0 -30 816.72 35.70 2 0 -30 798.32 40.10 1 0 -30 6.90 6.60 0 0 -30 300.77 22.10 0 0 -30 306.27 20.80 -1 0 -30 -8.50 5.10 -1 0 -30 10.00 6.70 -2 0 -30 10.80 6.60 -2 0 -30 14.80 6.50 16 -1 -30 17.40 6.80 16 -1 -30 25.20 6.10 16 -1 -30 29.60 8.30 16 1 -30 10.30 6.00 16 1 -30 30.60 8.00 16 1 -30 30.30 6.40 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-1 -30 -3.10 4.20 7 1 -30 -6.80 3.80 7 1 -30 -5.30 4.70 6 -1 -30 -2.80 3.70 6 -1 -30 -10.50 5.00 6 1 -30 -3.50 4.60 6 1 -30 -5.80 4.20 5 -1 -30 50.29 10.70 5 -1 -30 70.99 10.30 5 1 -30 58.59 10.20 5 1 -30 56.99 10.70 4 -1 -30 20.00 6.70 4 -1 -30 11.50 7.40 4 1 -30 20.60 7.50 4 1 -30 18.70 8.00 3 -1 -30 208.88 17.60 3 -1 -30 216.78 16.30 3 1 -30 220.08 17.20 3 1 -30 212.48 21.70 2 -1 -30 17.00 7.70 2 1 -30 10.40 6.90 1 -1 -30 203.98 16.60 1 -1 -30 239.78 20.70 1 1 -30 217.68 17.40 1 1 -30 169.58 19.20 0 -1 -30 3.00 5.60 0 1 -30 3.70 6.70 -1 -1 -30 77.39 11.90 -1 1 -30 61.79 10.80 -1 1 -30 42.20 9.70 -2 -1 -30 3.10 5.40 -2 -1 -30 7.90 5.70 -2 1 -30 -2.00 4.00 -2 1 -30 -3.00 4.10 16 -2 -30 4.80 5.60 16 -2 -30 2.10 5.90 16 -2 -30 4.10 4.10 16 2 -30 0.10 4.80 16 2 -30 10.00 5.20 16 2 -30 -1.10 5.10 15 -2 -30 40.20 8.40 15 -2 -30 53.99 10.10 15 -2 -30 49.70 7.80 15 2 -30 47.90 9.90 15 2 -30 55.19 10.40 15 2 -30 47.90 8.70 14 -2 -30 41.80 8.20 14 -2 -30 32.30 8.30 14 -2 -30 38.50 6.80 14 2 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23.50 8.00 4 -2 -30 45.60 8.80 4 2 -30 52.29 15.20 4 2 -30 20.90 7.90 3 -2 -30 19.90 6.70 3 -2 -30 12.70 6.90 3 2 -30 22.60 7.70 2 -2 -30 65.99 11.00 2 -2 -30 72.99 10.60 2 2 -30 74.99 12.00 2 2 -30 61.39 13.10 1 -2 -30 19.70 7.30 1 -2 -30 16.50 6.90 1 2 -30 27.40 9.10 1 2 -30 20.40 8.10 0 -2 -30 6.90 8.00 0 -2 -30 11.50 5.60 0 2 -30 4.40 6.10 0 2 -30 13.10 7.40 -1 -2 -30 -1.70 6.00 -1 2 -30 4.70 5.40 -1 2 -30 -1.90 5.00 16 3 -30 -0.50 4.10 15 -3 -30 10.60 5.50 15 -3 -30 -0.90 5.00 15 3 -30 7.80 5.80 15 3 -30 11.20 5.50 15 3 -30 5.60 5.70 14 -3 -30 3.20 5.50 14 -3 -30 0.10 4.00 14 -3 -30 3.50 3.90 -14 -3 30 9.10 5.00 14 3 -30 -0.80 4.30 14 3 -30 10.60 5.30 14 3 -30 3.80 5.60 13 -3 -30 7.90 5.90 -13 -3 30 5.60 4.90 13 -3 -30 7.30 4.10 13 -3 -30 2.70 4.10 13 3 -30 9.80 6.10 13 3 -30 11.70 5.60 -12 -3 30 18.70 5.70 12 -3 -30 14.30 4.90 12 -3 -30 8.30 5.00 12 -3 -30 8.60 7.40 12 3 -30 4.40 4.40 12 3 -30 6.60 5.70 12 3 -30 11.80 5.30 11 -3 -30 23.30 10.00 11 -3 -30 38.10 6.80 11 -3 -30 23.80 5.40 -11 -3 30 28.50 5.70 11 3 -30 28.40 7.00 11 3 -30 26.20 8.00 11 3 -30 24.70 6.40 10 -3 -30 27.20 6.00 10 -3 -30 24.90 8.20 -10 -3 30 29.60 8.10 10 3 -30 26.50 6.70 10 3 -30 25.50 6.80 10 3 -30 22.80 9.90 9 -3 -30 86.29 12.60 9 -3 -30 78.59 9.60 9 3 -30 94.89 11.90 9 3 -30 111.29 11.40 8 -3 -30 6.80 4.70 8 -3 -30 -4.40 5.30 8 3 -30 8.60 4.50 8 3 -30 5.10 5.30 7 -3 -30 -6.20 5.30 7 -3 -30 3.10 4.70 7 3 -30 11.60 6.10 6 -3 -30 7.80 4.60 6 -3 -30 -0.40 6.00 6 3 -30 -13.10 4.20 5 -3 -30 107.59 13.80 5 -3 -30 126.39 13.00 5 3 -30 77.49 11.70 4 -3 -30 3.40 6.80 4 -3 -30 14.00 5.80 4 3 -30 34.10 14.60 4 3 -30 -1.10 5.40 3 -3 -30 399.96 21.10 3 -3 -30 341.67 21.70 3 3 -30 372.36 24.40 3 3 -30 299.37 20.40 2 -3 -30 3.00 6.20 2 -3 -30 3.70 5.50 2 3 -30 5.50 5.90 2 3 -30 26.50 8.60 1 -3 -30 263.37 18.10 1 -3 -30 285.97 19.50 1 3 -30 273.57 24.30 1 3 -30 281.47 20.30 0 -3 -30 -1.20 5.10 0 -3 -30 -0.50 5.00 0 3 -30 2.20 6.10 0 3 -30 -1.10 5.10 -1 -3 -30 36.50 9.60 -1 3 -30 25.40 7.30 -1 3 -30 26.70 8.00 15 -4 -30 40.60 7.90 15 -4 -30 43.40 9.50 15 -4 -30 67.49 8.00 15 4 -30 66.49 11.60 15 4 -30 67.89 9.90 15 4 -30 60.99 11.10 14 -4 -30 48.80 7.20 14 -4 -30 36.60 8.60 14 -4 -30 46.60 8.50 14 4 -30 60.59 9.50 14 4 -30 45.70 9.50 14 4 -30 56.99 10.20 13 -4 -30 90.09 10.10 13 -4 -30 95.99 12.60 13 -4 -30 88.39 9.20 -13 -4 30 76.39 11.00 13 4 -30 91.69 12.50 13 4 -30 84.69 11.20 13 4 -30 87.79 12.00 12 -4 -30 102.69 9.30 12 -4 -30 83.99 15.00 -12 -4 30 104.99 12.00 12 4 -30 110.29 17.20 12 4 -30 117.29 14.30 12 4 -30 95.79 11.90 11 -4 -30 36.70 6.00 -11 -4 30 38.60 10.20 11 -4 -30 38.20 11.20 11 -4 -30 36.50 6.40 11 4 -30 38.80 7.80 11 4 -30 38.20 8.70 11 4 -30 38.40 8.00 10 -4 -30 53.59 9.80 -10 -4 30 27.70 6.20 10 -4 -30 38.90 6.80 10 4 -30 37.60 7.50 10 4 -30 19.30 6.70 10 4 -30 33.00 8.50 9 -4 -30 -1.40 5.20 9 -4 -30 -3.70 2.80 -9 -4 30 8.40 3.90 9 4 -30 -4.70 4.60 9 4 -30 -1.40 4.70 9 4 -30 5.00 4.40 8 -4 -30 8.30 6.70 8 -4 -30 24.20 6.50 8 4 -30 34.50 8.20 8 4 -30 17.10 9.30 8 4 -30 14.60 5.40 7 -4 -30 6.20 4.60 7 -4 -30 -9.60 4.90 7 4 -30 3.10 6.00 7 4 -30 2.70 5.60 6 -4 -30 144.29 15.80 6 -4 -30 156.28 12.20 6 4 -30 113.39 16.10 6 4 -30 123.79 14.10 5 -4 -30 16.50 5.40 5 -4 -30 -2.60 5.10 5 4 -30 -2.70 4.50 5 4 -30 -0.90 5.70 4 -4 -30 164.18 13.20 4 -4 -30 145.89 15.60 4 4 -30 114.79 14.50 4 4 -30 173.58 17.90 3 -4 -30 5.50 4.60 3 -4 -30 10.80 6.60 3 4 -30 3.60 5.60 3 4 -30 -1.90 5.20 2 -4 -30 99.19 12.10 2 -4 -30 106.29 13.30 2 4 -30 97.99 17.70 2 4 -30 116.69 14.50 1 -4 -30 6.20 5.30 1 -4 -30 4.60 4.90 1 4 -30 -3.60 5.10 1 4 -30 11.70 7.20 0 -4 -30 65.29 10.50 0 -4 -30 65.49 10.50 0 4 -30 66.29 11.60 0 4 -30 78.59 11.80 -1 -4 -30 8.40 5.60 -1 -4 -30 -4.30 3.60 -1 4 -30 1.00 4.80 -1 4 -30 -1.00 4.60 14 -5 -30 148.29 10.30 14 -5 -30 114.69 12.40 14 -5 -30 129.79 14.50 14 5 -30 129.79 14.90 14 5 -30 119.19 14.30 14 5 -30 124.39 13.60 13 -5 -30 116.59 10.30 13 -5 -30 97.89 9.70 13 -5 -30 115.79 14.10 13 5 -30 91.29 12.40 13 5 -30 117.19 14.40 13 5 -30 107.69 12.80 -12 -5 30 74.49 10.70 12 -5 -30 53.09 9.70 12 -5 -30 74.69 8.50 12 -5 -30 60.69 8.10 12 -5 -30 46.10 9.80 12 5 -30 63.89 11.10 12 5 -30 49.60 8.90 12 5 -30 58.29 9.70 11 -5 -30 34.30 12.60 -11 -5 30 27.50 6.80 11 -5 -30 10.30 4.30 11 5 -30 15.80 6.90 11 5 -30 22.20 7.00 11 5 -30 19.80 6.80 10 -5 -30 2.30 6.00 10 -5 -30 -5.60 4.00 10 5 -30 -3.90 4.20 10 5 -30 -4.30 4.70 10 5 -30 -1.20 3.90 -9 -5 30 50.59 8.30 9 -5 -30 35.40 8.30 9 -5 -30 48.60 7.40 9 5 -30 34.70 8.50 9 5 -30 44.60 9.60 9 5 -30 58.39 9.40 8 -5 -30 4.00 5.90 -8 -5 30 10.60 4.60 8 -5 -30 10.90 4.60 8 5 -30 0.60 5.30 8 5 -30 17.30 6.80 -7 -5 30 105.89 14.60 7 -5 -30 76.19 11.60 7 -5 -30 92.49 10.50 7 5 -30 99.39 12.60 7 5 -30 83.19 12.60 6 -5 -30 8.20 4.80 6 -5 -30 -7.80 3.80 6 5 -30 1.30 4.90 6 5 -30 1.60 5.50 5 -5 -30 15.90 7.00 5 -5 -30 25.50 6.20 5 5 -30 17.10 7.30 5 5 -30 21.10 7.40 4 -5 -30 0.80 4.80 4 -5 -30 1.30 4.10 4 5 -30 1.40 5.50 3 -5 -30 -5.70 4.00 3 -5 -30 9.20 4.90 3 5 -30 -4.20 5.00 3 5 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33.80 6.40 11 -1 -31 36.60 9.00 11 -1 -31 35.40 7.50 11 1 -31 26.50 6.60 11 1 -31 26.70 8.40 11 1 -31 31.80 7.20 10 -1 -31 7.20 3.80 10 -1 -31 -0.70 4.00 10 -1 -31 6.00 6.10 10 1 -31 -4.90 5.20 10 1 -31 4.70 5.00 10 1 -31 2.70 3.70 9 -1 -31 30.00 6.80 9 -1 -31 29.20 8.80 9 -1 -31 21.10 5.10 9 1 -31 18.50 6.10 9 1 -31 31.20 6.00 9 1 -31 34.90 8.90 8 -1 -31 -8.90 4.40 8 -1 -31 -6.80 2.90 8 1 -31 -1.50 5.60 8 1 -31 1.00 4.20 7 -1 -31 1.60 7.00 7 -1 -31 1.20 4.40 7 1 -31 -12.60 4.60 7 1 -31 1.70 4.90 6 -1 -31 7.80 5.10 6 -1 -31 -18.70 4.80 6 1 -31 2.20 4.90 6 1 -31 -4.00 5.10 5 -1 -31 174.28 14.20 5 -1 -31 135.69 18.40 5 1 -31 168.88 17.50 5 1 -31 141.99 14.90 4 -1 -31 -1.40 5.90 4 -1 -31 -2.20 4.70 4 1 -31 -3.20 5.40 4 1 -31 1.60 5.00 3 -1 -31 202.68 17.40 3 -1 -31 203.78 16.00 3 1 -31 224.48 16.90 3 1 -31 217.68 18.00 2 -1 -31 -6.10 5.00 2 -1 -31 1.90 5.50 2 1 -31 -2.50 5.40 1 -1 -31 42.00 9.00 1 1 -31 28.80 8.00 1 1 -31 32.20 8.90 14 -2 -31 37.40 7.80 14 -2 -31 39.80 9.60 14 -2 -31 51.39 8.00 14 2 -31 51.99 10.20 14 2 -31 49.99 9.50 14 2 -31 38.40 7.70 13 -2 -31 48.70 7.90 13 -2 -31 44.70 9.60 13 -2 -31 25.30 6.20 13 2 -31 31.90 7.30 13 2 -31 31.20 7.30 13 2 -31 32.20 8.30 12 -2 -31 62.19 8.50 12 -2 -31 70.29 11.50 12 -2 -31 61.19 8.40 12 2 -31 60.39 9.40 12 2 -31 73.89 10.20 12 2 -31 59.09 10.30 11 -2 -31 2.60 5.20 11 -2 -31 9.70 4.20 11 -2 -31 1.40 4.10 11 2 -31 7.10 4.70 11 2 -31 15.20 5.90 11 2 -31 17.00 7.10 10 -2 -31 28.20 6.80 10 -2 -31 34.60 7.40 10 -2 -31 35.30 8.70 10 2 -31 25.50 6.20 10 2 -31 26.20 8.20 10 2 -31 34.60 7.90 9 -2 -31 -5.50 3.20 9 -2 -31 -5.40 4.60 9 2 -31 -5.20 3.80 9 2 -31 1.10 3.50 9 2 -31 3.50 5.60 8 -2 -31 10.40 4.80 8 -2 -31 0.70 7.30 8 2 -31 -2.30 5.00 8 2 -31 4.90 4.90 7 -2 -31 -4.40 3.60 7 2 -31 1.40 5.20 7 2 -31 7.00 5.60 6 -2 -31 144.69 14.30 6 2 -31 180.28 18.40 6 2 -31 136.69 14.60 5 -2 -31 1.40 4.50 5 2 -31 1.40 5.30 5 2 -31 4.30 5.50 4 -2 -31 228.38 16.40 4 -2 -31 218.78 26.40 4 2 -31 253.57 18.90 4 2 -31 251.67 17.90 3 -2 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-31 -2.30 3.90 5 3 -31 -1.90 4.80 5 3 -31 -4.70 4.90 4 -3 -31 12.30 5.70 4 3 -31 9.80 6.30 3 -3 -31 4.20 5.00 3 3 -31 9.60 6.60 3 3 -31 0.90 5.30 2 -3 -31 1.00 4.60 2 -3 -31 4.00 5.00 2 3 -31 3.20 4.90 2 3 -31 2.60 6.00 13 -4 -31 35.40 8.80 13 -4 -31 27.50 5.60 13 4 -31 19.00 6.90 13 4 -31 27.00 6.80 13 4 -31 24.30 7.70 12 -4 -31 12.50 6.40 12 -4 -31 10.40 4.30 12 4 -31 13.20 5.50 12 4 -31 7.80 5.20 12 4 -31 6.10 6.20 11 -4 -31 7.30 4.10 -11 -4 31 6.50 4.40 11 -4 -31 5.20 5.20 11 4 -31 6.60 5.30 11 4 -31 -9.00 3.90 11 4 -31 3.10 4.50 10 -4 -31 8.70 6.10 10 -4 -31 -0.40 3.40 10 4 -31 -1.20 4.00 10 4 -31 0.40 4.80 10 4 -31 -3.30 4.30 9 -4 -31 -4.90 4.90 9 -4 -31 -2.80 3.10 9 4 -31 3.00 3.60 9 4 -31 3.90 5.20 9 4 -31 9.50 6.50 8 -4 -31 9.50 5.10 8 4 -31 4.20 5.40 8 4 -31 4.30 5.60 7 -4 -31 5.00 4.20 7 4 -31 -3.20 4.50 7 4 -31 -5.60 3.80 6 -4 -31 87.49 10.70 6 4 -31 88.99 12.70 6 4 -31 94.59 16.00 5 -4 -31 -2.00 3.70 5 4 -31 8.10 6.40 4 -4 -31 120.19 12.70 4 4 -31 69.69 11.10 4 4 -31 99.89 13.60 3 -4 -31 -3.50 3.40 3 4 -31 -3.80 4.00 3 4 -31 5.00 5.50 2 -4 -31 26.50 7.40 2 4 -31 28.30 7.80 2 4 -31 34.80 8.90 12 -5 -31 -4.40 3.80 12 5 -31 11.20 6.50 11 -5 -31 -0.10 3.20 11 -5 -31 -7.60 4.10 11 5 -31 -7.20 3.70 11 5 -31 -2.20 3.80 11 5 -31 -0.10 5.50 10 -5 -31 9.50 6.20 10 -5 -31 17.90 5.30 -10 -5 31 18.70 6.00 10 5 -31 8.20 6.50 10 5 -31 20.40 7.50 10 5 -31 14.50 6.00 9 -5 -31 67.79 8.70 9 -5 -31 46.60 10.20 9 5 -31 63.29 11.10 9 5 -31 80.09 11.00 8 -5 -31 13.00 4.90 8 5 -31 2.80 5.60 7 -5 -31 130.59 11.20 7 5 -31 101.89 17.50 7 5 -31 117.39 14.40 6 -5 -31 0.60 3.90 6 -5 -31 -5.30 9.00 6 5 -31 -0.10 4.60 6 5 -31 0.40 5.00 5 -5 -31 65.79 13.30 5 -5 -31 60.39 9.20 5 5 -31 85.59 12.70 5 5 -31 66.89 10.70 4 -5 -31 -0.10 4.10 4 -5 -31 -0.30 6.60 4 5 -31 -1.00 5.30 4 5 -31 3.20 5.50 3 -5 -31 8.90 5.00 3 5 -31 10.40 6.20 3 5 -31 11.70 6.30 10 -6 -31 22.10 7.10 10 -6 -31 22.70 5.70 10 6 -31 12.60 6.20 10 6 -31 14.00 5.90 10 6 -31 25.70 8.00 9 -6 -31 9.10 6.30 9 -6 -31 14.60 4.90 9 6 -31 10.80 6.10 9 6 -31 17.40 7.40 8 -6 -31 73.79 9.20 8 6 -31 57.29 10.60 8 6 -31 47.40 9.60 7 -6 -31 5.70 4.00 7 6 -31 11.20 6.40 7 6 -31 4.70 4.90 6 -6 -31 18.20 9.10 6 -6 -31 16.00 5.50 6 6 -31 21.10 7.90 6 6 -31 13.40 6.30 5 -6 -31 -2.10 3.00 5 -6 -31 -0.80 5.40 5 6 -31 8.70 6.00 5 6 -31 -1.40 4.50 11 0 -32 -1.50 4.50 11 0 -32 3.90 3.80 11 0 -32 -1.70 3.30 10 0 -32 50.59 10.10 10 0 -32 44.90 6.90 10 0 -32 51.49 8.60 9 0 -32 3.40 4.20 9 0 -32 2.50 5.60 8 0 -32 0.80 4.10 8 0 -32 7.80 6.20 7 0 -32 -6.50 4.10 7 0 -32 7.10 4.90 6 0 -32 18.50 7.20 6 0 -32 34.60 7.80 5 0 -32 1.10 5.70 5 0 -32 13.50 5.90 11 -1 -32 0.30 3.10 11 -1 -32 3.10 4.00 11 -1 -32 11.30 6.20 11 1 -32 3.40 3.90 11 1 -32 6.00 6.10 11 1 -32 4.60 4.80 10 -1 -32 -0.50 3.50 10 -1 -32 3.00 4.80 10 -1 -32 -2.50 4.40 10 1 -32 -0.70 3.70 10 1 -32 -2.90 3.30 10 1 -32 -0.10 5.10 9 -1 -32 4.50 4.60 9 -1 -32 6.30 6.20 9 1 -32 3.50 4.30 9 1 -32 5.20 5.20 9 1 -32 2.70 3.30 8 -1 -32 -3.30 4.30 8 -1 -32 4.10 4.60 8 1 -32 -1.60 3.50 8 1 -32 -7.50 4.30 7 -1 -32 -7.30 4.20 7 -1 -32 -3.50 3.60 7 1 -32 -0.20 4.20 7 1 -32 -2.20 5.30 6 -1 -32 -10.80 3.30 6 -1 -32 -1.80 4.00 6 1 -32 -5.90 4.20 6 1 -32 -9.70 3.10 5 -1 -32 1.10 4.60 5 -1 -32 5.50 5.60 5 1 -32 1.50 4.70 5 1 -32 -2.10 4.60 10 -2 -32 3.00 4.00 10 -2 -32 -5.90 4.40 10 2 -32 -4.70 3.80 10 2 -32 0.60 3.50 10 2 -32 -8.40 4.50 9 -2 -32 -11.00 3.90 9 -2 -32 -6.50 3.00 9 2 -32 -1.70 3.80 9 2 -32 -1.50 4.90 8 -2 -32 2.70 4.10 8 -2 -32 -4.50 4.20 8 2 -32 0.30 5.60 8 2 -32 1.00 4.20 7 -2 -32 -0.60 4.30 7 -2 -32 0.10 4.90 7 2 -32 -3.80 4.70 7 2 -32 -3.20 4.00 6 -2 -32 57.09 10.20 6 -2 -32 47.10 8.40 6 2 -32 49.00 11.30 6 2 -32 43.50 9.70 5 -2 -32 0.10 3.90 5 -2 -32 14.00 6.50 5 2 -32 1.10 5.20 5 2 -32 2.20 6.30 9 -3 -32 18.20 5.70 9 3 -32 18.20 6.70 8 -3 -32 -5.30 3.20 8 -3 -32 2.40 5.60 8 3 -32 0.10 5.50 8 3 -32 -0.50 4.90 7 -3 -32 19.80 6.20 7 -3 -32 33.00 8.30 7 3 -32 13.50 6.90 6 3 -32 3.40 4.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 51056 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p4n_b _database_code_depnum_ccdc_archive 'CCDC 2151510' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-11 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _vrf_PLAT431_p4n_b ; PROBLEM: Short Inter HL..A Contact F8_1 ..O2 . 2.77 Ang. RESPONSE: Coulomb-Interactions ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C21 Al F36 I O9 Ru' _chemical_formula_moiety 'C16 Al F36 O4, C5 I O5 Ru' _chemical_formula_weight 1335.16 _chemical_melting_point ? _space_group_crystal_system tetragonal _space_group_IT_number 85 _space_group_name_H-M_alt 'P 4/n' _space_group_name_Hall '-P 4a' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-y+1/2, x, z' 'y, -x+1/2, z' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'y-1/2, -x, -z' '-y, x-1/2, -z' _cell_length_a 13.7680(16) _cell_length_b 13.7680(16) _cell_length_c 9.5388(12) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1808.2(5) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9143 _cell_measurement_theta_min 2.5975 _cell_measurement_theta_max 31.079 _exptl_crystal_description needle _exptl_crystal_colour yellow _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.452 _exptl_crystal_F_000 1264 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.10 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 1.547 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6924 _exptl_absorpt_correction_T_max 0.7417 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 134767 _diffrn_reflns_av_unetI/netI 0.0163 _diffrn_reflns_av_R_equivalents 0.0816 _diffrn_reflns_theta_min 1.479 _diffrn_reflns_theta_max 31.523 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 14 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 3025 _reflns_number_gt 2797 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. Completness statistics refer to single and composite reflections containing twin component 1 only. ; _computing_data_collection 'Bruker BIS V6.2.15 Patch 4/2021-03-15 && APEX4 2021.10-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refined as a 2-component twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0309P)^2^+2.5837P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_number_reflns 3025 _refine_ls_number_parameters 160 _refine_ls_number_restraints 306 _refine_ls_R_factor_all 0.0288 _refine_ls_R_factor_gt 0.0250 _refine_ls_wR_factor_ref 0.0676 _refine_ls_wR_factor_gt 0.0648 _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_restrained_S_all 1.028 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.844 _refine_diff_density_min -0.976 _refine_diff_density_rms 0.097 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.750000 0.750000 0.12929(3) 0.02096(7) Uani 1 4 d S T P . . Ru1 Ru 0.750000 0.750000 0.41069(3) 0.01512(7) Uani 1 4 d S T P . . Al1 Al 0.250000 0.750000 0.000000 0.0114(2) Uani 1 4 d S T P . . O1 O 0.65236(16) 0.54715(16) 0.3796(2) 0.0255(4) Uani 1 1 d . . . . . O2 O 0.750000 0.750000 0.7330(4) 0.0249(6) Uani 1 4 d S T P . . C1 C 0.68589(18) 0.61692(19) 0.3910(3) 0.0166(4) Uani 1 1 d . . . . . C2 C 0.750000 0.750000 0.6177(4) 0.0159(7) Uani 1 4 d S T P . . O1_1 O 0.31552(14) 0.67044(13) 0.10417(19) 0.0161(3) Uani 1 1 d D U . . . C1_1 C 0.31479(17) 0.58596(17) 0.1761(2) 0.0144(4) Uani 1 1 d D U . . . C2_1 C 0.4185(2) 0.57046(19) 0.2381(3) 0.0195(5) Uani 1 1 d D U . . . F1_1 F 0.48045(12) 0.54140(14) 0.14044(19) 0.0274(4) Uani 1 1 d D U . . . F2_1 F 0.41951(13) 0.50358(13) 0.34104(18) 0.0265(4) Uani 1 1 d D U . . . F3_1 F 0.45297(13) 0.65295(13) 0.2926(2) 0.0287(4) Uani 1 1 d D U . . . C3_1 C 0.2399(2) 0.58916(18) 0.2980(3) 0.0194(5) Uani 1 1 d D U . . . F4_1 F 0.15673(13) 0.62710(15) 0.2552(2) 0.0275(4) Uani 1 1 d D U . . . F5_1 F 0.27287(14) 0.64257(15) 0.40404(18) 0.0301(4) Uani 1 1 d D U . . . F6_1 F 0.22053(13) 0.50002(14) 0.34995(19) 0.0265(4) Uani 1 1 d D U . . . C4_1 C 0.2905(2) 0.4990(2) 0.0769(3) 0.0194(5) Uani 1 1 d D U . . . F7_1 F 0.19510(15) 0.49299(14) 0.0563(2) 0.0257(4) Uani 1 1 d D U . . . F8_1 F 0.31921(15) 0.41426(12) 0.13256(18) 0.0273(4) Uani 1 1 d D U . . . F9_1 F 0.33275(14) 0.50946(13) -0.04586(17) 0.0261(4) Uani 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.02421(9) 0.02421(9) 0.01448(13) 0.000 0.000 0.000 Ru1 0.01557(9) 0.01557(9) 0.01423(15) 0.000 0.000 0.000 Al1 0.0105(3) 0.0105(3) 0.0130(5) 0.000 0.000 0.000 O1 0.0277(10) 0.0239(10) 0.0249(10) 0.0010(8) -0.0027(8) -0.0010(8) O2 0.0242(9) 0.0242(9) 0.0262(16) 0.000 0.000 0.000 C1 0.0145(10) 0.0202(11) 0.0152(10) 0.0083(9) 0.0029(8) 0.0036(9) C2 0.0172(10) 0.0172(10) 0.0132(17) 0.000 0.000 0.000 O1_1 0.0153(7) 0.0135(8) 0.0196(9) 0.0023(6) -0.0020(7) 0.0005(6) C1_1 0.0149(9) 0.0135(9) 0.0146(10) 0.0018(8) -0.0007(8) 0.0015(8) C2_1 0.0181(11) 0.0198(11) 0.0208(11) 0.0043(9) 0.0002(9) 0.0032(9) F1_1 0.0175(7) 0.0330(10) 0.0317(9) 0.0057(7) 0.0054(7) 0.0089(7) F2_1 0.0255(8) 0.0294(9) 0.0245(8) 0.0114(7) -0.0034(6) 0.0058(7) F3_1 0.0245(8) 0.0260(8) 0.0357(10) 0.0003(7) -0.0128(7) -0.0026(7) C3_1 0.0181(13) 0.0207(9) 0.0192(10) 0.0017(8) 0.0024(10) 0.0020(10) F4_1 0.0168(8) 0.0342(10) 0.0314(9) 0.0060(7) 0.0069(7) 0.0095(7) F5_1 0.0344(11) 0.0369(10) 0.0190(7) -0.0090(7) 0.0035(6) 0.0029(7) F6_1 0.0269(9) 0.0283(9) 0.0241(8) 0.0101(7) 0.0057(6) 0.0000(6) C4_1 0.0252(13) 0.0143(11) 0.0189(12) 0.0014(10) -0.0016(10) 0.0019(10) F7_1 0.0244(9) 0.0211(8) 0.0316(10) -0.0001(8) -0.0042(8) -0.0061(7) F8_1 0.0401(10) 0.0122(7) 0.0296(9) 0.0007(6) -0.0024(8) 0.0039(7) F9_1 0.0368(9) 0.0233(8) 0.0182(7) -0.0040(7) 0.0055(7) -0.0001(7) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 Ru1 2.6842(5) . ? Ru1 C2 1.974(4) . ? Ru1 C1 2.042(3) 2_665 ? Ru1 C1 2.042(3) 4_565 ? Ru1 C1 2.042(3) 3_655 ? Ru1 C1 2.042(3) . ? Al1 O1_1 1.7323(18) 7_565 ? Al1 O1_1 1.7323(18) 2_565 ? Al1 O1_1 1.7323(18) 8_665 ? Al1 O1_1 1.7323(18) . ? O1 C1 1.071(3) . ? O2 C2 1.100(5) . ? O1_1 C1_1 1.350(3) . ? C1_1 C3_1 1.555(3) . ? C1_1 C2_1 1.560(3) . ? C1_1 C4_1 1.562(4) . ? C2_1 F1_1 1.325(3) . ? C2_1 F3_1 1.336(3) . ? C2_1 F2_1 1.346(3) . ? C3_1 F4_1 1.323(3) . ? C3_1 F5_1 1.330(3) . ? C3_1 F6_1 1.350(3) . ? C4_1 F9_1 1.315(3) . ? C4_1 F7_1 1.331(3) . ? C4_1 F8_1 1.342(3) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 Ru1 C1 95.28(7) . 2_665 ? C2 Ru1 C1 95.28(7) . 4_565 ? C1 Ru1 C1 89.514(13) 2_665 4_565 ? C2 Ru1 C1 95.28(7) . 3_655 ? C1 Ru1 C1 89.514(13) 2_665 3_655 ? C1 Ru1 C1 169.43(14) 4_565 3_655 ? C2 Ru1 C1 95.29(7) . . ? C1 Ru1 C1 169.43(14) 2_665 . ? C1 Ru1 C1 89.515(14) 4_565 . ? C1 Ru1 C1 89.513(13) 3_655 . ? C2 Ru1 I1 180.0 . . ? C1 Ru1 I1 84.72(7) 2_665 . ? C1 Ru1 I1 84.72(7) 4_565 . ? C1 Ru1 I1 84.72(7) 3_655 . ? C1 Ru1 I1 84.71(7) . . ? O1_1 Al1 O1_1 109.21(6) 7_565 2_565 ? O1_1 Al1 O1_1 110.00(12) 7_565 8_665 ? O1_1 Al1 O1_1 109.21(6) 2_565 8_665 ? O1_1 Al1 O1_1 109.21(6) 7_565 . ? O1_1 Al1 O1_1 110.00(12) 2_565 . ? O1_1 Al1 O1_1 109.21(6) 8_665 . ? O1 C1 Ru1 179.5(2) . . ? O2 C2 Ru1 180.0 . . ? C1_1 O1_1 Al1 146.32(17) . . ? O1_1 C1_1 C3_1 111.1(2) . . ? O1_1 C1_1 C2_1 107.7(2) . . ? C3_1 C1_1 C2_1 109.1(2) . . ? O1_1 C1_1 C4_1 110.7(2) . . ? C3_1 C1_1 C4_1 109.4(2) . . ? C2_1 C1_1 C4_1 108.7(2) . . ? F1_1 C2_1 F3_1 107.6(2) . . ? F1_1 C2_1 F2_1 107.4(2) . . ? F3_1 C2_1 F2_1 107.1(2) . . ? F1_1 C2_1 C1_1 111.3(2) . . ? F3_1 C2_1 C1_1 110.9(2) . . ? F2_1 C2_1 C1_1 112.3(2) . . ? F4_1 C3_1 F5_1 108.2(2) . . ? F4_1 C3_1 F6_1 107.5(2) . . ? F5_1 C3_1 F6_1 106.9(2) . . ? F4_1 C3_1 C1_1 110.73(19) . . ? F5_1 C3_1 C1_1 111.0(2) . . ? F6_1 C3_1 C1_1 112.3(2) . . ? F9_1 C4_1 F7_1 108.2(3) . . ? F9_1 C4_1 F8_1 108.5(2) . . ? F7_1 C4_1 F8_1 107.1(3) . . ? F9_1 C4_1 C1_1 111.2(2) . . ? F7_1 C4_1 C1_1 110.4(2) . . ? F8_1 C4_1 C1_1 111.3(2) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_1 Al1 O1_1 C1_1 -33.7(3) 7_565 . . . ? O1_1 Al1 O1_1 C1_1 86.1(3) 2_565 . . . ? O1_1 Al1 O1_1 C1_1 -154.0(3) 8_665 . . . ? Al1 O1_1 C1_1 C3_1 -63.1(4) . . . . ? Al1 O1_1 C1_1 C2_1 177.5(2) . . . . ? Al1 O1_1 C1_1 C4_1 58.8(4) . . . . ? O1_1 C1_1 C2_1 F1_1 -76.2(3) . . . . ? C3_1 C1_1 C2_1 F1_1 163.1(2) . . . . ? C4_1 C1_1 C2_1 F1_1 43.8(3) . . . . ? O1_1 C1_1 C2_1 F3_1 43.6(3) . . . . ? C3_1 C1_1 C2_1 F3_1 -77.1(3) . . . . ? C4_1 C1_1 C2_1 F3_1 163.6(2) . . . . ? O1_1 C1_1 C2_1 F2_1 163.3(2) . . . . ? C3_1 C1_1 C2_1 F2_1 42.6(3) . . . . ? C4_1 C1_1 C2_1 F2_1 -76.7(3) . . . . ? O1_1 C1_1 C3_1 F4_1 44.9(3) . . . . ? C2_1 C1_1 C3_1 F4_1 163.4(2) . . . . ? C4_1 C1_1 C3_1 F4_1 -77.7(3) . . . . ? O1_1 C1_1 C3_1 F5_1 -75.3(3) . . . . ? C2_1 C1_1 C3_1 F5_1 43.3(3) . . . . ? C4_1 C1_1 C3_1 F5_1 162.1(2) . . . . ? O1_1 C1_1 C3_1 F6_1 165.1(2) . . . . ? C2_1 C1_1 C3_1 F6_1 -76.3(3) . . . . ? C4_1 C1_1 C3_1 F6_1 42.5(3) . . . . ? O1_1 C1_1 C4_1 F9_1 39.1(3) . . . . ? C3_1 C1_1 C4_1 F9_1 161.9(2) . . . . ? C2_1 C1_1 C4_1 F9_1 -79.0(3) . . . . ? O1_1 C1_1 C4_1 F7_1 -81.0(3) . . . . ? C3_1 C1_1 C4_1 F7_1 41.8(3) . . . . ? C2_1 C1_1 C4_1 F7_1 160.9(2) . . . . ? O1_1 C1_1 C4_1 F8_1 160.1(2) . . . . ? C3_1 C1_1 C4_1 F8_1 -77.0(3) . . . . ? C2_1 C1_1 C4_1 F8_1 42.0(3) . . . . ? _shelx_res_file ; TITL p4n_b.res in P4/n p4n_b.res created by SHELXL-2018/3 at 12:55:48 on 11-Feb-2022 REM Old TITL p4n in P4/n REM SHELXT solution in P4/n: R1 0.263, Rweak 0.029, Alpha 0.070 REM 0.152 for 117 systematic absences, Orientation as input REM Formula found by SHELXT: C89 O9 F4 Al Ru I CELL 0.71073 13.7680 13.7680 9.5388 90.000 90.000 90.000 ZERR 2.000 0.0016 0.0016 0.0012 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, 1/2-Y, Z SYMM 1/2-Y, X, Z SYMM Y, 1/2-X, Z SFAC C O F AL RU I UNIT 42 18 72 2 2 2 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 TEMP -173.150 L.S. 10 BOND $H CONF MORE -1 LIST 4 ACTA TWIN 1 0 0 0 -1 0 0 0 -1 FMAP 2 PLAN 20 WGHT 0.030900 2.583700 BASF 0.48756 FVAR 0.33630 I1 6 0.750000 0.750000 0.129288 10.25000 0.02421 0.02421 = 0.01448 0.00000 0.00000 0.00000 RU1 5 0.750000 0.750000 0.410690 10.25000 0.01557 0.01557 = 0.01423 0.00000 0.00000 0.00000 AL1 4 0.250000 0.750000 0.000000 10.25000 0.01054 0.01054 = 0.01303 0.00000 0.00000 0.00000 O1 2 0.652360 0.547154 0.379554 11.00000 0.02768 0.02389 = 0.02488 0.00095 -0.00265 -0.00096 O2 2 0.750000 0.750000 0.732999 10.25000 0.02423 0.02423 = 0.02622 0.00000 0.00000 0.00000 C1 1 0.685892 0.616919 0.390965 11.00000 0.01445 0.02024 = 0.01518 0.00830 0.00285 0.00357 C2 1 0.750000 0.750000 0.617668 10.25000 0.01718 0.01718 = 0.01323 0.00000 0.00000 0.00000 RESI CCF3 1 O1 2 0.315523 0.670443 0.104167 11.00000 0.01529 0.01355 = 0.01956 0.00230 -0.00198 0.00050 C1 1 0.314793 0.585961 0.176071 11.00000 0.01493 0.01353 = 0.01463 0.00179 -0.00073 0.00148 C2 1 0.418519 0.570464 0.238078 11.00000 0.01812 0.01975 = 0.02078 0.00433 0.00020 0.00317 F1 3 0.480453 0.541401 0.140441 11.00000 0.01751 0.03303 = 0.03169 0.00566 0.00543 0.00893 F2 3 0.419509 0.503578 0.341038 11.00000 0.02548 0.02936 = 0.02453 0.01144 -0.00344 0.00575 F3 3 0.452967 0.652953 0.292611 11.00000 0.02446 0.02598 = 0.03567 0.00032 -0.01277 -0.00257 C3 1 0.239892 0.589159 0.298041 11.00000 0.01814 0.02072 = 0.01924 0.00172 0.00239 0.00196 F4 3 0.156734 0.627103 0.255212 11.00000 0.01684 0.03419 = 0.03143 0.00597 0.00688 0.00949 F5 3 0.272867 0.642570 0.404037 11.00000 0.03436 0.03690 = 0.01899 -0.00898 0.00352 0.00287 F6 3 0.220529 0.500024 0.349951 11.00000 0.02693 0.02830 = 0.02414 0.01015 0.00566 0.00004 C4 1 0.290491 0.499048 0.076891 11.00000 0.02515 0.01430 = 0.01888 0.00143 -0.00163 0.00186 F7 3 0.195100 0.492986 0.056285 11.00000 0.02440 0.02105 = 0.03158 -0.00007 -0.00419 -0.00607 F8 3 0.319210 0.414263 0.132565 11.00000 0.04007 0.01222 = 0.02964 0.00067 -0.00237 0.00388 F9 3 0.332750 0.509456 -0.045859 11.00000 0.03680 0.02332 = 0.01825 -0.00396 0.00549 -0.00005 RESI 0 HKLF 4 REM p4n_b.res in P4/n REM wR2 = 0.0676, GooF = S = 1.073, Restrained GooF = 1.028 for all data REM R1 = 0.0250 for 2797 Fo > 4sig(Fo) and 0.0288 for all 3025 data REM 160 parameters refined using 306 restraints END WGHT 0.0309 2.5837 REM Highest difference peak 0.844, deepest hole -0.976, 1-sigma level 0.097 Q1 1 0.7528 0.7835 0.3608 11.00000 0.05 0.84 Q2 1 0.7500 0.7500 0.3384 10.25000 0.05 0.74 Q3 1 0.6816 0.5952 0.3470 11.00000 0.05 0.60 Q4 1 0.7014 0.6176 0.3624 11.00000 0.05 0.58 Q5 1 0.6779 0.6167 0.4266 11.00000 0.05 0.49 Q6 1 0.7500 0.7500 0.0323 10.25000 0.05 0.48 Q7 1 0.2500 0.7500 0.0346 10.50000 0.05 0.48 Q8 1 0.7500 0.7500 0.2555 10.25000 0.05 0.47 Q9 1 0.7500 0.7500 0.5478 10.25000 0.05 0.40 Q10 1 0.7735 0.8214 0.4555 11.00000 0.05 0.39 Q11 1 0.6177 0.6740 0.4089 11.00000 0.05 0.36 Q12 1 0.7978 0.7900 0.0642 11.00000 0.05 0.36 Q13 1 0.4157 0.6839 0.3046 11.00000 0.05 0.33 Q14 1 0.2779 0.5878 0.2405 11.00000 0.05 0.33 Q15 1 0.6752 0.6540 0.3754 11.00000 0.05 0.33 Q16 1 0.2736 0.6599 0.1351 11.00000 0.05 0.32 Q17 1 0.3051 0.5287 0.1085 11.00000 0.05 0.32 Q18 1 0.4213 0.6458 0.3399 11.00000 0.05 0.32 Q19 1 0.5723 0.6803 0.1977 11.00000 0.05 0.31 Q20 1 0.8966 0.8026 0.1341 11.00000 0.05 0.31 ; _shelx_res_checksum 48080 _shelx_hkl_file ; 1 0 0 0.40 0.60 1 0 0 0.80 0.70 0 1 0 0.00 0.40 0 1 0 -0.60 0.60 0 1 0 0.00 0.70 0 1 0 -0.20 0.50 1 0 0 0.20 0.50 1 0 0 -0.30 0.40 0 -1 0 0.20 0.70 0 1 0 0.20 0.60 0 1 0 -0.20 0.50 0 -1 0 -0.30 0.40 0 -1 0 0.70 0.70 0 -1 0 -0.20 0.40 0 -1 0 -0.40 0.30 0 -1 0 -0.20 0.30 -1 0 0 0.30 0.90 -1 0 0 -0.50 0.80 -1 0 0 0.30 1.00 -1 0 0 -0.40 0.70 -1 0 0 0.10 0.70 -1 0 0 1.00 1.00 -1 0 0 -0.70 0.60 -1 0 0 0.70 0.70 -1 -1 0 185.18 8.40 1 1 0 176.18 9.20 -1 -1 0 194.68 9.80 -1 1 0 179.18 8.70 1 -1 0 182.68 9.90 1 1 0 183.08 8.60 1 1 0 184.98 8.50 1 -1 0 179.58 9.70 1 -1 0 186.08 9.40 1 -1 0 174.18 8.90 1 -1 0 182.38 8.70 1 -1 0 183.88 8.90 -1 1 0 192.38 9.80 -1 1 0 178.48 9.30 -1 1 0 191.18 10.40 -1 -1 0 185.48 9.40 -1 1 0 193.08 9.00 -1 -1 0 185.98 10.60 -1 1 0 180.58 8.80 -1 1 0 175.98 9.10 -1 -1 0 183.98 8.60 -1 2 0 -0.40 1.20 1 -2 0 -2.20 1.20 1 -2 0 -1.00 1.50 1 -2 0 1.10 1.60 1 -2 0 -0.80 1.30 1 -2 0 1.90 2.00 2 1 0 0.20 1.20 2 1 0 -1.40 1.20 2 1 0 -1.20 1.10 2 1 0 1.40 1.60 2 1 0 0.60 2.00 2 1 0 0.90 1.40 1 -2 0 0.30 1.30 -1 2 0 1.20 1.90 -1 2 0 -0.60 1.50 1 -2 0 0.50 1.30 1 -2 0 1.30 1.30 -2 -1 0 -0.20 1.20 -2 -1 0 -1.20 1.40 -2 -1 0 -0.10 1.20 -2 -1 0 0.70 1.60 -2 -1 0 -1.30 1.80 -2 -1 0 4.00 1.70 -1 2 0 -1.30 0.90 -1 2 0 1.10 1.90 -1 2 0 -0.40 1.00 -1 2 0 -1.10 1.30 -1 2 0 -0.90 1.40 -2 0 0 2767.92 111.99 -2 0 0 2803.82 111.59 0 -2 0 2750.02 111.49 0 2 0 2747.33 111.09 0 2 0 2777.42 112.19 0 2 0 2819.02 111.59 2 0 0 2829.22 112.29 0 -2 0 2774.82 112.09 -2 0 0 2687.33 112.99 -2 0 0 2623.74 111.59 0 -2 0 2581.64 110.99 2 0 0 2782.02 113.29 -2 1 0 0.10 1.70 1 2 0 0.00 1.00 1 2 0 -0.40 1.30 1 2 0 0.00 1.50 -1 -2 0 0.70 1.50 -1 -2 0 1.30 2.20 -2 1 0 -0.70 1.30 1 2 0 2.20 2.50 2 -1 0 0.30 1.50 2 -1 0 1.30 1.90 2 -1 0 -0.50 1.90 -2 1 0 -2.50 1.60 -1 -2 0 1.10 1.30 -1 -2 0 0.90 1.80 -1 -2 0 0.00 1.50 -1 -2 0 -0.90 1.20 2 -1 0 0.50 1.40 2 -1 0 -0.60 1.00 2 -1 0 0.50 1.40 2 -1 0 0.50 1.40 2 -1 0 1.20 1.40 -2 1 0 -0.60 1.40 -2 1 0 0.30 1.50 -2 1 0 3.00 2.10 1 2 0 2.30 2.00 -2 1 0 2.60 1.60 -1 -2 0 0.90 1.70 -1 -2 0 -0.80 1.60 1 2 0 1.70 1.40 1 2 0 -0.60 1.40 1 2 0 -1.10 1.10 -2 1 0 0.10 1.10 2 2 0 904.61 40.60 2 -2 0 888.41 41.10 2 -2 0 871.51 40.60 -2 2 0 922.71 41.30 -2 2 0 824.62 39.50 2 -2 0 920.31 40.00 -2 -2 0 849.81 44.40 -2 2 0 923.91 39.50 2 2 0 922.71 39.80 -2 -2 0 790.42 40.70 2 2 0 897.81 38.00 -2 2 0 932.81 42.10 2 -2 0 901.71 41.80 2 2 0 844.12 39.60 2 2 0 920.61 38.00 2 2 0 871.91 42.40 -2 2 0 924.31 40.80 -2 -2 0 1007.80 46.30 -2 -2 0 968.70 42.70 -2 -2 0 918.51 39.30 -3 -2 0 1.90 2.20 2 -3 0 -0.40 1.50 2 -3 0 -1.80 1.60 -3 -2 0 1.50 1.70 -2 3 0 0.40 1.70 2 -3 0 0.60 2.20 -3 -2 0 2.20 4.60 3 2 0 -0.40 1.40 3 2 0 -1.90 1.70 -2 3 0 3.00 2.20 -2 3 0 1.40 1.70 -2 3 0 1.80 2.90 -3 -2 0 0.80 2.10 -2 3 0 -2.10 1.90 -3 -2 0 0.90 1.80 -3 -2 0 0.20 3.80 3 2 0 2.20 1.80 3 2 0 1.60 3.50 3 2 0 1.70 2.60 2 -3 0 -2.10 1.70 2 -3 0 0.00 1.90 2 -3 0 4.40 3.10 2 -3 0 0.80 1.90 3 2 0 0.10 2.50 -2 3 0 -0.10 1.70 2 -3 0 1.10 2.30 -1 3 0 4465.05 177.68 3 1 0 4279.97 175.88 -1 3 0 4238.48 176.68 1 -3 0 4257.37 176.28 -3 -1 0 4282.47 176.18 1 -3 0 4558.74 176.68 -3 -1 0 4599.94 176.18 -1 3 0 4119.29 176.18 -1 3 0 4345.06 176.98 1 -3 0 4373.46 177.28 3 1 0 4050.79 175.28 3 1 0 4478.05 178.88 1 -3 0 4366.76 176.88 -3 -1 0 4424.06 179.68 0 3 0 -1.10 1.40 0 3 0 -2.00 1.40 0 -3 0 -0.50 1.60 0 -3 0 -0.60 1.40 0 3 0 2.30 2.00 0 -3 0 -2.10 1.80 0 -3 0 1.00 2.00 0 -3 0 2.10 2.60 -3 0 0 0.30 2.30 -3 0 0 3.20 2.50 0 3 0 -0.10 2.10 3 0 0 -1.80 1.80 3 0 0 -1.20 2.80 0 -3 0 -1.00 1.60 3 0 0 -0.30 1.90 -3 0 0 -0.10 1.90 -3 0 0 -1.00 1.60 3 0 0 0.00 1.70 -3 0 0 -0.40 1.90 -3 0 0 0.30 1.90 -3 1 0 4720.03 189.38 3 -1 0 4642.54 188.98 3 -1 0 4443.76 188.08 -1 -3 0 4585.24 187.28 -3 1 0 4473.75 187.88 1 3 0 4640.14 186.68 3 -1 0 4880.71 188.08 -1 -3 0 4609.54 189.58 -1 -3 0 5190.48 187.48 -1 -3 0 4401.36 189.58 1 3 0 4770.32 190.18 -3 1 0 4521.05 187.28 -3 1 0 4401.56 188.98 1 3 0 4644.24 187.18 -2 -3 0 0.30 1.70 3 -2 0 1.00 1.70 -2 -3 0 -2.40 1.80 -3 2 0 -2.10 1.10 -3 2 0 0.80 2.00 -3 2 0 -1.70 2.70 -2 -3 0 0.90 1.70 -3 2 0 4.70 3.50 -3 2 0 -1.90 1.80 -3 2 0 0.20 2.20 2 3 0 1.30 2.10 2 3 0 0.00 2.10 2 3 0 -0.70 2.20 3 -2 0 -2.20 1.90 3 -2 0 -0.70 2.30 -2 -3 0 2.00 3.30 -2 -3 0 0.80 1.50 3 -2 0 1.20 2.00 -2 -3 0 0.40 2.00 2 3 0 0.30 1.50 2 3 0 -1.00 1.50 2 3 0 -2.00 1.40 3 -2 0 -1.10 2.60 -2 -3 0 0.10 2.10 3 -2 0 2.30 2.00 3 -2 0 0.10 1.80 -3 2 0 -0.90 1.70 -3 2 0 1.50 1.70 -2 -3 0 0.60 2.20 3 -2 0 1.50 2.40 -3 -3 0 1890.21 81.59 3 3 0 1895.01 81.99 -3 -3 0 1977.20 82.79 -3 3 0 1968.90 84.09 -3 3 0 1995.60 82.69 -3 3 0 1898.81 83.99 3 3 0 1862.71 86.69 3 -3 0 1962.70 85.69 -3 -3 0 1850.21 86.79 3 -3 0 1934.91 84.39 3 3 0 1936.91 83.69 3 3 0 1952.30 82.49 3 -3 0 1928.51 84.79 3 -4 0 1.30 2.70 -4 -3 0 4.90 2.90 3 -4 0 1.30 2.30 -3 4 0 -3.70 2.10 3 -4 0 0.90 2.10 3 -4 0 -2.00 1.30 -4 -3 0 0.70 2.60 -4 -3 0 0.20 1.80 -3 4 0 -0.70 1.90 -4 -3 0 1.50 2.10 4 3 0 2.30 2.90 -3 4 0 -0.40 1.90 -3 4 0 3.10 2.70 3 -4 0 2.70 3.00 -3 4 0 -3.40 2.20 -3 4 0 4.40 2.80 4 3 0 1.60 2.10 -4 -3 0 0.60 2.50 -4 -3 0 -0.70 1.90 -4 -3 0 -2.00 2.00 4 3 0 1.30 2.40 3 -4 0 0.10 2.50 3 -4 0 2.10 3.80 4 3 0 -1.20 2.00 -3 4 0 -0.10 1.90 -3 4 0 2.00 2.70 3 -4 0 -1.20 2.70 4 3 0 1.90 3.40 -4 -3 0 2.90 2.10 4 3 0 0.10 1.90 2 -4 0 4420.66 184.08 -4 -2 0 4353.16 186.48 -4 -2 0 4503.75 188.08 -2 4 0 4059.69 183.18 -2 4 0 4532.05 183.68 2 -4 0 4330.97 184.68 4 2 0 4696.63 181.88 4 2 0 4366.26 186.88 2 -4 0 4375.06 182.78 -2 4 0 4675.43 183.78 -4 -2 0 4652.63 182.78 4 2 0 4654.83 182.78 2 -4 0 4306.67 183.38 -2 4 0 4510.55 185.68 -4 -2 0 4441.06 182.78 4 1 0 -0.60 1.80 -1 4 0 3.00 2.70 -1 4 0 0.10 2.50 -1 4 0 1.10 1.70 -4 -1 0 0.40 2.40 1 -4 0 0.90 1.80 -4 -1 0 3.10 2.50 -4 -1 0 0.90 2.50 -4 -1 0 1.30 2.30 1 -4 0 -2.10 1.50 -4 -1 0 0.10 2.80 1 -4 0 -0.50 2.20 4 1 0 -1.30 2.10 1 -4 0 -0.20 1.90 1 -4 0 -1.20 1.50 1 -4 0 -0.30 2.20 1 -4 0 0.90 2.10 4 1 0 -0.90 1.80 -4 -1 0 1.30 2.10 -4 -1 0 1.30 2.70 -1 4 0 -2.30 2.90 4 1 0 2.40 2.90 -4 -1 0 -0.80 2.00 4 1 0 -1.60 3.70 4 1 0 3.10 2.90 -1 4 0 0.50 1.90 -1 4 0 0.50 1.80 1 -4 0 -3.00 1.70 4 1 0 -2.50 2.20 4 1 0 -0.50 2.50 0 4 0 6535.55 262.77 -4 0 0 6085.99 261.97 0 -4 0 6862.51 263.67 0 -4 0 6367.46 262.37 -4 0 0 6403.66 263.07 0 -4 0 6797.42 262.07 4 0 0 6326.27 263.77 -4 0 0 6390.56 265.37 0 4 0 6840.82 261.97 -4 0 0 6502.65 263.47 4 0 0 6352.26 266.17 4 -1 0 1.10 3.20 -1 -4 0 2.20 2.40 1 4 0 0.10 1.60 -1 -4 0 2.00 3.30 4 -1 0 1.30 2.20 -4 1 0 -1.60 1.80 -4 1 0 -1.90 2.00 1 4 0 -0.40 2.30 -4 1 0 2.20 2.30 4 -1 0 3.70 3.20 -4 1 0 0.50 3.00 -4 1 0 4.50 2.90 -1 -4 0 -1.60 1.90 -1 -4 0 1.80 3.10 -1 -4 0 -0.10 1.80 4 -1 0 0.60 2.70 4 -1 0 1.60 2.40 -4 1 0 0.40 2.10 -4 1 0 -0.10 1.80 1 4 0 -0.10 1.80 4 -1 0 0.10 2.20 4 -1 0 -2.00 2.00 1 4 0 0.80 1.80 1 4 0 4.00 2.30 1 4 0 1.40 4.10 -1 -4 0 1.10 1.80 -1 -4 0 0.30 2.40 4 -1 0 0.30 1.80 -1 -4 0 -2.20 1.40 -4 1 0 0.90 2.90 4 -2 0 4911.21 190.58 -4 2 0 4558.54 189.48 -2 -4 0 4914.41 187.98 -4 2 0 4540.05 188.08 -4 2 0 4326.07 190.18 -4 2 0 4719.03 191.68 2 4 0 4742.73 187.98 2 4 0 4178.78 186.38 4 -2 0 4589.94 191.08 -2 -4 0 4597.24 188.48 4 -2 0 4601.64 188.88 4 -2 0 4680.23 192.08 -2 -4 0 4580.44 192.88 -4 3 0 -1.60 2.20 4 -3 0 2.00 2.60 4 -3 0 -1.90 2.20 4 -3 0 -3.80 2.30 3 4 0 0.70 2.10 3 4 0 2.30 2.10 -4 3 0 2.70 2.60 -3 -4 0 0.00 2.20 -3 -4 0 3.90 3.20 4 -3 0 1.50 2.50 3 4 0 -0.10 2.50 -4 3 0 -1.50 2.00 -3 -4 0 -0.60 2.40 3 4 0 3.00 2.90 -4 3 0 -0.20 2.10 -4 3 0 3.10 3.50 -3 -4 0 -1.30 2.10 3 4 0 1.00 1.60 4 -3 0 0.70 2.30 -3 -4 0 0.30 1.90 4 -3 0 -4.90 3.00 -3 -4 0 -0.40 1.90 -3 -4 0 -1.10 2.20 -4 3 0 -0.60 1.70 3 4 0 1.50 2.30 -4 3 0 -2.20 2.60 4 -3 0 -0.20 1.80 -4 3 0 1.30 1.90 4 -3 0 -0.40 3.20 -3 -4 0 5.00 4.60 -4 -4 0 3866.71 143.59 4 4 0 3261.37 149.19 4 4 0 3233.98 142.99 4 4 0 3428.36 142.89 4 -4 0 3408.86 147.09 -4 4 0 3425.76 143.69 -4 4 0 3466.05 145.89 -4 -4 0 3453.75 149.99 -4 4 0 3242.58 145.09 -4 4 0 3530.05 148.49 4 -4 0 3352.26 145.79 4 -4 0 3448.56 147.69 4 -4 0 3424.16 143.79 -5 -4 0 1.60 2.90 -4 5 0 -3.10 1.70 -4 5 0 -6.30 2.90 -4 5 0 -0.10 2.90 4 -5 0 4.70 3.80 -4 5 0 3.00 2.60 -4 5 0 -1.90 2.00 5 4 0 0.60 4.40 4 -5 0 -0.20 1.90 -5 -4 0 1.60 2.30 4 -5 0 -1.00 1.90 -5 -4 0 2.20 3.30 5 4 0 -3.90 3.00 -5 -4 0 -2.80 1.60 -4 5 0 1.30 3.20 4 -5 0 4.70 3.40 -4 5 0 0.40 2.10 5 4 0 -0.80 2.00 -4 5 0 2.90 3.50 4 -5 0 1.70 3.20 -5 -4 0 2.40 2.70 4 -5 0 3.80 3.30 5 4 0 0.90 3.30 -5 -4 0 -2.70 3.40 4 -5 0 1.50 3.10 4 -5 0 6.30 4.10 -3 5 0 5003.90 227.08 3 -5 0 5387.26 228.58 5 3 0 5471.65 226.28 -5 -3 0 5710.93 226.98 -3 5 0 5630.54 231.08 -3 5 0 5704.73 228.88 3 -5 0 5257.07 226.38 -5 -3 0 5699.53 226.78 -5 -3 0 5704.73 232.88 5 3 0 5507.55 226.08 3 -5 0 5331.97 227.88 3 -5 0 5682.73 230.28 5 3 0 5609.34 232.68 -3 5 0 5619.54 227.58 5 2 0 -0.70 2.70 5 2 0 3.40 2.30 2 -5 0 2.20 2.70 2 -5 0 0.00 1.90 5 2 0 0.20 2.10 -2 5 0 -0.10 2.00 -2 5 0 0.30 2.50 2 -5 0 0.40 2.50 2 -5 0 -1.20 2.80 -5 -2 0 -2.00 3.20 -5 -2 0 -2.30 2.00 -5 -2 0 0.80 2.30 -5 -2 0 2.10 2.70 -5 -2 0 1.60 3.00 2 -5 0 1.40 2.50 -2 5 0 -1.10 2.30 -2 5 0 0.90 2.20 -5 -2 0 1.60 2.30 5 2 0 1.40 2.70 -5 -2 0 -0.70 1.90 5 2 0 4.60 3.30 -2 5 0 -1.80 2.10 2 -5 0 -0.70 1.90 2 -5 0 0.30 1.70 2 -5 0 -3.40 1.50 5 2 0 -2.00 2.50 -2 5 0 0.70 2.10 -5 -2 0 -0.80 2.40 -1 5 0 3501.95 145.59 5 1 0 3348.36 147.09 1 -5 0 3404.66 144.79 -1 5 0 3432.36 145.39 1 -5 0 3443.86 144.89 -1 5 0 3490.55 143.99 5 1 0 3471.25 143.39 5 1 0 3368.46 148.99 -5 -1 0 3446.06 144.49 5 1 0 3477.15 143.99 -5 -1 0 3508.85 143.99 1 -5 0 3406.86 144.79 -5 -1 0 3158.28 145.39 -5 -1 0 3493.25 148.69 1 -5 0 3443.46 144.09 5 0 0 0.90 2.90 0 -5 0 0.20 1.90 0 5 0 2.90 2.40 -5 0 0 1.80 2.50 0 -5 0 1.50 2.20 0 -5 0 0.20 2.80 5 0 0 0.50 2.80 -5 0 0 -1.20 2.50 0 5 0 -1.20 2.30 0 5 0 -1.20 1.80 0 -5 0 1.30 2.20 -5 0 0 1.30 3.00 -5 0 0 -0.10 2.60 5 0 0 0.00 3.10 -5 0 0 4.60 3.30 0 -5 0 5.20 3.10 0 5 0 0.30 3.20 -5 0 0 5.40 3.60 -5 0 0 1.80 2.60 -5 0 0 -0.30 1.80 5 0 0 2.20 2.80 0 5 0 1.30 2.30 0 -5 0 2.90 3.20 0 5 0 2.00 2.80 1 5 0 3446.26 142.19 -5 1 0 3495.35 145.09 -1 -5 0 3414.16 145.99 -5 1 0 3578.94 143.19 5 -1 0 3510.25 143.99 -1 -5 0 3500.65 142.69 -5 1 0 3417.86 143.09 1 5 0 3432.46 145.79 -1 -5 0 3338.97 141.49 -1 -5 0 3266.67 144.39 1 5 0 3217.08 140.99 -5 1 0 3486.95 146.09 5 -1 0 3507.65 144.59 5 -1 0 3312.87 146.69 5 -1 0 3017.30 142.79 -2 -5 0 2.20 2.70 -2 -5 0 2.30 4.20 -2 -5 0 -2.60 2.10 5 -2 0 -1.30 2.00 2 5 0 -0.30 1.80 2 5 0 0.20 1.90 5 -2 0 -1.20 2.30 -2 -5 0 -2.30 3.20 5 -2 0 -0.30 2.40 2 5 0 1.00 2.90 -2 -5 0 0.10 2.50 5 -2 0 1.70 2.30 5 -2 0 -3.40 2.80 5 -2 0 -0.30 2.30 5 -2 0 3.50 3.00 5 -2 0 2.80 3.00 -5 2 0 0.20 2.00 -5 2 0 0.20 2.30 -5 2 0 3.40 3.70 -5 2 0 -2.00 1.40 2 5 0 -3.20 1.90 2 5 0 -2.60 2.40 -2 -5 0 5.80 3.10 -2 -5 0 -1.30 1.90 -5 2 0 4.10 3.70 -5 2 0 -2.10 2.10 -5 2 0 1.70 2.50 2 5 0 1.60 2.10 -2 -5 0 -2.00 1.80 -5 2 0 0.80 2.40 -5 3 0 5338.17 241.18 5 -3 0 6088.79 242.48 -5 3 0 5936.01 244.08 -5 3 0 5957.90 241.28 -3 -5 0 5803.32 239.48 5 -3 0 6521.15 245.18 5 -3 0 5624.44 239.68 3 5 0 5853.91 245.38 3 5 0 6235.08 237.48 -5 3 0 5609.84 238.68 3 5 0 5508.65 237.98 5 -3 0 5820.02 243.38 -4 -5 0 2.40 2.90 -5 4 0 1.80 2.60 -4 -5 0 4.10 4.90 -5 4 0 -1.20 2.90 -4 -5 0 -2.50 1.90 4 5 0 -2.70 1.80 5 -4 0 -1.40 2.60 -4 -5 0 -1.70 2.80 5 -4 0 -1.30 3.00 5 -4 0 3.10 4.20 -4 -5 0 2.00 3.50 5 -4 0 -0.80 2.10 -5 4 0 -2.30 2.70 5 -4 0 0.40 2.80 -5 4 0 0.90 2.70 4 5 0 0.10 3.70 -5 4 0 5.00 4.70 5 -4 0 4.50 3.70 -4 -5 0 -0.90 2.20 -5 4 0 -0.80 2.30 -5 4 0 0.80 2.50 5 -4 0 -0.50 2.70 5 -4 0 -2.00 1.70 -4 -5 0 -0.60 2.60 -5 4 0 -1.60 1.60 -4 -5 0 -2.00 2.20 -5 5 0 708.73 34.70 -5 -5 0 739.43 44.00 5 5 0 718.33 37.50 -5 5 0 654.03 39.10 5 -5 0 730.63 36.00 -5 -5 0 741.43 37.80 5 -5 0 664.13 35.90 -5 -5 0 762.32 37.30 5 5 0 685.23 36.60 -5 -5 0 736.03 39.60 5 5 0 689.13 33.00 5 -5 0 603.94 39.30 -5 -5 0 672.13 33.90 5 -5 0 656.03 35.50 -5 -5 0 616.54 32.80 5 -5 0 637.44 36.80 -5 5 0 743.73 37.10 5 -5 0 710.13 40.30 -5 5 0 655.53 36.90 -5 -5 0 669.13 37.30 -5 -5 0 622.44 42.00 5 -5 0 630.24 40.00 -5 5 0 755.52 42.90 5 -5 0 741.23 35.10 5 5 0 738.23 33.70 -5 5 0 672.03 34.70 -5 5 0 696.13 39.20 -5 5 0 645.74 35.00 6 5 0 -1.10 3.10 5 -6 0 -4.20 2.00 -6 -5 0 -1.20 2.00 6 5 0 1.50 3.50 5 -6 0 2.30 4.90 -5 6 0 -1.00 2.30 -6 -5 0 -0.20 3.50 -5 6 0 -0.90 1.80 -5 6 0 -3.60 1.20 -5 6 0 -0.40 2.60 5 -6 0 1.60 3.20 5 -6 0 -0.40 2.30 -6 -5 0 -1.20 2.00 -5 6 0 -1.30 4.40 5 -6 0 -2.70 3.20 6 5 0 -0.20 2.40 -6 -5 0 0.10 3.20 -5 6 0 1.40 3.30 -6 -5 0 0.10 3.40 6 5 0 0.70 3.50 6 5 0 0.10 2.20 5 -6 0 -1.10 2.70 -6 -5 0 -1.60 2.40 -6 -5 0 -1.40 2.90 5 -6 0 0.40 2.60 5 -6 0 -0.50 4.00 -6 -5 0 -3.50 2.50 -5 6 0 2.20 3.20 -5 6 0 1.00 3.00 6 5 0 -8.00 3.30 -6 -4 0 2288.07 101.19 4 -6 0 2225.88 104.89 4 -6 0 1987.20 102.49 -4 6 0 2320.67 103.79 -6 -4 0 2296.77 100.19 4 -6 0 2508.85 98.79 4 -6 0 2326.07 99.19 -6 -4 0 2252.57 102.39 -4 6 0 2283.37 101.99 -6 -4 0 2334.77 96.59 -4 6 0 2298.37 106.29 -4 6 0 2285.67 99.79 4 -6 0 2343.97 103.69 4 -6 0 2220.68 101.19 6 4 0 2369.66 100.89 -6 -4 0 2064.39 96.29 -6 -4 0 2097.49 106.69 6 4 0 1991.10 99.29 6 4 0 2404.66 103.29 6 4 0 2272.17 96.29 6 4 0 2246.88 107.79 6 4 0 2373.46 96.39 -6 -4 0 2258.87 96.39 -4 6 0 2565.14 104.89 3 -6 0 -0.40 2.50 -6 -3 0 -1.70 2.60 -3 6 0 1.20 4.40 3 -6 0 -3.20 2.90 -6 -3 0 3.30 3.80 -6 -3 0 -3.40 1.80 -6 -3 0 -1.40 2.20 -3 6 0 -2.30 2.50 6 3 0 -3.80 5.50 -3 6 0 -1.50 2.80 -3 6 0 -1.80 1.80 -3 6 0 0.50 2.40 -3 6 0 0.80 3.80 3 -6 0 -0.80 2.00 -6 -3 0 -3.30 1.80 3 -6 0 -2.70 2.40 -6 -3 0 3.60 4.20 6 3 0 2.30 2.60 6 3 0 -3.10 3.30 -6 -3 0 0.10 3.80 -3 6 0 2.00 3.10 -6 -3 0 0.00 2.60 3 -6 0 -0.10 2.30 -3 6 0 3.50 3.20 3 -6 0 3.50 3.10 -2 6 0 3066.99 135.79 2 -6 0 3162.38 134.89 -2 6 0 2970.70 134.29 -6 -2 0 3131.19 138.19 6 2 0 2914.51 133.69 -6 -2 0 3226.08 141.29 2 -6 0 3131.09 135.89 -2 6 0 3204.18 137.79 6 2 0 3317.07 133.39 2 -6 0 3138.09 136.49 6 2 0 3287.37 134.29 -6 -2 0 3033.90 133.69 2 -6 0 3161.98 135.09 -6 -2 0 3221.48 135.09 6 2 0 3060.49 138.79 -1 6 0 -0.70 2.30 -6 -1 0 0.40 2.90 -6 -1 0 0.10 2.80 1 -6 0 -1.00 1.90 1 -6 0 0.50 2.30 -1 6 0 -4.20 1.60 6 1 0 4.70 3.70 1 -6 0 -0.10 2.90 6 1 0 0.80 2.80 -1 6 0 -4.40 1.70 1 -6 0 -0.10 2.30 6 1 0 -1.20 2.10 6 1 0 0.10 4.00 1 -6 0 -0.60 2.10 -6 -1 0 1.20 2.30 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4 0 1903.01 95.79 -8 -4 0 2128.39 91.89 4 -8 0 2174.68 93.69 -8 -4 0 2095.19 97.89 4 -8 0 2056.09 93.39 -4 8 0 2076.19 102.79 -4 8 0 2201.48 95.89 8 4 0 2124.79 99.19 -8 -4 0 2091.09 97.79 -8 -4 0 2183.08 97.79 4 -8 0 2110.89 93.99 -4 8 0 2183.88 93.39 8 4 0 2117.09 90.99 -8 -4 0 2018.00 105.79 4 -8 0 2001.60 100.09 -8 -4 0 2187.28 92.79 -3 8 0 -2.40 1.40 8 3 0 1.80 3.50 3 -8 0 -1.80 3.10 -3 8 0 1.40 2.90 8 3 0 -2.80 1.70 3 -8 0 -1.90 2.60 -3 8 0 -1.70 5.20 -8 -3 0 8.90 5.50 -8 -3 0 9.80 5.20 -8 -3 0 2.60 4.00 -8 -3 0 3.30 3.20 8 3 0 2.20 4.00 -3 8 0 5.50 4.20 -3 8 0 1.50 2.90 -8 -3 0 -3.90 3.80 3 -8 0 2.10 4.30 8 3 0 2.00 2.70 8 3 0 3.70 4.30 3 -8 0 -3.60 2.50 -8 -3 0 -1.40 2.20 -8 -3 0 -0.90 5.00 -3 8 0 1.40 3.50 3 -8 0 1.70 3.20 3 -8 0 -2.90 1.80 8 3 0 1.80 5.30 3 -8 0 -1.50 3.90 -8 -3 0 3.50 4.80 3 -8 0 -3.30 1.40 8 2 0 5666.53 231.78 -8 -2 0 5302.87 240.38 -8 -2 0 5543.75 234.48 -8 -2 0 5443.26 232.98 8 2 0 5555.84 239.18 -8 -2 0 5477.95 237.18 -2 8 0 5643.14 237.28 -2 8 0 5360.36 233.28 2 -8 0 5781.52 234.48 -2 8 0 5760.32 236.58 8 2 0 5607.54 232.98 2 -8 0 5561.04 235.68 2 -8 0 5708.13 235.68 2 -8 0 5383.06 233.88 8 1 0 -1.40 2.50 -1 8 0 -4.40 1.80 -1 8 0 -2.90 3.80 -8 -1 0 -1.20 2.40 -1 8 0 -3.10 1.90 1 -8 0 0.50 2.20 1 -8 0 -0.40 3.30 1 -8 0 0.30 3.70 -8 -1 0 2.10 4.60 -8 -1 0 2.80 2.70 -8 -1 0 7.80 5.20 1 -8 0 2.90 3.20 8 1 0 0.20 4.00 -8 -1 0 -0.80 2.70 1 -8 0 -2.10 2.00 8 1 0 2.30 3.90 8 1 0 -0.90 3.90 1 -8 0 4.30 3.70 8 1 0 -2.70 2.10 8 1 0 -4.40 2.50 -1 8 0 2.40 3.20 -1 8 0 0.50 3.80 -8 -1 0 -2.00 2.20 -8 -1 0 2.90 3.70 -8 -1 0 1.90 4.70 8 1 0 -1.40 3.30 1 -8 0 4.60 4.00 8 1 0 3.20 3.30 1 -8 0 3.10 3.10 -1 8 0 3.60 4.10 -8 0 0 1728.23 83.79 0 8 0 1717.43 76.79 0 8 0 1756.22 78.39 8 0 0 1732.03 81.79 8 0 0 1487.65 78.29 -8 0 0 1745.83 81.99 0 -8 0 1742.53 77.19 0 -8 0 1844.62 77.09 -8 0 0 1652.53 86.09 0 8 0 1762.92 82.89 0 8 0 1574.34 79.79 8 0 0 1790.82 80.49 8 0 0 1505.75 75.89 0 -8 0 1690.43 82.19 0 -8 0 1750.32 84.29 0 -8 0 1822.02 77.29 0 8 0 1530.35 83.89 8 0 0 1735.33 85.19 8 0 0 1468.25 81.09 0 -8 0 1837.32 80.29 8 0 0 1733.43 89.09 -8 0 0 1686.43 78.29 0 8 0 1779.12 76.39 -8 0 0 1705.73 76.89 -8 0 0 1797.22 83.39 0 -8 0 1882.01 81.89 0 -8 0 1818.42 84.09 -8 0 0 1798.82 77.99 -8 0 0 1763.32 79.49 8 0 0 1682.43 80.29 1 8 0 6.60 4.50 -1 -8 0 -1.50 3.80 -8 1 0 -1.30 2.80 1 8 0 -1.70 4.20 1 8 0 -0.10 2.50 1 8 0 -1.10 3.90 -1 -8 0 0.90 2.90 -8 1 0 0.90 3.40 -1 -8 0 -0.20 2.60 -8 1 0 -1.60 2.60 -1 -8 0 -3.20 2.20 -1 -8 0 0.60 3.50 8 -1 0 -3.80 3.20 -8 1 0 -2.30 2.10 -8 1 0 -0.80 3.00 -8 1 0 4.20 4.30 -1 -8 0 5.30 4.50 1 8 0 -2.40 2.30 -8 1 0 1.50 3.30 8 -1 0 -0.30 3.30 -8 1 0 -1.10 3.40 -1 -8 0 8.10 6.00 -1 -8 0 1.50 2.70 8 -1 0 -2.20 3.20 1 8 0 0.70 2.50 8 -1 0 3.10 3.80 -8 2 0 5641.44 232.78 -8 2 0 5299.27 228.48 2 8 0 5360.86 233.98 -2 -8 0 5287.67 227.68 -2 -8 0 5412.36 226.38 2 8 0 5778.42 225.88 -2 -8 0 5602.04 234.78 -8 2 0 5336.87 231.78 8 -2 0 5176.48 229.48 8 -2 0 5269.77 230.18 -2 -8 0 5122.49 230.58 8 -2 0 5728.43 237.08 2 8 0 5560.94 227.38 -8 2 0 5237.28 227.28 8 -2 0 5514.55 230.28 -3 -8 0 0.80 3.30 -8 3 0 1.30 3.30 8 -3 0 0.70 3.70 -8 3 0 -7.00 5.80 -8 3 0 -3.90 3.80 -3 -8 0 -3.20 1.90 8 -3 0 -0.20 2.70 -8 3 0 0.30 2.80 3 8 0 2.10 3.30 -3 -8 0 4.20 4.90 3 8 0 1.80 2.30 -8 3 0 1.30 3.70 3 8 0 -3.90 1.60 3 8 0 -4.10 3.20 8 -3 0 4.50 5.40 -3 -8 0 -0.10 2.60 8 -3 0 8.10 5.20 -3 -8 0 -1.70 6.00 -3 -8 0 1.90 2.90 -3 -8 0 -0.10 2.80 -8 3 0 1.40 2.40 -8 3 0 1.40 4.70 8 -3 0 -1.90 2.70 8 -3 0 7.30 4.50 3 8 0 -2.00 2.60 3 8 0 -1.10 2.30 -3 -8 0 0.50 4.70 -8 3 0 4.00 5.40 8 -3 0 -0.30 2.40 8 -3 0 -1.50 2.20 -8 4 0 2122.59 94.69 -8 4 0 2181.28 92.99 4 8 0 2067.69 89.39 8 -4 0 2105.79 93.69 8 -4 0 2168.38 97.99 -4 -8 0 2142.69 97.19 4 8 0 2100.99 92.29 8 -4 0 2002.20 99.19 -4 -8 0 2037.80 93.69 -4 -8 0 2122.79 90.49 -4 -8 0 2070.19 102.59 -8 4 0 2001.80 94.99 -4 -8 0 2206.78 98.79 -4 -8 0 2023.70 94.79 -8 4 0 2118.99 92.89 8 -4 0 2015.80 92.49 -8 4 0 2102.59 98.29 4 8 0 2026.30 88.39 4 8 0 1984.50 93.89 8 -4 0 2184.28 95.49 -4 -8 0 2088.99 90.89 -4 -8 0 2026.00 103.79 8 -4 0 2102.99 103.89 -8 4 0 2020.40 99.49 -8 4 0 2038.20 101.99 -8 4 0 1878.11 90.39 8 -5 0 0.50 3.70 5 8 0 -7.50 3.60 5 8 0 -0.50 2.80 -8 5 0 -3.10 2.80 -5 -8 0 -1.70 2.10 -5 -8 0 1.50 3.10 -8 5 0 4.90 5.00 -8 5 0 -1.00 2.30 -5 -8 0 -2.90 6.80 8 -5 0 3.40 7.10 8 -5 0 2.80 3.80 -5 -8 0 -3.80 4.20 -8 5 0 -0.50 5.60 -5 -8 0 -1.20 2.10 8 -5 0 2.00 6.10 5 8 0 2.80 4.30 8 -5 0 0.00 2.30 -8 5 0 1.40 2.80 -8 5 0 -2.10 2.30 -5 -8 0 1.00 3.90 -5 -8 0 4.70 4.60 8 -5 0 2.50 5.50 -8 5 0 4.60 4.40 8 -5 0 6.30 4.30 8 -5 0 0.20 3.10 5 8 0 -1.90 2.10 -5 -8 0 3.90 4.30 -8 5 0 2.10 3.30 8 -6 0 2782.92 120.49 8 -6 0 2747.63 120.59 -8 6 0 2708.03 130.39 -6 -8 0 2924.71 116.79 6 8 0 2622.64 119.49 8 -6 0 2803.72 118.89 -8 6 0 2794.82 117.59 -8 6 0 2531.65 117.29 6 8 0 2750.02 115.79 -8 6 0 2773.52 121.29 -6 -8 0 2610.54 120.69 8 -6 0 2596.44 126.29 -8 6 0 2526.95 124.39 6 8 0 2805.82 114.79 -8 6 0 2717.53 121.99 -6 -8 0 2470.75 129.29 8 -6 0 2611.84 123.19 -6 -8 0 2686.43 125.49 -6 -8 0 2716.83 121.09 -6 -8 0 2755.12 123.39 8 -6 0 2630.44 129.09 8 -6 0 2729.53 128.99 6 8 0 2657.43 121.49 -8 6 0 2682.13 118.79 -6 -8 0 2720.73 116.59 -8 6 0 2676.73 126.09 8 -6 0 2821.92 120.39 -6 -8 0 2729.33 133.59 -8 7 0 0.10 3.40 -8 7 0 0.10 2.70 -7 -8 0 -0.20 4.70 7 8 0 3.40 7.10 -7 -8 0 0.10 4.10 -8 7 0 -3.60 3.10 8 -7 0 -2.20 3.20 8 -7 0 0.20 4.80 -7 -8 0 3.40 4.90 7 8 0 1.20 2.70 7 8 0 -1.90 4.00 8 -7 0 -4.20 3.10 8 -7 0 0.30 3.40 8 -7 0 1.00 3.70 8 -7 0 -6.40 5.40 -7 -8 0 -0.40 2.90 8 -7 0 2.90 6.00 7 8 0 -3.80 2.80 -7 -8 0 0.80 2.80 -8 7 0 5.90 7.50 7 8 0 0.00 2.60 8 -7 0 -0.50 2.70 -7 -8 0 2.90 6.70 -7 -8 0 -1.60 2.60 -7 -8 0 -3.70 2.30 -8 7 0 -1.40 5.70 -8 7 0 -5.70 3.90 7 8 0 -2.80 3.90 -8 8 0 517.35 38.00 8 -8 0 589.24 37.80 -8 8 0 498.55 35.70 8 8 0 560.64 44.30 8 -8 0 518.85 33.90 8 -8 0 496.65 31.80 8 -8 0 558.44 34.60 -8 8 0 519.85 32.30 8 8 0 549.54 38.10 8 8 0 483.05 34.00 -8 8 0 460.05 40.20 8 -8 0 523.25 39.40 8 8 0 501.75 28.70 -8 -8 0 546.15 43.40 -8 8 0 497.25 32.60 -8 -8 0 475.45 34.40 -8 -8 0 514.95 36.30 -8 -8 0 517.55 31.60 8 -8 0 508.65 40.00 -8 8 0 510.55 38.00 8 8 0 505.65 29.40 -8 -8 0 512.55 30.40 8 -8 0 568.74 34.90 8 8 0 553.44 33.90 -8 -8 0 509.75 34.40 8 -8 0 569.94 41.80 -8 8 0 593.44 36.40 -8 8 0 549.85 32.70 9 8 0 2.70 5.60 -9 -8 0 0.10 3.10 -8 9 0 4.50 7.10 8 -9 0 -2.10 3.40 8 -9 0 -11.70 5.90 9 8 0 -2.90 6.10 -9 -8 0 3.80 6.10 -9 -8 0 -2.90 1.80 9 8 0 -5.10 3.70 -8 9 0 -1.80 3.10 -9 -8 0 4.20 5.20 9 8 0 3.80 3.30 8 -9 0 3.40 4.60 9 8 0 -3.30 3.30 -8 9 0 0.40 7.00 -8 9 0 -4.10 2.10 -9 -8 0 -0.80 5.90 8 -9 0 2.30 4.00 8 -9 0 -2.40 2.90 8 -9 0 0.60 4.40 -9 -8 0 -1.60 3.90 9 8 0 0.90 2.70 -8 9 0 -1.80 2.40 8 -9 0 3.50 4.70 -8 9 0 -1.50 3.70 -9 -8 0 -2.00 7.10 -8 9 0 -4.00 4.30 -8 9 0 8.40 6.10 8 -9 0 -12.40 6.80 -9 -8 0 1.60 5.60 -7 9 0 799.72 45.70 7 -9 0 810.52 46.00 -7 9 0 867.31 46.10 7 -9 0 793.52 46.30 9 7 0 780.12 50.29 7 -9 0 838.42 53.19 -9 -7 0 838.02 49.10 7 -9 0 834.92 49.50 7 -9 0 832.42 47.00 -7 9 0 894.11 51.39 -7 9 0 839.02 56.49 -9 -7 0 799.32 49.10 7 -9 0 833.92 45.00 -7 9 0 821.82 52.19 -7 9 0 878.41 45.60 -9 -7 0 784.62 42.80 -9 -7 0 811.42 57.79 -9 -7 0 894.11 44.90 9 7 0 751.22 55.29 -9 -7 0 832.32 50.19 9 7 0 773.72 41.40 9 7 0 791.02 41.30 7 -9 0 784.92 53.39 -9 -7 0 785.12 47.40 9 7 0 857.71 47.30 7 -9 0 873.51 54.69 -7 9 0 863.91 52.29 -7 9 0 816.22 47.80 9 7 0 797.52 46.80 -9 -6 0 0.30 3.30 6 -9 0 5.10 5.40 6 -9 0 -3.30 2.80 -6 9 0 0.30 2.70 -6 9 0 -0.60 5.30 -9 -6 0 -1.90 6.00 -9 -6 0 -2.10 3.20 6 -9 0 -2.40 3.50 -9 -6 0 -5.60 5.20 9 6 0 -4.80 2.40 6 -9 0 0.10 3.20 6 -9 0 -0.30 2.90 6 -9 0 -0.20 4.00 -6 9 0 -0.60 2.50 6 -9 0 -5.90 6.10 9 6 0 -0.40 2.80 -9 -6 0 -0.10 2.90 -9 -6 0 3.60 5.50 -6 9 0 3.10 3.60 -6 9 0 2.60 4.50 6 -9 0 -1.00 5.10 -6 9 0 11.10 7.60 9 6 0 0.30 2.60 -9 -6 0 2.30 6.90 -6 9 0 2.20 5.10 9 6 0 -5.10 4.00 -6 9 0 -2.60 3.40 -9 -6 0 -2.50 2.70 9 6 0 4.00 7.70 9 6 0 1.70 5.40 5 -9 0 953.10 57.19 -5 9 0 972.20 49.99 -5 9 0 1034.70 56.59 5 -9 0 912.51 49.90 9 5 0 960.90 60.89 5 -9 0 1109.29 51.19 -9 -5 0 855.31 47.10 5 -9 0 971.10 54.29 9 5 0 957.80 55.09 5 -9 0 924.11 57.29 -9 -5 0 989.30 53.89 -9 -5 0 933.11 53.79 -9 -5 0 982.80 48.00 5 -9 0 942.01 49.40 -5 9 0 843.32 54.29 -5 9 0 955.40 51.69 5 -9 0 1051.59 57.49 -5 9 0 983.50 59.69 9 5 0 875.01 51.79 9 5 0 1005.50 52.69 -9 -5 0 890.21 58.49 -9 -5 0 1013.60 49.10 -5 9 0 950.20 49.20 5 -9 0 926.11 50.39 9 5 0 1029.50 47.40 9 5 0 888.31 46.70 -9 -5 0 1004.30 54.29 -9 -5 0 1020.00 60.19 -9 -5 0 1158.08 77.99 -9 -5 0 874.61 51.89 9 4 0 3.80 6.10 -4 9 0 -5.30 3.50 -4 9 0 5.10 5.60 9 4 0 0.50 3.00 -4 9 0 0.10 3.00 4 -9 0 0.50 2.60 -4 9 0 1.10 4.80 -4 9 0 -4.10 1.80 -9 -4 0 0.70 2.60 4 -9 0 3.20 3.20 -9 -4 0 5.20 5.20 4 -9 0 2.30 3.40 -9 -4 0 -2.30 2.70 -9 -4 0 -1.90 5.20 4 -9 0 1.30 6.30 -9 -4 0 -0.10 3.50 -9 -4 0 0.20 5.00 9 4 0 1.00 5.10 4 -9 0 3.60 5.00 -9 -4 0 3.10 4.20 4 -9 0 0.80 5.00 4 -9 0 -3.60 2.30 -4 9 0 4.70 4.20 9 4 0 2.90 4.60 9 4 0 6.00 4.70 4 -9 0 0.20 3.30 9 4 0 -0.30 2.70 -9 -4 0 3.10 3.00 -3 9 0 1821.62 91.59 -9 -3 0 1962.70 96.89 9 3 0 1899.81 90.29 9 3 0 1946.11 92.29 3 -9 0 1862.91 93.89 -9 -3 0 1920.21 85.49 -9 -3 0 1921.81 91.49 3 -9 0 1999.90 87.29 -9 -3 0 1754.02 89.09 -3 9 0 1902.61 95.89 3 -9 0 2125.29 87.39 -3 9 0 1791.72 93.19 -3 9 0 1849.91 86.19 -3 9 0 1946.01 88.29 3 -9 0 1871.01 87.09 -9 -3 0 1943.51 100.19 3 -9 0 1904.61 92.69 -3 9 0 1780.72 85.89 3 -9 0 1945.91 87.29 9 3 0 1895.91 84.29 -9 -3 0 1915.81 92.29 -9 -3 0 2003.20 85.99 3 -9 0 1940.21 92.19 3 -9 0 2028.00 94.99 -9 -3 0 1850.11 89.49 9 3 0 1803.02 97.59 9 3 0 1974.50 83.89 9 3 0 1841.62 87.89 -9 -2 0 -0.90 2.20 -2 9 0 6.10 6.30 -2 9 0 -2.10 2.00 2 -9 0 0.10 3.30 9 2 0 1.30 4.50 9 2 0 3.00 3.20 2 -9 0 6.40 3.70 2 -9 0 -2.70 3.50 -9 -2 0 -5.40 3.30 -9 -2 0 1.50 3.50 -2 9 0 2.10 3.60 2 -9 0 2.60 5.40 -9 -2 0 -2.30 4.30 -9 -2 0 -9.70 3.40 2 -9 0 0.90 3.10 2 -9 0 -0.30 2.40 9 2 0 -1.40 4.60 -2 9 0 1.70 4.80 -2 9 0 -2.80 3.40 -9 -2 0 5.50 5.70 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1.60 4.10 0 9 0 -0.30 3.40 9 0 0 -0.70 4.40 9 0 0 0.20 3.00 0 -9 0 1.60 3.50 -9 0 0 1.40 3.60 0 -9 0 0.90 3.10 0 9 0 -2.50 2.10 -9 0 0 -2.50 2.10 0 -9 0 -1.20 2.80 9 0 0 -3.30 2.60 0 -9 0 1.50 3.70 0 9 0 3.50 3.70 -1 -9 0 505.75 31.40 1 9 0 578.14 33.80 -1 -9 0 635.84 41.10 -1 -9 0 591.64 36.00 -9 1 0 520.15 32.80 -1 -9 0 543.55 31.10 1 9 0 598.64 36.90 1 9 0 554.04 31.30 -9 1 0 553.44 32.60 -1 -9 0 559.54 36.20 1 9 0 615.14 31.40 -9 1 0 544.85 39.10 -1 -9 0 545.25 37.50 -9 1 0 561.84 38.30 9 -1 0 526.85 38.00 -1 -9 0 555.84 35.10 -9 1 0 596.74 32.60 9 -1 0 660.63 37.00 -9 1 0 560.94 32.90 9 -1 0 503.25 40.70 9 -1 0 600.34 34.90 -9 1 0 619.24 37.70 -9 1 0 556.74 36.40 -1 -9 0 555.24 31.70 1 9 0 573.84 34.90 -9 2 0 -1.00 2.30 -2 -9 0 0.30 2.60 2 9 0 2.00 4.30 9 -2 0 3.40 5.70 -2 -9 0 -2.20 1.80 2 9 0 -5.40 3.90 -9 2 0 -2.00 2.10 2 9 0 2.40 2.70 -9 2 0 -1.80 3.30 9 -2 0 -3.80 4.50 -2 -9 0 2.90 3.30 2 9 0 -0.10 3.80 -9 2 0 -2.20 2.20 9 -2 0 -1.60 4.80 9 -2 0 3.50 5.00 9 -2 0 1.20 3.60 -9 2 0 0.30 3.90 -2 -9 0 3.20 5.40 9 -2 0 0.60 2.70 -9 2 0 8.40 6.60 -2 -9 0 -0.30 4.20 -2 -9 0 -2.20 2.30 -9 2 0 0.50 3.00 9 -2 0 0.80 3.10 9 -2 0 4.00 3.50 2 9 0 1.50 2.80 -2 -9 0 3.70 6.10 -9 2 0 -0.30 4.60 -2 -9 0 0.10 3.20 2 9 0 2.70 3.20 3 9 0 1943.71 84.99 -3 -9 0 1872.31 98.79 -3 -9 0 1882.41 92.19 -3 -9 0 1993.70 85.99 9 -3 0 2064.99 89.39 9 -3 0 1903.51 95.69 -9 3 0 1920.31 90.89 3 9 0 2042.60 100.99 -3 -9 0 1977.60 90.89 -9 3 0 2024.10 87.09 -3 -9 0 1992.90 88.59 9 -3 0 1871.91 94.29 -9 3 0 1929.21 89.19 3 9 0 1981.20 90.49 9 -3 0 1866.71 99.49 9 -3 0 1770.32 89.69 9 -3 0 1916.11 88.29 -9 3 0 1897.81 95.59 -3 -9 0 1851.21 92.19 3 9 0 1676.83 83.09 -3 -9 0 2002.40 97.29 -3 -9 0 1883.31 85.89 3 9 0 1940.51 90.79 -9 3 0 1874.61 96.59 9 -3 0 1960.30 88.39 3 9 0 2060.89 89.19 -9 3 0 1915.21 87.89 -9 3 0 1970.80 93.59 9 -3 0 1946.21 94.09 -9 3 0 1876.01 87.19 4 9 0 1.40 4.30 4 9 0 0.20 2.30 -4 -9 0 0.80 3.80 -4 -9 0 -1.60 1.90 -9 4 0 -4.50 2.80 -4 -9 0 -0.90 3.70 9 -4 0 2.00 6.20 9 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0 397.56 37.90 10 -14 0 463.45 37.30 10 -14 0 419.66 33.70 10 -14 0 498.65 49.20 -14 -10 0 442.66 32.50 10 -14 0 413.26 36.40 14 10 0 407.26 39.90 14 10 0 458.95 34.80 9 -14 0 1.50 4.50 14 9 0 0.10 7.70 -9 14 0 2.50 5.60 -9 14 0 0.00 19.10 -14 -9 0 0.90 9.40 14 9 0 2.40 3.90 9 -14 0 0.10 5.40 -14 -9 0 6.30 11.40 -14 -9 0 -0.20 3.30 -9 14 0 -5.60 14.80 -14 -9 0 -2.10 3.30 9 -14 0 -1.10 9.30 -14 -9 0 -4.90 4.20 9 -14 0 3.60 12.80 14 9 0 -2.80 3.20 -14 -9 0 1.40 13.10 14 9 0 0.00 10.50 9 -14 0 -3.00 4.30 14 9 0 2.00 3.90 9 -14 0 2.70 19.50 14 9 0 -7.70 10.90 -9 14 0 1.50 6.10 -14 -8 0 506.35 50.39 8 -14 0 616.14 40.80 14 8 0 534.15 38.00 14 8 0 458.05 48.30 14 8 0 478.95 31.10 -14 -8 0 534.85 41.50 8 -14 0 553.54 50.09 8 -14 0 499.15 46.60 14 8 0 569.84 32.30 8 -14 0 536.25 48.00 8 -14 0 541.75 37.40 -14 -8 0 489.95 35.00 -8 14 0 534.15 41.20 -14 -8 0 522.05 35.60 8 -14 0 543.25 39.90 -14 -8 0 474.15 42.20 8 -14 0 519.25 41.90 14 8 0 526.45 38.10 -14 -8 0 490.05 42.00 -14 -8 0 481.15 50.49 -8 14 0 471.55 36.60 -8 14 0 518.15 47.90 -8 14 0 536.25 50.99 8 -14 0 516.65 39.10 14 8 0 483.55 42.70 -7 14 0 1.20 5.10 14 7 0 -1.00 4.10 7 -14 0 5.50 5.80 -14 -7 0 0.60 3.70 -14 -7 0 3.20 5.90 -14 -7 0 6.90 16.60 -7 14 0 0.50 4.00 7 -14 0 -0.20 7.00 14 7 0 4.70 4.50 -14 -7 0 -3.80 9.40 -7 14 0 10.60 13.60 -14 -7 0 -5.00 9.60 -7 14 0 7.90 12.40 14 7 0 -0.70 8.60 -7 14 0 -4.10 11.30 7 -14 0 -3.30 3.40 7 -14 0 11.00 15.90 -14 -7 0 -0.90 4.40 -14 -7 0 9.70 9.50 -14 -7 0 11.80 12.20 -14 -7 0 -0.40 4.50 -14 -7 0 0.10 4.20 -7 14 0 -2.90 4.50 14 7 0 14.50 11.80 7 -14 0 1.00 3.70 7 -14 0 4.10 10.20 7 -14 0 -3.40 9.10 14 7 0 -4.90 7.10 14 7 0 -2.20 3.20 7 -14 0 14.40 7.90 14 6 0 472.95 30.30 14 6 0 475.65 36.10 -6 14 0 542.45 36.20 14 6 0 402.16 37.50 6 -14 0 465.75 33.60 -14 -6 0 444.46 31.70 -6 14 0 361.36 41.60 6 -14 0 441.56 34.60 14 6 0 435.06 28.80 6 -14 0 440.66 41.50 -14 -6 0 440.76 37.20 14 6 0 434.96 35.10 6 -14 0 376.06 32.40 -6 14 0 412.46 43.00 -14 -6 0 442.06 37.00 -6 14 0 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725.33 44.20 14 2 0 681.93 55.69 -14 -2 0 698.73 42.70 14 2 0 801.32 48.70 14 2 0 785.82 50.49 -2 14 0 686.73 49.50 2 -14 0 745.43 53.29 14 2 0 768.32 50.59 14 2 0 768.92 41.60 -14 -2 0 788.92 47.60 -14 -2 0 655.03 55.29 2 -14 0 761.22 52.09 2 -14 0 724.73 53.69 2 -14 0 740.63 44.40 2 -14 0 680.23 46.90 -2 14 0 648.94 44.60 -2 14 0 787.92 57.69 -14 -2 0 584.24 46.30 -14 -2 0 654.73 42.90 -2 14 0 685.23 42.70 2 -14 0 724.33 54.89 14 2 0 712.33 41.80 2 -14 0 785.42 52.29 -14 -1 0 1.40 5.20 14 1 0 -2.50 3.00 1 -14 0 -1.30 3.00 14 1 0 -4.60 3.00 -1 14 0 2.80 5.40 -1 14 0 -1.20 3.90 -1 14 0 -4.30 8.60 14 1 0 -3.90 3.10 14 1 0 -8.50 7.20 1 -14 0 -4.50 10.80 1 -14 0 4.10 7.80 1 -14 0 3.20 4.60 -1 14 0 14.80 9.90 -14 -1 0 -3.70 8.30 1 -14 0 6.10 5.90 1 -14 0 12.10 6.60 -14 -1 0 -15.30 7.30 -14 -1 0 1.30 3.50 -1 14 0 0.60 3.30 1 -14 0 -2.50 3.60 1 -14 0 -3.40 6.20 -14 -1 0 -2.40 3.00 -1 14 0 -1.60 8.30 14 1 0 -4.20 8.80 -14 -1 0 2.40 4.40 1 -14 0 -3.90 2.50 -14 -1 0 -16.90 9.60 14 1 0 -3.20 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466.95 46.20 8 14 0 522.55 31.20 -14 9 0 9.40 23.70 14 -9 0 -14.60 16.90 -9 -14 0 -1.00 3.00 -14 9 0 -1.00 3.10 -9 -14 0 4.00 13.20 -14 9 0 9.90 15.60 -9 -14 0 7.00 5.70 9 14 0 2.60 7.80 -9 -14 0 6.50 8.10 -14 9 0 0.90 5.40 14 -9 0 -4.80 9.70 9 14 0 2.40 3.50 14 -9 0 14.40 19.60 -9 -14 0 2.30 5.10 -14 9 0 -4.70 6.00 14 -9 0 7.40 6.10 9 14 0 2.90 4.10 9 14 0 6.50 12.80 -9 -14 0 13.10 11.60 14 -9 0 -0.10 3.60 14 -9 0 -5.80 4.10 14 -9 0 6.00 12.40 14 -9 0 -2.50 4.60 -14 9 0 -20.80 10.50 -10 -14 0 380.16 34.50 -14 10 0 438.26 33.40 -10 -14 0 417.96 33.40 14 -10 0 450.45 37.40 -14 10 0 371.16 41.60 10 14 0 470.35 27.80 10 14 0 460.35 33.50 -10 -14 0 419.36 43.10 14 -10 0 426.96 54.99 -10 -14 0 367.56 35.10 -10 -14 0 403.96 46.00 -14 10 0 409.56 54.59 14 -10 0 488.05 38.20 -10 -14 0 420.06 30.90 14 -10 0 508.05 52.19 14 -10 0 399.46 47.90 -14 10 0 480.05 47.40 14 -10 0 341.07 38.90 14 -10 0 452.35 48.20 10 14 0 398.36 27.80 10 14 0 407.76 35.40 14 -10 0 489.85 45.80 -14 10 0 385.76 34.00 -14 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159.38 26.40 -11 -15 0 110.19 29.30 15 -11 0 156.98 35.60 11 15 0 142.49 22.40 -15 11 0 173.58 28.80 11 15 0 150.18 17.50 -15 11 0 168.78 35.60 15 -11 0 165.68 25.20 -15 11 0 179.48 32.80 15 -11 0 122.39 26.40 15 -12 0 42.40 35.70 12 15 0 -1.20 10.00 12 15 0 23.40 13.90 -15 12 0 1.80 6.10 -15 12 0 5.80 7.90 15 -12 0 -19.20 23.20 12 15 0 1.00 3.00 -12 -15 0 -0.70 5.30 -15 12 0 -12.10 27.30 -12 -15 0 -14.40 15.30 -12 -15 0 5.50 22.30 12 15 0 0.60 3.50 15 -12 0 -1.00 3.30 -12 -15 0 3.40 7.00 15 -12 0 -1.90 3.90 -15 12 0 -49.70 25.20 -12 -15 0 7.80 5.80 -12 -15 0 -10.90 12.20 15 -12 0 27.40 15.60 15 -12 0 -81.49 33.60 15 -12 0 1.20 6.30 -15 13 0 40.40 32.00 -13 -15 0 62.99 13.80 -13 -15 0 92.49 28.50 15 -13 0 51.39 27.90 15 -13 0 78.59 17.60 -13 -15 0 89.09 28.40 -13 -15 0 78.99 17.40 -13 -15 0 53.29 21.00 15 -13 0 80.99 22.60 -13 -15 0 52.49 15.60 13 15 0 69.69 16.70 13 15 0 68.79 13.70 13 15 0 70.99 9.70 15 -13 0 -23.00 45.20 -15 13 0 58.29 19.00 15 -13 0 66.09 18.30 13 15 0 64.09 10.10 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9 -16 0 4.30 26.80 -16 -9 0 -5.50 15.80 -9 16 0 12.60 18.80 9 -16 0 2.10 6.40 16 9 0 -1.30 4.60 16 9 0 1.30 3.80 16 9 0 4.10 13.40 -9 16 0 8.50 7.70 -16 -9 0 9.10 17.20 -16 -9 0 -3.00 5.50 16 9 0 14.00 11.20 16 9 0 8.80 5.00 9 -16 0 17.10 15.90 16 9 0 14.00 15.00 9 -16 0 -3.10 11.50 9 -16 0 -5.60 4.70 -16 -9 0 3.60 5.60 9 -16 0 3.60 4.80 -16 -9 0 -13.00 13.10 9 -16 0 -5.50 20.30 9 -16 0 11.70 8.30 -16 -9 0 -2.00 3.80 16 8 0 134.09 16.90 8 -16 0 181.18 32.90 -8 16 0 187.48 36.90 8 -16 0 153.88 23.60 8 -16 0 184.88 26.70 8 -16 0 168.88 27.00 8 -16 0 179.68 26.50 -8 16 0 165.48 26.60 16 8 0 184.38 35.30 16 8 0 164.98 18.40 8 -16 0 173.48 24.70 -16 -8 0 132.29 30.40 16 8 0 221.18 26.70 -16 -8 0 172.08 22.50 8 -16 0 180.78 37.50 -16 -8 0 142.99 26.30 -16 -8 0 173.28 27.40 8 -16 0 110.69 23.30 -16 -8 0 225.68 31.80 16 8 0 178.28 24.00 -16 -8 0 141.59 20.70 16 8 0 208.48 32.80 -16 -7 0 9.70 13.70 7 -16 0 -3.20 3.20 -16 -7 0 -2.20 3.80 -16 -7 0 -7.80 12.50 -7 16 0 -1.10 5.50 7 -16 0 -2.10 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558.94 34.20 -4 11 -3 585.94 44.50 -4 11 -3 608.94 37.60 11 4 -3 534.05 25.90 4 -11 -3 514.65 36.70 -11 -4 -3 621.44 46.20 4 -11 -3 584.34 35.10 -11 -4 -3 506.55 41.80 -11 -4 -3 572.84 45.90 4 -11 -3 548.95 36.10 -11 -4 -3 577.44 39.90 4 -11 -3 570.04 36.60 11 4 -3 515.15 28.70 -4 11 -3 522.85 33.00 11 4 -3 584.04 43.10 -4 11 -3 567.84 41.10 4 -11 -3 570.74 36.40 -4 11 -3 657.73 40.40 4 -11 -3 551.84 38.90 -11 -4 -3 591.94 38.60 11 4 -3 545.55 28.10 11 4 -3 533.95 36.70 -11 -4 -3 589.24 38.00 -11 -4 3 601.44 34.80 11 4 3 570.34 44.60 4 -11 3 582.54 35.70 4 -11 3 554.04 33.30 11 4 3 558.44 37.40 11 4 3 530.15 41.30 -4 11 3 512.35 36.50 11 4 3 596.84 37.40 -4 11 3 527.65 36.30 -11 -4 3 503.25 37.40 4 -11 3 529.85 35.10 -4 11 3 606.74 44.40 4 -11 3 551.74 39.90 -4 11 3 517.35 44.10 4 -11 3 565.94 42.40 11 4 3 571.44 47.90 -11 -4 3 516.75 45.00 -11 -4 3 619.54 34.40 -11 -4 3 584.04 29.90 -4 11 3 544.85 43.00 4 -11 3 623.34 42.90 -4 11 3 551.54 35.90 11 4 3 539.45 43.50 -11 -4 3 563.94 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110.29 20.30 10 -11 4 97.99 22.30 -11 -10 4 102.59 26.00 -10 11 4 135.09 31.00 -11 -10 4 113.29 22.10 10 -11 4 148.59 24.30 -11 -10 4 149.88 23.50 -10 11 4 96.79 29.90 10 -11 4 133.19 19.70 11 10 4 77.29 18.70 -11 -10 4 112.09 11.70 10 -11 4 119.59 20.20 10 -11 4 102.59 19.10 11 10 4 116.39 19.50 11 10 4 104.99 26.10 -10 11 4 81.69 20.30 -11 -10 4 99.59 13.30 10 -11 4 129.19 29.50 10 -11 4 150.78 27.80 11 10 4 109.29 25.50 -11 -10 4 126.19 26.30 -10 11 4 151.78 30.30 10 -11 4 144.29 27.50 -11 -10 4 125.19 10.10 11 10 4 117.99 25.00 -11 -10 4 105.69 29.60 11 10 4 111.89 19.00 -10 11 4 125.29 22.40 -11 -10 4 130.99 12.80 9 -11 -4 426.86 26.70 -11 -9 -4 379.16 43.10 9 -11 -4 427.66 35.00 9 -11 -4 519.15 35.50 9 -11 -4 504.95 48.70 -11 -9 -4 346.37 47.40 -9 11 -4 366.76 50.29 -9 11 -4 425.86 36.60 9 -11 -4 488.05 45.90 9 -11 -4 469.25 30.30 -11 -9 -4 484.95 43.10 -9 11 -4 481.75 41.60 -11 -9 -4 510.35 45.50 -9 11 -4 441.56 42.40 -9 11 -4 412.26 35.70 -11 -9 -4 490.85 36.00 -9 11 -4 438.66 36.00 -9 11 -4 422.16 29.70 -11 -9 -4 459.95 35.30 9 -11 -4 466.75 36.10 -11 -9 -4 407.46 35.00 -9 11 -4 405.26 31.80 -11 -9 -4 448.66 38.50 -11 -9 -4 405.46 45.20 -11 -9 -4 437.06 42.00 9 -11 -4 450.45 26.70 9 -11 -4 473.25 31.80 9 -11 -4 490.65 42.00 -11 -9 4 481.75 27.50 -9 11 4 476.45 36.60 -9 11 4 429.36 44.70 11 9 4 373.26 32.10 -11 -9 4 427.96 27.10 9 -11 4 409.16 34.90 -11 -9 4 533.15 64.79 -9 11 4 453.85 35.40 -11 -9 4 377.06 43.00 -11 -9 4 500.85 24.80 11 9 4 516.45 44.50 9 -11 4 461.95 36.60 9 -11 4 436.26 41.30 -9 11 4 455.05 34.00 -11 -9 4 379.66 43.10 -11 -9 4 458.65 36.40 -11 -9 4 437.06 37.80 -9 11 4 461.75 41.70 -9 11 4 414.16 41.50 11 9 4 437.76 47.80 9 -11 4 429.26 41.60 9 -11 4 493.35 46.30 9 -11 4 420.86 31.40 9 -11 4 389.66 33.60 -11 -9 4 474.65 24.30 9 -11 4 502.75 41.20 11 9 4 448.86 40.30 -11 -9 4 413.46 70.29 -8 11 -4 95.49 24.90 -11 -8 -4 51.69 17.80 -8 11 -4 67.69 18.00 -8 11 -4 82.49 17.20 -8 11 -4 74.49 12.10 -11 -8 -4 92.89 24.80 -11 -8 -4 84.39 16.10 8 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16.40 8.20 1 6 13 -17.40 14.50 6 -1 13 6.80 8.80 6 -1 13 1.90 5.20 6 -1 13 18.90 11.40 -1 -6 13 7.40 6.80 -1 -6 13 7.80 6.80 -1 -6 13 -15.80 17.60 6 -1 13 11.50 25.70 6 -1 13 7.50 18.00 -6 1 13 12.50 8.40 1 6 13 1.50 3.70 -6 1 13 -7.50 25.40 1 6 13 3.50 7.40 1 6 13 -28.00 24.80 -1 -6 13 6.90 15.10 -1 -6 13 47.70 26.10 6 -1 13 30.60 36.70 -6 2 -13 -0.20 5.20 -6 2 -13 -25.30 29.70 -2 -6 -13 -8.00 18.00 -2 -6 13 19.80 8.60 2 6 13 20.40 30.90 -2 -6 13 22.10 9.70 -6 2 13 5.20 7.10 -6 2 13 22.70 25.10 -2 -6 13 -9.00 23.20 2 6 13 22.80 16.50 2 6 13 26.70 12.60 6 -2 13 4.70 32.40 2 6 13 13.60 7.20 6 -2 13 14.10 9.60 6 -2 13 21.40 21.20 -2 -6 13 17.50 14.30 6 -2 13 8.00 8.40 -3 -6 -13 0.30 21.70 -6 3 -13 -5.80 37.80 -6 3 -13 0.50 7.70 -3 -6 -13 -0.80 3.70 6 -3 13 -11.40 24.50 -3 -6 13 1.20 4.70 -3 -6 13 -5.50 14.40 6 -3 13 -0.20 6.70 3 6 13 0.50 6.30 6 -3 13 18.40 35.60 3 6 13 -4.30 29.70 6 -3 13 7.90 21.80 -6 3 13 2.30 26.40 3 6 13 -3.60 31.70 6 -3 13 0.50 6.30 6 -3 13 2.70 6.90 -6 3 13 7.10 7.80 -4 -6 -13 49.50 13.10 -4 -6 -13 50.59 27.00 6 -4 -13 62.29 22.40 6 -4 13 48.30 23.40 4 6 13 64.79 18.10 6 -4 13 73.49 29.10 4 6 13 72.69 36.90 4 6 13 41.90 13.00 4 6 13 10.40 21.50 6 -4 13 16.70 11.00 -4 -6 13 55.49 13.10 6 -4 13 24.80 34.20 -4 -6 13 52.79 19.20 3 -7 -13 -7.30 18.90 7 3 13 35.10 35.60 7 3 13 1.70 21.70 -7 -3 13 57.29 18.00 7 3 13 32.20 12.70 7 3 13 29.60 14.60 2 -7 -13 1.20 3.10 2 -7 -13 -33.60 17.20 -7 -2 13 -6.60 21.10 7 2 13 13.30 9.40 -2 7 13 17.40 12.10 -2 7 13 64.39 34.90 7 2 13 5.20 37.90 7 2 13 11.50 9.90 -7 -2 13 4.90 6.40 2 -7 13 -2.50 18.60 2 -7 13 21.90 10.80 7 2 13 27.50 22.70 7 1 13 110.79 24.30 7 1 13 45.70 25.80 7 1 13 111.89 41.30 7 1 13 98.89 21.10 -7 -1 13 89.39 11.20 -7 -1 13 135.59 30.40 1 -7 13 95.59 20.20 -1 7 13 138.29 37.80 -1 7 13 98.69 21.00 -7 -1 13 125.99 19.80 1 -7 13 106.49 25.20 0 -7 -13 44.00 18.40 0 -7 -13 0.90 2.40 7 0 13 -33.50 18.70 7 0 13 8.90 37.40 7 0 13 8.40 10.30 -7 0 13 4.80 5.80 7 0 13 1.60 5.50 0 -7 13 -0.20 4.10 0 -7 13 -0.10 16.20 -7 0 13 12.20 25.70 0 7 13 8.40 31.80 0 7 13 -3.50 5.60 7 -1 13 118.89 24.90 -7 1 13 178.38 46.50 7 -1 13 70.49 35.30 1 7 13 162.68 40.50 1 7 13 108.39 22.00 7 -1 13 85.69 27.40 7 -1 13 97.29 26.20 -1 -7 13 70.09 16.40 -1 -7 13 97.69 23.20 1 7 13 88.99 13.60 7 -1 13 70.59 41.70 1 7 13 124.49 21.50 -2 -7 13 5.90 6.10 2 7 13 -52.99 31.20 7 -2 13 4.10 7.80 7 -2 13 -25.40 33.10 7 -2 13 0.40 8.40 2 7 13 23.90 17.50 -2 -7 13 -2.10 17.30 2 7 13 10.50 6.30 2 7 13 2.20 7.40 -7 2 13 10.40 8.70 -7 2 13 7.40 26.40 7 -2 13 -6.90 35.90 3 7 13 76.49 36.00 3 7 13 33.10 14.40 7 -3 13 44.80 15.00 3 7 13 86.49 37.50 7 -3 13 18.30 25.10 3 7 13 55.29 20.90 0 0 14 9.30 17.10 0 0 14 -0.60 3.90 -1 0 14 148.49 24.70 0 -1 14 110.19 19.10 0 -1 14 119.69 24.10 0 1 14 132.29 19.70 0 1 14 185.88 28.40 1 0 14 131.59 21.00 1 0 14 161.38 29.10 -1 0 14 145.69 19.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 76585 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p-1_a_CCDC3 _database_code_depnum_ccdc_archive 'CCDC 2159967' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-03-18 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C68 H2 Al4 F114 O26 Ru3' _chemical_formula_moiety '2(C24 Al2 F55 O6), C14 O14 Ru3, C6 H2 F4' _chemical_formula_weight 3811.83 _chemical_melting_point ? _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.819(3) _cell_length_b 12.940(3) _cell_length_c 19.477(5) _cell_angle_alpha 102.636(12) _cell_angle_beta 103.912(17) _cell_angle_gamma 92.736(17) _cell_volume 2805.5(12) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9782 _cell_measurement_theta_min 2.417 _cell_measurement_theta_max 30.5615 _exptl_crystal_description plate _exptl_crystal_colour colourless _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.256 _exptl_crystal_F_000 1828 _exptl_crystal_size_max 0.231 _exptl_crystal_size_mid 0.134 _exptl_crystal_size_min 0.115 _exptl_absorpt_coefficient_mu 0.689 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6919 _exptl_absorpt_correction_T_max 0.7463 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min 0.857 _shelx_estimated_absorpt_T_max 0.925 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 227209 _diffrn_reflns_av_unetI/netI 0.0343 _diffrn_reflns_av_R_equivalents 0.0779 _diffrn_reflns_theta_min 1.622 _diffrn_reflns_theta_max 32.107 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_limit_l_max 28 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measured_fraction_theta_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_point_group_measured_fraction_full 0.991 _reflns_number_total 19545 _reflns_number_gt 15945 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS V6.2.15 Patch 4/2021-03-15 && APEX4 2021.10-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0388P)^2^+3.3326P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_number_reflns 19545 _refine_ls_number_parameters 1265 _refine_ls_number_restraints 10839 _refine_ls_R_factor_all 0.0513 _refine_ls_R_factor_gt 0.0382 _refine_ls_wR_factor_ref 0.0962 _refine_ls_wR_factor_gt 0.0869 _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_restrained_S_all 1.086 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.877 _refine_diff_density_min -0.805 _refine_diff_density_rms 0.094 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.04897(2) 0.08141(2) 0.65584(2) 0.01560(4) Uani 1 1 d . . . . . Ru2 Ru 0.000000 0.000000 0.500000 0.01413(4) Uani 1 2 d S . P . . Al1 Al 0.66650(5) 0.54907(5) 0.80351(3) 0.01610(10) Uani 1 1 d . . . . . Al2 Al 0.59089(5) 0.80376(5) 0.78366(3) 0.01610(10) Uani 1 1 d . . . . . F1 F 0.62391(10) 0.67519(9) 0.79338(6) 0.0198(2) Uani 1 1 d . . . . . C3 C -0.12003(18) 0.10187(16) 0.63674(11) 0.0205(4) Uani 1 1 d . . . . . O3 O -0.21580(14) 0.11279(14) 0.62393(9) 0.0287(3) Uani 1 1 d . . . . . O4 O -0.00724(15) -0.14811(13) 0.67128(10) 0.0292(3) Uani 1 1 d . . . . . O5 O 0.30189(13) 0.02908(13) 0.65431(9) 0.0253(3) Uani 1 1 d . . . . . O6 O -0.13858(14) 0.19193(13) 0.47829(9) 0.0282(3) Uani 1 1 d . . . . . O7 O -0.23014(14) -0.12495(14) 0.49817(9) 0.0276(3) Uani 1 1 d . . . . . C1 C 0.08557(18) 0.14271(16) 0.76292(11) 0.0215(4) Uani 1 1 d . . . . . C2 C 0.07996(17) 0.22062(16) 0.63457(11) 0.0195(3) Uani 1 1 d . . . . . O1 O 0.10750(15) 0.17836(14) 0.82260(8) 0.0291(3) Uani 1 1 d . . . . . O2 O 0.09560(14) 0.30003(12) 0.62199(9) 0.0254(3) Uani 1 1 d . . . . . C4 C 0.01245(18) -0.06607(17) 0.66503(11) 0.0212(4) Uani 1 1 d . . . . . C5 C 0.21128(17) 0.04906(16) 0.65594(10) 0.0195(3) Uani 1 1 d . . . . . C6 C -0.08740(17) 0.12199(16) 0.48537(11) 0.0189(3) Uani 1 1 d . . . . . C7 C -0.14501(17) -0.08023(16) 0.49970(10) 0.0194(3) Uani 1 1 d . . . . . O1_1 O 0.54759(15) 0.46273(13) 0.75283(9) 0.0295(3) Uani 1 1 d D U . . . C1_1 C 0.46670(18) 0.38248(16) 0.74832(11) 0.0226(4) Uani 1 1 d D U . . . C2_1 C 0.4400(2) 0.31070(18) 0.66981(13) 0.0283(4) Uani 1 1 d D U . . . F1_1 F 0.52392(15) 0.24750(14) 0.66294(10) 0.0459(4) Uani 1 1 d D U . . . F2_1 F 0.33828(13) 0.24745(11) 0.65244(8) 0.0354(3) Uani 1 1 d D U . . . F3_1 F 0.43106(14) 0.36769(13) 0.62082(8) 0.0372(3) Uani 1 1 d D U . . . C3_1 C 0.3530(2) 0.42942(19) 0.76188(13) 0.0305(5) Uani 1 1 d D U . . . F4_1 F 0.37839(16) 0.51010(14) 0.81953(9) 0.0459(4) Uani 1 1 d D U . . . F5_1 F 0.29694(14) 0.46443(12) 0.70479(9) 0.0389(3) Uani 1 1 d D U . . . F6_1 F 0.27810(14) 0.35648(15) 0.77227(9) 0.0434(4) Uani 1 1 d D U . . . C4_1 C 0.5101(2) 0.31553(19) 0.80502(14) 0.0320(5) Uani 1 1 d D U . . . F7_1 F 0.50159(15) 0.36364(13) 0.87061(8) 0.0388(3) Uani 1 1 d D U . . . F8_1 F 0.44849(18) 0.21958(13) 0.78585(11) 0.0528(5) Uani 1 1 d D U . . . F9_1 F 0.62231(15) 0.30091(15) 0.80990(10) 0.0470(4) Uani 1 1 d D U . . . O1_3 O 0.69207(13) 0.54450(12) 0.89242(8) 0.0220(3) Uani 1 1 d D U . . . C1_3 C 0.74321(17) 0.59508(17) 0.96304(11) 0.0222(4) Uani 1 1 d D U . . . C2_3 C 0.86382(19) 0.65497(19) 0.96937(12) 0.0270(4) Uani 1 1 d D U . . . F1_3 F 0.94498(12) 0.58751(14) 0.96598(9) 0.0401(4) Uani 1 1 d D U . . . F2_3 F 0.90155(14) 0.73041(14) 1.03055(8) 0.0414(4) Uani 1 1 d D U . . . F3_3 F 0.85527(14) 0.70059(12) 0.91364(8) 0.0350(3) Uani 1 1 d D U . . . C3_3 C 0.6617(2) 0.6762(2) 0.99023(13) 0.0333(5) Uani 1 1 d D U . . . F4_3 F 0.55095(13) 0.63222(16) 0.96981(10) 0.0473(4) Uani 1 1 d D U . . . F5_3 F 0.66538(16) 0.76024(14) 0.96155(10) 0.0461(4) Uani 1 1 d D U . . . F6_3 F 0.69017(15) 0.71117(17) 1.06237(9) 0.0506(5) Uani 1 1 d D U . . . C4_3 C 0.7599(2) 0.5108(2) 1.00918(14) 0.0374(6) Uani 1 1 d D U . . . F7_3 F 0.65867(16) 0.47787(17) 1.01987(10) 0.0522(5) Uani 1 1 d D U . . . F8_3 F 0.83424(17) 0.55058(18) 1.07442(9) 0.0573(5) Uani 1 1 d D U . . . F9_3 F 0.80147(16) 0.42641(15) 0.97580(11) 0.0501(4) Uani 1 1 d D U . . . O1_5 O 0.48920(14) 0.83500(15) 0.83146(8) 0.0282(3) Uani 1 1 d D U . . . C1_5 C 0.37688(17) 0.85056(16) 0.83119(11) 0.0200(3) Uani 1 1 d D U . . . C2_5 C 0.3623(2) 0.97032(19) 0.83750(14) 0.0356(5) Uani 1 1 d D U . . . F1_5 F 0.40500(17) 1.02780(13) 0.90481(9) 0.0483(4) Uani 1 1 d D U . . . F2_5 F 0.24916(17) 0.98724(15) 0.81613(11) 0.0591(6) Uani 1 1 d D U . . . F3_5 F 0.41723(18) 1.00728(13) 0.79405(10) 0.0518(5) Uani 1 1 d D U . . . C3_5 C 0.28980(19) 0.78379(17) 0.76058(12) 0.0248(4) Uani 1 1 d D U . . . F4_5 F 0.32608(15) 0.68863(11) 0.74132(8) 0.0368(3) Uani 1 1 d D U . . . F5_5 F 0.28404(12) 0.83011(11) 0.70444(7) 0.0281(3) Uani 1 1 d D U . . . F6_5 F 0.18148(13) 0.77015(15) 0.76730(9) 0.0425(4) Uani 1 1 d D U . . . C4_5 C 0.3495(2) 0.8171(2) 0.89797(13) 0.0319(5) Uani 1 1 d D U . . . F7_5 F 0.33636(19) 0.71193(14) 0.88621(9) 0.0516(5) Uani 1 1 d D U . . . F8_5 F 0.25169(15) 0.85344(18) 0.91086(9) 0.0522(5) Uani 1 1 d D U . . . F9_5 F 0.43633(14) 0.85445(14) 0.95725(7) 0.0371(3) Uani 1 1 d D U . . . O1_6 O 0.53346(13) 0.79542(12) 0.69266(7) 0.0212(3) Uani 1 1 d D U . . . C1_6 C 0.54569(17) 0.76295(17) 0.62396(11) 0.0209(4) Uani 1 1 d D U . . . C2_6 C 0.4950(2) 0.8441(2) 0.57948(12) 0.0282(4) Uani 1 1 d D U . . . F1_6 F 0.37798(13) 0.83314(15) 0.56304(9) 0.0423(4) Uani 1 1 d D U . . . F2_6 F 0.52616(14) 0.83111(15) 0.51705(8) 0.0394(4) Uani 1 1 d D U . . . F3_6 F 0.52918(15) 0.94362(13) 0.61739(9) 0.0396(3) Uani 1 1 d D U . . . C3_6 C 0.67759(19) 0.75878(19) 0.62489(12) 0.0264(4) Uani 1 1 d D U . . . F4_6 F 0.73280(13) 0.71998(13) 0.67983(8) 0.0349(3) Uani 1 1 d D U . . . F5_6 F 0.73071(12) 0.85768(13) 0.63519(8) 0.0345(3) Uani 1 1 d D U . . . F6_6 F 0.69272(13) 0.69997(13) 0.56336(8) 0.0348(3) Uani 1 1 d D U . . . C4_6 C 0.4787(2) 0.6510(2) 0.58839(13) 0.0330(5) Uani 1 1 d D U . . . F7_6 F 0.53812(18) 0.57841(12) 0.61699(10) 0.0470(4) Uani 1 1 d D U . . . F8_6 F 0.46460(16) 0.62393(14) 0.51654(8) 0.0448(4) Uani 1 1 d D U . . . F9_6 F 0.37376(15) 0.64619(15) 0.60091(10) 0.0502(5) Uani 1 1 d D U . . . F1_7 F 0.0879(8) 0.3087(8) 0.4664(6) 0.0343(16) Uani 0.5 1 d D U P A -1 F2_7 F -0.1259(3) 0.3477(2) 0.39840(15) 0.0333(6) Uani 0.5 1 d D U P A -1 F3_7 F -0.2017(2) 0.5425(2) 0.43890(17) 0.0352(7) Uani 0.5 1 d D U P A -1 F4_7 F -0.0603(8) 0.6980(8) 0.5417(6) 0.0372(19) Uani 0.5 1 d D U P A -1 C1_7 C 0.0528(7) 0.4061(7) 0.4887(5) 0.0240(14) Uani 0.5 1 d D U P A -1 C2_7 C -0.0562(7) 0.4243(7) 0.4527(4) 0.0249(14) Uani 0.5 1 d D U P A -1 C3_7 C -0.0959(7) 0.5231(7) 0.4727(5) 0.0249(14) Uani 0.5 1 d D U P A -1 C4_7 C -0.0220(7) 0.6001(7) 0.5265(4) 0.0233(14) Uani 0.5 1 d D U P A -1 C5_7 C 0.0864(7) 0.5821(7) 0.5620(4) 0.0240(14) Uani 0.5 1 d D U P A -1 H5_7 H 0.135044 0.636624 0.599843 0.029 Uiso 0.5 1 calc R U P A -1 C6_7 C 0.1254(7) 0.4823(7) 0.5420(5) 0.0250(15) Uani 0.5 1 d D U P A -1 H6_7 H 0.201438 0.468291 0.565463 0.030 Uiso 0.5 1 calc R U P A -1 O1_8 O 0.7247(2) 0.8776(2) 0.8213(2) 0.0246(5) Uani 0.880(4) 1 d D U P B 1 C1_8 C 0.7910(2) 0.9719(2) 0.85433(15) 0.0223(4) Uani 0.880(4) 1 d D U P B 1 C2_8 C 0.7757(3) 1.0481(2) 0.80243(17) 0.0317(5) Uani 0.880(4) 1 d D U P B 1 F1_8 F 0.8392(2) 1.01718(19) 0.75237(11) 0.0475(6) Uani 0.880(4) 1 d D U P B 1 F2_8 F 0.8161(3) 1.1488(2) 0.8364(2) 0.0429(7) Uani 0.880(4) 1 d D U P B 1 F3_8 F 0.6664(2) 1.0431(2) 0.76516(14) 0.0463(6) Uani 0.880(4) 1 d D U P B 1 C3_8 C 0.7593(3) 1.0246(3) 0.92554(18) 0.0453(8) Uani 0.880(4) 1 d D U P B 1 F4_8 F 0.7392(3) 0.9579(3) 0.96203(13) 0.0747(10) Uani 0.880(4) 1 d D U P B 1 F5_8 F 0.6562(2) 1.0698(2) 0.90597(16) 0.0658(8) Uani 0.880(4) 1 d D U P B 1 F6_8 F 0.8405(2) 1.1020(2) 0.96762(14) 0.0478(7) Uani 0.880(4) 1 d D U P B 1 C4_8 C 0.9214(3) 0.9482(2) 0.87284(19) 0.0366(6) Uani 0.880(4) 1 d D U P B 1 F7_8 F 0.9443(2) 0.90834(18) 0.93272(14) 0.0607(8) Uani 0.880(4) 1 d D U P B 1 F8_8 F 0.9959(2) 1.0352(2) 0.88890(18) 0.0423(6) Uani 0.880(4) 1 d D U P B 1 F9_8 F 0.9441(2) 0.8769(2) 0.82155(17) 0.0572(7) Uani 0.880(4) 1 d D U P B 1 O1_9 O 0.703(2) 0.8847(19) 0.8214(17) 0.030(3) Uani 0.120(4) 1 d D U P B 2 C1_9 C 0.7804(14) 0.9715(15) 0.8555(8) 0.0318(16) Uani 0.120(4) 1 d D U P B 2 C2_9 C 0.9016(14) 0.9484(14) 0.8976(9) 0.040(2) Uani 0.120(4) 1 d D U P B 2 F1_9 F 0.8814(15) 0.9290(12) 0.9607(7) 0.047(3) Uani 0.120(4) 1 d D U P B 2 F2_9 F 0.980(2) 1.0332(18) 0.9061(13) 0.048(4) Uani 0.120(4) 1 d D U P B 2 F3_9 F 0.9398(15) 0.8677(14) 0.8572(10) 0.050(3) Uani 0.120(4) 1 d D U P B 2 C3_9 C 0.8108(15) 1.0329(15) 0.8005(9) 0.042(2) Uani 0.120(4) 1 d D U P B 2 F4_9 F 0.7098(16) 1.0383(18) 0.7541(11) 0.054(4) Uani 0.120(4) 1 d D U P B 2 F5_9 F 0.8972(14) 0.9764(13) 0.7770(9) 0.055(3) Uani 0.120(4) 1 d D U P B 2 F6_9 F 0.843(2) 1.1360(15) 0.8339(17) 0.046(4) Uani 0.120(4) 1 d D U P B 2 C4_9 C 0.7246(15) 1.0447(13) 0.9104(9) 0.038(2) Uani 0.120(4) 1 d D U P B 2 F7_9 F 0.6552(16) 1.0995(14) 0.8673(10) 0.061(4) Uani 0.120(4) 1 d D U P B 2 F8_9 F 0.8032(17) 1.1181(17) 0.9596(11) 0.0478(7) Uani 0.120(4) 1 d D U P B 2 F9_9 F 0.6839(12) 0.9847(11) 0.9479(8) 0.030(2) Uani 0.120(4) 1 d D U P B 2 O1_10 O 0.7818(3) 0.5405(3) 0.7645(2) 0.0217(5) Uani 0.921(2) 1 d D U P C 1 C1_10 C 0.8595(2) 0.4843(2) 0.73565(14) 0.0206(4) Uani 0.921(2) 1 d D U P C 1 C2_10 C 0.9741(2) 0.5597(2) 0.75120(15) 0.0274(5) Uani 0.921(2) 1 d D U P C 1 F1_10 F 1.03352(14) 0.57600(15) 0.82055(9) 0.0383(4) Uani 0.921(2) 1 d D U P C 1 F2_10 F 1.0449(2) 0.5197(2) 0.70967(13) 0.0384(5) Uani 0.921(2) 1 d D U P C 1 F3_10 F 0.94955(14) 0.65318(13) 0.73816(11) 0.0369(4) Uani 0.921(2) 1 d D U P C 1 C3_10 C 0.8084(2) 0.4423(2) 0.65181(15) 0.0272(5) Uani 0.921(2) 1 d D U P C 1 F4_10 F 0.69740(14) 0.40279(15) 0.63633(9) 0.0354(4) Uani 0.921(2) 1 d D U P C 1 F5_10 F 0.81246(17) 0.52011(15) 0.61740(9) 0.0366(4) Uani 0.921(2) 1 d D U P C 1 F6_10 F 0.8672(2) 0.36490(18) 0.62279(14) 0.0386(5) Uani 0.921(2) 1 d D U P C 1 C4_10 C 0.8879(3) 0.3874(2) 0.76996(15) 0.0286(5) Uani 0.921(2) 1 d D U P C 1 F7_10 F 0.80280(17) 0.30735(13) 0.74048(10) 0.0408(4) Uani 0.921(2) 1 d D U P C 1 F8_10 F 0.98834(19) 0.34977(18) 0.75915(12) 0.0421(5) Uani 0.921(2) 1 d D U P C 1 F9_10 F 0.89845(18) 0.41316(14) 0.84077(9) 0.0364(4) Uani 0.921(2) 1 d D U P C 1 O1_13 O 0.777(3) 0.542(3) 0.760(2) 0.026(4) Uani 0.079(2) 1 d D U P C 2 C1_13 C 0.8558(17) 0.4858(14) 0.7315(10) 0.025(2) Uani 0.079(2) 1 d D U P C 2 C2_13 C 0.8960(17) 0.4002(15) 0.7745(10) 0.032(3) Uani 0.079(2) 1 d D U P C 2 F1_13 F 0.9728(17) 0.4453(14) 0.8381(9) 0.038(3) Uani 0.079(2) 1 d D U P C 2 F2_13 F 0.946(2) 0.3234(17) 0.7375(12) 0.034(3) Uani 0.079(2) 1 d D U P C 2 F3_13 F 0.8044(14) 0.3542(14) 0.7895(11) 0.035(3) Uani 0.079(2) 1 d D U P C 2 C3_13 C 0.7977(17) 0.4289(15) 0.6506(10) 0.029(3) Uani 0.079(2) 1 d D U P C 2 F4_13 F 0.7355(17) 0.4928(14) 0.6148(9) 0.033(3) Uani 0.079(2) 1 d D U P C 2 F5_13 F 0.7242(16) 0.3451(14) 0.6465(11) 0.039(3) Uani 0.079(2) 1 d D U P C 2 F6_13 F 0.882(2) 0.395(2) 0.6184(17) 0.034(4) Uani 0.079(2) 1 d D U P C 2 C4_13 C 0.9644(18) 0.5619(14) 0.7358(10) 0.033(3) Uani 0.079(2) 1 d D U P C 2 F7_13 F 0.9413(16) 0.6188(14) 0.6856(10) 0.035(3) Uani 0.079(2) 1 d D U P C 2 F8_13 F 1.053(2) 0.503(2) 0.7275(15) 0.035(4) Uani 0.079(2) 1 d D U P C 2 F9_13 F 1.0010(16) 0.6296(15) 0.8009(9) 0.036(3) Uani 0.079(2) 1 d D U P C 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.01503(7) 0.01659(7) 0.01441(7) 0.00140(5) 0.00462(5) 0.00059(5) Ru2 0.01304(9) 0.01480(9) 0.01404(9) 0.00165(7) 0.00440(7) -0.00001(6) Al1 0.0154(2) 0.0162(2) 0.0165(2) 0.0037(2) 0.0039(2) 0.00063(19) Al2 0.0163(2) 0.0174(3) 0.0150(2) 0.0033(2) 0.0054(2) 0.0026(2) F1 0.0220(6) 0.0180(5) 0.0209(5) 0.0057(4) 0.0068(4) 0.0048(4) C3 0.0212(9) 0.0212(9) 0.0190(8) 0.0017(7) 0.0081(7) 0.0011(7) O3 0.0213(7) 0.0329(8) 0.0321(8) 0.0041(7) 0.0102(6) 0.0048(6) O4 0.0296(8) 0.0246(8) 0.0346(9) 0.0096(7) 0.0090(7) 0.0007(6) O5 0.0205(7) 0.0274(8) 0.0289(8) 0.0076(6) 0.0069(6) 0.0045(6) O6 0.0236(7) 0.0250(8) 0.0366(9) 0.0083(7) 0.0070(6) 0.0064(6) O7 0.0227(7) 0.0330(8) 0.0263(7) 0.0041(6) 0.0091(6) -0.0059(6) C1 0.0227(9) 0.0218(9) 0.0200(9) 0.0037(7) 0.0066(7) 0.0031(7) C2 0.0158(8) 0.0218(9) 0.0191(8) 0.0012(7) 0.0046(7) 0.0014(6) O1 0.0351(9) 0.0309(8) 0.0188(7) 0.0019(6) 0.0058(6) 0.0042(7) O2 0.0235(7) 0.0225(7) 0.0302(8) 0.0047(6) 0.0086(6) 0.0006(6) C4 0.0198(9) 0.0241(9) 0.0197(8) 0.0037(7) 0.0065(7) 0.0017(7) C5 0.0204(9) 0.0193(8) 0.0175(8) 0.0031(7) 0.0037(7) 0.0005(7) C6 0.0159(8) 0.0204(8) 0.0194(8) 0.0032(7) 0.0047(6) -0.0018(6) C7 0.0198(8) 0.0207(9) 0.0167(8) 0.0020(7) 0.0057(7) 0.0004(7) O1_1 0.0299(8) 0.0312(8) 0.0224(7) 0.0076(6) -0.0004(6) -0.0147(6) C1_1 0.0217(9) 0.0212(9) 0.0230(9) 0.0043(7) 0.0041(7) -0.0035(7) C2_1 0.0243(10) 0.0253(10) 0.0320(11) -0.0002(8) 0.0082(8) -0.0027(8) F1_1 0.0368(8) 0.0462(9) 0.0484(10) -0.0074(8) 0.0143(7) 0.0115(7) F2_1 0.0312(7) 0.0270(7) 0.0386(8) -0.0057(6) 0.0059(6) -0.0103(6) F3_1 0.0407(8) 0.0422(8) 0.0228(6) 0.0026(6) 0.0045(6) -0.0120(7) C3_1 0.0291(11) 0.0283(11) 0.0293(11) -0.0011(9) 0.0057(9) 0.0014(8) F4_1 0.0493(10) 0.0399(9) 0.0365(8) -0.0105(7) 0.0046(7) 0.0122(7) F5_1 0.0366(8) 0.0329(8) 0.0380(8) 0.0026(6) -0.0035(6) 0.0086(6) F6_1 0.0288(8) 0.0578(10) 0.0434(9) 0.0068(8) 0.0155(7) -0.0052(7) C4_1 0.0334(12) 0.0257(11) 0.0360(12) 0.0110(9) 0.0048(10) -0.0022(9) F7_1 0.0440(9) 0.0443(9) 0.0291(7) 0.0156(6) 0.0076(6) -0.0078(7) F8_1 0.0685(12) 0.0257(8) 0.0584(11) 0.0190(7) 0.0007(9) -0.0119(8) F9_1 0.0372(9) 0.0513(10) 0.0520(10) 0.0173(8) 0.0038(7) 0.0163(8) O1_3 0.0236(7) 0.0248(7) 0.0164(6) 0.0058(5) 0.0028(5) -0.0008(5) C1_3 0.0185(8) 0.0298(10) 0.0179(8) 0.0066(7) 0.0032(7) 0.0015(7) C2_3 0.0226(9) 0.0331(11) 0.0222(9) 0.0008(8) 0.0061(8) -0.0020(8) F1_3 0.0196(6) 0.0507(9) 0.0477(9) 0.0067(7) 0.0082(6) 0.0073(6) F2_3 0.0320(8) 0.0525(10) 0.0279(7) -0.0106(7) 0.0063(6) -0.0110(7) F3_3 0.0424(8) 0.0322(7) 0.0301(7) 0.0053(6) 0.0130(6) -0.0090(6) C3_3 0.0228(10) 0.0475(14) 0.0258(10) 0.0003(10) 0.0066(8) 0.0040(9) F4_3 0.0203(7) 0.0684(12) 0.0457(9) -0.0029(8) 0.0092(6) 0.0043(7) F5_3 0.0482(10) 0.0377(9) 0.0495(10) 0.0031(7) 0.0108(8) 0.0178(7) F6_3 0.0386(9) 0.0773(13) 0.0271(7) -0.0116(8) 0.0146(7) -0.0004(8) C4_3 0.0325(12) 0.0518(15) 0.0306(12) 0.0241(11) 0.0012(9) -0.0002(11) F7_3 0.0465(10) 0.0770(13) 0.0400(9) 0.0316(9) 0.0117(8) -0.0122(9) F8_3 0.0491(10) 0.0876(15) 0.0311(8) 0.0313(9) -0.0108(7) -0.0055(10) F9_3 0.0497(10) 0.0444(10) 0.0608(11) 0.0310(9) 0.0047(9) 0.0122(8) O1_5 0.0208(7) 0.0452(10) 0.0223(7) 0.0093(7) 0.0099(6) 0.0128(7) C1_5 0.0184(8) 0.0220(9) 0.0204(8) 0.0038(7) 0.0072(7) 0.0056(7) C2_5 0.0395(13) 0.0250(11) 0.0335(12) 0.0010(9) -0.0029(10) 0.0087(9) F1_5 0.0596(11) 0.0311(8) 0.0382(9) -0.0075(7) -0.0041(8) 0.0094(7) F2_5 0.0527(11) 0.0472(10) 0.0600(11) -0.0045(9) -0.0086(9) 0.0356(9) F3_5 0.0706(12) 0.0321(8) 0.0430(9) 0.0172(7) -0.0075(8) -0.0148(8) C3_5 0.0255(10) 0.0256(10) 0.0233(9) 0.0050(8) 0.0071(8) 0.0005(8) F4_5 0.0576(10) 0.0216(6) 0.0290(7) 0.0020(5) 0.0104(7) 0.0049(6) F5_5 0.0298(7) 0.0294(7) 0.0229(6) 0.0085(5) 0.0011(5) 0.0015(5) F6_5 0.0245(7) 0.0613(11) 0.0369(8) 0.0047(7) 0.0083(6) -0.0105(7) C4_5 0.0327(12) 0.0413(13) 0.0242(10) 0.0054(9) 0.0144(9) 0.0043(10) F7_5 0.0822(14) 0.0418(9) 0.0352(8) 0.0166(7) 0.0190(9) -0.0068(9) F8_5 0.0312(8) 0.0887(14) 0.0374(9) 0.0010(9) 0.0227(7) 0.0071(9) F9_5 0.0385(8) 0.0539(10) 0.0198(6) 0.0067(6) 0.0106(6) 0.0096(7) O1_6 0.0207(7) 0.0285(7) 0.0148(6) 0.0040(5) 0.0063(5) 0.0037(5) C1_6 0.0176(8) 0.0277(10) 0.0176(8) 0.0051(7) 0.0053(7) 0.0024(7) C2_6 0.0251(10) 0.0405(12) 0.0220(9) 0.0119(9) 0.0065(8) 0.0088(9) F1_6 0.0228(7) 0.0723(12) 0.0340(8) 0.0175(8) 0.0050(6) 0.0172(7) F2_6 0.0400(8) 0.0636(11) 0.0268(7) 0.0244(7) 0.0162(6) 0.0211(8) F3_6 0.0470(9) 0.0341(8) 0.0415(8) 0.0158(7) 0.0104(7) 0.0128(7) C3_6 0.0227(9) 0.0377(12) 0.0225(9) 0.0099(8) 0.0097(8) 0.0074(8) F4_6 0.0275(7) 0.0526(9) 0.0290(7) 0.0158(6) 0.0074(6) 0.0181(6) F5_6 0.0240(7) 0.0443(8) 0.0363(8) 0.0117(6) 0.0092(6) -0.0036(6) F6_6 0.0345(7) 0.0480(9) 0.0287(7) 0.0096(6) 0.0183(6) 0.0171(7) C4_6 0.0364(12) 0.0351(12) 0.0242(10) 0.0001(9) 0.0096(9) -0.0047(9) F7_6 0.0714(12) 0.0257(7) 0.0429(9) 0.0051(7) 0.0164(8) 0.0000(7) F8_6 0.0499(10) 0.0529(10) 0.0220(7) -0.0086(7) 0.0085(6) -0.0038(8) F9_6 0.0386(9) 0.0587(11) 0.0441(9) -0.0090(8) 0.0178(7) -0.0218(8) F1_7 0.024(4) 0.025(2) 0.057(3) 0.010(2) 0.017(3) 0.003(2) F2_7 0.0332(15) 0.0285(14) 0.0287(14) 0.0010(11) -0.0029(11) -0.0074(11) F3_7 0.0202(13) 0.0342(15) 0.0503(18) 0.0193(13) -0.0006(12) -0.0004(11) F4_7 0.029(4) 0.0232(19) 0.060(4) -0.0021(19) 0.023(3) -0.001(2) C1_7 0.026(3) 0.021(2) 0.026(4) 0.007(2) 0.006(2) 0.004(2) C2_7 0.028(4) 0.026(2) 0.016(3) 0.004(2) 0.000(2) -0.003(2) C3_7 0.019(3) 0.030(3) 0.026(4) 0.012(2) 0.001(2) 0.001(2) C4_7 0.030(4) 0.019(2) 0.021(3) 0.004(2) 0.009(3) -0.001(3) C5_7 0.027(4) 0.025(2) 0.017(3) 0.005(2) 0.003(2) -0.003(2) C6_7 0.025(4) 0.025(2) 0.022(3) 0.009(2) 0.000(3) -0.002(2) O1_8 0.0193(11) 0.0263(10) 0.0235(9) 0.0004(7) 0.0035(9) -0.0058(8) C1_8 0.0213(10) 0.0234(10) 0.0213(9) 0.0027(8) 0.0073(8) -0.0046(8) C2_8 0.0270(13) 0.0321(12) 0.0357(13) 0.0121(10) 0.0041(10) 0.0008(10) F1_8 0.0544(13) 0.0631(13) 0.0336(10) 0.0192(9) 0.0220(9) -0.0007(10) F2_8 0.0460(16) 0.0246(9) 0.0567(13) 0.0151(9) 0.0063(12) 0.0009(8) F3_8 0.0360(11) 0.0428(11) 0.0529(13) 0.0151(9) -0.0063(10) 0.0092(10) C3_8 0.0486(17) 0.0475(17) 0.0328(14) -0.0124(11) 0.0219(13) -0.0212(13) F4_8 0.113(3) 0.0759(19) 0.0302(11) -0.0028(11) 0.0344(15) -0.0462(17) F5_8 0.0470(12) 0.0658(16) 0.0743(17) -0.0271(13) 0.0383(12) -0.0075(11) F6_8 0.0517(15) 0.0457(12) 0.0338(10) -0.0136(8) 0.0137(11) -0.0208(11) C4_8 0.0250(12) 0.0313(13) 0.0483(16) 0.0088(12) 0.0017(11) -0.0028(10) F7_8 0.0594(15) 0.0447(12) 0.0604(14) 0.0263(11) -0.0266(12) -0.0152(11) F8_8 0.0232(10) 0.0400(10) 0.0606(18) 0.0152(10) 0.0042(9) -0.0084(8) F9_8 0.0291(10) 0.0524(13) 0.0770(17) -0.0069(13) 0.0074(12) 0.0131(9) O1_9 0.030(5) 0.028(4) 0.027(5) 0.002(4) 0.003(4) -0.003(4) C1_9 0.029(3) 0.032(3) 0.030(3) 0.002(2) 0.006(2) -0.005(3) C2_9 0.032(3) 0.037(4) 0.043(4) 0.007(3) -0.002(3) -0.008(3) F1_9 0.052(7) 0.038(6) 0.039(5) 0.011(4) -0.011(4) -0.012(5) F2_9 0.038(6) 0.053(5) 0.043(7) 0.016(5) -0.009(6) -0.019(5) F3_9 0.032(6) 0.052(5) 0.060(7) 0.008(5) 0.008(6) 0.003(4) C3_9 0.044(4) 0.043(4) 0.038(4) 0.009(3) 0.008(3) -0.009(3) F4_9 0.056(6) 0.054(7) 0.046(6) 0.019(5) -0.001(5) -0.011(6) F5_9 0.056(6) 0.056(6) 0.053(6) 0.002(5) 0.027(5) -0.013(5) F6_9 0.042(8) 0.037(4) 0.057(7) 0.015(5) 0.010(6) -0.004(5) C4_9 0.039(4) 0.034(4) 0.034(3) -0.004(3) 0.009(3) -0.008(3) F7_9 0.064(7) 0.049(7) 0.065(7) 0.006(5) 0.008(5) 0.021(5) F8_9 0.0517(15) 0.0457(12) 0.0338(10) -0.0136(8) 0.0137(11) -0.0208(11) F9_9 0.028(5) 0.026(4) 0.033(5) -0.010(4) 0.016(4) 0.000(3) O1_10 0.0206(9) 0.0226(10) 0.0246(10) 0.0051(8) 0.0109(8) 0.0066(7) C1_10 0.0188(9) 0.0222(10) 0.0221(9) 0.0038(8) 0.0084(8) 0.0064(7) C2_10 0.0196(10) 0.0298(11) 0.0345(12) 0.0071(10) 0.0100(9) 0.0066(8) F1_10 0.0252(8) 0.0454(10) 0.0373(9) 0.0042(7) 0.0000(6) 0.0022(7) F2_10 0.0247(8) 0.0490(12) 0.0495(13) 0.0131(9) 0.0224(9) 0.0108(8) F3_10 0.0258(7) 0.0296(8) 0.0595(12) 0.0175(8) 0.0125(7) 0.0018(6) C3_10 0.0279(11) 0.0319(12) 0.0228(10) 0.0032(9) 0.0105(9) 0.0075(9) F4_10 0.0283(8) 0.0449(10) 0.0270(7) -0.0015(7) 0.0058(6) -0.0018(7) F5_10 0.0427(10) 0.0474(10) 0.0268(7) 0.0156(7) 0.0152(7) 0.0104(8) F6_10 0.0410(11) 0.0429(13) 0.0305(9) -0.0031(9) 0.0154(8) 0.0145(9) C4_10 0.0365(13) 0.0251(11) 0.0287(11) 0.0068(9) 0.0146(10) 0.0125(9) F7_10 0.0558(11) 0.0226(7) 0.0459(10) 0.0082(7) 0.0167(8) 0.0025(7) F8_10 0.0475(12) 0.0437(12) 0.0454(12) 0.0161(9) 0.0217(9) 0.0309(10) F9_10 0.0524(11) 0.0362(9) 0.0276(7) 0.0137(6) 0.0151(7) 0.0198(8) O1_13 0.027(7) 0.026(9) 0.027(8) 0.004(7) 0.014(7) 0.011(6) C1_13 0.024(4) 0.025(4) 0.028(4) 0.004(3) 0.013(3) 0.009(3) C2_13 0.036(5) 0.030(5) 0.035(5) 0.009(4) 0.014(4) 0.014(4) F1_13 0.043(6) 0.035(6) 0.036(5) 0.009(4) 0.009(5) 0.019(5) F2_13 0.041(7) 0.031(6) 0.037(7) 0.012(5) 0.017(6) 0.018(6) F3_13 0.039(5) 0.031(6) 0.045(7) 0.017(5) 0.019(5) 0.018(4) C3_13 0.031(5) 0.029(5) 0.027(4) 0.001(4) 0.013(4) 0.011(4) F4_13 0.035(6) 0.035(6) 0.029(5) 0.003(5) 0.009(5) 0.013(5) F5_13 0.035(6) 0.032(5) 0.044(7) 0.001(5) 0.008(5) 0.002(5) F6_13 0.040(6) 0.031(8) 0.034(6) -0.001(6) 0.020(5) 0.015(5) C4_13 0.027(5) 0.036(5) 0.037(5) 0.008(4) 0.014(4) 0.003(4) F7_13 0.031(6) 0.037(6) 0.043(5) 0.012(5) 0.017(5) 0.003(5) F8_13 0.026(5) 0.042(7) 0.041(8) 0.010(6) 0.016(6) 0.005(5) F9_13 0.026(6) 0.039(6) 0.041(5) 0.003(5) 0.010(5) 0.001(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 C2 1.972(2) . ? Ru1 C5 1.983(2) . ? Ru1 C3 1.983(2) . ? Ru1 C4 1.992(2) . ? Ru1 C1 1.994(2) . ? Ru1 Ru2 2.8907(7) . ? Ru2 C7 1.959(2) 2_556 ? Ru2 C7 1.959(2) . ? Ru2 C6 1.962(2) . ? Ru2 C6 1.962(2) 2_556 ? Al1 O1_3 1.6996(16) . ? Al1 O1_1 1.7024(17) . ? Al1 O1_10 1.709(3) . ? Al1 O1_13 1.72(3) . ? Al1 F1 1.7683(14) . ? Al2 O1_9 1.567(19) . ? Al2 O1_5 1.7013(16) . ? Al2 O1_8 1.716(3) . ? Al2 O1_6 1.7160(16) . ? Al2 F1 1.7665(13) . ? C3 O3 1.122(3) . ? O4 C4 1.115(3) . ? O5 C5 1.120(2) . ? O6 C6 1.127(3) . ? O7 C7 1.127(2) . ? C1 O1 1.114(3) . ? C2 O2 1.124(3) . ? O1_1 C1_1 1.351(2) . ? C1_1 C2_1 1.555(3) . ? C1_1 C4_1 1.556(3) . ? C1_1 C3_1 1.557(3) . ? C2_1 F3_1 1.316(3) . ? C2_1 F1_1 1.328(3) . ? C2_1 F2_1 1.348(3) . ? C3_1 F4_1 1.318(3) . ? C3_1 F5_1 1.332(3) . ? C3_1 F6_1 1.343(3) . ? C4_1 F7_1 1.323(3) . ? C4_1 F9_1 1.332(3) . ? C4_1 F8_1 1.339(3) . ? O1_3 C1_3 1.362(2) . ? C1_3 C4_3 1.549(3) . ? C1_3 C3_3 1.552(3) . ? C1_3 C2_3 1.554(3) . ? C2_3 F2_3 1.329(3) . ? C2_3 F3_3 1.330(3) . ? C2_3 F1_3 1.331(3) . ? C3_3 F5_3 1.331(3) . ? C3_3 F6_3 1.331(3) . ? C3_3 F4_3 1.332(3) . ? C4_3 F9_3 1.324(4) . ? C4_3 F7_3 1.329(3) . ? C4_3 F8_3 1.336(3) . ? O1_5 C1_5 1.351(2) . ? C1_5 C2_5 1.549(3) . ? C1_5 C3_5 1.553(3) . ? C1_5 C4_5 1.556(3) . ? C2_5 F1_5 1.321(3) . ? C2_5 F3_5 1.333(3) . ? C2_5 F2_5 1.345(3) . ? C3_5 F6_5 1.325(3) . ? C3_5 F4_5 1.329(3) . ? C3_5 F5_5 1.347(2) . ? C4_5 F7_5 1.324(3) . ? C4_5 F9_5 1.326(3) . ? C4_5 F8_5 1.327(3) . ? O1_6 C1_6 1.357(2) . ? C1_6 C4_6 1.546(3) . ? C1_6 C2_6 1.556(3) . ? C1_6 C3_6 1.558(3) . ? C2_6 F3_6 1.326(3) . ? C2_6 F2_6 1.332(3) . ? C2_6 F1_6 1.336(3) . ? C3_6 F4_6 1.324(3) . ? C3_6 F6_6 1.328(3) . ? C3_6 F5_6 1.350(3) . ? C4_6 F9_6 1.322(3) . ? C4_6 F8_6 1.333(3) . ? C4_6 F7_6 1.338(3) . ? F1_7 C1_7 1.360(9) . ? F2_7 C2_7 1.351(7) . ? F3_7 C3_7 1.329(7) . ? F4_7 C4_7 1.361(9) . ? C1_7 C6_7 1.353(8) . ? C1_7 C2_7 1.369(7) . ? C2_7 C3_7 1.390(9) . ? C3_7 C4_7 1.369(8) . ? C4_7 C5_7 1.359(8) . ? C5_7 C6_7 1.398(9) . ? C5_7 H5_7 0.9500 . ? C6_7 H6_7 0.9500 . ? O1_8 C1_8 1.356(3) . ? C1_8 C3_8 1.546(4) . ? C1_8 C2_8 1.547(4) . ? C1_8 C4_8 1.558(4) . ? C2_8 F3_8 1.311(3) . ? C2_8 F2_8 1.331(4) . ? C2_8 F1_8 1.373(4) . ? C3_8 F4_8 1.279(4) . ? C3_8 F6_8 1.329(3) . ? C3_8 F5_8 1.384(5) . ? C4_8 F9_8 1.292(4) . ? C4_8 F8_8 1.327(3) . ? C4_8 F7_8 1.350(4) . ? O1_9 C1_9 1.350(14) . ? C1_9 C2_9 1.548(12) . ? C1_9 C4_9 1.559(12) . ? C1_9 C3_9 1.561(12) . ? C2_9 F3_9 1.331(12) . ? C2_9 F2_9 1.353(13) . ? C2_9 F1_9 1.379(12) . ? C3_9 F4_9 1.327(13) . ? C3_9 F6_9 1.343(13) . ? C3_9 F5_9 1.392(12) . ? C4_9 F9_9 1.323(12) . ? C4_9 F8_9 1.332(13) . ? C4_9 F7_9 1.366(12) . ? O1_10 C1_10 1.350(3) . ? C1_10 C2_10 1.558(3) . ? C1_10 C4_10 1.558(3) . ? C1_10 C3_10 1.560(3) . ? C2_10 F3_10 1.320(3) . ? C2_10 F1_10 1.329(3) . ? C2_10 F2_10 1.344(3) . ? C3_10 F4_10 1.323(3) . ? C3_10 F5_10 1.331(3) . ? C3_10 F6_10 1.347(3) . ? C4_10 F9_10 1.319(3) . ? C4_10 F7_10 1.333(3) . ? C4_10 F8_10 1.350(3) . ? O1_13 C1_13 1.354(14) . ? C1_13 C4_13 1.554(13) . ? C1_13 C2_13 1.555(13) . ? C1_13 C3_13 1.556(13) . ? C2_13 F3_13 1.334(13) . ? C2_13 F1_13 1.338(13) . ? C2_13 F2_13 1.341(13) . ? C3_13 F4_13 1.332(13) . ? C3_13 F5_13 1.332(13) . ? C3_13 F6_13 1.339(13) . ? C4_13 F9_13 1.333(13) . ? C4_13 F7_13 1.335(13) . ? C4_13 F8_13 1.341(13) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 Ru1 C5 90.84(8) . . ? C2 Ru1 C3 88.96(8) . . ? C5 Ru1 C3 169.70(8) . . ? C2 Ru1 C4 173.43(8) . . ? C5 Ru1 C4 88.95(8) . . ? C3 Ru1 C4 90.07(9) . . ? C2 Ru1 C1 93.18(8) . . ? C5 Ru1 C1 94.84(8) . . ? C3 Ru1 C1 95.45(8) . . ? C4 Ru1 C1 93.37(8) . . ? C2 Ru1 Ru2 84.70(6) . . ? C5 Ru1 Ru2 84.67(6) . . ? C3 Ru1 Ru2 85.06(6) . . ? C4 Ru1 Ru2 88.75(6) . . ? C1 Ru1 Ru2 177.82(6) . . ? C7 Ru2 C7 180.00(10) 2_556 . ? C7 Ru2 C6 90.44(8) 2_556 . ? C7 Ru2 C6 89.56(8) . . ? C7 Ru2 C6 89.56(8) 2_556 2_556 ? C7 Ru2 C6 90.44(8) . 2_556 ? C6 Ru2 C6 180.0 . 2_556 ? C7 Ru2 Ru1 90.47(6) 2_556 2_556 ? C7 Ru2 Ru1 89.53(6) . 2_556 ? C6 Ru2 Ru1 90.19(6) . 2_556 ? C6 Ru2 Ru1 89.81(6) 2_556 2_556 ? C7 Ru2 Ru1 89.53(6) 2_556 . ? C7 Ru2 Ru1 90.47(6) . . ? C6 Ru2 Ru1 89.80(6) . . ? C6 Ru2 Ru1 90.20(6) 2_556 . ? Ru1 Ru2 Ru1 180.0 2_556 . ? O1_3 Al1 O1_1 109.98(8) . . ? O1_3 Al1 O1_10 118.17(14) . . ? O1_1 Al1 O1_10 112.62(15) . . ? O1_3 Al1 O1_13 121.5(15) . . ? O1_1 Al1 O1_13 110.8(15) . . ? O1_3 Al1 F1 109.67(7) . . ? O1_1 Al1 F1 103.85(8) . . ? O1_10 Al1 F1 101.20(13) . . ? O1_13 Al1 F1 99.1(14) . . ? O1_9 Al2 O1_5 107.8(11) . . ? O1_5 Al2 O1_8 114.49(14) . . ? O1_9 Al2 O1_6 115.7(13) . . ? O1_5 Al2 O1_6 111.13(8) . . ? O1_8 Al2 O1_6 115.23(16) . . ? O1_9 Al2 F1 109.1(11) . . ? O1_5 Al2 F1 105.01(8) . . ? O1_8 Al2 F1 102.19(13) . . ? O1_6 Al2 F1 107.59(7) . . ? Al2 F1 Al1 176.30(8) . . ? O3 C3 Ru1 178.08(18) . . ? O1 C1 Ru1 178.7(2) . . ? O2 C2 Ru1 178.80(18) . . ? O4 C4 Ru1 178.9(2) . . ? O5 C5 Ru1 178.24(19) . . ? O6 C6 Ru2 178.42(18) . . ? O7 C7 Ru2 178.07(19) . . ? C1_1 O1_1 Al1 148.81(15) . . ? O1_1 C1_1 C2_1 107.14(17) . . ? O1_1 C1_1 C4_1 112.27(18) . . ? C2_1 C1_1 C4_1 110.03(18) . . ? O1_1 C1_1 C3_1 109.34(18) . . ? C2_1 C1_1 C3_1 109.56(17) . . ? C4_1 C1_1 C3_1 108.47(18) . . ? F3_1 C2_1 F1_1 108.1(2) . . ? F3_1 C2_1 F2_1 106.92(19) . . ? F1_1 C2_1 F2_1 107.16(19) . . ? F3_1 C2_1 C1_1 111.66(18) . . ? F1_1 C2_1 C1_1 110.87(19) . . ? F2_1 C2_1 C1_1 111.89(18) . . ? F4_1 C3_1 F5_1 108.1(2) . . ? F4_1 C3_1 F6_1 108.3(2) . . ? F5_1 C3_1 F6_1 107.3(2) . . ? F4_1 C3_1 C1_1 110.52(19) . . ? F5_1 C3_1 C1_1 110.44(19) . . ? F6_1 C3_1 C1_1 112.01(19) . . ? F7_1 C4_1 F9_1 107.7(2) . . ? F7_1 C4_1 F8_1 108.0(2) . . ? F9_1 C4_1 F8_1 107.9(2) . . ? F7_1 C4_1 C1_1 111.7(2) . . ? F9_1 C4_1 C1_1 110.0(2) . . ? F8_1 C4_1 C1_1 111.3(2) . . ? C1_3 O1_3 Al1 146.80(14) . . ? O1_3 C1_3 C4_3 108.54(19) . . ? O1_3 C1_3 C3_3 108.85(17) . . ? C4_3 C1_3 C3_3 109.82(19) . . ? O1_3 C1_3 C2_3 110.20(17) . . ? C4_3 C1_3 C2_3 110.00(18) . . ? C3_3 C1_3 C2_3 109.41(19) . . ? F2_3 C2_3 F3_3 108.0(2) . . ? F2_3 C2_3 F1_3 108.30(19) . . ? F3_3 C2_3 F1_3 107.14(18) . . ? F2_3 C2_3 C1_3 112.97(18) . . ? F3_3 C2_3 C1_3 109.39(18) . . ? F1_3 C2_3 C1_3 110.82(19) . . ? F5_3 C3_3 F6_3 107.9(2) . . ? F5_3 C3_3 F4_3 107.4(2) . . ? F6_3 C3_3 F4_3 107.4(2) . . ? F5_3 C3_3 C1_3 110.38(19) . . ? F6_3 C3_3 C1_3 113.0(2) . . ? F4_3 C3_3 C1_3 110.5(2) . . ? F9_3 C4_3 F7_3 107.6(2) . . ? F9_3 C4_3 F8_3 108.4(2) . . ? F7_3 C4_3 F8_3 107.8(2) . . ? F9_3 C4_3 C1_3 110.7(2) . . ? F7_3 C4_3 C1_3 111.1(2) . . ? F8_3 C4_3 C1_3 111.2(2) . . ? C1_5 O1_5 Al2 148.71(14) . . ? O1_5 C1_5 C2_5 108.83(19) . . ? O1_5 C1_5 C3_5 111.64(16) . . ? C2_5 C1_5 C3_5 109.39(17) . . ? O1_5 C1_5 C4_5 108.54(17) . . ? C2_5 C1_5 C4_5 109.43(18) . . ? C3_5 C1_5 C4_5 108.97(18) . . ? F1_5 C2_5 F3_5 108.6(2) . . ? F1_5 C2_5 F2_5 107.6(2) . . ? F3_5 C2_5 F2_5 106.5(2) . . ? F1_5 C2_5 C1_5 112.1(2) . . ? F3_5 C2_5 C1_5 109.8(2) . . ? F2_5 C2_5 C1_5 111.9(2) . . ? F6_5 C3_5 F4_5 108.55(19) . . ? F6_5 C3_5 F5_5 106.92(18) . . ? F4_5 C3_5 F5_5 106.62(17) . . ? F6_5 C3_5 C1_5 113.15(18) . . ? F4_5 C3_5 C1_5 109.92(18) . . ? F5_5 C3_5 C1_5 111.40(17) . . ? F7_5 C4_5 F9_5 108.0(2) . . ? F7_5 C4_5 F8_5 108.1(2) . . ? F9_5 C4_5 F8_5 108.27(19) . . ? F7_5 C4_5 C1_5 110.27(18) . . ? F9_5 C4_5 C1_5 110.70(19) . . ? F8_5 C4_5 C1_5 111.3(2) . . ? C1_6 O1_6 Al2 147.10(14) . . ? O1_6 C1_6 C4_6 109.41(17) . . ? O1_6 C1_6 C2_6 108.72(17) . . ? C4_6 C1_6 C2_6 110.14(18) . . ? O1_6 C1_6 C3_6 110.55(16) . . ? C4_6 C1_6 C3_6 109.42(18) . . ? C2_6 C1_6 C3_6 108.59(17) . . ? F3_6 C2_6 F2_6 108.6(2) . . ? F3_6 C2_6 F1_6 106.4(2) . . ? F2_6 C2_6 F1_6 107.34(18) . . ? F3_6 C2_6 C1_6 111.38(18) . . ? F2_6 C2_6 C1_6 112.18(18) . . ? F1_6 C2_6 C1_6 110.71(19) . . ? F4_6 C3_6 F6_6 108.81(19) . . ? F4_6 C3_6 F5_6 106.70(19) . . ? F6_6 C3_6 F5_6 107.83(18) . . ? F4_6 C3_6 C1_6 110.22(17) . . ? F6_6 C3_6 C1_6 112.51(18) . . ? F5_6 C3_6 C1_6 110.57(18) . . ? F9_6 C4_6 F8_6 107.9(2) . . ? F9_6 C4_6 F7_6 108.0(2) . . ? F8_6 C4_6 F7_6 108.0(2) . . ? F9_6 C4_6 C1_6 110.7(2) . . ? F8_6 C4_6 C1_6 112.7(2) . . ? F7_6 C4_6 C1_6 109.5(2) . . ? C6_7 C1_7 F1_7 120.7(7) . . ? C6_7 C1_7 C2_7 122.2(7) . . ? F1_7 C1_7 C2_7 117.0(7) . . ? F2_7 C2_7 C1_7 121.0(6) . . ? F2_7 C2_7 C3_7 119.6(6) . . ? C1_7 C2_7 C3_7 119.4(6) . . ? F3_7 C3_7 C4_7 121.2(6) . . ? F3_7 C3_7 C2_7 120.5(6) . . ? C4_7 C3_7 C2_7 118.2(6) . . ? C5_7 C4_7 F4_7 120.7(7) . . ? C5_7 C4_7 C3_7 122.3(6) . . ? F4_7 C4_7 C3_7 116.9(7) . . ? C4_7 C5_7 C6_7 119.2(6) . . ? C4_7 C5_7 H5_7 120.4 . . ? C6_7 C5_7 H5_7 120.4 . . ? C1_7 C6_7 C5_7 118.6(6) . . ? C1_7 C6_7 H6_7 120.7 . . ? C5_7 C6_7 H6_7 120.7 . . ? C1_8 O1_8 Al2 151.0(3) . . ? O1_8 C1_8 C3_8 111.2(3) . . ? O1_8 C1_8 C2_8 110.5(3) . . ? C3_8 C1_8 C2_8 110.0(3) . . ? O1_8 C1_8 C4_8 107.3(2) . . ? C3_8 C1_8 C4_8 109.0(3) . . ? C2_8 C1_8 C4_8 108.8(2) . . ? F3_8 C2_8 F2_8 109.9(3) . . ? F3_8 C2_8 F1_8 106.4(3) . . ? F2_8 C2_8 F1_8 106.4(3) . . ? F3_8 C2_8 C1_8 112.0(2) . . ? F2_8 C2_8 C1_8 113.1(3) . . ? F1_8 C2_8 C1_8 108.6(2) . . ? F4_8 C3_8 F6_8 109.9(3) . . ? F4_8 C3_8 F5_8 106.6(3) . . ? F6_8 C3_8 F5_8 107.6(3) . . ? F4_8 C3_8 C1_8 113.2(3) . . ? F6_8 C3_8 C1_8 112.2(3) . . ? F5_8 C3_8 C1_8 107.1(3) . . ? F9_8 C4_8 F8_8 110.1(3) . . ? F9_8 C4_8 F7_8 106.2(3) . . ? F8_8 C4_8 F7_8 105.9(3) . . ? F9_8 C4_8 C1_8 112.2(3) . . ? F8_8 C4_8 C1_8 112.6(3) . . ? F7_8 C4_8 C1_8 109.5(3) . . ? C1_9 O1_9 Al2 166(2) . . ? O1_9 C1_9 C2_9 115.1(15) . . ? O1_9 C1_9 C4_9 107.5(14) . . ? C2_9 C1_9 C4_9 108.4(11) . . ? O1_9 C1_9 C3_9 111.8(16) . . ? C2_9 C1_9 C3_9 103.6(11) . . ? C4_9 C1_9 C3_9 110.4(11) . . ? F3_9 C2_9 F2_9 104.5(15) . . ? F3_9 C2_9 F1_9 114.5(14) . . ? F2_9 C2_9 F1_9 116.1(14) . . ? F3_9 C2_9 C1_9 110.1(13) . . ? F2_9 C2_9 C1_9 107.8(14) . . ? F1_9 C2_9 C1_9 103.7(11) . . ? F4_9 C3_9 F6_9 101.5(15) . . ? F4_9 C3_9 F5_9 120.9(16) . . ? F6_9 C3_9 F5_9 115.8(15) . . ? F4_9 C3_9 C1_9 106.3(13) . . ? F6_9 C3_9 C1_9 109.7(16) . . ? F5_9 C3_9 C1_9 102.3(11) . . ? F9_9 C4_9 F8_9 105.5(14) . . ? F9_9 C4_9 F7_9 123.3(16) . . ? F8_9 C4_9 F7_9 105.5(14) . . ? F9_9 C4_9 C1_9 107.8(12) . . ? F8_9 C4_9 C1_9 112.5(14) . . ? F7_9 C4_9 C1_9 102.5(12) . . ? C1_10 O1_10 Al1 151.6(3) . . ? O1_10 C1_10 C2_10 108.1(2) . . ? O1_10 C1_10 C4_10 111.2(2) . . ? C2_10 C1_10 C4_10 109.3(2) . . ? O1_10 C1_10 C3_10 109.8(2) . . ? C2_10 C1_10 C3_10 109.7(2) . . ? C4_10 C1_10 C3_10 108.7(2) . . ? F3_10 C2_10 F1_10 107.9(2) . . ? F3_10 C2_10 F2_10 107.7(2) . . ? F1_10 C2_10 F2_10 107.9(2) . . ? F3_10 C2_10 C1_10 110.6(2) . . ? F1_10 C2_10 C1_10 110.5(2) . . ? F2_10 C2_10 C1_10 112.0(2) . . ? F4_10 C3_10 F5_10 107.5(2) . . ? F4_10 C3_10 F6_10 107.3(2) . . ? F5_10 C3_10 F6_10 107.2(2) . . ? F4_10 C3_10 C1_10 110.9(2) . . ? F5_10 C3_10 C1_10 111.2(2) . . ? F6_10 C3_10 C1_10 112.4(2) . . ? F9_10 C4_10 F7_10 107.7(2) . . ? F9_10 C4_10 F8_10 107.8(2) . . ? F7_10 C4_10 F8_10 107.1(2) . . ? F9_10 C4_10 C1_10 111.3(2) . . ? F7_10 C4_10 C1_10 110.8(2) . . ? F8_10 C4_10 C1_10 112.0(2) . . ? C1_13 O1_13 Al1 150(3) . . ? O1_13 C1_13 C4_13 109.8(19) . . ? O1_13 C1_13 C2_13 110.3(19) . . ? C4_13 C1_13 C2_13 109.1(12) . . ? O1_13 C1_13 C3_13 109.3(18) . . ? C4_13 C1_13 C3_13 109.5(12) . . ? C2_13 C1_13 C3_13 108.8(12) . . ? F3_13 C2_13 F1_13 107.2(16) . . ? F3_13 C2_13 F2_13 107.8(16) . . ? F1_13 C2_13 F2_13 108.5(16) . . ? F3_13 C2_13 C1_13 110.0(14) . . ? F1_13 C2_13 C1_13 110.5(14) . . ? F2_13 C2_13 C1_13 112.6(15) . . ? F4_13 C3_13 F5_13 106.9(15) . . ? F4_13 C3_13 F6_13 109.8(17) . . ? F5_13 C3_13 F6_13 108.9(17) . . ? F4_13 C3_13 C1_13 112.0(14) . . ? F5_13 C3_13 C1_13 110.5(14) . . ? F6_13 C3_13 C1_13 108.7(16) . . ? F9_13 C4_13 F7_13 107.9(15) . . ? F9_13 C4_13 F8_13 106.4(17) . . ? F7_13 C4_13 F8_13 110.6(17) . . ? F9_13 C4_13 C1_13 111.6(14) . . ? F7_13 C4_13 C1_13 111.6(14) . . ? F8_13 C4_13 C1_13 108.5(16) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_3 Al1 O1_1 C1_1 -9.9(3) . . . . ? O1_10 Al1 O1_1 C1_1 124.1(3) . . . . ? O1_13 Al1 O1_1 C1_1 127.2(15) . . . . ? F1 Al1 O1_1 C1_1 -127.2(3) . . . . ? Al1 O1_1 C1_1 C2_1 -145.4(3) . . . . ? Al1 O1_1 C1_1 C4_1 -24.5(4) . . . . ? Al1 O1_1 C1_1 C3_1 95.9(3) . . . . ? O1_1 C1_1 C2_1 F3_1 -42.2(2) . . . . ? C4_1 C1_1 C2_1 F3_1 -164.47(19) . . . . ? C3_1 C1_1 C2_1 F3_1 76.4(2) . . . . ? O1_1 C1_1 C2_1 F1_1 78.5(2) . . . . ? C4_1 C1_1 C2_1 F1_1 -43.8(2) . . . . ? C3_1 C1_1 C2_1 F1_1 -163.02(19) . . . . ? O1_1 C1_1 C2_1 F2_1 -161.96(19) . . . . ? C4_1 C1_1 C2_1 F2_1 75.7(2) . . . . ? C3_1 C1_1 C2_1 F2_1 -43.5(3) . . . . ? O1_1 C1_1 C3_1 F4_1 -46.9(3) . . . . ? C2_1 C1_1 C3_1 F4_1 -164.1(2) . . . . ? C4_1 C1_1 C3_1 F4_1 75.8(2) . . . . ? O1_1 C1_1 C3_1 F5_1 72.7(2) . . . . ? C2_1 C1_1 C3_1 F5_1 -44.4(2) . . . . ? C4_1 C1_1 C3_1 F5_1 -164.58(18) . . . . ? O1_1 C1_1 C3_1 F6_1 -167.81(18) . . . . ? C2_1 C1_1 C3_1 F6_1 75.0(2) . . . . ? C4_1 C1_1 C3_1 F6_1 -45.1(2) . . . . ? O1_1 C1_1 C4_1 F7_1 78.9(2) . . . . ? C2_1 C1_1 C4_1 F7_1 -161.84(18) . . . . ? C3_1 C1_1 C4_1 F7_1 -42.0(2) . . . . ? O1_1 C1_1 C4_1 F9_1 -40.6(3) . . . . ? C2_1 C1_1 C4_1 F9_1 78.6(2) . . . . ? C3_1 C1_1 C4_1 F9_1 -161.54(19) . . . . ? O1_1 C1_1 C4_1 F8_1 -160.2(2) . . . . ? C2_1 C1_1 C4_1 F8_1 -41.0(3) . . . . ? C3_1 C1_1 C4_1 F8_1 78.9(2) . . . . ? O1_1 Al1 O1_3 C1_3 -159.0(2) . . . . ? O1_10 Al1 O1_3 C1_3 69.8(3) . . . . ? O1_13 Al1 O1_3 C1_3 69.2(17) . . . . ? F1 Al1 O1_3 C1_3 -45.4(3) . . . . ? Al1 O1_3 C1_3 C4_3 -158.7(2) . . . . ? Al1 O1_3 C1_3 C3_3 81.8(3) . . . . ? Al1 O1_3 C1_3 C2_3 -38.2(3) . . . . ? O1_3 C1_3 C2_3 F2_3 160.81(19) . . . . ? C4_3 C1_3 C2_3 F2_3 -79.6(3) . . . . ? C3_3 C1_3 C2_3 F2_3 41.2(3) . . . . ? O1_3 C1_3 C2_3 F3_3 40.4(2) . . . . ? C4_3 C1_3 C2_3 F3_3 160.1(2) . . . . ? C3_3 C1_3 C2_3 F3_3 -79.2(2) . . . . ? O1_3 C1_3 C2_3 F1_3 -77.5(2) . . . . ? C4_3 C1_3 C2_3 F1_3 42.2(2) . . . . ? C3_3 C1_3 C2_3 F1_3 162.89(18) . . . . ? O1_3 C1_3 C3_3 F5_3 -73.8(2) . . . . ? C4_3 C1_3 C3_3 F5_3 167.46(19) . . . . ? C2_3 C1_3 C3_3 F5_3 46.6(2) . . . . ? O1_3 C1_3 C3_3 F6_3 165.2(2) . . . . ? C4_3 C1_3 C3_3 F6_3 46.5(3) . . . . ? C2_3 C1_3 C3_3 F6_3 -74.3(3) . . . . ? O1_3 C1_3 C3_3 F4_3 44.9(3) . . . . ? C4_3 C1_3 C3_3 F4_3 -73.8(2) . . . . ? C2_3 C1_3 C3_3 F4_3 165.33(19) . . . . ? O1_3 C1_3 C4_3 F9_3 44.3(3) . . . . ? C3_3 C1_3 C4_3 F9_3 163.2(2) . . . . ? C2_3 C1_3 C4_3 F9_3 -76.4(2) . . . . ? O1_3 C1_3 C4_3 F7_3 -75.2(3) . . . . ? C3_3 C1_3 C4_3 F7_3 43.7(3) . . . . ? C2_3 C1_3 C4_3 F7_3 164.2(2) . . . . ? O1_3 C1_3 C4_3 F8_3 164.8(2) . . . . ? C3_3 C1_3 C4_3 F8_3 -76.3(3) . . . . ? C2_3 C1_3 C4_3 F8_3 44.2(3) . . . . ? O1_9 Al2 O1_5 C1_5 135.1(13) . . . . ? O1_8 Al2 O1_5 C1_5 140.0(3) . . . . ? O1_6 Al2 O1_5 C1_5 7.3(3) . . . . ? F1 Al2 O1_5 C1_5 -108.7(3) . . . . ? Al2 O1_5 C1_5 C2_5 -92.7(3) . . . . ? Al2 O1_5 C1_5 C3_5 28.2(4) . . . . ? Al2 O1_5 C1_5 C4_5 148.3(3) . . . . ? O1_5 C1_5 C2_5 F1_5 -77.5(3) . . . . ? C3_5 C1_5 C2_5 F1_5 160.3(2) . . . . ? C4_5 C1_5 C2_5 F1_5 41.0(3) . . . . ? O1_5 C1_5 C2_5 F3_5 43.4(2) . . . . ? C3_5 C1_5 C2_5 F3_5 -78.9(2) . . . . ? C4_5 C1_5 C2_5 F3_5 161.83(19) . . . . ? O1_5 C1_5 C2_5 F2_5 161.5(2) . . . . ? C3_5 C1_5 C2_5 F2_5 39.3(3) . . . . ? C4_5 C1_5 C2_5 F2_5 -80.1(3) . . . . ? O1_5 C1_5 C3_5 F6_5 160.10(19) . . . . ? C2_5 C1_5 C3_5 F6_5 -79.4(2) . . . . ? C4_5 C1_5 C3_5 F6_5 40.2(2) . . . . ? O1_5 C1_5 C3_5 F4_5 38.6(2) . . . . ? C2_5 C1_5 C3_5 F4_5 159.08(19) . . . . ? C4_5 C1_5 C3_5 F4_5 -81.3(2) . . . . ? O1_5 C1_5 C3_5 F5_5 -79.4(2) . . . . ? C2_5 C1_5 C3_5 F5_5 41.1(2) . . . . ? C4_5 C1_5 C3_5 F5_5 160.72(18) . . . . ? O1_5 C1_5 C4_5 F7_5 -74.9(2) . . . . ? C2_5 C1_5 C4_5 F7_5 166.4(2) . . . . ? C3_5 C1_5 C4_5 F7_5 46.8(3) . . . . ? O1_5 C1_5 C4_5 F9_5 44.6(2) . . . . ? C2_5 C1_5 C4_5 F9_5 -74.1(2) . . . . ? C3_5 C1_5 C4_5 F9_5 166.34(18) . . . . ? O1_5 C1_5 C4_5 F8_5 165.1(2) . . . . ? C2_5 C1_5 C4_5 F8_5 46.4(3) . . . . ? C3_5 C1_5 C4_5 F8_5 -73.2(2) . . . . ? O1_9 Al2 O1_6 C1_6 71.1(12) . . . . ? O1_5 Al2 O1_6 C1_6 -165.6(3) . . . . ? O1_8 Al2 O1_6 C1_6 62.1(3) . . . . ? F1 Al2 O1_6 C1_6 -51.1(3) . . . . ? Al2 O1_6 C1_6 C4_6 94.3(3) . . . . ? Al2 O1_6 C1_6 C2_6 -145.4(2) . . . . ? Al2 O1_6 C1_6 C3_6 -26.3(3) . . . . ? O1_6 C1_6 C2_6 F3_6 44.4(2) . . . . ? C4_6 C1_6 C2_6 F3_6 164.29(18) . . . . ? C3_6 C1_6 C2_6 F3_6 -75.9(2) . . . . ? O1_6 C1_6 C2_6 F2_6 166.36(18) . . . . ? C4_6 C1_6 C2_6 F2_6 -73.8(2) . . . . ? C3_6 C1_6 C2_6 F2_6 46.0(2) . . . . ? O1_6 C1_6 C2_6 F1_6 -73.8(2) . . . . ? C4_6 C1_6 C2_6 F1_6 46.1(2) . . . . ? C3_6 C1_6 C2_6 F1_6 165.92(18) . . . . ? O1_6 C1_6 C3_6 F4_6 40.3(2) . . . . ? C4_6 C1_6 C3_6 F4_6 -80.3(2) . . . . ? C2_6 C1_6 C3_6 F4_6 159.49(19) . . . . ? O1_6 C1_6 C3_6 F6_6 161.95(18) . . . . ? C4_6 C1_6 C3_6 F6_6 41.4(2) . . . . ? C2_6 C1_6 C3_6 F6_6 -78.9(2) . . . . ? O1_6 C1_6 C3_6 F5_6 -77.4(2) . . . . ? C4_6 C1_6 C3_6 F5_6 162.01(18) . . . . ? C2_6 C1_6 C3_6 F5_6 41.8(2) . . . . ? O1_6 C1_6 C4_6 F9_6 45.0(3) . . . . ? C2_6 C1_6 C4_6 F9_6 -74.4(2) . . . . ? C3_6 C1_6 C4_6 F9_6 166.31(19) . . . . ? O1_6 C1_6 C4_6 F8_6 165.95(19) . . . . ? C2_6 C1_6 C4_6 F8_6 46.5(3) . . . . ? C3_6 C1_6 C4_6 F8_6 -72.8(3) . . . . ? O1_6 C1_6 C4_6 F7_6 -73.9(2) . . . . ? C2_6 C1_6 C4_6 F7_6 166.63(18) . . . . ? C3_6 C1_6 C4_6 F7_6 47.3(2) . . . . ? C6_7 C1_7 C2_7 F2_7 178.3(8) . . . . ? F1_7 C1_7 C2_7 F2_7 1.2(12) . . . . ? C6_7 C1_7 C2_7 C3_7 -2.0(12) . . . . ? F1_7 C1_7 C2_7 C3_7 -179.2(8) . . . . ? F2_7 C2_7 C3_7 F3_7 0.1(12) . . . . ? C1_7 C2_7 C3_7 F3_7 -179.6(8) . . . . ? F2_7 C2_7 C3_7 C4_7 -178.2(7) . . . . ? C1_7 C2_7 C3_7 C4_7 2.2(12) . . . . ? F3_7 C3_7 C4_7 C5_7 179.9(8) . . . . ? C2_7 C3_7 C4_7 C5_7 -1.9(12) . . . . ? F3_7 C3_7 C4_7 F4_7 -2.3(12) . . . . ? C2_7 C3_7 C4_7 F4_7 175.9(8) . . . . ? F4_7 C4_7 C5_7 C6_7 -176.3(8) . . . . ? C3_7 C4_7 C5_7 C6_7 1.4(12) . . . . ? F1_7 C1_7 C6_7 C5_7 178.5(8) . . . . ? C2_7 C1_7 C6_7 C5_7 1.5(13) . . . . ? C4_7 C5_7 C6_7 C1_7 -1.1(12) . . . . ? O1_5 Al2 O1_8 C1_8 -42.7(7) . . . . ? O1_6 Al2 O1_8 C1_8 88.1(6) . . . . ? F1 Al2 O1_8 C1_8 -155.6(6) . . . . ? Al2 O1_8 C1_8 C3_8 56.6(7) . . . . ? Al2 O1_8 C1_8 C2_8 -65.8(7) . . . . ? Al2 O1_8 C1_8 C4_8 175.7(6) . . . . ? O1_8 C1_8 C2_8 F3_8 40.5(3) . . . . ? C3_8 C1_8 C2_8 F3_8 -82.6(3) . . . . ? C4_8 C1_8 C2_8 F3_8 158.0(3) . . . . ? O1_8 C1_8 C2_8 F2_8 165.4(3) . . . . ? C3_8 C1_8 C2_8 F2_8 42.3(3) . . . . ? C4_8 C1_8 C2_8 F2_8 -77.1(3) . . . . ? O1_8 C1_8 C2_8 F1_8 -76.7(3) . . . . ? C3_8 C1_8 C2_8 F1_8 160.2(2) . . . . ? C4_8 C1_8 C2_8 F1_8 40.8(3) . . . . ? O1_8 C1_8 C3_8 F4_8 39.5(4) . . . . ? C2_8 C1_8 C3_8 F4_8 162.2(3) . . . . ? C4_8 C1_8 C3_8 F4_8 -78.6(4) . . . . ? O1_8 C1_8 C3_8 F6_8 164.5(3) . . . . ? C2_8 C1_8 C3_8 F6_8 -72.8(4) . . . . ? C4_8 C1_8 C3_8 F6_8 46.4(4) . . . . ? O1_8 C1_8 C3_8 F5_8 -77.7(3) . . . . ? C2_8 C1_8 C3_8 F5_8 45.0(3) . . . . ? C4_8 C1_8 C3_8 F5_8 164.2(3) . . . . ? O1_8 C1_8 C4_8 F9_8 39.7(4) . . . . ? C3_8 C1_8 C4_8 F9_8 160.2(3) . . . . ? C2_8 C1_8 C4_8 F9_8 -79.9(3) . . . . ? O1_8 C1_8 C4_8 F8_8 164.6(3) . . . . ? C3_8 C1_8 C4_8 F8_8 -74.9(3) . . . . ? C2_8 C1_8 C4_8 F8_8 45.1(4) . . . . ? O1_8 C1_8 C4_8 F7_8 -78.0(3) . . . . ? C3_8 C1_8 C4_8 F7_8 42.6(3) . . . . ? C2_8 C1_8 C4_8 F7_8 162.5(2) . . . . ? O1_5 Al2 O1_9 C1_9 -41(11) . . . . ? O1_6 Al2 O1_9 C1_9 84(11) . . . . ? F1 Al2 O1_9 C1_9 -154(11) . . . . ? Al2 O1_9 C1_9 C2_9 156(10) . . . . ? Al2 O1_9 C1_9 C4_9 35(11) . . . . ? Al2 O1_9 C1_9 C3_9 -86(11) . . . . ? O1_9 C1_9 C2_9 F3_9 45(2) . . . . ? C4_9 C1_9 C2_9 F3_9 165.6(14) . . . . ? C3_9 C1_9 C2_9 F3_9 -77.1(15) . . . . ? O1_9 C1_9 C2_9 F2_9 158.7(19) . . . . ? C4_9 C1_9 C2_9 F2_9 -80.9(16) . . . . ? C3_9 C1_9 C2_9 F2_9 36.3(17) . . . . ? O1_9 C1_9 C2_9 F1_9 -77.7(19) . . . . ? C4_9 C1_9 C2_9 F1_9 42.7(15) . . . . ? C3_9 C1_9 C2_9 F1_9 159.9(13) . . . . ? O1_9 C1_9 C3_9 F4_9 44.6(19) . . . . ? C2_9 C1_9 C3_9 F4_9 169.1(15) . . . . ? C4_9 C1_9 C3_9 F4_9 -75.1(16) . . . . ? O1_9 C1_9 C3_9 F6_9 153.6(18) . . . . ? C2_9 C1_9 C3_9 F6_9 -81.9(16) . . . . ? C4_9 C1_9 C3_9 F6_9 33.9(18) . . . . ? O1_9 C1_9 C3_9 F5_9 -83.1(18) . . . . ? C2_9 C1_9 C3_9 F5_9 41.4(15) . . . . ? C4_9 C1_9 C3_9 F5_9 157.2(14) . . . . ? O1_9 C1_9 C4_9 F9_9 48(2) . . . . ? C2_9 C1_9 C4_9 F9_9 -77.0(15) . . . . ? C3_9 C1_9 C4_9 F9_9 170.2(14) . . . . ? O1_9 C1_9 C4_9 F8_9 164(2) . . . . ? C2_9 C1_9 C4_9 F8_9 38.9(18) . . . . ? C3_9 C1_9 C4_9 F8_9 -73.9(17) . . . . ? O1_9 C1_9 C4_9 F7_9 -83.4(19) . . . . ? C2_9 C1_9 C4_9 F7_9 151.6(15) . . . . ? C3_9 C1_9 C4_9 F7_9 38.8(16) . . . . ? O1_3 Al1 O1_10 C1_10 75.6(6) . . . . ? O1_1 Al1 O1_10 C1_10 -54.4(6) . . . . ? F1 Al1 O1_10 C1_10 -164.7(6) . . . . ? Al1 O1_10 C1_10 C2_10 -149.9(5) . . . . ? Al1 O1_10 C1_10 C4_10 -29.9(7) . . . . ? Al1 O1_10 C1_10 C3_10 90.5(6) . . . . ? O1_10 C1_10 C2_10 F3_10 -44.2(3) . . . . ? C4_10 C1_10 C2_10 F3_10 -165.4(2) . . . . ? C3_10 C1_10 C2_10 F3_10 75.4(3) . . . . ? O1_10 C1_10 C2_10 F1_10 75.1(3) . . . . ? C4_10 C1_10 C2_10 F1_10 -46.0(3) . . . . ? C3_10 C1_10 C2_10 F1_10 -165.2(2) . . . . ? O1_10 C1_10 C2_10 F2_10 -164.5(3) . . . . ? C4_10 C1_10 C2_10 F2_10 74.4(3) . . . . ? C3_10 C1_10 C2_10 F2_10 -44.8(3) . . . . ? O1_10 C1_10 C3_10 F4_10 -44.3(3) . . . . ? C2_10 C1_10 C3_10 F4_10 -162.9(2) . . . . ? C4_10 C1_10 C3_10 F4_10 77.5(3) . . . . ? O1_10 C1_10 C3_10 F5_10 75.3(3) . . . . ? C2_10 C1_10 C3_10 F5_10 -43.4(3) . . . . ? C4_10 C1_10 C3_10 F5_10 -162.9(2) . . . . ? O1_10 C1_10 C3_10 F6_10 -164.5(3) . . . . ? C2_10 C1_10 C3_10 F6_10 76.9(3) . . . . ? C4_10 C1_10 C3_10 F6_10 -42.7(3) . . . . ? O1_10 C1_10 C4_10 F9_10 -40.7(3) . . . . ? C2_10 C1_10 C4_10 F9_10 78.6(3) . . . . ? C3_10 C1_10 C4_10 F9_10 -161.6(2) . . . . ? O1_10 C1_10 C4_10 F7_10 79.2(3) . . . . ? C2_10 C1_10 C4_10 F7_10 -161.6(2) . . . . ? C3_10 C1_10 C4_10 F7_10 -41.8(3) . . . . ? O1_10 C1_10 C4_10 F8_10 -161.4(3) . . . . ? C2_10 C1_10 C4_10 F8_10 -42.1(3) . . . . ? C3_10 C1_10 C4_10 F8_10 77.6(3) . . . . ? O1_3 Al1 O1_13 C1_13 69(7) . . . . ? O1_1 Al1 O1_13 C1_13 -62(6) . . . . ? F1 Al1 O1_13 C1_13 -171(6) . . . . ? Al1 O1_13 C1_13 C4_13 -151(6) . . . . ? Al1 O1_13 C1_13 C2_13 -31(7) . . . . ? Al1 O1_13 C1_13 C3_13 89(6) . . . . ? O1_13 C1_13 C2_13 F3_13 42(2) . . . . ? C4_13 C1_13 C2_13 F3_13 162.2(16) . . . . ? C3_13 C1_13 C2_13 F3_13 -78.4(18) . . . . ? O1_13 C1_13 C2_13 F1_13 -77(2) . . . . ? C4_13 C1_13 C2_13 F1_13 44.0(19) . . . . ? C3_13 C1_13 C2_13 F1_13 163.4(16) . . . . ? O1_13 C1_13 C2_13 F2_13 162(2) . . . . ? C4_13 C1_13 C2_13 F2_13 -77.5(19) . . . . ? C3_13 C1_13 C2_13 F2_13 41.9(19) . . . . ? O1_13 C1_13 C3_13 F4_13 44(2) . . . . ? C4_13 C1_13 C3_13 F4_13 -76.6(18) . . . . ? C2_13 C1_13 C3_13 F4_13 164.2(17) . . . . ? O1_13 C1_13 C3_13 F5_13 -75(2) . . . . ? C4_13 C1_13 C3_13 F5_13 164.3(16) . . . . ? C2_13 C1_13 C3_13 F5_13 45.1(19) . . . . ? O1_13 C1_13 C3_13 F6_13 165(2) . . . . ? C4_13 C1_13 C3_13 F6_13 44.9(19) . . . . ? C2_13 C1_13 C3_13 F6_13 -74.3(19) . . . . ? O1_13 C1_13 C4_13 F9_13 46(2) . . . . ? C2_13 C1_13 C4_13 F9_13 -75.2(18) . . . . ? C3_13 C1_13 C4_13 F9_13 165.8(16) . . . . ? O1_13 C1_13 C4_13 F7_13 -75(2) . . . . ? C2_13 C1_13 C4_13 F7_13 163.9(17) . . . . ? C3_13 C1_13 C4_13 F7_13 44.9(19) . . . . ? O1_13 C1_13 C4_13 F8_13 163(2) . . . . ? C2_13 C1_13 C4_13 F8_13 41.7(19) . . . . ? C3_13 C1_13 C4_13 F8_13 -77.3(19) . . . . ? _shelx_res_file ; TITL p-1_a.res in P-1 p-1_a.res created by SHELXL-2018/3 at 13:02:04 on 18-Mar-2022 REM Old TITL p-1 in P-1 REM SHELXT solution in P-1: R1 0.114, Rweak 0.005, Alpha 0.098 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C70 O6 F134 Al4 Ru3 CELL 0.71073 11.8190 12.9397 19.4772 102.636 103.912 92.736 ZERR 1.000 0.0025 0.0033 0.0045 0.012 0.017 0.017 LATT 1 SFAC C H O F AL RU UNIT 68 2 26 114 4 3 EADP F8_9 F6_8 SIMU 0.01 0.02 2 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 RIGU 0.002 0.002 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 O1_9 C1_9 C2_9 F1_9 F2_9 F3_9 C3_9 F4_9 F5_9 F6_9 = C4_9 F7_9 F8_9 F9_9 SIMU 0.02 0.02 2 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 F4_10 F5_10 = F6_10 C4_10 F7_10 F8_10 F9_10 O1_13 C1_13 C2_13 F1_13 F2_13 F3_13 C3_13 = F4_13 F5_13 F6_13 C4_13 F7_13 F8_13 F9_13 RIGU 0.002 0.002 O1_10 C1_10 C2_10 F1_10 F2_10 F3_10 C3_10 F4_10 F5_10 = F6_10 C4_10 F7_10 F8_10 F9_10 O1_13 C1_13 C2_13 F1_13 F2_13 F3_13 C3_13 = F4_13 F5_13 F6_13 C4_13 F7_13 F8_13 F9_13 REM Restraints for Fragment tetfluorbenz, 1,2,3,4-Tetrafluorobenzene, REM C6H2F4 from: CCDC ZELDOJ, http://dx.doi.org/10.1002/anie.199515171. REM Please cite https://doi.org/10.1107/S1600576718004508 REM HFIX_TFB 43 C5 C6 OMIT 3 -6 3 BIND RU1 RU2 OMIT -1 1 7 SIMU_TFB F1 > C6 RIGU_TFB F1 > C6 FLAT_TFB F1 > C6 SADI_TFB 0.02 C1 C2 C2 C3 C3 C4 C4 C5 C5 C6 C6 C1 SADI_TFB 0.02 C1 F1 C2 F2 C3 F3 C4 F4 SADI_TFB 0.04 C1 C3 C3 C5 C5 C1 C2 C6 C6 C4 C2 C4 SADI_TFB 0.05 C2 F1 C6 F1 C1 F2 C3 F2 C2 F3 C4 F3 C3 F4 C5 F4 SAME_TFB F1 > C6 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 SIMU 0.04 0.08 1 TEMP -173.150 SIZE 0.115 0.134 0.231 L.S. 10 BOND $H CONF MORE -1 LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.038800 3.332600 FVAR 0.52227 0.92071 0.87976 0.31617 0.10847 RU1 6 0.048966 0.081409 0.655839 11.00000 0.01503 0.01659 = 0.01441 0.00140 0.00462 0.00059 RU2 6 0.000000 0.000000 0.500000 10.50000 0.01304 0.01480 = 0.01404 0.00165 0.00440 -0.00001 AL1 5 0.666497 0.549069 0.803506 11.00000 0.01536 0.01621 = 0.01646 0.00373 0.00393 0.00063 AL2 5 0.590892 0.803764 0.783661 11.00000 0.01634 0.01743 = 0.01505 0.00329 0.00536 0.00265 F1 4 0.623906 0.675189 0.793384 11.00000 0.02199 0.01798 = 0.02089 0.00572 0.00677 0.00478 C3 1 -0.120027 0.101872 0.636739 11.00000 0.02116 0.02118 = 0.01903 0.00168 0.00812 0.00113 O3 3 -0.215796 0.112793 0.623929 11.00000 0.02127 0.03292 = 0.03208 0.00406 0.01017 0.00478 O4 3 -0.007241 -0.148109 0.671285 11.00000 0.02964 0.02463 = 0.03459 0.00957 0.00904 0.00074 O5 3 0.301888 0.029079 0.654309 11.00000 0.02046 0.02740 = 0.02887 0.00759 0.00695 0.00454 O6 3 -0.138576 0.191935 0.478286 11.00000 0.02357 0.02504 = 0.03659 0.00833 0.00701 0.00635 O7 3 -0.230139 -0.124946 0.498175 11.00000 0.02266 0.03300 = 0.02629 0.00415 0.00914 -0.00593 C1 1 0.085570 0.142713 0.762924 11.00000 0.02267 0.02177 = 0.02000 0.00366 0.00656 0.00315 C2 1 0.079963 0.220624 0.634570 11.00000 0.01576 0.02182 = 0.01910 0.00122 0.00458 0.00142 O1 3 0.107502 0.178358 0.822600 11.00000 0.03505 0.03090 = 0.01879 0.00187 0.00582 0.00415 O2 3 0.095603 0.300030 0.621993 11.00000 0.02354 0.02251 = 0.03022 0.00473 0.00859 0.00062 C4 1 0.012453 -0.066069 0.665035 11.00000 0.01976 0.02410 = 0.01972 0.00371 0.00652 0.00167 C5 1 0.211281 0.049058 0.655937 11.00000 0.02041 0.01926 = 0.01754 0.00313 0.00374 0.00047 C6 1 -0.087396 0.121990 0.485368 11.00000 0.01593 0.02041 = 0.01937 0.00318 0.00465 -0.00183 C7 1 -0.145006 -0.080233 0.499701 11.00000 0.01982 0.02073 = 0.01672 0.00204 0.00574 0.00035 RESI CCF3 1 O1 3 0.547589 0.462726 0.752827 11.00000 0.02990 0.03124 = 0.02235 0.00764 -0.00043 -0.01469 C1 1 0.466699 0.382483 0.748324 11.00000 0.02172 0.02117 = 0.02300 0.00431 0.00415 -0.00355 C2 1 0.439957 0.310695 0.669808 11.00000 0.02430 0.02526 = 0.03196 -0.00020 0.00816 -0.00272 F1 4 0.523917 0.247495 0.662942 11.00000 0.03679 0.04620 = 0.04836 -0.00743 0.01431 0.01154 F2 4 0.338285 0.247449 0.652435 11.00000 0.03120 0.02702 = 0.03861 -0.00571 0.00586 -0.01032 F3 4 0.431060 0.367689 0.620816 11.00000 0.04071 0.04217 = 0.02277 0.00259 0.00450 -0.01203 C3 1 0.352966 0.429419 0.761877 11.00000 0.02911 0.02833 = 0.02926 -0.00108 0.00573 0.00139 F4 4 0.378388 0.510099 0.819528 11.00000 0.04931 0.03986 = 0.03650 -0.01052 0.00464 0.01217 F5 4 0.296935 0.464430 0.704795 11.00000 0.03659 0.03288 = 0.03804 0.00259 -0.00353 0.00862 F6 4 0.278099 0.356475 0.772265 11.00000 0.02877 0.05785 = 0.04343 0.00682 0.01550 -0.00520 C4 1 0.510147 0.315526 0.805021 11.00000 0.03341 0.02574 = 0.03596 0.01103 0.00483 -0.00221 F7 4 0.501590 0.363644 0.870610 11.00000 0.04401 0.04433 = 0.02912 0.01560 0.00757 -0.00782 F8 4 0.448489 0.219582 0.785849 11.00000 0.06852 0.02570 = 0.05844 0.01902 0.00070 -0.01189 F9 4 0.622313 0.300913 0.809902 11.00000 0.03721 0.05132 = 0.05199 0.01730 0.00385 0.01633 RESI 0 RESI CCF3 2 RESI 0 RESI CCF3 3 O1 3 0.692070 0.544503 0.892416 11.00000 0.02359 0.02484 = 0.01643 0.00584 0.00282 -0.00080 C1 1 0.743208 0.595078 0.963043 11.00000 0.01849 0.02980 = 0.01795 0.00657 0.00319 0.00148 C2 1 0.863819 0.654974 0.969365 11.00000 0.02260 0.03310 = 0.02216 0.00077 0.00610 -0.00197 F1 4 0.944976 0.587510 0.965975 11.00000 0.01960 0.05068 = 0.04767 0.00670 0.00824 0.00733 F2 4 0.901548 0.730405 1.030549 11.00000 0.03196 0.05253 = 0.02790 -0.01057 0.00628 -0.01105 F3 4 0.855272 0.700587 0.913638 11.00000 0.04239 0.03217 = 0.03015 0.00526 0.01298 -0.00902 C3 1 0.661701 0.676169 0.990231 11.00000 0.02284 0.04753 = 0.02579 0.00026 0.00661 0.00404 F4 4 0.550951 0.632216 0.969812 11.00000 0.02032 0.06843 = 0.04573 -0.00294 0.00924 0.00432 F5 4 0.665379 0.760241 0.961548 11.00000 0.04817 0.03769 = 0.04946 0.00309 0.01081 0.01782 F6 4 0.690172 0.711171 1.062371 11.00000 0.03861 0.07726 = 0.02709 -0.01162 0.01457 -0.00044 C4 1 0.759881 0.510820 1.009185 11.00000 0.03248 0.05175 = 0.03056 0.02406 0.00119 -0.00017 F7 4 0.658666 0.477872 1.019871 11.00000 0.04647 0.07701 = 0.04000 0.03156 0.01172 -0.01218 F8 4 0.834236 0.550581 1.074424 11.00000 0.04906 0.08765 = 0.03108 0.03135 -0.01081 -0.00547 F9 4 0.801473 0.426407 0.975799 11.00000 0.04967 0.04441 = 0.06083 0.03103 0.00467 0.01222 RESI 0 RESI CCF3 4 RESI 0 RESI CCF3 5 O1 3 0.489203 0.834997 0.831458 11.00000 0.02080 0.04521 = 0.02233 0.00929 0.00988 0.01284 C1 1 0.376876 0.850565 0.831190 11.00000 0.01845 0.02201 = 0.02042 0.00378 0.00721 0.00561 C2 1 0.362297 0.970318 0.837497 11.00000 0.03945 0.02499 = 0.03353 0.00098 -0.00292 0.00865 F1 4 0.404998 1.027796 0.904806 11.00000 0.05965 0.03111 = 0.03817 -0.00748 -0.00406 0.00939 F2 4 0.249164 0.987241 0.816134 11.00000 0.05267 0.04720 = 0.06002 -0.00455 -0.00860 0.03564 F3 4 0.417232 1.007281 0.794054 11.00000 0.07058 0.03206 = 0.04298 0.01719 -0.00751 -0.01485 C3 1 0.289799 0.783790 0.760578 11.00000 0.02549 0.02557 = 0.02329 0.00498 0.00709 0.00050 F4 4 0.326080 0.688630 0.741324 11.00000 0.05758 0.02159 = 0.02898 0.00198 0.01045 0.00494 F5 4 0.284042 0.830105 0.704439 11.00000 0.02985 0.02943 = 0.02293 0.00853 0.00114 0.00152 F6 4 0.181479 0.770145 0.767297 11.00000 0.02451 0.06132 = 0.03686 0.00469 0.00828 -0.01050 C4 1 0.349479 0.817073 0.897966 11.00000 0.03273 0.04128 = 0.02423 0.00545 0.01441 0.00428 F7 4 0.336361 0.711932 0.886210 11.00000 0.08215 0.04185 = 0.03517 0.01658 0.01905 -0.00677 F8 4 0.251689 0.853442 0.910864 11.00000 0.03117 0.08868 = 0.03739 0.00095 0.02272 0.00708 F9 4 0.436334 0.854454 0.957249 11.00000 0.03855 0.05393 = 0.01984 0.00672 0.01063 0.00963 RESI 0 RESI CCF3 6 O1 3 0.533456 0.795423 0.692659 11.00000 0.02073 0.02848 = 0.01475 0.00405 0.00631 0.00370 C1 1 0.545686 0.762945 0.623961 11.00000 0.01761 0.02766 = 0.01757 0.00506 0.00527 0.00236 C2 1 0.495009 0.844093 0.579476 11.00000 0.02505 0.04046 = 0.02195 0.01193 0.00653 0.00884 F1 4 0.377976 0.833144 0.563038 11.00000 0.02279 0.07227 = 0.03402 0.01748 0.00496 0.01721 F2 4 0.526158 0.831111 0.517054 11.00000 0.04003 0.06365 = 0.02679 0.02438 0.01621 0.02108 F3 4 0.529184 0.943616 0.617390 11.00000 0.04695 0.03410 = 0.04145 0.01581 0.01035 0.01276 C3 1 0.677593 0.758782 0.624893 11.00000 0.02272 0.03770 = 0.02254 0.00986 0.00967 0.00743 F4 4 0.732796 0.719975 0.679834 11.00000 0.02747 0.05255 = 0.02900 0.01579 0.00737 0.01808 F5 4 0.730707 0.857683 0.635195 11.00000 0.02397 0.04431 = 0.03631 0.01172 0.00918 -0.00362 F6 4 0.692721 0.699972 0.563361 11.00000 0.03446 0.04798 = 0.02872 0.00962 0.01829 0.01706 C4 1 0.478750 0.651019 0.588393 11.00000 0.03644 0.03507 = 0.02416 0.00005 0.00963 -0.00468 F7 4 0.538116 0.578410 0.616989 11.00000 0.07139 0.02569 = 0.04291 0.00509 0.01636 0.00004 F8 4 0.464599 0.623928 0.516538 11.00000 0.04988 0.05294 = 0.02196 -0.00861 0.00854 -0.00385 F9 4 0.373755 0.646187 0.600909 11.00000 0.03861 0.05869 = 0.04409 -0.00901 0.01784 -0.02184 RESI 0 RESI TFB 7 PART -1 10.5 F1 4 0.087894 0.308676 0.466421 10.50000 0.02437 0.02451 = 0.05734 0.00962 0.01694 0.00312 F2 4 -0.125929 0.347659 0.398397 10.50000 0.03317 0.02853 = 0.02867 0.00104 -0.00294 -0.00739 F3 4 -0.201673 0.542524 0.438899 10.50000 0.02021 0.03418 = 0.05029 0.01930 -0.00064 -0.00036 F4 4 -0.060278 0.697965 0.541715 10.50000 0.02881 0.02319 = 0.05952 -0.00212 0.02259 -0.00125 C1 1 0.052757 0.406131 0.488725 10.50000 0.02596 0.02112 = 0.02574 0.00744 0.00602 0.00369 C2 1 -0.056229 0.424318 0.452719 10.50000 0.02774 0.02622 = 0.01648 0.00354 -0.00012 -0.00261 C3 1 -0.095871 0.523057 0.472711 10.50000 0.01945 0.02971 = 0.02559 0.01216 0.00125 0.00071 C4 1 -0.022015 0.600093 0.526522 10.50000 0.02978 0.01944 = 0.02101 0.00367 0.00899 -0.00085 C5 1 0.086382 0.582078 0.561973 10.50000 0.02741 0.02486 = 0.01741 0.00454 0.00272 -0.00316 AFIX 43 H5 2 0.135044 0.636624 0.599843 10.50000 -1.20000 AFIX 0 C6 1 0.125438 0.482311 0.542048 10.50000 0.02532 0.02508 = 0.02248 0.00899 -0.00008 -0.00203 AFIX 43 H6 2 0.201438 0.468291 0.565463 10.50000 -1.20000 PART 0 RESI 0 AFIX 0 RESI CCF3 8 PART 1 31 O1 3 0.724720 0.877623 0.821287 31.00000 0.01932 0.02634 = 0.02353 0.00035 0.00351 -0.00583 C1 1 0.790985 0.971896 0.854333 31.00000 0.02132 0.02341 = 0.02128 0.00268 0.00732 -0.00462 C2 1 0.775665 1.048147 0.802430 31.00000 0.02702 0.03206 = 0.03565 0.01214 0.00411 0.00083 F1 4 0.839174 1.017182 0.752372 31.00000 0.05441 0.06314 = 0.03359 0.01916 0.02199 -0.00072 F2 4 0.816107 1.148768 0.836372 31.00000 0.04601 0.02460 = 0.05665 0.01510 0.00630 0.00093 F3 4 0.666380 1.043095 0.765165 31.00000 0.03604 0.04283 = 0.05287 0.01512 -0.00625 0.00920 C3 1 0.759300 1.024598 0.925538 31.00000 0.04858 0.04745 = 0.03282 -0.01236 0.02188 -0.02123 F4 4 0.739160 0.957940 0.962027 31.00000 0.11323 0.07591 = 0.03022 -0.00276 0.03445 -0.04623 F5 4 0.656235 1.069836 0.905974 31.00000 0.04701 0.06579 = 0.07433 -0.02713 0.03829 -0.00751 F6 4 0.840469 1.102026 0.967617 31.00000 0.05165 0.04570 = 0.03380 -0.01357 0.01369 -0.02077 C4 1 0.921386 0.948159 0.872843 31.00000 0.02503 0.03133 = 0.04833 0.00881 0.00166 -0.00276 F7 4 0.944304 0.908340 0.932722 31.00000 0.05939 0.04469 = 0.06036 0.02635 -0.02657 -0.01522 F8 4 0.995866 1.035209 0.888903 31.00000 0.02317 0.04001 = 0.06059 0.01521 0.00419 -0.00837 F9 4 0.944112 0.876881 0.821553 31.00000 0.02914 0.05237 = 0.07703 -0.00689 0.00740 0.01313 PART 0 RESI 0 RESI CCF3 9 PART 2 -31 O1 3 0.703027 0.884665 0.821421 -31.00000 0.02996 0.02779 = 0.02703 0.00179 0.00286 -0.00272 C1 1 0.780396 0.971538 0.855467 -31.00000 0.02943 0.03205 = 0.02996 0.00244 0.00605 -0.00539 C2 1 0.901564 0.948442 0.897623 -31.00000 0.03239 0.03659 = 0.04328 0.00660 -0.00223 -0.00756 F1 4 0.881368 0.928961 0.960696 -31.00000 0.05185 0.03787 = 0.03897 0.01148 -0.01141 -0.01211 F2 4 0.979553 1.033166 0.906068 -31.00000 0.03810 0.05335 = 0.04318 0.01559 -0.00873 -0.01920 F3 4 0.939801 0.867732 0.857159 -31.00000 0.03242 0.05225 = 0.06021 0.00773 0.00820 0.00287 C3 1 0.810770 1.032868 0.800466 -31.00000 0.04394 0.04251 = 0.03758 0.00918 0.00832 -0.00929 F4 4 0.709848 1.038274 0.754142 -31.00000 0.05587 0.05420 = 0.04586 0.01857 -0.00142 -0.01073 F5 4 0.897210 0.976362 0.776979 -31.00000 0.05638 0.05625 = 0.05310 0.00176 0.02727 -0.01287 F6 4 0.843320 1.135983 0.833888 -31.00000 0.04240 0.03726 = 0.05746 0.01482 0.01016 -0.00381 C4 1 0.724641 1.044697 0.910407 -31.00000 0.03871 0.03426 = 0.03407 -0.00418 0.00919 -0.00797 F7 4 0.655205 1.099493 0.867333 -31.00000 0.06359 0.04856 = 0.06535 0.00617 0.00844 0.02118 F8 4 0.803195 1.118138 0.959629 -31.00000 0.05165 0.04570 = 0.03380 -0.01357 0.01369 -0.02077 F9 4 0.683881 0.984717 0.947911 -31.00000 0.02767 0.02575 = 0.03276 -0.00957 0.01630 0.00003 PART 0 RESI 0 RESI CCF3 10 PART 1 21 O1 3 0.781771 0.540494 0.764521 21.00000 0.02064 0.02259 = 0.02458 0.00507 0.01088 0.00657 C1 1 0.859533 0.484294 0.735653 21.00000 0.01878 0.02221 = 0.02214 0.00379 0.00835 0.00637 C2 1 0.974137 0.559740 0.751195 21.00000 0.01957 0.02977 = 0.03454 0.00715 0.01005 0.00656 F1 4 1.033516 0.576004 0.820555 21.00000 0.02519 0.04539 = 0.03731 0.00419 -0.00005 0.00223 F2 4 1.044900 0.519655 0.709674 21.00000 0.02473 0.04902 = 0.04952 0.01310 0.02237 0.01077 F3 4 0.949554 0.653175 0.738160 21.00000 0.02576 0.02956 = 0.05951 0.01746 0.01251 0.00183 C3 1 0.808377 0.442339 0.651815 21.00000 0.02792 0.03190 = 0.02283 0.00318 0.01053 0.00755 F4 4 0.697402 0.402787 0.636328 21.00000 0.02833 0.04494 = 0.02698 -0.00155 0.00584 -0.00178 F5 4 0.812464 0.520113 0.617396 21.00000 0.04275 0.04743 = 0.02683 0.01562 0.01524 0.01035 F6 4 0.867185 0.364901 0.622793 21.00000 0.04102 0.04286 = 0.03055 -0.00308 0.01540 0.01447 C4 1 0.887865 0.387450 0.769961 21.00000 0.03647 0.02514 = 0.02870 0.00676 0.01462 0.01253 F7 4 0.802804 0.307346 0.740481 21.00000 0.05583 0.02258 = 0.04587 0.00816 0.01665 0.00252 F8 4 0.988342 0.349775 0.759149 21.00000 0.04747 0.04372 = 0.04539 0.01605 0.02165 0.03088 F9 4 0.898452 0.413162 0.840773 21.00000 0.05237 0.03622 = 0.02755 0.01368 0.01508 0.01983 PART 0 RESI 0 RESI CCF3 13 PART 2 -21 O1 3 0.777192 0.542169 0.759811 -21.00000 0.02696 0.02624 = 0.02682 0.00351 0.01427 0.01055 C1 1 0.855755 0.485758 0.731518 -21.00000 0.02416 0.02477 = 0.02807 0.00366 0.01313 0.00933 C2 1 0.896003 0.400232 0.774533 -21.00000 0.03615 0.03006 = 0.03456 0.00876 0.01448 0.01372 F1 4 0.972813 0.445272 0.838143 -21.00000 0.04261 0.03452 = 0.03628 0.00879 0.00865 0.01877 F2 4 0.945591 0.323376 0.737515 -21.00000 0.04150 0.03100 = 0.03680 0.01186 0.01705 0.01826 F3 4 0.804369 0.354240 0.789534 -21.00000 0.03853 0.03117 = 0.04510 0.01696 0.01886 0.01782 C3 1 0.797656 0.428896 0.650610 -21.00000 0.03128 0.02862 = 0.02725 0.00074 0.01316 0.01069 F4 4 0.735465 0.492808 0.614798 -21.00000 0.03529 0.03458 = 0.02910 0.00291 0.00868 0.01281 F5 4 0.724170 0.345074 0.646473 -21.00000 0.03502 0.03202 = 0.04393 0.00131 0.00825 0.00234 F6 4 0.881787 0.395389 0.618386 -21.00000 0.04026 0.03103 = 0.03353 -0.00100 0.02033 0.01481 C4 1 0.964359 0.561851 0.735845 -21.00000 0.02727 0.03596 = 0.03683 0.00762 0.01361 0.00329 F7 4 0.941256 0.618808 0.685618 -21.00000 0.03101 0.03700 = 0.04274 0.01229 0.01698 0.00318 F8 4 1.053020 0.503485 0.727508 -21.00000 0.02580 0.04162 = 0.04110 0.01010 0.01597 0.00483 F9 4 1.001005 0.629570 0.800922 -21.00000 0.02610 0.03890 = 0.04132 0.00327 0.01045 0.00073 PART 0 RESI 0 HKLF 4 REM p-1_a.res in P-1 REM wR2 = 0.0962, GooF = S = 1.032, Restrained GooF = 1.086 for all data REM R1 = 0.0382 for 15945 Fo > 4sig(Fo) and 0.0513 for all 19545 data REM 1265 parameters refined using 10839 restraints END WGHT 0.0361 3.5445 REM Highest difference peak 0.877, deepest hole -0.805, 1-sigma level 0.094 Q1 1 0.7430 1.0710 0.8291 11.00000 0.05 0.88 Q2 1 0.8545 0.9375 0.9798 11.00000 0.05 0.79 Q3 1 0.9400 0.9508 0.7887 11.00000 0.05 0.75 Q4 1 0.4529 0.7832 0.8113 11.00000 0.05 0.73 Q5 1 -0.0023 0.0387 0.6313 11.00000 0.05 0.68 Q6 1 0.2563 0.6868 0.7516 11.00000 0.05 0.68 Q7 1 0.0993 0.1314 0.6860 11.00000 0.05 0.67 Q8 1 0.4380 0.8978 0.5926 11.00000 0.05 0.65 Q9 1 0.6411 0.5936 0.6327 11.00000 0.05 0.63 Q10 1 0.8254 0.4662 0.6919 11.00000 0.05 0.63 Q11 1 0.6640 1.1078 0.8375 11.00000 0.05 0.62 Q12 1 0.7987 0.9904 0.9469 11.00000 0.05 0.62 Q13 1 -0.0483 -0.0492 0.4703 11.00000 0.05 0.61 Q14 1 0.7877 0.9645 0.7223 11.00000 0.05 0.60 Q15 1 0.9846 0.9890 0.8356 11.00000 0.05 0.58 Q16 1 0.8730 0.8320 0.8043 11.00000 0.05 0.56 Q17 1 -0.0035 0.0787 0.4915 11.00000 0.05 0.55 Q18 1 0.1613 0.8306 0.7731 11.00000 0.05 0.53 Q19 1 0.7531 0.5504 0.9883 11.00000 0.05 0.53 Q20 1 0.9092 0.9580 0.8355 11.00000 0.05 0.53 ; _shelx_res_checksum 4486 _shelx_hkl_file ; -1 0 0 269.57 13.50 -1 0 0 260.67 10.60 -1 0 0 281.67 9.50 -1 0 0 267.67 10.40 -1 0 0 251.67 13.10 -1 0 0 290.37 10.80 -1 0 0 260.97 10.40 -1 0 0 268.87 9.40 1 0 0 247.78 13.00 1 0 0 260.37 10.20 1 0 0 268.17 13.10 1 0 0 249.68 10.20 1 0 0 267.47 9.40 1 0 0 281.17 10.70 1 0 0 276.27 9.40 1 0 0 282.67 10.60 -2 0 0 1979.50 70.39 -2 0 0 1994.70 70.89 2 0 0 2077.89 70.79 2 0 0 2010.80 70.79 -4 0 0 1600.44 60.09 -4 0 0 1752.52 72.49 -4 0 0 1615.84 59.79 -4 0 0 1660.93 55.29 -4 0 0 1608.54 55.09 -4 0 0 1640.04 59.29 -4 0 0 1656.73 72.29 -4 0 0 1718.13 59.89 4 0 0 1748.33 59.69 4 0 0 1608.84 53.89 4 0 0 1698.43 56.89 4 0 0 1751.62 59.19 4 0 0 1715.63 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3219.58 112.89 6 -3 0 3428.56 123.39 6 -3 0 3287.17 113.19 6 -3 0 3510.15 161.58 -6 3 0 3345.37 122.39 -6 3 0 3295.27 137.69 -6 3 0 3294.17 117.69 -6 3 0 3290.77 138.39 -6 3 0 3368.56 126.69 -6 3 0 3476.55 121.79 -6 3 0 3319.37 124.29 -6 3 0 3333.67 124.79 -6 3 0 3163.18 126.19 -6 3 0 3409.06 118.39 5 -3 0 4184.28 148.89 5 -3 0 3914.91 146.39 5 -3 0 4299.27 160.18 5 -3 0 4487.45 160.78 -5 3 0 4380.56 151.78 -5 3 0 4254.37 160.48 -5 3 0 4310.97 143.89 -5 3 0 4303.67 144.69 -5 3 0 4328.97 142.29 -5 3 0 4173.48 148.09 -5 3 0 4413.96 149.59 -5 3 0 4448.65 142.79 -5 3 0 4157.08 158.88 -5 3 0 4234.08 151.58 4 -3 0 749.03 43.70 4 -3 0 812.82 36.50 4 -3 0 802.62 48.40 4 -3 0 778.42 36.10 4 -3 0 783.62 42.60 4 -3 0 869.71 44.00 4 -3 0 832.42 44.50 4 -3 0 683.03 46.80 -4 3 0 798.42 50.89 -4 3 0 734.03 44.00 -4 3 0 837.42 39.00 -4 3 0 760.12 47.70 -4 3 0 804.62 38.50 -4 3 0 822.02 38.60 -4 3 0 792.72 50.29 -4 3 0 817.22 38.00 -4 3 0 789.62 44.50 -4 3 0 770.12 48.10 3 -3 0 1585.14 69.99 3 -3 0 1658.33 66.69 3 -3 0 1674.53 60.89 3 -3 0 1671.43 71.59 3 -3 0 1699.93 67.39 3 -3 0 1686.03 61.09 3 -3 0 1602.54 69.39 3 -3 0 1687.03 69.39 -3 3 0 1694.03 60.19 -3 3 0 1721.63 69.99 -3 3 0 1649.54 69.99 -3 3 0 1712.73 60.69 -3 3 0 1618.34 66.09 -3 3 0 1540.85 69.99 -3 3 0 1764.72 67.29 -3 3 0 1542.75 69.29 2 -3 0 2601.74 84.59 2 -3 0 2530.75 92.79 2 -3 0 2462.85 90.69 2 -3 0 2553.34 84.39 2 -3 0 2532.75 93.59 2 -3 0 2508.15 90.69 -2 3 0 2507.15 92.99 -2 3 0 2408.76 88.09 -2 3 0 2459.85 89.99 -2 3 0 2487.05 88.59 -2 3 0 2566.94 85.19 -2 3 0 2461.85 91.99 -2 3 0 2532.95 90.79 1 -3 0 33.40 10.80 1 -3 0 33.30 8.50 1 -3 0 48.20 8.20 1 -3 0 62.89 7.50 1 -3 0 43.20 11.80 1 -3 0 44.20 8.80 1 -3 0 44.50 6.40 1 -3 0 51.59 8.40 1 -3 0 30.10 8.50 1 -3 0 42.10 8.90 -1 3 0 55.39 7.00 -1 3 0 33.60 6.80 -1 3 0 36.70 6.90 -1 3 0 35.40 7.30 -1 3 0 42.00 10.90 -1 3 0 33.20 9.00 -1 3 0 39.30 9.40 -1 3 0 59.99 7.60 -1 3 0 42.80 10.00 -1 3 0 39.40 8.10 0 -3 0 862.61 33.00 0 -3 0 885.01 33.60 0 -3 0 820.22 32.90 0 -3 0 900.71 36.30 0 -3 0 893.41 36.30 0 -3 0 833.72 40.90 0 -3 0 855.41 32.60 0 -3 0 848.52 32.90 0 -3 0 830.72 41.20 0 -3 0 839.52 33.20 0 3 0 827.42 31.50 0 3 0 852.71 32.10 0 3 0 878.41 31.70 0 3 0 831.62 34.90 0 3 0 881.91 41.10 0 3 0 901.31 31.90 0 3 0 849.81 35.10 0 3 0 801.92 39.60 -1 -3 0 266.47 13.70 -1 -3 0 273.07 14.50 -1 -3 0 264.37 16.10 -1 -3 0 314.27 22.20 -1 -3 0 288.37 16.30 -1 -3 0 282.87 14.00 -1 -3 0 287.57 17.00 -1 -3 0 273.27 15.90 -1 -3 0 255.07 21.00 -1 -3 0 282.37 14.40 1 3 0 285.27 16.80 1 3 0 257.97 14.40 1 3 0 268.57 16.90 1 3 0 273.27 13.60 1 3 0 294.47 20.90 1 3 0 269.77 13.60 1 3 0 233.58 13.90 -2 -3 0 395.26 20.90 -2 -3 0 377.26 17.00 -2 -3 0 399.36 23.40 -2 -3 0 410.56 18.60 -2 -3 0 422.66 26.20 -2 -3 0 401.96 24.00 -2 -3 0 371.96 18.00 -2 -3 0 397.26 21.20 -2 -3 0 409.26 26.30 -2 -3 0 392.56 17.00 2 3 0 405.96 24.00 2 3 0 388.56 23.30 -3 -3 0 2346.27 70.69 -3 -3 0 2294.87 83.49 -3 -3 0 2277.67 69.59 -3 -3 0 2222.48 82.39 -3 -3 0 2256.07 80.69 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26.10 -8 -3 0 104.59 12.70 -8 -3 0 128.69 21.40 -8 -3 0 111.19 15.70 -8 -3 0 72.39 22.70 -8 -3 0 110.29 15.80 -8 -3 0 85.59 11.60 8 3 0 80.19 20.20 8 3 0 88.69 21.50 -9 -3 0 52.69 15.30 -9 -3 0 36.80 12.40 -9 -3 0 35.50 9.20 -9 -3 0 26.60 10.20 -9 -3 0 64.29 15.90 -9 -3 0 58.59 11.20 -9 -3 0 39.10 17.10 -9 -3 0 20.90 13.60 9 3 0 30.70 19.30 -10 -3 0 339.47 36.70 -10 -3 0 265.87 43.90 -10 -3 0 257.37 42.40 -10 -3 0 275.07 20.50 -10 -3 0 308.37 35.60 -10 -3 0 257.07 20.40 -10 -3 0 258.47 37.50 -10 -3 0 280.97 40.30 -11 -3 0 170.88 39.20 -11 -3 0 179.18 21.50 -11 -3 0 177.58 21.00 -11 -3 0 201.28 29.90 -11 -3 0 141.99 33.30 -11 -3 0 150.08 37.10 -11 -3 0 182.38 28.20 -11 -3 0 140.09 34.30 -12 -3 0 338.07 34.70 -12 -3 0 422.56 72.89 -12 -3 0 297.87 38.70 -12 -3 0 337.47 40.60 -12 -3 0 347.07 36.00 -12 -3 0 291.57 37.30 -12 -3 0 332.77 38.70 -12 -3 0 337.07 65.19 -12 -3 0 338.47 35.90 -12 -3 0 327.57 35.50 -13 -3 0 760.92 42.90 -13 -3 0 827.52 53.29 -13 -3 0 779.12 48.70 -13 -3 0 673.13 50.09 -13 -3 0 739.63 48.80 -13 -3 0 786.12 50.79 -13 -3 0 740.03 50.29 -13 -3 0 739.53 42.30 -14 -3 0 675.33 82.39 -14 -3 0 603.94 39.80 -14 -3 0 598.94 39.40 -14 -3 0 653.63 46.40 -14 -3 0 639.24 45.80 -14 -3 0 635.54 45.90 -14 -3 0 564.44 44.70 -15 -3 0 248.58 34.20 -15 -3 0 162.98 25.90 -15 -3 0 124.29 34.20 -15 -3 0 194.98 31.30 -15 -3 0 215.28 34.00 -15 -3 0 122.89 34.00 -15 -3 0 191.18 30.90 -15 -3 0 178.08 27.10 -16 -3 0 382.16 65.49 -16 -3 0 495.85 43.30 -16 -3 0 376.46 43.80 -16 -3 0 331.87 44.00 -16 -3 0 332.47 46.50 -16 -3 0 475.25 71.09 17 -4 0 9.00 18.60 17 -4 0 -4.60 13.30 -17 4 0 -4.60 11.00 -17 4 0 -2.60 12.20 -17 4 0 -2.20 8.50 -17 4 0 -7.20 9.70 16 -4 0 111.49 24.00 16 -4 0 56.89 26.20 16 -4 0 38.90 25.50 16 -4 0 82.19 21.10 -16 4 0 64.59 27.10 -16 4 0 76.59 29.60 -16 4 0 36.70 19.20 -16 4 0 100.89 29.70 -16 4 0 94.49 26.60 -16 4 0 84.79 32.70 -16 4 0 99.49 28.30 -16 4 0 119.29 34.80 15 -4 0 17.10 11.70 15 -4 0 -2.80 8.50 15 -4 0 -15.20 14.20 15 -4 0 21.60 24.80 -15 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39.40 -12 4 0 269.27 38.90 -12 4 0 258.77 39.80 -12 4 0 235.48 49.99 11 -4 0 119.59 29.60 11 -4 0 137.49 27.30 11 -4 0 129.49 25.20 11 -4 0 172.48 27.60 11 -4 0 168.88 26.30 11 -4 0 217.78 32.40 11 -4 0 201.88 31.20 -11 4 0 147.39 25.70 -11 4 0 193.08 36.50 -11 4 0 103.29 43.10 -11 4 0 119.99 28.40 -11 4 0 238.78 44.60 -11 4 0 194.78 52.49 -11 4 0 146.19 29.40 -11 4 0 148.79 29.00 -11 4 0 108.79 27.80 -11 4 0 188.48 39.80 -11 4 0 146.29 26.70 -11 4 0 166.18 34.20 10 -4 0 96.59 23.30 10 -4 0 52.29 24.00 10 -4 0 68.99 26.00 10 -4 0 70.79 20.10 10 -4 0 75.89 21.40 10 -4 0 71.89 14.80 10 -4 0 53.49 13.30 10 -4 0 75.99 20.00 -10 4 0 62.99 20.30 -10 4 0 53.29 16.30 -10 4 0 145.59 39.00 -10 4 0 63.19 20.20 -10 4 0 85.39 26.10 -10 4 0 71.29 30.50 -10 4 0 72.79 18.10 -10 4 0 74.49 22.50 -10 4 0 59.69 18.90 -10 4 0 61.79 22.40 -10 4 0 75.79 20.50 -10 4 0 79.99 20.20 9 -4 0 1090.49 51.19 9 -4 0 1182.88 62.99 9 -4 0 1075.69 76.99 9 -4 0 1127.29 51.79 9 -4 0 981.50 76.19 9 -4 0 987.10 60.29 9 -4 0 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291.67 31.90 -5 -4 0 264.57 30.20 -5 -4 0 276.27 32.00 -5 -4 0 240.48 31.70 -5 -4 0 233.38 28.10 -5 -4 0 226.98 14.00 -6 -4 0 672.03 29.20 -6 -4 0 614.24 44.40 -6 -4 0 690.23 46.20 -6 -4 0 695.33 41.70 -6 -4 0 683.33 37.50 -6 -4 0 632.44 28.00 -6 -4 0 691.13 45.40 -6 -4 0 693.03 38.10 -6 -4 0 661.23 40.90 -6 -4 0 663.43 46.80 -7 -4 0 117.39 31.50 -7 -4 0 83.19 27.20 -7 -4 0 57.39 19.70 -7 -4 0 59.59 16.20 -7 -4 0 56.69 13.50 -7 -4 0 100.29 24.10 -7 -4 0 94.09 11.90 -7 -4 0 64.39 11.10 -7 -4 0 79.59 16.30 -7 -4 0 100.69 19.30 -8 -4 0 643.64 43.80 -8 -4 0 694.53 41.40 -8 -4 0 728.33 55.69 -8 -4 0 705.33 54.79 -8 -4 0 692.93 33.70 -8 -4 0 770.02 46.60 -8 -4 0 750.22 31.90 -8 -4 0 643.04 52.39 -8 -4 0 729.83 34.30 -8 -4 0 706.73 53.29 -8 -4 0 700.63 31.10 -8 -4 0 635.34 40.80 -9 -4 0 1181.68 62.39 -9 -4 0 1129.19 74.69 -9 -4 0 1113.09 85.69 -9 -4 0 1149.78 85.49 -9 -4 0 1263.27 76.09 -9 -4 0 1194.48 45.70 -9 -4 0 1184.08 45.60 -9 -4 0 1044.30 53.99 -9 -4 0 1087.79 60.39 -9 -4 0 1142.09 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1899.41 94.79 -11 7 0 1999.10 98.69 10 -7 0 1295.57 79.69 10 -7 0 1187.88 63.39 10 -7 0 1292.77 92.09 10 -7 0 1257.87 77.19 10 -7 0 1118.69 75.99 10 -7 0 993.20 72.69 10 -7 0 1409.86 96.69 10 -7 0 1257.37 64.19 -10 7 0 1127.09 87.39 -10 7 0 1235.98 79.49 -10 7 0 1447.16 86.09 -10 7 0 1205.18 72.99 -10 7 0 1219.28 79.59 -10 7 0 1260.67 82.99 -10 7 0 1274.07 72.49 -10 7 0 1167.78 90.39 -10 7 0 1276.97 71.29 -10 7 0 1345.57 75.49 9 -7 0 60.29 15.40 9 -7 0 28.90 20.50 9 -7 0 75.09 24.30 9 -7 0 91.99 27.20 9 -7 0 63.09 21.90 9 -7 0 31.10 20.70 9 -7 0 34.70 13.20 9 -7 0 46.90 21.80 -9 7 0 65.79 19.70 -9 7 0 83.89 24.10 -9 7 0 65.69 27.50 -9 7 0 63.49 23.50 -9 7 0 76.39 24.40 -9 7 0 43.60 21.00 -9 7 0 60.59 19.00 -9 7 0 52.99 21.10 -9 7 0 34.80 23.10 -9 7 0 59.89 27.50 8 -7 0 60.89 29.30 8 -7 0 24.40 16.40 8 -7 0 27.80 24.20 8 -7 0 29.70 13.20 8 -7 0 42.20 20.40 8 -7 0 36.30 15.40 8 -7 0 13.10 16.40 8 -7 0 12.90 16.70 -8 7 0 0.90 14.00 -8 7 0 55.39 22.10 -8 7 0 35.90 19.00 -8 7 0 22.10 12.20 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31.40 -4 -7 0 1459.45 75.79 -4 -7 0 1225.88 63.39 -4 -7 0 1386.66 58.29 -4 -7 0 1318.57 57.09 -4 -7 0 1295.87 52.59 -4 -7 0 1262.57 62.49 -4 -7 0 1237.88 53.89 -4 -7 0 1276.67 53.69 -4 -7 0 1221.18 51.89 -4 -7 0 1297.17 56.99 -4 -7 0 1347.67 74.99 -4 -7 0 1265.47 56.59 4 7 0 1253.87 62.99 4 7 0 1283.97 62.49 -5 -7 0 489.05 31.10 -5 -7 0 510.55 54.29 -5 -7 0 454.85 34.10 -5 -7 0 407.06 29.70 -5 -7 0 495.65 27.60 -5 -7 0 489.95 44.70 -5 -7 0 478.65 30.60 -5 -7 0 548.45 40.60 -5 -7 0 467.05 30.40 -5 -7 0 472.55 34.00 -5 -7 0 467.55 39.10 -5 -7 0 495.15 27.50 5 7 0 453.95 36.50 5 7 0 452.15 37.00 -6 -7 0 755.22 56.49 -6 -7 0 826.42 45.80 -6 -7 0 798.82 45.00 -6 -7 0 745.83 48.50 -6 -7 0 724.03 60.69 -6 -7 0 890.71 42.00 -6 -7 0 824.42 40.90 -6 -7 0 792.02 48.80 -6 -7 0 739.93 36.20 -6 -7 0 812.92 37.00 -6 -7 0 786.32 56.49 -6 -7 0 688.03 57.99 -7 -7 0 605.84 33.90 -7 -7 0 603.74 48.30 -7 -7 0 638.34 47.20 -7 -7 0 652.33 52.69 -7 -7 0 555.14 46.40 -7 -7 0 592.64 45.20 -7 -7 0 564.94 49.20 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372.46 54.49 -13 8 0 369.46 60.69 -13 8 0 385.76 51.49 -13 8 0 360.96 49.00 -13 8 0 323.07 52.69 -13 8 0 358.96 50.99 -13 8 0 324.97 56.89 12 -8 0 429.76 55.89 12 -8 0 384.96 50.59 12 -8 0 441.46 61.19 12 -8 0 341.97 63.69 12 -8 0 440.66 58.39 12 -8 0 266.57 53.89 -12 8 0 290.97 46.10 -12 8 0 427.06 69.19 -12 8 0 355.36 52.29 -12 8 0 314.27 46.80 -12 8 0 484.75 61.69 -12 8 0 430.46 72.79 -12 8 0 337.67 54.09 -12 8 0 474.35 58.49 -12 8 0 272.17 48.60 -12 8 0 347.07 55.09 11 -8 0 637.54 81.99 11 -8 0 671.33 59.89 11 -8 0 640.04 81.39 11 -8 0 645.84 47.20 11 -8 0 785.12 62.89 11 -8 0 673.83 47.90 -11 8 0 725.23 54.19 -11 8 0 635.64 55.39 -11 8 0 973.10 105.59 -11 8 0 707.23 84.39 -11 8 0 738.43 64.49 -11 8 0 630.94 103.69 -11 8 0 695.53 70.69 -11 8 0 715.03 76.29 -11 8 0 599.44 74.59 -11 8 0 699.43 54.99 -11 8 0 688.63 63.99 -11 8 0 675.93 56.99 10 -8 0 11.30 16.50 10 -8 0 49.50 21.70 10 -8 0 59.19 27.80 10 -8 0 34.80 24.60 10 -8 0 8.20 14.80 10 -8 0 29.90 19.30 -10 8 0 35.10 25.90 -10 8 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114.79 -6 10 -3 1762.12 102.19 -6 10 -3 1924.21 95.69 -6 10 -3 1887.81 86.19 -6 10 -3 1863.91 110.59 -6 10 -3 1822.72 94.29 6 -10 3 2019.50 102.29 6 -10 3 1950.20 106.49 6 -10 3 1729.83 101.79 6 -10 3 2006.60 116.19 6 -10 3 1869.11 101.29 6 -10 3 1829.42 111.49 -7 10 -3 1816.92 112.69 -7 10 -3 1978.00 99.49 -7 10 -3 1757.72 109.99 -7 10 -3 1833.12 105.99 -7 10 -3 1970.30 99.09 -7 10 -3 1875.71 104.59 -7 10 -3 1935.51 109.79 -7 10 -3 1832.72 103.59 -7 10 -3 1912.81 90.79 -7 10 -3 1911.11 89.29 7 -10 3 1907.61 107.69 7 -10 3 2023.40 108.79 7 -10 3 1954.60 107.89 7 -10 3 1786.92 89.29 7 -10 3 1789.02 89.49 7 -10 3 2023.80 117.19 7 -10 3 2008.40 115.59 7 -10 3 1893.21 105.19 -8 10 -3 995.90 105.39 -8 10 -3 884.51 59.09 -8 10 -3 828.52 75.69 -8 10 -3 956.30 65.79 -8 10 -3 945.91 75.29 -8 10 -3 898.01 64.79 -8 10 -3 771.12 66.09 -8 10 -3 788.92 66.29 -8 10 -3 851.71 74.59 -8 10 -3 836.92 56.69 8 -10 3 923.41 75.99 8 -10 3 861.11 57.19 8 -10 3 902.31 76.69 8 -10 3 896.01 71.09 8 -10 3 902.21 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323.87 42.40 0 8 -3 345.77 28.40 0 8 -3 342.27 28.60 0 -8 3 386.26 27.20 0 -8 3 247.98 34.40 0 -8 3 350.06 29.30 0 -8 3 359.76 44.50 0 -8 3 351.46 25.80 0 -8 3 333.37 40.30 0 -8 3 335.67 44.70 0 -8 3 350.56 28.90 -1 8 -3 269.87 36.50 -1 8 -3 333.97 29.30 -1 8 -3 237.28 34.80 -1 8 -3 307.17 24.00 -1 8 -3 266.67 28.10 -1 8 -3 356.46 41.80 -1 8 -3 297.67 24.60 -1 8 -3 323.57 27.90 -1 8 -3 430.56 45.30 -1 8 -3 316.47 26.90 1 -8 3 356.76 29.50 1 -8 3 324.17 24.20 1 -8 3 296.47 23.20 1 -8 3 304.97 24.50 1 -8 3 397.46 45.00 1 -8 3 463.25 57.99 1 -8 3 314.87 24.40 1 -8 3 348.37 36.70 1 -8 3 475.55 58.39 1 -8 3 321.77 40.00 -2 8 -3 703.93 56.49 -2 8 -3 672.23 41.20 -2 8 -3 740.23 45.00 -2 8 -3 644.04 41.50 -2 8 -3 713.63 43.60 -2 8 -3 691.43 48.20 -2 8 -3 709.33 48.70 -2 8 -3 783.62 45.90 -2 8 -3 680.13 40.40 -2 8 -3 749.33 56.89 2 -8 3 764.22 40.00 2 -8 3 858.31 61.89 2 -8 3 751.32 42.50 2 -8 3 655.13 41.40 2 -8 3 740.33 59.89 2 -8 3 733.83 38.50 2 -8 3 801.32 53.09 2 -8 3 702.83 43.30 2 -8 3 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15.00 4 8 -28 24.90 24.10 -4 -8 28 1.50 7.40 -4 -8 28 -2.10 14.20 -4 -8 28 38.70 25.20 -4 -8 28 1.60 7.40 3 8 -28 -16.30 13.10 3 8 -28 0.80 18.30 3 8 -28 16.20 19.20 3 8 -28 33.30 24.90 3 8 -28 7.90 14.50 3 8 -28 12.10 17.30 -3 -8 28 10.50 17.40 -3 -8 28 -4.10 15.80 2 8 -28 102.19 37.40 2 8 -28 88.99 32.50 2 8 -28 65.69 29.50 2 8 -28 93.99 32.50 2 8 -28 109.09 35.20 2 8 -28 129.59 38.90 -2 -8 28 103.39 35.10 -2 -8 28 57.19 26.50 1 8 -28 1.00 18.80 1 8 -28 7.90 15.10 1 8 -28 7.10 16.50 1 8 -28 21.60 25.20 1 8 -28 24.00 20.70 1 8 -28 14.90 18.20 7 7 -28 22.40 27.10 7 7 -28 -1.00 22.80 7 7 -28 13.30 24.80 7 7 -28 -12.80 19.10 7 7 -28 17.80 24.00 7 7 -28 -11.80 11.20 -7 -7 28 0.10 7.10 -7 -7 28 -2.90 7.70 6 7 -28 28.80 19.50 6 7 -28 -5.00 22.90 6 7 -28 11.50 19.60 6 7 -28 53.89 44.90 6 7 -28 4.90 28.20 -6 -7 28 -2.60 6.60 -6 -7 28 5.50 11.20 5 7 -28 6.80 16.10 5 7 -28 2.00 17.90 5 7 -28 -26.40 19.80 5 7 -28 32.60 26.30 5 7 -28 29.70 24.60 5 7 -28 13.50 32.50 -5 -7 28 -0.10 8.10 -5 -7 28 -5.00 7.20 4 7 -28 49.30 26.90 4 7 -28 9.40 23.40 4 7 -28 22.10 22.80 4 7 -28 20.60 27.70 4 7 -28 25.30 26.40 4 7 -28 -8.80 12.20 -4 -7 28 -0.60 7.80 -4 -7 28 6.50 10.50 3 7 -28 -1.60 14.90 3 7 -28 12.80 20.30 3 7 -28 37.70 29.10 3 7 -28 0.80 16.30 3 7 -28 7.90 17.80 3 7 -28 -16.30 11.70 -3 -7 28 2.30 15.50 -3 -7 28 -6.00 11.40 2 7 -28 9.00 19.30 2 7 -28 15.40 17.10 2 7 -28 16.20 16.70 2 7 -28 26.40 22.60 2 7 -28 18.40 20.70 2 7 -28 15.10 18.40 -2 -7 28 12.60 17.60 -2 -7 28 -4.50 12.10 1 7 -28 67.49 32.40 1 7 -28 66.19 35.90 1 7 -28 102.89 60.79 1 7 -28 101.29 34.20 1 7 -28 52.89 25.70 1 7 -28 13.00 23.90 -1 -7 28 53.19 30.50 -1 -7 28 -4.10 17.70 0 7 -28 78.99 29.60 0 7 -28 62.29 30.80 0 7 -28 115.29 36.60 0 7 -28 113.59 37.80 8 6 -28 -4.70 13.50 8 6 -28 49.50 26.90 8 6 -28 23.60 26.40 8 6 -28 26.60 28.00 8 6 -28 1.50 17.40 8 6 -28 19.70 19.00 -8 -6 28 1.00 13.40 -8 -6 28 4.20 13.90 7 6 -28 48.30 27.40 7 6 -28 -8.50 16.60 7 6 -28 -4.20 16.80 7 6 -28 -0.40 14.50 7 6 -28 0.70 22.50 7 6 -28 44.80 34.70 -7 -6 28 -4.80 7.20 -7 -6 28 -1.20 6.80 6 6 -28 22.40 28.70 6 6 -28 1.40 16.00 6 6 -28 7.40 30.80 6 6 -28 -5.40 14.10 6 6 -28 -19.40 20.60 6 6 -28 12.70 25.90 -6 -6 28 -0.90 6.80 -6 -6 28 -1.50 7.30 5 6 -28 89.69 42.50 5 6 -28 123.49 49.70 5 6 -28 80.69 30.70 5 6 -28 121.89 45.20 5 6 -28 164.58 46.60 4 6 -28 6.50 15.80 4 6 -28 7.00 20.70 4 6 -28 -12.10 18.80 4 6 -28 14.50 17.30 4 6 -28 31.90 21.30 4 6 -28 12.50 18.90 -4 -6 28 1.60 8.80 -4 -6 28 1.70 8.20 3 6 -28 -3.20 15.60 3 6 -28 -13.60 14.70 3 6 -28 -2.90 14.80 3 6 -28 -8.30 14.30 3 6 -28 3.00 19.30 3 6 -28 -13.10 11.30 2 6 -28 112.69 38.30 2 6 -28 66.79 31.40 2 6 -28 61.39 27.40 2 6 -28 79.59 37.10 2 6 -28 35.40 26.40 2 6 -28 117.99 38.30 1 6 -28 43.50 24.30 1 6 -28 86.59 37.80 1 6 -28 35.40 24.40 1 6 -28 32.40 20.50 1 6 -28 42.80 28.80 1 6 -28 58.99 27.40 -1 -6 28 7.80 19.70 -1 -6 28 26.80 23.20 0 6 -28 125.89 44.40 0 6 -28 58.79 35.90 0 6 -28 118.69 46.80 0 6 -28 77.79 30.60 0 6 -28 131.69 61.69 0 6 -28 80.99 31.10 0 -6 28 154.78 44.40 0 -6 28 158.28 41.00 8 5 -28 12.00 18.90 8 5 -28 18.70 20.10 8 5 -28 29.80 26.40 8 5 -28 36.90 27.80 8 5 -28 49.10 28.60 8 5 -28 16.60 30.20 -8 -5 28 -7.30 7.30 -8 -5 28 -5.00 6.70 7 5 -28 30.50 24.40 7 5 -28 41.10 28.50 7 5 -28 25.30 29.40 7 5 -28 27.20 26.90 7 5 -28 -1.40 13.80 7 5 -28 -34.50 16.90 -7 -5 28 -3.80 6.70 -7 -5 28 13.40 14.30 6 5 -28 1.90 18.70 6 5 -28 -12.40 23.70 6 5 -28 -5.10 13.80 6 5 -28 -43.50 13.70 6 5 -28 32.70 21.10 6 5 -28 -1.70 13.30 -6 -5 28 -3.20 9.10 -6 -5 28 6.20 10.20 5 5 -28 82.89 39.30 5 5 -28 52.19 33.50 5 5 -28 100.69 33.50 5 5 -28 72.09 30.30 5 5 -28 87.09 33.20 5 5 -28 112.09 35.90 4 5 -28 -9.90 9.60 4 5 -28 22.30 28.10 4 5 -28 23.90 19.20 4 5 -28 15.90 18.50 4 5 -28 12.60 25.80 4 5 -28 17.00 25.00 3 5 -28 98.89 38.70 3 5 -28 138.59 41.70 3 5 -28 56.59 28.30 3 5 -28 60.89 32.70 3 5 -28 110.99 38.80 3 5 -28 17.40 25.60 2 5 -28 54.09 32.30 2 5 -28 36.80 30.90 2 5 -28 32.80 23.90 2 5 -28 16.40 17.80 2 5 -28 37.00 28.80 2 5 -28 26.50 26.00 1 5 -28 209.78 45.30 1 5 -28 226.78 45.60 1 5 -28 198.18 45.90 1 5 -28 176.98 43.10 1 5 -28 309.97 66.29 1 5 -28 196.68 54.89 0 5 -28 74.79 31.50 0 5 -28 90.19 43.90 0 5 -28 133.49 39.30 0 5 -28 72.29 28.80 0 5 -28 106.79 46.30 0 5 -28 111.29 31.90 8 4 -28 27.50 25.80 8 4 -28 15.40 32.30 8 4 -28 12.90 18.40 8 4 -28 29.00 23.30 8 4 -28 76.19 44.10 -8 -4 28 -6.40 7.20 -8 -4 28 -2.30 8.40 7 4 -28 28.60 36.20 7 4 -28 58.09 34.90 7 4 -28 45.00 37.20 7 4 -28 31.10 26.40 7 4 -28 91.69 36.00 7 4 -28 113.59 41.10 6 4 -28 6.30 16.50 6 4 -28 3.00 23.90 6 4 -28 82.79 35.40 6 4 -28 34.50 23.10 6 4 -28 19.80 29.90 6 4 -28 17.70 20.20 -6 -4 28 -6.80 6.40 -6 -4 28 -6.50 6.10 5 4 -28 0.60 18.10 5 4 -28 0.20 27.50 5 4 -28 26.90 20.60 5 4 -28 -5.90 12.40 5 4 -28 7.20 17.10 5 4 -28 45.70 38.80 -5 -4 28 -7.20 7.30 -5 -4 28 -4.20 7.00 4 4 -28 159.58 42.80 4 4 -28 177.38 41.70 4 4 -28 185.18 51.59 4 4 -28 179.98 54.19 4 4 -28 183.58 49.00 4 4 -28 159.58 44.40 3 4 -28 273.37 56.99 3 4 -28 218.58 55.09 3 4 -28 188.38 49.90 3 4 -28 141.39 45.60 3 4 -28 197.28 47.60 3 4 -28 180.88 40.80 2 4 -28 365.46 63.99 2 4 -28 261.07 50.29 2 4 -28 227.08 60.79 2 4 -28 236.88 54.69 2 4 -28 234.08 44.40 2 4 -28 359.36 72.09 1 4 -28 218.18 45.80 1 4 -28 274.47 58.29 1 4 -28 225.58 58.39 1 4 -28 244.58 51.19 1 4 -28 258.77 51.79 1 4 -28 229.18 58.89 0 4 -28 319.07 56.99 0 4 -28 249.97 46.70 0 4 -28 299.37 59.49 0 4 -28 265.27 52.79 0 4 -28 155.08 37.50 0 4 -28 332.37 58.99 8 3 -28 23.40 27.90 8 3 -28 32.00 22.90 8 3 -28 17.50 21.70 8 3 -28 68.19 37.60 -8 -3 28 -8.50 7.90 -8 -3 28 -7.50 7.50 7 3 -28 51.09 31.40 7 3 -28 92.99 37.50 7 3 -28 25.90 24.70 7 3 -28 10.70 18.20 7 3 -28 24.30 32.20 7 3 -28 69.69 45.50 -7 -3 28 6.90 11.50 -7 -3 28 -11.30 7.00 6 3 -28 143.79 40.60 6 3 -28 179.48 58.59 6 3 -28 210.98 52.29 6 3 -28 159.48 45.60 6 3 -28 191.98 56.89 6 3 -28 185.38 44.00 5 3 -28 285.77 53.59 5 3 -28 341.17 61.49 5 3 -28 206.48 57.29 5 3 -28 274.57 65.09 5 3 -28 262.07 53.49 5 3 -28 230.58 50.19 4 3 -28 320.47 75.59 4 3 -28 279.47 57.69 4 3 -28 272.57 53.69 4 3 -28 243.08 52.99 4 3 -28 264.67 53.89 4 3 -28 383.96 77.09 3 3 -28 132.89 42.90 3 3 -28 128.79 37.20 3 3 -28 124.09 37.90 3 3 -28 140.59 41.40 3 3 -28 127.89 41.90 3 3 -28 165.78 47.00 2 3 -28 79.99 30.20 2 3 -28 143.09 41.20 2 3 -28 129.59 57.19 2 3 -28 140.29 51.89 2 3 -28 64.69 26.60 2 3 -28 155.08 42.30 1 3 -28 231.68 49.20 1 3 -28 226.28 56.99 1 3 -28 247.18 50.19 1 3 -28 188.78 44.80 1 3 -28 176.48 49.70 1 3 -28 279.57 49.99 0 3 -28 75.99 28.60 0 3 -28 104.09 38.20 0 3 -28 106.19 37.30 0 3 -28 88.79 34.10 0 3 -28 96.29 35.20 0 3 -28 69.29 31.40 8 2 -28 7.30 16.30 8 2 -28 23.70 17.80 8 2 -28 16.80 16.00 8 2 -28 -27.20 34.70 8 2 -28 -0.50 13.90 8 2 -28 -15.20 47.80 8 2 -28 19.70 24.20 8 2 -28 27.90 25.80 -8 -2 28 -9.00 7.20 -8 -2 28 -6.30 8.70 7 2 -28 366.86 105.09 7 2 -28 667.43 130.69 7 2 -28 329.07 59.49 7 2 -28 454.95 71.39 6 2 -28 15.90 17.80 6 2 -28 36.20 32.90 6 2 -28 26.80 24.90 6 2 -28 44.90 24.10 6 2 -28 63.19 28.00 6 2 -28 58.39 37.90 5 2 -28 407.86 68.99 5 2 -28 278.17 53.19 5 2 -28 301.17 77.29 5 2 -28 289.87 57.69 5 2 -28 217.38 48.10 5 2 -28 283.57 71.99 4 2 -28 443.06 67.39 4 2 -28 382.36 68.29 4 2 -28 528.35 75.59 4 2 -28 260.97 56.49 4 2 -28 416.26 63.99 4 2 -28 414.66 59.39 3 2 -28 191.78 45.80 3 2 -28 217.58 92.59 3 2 -28 345.97 109.99 3 2 -28 141.09 43.70 3 2 -28 241.68 56.69 3 2 -28 145.59 36.20 2 2 -28 170.98 43.50 2 2 -28 204.18 66.49 2 2 -28 264.17 51.29 2 2 -28 129.89 53.29 2 2 -28 103.29 31.90 2 2 -28 198.68 45.50 1 2 -28 81.79 28.80 1 2 -28 37.00 23.30 1 2 -28 53.89 31.50 1 2 -28 55.99 28.10 1 2 -28 4.00 15.90 1 2 -28 35.80 23.00 8 1 -28 22.00 33.90 8 1 -28 23.60 21.90 8 1 -28 38.40 24.20 8 1 -28 33.60 23.30 8 1 -28 25.50 25.50 8 1 -28 26.00 19.00 8 1 -28 25.20 25.80 8 1 -28 122.99 55.99 7 1 -28 591.14 72.99 7 1 -28 376.86 63.89 7 1 -28 460.25 90.49 7 1 -28 606.24 79.29 7 1 -28 524.95 77.39 7 1 -28 442.46 63.19 7 1 -28 463.95 63.39 7 1 -28 467.95 91.69 6 1 -28 350.06 54.29 6 1 -28 395.86 62.39 6 1 -28 382.16 93.19 6 1 -28 363.56 97.99 5 1 -28 56.59 36.50 5 1 -28 189.38 42.40 5 1 -28 149.09 60.09 5 1 -28 256.67 47.80 5 1 -28 194.38 47.00 5 1 -28 167.78 44.30 4 1 -28 99.19 43.10 4 1 -28 59.79 35.00 4 1 -28 97.79 35.50 4 1 -28 60.39 25.10 4 1 -28 100.89 30.40 4 1 -28 56.79 35.10 3 1 -28 148.59 37.20 3 1 -28 251.97 51.59 3 1 -28 148.99 41.80 3 1 -28 105.49 36.50 3 1 -28 189.38 52.49 3 1 -28 219.68 55.39 2 1 -28 22.20 21.00 2 1 -28 26.80 21.60 2 1 -28 15.00 19.80 2 1 -28 15.60 17.70 2 1 -28 33.50 22.50 2 1 -28 12.10 23.60 1 1 -28 13.10 19.70 1 1 -28 57.99 33.20 1 1 -28 38.40 34.70 1 1 -28 43.00 21.70 1 1 -28 140.59 65.19 1 1 -28 70.79 25.40 7 0 -28 316.97 55.79 7 0 -28 282.37 50.89 7 0 -28 250.27 62.59 7 0 -28 289.07 63.49 7 0 -28 446.36 76.89 7 0 -28 267.97 56.49 7 0 -28 308.57 50.89 7 0 -28 274.77 52.79 6 0 -28 20.50 38.40 6 0 -28 46.80 23.40 6 0 -28 2.90 15.60 6 0 -28 68.59 26.60 6 0 -28 68.89 28.90 6 0 -28 16.80 19.10 6 0 -28 -22.10 25.40 5 0 -28 251.07 47.60 5 0 -28 195.18 57.49 5 0 -28 194.08 39.20 5 0 -28 174.28 54.89 4 0 -28 194.28 55.99 4 0 -28 302.27 50.49 4 0 -28 172.58 41.40 4 0 -28 177.98 55.59 4 0 -28 284.77 49.80 4 0 -28 248.88 50.59 3 0 -28 38.70 31.00 3 0 -28 69.79 34.50 3 0 -28 154.68 36.90 3 0 -28 130.19 36.80 3 0 -28 117.29 45.30 2 0 -28 -1.70 19.20 2 0 -28 26.50 17.80 2 0 -28 14.80 22.30 2 0 -28 10.90 24.10 2 0 -28 11.30 15.50 2 0 -28 -22.20 12.00 5 -1 -28 88.39 31.80 5 -1 -28 103.59 35.70 5 -1 -28 25.50 36.60 5 -1 -28 86.19 30.30 5 -1 -28 103.69 31.70 5 -1 -28 75.49 43.80 5 -1 -28 82.89 28.60 4 -1 -28 -12.80 20.20 4 -1 -28 3.10 13.60 4 -1 -28 11.80 13.70 4 -1 -28 1.00 24.50 5 5 -29 387.26 84.29 5 5 -29 383.16 86.09 5 5 -29 275.17 56.99 5 5 -29 283.97 55.99 5 5 -29 262.67 53.99 5 5 -29 275.67 55.29 4 5 -29 124.19 45.90 4 5 -29 150.98 40.80 4 5 -29 196.48 47.50 4 5 -29 129.69 38.20 4 5 -29 192.68 59.49 4 5 -29 160.88 44.60 3 5 -29 99.29 35.50 3 5 -29 181.48 61.89 3 5 -29 158.78 41.60 3 5 -29 187.78 47.20 5 4 -29 122.59 38.50 5 4 -29 121.09 36.30 5 4 -29 152.58 39.60 5 4 -29 112.59 37.50 4 4 -29 158.28 43.50 4 4 -29 241.98 50.19 4 4 -29 338.17 61.79 4 4 -29 181.08 47.00 3 4 -29 133.49 46.30 3 4 -29 156.48 46.20 3 4 -29 141.39 40.70 3 4 -29 53.59 25.50 3 4 -29 175.38 45.70 3 4 -29 133.89 44.10 5 3 -29 176.18 42.20 5 3 -29 259.57 70.09 5 3 -29 180.38 45.50 5 3 -29 229.68 57.19 5 3 -29 249.18 68.79 5 3 -29 234.78 48.70 4 3 -29 120.19 34.60 4 3 -29 251.37 58.39 4 3 -29 241.88 61.69 4 3 -29 231.28 52.59 4 3 -29 170.68 54.89 4 3 -29 194.18 45.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 92025 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_p-1_a_CCDC4 _database_code_depnum_ccdc_archive 'CCDC 2151852' loop_ _audit_author_name _audit_author_address 'Malte Sellin' ;Albert Ludwigs Universaet Freiburg Germany ; _audit_update_record ; 2022-02-14 deposited with the CCDC. 2022-07-07 downloaded from the CCDC. ; _vrf_PLAT601_p-1_a ; PROBLEM: Unit Cell Contains Solvent Accessible VOIDS of . 75 Ang**3 RESPONSE: very small fraction of n-pentane crystallized at position of disordered 1,2,3,4-tetrafluorobenzene. ; _audit_creation_method ; FinalCif V98 by Daniel Kratzert, Freiburg 2022, https://dkratzert.de/finalcif.html ; _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_sum 'C46 H2 Ag Al F40 O28 Ru6' _chemical_formula_moiety 'C16 Al F36 O4, C24 Ag O24 Ru6, C6 H2 F4' _chemical_formula_weight 2503.75 _chemical_melting_point ? _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.349(6) _cell_length_b 12.385(4) _cell_length_c 23.041(10) _cell_angle_alpha 90.85(2) _cell_angle_beta 94.031(10) _cell_angle_gamma 93.152(13) _cell_volume 3509(3) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9152 _cell_measurement_theta_min 2.269 _cell_measurement_theta_max 30.631 _exptl_crystal_description needle _exptl_crystal_colour red _exptl_crystal_recrystallization_method 'diffusion of n-pentane in 1,2,3,4-tetrafluorobenzene' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 2.369 _exptl_crystal_F_000 2372 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 1.728 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6579 _exptl_absorpt_correction_T_max 0.7465 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_absorpt_special_details ? _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_ambient_environment N~2~ _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'mirror optics' _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _diffrn_measurement_ambient_temperature_device_make ? _diffrn_radiation_probe x-ray _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_source_current 1.4 _diffrn_detector CPAD _diffrn_detector_type 'Bruker PHOTON III' _diffrn_detector_area_resol_mean 7.41 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE dual wavelength Mo/Cu' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_reflns_number 206219 _diffrn_reflns_av_unetI/netI 0.0574 _diffrn_reflns_av_R_equivalents 0.0858 _diffrn_reflns_theta_min 1.647 _diffrn_reflns_theta_max 33.213 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -35 _diffrn_reflns_limit_l_max 35 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 26616 _reflns_number_gt 20242 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker BIS V6.2.14 Patch 4/2020-11-09' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0309P)^2^+11.0821P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_number_reflns 26616 _refine_ls_number_parameters 1444 _refine_ls_number_restraints 7259 _refine_ls_R_factor_all 0.0723 _refine_ls_R_factor_gt 0.0495 _refine_ls_wR_factor_ref 0.1053 _refine_ls_wR_factor_gt 0.0955 _refine_ls_goodness_of_fit_ref 1.070 _refine_ls_restrained_S_all 0.972 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 1.145 _refine_diff_density_min -2.015 _refine_diff_density_rms 0.185 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ag1 Ag 0.05726(2) 0.25665(2) 0.73575(2) 0.01517(5) Uani 1 1 d . . . . . Ru1 Ru 0.15023(2) 0.23809(2) 0.62449(2) 0.01413(5) Uani 1 1 d . . . . . Ru2 Ru 0.00509(2) 0.25179(2) 0.52223(2) 0.01462(6) Uani 1 1 d . . . . . Ru3 Ru -0.08667(2) 0.27526(2) 0.63245(2) 0.01484(6) Uani 1 1 d . . . . . Ru4 Ru 0.08477(2) 0.13598(2) 0.84151(2) 0.01675(6) Uani 1 1 d . . . . . Ru5 Ru 0.11425(2) 0.25808(3) 0.94906(2) 0.02125(7) Uani 1 1 d . . . . . Ru6 Ru 0.08350(2) 0.37869(2) 0.84418(2) 0.01513(6) Uani 1 1 d . . . . . Al1 Al 0.45140(8) 0.24574(9) 0.28418(5) 0.01426(19) Uani 1 1 d . . . . . O4 O 0.1084(2) -0.0084(2) 0.60476(13) 0.0245(6) Uani 1 1 d . . . . . O5 O 0.1225(2) 0.4768(2) 0.51767(12) 0.0237(6) Uani 1 1 d . . . . . O6 O 0.1438(3) 0.1896(3) 0.42359(14) 0.0365(8) Uani 1 1 d . . . . . O7 O -0.1102(2) 0.0255(2) 0.52519(13) 0.0237(6) Uani 1 1 d . . . . . O8 O -0.1809(3) 0.3052(3) 0.43377(17) 0.0425(9) Uani 1 1 d . . . . . O9 O -0.0507(2) 0.5197(2) 0.61142(12) 0.0231(6) Uani 1 1 d . . . . . O10 O -0.2053(2) 0.3288(3) 0.74046(13) 0.0303(7) Uani 1 1 d . . . . . O11 O -0.3020(2) 0.2689(3) 0.55782(14) 0.0314(7) Uani 1 1 d . . . . . O12 O -0.1081(2) 0.0312(2) 0.65717(13) 0.0233(6) Uani 1 1 d . . . . . O13 O -0.1584(2) 0.3726(2) 0.86982(13) 0.0262(6) Uani 1 1 d . . . . . O14 O 0.1268(3) 0.5787(3) 0.92340(14) 0.0324(7) Uani 1 1 d . . . . . O2 O 0.3189(2) 0.1938(3) 0.72400(12) 0.0261(6) Uani 1 1 d . . . . . O1 O 0.1814(2) 0.4831(2) 0.64991(13) 0.0231(6) Uani 1 1 d . . . . . O15 O 0.0238(2) 0.5236(2) 0.74155(12) 0.0227(6) Uani 1 1 d . . . . . O16 O 0.3227(2) 0.3804(2) 0.81275(14) 0.0266(6) Uani 1 1 d . . . . . O17 O -0.1288(3) 0.2015(3) 0.96161(15) 0.0380(8) Uani 1 1 d . . . . . O18 O 0.1109(3) 0.4373(3) 1.04103(14) 0.0416(8) Uani 1 1 d . . . . . O19 O 0.1637(3) 0.0666(3) 1.02710(16) 0.0517(10) Uani 1 1 d . . . . . O20 O 0.3594(2) 0.3170(3) 0.94397(15) 0.0371(8) Uani 1 1 d . . . . . O21 O -0.1663(2) 0.1361(3) 0.82962(15) 0.0325(7) Uani 1 1 d . . . . . O22 O 0.0799(3) -0.0652(3) 0.91650(15) 0.0363(8) Uani 1 1 d . . . . . O23 O 0.0876(2) -0.0127(2) 0.73442(13) 0.0276(6) Uani 1 1 d . . . . . O24 O 0.3357(2) 0.1422(2) 0.85025(13) 0.0266(6) Uani 1 1 d . . . . . O3 O 0.3292(2) 0.2475(3) 0.53905(13) 0.0299(7) Uani 1 1 d . . . . . C1 C 0.1659(3) 0.3938(3) 0.63953(15) 0.0169(7) Uani 1 1 d . . . . . C2 C 0.2507(3) 0.2120(3) 0.69060(15) 0.0183(7) Uani 1 1 d . . . . . C3 C 0.2618(3) 0.2427(3) 0.56955(16) 0.0207(7) Uani 1 1 d . . . . . C4 C 0.1193(3) 0.0822(3) 0.61145(15) 0.0185(7) Uani 1 1 d . . . . . C5 C 0.0773(3) 0.3955(3) 0.52263(16) 0.0180(7) Uani 1 1 d . . . . . C6 C 0.0949(3) 0.2112(3) 0.46102(17) 0.0231(8) Uani 1 1 d . . . . . C7 C -0.0648(3) 0.1081(3) 0.52728(15) 0.0172(6) Uani 1 1 d . . . . . C8 C -0.1136(3) 0.2874(3) 0.46783(19) 0.0264(8) Uani 1 1 d . . . . . C9 C -0.0600(3) 0.4296(3) 0.61830(16) 0.0181(7) Uani 1 1 d . . . . . C10 C -0.1548(3) 0.3070(3) 0.70370(17) 0.0196(7) Uani 1 1 d . . . . . C11 C -0.2212(3) 0.2716(3) 0.58463(18) 0.0227(7) Uani 1 1 d . . . . . C12 C -0.0964(3) 0.1201(3) 0.64690(16) 0.0196(7) Uani 1 1 d . . . . . C13 C -0.0696(3) 0.3693(3) 0.86088(16) 0.0199(7) Uani 1 1 d . . . . . C14 C 0.1112(3) 0.5030(4) 0.89481(17) 0.0234(8) Uani 1 1 d . . . . . C15 C 0.0477(3) 0.4630(3) 0.77607(16) 0.0185(7) Uani 1 1 d . . . . . C16 C 0.2357(3) 0.3758(3) 0.82590(16) 0.0185(7) Uani 1 1 d . . . . . C17 C -0.0411(3) 0.2228(4) 0.95381(18) 0.0285(9) Uani 1 1 d . . . . . C18 C 0.1121(3) 0.3716(4) 1.00713(19) 0.0303(9) Uani 1 1 d . . . . . C19 C 0.1465(4) 0.1388(4) 0.9991(2) 0.0351(10) Uani 1 1 d . . . . . C20 C 0.2692(3) 0.2954(4) 0.94256(17) 0.0270(8) Uani 1 1 d . . . . . C21 C -0.0741(3) 0.1401(3) 0.83511(18) 0.0247(8) Uani 1 1 d . . . . . C22 C 0.0823(3) 0.0112(4) 0.88956(19) 0.0273(9) Uani 1 1 d . . . . . C23 C 0.0840(3) 0.0500(3) 0.77079(17) 0.0200(7) Uani 1 1 d . . . . . C24 C 0.2439(3) 0.1453(3) 0.84734(16) 0.0201(7) Uani 1 1 d . . . . . O1_2 O 0.3480(6) 0.2267(11) 0.2286(5) 0.0173(15) Uani 0.718(5) 1 d D U P A 1 C1_2 C 0.2439(5) 0.2438(5) 0.2114(3) 0.0167(11) Uani 0.718(5) 1 d D U P A 1 C2_2 C 0.2220(4) 0.3664(4) 0.2117(2) 0.0230(10) Uani 0.718(5) 1 d D U P A 1 F1_2 F 0.3063(5) 0.4240(5) 0.1944(3) 0.0305(14) Uani 0.718(5) 1 d D U P A 1 F2_2 F 0.1342(4) 0.3894(4) 0.1771(3) 0.0296(12) Uani 0.718(5) 1 d D U P A 1 F3_2 F 0.2058(3) 0.4027(3) 0.26498(18) 0.0279(9) Uani 0.718(5) 1 d D U P A 1 C3_2 C 0.1635(4) 0.1839(4) 0.2506(2) 0.0239(11) Uani 0.718(5) 1 d D U P A 1 F4_2 F 0.1573(6) 0.0777(5) 0.2381(3) 0.0349(15) Uani 0.718(5) 1 d D U P A 1 F5_2 F 0.1962(9) 0.1981(8) 0.3062(3) 0.0342(18) Uani 0.718(5) 1 d D U P A 1 F6_2 F 0.0629(4) 0.2186(6) 0.2429(2) 0.0324(13) Uani 0.718(5) 1 d D U P A 1 C4_2 C 0.2245(4) 0.1994(5) 0.1477(2) 0.0232(10) Uani 0.718(5) 1 d D U P A 1 F7_2 F 0.2668(6) 0.1043(6) 0.1425(3) 0.0302(13) Uani 0.718(5) 1 d D U P A 1 F8_2 F 0.1184(3) 0.1865(3) 0.13087(16) 0.0326(9) Uani 0.718(5) 1 d D U P A 1 F9_2 F 0.2715(5) 0.2656(5) 0.1104(2) 0.0318(12) Uani 0.718(5) 1 d D U P A 1 O1_3 O 0.4462(9) 0.1514(6) 0.3379(5) 0.0226(13) Uani 0.805(5) 1 d D U P A 1 C1_3 C 0.4729(4) 0.0529(5) 0.3577(2) 0.0215(8) Uani 0.805(5) 1 d D U P A 1 C2_3 C 0.5988(5) 0.0489(5) 0.3704(3) 0.0308(10) Uani 0.805(5) 1 d D U P A 1 F1_3 F 0.6411(3) 0.1404(3) 0.3943(2) 0.0419(10) Uani 0.805(5) 1 d D U P A 1 F2_3 F 0.6258(6) -0.0308(4) 0.4066(2) 0.0452(14) Uani 0.805(5) 1 d D U P A 1 F3_3 F 0.6477(3) 0.0330(3) 0.32138(18) 0.0375(8) Uani 0.805(5) 1 d D U P A 1 C3_3 C 0.4329(4) -0.0378(5) 0.3132(3) 0.0285(10) Uani 0.805(5) 1 d D U P A 1 F4_3 F 0.3246(3) -0.0562(3) 0.31251(19) 0.0396(9) Uani 0.805(5) 1 d D U P A 1 F5_3 F 0.4550(3) -0.0092(3) 0.25966(16) 0.0400(9) Uani 0.805(5) 1 d D U P A 1 F6_3 F 0.4776(4) -0.1320(4) 0.3245(3) 0.0423(11) Uani 0.805(5) 1 d D U P A 1 C4_3 C 0.4170(5) 0.0354(5) 0.4152(3) 0.0253(9) Uani 0.805(5) 1 d D U P A 1 F7_3 F 0.3144(3) 0.0625(4) 0.40958(17) 0.0360(9) Uani 0.805(5) 1 d D U P A 1 F8_3 F 0.4166(4) -0.0678(4) 0.4317(2) 0.0408(12) Uani 0.805(5) 1 d D U P A 1 F9_3 F 0.4667(4) 0.0963(3) 0.45839(15) 0.0417(9) Uani 0.805(5) 1 d D U P A 1 O1_4 O 0.3458(14) 0.236(3) 0.2332(14) 0.021(4) Uani 0.282(5) 1 d D U P A 2 C1_4 C 0.2388(12) 0.2398(9) 0.2167(5) 0.019(2) Uani 0.282(5) 1 d D U P A 2 C2_4 C 0.2217(9) 0.3278(9) 0.1706(5) 0.026(2) Uani 0.282(5) 1 d D U P A 2 F1_4 F 0.2493(12) 0.2945(13) 0.1186(6) 0.031(3) Uani 0.282(5) 1 d D U P A 2 F2_4 F 0.1178(9) 0.3529(12) 0.1642(7) 0.035(3) Uani 0.282(5) 1 d D U P A 2 F3_4 F 0.2819(14) 0.4187(13) 0.1827(9) 0.035(3) Uani 0.282(5) 1 d D U P A 2 C3_4 C 0.1739(9) 0.2660(9) 0.2702(5) 0.025(2) Uani 0.282(5) 1 d D U P A 2 F4_4 F 0.2134(19) 0.2115(18) 0.3154(7) 0.027(4) Uani 0.282(5) 1 d D U P A 2 F5_4 F 0.1859(8) 0.3704(8) 0.2852(5) 0.031(2) Uani 0.282(5) 1 d D U P A 2 F6_4 F 0.0672(10) 0.2405(15) 0.2619(6) 0.033(3) Uani 0.282(5) 1 d D U P A 2 C4_4 C 0.1960(9) 0.1273(9) 0.1907(5) 0.026(2) Uani 0.282(5) 1 d D U P A 2 F7_4 F 0.1839(17) 0.0570(14) 0.2335(8) 0.041(4) Uani 0.282(5) 1 d D U P A 2 F8_4 F 0.1001(7) 0.1328(10) 0.1606(5) 0.044(3) Uani 0.282(5) 1 d D U P A 2 F9_4 F 0.2666(17) 0.0877(16) 0.1567(7) 0.033(4) Uani 0.282(5) 1 d D U P A 2 F1_6 F 0.5717(4) 0.1962(4) -0.1843(2) 0.0620(15) Uani 0.746(6) 1 d D U P B 1 F2_6 F 0.6286(4) 0.1110(4) -0.0788(3) 0.0593(15) Uani 0.746(6) 1 d D U P B 1 F3_6 F 0.6652(4) 0.2423(5) 0.0166(2) 0.0580(15) Uani 0.746(6) 1 d D U P B 1 F4_6 F 0.6465(4) 0.4585(5) 0.0074(2) 0.0536(13) Uani 0.746(6) 1 d D U P B 1 C1_6 C 0.5891(6) 0.2616(7) -0.1371(3) 0.0372(16) Uani 0.746(6) 1 d D U P B 1 C2_6 C 0.6177(6) 0.2189(6) -0.0834(3) 0.0386(14) Uani 0.746(6) 1 d D U P B 1 C3_6 C 0.6369(5) 0.2852(6) -0.0356(3) 0.0364(14) Uani 0.746(6) 1 d D U P B 1 C4_6 C 0.6267(5) 0.3949(5) -0.0408(3) 0.0313(12) Uani 0.746(6) 1 d D U P B 1 C5_6 C 0.5972(6) 0.4383(6) -0.0940(3) 0.0364(15) Uani 0.746(6) 1 d D U P B 1 H5_6 H 0.589779 0.513974 -0.097302 0.044 Uiso 0.746(6) 1 calc R U P B 1 C6_6 C 0.5785(7) 0.3712(7) -0.1422(4) 0.0365(17) Uani 0.746(6) 1 d D U P B 1 H6_6 H 0.558283 0.400525 -0.179022 0.044 Uiso 0.746(6) 1 calc R U P B 1 O1_8 O 0.451(3) 0.154(2) 0.3410(17) 0.019(4) Uani 0.195(5) 1 d D U P A 2 C1_8 C 0.4737(12) 0.0547(16) 0.3609(7) 0.022(2) Uani 0.195(5) 1 d D U P A 2 C2_8 C 0.4444(13) -0.0332(15) 0.3130(7) 0.029(2) Uani 0.195(5) 1 d D U P A 2 F1_8 F 0.5171(13) -0.0307(12) 0.2728(6) 0.039(3) Uani 0.195(5) 1 d D U P A 2 F2_8 F 0.4417(14) -0.1330(14) 0.3340(9) 0.037(3) Uani 0.195(5) 1 d D U P A 2 F3_8 F 0.3473(11) -0.0187(12) 0.2859(7) 0.036(3) Uani 0.195(5) 1 d D U P A 2 C3_8 C 0.4064(12) 0.0316(14) 0.4143(7) 0.025(2) Uani 0.195(5) 1 d D U P A 2 F4_8 F 0.4077(12) 0.1178(10) 0.4496(5) 0.031(2) Uani 0.195(5) 1 d D U P A 2 F5_8 F 0.3029(9) 0.0044(13) 0.3981(6) 0.030(3) Uani 0.195(5) 1 d D U P A 2 F6_8 F 0.4444(14) -0.0496(13) 0.4456(7) 0.023(3) Uani 0.195(5) 1 d D U P A 2 C4_8 C 0.5970(13) 0.0543(14) 0.3804(7) 0.028(2) Uani 0.195(5) 1 d D U P A 2 F7_8 F 0.6181(10) 0.1102(11) 0.4301(6) 0.035(3) Uani 0.195(5) 1 d D U P A 2 F8_8 F 0.630(2) -0.0457(14) 0.3879(9) 0.029(3) Uani 0.195(5) 1 d D U P A 2 F9_8 F 0.6593(9) 0.0991(12) 0.3416(7) 0.035(3) Uani 0.195(5) 1 d D U P A 2 F1_5 F 0.6027(11) 0.5265(10) -0.0770(7) 0.061(4) Uani 0.254(6) 1 d D U P B 2 F2_5 F 0.6475(14) 0.3930(19) 0.0145(7) 0.093(6) Uani 0.254(6) 1 d D U P B 2 F3_5 F 0.6445(13) 0.1713(17) -0.0050(8) 0.086(5) Uani 0.254(6) 1 d D U P B 2 F4_5 F 0.5996(15) 0.0885(13) -0.1120(11) 0.093(6) Uani 0.254(6) 1 d D U P B 2 C1_5 C 0.6024(14) 0.4179(13) -0.0840(8) 0.044(4) Uani 0.254(6) 1 d D U P B 2 C2_5 C 0.6246(13) 0.3500(13) -0.0390(7) 0.048(3) Uani 0.254(6) 1 d D U P B 2 C3_5 C 0.6223(13) 0.2403(12) -0.0486(7) 0.046(3) Uani 0.254(6) 1 d D U P B 2 C4_5 C 0.5996(14) 0.1977(13) -0.1038(7) 0.046(3) Uani 0.254(6) 1 d D U P B 2 C5_5 C 0.5772(18) 0.2660(16) -0.1484(9) 0.042(4) Uani 0.254(6) 1 d D U P B 2 H5_5 H 0.560342 0.236920 -0.186547 0.051 Uiso 0.254(6) 1 calc R U P B 2 C6_5 C 0.5784(18) 0.3758(17) -0.1394(9) 0.039(4) Uani 0.254(6) 1 d D U P B 2 H6_5 H 0.562747 0.422254 -0.170965 0.047 Uiso 0.254(6) 1 calc R U P B 2 O1_7 O 0.5715(2) 0.2317(2) 0.25167(12) 0.0199(5) Uani 1 1 d D U . . . C1_7 C 0.6328(3) 0.2493(3) 0.20591(15) 0.0194(7) Uani 1 1 d D U . . . C2_7 C 0.5819(3) 0.3311(3) 0.16292(16) 0.0246(8) Uani 1 1 d D U . . . F1_7 F 0.5034(2) 0.2832(2) 0.12725(11) 0.0319(6) Uani 1 1 d D U . . . F2_7 F 0.6558(2) 0.3785(2) 0.12999(11) 0.0337(6) Uani 1 1 d D U . . . F3_7 F 0.5380(2) 0.4096(2) 0.19210(11) 0.0299(5) Uani 1 1 d D U . . . C3_7 C 0.7473(3) 0.2964(3) 0.23018(17) 0.0259(8) Uani 1 1 d D U . . . F4_7 F 0.7817(2) 0.2451(2) 0.27742(11) 0.0332(6) Uani 1 1 d D U . . . F5_7 F 0.7414(2) 0.4014(2) 0.24488(12) 0.0344(6) Uani 1 1 d D U . . . F6_7 F 0.8225(2) 0.2902(3) 0.19146(12) 0.0370(6) Uani 1 1 d D U . . . C4_7 C 0.6446(3) 0.1403(3) 0.17390(18) 0.0276(8) Uani 1 1 d D U . . . F7_7 F 0.7100(2) 0.0775(2) 0.20569(13) 0.0392(7) Uani 1 1 d D U . . . F8_7 F 0.6874(2) 0.1534(3) 0.12257(12) 0.0419(7) Uani 1 1 d D U . . . F9_7 F 0.5497(2) 0.0862(2) 0.16405(13) 0.0371(6) Uani 1 1 d D U . . . O1_9 O 0.4357(2) 0.3715(2) 0.31522(12) 0.0203(5) Uani 1 1 d D U . . . C1_9 C 0.4668(3) 0.4428(3) 0.35891(15) 0.0168(6) Uani 1 1 d D U . . . C2_9 C 0.4939(3) 0.5548(3) 0.33146(16) 0.0217(7) Uani 1 1 d D U . . . F1_9 F 0.59056(19) 0.5537(2) 0.30796(11) 0.0303(6) Uani 1 1 d D U . . . F2_9 F 0.4997(2) 0.6366(2) 0.36992(12) 0.0339(6) Uani 1 1 d D U . . . F3_9 F 0.4207(2) 0.5757(2) 0.28905(11) 0.0299(5) Uani 1 1 d D U . . . C3_9 C 0.3714(3) 0.4544(3) 0.39908(17) 0.0240(7) Uani 1 1 d D U . . . F4_9 F 0.3261(2) 0.3579(2) 0.41041(13) 0.0378(6) Uani 1 1 d D U . . . F5_9 F 0.29297(19) 0.5103(2) 0.37242(12) 0.0322(6) Uani 1 1 d D U . . . F6_9 F 0.4028(2) 0.5056(2) 0.44902(11) 0.0348(6) Uani 1 1 d D U . . . C4_9 C 0.5685(3) 0.4080(3) 0.39650(16) 0.0201(7) Uani 1 1 d D U . . . F7_9 F 0.5406(2) 0.3355(2) 0.43584(11) 0.0302(6) Uani 1 1 d D U . . . F8_9 F 0.62265(19) 0.4910(2) 0.42506(10) 0.0266(5) Uani 1 1 d D U . . . F9_9 F 0.63605(18) 0.3627(2) 0.36229(10) 0.0247(5) Uani 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ag1 0.01697(11) 0.01570(12) 0.01295(11) 0.00074(9) 0.00091(8) 0.00191(9) Ru1 0.01472(11) 0.01582(13) 0.01197(12) -0.00002(10) 0.00065(9) 0.00240(9) Ru2 0.01924(12) 0.01202(12) 0.01239(12) 0.00079(9) -0.00115(9) 0.00162(9) Ru3 0.01435(11) 0.01556(13) 0.01462(12) 0.00032(10) -0.00009(9) 0.00234(9) Ru4 0.01764(12) 0.01699(14) 0.01574(13) 0.00396(10) 0.00104(9) 0.00135(10) Ru5 0.02181(13) 0.02985(17) 0.01267(13) 0.00291(12) 0.00193(10) 0.00525(12) Ru6 0.01617(11) 0.01636(13) 0.01302(12) -0.00020(10) 0.00230(9) 0.00094(10) Al1 0.0153(4) 0.0132(5) 0.0142(5) 0.0002(4) 0.0004(3) 0.0015(4) O4 0.0297(14) 0.0203(14) 0.0236(14) 0.0001(11) 0.0001(11) 0.0040(11) O5 0.0299(14) 0.0180(13) 0.0223(14) 0.0031(11) -0.0035(11) 0.0002(11) O6 0.061(2) 0.0238(16) 0.0270(16) 0.0020(13) 0.0188(15) 0.0027(15) O7 0.0305(14) 0.0155(13) 0.0250(14) -0.0010(11) 0.0039(11) -0.0019(11) O8 0.048(2) 0.0237(17) 0.051(2) 0.0023(15) -0.0290(17) 0.0008(14) O9 0.0258(13) 0.0184(14) 0.0250(14) -0.0005(11) 0.0006(10) 0.0011(10) O10 0.0259(14) 0.0437(19) 0.0230(14) 0.0009(13) 0.0057(11) 0.0114(13) O11 0.0265(14) 0.0286(17) 0.0371(17) -0.0053(14) -0.0119(12) 0.0020(12) O12 0.0236(13) 0.0198(14) 0.0267(14) 0.0042(11) 0.0026(10) 0.0005(10) O13 0.0230(13) 0.0279(16) 0.0284(15) 0.0047(12) 0.0059(11) 0.0025(11) O14 0.0361(16) 0.0338(18) 0.0267(16) -0.0131(14) 0.0041(12) -0.0024(13) O2 0.0216(13) 0.0389(18) 0.0177(13) -0.0033(12) -0.0026(10) 0.0081(12) O1 0.0215(12) 0.0208(14) 0.0268(14) -0.0024(11) 0.0019(10) -0.0002(10) O15 0.0287(13) 0.0189(13) 0.0206(13) 0.0025(11) 0.0014(10) 0.0037(11) O16 0.0211(13) 0.0248(15) 0.0346(16) -0.0008(13) 0.0075(11) 0.0010(11) O17 0.0301(16) 0.052(2) 0.0326(17) 0.0163(16) 0.0068(13) 0.0031(15) O18 0.047(2) 0.057(2) 0.0210(16) -0.0086(16) 0.0028(14) 0.0123(17) O19 0.070(3) 0.054(3) 0.0331(19) 0.0201(18) -0.0012(18) 0.018(2) O20 0.0253(15) 0.053(2) 0.0325(17) -0.0090(16) -0.0009(12) 0.0007(14) O21 0.0219(13) 0.0309(17) 0.0446(19) 0.0043(15) 0.0003(12) 0.0022(12) O22 0.0384(17) 0.0312(18) 0.0384(18) 0.0200(15) -0.0027(14) -0.0042(13) O23 0.0350(15) 0.0202(14) 0.0268(15) -0.0010(12) -0.0042(12) 0.0035(12) O24 0.0240(13) 0.0252(15) 0.0307(16) -0.0014(12) 0.0013(11) 0.0047(11) O3 0.0314(15) 0.0350(18) 0.0251(15) 0.0049(13) 0.0098(12) 0.0065(13) C1 0.0138(14) 0.0224(18) 0.0149(15) 0.0001(13) 0.0023(11) 0.0021(12) C2 0.0190(15) 0.0217(18) 0.0141(15) -0.0024(13) 0.0010(12) 0.0024(13) C3 0.0234(16) 0.0212(18) 0.0181(17) 0.0025(14) 0.0032(13) 0.0045(14) C4 0.0198(15) 0.0220(18) 0.0138(15) -0.0005(13) -0.0002(12) 0.0035(13) C5 0.0220(16) 0.0138(16) 0.0176(16) -0.0003(13) -0.0038(12) 0.0038(13) C6 0.038(2) 0.0150(17) 0.0162(17) 0.0000(14) 0.0047(14) -0.0018(15) C7 0.0209(15) 0.0159(16) 0.0147(15) -0.0006(13) 0.0001(12) 0.0023(13) C8 0.0301(19) 0.0157(18) 0.031(2) 0.0040(16) -0.0120(16) -0.0021(15) C9 0.0162(14) 0.0208(18) 0.0173(16) -0.0010(13) -0.0003(12) 0.0040(13) C10 0.0141(14) 0.0224(18) 0.0220(17) 0.0007(14) -0.0015(12) 0.0023(13) C11 0.0214(16) 0.0171(18) 0.029(2) -0.0039(15) -0.0022(14) 0.0043(14) C12 0.0139(14) 0.0248(19) 0.0202(17) -0.0004(14) 0.0014(12) 0.0016(13) C13 0.0229(16) 0.0187(18) 0.0187(17) 0.0012(14) 0.0040(13) 0.0019(13) C14 0.0206(16) 0.029(2) 0.0205(18) -0.0010(16) 0.0024(13) 0.0014(15) C15 0.0199(15) 0.0188(17) 0.0169(16) -0.0029(13) 0.0027(12) 0.0008(13) C16 0.0203(15) 0.0156(17) 0.0195(17) -0.0008(13) 0.0014(12) 0.0000(13) C17 0.0268(19) 0.037(2) 0.0229(19) 0.0078(18) 0.0031(15) 0.0058(17) C18 0.029(2) 0.039(3) 0.025(2) -0.0007(19) 0.0069(16) 0.0073(18) C19 0.038(2) 0.043(3) 0.025(2) 0.010(2) 0.0004(17) 0.008(2) C20 0.0284(19) 0.034(2) 0.0178(18) -0.0025(16) -0.0023(14) 0.0049(17) C21 0.0301(19) 0.0202(19) 0.0240(19) 0.0045(15) 0.0016(15) 0.0011(15) C22 0.0232(17) 0.030(2) 0.029(2) 0.0097(17) 0.0011(15) -0.0013(15) C23 0.0198(15) 0.0165(17) 0.0227(18) 0.0034(14) -0.0036(13) -0.0007(13) C24 0.0233(16) 0.0198(18) 0.0171(16) -0.0010(14) 0.0003(13) 0.0024(14) O1_2 0.018(2) 0.021(3) 0.013(3) -0.003(2) -0.0001(18) 0.003(2) C1_2 0.017(2) 0.019(2) 0.013(2) -0.0013(19) -0.0014(18) -0.0007(19) C2_2 0.021(2) 0.024(2) 0.025(2) 0.0029(19) -0.0007(18) 0.0031(18) F1_2 0.029(3) 0.023(2) 0.039(4) 0.009(2) -0.001(2) -0.0008(18) F2_2 0.029(2) 0.027(3) 0.033(3) 0.005(2) -0.0046(17) 0.0091(18) F3_2 0.030(2) 0.026(2) 0.028(2) -0.0077(16) -0.0031(15) 0.0066(16) C3_2 0.025(2) 0.028(3) 0.019(2) 0.001(2) 0.0030(18) -0.0031(19) F4_2 0.042(3) 0.025(3) 0.038(3) 0.008(2) 0.003(2) -0.006(2) F5_2 0.038(4) 0.044(3) 0.021(3) 0.007(2) 0.002(2) -0.002(2) F6_2 0.0208(17) 0.044(3) 0.033(3) 0.004(2) 0.0083(18) -0.0024(17) C4_2 0.023(2) 0.031(3) 0.014(2) -0.0014(19) 0.0005(17) -0.0035(19) F7_2 0.041(2) 0.028(3) 0.021(3) -0.012(2) -0.007(2) 0.004(2) F8_2 0.0251(16) 0.047(2) 0.0239(18) -0.0042(17) -0.0078(13) -0.0014(15) F9_2 0.029(3) 0.047(3) 0.021(2) 0.011(2) 0.0051(16) 0.006(2) O1_3 0.024(3) 0.0201(19) 0.025(3) 0.0090(18) 0.003(2) 0.0064(18) C1_3 0.0203(17) 0.0172(19) 0.0274(19) 0.0057(15) 0.0012(15) 0.0033(15) C2_3 0.0229(18) 0.021(2) 0.049(3) 0.0099(18) 0.0012(17) 0.0060(16) F1_3 0.0279(16) 0.0275(17) 0.069(3) 0.0022(17) -0.0068(17) -0.0017(13) F2_3 0.031(2) 0.037(2) 0.067(4) 0.025(2) -0.007(3) 0.0109(19) F3_3 0.0245(15) 0.0267(19) 0.063(2) 0.0077(16) 0.0129(14) 0.0059(14) C3_3 0.0255(19) 0.022(2) 0.038(2) -0.0017(17) 0.0085(18) -0.0004(16) F4_3 0.0257(15) 0.039(2) 0.053(2) -0.0102(18) 0.0037(14) -0.0058(13) F5_3 0.049(2) 0.037(2) 0.0347(18) -0.0085(15) 0.0129(16) -0.0033(17) F6_3 0.037(2) 0.0206(16) 0.072(3) -0.0025(17) 0.017(2) 0.0034(16) C4_3 0.0277(19) 0.023(2) 0.026(2) 0.0086(16) 0.0032(16) 0.0030(17) F7_3 0.0279(15) 0.045(2) 0.037(2) 0.0120(18) 0.0100(13) 0.0062(15) F8_3 0.049(3) 0.0296(19) 0.045(3) 0.0223(19) 0.006(2) -0.0014(17) F9_3 0.054(2) 0.044(2) 0.0257(16) 0.0061(15) -0.0044(15) -0.0027(18) O1_4 0.021(5) 0.023(8) 0.019(8) -0.006(6) -0.003(5) 0.005(5) C1_4 0.019(4) 0.023(4) 0.013(4) 0.003(3) -0.004(4) -0.002(4) C2_4 0.024(4) 0.029(5) 0.024(4) 0.009(4) 0.003(4) 0.005(4) F1_4 0.025(6) 0.050(8) 0.019(4) 0.010(4) 0.003(4) 0.005(5) F2_4 0.027(5) 0.048(9) 0.031(7) 0.015(6) -0.002(4) 0.014(5) F3_4 0.036(7) 0.029(5) 0.039(7) 0.016(4) -0.012(6) 0.003(4) C3_4 0.021(4) 0.032(5) 0.020(4) 0.002(4) -0.002(3) 0.003(4) F4_4 0.020(6) 0.048(8) 0.015(5) 0.008(6) 0.004(4) 0.010(6) F5_4 0.024(4) 0.038(5) 0.034(6) -0.007(4) 0.003(4) 0.008(4) F6_4 0.019(4) 0.055(8) 0.025(7) 0.003(6) 0.006(4) -0.002(4) C4_4 0.033(5) 0.029(5) 0.015(4) -0.003(4) -0.003(3) -0.011(4) F7_4 0.059(11) 0.030(7) 0.034(6) 0.008(5) 0.011(6) -0.013(6) F8_4 0.029(4) 0.061(7) 0.036(5) -0.008(5) -0.010(4) -0.020(4) F9_4 0.048(6) 0.028(6) 0.025(8) 0.002(5) 0.008(6) 0.002(5) F1_6 0.065(3) 0.068(3) 0.050(3) -0.019(2) 0.003(2) -0.006(3) F2_6 0.072(4) 0.038(3) 0.069(4) 0.010(3) 0.015(3) 0.003(2) F3_6 0.070(3) 0.075(4) 0.033(2) 0.023(2) 0.011(2) 0.025(3) F4_6 0.060(3) 0.061(3) 0.039(2) -0.014(2) 0.002(2) 0.004(3) C1_6 0.029(3) 0.047(3) 0.034(3) -0.001(3) 0.000(3) -0.003(3) C2_6 0.035(3) 0.043(3) 0.038(3) 0.004(3) 0.007(3) 0.000(3) C3_6 0.036(3) 0.044(3) 0.031(3) 0.010(2) 0.007(2) 0.004(3) C4_6 0.028(3) 0.035(3) 0.030(3) -0.001(2) 0.005(2) -0.002(2) C5_6 0.031(3) 0.040(4) 0.039(3) 0.005(3) 0.003(3) 0.002(3) C6_6 0.027(3) 0.050(3) 0.031(3) 0.004(3) 0.001(3) -0.001(3) O1_8 0.024(8) 0.020(5) 0.014(8) 0.003(5) 0.003(7) 0.004(5) C1_8 0.021(3) 0.021(4) 0.025(4) 0.006(3) 0.002(3) 0.003(3) C2_8 0.030(4) 0.025(4) 0.034(4) -0.002(3) 0.004(3) 0.004(4) F1_8 0.046(5) 0.039(6) 0.035(5) -0.002(4) 0.014(5) 0.015(5) F2_8 0.037(7) 0.025(4) 0.049(7) 0.001(4) 0.004(6) 0.003(5) F3_8 0.035(4) 0.034(6) 0.038(6) -0.005(5) -0.006(4) 0.001(4) C3_8 0.025(4) 0.028(4) 0.022(4) 0.008(3) 0.002(3) -0.001(4) F4_8 0.037(6) 0.035(4) 0.021(4) 0.004(4) -0.005(4) 0.010(4) F5_8 0.021(4) 0.032(6) 0.037(6) 0.013(5) 0.003(4) 0.000(4) F6_8 0.028(6) 0.030(5) 0.012(5) 0.005(4) -0.001(4) -0.002(5) C4_8 0.022(4) 0.021(4) 0.042(5) 0.010(4) 0.000(3) 0.003(4) F7_8 0.021(5) 0.032(5) 0.051(5) 0.000(4) -0.007(4) 0.001(4) F8_8 0.026(6) 0.024(4) 0.037(7) 0.012(4) -0.005(6) 0.008(4) F9_8 0.020(4) 0.030(6) 0.058(6) 0.022(5) 0.008(4) 0.009(4) F1_5 0.061(8) 0.054(6) 0.069(9) -0.008(6) 0.011(7) -0.002(6) F2_5 0.111(12) 0.111(12) 0.052(7) -0.013(8) -0.003(8) -0.020(12) F3_5 0.094(10) 0.096(11) 0.073(9) 0.045(9) 0.023(8) 0.000(9) F4_5 0.088(12) 0.048(7) 0.143(16) -0.007(8) -0.001(12) 0.010(8) C1_5 0.036(7) 0.052(6) 0.044(6) -0.004(5) 0.012(6) -0.003(6) C2_5 0.039(7) 0.061(6) 0.042(6) 0.001(5) 0.002(6) -0.005(7) C3_5 0.035(7) 0.060(6) 0.044(6) 0.009(5) 0.007(6) -0.001(6) C4_5 0.041(7) 0.046(6) 0.051(6) 0.008(5) 0.002(6) 0.005(6) C5_5 0.039(8) 0.052(6) 0.036(7) 0.001(5) 0.000(6) -0.002(6) C6_5 0.032(8) 0.049(6) 0.037(6) 0.005(6) 0.010(7) -0.001(7) O1_7 0.0176(11) 0.0223(14) 0.0207(13) 0.0010(11) 0.0051(9) 0.0033(10) C1_7 0.0196(15) 0.0207(17) 0.0183(16) -0.0025(13) 0.0031(12) 0.0022(13) C2_7 0.0290(18) 0.026(2) 0.0187(17) -0.0002(14) 0.0055(13) -0.0002(15) F1_7 0.0316(12) 0.0400(15) 0.0232(12) 0.0020(11) -0.0034(10) 0.0015(11) F2_7 0.0384(14) 0.0368(15) 0.0272(13) 0.0073(11) 0.0116(10) 0.0001(11) F3_7 0.0375(13) 0.0222(12) 0.0315(13) 0.0053(10) 0.0082(10) 0.0078(10) C3_7 0.0200(16) 0.032(2) 0.0254(19) -0.0029(16) 0.0050(13) -0.0040(15) F4_7 0.0250(12) 0.0415(16) 0.0320(14) 0.0024(12) -0.0038(10) -0.0011(11) F5_7 0.0335(13) 0.0286(14) 0.0399(15) -0.0089(12) 0.0039(11) -0.0094(11) F6_7 0.0224(11) 0.0535(18) 0.0355(15) -0.0034(13) 0.0108(10) -0.0040(11) C4_7 0.0309(19) 0.028(2) 0.0235(19) -0.0083(16) 0.0024(15) 0.0035(16) F7_7 0.0438(15) 0.0294(15) 0.0452(17) -0.0070(12) -0.0019(12) 0.0174(12) F8_7 0.0516(17) 0.0488(18) 0.0270(14) -0.0129(13) 0.0140(12) 0.0074(14) F9_7 0.0393(14) 0.0268(14) 0.0433(16) -0.0115(12) -0.0044(12) -0.0033(11) O1_9 0.0218(12) 0.0180(13) 0.0207(13) -0.0039(10) -0.0013(10) 0.0026(10) C1_9 0.0181(14) 0.0149(15) 0.0175(15) -0.0015(12) 0.0016(11) 0.0023(12) C2_9 0.0221(16) 0.0192(17) 0.0231(18) 0.0026(14) -0.0027(13) -0.0004(13) F1_9 0.0269(11) 0.0343(14) 0.0299(13) 0.0098(11) 0.0053(10) -0.0025(10) F2_9 0.0488(16) 0.0149(12) 0.0368(15) -0.0043(10) -0.0039(12) 0.0015(11) F3_9 0.0327(12) 0.0271(13) 0.0289(13) 0.0094(10) -0.0082(10) 0.0052(10) C3_9 0.0253(17) 0.0237(19) 0.0233(18) -0.0024(15) 0.0035(13) 0.0026(14) F4_9 0.0330(13) 0.0381(16) 0.0436(16) 0.0084(13) 0.0163(12) -0.0049(11) F5_9 0.0216(11) 0.0381(15) 0.0378(15) -0.0084(12) 0.0029(10) 0.0123(10) F6_9 0.0366(14) 0.0480(17) 0.0207(12) -0.0097(11) 0.0063(10) 0.0078(12) C4_9 0.0239(16) 0.0179(17) 0.0179(16) -0.0004(13) -0.0015(12) 0.0010(13) F7_9 0.0371(13) 0.0294(14) 0.0244(12) 0.0117(10) 0.0010(10) 0.0039(10) F8_9 0.0265(11) 0.0301(13) 0.0218(11) -0.0053(10) -0.0060(9) -0.0015(10) F9_9 0.0229(10) 0.0287(13) 0.0229(11) -0.0030(10) -0.0010(8) 0.0097(9) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ag1 Ru4 2.8870(11) . ? Ag1 Ru3 2.8886(10) . ? Ag1 Ru6 2.8899(11) . ? Ag1 Ru1 2.8927(11) . ? Ru1 C3 1.934(4) . ? Ru1 C2 1.938(4) . ? Ru1 C1 1.951(4) . ? Ru1 C4 1.962(4) . ? Ru1 Ru2 2.8714(10) . ? Ru1 Ru3 3.0044(14) . ? Ru2 C6 1.932(4) . ? Ru2 C8 1.935(4) . ? Ru2 C7 1.943(4) . ? Ru2 C5 1.945(4) . ? Ru2 Ru3 2.8699(11) . ? Ru3 C11 1.926(4) . ? Ru3 C10 1.941(4) . ? Ru3 C12 1.953(4) . ? Ru3 C9 1.958(4) . ? Ru4 C22 1.914(4) . ? Ru4 C23 1.933(4) . ? Ru4 C24 1.957(4) . ? Ru4 C21 1.961(4) . ? Ru4 Ru5 2.8743(11) . ? Ru4 Ru6 3.0066(11) . ? Ru5 C19 1.928(5) . ? Ru5 C18 1.929(5) . ? Ru5 C17 1.955(4) . ? Ru5 C20 1.960(4) . ? Ru5 Ru6 2.8732(11) . ? Ru6 C14 1.919(4) . ? Ru6 C15 1.936(4) . ? Ru6 C13 1.954(4) . ? Ru6 C16 1.957(4) . ? Al1 O1_4 1.69(2) . ? Al1 O1_3 1.718(8) . ? Al1 O1_7 1.724(3) . ? Al1 O1_9 1.731(3) . ? Al1 O1_8 1.75(3) . ? Al1 O1_2 1.747(9) . ? O4 C4 1.130(5) . ? O5 C5 1.136(4) . ? O6 C6 1.124(5) . ? O7 C7 1.138(4) . ? O8 C8 1.135(5) . ? O9 C9 1.130(5) . ? O10 C10 1.125(5) . ? O11 C11 1.134(5) . ? O12 C12 1.133(5) . ? O13 C13 1.133(4) . ? O14 C14 1.138(5) . ? O2 C2 1.135(4) . ? O1 C1 1.131(5) . ? O15 C15 1.137(4) . ? O16 C16 1.135(4) . ? O17 C17 1.129(5) . ? O18 C18 1.121(6) . ? O19 C19 1.132(6) . ? O20 C20 1.130(5) . ? O21 C21 1.134(5) . ? O22 C22 1.140(5) . ? O23 C23 1.139(5) . ? O24 C24 1.134(5) . ? O3 C3 1.126(5) . ? O1_2 C1_2 1.348(7) . ? C1_2 C3_2 1.555(7) . ? C1_2 C2_2 1.557(7) . ? C1_2 C4_2 1.557(7) . ? C2_2 F1_2 1.317(7) . ? C2_2 F3_2 1.333(6) . ? C2_2 F2_2 1.346(6) . ? C3_2 F5_2 1.323(8) . ? C3_2 F6_2 1.339(7) . ? C3_2 F4_2 1.339(8) . ? C4_2 F7_2 1.321(7) . ? C4_2 F9_2 1.336(7) . ? C4_2 F8_2 1.341(6) . ? O1_3 C1_3 1.357(6) . ? C1_3 C3_3 1.546(7) . ? C1_3 C4_3 1.549(6) . ? C1_3 C2_3 1.565(6) . ? C2_3 F1_3 1.317(7) . ? C2_3 F3_3 1.335(7) . ? C2_3 F2_3 1.343(6) . ? C3_3 F5_3 1.331(6) . ? C3_3 F6_3 1.339(6) . ? C3_3 F4_3 1.344(6) . ? C4_3 F7_3 1.327(6) . ? C4_3 F9_3 1.333(6) . ? C4_3 F8_3 1.339(6) . ? O1_4 C1_4 1.353(13) . ? C1_4 C2_4 1.545(11) . ? C1_4 C3_4 1.556(11) . ? C1_4 C4_4 1.559(11) . ? C2_4 F3_4 1.329(12) . ? C2_4 F1_4 1.335(11) . ? C2_4 F2_4 1.336(11) . ? C3_4 F4_4 1.328(12) . ? C3_4 F5_4 1.331(11) . ? C3_4 F6_4 1.337(11) . ? C4_4 F9_4 1.322(12) . ? C4_4 F8_4 1.335(11) . ? C4_4 F7_4 1.337(12) . ? F1_6 C1_6 1.344(8) . ? F2_6 C2_6 1.356(7) . ? F3_6 C3_6 1.353(7) . ? F4_6 C4_6 1.353(7) . ? C1_6 C6_6 1.377(9) . ? C1_6 C2_6 1.382(8) . ? C2_6 C3_6 1.363(8) . ? C3_6 C4_6 1.378(8) . ? C4_6 C5_6 1.378(8) . ? C5_6 C6_6 1.376(8) . ? C5_6 H5_6 0.9500 . ? C6_6 H6_6 0.9500 . ? O1_8 C1_8 1.356(13) . ? C1_8 C2_8 1.549(12) . ? C1_8 C3_8 1.554(12) . ? C1_8 C4_8 1.557(12) . ? C2_8 F2_8 1.334(13) . ? C2_8 F3_8 1.334(13) . ? C2_8 F1_8 1.335(13) . ? C3_8 F4_8 1.330(13) . ? C3_8 F5_8 1.330(13) . ? C3_8 F6_8 1.332(13) . ? C4_8 F9_8 1.328(13) . ? C4_8 F7_8 1.330(13) . ? C4_8 F8_8 1.334(13) . ? F1_5 C1_5 1.352(13) . ? F2_5 C2_5 1.340(13) . ? F3_5 C3_5 1.351(13) . ? F4_5 C4_5 1.362(13) . ? C1_5 C2_5 1.369(12) . ? C1_5 C6_5 1.377(13) . ? C2_5 C3_5 1.372(12) . ? C3_5 C4_5 1.375(12) . ? C4_5 C5_5 1.363(13) . ? C5_5 C6_5 1.372(13) . ? C5_5 H5_5 0.9500 . ? C6_5 H6_5 0.9500 . ? O1_7 C1_7 1.354(4) . ? C1_7 C4_7 1.548(5) . ? C1_7 C2_7 1.554(5) . ? C1_7 C3_7 1.562(5) . ? C2_7 F1_7 1.333(4) . ? C2_7 F3_7 1.334(5) . ? C2_7 F2_7 1.343(4) . ? C3_7 F4_7 1.325(5) . ? C3_7 F6_7 1.337(4) . ? C3_7 F5_7 1.346(5) . ? C4_7 F9_7 1.321(5) . ? C4_7 F8_7 1.337(5) . ? C4_7 F7_7 1.340(5) . ? O1_9 C1_9 1.350(4) . ? C1_9 C4_9 1.559(5) . ? C1_9 C3_9 1.560(5) . ? C1_9 C2_9 1.562(5) . ? C2_9 F3_9 1.323(4) . ? C2_9 F2_9 1.332(5) . ? C2_9 F1_9 1.345(4) . ? C3_9 F4_9 1.329(4) . ? C3_9 F6_9 1.329(5) . ? C3_9 F5_9 1.341(4) . ? C4_9 F9_9 1.328(4) . ? C4_9 F8_9 1.334(4) . ? C4_9 F7_9 1.335(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Ru4 Ag1 Ru3 142.30(2) . . ? Ru4 Ag1 Ru6 62.73(3) . . ? Ru3 Ag1 Ru6 132.31(2) . . ? Ru4 Ag1 Ru1 132.09(2) . . ? Ru3 Ag1 Ru1 62.62(3) . . ? Ru6 Ag1 Ru1 141.57(2) . . ? C3 Ru1 C2 93.99(15) . . ? C3 Ru1 C1 92.87(16) . . ? C2 Ru1 C1 91.17(15) . . ? C3 Ru1 C4 92.25(16) . . ? C2 Ru1 C4 91.09(15) . . ? C1 Ru1 C4 174.25(14) . . ? C3 Ru1 Ru2 83.90(12) . . ? C2 Ru1 Ru2 173.41(12) . . ? C1 Ru1 Ru2 95.17(10) . . ? C4 Ru1 Ru2 82.77(10) . . ? C3 Ru1 Ag1 157.66(12) . . ? C2 Ru1 Ag1 66.06(11) . . ? C1 Ru1 Ag1 78.28(10) . . ? C4 Ru1 Ag1 97.84(11) . . ? Ru2 Ru1 Ag1 117.03(3) . . ? C3 Ru1 Ru3 141.23(11) . . ? C2 Ru1 Ru3 124.47(11) . . ? C1 Ru1 Ru3 82.63(10) . . ? C4 Ru1 Ru3 91.73(10) . . ? Ru2 Ru1 Ru3 58.42(2) . . ? Ag1 Ru1 Ru3 58.624(16) . . ? C6 Ru2 C8 92.97(19) . . ? C6 Ru2 C7 94.19(16) . . ? C8 Ru2 C7 88.26(16) . . ? C6 Ru2 C5 88.13(16) . . ? C8 Ru2 C5 94.54(15) . . ? C7 Ru2 C5 176.27(15) . . ? C6 Ru2 Ru3 163.62(12) . . ? C8 Ru2 Ru3 102.40(15) . . ? C7 Ru2 Ru3 80.82(11) . . ? C5 Ru2 Ru3 96.16(12) . . ? C6 Ru2 Ru1 102.32(13) . . ? C8 Ru2 Ru1 163.63(14) . . ? C7 Ru2 Ru1 96.32(10) . . ? C5 Ru2 Ru1 80.32(10) . . ? Ru3 Ru2 Ru1 63.11(3) . . ? C11 Ru3 C10 94.00(16) . . ? C11 Ru3 C12 93.90(16) . . ? C10 Ru3 C12 91.75(16) . . ? C11 Ru3 C9 91.25(16) . . ? C10 Ru3 C9 91.22(16) . . ? C12 Ru3 C9 173.86(14) . . ? C11 Ru3 Ru2 82.84(13) . . ? C10 Ru3 Ru2 173.30(11) . . ? C12 Ru3 Ru2 94.35(11) . . ? C9 Ru3 Ru2 82.97(11) . . ? C11 Ru3 Ag1 158.27(12) . . ? C10 Ru3 Ag1 66.90(11) . . ? C12 Ru3 Ag1 77.15(11) . . ? C9 Ru3 Ag1 99.12(11) . . ? Ru2 Ru3 Ag1 117.21(3) . . ? C11 Ru3 Ru1 140.67(13) . . ? C10 Ru3 Ru1 125.22(10) . . ? C12 Ru3 Ru1 83.11(10) . . ? C9 Ru3 Ru1 90.79(10) . . ? Ru2 Ru3 Ru1 58.471(17) . . ? Ag1 Ru3 Ru1 58.76(2) . . ? C22 Ru4 C23 92.83(18) . . ? C22 Ru4 C24 91.14(16) . . ? C23 Ru4 C24 90.23(16) . . ? C22 Ru4 C21 93.07(16) . . ? C23 Ru4 C21 92.08(17) . . ? C24 Ru4 C21 175.09(17) . . ? C22 Ru4 Ru5 85.43(15) . . ? C23 Ru4 Ru5 172.78(11) . . ? C24 Ru4 Ru5 82.81(12) . . ? C21 Ru4 Ru5 95.01(13) . . ? C22 Ru4 Ag1 156.87(14) . . ? C23 Ru4 Ag1 65.44(11) . . ? C24 Ru4 Ag1 96.51(11) . . ? C21 Ru4 Ag1 80.54(11) . . ? Ru5 Ru4 Ag1 117.12(3) . . ? C22 Ru4 Ru6 143.37(15) . . ? C23 Ru4 Ru6 123.77(11) . . ? C24 Ru4 Ru6 90.14(12) . . ? C21 Ru4 Ru6 84.98(12) . . ? Ru5 Ru4 Ru6 58.44(2) . . ? Ag1 Ru4 Ru6 58.68(2) . . ? C19 Ru5 C18 99.4(2) . . ? C19 Ru5 C17 89.64(19) . . ? C18 Ru5 C17 91.27(19) . . ? C19 Ru5 C20 91.68(19) . . ? C18 Ru5 C20 88.99(19) . . ? C17 Ru5 C20 178.60(17) . . ? C19 Ru5 Ru6 159.38(16) . . ? C18 Ru5 Ru6 100.81(14) . . ? C17 Ru5 Ru6 93.89(12) . . ? C20 Ru5 Ru6 84.71(12) . . ? C19 Ru5 Ru4 97.18(16) . . ? C18 Ru5 Ru4 162.74(13) . . ? C17 Ru5 Ru4 84.13(14) . . ? C20 Ru5 Ru4 95.23(13) . . ? Ru6 Ru5 Ru4 63.08(3) . . ? C14 Ru6 C15 94.09(17) . . ? C14 Ru6 C13 91.17(16) . . ? C15 Ru6 C13 89.85(15) . . ? C14 Ru6 C16 92.99(16) . . ? C15 Ru6 C16 91.74(15) . . ? C13 Ru6 C16 175.43(16) . . ? C14 Ru6 Ru5 84.52(12) . . ? C15 Ru6 Ru5 173.96(11) . . ? C13 Ru6 Ru5 84.31(11) . . ? C16 Ru6 Ru5 94.20(11) . . ? C14 Ru6 Ag1 157.61(12) . . ? C15 Ru6 Ag1 65.07(12) . . ? C13 Ru6 Ag1 96.61(12) . . ? C16 Ru6 Ag1 80.20(11) . . ? Ru5 Ru6 Ag1 117.06(3) . . ? C14 Ru6 Ru4 142.65(12) . . ? C15 Ru6 Ru4 123.24(12) . . ? C13 Ru6 Ru4 90.06(12) . . ? C16 Ru6 Ru4 85.49(11) . . ? Ru5 Ru6 Ru4 58.48(2) . . ? Ag1 Ru6 Ru4 58.59(2) . . ? O1_4 Al1 O1_7 109.8(11) . . ? O1_3 Al1 O1_7 107.0(4) . . ? O1_4 Al1 O1_9 101.4(11) . . ? O1_3 Al1 O1_9 108.1(4) . . ? O1_7 Al1 O1_9 115.60(14) . . ? O1_4 Al1 O1_8 117.9(18) . . ? O1_7 Al1 O1_8 106.3(13) . . ? O1_9 Al1 O1_8 106.2(12) . . ? O1_3 Al1 O1_2 114.0(6) . . ? O1_7 Al1 O1_2 106.0(4) . . ? O1_9 Al1 O1_2 106.3(4) . . ? O1 C1 Ru1 175.6(3) . . ? O2 C2 Ru1 171.0(3) . . ? O3 C3 Ru1 177.4(4) . . ? O4 C4 Ru1 175.6(3) . . ? O5 C5 Ru2 173.3(3) . . ? O6 C6 Ru2 176.8(4) . . ? O7 C7 Ru2 173.6(3) . . ? O8 C8 Ru2 176.4(5) . . ? O9 C9 Ru3 175.7(3) . . ? O10 C10 Ru3 171.2(3) . . ? O11 C11 Ru3 178.1(4) . . ? O12 C12 Ru3 175.5(3) . . ? O13 C13 Ru6 174.4(3) . . ? O14 C14 Ru6 177.9(4) . . ? O15 C15 Ru6 170.3(3) . . ? O16 C16 Ru6 175.0(3) . . ? O17 C17 Ru5 174.0(4) . . ? O18 C18 Ru5 179.7(4) . . ? O19 C19 Ru5 177.8(5) . . ? O20 C20 Ru5 174.0(4) . . ? O21 C21 Ru4 175.5(4) . . ? O22 C22 Ru4 177.6(4) . . ? O23 C23 Ru4 169.9(3) . . ? O24 C24 Ru4 174.7(4) . . ? C1_2 O1_2 Al1 145.9(9) . . ? O1_2 C1_2 C3_2 111.4(7) . . ? O1_2 C1_2 C2_2 111.8(7) . . ? C3_2 C1_2 C2_2 108.9(5) . . ? O1_2 C1_2 C4_2 106.6(7) . . ? C3_2 C1_2 C4_2 109.7(5) . . ? C2_2 C1_2 C4_2 108.4(5) . . ? F1_2 C2_2 F3_2 106.5(5) . . ? F1_2 C2_2 F2_2 107.9(5) . . ? F3_2 C2_2 F2_2 106.9(5) . . ? F1_2 C2_2 C1_2 110.6(5) . . ? F3_2 C2_2 C1_2 111.6(4) . . ? F2_2 C2_2 C1_2 113.0(5) . . ? F5_2 C3_2 F6_2 107.8(6) . . ? F5_2 C3_2 F4_2 108.5(6) . . ? F6_2 C3_2 F4_2 107.3(6) . . ? F5_2 C3_2 C1_2 110.8(6) . . ? F6_2 C3_2 C1_2 112.1(5) . . ? F4_2 C3_2 C1_2 110.1(5) . . ? F7_2 C4_2 F9_2 107.3(5) . . ? F7_2 C4_2 F8_2 107.6(5) . . ? F9_2 C4_2 F8_2 108.0(5) . . ? F7_2 C4_2 C1_2 110.6(5) . . ? F9_2 C4_2 C1_2 111.2(5) . . ? F8_2 C4_2 C1_2 111.9(4) . . ? C1_3 O1_3 Al1 148.5(8) . . ? O1_3 C1_3 C3_3 111.1(6) . . ? O1_3 C1_3 C4_3 107.0(6) . . ? C3_3 C1_3 C4_3 109.7(4) . . ? O1_3 C1_3 C2_3 111.0(5) . . ? C3_3 C1_3 C2_3 109.1(4) . . ? C4_3 C1_3 C2_3 108.9(4) . . ? F1_3 C2_3 F3_3 107.3(5) . . ? F1_3 C2_3 F2_3 107.3(5) . . ? F3_3 C2_3 F2_3 107.3(5) . . ? F1_3 C2_3 C1_3 111.2(5) . . ? F3_3 C2_3 C1_3 111.0(5) . . ? F2_3 C2_3 C1_3 112.5(5) . . ? F5_3 C3_3 F6_3 108.2(5) . . ? F5_3 C3_3 F4_3 106.8(5) . . ? F6_3 C3_3 F4_3 107.2(5) . . ? F5_3 C3_3 C1_3 110.4(4) . . ? F6_3 C3_3 C1_3 113.0(5) . . ? F4_3 C3_3 C1_3 111.0(5) . . ? F7_3 C4_3 F9_3 107.2(5) . . ? F7_3 C4_3 F8_3 107.4(5) . . ? F9_3 C4_3 F8_3 107.9(5) . . ? F7_3 C4_3 C1_3 110.8(4) . . ? F9_3 C4_3 C1_3 111.2(4) . . ? F8_3 C4_3 C1_3 112.1(5) . . ? C1_4 O1_4 Al1 152(2) . . ? O1_4 C1_4 C2_4 109.9(16) . . ? O1_4 C1_4 C3_4 110.1(16) . . ? C2_4 C1_4 C3_4 109.3(9) . . ? O1_4 C1_4 C4_4 109.0(16) . . ? C2_4 C1_4 C4_4 109.8(9) . . ? C3_4 C1_4 C4_4 108.7(9) . . ? F3_4 C2_4 F1_4 105.4(13) . . ? F3_4 C2_4 F2_4 107.8(12) . . ? F1_4 C2_4 F2_4 107.0(11) . . ? F3_4 C2_4 C1_4 113.4(11) . . ? F1_4 C2_4 C1_4 111.3(10) . . ? F2_4 C2_4 C1_4 111.5(10) . . ? F4_4 C3_4 F5_4 106.7(13) . . ? F4_4 C3_4 F6_4 108.6(13) . . ? F5_4 C3_4 F6_4 107.5(11) . . ? F4_4 C3_4 C1_4 108.6(12) . . ? F5_4 C3_4 C1_4 111.5(9) . . ? F6_4 C3_4 C1_4 113.7(10) . . ? F9_4 C4_4 F8_4 109.4(13) . . ? F9_4 C4_4 F7_4 106.7(12) . . ? F8_4 C4_4 F7_4 108.2(12) . . ? F9_4 C4_4 C1_4 110.8(12) . . ? F8_4 C4_4 C1_4 111.7(10) . . ? F7_4 C4_4 C1_4 109.8(11) . . ? F1_6 C1_6 C6_6 119.9(7) . . ? F1_6 C1_6 C2_6 120.1(7) . . ? C6_6 C1_6 C2_6 120.0(7) . . ? F2_6 C2_6 C3_6 120.1(6) . . ? F2_6 C2_6 C1_6 119.6(6) . . ? C3_6 C2_6 C1_6 120.2(6) . . ? F3_6 C3_6 C2_6 119.5(6) . . ? F3_6 C3_6 C4_6 120.7(6) . . ? C2_6 C3_6 C4_6 119.7(6) . . ? F4_6 C4_6 C3_6 118.3(6) . . ? F4_6 C4_6 C5_6 121.1(6) . . ? C3_6 C4_6 C5_6 120.6(6) . . ? C6_6 C5_6 C4_6 119.5(7) . . ? C6_6 C5_6 H5_6 120.2 . . ? C4_6 C5_6 H5_6 120.2 . . ? C5_6 C6_6 C1_6 120.0(7) . . ? C5_6 C6_6 H6_6 120.0 . . ? C1_6 C6_6 H6_6 120.0 . . ? C1_8 O1_8 Al1 148(3) . . ? O1_8 C1_8 C2_8 110.8(18) . . ? O1_8 C1_8 C3_8 108.2(17) . . ? C2_8 C1_8 C3_8 109.9(11) . . ? O1_8 C1_8 C4_8 109.0(18) . . ? C2_8 C1_8 C4_8 109.7(11) . . ? C3_8 C1_8 C4_8 109.0(11) . . ? F2_8 C2_8 F3_8 107.6(14) . . ? F2_8 C2_8 F1_8 106.5(14) . . ? F3_8 C2_8 F1_8 107.5(14) . . ? F2_8 C2_8 C1_8 112.6(14) . . ? F3_8 C2_8 C1_8 111.1(13) . . ? F1_8 C2_8 C1_8 111.3(12) . . ? F4_8 C3_8 F5_8 107.3(13) . . ? F4_8 C3_8 F6_8 107.5(14) . . ? F5_8 C3_8 F6_8 107.0(14) . . ? F4_8 C3_8 C1_8 111.6(12) . . ? F5_8 C3_8 C1_8 111.4(12) . . ? F6_8 C3_8 C1_8 111.8(13) . . ? F9_8 C4_8 F7_8 107.1(14) . . ? F9_8 C4_8 F8_8 106.0(14) . . ? F7_8 C4_8 F8_8 108.7(15) . . ? F9_8 C4_8 C1_8 112.4(12) . . ? F7_8 C4_8 C1_8 110.2(12) . . ? F8_8 C4_8 C1_8 112.1(15) . . ? F1_5 C1_5 C2_5 122.9(14) . . ? F1_5 C1_5 C6_5 117.4(14) . . ? C2_5 C1_5 C6_5 119.7(13) . . ? F2_5 C2_5 C1_5 118.5(13) . . ? F2_5 C2_5 C3_5 121.1(13) . . ? C1_5 C2_5 C3_5 120.4(12) . . ? F3_5 C3_5 C2_5 121.7(13) . . ? F3_5 C3_5 C4_5 118.0(13) . . ? C2_5 C3_5 C4_5 120.2(12) . . ? F4_5 C4_5 C5_5 122.3(14) . . ? F4_5 C4_5 C3_5 118.8(14) . . ? C5_5 C4_5 C3_5 118.9(13) . . ? C4_5 C5_5 C6_5 121.5(16) . . ? C4_5 C5_5 H5_5 119.2 . . ? C6_5 C5_5 H5_5 119.2 . . ? C5_5 C6_5 C1_5 119.3(16) . . ? C5_5 C6_5 H6_5 120.4 . . ? C1_5 C6_5 H6_5 120.4 . . ? C1_7 O1_7 Al1 149.6(2) . . ? O1_7 C1_7 C4_7 108.9(3) . . ? O1_7 C1_7 C2_7 111.8(3) . . ? C4_7 C1_7 C2_7 109.8(3) . . ? O1_7 C1_7 C3_7 107.9(3) . . ? C4_7 C1_7 C3_7 109.5(3) . . ? C2_7 C1_7 C3_7 108.9(3) . . ? F1_7 C2_7 F3_7 107.6(3) . . ? F1_7 C2_7 F2_7 107.8(3) . . ? F3_7 C2_7 F2_7 107.2(3) . . ? F1_7 C2_7 C1_7 111.4(3) . . ? F3_7 C2_7 C1_7 110.3(3) . . ? F2_7 C2_7 C1_7 112.3(3) . . ? F4_7 C3_7 F6_7 107.9(3) . . ? F4_7 C3_7 F5_7 107.8(3) . . ? F6_7 C3_7 F5_7 107.6(3) . . ? F4_7 C3_7 C1_7 111.1(3) . . ? F6_7 C3_7 C1_7 112.7(3) . . ? F5_7 C3_7 C1_7 109.5(3) . . ? F9_7 C4_7 F8_7 107.4(3) . . ? F9_7 C4_7 F7_7 107.6(4) . . ? F8_7 C4_7 F7_7 107.1(3) . . ? F9_7 C4_7 C1_7 111.4(3) . . ? F8_7 C4_7 C1_7 112.3(3) . . ? F7_7 C4_7 C1_7 110.7(3) . . ? C1_9 O1_9 Al1 147.0(2) . . ? O1_9 C1_9 C4_9 112.5(3) . . ? O1_9 C1_9 C3_9 109.5(3) . . ? C4_9 C1_9 C3_9 108.8(3) . . ? O1_9 C1_9 C2_9 108.0(3) . . ? C4_9 C1_9 C2_9 109.1(3) . . ? C3_9 C1_9 C2_9 108.8(3) . . ? F3_9 C2_9 F2_9 108.0(3) . . ? F3_9 C2_9 F1_9 107.0(3) . . ? F2_9 C2_9 F1_9 107.5(3) . . ? F3_9 C2_9 C1_9 111.1(3) . . ? F2_9 C2_9 C1_9 113.2(3) . . ? F1_9 C2_9 C1_9 109.8(3) . . ? F4_9 C3_9 F6_9 109.0(3) . . ? F4_9 C3_9 F5_9 106.6(3) . . ? F6_9 C3_9 F5_9 107.5(3) . . ? F4_9 C3_9 C1_9 110.6(3) . . ? F6_9 C3_9 C1_9 112.6(3) . . ? F5_9 C3_9 C1_9 110.4(3) . . ? F9_9 C4_9 F8_9 108.1(3) . . ? F9_9 C4_9 F7_9 107.8(3) . . ? F8_9 C4_9 F7_9 107.5(3) . . ? F9_9 C4_9 C1_9 109.4(3) . . ? F8_9 C4_9 C1_9 112.8(3) . . ? F7_9 C4_9 C1_9 111.1(3) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1_3 Al1 O1_2 C1_2 83.2(17) . . . . ? O1_7 Al1 O1_2 C1_2 -159.4(15) . . . . ? O1_9 Al1 O1_2 C1_2 -35.9(17) . . . . ? Al1 O1_2 C1_2 C3_2 -64.1(17) . . . . ? Al1 O1_2 C1_2 C2_2 58.0(17) . . . . ? Al1 O1_2 C1_2 C4_2 176.3(14) . . . . ? O1_2 C1_2 C2_2 F1_2 37.5(8) . . . . ? C3_2 C1_2 C2_2 F1_2 161.0(5) . . . . ? C4_2 C1_2 C2_2 F1_2 -79.7(6) . . . . ? O1_2 C1_2 C2_2 F3_2 -80.9(8) . . . . ? C3_2 C1_2 C2_2 F3_2 42.5(6) . . . . ? C4_2 C1_2 C2_2 F3_2 161.8(4) . . . . ? O1_2 C1_2 C2_2 F2_2 158.6(7) . . . . ? C3_2 C1_2 C2_2 F2_2 -78.0(6) . . . . ? C4_2 C1_2 C2_2 F2_2 41.3(6) . . . . ? O1_2 C1_2 C3_2 F5_2 45.4(9) . . . . ? C2_2 C1_2 C3_2 F5_2 -78.3(7) . . . . ? C4_2 C1_2 C3_2 F5_2 163.2(6) . . . . ? O1_2 C1_2 C3_2 F6_2 165.9(7) . . . . ? C2_2 C1_2 C3_2 F6_2 42.2(6) . . . . ? C4_2 C1_2 C3_2 F6_2 -76.3(6) . . . . ? O1_2 C1_2 C3_2 F4_2 -74.6(8) . . . . ? C2_2 C1_2 C3_2 F4_2 161.7(5) . . . . ? C4_2 C1_2 C3_2 F4_2 43.2(7) . . . . ? O1_2 C1_2 C4_2 F7_2 44.2(8) . . . . ? C3_2 C1_2 C4_2 F7_2 -76.5(6) . . . . ? C2_2 C1_2 C4_2 F7_2 164.7(5) . . . . ? O1_2 C1_2 C4_2 F9_2 -74.9(8) . . . . ? C3_2 C1_2 C4_2 F9_2 164.4(5) . . . . ? C2_2 C1_2 C4_2 F9_2 45.6(6) . . . . ? O1_2 C1_2 C4_2 F8_2 164.1(7) . . . . ? C3_2 C1_2 C4_2 F8_2 43.4(6) . . . . ? C2_2 C1_2 C4_2 F8_2 -75.4(6) . . . . ? O1_7 Al1 O1_3 C1_3 -30.7(16) . . . . ? O1_9 Al1 O1_3 C1_3 -155.8(14) . . . . ? O1_2 Al1 O1_3 C1_3 86.2(15) . . . . ? Al1 O1_3 C1_3 C3_3 -55.3(16) . . . . ? Al1 O1_3 C1_3 C4_3 -175.1(13) . . . . ? Al1 O1_3 C1_3 C2_3 66.2(16) . . . . ? O1_3 C1_3 C2_3 F1_3 39.3(8) . . . . ? C3_3 C1_3 C2_3 F1_3 162.1(5) . . . . ? C4_3 C1_3 C2_3 F1_3 -78.2(6) . . . . ? O1_3 C1_3 C2_3 F3_3 -80.0(7) . . . . ? C3_3 C1_3 C2_3 F3_3 42.8(6) . . . . ? C4_3 C1_3 C2_3 F3_3 162.5(5) . . . . ? O1_3 C1_3 C2_3 F2_3 159.8(7) . . . . ? C3_3 C1_3 C2_3 F2_3 -77.4(6) . . . . ? C4_3 C1_3 C2_3 F2_3 42.3(7) . . . . ? O1_3 C1_3 C3_3 F5_3 44.5(7) . . . . ? C4_3 C1_3 C3_3 F5_3 162.7(5) . . . . ? C2_3 C1_3 C3_3 F5_3 -78.1(6) . . . . ? O1_3 C1_3 C3_3 F6_3 166.0(6) . . . . ? C4_3 C1_3 C3_3 F6_3 -75.9(6) . . . . ? C2_3 C1_3 C3_3 F6_3 43.3(6) . . . . ? O1_3 C1_3 C3_3 F4_3 -73.6(7) . . . . ? C4_3 C1_3 C3_3 F4_3 44.5(6) . . . . ? C2_3 C1_3 C3_3 F4_3 163.7(5) . . . . ? O1_3 C1_3 C4_3 F7_3 45.6(7) . . . . ? C3_3 C1_3 C4_3 F7_3 -75.1(6) . . . . ? C2_3 C1_3 C4_3 F7_3 165.6(5) . . . . ? O1_3 C1_3 C4_3 F9_3 -73.5(7) . . . . ? C3_3 C1_3 C4_3 F9_3 165.8(5) . . . . ? C2_3 C1_3 C4_3 F9_3 46.5(6) . . . . ? O1_3 C1_3 C4_3 F8_3 165.6(6) . . . . ? C3_3 C1_3 C4_3 F8_3 44.9(6) . . . . ? C2_3 C1_3 C4_3 F8_3 -74.4(6) . . . . ? O1_7 Al1 O1_4 C1_4 -176(5) . . . . ? O1_9 Al1 O1_4 C1_4 -53(5) . . . . ? O1_8 Al1 O1_4 C1_4 62(6) . . . . ? Al1 O1_4 C1_4 C2_4 121(5) . . . . ? Al1 O1_4 C1_4 C3_4 0(6) . . . . ? Al1 O1_4 C1_4 C4_4 -119(5) . . . . ? O1_4 C1_4 C2_4 F3_4 -42(2) . . . . ? C3_4 C1_4 C2_4 F3_4 78.7(15) . . . . ? C4_4 C1_4 C2_4 F3_4 -162.1(14) . . . . ? O1_4 C1_4 C2_4 F1_4 76.5(19) . . . . ? C3_4 C1_4 C2_4 F1_4 -162.6(11) . . . . ? C4_4 C1_4 C2_4 F1_4 -43.4(14) . . . . ? O1_4 C1_4 C2_4 F2_4 -164.1(18) . . . . ? C3_4 C1_4 C2_4 F2_4 -43.2(14) . . . . ? C4_4 C1_4 C2_4 F2_4 76.0(13) . . . . ? O1_4 C1_4 C3_4 F4_4 -41(2) . . . . ? C2_4 C1_4 C3_4 F4_4 -161.4(14) . . . . ? C4_4 C1_4 C3_4 F4_4 78.8(15) . . . . ? O1_4 C1_4 C3_4 F5_4 76.7(18) . . . . ? C2_4 C1_4 C3_4 F5_4 -44.1(13) . . . . ? C4_4 C1_4 C3_4 F5_4 -163.9(10) . . . . ? O1_4 C1_4 C3_4 F6_4 -161.6(19) . . . . ? C2_4 C1_4 C3_4 F6_4 77.6(14) . . . . ? C4_4 C1_4 C3_4 F6_4 -42.2(15) . . . . ? O1_4 C1_4 C4_4 F9_4 -42.0(19) . . . . ? C2_4 C1_4 C4_4 F9_4 78.5(13) . . . . ? C3_4 C1_4 C4_4 F9_4 -162.0(12) . . . . ? O1_4 C1_4 C4_4 F8_4 -164.2(17) . . . . ? C2_4 C1_4 C4_4 F8_4 -43.8(13) . . . . ? C3_4 C1_4 C4_4 F8_4 75.7(12) . . . . ? O1_4 C1_4 C4_4 F7_4 76(2) . . . . ? C2_4 C1_4 C4_4 F7_4 -163.9(12) . . . . ? C3_4 C1_4 C4_4 F7_4 -44.4(14) . . . . ? F1_6 C1_6 C2_6 F2_6 0.5(10) . . . . ? C6_6 C1_6 C2_6 F2_6 -179.6(6) . . . . ? F1_6 C1_6 C2_6 C3_6 179.1(6) . . . . ? C6_6 C1_6 C2_6 C3_6 -1.0(10) . . . . ? F2_6 C2_6 C3_6 F3_6 -1.1(9) . . . . ? C1_6 C2_6 C3_6 F3_6 -179.7(6) . . . . ? F2_6 C2_6 C3_6 C4_6 179.3(6) . . . . ? C1_6 C2_6 C3_6 C4_6 0.7(10) . . . . ? F3_6 C3_6 C4_6 F4_6 0.5(9) . . . . ? C2_6 C3_6 C4_6 F4_6 -179.9(6) . . . . ? F3_6 C3_6 C4_6 C5_6 -179.6(6) . . . . ? C2_6 C3_6 C4_6 C5_6 0.0(10) . . . . ? F4_6 C4_6 C5_6 C6_6 179.5(6) . . . . ? C3_6 C4_6 C5_6 C6_6 -0.4(10) . . . . ? C4_6 C5_6 C6_6 C1_6 0.1(10) . . . . ? F1_6 C1_6 C6_6 C5_6 -179.5(7) . . . . ? C2_6 C1_6 C6_6 C5_6 0.6(11) . . . . ? O1_4 Al1 O1_8 C1_8 84(6) . . . . ? O1_7 Al1 O1_8 C1_8 -40(6) . . . . ? O1_9 Al1 O1_8 C1_8 -163(5) . . . . ? Al1 O1_8 C1_8 C2_8 -40(6) . . . . ? Al1 O1_8 C1_8 C3_8 -160(5) . . . . ? Al1 O1_8 C1_8 C4_8 81(6) . . . . ? O1_8 C1_8 C2_8 F2_8 -166(2) . . . . ? C3_8 C1_8 C2_8 F2_8 -46.1(17) . . . . ? C4_8 C1_8 C2_8 F2_8 73.8(16) . . . . ? O1_8 C1_8 C2_8 F3_8 -45(2) . . . . ? C3_8 C1_8 C2_8 F3_8 74.7(16) . . . . ? C4_8 C1_8 C2_8 F3_8 -165.4(14) . . . . ? O1_8 C1_8 C2_8 F1_8 75(2) . . . . ? C3_8 C1_8 C2_8 F1_8 -165.6(14) . . . . ? C4_8 C1_8 C2_8 F1_8 -45.7(17) . . . . ? O1_8 C1_8 C3_8 F4_8 -43(2) . . . . ? C2_8 C1_8 C3_8 F4_8 -163.9(14) . . . . ? C4_8 C1_8 C3_8 F4_8 75.7(16) . . . . ? O1_8 C1_8 C3_8 F5_8 77(2) . . . . ? C2_8 C1_8 C3_8 F5_8 -44.1(17) . . . . ? C4_8 C1_8 C3_8 F5_8 -164.4(14) . . . . ? O1_8 C1_8 C3_8 F6_8 -163(2) . . . . ? C2_8 C1_8 C3_8 F6_8 75.6(16) . . . . ? C4_8 C1_8 C3_8 F6_8 -44.7(17) . . . . ? O1_8 C1_8 C4_8 F9_8 -46(2) . . . . ? C2_8 C1_8 C4_8 F9_8 75.2(17) . . . . ? C3_8 C1_8 C4_8 F9_8 -164.4(15) . . . . ? O1_8 C1_8 C4_8 F7_8 73(2) . . . . ? C2_8 C1_8 C4_8 F7_8 -165.4(14) . . . . ? C3_8 C1_8 C4_8 F7_8 -44.9(16) . . . . ? O1_8 C1_8 C4_8 F8_8 -166(2) . . . . ? C2_8 C1_8 C4_8 F8_8 -44.2(17) . . . . ? C3_8 C1_8 C4_8 F8_8 76.3(17) . . . . ? F1_5 C1_5 C2_5 F2_5 0(2) . . . . ? C6_5 C1_5 C2_5 F2_5 -179.8(12) . . . . ? F1_5 C1_5 C2_5 C3_5 179.5(12) . . . . ? C6_5 C1_5 C2_5 C3_5 0(2) . . . . ? F2_5 C2_5 C3_5 F3_5 -1.1(19) . . . . ? C1_5 C2_5 C3_5 F3_5 179.5(12) . . . . ? F2_5 C2_5 C3_5 C4_5 -179.4(12) . . . . ? C1_5 C2_5 C3_5 C4_5 1(2) . . . . ? F3_5 C3_5 C4_5 F4_5 0.6(19) . . . . ? C2_5 C3_5 C4_5 F4_5 179.0(13) . . . . ? F3_5 C3_5 C4_5 C5_5 -179.8(12) . . . . ? C2_5 C3_5 C4_5 C5_5 -1(2) . . . . ? F4_5 C4_5 C5_5 C6_5 -179.5(14) . . . . ? C3_5 C4_5 C5_5 C6_5 1(2) . . . . ? C4_5 C5_5 C6_5 C1_5 0(2) . . . . ? F1_5 C1_5 C6_5 C5_5 -180.0(12) . . . . ? C2_5 C1_5 C6_5 C5_5 0(2) . . . . ? O1_4 Al1 O1_7 C1_7 35.8(14) . . . . ? O1_3 Al1 O1_7 C1_7 161.3(6) . . . . ? O1_9 Al1 O1_7 C1_7 -78.2(5) . . . . ? O1_8 Al1 O1_7 C1_7 164.3(15) . . . . ? O1_2 Al1 O1_7 C1_7 39.2(7) . . . . ? Al1 O1_7 C1_7 C4_7 -110.0(5) . . . . ? Al1 O1_7 C1_7 C2_7 11.5(7) . . . . ? Al1 O1_7 C1_7 C3_7 131.2(4) . . . . ? O1_7 C1_7 C2_7 F1_7 -81.2(4) . . . . ? C4_7 C1_7 C2_7 F1_7 39.8(4) . . . . ? C3_7 C1_7 C2_7 F1_7 159.7(3) . . . . ? O1_7 C1_7 C2_7 F3_7 38.3(4) . . . . ? C4_7 C1_7 C2_7 F3_7 159.3(3) . . . . ? C3_7 C1_7 C2_7 F3_7 -80.9(4) . . . . ? O1_7 C1_7 C2_7 F2_7 157.8(3) . . . . ? C4_7 C1_7 C2_7 F2_7 -81.2(4) . . . . ? C3_7 C1_7 C2_7 F2_7 38.7(4) . . . . ? O1_7 C1_7 C3_7 F4_7 42.1(4) . . . . ? C4_7 C1_7 C3_7 F4_7 -76.3(4) . . . . ? C2_7 C1_7 C3_7 F4_7 163.6(3) . . . . ? O1_7 C1_7 C3_7 F6_7 163.4(3) . . . . ? C4_7 C1_7 C3_7 F6_7 45.0(4) . . . . ? C2_7 C1_7 C3_7 F6_7 -75.1(4) . . . . ? O1_7 C1_7 C3_7 F5_7 -76.8(4) . . . . ? C4_7 C1_7 C3_7 F5_7 164.8(3) . . . . ? C2_7 C1_7 C3_7 F5_7 44.7(4) . . . . ? O1_7 C1_7 C4_7 F9_7 48.3(4) . . . . ? C2_7 C1_7 C4_7 F9_7 -74.4(4) . . . . ? C3_7 C1_7 C4_7 F9_7 166.0(3) . . . . ? O1_7 C1_7 C4_7 F8_7 168.9(3) . . . . ? C2_7 C1_7 C4_7 F8_7 46.2(4) . . . . ? C3_7 C1_7 C4_7 F8_7 -73.4(4) . . . . ? O1_7 C1_7 C4_7 F7_7 -71.5(4) . . . . ? C2_7 C1_7 C4_7 F7_7 165.8(3) . . . . ? C3_7 C1_7 C4_7 F7_7 46.3(4) . . . . ? O1_4 Al1 O1_9 C1_9 169.9(12) . . . . ? O1_3 Al1 O1_9 C1_9 48.5(6) . . . . ? O1_7 Al1 O1_9 C1_9 -71.4(5) . . . . ? O1_8 Al1 O1_9 C1_9 46.2(15) . . . . ? O1_2 Al1 O1_9 C1_9 171.4(6) . . . . ? Al1 O1_9 C1_9 C4_9 9.6(6) . . . . ? Al1 O1_9 C1_9 C3_9 -111.6(4) . . . . ? Al1 O1_9 C1_9 C2_9 130.1(4) . . . . ? O1_9 C1_9 C2_9 F3_9 42.7(4) . . . . ? C4_9 C1_9 C2_9 F3_9 165.3(3) . . . . ? C3_9 C1_9 C2_9 F3_9 -76.1(4) . . . . ? O1_9 C1_9 C2_9 F2_9 164.5(3) . . . . ? C4_9 C1_9 C2_9 F2_9 -72.9(4) . . . . ? C3_9 C1_9 C2_9 F2_9 45.7(4) . . . . ? O1_9 C1_9 C2_9 F1_9 -75.5(3) . . . . ? C4_9 C1_9 C2_9 F1_9 47.1(4) . . . . ? C3_9 C1_9 C2_9 F1_9 165.7(3) . . . . ? O1_9 C1_9 C3_9 F4_9 45.0(4) . . . . ? C4_9 C1_9 C3_9 F4_9 -78.4(4) . . . . ? C2_9 C1_9 C3_9 F4_9 162.9(3) . . . . ? O1_9 C1_9 C3_9 F6_9 167.2(3) . . . . ? C4_9 C1_9 C3_9 F6_9 43.8(4) . . . . ? C2_9 C1_9 C3_9 F6_9 -75.0(4) . . . . ? O1_9 C1_9 C3_9 F5_9 -72.7(4) . . . . ? C4_9 C1_9 C3_9 F5_9 163.9(3) . . . . ? C2_9 C1_9 C3_9 F5_9 45.1(4) . . . . ? O1_9 C1_9 C4_9 F9_9 37.3(4) . . . . ? C3_9 C1_9 C4_9 F9_9 158.8(3) . . . . ? C2_9 C1_9 C4_9 F9_9 -82.6(4) . . . . ? O1_9 C1_9 C4_9 F8_9 157.5(3) . . . . ? C3_9 C1_9 C4_9 F8_9 -81.0(4) . . . . ? C2_9 C1_9 C4_9 F8_9 37.6(4) . . . . ? O1_9 C1_9 C4_9 F7_9 -81.7(4) . . . . ? C3_9 C1_9 C4_9 F7_9 39.9(4) . . . . ? C2_9 C1_9 C4_9 F7_9 158.5(3) . . . . ? _shelx_res_file ; TITL P-1_PD_a.res in P-1 p-1_a.res created by SHELXL-2018/3 at 11:22:07 on 14-Feb-2022 REM Old TITL P-1_PD in P-1 REM SHELXT solution in P-1: R1 0.092, Rweak 0.006, Alpha 0.074 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C49 O26 F39 Al Ru6 Ag CELL 0.71073 12.3495 12.3853 23.0407 90.852 94.031 93.152 ZERR 2.000 0.0059 0.0044 0.0095 0.022 0.010 0.013 LATT 1 SFAC C O F AL RU AG H UNIT 92 56 80 2 12 2 4 OMIT -8 -1 2 RIGU 0.004 0.004 F1_6 F2_6 F3_6 F4_6 C1_6 C2_6 C3_6 C4_6 C5_6 C6_6 = F1_5 F2_5 F3_5 F4_5 C1_5 C2_5 C3_5 C4_5 C5_5 C6_5 SIMU 0.02 0.04 2 F1_6 F2_6 F3_6 F4_6 C1_6 C2_6 C3_6 C4_6 C5_6 C6_6 = F1_5 F2_5 F3_5 F4_5 C1_5 C2_5 C3_5 C4_5 C5_5 C6_5 RIGU 0.004 0.004 O1_2 C1_2 C2_2 F1_2 F2_2 F3_2 C3_2 F4_2 F5_2 F6_2 = C4_2 F7_2 F8_2 F9_2 O1_4 C1_4 C2_4 F1_4 F2_4 F3_4 C3_4 F4_4 F5_4 F6_4 = C4_4 F7_4 F8_4 F9_4 SIMU 0.02 0.04 2 O1_2 C1_2 C2_2 F1_2 F2_2 F3_2 C3_2 F4_2 F5_2 F6_2 = C4_2 F7_2 F8_2 F9_2 O1_4 C1_4 C2_4 F1_4 F2_4 F3_4 C3_4 F4_4 F5_4 F6_4 = C4_4 F7_4 F8_4 F9_4 RIGU 0.002 0.002 O1_3 C1_3 C2_3 F1_3 F2_3 F3_3 C3_3 F4_3 F5_3 F6_3 = C4_3 F7_3 F8_3 F9_3 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 SIMU 0.02 0.02 2 O1_3 C1_3 C2_3 F1_3 F2_3 F3_3 C3_3 F4_3 F5_3 F6_3 = C4_3 F7_3 F8_3 F9_3 O1_8 C1_8 C2_8 F1_8 F2_8 F3_8 C3_8 F4_8 F5_8 F6_8 = C4_8 F7_8 F8_8 F9_8 REM Restraints for Fragment oc(cf3)3, Nonafluoro-tert-butoxy, [(CF3)3CO]- REM from: TURBOMOLE V6.0 B-P86/def-SV(P). Please cite REM https://doi.org/10.1107/S1600576718004508 SADI_CCF3 0.02 C1 C2 C1 C3 C1 C4 SADI_CCF3 0.02 F1 C2 F2 C2 F3 C2 F4 C3 F5 C3 F6 C3 F7 C4 F8 C4 F9 C4 SADI_CCF3 0.04 C2 C3 C3 C4 C2 C4 SADI_CCF3 0.04 O1 C2 O1 C3 O1 C4 SADI_CCF3 0.04 F1 F2 F2 F3 F3 F1 F4 F5 F5 F6 F6 F4 F7 F8 F8 F9 F9 F7 SADI_CCF3 0.02 O1 C1 SADI_CCF3 0.04 F1 C1 F2 C1 F3 C1 F4 C1 F5 C1 F6 C1 F7 C1 F8 C1 F9 C1 SIMU_CCF3 O1 > F9 RIGU_CCF3 O1 > F9 SAME_CCF3 O1 > F9 REM Restraints for Fragment tetfluorbenz, 1,2,3,4-Tetrafluorobenzene, REM C6H2F4 from: CCDC ZELDOJ, http://dx.doi.org/10.1002/anie.199515171. REM Please cite https://doi.org/10.1107/S1600576718004508 REM HFIX_TFB 43 C5 C6 SIMU_TFB F1 > C6 RIGU_TFB F1 > C6 FLAT_TFB F1 > C6 SADI_TFB 0.02 C1 C2 C2 C3 C3 C4 C4 C5 C5 C6 C6 C1 SADI_TFB 0.02 C1 F1 C2 F2 C3 F3 C4 F4 SADI_TFB 0.04 C1 C3 C3 C5 C5 C1 C2 C6 C6 C4 C2 C4 SADI_TFB 0.05 C2 F1 C6 F1 C1 F2 C3 F2 C2 F3 C4 F3 C3 F4 C5 F4 SAME_TFB F1 > C6 SIMU 0.04 0.08 1 TEMP -173.150 L.S. 10 BOND $H CONF MORE -1 LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.030900 11.082100 FVAR 0.19853 0.71782 0.80474 0.74573 AG1 6 0.057258 0.256655 0.735749 11.00000 0.01697 0.01570 = 0.01295 0.00074 0.00091 0.00191 RU1 5 0.150235 0.238088 0.624494 11.00000 0.01472 0.01582 = 0.01197 -0.00002 0.00065 0.00240 RU2 5 0.005093 0.251795 0.522231 11.00000 0.01924 0.01202 = 0.01239 0.00079 -0.00115 0.00162 RU3 5 -0.086673 0.275261 0.632447 11.00000 0.01435 0.01556 = 0.01462 0.00032 -0.00009 0.00234 RU4 5 0.084767 0.135984 0.841509 11.00000 0.01764 0.01699 = 0.01574 0.00396 0.00104 0.00135 RU5 5 0.114245 0.258085 0.949060 11.00000 0.02181 0.02985 = 0.01267 0.00291 0.00193 0.00525 RU6 5 0.083499 0.378687 0.844183 11.00000 0.01617 0.01636 = 0.01302 -0.00020 0.00230 0.00094 AL1 4 0.451399 0.245741 0.284175 11.00000 0.01531 0.01325 = 0.01421 0.00020 0.00043 0.00153 O4 2 0.108403 -0.008362 0.604762 11.00000 0.02968 0.02027 = 0.02357 0.00010 0.00010 0.00397 O5 2 0.122522 0.476750 0.517670 11.00000 0.02991 0.01799 = 0.02234 0.00311 -0.00346 0.00019 O6 2 0.143751 0.189580 0.423589 11.00000 0.06086 0.02382 = 0.02698 0.00199 0.01883 0.00267 O7 2 -0.110155 0.025521 0.525188 11.00000 0.03052 0.01553 = 0.02499 -0.00099 0.00391 -0.00189 O8 2 -0.180893 0.305179 0.433773 11.00000 0.04756 0.02374 = 0.05139 0.00231 -0.02905 0.00076 O9 2 -0.050740 0.519733 0.611422 11.00000 0.02577 0.01836 = 0.02501 -0.00045 0.00057 0.00111 O10 2 -0.205274 0.328776 0.740459 11.00000 0.02590 0.04366 = 0.02302 0.00087 0.00575 0.01137 O11 2 -0.302006 0.268913 0.557815 11.00000 0.02646 0.02859 = 0.03709 -0.00531 -0.01191 0.00195 O12 2 -0.108065 0.031233 0.657174 11.00000 0.02356 0.01980 = 0.02674 0.00424 0.00258 0.00049 O13 2 -0.158421 0.372636 0.869820 11.00000 0.02304 0.02786 = 0.02843 0.00473 0.00592 0.00255 O14 2 0.126774 0.578699 0.923402 11.00000 0.03605 0.03381 = 0.02674 -0.01312 0.00414 -0.00239 O2 2 0.318936 0.193836 0.724000 11.00000 0.02157 0.03889 = 0.01775 -0.00329 -0.00258 0.00810 O1 2 0.181414 0.483140 0.649907 11.00000 0.02153 0.02084 = 0.02685 -0.00239 0.00189 -0.00017 O15 2 0.023800 0.523604 0.741552 11.00000 0.02871 0.01893 = 0.02060 0.00250 0.00140 0.00373 O16 2 0.322687 0.380392 0.812746 11.00000 0.02107 0.02477 = 0.03462 -0.00084 0.00749 0.00102 O17 2 -0.128846 0.201505 0.961610 11.00000 0.03009 0.05249 = 0.03263 0.01630 0.00681 0.00308 O18 2 0.110909 0.437321 1.041025 11.00000 0.04743 0.05712 = 0.02096 -0.00864 0.00275 0.01226 O19 2 0.163723 0.066577 1.027103 11.00000 0.07005 0.05351 = 0.03314 0.02006 -0.00116 0.01780 O20 2 0.359448 0.316961 0.943972 11.00000 0.02534 0.05253 = 0.03255 -0.00904 -0.00087 0.00068 O21 2 -0.166269 0.136150 0.829621 11.00000 0.02193 0.03086 = 0.04456 0.00433 0.00032 0.00225 O22 2 0.079923 -0.065247 0.916500 11.00000 0.03842 0.03119 = 0.03838 0.02001 -0.00267 -0.00417 O23 2 0.087555 -0.012729 0.734417 11.00000 0.03504 0.02020 = 0.02680 -0.00098 -0.00424 0.00346 O24 2 0.335693 0.142226 0.850251 11.00000 0.02395 0.02518 = 0.03074 -0.00139 0.00130 0.00467 O3 2 0.329179 0.247541 0.539052 11.00000 0.03136 0.03499 = 0.02511 0.00494 0.00978 0.00650 C1 1 0.165902 0.393835 0.639528 11.00000 0.01384 0.02238 = 0.01487 0.00010 0.00231 0.00215 C2 1 0.250715 0.211980 0.690597 11.00000 0.01898 0.02174 = 0.01412 -0.00243 0.00100 0.00236 C3 1 0.261773 0.242697 0.569551 11.00000 0.02342 0.02118 = 0.01807 0.00250 0.00323 0.00446 C4 1 0.119346 0.082216 0.611454 11.00000 0.01978 0.02203 = 0.01377 -0.00051 -0.00019 0.00350 C5 1 0.077284 0.395451 0.522626 11.00000 0.02203 0.01385 = 0.01757 -0.00025 -0.00376 0.00384 C6 1 0.094861 0.211231 0.461016 11.00000 0.03826 0.01502 = 0.01616 0.00004 0.00474 -0.00177 C7 1 -0.064846 0.108126 0.527275 11.00000 0.02091 0.01590 = 0.01472 -0.00055 0.00013 0.00235 C8 1 -0.113589 0.287448 0.467830 11.00000 0.03008 0.01572 = 0.03119 0.00398 -0.01198 -0.00212 C9 1 -0.059978 0.429619 0.618297 11.00000 0.01615 0.02079 = 0.01729 -0.00096 -0.00031 0.00401 C10 1 -0.154779 0.307039 0.703699 11.00000 0.01410 0.02245 = 0.02199 0.00068 -0.00150 0.00229 C11 1 -0.221229 0.271565 0.584628 11.00000 0.02136 0.01709 = 0.02930 -0.00387 -0.00223 0.00432 C12 1 -0.096439 0.120138 0.646901 11.00000 0.01386 0.02480 = 0.02016 -0.00036 0.00140 0.00164 C13 1 -0.069641 0.369256 0.860879 11.00000 0.02288 0.01871 = 0.01865 0.00122 0.00402 0.00193 C14 1 0.111198 0.502996 0.894811 11.00000 0.02062 0.02912 = 0.02047 -0.00103 0.00244 0.00140 C15 1 0.047744 0.462961 0.776070 11.00000 0.01986 0.01882 = 0.01695 -0.00295 0.00269 0.00078 C16 1 0.235697 0.375805 0.825899 11.00000 0.02031 0.01561 = 0.01950 -0.00083 0.00144 0.00002 C17 1 -0.041069 0.222818 0.953807 11.00000 0.02678 0.03653 = 0.02294 0.00783 0.00310 0.00584 C18 1 0.112146 0.371620 1.007126 11.00000 0.02883 0.03887 = 0.02451 -0.00067 0.00687 0.00732 C19 1 0.146479 0.138822 0.999071 11.00000 0.03823 0.04326 = 0.02454 0.00952 0.00037 0.00760 C20 1 0.269153 0.295413 0.942560 11.00000 0.02840 0.03448 = 0.01776 -0.00248 -0.00229 0.00489 C21 1 -0.074147 0.140143 0.835109 11.00000 0.03007 0.02018 = 0.02402 0.00447 0.00158 0.00111 C22 1 0.082294 0.011220 0.889557 11.00000 0.02321 0.02998 = 0.02864 0.00974 0.00107 -0.00128 C23 1 0.084015 0.049956 0.770792 11.00000 0.01984 0.01648 = 0.02273 0.00338 -0.00359 -0.00068 C24 1 0.243862 0.145322 0.847339 11.00000 0.02334 0.01976 = 0.01710 -0.00104 0.00030 0.00244 RESI TFB 1 RESI 0 RESI CCF3 2 PART 1 21 O1 2 0.348000 0.226724 0.228643 21.00000 0.01830 0.02105 = 0.01252 -0.00251 -0.00007 0.00339 C1 1 0.243880 0.243844 0.211355 21.00000 0.01749 0.01870 = 0.01325 -0.00126 -0.00140 -0.00074 C2 1 0.221998 0.366424 0.211685 21.00000 0.02084 0.02358 = 0.02459 0.00294 -0.00071 0.00306 F1 3 0.306282 0.424001 0.194422 21.00000 0.02916 0.02295 = 0.03890 0.00928 -0.00109 -0.00078 F2 3 0.134215 0.389428 0.177108 21.00000 0.02887 0.02703 = 0.03281 0.00547 -0.00461 0.00910 F3 3 0.205844 0.402672 0.264983 21.00000 0.03005 0.02575 = 0.02755 -0.00769 -0.00309 0.00658 C3 1 0.163540 0.183923 0.250606 21.00000 0.02476 0.02777 = 0.01888 0.00117 0.00296 -0.00310 F4 3 0.157298 0.077710 0.238116 21.00000 0.04150 0.02478 = 0.03797 0.00834 0.00339 -0.00632 F5 3 0.196229 0.198136 0.306238 21.00000 0.03762 0.04357 = 0.02099 0.00722 0.00223 -0.00235 F6 3 0.062877 0.218648 0.242872 21.00000 0.02081 0.04359 = 0.03335 0.00422 0.00830 -0.00241 C4 1 0.224525 0.199358 0.147676 21.00000 0.02347 0.03131 = 0.01409 -0.00141 0.00054 -0.00347 F7 3 0.266803 0.104348 0.142473 21.00000 0.04077 0.02796 = 0.02052 -0.01173 -0.00658 0.00420 F8 3 0.118361 0.186457 0.130865 21.00000 0.02507 0.04685 = 0.02393 -0.00417 -0.00778 -0.00135 F9 3 0.271465 0.265619 0.110419 21.00000 0.02892 0.04705 = 0.02050 0.01060 0.00508 0.00557 PART 0 RESI 0 RESI CCF3 3 PART 1 31 O1 2 0.446178 0.151367 0.337936 31.00000 0.02367 0.02007 = 0.02494 0.00896 0.00260 0.00637 C1 1 0.472864 0.052913 0.357688 31.00000 0.02035 0.01720 = 0.02743 0.00565 0.00123 0.00333 C2 1 0.598757 0.048906 0.370414 31.00000 0.02286 0.02119 = 0.04908 0.00992 0.00118 0.00604 F1 3 0.641079 0.140375 0.394285 31.00000 0.02793 0.02746 = 0.06850 0.00222 -0.00683 -0.00169 F2 3 0.625754 -0.030769 0.406638 31.00000 0.03135 0.03735 = 0.06729 0.02498 -0.00668 0.01090 F3 3 0.647696 0.032960 0.321375 31.00000 0.02449 0.02671 = 0.06338 0.00767 0.01287 0.00589 C3 1 0.432903 -0.037830 0.313206 31.00000 0.02555 0.02211 = 0.03834 -0.00166 0.00850 -0.00038 F4 3 0.324559 -0.056213 0.312507 31.00000 0.02572 0.03926 = 0.05273 -0.01021 0.00366 -0.00576 F5 3 0.454985 -0.009156 0.259657 31.00000 0.04924 0.03655 = 0.03473 -0.00848 0.01288 -0.00327 F6 3 0.477635 -0.132003 0.324503 31.00000 0.03653 0.02056 = 0.07188 -0.00253 0.01679 0.00343 C4 1 0.417019 0.035406 0.415226 31.00000 0.02775 0.02265 = 0.02622 0.00858 0.00316 0.00303 F7 3 0.314383 0.062545 0.409578 31.00000 0.02790 0.04539 = 0.03666 0.01199 0.01002 0.00622 F8 3 0.416572 -0.067819 0.431682 31.00000 0.04875 0.02964 = 0.04458 0.02231 0.00586 -0.00137 F9 3 0.466730 0.096346 0.458393 31.00000 0.05423 0.04371 = 0.02570 0.00608 -0.00441 -0.00275 PART 0 RESI 0 RESI CCF3 4 PART 2 -21 O1 2 0.345836 0.236304 0.233244 -21.00000 0.02087 0.02253 = 0.01866 -0.00577 -0.00311 0.00501 C1 1 0.238751 0.239844 0.216732 -21.00000 0.01915 0.02252 = 0.01291 0.00284 -0.00441 -0.00196 C2 1 0.221733 0.327797 0.170623 -21.00000 0.02408 0.02942 = 0.02429 0.00906 0.00291 0.00520 F1 3 0.249294 0.294536 0.118567 -21.00000 0.02465 0.04960 = 0.01850 0.00984 0.00282 0.00537 F2 3 0.117803 0.352906 0.164210 -21.00000 0.02743 0.04756 = 0.03125 0.01512 -0.00170 0.01355 F3 3 0.281898 0.418701 0.182733 -21.00000 0.03622 0.02877 = 0.03851 0.01637 -0.01163 0.00339 C3 1 0.173877 0.265960 0.270247 -21.00000 0.02123 0.03241 = 0.02004 0.00240 -0.00209 0.00332 F4 3 0.213431 0.211519 0.315446 -21.00000 0.02033 0.04779 = 0.01485 0.00770 0.00401 0.00951 F5 3 0.185948 0.370373 0.285211 -21.00000 0.02352 0.03765 = 0.03385 -0.00749 0.00294 0.00802 F6 3 0.067214 0.240505 0.261910 -21.00000 0.01944 0.05475 = 0.02517 0.00295 0.00595 -0.00177 C4 1 0.195978 0.127345 0.190693 -21.00000 0.03304 0.02933 = 0.01461 -0.00259 -0.00264 -0.01116 F7 3 0.183902 0.056980 0.233529 -21.00000 0.05935 0.02997 = 0.03381 0.00786 0.01122 -0.01295 F8 3 0.100105 0.132820 0.160596 -21.00000 0.02949 0.06102 = 0.03582 -0.00757 -0.01010 -0.02037 F9 3 0.266642 0.087665 0.156740 -21.00000 0.04792 0.02806 = 0.02476 0.00171 0.00824 0.00208 PART 0 RESI 0 RESI TFB 6 PART 1 41 F1 3 0.571660 0.196249 -0.184287 41.00000 0.06549 0.06819 = 0.05035 -0.01930 0.00261 -0.00628 F2 3 0.628638 0.111035 -0.078817 41.00000 0.07231 0.03815 = 0.06896 0.01025 0.01478 0.00318 F3 3 0.665186 0.242300 0.016569 41.00000 0.06994 0.07532 = 0.03284 0.02276 0.01144 0.02500 F4 3 0.646485 0.458536 0.007437 41.00000 0.06035 0.06052 = 0.03927 -0.01430 0.00197 0.00432 C1 1 0.589142 0.261605 -0.137108 41.00000 0.02903 0.04714 = 0.03437 -0.00125 -0.00001 -0.00287 C2 1 0.617650 0.218936 -0.083438 41.00000 0.03540 0.04313 = 0.03776 0.00369 0.00744 -0.00018 C3 1 0.636853 0.285202 -0.035613 41.00000 0.03601 0.04387 = 0.03051 0.00965 0.00700 0.00362 C4 1 0.626656 0.394947 -0.040825 41.00000 0.02820 0.03532 = 0.03032 -0.00110 0.00495 -0.00247 C5 1 0.597166 0.438328 -0.093982 41.00000 0.03078 0.03963 = 0.03903 0.00455 0.00327 0.00202 AFIX 43 H5 7 0.589779 0.513974 -0.097302 41.00000 -1.20000 AFIX 0 C6 1 0.578501 0.371230 -0.142216 41.00000 0.02731 0.05025 = 0.03137 0.00449 0.00052 -0.00132 AFIX 43 H6 7 0.558283 0.400525 -0.179022 41.00000 -1.20000 AFIX 0 PART 0 RESI 0 RESI CCF3 8 PART 2 -31 O1 2 0.451084 0.154103 0.341043 -31.00000 0.02351 0.02048 = 0.01398 0.00285 0.00311 0.00413 C1 1 0.473650 0.054697 0.360911 -31.00000 0.02057 0.02068 = 0.02495 0.00631 0.00245 0.00267 C2 1 0.444407 -0.033180 0.312997 -31.00000 0.03005 0.02528 = 0.03364 -0.00187 0.00422 0.00443 F1 3 0.517150 -0.030656 0.272767 -31.00000 0.04616 0.03885 = 0.03536 -0.00187 0.01372 0.01466 F2 3 0.441746 -0.133018 0.334024 -31.00000 0.03706 0.02540 = 0.04932 0.00112 0.00390 0.00337 F3 3 0.347345 -0.018685 0.285900 -31.00000 0.03474 0.03383 = 0.03837 -0.00469 -0.00609 0.00062 C3 1 0.406398 0.031583 0.414348 -31.00000 0.02517 0.02849 = 0.02214 0.00766 0.00227 -0.00075 F4 3 0.407683 0.117767 0.449569 -31.00000 0.03745 0.03461 = 0.02107 0.00440 -0.00475 0.01024 F5 3 0.302909 0.004359 0.398056 -31.00000 0.02055 0.03181 = 0.03747 0.01273 0.00331 0.00027 F6 3 0.444384 -0.049553 0.445631 -31.00000 0.02800 0.02975 = 0.01209 0.00532 -0.00105 -0.00180 C4 1 0.596952 0.054345 0.380438 -31.00000 0.02157 0.02144 = 0.04205 0.01016 0.00012 0.00285 F7 3 0.618108 0.110185 0.430058 -31.00000 0.02060 0.03188 = 0.05068 -0.00029 -0.00721 0.00061 F8 3 0.629869 -0.045651 0.387858 -31.00000 0.02633 0.02376 = 0.03702 0.01233 -0.00536 0.00769 F9 3 0.659252 0.099146 0.341649 -31.00000 0.01995 0.03009 = 0.05763 0.02177 0.00789 0.00882 PART 0 RESI 0 RESI TFB 5 PART 2 -41 F1 3 0.602700 0.526498 -0.076992 -41.00000 0.06070 0.05396 = 0.06908 -0.00805 0.01080 -0.00236 F2 3 0.647473 0.393030 0.014513 -41.00000 0.11051 0.11104 = 0.05165 -0.01335 -0.00268 -0.01969 F3 3 0.644538 0.171282 -0.005026 -41.00000 0.09364 0.09606 = 0.07290 0.04514 0.02307 0.00041 F4 3 0.599632 0.088541 -0.112006 -41.00000 0.08823 0.04846 = 0.14260 -0.00671 -0.00132 0.00984 C1 1 0.602434 0.417945 -0.084045 -41.00000 0.03597 0.05182 = 0.04353 -0.00361 0.01190 -0.00286 C2 1 0.624555 0.349994 -0.038957 -41.00000 0.03917 0.06074 = 0.04236 0.00108 0.00235 -0.00470 C3 1 0.622273 0.240255 -0.048565 -41.00000 0.03467 0.05980 = 0.04431 0.00850 0.00679 -0.00067 C4 1 0.599581 0.197657 -0.103828 -41.00000 0.04077 0.04567 = 0.05064 0.00773 0.00222 0.00470 C5 1 0.577166 0.266005 -0.148391 -41.00000 0.03872 0.05153 = 0.03554 0.00070 0.00011 -0.00170 AFIX 43 H5 7 0.560342 0.236920 -0.186547 -41.00000 -1.20000 AFIX 0 C6 1 0.578357 0.375806 -0.139384 -41.00000 0.03168 0.04883 = 0.03721 0.00544 0.00960 -0.00080 AFIX 43 H6 7 0.562747 0.422254 -0.170965 -41.00000 -1.20000 PART 0 RESI 0 REM ##### AFIX 0 RESI CCF3 7 O1 2 0.571494 0.231712 0.251673 11.00000 0.01764 0.02231 = 0.02067 0.00100 0.00510 0.00331 C1 1 0.632779 0.249331 0.205914 11.00000 0.01958 0.02069 = 0.01831 -0.00247 0.00308 0.00223 C2 1 0.581894 0.331079 0.162920 11.00000 0.02896 0.02638 = 0.01873 -0.00019 0.00552 -0.00017 F1 3 0.503437 0.283207 0.127253 11.00000 0.03163 0.03998 = 0.02323 0.00204 -0.00338 0.00148 F2 3 0.655763 0.378516 0.129987 11.00000 0.03840 0.03680 = 0.02720 0.00725 0.01163 0.00011 F3 3 0.538048 0.409607 0.192096 11.00000 0.03745 0.02225 = 0.03152 0.00527 0.00824 0.00782 C3 1 0.747306 0.296407 0.230178 11.00000 0.01995 0.03220 = 0.02541 -0.00293 0.00495 -0.00398 F4 3 0.781707 0.245084 0.277424 11.00000 0.02501 0.04150 = 0.03195 0.00238 -0.00376 -0.00112 F5 3 0.741386 0.401434 0.244880 11.00000 0.03351 0.02860 = 0.03987 -0.00893 0.00390 -0.00940 F6 3 0.822512 0.290228 0.191460 11.00000 0.02235 0.05346 = 0.03553 -0.00342 0.01078 -0.00401 C4 1 0.644650 0.140294 0.173905 11.00000 0.03089 0.02847 = 0.02346 -0.00826 0.00239 0.00346 F7 3 0.710041 0.077550 0.205690 11.00000 0.04385 0.02941 = 0.04516 -0.00698 -0.00192 0.01741 F8 3 0.687411 0.153363 0.122567 11.00000 0.05165 0.04879 = 0.02698 -0.01289 0.01397 0.00736 F9 3 0.549708 0.086242 0.164053 11.00000 0.03926 0.02677 = 0.04332 -0.01155 -0.00439 -0.00334 RESI 0 RESI CCF3 9 O1 2 0.435661 0.371509 0.315215 11.00000 0.02176 0.01797 = 0.02066 -0.00391 -0.00130 0.00256 C1 1 0.466792 0.442793 0.358910 11.00000 0.01814 0.01494 = 0.01754 -0.00148 0.00165 0.00226 C2 1 0.493949 0.554774 0.331465 11.00000 0.02213 0.01923 = 0.02314 0.00265 -0.00273 -0.00045 F1 3 0.590555 0.553718 0.307961 11.00000 0.02685 0.03430 = 0.02994 0.00979 0.00532 -0.00246 F2 3 0.499680 0.636595 0.369916 11.00000 0.04882 0.01489 = 0.03683 -0.00429 -0.00386 0.00149 F3 3 0.420697 0.575710 0.289047 11.00000 0.03275 0.02709 = 0.02894 0.00940 -0.00816 0.00516 C3 1 0.371370 0.454389 0.399083 11.00000 0.02525 0.02370 = 0.02325 -0.00236 0.00353 0.00262 F4 3 0.326060 0.357908 0.410412 11.00000 0.03303 0.03806 = 0.04355 0.00838 0.01629 -0.00492 F5 3 0.292967 0.510319 0.372423 11.00000 0.02162 0.03812 = 0.03777 -0.00845 0.00292 0.01230 F6 3 0.402812 0.505631 0.449022 11.00000 0.03665 0.04800 = 0.02074 -0.00967 0.00631 0.00784 C4 1 0.568524 0.408035 0.396498 11.00000 0.02395 0.01787 = 0.01791 -0.00040 -0.00150 0.00099 F7 3 0.540583 0.335495 0.435845 11.00000 0.03713 0.02944 = 0.02436 0.01175 0.00095 0.00393 F8 3 0.622649 0.491017 0.425059 11.00000 0.02646 0.03007 = 0.02178 -0.00529 -0.00597 -0.00148 F9 3 0.636048 0.362719 0.362285 11.00000 0.02294 0.02875 = 0.02290 -0.00303 -0.00096 0.00973 RESI 0 HKLF 4 REM P-1_PD_a.res in P-1 REM wR2 = 0.1053, GooF = S = 1.070, Restrained GooF = 0.972 for all data REM R1 = 0.0495 for 20242 Fo > 4sig(Fo) and 0.0723 for all 26616 data REM 1444 parameters refined using 7259 restraints END WGHT 0.0309 11.0818 REM Highest difference peak 1.145, deepest hole -2.015, 1-sigma level 0.185 Q1 1 0.0831 0.2137 0.8489 11.00000 0.05 1.14 Q2 1 0.0773 0.2784 0.8415 11.00000 0.05 1.13 Q3 1 0.1431 0.3235 0.6284 11.00000 0.05 1.11 Q4 1 0.0586 0.1784 0.7296 11.00000 0.05 1.04 Q5 1 0.1991 0.2758 0.5882 11.00000 0.05 1.02 Q6 1 -0.0031 0.1565 0.5171 11.00000 0.05 1.00 Q7 1 0.1078 0.3148 0.9540 11.00000 0.05 0.98 Q8 1 0.0439 0.3293 0.7476 11.00000 0.05 0.95 Q9 1 0.5796 0.0726 -0.0479 11.00000 0.05 0.92 Q10 1 0.0569 0.3468 0.7402 11.00000 0.05 0.92 Q11 1 0.2931 0.2919 0.6697 11.00000 0.05 0.91 Q12 1 -0.0815 0.1907 0.6259 11.00000 0.05 0.85 Q13 1 0.0730 0.0344 0.8394 11.00000 0.05 0.85 Q14 1 0.0756 0.4958 0.8424 11.00000 0.05 0.84 Q15 1 0.1597 0.1220 0.6207 11.00000 0.05 0.84 Q16 1 -0.0987 0.3569 0.6410 11.00000 0.05 0.82 Q17 1 -0.0286 0.1338 0.6089 11.00000 0.05 0.82 Q18 1 0.0011 0.3425 0.5275 11.00000 0.05 0.82 Q19 1 -0.1596 0.3320 0.6120 11.00000 0.05 0.80 Q20 1 0.1015 0.3864 0.9492 11.00000 0.05 0.80 ; _shelx_res_checksum 96312 _shelx_hkl_file ; -1 0 0 3472.75 89.69 -1 0 0 3362.66 90.09 1 0 0 3457.05 90.19 -2 0 0 1922.01 60.69 -2 0 0 1903.51 52.39 -2 0 0 1897.71 52.79 2 0 0 1863.01 52.19 2 0 0 2056.89 54.29 2 0 0 1825.72 52.69 2 0 0 1957.70 55.49 -3 0 0 125.79 8.30 -3 0 0 136.09 17.00 -3 0 0 126.49 8.60 -3 0 0 124.59 7.50 -3 0 0 135.19 7.20 -3 0 0 120.69 8.60 -3 0 0 109.49 7.80 -3 0 0 136.29 15.20 -3 0 0 135.69 7.80 3 0 0 137.19 13.20 3 0 0 129.39 8.10 3 0 0 118.19 6.70 3 0 0 122.79 8.50 3 0 0 144.79 9.00 3 0 0 138.79 10.10 3 0 0 135.69 12.30 3 0 0 138.59 8.10 3 0 0 125.89 7.60 -4 0 0 5775.62 159.98 4 0 0 5849.41 160.88 -5 0 0 2562.34 98.89 -5 0 0 2634.84 73.99 -5 0 0 2583.94 78.49 -5 0 0 2765.32 96.19 -5 0 0 2520.65 76.09 -5 0 0 2580.44 76.49 -5 0 0 2533.85 75.49 -5 0 0 2595.04 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27.70 9.70 5 -2 0 23.60 6.00 5 -2 0 23.90 6.50 5 -2 0 32.50 7.70 5 -2 0 16.60 12.40 -5 2 0 34.40 7.00 -5 2 0 16.20 7.80 -5 2 0 38.40 7.90 -5 2 0 26.80 6.40 -5 2 0 22.60 8.90 -5 2 0 36.20 7.30 -5 2 0 34.90 7.30 -5 2 0 47.30 8.30 4 -2 0 511.65 21.30 4 -2 0 521.95 21.30 4 -2 0 538.45 22.00 4 -2 0 515.15 27.20 4 -2 0 517.55 22.20 4 -2 0 559.04 24.00 4 -2 0 527.45 29.80 -4 2 0 530.35 22.20 -4 2 0 530.45 21.70 -4 2 0 559.74 30.50 -4 2 0 513.05 21.40 -4 2 0 524.85 21.50 -4 2 0 548.05 28.10 -4 2 0 539.75 22.90 -4 2 0 517.65 22.20 3 -2 0 16.90 4.60 3 -2 0 9.50 5.10 3 -2 0 16.00 5.10 3 -2 0 11.80 5.60 3 -2 0 20.40 4.50 3 -2 0 14.50 4.40 3 -2 0 17.00 4.00 -3 2 0 15.90 5.90 -3 2 0 17.80 4.30 -3 2 0 12.40 5.50 -3 2 0 13.80 4.00 -3 2 0 11.80 4.00 -3 2 0 18.70 4.70 -3 2 0 24.10 5.10 2 -2 0 97.79 6.30 2 -2 0 106.69 9.10 2 -2 0 90.19 7.10 2 -2 0 93.79 9.10 2 -2 0 90.49 6.90 2 -2 0 100.69 6.70 2 -2 0 100.49 6.30 2 -2 0 94.69 7.20 -2 2 0 107.99 7.50 -2 2 0 93.09 8.60 -2 2 0 100.69 9.60 -2 2 0 102.69 6.50 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27.20 6.40 5 2 0 24.30 6.70 5 2 0 12.80 7.80 5 2 0 30.90 10.40 5 2 0 34.30 7.60 5 2 0 18.40 6.00 -6 -2 0 22.10 7.10 -6 -2 0 33.10 12.20 -6 -2 0 23.10 7.00 -6 -2 0 18.50 6.10 -6 -2 0 33.20 7.90 -6 -2 0 17.80 9.80 6 2 0 25.40 4.70 6 2 0 26.40 7.30 6 2 0 38.40 8.40 6 2 0 39.80 14.50 6 2 0 23.00 10.90 6 2 0 9.80 5.10 6 2 0 28.80 7.10 6 2 0 26.40 6.60 -7 -2 0 1.60 3.90 -7 -2 0 7.10 4.60 -7 -2 0 4.70 4.70 -7 -2 0 1.30 4.00 -7 -2 0 4.00 6.40 -7 -2 0 -2.60 5.00 7 2 0 3.20 4.00 7 2 0 -2.50 4.40 7 2 0 -2.60 3.20 7 2 0 1.40 4.80 7 2 0 2.00 4.80 7 2 0 -1.10 2.30 7 2 0 -0.40 5.00 7 2 0 -1.10 4.10 -8 -2 0 36.60 10.00 -8 -2 0 44.20 14.50 -8 -2 0 36.50 9.50 -8 -2 0 32.70 9.20 -8 -2 0 44.10 15.50 -8 -2 0 29.10 8.20 8 2 0 26.10 8.90 8 2 0 29.60 13.20 8 2 0 28.50 6.20 8 2 0 35.70 9.10 8 2 0 33.70 9.40 8 2 0 32.90 9.20 8 2 0 32.50 14.30 8 2 0 44.00 10.50 -9 -2 0 149.88 19.90 -9 -2 0 160.88 22.30 -9 -2 0 130.79 26.50 -9 -2 0 138.29 16.90 -9 -2 0 168.58 20.10 -9 -2 0 112.49 25.40 9 2 0 149.69 28.00 9 2 0 128.39 17.60 9 2 0 178.98 20.40 9 2 0 123.69 17.40 9 2 0 137.19 17.40 9 2 0 170.08 21.20 9 2 0 128.99 11.20 9 2 0 175.78 33.90 -10 -2 0 146.99 18.60 -10 -2 0 121.19 18.60 -10 -2 0 131.39 18.90 -10 -2 0 150.18 28.30 -10 -2 0 139.59 28.40 -10 -2 0 154.78 21.60 10 2 0 144.79 21.30 10 2 0 127.99 18.60 10 2 0 110.29 17.50 10 2 0 115.29 27.30 10 2 0 123.99 18.40 10 2 0 130.99 11.80 10 2 0 176.58 33.00 10 2 0 95.79 14.90 -11 -2 0 -1.30 4.70 -11 -2 0 3.40 8.40 -11 -2 0 1.40 7.30 -11 -2 0 5.90 9.30 -11 -2 0 1.90 6.00 -11 -2 0 11.00 7.60 11 2 0 9.40 7.30 11 2 0 8.40 7.70 11 2 0 2.60 5.60 11 2 0 19.50 12.40 11 2 0 -2.10 4.30 11 2 0 6.50 4.90 11 2 0 -4.80 5.30 11 2 0 0.40 6.90 -12 -2 0 108.79 17.70 -12 -2 0 84.59 15.40 -12 -2 0 86.49 18.10 -12 -2 0 122.09 19.70 -12 -2 0 120.59 29.80 -12 -2 0 63.99 26.60 12 2 0 150.98 32.90 12 2 0 98.99 18.20 12 2 0 80.89 16.60 12 2 0 111.29 28.50 12 2 0 104.89 13.90 12 2 0 99.39 18.10 12 2 0 132.09 33.40 12 2 0 148.69 23.50 -13 -2 0 162.38 23.90 -13 -2 0 108.69 29.70 -13 -2 0 178.38 26.90 -13 -2 0 169.18 25.40 -13 -2 0 184.18 36.80 -13 -2 0 173.08 22.50 13 2 0 163.28 24.20 13 2 0 155.98 35.10 13 2 0 174.38 15.30 13 2 0 205.58 27.90 13 2 0 200.38 43.10 13 2 0 134.29 22.60 13 2 0 171.68 25.10 -14 -2 0 161.68 22.00 -14 -2 0 138.79 23.00 -14 -2 0 161.88 34.60 -14 -2 0 119.99 23.60 -14 -2 0 116.19 34.30 -14 -2 0 122.19 21.30 14 2 0 148.99 25.80 14 2 0 160.58 18.00 14 2 0 127.09 16.60 14 2 0 156.48 25.90 14 2 0 125.49 21.70 14 2 0 143.29 39.00 14 2 0 107.59 30.10 14 2 0 163.48 23.60 14 2 0 169.08 27.60 -15 -2 0 28.40 13.00 -15 -2 0 48.60 13.20 -15 -2 0 45.30 15.20 -15 -2 0 24.10 10.50 -15 -2 0 37.40 20.10 -15 -2 0 38.40 19.60 15 2 0 41.20 17.90 15 2 0 54.49 15.60 15 2 0 52.09 11.60 15 2 0 65.39 18.00 15 2 0 84.79 15.00 15 2 0 58.59 16.50 15 2 0 36.50 22.50 15 2 0 35.90 23.60 15 2 0 49.80 15.00 -16 -2 0 22.70 10.40 -16 -2 0 51.39 17.80 -16 -2 0 49.00 14.50 -16 -2 0 30.10 22.20 -16 -2 0 15.00 15.10 -16 -2 0 25.50 14.70 16 2 0 27.30 11.90 16 2 0 36.80 20.80 16 2 0 40.10 17.00 16 2 0 7.50 13.20 16 2 0 29.60 15.70 -17 -2 0 11.10 12.10 -17 -2 0 -3.60 11.00 -17 -2 0 1.80 23.40 -17 -2 0 -1.90 7.50 17 2 0 1.70 5.90 17 2 0 2.10 10.60 17 2 0 1.50 10.10 17 2 0 8.30 13.00 17 2 0 5.00 11.30 17 2 0 3.30 7.70 -18 -2 0 -3.00 9.90 -18 -2 0 -3.10 10.40 18 2 0 -3.30 15.40 18 2 0 -2.60 8.70 18 2 0 -5.20 7.10 18 2 0 3.90 16.20 18 2 0 -11.60 13.00 18 -3 0 3.20 11.50 18 -3 0 3.90 8.30 18 -3 0 27.30 15.60 -18 3 0 7.80 12.20 17 -3 0 4.70 8.10 17 -3 0 18.40 23.70 17 -3 0 16.00 10.80 17 -3 0 24.50 14.90 -17 3 0 -1.50 6.30 -17 3 0 43.50 18.50 16 -3 0 -0.50 10.20 16 -3 0 19.70 9.80 16 -3 0 25.00 10.30 16 -3 0 33.60 13.30 16 -3 0 30.90 16.00 16 -3 0 42.00 14.10 -16 3 0 45.20 14.60 -16 3 0 27.10 14.10 -16 3 0 21.30 18.60 -16 3 0 53.29 19.70 15 -3 0 91.39 17.40 15 -3 0 88.09 20.20 15 -3 0 102.39 18.40 15 -3 0 88.99 32.80 15 -3 0 118.09 23.40 15 -3 0 54.39 17.30 15 -3 0 89.89 27.20 -15 3 0 57.29 16.20 -15 3 0 73.09 17.60 -15 3 0 88.39 19.10 -15 3 0 75.79 25.30 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94.69 17.30 -11 3 0 118.09 24.40 -11 3 0 65.19 25.20 -11 3 0 94.29 26.10 -11 3 0 87.89 16.30 -11 3 0 90.99 17.70 10 -3 0 74.59 21.50 10 -3 0 69.19 15.30 10 -3 0 90.09 19.10 10 -3 0 99.59 15.20 10 -3 0 68.19 13.80 10 -3 0 91.69 14.20 10 -3 0 81.89 21.40 -10 3 0 61.19 18.90 -10 3 0 79.39 15.30 -10 3 0 62.19 12.70 -10 3 0 78.49 15.40 -10 3 0 52.39 12.20 -10 3 0 70.39 13.90 -10 3 0 62.99 20.10 9 -3 0 669.93 32.30 9 -3 0 644.04 33.90 9 -3 0 630.34 41.70 9 -3 0 657.83 48.50 9 -3 0 614.74 32.00 9 -3 0 606.24 32.40 9 -3 0 608.74 43.90 -9 3 0 619.14 31.60 -9 3 0 651.83 45.20 -9 3 0 637.34 32.80 -9 3 0 607.94 33.20 -9 3 0 690.13 50.49 -9 3 0 600.74 37.30 -9 3 0 652.73 33.80 -9 3 0 730.53 35.20 8 -3 0 530.55 41.00 8 -3 0 560.74 28.60 8 -3 0 518.15 27.90 8 -3 0 512.35 37.50 8 -3 0 518.35 30.60 8 -3 0 541.25 27.20 8 -3 0 570.34 29.40 -8 3 0 521.65 28.50 -8 3 0 544.55 38.40 -8 3 0 498.85 27.00 -8 3 0 510.95 27.60 -8 3 0 541.95 28.90 -8 3 0 521.65 28.50 -8 3 0 545.05 28.70 -8 3 0 534.45 41.80 7 -3 0 501.65 25.10 7 -3 0 530.35 26.80 7 -3 0 506.25 34.90 7 -3 0 563.14 29.30 7 -3 0 581.14 27.90 7 -3 0 452.55 35.90 7 -3 0 520.65 26.10 -7 3 0 531.85 26.90 -7 3 0 464.45 26.10 -7 3 0 496.85 25.70 -7 3 0 558.34 36.40 -7 3 0 552.54 27.10 -7 3 0 507.35 38.00 -7 3 0 576.14 27.10 -7 3 0 511.85 27.00 6 -3 0 10.50 4.90 6 -3 0 9.20 4.80 6 -3 0 13.80 7.80 6 -3 0 7.30 6.60 6 -3 0 8.20 4.90 6 -3 0 10.90 6.10 6 -3 0 4.30 3.80 -6 3 0 10.10 5.70 -6 3 0 11.30 7.00 -6 3 0 12.20 5.10 -6 3 0 7.90 4.20 -6 3 0 10.60 5.30 -6 3 0 7.90 4.40 -6 3 0 2.60 3.70 -6 3 0 -1.20 5.40 5 -3 0 46.60 8.10 5 -3 0 50.09 10.00 5 -3 0 56.49 8.40 5 -3 0 57.49 13.60 5 -3 0 48.20 8.90 5 -3 0 54.79 11.50 5 -3 0 48.80 8.70 -5 3 0 49.60 9.30 -5 3 0 37.30 7.40 -5 3 0 34.50 7.40 -5 3 0 38.90 8.80 -5 3 0 54.39 9.50 -5 3 0 39.60 12.30 -5 3 0 38.10 10.50 4 -3 0 13.30 5.40 4 -3 0 5.50 3.70 4 -3 0 0.10 3.20 4 -3 0 2.90 3.20 4 -3 0 1.10 2.80 -4 3 0 5.50 4.60 -4 3 0 3.70 4.00 -4 3 0 5.10 4.60 -4 3 0 0.70 2.90 -4 3 0 0.70 2.80 -4 3 0 3.60 5.20 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0 32.90 8.30 -2 -3 0 34.80 5.70 -2 -3 0 42.20 8.90 2 3 0 40.50 6.80 2 3 0 35.40 6.40 2 3 0 35.00 9.40 -3 -3 0 18.00 7.00 -3 -3 0 13.30 4.10 -3 -3 0 15.90 7.10 -3 -3 0 15.40 4.60 -3 -3 0 17.90 5.10 3 3 0 15.20 4.50 3 3 0 18.80 7.30 3 3 0 14.80 5.10 3 3 0 15.10 4.50 3 3 0 12.00 4.40 3 3 0 14.40 6.80 -4 -3 0 3.90 3.40 -4 -3 0 2.10 3.20 -4 -3 0 0.90 4.10 -4 -3 0 1.40 3.30 -4 -3 0 -4.40 3.20 -4 -3 0 -0.10 3.20 4 3 0 1.30 2.80 4 3 0 -4.10 3.00 4 3 0 -1.20 2.80 4 3 0 4.00 2.90 4 3 0 2.20 4.90 4 3 0 3.10 3.40 4 3 0 -1.00 3.00 -5 -3 0 106.59 18.90 -5 -3 0 183.08 23.90 -5 -3 0 158.88 12.10 -5 -3 0 165.58 25.60 -5 -3 0 175.98 13.10 -5 -3 0 162.48 11.90 5 3 0 173.58 26.60 5 3 0 161.98 12.70 5 3 0 205.78 25.40 5 3 0 144.49 11.00 5 3 0 155.58 12.40 5 3 0 152.78 12.90 5 3 0 154.68 13.00 -6 -3 0 109.79 13.90 -6 -3 0 70.39 15.20 -6 -3 0 74.59 12.10 -6 -3 0 105.89 36.50 -6 -3 0 107.29 13.30 -6 -3 0 96.79 11.40 6 3 0 94.29 20.40 6 3 0 99.99 13.80 6 3 0 105.49 14.20 6 3 0 101.99 12.80 6 3 0 79.99 11.20 6 3 0 93.69 13.40 6 3 0 110.39 20.40 -7 -3 0 1.70 5.90 -7 -3 0 15.30 6.70 -7 -3 0 12.60 5.30 -7 -3 0 7.40 6.10 -7 -3 0 3.50 8.60 -7 -3 0 10.00 8.00 7 3 0 9.40 6.10 7 3 0 13.00 6.00 7 3 0 6.80 9.40 7 3 0 15.10 10.00 7 3 0 18.80 7.10 7 3 0 15.40 6.40 7 3 0 8.10 5.10 -8 -3 0 328.27 20.30 -8 -3 0 305.27 21.10 -8 -3 0 314.37 22.80 -8 -3 0 351.76 40.00 -8 -3 0 325.17 22.50 -8 -3 0 278.67 38.70 8 3 0 360.16 23.20 8 3 0 340.37 22.60 8 3 0 389.06 43.40 8 3 0 387.26 37.20 8 3 0 308.07 21.30 8 3 0 344.37 23.50 8 3 0 348.17 21.90 -9 -3 0 1387.46 57.19 -9 -3 0 1202.28 68.89 -9 -3 0 1446.76 56.89 -9 -3 0 1339.47 76.99 -9 -3 0 1356.16 52.19 -9 -3 0 1336.77 53.89 9 3 0 1353.16 53.79 9 3 0 1486.75 81.69 9 3 0 1392.76 55.69 9 3 0 1340.07 73.89 9 3 0 1333.47 56.49 9 3 0 1333.87 54.09 -10 -3 0 277.57 42.20 -10 -3 0 283.97 23.90 -10 -3 0 270.57 40.80 -10 -3 0 291.57 22.80 -10 -3 0 291.37 23.30 -10 -3 0 294.67 21.40 10 3 0 267.77 23.40 10 3 0 283.17 22.50 10 3 0 275.47 22.30 10 3 0 380.96 47.40 10 3 0 274.47 22.40 10 3 0 299.77 17.30 10 3 0 284.37 22.60 10 3 0 314.67 45.50 -11 -3 0 9.90 10.80 -11 -3 0 7.20 9.40 -11 -3 0 -0.20 7.40 -11 -3 0 3.20 6.20 -11 -3 0 1.90 7.20 11 3 0 14.10 7.90 11 3 0 5.60 7.30 11 3 0 12.50 12.80 11 3 0 4.10 4.70 11 3 0 27.50 14.80 11 3 0 8.60 7.60 11 3 0 0.60 4.80 -12 -3 0 1.10 5.90 -12 -3 0 -4.60 5.90 -12 -3 0 2.50 7.40 -12 -3 0 -3.10 8.00 -12 -3 0 -2.10 5.90 -12 -3 0 8.50 8.50 12 3 0 2.00 8.60 12 3 0 10.20 7.70 12 3 0 -3.50 4.60 12 3 0 9.40 6.60 12 3 0 -4.10 7.10 12 3 0 -1.70 6.90 12 3 0 -0.20 8.20 -13 -3 0 203.68 39.00 -13 -3 0 223.08 24.90 -13 -3 0 127.79 21.40 -13 -3 0 212.18 30.10 -13 -3 0 185.28 26.50 -13 -3 0 202.98 41.20 13 3 0 174.88 23.80 13 3 0 229.98 17.20 13 3 0 211.28 27.60 13 3 0 192.18 28.10 13 3 0 191.28 38.80 13 3 0 236.68 76.89 13 3 0 188.28 26.30 13 3 0 173.38 29.20 -14 -3 0 102.59 30.60 -14 -3 0 142.49 38.60 -14 -3 0 153.28 23.50 -14 -3 0 229.48 45.60 -14 -3 0 153.78 22.60 -14 -3 0 175.88 27.70 14 3 0 133.09 24.10 14 3 0 151.48 23.30 14 3 0 185.68 40.00 14 3 0 193.78 27.80 14 3 0 144.49 44.20 14 3 0 179.38 28.30 14 3 0 152.38 24.80 -15 -3 0 143.89 27.10 -15 -3 0 136.99 21.00 -15 -3 0 39.30 23.50 -15 -3 0 149.49 24.50 -15 -3 0 107.29 29.70 -15 -3 0 105.59 21.20 15 3 0 107.89 22.10 15 3 0 155.68 27.90 15 3 0 146.39 24.90 15 3 0 167.58 40.90 15 3 0 141.29 43.00 15 3 0 145.89 25.70 15 3 0 108.99 22.00 -16 -3 0 50.99 16.50 -16 -3 0 21.30 18.80 -16 -3 0 20.30 11.40 -16 -3 0 34.40 15.10 -16 -3 0 19.40 14.50 16 3 0 18.80 11.90 16 3 0 38.00 25.20 16 3 0 24.90 11.70 16 3 0 40.10 14.90 16 3 0 18.80 10.60 16 3 0 21.30 12.50 -17 -3 0 2.20 13.70 -17 -3 0 15.60 11.70 -17 -3 0 37.20 17.90 -17 -3 0 19.00 13.90 17 3 0 37.20 16.40 17 3 0 11.50 14.40 -18 -3 0 0.00 10.50 -18 -3 0 17.90 12.30 -18 -3 0 42.80 42.70 -18 -3 0 0.30 11.80 18 3 0 1.80 13.90 18 3 0 -8.90 9.40 18 3 0 -1.40 9.60 18 -4 0 148.39 30.20 -18 4 0 172.98 32.80 17 -4 0 76.59 20.80 17 -4 0 92.99 19.90 17 -4 0 109.99 27.80 17 -4 0 106.89 24.80 17 -4 0 111.09 40.10 -17 4 0 127.39 28.40 16 -4 0 0.50 6.20 16 -4 0 -0.90 8.60 16 -4 0 12.00 8.80 16 -4 0 2.10 8.50 16 -4 0 3.70 8.80 16 -4 0 15.90 9.00 -16 4 0 -0.80 4.80 -16 4 0 22.80 12.80 -16 4 0 11.50 10.90 -16 4 0 0.00 11.30 15 -4 0 2.70 5.20 15 -4 0 0.00 6.60 15 -4 0 1.50 5.70 15 -4 0 4.80 6.30 15 -4 0 6.10 9.10 15 -4 0 0.10 9.90 -15 4 0 4.30 8.50 -15 4 0 7.90 11.50 -15 4 0 -2.20 3.80 -15 4 0 6.30 7.00 14 -4 0 31.70 16.70 14 -4 0 70.89 19.40 14 -4 0 83.69 28.80 14 -4 0 43.90 11.40 14 -4 0 84.49 19.70 14 -4 0 66.19 16.50 14 -4 0 52.39 13.10 -14 4 0 45.40 13.60 -14 4 0 22.10 15.00 -14 4 0 72.49 18.80 -14 4 0 69.39 16.50 -14 4 0 87.79 28.50 -14 4 0 29.60 12.00 -14 4 0 66.49 16.60 13 -4 0 34.80 13.10 13 -4 0 59.49 13.30 13 -4 0 55.09 14.70 13 -4 0 48.50 13.00 -13 4 0 55.99 14.80 -13 4 0 45.60 13.50 -13 4 0 86.69 31.10 -13 4 0 69.99 24.30 -13 4 0 81.09 17.50 -13 4 0 66.19 17.10 -13 4 0 42.20 14.60 12 -4 0 107.09 18.10 12 -4 0 98.89 16.30 12 -4 0 99.99 37.00 12 -4 0 84.49 17.10 12 -4 0 69.39 16.30 12 -4 0 105.29 27.30 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82.19 18.40 16 -5 0 45.40 13.60 -16 5 0 54.69 17.70 -16 5 0 58.89 18.60 15 -5 0 88.89 23.90 15 -5 0 144.29 24.70 15 -5 0 106.99 33.10 15 -5 0 108.89 19.90 15 -5 0 141.39 24.90 15 -5 0 109.29 21.70 -15 5 0 82.89 21.20 -15 5 0 117.59 34.00 -15 5 0 94.39 22.10 14 -5 0 95.19 17.60 14 -5 0 122.09 25.90 14 -5 0 138.39 21.20 14 -5 0 80.69 17.30 14 -5 0 118.59 23.60 14 -5 0 71.59 23.30 -14 5 0 81.89 21.10 -14 5 0 68.89 15.30 -14 5 0 80.69 17.60 -14 5 0 58.19 23.80 -14 5 0 99.19 19.40 13 -5 0 91.39 26.20 13 -5 0 111.19 21.10 13 -5 0 68.49 18.70 13 -5 0 67.39 18.00 13 -5 0 135.79 21.30 13 -5 0 124.19 33.50 13 -5 0 89.09 16.70 -13 5 0 100.19 19.50 -13 5 0 100.89 18.70 -13 5 0 88.69 28.80 -13 5 0 83.89 19.70 -13 5 0 116.69 24.00 -13 5 0 114.99 28.60 12 -5 0 4.60 7.80 12 -5 0 34.50 12.30 12 -5 0 22.10 11.70 12 -5 0 31.40 10.40 12 -5 0 27.40 10.40 -12 5 0 36.60 18.70 -12 5 0 51.09 14.30 -12 5 0 43.20 30.10 -12 5 0 39.50 11.50 -12 5 0 33.00 13.20 -12 5 0 17.70 9.40 11 -5 0 8.60 7.10 11 -5 0 24.70 9.60 11 -5 0 11.00 7.50 11 -5 0 22.30 11.10 11 -5 0 20.90 8.10 11 -5 0 38.30 15.60 11 -5 0 20.30 11.90 -11 5 0 13.50 7.80 -11 5 0 21.20 9.70 -11 5 0 15.90 8.60 -11 5 0 32.80 17.30 -11 5 0 23.70 13.50 -11 5 0 29.10 11.50 10 -5 0 16.80 11.60 10 -5 0 -0.30 4.80 10 -5 0 15.50 8.00 10 -5 0 3.90 6.50 10 -5 0 4.30 8.00 10 -5 0 4.20 7.80 -10 5 0 8.70 7.80 -10 5 0 5.00 7.30 -10 5 0 -0.50 5.90 -10 5 0 11.00 6.10 -10 5 0 21.70 13.80 9 -5 0 1545.15 94.69 9 -5 0 1568.14 59.19 9 -5 0 1529.15 61.29 9 -5 0 1610.54 59.79 9 -5 0 1455.05 73.89 9 -5 0 1569.24 64.39 9 -5 0 1511.95 60.99 -9 5 0 1650.83 64.19 -9 5 0 1410.76 60.89 -9 5 0 1619.74 77.79 -9 5 0 1501.15 81.09 -9 5 0 1556.04 60.29 8 -5 0 559.14 28.90 8 -5 0 556.14 30.70 8 -5 0 625.24 40.90 8 -5 0 580.24 29.70 8 -5 0 507.75 34.30 8 -5 0 572.24 42.90 8 -5 0 581.04 30.80 -8 5 0 564.44 40.30 -8 5 0 543.05 31.50 -8 5 0 569.24 43.60 -8 5 0 567.84 30.00 -8 5 0 533.85 30.70 -8 5 0 524.55 28.30 7 -5 0 543.55 27.00 7 -5 0 530.45 27.70 7 -5 0 495.95 29.70 7 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202.98 17.80 -8 -5 0 661.23 55.99 -8 -5 0 678.53 32.00 -8 -5 0 659.63 33.20 -8 -5 0 613.24 34.80 -8 -5 0 525.35 45.80 8 5 0 651.53 35.90 8 5 0 648.64 48.00 8 5 0 634.64 30.20 8 5 0 676.63 35.50 8 5 0 678.13 35.10 8 5 0 622.44 50.89 8 5 0 633.04 33.30 -9 -5 0 408.66 29.20 -9 -5 0 352.96 48.10 -9 -5 0 423.76 28.40 -9 -5 0 457.55 28.30 -9 -5 0 422.56 25.70 -9 -5 0 459.65 40.70 9 5 0 485.35 30.70 9 5 0 469.15 54.79 9 5 0 427.96 29.90 9 5 0 415.86 25.60 9 5 0 410.96 28.00 9 5 0 517.65 29.90 9 5 0 454.85 57.09 -10 -5 0 89.19 17.00 -10 -5 0 112.69 26.80 -10 -5 0 113.29 20.10 -10 -5 0 88.59 24.80 -10 -5 0 116.99 18.20 -10 -5 0 150.08 20.60 10 5 0 123.99 32.80 10 5 0 162.58 32.50 10 5 0 115.59 20.00 10 5 0 98.59 16.50 10 5 0 102.39 17.70 10 5 0 125.19 18.10 10 5 0 126.59 21.00 -11 -5 0 34.60 11.60 -11 -5 0 26.10 10.90 -11 -5 0 40.20 13.90 -11 -5 0 120.79 34.30 -11 -5 0 75.99 26.10 -11 -5 0 66.69 14.00 11 5 0 99.29 28.30 11 5 0 31.10 18.00 11 5 0 44.40 12.50 11 5 0 50.59 14.20 11 5 0 47.80 14.40 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68.19 29.30 15 5 0 117.59 21.70 -16 -5 0 53.99 26.80 -16 -5 0 72.59 27.40 -16 -5 0 50.59 19.10 -16 -5 0 15.00 10.80 -16 -5 0 32.70 20.20 16 5 0 42.60 15.40 16 5 0 -1.60 9.60 16 5 0 11.20 12.10 16 5 0 23.90 12.20 16 5 0 -2.80 6.60 16 5 0 14.40 10.80 -17 -5 0 9.90 17.40 -17 -5 0 15.10 12.40 -17 -5 0 20.80 13.80 -17 -5 0 1.80 11.00 17 5 0 1.60 10.30 17 5 0 -6.60 8.40 17 5 0 3.60 9.80 17 5 0 5.20 16.80 18 -6 0 73.59 24.60 -18 6 0 42.70 20.30 17 -6 0 -1.70 12.20 17 -6 0 -2.90 6.50 -17 6 0 15.40 12.80 16 -6 0 -1.00 11.10 16 -6 0 -0.90 6.20 16 -6 0 8.20 12.90 16 -6 0 6.10 8.20 16 -6 0 13.80 15.50 -16 6 0 3.70 11.90 -16 6 0 1.20 13.20 -16 6 0 0.10 6.40 15 -6 0 0.60 5.00 15 -6 0 1.40 10.60 15 -6 0 14.40 13.40 15 -6 0 8.30 7.10 15 -6 0 0.80 6.40 15 -6 0 6.70 6.60 -15 6 0 1.10 7.30 -15 6 0 0.30 6.00 -15 6 0 0.10 9.20 -15 6 0 5.70 13.10 14 -6 0 3.30 9.60 14 -6 0 15.80 9.00 14 -6 0 22.50 12.00 14 -6 0 26.50 11.20 14 -6 0 20.80 11.30 14 -6 0 29.90 14.10 -14 6 0 6.00 8.10 -14 6 0 22.80 10.90 -14 6 0 18.00 13.60 13 -6 0 11.80 11.20 13 -6 0 7.90 7.40 13 -6 0 3.20 5.30 13 -6 0 18.70 14.00 13 -6 0 19.00 8.80 13 -6 0 7.40 6.60 13 -6 0 6.40 10.50 -13 6 0 0.00 5.40 -13 6 0 3.40 10.20 -13 6 0 -1.60 7.70 -13 6 0 -0.10 7.40 12 -6 0 124.29 36.70 12 -6 0 82.69 17.90 12 -6 0 99.49 21.30 12 -6 0 83.09 15.90 12 -6 0 108.29 18.30 -12 6 0 123.99 24.60 -12 6 0 76.29 23.80 -12 6 0 60.39 19.50 -12 6 0 105.59 20.30 -12 6 0 75.59 22.80 -12 6 0 108.29 20.80 11 -6 0 41.60 23.20 11 -6 0 20.00 9.00 11 -6 0 7.90 9.50 11 -6 0 35.20 15.50 11 -6 0 6.50 7.10 11 -6 0 15.40 7.90 -11 6 0 -3.70 7.70 -11 6 0 13.40 7.40 -11 6 0 16.50 9.70 -11 6 0 28.00 13.70 -11 6 0 5.00 6.50 -11 6 0 23.90 14.70 10 -6 0 13.40 7.40 10 -6 0 5.80 4.80 10 -6 0 9.30 8.60 10 -6 0 4.40 6.70 10 -6 0 0.50 8.10 10 -6 0 9.30 6.20 10 -6 0 3.20 5.80 -10 6 0 4.70 9.00 -10 6 0 20.20 13.10 -10 6 0 5.00 5.20 -10 6 0 5.40 8.10 -10 6 0 12.90 9.40 -10 6 0 18.30 8.90 9 -6 0 110.59 20.70 9 -6 0 103.29 16.10 9 -6 0 106.09 24.20 9 -6 0 129.49 25.20 9 -6 0 103.29 19.00 9 -6 0 114.69 16.40 9 -6 0 101.89 17.40 -9 6 0 101.49 35.10 -9 6 0 87.99 15.80 -9 6 0 113.39 20.40 -9 6 0 87.09 17.80 -9 6 0 130.69 26.90 -9 6 0 90.89 14.30 -9 6 0 105.69 16.70 8 -6 0 83.79 14.80 8 -6 0 85.49 16.40 8 -6 0 75.99 12.30 8 -6 0 109.99 16.20 8 -6 0 95.79 15.80 8 -6 0 89.49 31.20 8 -6 0 72.69 18.90 -8 6 0 107.09 20.70 -8 6 0 94.79 13.90 -8 6 0 80.89 15.10 -8 6 0 103.79 21.70 -8 6 0 58.69 14.10 -8 6 0 90.09 13.40 -8 6 0 66.59 18.70 7 -6 0 72.29 13.30 7 -6 0 100.49 14.70 7 -6 0 88.89 12.50 7 -6 0 94.39 18.90 7 -6 0 96.89 21.00 7 -6 0 78.49 12.70 7 -6 0 66.89 14.50 -7 6 0 93.19 16.00 -7 6 0 101.89 21.60 -7 6 0 108.99 17.50 -7 6 0 96.59 19.40 -7 6 0 83.99 12.40 -7 6 0 77.39 11.80 -7 6 0 51.79 11.00 6 -6 0 17.70 6.10 6 -6 0 13.90 8.20 6 -6 0 10.80 5.70 6 -6 0 4.80 4.60 6 -6 0 8.20 6.10 6 -6 0 8.20 4.60 6 -6 0 14.60 6.50 -6 6 0 13.10 7.90 -6 6 0 7.70 4.70 -6 6 0 7.30 6.40 -6 6 0 11.50 7.50 -6 6 0 5.00 4.80 -6 6 0 14.90 7.60 -6 6 0 1.90 4.10 5 -6 0 -0.50 4.10 5 -6 0 8.80 6.70 5 -6 0 6.80 4.10 5 -6 0 6.90 5.80 5 -6 0 6.90 4.00 5 -6 0 0.90 3.80 5 -6 0 1.10 4.50 -5 6 0 1.70 4.30 -5 6 0 9.70 6.90 -5 6 0 8.60 7.10 -5 6 0 2.20 4.90 -5 6 0 6.10 5.30 4 -6 0 17.50 5.10 4 -6 0 10.90 5.50 4 -6 0 21.90 8.40 4 -6 0 32.60 8.70 4 -6 0 12.70 6.80 -4 6 0 19.90 8.30 -4 6 0 7.60 5.70 -4 6 0 18.70 7.60 -4 6 0 25.70 7.90 -4 6 0 12.70 6.40 3 -6 0 31.50 7.70 3 -6 0 11.40 6.30 3 -6 0 35.60 8.40 3 -6 0 33.40 9.60 3 -6 0 36.90 8.80 -3 6 0 14.10 6.60 -3 6 0 19.80 6.60 -3 6 0 18.90 7.20 -3 6 0 18.10 7.90 2 -6 0 0.40 3.50 2 -6 0 -0.40 3.50 2 -6 0 -5.00 3.80 2 -6 0 3.60 3.20 -2 6 0 -1.00 3.70 -2 6 0 -2.50 3.90 -2 6 0 3.30 3.90 -2 6 0 -2.90 4.50 1 -6 0 143.29 18.60 1 -6 0 155.48 18.90 1 -6 0 141.89 16.00 1 -6 0 132.99 10.50 -1 6 0 134.79 18.80 -1 6 0 145.99 16.90 0 -6 0 3547.34 113.19 0 -6 0 3482.85 110.49 0 -6 0 3482.45 105.29 0 6 0 3595.84 105.79 0 6 0 3473.35 106.29 -1 -6 0 1904.91 56.49 -1 -6 0 1841.52 69.89 -1 -6 0 1972.00 64.89 -1 -6 0 1917.11 73.19 -1 -6 0 1905.81 72.09 1 6 0 1921.91 59.59 1 6 0 1997.70 57.69 1 6 0 1895.51 64.79 1 6 0 1947.71 66.09 -2 -6 0 1116.49 42.70 -2 -6 0 1081.49 38.20 -2 -6 0 1074.99 39.50 -2 -6 0 1170.58 53.49 -2 -6 0 1054.79 49.90 -2 -6 0 1091.69 49.10 -2 -6 0 1079.39 39.40 2 6 0 1054.59 39.60 2 6 0 1092.09 43.10 -3 -6 0 13.20 6.80 -3 -6 0 12.00 5.40 -3 -6 0 11.60 4.60 -3 -6 0 5.30 5.80 -3 -6 0 8.70 4.00 3 6 0 3.60 4.60 3 6 0 1.90 3.10 3 6 0 9.20 4.30 3 6 0 11.70 5.70 -4 -6 0 27.70 11.90 -4 -6 0 29.90 7.70 -4 -6 0 23.70 7.10 -4 -6 0 18.70 6.20 -4 -6 0 13.40 8.80 4 6 0 27.00 7.50 4 6 0 28.00 6.80 4 6 0 24.10 7.60 4 6 0 24.50 10.00 4 6 0 19.00 7.20 -5 -6 0 133.79 23.50 -5 -6 0 152.88 17.20 -5 -6 0 137.09 24.90 -5 -6 0 131.99 17.00 -5 -6 0 121.69 15.10 -5 -6 0 105.69 15.00 5 6 0 108.89 15.10 5 6 0 154.58 16.60 5 6 0 123.29 26.30 5 6 0 140.49 18.00 -6 -6 0 1.50 4.50 -6 -6 0 2.10 4.00 -6 -6 0 7.50 5.60 -6 -6 0 3.20 6.90 -6 -6 0 9.90 5.80 -6 -6 0 -3.80 3.90 6 6 0 5.30 8.00 6 6 0 -2.70 3.10 6 6 0 3.80 5.90 6 6 0 7.90 5.80 6 6 0 2.80 5.00 6 6 0 0.70 5.10 -7 -6 0 307.17 20.50 -7 -6 0 301.07 21.50 -7 -6 0 271.37 20.80 -7 -6 0 245.28 33.10 -7 -6 0 294.37 39.70 -7 -6 0 255.97 21.30 7 6 0 274.27 22.10 7 6 0 354.36 49.40 7 6 0 277.77 21.70 7 6 0 253.57 21.10 7 6 0 250.47 19.60 7 6 0 345.67 42.80 -8 -6 0 33.10 9.00 -8 -6 0 4.70 7.70 -8 -6 0 14.50 7.90 -8 -6 0 7.00 11.10 -8 -6 0 24.90 8.60 -8 -6 0 1.10 5.40 8 6 0 16.60 7.40 8 6 0 8.40 6.70 8 6 0 17.30 7.90 8 6 0 28.20 15.30 8 6 0 33.00 12.20 8 6 0 24.10 12.80 -9 -6 0 22.50 9.70 -9 -6 0 36.00 10.50 -9 -6 0 31.70 10.50 -9 -6 0 5.30 7.00 -9 -6 0 37.40 15.80 -9 -6 0 16.70 9.30 9 6 0 2.30 8.20 9 6 0 25.50 14.00 9 6 0 27.60 9.80 9 6 0 31.10 10.40 9 6 0 28.10 11.00 9 6 0 32.30 12.40 -10 -6 0 158.08 22.10 -10 -6 0 153.78 24.70 -10 -6 0 144.19 19.10 -10 -6 0 115.99 29.40 -10 -6 0 173.18 35.70 -10 -6 0 183.68 25.00 10 6 0 138.39 20.10 10 6 0 121.29 32.00 10 6 0 161.38 19.80 10 6 0 155.08 25.40 10 6 0 201.38 27.40 10 6 0 136.09 31.20 10 6 0 171.48 22.60 -11 -6 0 22.00 10.60 -11 -6 0 30.20 11.80 -11 -6 0 20.70 8.60 -11 -6 0 33.40 13.70 -11 -6 0 27.80 16.60 -11 -6 0 42.80 21.80 11 6 0 51.79 23.00 11 6 0 32.30 12.00 11 6 0 2.10 9.10 11 6 0 20.50 9.50 11 6 0 42.40 13.40 11 6 0 25.70 12.20 -12 -6 0 6.00 7.40 -12 -6 0 -6.10 6.80 -12 -6 0 6.10 10.40 -12 -6 0 0.30 5.90 -12 -6 0 -3.30 6.90 12 6 0 1.90 4.80 12 6 0 2.50 5.10 12 6 0 7.30 6.80 12 6 0 -1.90 7.00 12 6 0 0.80 9.20 12 6 0 0.60 8.40 -13 -6 0 148.49 24.40 -13 -6 0 202.88 40.50 -13 -6 0 186.18 28.10 -13 -6 0 245.68 51.29 -13 -6 0 150.88 21.80 13 6 0 168.08 25.40 13 6 0 173.98 43.60 13 6 0 175.08 23.90 13 6 0 155.58 26.10 13 6 0 170.38 27.30 13 6 0 116.39 24.20 13 6 0 167.98 40.50 -14 -6 0 337.97 39.50 -14 -6 0 216.68 44.20 -14 -6 0 227.08 32.70 -14 -6 0 196.18 29.30 -14 -6 0 239.98 28.80 -14 -6 0 228.58 51.69 14 6 0 230.58 31.50 14 6 0 187.48 26.60 14 6 0 246.08 50.79 14 6 0 153.18 28.80 14 6 0 230.38 33.00 14 6 0 332.87 63.29 14 6 0 303.57 27.20 -15 -6 0 172.58 27.30 -15 -6 0 124.59 34.50 -15 -6 0 252.57 35.10 -15 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116.89 21.50 -5 -14 0 91.99 26.70 -5 -14 0 133.79 35.20 -5 -14 0 56.79 21.90 5 14 0 112.99 22.90 5 14 0 123.99 23.60 -6 -14 0 23.90 10.90 -6 -14 0 7.80 6.50 -6 -14 0 5.40 8.40 -6 -14 0 14.00 9.60 -6 -14 0 6.60 10.10 -6 -14 0 14.30 13.40 6 14 0 7.30 10.30 6 14 0 36.00 15.60 -7 -14 0 15.10 9.20 -7 -14 0 32.90 13.60 -7 -14 0 49.70 21.50 -7 -14 0 26.10 12.20 -7 -14 0 37.50 14.60 -7 -14 0 32.60 16.40 7 14 0 34.50 14.80 7 14 0 8.70 8.30 -8 -14 0 8.40 11.20 -8 -14 0 19.80 17.20 -8 -14 0 13.40 8.60 -8 -14 0 12.60 10.90 8 14 0 13.30 12.40 8 14 0 13.30 12.00 -9 -14 0 13.10 14.40 -9 -14 0 30.00 13.60 9 14 0 -7.60 6.70 -10 -14 0 114.89 37.20 -10 -14 0 32.10 13.70 -10 -14 0 46.80 16.90 10 14 0 18.00 15.50 -11 -14 0 5.00 11.70 11 14 0 19.50 13.30 -12 -14 0 9.20 12.60 12 14 0 16.70 12.70 12 -15 0 13.30 13.10 -12 15 0 -0.30 10.40 11 -15 0 21.90 13.90 -11 15 0 24.60 19.60 10 -15 0 120.19 25.80 -10 15 0 82.89 25.90 9 -15 0 45.00 17.00 -9 15 0 38.50 33.00 8 -15 0 -3.70 5.80 -8 15 0 0.90 10.00 7 -15 0 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196.18 38.60 2 -16 0 106.89 18.50 -2 16 0 114.19 25.80 1 -16 0 136.59 29.30 1 -16 0 145.79 20.30 1 -16 0 210.78 36.10 1 -16 0 138.69 27.20 1 -16 0 96.89 22.30 0 -16 0 264.57 36.50 0 -16 0 294.47 23.00 0 -16 0 252.17 31.80 0 -16 0 339.47 45.50 0 -16 0 332.17 47.50 -1 -16 0 80.09 20.40 -1 -16 0 136.89 29.40 -1 -16 0 94.39 21.00 -2 -16 0 29.90 13.20 -2 -16 0 20.60 11.80 -2 -16 0 16.20 11.00 -3 -16 0 14.70 11.50 -4 -16 0 56.99 19.60 4 16 0 23.90 12.50 -5 -16 0 35.70 17.60 5 16 0 30.30 13.60 -6 -16 0 15.90 10.90 -6 -16 0 13.60 11.90 6 16 0 25.20 12.90 -7 -16 0 -4.00 8.10 -7 -16 0 18.50 13.00 7 16 0 7.40 10.00 -8 -16 0 12.50 12.20 8 16 0 4.50 10.70 -9 -16 0 24.10 12.80 9 16 0 7.60 9.70 9 -17 0 87.89 22.80 -9 17 0 78.99 26.00 -8 17 0 5.50 13.50 -7 17 0 98.19 32.30 -6 17 0 121.69 32.90 5 -17 0 136.49 29.00 5 -17 0 102.89 22.00 -5 17 0 143.29 33.10 4 -17 0 77.89 20.60 4 -17 0 153.88 33.40 4 -17 0 93.59 19.10 -4 17 0 126.69 31.00 3 -17 0 34.00 16.40 3 -17 0 34.70 12.80 3 -17 0 71.39 20.30 -3 17 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11 -3 3.10 4.90 7 11 -3 -3.50 6.40 7 11 -3 5.90 6.70 7 11 -3 2.70 5.00 -7 -11 3 1.50 7.30 -7 -11 3 13.40 11.10 -7 -11 3 -1.80 3.60 -7 -11 3 -0.20 6.30 -7 -11 3 5.40 7.60 -7 -11 3 -3.80 3.20 6 11 -3 64.59 17.90 6 11 -3 56.19 12.10 6 11 -3 92.09 18.00 6 11 -3 44.90 13.90 -6 -11 3 56.89 14.10 -6 -11 3 110.69 29.70 -6 -11 3 62.69 28.60 -6 -11 3 56.89 20.80 -6 -11 3 62.69 15.10 5 11 -3 37.20 13.10 5 11 -3 36.70 9.90 5 11 -3 26.60 9.80 -5 -11 3 31.10 10.20 -5 -11 3 51.79 17.80 -5 -11 3 37.40 17.10 -5 -11 3 18.00 8.20 -5 -11 3 23.40 9.00 4 11 -3 7.60 8.30 4 11 -3 6.90 5.10 -4 -11 3 9.30 9.50 -4 -11 3 5.00 6.70 -4 -11 3 15.80 12.80 -4 -11 3 7.00 5.80 -4 -11 3 0.50 4.70 -4 -11 3 9.90 9.40 3 11 -3 372.76 22.80 3 11 -3 384.56 30.20 3 11 -3 406.96 26.30 -3 -11 3 390.66 29.30 -3 -11 3 377.86 48.20 -3 -11 3 320.07 25.00 -3 -11 3 418.36 49.40 -3 -11 3 405.76 51.49 -3 -11 3 453.55 55.99 -3 -11 3 360.76 25.20 -3 -11 3 376.66 28.60 2 11 -3 329.97 44.80 2 11 -3 306.77 19.70 -2 -11 3 360.06 25.40 -2 -11 3 375.86 47.70 -2 -11 3 303.17 26.20 -2 -11 3 337.07 43.30 -2 -11 3 368.26 46.90 -2 -11 3 319.37 19.40 -2 -11 3 306.37 23.50 -2 -11 3 352.36 35.00 1 11 -3 452.15 26.00 1 11 -3 507.55 44.30 -1 -11 3 472.75 41.30 -1 -11 3 499.85 30.30 -1 -11 3 485.05 30.20 -1 -11 3 565.14 43.90 -1 -11 3 541.45 42.60 -1 -11 3 533.65 30.90 -1 -11 3 487.35 26.10 -1 -11 3 510.15 33.80 0 11 -3 48.80 15.10 0 11 -3 81.29 14.10 0 -11 3 50.69 12.30 0 -11 3 64.09 11.60 0 -11 3 62.39 13.00 0 -11 3 57.29 18.70 0 -11 3 53.19 13.30 0 -11 3 55.29 13.30 0 -11 3 89.09 22.50 -1 11 -3 306.27 22.20 -1 11 -3 301.97 34.30 1 -11 3 253.87 22.40 1 -11 3 290.97 21.70 1 -11 3 283.07 22.20 1 -11 3 272.97 30.90 1 -11 3 255.07 19.50 -2 11 -3 225.58 25.10 -2 11 -3 185.58 31.50 -2 11 -3 156.98 24.20 2 -11 3 208.98 23.80 2 -11 3 219.08 27.60 2 -11 3 199.28 40.60 2 -11 3 208.18 18.30 2 -11 3 218.38 25.50 -3 11 -3 647.34 49.60 -3 11 -3 725.23 43.90 -3 11 -3 611.14 36.50 3 -11 3 625.54 44.80 3 -11 3 652.13 39.80 3 -11 3 649.93 35.10 3 -11 3 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1.10 12.60 5 -17 4 -5.10 6.20 -6 17 -4 78.49 27.80 -7 17 -4 16.00 17.70 7 -17 4 -4.00 8.20 -8 17 -4 21.20 19.40 8 -17 4 5.30 12.30 8 -17 4 15.00 9.10 -9 17 -4 157.78 36.50 9 -17 4 200.98 30.60 9 -17 4 95.99 24.50 9 16 -4 2.20 10.20 -9 -16 4 3.00 11.20 8 16 -4 87.09 23.80 -8 -16 4 77.59 20.90 7 16 -4 26.10 14.60 -7 -16 4 9.90 12.20 -7 -16 4 16.40 11.50 6 16 -4 5.50 9.60 -6 -16 4 -0.30 9.50 -6 -16 4 2.10 6.90 -5 -16 4 47.50 14.80 -5 -16 4 42.20 21.50 -4 -16 4 92.09 27.90 -4 -16 4 69.39 19.40 -4 -16 4 104.99 21.30 -3 -16 4 30.10 10.50 -3 -16 4 10.00 10.30 -3 -16 4 17.10 12.90 -2 -16 4 6.60 5.10 -2 -16 4 28.10 16.80 -2 -16 4 0.40 9.40 -2 -16 4 4.30 6.20 -1 -16 4 14.50 8.00 -1 -16 4 7.00 9.00 -1 -16 4 20.00 10.20 -1 -16 4 10.90 10.30 0 -16 4 34.00 12.30 0 -16 4 55.29 13.90 0 -16 4 23.40 12.10 0 -16 4 76.19 26.60 -1 16 -4 80.89 17.60 1 -16 4 48.20 13.00 1 -16 4 78.49 18.40 1 -16 4 97.99 31.60 1 -16 4 71.59 20.00 1 -16 4 39.10 28.40 -2 16 -4 112.19 20.40 -2 16 -4 96.79 26.30 2 -16 4 125.79 20.50 2 -16 4 121.79 31.40 2 -16 4 86.09 20.60 -3 16 -4 189.38 35.80 -3 16 -4 121.69 21.50 3 -16 4 112.19 22.50 3 -16 4 125.49 21.80 -4 16 -4 37.20 17.70 -4 16 -4 10.10 7.50 4 -16 4 12.50 12.10 4 -16 4 9.50 9.90 -5 16 -4 2.70 5.90 -5 16 -4 3.90 12.90 5 -16 4 1.10 6.10 5 -16 4 -3.20 6.00 -6 16 -4 -3.80 5.10 -6 16 -4 29.40 17.30 6 -16 4 1.00 6.30 6 -16 4 0.30 12.50 -7 16 -4 -0.80 14.50 7 -16 4 -4.50 8.60 7 -16 4 -4.20 5.80 -8 16 -4 28.40 17.60 8 -16 4 35.40 13.20 -9 16 -4 83.99 29.10 9 -16 4 96.79 21.70 -10 16 -4 81.19 28.60 10 -16 4 47.00 16.50 10 15 -4 21.10 14.90 -10 -15 4 43.90 19.40 9 15 -4 17.80 12.90 -9 -15 4 32.40 19.40 -9 -15 4 20.90 14.10 8 15 -4 10.90 10.90 -8 -15 4 34.50 21.10 -8 -15 4 22.80 11.20 -8 -15 4 17.30 13.90 7 15 -4 75.29 21.10 -7 -15 4 60.79 17.10 -7 -15 4 72.99 23.30 -7 -15 4 66.99 28.50 6 15 -4 115.09 23.90 -6 -15 4 177.88 27.60 -6 -15 4 155.28 34.40 -6 -15 4 116.69 31.00 5 15 -4 38.60 14.90 5 15 -4 50.59 16.60 -5 -15 4 52.99 15.40 -5 -15 4 31.00 16.60 -5 -15 4 59.59 22.60 -5 -15 4 73.79 24.80 -5 -15 4 66.69 18.70 4 15 -4 10.80 9.70 -4 -15 4 7.70 6.70 -4 -15 4 -0.10 7.10 -4 -15 4 4.70 5.80 -4 -15 4 3.70 6.60 -4 -15 4 6.00 9.10 3 15 -4 32.40 15.20 -3 -15 4 39.90 13.40 -3 -15 4 34.00 11.40 -3 -15 4 26.20 16.00 -3 -15 4 41.40 19.60 -3 -15 4 33.60 14.30 -3 -15 4 84.49 28.00 -3 -15 4 13.30 9.50 -2 -15 4 61.39 23.50 -2 -15 4 82.89 24.30 -2 -15 4 68.49 23.30 -2 -15 4 71.19 25.40 -2 -15 4 46.30 14.70 -2 -15 4 76.29 18.80 -2 -15 4 69.69 16.30 1 15 -4 5.60 4.20 -1 -15 4 8.10 7.80 -1 -15 4 1.60 6.20 -1 -15 4 -1.50 5.20 -1 -15 4 -1.10 3.80 -1 -15 4 -4.20 5.90 -1 -15 4 -0.50 6.30 -1 -15 4 1.00 4.20 0 -15 4 -3.00 5.60 0 -15 4 3.10 4.00 0 -15 4 0.20 5.80 0 -15 4 6.60 8.90 0 -15 4 1.00 8.30 0 -15 4 8.70 10.90 0 -15 4 -0.90 5.70 0 -15 4 13.20 9.90 -1 15 -4 31.50 16.20 1 -15 4 43.70 19.20 1 -15 4 20.50 17.80 1 -15 4 23.10 8.60 1 -15 4 16.60 12.90 1 -15 4 24.60 11.40 1 -15 4 31.80 25.70 1 -15 4 12.70 10.50 -2 15 -4 14.40 11.50 -2 15 -4 -1.80 3.60 2 -15 4 -0.20 7.20 2 -15 4 4.10 8.00 2 -15 4 2.80 6.00 2 -15 4 1.80 5.80 2 -15 4 8.10 6.10 2 -15 4 5.40 8.40 -3 15 -4 46.60 14.00 -3 15 -4 40.50 18.10 3 -15 4 39.70 17.20 3 -15 4 26.40 13.40 3 -15 4 32.30 14.70 3 -15 4 16.90 11.30 3 -15 4 24.30 9.80 -4 15 -4 48.60 14.60 -4 15 -4 118.39 27.90 4 -15 4 50.39 15.40 4 -15 4 94.19 25.40 4 -15 4 74.29 19.20 4 -15 4 79.99 17.50 4 -15 4 68.99 15.40 -5 15 -4 11.50 7.90 -5 15 -4 39.20 19.90 5 -15 4 12.10 9.80 5 -15 4 24.50 10.40 5 -15 4 40.70 17.60 5 -15 4 40.40 14.70 -6 15 -4 22.10 14.50 6 -15 4 11.30 11.50 6 -15 4 16.80 10.50 6 -15 4 18.00 10.30 6 -15 4 -0.70 5.90 -7 15 -4 -3.50 8.10 -7 15 -4 4.60 6.10 7 -15 4 0.00 5.60 7 -15 4 15.40 9.50 7 -15 4 3.90 8.00 -8 15 -4 -0.10 8.70 8 -15 4 10.50 10.40 8 -15 4 6.50 10.70 -9 15 -4 154.08 37.30 9 -15 4 113.49 23.60 -10 15 -4 134.99 33.60 10 -15 4 97.09 23.40 -11 15 -4 201.68 41.10 11 -15 4 250.47 40.70 -12 15 -4 156.38 37.70 12 -15 4 98.29 25.00 12 14 -4 25.50 15.50 -12 -14 4 36.70 18.10 11 14 -4 29.60 14.50 -11 -14 4 79.29 20.60 10 14 -4 38.10 15.70 -10 -14 4 60.99 18.20 -10 -14 4 60.99 27.00 -10 -14 4 92.29 41.00 9 14 -4 -1.40 5.40 9 14 -4 28.50 15.20 -9 -14 4 19.00 11.20 -9 -14 4 6.80 12.80 8 14 -4 -1.50 4.70 8 14 -4 4.30 8.70 -8 -14 4 16.20 16.00 -8 -14 4 8.50 11.30 -8 -14 4 11.40 9.20 -8 -14 4 0.90 9.70 -8 -14 4 5.40 6.50 7 14 -4 1.50 4.70 7 14 -4 -1.30 7.30 7 14 -4 17.60 12.30 7 14 -4 6.20 8.00 -7 -14 4 14.70 9.70 -7 -14 4 -1.00 6.60 -7 -14 4 5.30 7.40 -7 -14 4 -1.20 5.00 -7 -14 4 -1.90 7.70 -7 -14 4 1.30 8.10 6 14 -4 -5.10 6.40 6 14 -4 12.40 11.30 -6 -14 4 16.00 14.60 -6 -14 4 1.10 5.80 -6 -14 4 5.30 5.40 -6 -14 4 3.90 6.50 -6 -14 4 28.30 18.40 5 14 -4 10.10 9.80 5 14 -4 6.80 13.00 -5 -14 4 -2.20 4.40 -5 -14 4 12.30 10.40 -5 -14 4 5.70 6.30 -5 -14 4 4.30 5.50 4 14 -4 7.80 8.40 -4 -14 4 6.10 6.20 -4 -14 4 9.30 12.00 -4 -14 4 -2.10 4.10 -4 -14 4 12.40 12.60 -4 -14 4 17.60 12.30 -4 -14 4 0.10 5.70 -4 -14 4 18.30 12.80 3 14 -4 48.70 16.10 -3 -14 4 35.80 17.20 -3 -14 4 67.39 16.70 -3 -14 4 55.49 20.80 -3 -14 4 50.99 14.20 -3 -14 4 42.80 13.20 -3 -14 4 29.00 16.50 -3 -14 4 21.70 11.30 2 14 -4 40.90 9.90 -2 -14 4 33.90 15.30 -2 -14 4 47.40 19.70 -2 -14 4 69.49 16.00 -2 -14 4 69.39 11.90 -2 -14 4 50.19 20.20 -2 -14 4 79.79 17.50 -2 -14 4 64.99 15.10 -2 -14 4 57.09 15.30 1 14 -4 6.00 4.60 -1 -14 4 -0.60 6.80 -1 -14 4 12.70 11.00 -1 -14 4 3.80 7.80 -1 -14 4 4.80 5.30 -1 -14 4 0.00 5.40 -1 -14 4 9.10 10.20 -1 -14 4 3.60 7.50 -1 -14 4 2.90 4.60 0 14 -4 129.39 19.10 0 -14 4 165.48 33.70 0 -14 4 117.19 19.70 0 -14 4 153.98 35.10 0 -14 4 143.29 22.40 0 -14 4 182.08 35.20 0 -14 4 120.19 23.10 0 -14 4 143.69 22.70 0 -14 4 129.49 22.50 -1 14 -4 401.66 34.10 -1 14 -4 443.16 39.50 1 -14 4 423.06 28.50 1 -14 4 395.56 32.60 1 -14 4 434.36 53.69 1 -14 4 441.36 30.60 1 -14 4 519.85 47.00 1 -14 4 433.36 55.39 1 -14 4 482.35 33.00 1 -14 4 438.16 36.30 -2 14 -4 784.22 52.19 2 -14 4 733.23 47.80 2 -14 4 663.73 52.39 2 -14 4 798.72 43.80 2 -14 4 721.03 44.40 2 -14 4 740.03 40.30 2 -14 4 745.03 41.10 -3 14 -4 634.24 47.20 -3 14 -4 621.24 40.70 3 -14 4 635.24 50.89 3 -14 4 648.24 42.50 3 -14 4 698.63 39.60 3 -14 4 664.43 40.40 3 -14 4 693.93 45.90 -4 14 -4 301.37 27.70 -4 14 -4 317.47 42.20 4 -14 4 240.88 38.40 4 -14 4 299.37 24.60 4 -14 4 199.68 30.00 4 -14 4 267.87 31.40 4 -14 4 228.48 32.30 4 -14 4 283.97 25.30 -5 14 -4 5.20 9.50 -5 14 -4 22.90 9.10 5 -14 4 1.50 4.30 5 -14 4 1.90 5.20 5 -14 4 5.00 5.20 5 -14 4 7.50 7.90 5 -14 4 20.10 12.50 -6 14 -4 2.30 12.70 -6 14 -4 32.20 12.30 6 -14 4 39.60 16.70 6 -14 4 19.60 10.00 6 -14 4 38.30 21.80 6 -14 4 18.00 9.60 6 -14 4 19.70 10.40 6 -14 4 15.60 10.40 6 -14 4 11.70 8.10 -7 14 -4 143.99 25.20 -7 14 -4 176.38 33.70 7 -14 4 234.48 34.40 7 -14 4 132.99 23.70 7 -14 4 219.08 29.40 7 -14 4 155.18 27.70 7 -14 4 115.49 27.80 7 -14 4 182.68 24.60 7 -14 4 111.79 24.60 -8 14 -4 19.20 10.30 -8 14 -4 25.30 16.30 8 -14 4 20.80 11.70 8 -14 4 13.40 11.10 8 -14 4 22.00 9.60 8 -14 4 30.80 13.10 8 -14 4 22.00 10.90 8 -14 4 22.30 12.40 8 -14 4 19.30 12.10 -9 14 -4 23.50 10.70 -9 14 -4 13.30 14.30 9 -14 4 8.60 8.50 9 -14 4 26.40 13.00 9 -14 4 19.50 12.40 -10 14 -4 33.80 20.10 10 -14 4 20.80 12.60 10 -14 4 0.20 6.60 -11 14 -4 16.30 16.80 11 -14 4 16.10 15.00 11 -14 4 5.90 8.80 -12 14 -4 -1.90 14.40 -13 14 -4 9.50 16.10 13 -14 4 2.30 9.90 13 13 -4 -10.00 9.20 -13 -13 4 -5.10 10.40 12 13 -4 13.30 12.70 -12 -13 4 -5.10 8.30 11 13 -4 11.10 11.90 -11 -13 4 -1.20 9.90 -11 -13 4 -2.60 8.70 -11 -13 4 18.10 10.80 10 13 -4 11.30 14.20 10 13 -4 0.90 5.90 -10 -13 4 10.50 18.30 -10 -13 4 32.40 18.70 -10 -13 4 50.29 19.10 -10 -13 4 24.50 14.90 -10 -13 4 42.90 15.40 9 13 -4 6.60 7.00 9 13 -4 6.80 9.70 9 13 -4 39.70 15.40 -9 -13 4 25.50 12.00 -9 -13 4 39.50 14.40 -9 -13 4 28.20 13.60 -9 -13 4 49.30 24.30 -9 -13 4 56.19 17.20 -9 -13 4 27.00 18.00 8 13 -4 49.00 16.20 8 13 -4 43.80 15.00 8 13 -4 77.29 15.40 -8 -13 4 77.69 17.90 -8 -13 4 53.09 18.20 -8 -13 4 58.79 31.10 -8 -13 4 74.69 28.90 -8 -13 4 50.39 23.20 -8 -13 4 52.09 15.40 7 13 -4 6.50 11.90 7 13 -4 -4.60 7.80 7 13 -4 0.30 7.10 7 13 -4 7.90 6.00 -7 -13 4 -0.40 8.70 -7 -13 4 0.10 5.00 -7 -13 4 12.90 13.80 -7 -13 4 4.60 6.10 -7 -13 4 -2.30 4.90 -7 -13 4 12.30 11.20 -7 -13 4 1.90 6.90 6 13 -4 33.80 14.60 6 13 -4 -8.10 7.80 6 13 -4 19.70 9.50 -6 -13 4 21.70 17.10 -6 -13 4 25.30 17.10 -6 -13 4 5.80 6.90 -6 -13 4 12.20 8.90 -6 -13 4 7.70 6.10 -6 -13 4 1.60 5.90 5 13 -4 4.60 9.10 5 13 -4 6.30 6.30 -5 -13 4 9.70 7.00 -5 -13 4 0.50 4.40 -5 -13 4 -1.70 5.00 -5 -13 4 12.40 7.70 -5 -13 4 -1.20 9.10 -5 -13 4 8.80 8.90 -5 -13 4 -0.50 5.90 4 13 -4 120.69 23.10 -4 -13 4 71.29 17.30 -4 -13 4 89.39 18.50 -4 -13 4 94.09 18.90 -4 -13 4 62.39 20.60 -4 -13 4 65.29 21.50 -4 -13 4 83.79 25.80 -4 -13 4 81.59 16.20 3 13 -4 48.00 14.70 3 13 -4 36.30 12.30 -3 -13 4 37.50 15.20 -3 -13 4 25.80 12.50 -3 -13 4 38.30 19.70 -3 -13 4 31.50 16.10 -3 -13 4 36.80 19.40 -3 -13 4 20.30 9.80 -3 -13 4 42.30 13.20 -3 -13 4 52.69 14.30 2 13 -4 -2.90 6.40 2 13 -4 6.10 5.60 -2 -13 4 19.60 10.10 -2 -13 4 3.30 7.40 -2 -13 4 2.20 5.70 -2 -13 4 22.90 13.90 -2 -13 4 11.60 5.90 -2 -13 4 6.30 6.70 -2 -13 4 5.00 8.40 -2 -13 4 1.40 9.90 -2 -13 4 6.40 9.00 1 13 -4 16.10 7.10 -1 -13 4 12.40 7.80 -1 -13 4 35.00 17.70 -1 -13 4 12.80 6.50 -1 -13 4 25.80 9.60 -1 -13 4 4.20 8.60 -1 -13 4 20.30 11.10 -1 -13 4 21.60 9.10 -1 -13 4 5.90 8.70 -1 -13 4 35.70 18.00 0 13 -4 165.78 29.40 0 13 -4 180.28 22.90 0 -13 4 152.68 23.20 0 -13 4 171.08 21.00 0 -13 4 169.58 33.20 0 -13 4 130.59 22.00 0 -13 4 142.49 24.90 0 -13 4 175.18 34.20 0 -13 4 139.59 20.90 0 -13 4 176.88 33.90 0 -13 4 123.09 27.30 -1 13 -4 389.46 35.40 -1 13 -4 407.96 28.40 1 -13 4 434.16 51.89 1 -13 4 404.86 29.70 1 -13 4 385.86 30.80 1 -13 4 434.06 29.50 1 -13 4 397.26 40.10 1 -13 4 392.86 32.80 1 -13 4 424.26 41.40 1 -13 4 388.96 27.40 -2 13 -4 83.69 22.20 -2 13 -4 128.39 21.50 2 -13 4 71.99 14.60 2 -13 4 83.19 19.40 2 -13 4 69.49 14.00 2 -13 4 99.19 25.30 2 -13 4 69.59 15.90 2 -13 4 71.39 16.70 2 -13 4 92.19 24.90 -3 13 -4 98.59 22.30 -3 13 -4 125.09 25.00 3 -13 4 109.69 22.10 3 -13 4 101.69 21.00 3 -13 4 120.39 20.20 3 -13 4 105.59 25.20 3 -13 4 93.59 16.60 3 -13 4 114.79 26.30 3 -13 4 118.89 19.00 -4 13 -4 224.38 42.00 -4 13 -4 268.27 38.00 4 -13 4 193.28 41.30 4 -13 4 189.18 28.10 4 -13 4 188.38 25.30 4 -13 4 214.18 27.10 4 -13 4 217.48 25.50 4 -13 4 196.48 33.60 -5 13 -4 360.96 43.60 -5 13 -4 287.57 33.50 5 -13 4 316.67 42.60 5 -13 4 331.37 27.70 5 -13 4 345.37 39.50 5 -13 4 339.67 25.80 5 -13 4 398.26 30.50 5 -13 4 317.77 27.90 -6 13 -4 131.29 26.70 -6 13 -4 85.89 19.10 6 -13 4 142.79 25.00 6 -13 4 170.18 27.10 6 -13 4 107.29 27.20 6 -13 4 89.59 18.60 6 -13 4 96.59 17.00 6 -13 4 148.49 24.20 6 -13 4 139.79 22.30 -7 13 -4 22.20 10.10 -7 13 -4 34.30 15.80 7 -13 4 23.00 10.40 7 -13 4 34.40 11.30 7 -13 4 51.39 15.30 7 -13 4 43.90 15.30 7 -13 4 23.10 11.70 7 -13 4 35.00 14.90 7 -13 4 24.50 10.90 -8 13 -4 12.60 13.90 -8 13 -4 14.50 9.70 -8 13 -4 35.30 15.20 8 -13 4 11.70 8.30 8 -13 4 6.80 10.30 8 -13 4 34.60 13.20 8 -13 4 17.70 11.00 8 -13 4 21.80 10.10 -9 13 -4 37.00 19.10 -9 13 -4 22.40 13.80 -9 13 -4 29.00 12.30 9 -13 4 18.80 9.60 9 -13 4 6.80 9.20 9 -13 4 19.10 8.50 9 -13 4 16.80 8.00 9 -13 4 29.10 13.80 9 -13 4 45.60 16.20 9 -13 4 25.60 11.70 -10 13 -4 42.10 18.10 -10 13 -4 38.60 14.50 10 -13 4 41.70 12.50 10 -13 4 36.60 14.90 10 -13 4 55.79 17.30 10 -13 4 50.89 21.30 10 -13 4 53.59 16.90 10 -13 4 61.29 17.10 -11 13 -4 39.40 19.50 11 -13 4 57.29 18.90 11 -13 4 12.70 12.00 -12 13 -4 15.70 14.80 12 -13 4 15.00 10.90 12 -13 4 6.90 10.80 -13 13 -4 26.70 21.30 13 -13 4 36.40 18.30 -14 13 -4 23.70 19.40 14 -13 4 13.90 13.70 14 12 -4 -1.90 10.70 -14 -12 4 3.50 10.80 13 12 -4 1.70 10.40 -13 -12 4 -4.00 13.20 -13 -12 4 6.30 10.30 12 12 -4 42.50 18.30 -12 -12 4 45.40 15.60 -12 -12 4 26.00 18.30 -12 -12 4 52.69 17.90 11 12 -4 127.39 26.80 -11 -12 4 182.18 42.40 -11 -12 4 150.98 26.30 -11 -12 4 231.88 37.70 -11 -12 4 157.98 28.60 10 12 -4 94.09 23.10 10 12 -4 68.99 18.60 10 12 -4 90.99 18.40 -10 -12 4 119.49 23.10 -10 -12 4 52.19 21.50 -10 -12 4 64.19 17.10 -10 -12 4 39.30 13.90 9 12 -4 105.59 23.80 9 12 -4 77.59 16.90 -9 -12 4 78.99 26.90 -9 -12 4 104.29 19.50 -9 -12 4 91.79 32.60 -9 -12 4 120.19 29.30 -9 -12 4 99.39 21.70 8 12 -4 71.09 16.70 8 12 -4 50.89 17.90 8 12 -4 57.29 16.70 8 12 -4 65.79 17.30 -8 -12 4 55.79 14.70 -8 -12 4 59.99 22.80 -8 -12 4 83.09 29.50 -8 -12 4 55.99 23.70 -8 -12 4 45.30 16.00 -8 -12 4 54.19 15.90 7 12 -4 6.40 9.30 7 12 -4 4.30 5.30 7 12 -4 1.80 4.60 7 12 -4 3.60 4.70 -7 -12 4 1.30 8.70 -7 -12 4 8.00 9.50 -7 -12 4 8.60 5.90 -7 -12 4 1.80 5.80 -7 -12 4 6.80 10.20 -7 -12 4 11.10 7.40 -7 -12 4 2.60 7.70 6 12 -4 10.70 8.60 6 12 -4 12.80 9.00 6 12 -4 -4.00 9.30 6 12 -4 11.30 6.90 -6 -12 4 16.80 8.30 -6 -12 4 34.40 16.20 -6 -12 4 21.20 9.90 -6 -12 4 31.70 17.00 -6 -12 4 23.10 15.90 -6 -12 4 24.50 11.00 -6 -12 4 0.40 4.60 -6 -12 4 30.20 17.50 5 12 -4 9.40 7.20 5 12 -4 8.20 6.80 5 12 -4 -0.50 7.60 5 12 -4 10.80 7.70 -5 -12 4 17.70 9.50 -5 -12 4 15.50 8.40 -5 -12 4 22.50 14.80 -5 -12 4 13.20 11.50 -5 -12 4 2.00 6.40 -5 -12 4 10.70 8.80 -5 -12 4 9.10 8.00 -5 -12 4 -0.40 8.30 4 12 -4 75.99 16.30 4 12 -4 59.49 12.40 4 12 -4 57.19 16.50 -4 -12 4 61.79 22.30 -4 -12 4 73.49 22.10 -4 -12 4 40.10 11.70 -4 -12 4 85.79 23.10 -4 -12 4 55.49 14.40 -4 -12 4 69.39 21.40 -4 -12 4 80.39 18.20 -4 -12 4 59.89 14.70 3 12 -4 118.39 22.90 -3 -12 4 121.89 34.40 -3 -12 4 123.29 24.20 -3 -12 4 115.79 26.20 -3 -12 4 170.58 36.20 -3 -12 4 118.49 19.80 -3 -12 4 126.19 20.00 -3 -12 4 88.39 17.40 -3 -12 4 88.19 24.00 2 12 -4 456.85 25.30 -2 -12 4 363.66 28.20 -2 -12 4 381.66 28.00 -2 -12 4 399.66 50.39 -2 -12 4 416.76 23.90 -2 -12 4 407.26 31.70 -2 -12 4 449.86 42.00 1 12 -4 185.38 21.50 -1 -12 4 200.18 37.40 -1 -12 4 142.89 21.10 -1 -12 4 125.59 15.90 -1 -12 4 91.69 24.10 -1 -12 4 148.19 23.60 -1 -12 4 165.78 22.30 0 12 -4 171.98 28.40 0 12 -4 130.99 18.70 0 -12 4 146.19 24.50 0 -12 4 180.28 20.30 0 -12 4 144.09 20.50 0 -12 4 166.58 23.90 0 -12 4 89.29 22.50 -1 12 -4 477.85 30.00 -1 12 -4 518.45 38.10 1 -12 4 432.66 30.10 1 -12 4 492.35 29.10 1 -12 4 483.75 32.30 1 -12 4 454.25 33.60 -2 12 -4 1691.33 67.49 -2 12 -4 1683.03 75.69 -2 12 -4 1613.24 87.49 2 -12 4 1688.03 69.49 2 -12 4 1675.73 72.79 2 -12 4 1631.64 67.19 2 -12 4 1631.94 64.39 -3 12 -4 1294.37 65.29 -3 12 -4 1338.77 59.19 -3 12 -4 1314.07 77.39 3 -12 4 1354.46 58.99 3 -12 4 1280.57 62.19 3 -12 4 1262.27 55.39 3 -12 4 1164.68 74.19 -4 12 -4 758.82 57.89 -4 12 -4 783.32 44.00 -4 12 -4 817.82 49.70 4 -12 4 765.52 40.00 4 -12 4 814.82 37.70 4 -12 4 790.62 46.40 4 -12 4 726.93 51.89 4 -12 4 738.83 40.90 4 -12 4 790.72 43.20 -5 12 -4 92.39 23.70 -5 12 -4 93.49 21.10 -5 12 -4 109.09 23.60 5 -12 4 107.49 17.30 5 -12 4 99.99 23.90 5 -12 4 136.79 20.70 5 -12 4 114.89 19.90 5 -12 4 107.19 19.40 5 -12 4 106.69 25.90 5 -12 4 140.29 24.10 -6 12 -4 10.40 7.70 -6 12 -4 8.20 12.20 -6 12 -4 11.50 10.10 6 -12 4 22.10 11.50 6 -12 4 9.20 6.70 6 -12 4 16.00 9.10 6 -12 4 30.60 10.90 6 -12 4 17.80 9.30 6 -12 4 6.80 7.90 6 -12 4 20.80 12.10 6 -12 4 3.70 6.60 -7 12 -4 358.26 44.20 -7 12 -4 269.67 32.40 -7 12 -4 307.57 41.30 7 -12 4 225.28 29.40 7 -12 4 338.17 27.40 7 -12 4 285.47 32.90 7 -12 4 286.77 35.80 7 -12 4 264.27 22.90 7 -12 4 212.18 33.70 7 -12 4 281.47 34.50 -8 12 -4 122.59 22.30 -8 12 -4 164.08 31.20 -8 12 -4 149.09 29.90 8 -12 4 165.78 25.60 8 -12 4 184.98 28.00 8 -12 4 123.29 25.80 8 -12 4 108.39 17.80 8 -12 4 147.49 24.90 8 -12 4 101.99 18.90 8 -12 4 128.29 24.30 -9 12 -4 76.49 21.40 -9 12 -4 84.79 23.30 -9 12 -4 112.59 21.70 9 -12 4 150.18 26.80 9 -12 4 123.49 27.60 9 -12 4 94.49 17.60 9 -12 4 71.59 20.30 9 -12 4 114.19 22.90 9 -12 4 192.68 29.10 9 -12 4 99.19 22.10 -10 12 -4 43.80 19.70 -10 12 -4 4.50 7.10 -10 12 -4 40.90 18.10 10 -12 4 30.90 17.40 10 -12 4 12.80 8.90 10 -12 4 22.50 13.20 10 -12 4 10.90 8.40 10 -12 4 31.60 14.40 10 -12 4 23.20 13.50 -11 12 -4 -12.30 8.20 -11 12 -4 0.40 4.60 11 -12 4 0.30 5.70 11 -12 4 27.20 10.90 11 -12 4 -0.60 7.80 11 -12 4 1.40 6.30 11 -12 4 10.90 8.30 11 -12 4 3.40 7.30 -12 12 -4 1.80 13.50 12 -12 4 -6.70 6.20 12 -12 4 4.60 7.30 -13 12 -4 118.29 30.40 13 -12 4 91.99 26.10 13 -12 4 70.69 20.60 -14 12 -4 93.79 29.00 14 -12 4 115.29 29.10 -15 12 -4 65.29 25.30 15 -12 4 64.79 22.90 14 11 -4 -2.10 11.60 -14 -11 4 6.50 11.10 -14 -11 4 1.50 12.90 13 11 -4 -2.30 9.10 -13 -11 4 3.70 8.20 -13 -11 4 2.20 9.50 -13 -11 4 -7.50 6.80 -13 -11 4 2.30 12.40 12 11 -4 -1.00 5.80 12 11 -4 6.20 12.00 -12 -11 4 14.80 10.30 -12 -11 4 -1.10 9.70 -12 -11 4 3.00 12.20 -12 -11 4 22.40 13.50 11 11 -4 102.99 22.60 11 11 -4 112.09 24.30 11 11 -4 109.69 19.70 -11 -11 4 109.39 31.90 -11 -11 4 91.99 21.10 -11 -11 4 107.99 21.40 -11 -11 4 105.09 24.90 -11 -11 4 150.98 27.70 10 11 -4 106.19 29.90 10 11 -4 41.50 14.50 10 11 -4 52.19 18.00 -10 -11 4 53.49 21.20 -10 -11 4 72.19 19.70 -10 -11 4 71.79 29.60 -10 -11 4 74.79 16.70 -10 -11 4 38.40 15.30 -10 -11 4 49.99 15.20 9 11 -4 88.39 18.00 9 11 -4 51.79 15.00 9 11 -4 49.10 16.50 -9 -11 4 97.09 27.70 -9 -11 4 53.29 16.60 -9 -11 4 49.90 15.60 -9 -11 4 39.20 19.80 -9 -11 4 61.69 17.00 -9 -11 4 75.49 17.00 8 11 -4 5.80 9.80 8 11 -4 4.90 7.00 8 11 -4 7.30 8.00 8 11 -4 15.20 7.40 -8 -11 4 16.40 10.10 -8 -11 4 20.20 11.30 -8 -11 4 6.70 7.10 -8 -11 4 32.30 18.10 -8 -11 4 3.40 7.80 -8 -11 4 0.30 8.10 7 11 -4 2.40 8.40 7 11 -4 4.10 5.50 7 11 -4 11.40 8.40 7 11 -4 1.40 4.00 -7 -11 4 4.80 8.80 -7 -11 4 18.10 12.40 -7 -11 4 -0.50 5.00 -7 -11 4 6.60 6.40 -7 -11 4 0.30 7.30 -7 -11 4 7.30 10.20 6 11 -4 117.99 20.40 6 11 -4 72.59 17.90 6 11 -4 100.99 19.70 6 11 -4 98.59 16.30 -6 -11 4 116.49 19.80 -6 -11 4 91.99 23.40 -6 -11 4 68.69 14.90 -6 -11 4 68.79 21.70 -6 -11 4 91.29 16.70 5 11 -4 57.89 22.10 5 11 -4 48.10 11.20 5 11 -4 20.10 11.30 5 11 -4 39.30 12.00 -5 -11 4 22.60 9.60 -5 -11 4 36.90 10.70 -5 -11 4 73.89 22.40 -5 -11 4 41.60 11.70 -5 -11 4 38.30 17.50 4 11 -4 8.00 7.00 4 11 -4 4.70 5.10 4 11 -4 8.60 5.10 -4 -11 4 5.60 6.00 -4 -11 4 8.70 10.10 -4 -11 4 15.20 11.90 -4 -11 4 1.60 5.90 -4 -11 4 -1.90 5.50 -4 -11 4 6.50 7.10 -4 -11 4 2.00 4.00 3 11 -4 6.10 5.20 3 11 -4 11.20 6.00 3 11 -4 7.80 7.20 3 11 -4 8.10 4.90 3 11 -4 0.80 5.20 -3 -11 4 1.30 6.70 -3 -11 4 22.40 12.30 -3 -11 4 6.70 4.60 -3 -11 4 3.70 7.60 -3 -11 4 13.70 7.60 -3 -11 4 11.70 10.50 -3 -11 4 19.30 8.40 -3 -11 4 8.20 6.60 -3 -11 4 7.00 7.90 2 11 -4 21.00 7.50 -2 -11 4 27.80 14.90 -2 -11 4 23.50 11.00 -2 -11 4 18.70 12.60 -2 -11 4 42.40 11.60 -2 -11 4 29.00 7.90 -2 -11 4 39.00 17.60 -2 -11 4 19.70 13.00 -2 -11 4 28.30 9.30 -2 -11 4 28.70 12.50 1 11 -4 18.30 7.10 -1 -11 4 6.50 5.50 -1 -11 4 25.50 9.40 -1 -11 4 15.90 10.70 -1 -11 4 19.60 11.40 -1 -11 4 9.70 9.00 -1 -11 4 26.70 8.70 -1 -11 4 15.20 8.20 -1 -11 4 15.20 6.40 0 11 -4 18.20 10.20 0 11 -4 11.30 7.00 0 -11 4 10.70 8.10 0 -11 4 30.80 10.90 0 -11 4 2.10 5.20 0 -11 4 16.30 7.80 0 -11 4 17.60 8.70 0 -11 4 15.40 6.30 -1 11 -4 122.89 22.40 -1 11 -4 151.28 31.00 -1 11 -4 101.29 16.90 1 -11 4 96.29 17.40 1 -11 4 118.59 17.20 1 -11 4 115.89 17.60 1 -11 4 74.99 20.20 1 -11 4 123.39 21.40 1 -11 4 124.69 18.50 -2 11 -4 50.39 18.80 -2 11 -4 34.00 13.40 -2 11 -4 40.70 11.40 2 -11 4 28.80 16.50 2 -11 4 46.10 13.70 2 -11 4 46.50 13.50 2 -11 4 58.89 16.30 2 -11 4 27.70 9.20 2 -11 4 55.09 11.90 2 -11 4 20.10 12.00 -3 11 -4 42.00 11.80 -3 11 -4 42.00 15.10 -3 11 -4 38.40 14.30 3 -11 4 22.70 8.70 3 -11 4 54.79 16.80 3 -11 4 20.70 8.00 3 -11 4 42.10 15.80 3 -11 4 27.50 10.90 3 -11 4 38.70 13.60 -4 11 -4 483.35 35.50 -4 11 -4 482.75 31.80 -4 11 -4 421.86 41.50 -4 11 -4 507.35 39.00 4 -11 4 469.55 33.50 4 -11 4 459.35 30.70 4 -11 4 436.66 38.50 4 -11 4 411.26 28.50 4 -11 4 474.45 47.80 4 -11 4 445.06 28.60 4 -11 4 456.35 26.60 -5 11 -4 320.57 27.60 -5 11 -4 368.86 31.40 -5 11 -4 349.27 40.80 5 -11 4 308.87 25.70 5 -11 4 312.77 25.40 5 -11 4 366.66 29.70 5 -11 4 374.46 25.20 -6 11 -4 156.88 28.50 -6 11 -4 139.79 31.60 -6 11 -4 150.38 27.50 6 -11 4 115.59 19.50 6 -11 4 132.39 21.00 6 -11 4 178.08 24.20 6 -11 4 157.38 24.80 -7 11 -4 23.70 12.30 -7 11 -4 9.70 10.00 -7 11 -4 10.00 7.90 -7 11 -4 9.20 9.70 7 -11 4 -3.80 4.50 7 -11 4 16.10 10.30 7 -11 4 27.90 11.20 7 -11 4 12.20 7.70 7 -11 4 8.40 6.40 7 -11 4 -2.80 5.40 7 -11 4 5.90 5.70 7 -11 4 7.50 8.10 -8 11 -4 57.49 19.50 -8 11 -4 67.59 19.50 -8 11 -4 46.90 14.30 8 -11 4 62.59 16.10 8 -11 4 54.49 13.60 8 -11 4 83.99 17.80 8 -11 4 77.89 21.00 8 -11 4 54.09 18.80 8 -11 4 32.90 10.20 8 -11 4 62.09 16.90 8 -11 4 41.50 13.40 -9 11 -4 19.60 12.30 -9 11 -4 12.80 11.90 -9 11 -4 5.60 5.10 9 -11 4 14.80 10.70 9 -11 4 19.30 9.60 9 -11 4 18.00 9.70 9 -11 4 22.00 10.40 9 -11 4 7.80 6.90 9 -11 4 11.70 7.00 9 -11 4 16.90 12.00 -10 11 -4 14.40 9.10 -10 11 -4 37.60 20.40 -10 11 -4 11.30 12.40 10 -11 4 -1.80 6.90 10 -11 4 2.30 6.00 10 -11 4 5.50 5.60 10 -11 4 9.80 8.60 10 -11 4 18.40 9.90 10 -11 4 17.90 8.00 10 -11 4 2.00 5.20 -11 11 -4 74.29 16.30 -11 11 -4 55.59 21.60 -11 11 -4 41.40 17.80 -11 11 -4 61.69 14.10 -11 11 -4 45.40 15.60 11 -11 4 57.69 30.90 11 -11 4 66.99 17.40 11 -11 4 38.40 12.90 11 -11 4 96.59 21.00 11 -11 4 63.99 15.80 11 -11 4 59.59 18.30 11 -11 4 35.50 16.30 -12 11 -4 21.70 10.20 -12 11 -4 4.00 5.40 -12 11 -4 63.59 22.60 12 -11 4 55.99 18.70 12 -11 4 29.30 12.30 12 -11 4 54.09 17.10 12 -11 4 23.50 14.10 12 -11 4 34.40 11.20 12 -11 4 77.49 18.90 -13 11 -4 -0.90 11.20 -13 11 -4 -2.10 4.90 13 -11 4 3.40 7.80 13 -11 4 8.10 12.90 -14 11 -4 -1.40 5.90 -14 11 -4 1.70 15.00 14 -11 4 -0.50 10.70 14 -11 4 -3.60 7.50 -15 11 -4 34.50 21.90 15 -11 4 22.20 14.90 15 10 -4 4.80 14.50 -15 -10 4 10.70 12.70 14 10 -4 -5.40 8.60 -14 -10 4 2.50 9.30 -14 -10 4 5.50 9.10 -14 -10 4 6.40 20.40 -14 -10 4 8.60 12.10 13 10 -4 15.40 15.60 13 10 -4 3.00 7.00 -13 -10 4 6.30 11.50 -13 -10 4 1.70 10.50 -13 -10 4 0.80 11.90 -13 -10 4 5.20 8.40 12 10 -4 25.70 14.00 12 10 -4 14.10 9.00 12 10 -4 18.20 10.20 12 10 -4 0.10 5.30 -12 -10 4 16.20 12.10 -12 -10 4 17.50 12.20 -12 -10 4 38.30 13.50 -12 -10 4 36.20 21.70 -12 -10 4 23.10 12.20 11 10 -4 29.30 14.40 11 10 -4 -0.90 4.10 11 10 -4 12.80 9.70 11 10 -4 22.00 10.60 -11 -10 4 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530.85 29.10 -9 -3 4 549.25 27.10 -9 -3 4 458.05 43.10 -9 -3 4 541.65 31.40 -9 -3 4 608.04 31.40 -9 -3 4 546.95 33.50 -9 -3 4 550.84 30.10 -9 -3 4 582.04 44.70 8 3 -4 201.18 32.00 8 3 -4 199.58 16.00 8 3 -4 208.98 19.00 8 3 -4 206.98 13.40 8 3 -4 198.58 16.30 8 3 -4 230.48 39.70 8 3 -4 212.08 17.90 8 3 -4 202.98 17.20 8 3 -4 184.48 17.00 -8 -3 4 272.17 34.50 -8 -3 4 219.88 17.20 -8 -3 4 193.58 31.60 -8 -3 4 188.28 17.30 -8 -3 4 183.58 14.20 -8 -3 4 208.58 16.70 -8 -3 4 204.28 18.90 7 3 -4 262.27 19.00 7 3 -4 286.47 15.90 7 3 -4 325.57 39.50 7 3 -4 264.77 20.40 7 3 -4 266.07 17.30 7 3 -4 233.38 18.40 7 3 -4 364.86 49.30 7 3 -4 296.97 20.20 -7 -3 4 265.27 18.00 -7 -3 4 309.67 17.10 -7 -3 4 354.66 44.40 -7 -3 4 282.07 35.60 -7 -3 4 292.07 18.60 -7 -3 4 273.37 21.60 -7 -3 4 275.17 19.60 6 3 -4 202.78 15.80 6 3 -4 186.48 15.40 6 3 -4 208.28 31.30 6 3 -4 190.98 13.10 6 3 -4 160.88 25.90 6 3 -4 191.98 12.10 6 3 -4 220.18 16.10 6 3 -4 204.98 16.80 -6 -3 4 220.58 15.30 -6 -3 4 188.18 27.70 -6 -3 4 169.38 26.80 -6 -3 4 208.98 16.20 -6 -3 4 176.88 15.70 -6 -3 4 188.28 14.00 -6 -3 4 196.08 12.90 5 3 -4 322.07 19.10 5 3 -4 326.77 19.10 5 3 -4 380.66 20.40 5 3 -4 301.27 26.60 5 3 -4 308.17 15.30 5 3 -4 359.06 21.00 5 3 -4 340.17 30.10 -5 -3 4 320.17 28.50 -5 -3 4 339.77 20.00 -5 -3 4 322.17 20.00 -5 -3 4 322.97 39.70 -5 -3 4 321.87 18.40 -5 -3 4 306.67 16.30 -5 -3 4 307.07 17.30 4 3 -4 -1.00 2.80 4 3 -4 8.90 4.50 4 3 -4 -3.60 3.60 4 3 -4 7.40 4.40 4 3 -4 9.10 3.40 4 3 -4 11.00 7.20 4 3 -4 3.10 6.10 -4 -3 4 9.20 6.50 -4 -3 4 8.30 4.60 -4 -3 4 6.80 3.90 -4 -3 4 4.70 3.30 -4 -3 4 10.60 4.60 -4 -3 4 8.50 7.60 -4 -3 4 8.70 4.70 -4 -3 4 5.90 2.90 3 3 -4 30.00 5.10 3 3 -4 35.20 10.40 3 3 -4 40.00 7.30 3 3 -4 30.20 7.10 -3 -3 4 34.70 6.40 -3 -3 4 43.60 13.20 -3 -3 4 43.00 7.50 -3 -3 4 32.60 10.00 -3 -3 4 29.40 6.60 -3 -3 4 39.50 7.60 -3 -3 4 33.50 5.40 2 3 -4 121.69 11.80 2 3 -4 98.79 10.80 2 3 -4 91.79 10.50 2 3 -4 93.69 7.10 2 3 -4 89.19 10.50 -2 -3 4 59.49 8.60 -2 -3 4 94.89 15.50 -2 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13 2 -4 5.00 7.50 13 2 -4 7.80 7.10 13 2 -4 -1.30 7.30 13 2 -4 -0.30 4.80 13 2 -4 7.80 6.10 -13 -2 4 16.20 9.90 -13 -2 4 4.30 9.00 -13 -2 4 7.10 6.50 -13 -2 4 -11.70 4.60 -13 -2 4 3.10 6.30 -13 -2 4 5.50 12.50 12 2 -4 71.29 25.80 12 2 -4 116.49 19.60 12 2 -4 171.88 37.60 12 2 -4 142.99 21.30 12 2 -4 115.79 16.10 12 2 -4 104.99 13.80 12 2 -4 79.19 17.60 12 2 -4 81.69 18.40 -12 -2 4 94.19 17.00 -12 -2 4 102.79 17.90 -12 -2 4 107.79 18.00 -12 -2 4 105.69 20.00 -12 -2 4 103.29 26.80 -12 -2 4 70.59 24.40 11 2 -4 51.09 12.80 11 2 -4 43.90 8.90 11 2 -4 37.00 12.00 11 2 -4 40.50 9.50 11 2 -4 46.30 12.40 11 2 -4 25.40 14.40 11 2 -4 45.60 19.80 11 2 -4 45.50 12.20 11 2 -4 44.00 13.50 -11 -2 4 51.19 13.40 -11 -2 4 67.29 21.00 -11 -2 4 33.00 10.30 -11 -2 4 34.60 15.30 -11 -2 4 40.50 11.80 -11 -2 4 36.50 10.40 10 2 -4 68.59 11.90 10 2 -4 82.39 25.70 10 2 -4 63.29 14.80 10 2 -4 74.09 11.30 10 2 -4 73.69 15.00 10 2 -4 56.09 12.20 10 2 -4 60.49 13.20 10 2 -4 67.39 22.40 10 2 -4 69.69 14.10 -10 -2 4 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-2 4 148.79 16.20 6 2 -4 202.88 15.40 6 2 -4 222.38 13.60 6 2 -4 230.28 15.90 6 2 -4 209.08 16.20 6 2 -4 227.98 32.90 6 2 -4 171.58 14.40 6 2 -4 230.88 29.10 -6 -2 4 185.68 26.90 -6 -2 4 207.28 16.20 -6 -2 4 233.08 30.10 -6 -2 4 187.98 14.10 -6 -2 4 219.28 15.90 -6 -2 4 225.28 14.80 -6 -2 4 208.58 13.10 5 2 -4 39.50 15.70 5 2 -4 29.80 7.50 5 2 -4 26.90 6.60 5 2 -4 46.00 9.50 5 2 -4 17.40 8.60 5 2 -4 31.90 6.20 5 2 -4 36.30 8.40 -5 -2 4 31.10 8.20 -5 -2 4 37.70 6.70 -5 -2 4 34.80 12.20 -5 -2 4 26.80 6.20 -5 -2 4 38.10 8.40 -5 -2 4 33.00 7.20 -5 -2 4 50.79 13.50 4 2 -4 7.10 4.20 4 2 -4 7.60 6.40 4 2 -4 24.00 9.20 4 2 -4 8.30 4.20 4 2 -4 12.50 4.50 4 2 -4 4.50 3.90 4 2 -4 12.20 3.80 -4 -2 4 11.20 6.90 -4 -2 4 6.00 4.10 -4 -2 4 11.50 4.90 -4 -2 4 17.60 5.10 -4 -2 4 9.00 4.00 -4 -2 4 4.80 5.10 -4 -2 4 16.70 4.80 3 2 -4 821.12 39.10 3 2 -4 843.22 28.70 3 2 -4 811.52 27.40 3 2 -4 776.22 40.70 3 2 -4 783.82 30.70 3 2 -4 727.23 26.70 3 2 -4 821.52 30.30 -3 -2 4 760.02 29.80 -3 -2 4 785.72 27.10 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115.49 29.80 2 -15 9 121.49 22.50 2 -15 9 114.69 24.50 2 -15 9 68.49 19.30 2 -15 9 105.99 21.70 2 -15 9 115.69 21.10 2 -15 9 43.10 19.10 -3 15 -9 114.49 21.90 -3 15 -9 202.28 36.30 3 -15 9 119.79 24.90 3 -15 9 114.19 25.50 3 -15 9 183.98 26.60 3 -15 9 129.69 32.30 3 -15 9 145.49 26.90 3 -15 9 178.48 27.40 -4 15 -9 337.77 49.10 -4 15 -9 293.07 36.70 4 -15 9 224.58 32.70 4 -15 9 127.89 26.50 4 -15 9 180.78 42.60 4 -15 9 187.38 30.40 4 -15 9 263.07 46.50 4 -15 9 252.67 32.50 -5 15 -9 273.57 42.00 -5 15 -9 234.78 33.30 5 -15 9 222.78 32.80 5 -15 9 250.47 33.40 5 -15 9 302.37 60.69 5 -15 9 249.18 33.20 5 -15 9 236.48 35.80 -6 15 -9 189.18 36.70 -6 15 -9 176.88 29.90 6 -15 9 153.08 26.50 6 -15 9 172.38 30.90 6 -15 9 150.38 27.90 -7 15 -9 151.38 32.70 7 -15 9 231.88 32.10 7 -15 9 135.79 27.20 -8 15 -9 -11.20 13.90 8 -15 9 13.80 11.60 8 -15 9 4.40 8.40 8 -15 9 -2.30 6.40 -9 15 -9 15.50 15.20 9 -15 9 34.70 16.40 9 -15 9 12.40 12.70 9 -15 9 20.10 13.60 -10 15 -9 73.19 26.90 10 -15 9 67.89 19.90 10 -15 9 47.00 18.30 -11 15 -9 -8.30 9.70 11 -15 9 7.10 12.60 11 -15 9 7.80 8.90 11 14 -9 25.20 15.90 -11 -14 9 48.80 17.30 10 14 -9 3.80 9.20 -10 -14 9 12.90 13.00 -10 -14 9 17.90 14.00 9 14 -9 7.10 11.40 -9 -14 9 16.30 12.50 -9 -14 9 12.60 17.90 -9 -14 9 -3.20 9.20 8 14 -9 9.60 9.90 8 14 -9 0.20 5.80 -8 -14 9 1.50 10.40 -8 -14 9 12.30 9.80 -8 -14 9 24.60 15.10 -8 -14 9 14.00 10.40 -8 -14 9 9.40 13.90 -8 -14 9 21.30 12.10 7 14 -9 9.80 9.80 7 14 -9 -0.80 4.90 -7 -14 9 11.20 7.20 -7 -14 9 27.80 19.50 -7 -14 9 9.70 8.80 -7 -14 9 2.10 9.00 -7 -14 9 1.20 9.40 6 14 -9 1.60 4.70 6 14 -9 -1.20 4.30 6 14 -9 6.10 8.00 6 14 -9 -9.00 6.60 -6 -14 9 5.40 9.60 -6 -14 9 -6.00 6.50 -6 -14 9 11.20 10.50 -6 -14 9 13.20 13.70 -6 -14 9 2.70 8.20 5 14 -9 -2.90 3.90 5 14 -9 5.10 5.20 5 14 -9 11.60 10.90 5 14 -9 -8.10 6.60 -5 -14 9 7.40 7.70 -5 -14 9 25.30 13.50 -5 -14 9 -4.90 13.10 -5 -14 9 0.80 5.30 -5 -14 9 -3.60 8.10 -5 -14 9 17.00 13.10 4 14 -9 -2.40 4.40 4 14 -9 1.20 4.60 4 14 -9 5.10 6.30 -4 -14 9 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14.90 9.50 -7 14 -9 -1.00 8.50 -7 14 -9 -2.00 4.30 7 -14 9 7.70 7.10 7 -14 9 6.60 8.00 7 -14 9 6.50 7.10 7 -14 9 23.30 14.00 7 -14 9 2.70 5.50 7 -14 9 -2.90 7.00 7 -14 9 3.80 6.70 7 -14 9 8.50 12.00 -8 14 -9 77.59 24.20 8 -14 9 46.50 15.50 8 -14 9 13.00 12.30 8 -14 9 62.19 17.60 8 -14 9 35.00 12.80 8 -14 9 16.30 10.10 -9 14 -9 16.20 14.90 9 -14 9 12.30 9.60 9 -14 9 3.30 19.70 9 -14 9 7.50 10.10 -10 14 -9 51.49 20.70 10 -14 9 23.10 14.70 10 -14 9 13.00 11.80 10 -14 9 3.30 9.20 -11 14 -9 41.50 21.30 11 -14 9 38.90 15.50 11 -14 9 58.49 18.80 -12 14 -9 8.80 13.80 12 -14 9 -1.20 8.70 12 -14 9 7.70 11.20 12 13 -9 -4.10 8.70 -12 -13 9 1.00 10.10 11 13 -9 8.00 12.40 -11 -13 9 25.60 13.30 -11 -13 9 20.90 18.90 -11 -13 9 29.40 15.20 10 13 -9 65.59 20.80 -10 -13 9 91.69 33.70 -10 -13 9 101.99 24.30 -10 -13 9 110.19 28.30 -10 -13 9 101.49 40.10 -10 -13 9 87.29 25.90 9 13 -9 55.19 17.70 -9 -13 9 53.69 25.30 -9 -13 9 57.99 20.10 -9 -13 9 57.39 18.00 -9 -13 9 32.00 24.30 -9 -13 9 54.99 18.30 8 13 -9 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162.18 37.90 -1 -5 21 207.58 33.30 -1 -5 21 205.98 27.00 -1 -5 21 215.88 33.00 -1 -5 21 177.28 26.60 -1 -5 21 214.88 32.00 0 5 -21 291.37 22.50 0 5 -21 287.37 52.69 0 5 -21 352.36 30.90 0 5 -21 331.07 30.20 0 5 -21 257.37 45.60 0 -5 21 314.27 27.60 0 -5 21 322.87 29.90 0 -5 21 383.16 56.39 0 -5 21 342.77 37.30 0 -5 21 341.17 53.69 0 -5 21 317.07 29.50 0 -5 21 320.37 24.60 -1 5 -21 224.78 31.70 -1 5 -21 236.48 32.40 -1 5 -21 190.38 41.10 -1 5 -21 177.08 44.00 -1 5 -21 243.58 26.30 1 -5 21 222.78 27.20 1 -5 21 291.57 33.30 1 -5 21 187.38 39.80 1 -5 21 146.09 25.70 1 -5 21 249.38 31.30 1 -5 21 260.77 35.10 1 -5 21 247.18 44.70 -2 5 -21 308.57 36.30 -2 5 -21 245.38 47.10 -2 5 -21 255.07 32.70 -2 5 -21 327.37 59.39 2 -5 21 243.88 36.50 2 -5 21 256.27 32.00 2 -5 21 243.38 28.10 2 -5 21 268.17 32.80 2 -5 21 208.48 42.50 2 -5 21 196.28 37.80 2 -5 21 246.38 43.90 -3 5 -21 82.59 18.60 -3 5 -21 108.29 22.40 -3 5 -21 60.39 23.60 -3 5 -21 73.09 27.20 3 -5 21 106.49 21.00 3 -5 21 98.09 19.60 3 -5 21 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22 345.47 45.60 4 -13 22 316.47 42.90 4 -13 22 290.37 56.79 5 -13 22 147.79 30.70 5 -13 22 110.89 27.40 5 -13 22 69.39 24.30 5 -13 22 103.19 24.40 5 -13 22 85.29 25.90 6 -13 22 20.90 15.80 6 -13 22 33.50 15.10 6 -13 22 19.80 13.20 7 -13 22 25.80 13.30 7 -13 22 66.49 21.30 9 12 -22 54.39 15.80 9 12 -22 76.79 21.50 -9 -12 22 112.79 47.90 -9 -12 22 112.59 48.20 -9 -12 22 45.70 24.60 -9 -12 22 92.29 23.00 -9 -12 22 86.19 25.60 8 12 -22 -2.80 11.20 8 12 -22 30.70 14.00 8 12 -22 20.50 12.30 -8 -12 22 15.10 23.10 -8 -12 22 13.90 12.70 -8 -12 22 0.90 33.70 -8 -12 22 14.70 17.00 -8 -12 22 26.70 20.40 -8 -12 22 11.70 9.20 7 12 -22 4.70 7.60 7 12 -22 -9.60 8.50 -7 -12 22 1.30 11.50 -7 -12 22 14.20 15.40 -7 -12 22 14.30 11.70 -7 -12 22 13.20 9.30 -7 -12 22 3.90 10.50 -7 -12 22 25.20 19.40 6 12 -22 -2.50 7.50 6 12 -22 4.90 8.20 6 12 -22 1.80 9.20 -6 -12 22 3.80 12.40 -6 -12 22 18.80 13.40 -6 -12 22 -1.80 11.70 -6 -12 22 17.10 20.00 -6 -12 22 7.90 7.70 -6 -12 22 1.40 7.40 5 12 -22 1.20 7.70 5 12 -22 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16.90 10.00 0 12 -22 19.00 9.60 0 12 -22 2.40 7.00 0 12 -22 -2.40 4.80 0 -12 22 2.10 9.30 0 -12 22 13.70 15.50 0 -12 22 5.60 8.40 0 -12 22 2.70 6.70 0 -12 22 8.30 9.30 -1 12 -22 104.59 24.90 -1 12 -22 75.49 19.50 1 -12 22 89.09 23.50 1 -12 22 110.99 35.30 1 -12 22 91.09 24.30 1 -12 22 48.30 18.30 -2 12 -22 -1.50 4.80 2 -12 22 2.40 7.30 2 -12 22 9.90 10.20 2 -12 22 8.10 10.30 2 -12 22 9.60 13.00 -3 12 -22 -0.60 5.60 -3 12 -22 12.80 9.10 -3 12 -22 36.20 23.90 3 -12 22 14.60 12.90 3 -12 22 18.10 17.20 3 -12 22 40.30 16.00 3 -12 22 19.90 11.70 -4 12 -22 88.19 26.00 4 -12 22 127.39 26.90 4 -12 22 90.89 33.60 4 -12 22 90.99 26.90 4 -12 22 66.49 21.30 4 -12 22 77.19 22.50 5 -12 22 200.78 33.80 5 -12 22 141.19 30.30 5 -12 22 230.68 37.90 6 -12 22 71.09 30.70 6 -12 22 138.59 37.60 6 -12 22 76.29 24.00 6 -12 22 134.39 30.40 6 -12 22 86.79 22.20 7 -12 22 145.79 30.60 7 -12 22 71.29 25.60 7 -12 22 64.19 30.30 7 -12 22 144.99 32.10 7 -12 22 82.89 21.80 8 -12 22 19.70 15.30 8 -12 22 42.60 14.30 8 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21.50 13.00 -5 -11 22 23.60 10.90 -5 -11 22 1.90 9.60 -5 -11 22 12.50 13.00 -5 -11 22 29.30 15.00 4 11 -22 12.60 9.80 4 11 -22 7.80 10.70 4 11 -22 18.40 11.50 4 11 -22 9.60 9.30 4 11 -22 28.70 11.20 -4 -11 22 29.60 17.60 -4 -11 22 35.80 22.30 -4 -11 22 30.80 14.30 -4 -11 22 28.90 12.30 -4 -11 22 39.00 30.40 -4 -11 22 15.20 21.30 -4 -11 22 11.10 8.50 -4 -11 22 19.10 17.20 -4 -11 22 48.10 18.80 3 11 -22 14.20 9.40 3 11 -22 10.50 9.20 3 11 -22 26.80 11.50 3 11 -22 16.70 12.40 -3 -11 22 23.00 13.80 -3 -11 22 13.10 18.60 -3 -11 22 7.00 16.30 -3 -11 22 2.00 7.40 -3 -11 22 15.10 17.10 -3 -11 22 -2.50 8.30 -3 -11 22 19.10 17.30 -3 -11 22 22.30 13.40 -3 -11 22 8.60 9.30 2 11 -22 106.99 27.30 2 11 -22 89.99 23.30 2 11 -22 68.89 19.30 2 11 -22 80.39 21.10 -2 -11 22 74.59 19.80 -2 -11 22 107.79 37.30 -2 -11 22 78.09 30.90 -2 -11 22 29.60 24.80 -2 -11 22 67.09 18.50 -2 -11 22 67.69 18.00 -2 -11 22 102.89 25.90 -2 -11 22 96.79 27.80 1 11 -22 166.58 34.10 1 11 -22 131.39 26.60 -1 -11 22 244.58 55.69 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99.39 25.10 -5 11 -22 60.59 26.40 5 -11 22 192.08 33.00 5 -11 22 90.29 22.00 5 -11 22 137.49 29.70 5 -11 22 64.79 25.30 5 -11 22 93.79 24.70 -6 11 -22 30.40 20.80 -6 11 -22 -1.80 5.30 -6 11 -22 -0.40 5.90 6 -11 22 16.50 12.70 6 -11 22 12.00 10.00 6 -11 22 7.70 7.90 6 -11 22 0.70 11.00 6 -11 22 10.30 9.80 -7 11 -22 -3.40 5.80 7 -11 22 6.40 8.70 7 -11 22 38.90 25.20 7 -11 22 5.50 7.70 7 -11 22 8.70 9.90 7 -11 22 20.80 14.00 8 -11 22 45.10 18.30 8 -11 22 95.19 26.00 8 -11 22 94.79 35.20 9 -11 22 94.89 29.10 9 -11 22 50.49 27.80 9 -11 22 57.79 17.10 9 -11 22 11.40 12.10 9 -11 22 67.09 22.00 10 -11 22 38.50 14.40 11 10 -22 122.79 28.00 11 10 -22 152.88 30.20 -11 -10 22 230.98 36.00 10 10 -22 224.58 35.80 10 10 -22 207.88 36.60 10 10 -22 215.98 33.90 -10 -10 22 235.58 57.39 -10 -10 22 187.58 32.30 -10 -10 22 271.27 38.00 9 10 -22 174.58 27.80 9 10 -22 234.18 36.80 9 10 -22 205.38 34.70 -9 -10 22 196.88 77.19 -9 -10 22 285.87 40.60 -9 -10 22 158.28 33.20 -9 -10 22 110.29 37.60 -9 -10 22 111.29 31.20 -9 -10 22 136.59 37.50 8 10 -22 34.20 11.70 8 10 -22 25.00 12.80 8 10 -22 63.39 27.30 8 10 -22 49.70 16.30 -8 -10 22 40.50 28.60 -8 -10 22 40.90 16.70 -8 -10 22 49.60 25.50 -8 -10 22 56.19 20.40 -8 -10 22 22.60 24.90 7 10 -22 8.20 9.60 7 10 -22 -3.40 8.90 7 10 -22 10.10 7.60 7 10 -22 4.30 7.90 7 10 -22 26.20 15.80 -7 -10 22 18.80 10.30 -7 -10 22 -1.10 15.40 -7 -10 22 -0.80 8.00 -7 -10 22 -0.40 5.40 -7 -10 22 4.50 10.40 -7 -10 22 -0.90 13.50 6 10 -22 76.19 24.20 6 10 -22 81.89 21.80 6 10 -22 42.90 17.20 6 10 -22 126.09 23.20 6 10 -22 106.79 24.50 -6 -10 22 100.39 20.30 -6 -10 22 67.39 19.10 -6 -10 22 84.59 30.30 -6 -10 22 95.79 35.30 -6 -10 22 81.09 36.40 -6 -10 22 51.09 14.50 -6 -10 22 95.59 23.10 -6 -10 22 55.89 33.50 5 10 -22 86.39 20.20 5 10 -22 90.49 25.70 5 10 -22 102.49 20.80 5 10 -22 85.59 21.60 -5 -10 22 83.89 21.10 -5 -10 22 82.09 30.80 -5 -10 22 114.29 37.10 -5 -10 22 69.69 20.60 -5 -10 22 92.29 21.10 -5 -10 22 44.20 17.30 -5 -10 22 69.59 16.50 -5 -10 22 38.80 25.50 4 10 -22 -1.80 6.00 4 10 -22 6.80 5.90 4 10 -22 -1.90 3.60 4 10 -22 19.70 11.20 -4 -10 22 4.90 6.40 -4 -10 22 -7.40 6.50 -4 -10 22 26.00 20.00 -4 -10 22 7.80 8.40 -4 -10 22 -1.80 7.80 -4 -10 22 8.10 6.80 -4 -10 22 13.50 15.20 3 10 -22 2.80 5.80 3 10 -22 -4.80 5.40 3 10 -22 -0.10 4.50 3 10 -22 18.80 9.40 3 10 -22 -1.20 4.40 -3 -10 22 5.10 11.00 -3 -10 22 -1.90 3.50 -3 -10 22 8.40 15.00 -3 -10 22 -4.70 9.40 -3 -10 22 5.50 5.50 -3 -10 22 -4.70 5.70 -3 -10 22 -4.10 3.90 2 10 -22 50.19 16.60 2 10 -22 43.80 14.30 2 10 -22 70.79 21.00 -2 -10 22 92.39 35.70 -2 -10 22 62.19 15.90 -2 -10 22 38.80 14.70 -2 -10 22 81.09 22.50 -2 -10 22 15.90 16.50 -2 -10 22 63.59 18.80 1 10 -22 3.90 5.60 1 10 -22 1.90 5.50 1 10 -22 -2.50 3.90 -1 -10 22 15.40 10.10 -1 -10 22 -4.20 5.50 -1 -10 22 4.70 7.10 -1 -10 22 8.10 7.00 -1 -10 22 5.80 7.70 0 10 -22 -1.10 6.90 0 10 -22 4.10 6.40 0 10 -22 8.30 7.80 0 -10 22 21.70 11.10 0 -10 22 10.20 9.20 0 -10 22 3.40 8.20 0 -10 22 5.80 7.70 -1 10 -22 7.30 10.20 -1 10 -22 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23.90 5 -10 22 145.19 42.90 5 -10 22 198.18 34.10 5 -10 22 99.69 23.00 -6 10 -22 28.60 18.30 6 -10 22 30.90 18.30 6 -10 22 37.50 16.50 6 -10 22 67.89 21.30 6 -10 22 32.00 13.00 6 -10 22 27.00 13.60 -7 10 -22 -0.20 8.40 -7 10 -22 -2.40 5.00 -7 10 -22 0.00 5.80 7 -10 22 2.00 8.10 7 -10 22 8.80 15.80 7 -10 22 18.30 15.60 7 -10 22 2.10 7.00 7 -10 22 -3.80 5.50 -8 10 -22 11.40 25.80 -8 10 -22 6.70 8.20 -8 10 -22 3.30 8.50 8 -10 22 -4.20 5.90 8 -10 22 7.40 8.10 8 -10 22 14.00 14.10 8 -10 22 1.70 6.90 8 -10 22 -3.30 7.50 -9 10 -22 -2.60 6.70 9 -10 22 9.90 18.50 9 -10 22 6.30 7.50 9 -10 22 5.50 9.10 9 -10 22 9.90 10.40 10 -10 22 2.10 11.80 10 -10 22 13.40 13.40 10 -10 22 38.50 21.10 10 -10 22 8.70 10.60 12 9 -22 6.80 10.10 12 9 -22 -5.90 10.00 12 9 -22 -5.10 12.00 12 9 -22 7.00 11.90 -12 -9 22 9.80 11.80 11 9 -22 -3.70 7.70 11 9 -22 1.40 12.20 11 9 -22 12.00 12.00 -11 -9 22 -3.70 14.10 -11 -9 22 1.00 9.20 -11 -9 22 0.80 8.40 10 9 -22 39.00 16.90 10 9 -22 34.90 13.60 10 9 -22 41.40 19.20 10 9 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23 14.70 18.10 -7 -11 23 7.60 10.70 -7 -11 23 7.00 6.80 6 11 -23 13.30 10.50 6 11 -23 11.10 8.60 6 11 -23 -0.70 7.20 6 11 -23 -12.40 8.20 -6 -11 23 14.00 15.80 -6 -11 23 -2.50 9.80 -6 -11 23 3.60 6.90 -6 -11 23 13.40 10.00 -6 -11 23 8.30 11.10 -6 -11 23 20.20 14.90 5 11 -23 46.10 22.30 5 11 -23 44.90 16.70 5 11 -23 32.20 12.70 -5 -11 23 11.10 9.60 -5 -11 23 34.90 13.10 -5 -11 23 8.00 10.40 -5 -11 23 52.49 27.70 -5 -11 23 1.80 12.00 4 11 -23 12.70 9.10 4 11 -23 -1.80 5.70 4 11 -23 22.50 11.90 4 11 -23 32.30 15.60 -4 -11 23 39.70 17.70 -4 -11 23 25.50 10.60 -4 -11 23 12.30 15.40 -4 -11 23 23.90 11.00 -4 -11 23 16.60 12.10 -4 -11 23 -3.10 7.00 -4 -11 23 19.70 13.20 3 11 -23 56.09 18.90 3 11 -23 32.10 14.60 3 11 -23 17.00 9.60 3 11 -23 -0.90 5.50 -3 -11 23 8.70 11.70 -3 -11 23 11.70 10.80 -3 -11 23 26.60 12.30 -3 -11 23 25.60 20.80 -3 -11 23 16.60 8.20 -3 -11 23 9.60 22.30 -3 -11 23 41.30 14.20 -3 -11 23 33.70 16.30 2 11 -23 32.30 13.00 2 11 -23 12.60 9.50 2 11 -23 7.50 8.20 -2 -11 23 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272.17 36.70 -8 -5 23 254.97 50.59 7 5 -23 178.28 27.20 7 5 -23 154.08 28.10 7 5 -23 187.58 28.30 -7 -5 23 162.68 43.20 -7 -5 23 180.68 28.60 -7 -5 23 184.08 27.90 -7 -5 23 174.98 28.10 -7 -5 23 149.49 23.40 -7 -5 23 135.49 38.30 -7 -5 23 216.08 43.30 -7 -5 23 106.59 32.10 -7 -5 23 153.58 38.00 6 5 -23 31.20 12.40 6 5 -23 42.90 15.80 6 5 -23 10.20 10.40 6 5 -23 37.30 12.80 -6 -5 23 48.80 15.60 -6 -5 23 33.70 19.10 -6 -5 23 39.10 11.50 -6 -5 23 27.10 18.00 -6 -5 23 44.70 14.00 -6 -5 23 57.39 15.80 -6 -5 23 44.30 24.10 -6 -5 23 33.20 18.90 -6 -5 23 38.60 13.60 5 5 -23 17.60 8.10 5 5 -23 5.30 7.80 5 5 -23 15.30 9.50 5 5 -23 3.60 9.20 -5 -5 23 7.90 19.80 -5 -5 23 6.50 8.40 -5 -5 23 3.60 5.60 -5 -5 23 24.00 11.90 -5 -5 23 6.00 6.10 -5 -5 23 13.90 12.70 -5 -5 23 6.80 8.60 -5 -5 23 9.40 12.80 -5 -5 23 15.70 15.50 4 5 -23 218.38 29.00 4 5 -23 213.08 30.00 4 5 -23 235.38 33.20 -4 -5 23 242.18 33.30 -4 -5 23 197.48 28.80 -4 -5 23 216.38 49.30 -4 -5 23 232.78 65.69 -4 -5 23 227.38 31.70 -4 -5 23 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112.79 25.80 9 5 -28 239.38 44.60 9 5 -28 186.68 31.10 9 5 -28 183.18 35.70 -9 -5 28 226.68 34.30 -9 -5 28 202.08 32.40 8 5 -28 193.88 39.10 8 5 -28 138.19 29.10 8 5 -28 169.98 31.30 -8 -5 28 137.99 27.20 -8 -5 28 193.28 32.80 7 5 -28 0.80 10.40 7 5 -28 28.80 14.70 -7 -5 28 -0.70 6.60 -7 -5 28 -0.60 5.70 -7 -5 28 8.70 13.50 -7 -5 28 14.30 11.30 6 5 -28 14.30 10.60 6 5 -28 33.00 17.60 6 5 -28 23.80 13.40 6 5 -28 4.20 8.00 -6 -5 28 13.50 8.70 -6 -5 28 10.80 10.30 -6 -5 28 -1.70 8.60 -6 -5 28 36.70 29.30 -6 -5 28 6.00 8.40 -6 -5 28 -1.40 6.10 5 5 -28 126.79 26.10 5 5 -28 108.49 21.70 5 5 -28 182.88 36.20 5 5 -28 169.28 32.20 -5 -5 28 109.09 35.30 -5 -5 28 146.79 26.40 -5 -5 28 74.59 25.00 -5 -5 28 114.69 27.20 -5 -5 28 111.19 23.50 4 5 -28 53.49 18.00 4 5 -28 76.99 24.10 4 5 -28 128.09 25.60 4 5 -28 81.69 19.40 -4 -5 28 64.69 18.90 -4 -5 28 33.40 13.50 -4 -5 28 105.89 35.00 -4 -5 28 70.49 19.20 -4 -5 28 115.79 27.20 3 5 -28 37.10 14.20 3 5 -28 62.39 17.90 3 5 -28 29.10 14.60 3 5 -28 94.99 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13.80 10 4 -28 26.50 15.00 10 4 -28 32.40 14.50 -10 -4 28 16.30 15.30 9 4 -28 22.10 12.00 9 4 -28 32.40 17.00 9 4 -28 21.20 12.40 -9 -4 28 41.30 17.60 -9 -4 28 6.70 9.40 8 4 -28 206.48 39.80 8 4 -28 154.88 29.40 -8 -4 28 226.38 34.40 7 4 -28 146.09 28.40 7 4 -28 151.58 28.00 -7 -4 28 113.29 25.40 -7 -4 28 93.39 21.10 6 4 -28 101.89 23.90 6 4 -28 85.79 21.70 6 4 -28 92.59 25.50 6 4 -28 82.79 22.20 -6 -4 28 92.19 20.50 -6 -4 28 106.09 24.60 -6 -4 28 122.99 39.10 -6 -4 28 64.99 18.50 5 4 -28 11.20 9.00 5 4 -28 41.90 15.30 5 4 -28 8.70 9.90 5 4 -28 39.60 15.40 -5 -4 28 20.40 10.50 -5 -4 28 -1.30 3.80 -5 -4 28 12.10 8.70 -5 -4 28 3.70 7.60 -5 -4 28 32.30 13.90 -5 -4 28 26.70 13.80 -5 -4 28 24.60 17.80 4 4 -28 65.89 20.80 4 4 -28 59.09 18.30 4 4 -28 82.49 20.00 4 4 -28 60.99 17.50 -4 -4 28 48.70 23.30 -4 -4 28 100.49 23.30 -4 -4 28 55.09 19.00 -4 -4 28 52.49 17.90 -4 -4 28 90.39 20.70 3 4 -28 29.50 13.70 3 4 -28 37.30 14.30 3 4 -28 36.20 13.90 3 4 -28 12.10 10.10 -3 -4 28 18.20 14.40 -3 -4 28 19.80 10.70 -3 -4 28 17.50 12.70 -3 -4 28 16.30 10.20 -3 -4 28 -3.70 8.10 -3 -4 28 0.00 4.70 -3 -4 28 24.10 11.30 2 4 -28 11.30 8.90 2 4 -28 8.10 15.20 2 4 -28 -2.20 4.40 2 4 -28 10.00 8.30 -2 -4 28 -0.40 8.30 -2 -4 28 8.30 10.30 -2 -4 28 12.80 9.70 -2 -4 28 0.20 8.30 -2 -4 28 0.50 5.60 -2 -4 28 2.50 5.30 -2 -4 28 18.60 14.40 1 4 -28 102.69 24.70 1 4 -28 111.39 39.70 1 4 -28 125.29 39.10 1 4 -28 82.19 19.90 1 4 -28 73.39 19.40 1 4 -28 81.99 22.30 -1 -4 28 91.99 23.20 -1 -4 28 42.50 22.20 -1 -4 28 101.49 28.10 -1 -4 28 65.19 31.10 -1 -4 28 106.79 21.20 0 4 -28 247.08 35.40 0 4 -28 160.88 28.60 0 4 -28 233.28 53.69 0 4 -28 258.97 56.49 0 4 -28 209.28 34.50 0 4 -28 163.88 25.50 0 -4 28 270.47 48.00 0 -4 28 212.58 32.70 0 -4 28 213.78 29.80 0 -4 28 257.87 40.40 -1 4 -28 146.79 42.40 -1 4 -28 163.68 30.20 -1 4 -28 200.28 31.10 -1 4 -28 195.48 27.30 -1 4 -28 134.99 38.80 -1 4 -28 176.18 30.50 1 -4 28 199.78 32.20 1 -4 28 183.18 28.40 1 -4 28 236.08 39.50 -2 4 -28 32.50 13.20 -2 4 -28 16.30 13.00 -2 4 -28 2.20 5.50 -2 4 -28 51.99 18.10 -2 4 -28 3.30 11.90 2 -4 28 -0.80 4.60 2 -4 28 -4.60 7.70 2 -4 28 -1.10 3.10 2 -4 28 12.60 13.30 2 -4 28 19.20 10.30 -3 4 -28 -1.90 4.50 -3 4 -28 6.50 7.50 -3 4 -28 4.30 6.80 -3 4 -28 14.90 15.80 3 -4 28 -2.30 3.20 3 -4 28 8.10 11.30 3 -4 28 -1.30 4.50 3 -4 28 -0.80 8.90 3 -4 28 1.70 5.30 3 -4 28 4.10 11.70 -4 4 -28 0.50 9.60 -4 4 -28 0.60 7.90 -4 4 -28 6.00 7.40 -4 4 -28 3.00 6.40 4 -4 28 2.20 5.00 4 -4 28 -1.40 3.50 4 -4 28 -5.20 5.80 -5 4 -28 15.90 10.10 -5 4 -28 0.50 8.60 -5 4 -28 7.00 8.90 5 -4 28 27.10 16.10 5 -4 28 7.00 8.90 5 -4 28 -2.00 4.50 5 -4 28 -0.90 5.60 -6 4 -28 45.50 16.60 -6 4 -28 61.69 26.20 -6 4 -28 30.80 14.70 6 -4 28 61.09 24.60 6 -4 28 27.70 17.90 -7 4 -28 53.59 27.80 -7 4 -28 23.10 13.30 7 -4 28 2.00 8.40 7 -4 28 68.79 27.40 7 -4 28 -1.50 4.80 -8 4 -28 3.70 12.30 -8 4 -28 15.80 12.90 -8 4 -28 12.30 10.70 8 -4 28 -2.00 8.10 8 -4 28 19.10 17.20 8 -4 28 -3.40 5.50 -9 4 -28 35.40 18.10 -9 4 -28 15.20 12.40 -9 4 -28 5.20 17.70 9 -4 28 21.90 15.90 10 -4 28 75.39 27.60 12 3 -28 -0.30 8.90 -12 -3 28 7.10 11.00 11 3 -28 -2.10 9.80 -11 -3 28 -1.40 7.50 10 3 -28 -0.10 10.80 10 3 -28 -3.90 6.20 -10 -3 28 1.60 9.80 9 3 -28 73.79 20.20 9 3 -28 72.19 21.30 9 3 -28 69.89 28.50 -9 -3 28 47.10 17.60 -9 -3 28 63.19 19.20 8 3 -28 33.70 16.40 8 3 -28 22.70 12.60 8 3 -28 23.90 13.40 -8 -3 28 29.90 15.50 -8 -3 28 14.20 11.60 7 3 -28 4.60 6.50 7 3 -28 4.70 8.20 7 3 -28 30.00 18.60 7 3 -28 -1.00 9.00 -7 -3 28 -1.20 6.70 -7 -3 28 8.00 10.30 -7 -3 28 16.20 11.30 6 3 -28 -1.00 4.90 6 3 -28 2.40 6.50 6 3 -28 -1.40 5.50 6 3 -28 11.10 10.10 -6 -3 28 3.40 7.20 -6 -3 28 17.00 11.10 -6 -3 28 2.40 9.90 -6 -3 28 -1.30 5.00 -6 -3 28 13.70 14.90 -6 -3 28 2.80 4.70 5 3 -28 87.69 25.70 5 3 -28 69.59 18.40 5 3 -28 41.10 15.30 5 3 -28 70.79 20.10 -5 -3 28 65.89 17.80 -5 -3 28 72.79 26.30 -5 -3 28 50.29 18.10 -5 -3 28 64.09 16.70 -5 -3 28 69.29 18.60 4 3 -28 14.60 10.30 4 3 -28 21.90 11.10 4 3 -28 21.50 10.90 4 3 -28 24.10 12.60 -4 -3 28 -1.80 7.50 -4 -3 28 26.10 11.50 -4 -3 28 5.50 9.50 -4 -3 28 9.50 9.90 -4 -3 28 -0.80 4.50 -4 -3 28 -1.20 3.30 -4 -3 28 15.30 8.70 -4 -3 28 12.60 12.00 3 3 -28 1.20 5.40 3 3 -28 5.80 7.20 3 3 -28 0.60 7.60 3 3 -28 12.20 8.40 -3 -3 28 5.30 5.90 -3 -3 28 -1.20 7.20 -3 -3 28 1.50 7.20 -3 -3 28 6.70 9.70 -3 -3 28 -1.00 5.90 -3 -3 28 2.00 5.70 -3 -3 28 7.60 8.00 -3 -3 28 5.30 6.40 2 3 -28 -3.10 7.70 2 3 -28 0.90 5.10 2 3 -28 15.20 8.10 2 3 -28 -2.50 7.30 -2 -3 28 -0.40 3.10 -2 -3 28 0.10 8.50 -2 -3 28 2.40 8.50 -2 -3 28 -0.50 4.70 -2 -3 28 -3.40 6.80 -2 -3 28 -5.70 4.90 -2 -3 28 -2.30 4.10 1 3 -28 20.20 10.20 1 3 -28 7.30 8.90 1 3 -28 33.10 14.00 1 3 -28 21.10 17.10 1 3 -28 22.70 10.80 1 3 -28 36.90 19.40 -1 -3 28 33.80 12.90 -1 -3 28 1.10 7.00 -1 -3 28 -2.40 7.20 -1 -3 28 57.79 21.90 -1 -3 28 16.30 9.80 0 3 -28 71.19 29.80 0 3 -28 92.09 22.10 0 3 -28 104.89 24.70 0 3 -28 59.49 26.80 0 3 -28 122.39 25.90 0 -3 28 146.79 31.60 0 -3 28 74.19 19.40 0 -3 28 92.29 19.70 -1 3 -28 156.38 28.60 -1 3 -28 194.68 50.09 -1 3 -28 170.18 43.20 -1 3 -28 248.28 36.80 -1 3 -28 237.48 33.40 1 -3 28 226.38 37.30 1 -3 28 212.08 32.00 1 -3 28 208.48 27.60 -2 3 -28 178.88 45.00 -2 3 -28 181.48 49.30 -2 3 -28 160.28 29.60 -2 3 -28 212.48 33.80 -2 3 -28 287.57 38.50 2 -3 28 214.48 37.90 2 -3 28 183.28 31.10 2 -3 28 165.58 35.50 -3 3 -28 37.70 14.10 -3 3 -28 65.69 18.60 -3 3 -28 93.89 31.40 -3 3 -28 67.19 19.50 3 -3 28 42.30 14.70 3 -3 28 60.19 18.00 3 -3 28 91.69 26.90 -4 3 -28 8.80 7.80 -4 3 -28 18.30 10.00 -4 3 -28 21.20 11.60 -4 3 -28 14.20 15.20 4 -3 28 4.50 5.40 4 -3 28 -1.10 9.30 4 -3 28 -0.60 5.00 4 -3 28 14.10 9.30 4 -3 28 32.40 13.90 -5 3 -28 12.80 10.70 -5 3 -28 42.20 14.90 -5 3 -28 20.30 10.80 -5 3 -28 37.70 25.00 5 -3 28 -0.40 6.00 5 -3 28 30.60 13.30 5 -3 28 35.80 17.70 -6 3 -28 7.80 11.20 -6 3 -28 8.80 9.00 -6 3 -28 15.00 11.90 6 -3 28 -1.60 5.90 6 -3 28 1.00 10.60 6 -3 28 -1.40 4.10 -7 3 -28 20.40 13.10 -7 3 -28 9.20 13.60 -7 3 -28 32.10 15.80 7 -3 28 0.50 11.50 7 -3 28 -1.00 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5 -30 95.39 35.50 1 -5 30 140.49 33.40 1 -5 30 131.29 25.00 -2 5 -30 195.18 36.10 -2 5 -30 120.99 22.40 -2 5 -30 115.29 28.70 -2 5 -30 121.79 40.50 2 -5 30 160.28 34.20 -3 5 -30 2.50 6.20 -3 5 -30 -1.70 9.40 -3 5 -30 5.10 8.00 3 -5 30 -2.60 4.40 3 -5 30 -8.60 7.60 3 -5 30 0.00 7.00 -4 5 -30 13.30 12.90 -4 5 -30 18.60 16.10 -4 5 -30 9.20 10.30 4 -5 30 -1.90 4.90 4 -5 30 -4.00 7.20 -5 5 -30 69.99 24.20 -5 5 -30 56.19 31.90 -5 5 -30 34.60 17.00 5 -5 30 0.70 8.50 5 -5 30 14.80 14.60 -6 5 -30 55.49 27.60 -6 5 -30 57.29 21.30 -6 5 -30 66.59 22.10 6 -5 30 109.39 30.00 -7 5 -30 3.60 10.40 7 -5 30 57.19 25.90 10 4 -30 13.20 11.90 -10 -4 30 -0.60 10.70 9 4 -30 57.19 19.30 -9 -4 30 29.90 15.40 -9 -4 30 40.30 20.00 8 4 -30 29.50 15.00 8 4 -30 34.20 16.80 -8 -4 30 56.59 19.70 -8 -4 30 64.99 20.50 7 4 -30 108.49 25.40 7 4 -30 114.09 28.40 -7 -4 30 69.69 20.60 -7 -4 30 99.69 24.50 6 4 -30 5.10 8.00 6 4 -30 19.40 12.70 -6 -4 30 27.40 15.70 -6 -4 30 -0.80 6.90 -6 -4 30 -1.10 4.90 5 4 -30 2.10 8.80 5 4 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2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 96934