data_shelx _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H30 Cl2 N4 O7 S U' _chemical_formula_sum 'C36 H30 Cl2 N4 O7 S U' _chemical_formula_weight 971.63 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'U' 'U' -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.248(2) _cell_length_b 15.054(4) _cell_length_c 28.262(8) _cell_angle_alpha 90 _cell_angle_beta 95.583(10) _cell_angle_gamma 90 _cell_volume 3492.5(16) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9802 _cell_measurement_theta_min 2.52 _cell_measurement_theta_max 28.25 _exptl_crystal_description plate _exptl_crystal_colour orange _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.848 _exptl_crystal_F_000 1888 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.26 _exptl_crystal_size_min 0.07 _exptl_absorpt_coefficient_mu 4.916 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.3066 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_process_details 'Sadabs (Sheldrick, 1996)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 82544 _diffrn_reflns_av_unetI/netI 0.0792 _diffrn_reflns_av_R_equivalents 0.0872 _diffrn_reflns_limit_h_min ? _diffrn_reflns_limit_h_max ? _diffrn_reflns_limit_k_min ? _diffrn_reflns_limit_k_max ? _diffrn_reflns_limit_l_min ? _diffrn_reflns_limit_l_max ? _diffrn_reflns_theta_min 2.516 _diffrn_reflns_theta_max 25.297 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 6325 _reflns_number_gt 5366 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. Completness statistics refer to single and composite reflections containing twin component 1 only. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXT (Sheldrick 2015a)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2015b)' _computing_molecular_graphics 'Bruker SHELXTL (Sheldrick 2008)' _computing_publication_material 'Bruker SHELXTL (Sheldrick 2008)' _refine_special_details ; Refined as a 2-component twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0219P)^2^+70.3192P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 6325 _refine_ls_number_parameters 465 _refine_ls_number_restraints 450 _refine_ls_R_factor_all 0.0893 _refine_ls_R_factor_gt 0.0755 _refine_ls_wR_factor_ref 0.1593 _refine_ls_wR_factor_gt 0.1531 _refine_ls_goodness_of_fit_ref 1.147 _refine_ls_restrained_S_all 1.109 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group U1 U 0.22988(5) 0.82324(3) 0.05790(2) 0.02532(15) Uani 1 1 d . . . . . Cl1 Cl -0.6050(3) 0.8462(2) -0.16315(13) 0.0373(8) Uani 1 1 d . . . . . Cl2 Cl 1.1468(3) 0.5625(2) 0.19446(13) 0.0369(8) Uani 1 1 d . . . . . S1 S -0.1570(3) 0.9327(2) 0.02948(11) 0.0258(6) Uani 1 1 d . . . . . O1 O 0.3471(8) 0.9148(5) 0.0425(3) 0.0248(17) Uani 1 1 d . . . . . O2 O 0.1139(9) 0.7310(5) 0.0722(3) 0.0311(19) Uani 1 1 d . . . . . O3 O 0.3531(9) 0.7315(5) 0.0036(3) 0.0262(17) Uani 1 1 d . . . . . O4 O 0.0760(8) 0.8346(5) -0.0189(3) 0.0254(16) Uani 1 1 d . . . . . O5 O 0.2413(8) 0.8773(5) 0.1357(3) 0.0285(17) Uani 1 1 d . . . . . O6 O 0.4660(9) 0.7609(5) 0.1034(3) 0.0277(17) Uani 1 1 d . . . . . O7 O -0.0063(9) 0.9133(5) 0.0640(3) 0.0298(18) Uani 1 1 d . . . . . N1 N 0.3753(10) 0.6334(6) -0.0593(3) 0.026(2) Uani 1 1 d . . . . . N2 N 0.2879(11) 0.6114(7) -0.1035(4) 0.028(2) Uani 1 1 d . . . . . N3 N 0.2117(10) 0.8403(6) 0.2143(4) 0.0260(19) Uani 1 1 d . . . . . N4 N 0.2814(10) 0.7832(7) 0.2500(4) 0.028(2) Uani 1 1 d . . . . . C1 C 0.5202(12) 0.5874(8) -0.0475(4) 0.026(2) Uani 1 1 d . . . . . C2 C 0.6141(13) 0.6017(8) -0.0035(4) 0.029(2) Uani 1 1 d . . . . . H2A H 0.581459 0.644006 0.018618 0.035 Uiso 1 1 calc R U . . . C3 C 0.7547(13) 0.5522(8) 0.0063(5) 0.030(3) Uani 1 1 d . . . . . H3A H 0.819778 0.561202 0.035543 0.036 Uiso 1 1 calc R U . . . C4 C 0.8018(13) 0.4910(8) -0.0250(5) 0.031(3) Uani 1 1 d . . . . . H4A H 0.898985 0.457777 -0.017743 0.037 Uiso 1 1 calc R U . . . C5 C 0.7078(12) 0.4777(9) -0.0672(4) 0.028(2) Uani 1 1 d . U . . . H5A H 0.740190 0.433787 -0.088530 0.034 Uiso 1 1 calc R U . . . C6 C 0.5719(12) 0.5243(7) -0.0793(5) 0.026(2) Uani 1 1 d . . . . . H6A H 0.511139 0.514804 -0.109187 0.032 Uiso 1 1 calc R U . . . C7 C 0.2998(12) 0.6973(7) -0.0364(4) 0.023(2) Uani 1 1 d . . . . . C8 C 0.1498(12) 0.7171(8) -0.0654(4) 0.024(2) Uani 1 1 d . . . . . C9 C 0.1558(13) 0.6616(8) -0.1068(4) 0.029(2) Uani 1 1 d . . . . . C10 C 0.0434(14) 0.6544(8) -0.1512(4) 0.032(3) Uani 1 1 d . . . . . H10A H 0.101636 0.628369 -0.176413 0.047 Uiso 1 1 calc R U . . . H10B H 0.003901 0.713705 -0.160902 0.047 Uiso 1 1 calc R U . . . H10C H -0.049184 0.616545 -0.145373 0.047 Uiso 1 1 calc R U . . . C11 C 0.0437(12) 0.7845(8) -0.0545(4) 0.026(2) Uani 1 1 d . . . . . C12 C -0.1152(12) 0.8000(8) -0.0833(4) 0.026(2) Uani 1 1 d . . . . . C13 C -0.1621(13) 0.8838(8) -0.0966(5) 0.031(3) Uani 1 1 d . . . . . H13A H -0.091777 0.932446 -0.088110 0.037 Uiso 1 1 calc R U . . . C14 C -0.3109(13) 0.8991(8) -0.1222(5) 0.032(3) Uani 1 1 d . . . . . H14A H -0.341040 0.957408 -0.132465 0.038 Uiso 1 1 calc R U . . . C15 C -0.4147(13) 0.8288(9) -0.1328(5) 0.033(3) Uani 1 1 d . . . . . C16 C -0.3706(12) 0.7444(8) -0.1184(4) 0.027(2) Uani 1 1 d . . . . . H16A H -0.443698 0.696464 -0.125577 0.032 Uiso 1 1 calc R U . . . C17 C -0.2212(12) 0.7288(8) -0.0938(4) 0.025(2) Uani 1 1 d . . . . . H17A H -0.190567 0.670300 -0.083997 0.030 Uiso 1 1 calc R U . . . C18 C 0.0688(13) 0.8901(8) 0.2245(5) 0.029(2) Uani 1 1 d . . . . . C19 C -0.0368(14) 0.9231(9) 0.1877(5) 0.035(3) Uani 1 1 d . . . . . H19A H -0.012071 0.918331 0.155678 0.042 Uiso 1 1 calc R U . . . C20 C -0.1803(14) 0.9633(8) 0.1988(5) 0.034(3) Uani 1 1 d . . . . . H20A H -0.254182 0.987061 0.174085 0.040 Uiso 1 1 calc R U . . . C21 C -0.2159(13) 0.9688(8) 0.2455(5) 0.033(3) Uani 1 1 d . . . . . H21A H -0.316687 0.993676 0.252520 0.039 Uiso 1 1 calc R U . . . C22 C -0.1067(13) 0.9386(8) 0.2819(5) 0.031(2) Uani 1 1 d . . . . . H22A H -0.128871 0.945826 0.314063 0.037 Uiso 1 1 calc R U . . . C23 C 0.0385(13) 0.8969(8) 0.2711(5) 0.029(2) Uani 1 1 d . . . . . H23A H 0.113620 0.873893 0.295713 0.035 Uiso 1 1 calc R U . . . C24 C 0.2807(12) 0.8339(8) 0.1728(4) 0.027(2) Uani 1 1 d . . . . . C25 C 0.4086(13) 0.7704(7) 0.1828(4) 0.025(2) Uani 1 1 d . . . . . C26 C 0.3978(13) 0.7440(8) 0.2305(4) 0.027(2) Uani 1 1 d . . . . . C27 C 0.4843(14) 0.6700(9) 0.2588(5) 0.035(3) Uani 1 1 d . . . . . H27A H 0.417409 0.650328 0.283677 0.053 Uiso 1 1 calc R U . . . H27B H 0.589490 0.691541 0.273521 0.053 Uiso 1 1 calc R U . . . H27C H 0.502062 0.620076 0.237685 0.053 Uiso 1 1 calc R U . . . C28 C 0.5086(13) 0.7464(7) 0.1468(4) 0.024(2) Uani 1 1 d . . . . . C29 C 0.6682(12) 0.7019(7) 0.1589(4) 0.023(2) Uani 1 1 d . . . . . C30 C 0.7188(13) 0.6365(8) 0.1290(4) 0.028(2) Uani 1 1 d . . . . . H30A H 0.650535 0.620909 0.101237 0.033 Uiso 1 1 calc R U . . . C31 C 0.8662(12) 0.5937(8) 0.1388(4) 0.029(3) Uani 1 1 d . . . . . H31A H 0.900507 0.548655 0.118475 0.034 Uiso 1 1 calc R U . . . C32 C 0.9627(12) 0.6192(8) 0.1799(4) 0.027(2) Uani 1 1 d . . . . . C33 C 0.9187(13) 0.6861(8) 0.2094(4) 0.029(2) Uani 1 1 d . . . . . H33A H 0.989532 0.704311 0.236134 0.035 Uiso 1 1 calc R U . . . C34 C 0.7699(13) 0.7255(8) 0.1990(4) 0.029(2) Uani 1 1 d . . . . . H34A H 0.735475 0.770004 0.219629 0.034 Uiso 1 1 calc R U . . . C35 C -0.2708(15) 0.8322(9) 0.0265(5) 0.041(3) Uani 1 1 d . . . . . H35A H -0.202257 0.783525 0.016908 0.062 Uiso 1 1 calc R U . . . H35B H -0.366133 0.838573 0.003259 0.062 Uiso 1 1 calc R U . . . H35C H -0.306612 0.819095 0.057862 0.062 Uiso 1 1 calc R U . . . C36 C -0.2838(13) 0.9962(9) 0.0644(4) 0.032(3) Uani 1 1 d . . . . . H36A H -0.231127 1.053220 0.072775 0.048 Uiso 1 1 calc R U . . . H36B H -0.300695 0.963501 0.093477 0.048 Uiso 1 1 calc R U . . . H36C H -0.389106 1.006901 0.046106 0.048 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 U1 0.0091(2) 0.0271(2) 0.0395(3) -0.0005(2) 0.00079(15) 0.00166(19) Cl1 0.0180(13) 0.0289(17) 0.062(2) -0.0028(14) -0.0097(13) 0.0021(12) Cl2 0.0142(13) 0.0328(17) 0.062(2) -0.0021(15) -0.0044(13) 0.0065(12) S1 0.0075(11) 0.0274(16) 0.0425(17) 0.0003(13) 0.0016(11) 0.0005(11) O1 0.009(3) 0.011(4) 0.054(5) 0.003(3) -0.003(3) -0.005(3) O2 0.014(3) 0.016(4) 0.062(6) 0.007(4) -0.002(3) -0.002(3) O3 0.018(4) 0.022(4) 0.039(4) -0.001(3) 0.004(3) 0.006(3) O4 0.013(3) 0.024(4) 0.039(4) -0.002(3) 0.000(3) 0.005(3) O5 0.014(4) 0.034(5) 0.038(4) 0.003(3) 0.004(3) 0.007(3) O6 0.017(4) 0.034(5) 0.032(4) 0.001(3) 0.000(3) 0.002(3) O7 0.015(3) 0.028(4) 0.046(5) -0.006(4) 0.001(3) 0.001(3) N1 0.016(4) 0.025(5) 0.037(5) 0.002(4) 0.003(3) 0.009(3) N2 0.021(4) 0.024(5) 0.040(5) 0.000(4) 0.001(3) 0.000(4) N3 0.017(4) 0.024(5) 0.037(4) 0.002(4) 0.003(3) 0.001(3) N4 0.012(4) 0.036(5) 0.036(5) 0.004(4) -0.001(3) 0.001(4) C1 0.013(4) 0.024(6) 0.042(6) 0.002(4) 0.003(4) 0.003(4) C2 0.017(5) 0.033(7) 0.037(6) 0.001(5) 0.006(4) 0.000(4) C3 0.014(5) 0.033(6) 0.044(6) -0.004(5) 0.004(4) 0.001(4) C4 0.014(5) 0.026(6) 0.051(6) -0.011(5) -0.003(4) -0.006(4) C5 0.013(3) 0.037(4) 0.035(4) 0.000(4) 0.004(3) 0.005(3) C6 0.016(4) 0.017(5) 0.046(6) -0.004(4) 0.003(4) -0.004(4) C7 0.013(4) 0.020(5) 0.035(5) 0.002(4) 0.004(3) 0.004(4) C8 0.012(4) 0.024(5) 0.037(5) 0.003(4) -0.001(4) 0.000(4) C9 0.018(4) 0.029(6) 0.038(5) 0.003(4) 0.000(4) 0.000(4) C10 0.020(5) 0.035(7) 0.038(6) -0.003(5) -0.002(4) 0.010(5) C11 0.010(4) 0.025(5) 0.043(6) 0.000(4) 0.001(4) 0.000(4) C12 0.009(4) 0.029(5) 0.039(6) -0.003(4) 0.002(4) -0.001(3) C13 0.013(5) 0.027(5) 0.052(8) -0.002(5) 0.001(4) -0.003(4) C14 0.017(5) 0.026(5) 0.052(8) 0.004(5) -0.002(5) -0.001(4) C15 0.014(5) 0.034(5) 0.051(8) -0.006(5) -0.002(5) 0.000(4) C16 0.011(4) 0.031(5) 0.039(7) -0.001(5) 0.004(4) -0.005(4) C17 0.013(4) 0.028(5) 0.035(6) 0.002(5) 0.003(4) -0.005(4) C18 0.015(5) 0.026(6) 0.044(5) -0.003(5) 0.002(4) 0.000(4) C19 0.021(5) 0.042(7) 0.041(6) 0.000(6) 0.006(4) 0.013(5) C20 0.026(5) 0.024(6) 0.051(6) 0.003(5) 0.008(5) 0.014(5) C21 0.015(5) 0.032(7) 0.052(6) -0.002(5) 0.011(4) -0.002(5) C22 0.021(5) 0.023(6) 0.050(6) -0.004(5) 0.007(4) -0.004(4) C23 0.018(5) 0.028(6) 0.042(5) -0.004(5) 0.005(4) -0.002(4) C24 0.013(4) 0.027(6) 0.040(5) 0.003(4) 0.002(4) -0.001(4) C25 0.018(5) 0.015(5) 0.041(5) -0.002(4) 0.003(4) -0.001(4) C26 0.014(5) 0.027(6) 0.041(5) 0.002(4) 0.001(4) -0.002(4) C27 0.022(6) 0.044(7) 0.039(7) 0.007(6) -0.001(5) 0.008(5) C28 0.016(4) 0.018(5) 0.036(4) -0.002(4) -0.001(3) -0.005(4) C29 0.011(4) 0.019(5) 0.040(6) 0.005(4) 0.004(3) -0.005(4) C30 0.016(4) 0.028(6) 0.039(6) 0.000(5) 0.001(4) -0.002(4) C31 0.014(4) 0.033(7) 0.038(6) -0.011(5) -0.001(4) -0.001(4) C32 0.010(5) 0.027(6) 0.041(6) -0.003(5) -0.004(4) 0.000(4) C33 0.017(4) 0.031(6) 0.038(6) -0.007(5) -0.004(4) -0.005(4) C34 0.013(4) 0.031(6) 0.042(6) -0.001(5) 0.002(4) -0.002(4) C35 0.024(6) 0.039(7) 0.061(9) -0.007(7) 0.008(6) -0.006(6) C36 0.014(5) 0.038(7) 0.044(7) 0.007(6) 0.005(5) 0.005(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag U1 O2 1.756(7) . ? U1 O1 1.762(7) . ? U1 O5 2.337(8) . ? U1 O3 2.366(8) . ? U1 O7 2.393(7) . ? U1 O4 2.411(8) . ? U1 O6 2.416(7) . ? Cl1 C15 1.734(11) . ? Cl2 C32 1.756(11) . ? S1 O7 1.533(8) . ? S1 C35 1.778(13) . ? S1 C36 1.784(12) . ? O3 C7 1.280(14) . ? O4 C11 1.266(14) . ? O5 C24 1.252(14) . ? O6 C28 1.262(13) . ? N1 C7 1.346(14) . ? N1 C1 1.394(14) . ? N1 N2 1.418(13) . ? N2 C9 1.322(14) . ? N3 C24 1.357(15) . ? N3 N4 1.405(13) . ? N3 C18 1.450(14) . ? N4 C26 1.294(15) . ? C1 C6 1.402(16) . ? C1 C2 1.415(17) . ? C2 C3 1.384(16) . ? C2 H2A 0.9500 . ? C3 C4 1.360(17) . ? C3 H3A 0.9500 . ? C4 C5 1.373(17) . ? C4 H4A 0.9500 . ? C5 C6 1.338(15) . ? C5 H5A 0.9500 . ? C6 H6A 0.9500 . ? C7 C8 1.447(15) . ? C8 C11 1.393(16) . ? C8 C9 1.444(17) . ? C9 C10 1.488(16) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 C12 1.493(14) . ? C12 C13 1.362(17) . ? C12 C17 1.397(15) . ? C13 C14 1.382(16) . ? C13 H13A 0.9500 . ? C14 C15 1.375(17) . ? C14 H14A 0.9500 . ? C15 C16 1.372(17) . ? C16 C17 1.375(15) . ? C16 H16A 0.9500 . ? C17 H17A 0.9500 . ? C18 C23 1.368(17) . ? C18 C19 1.382(17) . ? C19 C20 1.392(16) . ? C19 H19A 0.9500 . ? C20 C21 1.383(18) . ? C20 H20A 0.9500 . ? C21 C22 1.378(18) . ? C21 H21A 0.9500 . ? C22 C23 1.412(16) . ? C22 H22A 0.9500 . ? C23 H23A 0.9500 . ? C24 C25 1.431(15) . ? C25 C26 1.416(17) . ? C25 C28 1.418(16) . ? C26 C27 1.510(16) . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 C29 1.486(15) . ? C29 C30 1.387(16) . ? C29 C34 1.389(16) . ? C30 C31 1.381(15) . ? C30 H30A 0.9500 . ? C31 C32 1.395(16) . ? C31 H31A 0.9500 . ? C32 C33 1.379(17) . ? C33 C34 1.369(16) . ? C33 H33A 0.9500 . ? C34 H34A 0.9500 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 U1 O1 178.8(4) . . ? O2 U1 O5 91.8(4) . . ? O1 U1 O5 89.3(3) . . ? O2 U1 O3 88.0(3) . . ? O1 U1 O3 90.9(3) . . ? O5 U1 O3 146.4(3) . . ? O2 U1 O7 88.0(3) . . ? O1 U1 O7 92.6(3) . . ? O5 U1 O7 72.1(3) . . ? O3 U1 O7 141.4(3) . . ? O2 U1 O4 90.7(3) . . ? O1 U1 O4 88.6(3) . . ? O5 U1 O4 142.3(2) . . ? O3 U1 O4 71.3(3) . . ? O7 U1 O4 70.4(3) . . ? O2 U1 O6 90.0(3) . . ? O1 U1 O6 90.1(3) . . ? O5 U1 O6 71.2(3) . . ? O3 U1 O6 75.1(3) . . ? O7 U1 O6 143.2(3) . . ? O4 U1 O6 146.4(3) . . ? O7 S1 C35 105.0(6) . . ? O7 S1 C36 103.4(5) . . ? C35 S1 C36 98.5(6) . . ? C7 O3 U1 132.4(6) . . ? C11 O4 U1 136.5(7) . . ? C24 O5 U1 126.1(8) . . ? C28 O6 U1 135.9(7) . . ? S1 O7 U1 132.6(5) . . ? C7 N1 C1 131.7(10) . . ? C7 N1 N2 111.8(9) . . ? C1 N1 N2 116.5(9) . . ? C9 N2 N1 105.9(9) . . ? C24 N3 N4 113.6(9) . . ? C24 N3 C18 128.8(10) . . ? N4 N3 C18 117.3(9) . . ? C26 N4 N3 104.0(9) . . ? N1 C1 C6 119.3(11) . . ? N1 C1 C2 121.2(11) . . ? C6 C1 C2 119.4(10) . . ? C3 C2 C1 118.1(11) . . ? C3 C2 H2A 121.0 . . ? C1 C2 H2A 121.0 . . ? C4 C3 C2 121.4(12) . . ? C4 C3 H3A 119.3 . . ? C2 C3 H3A 119.3 . . ? C3 C4 C5 119.4(11) . . ? C3 C4 H4A 120.3 . . ? C5 C4 H4A 120.3 . . ? C6 C5 C4 122.3(12) . . ? C6 C5 H5A 118.9 . . ? C4 C5 H5A 118.9 . . ? C5 C6 C1 119.4(11) . . ? C5 C6 H6A 120.3 . . ? C1 C6 H6A 120.3 . . ? O3 C7 N1 125.3(9) . . ? O3 C7 C8 128.2(10) . . ? N1 C7 C8 106.5(10) . . ? C11 C8 C9 132.2(10) . . ? C11 C8 C7 123.1(11) . . ? C9 C8 C7 104.2(9) . . ? N2 C9 C8 111.4(10) . . ? N2 C9 C10 117.4(11) . . ? C8 C9 C10 131.1(10) . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? O4 C11 C8 121.4(10) . . ? O4 C11 C12 116.5(10) . . ? C8 C11 C12 122.1(10) . . ? C13 C12 C17 119.8(10) . . ? C13 C12 C11 120.4(10) . . ? C17 C12 C11 119.6(10) . . ? C12 C13 C14 120.8(11) . . ? C12 C13 H13A 119.6 . . ? C14 C13 H13A 119.6 . . ? C15 C14 C13 119.2(11) . . ? C15 C14 H14A 120.4 . . ? C13 C14 H14A 120.4 . . ? C16 C15 C14 120.4(10) . . ? C16 C15 Cl1 119.2(9) . . ? C14 C15 Cl1 120.4(10) . . ? C15 C16 C17 120.5(11) . . ? C15 C16 H16A 119.8 . . ? C17 C16 H16A 119.8 . . ? C16 C17 C12 119.2(11) . . ? C16 C17 H17A 120.4 . . ? C12 C17 H17A 120.4 . . ? C23 C18 C19 122.5(11) . . ? C23 C18 N3 117.2(10) . . ? C19 C18 N3 120.1(11) . . ? C18 C19 C20 118.3(12) . . ? C18 C19 H19A 120.8 . . ? C20 C19 H19A 120.8 . . ? C21 C20 C19 120.3(12) . . ? C21 C20 H20A 119.9 . . ? C19 C20 H20A 119.9 . . ? C22 C21 C20 120.7(11) . . ? C22 C21 H21A 119.7 . . ? C20 C21 H21A 119.7 . . ? C21 C22 C23 119.5(12) . . ? C21 C22 H22A 120.3 . . ? C23 C22 H22A 120.3 . . ? C18 C23 C22 118.6(11) . . ? C18 C23 H23A 120.7 . . ? C22 C23 H23A 120.7 . . ? O5 C24 N3 126.2(10) . . ? O5 C24 C25 129.8(11) . . ? N3 C24 C25 103.9(10) . . ? C26 C25 C28 134.9(11) . . ? C26 C25 C24 105.2(10) . . ? C28 C25 C24 119.9(11) . . ? N4 C26 C25 113.3(10) . . ? N4 C26 C27 116.2(11) . . ? C25 C26 C27 129.9(11) . . ? C26 C27 H27A 109.5 . . ? C26 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C26 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? O6 C28 C25 121.8(10) . . ? O6 C28 C29 117.2(10) . . ? C25 C28 C29 121.0(10) . . ? C30 C29 C34 119.0(10) . . ? C30 C29 C28 119.5(10) . . ? C34 C29 C28 121.5(10) . . ? C31 C30 C29 121.4(11) . . ? C31 C30 H30A 119.3 . . ? C29 C30 H30A 119.3 . . ? C30 C31 C32 117.3(11) . . ? C30 C31 H31A 121.3 . . ? C32 C31 H31A 121.3 . . ? C33 C32 C31 122.8(10) . . ? C33 C32 Cl2 119.0(9) . . ? C31 C32 Cl2 118.2(9) . . ? C34 C33 C32 118.0(11) . . ? C34 C33 H33A 121.0 . . ? C32 C33 H33A 121.0 . . ? C33 C34 C29 121.5(12) . . ? C33 C34 H34A 119.3 . . ? C29 C34 H34A 119.3 . . ? S1 C35 H35A 109.5 . . ? S1 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? S1 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? S1 C36 H36A 109.5 . . ? S1 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? S1 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C35 S1 O7 U1 71.0(8) . . . . ? C36 S1 O7 U1 173.8(6) . . . . ? C7 N1 N2 C9 -1.2(13) . . . . ? C1 N1 N2 C9 179.2(10) . . . . ? C24 N3 N4 C26 2.3(12) . . . . ? C18 N3 N4 C26 176.1(9) . . . . ? C7 N1 C1 C6 -178.6(11) . . . . ? N2 N1 C1 C6 0.9(15) . . . . ? C7 N1 C1 C2 2.9(19) . . . . ? N2 N1 C1 C2 -177.6(10) . . . . ? N1 C1 C2 C3 178.6(11) . . . . ? C6 C1 C2 C3 0.0(17) . . . . ? C1 C2 C3 C4 -0.5(18) . . . . ? C2 C3 C4 C5 -0.2(19) . . . . ? C3 C4 C5 C6 1.5(19) . . . . ? C4 C5 C6 C1 -1.9(18) . . . . ? N1 C1 C6 C5 -177.4(11) . . . . ? C2 C1 C6 C5 1.1(17) . . . . ? U1 O3 C7 N1 -167.3(8) . . . . ? U1 O3 C7 C8 11.8(17) . . . . ? C1 N1 C7 O3 1(2) . . . . ? N2 N1 C7 O3 -178.2(10) . . . . ? C1 N1 C7 C8 -177.9(11) . . . . ? N2 N1 C7 C8 2.6(12) . . . . ? O3 C7 C8 C11 5.0(19) . . . . ? N1 C7 C8 C11 -175.7(11) . . . . ? O3 C7 C8 C9 177.9(11) . . . . ? N1 C7 C8 C9 -2.8(12) . . . . ? N1 N2 C9 C8 -0.7(13) . . . . ? N1 N2 C9 C10 177.8(10) . . . . ? C11 C8 C9 N2 174.2(12) . . . . ? C7 C8 C9 N2 2.2(13) . . . . ? C11 C8 C9 C10 -4(2) . . . . ? C7 C8 C9 C10 -176.1(12) . . . . ? U1 O4 C11 C8 -28.0(17) . . . . ? U1 O4 C11 C12 150.5(8) . . . . ? C9 C8 C11 O4 -168.5(12) . . . . ? C7 C8 C11 O4 2.2(18) . . . . ? C9 C8 C11 C12 13(2) . . . . ? C7 C8 C11 C12 -176.2(11) . . . . ? O4 C11 C12 C13 46.9(16) . . . . ? C8 C11 C12 C13 -134.6(13) . . . . ? O4 C11 C12 C17 -128.5(12) . . . . ? C8 C11 C12 C17 50.0(17) . . . . ? C17 C12 C13 C14 -2.9(19) . . . . ? C11 C12 C13 C14 -178.3(12) . . . . ? C12 C13 C14 C15 3(2) . . . . ? C13 C14 C15 C16 -1(2) . . . . ? C13 C14 C15 Cl1 177.8(10) . . . . ? C14 C15 C16 C17 -0.7(19) . . . . ? Cl1 C15 C16 C17 -179.2(9) . . . . ? C15 C16 C17 C12 0.3(18) . . . . ? C13 C12 C17 C16 1.5(18) . . . . ? C11 C12 C17 C16 177.0(11) . . . . ? C24 N3 C18 C23 -170.1(11) . . . . ? N4 N3 C18 C23 17.1(15) . . . . ? C24 N3 C18 C19 14.6(18) . . . . ? N4 N3 C18 C19 -158.1(11) . . . . ? C23 C18 C19 C20 -1(2) . . . . ? N3 C18 C19 C20 174.1(11) . . . . ? C18 C19 C20 C21 -0.8(19) . . . . ? C19 C20 C21 C22 3.2(19) . . . . ? C20 C21 C22 C23 -3.8(18) . . . . ? C19 C18 C23 C22 0.3(18) . . . . ? N3 C18 C23 C22 -174.8(10) . . . . ? C21 C22 C23 C18 2.0(17) . . . . ? U1 O5 C24 N3 -141.2(9) . . . . ? U1 O5 C24 C25 41.7(16) . . . . ? N4 N3 C24 O5 -180.0(10) . . . . ? C18 N3 C24 O5 7.0(19) . . . . ? N4 N3 C24 C25 -2.3(12) . . . . ? C18 N3 C24 C25 -175.3(10) . . . . ? O5 C24 C25 C26 178.9(12) . . . . ? N3 C24 C25 C26 1.4(12) . . . . ? O5 C24 C25 C28 -2.7(19) . . . . ? N3 C24 C25 C28 179.8(10) . . . . ? N3 N4 C26 C25 -1.3(13) . . . . ? N3 N4 C26 C27 -173.3(10) . . . . ? C28 C25 C26 N4 -178.1(12) . . . . ? C24 C25 C26 N4 0.0(13) . . . . ? C28 C25 C26 C27 -7(2) . . . . ? C24 C25 C26 C27 170.6(11) . . . . ? U1 O6 C28 C25 -1.7(17) . . . . ? U1 O6 C28 C29 177.6(7) . . . . ? C26 C25 C28 O6 159.7(12) . . . . ? C24 C25 C28 O6 -18.2(16) . . . . ? C26 C25 C28 C29 -19.7(19) . . . . ? C24 C25 C28 C29 162.5(10) . . . . ? O6 C28 C29 C30 -36.5(15) . . . . ? C25 C28 C29 C30 142.9(11) . . . . ? O6 C28 C29 C34 142.2(11) . . . . ? C25 C28 C29 C34 -38.4(16) . . . . ? C34 C29 C30 C31 1.1(17) . . . . ? C28 C29 C30 C31 179.9(11) . . . . ? C29 C30 C31 C32 -0.4(18) . . . . ? C30 C31 C32 C33 -2.0(19) . . . . ? C30 C31 C32 Cl2 177.4(9) . . . . ? C31 C32 C33 C34 3.5(19) . . . . ? Cl2 C32 C33 C34 -175.9(9) . . . . ? C32 C33 C34 C29 -2.6(18) . . . . ? C30 C29 C34 C33 0.4(18) . . . . ? C28 C29 C34 C33 -178.3(11) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C2 H2A O3 0.95 2.30 2.929(14) 122.7 . yes C14 H14A O5 0.95 2.63 3.443(15) 144.4 3_575 yes C16 H16A N1 0.95 2.68 3.265(15) 120.4 1_455 yes C16 H16A N2 0.95 2.68 3.516(14) 146.6 1_455 yes C19 H19A O5 0.95 2.30 2.925(14) 122.6 . yes C19 H19A O7 0.95 2.60 3.532(16) 168.4 . yes C33 H33A N4 0.95 2.68 3.426(14) 135.9 1_655 yes C35 H35C O6 0.98 2.53 3.391(16) 146.3 1_455 yes C36 H36C O1 0.98 2.57 3.285(13) 129.4 1_455 yes _refine_diff_density_max 1.645 _refine_diff_density_min -2.121 _refine_diff_density_rms 0.207 _shelx_res_file ; TITL shelxt_a.res in P-1 New:P21/n shelx.res created by SHELXL-2018/3 at 19:15:55 on 11-Feb-2022 CELL 0.71073 8.2480 15.0540 28.2620 90.000 95.583 90.000 ZERR 4 0.0020 0.0040 0.0080 0.000 0.010 0.000 LATT 1 SYMM 0.50000 - X , 0.50000 + Y , 0.50000 - Z SFAC C H Cl N O S U UNIT 144 120 8 16 28 4 4 TEMP -173 L.S. 15 ACTA CONF BOND $H htab HTAB C2 O3 EQIV $1 -x, -y+2, -z HTAB C14 O5_$1 EQIV $2 x-1, y, z HTAB C16 N1_$2 HTAB C16 N2_$2 HTAB C19 O5 HTAB C19 O7 EQIV $3 x+1, y, z HTAB C33 N4_$3 HTAB C35 O6_$2 HTAB C36 O1_$2 rigu isor .005 c5 twin 0.986 0 -0.029 0 -1 0 -0.993 0 -0.986 WGHT 0.021900 70.319206 BASF 0.00609 FVAR 0.99946 U1 7 0.229882 0.823241 0.057896 11.00000 0.00906 0.02710 = 0.03949 -0.00048 0.00079 0.00166 CL1 3 -0.605003 0.846188 -0.163145 11.00000 0.01799 0.02889 = 0.06232 -0.00279 -0.00969 0.00205 CL2 3 1.146762 0.562462 0.194464 11.00000 0.01419 0.03278 = 0.06228 -0.00211 -0.00442 0.00646 S1 6 -0.157026 0.932712 0.029481 11.00000 0.00750 0.02736 = 0.04251 0.00027 0.00158 0.00055 O1 5 0.347122 0.914753 0.042490 11.00000 0.00872 0.01084 = 0.05383 0.00258 -0.00286 -0.00477 O2 5 0.113900 0.730969 0.072168 11.00000 0.01365 0.01635 = 0.06233 0.00661 -0.00153 -0.00178 O3 5 0.353137 0.731545 0.003567 11.00000 0.01827 0.02155 = 0.03907 -0.00080 0.00381 0.00602 O4 5 0.075978 0.834596 -0.018866 11.00000 0.01289 0.02421 = 0.03869 -0.00184 0.00018 0.00472 O5 5 0.241284 0.877273 0.135668 11.00000 0.01351 0.03389 = 0.03843 0.00299 0.00430 0.00744 O6 5 0.465983 0.760854 0.103366 11.00000 0.01668 0.03399 = 0.03206 0.00076 0.00012 0.00166 O7 5 -0.006317 0.913271 0.064049 11.00000 0.01520 0.02780 = 0.04616 -0.00562 0.00117 0.00085 N1 4 0.375257 0.633383 -0.059326 11.00000 0.01607 0.02480 = 0.03723 0.00238 0.00324 0.00944 N2 4 0.287872 0.611384 -0.103456 11.00000 0.02080 0.02425 = 0.03991 -0.00048 0.00060 0.00006 N3 4 0.211707 0.840272 0.214321 11.00000 0.01712 0.02381 = 0.03716 0.00204 0.00275 0.00110 N4 4 0.281428 0.783154 0.249982 11.00000 0.01176 0.03637 = 0.03561 0.00447 -0.00140 0.00119 C1 1 0.520201 0.587377 -0.047492 11.00000 0.01259 0.02418 = 0.04168 0.00210 0.00286 0.00299 C2 1 0.614077 0.601675 -0.003515 11.00000 0.01724 0.03349 = 0.03663 0.00112 0.00573 0.00040 AFIX 43 H2A 2 0.581459 0.644006 0.018618 11.00000 -1.20000 AFIX 0 C3 1 0.754729 0.552218 0.006309 11.00000 0.01429 0.03323 = 0.04380 -0.00362 0.00418 0.00066 AFIX 43 H3A 2 0.819778 0.561202 0.035543 11.00000 -1.20000 AFIX 0 C4 1 0.801827 0.491003 -0.025008 11.00000 0.01431 0.02575 = 0.05098 -0.01059 -0.00260 -0.00586 AFIX 43 H4A 2 0.898985 0.457777 -0.017743 11.00000 -1.20000 AFIX 0 C5 1 0.707764 0.477654 -0.067197 11.00000 0.01274 0.03733 = 0.03516 0.00033 0.00439 0.00451 AFIX 43 H5A 2 0.740190 0.433787 -0.088530 11.00000 -1.20000 AFIX 0 C6 1 0.571941 0.524313 -0.079311 11.00000 0.01561 0.01735 = 0.04601 -0.00421 0.00326 -0.00431 AFIX 43 H6A 2 0.511139 0.514804 -0.109187 11.00000 -1.20000 AFIX 0 C7 1 0.299773 0.697276 -0.036386 11.00000 0.01307 0.02010 = 0.03537 0.00214 0.00398 0.00350 C8 1 0.149806 0.717116 -0.065376 11.00000 0.01159 0.02380 = 0.03705 0.00261 -0.00066 -0.00001 C9 1 0.155779 0.661629 -0.106826 11.00000 0.01815 0.02937 = 0.03831 0.00280 0.00014 0.00022 C10 1 0.043444 0.654449 -0.151163 11.00000 0.02049 0.03543 = 0.03803 -0.00329 -0.00177 0.01000 AFIX 137 H10A 2 0.101636 0.628369 -0.176413 11.00000 -1.50000 H10B 2 0.003901 0.713705 -0.160902 11.00000 -1.50000 H10C 2 -0.049184 0.616545 -0.145373 11.00000 -1.50000 AFIX 0 C11 1 0.043732 0.784491 -0.054512 11.00000 0.00957 0.02457 = 0.04264 -0.00033 0.00076 0.00028 C12 1 -0.115184 0.800040 -0.083328 11.00000 0.00872 0.02875 = 0.03939 -0.00305 0.00197 -0.00079 C13 1 -0.162134 0.883842 -0.096591 11.00000 0.01329 0.02665 = 0.05208 -0.00174 0.00131 -0.00329 AFIX 43 H13A 2 -0.091777 0.932446 -0.088110 11.00000 -1.20000 AFIX 0 C14 1 -0.310873 0.899078 -0.122239 11.00000 0.01707 0.02584 = 0.05211 0.00442 -0.00244 -0.00108 AFIX 43 H14A 2 -0.341040 0.957408 -0.132465 11.00000 -1.20000 AFIX 0 C15 1 -0.414683 0.828834 -0.132784 11.00000 0.01434 0.03371 = 0.05110 -0.00554 -0.00171 0.00028 C16 1 -0.370560 0.744437 -0.118434 11.00000 0.01084 0.03105 = 0.03881 -0.00098 0.00388 -0.00512 AFIX 43 H16A 2 -0.443698 0.696464 -0.125577 11.00000 -1.20000 AFIX 0 C17 1 -0.221242 0.728799 -0.093789 11.00000 0.01302 0.02772 = 0.03525 0.00213 0.00332 -0.00453 AFIX 43 H17A 2 -0.190567 0.670300 -0.083997 11.00000 -1.20000 AFIX 0 C18 1 0.068784 0.890147 0.224511 11.00000 0.01541 0.02616 = 0.04440 -0.00340 0.00194 -0.00010 C19 1 -0.036810 0.923051 0.187716 11.00000 0.02118 0.04247 = 0.04103 0.00004 0.00632 0.01279 AFIX 43 H19A 2 -0.012071 0.918331 0.155678 11.00000 -1.20000 AFIX 0 C20 1 -0.180349 0.963291 0.198758 11.00000 0.02614 0.02443 = 0.05095 0.00295 0.00774 0.01412 AFIX 43 H20A 2 -0.254182 0.987061 0.174085 11.00000 -1.20000 AFIX 0 C21 1 -0.215931 0.968815 0.245477 11.00000 0.01536 0.03183 = 0.05235 -0.00220 0.01119 -0.00161 AFIX 43 H21A 2 -0.316687 0.993676 0.252520 11.00000 -1.20000 AFIX 0 C22 1 -0.106674 0.938610 0.281928 11.00000 0.02053 0.02279 = 0.04995 -0.00385 0.00702 -0.00363 AFIX 43 H22A 2 -0.128871 0.945826 0.314063 11.00000 -1.20000 AFIX 0 C23 1 0.038504 0.896857 0.271124 11.00000 0.01779 0.02849 = 0.04204 -0.00378 0.00465 -0.00191 AFIX 43 H23A 2 0.113620 0.873893 0.295713 11.00000 -1.20000 AFIX 0 C24 1 0.280710 0.833859 0.172788 11.00000 0.01314 0.02712 = 0.03986 0.00274 0.00155 -0.00135 C25 1 0.408586 0.770421 0.182792 11.00000 0.01788 0.01539 = 0.04107 -0.00165 0.00329 -0.00139 C26 1 0.397828 0.744034 0.230485 11.00000 0.01418 0.02666 = 0.04125 0.00179 0.00102 -0.00235 C27 1 0.484288 0.669994 0.258830 11.00000 0.02151 0.04437 = 0.03857 0.00651 -0.00140 0.00774 AFIX 137 H27A 2 0.417409 0.650328 0.283677 11.00000 -1.50000 H27B 2 0.589490 0.691541 0.273521 11.00000 -1.50000 H27C 2 0.502062 0.620076 0.237685 11.00000 -1.50000 AFIX 0 C28 1 0.508624 0.746362 0.146796 11.00000 0.01602 0.01794 = 0.03609 -0.00188 -0.00125 -0.00459 C29 1 0.668212 0.701926 0.158861 11.00000 0.01072 0.01867 = 0.04025 0.00491 0.00404 -0.00469 C30 1 0.718759 0.636543 0.129017 11.00000 0.01565 0.02803 = 0.03871 0.00047 0.00066 -0.00222 AFIX 43 H30A 2 0.650535 0.620909 0.101237 11.00000 -1.20000 AFIX 0 C31 1 0.866185 0.593688 0.138835 11.00000 0.01381 0.03290 = 0.03820 -0.01135 -0.00079 -0.00091 AFIX 43 H31A 2 0.900507 0.548655 0.118475 11.00000 -1.20000 AFIX 0 C32 1 0.962692 0.619188 0.179856 11.00000 0.01029 0.02727 = 0.04089 -0.00287 -0.00444 0.00029 C33 1 0.918706 0.686102 0.209372 11.00000 0.01738 0.03084 = 0.03834 -0.00668 -0.00388 -0.00512 AFIX 43 H33A 2 0.989532 0.704311 0.236134 11.00000 -1.20000 AFIX 0 C34 1 0.769921 0.725523 0.198964 11.00000 0.01288 0.03089 = 0.04204 -0.00072 0.00181 -0.00231 AFIX 43 H34A 2 0.735475 0.770004 0.219629 11.00000 -1.20000 AFIX 0 C35 1 -0.270770 0.832198 0.026549 11.00000 0.02432 0.03926 = 0.06059 -0.00723 0.00828 -0.00607 AFIX 137 H35A 2 -0.202257 0.783525 0.016908 11.00000 -1.50000 H35B 2 -0.366133 0.838573 0.003259 11.00000 -1.50000 H35C 2 -0.306612 0.819095 0.057862 11.00000 -1.50000 AFIX 0 C36 1 -0.283765 0.996240 0.064392 11.00000 0.01389 0.03835 = 0.04371 0.00654 0.00543 0.00466 AFIX 137 H36A 2 -0.231127 1.053220 0.072775 11.00000 -1.50000 H36B 2 -0.300695 0.963501 0.093477 11.00000 -1.50000 H36C 2 -0.389106 1.006901 0.046106 11.00000 -1.50000 AFIX 0 HKLF 4 REM shelxt_a.res in P-1 New:P21/n REM wR2 = 0.1593, GooF = S = 1.147, Restrained GooF = 1.109 for all data REM R1 = 0.0755 for 5366 Fo > 4sig(Fo) and 0.0893 for all 6325 data REM 465 parameters refined using 450 restraints END WGHT 0.0216 70.4132 REM Instructions for potential hydrogen bonds HTAB C2 O3 HTAB C14 O5_$1 HTAB C16 N1_$2 HTAB C16 N2_$2 HTAB C19 O5 HTAB C19 O7 HTAB C33 N4_$3 HTAB C35 O6_$2 HTAB C36 O1_$2 REM Highest difference peak 1.645, deepest hole -2.121, 1-sigma level 0.207 Q1 1 0.2179 0.8182 0.0245 11.00000 0.05 1.65 Q2 1 0.1353 0.8021 0.0564 11.00000 0.05 1.50 Q3 1 0.2322 0.8271 0.0918 11.00000 0.05 1.41 Q4 1 0.2941 0.7747 0.0247 11.00000 0.05 1.32 Q5 1 0.3130 0.8043 0.0593 11.00000 0.05 1.28 Q6 1 -0.1857 0.9705 0.3292 11.00000 0.05 1.14 Q7 1 0.3000 0.8736 0.0240 11.00000 0.05 1.11 Q8 1 0.7321 0.4330 -0.0619 11.00000 0.05 1.05 Q9 1 0.1680 0.7728 0.0919 11.00000 0.05 1.05 Q10 1 0.0649 0.7772 0.0178 11.00000 0.05 1.00 Q11 1 0.8233 0.4330 -0.0508 11.00000 0.05 0.99 Q12 1 0.0372 0.8258 0.0698 11.00000 0.05 0.98 Q13 1 0.1551 0.7365 0.0263 11.00000 0.05 0.93 Q14 1 0.1886 0.8252 0.1198 11.00000 0.05 0.93 Q15 1 0.0000 1.0000 0.0000 10.50000 0.05 0.92 Q16 1 0.1367 0.8773 0.0898 11.00000 0.05 0.91 Q17 1 0.4441 0.8219 0.0455 11.00000 0.05 0.91 Q18 1 0.0735 0.8683 0.0187 11.00000 0.05 0.90 Q19 1 0.2680 0.8223 -0.0050 11.00000 0.05 0.90 Q20 1 0.1915 0.9019 0.0297 11.00000 0.05 0.88 ; _shelx_res_checksum 51531 _shelx_hkl_file ; 2 0 0153084.0 9594.11 1 4 0 022339.40 1210.97 1 6 0 017336.60 988.157 1 8 0 014627.40 929.175 1 1 1 012454.50 394.213 1 2 1 0 303.264 53.242 1 3 1 0 309.279 71.145 1 4 1 0 7955.61 383.528 1 5 1 010146.80 453.588 1 6 1 017366.30 699.767 1 7 1 0 5758.31 370.381 1 8 1 0 8952.84 488.941 1 9 1 0 3491.83 373.437 1 0 2 096608.20 5240.09 1 1 2 061546.30 2244.57 1 2 2 0 9848.96 373.479 1 3 2 031013.00 1099.00 1 4 2 014152.80 603.477 1 5 2 064310.30 2231.28 1 6 2 020324.50 835.213 1 7 2 019954.50 820.062 1 8 2 0 5336.43 382.469 1 9 2 0 1403.24 266.486 1 1 3 0 840.181 343.496 1 2 3 0 2901.24 155.764 1 3 3 010585.90 417.749 1 4 3 0 3097.23 253.038 1 5 3 025956.70 1180.64 1 6 3 0 617.38 138.203 1 7 3 013846.60 692.197 1 8 3 0 496.076 172.577 1 9 3 013328.60 694.409 1 0 4 016615.10 806.558 1 1 4 0170399.0 5860.90 1 2 4 0 2778.89 728.575 1 3 4 050132.30 1669.36 1 4 4 0 2746.89 194.245 1 5 4 019916.30 873.61 1 6 4 0 2465.04 239.25 1 7 4 0 7613.46 394.66 1 8 4 0 713.636 193.293 1 9 4 0 2177.85 304.133 1 1 5 0 2160.76 135.036 1 2 5 0 6195.93 292.591 1 3 5 0 7828.95 344.524 1 4 5 012050.40 586.963 1 5 5 0 5706.64 340.858 1 6 5 021371.40 875.541 1 7 5 0 6645.53 371.875 1 8 5 0 8433.42 503.565 1 9 5 0 4586.08 454.553 1 0 6 016525.40 793.458 1 1 6 0 267.365 55.5572 1 2 6 066227.00 2147.91 1 3 6 013276.90 539.155 1 4 6 041774.60 2170.28 1 5 6 010579.40 481.863 1 6 6 040536.80 1511.71 1 7 6 0 1424.53 190.129 1 8 6 0 1367.73 214.097 1 9 6 0 1112.91 273.606 1 1 7 0 2336.12 170.954 1 2 7 0 6736.22 336.316 1 3 7 0 2348.63 202.013 1 4 7 010145.30 609.624 1 5 7 0 752.333 231.149 1 6 7 013049.30 633.935 1 7 7 0 1089.56 321.631 1 8 7 0 9425.52 574.779 1 9 7 0 284.558 262.943 1 0 8 033593.30 2886.67 1 1 8 0 9965.97 427.331 1 2 8 029822.80 1209.34 1 3 8 0 6182.06 334.983 1 4 8 0 8886.36 446.473 1 5 8 0 2623.99 278.182 1 6 8 0 3660.58 294.576 1 7 8 0 7371.08 518.077 1 8 8 0 3480.33 304.594 1 1 9 0 320.933 103.948 1 2 9 0 1779.76 223.393 1 3 9 0 2592.84 284.117 1 4 9 0 1491.82 152.933 1 5 9 012247.50 706.683 1 6 9 0 3527.96 347.412 1 7 9 011147.50 658.405 1 8 9 0 4700.42 1035.88 1 0 10 0 1169.08 236.535 1 1 10 026275.30 1252.27 1 2 10 0 714.392 110.184 1 3 10 023993.00 1061.00 1 4 10 0 3144.06 248.932 1 5 10 0 6674.72 497.894 1 6 10 0 1275.32 324.19 1 7 10 0 8258.12 1248.40 1 8 10 0 7124.30 3332.92 1 1 11 0 2916.45 232.946 1 2 11 0 5611.71 2706.45 1 3 11 0 663.913 186.255 1 4 11 0 3020.62 359.284 1 5 11 0 5686.05 589.007 1 6 11 0 4418.37 677.761 1 7 11 0 7864.70 3163.65 1 0 12 022807.50 1441.01 1 1 12 010835.60 613.008 1 2 12 0 5373.29 364.578 1 3 12 0 1404.71 248.973 1 4 12 0 5860.37 377.285 1 5 12 0 601.118 283.097 1 6 12 0 2680.14 564.185 1 7 12 0 2243.69 534.062 1 1 13 0 5212.91 591.213 1 2 13 0 2379.12 213.69 1 3 13 0 4665.21 898.717 1 4 13 0 2511.33 297.896 1 5 13 0 2087.90 563.352 1 6 13 0 5638.88 901.143 1 0 14 010932.30 760.411 1 1 14 0 3301.34 363.55 1 2 14 0 8350.22 551.328 1 3 14 0 483.065 164.056 1 4 14 013384.60 962.674 1 5 14 0 755.814 397.007 1 6 14 0 9251.03 1518.91 1 1 15 0 3361.10 839.219 1 2 15 0 2334.46 773.967 1 3 15 0 3212.28 1883.18 1 4 15 0 2575.80 300.965 1 5 15 0 2941.19 614.382 1 0 16 0 1373.90 283.46 1 1 16 0 7066.07 1014.01 1 2 16 0 3068.45 477.42 1 3 16 0 5678.08 594.907 1 4 16 0 1513.30 331.524 1 1 17 0 138.497 204.33 1 2 17 0 4077.56 701.086 1 3 17 0 1278.68 308.853 1 0 18 0 1830.63 538.773 1 -9 0 110383.40 847.597 1 -7 0 117717.80 1044.82 1 -5 0 135910.70 1898.71 1 -3 0 130478.60 1759.48 1 -1 0 128245.70 1390.16 1 1 0 1 8079.30 388.338 1 3 0 1 274.083 87.496 1 5 0 1 4105.95 337.827 1 7 0 1 3233.28 406.183 1 9 0 1 2018.19 421.951 1 -9 1 1 362.095 228.319 1 -8 1 1 587.748 180.81 1 -7 1 1 2764.17 254.531 1 -6 1 1 211.194 114.631 1 -5 1 121400.80 839.218 1 -4 1 119300.40 739.359 1 -3 1 1 6441.48 343.418 1 -2 1 119101.00 744.286 1 -1 1 165812.30 2523.47 1 1 1 1117312.0 3638.34 1 2 1 1 8563.23 316.629 1 3 1 143793.20 1379.62 1 4 1 1 710.366 103.507 1 5 1 119960.30 755.504 1 6 1 1 5445.06 323.165 1 7 1 120973.00 830.327 1 8 1 1 5496.85 378.432 1 9 1 1 8984.93 538.506 1 -9 2 1 7129.92 521.532 1 -8 2 125269.90 1005.77 1 -7 2 125139.00 979.384 1 -6 2 136218.70 1370.49 1 -5 2 113039.30 538.201 1 -4 2 149989.60 1930.45 1 -3 2 1 8654.11 382.67 1 -2 2 1 8386.53 328.596 1 -1 2 113205.40 527.786 1 0 2 1 9834.51 602.234 1 1 2 113636.10 580.853 1 2 2 119518.00 638.048 1 3 2 1 1071.29 102.445 1 4 2 1 5794.81 275.655 1 5 2 1 423.944 109.533 1 6 2 1 9311.39 454.491 1 7 2 1 6940.08 431.294 1 8 2 118895.50 830.138 1 9 2 1 7688.19 539.101 1 -9 3 1 1813.42 315.514 1 -8 3 1 1712.64 230.592 1 -7 3 1 3254.97 264.368 1 -6 3 125006.70 907.005 1 -5 3 1 1368.71 249.279 1 -4 3 136777.10 1376.76 1 -3 3 1 703.633 275.202 1 -2 3 112325.30 446.52 1 -1 3 1106606.0 6241.59 1 0 3 190671.50 3280.67 1 1 3 112707.00 532.465 1 2 3 1108873.0 3290.47 1 3 3 1 2481.31 150.851 1 4 3 148133.50 1780.09 1 5 3 1 280.403 107.611 1 6 3 142635.40 1574.74 1 7 3 1 372.442 151.149 1 8 3 111907.90 582.083 1 9 3 1 1882.02 305.657 1 -9 4 1 273.562 218.214 1 -8 4 112819.80 594.244 1 -7 4 1 545.41 198.267 1 -6 4 122053.60 896.895 1 -5 4 1 6350.60 357.271 1 -4 4 132298.00 1172.99 1 -3 4 1 6913.37 320.09 1 -2 4 1104753.0 3867.16 1 -1 4 1 4874.07 631.271 1 0 4 1 1315.34 90.5409 1 1 4 1 317.628 78.0029 1 2 4 1 4116.69 187.612 1 3 4 121638.00 716.998 1 4 4 1 2174.01 176.031 1 5 4 1 855.627 130.504 1 6 4 112054.00 580.135 1 7 4 1 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11 115083.40 874.172 1 5 11 1 516.001 241.206 1 6 11 112657.00 2787.03 1 7 11 1 1217.91 459.835 1 -7 12 1 3817.95 1476.57 1 -6 12 1 6259.95 1020.53 1 -5 12 1 6434.04 539.724 1 -4 12 1 6529.36 425.334 1 -3 12 1 6193.66 515.988 1 -2 12 1 9517.94 497.962 1 -1 12 1 4485.13 452.301 1 0 12 1 6877.16 526.917 1 1 12 1 4509.94 335.688 1 2 12 1 1415.59 323.784 1 3 12 1 1241.87 441.086 1 4 12 1 2305.88 425.551 1 5 12 1 1391.44 324.32 1 6 12 1 1738.19 455.251 1 7 12 1 5062.83 745.555 1 -6 13 1 1767.28 575.07 1 -5 13 1 2872.82 332.309 1 -4 13 1 2003.45 209.735 1 -3 13 111361.10 617.40 1 -2 13 1 4280.04 1163.72 1 -1 13 115545.70 1494.92 1 0 13 1 605.612 256.127 1 1 13 115072.40 1185.56 1 2 13 1 2548.90 247.789 1 3 13 114780.10 954.852 1 4 13 1 622.487 136.029 1 5 13 110287.30 1005.21 1 6 13 1 1559.32 411.803 1 -6 14 1 1450.57 491.579 1 -5 14 1 7484.96 1810.50 1 -4 14 1 3041.80 1136.65 1 -3 14 1 2063.65 272.793 1 -2 14 1 5683.25 1787.84 1 -1 14 1 2325.96 262.678 1 0 14 1 4728.72 1166.03 1 1 14 1 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9 2 6248.25 560.907 1 6 9 2 2007.46 342.039 1 7 9 2 1013.81 667.066 1 8 9 2 2214.07 1197.14 1 -8 10 2 2288.62 1550.68 1 -7 10 2 121.786 302.967 1 -6 10 2 2591.04 1564.66 1 -5 10 2 2072.50 218.365 1 -4 10 2 866.868 147.70 1 -3 10 2 5172.35 333.978 1 -2 10 2 2072.25 261.828 1 -1 10 210945.60 557.548 1 0 10 2 3521.84 311.223 1 1 10 242096.20 1751.23 1 2 10 2 1221.94 262.178 1 3 10 212858.30 647.922 1 4 10 2 1070.53 244.428 1 5 10 213489.50 856.382 1 6 10 2 945.263 328.496 1 7 10 213342.90 1394.21 1 8 10 2 1232.64 520.811 1 -7 11 214396.10 867.89 1 -6 11 2 688.462 198.811 1 -5 11 2 8784.48 486.473 1 -4 11 2 913.556 395.061 1 -3 11 2 9185.97 482.127 1 -2 11 2 3871.75 1561.92 1 -1 11 214774.50 859.25 1 0 11 2 6693.36 869.051 1 1 11 211173.20 615.856 1 2 11 2 3758.36 375.717 1 3 11 2 2882.85 286.884 1 4 11 2 4784.66 432.439 1 5 11 2 635.604 235.967 1 6 11 2 2589.61 496.196 1 7 11 2 754.487 410.076 1 -7 12 2 1521.45 487.453 1 -6 12 2 980.764 651.729 1 -5 12 2 545.376 225.555 1 -4 12 2 3260.20 337.674 1 -3 12 2 2658.08 602.167 1 -2 12 2 9167.00 1031.24 1 -1 12 2 7861.47 512.038 1 0 12 2 9648.77 693.949 1 1 12 2 7756.69 495.222 1 2 12 2 6544.71 679.685 1 3 12 2 7067.60 503.286 1 4 12 2 8138.73 643.771 1 5 12 2 3439.07 435.796 1 6 12 2 6082.03 979.89 1 7 12 2 5604.72 2505.27 1 -6 13 2 6616.41 879.831 1 -5 13 2 1406.02 290.607 1 -4 13 217262.30 1238.73 1 -3 13 2 1955.54 1253.09 1 -2 13 212122.80 846.139 1 -1 13 2 5137.01 1310.75 1 0 13 2 6294.26 417.632 1 1 13 2 8318.79 528.621 1 2 13 2 514.489 156.347 1 3 13 2 3026.76 575.45 1 4 13 2 725.194 258.88 1 5 13 2 1146.47 376.586 1 6 13 2 537.62 415.424 1 -6 14 2 739.489 372.126 1 -5 14 2 2942.00 1054.63 1 -4 14 2 1772.76 218.052 1 -3 14 2 1958.19 307.142 1 -2 14 2 7048.35 661.006 1 -1 14 2 3696.82 1632.49 1 0 14 2 5403.36 409.935 1 1 14 2 3345.01 835.197 1 2 14 2 5635.42 432.648 1 3 14 2 1767.43 1034.15 1 4 14 211347.60 882.554 1 5 14 2 543.26 395.951 1 6 14 213043.90 2671.98 1 -5 15 2 1909.33 263.792 1 -4 15 2 7171.66 499.223 1 -3 15 2 1553.58 284.381 1 -2 15 2 1966.25 221.393 1 -1 15 2 3122.34 349.398 1 0 15 2 5959.07 433.162 1 1 15 2 3713.20 338.433 1 2 15 2 2388.42 455.653 1 3 15 2 4762.08 703.843 1 4 15 2 1769.89 470.053 1 5 15 2 1885.59 632.271 1 -4 16 2 3389.07 660.569 1 -3 16 2 2285.78 281.827 1 -2 16 2 3248.14 519.803 1 -1 16 2 5382.12 583.055 1 0 16 2 2997.69 506.803 1 1 16 2 4269.16 408.339 1 2 16 2 6690.41 687.633 1 3 16 2 5962.31 790.215 1 4 16 2 3569.46 600.354 1 -3 17 2 8435.45 692.69 1 -2 17 2 1254.69 363.562 1 -1 17 2 3660.34 405.766 1 0 17 2 4616.75 807.186 1 1 17 2 1804.51 253.623 1 2 17 2 2045.00 522.454 1 3 17 2 507.978 193.129 1 0 18 2 2325.90 594.03 1 -9 0 311205.40 771.617 1 -7 0 343071.90 2181.59 1 -5 0 341684.40 2488.89 1 -3 0 352737.30 2960.63 1 -1 0 397036.70 4687.43 1 1 0 347305.80 2332.93 1 3 0 328919.80 1528.60 1 5 0 322625.30 1341.11 1 7 0 3 1052.91 258.977 1 9 0 3 1622.58 387.811 1 -9 1 310825.30 566.184 1 -8 1 3 3230.21 332.558 1 -7 1 3 8028.31 424.022 1 -6 1 3 5512.84 341.343 1 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3 317619.70 669.904 1 -1 3 328406.80 1219.44 1 0 3 312193.70 878.408 1 1 3 319722.10 762.635 1 2 3 3 8349.35 299.04 1 3 3 310378.60 375.485 1 4 3 377563.90 2496.48 1 5 3 3 3316.99 233.712 1 6 3 316894.20 680.818 1 7 3 3 3333.21 290.866 1 8 3 3 9080.27 502.523 1 9 3 3 3512.31 388.108 1 -9 4 3 2096.04 313.955 1 -8 4 312827.70 602.032 1 -7 4 3 4662.84 343.977 1 -6 4 334222.60 1237.66 1 -5 4 3 1271.04 151.442 1 -4 4 361562.50 2105.58 1 -3 4 316036.70 648.949 1 -2 4 3146032.0 7033.56 1 -1 4 3 5711.28 304.723 1 0 4 348644.10 2239.48 1 1 4 3 2178.28 125.95 1 2 4 3 9728.06 392.084 1 3 4 3 1272.93 110.976 1 4 4 319038.90 650.115 1 5 4 3 352.482 103.089 1 6 4 3 6848.80 377.887 1 7 4 3 594.341 174.398 1 8 4 3 153.397 166.258 1 9 4 3 1164.02 273.086 1 -9 5 3 3393.26 376.78 1 -8 5 3 4832.69 387.873 1 -7 5 3 4644.10 427.184 1 -6 5 3 174.126 128.57 1 -5 5 3 4275.65 246.822 1 -4 5 3 255.538 115.705 1 -3 5 3 109.69 85.0532 1 -2 5 3 1026.87 109.417 1 -1 5 3 724.344 75.8111 1 0 5 3 2142.99 138.357 1 1 5 3 3692.88 191.666 1 2 5 319744.30 758.776 1 3 5 3 5143.70 249.448 1 4 5 342310.60 1690.30 1 5 5 313609.10 563.565 1 6 5 330656.50 1163.28 1 7 5 3 6985.91 398.302 1 8 5 312365.30 738.25 1 9 5 310415.80 632.923 1 -9 6 3 8171.95 602.365 1 -8 6 3 358.43 171.008 1 -7 6 317569.50 738.029 1 -6 6 3 3205.96 261.525 1 -5 6 315577.90 647.577 1 -4 6 3 6264.18 292.87 1 -3 6 350165.40 1777.84 1 -2 6 3 7014.40 332.281 1 -1 6 346839.40 1613.01 1 0 6 3 4937.92 240.143 1 1 6 315675.50 616.315 1 2 6 3 879.463 90.0748 1 3 6 3 7578.97 378.889 1 4 6 3 432.634 110.995 1 5 6 311183.60 499.433 1 6 6 3 710.712 172.31 1 7 6 3 1100.39 175.465 1 8 6 3 522.547 163.574 1 9 6 3 645.528 210.071 1 -9 7 3 5720.18 788.817 1 -8 7 3 1408.83 790.851 1 -7 7 3 3473.19 265.481 1 -6 7 3 818.616 360.933 1 -5 7 3 265.033 183.13 1 -4 7 3 4437.74 295.507 1 -3 7 3 6546.28 340.425 1 -2 7 3 1401.52 120.059 1 -1 7 3 2358.76 167.747 1 0 7 3 6157.83 293.779 1 1 7 3 6853.75 307.559 1 2 7 3 1313.53 127.351 1 3 7 3 8546.12 463.048 1 4 7 3 6646.26 431.011 1 5 7 335452.10 2614.96 1 6 7 3 2882.40 207.574 1 7 7 320008.50 1101.46 1 8 7 3 336.686 128.866 1 -8 8 3 5620.88 375.694 1 -7 8 317623.50 922.107 1 -6 8 3 6969.75 477.584 1 -5 8 324550.10 1122.94 1 -4 8 3 5406.58 324.623 1 -3 8 323827.30 993.252 1 -2 8 315986.90 682.121 1 -1 8 316535.90 622.591 1 0 8 3 6637.38 326.797 1 1 8 315443.00 683.133 1 2 8 3 630.369 91.8723 1 3 8 3 5952.60 380.538 1 4 8 3 838.346 191.095 1 5 8 3 8450.11 568.201 1 6 8 3 4156.34 470.663 1 7 8 3 2028.13 257.755 1 8 8 3 933.928 561.71 1 -8 9 3 3830.97 731.261 1 -7 9 3 2057.91 862.223 1 -6 9 3 5395.47 439.492 1 -5 9 3 4812.24 1419.15 1 -4 9 3 1815.60 190.824 1 -3 9 3 871.073 236.992 1 -2 9 3 875.739 142.198 1 -1 9 3 2959.81 341.716 1 0 9 313442.40 563.283 1 1 9 3 2920.44 237.077 1 2 9 316804.40 740.98 1 3 9 3 2250.31 260.649 1 4 9 3 4014.97 354.654 1 5 9 324450.30 1299.13 1 6 9 3 9441.98 1242.15 1 7 9 3 9101.57 881.799 1 8 9 3 9507.46 1076.21 1 -8 10 314176.30 876.316 1 -7 10 3 136.554 345.729 1 -6 10 311836.70 838.079 1 -5 10 3 1048.05 222.299 1 -4 10 318012.00 802.445 1 -3 10 3 768.86 264.422 1 -2 10 323898.60 1147.34 1 -1 10 3 876.31 349.323 1 0 10 337807.10 1733.87 1 1 10 3 5949.89 349.961 1 2 10 320294.80 846.641 1 3 10 3 456.695 182.174 1 4 10 3 7805.01 538.419 1 5 10 3 3960.30 449.183 1 6 10 3 269.224 265.278 1 7 10 3 1734.91 1324.27 1 8 10 3-89.2332 473.239 1 -7 11 3 3838.76 1267.08 1 -6 11 3 771.934 198.106 1 -5 11 3 2429.87 266.481 1 -4 11 3 449.006 131.194 1 -3 11 3 1592.05 794.646 1 -2 11 3 1618.74 178.319 1 -1 11 3 6373.19 612.217 1 0 11 3 9534.89 876.299 1 1 11 3 2002.32 334.676 1 2 11 3 8825.58 470.636 1 3 11 3 3270.85 455.874 1 4 11 3 6922.42 494.651 1 5 11 3 4456.30 598.862 1 6 11 312407.30 1602.70 1 7 11 3 3453.21 592.409 1 -7 12 3 5057.96 493.259 1 -6 12 310132.50 798.353 1 -5 12 3 6198.21 596.174 1 -4 12 315113.20 804.348 1 -3 12 3 7024.41 424.621 1 -2 12 3 4615.89 1200.58 1 -1 12 314198.30 680.521 1 0 12 3 6094.21 671.813 1 1 12 3 5075.66 364.153 1 2 12 3 9576.95 525.297 1 3 12 3 3848.71 339.512 1 4 12 3 2073.95 305.942 1 5 12 3 2515.17 387.659 1 6 12 3 3016.17 530.499 1 7 12 3 1843.75 532.461 1 -6 13 3 2361.07 957.665 1 -5 13 3 1276.73 192.549 1 -4 13 3 5479.30 1635.81 1 -3 13 3 472.881 192.808 1 -2 13 3 9121.43 2391.63 1 -1 13 3 3113.50 556.002 1 0 13 3 6130.79 1131.44 1 1 13 313426.90 662.189 1 2 13 3 1358.54 773.585 1 3 13 3 4810.73 416.531 1 4 13 3 1871.22 473.861 1 5 13 3 4382.28 554.826 1 6 13 3 2226.08 539.51 1 -6 14 3 699.236 353.225 1 -5 14 3 9561.63 649.745 1 -4 14 3 535.322 260.356 1 -3 14 3 6776.38 1112.13 1 -2 14 3 3935.23 1425.08 1 -1 14 3 9625.49 1094.59 1 0 14 3 984.257 414.334 1 1 14 316117.10 1123.18 1 2 14 3 1929.95 247.233 1 3 14 3 6670.79 696.069 1 4 14 3 3887.52 913.994 1 5 14 3 559.396 353.851 1 6 14 3 2362.37 981.667 1 -5 15 3 803.038 176.587 1 -4 15 3 3164.61 388.095 1 -3 15 3 1478.23 272.464 1 -2 15 3 2572.76 1215.87 1 -1 15 3 2544.74 446.505 1 0 15 3 1926.56 378.218 1 1 15 3 956.807 229.156 1 2 15 3 1517.54 350.237 1 3 15 3 3518.24 370.645 1 4 15 3 7372.01 884.966 1 5 15 3 5811.73 665.817 1 -4 16 312133.00 860.607 1 -3 16 3 1906.88 324.793 1 -2 16 3 5858.61 867.988 1 -1 16 3 1191.25 407.292 1 0 16 3 3597.81 512.865 1 1 16 3 2541.89 308.217 1 2 16 3 6319.74 766.398 1 3 16 3 1091.22 382.455 1 4 16 3 2688.22 478.082 1 -3 17 3 3459.76 537.93 1 -2 17 3 947.427 222.076 1 -1 17 3 4875.75 825.185 1 0 17 3 3106.70 502.045 1 1 17 3 1363.33 246.961 1 2 17 3 1766.38 284.441 1 3 17 3 879.689 328.987 1 0 18 3 3053.27 824.871 1 -8 0 438588.40 1868.24 1 -6 0 429210.80 1837.87 1 -4 0 4 8978.22 580.186 1 -2 0 4 2100.53 159.159 1 0 0 4 4652.37 580.776 1 2 0 4 4013.86 214.183 1 4 0 413949.80 834.856 1 6 0 433292.40 1617.39 1 8 0 436177.50 1795.62 1 -9 1 4 2506.63 305.319 1 -8 1 414592.70 636.379 1 -7 1 4 3216.52 283.251 1 -6 1 422029.00 896.142 1 -5 1 4 410.065 126.706 1 -4 1 414131.40 542.138 1 -3 1 4 7717.76 346.28 1 -2 1 422374.70 748.305 1 -1 1 460291.70 2711.24 1 0 1 411987.50 459.532 1 1 1 4 344.668 44.9621 1 2 1 450163.30 1556.37 1 3 1 4 3938.43 179.998 1 4 1 444231.70 1489.69 1 5 1 4 908.778 138.439 1 6 1 410384.20 480.849 1 7 1 4 4782.23 330.754 1 8 1 4 3555.48 320.471 1 9 1 4 1919.76 291.849 1 -9 2 4 9530.94 633.016 1 -8 2 410772.40 540.29 1 -7 2 4 5923.34 374.568 1 -6 2 4 185.446 132.442 1 -5 2 4 6907.29 365.467 1 -4 2 4 2343.20 170.212 1 -3 2 4 6455.01 300.201 1 -2 2 410251.90 385.629 1 -1 2 4 1099.35 81.6762 1 0 2 4 5271.75 228.876 1 1 2 4 103.253 35.2039 1 2 2 423250.00 867.40 1 3 2 4 2128.80 139.021 1 4 2 411496.30 438.827 1 5 2 428202.50 948.611 1 6 2 4 6652.37 350.133 1 7 2 4 4345.02 357.429 1 8 2 4 7263.35 456.923 1 9 2 4 4805.88 412.213 1 -9 3 4 3543.08 375.068 1 -8 3 4 467.043 232.414 1 -7 3 421243.90 874.332 1 -6 3 4 2944.98 254.396 1 -5 3 411855.30 488.704 1 -4 3 4 3602.31 212.181 1 -3 3 436185.50 1210.75 1 -2 3 4 1414.70 116.108 1 -1 3 4161213.0 6159.86 1 0 3 4 129.98 47.5598 1 1 3 429346.30 1238.14 1 2 3 4 6640.60 293.448 1 3 3 447616.20 1517.26 1 4 3 4 121.021 68.5734 1 5 3 421366.70 759.968 1 6 3 4 61.0579 102.35 1 7 3 410998.50 542.813 1 8 3 4 828.844 199.423 1 9 3 4 934.538 255.633 1 -9 4 412623.50 788.737 1 -8 4 4 664.12 199.136 1 -7 4 422804.50 923.598 1 -6 4 4 4104.45 300.822 1 -5 4 418452.00 656.268 1 -4 4 4 246.925 74.9131 1 -3 4 4 2716.27 167.812 1 -2 4 411147.00 538.041 1 -1 4 4 6159.58 319.34 1 0 4 4 3177.45 223.283 1 1 4 4 131.779 36.9709 1 2 4 418194.90 681.515 1 3 4 4 442.717 51.3839 1 4 4 4 511.516 85.595 1 5 4 417394.90 672.887 1 6 4 4 2438.10 217.118 1 7 4 427687.00 1022.95 1 8 4 4 484.933 206.332 1 9 4 412380.50 711.094 1 -9 5 4 5254.81 508.667 1 -8 5 4 7559.28 500.701 1 -7 5 4 8551.01 465.977 1 -6 5 4 7257.57 383.275 1 -5 5 415857.90 580.559 1 -4 5 420451.50 783.612 1 -3 5 424684.10 1161.61 1 -2 5 448917.60 1875.31 1 -1 5 4 7352.89 487.858 1 0 5 433959.00 1260.70 1 1 5 415241.40 531.962 1 2 5 4 1190.83 119.07 1 3 5 420939.60 859.682 1 4 5 4 5420.34 244.336 1 5 5 4 7332.69 342.773 1 6 5 415741.10 678.218 1 7 5 4 3480.48 273.939 1 8 5 4 2028.03 259.718 1 9 5 4 1568.03 311.733 1 -9 6 4 3134.25 517.65 1 -8 6 4 4093.39 362.033 1 -7 6 4 746.161 219.625 1 -6 6 4 9873.60 449.25 1 -5 6 4 739.502 119.935 1 -4 6 4 2611.81 169.919 1 -3 6 4 4033.22 238.443 1 -2 6 4 3071.16 242.422 1 -1 6 4 3223.48 230.79 1 0 6 4 136.25 65.1684 1 1 6 4 157.633 68.7263 1 2 6 410175.70 456.114 1 3 6 417441.70 672.684 1 4 6 443670.70 2549.13 1 5 6 4 4123.86 239.407 1 6 6 414987.40 645.243 1 7 6 4 5079.40 339.438 1 8 6 4 3706.12 309.203 1 9 6 4 2733.85 335.901 1 -9 7 4 704.619 352.981 1 -8 7 410496.50 649.827 1 -7 7 4 2794.92 255.157 1 -6 7 413811.50 755.033 1 -5 7 4 307.177 87.9505 1 -4 7 442557.90 1752.97 1 -3 7 4 2860.88 220.861 1 -2 7 440396.80 1374.40 1 -1 7 4 41.2941 64.1817 1 0 7 447197.30 1807.76 1 1 7 4 86.136 74.4588 1 2 7 442400.90 1646.83 1 3 7 4 99.8961 70.3148 1 4 7 422972.40 1068.98 1 5 7 4 1227.57 182.759 1 6 7 420396.70 1177.70 1 7 7 4 747.212 150.164 1 8 7 4 2324.88 215.988 1 -8 8 4 9963.26 1217.35 1 -7 8 4 2172.29 220.762 1 -6 8 416076.30 976.786 1 -5 8 4 6009.94 406.293 1 -4 8 4 507.792 135.326 1 -3 8 4 1279.81 182.414 1 -2 8 4 6428.99 345.985 1 -1 8 4 333.58 157.368 1 0 8 413363.50 526.818 1 1 8 4 518.898 100.665 1 2 8 4 205.489 75.3899 1 3 8 4 985.33 186.844 1 4 8 4 5658.01 420.302 1 5 8 4 4293.40 454.027 1 6 8 414494.90 1284.28 1 7 8 4 2542.48 424.473 1 8 8 420413.20 1118.49 1 -8 9 4 4318.23 795.249 1 -7 9 410271.20 732.558 1 -6 9 4 2819.23 271.267 1 -5 9 416053.70 757.192 1 -4 9 4 6813.39 413.664 1 -3 9 422197.50 1156.67 1 -2 9 410641.60 473.201 1 -1 9 439944.60 1501.61 1 0 9 4 8972.00 413.364 1 1 9 423740.10 973.51 1 2 9 4 9046.53 415.151 1 3 9 4 5921.61 402.149 1 4 9 4 8875.17 564.974 1 5 9 4 8214.50 701.268 1 6 9 4 2500.00 375.658 1 7 9 4 5041.38 652.385 1 8 9 4 2213.98 589.41 1 -8 10 4 3995.40 1753.44 1 -7 10 4 4210.93 718.496 1 -6 10 4 1068.58 1432.14 1 -5 10 4 1696.83 199.291 1 -4 10 4 1468.75 1237.52 1 -3 10 4 5489.62 345.351 1 -2 10 4 7354.53 450.513 1 -1 10 4 272.751 102.74 1 0 10 4 6717.85 1923.61 1 1 10 4 7490.91 378.895 1 2 10 4 1375.97 284.938 1 3 10 4 9684.49 595.839 1 4 10 4 2140.31 322.665 1 5 10 411971.50 897.612 1 6 10 4 551.569 344.878 1 7 10 4 8033.66 1000.83 1 8 10 4 116.256 809.411 1 -7 11 4 5973.94 1048.05 1 -6 11 4 4773.35 782.783 1 -5 11 414078.00 709.969 1 -4 11 4 964.919 159.77 1 -3 11 417067.10 785.827 1 -2 11 4 758.077 174.799 1 -1 11 419163.00 813.346 1 0 11 4 9181.39 705.861 1 1 11 417533.00 1068.98 1 2 11 4 3632.91 293.949 1 3 11 416426.90 836.967 1 4 11 4 486.34 195.118 1 5 11 4 8041.97 754.241 1 6 11 4 1276.77 366.697 1 7 11 4 3527.56 1498.45 1 -7 12 4 5031.94 870.891 1 -6 12 4 5431.56 912.503 1 -5 12 4 4007.49 493.073 1 -4 12 4 3129.58 1383.88 1 -3 12 4 1371.01 773.482 1 -2 12 4 960.691 228.076 1 -1 12 4 9561.11 1718.41 1 0 12 4 1701.90 258.566 1 1 12 4 3790.78 315.62 1 2 12 4 1417.74 172.345 1 3 12 4 1681.56 224.792 1 4 12 4 3329.48 372.76 1 5 12 4 1447.64 488.783 1 6 12 4 5998.56 1209.95 1 7 12 4 6254.37 873.256 1 -6 13 4 5875.55 606.735 1 -5 13 4 1981.53 236.69 1 -4 13 413598.20 1105.78 1 -3 13 4 1563.48 204.94 1 -2 13 416125.50 807.604 1 -1 13 4 1202.53 186.357 1 0 13 419535.90 1984.36 1 1 13 4 8711.28 503.344 1 2 13 411513.70 625.384 1 3 13 4 4420.76 498.079 1 4 13 4 4943.62 544.789 1 5 13 4 846.604 370.768 1 6 13 4 2209.83 650.569 1 -6 14 4 977.353 239.657 1 -5 14 4 1914.27 760.29 1 -4 14 4 3173.15 459.634 1 -3 14 4 2217.37 1373.69 1 -2 14 4 3303.94 276.221 1 -1 14 4 7796.74 3207.89 1 0 14 4 229.915 130.718 1 1 14 4 6206.33 1062.67 1 2 14 4 3045.62 301.83 1 3 14 4 1615.47 875.73 1 4 14 4 6755.44 709.565 1 5 14 4 2467.78 640.651 1 6 14 4 7969.28 1438.46 1 -5 15 4 2244.70 304.718 1 -4 15 4 8497.96 931.80 1 -3 15 4 5126.00 522.838 1 -2 15 4 4712.55 777.109 1 -1 15 4 5025.19 684.146 1 0 15 4 4360.43 378.706 1 1 15 4 472.19 152.239 1 2 15 4 6452.86 486.681 1 3 15 4 2838.79 279.572 1 4 15 4 5157.80 660.506 1 5 15 4 2228.17 688.697 1 -4 16 4 3237.93 471.136 1 -3 16 4 1243.31 252.872 1 -2 16 4 6437.82 1182.75 1 -1 16 4 998.734 360.534 1 0 16 4 1810.45 488.174 1 1 16 4 1950.23 308.853 1 2 16 4 1399.06 262.276 1 3 16 4 1617.17 212.861 1 4 16 4 2159.19 565.041 1 -3 17 4 7054.65 847.076 1 -2 17 4 703.689 213.914 1 -1 17 4 4453.57 564.817 1 0 17 4 1132.66 381.486 1 1 17 4 3334.13 729.078 1 2 17 4 1521.20 333.002 1 3 17 4 6840.26 1353.25 1 -9 0 5-36.5287 284.093 1 -7 0 5 9453.95 690.325 1 -5 0 542379.70 2246.98 1 -3 0 515483.70 785.628 1 -1 0 5134192.0 6478.04 1 1 0 555525.80 2803.87 1 3 0 534404.40 1623.77 1 5 0 522895.30 1323.20 1 7 0 514969.30 849.161 1 9 0 511416.20 1073.92 1 -9 1 516772.20 736.612 1 -8 1 511036.80 540.462 1 -7 1 510528.10 506.215 1 -6 1 511639.20 577.986 1 -5 1 551026.80 1990.84 1 -4 1 5 1833.97 156.71 1 -3 1 520217.50 705.829 1 -2 1 5 131.758 46.4219 1 -1 1 5 1072.46 82.8512 1 0 1 5 1817.73 114.996 1 1 1 5 45.4858 32.0886 1 2 1 5 2447.39 115.709 1 3 1 5 1773.62 108.425 1 4 1 5 461.162 82.4427 1 5 1 5 6437.89 333.886 1 6 1 5 9257.28 459.386 1 7 1 511462.40 523.821 1 8 1 5 1659.94 233.622 1 9 1 5 3700.27 371.353 1 -9 2 5 2028.92 327.702 1 -8 2 5 4889.82 383.716 1 -7 2 5 5400.94 376.893 1 -6 2 5 4788.50 331.76 1 -5 2 5 2257.56 193.247 1 -4 2 5 1285.42 137.606 1 -3 2 5 327.048 74.6571 1 -2 2 531439.60 1082.84 1 -1 2 516645.00 832.649 1 0 2 5174246.0 5698.22 1 1 2 573050.30 2925.66 1 2 2 573358.40 2454.65 1 3 2 594107.40 2978.13 1 4 2 521579.70 747.81 1 5 2 5 9596.13 416.129 1 6 2 5 6656.68 351.61 1 7 2 5 6721.26 388.817 1 8 2 5 7426.05 454.841 1 9 2 5 2711.21 317.245 1 -9 3 5 1520.04 367.572 1 -8 3 513479.10 634.217 1 -7 3 5 951.477 195.298 1 -6 3 523266.70 953.821 1 -5 3 5 158.886 87.9652 1 -4 3 537318.70 1278.47 1 -3 3 5 389.629 74.9393 1 -2 3 5 969.584 75.08 1 -1 3 5 1994.32 122.063 1 0 3 5 98.3165 45.117 1 1 3 5 852.319 113.939 1 2 3 5 488.462 56.4202 1 3 3 5 2371.31 149.824 1 4 3 5 8800.43 356.33 1 5 3 5 468.454 104.489 1 6 3 514687.00 583.217 1 7 3 5 1041.68 188.552 1 8 3 510617.00 569.334 1 9 3 5 887.344 303.928 1 -9 4 5 1496.54 343.335 1 -8 4 5-56.4238 177.313 1 -7 4 5 1149.45 247.829 1 -6 4 515617.80 635.00 1 -5 4 5 894.63 126.603 1 -4 4 551716.80 1705.63 1 -3 4 5 575.491 83.2675 1 -2 4 5192540.0 7387.49 1 -1 4 5 3901.61 180.388 1 0 4 526067.10 1017.80 1 1 4 5 5259.84 272.815 1 2 4 539428.30 1414.86 1 3 4 5 103.779 39.43 1 4 4 525279.30 886.885 1 5 4 5 4858.38 258.692 1 6 4 541686.50 1368.29 1 7 4 5 100.687 133.143 1 8 4 517201.30 849.623 1 9 4 5 1678.31 270.934 1 -9 5 5 8864.25 612.872 1 -8 5 5 6329.76 452.836 1 -7 5 513923.70 639.355 1 -6 5 5 6588.73 361.642 1 -5 5 5 5441.37 275.76 1 -4 5 518385.40 706.991 1 -3 5 5 5656.05 314.102 1 -2 5 521171.40 882.358 1 -1 5 5 124.676 50.6247 1 0 5 5 149.724 53.1711 1 1 5 5 5621.35 244.734 1 2 5 5 1278.10 132.445 1 3 5 5 5969.29 303.532 1 4 5 5 3625.29 186.372 1 5 5 511887.30 483.112 1 6 5 5 1081.30 146.483 1 7 5 5 4277.97 291.677 1 8 5 5 5121.28 374.46 1 9 5 5 1906.96 276.703 1 -9 6 5 2152.22 330.069 1 -8 6 5 1845.51 377.228 1 -7 6 5 7502.06 419.098 1 -6 6 5 379.835 284.901 1 -5 6 5 3913.21 226.982 1 -4 6 5 1493.78 136.302 1 -3 6 521768.40 1557.25 1 -2 6 523194.70 884.224 1 -1 6 546748.80 1612.47 1 0 6 5 4992.30 228.805 1 1 6 533549.70 1224.56 1 2 6 520131.90 812.869 1 3 6 543405.80 1637.86 1 4 6 515691.90 665.595 1 5 6 523125.30 928.473 1 6 6 5 1592.82 201.539 1 7 6 5 5739.16 347.804 1 8 6 5 164.717 133.892 1 9 6 5 2696.90 368.277 1 -9 7 5 9172.58 729.337 1 -8 7 5 415.644 669.357 1 -7 7 516376.90 749.601 1 -6 7 5 710.211 139.841 1 -5 7 514524.30 852.897 1 -4 7 5 5451.19 307.934 1 -3 7 545536.00 1729.02 1 -2 7 5 312.299 114.822 1 -1 7 5 1492.21 133.295 1 0 7 5 6179.21 326.042 1 1 7 5 3911.10 201.743 1 2 7 5 212.072 98.8095 1 3 7 5 3229.68 248.623 1 4 7 5 1403.84 169.767 1 5 7 512434.30 621.542 1 6 7 5 1347.36 271.741 1 7 7 5 9862.52 602.938 1 8 7 5 512.086 157.288 1 -8 8 5 2151.17 563.059 1 -7 8 5 877.393 169.054 1 -6 8 511259.60 765.136 1 -5 8 5 5842.27 373.666 1 -4 8 5 1613.06 182.38 1 -3 8 538317.10 1544.70 1 -2 8 5 5496.84 283.349 1 -1 8 523098.10 869.769 1 0 8 5 4916.17 306.659 1 1 8 512402.10 787.408 1 2 8 5 9466.67 406.834 1 3 8 519231.00 1259.89 1 4 8 5 2978.40 320.271 1 5 8 523648.40 1063.43 1 6 8 510895.10 649.997 1 7 8 517947.20 931.395 1 8 8 5 4048.01 420.694 1 -8 9 515556.20 1290.99 1 -7 9 5 5823.91 629.401 1 -6 9 518165.60 1203.28 1 -5 9 5 5988.83 378.234 1 -4 9 5 7562.21 420.332 1 -3 9 5 1844.77 202.693 1 -2 9 5 1793.75 172.883 1 -1 9 5 3018.71 231.486 1 0 9 5 313.799 105.929 1 1 9 5 716.138 132.307 1 2 9 5 787.254 110.663 1 3 9 5 1110.27 239.495 1 4 9 5 3992.27 379.375 1 5 9 5 1416.81 287.688 1 6 9 5 4330.36 509.129 1 7 9 5 1775.10 502.427 1 8 9 5 4528.97 773.489 1 -8 10 5 8932.57 768.525 1 -7 10 5 1882.72 693.429 1 -6 10 5 6355.20 454.42 1 -5 10 5 802.039 188.35 1 -4 10 5 7639.11 458.293 1 -3 10 5 998.821 470.444 1 -2 10 513868.80 578.984 1 -1 10 5 55.3617 153.706 1 0 10 540231.30 1502.49 1 1 10 5 2319.73 205.555 1 2 10 539311.90 1405.25 1 3 10 5 1060.69 212.481 1 4 10 515422.10 879.611 1 5 10 5 314.844 220.741 1 6 10 5 8066.75 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3 716356.10 719.952 1 -7 3 7 6224.73 397.331 1 -6 3 717917.20 766.696 1 -5 3 711515.90 501.008 1 -4 3 751103.40 1886.48 1 -3 3 7 64.7378 61.6841 1 -2 3 742420.30 2083.03 1 -1 3 710092.00 434.676 1 0 3 735041.80 1363.08 1 1 3 7 1750.20 173.072 1 2 3 711728.30 506.434 1 3 3 7 847.563 85.0432 1 4 3 710458.40 437.718 1 5 3 7 1448.65 140.579 1 6 3 7 113.043 100.977 1 7 3 7 6194.52 381.902 1 8 3 7 560.541 199.205 1 9 3 7 2338.93 329.234 1 -9 4 7 1173.51 659.113 1 -8 4 7 1570.84 261.429 1 -7 4 7 4307.81 350.628 1 -6 4 7 655.855 145.159 1 -5 4 7 128.437 105.863 1 -4 4 7 1255.94 137.38 1 -3 4 7 4622.82 245.235 1 -2 4 7 4261.60 235.575 1 -1 4 7 4062.86 294.013 1 0 4 7 7443.00 322.221 1 1 4 7 1855.32 149.666 1 2 4 741471.70 2859.05 1 3 4 7 7362.37 370.136 1 4 4 751470.10 1845.83 1 5 4 7 2542.71 181.267 1 6 4 743057.20 1591.79 1 7 4 7 6113.56 335.834 1 8 4 715566.60 813.584 1 9 4 7 3418.80 353.27 1 -9 5 7 5520.07 546.873 1 -8 5 7 5642.86 472.761 1 -7 5 7 7054.48 424.078 1 -6 5 7 6480.93 336.101 1 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1 -1 7 735280.30 1260.36 1 0 7 7 92.7804 69.2038 1 1 7 720899.70 979.493 1 2 7 7 763.255 139.059 1 3 7 714672.60 679.329 1 4 7 7 255.397 126.198 1 5 7 7 5221.24 336.318 1 6 7 7 485.155 194.477 1 7 7 7 831.774 262.353 1 8 7 7 1146.35 363.68 1 -8 8 7 1189.43 323.036 1 -7 8 7 1252.54 312.762 1 -6 8 7 839.216 213.802 1 -5 8 7 341.608 188.164 1 -4 8 7 3234.87 264.227 1 -3 8 7 226.80 82.2298 1 -2 8 7 230.959 83.9168 1 -1 8 7 2967.75 219.277 1 0 8 7 843.223 115.451 1 1 8 713230.00 600.042 1 2 8 714883.10 1075.65 1 3 8 711570.60 744.704 1 4 8 720410.30 847.613 1 5 8 716976.80 826.081 1 6 8 7 4230.67 404.607 1 7 8 717060.70 1030.08 1 8 8 7 3146.37 405.621 1 -8 9 714101.40 1006.35 1 -7 9 7 3113.46 329.068 1 -6 9 711733.00 819.399 1 -5 9 7 5904.80 382.636 1 -4 9 723827.80 1000.17 1 -3 9 7 7445.81 374.335 1 -2 9 719129.90 746.708 1 -1 9 712154.10 547.363 1 0 9 7 7513.78 429.431 1 1 9 7 8286.43 401.615 1 2 9 720898.90 1257.86 1 3 9 7 2920.43 338.556 1 4 9 721678.70 1030.51 1 5 9 7 596.682 166.104 1 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949.671 1 5 1 810180.60 444.292 1 6 1 8 6522.31 402.563 1 7 1 8 4853.77 348.189 1 8 1 810827.80 539.53 1 9 1 8 4453.20 474.236 1 -9 2 8 1485.98 378.325 1 -8 2 8 1063.54 226.064 1 -7 2 8 3744.55 328.476 1 -6 2 810714.50 482.35 1 -5 2 815078.90 656.963 1 -4 2 817771.00 730.367 1 -3 2 843683.80 1453.71 1 -2 2 858296.40 1885.79 1 -1 2 848792.50 1595.12 1 0 2 8 6901.45 375.361 1 1 2 8 9108.03 390.30 1 2 2 8 9644.68 437.331 1 3 2 818285.00 684.888 1 4 2 8 5545.11 253.524 1 5 2 820336.70 776.764 1 6 2 815469.50 652.289 1 7 2 8 4167.53 301.83 1 8 2 8 3177.80 291.835 1 9 2 8 175.734 236.52 1 -9 3 8 7490.54 652.541 1 -8 3 8 370.158 194.933 1 -7 3 810779.00 585.01 1 -6 3 8 1053.89 160.795 1 -5 3 8 7702.17 393.049 1 -4 3 8 378.035 107.202 1 -3 3 8 30.2387 65.6922 1 -2 3 8 5182.72 274.42 1 -1 3 8 410.586 76.7802 1 0 3 8 8042.33 353.479 1 1 3 8 178.027 52.957 1 2 3 8 1385.38 102.355 1 3 3 830844.00 1761.69 1 4 3 8 1178.01 111.842 1 5 3 818993.40 688.553 1 6 3 8 4698.26 269.482 1 7 3 8 8308.81 474.487 1 8 3 8 1221.85 218.815 1 9 3 814208.90 1127.24 1 -9 4 811459.80 871.282 1 -8 4 8 4251.81 395.09 1 -7 4 814691.20 652.60 1 -6 4 8 889.63 152.496 1 -5 4 818904.20 734.272 1 -4 4 8 1346.92 146.84 1 -3 4 820047.70 1193.55 1 -2 4 8 1224.36 124.377 1 -1 4 894053.00 3431.14 1 0 4 8 571.003 77.9256 1 1 4 856538.50 4105.14 1 2 4 8 2704.73 218.498 1 3 4 831300.60 1583.45 1 4 4 8 2340.92 231.057 1 5 4 820285.80 716.867 1 6 4 8 1554.90 186.129 1 7 4 8 4498.96 312.956 1 8 4 8 297.565 161.838 1 9 4 8 967.313 259.096 1 -9 5 8 5207.71 632.174 1 -8 5 8 3769.58 395.315 1 -7 5 8 9710.93 541.299 1 -6 5 8 6863.87 355.659 1 -5 5 8 4502.88 278.609 1 -4 5 8 374.622 96.9245 1 -3 5 8 718.81 113.334 1 -2 5 813192.70 730.92 1 -1 5 8 2597.41 169.974 1 0 5 8 916.785 104.687 1 1 5 8 3413.41 198.144 1 2 5 8 379.612 62.8901 1 3 5 813387.30 575.711 1 4 5 817486.10 688.221 1 5 5 8 8027.83 356.166 1 6 5 8 9324.23 494.146 1 7 5 8 9920.17 484.053 1 8 5 8 7580.07 488.873 1 -9 6 8 807.488 405.786 1 -8 6 8 5984.35 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10 8 9542.74 803.108 1 6 10 8 259.606 293.597 1 7 10 8 5464.25 627.966 1 -7 11 8 3950.65 347.07 1 -6 11 8 1908.11 266.841 1 -5 11 8 2797.88 315.271 1 -4 11 8 1303.94 349.181 1 -3 11 8 1891.95 177.791 1 -2 11 8 539.631 137.449 1 -1 11 8 919.704 293.318 1 0 11 8 970.783 288.748 1 1 11 8 3745.06 269.726 1 2 11 8 2135.93 315.21 1 3 11 8 6582.32 474.791 1 4 11 8 2420.83 337.627 1 5 11 8 5433.28 588.412 1 6 11 8 54.6279 337.816 1 7 11 8 5128.48 811.707 1 -7 12 8 4662.07 471.713 1 -6 12 8 4472.07 462.538 1 -5 12 8 5199.22 615.272 1 -4 12 811102.30 538.707 1 -3 12 8 4784.58 288.426 1 -2 12 811352.20 742.733 1 -1 12 8 5995.31 346.439 1 0 12 8 8196.47 412.70 1 1 12 816211.50 811.943 1 2 12 811349.00 961.541 1 3 12 8 7673.24 658.197 1 4 12 812489.80 962.996 1 5 12 8 1489.24 369.88 1 6 12 8 3764.04 562.30 1 -6 13 8 3529.91 416.16 1 -5 13 8 1606.53 1016.48 1 -4 13 8 68.8312 132.406 1 -3 13 8 3145.62 289.778 1 -2 13 8 812.992 146.506 1 -1 13 8 1063.73 215.949 1 0 13 8 491.74 130.041 1 1 13 8 2713.43 403.499 1 2 13 8 905.969 133.363 1 3 13 8 3601.80 429.997 1 4 13 8 4344.76 532.16 1 5 13 8 898.792 372.97 1 6 13 8 5995.23 1296.20 1 -6 14 8 7036.34 700.295 1 -5 14 8 128.156 410.395 1 -4 14 814662.40 947.254 1 -3 14 8 593.333 213.484 1 -2 14 813410.90 1638.00 1 -1 14 8 1925.34 209.78 1 0 14 8 4148.10 332.044 1 1 14 8 3189.73 249.944 1 2 14 8 6474.02 829.947 1 3 14 8 2123.93 342.358 1 4 14 8 5177.60 715.332 1 5 14 8 669.803 447.924 1 -5 15 8 3443.44 611.738 1 -4 15 8 780.187 316.49 1 -3 15 8 1893.36 288.943 1 -2 15 8 1096.72 255.082 1 -1 15 8 1362.80 467.576 1 0 15 8 943.581 169.665 1 1 15 8 1324.17 280.92 1 2 15 8 1009.87 199.673 1 3 15 8 1874.42 439.732 1 4 15 8 2779.52 694.194 1 -4 16 8 480.668 203.317 1 -3 16 8 5998.54 624.346 1 -2 16 8 1453.35 204.999 1 -1 16 8 8530.41 527.778 1 0 16 8 1593.21 221.642 1 1 16 8 7347.88 531.209 1 2 16 8 3761.90 409.745 1 3 16 8 4634.48 873.21 1 -2 17 8 2598.61 450.566 1 -1 17 8 690.386 210.208 1 0 17 8 1766.41 506.679 1 1 17 8 330.811 189.546 1 2 17 8 1634.05 970.373 1 -9 0 914768.80 1433.81 1 -7 0 911002.50 826.229 1 -5 0 9 7077.77 485.677 1 -3 0 9 470.02 126.837 1 -1 0 924801.60 1912.48 1 1 0 9 4889.03 465.727 1 3 0 9 1474.96 160.27 1 5 0 921478.90 1152.62 1 7 0 9 6778.78 642.43 1 9 0 9 4533.75 659.821 1 -9 1 9 1259.80 390.931 1 -8 1 9 1723.04 269.562 1 -7 1 910825.90 576.986 1 -6 1 9 1738.03 203.412 1 -5 1 910646.70 493.947 1 -4 1 9 1998.74 185.286 1 -3 1 936842.70 1245.70 1 -2 1 9 8064.04 357.851 1 -1 1 957387.70 2729.92 1 0 1 927311.00 1183.62 1 1 1 9106648.0 4173.18 1 2 1 920952.90 996.869 1 3 1 916754.40 755.512 1 4 1 910227.20 411.568 1 5 1 924726.00 963.903 1 6 1 9 9986.23 521.041 1 7 1 920559.50 913.291 1 8 1 9 5922.50 424.959 1 9 1 9 4266.13 364.411 1 -9 2 9 1747.04 405.255 1 -8 2 9 4930.58 451.97 1 -7 2 9 5382.54 395.016 1 -6 2 915895.10 649.176 1 -5 2 912346.00 577.866 1 -4 2 915482.20 632.299 1 -3 2 9 6832.21 309.212 1 -2 2 9 2655.38 157.692 1 -1 2 9 2270.45 145.766 1 0 2 9 135.789 60.1158 1 1 2 9 1283.90 112.69 1 2 2 9 125.415 63.7878 1 3 2 9 2440.30 172.919 1 4 2 9 2516.10 196.504 1 5 2 9 470.57 97.0344 1 6 2 9 2948.58 235.855 1 7 2 9 3701.73 281.101 1 8 2 9 4746.14 375.439 1 9 2 9 6286.63 506.081 1 -9 3 9 555.641 441.932 1 -8 3 9 5291.17 427.334 1 -7 3 9 378.127 178.406 1 -6 3 918457.30 754.898 1 -5 3 9 2076.21 217.763 1 -4 3 921461.00 829.208 1 -3 3 9 151.075 79.4006 1 -2 3 936489.10 2459.30 1 -1 3 9 1575.51 128.316 1 0 3 953126.30 3148.10 1 1 3 9 186.91 72.9055 1 2 3 956686.10 2013.97 1 3 3 9 3805.07 256.473 1 4 3 922708.70 848.917 1 5 3 9 5111.81 260.75 1 6 3 917909.60 693.678 1 7 3 9 568.79 150.074 1 8 3 9 8148.62 510.184 1 9 3 9 467.036 212.356 1 -9 4 9 1029.65 359.268 1 -8 4 9 9402.21 601.926 1 -7 4 9 4051.18 328.024 1 -6 4 9 8628.42 458.416 1 -5 4 9 4039.71 262.167 1 -4 4 9 4237.44 255.67 1 -3 4 9 435.124 84.9027 1 -2 4 9 2228.97 182.259 1 -1 4 9 1292.81 115.66 1 0 4 9 8477.55 518.214 1 1 4 9 3854.32 339.761 1 2 4 9 319.397 65.7493 1 3 4 9 2016.60 150.009 1 4 4 915090.40 587.052 1 5 4 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9 5822.70 372.184 1 -6 7 9 197.987 122.309 1 -5 7 926223.90 2195.02 1 -4 7 9 968.314 137.988 1 -3 7 926034.40 1584.64 1 -2 7 9 394.30 104.549 1 -1 7 930874.40 1747.66 1 0 7 9 64.4609 82.1706 1 1 7 946146.40 2347.58 1 2 7 9 1421.04 137.373 1 3 7 926459.00 1402.32 1 4 7 9 529.151 152.819 1 5 7 925704.80 1107.75 1 6 7 9 615.30 174.154 1 7 7 9 9408.35 550.961 1 8 7 9 723.693 350.395 1 -8 8 9 1368.96 457.125 1 -7 8 9 7869.82 531.766 1 -6 8 9 4405.45 355.817 1 -5 8 9 2378.10 248.728 1 -4 8 9 5780.13 411.125 1 -3 8 9 6692.16 441.173 1 -2 8 9 3314.42 268.768 1 -1 8 9 7024.35 373.998 1 0 8 9 4349.23 339.331 1 1 8 9 7705.13 404.364 1 2 8 9 480.603 145.711 1 3 8 9 354.116 140.399 1 4 8 9 6713.05 419.622 1 5 8 9 8181.86 490.912 1 6 8 9 1023.12 228.092 1 7 8 9 7653.13 882.235 1 8 8 9 951.705 291.263 1 -8 9 9 1846.97 399.753 1 -7 9 9 425.985 413.995 1 -6 9 9 7550.50 500.611 1 -5 9 9 2623.09 276.268 1 -4 9 912540.60 628.404 1 -3 9 9 7958.00 440.44 1 -2 9 915727.80 889.222 1 -1 9 9 8663.01 445.242 1 0 9 924226.30 974.819 1 1 9 9 4220.55 339.465 1 2 9 915753.90 1132.43 1 3 9 9 6314.53 506.121 1 4 9 9 4427.34 357.568 1 5 9 9 5444.04 368.149 1 6 9 9 6436.10 536.43 1 7 9 9 1714.22 365.987 1 -8 10 913397.80 1025.40 1 -7 10 9 1328.72 474.294 1 -6 10 912970.70 1257.71 1 -5 10 9 579.999 239.902 1 -4 10 917162.90 811.347 1 -3 10 9 1340.67 806.708 1 -2 10 9 727.347 125.272 1 -1 10 9 1242.30 319.619 1 0 10 9 75.4442 104.787 1 1 10 9 3213.63 268.985 1 2 10 9 162.353 91.8505 1 3 10 9 373.289 147.375 1 4 10 9 459.879 154.574 1 5 10 9 330.963 195.723 1 6 10 9 597.589 300.969 1 7 10 9 959.876 443.133 1 -7 11 9 1808.10 331.015 1 -6 11 9 5436.67 477.998 1 -5 11 9 1321.27 232.414 1 -4 11 9 9320.64 940.127 1 -3 11 9 1430.44 196.157 1 -2 11 9 8675.56 442.988 1 -1 11 9 863.94 139.491 1 0 11 918132.10 1761.36 1 1 11 9 4161.22 364.015 1 2 11 921204.90 937.665 1 3 11 9 2118.09 287.501 1 4 11 910778.50 1177.16 1 5 11 9 2926.28 427.467 1 6 11 9 3274.27 476.933 1 7 11 9 2787.54 682.681 1 -7 12 9 3690.86 599.887 1 -6 12 9 1061.25 370.886 1 -5 12 9 3661.75 410.091 1 -4 12 9 2012.88 570.537 1 -3 12 9 3257.87 245.17 1 -2 12 9 6603.92 489.276 1 -1 12 9 1498.99 249.223 1 0 12 9 1700.74 237.759 1 1 12 9 1498.72 211.895 1 2 12 9 1114.42 208.045 1 3 12 9 1555.44 303.246 1 4 12 9 3240.91 488.608 1 5 12 9 533.888 393.045 1 6 12 9 3716.64 557.592 1 -6 13 9 1593.04 614.752 1 -5 13 9 4163.85 570.923 1 -4 13 9 4145.26 395.52 1 -3 13 9 9346.12 857.883 1 -2 13 9 544.455 138.247 1 -1 13 910630.90 910.049 1 0 13 9 505.029 202.544 1 1 13 912473.60 634.396 1 2 13 9 1457.08 160.473 1 3 13 9 6670.26 906.895 1 4 13 9 947.916 343.323 1 5 13 9 4537.35 868.705 1 6 13 9 977.695 469.965 1 -5 14 9 6304.14 586.35 1 -4 14 9 2480.84 1127.98 1 -3 14 9 5837.25 416.199 1 -2 14 9 1637.85 430.162 1 -1 14 9 328.55 130.50 1 0 14 9 2385.84 234.79 1 1 14 9 422.439 143.424 1 2 14 9 1693.52 366.129 1 3 14 9 749.388 298.031 1 4 14 9 1113.64 447.613 1 5 14 9 143.428 339.243 1 -5 15 9 3435.47 575.251 1 -4 15 9 1603.76 306.419 1 -3 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250.306 73.0787 1 2 1 10 595.588 422.41 1 3 1 10 719.651 94.5777 1 4 1 10 1270.13 224.51 1 5 1 10 3561.11 225.132 1 6 1 10 8266.77 495.947 1 7 1 10 784.983 174.619 1 8 1 10 3930.42 310.578 1 9 1 10 188.531 223.884 1 -9 2 10 6.86529 319.741 1 -8 2 10 1080.83 250.479 1 -7 2 10 251.525 186.379 1 -6 2 10 1876.87 220.963 1 -5 2 10 1900.00 208.303 1 -4 2 1013545.60 543.582 1 -3 2 1028632.60 1000.40 1 -2 2 10 2449.08 162.501 1 -1 2 1039630.60 1391.86 1 0 2 1021002.40 782.816 1 1 2 1063728.90 4944.14 1 2 2 1024205.90 910.801 1 3 2 1012420.40 549.956 1 4 2 10 3244.73 226.848 1 5 2 10 6730.37 382.092 1 6 2 10 5988.11 364.059 1 7 2 1011222.70 614.565 1 8 2 1010511.40 587.971 1 9 2 1011312.00 679.536 1 -9 3 1014621.70 955.283 1 -8 3 10 55.1241 230.424 1 -7 3 1020315.20 815.648 1 -6 3 10 122.132 132.128 1 -5 3 1036069.40 1394.02 1 -4 3 10 210.619 99.4997 1 -3 3 1016691.90 663.454 1 -2 3 1040463.10 2274.79 1 -1 3 1013667.60 534.383 1 0 3 10 2687.25 166.938 1 1 3 10 7861.96 419.968 1 2 3 10 1397.19 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746.113 372.103 1 -3 13 13 952.918 192.221 1 -2 13 13 836.092 268.517 1 -1 13 13 1095.26 243.805 1 0 13 13 1506.11 296.702 1 1 13 13 436.392 154.34 1 2 13 13 1048.04 273.903 1 3 13 13 573.364 264.816 1 4 13 13 122.486 236.048 1 5 13 13 3413.47 975.691 1 -5 14 13 7458.49 687.80 1 -4 14 13-175.841 191.142 1 -3 14 13 6676.48 541.629 1 -2 14 13 251.047 147.603 1 -1 14 13 9645.72 607.759 1 0 14 13 165.185 140.997 1 1 14 1313355.70 743.345 1 2 14 13 586.622 267.774 1 3 14 1313877.40 1021.64 1 4 14 13 826.251 419.668 1 -4 15 13 1042.31 389.932 1 -3 15 13 1576.00 253.241 1 -2 15 13 845.353 290.468 1 -1 15 13 916.925 193.654 1 0 15 13 1021.69 263.294 1 1 15 13 823.826 188.579 1 2 15 13 1126.61 321.663 1 3 15 13 1148.06 276.578 1 -2 16 13 3568.31 428.634 1 -1 16 13 2476.47 319.108 1 0 16 13 3613.42 423.551 1 1 16 13 701.724 220.028 1 2 16 13 4725.23 951.176 1 -8 0 1419013.10 1699.11 1 -6 0 1427879.50 1461.53 1 -4 0 1416940.20 942.04 1 -2 0 14 4225.83 367.862 1 0 0 14 7533.09 588.821 1 2 0 14 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14 16 327.052 153.444 1 2 14 16 3462.65 488.665 1 3 14 16 914.083 457.605 1 -3 15 16 1056.41 424.001 1 -2 15 16 615.432 269.965 1 -1 15 16 207.02 195.757 1 0 15 16 1339.92 234.075 1 1 15 16 1976.69 348.154 1 2 15 16 1523.48 361.195 1 -9 0 17 4413.89 1316.45 1 -7 0 1713808.60 959.666 1 -5 0 17 2298.19 305.962 1 -3 0 17 7157.72 791.602 1 -1 0 17-151.863 161.561 1 1 0 17 2787.21 305.295 1 3 0 17 360.908 195.829 1 5 0 1718095.40 1264.19 1 7 0 17 2939.06 451.399 1 -8 1 17-100.969 373.647 1 -7 1 1712436.90 682.347 1 -6 1 17 3693.42 289.561 1 -5 1 17 7486.74 426.404 1 -4 1 17 6861.73 392.722 1 -3 1 1716334.40 758.557 1 -2 1 17 9088.91 501.859 1 -1 1 1733844.10 1780.05 1 0 1 17 4450.92 301.859 1 1 1 1743536.00 1889.11 1 2 1 17 364.035 118.82 1 3 1 1711169.80 726.179 1 4 1 17 6219.22 400.397 1 5 1 17 6621.83 600.944 1 6 1 17 2299.04 251.634 1 7 1 17 1752.15 287.752 1 8 1 17 273.454 268.656 1 -8 2 17 2107.71 428.607 1 -7 2 17 1059.81 288.702 1 -6 2 17 3640.85 298.509 1 -5 2 17 5920.69 351.852 1 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3434.23 659.509 1 -7 2 21 1104.83 337.289 1 -6 2 21 3514.44 416.786 1 -5 2 21 8838.99 654.19 1 -4 2 2113179.20 680.262 1 -3 2 2112411.30 628.716 1 -2 2 2110163.00 561.591 1 -1 2 21 2403.20 367.003 1 0 2 2110109.70 517.235 1 1 2 21 7744.02 423.582 1 2 2 21 7399.40 462.136 1 3 2 21 9272.00 996.347 1 4 2 21 6061.05 571.372 1 5 2 21 2907.70 314.446 1 6 2 21 2173.43 374.759 1 7 2 21 172.033 225.967 1 -8 3 21 3033.05 583.319 1 -7 3 21 232.756 308.869 1 -6 3 21 4111.00 564.424 1 -5 3 21 979.50 187.874 1 -4 3 21 1544.31 247.504 1 -3 3 21 621.119 179.00 1 -2 3 21 500.451 170.586 1 -1 3 21 164.716 146.888 1 0 3 21 58.9518 140.851 1 1 3 21-16.4583 121.292 1 2 3 21 3440.07 331.577 1 3 3 21 157.658 151.258 1 4 3 21 4339.95 721.797 1 5 3 21 244.941 168.355 1 6 3 21 3207.61 331.991 1 -8 4 21 4810.23 614.731 1 -7 4 21 236.156 323.18 1 -6 4 21 3612.57 645.25 1 -5 4 21 256.778 150.894 1 -4 4 21 9037.94 538.489 1 -3 4 21 1839.22 241.689 1 -2 4 2126952.20 2073.41 1 -1 4 21 1486.12 214.819 1 0 4 2118219.10 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7 21 986.613 176.415 1 -1 7 21 50.5758 140.562 1 0 7 21 273.378 155.50 1 1 7 21 706.694 163.201 1 2 7 21 521.308 162.486 1 3 7 21 2030.97 254.037 1 4 7 21 106.334 146.166 1 5 7 21 4757.25 820.803 1 6 7 21 345.975 339.896 1 -6 8 21 407.407 320.968 1 -5 8 21 3052.98 669.407 1 -4 8 21 926.153 237.603 1 -3 8 21 7461.94 626.563 1 -2 8 21 2669.03 391.853 1 -1 8 2115585.30 1676.10 1 0 8 21 3075.30 265.295 1 1 8 2111971.90 600.986 1 2 8 21 4339.88 313.055 1 3 8 21 6562.83 443.518 1 4 8 21 2407.96 301.503 1 5 8 21 1657.14 383.784 1 -6 9 21 1531.87 427.107 1 -5 9 21 928.652 344.39 1 -4 9 21 423.772 268.753 1 -3 9 21 634.241 207.762 1 -2 9 21 892.866 234.033 1 -1 9 21 402.702 212.664 1 0 9 21 94.199 186.721 1 1 9 21 1774.90 277.334 1 2 9 21 1535.75 265.872 1 3 9 21 179.352 166.542 1 4 9 21 3119.42 478.201 1 5 9 21 439.66 332.886 1 -6 10 21 6006.25 842.37 1 -5 10 21 139.147 283.245 1 -4 10 21 9215.23 2092.60 1 -3 10 21 19.3608 198.574 1 -2 10 21 4542.05 522.128 1 -1 10 21 130.104 183.172 1 0 10 21 5493.25 562.723 1 1 10 21 288.825 196.787 1 2 10 2110979.30 800.772 1 3 10 21 300.913 150.232 1 4 10 21 5472.88 488.858 1 -5 11 21 1667.81 438.064 1 -4 11 21 728.984 426.496 1 -3 11 21 518.572 264.396 1 -2 11 21 373.324 241.915 1 -1 11 21 228.874 203.665 1 0 11 21 96.7092 191.312 1 1 11 21 714.746 223.545 1 2 11 21 2385.44 285.191 1 3 11 21 385.001 272.43 1 4 11 21 2106.94 394.527 1 -4 12 21 933.081 387.707 1 -3 12 21 2596.76 828.576 1 -2 12 21 2513.99 427.257 1 -1 12 21 2607.43 329.977 1 0 12 21 4087.71 463.489 1 1 12 21 4430.76 471.111 1 2 12 21 6320.13 755.528 1 3 12 21 1998.87 415.857 1 -3 13 21 691.532 298.54 1 -2 13 21 1170.18 274.283 1 -1 13 21 238.864 193.172 1 0 13 21 1253.14 294.881 1 1 13 21-91.2192 160.802 1 2 13 21-118.388 237.994 1 -1 14 21 1530.26 385.368 1 0 14 21 410.914 210.673 1 -8 0 22 2770.04 617.532 1 -6 0 22 2091.77 431.422 1 -4 0 22 6884.65 965.602 1 -2 0 22 5940.22 593.411 1 0 0 22 1879.69 279.667 1 2 0 22-105.818 142.213 1 4 0 22 6759.88 634.372 1 6 0 22 1538.27 438.533 1 -8 1 22 1950.20 471.994 1 -7 1 22 1092.65 297.961 1 -6 1 22 4567.77 504.233 1 -5 1 22 540.943 171.965 1 -4 1 22 5049.10 352.608 1 -3 1 22 1031.30 192.189 1 -2 1 22 4059.27 505.854 1 -1 1 22 2738.90 295.598 1 0 1 2216189.60 785.456 1 1 1 22 2622.27 244.938 1 2 1 2213251.90 947.885 1 3 1 22 3228.02 236.278 1 4 1 22 8763.71 545.297 1 5 1 22 1675.25 269.461 1 6 1 22 3832.53 404.616 1 -8 2 22 4130.64 740.884 1 -7 2 22 5767.45 1180.72 1 -6 2 22 3455.12 384.136 1 -5 2 22 3030.16 360.12 1 -4 2 22 805.568 191.796 1 -3 2 22 64.5056 149.807 1 -2 2 22 382.494 172.635 1 -1 2 22 321.75 160.692 1 0 2 22 534.836 155.235 1 1 2 22-109.089 126.566 1 2 2 22-27.3907 135.047 1 3 2 22-129.557 158.212 1 4 2 22 346.249 167.946 1 5 2 22 1352.11 232.592 1 6 2 22 804.596 232.88 1 -7 3 22 2275.66 501.486 1 -6 3 22 327.003 216.988 1 -5 3 22 3764.49 357.185 1 -4 3 22 241.53 164.123 1 -3 3 2214947.30 710.545 1 -2 3 22 105.896 151.306 1 -1 3 2216189.30 1874.44 1 0 3 22 1304.34 200.846 1 1 3 2212321.10 598.287 1 2 3 22 3018.07 251.077 1 3 3 22 7966.50 496.808 1 4 3 22 509.397 153.756 1 5 3 22 5982.88 638.501 1 6 3 22-135.339 208.119 1 -7 4 22 2379.18 493.79 1 -6 4 22 396.553 274.964 1 -5 4 22 3818.29 444.215 1 -4 4 22 185.776 165.447 1 -3 4 22 9167.86 532.648 1 -2 4 22 93.0461 204.041 1 -1 4 22 5191.62 597.434 1 0 4 22 303.988 158.454 1 1 4 22 1210.72 181.01 1 2 4 22 873.014 174.079 1 3 4 22 5993.43 612.263 1 4 4 22 1248.49 211.933 1 5 4 22 3266.61 285.445 1 6 4 22 413.899 285.863 1 -7 5 22 36.1207 361.265 1 -6 5 22-31.9688 297.076 1 -5 5 22 2555.92 471.722 1 -4 5 22 843.028 195.128 1 -3 5 22 7722.27 461.728 1 -2 5 22 8373.42 984.091 1 -1 5 22 5336.62 896.043 1 0 5 22 473.245 200.594 1 1 5 22 4542.24 383.296 1 2 5 22 2662.25 244.087 1 3 5 22 3383.42 345.646 1 4 5 22 4141.57 378.075 1 5 5 22 4176.48 429.54 1 6 5 22 5652.33 388.821 1 -7 6 22 1346.84 486.603 1 -6 6 22 8358.90 1042.03 1 -5 6 22 1202.61 357.615 1 -4 6 22 377.249 199.516 1 -3 6 22 1606.93 231.452 1 -2 6 22 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383.116 1 0 9 22 2211.06 261.607 1 1 9 22 8916.64 843.007 1 2 9 22 4231.10 392.116 1 3 9 22 6233.63 693.444 1 4 9 22 3022.99 559.265 1 5 9 22 5389.29 991.368 1 -5 10 22 4071.55 966.553 1 -4 10 22 220.92 362.989 1 -3 10 22 895.382 293.583 1 -2 10 22 461.683 248.575 1 -1 10 22 169.492 189.058 1 0 10 22 420.029 208.814 1 1 10 22 185.353 187.621 1 2 10 22 136.134 266.605 1 3 10 22 247.645 172.898 1 4 10 22 417.251 400.724 1 -5 11 22 1496.02 487.304 1 -4 11 22 579.495 312.344 1 -3 11 22 5678.80 768.874 1 -2 11 22 92.4622 207.768 1 -1 11 22 4306.10 397.149 1 0 11 22 1119.90 265.573 1 1 11 22 7316.14 860.446 1 2 11 22 274.102 224.92 1 3 11 2210309.60 883.206 1 -4 12 22 1627.41 570.196 1 -3 12 22 3034.89 643.159 1 -2 12 22 1011.80 283.325 1 -1 12 22 551.228 240.515 1 0 12 22 506.875 242.573 1 1 12 22 292.602 203.412 1 2 12 22 168.493 210.099 1 3 12 22 1376.82 793.316 1 -3 13 22 663.066 304.176 1 -2 13 22 3012.22 529.031 1 -1 13 22 57.0575 196.242 1 0 13 22 5504.60 443.40 1 1 13 22 523.548 191.533 1 -7 0 23 1606.23 470.556 1 -5 0 23 992.399 279.059 1 -3 0 23 1032.55 280.559 1 -1 0 23 7857.36 634.591 1 1 0 2336141.80 2439.58 1 3 0 2313785.00 1050.76 1 5 0 23 6926.44 740.567 1 -7 1 23 7356.28 623.218 1 -6 1 23 2168.83 331.433 1 -5 1 23 9256.22 1090.72 1 -4 1 23 6389.26 521.987 1 -3 1 23 1093.98 208.069 1 -2 1 23 743.42 174.766 1 -1 1 23 1312.99 223.139 1 0 1 23 575.885 151.862 1 1 1 23 5932.77 393.889 1 2 1 23 340.645 123.723 1 3 1 23 36.7933 109.671 1 4 1 23 308.484 167.207 1 5 1 23 836.538 224.442 1 6 1 23 275.40 259.772 1 -7 2 23-63.5258 263.595 1 -6 2 23 1636.48 297.613 1 -5 2 23 1631.73 263.244 1 -4 2 23 2778.11 278.086 1 -3 2 23 1985.48 267.687 1 -2 2 23 2342.06 469.379 1 -1 2 23 7848.38 492.293 1 0 2 2311597.00 639.504 1 1 2 23 3448.76 295.828 1 2 2 23 2972.85 289.545 1 3 2 23 3377.59 449.91 1 4 2 23 5868.72 492.989 1 5 2 23 4076.54 563.293 1 6 2 23 8005.01 695.119 1 -7 3 23 239.909 288.881 1 -6 3 23 6549.16 815.936 1 -5 3 23 719.728 227.004 1 -4 3 2311942.90 659.117 1 -3 3 23 1155.18 211.92 1 -2 3 23 2304.08 350.767 1 -1 3 23 588.984 221.277 1 0 3 23 1494.20 213.044 1 1 3 23 1245.40 192.158 1 2 3 23 771.935 164.576 1 3 3 23 746.111 209.35 1 4 3 23 21.8784 144.407 1 5 3 23 248.294 179.891 1 6 3 23 1031.78 277.161 1 -7 4 23 447.556 342.311 1 -6 4 23 826.945 327.185 1 -5 4 23 277.879 205.767 1 -4 4 23 409.745 166.093 1 -3 4 23 816.52 225.273 1 -2 4 23 7123.48 478.588 1 -1 4 23 322.113 174.213 1 0 4 2313885.20 1010.24 1 1 4 23 1435.42 209.16 1 2 4 23 9905.90 786.761 1 3 4 23-156.178 156.178 1 4 4 23 4147.63 710.298 1 5 4 23 1165.00 367.95 1 6 4 23 3059.28 771.796 1 -7 5 23 1295.43 437.804 1 -6 5 23 4970.77 660.67 1 -5 5 23 2410.18 534.85 1 -4 5 23 7638.43 444.619 1 -3 5 23 2540.39 276.569 1 -2 5 23 2240.17 273.199 1 -1 5 23 3785.93 361.441 1 0 5 23 1015.20 195.642 1 1 5 23-32.0532 143.927 1 2 5 23 2657.36 244.969 1 3 5 23 246.95 227.098 1 4 5 23 111.656 248.857 1 5 5 23 494.968 291.725 1 6 5 23 946.823 583.811 1 -7 6 23 207.386 391.788 1 -6 6 23 815.79 360.607 1 -5 6 23 1527.71 365.001 1 -4 6 23 1348.27 279.388 1 -3 6 23 9042.05 538.434 1 -2 6 23 1743.86 316.484 1 -1 6 23 6008.02 593.037 1 0 6 23 169.431 158.508 1 1 6 23 6475.43 467.122 1 2 6 23-103.842 161.389 1 3 6 23 3044.71 495.00 1 4 6 23 188.301 168.827 1 5 6 23 6867.09 685.764 1 -6 7 23 549.296 413.468 1 -5 7 23 5706.19 936.639 1 -4 7 23 396.58 281.395 1 -3 7 23 4214.41 513.557 1 -2 7 23 149.585 174.647 1 -1 7 23 2808.33 313.46 1 0 7 23 41.3086 153.363 1 1 7 23 1730.27 245.993 1 2 7 23 1267.41 230.347 1 3 7 23 153.447 205.301 1 4 7 23 8.5099 492.651 1 5 7 23 218.404 162.761 1 -6 8 23 420.036 379.589 1 -5 8 23 251.54 367.91 1 -4 8 23 1004.86 518.016 1 -3 8 23 1481.02 257.165 1 -2 8 23 1131.97 186.272 1 -1 8 23 2141.99 317.946 1 0 8 23 1684.84 233.901 1 1 8 2317298.30 1583.38 1 2 8 23 2669.22 301.604 1 3 8 23 6692.40 835.239 1 4 8 23 687.984 194.761 1 5 8 23 3555.76 491.733 1 -5 9 23 977.606 415.768 1 -4 9 23 3351.53 1444.19 1 -3 9 23 1625.37 301.106 1 -2 9 23 1841.90 333.987 1 -1 9 23 2277.08 307.324 1 0 9 23 1855.51 304.169 1 1 9 23 251.033 166.461 1 2 9 23 1345.39 292.727 1 3 9 23-38.7071 214.704 1 4 9 23 205.448 450.591 1 -5 10 23 641.347 334.84 1 -4 10 23 1215.44 474.324 1 -3 10 23 382.626 237.383 1 -2 10 23 2091.75 552.743 1 -1 10 23 212.509 184.219 1 0 10 23 3500.10 926.158 1 1 10 23 36.0244 191.099 1 2 10 23 4123.74 770.023 1 3 10 23-170.081 170.081 1 4 10 23 6138.04 1213.75 1 -4 11 23 2260.27 790.202 1 -3 11 23 24.4076 348.532 1 -2 11 23 2194.53 414.392 1 -1 11 23 -27.869 227.285 1 0 11 23 1901.05 290.477 1 1 11 23 987.557 262.624 1 2 11 23 61.5482 203.659 1 3 11 23 439.928 312.056 1 -3 12 23 1646.89 394.846 1 -2 12 23 357.432 252.663 1 -1 12 23 538.612 228.105 1 0 12 23 2869.95 374.139 1 1 12 23 3886.30 1057.74 1 2 12 23 6031.57 938.307 1 -2 13 23 987.113 284.921 1 -1 13 23 858.931 256.577 1 0 13 23 184.027 209.715 1 -6 0 24 6968.70 967.177 1 -4 0 2417979.50 2374.46 1 -2 0 24 6502.98 597.701 1 0 0 2413643.80 1104.88 1 2 0 24 1823.04 269.909 1 4 0 24 287.364 278.31 1 6 0 24 544.334 330.607 1 -7 1 24 248.968 264.035 1 -6 1 24-173.763 232.501 1 -5 1 24 160.777 216.476 1 -4 1 24 675.854 179.225 1 -3 1 24 171.613 153.534 1 -2 1 24 463.163 178.558 1 -1 1 24 5681.82 387.065 1 0 1 24 5189.81 370.976 1 1 1 2412308.30 753.251 1 2 1 24 9456.96 525.994 1 3 1 24 553.533 198.316 1 4 1 24 7376.32 553.165 1 5 1 24 342.20 200.752 1 6 1 24 5960.84 565.874 1 -7 2 24 5892.48 810.65 1 -6 2 24 3302.57 557.154 1 -5 2 24 6949.29 784.736 1 -4 2 24 5752.12 487.507 1 -3 2 24 5854.57 407.734 1 -2 2 24 297.148 175.587 1 -1 2 24 502.294 170.383 1 0 2 24 2024.65 251.443 1 1 2 24 2482.51 241.002 1 2 2 24 1036.95 175.446 1 3 2 24 2166.83 260.438 1 4 2 24 696.512 207.567 1 5 2 24 742.402 258.976 1 6 2 24 373.485 552.309 1 -7 3 24 480.838 321.936 1 -6 3 24 1418.01 299.529 1 -5 3 24 497.227 253.701 1 -4 3 24 1591.29 238.438 1 -3 3 24 771.587 184.899 1 -2 3 24 -1.9514 164.403 1 -1 3 24 1642.82 303.77 1 0 3 24 898.814 194.376 1 1 3 24 9027.19 661.012 1 2 3 24 186.03 147.522 1 3 3 24 5276.01 1131.04 1 4 3 24-28.9667 154.158 1 5 3 24 6159.08 557.815 1 6 3 24 44.8555 234.807 1 -7 4 24 4637.12 821.697 1 -6 4 24 478.904 280.316 1 -5 4 2411886.80 861.212 1 -4 4 24 855.069 212.055 1 -3 4 2411094.30 586.074 1 -2 4 24 867.439 213.144 1 -1 4 2410594.80 940.799 1 0 4 24 399.203 179.078 1 1 4 24 4706.73 351.717 1 2 4 24 163.28 149.594 1 3 4 24 569.424 188.749 1 4 4 24 105.637 307.269 1 5 4 24 286.332 223.482 1 -7 5 24-43.4505 375.099 1 -6 5 24 118.571 303.339 1 -5 5 24 313.172 294.256 1 -4 5 24 1626.08 273.234 1 -3 5 24 1343.67 229.428 1 -2 5 24 1221.85 230.054 1 -1 5 24 1489.72 220.269 1 0 5 24 9254.33 670.171 1 1 5 24 388.813 165.588 1 2 5 24 5648.91 475.762 1 3 5 24 1985.82 343.92 1 4 5 24 681.417 229.88 1 5 5 24 2907.48 448.012 1 -6 6 24 6590.03 974.509 1 -5 6 24 679.068 349.106 1 -4 6 24 4579.67 1212.79 1 -3 6 24 1095.38 242.427 1 -2 6 24 9245.48 1172.14 1 -1 6 24 1423.08 236.621 1 0 6 24 1803.63 257.416 1 1 6 24 327.739 173.327 1 2 6 24 5723.17 452.73 1 3 6 24 813.979 418.547 1 4 6 24 1056.67 225.06 1 5 6 24 131.261 340.106 1 -6 7 24-168.496 351.697 1 -5 7 24 2333.08 608.694 1 -4 7 24 974.267 342.227 1 -3 7 24 179.20 224.189 1 -2 7 24 167.236 191.353 1 -1 7 24 39.4108 180.104 1 0 7 24 2159.82 306.985 1 1 7 24 413.715 200.77 1 2 7 24 8948.26 562.472 1 3 7 24 639.118 297.073 1 4 7 24 6493.07 953.235 1 5 7 24-31.1518 215.396 1 -6 8 24 1102.40 473.078 1 -5 8 24 991.173 495.809 1 -4 8 24 4412.58 920.78 1 -3 8 24 1668.21 301.666 1 -2 8 24 3173.49 580.347 1 -1 8 24 1288.36 232.934 1 0 8 24 1917.47 325.315 1 1 8 24 257.396 242.201 1 2 8 24 3661.51 368.524 1 3 8 24 1346.38 214.871 1 4 8 24 314.67 187.933 1 -5 9 24-101.634 329.216 1 -4 9 24 421.055 448.879 1 -3 9 24 720.198 273.644 1 -2 9 24 568.548 234.153 1 -1 9 24 3312.20 376.485 1 0 9 24 244.091 169.558 1 1 9 24 8631.59 704.199 1 2 9 24 3240.59 361.423 1 3 9 24 4235.51 460.659 1 4 9 24 1845.11 323.865 1 -5 10 24 5792.45 2308.28 1 -4 10 24 236.713 327.176 1 -3 10 24 3577.23 1001.04 1 -2 10 24 170.502 236.519 1 -1 10 24 4086.88 619.723 1 0 10 24-208.516 208.516 1 1 10 24 3409.49 494.288 1 2 10 24 470.577 357.49 1 3 10 24 3132.91 593.336 1 -4 11 24 835.065 361.814 1 -3 11 24 657.177 290.856 1 -2 11 24 288.516 254.637 1 -1 11 24 286.817 245.341 1 0 11 24 213.223 295.47 1 1 11 24 4273.32 599.62 1 2 11 24 764.379 251.984 1 -3 12 24 1203.52 364.372 1 -2 12 24 1565.57 306.293 1 -1 12 24 2496.98 492.169 1 0 12 24 2764.78 353.221 1 1 12 24 2552.16 375.436 1 -7 0 25 2155.40 581.124 1 -5 0 25 681.314 356.593 1 -3 0 25 48.9756 218.038 1 -1 0 25 518.038 214.658 1 1 0 25 9168.91 754.083 1 3 0 25 9939.50 1631.70 1 5 0 25 2324.91 573.231 1 -7 1 25 4285.19 776.968 1 -6 1 25 293.865 241.524 1 -5 1 25 4961.14 630.395 1 -4 1 25 3344.27 462.411 1 -3 1 25 6203.17 448.781 1 -2 1 25 4755.52 385.996 1 -1 1 2515570.20 745.184 1 0 1 25 2880.12 264.096 1 1 1 2511568.70 567.224 1 2 1 25 396.717 131.037 1 3 1 25 7382.41 1206.90 1 4 1 25 833.929 245.241 1 5 1 25 4631.15 447.808 1 -7 2 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514.534 1 -5 5 25 1197.32 399.725 1 -4 5 25 3202.66 455.965 1 -3 5 2510748.80 620.287 1 -2 5 25 4127.31 443.48 1 -1 5 25 6753.70 620.462 1 0 5 25 7487.90 475.353 1 1 5 25 1410.76 207.548 1 2 5 25 4663.35 391.255 1 3 5 25 979.247 233.479 1 4 5 25 3569.30 415.379 1 5 5 25 642.816 307.806 1 -6 6 25 808.695 460.265 1 -5 6 25 231.131 361.974 1 -4 6 25-37.5695 319.289 1 -3 6 25 184.068 204.856 1 -2 6 25 104.691 226.35 1 -1 6 25 238.739 190.358 1 0 6 25 279.99 196.594 1 1 6 25 678.064 195.708 1 2 6 25 323.713 184.498 1 3 6 25 1828.73 290.081 1 4 6 25 774.879 248.492 1 5 6 25 2860.20 514.904 1 -6 7 25 288.693 419.37 1 -5 7 25 6077.99 744.77 1 -4 7 25-47.8097 283.917 1 -3 7 25 9767.05 675.672 1 -2 7 25 65.746 199.578 1 -1 7 25 7748.84 903.624 1 0 7 25 107.053 196.714 1 1 7 25 5814.64 485.021 1 2 7 25 722.601 211.234 1 3 7 25 3148.01 494.839 1 4 7 25 205.767 225.64 1 -5 8 25 1459.31 462.188 1 -4 8 25-444.276 470.678 1 -3 8 25-12.4122 272.953 1 -2 8 25 171.322 202.155 1 -1 8 25 913.846 262.301 1 0 8 25 223.984 186.691 1 1 8 25 856.762 294.916 1 2 8 25 2137.54 415.848 1 3 8 25 649.602 223.493 1 4 8 25 689.061 213.369 1 -5 9 25 336.891 385.947 1 -4 9 25 6791.83 1285.66 1 -3 9 25 242.289 404.007 1 -2 9 25 9019.11 676.677 1 -1 9 25 466.403 196.199 1 0 9 25 3540.13 699.961 1 1 9 25 2754.42 418.261 1 2 9 25 3937.17 439.518 1 3 9 25 827.536 304.134 1 -4 10 25-165.322 351.655 1 -3 10 25 516.252 357.749 1 -2 10 25-44.7752 227.064 1 -1 10 25 90.5749 225.085 1 0 10 25-26.0534 211.088 1 1 10 25 1137.47 259.848 1 2 10 25 2152.86 352.448 1 3 10 25 93.5247 287.728 1 -3 11 25 309.096 367.251 1 -2 11 25 2713.29 536.762 1 -1 11 25 171.226 229.675 1 0 11 25 3062.15 819.592 1 1 11 25-234.671 234.671 1 2 11 25 3505.96 584.082 1 -2 12 25 536.532 532.034 1 -1 12 25 455.238 279.766 1 0 12 25 365.152 266.921 1 -6 0 26 3109.38 868.164 1 -4 0 26 6934.54 1391.19 1 -2 0 2617904.90 1226.64 1 0 0 2613397.90 892.367 1 2 0 26 8924.90 827.277 1 4 0 26 9964.40 1219.08 1 -7 1 26 364.317 300.938 1 -6 1 26 2605.58 583.737 1 -5 1 26 559.143 267.44 1 -4 1 26 1399.41 238.861 1 -3 1 26 168.324 165.242 1 -2 1 26 126.378 158.855 1 -1 1 26 116.283 152.378 1 0 1 26 1026.78 168.394 1 1 1 26 143.912 206.52 1 2 1 26 1578.56 193.255 1 3 1 26 1667.36 238.532 1 4 1 26 1087.38 258.427 1 5 1 26 783.482 289.178 1 -6 2 26 1304.54 369.076 1 -5 2 26 2651.07 394.332 1 -4 2 26 2444.25 334.619 1 -3 2 26 7365.32 510.665 1 -2 2 26 4123.09 343.649 1 -1 2 26 9015.30 667.538 1 0 2 26 6540.48 432.646 1 1 2 2611718.90 643.536 1 2 2 26 2689.20 267.197 1 3 2 26 5304.41 653.216 1 4 2 26 3390.41 478.161 1 5 2 26 4668.35 558.855 1 -6 3 26 331.424 262.238 1 -5 3 26 2029.72 559.05 1 -4 3 26 17.8395 233.913 1 -3 3 26 255.02 205.966 1 -2 3 26 470.181 193.344 1 -1 3 26 990.001 200.014 1 0 3 26 132.932 159.12 1 1 3 26 307.504 157.684 1 2 3 26 561.63 178.512 1 3 3 26 860.949 232.376 1 4 3 26 284.585 381.752 1 5 3 26 1248.95 576.202 1 -6 4 26 680.229 292.608 1 -5 4 26 8428.40 736.423 1 -4 4 26 6.473 205.33 1 -3 4 2610334.20 687.693 1 -2 4 26 1116.86 219.446 1 -1 4 2617082.90 1123.37 1 0 4 26 1730.01 232.883 1 1 4 26 9024.16 519.759 1 2 4 26 414.482 174.126 1 3 4 26 3131.70 554.101 1 4 4 26 203.657 278.64 1 5 4 26 6425.94 1301.52 1 -6 5 26 2148.94 444.54 1 -5 5 26 432.743 271.008 1 -4 5 26 1163.99 283.047 1 -3 5 26-58.2235 249.466 1 -2 5 26 524.552 226.29 1 -1 5 26-31.5381 173.31 1 0 5 26-107.149 199.504 1 1 5 26 111.423 178.212 1 2 5 26 227.998 177.514 1 3 5 26 78.4292 195.542 1 4 5 26 1088.77 287.812 1 -6 6 26 914.617 625.407 1 -5 6 26-151.126 290.206 1 -4 6 26 1555.37 660.166 1 -3 6 26-210.073 210.073 1 -2 6 26 7449.57 866.499 1 -1 6 26 869.62 234.764 1 0 6 2610352.20 1099.92 1 1 6 26 2302.24 279.733 1 2 6 26 5041.18 382.62 1 3 6 26 482.543 238.967 1 4 6 26 3258.47 416.927 1 -5 7 26 65.6282 395.351 1 -4 7 26 1309.07 404.29 1 -3 7 26 300.158 383.489 1 -2 7 26 1534.34 299.773 1 -1 7 26 339.839 328.299 1 0 7 26 120.79 204.046 1 1 7 26 87.3681 206.44 1 2 7 26 163.427 206.301 1 3 7 26 345.437 235.421 1 4 7 26 1047.59 243.083 1 -5 8 26 1131.43 449.526 1 -4 8 26 5872.56 973.716 1 -3 8 26 1181.62 394.661 1 -2 8 26 4440.22 450.102 1 -1 8 26 1558.56 299.355 1 0 8 26 3986.12 489.263 1 1 8 26 982.803 246.332 1 2 8 26 1156.81 244.124 1 3 8 26 1132.78 262.75 1 -4 9 26 161.595 428.719 1 -3 9 26 962.055 403.346 1 -2 9 26 279.315 236.401 1 -1 9 26 275.298 235.455 1 0 9 26-78.6256 214.974 1 1 9 26 544.721 293.466 1 2 9 26 215.392 230.917 1 3 9 26 528.651 280.392 1 -3 10 26 3591.33 735.675 1 -2 10 26-4.10182 243.805 1 -1 10 26 2346.08 506.258 1 0 10 26 13.8972 203.737 1 1 10 26 9832.38 1158.48 1 2 10 26 479.599 288.185 1 -2 11 26 425.563 380.334 1 -1 11 26 -220.56 220.56 1 0 11 26 174.74 251.353 1 1 11 26 123.616 229.251 1 -5 0 27 9759.79 1127.59 1 -3 0 27 8906.21 964.175 1 -1 0 27 1435.76 321.149 1 1 0 27-113.033 171.999 1 3 0 27 389.429 316.987 1 5 0 27 185.732 309.922 1 -6 1 27 211.123 315.917 1 -5 1 27 2120.47 406.823 1 -4 1 27 173.771 206.593 1 -3 1 27 1791.20 289.215 1 -2 1 27 1325.05 207.342 1 -1 1 27 4703.57 354.361 1 0 1 27 3972.14 318.621 1 1 1 27 5174.29 586.085 1 2 1 27 1223.87 184.935 1 3 1 27 4115.77 546.059 1 4 1 27 1966.71 321.733 1 5 1 27 3581.05 596.837 1 -6 2 27 1827.72 402.699 1 -5 2 27 1733.06 417.503 1 -4 2 27 1571.75 304.115 1 -3 2 27 569.149 224.50 1 -2 2 27 7839.76 473.755 1 -1 2 27 3051.38 323.77 1 0 2 27 5274.95 442.282 1 1 2 27 714.616 197.08 1 2 2 27 1398.71 194.909 1 3 2 27 47.1176 146.862 1 4 2 27 52.8016 212.893 1 5 2 27 648.125 337.367 1 -6 3 27 326.852 260.329 1 -5 3 27 74.9828 260.572 1 -4 3 27 1511.88 370.162 1 -3 3 27 348.589 224.763 1 -2 3 27 5261.09 554.745 1 -1 3 27 211.696 171.935 1 0 3 2712212.60 655.784 1 1 3 27-60.1482 151.213 1 2 3 27 5179.05 474.435 1 3 3 27 290.225 174.042 1 4 3 27 4073.56 891.902 1 -6 4 27 4677.10 581.974 1 -5 4 27-122.872 250.358 1 -4 4 27 4548.60 769.676 1 -3 4 27-13.9326 231.629 1 -2 4 27 2606.67 377.972 1 -1 4 27 249.521 258.193 1 0 4 27 1709.73 248.144 1 1 4 27 603.477 213.549 1 2 4 27 64.5294 178.789 1 3 4 27 39.8843 337.976 1 4 4 27-53.8597 191.334 1 -6 5 27 474.245 338.253 1 -5 5 27 377.053 281.786 1 -4 5 27 1176.14 295.622 1 -3 5 27 1602.48 336.009 1 -2 5 27 1896.56 309.972 1 -1 5 27 2267.98 410.951 1 0 5 27 5107.84 428.852 1 1 5 27 4497.74 423.094 1 2 5 27 2904.42 386.258 1 3 5 27 1563.67 359.955 1 4 5 27 2704.60 435.873 1 -5 6 27 2302.45 519.787 1 -4 6 27-18.3267 330.434 1 -3 6 27 696.639 263.546 1 -2 6 27 117.581 355.986 1 -1 6 27 3036.79 356.964 1 0 6 27 1190.25 247.76 1 1 6 27 3140.92 318.438 1 2 6 27-46.1063 213.275 1 3 6 27 94.4185 219.946 1 4 6 27 137.802 327.061 1 -5 7 27 849.891 446.428 1 -4 7 27 627.273 408.853 1 -3 7 27 3905.92 535.87 1 -2 7 27 55.6552 248.543 1 -1 7 27 4731.31 447.515 1 0 7 27 114.704 214.221 1 1 7 27 6851.38 527.957 1 2 7 27-178.458 178.458 1 3 7 27 4448.44 548.518 1 -4 8 27-173.892 459.119 1 -3 8 27 2235.90 435.059 1 -2 8 27 239.446 217.616 1 -1 8 27 506.655 249.482 1 0 8 27 103.428 212.805 1 1 8 27 139.385 206.188 1 2 8 27 226.894 202.924 1 3 8 27 99.6529 220.543 1 -4 9 27 1075.12 459.289 1 -3 9 27 1186.96 463.257 1 -2 9 27 2066.82 297.601 1 -1 9 27 516.764 265.631 1 0 9 27 5986.70 744.79 1 1 9 27 2549.22 350.974 1 2 9 27 4741.60 526.652 1 -3 10 27 804.409 450.982 1 -2 10 27 1393.55 864.249 1 -1 10 27 -111.88 273.076 1 0 10 27 1035.99 299.438 1 1 10 27 63.159 386.073 1 -6 0 28-317.599 317.599 1 -4 0 28 16.5217 339.017 1 -2 0 28 964.784 325.01 1 0 0 28 4015.83 455.868 1 2 0 28 4668.90 456.751 1 4 0 28 2215.77 526.508 1 -6 1 28 5996.84 703.972 1 -5 1 28 1049.01 298.174 1 -4 1 28 7117.14 686.283 1 -3 1 28 363.623 212.104 1 -2 1 28 8855.20 570.66 1 -1 1 28 561.041 169.284 1 0 1 28 3621.21 298.495 1 1 1 28 310.306 222.791 1 2 1 28 1103.82 182.436 1 3 1 28 538.653 142.123 1 4 1 28 298.852 258.002 1 -6 2 28 265.679 274.682 1 -5 2 28 301.613 245.288 1 -4 2 28 4.2313 263.438 1 -3 2 28-15.3753 196.912 1 -2 2 28 838.308 229.696 1 -1 2 28 2293.20 274.492 1 0 2 28 2147.77 233.613 1 1 2 28 5522.23 367.922 1 2 2 28 2144.66 355.015 1 3 2 28 3753.27 574.662 1 4 2 28 2448.83 478.431 1 -6 3 28 452.701 301.605 1 -5 3 28 4684.61 507.266 1 -4 3 28 134.262 276.678 1 -3 3 28 4180.14 555.713 1 -2 3 28-174.699 185.599 1 -1 3 2811323.00 819.995 1 0 3 28 108.08 243.409 1 1 3 28 3339.25 405.20 1 2 3 28 109.577 186.982 1 3 3 28 1326.93 290.40 1 4 3 28 669.886 471.417 1 -5 4 28 126.126 254.814 1 -4 4 28 332.627 311.154 1 -3 4 28 891.345 267.845 1 -2 4 28-118.361 197.69 1 -1 4 28 8357.10 560.153 1 0 4 28 567.638 206.649 1 1 4 28 4077.02 503.463 1 2 4 28 31.9043 183.272 1 3 4 28 2808.62 413.41 1 4 4 28 291.718 168.022 1 -5 5 28 1548.92 351.67 1 -4 5 28 3806.81 444.313 1 -3 5 28 3542.12 420.27 1 -2 5 28 863.079 242.639 1 -1 5 28 3216.41 434.112 1 0 5 28 836.831 258.95 1 1 5 28 454.099 231.979 1 2 5 28 2802.54 359.625 1 3 5 28-30.9674 218.944 1 4 5 28 944.069 376.761 1 -5 6 28-20.4897 359.84 1 -4 6 28-132.029 320.007 1 -3 6 28 92.6611 294.365 1 -2 6 28 449.15 259.557 1 -1 6 28-41.2033 261.967 1 0 6 28 3332.79 454.707 1 1 6 28 1437.25 269.338 1 2 6 28 2471.73 364.549 1 3 6 28 1576.02 297.88 1 -4 7 28 5353.52 709.468 1 -3 7 28 529.323 261.157 1 -2 7 28 5291.33 940.57 1 -1 7 28 81.9577 241.973 1 0 7 28 2283.99 374.691 1 1 7 28 403.052 226.717 1 2 7 28 1035.36 280.969 1 3 7 28-27.2406 240.017 1 -4 8 28 1268.55 417.312 1 -3 8 28 1137.57 707.72 1 -2 8 28 1780.42 364.003 1 -1 8 28 1233.74 278.918 1 0 8 28 1961.83 373.323 1 1 8 28 524.377 250.726 1 2 8 28 207.199 218.986 1 -3 9 28 1663.64 509.108 1 -2 9 28 2174.96 328.291 1 -1 9 28 207.258 238.128 1 0 9 28 1173.89 322.057 1 1 9 28 1623.35 312.897 1 -1 10 28 661.371 283.288 1 0 10 28-151.732 312.187 1 -5 0 29 6493.69 1301.56 1 -3 0 29 8026.66 872.505 1 -1 0 29 5095.05 603.763 1 1 0 29 3166.51 651.762 1 3 0 29 3170.91 1053.24 1 -5 1 29-35.7244 252.606 1 -4 1 29 538.82 325.454 1 -3 1 29 133.641 200.205 1 -2 1 29 513.293 241.991 1 -1 1 29-166.252 166.252 1 0 1 29 411.331 168.98 1 1 1 29 1486.47 224.577 1 2 1 29 257.851 159.679 1 3 1 29 1177.99 210.456 1 4 1 29-151.691 238.809 1 -5 2 29 1706.63 361.567 1 -4 2 29 5238.85 571.474 1 -3 2 29 1153.39 254.477 1 -2 2 29 5233.89 455.268 1 -1 2 29 2299.66 278.871 1 0 2 29 2393.64 266.889 1 1 2 29 1062.88 217.854 1 2 2 29 2240.51 241.924 1 3 2 29 1306.65 219.263 1 4 2 29 1434.09 331.808 1 -5 3 29 518.32 291.115 1 -4 3 29 319.167 262.462 1 -3 3 29 453.661 269.63 1 -2 3 29 63.5515 213.306 1 -1 3 29 204.361 189.818 1 0 3 29 2244.31 355.105 1 1 3 29 530.756 228.442 1 2 3 29 2892.63 387.806 1 3 3 29 177.765 177.105 1 4 3 29 1430.93 405.527 1 -5 4 29 65.3722 256.682 1 -4 4 29 3219.51 885.989 1 -3 4 29 355.67 240.851 1 -2 4 29 4799.24 715.44 1 -1 4 29 254.683 235.096 1 0 4 29 3697.94 498.731 1 1 4 29 387.601 216.744 1 2 4 29 3638.80 439.378 1 3 4 29 406.828 239.416 1 -5 5 29 494.344 234.031 1 -4 5 29 238.675 279.495 1 -3 5 29-187.969 258.282 1 -2 5 29 61.8833 242.85 1 -1 5 29-169.028 217.312 1 0 5 29 994.641 264.486 1 1 5 29 513.015 251.736 1 2 5 29 1540.65 255.431 1 3 5 29 105.725 316.847 1 -4 6 29 352.611 339.183 1 -3 6 29 5185.80 576.947 1 -2 6 29 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