data_007b-18129 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C18 H27 N O4' _chemical_formula_sum 'C18 H27 N O4' _chemical_formula_weight 321.40 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_H-M_alt 'P 21' _space_group_name_Hall 'P 2yb' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 9.04910(10) _cell_length_b 8.26590(10) _cell_length_c 11.43230(10) _cell_angle_alpha 90 _cell_angle_beta 103.3330(10) _cell_angle_gamma 90 _cell_volume 832.075(16) _cell_formula_units_Z 2 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 26269 _cell_measurement_theta_min 3.9500 _cell_measurement_theta_max 66.5530 _exptl_crystal_description Plate _exptl_crystal_colour Yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.283 _exptl_crystal_F_000 348 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.060 _exptl_absorpt_coefficient_mu 0.727 _shelx_estimated_absorpt_T_min 0.868 _shelx_estimated_absorpt_T_max 0.958 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.82417 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.16b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 29673 _diffrn_reflns_av_unetI/netI 0.0093 _diffrn_reflns_av_R_equivalents 0.0219 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_theta_min 3.974 _diffrn_reflns_theta_max 66.576 _diffrn_reflns_theta_full 66.576 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.975 _diffrn_reflns_point_group_measured_fraction_full 0.975 _reflns_number_total 2867 _reflns_number_gt 2850 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.812 _reflns_Friedel_fraction_max 0.946 _reflns_Friedel_fraction_full 0.946 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were first found in the difference map, then generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0436P)^2^+0.0956P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_extinction_coef 0.0324(19) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_abs_structure_details ; Flack x determined using 1266 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.04(4) _chemical_absolute_configuration ad _refine_ls_number_reflns 2867 _refine_ls_number_parameters 213 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0275 _refine_ls_R_factor_gt 0.0273 _refine_ls_wR_factor_ref 0.0679 _refine_ls_wR_factor_gt 0.0677 _refine_ls_goodness_of_fit_ref 1.129 _refine_ls_restrained_S_all 1.129 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.48492(14) 0.24755(16) 0.22024(11) 0.0252(3) Uani 1 1 d . . . . . O2 O 0.50089(12) 0.36415(16) 0.04395(10) 0.0214(3) Uani 1 1 d . . . . . O3 O 0.94220(14) 0.55955(17) 0.09543(10) 0.0253(3) Uani 1 1 d . . . . . O4 O 1.07807(14) 0.71883(17) 0.23864(11) 0.0252(3) Uani 1 1 d . . . . . N1 N 0.78332(17) 0.8273(2) 0.33804(14) 0.0263(4) Uani 1 1 d . . . . . C1 C 0.84464(17) 0.3654(2) 0.28484(14) 0.0170(3) Uani 1 1 d . . . . . C2 C 0.82714(19) 0.2925(2) 0.40568(14) 0.0204(4) Uani 1 1 d . . . . . H2A H 0.7566 0.1994 0.3890 0.024 Uiso 1 1 calc R U . . . H2B H 0.9270 0.2516 0.4504 0.024 Uiso 1 1 calc R U . . . C3 C 0.76763(19) 0.4137(2) 0.48442(14) 0.0206(4) Uani 1 1 d . . . . . H3A H 0.8411 0.5038 0.5055 0.025 Uiso 1 1 calc R U . . . H3B H 0.7594 0.3600 0.5600 0.025 Uiso 1 1 calc R U . . . C4 C 0.61260(18) 0.4821(2) 0.42196(14) 0.0190(4) Uani 1 1 d . . . . . H4 H 0.5408 0.3887 0.4037 0.023 Uiso 1 1 calc R U . . . C5 C 0.61917(17) 0.5612(2) 0.29977(13) 0.0170(3) Uani 1 1 d . . . . . C6 C 0.69170(17) 0.4457(2) 0.22096(14) 0.0161(3) Uani 1 1 d . . . . . H6 H 0.7153 0.5147 0.1557 0.019 Uiso 1 1 calc R U . . . C7 C 0.59127(19) 0.3063(2) 0.15655(14) 0.0185(4) Uani 1 1 d . . . . . C8 C 0.7013(2) 0.1713(2) 0.13808(17) 0.0268(4) Uani 1 1 d . . . . . H8A H 0.6774 0.0692 0.1750 0.032 Uiso 1 1 calc R U . . . H8B H 0.6925 0.1523 0.0512 0.032 Uiso 1 1 calc R U . . . C9 C 0.8623(2) 0.2275(2) 0.19811(15) 0.0215(4) Uani 1 1 d . . . . . H9A H 0.9153 0.2669 0.1370 0.026 Uiso 1 1 calc R U . . . H9B H 0.9216 0.1372 0.2428 0.026 Uiso 1 1 calc R U . . . C10 C 0.71482(18) 0.7089(2) 0.32279(14) 0.0184(4) Uani 1 1 d . . . . . C11 C 0.5518(2) 0.5957(2) 0.50547(16) 0.0252(4) Uani 1 1 d . . . . . H11A H 0.5523 0.5398 0.5812 0.038 Uiso 1 1 calc R U . . . H11B H 0.4478 0.6280 0.4669 0.038 Uiso 1 1 calc R U . . . H11C H 0.6165 0.6920 0.5219 0.038 Uiso 1 1 calc R U . . . C12 C 0.46150(18) 0.6220(2) 0.23073(16) 0.0214(4) Uani 1 1 d . . . . . H12A H 0.4276 0.7093 0.2763 0.032 Uiso 1 1 calc R U . . . H12B H 0.3885 0.5327 0.2205 0.032 Uiso 1 1 calc R U . . . H12C H 0.4686 0.6626 0.1516 0.032 Uiso 1 1 calc R U . . . C13 C 0.3669(2) 0.1767(2) 0.12861(17) 0.0273(4) Uani 1 1 d . . . . . H13A H 0.2712 0.1658 0.1559 0.033 Uiso 1 1 calc R U . . . H13B H 0.3974 0.0693 0.1039 0.033 Uiso 1 1 calc R U . . . C14 C 0.3512(2) 0.2984(3) 0.02818(16) 0.0259(4) Uani 1 1 d . . . . . H14A H 0.3184 0.2453 -0.0512 0.031 Uiso 1 1 calc R U . . . H14B H 0.2770 0.3837 0.0354 0.031 Uiso 1 1 calc R U . . . C15 C 0.98297(17) 0.4823(2) 0.30750(14) 0.0184(4) Uani 1 1 d . . . . . H15 H 0.9730 0.5566 0.3742 0.022 Uiso 1 1 calc R U . . . C16 C 0.99436(17) 0.5872(2) 0.20053(15) 0.0186(4) Uani 1 1 d . . . . . C17 C 1.0973(2) 0.8300(3) 0.14626(18) 0.0302(4) Uani 1 1 d . . . . . H17A H 1.1497 0.7753 0.0913 0.045 Uiso 1 1 calc R U . . . H17B H 1.1578 0.9228 0.1832 0.045 Uiso 1 1 calc R U . . . H17C H 0.9976 0.8676 0.1014 0.045 Uiso 1 1 calc R U . . . C18 C 1.1354(2) 0.3937(3) 0.34769(18) 0.0298(4) Uani 1 1 d . . . . . H18A H 1.1522 0.3253 0.2819 0.045 Uiso 1 1 calc R U . . . H18B H 1.1336 0.3261 0.4178 0.045 Uiso 1 1 calc R U . . . H18C H 1.2177 0.4730 0.3690 0.045 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0303(7) 0.0263(7) 0.0206(6) -0.0026(5) 0.0091(5) -0.0128(5) O2 0.0185(6) 0.0271(7) 0.0165(6) 0.0013(5) -0.0001(4) -0.0054(5) O3 0.0274(6) 0.0319(7) 0.0167(6) 0.0004(5) 0.0054(5) -0.0052(5) O4 0.0244(6) 0.0282(7) 0.0231(6) 0.0006(5) 0.0057(5) -0.0080(5) N1 0.0257(7) 0.0224(9) 0.0301(8) -0.0010(6) 0.0053(6) -0.0035(6) C1 0.0168(7) 0.0178(8) 0.0164(8) 0.0024(7) 0.0037(6) 0.0024(6) C2 0.0226(8) 0.0211(9) 0.0175(8) 0.0036(7) 0.0047(6) 0.0017(7) C3 0.0227(8) 0.0254(10) 0.0142(7) 0.0022(7) 0.0052(6) -0.0016(7) C4 0.0199(8) 0.0218(9) 0.0163(8) -0.0014(7) 0.0065(6) -0.0027(7) C5 0.0155(7) 0.0181(9) 0.0173(7) -0.0006(7) 0.0036(6) -0.0008(6) C6 0.0159(7) 0.0182(9) 0.0141(7) 0.0014(6) 0.0033(6) -0.0015(6) C7 0.0221(8) 0.0199(9) 0.0136(7) 0.0016(7) 0.0045(6) -0.0019(7) C8 0.0310(10) 0.0219(10) 0.0252(9) -0.0033(7) 0.0022(7) 0.0018(7) C9 0.0263(9) 0.0188(9) 0.0207(8) -0.0005(7) 0.0081(6) 0.0031(7) C10 0.0175(8) 0.0214(9) 0.0166(7) 0.0010(7) 0.0044(6) 0.0036(7) C11 0.0224(8) 0.0321(11) 0.0226(8) -0.0063(7) 0.0082(7) -0.0028(7) C12 0.0158(8) 0.0251(10) 0.0230(8) -0.0006(7) 0.0038(6) 0.0008(7) C13 0.0264(9) 0.0267(11) 0.0308(9) -0.0090(8) 0.0104(8) -0.0106(7) C14 0.0190(8) 0.0287(10) 0.0282(9) -0.0080(8) 0.0019(7) -0.0066(7) C15 0.0156(7) 0.0247(9) 0.0147(7) 0.0011(6) 0.0033(6) 0.0008(6) C16 0.0132(7) 0.0230(9) 0.0202(8) -0.0001(7) 0.0054(6) 0.0010(6) C17 0.0268(9) 0.0293(11) 0.0351(10) 0.0076(8) 0.0086(7) -0.0065(8) C18 0.0192(8) 0.0401(12) 0.0297(9) 0.0101(9) 0.0048(7) 0.0061(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C7 1.420(2) . ? O1 C13 1.437(2) . ? O2 C14 1.432(2) . ? O2 C7 1.439(2) . ? O3 C16 1.207(2) . ? O4 C16 1.340(2) . ? O4 C17 1.441(2) . ? N1 C10 1.150(3) . ? C1 C9 1.543(2) . ? C1 C2 1.548(2) . ? C1 C15 1.555(2) . ? C1 C6 1.557(2) . ? C2 C3 1.526(2) . ? C3 C4 1.528(2) . ? C4 C11 1.529(2) . ? C4 C5 1.556(2) . ? C5 C10 1.485(2) . ? C5 C12 1.547(2) . ? C5 C6 1.558(2) . ? C6 C7 1.545(2) . ? C7 C8 1.542(2) . ? C8 C9 1.532(2) . ? C13 C14 1.508(3) . ? C15 C16 1.522(2) . ? C15 C18 1.536(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C7 O1 C13 104.06(12) . . ? C14 O2 C7 108.21(13) . . ? C16 O4 C17 115.77(14) . . ? C9 C1 C2 109.44(14) . . ? C9 C1 C15 111.57(13) . . ? C2 C1 C15 109.70(13) . . ? C9 C1 C6 103.07(12) . . ? C2 C1 C6 108.76(13) . . ? C15 C1 C6 114.06(13) . . ? C3 C2 C1 113.19(14) . . ? C2 C3 C4 112.21(13) . . ? C3 C4 C11 111.03(14) . . ? C3 C4 C5 110.72(13) . . ? C11 C4 C5 113.36(15) . . ? C10 C5 C12 104.74(14) . . ? C10 C5 C4 109.14(13) . . ? C12 C5 C4 111.90(13) . . ? C10 C5 C6 107.48(12) . . ? C12 C5 C6 111.48(13) . . ? C4 C5 C6 111.74(13) . . ? C7 C6 C1 105.49(13) . . ? C7 C6 C5 116.92(13) . . ? C1 C6 C5 115.95(12) . . ? O1 C7 O2 105.06(13) . . ? O1 C7 C8 111.02(15) . . ? O2 C7 C8 111.72(13) . . ? O1 C7 C6 113.85(13) . . ? O2 C7 C6 109.20(13) . . ? C8 C7 C6 106.10(13) . . ? C9 C8 C7 107.26(14) . . ? C8 C9 C1 106.46(13) . . ? N1 C10 C5 176.93(17) . . ? O1 C13 C14 101.97(14) . . ? O2 C14 C13 103.70(14) . . ? C16 C15 C18 106.84(13) . . ? C16 C15 C1 114.91(13) . . ? C18 C15 C1 112.73(15) . . ? O3 C16 O4 122.63(16) . . ? O3 C16 C15 127.50(16) . . ? O4 C16 C15 109.84(13) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C9 C1 C2 C3 -164.69(13) . . . . ? C15 C1 C2 C3 72.59(17) . . . . ? C6 C1 C2 C3 -52.79(18) . . . . ? C1 C2 C3 C4 59.04(19) . . . . ? C2 C3 C4 C11 176.78(15) . . . . ? C2 C3 C4 C5 -56.37(18) . . . . ? C3 C4 C5 C10 -68.11(17) . . . . ? C11 C4 C5 C10 57.43(18) . . . . ? C3 C4 C5 C12 176.44(14) . . . . ? C11 C4 C5 C12 -58.02(19) . . . . ? C3 C4 C5 C6 50.62(17) . . . . ? C11 C4 C5 C6 176.16(13) . . . . ? C9 C1 C6 C7 33.69(15) . . . . ? C2 C1 C6 C7 -82.39(16) . . . . ? C15 C1 C6 C7 154.82(13) . . . . ? C9 C1 C6 C5 164.79(13) . . . . ? C2 C1 C6 C5 48.71(18) . . . . ? C15 C1 C6 C5 -74.08(16) . . . . ? C10 C5 C6 C7 -163.78(13) . . . . ? C12 C5 C6 C7 -49.54(19) . . . . ? C4 C5 C6 C7 76.51(17) . . . . ? C10 C5 C6 C1 70.75(17) . . . . ? C12 C5 C6 C1 -175.01(14) . . . . ? C4 C5 C6 C1 -48.96(17) . . . . ? C13 O1 C7 O2 36.43(16) . . . . ? C13 O1 C7 C8 -84.49(16) . . . . ? C13 O1 C7 C6 155.85(15) . . . . ? C14 O2 C7 O1 -16.39(17) . . . . ? C14 O2 C7 C8 104.07(16) . . . . ? C14 O2 C7 C6 -138.88(14) . . . . ? C1 C6 C7 O1 99.16(15) . . . . ? C5 C6 C7 O1 -31.4(2) . . . . ? C1 C6 C7 O2 -143.79(12) . . . . ? C5 C6 C7 O2 85.67(16) . . . . ? C1 C6 C7 C8 -23.24(16) . . . . ? C5 C6 C7 C8 -153.78(14) . . . . ? O1 C7 C8 C9 -120.64(15) . . . . ? O2 C7 C8 C9 122.44(15) . . . . ? C6 C7 C8 C9 3.53(18) . . . . ? C7 C8 C9 C1 17.75(19) . . . . ? C2 C1 C9 C8 83.98(16) . . . . ? C15 C1 C9 C8 -154.42(14) . . . . ? C6 C1 C9 C8 -31.61(17) . . . . ? C7 O1 C13 C14 -41.32(17) . . . . ? C7 O2 C14 C13 -9.02(18) . . . . ? O1 C13 C14 O2 30.62(17) . . . . ? C9 C1 C15 C16 70.15(18) . . . . ? C2 C1 C15 C16 -168.40(14) . . . . ? C6 C1 C15 C16 -46.13(18) . . . . ? C9 C1 C15 C18 -52.59(18) . . . . ? C2 C1 C15 C18 68.86(17) . . . . ? C6 C1 C15 C18 -168.87(14) . . . . ? C17 O4 C16 O3 2.4(2) . . . . ? C17 O4 C16 C15 -179.55(14) . . . . ? C18 C15 C16 O3 101.3(2) . . . . ? C1 C15 C16 O3 -24.5(2) . . . . ? C18 C15 C16 O4 -76.54(17) . . . . ? C1 C15 C16 O4 157.61(13) . . . . ? _refine_diff_density_max 0.169 _refine_diff_density_min -0.176 _refine_diff_density_rms 0.048 _shelx_res_file ; 007b-18129.res created by SHELXL-2014/7 TITL 007b-18129 CELL 1.54184 9.0491 8.2659 11.4323 90 103.333 90 ZERR 2 0.0001 0.0001 0.0001 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 36 54 2 8 L.S. 10 TEMP -180 SIZE 0.20 0.10 0.06 CONF MORE -1 ACTA WGHT 0.043600 0.095600 EXTI 0.032411 FVAR 1.84814 O1 4 0.484918 0.247551 0.220240 11.00000 0.03026 0.02628 = 0.02062 -0.00264 0.00913 -0.01282 O2 4 0.500888 0.364150 0.043952 11.00000 0.01848 0.02708 = 0.01654 0.00130 -0.00012 -0.00537 O3 4 0.942197 0.559555 0.095427 11.00000 0.02739 0.03188 = 0.01666 0.00044 0.00543 -0.00522 O4 4 1.078074 0.718834 0.238639 11.00000 0.02436 0.02822 = 0.02312 0.00058 0.00572 -0.00803 N1 3 0.783321 0.827303 0.338037 11.00000 0.02574 0.02245 = 0.03006 -0.00097 0.00531 -0.00346 C1 1 0.844643 0.365413 0.284836 11.00000 0.01681 0.01776 = 0.01644 0.00244 0.00365 0.00242 C2 1 0.827141 0.292543 0.405680 11.00000 0.02260 0.02112 = 0.01752 0.00355 0.00475 0.00166 AFIX 23 H2A 2 0.756606 0.199423 0.388993 11.00000 -1.20000 H2B 2 0.927045 0.251570 0.450386 11.00000 -1.20000 AFIX 0 C3 1 0.767629 0.413730 0.484420 11.00000 0.02270 0.02539 = 0.01416 0.00216 0.00516 -0.00157 AFIX 23 H3A 2 0.841108 0.503769 0.505456 11.00000 -1.20000 H3B 2 0.759400 0.359952 0.560034 11.00000 -1.20000 AFIX 0 C4 1 0.612602 0.482099 0.421961 11.00000 0.01992 0.02181 = 0.01626 -0.00137 0.00647 -0.00272 AFIX 13 H4 2 0.540760 0.388673 0.403692 11.00000 -1.20000 AFIX 0 C5 1 0.619175 0.561176 0.299767 11.00000 0.01545 0.01810 = 0.01732 -0.00059 0.00364 -0.00079 C6 1 0.691702 0.445704 0.220962 11.00000 0.01593 0.01820 = 0.01415 0.00136 0.00333 -0.00152 AFIX 13 H6 2 0.715315 0.514653 0.155736 11.00000 -1.20000 AFIX 0 C7 1 0.591274 0.306258 0.156546 11.00000 0.02210 0.01990 = 0.01359 0.00164 0.00454 -0.00191 C8 1 0.701345 0.171298 0.138077 11.00000 0.03102 0.02191 = 0.02524 -0.00332 0.00216 0.00175 AFIX 23 H8A 2 0.677386 0.069194 0.175038 11.00000 -1.20000 H8B 2 0.692457 0.152312 0.051228 11.00000 -1.20000 AFIX 0 C9 1 0.862275 0.227467 0.198105 11.00000 0.02629 0.01879 = 0.02075 -0.00048 0.00810 0.00310 AFIX 23 H9A 2 0.915323 0.266905 0.136961 11.00000 -1.20000 H9B 2 0.921596 0.137178 0.242841 11.00000 -1.20000 AFIX 0 C10 1 0.714824 0.708944 0.322793 11.00000 0.01755 0.02138 = 0.01657 0.00097 0.00440 0.00360 C11 1 0.551849 0.595661 0.505473 11.00000 0.02243 0.03210 = 0.02258 -0.00630 0.00825 -0.00276 AFIX 137 H11A 2 0.552254 0.539790 0.581153 11.00000 -1.50000 H11B 2 0.447837 0.628044 0.466931 11.00000 -1.50000 H11C 2 0.616509 0.691951 0.521872 11.00000 -1.50000 AFIX 0 C12 1 0.461497 0.622014 0.230726 11.00000 0.01583 0.02506 = 0.02298 -0.00064 0.00381 0.00079 AFIX 137 H12A 2 0.427585 0.709346 0.276295 11.00000 -1.50000 H12B 2 0.388452 0.532664 0.220491 11.00000 -1.50000 H12C 2 0.468550 0.662581 0.151649 11.00000 -1.50000 AFIX 0 C13 1 0.366950 0.176743 0.128606 11.00000 0.02641 0.02673 = 0.03075 -0.00902 0.01042 -0.01065 AFIX 23 H13A 2 0.271226 0.165846 0.155868 11.00000 -1.20000 H13B 2 0.397410 0.069318 0.103905 11.00000 -1.20000 AFIX 0 C14 1 0.351208 0.298365 0.028185 11.00000 0.01904 0.02867 = 0.02819 -0.00798 0.00192 -0.00657 AFIX 23 H14A 2 0.318378 0.245340 -0.051223 11.00000 -1.20000 H14B 2 0.277042 0.383697 0.035369 11.00000 -1.20000 AFIX 0 C15 1 0.982975 0.482303 0.307497 11.00000 0.01559 0.02473 = 0.01472 0.00111 0.00331 0.00085 AFIX 13 H15 2 0.972976 0.556648 0.374247 11.00000 -1.20000 AFIX 0 C16 1 0.994358 0.587175 0.200533 11.00000 0.01325 0.02304 = 0.02018 -0.00012 0.00543 0.00101 C17 1 1.097328 0.830024 0.146263 11.00000 0.02684 0.02931 = 0.03511 0.00761 0.00860 -0.00651 AFIX 137 H17A 2 1.149653 0.775302 0.091327 11.00000 -1.50000 H17B 2 1.157831 0.922850 0.183234 11.00000 -1.50000 H17C 2 0.997597 0.867562 0.101385 11.00000 -1.50000 AFIX 0 C18 1 1.135412 0.393664 0.347691 11.00000 0.01919 0.04009 = 0.02967 0.01011 0.00479 0.00610 AFIX 137 H18A 2 1.152227 0.325277 0.281944 11.00000 -1.50000 H18B 2 1.133608 0.326107 0.417791 11.00000 -1.50000 H18C 2 1.217678 0.473046 0.368985 11.00000 -1.50000 AFIX 0 HKLF 4 REM 007b-18129 REM R1 = 0.0273 for 2850 Fo > 4sig(Fo) and 0.0275 for all 2867 data REM 213 parameters refined using 1 restraints END WGHT 0.0423 0.0996 REM Highest difference peak 0.169, deepest hole -0.176, 1-sigma level 0.048 Q1 1 0.3690 0.6984 0.4327 11.00000 0.05 0.17 Q2 1 0.6167 0.5222 0.3616 11.00000 0.05 0.17 Q3 1 0.6532 0.5034 0.2604 11.00000 0.05 0.17 Q4 1 0.8415 0.3322 0.3512 11.00000 0.05 0.16 Q5 1 0.9170 0.4292 0.3005 11.00000 0.05 0.16 Q6 1 0.2613 0.2921 0.1845 11.00000 0.05 0.15 Q7 1 0.8005 0.3534 0.4428 11.00000 0.05 0.15 Q8 1 1.1883 0.3511 0.2174 11.00000 0.05 0.15 Q9 1 0.2468 0.2747 0.1563 11.00000 0.05 0.15 Q10 1 0.8306 0.6623 0.1461 11.00000 0.05 0.15 Q11 1 1.3399 0.4627 0.3287 11.00000 0.05 0.14 Q12 1 1.1754 0.3604 0.1486 11.00000 0.05 0.14 Q13 1 0.5425 0.5969 0.2644 11.00000 0.05 0.14 Q14 1 0.6964 0.4478 0.4536 11.00000 0.05 0.14 Q15 1 0.7643 0.4173 0.2559 11.00000 0.05 0.13 Q16 1 0.6391 0.3908 0.1991 11.00000 0.05 0.13 Q17 1 0.9230 0.5580 0.5037 11.00000 0.05 0.13 Q18 1 0.5380 0.2691 0.2080 11.00000 0.05 0.13 Q19 1 0.9617 0.5675 0.5170 11.00000 0.05 0.13 Q20 1 1.2049 0.3438 0.2924 11.00000 0.05 0.12 ; _shelx_res_checksum 77023 _shelx_hkl_file ; 0 -8 -5 94.36 4.81 0 -8 -6 120.22 5.11 0 -8 -7 145.69 4.92 0 -7 0 -1.24 5.16 0 -7 1 292.25 17.95 0 -7 1 257.49 17.70 0 -7 -1 282.30 19.24 0 -7 2 128.91 12.90 0 -7 -2 138.65 13.78 0 -7 3 6.94 5.59 0 -7 3 2.37 5.41 0 -7 3 9.82 6.12 0 -7 -3 3.94 5.49 0 -7 -4 254.01 7.92 0 -7 -6 15.31 2.50 0 -7 7 76.95 4.52 0 -7 -7 83.45 4.68 0 -7 -8 229.22 7.36 0 -7 8 242.94 7.09 0 -7 -9 12.61 1.91 0 -7 -9 10.50 1.93 0 -7 9 13.63 1.97 0 -6 0 292.94 15.91 0 -6 -1 213.11 15.19 0 -6 1 199.57 12.34 0 -6 1 200.42 12.13 0 -6 1 191.13 13.28 0 -6 -1 211.43 13.26 0 -6 -2 222.41 15.87 0 -6 -2 231.41 13.32 0 -6 2 216.62 13.57 0 -6 2 211.79 13.10 0 -6 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466.13 12.35 0 3 -3 456.10 8.14 0 3 -3 452.92 7.54 0 3 3 451.22 7.99 0 3 -3 437.71 11.39 0 3 3 461.21 10.95 0 3 -4 1383.42 14.01 0 3 -4 1390.60 21.72 0 3 4 1379.18 21.82 0 3 4 1340.18 13.67 0 3 -4 1367.85 17.35 0 3 -4 1393.02 14.07 0 3 -4 1391.29 23.20 0 3 4 1376.23 13.97 0 3 -4 1351.00 13.99 0 3 -4 1383.62 14.04 0 3 4 1349.65 14.53 0 3 4 1365.71 14.42 0 3 4 1397.67 14.57 0 3 4 1383.11 14.10 0 3 4 1355.92 22.96 0 3 4 1347.50 22.52 0 3 -4 1424.76 23.56 0 3 4 1400.57 14.17 0 3 4 1373.67 23.38 0 3 -4 1399.91 14.22 0 3 4 1415.54 15.78 0 3 -4 1350.58 14.12 0 3 -4 1348.33 22.94 0 3 5 1876.68 18.49 0 3 5 1840.42 17.34 0 3 -5 1838.19 16.07 0 3 5 1917.13 29.24 0 3 5 1881.27 28.98 0 3 -5 1949.78 18.25 0 3 -5 1929.07 17.44 0 3 -5 1920.89 17.96 0 3 5 1917.60 16.84 0 3 5 1815.68 28.83 0 3 -5 1887.85 17.58 0 3 5 1882.87 28.92 0 3 5 1892.69 18.37 0 3 5 1878.80 18.25 0 3 5 1912.26 17.73 0 3 -5 1892.32 27.49 0 3 -5 1903.16 24.02 0 3 -5 1935.17 29.54 0 3 -5 1861.87 17.62 0 3 5 1856.32 16.53 0 3 -5 1883.42 29.50 0 3 -5 1889.24 29.58 0 3 -5 1914.07 18.10 0 3 -5 1885.08 17.51 0 3 5 1948.36 17.48 0 3 5 1885.31 17.46 0 3 -5 1912.78 17.69 0 3 -6 1120.96 14.63 0 3 -6 1149.47 15.17 0 3 6 1122.35 24.92 0 3 -6 1128.36 14.61 0 3 -6 1117.41 14.97 0 3 -6 1142.73 14.71 0 3 6 1110.86 13.87 0 3 -6 1083.66 24.50 0 3 6 1123.55 14.39 0 3 6 1163.80 24.42 0 3 6 1118.90 24.72 0 3 -6 1125.24 14.63 0 3 -6 1137.23 14.74 0 3 6 1149.72 14.67 0 3 6 1146.60 14.48 0 3 -6 1147.79 15.09 0 3 6 1113.95 15.60 0 3 -6 1135.71 13.43 0 3 -6 1121.73 24.67 0 3 6 1131.68 14.15 0 3 6 1157.43 24.16 0 3 6 1138.89 14.30 0 3 6 1109.96 15.08 0 3 -6 1123.73 21.01 0 3 -6 1173.80 23.54 0 3 -7 213.04 7.14 0 3 7 222.52 6.62 0 3 -7 195.44 6.64 0 3 7 210.17 6.61 0 3 7 206.31 7.23 0 3 7 216.39 6.69 0 3 -7 198.47 10.05 0 3 -7 199.33 11.29 0 3 -7 203.75 7.07 0 3 -7 209.76 6.72 0 3 -7 201.36 11.54 0 3 7 215.98 6.55 0 3 -7 212.61 6.94 0 3 7 214.70 6.80 0 3 -7 196.68 5.84 0 3 -7 214.19 10.98 0 3 -7 198.09 6.76 0 3 7 209.81 6.78 0 3 -7 216.13 7.19 0 3 7 208.26 7.06 0 3 7 211.75 11.85 0 3 7 217.33 11.52 0 3 -8 207.92 7.09 0 3 8 221.24 13.19 0 3 8 208.28 7.14 0 3 8 215.20 11.97 0 3 -8 218.86 12.79 0 3 -8 200.75 7.41 0 3 -8 204.38 6.38 0 3 -8 205.07 7.27 0 3 8 206.89 7.11 0 3 -8 212.80 7.72 0 3 8 216.43 13.12 0 3 -8 215.54 7.33 0 3 -8 209.97 7.28 0 3 8 188.36 7.04 0 3 8 199.76 6.42 0 3 8 190.70 6.62 0 3 8 202.43 6.51 0 3 -8 213.71 7.47 0 3 8 210.69 7.49 0 3 9 668.40 13.54 0 3 9 655.11 12.65 0 3 -9 643.35 13.52 0 3 9 586.21 12.45 0 3 -9 620.45 12.80 0 3 -9 629.67 22.66 0 3 9 639.88 11.74 0 3 -9 644.93 12.45 0 3 -9 638.67 12.50 0 3 9 648.18 23.67 0 3 9 641.96 12.51 0 3 -9 610.80 12.73 0 3 -9 652.80 13.26 0 3 9 633.98 23.05 0 3 -9 637.61 11.45 0 3 -10 73.37 4.56 0 3 -10 58.95 4.40 0 3 -10 62.38 4.02 0 3 -10 63.65 4.35 0 3 10 65.79 4.31 0 3 10 62.39 4.13 0 3 10 61.69 4.44 0 3 -10 63.70 4.41 0 3 -10 61.68 3.93 0 3 -10 50.81 3.54 0 3 11 175.94 6.21 0 3 -11 164.96 6.30 0 3 11 187.41 6.83 0 3 -11 170.61 6.61 0 3 -11 160.85 6.12 0 3 -11 175.62 5.75 0 3 11 179.68 6.02 0 3 -12 65.98 3.41 0 3 12 58.03 3.27 0 3 -12 60.63 3.46 0 3 -12 60.83 3.60 0 3 12 55.80 3.50 0 4 0 462.32 12.47 0 4 0 483.93 13.02 0 4 0 469.69 13.20 0 4 0 467.99 11.54 0 4 0 466.70 10.89 0 4 0 467.14 11.77 0 4 1 441.28 7.96 0 4 -1 437.78 11.88 0 4 1 470.93 13.09 0 4 -1 447.90 12.74 0 4 1 422.33 7.75 0 4 1 422.68 7.65 0 4 -1 421.88 11.23 0 4 1 429.23 11.38 0 4 -1 419.10 10.75 0 4 1 445.40 9.43 0 4 -1 435.11 11.71 0 4 -1 425.69 10.78 0 4 1 424.41 12.11 0 4 1 447.00 13.22 0 4 1 428.89 7.50 0 4 -2 1370.59 22.42 0 4 2 1331.51 21.39 0 4 2 1399.53 23.69 0 4 2 1356.42 14.02 0 4 -2 1401.66 13.90 0 4 2 1359.80 22.83 0 4 2 1378.68 13.35 0 4 2 1331.15 13.85 0 4 2 1404.19 15.54 0 4 2 1407.60 14.42 0 4 -2 1390.86 13.70 0 4 2 1385.71 14.33 0 4 -2 1394.79 13.89 0 4 -2 1407.23 14.38 0 4 -2 1391.72 22.77 0 4 2 1391.09 14.64 0 4 -2 1401.42 17.77 0 4 -2 1344.98 14.18 0 4 -2 1440.30 23.49 0 4 2 1377.06 14.64 0 4 -2 1431.08 19.37 0 4 -2 1364.43 22.30 0 4 -3 278.83 6.62 0 4 3 289.07 6.80 0 4 -3 288.30 6.78 0 4 3 259.51 10.26 0 4 -3 281.47 6.82 0 4 3 292.41 7.08 0 4 3 288.78 11.38 0 4 3 287.43 6.58 0 4 -3 281.96 11.08 0 4 3 290.75 11.27 0 4 -3 268.02 10.97 0 4 -3 276.71 6.58 0 4 3 270.13 8.51 0 4 3 277.57 6.84 0 4 -3 288.95 6.78 0 4 3 271.70 6.65 0 4 3 276.75 6.80 0 4 3 288.63 7.15 0 4 -3 265.33 7.85 0 4 -3 282.94 6.85 0 4 -3 277.49 6.18 0 4 -3 294.91 10.83 0 4 -3 280.95 11.10 0 4 -3 291.37 6.47 0 4 -4 291.49 12.14 0 4 -4 317.08 7.51 0 4 -4 319.13 7.48 0 4 4 290.10 12.15 0 4 4 303.93 7.53 0 4 -4 294.12 6.62 0 4 -4 284.45 11.88 0 4 4 313.21 7.51 0 4 4 290.49 7.50 0 4 -4 304.55 7.37 0 4 4 302.61 7.35 0 4 -4 289.53 7.10 0 4 4 317.54 6.63 0 4 4 298.09 7.72 0 4 4 290.62 10.26 0 4 -4 309.61 7.45 0 4 4 289.21 12.22 0 4 4 302.49 7.19 0 4 -4 290.55 11.22 0 4 4 298.35 7.62 0 4 4 299.40 7.24 0 4 4 311.40 11.81 0 4 -4 310.84 6.93 0 4 -4 296.89 7.31 0 4 -4 327.04 7.76 0 4 5 665.56 12.01 0 4 -5 645.43 19.19 0 4 -5 679.55 10.35 0 4 5 637.12 11.31 0 4 5 668.96 19.30 0 4 5 665.47 12.02 0 4 -5 663.43 11.33 0 4 5 637.66 11.45 0 4 5 659.57 11.46 0 4 5 634.54 11.67 0 4 5 656.78 11.22 0 4 -5 568.28 10.63 0 4 5 682.66 19.68 0 4 -5 646.75 11.44 0 4 5 670.94 10.26 0 4 -5 673.16 10.96 0 4 -5 668.84 11.52 0 4 -5 659.86 11.47 0 4 -5 629.04 17.32 0 4 -5 663.99 11.59 0 4 -5 667.75 11.73 0 4 -5 613.31 18.69 0 4 5 654.43 18.60 0 4 5 634.01 9.97 0 4 -6 476.05 10.47 0 4 6 478.55 9.33 0 4 6 479.95 10.18 0 4 6 470.71 17.32 0 4 -6 475.59 9.90 0 4 -6 481.59 10.27 0 4 -6 437.94 10.08 0 4 6 482.72 11.04 0 4 6 470.20 9.41 0 4 6 447.57 10.55 0 4 6 460.81 10.06 0 4 -6 464.78 17.42 0 4 -6 452.28 17.25 0 4 -6 476.35 15.97 0 4 -6 461.32 10.20 0 4 6 476.31 9.99 0 4 6 463.16 17.16 0 4 6 459.98 17.03 0 4 -6 482.21 10.54 0 4 -6 483.19 10.50 0 4 6 466.37 10.22 0 4 6 483.38 16.60 0 4 -6 478.88 10.17 0 4 -7 70.08 4.57 0 4 7 76.10 4.15 0 4 7 76.27 4.49 0 4 7 76.66 4.21 0 4 7 77.55 4.75 0 4 -7 71.74 4.50 0 4 -7 73.82 4.62 0 4 -7 76.73 4.66 0 4 7 67.11 7.22 0 4 7 68.68 7.62 0 4 -7 77.30 4.81 0 4 7 73.52 4.37 0 4 7 81.61 7.98 0 4 7 72.04 4.43 0 4 -7 80.36 4.82 0 4 -7 77.16 7.97 0 4 -7 79.14 4.54 0 4 -7 71.19 7.51 0 4 7 81.33 4.44 0 4 7 74.87 4.94 0 4 -8 210.20 7.81 0 4 8 225.80 13.37 0 4 -8 229.02 7.70 0 4 -8 208.07 7.59 0 4 8 225.06 7.43 0 4 8 225.96 7.36 0 4 8 207.02 7.17 0 4 8 219.83 7.84 0 4 8 214.01 7.36 0 4 8 210.27 13.13 0 4 -8 228.11 8.08 0 4 8 235.01 7.19 0 4 -8 217.00 7.63 0 4 -8 217.50 7.47 0 4 8 208.68 7.42 0 4 -8 224.31 8.12 0 4 -8 222.29 13.61 0 4 8 226.85 13.23 0 4 -9 592.75 12.94 0 4 9 605.22 12.33 0 4 -9 601.33 12.38 0 4 9 575.26 11.63 0 4 9 543.17 12.25 0 4 9 574.81 11.99 0 4 -9 570.79 12.13 0 4 -9 578.57 12.18 0 4 -9 590.05 12.57 0 4 9 614.60 11.73 0 4 -9 575.60 12.75 0 4 -10 228.43 7.26 0 4 10 219.70 6.75 0 4 -10 234.16 7.39 0 4 -10 236.32 7.90 0 4 10 234.68 6.99 0 4 -10 224.99 7.88 0 4 10 230.49 7.27 0 4 -10 238.45 7.44 0 4 10 217.63 7.30 0 4 -10 238.00 7.79 0 4 -11 147.22 5.19 0 4 11 148.91 5.34 0 4 -11 154.49 5.42 0 4 -11 156.32 5.65 0 4 -11 152.79 5.88 0 4 11 151.84 5.47 0 4 -11 152.12 5.20 0 4 -12 53.99 3.16 0 4 -12 59.93 3.06 0 5 0 1.99 1.35 0 5 0 -0.74 1.41 0 5 0 -2.25 2.41 0 5 0 1.20 2.00 0 5 0 4.18 1.26 0 5 0 -0.29 1.28 0 5 0 -0.22 1.17 0 5 0 -0.13 1.24 0 5 0 -0.08 1.25 0 5 0 1.00 1.90 0 5 0 0.15 1.20 0 5 0 1.46 2.36 0 5 0 -1.66 1.48 0 5 0 -0.34 1.34 0 5 -1 99.26 4.43 0 5 1 96.68 4.23 0 5 1 100.35 4.33 0 5 1 104.57 6.54 0 5 -1 91.63 5.96 0 5 1 100.88 3.99 0 5 1 97.98 7.38 0 5 1 100.83 4.48 0 5 -1 112.28 7.60 0 5 1 101.00 4.28 0 5 1 96.22 4.40 0 5 -1 97.61 3.99 0 5 1 94.37 4.07 0 5 -1 93.20 4.05 0 5 -1 105.23 4.42 0 5 1 98.58 7.22 0 5 1 97.81 7.00 0 5 -1 104.82 4.25 0 5 -1 97.37 4.01 0 5 -1 88.05 3.69 0 5 -1 99.43 4.21 0 5 -1 96.12 6.57 0 5 1 97.90 4.47 0 5 1 90.16 4.19 0 5 -1 99.63 4.27 0 5 -1 111.51 7.48 0 5 -1 103.06 3.93 0 5 2 721.14 19.94 0 5 -2 777.63 19.23 0 5 -2 734.70 10.47 0 5 2 731.73 11.91 0 5 -2 730.51 11.79 0 5 -2 760.93 19.71 0 5 -2 743.71 11.34 0 5 2 730.13 11.06 0 5 2 735.08 12.08 0 5 -2 736.45 11.46 0 5 2 758.35 11.82 0 5 -2 735.49 11.37 0 5 -2 740.84 16.81 0 5 2 728.19 11.87 0 5 -2 734.99 11.92 0 5 2 728.13 11.48 0 5 -2 733.38 11.15 0 5 -2 730.12 10.69 0 5 2 735.42 12.07 0 5 2 697.94 18.91 0 5 -2 762.26 11.01 0 5 2 731.10 17.82 0 5 2 751.68 11.74 0 5 -3 291.78 7.54 0 5 3 306.37 13.13 0 5 -3 290.44 7.81 0 5 3 289.96 8.04 0 5 -3 301.84 12.37 0 5 3 301.18 8.13 0 5 -3 306.55 13.18 0 5 -3 286.09 7.43 0 5 3 298.69 7.83 0 5 -3 302.38 7.14 0 5 -3 281.70 12.46 0 5 3 294.59 12.02 0 5 3 297.92 7.80 0 5 -3 294.45 7.64 0 5 3 297.59 7.78 0 5 -3 281.61 7.59 0 5 3 292.85 7.47 0 5 -3 305.62 7.54 0 5 3 293.63 13.43 0 5 3 291.31 7.86 0 5 -3 296.43 7.09 0 5 3 296.37 7.40 0 5 -4 1619.80 17.93 0 5 -4 1639.59 29.29 0 5 -4 1686.68 18.68 0 5 -4 1633.67 18.60 0 5 -4 1653.41 18.76 0 5 4 1639.06 18.15 0 5 -4 1635.46 17.01 0 5 4 1678.20 32.71 0 5 4 1652.07 18.85 0 5 -4 1655.31 16.66 0 5 4 1582.99 18.02 0 5 -4 1612.23 18.98 0 5 -4 1603.33 18.52 0 5 4 1673.51 19.08 0 5 4 1660.65 19.78 0 5 -4 1623.24 18.53 0 5 4 1643.19 19.25 0 5 4 1642.59 19.70 0 5 -4 1608.41 31.19 0 5 4 1690.39 19.29 0 5 4 1611.31 29.83 0 5 -4 1651.62 32.03 0 5 4 1631.53 31.83 0 5 -5 104.53 7.83 0 5 -5 99.15 5.15 0 5 -5 103.25 8.87 0 5 -5 101.17 4.94 0 5 5 115.57 5.57 0 5 5 113.96 9.26 0 5 5 110.26 5.26 0 5 -5 101.52 4.54 0 5 -5 98.03 5.16 0 5 5 101.19 5.13 0 5 5 110.34 5.35 0 5 5 100.93 5.37 0 5 5 99.82 5.01 0 5 -5 106.39 5.22 0 5 5 102.85 8.39 0 5 -5 110.20 5.18 0 5 -5 96.96 4.90 0 5 5 101.17 8.65 0 5 5 98.38 4.88 0 5 -5 105.02 5.05 0 5 6 380.90 17.19 0 5 6 369.26 9.83 0 5 6 338.86 16.22 0 5 6 373.29 9.57 0 5 6 361.81 10.21 0 5 -6 369.90 9.90 0 5 -6 380.19 9.88 0 5 6 380.60 10.00 0 5 -6 379.57 9.88 0 5 -6 387.92 17.15 0 5 6 368.61 10.34 0 5 -6 373.74 9.91 0 5 -6 375.29 9.58 0 5 -6 377.97 9.74 0 5 6 390.73 16.62 0 5 -6 367.70 9.96 0 5 6 366.23 9.68 0 5 7 11.68 2.55 0 5 7 11.98 2.48 0 5 7 10.16 2.68 0 5 -7 12.79 2.83 0 5 -7 8.70 2.51 0 5 -7 10.38 2.62 0 5 -7 9.83 4.28 0 5 7 6.85 4.25 0 5 7 7.91 2.39 0 5 -7 10.98 2.56 0 5 -7 10.32 2.18 0 5 -7 11.74 2.85 0 5 7 9.68 4.49 0 5 7 11.71 2.54 0 5 7 9.71 2.57 0 5 -7 12.22 2.81 0 5 -8 873.72 14.96 0 5 8 871.91 16.08 0 5 -8 881.07 15.34 0 5 8 867.22 15.01 0 5 -8 884.10 15.56 0 5 8 896.68 15.25 0 5 8 898.43 14.89 0 5 -8 909.53 15.57 0 5 -8 895.11 15.35 0 5 -8 846.17 15.50 0 5 -8 876.05 15.83 0 5 8 875.59 14.99 0 5 9 80.86 4.44 0 5 9 73.76 4.22 0 5 -9 77.37 4.74 0 5 9 76.05 4.57 0 5 -9 74.68 4.73 0 5 -9 71.33 4.75 0 5 -9 71.30 4.36 0 5 -9 71.36 4.51 0 5 -9 69.34 4.44 0 5 9 70.32 4.68 0 5 9 71.76 4.23 0 5 -10 159.47 5.90 0 5 -10 155.86 5.85 0 5 -10 149.90 6.01 0 5 -10 155.20 6.10 0 5 10 155.11 5.39 0 5 -10 172.00 6.22 0 5 -10 157.46 5.53 0 5 10 160.29 5.85 0 5 -11 125.21 4.78 0 5 11 129.73 4.53 0 5 -11 126.58 4.65 0 5 -11 119.19 4.32 0 5 -11 119.31 4.32 0 6 0 275.73 7.89 0 6 0 282.24 7.61 0 6 0 298.01 7.49 0 6 0 288.96 13.53 0 6 0 287.94 7.59 0 6 0 276.92 12.90 0 6 0 282.10 7.80 0 6 0 292.04 8.12 0 6 0 277.78 12.29 0 6 0 290.89 8.11 0 6 0 305.27 8.23 0 6 -1 204.15 6.07 0 6 1 201.47 6.79 0 6 1 207.78 6.81 0 6 1 191.71 11.21 0 6 1 197.71 6.69 0 6 -1 199.88 6.60 0 6 1 197.68 10.89 0 6 1 186.99 6.78 0 6 -1 194.30 6.14 0 6 1 200.12 6.70 0 6 -1 206.32 6.86 0 6 1 203.72 6.19 0 6 -1 204.51 6.80 0 6 -1 194.66 6.24 0 6 -1 193.39 10.40 0 6 -1 196.96 6.01 0 6 -1 200.93 6.59 0 6 1 192.60 6.52 0 6 -1 188.72 6.30 0 6 -1 205.43 11.50 0 6 1 195.61 6.42 0 6 -2 217.67 6.71 0 6 2 211.25 7.25 0 6 2 217.01 7.20 0 6 2 207.30 10.77 0 6 -2 219.03 7.00 0 6 -2 227.20 12.32 0 6 2 222.47 7.38 0 6 -2 217.45 11.63 0 6 2 222.11 6.95 0 6 -2 206.48 6.37 0 6 -2 214.35 7.25 0 6 2 213.55 11.84 0 6 -2 221.17 6.73 0 6 2 209.16 6.51 0 6 2 199.37 7.22 0 6 -2 211.22 6.77 0 6 -2 207.50 6.90 0 6 2 219.12 12.65 0 6 2 202.58 7.00 0 6 2 221.56 7.04 0 6 -2 215.84 6.58 0 6 3 529.49 19.20 0 6 3 540.51 20.09 0 6 3 520.77 11.15 0 6 3 525.29 10.81 0 6 3 536.84 11.47 0 6 -3 536.70 10.69 0 6 -3 524.74 11.05 0 6 3 517.15 11.49 0 6 -3 530.82 18.00 0 6 -3 532.63 11.50 0 6 3 522.07 17.57 0 6 -3 534.14 10.39 0 6 -3 510.87 18.98 0 6 -3 529.37 11.14 0 6 3 521.31 11.72 0 6 3 527.20 11.38 0 6 3 530.93 10.67 0 6 -3 524.99 10.88 0 6 3 543.04 11.74 0 6 -3 530.05 10.05 0 6 -3 554.10 11.23 0 6 -4 1161.15 29.41 0 6 4 1160.99 17.15 0 6 4 1192.77 29.72 0 6 4 1157.84 27.14 0 6 -4 1199.20 16.63 0 6 4 1220.53 18.40 0 6 4 1192.44 16.60 0 6 -4 1189.18 17.12 0 6 4 1148.75 29.96 0 6 -4 1166.79 17.51 0 6 -4 1203.88 16.96 0 6 -4 1160.06 16.80 0 6 4 1191.65 17.62 0 6 4 1185.70 17.42 0 6 -4 1195.31 17.11 0 6 -4 1158.37 15.69 0 6 4 1196.43 17.86 0 6 4 1168.59 18.01 0 6 5 659.28 13.51 0 6 -5 669.42 12.54 0 6 -5 668.69 12.81 0 6 5 648.65 23.14 0 6 5 676.96 14.11 0 6 5 644.00 13.72 0 6 -5 637.53 13.06 0 6 -5 647.91 12.94 0 6 5 657.26 23.02 0 6 5 653.61 13.38 0 6 -5 661.48 23.04 0 6 5 621.55 21.12 0 6 -5 669.39 13.13 0 6 -5 665.29 13.43 0 6 -5 650.75 13.12 0 6 5 643.70 12.77 0 6 5 684.44 13.58 0 6 5 671.64 13.52 0 6 -6 89.79 5.02 0 6 6 97.07 9.91 0 6 6 94.00 5.47 0 6 -6 99.26 5.58 0 6 -6 98.92 5.63 0 6 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2.62 -1 6 6 15.33 3.18 -1 6 6 13.43 2.86 -1 6 5 48.74 6.83 1 6 -5 57.51 3.81 1 6 -5 63.03 4.58 1 6 -5 55.87 3.83 -1 6 5 60.47 4.64 -1 6 5 61.12 4.47 1 6 -5 71.78 4.78 -1 6 5 63.98 4.57 1 6 -5 61.21 4.49 -1 6 5 60.00 4.39 1 6 -5 59.37 4.23 -1 6 5 63.76 4.22 -1 6 5 74.27 8.45 1 6 -5 61.89 4.52 -1 6 5 61.43 4.23 1 6 -5 68.13 8.56 1 6 -5 65.38 4.62 -1 6 5 58.92 4.47 1 6 -5 57.87 7.42 -1 6 4 183.68 7.01 1 6 -4 181.72 7.25 1 6 -4 189.23 6.74 -1 6 4 196.42 12.53 -1 6 4 192.25 7.34 -1 6 4 202.19 6.85 1 6 -4 186.78 11.76 1 6 -4 192.23 6.95 -1 6 4 203.99 11.98 1 6 -4 185.00 6.69 -1 6 4 195.83 7.26 1 6 -4 193.09 7.49 1 6 -4 188.74 7.06 -1 6 4 191.19 7.57 -1 6 4 188.01 7.14 1 6 -4 181.83 12.24 1 6 -4 194.29 7.23 -1 6 4 183.70 6.76 1 6 -3 198.73 6.70 -1 6 3 204.05 12.37 -1 6 3 191.88 6.97 -1 6 3 197.22 6.70 -1 6 3 193.80 6.99 1 6 -3 180.33 11.48 1 6 -3 186.81 11.96 -1 6 3 205.27 11.71 1 6 -3 184.34 6.21 -1 6 3 186.08 7.11 1 6 -3 186.15 6.83 -1 6 3 186.68 6.56 -1 6 3 197.71 6.99 -1 6 3 183.26 6.91 1 6 -3 181.76 6.93 -1 6 3 185.24 11.69 1 6 -3 188.44 7.09 1 6 -3 181.79 6.62 1 6 -3 183.14 6.76 1 6 -3 191.34 6.30 1 6 -2 217.33 6.48 1 6 -2 231.66 7.57 -1 6 2 224.32 7.37 1 6 -2 212.80 6.97 -1 6 2 219.13 12.09 1 6 -2 217.00 7.20 -1 6 2 224.39 11.97 -1 6 2 223.51 7.28 1 6 -2 225.82 6.83 1 6 -2 215.97 7.21 -1 6 2 224.02 7.21 1 6 -2 225.86 6.92 1 6 -2 209.08 12.02 -1 6 2 223.00 12.45 -1 6 2 218.77 7.15 1 6 -2 220.95 7.71 -1 6 2 225.92 6.87 -1 6 2 220.09 7.06 1 6 -2 217.69 10.81 -1 6 2 217.35 6.80 1 6 -1 349.37 8.35 -1 6 1 357.74 8.75 1 6 -1 350.79 9.24 1 6 -1 358.49 8.96 -1 6 1 361.97 14.40 -1 6 1 356.60 8.50 1 6 -1 357.26 8.84 -1 6 1 347.37 14.69 1 6 -1 354.37 8.13 -1 6 1 347.80 8.50 -1 6 1 362.74 8.75 1 6 -1 359.16 15.61 -1 6 1 352.46 8.88 -1 6 1 356.51 9.00 1 6 -1 357.93 9.37 1 6 -1 356.49 8.51 -1 6 1 345.43 14.71 1 6 -1 366.11 14.45 1 6 -1 345.80 9.02 -1 6 1 355.27 8.36 1 6 0 319.94 8.94 1 6 0 322.58 8.68 1 6 0 339.71 15.54 1 6 0 322.74 8.79 1 6 0 329.50 8.23 1 6 0 318.08 8.28 1 6 0 311.07 8.81 1 6 0 317.72 12.88 -1 6 0 313.48 8.18 -1 6 0 313.94 7.87 1 6 0 325.82 14.27 -1 6 0 319.15 13.45 -1 6 0 319.08 7.94 -1 6 0 315.70 7.84 -1 6 0 324.45 8.04 -1 6 0 325.38 7.83 1 6 0 311.91 8.40 -1 6 0 321.89 7.93 1 6 0 323.00 7.81 1 6 0 308.24 7.80 -1 6 0 338.80 13.76 -1 6 0 332.28 13.51 -1 6 0 322.06 7.99 1 6 1 137.95 5.79 -1 6 -1 135.15 4.93 -1 6 -1 133.60 5.20 -1 6 -1 141.74 5.21 1 6 1 126.67 5.68 -1 6 -1 138.82 5.04 1 6 1 141.69 6.01 1 6 1 145.75 6.10 -1 6 -1 141.07 5.52 1 6 1 126.44 9.38 1 6 1 136.19 5.97 1 6 1 138.67 5.96 -1 6 -1 142.36 5.25 1 6 1 135.82 5.63 -1 6 -1 140.08 5.36 -1 6 -1 139.24 5.23 -1 6 -1 145.41 5.40 1 6 1 138.65 4.95 1 6 1 138.78 9.07 1 6 1 137.97 5.38 -1 6 -2 578.82 18.94 -1 6 -2 601.92 11.47 1 6 2 562.53 12.05 1 6 2 577.25 11.43 1 6 2 589.65 20.31 1 6 2 577.59 19.15 -1 6 -2 607.05 11.14 1 6 2 577.70 12.01 1 6 2 597.97 12.36 1 6 2 584.44 10.62 1 6 2 598.43 11.86 -1 6 -2 584.45 10.68 1 6 2 593.23 12.18 1 6 2 585.60 11.11 -1 6 -2 571.70 10.85 -1 6 -2 582.62 11.01 -1 6 -2 575.98 11.06 -1 6 -2 594.96 10.49 -1 6 -2 583.24 10.64 1 6 2 584.73 11.91 1 6 3 610.33 12.78 1 6 3 652.93 12.66 -1 6 -3 608.78 11.40 -1 6 -3 654.02 12.34 -1 6 -3 608.60 11.85 1 6 3 625.47 12.97 1 6 3 619.76 21.84 1 6 3 607.31 20.58 1 6 3 630.94 12.41 -1 6 -3 623.33 20.67 -1 6 -3 622.85 11.17 1 6 3 629.38 13.23 1 6 3 600.87 12.28 -1 6 -3 584.85 11.68 -1 6 -3 627.48 11.96 1 6 3 623.53 12.65 -1 6 -3 651.71 12.13 -1 6 -3 607.80 10.93 1 6 3 623.21 11.61 -1 6 -4 1053.97 16.13 -1 6 -4 1059.38 16.24 1 6 4 1028.59 28.76 -1 6 -4 1057.36 16.03 1 6 4 1074.13 28.29 -1 6 -4 1075.59 27.97 1 6 4 1108.08 16.65 1 6 4 1097.65 17.50 1 6 4 1053.89 17.53 1 6 4 1072.22 16.96 1 6 4 1054.07 17.06 -1 6 -4 1039.82 16.04 -1 6 -4 1073.45 14.92 1 6 4 1037.19 16.28 -1 6 -4 1032.02 15.97 1 6 4 1072.23 16.69 -1 6 -4 1105.12 15.21 -1 6 -4 1089.70 15.79 1 6 4 1061.59 15.69 -1 6 -5 367.22 9.85 -1 6 -5 348.63 16.69 1 6 5 369.06 10.07 1 6 5 375.38 10.70 -1 6 -5 370.74 9.84 1 6 5 389.01 10.52 -1 6 -5 367.96 9.11 -1 6 -5 345.59 9.72 1 6 5 358.20 9.96 1 6 5 361.34 10.56 1 6 5 358.94 17.41 1 6 5 374.92 17.35 1 6 5 371.19 10.31 -1 6 -5 360.71 9.73 -1 6 -5 359.08 9.84 -1 6 -5 346.93 9.56 1 6 5 397.86 9.95 1 6 6 275.24 8.75 -1 6 -6 262.31 8.63 1 6 6 277.55 8.86 -1 6 -6 267.58 8.37 -1 6 -6 255.10 8.31 -1 6 -6 269.96 8.58 1 6 6 272.05 8.71 -1 6 -6 271.49 8.54 1 6 6 276.32 9.17 1 6 6 269.99 8.45 -1 6 -6 272.43 8.88 1 6 6 271.96 9.25 -1 6 -6 268.47 7.81 1 6 7 23.91 2.92 -1 6 -7 22.63 3.04 -1 6 -7 20.20 3.03 1 6 7 17.44 2.77 -1 6 -7 23.38 3.02 1 6 7 24.49 2.98 -1 6 -7 26.14 3.17 -1 6 -7 21.69 3.03 1 6 7 16.04 2.94 1 6 7 20.24 2.82 -1 6 -7 27.06 3.45 1 6 7 26.25 3.13 1 6 8 196.01 6.95 1 6 8 195.98 6.71 -1 6 -8 175.30 6.44 -1 6 -8 173.98 6.83 -1 6 -8 183.88 6.80 -1 6 -8 179.07 6.98 1 6 8 169.66 6.87 -1 6 -8 181.56 6.76 1 6 8 189.90 6.78 1 6 8 183.18 6.59 -1 6 -8 182.53 6.73 1 6 9 8.47 1.82 -1 6 -9 10.30 2.15 1 6 9 11.82 1.90 1 6 9 7.40 1.97 1 6 9 7.87 1.97 -1 6 -9 9.92 2.11 -1 6 -9 10.81 2.18 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5.17 1 8 1 572.53 12.36 1 8 1 526.45 10.45 1 8 1 557.80 11.81 1 8 1 574.10 12.43 1 8 1 567.44 11.71 1 8 1 528.55 11.47 1 8 1 553.42 12.00 1 8 2 694.80 13.10 1 8 2 656.77 13.03 1 8 2 659.96 12.36 1 8 2 653.09 12.03 1 8 2 663.05 13.15 1 8 2 671.75 13.55 1 8 2 695.36 13.71 -1 8 -3 139.23 5.30 1 8 3 154.08 6.40 1 8 3 160.31 6.69 1 8 3 154.02 6.06 1 8 3 158.23 6.46 1 8 3 154.02 6.77 -1 8 -3 140.12 5.50 1 8 3 164.59 6.52 -1 8 -3 146.37 5.69 1 8 4 96.67 5.11 -1 8 -4 85.90 4.35 1 8 4 106.58 4.64 1 8 4 111.59 5.41 -1 8 -4 95.89 4.57 1 8 4 105.42 5.44 1 8 4 115.09 5.60 -1 8 -4 88.66 4.28 1 8 4 109.49 5.46 -1 8 -4 109.06 4.91 1 8 4 109.02 5.10 -1 8 -5 23.74 2.38 -1 8 -5 23.08 2.53 1 8 5 28.51 2.52 1 8 5 27.38 3.02 1 8 5 29.29 2.98 1 8 5 31.72 3.21 -1 8 -5 27.59 2.74 1 8 5 25.97 2.83 1 8 5 29.11 3.02 -1 8 -6 246.90 6.53 -1 8 -6 253.02 6.51 1 8 6 262.04 7.19 1 8 6 267.85 7.50 -1 8 -6 245.69 6.67 1 8 6 259.51 7.61 1 8 6 259.80 7.68 1 8 6 267.30 7.36 1 8 6 268.86 6.59 1 8 7 333.07 7.39 1 8 7 337.74 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317.57 7.50 2 -8 -6 31.83 2.75 -2 -8 -4 226.19 7.42 -2 -8 -5 65.25 3.72 -2 -8 -6 11.79 2.07 2 -7 -9 16.26 2.19 -2 -7 9 8.85 1.83 2 -7 -8 6.35 2.02 -2 -7 8 7.14 2.28 2 -7 -7 364.34 9.61 2 -7 -3 14.86 6.47 -2 -7 3 22.70 6.71 -2 -7 3 15.68 6.41 -2 -7 2 1726.60 45.49 2 -7 -2 1677.24 40.73 2 -7 -1 30.90 6.55 2 -7 -1 26.77 6.61 -2 -7 1 36.62 7.77 -2 -7 0 230.06 17.11 -2 -7 -1 9.26 6.65 -2 -7 -1 25.76 6.80 -2 -7 -2 486.31 22.95 -2 -7 -2 448.03 25.95 -2 -7 -4 144.87 6.98 -2 -7 -5 157.89 6.76 -2 -7 -6 67.09 4.60 -2 -7 -6 67.78 4.27 -2 -7 -7 159.33 5.82 -2 -7 -7 162.71 6.22 -2 -7 -8 43.49 3.12 -2 -7 -8 43.90 3.11 2 -6 -10 57.35 3.15 2 -6 -10 54.60 3.61 -2 -6 10 46.77 3.71 -2 -6 10 49.56 3.33 2 -6 -10 57.20 3.57 -2 -6 9 247.11 8.60 2 -6 -9 254.57 7.22 -2 -6 9 231.38 7.43 2 -6 -8 5.70 2.22 -2 -6 8 3.89 2.05 2 -6 -8 5.65 1.88 -2 -6 7 121.26 5.68 2 -6 -7 129.73 5.59 -2 -6 6 76.65 4.58 -2 -6 6 71.01 10.69 2 -6 -6 80.28 9.44 2 -6 -6 70.06 9.60 2 -6 -6 76.62 4.61 -2 -6 6 67.13 10.47 -2 -6 6 65.70 9.27 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657.06 11.49 -2 4 -3 676.80 10.82 2 4 3 653.05 15.74 2 4 3 624.96 9.45 2 4 3 673.70 11.65 -2 4 -3 669.15 11.22 -2 4 -3 685.42 11.11 -2 4 -3 667.62 11.16 2 4 3 668.13 18.66 -2 4 -3 681.96 17.39 2 4 3 660.74 10.51 -2 4 -4 14.98 2.01 2 4 4 19.52 2.36 -2 4 -4 20.33 4.10 2 4 4 16.05 2.47 -2 4 -4 12.80 2.06 2 4 4 18.64 2.26 -2 4 -4 16.32 2.33 2 4 4 15.42 2.20 -2 4 -4 14.17 2.25 2 4 4 13.99 2.24 2 4 4 25.00 4.06 -2 4 -4 14.56 4.08 2 4 4 17.19 2.57 2 4 4 16.59 3.75 2 4 4 17.06 2.53 2 4 4 19.80 3.65 2 4 4 16.42 2.12 2 4 4 14.94 2.38 -2 4 -4 18.32 2.52 2 4 4 18.49 3.99 -2 4 -4 19.18 3.74 -2 4 -4 18.72 3.77 -2 4 -4 21.25 2.79 -2 4 -4 16.15 2.19 2 4 5 721.95 21.63 -2 4 -5 720.04 12.95 -2 4 -5 738.52 12.48 -2 4 -5 719.99 12.24 -2 4 -5 723.95 12.71 2 4 5 747.79 12.77 2 4 5 750.54 21.70 2 4 5 733.11 12.94 2 4 5 723.62 13.19 -2 4 -5 733.89 22.11 2 4 5 697.23 12.42 -2 4 -5 720.85 12.98 2 4 5 711.59 12.78 2 4 5 748.09 11.94 2 4 5 730.73 13.34 -2 4 -5 728.81 12.72 2 4 5 760.92 21.61 -2 4 -5 676.27 20.32 2 4 5 710.65 20.05 -2 4 -5 698.24 21.34 -2 4 -5 730.43 13.09 2 4 5 725.45 12.61 -2 4 -6 917.05 26.05 2 4 6 994.57 26.63 -2 4 -6 958.29 15.70 -2 4 -6 981.66 15.80 2 4 6 1008.51 15.31 -2 4 -6 967.25 15.13 -2 4 -6 895.75 25.08 2 4 6 950.85 15.46 2 4 6 964.52 14.58 -2 4 -6 997.83 15.59 2 4 6 937.68 25.03 2 4 6 984.68 15.38 -2 4 -6 970.90 15.44 -2 4 -6 939.42 15.06 2 4 6 983.07 14.97 2 4 6 1001.00 25.92 2 4 6 970.81 15.94 -2 4 -6 919.84 26.06 -2 4 -6 973.24 15.83 2 4 6 1032.31 27.47 2 4 6 970.91 15.45 2 4 7 766.47 13.97 -2 4 -7 749.27 24.00 -2 4 -7 690.17 23.67 2 4 7 733.58 24.27 -2 4 -7 726.13 14.57 -2 4 -7 738.96 13.80 -2 4 -7 725.84 13.85 2 4 7 717.95 23.25 2 4 7 705.23 23.97 -2 4 -7 752.85 14.51 2 4 7 723.65 13.43 2 4 7 733.87 13.10 -2 4 -7 756.07 14.09 2 4 7 781.13 13.47 2 4 7 698.49 14.05 2 4 7 697.30 13.21 -2 4 -7 691.98 13.58 -2 4 -7 739.83 24.02 -2 4 -7 746.67 14.34 2 4 7 749.15 13.94 -2 4 -8 114.00 5.60 2 4 8 120.34 5.60 -2 4 -8 105.97 5.65 2 4 8 104.36 4.88 -2 4 -8 110.93 5.64 -2 4 -8 107.08 5.96 2 4 8 104.72 5.38 -2 4 -8 111.18 5.57 -2 4 -8 111.63 5.63 2 4 8 111.09 5.68 -2 4 -9 41.57 3.42 -2 4 -9 42.82 3.73 -2 4 -9 49.64 3.98 -2 4 -9 54.35 3.94 2 4 9 44.70 3.50 2 4 9 51.15 3.87 -2 4 -9 45.74 3.90 -2 4 -9 47.76 3.92 2 4 9 51.03 3.97 -2 4 -10 296.86 8.09 -2 4 -10 299.92 7.99 -2 4 -10 285.27 7.73 2 4 10 297.81 7.90 -2 4 -10 298.98 7.49 2 4 10 309.10 8.03 -2 4 -10 288.11 7.76 -2 4 -11 85.34 3.81 -2 4 -11 80.19 3.45 -2 4 -11 88.07 3.91 2 4 11 87.35 3.73 2 4 11 81.01 3.61 2 5 -11 28.36 2.83 2 5 -11 25.65 2.43 2 5 -11 24.90 2.42 2 5 -11 25.63 2.33 -2 5 11 32.20 2.45 2 5 -11 28.98 2.70 -2 5 11 27.86 2.36 2 5 -10 33.85 3.06 2 5 -10 29.68 3.08 -2 5 10 31.46 2.87 2 5 -10 36.79 3.27 -2 5 10 34.31 3.08 -2 5 10 27.98 2.66 -2 5 10 27.51 2.74 -2 5 10 30.45 2.84 2 5 -10 32.18 3.09 2 5 -10 25.87 3.10 -2 5 9 14.06 2.91 2 5 -9 20.12 2.56 -2 5 9 16.26 2.63 2 5 -9 17.08 2.98 -2 5 9 18.96 2.61 -2 5 9 16.31 2.44 2 5 -9 12.57 2.44 2 5 -9 12.77 2.62 2 5 -9 17.06 2.81 2 5 -9 16.98 2.84 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117.04 9.55 2 5 -5 119.59 9.63 -2 5 5 114.84 5.53 -2 5 5 117.76 9.29 -2 5 5 127.33 5.42 2 5 -5 126.42 5.58 2 5 -5 117.61 5.52 -2 5 5 127.03 5.95 -2 5 5 114.78 5.51 2 5 -5 110.37 5.59 2 5 -5 118.57 5.79 -2 5 5 115.36 5.56 2 5 -5 117.31 5.56 2 5 -5 117.79 5.46 2 5 -5 119.32 9.83 -2 5 5 120.71 5.43 -2 5 4 5.65 2.15 -2 5 4 7.50 1.94 2 5 -4 3.02 1.79 -2 5 4 7.61 3.50 2 5 -4 5.77 2.00 -2 5 4 6.34 3.34 2 5 -4 3.66 3.68 -2 5 4 11.29 2.21 -2 5 4 4.33 1.74 -2 5 4 5.41 1.87 2 5 -4 2.50 1.72 -2 5 4 4.82 2.01 2 5 -4 5.54 2.03 -2 5 4 6.45 1.84 2 5 -4 3.45 1.55 -2 5 4 5.32 1.55 2 5 -4 3.73 1.76 2 5 -4 -2.09 3.57 2 5 -4 3.46 1.74 2 5 -4 5.71 1.80 -2 5 3 271.07 7.26 -2 5 3 273.16 10.98 -2 5 3 262.43 6.36 2 5 -3 258.90 7.83 -2 5 3 258.45 12.39 -2 5 3 271.00 7.60 2 5 -3 265.38 7.08 -2 5 3 263.97 7.52 2 5 -3 265.65 10.99 2 5 -3 261.70 13.07 2 5 -3 266.01 7.61 -2 5 3 261.44 7.06 2 5 -3 261.03 6.52 2 5 -3 257.96 7.15 -2 5 3 243.45 7.61 2 5 -3 265.30 7.93 2 5 -3 280.42 7.78 2 5 -3 259.19 7.53 2 5 -3 260.60 7.28 -2 5 3 254.50 6.65 -2 5 3 268.24 12.96 2 5 -3 254.36 13.14 -2 5 3 256.90 7.59 -2 5 3 259.89 7.29 2 5 -2 371.18 9.17 -2 5 2 384.25 13.22 -2 5 2 392.16 7.70 -2 5 2 387.96 8.26 -2 5 2 366.66 14.49 -2 5 2 389.04 8.81 -2 5 2 394.77 14.74 2 5 -2 371.07 8.73 2 5 -2 379.80 9.08 2 5 -2 385.93 8.09 -2 5 2 382.34 8.73 2 5 -2 383.97 8.77 2 5 -2 377.13 8.35 -2 5 2 372.98 11.58 2 5 -2 386.19 15.50 2 5 -2 364.94 13.30 2 5 -2 411.25 8.05 -2 5 2 383.30 8.75 2 5 -2 379.29 9.19 -2 5 2 372.86 8.21 2 5 -2 372.88 8.59 2 5 -2 358.23 14.93 -2 5 2 374.16 8.76 -2 5 2 368.23 8.40 -2 5 1 54.84 4.77 -2 5 1 47.51 2.89 -2 5 1 45.09 4.96 -2 5 1 46.85 2.87 -2 5 1 44.53 5.09 -2 5 1 46.92 4.84 -2 5 1 43.19 2.72 2 5 -1 51.57 3.71 2 5 -1 50.78 4.54 2 5 -1 45.20 2.86 -2 5 1 49.96 3.25 2 5 -1 51.06 3.18 2 5 -1 54.43 6.35 2 5 -1 40.74 5.07 2 5 -1 47.30 3.03 -2 5 1 43.78 3.10 2 5 -1 46.04 3.39 2 5 -1 49.69 3.57 2 5 -1 45.57 3.40 -2 5 1 46.84 3.32 2 5 -1 49.53 3.52 -2 5 1 51.18 3.23 -2 5 1 47.72 3.18 -2 5 1 42.12 3.98 -2 5 1 48.42 5.73 -2 5 1 42.87 2.99 2 5 -1 50.02 3.33 -2 5 0 177.60 8.85 2 5 0 172.26 6.19 -2 5 0 168.43 9.32 -2 5 0 180.12 5.57 2 5 0 168.68 8.81 -2 5 0 178.71 9.06 2 5 0 187.24 6.57 -2 5 0 183.42 5.57 2 5 0 178.51 5.49 -2 5 0 180.11 5.72 2 5 0 184.33 10.77 2 5 0 170.58 6.18 2 5 0 175.35 5.88 -2 5 0 185.42 5.60 -2 5 0 188.64 10.17 -2 5 0 190.82 5.91 -2 5 0 184.20 5.51 2 5 0 178.94 6.16 2 5 0 177.53 6.15 2 5 0 165.52 9.55 2 5 0 178.66 5.81 2 5 0 182.78 5.75 -2 5 0 186.23 5.33 -2 5 0 181.08 5.57 -2 5 0 190.29 8.76 -2 5 0 178.20 5.66 -2 5 -1 112.61 7.74 -2 5 -1 111.96 7.59 -2 5 -1 115.41 4.65 2 5 1 117.62 5.11 2 5 1 115.44 7.58 -2 5 -1 128.25 8.75 2 5 1 111.01 8.20 2 5 1 107.59 5.07 2 5 1 114.22 5.06 2 5 1 99.06 8.21 2 5 1 101.33 4.47 -2 5 -1 121.36 7.32 2 5 1 109.18 5.09 -2 5 -1 108.43 4.37 -2 5 -1 103.73 4.20 2 5 1 110.87 5.01 2 5 1 111.36 4.78 -2 5 -1 111.75 4.57 -2 5 -1 106.53 4.23 2 5 1 117.25 4.66 -2 5 -1 114.43 7.47 -2 5 -1 107.28 4.61 -2 5 -1 112.07 4.44 2 5 1 107.31 5.16 2 5 1 102.82 4.06 -2 5 -1 119.74 4.69 -2 5 -2 676.28 10.97 -2 5 -2 712.23 20.72 2 5 2 707.16 11.82 -2 5 -2 643.95 18.89 2 5 2 704.89 19.80 -2 5 -2 676.12 11.37 2 5 2 665.13 20.32 -2 5 -2 679.99 19.30 -2 5 -2 642.03 10.71 -2 5 -2 670.51 11.47 2 5 2 683.46 12.44 2 5 2 665.40 11.51 2 5 2 704.50 12.17 2 5 2 668.83 12.41 2 5 2 659.39 10.52 2 5 2 676.36 11.82 -2 5 -2 661.61 11.28 2 5 2 676.28 12.52 -2 5 -2 690.21 11.19 -2 5 -2 692.86 19.19 2 5 2 679.04 12.35 -2 5 -2 700.30 18.18 -2 5 -2 681.38 11.61 -2 5 -3 828.71 22.39 -2 5 -3 767.44 22.01 2 5 3 812.94 22.53 -2 5 -3 810.62 13.05 -2 5 -3 770.81 12.45 2 5 3 816.09 14.20 2 5 3 820.19 13.40 2 5 3 840.67 13.93 2 5 3 835.87 13.52 2 5 3 829.06 13.99 -2 5 -3 798.82 12.35 2 5 3 799.37 13.96 -2 5 -3 774.04 12.64 2 5 3 812.88 23.18 2 5 3 789.10 13.98 -2 5 -3 826.11 21.02 -2 5 -3 820.30 22.08 -2 5 -3 822.01 13.14 -2 5 -3 810.74 13.36 2 5 3 804.07 12.52 -2 5 -3 802.05 13.00 -2 5 -4 414.49 16.89 2 5 4 420.54 10.10 2 5 4 411.96 17.09 -2 5 -4 429.70 10.12 2 5 4 401.77 14.65 2 5 4 426.17 10.59 -2 5 -4 424.13 10.01 2 5 4 413.25 10.17 -2 5 -4 444.68 9.85 -2 5 -4 412.65 10.00 2 5 4 437.40 10.55 2 5 4 442.86 10.23 2 5 4 424.16 10.62 2 5 4 454.70 17.96 2 5 4 402.50 10.38 -2 5 -4 420.05 9.89 -2 5 -4 446.58 16.57 -2 5 -4 435.01 17.30 -2 5 -4 406.21 9.79 2 5 4 423.45 9.64 -2 5 -4 415.53 9.50 2 5 5 160.93 6.88 -2 5 -5 157.09 11.19 2 5 5 151.70 11.05 -2 5 -5 156.49 6.64 -2 5 -5 153.07 6.59 2 5 5 169.54 11.78 -2 5 -5 149.35 6.14 2 5 5 141.94 6.41 -2 5 -5 148.32 6.32 2 5 5 155.20 9.99 2 5 5 158.16 6.42 -2 5 -5 160.75 6.41 2 5 5 156.20 6.72 -2 5 -5 156.89 6.34 2 5 5 151.59 6.82 2 5 5 144.51 6.22 -2 5 -5 168.94 10.89 -2 5 -5 150.04 6.30 -2 5 -5 151.22 11.09 2 5 5 146.53 6.12 -2 5 -6 1099.07 29.91 2 5 6 1134.16 30.50 -2 5 -6 1081.95 16.44 2 5 6 1136.73 17.66 2 5 6 1097.44 27.48 2 5 6 1130.05 17.20 -2 5 -6 1129.43 17.06 -2 5 -6 1111.91 17.44 2 5 6 1111.71 17.50 2 5 6 1080.60 29.51 -2 5 -6 1153.35 17.68 2 5 6 1137.71 17.91 -2 5 -6 1074.15 16.84 -2 5 -6 1025.27 28.11 -2 5 -6 1103.35 30.24 2 5 6 1129.08 16.93 -2 5 -6 1148.46 17.33 2 5 6 1111.57 16.81 2 5 7 36.39 3.30 -2 5 -7 33.39 3.56 2 5 7 36.99 3.66 -2 5 -7 28.15 3.32 -2 5 -7 33.47 3.31 2 5 7 34.44 3.57 2 5 7 33.60 3.35 -2 5 -7 24.46 3.16 -2 5 -7 38.49 3.75 2 5 7 25.96 3.03 2 5 7 28.90 3.00 -2 5 -7 35.40 3.61 2 5 7 31.79 2.95 -2 5 -7 32.44 3.48 -2 5 -8 151.46 6.36 2 5 8 156.87 6.26 -2 5 -8 150.02 6.64 2 5 8 141.75 5.76 -2 5 -8 154.98 6.21 2 5 8 158.26 6.37 2 5 8 141.72 5.69 -2 5 -8 154.28 6.61 2 5 8 147.34 5.68 -2 5 -8 148.89 6.39 -2 5 -8 152.02 6.41 2 5 8 139.12 5.95 -2 5 -9 189.25 6.61 -2 5 -9 193.91 6.60 -2 5 -9 187.99 6.70 -2 5 -9 180.11 6.28 -2 5 -9 177.73 6.75 2 5 9 198.44 6.42 -2 5 -9 192.01 6.77 2 5 9 193.02 6.53 -2 5 -10 102.12 4.37 2 5 10 86.09 3.65 -2 5 -10 87.16 3.83 -2 5 -10 96.23 4.08 -2 5 -10 94.26 4.12 -2 5 -10 85.93 4.10 2 5 10 88.25 4.04 2 6 -10 56.25 3.54 2 6 -10 53.13 3.34 -2 6 10 46.75 3.14 2 6 -10 49.52 3.24 -2 6 10 55.31 3.21 2 6 -10 49.59 3.47 -2 6 10 47.98 2.93 2 6 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6 -3 433.74 10.05 -2 6 3 430.27 10.49 2 6 -3 414.23 18.01 -2 6 3 423.95 10.41 -2 6 3 453.74 9.65 2 6 -3 449.38 10.69 -2 6 3 434.66 10.12 -2 6 2 978.30 14.88 2 6 -2 1015.85 15.86 2 6 -2 989.72 14.24 2 6 -2 990.33 14.28 -2 6 2 993.02 26.10 2 6 -2 1004.10 15.77 2 6 -2 1007.36 15.37 2 6 -2 994.10 24.44 -2 6 2 1027.02 14.53 2 6 -2 975.25 15.22 -2 6 2 1034.98 26.47 -2 6 2 997.23 15.30 2 6 -2 977.93 27.33 2 6 -2 987.15 13.50 -2 6 2 976.88 15.26 2 6 -2 1026.37 16.24 -2 6 2 989.10 15.25 -2 6 2 997.50 14.21 2 6 -2 1000.46 16.38 -2 6 2 979.16 15.41 2 6 -1 246.97 7.13 -2 6 1 263.68 6.86 -2 6 1 256.50 12.07 2 6 -1 264.48 8.36 -2 6 1 251.97 7.64 2 6 -1 254.80 7.57 2 6 -1 261.18 7.76 -2 6 1 250.96 7.54 -2 6 1 265.31 7.08 2 6 -1 246.66 7.83 -2 6 1 264.83 7.73 2 6 -1 279.26 14.70 2 6 -1 255.02 8.07 -2 6 1 256.86 13.33 -2 6 1 247.14 7.49 2 6 -1 257.91 8.29 2 6 -1 258.74 12.91 2 6 -1 265.21 8.20 -2 6 1 263.31 7.40 -2 6 1 263.26 12.98 -2 6 1 252.92 7.48 2 6 0 363.59 9.25 -2 6 0 370.84 8.30 -2 6 0 380.31 8.52 -2 6 0 383.06 9.04 2 6 0 381.69 8.54 -2 6 0 372.85 14.09 2 6 0 378.11 14.31 2 6 0 368.65 9.64 -2 6 0 383.17 8.77 -2 6 0 361.31 15.01 2 6 0 395.99 10.00 2 6 0 373.12 16.09 2 6 0 367.97 16.88 2 6 0 365.01 9.00 -2 6 0 367.60 8.59 -2 6 0 396.11 16.03 2 6 0 381.56 10.05 2 6 0 390.35 10.14 2 6 0 387.59 8.96 -2 6 0 388.37 8.83 2 6 0 391.31 10.21 -2 6 0 385.20 9.04 -2 6 -1 182.81 6.20 2 6 1 172.11 6.15 -2 6 -1 168.74 10.14 -2 6 -1 169.39 10.90 -2 6 -1 180.46 6.15 -2 6 -1 179.63 6.01 2 6 1 168.01 6.86 -2 6 -1 170.93 10.31 2 6 1 168.83 6.64 2 6 1 162.08 6.73 -2 6 -1 180.78 6.04 2 6 1 171.54 6.54 -2 6 -1 174.36 5.89 2 6 1 176.80 6.94 -2 6 -1 182.74 6.19 2 6 1 155.49 11.03 2 6 1 164.76 6.40 2 6 1 177.83 6.99 2 6 1 161.75 10.17 -2 6 -1 164.91 5.66 -2 6 -1 150.42 9.96 -2 6 -2 924.56 24.44 2 6 2 925.60 14.70 -2 6 -2 968.40 14.46 2 6 2 907.76 13.11 2 6 2 928.49 15.83 2 6 2 923.25 15.12 -2 6 -2 955.37 13.79 2 6 2 984.34 14.92 2 6 2 935.78 15.31 2 6 2 959.84 16.39 -2 6 -2 976.62 14.17 -2 6 -2 972.27 14.47 -2 6 -2 942.24 14.39 2 6 2 947.26 16.16 2 6 2 955.57 26.69 2 6 2 954.22 16.11 -2 6 -2 886.21 23.75 2 6 2 898.77 24.64 -2 6 -2 934.12 14.20 2 6 3 100.94 5.60 2 6 3 105.85 5.53 -2 6 -3 101.96 4.98 -2 6 -3 99.90 8.97 -2 6 -3 98.28 5.13 2 6 3 108.39 5.83 2 6 3 107.94 5.48 2 6 3 97.23 8.94 -2 6 -3 109.61 5.25 2 6 3 108.57 5.89 2 6 3 115.27 10.01 2 6 3 102.93 5.65 -2 6 -3 102.60 4.99 -2 6 -3 99.78 8.69 -2 6 -3 104.12 5.08 -2 6 -3 101.50 5.24 2 6 3 95.39 4.70 2 6 4 511.40 12.41 -2 6 -4 493.05 19.79 -2 6 -4 495.10 11.32 2 6 4 503.37 12.00 -2 6 -4 498.34 10.50 -2 6 -4 508.17 11.02 2 6 4 506.24 11.73 -2 6 -4 502.55 11.33 2 6 4 486.32 12.12 2 6 4 518.87 20.24 -2 6 -4 510.33 11.37 2 6 4 533.20 21.08 2 6 4 515.33 12.32 -2 6 -4 504.24 11.24 -2 6 -4 466.72 18.39 -2 6 -4 492.99 19.36 -2 6 -4 517.10 11.12 2 6 4 511.77 11.79 2 6 4 501.32 10.77 -2 6 -5 65.78 4.52 -2 6 -5 72.80 4.22 -2 6 -5 78.41 4.83 -2 6 -5 74.14 4.80 2 6 5 68.75 4.63 2 6 5 70.47 4.92 2 6 5 72.16 5.00 2 6 5 79.51 8.72 2 6 5 67.62 4.60 2 6 5 77.92 8.88 2 6 5 78.57 5.23 2 6 5 68.93 4.61 -2 6 -5 72.31 4.62 -2 6 -5 58.00 7.73 -2 6 -5 70.21 4.56 -2 6 -5 68.35 4.48 2 6 5 84.35 4.75 2 6 6 555.96 12.88 -2 6 -6 557.48 12.29 -2 6 -6 547.74 12.32 -2 6 -6 570.40 11.52 -2 6 -6 544.34 11.89 2 6 6 576.84 12.64 2 6 6 552.37 12.17 2 6 6 542.11 12.58 2 6 6 555.26 12.19 -2 6 -6 557.19 12.09 -2 6 -6 561.45 12.13 -2 6 -6 551.98 11.68 2 6 6 573.00 11.85 -2 6 -7 148.92 6.49 2 6 7 162.53 6.84 -2 6 -7 151.21 5.93 -2 6 -7 161.93 6.37 2 6 7 163.52 6.60 -2 6 -7 161.67 6.50 2 6 7 157.46 6.35 2 6 7 165.24 6.73 2 6 7 165.10 6.43 -2 6 -7 154.44 6.52 -2 6 -7 158.42 6.54 2 6 7 169.91 6.47 -2 6 -8 49.72 3.50 -2 6 -8 44.33 3.74 -2 6 -8 51.69 3.73 2 6 8 52.55 3.65 2 6 8 48.69 3.38 -2 6 -8 54.09 3.73 -2 6 -8 42.20 3.69 2 6 8 50.39 3.63 2 6 8 51.85 3.45 -2 6 -8 52.46 3.63 2 6 8 51.51 3.55 -2 6 -9 117.07 4.89 -2 6 -9 136.19 4.96 2 6 9 121.35 4.60 -2 6 -9 128.96 4.85 -2 6 -9 129.74 4.91 2 6 9 132.58 4.86 -2 7 9 11.41 1.90 2 7 -9 12.45 2.11 2 7 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10.52 -2 7 4 452.24 11.42 2 7 -4 436.69 11.14 2 7 -4 438.13 11.28 2 7 -4 435.48 9.90 -2 7 4 466.15 11.51 -2 7 4 439.97 11.24 2 7 -4 452.03 11.16 -2 7 4 439.18 11.22 -2 7 4 465.67 10.96 -2 7 3 16.18 2.65 -2 7 3 15.26 4.66 2 7 -3 17.30 2.97 2 7 -3 14.74 2.84 -2 7 3 19.03 2.91 -2 7 3 18.80 2.61 -2 7 3 17.79 2.67 -2 7 3 10.09 4.27 2 7 -3 14.79 2.63 -2 7 3 14.34 2.73 2 7 -3 16.44 2.35 2 7 -3 9.36 4.51 -2 7 3 14.76 2.61 2 7 -3 18.24 2.97 2 7 -3 13.25 2.51 2 7 -3 16.10 2.42 2 7 -2 1802.51 19.58 -2 7 2 1839.30 21.60 2 7 -2 1789.23 22.09 2 7 -2 1843.94 21.13 2 7 -2 1892.92 23.01 -2 7 2 1783.89 36.66 -2 7 2 1840.60 21.68 -2 7 2 1833.45 20.03 -2 7 2 1808.38 21.55 2 7 -2 1778.63 39.10 2 7 -2 1804.93 21.59 -2 7 2 1846.99 21.64 2 7 -2 1803.60 22.73 2 7 -2 1843.73 23.14 -2 7 2 1866.41 20.99 2 7 -1 32.38 3.54 -2 7 1 35.54 3.34 2 7 -1 34.75 3.62 2 7 -1 31.57 3.11 -2 7 1 33.36 3.31 2 7 -1 36.01 3.93 2 7 -1 25.20 5.36 2 7 -1 36.32 3.67 -2 7 1 34.32 3.25 2 7 -1 32.54 3.11 2 7 -1 32.90 3.68 2 7 -1 31.89 6.00 -2 7 1 36.69 3.30 2 7 -1 33.82 3.29 -2 7 1 37.37 3.33 -2 7 0 220.92 7.08 2 7 0 211.44 7.88 2 7 0 220.37 8.12 -2 7 0 203.60 6.79 2 7 0 210.46 7.41 2 7 0 195.90 7.58 2 7 0 206.25 7.91 2 7 0 199.45 12.64 2 7 0 210.06 7.20 -2 7 0 220.32 6.70 2 7 0 221.49 8.10 -2 7 0 219.76 6.94 -2 7 -1 22.71 2.50 2 7 1 22.25 3.38 2 7 1 22.48 3.14 2 7 1 25.13 2.79 2 7 1 26.46 3.19 2 7 1 23.21 3.30 2 7 1 23.44 3.28 2 7 1 23.17 2.96 2 7 1 21.51 3.00 -2 7 -1 22.92 2.52 2 7 1 13.26 4.76 -2 7 -2 484.07 10.17 2 7 2 513.97 11.19 2 7 2 455.87 20.10 2 7 2 500.45 11.82 2 7 2 458.41 18.79 -2 7 -2 485.95 10.17 2 7 2 497.57 12.22 2 7 2 509.93 12.46 2 7 2 492.88 11.40 2 7 2 483.65 12.00 -2 7 -2 476.65 10.25 2 7 2 492.74 11.98 -2 7 -2 478.81 10.41 -2 7 -2 498.40 10.23 -2 7 -3 398.70 9.48 2 7 3 391.25 10.46 -2 7 -3 374.80 9.51 -2 7 -3 381.77 9.54 2 7 3 395.48 11.03 2 7 3 396.87 10.45 2 7 3 397.31 10.89 2 7 3 385.95 11.10 2 7 3 374.37 10.42 -2 7 -3 397.38 9.50 2 7 3 389.62 10.07 -2 7 -3 381.43 9.20 -2 7 -3 408.81 9.31 2 7 3 383.35 8.88 -2 7 -4 154.55 6.25 -2 7 -4 140.39 6.11 -2 7 -4 161.77 6.23 2 7 4 148.69 6.48 2 7 4 152.72 6.67 2 7 4 161.06 7.03 -2 7 -4 151.19 6.29 2 7 4 156.90 6.99 2 7 4 158.39 6.84 2 7 4 145.87 6.91 -2 7 -4 155.49 5.94 -2 7 -4 144.86 5.72 2 7 4 162.60 5.96 -2 7 -5 146.66 6.18 -2 7 -5 158.94 6.43 2 7 5 161.12 6.54 2 7 5 161.64 5.96 2 7 5 158.25 6.70 -2 7 -5 149.79 6.22 -2 7 -5 153.09 5.84 -2 7 -5 147.81 6.03 2 7 5 151.03 6.91 2 7 5 154.52 6.54 2 7 5 158.63 6.91 2 7 5 158.88 6.78 -2 7 -5 150.73 5.71 -2 7 -6 75.48 4.18 -2 7 -6 83.49 4.57 2 7 6 69.49 4.41 2 7 6 75.43 4.68 2 7 6 74.93 4.60 -2 7 -6 72.47 4.29 -2 7 -6 68.53 4.23 -2 7 -6 68.14 4.29 2 7 6 71.87 4.41 2 7 6 77.37 4.84 2 7 6 75.98 4.15 2 7 7 165.97 6.27 -2 7 -7 154.51 5.87 -2 7 -7 155.95 5.68 2 7 7 159.58 5.92 2 7 7 171.23 5.69 2 7 7 158.51 5.92 -2 7 -7 154.80 5.68 2 7 7 149.17 5.89 -2 7 -7 165.64 5.53 2 7 7 160.39 5.81 -2 7 -7 160.02 5.79 -2 7 -8 48.58 2.94 2 7 8 51.28 3.19 -2 7 -8 46.42 3.06 2 7 8 46.40 2.73 -2 7 -8 52.47 3.12 2 7 8 43.34 2.89 2 7 8 49.29 2.94 -2 7 -8 47.87 3.01 2 7 8 48.96 2.96 -2 8 7 307.59 7.92 -2 8 7 275.43 7.15 -2 8 7 309.49 7.84 2 8 -7 303.62 7.05 2 8 -7 295.94 7.00 -2 8 7 315.39 7.82 2 8 -7 281.02 7.40 2 8 -7 325.16 7.53 2 8 -7 313.03 7.70 -2 8 7 337.12 7.56 2 8 -6 26.93 3.01 2 8 -6 31.47 2.99 -2 8 6 29.99 3.06 -2 8 6 42.59 3.30 2 8 -6 31.75 2.70 -2 8 6 33.27 3.13 -2 8 6 38.01 3.24 2 8 -6 30.00 2.96 2 8 -6 31.70 3.08 -2 8 6 32.51 2.91 2 8 -5 172.53 6.71 2 8 -5 174.70 5.99 -2 8 5 191.84 6.87 -2 8 5 188.71 6.80 2 8 -5 177.30 5.94 -2 8 5 196.00 7.01 2 8 -5 183.48 6.83 -2 8 5 183.39 6.97 2 8 -5 182.61 6.63 2 8 -5 196.70 6.72 -2 8 5 193.01 6.52 2 8 -4 185.73 7.11 2 8 -4 184.37 6.69 -2 8 4 184.89 7.02 2 8 -4 171.65 5.92 2 8 -4 195.54 7.01 -2 8 4 185.29 6.99 2 8 -4 179.50 6.52 -2 8 4 191.72 6.40 2 8 -4 179.36 6.88 -2 8 4 184.88 6.81 -2 8 4 199.99 6.71 -2 8 4 191.73 7.00 -2 8 3 657.87 12.70 -2 8 3 621.49 11.31 2 8 -3 628.73 12.64 2 8 -3 624.30 12.24 2 8 -3 628.19 11.90 2 8 -3 627.34 11.61 -2 8 3 647.35 12.41 2 8 -3 644.00 12.93 -2 8 3 650.91 12.55 2 8 -3 646.40 12.95 -2 8 3 638.32 12.39 -2 8 3 637.68 11.90 2 8 -2 137.15 6.27 2 8 -2 151.04 6.60 2 8 -2 160.07 6.59 2 8 -2 155.49 6.08 -2 8 2 151.74 5.98 -2 8 2 146.46 6.08 -2 8 2 161.88 6.20 2 8 -2 149.43 6.62 -2 8 2 154.81 6.18 2 8 -2 138.01 5.75 -2 8 2 154.96 5.81 -2 8 1 203.28 6.49 2 8 -1 209.26 7.64 -2 8 1 200.22 6.69 2 8 -1 187.12 7.04 2 8 -1 211.02 6.81 2 8 -1 209.04 7.55 2 8 -1 213.88 7.48 -2 8 1 202.29 6.73 -2 8 1 195.61 6.57 2 8 -1 201.22 7.59 2 8 0 748.57 12.82 2 8 0 766.56 13.30 2 8 0 762.70 14.32 2 8 0 737.71 14.18 2 8 0 752.33 14.04 2 8 0 715.70 12.57 2 8 0 739.94 13.98 2 8 1 123.29 5.95 2 8 1 116.11 5.82 2 8 1 119.11 5.65 2 8 1 114.90 5.88 2 8 1 116.49 5.34 2 8 1 118.61 5.91 2 8 2 38.78 3.61 2 8 2 40.13 3.22 2 8 2 44.02 3.74 2 8 2 41.71 3.87 2 8 2 41.08 3.79 2 8 2 40.76 3.64 2 8 2 41.93 3.84 2 8 3 549.51 11.77 2 8 3 539.53 10.82 2 8 3 575.43 12.29 -2 8 -3 473.41 9.29 -2 8 -3 488.52 9.40 2 8 3 564.67 12.19 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6.90 -4 4 -9 43.22 3.02 -4 4 -9 45.44 3.20 4 4 9 40.12 2.83 -4 4 -9 45.57 3.07 4 4 9 46.42 3.16 -4 4 -9 49.77 3.34 4 4 9 49.73 3.37 4 5 -11 31.37 2.60 4 5 -11 29.01 2.61 -4 5 11 34.66 2.62 4 5 -10 32.86 3.02 4 5 -10 30.72 2.85 -4 5 10 33.37 2.82 4 5 -10 38.22 3.11 -4 5 10 29.35 2.74 4 5 -10 33.54 3.19 4 5 -10 28.68 2.65 -4 5 10 31.34 2.81 -4 5 10 35.06 2.75 4 5 -9 106.39 5.58 4 5 -9 121.22 5.44 -4 5 9 122.71 5.45 4 5 -9 124.34 5.67 -4 5 9 111.40 5.83 -4 5 9 120.39 5.70 4 5 -9 114.94 5.53 -4 5 9 121.72 5.48 4 5 -9 106.73 5.69 -4 5 9 127.15 5.49 -4 5 8 229.05 6.76 4 5 -8 215.71 7.94 4 5 -8 216.78 7.60 -4 5 8 218.15 7.71 4 5 -8 223.27 7.89 -4 5 8 221.62 8.20 4 5 -8 221.00 8.08 4 5 -8 214.20 6.80 -4 5 8 212.15 7.84 4 5 -8 214.29 8.02 4 5 -8 199.02 7.46 -4 5 8 217.61 7.67 -4 5 8 229.67 7.80 -4 5 7 103.71 4.80 -4 5 7 97.54 5.63 4 5 -7 79.68 5.21 4 5 -7 93.68 5.44 -4 5 7 91.15 5.38 4 5 -7 87.31 5.22 -4 5 7 82.83 9.03 4 5 -7 86.00 5.29 4 5 -7 82.87 9.41 4 5 -7 92.17 4.81 -4 5 7 90.28 5.73 -4 5 7 95.34 5.69 4 5 -7 82.94 5.41 4 5 -7 91.55 5.51 -4 5 7 95.64 5.31 4 5 -7 87.77 9.58 -4 5 7 92.70 5.24 -4 5 6 455.83 10.10 4 5 -6 451.97 11.65 4 5 -6 446.01 11.03 -4 5 6 456.96 11.35 4 5 -6 458.70 11.56 -4 5 6 442.37 19.73 -4 5 6 439.38 11.73 4 5 -6 455.04 11.25 4 5 -6 459.78 10.56 4 5 -6 454.38 19.80 -4 5 6 448.27 11.78 -4 5 6 433.99 11.36 4 5 -6 457.04 11.59 4 5 -6 447.60 11.27 -4 5 6 478.28 11.28 4 5 -6 454.58 20.12 -4 5 6 465.21 11.10 -4 5 5 2155.78 38.26 -4 5 5 2203.63 21.89 4 5 -5 2114.07 24.34 4 5 -5 2151.93 23.66 -4 5 5 2168.37 24.31 4 5 -5 2127.42 24.19 -4 5 5 2263.30 42.68 -4 5 5 2143.26 24.71 4 5 -5 2107.03 23.69 4 5 -5 2130.35 23.05 4 5 -5 2235.43 43.65 -4 5 5 2113.88 24.58 -4 5 5 2148.66 24.37 4 5 -5 2144.16 24.52 4 5 -5 2185.33 24.20 -4 5 5 2132.96 23.35 -4 5 5 2218.64 23.76 -4 5 4 1717.36 34.25 -4 5 4 1741.76 19.47 4 5 -4 1797.45 19.14 4 5 -4 1738.55 21.72 4 5 -4 1822.56 21.54 -4 5 4 1766.52 21.79 4 5 -4 1787.21 21.68 -4 5 4 1767.17 36.90 -4 5 4 1757.47 21.68 4 5 -4 1771.83 20.95 4 5 -4 1799.81 21.17 4 5 -4 1715.21 37.31 -4 5 4 1726.06 21.29 4 5 -4 1696.90 32.13 -4 5 4 1728.94 21.45 4 5 -4 1716.30 21.38 4 5 -4 1734.35 21.39 -4 5 4 1676.87 20.43 -4 5 4 1737.87 20.71 -4 5 3 635.03 21.06 -4 5 3 641.34 11.82 -4 5 3 640.62 10.84 -4 5 3 648.54 18.68 4 5 -3 613.52 12.86 -4 5 3 618.17 12.56 4 5 -3 643.48 11.75 -4 5 3 653.65 22.17 -4 5 3 624.25 12.65 4 5 -3 639.93 12.62 4 5 -3 638.66 12.87 4 5 -3 637.58 22.06 -4 5 3 628.02 12.15 4 5 -3 610.79 19.53 4 5 -3 632.45 11.09 -4 5 3 641.99 12.67 4 5 -3 628.17 12.73 4 5 -3 646.84 12.90 4 5 -3 632.41 12.77 -4 5 3 646.34 12.38 -4 5 3 632.28 12.34 -4 5 2 1196.56 28.66 -4 5 2 1172.61 15.89 -4 5 2 1135.74 14.83 4 5 -2 1150.68 17.02 -4 5 2 1150.94 25.59 4 5 -2 1139.60 17.14 -4 5 2 1110.56 16.73 4 5 -2 1152.45 16.09 4 5 -2 1135.19 16.93 -4 5 2 1119.16 16.20 -4 5 2 1153.91 29.01 4 5 -2 1154.33 16.75 -4 5 2 1111.57 15.32 4 5 -2 1099.79 28.77 4 5 -2 1097.82 26.91 4 5 -2 1118.53 15.19 -4 5 2 1128.53 16.37 4 5 -2 1159.55 16.93 4 5 -2 1113.97 16.53 -4 5 2 1150.01 16.39 -4 5 2 1115.32 16.21 -4 5 1 348.70 13.81 -4 5 1 364.93 8.06 -4 5 1 367.36 16.04 -4 5 1 372.08 9.09 -4 5 1 380.66 8.89 -4 5 1 358.67 14.68 4 5 -1 357.67 9.84 4 5 -1 359.77 9.73 4 5 -1 369.55 8.13 -4 5 1 377.73 9.64 4 5 -1 376.31 9.45 -4 5 1 378.85 9.06 -4 5 1 347.09 16.08 4 5 -1 356.15 9.58 4 5 -1 374.66 16.65 4 5 -1 357.73 15.78 4 5 -1 391.53 9.29 -4 5 1 364.70 9.07 4 5 -1 361.89 9.64 4 5 -1 368.33 9.44 -4 5 1 362.09 9.39 -4 5 1 360.02 9.31 -4 5 0 51.16 3.72 -4 5 0 52.49 5.96 -4 5 0 53.54 6.74 4 5 0 53.26 5.64 -4 5 0 53.47 3.79 -4 5 0 48.90 3.59 -4 5 0 49.32 3.46 4 5 0 50.79 3.99 -4 5 0 45.89 6.09 4 5 0 50.62 3.97 4 5 0 51.52 3.51 4 5 0 53.84 3.85 4 5 0 51.72 3.95 -4 5 0 52.72 3.39 4 5 0 52.43 4.10 4 5 0 53.94 6.81 4 5 0 52.90 6.81 4 5 0 55.26 3.79 -4 5 0 53.21 3.54 4 5 0 50.53 3.91 -4 5 0 46.47 5.52 -4 5 0 53.89 3.91 -4 5 -1 633.13 12.30 -4 5 -1 600.26 19.94 4 5 1 654.80 20.07 -4 5 -1 644.33 12.45 -4 5 -1 665.55 22.53 -4 5 -1 648.49 21.24 4 5 1 663.24 12.95 4 5 1 632.35 13.12 4 5 1 640.87 11.89 4 5 1 641.56 12.71 4 5 1 630.20 12.71 -4 5 -1 628.90 12.24 -4 5 -1 624.11 11.63 4 5 1 620.45 12.76 4 5 1 636.37 12.45 4 5 1 652.58 22.12 4 5 1 625.06 12.77 -4 5 -1 633.79 12.15 -4 5 -1 655.77 11.08 -4 5 -1 591.66 18.96 -4 5 -1 656.51 12.78 -4 5 -2 90.14 4.84 -4 5 -2 88.64 4.77 -4 5 -2 88.58 8.51 4 5 2 81.40 7.95 -4 5 -2 84.47 4.90 -4 5 -2 79.94 8.18 4 5 2 82.85 5.08 4 5 2 81.44 4.70 4 5 2 86.98 4.98 4 5 2 86.24 4.91 -4 5 -2 90.71 4.96 4 5 2 82.26 4.79 4 5 2 89.67 8.75 -4 5 -2 94.08 9.72 4 5 2 93.36 5.00 4 5 2 83.87 4.96 -4 5 -2 87.53 4.53 -4 5 -2 83.51 4.44 -4 5 -2 88.21 8.16 -4 5 -2 82.56 4.97 4 5 2 90.50 4.20 -4 5 -3 553.83 11.54 -4 5 -3 545.27 20.53 4 5 3 544.25 20.33 -4 5 -3 562.59 12.09 -4 5 -3 542.24 11.95 -4 5 -3 525.87 20.52 -4 5 -3 555.79 10.62 4 5 3 534.28 11.84 4 5 3 558.59 12.24 4 5 3 546.17 12.04 4 5 3 579.39 12.77 -4 5 -3 553.14 11.71 4 5 3 534.59 11.96 4 5 3 522.09 20.59 4 5 3 569.06 12.19 4 5 3 529.37 10.19 4 5 3 521.65 12.11 -4 5 -3 539.38 22.11 -4 5 -3 580.35 11.61 -4 5 -3 543.72 20.03 -4 5 -3 530.42 12.20 4 5 3 544.95 10.85 -4 5 -4 526.44 20.78 4 5 4 547.15 21.28 -4 5 -4 528.68 12.12 -4 5 -4 522.00 20.77 -4 5 -4 517.40 10.60 4 5 4 514.02 11.91 -4 5 -4 518.54 12.14 4 5 4 514.10 11.76 -4 5 -4 533.45 11.84 4 5 4 529.57 11.89 4 5 4 531.14 11.99 4 5 4 527.04 12.02 4 5 4 508.01 20.77 4 5 4 502.11 10.27 4 5 4 502.43 11.97 -4 5 -4 514.03 11.42 -4 5 -4 502.76 20.25 -4 5 -4 501.99 12.08 4 5 4 493.18 10.73 -4 5 -5 93.72 5.45 -4 5 -5 125.79 6.20 -4 5 -5 134.53 5.77 4 5 5 103.55 5.54 4 5 5 117.69 5.75 4 5 5 116.99 5.72 -4 5 -5 118.73 5.91 4 5 5 120.00 5.56 4 5 5 119.38 5.74 4 5 5 125.19 5.36 4 5 5 116.77 5.99 -4 5 -5 117.23 5.70 -4 5 -5 126.05 6.26 4 5 5 125.22 5.62 -4 5 -6 1187.01 18.21 -4 5 -6 1192.58 16.63 4 5 6 1177.46 17.80 -4 5 -6 1162.38 17.88 4 5 6 1159.97 16.47 4 5 6 1129.27 16.49 -4 5 -6 1218.56 17.88 4 5 6 1131.41 15.80 4 5 6 1201.55 16.98 4 5 6 1190.02 16.06 -4 5 -6 1252.87 17.74 -4 5 -6 1186.11 17.98 4 5 6 1154.35 16.78 -4 5 -7 32.44 3.42 -4 5 -7 30.62 2.99 -4 5 -7 32.15 3.23 -4 5 -7 34.70 3.31 4 5 7 29.37 2.72 4 5 7 31.49 2.81 -4 5 -7 35.89 3.29 -4 5 -7 30.71 3.30 4 5 7 31.27 3.03 4 5 7 24.90 2.81 -4 5 -8 87.10 4.64 -4 5 -8 87.68 4.36 -4 5 -8 93.11 4.38 4 5 8 89.75 4.34 -4 5 -8 93.66 4.52 4 5 8 102.39 4.22 -4 5 -8 93.13 4.51 4 5 8 82.04 4.21 -4 5 -9 29.38 2.28 -4 5 -9 35.26 2.66 4 5 9 29.98 2.21 -4 5 -9 28.68 2.34 -4 5 -9 33.90 2.60 4 5 9 29.08 2.27 4 6 -10 65.14 3.52 4 6 -10 58.77 3.29 4 6 -10 62.64 3.22 -4 6 10 65.26 3.26 -4 6 10 61.80 3.39 4 6 -10 72.37 3.71 4 6 -10 65.49 3.39 -4 6 10 72.87 3.37 -4 6 10 72.71 3.47 -4 6 9 5.97 1.74 4 6 -9 5.90 1.83 4 6 -9 4.86 1.89 -4 6 9 7.89 1.96 -4 6 9 3.69 1.92 4 6 -9 6.35 1.84 -4 6 9 7.99 2.00 4 6 -9 8.37 2.12 4 6 -9 5.63 1.92 -4 6 9 7.29 1.87 4 6 -8 379.87 9.91 4 6 -8 405.79 9.86 -4 6 8 386.47 9.85 4 6 -8 374.30 9.48 -4 6 8 365.21 10.05 -4 6 8 380.85 9.98 4 6 -8 382.53 9.77 -4 6 8 401.91 9.36 -4 6 8 395.52 9.53 -4 6 7 5.29 1.93 4 6 -7 0.03 2.27 4 6 -7 2.76 1.97 -4 6 7 3.79 2.07 -4 6 7 3.45 2.26 4 6 -7 6.23 2.24 4 6 -7 4.37 2.42 4 6 -7 3.01 1.79 -4 6 7 3.90 2.14 4 6 -7 -0.16 2.15 4 6 -7 3.09 2.20 -4 6 7 2.32 1.94 4 6 -6 104.19 5.97 4 6 -6 107.86 5.96 -4 6 6 112.67 5.98 4 6 -6 111.01 5.84 -4 6 6 107.08 5.95 4 6 -6 114.97 5.88 4 6 -6 106.44 5.25 -4 6 6 113.40 6.11 -4 6 6 106.56 5.78 4 6 -6 114.78 6.22 4 6 -6 110.95 5.94 -4 6 6 120.44 5.76 -4 6 6 108.92 5.61 -4 6 5 709.83 12.09 4 6 -5 763.31 15.33 4 6 -5 785.58 15.21 -4 6 5 758.81 14.99 4 6 -5 787.12 14.97 -4 6 5 773.56 15.20 4 6 -5 747.11 13.73 -4 6 5 726.02 14.59 -4 6 5 773.06 14.92 4 6 -5 754.64 15.31 4 6 -5 763.59 14.80 -4 6 5 791.81 14.12 -4 6 5 783.87 14.84 -4 6 4 282.59 7.81 4 6 -4 282.32 9.37 4 6 -4 282.21 9.16 -4 6 4 295.86 9.24 4 6 -4 273.55 8.99 4 6 -4 282.60 7.80 -4 6 4 283.02 15.82 -4 6 4 297.67 9.26 4 6 -4 268.52 8.65 4 6 -4 265.30 15.72 -4 6 4 284.08 8.84 -4 6 4 267.75 8.88 4 6 -4 277.52 9.09 4 6 -4 284.33 9.25 -4 6 4 286.89 8.63 -4 6 4 274.71 8.76 -4 6 3 1810.84 36.28 -4 6 3 1917.12 20.53 -4 6 3 1836.06 39.78 4 6 -3 1908.91 23.63 -4 6 3 1862.54 22.80 4 6 -3 1932.45 23.54 4 6 -3 1918.74 21.06 -4 6 3 1824.07 22.32 4 6 -3 1861.50 22.60 -4 6 3 1876.12 21.59 4 6 -3 1841.93 40.08 4 6 -3 1715.06 35.15 4 6 -3 1890.76 19.41 -4 6 3 1904.33 22.82 4 6 -3 1840.47 23.12 4 6 -3 1885.33 23.08 -4 6 3 1859.67 21.79 -4 6 3 1843.33 22.17 -4 6 2 976.61 27.22 -4 6 2 978.96 14.89 -4 6 2 924.39 13.73 4 6 -2 951.65 16.75 4 6 -2 967.36 16.60 -4 6 2 947.25 16.17 4 6 -2 996.56 15.55 4 6 -2 988.67 16.83 -4 6 2 955.65 15.58 -4 6 2 1000.25 29.11 4 6 -2 976.18 16.45 4 6 -2 977.71 29.19 4 6 -2 919.14 26.45 4 6 -2 950.41 14.57 -4 6 2 988.89 15.88 4 6 -2 952.97 16.55 4 6 -2 979.13 16.25 -4 6 2 988.55 15.86 -4 6 2 965.26 15.86 -4 6 1 456.76 11.04 -4 6 1 466.07 19.14 -4 6 1 489.88 10.70 -4 6 1 468.78 10.23 -4 6 1 441.65 17.25 4 6 -1 480.84 11.98 4 6 -1 468.77 11.11 4 6 -1 475.12 11.68 -4 6 1 489.76 10.66 4 6 -1 472.47 11.68 4 6 -1 474.11 11.64 4 6 -1 489.58 19.73 4 6 -1 466.89 20.25 4 6 -1 496.16 10.88 -4 6 1 467.69 10.73 4 6 -1 465.46 11.63 -4 6 1 487.83 11.39 -4 6 1 488.02 11.20 -4 6 0 124.70 5.87 -4 6 0 127.36 5.87 -4 6 0 142.08 11.00 4 6 0 127.53 6.38 4 6 0 128.66 6.42 4 6 0 126.29 5.37 -4 6 0 124.19 5.89 4 6 0 132.51 6.20 4 6 0 121.69 6.19 -4 6 0 122.14 5.51 -4 6 0 123.40 5.23 4 6 0 124.28 6.22 4 6 0 122.40 10.58 4 6 0 112.48 10.32 4 6 0 118.13 5.77 -4 6 0 124.07 5.35 4 6 0 119.67 6.03 -4 6 0 111.35 9.30 -4 6 0 125.03 5.91 -4 6 -1 103.20 5.36 -4 6 -1 96.00 8.70 -4 6 -1 107.03 5.45 4 6 1 94.42 8.61 -4 6 -1 115.83 10.02 4 6 1 103.46 5.03 4 6 1 86.68 5.56 4 6 1 100.09 5.47 4 6 1 105.39 5.75 -4 6 -1 100.22 5.15 4 6 1 118.34 5.90 -4 6 -1 100.74 4.88 -4 6 -1 106.41 10.05 4 6 1 102.20 5.67 4 6 1 105.31 10.15 4 6 1 97.46 5.30 4 6 1 108.39 5.78 -4 6 -1 102.27 5.26 -4 6 -1 104.09 5.49 -4 6 -2 588.79 11.86 -4 6 -2 565.31 20.78 -4 6 -2 618.34 12.65 4 6 2 567.60 20.66 -4 6 -2 604.55 12.63 -4 6 -2 587.53 21.79 4 6 2 572.52 13.33 4 6 2 585.04 12.12 4 6 2 599.05 13.20 -4 6 -2 593.68 11.89 4 6 2 591.87 13.09 4 6 2 604.06 22.95 4 6 2 589.77 12.81 4 6 2 586.73 12.97 -4 6 -2 584.13 11.10 -4 6 -2 559.79 20.42 -4 6 -2 608.22 12.76 4 6 2 561.85 12.73 -4 6 -3 1230.11 16.67 -4 6 -3 1303.12 18.45 -4 6 -3 1270.64 18.26 4 6 3 1272.62 19.52 4 6 3 1266.44 18.26 4 6 3 1245.47 18.72 4 6 3 1266.29 18.77 -4 6 -3 1240.49 17.59 4 6 3 1231.27 18.75 4 6 3 1209.75 18.37 4 6 3 1231.71 18.86 -4 6 -3 1253.72 17.02 -4 6 -3 1281.34 18.62 4 6 3 1263.49 15.64 -4 6 -4 33.73 3.43 -4 6 -4 36.38 3.48 4 6 4 38.62 3.53 4 6 4 35.52 3.69 4 6 4 37.62 3.59 -4 6 -4 39.53 3.57 4 6 4 33.77 3.42 4 6 4 36.26 3.64 4 6 4 34.87 3.55 -4 6 -4 39.24 3.64 -4 6 -4 32.86 3.57 4 6 4 36.48 2.97 4 6 5 83.41 4.82 -4 6 -5 77.88 4.77 -4 6 -5 87.68 5.04 -4 6 -5 82.53 4.31 4 6 5 90.93 5.10 4 6 5 86.03 4.83 -4 6 -5 86.74 4.93 4 6 5 76.76 4.63 4 6 5 79.67 4.77 4 6 5 83.65 5.08 -4 6 -5 78.05 4.51 -4 6 -5 81.18 4.96 4 6 5 82.34 4.32 -4 6 -6 25.35 2.96 4 6 6 34.05 3.32 -4 6 -6 34.92 3.38 -4 6 -6 28.73 2.68 4 6 6 27.34 2.78 4 6 6 24.02 2.66 -4 6 -6 29.88 3.03 4 6 6 27.13 2.67 4 6 6 32.42 3.03 -4 6 -6 33.50 3.21 -4 6 -6 34.95 3.22 4 6 6 36.10 2.84 -4 6 -7 83.02 4.38 -4 6 -7 100.57 4.80 -4 6 -7 94.52 4.07 4 6 7 88.81 4.37 4 6 7 81.79 3.78 -4 6 -7 86.10 4.29 4 6 7 88.31 4.04 -4 6 -7 97.86 4.38 4 6 7 102.49 4.29 -4 6 -8 56.06 3.16 -4 6 -8 53.11 3.12 4 6 8 54.71 3.06 -4 6 -8 54.07 3.02 -4 6 -8 56.37 3.18 4 6 8 65.90 3.10 -4 7 9 10.97 1.72 4 7 -9 6.53 1.61 4 7 -9 6.13 1.76 -4 7 9 6.88 1.50 -4 7 9 5.97 1.49 -4 7 9 8.56 1.79 4 7 -9 11.79 1.96 4 7 -9 6.65 1.57 4 7 -8 389.89 8.55 4 7 -8 395.68 8.94 4 7 -8 401.68 8.28 -4 7 8 389.45 9.11 -4 7 8 405.15 9.10 4 7 -8 411.25 8.99 4 7 -8 404.65 8.84 -4 7 8 398.78 8.86 -4 7 8 416.30 7.74 -4 7 8 414.87 8.85 -4 7 7 21.25 2.62 4 7 -7 18.94 2.75 4 7 -7 20.23 2.83 -4 7 7 19.61 2.47 4 7 -7 23.33 2.78 -4 7 7 22.11 2.79 -4 7 7 25.54 2.71 4 7 -7 19.41 2.61 4 7 -7 17.94 2.72 -4 7 7 27.25 2.55 -4 7 6 24.99 3.02 4 7 -6 21.54 3.19 4 7 -6 16.77 2.78 -4 7 6 19.66 2.80 4 7 -6 22.16 2.97 -4 7 6 23.79 3.03 4 7 -6 19.41 2.35 -4 7 6 22.39 2.73 4 7 -6 23.81 3.01 4 7 -6 19.43 2.91 -4 7 6 22.29 2.64 4 7 -5 181.60 7.39 -4 7 5 194.20 7.40 4 7 -5 193.67 7.24 -4 7 5 188.41 7.46 4 7 -5 179.88 6.60 4 7 -5 197.55 7.49 -4 7 5 184.60 7.05 -4 7 5 188.46 7.30 4 7 -5 192.23 7.51 4 7 -5 197.82 7.40 -4 7 5 198.71 6.69 -4 7 5 192.38 7.23 4 7 -4 329.43 9.97 -4 7 4 321.24 9.65 4 7 -4 329.22 9.67 -4 7 4 338.25 9.73 4 7 -4 325.99 9.16 -4 7 4 330.69 9.12 -4 7 4 319.09 9.48 4 7 -4 320.16 9.51 4 7 -4 328.64 9.59 -4 7 4 323.06 8.75 -4 7 4 331.83 9.52 -4 7 3 83.58 4.25 4 7 -3 84.18 5.50 4 7 -3 79.92 5.33 -4 7 3 96.00 5.53 4 7 -3 89.47 4.53 4 7 -3 97.30 5.51 -4 7 3 91.07 5.16 4 7 -3 92.16 5.13 -4 7 3 89.92 4.70 -4 7 3 99.52 5.26 4 7 -3 89.54 5.42 4 7 -3 94.69 5.40 -4 7 3 84.76 4.75 -4 7 3 89.47 5.06 -4 7 2 225.27 7.88 -4 7 2 221.67 6.90 4 7 -2 224.61 8.40 -4 7 2 227.65 8.03 4 7 -2 232.36 7.41 4 7 -2 223.76 8.29 -4 7 2 226.28 7.56 4 7 -2 239.96 8.36 4 7 -2 229.82 6.99 -4 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179.74 6.79 -5 6 6 190.25 7.53 5 6 -6 182.47 7.33 5 6 -6 179.11 7.33 -5 6 6 186.03 6.97 -5 6 6 195.91 7.19 -5 6 5 36.91 3.34 5 6 -5 37.61 3.90 -5 6 5 40.45 4.05 5 6 -5 37.76 3.90 -5 6 5 36.59 3.83 5 6 -5 37.40 3.56 -5 6 5 33.25 3.47 5 6 -5 41.97 3.93 5 6 -5 38.94 4.13 5 6 -5 35.87 3.83 -5 6 5 39.90 3.69 -5 6 5 38.57 3.83 -5 6 4 146.53 5.93 5 6 -4 148.53 6.88 5 6 -4 134.66 6.82 -5 6 4 151.31 7.04 5 6 -4 150.99 6.68 5 6 -4 147.03 5.76 -5 6 4 145.15 6.68 5 6 -4 144.63 6.55 -5 6 4 143.30 6.74 5 6 -4 140.19 6.53 5 6 -4 152.09 6.89 -5 6 4 147.64 6.47 -5 6 4 144.03 6.56 -5 6 3 794.76 13.86 -5 6 3 760.23 12.38 5 6 -3 698.47 14.42 5 6 -3 698.56 14.40 -5 6 3 790.74 15.09 5 6 -3 804.48 13.93 5 6 -3 695.04 14.23 -5 6 3 790.52 14.77 5 6 -3 756.81 14.70 5 6 -3 755.23 12.88 -5 6 3 766.15 14.75 5 6 -3 726.20 14.32 -5 6 3 784.45 14.52 -5 6 3 759.24 14.52 -5 6 2 219.16 7.91 -5 6 2 215.52 13.97 -5 6 2 230.53 7.62 -5 6 2 213.04 6.96 5 6 -2 216.02 8.33 5 6 -2 232.82 8.36 -5 6 2 230.13 8.23 5 6 -2 230.86 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6 -2 55.61 4.41 5 6 2 61.79 4.45 -5 6 -2 57.86 4.25 5 6 2 52.18 4.47 5 6 2 56.53 4.19 5 6 2 52.72 4.02 -5 6 -2 54.31 3.96 5 6 2 58.06 4.30 5 6 2 60.69 4.41 5 6 2 54.79 4.32 -5 6 -2 60.91 3.83 -5 6 -2 55.01 4.19 -5 6 -3 27.57 3.21 -5 6 -3 27.31 3.27 5 6 3 29.23 3.07 5 6 3 29.09 3.19 5 6 3 26.63 3.15 -5 6 -3 29.52 3.12 5 6 3 26.46 3.24 5 6 3 30.08 3.22 5 6 3 26.19 3.23 -5 6 -3 31.23 2.93 -5 6 -3 33.70 3.33 5 6 4 5.79 1.81 5 6 4 1.63 1.83 -5 6 -4 4.33 1.92 5 6 4 1.45 1.83 5 6 4 5.10 1.86 -5 6 -4 4.64 1.93 5 6 4 5.18 2.07 -5 6 -4 4.32 2.26 5 6 4 3.37 1.79 5 6 4 3.95 1.88 -5 6 -4 3.08 1.73 -5 6 -4 1.53 1.82 -5 6 -5 49.15 3.67 -5 6 -5 46.75 3.69 5 6 5 48.91 3.40 5 6 5 46.11 3.44 5 6 5 51.75 3.56 -5 6 -5 52.48 3.69 5 6 5 51.15 3.38 5 6 5 51.57 3.52 -5 6 -5 51.84 3.42 -5 6 -5 52.72 3.85 5 6 5 54.01 3.22 5 6 6 16.35 1.96 -5 6 -6 16.28 2.18 -5 6 -6 13.35 2.04 5 6 6 14.49 1.90 -5 6 -6 14.90 2.10 5 6 6 13.01 1.93 5 6 6 13.52 1.91 -5 6 -6 12.53 2.01 -5 6 -6 10.68 2.07 -5 6 -7 157.53 4.91 5 6 7 161.04 4.95 -5 6 -7 154.54 4.88 -5 6 -7 146.74 4.93 -5 6 -7 154.25 4.80 5 7 -8 70.47 3.58 -5 7 8 72.95 3.68 5 7 -8 74.00 3.64 -5 7 8 75.97 3.86 5 7 -8 65.43 3.60 -5 7 8 79.13 3.41 -5 7 8 77.56 3.68 5 7 -7 117.24 5.17 5 7 -7 120.22 4.98 -5 7 7 130.25 5.34 5 7 -7 139.42 5.21 -5 7 7 128.96 5.57 -5 7 7 104.00 4.87 5 7 -7 129.75 5.27 5 7 -7 138.05 5.33 -5 7 7 134.33 4.88 -5 7 7 139.48 5.30 5 7 -6 307.17 8.49 5 7 -6 296.16 8.54 -5 7 6 311.20 8.62 5 7 -6 311.80 8.52 -5 7 6 301.18 8.76 5 7 -6 322.58 7.90 -5 7 6 315.71 8.87 5 7 -6 327.18 8.70 5 7 -6 317.27 8.61 -5 7 6 336.10 8.04 -5 7 6 332.45 8.58 5 7 -5 46.57 3.82 -5 7 5 42.47 3.71 5 7 -5 47.69 3.77 -5 7 5 39.37 3.56 5 7 -5 49.45 3.66 -5 7 5 40.54 3.65 5 7 -5 46.28 3.77 -5 7 5 44.84 3.26 -5 7 5 45.27 3.62 -5 7 4 35.24 3.45 -5 7 4 28.70 2.65 5 7 -4 30.13 3.54 5 7 -4 33.53 3.36 -5 7 4 36.20 3.52 5 7 -4 31.73 3.30 -5 7 4 28.77 3.14 5 7 -4 29.84 3.12 -5 7 4 34.16 3.37 5 7 -4 32.64 3.56 -5 7 4 33.83 2.98 -5 7 3 6.02 2.03 -5 7 3 9.43 1.99 5 7 -3 12.72 2.67 5 7 -3 7.75 2.62 5 7 -3 9.74 2.08 -5 7 3 7.21 2.24 5 7 -3 8.58 2.39 5 7 -3 9.87 2.32 -5 7 3 8.82 2.22 5 7 -3 9.68 2.32 -5 7 3 10.99 2.35 -5 7 3 10.31 2.50 -5 7 2 126.54 5.89 -5 7 2 120.63 5.25 5 7 -2 135.87 6.41 5 7 -2 127.24 5.99 -5 7 2 135.11 6.08 5 7 -2 132.08 5.67 5 7 -2 129.91 6.14 5 7 -2 138.23 6.21 5 7 -2 129.36 5.36 -5 7 2 118.54 5.60 5 7 -2 133.20 6.26 -5 7 2 131.29 5.82 -5 7 1 275.73 8.40 -5 7 1 264.10 7.74 5 7 -1 248.33 8.64 5 7 -1 276.96 8.57 -5 7 1 254.92 8.08 5 7 -1 270.10 8.30 5 7 -1 256.26 8.52 -5 7 1 245.51 6.99 5 7 -1 256.22 8.49 5 7 -1 274.70 7.89 5 7 -1 249.96 8.46 -5 7 1 272.88 8.32 -5 7 0 214.43 7.21 -5 7 0 208.94 7.09 5 7 0 194.49 7.61 -5 7 0 205.10 6.87 -5 7 0 195.61 6.47 5 7 0 215.08 7.47 5 7 0 205.83 7.60 5 7 0 203.67 7.69 5 7 0 214.73 7.18 5 7 0 201.64 7.50 -5 7 0 218.51 7.40 -5 7 -1 16.86 2.51 -5 7 -1 23.40 2.88 -5 7 -1 15.30 2.31 5 7 1 13.92 2.65 5 7 1 17.25 2.24 5 7 1 21.81 2.93 5 7 1 20.81 2.78 5 7 1 16.78 2.69 5 7 1 17.76 2.59 5 7 1 15.95 2.59 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57.53 3.50 10 0 -5 50.51 3.34 -10 0 5 52.06 3.29 -10 0 5 54.61 3.58 10 0 -5 51.19 3.38 10 0 -5 58.57 3.58 -10 0 4 24.58 2.61 10 0 -4 18.43 2.07 10 0 -4 22.67 2.49 -10 0 4 20.46 2.45 -10 0 4 21.13 2.51 10 0 -4 17.66 2.38 10 0 -4 18.67 2.33 -10 0 3 203.50 6.18 10 0 -3 212.61 6.27 10 0 -3 196.66 6.31 -10 0 3 208.24 6.58 -10 0 3 196.30 6.63 10 0 -3 212.52 6.68 10 0 -3 201.00 6.52 -10 0 2 788.57 11.80 10 0 -2 803.59 12.45 10 0 -2 806.36 12.30 -10 0 2 816.27 13.12 10 0 -2 817.07 12.71 10 0 -2 813.09 12.88 -10 0 2 764.94 10.84 -10 0 1 23.35 2.23 10 0 -1 21.65 2.49 10 0 -1 15.30 1.93 -10 0 1 21.85 2.55 -10 0 1 22.11 2.53 10 0 -1 23.48 2.46 10 0 -1 20.07 2.31 -10 0 1 20.37 2.27 10 0 0 75.04 3.88 -10 0 0 77.31 3.96 -10 0 0 71.31 3.76 10 0 0 68.04 3.49 10 0 0 73.10 3.83 -10 0 0 71.09 3.52 10 0 1 261.44 6.71 -10 0 -1 256.64 6.39 -10 0 -1 254.16 6.37 10 0 1 253.92 6.47 -10 0 -1 273.01 6.37 10 0 2 13.77 1.68 -10 0 -2 17.06 1.78 -10 1 7 33.92 2.65 10 1 -7 41.40 2.79 -10 1 7 41.37 2.80 10 1 -7 39.43 2.64 10 1 -7 38.12 2.49 10 1 -7 39.90 2.76 -10 1 6 216.50 5.40 -10 1 6 247.81 6.78 10 1 -6 236.62 6.62 -10 1 6 235.29 5.78 -10 1 6 234.83 6.28 10 1 -6 220.95 5.95 10 1 -6 240.56 6.22 10 1 -6 238.04 6.51 -10 1 5 68.37 3.81 10 1 -5 67.56 3.85 -10 1 5 66.49 3.53 -10 1 5 65.22 3.67 10 1 -5 61.30 3.16 10 1 -5 76.85 3.84 10 1 -5 68.69 3.85 -10 1 4 58.94 3.62 10 1 -4 55.52 3.51 -10 1 4 59.58 3.48 -10 1 4 52.71 3.33 10 1 -4 56.76 3.55 10 1 -4 57.34 3.63 -10 1 3 174.87 5.96 10 1 -3 187.24 5.54 10 1 -3 173.55 6.08 -10 1 3 181.45 6.09 -10 1 3 180.66 5.85 10 1 -3 178.09 6.04 10 1 -3 177.82 6.21 -10 1 2 96.24 4.40 10 1 -2 93.36 4.24 10 1 -2 81.83 4.26 -10 1 2 94.77 4.43 -10 1 2 88.92 4.22 10 1 -2 95.91 4.43 10 1 -2 83.31 4.31 -10 1 1 14.94 1.91 10 1 -1 17.65 2.19 10 1 -1 16.35 2.02 -10 1 1 18.10 2.39 -10 1 1 13.78 1.91 10 1 -1 16.70 2.13 10 1 -1 17.49 2.23 -10 1 1 15.99 1.87 -10 1 0 8.19 1.62 10 1 0 8.28 1.67 -10 1 0 10.70 2.08 -10 1 0 6.56 1.68 10 1 0 11.89 1.84 10 1 0 6.88 1.73 -10 1 0 9.00 1.65 10 1 1 103.16 4.25 -10 1 -1 106.46 4.27 10 1 1 100.72 3.78 10 1 1 113.34 4.39 -10 1 -1 103.81 3.94 -10 2 7 246.24 5.87 10 2 -7 232.46 5.71 10 2 -7 225.91 5.60 10 2 -7 237.28 5.90 -10 2 6 32.65 2.29 -10 2 6 35.79 2.72 10 2 -6 36.14 2.77 10 2 -6 35.27 2.53 10 2 -6 33.93 2.39 10 2 -6 33.26 2.57 -10 2 5 193.11 5.28 -10 2 5 195.47 5.96 10 2 -5 201.53 6.17 -10 2 5 184.94 4.99 10 2 -5 178.25 5.19 10 2 -5 196.65 5.68 10 2 -5 191.62 5.96 -10 2 4 58.05 3.11 -10 2 4 61.91 3.56 10 2 -4 56.23 3.50 -10 2 4 58.56 3.22 10 2 -4 60.49 3.50 10 2 -4 55.54 3.52 -10 2 3 77.10 3.91 10 2 -3 83.17 4.15 -10 2 3 80.58 3.87 10 2 -3 77.60 3.97 10 2 -3 74.34 3.95 -10 2 2 96.38 4.30 10 2 -2 102.24 3.99 10 2 -2 98.03 4.41 -10 2 2 100.61 4.34 10 2 -2 104.47 4.49 10 2 -2 107.01 4.69 -10 2 1 102.62 4.18 10 2 -1 93.90 3.94 10 2 -1 100.23 4.19 -10 2 1 108.75 4.40 10 2 -1 96.12 4.23 10 2 -1 107.16 4.54 -10 2 0 19.26 1.97 10 2 0 19.98 2.07 10 2 0 16.00 1.83 -10 2 0 21.40 2.25 10 2 0 20.62 2.17 10 2 0 16.19 2.00 10 2 1 60.50 3.12 -10 2 -1 66.27 3.32 10 2 1 64.93 3.34 -10 3 5 42.54 2.55 -10 3 5 44.24 2.75 10 3 -5 40.36 2.71 10 3 -5 42.74 2.54 10 3 -5 45.19 2.80 -10 3 4 131.29 4.33 -10 3 4 149.64 4.98 10 3 -4 134.20 4.74 10 3 -4 144.99 4.74 10 3 -4 145.61 4.85 -10 3 3 73.93 3.30 -10 3 3 76.88 3.70 10 3 -3 66.42 3.53 -10 3 3 68.00 3.13 10 3 -3 73.46 3.54 10 3 -3 76.67 3.64 -10 3 2 189.65 5.53 10 3 -2 181.96 5.45 -10 3 2 193.24 5.25 10 3 -2 190.45 5.61 10 3 -2 188.38 5.61 -10 3 1 50.76 2.91 10 3 -1 40.87 2.62 -10 3 1 43.84 2.73 10 3 -1 48.72 2.90 10 3 -1 50.61 3.04 0 0 0 0.00 0.00 TITL 007b-1812 in P2(1) REM P2(1) (#4 in standard setting) CELL 1.54184 9.049073 8.265926 11.432336 90.0000 103.3328 90.0000 ZERR 1.00 0.000084 0.000088 0.000112 0.0000 0.0010 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C O UNIT 1.00 1.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 74473