data_mo_yz001_0m _audit_creation_date 2019-07-03 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2014/7' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C24 H28 N2 O6' _chemical_formula_sum 'C24 H28 N2 O6' _chemical_formula_weight 440.48 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.348(3) _cell_length_b 9.557(3) _cell_length_c 14.427(4) _cell_angle_alpha 72.333(9) _cell_angle_beta 77.148(9) _cell_angle_gamma 63.908(8) _cell_volume 1097.0(5) _cell_formula_units_Z 2 _cell_measurement_reflns_used 9425 _cell_measurement_temperature 100 _cell_measurement_theta_max 26.812 _cell_measurement_theta_min 2.439 _shelx_estimated_absorpt_T_max 0.992 _shelx_estimated_absorpt_T_min 0.971 _exptl_absorpt_coefficient_mu 0.096 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.7261 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0478 before and 0.0386 after correction. The Ratio of minimum to maximum transmission is 0.9741. The \l/2 correction factor is 0.0015.' _exptl_absorpt_special_details ? _exptl_crystal_colour 'metallic light colourless' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.334 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description irregular _exptl_crystal_F_000 468 _exptl_crystal_size_max 0.31 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.08 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0238 _diffrn_reflns_av_unetI/netI 0.0117 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 47843 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.859 _diffrn_reflns_theta_min 2.439 _diffrn_ambient_temperature 100 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4316 _reflns_number_total 4715 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.323 _refine_diff_density_min -0.195 _refine_diff_density_rms 0.037 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.009 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 297 _refine_ls_number_reflns 4715 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0353 _refine_ls_R_factor_gt 0.0318 _refine_ls_restrained_S_all 1.009 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0427P)^2^+0.4336P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0812 _refine_ls_wR_factor_ref 0.0844 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C16(H16), C15(H15) 2.b Secondary CH2 refined with riding coordinates: C17(H17A,H17B), C7(H7A,H7B) 2.c Aromatic/amide H refined with riding coordinates: C1(H1), C10(H10), C5(H5), C11(H11), C3(H3), C2(H2A), C13(H13), C4(H4), C12(H12) 2.d Idealised Me refined as rotating group: C20(H20A,H20B,H20C), C21(H21A,H21B,H21C), C22(H22A,H22B,H22C), C24(H24A,H24B, H24C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.52402(8) 0.70622(8) 0.54851(5) 0.01524(15) Uani 1 1 d . . . . . O2 O 0.32589(9) 0.66976(9) 0.50613(5) 0.01803(16) Uani 1 1 d . . . . . O3 O 0.75458(9) 0.00363(9) 0.74689(5) 0.01748(16) Uani 1 1 d . . . . . O5 O 0.32495(9) 0.71570(9) 0.86853(5) 0.02007(17) Uani 1 1 d . . . . . O4 O 0.76956(10) 0.12739(9) 0.85492(6) 0.02415(18) Uani 1 1 d . . . . . N2 N 0.69514(10) 0.26392(10) 0.70233(6) 0.01598(18) Uani 1 1 d . . . . . N1 N 0.40617(10) 0.55915(10) 0.65973(6) 0.01385(17) Uani 1 1 d . . . . . O6 O 0.32460(13) 0.50538(11) 0.99109(6) 0.0359(2) Uani 1 1 d . . . . . C9 C 0.29625(12) 0.48625(11) 0.70142(7) 0.0143(2) Uani 1 1 d . . . . . C8 C 0.41123(11) 0.64711(11) 0.56617(7) 0.01387(19) Uani 1 1 d . . . . . C6 C 0.66797(12) 0.85789(12) 0.43996(7) 0.0146(2) Uani 1 1 d . . . . . C16 C 0.51110(12) 0.53137(12) 0.73306(7) 0.0145(2) Uani 1 1 d . . . . . H16 H 0.5091 0.6357 0.7355 0.017 Uiso 1 1 calc R . . . . C18 C 0.74259(12) 0.13090(12) 0.77544(7) 0.0162(2) Uani 1 1 d . . . . . C14 C 0.30838(12) 0.42514(12) 0.80134(7) 0.0159(2) Uani 1 1 d . . . . . C17 C 0.68359(12) 0.41645(12) 0.70944(7) 0.0164(2) Uani 1 1 d . . . . . H17A H 0.7291 0.4674 0.6467 0.020 Uiso 1 1 calc R . . . . H17B H 0.7486 0.3976 0.7611 0.020 Uiso 1 1 calc R . . . . C23 C 0.35645(13) 0.56078(13) 0.90650(8) 0.0191(2) Uani 1 1 d . . . . . C7 C 0.52815(12) 0.81273(12) 0.45310(7) 0.0149(2) Uani 1 1 d . . . . . H7A H 0.4271 0.9102 0.4476 0.018 Uiso 1 1 calc R . . . . H7B H 0.5395 0.7587 0.4016 0.018 Uiso 1 1 calc R . . . . C1 C 0.78494(13) 0.78472(12) 0.50418(8) 0.0181(2) Uani 1 1 d . . . . . H1 H 0.7780 0.7026 0.5598 0.022 Uiso 1 1 calc R . . . . C10 C 0.19165(12) 0.46759(12) 0.65599(8) 0.0167(2) Uani 1 1 d . . . . . H10 H 0.1831 0.5099 0.5878 0.020 Uiso 1 1 calc R . . . . C5 C 0.68186(13) 0.97626(12) 0.35814(8) 0.0185(2) Uani 1 1 d . . . . . H5 H 0.6033 1.0264 0.3132 0.022 Uiso 1 1 calc R . . . . C15 C 0.43324(12) 0.45910(12) 0.83147(7) 0.0162(2) Uani 1 1 d . . . . . H15 H 0.5164 0.3547 0.8623 0.019 Uiso 1 1 calc R . . . . C11 C 0.09955(12) 0.38459(13) 0.71385(8) 0.0197(2) Uani 1 1 d . . . . . H11 H 0.0283 0.3689 0.6842 0.024 Uiso 1 1 calc R . . . . C3 C 0.92447(13) 0.94955(13) 0.40667(8) 0.0198(2) Uani 1 1 d . . . . . H3 H 1.0110 0.9814 0.3957 0.024 Uiso 1 1 calc R . . . . C19 C 0.76005(12) -0.14332(12) 0.82161(7) 0.0162(2) Uani 1 1 d . . . . . C2 C 0.91243(13) 0.83075(13) 0.48776(8) 0.0212(2) Uani 1 1 d . . . . . H2A H 0.9914 0.7804 0.5324 0.025 Uiso 1 1 calc R . . . . C20 C 0.91484(13) -0.22413(13) 0.86957(8) 0.0219(2) Uani 1 1 d . . . . . H20A H 1.0060 -0.2370 0.8189 0.033 Uiso 1 1 calc GR . . . . H20B H 0.9239 -0.3296 0.9108 0.033 Uiso 1 1 calc GR . . . . H20C H 0.9145 -0.1579 0.9099 0.033 Uiso 1 1 calc GR . . . . C13 C 0.21502(13) 0.34447(13) 0.85810(8) 0.0204(2) Uani 1 1 d . . . . . H13 H 0.2227 0.3034 0.9264 0.024 Uiso 1 1 calc R . . . . C4 C 0.80915(13) 1.02169(13) 0.34156(8) 0.0205(2) Uani 1 1 d . . . . . H4 H 0.8173 1.1025 0.2854 0.025 Uiso 1 1 calc R . . . . C12 C 0.10968(13) 0.32444(13) 0.81367(8) 0.0222(2) Uani 1 1 d . . . . . H12 H 0.0447 0.2695 0.8517 0.027 Uiso 1 1 calc R . . . . C21 C 0.75707(15) -0.24797(13) 0.76216(9) 0.0253(2) Uani 1 1 d . . . . . H21A H 0.6615 -0.1914 0.7268 0.038 Uiso 1 1 calc GR . . . . H21B H 0.7546 -0.3480 0.8060 0.038 Uiso 1 1 calc GR . . . . H21C H 0.8531 -0.2723 0.7152 0.038 Uiso 1 1 calc GR . . . . C22 C 0.61120(14) -0.10180(14) 0.89448(9) 0.0252(2) Uani 1 1 d . . . . . H22A H 0.6188 -0.0402 0.9352 0.038 Uiso 1 1 calc GR . . . . H22B H 0.6029 -0.2007 0.9362 0.038 Uiso 1 1 calc GR . . . . H22C H 0.5161 -0.0377 0.8590 0.038 Uiso 1 1 calc GR . . . . C24 C 0.24936(15) 0.81754(15) 0.93745(9) 0.0258(2) Uani 1 1 d . . . . . H24A H 0.2192 0.9300 0.9020 0.039 Uiso 1 1 calc GR . . . . H24B H 0.3245 0.7903 0.9843 0.039 Uiso 1 1 calc GR . . . . H24C H 0.1534 0.8011 0.9726 0.039 Uiso 1 1 calc GR . . . . H2 H 0.6891(16) 0.2554(16) 0.6472(11) 0.023(3) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0173(3) 0.0161(3) 0.0129(3) -0.0001(3) -0.0018(3) -0.0092(3) O2 0.0192(4) 0.0217(4) 0.0142(3) -0.0017(3) -0.0035(3) -0.0099(3) O3 0.0241(4) 0.0149(3) 0.0130(3) -0.0019(3) -0.0020(3) -0.0082(3) O5 0.0252(4) 0.0183(4) 0.0159(4) -0.0059(3) -0.0021(3) -0.0068(3) O4 0.0387(5) 0.0186(4) 0.0160(4) -0.0015(3) -0.0097(3) -0.0107(3) N2 0.0188(4) 0.0156(4) 0.0126(4) -0.0023(3) -0.0027(3) -0.0062(3) N1 0.0141(4) 0.0149(4) 0.0138(4) -0.0023(3) -0.0021(3) -0.0071(3) O6 0.0629(6) 0.0336(5) 0.0152(4) -0.0058(4) 0.0052(4) -0.0272(5) C9 0.0137(4) 0.0109(4) 0.0167(5) -0.0042(4) 0.0014(4) -0.0043(4) C8 0.0141(5) 0.0120(4) 0.0141(5) -0.0042(4) 0.0001(4) -0.0041(4) C6 0.0162(5) 0.0132(4) 0.0141(5) -0.0052(4) 0.0008(4) -0.0052(4) C16 0.0173(5) 0.0146(5) 0.0130(4) -0.0016(4) -0.0036(4) -0.0078(4) C18 0.0173(5) 0.0163(5) 0.0145(5) -0.0034(4) -0.0004(4) -0.0069(4) C14 0.0172(5) 0.0133(5) 0.0167(5) -0.0044(4) -0.0002(4) -0.0058(4) C17 0.0158(5) 0.0154(5) 0.0179(5) -0.0002(4) -0.0031(4) -0.0079(4) C23 0.0232(5) 0.0223(5) 0.0154(5) -0.0037(4) -0.0036(4) -0.0120(4) C7 0.0171(5) 0.0146(5) 0.0115(4) -0.0008(4) -0.0017(4) -0.0064(4) C1 0.0223(5) 0.0160(5) 0.0159(5) -0.0001(4) -0.0032(4) -0.0093(4) C10 0.0147(5) 0.0156(5) 0.0188(5) -0.0051(4) -0.0014(4) -0.0048(4) C5 0.0203(5) 0.0163(5) 0.0160(5) -0.0010(4) -0.0028(4) -0.0063(4) C15 0.0192(5) 0.0156(5) 0.0143(5) -0.0017(4) -0.0018(4) -0.0086(4) C11 0.0151(5) 0.0193(5) 0.0269(6) -0.0083(4) -0.0009(4) -0.0075(4) C3 0.0183(5) 0.0193(5) 0.0239(5) -0.0072(4) 0.0026(4) -0.0101(4) C19 0.0174(5) 0.0136(5) 0.0159(5) -0.0010(4) -0.0013(4) -0.0063(4) C2 0.0203(5) 0.0204(5) 0.0229(5) -0.0023(4) -0.0058(4) -0.0083(4) C20 0.0192(5) 0.0204(5) 0.0227(5) -0.0010(4) -0.0046(4) -0.0066(4) C13 0.0240(5) 0.0197(5) 0.0171(5) -0.0030(4) 0.0020(4) -0.0113(4) C4 0.0244(5) 0.0174(5) 0.0175(5) -0.0011(4) 0.0020(4) -0.0105(4) C12 0.0210(5) 0.0213(5) 0.0261(6) -0.0060(4) 0.0042(4) -0.0130(4) C21 0.0313(6) 0.0178(5) 0.0288(6) -0.0055(4) -0.0089(5) -0.0087(5) C22 0.0199(5) 0.0222(5) 0.0260(6) -0.0016(4) 0.0040(4) -0.0073(4) C24 0.0283(6) 0.0282(6) 0.0252(6) -0.0156(5) 0.0014(5) -0.0109(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C8 1.3464(12) . ? O1 C7 1.4467(12) . ? O2 C8 1.2147(13) . ? O3 C18 1.3510(13) . ? O3 C19 1.4763(12) . ? O5 C23 1.3323(14) . ? O5 C24 1.4510(13) . ? O4 C18 1.2155(13) . ? N2 C18 1.3504(13) . ? N2 C17 1.4473(14) . ? N2 H2 0.840(15) . ? N1 C9 1.4155(13) . ? N1 C8 1.3597(13) . ? N1 C16 1.4878(13) . ? O6 C23 1.2013(14) . ? C9 C14 1.3913(14) . ? C9 C10 1.3881(14) . ? C6 C7 1.5057(14) . ? C6 C1 1.3884(15) . ? C6 C5 1.3930(14) . ? C16 H16 1.0000 . ? C16 C17 1.5321(14) . ? C16 C15 1.5524(14) . ? C14 C15 1.5170(14) . ? C14 C13 1.3847(15) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C23 C15 1.5200(15) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C1 H1 0.9500 . ? C1 C2 1.3937(15) . ? C10 H10 0.9500 . ? C10 C11 1.3951(15) . ? C5 H5 0.9500 . ? C5 C4 1.3881(16) . ? C15 H15 1.0000 . ? C11 H11 0.9500 . ? C11 C12 1.3869(16) . ? C3 H3 0.9500 . ? C3 C2 1.3849(15) . ? C3 C4 1.3869(16) . ? C19 C20 1.5189(15) . ? C19 C21 1.5141(15) . ? C19 C22 1.5218(15) . ? C2 H2A 0.9500 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C13 H13 0.9500 . ? C13 C12 1.3922(16) . ? C4 H4 0.9500 . ? C12 H12 0.9500 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 O1 C7 114.52(8) . . ? C18 O3 C19 119.21(8) . . ? C23 O5 C24 115.24(9) . . ? C18 N2 C17 122.02(9) . . ? C18 N2 H2 119.4(9) . . ? C17 N2 H2 117.6(9) . . ? C9 N1 C16 110.87(8) . . ? C8 N1 C9 124.38(8) . . ? C8 N1 C16 124.72(8) . . ? C14 C9 N1 109.60(9) . . ? C10 C9 N1 129.14(9) . . ? C10 C9 C14 121.23(9) . . ? O1 C8 N1 110.95(8) . . ? O2 C8 O1 124.20(9) . . ? O2 C8 N1 124.85(9) . . ? C1 C6 C7 123.12(9) . . ? C1 C6 C5 118.75(10) . . ? C5 C6 C7 118.11(9) . . ? N1 C16 H16 109.9 . . ? N1 C16 C17 111.37(8) . . ? N1 C16 C15 104.05(8) . . ? C17 C16 H16 109.9 . . ? C17 C16 C15 111.57(8) . . ? C15 C16 H16 109.9 . . ? O4 C18 O3 125.49(9) . . ? O4 C18 N2 124.75(10) . . ? N2 C18 O3 109.76(9) . . ? C9 C14 C15 110.41(9) . . ? C13 C14 C9 120.43(10) . . ? C13 C14 C15 129.15(10) . . ? N2 C17 C16 112.93(8) . . ? N2 C17 H17A 109.0 . . ? N2 C17 H17B 109.0 . . ? C16 C17 H17A 109.0 . . ? C16 C17 H17B 109.0 . . ? H17A C17 H17B 107.8 . . ? O5 C23 C15 113.43(9) . . ? O6 C23 O5 124.10(10) . . ? O6 C23 C15 122.45(10) . . ? O1 C7 C6 108.81(8) . . ? O1 C7 H7A 109.9 . . ? O1 C7 H7B 109.9 . . ? C6 C7 H7A 109.9 . . ? C6 C7 H7B 109.9 . . ? H7A C7 H7B 108.3 . . ? C6 C1 H1 119.7 . . ? C6 C1 C2 120.53(10) . . ? C2 C1 H1 119.7 . . ? C9 C10 H10 121.1 . . ? C9 C10 C11 117.74(10) . . ? C11 C10 H10 121.1 . . ? C6 C5 H5 119.6 . . ? C4 C5 C6 120.72(10) . . ? C4 C5 H5 119.6 . . ? C16 C15 H15 108.4 . . ? C14 C15 C16 103.96(8) . . ? C14 C15 C23 110.06(9) . . ? C14 C15 H15 108.4 . . ? C23 C15 C16 117.37(9) . . ? C23 C15 H15 108.4 . . ? C10 C11 H11 119.3 . . ? C12 C11 C10 121.49(10) . . ? C12 C11 H11 119.3 . . ? C2 C3 H3 120.3 . . ? C2 C3 C4 119.46(10) . . ? C4 C3 H3 120.3 . . ? O3 C19 C20 110.92(8) . . ? O3 C19 C21 102.80(8) . . ? O3 C19 C22 109.05(8) . . ? C20 C19 C22 113.08(9) . . ? C21 C19 C20 109.76(9) . . ? C21 C19 C22 110.74(9) . . ? C1 C2 H2A 119.9 . . ? C3 C2 C1 120.30(10) . . ? C3 C2 H2A 119.9 . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C14 C13 H13 120.5 . . ? C14 C13 C12 119.08(10) . . ? C12 C13 H13 120.5 . . ? C5 C4 H4 119.9 . . ? C3 C4 C5 120.22(10) . . ? C3 C4 H4 119.9 . . ? C11 C12 C13 120.02(10) . . ? C11 C12 H12 120.0 . . ? C13 C12 H12 120.0 . . ? C19 C21 H21A 109.5 . . ? C19 C21 H21B 109.5 . . ? C19 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C19 C22 H22A 109.5 . . ? C19 C22 H22B 109.5 . . ? C19 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? O5 C24 H24A 109.5 . . ? O5 C24 H24B 109.5 . . ? O5 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? _shelx_res_file ; mo_yz001_0m.res created by SHELXL-2014/7 TITL mo_yz001_0m_a.res in P-1 REM Old TITL mo_YZ001_0m in P-1 REM SHELXT solution in P-1 REM R1 0.112, Rweak 0.006, Alpha 0.034, Orientation as input REM Formula found by SHELXT: C24 N2 O6 CELL 0.71073 9.3482 9.5571 14.427 72.333 77.148 63.908 ZERR 2 0.0025 0.0027 0.0038 0.009 0.009 0.008 LATT 1 SFAC C H N O UNIT 48 56 4 12 L.S. 15 PLAN 20 SIZE 0.08 0.15 0.31 TEMP -173.15 BOND $H list 4 fmap 2 53 ACTA OMIT 0 0 1 REM REM REM WGHT 0.042700 0.433600 FVAR 0.74529 O1 4 0.524023 0.706219 0.548513 11.00000 0.01732 0.01606 = 0.01292 -0.00013 -0.00183 -0.00920 O2 4 0.325894 0.669755 0.506126 11.00000 0.01915 0.02172 = 0.01422 -0.00167 -0.00347 -0.00994 O3 4 0.754585 0.003630 0.746892 11.00000 0.02407 0.01488 = 0.01297 -0.00194 -0.00199 -0.00817 O5 4 0.324947 0.715697 0.868526 11.00000 0.02522 0.01826 = 0.01593 -0.00592 -0.00205 -0.00680 O4 4 0.769564 0.127391 0.854922 11.00000 0.03866 0.01861 = 0.01604 -0.00148 -0.00974 -0.01072 N2 3 0.695138 0.263918 0.702331 11.00000 0.01879 0.01555 = 0.01263 -0.00234 -0.00268 -0.00616 N1 3 0.406172 0.559150 0.659734 11.00000 0.01406 0.01485 = 0.01375 -0.00235 -0.00208 -0.00713 O6 4 0.324603 0.505383 0.991091 11.00000 0.06289 0.03359 = 0.01522 -0.00577 0.00524 -0.02721 C9 1 0.296248 0.486245 0.701417 11.00000 0.01369 0.01088 = 0.01673 -0.00419 0.00138 -0.00435 C8 1 0.411231 0.647107 0.566172 11.00000 0.01412 0.01204 = 0.01411 -0.00416 0.00008 -0.00407 C6 1 0.667967 0.857891 0.439960 11.00000 0.01619 0.01316 = 0.01407 -0.00519 0.00080 -0.00525 C16 1 0.511100 0.531367 0.733058 11.00000 0.01731 0.01456 = 0.01297 -0.00158 -0.00357 -0.00776 AFIX 13 H16 2 0.509110 0.635689 0.735465 11.00000 -1.20000 AFIX 0 C18 1 0.742594 0.130897 0.775442 11.00000 0.01729 0.01627 = 0.01446 -0.00336 -0.00040 -0.00692 C14 1 0.308376 0.425140 0.801343 11.00000 0.01719 0.01328 = 0.01669 -0.00443 -0.00015 -0.00584 C17 1 0.683592 0.416448 0.709442 11.00000 0.01583 0.01545 = 0.01786 -0.00024 -0.00312 -0.00792 AFIX 23 H17A 2 0.729083 0.467368 0.646717 11.00000 -1.20000 H17B 2 0.748574 0.397617 0.761076 11.00000 -1.20000 AFIX 0 C23 1 0.356455 0.560775 0.906501 11.00000 0.02316 0.02228 = 0.01538 -0.00372 -0.00356 -0.01203 C7 1 0.528145 0.812730 0.453101 11.00000 0.01714 0.01462 = 0.01152 -0.00077 -0.00170 -0.00642 AFIX 23 H7A 2 0.427147 0.910180 0.447648 11.00000 -1.20000 H7B 2 0.539496 0.758733 0.401561 11.00000 -1.20000 AFIX 0 C1 1 0.784936 0.784723 0.504176 11.00000 0.02234 0.01597 = 0.01594 -0.00013 -0.00316 -0.00933 AFIX 43 H1 2 0.778009 0.702623 0.559754 11.00000 -1.20000 AFIX 0 C10 1 0.191645 0.467589 0.655987 11.00000 0.01469 0.01561 = 0.01883 -0.00508 -0.00135 -0.00475 AFIX 43 H10 2 0.183061 0.509903 0.587813 11.00000 -1.20000 AFIX 0 C5 1 0.681858 0.976256 0.358137 11.00000 0.02034 0.01626 = 0.01598 -0.00097 -0.00282 -0.00626 AFIX 43 H5 2 0.603348 1.026431 0.313189 11.00000 -1.20000 AFIX 0 C15 1 0.433239 0.459097 0.831470 11.00000 0.01920 0.01561 = 0.01426 -0.00165 -0.00176 -0.00858 AFIX 13 H15 2 0.516357 0.354675 0.862327 11.00000 -1.20000 AFIX 0 C11 1 0.099553 0.384588 0.713847 11.00000 0.01513 0.01928 = 0.02686 -0.00827 -0.00093 -0.00752 AFIX 43 H11 2 0.028290 0.368915 0.684204 11.00000 -1.20000 AFIX 0 C3 1 0.924474 0.949546 0.406667 11.00000 0.01829 0.01931 = 0.02385 -0.00721 0.00259 -0.01009 AFIX 43 H3 2 1.011030 0.981357 0.395727 11.00000 -1.20000 AFIX 0 C19 1 0.760052 -0.143322 0.821608 11.00000 0.01738 0.01356 = 0.01593 -0.00104 -0.00131 -0.00633 C2 1 0.912431 0.830751 0.487760 11.00000 0.02032 0.02045 = 0.02293 -0.00231 -0.00582 -0.00833 AFIX 43 H2A 2 0.991427 0.780411 0.532396 11.00000 -1.20000 AFIX 0 C20 1 0.914841 -0.224134 0.869568 11.00000 0.01917 0.02042 = 0.02270 -0.00095 -0.00458 -0.00659 AFIX 137 H20A 2 1.005994 -0.237004 0.818927 11.00000 -1.50000 H20B 2 0.923949 -0.329622 0.910786 11.00000 -1.50000 H20C 2 0.914452 -0.157915 0.909934 11.00000 -1.50000 AFIX 0 C13 1 0.215016 0.344466 0.858103 11.00000 0.02402 0.01971 = 0.01712 -0.00300 0.00198 -0.01134 AFIX 43 H13 2 0.222733 0.303359 0.926414 11.00000 -1.20000 AFIX 0 C4 1 0.809155 1.021692 0.341559 11.00000 0.02441 0.01742 = 0.01747 -0.00106 0.00204 -0.01049 AFIX 43 H4 2 0.817311 1.102476 0.285428 11.00000 -1.20000 AFIX 0 C12 1 0.109684 0.324436 0.813667 11.00000 0.02102 0.02133 = 0.02614 -0.00601 0.00418 -0.01298 AFIX 43 H12 2 0.044726 0.269546 0.851731 11.00000 -1.20000 AFIX 0 C21 1 0.757075 -0.247970 0.762160 11.00000 0.03125 0.01776 = 0.02879 -0.00551 -0.00889 -0.00867 AFIX 137 H21A 2 0.661534 -0.191352 0.726823 11.00000 -1.50000 H21B 2 0.754624 -0.348036 0.805955 11.00000 -1.50000 H21C 2 0.853139 -0.272259 0.715222 11.00000 -1.50000 AFIX 0 C22 1 0.611199 -0.101800 0.894481 11.00000 0.01989 0.02223 = 0.02602 -0.00163 0.00401 -0.00731 AFIX 137 H22A 2 0.618815 -0.040250 0.935156 11.00000 -1.50000 H22B 2 0.602852 -0.200715 0.936171 11.00000 -1.50000 H22C 2 0.516071 -0.037696 0.859046 11.00000 -1.50000 AFIX 0 C24 1 0.249362 0.817544 0.937453 11.00000 0.02830 0.02817 = 0.02516 -0.01560 0.00140 -0.01087 AFIX 137 H24A 2 0.219200 0.930029 0.902027 11.00000 -1.50000 H24B 2 0.324453 0.790322 0.984276 11.00000 -1.50000 H24C 2 0.153385 0.801066 0.972609 11.00000 -1.50000 AFIX 0 H2 2 0.689112 0.255430 0.647166 11.00000 0.02290 HKLF 4 REM mo_yz001_0m_a.res in P-1 REM R1 = 0.0318 for 4316 Fo > 4sig(Fo) and 0.0353 for all 4715 data REM 297 parameters refined using 0 restraints END WGHT 0.0366 0.4560 REM Highest difference peak 0.323, deepest hole -0.195, 1-sigma level 0.037 Q1 1 0.5959 0.4730 0.7183 11.00000 0.05 0.32 Q2 1 0.3875 0.5213 0.8617 11.00000 0.05 0.32 Q3 1 0.3669 0.4454 0.8220 11.00000 0.05 0.28 Q4 1 0.4733 0.4963 0.7840 11.00000 0.05 0.28 Q5 1 0.5936 0.8364 0.4507 11.00000 0.05 0.27 Q6 1 0.8345 -0.1840 0.8448 11.00000 0.05 0.27 Q7 1 0.6868 -0.1242 0.8571 11.00000 0.05 0.26 Q8 1 0.2763 0.4774 0.7554 11.00000 0.05 0.26 Q9 1 0.4633 0.5448 0.6935 11.00000 0.05 0.25 Q10 1 0.3452 0.5259 0.6777 11.00000 0.05 0.25 Q11 1 0.7391 0.8009 0.4626 11.00000 0.05 0.24 Q12 1 0.7565 -0.2018 0.7956 11.00000 0.05 0.23 Q13 1 0.7206 0.8269 0.4712 11.00000 0.05 0.23 Q14 1 0.6843 0.9026 0.3955 11.00000 0.05 0.23 Q15 1 0.3185 0.4394 0.7465 11.00000 0.05 0.22 Q16 1 0.8410 0.8230 0.4989 11.00000 0.05 0.21 Q17 1 0.1608 0.4172 0.6855 11.00000 0.05 0.21 Q18 1 0.2872 0.3676 0.8238 11.00000 0.05 0.20 Q19 1 0.0968 0.3750 0.7624 11.00000 0.05 0.20 Q20 1 0.2141 0.5106 0.6836 11.00000 0.05 0.20 ; _shelx_res_checksum 86987 _shelx_hkl_file ; -1 0 0 2411.06 48.70 -1 0 0 2376.96 48.60 -1 0 0 2380.26 48.90 -1 0 0 2328.27 49.20 -1 0 0 2231.58 46.90 -1 0 0 2394.66 47.40 -1 0 0 2410.26 47.00 -1 0 0 2274.67 46.90 -1 0 0 2323.97 49.10 1 0 0 2407.76 48.90 1 0 0 2349.67 48.60 1 0 0 2370.06 49.40 1 0 0 2235.48 49.20 1 0 0 2378.16 47.20 1 0 0 2458.45 47.10 1 0 0 2384.16 49.60 1 0 0 2434.86 48.10 1 0 0 2412.56 47.20 1 0 0 2424.06 47.10 -2 0 0 4648.73 92.79 -2 0 0 4709.43 93.09 -2 0 0 4502.45 96.79 -2 0 0 4584.74 96.89 -2 0 0 4798.72 94.19 -2 0 0 4607.14 93.99 -2 0 0 4743.73 92.09 -2 0 0 4575.74 92.19 -2 0 0 4694.63 92.49 -2 0 0 4637.54 96.29 -2 0 0 4608.74 96.99 -2 0 0 4750.62 91.59 2 0 0 4573.14 95.59 2 0 0 4671.73 97.09 2 0 0 4490.55 94.19 2 0 0 4638.34 94.09 2 0 0 4741.53 92.49 2 0 0 4620.54 93.79 2 0 0 4665.73 93.89 2 0 0 4692.13 91.99 2 0 0 4830.92 93.59 2 0 0 4602.34 91.99 2 0 0 4752.92 91.49 2 0 0 4522.85 96.79 -3 0 0 424.46 9.10 -3 0 0 416.66 8.40 -3 0 0 418.06 8.60 -3 0 0 412.96 9.50 -3 0 0 422.66 8.90 -3 0 0 425.56 9.50 -3 0 0 434.56 9.30 -3 0 0 412.76 9.20 -3 0 0 406.46 9.00 -3 0 0 401.66 9.40 -3 0 0 409.56 9.10 3 0 0 409.96 9.30 3 0 0 397.36 9.70 3 0 0 416.36 8.40 3 0 0 423.86 9.30 3 0 0 426.46 9.10 3 0 0 430.76 8.90 3 0 0 421.16 8.90 3 0 0 420.56 9.30 3 0 0 422.66 9.30 3 0 0 418.36 8.90 3 0 0 406.36 9.50 -4 0 0 297.67 6.80 -4 0 0 287.87 7.10 -4 0 0 284.07 7.10 -4 0 0 303.37 7.30 -4 0 0 297.77 7.20 -4 0 0 295.47 7.00 -4 0 0 303.47 6.40 -4 0 0 284.57 7.20 -4 0 0 292.27 6.00 4 0 0 302.67 7.20 4 0 0 284.77 7.10 4 0 0 286.37 7.70 4 0 0 291.67 7.20 4 0 0 301.97 6.80 4 0 0 297.17 6.80 4 0 0 315.37 7.10 4 0 0 288.77 7.50 -5 0 0 445.06 10.70 -5 0 0 483.55 10.30 -5 0 0 472.85 9.80 -5 0 0 451.85 11.00 -5 0 0 480.55 11.20 -5 0 0 462.85 10.60 -5 0 0 461.85 10.80 -5 0 0 485.85 11.00 5 0 0 455.05 11.60 5 0 0 469.45 11.00 5 0 0 462.05 10.30 5 0 0 462.75 10.30 5 0 0 484.65 11.00 5 0 0 470.85 11.00 5 0 0 438.16 11.30 -6 0 0 34.20 2.10 -6 0 0 24.50 1.80 -6 0 0 28.00 1.90 -6 0 0 27.10 1.20 -6 0 0 24.50 1.60 -6 0 0 30.00 2.00 -6 0 0 27.40 1.90 -6 0 0 31.20 2.00 6 0 0 31.60 2.40 6 0 0 25.10 1.80 6 0 0 27.40 2.20 6 0 0 25.50 1.90 6 0 0 27.70 2.30 6 0 0 28.40 2.00 6 0 0 25.30 1.60 -7 0 0 187.48 5.80 -7 0 0 180.18 5.80 -7 0 0 180.58 5.90 -7 0 0 193.68 6.50 -7 0 0 181.38 5.90 -7 0 0 180.28 5.70 7 0 0 171.98 6.40 7 0 0 180.78 5.00 7 0 0 177.68 6.40 7 0 0 180.88 5.70 7 0 0 184.78 6.90 7 0 0 183.78 5.80 -8 0 0 52.89 3.00 -8 0 0 57.59 3.20 -8 0 0 48.60 3.00 -8 0 0 49.50 3.00 8 0 0 47.30 2.90 8 0 0 46.60 3.60 8 0 0 53.99 3.90 8 0 0 50.89 2.40 8 0 0 51.29 3.40 -9 0 0 115.79 5.00 -9 0 0 113.19 4.80 -9 0 0 115.59 5.00 -9 0 0 119.69 5.00 9 0 0 123.89 5.70 9 0 0 111.79 5.60 9 0 0 113.59 5.90 -10 0 0 104.99 4.70 -10 0 0 96.99 4.80 -10 0 0 101.99 4.90 -10 0 0 104.79 4.90 -10 0 0 107.39 5.60 10 0 0 101.59 5.70 10 0 0 87.49 5.70 10 0 0 97.89 5.40 10 -1 0 194.48 8.40 10 -1 0 210.88 8.90 10 -1 0 211.98 8.60 -10 1 0 216.78 7.80 -10 1 0 213.18 7.90 -10 1 0 210.98 7.50 -10 1 0 211.38 7.80 9 -1 0 2.30 1.40 9 -1 0 1.40 1.40 9 -1 0 6.90 2.20 -9 1 0 1.40 1.20 -9 1 0 4.40 1.40 -9 1 0 3.00 1.60 -9 1 0 1.30 1.20 8 -1 0 27.20 3.00 8 -1 0 29.90 2.00 8 -1 0 29.20 3.20 8 -1 0 21.70 2.80 -8 1 0 26.20 2.60 -8 1 0 31.40 3.00 -8 1 0 30.80 2.80 -8 1 0 31.00 2.50 7 -1 0 136.69 4.50 7 -1 0 131.39 5.70 7 -1 0 124.09 5.30 7 -1 0 126.19 4.90 7 -1 0 130.79 4.30 7 -1 0 138.09 5.60 -7 1 0 129.99 4.80 -7 1 0 122.39 4.70 -7 1 0 131.99 5.00 -7 1 0 133.39 5.10 6 -1 0 152.48 5.70 6 -1 0 161.78 5.30 6 -1 0 161.88 3.70 6 -1 0 167.88 5.30 6 -1 0 156.88 5.70 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-0.50 0.70 -2 3 0 -0.40 0.60 -2 3 0 -0.40 0.60 1 -3 0 37.10 1.60 1 -3 0 37.60 1.90 1 -3 0 37.30 1.90 1 -3 0 35.30 1.90 1 -3 0 40.50 1.80 1 -3 0 36.30 2.00 1 -3 0 40.60 1.80 1 -3 0 34.40 1.90 1 -3 0 37.40 1.20 1 -3 0 35.80 1.30 1 -3 0 39.60 1.90 1 -3 0 36.50 1.90 -1 3 0 36.10 1.90 -1 3 0 36.40 1.90 -1 3 0 35.10 1.90 -1 3 0 35.60 1.90 -1 3 0 37.50 1.60 -1 3 0 38.40 1.90 -1 3 0 36.00 1.80 -1 3 0 35.70 1.80 -1 3 0 38.50 1.90 -1 3 0 32.80 1.80 0 -3 0 138.09 3.90 0 -3 0 143.69 3.50 0 -3 0 137.69 4.10 0 -3 0 137.69 4.00 0 -3 0 128.79 3.90 0 -3 0 139.09 3.70 0 -3 0 139.69 4.10 0 -3 0 140.29 4.00 0 -3 0 136.99 3.50 0 -3 0 137.39 4.00 0 3 0 142.89 3.70 0 3 0 143.39 4.00 0 3 0 137.59 4.00 0 3 0 139.09 4.00 0 3 0 139.89 3.40 0 3 0 133.89 3.90 0 3 0 142.99 4.10 0 3 0 143.89 3.50 0 3 0 136.99 4.00 0 3 0 139.09 3.80 -1 -3 0 142.89 4.10 -1 -3 0 158.28 4.10 -1 -3 0 158.58 4.30 -1 -3 0 154.98 3.60 -1 -3 0 153.38 4.00 -1 -3 0 150.48 4.10 -1 -3 0 156.68 4.00 -1 -3 0 149.29 4.10 -1 -3 0 158.08 4.20 -1 -3 0 152.08 4.20 1 3 0 150.18 4.00 1 3 0 158.68 4.20 1 3 0 151.68 3.70 1 3 0 145.09 3.90 1 3 0 154.18 4.20 1 3 0 151.58 4.10 1 3 0 143.59 4.10 1 3 0 150.58 4.00 1 3 0 152.28 4.10 1 3 0 156.98 4.00 -2 -3 0 265.07 5.50 -2 -3 0 261.47 6.40 -2 -3 0 271.37 6.30 -2 -3 0 264.47 6.20 -2 -3 0 268.57 6.40 -2 -3 0 256.27 6.30 -2 -3 0 258.47 6.50 -2 -3 0 265.67 6.30 -2 -3 0 272.77 6.60 -2 -3 0 270.17 6.40 -2 -3 0 273.47 6.30 2 3 0 254.27 6.30 2 3 0 268.27 6.40 2 3 0 266.87 5.50 2 3 0 259.07 6.30 2 3 0 266.97 6.60 2 3 0 271.57 5.60 2 3 0 267.47 6.30 2 3 0 265.57 6.10 2 3 0 260.77 6.10 -3 -3 0 16.40 1.10 -3 -3 0 14.00 1.10 -3 -3 0 15.40 1.10 -3 -3 0 13.50 1.10 -3 -3 0 17.80 1.50 -3 -3 0 13.80 1.10 -3 -3 0 18.20 1.20 -3 -3 0 14.20 1.10 -3 -3 0 16.10 0.70 3 3 0 13.90 1.00 3 3 0 14.60 1.00 3 3 0 12.70 1.40 3 3 0 16.00 1.20 3 3 0 16.10 1.00 3 3 0 15.90 1.40 3 3 0 15.50 1.10 3 3 0 14.70 1.20 3 3 0 14.90 1.30 3 3 0 14.50 1.10 -4 -3 0 1166.78 24.20 -4 -3 0 1099.99 24.10 -4 -3 0 1111.59 24.70 -4 -3 0 1182.68 23.70 -4 -3 0 1167.58 24.60 -4 -3 0 1140.39 24.60 -4 -3 0 1180.28 23.20 -4 -3 0 1193.48 22.70 -4 -3 0 1139.09 23.60 -4 -3 0 1183.98 23.70 4 3 0 1171.18 24.10 4 3 0 1175.18 26.20 4 3 0 1198.18 23.40 4 3 0 1172.58 24.00 4 3 0 1122.39 25.10 4 3 0 1165.18 23.30 4 3 0 1159.78 24.30 -5 -3 0 112.19 3.50 -5 -3 0 111.39 3.40 -5 -3 0 108.09 3.40 -5 -3 0 107.39 3.90 -5 -3 0 113.79 3.50 -5 -3 0 111.49 3.10 -5 -3 0 111.89 3.50 -5 -3 0 114.49 3.50 -5 -3 0 114.19 2.80 -5 -3 0 112.39 3.10 5 3 0 114.09 2.80 5 3 0 110.79 3.40 5 3 0 110.59 3.00 5 3 0 112.49 3.40 5 3 0 105.69 4.10 5 3 0 105.99 4.30 5 3 0 104.69 4.00 5 3 0 114.89 3.00 5 3 0 114.69 3.50 -6 -3 0 228.18 6.80 -6 -3 0 225.98 5.90 -6 -3 0 227.78 5.40 -6 -3 0 215.38 6.00 -6 -3 0 217.18 6.10 -6 -3 0 232.18 6.10 -6 -3 0 229.58 5.80 -6 -3 0 223.58 6.20 -6 -3 0 229.68 5.30 6 3 0 230.48 5.90 6 3 0 232.38 5.30 6 3 0 217.88 6.80 6 3 0 218.18 7.20 6 3 0 234.88 5.80 6 3 0 230.68 6.10 6 3 0 228.18 5.30 6 3 0 226.68 5.30 6 3 0 212.58 6.60 -7 -3 0 61.19 2.80 -7 -3 0 67.09 2.80 -7 -3 0 63.19 1.80 -7 -3 0 61.99 2.80 -7 -3 0 60.29 3.30 -7 -3 0 66.09 2.80 -7 -3 0 62.29 2.40 -7 -3 0 65.19 2.80 7 3 0 61.99 2.80 7 3 0 62.19 2.10 7 3 0 62.09 3.40 7 3 0 57.89 2.30 7 3 0 61.29 3.30 7 3 0 59.89 2.00 7 3 0 66.19 2.50 7 3 0 61.69 3.70 -8 -3 0 35.00 2.70 -8 -3 0 35.50 2.30 -8 -3 0 37.60 2.30 -8 -3 0 41.50 2.40 -8 -3 0 36.20 2.40 -8 -3 0 38.40 2.00 8 3 0 37.10 2.30 8 3 0 40.00 3.00 8 3 0 40.10 1.50 8 3 0 38.20 3.20 8 3 0 38.10 3.10 -9 -3 0 161.78 5.40 -9 -3 0 156.28 4.90 -9 -3 0 163.18 6.30 -9 -3 0 156.28 5.30 -9 -3 0 156.78 5.50 9 3 0 154.78 6.40 9 3 0 153.18 6.90 9 3 0 155.88 6.20 -10 -3 0 1.60 1.00 -10 -3 0 1.10 1.00 -10 -3 0 1.80 1.10 -10 -3 0 1.60 1.30 10 3 0 2.30 1.50 10 3 0 0.80 1.60 10 3 0 -0.40 1.50 -11 -3 0 16.60 2.70 -11 -3 0 16.30 2.10 -11 -3 0 15.30 2.10 11 3 0 21.80 3.00 11 3 0 20.00 3.00 11 3 0 13.50 2.80 8 -4 0 8.60 2.30 8 -4 0 12.10 2.60 8 -4 0 10.20 2.40 -8 4 0 12.40 2.30 -8 4 0 6.50 1.80 -8 4 0 11.40 2.20 -8 4 0 8.00 2.10 7 -4 0 53.69 4.00 7 -4 0 56.89 4.00 7 -4 0 55.89 3.40 -7 4 0 56.69 3.70 -7 4 0 63.39 4.00 -7 4 0 63.59 4.00 -7 4 0 60.49 4.00 6 -4 0 126.89 5.00 6 -4 0 124.99 5.50 6 -4 0 133.59 5.80 6 -4 0 130.69 5.70 -6 4 0 134.09 5.50 -6 4 0 132.19 5.60 -6 4 0 127.69 5.50 -6 4 0 127.89 5.40 5 -4 0 25.00 2.80 5 -4 0 26.20 2.70 5 -4 0 23.90 2.60 -5 4 0 20.30 2.20 -5 4 0 24.50 2.50 -5 4 0 19.30 2.30 -5 4 0 25.20 1.90 -5 4 0 24.60 2.50 4 -4 0 33.00 2.90 4 -4 0 26.70 2.60 4 -4 0 29.00 2.30 4 -4 0 23.80 2.40 4 -4 0 28.50 1.10 4 -4 0 29.90 2.70 -4 4 0 31.90 2.50 -4 4 0 28.90 2.60 -4 4 0 31.30 2.80 -4 4 0 31.80 2.40 -4 4 0 26.10 2.00 -4 4 0 31.50 2.70 3 -4 0 19.00 2.00 3 -4 0 15.30 1.80 3 -4 0 15.70 1.80 3 -4 0 16.40 1.90 3 -4 0 17.90 0.90 3 -4 0 19.00 1.90 -3 4 0 17.70 1.70 -3 4 0 18.70 1.90 -3 4 0 18.60 2.00 -3 4 0 21.00 2.00 -3 4 0 17.50 1.90 -3 4 0 17.00 1.90 2 -4 0 3.10 1.00 2 -4 0 4.40 1.00 2 -4 0 4.40 1.10 2 -4 0 3.70 0.60 2 -4 0 5.90 1.20 2 -4 0 4.60 1.10 -2 4 0 3.60 1.00 -2 4 0 4.60 1.00 -2 4 0 4.00 1.00 -2 4 0 3.80 1.00 -2 4 0 5.70 1.10 -2 4 0 5.30 1.10 1 -4 0 195.08 5.60 1 -4 0 186.38 5.50 1 -4 0 201.18 4.50 1 -4 0 197.48 5.10 1 -4 0 201.68 5.70 1 -4 0 193.68 5.80 1 -4 0 196.98 4.70 1 -4 0 194.78 5.80 1 -4 0 176.28 5.60 -1 4 0 186.58 5.60 -1 4 0 187.88 5.40 -1 4 0 195.58 5.80 -1 4 0 197.08 5.80 -1 4 0 199.88 5.10 -1 4 0 196.08 5.50 -1 4 0 187.28 5.50 0 -4 0 297.07 7.70 0 -4 0 307.77 8.00 0 -4 0 313.47 7.80 0 -4 0 309.97 7.10 0 -4 0 324.67 7.40 0 -4 0 305.77 7.90 0 -4 0 305.97 7.90 0 -4 0 308.07 7.80 0 -4 0 305.37 7.10 0 -4 0 316.57 8.00 0 4 0 307.17 7.40 0 4 0 299.57 7.80 0 4 0 317.57 8.00 0 4 0 318.27 7.10 0 4 0 305.77 7.70 0 4 0 315.77 7.90 0 4 0 316.07 7.80 0 4 0 312.57 7.20 0 4 0 315.57 7.70 -1 -4 0 0.50 0.60 -1 -4 0 0.30 0.50 -1 -4 0 1.40 0.50 -1 -4 0 1.20 0.70 -1 -4 0 1.50 0.70 -1 -4 0 1.10 0.40 -1 -4 0 0.90 0.60 -1 -4 0 1.30 0.60 -1 -4 0 1.40 0.70 -1 -4 0 -0.60 0.60 -1 -4 0 -0.50 0.60 1 4 0 0.90 0.60 1 4 0 1.30 0.60 1 4 0 1.50 0.70 1 4 0 1.90 0.80 1 4 0 0.00 0.60 1 4 0 0.90 0.60 1 4 0 0.40 0.60 1 4 0 0.80 0.60 1 4 0 0.80 0.70 1 4 0 0.90 0.60 1 4 0 1.00 0.60 -2 -4 0 63.89 2.50 -2 -4 0 66.79 1.90 -2 -4 0 60.79 2.50 -2 -4 0 59.79 2.50 -2 -4 0 64.89 2.60 -2 -4 0 62.09 2.40 -2 -4 0 65.89 2.40 -2 -4 0 67.89 2.60 -2 -4 0 64.49 2.50 -2 -4 0 65.69 2.50 2 4 0 61.49 1.90 2 4 0 66.09 2.60 2 4 0 64.89 2.50 2 4 0 64.69 2.50 2 4 0 63.79 2.60 2 4 0 61.09 2.50 2 4 0 61.79 2.60 2 4 0 67.39 2.50 2 4 0 62.49 2.40 -3 -4 0 7.30 1.10 -3 -4 0 6.40 1.00 -3 -4 0 6.40 1.00 -3 -4 0 3.30 0.80 -3 -4 0 6.10 0.40 -3 -4 0 5.70 0.90 -3 -4 0 6.70 0.90 -3 -4 0 6.00 1.00 -3 -4 0 4.60 0.80 3 4 0 5.10 0.80 3 4 0 6.20 1.10 3 4 0 6.20 1.10 3 4 0 5.30 0.90 3 4 0 5.60 0.50 3 4 0 7.60 1.00 3 4 0 6.50 0.90 3 4 0 6.60 0.80 3 4 0 5.70 1.10 -4 -4 0 219.78 5.70 -4 -4 0 219.98 5.80 -4 -4 0 227.28 5.90 -4 -4 0 237.48 5.80 -4 -4 0 219.88 6.30 -4 -4 0 224.38 5.90 -4 -4 0 220.18 6.20 -4 -4 0 231.88 5.80 -4 -4 0 208.78 5.90 4 4 0 225.08 5.80 4 4 0 226.38 5.50 4 4 0 238.08 6.70 4 4 0 225.88 6.10 4 4 0 226.38 5.40 4 4 0 229.48 6.20 4 4 0 226.58 5.90 4 4 0 227.18 6.50 -5 -4 0 138.89 4.20 -5 -4 0 130.09 4.10 -5 -4 0 135.89 3.90 -5 -4 0 134.29 4.20 -5 -4 0 139.69 4.10 -5 -4 0 140.69 4.20 -5 -4 0 147.59 3.40 -5 -4 0 136.69 4.70 5 4 0 135.59 4.20 5 4 0 144.69 4.10 5 4 0 138.79 3.70 5 4 0 135.39 5.00 5 4 0 136.19 4.60 5 4 0 132.79 3.60 5 4 0 141.39 4.20 5 4 0 129.69 4.80 -6 -4 0 91.49 3.30 -6 -4 0 88.39 2.70 -6 -4 0 87.69 3.30 -6 -4 0 84.79 3.70 -6 -4 0 93.09 3.00 -6 -4 0 91.49 2.20 -6 -4 0 86.89 3.20 -6 -4 0 88.59 3.20 -6 -4 0 94.89 3.40 6 4 0 90.89 2.70 6 4 0 96.39 3.20 6 4 0 90.89 3.80 6 4 0 90.99 4.00 6 4 0 86.59 3.20 6 4 0 91.69 2.70 6 4 0 86.69 4.10 -7 -4 0 206.08 6.00 -7 -4 0 205.48 5.20 -7 -4 0 210.98 6.10 -7 -4 0 210.08 6.00 -7 -4 0 210.38 6.10 -7 -4 0 208.68 5.90 -7 -4 0 220.38 5.50 -7 -4 0 210.58 4.90 -7 -4 0 198.58 6.70 7 4 0 199.38 7.30 7 4 0 195.38 5.60 7 4 0 213.88 7.10 7 4 0 207.08 4.90 7 4 0 215.18 5.00 7 4 0 209.18 6.80 7 4 0 223.78 6.10 -8 -4 0 168.88 5.50 -8 -4 0 170.58 4.50 -8 -4 0 163.68 5.30 -8 -4 0 174.08 5.40 -8 -4 0 169.68 5.50 -8 -4 0 168.88 6.20 8 4 0 168.58 6.90 8 4 0 174.28 5.40 8 4 0 174.88 4.00 8 4 0 169.78 4.90 8 4 0 160.98 6.30 8 4 0 166.78 6.30 -9 -4 0 125.19 4.60 -9 -4 0 118.19 5.40 -9 -4 0 131.79 4.80 -9 -4 0 131.79 4.90 9 4 0 120.69 6.10 9 4 0 134.79 5.80 9 4 0 129.59 5.70 -10 -4 0 24.90 2.30 -10 -4 0 29.30 3.30 -10 -4 0 28.00 2.60 -10 -4 0 24.80 2.40 10 4 0 31.10 3.40 10 4 0 32.80 3.40 10 4 0 18.60 3.00 -11 -4 0 -0.60 1.40 -11 -4 0 1.30 1.10 -11 -4 0 -0.70 0.90 11 4 0 3.30 1.80 11 4 0 2.80 1.50 11 4 0 -1.60 1.20 7 -5 0 1.70 1.60 7 -5 0 3.00 1.90 7 -5 0 1.60 1.30 -7 5 0 3.30 1.70 -7 5 0 2.60 1.70 -7 5 0 3.10 1.50 -7 5 0 0.30 1.30 6 -5 0 45.00 3.50 6 -5 0 54.09 3.40 6 -5 0 50.59 3.80 6 -5 0 46.60 3.60 -6 5 0 48.60 3.60 -6 5 0 46.20 3.60 -6 5 0 47.80 3.50 -6 5 0 47.40 3.60 5 -5 0 104.79 4.90 5 -5 0 96.09 4.80 5 -5 0 100.89 4.90 -5 5 0 92.69 4.60 -5 5 0 94.09 4.70 -5 5 0 92.19 4.60 -5 5 0 95.59 4.70 4 -5 0 11.10 1.80 4 -5 0 9.00 1.80 4 -5 0 11.40 1.90 4 -5 0 14.20 2.10 -4 5 0 14.70 1.80 -4 5 0 12.40 2.00 -4 5 0 11.50 1.90 -4 5 0 10.20 1.80 -4 5 0 14.70 2.00 3 -5 0 50.79 3.00 3 -5 0 44.00 1.60 3 -5 0 45.90 2.80 3 -5 0 42.70 2.90 3 -5 0 49.10 3.00 3 -5 0 46.00 2.90 -3 5 0 38.40 2.80 -3 5 0 38.10 2.80 -3 5 0 41.60 2.80 -3 5 0 44.10 2.60 -3 5 0 43.30 2.90 -3 5 0 43.10 2.80 2 -5 0 4.90 1.30 2 -5 0 1.30 0.90 2 -5 0 2.10 1.00 2 -5 0 2.70 0.60 2 -5 0 3.30 1.00 2 -5 0 2.40 1.00 -2 5 0 2.40 1.00 -2 5 0 -1.00 0.60 -2 5 0 2.30 1.00 -2 5 0 2.30 0.70 -2 5 0 2.70 1.00 -2 5 0 3.10 1.10 -2 5 0 1.10 0.90 1 -5 0 176.88 5.50 1 -5 0 193.18 6.10 1 -5 0 170.08 5.70 1 -5 0 170.58 5.70 1 -5 0 174.48 5.60 1 -5 0 183.58 4.30 1 -5 0 169.78 4.50 -1 5 0 181.58 4.80 -1 5 0 174.88 5.50 -1 5 0 174.58 5.70 -1 5 0 175.68 5.60 -1 5 0 167.08 5.60 -1 5 0 171.98 5.30 -1 5 0 168.38 5.40 0 -5 0 29.60 2.10 0 -5 0 24.90 1.90 0 -5 0 27.50 2.00 0 -5 0 25.20 1.80 0 -5 0 26.80 1.90 0 -5 0 26.00 1.30 0 -5 0 31.00 2.10 0 -5 0 27.40 1.40 0 5 0 25.10 1.90 0 5 0 28.30 2.00 0 5 0 25.50 2.00 0 5 0 23.30 1.80 0 5 0 27.80 1.50 0 5 0 25.40 1.70 0 5 0 28.00 1.90 -1 -5 0 245.18 6.80 -1 -5 0 240.28 6.60 -1 -5 0 239.38 5.90 -1 -5 0 242.68 6.70 -1 -5 0 230.08 5.50 -1 -5 0 222.48 6.50 -1 -5 0 234.78 6.70 -1 -5 0 234.08 6.50 1 5 0 227.48 5.90 1 5 0 232.88 6.10 1 5 0 224.48 6.30 1 5 0 244.08 6.70 1 5 0 241.18 6.60 1 5 0 242.48 6.70 1 5 0 229.68 6.60 -2 -5 0 1.00 0.80 -2 -5 0 1.70 0.80 -2 -5 0 1.60 0.70 -2 -5 0 1.40 0.50 -2 -5 0 2.80 0.80 -2 -5 0 1.50 0.70 -2 -5 0 1.20 0.80 -2 -5 0 0.80 0.70 -2 -5 0 1.60 0.80 2 5 0 0.30 0.60 2 5 0 0.90 0.70 2 5 0 1.50 0.70 2 5 0 0.70 0.50 2 5 0 2.60 0.80 2 5 0 1.40 0.90 2 5 0 1.20 0.70 -3 -5 0 0.30 0.60 -3 -5 0 -0.10 0.60 -3 -5 0 -0.20 0.30 -3 -5 0 0.40 0.60 -3 -5 0 1.10 0.60 -3 -5 0 -0.80 0.50 -3 -5 0 -0.40 0.60 -3 -5 0 0.20 0.50 3 5 0 0.00 0.60 3 5 0 0.10 0.30 3 5 0 -0.50 0.60 3 5 0 1.00 0.60 3 5 0 0.20 0.50 3 5 0 0.90 0.80 3 5 0 0.60 0.60 3 5 0 -0.10 0.60 3 5 0 0.00 0.40 -4 -5 0 66.59 3.00 -4 -5 0 68.69 2.80 -4 -5 0 66.19 2.70 -4 -5 0 62.09 2.70 -4 -5 0 60.79 3.00 -4 -5 0 64.39 2.80 -4 -5 0 69.09 2.80 4 5 0 63.29 3.10 4 5 0 64.39 2.90 4 5 0 67.89 2.70 4 5 0 67.89 2.50 4 5 0 71.49 3.20 4 5 0 66.19 2.80 4 5 0 66.29 1.70 -5 -5 0 70.69 3.30 -5 -5 0 83.29 3.10 -5 -5 0 81.99 3.10 -5 -5 0 78.89 3.40 -5 -5 0 75.69 3.10 -5 -5 0 76.09 3.00 -5 -5 0 72.29 3.00 5 5 0 76.49 3.60 5 5 0 77.99 3.10 5 5 0 78.59 3.60 5 5 0 76.29 3.40 5 5 0 75.89 3.20 5 5 0 79.39 2.70 5 5 0 85.99 3.10 -6 -5 0 105.29 4.40 -6 -5 0 114.69 3.90 -6 -5 0 115.49 4.10 -6 -5 0 109.99 3.90 -6 -5 0 117.79 4.00 -6 -5 0 116.39 4.00 -6 -5 0 110.29 2.80 6 5 0 106.09 4.70 6 5 0 110.39 4.00 6 5 0 116.49 3.80 6 5 0 116.39 4.00 6 5 0 111.29 3.40 6 5 0 118.59 3.30 6 5 0 115.89 4.50 6 5 0 105.99 4.70 -7 -5 0 5.80 1.10 -7 -5 0 8.10 1.30 -7 -5 0 6.20 1.40 -7 -5 0 7.20 1.30 -7 -5 0 8.70 1.30 -7 -5 0 7.00 1.20 -7 -5 0 7.70 0.90 7 5 0 5.60 1.20 7 5 0 6.90 0.90 7 5 0 6.30 1.70 7 5 0 7.60 0.90 7 5 0 5.70 1.40 7 5 0 5.30 1.50 7 5 0 6.50 1.10 -8 -5 0 2.10 1.20 -8 -5 0 2.20 0.90 -8 -5 0 3.00 1.00 -8 -5 0 0.70 0.80 8 5 0 2.10 0.50 8 5 0 2.10 0.90 8 5 0 1.80 1.30 8 5 0 3.10 1.30 8 5 0 2.10 1.30 -9 -5 0 4.70 1.20 -9 -5 0 5.20 1.20 -9 -5 0 5.30 1.20 -9 -5 0 4.60 1.60 9 5 0 6.40 1.90 9 5 0 4.10 1.50 9 5 0 3.20 1.50 -10 -5 0 3.10 1.60 -10 -5 0 2.10 1.10 -10 -5 0 3.80 1.20 -10 -5 0 3.00 1.20 10 5 0 1.50 1.60 10 5 0 2.50 1.60 10 5 0 2.00 1.60 -11 -5 0 41.90 3.10 -11 -5 0 40.20 4.00 -11 -5 0 44.90 3.00 11 5 0 49.60 3.90 11 5 0 44.60 4.80 11 5 0 30.60 3.60 6 -6 0 -0.30 1.60 6 -6 0 1.20 1.60 6 -6 0 -0.10 1.10 6 -6 0 0.20 1.30 -6 6 0 0.90 1.50 -6 6 0 1.80 1.60 -6 6 0 1.80 1.40 -6 6 0 0.30 1.40 5 -6 0 1.10 1.50 5 -6 0 -1.60 1.10 5 -6 0 -2.20 1.00 5 -6 0 0.10 1.30 -5 6 0 2.10 1.60 -5 6 0 0.50 1.30 -5 6 0 1.40 1.30 -5 6 0 0.70 1.40 4 -6 0 241.08 8.50 4 -6 0 248.58 8.50 4 -6 0 248.38 8.10 4 -6 0 254.47 8.40 -4 6 0 235.68 8.20 -4 6 0 241.98 8.40 -4 6 0 237.18 8.10 -4 6 0 255.47 8.10 3 -6 0 38.50 3.10 3 -6 0 35.40 2.80 3 -6 0 36.20 2.80 3 -6 0 37.50 3.00 -3 6 0 38.20 3.00 -3 6 0 34.90 2.60 -3 6 0 38.30 3.00 -3 6 0 38.10 3.00 -3 6 0 39.90 2.90 2 -6 0 10.50 1.80 2 -6 0 10.10 1.80 2 -6 0 17.40 1.20 2 -6 0 18.70 2.20 2 -6 0 13.30 1.80 2 -6 0 14.30 2.00 -2 6 0 13.30 2.00 -2 6 0 14.80 2.00 -2 6 0 13.70 1.90 -2 6 0 15.70 2.10 -2 6 0 14.30 2.00 1 -6 0 64.29 2.50 1 -6 0 62.99 3.40 1 -6 0 62.59 3.30 1 -6 0 60.19 3.30 1 -6 0 59.19 3.30 1 -6 0 61.39 3.40 -1 6 0 63.69 3.20 -1 6 0 63.19 3.10 -1 6 0 57.29 3.20 -1 6 0 63.09 3.30 -1 6 0 62.89 3.40 0 -6 0 288.77 8.00 0 -6 0 281.87 8.30 0 -6 0 276.87 8.30 0 -6 0 281.17 8.30 0 -6 0 299.17 8.30 0 -6 0 287.27 8.20 0 -6 0 290.77 6.90 0 6 0 278.37 7.60 0 6 0 288.47 8.20 0 6 0 277.67 8.10 0 6 0 283.57 8.00 0 6 0 287.57 8.20 0 6 0 293.17 7.20 -1 -6 0 93.69 3.90 -1 -6 0 94.29 3.90 -1 -6 0 90.89 3.70 -1 -6 0 96.69 4.00 -1 -6 0 92.19 3.90 -1 -6 0 95.99 2.80 -1 -6 0 97.29 3.40 -1 -6 0 104.49 4.00 1 6 0 90.59 3.80 1 6 0 96.39 3.80 1 6 0 92.99 3.90 1 6 0 97.89 3.40 1 6 0 100.89 3.90 1 6 0 95.39 3.40 -2 -6 0 118.69 4.50 -2 -6 0 128.29 4.60 -2 -6 0 120.39 4.40 -2 -6 0 130.99 4.50 -2 -6 0 122.59 4.50 -2 -6 0 121.59 4.40 -2 -6 0 127.59 3.60 2 6 0 121.19 3.70 2 6 0 119.89 4.20 2 6 0 118.49 4.60 2 6 0 120.59 4.40 2 6 0 118.79 4.20 2 6 0 127.19 4.10 2 6 0 126.19 4.40 -3 -6 0 40.10 2.40 -3 -6 0 42.30 2.50 -3 -6 0 46.20 1.70 -3 -6 0 48.40 2.50 -3 -6 0 44.50 2.50 -3 -6 0 46.70 2.70 -3 -6 0 43.60 2.40 3 6 0 44.60 2.40 3 6 0 46.60 1.80 3 6 0 42.20 2.30 3 6 0 44.60 2.60 3 6 0 48.00 2.50 3 6 0 43.40 2.60 3 6 0 45.50 2.50 -4 -6 0 57.59 2.80 -4 -6 0 61.79 1.60 -4 -6 0 57.19 2.90 -4 -6 0 62.69 3.10 -4 -6 0 55.99 2.80 -4 -6 0 55.89 2.90 4 6 0 59.69 3.10 4 6 0 60.49 1.80 4 6 0 63.19 2.90 4 6 0 59.39 3.00 4 6 0 56.69 2.60 4 6 0 64.89 3.10 4 6 0 60.39 2.80 4 6 0 58.99 3.00 -5 -6 0 3.30 0.90 -5 -6 0 4.30 1.20 -5 -6 0 4.00 1.00 -5 -6 0 5.30 1.00 -5 -6 0 4.80 1.10 -5 -6 0 5.40 1.30 -5 -6 0 6.50 1.20 5 6 0 3.60 0.90 5 6 0 3.10 0.80 5 6 0 3.90 1.20 5 6 0 4.60 1.10 5 6 0 3.70 1.10 5 6 0 5.50 1.30 5 6 0 5.20 0.90 -6 -6 0 12.10 1.50 -6 -6 0 11.00 1.50 -6 -6 0 12.80 1.60 -6 -6 0 10.60 1.70 -6 -6 0 11.10 1.40 -6 -6 0 10.90 1.60 -6 -6 0 12.90 1.60 6 6 0 9.70 1.30 6 6 0 11.40 1.90 6 6 0 10.90 1.60 6 6 0 12.40 1.30 6 6 0 13.60 2.00 6 6 0 14.40 1.90 6 6 0 12.70 1.40 -7 -6 0 1.00 0.80 -7 -6 0 -1.20 0.60 -7 -6 0 1.20 1.00 -7 -6 0 0.40 0.80 -7 -6 0 -0.80 0.80 -7 -6 0 0.20 0.70 7 6 0 0.50 0.90 7 6 0 0.00 0.90 7 6 0 1.30 0.80 7 6 0 0.70 0.90 7 6 0 -0.50 1.20 7 6 0 0.00 0.60 -8 -6 0 70.09 3.90 -8 -6 0 72.59 3.40 -8 -6 0 75.09 3.40 -8 -6 0 70.89 3.50 8 6 0 72.29 4.30 8 6 0 67.49 4.10 8 6 0 69.09 4.00 8 6 0 73.99 3.50 -9 -6 0 85.79 3.90 -9 -6 0 81.39 4.60 -9 -6 0 94.49 4.00 -9 -6 0 90.59 4.10 9 6 0 77.99 4.90 9 6 0 89.49 4.80 9 6 0 88.29 4.90 9 6 0 88.19 3.80 -10 -6 0 17.10 2.00 -10 -6 0 16.50 2.10 -10 -6 0 10.60 2.20 -10 -6 0 12.80 1.90 10 6 0 21.70 3.30 10 6 0 18.40 2.80 10 6 0 19.80 3.00 -11 -6 0 7.80 1.60 -11 -6 0 6.40 1.90 -11 -6 0 6.50 1.50 11 6 0 8.20 2.40 11 6 0 9.90 2.70 11 6 0 9.80 2.30 5 -7 0 1.00 1.50 5 -7 0 -2.10 1.20 5 -7 0 0.30 1.20 5 -7 0 0.70 1.50 -5 7 0 1.30 1.60 -5 7 0 1.50 1.40 -5 7 0 -0.20 1.30 -5 7 0 -1.30 1.40 4 -7 0 23.50 2.80 4 -7 0 20.90 2.90 4 -7 0 19.80 2.80 4 -7 0 22.50 3.00 -4 7 0 19.70 2.80 -4 7 0 20.50 2.80 -4 7 0 20.10 2.70 -4 7 0 23.30 3.00 3 -7 0 48.50 3.50 3 -7 0 46.40 3.50 3 -7 0 43.40 3.30 3 -7 0 45.70 3.50 -3 7 0 44.00 3.40 -3 7 0 43.90 3.30 -3 7 0 50.59 3.60 -3 7 0 48.80 3.60 -3 7 0 47.00 3.30 2 -7 0 55.09 3.50 2 -7 0 50.39 3.30 2 -7 0 51.69 3.60 2 -7 0 51.99 3.60 -2 7 0 48.20 3.40 -2 7 0 46.40 3.20 -2 7 0 51.49 3.40 -2 7 0 46.00 3.20 -2 7 0 48.20 3.30 1 -7 0 21.30 2.60 1 -7 0 18.40 1.60 1 -7 0 17.20 2.30 1 -7 0 19.20 2.40 1 -7 0 23.20 2.70 1 -7 0 18.50 2.20 -1 7 0 20.80 2.40 -1 7 0 18.50 2.30 -1 7 0 22.90 2.50 -1 7 0 22.10 2.40 -1 7 0 19.70 2.50 0 -7 0 143.49 5.80 0 -7 0 141.59 5.70 0 -7 0 161.98 5.70 0 -7 0 157.78 4.80 0 -7 0 159.88 6.00 0 -7 0 158.98 5.80 0 7 0 149.69 5.70 0 7 0 155.38 5.60 0 7 0 152.08 5.70 0 7 0 157.88 4.60 0 7 0 143.59 5.10 0 7 0 156.28 5.80 -1 -7 0 161.88 5.90 -1 -7 0 167.88 4.30 -1 -7 0 169.08 6.10 -1 -7 0 162.28 5.90 -1 -7 0 176.58 6.00 -1 -7 0 170.18 6.10 -1 -7 0 162.78 5.70 1 7 0 169.58 5.70 1 7 0 165.48 5.90 1 7 0 172.58 5.30 1 7 0 173.98 6.00 1 7 0 165.98 5.10 1 7 0 166.18 6.00 -2 -7 0 262.17 7.90 -2 -7 0 276.87 8.10 -2 -7 0 272.57 7.90 -2 -7 0 271.47 6.40 -2 -7 0 255.37 8.00 -2 -7 0 264.57 8.10 -2 -7 0 275.07 8.00 2 7 0 277.07 7.70 2 7 0 265.07 7.90 2 7 0 267.67 7.50 2 7 0 265.77 7.90 2 7 0 259.27 6.90 2 7 0 276.07 8.20 -3 -7 0 43.10 2.60 -3 -7 0 41.70 1.80 -3 -7 0 43.10 2.70 -3 -7 0 44.10 2.70 -3 -7 0 44.80 2.80 -3 -7 0 42.20 1.90 -3 -7 0 47.30 2.90 -3 -7 0 38.10 2.60 3 7 0 40.80 2.60 3 7 0 43.40 2.70 3 7 0 38.20 2.40 3 7 0 41.70 2.60 3 7 0 48.20 2.50 3 7 0 40.50 2.90 3 7 0 44.10 2.00 -4 -7 0 51.99 3.00 -4 -7 0 49.90 2.90 -4 -7 0 52.59 1.80 -4 -7 0 52.89 2.90 -4 -7 0 51.49 3.00 -4 -7 0 53.59 3.10 4 7 0 55.59 1.90 4 7 0 57.69 3.00 4 7 0 52.39 3.10 4 7 0 51.39 2.80 4 7 0 52.69 2.70 4 7 0 53.89 3.10 4 7 0 58.09 1.90 4 7 0 49.30 2.90 -5 -7 0 127.89 5.10 -5 -7 0 133.69 4.90 -5 -7 0 128.59 5.00 -5 -7 0 133.29 4.80 -5 -7 0 119.09 4.80 -5 -7 0 125.99 4.70 5 7 0 128.19 4.60 5 7 0 131.59 5.10 5 7 0 134.19 4.40 5 7 0 115.59 4.60 5 7 0 132.99 5.10 5 7 0 128.09 5.20 -6 -7 0 189.98 6.10 -6 -7 0 188.18 6.30 -6 -7 0 189.58 6.10 -6 -7 0 185.48 6.60 -6 -7 0 197.18 6.60 6 7 0 196.68 6.10 6 7 0 186.18 6.80 6 7 0 185.38 6.80 6 7 0 190.38 6.40 6 7 0 178.68 5.40 -7 -7 0 54.49 3.10 -7 -7 0 51.19 3.00 -7 -7 0 61.59 3.70 -7 -7 0 55.19 3.40 -7 -7 0 53.49 3.00 7 7 0 53.89 2.40 7 7 0 56.59 3.30 7 7 0 56.79 3.70 7 7 0 56.39 3.70 7 7 0 52.79 2.90 -8 -7 0 66.49 4.00 -8 -7 0 64.69 3.30 -8 -7 0 63.39 3.40 -8 -7 0 62.89 3.40 -8 -7 0 65.79 3.90 8 7 0 70.09 4.40 8 7 0 68.39 4.40 8 7 0 54.49 3.30 8 7 0 62.59 3.70 -9 -7 0 44.20 3.00 -9 -7 0 46.90 3.60 -9 -7 0 50.99 3.20 -9 -7 0 52.19 3.80 -9 -7 0 45.30 2.90 9 7 0 48.70 3.90 9 7 0 45.50 3.80 9 7 0 51.09 3.20 9 7 0 46.90 3.60 -10 -7 0 24.60 2.40 -10 -7 0 22.60 2.90 -10 -7 0 24.90 2.60 -10 -7 0 21.50 2.50 10 7 0 23.10 3.30 10 7 0 20.20 2.90 10 7 0 21.00 3.20 -11 -7 0 74.59 4.10 -11 -7 0 70.39 3.80 -11 -7 0 68.29 4.90 11 7 0 75.39 5.40 11 7 0 76.29 5.00 11 7 0 66.59 5.10 4 -8 0 87.79 5.20 4 -8 0 82.49 5.30 4 -8 0 96.89 5.50 4 -8 0 87.59 5.10 -4 8 0 81.39 4.90 -4 8 0 96.89 5.30 -4 8 0 93.79 5.40 3 -8 0 42.70 4.10 3 -8 0 47.50 3.90 3 -8 0 45.50 3.70 3 -8 0 46.00 3.70 -3 8 0 39.40 3.70 -3 8 0 46.30 3.70 -3 8 0 46.70 3.70 2 -8 0 241.48 8.80 2 -8 0 250.87 8.50 2 -8 0 255.37 9.00 2 -8 0 248.28 8.60 -2 8 0 261.07 9.10 -2 8 0 246.48 8.30 -2 8 0 246.68 8.40 -2 8 0 251.67 8.70 1 -8 0 10.20 2.00 1 -8 0 8.60 1.80 1 -8 0 7.70 1.90 -1 8 0 6.30 1.70 -1 8 0 8.40 1.90 -1 8 0 8.70 2.00 -1 8 0 7.40 1.80 -1 8 0 10.20 2.00 0 -8 0 13.80 2.10 0 -8 0 11.20 2.10 0 -8 0 9.90 1.90 0 -8 0 12.80 2.20 0 -8 0 14.40 2.20 0 -8 0 13.20 1.60 0 8 0 15.30 2.10 0 8 0 11.60 2.00 0 8 0 12.00 1.90 0 8 0 11.00 1.90 0 8 0 10.90 2.00 -1 -8 0 137.39 5.60 -1 -8 0 134.29 5.70 -1 -8 0 133.69 5.70 -1 -8 0 133.89 5.30 -1 -8 0 133.19 5.50 1 8 0 131.99 4.60 1 8 0 137.89 5.60 1 8 0 125.99 5.30 1 8 0 130.69 5.20 1 8 0 137.79 5.70 1 8 0 130.39 4.80 -2 -8 0 165.78 6.30 -2 -8 0 172.58 6.10 -2 -8 0 156.98 6.20 -2 -8 0 162.18 6.30 -2 -8 0 168.58 6.20 2 8 0 166.08 5.20 2 8 0 172.88 6.20 2 8 0 178.08 6.50 2 8 0 174.68 5.90 2 8 0 172.08 6.20 2 8 0 170.48 5.70 -3 -8 0 20.60 2.40 -3 -8 0 17.70 2.30 -3 -8 0 23.30 2.50 -3 -8 0 21.10 2.30 -3 -8 0 21.70 2.50 -3 -8 0 24.20 1.40 3 8 0 23.00 2.30 3 8 0 22.90 2.00 3 8 0 21.10 1.60 3 8 0 19.50 2.20 3 8 0 22.00 2.50 3 8 0 23.60 2.30 -4 -8 0 8.20 1.50 -4 -8 0 10.00 1.80 -4 -8 0 8.40 1.70 -4 -8 0 11.20 1.80 -4 -8 0 11.40 1.90 4 8 0 8.60 1.80 4 8 0 13.00 1.70 4 8 0 8.90 1.60 4 8 0 10.80 1.10 4 8 0 9.80 1.10 4 8 0 7.90 1.50 4 8 0 9.80 1.80 -5 -8 0 21.40 2.40 -5 -8 0 18.80 2.40 -5 -8 0 23.70 2.50 -5 -8 0 18.40 2.30 -5 -8 0 20.20 2.30 5 8 0 23.00 2.40 5 8 0 18.20 2.20 5 8 0 18.50 2.40 5 8 0 23.30 2.70 5 8 0 19.70 2.00 -6 -8 0 0.50 1.00 -6 -8 0 0.80 1.10 -6 -8 0 0.00 0.90 -6 -8 0 -0.80 0.80 -6 -8 0 0.50 1.00 6 8 0 0.10 0.80 6 8 0 0.50 1.00 6 8 0 0.70 0.90 6 8 0 0.10 1.10 6 8 0 0.60 1.20 -7 -8 0 2.00 1.20 -7 -8 0 7.60 1.60 -7 -8 0 7.30 1.60 -7 -8 0 3.60 1.40 -7 -8 0 4.70 1.30 7 8 0 6.10 1.80 7 8 0 6.60 1.10 7 8 0 4.00 1.50 7 8 0 6.10 1.60 -8 -8 0 16.30 2.50 -8 -8 0 15.00 2.10 -8 -8 0 11.60 1.90 -8 -8 0 14.80 2.10 -8 -8 0 15.40 2.40 8 8 0 15.30 2.50 8 8 0 12.20 2.40 8 8 0 14.80 2.20 -9 -8 0 12.00 2.30 -9 -8 0 11.10 1.80 -9 -8 0 9.60 1.80 -9 -8 0 9.70 1.80 -9 -8 0 8.60 2.00 9 8 0 5.90 2.20 9 8 0 13.60 2.10 9 8 0 7.40 2.20 -10 -8 0 3.00 1.40 -10 -8 0 3.50 1.70 -10 -8 0 1.00 1.10 -10 -8 0 3.80 1.80 -10 -8 0 3.60 1.40 10 8 0 2.20 1.80 10 8 0 0.50 1.60 10 8 0 3.10 1.60 3 -9 0 20.90 3.10 3 -9 0 26.10 3.60 3 -9 0 15.90 2.60 3 -9 0 19.00 3.00 -3 9 0 21.80 3.00 2 -9 0 31.30 3.50 2 -9 0 27.60 3.40 2 -9 0 27.20 3.30 2 -9 0 21.70 3.00 -2 9 0 32.60 3.70 -2 9 0 26.10 3.00 -2 9 0 27.30 3.30 1 -9 0 0.50 1.30 1 -9 0 1.60 1.50 1 -9 0 2.30 1.40 -1 9 0 0.10 1.30 -1 9 0 0.70 1.30 -1 9 0 0.50 1.20 0 -9 0 52.89 3.90 0 -9 0 47.00 3.80 0 -9 0 50.79 3.80 0 -9 0 45.40 3.40 0 9 0 45.40 3.30 0 9 0 47.60 3.70 0 9 0 49.30 3.30 -1 -9 0 42.40 3.40 -1 -9 0 44.50 3.50 -1 -9 0 39.80 3.30 -1 -9 0 42.50 3.10 -1 -9 0 34.00 3.40 1 9 0 38.40 3.10 1 9 0 39.40 2.80 1 9 0 41.00 3.70 -2 -9 0 17.80 2.50 -2 -9 0 14.30 2.20 -2 -9 0 17.80 2.50 -2 -9 0 13.60 2.20 -2 -9 0 16.40 2.40 2 9 0 16.10 1.90 2 9 0 14.40 2.10 2 9 0 15.10 2.30 2 9 0 17.90 2.10 -3 -9 0 0.50 1.10 -3 -9 0 1.60 1.30 -3 -9 0 0.50 1.10 -3 -9 0 0.40 1.00 -3 -9 0 -1.60 1.10 3 9 0 0.90 1.40 3 9 0 -0.30 1.00 3 9 0 0.10 1.10 3 9 0 0.40 1.00 3 9 0 0.00 0.70 -4 -9 0 39.10 3.10 -4 -9 0 37.70 3.10 -4 -9 0 44.60 3.10 -4 -9 0 37.80 3.10 -4 -9 0 38.20 3.10 4 9 0 43.50 3.00 4 9 0 37.70 3.00 4 9 0 37.30 2.80 4 9 0 39.90 3.10 4 9 0 42.00 3.30 -5 -9 0 344.27 10.40 -5 -9 0 361.16 10.70 -5 -9 0 350.86 10.90 -5 -9 0 361.86 10.40 -5 -9 0 330.97 10.30 5 9 0 361.26 9.70 5 9 0 354.96 10.30 5 9 0 350.76 10.70 5 9 0 370.26 10.60 5 9 0 360.36 10.70 -6 -9 0 68.49 4.30 -6 -9 0 71.39 3.90 -6 -9 0 69.49 4.00 -6 -9 0 64.89 3.90 -6 -9 0 67.69 3.90 6 9 0 65.99 3.30 6 9 0 66.09 3.90 6 9 0 69.69 3.80 6 9 0 61.49 4.10 6 9 0 70.39 4.20 -7 -9 0 16.20 2.40 -7 -9 0 14.20 2.20 -7 -9 0 15.50 2.40 -7 -9 0 13.60 2.20 -7 -9 0 18.30 2.30 7 9 0 18.30 1.90 7 9 0 15.60 2.50 7 9 0 18.20 2.60 7 9 0 18.30 2.60 -8 -9 0 54.49 3.90 -8 -9 0 56.49 3.50 -8 -9 0 52.49 3.50 -8 -9 0 54.59 3.90 -8 -9 0 50.39 3.50 8 9 0 48.10 3.90 8 9 0 57.79 3.90 8 9 0 56.39 4.20 -9 -9 0 24.40 3.10 -9 -9 0 26.20 3.30 -9 -9 0 23.90 2.70 -9 -9 0 29.60 3.00 -9 -9 0 20.60 2.50 9 9 0 26.70 3.10 9 9 0 24.80 3.40 9 9 0 29.60 3.80 -10 -9 0 29.20 3.60 -10 -9 0 27.90 2.90 -10 -9 0 35.70 3.50 -10 -9 0 30.10 3.10 -10 -9 0 34.50 3.90 10 9 0 32.80 4.10 10 9 0 25.20 3.70 1 -10 0 1.70 1.60 1 -10 0 0.30 1.50 1 -10 0 3.30 1.60 1 -10 0 2.60 1.80 -1 10 0 4.20 1.90 -1 10 0 1.60 1.50 -1 10 0 2.20 1.40 0 -10 0 9.80 2.30 0 -10 0 16.10 2.60 0 -10 0 20.80 3.10 0 -10 0 14.30 2.60 0 10 0 14.50 2.30 0 10 0 12.10 2.50 0 10 0 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39.50 3.90 -9 -3 3 35.30 3.40 -9 -3 3 35.00 2.10 -9 -3 3 36.50 2.30 8 3 -3 45.50 3.80 8 3 -3 45.40 2.60 8 3 -3 47.00 3.40 8 3 -3 46.60 3.30 -8 -3 3 46.80 3.20 -8 -3 3 48.10 2.40 -8 -3 3 45.80 2.40 -8 -3 3 50.09 2.40 -8 -3 3 49.50 2.20 -8 -3 3 45.40 2.30 7 3 -3 44.20 3.30 7 3 -3 35.30 2.80 7 3 -3 40.70 2.90 7 3 -3 39.90 2.40 -7 -3 3 41.60 1.90 -7 -3 3 41.90 2.10 -7 -3 3 46.60 2.10 -7 -3 3 46.60 2.10 -7 -3 3 40.40 2.20 -7 -3 3 37.50 2.00 -7 -3 3 41.30 2.90 6 3 -3 529.65 11.50 6 3 -3 514.05 13.50 6 3 -3 518.45 14.20 6 3 -3 523.55 13.20 6 3 -3 528.05 12.50 -6 -3 3 522.05 11.90 -6 -3 3 533.45 13.20 -6 -3 3 538.85 11.60 -6 -3 3 539.75 11.50 -6 -3 3 529.75 11.50 -6 -3 3 519.35 12.30 -6 -3 3 537.25 11.50 -6 -3 3 525.75 11.60 -6 -3 3 530.25 11.90 5 3 -3 41.50 2.50 5 3 -3 40.80 1.60 5 3 -3 39.80 2.20 5 3 -3 38.20 2.60 5 3 -3 36.70 2.60 -5 -3 3 40.50 1.70 -5 -3 3 39.00 2.30 -5 -3 3 40.90 1.60 -5 -3 3 38.20 1.60 -5 -3 3 41.70 1.70 -5 -3 3 38.50 1.60 -5 -3 3 38.40 1.90 -5 -3 3 40.40 1.60 -5 -3 3 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70.09 3.00 -3 -4 5 71.69 2.60 -3 -4 5 72.09 2.60 -3 -4 5 70.59 3.30 -3 -4 5 73.59 2.60 -3 -4 5 70.49 2.70 -3 -4 5 68.89 2.70 -3 -4 5 71.09 2.60 -3 -4 5 67.79 2.70 2 4 -5 0.40 0.40 2 4 -5 0.40 0.50 2 4 -5 1.10 0.50 2 4 -5 0.30 0.50 2 4 -5 1.90 1.00 2 4 -5 0.20 0.80 2 4 -5 0.40 0.80 2 4 -5 0.60 0.70 -2 -4 5 0.40 0.60 -2 -4 5 0.70 0.60 -2 -4 5 1.00 0.60 -2 -4 5 0.80 0.50 -2 -4 5 0.90 0.60 -2 -4 5 1.40 0.40 -2 -4 5 0.20 0.80 -2 -4 5 0.30 0.60 1 4 -5 169.78 5.60 1 4 -5 166.68 5.20 1 4 -5 168.38 5.60 1 4 -5 169.18 5.00 1 4 -5 172.78 4.70 1 4 -5 172.38 5.10 -1 -4 5 163.88 5.20 -1 -4 5 164.28 5.30 -1 -4 5 163.28 5.10 -1 -4 5 163.48 5.50 -1 -4 5 172.38 5.20 -1 -4 5 174.68 5.10 -1 -4 5 170.98 5.10 -1 -4 5 163.98 4.90 0 4 -5 25.10 2.30 0 4 -5 25.10 1.90 0 4 -5 25.80 1.90 0 4 -5 24.50 1.70 0 4 -5 25.70 1.90 0 -4 5 23.90 1.90 0 -4 5 26.20 1.90 0 -4 5 22.50 2.20 0 -4 5 24.20 1.70 0 -4 5 23.60 1.80 0 -4 5 25.60 1.90 0 -4 5 24.00 1.80 0 -4 5 27.50 2.00 -1 4 -5 339.87 8.80 -1 4 -5 358.56 9.30 -1 4 -5 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322.77 8.40 0 -5 7 319.17 8.50 0 -5 7 312.37 9.40 0 -5 7 316.87 9.10 0 -5 7 324.07 9.20 0 -5 7 308.97 9.20 0 -5 7 314.27 9.10 -1 5 -7 23.80 2.50 -1 5 -7 32.30 2.40 -1 5 -7 26.30 2.70 -1 5 -7 25.70 2.50 1 -5 7 24.30 2.60 1 -5 7 29.40 2.90 1 -5 7 33.10 3.20 1 -5 7 24.40 2.00 1 -5 7 27.70 2.80 1 -5 7 27.40 2.80 -2 5 -7 394.76 11.00 -2 5 -7 405.26 11.30 -2 5 -7 395.96 10.60 -2 5 -7 402.56 11.10 2 -5 7 399.36 11.40 2 -5 7 394.66 11.30 2 -5 7 382.86 11.50 2 -5 7 395.16 10.60 2 -5 7 389.46 11.50 -3 5 -7 28.40 3.10 -3 5 -7 30.30 2.90 -3 5 -7 27.10 2.70 -3 5 -7 33.30 3.30 3 -5 7 31.60 3.20 3 -5 7 33.20 2.60 3 -5 7 28.10 3.00 3 -5 7 34.30 3.50 3 -5 7 31.80 2.30 3 -5 7 34.50 3.40 -4 5 -7 294.87 9.70 -4 5 -7 304.97 9.00 -4 5 -7 308.77 9.80 -4 5 -7 290.47 9.20 4 -5 7 291.77 9.70 4 -5 7 300.57 8.60 4 -5 7 279.07 9.80 4 -5 7 296.17 10.00 4 -5 7 291.57 9.90 -5 5 -7 102.09 5.50 -5 5 -7 100.89 5.50 -5 5 -7 107.39 5.20 5 -5 7 104.29 5.60 5 -5 7 110.99 5.80 -6 5 -7 9.00 2.50 -6 5 -7 5.50 1.80 -6 5 -7 7.80 2.30 6 -5 7 7.60 2.10 6 -5 7 6.00 2.10 6 -5 7 7.80 2.40 9 4 -7 4.90 1.90 9 4 -7 7.60 2.20 9 4 -7 5.50 2.20 9 4 -7 4.70 1.80 -9 -4 7 7.10 0.80 -9 -4 7 8.90 2.00 -9 -4 7 5.60 1.70 -9 -4 7 5.30 0.80 8 4 -7 1.10 1.60 8 4 -7 0.10 1.60 8 4 -7 1.70 1.40 8 4 -7 -0.60 1.20 -8 -4 7 -0.30 1.10 -8 -4 7 1.10 1.20 -8 -4 7 0.60 0.50 -8 -4 7 0.20 0.50 -8 -4 7 0.80 1.00 7 4 -7 14.20 2.60 7 4 -7 13.70 2.30 7 4 -7 18.80 2.70 -7 -4 7 19.00 1.20 -7 -4 7 21.10 2.70 -7 -4 7 22.00 2.60 -7 -4 7 19.00 1.20 6 4 -7 7.50 1.90 6 4 -7 10.10 1.60 6 4 -7 8.00 1.80 6 4 -7 6.90 1.80 -6 -4 7 8.10 1.60 -6 -4 7 8.60 0.90 -6 -4 7 7.20 0.80 -6 -4 7 5.60 1.50 -6 -4 7 6.10 1.10 5 4 -7 727.33 16.60 5 4 -7 699.33 18.90 5 4 -7 696.53 18.10 5 4 -7 683.93 17.30 -5 -4 7 693.53 15.50 -5 -4 7 718.53 14.80 -5 -4 7 716.13 16.90 -5 -4 7 710.13 17.30 -5 -4 7 716.53 15.10 4 4 -7 86.69 4.60 4 4 -7 83.99 4.60 4 4 -7 87.39 3.80 4 4 -7 97.69 4.50 -4 -4 7 95.89 4.20 -4 -4 7 93.69 3.00 -4 -4 7 89.39 3.10 -4 -4 7 91.89 3.10 -4 -4 7 89.79 2.90 -4 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99.89 4.10 0 -4 7 99.69 4.30 0 -4 7 103.39 4.30 0 -4 7 101.69 3.50 0 -4 7 95.49 3.90 0 -4 7 101.09 4.10 0 -4 7 99.29 4.10 -1 4 -7 5.20 1.30 -1 4 -7 5.10 1.10 -1 4 -7 5.60 0.60 -1 4 -7 8.60 1.60 -1 4 -7 5.20 1.20 -1 4 -7 5.00 1.20 1 -4 7 7.40 1.40 1 -4 7 5.10 1.00 1 -4 7 5.20 1.20 1 -4 7 5.10 1.40 1 -4 7 4.20 1.10 1 -4 7 4.60 1.20 1 -4 7 6.40 1.40 -2 4 -7 450.65 11.40 -2 4 -7 457.15 11.90 -2 4 -7 443.06 11.90 -2 4 -7 463.05 10.20 -2 4 -7 455.75 11.80 -2 4 -7 443.56 11.90 2 -4 7 461.45 12.30 2 -4 7 443.36 12.10 2 -4 7 457.95 11.60 2 -4 7 463.55 12.10 2 -4 7 438.96 12.20 -3 4 -7 88.39 4.30 -3 4 -7 87.69 4.30 -3 4 -7 82.49 3.90 -3 4 -7 80.29 3.80 3 -4 7 76.69 4.20 3 -4 7 79.69 4.30 3 -4 7 80.09 3.70 3 -4 7 81.19 3.30 3 -4 7 83.89 4.30 3 -4 7 89.29 4.40 -4 4 -7 0.90 1.10 -4 4 -7 1.80 1.10 -4 4 -7 1.00 1.10 -4 4 -7 1.30 1.30 4 -4 7 0.70 0.80 4 -4 7 0.90 1.20 4 -4 7 0.70 1.20 4 -4 7 0.70 1.20 4 -4 7 0.40 0.90 4 -4 7 0.50 1.20 -5 4 -7 136.19 5.90 -5 4 -7 130.39 5.90 -5 4 -7 131.19 4.90 -5 4 -7 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10.10 1.80 4 6 -8 61.59 4.30 4 6 -8 68.29 4.20 4 6 -8 56.89 4.30 4 6 -8 63.69 3.50 -4 -6 8 59.99 4.00 -4 -6 8 70.89 4.20 -4 -6 8 64.09 3.10 -4 -6 8 63.99 3.50 -4 -6 8 64.29 3.30 -4 -6 8 66.09 3.30 3 6 -8 220.08 8.20 3 6 -8 221.38 8.10 3 6 -8 232.58 7.40 -3 -6 8 214.08 6.80 -3 -6 8 228.48 8.00 -3 -6 8 230.58 7.90 -3 -6 8 217.08 7.00 -3 -6 8 223.38 7.10 -3 -6 8 221.68 7.00 2 6 -8 59.99 3.60 2 6 -8 56.49 3.90 -2 -6 8 65.79 3.90 -2 -6 8 59.89 3.40 -2 -6 8 59.09 3.20 -2 -6 8 59.79 3.40 -2 -6 8 61.89 4.00 -2 -6 8 59.69 3.50 1 6 -8 535.85 15.00 1 6 -8 529.65 12.80 1 6 -8 585.54 14.50 -1 -6 8 567.74 14.40 -1 -6 8 556.44 14.60 -1 -6 8 575.34 15.20 -1 -6 8 548.05 13.60 -1 -6 8 551.14 14.50 -1 -6 8 552.94 14.30 0 6 -8 10.80 1.60 0 6 -8 10.40 2.00 0 6 -8 7.80 1.70 0 6 -8 8.00 2.10 0 -6 8 11.30 2.00 0 -6 8 7.10 1.90 0 -6 8 8.60 1.60 0 -6 8 7.40 1.80 0 -6 8 7.00 1.60 0 -6 8 7.40 1.70 -1 6 -8 12.80 2.10 -1 6 -8 15.20 2.00 -1 6 -8 13.60 2.20 -1 6 -8 14.90 2.30 -1 6 -8 9.30 2.10 1 -6 8 11.70 2.00 1 -6 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2.00 -8 -4 8 8.40 2.00 7 4 -8 -0.60 1.30 7 4 -8 -1.00 1.20 7 4 -8 -2.20 1.30 -7 -4 8 0.10 0.40 -7 -4 8 0.00 0.40 -7 -4 8 -0.60 1.10 -7 -4 8 1.50 1.20 6 4 -8 2.90 1.50 6 4 -8 -0.50 1.40 6 4 -8 1.90 1.30 6 4 -8 1.00 1.10 -6 -4 8 2.20 1.10 -6 -4 8 1.10 1.10 -6 -4 8 0.80 0.80 -6 -4 8 2.30 0.60 -6 -4 8 1.00 0.50 5 4 -8 1.70 1.30 5 4 -8 -0.30 0.90 5 4 -8 -0.60 1.00 5 4 -8 1.20 1.40 -5 -4 8 0.00 0.80 -5 -4 8 -0.20 0.30 -5 -4 8 -0.50 1.00 -5 -4 8 2.00 1.10 -5 -4 8 -0.60 0.50 4 4 -8 36.00 2.90 4 4 -8 36.20 3.10 4 4 -8 36.60 2.70 4 4 -8 37.20 3.50 -4 -4 8 42.30 2.60 -4 -4 8 32.20 2.60 -4 -4 8 39.00 2.00 -4 -4 8 36.40 1.90 -4 -4 8 42.50 2.90 -4 -4 8 37.70 2.00 -4 -4 8 37.00 1.80 3 4 -8 251.67 8.40 3 4 -8 259.97 7.70 3 4 -8 241.28 8.10 3 4 -8 240.68 8.60 -3 -4 8 247.28 6.80 -3 -4 8 251.57 6.60 -3 -4 8 258.97 8.00 -3 -4 8 263.37 7.10 -3 -4 8 251.67 6.70 -3 -4 8 248.78 6.70 -3 -4 8 258.07 8.00 2 4 -8 3.80 1.20 2 4 -8 1.90 1.20 2 4 -8 3.90 0.90 -2 -4 8 3.30 1.00 -2 -4 8 2.10 0.90 -2 -4 8 4.40 1.00 -2 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3.70 3 -4 8 62.19 3.80 3 -4 8 57.59 2.70 3 -4 8 57.19 3.70 3 -4 8 50.69 3.20 -4 4 -8 48.30 3.60 -4 4 -8 54.59 3.20 -4 4 -8 50.29 3.40 -4 4 -8 55.59 3.70 4 -4 8 46.70 3.40 4 -4 8 55.89 3.80 4 -4 8 47.30 3.60 4 -4 8 50.79 3.80 4 -4 8 53.99 3.20 -5 4 -8 26.80 3.10 -5 4 -8 28.10 3.00 -5 4 -8 31.00 3.50 5 -4 8 24.80 2.60 5 -4 8 24.80 3.20 5 -4 8 25.40 3.10 -6 4 -8 18.30 2.80 -6 4 -8 21.20 3.10 -6 4 -8 21.70 2.90 6 -4 8 22.20 3.20 6 -4 8 15.50 2.60 6 -4 8 19.80 3.00 9 3 -8 -0.70 1.80 9 3 -8 1.20 1.70 9 3 -8 -1.70 1.30 -9 -3 8 -1.10 1.30 -9 -3 8 -0.10 1.20 -9 -3 8 -0.30 1.20 8 3 -8 26.70 3.40 8 3 -8 28.90 3.20 8 3 -8 22.30 3.00 8 3 -8 19.20 3.10 -8 -3 8 26.70 3.00 -8 -3 8 27.50 3.10 7 3 -8 4.60 1.70 7 3 -8 3.40 1.50 7 3 -8 5.10 2.10 7 3 -8 7.80 1.70 -7 -3 8 8.20 1.50 -7 -3 8 7.60 1.40 -7 -3 8 5.50 1.60 -7 -3 8 9.20 1.80 6 3 -8 45.20 3.50 6 3 -8 51.19 3.50 6 3 -8 33.30 3.60 -6 -3 8 39.60 2.90 -6 -3 8 50.09 3.20 -6 -3 8 42.30 2.40 -6 -3 8 49.70 3.10 5 3 -8 24.70 2.50 5 3 -8 22.40 2.70 5 3 -8 19.10 2.70 5 3 -8 21.70 2.50 -5 -3 8 20.10 2.30 -5 -3 8 18.10 1.80 -5 -3 8 14.70 1.80 -5 -3 8 23.50 2.50 -5 -3 8 21.10 1.00 -5 -3 8 18.40 1.00 4 3 -8 754.02 17.60 4 3 -8 760.02 18.20 4 3 -8 744.13 18.70 4 3 -8 718.43 19.40 -4 -3 8 753.02 17.90 -4 -3 8 760.02 15.30 -4 -3 8 727.73 16.00 -4 -3 8 751.42 17.30 -4 -3 8 730.33 16.10 -4 -3 8 750.02 15.30 -4 -3 8 778.52 17.80 -4 -3 8 760.12 15.60 3 3 -8 106.49 4.80 3 3 -8 113.29 3.10 3 3 -8 105.19 4.00 3 3 -8 106.39 4.70 3 3 -8 103.79 4.40 3 3 -8 104.19 4.90 -3 -3 8 104.19 3.30 -3 -3 8 115.29 3.90 -3 -3 8 109.99 3.40 -3 -3 8 105.79 4.50 -3 -3 8 114.19 4.50 -3 -3 8 108.49 3.20 -3 -3 8 118.39 3.60 -3 -3 8 104.99 3.40 -3 -3 8 105.69 3.10 2 3 -8 314.47 7.50 2 3 -8 299.77 9.50 2 3 -8 307.07 9.00 2 3 -8 303.27 8.00 2 3 -8 306.27 8.70 -2 -3 8 307.47 8.00 -2 -3 8 312.57 7.90 -2 -3 8 318.47 7.80 -2 -3 8 315.87 7.70 -2 -3 8 305.97 7.70 -2 -3 8 311.67 8.80 -2 -3 8 306.67 8.80 -2 -3 8 313.17 7.50 -2 -3 8 311.97 7.70 1 3 -8 3.70 1.20 1 3 -8 5.60 0.60 1 3 -8 5.50 1.00 1 3 -8 6.80 0.70 1 3 -8 8.10 1.00 1 3 -8 6.00 1.30 -1 -3 8 4.70 1.00 -1 -3 8 4.60 1.30 -1 -3 8 5.90 1.10 -1 -3 8 7.10 0.90 -1 -3 8 6.10 1.00 -1 -3 8 5.00 1.30 -1 -3 8 6.00 1.00 -1 -3 8 7.60 1.20 0 3 -8 9.30 1.10 0 3 -8 7.30 1.50 0 3 -8 8.00 1.20 0 3 -8 9.90 1.10 0 3 -8 7.60 1.40 0 3 -8 8.40 1.20 0 -3 8 10.70 1.10 0 -3 8 6.90 1.20 0 -3 8 9.50 1.30 0 -3 8 8.70 1.30 0 -3 8 6.60 1.30 0 -3 8 12.10 1.70 0 -3 8 10.20 1.40 0 -3 8 11.30 1.50 -1 3 -8 151.48 4.00 -1 3 -8 138.79 4.90 -1 3 -8 150.18 5.40 -1 3 -8 155.38 5.50 -1 3 -8 152.48 4.20 -1 3 -8 148.09 4.60 -1 3 -8 144.99 4.90 1 -3 8 148.29 5.20 1 -3 8 147.19 4.10 1 -3 8 139.59 5.10 1 -3 8 152.58 5.40 1 -3 8 151.48 5.20 1 -3 8 153.38 5.30 1 -3 8 148.49 5.50 -2 3 -8 242.38 6.30 -2 3 -8 245.48 7.30 -2 3 -8 236.48 6.90 -2 3 -8 236.98 7.30 -2 3 -8 246.78 7.40 -2 3 -8 238.38 7.50 -2 3 -8 236.18 7.70 2 -3 8 237.48 7.60 2 -3 8 237.08 7.50 2 -3 8 233.08 7.40 2 -3 8 249.08 7.40 2 -3 8 248.48 7.50 -3 3 -8 318.27 9.40 -3 3 -8 323.77 9.00 -3 3 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73.29 3.20 -2 -4 9 69.79 3.20 -2 -4 9 70.99 3.20 -2 -4 9 71.69 3.10 -2 -4 9 79.29 3.10 1 4 -9 18.10 1.20 1 4 -9 17.80 2.30 1 4 -9 17.80 2.40 1 4 -9 19.40 1.80 1 4 -9 17.20 1.30 -1 -4 9 21.80 2.20 -1 -4 9 17.40 1.60 -1 -4 9 15.80 1.90 -1 -4 9 15.80 2.20 -1 -4 9 17.20 1.90 -1 -4 9 15.30 2.20 0 4 -9 34.70 2.00 0 4 -9 31.00 3.00 0 4 -9 29.30 2.90 0 4 -9 31.80 2.30 0 -4 9 33.10 2.50 0 -4 9 32.30 2.60 0 -4 9 36.10 2.60 0 -4 9 34.90 1.90 0 -4 9 32.70 3.00 0 -4 9 39.60 2.70 -1 4 -9 107.59 4.80 -1 4 -9 99.29 4.40 -1 4 -9 109.79 4.90 -1 4 -9 106.49 4.00 1 -4 9 106.69 4.70 1 -4 9 103.59 4.60 1 -4 9 109.99 4.70 1 -4 9 108.69 4.70 1 -4 9 108.79 5.00 -2 4 -9 128.69 5.60 -2 4 -9 137.49 5.50 -2 4 -9 134.49 5.40 -2 4 -9 123.09 4.80 2 -4 9 130.39 5.30 2 -4 9 130.59 5.40 2 -4 9 129.99 5.70 2 -4 9 131.19 5.50 2 -4 9 131.79 5.50 -3 4 -9 0.70 1.10 -3 4 -9 0.10 1.10 -3 4 -9 1.30 1.20 -3 4 -9 1.10 1.20 3 -4 9 0.80 1.20 3 -4 9 2.40 1.50 3 -4 9 2.00 1.30 3 -4 9 0.60 1.00 3 -4 9 2.30 1.40 -4 4 -9 3.80 1.70 -4 4 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1.30 4 3 -9 2.10 1.20 4 3 -9 0.80 1.20 -4 -3 9 1.10 0.50 -4 -3 9 1.00 1.00 -4 -3 9 1.70 0.90 -4 -3 9 1.70 1.10 -4 -3 9 0.90 0.50 3 3 -9 7.60 1.80 3 3 -9 9.20 1.70 3 3 -9 8.00 1.80 3 3 -9 7.80 1.30 -3 -3 9 9.20 1.10 -3 -3 9 8.60 0.90 -3 -3 9 8.80 1.10 -3 -3 9 7.70 1.00 -3 -3 9 8.90 1.70 -3 -3 9 9.60 1.70 -3 -3 9 8.30 1.30 2 3 -9 231.68 8.20 2 3 -9 236.08 6.70 2 3 -9 234.18 6.00 2 3 -9 232.28 7.30 2 3 -9 226.58 7.60 -2 -3 9 233.48 7.30 -2 -3 9 252.17 6.50 -2 -3 9 237.08 6.30 -2 -3 9 233.98 6.30 -2 -3 9 235.18 7.50 -2 -3 9 228.38 6.30 -2 -3 9 230.48 6.40 -2 -3 9 234.28 6.20 1 3 -9 1.70 1.10 1 3 -9 1.10 0.60 1 3 -9 1.60 0.80 1 3 -9 1.40 1.10 1 3 -9 1.50 0.70 -1 -3 9 1.60 0.80 -1 -3 9 1.70 1.00 -1 -3 9 1.80 0.80 -1 -3 9 1.50 0.70 -1 -3 9 0.10 1.00 -1 -3 9 0.50 0.60 -1 -3 9 0.10 0.70 -1 -3 9 1.00 0.60 0 3 -9 108.89 4.60 0 3 -9 111.29 3.60 0 3 -9 113.79 4.10 0 3 -9 112.29 3.30 0 3 -9 105.49 4.70 0 3 -9 105.59 3.40 0 -3 9 109.99 3.30 0 -3 9 103.09 4.00 0 -3 9 107.49 4.10 0 -3 9 106.89 4.60 0 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165.68 5.90 3 2 -9 163.68 6.10 3 2 -9 161.58 5.70 -3 -2 9 172.48 5.70 -3 -2 9 170.08 4.20 -3 -2 9 160.48 4.20 -3 -2 9 160.28 5.00 -3 -2 9 167.58 4.30 -3 -2 9 160.38 4.30 -3 -2 9 164.48 3.80 -3 -2 9 173.18 5.90 -3 -2 9 160.58 3.70 2 2 -9 67.99 3.70 2 2 -9 76.79 4.20 2 2 -9 77.49 2.40 2 2 -9 71.49 3.60 2 2 -9 72.79 3.30 -2 -2 9 73.39 2.70 -2 -2 9 74.89 2.70 -2 -2 9 78.99 2.70 -2 -2 9 75.49 2.50 -2 -2 9 72.89 3.40 -2 -2 9 72.49 2.50 -2 -2 9 72.49 2.60 -2 -2 9 67.49 3.50 1 2 -9 218.98 5.60 1 2 -9 202.28 6.10 1 2 -9 215.08 6.90 1 2 -9 210.68 5.60 1 2 -9 214.08 6.80 -1 -2 9 199.28 5.60 -1 -2 9 210.68 5.80 -1 -2 9 202.78 5.80 -1 -2 9 208.08 6.40 -1 -2 9 215.28 6.70 -1 -2 9 201.98 5.70 -1 -2 9 213.98 5.30 -1 -2 9 218.08 5.60 0 2 -9 100.99 3.50 0 2 -9 93.29 4.20 0 2 -9 94.39 3.50 0 2 -9 97.89 2.90 0 2 -9 98.39 2.80 0 2 -9 97.19 4.20 0 2 -9 98.89 3.40 0 -2 9 92.69 3.50 0 -2 9 99.59 3.60 0 -2 9 103.59 3.20 0 -2 9 87.79 4.10 0 -2 9 98.59 3.70 0 -2 9 93.59 3.60 0 -2 9 97.49 4.00 0 -2 9 95.39 2.70 0 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1.70 1.40 -1 4 -10 2.70 1.20 1 -4 10 2.80 1.30 1 -4 10 2.70 1.30 1 -4 10 5.80 1.60 1 -4 10 5.20 1.50 1 -4 10 4.20 1.40 -2 4 -10 11.40 2.20 -2 4 -10 18.30 2.10 -2 4 -10 13.30 2.10 -2 4 -10 15.60 2.30 2 -4 10 14.80 2.30 2 -4 10 11.90 2.00 2 -4 10 11.60 1.90 2 -4 10 13.40 2.10 2 -4 10 11.60 2.10 -3 4 -10 43.30 3.40 -3 4 -10 43.20 3.00 -3 4 -10 49.10 3.40 -3 4 -10 48.70 3.50 3 -4 10 44.50 3.50 3 -4 10 49.99 3.70 3 -4 10 41.90 3.30 3 -4 10 45.10 3.30 3 -4 10 43.80 3.50 -4 4 -10 2.90 1.40 -4 4 -10 6.70 1.90 -4 4 -10 6.10 1.90 -4 4 -10 5.50 1.60 4 -4 10 3.70 1.40 4 -4 10 5.10 1.90 4 -4 10 8.10 2.10 4 -4 10 10.10 2.20 -5 4 -10 1.40 1.60 -5 4 -10 0.50 1.20 -5 4 -10 0.60 1.70 5 -4 10 1.50 1.40 5 -4 10 1.80 1.40 5 -4 10 2.40 1.50 5 -4 10 0.20 1.50 -6 4 -10 22.60 3.30 6 -4 10 23.00 3.50 8 3 -10 51.49 5.30 8 3 -10 53.49 5.00 -8 -3 10 61.89 4.10 -8 -3 10 55.29 3.80 -8 -3 10 50.99 3.90 7 3 -10 122.79 6.30 7 3 -10 126.99 6.10 7 3 -10 129.99 7.00 -7 -3 10 135.89 6.00 -7 -3 10 139.39 5.60 -7 -3 10 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2.80 -1 -3 10 54.69 3.40 -1 -3 10 46.70 3.10 -1 -3 10 54.39 2.70 -1 -3 10 48.70 2.70 -1 -3 10 49.80 2.10 -1 -3 10 48.70 2.60 0 3 -10 62.69 2.40 0 3 -10 61.59 3.70 0 3 -10 63.89 3.10 0 3 -10 65.39 2.80 0 3 -10 62.09 3.70 0 -3 10 61.99 3.20 0 -3 10 62.89 3.60 0 -3 10 60.99 2.20 0 -3 10 65.59 3.60 0 -3 10 60.39 3.10 0 -3 10 66.69 3.30 -1 3 -10 26.60 2.80 -1 3 -10 21.60 1.60 -1 3 -10 21.10 2.50 -1 3 -10 21.00 1.70 -1 3 -10 22.60 2.20 1 -3 10 21.70 2.50 1 -3 10 21.70 2.30 1 -3 10 27.80 2.60 1 -3 10 21.60 2.50 1 -3 10 20.30 2.30 -2 3 -10 94.89 4.40 -2 3 -10 105.89 4.90 -2 3 -10 91.99 4.30 -2 3 -10 97.99 3.50 -2 3 -10 90.29 3.80 2 -3 10 97.29 4.50 2 -3 10 107.19 4.80 2 -3 10 99.39 4.50 2 -3 10 105.19 4.70 2 -3 10 93.49 4.50 -3 3 -10 9.50 2.00 -3 3 -10 10.10 2.00 -3 3 -10 8.40 1.60 -3 3 -10 8.10 1.70 3 -3 10 5.20 1.50 3 -3 10 6.20 1.60 3 -3 10 9.50 2.00 3 -3 10 7.50 1.70 -4 3 -10 87.09 4.20 -4 3 -10 92.79 4.70 -4 3 -10 76.09 4.10 4 -3 10 91.99 4.80 4 -3 10 91.79 4.90 4 -3 10 83.29 4.60 4 -3 10 74.19 4.00 -5 3 -10 187.98 6.90 -5 3 -10 179.98 6.40 -5 3 -10 176.28 7.20 -5 3 -10 188.18 7.30 5 -3 10 183.58 7.40 5 -3 10 198.28 7.60 5 -3 10 186.68 7.20 5 -3 10 175.48 6.60 5 -3 10 179.18 7.30 -6 3 -10 0.10 1.20 -6 3 -10 0.60 1.30 -6 3 -10 0.90 1.40 6 -3 10 1.00 1.60 6 -3 10 1.60 1.40 6 -3 10 -0.40 1.10 6 -3 10 1.20 1.40 -7 3 -10 2.90 1.70 7 -3 10 5.20 2.10 7 -3 10 2.40 1.70 8 2 -10 30.70 3.90 8 2 -10 31.00 3.70 8 2 -10 22.00 3.20 -8 -2 10 30.30 3.40 -8 -2 10 30.90 3.30 -8 -2 10 36.10 3.40 7 2 -10 4.70 2.00 7 2 -10 2.40 1.60 -7 -2 10 2.50 1.20 -7 -2 10 4.10 1.30 -7 -2 10 3.70 1.40 -7 -2 10 3.70 1.40 -7 -2 10 2.90 1.50 6 2 -10 3.50 1.70 6 2 -10 1.50 1.60 6 2 -10 4.20 1.80 -6 -2 10 3.30 1.20 -6 -2 10 3.30 1.30 -6 -2 10 3.30 1.30 -6 -2 10 2.40 1.30 -6 -2 10 3.30 1.20 5 2 -10 179.88 6.90 5 2 -10 173.68 6.60 5 2 -10 176.08 7.40 -5 -2 10 168.38 6.20 -5 -2 10 182.88 6.40 -5 -2 10 173.88 5.90 -5 -2 10 162.18 6.20 -5 -2 10 180.98 6.10 4 2 -10 2.50 1.60 4 2 -10 1.90 1.40 4 2 -10 1.60 1.00 4 2 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2.50 1.10 5 -2 10 1.80 1.30 5 -2 10 3.00 1.50 5 -2 10 3.20 1.40 5 -2 10 2.70 1.20 5 -2 10 0.10 1.30 -6 2 -10 211.48 8.00 -6 2 -10 216.88 8.00 -6 2 -10 219.18 7.70 6 -2 10 228.48 8.40 6 -2 10 216.78 8.00 6 -2 10 237.38 8.50 6 -2 10 216.38 7.50 -7 2 -10 48.90 3.70 -7 2 -10 51.19 4.00 -7 2 -10 52.89 4.60 7 -2 10 53.89 3.80 7 -2 10 51.49 4.20 7 -2 10 52.59 3.90 7 -2 10 49.50 4.00 8 1 -10 5.60 1.90 8 1 -10 6.90 2.40 -8 -1 10 4.30 1.80 -8 -1 10 7.70 1.80 -8 -1 10 8.70 1.80 7 1 -10 133.59 6.90 7 1 -10 164.38 6.80 -7 -1 10 146.59 6.00 -7 -1 10 158.38 5.80 -7 -1 10 144.09 6.10 -7 -1 10 146.09 5.70 -7 -1 10 148.79 5.60 6 1 -10 219.78 8.80 6 1 -10 220.88 8.00 -6 -1 10 223.18 7.50 -6 -1 10 240.08 7.50 -6 -1 10 231.78 7.60 -6 -1 10 233.78 7.40 -6 -1 10 230.88 7.30 5 1 -10 29.20 3.20 5 1 -10 24.50 3.10 5 1 -10 22.60 2.70 -5 -1 10 30.00 2.40 -5 -1 10 24.90 2.60 -5 -1 10 27.90 2.60 -5 -1 10 21.20 2.40 -5 -1 10 28.00 2.60 4 1 -10 89.69 4.60 4 1 -10 91.09 4.40 4 1 -10 86.29 4.40 4 1 -10 81.99 4.60 -4 -1 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2.00 0 5 17 4.90 1.30 0 5 17 3.20 1.50 0 5 17 4.30 1.90 0 5 17 8.10 2.10 0 5 17 5.40 1.50 -1 -5 -17 173.28 7.40 -1 -5 -17 167.28 7.90 1 5 17 168.28 6.70 1 5 17 185.48 6.30 1 5 17 166.98 7.10 1 5 17 169.58 7.30 -2 -5 -17 3.20 1.70 -2 -5 -17 6.40 2.20 2 5 17 6.90 2.00 2 5 17 6.10 1.50 2 5 17 3.80 1.40 2 5 17 4.60 1.60 2 5 17 4.80 1.90 -3 -5 -17 2.70 1.70 -3 -5 -17 0.80 1.50 3 5 17 0.50 1.10 3 5 17 0.20 1.30 3 5 17 -1.80 0.80 3 5 17 1.00 1.40 -4 -5 -17 2.30 1.50 -4 -5 -17 2.50 1.80 4 5 17 0.50 1.40 4 5 17 1.60 1.40 4 5 17 2.60 1.40 4 5 17 3.50 1.50 4 5 17 0.00 1.10 -5 -5 -17 5.40 2.20 -5 -5 -17 9.40 2.10 5 5 17 8.10 2.00 5 5 17 3.80 1.60 5 5 17 9.20 2.20 5 5 17 4.80 2.10 5 5 17 6.80 1.80 -6 -5 -17 3.80 1.90 -6 -5 -17 3.70 1.50 -6 -5 -17 6.00 2.00 6 5 17 1.90 1.70 6 5 17 6.10 1.90 6 5 17 1.20 1.30 6 5 17 3.00 1.70 6 5 17 1.50 1.60 -1 -6 -17 77.89 5.10 -1 -6 -17 78.39 5.60 1 6 17 76.09 4.70 1 6 17 78.29 5.10 1 6 17 75.09 4.20 1 6 17 87.09 4.60 1 6 17 78.79 4.10 -2 -6 -17 41.00 4.50 -2 -6 -17 52.49 4.10 2 6 17 41.80 4.10 2 6 17 44.50 3.60 2 6 17 42.60 3.20 2 6 17 52.59 3.60 2 6 17 50.39 3.70 -3 -6 -17 -0.80 1.40 -3 -6 -17 0.10 1.30 3 6 17 0.80 1.10 3 6 17 1.50 1.30 3 6 17 -0.10 1.30 3 6 17 -0.70 1.30 3 6 17 -0.50 1.20 -4 -6 -17 -0.30 1.40 -4 -6 -17 3.90 1.90 4 6 17 2.30 1.60 4 6 17 -0.50 1.40 4 6 17 -0.90 1.00 4 6 17 0.40 1.40 -5 -6 -17 18.40 3.20 -5 -6 -17 21.60 3.00 5 6 17 25.60 3.10 5 6 17 20.90 3.00 5 6 17 17.10 2.50 5 6 17 22.70 3.20 5 6 17 18.50 2.80 -6 -6 -17 65.39 4.30 -6 -6 -17 64.59 3.90 -6 -6 -17 65.39 5.00 6 6 17 61.09 4.20 6 6 17 57.99 4.30 6 6 17 75.39 4.80 6 6 17 56.99 4.30 6 6 17 64.99 4.50 -2 -7 -17 25.90 3.80 2 7 17 28.50 3.50 2 7 17 32.00 3.30 2 7 17 32.90 3.70 -3 -7 -17 25.60 3.80 -3 -7 -17 27.90 3.50 3 7 17 23.40 3.00 3 7 17 19.60 2.80 3 7 17 24.90 3.10 3 7 17 25.00 2.90 3 7 17 22.00 3.10 -4 -7 -17 0.50 1.40 -4 -7 -17 0.90 1.60 4 7 17 -1.10 1.20 4 7 17 0.70 1.10 4 7 17 3.10 1.70 4 7 17 0.30 1.30 4 7 17 -0.40 1.40 -5 -7 -17 57.59 4.10 -5 -7 -17 48.40 3.90 5 7 17 48.70 4.50 5 7 17 40.20 3.90 5 7 17 44.30 4.10 5 7 17 50.39 3.90 5 7 17 43.00 4.10 -6 -7 -17 39.30 3.80 -6 -7 -17 39.30 4.60 6 7 17 38.60 4.10 6 7 17 36.20 3.80 6 7 17 33.70 3.80 -1 -2 -18 0.70 1.70 -1 -2 -18 -0.30 1.70 1 2 18 2.90 1.20 1 2 18 -1.50 1.10 1 2 18 1.20 1.20 1 2 18 3.30 1.70 -2 -2 -18 105.49 5.90 -2 -2 -18 96.19 5.50 2 2 18 100.99 5.60 2 2 18 96.89 4.80 2 2 18 101.29 5.50 2 2 18 95.09 4.60 -3 -2 -18 0.60 1.50 -3 -2 -18 -0.20 1.50 3 2 18 2.10 1.40 3 2 18 2.30 1.60 3 2 18 3.40 1.30 3 2 18 1.30 1.50 -1 -3 -18 6.60 2.10 -1 -3 -18 7.20 2.40 1 3 18 5.60 2.00 1 3 18 4.10 1.70 1 3 18 8.10 1.70 -2 -3 -18 83.09 5.50 -2 -3 -18 92.39 5.70 2 3 18 88.29 4.50 2 3 18 95.89 5.40 2 3 18 87.09 4.40 2 3 18 93.49 5.20 -3 -3 -18 1.30 1.70 -3 -3 -18 0.30 1.50 3 3 18 1.00 1.30 3 3 18 -0.20 1.20 3 3 18 1.70 1.40 3 3 18 1.30 1.50 3 3 18 1.60 1.60 -4 -3 -18 16.50 2.80 -4 -3 -18 8.10 2.30 4 3 18 8.00 2.20 4 3 18 14.80 2.30 4 3 18 10.10 2.20 4 3 18 10.20 2.10 -1 -4 -18 145.99 7.10 -1 -4 -18 154.28 7.50 1 4 18 143.89 5.80 1 4 18 150.88 6.90 1 4 18 151.58 6.60 -2 -4 -18 0.20 1.70 -2 -4 -18 1.90 1.60 2 4 18 0.20 1.10 2 4 18 1.60 1.70 2 4 18 0.10 1.30 -3 -4 -18 19.10 3.10 -3 -4 -18 19.40 3.20 3 4 18 15.00 2.60 3 4 18 18.10 2.50 3 4 18 20.40 2.80 3 4 18 19.20 2.50 3 4 18 22.50 3.20 -4 -4 -18 17.30 3.10 -4 -4 -18 24.10 3.40 4 4 18 23.00 3.10 4 4 18 19.00 2.90 4 4 18 25.40 3.00 4 4 18 18.50 2.60 -2 -5 -18 -0.20 1.70 -2 -5 -18 1.40 1.80 2 5 18 1.20 1.60 2 5 18 1.70 1.60 2 5 18 1.70 1.30 -3 -5 -18 1.90 2.00 -3 -5 -18 5.10 1.90 3 5 18 6.00 1.70 3 5 18 3.40 1.70 3 5 18 0.00 1.70 -4 -5 -18 0.90 1.50 -4 -5 -18 2.50 1.80 4 5 18 -0.20 1.20 4 5 18 -1.00 1.40 4 5 18 -1.40 1.10 4 5 18 0.90 1.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 58609 _olex2_submission_special_instructions 'No special instructions were received'