data_s-cu4au8 _audit_creation_date 2022-02-04 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2016/6' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C144 H96 Au8 Cu4 N6 P6 S6' _chemical_formula_sum 'C144 H96 Au8 Cu4 N6 P6 S6' _chemical_formula_weight 4118.33 _chemical_absolute_configuration S _chemical_melting_point ? _chemical_oxdiff_usercomment ' ' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Au' 'Au' -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 4 _space_group_name_H-M_alt 'P 1 21 1' _space_group_name_Hall 'P 2yb' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 16.6336(2) _cell_length_b 26.8950(3) _cell_length_c 31.7629(4) _cell_angle_alpha 90 _cell_angle_beta 91.3460(10) _cell_angle_gamma 90 _cell_volume 14205.6(3) _cell_formula_units_Z 4 _cell_measurement_reflns_used 35038 _cell_measurement_temperature 200.00(10) _cell_measurement_theta_max 73.8060 _cell_measurement_theta_min 2.6370 _shelx_estimated_absorpt_T_max 0.227 _shelx_estimated_absorpt_T_min 0.127 _exptl_absorpt_coefficient_mu 17.577 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.53081 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.7b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour black _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 1.926 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 7744 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.12 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0688 _diffrn_reflns_av_unetI/netI 0.0908 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.978 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 32 _diffrn_reflns_limit_k_min -33 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -39 _diffrn_reflns_number 123404 _diffrn_reflns_point_group_measured_fraction_full 0.960 _diffrn_reflns_point_group_measured_fraction_max 0.923 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.127 _diffrn_reflns_theta_min 2.657 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 200.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.978 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -19.00 89.00 0.50 0.50 -- 0.00 38.00 120.00 216 2 \w -89.00 19.00 0.50 0.50 -- 0.00 -38.00 120.00 216 3 \w 59.00 128.00 0.50 5.20 -- 95.20 -82.00-120.00 138 4 \w 75.00 180.00 0.50 5.20 -- 95.20 45.00 30.00 210 5 \w 42.00 109.00 0.50 5.20 -- 95.20 -82.00 150.00 134 6 \w 70.00 185.00 0.50 5.20 -- 95.20 15.00 -30.00 230 7 \w 38.00 118.00 0.50 5.20 -- 95.20 -82.00 30.00 160 8 \w 6.00 34.00 0.50 5.20 -- 95.20 -82.00 30.00 56 9 \w 7.00 98.00 0.50 5.20 -- 95.20 -61.00 150.00 182 10 \w 6.00 106.00 0.50 5.20 -- 95.20 -61.00 30.00 200 11 \w 15.00 120.00 0.50 5.20 -- 95.20 -61.00-120.00 210 12 \w 6.00 35.00 0.50 5.20 -- 95.20 -82.00-120.00 58 13 \w 6.00 123.00 0.50 5.20 -- 95.20 -15.00 60.00 234 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Pro: Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0308744000 _diffrn_orient_matrix_UB_12 -0.0329750000 _diffrn_orient_matrix_UB_13 0.0365808000 _diffrn_orient_matrix_UB_21 -0.0524644000 _diffrn_orient_matrix_UB_22 0.0292362000 _diffrn_orient_matrix_UB_23 0.0307358000 _diffrn_orient_matrix_UB_31 -0.0698207000 _diffrn_orient_matrix_UB_32 -0.0365968000 _diffrn_orient_matrix_UB_33 -0.0084450000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _reflns_Friedel_coverage 0.845 _reflns_Friedel_fraction_full 0.921 _reflns_Friedel_fraction_max 0.865 _reflns_number_gt 42412 _reflns_number_total 53322 _reflns_odcompleteness_completeness 99.82 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.7b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.7b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.7b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 5.749 _refine_diff_density_min -2.520 _refine_diff_density_rms 0.369 _refine_ls_abs_structure_details ; Flack x determined using 15378 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.019(7) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 3121 _refine_ls_number_reflns 53322 _refine_ls_number_restraints 651 _refine_ls_R_factor_all 0.0994 _refine_ls_R_factor_gt 0.0808 _refine_ls_restrained_S_all 1.038 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1293P)^2^+148.5341P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2088 _refine_ls_wR_factor_ref 0.2239 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2. Restrained distances C4-N2 1.13 with sigma of 0.01 C62-C57 = C62-C61 = C61-C60 = C60-C59 = C59-C58 = C58-C57 1.39 with sigma of 0.01 C24-C19 = C20-C19 = C21-C20 = C22-C21 = C23-C22 = C24-C23 1.39 with sigma of 0.01 C211-C210 = C210-C209 = C208-C207 = C212-C207 = C212-C211 = C209-C208 1.39 with sigma of 0.01 C29-C28 = C30-C29 = C31-C30 = C32-C31 = C33-C32 = C33-C28 1.39 with sigma of 0.01 C136-C135 = C137-C136 = C138-C137 = C138-C133 = C134-C133 = C135-C134 1.39 with sigma of 0.01 C29-C28 = C30-C29 = C31-C30 = C32-C31 = C33-C32 = C33-C28 = C28-C27 = C27-C26 = C26-C25 = C34-C25 = C34-C33 1.39 with sigma of 0.01 C238-C237 = C237-C236 = C236-C235 = C235-C234 = C234-C233 = C238-C233 1.39 with sigma of 0.01 C79-C78 1.5 with sigma of 0.02 C123-C122 1.5 with sigma of 0.02 C15-C14 = C14-C13 = C18-C13 = C18-C17 = C17-C16 = C16-C15 1.39 with sigma of 0.01 3. Rigid bond restraints C13, C14, C15, C16, C17, C18 with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005 4. Uiso/Uaniso restraints and constraints Uanis(C50) \\sim Ueq, Uanis(C48) \\sim Ueq, Uanis(C31) \\sim Ueq, Uanis(C286) \\sim Ueq, Uanis(N2) \\sim Ueq, Uanis(C144) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C49) \\sim Ueq, Uanis(C240) \\sim Ueq, Uanis(C142) \\sim Ueq, Uanis(C47) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C143) \\sim Ueq, Uanis(C140) \\sim Ueq, Uanis(C141) \\sim Ueq, Uanis(C67) \\sim Ueq, Uanis(C119) \\sim Ueq, Uanis(C133) \\sim Ueq, Uanis(C134) \\sim Ueq, Uanis(C136) \\sim Ueq, Uanis(C137) \\sim Ueq, Uanis(C135) \\sim Ueq, Uanis(C111) \\sim Ueq, Uanis(C110) \\sim Ueq, Uanis(C26) \\sim Ueq, Uanis(C27) \\sim Ueq, Uanis(C25) \\sim Ueq, Uanis(C28) \\sim Ueq, Uanis(C30) \\sim Ueq, Uanis(C32) \\sim Ueq, Uanis(C45) \\sim Ueq, Uanis(C46) \\sim Ueq, Uanis(C245) \\sim Ueq, Uanis(C237) \\sim Ueq, Uanis(C236) \\sim Ueq, Uanis(C238) \\sim Ueq, Uanis(C220) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C219) \\sim Ueq, Uanis(C217) \\sim Ueq, Uanis(C218) \\sim Ueq, Uanis(C221) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C227) \\sim Ueq, Uanis(C229) \\sim Ueq, Uanis(C4) \\sim Ueq, Uanis(C112) \\sim Ueq, Uanis(C53) \\sim Ueq, Uanis(C52) \\sim Ueq, Uanis(C183) \\sim Ueq, Uanis(C254) \\sim Ueq, Uanis(C255) \\sim Ueq, Uanis(C242) \\sim Ueq, Uanis(C244) \\sim Ueq, Uanis(C241) \\sim Ueq, Uanis(C197) \\sim Ueq, Uanis(C198) \\sim Ueq, Uanis(C199) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C198) \\sim Ueq, Uanis(C254) \\sim Ueq, Uanis(N11) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C9) \\sim Ueq, Uanis(N5) \\sim Ueq, Uanis(N4) \\sim Ueq, Uanis(C57) \\sim Ueq, Uanis(C60) \\sim Ueq, Uanis(C58) \\sim Ueq, Uanis(C59) \\sim Ueq, Uanis(C206) \\sim Ueq, Uanis(C209) \\sim Ueq, Uanis(C214) \\sim Ueq, Uanis(C216) \\sim Ueq, Uanis(C213) \\sim Ueq, Uanis(C284) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C18) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C235) \\sim Ueq, Uanis(C211) \\sim Ueq, Uanis(C210) \\sim Ueq, Uanis(C252) \\sim Ueq, Uanis(C253) \\sim Ueq, Uanis(C22) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C3) \\sim Ueq, Uanis(C2) \\sim Ueq, Uanis(C14) \\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C15) \\sim Ueq, Uanis(C153) \\sim Ueq, Uanis(C156) \\sim Ueq, Uanis(C287) \\sim Ueq, Uanis(C277) \\sim Ueq, Uanis(C5) \\sim Ueq, Uanis(C8) \\sim Ueq, Uanis(C65) \\sim Ueq, Uanis(C83) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C285) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C44) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C13) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C212) \\sim Ueq, Uanis(C207) \\sim Ueq, Uanis(C208) \\sim Ueq, Uanis(C209) \\sim Ueq, Uanis(C210) \\sim Ueq, Uanis(C211) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(N8) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C233) \\sim Ueq, Uanis(C234) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 5.a Aromatic/amide H refined with riding coordinates: C73(H73), C93(H93), C91(H91), C92(H92), C68(H68), C231(H231), C125(H125), C114(H114), C60(H60), C59(H59), C174(H174), C74(H74), C275(H275), C37(H37), C42(H42), C43(H43), C24(H24), C259(H259), C75(H75), C71(H71), C258(H258), C274(H274), C263(H263), C190(H190), C20(H20), C61(H61), C65(H65), C87(H87), C99(H99), C26(H26), C108(H108), C164(H164), C112(H112), C162(H162), C111(H111), C194(H194), C168(H168), C101(H101), C81(H81), C115(H115), C171(H171), C86(H86), C264(H264), C203(H203), C70(H70), C58(H58), C208(H208), C130(H130), C225(H225), C90(H90), C161(H161), C38(H38), C14(H14), C186(H186), C187(H187), C230(H230), C228(H228), C62(H62), C200(H200), C170(H170), C160(H160), C176(H176), C104(H104), C109(H109), C27(H27), C64(H64), C110(H110), C199(H199), C281(H281), C175(H175), C269(H269), C76(H76), C159(H159), C246(H246), C261(H261), C89(H89), C120(H120), C204(H204), C128(H128), C278(H278), C184(H184), C198(H198), C84(H84), C134(H134), C32(H32), C197(H197), C141(H141), C282(H282), C29(H29), C255(H255), C103(H103), C288(H288), C102(H102), C105(H105), C49(H49), C48(H48), C47(H47), C46(H46), C50(H50), C183(H183), C40(H40), C193(H193), C181(H181), C196(H196), C140(H140), C18(H18), C82(H82), C205(H205), C16(H16), C67(H67), C17(H17), C126(H126), C244(H244), C242(H242), C253(H253), C252(H252), C55(H55), C173(H173), C248(H248), C234(H234), C215(H215), C249(H249), C23(H23), C95(H95), C240(H240), C256(H256), C262(H262), C56(H56), C254(H254), C119(H119), C39(H39), C96(H96), C135(H135), C272(H272), C127(H127), C243(H243), C192(H192), C98(H98), C250(H250), C279(H279), C220(H220), C66(H66), C206(H206), C212(H212), C280(H280), C270(H270), C131(H131), C30(H30), C166(H166), C31(H31), C284(H284), C21(H21), C191(H191), C158(H158), C165(H165), C227(H227), C138(H138), C83(H83), C142(H142), C167(H167), C214(H214), C286(H286), C137(H137), C202(H202), C285(H285), C218(H218), C117(H117), C53(H53), C54(H54), C182(H182), C209(H209), C143(H143), C97(H97), C118(H118), C247(H247), C136(H136), C271(H271), C226(H226), C144(H144), C236(H236), C22(H22), C237(H237), C238(H238), C235(H235), C210(H210), C211(H211), C241(H241), C52(H52), C217(H217), C219(H219), C287(H287), C15(H15) 5.b Fitted hexagon refined as free rotating group: C49(C48,C47,C46,C45,C50) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au7 Au 0.65219(7) 0.51271(5) 0.87273(4) 0.0377(3) Uani 1 1 d . . . . . Au15 Au 0.19514(7) 0.52104(5) 0.40194(4) 0.0381(3) Uani 1 1 d . . . . . Au3 Au 0.49610(7) 0.53040(5) 0.84481(4) 0.0390(3) Uani 1 1 d . . . . . Au5 Au 0.70254(7) 0.41837(5) 0.90766(4) 0.0396(3) Uani 1 1 d . . . . . Au13 Au 0.27118(7) 0.50388(5) 0.48002(4) 0.0424(3) Uani 1 1 d . . . . . Au2 Au 0.60935(7) 0.60688(5) 0.84696(4) 0.0424(3) Uani 1 1 d . . . . . Au12 Au 0.18037(8) 0.42979(5) 0.43826(4) 0.0464(3) Uani 1 1 d . . . . . Au4 Au 0.54329(7) 0.43824(5) 0.87787(4) 0.0425(3) Uani 1 1 d . . . . . Au14 Au 0.28633(8) 0.59262(5) 0.43840(5) 0.0458(3) Uani 1 1 d . . . . . Au6 Au 0.80130(7) 0.50013(5) 0.90427(4) 0.0439(3) Uani 1 1 d . . . . . Au8 Au 0.59784(7) 0.47486(6) 0.79978(4) 0.0473(3) Uani 1 1 d . . . . . Au9 Au 0.27746(8) 0.55959(5) 0.33456(4) 0.0438(3) Uani 1 1 d . . . . . Au11 Au 0.09228(8) 0.45100(5) 0.36480(4) 0.0457(3) Uani 1 1 d . . . . . Au1 Au 0.73932(8) 0.56048(5) 0.81255(5) 0.0483(3) Uani 1 1 d . . . . . Au10 Au 0.11396(8) 0.54638(6) 0.33028(5) 0.0499(3) Uani 1 1 d . . . . . Au16 Au 0.25200(8) 0.44529(6) 0.35814(5) 0.0525(3) Uani 1 1 d . . . . . Cu5 Cu 0.1785(3) 0.61607(17) 0.37827(15) 0.0434(10) Uani 1 1 d . . . . . Cu2 Cu 0.6717(3) 0.49947(19) 0.95105(14) 0.0464(11) Uani 1 1 d . . . . . Cu6 Cu 0.1443(3) 0.5625(2) 0.46761(15) 0.0480(11) Uani 1 1 d . . . . . Cu1 Cu 0.7398(3) 0.59202(19) 0.89282(16) 0.0491(11) Uani 1 1 d . . . . . Cu7 Cu 0.1509(3) 0.6597(2) 0.45919(18) 0.0546(12) Uani 1 1 d . . . . . Cu3 Cu 0.7759(3) 0.5651(2) 0.98091(18) 0.0586(13) Uani 1 1 d . . . . . Cu8 Cu 0.2764(3) 0.6887(2) 0.40856(19) 0.0567(13) Uani 1 1 d . . . . . Cu4 Cu 0.8966(3) 0.5822(2) 0.91976(18) 0.0585(13) Uani 1 1 d . . . . . P5 P 0.7533(5) 0.3393(3) 0.9232(3) 0.0417(17) Uani 1 1 d . . . . . P11 P 0.3551(4) 0.4902(4) 0.5377(2) 0.0453(19) Uani 1 1 d . . . . . P2 P 0.5203(4) 0.6720(3) 0.8482(3) 0.0407(16) Uani 1 1 d . . . . . P3 P 0.3643(4) 0.5491(3) 0.8281(3) 0.0415(17) Uani 1 1 d . . . . . P6 P 0.6638(4) 0.4446(4) 0.7434(2) 0.0445(18) Uani 1 1 d . . . . . S9 S 0.0189(5) 0.5377(4) 0.4522(3) 0.054(2) Uani 1 1 d . . . . . P7 P 0.3631(5) 0.5794(3) 0.2805(3) 0.0429(17) Uani 1 1 d . . . . . P4 P 0.4846(4) 0.3701(3) 0.9079(3) 0.0409(17) Uani 1 1 d . . . . . P12 P 0.3686(5) 0.4213(3) 0.3291(3) 0.0431(17) Uani 1 1 d . . . . . S12 S 0.3892(4) 0.6549(3) 0.4403(3) 0.0509(19) Uani 1 1 d . . . . . S3 S 0.5458(5) 0.5261(4) 0.9595(3) 0.054(2) Uani 1 1 d . . . . . P1 P 0.8094(5) 0.5847(4) 0.7534(3) 0.053(2) Uani 1 1 d . . . . . P10 P 0.1718(5) 0.3810(3) 0.4972(3) 0.0487(19) Uani 1 1 d . . . . . P8 P -0.0025(5) 0.5495(4) 0.2909(3) 0.053(2) Uani 1 1 d . . . . . S7 S 0.2212(5) 0.6867(3) 0.3441(3) 0.0532(19) Uani 1 1 d . . . . . P9 P -0.0002(5) 0.3945(3) 0.3389(3) 0.0484(19) Uani 1 1 d . . . . . S8 S 0.0632(4) 0.6509(4) 0.4022(3) 0.0511(19) Uani 1 1 d . . . . . S2 S 0.6983(5) 0.6289(4) 0.9539(3) 0.061(2) Uani 1 1 d . . . . . S6 S 0.9445(4) 0.5053(4) 0.9062(3) 0.055(2) Uani 1 1 d . . . . . S4 S 0.7147(5) 0.5025(4) 1.0182(2) 0.0524(19) Uani 1 1 d . . . . . S11 S 0.2342(6) 0.7283(4) 0.4677(4) 0.064(3) Uani 1 1 d . . . . . S10 S 0.1142(5) 0.6172(4) 0.5187(3) 0.0510(19) Uani 1 1 d . . . . . S5 S 0.9123(6) 0.5780(4) 0.9905(3) 0.066(3) Uani 1 1 d . . . . . S1 S 0.8455(6) 0.6463(4) 0.8837(4) 0.065(3) Uani 1 1 d . . . . . C73 C 0.231(2) 0.7335(15) 0.7390(12) 0.056(9) Uani 1 1 d . . . . . H73 H 0.211086 0.731632 0.711521 0.067 Uiso 1 1 calc R . . . . C276 C 0.3469(18) 0.4367(15) 0.5714(10) 0.050(8) Uani 1 1 d . . . . . C72 C 0.2627(18) 0.6903(12) 0.7585(9) 0.041(6) Uani 1 1 d . . . . . C163 C 0.291(2) 0.6072(14) 0.2422(9) 0.048(7) Uani 1 1 d . . . . . C79 C 0.3543(15) 0.6563(11) 0.8683(7) 0.034(6) Uani 1 1 d D . . . . C257 C 0.1491(19) 0.4254(12) 0.5394(10) 0.044(7) Uani 1 1 d . . . . . C94 C 0.4888(19) 0.6945(13) 0.7966(10) 0.045(7) Uani 1 1 d . . . . . C69 C 0.3235(17) 0.6058(11) 0.8034(11) 0.044(7) Uani 1 1 d . . . . . C93 C 0.4697(18) 0.7433(12) 0.7885(13) 0.050(8) Uani 1 1 d . . . . . H93 H 0.471119 0.766131 0.810484 0.060 Uiso 1 1 calc R . . . . C91 C 0.4457(17) 0.7248(17) 0.7149(12) 0.060(10) Uani 1 1 d . . . . . H91 H 0.431221 0.735738 0.687956 0.072 Uiso 1 1 calc R . . . . C189 C 0.3558(19) 0.4076(12) 0.2734(12) 0.050(8) Uani 1 1 d . . . . . N4 N 0.616(3) 0.5329(18) 1.1167(12) 0.090(12) Uani 1 1 d . U . . . C35 C 0.835(2) 0.4722(14) 0.7388(11) 0.052(8) Uani 1 1 d . . . . . C92 C 0.449(2) 0.7587(17) 0.7501(14) 0.062(10) Uani 1 1 d . . . . . H92 H 0.437074 0.792089 0.745685 0.075 Uiso 1 1 calc R . . . . C68 C 0.216(2) 0.5357(17) 0.8672(16) 0.070(11) Uani 1 1 d . . . . . H68 H 0.191898 0.542517 0.841107 0.084 Uiso 1 1 calc R . . . . C2 C 0.826(2) 0.6841(13) 0.9260(12) 0.053(8) Uani 1 1 d . U . . . C231 C -0.039(2) 0.3660(16) 0.2561(11) 0.059(9) Uani 1 1 d . . . . . H231 H -0.005204 0.339119 0.261662 0.070 Uiso 1 1 calc R . . . . C125 C 0.677(2) 0.2945(16) 1.0316(11) 0.058(9) Uani 1 1 d . . . . . H125 H 0.690372 0.266853 1.015653 0.070 Uiso 1 1 calc R . . . . C114 C 0.711(2) 0.2396(14) 0.9084(12) 0.057(9) Uani 1 1 d . . . . . H114 H 0.762909 0.237664 0.897791 0.068 Uiso 1 1 calc R . . . . C60 C 0.337(2) 0.4294(15) 0.7245(12) 0.073(11) Uani 1 1 d D U . . . H60 H 0.332865 0.404593 0.704250 0.088 Uiso 1 1 calc R . . . . C59 C 0.3972(19) 0.4653(11) 0.7213(8) 0.048(7) Uani 1 1 d D U . . . H59 H 0.432451 0.466269 0.699078 0.058 Uiso 1 1 calc R . . . . C132 C 0.5337(19) 0.3639(13) 0.9599(10) 0.044(7) Uani 1 1 d . . . . . C78 C 0.3250(16) 0.6520(13) 0.8231(7) 0.041(7) Uani 1 1 d D . . . . C185 C 0.542(2) 0.5441(18) 0.3793(11) 0.066(12) Uani 1 1 d . . . . . C88 C 0.434(2) 0.6587(14) 0.8814(13) 0.060(9) Uani 1 1 d . . . . . C100 C 0.5664(18) 0.7249(15) 0.8751(12) 0.056(9) Uani 1 1 d . . . . . C174 C 0.595(2) 0.3957(16) 0.1943(14) 0.065(10) Uani 1 1 d . . . . . H174 H 0.621575 0.372350 0.178051 0.078 Uiso 1 1 calc R . . . . C267 C 0.2777(19) 0.4161(12) 0.5838(9) 0.042(7) Uani 1 1 d . . . . . C107 C 0.8077(18) 0.3395(12) 0.9713(12) 0.047(7) Uani 1 1 d . . . . . C74 C 0.230(2) 0.7771(16) 0.7592(13) 0.059(9) Uani 1 1 d . . . . . H74 H 0.210463 0.804995 0.744851 0.071 Uiso 1 1 calc R . . . . C19 C 0.9120(18) 0.6008(14) 0.7669(9) 0.055(9) Uani 1 1 d D . . . . C34 C 0.8217(16) 0.5019(10) 0.7001(8) 0.047(8) Uani 1 1 d D . . . . C275 C 0.420(2) 0.4139(16) 0.5882(12) 0.059(9) Uani 1 1 d . . . . . H275 H 0.468140 0.427296 0.579027 0.071 Uiso 1 1 calc R . . . . C37 C 0.980(2) 0.4880(17) 0.7379(13) 0.063(10) Uani 1 1 d . . . . . H37 H 0.971309 0.505018 0.712660 0.076 Uiso 1 1 calc R . . . . C42 C 0.8594(19) 0.4251(13) 0.8167(10) 0.047(8) Uani 1 1 d . . . . . H42 H 0.866396 0.410841 0.843210 0.057 Uiso 1 1 calc R . . . . C43 C 0.7817(15) 0.4263(12) 0.7986(9) 0.038(6) Uani 1 1 d . . . . . H43 H 0.738523 0.412078 0.812202 0.046 Uiso 1 1 calc R . . . . C44 C 0.7711(15) 0.4497(12) 0.7594(9) 0.038(6) Uani 1 1 d . U . . . C124 C 0.624(2) 0.3312(14) 1.0137(10) 0.049(8) Uani 1 1 d . . . . . C24 C 0.959(2) 0.6277(19) 0.7396(12) 0.086(16) Uani 1 1 d D . . . . H24 H 0.936077 0.638968 0.714404 0.103 Uiso 1 1 calc R . . . . C259 C 0.047(2) 0.4836(16) 0.5589(9) 0.058(10) Uani 1 1 d . . . . . H259 H -0.002876 0.498546 0.553276 0.069 Uiso 1 1 calc R . . . . C106 C 0.8238(19) 0.3220(13) 0.8818(10) 0.047(7) Uani 1 1 d . . . . . C75 C 0.255(2) 0.7818(12) 0.7999(11) 0.048(7) Uani 1 1 d . . . . . H75 H 0.250501 0.812214 0.813587 0.058 Uiso 1 1 calc R . . . . C71 C 0.264(2) 0.6435(14) 0.7427(11) 0.055(8) Uani 1 1 d . . . . . H71 H 0.240162 0.639568 0.716005 0.066 Uiso 1 1 calc R . . . . C178 C 0.4709(17) 0.5009(12) 0.2699(11) 0.046(7) Uani 1 1 d . . . . . C77 C 0.2904(16) 0.6946(11) 0.8013(11) 0.041(7) Uani 1 1 d . . . . . C258 C 0.0741(18) 0.4477(13) 0.5322(11) 0.047(7) Uani 1 1 d . . . . . H258 H 0.042436 0.438095 0.509114 0.057 Uiso 1 1 calc R . . . . C157 C 0.437(2) 0.6260(14) 0.2922(13) 0.060(9) Uani 1 1 d . . . . . C188 C 0.4400(17) 0.4715(12) 0.3417(11) 0.044(7) Uani 1 1 d . . . . . C265 C 0.1677(19) 0.4774(12) 0.6023(10) 0.044(7) Uani 1 1 d . . . . . C274 C 0.426(3) 0.3768(15) 0.6148(16) 0.069(11) Uani 1 1 d . . . . . H274 H 0.476362 0.365092 0.624071 0.083 Uiso 1 1 calc R . . . . C263 C 0.182(3) 0.528(2) 0.6651(13) 0.076(13) Uani 1 1 d . . . . . H263 H 0.210997 0.536878 0.689426 0.092 Uiso 1 1 calc R . . . . C190 C 0.301(2) 0.4340(14) 0.2501(11) 0.056(9) Uani 1 1 d . . . . . H190 H 0.272574 0.459802 0.262141 0.068 Uiso 1 1 calc R . . . . C266 C 0.1975(19) 0.4396(12) 0.5741(10) 0.043(7) Uani 1 1 d . . . . . C51 C 0.643(2) 0.3811(16) 0.7363(12) 0.057(9) Uani 1 1 d . . . . . C41 C 0.9267(16) 0.4443(13) 0.7968(11) 0.045(7) Uani 1 1 d . . . . . C8 C 0.620(2) 0.5289(15) 1.0836(12) 0.059(9) Uani 1 1 d . U . . . C20 C 0.9477(16) 0.5847(17) 0.8043(10) 0.068(11) Uani 1 1 d D . . . . H20 H 0.918034 0.565393 0.822571 0.081 Uiso 1 1 calc R . . . . C145 C 0.130(2) 0.7687(15) 0.3253(16) 0.069(11) Uani 1 1 d . . . . . C3 C 0.768(2) 0.6776(14) 0.9552(12) 0.055(8) Uani 1 1 d . U . . . C7 C 0.623(2) 0.5213(15) 1.0389(9) 0.056(9) Uani 1 1 d . . . . . C6 C 0.556(2) 0.5297(12) 1.0144(12) 0.053(8) Uani 1 1 d . . . . . C61 C 0.284(3) 0.4303(15) 0.7577(12) 0.084(14) Uani 1 1 d D . . . . H61 H 0.244994 0.405782 0.759046 0.101 Uiso 1 1 calc R . . . . C65 C 0.283(3) 0.5135(19) 0.9428(15) 0.077(12) Uani 1 1 d . U . . . H65 H 0.305417 0.503032 0.968289 0.093 Uiso 1 1 calc R . . . . C63 C 0.3010(18) 0.5367(13) 0.8720(11) 0.046(7) Uani 1 1 d . . . . . C277 C 0.3477(19) 0.5412(13) 0.5743(10) 0.045(7) Uani 1 1 d . U . . . C273 C 0.353(3) 0.3547(13) 0.6290(12) 0.058(9) Uani 1 1 d . . . . . C87 C 0.454(2) 0.6543(15) 0.9244(11) 0.054(9) Uani 1 1 d . . . . . H87 H 0.507955 0.654581 0.932603 0.065 Uiso 1 1 calc R . . . . C57 C 0.3488(13) 0.5018(10) 0.7883(8) 0.035(6) Uani 1 1 d D U . . . C99 C 0.649(2) 0.7327(15) 0.8693(13) 0.060(10) Uani 1 1 d . . . . . H99 H 0.678698 0.711989 0.852268 0.072 Uiso 1 1 calc R . . . . C129 C 0.602(2) 0.3709(14) 1.0399(10) 0.050(8) Uani 1 1 d . . . . . C26 C 0.819(2) 0.5801(13) 0.6634(8) 0.061(9) Uani 1 1 d D U . . . H26 H 0.821088 0.614672 0.663869 0.073 Uiso 1 1 calc R . . . . C1 C 0.880(2) 0.7272(17) 0.9303(16) 0.074(13) Uani 1 1 d . . . . . C177 C 0.517(2) 0.4669(13) 0.2439(10) 0.050(8) Uani 1 1 d . . . . . C108 C 0.816(3) 0.3817(16) 0.9958(12) 0.069(11) Uani 1 1 d . . . . . H108 H 0.792524 0.411211 0.986308 0.083 Uiso 1 1 calc R . . . . C239 C 0.0598(19) 0.3426(14) 0.3318(10) 0.049(8) Uani 1 1 d . . . . . C164 C 0.300(3) 0.6577(16) 0.2310(12) 0.065(10) Uani 1 1 d . . . . . H164 H 0.341100 0.677412 0.242613 0.077 Uiso 1 1 calc R . . . . C112 C 0.851(2) 0.2966(16) 0.9865(13) 0.062(9) Uani 1 1 d . U . . . H112 H 0.846706 0.266888 0.971610 0.075 Uiso 1 1 calc R . . . . C25 C 0.8155(19) 0.5535(10) 0.7010(9) 0.047(7) Uani 1 1 d D U . . . C162 C 0.491(2) 0.6413(13) 0.2621(13) 0.057(9) Uani 1 1 d . . . . . H162 H 0.488607 0.628008 0.235074 0.068 Uiso 1 1 calc R . . . . C111 C 0.899(3) 0.298(2) 1.0224(16) 0.082(13) Uani 1 1 d . U . . . H111 H 0.929402 0.270704 1.030643 0.098 Uiso 1 1 calc R . . . . C169 C 0.419(2) 0.5345(13) 0.2501(12) 0.053(8) Uani 1 1 d . . . . . C133 C 0.4900(19) 0.3134(13) 0.8769(11) 0.059(9) Uani 1 1 d D U . . . C10 C 0.954(3) 0.5195(19) 0.9897(12) 0.072(12) Uani 1 1 d . . . . . C194 C 0.3961(19) 0.3665(12) 0.2534(11) 0.045(7) Uani 1 1 d . . . . . H194 H 0.432710 0.347976 0.269468 0.054 Uiso 1 1 calc R . . . . C168 C 0.231(2) 0.5794(16) 0.2284(14) 0.067(11) Uani 1 1 d . . . . . H168 H 0.224965 0.546647 0.236959 0.080 Uiso 1 1 calc R . . . . N6 N 1.024(2) 0.402(2) 0.9659(11) 0.090(13) Uani 1 1 d . . . . . C260 C 0.092(2) 0.4984(14) 0.5947(9) 0.049(8) Uani 1 1 d . . . . . C101 C 0.798(2) 0.3105(13) 0.8433(12) 0.053(8) Uani 1 1 d . . . . . H101 H 0.742776 0.308235 0.837357 0.064 Uiso 1 1 calc R . . . . C195 C 0.410(2) 0.3672(16) 0.3527(11) 0.059(9) Uani 1 1 d . . . . . C121 C 0.566(2) 0.2408(13) 0.9476(11) 0.051(8) Uani 1 1 d . . . . . C81 C 0.2104(19) 0.6574(15) 0.8909(12) 0.055(9) Uani 1 1 d . . . . . H81 H 0.193102 0.655048 0.862876 0.065 Uiso 1 1 calc R . . . . C115 C 0.669(3) 0.1994(13) 0.9069(11) 0.059(10) Uani 1 1 d . . . . . H115 H 0.687720 0.171467 0.892727 0.071 Uiso 1 1 calc R . . . . C171 C 0.451(2) 0.5011(17) 0.1815(13) 0.064(10) Uani 1 1 d . . . . . H171 H 0.444222 0.502151 0.152380 0.077 Uiso 1 1 calc R . . . . C86 C 0.401(3) 0.6498(16) 0.9530(14) 0.070(12) Uani 1 1 d . . . . . H86 H 0.417417 0.644226 0.980777 0.084 Uiso 1 1 calc R . . . . C113 C 0.689(2) 0.2852(13) 0.9242(13) 0.056(9) Uani 1 1 d . . . . . C264 C 0.212(2) 0.4918(17) 0.6393(14) 0.064(10) Uani 1 1 d . . . . . H264 H 0.260887 0.476671 0.645928 0.077 Uiso 1 1 calc R . . . . C232 C -0.0567(19) 0.4021(13) 0.2874(12) 0.050(8) Uani 1 1 d . . . . . C203 C 0.073(2) 0.4577(18) 0.1977(17) 0.078(13) Uani 1 1 d . . . . . H203 H 0.104528 0.429157 0.195591 0.093 Uiso 1 1 calc R . . . . C70 C 0.2930(16) 0.6033(13) 0.7601(11) 0.045(7) Uani 1 1 d . . . . . H70 H 0.294450 0.573548 0.745172 0.054 Uiso 1 1 calc R . . . . C154 C 0.315(2) 0.7117(13) 0.5006(15) 0.061(10) Uani 1 1 d . . . . . C58 C 0.4000(15) 0.4999(11) 0.7543(7) 0.041(6) Uani 1 1 d D U . . . H58 H 0.440037 0.524029 0.753299 0.050 Uiso 1 1 calc R . . . . C208 C 0.022(3) 0.6473(14) 0.2727(14) 0.071(11) Uani 1 1 d D U . . . H208 H 0.075548 0.638215 0.271173 0.086 Uiso 1 1 calc R . . . . C130 C 0.546(2) 0.4049(15) 1.0274(11) 0.057(9) Uani 1 1 d . . . . . H130 H 0.528937 0.429247 1.045978 0.068 Uiso 1 1 calc R . . . . C225 C -0.202(3) 0.4833(18) 0.2296(11) 0.067(11) Uani 1 1 d . . . . . H225 H -0.213058 0.506532 0.250328 0.081 Uiso 1 1 calc R . . . . C90 C 0.464(2) 0.6768(15) 0.7223(11) 0.057(9) Uani 1 1 d . . . . . H90 H 0.460536 0.654075 0.700270 0.069 Uiso 1 1 calc R . . . . C155 C 0.377(2) 0.6816(14) 0.4896(14) 0.061(10) Uani 1 1 d . . . . . C161 C 0.548(3) 0.6771(16) 0.273(2) 0.088(16) Uani 1 1 d . . . . . H161 H 0.583783 0.688099 0.253334 0.106 Uiso 1 1 calc R . . . . C151 C 0.010(2) 0.6070(14) 0.5167(12) 0.052(8) Uani 1 1 d . . . . . C38 C 1.056(2) 0.4834(18) 0.7523(14) 0.068(11) Uani 1 1 d . . . . . H38 H 1.098980 0.495094 0.736767 0.081 Uiso 1 1 calc R . . . . C147 C 0.068(2) 0.7060(13) 0.3766(15) 0.061(10) Uani 1 1 d . . . . . C146 C 0.132(3) 0.7213(15) 0.3496(12) 0.060(9) Uani 1 1 d . . . . . C14 C 0.765(3) 0.6805(14) 0.7694(14) 0.084(9) Uani 1 1 d D U . . . H14 H 0.804443 0.677763 0.790736 0.100 Uiso 1 1 calc R . . . . C186 C 0.490(2) 0.5160(16) 0.4040(12) 0.059(9) Uani 1 1 d . . . . . H186 H 0.486858 0.522447 0.432725 0.071 Uiso 1 1 calc R . . . . C187 C 0.444(2) 0.4809(12) 0.3873(10) 0.045(7) Uani 1 1 d . . . . . H187 H 0.413520 0.461255 0.404871 0.054 Uiso 1 1 calc R . . . . C230 C -0.075(3) 0.3736(16) 0.2166(12) 0.064(10) Uani 1 1 d . . . . . H230 H -0.063067 0.350953 0.195501 0.077 Uiso 1 1 calc R . . . . C228 C -0.165(3) 0.4181(18) 0.1651(16) 0.079(13) Uani 1 1 d . . . . . H228 H -0.152338 0.396230 0.143547 0.095 Uiso 1 1 calc R . . . . C150 C -0.0278(18) 0.5740(13) 0.4890(11) 0.048(8) Uani 1 1 d . . . . . C62 C 0.2880(18) 0.4664(11) 0.7889(11) 0.057(9) Uani 1 1 d D . . . . H62 H 0.250082 0.466939 0.809965 0.068 Uiso 1 1 calc R . . . . C200 C 0.494(3) 0.3628(16) 0.3640(16) 0.077(13) Uani 1 1 d . . . . . H200 H 0.528038 0.390025 0.361094 0.093 Uiso 1 1 calc R . . . . C170 C 0.411(2) 0.5331(14) 0.2049(9) 0.053(9) Uani 1 1 d . . . . . H170 H 0.377236 0.555811 0.191543 0.063 Uiso 1 1 calc R . . . . C160 C 0.553(2) 0.6962(16) 0.313(2) 0.085(16) Uani 1 1 d . . . . . H160 H 0.594012 0.718538 0.320281 0.102 Uiso 1 1 calc R . . . . C176 C 0.5716(18) 0.4321(15) 0.2601(12) 0.055(9) Uani 1 1 d . . . . . H176 H 0.581315 0.432258 0.289042 0.066 Uiso 1 1 calc R . . . . C104 C 0.959(3) 0.3168(19) 0.8589(18) 0.080(14) Uani 1 1 d . . . . . H104 H 1.013978 0.320344 0.863931 0.096 Uiso 1 1 calc R . . . . C109 C 0.857(3) 0.381(2) 1.0343(14) 0.079(13) Uani 1 1 d . . . . . H109 H 0.856561 0.408961 1.052001 0.094 Uiso 1 1 calc R . . . . C27 C 0.818(2) 0.5550(11) 0.6252(11) 0.068(10) Uani 1 1 d D U . . . H27 H 0.812653 0.573274 0.600416 0.082 Uiso 1 1 calc R . . . . C64 C 0.334(2) 0.5253(16) 0.9096(11) 0.057(9) Uani 1 1 d . . . . . H64 H 0.389809 0.525128 0.913621 0.068 Uiso 1 1 calc R . . . . C283 C 0.4580(19) 0.4926(18) 0.5202(10) 0.060(10) Uani 1 1 d . . . . . C152 C -0.034(2) 0.6319(15) 0.5455(12) 0.056(9) Uani 1 1 d . . . . . C110 C 0.900(3) 0.3398(19) 1.0452(16) 0.080(13) Uani 1 1 d . U . . . H110 H 0.931104 0.340430 1.069866 0.096 Uiso 1 1 calc R . . . . C199 C 0.524(4) 0.319(2) 0.3788(17) 0.089(14) Uani 1 1 d . U . . . H199 H 0.579538 0.314814 0.382097 0.107 Uiso 1 1 calc R . . . . C179 C 0.486(2) 0.4997(14) 0.3167(9) 0.050(8) Uani 1 1 d . . . . . C281 C 0.292(3) 0.6207(18) 0.5923(15) 0.076(12) Uani 1 1 d . . . . . H281 H 0.259111 0.647512 0.585217 0.091 Uiso 1 1 calc R . . . . C85 C 0.319(2) 0.6531(13) 0.9429(9) 0.049(8) Uani 1 1 d . . . . . C139 C 0.376(2) 0.3749(13) 0.9172(14) 0.058(9) Uani 1 1 d . . . . . C175 C 0.612(2) 0.3979(17) 0.2371(14) 0.065(10) Uani 1 1 d . . . . . H175 H 0.649096 0.376627 0.249794 0.078 Uiso 1 1 calc R . . . . C269 C 0.206(3) 0.3568(17) 0.6311(14) 0.071(12) Uani 1 1 d . . . . . H269 H 0.156137 0.369951 0.622566 0.085 Uiso 1 1 calc R . . . . C76 C 0.2874(19) 0.7424(13) 0.8204(12) 0.050(8) Uani 1 1 d . . . . . H76 H 0.308025 0.746484 0.847601 0.061 Uiso 1 1 calc R . . . . C33 C 0.8322(19) 0.4792(11) 0.6610(7) 0.062(10) Uani 1 1 d D . . . . C159 C 0.498(3) 0.6826(17) 0.3420(16) 0.075(13) Uani 1 1 d . . . . . H159 H 0.497990 0.696878 0.368678 0.090 Uiso 1 1 calc R . . . . N10 N -0.067(3) 0.6507(18) 0.5741(17) 0.103(15) Uani 1 1 d . . . . . C229 C -0.128(3) 0.4120(17) 0.2058(13) 0.067(10) Uani 1 1 d . U . . . C246 C 0.082(3) 0.3065(15) 0.4612(11) 0.062(10) Uani 1 1 d . . . . . H246 H 0.118569 0.310134 0.439498 0.074 Uiso 1 1 calc R . . . . C261 C 0.065(2) 0.5353(16) 0.6209(15) 0.068(11) Uani 1 1 d . . . . . H261 H 0.014878 0.549886 0.615424 0.081 Uiso 1 1 calc R . . . . C89 C 0.489(2) 0.6598(13) 0.7633(11) 0.049(8) Uani 1 1 d . . . . . H89 H 0.504741 0.627021 0.767790 0.059 Uiso 1 1 calc R . . . . C120 C 0.495(2) 0.2391(14) 0.9711(14) 0.061(10) Uani 1 1 d . . . . . H120 H 0.482195 0.265856 0.988107 0.073 Uiso 1 1 calc R . . . . C204 C 0.035(3) 0.4787(19) 0.1636(14) 0.072(12) Uani 1 1 d . . . . . H204 H 0.047685 0.466265 0.137135 0.087 Uiso 1 1 calc R . . . . N9 N -0.184(2) 0.564(2) 0.4936(15) 0.095(13) Uani 1 1 d . . . . . C128 C 0.644(3) 0.3759(19) 1.0816(14) 0.071(12) Uani 1 1 d . . . . . H128 H 0.635392 0.403684 1.098373 0.086 Uiso 1 1 calc R . . . . C13 C 0.757(2) 0.6413(14) 0.7413(11) 0.070(7) Uani 1 1 d D U . . . C278 C 0.3945(19) 0.5399(14) 0.6117(10) 0.049(8) Uani 1 1 d . . . . . H278 H 0.428298 0.513101 0.617582 0.059 Uiso 1 1 calc R . . . . C184 C 0.595(3) 0.5798(15) 0.3953(14) 0.070(12) Uani 1 1 d . . . . . H184 H 0.592201 0.588754 0.423512 0.084 Uiso 1 1 calc R . . . . C198 C 0.475(3) 0.281(2) 0.3889(16) 0.082(13) Uani 1 1 d . U . . . H198 H 0.495783 0.251974 0.400451 0.098 Uiso 1 1 calc R . . . . C84 C 0.259(2) 0.6542(16) 0.9748(14) 0.065(10) Uani 1 1 d . . . . . H84 H 0.274880 0.652202 1.003038 0.079 Uiso 1 1 calc R . . . . C134 C 0.554(2) 0.3082(15) 0.8500(12) 0.066(10) Uani 1 1 d D U . . . H134 H 0.592429 0.333409 0.849124 0.080 Uiso 1 1 calc R . . . . C123 C 0.588(2) 0.3281(13) 0.9731(10) 0.054(9) Uani 1 1 d D . . . . C32 C 0.846(3) 0.4287(11) 0.6552(12) 0.069(10) Uani 1 1 d D U . . . H32 H 0.854031 0.410327 0.679654 0.082 Uiso 1 1 calc R . . . . C12 C 1.001(2) 0.4420(18) 0.9631(15) 0.069(11) Uani 1 1 d . . . . . C197 C 0.391(3) 0.285(2) 0.3819(16) 0.081(13) Uani 1 1 d . U . . . H197 H 0.357151 0.258897 0.387908 0.098 Uiso 1 1 calc R . . . . C172 C 0.502(2) 0.4652(15) 0.2002(14) 0.063(10) Uani 1 1 d . . . . . C141 C 0.257(4) 0.356(2) 0.955(2) 0.096(16) Uani 1 1 d . U . . . H141 H 0.233041 0.342702 0.978498 0.116 Uiso 1 1 calc R . . . . N7 N 0.125(3) 0.8023(17) 0.3068(17) 0.099(15) Uani 1 1 d . . . . . C282 C 0.298(3) 0.5801(17) 0.5668(14) 0.069(11) Uani 1 1 d . . . . . H282 H 0.265143 0.579085 0.542602 0.083 Uiso 1 1 calc R . . . . N8 N -0.053(3) 0.762(2) 0.3782(18) 0.113(15) Uani 1 1 d . U . . . C29 C 0.826(2) 0.4810(16) 0.5834(10) 0.082(15) Uani 1 1 d D . . . . H29 H 0.818950 0.499554 0.558864 0.098 Uiso 1 1 calc R . . . . N12 N 0.497(3) 0.669(2) 0.5403(13) 0.094(13) Uani 1 1 d . . . . . C255 C 0.391(3) 0.319(2) 0.4937(18) 0.086(14) Uani 1 1 d . U . . . H255 H 0.438662 0.324149 0.479540 0.103 Uiso 1 1 calc R . . . . C103 C 0.932(3) 0.3032(18) 0.8196(18) 0.079(13) Uani 1 1 d . . . . . H103 H 0.968983 0.295216 0.798970 0.095 Uiso 1 1 calc R . . . . C288 C 0.502(2) 0.5376(19) 0.5229(11) 0.065(11) Uani 1 1 d . . . . . H288 H 0.476603 0.565941 0.532894 0.078 Uiso 1 1 calc R . . . . C36 C 0.9112(18) 0.4693(12) 0.7579(10) 0.045(7) Uani 1 1 d . . . . . C102 C 0.854(3) 0.3016(18) 0.8112(18) 0.083(14) Uani 1 1 d . . . . . H102 H 0.835799 0.294547 0.783950 0.100 Uiso 1 1 calc R . . . . C105 C 0.908(2) 0.3254(17) 0.8909(14) 0.066(10) Uani 1 1 d . . . . . H105 H 0.927198 0.333227 0.917806 0.079 Uiso 1 1 calc R . . . . C49 C 0.6207(19) 0.4756(12) 0.6197(7) 0.076(11) Uani 1 1 d . U . . . H49 H 0.622225 0.459211 0.593942 0.091 Uiso 1 1 calc R . . . . C48 C 0.5995(19) 0.5255(11) 0.6213(8) 0.081(12) Uani 1 1 d G U . . . H48 H 0.586811 0.542571 0.596531 0.097 Uiso 1 1 calc R . . . . C47 C 0.597(2) 0.5499(9) 0.6598(10) 0.087(14) Uani 1 1 d G U . . . H47 H 0.583088 0.583343 0.660823 0.105 Uiso 1 1 calc R . . . . C46 C 0.616(2) 0.5244(10) 0.6968(8) 0.084(13) Uani 1 1 d G U . . . H46 H 0.614778 0.540756 0.722526 0.101 Uiso 1 1 calc R . . . . C45 C 0.6375(18) 0.4745(10) 0.6952(7) 0.064(10) Uani 1 1 d G U . . . C50 C 0.6397(17) 0.4500(9) 0.6567(9) 0.070(10) Uani 1 1 d G U . . . H50 H 0.653916 0.416623 0.655647 0.085 Uiso 1 1 calc R . . . . C183 C 0.650(3) 0.6020(19) 0.3708(16) 0.078(12) Uani 1 1 d . U . . . H183 H 0.685166 0.625461 0.382473 0.094 Uiso 1 1 calc R . . . . C40 C 1.0047(17) 0.4414(15) 0.8147(12) 0.054(9) Uani 1 1 d . . . . . H40 H 1.013268 0.427398 0.841229 0.065 Uiso 1 1 calc R . . . . C4 C 0.756(5) 0.712(3) 0.989(3) 0.13(2) Uani 1 1 d D U . . . C222 C -0.1242(16) 0.4769(16) 0.3143(11) 0.057(10) Uani 1 1 d . . . . . C207 C -0.033(2) 0.6107(18) 0.2830(18) 0.096(16) Uani 1 1 d D U . . . C156 C 0.442(2) 0.6764(16) 0.5168(14) 0.065(10) Uani 1 1 d . U . . . C193 C 0.384(3) 0.3545(15) 0.2150(11) 0.062(10) Uani 1 1 d . . . . . H193 H 0.410742 0.327147 0.203954 0.074 Uiso 1 1 calc R . . . . C181 C 0.601(2) 0.5599(13) 0.3103(14) 0.060(9) Uani 1 1 d . . . . . H181 H 0.599873 0.555641 0.281272 0.072 Uiso 1 1 calc R . . . . C196 C 0.362(3) 0.3263(17) 0.3672(13) 0.070(11) Uani 1 1 d . . . . . H196 H 0.306565 0.329666 0.365760 0.084 Uiso 1 1 calc R . . . . C140 C 0.340(2) 0.3555(16) 0.9514(13) 0.061(9) Uani 1 1 d . U . . . H140 H 0.371072 0.341378 0.972814 0.074 Uiso 1 1 calc R . . . . C18 C 0.695(2) 0.6487(15) 0.7113(14) 0.076(8) Uani 1 1 d D U . . . H18 H 0.681176 0.621256 0.694863 0.091 Uiso 1 1 calc R . . . . C82 C 0.154(2) 0.6615(17) 0.9208(14) 0.069(11) Uani 1 1 d . . . . . H82 H 0.099665 0.666247 0.913406 0.083 Uiso 1 1 calc R . . . . C205 C -0.018(3) 0.5157(19) 0.1652(11) 0.069(12) Uani 1 1 d . . . . . H205 H -0.047491 0.526076 0.141664 0.083 Uiso 1 1 calc R . . . . C16 C 0.665(3) 0.7283(17) 0.7340(13) 0.081(10) Uani 1 1 d D U . . . H16 H 0.633911 0.757176 0.732195 0.098 Uiso 1 1 calc R . . . . C67 C 0.169(2) 0.5247(16) 0.9003(14) 0.063(9) Uani 1 1 d . U . . . H67 H 0.113610 0.522622 0.896715 0.076 Uiso 1 1 calc R . . . . C80 C 0.2920(18) 0.6564(12) 0.8994(11) 0.046(7) Uani 1 1 d . . . . . C17 C 0.653(3) 0.6923(14) 0.7031(14) 0.081(9) Uani 1 1 d D U . . . H17 H 0.619951 0.696951 0.679337 0.097 Uiso 1 1 calc R . . . . C126 C 0.707(3) 0.2992(15) 1.0710(11) 0.061(10) Uani 1 1 d . . . . . H126 H 0.737706 0.273303 1.082013 0.073 Uiso 1 1 calc R . . . . C244 C 0.128(3) 0.3481(17) 0.3050(13) 0.066(10) Uani 1 1 d . U . . . H244 H 0.138681 0.379393 0.294019 0.079 Uiso 1 1 calc R . . . . C148 C 0.000(3) 0.7399(19) 0.3737(13) 0.076(13) Uani 1 1 d . . . . . C242 C 0.167(3) 0.264(2) 0.3176(18) 0.085(13) Uani 1 1 d . U . . . H242 H 0.201042 0.237566 0.312446 0.102 Uiso 1 1 calc R . . . . C253 C 0.324(3) 0.270(2) 0.5422(17) 0.084(13) Uani 1 1 d . U . . . H253 H 0.324966 0.243224 0.560620 0.101 Uiso 1 1 calc R . . . . C252 C 0.255(3) 0.3024(18) 0.5368(15) 0.074(11) Uani 1 1 d . U . . . H252 H 0.209697 0.296207 0.552369 0.088 Uiso 1 1 calc R . . . . C55 C 0.544(3) 0.3153(19) 0.7274(15) 0.077(12) Uani 1 1 d . . . . . H55 H 0.490905 0.304832 0.727100 0.092 Uiso 1 1 calc R . . . . C268 C 0.277(2) 0.3753(14) 0.6154(12) 0.056(8) Uani 1 1 d . . . . . C173 C 0.541(3) 0.4266(18) 0.1755(12) 0.072(12) Uani 1 1 d . . . . . H173 H 0.528797 0.423303 0.146951 0.087 Uiso 1 1 calc R . . . . C248 C -0.026(3) 0.266(2) 0.4927(17) 0.090(17) Uani 1 1 d . . . . . H248 H -0.062843 0.239298 0.492406 0.108 Uiso 1 1 calc R . . . . C224 C -0.149(2) 0.4461(18) 0.2392(14) 0.068(11) Uani 1 1 d . . . . . C153 C 0.312(3) 0.7302(17) 0.5420(14) 0.067(10) Uani 1 1 d . U . . . C234 C -0.076(3) 0.399(2) 0.4161(12) 0.094(15) Uani 1 1 d D U . . . H234 H -0.042198 0.426008 0.421780 0.113 Uiso 1 1 calc R . . . . C233 C -0.073(2) 0.3769(14) 0.3769(12) 0.066(10) Uani 1 1 d D U . . . C215 C -0.166(3) 0.539(2) 0.3794(16) 0.089(17) Uani 1 1 d . . . . . H215 H -0.179450 0.560712 0.401193 0.107 Uiso 1 1 calc R . . . . C249 C -0.025(4) 0.296(2) 0.5264(18) 0.101(19) Uani 1 1 d . . . . . H249 H -0.063750 0.294245 0.546760 0.121 Uiso 1 1 calc R . . . . C23 C 1.039(2) 0.638(2) 0.7485(14) 0.092(16) Uani 1 1 d D . . . . H23 H 1.070952 0.654379 0.728779 0.111 Uiso 1 1 calc R . . . . C251 C 0.255(3) 0.3439(14) 0.5081(12) 0.063(10) Uani 1 1 d . . . . . C95 C 0.522(2) 0.7619(15) 0.8937(14) 0.064(11) Uani 1 1 d . . . . . H95 H 0.466653 0.759346 0.893506 0.077 Uiso 1 1 calc R . . . . C240 C 0.057(4) 0.296(2) 0.351(2) 0.101(17) Uani 1 1 d . U . . . H240 H 0.014341 0.290725 0.368614 0.121 Uiso 1 1 calc R . . . . C116 C 0.592(3) 0.1985(13) 0.9278(11) 0.056(9) Uani 1 1 d . . . . . C256 C 0.332(2) 0.3514(18) 0.4871(15) 0.069(11) Uani 1 1 d . . . . . H256 H 0.338622 0.378498 0.469361 0.083 Uiso 1 1 calc R . . . . C213 C -0.086(2) 0.5243(15) 0.3185(12) 0.059(9) Uani 1 1 d . U . . . C262 C 0.111(2) 0.5505(18) 0.6554(13) 0.065(11) Uani 1 1 d . . . . . H262 H 0.092614 0.576485 0.672057 0.078 Uiso 1 1 calc R . . . . C56 C 0.561(2) 0.3627(18) 0.7380(12) 0.063(10) Uani 1 1 d . . . . . H56 H 0.520437 0.383770 0.746500 0.076 Uiso 1 1 calc R . . . . C254 C 0.386(4) 0.281(2) 0.519(2) 0.103(17) Uani 1 1 d . U . . . H254 H 0.430162 0.260430 0.521041 0.124 Uiso 1 1 calc R . . . . C119 C 0.446(3) 0.1986(16) 0.9692(14) 0.069(10) Uani 1 1 d . U . . . H119 H 0.397988 0.198854 0.983320 0.082 Uiso 1 1 calc R . . . . C11 C 0.969(2) 0.4896(16) 0.9566(12) 0.059(9) Uani 1 1 d . . . . . N5 N 0.990(4) 0.488(2) 1.0667(17) 0.122(17) Uani 1 1 d . U . . . C39 C 1.069(2) 0.4600(15) 0.7922(14) 0.061(10) Uani 1 1 d . . . . . H39 H 1.121073 0.457098 0.803353 0.073 Uiso 1 1 calc R . . . . C96 C 0.559(3) 0.8034(16) 0.9130(16) 0.075(13) Uani 1 1 d . . . . . H96 H 0.527825 0.826767 0.926861 0.090 Uiso 1 1 calc R . . . . C149 C -0.113(2) 0.5715(17) 0.4919(12) 0.062(10) Uani 1 1 d . . . . . C135 C 0.563(3) 0.2667(15) 0.8244(16) 0.093(15) Uani 1 1 d D U . . . H135 H 0.604964 0.264151 0.805544 0.112 Uiso 1 1 calc R . . . . C272 C 0.349(4) 0.3178(18) 0.6581(15) 0.083(14) Uani 1 1 d . . . . . H272 H 0.397210 0.304597 0.668608 0.100 Uiso 1 1 calc R . . . . C127 C 0.695(3) 0.3382(19) 1.0951(14) 0.073(12) Uani 1 1 d . . . . . H127 H 0.720777 0.340417 1.121213 0.088 Uiso 1 1 calc R . . . . C243 C 0.179(3) 0.3085(18) 0.2947(17) 0.079(13) Uani 1 1 d . . . . . H243 H 0.218187 0.311292 0.274385 0.095 Uiso 1 1 calc R . . . . C192 C 0.332(3) 0.3817(17) 0.1897(17) 0.083(14) Uani 1 1 d . . . . . H192 H 0.325295 0.374143 0.161332 0.099 Uiso 1 1 calc R . . . . C98 C 0.683(2) 0.7730(16) 0.8903(14) 0.065(11) Uani 1 1 d . . . . . H98 H 0.739052 0.775943 0.890290 0.078 Uiso 1 1 calc R . . . . C28 C 0.825(2) 0.5037(11) 0.6227(8) 0.066(10) Uani 1 1 d D U . . . C250 C 0.039(3) 0.3309(19) 0.5297(12) 0.071(12) Uani 1 1 d . . . . . H250 H 0.046981 0.349399 0.554196 0.085 Uiso 1 1 calc R . . . . C279 C 0.389(2) 0.5791(18) 0.6396(12) 0.065(11) Uani 1 1 d . . . . . H279 H 0.419001 0.578234 0.664798 0.079 Uiso 1 1 calc R . . . . C223 C -0.1063(18) 0.4412(14) 0.2789(11) 0.051(8) Uani 1 1 d . . . . . C220 C -0.238(2) 0.4195(17) 0.3306(13) 0.064(9) Uani 1 1 d . U . . . H220 H -0.225427 0.398332 0.308605 0.076 Uiso 1 1 calc R . . . . C66 C 0.204(2) 0.517(2) 0.9391(14) 0.080(14) Uani 1 1 d . . . . . H66 H 0.172431 0.513825 0.962744 0.096 Uiso 1 1 calc R . . . . C206 C -0.025(2) 0.5374(17) 0.2042(12) 0.064(10) Uani 1 1 d . U . . . H206 H -0.059704 0.564604 0.205960 0.076 Uiso 1 1 calc R . . . . C212 C -0.113(3) 0.6229(18) 0.2749(19) 0.102(17) Uani 1 1 d D U . . . H212 H -0.152476 0.598386 0.277534 0.122 Uiso 1 1 calc R . . . . C280 C 0.340(3) 0.620(2) 0.6307(16) 0.086(14) Uani 1 1 d . . . . . H280 H 0.338155 0.646685 0.649393 0.104 Uiso 1 1 calc R . . . . N11 N 0.320(3) 0.7476(19) 0.5763(15) 0.096(13) Uani 1 1 d . U . . . C270 C 0.211(4) 0.317(2) 0.6604(17) 0.094(16) Uani 1 1 d . . . . . H270 H 0.164320 0.303871 0.671494 0.113 Uiso 1 1 calc R . . . . C180 C 0.5434(19) 0.5343(14) 0.3355(12) 0.052(8) Uani 1 1 d . . . . . C131 C 0.514(2) 0.4030(13) 0.9875(12) 0.055(9) Uani 1 1 d . . . . . H131 H 0.479644 0.427960 0.978225 0.066 Uiso 1 1 calc R . . . . C30 C 0.839(3) 0.4301(15) 0.5814(14) 0.080(12) Uani 1 1 d D U . . . H30 H 0.841807 0.414629 0.555326 0.096 Uiso 1 1 calc R . . . . C166 C 0.182(3) 0.649(2) 0.1867(16) 0.081(14) Uani 1 1 d . . . . . H166 H 0.142721 0.662174 0.168392 0.097 Uiso 1 1 calc R . . . . C31 C 0.848(4) 0.4018(17) 0.6179(10) 0.098(16) Uani 1 1 d D U . . . H31 H 0.855230 0.367543 0.617331 0.117 Uiso 1 1 calc R . . . . C245 C 0.090(2) 0.3374(15) 0.4962(11) 0.056(8) Uani 1 1 d . U . . . C284 C 0.499(3) 0.4533(17) 0.5039(12) 0.066(10) Uani 1 1 d . U . . . H284 H 0.471752 0.423333 0.501009 0.079 Uiso 1 1 calc R . . . . C122 C 0.617(2) 0.2851(10) 0.9473(11) 0.049(8) Uani 1 1 d D . . . . C21 C 1.0270(17) 0.5966(17) 0.8151(11) 0.067(11) Uani 1 1 d D . . . . H21 H 1.049805 0.585751 0.840539 0.080 Uiso 1 1 calc R . . . . C191 C 0.290(3) 0.422(2) 0.2085(15) 0.083(14) Uani 1 1 d . . . . . H191 H 0.253496 0.440355 0.192088 0.100 Uiso 1 1 calc R . . . . C158 C 0.445(3) 0.6480(15) 0.331(2) 0.082(15) Uani 1 1 d . . . . . H158 H 0.409725 0.637691 0.351256 0.098 Uiso 1 1 calc R . . . . C165 C 0.242(4) 0.677(2) 0.1998(15) 0.086(15) Uani 1 1 d . . . . . H165 H 0.246896 0.709524 0.189465 0.103 Uiso 1 1 calc R . . . . C227 C -0.216(3) 0.4546(19) 0.1580(16) 0.079(12) Uani 1 1 d . U . . . H227 H -0.239023 0.458884 0.131216 0.095 Uiso 1 1 calc R . . . . C138 C 0.432(2) 0.2768(13) 0.8786(13) 0.071(12) Uani 1 1 d D . . . . H138 H 0.386722 0.280889 0.895219 0.086 Uiso 1 1 calc R . . . . C83 C 0.180(3) 0.6581(16) 0.9647(13) 0.064(10) Uani 1 1 d . U . . . H83 H 0.141827 0.658696 0.985819 0.077 Uiso 1 1 calc R . . . . C142 C 0.210(4) 0.378(2) 0.9223(19) 0.092(15) Uani 1 1 d . U . . . H142 H 0.154643 0.381085 0.925072 0.110 Uiso 1 1 calc R . . . . C167 C 0.176(3) 0.603(3) 0.1989(19) 0.10(2) Uani 1 1 d . . . . . H167 H 0.133393 0.584533 0.187939 0.124 Uiso 1 1 calc R . . . . C214 C -0.107(3) 0.5505(19) 0.3550(14) 0.077(12) Uani 1 1 d . U . . . H214 H -0.075719 0.577947 0.362349 0.092 Uiso 1 1 calc R . . . . C286 C 0.617(3) 0.4972(19) 0.4976(14) 0.073(11) Uani 1 1 d . U . . . H286 H 0.671571 0.497791 0.492113 0.087 Uiso 1 1 calc R . . . . C137 C 0.441(3) 0.2339(17) 0.8550(16) 0.098(16) Uani 1 1 d D U . . . H137 H 0.404528 0.208034 0.856873 0.117 Uiso 1 1 calc R . . . . C202 C 0.061(3) 0.4824(18) 0.2370(14) 0.073(12) Uani 1 1 d . . . . . H202 H 0.087913 0.470435 0.261061 0.088 Uiso 1 1 calc R . . . . C221 C -0.1932(18) 0.4640(13) 0.3375(10) 0.045(7) Uani 1 1 d . U . . . C5 C 0.481(3) 0.5366(18) 1.0352(16) 0.074(11) Uani 1 1 d . U . . . N3 N 0.422(2) 0.540(2) 1.0534(18) 0.111(18) Uani 1 1 d . . . . . C285 C 0.578(3) 0.454(2) 0.4916(15) 0.078(12) Uani 1 1 d . U . . . H285 H 0.602774 0.426843 0.479806 0.094 Uiso 1 1 calc R . . . . C218 C -0.319(3) 0.4404(18) 0.3898(14) 0.074(11) Uani 1 1 d . U . . . H218 H -0.362274 0.431548 0.406368 0.089 Uiso 1 1 calc R . . . . C216 C -0.212(3) 0.4943(18) 0.3730(14) 0.071(11) Uani 1 1 d . U . . . C117 C 0.535(3) 0.1560(16) 0.9255(16) 0.077(12) Uani 1 1 d . . . . . H117 H 0.548502 0.128733 0.908989 0.092 Uiso 1 1 calc R . . . . C201 C 0.013(3) 0.5224(15) 0.2405(14) 0.065(10) Uani 1 1 d . . . . . C53 C 0.683(3) 0.2963(19) 0.7175(17) 0.082(13) Uani 1 1 d . U . . . H53 H 0.723904 0.273509 0.713482 0.098 Uiso 1 1 calc R . . . . C54 C 0.604(4) 0.281(3) 0.7167(18) 0.103(19) Uani 1 1 d . . . . . H54 H 0.590528 0.248876 0.709263 0.124 Uiso 1 1 calc R . . . . C182 C 0.655(2) 0.5898(19) 0.3285(16) 0.079(14) Uani 1 1 d . . . . . H182 H 0.696379 0.602647 0.312705 0.094 Uiso 1 1 calc R . . . . C209 C 0.002(3) 0.6964(16) 0.264(2) 0.105(18) Uani 1 1 d D U . . . H209 H 0.040389 0.721411 0.264668 0.125 Uiso 1 1 calc R . . . . C143 C 0.247(3) 0.396(2) 0.8844(19) 0.089(14) Uani 1 1 d . U . . . H143 H 0.219001 0.407181 0.860562 0.107 Uiso 1 1 calc R . . . . C97 C 0.640(3) 0.8091(17) 0.9111(15) 0.076(14) Uani 1 1 d . . . . . H97 H 0.665765 0.836343 0.923459 0.092 Uiso 1 1 calc R . . . . C118 C 0.469(3) 0.155(2) 0.945(2) 0.101(18) Uani 1 1 d . . . . . H118 H 0.436003 0.126983 0.943948 0.121 Uiso 1 1 calc R . . . . N2 N 0.752(6) 0.736(3) 1.019(3) 0.18(3) Uani 1 1 d D U . . . C247 C 0.025(3) 0.272(2) 0.4571(18) 0.096(17) Uani 1 1 d . . . . . H247 H 0.018516 0.252494 0.432876 0.115 Uiso 1 1 calc R . . . . C9 C 0.975(3) 0.498(2) 1.0322(16) 0.083(13) Uani 1 1 d . U . . . C136 C 0.506(3) 0.229(2) 0.8285(18) 0.106(18) Uani 1 1 d D U . . . H136 H 0.511906 0.200406 0.813018 0.127 Uiso 1 1 calc R . . . . C271 C 0.284(3) 0.2998(19) 0.6721(17) 0.082(14) Uani 1 1 d . . . . . H271 H 0.286582 0.273555 0.691119 0.098 Uiso 1 1 calc R . . . . C226 C -0.238(3) 0.488(2) 0.1917(15) 0.078(13) Uani 1 1 d . . . . . H226 H -0.276120 0.512554 0.187056 0.093 Uiso 1 1 calc R . . . . C144 C 0.327(3) 0.3953(19) 0.8878(17) 0.082(13) Uani 1 1 d . U . . . H144 H 0.353003 0.411417 0.866226 0.099 Uiso 1 1 calc R . . . . C236 C -0.173(3) 0.3428(19) 0.4346(17) 0.099(16) Uani 1 1 d D U . . . H236 H -0.204705 0.329706 0.455517 0.119 Uiso 1 1 calc R . . . . N1 N 0.928(4) 0.756(2) 0.933(2) 0.14(2) Uani 1 1 d . . . . . C22 C 1.071(3) 0.6248(17) 0.7875(12) 0.081(13) Uani 1 1 d D U . . . H22 H 1.123100 0.634685 0.795282 0.097 Uiso 1 1 calc R . . . . C237 C -0.180(3) 0.318(2) 0.3965(15) 0.103(17) Uani 1 1 d D U . . . H237 H -0.212907 0.290520 0.391102 0.124 Uiso 1 1 calc R . . . . C238 C -0.129(3) 0.3394(18) 0.3679(17) 0.096(16) Uani 1 1 d D U . . . H238 H -0.131612 0.327791 0.340331 0.116 Uiso 1 1 calc R . . . . C235 C -0.128(3) 0.384(2) 0.4475(17) 0.105(18) Uani 1 1 d D U . . . H235 H -0.131507 0.398983 0.473677 0.126 Uiso 1 1 calc R . . . . C210 C -0.079(3) 0.707(2) 0.256(3) 0.13(2) Uani 1 1 d D U . . . H210 H -0.094167 0.737524 0.245463 0.158 Uiso 1 1 calc R . . . . C211 C -0.137(3) 0.6705(16) 0.2629(18) 0.093(15) Uani 1 1 d D U . . . H211 H -0.191188 0.678210 0.259675 0.111 Uiso 1 1 calc R . . . . C241 C 0.110(4) 0.257(3) 0.346(2) 0.11(2) Uani 1 1 d . U . . . H241 H 0.106297 0.228056 0.361810 0.138 Uiso 1 1 calc R . . . . C52 C 0.699(3) 0.3433(17) 0.7239(14) 0.071(11) Uani 1 1 d . U . . . H52 H 0.751422 0.353282 0.720038 0.085 Uiso 1 1 calc R . . . . C217 C -0.278(3) 0.483(2) 0.3991(16) 0.082(13) Uani 1 1 d . U . . . H217 H -0.292748 0.503704 0.421136 0.099 Uiso 1 1 calc R . . . . C219 C -0.298(3) 0.4083(19) 0.3552(15) 0.075(12) Uani 1 1 d . U . . . H219 H -0.327821 0.379376 0.350216 0.090 Uiso 1 1 calc R . . . . C287 C 0.582(4) 0.541(2) 0.5114(18) 0.095(15) Uani 1 1 d . U . . . H287 H 0.610145 0.570752 0.512740 0.114 Uiso 1 1 calc R . . . . C15 C 0.719(3) 0.7236(17) 0.7673(15) 0.088(10) Uani 1 1 d D U . . . H15 H 0.724978 0.748390 0.787592 0.105 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au7 0.0261(5) 0.0439(7) 0.0429(6) 0.0020(5) -0.0025(4) -0.0004(5) Au15 0.0317(6) 0.0449(7) 0.0378(6) -0.0016(5) -0.0009(4) -0.0013(5) Au3 0.0254(5) 0.0458(7) 0.0457(7) 0.0017(5) -0.0021(5) 0.0007(5) Au5 0.0335(6) 0.0439(7) 0.0414(6) 0.0019(5) 0.0015(5) 0.0025(5) Au13 0.0331(6) 0.0552(8) 0.0388(6) -0.0002(5) -0.0042(5) -0.0002(5) Au2 0.0267(5) 0.0435(7) 0.0569(8) 0.0012(6) -0.0014(5) 0.0014(5) Au12 0.0462(7) 0.0546(8) 0.0384(6) 0.0033(5) -0.0029(5) -0.0098(6) Au4 0.0304(6) 0.0485(7) 0.0488(7) 0.0091(5) 0.0036(5) 0.0004(5) Au14 0.0339(6) 0.0489(8) 0.0542(8) -0.0032(6) -0.0055(5) -0.0022(5) Au6 0.0270(5) 0.0540(8) 0.0506(7) -0.0015(6) -0.0020(5) -0.0005(5) Au8 0.0295(6) 0.0719(9) 0.0404(7) -0.0020(6) 0.0002(5) 0.0049(6) Au9 0.0386(6) 0.0490(7) 0.0442(7) 0.0043(5) 0.0056(5) 0.0024(5) Au11 0.0400(6) 0.0573(8) 0.0397(6) -0.0019(6) -0.0039(5) -0.0087(6) Au1 0.0341(6) 0.0499(8) 0.0614(8) 0.0087(6) 0.0112(5) 0.0037(5) Au10 0.0422(7) 0.0599(9) 0.0471(7) 0.0037(6) -0.0120(6) -0.0067(6) Au16 0.0417(7) 0.0577(9) 0.0586(8) -0.0102(7) 0.0134(6) -0.0016(6) Cu5 0.039(2) 0.040(2) 0.051(3) -0.0031(19) 0.0029(19) 0.0006(18) Cu2 0.041(2) 0.060(3) 0.038(2) -0.002(2) -0.0018(18) 0.007(2) Cu6 0.031(2) 0.067(3) 0.046(3) -0.009(2) -0.0028(18) 0.000(2) Cu1 0.031(2) 0.054(3) 0.062(3) -0.006(2) -0.010(2) -0.005(2) Cu7 0.034(2) 0.068(3) 0.062(3) -0.008(2) 0.004(2) 0.003(2) Cu3 0.041(3) 0.070(3) 0.065(3) -0.012(3) 0.003(2) 0.001(2) Cu8 0.042(3) 0.052(3) 0.076(4) -0.001(3) 0.001(2) -0.003(2) Cu4 0.035(2) 0.072(4) 0.068(3) 0.001(3) -0.005(2) -0.007(2) P5 0.036(4) 0.043(4) 0.047(4) 0.007(3) 0.006(3) 0.007(3) P11 0.030(4) 0.070(6) 0.035(4) -0.002(3) -0.007(3) 0.001(3) P2 0.029(3) 0.040(4) 0.053(4) -0.005(3) -0.003(3) 0.001(3) P3 0.019(3) 0.050(5) 0.056(5) 0.001(3) -0.006(3) 0.001(3) P6 0.029(3) 0.073(6) 0.031(4) -0.003(3) 0.005(3) -0.001(4) S9 0.033(4) 0.082(6) 0.046(4) -0.003(4) -0.002(3) -0.007(4) P7 0.040(4) 0.043(4) 0.046(4) 0.006(3) 0.011(3) -0.001(3) P4 0.028(3) 0.043(4) 0.052(4) 0.003(3) 0.006(3) -0.008(3) P12 0.039(4) 0.048(4) 0.044(4) 0.002(3) 0.013(3) 0.007(3) S12 0.029(3) 0.055(5) 0.068(5) -0.010(4) 0.003(3) -0.008(3) S3 0.029(3) 0.066(5) 0.067(5) -0.010(4) 0.000(3) 0.007(3) P1 0.036(4) 0.058(5) 0.065(5) 0.021(4) 0.013(4) 0.006(4) P10 0.053(5) 0.056(5) 0.037(4) 0.009(3) -0.006(3) -0.011(4) P8 0.041(4) 0.066(6) 0.051(5) -0.002(4) -0.026(4) 0.000(4) S7 0.045(4) 0.056(5) 0.059(5) 0.007(4) 0.001(4) -0.003(4) P9 0.049(5) 0.051(5) 0.046(4) 0.001(4) 0.003(4) -0.012(4) S8 0.028(3) 0.071(6) 0.054(5) 0.000(4) 0.001(3) 0.005(3) S2 0.039(4) 0.060(5) 0.083(7) -0.025(5) -0.003(4) 0.003(4) S6 0.026(3) 0.090(6) 0.049(4) 0.001(4) -0.002(3) 0.002(4) S4 0.050(4) 0.071(5) 0.036(4) -0.003(4) -0.003(3) 0.005(4) S11 0.045(5) 0.055(5) 0.093(7) -0.022(5) 0.003(4) 0.003(4) S10 0.037(4) 0.070(6) 0.046(4) -0.010(4) 0.001(3) 0.005(4) S5 0.048(5) 0.090(7) 0.059(5) -0.013(5) -0.014(4) -0.002(5) S1 0.045(5) 0.067(6) 0.082(7) 0.009(5) -0.007(4) -0.015(4) C73 0.05(2) 0.07(2) 0.049(19) 0.002(16) 0.013(15) -0.005(17) C276 0.032(14) 0.08(2) 0.038(16) -0.016(16) -0.003(12) -0.002(15) C72 0.035(14) 0.049(18) 0.038(15) 0.000(12) -0.002(11) 0.013(13) C163 0.06(2) 0.06(2) 0.027(14) 0.008(13) 0.002(13) -0.003(16) C79 0.025(12) 0.041(15) 0.037(14) -0.001(11) 0.000(10) 0.004(11) C257 0.044(16) 0.047(17) 0.041(16) 0.005(13) -0.016(13) -0.004(13) C94 0.041(16) 0.054(19) 0.040(16) -0.011(14) 0.004(13) 0.004(14) C69 0.027(13) 0.034(15) 0.07(2) -0.019(14) 0.007(13) -0.009(11) C93 0.034(15) 0.041(17) 0.07(2) 0.018(16) 0.003(15) -0.008(13) C91 0.018(13) 0.10(3) 0.06(2) 0.01(2) -0.012(13) -0.002(16) C189 0.038(16) 0.039(17) 0.07(2) -0.015(15) 0.025(15) -0.011(13) N4 0.10(2) 0.12(2) 0.053(17) -0.003(17) 0.014(16) -0.007(19) C35 0.044(18) 0.07(2) 0.046(18) 0.004(16) -0.014(14) 0.004(16) C92 0.035(17) 0.07(3) 0.08(3) 0.01(2) 0.007(17) -0.009(16) C68 0.030(17) 0.08(3) 0.10(3) 0.01(2) 0.020(18) -0.001(17) C2 0.044(12) 0.052(13) 0.061(13) -0.001(11) -0.012(10) -0.005(10) C231 0.06(2) 0.07(2) 0.045(19) 0.016(17) 0.002(16) -0.015(18) C125 0.046(18) 0.08(3) 0.046(19) 0.019(17) -0.005(15) -0.007(17) C114 0.06(2) 0.05(2) 0.05(2) -0.001(16) -0.001(17) 0.014(17) C60 0.079(16) 0.072(15) 0.069(15) -0.004(12) -0.010(12) 0.001(12) C59 0.052(12) 0.063(13) 0.029(10) -0.007(10) -0.009(9) 0.007(10) C132 0.039(16) 0.057(19) 0.037(15) 0.010(13) 0.014(12) 0.001(14) C78 0.027(13) 0.07(2) 0.028(13) -0.005(13) 0.001(10) -0.008(13) C185 0.044(18) 0.11(3) 0.041(18) 0.015(19) -0.019(14) -0.04(2) C88 0.06(2) 0.05(2) 0.07(2) -0.009(17) -0.018(18) -0.003(17) C100 0.019(13) 0.08(3) 0.07(2) -0.005(19) -0.011(14) -0.005(14) C174 0.06(2) 0.06(2) 0.08(3) -0.01(2) 0.006(19) 0.009(18) C267 0.052(18) 0.043(16) 0.031(14) 0.005(12) -0.022(13) 0.005(13) C107 0.031(15) 0.041(17) 0.07(2) 0.011(15) 0.008(14) -0.002(12) C74 0.045(19) 0.07(2) 0.07(2) 0.016(18) -0.002(16) 0.019(17) C19 0.049(18) 0.07(2) 0.049(19) 0.011(16) 0.023(15) 0.001(17) C34 0.021(12) 0.08(2) 0.040(16) 0.011(15) -0.004(11) 0.001(14) C275 0.045(19) 0.07(3) 0.06(2) 0.000(18) -0.015(16) 0.003(17) C37 0.032(16) 0.09(3) 0.07(2) 0.02(2) -0.011(16) -0.005(17) C42 0.038(16) 0.06(2) 0.043(16) 0.005(14) -0.008(13) 0.016(14) C43 0.022(12) 0.060(19) 0.034(14) 0.004(12) 0.011(10) 0.002(12) C44 0.022(9) 0.049(12) 0.044(11) -0.009(10) -0.004(8) -0.001(9) C124 0.052(19) 0.06(2) 0.040(17) -0.004(14) -0.005(14) -0.006(15) C24 0.05(2) 0.14(4) 0.07(3) -0.01(3) 0.016(19) -0.05(3) C259 0.041(17) 0.11(3) 0.026(14) 0.014(16) 0.009(12) 0.019(18) C106 0.041(16) 0.06(2) 0.036(16) 0.012(14) 0.008(13) 0.003(14) C75 0.055(19) 0.040(17) 0.050(18) 0.002(14) 0.005(15) 0.005(14) C71 0.06(2) 0.06(2) 0.047(19) 0.005(15) -0.001(16) -0.009(17) C178 0.029(14) 0.038(16) 0.07(2) 0.006(14) 0.002(13) -0.002(12) C77 0.024(12) 0.034(15) 0.07(2) 0.010(13) 0.000(12) -0.006(11) C258 0.031(14) 0.049(18) 0.06(2) 0.002(15) -0.014(13) -0.009(13) C157 0.06(2) 0.05(2) 0.07(2) 0.003(17) 0.007(18) 0.020(17) C188 0.028(13) 0.049(18) 0.055(18) -0.014(14) 0.000(12) 0.003(12) C265 0.042(16) 0.043(17) 0.049(17) 0.004(13) 0.008(13) -0.002(13) C274 0.05(2) 0.05(2) 0.10(3) 0.01(2) -0.01(2) 0.003(17) C263 0.06(2) 0.12(4) 0.05(2) -0.01(2) -0.029(19) 0.00(2) C190 0.06(2) 0.06(2) 0.048(19) 0.010(16) 0.012(16) 0.006(17) C266 0.043(16) 0.043(17) 0.044(16) 0.004(13) -0.009(12) -0.008(13) C51 0.036(16) 0.08(3) 0.06(2) -0.003(18) 0.012(15) 0.012(16) C41 0.021(13) 0.054(19) 0.059(19) 0.002(15) -0.004(12) -0.004(12) C8 0.060(13) 0.066(14) 0.053(13) -0.003(11) 0.005(11) 0.002(11) C20 0.05(2) 0.09(3) 0.06(2) 0.01(2) 0.033(18) -0.005(19) C145 0.05(2) 0.04(2) 0.11(3) 0.01(2) 0.00(2) 0.019(17) C3 0.050(12) 0.050(13) 0.064(13) -0.011(11) -0.014(11) -0.004(10) C7 0.08(2) 0.07(2) 0.016(12) 0.005(13) 0.008(13) -0.008(19) C6 0.06(2) 0.036(17) 0.06(2) -0.006(14) 0.029(17) 0.003(15) C61 0.09(3) 0.06(3) 0.11(4) 0.00(2) 0.00(3) -0.03(2) C65 0.075(16) 0.083(16) 0.074(16) 0.013(12) 0.007(12) -0.002(12) C63 0.030(14) 0.049(18) 0.060(19) -0.013(15) 0.005(13) 0.008(13) C277 0.040(11) 0.055(12) 0.040(11) 0.005(10) 0.000(9) -0.001(10) C273 0.07(2) 0.041(18) 0.06(2) 0.009(15) -0.008(18) 0.009(17) C87 0.042(18) 0.08(3) 0.041(18) -0.007(16) -0.010(14) -0.009(17) C57 0.024(9) 0.038(11) 0.043(11) -0.004(9) -0.010(8) -0.001(9) C99 0.034(17) 0.07(2) 0.07(3) -0.012(19) -0.018(16) -0.001(16) C129 0.042(17) 0.07(2) 0.039(16) 0.003(15) 0.012(13) -0.019(16) C26 0.058(13) 0.063(14) 0.061(14) 0.010(11) -0.003(11) -0.002(11) C1 0.05(2) 0.07(3) 0.10(3) -0.03(2) -0.02(2) -0.013(19) C177 0.051(18) 0.05(2) 0.045(17) 0.002(14) 0.013(14) -0.005(15) C108 0.10(3) 0.07(2) 0.04(2) -0.014(17) 0.03(2) -0.01(2) C239 0.033(15) 0.07(2) 0.038(16) 0.002(15) -0.017(12) -0.007(15) C164 0.07(3) 0.07(3) 0.05(2) 0.014(18) -0.007(18) 0.01(2) C112 0.058(14) 0.066(14) 0.063(14) 0.008(11) -0.010(11) 0.007(11) C25 0.040(11) 0.055(13) 0.047(12) 0.013(10) 0.004(10) -0.001(10) C162 0.05(2) 0.048(19) 0.07(2) 0.032(17) -0.008(17) -0.014(16) C111 0.077(16) 0.085(17) 0.083(17) 0.007(13) 0.000(12) 0.010(12) C169 0.041(17) 0.045(18) 0.07(2) -0.003(16) -0.016(16) 0.011(14) C133 0.064(14) 0.057(14) 0.056(13) -0.005(11) 0.004(11) 0.007(11) C10 0.08(3) 0.09(3) 0.04(2) -0.02(2) -0.010(18) 0.01(2) C194 0.041(16) 0.040(17) 0.055(19) -0.001(14) 0.011(14) 0.006(13) C168 0.05(2) 0.06(2) 0.09(3) 0.03(2) 0.00(2) -0.005(18) N6 0.07(2) 0.15(4) 0.05(2) 0.02(2) 0.013(17) 0.02(3) C260 0.047(17) 0.07(2) 0.032(15) 0.011(14) 0.009(12) -0.010(15) C101 0.047(18) 0.05(2) 0.06(2) -0.005(16) 0.014(16) 0.006(15) C195 0.06(2) 0.07(3) 0.039(17) 0.009(16) 0.004(15) 0.018(19) C121 0.06(2) 0.051(19) 0.043(17) 0.016(14) -0.013(15) -0.007(16) C81 0.030(15) 0.08(3) 0.052(19) -0.010(17) -0.004(13) -0.009(15) C115 0.11(3) 0.032(17) 0.040(17) 0.004(13) 0.004(18) 0.006(18) C171 0.048(19) 0.08(3) 0.06(2) 0.01(2) 0.005(16) -0.002(18) C86 0.07(3) 0.07(3) 0.07(3) -0.02(2) -0.03(2) 0.00(2) C113 0.042(18) 0.05(2) 0.08(2) -0.003(17) -0.012(17) 0.014(15) C264 0.033(16) 0.08(3) 0.07(3) -0.01(2) -0.008(16) -0.012(17) C232 0.038(16) 0.050(19) 0.06(2) -0.020(15) 0.012(14) -0.013(14) C203 0.040(19) 0.08(3) 0.11(4) -0.03(3) 0.00(2) 0.008(19) C70 0.020(12) 0.056(19) 0.059(19) 0.007(15) -0.004(12) 0.002(12) C154 0.045(18) 0.041(19) 0.10(3) -0.014(18) 0.021(19) 0.006(15) C58 0.036(11) 0.056(12) 0.031(10) 0.007(9) -0.013(9) 0.004(10) C208 0.067(15) 0.070(15) 0.076(15) 0.001(12) -0.016(12) -0.003(12) C130 0.06(2) 0.07(2) 0.047(19) -0.016(16) 0.009(16) -0.009(18) C225 0.08(3) 0.10(3) 0.029(16) 0.006(17) -0.006(16) -0.01(2) C90 0.06(2) 0.07(2) 0.041(18) -0.006(16) 0.001(16) 0.001(18) C155 0.05(2) 0.043(19) 0.09(3) -0.013(18) -0.003(19) -0.001(16) C161 0.07(3) 0.05(2) 0.15(5) -0.01(3) 0.02(3) 0.00(2) C151 0.039(16) 0.05(2) 0.06(2) -0.002(16) 0.013(15) 0.010(15) C38 0.029(16) 0.10(3) 0.08(3) 0.02(2) 0.001(16) -0.011(18) C147 0.042(18) 0.033(17) 0.11(3) -0.009(18) -0.008(19) 0.004(14) C146 0.07(2) 0.06(2) 0.05(2) 0.006(17) 0.005(17) -0.004(18) C14 0.088(15) 0.085(13) 0.078(14) 0.003(10) 0.004(11) 0.001(10) C186 0.06(2) 0.07(3) 0.044(18) -0.001(17) 0.008(15) 0.004(19) C187 0.051(18) 0.037(16) 0.047(17) 0.005(13) 0.013(14) -0.011(14) C230 0.08(3) 0.07(3) 0.040(18) -0.011(17) -0.015(17) 0.00(2) C228 0.07(3) 0.07(3) 0.09(3) 0.00(2) -0.01(2) -0.03(2) C150 0.033(15) 0.047(18) 0.06(2) 0.016(15) 0.017(14) -0.002(13) C62 0.05(2) 0.05(2) 0.07(2) -0.012(17) -0.003(17) 0.010(16) C200 0.08(3) 0.05(2) 0.10(3) 0.03(2) 0.03(3) 0.02(2) C170 0.07(2) 0.07(2) 0.020(13) 0.008(13) 0.024(13) 0.010(18) C160 0.04(2) 0.05(2) 0.17(5) 0.00(3) -0.02(3) -0.006(17) C176 0.026(14) 0.09(3) 0.054(19) -0.002(17) 0.008(13) 0.017(15) C104 0.05(2) 0.09(3) 0.10(4) 0.02(3) 0.03(2) 0.02(2) C109 0.08(3) 0.10(4) 0.06(2) 0.00(2) 0.00(2) 0.01(3) C27 0.060(14) 0.080(15) 0.065(14) 0.006(12) 0.001(11) -0.002(12) C64 0.032(15) 0.09(3) 0.051(19) 0.022(18) -0.006(13) -0.012(16) C283 0.030(15) 0.11(3) 0.036(16) 0.006(18) -0.010(12) 0.002(18) C152 0.05(2) 0.06(2) 0.06(2) 0.000(17) 0.017(16) 0.011(17) C110 0.079(16) 0.084(17) 0.079(16) 0.004(12) -0.001(12) 0.005(12) C199 0.086(18) 0.093(18) 0.089(18) 0.007(13) 0.004(13) 0.006(13) C179 0.055(18) 0.07(2) 0.027(14) 0.012(14) 0.013(12) 0.019(16) C281 0.07(3) 0.08(3) 0.08(3) -0.01(2) -0.03(2) 0.00(2) C85 0.07(2) 0.054(19) 0.023(13) 0.009(12) 0.007(13) 0.005(16) C139 0.041(18) 0.041(18) 0.09(3) 0.006(17) 0.005(18) -0.009(14) C175 0.040(18) 0.08(3) 0.08(3) 0.01(2) 0.006(17) 0.006(17) C269 0.06(2) 0.07(3) 0.08(3) 0.03(2) -0.01(2) -0.01(2) C76 0.035(15) 0.06(2) 0.06(2) -0.019(16) -0.008(14) 0.006(14) C33 0.032(16) 0.09(3) 0.06(2) 0.01(2) -0.004(15) -0.011(17) C159 0.06(2) 0.07(3) 0.09(3) 0.00(2) -0.03(2) -0.03(2) N10 0.09(3) 0.09(3) 0.13(4) -0.02(3) 0.05(3) 0.01(2) C229 0.069(15) 0.070(15) 0.061(14) 0.001(12) -0.007(11) -0.009(12) C246 0.08(3) 0.07(2) 0.031(16) 0.013(15) -0.010(16) -0.02(2) C261 0.042(19) 0.07(2) 0.10(3) -0.01(2) 0.021(19) 0.011(17) C89 0.054(19) 0.043(18) 0.053(19) -0.012(14) 0.026(15) -0.003(14) C120 0.06(2) 0.041(19) 0.08(3) 0.017(17) 0.018(19) -0.004(16) C204 0.07(3) 0.09(3) 0.06(2) 0.01(2) 0.00(2) -0.03(2) N9 0.040(18) 0.13(4) 0.11(3) 0.01(3) 0.024(19) -0.02(2) C128 0.06(2) 0.09(3) 0.07(3) -0.02(2) 0.02(2) -0.02(2) C13 0.073(13) 0.069(11) 0.067(13) 0.017(9) 0.006(10) -0.008(10) C278 0.039(16) 0.07(2) 0.034(16) 0.002(14) -0.006(12) -0.002(15) C184 0.09(3) 0.06(2) 0.06(2) -0.005(18) -0.03(2) -0.01(2) C198 0.088(17) 0.077(17) 0.081(17) 0.003(12) 0.003(13) 0.005(13) C84 0.06(2) 0.07(3) 0.06(2) -0.018(19) 0.004(18) -0.014(19) C134 0.059(14) 0.073(15) 0.067(14) -0.007(12) 0.009(11) 0.015(12) C123 0.053(19) 0.08(2) 0.035(16) -0.001(15) 0.016(14) -0.022(17) C32 0.068(15) 0.074(15) 0.065(14) -0.008(12) 0.004(12) -0.002(12) C12 0.041(19) 0.07(3) 0.09(3) 0.03(2) -0.014(18) 0.015(19) C197 0.086(17) 0.081(17) 0.077(16) 0.004(12) 0.007(12) 0.002(13) C172 0.05(2) 0.06(2) 0.08(3) 0.010(19) 0.035(18) 0.007(17) C141 0.090(19) 0.099(19) 0.100(19) 0.001(13) 0.013(13) -0.005(13) N7 0.07(2) 0.08(3) 0.15(4) 0.05(3) 0.00(3) 0.01(2) C282 0.06(2) 0.07(3) 0.07(3) 0.00(2) 0.016(19) 0.02(2) N8 0.10(2) 0.12(3) 0.12(3) 0.00(2) -0.01(2) 0.05(2) C29 0.05(2) 0.15(5) 0.05(2) 0.00(3) -0.001(17) -0.01(2) N12 0.07(3) 0.14(4) 0.07(2) -0.02(2) -0.03(2) 0.00(2) C255 0.076(17) 0.093(18) 0.089(18) -0.009(13) -0.001(13) 0.004(13) C103 0.06(3) 0.08(3) 0.10(4) -0.01(3) 0.03(3) 0.01(2) C288 0.033(16) 0.12(3) 0.048(19) -0.01(2) 0.006(14) -0.020(19) C36 0.034(15) 0.048(18) 0.052(17) 0.014(14) -0.014(13) -0.004(13) C102 0.10(4) 0.06(3) 0.09(3) 0.00(2) 0.02(3) 0.00(3) C105 0.043(19) 0.09(3) 0.07(3) 0.01(2) 0.010(17) 0.008(18) C49 0.067(15) 0.094(16) 0.065(15) 0.001(12) -0.005(12) -0.012(12) C48 0.069(16) 0.096(17) 0.079(16) 0.013(13) -0.005(12) -0.010(12) C47 0.083(17) 0.089(18) 0.089(18) 0.016(13) 0.003(13) 0.001(13) C46 0.082(17) 0.086(17) 0.085(17) 0.009(13) -0.001(12) 0.000(13) C45 0.057(14) 0.071(15) 0.066(14) -0.004(12) 0.007(11) -0.011(11) C50 0.062(14) 0.087(16) 0.062(14) -0.002(12) -0.001(11) -0.001(12) C183 0.075(16) 0.076(16) 0.083(16) 0.004(12) -0.009(12) -0.004(12) C40 0.023(14) 0.08(2) 0.06(2) 0.005(18) -0.013(13) 0.002(15) C4 0.13(3) 0.13(3) 0.13(3) -0.010(14) 0.001(14) -0.006(14) C222 0.010(11) 0.10(3) 0.055(19) 0.016(19) -0.004(12) 0.014(14) C207 0.095(19) 0.096(19) 0.096(19) 0.000(13) 0.005(13) -0.002(13) C156 0.058(14) 0.065(14) 0.074(15) -0.011(12) -0.001(12) 0.001(11) C193 0.08(3) 0.06(2) 0.044(19) -0.024(17) 0.021(18) 0.02(2) C181 0.06(2) 0.040(18) 0.08(3) 0.014(18) 0.004(18) -0.004(16) C196 0.07(3) 0.07(3) 0.06(2) 0.01(2) -0.01(2) -0.01(2) C140 0.052(13) 0.068(14) 0.065(14) 0.011(11) 0.017(11) -0.012(11) C18 0.073(14) 0.077(12) 0.077(13) 0.014(11) 0.003(10) 0.000(10) C82 0.05(2) 0.09(3) 0.07(3) -0.03(2) 0.021(18) 0.001(19) C205 0.06(2) 0.11(4) 0.029(16) 0.013(19) -0.004(15) 0.00(2) C16 0.06(2) 0.072(19) 0.11(3) 0.006(16) 0.003(18) -0.014(16) C67 0.052(13) 0.066(14) 0.073(14) 0.005(12) 0.013(11) -0.008(11) C80 0.030(14) 0.047(18) 0.06(2) -0.013(14) -0.009(13) -0.009(12) C17 0.074(14) 0.083(13) 0.087(14) 0.006(10) 0.003(11) 0.008(11) C126 0.09(3) 0.05(2) 0.042(18) 0.010(15) -0.003(17) -0.005(19) C244 0.063(14) 0.069(15) 0.065(14) -0.003(12) -0.009(11) 0.002(12) C148 0.09(3) 0.09(3) 0.05(2) 0.01(2) 0.01(2) 0.04(3) C242 0.079(17) 0.082(17) 0.095(18) -0.001(13) 0.005(13) 0.012(13) C253 0.090(17) 0.080(17) 0.082(17) 0.003(12) -0.002(13) 0.002(13) C252 0.076(16) 0.074(16) 0.070(15) -0.003(12) -0.003(12) 0.009(12) C55 0.07(3) 0.08(3) 0.08(3) -0.01(2) -0.01(2) 0.00(2) C268 0.05(2) 0.05(2) 0.06(2) -0.002(16) 0.000(16) -0.004(16) C173 0.08(3) 0.10(3) 0.042(19) -0.02(2) 0.021(18) 0.02(2) C248 0.09(4) 0.09(4) 0.09(4) 0.03(3) -0.01(3) -0.04(3) C224 0.040(18) 0.09(3) 0.07(3) 0.00(2) -0.010(17) -0.010(19) C153 0.064(14) 0.073(15) 0.063(14) -0.009(12) 0.001(11) 0.001(12) C234 0.092(19) 0.094(19) 0.096(19) 0.005(13) 0.001(13) 0.009(13) C233 0.068(15) 0.067(15) 0.065(14) 0.009(11) 0.009(12) 0.002(12) C215 0.06(3) 0.14(5) 0.07(3) -0.02(3) -0.03(2) 0.02(3) C249 0.11(4) 0.11(4) 0.08(3) -0.01(3) 0.06(3) -0.04(3) C23 0.06(3) 0.12(4) 0.10(4) 0.01(3) -0.01(3) -0.04(3) C251 0.09(3) 0.05(2) 0.05(2) -0.006(16) 0.000(19) 0.003(19) C95 0.047(19) 0.07(2) 0.08(3) -0.04(2) 0.006(18) -0.008(17) C240 0.10(2) 0.10(2) 0.10(2) 0.000(13) 0.019(13) 0.004(13) C116 0.08(3) 0.041(18) 0.045(18) 0.006(14) -0.007(17) -0.009(17) C256 0.033(17) 0.09(3) 0.09(3) 0.00(2) 0.011(18) 0.001(18) C213 0.061(13) 0.056(13) 0.059(13) 0.000(11) -0.008(11) 0.004(11) C262 0.036(17) 0.10(3) 0.06(2) -0.01(2) 0.019(15) 0.010(18) C56 0.05(2) 0.09(3) 0.05(2) 0.000(19) 0.005(16) -0.004(19) C254 0.10(2) 0.10(2) 0.11(2) -0.010(13) 0.000(13) 0.010(13) C119 0.074(15) 0.063(15) 0.069(15) 0.008(12) 0.009(12) -0.001(12) C11 0.05(2) 0.07(3) 0.05(2) 0.006(17) -0.005(16) 0.007(18) N5 0.14(3) 0.15(3) 0.08(2) 0.00(2) -0.03(2) 0.01(2) C39 0.033(16) 0.06(2) 0.09(3) 0.015(19) -0.004(17) 0.002(15) C96 0.08(3) 0.05(2) 0.10(3) -0.04(2) 0.00(2) 0.00(2) C149 0.05(2) 0.08(3) 0.05(2) 0.011(18) -0.006(16) -0.001(19) C135 0.095(19) 0.095(19) 0.088(18) -0.008(13) 0.000(13) 0.007(13) C272 0.11(4) 0.07(3) 0.07(3) 0.02(2) -0.03(3) 0.01(3) C127 0.08(3) 0.09(3) 0.06(2) 0.00(2) 0.01(2) 0.00(2) C243 0.08(3) 0.07(3) 0.09(3) -0.02(2) 0.01(2) 0.01(2) C192 0.11(4) 0.06(3) 0.08(3) -0.02(2) 0.01(3) -0.01(3) C98 0.035(17) 0.07(3) 0.09(3) -0.01(2) -0.036(18) -0.013(17) C28 0.062(14) 0.076(15) 0.060(14) 0.000(12) 0.000(11) -0.006(12) C250 0.06(2) 0.11(3) 0.04(2) 0.01(2) 0.014(17) -0.02(2) C279 0.05(2) 0.10(3) 0.045(19) -0.010(19) -0.024(16) -0.01(2) C223 0.031(15) 0.07(2) 0.053(19) -0.011(16) -0.014(13) -0.018(15) C220 0.052(13) 0.077(15) 0.062(14) 0.000(12) 0.003(11) 0.004(11) C66 0.041(19) 0.13(4) 0.07(3) 0.03(3) 0.034(18) 0.02(2) C206 0.062(14) 0.072(15) 0.057(14) 0.003(11) -0.007(11) -0.008(11) C212 0.10(2) 0.10(2) 0.11(2) -0.001(13) 0.002(13) 0.005(13) C280 0.07(3) 0.11(4) 0.07(3) -0.02(3) 0.00(2) -0.01(3) N11 0.09(2) 0.11(2) 0.09(2) -0.030(19) 0.005(18) 0.021(19) C270 0.11(4) 0.08(3) 0.09(4) 0.02(3) -0.02(3) -0.01(3) C180 0.038(16) 0.05(2) 0.06(2) 0.004(16) 0.007(14) 0.003(14) C131 0.052(19) 0.043(18) 0.07(2) 0.000(16) 0.028(17) 0.009(15) C30 0.081(16) 0.087(17) 0.073(16) 0.000(12) -0.001(12) 0.004(13) C166 0.06(3) 0.11(4) 0.07(3) 0.04(3) 0.01(2) 0.01(3) C31 0.095(19) 0.10(2) 0.095(19) -0.005(13) 0.001(13) -0.003(13) C245 0.059(13) 0.062(13) 0.047(12) 0.003(11) -0.021(11) -0.005(11) C284 0.066(14) 0.076(15) 0.054(13) 0.001(11) -0.007(11) 0.003(12) C122 0.057(19) 0.025(14) 0.06(2) 0.009(13) 0.015(16) 0.004(13) C21 0.045(19) 0.11(3) 0.045(19) 0.02(2) 0.002(15) 0.00(2) C191 0.07(3) 0.12(4) 0.06(3) 0.01(3) -0.02(2) 0.01(3) C158 0.06(2) 0.04(2) 0.14(5) -0.03(2) 0.00(3) 0.000(18) C165 0.11(4) 0.08(3) 0.07(3) 0.04(2) 0.00(3) 0.03(3) C227 0.077(16) 0.085(17) 0.074(16) -0.004(12) -0.011(12) -0.007(12) C138 0.07(3) 0.07(3) 0.07(3) -0.02(2) -0.02(2) 0.00(2) C83 0.063(14) 0.073(15) 0.058(14) 0.003(11) 0.013(11) -0.002(12) C142 0.086(18) 0.087(18) 0.102(19) 0.000(13) 0.004(13) 0.004(13) C167 0.05(3) 0.15(6) 0.11(4) -0.02(4) 0.02(3) -0.04(3) C214 0.083(16) 0.082(16) 0.064(15) -0.007(12) -0.006(12) 0.002(12) C286 0.061(14) 0.090(16) 0.067(15) 0.005(12) -0.003(12) 0.001(12) C137 0.10(2) 0.094(19) 0.10(2) 0.001(13) -0.009(13) -0.003(13) C202 0.07(3) 0.09(3) 0.06(2) 0.01(2) 0.03(2) 0.00(2) C221 0.033(11) 0.056(12) 0.045(11) 0.006(10) -0.007(9) 0.011(10) C5 0.068(15) 0.070(15) 0.084(16) -0.005(12) 0.005(12) 0.000(12) N3 0.05(2) 0.14(4) 0.14(4) -0.05(3) 0.05(2) 0.00(2) C285 0.082(16) 0.081(16) 0.072(16) 0.004(12) 0.011(12) 0.004(12) C218 0.072(15) 0.081(16) 0.071(15) 0.007(12) 0.014(12) 0.003(12) C216 0.071(15) 0.079(16) 0.063(15) 0.003(12) 0.010(12) 0.004(12) C117 0.09(3) 0.05(2) 0.09(3) -0.01(2) 0.02(3) -0.01(2) C201 0.06(2) 0.05(2) 0.08(3) -0.009(19) -0.01(2) -0.008(18) C53 0.079(17) 0.078(17) 0.089(17) -0.011(12) 0.005(12) -0.006(12) C54 0.10(4) 0.13(5) 0.08(4) -0.04(3) 0.00(3) 0.00(4) C182 0.05(2) 0.10(3) 0.09(3) 0.04(3) -0.01(2) -0.02(2) C209 0.10(2) 0.10(2) 0.11(2) 0.005(13) -0.002(13) -0.001(13) C143 0.080(18) 0.091(18) 0.097(18) 0.003(13) -0.006(13) 0.001(13) C97 0.09(3) 0.06(3) 0.07(3) 0.01(2) -0.04(2) -0.03(2) C118 0.07(3) 0.09(4) 0.14(5) -0.01(3) -0.01(3) -0.02(3) N2 0.19(4) 0.19(4) 0.18(4) -0.03(3) 0.02(3) 0.00(3) C247 0.10(4) 0.10(4) 0.09(4) -0.04(3) 0.01(3) -0.04(3) C9 0.085(17) 0.091(17) 0.072(16) 0.001(12) -0.009(12) 0.000(13) C136 0.11(2) 0.11(2) 0.10(2) -0.006(13) -0.007(13) 0.002(13) C271 0.08(3) 0.08(3) 0.09(3) 0.03(3) -0.02(3) 0.00(3) C226 0.06(2) 0.09(3) 0.08(3) 0.01(2) -0.01(2) -0.02(2) C144 0.072(16) 0.083(17) 0.093(17) 0.008(13) 0.005(12) -0.006(12) C236 0.09(2) 0.10(2) 0.10(2) 0.011(13) 0.006(13) 0.004(13) N1 0.12(4) 0.11(4) 0.19(6) -0.01(4) 0.02(4) -0.07(4) C22 0.068(16) 0.085(17) 0.089(17) -0.005(13) 0.000(12) -0.005(12) C237 0.10(2) 0.10(2) 0.11(2) 0.009(13) 0.005(13) -0.001(13) C238 0.096(19) 0.095(19) 0.098(19) 0.006(13) 0.004(13) -0.006(13) C235 0.11(2) 0.11(2) 0.10(2) 0.004(13) 0.007(13) 0.000(13) C210 0.13(3) 0.13(3) 0.13(3) 0.001(14) -0.003(14) 0.002(14) C211 0.096(19) 0.089(18) 0.092(19) 0.008(13) -0.002(13) 0.006(13) C241 0.12(2) 0.11(2) 0.12(2) 0.008(13) 0.004(14) 0.007(14) C52 0.067(15) 0.072(15) 0.072(15) -0.015(12) 0.005(12) -0.005(12) C217 0.081(17) 0.087(17) 0.078(17) 0.005(12) 0.006(12) 0.009(13) C219 0.068(15) 0.077(16) 0.081(16) 0.003(12) -0.003(12) 0.000(12) C287 0.092(19) 0.099(19) 0.094(19) -0.006(13) 0.002(13) -0.008(13) C15 0.085(15) 0.091(13) 0.087(14) -0.005(11) 0.008(11) 0.005(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au7 Au3 2.7651(16) . ? Au7 Au5 2.8855(17) . ? Au7 Au2 2.7505(18) . ? Au7 Au4 2.7078(17) . ? Au7 Au6 2.6745(16) . ? Au7 Au8 2.6690(18) . ? Au7 Au1 2.7450(18) . ? Au7 Cu2 2.526(5) . ? Au7 Cu1 2.653(5) . ? Au15 Au13 2.7958(17) . ? Au15 Au12 2.7256(18) . ? Au15 Au14 2.6955(18) . ? Au15 Au9 2.7691(18) . ? Au15 Au11 2.7879(18) . ? Au15 Au10 2.7063(18) . ? Au15 Au16 2.6537(19) . ? Au15 Cu5 2.676(5) . ? Au15 Cu6 2.528(5) . ? Au3 Au2 2.7890(18) . ? Au3 Au4 2.7969(18) . ? Au3 Au8 2.6934(19) . ? Au3 P3 2.299(7) . ? Au5 Au4 2.8424(17) . ? Au5 Au6 2.7486(18) . ? Au5 Cu2 2.637(5) . ? Au5 P5 2.335(8) . ? Au13 Au12 2.8139(18) . ? Au13 Au14 2.743(2) . ? Au13 Cu6 2.656(5) . ? Au13 P11 2.305(7) . ? Au2 Au1 2.7452(18) . ? Au2 Cu1 2.616(5) . ? Au2 P2 2.295(8) . ? Au12 Au11 2.7851(18) . ? Au12 Au16 2.866(2) . ? Au12 P10 2.294(8) . ? Au4 Au8 2.8375(19) . ? Au4 P4 2.294(8) . ? Au14 Cu5 2.665(5) . ? Au14 Cu6 2.684(5) . ? Au14 Cu7 2.974(5) . ? Au14 Cu8 2.756(6) . ? Au14 S12 2.395(8) . ? Au6 Cu2 2.646(5) . ? Au6 Cu1 2.696(5) . ? Au6 Cu3 3.034(6) . ? Au6 Cu4 2.756(6) . ? Au6 S6 2.386(7) . ? Au8 Au1 3.310(2) . ? Au8 P6 2.273(8) . ? Au9 Au10 2.7429(19) . ? Au9 Au16 3.195(2) . ? Au9 Cu5 2.656(5) . ? Au9 P7 2.319(8) . ? Au11 Au10 2.816(2) . ? Au11 Au16 2.6745(19) . ? Au11 P9 2.301(9) . ? Au1 Cu1 2.687(5) . ? Au1 P1 2.328(9) . ? Au10 Cu5 2.629(5) . ? Au10 P8 2.282(7) . ? Au16 P12 2.261(8) . ? Cu5 Cu7 2.873(7) . ? Cu5 Cu8 2.706(7) . ? Cu5 S7 2.309(10) . ? Cu5 S8 2.280(9) . ? Cu2 Cu3 2.633(7) . ? Cu2 S3 2.236(9) . ? Cu2 S4 2.234(9) . ? Cu6 Cu7 2.632(8) . ? Cu6 S9 2.233(9) . ? Cu6 S10 2.255(10) . ? Cu1 Cu3 2.939(8) . ? Cu1 Cu4 2.739(6) . ? Cu1 S2 2.299(11) . ? Cu1 S1 2.308(10) . ? Cu7 Cu8 2.777(8) . ? Cu7 S8 2.311(10) . ? Cu7 S11 2.319(11) . ? Cu7 S10 2.304(11) . ? Cu3 Cu4 2.864(8) . ? Cu3 S2 2.302(12) . ? Cu3 S4 2.307(12) . ? Cu3 S5 2.310(10) . ? Cu8 S12 2.296(10) . ? Cu8 S7 2.226(11) . ? Cu8 S11 2.284(12) . ? Cu4 S6 2.262(12) . ? Cu4 S5 2.260(12) . ? Cu4 S1 2.227(12) . ? P5 C107 1.76(4) . ? P5 C106 1.84(3) . ? P5 C113 1.81(4) . ? P11 C276 1.80(4) . ? P11 C277 1.81(4) . ? P11 C283 1.81(3) . ? P2 C94 1.81(3) . ? P2 C88 1.84(5) . ? P2 C100 1.82(4) . ? P3 C69 1.84(4) . ? P3 C63 1.80(4) . ? P3 C57 1.81(3) . ? P6 C44 1.85(3) . ? P6 C51 1.75(4) . ? P6 C45 1.77(2) . ? S9 C150 1.72(4) . ? P7 C163 1.84(3) . ? P7 C157 1.79(4) . ? P7 C169 1.81(4) . ? P4 C132 1.83(3) . ? P4 C133 1.82(4) . ? P4 C139 1.85(4) . ? P12 C189 1.82(4) . ? P12 C188 1.84(3) . ? P12 C195 1.77(4) . ? S12 C155 1.74(4) . ? S3 C6 1.75(4) . ? P1 C19 1.80(3) . ? P1 C25 1.87(3) . ? P1 C13 1.79(4) . ? P10 C257 1.84(4) . ? P10 C251 1.73(4) . ? P10 C245 1.79(4) . ? P8 C207 1.74(5) . ? P8 C213 1.80(4) . ? P8 C201 1.79(5) . ? S7 C146 1.76(4) . ? P9 C239 1.73(4) . ? P9 C232 1.88(4) . ? P9 C233 1.80(4) . ? S8 C147 1.69(4) . ? S2 C3 1.75(4) . ? S6 C11 1.70(4) . ? S4 C7 1.75(4) . ? S11 C154 1.74(4) . ? S10 C151 1.76(3) . ? S5 C10 1.72(5) . ? S1 C2 1.72(4) . ? C73 H73 0.9300 . ? C73 C72 1.41(5) . ? C73 C74 1.33(6) . ? C276 C267 1.34(5) . ? C276 C275 1.45(5) . ? C72 C71 1.36(5) . ? C72 C77 1.43(4) . ? C163 C164 1.41(5) . ? C163 C168 1.31(5) . ? C79 C78 1.51(2) . ? C79 C88 1.38(4) . ? C79 C80 1.45(4) . ? C257 C258 1.40(4) . ? C257 C266 1.40(4) . ? C94 C93 1.37(5) . ? C94 C89 1.41(4) . ? C69 C78 1.39(4) . ? C69 C70 1.45(5) . ? C93 H93 0.9300 . ? C93 C92 1.33(5) . ? C91 H91 0.9300 . ? C91 C92 1.44(6) . ? C91 C90 1.35(6) . ? C189 C190 1.36(5) . ? C189 C194 1.45(4) . ? N4 C8 1.06(5) . ? C35 C34 1.48(4) . ? C35 C44 1.40(5) . ? C35 C36 1.39(4) . ? C92 H92 0.9300 . ? C68 H68 0.9300 . ? C68 C63 1.42(5) . ? C68 C67 1.35(6) . ? C2 C3 1.37(6) . ? C2 C1 1.48(5) . ? C231 H231 0.9300 . ? C231 C232 1.43(5) . ? C231 C230 1.39(5) . ? C125 H125 0.9300 . ? C125 C124 1.43(5) . ? C125 C126 1.34(5) . ? C114 H114 0.9300 . ? C114 C115 1.29(6) . ? C114 C113 1.38(5) . ? C60 H60 0.9300 . ? C60 C59 1.391(14) . ? C60 C61 1.391(14) . ? C59 H59 0.9300 . ? C59 C58 1.399(14) . ? C132 C123 1.38(5) . ? C132 C131 1.41(5) . ? C78 C77 1.45(4) . ? C185 C186 1.41(5) . ? C185 C184 1.39(5) . ? C185 C180 1.42(5) . ? C88 C87 1.40(5) . ? C100 C99 1.40(5) . ? C100 C95 1.38(5) . ? C174 H174 0.9300 . ? C174 C175 1.38(6) . ? C174 C173 1.35(6) . ? C267 C266 1.50(4) . ? C267 C268 1.49(5) . ? C107 C108 1.38(5) . ? C107 C112 1.44(5) . ? C74 H74 0.9300 . ? C74 C75 1.36(5) . ? C19 C24 1.387(14) . ? C19 C20 1.383(14) . ? C34 C25 1.393(14) . ? C34 C33 1.396(14) . ? C275 H275 0.9300 . ? C275 C274 1.31(6) . ? C37 H37 0.9300 . ? C37 C38 1.35(5) . ? C37 C36 1.41(5) . ? C42 H42 0.9300 . ? C42 C43 1.40(4) . ? C42 C41 1.40(5) . ? C43 H43 0.9300 . ? C43 C44 1.40(4) . ? C124 C129 1.41(5) . ? C124 C123 1.41(5) . ? C24 H24 0.9300 . ? C24 C23 1.389(14) . ? C259 H259 0.9300 . ? C259 C258 1.37(5) . ? C259 C260 1.41(5) . ? C106 C101 1.32(5) . ? C106 C105 1.42(5) . ? C75 H75 0.9300 . ? C75 C76 1.35(5) . ? C71 H71 0.9300 . ? C71 C70 1.31(5) . ? C178 C177 1.46(5) . ? C178 C169 1.39(4) . ? C178 C179 1.50(5) . ? C77 C76 1.42(5) . ? C258 H258 0.9300 . ? C157 C162 1.39(5) . ? C157 C158 1.36(7) . ? C188 C187 1.47(5) . ? C188 C179 1.35(5) . ? C265 C266 1.45(5) . ? C265 C260 1.39(5) . ? C265 C264 1.43(5) . ? C274 H274 0.9300 . ? C274 C273 1.44(6) . ? C263 H263 0.9300 . ? C263 C264 1.37(6) . ? C263 C262 1.37(6) . ? C190 H190 0.9300 . ? C190 C191 1.37(6) . ? C51 C56 1.45(5) . ? C51 C52 1.43(6) . ? C41 C36 1.43(4) . ? C41 C40 1.41(4) . ? C8 C7 1.44(5) . ? C20 H20 0.9300 . ? C20 C21 1.392(14) . ? C145 C146 1.49(6) . ? C145 N7 1.08(5) . ? C3 C4 1.45(8) . ? C7 C6 1.37(5) . ? C6 C5 1.43(6) . ? C61 H61 0.9300 . ? C61 C62 1.388(14) . ? C65 H65 0.9300 . ? C65 C64 1.41(6) . ? C65 C66 1.31(6) . ? C63 C64 1.34(5) . ? C277 C278 1.40(4) . ? C277 C282 1.35(5) . ? C273 C268 1.44(5) . ? C273 C272 1.36(6) . ? C87 H87 0.9300 . ? C87 C86 1.29(6) . ? C57 C58 1.394(14) . ? C57 C62 1.390(14) . ? C99 H99 0.9300 . ? C99 C98 1.39(5) . ? C129 C130 1.36(5) . ? C129 C128 1.49(6) . ? C26 H26 0.9300 . ? C26 C25 1.394(14) . ? C26 C27 1.387(14) . ? C1 N1 1.12(6) . ? C177 C176 1.39(5) . ? C177 C172 1.41(6) . ? C108 H108 0.9300 . ? C108 C109 1.39(6) . ? C239 C244 1.44(6) . ? C239 C240 1.39(7) . ? C164 H164 0.9300 . ? C164 C165 1.47(6) . ? C112 H112 0.9300 . ? C112 C111 1.37(6) . ? C162 H162 0.9300 . ? C162 C161 1.40(6) . ? C111 H111 0.9300 . ? C111 C110 1.33(7) . ? C169 C170 1.44(5) . ? C133 C134 1.389(14) . ? C133 C138 1.386(14) . ? C10 C11 1.35(6) . ? C10 C9 1.51(6) . ? C194 H194 0.9300 . ? C194 C193 1.27(5) . ? C168 H168 0.9300 . ? C168 C167 1.45(8) . ? N6 C12 1.15(6) . ? C260 C261 1.38(5) . ? C101 H101 0.9300 . ? C101 C102 1.42(6) . ? C195 C200 1.45(6) . ? C195 C196 1.44(6) . ? C121 C120 1.40(5) . ? C121 C116 1.38(5) . ? C121 C122 1.46(5) . ? C81 H81 0.9300 . ? C81 C82 1.36(5) . ? C81 C80 1.38(4) . ? C115 H115 0.9300 . ? C115 C116 1.46(6) . ? C171 H171 0.9300 . ? C171 C170 1.32(5) . ? C171 C172 1.41(6) . ? C86 H86 0.9300 . ? C86 C85 1.39(5) . ? C113 C122 1.42(5) . ? C264 H264 0.9300 . ? C232 C223 1.36(5) . ? C203 H203 0.9300 . ? C203 C204 1.36(7) . ? C203 C202 1.43(6) . ? C70 H70 0.9300 . ? C154 C155 1.36(5) . ? C154 C153 1.41(6) . ? C58 H58 0.9300 . ? C208 H208 0.9300 . ? C208 C207 1.388(14) . ? C208 C209 1.387(14) . ? C130 H130 0.9300 . ? C130 C131 1.36(5) . ? C225 H225 0.9300 . ? C225 C224 1.36(6) . ? C225 C226 1.34(6) . ? C90 H90 0.9300 . ? C90 C89 1.43(5) . ? C155 C156 1.38(6) . ? C161 H161 0.9300 . ? C161 C160 1.36(8) . ? C151 C150 1.39(5) . ? C151 C152 1.36(5) . ? C38 H38 0.9300 . ? C38 C39 1.43(6) . ? C147 C146 1.44(6) . ? C147 C148 1.46(6) . ? C14 H14 0.9300 . ? C14 C13 1.385(14) . ? C14 C15 1.393(14) . ? C186 H186 0.9300 . ? C186 C187 1.31(5) . ? C187 H187 0.9300 . ? C230 H230 0.9300 . ? C230 C229 1.39(6) . ? C228 H228 0.9300 . ? C228 C229 1.43(6) . ? C228 C227 1.32(7) . ? C150 C149 1.43(5) . ? C62 H62 0.9300 . ? C200 H200 0.9300 . ? C200 C199 1.36(7) . ? C170 H170 0.9300 . ? C160 H160 0.9300 . ? C160 C159 1.36(7) . ? C176 H176 0.9300 . ? C176 C175 1.36(5) . ? C104 H104 0.9300 . ? C104 C103 1.36(7) . ? C104 C105 1.36(6) . ? C109 H109 0.9300 . ? C109 C110 1.37(7) . ? C27 H27 0.9300 . ? C27 C28 1.387(14) . ? C64 H64 0.9300 . ? C283 C288 1.42(6) . ? C283 C284 1.37(6) . ? C152 N10 1.19(5) . ? C110 H110 0.9300 . ? C199 H199 0.9300 . ? C199 C198 1.35(7) . ? C179 C180 1.46(5) . ? C281 H281 0.9300 . ? C281 C282 1.36(6) . ? C281 C280 1.44(6) . ? C85 C84 1.44(5) . ? C85 C80 1.45(4) . ? C139 C140 1.36(5) . ? C139 C144 1.34(6) . ? C175 H175 0.9300 . ? C269 H269 0.9300 . ? C269 C268 1.39(6) . ? C269 C270 1.41(6) . ? C76 H76 0.9300 . ? C33 C32 1.390(10) . ? C33 C28 1.388(10) . ? C159 H159 0.9300 . ? C159 C158 1.33(5) . ? C229 C224 1.45(6) . ? C246 H246 0.9300 . ? C246 C245 1.39(5) . ? C246 C247 1.34(6) . ? C261 H261 0.9300 . ? C261 C262 1.38(6) . ? C89 H89 0.9300 . ? C120 H120 0.9300 . ? C120 C119 1.36(6) . ? C204 H204 0.9300 . ? C204 C205 1.33(7) . ? N9 C149 1.20(5) . ? C128 H128 0.9300 . ? C128 C127 1.38(7) . ? C13 C18 1.392(14) . ? C278 H278 0.9300 . ? C278 C279 1.38(5) . ? C184 H184 0.9300 . ? C184 C183 1.36(7) . ? C198 H198 0.9300 . ? C198 C197 1.41(7) . ? C84 H84 0.9300 . ? C84 C83 1.35(6) . ? C134 H134 0.9300 . ? C134 C135 1.392(14) . ? C123 C122 1.50(3) . ? C32 H32 0.9300 . ? C32 C31 1.389(10) . ? C12 C11 1.40(6) . ? C197 H197 0.9300 . ? C197 C196 1.29(6) . ? C172 C173 1.46(5) . ? C141 H141 0.9300 . ? C141 C140 1.38(7) . ? C141 C142 1.42(8) . ? C282 H282 0.9300 . ? N8 C148 1.07(6) . ? C29 H29 0.9300 . ? C29 C28 1.390(10) . ? C29 C30 1.387(10) . ? N12 C156 1.18(5) . ? C255 H255 0.9300 . ? C255 C256 1.32(7) . ? C255 C254 1.31(8) . ? C103 H103 0.9300 . ? C103 C102 1.33(7) . ? C288 H288 0.9300 . ? C288 C287 1.39(7) . ? C102 H102 0.9300 . ? C105 H105 0.9300 . ? C49 H49 0.9300 . ? C49 C48 1.3900 . ? C49 C50 1.3900 . ? C48 H48 0.9300 . ? C48 C47 1.3900 . ? C47 H47 0.9300 . ? C47 C46 1.3900 . ? C46 H46 0.9300 . ? C46 C45 1.3900 . ? C45 C50 1.3900 . ? C50 H50 0.9300 . ? C183 H183 0.9300 . ? C183 C182 1.39(7) . ? C40 H40 0.9300 . ? C40 C39 1.39(5) . ? C4 N2 1.135(14) . ? C222 C213 1.43(6) . ? C222 C223 1.51(5) . ? C222 C221 1.42(4) . ? C207 C212 1.391(14) . ? C193 H193 0.9300 . ? C193 C192 1.37(7) . ? C181 H181 0.9300 . ? C181 C180 1.43(5) . ? C181 C182 1.33(6) . ? C196 H196 0.9300 . ? C140 H140 0.9300 . ? C18 H18 0.9300 . ? C18 C17 1.392(14) . ? C82 H82 0.9300 . ? C82 C83 1.45(6) . ? C205 H205 0.9300 . ? C205 C206 1.38(6) . ? C16 H16 0.9300 . ? C16 C17 1.388(14) . ? C16 C15 1.386(14) . ? C67 H67 0.9300 . ? C67 C66 1.37(6) . ? C17 H17 0.9300 . ? C126 H126 0.9300 . ? C126 C127 1.31(6) . ? C244 H244 0.9300 . ? C244 C243 1.41(6) . ? C242 H242 0.9300 . ? C242 C243 1.42(7) . ? C242 C241 1.34(9) . ? C253 H253 0.9300 . ? C253 C252 1.45(7) . ? C253 C254 1.31(8) . ? C252 H252 0.9300 . ? C252 C251 1.44(6) . ? C55 H55 0.9300 . ? C55 C56 1.35(6) . ? C55 C54 1.40(8) . ? C173 H173 0.9300 . ? C248 H248 0.9300 . ? C248 C249 1.35(8) . ? C248 C247 1.44(8) . ? C224 C223 1.44(5) . ? C153 N11 1.19(6) . ? C234 H234 0.9300 . ? C234 C233 1.387(14) . ? C234 C235 1.392(14) . ? C233 C238 1.389(14) . ? C215 H215 0.9300 . ? C215 C214 1.31(7) . ? C215 C216 1.44(7) . ? C249 H249 0.9300 . ? C249 C250 1.42(7) . ? C23 H23 0.9300 . ? C23 C22 1.387(14) . ? C251 C256 1.47(6) . ? C95 H95 0.9300 . ? C95 C96 1.40(5) . ? C240 H240 0.9300 . ? C240 C241 1.38(9) . ? C116 C117 1.49(6) . ? C256 H256 0.9300 . ? C213 C214 1.40(6) . ? C262 H262 0.9300 . ? C56 H56 0.9300 . ? C254 H254 0.9300 . ? C119 H119 0.9300 . ? C119 C118 1.46(8) . ? N5 C9 1.15(6) . ? C39 H39 0.9300 . ? C96 H96 0.9300 . ? C96 C97 1.36(7) . ? C135 H135 0.9300 . ? C135 C136 1.386(14) . ? C272 H272 0.9300 . ? C272 C271 1.28(7) . ? C127 H127 0.9300 . ? C243 H243 0.9300 . ? C192 H192 0.9300 . ? C192 C191 1.43(7) . ? C98 H98 0.9300 . ? C98 C97 1.39(7) . ? C250 H250 0.9300 . ? C250 C245 1.39(5) . ? C279 H279 0.9300 . ? C279 C280 1.40(7) . ? C220 H220 0.9300 . ? C220 C221 1.43(6) . ? C220 C219 1.32(6) . ? C66 H66 0.9300 . ? C206 H206 0.9300 . ? C206 C201 1.37(6) . ? C212 H212 0.9300 . ? C212 C211 1.389(14) . ? C280 H280 0.9300 . ? C270 H270 0.9300 . ? C270 C271 1.35(7) . ? C131 H131 0.9300 . ? C30 H30 0.9300 . ? C30 C31 1.390(10) . ? C166 H166 0.9300 . ? C166 C165 1.31(8) . ? C166 C167 1.29(8) . ? C31 H31 0.9300 . ? C284 H284 0.9300 . ? C284 C285 1.38(6) . ? C21 H21 0.9300 . ? C21 C22 1.385(14) . ? C191 H191 0.9300 . ? C158 H158 0.9300 . ? C165 H165 0.9300 . ? C227 H227 0.9300 . ? C227 C226 1.45(7) . ? C138 H138 0.9300 . ? C138 C137 1.389(14) . ? C83 H83 0.9300 . ? C142 H142 0.9300 . ? C142 C143 1.45(8) . ? C167 H167 0.9300 . ? C214 H214 0.9300 . ? C286 H286 0.9300 . ? C286 C285 1.33(7) . ? C286 C287 1.39(7) . ? C137 H137 0.9300 . ? C137 C136 1.388(14) . ? C202 H202 0.9300 . ? C202 C201 1.35(6) . ? C221 C216 1.43(6) . ? C5 N3 1.15(6) . ? C285 H285 0.9300 . ? C218 H218 0.9300 . ? C218 C217 1.36(7) . ? C218 C219 1.45(7) . ? C216 C217 1.43(7) . ? C117 H117 0.9300 . ? C117 C118 1.28(7) . ? C53 H53 0.9300 . ? C53 C54 1.37(8) . ? C53 C52 1.31(7) . ? C54 H54 0.9300 . ? C182 H182 0.9300 . ? C209 H209 0.9300 . ? C209 C210 1.389(14) . ? C143 H143 0.9300 . ? C143 C144 1.32(7) . ? C97 H97 0.9300 . ? C118 H118 0.9300 . ? C247 H247 0.9300 . ? C136 H136 0.9300 . ? C271 H271 0.9300 . ? C226 H226 0.9300 . ? C144 H144 0.9300 . ? C236 H236 0.9300 . ? C236 C237 1.387(14) . ? C236 C235 1.390(14) . ? C22 H22 0.9300 . ? C237 H237 0.9300 . ? C237 C238 1.386(14) . ? C238 H238 0.9300 . ? C235 H235 0.9300 . ? C210 H210 0.9300 . ? C210 C211 1.389(14) . ? C211 H211 0.9300 . ? C241 H241 0.9300 . ? C52 H52 0.9300 . ? C217 H217 0.9300 . ? C219 H219 0.9300 . ? C287 H287 0.9300 . ? C15 H15 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Au3 Au7 Au5 122.44(6) . . ? Au2 Au7 Au3 60.75(4) . . ? Au2 Au7 Au5 174.24(6) . . ? Au4 Au7 Au3 61.46(4) . . ? Au4 Au7 Au5 60.99(4) . . ? Au4 Au7 Au2 122.00(5) . . ? Au4 Au7 Au1 138.85(6) . . ? Au6 Au7 Au3 175.89(7) . . ? Au6 Au7 Au5 59.11(5) . . ? Au6 Au7 Au2 117.35(6) . . ? Au6 Au7 Au4 119.98(6) . . ? Au6 Au7 Au1 79.62(5) . . ? Au8 Au7 Au3 59.39(5) . . ? Au8 Au7 Au5 95.04(6) . . ? Au8 Au7 Au2 90.73(6) . . ? Au8 Au7 Au4 63.70(5) . . ? Au8 Au7 Au6 124.69(6) . . ? Au8 Au7 Au1 75.38(6) . . ? Au1 Au7 Au3 101.73(6) . . ? Au1 Au7 Au5 121.74(6) . . ? Au1 Au7 Au2 59.94(5) . . ? Cu2 Au7 Au3 115.99(12) . . ? Cu2 Au7 Au5 57.86(12) . . ? Cu2 Au7 Au2 116.70(13) . . ? Cu2 Au7 Au4 84.67(13) . . ? Cu2 Au7 Au6 61.09(11) . . ? Cu2 Au7 Au8 146.53(14) . . ? Cu2 Au7 Au1 133.93(13) . . ? Cu2 Au7 Cu1 79.58(17) . . ? Cu1 Au7 Au3 116.44(11) . . ? Cu1 Au7 Au5 117.50(11) . . ? Cu1 Au7 Au2 57.87(11) . . ? Cu1 Au7 Au4 160.85(13) . . ? Cu1 Au7 Au6 60.80(11) . . ? Cu1 Au7 Au8 133.51(13) . . ? Cu1 Au7 Au1 59.68(12) . . ? Au12 Au15 Au13 61.26(5) . . ? Au12 Au15 Au9 135.68(6) . . ? Au12 Au15 Au11 60.67(5) . . ? Au14 Au15 Au13 59.90(5) . . ? Au14 Au15 Au12 121.11(6) . . ? Au14 Au15 Au9 77.36(5) . . ? Au14 Au15 Au11 176.31(7) . . ? Au14 Au15 Au10 116.50(6) . . ? Au9 Au15 Au13 121.72(6) . . ? Au9 Au15 Au11 103.63(6) . . ? Au11 Au15 Au13 121.61(6) . . ? Au10 Au15 Au13 173.75(7) . . ? Au10 Au15 Au12 122.32(6) . . ? Au10 Au15 Au9 60.11(5) . . ? Au10 Au15 Au11 61.65(5) . . ? Au16 Au15 Au13 100.31(6) . . ? Au16 Au15 Au12 64.36(5) . . ? Au16 Au15 Au14 124.73(6) . . ? Au16 Au15 Au9 72.15(5) . . ? Au16 Au15 Au11 58.82(5) . . ? Au16 Au15 Au10 85.95(6) . . ? Au16 Au15 Cu5 128.44(12) . . ? Cu5 Au15 Au13 116.64(11) . . ? Cu5 Au15 Au12 165.69(12) . . ? Cu5 Au15 Au14 59.48(11) . . ? Cu5 Au15 Au9 58.34(11) . . ? Cu5 Au15 Au11 117.90(11) . . ? Cu5 Au15 Au10 58.47(11) . . ? Cu6 Au15 Au13 59.60(11) . . ? Cu6 Au15 Au12 90.71(14) . . ? Cu6 Au15 Au14 61.74(12) . . ? Cu6 Au15 Au9 130.82(14) . . ? Cu6 Au15 Au11 115.66(12) . . ? Cu6 Au15 Au10 114.39(12) . . ? Cu6 Au15 Au16 154.32(14) . . ? Cu6 Au15 Cu5 77.08(16) . . ? Au7 Au3 Au2 59.37(4) . . ? Au7 Au3 Au4 58.26(4) . . ? Au2 Au3 Au4 117.45(5) . . ? Au8 Au3 Au7 58.53(4) . . ? Au8 Au3 Au2 89.40(5) . . ? Au8 Au3 Au4 62.20(5) . . ? P3 Au3 Au7 174.1(2) . . ? P3 Au3 Au2 119.0(2) . . ? P3 Au3 Au4 122.5(2) . . ? P3 Au3 Au8 127.3(2) . . ? Au4 Au5 Au7 56.42(4) . . ? Au6 Au5 Au7 56.62(4) . . ? Au6 Au5 Au4 112.93(6) . . ? Cu2 Au5 Au7 54.22(11) . . ? Cu2 Au5 Au4 80.06(11) . . ? Cu2 Au5 Au6 58.82(12) . . ? P5 Au5 Au7 169.0(2) . . ? P5 Au5 Au4 124.8(2) . . ? P5 Au5 Au6 121.5(2) . . ? P5 Au5 Cu2 135.8(2) . . ? Au15 Au13 Au12 58.14(4) . . ? Au14 Au13 Au15 58.23(5) . . ? Au14 Au13 Au12 116.32(6) . . ? Cu6 Au13 Au15 55.18(11) . . ? Cu6 Au13 Au12 86.24(11) . . ? Cu6 Au13 Au14 59.59(12) . . ? P11 Au13 Au15 169.6(2) . . ? P11 Au13 Au12 124.7(2) . . ? P11 Au13 Au14 117.4(2) . . ? P11 Au13 Cu6 132.6(2) . . ? Au7 Au2 Au3 59.88(4) . . ? Au1 Au2 Au7 59.93(5) . . ? Au1 Au2 Au3 101.11(6) . . ? Cu1 Au2 Au7 59.19(12) . . ? Cu1 Au2 Au3 116.87(12) . . ? Cu1 Au2 Au1 60.10(12) . . ? P2 Au2 Au7 149.4(2) . . ? P2 Au2 Au3 97.3(2) . . ? P2 Au2 Au1 150.3(2) . . ? P2 Au2 Cu1 129.4(2) . . ? Au15 Au12 Au13 60.60(5) . . ? Au15 Au12 Au11 60.77(5) . . ? Au15 Au12 Au16 56.60(5) . . ? Au13 Au12 Au16 94.92(6) . . ? Au11 Au12 Au13 121.05(6) . . ? Au11 Au12 Au16 56.48(5) . . ? P10 Au12 Au15 150.3(2) . . ? P10 Au12 Au13 93.7(2) . . ? P10 Au12 Au11 139.4(2) . . ? P10 Au12 Au16 147.5(3) . . ? Au7 Au4 Au3 60.28(4) . . ? Au7 Au4 Au5 62.60(4) . . ? Au7 Au4 Au8 57.49(5) . . ? Au3 Au4 Au5 122.87(6) . . ? Au3 Au4 Au8 57.11(5) . . ? Au8 Au4 Au5 92.39(5) . . ? P4 Au4 Au7 155.2(2) . . ? P4 Au4 Au3 138.2(2) . . ? P4 Au4 Au5 96.5(2) . . ? P4 Au4 Au8 142.0(2) . . ? Au15 Au14 Au13 61.87(5) . . ? Au15 Au14 Cu7 96.16(11) . . ? Au15 Au14 Cu8 119.56(13) . . ? Au13 Au14 Cu7 110.03(12) . . ? Au13 Au14 Cu8 167.47(13) . . ? Cu5 Au14 Au15 59.91(10) . . ? Cu5 Au14 Au13 118.91(11) . . ? Cu5 Au14 Cu6 74.70(15) . . ? Cu5 Au14 Cu7 60.97(15) . . ? Cu5 Au14 Cu8 59.86(15) . . ? Cu6 Au14 Au15 56.07(11) . . ? Cu6 Au14 Au13 58.60(12) . . ? Cu6 Au14 Cu7 55.16(16) . . ? Cu6 Au14 Cu8 110.85(16) . . ? Cu8 Au14 Cu7 57.83(16) . . ? S12 Au14 Au15 154.8(2) . . ? S12 Au14 Au13 132.1(2) . . ? S12 Au14 Cu5 108.7(3) . . ? S12 Au14 Cu6 146.8(2) . . ? S12 Au14 Cu7 96.6(2) . . ? S12 Au14 Cu8 52.4(2) . . ? Au7 Au6 Au5 64.28(5) . . ? Au7 Au6 Cu1 59.20(10) . . ? Au7 Au6 Cu3 94.71(11) . . ? Au7 Au6 Cu4 119.35(13) . . ? Au5 Au6 Cu3 109.53(12) . . ? Au5 Au6 Cu4 167.40(14) . . ? Cu2 Au6 Au7 56.69(10) . . ? Cu2 Au6 Au5 58.48(12) . . ? Cu2 Au6 Cu1 76.73(16) . . ? Cu2 Au6 Cu3 54.73(15) . . ? Cu2 Au6 Cu4 112.20(17) . . ? Cu1 Au6 Au5 120.89(11) . . ? Cu1 Au6 Cu3 61.38(16) . . ? Cu1 Au6 Cu4 60.29(15) . . ? Cu4 Au6 Cu3 59.07(16) . . ? S6 Au6 Au7 156.7(2) . . ? S6 Au6 Au5 130.0(3) . . ? S6 Au6 Cu2 144.3(2) . . ? S6 Au6 Cu1 109.0(3) . . ? S6 Au6 Cu3 96.0(3) . . ? S6 Au6 Cu4 51.6(3) . . ? Au7 Au8 Au3 62.08(5) . . ? Au7 Au8 Au4 58.82(5) . . ? Au7 Au8 Au1 53.35(4) . . ? Au3 Au8 Au4 60.69(5) . . ? Au3 Au8 Au1 90.17(6) . . ? Au4 Au8 Au1 112.04(6) . . ? P6 Au8 Au7 131.4(2) . . ? P6 Au8 Au3 159.7(2) . . ? P6 Au8 Au4 137.3(3) . . ? P6 Au8 Au1 89.5(2) . . ? Au15 Au9 Au16 52.25(4) . . ? Au10 Au9 Au15 58.81(5) . . ? Au10 Au9 Au16 75.53(5) . . ? Cu5 Au9 Au15 59.08(11) . . ? Cu5 Au9 Au10 58.26(11) . . ? Cu5 Au9 Au16 109.91(11) . . ? P7 Au9 Au15 169.1(2) . . ? P7 Au9 Au10 128.2(2) . . ? P7 Au9 Au16 118.8(2) . . ? P7 Au9 Cu5 130.9(2) . . ? Au15 Au11 Au10 57.75(5) . . ? Au12 Au11 Au15 58.56(5) . . ? Au12 Au11 Au10 116.31(6) . . ? Au16 Au11 Au15 58.09(5) . . ? Au16 Au11 Au12 63.28(5) . . ? Au16 Au11 Au10 83.39(6) . . ? P9 Au11 Au15 175.0(2) . . ? P9 Au11 Au12 119.9(2) . . ? P9 Au11 Au10 123.6(2) . . ? P9 Au11 Au16 126.2(2) . . ? Au7 Au1 Au2 60.13(5) . . ? Au7 Au1 Au8 51.27(4) . . ? Au2 Au1 Au8 78.51(5) . . ? Cu1 Au1 Au7 58.46(11) . . ? Cu1 Au1 Au2 57.56(11) . . ? Cu1 Au1 Au8 108.79(11) . . ? P1 Au1 Au7 167.4(3) . . ? P1 Au1 Au2 127.4(2) . . ? P1 Au1 Au8 117.6(3) . . ? P1 Au1 Cu1 133.4(3) . . ? Au15 Au10 Au9 61.08(5) . . ? Au15 Au10 Au11 60.60(5) . . ? Au9 Au10 Au11 103.57(6) . . ? Cu5 Au10 Au15 60.19(11) . . ? Cu5 Au10 Au9 59.20(11) . . ? Cu5 Au10 Au11 118.54(12) . . ? P8 Au10 Au15 150.5(3) . . ? P8 Au10 Au9 148.2(3) . . ? P8 Au10 Au11 97.6(3) . . ? P8 Au10 Cu5 128.4(3) . . ? Au15 Au16 Au12 59.03(5) . . ? Au15 Au16 Au9 55.60(5) . . ? Au15 Au16 Au11 63.10(5) . . ? Au12 Au16 Au9 114.11(6) . . ? Au11 Au16 Au12 60.24(5) . . ? Au11 Au16 Au9 95.78(6) . . ? P12 Au16 Au15 138.8(2) . . ? P12 Au16 Au12 134.3(2) . . ? P12 Au16 Au9 93.4(2) . . ? P12 Au16 Au11 155.8(2) . . ? Au15 Cu5 Cu7 99.03(19) . . ? Au15 Cu5 Cu8 122.2(2) . . ? Au14 Cu5 Au15 60.62(11) . . ? Au14 Cu5 Cu7 64.83(15) . . ? Au14 Cu5 Cu8 61.75(16) . . ? Au9 Cu5 Au15 62.57(11) . . ? Au9 Cu5 Au14 79.89(13) . . ? Au9 Cu5 Cu7 144.7(2) . . ? Au9 Cu5 Cu8 102.92(19) . . ? Au10 Cu5 Au15 61.33(11) . . ? Au10 Cu5 Au14 120.38(18) . . ? Au10 Cu5 Au9 62.53(11) . . ? Au10 Cu5 Cu7 137.6(2) . . ? Au10 Cu5 Cu8 162.8(2) . . ? Cu8 Cu5 Cu7 59.62(19) . . ? S7 Cu5 Au15 152.5(3) . . ? S7 Cu5 Au14 108.8(3) . . ? S7 Cu5 Au9 91.3(3) . . ? S7 Cu5 Au10 116.1(3) . . ? S7 Cu5 Cu7 98.2(3) . . ? S7 Cu5 Cu8 52.0(3) . . ? S8 Cu5 Au15 112.4(3) . . ? S8 Cu5 Au14 114.6(3) . . ? S8 Cu5 Au9 161.0(3) . . ? S8 Cu5 Au10 98.7(3) . . ? S8 Cu5 Cu7 51.7(3) . . ? S8 Cu5 Cu8 95.1(3) . . ? S8 Cu5 S7 95.1(4) . . ? Au7 Cu2 Au5 67.92(12) . . ? Au7 Cu2 Au6 62.21(12) . . ? Au7 Cu2 Cu3 109.2(2) . . ? Au5 Cu2 Au6 62.70(11) . . ? Cu3 Cu2 Au5 127.5(2) . . ? Cu3 Cu2 Au6 70.14(17) . . ? S3 Cu2 Au7 88.5(3) . . ? S3 Cu2 Au5 121.5(3) . . ? S3 Cu2 Au6 147.5(3) . . ? S3 Cu2 Cu3 110.6(3) . . ? S4 Cu2 Au7 164.9(4) . . ? S4 Cu2 Au5 117.9(3) . . ? S4 Cu2 Au6 106.8(3) . . ? S4 Cu2 Cu3 55.9(3) . . ? S4 Cu2 S3 98.8(4) . . ? Au15 Cu6 Au13 65.21(12) . . ? Au15 Cu6 Au14 62.20(11) . . ? Au15 Cu6 Cu7 109.8(2) . . ? Au13 Cu6 Au14 61.81(10) . . ? Cu7 Cu6 Au13 124.7(2) . . ? Cu7 Cu6 Au14 68.02(17) . . ? S9 Cu6 Au15 91.0(3) . . ? S9 Cu6 Au13 126.2(4) . . ? S9 Cu6 Au14 147.1(3) . . ? S9 Cu6 Cu7 108.4(3) . . ? S9 Cu6 S10 97.5(4) . . ? S10 Cu6 Au15 164.9(4) . . ? S10 Cu6 Au13 118.0(3) . . ? S10 Cu6 Au14 105.3(3) . . ? S10 Cu6 Cu7 55.6(3) . . ? Au7 Cu1 Au6 60.00(11) . . ? Au7 Cu1 Au1 61.87(11) . . ? Au7 Cu1 Cu3 97.4(2) . . ? Au7 Cu1 Cu4 120.8(2) . . ? Au2 Cu1 Au7 62.94(10) . . ? Au2 Cu1 Au6 121.49(18) . . ? Au2 Cu1 Au1 62.34(11) . . ? Au2 Cu1 Cu3 135.7(2) . . ? Au2 Cu1 Cu4 163.8(3) . . ? Au6 Cu1 Cu3 64.98(16) . . ? Au6 Cu1 Cu4 60.93(16) . . ? Au1 Cu1 Au6 80.28(15) . . ? Au1 Cu1 Cu3 145.2(2) . . ? Au1 Cu1 Cu4 104.3(2) . . ? Cu4 Cu1 Cu3 60.48(18) . . ? S2 Cu1 Au7 112.1(3) . . ? S2 Cu1 Au2 98.2(3) . . ? S2 Cu1 Au6 113.7(3) . . ? S2 Cu1 Au1 160.5(3) . . ? S2 Cu1 Cu3 50.4(3) . . ? S2 Cu1 Cu4 94.6(3) . . ? S2 Cu1 S1 94.5(4) . . ? S1 Cu1 Au7 153.4(4) . . ? S1 Cu1 Au2 117.2(3) . . ? S1 Cu1 Au6 108.0(3) . . ? S1 Cu1 Au1 93.8(3) . . ? S1 Cu1 Cu3 97.9(3) . . ? S1 Cu1 Cu4 51.5(3) . . ? Cu5 Cu7 Au14 54.20(13) . . ? Cu6 Cu7 Au14 56.82(15) . . ? Cu6 Cu7 Cu5 72.09(19) . . ? Cu6 Cu7 Cu8 111.8(2) . . ? Cu8 Cu7 Au14 57.15(15) . . ? Cu8 Cu7 Cu5 57.20(18) . . ? S8 Cu7 Au14 103.3(3) . . ? S8 Cu7 Cu5 50.8(2) . . ? S8 Cu7 Cu6 87.1(3) . . ? S8 Cu7 Cu8 92.5(3) . . ? S8 Cu7 S11 122.5(5) . . ? S11 Cu7 Au14 93.1(3) . . ? S11 Cu7 Cu5 108.8(4) . . ? S11 Cu7 Cu6 143.6(3) . . ? S11 Cu7 Cu8 52.3(3) . . ? S10 Cu7 Au14 95.6(3) . . ? S10 Cu7 Cu5 125.6(3) . . ? S10 Cu7 Cu6 53.9(3) . . ? S10 Cu7 Cu8 146.3(3) . . ? S10 Cu7 S8 114.7(4) . . ? S10 Cu7 S11 117.9(4) . . ? Cu2 Cu3 Au6 55.13(15) . . ? Cu2 Cu3 Cu1 72.81(19) . . ? Cu2 Cu3 Cu4 109.2(2) . . ? Cu1 Cu3 Au6 53.64(14) . . ? Cu4 Cu3 Au6 55.62(15) . . ? Cu4 Cu3 Cu1 56.30(17) . . ? S2 Cu3 Au6 102.6(3) . . ? S2 Cu3 Cu2 90.4(3) . . ? S2 Cu3 Cu1 50.3(3) . . ? S2 Cu3 Cu4 91.3(4) . . ? S2 Cu3 S4 119.0(4) . . ? S2 Cu3 S5 118.5(5) . . ? S4 Cu3 Au6 93.7(3) . . ? S4 Cu3 Cu2 53.3(3) . . ? S4 Cu3 Cu1 125.9(3) . . ? S4 Cu3 Cu4 142.2(4) . . ? S4 Cu3 S5 119.1(4) . . ? S5 Cu3 Au6 92.1(3) . . ? S5 Cu3 Cu2 141.7(4) . . ? S5 Cu3 Cu1 105.5(4) . . ? S5 Cu3 Cu4 50.4(3) . . ? Au14 Cu8 Cu7 65.02(17) . . ? Cu5 Cu8 Au14 58.40(15) . . ? Cu5 Cu8 Cu7 63.19(19) . . ? S12 Cu8 Au14 55.7(2) . . ? S12 Cu8 Cu5 110.4(3) . . ? S12 Cu8 Cu7 104.7(3) . . ? S7 Cu8 Au14 108.3(3) . . ? S7 Cu8 Cu5 54.8(3) . . ? S7 Cu8 Cu7 103.1(3) . . ? S7 Cu8 S12 135.2(4) . . ? S7 Cu8 S11 129.8(4) . . ? S11 Cu8 Au14 99.9(4) . . ? S11 Cu8 Cu5 115.8(3) . . ? S11 Cu8 Cu7 53.5(3) . . ? S11 Cu8 S12 95.0(4) . . ? Au6 Cu4 Cu3 65.30(17) . . ? Cu1 Cu4 Au6 58.77(15) . . ? Cu1 Cu4 Cu3 63.22(19) . . ? S6 Cu4 Au6 55.7(2) . . ? S6 Cu4 Cu1 111.4(3) . . ? S6 Cu4 Cu3 103.8(3) . . ? S5 Cu4 Au6 100.9(4) . . ? S5 Cu4 Cu1 113.8(3) . . ? S5 Cu4 Cu3 52.0(3) . . ? S5 Cu4 S6 96.3(4) . . ? S1 Cu4 Au6 108.5(3) . . ? S1 Cu4 Cu1 54.2(3) . . ? S1 Cu4 Cu3 102.0(4) . . ? S1 Cu4 S6 137.8(5) . . ? S1 Cu4 S5 125.8(5) . . ? C107 P5 Au5 110.9(12) . . ? C107 P5 C106 107.2(15) . . ? C107 P5 C113 106.3(16) . . ? C106 P5 Au5 108.3(11) . . ? C113 P5 Au5 121.6(11) . . ? C113 P5 C106 101.4(18) . . ? C276 P11 Au13 123.2(10) . . ? C276 P11 C277 102.4(15) . . ? C276 P11 C283 107.2(17) . . ? C277 P11 Au13 110.0(11) . . ? C277 P11 C283 104.5(18) . . ? C283 P11 Au13 108.0(11) . . ? C94 P2 Au2 114.4(11) . . ? C94 P2 C88 111.8(16) . . ? C94 P2 C100 105.8(17) . . ? C88 P2 Au2 112.0(13) . . ? C100 P2 Au2 109.8(11) . . ? C100 P2 C88 102.0(17) . . ? C69 P3 Au3 128.3(9) . . ? C63 P3 Au3 110.7(11) . . ? C63 P3 C69 105.5(15) . . ? C63 P3 C57 109.6(13) . . ? C57 P3 Au3 97.3(8) . . ? C57 P3 C69 103.9(13) . . ? C44 P6 Au8 103.7(10) . . ? C51 P6 Au8 110.8(12) . . ? C51 P6 C44 106.9(15) . . ? C51 P6 C45 106.7(16) . . ? C45 P6 Au8 113.8(10) . . ? C45 P6 C44 114.9(14) . . ? C150 S9 Cu6 96.6(12) . . ? C163 P7 Au9 100.5(11) . . ? C157 P7 Au9 115.8(14) . . ? C157 P7 C163 106.4(17) . . ? C157 P7 C169 102.8(17) . . ? C169 P7 Au9 124.9(13) . . ? C169 P7 C163 104.7(15) . . ? C132 P4 Au4 105.2(11) . . ? C132 P4 C139 106.3(17) . . ? C133 P4 Au4 114.7(11) . . ? C133 P4 C132 112.6(17) . . ? C133 P4 C139 101.9(16) . . ? C139 P4 Au4 116.0(12) . . ? C189 P12 Au16 111.9(11) . . ? C189 P12 C188 114.9(15) . . ? C188 P12 Au16 105.0(10) . . ? C195 P12 Au16 112.9(13) . . ? C195 P12 C189 106.3(17) . . ? C195 P12 C188 105.9(18) . . ? Cu8 S12 Au14 71.9(3) . . ? C155 S12 Au14 102.1(14) . . ? C155 S12 Cu8 96.7(13) . . ? C6 S3 Cu2 94.2(13) . . ? C19 P1 Au1 111.3(9) . . ? C19 P1 C25 104.4(15) . . ? C19 P1 C13 107.7(17) . . ? C25 P1 Au1 129.2(10) . . ? C13 P1 Au1 99.1(14) . . ? C13 P1 C25 103.1(15) . . ? C257 P10 Au12 103.9(11) . . ? C251 P10 Au12 115.3(15) . . ? C251 P10 C257 113.9(16) . . ? C251 P10 C245 103.1(19) . . ? C245 P10 Au12 115.0(11) . . ? C245 P10 C257 105.6(17) . . ? C207 P8 Au10 111.0(16) . . ? C207 P8 C213 101.4(19) . . ? C207 P8 C201 108(2) . . ? C213 P8 Au10 112.1(12) . . ? C201 P8 Au10 109.6(14) . . ? C201 P8 C213 114.5(19) . . ? Cu8 S7 Cu5 73.2(3) . . ? C146 S7 Cu5 96.9(13) . . ? C146 S7 Cu8 103.0(13) . . ? C239 P9 Au11 101.3(11) . . ? C239 P9 C232 104.6(15) . . ? C239 P9 C233 106.0(18) . . ? C232 P9 Au11 123.8(11) . . ? C233 P9 Au11 113.1(12) . . ? C233 P9 C232 106.2(17) . . ? Cu5 S8 Cu7 77.5(3) . . ? C147 S8 Cu5 98.5(14) . . ? C147 S8 Cu7 104.3(14) . . ? Cu1 S2 Cu3 79.4(3) . . ? C3 S2 Cu1 97.6(14) . . ? C3 S2 Cu3 100.6(13) . . ? Cu4 S6 Au6 72.7(3) . . ? C11 S6 Au6 102.9(14) . . ? C11 S6 Cu4 97.1(15) . . ? Cu2 S4 Cu3 70.9(3) . . ? C7 S4 Cu2 96.2(11) . . ? C7 S4 Cu3 112.5(13) . . ? Cu8 S11 Cu7 74.2(3) . . ? C154 S11 Cu7 108.4(13) . . ? C154 S11 Cu8 97.3(13) . . ? Cu6 S10 Cu7 70.5(3) . . ? C151 S10 Cu6 96.3(12) . . ? C151 S10 Cu7 109.2(13) . . ? Cu4 S5 Cu3 77.6(3) . . ? C10 S5 Cu3 104.6(17) . . ? C10 S5 Cu4 93.9(13) . . ? Cu4 S1 Cu1 74.3(4) . . ? C2 S1 Cu1 96.8(13) . . ? C2 S1 Cu4 97.6(13) . . ? C72 C73 H73 119.2 . . ? C74 C73 H73 119.2 . . ? C74 C73 C72 122(3) . . ? C267 C276 P11 125(3) . . ? C267 C276 C275 116(3) . . ? C275 C276 P11 119(3) . . ? C73 C72 C77 117(3) . . ? C71 C72 C73 128(3) . . ? C71 C72 C77 115(3) . . ? C164 C163 P7 119(3) . . ? C168 C163 P7 118(3) . . ? C168 C163 C164 123(3) . . ? C88 C79 C78 125(3) . . ? C88 C79 C80 119(3) . . ? C80 C79 C78 115(2) . . ? C258 C257 P10 111(2) . . ? C258 C257 C266 120(3) . . ? C266 C257 P10 129(3) . . ? C93 C94 P2 123(3) . . ? C93 C94 C89 120(3) . . ? C89 C94 P2 117(3) . . ? C78 C69 P3 123(2) . . ? C78 C69 C70 118(3) . . ? C70 C69 P3 119(2) . . ? C94 C93 H93 119.2 . . ? C92 C93 C94 122(4) . . ? C92 C93 H93 119.2 . . ? C92 C91 H91 121.2 . . ? C90 C91 H91 121.2 . . ? C90 C91 C92 118(3) . . ? C190 C189 P12 119(3) . . ? C190 C189 C194 118(3) . . ? C194 C189 P12 123(3) . . ? C44 C35 C34 121(3) . . ? C36 C35 C34 121(3) . . ? C36 C35 C44 118(3) . . ? C93 C92 C91 121(4) . . ? C93 C92 H92 119.3 . . ? C91 C92 H92 119.3 . . ? C63 C68 H68 119.7 . . ? C67 C68 H68 119.7 . . ? C67 C68 C63 121(4) . . ? C3 C2 S1 127(3) . . ? C3 C2 C1 119(4) . . ? C1 C2 S1 114(3) . . ? C232 C231 H231 122.1 . . ? C230 C231 H231 122.1 . . ? C230 C231 C232 116(4) . . ? C124 C125 H125 119.4 . . ? C126 C125 H125 119.4 . . ? C126 C125 C124 121(4) . . ? C115 C114 H114 116.4 . . ? C115 C114 C113 127(4) . . ? C113 C114 H114 116.4 . . ? C59 C60 H60 119.6 . . ? C61 C60 H60 119.6 . . ? C61 C60 C59 121(4) . . ? C60 C59 H59 122.6 . . ? C60 C59 C58 115(3) . . ? C58 C59 H59 122.6 . . ? C123 C132 P4 128(3) . . ? C123 C132 C131 119(3) . . ? C131 C132 P4 113(3) . . ? C69 C78 C79 120(3) . . ? C69 C78 C77 119(3) . . ? C77 C78 C79 121(3) . . ? C186 C185 C180 118(3) . . ? C184 C185 C186 124(4) . . ? C184 C185 C180 118(4) . . ? C79 C88 P2 126(3) . . ? C79 C88 C87 120(4) . . ? C87 C88 P2 114(3) . . ? C99 C100 P2 117(3) . . ? C95 C100 P2 123(2) . . ? C95 C100 C99 119(4) . . ? C175 C174 H174 119.2 . . ? C173 C174 H174 119.2 . . ? C173 C174 C175 122(4) . . ? C276 C267 C266 122(3) . . ? C276 C267 C268 121(3) . . ? C268 C267 C266 115(3) . . ? C108 C107 P5 122(3) . . ? C108 C107 C112 115(4) . . ? C112 C107 P5 122(3) . . ? C73 C74 H74 119.0 . . ? C73 C74 C75 122(3) . . ? C75 C74 H74 119.0 . . ? C24 C19 P1 121(2) . . ? C20 C19 P1 121(2) . . ? C20 C19 C24 118(3) . . ? C25 C34 C35 122(2) . . ? C25 C34 C33 118(3) . . ? C33 C34 C35 119(3) . . ? C276 C275 H275 116.2 . . ? C274 C275 C276 128(4) . . ? C274 C275 H275 116.2 . . ? C38 C37 H37 117.3 . . ? C38 C37 C36 125(4) . . ? C36 C37 H37 117.3 . . ? C43 C42 H42 118.4 . . ? C41 C42 H42 118.4 . . ? C41 C42 C43 123(3) . . ? C42 C43 H43 120.9 . . ? C44 C43 C42 118(3) . . ? C44 C43 H43 120.9 . . ? C35 C44 P6 130(2) . . ? C43 C44 P6 108(2) . . ? C43 C44 C35 122(2) . . ? C129 C124 C125 117(3) . . ? C129 C124 C123 118(3) . . ? C123 C124 C125 125(3) . . ? C19 C24 H24 118.8 . . ? C19 C24 C23 122(4) . . ? C23 C24 H24 118.8 . . ? C258 C259 H259 119.5 . . ? C258 C259 C260 121(3) . . ? C260 C259 H259 119.5 . . ? C101 C106 P5 121(3) . . ? C101 C106 C105 120(3) . . ? C105 C106 P5 119(3) . . ? C74 C75 H75 120.1 . . ? C76 C75 C74 120(3) . . ? C76 C75 H75 120.1 . . ? C72 C71 H71 115.9 . . ? C70 C71 C72 128(3) . . ? C70 C71 H71 115.9 . . ? C177 C178 C179 118(3) . . ? C169 C178 C177 119(3) . . ? C169 C178 C179 123(3) . . ? C72 C77 C78 120(3) . . ? C76 C77 C72 118(3) . . ? C76 C77 C78 122(3) . . ? C257 C258 H258 119.6 . . ? C259 C258 C257 121(3) . . ? C259 C258 H258 119.6 . . ? C162 C157 P7 121(3) . . ? C158 C157 P7 123(4) . . ? C158 C157 C162 116(4) . . ? C187 C188 P12 111(2) . . ? C179 C188 P12 131(3) . . ? C179 C188 C187 118(3) . . ? C260 C265 C266 120(3) . . ? C260 C265 C264 119(3) . . ? C264 C265 C266 122(3) . . ? C275 C274 H274 121.2 . . ? C275 C274 C273 118(4) . . ? C273 C274 H274 121.2 . . ? C264 C263 H263 119.9 . . ? C262 C263 H263 119.9 . . ? C262 C263 C264 120(3) . . ? C189 C190 H190 120.7 . . ? C189 C190 C191 119(4) . . ? C191 C190 H190 120.7 . . ? C257 C266 C267 123(3) . . ? C257 C266 C265 119(3) . . ? C265 C266 C267 119(3) . . ? C56 C51 P6 120(3) . . ? C52 C51 P6 127(3) . . ? C52 C51 C56 112(4) . . ? C42 C41 C36 116(3) . . ? C42 C41 C40 123(3) . . ? C40 C41 C36 121(3) . . ? N4 C8 C7 177(5) . . ? C19 C20 H20 119.1 . . ? C19 C20 C21 122(3) . . ? C21 C20 H20 119.1 . . ? N7 C145 C146 177(5) . . ? C2 C3 S2 124(3) . . ? C2 C3 C4 123(4) . . ? C4 C3 S2 113(4) . . ? C8 C7 S4 117(3) . . ? C6 C7 S4 123(2) . . ? C6 C7 C8 120(3) . . ? C7 C6 S3 128(3) . . ? C7 C6 C5 118(4) . . ? C5 C6 S3 114(3) . . ? C60 C61 H61 118.9 . . ? C62 C61 C60 122(4) . . ? C62 C61 H61 118.9 . . ? C64 C65 H65 118.7 . . ? C66 C65 H65 118.7 . . ? C66 C65 C64 123(4) . . ? C68 C63 P3 121(3) . . ? C64 C63 P3 120(2) . . ? C64 C63 C68 119(3) . . ? C278 C277 P11 119(3) . . ? C282 C277 P11 122(3) . . ? C282 C277 C278 120(4) . . ? C274 C273 C268 120(3) . . ? C272 C273 C274 125(4) . . ? C272 C273 C268 115(4) . . ? C88 C87 H87 118.6 . . ? C86 C87 C88 123(4) . . ? C86 C87 H87 118.6 . . ? C58 C57 P3 119.3(17) . . ? C62 C57 P3 124.4(19) . . ? C62 C57 C58 116(3) . . ? C100 C99 H99 121.6 . . ? C98 C99 C100 117(4) . . ? C98 C99 H99 121.6 . . ? C124 C129 C128 118(4) . . ? C130 C129 C124 121(3) . . ? C130 C129 C128 120(4) . . ? C25 C26 H26 120.0 . . ? C27 C26 H26 120.0 . . ? C27 C26 C25 120(3) . . ? N1 C1 C2 172(6) . . ? C176 C177 C178 124(3) . . ? C176 C177 C172 116(3) . . ? C172 C177 C178 119(3) . . ? C107 C108 H108 118.9 . . ? C107 C108 C109 122(4) . . ? C109 C108 H108 118.9 . . ? C244 C239 P9 117(3) . . ? C240 C239 P9 130(4) . . ? C240 C239 C244 113(4) . . ? C163 C164 H164 121.9 . . ? C163 C164 C165 116(4) . . ? C165 C164 H164 121.9 . . ? C107 C112 H112 119.0 . . ? C111 C112 C107 122(4) . . ? C111 C112 H112 119.0 . . ? C34 C25 P1 118.1(19) . . ? C34 C25 C26 119(3) . . ? C26 C25 P1 122(2) . . ? C157 C162 H162 120.8 . . ? C157 C162 C161 118(4) . . ? C161 C162 H162 120.8 . . ? C112 C111 H111 120.8 . . ? C110 C111 C112 118(5) . . ? C110 C111 H111 120.8 . . ? C178 C169 P7 121(3) . . ? C178 C169 C170 118(3) . . ? C170 C169 P7 121(2) . . ? C134 C133 P4 118(3) . . ? C138 C133 P4 122(2) . . ? C138 C133 C134 120(4) . . ? C11 C10 S5 130(3) . . ? C11 C10 C9 115(4) . . ? C9 C10 S5 115(3) . . ? C189 C194 H194 118.2 . . ? C193 C194 C189 124(4) . . ? C193 C194 H194 118.2 . . ? C163 C168 H168 122.2 . . ? C163 C168 C167 116(4) . . ? C167 C168 H168 122.2 . . ? C265 C260 C259 120(3) . . ? C261 C260 C259 121(3) . . ? C261 C260 C265 120(3) . . ? C106 C101 H101 120.2 . . ? C106 C101 C102 120(4) . . ? C102 C101 H101 120.2 . . ? C200 C195 P12 122(3) . . ? C196 C195 P12 124(3) . . ? C196 C195 C200 113(3) . . ? C120 C121 C122 121(3) . . ? C116 C121 C120 120(3) . . ? C116 C121 C122 119(3) . . ? C82 C81 H81 117.9 . . ? C82 C81 C80 124(4) . . ? C80 C81 H81 117.9 . . ? C114 C115 H115 120.7 . . ? C114 C115 C116 119(3) . . ? C116 C115 H115 120.7 . . ? C170 C171 H171 119.6 . . ? C170 C171 C172 121(4) . . ? C172 C171 H171 119.6 . . ? C87 C86 H86 119.5 . . ? C87 C86 C85 121(4) . . ? C85 C86 H86 119.5 . . ? C114 C113 P5 123(3) . . ? C114 C113 C122 115(3) . . ? C122 C113 P5 121(3) . . ? C265 C264 H264 120.0 . . ? C263 C264 C265 120(3) . . ? C263 C264 H264 120.0 . . ? C231 C232 P9 115(3) . . ? C223 C232 P9 123(2) . . ? C223 C232 C231 122(3) . . ? C204 C203 H203 122.2 . . ? C204 C203 C202 116(4) . . ? C202 C203 H203 122.2 . . ? C69 C70 H70 120.6 . . ? C71 C70 C69 119(3) . . ? C71 C70 H70 120.6 . . ? C155 C154 S11 125(3) . . ? C155 C154 C153 119(4) . . ? C153 C154 S11 116(3) . . ? C59 C58 H58 116.8 . . ? C57 C58 C59 126(3) . . ? C57 C58 H58 116.8 . . ? C207 C208 H208 117.9 . . ? C209 C208 H208 117.9 . . ? C209 C208 C207 124(5) . . ? C129 C130 H130 120.3 . . ? C131 C130 C129 119(3) . . ? C131 C130 H130 120.3 . . ? C224 C225 H225 118.5 . . ? C226 C225 H225 118.5 . . ? C226 C225 C224 123(5) . . ? C91 C90 H90 119.1 . . ? C91 C90 C89 122(3) . . ? C89 C90 H90 119.1 . . ? C154 C155 S12 126(3) . . ? C154 C155 C156 119(4) . . ? C156 C155 S12 114(3) . . ? C162 C161 H161 119.1 . . ? C160 C161 C162 122(5) . . ? C160 C161 H161 119.1 . . ? C150 C151 S10 123(2) . . ? C152 C151 S10 117(3) . . ? C152 C151 C150 120(3) . . ? C37 C38 H38 121.2 . . ? C37 C38 C39 118(3) . . ? C39 C38 H38 121.2 . . ? C146 C147 S8 125(3) . . ? C146 C147 C148 112(4) . . ? C148 C147 S8 122(3) . . ? C145 C146 S7 115(3) . . ? C147 C146 S7 123(3) . . ? C147 C146 C145 123(4) . . ? C13 C14 H14 118.2 . . ? C13 C14 C15 124(4) . . ? C15 C14 H14 118.2 . . ? C185 C186 H186 119.4 . . ? C187 C186 C185 121(3) . . ? C187 C186 H186 119.4 . . ? C188 C187 H187 118.8 . . ? C186 C187 C188 122(3) . . ? C186 C187 H187 118.8 . . ? C231 C230 H230 117.1 . . ? C231 C230 C229 126(4) . . ? C229 C230 H230 117.1 . . ? C229 C228 H228 119.9 . . ? C227 C228 H228 119.9 . . ? C227 C228 C229 120(5) . . ? C151 C150 S9 126(2) . . ? C151 C150 C149 115(3) . . ? C149 C150 S9 119(3) . . ? C61 C62 C57 119(3) . . ? C61 C62 H62 120.3 . . ? C57 C62 H62 120.3 . . ? C195 C200 H200 119.9 . . ? C199 C200 C195 120(5) . . ? C199 C200 H200 119.9 . . ? C169 C170 H170 118.5 . . ? C171 C170 C169 123(4) . . ? C171 C170 H170 118.5 . . ? C161 C160 H160 120.2 . . ? C161 C160 C159 120(4) . . ? C159 C160 H160 120.2 . . ? C177 C176 H176 117.3 . . ? C175 C176 C177 125(4) . . ? C175 C176 H176 117.3 . . ? C103 C104 H104 118.8 . . ? C103 C104 C105 122(4) . . ? C105 C104 H104 118.8 . . ? C108 C109 H109 120.9 . . ? C110 C109 C108 118(5) . . ? C110 C109 H109 120.9 . . ? C26 C27 H27 118.8 . . ? C26 C27 C28 122(3) . . ? C28 C27 H27 118.8 . . ? C65 C64 H64 120.9 . . ? C63 C64 C65 118(3) . . ? C63 C64 H64 120.9 . . ? C288 C283 P11 120(3) . . ? C284 C283 P11 125(4) . . ? C284 C283 C288 115(3) . . ? N10 C152 C151 172(5) . . ? C111 C110 C109 123(5) . . ? C111 C110 H110 118.3 . . ? C109 C110 H110 118.3 . . ? C200 C199 H199 119.6 . . ? C198 C199 C200 121(5) . . ? C198 C199 H199 119.6 . . ? C188 C179 C178 121(3) . . ? C188 C179 C180 120(3) . . ? C180 C179 C178 119(3) . . ? C282 C281 H281 121.7 . . ? C282 C281 C280 117(5) . . ? C280 C281 H281 121.7 . . ? C86 C85 C84 122(3) . . ? C86 C85 C80 120(3) . . ? C84 C85 C80 118(3) . . ? C140 C139 P4 124(3) . . ? C144 C139 P4 120(4) . . ? C144 C139 C140 116(4) . . ? C174 C175 H175 121.0 . . ? C176 C175 C174 118(4) . . ? C176 C175 H175 121.0 . . ? C268 C269 H269 121.1 . . ? C268 C269 C270 118(4) . . ? C270 C269 H269 121.1 . . ? C75 C76 C77 122(3) . . ? C75 C76 H76 119.2 . . ? C77 C76 H76 119.2 . . ? C32 C33 C34 125(3) . . ? C28 C33 C34 124(3) . . ? C28 C33 C32 111(3) . . ? C160 C159 H159 121.3 . . ? C158 C159 C160 117(5) . . ? C158 C159 H159 121.3 . . ? C230 C229 C228 124(4) . . ? C230 C229 C224 117(4) . . ? C228 C229 C224 119(4) . . ? C245 C246 H246 118.4 . . ? C247 C246 H246 118.4 . . ? C247 C246 C245 123(4) . . ? C260 C261 H261 119.8 . . ? C260 C261 C262 120(4) . . ? C262 C261 H261 119.8 . . ? C94 C89 C90 118(3) . . ? C94 C89 H89 121.2 . . ? C90 C89 H89 121.2 . . ? C121 C120 H120 119.7 . . ? C119 C120 C121 121(4) . . ? C119 C120 H120 119.7 . . ? C203 C204 H204 117.5 . . ? C205 C204 C203 125(4) . . ? C205 C204 H204 117.5 . . ? C129 C128 H128 120.7 . . ? C127 C128 C129 118(4) . . ? C127 C128 H128 120.8 . . ? C14 C13 P1 118(3) . . ? C14 C13 C18 114(4) . . ? C18 C13 P1 128(3) . . ? C277 C278 H278 120.6 . . ? C279 C278 C277 119(3) . . ? C279 C278 H278 120.6 . . ? C185 C184 H184 119.2 . . ? C183 C184 C185 122(4) . . ? C183 C184 H184 119.2 . . ? C199 C198 H198 119.8 . . ? C199 C198 C197 120(5) . . ? C197 C198 H198 119.8 . . ? C85 C84 H84 119.2 . . ? C83 C84 C85 122(4) . . ? C83 C84 H84 119.2 . . ? C133 C134 H134 118.8 . . ? C133 C134 C135 122(4) . . ? C135 C134 H134 118.8 . . ? C132 C123 C124 120(3) . . ? C132 C123 C122 126(3) . . ? C124 C123 C122 114(3) . . ? C33 C32 H32 115.4 . . ? C31 C32 C33 129(4) . . ? C31 C32 H32 115.4 . . ? N6 C12 C11 175(5) . . ? C198 C197 H197 120.4 . . ? C196 C197 C198 119(5) . . ? C196 C197 H197 120.4 . . ? C177 C172 C171 119(4) . . ? C177 C172 C173 119(4) . . ? C171 C172 C173 122(4) . . ? C140 C141 H141 120.7 . . ? C140 C141 C142 119(5) . . ? C142 C141 H141 120.7 . . ? C277 C282 C281 124(4) . . ? C277 C282 H282 117.9 . . ? C281 C282 H282 117.9 . . ? C28 C29 H29 120.7 . . ? C30 C29 H29 120.7 . . ? C30 C29 C28 119(4) . . ? C256 C255 H255 118.4 . . ? C254 C255 H255 118.4 . . ? C254 C255 C256 123(6) . . ? C104 C103 H103 120.3 . . ? C102 C103 C104 119(4) . . ? C102 C103 H103 120.3 . . ? C283 C288 H288 118.8 . . ? C287 C288 C283 122(5) . . ? C287 C288 H288 118.8 . . ? C35 C36 C37 121(3) . . ? C35 C36 C41 123(3) . . ? C37 C36 C41 115(3) . . ? C101 C102 H102 119.6 . . ? C103 C102 C101 121(5) . . ? C103 C102 H102 119.6 . . ? C106 C105 H105 121.1 . . ? C104 C105 C106 118(4) . . ? C104 C105 H105 121.1 . . ? C48 C49 H49 120.0 . . ? C48 C49 C50 120.0 . . ? C50 C49 H49 120.0 . . ? C49 C48 H48 120.0 . . ? C47 C48 C49 120.0 . . ? C47 C48 H48 120.0 . . ? C48 C47 H47 120.0 . . ? C48 C47 C46 120.0 . . ? C46 C47 H47 120.0 . . ? C47 C46 H46 120.0 . . ? C45 C46 C47 120.0 . . ? C45 C46 H46 120.0 . . ? C46 C45 P6 117.7(16) . . ? C46 C45 C50 120.0 . . ? C50 C45 P6 122.3(16) . . ? C49 C50 H50 120.0 . . ? C45 C50 C49 120.0 . . ? C45 C50 H50 120.0 . . ? C184 C183 H183 119.8 . . ? C184 C183 C182 120(4) . . ? C182 C183 H183 119.8 . . ? C41 C40 H40 120.5 . . ? C39 C40 C41 119(3) . . ? C39 C40 H40 120.5 . . ? N2 C4 C3 172(10) . . ? C213 C222 C223 123(3) . . ? C221 C222 C213 122(4) . . ? C221 C222 C223 114(3) . . ? C208 C207 P8 121(3) . . ? C208 C207 C212 115(5) . . ? C212 C207 P8 122(3) . . ? N12 C156 C155 176(5) . . ? C194 C193 H193 119.8 . . ? C194 C193 C192 120(4) . . ? C192 C193 H193 119.8 . . ? C180 C181 H181 120.0 . . ? C182 C181 H181 120.0 . . ? C182 C181 C180 120(4) . . ? C195 C196 H196 117.6 . . ? C197 C196 C195 125(5) . . ? C197 C196 H196 117.6 . . ? C139 C140 C141 121(4) . . ? C139 C140 H140 119.4 . . ? C141 C140 H140 119.4 . . ? C13 C18 H18 116.3 . . ? C13 C18 C17 127(4) . . ? C17 C18 H18 116.3 . . ? C81 C82 H82 121.0 . . ? C81 C82 C83 118(4) . . ? C83 C82 H82 121.0 . . ? C204 C205 H205 122.3 . . ? C204 C205 C206 115(4) . . ? C206 C205 H205 122.3 . . ? C17 C16 H16 118.1 . . ? C15 C16 H16 118.1 . . ? C15 C16 C17 124(4) . . ? C68 C67 H67 120.2 . . ? C68 C67 C66 120(4) . . ? C66 C67 H67 120.2 . . ? C79 C80 C85 116(3) . . ? C81 C80 C79 126(3) . . ? C81 C80 C85 118(3) . . ? C18 C17 H17 123.4 . . ? C16 C17 C18 113(4) . . ? C16 C17 H17 123.4 . . ? C125 C126 H126 118.0 . . ? C127 C126 C125 124(4) . . ? C127 C126 H126 118.0 . . ? C239 C244 H244 118.4 . . ? C243 C244 C239 123(4) . . ? C243 C244 H244 118.4 . . ? N8 C148 C147 168(5) . . ? C243 C242 H242 117.3 . . ? C241 C242 H242 117.3 . . ? C241 C242 C243 125(6) . . ? C252 C253 H253 122.5 . . ? C254 C253 H253 122.5 . . ? C254 C253 C252 115(5) . . ? C253 C252 H252 119.0 . . ? C251 C252 C253 122(5) . . ? C251 C252 H252 119.0 . . ? C56 C55 H55 118.9 . . ? C56 C55 C54 122(5) . . ? C54 C55 H55 118.9 . . ? C273 C268 C267 118(3) . . ? C269 C268 C267 122(3) . . ? C269 C268 C273 121(4) . . ? C174 C173 C172 120(4) . . ? C174 C173 H173 120.1 . . ? C172 C173 H173 120.1 . . ? C249 C248 H248 118.3 . . ? C249 C248 C247 123(4) . . ? C247 C248 H248 118.3 . . ? C225 C224 C229 118(4) . . ? C225 C224 C223 124(4) . . ? C223 C224 C229 118(4) . . ? N11 C153 C154 171(5) . . ? C233 C234 H234 118.4 . . ? C233 C234 C235 123(5) . . ? C235 C234 H234 118.4 . . ? C234 C233 P9 122(3) . . ? C234 C233 C238 118(4) . . ? C238 C233 P9 121(3) . . ? C214 C215 H215 119.6 . . ? C214 C215 C216 121(5) . . ? C216 C215 H215 119.6 . . ? C248 C249 H249 121.2 . . ? C248 C249 C250 118(4) . . ? C250 C249 H249 121.2 . . ? C24 C23 H23 120.9 . . ? C22 C23 C24 118(4) . . ? C22 C23 H23 120.9 . . ? C252 C251 P10 124(4) . . ? C252 C251 C256 114(4) . . ? C256 C251 P10 122(3) . . ? C100 C95 H95 118.9 . . ? C100 C95 C96 122(4) . . ? C96 C95 H95 118.9 . . ? C239 C240 H240 116.2 . . ? C241 C240 C239 128(6) . . ? C241 C240 H240 116.2 . . ? C121 C116 C115 119(3) . . ? C121 C116 C117 117(4) . . ? C115 C116 C117 124(4) . . ? C255 C256 C251 119(5) . . ? C255 C256 H256 120.3 . . ? C251 C256 H256 120.3 . . ? C222 C213 P8 130(3) . . ? C214 C213 P8 115(3) . . ? C214 C213 C222 114(4) . . ? C263 C262 C261 121(4) . . ? C263 C262 H262 119.7 . . ? C261 C262 H262 119.7 . . ? C51 C56 H56 119.8 . . ? C55 C56 C51 120(4) . . ? C55 C56 H56 119.8 . . ? C255 C254 C253 126(6) . . ? C255 C254 H254 116.8 . . ? C253 C254 H254 116.8 . . ? C120 C119 H119 119.8 . . ? C120 C119 C118 120(4) . . ? C118 C119 H119 119.8 . . ? C10 C11 S6 123(3) . . ? C10 C11 C12 120(4) . . ? C12 C11 S6 117(3) . . ? C38 C39 H39 119.6 . . ? C40 C39 C38 121(3) . . ? C40 C39 H39 119.6 . . ? C95 C96 H96 120.4 . . ? C97 C96 C95 119(4) . . ? C97 C96 H96 120.4 . . ? N9 C149 C150 172(5) . . ? C134 C135 H135 121.9 . . ? C136 C135 C134 116(5) . . ? C136 C135 H135 121.9 . . ? C273 C272 H272 117.7 . . ? C271 C272 C273 125(5) . . ? C271 C272 H272 117.7 . . ? C128 C127 H127 119.8 . . ? C126 C127 C128 120(4) . . ? C126 C127 H127 119.8 . . ? C244 C243 C242 115(5) . . ? C244 C243 H243 122.5 . . ? C242 C243 H243 122.5 . . ? C193 C192 H192 121.0 . . ? C193 C192 C191 118(4) . . ? C191 C192 H192 121.0 . . ? C99 C98 H98 117.9 . . ? C97 C98 C99 124(4) . . ? C97 C98 H98 117.9 . . ? C27 C28 C33 115(3) . . ? C27 C28 C29 120(3) . . ? C33 C28 C29 125(3) . . ? C249 C250 H250 120.1 . . ? C245 C250 C249 120(4) . . ? C245 C250 H250 120.1 . . ? C278 C279 H279 119.4 . . ? C278 C279 C280 121(3) . . ? C280 C279 H279 119.4 . . ? C232 C223 C222 118(3) . . ? C232 C223 C224 122(3) . . ? C224 C223 C222 120(3) . . ? C221 C220 H220 119.9 . . ? C219 C220 H220 119.9 . . ? C219 C220 C221 120(4) . . ? C65 C66 C67 119(4) . . ? C65 C66 H66 120.3 . . ? C67 C66 H66 120.3 . . ? C205 C206 H206 117.3 . . ? C201 C206 C205 125(4) . . ? C201 C206 H206 117.3 . . ? C207 C212 H212 119.0 . . ? C211 C212 C207 122(5) . . ? C211 C212 H212 119.0 . . ? C281 C280 H280 120.3 . . ? C279 C280 C281 119(4) . . ? C279 C280 H280 120.3 . . ? C269 C270 H270 120.5 . . ? C271 C270 C269 119(6) . . ? C271 C270 H270 120.5 . . ? C185 C180 C179 120(3) . . ? C185 C180 C181 119(3) . . ? C181 C180 C179 121(3) . . ? C132 C131 H131 119.4 . . ? C130 C131 C132 121(3) . . ? C130 C131 H131 119.4 . . ? C29 C30 H30 119.4 . . ? C29 C30 C31 121(4) . . ? C31 C30 H30 119.4 . . ? C165 C166 H166 119.4 . . ? C167 C166 H166 119.4 . . ? C167 C166 C165 121(5) . . ? C32 C31 C30 115(4) . . ? C32 C31 H31 122.6 . . ? C30 C31 H31 122.6 . . ? C246 C245 P10 118(3) . . ? C250 C245 P10 123(3) . . ? C250 C245 C246 119(4) . . ? C283 C284 H284 117.3 . . ? C283 C284 C285 125(4) . . ? C285 C284 H284 117.3 . . ? C121 C122 C123 115(3) . . ? C113 C122 C121 120(3) . . ? C113 C122 C123 125(3) . . ? C20 C21 H21 120.6 . . ? C22 C21 C20 119(3) . . ? C22 C21 H21 120.6 . . ? C190 C191 C192 121(4) . . ? C190 C191 H191 119.4 . . ? C192 C191 H191 119.4 . . ? C157 C158 H158 116.6 . . ? C159 C158 C157 127(5) . . ? C159 C158 H158 116.6 . . ? C164 C165 H165 120.3 . . ? C166 C165 C164 119(5) . . ? C166 C165 H165 120.3 . . ? C228 C227 H227 119.9 . . ? C228 C227 C226 120(5) . . ? C226 C227 H227 119.9 . . ? C133 C138 H138 120.7 . . ? C133 C138 C137 119(4) . . ? C137 C138 H138 120.7 . . ? C84 C83 C82 120(4) . . ? C84 C83 H83 120.0 . . ? C82 C83 H83 120.0 . . ? C141 C142 H142 119.8 . . ? C141 C142 C143 120(5) . . ? C143 C142 H142 119.8 . . ? C168 C167 H167 117.8 . . ? C166 C167 C168 124(5) . . ? C166 C167 H167 117.8 . . ? C215 C214 C213 125(5) . . ? C215 C214 H214 117.3 . . ? C213 C214 H214 117.4 . . ? C285 C286 H286 117.6 . . ? C285 C286 C287 125(5) . . ? C287 C286 H286 117.6 . . ? C138 C137 H137 120.0 . . ? C136 C137 C138 120(5) . . ? C136 C137 H137 120.0 . . ? C203 C202 H202 118.8 . . ? C201 C202 C203 122(5) . . ? C201 C202 H202 118.8 . . ? C222 C221 C220 123(3) . . ? C222 C221 C216 118(4) . . ? C220 C221 C216 118(3) . . ? N3 C5 C6 176(6) . . ? C284 C285 H285 122.0 . . ? C286 C285 C284 116(5) . . ? C286 C285 H285 122.0 . . ? C217 C218 H218 118.7 . . ? C217 C218 C219 123(5) . . ? C219 C218 H218 118.7 . . ? C221 C216 C215 118(4) . . ? C217 C216 C215 120(4) . . ? C217 C216 C221 121(4) . . ? C116 C117 H117 118.4 . . ? C118 C117 C116 123(5) . . ? C118 C117 H117 118.4 . . ? C206 C201 P8 124(3) . . ? C202 C201 P8 120(3) . . ? C202 C201 C206 116(4) . . ? C54 C53 H53 120.8 . . ? C52 C53 H53 120.8 . . ? C52 C53 C54 118(5) . . ? C55 C54 H54 120.4 . . ? C53 C54 C55 119(6) . . ? C53 C54 H54 120.4 . . ? C183 C182 H182 119.7 . . ? C181 C182 C183 121(4) . . ? C181 C182 H182 119.7 . . ? C208 C209 H209 121.6 . . ? C208 C209 C210 117(5) . . ? C210 C209 H209 121.6 . . ? C142 C143 H143 124.1 . . ? C144 C143 C142 112(5) . . ? C144 C143 H143 124.1 . . ? C96 C97 C98 118(4) . . ? C96 C97 H97 121.0 . . ? C98 C97 H97 121.0 . . ? C119 C118 H118 120.8 . . ? C117 C118 C119 118(5) . . ? C117 C118 H118 120.8 . . ? C246 C247 C248 116(4) . . ? C246 C247 H247 122.0 . . ? C248 C247 H247 122.0 . . ? N5 C9 C10 170(6) . . ? C135 C136 C137 123(6) . . ? C135 C136 H136 118.7 . . ? C137 C136 H136 118.7 . . ? C272 C271 C270 123(5) . . ? C272 C271 H271 118.7 . . ? C270 C271 H271 118.7 . . ? C225 C226 C227 120(5) . . ? C225 C226 H226 120.2 . . ? C227 C226 H226 120.2 . . ? C139 C144 H144 114.6 . . ? C143 C144 C139 131(5) . . ? C143 C144 H144 114.6 . . ? C237 C236 H236 113.7 . . ? C237 C236 C235 133(6) . . ? C235 C236 H236 113.7 . . ? C23 C22 H22 119.5 . . ? C21 C22 C23 121(4) . . ? C21 C22 H22 119.5 . . ? C236 C237 H237 125.4 . . ? C238 C237 C236 109(5) . . ? C238 C237 H237 125.4 . . ? C233 C238 H238 117.2 . . ? C237 C238 C233 126(5) . . ? C237 C238 H238 117.2 . . ? C234 C235 H235 124.4 . . ? C236 C235 C234 111(5) . . ? C236 C235 H235 124.4 . . ? C209 C210 H210 119.9 . . ? C211 C210 C209 120(6) . . ? C211 C210 H210 119.9 . . ? C212 C211 H211 120.1 . . ? C210 C211 C212 120(6) . . ? C210 C211 H211 120.1 . . ? C242 C241 C240 115(6) . . ? C242 C241 H241 122.3 . . ? C240 C241 H241 122.3 . . ? C51 C52 H52 116.5 . . ? C53 C52 C51 127(5) . . ? C53 C52 H52 116.5 . . ? C218 C217 C216 116(5) . . ? C218 C217 H217 121.9 . . ? C216 C217 H217 121.9 . . ? C220 C219 C218 121(5) . . ? C220 C219 H219 119.6 . . ? C218 C219 H219 119.6 . . ? C288 C287 H287 122.0 . . ? C286 C287 C288 116(5) . . ? C286 C287 H287 122.0 . . ? C14 C15 H15 121.2 . . ? C16 C15 C14 118(4) . . ? C16 C15 H15 121.2 . . ? _shelx_res_file ; TITL s_a.res in P2(1) s-cu4au8.res created by SHELXL-2016/6 at 23:12:11 on 04-Feb-2022 REM Old TITL S in P2(1) REM SHELXT solution in P2(1) REM R1 0.131, Rweak 0.035, Alpha 0.007, Orientation as input REM Flack x = 0.015 ( 0.006 ) from Parsons' quotients REM Formula found by SHELXT: C216 N54 O12 S24 Au5 Cu4 CELL 1.54184 16.6336 26.895 31.7629 90 91.346 90 ZERR 4 0.0002 0.0003 0.0004 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H Au Cu N P S UNIT 576 384 32 16 24 24 24 DFIX 1.13 0.01 C4 N2 DFIX 1.39 0.01 C62 C57 C62 C61 C61 C60 C60 C59 C59 C58 C58 C57 DFIX 1.39 0.01 C24 C19 C20 C19 C21 C20 C22 C21 C23 C22 C24 C23 DFIX 1.39 0.01 C211 C210 C210 C209 C208 C207 C212 C207 C212 C211 C209 C208 DFIX 1.39 0.01 C29 C28 C30 C29 C31 C30 C32 C31 C33 C32 C33 C28 DFIX 1.39 0.01 C136 C135 C137 C136 C138 C137 C138 C133 C134 C133 C135 C134 DFIX 1.39 0.01 C29 C28 C30 C29 C31 C30 C32 C31 C33 C32 C33 C28 C28 C27 C27 = C26 C26 C25 C34 C25 C34 C33 DFIX 1.39 0.01 C238 C237 C237 C236 C236 C235 C235 C234 C234 C233 C238 C233 DFIX 1.5 C79 C78 DFIX 1.5 C123 C122 DFIX 1.39 0.01 C15 C14 C14 C13 C18 C13 C18 C17 C17 C16 C16 C15 DELU 0.005 0.005 C13 C14 C15 C16 C17 C18 ISOR 0.01 0.02 C50 C48 C31 C286 N2 C144 ISOR 0.01 0.02 C49 C240 C142 C47 ISOR 0.01 0.02 C143 C140 C141 C67 C119 C133 C134 C136 C137 C135 C111 C110 = C26 C27 C25 C28 C30 C32 C45 C46 C245 C237 C236 C238 C220 ISOR 0.01 0.02 C219 C217 C218 C221 ISOR 0.01 0.02 C227 C229 C4 C112 C53 C52 C183 C254 C255 C242 C244 C241 C197 = C198 C199 ISOR 0.01 0.02 C198 C254 N11 ISOR 0.01 0.02 C9 N5 N4 C57 C60 C58 C59 C206 C209 C214 C216 C213 C284 ISOR 0.01 0.02 C18 ISOR 0.01 0.02 C235 C211 C210 C252 C253 C22 ISOR 0.01 0.02 C3 C2 C14 C17 C15 C153 C156 C287 C277 C5 C8 C65 C83 ISOR 0.01 0.02 C285 ISOR 0.01 0.02 C44 ISOR 0.01 0.02 C13 ISOR 0.01 0.02 C212 C207 C208 C209 C210 C211 ISOR 0.01 0.02 N8 ISOR 0.01 0.02 C233 C234 L.S. 14 0 0 PLAN 10 SIZE 0.12 0.12 0.2 BOND $H list 4 ABIN fmap 2 53 ACTA OMIT 9 0 21 OMIT 11 0 16 OMIT 11 -2 15 OMIT 7 0 23 OMIT 11 -1 17 OMIT 10 -2 15 OMIT 11 -1 18 OMIT 8 -1 22 OMIT 11 0 15 REM REM REM WGHT 0.129300 148.534103 FVAR 0.03531 AU7 3 0.652192 0.512706 0.872729 11.00000 0.02613 0.04394 = 0.04292 0.00197 -0.00251 -0.00038 AU15 3 0.195145 0.521042 0.401936 11.00000 0.03166 0.04487 = 0.03782 -0.00155 -0.00085 -0.00133 AU3 3 0.496100 0.530395 0.844808 11.00000 0.02538 0.04581 = 0.04569 0.00170 -0.00209 0.00072 AU5 3 0.702536 0.418365 0.907659 11.00000 0.03351 0.04392 = 0.04139 0.00191 0.00147 0.00253 AU13 3 0.271183 0.503881 0.480021 11.00000 0.03309 0.05522 = 0.03876 -0.00022 -0.00415 -0.00020 AU2 3 0.609350 0.606877 0.846956 11.00000 0.02666 0.04347 = 0.05685 0.00116 -0.00142 0.00138 AU12 3 0.180371 0.429785 0.438262 11.00000 0.04615 0.05461 = 0.03840 0.00335 -0.00293 -0.00983 AU4 3 0.543294 0.438244 0.877872 11.00000 0.03043 0.04850 = 0.04882 0.00907 0.00364 0.00040 AU14 3 0.286333 0.592624 0.438397 11.00000 0.03385 0.04893 = 0.05423 -0.00318 -0.00548 -0.00217 AU6 3 0.801302 0.500129 0.904267 11.00000 0.02699 0.05400 = 0.05064 -0.00148 -0.00202 -0.00048 AU8 3 0.597845 0.474861 0.799780 11.00000 0.02945 0.07193 = 0.04041 -0.00198 0.00023 0.00495 AU9 3 0.277462 0.559590 0.334556 11.00000 0.03855 0.04902 = 0.04416 0.00431 0.00559 0.00236 AU11 3 0.092276 0.451002 0.364802 11.00000 0.03996 0.05731 = 0.03965 -0.00192 -0.00392 -0.00874 AU1 3 0.739318 0.560476 0.812549 11.00000 0.03408 0.04990 = 0.06140 0.00869 0.01118 0.00366 AU10 3 0.113963 0.546376 0.330276 11.00000 0.04215 0.05991 = 0.04707 0.00366 -0.01202 -0.00675 AU16 3 0.251998 0.445290 0.358140 11.00000 0.04168 0.05775 = 0.05860 -0.01020 0.01344 -0.00159 CU5 4 0.178506 0.616067 0.378271 11.00000 0.03855 0.04040 = 0.05125 -0.00309 0.00294 0.00056 CU2 4 0.671737 0.499468 0.951048 11.00000 0.04114 0.05989 = 0.03817 -0.00223 -0.00181 0.00706 CU6 4 0.144283 0.562483 0.467609 11.00000 0.03058 0.06677 = 0.04645 -0.00947 -0.00279 0.00003 CU1 4 0.739808 0.592016 0.892821 11.00000 0.03077 0.05378 = 0.06212 -0.00575 -0.00959 -0.00507 CU7 4 0.150864 0.659747 0.459190 11.00000 0.03407 0.06765 = 0.06227 -0.00771 0.00405 0.00314 CU3 4 0.775863 0.565052 0.980910 11.00000 0.04120 0.07006 = 0.06461 -0.01198 0.00258 0.00088 CU8 4 0.276408 0.688705 0.408564 11.00000 0.04226 0.05188 = 0.07591 -0.00078 0.00069 -0.00267 CU4 4 0.896614 0.582228 0.919757 11.00000 0.03485 0.07217 = 0.06826 0.00102 -0.00489 -0.00657 P5 6 0.753259 0.339344 0.923157 11.00000 0.03570 0.04252 = 0.04714 0.00724 0.00566 0.00693 P11 6 0.355108 0.490239 0.537652 11.00000 0.03041 0.07048 = 0.03473 -0.00169 -0.00735 0.00054 P2 6 0.520284 0.671998 0.848160 11.00000 0.02896 0.04033 = 0.05274 -0.00459 -0.00327 0.00109 P3 6 0.364308 0.549051 0.828128 11.00000 0.01914 0.04958 = 0.05553 0.00100 -0.00566 0.00126 P6 6 0.663759 0.444556 0.743373 11.00000 0.02905 0.07309 = 0.03147 -0.00318 0.00505 -0.00060 S9 7 0.018861 0.537699 0.452229 11.00000 0.03272 0.08219 = 0.04607 -0.00258 -0.00166 -0.00657 P7 6 0.363052 0.579356 0.280459 11.00000 0.04014 0.04331 = 0.04579 0.00577 0.01076 -0.00099 P4 6 0.484589 0.370120 0.907883 11.00000 0.02767 0.04308 = 0.05227 0.00301 0.00607 -0.00849 P12 6 0.368634 0.421290 0.329149 11.00000 0.03853 0.04772 = 0.04366 0.00172 0.01262 0.00670 S12 7 0.389220 0.654918 0.440267 11.00000 0.02927 0.05525 = 0.06840 -0.00950 0.00276 -0.00752 S3 7 0.545798 0.526062 0.959545 11.00000 0.02933 0.06622 = 0.06658 -0.01034 0.00005 0.00693 P1 6 0.809407 0.584738 0.753368 11.00000 0.03637 0.05760 = 0.06463 0.02132 0.01305 0.00599 P10 6 0.171810 0.380955 0.497192 11.00000 0.05319 0.05592 = 0.03658 0.00941 -0.00592 -0.01063 P8 6 -0.002466 0.549529 0.290914 11.00000 0.04144 0.06638 = 0.05132 -0.00162 -0.02600 0.00010 S7 7 0.221163 0.686711 0.344056 11.00000 0.04460 0.05624 = 0.05882 0.00688 0.00084 -0.00276 P9 6 -0.000214 0.394489 0.338902 11.00000 0.04912 0.05056 = 0.04562 0.00135 0.00340 -0.01189 S8 7 0.063203 0.650878 0.402168 11.00000 0.02847 0.07063 = 0.05433 -0.00028 0.00127 0.00544 S2 7 0.698276 0.628905 0.953868 11.00000 0.03887 0.05960 = 0.08336 -0.02450 -0.00325 0.00305 S6 7 0.944515 0.505323 0.906153 11.00000 0.02612 0.08979 = 0.04906 0.00073 -0.00158 0.00231 S4 7 0.714669 0.502534 1.018180 11.00000 0.04986 0.07093 = 0.03621 -0.00337 -0.00303 0.00534 S11 7 0.234156 0.728318 0.467698 11.00000 0.04472 0.05453 = 0.09263 -0.02177 0.00304 0.00270 S10 7 0.114156 0.617193 0.518694 11.00000 0.03690 0.06967 = 0.04634 -0.01001 0.00119 0.00462 S5 7 0.912344 0.577961 0.990518 11.00000 0.04758 0.08978 = 0.05897 -0.01252 -0.01394 -0.00242 S1 7 0.845480 0.646292 0.883690 11.00000 0.04522 0.06717 = 0.08216 0.00856 -0.00713 -0.01475 C73 1 0.231219 0.733546 0.739037 11.00000 0.05357 0.06651 = 0.04867 0.00176 0.01316 -0.00498 AFIX 43 H73 2 0.211086 0.731632 0.711521 11.00000 -1.20000 AFIX 0 C276 1 0.346929 0.436675 0.571431 11.00000 0.03152 0.08094 = 0.03849 -0.01578 -0.00300 -0.00160 C72 1 0.262706 0.690328 0.758504 11.00000 0.03457 0.04890 = 0.03835 0.00000 -0.00219 0.01299 C163 1 0.291230 0.607211 0.242229 11.00000 0.05925 0.05807 = 0.02681 0.00836 0.00180 -0.00326 C79 1 0.354307 0.656289 0.868299 11.00000 0.02508 0.04055 = 0.03717 -0.00123 -0.00027 0.00433 C257 1 0.149050 0.425370 0.539371 11.00000 0.04421 0.04677 = 0.04120 0.00484 -0.01642 -0.00424 C94 1 0.488832 0.694521 0.796564 11.00000 0.04052 0.05439 = 0.03997 -0.01064 0.00384 0.00393 C69 1 0.323475 0.605798 0.803353 11.00000 0.02691 0.03438 = 0.07108 -0.01879 0.00700 -0.00861 C93 1 0.469716 0.743329 0.788467 11.00000 0.03389 0.04142 = 0.07469 0.01849 0.00258 -0.00831 AFIX 43 H93 2 0.471119 0.766131 0.810484 11.00000 -1.20000 AFIX 0 C91 1 0.445728 0.724815 0.714856 11.00000 0.01752 0.10295 = 0.06018 0.01324 -0.01192 -0.00222 AFIX 43 H91 2 0.431221 0.735738 0.687956 11.00000 -1.20000 AFIX 0 C189 1 0.355776 0.407569 0.273445 11.00000 0.03836 0.03865 = 0.07341 -0.01510 0.02512 -0.01118 N4 5 0.615885 0.532882 1.116731 11.00000 0.10116 0.11505 = 0.05306 -0.00302 0.01411 -0.00717 C35 1 0.835054 0.472244 0.738802 11.00000 0.04420 0.06578 = 0.04583 0.00352 -0.01375 0.00353 C92 1 0.449327 0.758720 0.750053 11.00000 0.03455 0.07354 = 0.07927 0.01031 0.00677 -0.00880 AFIX 43 H92 2 0.437074 0.792089 0.745685 11.00000 -1.20000 AFIX 0 C68 1 0.215794 0.535651 0.867226 11.00000 0.03007 0.08486 = 0.09641 0.00625 0.01991 -0.00096 AFIX 43 H68 2 0.191898 0.542517 0.841107 11.00000 -1.20000 AFIX 0 C2 1 0.826068 0.684098 0.925966 11.00000 0.04433 0.05231 = 0.06064 -0.00086 -0.01230 -0.00478 C231 1 -0.038911 0.366028 0.256075 11.00000 0.05913 0.07183 = 0.04492 0.01558 0.00219 -0.01508 AFIX 43 H231 2 -0.005204 0.339119 0.261662 11.00000 -1.20000 AFIX 0 C125 1 0.676613 0.294465 1.031570 11.00000 0.04584 0.08259 = 0.04580 0.01852 -0.00509 -0.00655 AFIX 43 H125 2 0.690372 0.266853 1.015653 11.00000 -1.20000 AFIX 0 C114 1 0.711394 0.239564 0.908441 11.00000 0.06230 0.05474 = 0.05339 -0.00053 -0.00095 0.01418 AFIX 43 H114 2 0.762909 0.237664 0.897791 11.00000 -1.20000 AFIX 0 C60 1 0.337383 0.429435 0.724535 11.00000 0.07856 0.07183 = 0.06914 -0.00405 -0.01011 0.00136 AFIX 43 H60 2 0.332865 0.404593 0.704250 11.00000 -1.20000 AFIX 0 C59 1 0.397163 0.465334 0.721345 11.00000 0.05208 0.06306 = 0.02931 -0.00695 -0.00896 0.00673 AFIX 43 H59 2 0.432451 0.466269 0.699078 11.00000 -1.20000 AFIX 0 C132 1 0.533664 0.363855 0.959903 11.00000 0.03936 0.05743 = 0.03668 0.00982 0.01388 0.00101 C78 1 0.324983 0.651970 0.823072 11.00000 0.02717 0.06831 = 0.02773 -0.00528 0.00127 -0.00790 C185 1 0.542285 0.544080 0.379293 11.00000 0.04431 0.11096 = 0.04064 0.01500 -0.01883 -0.03817 C88 1 0.433773 0.658730 0.881441 11.00000 0.06393 0.04751 = 0.06657 -0.00946 -0.01846 -0.00259 C100 1 0.566436 0.724912 0.875067 11.00000 0.01890 0.07844 = 0.06976 -0.00463 -0.01120 -0.00529 C174 1 0.595048 0.395661 0.194302 11.00000 0.05879 0.06023 = 0.07684 -0.01433 0.00569 0.00946 AFIX 43 H174 2 0.621575 0.372350 0.178051 11.00000 -1.20000 AFIX 0 C267 1 0.277705 0.416104 0.583755 11.00000 0.05187 0.04340 = 0.03091 0.00531 -0.02188 0.00544 C107 1 0.807742 0.339525 0.971267 11.00000 0.03144 0.04094 = 0.06919 0.01096 0.00769 -0.00227 C74 1 0.229634 0.777078 0.759150 11.00000 0.04537 0.06640 = 0.06581 0.01620 -0.00225 0.01852 AFIX 43 H74 2 0.210463 0.804995 0.744851 11.00000 -1.20000 AFIX 0 C19 1 0.912019 0.600751 0.766939 11.00000 0.04867 0.06903 = 0.04922 0.01124 0.02321 0.00085 C34 1 0.821715 0.501895 0.700064 11.00000 0.02071 0.08068 = 0.04042 0.01069 -0.00372 0.00069 C275 1 0.420072 0.413919 0.588219 11.00000 0.04528 0.07452 = 0.05786 0.00002 -0.01484 0.00311 AFIX 43 H275 2 0.468140 0.427296 0.579027 11.00000 -1.20000 AFIX 0 C37 1 0.979665 0.488048 0.737895 11.00000 0.03235 0.08786 = 0.06882 0.01830 -0.01105 -0.00475 AFIX 43 H37 2 0.971309 0.505018 0.712660 11.00000 -1.20000 AFIX 0 C42 1 0.859372 0.425098 0.816703 11.00000 0.03813 0.06061 = 0.04316 0.00509 -0.00808 0.01632 AFIX 43 H42 2 0.866396 0.410841 0.843210 11.00000 -1.20000 AFIX 0 C43 1 0.781731 0.426336 0.798598 11.00000 0.02153 0.05972 = 0.03388 0.00421 0.01076 0.00208 AFIX 43 H43 2 0.738523 0.412078 0.812202 11.00000 -1.20000 AFIX 0 C44 1 0.771070 0.449654 0.759434 11.00000 0.02172 0.04867 = 0.04391 -0.00891 -0.00355 -0.00072 C124 1 0.623917 0.331167 1.013665 11.00000 0.05174 0.05576 = 0.04030 -0.00355 -0.00486 -0.00583 C24 1 0.959120 0.627694 0.739600 11.00000 0.04743 0.13718 = 0.07396 -0.00913 0.01582 -0.04961 AFIX 43 H24 2 0.936077 0.638968 0.714404 11.00000 -1.20000 AFIX 0 C259 1 0.046674 0.483640 0.558890 11.00000 0.04150 0.10561 = 0.02636 0.01384 0.00925 0.01943 AFIX 43 H259 2 -0.002876 0.498546 0.553276 11.00000 -1.20000 AFIX 0 C106 1 0.823789 0.321970 0.881824 11.00000 0.04130 0.06318 = 0.03600 0.01198 0.00820 0.00252 C75 1 0.255172 0.781841 0.799865 11.00000 0.05461 0.04039 = 0.05047 0.00219 0.00490 0.00484 AFIX 43 H75 2 0.250501 0.812214 0.813587 11.00000 -1.20000 AFIX 0 C71 1 0.263543 0.643520 0.742680 11.00000 0.05912 0.05882 = 0.04663 0.00479 -0.00139 -0.00858 AFIX 43 H71 2 0.240162 0.639568 0.716005 11.00000 -1.20000 AFIX 0 C178 1 0.470948 0.500935 0.269855 11.00000 0.02892 0.03840 = 0.07010 0.00642 0.00160 -0.00229 C77 1 0.290401 0.694562 0.801259 11.00000 0.02353 0.03375 = 0.06655 0.00982 0.00047 -0.00645 C258 1 0.074069 0.447725 0.532231 11.00000 0.03061 0.04946 = 0.06151 0.00157 -0.01350 -0.00914 AFIX 43 H258 2 0.042436 0.438095 0.509114 11.00000 -1.20000 AFIX 0 C157 1 0.436665 0.626037 0.292246 11.00000 0.05942 0.04787 = 0.07156 0.00322 0.00690 0.02014 C188 1 0.439951 0.471526 0.341653 11.00000 0.02820 0.04872 = 0.05466 -0.01400 0.00008 0.00272 C265 1 0.167731 0.477357 0.602315 11.00000 0.04187 0.04293 = 0.04858 0.00413 0.00812 -0.00196 C274 1 0.426379 0.376755 0.614795 11.00000 0.05395 0.05114 = 0.10173 0.00772 -0.00540 0.00308 AFIX 43 H274 2 0.476362 0.365092 0.624071 11.00000 -1.20000 AFIX 0 C263 1 0.182302 0.527797 0.665147 11.00000 0.05961 0.11546 = 0.05265 -0.00550 -0.02901 -0.00343 AFIX 43 H263 2 0.210997 0.536878 0.689426 11.00000 -1.20000 AFIX 0 C190 1 0.301389 0.434023 0.250117 11.00000 0.06308 0.05798 = 0.04830 0.01010 0.01248 0.00559 AFIX 43 H190 2 0.272574 0.459802 0.262141 11.00000 -1.20000 AFIX 0 C266 1 0.197483 0.439552 0.574093 11.00000 0.04258 0.04286 = 0.04358 0.00438 -0.00895 -0.00790 C51 1 0.643281 0.381136 0.736278 11.00000 0.03567 0.07895 = 0.05837 -0.00295 0.01236 0.01218 C41 1 0.926688 0.444257 0.796834 11.00000 0.02104 0.05366 = 0.05915 0.00178 -0.00356 -0.00385 C8 1 0.620231 0.528908 1.083649 11.00000 0.06028 0.06575 = 0.05265 -0.00260 0.00530 0.00241 C20 1 0.947741 0.584671 0.804256 11.00000 0.04936 0.09194 = 0.06356 0.01147 0.03340 -0.00458 AFIX 43 H20 2 0.918034 0.565393 0.822571 11.00000 -1.20000 AFIX 0 C145 1 0.129801 0.768685 0.325334 11.00000 0.05346 0.04485 = 0.10936 0.01153 -0.00352 0.01878 C3 1 0.767953 0.677617 0.955241 11.00000 0.05006 0.05029 = 0.06426 -0.01125 -0.01433 -0.00355 C7 1 0.623028 0.521263 1.038876 11.00000 0.07835 0.07259 = 0.01600 0.00533 0.00754 -0.00806 C6 1 0.555525 0.529718 1.014383 11.00000 0.06270 0.03608 = 0.06124 -0.00555 0.02872 0.00254 C61 1 0.284312 0.430279 0.757711 11.00000 0.08608 0.06189 = 0.10515 -0.00432 -0.00005 -0.02836 AFIX 43 H61 2 0.244994 0.405782 0.759046 11.00000 -1.20000 AFIX 0 C65 1 0.282764 0.513546 0.942764 11.00000 0.07520 0.08295 = 0.07420 0.01302 0.00744 -0.00179 AFIX 43 H65 2 0.305417 0.503032 0.968289 11.00000 -1.20000 AFIX 0 C63 1 0.300972 0.536712 0.872017 11.00000 0.03045 0.04909 = 0.05998 -0.01339 0.00490 0.00810 C277 1 0.347741 0.541201 0.574345 11.00000 0.03954 0.05540 = 0.03995 0.00480 -0.00050 -0.00126 C273 1 0.353259 0.354728 0.629047 11.00000 0.07161 0.04125 = 0.06090 0.00901 -0.00848 0.00942 C87 1 0.453904 0.654269 0.924424 11.00000 0.04163 0.07930 = 0.04103 -0.00674 -0.01009 -0.00854 AFIX 43 H87 2 0.507955 0.654581 0.932603 11.00000 -1.20000 AFIX 0 C57 1 0.348833 0.501780 0.788342 11.00000 0.02423 0.03816 = 0.04285 -0.00431 -0.01009 -0.00140 C99 1 0.648728 0.732734 0.869292 11.00000 0.03379 0.07027 = 0.07487 -0.01180 -0.01835 -0.00120 AFIX 43 H99 2 0.678698 0.711989 0.852268 11.00000 -1.20000 AFIX 0 C129 1 0.602180 0.370859 1.039866 11.00000 0.04182 0.06829 = 0.03947 0.00340 0.01182 -0.01946 C26 1 0.818575 0.580132 0.663368 11.00000 0.05789 0.06282 = 0.06112 0.01035 -0.00256 -0.00201 AFIX 43 H26 2 0.821088 0.614672 0.663869 11.00000 -1.20000 AFIX 0 C1 1 0.880397 0.727244 0.930263 11.00000 0.04512 0.07497 = 0.10184 -0.02509 -0.01724 -0.01304 C177 1 0.517381 0.466927 0.243909 11.00000 0.05067 0.05454 = 0.04502 0.00248 0.01275 -0.00521 C108 1 0.815770 0.381704 0.995808 11.00000 0.09857 0.06616 = 0.04419 -0.01449 0.02987 -0.01146 AFIX 43 H108 2 0.792524 0.411211 0.986308 11.00000 -1.20000 AFIX 0 C239 1 0.059761 0.342570 0.331785 11.00000 0.03318 0.07485 = 0.03772 0.00175 -0.01744 -0.00737 C164 1 0.300342 0.657715 0.230985 11.00000 0.07290 0.06841 = 0.05190 0.01444 -0.00683 0.00833 AFIX 43 H164 2 0.341100 0.677412 0.242613 11.00000 -1.20000 AFIX 0 C112 1 0.851080 0.296563 0.986518 11.00000 0.05825 0.06567 = 0.06260 0.00849 -0.01039 0.00696 AFIX 43 H112 2 0.846706 0.266888 0.971610 11.00000 -1.20000 AFIX 0 C25 1 0.815488 0.553535 0.700966 11.00000 0.04002 0.05484 = 0.04742 0.01297 0.00357 -0.00099 C162 1 0.490659 0.641295 0.262110 11.00000 0.05442 0.04775 = 0.06810 0.03192 -0.00811 -0.01389 AFIX 43 H162 2 0.488607 0.628008 0.235074 11.00000 -1.20000 AFIX 0 C111 1 0.898690 0.298076 1.022420 11.00000 0.07690 0.08540 = 0.08327 0.00650 -0.00003 0.01049 AFIX 43 H111 2 0.929402 0.270704 1.030643 11.00000 -1.20000 AFIX 0 C169 1 0.418953 0.534488 0.250129 11.00000 0.04081 0.04545 = 0.07167 -0.00275 -0.01598 0.01128 C133 1 0.489993 0.313416 0.876883 11.00000 0.06446 0.05747 = 0.05586 -0.00535 0.00415 0.00712 C10 1 0.953578 0.519519 0.989688 11.00000 0.07994 0.09296 = 0.04370 -0.01510 -0.01026 0.00785 C194 1 0.396125 0.366548 0.253424 11.00000 0.04148 0.04023 = 0.05478 -0.00096 0.01061 0.00628 AFIX 43 H194 2 0.432710 0.347976 0.269468 11.00000 -1.20000 AFIX 0 C168 1 0.231390 0.579448 0.228400 11.00000 0.05387 0.06090 = 0.08536 0.03208 -0.00188 -0.00472 AFIX 43 H168 2 0.224965 0.546647 0.236959 11.00000 -1.20000 AFIX 0 N6 5 1.024340 0.401838 0.965934 11.00000 0.07016 0.15005 = 0.05103 0.02101 0.01276 0.01937 C260 1 0.092283 0.498370 0.594654 11.00000 0.04716 0.06765 = 0.03154 0.01085 0.00850 -0.01032 C101 1 0.797655 0.310482 0.843343 11.00000 0.04681 0.05119 = 0.06238 -0.00478 0.01355 0.00644 AFIX 43 H101 2 0.742776 0.308235 0.837357 11.00000 -1.20000 AFIX 0 C195 1 0.409606 0.367214 0.352724 11.00000 0.06260 0.07498 = 0.03850 0.00939 0.00375 0.01785 C121 1 0.565812 0.240760 0.947628 11.00000 0.05853 0.05068 = 0.04285 0.01644 -0.01252 -0.00658 C81 1 0.210441 0.657357 0.890857 11.00000 0.02995 0.08183 = 0.05170 -0.00978 -0.00357 -0.00949 AFIX 43 H81 2 0.193102 0.655048 0.862876 11.00000 -1.20000 AFIX 0 C115 1 0.669323 0.199351 0.906891 11.00000 0.10564 0.03159 = 0.04031 0.00360 0.00384 0.00553 AFIX 43 H115 2 0.687720 0.171467 0.892727 11.00000 -1.20000 AFIX 0 C171 1 0.450609 0.501087 0.181533 11.00000 0.04832 0.08032 = 0.06314 0.01233 0.00549 -0.00239 AFIX 43 H171 2 0.444222 0.502151 0.152380 11.00000 -1.20000 AFIX 0 C86 1 0.400909 0.649770 0.952996 11.00000 0.06817 0.07388 = 0.06645 -0.01836 -0.03088 -0.00025 AFIX 43 H86 2 0.417417 0.644226 0.980777 11.00000 -1.20000 AFIX 0 C113 1 0.688526 0.285169 0.924154 11.00000 0.04234 0.04780 = 0.07748 -0.00275 -0.01190 0.01433 C264 1 0.211896 0.491767 0.639320 11.00000 0.03322 0.08493 = 0.07477 -0.01074 -0.00831 -0.01244 AFIX 43 H264 2 0.260887 0.476671 0.645928 11.00000 -1.20000 AFIX 0 C232 1 -0.056749 0.402141 0.287382 11.00000 0.03825 0.05002 = 0.06175 -0.02041 0.01160 -0.01344 C203 1 0.073197 0.457651 0.197682 11.00000 0.04049 0.08036 = 0.11176 -0.02800 -0.00463 0.00795 AFIX 43 H203 2 0.104528 0.429157 0.195591 11.00000 -1.20000 AFIX 0 C70 1 0.292999 0.603257 0.760117 11.00000 0.01952 0.05644 = 0.05932 0.00681 -0.00379 0.00200 AFIX 43 H70 2 0.294450 0.573548 0.745172 11.00000 -1.20000 AFIX 0 C154 1 0.314574 0.711698 0.500621 11.00000 0.04501 0.04087 = 0.09910 -0.01395 0.02120 0.00629 C58 1 0.400042 0.499920 0.754257 11.00000 0.03577 0.05638 = 0.03144 0.00682 -0.01251 0.00386 AFIX 43 H58 2 0.440037 0.524029 0.753299 11.00000 -1.20000 AFIX 0 C208 1 0.021732 0.647272 0.272676 11.00000 0.06695 0.07028 = 0.07636 0.00056 -0.01578 -0.00266 AFIX 43 H208 2 0.075548 0.638215 0.271173 11.00000 -1.20000 AFIX 0 C130 1 0.545813 0.404897 1.027368 11.00000 0.05623 0.06813 = 0.04671 -0.01558 0.00947 -0.00911 AFIX 43 H130 2 0.528937 0.429247 1.045978 11.00000 -1.20000 AFIX 0 C225 1 -0.201508 0.483326 0.229622 11.00000 0.07709 0.09520 = 0.02945 0.00589 -0.00592 -0.01374 AFIX 43 H225 2 -0.213058 0.506532 0.250328 11.00000 -1.20000 AFIX 0 C90 1 0.464114 0.676784 0.722315 11.00000 0.06401 0.06665 = 0.04146 -0.00555 0.00109 0.00129 AFIX 43 H90 2 0.460536 0.654075 0.700270 11.00000 -1.20000 AFIX 0 C155 1 0.376665 0.681604 0.489594 11.00000 0.05313 0.04253 = 0.08699 -0.01340 -0.00325 -0.00141 C161 1 0.548105 0.677085 0.273424 11.00000 0.06817 0.04513 = 0.15272 -0.00802 0.02076 -0.00202 AFIX 43 H161 2 0.583783 0.688099 0.253334 11.00000 -1.20000 AFIX 0 C151 1 0.009670 0.606992 0.516746 11.00000 0.03918 0.05415 = 0.06246 -0.00235 0.01295 0.00963 C38 1 1.056156 0.483442 0.752280 11.00000 0.02945 0.09737 = 0.07604 0.01818 0.00102 -0.01140 AFIX 43 H38 2 1.098980 0.495094 0.736767 11.00000 -1.20000 AFIX 0 C147 1 0.068319 0.705991 0.376647 11.00000 0.04153 0.03336 = 0.10622 -0.00929 -0.00755 0.00435 C146 1 0.132392 0.721290 0.349587 11.00000 0.06642 0.05927 = 0.05324 0.00561 0.00516 -0.00431 C14 1 0.765494 0.680456 0.769369 11.00000 0.08789 0.08488 = 0.07833 0.00266 0.00389 0.00075 AFIX 43 H14 2 0.804443 0.677763 0.790736 11.00000 -1.20000 AFIX 0 C186 1 0.489545 0.516001 0.404026 11.00000 0.05945 0.07420 = 0.04379 -0.00058 0.00839 0.00414 AFIX 43 H186 2 0.486858 0.522447 0.432725 11.00000 -1.20000 AFIX 0 C187 1 0.444133 0.480893 0.387250 11.00000 0.05130 0.03718 = 0.04720 0.00519 0.01276 -0.01137 AFIX 43 H187 2 0.413520 0.461255 0.404871 11.00000 -1.20000 AFIX 0 C230 1 -0.075178 0.373591 0.216557 11.00000 0.07796 0.07391 = 0.03993 -0.01115 -0.01466 0.00403 AFIX 43 H230 2 -0.063067 0.350953 0.195501 11.00000 -1.20000 AFIX 0 C228 1 -0.164718 0.418087 0.165138 11.00000 0.07114 0.07344 = 0.09112 -0.00040 -0.01354 -0.03072 AFIX 43 H228 2 -0.152338 0.396230 0.143547 11.00000 -1.20000 AFIX 0 C150 1 -0.027764 0.574003 0.489009 11.00000 0.03324 0.04740 = 0.06417 0.01625 0.01651 -0.00226 C62 1 0.287977 0.466410 0.788902 11.00000 0.05303 0.04887 = 0.06898 -0.01217 -0.00298 0.00989 AFIX 43 H62 2 0.250082 0.466939 0.809965 11.00000 -1.20000 AFIX 0 C200 1 0.494145 0.362799 0.363990 11.00000 0.08156 0.05024 = 0.10131 0.03264 0.03187 0.01930 AFIX 43 H200 2 0.528038 0.390025 0.361094 11.00000 -1.20000 AFIX 0 C170 1 0.411381 0.533090 0.204909 11.00000 0.06616 0.07340 = 0.02027 0.00800 0.02397 0.01002 AFIX 43 H170 2 0.377236 0.555811 0.191543 11.00000 -1.20000 AFIX 0 C160 1 0.553251 0.696248 0.313021 11.00000 0.03781 0.04915 = 0.16748 -0.00380 -0.01688 -0.00635 AFIX 43 H160 2 0.594012 0.718538 0.320281 11.00000 -1.20000 AFIX 0 C176 1 0.571632 0.432108 0.260086 11.00000 0.02644 0.08572 = 0.05426 -0.00185 0.00762 0.01669 AFIX 43 H176 2 0.581315 0.432258 0.289042 11.00000 -1.20000 AFIX 0 C104 1 0.958982 0.316813 0.858856 11.00000 0.05210 0.08679 = 0.10119 0.02143 0.02819 0.01740 AFIX 43 H104 2 1.013978 0.320344 0.863931 11.00000 -1.20000 AFIX 0 C109 1 0.857475 0.381478 1.034251 11.00000 0.08025 0.10016 = 0.05560 0.00343 0.00260 0.00991 AFIX 43 H109 2 0.856561 0.408961 1.052001 11.00000 -1.20000 AFIX 0 C27 1 0.817894 0.555031 0.625202 11.00000 0.06029 0.07991 = 0.06494 0.00650 0.00135 -0.00181 AFIX 43 H27 2 0.812653 0.573274 0.600416 11.00000 -1.20000 AFIX 0 C64 1 0.334259 0.525301 0.909552 11.00000 0.03222 0.08652 = 0.05057 0.02152 -0.00569 -0.01152 AFIX 43 H64 2 0.389809 0.525128 0.913621 11.00000 -1.20000 AFIX 0 C283 1 0.457997 0.492617 0.520153 11.00000 0.02953 0.11481 = 0.03565 0.00555 -0.01049 0.00185 C152 1 -0.034274 0.631886 0.545455 11.00000 0.05106 0.06313 = 0.05585 -0.00035 0.01674 0.01091 C110 1 0.899827 0.339757 1.045216 11.00000 0.07882 0.08367 = 0.07856 0.00419 -0.00076 0.00538 AFIX 43 H110 2 0.931104 0.340430 1.069866 11.00000 -1.20000 AFIX 0 C199 1 0.524215 0.318854 0.378830 11.00000 0.08612 0.09275 = 0.08874 0.00742 0.00396 0.00627 AFIX 43 H199 2 0.579538 0.314814 0.382097 11.00000 -1.20000 AFIX 0 C179 1 0.485763 0.499668 0.316701 11.00000 0.05501 0.06731 = 0.02677 0.01229 0.01333 0.01864 C281 1 0.292156 0.620744 0.592277 11.00000 0.06806 0.07656 = 0.08061 -0.01399 -0.02557 -0.00323 AFIX 43 H281 2 0.259111 0.647512 0.585217 11.00000 -1.20000 AFIX 0 C85 1 0.319095 0.653081 0.942938 11.00000 0.07106 0.05354 = 0.02290 0.00853 0.00711 0.00478 C139 1 0.375596 0.374937 0.917172 11.00000 0.04078 0.04092 = 0.09172 0.00612 0.00459 -0.00889 C175 1 0.611672 0.397889 0.237116 11.00000 0.03995 0.07754 = 0.07691 0.00562 0.00573 0.00602 AFIX 43 H175 2 0.649096 0.376627 0.249794 11.00000 -1.20000 AFIX 0 C269 1 0.205602 0.356816 0.631107 11.00000 0.06097 0.07394 = 0.07730 0.03289 -0.01078 -0.00998 AFIX 43 H269 2 0.156137 0.369951 0.622566 11.00000 -1.20000 AFIX 0 C76 1 0.287361 0.742356 0.820365 11.00000 0.03481 0.05613 = 0.06003 -0.01941 -0.00812 0.00640 AFIX 43 H76 2 0.308025 0.746484 0.847601 11.00000 -1.20000 AFIX 0 C33 1 0.832185 0.479230 0.661019 11.00000 0.03248 0.09429 = 0.05924 0.01299 -0.00378 -0.01071 C159 1 0.498209 0.682553 0.342032 11.00000 0.06265 0.07109 = 0.09083 -0.00341 -0.02697 -0.03210 AFIX 43 H159 2 0.497990 0.696878 0.368678 11.00000 -1.20000 AFIX 0 N10 5 -0.066999 0.650744 0.574149 11.00000 0.09305 0.08941 = 0.12924 -0.02024 0.05299 0.00833 C229 1 -0.127898 0.412007 0.205812 11.00000 0.06909 0.07001 = 0.06071 0.00093 -0.00727 -0.00858 C246 1 0.082384 0.306457 0.461160 11.00000 0.08256 0.07154 = 0.03149 0.01273 -0.00992 -0.01870 AFIX 43 H246 2 0.118569 0.310134 0.439498 11.00000 -1.20000 AFIX 0 C261 1 0.064678 0.535257 0.620947 11.00000 0.04246 0.06655 = 0.09522 -0.00837 0.02068 0.01144 AFIX 43 H261 2 0.014878 0.549886 0.615424 11.00000 -1.20000 AFIX 0 C89 1 0.488999 0.659807 0.763271 11.00000 0.05395 0.04277 = 0.05281 -0.01242 0.02624 -0.00262 AFIX 43 H89 2 0.504741 0.627021 0.767790 11.00000 -1.20000 AFIX 0 C120 1 0.495418 0.239078 0.971088 11.00000 0.06237 0.04123 = 0.08020 0.01678 0.01828 -0.00415 AFIX 43 H120 2 0.482195 0.265856 0.988107 11.00000 -1.20000 AFIX 0 C204 1 0.035447 0.478670 0.163553 11.00000 0.06696 0.09095 = 0.05875 0.01005 0.00091 -0.02642 AFIX 43 H204 2 0.047685 0.466265 0.137135 11.00000 -1.20000 AFIX 0 N9 5 -0.184191 0.563608 0.493584 11.00000 0.03970 0.13373 = 0.11200 0.00719 0.02417 -0.02260 C128 1 0.643625 0.375854 1.081640 11.00000 0.05829 0.08680 = 0.06957 -0.01961 0.01912 -0.01524 AFIX 43 H128 2 0.635392 0.403684 1.098373 11.00000 -1.20000 AFIX 0 C13 1 0.756545 0.641337 0.741294 11.00000 0.07275 0.06876 = 0.06740 0.01705 0.00630 -0.00773 C278 1 0.394469 0.539875 0.611720 11.00000 0.03891 0.07330 = 0.03431 0.00162 -0.00640 -0.00233 AFIX 43 H278 2 0.428298 0.513101 0.617582 11.00000 -1.20000 AFIX 0 C184 1 0.594917 0.579801 0.395300 11.00000 0.08933 0.05613 = 0.06305 -0.00505 -0.03296 -0.00927 AFIX 43 H184 2 0.592201 0.588754 0.423512 11.00000 -1.20000 AFIX 0 C198 1 0.474530 0.281030 0.388868 11.00000 0.08831 0.07655 = 0.08132 0.00341 0.00303 0.00514 AFIX 43 H198 2 0.495783 0.251974 0.400451 11.00000 -1.20000 AFIX 0 C84 1 0.258900 0.654212 0.974834 11.00000 0.06223 0.07162 = 0.06273 -0.01764 0.00380 -0.01428 AFIX 43 H84 2 0.274880 0.652202 1.003038 11.00000 -1.20000 AFIX 0 C134 1 0.554155 0.308248 0.850016 11.00000 0.05925 0.07315 = 0.06726 -0.00666 0.00869 0.01537 AFIX 43 H134 2 0.592429 0.333409 0.849124 11.00000 -1.20000 AFIX 0 C123 1 0.587701 0.328075 0.973125 11.00000 0.05287 0.07632 = 0.03495 -0.00150 0.01640 -0.02231 C32 1 0.845571 0.428721 0.655155 11.00000 0.06762 0.07384 = 0.06452 -0.00785 0.00362 -0.00160 AFIX 43 H32 2 0.854031 0.410327 0.679654 11.00000 -1.20000 AFIX 0 C12 1 1.001352 0.442043 0.963101 11.00000 0.04095 0.07455 = 0.09146 0.02598 -0.01397 0.01545 C197 1 0.391063 0.285332 0.381918 11.00000 0.08627 0.08079 = 0.07694 0.00437 0.00667 0.00170 AFIX 43 H197 2 0.357151 0.258897 0.387908 11.00000 -1.20000 AFIX 0 C172 1 0.502162 0.465244 0.200226 11.00000 0.04938 0.06078 = 0.07994 0.01037 0.03542 0.00722 C141 1 0.257189 0.356291 0.955024 11.00000 0.09030 0.09929 = 0.09976 0.00076 0.01308 -0.00538 AFIX 43 H141 2 0.233041 0.342702 0.978498 11.00000 -1.20000 AFIX 0 N7 5 0.125172 0.802303 0.306764 11.00000 0.06997 0.07773 = 0.14841 0.04942 -0.00038 0.01350 C282 1 0.297766 0.580119 0.566769 11.00000 0.06100 0.07464 = 0.07173 -0.00058 0.01569 0.02408 AFIX 43 H282 2 0.265143 0.579085 0.542602 11.00000 -1.20000 AFIX 0 N8 5 -0.052716 0.762301 0.378196 11.00000 0.10032 0.11951 = 0.11980 -0.00090 -0.01178 0.05377 C29 1 0.826333 0.481000 0.583358 11.00000 0.04547 0.14905 = 0.05058 0.00404 -0.00089 -0.00771 AFIX 43 H29 2 0.818950 0.499554 0.558864 11.00000 -1.20000 AFIX 0 N12 5 0.496885 0.668829 0.540301 11.00000 0.07465 0.13859 = 0.06741 -0.01682 -0.03156 0.00010 C255 1 0.390965 0.319410 0.493705 11.00000 0.07644 0.09262 = 0.08898 -0.00864 -0.00138 0.00401 AFIX 43 H255 2 0.438662 0.324149 0.479540 11.00000 -1.20000 AFIX 0 C103 1 0.932467 0.303244 0.819630 11.00000 0.06314 0.07819 = 0.09777 -0.01037 0.03135 0.01444 AFIX 43 H103 2 0.968983 0.295216 0.798970 11.00000 -1.20000 AFIX 0 C288 1 0.502031 0.537627 0.522948 11.00000 0.03303 0.11532 = 0.04780 -0.00508 0.00618 -0.01961 AFIX 43 H288 2 0.476603 0.565941 0.532894 11.00000 -1.20000 AFIX 0 C36 1 0.911240 0.469292 0.757902 11.00000 0.03355 0.04798 = 0.05155 0.01357 -0.01371 -0.00397 C102 1 0.854118 0.301593 0.811188 11.00000 0.10054 0.06420 = 0.08621 -0.00388 0.02473 0.00253 AFIX 43 H102 2 0.835799 0.294547 0.783950 11.00000 -1.20000 AFIX 0 C105 1 0.907877 0.325395 0.890904 11.00000 0.04269 0.08585 = 0.07017 0.01223 0.00957 0.00791 AFIX 43 H105 2 0.927198 0.333227 0.917806 11.00000 -1.20000 AFIX 66 C49 1 0.620732 0.475555 0.619715 11.00000 0.06734 0.09426 = 0.06516 0.00083 -0.00533 -0.01156 AFIX 43 H49 2 0.622225 0.459211 0.593942 11.00000 -1.20000 AFIX 65 C48 1 0.599515 0.525499 0.621266 11.00000 0.06894 0.09572 = 0.07862 0.01262 -0.00547 -0.00993 AFIX 43 H48 2 0.586811 0.542571 0.596531 11.00000 -1.20000 AFIX 65 C47 1 0.597284 0.549927 0.659785 11.00000 0.08345 0.08875 = 0.08944 0.01564 0.00269 0.00072 AFIX 43 H47 2 0.583088 0.583343 0.660823 11.00000 -1.20000 AFIX 65 C46 1 0.616270 0.524411 0.696754 11.00000 0.08191 0.08617 = 0.08486 0.00855 -0.00055 0.00024 AFIX 43 H46 2 0.614778 0.540756 0.722526 11.00000 -1.20000 AFIX 65 C45 1 0.637488 0.474468 0.695204 11.00000 0.05652 0.07107 = 0.06571 -0.00376 0.00706 -0.01083 C50 1 0.639719 0.450039 0.656684 11.00000 0.06225 0.08694 = 0.06213 -0.00233 -0.00148 -0.00052 AFIX 43 H50 2 0.653916 0.416623 0.655647 11.00000 -1.20000 AFIX 0 C183 1 0.650185 0.601958 0.370825 11.00000 0.07450 0.07600 = 0.08329 0.00359 -0.00872 -0.00409 AFIX 43 H183 2 0.685166 0.625461 0.382473 11.00000 -1.20000 AFIX 0 C40 1 1.004741 0.441444 0.814744 11.00000 0.02345 0.07907 = 0.05929 0.00508 -0.01317 0.00227 AFIX 43 H40 2 1.013268 0.427398 0.841229 11.00000 -1.20000 AFIX 0 C4 1 0.755595 0.712143 0.989424 11.00000 0.12797 0.12703 = 0.12852 -0.01026 0.00140 -0.00584 C222 1 -0.124210 0.476881 0.314252 11.00000 0.00992 0.10484 = 0.05521 0.01589 -0.00399 0.01361 C207 1 -0.033283 0.610693 0.282991 11.00000 0.09482 0.09625 = 0.09581 -0.00003 0.00451 -0.00205 C156 1 0.442156 0.676392 0.516822 11.00000 0.05783 0.06487 = 0.07366 -0.01114 -0.00142 0.00058 C193 1 0.384234 0.354486 0.214977 11.00000 0.08010 0.06188 = 0.04378 -0.02410 0.02092 0.01523 AFIX 43 H193 2 0.410742 0.327147 0.203954 11.00000 -1.20000 AFIX 0 C181 1 0.600655 0.559933 0.310332 11.00000 0.05651 0.04013 = 0.08434 0.01359 0.00433 -0.00443 AFIX 43 H181 2 0.599873 0.555641 0.281272 11.00000 -1.20000 AFIX 0 C196 1 0.362208 0.326300 0.367170 11.00000 0.07424 0.07193 = 0.06305 0.00705 -0.01354 -0.00528 AFIX 43 H196 2 0.306565 0.329666 0.365760 11.00000 -1.20000 AFIX 0 C140 1 0.339538 0.355496 0.951407 11.00000 0.05191 0.06826 = 0.06502 0.01140 0.01683 -0.01220 AFIX 43 H140 2 0.371072 0.341378 0.972814 11.00000 -1.20000 AFIX 0 C18 1 0.695311 0.648656 0.711293 11.00000 0.07314 0.07689 = 0.07719 0.01380 0.00285 -0.00039 AFIX 43 H18 2 0.681176 0.621256 0.694863 11.00000 -1.20000 AFIX 0 C82 1 0.153532 0.661462 0.920818 11.00000 0.04660 0.08731 = 0.07441 -0.02919 0.02079 0.00083 AFIX 43 H82 2 0.099665 0.666247 0.913406 11.00000 -1.20000 AFIX 0 C205 1 -0.017688 0.515666 0.165186 11.00000 0.06287 0.11488 = 0.02909 0.01304 -0.00366 -0.00360 AFIX 43 H205 2 -0.047491 0.526076 0.141664 11.00000 -1.20000 AFIX 0 C16 1 0.664544 0.728293 0.733975 11.00000 0.06393 0.07193 = 0.10837 0.00635 0.00303 -0.01394 AFIX 43 H16 2 0.633911 0.757176 0.732195 11.00000 -1.20000 AFIX 0 C67 1 0.169147 0.524735 0.900348 11.00000 0.05193 0.06608 = 0.07267 0.00487 0.01318 -0.00821 AFIX 43 H67 2 0.113610 0.522622 0.896715 11.00000 -1.20000 AFIX 0 C80 1 0.292047 0.656406 0.899359 11.00000 0.02993 0.04699 = 0.05973 -0.01304 -0.00905 -0.00850 C17 1 0.652839 0.692336 0.703099 11.00000 0.07364 0.08303 = 0.08668 0.00622 0.00343 0.00752 AFIX 43 H17 2 0.619951 0.696951 0.679337 11.00000 -1.20000 AFIX 0 C126 1 0.706628 0.299189 1.071042 11.00000 0.08576 0.05398 = 0.04157 0.01018 -0.00255 -0.00480 AFIX 43 H126 2 0.737706 0.273303 1.082013 11.00000 -1.20000 AFIX 0 C244 1 0.127972 0.348105 0.305023 11.00000 0.06267 0.06937 = 0.06475 -0.00341 -0.00881 0.00196 AFIX 43 H244 2 0.138681 0.379393 0.294019 11.00000 -1.20000 AFIX 0 C148 1 -0.000385 0.739923 0.373686 11.00000 0.09159 0.09011 = 0.04518 0.00504 0.00797 0.03529 C242 1 0.166800 0.264089 0.317642 11.00000 0.07883 0.08182 = 0.09476 -0.00081 0.00477 0.01210 AFIX 43 H242 2 0.201042 0.237566 0.312446 11.00000 -1.20000 AFIX 0 C253 1 0.324363 0.270072 0.542164 11.00000 0.08975 0.07956 = 0.08218 0.00271 -0.00175 0.00248 AFIX 43 H253 2 0.324966 0.243224 0.560620 11.00000 -1.20000 AFIX 0 C252 1 0.255286 0.302400 0.536801 11.00000 0.07647 0.07388 = 0.07045 -0.00348 -0.00278 0.00860 AFIX 43 H252 2 0.209697 0.296207 0.552369 11.00000 -1.20000 AFIX 0 C55 1 0.544212 0.315281 0.727374 11.00000 0.06973 0.08219 = 0.07830 -0.01143 -0.01302 -0.00486 AFIX 43 H55 2 0.490905 0.304832 0.727100 11.00000 -1.20000 AFIX 0 C268 1 0.276948 0.375319 0.615420 11.00000 0.05447 0.05449 = 0.05834 -0.00165 0.00028 -0.00442 C173 1 0.541117 0.426592 0.175527 11.00000 0.07660 0.10020 = 0.04155 -0.01503 0.02118 0.02335 AFIX 43 H173 2 0.528797 0.423303 0.146951 11.00000 -1.20000 AFIX 0 C248 1 -0.026497 0.265579 0.492721 11.00000 0.09439 0.08874 = 0.08707 0.03339 -0.00763 -0.03844 AFIX 43 H248 2 -0.062843 0.239298 0.492406 11.00000 -1.20000 AFIX 0 C224 1 -0.148555 0.446054 0.239249 11.00000 0.03973 0.08992 = 0.07431 -0.00251 -0.00951 -0.00953 C153 1 0.311901 0.730174 0.542042 11.00000 0.06388 0.07345 = 0.06319 -0.00903 0.00078 0.00149 C234 1 -0.076322 0.399318 0.416126 11.00000 0.09186 0.09382 = 0.09560 0.00539 0.00070 0.00860 AFIX 43 H234 2 -0.042198 0.426008 0.421780 11.00000 -1.20000 AFIX 0 C233 1 -0.073449 0.376889 0.376862 11.00000 0.06800 0.06653 = 0.06490 0.00859 0.00943 0.00249 C215 1 -0.166319 0.539302 0.379414 11.00000 0.05781 0.14103 = 0.06820 -0.01976 -0.02593 0.02363 AFIX 43 H215 2 -0.179450 0.560712 0.401193 11.00000 -1.20000 AFIX 0 C249 1 -0.024598 0.296009 0.526387 11.00000 0.10844 0.11346 = 0.08307 -0.00646 0.06087 -0.03568 AFIX 43 H249 2 -0.063750 0.294245 0.546760 11.00000 -1.20000 AFIX 0 C23 1 1.039431 0.638455 0.748469 11.00000 0.06167 0.11606 = 0.09877 0.00528 -0.00683 -0.04379 AFIX 43 H23 2 1.070952 0.654379 0.728779 11.00000 -1.20000 AFIX 0 C251 1 0.255006 0.343852 0.508100 11.00000 0.09302 0.04850 = 0.04886 -0.00644 -0.00022 0.00328 C95 1 0.522413 0.761943 0.893708 11.00000 0.04683 0.06826 = 0.07859 -0.03806 0.00618 -0.00830 AFIX 43 H95 2 0.466653 0.759346 0.893506 11.00000 -1.20000 AFIX 0 C240 1 0.056924 0.296187 0.350729 11.00000 0.10067 0.10019 = 0.10184 -0.00015 0.01939 0.00423 AFIX 43 H240 2 0.014341 0.290725 0.368614 11.00000 -1.20000 AFIX 0 C116 1 0.592243 0.198502 0.927823 11.00000 0.08026 0.04126 = 0.04483 0.00634 -0.00717 -0.00850 C256 1 0.331750 0.351417 0.487124 11.00000 0.03256 0.09058 = 0.08501 0.00191 0.01075 0.00147 AFIX 43 H256 2 0.338622 0.378498 0.469361 11.00000 -1.20000 AFIX 0 C213 1 -0.086287 0.524293 0.318530 11.00000 0.06112 0.05633 = 0.05852 0.00027 -0.00835 0.00366 C262 1 0.110572 0.550531 0.655368 11.00000 0.03552 0.09646 = 0.06343 -0.01480 0.01857 0.01004 AFIX 43 H262 2 0.092614 0.576485 0.672057 11.00000 -1.20000 AFIX 0 C56 1 0.561341 0.362718 0.738007 11.00000 0.04890 0.08831 = 0.05268 0.00012 0.00532 -0.00434 AFIX 43 H56 2 0.520437 0.383770 0.746500 11.00000 -1.20000 AFIX 0 C254 1 0.385803 0.281427 0.519138 11.00000 0.10060 0.10204 = 0.10653 -0.01005 -0.00024 0.00950 AFIX 43 H254 2 0.430162 0.260430 0.521041 11.00000 -1.20000 AFIX 0 C119 1 0.446296 0.198602 0.969163 11.00000 0.07412 0.06321 = 0.06899 0.00821 0.00879 -0.00089 AFIX 43 H119 2 0.397988 0.198854 0.983320 11.00000 -1.20000 AFIX 0 C11 1 0.968615 0.489615 0.956627 11.00000 0.05146 0.07298 = 0.05315 0.00624 -0.00474 0.00718 N5 5 0.989632 0.487734 1.066728 11.00000 0.13538 0.14538 = 0.08385 0.00259 -0.02556 0.01466 C39 1 1.069066 0.460004 0.792231 11.00000 0.03311 0.06122 = 0.08745 0.01537 -0.00414 0.00221 AFIX 43 H39 2 1.121073 0.457098 0.803353 11.00000 -1.20000 AFIX 0 C96 1 0.558792 0.803416 0.912977 11.00000 0.07566 0.05228 = 0.09726 -0.03807 -0.00010 -0.00360 AFIX 43 H96 2 0.527825 0.826767 0.926861 11.00000 -1.20000 AFIX 0 C149 1 -0.113030 0.571507 0.491924 11.00000 0.05385 0.08047 = 0.05157 0.01121 -0.00579 -0.00126 C135 1 0.563196 0.266736 0.824377 11.00000 0.09537 0.09514 = 0.08836 -0.00780 -0.00026 0.00720 AFIX 43 H135 2 0.604964 0.264151 0.805544 11.00000 -1.20000 AFIX 0 C272 1 0.349075 0.317772 0.658130 11.00000 0.10582 0.06775 = 0.07439 0.02185 -0.02877 0.00573 AFIX 43 H272 2 0.397210 0.304597 0.668608 11.00000 -1.20000 AFIX 0 C127 1 0.694720 0.338158 1.095056 11.00000 0.07899 0.08645 = 0.05521 -0.00076 0.00930 -0.00417 AFIX 43 H127 2 0.720777 0.340417 1.121213 11.00000 -1.20000 AFIX 0 C243 1 0.179136 0.308510 0.294732 11.00000 0.08349 0.06848 = 0.08611 -0.02244 0.00511 0.00603 AFIX 43 H243 2 0.218187 0.311292 0.274385 11.00000 -1.20000 AFIX 0 C192 1 0.332457 0.381674 0.189750 11.00000 0.11255 0.06027 = 0.07616 -0.02037 0.00967 -0.01203 AFIX 43 H192 2 0.325295 0.374143 0.161332 11.00000 -1.20000 AFIX 0 C98 1 0.683341 0.773014 0.890255 11.00000 0.03471 0.07310 = 0.08582 -0.00549 -0.03608 -0.01333 AFIX 43 H98 2 0.739052 0.775943 0.890290 11.00000 -1.20000 AFIX 0 C28 1 0.824745 0.503716 0.622654 11.00000 0.06151 0.07572 = 0.06011 0.00025 0.00043 -0.00616 C250 1 0.039378 0.330921 0.529676 11.00000 0.06263 0.10672 = 0.04402 0.00905 0.01386 -0.02170 AFIX 43 H250 2 0.046981 0.349399 0.554196 11.00000 -1.20000 AFIX 0 C279 1 0.389256 0.579114 0.639648 11.00000 0.04882 0.10139 = 0.04491 -0.01000 -0.02386 -0.00650 AFIX 43 H279 2 0.419001 0.578234 0.664798 11.00000 -1.20000 AFIX 0 C223 1 -0.106262 0.441230 0.278940 11.00000 0.03107 0.06839 = 0.05308 -0.01104 -0.01362 -0.01826 C220 1 -0.238430 0.419494 0.330578 11.00000 0.05214 0.07677 = 0.06203 -0.00017 0.00253 0.00397 AFIX 43 H220 2 -0.225427 0.398332 0.308605 11.00000 -1.20000 AFIX 0 C66 1 0.204065 0.516841 0.939124 11.00000 0.04135 0.13195 = 0.06782 0.02602 0.03365 0.01875 AFIX 43 H66 2 0.172431 0.513825 0.962744 11.00000 -1.20000 AFIX 0 C206 1 -0.025384 0.537425 0.204184 11.00000 0.06153 0.07206 = 0.05655 0.00342 -0.00727 -0.00826 AFIX 43 H206 2 -0.059704 0.564604 0.205960 11.00000 -1.20000 AFIX 0 C212 1 -0.113428 0.622864 0.274884 11.00000 0.09880 0.09908 = 0.10835 -0.00127 0.00203 0.00522 AFIX 43 H212 2 -0.152476 0.598386 0.277534 11.00000 -1.20000 AFIX 0 C280 1 0.340017 0.620099 0.630719 11.00000 0.07474 0.11202 = 0.07264 -0.01518 0.00465 -0.00882 AFIX 43 H280 2 0.338155 0.646685 0.649393 11.00000 -1.20000 AFIX 0 N11 5 0.320252 0.747610 0.576261 11.00000 0.08640 0.11049 = 0.09096 -0.03033 0.00460 0.02077 C270 1 0.210685 0.317455 0.660412 11.00000 0.11140 0.08263 = 0.08686 0.01629 -0.02402 -0.00527 AFIX 43 H270 2 0.164320 0.303871 0.671494 11.00000 -1.20000 AFIX 0 C180 1 0.543390 0.534349 0.335494 11.00000 0.03754 0.05337 = 0.06404 0.00434 0.00658 0.00309 C131 1 0.514447 0.402990 0.987499 11.00000 0.05175 0.04319 = 0.07181 -0.00025 0.02796 0.00926 AFIX 43 H131 2 0.479644 0.427960 0.978225 11.00000 -1.20000 AFIX 0 C30 1 0.839152 0.430103 0.581440 11.00000 0.08113 0.08699 = 0.07272 0.00008 -0.00145 0.00440 AFIX 43 H30 2 0.841807 0.414629 0.555326 11.00000 -1.20000 AFIX 0 C166 1 0.181683 0.649083 0.186714 11.00000 0.06446 0.10654 = 0.07133 0.03872 0.01042 0.00678 AFIX 43 H166 2 0.142721 0.662174 0.168392 11.00000 -1.20000 AFIX 0 C31 1 0.848098 0.401832 0.617871 11.00000 0.09463 0.10376 = 0.09480 -0.00476 0.00138 -0.00347 AFIX 43 H31 2 0.855230 0.367543 0.617331 11.00000 -1.20000 AFIX 0 C245 1 0.090456 0.337356 0.496202 11.00000 0.05865 0.06226 = 0.04711 0.00314 -0.02102 -0.00547 C284 1 0.499216 0.453298 0.503950 11.00000 0.06593 0.07591 = 0.05438 0.00087 -0.00718 0.00347 AFIX 43 H284 2 0.471752 0.423333 0.501009 11.00000 -1.20000 AFIX 0 C122 1 0.616749 0.285071 0.947314 11.00000 0.05677 0.02502 = 0.06446 0.00939 0.01530 0.00396 C21 1 1.026987 0.596566 0.815144 11.00000 0.04542 0.11030 = 0.04494 0.01790 0.00199 -0.00475 AFIX 43 H21 2 1.049805 0.585751 0.840539 11.00000 -1.20000 AFIX 0 C191 1 0.289780 0.421995 0.208495 11.00000 0.06969 0.11705 = 0.06243 0.01475 -0.01747 0.00732 AFIX 43 H191 2 0.253496 0.440355 0.192088 11.00000 -1.20000 AFIX 0 C158 1 0.445029 0.648002 0.330727 11.00000 0.06070 0.04331 = 0.14050 -0.02842 -0.00310 -0.00047 AFIX 43 H158 2 0.409725 0.637691 0.351256 11.00000 -1.20000 AFIX 0 C165 1 0.241603 0.677366 0.199800 11.00000 0.10691 0.08486 = 0.06500 0.03507 0.00292 0.03097 AFIX 43 H165 2 0.246896 0.709524 0.189465 11.00000 -1.20000 AFIX 0 C227 1 -0.216283 0.454593 0.157997 11.00000 0.07732 0.08492 = 0.07446 -0.00447 -0.01147 -0.00663 AFIX 43 H227 2 -0.239023 0.458884 0.131216 11.00000 -1.20000 AFIX 0 C138 1 0.431554 0.276807 0.878611 11.00000 0.07329 0.07114 = 0.06888 -0.02007 -0.02354 0.00481 AFIX 43 H138 2 0.386722 0.280889 0.895219 11.00000 -1.20000 AFIX 0 C83 1 0.179586 0.658134 0.964690 11.00000 0.06252 0.07309 = 0.05824 0.00332 0.01326 -0.00190 AFIX 43 H83 2 0.141827 0.658696 0.985819 11.00000 -1.20000 AFIX 0 C142 1 0.209979 0.378227 0.922266 11.00000 0.08591 0.08695 = 0.10236 0.00000 0.00436 0.00350 AFIX 43 H142 2 0.154643 0.381085 0.925072 11.00000 -1.20000 AFIX 0 C167 1 0.175913 0.603340 0.198863 11.00000 0.05495 0.14678 = 0.10874 -0.01519 0.01834 -0.04359 AFIX 43 H167 2 0.133393 0.584533 0.187939 11.00000 -1.20000 AFIX 0 C214 1 -0.106919 0.550452 0.355003 11.00000 0.08349 0.08248 = 0.06366 -0.00683 -0.00625 0.00207 AFIX 43 H214 2 -0.075719 0.577947 0.362349 11.00000 -1.20000 AFIX 0 C286 1 0.616895 0.497152 0.497574 11.00000 0.06057 0.09047 = 0.06653 0.00513 -0.00317 0.00062 AFIX 43 H286 2 0.671571 0.497791 0.492113 11.00000 -1.20000 AFIX 0 C137 1 0.441435 0.233866 0.854980 11.00000 0.09620 0.09447 = 0.10171 0.00119 -0.00879 -0.00253 AFIX 43 H137 2 0.404528 0.208034 0.856873 11.00000 -1.20000 AFIX 0 C202 1 0.061369 0.482418 0.237045 11.00000 0.07242 0.08700 = 0.06135 0.01044 0.03374 -0.00481 AFIX 43 H202 2 0.087913 0.470435 0.261061 11.00000 -1.20000 AFIX 0 C221 1 -0.193209 0.464043 0.337520 11.00000 0.03327 0.05634 = 0.04455 0.00551 -0.00677 0.01076 C5 1 0.480949 0.536575 1.035187 11.00000 0.06812 0.07045 = 0.08354 -0.00540 0.00453 -0.00032 N3 5 0.422312 0.539662 1.053371 11.00000 0.05440 0.13791 = 0.14443 -0.04936 0.05334 -0.00096 C285 1 0.578117 0.454391 0.491609 11.00000 0.08197 0.08133 = 0.07152 0.00396 0.01082 0.00411 AFIX 43 H285 2 0.602774 0.426843 0.479806 11.00000 -1.20000 AFIX 0 C218 1 -0.319212 0.440374 0.389775 11.00000 0.07180 0.08111 = 0.07097 0.00682 0.01359 0.00251 AFIX 43 H218 2 -0.362274 0.431548 0.406368 11.00000 -1.20000 AFIX 0 C216 1 -0.211715 0.494307 0.373044 11.00000 0.07135 0.07927 = 0.06254 0.00344 0.00956 0.00427 C117 1 0.535271 0.155957 0.925497 11.00000 0.08895 0.05272 = 0.08973 -0.00705 0.02218 -0.01164 AFIX 43 H117 2 0.548502 0.128733 0.908989 11.00000 -1.20000 AFIX 0 C201 1 0.013243 0.522379 0.240486 11.00000 0.06269 0.05347 = 0.07966 -0.00855 -0.00945 -0.00772 C53 1 0.682691 0.296272 0.717473 11.00000 0.07920 0.07777 = 0.08882 -0.01110 0.00509 -0.00607 AFIX 43 H53 2 0.723904 0.273509 0.713482 11.00000 -1.20000 AFIX 0 C54 1 0.604041 0.281299 0.716745 11.00000 0.09841 0.12784 = 0.08262 -0.04479 -0.00282 -0.00363 AFIX 43 H54 2 0.590528 0.248876 0.709263 11.00000 -1.20000 AFIX 0 C182 1 0.654869 0.589786 0.328516 11.00000 0.04831 0.09574 = 0.09111 0.04118 -0.01257 -0.02118 AFIX 43 H182 2 0.696379 0.602647 0.312705 11.00000 -1.20000 AFIX 0 C209 1 0.001719 0.696431 0.264464 11.00000 0.10492 0.10140 = 0.10698 0.00456 -0.00207 -0.00075 AFIX 43 H209 2 0.040389 0.721411 0.264668 11.00000 -1.20000 AFIX 0 C143 1 0.247394 0.396256 0.884380 11.00000 0.07995 0.09070 = 0.09682 0.00267 -0.00638 0.00104 AFIX 43 H143 2 0.219001 0.407181 0.860562 11.00000 -1.20000 AFIX 0 C97 1 0.640120 0.809096 0.911113 11.00000 0.09174 0.06151 = 0.07394 0.01440 -0.03835 -0.03270 AFIX 43 H97 2 0.665765 0.836343 0.923459 11.00000 -1.20000 AFIX 0 C118 1 0.468929 0.154921 0.945074 11.00000 0.07135 0.08544 = 0.14469 -0.00549 -0.00754 -0.01815 AFIX 43 H118 2 0.436003 0.126983 0.943948 11.00000 -1.20000 AFIX 0 N2 5 0.751602 0.735519 1.019060 11.00000 0.18517 0.18804 = 0.18079 -0.02530 0.02024 -0.00467 C247 1 0.024835 0.271587 0.457140 11.00000 0.09851 0.10200 = 0.08728 -0.03778 0.00914 -0.04132 AFIX 43 H247 2 0.018516 0.252494 0.432876 11.00000 -1.20000 AFIX 0 C9 1 0.975162 0.497683 1.032195 11.00000 0.08483 0.09086 = 0.07167 0.00096 -0.00881 0.00043 C136 1 0.506347 0.229474 0.828539 11.00000 0.10816 0.10932 = 0.09915 -0.00553 -0.00722 0.00203 AFIX 43 H136 2 0.511906 0.200406 0.813018 11.00000 -1.20000 AFIX 0 C271 1 0.283645 0.299829 0.672110 11.00000 0.07746 0.08084 = 0.08589 0.02770 -0.02336 0.00336 AFIX 43 H271 2 0.286582 0.273555 0.691119 11.00000 -1.20000 AFIX 0 C226 1 -0.237578 0.487990 0.191717 11.00000 0.05996 0.09079 = 0.08150 0.00644 -0.00784 -0.01731 AFIX 43 H226 2 -0.276120 0.512554 0.187056 11.00000 -1.20000 AFIX 0 C144 1 0.326698 0.395268 0.887826 11.00000 0.07186 0.08273 = 0.09257 0.00834 0.00542 -0.00558 AFIX 43 H144 2 0.353003 0.411417 0.866226 11.00000 -1.20000 AFIX 0 C236 1 -0.172837 0.342821 0.434564 11.00000 0.09453 0.10251 = 0.10024 0.01141 0.00612 0.00361 AFIX 43 H236 2 -0.204705 0.329706 0.455517 11.00000 -1.20000 AFIX 0 N1 5 0.928404 0.756455 0.933330 11.00000 0.11612 0.11210 = 0.18927 -0.01274 0.02180 -0.07348 C22 1 1.071273 0.624774 0.787529 11.00000 0.06815 0.08512 = 0.08857 -0.00516 -0.00020 -0.00498 AFIX 43 H22 2 1.123100 0.634685 0.795282 11.00000 -1.20000 AFIX 0 C237 1 -0.179556 0.317637 0.396533 11.00000 0.09886 0.10299 = 0.10747 0.00881 0.00478 -0.00088 AFIX 43 H237 2 -0.212907 0.290520 0.391102 11.00000 -1.20000 AFIX 0 C238 1 -0.128601 0.339357 0.367916 11.00000 0.09611 0.09455 = 0.09850 0.00581 0.00383 -0.00589 AFIX 43 H238 2 -0.131612 0.327791 0.340331 11.00000 -1.20000 AFIX 0 C235 1 -0.127764 0.383840 0.447474 11.00000 0.10606 0.10621 = 0.10210 0.00432 0.00691 -0.00010 AFIX 43 H235 2 -0.131507 0.398983 0.473677 11.00000 -1.20000 AFIX 0 C210 1 -0.078944 0.706539 0.255918 11.00000 0.13237 0.12914 = 0.13424 0.00052 -0.00325 0.00250 AFIX 43 H210 2 -0.094167 0.737524 0.245463 11.00000 -1.20000 AFIX 0 C211 1 -0.136898 0.670494 0.262946 11.00000 0.09578 0.08949 = 0.09248 0.00789 -0.00250 0.00620 AFIX 43 H211 2 -0.191188 0.678210 0.259675 11.00000 -1.20000 AFIX 0 C241 1 0.109899 0.257160 0.346156 11.00000 0.11733 0.11199 = 0.11574 0.00835 0.00432 0.00709 AFIX 43 H241 2 0.106297 0.228056 0.361810 11.00000 -1.20000 AFIX 0 C52 1 0.698571 0.343311 0.723907 11.00000 0.06735 0.07216 = 0.07231 -0.01495 0.00484 -0.00536 AFIX 43 H52 2 0.751422 0.353282 0.720038 11.00000 -1.20000 AFIX 0 C217 1 -0.278222 0.483072 0.399084 11.00000 0.08142 0.08725 = 0.07801 0.00458 0.00618 0.00916 AFIX 43 H217 2 -0.292748 0.503704 0.421136 11.00000 -1.20000 AFIX 0 C219 1 -0.298435 0.408292 0.355171 11.00000 0.06767 0.07721 = 0.08065 0.00282 -0.00317 0.00020 AFIX 43 H219 2 -0.327821 0.379376 0.350216 11.00000 -1.20000 AFIX 0 C287 1 0.581827 0.540958 0.511359 11.00000 0.09246 0.09911 = 0.09359 -0.00577 0.00220 -0.00842 AFIX 43 H287 2 0.610145 0.570752 0.512740 11.00000 -1.20000 AFIX 0 C15 1 0.719301 0.723607 0.767321 11.00000 0.08534 0.09071 = 0.08725 -0.00513 0.00770 0.00498 AFIX 43 H15 2 0.724978 0.748390 0.787592 11.00000 -1.20000 AFIX 0 HKLF 4 REM s_a.res in P2(1) REM R1 = 0.0808 for 42412 Fo > 4sig(Fo) and 0.0994 for all 53322 data REM 3121 parameters refined using 651 restraints END WGHT 0.1294 148.9016 REM Highest difference peak 5.749, deepest hole -2.520, 1-sigma level 0.369 Q1 1 0.5999 0.5207 0.7988 11.00000 0.05 5.75 Q2 1 0.1941 0.5634 0.4014 11.00000 0.05 5.33 Q3 1 0.2728 0.4604 0.4805 11.00000 0.05 5.09 Q4 1 0.1952 0.4793 0.4020 11.00000 0.05 5.06 Q5 1 0.5413 0.3964 0.8795 11.00000 0.05 5.03 Q6 1 0.7013 0.3784 0.9046 11.00000 0.05 4.83 Q7 1 0.6568 0.5606 0.8749 11.00000 0.05 4.80 Q8 1 0.7995 0.5442 0.9006 11.00000 0.05 4.78 Q9 1 0.2853 0.5560 0.4408 11.00000 0.05 4.66 Q10 1 0.5381 0.4826 0.8783 11.00000 0.05 4.62 ; _shelx_res_checksum 89042 _shelx_hkl_file ; 0 -33 0 0.07 0.94 0 -33 -1 0.92 0.96 0 -33 1 3.79 1.04 0 -33 -2 1.54 1.00 0 -33 2 1.47 0.97 0 -33 -3 0.07 0.90 0 -33 3 0.10 0.92 0 -33 4 1.43 0.90 0 -33 -4 -0.10 0.90 0 -33 -5 1.18 0.84 0 -33 5 0.61 0.85 0 -33 -6 0.80 0.83 0 -32 0 7.89 1.60 0 -32 -1 0.54 1.42 0 -32 1 3.06 1.42 0 -32 2 2.28 1.40 0 -32 -2 2.45 1.47 0 -32 -3 7.38 1.47 0 -32 3 7.84 1.56 0 -32 -4 0.39 1.31 0 -32 4 0.86 1.33 0 -32 -5 3.57 1.39 0 -32 5 2.11 1.30 0 -32 -6 1.30 1.27 0 -32 6 3.10 1.25 0 -32 7 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6.08 1.63 0 -29 15 6.26 1.61 0 -29 -15 1.56 1.03 0 -29 -16 2.19 1.44 0 -29 -17 6.83 1.47 0 -29 -18 2.31 1.19 0 -29 -19 4.39 1.04 0 -28 0 10.16 2.60 0 -28 0 6.34 2.98 0 -28 1 9.80 3.14 0 -28 1 6.01 2.56 0 -28 -1 8.59 2.99 0 -28 -1 5.90 2.50 0 -28 -2 2.30 2.49 0 -28 -2 2.28 2.73 0 -28 2 4.49 2.48 0 -28 2 5.58 3.16 0 -28 -3 12.05 2.84 0 -28 -3 20.09 2.95 0 -28 3 13.60 2.88 0 -28 3 17.15 3.35 0 -28 4 7.97 2.61 0 -28 4 10.79 3.27 0 -28 -4 8.12 2.63 0 -28 -4 9.59 2.55 0 -28 -5 4.71 2.43 0 -28 5 5.68 3.08 0 -28 5 6.97 2.56 0 -28 -5 8.67 2.25 0 -28 6 6.52 2.41 0 -28 -6 5.67 2.10 0 -28 6 9.31 3.08 0 -28 -6 5.03 2.42 0 -28 7 2.25 2.44 0 -28 -7 7.96 2.54 0 -28 -7 6.03 1.96 0 -28 7 11.49 3.02 0 -28 8 4.89 2.48 0 -28 -8 9.46 2.05 0 -28 8 12.05 2.90 0 -28 -8 10.54 2.56 0 -28 -9 5.63 2.41 0 -28 9 9.15 2.62 0 -28 -9 6.22 1.87 0 -28 9 11.40 2.59 0 -28 -10 3.59 2.30 0 -28 -10 1.96 1.64 0 -28 10 6.53 2.19 0 -28 10 3.96 2.35 0 -28 -11 6.20 1.75 0 -28 11 7.70 2.37 0 -28 11 8.12 2.11 0 -28 -11 5.94 2.40 0 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3.77 2.68 0 -27 8 3.09 2.61 0 -27 -8 5.56 1.98 0 -27 9 -0.33 2.38 0 -27 -9 2.45 2.45 0 -27 9 2.86 2.83 0 -27 -9 -0.07 1.92 0 -27 10 16.74 3.07 0 -27 -10 13.02 2.93 0 -27 10 13.22 2.86 0 -27 -10 12.89 2.25 0 -27 -11 30.47 3.10 0 -27 -11 27.63 3.58 0 -27 11 29.74 3.67 0 -27 11 28.76 3.59 0 -27 -12 -3.91 2.58 0 -27 12 -3.26 2.48 0 -27 12 1.51 2.20 0 -27 -12 2.14 1.74 0 -27 -13 13.08 2.13 0 -27 -13 13.55 2.80 0 -27 13 13.30 2.73 0 -27 -14 40.43 4.18 0 -27 14 40.52 4.13 0 -27 -14 43.39 3.78 0 -27 -15 20.99 2.88 0 -27 -15 16.16 2.21 0 -27 15 20.37 2.83 0 -27 16 0.46 2.13 0 -27 -16 -0.94 2.15 0 -27 -16 -3.26 1.52 0 -27 -17 24.02 2.43 0 -27 -18 16.34 1.85 0 -27 -19 7.25 1.29 0 -27 -20 3.88 0.99 0 -26 0 0.24 2.79 0 -26 0 2.85 2.75 0 -26 -1 7.36 2.76 0 -26 -1 3.13 2.47 0 -26 1 3.21 2.79 0 -26 1 8.34 3.02 0 -26 2 17.26 3.23 0 -26 2 16.32 3.53 0 -26 -2 14.16 3.21 0 -26 -2 18.26 2.82 0 -26 3 6.83 3.24 0 -26 -3 3.09 2.72 0 -26 -3 2.93 2.24 0 -26 3 3.23 2.70 0 -26 -4 14.18 2.63 0 -26 4 16.33 3.51 0 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2.00 0 -26 20 7.28 1.65 0 -26 -20 11.79 1.55 0 -26 21 5.56 1.49 0 -26 -21 9.31 1.31 0 -26 -22 4.36 0.95 0 -26 22 1.45 1.18 0 -25 0 1.30 2.49 0 -25 0 1.00 2.64 0 -25 -1 3.24 2.31 0 -25 1 -1.18 2.70 0 -25 -1 -1.72 2.71 0 -25 1 -0.74 2.83 0 -25 -2 18.08 2.89 0 -25 2 22.38 3.35 0 -25 2 20.04 3.66 0 -25 -2 18.88 3.35 0 -25 3 17.78 3.31 0 -25 -3 18.43 2.83 0 -25 3 17.21 3.57 0 -25 -3 15.97 3.31 0 -25 -4 22.95 3.06 0 -25 4 27.50 3.70 0 -25 -4 20.35 3.67 0 -25 4 24.48 3.86 0 -25 -5 12.42 2.59 0 -25 5 14.12 3.23 0 -25 5 14.91 3.46 0 -25 -5 12.04 3.21 0 -25 -6 37.30 3.94 0 -25 6 31.00 4.32 0 -25 6 37.05 4.55 0 -25 -6 41.52 4.42 0 -25 7 56.29 5.35 0 -25 -7 50.58 4.94 0 -25 7 55.89 5.44 0 -25 -7 51.41 5.37 0 -25 -8 9.67 2.43 0 -25 8 11.32 3.16 0 -25 -8 8.10 3.28 0 -25 8 11.41 3.18 0 -25 -9 18.62 2.77 0 -25 -9 17.52 3.44 0 -25 9 20.83 3.40 0 -25 9 16.86 3.30 0 -25 -10 0.26 3.02 0 -25 10 -0.92 2.80 0 -25 10 -1.28 2.75 0 -25 -10 0.30 2.02 0 -25 11 49.09 4.73 0 -25 -11 46.12 4.37 0 -25 -11 44.61 4.93 0 -25 11 50.32 4.85 0 -25 12 -0.42 2.57 0 -25 12 2.08 2.72 0 -25 -12 2.32 2.84 0 -25 12 0.07 1.55 0 -25 -12 0.44 2.01 0 -25 13 19.09 2.73 0 -25 13 23.06 3.60 0 -25 13 29.17 3.45 0 -25 -13 27.73 3.07 0 -25 -13 31.97 3.80 0 -25 14 22.98 3.07 0 -25 -14 34.49 3.32 0 -25 14 36.46 3.95 0 -25 14 34.26 3.67 0 -25 -15 15.94 2.44 0 -25 15 11.00 2.28 0 -25 16 1.41 2.67 0 -25 -16 4.61 1.95 0 -25 16 3.49 1.87 0 -25 17 38.47 3.76 0 -25 -17 31.67 3.12 0 -25 -18 31.32 2.95 0 -25 18 29.38 3.47 0 -25 18 20.49 2.96 0 -25 -19 22.63 2.49 0 -25 19 20.72 2.72 0 -25 -20 12.03 1.81 0 -25 20 7.73 2.08 0 -25 -21 19.96 2.07 0 -25 21 13.87 2.31 0 -25 -22 2.35 1.24 0 -25 22 4.37 1.62 0 -25 -23 5.72 1.15 0 -25 23 3.31 1.45 0 -25 -24 4.22 0.90 0 -25 24 3.93 1.40 0 -25 25 5.30 1.22 0 -24 0 13.25 3.16 0 -24 0 19.80 2.93 0 -24 1 9.93 2.93 0 -24 -1 6.95 2.43 0 -24 1 5.74 2.66 0 -24 -1 7.34 2.83 0 -24 2 30.52 3.82 0 -24 2 30.83 3.95 0 -24 -2 29.91 3.47 0 -24 -2 30.78 3.99 0 -24 3 24.23 3.67 0 -24 3 15.72 3.33 0 -24 -3 21.34 3.01 0 -24 -3 22.80 3.54 0 -24 4 25.88 3.66 0 -24 -4 19.37 3.58 0 -24 -4 22.27 3.08 0 -24 4 20.56 3.76 0 -24 -5 61.37 5.57 0 -24 5 66.94 6.03 0 -24 5 64.46 5.92 0 -24 -5 59.87 5.92 0 -24 -6 13.90 3.53 0 -24 6 15.73 3.55 0 -24 -6 11.90 2.85 0 -24 6 22.65 3.39 0 -24 -7 29.18 4.34 0 -24 7 43.13 4.41 0 -24 -7 37.64 3.91 0 -24 7 40.61 4.50 0 -24 -8 38.30 3.94 0 -24 8 39.70 4.37 0 -24 -8 33.93 4.51 0 -24 8 40.61 4.48 0 -24 -9 45.23 4.93 0 -24 9 50.45 4.99 0 -24 -9 41.11 4.32 0 -24 9 49.06 4.78 0 -24 -10 11.92 2.55 0 -24 10 11.29 2.95 0 -24 10 14.95 3.31 0 -24 -10 13.33 3.56 0 -24 -11 26.28 4.03 0 -24 11 34.84 3.91 0 -24 11 36.58 3.71 0 -24 11 20.89 2.92 0 -24 -11 28.94 3.35 0 -24 12 4.69 1.92 0 -24 12 7.24 2.61 0 -24 12 9.48 2.97 0 -24 -12 4.46 2.21 0 -24 13 33.13 3.81 0 -24 13 33.17 4.03 0 -24 13 25.15 3.27 0 -24 -13 37.09 3.49 0 -24 14 -3.17 2.96 0 -24 -14 0.30 2.07 0 -24 14 -0.44 2.50 0 -24 14 2.55 1.98 0 -24 15 54.37 4.67 0 -24 15 45.53 4.74 0 -24 -15 48.20 4.31 0 -24 -16 21.17 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0 1 -33 17.56 3.28 0 1 -34 12.65 2.92 0 1 -35 22.04 3.79 0 1 -35 27.07 3.39 0 1 -36 3.18 2.22 0 1 -36 1.47 2.86 0 1 -37 18.28 2.49 0 1 -37 16.46 3.09 0 1 -38 3.78 1.50 0 1 -38 -0.06 2.01 0 1 -39 5.16 1.53 0 1 -39 4.56 1.18 0 2 0 7166.62 513.64 0 2 -1 45.14 3.63 0 2 1 44.03 3.81 0 2 -2 32.53 2.87 0 2 2 35.29 3.21 0 2 -3 166.02 11.05 0 2 3 126.83 11.06 0 2 4 527.08 38.33 0 2 5 13.55 2.66 0 2 6 174.13 13.41 0 2 7 365.16 27.15 0 2 -8 122.03 9.67 0 2 8 103.25 9.25 0 2 -9 178.62 14.39 0 2 -10 57.16 6.13 0 2 -11 73.37 7.47 0 2 -12 64.34 6.99 0 2 -13 178.96 15.07 0 2 -14 56.81 6.79 0 2 -15 77.45 5.87 0 2 -15 73.86 5.80 0 2 -15 80.89 8.44 0 2 -16 26.95 2.53 0 2 16 26.85 5.58 0 2 -16 25.24 2.61 0 2 -16 37.21 5.57 0 2 -17 12.76 1.98 0 2 -17 14.67 1.85 0 2 17 11.83 4.93 0 2 -17 19.58 4.45 0 2 -18 59.92 7.74 0 2 -18 66.89 5.13 0 2 18 58.72 8.25 0 2 -18 61.83 5.17 0 2 -19 14.07 2.22 0 2 -19 14.83 2.05 0 2 -20 16.44 2.17 0 2 -20 12.45 3.92 0 2 -20 11.82 2.23 0 2 -21 85.52 6.89 0 2 -21 88.12 6.99 0 2 -22 32.30 3.52 0 2 -22 36.07 3.53 0 2 -23 38.41 4.11 0 2 -23 40.12 3.99 0 2 -23 41.81 4.36 0 2 -24 9.26 2.96 0 2 -24 13.69 3.11 0 2 -24 15.20 2.86 0 2 -25 134.04 10.33 0 2 -25 127.58 10.53 0 2 -26 100.55 9.26 0 2 -26 123.47 9.14 0 2 -27 82.26 6.71 0 2 -27 64.28 6.91 0 2 -28 86.03 7.09 0 2 -28 71.35 7.38 0 2 -29 65.78 5.60 0 2 -29 42.65 5.78 0 2 -30 45.17 4.93 0 2 -31 19.26 3.54 0 2 -32 8.40 2.98 0 2 -33 20.90 3.44 0 2 -34 10.76 2.85 0 2 -35 15.87 2.95 0 2 -36 7.23 2.32 0 2 -37 16.17 2.40 0 2 -38 7.36 1.70 0 2 -38 5.06 2.15 0 2 -39 5.85 1.61 0 3 0 2.27 2.35 0 3 1 51.10 4.41 0 3 -1 44.97 4.16 0 3 1 48.56 4.72 0 3 -2 753.62 53.72 0 3 2 731.60 53.89 0 3 3 13.23 2.49 0 3 -3 7.41 1.85 0 3 4 131.54 10.77 0 3 -4 145.14 10.69 0 3 5 224.11 16.91 0 3 6 184.86 14.22 0 3 7 188.31 14.58 0 3 8 144.70 11.66 0 3 9 370.76 29.15 0 3 -9 419.76 29.72 0 3 -10 187.14 14.24 0 3 10 158.74 13.59 0 3 -11 73.59 7.61 0 3 -12 135.81 11.99 0 3 -13 136.99 12.27 0 3 -14 114.04 10.90 0 3 -15 68.52 5.47 0 3 -15 78.82 5.65 0 3 -15 77.00 8.15 0 3 -15 66.81 5.53 0 3 -16 133.71 12.68 0 3 -16 135.39 10.10 0 3 -16 135.04 10.06 0 3 17 80.19 9.34 0 3 -17 72.71 5.55 0 3 -17 67.99 5.47 0 3 -17 61.38 7.96 0 3 -18 0.24 1.50 0 3 18 -3.51 4.55 0 3 -18 -1.84 3.45 0 3 -18 2.22 1.51 0 3 -19 65.50 5.45 0 3 -19 67.32 5.38 0 3 -19 70.25 8.43 0 3 -20 53.92 4.39 0 3 -20 52.53 4.47 0 3 -21 5.35 2.16 0 3 -21 4.02 1.90 0 3 -22 1.27 2.13 0 3 -22 2.22 2.02 0 3 -23 58.05 5.49 0 3 -23 68.41 5.49 0 3 -24 83.95 6.79 0 3 -24 79.64 6.86 0 3 -25 67.22 5.70 0 3 -25 57.11 5.77 0 3 -26 16.62 3.15 0 3 -27 64.29 5.95 0 3 -28 88.43 7.60 0 3 -29 29.60 4.00 0 3 -30 14.80 3.31 0 3 -31 8.11 3.08 0 3 -32 8.66 3.01 0 3 -33 19.29 3.33 0 3 -34 6.79 2.73 0 3 -35 17.68 2.94 0 3 -36 14.09 2.62 0 3 -37 7.76 2.03 0 3 -38 2.69 1.54 0 4 0 385.37 28.70 0 4 -1 18.62 2.88 0 4 1 15.29 2.97 0 4 1 15.03 3.60 0 4 -2 10.34 2.08 0 4 2 5.62 2.70 0 4 3 16.80 3.06 0 4 -3 15.64 2.41 0 4 4 53.80 5.14 0 4 -4 50.18 4.69 0 4 5 25.26 3.82 0 4 -5 25.89 3.28 0 4 6 779.77 56.87 0 4 7 106.02 8.95 0 4 8 117.77 9.89 0 4 9 28.52 3.96 0 4 10 109.12 9.74 0 4 -10 119.32 10.38 0 4 11 143.53 12.21 0 4 -11 152.27 12.85 0 4 -12 166.49 14.26 0 4 -13 74.26 8.16 0 4 -14 157.27 13.50 0 4 -14 156.88 11.08 0 4 -14 140.13 10.92 0 4 -14 150.14 10.98 0 4 -15 162.01 15.27 0 4 -15 172.47 12.92 0 4 -15 188.99 13.02 0 4 -15 169.11 12.87 0 4 -16 52.66 4.24 0 4 -16 49.00 4.12 0 4 -16 54.46 6.97 0 4 -16 47.88 4.06 0 4 -17 57.95 4.77 0 4 -17 59.89 4.82 0 4 -17 62.02 4.93 0 4 -17 51.34 7.39 0 4 18 103.14 12.66 0 4 -18 122.23 9.17 0 4 -18 120.06 9.09 0 4 -18 106.23 11.79 0 4 -18 123.46 9.26 0 4 -19 46.67 3.88 0 4 -19 45.51 4.01 0 4 -19 42.09 4.09 0 4 -19 33.40 6.34 0 4 -20 20.62 2.57 0 4 -20 19.83 2.75 0 4 -20 19.29 2.45 0 4 -21 85.85 6.52 0 4 -21 76.74 6.55 0 4 -22 35.94 3.71 0 4 -22 36.24 3.57 0 4 -23 20.49 2.86 0 4 -23 17.23 2.94 0 4 -24 1.27 2.35 0 4 -24 0.89 2.14 0 4 -25 44.07 4.49 0 4 -25 45.20 4.57 0 4 -26 50.64 4.93 0 4 -26 45.66 4.72 0 4 -27 78.17 6.78 0 4 -28 21.68 3.51 0 4 -29 3.97 2.93 0 4 -30 13.96 3.17 0 4 -31 15.94 3.34 0 4 -32 -1.23 2.81 0 4 -33 2.11 2.62 0 4 -34 25.11 3.42 0 4 -35 11.26 2.59 0 4 -36 7.20 2.31 0 4 -37 12.52 2.19 0 4 -38 4.34 1.56 0 5 0 3.72 3.61 0 5 1 68.16 7.16 0 5 -1 66.53 6.21 0 5 1 68.94 6.39 0 5 -2 1.80 2.26 0 5 2 1.01 2.66 0 5 2 -0.54 3.72 0 5 3 19.63 3.85 0 5 -3 26.78 3.08 0 5 -4 88.33 7.39 0 5 4 91.79 7.90 0 5 -5 80.77 7.05 0 5 5 84.81 7.59 0 5 6 177.31 14.17 0 5 -6 181.72 14.00 0 5 7 30.18 4.24 0 5 8 99.63 8.78 0 5 9 56.77 5.97 0 5 10 320.47 24.43 0 5 -11 116.85 11.00 0 5 11 118.82 10.26 0 5 12 257.77 20.59 0 5 -12 272.30 21.46 0 5 -13 691.16 52.06 0 5 -14 270.38 20.22 0 5 -14 272.24 20.19 0 5 -14 293.28 20.31 0 5 -14 292.50 22.82 0 5 -15 71.34 5.80 0 5 -15 70.62 5.86 0 5 -15 79.26 8.80 0 5 -15 86.23 5.98 0 5 -16 62.41 8.17 0 5 -16 65.75 5.43 0 5 -16 71.75 5.62 0 5 -16 72.90 5.52 0 5 -17 114.78 8.88 0 5 -17 119.88 11.93 0 5 -17 114.85 8.83 0 5 -17 123.42 9.02 0 5 -18 17.84 2.25 0 5 -18 18.39 2.43 0 5 -18 24.08 4.90 0 5 -18 19.14 2.31 0 5 -19 24.45 2.51 0 5 -19 19.74 2.72 0 5 -19 20.23 2.54 0 5 -19 17.20 4.73 0 5 -20 40.57 3.80 0 5 -20 39.82 3.69 0 5 -20 41.63 3.92 0 5 -21 0.14 2.05 0 5 -21 1.73 1.89 0 5 -21 3.43 2.28 0 5 -22 12.81 2.65 0 5 -22 12.33 2.36 0 5 -22 10.47 2.27 0 5 -23 96.61 7.73 0 5 -23 96.29 7.42 0 5 -23 84.54 7.49 0 5 -24 7.97 2.93 0 5 -24 5.45 2.51 0 5 -24 10.81 2.49 0 5 -25 40.67 4.25 0 5 -25 37.37 4.56 0 5 -25 38.94 4.14 0 5 -26 11.54 2.77 0 5 -26 10.98 3.46 0 5 -26 10.46 2.91 0 5 -27 7.10 2.87 0 5 -28 7.66 2.95 0 5 -29 17.90 3.29 0 5 -30 4.75 2.95 0 5 -31 6.67 3.00 0 5 -32 4.26 2.82 0 5 -33 4.57 2.66 0 5 -34 5.25 2.55 0 5 -35 7.58 2.44 0 5 -36 24.60 3.01 0 5 -37 8.74 1.99 0 5 -38 12.87 1.90 0 6 0 -1.62 4.04 0 6 1 48.95 6.61 0 6 -1 50.33 5.65 0 6 1 50.84 5.65 0 6 2 133.89 11.17 0 6 2 130.47 11.92 0 6 -2 135.33 10.68 0 6 3 77.60 7.90 0 6 -3 71.91 6.19 0 6 3 59.67 6.78 0 6 4 21.81 4.04 0 6 -4 21.68 3.15 0 6 -5 74.06 6.38 0 6 5 67.25 6.88 0 6 6 179.08 13.97 0 6 -6 168.95 13.55 0 6 7 28.21 4.21 0 6 -7 16.93 3.48 0 6 8 128.15 10.88 0 6 9 210.42 16.69 0 6 10 158.74 13.10 0 6 11 348.41 26.64 0 6 12 286.05 22.06 0 6 -12 276.97 22.87 0 6 13 23.51 4.21 0 6 -13 34.89 5.55 0 6 -14 146.06 11.05 0 6 -14 162.49 14.06 0 6 -14 150.67 11.14 0 6 -15 189.19 14.80 0 6 -15 210.11 14.96 0 6 -15 209.72 14.87 0 6 -15 210.97 17.95 0 6 -16 174.34 13.36 0 6 -16 189.00 13.51 0 6 -16 181.28 13.41 0 6 -16 194.83 16.64 0 6 -17 24.96 2.75 0 6 -17 27.19 2.66 0 6 -17 24.28 2.54 0 6 -18 79.51 6.34 0 6 -18 68.40 9.19 0 6 -18 77.78 6.29 0 6 -18 85.50 6.52 0 6 -19 82.00 6.05 0 6 -19 71.24 6.08 0 6 -19 72.72 6.22 0 6 -20 27.00 3.14 0 6 -20 27.83 2.92 0 6 -20 28.22 3.01 0 6 -21 41.69 4.25 0 6 -21 51.46 4.24 0 6 -21 47.35 4.48 0 6 -22 5.76 2.10 0 6 -22 2.98 2.39 0 6 -22 4.41 2.03 0 6 -23 0.21 2.26 0 6 -23 -0.82 2.31 0 6 -23 -2.60 2.66 0 6 -24 20.65 3.45 0 6 -24 21.16 3.08 0 6 -24 21.03 3.20 0 6 -25 43.83 4.27 0 6 -25 41.67 4.70 0 6 -25 40.51 4.41 0 6 -26 0.94 2.68 0 6 -26 -0.41 2.62 0 6 -26 0.11 2.93 0 6 -27 13.42 3.73 0 6 -27 16.58 3.33 0 6 -27 21.95 3.28 0 6 -28 13.40 3.03 0 6 -28 12.66 3.59 0 6 -29 20.84 3.49 0 6 -29 11.99 3.82 0 6 -30 -1.25 3.46 0 6 -30 0.80 2.75 0 6 -31 9.40 3.03 0 6 -31 4.77 3.59 0 6 -32 10.69 2.98 0 6 -33 1.47 2.56 0 6 -34 17.87 2.91 0 6 -35 6.70 2.34 0 6 -36 13.58 2.48 0 6 -37 4.79 1.84 0 6 -38 3.51 1.47 0 7 0 1.90 3.99 0 7 1 177.20 14.80 0 7 -1 180.99 13.97 0 7 1 159.07 13.97 0 7 -2 154.85 12.54 0 7 2 151.08 12.97 0 7 2 169.32 13.84 0 7 3 215.12 17.29 0 7 3 195.47 16.34 0 7 -3 206.85 15.79 0 7 4 152.61 13.13 0 7 -4 137.67 11.37 0 7 4 149.68 12.16 0 7 5 47.08 5.79 0 7 -5 50.95 5.01 0 7 -6 14.03 2.88 0 7 6 13.16 3.78 0 7 -7 57.08 5.95 0 7 7 68.53 6.72 0 7 8 71.75 7.32 0 7 9 77.14 7.61 0 7 10 155.01 12.95 0 7 11 161.93 13.47 0 7 12 143.32 12.27 0 7 -13 431.26 32.21 0 7 13 406.73 30.86 0 7 -13 423.56 29.32 0 7 -13 386.42 29.22 0 7 -14 340.82 25.59 0 7 -14 367.34 25.69 0 7 14 356.15 27.30 0 7 -14 352.87 28.55 0 7 -15 2.39 1.30 0 7 -15 3.47 1.52 0 7 -15 3.72 3.82 0 7 -16 111.38 8.49 0 7 -16 111.02 8.45 0 7 -16 112.84 8.62 0 7 -16 115.52 11.84 0 7 -17 116.33 8.86 0 7 -17 115.32 8.70 0 7 -17 103.77 11.80 0 7 -17 114.27 8.73 0 7 -18 95.06 7.56 0 7 -18 96.81 7.52 0 7 -18 100.35 7.72 0 7 -19 0.11 1.67 0 7 -19 -0.15 2.00 0 7 -19 -0.64 1.72 0 7 -20 2.19 1.76 0 7 -20 5.73 1.90 0 7 -20 5.95 2.23 0 7 -21 17.88 2.88 0 7 -21 23.40 2.60 0 7 -21 17.83 2.56 0 7 -22 8.56 2.54 0 7 -22 11.34 2.34 0 7 -22 9.53 2.22 0 7 -23 39.22 4.17 0 7 -23 44.62 4.52 0 7 -23 43.90 4.12 0 7 -24 20.27 2.95 0 7 -24 14.86 2.88 0 7 -24 18.01 3.34 0 7 -25 12.26 2.81 0 7 -25 8.00 3.15 0 7 -25 12.73 2.74 0 7 -26 11.71 3.43 0 7 -26 13.39 3.00 0 7 -26 15.98 2.97 0 7 -27 19.06 3.28 0 7 -27 22.37 3.81 0 7 -27 19.90 3.36 0 7 -28 1.49 3.29 0 7 -28 2.45 2.68 0 7 -29 18.40 3.96 0 7 -29 20.26 3.46 0 7 -30 5.19 2.94 0 7 -30 9.14 3.57 0 7 -31 31.72 4.47 0 7 -31 31.26 3.95 0 7 -32 3.53 2.79 0 7 -33 10.04 2.74 0 7 -34 9.86 2.58 0 7 -35 2.21 2.24 0 7 -36 16.48 2.53 0 7 -37 6.69 1.86 0 7 -38 17.77 2.02 0 8 0 302.87 23.71 0 8 1 180.78 16.03 0 8 -1 185.93 15.31 0 8 1 198.33 15.54 0 8 -2 152.48 11.84 0 8 2 133.99 12.25 0 8 2 138.50 13.17 0 8 3 149.97 13.90 0 8 3 146.11 13.02 0 8 -3 163.47 12.49 0 8 4 141.90 12.34 0 8 -4 140.69 11.53 0 8 4 156.38 13.74 0 8 5 86.53 8.59 0 8 -5 90.49 7.92 0 8 5 103.45 9.85 0 8 6 132.33 11.50 0 8 -6 132.35 10.84 0 8 7 121.52 10.12 0 8 -7 102.22 9.30 0 8 8 97.90 9.24 0 8 -8 96.93 8.67 0 8 9 247.00 19.65 0 8 10 74.02 7.60 0 8 11 214.94 17.38 0 8 12 76.92 7.74 0 8 -13 112.59 8.36 0 8 -13 107.88 8.25 0 8 -13 123.22 11.65 0 8 13 102.05 9.94 0 8 -14 130.04 10.00 0 8 -14 148.31 13.42 0 8 -14 138.03 10.12 0 8 14 129.83 11.66 0 8 -15 58.43 7.80 0 8 -15 54.85 4.55 0 8 -15 58.06 4.70 0 8 -16 107.19 8.27 0 8 -16 112.22 8.39 0 8 -16 93.59 11.29 0 8 -17 6.89 1.69 0 8 -17 5.47 1.71 0 8 -17 7.29 1.91 0 8 -18 33.37 3.32 0 8 -18 36.81 3.42 0 8 -18 41.09 3.68 0 8 -19 84.25 6.83 0 8 -19 82.26 6.69 0 8 -19 84.12 6.65 0 8 -20 26.68 2.94 0 8 -20 26.92 3.22 0 8 -20 27.09 2.99 0 8 -21 3.10 1.98 0 8 -21 5.87 2.06 0 8 -21 3.16 2.33 0 8 -22 10.14 2.59 0 8 -22 8.48 2.35 0 8 -22 8.51 2.17 0 8 -23 27.80 3.69 0 8 -23 27.56 3.34 0 8 -23 28.25 3.42 0 8 -24 16.01 3.23 0 8 -24 13.51 2.88 0 8 -24 15.42 2.79 0 8 -25 10.02 2.78 0 8 -25 1.51 3.06 0 8 -25 6.03 2.59 0 8 -26 12.17 3.36 0 8 -26 5.76 2.74 0 8 -26 5.42 2.73 0 8 -27 11.79 2.98 0 8 -27 10.36 3.00 0 8 -27 9.82 3.49 0 8 -28 22.27 3.89 0 8 -28 12.33 3.19 0 8 -28 13.76 3.22 0 8 -29 52.34 5.10 0 8 -29 46.39 5.48 0 8 -30 3.10 3.38 0 8 -30 4.09 2.88 0 8 -31 11.79 3.60 0 8 -31 15.35 3.22 0 8 -32 8.32 2.82 0 8 -33 12.61 2.77 0 8 -34 -0.51 2.31 0 8 -35 6.87 2.28 0 8 -36 28.44 3.10 0 8 -37 1.20 2.05 0 8 -37 0.80 1.56 0 8 -38 -0.25 1.55 0 8 -38 2.85 1.18 0 9 0 -0.79 3.54 0 9 0 2.18 4.19 0 9 1 120.52 11.04 0 9 -1 128.10 10.99 0 9 1 115.58 11.62 0 9 2 218.00 19.48 0 9 2 237.33 18.93 0 9 -2 239.78 18.39 0 9 -3 113.23 9.20 0 9 3 115.51 11.27 0 9 3 90.26 9.71 0 9 4 177.53 15.36 0 9 4 196.02 16.74 0 9 -4 186.31 14.68 0 9 5 183.31 15.40 0 9 5 185.41 16.41 0 9 -5 183.54 14.56 0 9 6 152.32 13.52 0 9 6 142.82 12.17 0 9 -6 126.52 11.11 0 9 7 25.99 4.83 0 9 -7 28.97 3.98 0 9 7 32.69 6.59 0 9 8 168.43 13.15 0 9 -8 134.60 12.21 0 9 9 99.65 9.58 0 9 10 22.80 4.43 0 9 11 179.31 15.04 0 9 -12 5.89 1.25 0 9 -12 5.25 1.40 0 9 12 1.95 2.95 0 9 -13 53.06 4.53 0 9 -13 63.33 4.72 0 9 13 56.68 6.40 0 9 -14 29.45 2.74 0 9 -14 30.52 5.77 0 9 -14 25.56 2.55 0 9 14 27.82 4.30 0 9 -15 25.18 5.31 0 9 -15 21.77 2.26 0 9 -15 20.77 2.44 0 9 -16 63.90 5.15 0 9 -16 59.23 4.94 0 9 -17 84.21 6.76 0 9 -17 87.92 6.88 0 9 -18 48.25 4.34 0 9 -18 48.70 4.16 0 9 -18 44.75 4.11 0 9 -19 37.62 3.64 0 9 -19 35.42 3.40 0 9 -19 30.81 3.33 0 9 -20 3.48 1.93 0 9 -20 6.41 1.90 0 9 -20 2.65 2.22 0 9 -21 14.45 2.75 0 9 -21 13.71 2.48 0 9 -21 13.85 2.37 0 9 -22 28.38 3.71 0 9 -22 30.01 3.43 0 9 -22 34.31 3.55 0 9 -23 7.27 2.47 0 9 -23 3.69 2.42 0 9 -23 8.10 2.85 0 9 -24 16.25 3.07 0 9 -24 24.99 3.69 0 9 -24 21.10 3.18 0 9 -25 45.66 4.85 0 9 -25 45.29 5.14 0 9 -25 54.40 4.88 0 9 -26 1.02 3.06 0 9 -26 -1.26 2.70 0 9 -26 1.51 2.74 0 9 -27 19.76 3.36 0 9 -27 16.46 3.83 0 9 -27 23.64 3.51 0 9 -28 9.74 3.03 0 9 -28 7.67 2.97 0 9 -28 4.79 3.44 0 9 -29 10.35 3.11 0 9 -29 8.86 3.42 0 9 -30 30.35 3.93 0 9 -30 29.28 4.42 0 9 -31 51.16 5.70 0 9 -31 56.44 5.24 0 9 -32 2.42 2.71 0 9 -33 11.74 2.75 0 9 -34 30.15 3.47 0 9 -35 0.45 2.01 0 9 -36 -1.36 1.85 0 9 -37 1.86 1.93 0 9 -37 6.75 1.58 0 9 -38 11.22 1.78 0 10 0 130.79 11.84 0 10 0 121.70 11.66 0 10 1 70.17 7.97 0 10 1 68.99 8.29 0 10 -1 70.56 7.47 0 10 2 176.91 16.34 0 10 2 184.19 15.65 0 10 -2 186.03 15.04 0 10 3 173.39 16.41 0 10 3 162.50 15.14 0 10 -3 191.54 14.50 0 10 4 260.36 22.18 0 10 4 247.97 21.03 0 10 -4 268.84 20.20 0 10 5 67.22 7.83 0 10 5 65.87 9.08 0 10 -5 71.84 6.72 0 10 6 185.45 16.25 0 10 -6 165.33 13.74 0 10 6 169.93 14.68 0 10 -7 242.17 19.21 0 10 7 250.53 21.47 0 10 7 251.18 20.16 0 10 -8 89.36 8.72 0 10 8 94.41 9.50 0 10 9 24.93 4.67 0 10 9 29.09 6.40 0 10 10 158.09 13.87 0 10 11 73.42 7.56 0 10 -11 67.16 5.26 0 10 12 10.58 3.40 0 10 -12 10.22 1.65 0 10 -12 8.40 1.41 0 10 -13 78.71 6.22 0 10 13 76.21 8.04 0 10 -13 83.87 6.36 0 10 -14 -0.57 3.52 0 10 -14 -1.06 1.25 0 10 -14 -0.78 1.41 0 10 -15 36.37 3.15 0 10 -15 33.03 3.28 0 10 -16 54.09 4.68 0 10 -16 59.79 4.88 0 10 -17 23.37 2.64 0 10 -17 25.94 2.90 0 10 -18 4.95 2.11 0 10 -18 4.31 1.73 0 10 -19 10.50 2.14 0 10 -19 11.74 2.20 0 10 -19 11.80 2.41 0 10 -20 22.07 3.12 0 10 -20 19.89 2.75 0 10 -20 23.58 2.77 0 10 -21 43.37 4.13 0 10 -21 44.59 4.48 0 10 -21 43.42 4.22 0 10 -22 3.28 2.71 0 10 -22 5.99 2.34 0 10 -22 6.30 2.29 0 10 -23 65.41 5.77 0 10 -23 62.99 5.85 0 10 -23 68.60 6.14 0 10 -24 23.46 3.47 0 10 -24 27.48 3.94 0 10 -24 27.33 3.52 0 10 -25 23.98 3.40 0 10 -25 27.57 3.94 0 10 -25 19.38 3.38 0 10 -26 25.84 4.14 0 10 -26 27.54 3.78 0 10 -26 30.70 3.75 0 10 -27 11.81 3.13 0 10 -27 11.53 3.14 0 10 -27 17.82 3.78 0 10 -28 35.14 4.52 0 10 -28 30.35 4.00 0 10 -28 30.79 4.03 0 10 -29 58.02 5.59 0 10 -29 60.57 6.00 0 10 -30 1.14 3.33 0 10 -30 4.58 2.88 0 10 -31 5.81 3.24 0 10 -31 4.77 2.78 0 10 -32 33.96 3.88 0 10 -33 14.71 2.84 0 10 -34 0.75 2.22 0 10 -35 4.93 2.08 0 10 -36 27.06 2.87 0 10 -37 -1.35 1.70 0 10 -37 -0.35 1.32 0 11 0 -0.66 4.37 0 11 0 -4.11 4.03 0 11 -1 105.85 9.99 0 11 1 90.32 9.57 0 11 -1 90.16 9.13 0 11 1 82.08 10.05 0 11 -2 198.13 16.29 0 11 2 202.21 17.80 0 11 2 197.09 16.97 0 11 -3 65.14 6.70 0 11 3 67.57 7.89 0 11 3 57.36 8.88 0 11 4 333.96 27.24 0 11 -4 347.32 26.32 0 11 4 352.02 28.60 0 11 5 210.06 18.26 0 11 5 224.94 19.72 0 11 -5 216.78 17.19 0 11 6 250.36 20.43 0 11 6 237.78 21.71 0 11 -6 247.22 19.33 0 11 7 38.84 6.05 0 11 -7 39.97 4.83 0 11 7 32.13 7.12 0 11 -8 213.90 17.54 0 11 8 234.50 20.33 0 11 9 114.60 11.52 0 11 9 142.24 13.77 0 11 -10 24.55 2.30 0 11 10 28.76 6.96 0 11 10 24.22 4.81 0 11 -11 31.29 2.85 0 11 11 31.85 4.99 0 11 11 38.64 7.31 0 11 -11 29.81 2.74 0 11 12 100.25 10.03 0 11 12 99.25 12.51 0 11 -12 102.07 8.03 0 11 -12 114.02 8.17 0 11 13 -2.16 5.07 0 11 -13 3.01 1.31 0 11 -13 3.06 1.47 0 11 -14 34.39 3.20 0 11 -14 31.74 3.01 0 11 -15 22.05 2.40 0 11 -15 23.64 2.62 0 11 -16 1.40 1.55 0 11 -16 1.95 1.76 0 11 -17 96.24 7.36 0 11 -17 87.37 7.17 0 11 -18 4.16 1.86 0 11 -18 6.49 2.13 0 11 -19 89.43 7.02 0 11 -19 79.64 6.77 0 11 -19 84.90 6.83 0 11 -20 4.69 2.02 0 11 -20 5.75 2.09 0 11 -20 1.48 2.34 0 11 -21 44.53 4.35 0 11 -21 43.44 4.30 0 11 -21 49.53 4.69 0 11 -22 37.87 4.29 0 11 -22 45.06 4.36 0 11 -22 43.39 4.56 0 11 -23 61.47 5.80 0 11 -23 69.02 6.18 0 11 -23 64.67 5.84 0 11 -24 9.42 2.82 0 11 -24 8.45 3.24 0 11 -24 4.92 2.81 0 11 -25 36.35 4.37 0 11 -25 40.00 4.44 0 11 -25 40.57 4.72 0 11 -26 2.31 2.90 0 11 -26 0.47 3.25 0 11 -26 3.46 2.79 0 11 -27 49.85 5.05 0 11 -27 45.34 5.32 0 11 -27 48.73 5.02 0 11 -28 3.37 2.88 0 11 -28 4.82 3.32 0 11 -28 4.27 2.78 0 11 -29 3.37 3.29 0 11 -29 3.16 2.88 0 11 -30 38.36 5.06 0 11 -30 52.57 4.80 0 11 -31 31.28 4.03 0 11 -31 21.35 3.42 0 11 -32 11.94 2.79 0 11 -33 7.58 2.57 0 11 -34 31.96 3.49 0 11 -35 4.29 1.93 0 11 -36 3.77 1.58 0 11 -37 2.67 1.57 0 11 -37 3.14 1.20 0 12 0 206.07 17.85 0 12 0 201.19 17.47 0 12 1 30.01 6.60 0 12 -1 38.67 6.46 0 12 1 42.47 6.66 0 12 -1 39.79 5.90 0 12 -2 320.12 24.84 0 12 -2 315.10 23.57 0 12 2 271.19 24.74 0 12 2 278.46 24.18 0 12 3 131.22 15.15 0 12 3 159.33 14.43 0 12 -3 169.22 13.42 0 12 4 263.35 21.95 0 12 4 254.14 23.16 0 12 -4 269.07 20.80 0 12 5 109.18 10.35 0 12 5 92.80 11.83 0 12 -5 93.61 8.89 0 12 6 336.91 27.96 0 12 -6 355.87 26.83 0 12 6 351.35 29.49 0 12 7 106.69 12.95 0 12 -7 122.82 10.50 0 12 7 118.98 11.71 0 12 -8 179.01 14.87 0 12 8 180.89 17.61 0 12 8 179.87 15.94 0 12 9 91.66 11.07 0 12 9 90.46 9.23 0 12 -9 82.77 6.43 0 12 10 130.56 13.76 0 12 10 126.01 11.61 0 12 -10 114.19 8.81 0 12 -10 119.24 8.89 0 12 11 41.37 5.99 0 12 -11 38.70 3.46 0 12 -11 45.11 3.61 0 12 11 30.16 7.25 0 12 -12 20.84 2.34 0 12 12 24.33 6.28 0 12 -12 20.61 2.22 0 12 -13 10.97 1.74 0 12 -13 14.04 2.02 0 12 -14 86.39 6.56 0 12 -14 80.52 6.66 0 12 -15 119.75 9.06 0 12 -15 117.10 9.16 0 12 -16 7.99 1.81 0 12 -16 9.11 2.04 0 12 -17 2.67 1.97 0 12 -17 3.63 1.67 0 12 -18 -0.34 2.07 0 12 -18 3.05 1.82 0 12 -19 21.47 2.78 0 12 -19 22.10 3.05 0 12 -20 8.53 2.27 0 12 -20 6.92 2.57 0 12 -20 5.72 2.33 0 12 -21 82.38 6.60 0 12 -21 75.19 6.64 0 12 -21 77.74 6.86 0 12 -22 3.67 2.50 0 12 -22 5.70 2.94 0 12 -22 4.51 2.76 0 12 -23 89.40 7.55 0 12 -24 39.51 4.61 0 12 -24 37.59 4.27 0 12 -24 33.68 4.20 0 12 -25 129.18 10.11 0 12 -25 123.39 10.30 0 12 -25 123.42 10.10 0 12 -26 45.89 4.94 0 12 -26 46.34 5.36 0 12 -26 49.62 4.91 0 12 -27 20.49 3.50 0 12 -27 14.45 3.07 0 12 -27 10.28 3.53 0 12 -28 14.67 3.53 0 12 -28 17.53 3.28 0 12 -28 11.93 3.11 0 12 -29 11.91 3.44 0 12 -29 15.45 3.18 0 12 -30 1.15 2.69 0 12 -30 6.19 3.08 0 12 -31 -0.08 2.53 0 12 -31 2.40 2.83 0 12 -32 30.93 3.63 0 12 -33 2.13 2.22 0 12 -34 -0.62 2.02 0 12 -35 2.70 1.74 0 12 -36 12.06 1.81 0 13 0 1.53 3.86 0 13 0 1.32 4.32 0 13 1 29.43 6.23 0 13 -1 35.42 6.49 0 13 1 25.93 6.01 0 13 -1 28.42 5.36 0 13 -2 171.94 15.77 0 13 2 163.27 15.52 0 13 -2 164.95 14.40 0 13 2 177.98 16.13 0 13 3 63.81 10.39 0 13 -3 84.45 8.17 0 13 -3 86.14 10.01 0 13 3 81.26 9.57 0 13 -4 493.73 35.88 0 13 4 468.17 37.11 0 13 4 432.78 38.03 0 13 5 111.33 13.34 0 13 5 122.24 11.98 0 13 -5 117.21 10.49 0 13 6 235.34 20.08 0 13 6 217.40 21.39 0 13 -6 237.74 18.68 0 13 -7 197.54 16.93 0 13 7 194.57 19.82 0 13 7 191.26 18.22 0 13 -7 215.54 15.42 0 13 8 72.21 10.26 0 13 -8 64.23 7.04 0 13 -8 70.90 5.44 0 13 8 66.52 8.39 0 13 -9 96.30 7.14 0 13 9 90.96 10.07 0 13 -9 92.06 7.17 0 13 9 73.54 11.24 0 13 10 73.72 10.39 0 13 -10 74.92 5.58 0 13 10 63.80 8.19 0 13 -10 66.75 5.59 0 13 -11 26.11 2.73 0 13 11 25.92 6.90 0 13 -11 28.32 2.67 0 13 12 210.53 21.52 0 13 -12 227.86 16.59 0 13 -12 222.05 16.51 0 13 -13 27.00 2.94 0 13 -13 31.09 2.87 0 13 -14 17.44 2.37 0 13 -14 16.33 2.23 0 13 -15 12.50 2.28 0 13 -15 11.73 1.97 0 13 -16 6.14 1.78 0 13 -16 5.01 2.01 0 13 -17 53.90 4.88 0 13 -17 53.86 4.68 0 13 -18 34.79 3.75 0 13 -18 34.67 3.53 0 13 -19 84.74 7.18 0 13 -19 87.32 7.03 0 13 -20 1.99 2.54 0 13 -20 1.00 2.36 0 13 -20 -2.03 2.17 0 13 -21 109.66 9.01 0 13 -21 109.89 8.82 0 13 -21 108.34 8.79 0 13 -22 33.77 4.00 0 13 -22 28.43 4.18 0 13 -22 32.25 3.86 0 13 -23 121.68 10.22 0 13 -23 123.63 10.03 0 13 -23 130.63 10.07 0 13 -24 37.85 4.39 0 13 -24 40.18 4.85 0 13 -24 40.14 4.60 0 13 -25 69.04 6.12 0 13 -25 64.21 6.32 0 13 -25 64.35 6.16 0 13 -26 13.13 3.08 0 13 -26 7.29 3.15 0 13 -26 7.78 3.35 0 13 -27 42.23 4.40 0 13 -27 32.27 4.10 0 13 -27 34.33 4.64 0 13 -28 7.19 2.75 0 13 -28 10.90 3.07 0 13 -28 10.74 3.28 0 13 -29 0.75 2.78 0 13 -29 3.03 3.01 0 13 -30 17.43 3.39 0 13 -30 15.05 2.99 0 13 -31 4.03 2.48 0 13 -32 3.21 2.37 0 13 -33 4.00 2.15 0 13 -34 20.54 2.63 0 13 -35 1.74 1.63 0 13 -36 -0.71 1.18 0 14 0 145.34 14.17 0 14 0 139.84 13.36 0 14 1 20.04 5.47 0 14 -1 10.68 4.10 0 14 1 4.10 4.86 0 14 -1 10.60 5.08 0 14 -2 184.37 14.86 0 14 2 145.82 15.73 0 14 -2 188.66 16.50 0 14 2 162.47 16.04 0 14 3 25.71 6.98 0 14 -3 32.02 6.50 0 14 3 23.05 6.19 0 14 -3 30.05 4.75 0 14 4 90.40 10.98 0 14 -4 113.40 11.89 0 14 4 102.53 8.16 0 14 -4 114.18 8.06 0 14 4 72.37 11.58 0 14 -4 102.38 9.77 0 14 -5 131.84 8.90 0 14 5 107.00 12.03 0 14 5 103.90 12.96 0 14 5 104.35 8.96 0 14 -5 120.28 10.59 0 14 -6 143.71 13.48 0 14 6 146.53 16.36 0 14 6 148.36 15.04 0 14 -6 168.01 12.00 0 14 -7 87.80 6.66 0 14 7 74.71 11.07 0 14 7 81.69 9.69 0 14 -7 85.76 8.33 0 14 8 154.41 15.91 0 14 -8 180.18 13.06 0 14 8 156.75 17.56 0 14 -9 68.09 4.85 0 14 -9 52.63 4.77 0 14 9 45.68 8.81 0 14 -10 107.83 7.52 0 14 -10 89.28 7.48 0 14 10 77.64 11.75 0 14 -11 51.31 4.21 0 14 -11 48.77 4.26 0 14 11 41.27 8.45 0 14 -12 59.04 5.15 0 14 -12 65.80 5.12 0 14 -13 48.24 4.14 0 14 -13 44.04 3.97 0 14 -14 67.48 5.79 0 14 -14 72.06 5.70 0 14 -15 40.04 4.00 0 14 -15 44.78 3.92 0 14 -16 45.27 4.37 0 14 -16 44.51 4.11 0 14 -17 49.04 4.50 0 14 -17 51.47 4.72 0 14 -18 5.91 2.02 0 14 -18 3.61 2.38 0 14 -19 19.09 2.92 0 14 -19 23.37 3.26 0 14 -20 40.77 4.35 0 14 -20 41.37 4.15 0 14 -20 37.71 4.45 0 14 -21 129.80 10.27 0 14 -21 130.24 10.27 0 14 -21 129.38 10.44 0 14 -22 27.35 3.44 0 14 -22 23.79 3.72 0 14 -22 19.54 3.68 0 14 -23 109.46 9.36 0 14 -23 112.01 9.14 0 14 -23 116.23 9.27 0 14 -24 18.27 3.49 0 14 -24 19.11 3.89 0 14 -24 29.50 3.87 0 14 -25 89.49 7.55 0 14 -25 94.08 7.67 0 14 -25 80.53 7.76 0 14 -26 48.09 4.89 0 14 -26 51.92 5.27 0 14 -26 45.56 5.05 0 14 -27 3.11 2.98 0 14 -27 8.59 2.70 0 14 -27 6.87 2.92 0 14 -28 6.65 2.63 0 14 -28 9.23 3.08 0 14 -28 5.55 2.88 0 14 -29 8.96 2.95 0 14 -29 6.84 2.69 0 14 -30 2.75 2.71 0 14 -30 -3.27 2.59 0 14 -31 3.67 2.43 0 14 -32 12.19 2.48 0 14 -33 1.43 1.95 0 14 -34 -0.94 1.78 0 14 -35 2.25 1.42 0 15 0 0.89 1.23 0 15 0 2.53 3.64 0 15 0 -0.55 4.27 0 15 -1 4.51 4.21 0 15 1 4.27 1.42 0 15 1 -0.55 4.16 0 15 -1 -4.88 3.68 0 15 1 -2.85 4.13 0 15 -1 4.00 1.28 0 15 2 17.50 5.65 0 15 2 27.87 2.68 0 15 -2 28.48 4.77 0 15 -2 30.02 6.12 0 15 -2 26.87 2.57 0 15 2 31.96 6.27 0 15 3 25.84 3.03 0 15 3 38.67 6.85 0 15 -3 38.24 2.96 0 15 3 33.31 6.76 0 15 -3 29.68 6.33 0 15 -3 33.47 4.87 0 15 -4 114.73 13.25 0 15 -4 135.06 9.47 0 15 4 97.67 13.28 0 15 4 119.63 9.53 0 15 4 121.73 12.89 0 15 5 20.35 6.28 0 15 5 36.34 3.44 0 15 5 35.06 6.44 0 15 -5 29.27 7.04 0 15 -5 40.34 3.27 0 15 6 72.55 9.43 0 15 6 59.59 10.24 0 15 6 70.95 6.24 0 15 -6 87.90 6.18 0 15 -7 58.36 4.65 0 15 7 52.03 8.98 0 15 7 51.78 7.66 0 15 8 3.94 4.93 0 15 -8 9.27 1.58 0 15 -9 60.86 4.77 0 15 9 30.34 8.48 0 15 -10 195.63 13.53 0 15 -10 174.31 13.50 0 15 -11 33.33 3.24 0 15 -11 33.85 3.18 0 15 -12 63.77 5.49 0 15 -12 70.17 5.47 0 15 -13 4.11 1.70 0 15 -13 0.87 1.60 0 15 -14 26.23 2.99 0 15 -14 26.06 2.92 0 15 -15 170.73 12.08 0 15 -15 146.95 12.10 0 15 -16 16.60 2.76 0 15 -16 20.18 2.62 0 15 -17 5.16 2.18 0 15 -17 3.35 1.96 0 15 -18 53.29 5.13 0 15 -18 53.76 4.96 0 15 -19 117.49 9.89 0 15 -19 130.18 9.83 0 15 -20 8.93 2.63 0 15 -20 12.34 3.09 0 15 -20 8.45 3.14 0 15 -21 38.61 4.29 0 15 -21 35.84 4.28 0 15 -21 36.83 4.09 0 15 -22 8.10 3.21 0 15 -22 4.50 2.66 0 15 -22 2.76 3.04 0 15 -23 117.15 9.21 0 15 -23 108.11 9.31 0 15 -23 113.01 9.25 0 15 -24 43.89 5.10 0 15 -24 50.90 4.85 0 15 -24 47.32 5.07 0 15 -25 24.23 3.51 0 15 -25 25.08 3.85 0 15 -25 25.08 3.82 0 15 -26 9.54 3.04 0 15 -26 13.84 2.87 0 15 -26 8.64 3.17 0 15 -27 4.10 2.50 0 15 -27 4.85 2.80 0 15 -27 5.58 2.79 0 15 -28 5.27 2.75 0 15 -28 6.76 2.67 0 15 -28 6.42 2.44 0 15 -29 2.29 2.54 0 15 -29 1.23 2.71 0 15 -30 9.16 2.56 0 15 -31 0.63 2.19 0 15 -32 3.67 2.07 0 15 -33 3.42 1.85 0 15 -34 2.17 1.56 0 15 -35 3.31 1.23 0 16 0 60.31 4.85 0 16 0 50.17 8.29 0 16 1 2.49 1.41 0 16 -1 5.73 1.47 0 16 1 7.33 4.72 0 16 -1 8.82 4.83 0 16 2 18.71 5.57 0 16 -2 19.30 5.56 0 16 2 20.36 2.31 0 16 -2 20.95 2.22 0 16 -3 28.35 2.51 0 16 3 21.50 5.76 0 16 3 22.77 2.58 0 16 -3 33.63 6.48 0 16 -4 6.11 4.80 0 16 4 4.74 4.24 0 16 -4 6.24 1.40 0 16 4 6.01 1.62 0 16 4 -0.66 4.64 0 16 5 29.40 6.13 0 16 -5 40.88 3.38 0 16 5 41.03 7.74 0 16 5 35.41 3.52 0 16 6 29.35 7.55 0 16 -6 40.74 3.42 0 16 6 36.49 3.60 0 16 7 50.24 4.44 0 16 -7 52.19 4.25 0 16 -8 183.79 13.67 0 16 -9 12.45 1.99 0 16 -10 10.44 1.83 0 16 -11 12.86 1.92 0 16 -11 9.46 1.96 0 16 -12 16.56 2.42 0 16 -12 21.03 2.40 0 16 -13 74.15 5.84 0 16 -13 66.96 5.81 0 16 -14 6.90 2.12 0 16 -14 13.17 2.18 0 16 -15 0.46 1.85 0 16 -15 1.67 1.88 0 16 -16 20.26 3.10 0 16 -16 26.96 3.01 0 16 -17 140.41 10.52 0 16 -17 128.76 10.54 0 16 -18 16.05 3.03 0 16 -18 19.33 2.84 0 16 -19 2.62 2.45 0 16 -19 5.83 2.46 0 16 -20 43.49 4.50 0 16 -20 30.61 4.34 0 16 -20 43.56 4.21 0 16 -21 89.26 8.21 0 16 -21 105.88 8.30 0 16 -21 100.07 8.10 0 16 -22 19.61 3.13 0 16 -22 21.48 3.60 0 16 -22 13.02 3.31 0 16 -23 27.86 4.06 0 16 -23 26.94 3.65 0 16 -23 29.64 3.93 0 16 -24 2.57 2.79 0 16 -24 11.00 3.34 0 16 -24 4.01 2.59 0 16 -25 28.83 3.81 0 16 -25 25.17 3.53 0 16 -25 29.58 3.82 0 16 -26 10.34 2.75 0 16 -26 18.32 3.19 0 16 -26 12.54 3.09 0 16 -27 7.19 2.74 0 16 -27 1.34 2.66 0 16 -27 3.48 2.28 0 16 -28 6.20 2.32 0 16 -28 5.44 2.56 0 16 -28 4.98 2.64 0 16 -29 -4.25 2.50 0 16 -29 0.08 2.39 0 16 -30 0.86 2.22 0 16 -31 3.72 2.16 0 16 -32 1.21 1.83 0 16 -33 3.10 1.71 0 16 -34 4.26 1.48 0 17 0 -0.91 1.41 0 17 0 -2.06 4.11 0 17 1 14.25 5.51 0 17 1 21.84 2.42 0 17 -1 21.10 2.28 0 17 -1 9.78 4.94 0 17 -2 42.73 3.71 0 17 2 44.34 3.82 0 17 3 4.93 1.61 0 17 -3 5.03 1.42 0 17 4 22.24 2.63 0 17 -4 26.07 2.53 0 17 -5 73.15 5.60 0 17 5 65.11 5.67 0 17 -6 35.60 3.28 0 17 6 35.04 3.45 0 17 7 43.87 4.19 0 17 -7 48.08 4.04 0 17 -8 56.08 4.72 0 17 8 56.54 4.90 0 17 9 36.66 3.60 0 17 -9 35.85 3.46 0 17 -10 82.36 6.59 0 17 -11 11.17 2.04 0 17 -12 11.49 2.16 0 17 -13 15.11 2.27 0 17 -14 2.34 1.80 0 17 -14 0.08 1.86 0 17 -15 113.11 9.59 0 17 -15 133.35 9.62 0 17 -16 17.03 2.64 0 17 -16 15.40 2.73 0 17 -17 11.07 2.54 0 17 -17 9.39 2.46 0 17 -18 28.33 3.80 0 17 -18 37.86 3.74 0 17 -19 67.44 6.34 0 17 -19 77.39 6.33 0 17 -20 13.07 3.00 0 17 -20 18.70 2.94 0 17 -21 6.59 2.54 0 17 -21 3.26 2.58 0 17 -21 2.90 3.06 0 17 -22 17.46 3.02 0 17 -22 19.82 3.29 0 17 -22 21.47 3.58 0 17 -23 20.17 3.69 0 17 -23 17.80 3.35 0 17 -23 26.07 3.29 0 17 -24 15.39 3.25 0 17 -24 11.23 2.91 0 17 -24 11.38 2.65 0 17 -25 0.78 2.79 0 17 -25 3.57 2.54 0 17 -25 4.22 2.38 0 17 -26 -1.27 2.23 0 17 -26 2.45 2.53 0 17 -26 0.08 2.70 0 17 -27 0.98 2.40 0 17 -27 3.50 2.61 0 17 -27 -2.08 2.15 0 17 -28 1.28 2.26 0 17 -28 2.79 2.46 0 17 -29 0.07 2.35 0 17 -30 1.70 2.17 0 17 -31 6.53 2.12 0 17 32 4.84 1.09 0 17 -32 1.05 1.74 0 17 -33 4.99 1.62 0 18 0 61.30 5.06 0 18 1 11.52 1.89 0 18 -1 13.85 2.00 0 18 2 1.87 1.55 0 18 -2 3.24 1.47 0 18 3 20.36 2.41 0 18 -3 18.87 2.27 0 18 4 5.08 1.74 0 18 -4 6.26 1.59 0 18 5 28.75 3.39 0 18 -5 38.67 3.29 0 18 6 131.04 10.49 0 18 -6 142.71 10.43 0 18 -7 62.54 5.18 0 18 7 61.07 5.26 0 18 8 83.01 6.96 0 18 -8 88.54 6.86 0 18 9 42.71 4.32 0 18 -9 52.26 4.29 0 18 10 42.52 4.06 0 18 -10 41.88 3.89 0 18 -11 8.95 2.03 0 18 11 9.16 2.17 0 18 -12 12.43 2.18 0 18 -13 10.61 2.19 0 18 -14 0.08 1.93 0 18 -15 25.36 2.93 0 18 -15 18.43 2.79 0 18 -16 12.25 2.60 0 18 -16 14.91 2.56 0 18 -17 78.13 6.28 0 18 -17 68.22 6.20 0 18 -18 28.64 3.75 0 18 -18 41.92 3.92 0 18 -19 -3.06 2.30 0 18 -19 -1.17 2.35 0 18 -20 34.75 4.16 0 18 -20 44.81 4.21 0 18 -21 10.68 3.32 0 18 -21 6.46 2.51 0 18 -21 8.83 2.53 0 18 -22 11.88 2.76 0 18 -22 14.35 3.41 0 18 -22 10.06 2.63 0 18 -23 -0.56 2.26 0 18 -23 -1.11 2.44 0 18 -23 2.88 3.07 0 18 -24 -0.37 2.15 0 18 -24 -3.96 3.04 0 18 -24 -1.29 2.38 0 18 -25 4.53 2.82 0 18 -25 3.68 2.42 0 18 -25 7.93 2.33 0 18 -26 2.21 2.08 0 18 -26 4.85 2.67 0 18 -26 2.59 2.22 0 18 -27 0.26 2.18 0 18 -27 6.55 2.07 0 18 -27 7.53 2.63 0 18 -28 -1.63 2.31 0 18 -29 4.49 2.22 0 18 -30 1.46 2.00 0 18 30 1.24 1.19 0 18 -31 0.34 1.78 0 18 -32 0.55 1.56 0 18 -33 1.75 1.26 0 19 0 0.81 1.49 0 19 -1 9.92 1.88 0 19 1 10.77 1.91 0 19 -2 36.04 3.20 0 19 2 29.64 3.18 0 19 -3 2.09 1.57 0 19 3 1.56 1.64 0 19 4 20.80 2.69 0 19 -4 27.60 2.70 0 19 5 17.81 2.53 0 19 -5 22.46 2.49 0 19 -6 10.16 1.98 0 19 6 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12 -29 12.44 3.44 1 12 -28 15.12 3.63 1 12 -28 16.66 3.36 1 12 -27 28.67 3.92 1 12 -27 23.97 4.18 1 12 -27 27.33 3.75 1 12 -26 55.49 5.60 1 12 -26 49.11 5.32 1 12 -26 51.83 5.17 1 12 -25 2.90 3.07 1 12 -25 2.35 2.71 1 12 -25 8.51 3.28 1 12 -24 49.29 5.14 1 12 -24 44.07 4.71 1 12 -24 51.64 5.07 1 12 -23 31.76 4.15 1 12 -23 32.49 3.90 1 12 -23 35.86 4.08 1 12 -22 101.65 8.38 1 12 -22 98.81 8.14 1 12 -21 18.84 2.88 1 12 -21 21.70 3.25 1 12 -20 37.90 3.80 1 12 -20 28.92 3.48 1 12 -19 3.98 1.95 1 12 -19 4.02 2.24 1 12 -18 38.99 3.81 1 12 -18 35.99 3.63 1 12 -17 12.48 2.34 1 12 -17 11.20 1.99 1 12 -16 24.31 2.81 1 12 -16 23.41 2.61 1 12 -15 4.88 1.52 1 12 -15 4.77 1.77 1 12 -14 36.24 3.42 1 12 -14 42.62 3.62 1 12 -13 115.93 8.68 1 12 -13 112.84 8.75 1 12 -12 39.63 7.25 1 12 -12 38.10 3.34 -1 12 12 29.15 7.47 1 12 -12 42.02 3.48 -1 12 12 32.32 5.92 1 12 -11 17.49 2.00 -1 12 11 22.62 6.71 1 12 -11 17.71 1.93 -1 12 11 17.55 4.79 1 12 -10 70.76 5.51 -1 12 10 65.88 8.37 -1 12 9 114.17 13.79 -1 12 9 125.11 12.22 -1 12 8 73.45 9.13 -1 12 8 91.28 11.53 -1 12 7 425.01 35.46 -1 12 7 422.48 33.69 -1 12 6 258.60 23.05 1 12 -6 287.65 21.09 -1 12 6 256.41 24.46 -1 12 5 222.15 19.11 1 12 -5 215.03 16.94 -1 12 5 234.17 20.91 -1 12 4 12.13 6.92 1 12 -4 7.73 2.63 -1 12 4 5.42 4.71 1 12 -3 423.85 30.45 -1 12 3 376.23 32.13 -1 12 3 390.15 33.29 1 12 -2 186.06 14.00 -1 12 2 170.56 15.77 -1 12 2 133.14 16.12 -1 12 1 98.48 11.67 -1 12 1 108.08 11.35 1 12 -1 114.33 9.95 -1 12 0 68.75 8.57 -1 12 0 73.39 8.70 1 12 0 51.46 6.97 1 12 0 64.97 7.85 1 12 1 127.17 11.68 1 12 1 119.17 11.51 -1 12 -1 110.91 12.10 -1 12 -1 117.27 11.80 -1 12 -2 109.44 11.07 1 12 2 97.00 10.93 1 12 2 97.98 10.44 -1 12 -2 101.24 10.15 1 12 3 371.75 29.67 1 12 3 352.89 30.24 -1 12 -3 372.65 30.47 -1 12 -3 401.93 29.55 -1 12 -4 130.14 12.53 1 12 4 112.29 12.46 -1 12 -4 120.37 11.00 1 12 4 113.08 11.32 1 12 5 177.16 16.85 -1 12 -5 178.17 15.08 1 12 6 82.91 10.38 1 12 6 84.21 9.03 -1 12 -6 89.24 8.63 -1 12 -7 44.16 3.56 1 12 7 43.41 6.12 -1 12 -7 35.46 5.41 1 12 7 37.33 7.55 -1 12 -8 139.51 12.98 1 12 8 137.35 14.81 1 12 8 138.06 13.10 -1 12 -8 153.04 11.07 1 12 9 21.91 4.34 -1 12 -9 24.27 2.36 1 12 9 25.52 6.33 -1 12 -9 24.82 2.44 -1 12 -9 26.16 4.41 -1 12 -10 17.65 2.13 1 12 10 21.24 5.95 -1 12 -10 19.82 2.04 -1 12 -10 14.48 3.81 1 12 10 18.94 3.94 -1 12 -11 93.94 7.12 1 12 11 93.52 11.25 -1 12 -11 89.16 7.01 1 12 12 4.87 4.66 -1 12 -12 4.43 1.59 -1 12 -12 5.42 1.39 -1 12 -13 25.61 2.78 -1 12 -13 26.37 2.61 1 12 13 25.80 6.37 -1 12 -14 30.95 3.06 -1 12 -14 28.48 2.86 -1 12 -15 30.16 3.13 -1 12 -15 28.40 2.94 -1 12 -16 72.18 5.66 -1 12 -16 62.11 5.46 -1 12 -17 9.01 1.96 -1 12 -17 8.41 2.17 -1 12 -18 26.79 3.21 -1 12 -18 26.92 3.10 -1 12 -19 2.73 2.10 -1 12 -19 0.09 2.34 -1 12 -20 168.70 12.62 -1 12 -20 159.17 12.44 -1 12 -20 161.65 12.39 -1 12 -21 7.50 2.52 -1 12 -21 6.83 2.69 -1 12 -21 8.24 2.94 -1 12 -22 179.14 13.26 -1 12 -22 173.15 13.33 -1 12 -22 166.75 13.48 -1 12 -23 39.51 4.32 -1 12 -23 33.70 4.21 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98.27 8.36 1 13 -24 106.76 8.58 1 13 -24 101.40 8.64 1 13 -23 6.43 3.06 1 13 -23 7.36 2.56 1 13 -22 49.18 5.12 1 13 -22 49.41 4.71 1 13 -21 9.79 2.97 1 13 -21 11.32 2.55 1 13 -20 11.81 2.59 1 13 -20 5.11 2.18 1 13 -19 2.07 2.22 1 13 -19 3.03 1.96 1 13 -18 48.40 4.58 1 13 -18 48.00 4.36 1 13 -17 7.35 2.21 1 13 -17 4.91 1.86 1 13 -16 54.59 4.94 1 13 -16 57.61 4.79 1 13 -15 72.39 5.94 1 13 -15 76.33 6.09 1 13 -14 51.61 4.61 1 13 -14 56.26 4.55 1 13 -13 18.24 2.09 1 13 -13 17.32 2.22 1 13 -12 22.97 2.43 1 13 -12 21.18 2.30 1 13 -11 158.81 12.07 1 13 -11 165.55 12.04 -1 13 11 155.42 17.39 1 13 -10 150.78 11.08 -1 13 10 147.14 16.30 -1 13 10 133.54 14.12 1 13 -9 154.65 11.51 -1 13 9 146.34 16.43 -1 13 9 172.71 15.15 -1 13 8 134.82 13.37 -1 13 8 134.69 15.10 -1 13 7 157.69 14.11 -1 13 7 121.74 14.94 -1 13 6 32.07 8.05 1 13 -6 39.07 4.49 -1 13 6 46.18 7.15 -1 13 5 339.92 31.59 1 13 -5 383.62 28.27 -1 13 5 380.44 30.58 -1 13 4 154.12 11.88 -1 13 4 148.72 14.97 1 13 -4 176.76 12.94 -1 13 4 155.40 16.48 -1 13 3 120.57 13.56 -1 13 3 104.83 12.43 1 13 -3 136.03 10.63 -1 13 2 -4.34 5.73 -1 13 2 3.26 4.76 1 13 -2 8.58 3.13 1 13 -1 166.55 15.25 -1 13 1 147.73 15.68 -1 13 1 174.10 15.78 1 13 -1 168.57 13.95 -1 13 0 127.72 13.18 -1 13 0 150.46 13.68 1 13 0 121.62 12.02 1 13 0 133.19 13.05 -1 13 -1 338.77 27.67 1 13 1 357.42 27.81 1 13 1 326.05 27.26 -1 13 -1 354.51 28.34 -1 13 -2 117.17 11.65 1 13 2 102.18 10.88 -1 13 -2 107.54 10.64 1 13 2 86.74 10.71 1 13 3 50.16 7.96 1 13 3 70.33 7.97 -1 13 -3 62.95 8.61 -1 13 -3 56.19 7.11 -1 13 -4 122.21 11.86 -1 13 -4 158.87 14.14 1 13 4 98.50 12.81 1 13 4 104.18 12.04 -1 13 -4 135.50 9.73 1 13 5 145.53 15.10 -1 13 -5 181.03 12.79 -1 13 -5 159.45 16.36 -1 13 -5 157.99 14.71 1 13 5 162.01 16.52 1 13 6 126.54 13.31 -1 13 -6 154.86 10.96 -1 13 -6 118.66 12.68 1 13 6 148.18 14.96 1 13 7 119.34 11.99 1 13 7 123.88 13.66 -1 13 -7 129.50 11.63 -1 13 -7 129.11 9.59 1 13 8 40.81 6.27 -1 13 -8 44.74 6.10 -1 13 -8 59.71 4.27 1 13 8 48.47 8.24 -1 13 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16 -23 4.14 2.70 1 16 -23 0.86 2.28 1 16 -22 23.60 3.15 1 16 -22 19.35 3.33 1 16 -21 8.16 2.80 1 16 -21 13.26 2.60 1 16 -20 84.29 6.73 1 16 -20 74.62 6.81 1 16 -19 16.29 3.11 1 16 -19 25.36 3.08 1 16 -18 12.40 2.65 1 16 -18 13.73 2.48 1 16 -17 13.60 2.47 1 16 -17 15.62 2.58 1 16 -16 101.41 8.89 1 16 -16 126.19 8.93 1 16 -15 16.67 2.49 1 16 -15 19.53 2.46 1 16 -14 4.23 1.69 1 16 -13 46.94 4.13 1 16 -12 20.98 2.40 1 16 -11 81.34 6.42 1 16 -10 17.17 2.08 1 16 -9 7.26 1.50 1 16 -8 90.15 6.97 1 16 -7 98.49 7.62 -1 16 7 104.13 7.92 -1 16 6 18.78 6.16 -1 16 6 17.66 5.33 -1 16 6 17.68 2.50 -1 16 5 10.07 4.20 -1 16 5 8.17 1.90 -1 16 5 7.74 4.66 1 16 -4 32.91 6.58 -1 16 4 18.18 6.33 -1 16 4 37.74 3.33 -1 16 4 27.78 6.23 1 16 -3 -1.27 4.15 -1 16 3 -0.68 4.47 -1 16 3 0.34 1.58 -1 16 3 2.54 4.09 -1 16 2 17.54 2.27 1 16 -2 22.25 5.74 -1 16 2 13.19 5.08 -1 16 2 16.61 5.28 -1 16 1 48.87 4.14 1 16 -1 48.84 7.52 -1 16 1 38.09 7.47 -1 16 1 38.08 6.96 -1 16 0 37.94 7.13 -1 16 0 32.72 3.07 -1 16 0 24.31 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5.11 1.41 2 -29 -14 5.77 1.55 2 -29 -13 -2.23 1.59 2 -29 -12 4.06 1.71 2 -29 -11 5.25 1.83 -2 -29 11 6.78 2.08 -2 -29 10 26.16 3.16 2 -29 -10 26.14 2.86 -2 -29 9 1.80 2.63 2 -29 -9 2.70 1.91 -2 -29 8 6.28 3.03 2 -29 -8 10.14 2.17 -2 -29 7 15.01 3.43 2 -29 -7 14.69 2.47 2 -29 -6 15.46 2.58 -2 -29 6 23.37 3.94 -2 -29 5 6.92 3.80 2 -29 -5 3.16 2.10 2 -29 -4 0.07 1.96 -2 -29 4 3.91 4.14 2 -29 -3 5.20 2.09 -2 -29 3 1.25 4.50 -2 -29 2 13.14 4.68 2 -29 -2 14.29 2.48 2 -29 -1 2.26 2.06 -2 -29 1 -1.38 4.44 2 -29 0 4.88 2.16 -2 -29 0 7.14 4.53 -2 -29 -1 3.44 4.35 2 -29 1 0.27 1.99 2 -29 2 33.64 3.64 -2 -29 -2 39.64 4.87 -2 -29 -3 2.23 3.54 2 -29 3 6.47 2.23 2 -29 4 14.80 2.46 -2 -29 -4 12.40 3.36 2 -29 5 3.47 1.98 -2 -29 -5 5.18 2.70 -2 -29 -5 2.94 2.32 -2 -29 -6 13.99 2.61 2 -29 6 8.87 2.26 -2 -29 -6 9.68 2.53 2 -29 7 11.20 2.24 -2 -29 -7 13.58 2.49 -2 -29 -7 9.54 2.47 2 -29 8 18.33 2.55 -2 -29 -8 18.53 2.80 -2 -29 -8 16.65 2.61 2 -29 9 14.85 2.29 -2 -29 -9 9.47 2.45 -2 -29 -9 12.96 2.22 -2 -29 -10 1.98 2.07 2 -29 10 4.92 1.86 -2 -29 -10 8.36 1.91 -2 -29 -11 41.39 3.89 2 -29 11 36.10 3.75 -2 -29 -11 45.83 3.72 -2 -29 -12 7.24 1.75 -2 -29 -12 6.63 2.05 2 -29 13 6.14 1.61 -2 -29 -13 3.20 1.51 -2 -29 -13 3.61 1.68 -2 -29 -14 2.07 1.62 -2 -29 -14 -0.75 1.24 -2 -29 -15 7.12 1.70 -2 -29 -15 7.26 1.36 -2 -29 -16 13.72 1.53 -2 -29 -16 9.64 1.72 -2 -29 -17 16.52 1.64 -2 -29 -17 14.79 1.83 -2 -29 -18 8.39 1.34 -2 -29 -19 0.53 0.85 2 -28 -21 2.25 0.83 2 -28 -20 1.11 1.01 2 -28 -19 3.48 1.20 2 -28 -18 1.28 1.25 2 -28 -17 9.18 1.72 -2 -28 16 1.94 1.80 2 -28 -16 1.76 1.54 2 -28 -15 1.29 1.60 2 -28 -14 -0.23 1.70 2 -28 -13 2.98 1.93 -2 -28 13 3.16 2.00 -2 -28 12 31.49 3.47 2 -28 -12 30.39 3.28 2 -28 -11 4.85 2.11 -2 -28 11 5.05 2.66 2 -28 -10 13.66 2.57 -2 -28 10 16.32 3.34 -2 -28 9 5.18 3.30 2 -28 -9 4.44 2.31 2 -28 -8 17.92 2.78 -2 -28 8 23.43 3.97 -2 -28 7 -3.36 3.89 2 -28 -7 -0.54 1.51 2 -28 -7 -0.21 2.14 2 -28 -6 2.47 1.58 -2 -28 6 3.90 4.42 2 -28 -6 0.07 2.23 2 -28 -5 16.41 2.28 -2 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22.19 3.11 -2 -28 -11 31.47 3.38 -2 -28 -11 29.61 3.04 -2 -28 -12 10.68 2.12 2 -28 12 5.90 2.10 -2 -28 -12 6.06 2.33 2 -28 13 36.43 3.84 -2 -28 -13 40.46 3.97 -2 -28 -13 46.72 3.80 2 -28 14 17.18 2.40 -2 -28 -14 17.64 2.56 -2 -28 -14 18.20 2.30 -2 -28 -15 10.24 2.05 -2 -28 -15 8.81 1.80 -2 -28 -16 -0.31 1.68 -2 -28 -16 0.44 1.40 -2 -28 -17 4.57 1.36 -2 -28 -17 6.60 1.65 -2 -28 -18 9.18 1.36 -2 -28 -18 6.46 1.60 -2 -28 -19 17.28 2.04 -2 -28 -19 20.91 1.91 -2 -28 -20 12.12 1.33 -2 -28 -20 12.60 1.54 -2 -28 -21 1.98 0.82 2 -27 -22 3.00 1.01 2 -27 -21 4.47 1.23 -2 -27 20 1.97 0.98 2 -27 -20 5.94 1.42 2 -27 -19 6.00 1.58 -2 -27 19 3.30 1.12 -2 -27 18 2.87 1.12 2 -27 -18 4.87 1.58 2 -27 -17 6.73 1.84 2 -27 -16 5.39 1.93 2 -27 -15 12.49 2.30 2 -27 -14 3.20 2.02 -2 -27 14 3.30 2.16 -2 -27 13 11.69 2.73 2 -27 -13 5.37 2.20 2 -27 -12 1.03 1.25 -2 -27 12 0.72 2.71 2 -27 -12 -1.33 2.19 2 -27 -11 5.54 1.48 -2 -27 11 7.19 3.15 2 -27 -11 4.12 2.38 2 -27 -10 31.48 3.48 2 -27 -10 27.42 2.76 -2 -27 10 31.55 4.29 2 -27 -9 6.74 1.61 -2 -27 9 5.16 3.79 2 -27 -9 7.42 2.44 2 -27 -8 16.24 2.84 -2 -27 8 18.01 4.48 2 -27 -8 17.65 2.16 2 -27 -7 14.05 2.68 -2 -27 7 20.15 4.99 2 -27 -7 14.23 2.05 2 -27 -6 5.45 2.37 2 -27 -6 3.60 1.64 -2 -27 6 3.33 4.95 2 -27 -5 5.21 1.78 -2 -27 5 6.52 5.36 2 -27 -5 5.91 2.45 -2 -27 4 5.02 5.50 2 -27 -4 3.98 1.73 2 -27 -4 0.08 2.40 -2 -27 3 8.76 5.33 2 -27 -3 10.65 2.13 2 -27 -3 11.76 2.61 2 -27 -2 6.39 2.02 -2 -27 2 6.44 4.91 2 -27 -2 6.69 2.50 2 -27 -1 8.52 2.59 2 -27 -1 8.74 2.19 -2 -27 1 5.71 4.31 -2 -27 0 1.81 3.79 2 -27 0 3.04 2.39 2 -27 0 5.64 2.22 2 -27 1 1.65 2.34 -2 -27 -1 -1.88 3.18 2 -27 1 0.51 2.20 2 -27 2 9.31 2.46 -2 -27 -2 15.49 3.06 2 -27 2 7.51 2.56 2 -27 3 12.46 2.71 2 -27 3 13.73 2.54 -2 -27 -3 11.35 2.75 -2 -27 -4 13.52 2.58 2 -27 4 12.52 2.62 2 -27 4 5.09 2.25 -2 -27 -4 9.80 2.92 2 -27 5 11.13 2.21 -2 -27 -5 9.71 2.84 -2 -27 -5 8.31 2.41 2 -27 5 10.42 2.59 2 -27 6 4.97 2.32 2 -27 6 -0.13 1.79 -2 -27 -6 2.16 2.21 -2 -27 -6 0.73 2.56 2 -27 7 2.35 1.73 2 -27 7 0.73 2.32 -2 -27 -7 4.69 2.18 -2 -27 -7 0.24 2.60 2 -27 8 29.79 3.42 -2 -27 -8 27.31 3.26 -2 -27 -8 25.86 3.55 2 -27 8 26.45 2.90 -2 -27 -9 33.68 3.54 -2 -27 -9 31.54 3.78 2 -27 9 30.63 3.19 2 -27 9 33.15 3.61 -2 -27 -10 1.43 2.62 2 -27 10 3.56 1.64 -2 -27 -10 4.27 2.23 2 -27 10 3.54 2.41 -2 -27 -11 49.19 4.82 -2 -27 -11 58.69 4.68 2 -27 11 43.72 4.67 -2 -27 -12 36.99 3.97 -2 -27 -12 36.17 3.72 2 -27 12 35.89 3.84 -2 -27 -13 14.47 2.33 -2 -27 -13 11.99 2.62 2 -27 13 9.40 2.50 2 -27 14 9.33 2.24 -2 -27 -14 5.96 2.36 -2 -27 -14 7.99 2.07 -2 -27 -15 30.69 3.32 -2 -27 -15 28.36 3.11 2 -27 15 29.59 3.24 -2 -27 -16 13.85 2.28 -2 -27 -16 19.78 2.51 -2 -27 -17 35.74 3.29 -2 -27 -17 34.11 3.45 -2 -27 -18 5.94 1.59 -2 -27 -18 7.25 1.83 -2 -27 -19 3.35 1.59 -2 -27 -19 4.55 1.36 -2 -27 -20 2.64 1.42 -2 -27 -20 1.62 1.11 -2 -27 -21 5.76 1.29 -2 -27 -21 4.06 1.07 -2 -27 -22 4.31 1.09 2 -26 -24 3.27 0.98 2 -26 -23 5.05 1.22 -2 -26 23 5.35 1.15 2 -26 -22 11.86 1.68 2 -26 -21 2.46 1.46 2 -26 -20 0.78 1.62 2 -26 -19 5.52 1.80 2 -26 -18 15.40 2.37 2 -26 -17 5.13 2.04 2 -26 -16 8.90 2.31 2 -26 -15 10.62 1.64 2 -26 -15 14.43 2.54 2 -26 -14 2.12 2.24 -2 -26 14 1.52 2.62 2 -26 -14 1.80 1.32 2 -26 -13 13.46 1.91 -2 -26 13 17.20 3.27 2 -26 -13 17.92 2.75 2 -26 -12 8.45 1.72 2 -26 -12 10.67 2.58 -2 -26 12 15.84 3.53 -2 -26 11 19.05 3.91 2 -26 -11 20.13 3.03 2 -26 -11 17.02 2.17 2 -26 -10 11.02 2.78 -2 -26 10 15.03 4.06 2 -26 -10 14.37 1.98 2 -26 -9 2.04 2.42 2 -26 -9 -0.90 1.50 -2 -26 9 -1.17 4.31 2 -26 -8 22.14 2.56 2 -26 -8 26.58 3.28 -2 -26 8 22.11 5.33 2 -26 -7 -1.17 2.45 2 -26 -7 3.02 1.60 -2 -26 7 4.47 5.18 2 -26 -6 3.20 1.65 -2 -26 6 5.75 5.67 2 -26 -6 1.76 2.51 2 -26 -5 14.55 2.89 -2 -26 5 15.47 5.95 2 -26 -5 15.16 2.20 -2 -26 4 2.45 5.48 2 -26 -4 0.17 2.38 2 -26 -4 0.59 1.64 -2 -26 3 10.68 5.19 2 -26 -3 10.08 2.02 2 -26 -3 13.93 2.63 2 -26 -2 3.09 2.45 2 -26 -2 6.75 1.93 -2 -26 2 11.07 4.51 2 -26 -1 0.27 1.85 2 -26 -1 6.04 2.57 -2 -26 1 3.01 3.77 2 -26 0 0.76 1.99 2 -26 0 0.09 2.42 -2 -26 0 0.33 3.04 2 -26 1 28.20 3.73 -2 -26 -1 39.64 4.02 2 -26 1 30.43 3.42 2 -26 2 18.97 3.04 2 -26 2 16.58 2.68 -2 -26 -2 16.25 3.05 -2 -26 -3 18.40 3.42 -2 -26 -3 16.39 3.03 2 -26 3 19.22 2.75 2 -26 3 25.11 3.22 -2 -26 -4 3.11 2.93 -2 -26 -4 5.83 2.50 2 -26 4 2.05 2.03 2 -26 4 1.48 2.44 2 -26 5 32.17 3.53 -2 -26 -5 33.61 4.14 2 -26 5 38.39 4.06 -2 -26 -5 37.07 3.86 -2 -26 -6 14.94 2.71 2 -26 6 16.03 2.93 -2 -26 -6 10.42 3.07 2 -26 6 11.62 2.28 -2 -26 -7 32.32 3.49 2 -26 7 30.46 3.67 -2 -26 -7 30.91 3.86 2 -26 7 26.99 3.11 -2 -26 -8 1.71 2.31 -2 -26 -8 -2.01 2.70 2 -26 8 2.25 1.80 2 -26 8 1.47 2.48 -2 -26 -9 7.35 2.44 2 -26 9 4.94 1.88 -2 -26 -9 7.03 2.82 2 -26 9 9.14 2.55 2 -26 10 31.87 3.81 -2 -26 -10 31.84 3.90 -2 -26 -10 31.88 3.69 2 -26 10 32.83 3.27 -2 -26 -11 33.02 3.80 -2 -26 -11 30.12 3.48 2 -26 11 34.55 3.77 2 -26 11 29.68 3.19 2 -26 12 -0.49 2.35 -2 -26 -12 1.80 2.55 -2 -26 -12 3.88 2.25 -2 -26 -13 30.32 3.31 2 -26 13 25.08 3.48 -2 -26 -13 29.66 3.54 2 -26 14 15.16 3.04 -2 -26 -14 26.18 2.98 -2 -26 -14 22.15 3.11 2 -26 15 16.81 2.90 -2 -26 -15 17.48 2.88 -2 -26 -15 20.73 2.68 -2 -26 -16 3.05 2.32 2 -26 16 0.27 1.50 2 -26 16 1.04 2.14 -2 -26 -16 5.23 2.04 -2 -26 -17 26.61 2.94 -2 -26 -17 25.34 2.72 2 -26 18 2.77 1.47 -2 -26 -18 2.23 1.74 -2 -26 -18 3.81 2.08 -2 -26 -19 23.33 2.61 -2 -26 -19 22.69 2.38 2 -26 20 2.10 1.35 -2 -26 -20 4.15 1.73 -2 -26 -20 3.26 1.49 -2 -26 -21 6.66 1.38 2 -26 21 4.39 1.31 -2 -26 -21 7.63 1.62 2 -26 22 0.04 1.05 -2 -26 -22 0.90 1.06 -2 -26 -22 1.89 1.24 -2 -26 -23 -0.77 1.07 -2 -26 -23 0.03 0.87 -2 -26 -24 1.38 0.88 2 -25 -26 0.08 0.80 2 -25 -25 14.71 1.66 2 -25 -24 3.17 1.30 2 -25 -23 2.65 1.48 2 -25 -22 4.59 1.66 -2 -25 22 2.78 1.64 -2 -25 21 3.23 1.68 2 -25 -21 1.57 1.76 -2 -25 20 10.15 2.08 2 -25 -20 14.10 2.24 2 -25 -19 4.27 2.08 -2 -25 19 3.68 1.83 2 -25 -18 2.48 1.21 2 -25 -18 2.12 2.14 -2 -25 18 2.85 1.84 2 -25 -17 10.59 1.67 -2 -25 17 10.40 2.16 2 -25 -17 10.07 2.53 -2 -25 16 10.45 2.17 2 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0 10.05 2.82 2 -25 1 9.38 2.82 2 -25 1 5.64 2.10 -2 -25 -1 7.15 2.71 -2 -25 -2 3.64 2.70 2 -25 2 0.96 1.99 2 -25 2 3.41 2.69 -2 -25 -2 4.19 3.11 2 -25 3 80.48 7.03 -2 -25 -3 82.58 7.49 -2 -25 -3 96.41 7.43 2 -25 3 89.20 7.32 -2 -25 -4 34.37 4.33 2 -25 4 29.83 3.48 -2 -25 -4 31.73 3.90 2 -25 4 36.59 4.08 -2 -25 -5 35.07 3.93 -2 -25 -5 32.95 4.33 2 -25 5 35.08 4.07 2 -25 5 36.72 3.77 -2 -25 -6 4.31 2.58 -2 -25 -6 -5.03 3.14 2 -25 6 0.64 2.58 2 -25 6 1.82 2.04 2 -25 7 32.92 4.06 -2 -25 -7 36.76 4.27 2 -25 7 32.88 3.60 -2 -25 -7 41.26 3.97 2 -25 8 4.95 2.04 -2 -25 -8 10.79 2.66 -2 -25 -8 9.71 2.98 2 -25 8 9.54 2.77 2 -25 9 34.72 3.72 -2 -25 -9 40.98 4.04 -2 -25 -9 37.14 4.29 2 -25 9 37.96 4.16 2 -25 10 -0.09 2.39 -2 -25 -10 -0.56 2.23 -2 -25 -10 1.63 2.76 2 -25 10 0.98 1.94 -2 -25 -11 8.92 2.83 2 -25 11 10.47 2.14 -2 -25 -11 11.53 2.51 2 -25 11 4.46 2.53 -2 -25 -12 21.05 3.38 -2 -25 -12 27.62 3.24 2 -25 12 24.27 3.36 -2 -25 -13 6.72 2.66 2 -25 13 3.97 2.47 2 -25 13 3.93 1.72 -2 -25 -13 2.28 2.30 2 -25 14 0.46 1.68 -2 -25 -14 -1.41 2.23 2 -25 14 2.19 2.36 -2 -25 -14 0.48 2.54 -2 -25 -15 31.16 3.20 2 -25 15 31.34 3.40 -2 -25 -15 25.78 3.36 -2 -25 -16 6.81 2.53 2 -25 16 4.08 2.46 -2 -25 -16 2.07 2.24 2 -25 16 2.09 1.90 2 -25 17 30.15 3.37 -2 -25 -17 30.91 3.43 -2 -25 -17 35.96 3.30 -2 -25 -18 8.18 2.11 2 -25 18 2.70 1.99 -2 -25 -18 6.34 2.38 -2 -25 -19 32.33 3.21 -2 -25 -19 32.05 3.03 -2 -25 -20 2.70 1.92 -2 -25 -20 -0.05 1.72 2 -25 20 1.09 1.63 -2 -25 -21 2.29 1.56 -2 -25 -21 1.66 1.75 2 -25 21 1.67 1.51 -2 -25 -22 0.72 1.31 -2 -25 -22 -1.46 1.56 2 -25 22 0.70 1.39 2 -25 23 0.09 1.19 -2 -25 -23 -0.36 1.15 -2 -25 -23 -0.45 1.32 2 -25 24 -0.32 1.08 -2 -25 -24 2.76 1.22 -2 -25 -24 0.03 1.00 -2 -25 -25 0.10 0.95 2 -25 25 2.15 0.97 -2 -25 -25 -0.25 0.73 2 -24 -27 11.62 1.36 2 -24 -26 0.62 1.07 2 -24 -25 13.22 1.80 2 -24 -24 0.39 1.51 -2 -24 24 3.99 1.67 2 -24 -23 20.18 2.41 -2 -24 23 16.76 2.42 2 -24 -22 11.05 2.05 -2 -24 22 6.31 2.06 -2 -24 21 1.13 1.93 2 -24 -21 0.82 1.16 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2.56 2 5 -34 0.47 2.55 2 5 -33 15.40 3.21 2 5 -32 10.09 3.12 2 5 -31 9.55 3.21 2 5 -30 13.86 3.46 2 5 -29 9.66 3.42 2 5 -28 8.82 3.30 2 5 -27 -0.94 3.31 2 5 -26 4.57 3.31 2 5 -25 6.04 3.17 2 5 -24 7.21 3.03 2 5 -23 -1.09 2.70 2 5 -23 3.69 2.21 2 5 -22 23.52 3.29 2 5 -22 20.82 2.86 2 5 -21 12.53 2.80 2 5 -21 15.95 2.44 2 5 -20 18.92 2.51 2 5 -20 15.81 2.82 2 5 -19 195.70 14.36 2 5 -19 186.51 14.21 2 5 -18 12.01 1.98 2 5 -18 11.99 2.22 2 5 -17 61.39 8.50 2 5 -17 61.23 5.32 2 5 -17 63.92 5.14 2 5 -16 10.85 1.77 2 5 -16 12.09 4.72 2 5 -16 11.86 1.74 2 5 -16 10.44 1.95 -2 5 16 11.75 4.28 2 5 -15 647.89 47.25 2 5 -15 641.36 47.20 -2 5 15 702.08 50.13 2 5 -15 676.26 47.34 2 5 -15 657.91 50.38 2 5 -14 56.68 4.44 2 5 -14 53.82 4.60 -2 5 14 63.14 7.46 2 5 -14 57.02 7.55 -2 5 13 138.46 13.31 2 5 -13 146.38 10.74 2 5 -13 143.85 13.66 2 5 -12 300.52 23.70 -2 5 12 279.48 23.31 -2 5 11 418.78 32.44 2 5 -11 417.66 32.59 -2 5 10 58.59 7.06 2 5 -10 65.85 7.48 -2 5 9 5.16 3.82 -2 5 8 7.92 4.15 -2 5 7 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56.82 7.37 2 8 -13 41.29 7.46 -2 8 12 152.23 14.94 -2 8 12 131.91 12.99 -2 8 11 116.55 11.79 -2 8 11 128.07 13.34 -2 8 10 148.50 14.49 -2 8 10 130.88 12.85 2 8 -9 30.54 5.72 -2 8 9 23.89 5.32 -2 8 9 41.81 7.34 2 8 -8 318.74 25.38 -2 8 8 320.15 26.56 -2 8 8 306.51 25.26 -2 8 7 489.92 38.16 -2 8 7 507.58 39.38 -2 8 6 7.49 5.96 -2 8 6 8.72 4.52 -2 8 5 187.42 16.60 -2 8 5 208.40 18.14 -2 8 4 164.80 15.16 -2 8 4 145.98 13.48 -2 8 3 75.77 9.72 -2 8 3 74.56 8.18 -2 8 2 63.99 8.64 -2 8 2 56.22 7.03 2 8 -2 56.45 4.45 2 8 -1 95.03 7.56 -2 8 1 95.29 9.63 -2 8 1 94.80 10.74 2 8 0 72.27 6.41 -2 8 0 56.42 7.20 -2 8 0 63.09 8.24 -2 8 -1 120.54 10.82 -2 8 -1 111.72 10.93 2 8 1 108.32 9.85 -2 8 -2 185.35 16.74 2 8 2 209.55 16.22 -2 8 -2 203.66 16.72 -2 8 -3 58.71 6.70 2 8 3 60.20 5.82 -2 8 -4 208.05 15.85 2 8 4 182.01 14.90 2 8 5 73.37 6.90 -2 8 -5 82.79 7.77 2 8 6 52.28 4.88 -2 8 -6 44.78 5.90 -2 8 -7 87.95 8.47 2 8 7 86.69 7.05 -2 8 -8 122.24 9.48 2 8 8 90.95 7.37 2 8 9 115.88 8.95 -2 8 -9 180.77 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19.02 2.94 2 10 -19 39.46 3.89 2 10 -19 42.58 3.83 2 10 -19 39.52 4.08 2 10 -18 7.04 2.00 2 10 -18 6.77 1.75 2 10 -18 7.21 2.11 2 10 -17 -0.68 1.80 2 10 -17 0.06 1.44 2 10 -16 11.69 1.78 2 10 -16 9.56 1.99 2 10 -15 12.18 1.71 2 10 -15 11.61 1.90 2 10 -14 8.15 1.57 -2 10 14 -0.80 4.77 -2 10 14 5.89 3.85 2 10 -14 5.51 1.34 2 10 -13 17.13 1.87 -2 10 13 21.13 6.28 -2 10 13 24.82 5.38 2 10 -13 17.10 2.03 -2 10 12 70.96 8.24 2 10 -12 59.96 4.72 2 10 -12 60.56 4.84 -2 10 12 46.01 8.77 -2 10 11 48.58 7.67 -2 10 11 72.81 10.16 2 10 -11 69.15 8.39 2 10 -10 68.06 8.52 -2 10 10 50.61 8.90 -2 10 10 65.52 8.11 -2 10 9 139.31 14.62 2 10 -9 139.59 13.30 -2 10 9 121.96 12.73 -2 10 8 76.97 10.15 -2 10 8 63.77 8.50 -2 10 7 150.65 14.27 -2 10 7 154.58 15.81 -2 10 6 549.31 44.26 -2 10 6 562.03 42.93 -2 10 5 129.81 14.77 -2 10 5 147.92 13.41 -2 10 4 72.65 8.67 -2 10 4 75.10 10.60 -2 10 3 25.58 7.58 2 10 -3 21.11 2.15 -2 10 3 30.38 5.73 2 10 -2 290.52 21.69 -2 10 2 311.12 24.16 -2 10 2 304.94 25.17 -2 10 1 56.06 8.65 2 10 -1 57.35 5.35 -2 10 1 70.03 7.95 2 10 0 111.35 9.56 -2 10 0 109.37 11.02 -2 10 0 107.85 11.50 2 10 1 55.32 6.71 -2 10 -1 65.41 8.04 -2 10 -1 58.95 7.78 2 10 2 196.36 15.48 -2 10 -2 207.24 16.50 -2 10 -2 191.28 16.61 2 10 2 160.45 15.57 -2 10 -3 241.03 19.89 -2 10 -3 237.70 19.33 2 10 3 213.92 18.48 2 10 3 255.46 19.52 2 10 4 93.71 9.31 -2 10 -4 87.00 8.93 -2 10 -4 91.90 10.02 2 10 4 78.98 8.16 2 10 5 6.73 4.38 2 10 5 10.14 3.43 -2 10 -5 6.22 3.42 -2 10 -6 31.32 4.85 2 10 6 27.54 4.33 2 10 7 44.95 4.76 -2 10 -7 34.32 5.22 2 10 8 38.46 4.05 -2 10 -8 33.65 5.30 2 10 9 101.29 9.11 -2 10 -9 126.21 8.83 -2 10 -9 122.41 11.11 -2 10 -10 77.41 7.37 -2 10 -10 80.30 4.68 -2 10 -10 70.63 4.51 -2 10 -11 4.81 1.31 -2 10 -11 4.17 1.45 -2 10 -12 23.71 2.41 -2 10 -12 20.40 2.27 -2 10 -13 40.40 3.65 -2 10 -13 42.15 3.57 -2 10 -14 -0.05 1.35 -2 10 -14 0.87 1.46 -2 10 -15 23.57 2.59 -2 10 -15 26.40 2.80 -2 10 -16 1.97 1.74 -2 10 -16 5.05 1.66 -2 10 -17 17.27 2.49 -2 10 -17 14.81 2.23 -2 10 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1.46 2 11 -37 0.58 1.24 2 11 -36 14.44 2.08 2 11 -35 2.75 1.96 2 11 -34 1.82 2.23 2 11 -33 7.92 2.64 2 11 -32 21.41 3.27 2 11 -28 5.60 3.32 2 11 -27 19.04 3.84 2 11 -26 5.25 2.65 2 11 -26 2.93 3.19 2 11 -25 14.52 2.88 2 11 -25 13.99 3.43 2 11 -24 22.01 3.11 2 11 -24 17.90 3.58 2 11 -23 74.50 6.51 2 11 -23 78.43 6.86 2 11 -22 23.77 3.50 2 11 -22 18.56 2.93 2 11 -21 6.33 2.20 2 11 -21 7.79 2.60 2 11 -20 1.42 1.98 2 11 -20 -0.29 2.34 2 11 -19 15.49 2.26 2 11 -19 14.62 2.46 2 11 -19 12.35 2.62 2 11 -18 21.26 2.68 2 11 -18 26.19 3.01 2 11 -18 22.69 2.78 2 11 -17 73.30 6.07 2 11 -17 72.77 5.90 2 11 -16 11.58 2.00 2 11 -16 7.19 1.72 2 11 -15 16.29 2.19 2 11 -15 16.52 2.00 2 11 -14 8.71 1.49 2 11 -14 6.99 1.70 2 11 -13 1.40 1.15 2 11 -13 1.94 1.34 2 11 -12 14.90 1.95 2 11 -12 27.27 5.69 2 11 -12 16.70 1.78 -2 11 12 16.57 4.78 -2 11 12 28.12 6.97 -2 11 11 8.82 4.52 -2 11 11 14.22 6.11 2 11 -11 11.77 4.60 -2 11 10 36.61 7.98 -2 11 10 39.54 6.62 2 11 -10 44.98 7.19 -2 11 9 28.89 5.90 -2 11 9 37.46 7.87 2 11 -9 36.50 6.70 -2 11 8 356.63 30.63 -2 11 8 354.12 28.97 -2 11 7 285.81 24.42 -2 11 7 302.59 26.12 -2 11 6 -0.85 4.32 -2 11 6 -1.89 6.63 -2 11 5 212.98 18.22 -2 11 5 192.55 19.50 -2 11 4 573.31 45.37 -2 11 4 566.88 43.98 2 11 -3 101.05 7.93 -2 11 3 122.53 11.41 -2 11 3 99.59 12.35 2 11 -2 87.49 7.08 -2 11 2 84.07 9.75 -2 11 2 97.85 11.33 -2 11 1 89.86 10.98 -2 11 1 96.76 10.53 2 11 -1 93.16 7.90 -2 11 0 281.67 23.24 2 11 0 267.23 21.30 -2 11 0 290.88 23.46 -2 11 -1 113.42 11.06 -2 11 -1 95.14 10.39 2 11 1 86.16 9.21 -2 11 -2 160.27 15.08 2 11 2 153.24 14.17 -2 11 -2 168.24 14.73 2 11 2 165.17 13.97 -2 11 -3 47.12 7.50 -2 11 -3 54.15 6.71 2 11 3 57.60 7.26 2 11 3 41.74 5.99 -2 11 -4 136.86 12.34 2 11 4 127.91 11.75 -2 11 -4 141.89 13.33 2 11 4 129.36 12.70 2 11 5 31.30 5.10 -2 11 -5 41.88 6.92 2 11 5 37.51 6.50 -2 11 -5 39.95 5.55 2 11 6 7.62 4.61 -2 11 -6 11.95 3.59 2 11 6 8.95 3.50 2 11 7 79.81 7.19 -2 11 -7 70.80 5.58 -2 11 -7 70.04 7.77 -2 11 -8 42.49 3.61 -2 11 -8 33.35 5.40 2 11 8 45.23 4.76 -2 11 -8 46.47 3.70 -2 11 -9 23.13 4.69 2 11 9 25.93 3.19 -2 11 -9 31.80 2.74 -2 11 -9 28.52 2.65 2 11 10 5.76 1.20 -2 11 -10 7.26 1.44 -2 11 -10 10.14 1.63 -2 11 -10 10.72 3.68 -2 11 -11 51.11 4.46 -2 11 -11 54.08 6.83 -2 11 -11 61.21 4.61 -2 11 -12 1.13 1.44 -2 11 -12 0.31 1.25 -2 11 -13 27.19 2.66 -2 11 -13 26.42 2.77 -2 11 -14 13.97 2.16 -2 11 -14 14.74 1.97 -2 11 -15 1.40 1.50 -2 11 -15 0.14 1.73 -2 11 -16 36.35 3.48 -2 11 -16 36.95 3.59 -2 11 -17 47.80 4.20 -2 11 -17 46.20 4.34 -2 11 -18 3.25 2.21 -2 11 -18 4.69 1.99 -2 11 -19 63.56 5.33 -2 11 -19 64.31 5.47 -2 11 -19 62.11 5.63 -2 11 -20 31.94 3.74 -2 11 -20 35.45 3.61 -2 11 -20 38.88 4.01 -2 11 -21 39.26 4.08 -2 11 -21 43.03 4.29 -2 11 -21 46.29 4.61 -2 11 -22 16.71 3.06 -2 11 -22 18.13 3.29 -2 11 -22 15.43 2.91 -2 11 -23 1.68 3.02 -2 11 -23 3.59 2.73 -2 11 -23 0.72 2.45 -2 11 -24 13.55 3.40 -2 11 -24 12.74 3.14 -2 11 -24 15.78 3.06 -2 11 -25 32.85 3.85 -2 11 -25 31.74 4.41 -2 11 -25 31.29 4.11 -2 11 -26 35.55 4.74 -2 11 -26 32.07 4.35 -2 11 -26 40.65 4.22 -2 11 -27 16.51 3.44 -2 11 -27 12.86 3.18 -2 11 -27 20.47 3.88 -2 11 -28 76.55 6.89 -2 11 -28 75.21 6.63 -2 11 -28 77.27 7.13 -2 11 -29 9.32 2.98 -2 11 -29 6.74 3.36 -2 11 -29 6.55 2.66 -2 11 -30 40.62 4.78 -2 11 -30 40.68 4.23 -2 11 -30 37.77 4.38 -2 11 -31 7.32 2.48 -2 11 -31 6.46 3.25 -2 11 -32 19.33 2.85 -2 11 -32 18.89 3.44 -2 11 -33 3.37 2.59 -2 11 -33 -0.47 2.04 -2 11 -34 4.18 1.91 -2 11 -35 4.28 1.62 -2 11 -36 3.43 1.87 -2 11 -36 0.29 1.20 2 12 -36 5.27 1.61 2 12 -35 5.47 1.95 2 12 -34 20.95 2.77 2 12 -33 3.40 2.35 2 12 -32 3.74 2.69 2 12 -28 -0.24 3.22 2 12 -27 -1.58 3.06 2 12 -26 49.19 5.25 2 12 -26 48.19 4.85 2 12 -25 54.26 5.36 2 12 -25 47.12 4.91 2 12 -24 12.86 3.17 2 12 -24 11.30 2.76 2 12 -23 8.49 3.05 2 12 -23 4.83 2.39 2 12 -22 3.04 2.83 2 12 -22 6.88 2.26 2 12 -21 26.28 3.21 2 12 -21 25.99 3.62 2 12 -20 36.00 3.82 2 12 -20 42.46 4.17 2 12 -19 54.09 4.72 2 12 -19 54.69 4.90 2 12 -19 51.86 4.96 2 12 -18 3.10 1.74 2 12 -18 3.71 2.21 2 12 -17 16.26 2.46 2 12 -17 15.42 2.20 2 12 -16 26.37 2.94 2 12 -16 26.81 2.75 2 12 -15 61.98 5.25 2 12 -15 64.08 5.13 2 12 -14 28.02 2.97 2 12 -14 33.72 2.92 2 12 -13 3.97 1.41 2 12 -13 4.10 1.25 -2 12 12 28.11 5.92 2 12 -12 36.43 3.05 -2 12 12 29.62 7.86 2 12 -12 34.86 3.14 2 12 -11 36.15 6.42 2 12 -11 25.85 2.41 -2 12 11 28.05 5.77 -2 12 11 28.47 7.31 -2 12 10 17.06 4.94 -2 12 10 26.64 6.92 2 12 -10 13.93 5.03 -2 12 9 184.33 17.05 -2 12 9 183.12 18.67 -2 12 8 7.88 4.36 -2 12 8 6.59 6.21 -2 12 7 0.96 4.17 -2 12 7 4.97 6.00 -2 12 6 704.77 53.74 -2 12 6 694.92 55.42 -2 12 5 192.26 17.24 -2 12 5 180.87 18.76 -2 12 4 -0.63 6.60 -2 12 4 0.92 4.58 2 12 -3 67.55 5.60 -2 12 3 76.13 9.16 -2 12 3 80.44 10.57 -2 12 2 237.85 20.45 2 12 -2 212.65 16.27 -2 12 2 216.95 19.20 -2 12 1 84.85 11.35 -2 12 1 100.26 10.87 2 12 -1 96.24 8.14 2 12 0 260.05 20.38 -2 12 0 254.73 22.57 -2 12 0 271.79 22.56 2 12 1 160.05 13.84 -2 12 -1 176.13 15.54 2 12 1 160.65 14.27 -2 12 -1 148.18 15.04 -2 12 -2 125.78 12.52 -2 12 -2 137.79 13.31 2 12 2 144.27 12.15 2 12 2 108.22 11.82 -2 12 -3 92.38 11.00 2 12 3 106.64 10.69 2 12 3 93.11 9.70 -2 12 -3 108.61 10.62 2 12 4 20.91 5.56 -2 12 -4 17.46 5.28 -2 12 -4 21.95 4.74 2 12 4 21.40 4.60 -2 12 -5 55.41 6.86 2 12 5 52.19 7.45 2 12 5 52.50 6.57 -2 12 -5 56.68 4.48 -2 12 -5 51.63 8.17 -2 12 -6 38.05 5.60 2 12 6 34.40 5.20 -2 12 -6 37.81 3.21 2 12 6 36.23 6.61 -2 12 -6 34.29 6.85 -2 12 -7 1.93 1.17 -2 12 -7 2.49 3.15 2 12 7 3.48 4.56 2 12 7 2.87 3.10 -2 12 -7 1.24 1.24 -2 12 -8 1.45 1.34 -2 12 -8 4.73 3.27 2 12 8 6.71 2.74 2 12 8 7.87 4.99 -2 12 -8 2.95 1.29 -2 12 -9 78.99 5.78 -2 12 -9 79.68 5.84 2 12 9 86.53 9.71 -2 12 -9 63.99 7.85 -2 12 -10 3.26 1.42 -2 12 -10 0.39 2.70 -2 12 -10 1.96 1.30 -2 12 -11 31.88 2.84 -2 12 -11 33.97 5.28 -2 12 -11 26.79 2.87 -2 12 -12 26.58 2.74 -2 12 -12 31.96 2.95 -2 12 -13 9.66 1.77 -2 12 -13 9.59 1.90 -2 12 -14 38.71 3.52 -2 12 -14 37.23 3.64 -2 12 -15 32.80 3.32 -2 12 -15 29.91 3.12 -2 12 -16 12.18 2.07 -2 12 -16 9.16 2.17 -2 12 -17 36.98 3.51 -2 12 -17 33.68 3.70 -2 12 -18 18.52 2.84 -2 12 -18 17.69 2.65 -2 12 -19 14.29 2.81 -2 12 -19 11.99 2.45 -2 12 -19 11.68 2.41 -2 12 -20 11.16 2.68 -2 12 -20 11.59 2.55 -2 12 -20 8.89 2.85 -2 12 -21 93.26 7.74 -2 12 -21 90.32 7.39 -2 12 -21 88.88 7.56 -2 12 -22 5.91 2.73 -2 12 -22 3.04 2.97 -2 12 -22 9.21 2.85 -2 12 -23 67.33 6.20 -2 12 -23 63.30 5.97 -2 12 -23 76.69 6.47 -2 12 -24 44.25 4.84 -2 12 -24 45.23 4.65 -2 12 -24 45.48 5.05 -2 12 -25 33.81 4.22 -2 12 -25 32.96 4.45 -2 12 -25 29.81 3.85 -2 12 -26 60.14 6.09 -2 12 -26 67.75 5.94 -2 12 -26 68.91 6.38 -2 12 -27 11.64 3.03 -2 12 -27 10.57 3.48 -2 12 -27 12.55 3.26 -2 12 -28 30.21 3.99 -2 12 -28 32.08 3.83 -2 12 -28 29.90 4.48 -2 12 -29 2.19 3.27 -2 12 -29 1.41 2.49 -2 12 -29 2.21 2.84 -2 12 -30 27.65 3.79 -2 12 -30 23.20 3.89 -2 12 -30 31.71 3.54 -2 12 -31 3.60 2.95 -2 12 -31 0.23 2.23 -2 12 -32 6.35 2.82 -2 12 -32 7.83 2.31 -2 12 -33 17.30 2.50 -2 12 -34 3.65 1.79 -2 12 -35 0.77 1.39 -2 12 -36 0.82 1.49 2 13 -36 4.67 1.41 2 13 -35 8.56 1.94 2 13 -34 -0.41 1.92 2 13 -33 16.98 2.76 2 13 -27 17.09 3.47 2 13 -26 8.96 3.25 2 13 -26 5.37 2.63 2 13 -25 5.47 3.08 2 13 -25 3.12 2.46 2 13 -24 2.46 2.87 2 13 -24 2.79 2.40 2 13 -23 49.26 4.58 2 13 -23 42.09 4.87 2 13 -22 7.90 2.37 2 13 -22 10.29 2.93 2 13 -21 16.06 2.71 2 13 -21 15.19 3.11 2 13 -20 10.55 2.82 2 13 -20 14.18 2.99 2 13 -20 12.75 2.39 2 13 -19 19.31 2.69 2 13 -19 20.55 2.97 2 13 -19 20.06 3.02 2 13 -18 15.48 2.33 2 13 -18 12.80 2.61 2 13 -17 107.18 8.02 2 13 -17 96.07 8.11 2 13 -16 7.71 2.01 2 13 -16 7.42 1.77 2 13 -15 3.59 1.72 2 13 -15 5.83 1.53 2 13 -14 35.36 3.05 2 13 -14 29.97 3.12 2 13 -13 31.28 3.23 2 13 -13 39.21 3.19 2 13 -12 19.95 2.08 -2 13 11 7.98 4.29 -2 13 11 7.92 5.85 2 13 -11 9.07 1.41 2 13 -10 64.22 9.08 -2 13 10 78.12 10.77 -2 13 10 58.34 8.47 -2 13 9 44.29 8.85 -2 13 9 47.31 7.21 -2 13 8 176.18 16.95 -2 13 8 182.38 18.94 -2 13 7 213.71 19.33 -2 13 7 211.70 21.03 -2 13 6 73.89 11.68 -2 13 6 101.05 10.83 -2 13 5 37.15 6.97 -2 13 5 31.23 8.37 -2 13 4 324.31 23.56 -2 13 4 290.13 28.06 -2 13 4 322.22 26.95 -2 13 3 113.44 7.81 2 13 -3 86.93 7.67 -2 13 3 109.46 11.46 -2 13 3 91.83 12.32 -2 13 2 56.89 4.61 -2 13 2 50.52 9.08 2 13 -2 48.63 4.78 -2 13 2 69.70 8.60 -2 13 1 89.98 10.61 -2 13 1 81.21 10.99 2 13 -1 91.61 8.03 -2 13 1 96.81 7.32 2 13 0 98.65 8.93 -2 13 0 96.93 7.59 2 13 0 100.26 10.25 -2 13 0 89.05 11.04 -2 13 0 120.15 11.64 -2 13 -1 111.01 11.55 -2 13 -1 109.22 8.18 2 13 1 94.17 9.95 -2 13 -1 104.56 11.94 2 13 1 105.11 10.77 -2 13 -2 159.90 15.16 -2 13 -2 159.71 15.71 -2 13 -2 169.05 12.13 2 13 2 157.89 14.57 2 13 2 132.36 14.18 -2 13 -3 93.25 10.23 2 13 3 89.44 9.92 2 13 3 85.75 10.30 -2 13 -3 100.84 7.52 -2 13 -3 103.75 11.57 2 13 4 33.24 5.56 2 13 4 35.50 6.43 -2 13 -4 36.03 7.00 -2 13 -4 36.58 5.84 -2 13 -4 35.47 3.18 -2 13 -5 22.71 2.36 -2 13 -5 30.85 6.45 -2 13 -5 26.70 4.88 2 13 5 18.14 5.42 2 13 5 21.81 4.71 -2 13 -6 16.82 4.07 -2 13 -6 16.25 1.97 -2 13 -6 18.13 2.00 2 13 6 20.71 4.25 2 13 6 12.46 5.21 -2 13 -6 12.43 5.41 2 13 7 36.65 6.49 -2 13 -7 35.11 3.04 -2 13 -7 32.61 6.76 2 13 7 23.64 4.81 -2 13 -7 33.46 3.01 -2 13 -7 27.33 4.97 -2 13 -8 23.12 2.27 -2 13 -8 17.65 4.14 -2 13 -8 19.30 2.26 2 13 8 19.54 5.72 2 13 9 21.79 5.60 -2 13 -9 19.46 2.26 -2 13 -9 19.78 2.18 -2 13 -9 15.72 4.05 -2 13 -10 8.87 3.64 -2 13 -10 13.35 1.95 -2 13 -10 13.82 1.88 2 13 10 10.86 4.97 -2 13 -11 22.72 4.61 -2 13 -11 27.86 2.66 -2 13 -11 24.10 2.71 2 13 11 23.63 6.18 -2 13 -12 48.48 4.15 2 13 12 35.71 7.43 -2 13 -12 48.96 4.24 -2 13 -13 17.40 2.39 -2 13 -13 17.04 2.23 -2 13 -14 8.94 1.97 -2 13 -14 8.98 2.10 -2 13 -15 13.46 2.22 -2 13 -15 14.45 2.38 -2 13 -16 25.88 2.96 -2 13 -16 25.56 3.09 -2 13 -17 5.96 2.31 -2 13 -17 5.56 2.06 -2 13 -18 10.04 2.56 -2 13 -18 9.43 2.37 -2 13 -19 129.74 10.32 -2 13 -19 130.51 10.20 -2 13 -20 3.49 2.50 -2 13 -20 3.11 2.55 -2 13 -20 5.22 2.92 -2 13 -21 116.16 9.41 -2 13 -21 114.45 9.24 -2 13 -21 112.10 9.14 -2 13 -22 72.50 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14 -20 1.52 2.76 2 14 -20 3.81 2.53 2 14 -19 105.85 8.76 2 14 -19 122.22 8.97 2 14 -19 108.42 8.92 2 14 -18 5.03 2.29 2 14 -18 10.84 2.11 2 14 -17 26.11 2.83 2 14 -17 23.02 2.95 2 14 -16 34.62 3.09 2 14 -16 25.38 3.18 2 14 -15 82.99 5.96 2 14 -15 63.99 5.91 2 14 -14 34.92 3.23 2 14 -13 7.54 1.49 2 14 -12 20.12 2.13 -2 14 10 22.43 5.37 -2 14 9 48.37 7.51 -2 14 9 37.04 8.59 -2 14 8 39.17 8.83 -2 14 8 43.32 7.15 -2 14 7 44.79 7.37 -2 14 7 42.70 8.84 -2 14 6 235.84 21.25 -2 14 6 234.63 22.84 -2 14 5 36.08 3.60 -2 14 5 27.43 6.51 -2 14 4 102.64 8.03 -2 14 4 90.84 12.57 -2 14 4 111.54 11.74 -2 14 3 50.58 4.43 -2 14 3 51.28 7.99 -2 14 3 41.55 8.15 -2 14 2 26.13 2.76 -2 14 2 26.82 6.27 2 14 -2 21.97 2.76 -2 14 2 27.49 7.10 2 14 -1 138.81 12.93 -2 14 1 121.54 13.51 2 14 -1 106.92 10.03 -2 14 1 129.74 9.50 -2 14 1 137.94 13.69 2 14 0 224.81 20.60 -2 14 0 250.39 17.78 -2 14 0 245.30 21.53 -2 14 0 248.46 21.70 2 14 0 215.18 18.77 -2 14 -1 60.63 4.96 2 14 1 69.69 8.21 2 14 1 47.50 6.53 -2 14 -1 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5 -33 -1.42 2.84 4 5 -32 3.33 2.96 4 5 -31 7.78 3.18 4 5 -30 9.52 3.31 4 5 -29 66.96 6.27 4 5 -28 0.09 2.92 4 5 -27 7.31 3.22 4 5 -26 5.76 2.83 4 5 -25 167.60 12.85 4 5 -24 9.54 2.74 4 5 -23 22.46 3.17 4 5 -22 15.47 2.62 4 5 -22 12.44 3.19 4 5 -21 231.98 19.10 4 5 -21 273.08 18.92 4 5 -20 8.32 2.61 4 5 -20 9.99 2.23 4 5 -19 96.72 8.47 4 5 -19 109.56 8.16 4 5 -18 119.54 8.63 4 5 -18 102.50 8.84 4 5 -17 229.44 17.32 4 5 -17 212.63 17.14 4 5 -17 259.25 17.15 -4 5 17 200.27 20.66 4 5 -16 8.66 4.82 -4 5 16 7.82 4.35 4 5 -16 3.00 1.47 -4 5 16 2.91 5.03 4 5 -16 6.71 1.49 4 5 -16 2.57 1.85 4 5 -15 16.17 5.13 4 5 -15 10.19 1.62 -4 5 15 10.25 5.86 -4 5 15 11.61 4.55 4 5 -15 11.15 1.61 4 5 -15 9.56 1.90 -4 5 14 214.11 18.97 4 5 -14 184.15 14.21 4 5 -14 194.68 14.07 -4 5 14 212.11 17.78 4 5 -14 184.07 17.74 4 5 -13 21.09 2.05 -4 5 13 11.76 4.72 -4 5 13 24.85 6.50 -4 5 12 52.17 8.59 -4 5 12 59.85 7.68 -4 5 11 42.99 7.93 -4 5 11 59.75 7.53 -4 5 10 278.39 24.21 -4 5 10 281.67 23.33 4 5 -10 285.08 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132.62 10.49 4 7 -24 25.96 3.46 4 7 -23 5.39 3.14 4 7 -23 5.26 2.67 4 7 -22 23.50 3.06 4 7 -22 25.40 3.66 4 7 -21 193.57 15.52 4 7 -21 211.05 15.27 4 7 -20 47.03 4.13 4 7 -20 40.48 4.51 4 7 -19 21.37 3.06 4 7 -19 19.05 2.57 4 7 -19 14.88 2.53 4 7 -18 43.73 4.21 4 7 -18 38.38 3.84 4 7 -18 46.92 3.88 4 7 -17 165.85 12.70 4 7 -17 181.06 12.49 4 7 -17 156.32 12.49 -4 7 17 150.38 16.29 4 7 -16 33.49 3.44 4 7 -16 33.23 3.17 4 7 -16 37.41 3.17 -4 7 16 31.65 6.47 4 7 -15 25.44 2.58 -4 7 15 34.40 7.35 4 7 -15 26.96 2.83 4 7 -15 27.20 2.58 -4 7 15 32.39 6.13 4 7 -14 96.32 7.67 4 7 -14 105.31 7.69 -4 7 14 109.04 11.50 4 7 -14 100.73 7.84 -4 7 13 12.38 4.57 4 7 -13 2.68 1.38 -4 7 13 14.78 5.95 -4 7 12 35.45 6.51 4 7 -12 37.22 6.57 -4 7 12 34.14 7.41 4 7 -11 90.25 10.21 -4 7 11 93.24 10.40 -4 7 11 90.21 11.54 -4 7 10 71.80 9.83 4 7 -10 57.21 7.85 -4 7 10 53.76 7.98 -4 7 9 -1.18 5.83 4 7 -9 4.12 4.34 -4 7 9 -2.18 4.62 4 7 -8 46.72 6.70 -4 7 8 48.72 7.12 -4 7 7 160.14 14.72 4 7 -7 155.09 14.22 -4 7 6 35.67 6.18 4 7 -6 29.80 5.30 -4 7 5 33.36 5.93 4 7 -5 29.49 5.17 4 7 -4 217.54 18.11 -4 7 4 226.73 19.04 4 7 -3 179.63 14.87 -4 7 3 173.29 15.64 4 7 -2 82.68 7.93 -4 7 1 144.58 14.64 4 7 -1 159.97 12.82 4 7 0 138.64 11.06 -4 7 0 181.13 14.54 4 7 0 180.51 12.41 4 7 1 124.74 9.86 4 7 1 117.87 9.25 -4 7 -1 109.74 11.61 -4 7 -1 121.86 11.77 -4 7 -2 269.60 21.63 4 7 2 254.40 19.69 4 7 2 265.76 19.61 -4 7 -2 252.31 21.58 -4 7 -3 238.30 20.65 4 7 3 272.61 19.02 -4 7 -3 275.36 20.66 4 7 3 228.01 18.52 4 7 4 201.50 15.00 4 7 4 241.78 16.12 -4 7 -4 235.18 17.89 -4 7 -4 254.03 17.58 4 7 4 184.05 14.89 4 7 5 33.86 4.36 -4 7 -5 35.11 5.65 -4 7 -5 39.33 6.53 4 7 6 94.70 8.82 -4 7 -6 97.66 9.72 -4 7 -6 96.67 10.44 4 7 7 237.10 18.22 -4 7 -7 205.69 19.05 -4 7 -7 223.62 18.59 4 7 8 68.35 7.47 -4 7 -8 69.50 8.60 -4 7 -8 63.42 7.58 4 7 9 16.24 4.56 -4 7 -9 23.75 5.69 -4 7 -9 18.94 4.47 -4 7 -10 66.86 8.14 -4 7 -10 55.17 4.49 4 7 10 64.56 7.28 -4 7 -10 55.99 7.06 -4 7 -11 627.75 49.55 4 7 11 588.60 48.82 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8 -18 74.16 5.70 4 8 -17 22.00 2.42 4 8 -17 19.88 2.40 4 8 -17 20.03 2.72 4 8 -16 73.99 6.10 4 8 -16 75.90 5.90 4 8 -16 73.63 5.89 -4 8 16 69.50 9.44 4 8 -15 53.90 4.62 4 8 -15 51.54 4.40 4 8 -15 57.26 4.46 -4 8 15 58.67 8.20 4 8 -14 55.98 4.70 -4 8 14 50.19 9.42 -4 8 14 66.13 8.48 4 8 -14 56.72 4.54 -4 8 13 130.37 13.71 4 8 -13 126.04 12.58 4 8 -13 103.48 8.19 -4 8 13 122.56 12.17 -4 8 12 3.65 3.82 -4 8 12 3.62 5.78 4 8 -12 0.54 4.14 -4 8 11 12.53 4.81 4 8 -11 22.70 5.45 4 8 -10 85.61 10.36 -4 8 10 101.51 10.59 4 8 -9 150.22 14.19 -4 8 9 148.93 14.53 -4 8 8 33.32 6.11 4 8 -8 20.41 5.21 -4 8 7 3.04 4.48 4 8 -7 -1.14 4.29 4 8 -6 200.38 18.17 -4 8 6 234.42 19.01 4 8 -5 6.16 4.09 -4 8 5 11.85 5.07 -4 8 4 57.72 9.42 -4 8 4 56.68 7.61 4 8 -4 48.94 6.47 4 8 -3 165.34 13.92 -4 8 3 147.49 15.97 -4 8 3 168.40 15.20 -4 8 2 278.90 24.67 4 8 -2 300.43 22.82 -4 8 2 280.57 23.82 4 8 -1 386.68 28.99 -4 8 1 368.36 30.89 4 8 0 71.65 6.81 -4 8 0 73.11 9.25 4 8 1 17.29 2.20 4 8 1 21.01 3.11 -4 8 -1 21.38 5.77 4 8 2 308.26 22.43 4 8 2 295.36 22.17 -4 8 -2 324.95 24.64 -4 8 -2 250.63 24.02 4 8 3 28.93 3.30 -4 8 -3 28.51 5.73 -4 8 -3 35.88 6.63 4 8 3 29.61 3.51 -4 8 -4 224.46 17.58 4 8 4 189.42 15.11 4 8 4 226.53 16.08 -4 8 -4 231.53 18.22 4 8 4 196.94 15.13 4 8 5 282.70 21.85 -4 8 -5 285.49 22.90 -4 8 -5 275.81 23.40 4 8 6 70.04 7.08 -4 8 -6 76.43 8.28 -4 8 -6 64.80 8.73 4 8 7 44.32 5.68 -4 8 -7 56.26 6.73 -4 8 -7 44.44 7.27 4 8 8 67.66 7.67 -4 8 -8 80.26 8.46 -4 8 -8 66.60 8.93 -4 8 -8 70.24 5.68 -4 8 -8 78.83 5.77 -4 8 -9 237.61 16.84 -4 8 -9 244.43 20.30 -4 8 -9 219.17 16.76 4 8 9 245.97 19.20 -4 8 -9 235.01 19.40 -4 8 -10 32.60 3.11 4 8 10 30.54 5.69 -4 8 -10 37.77 6.98 -4 8 -10 36.23 5.85 -4 8 -10 38.94 3.24 -4 8 -11 19.25 5.60 -4 8 -11 19.80 4.64 4 8 11 15.28 4.48 -4 8 -11 16.86 2.08 4 8 12 59.92 7.81 -4 8 -12 68.24 8.79 -4 8 -12 65.53 7.78 -4 8 -12 59.11 4.93 4 8 13 220.21 22.00 -4 8 -13 270.44 19.34 -4 8 -13 253.99 22.97 -4 8 -14 54.85 8.21 4 8 14 49.13 7.49 -4 8 -15 1.90 4.34 4 8 15 1.16 3.79 -4 8 -15 4.58 1.35 -4 8 -16 127.07 9.03 -4 8 -16 112.09 9.02 -4 8 -17 69.62 5.57 -4 8 -17 69.94 5.58 -4 8 -18 12.11 1.95 -4 8 -18 14.28 1.98 -4 8 -19 65.49 5.12 -4 8 -19 58.03 5.04 -4 8 -20 66.12 5.26 -4 8 -20 60.14 5.19 -4 8 -21 5.64 1.95 -4 8 -21 5.57 1.68 -4 8 -22 69.53 5.45 -4 8 -22 59.79 5.28 -4 8 -23 19.63 2.53 -4 8 -23 24.08 2.87 -4 8 -24 6.53 2.37 -4 8 -24 9.67 2.05 -4 8 -25 12.94 2.56 -4 8 -25 12.13 2.12 -4 8 -26 105.24 8.40 -4 8 -27 9.75 2.52 -4 8 -28 -0.33 2.22 -4 8 -29 5.69 2.29 -4 8 -30 2.41 2.15 -4 8 -31 8.95 2.32 -4 8 -31 9.71 3.35 -4 8 -32 8.11 2.18 -4 8 -32 14.90 3.22 -4 8 -33 11.75 2.10 -4 8 -33 6.51 2.83 -4 8 -34 8.45 1.78 -4 8 -34 11.68 2.70 -4 8 -34 7.21 2.68 -4 8 -35 2.63 2.17 -4 8 -36 5.39 1.81 4 9 -37 8.90 1.52 4 9 -37 3.10 1.39 4 9 -36 2.17 1.65 4 9 -35 -3.92 1.99 4 9 -34 -0.07 2.19 4 9 -33 11.24 2.67 4 9 -32 14.58 3.00 4 9 -31 24.69 3.50 4 9 -30 26.55 3.73 4 9 -29 24.88 3.77 4 9 -28 24.33 3.75 4 9 -27 6.84 2.91 4 9 -26 57.49 5.50 4 9 -25 23.28 3.49 4 9 -24 10.01 2.84 4 9 -23 22.83 3.59 4 9 -23 22.01 3.21 4 9 -22 23.87 3.60 4 9 -22 22.56 3.19 4 9 -21 46.38 4.85 4 9 -21 46.83 4.47 4 9 -20 76.03 6.32 4 9 -20 80.97 6.36 4 9 -20 71.93 6.57 4 9 -19 1.02 1.87 4 9 -19 1.44 1.74 4 9 -19 0.82 2.16 4 9 -18 26.79 3.08 4 9 -18 20.85 2.57 4 9 -18 23.05 2.67 4 9 -17 115.49 9.13 4 9 -17 123.82 8.95 4 9 -17 110.89 8.91 -4 9 16 51.74 8.63 4 9 -16 71.12 5.25 4 9 -16 62.41 5.19 4 9 -16 61.15 5.41 -4 9 15 53.34 7.80 4 9 -15 47.66 3.74 4 9 -15 38.43 3.63 4 9 -15 42.49 3.85 4 9 -14 13.12 1.90 -4 9 14 15.50 4.85 4 9 -13 9.49 1.62 4 9 -13 12.30 4.84 -4 9 13 14.88 4.92 4 9 -12 116.30 12.66 -4 9 12 116.10 12.45 4 9 -11 129.84 13.58 -4 9 11 135.22 13.61 -4 9 10 1.54 4.30 4 9 -10 9.06 4.58 4 9 -9 52.30 7.28 -4 9 9 43.23 7.16 -4 9 8 193.01 17.10 4 9 -8 169.84 16.54 -4 9 8 192.07 18.56 -4 9 7 53.23 9.48 4 9 -7 56.29 7.83 -4 9 7 62.10 8.20 -4 9 6 112.01 12.87 -4 9 6 87.88 10.60 4 9 -6 103.14 10.32 -4 9 5 44.88 8.70 4 9 -5 29.80 5.87 -4 9 5 33.55 6.59 4 9 -4 427.53 31.77 -4 9 4 411.51 33.78 -4 9 4 377.51 32.28 -4 9 3 317.25 27.12 -4 9 3 307.70 28.12 4 9 -3 361.11 26.41 -4 9 2 8.07 5.37 -4 9 2 17.79 6.82 4 9 -2 21.20 4.62 -4 9 1 241.58 21.45 -4 9 1 244.04 22.20 4 9 -1 264.29 20.13 -4 9 0 294.65 25.39 4 9 0 305.71 23.35 4 9 1 81.21 6.92 4 9 1 78.38 6.55 -4 9 -1 93.82 10.12 4 9 1 94.44 7.69 4 9 2 151.45 11.64 4 9 2 138.19 11.20 -4 9 -2 142.20 13.69 4 9 3 56.83 5.32 -4 9 -3 58.92 7.71 -4 9 -3 51.85 7.75 4 9 3 60.67 5.52 4 9 4 65.45 5.85 -4 9 -4 64.19 7.56 4 9 4 53.28 5.11 4 9 4 53.92 4.98 4 9 5 15.40 3.09 -4 9 -5 22.69 4.88 -4 9 -5 17.36 5.56 -4 9 -6 263.71 22.58 4 9 6 255.64 20.79 -4 9 -6 277.94 22.00 -4 9 -7 219.26 19.07 -4 9 -7 230.81 16.48 4 9 7 199.19 18.08 -4 9 -7 214.58 19.77 -4 9 -8 133.37 13.35 -4 9 -8 118.40 12.08 4 9 8 104.05 11.47 -4 9 -8 135.03 9.72 -4 9 -9 116.56 12.41 4 9 9 90.99 10.62 -4 9 -9 120.62 8.82 -4 9 -9 121.23 11.56 -4 9 -10 13.21 1.83 4 9 10 5.88 3.25 -4 9 -10 9.82 4.99 -4 9 -10 11.05 3.89 -4 9 -11 251.35 17.69 -4 9 -11 228.10 21.27 -4 9 -11 233.89 20.40 4 9 11 188.62 19.85 -4 9 -12 5.65 1.61 -4 9 -12 6.62 3.64 4 9 12 0.47 3.53 -4 9 -13 34.66 5.88 -4 9 -13 43.22 7.43 -4 9 -13 40.23 3.48 4 9 14 21.54 5.03 -4 9 -14 26.12 2.75 -4 9 -14 23.67 5.88 -4 9 -15 45.68 3.99 -4 9 -15 42.81 3.72 -4 9 -16 46.22 4.00 -4 9 -16 38.69 3.59 -4 9 -17 74.10 5.66 -4 9 -17 66.55 5.61 -4 9 -17 71.76 5.96 -4 9 -18 73.02 5.68 -4 9 -18 64.45 5.25 -4 9 -18 59.49 5.20 -4 9 -19 49.67 4.27 -4 9 -19 48.31 4.22 -4 9 -20 38.82 3.38 -4 9 -20 30.34 3.20 -4 9 -21 63.74 5.15 -4 9 -21 57.15 4.99 -4 9 -22 15.56 2.39 -4 9 -22 9.62 1.94 -4 9 -23 10.53 2.26 -4 9 -23 11.22 1.96 -4 9 -24 138.08 9.59 -4 9 -24 110.52 9.39 -4 9 -25 14.35 2.66 -4 9 -26 11.22 2.65 -4 9 -27 4.14 2.41 -4 9 -28 31.83 3.54 -4 9 -29 15.84 2.74 -4 9 -30 11.68 2.47 -4 9 -31 2.45 2.03 -4 9 -32 5.22 2.00 -4 9 -33 6.74 1.81 -4 9 -34 9.41 1.75 -4 9 -35 5.22 2.01 -4 9 -36 0.76 1.57 4 10 -37 0.83 1.14 4 10 -36 2.74 1.55 4 10 -35 10.68 2.08 4 10 -34 3.16 2.11 4 10 -33 9.26 2.44 4 10 -32 -0.30 2.38 4 10 -31 29.43 3.76 4 10 -30 23.18 3.52 4 10 -29 13.57 3.20 4 10 -28 33.48 4.18 4 10 -27 6.56 2.98 4 10 -26 1.61 2.87 4 10 -25 27.77 3.72 4 10 -24 23.84 3.43 4 10 -23 9.79 3.17 4 10 -23 10.06 2.71 4 10 -22 46.43 5.22 4 10 -22 57.51 4.98 4 10 -21 21.02 3.38 4 10 -21 22.55 2.93 4 10 -21 24.11 3.16 4 10 -20 45.58 4.10 4 10 -20 39.95 4.35 4 10 -20 39.90 3.97 4 10 -19 59.36 5.13 4 10 -19 58.52 5.08 4 10 -19 59.98 5.39 4 10 -18 60.73 5.45 4 10 -18 68.41 5.28 4 10 -18 58.13 5.15 4 10 -17 4.14 1.53 4 10 -17 4.11 1.78 4 10 -17 1.98 1.90 4 10 -16 12.94 2.35 4 10 -16 20.30 2.17 4 10 -16 19.80 2.32 4 10 -15 35.38 3.32 -4 10 15 34.51 6.62 -4 10 14 55.33 8.13 4 10 -14 48.47 4.19 -4 10 13 69.04 9.27 -4 10 12 2.35 4.06 4 10 -12 20.34 5.21 -4 10 11 31.75 8.14 -4 10 11 39.83 6.78 4 10 -11 34.09 6.63 -4 10 10 42.77 7.23 -4 10 10 43.99 8.91 4 10 -10 43.95 6.95 4 10 -9 71.04 9.25 -4 10 9 75.54 9.43 -4 10 9 76.71 11.09 -4 10 8 43.37 8.49 4 10 -8 30.31 6.26 -4 10 8 39.30 6.78 -4 10 7 -3.56 6.06 4 10 -7 0.44 4.19 -4 10 7 2.51 4.47 -4 10 6 200.69 18.78 4 10 -6 223.29 18.47 -4 10 6 203.92 20.24 -4 10 5 37.94 8.44 -4 10 5 35.81 6.58 4 10 -5 35.45 5.97 -4 10 4 79.41 9.64 4 10 -4 87.19 9.24 -4 10 4 82.00 11.51 -4 10 3 188.82 18.97 4 10 -3 198.60 16.71 -4 10 3 198.59 17.89 -4 10 2 286.32 25.55 -4 10 2 322.67 27.02 4 10 -2 318.14 24.52 -4 10 1 233.11 21.51 -4 10 1 269.61 22.63 4 10 -1 255.13 20.13 -4 10 0 -0.47 4.69 4 10 0 3.94 2.47 -4 10 0 3.64 5.21 4 10 1 55.35 4.74 4 10 1 78.92 6.20 -4 10 -1 79.38 8.86 4 10 1 50.05 5.03 4 10 2 38.98 3.94 4 10 2 41.02 4.39 -4 10 -2 36.14 6.52 4 10 2 40.12 4.57 4 10 3 15.55 2.65 -4 10 -3 19.03 5.04 4 10 3 16.51 2.56 4 10 4 99.46 8.24 -4 10 -4 110.22 11.56 4 10 4 95.69 8.49 4 10 4 101.74 8.80 -4 10 -4 113.28 10.88 -4 10 -5 142.34 8.61 -4 10 -5 138.70 11.85 -4 10 -5 148.72 12.85 4 10 5 138.79 10.12 4 10 5 90.99 8.54 4 10 5 89.83 8.66 -4 10 -6 25.39 6.59 -4 10 -6 29.98 2.81 -4 10 -6 30.81 5.57 -4 10 -7 33.43 3.06 4 10 7 29.33 4.73 -4 10 -7 30.59 5.57 -4 10 -7 41.61 7.14 4 10 8 50.52 6.81 -4 10 -8 61.92 7.64 -4 10 -8 60.20 8.67 -4 10 -8 61.97 4.89 -4 10 -9 69.19 5.52 4 10 9 64.29 7.58 -4 10 -9 62.46 8.93 -4 10 -9 75.83 8.35 4 10 10 19.14 4.61 -4 10 -10 24.50 6.43 -4 10 -10 27.76 2.74 -4 10 -10 27.67 5.19 4 10 11 5.34 3.37 -4 10 -11 4.27 3.59 -4 10 -11 8.11 5.14 -4 10 -11 6.44 1.73 4 10 12 8.72 3.90 -4 10 -12 7.83 5.04 -4 10 -12 8.01 3.63 -4 10 -12 11.11 1.89 -4 10 -13 34.42 5.79 -4 10 -13 24.59 6.28 -4 10 -13 29.34 3.05 4 10 13 25.24 5.36 -4 10 -14 3.23 1.73 4 10 14 4.56 3.37 -4 10 -15 16.12 2.38 -4 10 -16 44.61 4.06 -4 10 -16 41.30 3.68 -4 10 -17 15.85 2.14 -4 10 -17 21.66 2.82 -4 10 -18 1.53 1.44 -4 10 -18 1.49 1.68 -4 10 -18 1.76 2.21 -4 10 -19 84.42 6.33 -4 10 -19 69.98 6.19 -4 10 -19 84.23 6.69 -4 10 -20 3.82 1.87 -4 10 -20 8.18 2.74 -4 10 -20 6.82 1.70 -4 10 -21 4.38 1.66 -4 10 -21 5.08 2.78 -4 10 -21 5.40 2.04 -4 10 -22 47.04 4.63 -4 10 -22 40.68 3.93 -4 10 -22 36.93 3.63 -4 10 -23 10.47 3.27 -4 10 -23 11.39 2.34 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11 11 21.16 5.49 -4 11 10 5.08 5.62 4 11 -10 7.02 4.35 -4 11 10 8.79 4.84 -4 11 9 98.31 12.94 4 11 -9 99.14 11.21 -4 11 9 94.21 11.16 -4 11 8 27.77 7.99 -4 11 8 41.06 7.07 4 11 -8 43.55 6.85 -4 11 7 19.20 7.43 4 11 -7 23.50 5.47 -4 11 7 23.23 5.74 -4 11 6 98.85 12.41 -4 11 6 78.02 10.31 4 11 -6 102.74 10.46 4 11 -5 58.25 7.61 -4 11 5 56.88 8.31 -4 11 5 42.34 9.51 4 11 -4 306.93 22.91 -4 11 4 252.18 23.27 -4 11 4 251.88 24.74 -4 11 3 90.24 7.41 4 11 -3 108.09 9.94 -4 11 3 117.49 11.39 -4 11 3 89.15 12.41 4 11 -2 14.78 4.09 -4 11 2 13.65 5.47 -4 11 2 13.51 2.12 -4 11 2 16.98 6.88 4 11 -1 101.95 8.74 -4 11 1 80.64 6.60 -4 11 1 82.97 10.83 -4 11 1 78.55 10.00 -4 11 0 37.44 3.51 -4 11 0 47.97 7.77 -4 11 0 39.77 7.21 4 11 0 43.43 5.00 -4 11 -1 9.65 1.68 4 11 1 6.26 1.13 4 11 1 13.76 2.61 -4 11 -1 7.46 5.06 -4 11 -1 11.85 5.21 4 11 1 7.29 1.46 4 11 2 1.74 1.50 -4 11 -2 1.16 1.43 4 11 2 0.20 2.33 -4 11 -2 3.03 4.49 4 11 2 3.04 2.00 4 11 3 9.05 3.26 4 11 3 6.56 2.01 4 11 3 3.74 1.76 4 11 3 9.86 3.03 -4 11 -3 7.11 1.57 -4 11 -3 10.00 1.62 -4 11 -3 7.71 4.58 -4 11 -4 12.18 1.82 -4 11 -4 11.17 1.78 4 11 4 12.96 2.28 4 11 4 10.14 3.80 4 11 4 13.35 2.50 4 11 4 12.11 2.81 -4 11 -4 16.76 5.17 4 11 5 18.59 3.02 -4 11 -5 13.96 1.85 -4 11 -5 14.90 1.92 -4 11 -5 12.76 4.78 -4 11 -5 9.41 5.35 4 11 5 11.65 1.93 4 11 5 14.77 2.41 -4 11 -6 30.72 6.09 4 11 6 39.47 4.95 -4 11 -6 38.96 3.53 -4 11 -6 29.02 6.95 -4 11 -6 46.32 3.65 -4 11 -7 101.58 7.60 -4 11 -7 100.66 7.63 -4 11 -7 92.14 11.32 4 11 7 82.29 9.11 -4 11 -7 102.88 10.62 -4 11 -8 53.97 4.37 4 11 8 38.21 5.88 -4 11 -8 45.49 7.96 -4 11 -8 53.74 4.31 -4 11 -8 41.88 6.73 4 11 9 4.64 2.95 -4 11 -9 4.69 1.47 -4 11 -9 2.82 3.30 -4 11 -9 8.81 4.82 -4 11 -9 5.67 1.61 -4 11 -10 30.70 6.73 -4 11 -10 38.61 3.26 4 11 10 27.53 5.15 -4 11 -10 27.65 5.47 -4 11 -10 32.62 3.11 -4 11 -11 5.90 1.78 -4 11 -11 7.77 1.66 -4 11 -11 6.81 4.32 -4 11 -11 11.10 3.93 4 11 11 8.77 3.57 -4 11 -12 7.44 3.71 -4 11 -12 15.53 2.14 4 11 12 10.55 4.12 -4 11 -12 18.83 2.34 4 11 13 8.17 3.79 -4 11 -13 12.71 2.01 -4 11 -13 14.23 2.18 -4 11 -14 9.84 2.06 -4 11 -14 5.92 1.89 -4 11 -15 17.38 2.43 -4 11 -15 13.75 2.30 -4 11 -16 -0.36 1.93 -4 11 -16 -0.40 2.14 -4 11 -16 0.53 1.34 -4 11 -17 58.27 4.78 -4 11 -17 56.64 4.87 -4 11 -17 46.62 4.38 -4 11 -18 4.85 2.31 -4 11 -18 9.81 2.50 -4 11 -18 5.56 1.88 -4 11 -18 5.86 1.62 -4 11 -19 23.35 3.26 -4 11 -19 26.48 3.21 -4 11 -19 28.65 2.83 -4 11 -19 17.12 2.43 -4 11 -20 15.37 2.96 -4 11 -20 12.34 2.87 -4 11 -20 11.39 2.30 -4 11 -20 12.24 1.97 -4 11 -21 29.51 3.79 -4 11 -21 23.13 3.46 -4 11 -21 21.92 2.93 -4 11 -21 24.81 2.65 -4 11 -22 16.93 3.29 -4 11 -22 14.80 2.52 -4 11 -22 16.28 3.40 -4 11 -23 11.35 3.16 -4 11 -23 11.04 2.48 -4 11 -23 14.92 3.39 -4 11 -24 65.72 6.03 -4 11 -24 58.47 5.44 -4 11 -24 63.82 6.14 -4 11 -25 15.53 3.60 -4 11 -25 10.81 3.58 -4 11 -25 12.21 2.66 -4 11 -26 16.26 3.88 -4 11 -26 17.14 2.92 -4 11 -26 21.62 3.98 -4 11 -27 8.84 3.53 -4 11 -27 9.20 2.48 -4 11 -27 9.27 3.59 -4 11 -28 44.87 5.34 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12.78 6.24 -4 12 8 15.52 5.19 4 12 -8 22.24 5.28 -4 12 7 61.88 9.71 -4 12 7 44.84 7.50 4 12 -7 44.72 7.03 -4 12 6 36.47 6.92 4 12 -6 38.92 6.46 -4 12 6 34.32 8.15 -4 12 5 12.89 5.09 4 12 -5 20.39 4.88 -4 12 5 6.93 5.93 4 12 -4 -0.42 3.76 -4 12 4 -2.77 4.59 -4 12 4 0.54 1.75 -4 12 4 -2.22 6.12 4 12 -3 33.65 5.48 -4 12 3 27.20 3.03 -4 12 3 22.06 6.19 -4 12 3 31.14 7.65 -4 12 2 94.36 11.32 -4 12 2 103.62 7.80 4 12 -2 107.50 10.16 -4 12 2 96.56 7.84 -4 12 2 95.23 12.24 4 12 -1 77.23 8.03 -4 12 1 75.77 6.16 -4 12 1 75.14 6.10 -4 12 1 85.74 10.79 -4 12 1 87.53 9.95 -4 12 0 43.72 7.56 4 12 0 36.05 4.87 -4 12 0 38.89 3.47 -4 12 0 36.79 3.43 -4 12 0 28.46 6.51 -4 12 -1 4.59 1.57 -4 12 -1 4.31 1.63 -4 12 -1 0.57 4.36 -4 12 -1 6.21 4.94 4 12 1 8.76 2.54 4 12 2 3.53 2.22 -4 12 -2 1.25 1.38 4 12 2 6.65 3.16 4 12 2 3.01 1.43 -4 12 -2 5.09 1.53 -4 12 -2 5.44 4.28 4 12 2 2.20 1.86 -4 12 -2 10.90 5.27 4 12 3 5.34 1.88 4 12 3 6.36 3.09 4 12 3 5.30 1.90 -4 12 -3 2.44 1.53 4 12 3 1.90 2.92 -4 12 -3 1.57 4.21 -4 12 -3 5.62 1.55 -4 12 -4 6.33 1.56 -4 12 -4 4.65 1.52 4 12 4 2.83 2.72 4 12 4 6.15 3.45 4 12 4 1.93 1.66 4 12 4 2.83 1.78 -4 12 -5 42.55 3.50 4 12 5 36.81 3.77 -4 12 -5 41.58 3.50 4 12 5 44.91 6.05 4 12 5 32.39 4.36 -4 12 -5 38.06 6.39 4 12 5 29.88 4.12 -4 12 -6 6.38 1.56 4 12 6 5.96 3.49 -4 12 -6 7.62 1.59 4 12 6 3.19 2.15 -4 12 -6 -1.88 5.00 -4 12 -6 7.34 3.83 -4 12 -7 13.71 4.67 4 12 7 24.56 3.99 -4 12 -7 25.03 2.53 -4 12 -7 23.20 6.23 -4 12 -7 25.69 2.56 -4 12 -8 21.60 2.36 4 12 8 15.65 3.66 -4 12 -8 17.35 4.55 -4 12 -8 15.98 5.59 -4 12 -8 22.95 2.43 -4 12 -9 9.09 4.00 -4 12 -9 7.02 1.70 4 12 9 1.60 2.56 -4 12 -9 11.69 1.79 -4 12 -9 5.51 4.64 -4 12 -10 55.48 4.27 -4 12 -10 52.00 4.32 -4 12 -11 9.89 1.78 -4 12 -11 10.22 3.98 4 12 11 6.22 3.28 -4 12 -11 6.82 1.82 -4 12 -12 77.48 6.17 -4 12 -12 84.15 6.29 -4 12 -13 9.50 2.00 -4 12 -13 9.43 2.19 -4 12 -14 4.80 1.89 -4 12 -14 1.48 2.05 -4 12 -15 22.93 2.86 -4 12 -15 25.49 3.08 -4 12 -16 3.56 2.00 -4 12 -16 0.09 2.33 -4 12 -16 1.91 1.46 -4 12 -17 31.18 3.36 -4 12 -17 34.19 3.58 -4 12 -17 24.18 2.81 -4 12 -18 7.07 2.67 -4 12 -18 3.21 2.30 -4 12 -18 2.26 1.52 -4 12 -19 29.59 3.63 -4 12 -19 29.77 3.34 -4 12 -19 26.83 3.07 -4 12 -19 21.74 2.67 -4 12 -20 4.28 2.59 -4 12 -20 4.71 2.81 -4 12 -20 2.67 2.11 -4 12 -20 0.67 1.56 -4 12 -21 14.97 3.00 -4 12 -21 14.01 2.54 -4 12 -21 11.69 3.23 -4 12 -22 10.64 3.25 -4 12 -22 10.04 2.45 -4 12 -22 10.20 3.04 -4 12 -23 0.78 2.86 -4 12 -23 4.89 3.26 -4 12 -23 5.44 2.35 -4 12 -24 21.07 3.95 -4 12 -24 20.38 3.68 -4 12 -24 20.33 2.92 -4 12 -25 13.85 3.38 -4 12 -25 13.60 2.65 -4 12 -25 16.77 3.76 -4 12 -26 43.81 4.79 -4 12 -26 37.36 4.08 -4 12 -26 42.30 4.95 -4 12 -27 11.92 3.54 -4 12 -27 6.55 3.01 -4 12 -27 3.12 2.26 -4 12 -28 23.63 3.10 -4 12 -28 24.16 3.84 -4 12 -28 24.49 3.93 -4 12 -29 1.12 2.09 -4 12 -29 6.41 3.23 -4 12 -29 2.06 2.81 -4 12 -30 4.51 2.08 -4 12 -30 1.34 2.61 -4 12 -30 1.58 2.92 -4 12 -31 8.72 2.68 -4 12 -31 3.44 2.78 -4 12 -31 2.47 1.88 -4 12 -32 14.71 2.97 -4 12 -32 13.70 2.18 -4 12 -33 4.76 2.32 -4 12 -33 1.83 1.49 -4 12 -34 0.17 1.72 4 13 -35 3.81 1.52 4 13 -34 4.48 1.85 4 13 -33 0.61 1.93 4 13 -32 0.07 2.05 4 13 -31 7.14 2.44 4 13 -30 5.45 2.54 4 13 -29 15.06 2.95 4 13 -28 3.44 2.65 4 13 -27 6.61 2.90 4 13 -26 3.55 2.70 4 13 -25 20.11 3.28 4 13 -24 9.27 2.88 4 13 -23 21.98 3.33 4 13 -22 20.44 3.17 4 13 -21 16.42 2.96 4 13 -21 13.70 2.85 4 13 -20 -2.94 2.28 4 13 -20 2.32 2.39 4 13 -19 31.11 3.69 4 13 -19 40.14 3.89 4 13 -18 38.14 3.42 4 13 -18 21.15 3.24 -4 13 11 24.07 6.14 -4 13 10 11.42 4.75 4 13 -9 87.20 10.72 -4 13 9 90.22 10.95 -4 13 8 31.90 8.15 -4 13 8 36.60 6.75 4 13 -8 35.58 6.62 -4 13 7 13.83 5.09 4 13 -7 16.95 4.81 -4 13 7 16.76 6.67 -4 13 6 8.02 4.57 4 13 -6 3.17 3.91 -4 13 6 2.56 5.31 4 13 -5 16.79 4.48 -4 13 5 12.16 5.11 -4 13 5 15.76 2.50 -4 13 5 12.33 6.33 4 13 -4 6.91 3.84 -4 13 4 6.79 2.01 -4 13 4 9.65 4.90 -4 13 4 1.58 5.41 -4 13 3 32.51 3.53 -4 13 3 40.82 3.47 4 13 -3 27.78 5.34 -4 13 3 40.79 8.23 -4 13 3 35.45 6.94 -4 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1.82 -4 13 -7 9.99 1.81 -4 13 -8 12.29 2.01 -4 13 -8 12.89 2.03 -4 13 -8 9.06 4.10 -4 13 -9 9.47 1.92 -4 13 -9 8.67 3.75 -4 13 -9 8.43 1.87 -4 13 -10 47.59 4.14 -4 13 -10 45.85 4.05 -4 13 -11 15.44 2.40 -4 13 -11 15.67 2.32 -4 13 -12 25.33 2.87 -4 13 -12 26.72 3.09 -4 13 -13 -0.24 2.14 -4 13 -13 0.72 1.84 -4 13 -14 44.02 4.05 -4 13 -14 42.19 4.24 -4 13 -15 47.17 4.44 -4 13 -15 43.76 4.26 -4 13 -16 19.51 2.98 -4 13 -16 15.74 2.67 -4 13 -16 12.81 2.07 -4 13 -17 91.02 6.92 -4 13 -17 73.42 6.48 -4 13 -17 91.05 7.06 -4 13 -18 3.37 2.55 -4 13 -18 2.63 2.69 -4 13 -18 1.92 1.55 -4 13 -19 31.88 3.14 -4 13 -19 30.40 3.78 -4 13 -19 24.83 3.49 -4 13 -19 19.46 2.67 -4 13 -20 11.98 3.18 -4 13 -20 15.11 3.07 -4 13 -20 9.75 2.43 -4 13 -21 3.82 2.79 -4 13 -21 5.55 2.33 -4 13 -21 6.96 3.06 -4 13 -22 7.00 3.15 -4 13 -22 4.92 2.29 -4 13 -22 9.21 3.06 -4 13 -23 33.46 4.41 -4 13 -23 34.91 4.34 -4 13 -23 33.70 3.68 -4 13 -24 2.58 3.26 -4 13 -24 2.87 2.31 -4 13 -24 3.23 2.96 -4 13 -25 4.04 3.21 -4 13 -25 0.16 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11.78 -4 14 6 107.77 14.04 4 14 -5 17.18 4.70 -4 14 5 19.13 5.79 -4 14 5 16.06 2.72 -4 14 5 27.01 7.31 4 14 -4 14.04 4.31 -4 14 4 14.10 2.40 -4 14 4 12.44 2.10 -4 14 4 15.73 5.26 -4 14 4 5.02 5.96 -4 14 3 28.13 6.33 4 14 -3 19.11 4.66 -4 14 3 25.30 2.76 -4 14 3 25.85 2.99 -4 14 3 21.62 6.86 -4 14 2 -2.63 4.67 -4 14 2 -0.87 1.68 -4 14 2 -1.33 1.90 4 14 -2 5.62 3.19 -4 14 2 -3.82 5.38 -4 14 1 24.57 2.75 -4 14 1 26.65 2.90 -4 14 1 23.27 6.69 4 14 -1 25.55 4.50 -4 14 1 25.12 6.40 4 14 0 37.01 4.97 -4 14 0 32.14 3.26 -4 14 0 34.12 3.37 -4 14 0 29.06 6.93 -4 14 0 40.03 7.34 -4 14 -1 12.03 2.01 4 14 1 12.36 2.91 -4 14 -1 9.19 5.18 4 14 1 11.68 4.04 -4 14 -1 12.80 2.11 -4 14 -1 6.76 4.98 -4 14 -2 18.57 2.28 -4 14 -2 20.43 2.54 -4 14 -2 15.09 5.19 -4 14 -2 15.81 5.68 -4 14 -3 -3.02 4.34 -4 14 -3 2.67 1.58 -4 14 -3 5.90 1.79 -4 14 -3 5.61 4.79 -4 14 -4 10.12 1.91 -4 14 -4 13.18 2.04 -4 14 -4 10.03 5.76 -4 14 -4 8.78 4.36 -4 14 -5 0.86 1.52 -4 14 -5 3.05 1.67 -4 14 -5 3.45 3.80 -4 14 -6 6.52 1.83 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7.20 2.72 7 7 -25 -1.93 2.44 7 7 -24 10.78 2.68 7 7 -23 94.91 7.76 7 7 -22 9.48 2.40 7 7 -21 29.25 3.38 7 7 -20 11.04 2.27 7 7 -19 18.41 2.53 7 7 -18 7.31 1.83 7 7 -17 66.74 5.43 7 7 -16 3.01 1.49 7 7 -15 37.93 3.29 -7 7 15 35.85 3.27 7 7 -14 9.18 1.48 -7 7 14 3.95 1.40 7 7 -13 12.71 1.70 -7 7 13 12.93 1.79 7 7 -12 5.56 1.29 -7 7 12 5.46 1.37 7 7 -11 70.67 10.16 -7 7 11 84.72 11.68 7 7 -11 73.33 5.83 -7 7 11 80.72 5.99 7 7 -10 15.34 5.66 -7 7 10 18.90 5.59 -7 7 10 18.19 2.03 -7 7 10 20.59 6.91 7 7 -9 92.56 11.69 -7 7 9 102.88 7.85 -7 7 9 120.07 12.39 -7 7 9 97.77 12.77 7 7 -8 214.63 21.01 -7 7 8 234.96 21.62 -7 7 8 237.42 17.35 -7 7 8 254.29 22.82 -7 7 7 58.55 4.72 -7 7 7 61.13 9.62 7 7 -7 52.68 8.26 7 7 -6 145.93 13.74 -7 7 6 128.04 9.80 -7 7 6 156.23 15.34 -7 7 5 86.72 11.17 7 7 -5 78.16 9.45 -7 7 4 125.00 12.68 7 7 -4 106.01 11.62 -7 7 4 110.73 8.61 -7 7 4 129.60 13.58 -7 7 3 29.15 6.36 -7 7 3 22.78 2.60 7 7 -3 22.98 5.87 -7 7 3 25.86 6.67 -7 7 2 494.14 36.04 -7 7 2 429.81 31.84 7 7 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4.67 -7 8 -7 50.02 7.68 7 8 7 45.56 6.41 -7 8 -7 53.06 8.45 -7 8 -7 56.89 4.62 -7 8 -8 43.19 3.56 -7 8 -8 37.47 3.78 -7 8 -8 42.96 6.87 -7 8 -8 39.09 3.70 7 8 8 42.53 5.99 -7 8 -8 43.50 7.41 -7 8 -9 33.81 3.34 -7 8 -9 36.55 3.18 -7 8 -9 31.87 3.46 7 8 9 37.10 5.92 -7 8 -9 27.74 6.69 -7 8 -10 16.37 2.35 -7 8 -10 17.44 2.12 7 8 10 16.00 4.53 -7 8 -10 12.56 5.28 -7 8 -11 14.16 2.23 -7 8 -11 15.55 2.10 7 8 11 10.81 4.22 -7 8 -11 6.78 4.58 -7 8 -12 44.16 3.90 -7 8 -12 41.25 3.74 7 8 12 30.67 6.34 -7 8 -12 37.54 7.10 -7 8 -13 32.45 3.23 -7 8 -13 31.47 3.34 -7 8 -14 100.09 7.59 -7 8 -14 92.02 7.71 -7 8 -15 32.76 3.51 -7 8 -15 36.11 3.30 -7 8 -15 26.84 3.28 -7 8 -16 20.36 2.78 -7 8 -16 22.36 3.00 -7 8 -16 19.28 2.77 -7 8 -17 9.16 2.51 -7 8 -17 7.80 2.24 -7 8 -17 7.93 2.29 -7 8 -18 27.71 3.62 -7 8 -18 35.86 3.46 -7 8 -18 26.20 3.36 -7 8 -19 128.06 10.56 -7 8 -19 142.00 10.47 -7 8 -19 130.92 10.39 -7 8 -20 37.41 4.03 -7 8 -20 38.84 4.21 -7 8 -20 32.88 3.79 -7 8 -21 13.62 3.33 -7 8 -21 18.65 3.18 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30.87 3.56 7 11 -22 9.44 2.51 7 11 -21 23.18 3.05 7 11 -20 6.29 2.27 7 11 -19 1.81 1.96 7 11 -18 90.61 7.29 7 11 -17 123.71 9.55 7 11 -16 35.51 3.52 7 11 -15 14.13 2.19 7 11 -14 20.33 2.41 7 11 -13 181.66 13.51 7 11 -12 41.20 3.59 7 11 -8 44.44 7.74 7 11 -7 72.01 9.33 7 11 -6 24.47 5.91 -7 11 6 36.74 3.72 7 11 -5 8.16 4.26 -7 11 5 17.04 2.59 -7 11 4 19.89 2.77 7 11 -4 22.87 5.17 7 11 -3 71.00 8.46 -7 11 3 67.10 6.02 -7 11 3 73.40 5.54 -7 11 3 68.27 5.92 -7 11 2 51.16 4.63 -7 11 2 42.27 4.41 -7 11 2 53.09 4.09 7 11 -2 44.77 6.64 -7 11 1 77.90 6.63 -7 11 1 73.18 10.78 -7 11 1 80.99 6.54 -7 11 1 82.14 6.29 -7 11 1 83.99 11.13 -7 11 0 19.17 2.81 -7 11 0 21.37 2.17 -7 11 0 16.54 2.55 -7 11 0 7.70 5.38 -7 11 0 10.46 5.82 -7 11 -1 37.30 3.80 -7 11 -1 38.78 7.84 -7 11 -1 33.91 3.56 -7 11 -1 38.16 3.35 -7 11 -1 29.85 7.25 -7 11 -2 90.12 7.27 -7 11 -2 89.95 7.18 -7 11 -2 89.91 7.02 -7 11 -2 89.76 11.69 -7 11 -3 163.09 13.39 -7 11 -3 181.19 13.33 -7 11 -3 184.55 13.25 -7 11 -4 177.03 14.01 -7 11 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-8 5 -4 29.81 3.15 -8 5 -4 29.27 5.69 8 5 4 30.56 5.46 -8 5 -4 30.45 3.06 -8 5 -5 81.97 10.17 -8 5 -5 88.70 6.65 -8 5 -5 95.53 10.08 -8 5 -5 78.53 6.95 -8 5 -5 92.09 6.83 8 5 5 63.85 9.20 -8 5 -5 91.41 6.89 -8 5 -6 11.65 1.92 -8 5 -6 9.67 1.67 -8 5 -6 10.96 4.64 -8 5 -6 7.70 1.40 -8 5 -6 15.60 4.71 8 5 6 9.28 4.19 -8 5 -7 16.10 2.37 -8 5 -7 26.33 5.21 -8 5 -7 19.16 2.18 -8 5 -7 19.55 2.01 -8 5 -7 25.56 5.13 8 5 7 17.09 4.71 -8 5 -8 8.00 2.07 -8 5 -8 3.72 3.58 -8 5 -8 10.67 1.67 -8 5 -8 10.23 1.49 -8 5 -8 14.23 4.61 8 5 8 9.86 4.29 -8 5 -9 24.73 5.57 -8 5 -9 36.05 3.11 -8 5 -9 36.29 3.28 8 5 9 36.21 6.26 -8 5 -10 21.21 5.17 -8 5 -10 33.94 2.89 -8 5 -10 29.74 3.07 -8 5 -10 32.61 3.36 8 5 10 29.11 5.91 -8 5 -11 14.76 1.90 -8 5 -11 15.13 2.55 8 5 11 13.58 4.73 -8 5 -11 17.33 2.20 -8 5 -12 27.66 3.01 -8 5 -12 32.19 2.88 -8 5 -13 5.55 1.76 -8 5 -13 6.67 1.61 -8 5 -13 2.41 1.97 -8 5 -14 17.11 2.57 -8 5 -14 20.03 2.33 -8 5 -14 18.22 2.68 -8 5 -15 9.24 1.87 -8 5 -15 7.53 2.12 -8 5 -15 6.57 2.20 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6.21 2.16 -8 5 -30 22.38 3.15 -8 5 -30 25.73 2.94 -8 5 -31 11.47 2.41 -8 5 -31 10.80 2.00 -8 5 -32 8.08 2.17 -8 5 -32 10.16 1.69 -8 5 -33 8.17 1.86 8 6 -35 7.62 1.36 8 6 -34 2.43 1.48 8 6 -33 12.47 2.13 8 6 -32 2.44 2.00 8 6 -31 1.97 2.22 8 6 -30 3.55 2.39 8 6 -29 11.47 2.58 8 6 -28 12.64 2.68 8 6 -27 2.84 2.27 8 6 -26 1.77 2.36 8 6 -25 10.34 2.55 8 6 -24 11.33 2.56 8 6 -23 0.08 2.18 8 6 -22 34.10 3.65 8 6 -21 4.07 2.10 -8 6 21 4.90 1.73 8 6 -20 23.22 2.82 -8 6 20 21.63 2.55 8 6 -19 2.47 1.80 -8 6 19 1.72 1.54 8 6 -18 35.58 3.44 -8 6 18 35.78 3.38 8 6 -17 2.20 1.59 -8 6 17 4.58 1.52 8 6 -16 28.00 2.91 -8 6 16 30.91 2.99 8 6 -15 -1.34 1.33 -8 6 15 -1.24 1.55 8 6 -14 19.68 2.17 -8 6 14 22.40 2.40 -8 6 13 3.31 1.51 -8 6 12 58.05 4.81 -8 6 11 47.99 4.17 -8 6 10 138.17 10.46 -8 6 9 93.12 7.30 8 6 -9 89.90 11.43 -8 6 9 96.89 12.21 8 6 -8 128.17 13.97 -8 6 8 123.59 9.51 -8 6 8 130.70 14.44 -8 6 7 36.56 7.46 -8 6 7 41.52 3.77 8 6 -7 42.07 7.49 -8 6 7 46.46 8.23 -8 6 6 11.80 1.59 -8 6 6 14.55 5.47 8 6 -6 21.09 5.55 -8 6 6 13.00 1.95 -8 6 6 12.93 5.94 -8 6 5 28.12 2.73 8 6 -5 31.36 6.20 -8 6 5 33.36 3.01 -8 6 5 32.65 3.03 -8 6 5 24.93 6.83 -8 6 5 35.54 6.88 -8 6 4 18.89 2.12 8 6 -4 19.00 5.61 -8 6 4 20.29 2.40 -8 6 4 22.49 2.40 -8 6 4 28.50 6.80 -8 6 4 19.81 5.72 8 6 -3 221.48 20.20 -8 6 3 225.39 16.98 -8 6 3 236.14 21.08 -8 6 3 240.93 17.09 -8 6 3 230.21 17.11 -8 6 3 254.93 21.50 -8 6 2 40.70 3.64 8 6 -2 46.83 7.07 -8 6 2 46.85 3.73 -8 6 2 43.18 3.83 -8 6 2 33.05 7.18 -8 6 2 49.13 7.73 -8 6 1 58.22 4.71 8 6 -1 60.06 6.33 8 6 -1 58.56 7.77 -8 6 1 52.00 4.87 -8 6 1 60.98 4.75 -8 6 1 59.68 4.87 -8 6 1 76.68 9.15 -8 6 1 60.99 8.58 -8 6 0 86.82 6.84 -8 6 0 92.87 6.85 -8 6 0 89.76 6.96 -8 6 0 104.73 11.16 -8 6 0 93.87 10.60 8 6 0 92.67 9.67 8 6 0 83.11 8.62 -8 6 0 84.43 6.98 -8 6 -1 13.68 1.83 8 6 1 7.95 3.55 -8 6 -1 14.19 2.01 -8 6 -1 19.52 5.47 -8 6 -1 13.33 1.72 -8 6 -1 13.37 2.04 -8 6 -1 9.38 4.56 8 6 1 10.44 4.20 -8 6 -2 38.62 3.45 8 6 2 30.32 5.30 -8 6 -2 37.20 3.60 -8 6 -2 40.85 3.59 -8 6 -2 37.85 6.95 -8 6 -2 40.57 3.35 -8 6 -2 36.49 6.49 8 6 2 39.47 5.60 -8 6 -3 5.12 1.62 -8 6 -3 10.15 1.82 -8 6 -3 12.82 5.03 -8 6 -3 9.59 1.48 -8 6 -3 7.29 1.90 -8 6 -3 9.22 4.36 8 6 3 12.54 3.29 8 6 3 12.18 3.84 -8 6 -4 81.18 6.53 -8 6 -4 94.62 10.43 -8 6 -4 90.04 6.39 -8 6 -4 72.84 6.58 -8 6 -4 71.61 9.49 8 6 4 72.24 8.85 -8 6 -4 84.81 6.53 -8 6 -5 20.75 2.31 -8 6 -5 20.13 2.02 -8 6 -5 16.90 2.50 -8 6 -5 18.06 2.25 -8 6 -5 20.79 5.20 -8 6 -5 10.16 4.66 8 6 5 21.11 4.74 -8 6 -6 41.87 3.82 -8 6 -6 41.01 7.14 -8 6 -6 44.20 3.64 -8 6 -6 41.83 3.93 -8 6 -6 40.52 6.82 8 6 6 40.67 6.34 -8 6 -6 44.80 3.87 -8 6 -7 46.41 3.75 -8 6 -7 44.28 3.54 -8 6 -7 35.63 3.87 -8 6 -7 47.58 6.91 -8 6 -7 31.68 6.39 8 6 7 41.69 6.32 -8 6 -7 39.26 3.84 -8 6 -8 8.42 1.74 -8 6 -8 8.42 1.51 8 6 8 11.31 4.11 -8 6 -8 7.59 4.11 -8 6 -8 9.31 1.97 -8 6 -9 10.06 4.02 -8 6 -9 5.84 1.68 -8 6 -9 8.22 1.51 8 6 9 3.28 3.56 -8 6 -9 4.26 1.85 -8 6 -10 1.80 3.54 -8 6 -10 3.61 1.60 -8 6 -10 1.80 1.36 8 6 10 4.07 3.48 -8 6 -11 82.30 6.41 8 6 11 80.93 10.00 -8 6 -11 81.97 6.56 -8 6 -12 5.07 1.89 -8 6 -12 9.12 1.66 -8 6 -13 7.05 1.72 -8 6 -13 6.33 2.03 -8 6 -13 4.75 1.85 -8 6 -14 112.87 8.66 -8 6 -14 113.22 8.53 -8 6 -14 105.06 8.66 -8 6 -15 21.59 2.88 -8 6 -15 24.06 2.62 -8 6 -15 17.06 2.80 -8 6 -16 114.64 8.71 -8 6 -16 116.26 8.84 -8 6 -16 102.88 8.83 -8 6 -17 89.21 7.18 -8 6 -17 85.50 7.01 -8 6 -17 85.65 7.16 -8 6 -18 8.68 2.79 -8 6 -18 10.58 2.55 -8 6 -18 10.84 2.85 -8 6 -19 3.96 2.61 -8 6 -19 -0.41 2.37 -8 6 -19 -1.04 2.73 -8 6 -20 127.19 9.64 -8 6 -20 127.86 9.70 -8 6 -20 120.17 9.67 -8 6 -20 113.13 9.39 -8 6 -21 61.00 5.64 -8 6 -21 64.72 5.86 -8 6 -21 67.34 5.85 -8 6 -21 59.86 5.29 -8 6 -22 41.31 4.18 -8 6 -22 33.06 3.93 -8 6 -22 30.24 3.35 -8 6 -22 37.00 4.06 -8 6 -23 43.26 4.69 -8 6 -23 43.99 4.58 -8 6 -23 44.36 4.60 -8 6 -24 41.08 4.31 -8 6 -24 38.37 4.20 -8 6 -24 36.97 4.32 -8 6 -25 17.69 3.21 -8 6 -25 16.87 2.95 -8 6 -25 13.11 2.86 -8 6 -26 11.68 2.71 -8 6 -26 7.46 2.80 -8 6 -26 3.26 2.52 -8 6 -27 14.99 2.96 -8 6 -27 14.71 2.94 -8 6 -27 18.71 2.79 -8 6 -28 15.97 2.80 -8 6 -28 9.53 2.48 -8 6 -28 14.50 2.76 -8 6 -29 12.93 2.76 -8 6 -29 15.83 2.65 -8 6 -29 9.51 2.38 -8 6 -30 0.08 2.37 -8 6 -30 4.10 1.86 -8 6 -31 -1.52 2.20 -8 6 -31 0.82 1.56 -8 6 -32 8.66 2.16 -8 6 -33 4.11 1.71 8 7 -34 2.45 1.39 8 7 -33 5.53 1.81 8 7 -32 6.40 2.03 8 7 -31 28.79 3.31 8 7 -30 15.87 2.69 8 7 -29 -0.08 2.19 8 7 -28 2.74 2.29 8 7 -27 2.79 2.31 8 7 -26 13.97 2.71 8 7 -25 3.08 2.39 8 7 -24 21.18 3.05 8 7 -23 2.09 2.21 8 7 -22 36.38 3.78 8 7 -21 1.51 2.03 8 7 -20 45.80 4.32 8 7 -19 0.69 1.76 8 7 -18 1.37 1.65 8 7 -17 2.46 1.59 -8 7 17 1.74 1.44 8 7 -16 25.03 2.76 -8 7 16 28.87 2.79 8 7 -15 20.63 2.22 -8 7 15 18.15 2.27 8 7 -14 20.33 2.19 -8 7 14 21.55 2.36 8 7 -13 3.78 1.30 -8 7 13 4.62 1.51 -8 7 12 62.80 5.13 -8 7 11 13.54 1.97 -8 7 10 23.24 2.54 -8 7 9 -0.40 1.45 8 7 -9 0.68 4.47 8 7 -8 124.52 13.75 -8 7 8 125.87 9.48 -8 7 8 110.41 14.12 8 7 -7 133.55 15.61 -8 7 7 158.77 11.80 -8 7 7 174.67 17.37 -8 7 6 128.91 13.50 -8 7 6 116.91 9.13 -8 7 6 123.47 9.19 8 7 -6 103.14 12.67 -8 7 6 121.51 14.23 -8 7 5 232.24 17.04 8 7 -5 229.76 20.86 -8 7 5 249.09 21.68 -8 7 5 247.94 17.27 -8 7 5 222.02 17.15 -8 7 5 226.22 21.98 -8 7 4 35.98 3.14 -8 7 4 36.99 3.40 -8 7 4 36.90 3.37 8 7 -4 43.12 6.72 -8 7 4 43.73 7.63 -8 7 4 26.02 6.59 -8 7 3 60.25 4.70 8 7 -3 55.11 7.75 -8 7 3 59.12 4.91 -8 7 3 57.57 4.90 -8 7 3 60.56 8.90 -8 7 3 71.66 9.33 -8 7 2 19.77 2.05 -8 7 2 14.61 2.50 8 7 -2 22.34 5.05 -8 7 2 23.06 2.32 -8 7 2 17.84 2.27 -8 7 2 17.56 5.72 -8 7 2 16.07 5.74 -8 7 1 21.73 2.10 -8 7 1 19.01 2.54 8 7 -1 17.12 4.77 -8 7 1 30.05 6.39 -8 7 1 18.84 2.32 -8 7 1 20.85 2.31 -8 7 1 20.61 5.75 -8 7 0 21.56 2.20 8 7 0 20.58 4.52 8 7 0 15.80 3.27 -8 7 0 22.82 2.64 -8 7 0 21.51 2.28 -8 7 0 20.34 5.73 -8 7 0 20.60 2.46 -8 7 0 28.65 6.02 -8 7 -1 4.30 1.36 8 7 1 5.69 3.43 8 7 1 3.44 2.84 -8 7 -1 4.20 1.79 -8 7 -1 2.39 4.34 -8 7 -1 2.78 1.37 -8 7 -1 2.37 1.48 -8 7 -1 5.36 4.24 8 7 2 34.37 5.35 -8 7 -2 41.78 3.88 -8 7 -2 37.68 7.15 -8 7 -2 45.24 3.66 -8 7 -2 40.12 3.87 -8 7 -2 30.56 6.65 8 7 2 39.29 5.51 -8 7 -2 46.95 3.72 -8 7 -3 6.87 1.57 -8 7 -3 5.97 1.78 -8 7 -3 5.99 1.50 -8 7 -3 9.39 1.84 -8 7 -3 4.67 3.98 8 7 3 5.76 3.19 -8 7 -4 56.86 4.93 -8 7 -4 64.13 4.84 -8 7 -4 58.18 4.99 -8 7 -4 55.44 8.15 8 7 4 54.21 7.02 -8 7 -4 52.06 8.31 -8 7 -4 60.49 4.88 -8 7 -5 17.21 2.18 -8 7 -5 7.94 5.20 -8 7 -5 19.13 2.02 -8 7 -5 15.37 2.42 -8 7 -5 19.37 5.07 8 7 5 17.62 4.27 -8 7 -5 16.67 2.24 -8 7 -6 2.78 1.76 -8 7 -6 9.27 4.73 -8 7 -6 5.27 1.72 -8 7 -6 2.65 1.33 -8 7 -6 3.22 1.85 -8 7 -6 1.78 3.79 8 7 6 2.25 3.20 -8 7 -7 6.89 4.19 -8 7 -7 2.08 1.70 -8 7 -7 0.97 1.33 -8 7 -7 2.17 1.88 8 7 7 1.44 3.02 -8 7 -7 -0.46 1.62 -8 7 -8 31.19 6.29 -8 7 -8 28.32 3.02 -8 7 -8 29.58 2.76 -8 7 -8 26.44 3.22 8 7 8 31.68 5.51 -8 7 -8 28.95 3.08 -8 7 -9 76.36 10.70 -8 7 -9 91.23 7.74 -8 7 -9 100.00 7.54 8 7 9 87.33 10.42 -8 7 -9 105.95 7.68 -8 7 -9 97.18 7.76 -8 7 -10 1.32 3.65 -8 7 -10 0.23 1.36 -8 7 -10 2.75 1.69 -8 7 -11 5.93 1.98 -8 7 -11 5.03 1.61 -8 7 -12 51.24 4.46 -8 7 -12 49.02 4.28 -8 7 -13 1.90 1.64 -8 7 -13 0.60 1.91 -8 7 -14 15.84 2.57 -8 7 -14 15.51 2.26 -8 7 -14 11.65 2.49 -8 7 -15 71.77 5.59 -8 7 -15 58.93 5.34 -8 7 -15 61.55 5.54 -8 7 -16 31.19 3.59 -8 7 -16 32.18 3.36 -8 7 -16 29.49 3.61 -8 7 -17 17.90 2.80 -8 7 -17 19.01 3.08 -8 7 -17 21.69 3.13 -8 7 -18 177.95 13.19 -8 7 -18 167.00 13.05 -8 7 -18 170.82 13.14 -8 7 -19 97.82 8.10 -8 7 -19 100.40 7.96 -8 7 -19 95.85 8.03 -8 7 -20 39.92 4.26 -8 7 -20 35.60 3.94 -8 7 -20 29.65 4.04 -8 7 -20 33.19 3.44 -8 7 -21 69.59 5.97 -8 7 -21 65.74 5.79 -8 7 -21 63.98 5.80 -8 7 -21 58.92 5.31 -8 7 -22 39.21 4.26 -8 7 -22 33.64 3.60 -8 7 -22 42.37 4.26 -8 7 -22 44.63 4.53 -8 7 -23 85.76 7.46 -8 7 -23 86.66 7.34 -8 7 -23 86.32 7.31 -8 7 -24 17.82 3.30 -8 7 -24 21.89 3.26 -8 7 -24 15.60 3.03 -8 7 -25 18.81 3.44 -8 7 -25 20.18 3.26 -8 7 -25 22.90 3.17 -8 7 -26 13.50 3.14 -8 7 -26 18.45 2.97 -8 7 -26 13.35 2.65 -8 7 -27 4.08 2.52 -8 7 -27 1.99 2.66 -8 7 -27 6.12 2.23 -8 7 -28 0.09 2.62 -8 7 -28 -0.08 2.04 -8 7 -28 0.09 2.38 -8 7 -29 2.88 2.48 -8 7 -29 3.74 2.37 -8 7 -29 2.64 1.91 -8 7 -30 10.82 2.42 -8 7 -30 6.56 1.87 -8 7 -31 10.73 1.78 -8 7 -31 11.36 2.51 -8 7 -32 4.81 2.01 -8 7 -33 4.09 1.76 -8 8 35 4.50 1.05 8 8 -34 1.09 1.25 8 8 -33 5.71 1.65 8 8 -32 6.47 1.96 8 8 -31 0.73 1.98 8 8 -30 4.28 2.19 8 8 -29 13.25 2.60 8 8 -28 7.16 2.38 8 8 -27 2.18 2.21 8 8 -26 3.77 2.33 8 8 -25 6.42 2.45 8 8 -24 42.97 4.28 8 8 -23 4.17 2.34 8 8 -22 52.88 4.89 8 8 -21 0.45 1.93 8 8 -20 10.11 2.25 8 8 -19 6.11 1.95 8 8 -18 27.68 2.96 8 8 -17 3.57 1.68 8 8 -16 2.42 1.57 8 8 -15 12.76 1.89 8 8 -14 36.71 3.21 -8 8 14 35.94 3.30 8 8 -13 16.75 1.99 -8 8 13 17.73 2.12 -8 8 12 31.77 3.01 -8 8 11 2.35 1.49 -8 8 10 228.78 16.87 -8 8 9 115.41 8.81 -8 8 8 25.54 2.64 8 8 -8 27.25 6.20 -8 8 7 66.96 5.21 8 8 -7 41.36 8.20 -8 8 6 58.66 4.85 -8 8 6 57.57 5.01 8 8 -6 58.12 8.33 -8 8 6 77.77 10.23 -8 8 5 39.63 3.57 -8 8 5 37.68 3.39 8 8 -5 29.11 6.32 -8 8 5 38.74 8.00 -8 8 5 34.53 7.11 -8 8 4 81.35 6.46 -8 8 4 86.97 6.77 -8 8 4 89.93 6.70 8 8 -4 69.75 9.58 -8 8 4 86.78 10.84 -8 8 4 96.29 11.52 -8 8 3 125.72 9.44 8 8 -3 129.70 12.95 -8 8 3 122.03 13.74 -8 8 3 123.86 9.65 -8 8 3 128.32 9.59 -8 8 3 145.77 14.68 -8 8 2 63.58 5.59 8 8 -2 65.80 8.24 -8 8 2 66.06 5.48 -8 8 2 69.05 5.43 -8 8 2 74.70 9.82 -8 8 2 73.44 9.85 -8 8 2 66.53 5.25 -8 8 1 29.15 3.33 8 8 -1 34.82 5.60 -8 8 1 32.32 3.04 -8 8 1 36.52 6.91 -8 8 1 31.07 3.03 -8 8 1 41.09 7.32 -8 8 1 30.41 2.81 -8 8 0 42.09 4.02 8 8 0 48.76 6.41 -8 8 0 60.70 8.24 -8 8 0 41.58 3.80 -8 8 0 42.14 3.86 -8 8 0 39.47 7.54 -8 8 0 44.90 3.65 -8 8 -1 5.18 1.41 -8 8 -1 0.57 1.86 -8 8 -1 7.03 4.86 -8 8 -1 3.15 1.49 -8 8 -1 5.26 1.73 -8 8 -1 2.58 4.22 -8 8 -2 27.23 3.08 -8 8 -2 29.52 6.51 -8 8 -2 33.11 2.94 -8 8 -2 27.81 2.98 -8 8 -2 31.12 6.39 -8 8 -2 33.34 2.90 -8 8 -3 31.21 3.25 -8 8 -3 30.37 6.63 -8 8 -3 34.46 3.07 -8 8 -3 34.16 3.25 -8 8 -3 32.05 6.34 -8 8 -3 30.52 3.02 -8 8 -4 30.96 3.16 -8 8 -4 29.65 2.90 -8 8 -4 33.36 3.26 -8 8 -4 27.58 6.35 -8 8 -4 24.80 6.36 -8 8 -4 32.16 3.06 -8 8 -5 13.75 2.30 -8 8 -5 17.22 1.99 -8 8 -5 12.48 2.17 -8 8 -5 12.54 4.90 -8 8 -5 15.86 2.15 -8 8 -6 81.28 6.73 -8 8 -6 86.44 6.56 -8 8 -6 79.41 6.74 -8 8 -6 78.28 10.53 -8 8 -6 87.19 6.70 -8 8 -7 94.84 7.38 -8 8 -7 98.26 7.21 -8 8 -7 83.87 7.42 -8 8 -7 95.82 7.37 -8 8 -8 22.12 5.90 -8 8 -8 33.19 3.19 -8 8 -8 30.13 2.92 -8 8 -8 27.17 3.18 -8 8 -9 21.05 2.71 -8 8 -9 23.45 2.52 -8 8 -9 22.72 2.99 -8 8 -10 -0.37 1.87 -8 8 -10 1.70 1.60 -8 8 -11 58.61 5.13 -8 8 -11 60.54 4.99 -8 8 -12 1.39 1.97 -8 8 -12 2.95 1.70 -8 8 -13 27.74 3.18 -8 8 -13 26.31 2.93 -8 8 -14 36.71 3.63 -8 8 -14 36.76 3.87 -8 8 -15 18.66 2.82 -8 8 -15 19.51 2.69 -8 8 -15 14.44 2.69 -8 8 -16 80.73 6.42 -8 8 -16 75.25 6.49 -8 8 -16 73.29 6.45 -8 8 -17 74.61 6.48 -8 8 -17 80.58 6.34 -8 8 -17 69.26 6.36 -8 8 -18 18.30 3.23 -8 8 -18 15.19 2.88 -8 8 -18 18.28 3.06 -8 8 -19 2.00 2.39 -8 8 -19 0.95 2.73 -8 8 -19 3.77 2.55 -8 8 -20 79.94 6.78 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8.05 2.96 -8 10 -25 7.00 2.38 -8 10 -26 21.69 3.50 -8 10 -26 25.15 3.73 -8 10 -26 20.08 2.87 -8 10 -27 13.06 3.16 -8 10 -27 11.35 2.81 -8 10 -27 7.99 2.18 -8 10 -28 25.32 3.38 -8 10 -28 24.58 3.60 -8 10 -28 21.22 2.72 -8 10 -29 12.65 2.79 -8 10 -29 12.37 2.88 -8 10 -30 12.58 2.57 -8 10 -30 11.07 2.78 -8 10 -31 10.12 2.46 -8 10 -32 4.27 1.86 -8 10 -33 4.62 1.65 -8 11 34 0.17 0.91 8 11 -33 2.44 1.23 -8 11 33 5.80 1.38 8 11 -32 0.85 1.46 8 11 -31 7.29 1.88 8 11 -30 13.30 2.28 8 11 -29 2.12 1.98 8 11 -28 1.88 2.03 8 11 -27 6.48 2.22 8 11 -26 8.24 2.37 8 11 -25 12.89 2.56 8 11 -24 19.92 2.83 8 11 -23 4.92 2.21 8 11 -22 2.90 2.23 8 11 -21 22.32 2.91 8 11 -20 8.09 2.21 8 11 -19 16.31 2.49 8 11 -18 27.05 3.05 8 11 -17 2.95 1.92 8 11 -16 172.22 12.94 8 11 -15 51.79 4.49 8 11 -14 8.44 1.83 8 11 -13 102.20 7.89 8 11 -12 225.68 16.61 -8 11 8 56.21 5.17 -8 11 7 2.83 2.28 -8 11 6 52.48 4.58 -8 11 6 66.98 5.21 -8 11 5 4.99 1.42 -8 11 5 5.27 2.30 -8 11 4 34.09 3.44 -8 11 4 28.66 2.85 -8 11 3 20.92 2.30 -8 11 3 20.84 2.88 -8 11 2 63.42 5.63 -8 11 2 67.05 5.31 -8 11 1 32.59 2.95 -8 11 1 25.96 3.24 -8 11 1 29.35 2.67 -8 11 0 47.73 4.64 -8 11 0 56.50 4.45 -8 11 0 51.40 4.26 -8 11 -1 26.41 2.73 -8 11 -1 21.13 2.83 -8 11 -2 120.05 9.85 -8 11 -2 134.91 9.84 -8 11 -3 108.95 8.72 -8 11 -3 114.07 8.69 -8 11 -4 48.73 4.43 -8 11 -4 49.41 4.44 -8 11 -5 13.51 2.30 -8 11 -5 12.59 2.30 -8 11 -6 5.04 1.97 -8 11 -6 1.70 2.08 -8 11 -7 14.76 2.35 -8 11 -8 64.04 5.47 -8 11 -9 22.14 2.89 -8 11 -10 50.71 4.60 -8 11 -11 35.04 3.63 -8 11 -12 16.72 2.67 -8 11 -13 84.29 6.96 -8 11 -14 40.62 4.48 -8 11 -14 37.27 4.01 -8 11 -15 1.59 2.98 -8 11 -15 5.44 2.41 -8 11 -16 49.64 5.38 -8 11 -16 57.38 5.11 -8 11 -16 51.02 5.09 -8 11 -17 43.80 5.04 -8 11 -17 46.59 4.71 -8 11 -17 47.52 4.65 -8 11 -18 51.34 5.49 -8 11 -18 54.51 5.12 -8 11 -18 53.19 5.09 -8 11 -19 15.07 3.76 -8 11 -19 22.76 3.42 -8 11 -19 21.61 3.18 -8 11 -20 39.44 4.31 -8 11 -20 33.68 3.95 -8 11 -20 33.24 4.57 -8 11 -21 60.89 6.07 -8 11 -21 59.31 5.73 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29.81 2.99 8 12 -12 17.15 2.11 -8 12 9 40.02 4.36 -8 12 8 140.13 10.98 -8 12 7 -2.00 2.54 -8 12 6 9.89 2.60 -8 12 5 33.40 3.97 -8 12 5 36.40 3.81 -8 12 4 22.14 3.26 -8 12 4 22.79 2.32 -8 12 4 21.57 3.11 -8 12 3 0.93 2.40 -8 12 3 4.83 1.41 -8 12 3 3.04 2.27 -8 12 2 67.48 5.69 -8 12 2 66.48 5.27 -8 12 2 60.17 5.78 -8 12 1 16.93 2.16 -8 12 1 13.24 3.01 -8 12 1 18.65 2.87 -8 12 0 84.97 7.58 -8 12 0 88.68 7.43 -8 12 0 95.65 7.15 -8 12 -1 89.39 7.94 -8 12 -1 94.86 7.75 -8 12 -1 99.95 7.52 -8 12 -2 65.93 6.09 -8 12 -2 65.20 5.83 -8 12 -2 72.86 5.67 -8 12 -3 4.35 2.64 -8 12 -3 2.93 1.74 -8 12 -3 6.66 2.32 -8 12 -4 52.21 4.78 -8 12 -4 52.59 4.69 -8 12 -5 89.53 7.37 -8 12 -5 92.93 7.38 -8 12 -6 69.56 5.89 -8 12 -7 6.67 2.17 -8 12 -8 87.73 7.17 -8 12 -9 37.98 3.88 -8 12 -10 23.04 3.04 -8 12 -11 37.85 4.03 -8 12 -12 70.02 6.13 -8 12 -13 4.85 2.62 -8 12 -14 27.40 3.56 -8 12 -15 128.96 10.22 -8 12 -16 57.64 5.75 -8 12 -16 66.29 5.72 -8 12 -17 16.29 3.28 -8 12 -18 36.36 3.89 -8 12 -18 23.41 3.67 -8 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25.72 3.08 8 13 -18 28.70 3.24 8 13 -17 59.34 5.14 8 13 -16 129.26 9.95 8 13 -15 26.16 2.91 8 13 -14 7.75 1.95 8 13 -13 24.84 2.74 8 13 -12 115.38 8.82 -8 13 11 30.57 4.16 -8 13 10 29.85 3.96 -8 13 9 12.84 2.99 -8 13 8 5.15 2.67 -8 13 7 10.33 2.84 -8 13 6 124.30 10.04 -8 13 6 125.58 10.00 -8 13 5 0.80 2.81 -8 13 5 -2.22 2.69 -8 13 4 10.83 2.91 -8 13 4 6.38 2.64 -8 13 3 70.72 6.25 -8 13 3 70.29 6.19 -8 13 2 24.68 3.40 -8 13 2 24.75 2.53 -8 13 2 20.61 3.26 -8 13 1 25.97 3.52 -8 13 1 24.92 2.62 -8 13 1 25.48 3.39 -8 13 0 122.63 10.23 -8 13 0 124.30 10.10 -8 13 0 134.55 9.80 -8 13 -1 15.09 3.10 -8 13 -1 12.96 2.04 -8 13 -1 8.70 2.58 -8 13 -2 81.56 7.18 -8 13 -2 78.03 7.01 -8 13 -2 90.23 6.77 -8 13 -3 156.55 12.45 -8 13 -3 172.35 12.33 -8 13 -3 155.96 12.54 -8 13 -4 5.61 2.63 -8 13 -4 4.87 2.45 -8 13 -5 17.92 3.15 -8 13 -5 17.58 2.94 -8 13 -6 9.44 2.70 -8 13 -6 8.11 2.54 -8 13 -7 21.31 3.32 -8 13 -7 17.29 2.87 -8 13 -8 32.68 4.32 -8 13 -8 43.89 4.12 -8 13 -9 67.36 6.32 -8 13 -9 69.81 6.04 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3.23 -9 9 7 27.14 2.83 -9 9 7 29.57 3.22 -9 9 6 5.53 1.69 -9 9 6 7.44 2.06 -9 9 5 38.36 3.61 -9 9 5 34.41 3.39 -9 9 4 4.01 1.30 -9 9 4 7.35 2.50 -9 9 4 7.60 1.73 -9 9 4 6.90 2.03 -9 9 3 23.37 3.19 -9 9 3 26.30 2.71 -9 9 3 24.31 2.86 -9 9 3 24.97 2.41 -9 9 2 11.46 1.64 -9 9 2 10.07 2.55 -9 9 2 10.20 2.04 -9 9 2 12.87 2.04 -9 9 1 18.78 2.03 -9 9 1 12.66 2.73 -9 9 1 17.82 2.26 -9 9 1 17.45 2.28 -9 9 0 14.70 1.83 -9 9 0 11.40 2.51 -9 9 0 10.03 2.06 -9 9 0 15.33 2.24 -9 9 -1 25.81 3.13 -9 9 -1 27.87 2.84 -9 9 -1 26.12 2.89 -9 9 -1 22.80 2.61 -9 9 -2 3.94 1.61 -9 9 -2 3.97 2.14 -9 9 -2 3.69 1.66 -9 9 -2 4.65 2.01 -9 9 -3 31.37 3.62 -9 9 -3 37.94 3.35 -9 9 -3 32.65 3.48 -9 9 -3 36.94 3.36 -9 9 -4 11.37 2.39 -9 9 -4 13.01 1.99 -9 9 -4 10.01 2.24 -9 9 -4 12.44 2.00 -9 9 -5 41.98 4.18 -9 9 -5 43.38 3.92 -9 9 -5 41.05 4.14 -9 9 -5 48.63 4.07 -9 9 -6 5.65 2.18 -9 9 -6 7.85 1.74 -9 9 -6 1.75 2.17 -9 9 -6 2.33 1.80 -9 9 -7 22.53 2.96 -9 9 -7 21.12 2.52 -9 9 -7 17.88 2.93 -9 9 -8 2.67 2.16 -9 9 -8 4.18 1.77 -9 9 -8 1.95 2.40 -9 9 -9 0.08 2.16 -9 9 -9 1.56 1.68 -9 9 -9 0.64 2.31 -9 9 -10 94.66 7.86 -9 9 -10 99.16 7.70 -9 9 -11 3.80 1.87 -9 9 -11 4.39 2.22 -9 9 -12 4.84 2.38 -9 9 -12 5.98 2.02 -9 9 -13 38.93 4.01 -9 9 -13 45.46 4.38 -9 9 -14 38.03 4.01 -9 9 -14 35.58 3.68 -9 9 -14 31.88 3.94 -9 9 -15 23.53 3.59 -9 9 -15 30.50 3.33 -9 9 -15 27.34 3.66 -9 9 -16 21.58 3.53 -9 9 -16 23.97 3.13 -9 9 -16 19.56 3.41 -9 9 -17 102.66 8.34 -9 9 -17 96.36 8.10 -9 9 -17 100.88 8.26 -9 9 -18 5.85 2.45 -9 9 -18 1.25 2.70 -9 9 -18 3.54 2.99 -9 9 -19 19.85 3.18 -9 9 -19 20.08 3.56 -9 9 -19 15.09 3.30 -9 9 -20 7.64 3.03 -9 9 -20 4.86 2.61 -9 9 -20 2.05 2.70 -9 9 -20 6.42 1.91 -9 9 -21 52.06 5.28 -9 9 -21 57.12 5.10 -9 9 -21 56.12 5.15 -9 9 -21 46.76 4.48 -9 9 -22 13.93 3.42 -9 9 -22 16.57 3.09 -9 9 -22 17.10 3.16 -9 9 -23 9.53 2.64 -9 9 -23 7.05 2.63 -9 9 -23 7.36 3.05 -9 9 -24 5.32 2.99 -9 9 -24 6.62 2.67 -9 9 -24 3.01 2.41 -9 9 -25 9.49 3.07 -9 9 -25 12.21 2.76 -9 9 -25 12.98 2.67 -9 9 -26 1.04 2.68 -9 9 -26 1.85 2.42 -9 9 -26 2.05 2.17 -9 9 -27 10.17 2.67 -9 9 -27 9.54 2.36 -9 9 -27 10.63 2.90 -9 9 -28 7.30 2.63 -9 9 -28 12.11 2.51 -9 9 -28 7.39 2.05 -9 9 -29 -2.05 2.36 -9 9 -29 1.39 2.06 -9 9 -29 0.18 1.62 -9 9 -30 4.77 2.07 -9 9 -30 0.71 1.36 -9 9 -31 1.10 1.80 -9 9 -32 4.81 1.63 -9 9 -33 2.55 1.25 -9 10 33 3.76 1.10 -9 10 32 1.69 1.28 9 10 -31 2.07 1.48 9 10 -30 13.47 2.08 9 10 -29 3.07 1.78 9 10 -28 6.39 2.06 9 10 -27 1.35 2.02 9 10 -26 1.77 1.98 9 10 -25 3.56 2.09 9 10 -24 4.76 2.12 9 10 -23 15.30 2.53 9 10 -22 5.64 2.06 9 10 -21 2.10 1.92 9 10 -20 9.21 2.14 9 10 -19 2.69 1.85 9 10 -18 0.41 1.72 9 10 -17 74.15 6.04 -9 10 10 39.55 3.80 -9 10 10 54.16 4.61 -9 10 9 88.24 7.38 -9 10 9 108.77 7.87 -9 10 8 25.42 2.71 -9 10 8 27.69 3.31 -9 10 7 9.97 1.78 -9 10 7 11.03 2.48 -9 10 6 3.17 1.46 -9 10 6 1.24 1.97 -9 10 5 6.16 1.65 -9 10 5 5.50 2.13 -9 10 4 13.71 2.83 -9 10 4 12.12 1.95 -9 10 4 15.13 2.46 -9 10 3 29.35 3.69 -9 10 3 34.57 3.31 -9 10 3 30.72 3.05 -9 10 3 28.87 2.74 -9 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2.74 -9 10 -14 5.72 2.27 -9 10 -15 76.28 6.65 -9 10 -15 73.55 6.32 -9 10 -15 72.68 6.53 -9 10 -16 17.15 3.30 -9 10 -16 13.96 2.89 -9 10 -16 13.70 3.08 -9 10 -17 19.69 3.63 -9 10 -17 23.12 3.24 -9 10 -17 18.34 3.43 -9 10 -18 4.72 3.01 -9 10 -18 8.57 2.70 -9 10 -18 5.29 2.79 -9 10 -19 91.80 7.27 -9 10 -19 79.40 6.93 -9 10 -19 74.03 6.93 -9 10 -20 9.48 2.91 -9 10 -20 11.68 3.35 -9 10 -20 9.91 2.90 -9 10 -20 9.41 2.06 -9 10 -21 3.08 2.73 -9 10 -21 1.06 3.10 -9 10 -21 1.55 2.69 -9 10 -22 17.45 3.61 -9 10 -22 18.95 3.30 -9 10 -22 20.79 3.29 -9 10 -23 17.94 3.50 -9 10 -23 20.70 3.27 -9 10 -23 17.71 2.97 -9 10 -24 30.22 4.09 -9 10 -24 27.18 3.73 -9 10 -24 31.93 3.59 -9 10 -25 26.35 3.69 -9 10 -25 19.77 3.28 -9 10 -25 20.56 3.13 -9 10 -26 13.78 3.26 -9 10 -26 15.77 2.97 -9 10 -26 17.54 2.71 -9 10 -27 13.54 2.99 -9 10 -27 13.15 2.76 -9 10 -27 12.47 2.35 -9 10 -28 2.10 2.39 -9 10 -28 1.09 2.22 -9 10 -28 2.65 1.81 -9 10 -29 0.08 2.30 -9 10 -29 0.50 2.03 -9 10 -29 1.22 1.46 -9 10 -30 8.22 2.24 -9 10 -31 3.22 1.82 -9 10 -32 5.88 1.63 -9 11 33 3.23 0.99 -9 11 32 8.18 1.49 -9 11 31 3.30 1.58 9 11 -30 2.90 1.58 9 11 -29 4.97 1.74 9 11 -28 -0.58 1.86 9 11 -27 3.76 1.96 9 11 -26 12.57 2.36 9 11 -25 10.78 2.32 9 11 -24 11.56 2.37 9 11 -23 2.88 2.01 9 11 -22 9.58 2.24 9 11 -21 12.31 2.28 9 11 -20 6.44 2.03 9 11 -19 41.58 3.96 9 11 -18 15.21 2.30 9 11 -17 39.36 3.71 -9 11 11 170.90 13.23 -9 11 10 16.22 3.06 -9 11 9 40.90 4.29 -9 11 8 23.53 2.64 -9 11 8 30.61 3.44 -9 11 7 36.79 3.42 -9 11 7 39.13 4.11 -9 11 6 75.64 5.89 -9 11 6 61.46 5.37 -9 11 5 5.07 1.63 -9 11 5 3.52 2.26 -9 11 4 17.24 2.17 -9 11 4 17.30 2.68 -9 11 3 17.61 2.23 -9 11 3 16.69 2.67 -9 11 2 12.96 2.09 -9 11 2 12.75 2.44 -9 11 2 13.43 1.77 -9 11 1 69.17 5.93 -9 11 1 72.51 5.75 -9 11 1 67.25 5.48 -9 11 0 42.13 4.16 -9 11 0 43.88 4.04 -9 11 0 43.99 3.76 -9 11 -1 8.79 2.10 -9 11 -1 6.53 2.20 -9 11 -1 7.83 1.66 -9 11 -2 22.78 2.96 -9 11 -2 23.70 2.91 -9 11 -3 17.16 3.18 -9 11 -3 19.19 2.73 -9 11 -3 21.19 2.69 -9 11 -4 26.23 3.55 -9 11 -4 26.95 3.14 -9 11 -4 27.78 3.15 -9 11 -5 66.94 5.89 -9 11 -5 60.65 5.48 -9 11 -5 67.85 5.66 -9 11 -6 17.38 3.03 -9 11 -6 16.88 2.59 -9 11 -6 18.10 2.87 -9 11 -7 112.11 9.39 -9 11 -7 121.55 9.22 -9 11 -8 12.13 2.94 -9 11 -8 11.96 2.42 -9 11 -9 1.62 2.60 -9 11 -9 -0.49 2.12 -9 11 -10 69.09 6.17 -9 11 -10 67.57 5.86 -9 11 -11 31.53 3.82 -9 11 -11 27.55 3.40 -9 11 -12 9.69 2.98 -9 11 -12 9.14 2.53 -9 11 -13 30.18 4.01 -9 11 -13 32.31 3.63 -9 11 -14 42.74 4.99 -9 11 -14 52.29 4.74 -9 11 -15 19.22 3.47 -9 11 -15 14.66 2.98 -9 11 -15 12.51 3.11 -9 11 -16 1.17 3.04 -9 11 -16 4.48 2.68 -9 11 -16 1.96 2.77 -9 11 -17 86.56 7.42 -9 11 -17 86.20 7.12 -9 11 -17 77.60 7.14 -9 11 -18 16.29 3.59 -9 11 -18 14.52 3.14 -9 11 -18 12.78 2.99 -9 11 -19 -1.31 3.16 -9 11 -19 -0.10 2.78 -9 11 -19 -0.10 2.63 -9 11 -20 30.50 4.31 -9 11 -20 35.04 4.01 -9 11 -20 28.07 3.85 -9 11 -21 34.43 3.94 -9 11 -21 29.96 4.28 -9 11 -21 25.88 3.68 -9 11 -22 43.07 4.46 -9 11 -22 38.22 4.29 -9 11 -22 44.33 4.90 -9 11 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0.90 1.99 -10 4 -26 2.15 2.53 -10 4 -26 2.58 1.92 -10 4 -27 11.61 2.41 -10 4 -27 13.72 2.77 -10 4 -28 0.58 1.92 -10 4 -28 -0.79 2.16 -10 4 -29 1.13 1.75 -10 4 -29 0.51 2.04 -10 4 -30 9.43 1.87 -10 4 -30 9.22 2.09 -10 4 -31 1.11 1.30 -10 4 -31 1.56 1.54 -10 4 -32 -0.45 1.18 -10 5 32 2.58 1.07 10 5 -30 12.09 1.95 10 5 -29 1.56 1.76 10 5 -28 9.57 2.16 10 5 -27 7.92 2.13 10 5 -26 2.93 2.04 10 5 -25 26.93 3.15 10 5 -24 -0.78 2.00 -10 5 24 2.11 1.61 10 5 -23 23.03 2.89 -10 5 23 19.23 2.58 10 5 -22 5.91 2.13 -10 5 22 6.42 1.92 10 5 -21 19.39 2.72 -10 5 21 19.33 2.65 -10 5 20 18.98 2.66 -10 5 19 48.48 4.51 -10 5 18 15.12 2.53 -10 5 17 26.99 3.19 -10 5 16 13.43 2.40 -10 5 15 44.55 4.19 -10 5 14 23.44 2.98 -10 5 13 30.92 3.42 -10 5 12 111.52 8.83 -10 5 11 28.78 3.29 -10 5 10 11.67 1.79 -10 5 10 10.78 2.25 -10 5 9 100.01 8.11 -10 5 9 117.79 8.29 -10 5 9 102.28 8.33 -10 5 8 110.27 8.60 -10 5 8 120.80 8.68 -10 5 8 105.30 8.82 -10 5 7 61.19 5.05 -10 5 7 62.85 5.09 -10 5 7 62.21 5.34 -10 5 6 124.40 9.37 -10 5 6 117.19 9.32 -10 5 6 129.47 9.58 -10 5 5 23.29 2.62 10 5 -5 22.29 6.02 -10 5 5 28.20 2.62 -10 5 5 26.33 3.09 -10 5 4 38.38 3.90 10 5 -4 43.67 7.79 -10 5 4 49.00 4.31 -10 5 4 47.06 3.81 -10 5 4 46.49 4.24 -10 5 3 11.17 1.91 -10 5 3 7.56 2.16 -10 5 3 10.54 1.60 -10 5 3 11.89 2.30 -10 5 2 1.53 1.67 -10 5 2 0.46 1.74 -10 5 2 2.28 1.20 -10 5 2 1.88 1.90 -10 5 1 109.35 8.59 -10 5 1 105.61 8.69 -10 5 1 114.63 8.43 -10 5 1 114.22 8.77 -10 5 0 25.39 2.82 -10 5 0 24.21 2.82 -10 5 0 25.52 2.40 -10 5 0 24.85 3.08 -10 5 -1 16.61 2.31 -10 5 -1 15.51 2.26 -10 5 -1 12.87 1.69 -10 5 -1 10.64 2.47 -10 5 -2 4.64 1.91 -10 5 -2 3.94 1.81 -10 5 -2 3.60 1.26 -10 5 -2 4.02 2.17 -10 5 -2 0.65 3.74 -10 5 -3 89.71 7.15 -10 5 -3 88.46 7.04 -10 5 -3 90.47 6.81 -10 5 -3 85.96 7.21 -10 5 -3 80.29 10.56 -10 5 -4 21.72 2.92 -10 5 -4 23.94 2.66 -10 5 -4 25.96 2.35 -10 5 -4 22.53 3.02 -10 5 -4 23.18 5.37 -10 5 -5 21.40 2.82 -10 5 -5 22.00 2.61 -10 5 -5 21.58 2.22 -10 5 -5 21.08 5.43 -10 5 -6 25.88 3.30 -10 5 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15.38 2.87 -11 5 -26 17.16 2.51 -11 5 -27 7.72 2.38 -11 5 -27 7.90 2.04 -11 5 -28 3.40 1.64 -11 5 -28 2.42 2.09 -11 5 -29 6.65 1.57 -11 5 -29 8.38 2.01 -11 5 -30 1.43 1.19 -11 5 -30 -0.27 1.49 -11 5 -31 0.71 1.16 -11 6 29 10.11 1.66 -11 6 28 -1.31 1.47 -11 6 22 4.19 1.68 -11 6 21 6.55 1.82 -11 6 20 12.62 2.26 -11 6 19 12.70 2.30 -11 6 18 21.92 2.85 -11 6 17 16.00 2.61 -11 6 16 92.62 7.52 -11 6 15 59.24 5.30 -11 6 14 66.44 5.82 -11 6 14 69.74 5.91 -11 6 13 38.00 3.88 -11 6 13 41.35 4.04 -11 6 12 22.51 3.00 -11 6 12 19.42 2.73 -11 6 11 22.64 3.32 -11 6 11 28.87 3.05 -11 6 10 70.52 6.03 -11 6 10 81.39 6.25 -11 6 10 78.67 6.48 -11 6 9 78.04 6.45 -11 6 9 88.69 6.63 -11 6 9 78.65 6.83 -11 6 8 128.39 10.20 -11 6 8 141.72 10.29 -11 6 8 134.08 10.50 -11 6 7 21.14 2.46 -11 6 7 20.44 2.48 -11 6 7 18.55 2.96 -11 6 6 44.99 4.13 -11 6 6 45.83 4.68 -11 6 6 47.34 4.11 -11 6 6 49.10 4.55 -11 6 5 10.86 2.15 -11 6 5 15.92 2.84 -11 6 5 11.31 1.95 -11 6 5 11.88 2.60 -11 6 4 144.06 11.12 -11 6 4 156.27 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4.37 -11 7 5 39.91 3.69 -11 7 5 38.67 4.08 -11 7 4 79.56 6.81 -11 7 4 84.47 7.28 -11 7 4 90.43 6.85 -11 7 4 89.79 7.10 -11 7 3 4.05 1.75 -11 7 3 1.77 2.54 -11 7 3 7.28 1.73 -11 7 3 5.95 2.33 -11 7 2 70.82 5.83 -11 7 2 64.69 6.10 -11 7 2 73.43 5.73 -11 7 2 69.71 6.14 -11 7 1 3.54 1.92 -11 7 1 5.07 2.39 -11 7 1 5.32 1.61 -11 7 1 3.22 2.42 -11 7 0 84.23 7.20 -11 7 0 88.64 6.84 -11 7 0 83.15 7.22 -11 7 0 88.71 6.98 -11 7 -1 1.68 1.93 -11 7 -1 1.78 2.29 -11 7 -1 3.21 1.62 -11 7 -1 2.07 2.29 -11 7 -2 116.73 9.62 -11 7 -2 122.41 9.34 -11 7 -2 120.87 9.75 -11 7 -2 127.88 9.57 -11 7 -3 6.81 2.29 -11 7 -3 4.11 2.35 -11 7 -3 6.43 1.71 -11 7 -3 11.28 2.64 -11 7 -4 59.35 6.01 -11 7 -4 79.18 5.76 -11 7 -4 65.89 6.31 -11 7 -4 73.54 6.06 -11 7 -5 11.75 2.77 -11 7 -5 19.07 2.76 -11 7 -5 16.62 2.18 -11 7 -5 14.87 2.98 -11 7 -6 15.61 2.82 -11 7 -6 11.70 2.51 -11 7 -6 11.56 1.98 -11 7 -6 14.99 3.04 -11 7 -7 1.40 2.12 -11 7 -7 2.24 1.56 -11 7 -7 0.91 2.71 -11 7 -7 2.03 2.37 -11 7 -8 35.01 3.96 -11 7 -8 39.33 3.56 -11 7 -8 40.70 4.64 -11 7 -8 40.51 4.21 -11 7 -9 2.41 2.23 -11 7 -9 1.03 1.61 -11 7 -9 3.53 2.78 -11 7 -10 21.87 3.21 -11 7 -10 25.14 2.79 -11 7 -11 60.15 5.56 -11 7 -11 63.17 5.27 -11 7 -12 96.47 7.90 -11 7 -12 96.66 7.61 -11 7 -12 92.72 8.09 -11 7 -13 120.80 9.08 -11 7 -13 104.95 8.75 -11 7 -14 13.77 2.80 -11 7 -14 4.31 2.07 -11 7 -15 94.98 7.64 -11 7 -15 88.57 7.37 -11 7 -16 29.78 3.46 -11 7 -16 20.06 2.90 -11 7 -17 72.24 6.07 -11 7 -17 63.80 5.68 -11 7 -17 63.25 6.39 -11 7 -18 3.72 2.16 -11 7 -18 6.72 2.70 -11 7 -18 6.08 3.26 -11 7 -19 2.13 2.65 -11 7 -19 2.91 2.15 -11 7 -19 5.25 3.35 -11 7 -19 4.31 2.34 -11 7 -20 6.39 2.13 -11 7 -20 5.42 3.12 -11 7 -20 3.26 2.59 -11 7 -20 5.71 2.34 -11 7 -21 8.98 2.24 -11 7 -21 9.06 3.09 -11 7 -21 10.58 2.76 -11 7 -21 10.03 2.24 -11 7 -22 6.47 2.51 -11 7 -22 3.80 2.02 -11 7 -22 1.57 2.74 -11 7 -22 3.08 1.87 -11 7 -23 22.56 3.00 -11 7 -23 17.00 2.62 -11 7 -23 20.73 3.36 -11 7 -23 17.67 2.41 -11 7 -24 1.12 2.17 -11 7 -24 1.74 1.84 -11 7 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5 20.28 3.16 -11 8 5 13.55 2.25 -11 8 5 16.53 2.59 -11 8 4 76.63 6.77 -11 8 4 81.58 6.39 -11 8 4 75.87 6.57 -11 8 4 78.62 6.29 -11 8 3 6.12 1.79 -11 8 3 8.28 2.71 -11 8 3 6.51 1.91 -11 8 3 7.65 2.40 -11 8 2 59.73 5.70 -11 8 2 63.08 5.29 -11 8 2 62.45 5.57 -11 8 2 65.08 5.28 -11 8 1 0.78 1.62 -11 8 1 2.29 2.44 -11 8 1 2.50 1.67 -11 8 1 2.36 2.19 -11 8 0 47.45 4.79 -11 8 0 48.49 4.31 -11 8 0 50.05 4.73 -11 8 0 51.96 4.47 -11 8 -1 12.27 2.29 -11 8 -1 16.45 2.86 -11 8 -1 14.36 2.15 -11 8 -1 14.67 2.88 -11 8 -2 35.80 4.24 -11 8 -2 43.69 3.78 -11 8 -2 41.53 4.30 -11 8 -2 41.06 3.97 -11 8 -3 8.97 2.33 -11 8 -3 11.07 2.62 -11 8 -3 8.41 1.93 -11 8 -3 9.90 2.75 -11 8 -4 135.84 11.06 -11 8 -4 141.76 10.80 -11 8 -4 137.96 11.14 -11 8 -4 151.94 11.04 -11 8 -5 4.51 2.33 -11 8 -5 6.66 1.78 -11 8 -5 8.57 2.82 -11 8 -5 7.43 2.41 -11 8 -6 16.99 3.01 -11 8 -6 22.99 2.55 -11 8 -6 18.33 3.27 -11 8 -6 22.95 3.11 -11 8 -7 8.44 2.56 -11 8 -7 6.96 1.84 -11 8 -7 10.82 2.88 -11 8 -7 7.48 2.64 -11 8 -8 10.93 2.70 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1.56 2.04 -11 10 6 19.12 2.62 -11 10 6 20.83 2.84 -11 10 5 12.19 3.27 -11 10 5 12.83 2.45 -11 10 5 15.74 2.51 -11 10 4 2.34 1.43 -11 10 4 4.06 2.99 -11 10 4 2.56 2.06 -11 10 4 1.66 2.02 -11 10 3 1.66 1.49 -11 10 3 0.53 2.88 -11 10 3 -0.16 2.02 -11 10 3 -0.34 2.09 -11 10 2 73.29 6.17 -11 10 2 63.86 5.62 -11 10 2 67.47 5.74 -11 10 2 63.36 5.39 -11 10 1 3.97 2.80 -11 10 1 3.77 2.05 -11 10 1 4.45 2.26 -11 10 1 1.93 1.65 -11 10 0 6.21 2.79 -11 10 0 5.88 2.06 -11 10 0 5.88 2.38 -11 10 -1 54.68 4.69 -11 10 -1 48.94 4.91 -11 10 -1 50.36 5.19 -11 10 -1 51.19 4.57 -11 10 -2 15.02 3.41 -11 10 -2 22.69 2.81 -11 10 -2 22.20 3.23 -11 10 -2 21.97 2.74 -11 10 -3 74.34 7.14 -11 10 -3 86.36 6.81 -11 10 -3 88.04 7.16 -11 10 -3 81.97 6.80 -11 10 -4 94.22 8.15 -11 10 -4 95.07 7.75 -11 10 -4 94.70 8.09 -11 10 -4 101.76 7.84 -11 10 -5 15.89 3.37 -11 10 -5 16.06 2.61 -11 10 -5 16.44 3.40 -11 10 -6 28.59 3.99 -11 10 -6 33.49 3.42 -11 10 -6 29.17 3.97 -11 10 -7 18.96 3.44 -11 10 -7 24.86 2.90 -11 10 -7 20.95 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6.92 2.65 -11 10 -24 7.51 2.25 -11 10 -24 11.15 2.59 -11 10 -25 9.55 2.65 -11 10 -25 12.78 2.32 -11 10 -25 12.26 2.58 -11 10 -26 5.57 2.30 -11 10 -26 5.83 1.95 -11 10 -26 7.96 2.17 -11 10 -27 0.72 1.58 -11 10 -27 -1.50 1.79 -11 10 -27 0.84 1.96 -11 10 -28 2.99 1.77 -11 10 -28 2.65 1.51 -11 10 -29 2.28 1.50 -11 10 -29 0.21 1.13 -11 10 -30 2.19 1.22 -11 11 30 1.22 0.88 -11 11 29 0.94 1.17 -11 11 28 8.50 1.70 -11 11 27 -1.30 1.64 -11 11 26 1.47 1.87 -11 11 25 39.29 3.94 -11 11 24 12.91 2.58 -11 11 23 14.67 2.81 -11 11 22 3.59 2.40 -11 11 21 53.05 5.11 -11 11 20 1.01 2.45 -11 11 19 10.29 2.72 -11 11 18 6.92 2.78 -11 11 17 30.02 3.86 -11 11 16 48.87 4.92 -11 11 15 20.85 3.33 -11 11 14 139.06 11.00 -11 11 13 33.24 4.05 -11 11 12 38.88 4.32 -11 11 11 31.78 3.35 -11 11 11 39.74 4.10 -11 11 10 101.08 8.02 -11 11 10 97.63 7.44 -11 11 10 76.78 6.95 -11 11 9 -3.12 3.53 -11 11 9 -3.53 1.90 -11 11 9 -3.36 2.61 -11 11 8 4.01 3.26 -11 11 8 5.33 1.82 -11 11 8 7.75 2.48 -11 11 7 1.25 3.08 -11 11 7 0.23 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46.70 4.33 -11 12 4 36.10 3.93 -11 12 3 10.35 3.55 -11 12 3 8.44 2.23 -11 12 3 10.46 2.66 -11 12 2 63.25 6.35 -11 12 2 68.83 5.90 -11 12 2 64.39 5.62 -11 12 1 5.40 3.43 -11 12 1 11.66 2.71 -11 12 1 13.91 2.58 -11 12 0 60.74 6.26 -11 12 0 65.22 5.73 -11 12 0 67.22 5.74 -11 12 -1 18.32 3.68 -11 12 -1 20.23 2.91 -11 12 -1 14.73 2.84 -11 12 -2 38.48 4.90 -11 12 -2 40.00 4.23 -11 12 -2 45.18 4.32 -11 12 -3 103.60 9.43 -11 12 -3 110.15 9.07 -11 12 -3 125.51 9.24 -11 12 -4 29.78 4.35 -11 12 -4 27.19 3.66 -11 12 -4 31.60 3.82 -11 12 -5 26.68 4.24 -11 12 -5 27.03 3.56 -11 12 -5 36.85 4.08 -11 12 -6 38.20 4.76 -11 12 -6 37.24 4.10 -11 12 -7 59.89 6.45 -11 12 -7 74.35 6.10 -11 12 -8 6.07 3.43 -11 12 -8 10.73 2.67 -11 12 -9 53.83 5.72 -11 12 -9 58.48 5.29 -11 12 -10 33.09 4.74 -11 12 -10 41.97 4.17 -11 12 -11 0.91 3.42 -11 12 -11 -0.09 2.45 -11 12 -12 37.32 4.90 -11 12 -12 41.79 4.26 -11 12 -13 35.84 4.69 -11 12 -13 37.05 4.12 -11 12 -14 28.79 4.26 -11 12 -14 32.38 3.75 -11 12 -14 26.86 4.12 -11 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1.99 -11 13 27 8.65 2.22 -11 13 27 8.23 1.75 -11 13 26 9.30 1.95 -11 13 25 12.52 2.31 -11 13 24 9.14 2.29 -11 13 23 10.03 2.45 -11 13 22 -1.14 2.36 -11 13 21 16.19 2.89 -11 13 20 11.25 2.82 -11 13 19 22.56 3.41 -11 13 18 11.31 2.97 -11 13 17 10.96 3.02 -11 13 16 58.95 5.63 -11 13 15 -1.31 2.91 -11 13 14 93.25 7.96 -11 13 13 10.24 3.08 -11 13 12 29.60 3.98 -11 13 11 -3.44 3.01 -11 13 10 186.14 14.35 -11 13 9 4.91 3.05 -11 13 8 11.73 2.99 -11 13 7 0.49 1.63 -11 13 7 2.96 2.67 -11 13 6 93.31 7.30 -11 13 6 79.89 6.78 -11 13 5 1.49 1.93 -11 13 5 -0.29 2.78 -11 13 4 74.06 6.26 -11 13 4 65.01 5.70 -11 13 3 18.96 2.67 -11 13 3 18.15 3.34 -11 13 2 51.86 5.05 -11 13 2 51.06 4.65 -11 13 1 16.32 3.02 -11 13 1 16.40 2.60 -11 13 0 5.19 3.69 -11 13 0 8.42 2.68 -11 13 0 14.56 2.55 -11 13 -1 13.84 3.92 -11 13 -1 10.37 2.81 -11 13 -1 17.62 2.73 -11 13 -2 32.29 4.73 -11 13 -2 37.03 3.98 -11 13 -2 36.80 3.98 -11 13 -3 9.78 3.60 -11 13 -3 11.98 2.88 -11 13 -3 12.77 2.80 -11 13 -4 44.50 5.43 -11 13 -4 51.32 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1.76 -14 5 19 3.68 1.92 -14 5 18 1.35 2.30 -14 5 18 1.54 1.97 -14 5 17 32.61 3.69 -14 5 17 29.42 3.43 -14 5 16 48.00 4.66 -14 5 16 45.15 4.51 -14 5 15 13.64 2.95 -14 5 15 12.48 2.71 -14 5 14 17.79 3.33 -14 5 14 22.29 3.09 -14 5 13 -1.84 2.62 -14 5 13 2.60 2.63 -14 5 12 77.50 6.74 -14 5 12 89.71 7.35 -14 5 12 95.30 7.37 -14 5 11 8.85 2.00 -14 5 11 9.18 2.78 -14 5 11 11.80 2.87 -14 5 10 35.95 3.54 -14 5 10 32.36 4.07 -14 5 10 36.29 4.25 -14 5 9 80.31 6.97 -14 5 9 83.15 7.31 -14 5 9 100.72 7.54 -14 5 8 54.84 4.94 -14 5 8 48.26 5.16 -14 5 8 62.34 5.51 -14 5 7 3.03 2.27 -14 5 7 1.42 2.66 -14 5 7 3.27 3.07 -14 5 6 135.34 10.51 -14 5 6 122.54 10.60 -14 5 6 150.47 10.94 -14 5 5 129.67 10.51 -14 5 5 131.13 10.58 -14 5 5 143.87 10.88 -14 5 4 71.04 6.09 -14 5 4 64.10 6.13 -14 5 4 69.62 6.53 -14 5 3 90.50 7.14 -14 5 3 73.35 7.04 -14 5 3 90.03 7.60 -14 5 2 71.33 6.28 -14 5 2 75.28 6.81 -14 5 2 69.08 6.35 -14 5 1 148.58 12.16 -14 5 1 160.27 12.62 -14 5 1 167.57 12.33 -14 5 0 13.03 3.07 -14 5 0 9.21 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1.65 1.71 -14 5 -18 2.13 2.80 -14 5 -18 1.13 2.36 -14 5 -19 12.12 2.06 -14 5 -19 11.87 3.05 -14 5 -19 17.33 2.75 -14 5 -20 11.04 1.95 -14 5 -20 12.05 3.11 -14 5 -20 15.68 2.62 -14 5 -21 -0.94 2.06 -14 5 -22 10.19 2.10 -14 5 -23 21.29 2.48 -14 5 -24 12.44 2.59 -14 5 -24 12.53 1.84 -14 5 -25 3.53 1.24 -14 5 -25 6.56 2.08 -14 5 -26 2.93 1.76 -14 5 -27 34.49 3.11 -14 6 28 11.25 1.41 -14 6 27 0.89 1.18 -14 6 26 7.56 1.66 -14 6 25 5.49 1.83 -14 6 24 3.57 1.91 -14 6 23 8.78 2.18 -14 6 22 11.72 2.43 -14 6 21 5.68 2.31 -14 6 21 3.41 1.45 -14 6 20 2.36 2.37 -14 6 20 2.15 1.55 -14 6 19 11.27 2.63 -14 6 19 8.20 1.97 -14 6 18 14.13 2.81 -14 6 18 9.33 2.22 -14 6 17 6.94 2.66 -14 6 17 6.61 2.12 -14 6 16 7.85 2.79 -14 6 16 2.91 2.22 -14 6 15 31.79 4.07 -14 6 15 39.62 3.93 -14 6 14 61.65 5.95 -14 6 14 67.35 5.79 -14 6 13 6.04 2.80 -14 6 13 8.28 2.57 -14 6 12 1.69 2.70 -14 6 12 3.42 2.53 -14 6 11 48.98 4.98 -14 6 11 50.91 4.95 -14 6 10 41.66 4.00 -14 6 10 44.65 4.70 -14 6 10 48.59 4.66 -14 6 9 10.72 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13.58 3.07 -14 8 5 12.48 2.32 -14 8 5 10.06 3.20 -14 8 5 13.42 3.12 -14 8 4 59.46 5.45 -14 8 4 56.00 5.42 -14 8 4 51.22 4.89 -14 8 3 113.17 9.20 -14 8 3 111.91 9.28 -14 8 3 110.25 8.85 -14 8 2 13.06 2.64 -14 8 2 10.85 3.17 -14 8 2 9.70 3.29 -14 8 1 21.33 3.01 -14 8 1 18.39 3.43 -14 8 1 19.16 3.83 -14 8 0 39.90 4.53 -14 8 0 37.72 4.85 -14 8 0 43.98 4.35 -14 8 -1 57.86 5.38 -14 8 -1 51.11 5.57 -14 8 -1 52.83 5.17 -14 8 -2 72.48 6.54 -14 8 -2 70.08 6.90 -14 8 -2 76.12 6.50 -14 8 -3 49.76 4.90 -14 8 -3 48.22 5.37 -14 8 -3 44.59 4.87 -14 8 -4 31.23 3.82 -14 8 -4 26.30 4.39 -14 8 -4 26.34 3.87 -14 8 -5 11.61 2.98 -14 8 -5 8.13 3.84 -14 8 -5 17.05 3.21 -14 8 -6 31.11 3.82 -14 8 -6 32.81 4.71 -14 8 -6 27.91 3.74 -14 8 -7 35.38 4.04 -14 8 -7 32.72 4.88 -14 8 -7 35.55 4.07 -14 8 -8 29.41 3.83 -14 8 -8 24.47 4.60 -14 8 -8 38.97 4.14 -14 8 -9 23.60 3.58 -14 8 -9 32.11 3.92 -14 8 -10 4.90 2.64 -14 8 -10 3.39 3.20 -14 8 -11 49.83 4.91 -14 8 -11 51.14 5.23 -14 8 -12 4.30 2.45 -14 8 -12 12.25 3.21 -14 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14.85 1.69 -20 3 7 6.21 1.34 -20 3 6 23.51 2.34 -20 3 5 24.13 2.41 -20 3 4 3.36 1.46 -20 3 3 3.71 1.53 -20 4 9 12.87 1.48 -20 4 8 3.34 1.07 -20 4 7 28.02 2.57 -20 4 6 5.53 1.40 -20 4 5 6.53 1.52 -20 4 4 22.58 2.29 -20 4 3 9.43 1.59 -20 5 7 4.65 1.09 -20 5 6 2.93 1.18 -20 5 5 14.37 1.77 0 0 0 0.00 0.00 TITL S in P2(1) REM P2(1) (#4 in standard setting) CELL 1.54184 16.633641 26.894979 31.762862 90.0000 91.3461 90.0000 ZERR 61.00 0.000170 0.000350 0.000424 0.0000 0.0010 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 671.00 610.00 61.00 61.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 94228 _shelx_fab_file ; -20 -8 -2 0.0000 -0.0000 -20 -8 -1 0.0000 -0.0000 -20 -8 0 0.0000 -0.0000 -20 -7 -2 0.0000 -0.0000 -20 -7 -1 0.0000 -0.0000 -20 -7 0 0.0000 -0.0000 -20 -6 -2 0.0000 -0.0000 -20 -6 -1 0.0000 -0.0000 -20 -5 -2 0.0000 -0.0000 -20 -4 0 0.0000 -0.0000 -20 -3 -1 0.0000 -0.0000 -20 -3 0 0.0000 -0.0000 -20 -2 -1 0.0000 -0.0000 -20 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were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.553 _oxdiff_exptl_absorpt_empirical_full_min 0.766