############################################################################## # # # This CIF contains the data for a data article accepted for # # publication in IUCrData. It conforms to the requirements of # # Notes for Authors for IUCrData, and has been # # peer reviewed under the auspices of IUCrData. # # # # Full details of the Crystallographic Information File format # # are given in the paper "The Crystallographic Information File (CIF): # # a New Standard Archive File for Crystallography" by S. R. Hall, F. H. # # Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # # # The current version of the core CIF dictionary is obtainable from # # ftp://ftp.iucr.org/pub/cif_core.dic. # # # # Software is freely available for graphical display of the structure(s) # # in this CIF. For information consult the CIF software page # # http://www.iucr.org/resources/cif/software. # # # # This file may be used for bona fide research purposes within the # # scientific community so long as proper attribution is given to the data # # article from which it was obtained. # # # ############################################################################## data_I _database_code_depnum_ccdc_archive 'CCDC 2005097' _audit_creation_method 'SHELXL-2018/3' _chemical_name_systematic ; 2,3-Dimethyl-1H-imidazol-3-ium benzenesulfonate; 1,2-dimethyl-1H-imidazole ; _chemical_name_common ? _chemical_formula_moiety 'C5 H9 N2 +, C6 H5 O3 S -, C5 H8 N2' _chemical_formula_sum 'C16 H22 N4 O3 S' _chemical_formula_iupac 'C5 H9 N2 +, C6 H5 O3 S -, C5 H8 N2' _chemical_formula_weight 350.43 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 10.8820(6) _cell_length_b 8.4029(4) _cell_length_c 18.9678(11) _cell_angle_alpha 90 _cell_angle_beta 95.440(2) _cell_angle_gamma 90 _cell_volume 1726.61(16) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9689 _cell_measurement_theta_min 2.6532 _cell_measurement_theta_max 33.1879 _cell_measurement_temperature 150(2) _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_size_max 0.550 _exptl_crystal_size_mid 0.420 _exptl_crystal_size_min 0.330 _exptl_crystal_density_diffrn 1.348 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 744 _exptl_absorpt_coefficient_mu 0.210 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_absorpt_correction_T_min 0.7163 _exptl_absorpt_correction_T_max 0.7465 _diffrn_ambient_temperature 150(2) _diffrn_source 'fine focus sealed tube X-ray source' _diffrn_source_voltage '50 kV' _diffrn_source_current '30 mA' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Triumph curved graphite crystal' _diffrn_measurement_device_type 'Bruker AXS D8 Quest CMOS diffractometer' _diffrn_measurement_method 'omega and phi scans' _diffrn_detector_area_resol_mean 10.4167 _diffrn_reflns_number 74762 _diffrn_reflns_av_R_equivalents 0.0316 _diffrn_reflns_av_unetI/netI 0.0180 _diffrn_reflns_theta_min 2.254 _diffrn_reflns_theta_max 33.238 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_limit_l_max 28 _refine_special_details ; H atoms attached to carbon atoms were positioned geometrically and constrained to ride on their parent atoms. C---H bond distances were constrained to 0.95 \%A for aromatic and alkene C---H moieties, and to 0.98 \%A for CH~3~ moieties, respectively. The N---H proton hydrogen bonding between atoms N1 and N3 was found to be disordered and was refined as split between two positions. The H atoms were assigned as bonded to a planar (sp^2^ hybridized) N atom, respectively with fixed bond angles and torsion angles, but the N---H bond distances were allowed to refine to account for asymmetry induced by charge and hydrogen bonding (AFIX 44 command). N---H distances refined to 0.83(5) for N1---H1 and to 0.89(2) for N3---H3, occupancies refined to 0.33(2) for H1 and 0.67(2) for H3. Methyl CH~3~ were allowed to rotate but not to tip to best fit the experimental electron density. U~iso~(H) values were set to a multiple of U~eq~(C/N) with 1.5 for CH~3~ and 1.2 for C---H and NH^+^, respectively. ; _reflns_number_total 6612 _reflns_number_gt 5787 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0406 _refine_ls_R_factor_gt 0.0345 _refine_ls_wR_factor_gt 0.0897 _refine_ls_wR_factor_ref 0.0945 _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_restrained_S_all 1.047 _refine_ls_number_reflns 6612 _refine_ls_number_parameters 225 _refine_ls_number_restraints 0 _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0417P)^2^+0.6618P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.403 _refine_diff_density_min -0.441 _refine_ls_extinction_method ; SHELXL-2018/3 (Sheldrick 2015) ; _refine_ls_extinction_coef 0.0085(10) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX3 (Bruker, 2018) ; _computing_cell_refinement ; SAINT (Bruker, 2018) ; _computing_data_reduction ; SAINT (Bruker, 2018) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015), shelXle (H\"ubschle et al., 2011) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; publCIF (Westrip, 2010), enCIFer (Allen et al., 2004) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.07995(8) 0.11974(12) 0.12505(5) 0.02370(17) Uani d 1 . . H H1 0.162507 0.154570 0.136425 0.028 Uiso calc 1 . . C C2 0.01650(8) 0.02111(12) 0.16550(5) 0.02268(16) Uani d 1 . . H H2 0.045537 -0.025178 0.209661 0.027 Uiso calc 1 . . C C3 -0.10216(8) 0.08832(10) 0.06876(4) 0.01832(14) Uani d 1 . . C C4 -0.20228(9) -0.08561(12) 0.15402(5) 0.02410(17) Uani d 1 . . H H4A -0.264761 -0.010298 0.167446 0.036 Uiso calc 1 . . H H4B -0.172925 -0.150361 0.195187 0.036 Uiso calc 1 . . H H4C -0.238614 -0.154975 0.116071 0.036 Uiso calc 1 . . C C5 -0.21283(8) 0.09673(13) 0.01670(5) 0.02515(18) Uani d 1 . . H H5A -0.194381 0.162346 -0.023687 0.038 Uiso calc 1 . . H H5B -0.281506 0.144135 0.039231 0.038 Uiso calc 1 . . H H5C -0.235631 -0.010751 0.000206 0.038 Uiso calc 1 . . C C6 0.23459(9) 0.40162(12) -0.00734(5) 0.02566(18) Uani d 1 . . H H6 0.285770 0.372447 0.034004 0.031 Uiso calc 1 . . C C7 0.26716(8) 0.49589(12) -0.06067(6) 0.02502(18) Uani d 1 . . H H7 0.345007 0.545291 -0.063695 0.030 Uiso calc 1 . . C C8 0.07312(8) 0.42021(10) -0.08640(4) 0.01863(14) Uani d 1 . . C C9 0.15832(10) 0.59191(13) -0.17707(5) 0.02847(19) Uani d 1 . . H H9A 0.142896 0.516294 -0.216246 0.043 Uiso calc 1 . . H H9B 0.236534 0.647282 -0.181302 0.043 Uiso calc 1 . . H H9C 0.090972 0.669653 -0.178780 0.043 Uiso calc 1 . . C C10 -0.05084(9) 0.40053(13) -0.12482(5) 0.02596(18) Uani d 1 . . H H10A -0.090249 0.504931 -0.131824 0.039 Uiso calc 1 . . H H10B -0.101453 0.332570 -0.097120 0.039 Uiso calc 1 . . H H10C -0.042876 0.351054 -0.170954 0.039 Uiso calc 1 . . C C11 0.43346(7) 0.00325(9) 0.14618(4) 0.01514(13) Uani d 1 . . C C12 0.36079(8) -0.06738(10) 0.19405(4) 0.01852(14) Uani d 1 . . H H12 0.326061 -0.004339 0.228696 0.022 Uiso calc 1 . . C C13 0.33919(9) -0.23035(11) 0.19101(5) 0.02475(18) Uani d 1 . . H H13 0.289972 -0.278763 0.223810 0.030 Uiso calc 1 . . C C14 0.38933(10) -0.32262(12) 0.14020(6) 0.0293(2) Uani d 1 . . H H14 0.375570 -0.434269 0.138722 0.035 Uiso calc 1 . . C C15 0.45951(9) -0.25157(13) 0.09161(6) 0.02817(19) Uani d 1 . . H H15 0.492304 -0.314441 0.056220 0.034 Uiso calc 1 . . C C16 0.48217(8) -0.08834(11) 0.09445(5) 0.02151(16) Uani d 1 . . H H16 0.530578 -0.039928 0.061247 0.026 Uiso calc 1 . . N N1 0.00522(7) 0.16129(10) 0.06471(4) 0.02100(14) Uani d 1 . . H H1N 0.0238(11) 0.220(3) 0.0325(19) 0.025 Uiso calc 0.33(2) A 2 N N2 -0.09869(7) 0.00209(9) 0.12923(4) 0.01850(13) Uani d 1 . . N N3 0.11314(7) 0.35581(10) -0.02425(4) 0.02125(14) Uani d 1 . . H H3N 0.0690(11) 0.2936(16) 0.0021(7) 0.026 Uiso calc 0.67(2) A 1 N N4 0.16511(7) 0.50600(9) -0.10967(4) 0.02018(14) Uani d 1 . . O O1 0.35734(8) 0.28443(9) 0.17511(6) 0.0439(2) Uani d 1 . . O O2 0.49875(9) 0.26229(11) 0.08516(4) 0.0383(2) Uani d 1 . . O O3 0.57130(9) 0.21999(10) 0.20780(5) 0.0400(2) Uani d 1 . . S S1 0.46799(2) 0.20953(2) 0.15392(2) 0.01791(6) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0187(4) 0.0277(4) 0.0242(4) -0.0014(3) -0.0009(3) 0.0018(3) C2 0.0207(4) 0.0263(4) 0.0202(4) 0.0008(3) -0.0024(3) 0.0030(3) C3 0.0179(3) 0.0208(4) 0.0163(3) 0.0012(3) 0.0019(3) 0.0019(3) C4 0.0218(4) 0.0268(4) 0.0244(4) -0.0017(3) 0.0057(3) 0.0059(3) C5 0.0206(4) 0.0326(5) 0.0214(4) -0.0007(3) -0.0025(3) 0.0057(3) C6 0.0217(4) 0.0257(4) 0.0285(4) -0.0007(3) -0.0032(3) -0.0017(3) C7 0.0176(4) 0.0236(4) 0.0338(5) -0.0029(3) 0.0020(3) -0.0033(3) C8 0.0182(3) 0.0197(3) 0.0183(3) -0.0019(3) 0.0032(3) -0.0005(3) C9 0.0367(5) 0.0263(4) 0.0240(4) -0.0061(4) 0.0108(4) 0.0020(3) C10 0.0209(4) 0.0326(5) 0.0237(4) -0.0051(3) -0.0017(3) 0.0037(3) C11 0.0138(3) 0.0151(3) 0.0160(3) -0.0013(2) -0.0009(2) 0.0004(2) C12 0.0195(3) 0.0185(3) 0.0174(3) -0.0033(3) 0.0012(3) 0.0012(3) C13 0.0264(4) 0.0195(4) 0.0271(4) -0.0066(3) -0.0035(3) 0.0064(3) C14 0.0310(5) 0.0154(4) 0.0388(5) 0.0007(3) -0.0104(4) -0.0017(3) C15 0.0254(4) 0.0259(4) 0.0320(5) 0.0068(3) -0.0036(3) -0.0108(4) C16 0.0171(3) 0.0271(4) 0.0203(4) 0.0017(3) 0.0017(3) -0.0031(3) N1 0.0185(3) 0.0238(3) 0.0208(3) -0.0010(3) 0.0027(2) 0.0026(3) N2 0.0179(3) 0.0203(3) 0.0174(3) 0.0002(2) 0.0017(2) 0.0026(2) N3 0.0206(3) 0.0230(3) 0.0199(3) -0.0013(3) 0.0008(2) 0.0010(3) N4 0.0199(3) 0.0193(3) 0.0219(3) -0.0027(2) 0.0051(2) -0.0011(3) O1 0.0321(4) 0.0167(3) 0.0868(7) -0.0008(3) 0.0267(5) -0.0041(4) O2 0.0559(5) 0.0311(4) 0.0288(4) -0.0159(4) 0.0089(4) 0.0088(3) O3 0.0445(5) 0.0265(4) 0.0438(5) -0.0125(3) -0.0235(4) 0.0020(3) S1 0.01652(9) 0.01532(9) 0.02171(10) -0.00380(6) 0.00082(7) 0.00194(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 C2 . 1.3612(13) ? C1 N1 . 1.3845(12) ? C1 H1 . 0.9500 ? C2 N2 . 1.3809(11) ? C2 H2 . 0.9500 ? C3 N1 . 1.3283(11) ? C3 N2 . 1.3541(11) ? C3 C5 . 1.4848(12) ? C4 N2 . 1.4613(11) ? C4 H4A . 0.9800 ? C4 H4B . 0.9800 ? C4 H4C . 0.9800 ? C5 H5A . 0.9800 ? C5 H5B . 0.9800 ? C5 H5C . 0.9800 ? C6 C7 . 1.3580(14) ? C6 N3 . 1.3847(12) ? C6 H6 . 0.9500 ? C7 N4 . 1.3815(12) ? C7 H7 . 0.9500 ? C8 N3 . 1.3322(11) ? C8 N4 . 1.3418(11) ? C8 C10 . 1.4805(12) ? C9 N4 . 1.4639(12) ? C9 H9A . 0.9800 ? C9 H9B . 0.9800 ? C9 H9C . 0.9800 ? C10 H10A . 0.9800 ? C10 H10B . 0.9800 ? C10 H10C . 0.9800 ? C11 C16 . 1.3910(12) ? C11 C12 . 1.3921(11) ? C11 S1 . 1.7767(8) ? C12 C13 . 1.3897(12) ? C12 H12 . 0.9500 ? C13 C14 . 1.3883(15) ? C13 H13 . 0.9500 ? C14 C15 . 1.3866(16) ? C14 H14 . 0.9500 ? C15 C16 . 1.3937(14) ? C15 H15 . 0.9500 ? C16 H16 . 0.9500 ? N1 H1N . 0.83(5) ? N3 H3N . 0.89(2) ? O1 S1 . 1.4489(8) ? O2 S1 . 1.4465(8) ? O3 S1 . 1.4484(8) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 C1 N1 . . 109.27(8) ? C2 C1 H1 . . 125.4 ? N1 C1 H1 . . 125.4 ? C1 C2 N2 . . 105.94(8) ? C1 C2 H2 . . 127.0 ? N2 C2 H2 . . 127.0 ? N1 C3 N2 . . 110.00(7) ? N1 C3 C5 . . 127.01(8) ? N2 C3 C5 . . 122.99(8) ? N2 C4 H4A . . 109.5 ? N2 C4 H4B . . 109.5 ? H4A C4 H4B . . 109.5 ? N2 C4 H4C . . 109.5 ? H4A C4 H4C . . 109.5 ? H4B C4 H4C . . 109.5 ? C3 C5 H5A . . 109.5 ? C3 C5 H5B . . 109.5 ? H5A C5 H5B . . 109.5 ? C3 C5 H5C . . 109.5 ? H5A C5 H5C . . 109.5 ? H5B C5 H5C . . 109.5 ? C7 C6 N3 . . 107.48(8) ? C7 C6 H6 . . 126.3 ? N3 C6 H6 . . 126.3 ? C6 C7 N4 . . 106.69(8) ? C6 C7 H7 . . 126.7 ? N4 C7 H7 . . 126.7 ? N3 C8 N4 . . 108.53(8) ? N3 C8 C10 . . 126.61(8) ? N4 C8 C10 . . 124.85(8) ? N4 C9 H9A . . 109.5 ? N4 C9 H9B . . 109.5 ? H9A C9 H9B . . 109.5 ? N4 C9 H9C . . 109.5 ? H9A C9 H9C . . 109.5 ? H9B C9 H9C . . 109.5 ? C8 C10 H10A . . 109.5 ? C8 C10 H10B . . 109.5 ? H10A C10 H10B . . 109.5 ? C8 C10 H10C . . 109.5 ? H10A C10 H10C . . 109.5 ? H10B C10 H10C . . 109.5 ? C16 C11 C12 . . 120.15(8) ? C16 C11 S1 . . 120.42(6) ? C12 C11 S1 . . 119.39(6) ? C13 C12 C11 . . 119.83(8) ? C13 C12 H12 . . 120.1 ? C11 C12 H12 . . 120.1 ? C14 C13 C12 . . 120.20(9) ? C14 C13 H13 . . 119.9 ? C12 C13 H13 . . 119.9 ? C15 C14 C13 . . 119.89(9) ? C15 C14 H14 . . 120.1 ? C13 C14 H14 . . 120.1 ? C14 C15 C16 . . 120.31(9) ? C14 C15 H15 . . 119.8 ? C16 C15 H15 . . 119.8 ? C11 C16 C15 . . 119.60(9) ? C11 C16 H16 . . 120.2 ? C15 C16 H16 . . 120.2 ? C3 N1 C1 . . 106.66(8) ? C3 N1 H1N . . 126.7 ? C1 N1 H1N . . 126.7 ? C3 N2 C2 . . 108.13(7) ? C3 N2 C4 . . 125.59(7) ? C2 N2 C4 . . 126.12(7) ? C8 N3 C6 . . 108.47(8) ? C8 N3 H3N . . 125.8 ? C6 N3 H3N . . 125.8 ? C8 N4 C7 . . 108.83(8) ? C8 N4 C9 . . 125.08(8) ? C7 N4 C9 . . 126.06(8) ? O2 S1 O3 . . 112.77(6) ? O2 S1 O1 . . 112.73(6) ? O3 S1 O1 . . 112.82(7) ? O2 S1 C11 . . 106.84(4) ? O3 S1 C11 . . 105.15(4) ? O1 S1 C11 . . 105.78(4) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N1 C1 C2 N2 . . . . 0.06(11) ? N3 C6 C7 N4 . . . . -0.20(11) ? C16 C11 C12 C13 . . . . 1.40(12) ? S1 C11 C12 C13 . . . . -176.27(7) ? C11 C12 C13 C14 . . . . -0.33(13) ? C12 C13 C14 C15 . . . . -1.04(14) ? C13 C14 C15 C16 . . . . 1.35(15) ? C12 C11 C16 C15 . . . . -1.09(12) ? S1 C11 C16 C15 . . . . 176.55(7) ? C14 C15 C16 C11 . . . . -0.28(14) ? N2 C3 N1 C1 . . . . 0.00(10) ? C5 C3 N1 C1 . . . . 179.55(9) ? C2 C1 N1 C3 . . . . -0.04(11) ? N1 C3 N2 C2 . . . . 0.03(10) ? C5 C3 N2 C2 . . . . -179.54(9) ? N1 C3 N2 C4 . . . . 175.76(8) ? C5 C3 N2 C4 . . . . -3.81(14) ? C1 C2 N2 C3 . . . . -0.06(10) ? C1 C2 N2 C4 . . . . -175.75(9) ? N4 C8 N3 C6 . . . . -0.12(10) ? C10 C8 N3 C6 . . . . 179.13(9) ? C7 C6 N3 C8 . . . . 0.20(11) ? N3 C8 N4 C7 . . . . 0.00(10) ? C10 C8 N4 C7 . . . . -179.28(9) ? N3 C8 N4 C9 . . . . 178.37(8) ? C10 C8 N4 C9 . . . . -0.91(14) ? C6 C7 N4 C8 . . . . 0.13(10) ? C6 C7 N4 C9 . . . . -178.22(9) ? C16 C11 S1 O2 . . . . 24.77(8) ? C12 C11 S1 O2 . . . . -157.57(7) ? C16 C11 S1 O3 . . . . -95.30(8) ? C12 C11 S1 O3 . . . . 82.36(8) ? C16 C11 S1 O1 . . . . 145.10(8) ? C12 C11 S1 O1 . . . . -37.24(9) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1N N3 . 0.83 1.90 2.6970(11) 162.5 yes N3 H3N N1 . 0.89 1.81 2.6970(11) 169.9 yes C1 H1 O1 . 0.95 2.43 3.3741(13) 169.8 yes C4 H4B O3 2_545 0.98 2.33 3.2956(12) 170.0 yes C6 H6 O2 . 0.95 2.60 3.4288(14) 146.4 yes C7 H7 O2 3_665 0.95 2.41 3.3254(12) 162.0 yes C9 H9A O3 4_565 0.98 2.53 3.4846(14) 164.0 yes C9 H9B O3 3_665 0.98 2.46 3.4381(14) 172.9 yes C13 H13 O1 2_545 0.95 2.67 3.4738(14) 143.2 yes C14 H14 O1 1_545 0.95 2.48 3.3920(13) 162.0 yes _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min 0.893 _shelx_estimated_absorpt_T_max 0.934 _shelx_hkl_file ; -2 0 0 5322.39 173.908 1 3 0 0 -0.2996 0.27120 5 -3 0 0 0.00723 0.28168 5 3 0 0 0.39608 0.77739 1 3 0 0 0.49075 0.10641 4 -3 0 0 0.18833 0.28931 5 -3 0 0 -0.1288 0.23564 3 -3 0 0 0.12588 0.11907 4 3 0 0 -0.1659 0.26804 2 -3 0 0 0.49987 0.79687 1 -4 0 0 138.814 6.15851 1 -4 0 0 136.974 4.70027 2 4 0 0 133.471 4.68038 2 -4 0 0 132.974 4.64586 5 4 0 0 138.501 4.67044 5 4 0 0 137.663 6.08835 1 -4 0 0 137.662 4.66887 5 4 0 0 103.647 4.79780 5 -4 0 0 133.925 4.39789 4 4 0 0 136.354 4.58987 3 4 0 0 135.379 4.39924 4 -5 0 0 -0.2023 0.45057 2 -5 0 0 0.00619 0.37113 3 -5 0 0 0.49786 1.27781 1 -5 0 0 0.18982 0.36907 5 5 0 0 -0.2585 1.21823 1 5 0 0 -0.2709 0.40774 2 5 0 0 0.02359 0.35659 3 5 0 0 0.37380 0.38994 5 5 0 0 0.12228 0.38322 5 -5 0 0 0.17969 0.38026 5 -6 0 0 35.4639 1.75553 5 -6 0 0 38.5187 1.79844 5 6 0 0 34.9627 1.78698 5 6 0 0 35.4241 1.76356 5 6 0 0 30.3676 3.73368 1 -6 0 0 39.0213 1.89761 2 -6 0 0 41.2804 1.70204 3 -6 0 0 37.1336 3.83321 1 6 0 0 36.3238 1.85869 2 6 0 0 36.1519 1.65926 3 6 0 0 35.0597 1.29001 4 7 0 0 1.39676 0.62218 5 -7 0 0 0.19442 0.57050 5 -7 0 0 0.35279 0.61615 5 7 0 0 -0.1439 0.64471 2 7 0 0 0.52638 0.49273 3 7 0 0 0.29746 0.16981 4 7 0 0 0.11648 0.54622 5 7 0 0 -3.1261 2.47233 1 -7 0 0 -0.9808 1.98000 1 -7 0 0 0.19851 0.63184 2 -7 0 0 0.00198 0.48532 3 8 0 0 86.4011 3.60376 5 -8 0 0 84.4428 3.58938 5 -8 0 0 88.2987 3.61387 5 8 0 0 88.2502 3.43087 3 -8 0 0 89.5333 3.44380 3 -8 0 0 86.9174 6.95148 1 -8 0 0 83.5793 3.66969 2 -9 0 0 -0.5612 0.76044 5 -9 0 0 0.77657 0.83841 5 -9 0 0 0.84807 0.77636 3 -9 0 0 0.59690 0.91643 2 -9 0 0 -1.3401 2.99469 1 9 0 0 -0.1380 0.78394 5 10 0 0 10.5577 1.28417 5 10 0 0 12.5247 1.61757 3 -10 0 0 9.65472 1.13758 3 -10 0 0 10.1115 3.77282 1 -10 0 0 14.8000 1.81046 5 -10 0 0 9.99843 1.34974 2 10 0 0 12.8175 1.83998 5 -10 0 0 14.0586 1.90204 5 -10 0 0 1.63084 3.76370 1 -11 0 0 3.37573 4.22660 1 11 0 0 0.35661 1.10626 5 -11 0 0 0.41352 1.04977 5 -11 0 0 -1.6447 4.43525 1 -11 0 0 -0.0069 0.85422 3 -11 0 0 -0.1758 1.22193 5 11 0 0 0.33136 1.10218 5 -11 0 0 0.06993 1.10883 2 11 0 0 -1.2060 0.88588 3 12 0 0 0.46435 1.11253 5 12 0 0 -0.9726 1.02850 3 12 0 0 0.90556 1.02768 5 -12 0 0 -4.9133 8.30685 1 -12 0 0 0.19160 1.18699 2 -12 0 0 -0.4343 1.01178 5 -12 0 0 0.34469 0.86795 3 -13 0 0 0.68073 1.32117 2 13 0 0 1.22308 1.37897 5 13 0 0 -1.7451 1.22085 3 -13 0 0 -1.1330 1.20085 5 13 0 0 0.62990 1.34144 5 -13 0 0 -0.0852 0.94516 3 -14 0 0 5.39863 1.71018 2 -14 0 0 3.52687 1.22313 3 14 0 0 2.76845 1.31465 5 15 0 0 1.74754 1.54552 5 -15 0 0 -0.2656 1.32196 3 -15 0 0 1.57938 1.86294 2 16 0 0 85.3720 5.06106 5 -16 0 0 93.1592 4.65640 3 -16 0 0 82.1597 5.36458 2 0 -1 0 -0.0680 0.07242 5 0 -1 0 0.12994 0.07026 5 0 -1 0 -0.1209 0.08941 2 0 -1 0 0.25091 0.22029 1 0 -1 0 -0.0869 0.11266 3 0 1 0 -0.1425 0.23526 1 0 1 0 0.06340 0.07684 5 0 1 0 0.27791 0.09498 5 0 1 0 -0.1433 0.11806 3 1 -1 0 264.928 11.9777 5 -1 -1 0 261.408 13.1501 1 1 -1 0 295.501 12.1187 1 -1 -1 0 428.963 12.1091 5 -1 -1 0 291.418 12.0433 2 1 -1 0 239.244 11.9763 5 -1 -1 0 383.152 12.0848 3 -1 -1 0 283.335 12.0870 5 1 1 0 443.039 12.0866 2 -1 1 0 472.973 12.2207 1 1 1 0 486.868 12.9527 1 1 1 0 428.408 12.0974 3 -1 1 0 433.910 12.0999 2 1 1 0 291.651 12.0362 4 1 1 0 453.133 12.1161 5 1 1 0 427.524 12.1059 5 -2 -1 0 678.870 23.1041 2 2 -1 0 682.696 23.0352 5 -2 -1 0 785.856 24.2847 1 -2 -1 0 704.881 23.1403 5 -2 -1 0 661.268 23.0914 3 2 -1 0 682.797 23.0799 3 -2 -1 0 694.414 23.1395 5 2 -1 0 687.861 23.0329 5 2 -1 0 755.956 23.5683 1 2 1 0 692.388 23.0941 3 2 1 0 689.222 23.1039 2 -2 1 0 688.306 23.0329 5 -2 1 0 738.288 23.5495 1 2 1 0 705.496 23.1437 5 2 1 0 693.759 23.1380 5 -2 1 0 691.357 23.0826 3 -2 1 0 678.018 23.0296 5 2 1 0 695.374 23.0520 4 2 1 0 804.011 24.3215 1 3 -1 0 3.25889 0.41088 5 3 -1 0 2.16749 0.31478 3 3 -1 0 2.19293 0.29103 5 -3 -1 0 1.11166 0.34533 5 -3 -1 0 1.03953 0.98340 1 -3 -1 0 2.24591 0.34364 3 -3 -1 0 1.83236 0.43200 2 3 -1 0 2.22789 0.73643 1 -3 -1 0 2.58871 0.41623 5 -3 1 0 1.38602 0.35996 2 -3 1 0 2.54805 0.70857 1 3 1 0 2.78228 0.38569 2 3 1 0 1.84324 0.30326 3 -3 1 0 1.23545 0.29383 3 3 1 0 3.16585 0.28953 4 3 1 0 2.24419 0.39933 5 -3 1 0 2.55692 0.29337 5 -3 1 0 2.21027 0.25577 4 -3 1 0 2.43783 0.29035 5 3 1 0 0.27733 0.94690 1 3 1 0 1.57505 0.34177 5 -4 -1 0 61.7887 2.32979 3 -4 -1 0 67.2837 2.44700 5 4 -1 0 61.2696 2.29757 3 4 -1 0 62.1338 2.30115 5 -4 -1 0 66.2469 4.08955 1 -4 -1 0 61.1569 2.40742 2 4 -1 0 63.1658 3.46769 1 4 -1 0 62.9042 2.29765 5 -4 -1 0 61.5122 2.42385 5 -4 1 0 60.3026 2.29299 5 -4 1 0 55.5988 2.42741 3 4 1 0 61.6154 2.18040 4 4 1 0 64.9513 2.44644 5 4 1 0 61.2302 4.02150 1 4 1 0 59.7348 2.43597 5 -4 1 0 57.8048 3.40935 1 -4 1 0 63.0109 2.07840 4 -4 1 0 63.7391 2.29699 5 -4 1 0 59.9180 2.40814 2 4 1 0 61.9706 2.32063 3 4 1 0 59.9660 2.38425 2 5 -1 0 29.4662 1.36216 3 5 -1 0 28.6697 1.35701 5 5 -1 0 30.1009 2.87759 1 -5 -1 0 25.7390 3.21634 1 -5 -1 0 29.7629 1.53217 5 -5 -1 0 28.8105 1.53012 2 -5 -1 0 28.9704 1.41314 3 5 -1 0 30.0752 1.38630 5 -5 -1 0 27.3265 1.51026 5 5 1 0 28.6394 1.52571 5 -5 1 0 28.5445 1.01073 4 5 1 0 28.7734 1.16979 4 -5 1 0 30.3303 1.38762 5 -5 1 0 28.8993 1.38789 3 -5 1 0 29.7013 1.56223 2 -5 1 0 30.2709 1.38037 5 -5 1 0 28.1457 2.85205 1 5 1 0 29.2413 3.23439 1 5 1 0 27.5717 1.46718 2 5 1 0 30.1393 1.38003 3 5 1 0 29.7299 1.52485 5 6 -1 0 85.7536 3.31129 5 6 -1 0 90.8159 3.28008 3 -6 -1 0 84.6159 3.41758 5 -6 -1 0 83.8933 3.44590 5 -6 -1 0 91.2009 5.90060 1 -6 -1 0 93.6173 3.46826 2 -6 -1 0 85.8219 3.30724 3 6 -1 0 84.0096 3.29176 5 6 -1 0 90.9170 5.31121 1 -6 1 0 87.0271 3.30596 5 -6 1 0 85.7707 3.31322 5 6 1 0 95.0264 5.96899 1 6 1 0 87.2633 3.40925 2 6 1 0 85.2003 3.42276 5 -6 1 0 87.2028 3.28445 3 6 1 0 88.2023 3.28883 3 -6 1 0 88.3087 3.47536 2 -6 1 0 85.7803 5.23565 1 6 1 0 86.0899 3.03990 4 6 1 0 90.0751 3.47478 5 7 -1 0 70.4015 5.14663 1 -7 -1 0 66.6818 5.79721 1 7 -1 0 66.5071 2.68774 3 -7 -1 0 65.5370 2.71110 3 7 -1 0 67.6494 2.74742 5 -7 -1 0 64.7229 2.91272 2 -7 -1 0 68.8545 2.92369 5 -7 -1 0 61.5739 2.85990 5 7 -1 0 67.3619 2.76762 5 -7 1 0 64.0050 2.91396 2 -7 1 0 66.1744 2.73391 5 7 1 0 65.5155 2.36810 4 7 1 0 65.8922 2.89685 5 -7 1 0 63.1023 2.73135 5 7 1 0 66.5262 2.71065 3 -7 1 0 66.0111 2.68999 3 -7 1 0 66.1015 5.05955 1 7 1 0 70.0797 2.91362 2 8 -1 0 397.413 13.4125 3 -8 -1 0 394.009 17.0916 1 8 -1 0 388.709 13.4980 5 -8 -1 0 402.326 13.6292 5 -8 -1 0 401.158 13.4495 3 -8 -1 0 402.511 13.6526 2 -8 -1 0 386.099 13.6198 5 -8 1 0 383.956 13.4897 5 8 1 0 390.559 13.0724 4 -8 1 0 410.690 16.5105 1 8 1 0 379.782 13.6467 3 -8 1 0 398.784 13.6647 2 -8 1 0 403.008 13.4218 3 -8 1 0 395.665 13.4924 5 8 1 0 400.088 13.6463 5 8 1 0 412.299 13.6527 2 -9 -1 0 711.712 24.2492 5 -9 -1 0 723.466 24.2673 2 -9 -1 0 710.845 24.0298 3 -9 -1 0 717.089 28.2523 1 -9 -1 0 704.505 28.0254 1 9 -1 0 704.796 24.1068 5 -9 -1 0 744.585 24.2680 5 9 -1 0 724.957 23.9921 3 9 1 0 701.305 23.5734 4 -9 1 0 717.734 23.9988 3 9 1 0 733.473 24.0226 3 9 1 0 715.466 24.2429 2 -9 1 0 725.377 24.2889 2 -9 1 0 725.746 24.1136 5 9 1 0 740.213 24.2729 5 -9 1 0 722.577 27.5272 1 -9 1 0 718.355 24.1022 5 -10 -1 0 155.834 6.11738 5 -10 -1 0 158.010 10.9144 1 -10 -1 0 142.720 10.2193 1 -10 -1 0 156.404 5.82037 3 -10 -1 0 156.746 6.13216 2 10 -1 0 151.217 5.91934 5 10 -1 0 152.099 5.76501 3 10 -1 0 159.483 5.91783 5 -10 -1 0 159.866 6.11258 5 -10 1 0 153.080 5.90878 5 10 1 0 157.546 5.12749 4 -10 1 0 148.783 6.09730 2 -10 1 0 154.895 5.76262 3 -10 1 0 154.322 5.91666 5 -10 1 0 146.342 9.76723 1 -10 1 0 144.351 10.0661 1 10 1 0 147.292 6.05855 5 10 1 0 156.495 5.80767 3 10 1 0 154.445 6.14066 2 10 1 0 152.150 6.07763 5 10 1 0 151.518 5.11452 4 -11 -1 0 97.5789 4.63084 5 11 -1 0 93.1616 4.12762 3 11 -1 0 102.386 4.36876 5 11 -1 0 102.913 4.29733 5 -11 -1 0 98.6718 9.99625 1 -11 -1 0 97.5338 4.55806 2 -11 -1 0 97.7698 4.14195 3 -11 -1 0 95.0469 4.46579 5 -11 -1 0 87.7158 9.55875 1 -11 1 0 99.4875 4.10514 3 -11 1 0 111.451 9.51255 1 -11 1 0 99.0991 4.63545 2 -11 1 0 91.4305 9.35060 1 11 1 0 96.8635 4.18463 3 11 1 0 98.5128 4.48449 5 11 1 0 101.697 4.59201 5 -11 1 0 97.2881 4.29555 5 -12 -1 0 9.54190 1.57565 2 12 -1 0 16.3817 2.03820 5 -12 -1 0 10.0410 1.25826 3 12 -1 0 10.8564 1.41811 3 -12 -1 0 6.61767 6.31152 1 -12 -1 0 9.78149 1.50450 5 12 -1 0 11.0697 1.39702 5 12 1 0 6.38284 1.49257 5 12 1 0 10.3465 1.36965 3 12 1 0 10.5573 1.57292 5 -12 1 0 8.94071 1.55160 2 -12 1 0 10.3673 1.26010 3 -12 1 0 8.26152 1.31790 5 13 -1 0 3.41217 1.38823 3 13 -1 0 3.88803 1.35957 5 -13 -1 0 5.44424 1.19790 3 -13 -1 0 6.58924 1.67509 2 13 -1 0 3.85320 1.22320 5 -13 -1 0 6.38994 1.75743 5 13 1 0 4.19734 1.71521 5 -13 1 0 4.98000 1.14666 3 13 1 0 4.05461 2.00082 5 -13 1 0 3.51936 1.59480 2 13 1 0 0.99675 1.39036 3 -13 1 0 5.19346 1.40615 5 -14 -1 0 -0.2791 1.82558 5 14 -1 0 -1.2617 1.17066 5 -14 -1 0 1.62521 1.51220 2 -14 -1 0 1.13503 1.21011 3 -14 1 0 0.62014 1.09997 3 -14 1 0 0.38946 1.46818 2 14 1 0 -0.7237 1.22491 5 -15 -1 0 0.98066 1.70052 2 -15 -1 0 1.95611 1.40908 3 15 -1 0 2.96805 1.45534 5 -15 1 0 -0.5408 1.75364 2 15 1 0 -1.1813 1.56144 5 -15 1 0 0.98413 1.37498 3 16 -1 0 2.67486 1.58712 5 -16 -1 0 2.67627 1.66857 3 -16 -1 0 3.72059 2.01896 2 -16 1 0 1.26202 1.95028 2 16 1 0 4.28957 1.80841 5 -16 1 0 2.52244 1.60575 3 0 -2 0 15.4794 0.61420 5 0 -2 0 10.0513 0.68450 2 0 -2 0 8.98822 0.70749 3 0 -2 0 15.5453 1.22555 1 0 2 0 11.4364 0.57794 5 0 2 0 14.1481 0.59968 5 0 2 0 10.4412 0.70412 2 0 2 0 10.1405 0.74024 3 1 -2 0 258.070 8.32007 5 1 -2 0 250.216 8.46423 2 -1 -2 0 230.268 8.51018 3 -1 -2 0 246.655 8.45100 5 1 -2 0 236.266 8.31510 5 1 -2 0 260.171 8.64871 1 -1 -2 0 250.596 8.45011 2 -1 -2 0 260.890 9.41117 1 1 2 0 257.686 8.45422 5 1 2 0 263.314 8.46061 5 -1 2 0 257.760 8.46775 2 -1 2 0 264.788 8.64200 1 -1 2 0 260.001 8.48230 3 1 2 0 256.846 8.45191 2 -1 2 0 248.321 8.31478 5 -1 2 0 252.269 8.31996 5 1 2 0 262.844 8.49773 3 -2 -2 0 3049.88 96.3872 1 2 -2 0 2834.39 95.1049 1 -2 2 0 2858.55 95.1137 1 3 -2 0 53.3760 1.86971 5 -3 -2 0 42.1978 2.25608 5 -3 -2 0 54.0312 2.08080 3 -3 -2 0 52.3909 2.06561 2 -3 -2 0 53.8154 2.11165 5 3 -2 0 53.3422 1.87283 5 -3 -2 0 58.2753 3.72323 1 3 -2 0 56.0510 2.51956 1 3 2 0 51.8620 2.05006 2 -3 2 0 55.9093 1.87382 5 3 2 0 51.2819 2.02119 4 -3 2 0 53.5496 1.90906 4 -3 2 0 53.6970 1.86771 5 -3 2 0 52.3010 2.03935 3 -3 2 0 52.6972 2.52175 1 3 2 0 52.3067 2.11125 5 3 2 0 53.6788 2.05992 3 4 -2 0 205.667 7.00122 5 -4 -2 0 200.567 7.21462 5 4 -2 0 208.573 7.98281 1 4 -2 0 210.192 7.00814 5 -4 -2 0 211.610 7.18179 2 -4 -2 0 215.285 9.29735 1 -4 -2 0 211.935 7.15805 3 -4 2 0 214.309 8.00629 1 -4 2 0 215.684 7.00241 5 4 2 0 197.912 7.22610 5 4 2 0 208.491 7.05201 4 4 2 0 213.972 7.17209 2 4 2 0 204.746 7.13352 3 4 2 0 202.787 7.22625 5 -4 2 0 210.135 7.00448 5 -4 2 0 212.474 6.94819 4 -4 2 0 209.093 7.11579 3 5 -2 0 93.1992 3.26887 5 -5 -2 0 88.7430 3.60230 5 -5 -2 0 87.1193 5.73846 1 -5 -2 0 91.2703 3.50095 5 -5 -2 0 90.7678 3.45821 2 5 -2 0 88.8381 3.24923 5 5 -2 0 95.5783 4.66368 1 -5 -2 0 86.2768 3.37630 3 -5 2 0 89.5721 3.25267 5 -5 2 0 88.0253 4.58652 1 -5 2 0 91.4429 3.34874 3 -5 2 0 91.6564 3.09206 4 -5 2 0 89.9046 3.49103 2 5 2 0 92.0810 3.24353 4 5 2 0 90.9639 3.44450 2 -5 2 0 93.7253 3.25289 5 5 2 0 90.8725 3.37909 3 5 2 0 85.9451 3.48667 5 6 -2 0 485.971 16.3992 5 -6 -2 0 497.036 19.4800 1 -6 -2 0 487.304 16.4986 3 -6 -2 0 510.874 16.6537 5 6 -2 0 507.256 16.4629 3 6 -2 0 490.652 16.4074 5 -6 -2 0 501.231 16.5914 2 -6 -2 0 495.459 16.6559 5 6 2 0 496.761 16.6411 5 -6 2 0 510.945 18.2102 1 -6 2 0 496.344 16.3989 5 -6 2 0 497.805 16.4042 5 -6 2 0 484.793 16.6095 2 -6 2 0 486.531 16.1396 4 -6 2 0 499.286 16.4619 3 6 2 0 431.356 16.6739 2 6 2 0 504.986 16.4929 3 6 2 0 494.649 16.3131 4 -7 -2 0 610.253 19.9220 5 7 -2 0 582.514 19.6669 5 7 -2 0 596.992 21.8326 1 7 -2 0 603.900 19.7007 3 -7 -2 0 589.960 19.8578 2 -7 -2 0 583.364 19.7364 3 -7 -2 0 604.439 19.9398 5 -7 -2 0 576.827 23.0835 1 7 -2 0 582.544 19.6638 5 7 2 0 608.812 19.8522 2 -7 2 0 587.220 19.8917 2 7 2 0 593.698 19.9064 5 -7 2 0 575.360 19.6805 3 -7 2 0 583.883 19.6563 5 -7 2 0 578.028 21.9664 1 -7 2 0 608.011 19.6635 5 7 2 0 590.186 19.4966 4 7 2 0 580.010 19.7148 3 -8 -2 0 16.6347 1.74429 2 -8 -2 0 21.1726 1.88870 5 -8 -2 0 18.8744 4.09415 1 8 -2 0 20.5516 1.45747 5 8 -2 0 14.9583 2.00147 3 -8 -2 0 13.2820 3.48581 1 -8 -2 0 18.5578 1.56781 3 -8 -2 0 20.3261 1.78870 5 -8 2 0 16.6069 1.79293 2 -8 2 0 18.5169 1.51766 3 -8 2 0 19.2150 1.44067 5 8 2 0 20.7382 1.79574 2 -8 2 0 20.1852 1.45192 5 -8 2 0 16.2748 2.94564 1 8 2 0 18.6638 1.77629 5 8 2 0 18.9936 1.12283 4 8 2 0 12.6969 1.29122 3 -9 -2 0 5.31582 1.22534 5 -9 -2 0 2.69162 3.25136 1 -9 -2 0 4.49693 0.93437 3 9 -2 0 7.22963 0.97583 3 -9 -2 0 6.75723 1.26314 5 9 -2 0 6.91902 0.96497 5 -9 -2 0 6.24644 1.11646 2 -9 -2 0 6.50299 3.86178 1 9 2 0 5.90599 1.20675 5 9 2 0 4.91217 0.93225 3 -9 2 0 4.95677 0.85364 5 9 2 0 7.51734 1.24416 5 9 2 0 5.38557 1.12539 2 -9 2 0 7.36666 2.88808 1 9 2 0 9.35458 0.89428 4 -9 2 0 5.21814 1.18959 2 -9 2 0 7.10531 0.96047 5 -9 2 0 5.45072 0.93800 3 -10 -2 0 40.6741 5.95776 1 -10 -2 0 43.3698 2.89953 5 -10 -2 0 43.3557 2.84687 2 -10 -2 0 40.3325 6.31319 1 10 -2 0 50.4659 2.55579 5 10 -2 0 44.6866 2.50546 5 -10 -2 0 46.4051 2.96897 5 -10 -2 0 43.5470 2.53365 3 10 -2 0 46.8838 2.54109 3 10 2 0 46.6546 1.88030 4 -10 2 0 44.8660 6.34230 1 10 2 0 44.4146 2.56439 3 -10 2 0 45.3207 2.51011 5 -10 2 0 45.1514 2.94068 2 -10 2 0 44.9169 2.45863 3 -10 2 0 44.7608 6.51231 1 -10 2 0 44.4967 2.49316 5 10 2 0 40.2812 2.88133 2 10 2 0 43.4570 2.87110 5 10 2 0 45.4148 2.89746 5 -11 -2 0 0.84510 0.90708 3 -11 -2 0 4.50362 1.44740 5 11 -2 0 2.26579 1.01070 3 11 -2 0 2.64521 0.99174 5 11 -2 0 0.70049 1.22336 5 -11 -2 0 7.83755 5.38908 1 -11 -2 0 1.99413 4.80241 1 -11 -2 0 2.88394 1.25438 2 -11 -2 0 0.51097 1.11395 5 -11 2 0 1.41229 1.21778 2 11 2 0 2.42109 1.15270 5 11 2 0 1.90754 0.48949 4 -11 2 0 3.94632 4.02098 1 11 2 0 -0.3169 1.23198 5 -11 2 0 1.91676 4.02824 1 -11 2 0 3.48727 1.03200 5 11 2 0 1.36494 1.03678 3 -11 2 0 2.57103 0.89741 3 11 2 0 2.42273 0.53266 4 12 -2 0 123.239 5.25204 5 -12 -2 0 119.843 5.47564 2 -12 -2 0 124.287 5.51664 5 -12 -2 0 126.069 5.06288 3 -12 -2 0 109.736 13.3497 1 12 -2 0 118.175 5.27325 5 -12 2 0 122.464 5.10143 5 -12 2 0 126.849 4.96747 3 12 2 0 119.025 5.13297 3 12 2 0 121.768 5.59710 5 -12 2 0 113.645 6.44325 2 12 2 0 125.589 5.48247 5 12 2 0 121.047 4.13765 4 -13 -2 0 3.37043 1.48067 5 -13 -2 0 4.27576 1.26365 3 13 -2 0 1.33732 1.07237 5 -13 -2 0 2.97918 1.47032 2 13 -2 0 2.81400 1.28755 5 -13 2 0 1.97054 1.50177 2 13 2 0 1.48366 1.41620 5 13 2 0 2.54151 2.52293 5 13 2 0 0.83960 1.46949 3 -13 2 0 1.12884 1.21865 5 -13 2 0 3.18300 1.13542 3 14 -2 0 60.8671 3.59427 5 -14 -2 0 64.1001 4.23987 2 -14 -2 0 61.7926 4.35005 5 -14 -2 0 68.3241 3.65039 3 -14 2 0 62.0131 3.51127 3 -14 2 0 55.6696 4.13801 2 14 2 0 64.8358 4.20310 5 15 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2.35215 1 2 -3 0 22.4086 0.81764 5 -2 -3 0 22.9686 1.25575 3 2 -3 0 22.2463 1.23184 1 -2 -3 0 23.5448 1.20332 2 -2 -3 0 22.5498 1.17303 5 2 -3 0 20.0452 0.82812 5 -2 3 0 21.6963 1.18609 2 2 3 0 21.2603 1.15052 2 -2 3 0 22.3403 1.22678 1 2 3 0 21.0441 1.14672 5 2 3 0 21.0876 1.14885 5 2 3 0 23.8561 1.18323 4 -2 3 0 21.7448 0.81084 5 2 3 0 21.0525 1.20131 3 -2 3 0 22.8035 0.81828 5 -3 -3 0 483.239 17.9902 1 -3 -3 0 468.993 16.0016 3 -3 -3 0 486.304 16.0254 5 3 -3 0 467.923 15.6974 5 3 -3 0 497.775 16.1429 1 -3 -3 0 467.490 16.0176 5 -3 -3 0 471.600 15.9628 2 -3 -3 0 502.858 18.0897 1 3 -3 0 455.688 15.6903 5 3 3 0 489.487 16.0278 5 -3 3 0 477.903 15.6942 5 -3 3 0 484.860 15.6953 5 3 3 0 467.986 16.0111 5 3 3 0 479.772 15.9354 4 3 3 0 475.464 15.9504 2 -3 3 0 495.532 16.1533 1 -3 3 0 493.252 16.0067 2 3 3 0 477.618 15.9925 3 -4 -3 0 14.7316 2.51340 1 4 -3 0 14.8369 0.72977 5 4 -3 0 14.9844 0.75358 5 -4 -3 0 15.7975 1.21001 5 -4 -3 0 14.0185 1.18886 2 -4 -3 0 15.8737 1.17894 3 4 -3 0 15.1463 1.56449 1 -4 -3 0 9.43439 2.20160 1 -4 -3 0 17.6705 1.24262 5 4 3 0 15.9733 1.17269 3 -4 3 0 15.4461 0.74099 5 4 3 0 15.1957 1.20332 5 -4 3 0 14.4763 1.08861 3 -4 3 0 16.5877 1.21920 2 -4 3 0 16.1353 0.74339 5 -4 3 0 16.4310 0.90330 4 4 3 0 15.1136 1.04367 4 -4 3 0 15.3708 1.63647 1 4 3 0 14.7459 1.20975 5 4 3 0 14.6663 1.14309 2 -5 -3 0 8.91129 1.13797 5 -5 -3 0 8.19330 1.07875 3 5 -3 0 8.63303 0.66773 5 -5 -3 0 8.83569 2.45540 1 -5 -3 0 6.16611 2.22664 1 5 -3 0 8.29211 1.29302 1 5 -3 0 11.6988 0.72256 5 -5 -3 0 9.00182 1.10431 2 -5 -3 0 8.41267 1.14403 5 -5 3 0 9.06888 0.78477 5 5 3 0 5.77058 0.73400 2 5 3 0 6.52647 0.82549 5 5 3 0 9.24651 0.92188 4 -5 3 0 9.08377 0.72063 4 5 3 0 8.96979 1.05852 3 -5 3 0 10.1416 1.47589 1 -5 3 0 7.49516 0.66638 5 -5 3 0 8.25354 1.00938 3 -6 -3 0 9.91373 2.88377 1 -6 -3 0 14.3370 1.41489 2 -6 -3 0 15.4072 1.52648 5 -6 -3 0 15.3703 1.45925 5 6 -3 0 16.0416 2.46083 1 6 -3 0 14.2236 0.96224 5 -6 -3 0 10.2350 2.91120 1 -6 -3 0 17.6460 1.38937 3 6 -3 0 15.9220 1.00087 5 6 3 0 13.6654 1.37829 3 -6 3 0 14.8902 1.27004 3 -6 3 0 15.9348 2.68563 1 -6 3 0 18.4133 1.54111 2 -6 3 0 12.0556 1.03064 4 6 3 0 15.8283 1.39030 2 -6 3 0 14.5339 0.97834 5 -6 3 0 15.3411 0.87032 4 6 3 0 14.3020 1.11209 4 6 3 0 13.8945 1.52428 5 -6 3 0 15.1620 0.97839 5 6 3 0 14.2422 1.49718 5 -7 -3 0 52.5970 2.66374 2 -7 -3 0 55.2726 6.01921 1 -7 -3 0 53.4967 2.56879 3 -7 -3 0 52.2489 2.74622 5 7 -3 0 53.2795 4.06784 1 -7 -3 0 52.8362 5.90585 1 -7 -3 0 53.0482 2.72097 5 7 -3 0 58.0657 2.30447 5 7 3 0 55.7705 2.76181 5 -7 3 0 53.2830 2.73359 2 7 3 0 54.4429 2.29159 4 -7 3 0 58.1937 2.28030 5 -7 3 0 57.4346 2.28730 5 -7 3 0 51.2147 4.30523 1 7 3 0 54.0020 2.61664 2 -7 3 0 54.8991 2.01147 4 -7 3 0 54.4367 2.48038 3 -7 3 0 53.8537 2.00172 4 7 3 0 55.4934 2.73948 5 7 3 0 54.5929 2.53533 3 -8 -3 0 72.9077 7.45856 1 -8 -3 0 73.5560 3.41177 2 -8 -3 0 76.3155 3.25908 3 8 -3 0 72.8688 2.98997 5 -8 -3 0 73.2002 7.77173 1 -8 -3 0 69.6587 3.85614 5 -8 -3 0 78.5116 3.55551 5 8 3 0 74.6678 3.24820 3 -8 3 0 73.0500 3.16601 3 -8 3 0 77.9218 2.99990 5 -8 3 0 73.3173 2.54820 4 8 3 0 75.4303 3.53357 5 -8 3 0 71.7576 2.53907 4 -8 3 0 75.5493 5.56985 1 -8 3 0 70.8664 2.96854 5 8 3 0 72.7056 3.37713 2 8 3 0 71.7301 2.90793 4 8 3 0 76.5566 3.52010 5 -8 3 0 70.2522 3.44844 2 -9 -3 0 49.2714 2.96111 5 9 -3 0 48.4990 2.32672 5 9 -3 0 49.5918 2.35788 5 -9 -3 0 46.3358 2.80253 2 -9 -3 0 50.6013 2.95087 5 -9 -3 0 47.0822 2.58498 3 -9 -3 0 55.9893 7.55864 1 9 3 0 50.7433 2.93753 5 9 3 0 47.3556 2.78988 2 -9 3 0 49.2924 2.51061 3 -9 3 0 46.3649 2.32963 5 -9 3 0 48.1927 2.34813 5 9 3 0 44.8553 2.57310 3 -9 3 0 45.2208 2.86195 2 9 3 0 46.7784 2.13755 4 9 3 0 48.6548 2.95786 5 -9 3 0 47.4879 5.57875 1 -9 3 0 47.4590 5.30488 1 -10 -3 0 200.572 7.83105 5 -10 -3 0 181.701 13.0917 1 -10 -3 0 211.613 7.55147 3 -10 -3 0 199.667 13.3581 1 10 -3 0 209.238 7.35871 5 -10 -3 0 205.305 7.76088 2 -10 -3 0 210.060 7.93180 5 10 -3 0 202.730 7.31869 5 -10 3 0 215.352 7.67929 5 -10 3 0 201.655 7.40982 3 -10 3 0 195.005 10.7687 1 10 3 0 200.335 7.49299 3 -10 3 0 196.916 7.76716 2 10 3 0 198.818 7.81196 5 10 3 0 200.833 7.73186 2 -10 3 0 204.679 7.33279 5 10 3 0 199.767 7.04230 4 -10 3 0 202.824 10.7846 1 10 3 0 211.250 7.92526 5 -11 -3 0 50.1956 3.33369 2 -11 -3 0 52.0128 2.94096 3 11 -3 0 55.5576 2.72992 5 -11 -3 0 34.1374 6.98698 1 11 -3 0 52.4742 2.74180 5 -11 -3 0 50.6431 3.36672 5 -11 -3 0 69.4685 11.0180 1 -11 -3 0 57.2984 3.58103 5 -11 3 0 51.4564 2.79262 3 11 3 0 59.4479 3.56881 5 -11 3 0 51.9545 3.43996 2 11 3 0 48.9084 3.02304 3 -11 3 0 48.4399 2.73746 5 -11 3 0 45.0459 7.55974 1 11 3 0 52.3904 2.25585 4 11 3 0 53.4529 3.32282 5 -12 -3 0 19.6877 2.54056 5 -12 -3 0 19.5443 2.79281 5 -12 -3 0 10.8620 7.09480 1 -12 -3 0 21.3957 2.29475 3 -12 -3 0 15.8543 2.13575 2 12 -3 0 21.7391 2.03357 5 12 -3 0 20.1410 2.00036 5 12 3 0 22.7372 2.47957 5 12 3 0 22.0014 2.85112 5 -12 3 0 21.2442 2.80729 2 12 3 0 21.3631 1.50735 4 12 3 0 19.3342 1.33476 4 -12 3 0 20.8777 2.12135 3 -12 3 0 20.6916 2.20093 5 12 3 0 18.8428 2.61940 3 -13 -3 0 115.027 4.95231 3 13 -3 0 106.586 4.66247 5 -13 -3 0 109.626 5.32972 2 -13 -3 0 103.384 5.42721 5 13 -3 0 105.842 4.64544 5 -13 3 0 106.304 4.69444 3 13 3 0 107.844 3.84903 4 13 3 0 107.409 5.43127 5 -13 3 0 108.003 5.34877 2 -14 -3 0 13.2940 1.78645 3 14 -3 0 13.3954 1.61175 5 -14 -3 0 10.6376 2.29006 5 -14 -3 0 13.9473 2.09991 2 14 -3 0 14.0906 1.73406 5 14 3 0 15.2752 2.29902 5 -14 3 0 16.3438 2.33262 2 -14 3 0 12.4702 1.63683 3 -15 -3 0 166.950 7.61181 2 15 -3 0 159.380 6.77099 5 -15 -3 0 165.058 7.00830 3 -15 3 0 174.850 7.33230 3 15 3 0 175.229 7.75715 5 -15 3 0 163.058 7.68480 2 16 -3 0 61.0388 4.00550 5 -16 -3 0 72.5790 4.54314 3 -16 -3 0 72.8546 5.35895 2 16 3 0 67.6105 5.17850 5 -16 3 0 71.8727 5.37537 2 -16 3 0 65.4243 5.87452 3 0 -4 0 1044.60 35.2411 5 0 -4 0 1069.09 35.3642 2 0 -4 0 1038.31 35.2351 5 0 -4 0 1150.33 36.5405 1 0 -4 0 1122.70 36.5070 1 0 -4 0 1059.24 35.4391 3 0 4 0 1111.46 35.4465 3 0 4 0 1055.41 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2.73170 1 -3 -4 0 75.2102 4.98411 1 -3 -4 0 69.3047 2.89153 5 -3 -4 0 74.8546 5.18867 1 -3 -4 0 69.4938 2.93071 3 -3 -4 0 70.9089 2.86587 2 -3 -4 0 74.0826 2.90240 5 3 4 0 73.2942 2.85501 2 3 4 0 73.1240 2.90664 5 -3 4 0 73.0602 2.89240 3 3 4 0 71.2262 2.87654 5 -3 4 0 68.9307 2.70230 1 3 4 0 70.6092 2.84506 4 3 4 0 73.4869 2.93441 3 -3 4 0 69.5785 2.89083 2 -4 -4 0 53.3340 2.40555 3 -4 -4 0 58.7329 5.10976 1 4 -4 0 54.7235 1.81506 5 -4 -4 0 51.6753 2.39938 5 -4 -4 0 51.3502 2.35017 5 -4 -4 0 52.2074 4.77744 1 4 -4 0 51.8064 1.80085 5 4 -4 0 55.7997 2.33328 1 -4 -4 0 50.3792 2.33081 2 4 4 0 46.5279 2.53547 3 4 4 0 50.4133 2.25226 4 -4 4 0 52.4006 1.80613 5 4 4 0 52.2552 2.39264 5 4 4 0 51.4725 2.37073 5 -4 4 0 55.3952 1.81098 5 -4 4 0 53.9654 2.53252 2 -4 4 0 50.5242 2.12822 4 -4 4 0 49.1080 2.28912 1 4 4 0 53.5146 2.30000 2 -5 -4 0 493.183 16.6408 3 -5 -4 0 501.494 16.6979 5 5 -4 0 483.084 16.1865 5 -5 -4 0 485.456 19.6869 1 -5 -4 0 491.031 16.6071 2 5 -4 0 496.415 17.0480 1 5 -4 0 486.411 16.1941 5 -5 -4 0 490.782 16.7050 5 -5 -4 0 498.849 19.8306 1 -5 4 0 511.169 16.6716 2 -5 4 0 501.548 16.1903 5 5 4 0 481.520 16.4995 4 -5 4 0 490.054 16.5633 3 5 4 0 497.524 16.6967 5 -5 4 0 488.247 16.3712 4 -5 4 0 502.068 16.1912 5 -5 4 0 476.069 16.3517 4 -5 4 0 501.866 16.9662 1 5 4 0 494.089 16.6154 3 5 4 0 495.276 16.7037 5 -6 -4 0 171.750 6.35137 2 -6 -4 0 173.371 9.85602 1 -6 -4 0 176.075 9.84672 1 -6 -4 0 165.522 6.33774 3 -6 -4 0 170.068 6.44725 5 6 -4 0 175.150 5.89829 5 -6 -4 0 175.046 6.45064 5 6 4 0 176.053 6.47071 5 -6 4 0 177.534 6.43403 2 -6 4 0 169.088 5.97726 4 -6 4 0 179.509 5.89482 5 -6 4 0 176.337 5.89050 5 6 4 0 176.562 6.46530 5 -6 4 0 168.401 7.10779 1 -6 4 0 171.944 5.97061 4 -6 4 0 169.846 6.25952 3 6 4 0 173.024 6.17715 4 6 4 0 174.743 6.32244 3 6 4 0 178.253 6.32705 2 -7 -4 0 1.19516 0.88841 2 -7 -4 0 -0.5488 0.82647 5 -7 -4 0 -0.4558 3.03586 1 -7 -4 0 1.14864 0.83636 3 -7 -4 0 2.24918 0.92871 5 -7 -4 0 -1.2162 3.15914 1 7 -4 0 0.29194 0.46583 5 -7 4 0 1.15263 0.47657 4 -7 4 0 1.19013 0.92000 2 -7 4 0 1.00116 1.58558 1 -7 4 0 0.13491 0.42855 5 -7 4 0 0.23512 0.83398 2 7 4 0 0.80384 0.88005 5 -7 4 0 1.11425 0.75021 3 -7 4 0 1.32148 0.47606 5 -7 4 0 1.20874 0.45087 4 7 4 0 1.32825 1.05579 5 7 4 0 1.00894 0.84667 2 7 4 0 1.07636 0.77053 3 7 4 0 1.35254 0.68238 4 -8 -4 0 7.94542 1.31857 5 -8 -4 0 11.6964 4.85901 1 -8 -4 0 6.81915 1.22881 5 -8 -4 0 7.66037 1.12953 3 -8 -4 0 4.48962 4.04231 1 8 -4 0 8.25242 1.02113 5 -8 -4 0 7.76598 1.24190 2 8 -4 0 8.60167 1.04541 5 8 4 0 10.6323 1.32131 4 8 4 0 7.60208 1.14018 2 -8 4 0 8.93792 2.19177 1 -8 4 0 9.33321 2.26860 1 8 4 0 7.24571 1.22825 5 -8 4 0 5.21628 1.18436 2 -8 4 0 9.87419 0.84293 4 -8 4 0 9.03251 0.85759 4 -8 4 0 8.14992 1.07984 3 -8 4 0 7.98147 1.05638 5 8 4 0 8.26053 1.71485 5 8 4 0 7.48792 1.06892 3 -8 4 0 9.48478 1.09870 5 -9 -4 0 157.681 6.29716 5 -9 -4 0 126.897 12.7448 1 -9 -4 0 155.855 6.00852 3 -9 -4 0 155.967 6.27482 5 -9 -4 0 149.566 6.09282 2 9 -4 0 158.201 5.57093 5 -9 -4 0 149.354 11.5724 1 9 -4 0 156.275 5.56371 5 -9 4 0 158.479 5.87815 3 9 4 0 154.752 5.62761 4 -9 4 0 157.494 5.57683 5 -9 4 0 157.449 6.21363 2 -9 4 0 154.045 5.21474 4 -9 4 0 151.645 8.22272 1 9 4 0 157.368 6.12802 2 -9 4 0 151.596 5.21401 4 -9 4 0 156.139 5.56797 5 9 4 0 152.452 6.22593 5 -9 4 0 153.138 8.31710 1 9 4 0 155.020 6.30587 5 9 4 0 155.967 5.98062 3 10 -4 0 178.243 6.38585 5 -10 -4 0 175.653 6.79856 3 10 -4 0 180.112 6.37921 5 -10 -4 0 178.200 6.97794 2 -10 -4 0 186.625 13.4903 1 -10 -4 0 179.272 7.16594 5 -10 -4 0 174.615 13.8894 1 -10 -4 0 179.992 7.15074 5 10 4 0 174.959 7.01322 2 -10 4 0 163.694 7.07607 5 -10 4 0 169.120 9.67855 1 10 4 0 177.108 6.34896 4 -10 4 0 179.226 6.65777 3 -10 4 0 179.669 7.07723 2 10 4 0 176.492 7.15638 5 10 4 0 170.248 6.76309 3 10 4 0 181.213 7.11774 5 -10 4 0 179.017 9.87878 1 -11 -4 0 174.243 6.97343 2 -11 -4 0 154.246 14.3687 1 11 -4 0 178.546 6.33504 5 11 -4 0 169.999 6.32666 5 -11 -4 0 168.579 7.10079 5 -11 -4 0 172.746 14.1894 1 -11 -4 0 174.990 7.29229 5 -11 -4 0 173.782 6.75651 3 11 4 0 173.777 7.29686 5 -11 4 0 170.964 6.57524 3 11 4 0 175.466 6.18811 4 -11 4 0 167.354 7.03766 2 -11 4 0 165.906 10.6874 1 -11 4 0 174.594 6.36821 5 11 4 0 167.568 6.75418 3 11 4 0 171.761 7.10254 5 -12 -4 0 -2.0221 1.80020 5 -12 -4 0 0.67362 1.59180 2 -12 -4 0 0.49394 1.17419 3 -12 -4 0 0.58522 1.42345 5 12 -4 0 3.09614 0.93496 5 12 -4 0 0.87289 0.84290 5 -12 -4 0 5.13215 7.69195 1 12 4 0 3.61865 1.51619 5 -12 4 0 -1.1159 1.06167 5 12 4 0 1.43957 0.77023 4 12 4 0 2.01453 1.76959 5 -12 4 0 1.30751 1.07947 3 12 4 0 1.58004 0.95976 4 -12 4 0 1.28070 1.48278 2 -13 -4 0 36.1652 3.30909 2 13 -4 0 33.6256 2.39715 5 -13 -4 0 36.5763 3.54141 5 -13 -4 0 30.5440 2.99668 3 13 -4 0 31.3084 2.30727 5 -13 4 0 32.5819 2.73836 3 -13 4 0 32.7918 3.36432 2 13 4 0 37.5094 3.49371 5 13 4 0 31.1989 1.88372 4 14 -4 0 18.3288 2.29421 5 14 -4 0 22.0517 2.19370 5 -14 -4 0 20.0578 2.57596 5 -14 -4 0 24.7814 2.94275 3 -14 -4 0 27.5433 3.40994 2 -14 4 0 24.9297 2.78898 3 14 4 0 18.8586 2.37588 5 -14 4 0 22.7728 2.66303 2 -15 -4 0 1.99837 2.07581 2 -15 -4 0 7.59481 1.90655 3 15 -4 0 3.71250 1.26162 5 -15 4 0 8.75089 1.79258 3 15 4 0 6.08816 2.24652 5 -15 4 0 5.97278 2.21180 2 0 -5 0 0.15007 1.35565 1 0 -5 0 -0.2784 0.34181 5 0 -5 0 0.03939 0.51165 2 0 -5 0 -0.1700 0.38366 5 0 -5 0 0.30107 1.12415 1 0 5 0 0.14248 0.52308 2 0 5 0 -0.5566 0.61152 3 0 5 0 0.97393 0.38954 5 0 5 0 -0.2888 0.49835 4 0 5 0 0.29076 0.33834 5 1 -5 0 9.71558 1.09641 2 1 -5 0 10.6875 0.72731 5 1 -5 0 8.64559 1.41123 1 -1 -5 0 8.65147 1.78702 1 -1 -5 0 12.1553 0.95436 5 -1 -5 0 9.75980 1.22475 3 -1 -5 0 9.27889 0.89863 5 1 -5 0 8.99888 0.71556 5 -1 -5 0 8.68137 1.09406 2 1 -5 0 8.15977 1.33114 1 -1 -5 0 10.1435 3.36591 1 -1 5 0 7.92118 1.05285 4 -1 5 0 9.95021 0.73692 5 1 5 0 8.31368 0.88300 5 1 5 0 10.9803 0.93513 5 -1 5 0 9.25150 0.82185 5 -1 5 0 10.8740 1.13384 2 1 5 0 10.9176 1.12295 2 1 5 0 10.7932 1.25222 3 -1 5 0 7.03839 0.99196 3 1 5 0 12.7170 1.17635 4 2 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4 5 0 1.40152 0.67805 4 -4 5 0 2.17331 0.60233 4 -4 5 0 2.94507 0.74501 3 4 5 0 1.67931 0.68145 5 4 5 0 1.80938 0.73970 3 -4 5 0 2.20938 0.75015 2 -4 5 0 1.64353 0.56951 4 -5 -5 0 35.2919 2.13821 5 -5 -5 0 47.3807 2.25754 5 -5 -5 0 38.2934 5.30460 1 -5 -5 0 31.5644 5.22291 1 -5 -5 0 34.5474 2.14827 3 -5 -5 0 36.3817 2.08269 2 5 5 0 38.0394 2.18602 3 5 5 0 35.7736 2.12758 5 -5 5 0 34.2538 2.05553 3 -5 5 0 34.4926 1.81163 4 5 5 0 37.0430 2.06343 2 5 5 0 44.1082 2.25857 5 -5 5 0 35.9074 2.18603 2 5 5 0 35.6488 2.00688 4 -5 5 0 34.5301 1.77001 4 -6 -5 0 73.9546 7.16273 1 -6 -5 0 76.2688 3.48635 3 -6 -5 0 72.6034 7.06311 1 -6 -5 0 77.5699 3.47287 2 -6 -5 0 79.4160 3.57232 5 -6 -5 0 78.0962 3.56187 5 -6 5 0 68.2060 3.71613 1 6 5 0 76.6576 3.64181 5 -6 5 0 77.8471 3.18908 1 -6 5 0 79.7683 3.39303 3 -6 5 0 81.7649 3.58162 2 -6 5 0 78.6728 3.04978 4 6 5 0 77.9736 3.28705 4 6 5 0 81.4509 3.43473 2 -6 5 0 79.5718 3.07536 4 6 5 0 79.2177 3.48967 3 6 5 0 82.0992 3.59904 5 -7 -5 0 202.231 7.48318 2 7 -5 0 200.380 6.77190 5 -7 -5 0 190.070 11.7429 1 -7 -5 0 195.792 7.47893 3 -7 -5 0 197.153 7.61440 5 -7 -5 0 199.341 11.8877 1 -7 -5 0 206.424 7.62784 5 7 -5 0 203.402 6.78437 5 7 5 0 202.443 7.61654 5 7 5 0 208.453 7.65321 5 -7 5 0 204.892 7.60221 2 -7 5 0 204.334 7.02833 4 -7 5 0 205.481 6.78225 5 -7 5 0 199.707 6.99636 4 7 5 0 204.665 7.44468 2 -7 5 0 197.922 7.37151 3 7 5 0 206.964 7.27190 4 -7 5 0 210.839 6.78606 5 -7 5 0 200.358 7.78423 1 7 5 0 201.251 7.45135 3 -8 -5 0 25.6405 2.31267 2 -8 -5 0 25.9278 2.36531 5 -8 -5 0 28.3428 2.24304 3 8 -5 0 27.7698 1.32409 5 8 -5 0 27.6427 1.34145 5 -8 -5 0 24.1959 5.16146 1 -8 -5 0 22.6509 5.42296 1 -8 -5 0 25.7066 2.44801 5 -8 5 0 29.7488 3.45764 1 8 5 0 27.6900 2.37122 5 -8 5 0 25.3177 2.31331 2 -8 5 0 28.2444 1.48808 4 -8 5 0 25.8872 2.59156 2 -8 5 0 28.8900 1.36941 5 -8 5 0 29.1192 2.05183 3 8 5 0 23.8688 2.27517 2 -8 5 0 28.0197 1.38870 5 8 5 0 27.3093 1.89571 4 -8 5 0 26.2900 4.50712 1 8 5 0 25.6587 2.26300 3 -8 5 0 27.4597 1.53956 4 8 5 0 28.3306 2.56220 5 9 -5 0 177.610 6.10039 5 -9 -5 0 171.949 6.85934 2 -9 -5 0 169.751 6.99159 5 -9 -5 0 181.793 6.81815 3 9 -5 0 177.287 6.10558 5 -9 -5 0 169.179 7.29067 5 -9 -5 0 168.327 13.1525 1 -9 -5 0 169.704 12.3931 1 -9 5 0 173.753 6.94775 2 9 5 0 179.339 6.81142 3 9 5 0 170.681 6.82088 2 9 5 0 176.910 6.45849 4 -9 5 0 173.897 8.19030 1 -9 5 0 173.731 6.05719 4 -9 5 0 189.002 6.30012 5 -9 5 0 181.455 6.12170 5 9 5 0 175.965 7.07028 5 9 5 0 172.704 6.99808 5 -9 5 0 176.982 6.64639 3 -9 5 0 173.808 6.04081 4 -9 5 0 176.028 8.31786 1 -10 -5 0 10.1261 5.85845 1 10 -5 0 11.9706 1.19191 5 -10 -5 0 12.4790 1.81995 5 -10 -5 0 9.41352 1.57736 5 -10 -5 0 9.75210 1.40149 3 10 -5 0 12.7495 1.19632 5 -10 -5 0 6.41014 6.40633 1 -10 -5 0 7.87054 1.51147 2 -10 5 0 10.5646 1.33603 3 10 5 0 10.7610 1.16563 4 -10 5 0 7.52842 2.99285 1 -10 5 0 13.3844 1.40941 5 10 5 0 8.65831 1.57289 3 10 5 0 10.4576 1.83553 5 10 5 0 9.24031 1.54263 5 -10 5 0 11.9724 0.88944 4 -10 5 0 8.16066 1.53672 2 -11 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0.22489 1.54661 3 -14 5 0 -0.9985 1.65575 3 14 5 0 2.44943 2.24462 5 -14 5 0 -1.8011 1.66851 2 -15 -5 0 6.99301 2.13089 2 -15 -5 0 13.0679 2.16032 3 15 -5 0 10.2386 1.32522 5 15 5 0 7.18178 2.62003 5 -15 5 0 9.74382 2.42887 2 -15 5 0 9.17904 1.95829 3 0 -6 0 231.129 9.56939 1 0 -6 0 217.655 7.71008 5 0 -6 0 227.981 7.71414 5 0 -6 0 218.063 7.92597 2 0 -6 0 229.071 9.55061 1 0 6 0 234.995 7.99092 4 0 6 0 226.836 7.70923 5 0 6 0 220.945 7.70439 5 0 6 0 225.654 7.94269 2 0 6 0 221.894 8.05822 3 1 -6 0 8.26192 0.75585 5 -1 -6 0 7.12138 0.99164 5 -1 -6 0 7.16802 1.00754 3 1 -6 0 7.32520 0.77613 5 -1 -6 0 4.78476 1.87765 1 -1 -6 0 5.90053 0.85915 2 -1 -6 0 6.47851 0.72986 5 1 -6 0 6.06834 1.48257 1 -1 -6 0 5.70783 1.94518 1 1 -6 0 6.08103 0.87003 2 1 -6 0 5.06867 1.52116 1 1 6 0 5.95615 0.92350 3 -1 6 0 7.25727 0.77914 5 -1 6 0 7.52891 0.95770 2 1 6 0 5.58310 0.88219 2 -1 6 0 6.70311 0.79761 5 1 6 0 7.68762 0.99944 5 1 6 0 5.08597 0.88416 4 1 6 0 6.34902 0.72558 5 -1 6 0 6.92288 0.91171 4 -1 6 0 4.83914 1.00862 3 -2 -6 0 7.97394 0.85998 5 -2 -6 0 4.30877 0.72570 5 2 -6 0 6.97483 1.28109 1 2 -6 0 8.65240 0.63319 5 -2 -6 0 5.43547 2.15943 1 -2 -6 0 6.52402 2.19617 1 -2 -6 0 5.48508 0.96063 3 2 -6 0 5.26653 0.89064 2 2 -6 0 7.16957 0.64123 5 2 -6 0 6.18582 1.19510 1 -2 -6 0 7.18790 0.93153 2 2 6 0 8.50031 1.16416 5 2 6 0 3.51810 0.85366 2 -2 6 0 6.10523 0.66503 5 -2 6 0 5.39181 0.81051 4 2 6 0 7.08701 0.85940 5 -2 6 0 7.27969 0.64309 5 2 6 0 12.6834 1.43507 4 -2 6 0 7.37265 0.99582 2 -2 6 0 5.81859 0.98740 3 2 6 0 8.28425 1.09418 3 -3 -6 0 7.70503 2.74281 1 -3 -6 0 5.67176 0.86833 2 -3 -6 0 4.47082 0.96859 3 -3 -6 0 10.9420 2.69917 1 -3 -6 0 9.17130 1.08937 5 -3 -6 0 5.24633 0.83418 5 -3 6 0 8.76983 1.03505 2 -3 6 0 5.94573 0.84007 4 -3 6 0 8.65925 1.11254 3 3 6 0 7.59030 1.03039 4 3 6 0 4.76550 0.79307 5 3 6 0 15.3261 1.42262 5 3 6 0 7.01901 0.93687 2 3 6 0 6.11547 1.00909 3 -4 -6 0 21.9029 3.71340 1 -4 -6 0 28.2883 1.91731 5 -4 -6 0 29.7354 1.96131 5 -4 -6 0 30.8457 1.95366 2 -4 -6 0 28.3439 2.11819 3 4 6 0 26.5855 1.89057 5 4 6 0 25.5102 2.08424 3 -4 6 0 24.7695 2.00656 2 -4 6 0 24.6042 2.01225 3 4 6 0 28.3894 1.90245 4 -4 6 0 27.5150 1.78999 4 -4 6 0 25.9233 1.72539 4 4 6 0 25.7924 1.94057 5 4 6 0 25.6367 1.90338 2 -5 -6 0 234.268 8.59054 5 -5 -6 0 244.317 8.59168 5 -5 -6 0 233.501 12.6007 1 -5 -6 0 237.980 8.51957 2 -5 -6 0 217.063 12.3554 1 -5 -6 0 238.452 8.65098 3 -5 6 0 233.260 8.28462 4 -5 6 0 234.854 8.52682 3 5 6 0 241.771 8.58620 5 5 6 0 228.445 8.53323 5 5 6 0 244.228 8.47963 2 -5 6 0 237.268 8.57681 2 -5 6 0 242.184 8.32884 4 5 6 0 242.746 8.62501 3 -5 6 0 247.365 8.58161 3 5 6 0 230.545 8.45358 4 -6 -6 0 16.2738 1.96869 2 -6 -6 0 21.1431 2.07322 5 -6 -6 0 17.9904 2.01854 5 -6 -6 0 21.7169 4.52968 1 -6 -6 0 16.1447 1.99550 3 -6 -6 0 20.1076 4.64101 1 6 6 0 19.0829 2.03618 5 -6 6 0 19.7416 1.52383 4 -6 6 0 20.1168 2.03902 3 -6 6 0 20.5354 1.57263 4 -6 6 0 18.5930 2.17993 2 -6 6 0 15.8316 1.89166 3 6 6 0 18.1187 1.96328 2 6 6 0 19.7780 2.14369 3 6 6 0 19.2213 1.83187 4 6 6 0 17.5082 2.10532 5 -7 -6 0 75.5493 3.78673 5 -7 -6 0 75.3301 3.75408 3 -7 -6 0 67.8780 9.01038 1 -7 -6 0 77.2599 3.81203 5 -7 -6 0 76.9143 3.69155 2 -7 -6 0 60.2571 8.87912 1 7 6 0 79.8404 3.81849 5 -7 6 0 75.6321 3.18795 4 7 6 0 74.1834 3.62596 2 -7 6 0 75.5413 3.68228 3 -7 6 0 76.7465 3.13039 4 7 6 0 71.1863 3.72147 3 -7 6 0 74.1693 3.61764 3 -7 6 0 74.8887 3.92782 2 7 6 0 78.5471 3.89217 5 7 6 0 76.6415 3.48497 4 -8 -6 0 63.9213 3.58881 5 -8 -6 0 64.3995 3.48443 5 -8 -6 0 58.7474 7.62859 1 -8 -6 0 59.5068 9.13725 1 -8 -6 0 61.6156 3.35022 2 -8 -6 0 57.5216 3.32336 3 8 6 0 58.4560 2.98757 4 -8 6 0 57.5404 2.89813 4 8 6 0 58.7136 3.45714 5 -8 6 0 57.3309 3.14524 3 8 6 0 55.8565 3.63350 5 -8 6 0 56.6881 2.55720 4 8 6 0 54.4619 3.36352 3 8 6 0 61.4809 3.35777 2 -9 -6 0 136.821 6.10907 5 -9 -6 0 136.763 5.71656 2 -9 -6 0 134.275 5.69338 3 -9 -6 0 131.199 5.81238 5 -9 -6 0 126.881 12.2451 1 -9 6 0 132.857 5.76048 2 -9 6 0 141.684 5.53093 3 -9 6 0 136.043 4.93592 4 9 6 0 134.956 5.31403 4 -9 6 0 133.290 4.85264 4 9 6 0 129.083 5.79930 5 9 6 0 130.811 6.04337 5 -10 -6 0 50.2348 3.93393 5 -10 -6 0 43.6556 8.66236 1 -10 -6 0 48.1271 3.62089 5 -10 -6 0 54.4015 3.37711 3 -10 -6 0 47.6470 3.44925 2 10 6 0 55.6851 3.69612 5 -10 6 0 51.0667 2.19360 4 10 6 0 59.8108 4.14412 5 -10 6 0 53.2628 2.29627 4 -10 6 0 55.1310 3.13448 3 -10 6 0 40.7546 5.05193 2 -10 6 0 48.4432 3.16366 1 10 6 0 50.6503 2.84704 4 -11 -6 0 259.911 10.4242 2 -11 -6 0 269.341 10.2772 5 11 -6 0 270.412 8.70501 5 11 -6 0 257.921 8.68410 5 -11 -6 0 272.249 9.99849 3 11 6 0 264.506 10.2299 5 -11 6 0 263.663 10.0931 2 -11 6 0 259.045 8.65384 4 11 6 0 267.827 9.37275 4 -11 6 0 264.745 9.66507 3 -11 6 0 229.910 12.4501 1 11 6 0 232.786 10.3359 5 12 -6 0 37.2222 2.24740 5 -12 -6 0 35.2731 3.84236 5 -12 -6 0 35.2730 3.30348 3 12 -6 0 37.6759 1.69717 5 -12 -6 0 39.2247 3.54868 2 -12 6 0 38.6895 3.65684 2 -12 6 0 38.0534 3.12772 3 12 6 0 36.0092 2.61136 4 12 6 0 40.3884 3.88526 5 13 -6 0 45.1047 2.05178 5 -13 -6 0 48.7070 4.47640 5 -13 -6 0 39.6637 3.96694 2 -13 -6 0 45.9057 3.66857 3 13 -6 0 43.0509 1.98398 5 13 6 0 42.7290 4.40872 5 13 6 0 47.8035 2.83173 4 -13 6 0 51.0469 4.10483 2 -13 6 0 50.1071 3.52464 3 14 -6 0 9.23689 1.27024 5 -14 -6 0 6.74976 2.26753 2 -14 -6 0 5.60881 1.86401 3 14 -6 0 11.0146 1.19126 5 -14 6 0 7.60548 1.81733 3 -14 6 0 3.74833 2.06889 2 14 6 0 11.8129 2.84424 5 0 -7 0 0.37375 0.51682 5 0 -7 0 -0.1802 0.76159 2 0 -7 0 -0.6246 1.81885 1 0 -7 0 0.56134 0.49786 5 0 -7 0 2.96005 1.91337 1 0 7 0 0.07803 0.50436 5 0 7 0 0.36131 0.87992 3 0 7 0 0.20404 0.77492 4 0 7 0 0.47258 0.81802 2 0 7 0 0.82945 0.56813 5 -1 -7 0 504.571 17.1573 2 1 -7 0 523.148 18.4778 1 -1 -7 0 496.420 16.9826 5 -1 -7 0 509.402 19.5895 1 1 -7 0 519.484 18.5083 1 1 -7 0 510.847 17.1855 2 -1 -7 0 521.459 16.9891 5 1 -7 0 515.734 16.7918 5 1 -7 0 483.387 16.7752 5 -1 -7 0 502.660 19.4592 1 -1 7 0 488.668 17.1516 4 -1 7 0 497.705 17.1544 2 -1 7 0 518.267 16.7946 5 1 7 0 525.867 17.1601 2 -1 7 0 506.035 16.7781 5 1 7 0 498.393 16.9696 5 -1 7 0 503.035 17.2903 3 1 7 0 489.887 17.1795 4 1 7 0 500.403 17.3026 3 1 7 0 504.182 16.9705 5 -2 -7 0 2.74501 2.52060 1 -2 -7 0 1.50950 2.48382 1 -2 -7 0 0.86693 0.76971 2 2 -7 0 -0.0583 0.33423 5 2 -7 0 3.21011 1.38398 1 -2 -7 0 0.76239 0.67368 5 -2 -7 0 0.60322 0.65208 5 2 -7 0 0.12386 0.34640 5 2 -7 0 0.69919 0.83052 2 -2 -7 0 0.11883 0.88998 3 2 7 0 -0.2131 0.85008 4 -2 7 0 0.32727 0.36380 5 2 7 0 -0.4764 0.61740 5 -2 7 0 -0.3066 0.81609 2 2 7 0 3.30129 0.74097 5 2 7 0 -1.6869 0.94563 3 -2 7 0 -0.2393 0.95834 3 -2 7 0 0.20415 0.76807 4 -2 7 0 -0.0899 0.38542 5 2 7 0 0.92488 0.86539 2 -3 -7 0 537.580 21.4979 1 -3 -7 0 533.235 18.3002 3 -3 -7 0 532.709 21.3883 1 -3 -7 0 528.971 18.0577 5 -3 -7 0 538.454 18.1015 2 -3 -7 0 511.344 18.0575 5 3 7 0 545.235 18.0835 2 3 7 0 535.211 18.1576 4 3 7 0 548.392 18.2789 3 -3 7 0 544.621 18.1639 2 -3 7 0 510.943 18.0243 4 3 7 0 546.544 18.0815 5 -3 7 0 528.962 18.2305 3 3 7 0 530.304 18.0616 5 -4 -7 0 5.72111 1.19535 3 -4 -7 0 8.71326 1.18277 2 -4 -7 0 8.68696 1.15981 5 -4 -7 0 3.33318 3.60948 1 -4 -7 0 8.06682 3.62458 1 -4 7 0 7.45770 1.01881 4 4 7 0 8.26824 1.13230 5 4 7 0 7.87313 1.16024 5 -4 7 0 6.81349 1.17501 2 4 7 0 6.56758 1.30556 3 4 7 0 10.2137 1.31585 4 -4 7 0 7.14158 1.06360 4 4 7 0 5.71689 1.04556 2 -4 7 0 6.88589 1.23442 3 -5 -7 0 66.3134 3.45609 3 -5 -7 0 72.9898 8.19217 1 -5 -7 0 66.8379 3.29487 5 -5 -7 0 65.8649 7.87773 1 -5 -7 0 63.6048 3.22685 2 -5 -7 0 63.6149 3.25766 5 5 7 0 61.7991 3.22206 4 -5 7 0 64.1315 2.99228 4 -5 7 0 66.8171 3.08906 4 5 7 0 65.5097 3.49752 3 5 7 0 69.4368 3.38227 5 5 7 0 66.8427 3.28388 5 -5 7 0 66.5741 3.41543 3 5 7 0 68.1654 3.25841 2 -5 7 0 62.4591 3.42066 2 -6 -7 0 78.3648 9.37198 1 -6 -7 0 91.6762 9.51689 1 -6 -7 0 91.0961 4.11686 2 -6 -7 0 92.5153 4.33442 3 -6 -7 0 90.1162 4.19236 5 -6 -7 0 90.3172 4.22807 5 6 7 0 93.8296 4.14647 2 -6 7 0 89.2736 4.30047 2 -6 7 0 87.1941 3.73582 4 -6 7 0 88.0774 3.79908 4 6 7 0 93.2328 4.31439 5 6 7 0 90.4929 4.21053 5 6 7 0 92.6899 4.08713 4 6 7 0 93.6790 4.41322 3 -6 7 0 88.6294 4.12052 3 -6 7 0 92.1140 4.27232 3 -7 -7 0 -1.0294 1.21986 5 -7 -7 0 0.21106 1.07842 2 -7 -7 0 2.42222 5.05452 1 -7 -7 0 0.84808 1.24028 3 -7 -7 0 1.90684 1.14950 5 -7 7 0 0.41124 0.77384 4 -7 7 0 1.15209 1.16201 3 -7 7 0 -1.2263 0.88217 4 7 7 0 -0.7434 1.24931 5 7 7 0 0.43967 0.98840 4 7 7 0 0.14730 1.31796 5 7 7 0 0.17663 1.15545 2 -7 7 0 1.43813 1.27790 3 -8 -7 0 8.86161 1.56990 5 -8 -7 0 9.48988 1.65566 3 -8 -7 0 6.15579 1.45404 2 -8 -7 0 8.80962 1.59389 5 -8 -7 0 10.9149 6.12376 1 8 7 0 8.46975 2.58865 2 8 7 0 11.8978 1.50746 4 8 7 0 9.99390 1.84522 5 8 7 0 7.21243 1.51777 5 -8 7 0 7.02658 1.46137 3 -8 7 0 7.33539 1.76635 3 -8 7 0 9.13047 1.05819 4 -8 7 0 10.4677 1.22225 4 -9 -7 0 5.33981 1.53481 3 -9 -7 0 2.97392 1.41789 5 -9 -7 0 6.57925 7.50612 1 -9 -7 0 2.59868 1.60008 5 -9 -7 0 0.52991 1.30638 2 9 7 0 2.81530 1.44359 5 -9 7 0 2.42834 1.24144 3 -9 7 0 2.98199 1.03693 4 9 7 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106.449 4.40838 2 0 -8 0 115.834 6.84333 1 0 -8 0 106.239 3.99999 5 0 -8 0 99.1256 6.63398 1 0 -8 0 105.650 3.98997 5 0 8 0 102.058 4.43102 2 0 8 0 102.508 4.45164 4 0 8 0 104.300 4.67588 3 0 8 0 103.921 3.99276 5 0 8 0 107.467 4.02238 5 -1 -8 0 60.4959 2.72236 5 1 -8 0 53.7738 5.85125 1 1 -8 0 62.9086 3.09369 2 1 -8 0 58.6470 4.79424 1 -1 -8 0 62.6550 2.75567 5 -1 -8 0 66.6727 6.15814 1 1 -8 0 62.9796 2.46593 5 -1 -8 0 63.5216 3.07822 2 -1 -8 0 64.7965 6.02504 1 1 -8 0 59.3119 2.46511 5 1 8 0 64.1609 3.18714 2 -1 8 0 61.1190 2.49701 5 -1 8 0 58.7923 2.47992 5 1 8 0 63.7800 3.19642 4 1 8 0 58.1542 2.76230 5 -1 8 0 56.8350 3.03119 4 1 8 0 61.6299 2.73617 5 -1 8 0 60.5019 3.35691 3 1 8 0 55.1651 3.36472 3 -1 8 0 59.4150 3.14435 2 2 -8 0 3.51562 0.45423 5 -2 -8 0 1.72992 0.93995 2 -2 -8 0 3.01999 0.85107 5 -2 -8 0 1.06438 3.12059 1 2 -8 0 2.07756 1.48288 1 -2 -8 0 3.89929 3.25310 1 2 -8 0 2.83810 0.47216 5 2 -8 0 1.75337 0.91260 2 -2 -8 0 3.15231 0.81540 5 2 -8 0 2.65578 1.60912 1 2 8 0 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8 0 10.2506 2.68414 3 -10 -8 0 4.71510 1.67979 3 -10 -8 0 4.97845 1.55709 2 -10 -8 0 2.02266 1.66620 5 -10 8 0 1.81274 0.97027 4 -10 8 0 5.56922 1.62448 3 10 8 0 1.90586 1.43252 4 -10 8 0 3.77988 1.61184 2 10 8 0 2.97809 1.89927 5 -11 -8 0 33.1486 3.58402 3 -11 -8 0 28.7678 3.45417 2 -11 -8 0 28.4987 3.05607 5 -11 8 0 31.0695 3.53140 2 -11 8 0 24.4019 3.19071 3 11 8 0 34.0574 4.59645 5 11 8 0 30.6854 3.01140 4 -12 -8 0 29.1736 3.84344 3 -12 -8 0 27.3418 3.72924 2 -12 -8 0 24.6731 3.06702 5 -12 8 0 24.8263 3.37814 3 -12 8 0 27.9781 2.98840 2 12 8 0 27.2064 3.07377 4 -13 -8 0 3.98961 2.59418 5 -13 -8 0 1.84015 2.04570 2 -13 -8 0 5.12987 2.20693 3 13 8 0 3.46899 1.92907 4 -13 8 0 4.39618 2.22519 2 -13 8 0 5.36617 2.07286 3 0 -9 0 3.90870 2.84524 1 0 -9 0 0.63685 1.01574 2 0 -9 0 0.19093 0.63267 5 0 -9 0 -0.3886 0.64558 5 0 9 0 -1.5045 1.01331 4 0 9 0 -0.9515 1.09787 2 1 -9 0 131.786 7.27847 1 -1 -9 0 131.855 5.15560 5 -1 -9 0 135.799 5.13000 5 -1 -9 0 133.335 5.52117 2 1 -9 0 139.074 4.84701 5 -1 -9 0 143.284 8.90830 1 1 -9 0 136.754 5.55711 2 1 -9 0 137.129 4.86653 5 1 9 0 139.430 5.19159 5 -1 9 0 127.919 5.61621 2 -1 9 0 137.048 5.61212 4 -1 9 0 135.970 4.87922 5 1 9 0 131.068 5.56997 2 1 9 0 130.093 5.60071 4 -2 -9 0 42.7024 2.41460 5 2 -9 0 39.6298 1.61420 5 -2 -9 0 41.9719 2.75777 2 -2 -9 0 39.9866 2.41937 5 2 -9 0 40.5133 3.92133 1 2 -9 0 39.7986 3.27849 1 2 -9 0 39.8862 1.58987 5 -2 9 0 40.5284 1.68123 5 2 9 0 39.4019 2.90413 2 2 9 0 39.5498 2.48401 5 2 9 0 38.1083 2.87500 4 -2 9 0 40.7883 2.80800 4 -2 9 0 36.9663 3.04827 2 -3 -9 0 97.6787 4.33658 5 -3 -9 0 102.989 4.52459 2 -3 -9 0 102.726 4.34574 5 -3 9 0 92.0169 5.60104 2 3 9 0 106.117 4.70609 4 -3 9 0 98.7833 4.50956 4 3 9 0 103.619 4.37866 5 3 9 0 95.0455 4.58513 2 -4 -9 0 51.7853 3.73355 3 -4 -9 0 56.8635 3.10424 5 -4 -9 0 53.2275 3.16217 2 -4 -9 0 50.1162 3.13445 5 4 9 0 46.4650 3.38681 2 -4 9 0 55.0429 3.11283 4 4 9 0 52.4083 3.41932 4 4 9 0 52.3536 3.15813 5 -5 -9 0 58.2757 3.23335 5 -5 -9 0 45.9308 4.67970 2 -5 -9 0 49.4778 4.01979 3 5 9 0 52.1211 3.22611 5 -5 9 0 50.5651 3.04045 4 5 9 0 41.2362 4.58469 4 -6 -9 0 20.7830 2.31566 3 -6 -9 0 26.3512 2.70414 2 -6 -9 0 21.3126 2.63648 5 6 9 0 21.5990 2.71791 5 6 9 0 25.7581 2.76728 4 -6 9 0 22.4086 2.33610 4 -7 -9 0 1.05867 1.50774 3 -7 -9 0 -0.5084 1.27716 5 -7 -9 0 -0.9449 1.30248 2 7 9 0 0.55638 1.30921 4 -7 9 0 -1.1663 1.05128 4 7 9 0 1.33621 1.50792 5 -7 9 0 1.71623 1.55996 3 -8 -9 0 116.861 5.54893 5 -8 -9 0 115.113 5.81283 2 -8 -9 0 114.135 5.56096 3 -8 9 0 112.456 5.36926 3 -8 9 0 106.698 4.71085 4 8 9 0 104.756 5.17365 4 -9 -9 0 98.5852 5.12095 2 -9 -9 0 100.318 5.35875 5 -9 -9 0 100.950 5.35129 3 -9 9 0 101.069 5.27067 2 -9 9 0 100.809 5.07409 3 9 9 0 96.8325 4.91597 4 -9 9 0 98.6056 4.33345 4 -10 -9 0 47.0356 4.25595 5 -10 -9 0 55.2779 4.18200 3 -10 -9 0 49.9246 3.99838 2 -10 9 0 45.4111 2.87285 4 -10 9 0 43.6733 3.96205 2 10 9 0 54.6866 3.72343 4 -10 9 0 45.3402 3.87575 3 -11 -9 0 0.30375 2.01434 3 -11 -9 0 2.24659 2.00841 5 -11 -9 0 2.96764 1.92548 2 -11 9 0 1.94644 1.75236 3 11 9 0 1.42780 1.71925 4 -11 9 0 3.27525 1.98863 2 -12 -9 0 30.3323 3.26397 3 0 -10 0 593.873 19.7161 5 0 -10 0 588.911 19.7415 5 0 -10 0 594.159 20.3179 2 0 10 0 580.799 19.7474 5 0 10 0 588.686 20.3816 4 1 -10 0 4.07546 1.33492 2 -1 -10 0 5.25614 1.04635 5 1 -10 0 5.75667 0.90020 5 -1 -10 0 6.43341 1.04553 5 1 -10 0 5.86775 0.71294 5 1 -10 0 4.99186 3.01467 1 -1 -10 0 6.94620 1.39148 2 1 10 0 6.45957 1.62402 4 -1 10 0 4.56728 0.88549 5 -1 10 0 4.17704 1.54839 4 1 10 0 9.32474 1.23997 5 -2 -10 0 6.92221 1.20092 5 -2 -10 0 6.77519 1.14712 5 -2 -10 0 4.87915 1.43188 2 2 10 0 7.95786 1.68896 4 -2 10 0 6.23055 1.59864 4 -3 -10 0 31.4009 2.78363 2 -3 -10 0 27.4629 2.39378 5 -3 -10 0 28.3524 2.42863 5 -3 10 0 26.9486 2.88916 4 3 10 0 29.2081 2.99438 4 3 10 0 24.2950 2.63432 5 -4 -10 0 18.0186 2.28458 5 -4 -10 0 16.8884 1.81461 5 -4 -10 0 16.0062 1.87625 2 -4 10 0 16.3371 2.08073 4 4 10 0 13.3525 2.00973 5 4 10 0 14.5478 1.91060 4 -5 -10 0 86.1335 4.59202 2 -5 -10 0 93.2606 4.48275 5 -5 -10 0 96.5336 5.48201 5 -5 10 0 91.4387 4.64107 4 5 10 0 87.1855 4.66554 4 -6 -10 0 11.7178 1.69868 5 -6 -10 0 18.5897 2.35800 3 -6 -10 0 16.4386 3.32567 2 6 10 0 13.3470 1.90501 4 -6 10 0 20.5018 2.29051 3 -6 10 0 14.4749 1.89733 4 -7 -10 0 21.8868 2.97608 5 -7 -10 0 15.3741 2.22607 3 -7 -10 0 19.3907 2.20177 2 7 10 0 22.9459 3.01697 4 -7 10 0 24.7147 2.93930 4 -7 10 0 19.7159 2.30875 3 -8 -10 0 15.0298 2.18062 2 -8 -10 0 12.4406 2.12965 3 -8 -10 0 16.1014 2.07949 5 8 10 0 11.4973 1.89991 4 -8 10 0 13.6686 2.04105 4 -8 10 0 12.6800 2.10136 3 -9 -10 0 9.47556 2.05944 2 -9 -10 0 7.05559 2.20890 5 -9 -10 0 9.35540 2.29711 3 -9 10 0 12.8888 2.16567 3 -9 10 0 8.05239 2.70235 4 9 10 0 12.0722 2.02670 4 -9 10 0 6.73620 1.94013 2 -10 -10 0 2.62934 1.99217 2 -10 -10 0 1.39485 2.14781 5 -10 -10 0 2.15422 2.05574 3 -10 10 0 1.62228 1.94347 3 10 10 0 5.88312 1.96147 4 -10 10 0 2.03391 2.01358 2 0 -11 0 1.80965 0.83105 5 0 -11 0 2.01254 1.88838 2 0 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43.4606 2.83059 2 -10 5 -9 45.8137 3.41822 3 -10 5 -9 45.7007 3.54773 2 10 5 9 44.6158 2.86935 4 10 5 9 41.7170 4.60459 5 10 5 9 48.7866 3.58923 5 10 5 9 48.0502 2.57571 4 -10 5 -9 42.6188 2.91345 5 -11 -5 -9 7.25084 1.48437 2 11 -5 9 6.58328 1.27546 5 11 -5 9 7.53540 1.37544 5 -11 -5 -9 6.31182 1.83660 5 -11 -5 -9 8.57258 1.84979 3 -11 5 -9 6.17992 1.63707 3 11 5 9 9.98067 1.20634 4 11 5 9 6.25607 1.83935 5 -11 5 -9 8.51081 1.87506 2 12 -5 9 40.1390 2.82701 5 -12 -5 -9 39.2170 4.23819 5 -12 -5 -9 40.6754 3.72309 3 12 5 9 37.0084 4.26631 5 12 5 9 38.8403 2.97752 4 -12 5 -9 38.2274 3.87829 2 -12 5 -9 34.8539 3.53849 3 13 -5 9 5.81701 1.45464 5 -13 -5 -9 6.41996 2.01670 3 -13 -5 -9 3.67752 1.78917 2 -13 5 -9 4.62507 2.01577 3 -13 5 -9 3.28370 2.16440 2 -14 -5 -9 32.6007 4.32197 3 -14 -5 -9 37.6527 4.07021 2 14 -5 9 32.0794 3.18422 5 14 5 9 32.4186 3.78442 5 -14 5 -9 28.9831 3.39734 2 -14 5 -9 30.5805 4.13949 3 -14 -6 9 18.4354 3.00496 2 -14 6 9 22.3790 2.71294 2 14 6 -9 15.3674 1.91931 4 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12.6788 1.48201 4 2 4 10 11.4921 1.44410 3 -3 -4 -10 73.2045 3.34951 5 -3 -4 -10 71.0363 6.80536 1 -3 -4 -10 75.2183 2.61190 2 3 -4 10 78.8768 3.34224 5 3 -4 10 75.8058 3.44241 2 -3 -4 -10 77.7036 3.36742 5 3 -4 10 75.9661 3.11819 4 -3 -4 -10 74.2572 3.43832 3 3 -4 10 76.5377 6.39764 1 3 4 10 73.5723 6.51129 1 3 4 10 78.1225 3.42472 3 3 4 10 77.9875 3.29915 4 3 4 10 74.0703 3.32521 5 -3 4 -10 75.6407 3.11786 4 -3 4 -10 76.3632 3.46624 2 -3 4 -10 76.8692 3.36675 5 3 4 10 78.3556 3.39626 5 -3 4 -10 75.7005 3.30431 5 -3 4 -10 75.7326 3.43764 3 -3 4 -10 74.3739 6.93392 1 4 -4 10 27.3480 4.02114 1 -4 -4 -10 31.4103 2.22352 3 -4 -4 -10 27.9293 4.55942 1 4 -4 10 21.8223 1.74241 5 4 -4 10 27.4145 1.93911 4 4 -4 10 30.8459 2.00329 5 -4 -4 -10 32.4520 2.12344 5 -4 -4 -10 31.3442 2.12673 5 4 4 10 24.8908 4.18419 1 -4 4 -10 31.0427 1.99178 5 4 4 10 31.5744 1.97404 4 4 4 10 31.3296 2.17815 5 -4 4 -10 33.2479 2.23281 2 -4 4 -10 31.3403 2.06928 5 -4 4 -10 34.8230 5.89490 1 4 4 10 29.5375 2.21157 3 -4 4 -10 30.5374 2.16795 3 4 4 10 30.1207 2.08459 5 -4 4 -10 30.2237 1.73013 4 -5 -4 -10 183.167 6.24281 2 5 -4 10 177.686 6.66117 5 5 -4 10 177.864 6.67005 5 -5 -4 -10 178.877 6.85084 5 -5 -4 -10 177.149 6.84158 5 -5 -4 -10 167.017 11.1512 1 -5 -4 -10 177.451 6.83406 3 5 -4 10 182.141 10.3508 1 5 -4 10 184.557 6.41214 4 5 4 10 179.794 6.87940 5 -5 4 -10 174.964 6.64758 5 5 4 10 184.590 6.58403 4 -5 4 -10 185.356 10.5473 1 5 4 10 192.372 11.0918 1 -5 4 -10 179.465 6.69452 5 -5 4 -10 185.204 6.37426 4 -5 4 -10 173.427 6.81062 2 -5 4 -10 179.113 6.84939 3 5 4 10 178.393 6.83758 5 5 4 10 181.903 6.85215 3 -6 -4 -10 66.2956 3.56281 5 6 -4 10 68.9890 2.78103 4 -6 -4 -10 66.9489 3.55298 3 -6 -4 -10 66.5439 3.52555 5 6 -4 10 67.1949 3.22301 5 -6 -4 -10 67.2137 2.80076 2 6 -4 10 70.4430 3.23669 5 6 -4 10 73.5490 7.07711 1 -6 -4 -10 57.2210 8.21012 1 -6 4 -10 69.6359 3.22530 5 6 4 10 67.9512 3.55262 3 6 4 10 66.5734 3.47937 5 6 4 10 75.0256 3.63288 5 -6 4 -10 68.1034 3.30078 5 -6 4 -10 64.6805 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108.496 4.45130 2 7 6 -10 104.582 5.17054 5 7 6 -10 107.015 4.62426 3 -7 6 10 109.522 4.62369 2 -6 -6 10 15.4417 5.28528 1 -6 -6 10 22.6136 2.39237 5 -6 -6 10 11.3569 2.40738 4 -6 -6 10 22.8571 2.50059 2 -6 -6 10 24.7897 2.53639 5 6 6 -10 25.0128 2.26660 3 6 6 -10 20.0107 2.64291 5 6 6 -10 26.0538 2.47461 5 6 6 -10 17.9900 2.16641 4 -6 6 10 23.1915 2.27045 4 -6 6 10 21.2930 1.76839 2 -6 6 10 22.6493 1.80854 3 -6 6 10 17.9855 1.94139 2 6 6 -10 17.2473 5.84242 1 -5 -6 10 146.137 6.19088 5 -5 -6 10 158.642 11.6506 1 -5 -6 10 147.218 6.09820 4 -5 -6 10 155.576 6.29406 5 -5 -6 10 156.523 6.32467 2 5 6 -10 147.921 11.9697 1 5 6 -10 159.515 6.30884 5 -5 6 10 155.486 5.77387 3 -5 6 10 155.457 5.74172 2 -5 6 10 154.506 5.67704 2 5 6 -10 157.291 6.02843 3 5 6 -10 155.893 6.10519 4 5 6 -10 150.424 6.32715 2 5 6 -10 159.550 6.35148 5 -5 6 10 159.839 6.05847 4 -4 -6 10 282.052 10.2014 4 -4 -6 10 278.854 10.3745 2 4 -6 -10 288.684 10.5632 1 -4 -6 10 279.358 14.9994 1 4 -6 -10 288.901 9.45758 5 -4 -6 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1.17195 4 -3 5 14 1.84774 0.82410 3 3 5 -14 1.19141 1.09694 4 3 5 -14 2.57926 1.04346 3 -3 5 14 2.21938 0.75780 5 3 5 -14 0.69344 1.19963 5 -3 5 14 0.05167 2.99936 1 3 5 -14 0.32052 4.68938 1 3 5 -14 1.50028 0.88778 3 3 5 -14 1.71242 1.13763 2 -3 5 14 1.51977 0.82156 5 -2 -5 14 46.3837 2.83873 5 -2 -5 14 42.6676 2.74389 4 2 -5 -14 44.1063 2.43296 3 2 -5 -14 44.4666 2.32127 5 2 -5 -14 41.4803 2.74619 4 -2 -5 14 44.0561 2.94194 5 2 -5 -14 31.8707 4.38771 1 -2 -5 14 46.7154 7.75370 1 -2 -5 14 42.9743 2.84162 2 2 -5 -14 42.7682 2.37153 5 2 5 -14 47.7700 3.09334 5 2 5 -14 44.9993 2.88741 5 -2 5 14 43.2301 2.41446 3 2 5 -14 45.3006 2.57619 3 -2 5 14 43.2885 2.32938 5 2 5 -14 41.5542 2.94453 2 2 5 -14 40.7631 2.73011 3 -2 5 14 45.4515 2.73286 4 -2 5 14 42.3861 2.34032 5 2 5 -14 42.1984 2.68628 4 -2 5 14 49.7140 6.21097 1 2 5 -14 34.8136 6.06350 1 -1 -5 14 117.880 4.95344 4 -1 -5 14 123.048 5.12220 5 1 -5 -14 121.900 8.63006 1 1 -5 -14 119.857 4.74971 5 -1 -5 14 120.604 5.10660 2 -1 -5 14 120.770 10.0335 1 1 -5 -14 118.284 4.99450 4 1 -5 -14 120.589 4.82036 3 -1 -5 14 120.292 5.07968 5 1 5 -14 123.859 10.5981 1 -1 5 14 122.262 5.05625 4 -1 5 14 119.654 8.40311 1 1 5 -14 122.151 4.94323 4 -1 5 14 123.322 4.80285 3 1 5 -14 123.202 5.22506 5 1 5 -14 118.506 5.15427 2 -1 5 14 121.297 4.72955 5 1 5 -14 117.826 4.89156 3 -1 5 14 115.188 4.77727 5 0 -5 14 132.238 5.45497 5 0 -5 -14 133.115 5.21848 5 0 -5 -14 134.177 9.20308 1 0 -5 14 125.276 10.0457 1 0 -5 14 129.487 5.45853 5 0 -5 -14 128.813 5.20756 5 0 -5 14 136.829 5.33882 4 0 -5 -14 129.978 5.43129 4 0 -5 14 130.655 5.49455 2 0 -5 -14 135.186 5.30566 3 0 5 14 130.679 5.25805 5 0 5 14 133.509 5.40939 4 0 5 14 139.002 5.21865 5 0 5 14 130.698 9.10085 1 0 5 -14 135.333 5.50711 5 0 5 -14 138.301 5.57848 5 0 5 -14 135.712 5.32439 4 0 5 -14 137.324 10.6377 1 0 5 -14 126.810 5.48202 2 0 5 14 130.225 5.26206 3 0 5 -14 132.931 5.36616 3 1 -5 14 274.240 10.0843 2 -1 -5 -14 277.031 9.96910 3 -1 -5 -14 282.274 9.93497 5 -1 -5 -14 277.517 10.0313 4 -1 -5 -14 273.727 13.8553 1 -1 -5 -14 273.565 9.87409 5 1 -5 14 277.029 10.0550 5 1 -5 14 279.189 9.88931 4 1 -5 14 277.924 14.8303 1 1 -5 14 274.644 10.0580 5 1 5 14 277.907 9.88507 5 -1 5 -14 279.454 10.1212 2 1 5 14 260.077 13.8450 1 1 5 14 282.501 9.93090 3 -1 5 -14 273.540 10.0010 3 -1 5 -14 274.103 10.0488 5 -1 5 -14 282.040 10.1157 5 1 5 14 274.721 9.98781 4 -1 5 -14 281.750 9.88619 4 1 5 14 272.220 9.91168 5 -1 5 -14 283.854 15.2539 1 -2 -5 -14 13.4222 1.89067 5 2 -5 14 10.8959 1.52695 2 2 -5 14 9.07951 4.47758 1 2 -5 14 10.0974 1.28690 4 2 -5 14 14.1750 1.57421 5 2 -5 14 9.52444 1.34833 5 -2 -5 -14 14.2546 1.60640 3 -2 5 -14 10.3070 1.31451 5 -2 5 -14 13.7701 1.66852 5 2 5 14 16.9927 2.21091 4 2 5 14 13.8883 1.56186 3 -2 5 -14 6.74984 4.65751 1 -2 5 -14 13.5754 1.40861 4 2 5 14 9.88189 1.33557 5 2 5 14 9.96676 1.25773 5 -2 5 -14 14.1213 1.58154 3 -2 5 -14 13.5748 1.71363 2 2 5 14 15.7755 4.47951 1 3 -5 14 260.379 9.51886 2 3 -5 14 257.439 9.19828 4 -3 -5 -14 259.277 9.45457 5 3 -5 14 258.275 9.43981 5 -3 -5 -14 253.871 9.40722 5 -3 -5 -14 261.037 9.51225 3 -3 -5 -14 256.087 14.8221 1 3 -5 14 265.063 14.4685 1 3 -5 14 258.118 9.44590 5 -3 5 -14 258.951 9.51368 3 3 5 14 258.160 9.39878 5 3 5 14 248.447 9.35126 4 -3 5 -14 258.324 9.42758 5 -3 5 -14 254.786 14.6177 1 -3 5 -14 259.360 9.17401 4 3 5 14 257.473 14.4355 1 -3 5 -14 258.687 9.50346 5 3 5 14 249.230 9.43459 5 3 5 14 257.424 9.46143 3 -3 5 -14 247.026 9.52440 2 -4 -5 -14 4.57332 1.39664 3 -4 -5 -14 5.30999 1.31952 5 4 -5 14 1.28343 4.95165 1 4 -5 14 6.55839 1.13363 4 -4 -5 -14 5.80840 1.34502 5 4 -5 14 3.94062 1.19237 5 4 5 14 5.32695 1.31898 5 4 5 14 1.72484 4.58172 1 -4 5 -14 3.82573 0.97687 4 -4 5 -14 -0.9088 5.09191 1 -4 5 -14 8.39842 1.50577 3 4 5 14 3.31931 1.24277 4 -4 5 -14 3.27665 1.16722 5 4 5 14 6.69306 1.42872 5 5 -5 14 28.4276 2.21372 4 5 -5 14 31.1926 2.52090 5 -5 -5 -14 30.8644 2.91890 5 -5 -5 -14 27.3876 2.71807 3 -5 -5 -14 31.1869 2.70110 5 -5 5 -14 28.1536 2.73905 3 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14.3353 1.96354 3 8 5 14 16.7796 2.05044 5 8 5 14 21.7968 2.93935 4 -8 5 -14 19.4982 2.09556 5 9 -5 14 20.1449 2.53641 5 -9 -5 -14 12.0218 2.11742 5 -9 -5 -14 16.6803 1.85818 2 -9 -5 -14 16.0982 2.19195 3 -9 5 -14 17.7509 2.19218 3 9 5 14 14.5054 2.13025 5 -9 5 -14 18.7482 1.46388 4 -10 -5 -14 8.54102 2.05619 3 -10 -5 -14 6.11486 2.95305 5 10 -5 14 9.88109 1.73336 5 -10 -5 -14 7.26162 1.27898 2 10 5 14 8.21011 2.10695 5 -10 5 -14 6.87556 2.04609 2 -10 5 -14 8.31726 2.09919 3 10 5 14 8.17352 1.46228 4 -11 -5 -14 59.6107 4.53824 3 -11 -5 -14 59.2367 4.79195 5 11 -5 14 51.8968 3.70407 5 11 5 14 51.1064 4.88965 5 -11 5 -14 52.2651 4.45642 2 -11 5 -14 47.4413 4.33981 3 12 -5 14 2.47365 1.66571 5 -12 -5 -14 4.28496 2.45008 3 -12 -5 -14 3.15099 2.70121 5 -12 5 -14 4.30335 2.15542 3 -12 5 -14 -0.4475 1.99208 2 -13 -6 14 23.7180 2.96579 2 13 6 -14 29.4808 3.47212 4 13 6 -14 25.5091 3.12373 5 -13 6 14 28.3435 2.74876 2 -12 -6 14 19.2916 2.68227 2 -12 -6 14 13.5770 2.85904 5 12 6 -14 14.4701 2.70089 5 -12 6 14 17.6898 2.23237 2 12 6 -14 19.6136 2.22667 4 -11 -6 14 26.6793 3.24252 5 -11 -6 14 27.0151 3.67510 2 -11 6 14 27.9647 3.08759 2 11 6 -14 26.4291 3.12102 5 11 6 -14 26.5922 3.01059 4 -10 -6 14 11.2874 2.22971 5 -10 -6 14 9.55595 2.03597 2 -10 6 14 10.1397 1.61322 2 10 6 -14 6.36995 1.61554 4 10 6 -14 13.4008 2.34069 5 -9 -6 14 40.0822 3.79541 5 -9 -6 14 35.7305 3.38422 2 -9 6 14 35.8372 2.69530 2 9 6 -14 31.6564 2.93250 4 9 6 -14 36.0767 3.72804 5 -9 6 14 30.9942 3.03280 2 -8 -6 14 -0.5868 1.46633 5 -8 -6 14 0.07459 1.89950 5 -8 -6 14 9.27474 8.28548 1 8 -6 -14 -0.2084 0.42773 5 -8 -6 14 -0.6354 1.51394 2 -8 6 14 2.36456 2.57881 1 -8 6 14 -0.3415 1.35598 2 8 6 -14 0.83004 1.26467 4 8 6 -14 -0.7747 1.20857 3 -8 6 14 -0.7967 0.65778 3 -8 6 14 -0.9798 0.88409 2 8 6 -14 0.29262 1.45839 5 -8 6 14 0.36337 0.74836 3 8 6 -14 -0.6037 2.00942 5 -7 -6 14 38.1195 3.33760 5 7 -6 -14 41.0029 1.78556 5 -7 -6 14 40.9497 3.68028 5 7 -6 -14 41.0349 1.77199 5 -7 -6 14 16.1881 7.87537 1 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53.6848 4.47346 4 1 2 -28 52.8673 5.39897 5 1 2 -28 54.4041 4.29209 4 1 2 -28 45.6372 3.79409 3 0 -2 -28 -0.1752 2.10518 4 0 -2 -28 0.72028 1.70084 3 0 -2 -28 1.34812 2.07564 5 0 -2 28 5.99908 3.84190 5 0 2 -28 4.68501 2.68324 5 0 2 -28 0.46913 1.81206 4 0 2 -28 2.21111 1.82859 3 -1 -2 -28 4.49138 2.13439 4 -1 -2 -28 5.08979 2.31260 5 -1 -2 -28 6.38337 2.07937 3 1 -2 28 6.88971 2.80629 5 -1 2 -28 7.88932 2.98036 5 -1 2 -28 10.5346 2.22305 4 -1 2 -28 11.1425 2.17262 3 -2 -2 -28 0.75503 1.99940 3 -2 -2 -28 -5.1606 2.04156 5 -2 -2 -28 -0.0291 1.93191 4 2 -2 28 1.87200 2.48138 5 -2 2 -28 -0.4946 1.93792 4 -2 2 -28 -2.1122 1.99498 3 -4 -3 28 -0.1861 1.96537 2 4 -3 -28 -1.0089 2.27455 4 4 -3 -28 0.47665 1.88605 5 4 3 -28 -2.2146 2.10342 4 4 3 -28 -3.0957 2.56165 5 3 -3 -28 -2.1272 2.11713 5 3 -3 -28 0.39457 2.38145 4 -3 -3 28 2.44090 1.81623 2 3 3 -28 0.65249 2.62986 5 3 3 -28 3.32173 2.02896 4 2 -3 -28 9.85363 2.71555 4 -2 -3 28 6.63429 1.89986 2 2 -3 -28 5.76760 2.11874 5 2 3 -28 8.07956 2.20459 4 2 3 -28 8.50600 3.00003 5 -1 -3 28 21.6381 3.59903 5 -1 -3 28 28.9169 3.48360 2 1 -3 -28 27.1237 3.06537 5 1 -3 -28 23.7180 3.09214 4 1 3 -28 27.4923 3.92625 5 1 3 -28 24.9642 3.40433 3 1 3 -28 23.5002 2.72266 4 0 -3 28 40.6456 5.17905 5 0 -3 -28 33.2501 4.29419 4 0 -3 -28 36.1208 3.96107 3 0 -3 -28 31.2333 4.30234 5 0 3 -28 38.7068 3.87682 3 0 3 -28 33.2641 3.98571 4 1 -3 28 36.1322 4.97127 5 -1 -3 -28 35.3972 3.95564 3 -1 -3 -28 36.6201 4.23677 4 -1 -3 -28 30.4875 4.32151 5 -1 3 -28 30.5538 3.95985 3 -1 3 -28 26.1830 2.86317 4 3 0 -29 29.1148 3.20388 4 3 0 -29 37.9011 4.73732 5 2 0 -29 0.29462 2.33780 4 2 0 -29 -3.8918 2.16375 5 1 0 -29 20.1785 3.30510 5 1 0 -29 23.7458 2.94935 4 0 0 -29 -0.5000 2.74570 5 0 0 -29 -1.7560 2.08330 4 0 0 -29 -1.3178 2.07326 3 3 -1 -29 0.87449 2.34566 4 3 -1 -29 -0.3074 2.49473 5 3 1 -29 1.98056 2.34890 4 3 1 -29 2.87821 2.80295 5 2 -1 -29 47.1670 4.87387 5 2 -1 -29 32.6595 4.43670 4 2 1 -29 44.1764 5.28081 5 2 1 -29 42.2142 4.50496 4 1 -1 -29 4.49356 2.45327 5 1 -1 -29 0.75619 2.17125 4 1 1 -29 4.79262 2.33747 4 1 1 -29 6.73203 2.68539 5 0 -1 -29 5.15813 2.39248 4 0 -1 -29 -0.9334 2.55726 5 0 1 -29 2.13249 2.63922 5 0 1 -29 1.28806 2.10578 3 0 1 -29 1.54734 2.11547 4 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7465 _exptl_absorpt_correction_T_min 0.7163 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71102 10.896 8.408 18.996 89.982 95.435 89.983 ) ; _shelx_hkl_checksum 28056 _shelx_res_file ; TITL DMim_BSF_NCyr_12420_0m in P2(1)/n DMim_BSF_NCyr_12420_0m.res created by SHELXL-2018/3 at 10:16:43 on 17-Feb-2020 CELL 0.71073 10.8820 8.4029 18.9678 90.0000 95.4398 90.0000 ZERR 4.00 0.0006 0.0004 0.0011 0.0000 0.0020 0.0000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C H N O S UNIT 64 88 16 12 4 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -123.140 SIZE 0.33 0.42 0.55 L.S. 4 BOND $H ACTA CONF FMAP 2 PLAN 20 WGHT 0.041700 0.661800 EXTI 0.008529 FVAR 0.62845 0.67358 C1 1 0.079954 0.119738 0.125048 11.00000 0.01866 0.02769 = 0.02419 0.00176 -0.00088 -0.00143 AFIX 43 H1 2 0.162507 0.154570 0.136425 11.00000 -1.20000 AFIX 0 C2 1 0.016504 0.021109 0.165502 11.00000 0.02074 0.02625 = 0.02023 0.00296 -0.00240 0.00080 AFIX 43 H2 2 0.045537 -0.025178 0.209661 11.00000 -1.20000 AFIX 0 C3 1 -0.102162 0.088317 0.068762 11.00000 0.01791 0.02079 = 0.01632 0.00188 0.00190 0.00117 C4 1 -0.202277 -0.085606 0.154025 11.00000 0.02184 0.02677 = 0.02438 0.00586 0.00573 -0.00171 AFIX 137 H4A 2 -0.264761 -0.010298 0.167446 11.00000 -1.50000 H4B 2 -0.172925 -0.150361 0.195187 11.00000 -1.50000 H4C 2 -0.238614 -0.154975 0.116071 11.00000 -1.50000 AFIX 0 C5 1 -0.212827 0.096727 0.016703 11.00000 0.02061 0.03256 = 0.02142 0.00570 -0.00246 -0.00067 AFIX 137 H5A 2 -0.194381 0.162346 -0.023687 11.00000 -1.50000 H5B 2 -0.281506 0.144135 0.039231 11.00000 -1.50000 H5C 2 -0.235631 -0.010751 0.000206 11.00000 -1.50000 AFIX 0 C6 1 0.234591 0.401623 -0.007342 11.00000 0.02169 0.02569 = 0.02853 -0.00170 -0.00319 -0.00067 AFIX 43 H6 2 0.285770 0.372447 0.034004 11.00000 -1.20000 AFIX 0 C7 1 0.267158 0.495889 -0.060671 11.00000 0.01759 0.02365 = 0.03375 -0.00327 0.00201 -0.00289 AFIX 43 H7 2 0.345007 0.545291 -0.063695 11.00000 -1.20000 AFIX 0 C8 1 0.073124 0.420206 -0.086400 11.00000 0.01824 0.01968 = 0.01825 -0.00054 0.00319 -0.00186 C9 1 0.158317 0.591906 -0.177069 11.00000 0.03665 0.02627 = 0.02400 0.00202 0.01083 -0.00607 AFIX 137 H9A 2 0.142896 0.516294 -0.216246 11.00000 -1.50000 H9B 2 0.236534 0.647282 -0.181302 11.00000 -1.50000 H9C 2 0.090972 0.669653 -0.178780 11.00000 -1.50000 AFIX 0 C10 1 -0.050840 0.400527 -0.124822 11.00000 0.02087 0.03257 = 0.02370 0.00371 -0.00169 -0.00507 AFIX 137 H10A 2 -0.090249 0.504931 -0.131824 11.00000 -1.50000 H10B 2 -0.101453 0.332570 -0.097120 11.00000 -1.50000 H10C 2 -0.042876 0.351054 -0.170954 11.00000 -1.50000 AFIX 0 C11 1 0.433463 0.003249 0.146182 11.00000 0.01384 0.01512 = 0.01601 0.00043 -0.00092 -0.00132 C12 1 0.360794 -0.067382 0.194048 11.00000 0.01948 0.01855 = 0.01743 0.00119 0.00117 -0.00325 AFIX 43 H12 2 0.326061 -0.004339 0.228696 11.00000 -1.20000 AFIX 0 C13 1 0.339192 -0.230352 0.191014 11.00000 0.02642 0.01954 = 0.02712 0.00642 -0.00353 -0.00655 AFIX 43 H13 2 0.289972 -0.278763 0.223810 11.00000 -1.20000 AFIX 0 C14 1 0.389327 -0.322625 0.140200 11.00000 0.03097 0.01538 = 0.03878 -0.00171 -0.01036 0.00067 AFIX 43 H14 2 0.375570 -0.434269 0.138722 11.00000 -1.20000 AFIX 0 C15 1 0.459510 -0.251567 0.091610 11.00000 0.02539 0.02593 = 0.03198 -0.01082 -0.00364 0.00683 AFIX 43 H15 2 0.492304 -0.314441 0.056220 11.00000 -1.20000 AFIX 0 C16 1 0.482165 -0.088342 0.094447 11.00000 0.01714 0.02706 = 0.02032 -0.00306 0.00173 0.00167 AFIX 43 H16 2 0.530578 -0.039928 0.061247 11.00000 -1.20000 AFIX 0 N1 3 0.005221 0.161293 0.064706 11.00000 0.01852 0.02382 = 0.02083 0.00256 0.00268 -0.00104 PART 2 -21 AFIX 44 H1N 2 0.023777 0.219981 0.032488 -21.00000 -1.20000 AFIX 0 PART 0 N2 3 -0.098693 0.002093 0.129227 11.00000 0.01786 0.02025 = 0.01737 0.00265 0.00166 0.00022 N3 3 0.113142 0.355811 -0.024253 11.00000 0.02064 0.02296 = 0.01993 0.00099 0.00077 -0.00128 PART 1 21 AFIX 44 H3N 2 0.069049 0.293555 0.002078 21.00000 -1.20000 AFIX 0 PART 0 N4 3 0.165110 0.506003 -0.109672 11.00000 0.01992 0.01931 = 0.02190 -0.00109 0.00512 -0.00273 O1 4 0.357339 0.284425 0.175107 11.00000 0.03213 0.01673 = 0.08678 -0.00412 0.02668 -0.00079 O2 4 0.498754 0.262292 0.085162 11.00000 0.05592 0.03115 = 0.02884 0.00878 0.00889 -0.01588 O3 4 0.571296 0.219985 0.207799 11.00000 0.04449 0.02646 = 0.04382 0.00199 -0.02350 -0.01249 S1 5 0.467994 0.209525 0.153920 11.00000 0.01652 0.01532 = 0.02171 0.00194 0.00082 -0.00380 HKLF 4 REM DMim_BSF_NCyr_12420_0m in P2(1)/n REM wR2 = 0.0945, GooF = S = 1.047, Restrained GooF = 1.047 for all data REM R1 = 0.0345 for 5787 Fo > 4sig(Fo) and 0.0406 for all 6612 data REM 225 parameters refined using 0 restraints END WGHT 0.0417 0.6618 REM Highest difference peak 0.403, deepest hole -0.441, 1-sigma level 0.049 Q1 1 0.3743 -0.2671 0.1677 11.00000 0.05 0.40 Q2 1 0.3976 -0.0318 0.1709 11.00000 0.05 0.39 Q3 1 0.4374 -0.2864 0.1237 11.00000 0.05 0.38 Q4 1 0.0547 0.0609 0.1440 11.00000 0.05 0.37 Q5 1 0.4034 0.2736 0.2013 11.00000 0.05 0.36 Q6 1 0.2565 0.4398 -0.0336 11.00000 0.05 0.35 Q7 1 0.1207 0.4589 -0.1002 11.00000 0.05 0.35 Q8 1 0.3491 -0.1483 0.1887 11.00000 0.05 0.35 Q9 1 -0.1038 0.0447 0.1007 11.00000 0.05 0.33 Q10 1 0.4612 -0.0464 0.1229 11.00000 0.05 0.33 Q11 1 0.4637 -0.1619 0.0911 11.00000 0.05 0.32 Q12 1 0.4412 0.0954 0.1475 11.00000 0.05 0.32 Q13 1 0.2136 0.4961 -0.0890 11.00000 0.05 0.32 Q14 1 0.0417 0.1450 0.0948 11.00000 0.05 0.31 Q15 1 -0.0475 0.0108 0.1482 11.00000 0.05 0.30 Q16 1 0.0981 0.3789 -0.0559 11.00000 0.05 0.30 Q17 1 0.5435 0.2265 0.0991 11.00000 0.05 0.29 Q18 1 0.0115 0.4114 -0.1068 11.00000 0.05 0.29 Q19 1 0.1718 0.3787 -0.0153 11.00000 0.05 0.28 Q20 1 0.3604 0.2828 0.1514 11.00000 0.05 0.28 ; _shelx_res_checksum 93947 data_global _journal_date_recd_electronic 2020-03-30 _journal_date_accepted 2020-05-21 _journal_name_full 'IUCrData' _journal_year 2020 _journal_volume 5 _journal_issue 5 _journal_page_first 0 _journal_page_last 0 _journal_paper_category HO _journal_paper_doi 10.1107/S2414314620006896 _journal_coeditor_code BV4031 _publ_contact_author_name 'Arsalan Mirjafari' _publ_contact_author_address ; Department of Chemistry and Physics Florida Gulf Coast University 10501 FGCU Blvd. South Fort Myers, FL 33965 ; _publ_contact_author_email 'amirjafari@fgcu.edu' _publ_contact_author_fax ? _publ_contact_author_phone '239-590-1270' _publ_section_title ; 2,3-Dimethyl-1H-imidazol-3-ium benzenesulfonate--1,2-dimethyl-1H-imidazole co-crystal ; loop_ _publ_author_name _publ_author_footnote _publ_author_address 'Cyr, Noah' . ; Department of Chemistry and Physics Florida Gulf Coast University 10501 FGCU Blvd. South Fort Myers, FL 33965 USA ; 'Zeller, Matthias' . ; Purdue University Department of Chemistry 560 Oval Drive West Lafayette, Indiana USA 47907 USA ; 'Hillesheim, Patrick C.' . ; Ave Maria University Department of Chemistry and Physics 5050 Ave Maria Blvd Ave Maria FL 34142 USA ; 'Mirjafari, Arsalan' . ; Department of Chemistry and Physics Florida Gulf Coast University 10501 FGCU Blvd. South Fort Myers, FL 33965 USA ; _publ_section_synopsis ; The title compound exists with one protonated imidazolium ring, one neutral imidazole ring, and a benzenesulfonate anion in the asymmetric unit. The imidazole rings are held together through hydrogen bonding via a protonated nitrogen on the ring. ;