####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_pph349 _database_code_depnum_ccdc_archive 'CCDC 2163065' loop_ _audit_author_name _audit_author_address 'Stephen A. Moggach' ;The University of Western Australia Australia ; _audit_update_record ; 2022-03-29 deposited with the CCDC. 2022-07-20 downloaded from the CCDC. ; _audit_creation_date 2019-08-09 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number 2018/3 _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C83 H84 O P4 Ru2 [+ solvent]' _chemical_formula_sum 'C83 H84 O P4 Ru2 [+ solvent]' _chemical_formula_weight 1423.52 _chemical_melting_point ? _chemical_oxdiff_formula 'C83 H84 O P4 Ru2' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru 0.0552 3.2960 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _audit_contact_author_name 'Stephen A. Moggach' _publ_contact_author_id_orcid 0000-0001-5339-7070 _cell_length_a 18.8881(3) _cell_length_b 20.8050(3) _cell_length_c 19.5529(3) _cell_angle_alpha 90 _cell_angle_beta 103.523(2) _cell_angle_gamma 90 _cell_volume 7470.6(2) _cell_formula_units_Z 4 _cell_measurement_reflns_used 32065 _cell_measurement_temperature 150.00(10) _cell_measurement_theta_max 75.3330 _cell_measurement_theta_min 2.3960 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 4.409 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.19532 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'orange' _exptl_crystal_density_diffrn 1.266 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'block' _exptl_crystal_F_000 2952 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.1196 _diffrn_reflns_av_unetI/netI 0.0577 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.979 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 109017 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.979 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 75.678 _diffrn_reflns_theta_min 2.406 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.979 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -73.00 27.00 0.50 2.10 -- -46.20 87.00 34.00 200 2 \w -25.00 73.00 0.50 2.10 -- 46.20 -87.00 -82.00 196 3 \w -129.00 -30.00 0.50 2.10 -- -102.41 87.00 34.00 198 4 \w -175.00 -79.00 0.50 2.10 -- -102.41 -87.00 -82.00 192 5 \w 30.00 130.00 0.50 2.10 -- 102.41 -87.00 -82.00 200 6 \w 79.00 175.00 0.50 2.10 -- 102.41 87.00 34.00 192 7 \w -118.00 -73.00 0.50 2.10 -- -46.20-125.00 60.00 90 8 \w -118.00 -73.00 0.50 2.10 -- -46.20-125.00 0.00 90 9 \w 34.00 119.00 0.50 2.10 -- 46.20 38.00-180.00 170 10 \w 34.00 119.00 0.50 2.10 -- 46.20 38.00-150.00 170 11 \w -174.00 -90.00 0.50 2.10 -- -102.41 -45.00 0.00 168 12 \w -111.00 -30.00 0.50 2.10 -- -102.41 125.00 60.00 162 13 \w -175.00 -86.00 0.50 2.10 -- -102.41 -61.00 -30.00 178 14 \w 30.00 105.00 0.50 2.10 -- 102.41 -94.00 -30.00 150 15 \w 30.00 111.00 0.50 2.10 -- 102.41-125.00 -90.00 162 16 \w 30.00 111.00 0.50 2.10 -- 102.41-125.00 120.00 162 17 \w 30.00 105.00 0.50 2.10 -- 102.41 -94.00 150.00 150 18 \w 31.00 118.00 0.50 2.10 -- 46.20 57.00-120.00 174 19 \w 31.00 118.00 0.50 2.10 -- 46.20 57.00 -60.00 174 20 \w 24.00 118.00 0.50 2.10 -- 46.20 77.00 30.00 188 21 \w 24.00 118.00 0.50 2.10 -- 46.20 77.00 -30.00 188 22 \w 24.00 118.00 0.50 2.10 -- 46.20 77.00 90.00 188 23 \w -175.00 -86.00 0.50 2.10 -- -102.41 -61.00-150.00 178 24 \w -174.00-137.00 0.50 2.10 -- -102.41 -45.00 30.00 74 25 \w 90.00 177.00 0.50 2.10 -- 102.41 30.00 150.00 174 26 \w 90.00 108.00 0.50 2.10 -- 102.41 45.00 90.00 36 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0348290000 _diffrn_orient_matrix_UB_12 -0.0629657000 _diffrn_orient_matrix_UB_13 -0.0333323000 _diffrn_orient_matrix_UB_21 -0.0760442000 _diffrn_orient_matrix_UB_22 0.0308045000 _diffrn_orient_matrix_UB_23 -0.0117172000 _diffrn_orient_matrix_UB_31 0.0063184000 _diffrn_orient_matrix_UB_32 0.0238794000 _diffrn_orient_matrix_UB_33 -0.0729366000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 11358 _reflns_number_total 15199 _reflns_odcompleteness_completeness 99.88 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.49 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _refine_diff_density_max 2.868 _refine_diff_density_min -1.535 _refine_diff_density_rms 0.174 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.110 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 787 _refine_ls_number_reflns 15199 _refine_ls_number_restraints 180 _refine_ls_R_factor_all 0.1291 _refine_ls_R_factor_gt 0.1129 _refine_ls_restrained_S_all 1.104 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1581P)^2^+89.3127P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3549 _refine_ls_wR_factor_ref 0.3651 _refine_special_details SQUEEZE _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints Uanis(C00L) = Uanis(C02H) = Uanis(C02P) = Uanis(C02N) = Uanis(C02F) = Uanis(C01Q) = Uanis(C00M) = Uanis(C02I) = Uanis(C02Q) = Uanis(C02O) = Uanis(C02G) = Uanis(C2AA) 3. Rigid body (RIGU) restrains C02P, C02H, C00L, C01Q, C02F, C02N with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C00L, C02H, C02P, C02N, C02F, C01Q, C00M, C02I, C02Q, C02O, C02G, C2AA with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C00W, C01D, C025, C02J, C02L, C029 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C00Q, C01T, C02C, C02A, C01N, C01P with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C02D, C02B, C021, C01K, C018, C01U with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 4. Others Sof(C00M)=Sof(C02I)=Sof(H02U)=Sof(C02Q)=Sof(H02V)=Sof(C02O)=Sof(H02W)= Sof(C02G)=Sof(H02X)=Sof(C2AA)=Sof(H2AB)=1-FVAR(1) Sof(C00L)=Sof(C02H)=Sof(H02H)=Sof(C02P)=Sof(H02P)=Sof(C02N)=Sof(H02N)= Sof(C02F)=Sof(H02F)=Sof(C01Q)=Sof(H01Q)=FVAR(1) 5.a Secondary CH2 refined with riding coordinates: C01G(H01O,H01P), C01H(H01R,H01S), C01M(H01Z,HB), C01V(H6AA,HG) 5.b Aromatic/amide H refined with riding coordinates: C00E(H00E), C02H(H02H), C02P(H02P), C02N(H02N), C02F(H02F), C01Q(H01Q), C00N(H00N), C00R(H00R), C00S(H00S), C00V(H00V), C00X(H00X), C00Y(H00Y), C010(H010), C012(H012), C016(H016), C017(H017), C01A(H01G), C01C(H01K), C01D(H01L), C01E(H01M), C01F(H01N), C01J(H01W), C01K(H01X), C01N(H01), C01P(H1AA), C01R(H2AA), C01T(H4AA), C01U(H5AA), C01W(H7AA), C01X(H8AA), C01Z(H0BA), C021(H021), C022(H022), C023(H023), C025(H025), C029(H029), C02A(H02L), C02B(H02M), C02C(H02O), C02D(H02Q), C02E(H02R), C02J(H02S), C02L(H02T), C02I(H02U), C02Q(H02V), C02O(H02W), C02G(H02X), C2AA(H2AB) 5.c Fitted hexagon refined as free rotating group: C00L(C02H,C02P,C02N,C02F,C01Q), C00M(C02I,C02Q,C02O,C02G,C2AA) 5.d Idealised Me refined as rotating group: C011(H01A,H01B,H01C), C019(H01D,H01E,H01F), C01B(H01H,H01I,H01J), C01I(H01T, H01U,H01V), C01L(H01Y,H,HA), C01O(H0AA,HC,HD), C01S(H3AA,HE,HF), C01Y(H9AA,HH, HI), C024(H02A,H02B,H02C), C026(H02D,H02E,H02G), C028(H02I,H02J,H02K) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru01 Ru 0.21624(4) 0.71446(3) 0.31816(5) 0.0453(2) Uani 1 1 d . . . . . Ru02 Ru 0.79660(4) 0.71326(4) 0.42674(4) 0.0434(2) Uani 1 1 d . . . . . P003 P 0.75557(16) 0.79612(12) 0.35418(16) 0.0507(6) Uani 1 1 d . . . . . P7 P 0.73349(14) 0.65250(12) 0.33679(15) 0.0468(6) Uani 1 1 d . . . . . P005 P 0.26896(15) 0.64704(13) 0.25386(18) 0.0538(7) Uani 1 1 d . . . . . P006 P 0.25732(16) 0.79165(12) 0.25552(16) 0.0505(6) Uani 1 1 d . . . . . O007 O 0.5052(4) 0.7171(4) 0.3789(4) 0.0544(19) Uani 1 1 d . . . . . C008 C 0.0930(6) 0.7212(5) 0.3019(6) 0.048(2) Uani 1 1 d . . . . . C009 C 0.1887(6) 0.8410(5) 0.1969(6) 0.050(2) Uani 1 1 d . . . . . C00A C 0.7764(6) 0.6191(5) 0.2691(6) 0.049(2) Uani 1 1 d . . . . . C00B C 0.5095(6) 0.7084(5) 0.4500(6) 0.051(2) Uani 1 1 d . . . . . C00C C 0.4441(6) 0.7033(5) 0.4711(6) 0.047(2) Uani 1 1 d . . . . . C00D C 0.1707(7) 0.7318(6) 0.4118(6) 0.060(3) Uani 1 1 d . . . . . C00E C 0.8436(7) 0.6409(6) 0.2645(6) 0.058(3) Uani 1 1 d . . . . . H00E H 0.867542 0.671906 0.295733 0.069 Uiso 1 1 calc R . . . . C00F C 0.5774(6) 0.7038(5) 0.4963(6) 0.050(2) Uani 1 1 d . . . . . C00G C 0.6432(6) 0.7099(5) 0.4715(8) 0.060(3) Uani 1 1 d . . . . . C00H C 0.1272(7) 0.7665(5) 0.3550(6) 0.056(3) Uani 1 1 d . . . . . C00I C 0.1155(6) 0.6588(5) 0.3258(7) 0.058(3) Uani 1 1 d . . . . . C00J C 0.6992(6) 0.7123(5) 0.4524(6) 0.049(2) Uani 1 1 d . . . . . C00K C 0.3154(7) 0.7125(5) 0.3791(6) 0.053(3) Uani 1 1 d . . . . . C00L C 0.6850(10) 0.5821(8) 0.3564(12) 0.074(2) Uani 0.578(16) 1 d . U P A 1 C02H C 0.6100(10) 0.5860(7) 0.3484(10) 0.074(2) Uani 0.578(16) 1 d G U P A 1 H02H H 0.585481 0.623700 0.331671 0.089 Uiso 0.578(16) 1 calc R . P A 1 C02P C 0.5718(8) 0.5337(7) 0.3654(11) 0.074(2) Uani 0.578(16) 1 d G U P A 1 H02P H 0.521612 0.536318 0.360079 0.089 Uiso 0.578(16) 1 calc R . P A 1 C02N C 0.6084(9) 0.4774(6) 0.3904(10) 0.074(2) Uani 0.578(16) 1 d G U P A 1 H02N H 0.582843 0.442368 0.401794 0.089 Uiso 0.578(16) 1 calc R . P A 1 C02F C 0.6834(9) 0.4735(7) 0.3984(10) 0.074(2) Uani 0.578(16) 1 d G U P A 1 H02F H 0.707946 0.435798 0.415100 0.089 Uiso 0.578(16) 1 calc R . P A 1 C01Q C 0.7217(8) 0.5258(10) 0.3814(13) 0.074(2) Uani 0.578(16) 1 d G U P A 1 H01Q H 0.771817 0.523180 0.386692 0.089 Uiso 0.578(16) 1 calc R . P A 1 C00N C 0.1735(7) 0.9039(5) 0.2139(7) 0.062(3) Uani 1 1 d . . . . . H00N H 0.203381 0.923182 0.253082 0.074 Uiso 1 1 calc R . . . . C00O C 0.8906(6) 0.7581(6) 0.5063(6) 0.058(3) Uani 1 1 d . . . . . C00P C 0.2197(7) 0.6163(5) 0.1685(7) 0.060(3) Uani 1 1 d . . . . . C00Q C 0.6967(7) 0.8579(5) 0.3793(8) 0.066(3) Uani 1 1 d . U . . . C00R C 0.1488(7) 0.6356(6) 0.1361(8) 0.067(3) Uani 1 1 d . . . . . H00R H 0.125414 0.664127 0.160179 0.080 Uiso 1 1 calc R . . . . C00S C 0.7418(7) 0.5725(6) 0.2223(6) 0.063(3) Uani 1 1 d . . . . . H00S H 0.696796 0.556770 0.226029 0.076 Uiso 1 1 calc R . . . . C00T C 0.8216(6) 0.8499(5) 0.3256(7) 0.056(3) Uani 1 1 d . . . . . C00U C 0.8997(7) 0.6563(6) 0.4656(6) 0.060(3) Uani 1 1 d . . . . . C00V C 0.8580(8) 0.8297(6) 0.2753(7) 0.067(3) Uani 1 1 d . . . . . H00V H 0.847745 0.789333 0.254899 0.080 Uiso 1 1 calc R . . . . C00W C 0.3072(7) 0.5727(6) 0.2978(8) 0.068(3) Uani 1 1 d . U . . . C00X C 0.8407(7) 0.9087(5) 0.3574(7) 0.064(3) Uani 1 1 d . . . . . H00X H 0.817826 0.922770 0.391940 0.076 Uiso 1 1 calc R . . . . C00Y C 0.2518(8) 0.5750(6) 0.1286(8) 0.066(3) Uani 1 1 d . . . . . H00Y H 0.299081 0.560938 0.147470 0.080 Uiso 1 1 calc R . . . . C00Z C 0.8569(6) 0.6527(6) 0.5173(6) 0.058(3) Uani 1 1 d . . . . . C010 C 0.4478(8) 0.6923(6) 0.5445(7) 0.070(4) Uani 1 1 d . . . . . H010 H 0.405379 0.687375 0.560405 0.084 Uiso 1 1 calc R . . . . C011 C 0.2107(8) 0.7593(9) 0.4817(8) 0.083(4) Uani 1 1 d . . . . . H01A H 0.258063 0.739953 0.495546 0.125 Uiso 1 1 calc GR . . . . H01B H 0.183741 0.750530 0.516558 0.125 Uiso 1 1 calc GR . . . . H01C H 0.215883 0.804948 0.477299 0.125 Uiso 1 1 calc GR . . . . C012 C 0.5787(7) 0.6933(6) 0.5667(7) 0.066(3) Uani 1 1 d . . . . . H012 H 0.623565 0.688891 0.598296 0.079 Uiso 1 1 calc R . . . . C013 C 0.8510(6) 0.7167(6) 0.5417(5) 0.057(3) Uani 1 1 d . . . . . C014 C 0.1635(7) 0.6647(6) 0.3944(7) 0.063(3) Uani 1 1 d . . . . . C015 C 0.9194(6) 0.7214(6) 0.4582(6) 0.056(3) Uani 1 1 d . . . . . C016 C 0.5164(7) 0.6891(7) 0.5919(7) 0.067(3) Uani 1 1 d . . . . . H016 H 0.519795 0.684299 0.639876 0.080 Uiso 1 1 calc R . . . . C017 C 0.9094(9) 0.8684(7) 0.2550(9) 0.083(4) Uani 1 1 d . . . . . H017 H 0.932009 0.854998 0.219991 0.100 Uiso 1 1 calc R . . . . C018 C 0.3173(7) 0.8552(6) 0.3025(8) 0.069(3) Uani 1 1 d . U . . . C019 C 0.1115(7) 0.8371(6) 0.3559(7) 0.064(3) Uani 1 1 d . . . . . H01D H 0.152014 0.858690 0.385986 0.095 Uiso 1 1 calc GR . . . . H01E H 0.068552 0.843911 0.373139 0.095 Uiso 1 1 calc GR . . . . H01F H 0.104026 0.854017 0.309024 0.095 Uiso 1 1 calc GR . . . . C01A C 0.8756(8) 0.6163(7) 0.2130(8) 0.073(4) Uani 1 1 d . . . . . H01G H 0.921061 0.631490 0.209826 0.088 Uiso 1 1 calc R . . . . C01B C 0.0351(7) 0.7380(7) 0.2380(7) 0.068(3) Uani 1 1 d . . . . . H01H H 0.046439 0.778573 0.219682 0.101 Uiso 1 1 calc GR . . . . H01I H -0.011056 0.741024 0.250466 0.101 Uiso 1 1 calc GR . . . . H01J H 0.032706 0.705316 0.202947 0.101 Uiso 1 1 calc GR . . . . C01C C 0.1425(8) 0.8147(7) 0.1362(6) 0.068(3) Uani 1 1 d . . . . . H01K H 0.150663 0.773343 0.121866 0.082 Uiso 1 1 calc R . . . . C01D C 0.2648(8) 0.5179(6) 0.2910(8) 0.071(3) Uani 1 1 d . U . . . H01L H 0.220853 0.517579 0.257469 0.085 Uiso 1 1 calc R . . . . C01E C 0.1122(8) 0.6153(7) 0.0719(8) 0.076(4) Uani 1 1 d . . . . . H01M H 0.064867 0.629201 0.053179 0.091 Uiso 1 1 calc R . . . . C01F C 0.8423(9) 0.5707(7) 0.1673(8) 0.078(4) Uani 1 1 d . . . . . H01N H 0.865496 0.553974 0.134177 0.093 Uiso 1 1 calc R . . . . C01G C 0.3437(7) 0.6920(6) 0.2293(8) 0.070(4) Uani 1 1 d . . . . . H01O H 0.382552 0.700300 0.270521 0.084 Uiso 1 1 calc R . . . . H01P H 0.363467 0.667659 0.195746 0.084 Uiso 1 1 calc R . . . . C01H C 0.3112(8) 0.7550(6) 0.1967(8) 0.074(4) Uani 1 1 d . . . . . H01R H 0.279949 0.747120 0.150517 0.089 Uiso 1 1 calc R . . . . H01S H 0.349722 0.784091 0.191387 0.089 Uiso 1 1 calc R . . . . C01I C 0.9736(7) 0.7450(9) 0.4187(7) 0.081(4) Uani 1 1 d . . . . . H01T H 0.976433 0.714983 0.382129 0.122 Uiso 1 1 calc GR . . . . H01U H 1.020556 0.748967 0.450434 0.122 Uiso 1 1 calc GR . . . . H01V H 0.958428 0.786159 0.398228 0.122 Uiso 1 1 calc GR . . . . C01J C 0.7735(8) 0.5490(6) 0.1697(7) 0.068(3) Uani 1 1 d . . . . . H01W H 0.749025 0.519324 0.136976 0.081 Uiso 1 1 calc R . . . . C01K C 0.3207(8) 0.8669(6) 0.3711(9) 0.079(3) Uani 1 1 d . U . . . H01X H 0.294626 0.840903 0.395130 0.095 Uiso 1 1 calc R . . . . C01L C 0.5056(8) 0.7826(6) 0.3582(8) 0.074(4) Uani 1 1 d . . . . . H01Y H 0.507691 0.784946 0.309697 0.111 Uiso 1 1 calc GR . . . . H H 0.547372 0.803786 0.386759 0.111 Uiso 1 1 calc GR . . . . HA H 0.462078 0.803305 0.364288 0.111 Uiso 1 1 calc GR . . . . C01M C 0.6988(7) 0.7664(6) 0.2705(8) 0.072(4) Uani 1 1 d . . . . . H01Z H 0.661727 0.797923 0.251149 0.086 Uiso 1 1 calc R . . . . HB H 0.728767 0.759938 0.236985 0.086 Uiso 1 1 calc R . . . . C01N C 0.6112(9) 0.9467(7) 0.3571(13) 0.103(5) Uani 1 1 d . U . . . H01 H 0.581535 0.974056 0.325194 0.124 Uiso 1 1 calc R . . . . C01O C 0.0879(8) 0.5963(6) 0.2927(10) 0.085(5) Uani 1 1 d . . . . . H0AA H 0.081085 0.599500 0.242579 0.127 Uiso 1 1 calc GR . . . . HC H 0.042347 0.586192 0.303857 0.127 Uiso 1 1 calc GR . . . . HD H 0.122619 0.563036 0.310280 0.127 Uiso 1 1 calc GR . . . . C01P C 0.6555(8) 0.8996(6) 0.3327(10) 0.082(4) Uani 1 1 d . U . . . H1AA H 0.655959 0.897705 0.285285 0.098 Uiso 1 1 calc R . . . . C01R C 0.1165(8) 0.9380(7) 0.1752(9) 0.083(4) Uani 1 1 d . . . . . H2AA H 0.107420 0.979502 0.188559 0.099 Uiso 1 1 calc R . . . . C01S C 0.9048(8) 0.8285(7) 0.5218(8) 0.077(4) Uani 1 1 d . . . . . H3AA H 0.931945 0.845849 0.490298 0.115 Uiso 1 1 calc GR . . . . HE H 0.932234 0.833565 0.569467 0.115 Uiso 1 1 calc GR . . . . HF H 0.859280 0.850829 0.515626 0.115 Uiso 1 1 calc GR . . . . C01T C 0.6971(8) 0.8648(7) 0.4507(9) 0.079(3) Uani 1 1 d . U . . . H4AA H 0.726473 0.837985 0.483496 0.095 Uiso 1 1 calc R . . . . C01U C 0.3572(7) 0.8943(6) 0.2682(10) 0.083(4) Uani 1 1 d . U . . . H5AA H 0.356189 0.887673 0.220954 0.100 Uiso 1 1 calc R . . . . C01V C 0.6631(7) 0.7037(6) 0.2824(7) 0.065(3) Uani 1 1 d . . . . . H6AA H 0.642577 0.682866 0.237788 0.079 Uiso 1 1 calc R . . . . HG H 0.624248 0.711411 0.306205 0.079 Uiso 1 1 calc R . . . . C01W C 0.1459(10) 0.5737(7) 0.0343(8) 0.083(4) Uani 1 1 d . . . . . H7AA H 0.121229 0.559057 -0.009804 0.100 Uiso 1 1 calc R . . . . C01X C 0.0857(10) 0.8499(8) 0.0984(8) 0.094(5) Uani 1 1 d . . . . . H8AA H 0.055304 0.831216 0.059071 0.113 Uiso 1 1 calc R . . . . C01Y C 0.9281(9) 0.5977(8) 0.4341(8) 0.091(5) Uani 1 1 d . . . . . H9AA H 0.912110 0.559369 0.453395 0.136 Uiso 1 1 calc GR . . . . HH H 0.980350 0.598736 0.445023 0.136 Uiso 1 1 calc GR . . . . HI H 0.909775 0.597875 0.383986 0.136 Uiso 1 1 calc GR . . . . C01Z C 0.2173(9) 0.5540(6) 0.0631(9) 0.078(4) Uani 1 1 d . . . . . H0BA H 0.241057 0.526835 0.037951 0.094 Uiso 1 1 calc R . . . . C020 C 0.3755(7) 0.7104(6) 0.4199(8) 0.069(3) Uani 1 1 d . . . . . C021 C 0.3623(9) 0.9166(8) 0.4062(11) 0.103(5) Uani 1 1 d . U . . . H021 H 0.362485 0.924045 0.453117 0.123 Uiso 1 1 calc R . . . . C022 C 0.8923(8) 0.9467(6) 0.3391(10) 0.082(4) Uani 1 1 d . . . . . H022 H 0.904451 0.985977 0.361598 0.098 Uiso 1 1 calc R . . . . C023 C 0.9264(8) 0.9273(7) 0.2877(9) 0.086(5) Uani 1 1 d . . . . . H023 H 0.960838 0.953709 0.274920 0.104 Uiso 1 1 calc R . . . . C024 C 0.1991(9) 0.6112(8) 0.4435(10) 0.092(5) Uani 1 1 d . . . . . H02A H 0.191143 0.570779 0.419125 0.138 Uiso 1 1 calc GR . . . . H02B H 0.178179 0.609782 0.483707 0.138 Uiso 1 1 calc GR . . . . H02C H 0.250449 0.619147 0.458540 0.138 Uiso 1 1 calc GR . . . . C025 C 0.2846(10) 0.4638(7) 0.3315(10) 0.095(5) Uani 1 1 d . U . . . H025 H 0.255880 0.426978 0.323150 0.114 Uiso 1 1 calc R . . . . C026 C 0.8153(9) 0.7369(10) 0.5988(8) 0.093(5) Uani 1 1 d . . . . . H02D H 0.793427 0.778454 0.587862 0.139 Uiso 1 1 calc GR . . . . H02E H 0.851073 0.739046 0.642578 0.139 Uiso 1 1 calc GR . . . . H02G H 0.778454 0.706243 0.602553 0.139 Uiso 1 1 calc GR . . . . C028 C 0.8280(10) 0.5932(8) 0.5441(9) 0.101(6) Uani 1 1 d . . . . . H02I H 0.797737 0.604918 0.575351 0.151 Uiso 1 1 calc GR . . . . H02J H 0.867871 0.567372 0.568987 0.151 Uiso 1 1 calc GR . . . . H02K H 0.799811 0.569188 0.505257 0.151 Uiso 1 1 calc GR . . . . C029 C 0.3721(9) 0.5720(7) 0.3486(10) 0.095(5) Uani 1 1 d . U . . . H029 H 0.403260 0.607270 0.354312 0.113 Uiso 1 1 calc R . . . . C02A C 0.6128(10) 0.9512(9) 0.4261(14) 0.115(6) Uani 1 1 d . U . . . H02L H 0.584695 0.982389 0.441300 0.138 Uiso 1 1 calc R . . . . C02B C 0.4008(11) 0.9530(9) 0.3757(15) 0.124(7) Uani 1 1 d . U . . . H02M H 0.429546 0.985200 0.401007 0.149 Uiso 1 1 calc R . . . . C02C C 0.6540(9) 0.9115(8) 0.4737(13) 0.106(5) Uani 1 1 d . U . . . H02O H 0.654042 0.914911 0.521098 0.127 Uiso 1 1 calc R . . . . C02D C 0.3994(8) 0.9442(7) 0.3062(14) 0.107(5) Uani 1 1 d . U . . . H02Q H 0.426309 0.971126 0.283863 0.128 Uiso 1 1 calc R . . . . C02E C 0.0717(10) 0.9105(8) 0.1156(9) 0.090(5) Uani 1 1 d . . . . . H02R H 0.033088 0.933550 0.088237 0.108 Uiso 1 1 calc R . . . . C02J C 0.3458(11) 0.4646(9) 0.3832(13) 0.120(7) Uani 1 1 d . U . . . H02S H 0.357902 0.429582 0.413233 0.144 Uiso 1 1 calc R . . . . C02L C 0.3901(10) 0.5178(9) 0.3910(13) 0.123(7) Uani 1 1 d . U . . . H02T H 0.433335 0.517640 0.425560 0.148 Uiso 1 1 calc R . . . . C00M C 0.6895(15) 0.5799(11) 0.3625(16) 0.074(2) Uani 0.422(16) 1 d . U P A 2 C02I C 0.6247(13) 0.5796(9) 0.3845(14) 0.074(2) Uani 0.422(16) 1 d G U P A 2 H02U H 0.594900 0.615743 0.377791 0.089 Uiso 0.422(16) 1 calc R . P A 2 C02Q C 0.6043(12) 0.5252(10) 0.4165(14) 0.074(2) Uani 0.422(16) 1 d G U P A 2 H02V H 0.560955 0.525003 0.431277 0.089 Uiso 0.422(16) 1 calc R . P A 2 C02O C 0.6488(13) 0.4712(9) 0.4266(13) 0.074(2) Uani 0.422(16) 1 d G U P A 2 H02W H 0.635233 0.434803 0.448004 0.089 Uiso 0.422(16) 1 calc R . P A 2 C02G C 0.7137(12) 0.4715(11) 0.4045(15) 0.074(2) Uani 0.422(16) 1 d G U P A 2 H02X H 0.743457 0.435343 0.411244 0.089 Uiso 0.422(16) 1 calc R . P A 2 C2AA C 0.7340(13) 0.5259(13) 0.3725(18) 0.074(2) Uani 0.422(16) 1 d G U P A 2 H2AB H 0.777403 0.526082 0.357758 0.089 Uiso 0.422(16) 1 calc R . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru01 0.0396(4) 0.0353(4) 0.0644(5) 0.0025(3) 0.0192(4) 0.0024(3) Ru02 0.0410(4) 0.0415(4) 0.0472(4) -0.0006(3) 0.0093(3) -0.0038(3) P003 0.0545(16) 0.0371(12) 0.0645(17) -0.0039(11) 0.0221(13) 0.0013(11) P7 0.0439(13) 0.0398(13) 0.0554(14) -0.0050(11) 0.0089(11) -0.0038(10) P005 0.0440(14) 0.0385(13) 0.086(2) -0.0065(13) 0.0291(14) 0.0017(11) P006 0.0538(16) 0.0351(12) 0.0657(17) 0.0019(11) 0.0200(13) -0.0033(11) O007 0.055(5) 0.056(5) 0.053(4) 0.007(3) 0.013(4) -0.001(3) C008 0.039(5) 0.051(6) 0.061(6) -0.007(5) 0.024(5) 0.002(4) C009 0.053(6) 0.037(5) 0.054(6) 0.004(4) 0.002(5) -0.008(4) C00A 0.050(6) 0.041(5) 0.056(6) -0.003(4) 0.011(5) -0.002(4) C00B 0.046(6) 0.045(5) 0.059(6) 0.005(5) 0.006(5) 0.008(4) C00C 0.043(5) 0.037(5) 0.064(6) 0.008(4) 0.019(5) 0.004(4) C00D 0.064(7) 0.073(8) 0.051(6) 0.000(6) 0.027(5) -0.004(6) C00E 0.061(7) 0.053(6) 0.059(6) -0.008(5) 0.014(5) -0.011(5) C00F 0.058(6) 0.041(5) 0.057(6) 0.005(4) 0.023(5) 0.003(4) C00G 0.038(6) 0.053(6) 0.092(9) -0.002(6) 0.021(6) 0.000(5) C00H 0.059(7) 0.048(6) 0.062(7) -0.002(5) 0.020(5) 0.003(5) C00I 0.053(6) 0.043(6) 0.087(8) 0.001(5) 0.037(6) -0.005(5) C00J 0.053(6) 0.036(5) 0.052(6) 0.001(4) 0.001(5) -0.006(4) C00K 0.057(7) 0.045(6) 0.058(6) 0.003(5) 0.017(5) 0.001(5) C00L 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02H 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02P 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02N 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02F 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C01Q 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C00N 0.065(7) 0.041(6) 0.074(8) 0.002(5) 0.005(6) 0.004(5) C00O 0.054(6) 0.059(7) 0.057(6) -0.009(5) 0.008(5) -0.016(5) C00P 0.062(7) 0.038(5) 0.087(8) 0.004(5) 0.031(6) 0.003(5) C00Q 0.067(7) 0.036(5) 0.097(7) -0.005(5) 0.025(6) -0.013(4) C00R 0.060(7) 0.048(6) 0.097(10) 0.015(6) 0.029(7) 0.008(5) C00S 0.068(8) 0.059(7) 0.056(7) -0.009(5) 0.001(6) -0.013(6) C00T 0.053(6) 0.043(5) 0.074(7) 0.010(5) 0.020(5) 0.014(5) C00U 0.055(6) 0.075(8) 0.046(6) 0.005(5) 0.002(5) 0.011(6) C00V 0.082(9) 0.057(7) 0.069(8) 0.009(6) 0.032(7) 0.020(6) C00W 0.067(7) 0.042(5) 0.092(9) -0.006(6) 0.014(6) 0.010(5) C00X 0.072(8) 0.044(6) 0.085(8) -0.002(6) 0.038(7) -0.007(5) C00Y 0.072(8) 0.049(6) 0.087(9) -0.004(6) 0.037(7) 0.004(6) C00Z 0.055(6) 0.064(7) 0.052(6) 0.014(5) 0.002(5) -0.001(5) C010 0.082(9) 0.060(7) 0.081(9) 0.008(6) 0.045(8) -0.012(7) C011 0.068(9) 0.111(12) 0.076(9) -0.013(9) 0.027(7) 0.010(8) C012 0.052(7) 0.064(7) 0.070(8) 0.002(6) -0.007(6) 0.007(6) C013 0.052(6) 0.082(8) 0.033(5) -0.006(5) 0.003(4) -0.014(6) C014 0.059(7) 0.063(7) 0.080(8) 0.019(6) 0.039(6) 0.010(6) C015 0.043(6) 0.085(8) 0.038(5) 0.009(5) 0.002(4) -0.013(5) C016 0.062(7) 0.091(9) 0.052(6) 0.019(6) 0.020(6) -0.003(7) C017 0.093(11) 0.063(8) 0.102(11) 0.030(8) 0.042(9) 0.020(8) C018 0.053(6) 0.044(6) 0.097(7) 0.008(5) -0.008(6) 0.002(5) C019 0.053(6) 0.055(7) 0.088(9) -0.013(6) 0.026(6) 0.004(5) C01A 0.065(8) 0.077(9) 0.085(9) 0.001(7) 0.035(7) -0.005(7) C01B 0.047(6) 0.078(8) 0.079(8) -0.004(7) 0.019(6) 0.010(6) C01C 0.079(9) 0.067(8) 0.052(7) -0.001(6) 0.003(6) 0.000(7) C01D 0.077(8) 0.050(6) 0.087(9) 0.002(5) 0.024(6) 0.002(5) C01E 0.074(9) 0.071(9) 0.084(10) 0.003(7) 0.019(8) 0.000(7) C01F 0.098(11) 0.065(8) 0.081(9) -0.003(7) 0.043(8) 0.004(8) C01G 0.054(7) 0.059(7) 0.108(11) -0.020(7) 0.042(7) -0.006(6) C01H 0.075(9) 0.059(7) 0.105(10) -0.004(7) 0.052(8) -0.016(6) C01I 0.043(6) 0.135(14) 0.067(8) 0.006(9) 0.015(6) -0.013(8) C01J 0.094(10) 0.049(6) 0.065(7) -0.010(5) 0.028(7) -0.007(6) C01K 0.077(8) 0.049(6) 0.098(7) 0.001(6) -0.008(7) 0.002(6) C01L 0.067(9) 0.067(8) 0.092(10) 0.024(7) 0.026(8) 0.004(6) C01M 0.064(8) 0.055(7) 0.082(9) 0.012(6) -0.009(7) 0.010(6) C01N 0.061(8) 0.051(7) 0.201(14) -0.009(9) 0.039(10) -0.003(6) C01O 0.075(9) 0.057(8) 0.137(14) -0.014(8) 0.055(9) -0.018(7) C01P 0.075(8) 0.041(6) 0.134(10) 0.014(6) 0.033(8) 0.001(5) C01R 0.080(10) 0.060(8) 0.101(11) 0.015(8) 0.005(8) 0.008(7) C01S 0.076(9) 0.071(9) 0.080(9) -0.019(7) 0.013(7) -0.022(7) C01T 0.080(9) 0.060(7) 0.106(8) -0.022(7) 0.037(7) -0.010(6) C01U 0.057(7) 0.049(6) 0.135(11) 0.023(6) 0.004(7) -0.005(5) C01V 0.049(6) 0.055(7) 0.079(8) -0.021(6) -0.010(6) 0.010(5) C01W 0.109(13) 0.063(8) 0.078(9) -0.001(7) 0.023(9) -0.011(8) C01X 0.107(12) 0.090(11) 0.066(9) 0.017(8) -0.019(8) -0.010(9) C01Y 0.084(10) 0.091(11) 0.088(10) 0.000(8) -0.002(8) 0.041(9) C01Z 0.092(11) 0.051(7) 0.101(11) -0.005(7) 0.044(9) 0.003(7) C020 0.048(7) 0.063(8) 0.093(10) 0.005(7) 0.013(7) -0.002(5) C021 0.081(10) 0.062(8) 0.142(12) -0.029(8) -0.023(8) 0.016(6) C022 0.072(9) 0.046(7) 0.134(13) 0.008(8) 0.037(9) -0.003(6) C023 0.075(9) 0.066(9) 0.128(13) 0.029(9) 0.043(9) 0.000(7) C024 0.084(10) 0.076(10) 0.122(13) 0.037(9) 0.037(10) 0.011(8) C025 0.113(11) 0.049(7) 0.122(12) 0.012(7) 0.028(8) 0.010(7) C026 0.083(10) 0.137(15) 0.066(9) -0.015(9) 0.033(8) -0.012(10) C028 0.118(14) 0.095(12) 0.079(10) 0.032(9) 0.002(9) -0.031(10) C029 0.070(8) 0.058(7) 0.142(13) 0.018(8) -0.002(8) 0.000(6) C02A 0.076(10) 0.068(9) 0.207(15) -0.047(10) 0.046(11) -0.006(7) C02B 0.084(11) 0.059(9) 0.203(15) -0.027(10) -0.019(11) -0.009(7) C02C 0.079(10) 0.078(10) 0.173(14) -0.046(9) 0.058(10) -0.011(7) C02D 0.060(8) 0.043(7) 0.207(15) 0.013(9) 0.009(10) -0.005(5) C02E 0.094(11) 0.081(10) 0.083(10) 0.019(8) -0.004(8) 0.009(9) C02J 0.111(12) 0.072(9) 0.168(17) 0.049(11) 0.013(10) 0.019(8) C02L 0.081(10) 0.085(10) 0.19(2) 0.051(11) 0.003(11) 0.021(7) C00M 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02I 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02Q 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02O 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C02G 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) C2AA 0.076(5) 0.064(4) 0.087(5) -0.001(4) 0.032(5) -0.021(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru01 P005 2.264(3) . ? Ru01 P006 2.264(3) . ? Ru01 C008 2.278(10) . ? Ru01 C00D 2.227(11) . ? Ru01 C00H 2.254(11) . ? Ru01 C00I 2.262(11) . ? Ru01 C00K 1.972(12) . ? Ru01 C014 2.232(11) . ? Ru02 P003 2.252(3) . ? Ru02 P7 2.265(3) . ? Ru02 C00J 2.016(12) . ? Ru02 C00O 2.269(11) . ? Ru02 C00U 2.254(12) . ? Ru02 C00Z 2.253(11) . ? Ru02 C013 2.243(10) . ? Ru02 C015 2.262(11) . ? P003 C00Q 1.840(13) . ? P003 C00T 1.856(12) . ? P003 C01M 1.841(14) . ? P7 C00A 1.842(11) . ? P7 C00L 1.815(11) . ? P7 C01V 1.836(12) . ? P7 C00M 1.849(16) . ? P005 C00P 1.826(14) . ? P005 C00W 1.835(13) . ? P005 C01G 1.849(12) . ? P006 C009 1.831(11) . ? P006 C018 1.841(13) . ? P006 C01H 1.867(13) . ? O007 C00B 1.387(14) . ? O007 C01L 1.422(15) . ? C008 C00H 1.438(16) . ? C008 C00I 1.411(15) . ? C008 C01B 1.497(17) . ? C009 C00N 1.397(15) . ? C009 C01C 1.408(16) . ? C00A C00E 1.369(16) . ? C00A C00S 1.387(15) . ? C00B C00C 1.395(15) . ? C00B C00F 1.389(16) . ? C00C C010 1.439(17) . ? C00C C020 1.447(17) . ? C00D C00H 1.413(17) . ? C00D C011 1.511(19) . ? C00D C014 1.437(18) . ? C00E H00E 0.9300 . ? C00E C01A 1.389(17) . ? C00F C00G 1.440(16) . ? C00F C012 1.388(17) . ? C00G C00J 1.204(16) . ? C00H C019 1.501(16) . ? C00I C014 1.437(19) . ? C00I C01O 1.491(17) . ? C00K C020 1.225(18) . ? C00L C02H 1.3900 . ? C00L C01Q 1.3900 . ? C02H H02H 0.9300 . ? C02H C02P 1.3900 . ? C02P H02P 0.9300 . ? C02P C02N 1.3900 . ? C02N H02N 0.9300 . ? C02N C02F 1.3900 . ? C02F H02F 0.9300 . ? C02F C01Q 1.3900 . ? C01Q H01Q 0.9300 . ? C00N H00N 0.9300 . ? C00N C01R 1.362(18) . ? C00O C013 1.421(16) . ? C00O C015 1.415(17) . ? C00O C01S 1.507(17) . ? C00P C00R 1.400(17) . ? C00P C00Y 1.392(16) . ? C00Q C01P 1.36(2) . ? C00Q C01T 1.40(2) . ? C00R H00R 0.9300 . ? C00R C01E 1.35(2) . ? C00S H00S 0.9300 . ? C00S C01J 1.393(18) . ? C00T C00V 1.389(17) . ? C00T C00X 1.383(16) . ? C00U C00Z 1.436(17) . ? C00U C015 1.420(17) . ? C00U C01Y 1.520(19) . ? C00V H00V 0.9300 . ? C00V C017 1.39(2) . ? C00W C01D 1.381(18) . ? C00W C029 1.39(2) . ? C00X H00X 0.9300 . ? C00X C022 1.366(17) . ? C00Y H00Y 0.9300 . ? C00Y C01Z 1.37(2) . ? C00Z C013 1.428(17) . ? C00Z C028 1.496(18) . ? C010 H010 0.9300 . ? C010 C016 1.409(19) . ? C011 H01A 0.9600 . ? C011 H01B 0.9600 . ? C011 H01C 0.9600 . ? C012 H012 0.9300 . ? C012 C016 1.380(18) . ? C013 C026 1.493(17) . ? C014 C024 1.521(18) . ? C015 C01I 1.503(16) . ? C016 H016 0.9300 . ? C017 H017 0.9300 . ? C017 C023 1.38(2) . ? C018 C01K 1.35(2) . ? C018 C01U 1.38(2) . ? C019 H01D 0.9600 . ? C019 H01E 0.9600 . ? C019 H01F 0.9600 . ? C01A H01G 0.9300 . ? C01A C01F 1.35(2) . ? C01B H01H 0.9600 . ? C01B H01I 0.9600 . ? C01B H01J 0.9600 . ? C01C H01K 0.9300 . ? C01C C01X 1.36(2) . ? C01D H01L 0.9300 . ? C01D C025 1.377(19) . ? C01E H01M 0.9300 . ? C01E C01W 1.38(2) . ? C01F H01N 0.9300 . ? C01F C01J 1.39(2) . ? C01G H01O 0.9700 . ? C01G H01P 0.9700 . ? C01G C01H 1.52(2) . ? C01H H01R 0.9700 . ? C01H H01S 0.9700 . ? C01I H01T 0.9600 . ? C01I H01U 0.9600 . ? C01I H01V 0.9600 . ? C01J H01W 0.9300 . ? C01K H01X 0.9300 . ? C01K C021 1.38(2) . ? C01L H01Y 0.9600 . ? C01L H 0.9600 . ? C01L HA 0.9600 . ? C01M H01Z 0.9700 . ? C01M HB 0.9700 . ? C01M C01V 1.512(18) . ? C01N H01 0.9300 . ? C01N C01P 1.44(2) . ? C01N C02A 1.35(3) . ? C01O H0AA 0.9600 . ? C01O HC 0.9600 . ? C01O HD 0.9600 . ? C01P H1AA 0.9300 . ? C01R H2AA 0.9300 . ? C01R C02E 1.39(2) . ? C01S H3AA 0.9600 . ? C01S HE 0.9600 . ? C01S HF 0.9600 . ? C01T H4AA 0.9300 . ? C01T C02C 1.41(2) . ? C01U H5AA 0.9300 . ? C01U C02D 1.41(2) . ? C01V H6AA 0.9700 . ? C01V HG 0.9700 . ? C01W H7AA 0.9300 . ? C01W C01Z 1.40(2) . ? C01X H8AA 0.9300 . ? C01X C02E 1.35(2) . ? C01Y H9AA 0.9600 . ? C01Y HH 0.9600 . ? C01Y HI 0.9600 . ? C01Z H0BA 0.9300 . ? C021 H021 0.9300 . ? C021 C02B 1.29(3) . ? C022 H022 0.9300 . ? C022 C023 1.38(2) . ? C023 H023 0.9300 . ? C024 H02A 0.9600 . ? C024 H02B 0.9600 . ? C024 H02C 0.9600 . ? C025 H025 0.9300 . ? C025 C02J 1.35(3) . ? C026 H02D 0.9600 . ? C026 H02E 0.9600 . ? C026 H02G 0.9600 . ? C028 H02I 0.9600 . ? C028 H02J 0.9600 . ? C028 H02K 0.9600 . ? C029 H029 0.9300 . ? C029 C02L 1.39(2) . ? C02A H02L 0.9300 . ? C02A C02C 1.35(3) . ? C02B H02M 0.9300 . ? C02B C02D 1.37(3) . ? C02C H02O 0.9300 . ? C02D H02Q 0.9300 . ? C02E H02R 0.9300 . ? C02J H02S 0.9300 . ? C02J C02L 1.38(3) . ? C02L H02T 0.9300 . ? C00M C02I 1.3900 . ? C00M C2AA 1.3900 . ? C02I H02U 0.9300 . ? C02I C02Q 1.3900 . ? C02Q H02V 0.9300 . ? C02Q C02O 1.3900 . ? C02O H02W 0.9300 . ? C02O C02G 1.3900 . ? C02G H02X 0.9300 . ? C02G C2AA 1.3900 . ? C2AA H2AB 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P005 Ru01 C008 121.9(3) . . ? P006 Ru01 P005 83.58(11) . . ? P006 Ru01 C008 110.4(3) . . ? C00D Ru01 P005 149.5(4) . . ? C00D Ru01 P006 125.2(4) . . ? C00D Ru01 C008 61.7(4) . . ? C00D Ru01 C00H 36.8(4) . . ? C00D Ru01 C00I 62.3(5) . . ? C00D Ru01 C014 37.6(5) . . ? C00H Ru01 P005 158.8(3) . . ? C00H Ru01 P006 102.0(3) . . ? C00H Ru01 C008 37.0(4) . . ? C00H Ru01 C00I 61.5(4) . . ? C00I Ru01 P005 101.9(3) . . ? C00I Ru01 P006 143.0(3) . . ? C00I Ru01 C008 36.2(4) . . ? C00K Ru01 P005 81.0(3) . . ? C00K Ru01 P006 86.8(3) . . ? C00K Ru01 C008 151.7(5) . . ? C00K Ru01 C00D 90.1(5) . . ? C00K Ru01 C00H 119.4(5) . . ? C00K Ru01 C00I 130.1(5) . . ? C00K Ru01 C014 95.5(5) . . ? C014 Ru01 P005 114.0(3) . . ? C014 Ru01 P006 162.4(3) . . ? C014 Ru01 C008 61.4(4) . . ? C014 Ru01 C00H 61.7(4) . . ? C014 Ru01 C00I 37.3(5) . . ? P003 Ru02 P7 84.09(10) . . ? P003 Ru02 C00O 102.5(3) . . ? P003 Ru02 C00U 139.3(3) . . ? P003 Ru02 C00Z 163.6(3) . . ? P003 Ru02 C015 107.1(3) . . ? P7 Ru02 C00O 161.2(3) . . ? C00J Ru02 P003 88.0(3) . . ? C00J Ru02 P7 80.9(3) . . ? C00J Ru02 C00O 116.5(4) . . ? C00J Ru02 C00U 132.6(4) . . ? C00J Ru02 C00Z 97.0(4) . . ? C00J Ru02 C013 89.0(4) . . ? C00J Ru02 C015 150.4(4) . . ? C00U Ru02 P7 103.0(3) . . ? C00U Ru02 C00O 60.6(5) . . ? C00U Ru02 C015 36.7(4) . . ? C00Z Ru02 P7 112.1(3) . . ? C00Z Ru02 C00O 61.4(4) . . ? C00Z Ru02 C00U 37.2(4) . . ? C00Z Ru02 C015 62.0(4) . . ? C013 Ru02 P003 128.0(3) . . ? C013 Ru02 P7 146.2(3) . . ? C013 Ru02 C00O 36.7(4) . . ? C013 Ru02 C00U 61.4(4) . . ? C013 Ru02 C00Z 37.0(4) . . ? C013 Ru02 C015 61.6(4) . . ? C015 Ru02 P7 124.9(3) . . ? C015 Ru02 C00O 36.4(4) . . ? C00Q P003 Ru02 120.5(5) . . ? C00Q P003 C00T 98.6(5) . . ? C00Q P003 C01M 102.1(6) . . ? C00T P003 Ru02 119.6(4) . . ? C01M P003 Ru02 110.2(4) . . ? C01M P003 C00T 103.1(6) . . ? C00A P7 Ru02 121.9(4) . . ? C00A P7 C00M 100.8(10) . . ? C00L P7 Ru02 119.1(7) . . ? C00L P7 C00A 100.1(8) . . ? C00L P7 C01V 104.9(8) . . ? C01V P7 Ru02 107.7(4) . . ? C01V P7 C00A 100.6(6) . . ? C01V P7 C00M 108.7(11) . . ? C00M P7 Ru02 115.7(10) . . ? C00P P005 Ru01 121.9(4) . . ? C00P P005 C00W 101.2(6) . . ? C00P P005 C01G 101.3(6) . . ? C00W P005 Ru01 116.0(5) . . ? C00W P005 C01G 107.9(6) . . ? C01G P005 Ru01 107.0(4) . . ? C009 P006 Ru01 117.0(4) . . ? C009 P006 C018 99.9(5) . . ? C009 P006 C01H 104.5(6) . . ? C018 P006 Ru01 119.2(5) . . ? C018 P006 C01H 103.9(7) . . ? C01H P006 Ru01 110.4(4) . . ? C00B O007 C01L 114.0(10) . . ? C00H C008 Ru01 70.6(6) . . ? C00H C008 C01B 124.6(10) . . ? C00I C008 Ru01 71.2(6) . . ? C00I C008 C00H 108.3(11) . . ? C00I C008 C01B 126.6(11) . . ? C01B C008 Ru01 130.9(8) . . ? C00N C009 P006 122.1(9) . . ? C00N C009 C01C 116.3(11) . . ? C01C C009 P006 121.3(9) . . ? C00E C00A P7 119.5(8) . . ? C00E C00A C00S 119.3(11) . . ? C00S C00A P7 121.3(9) . . ? O007 C00B C00C 117.2(10) . . ? O007 C00B C00F 119.4(10) . . ? C00F C00B C00C 123.4(11) . . ? C00B C00C C010 117.8(11) . . ? C00B C00C C020 120.0(11) . . ? C010 C00C C020 122.2(11) . . ? C00H C00D Ru01 72.7(6) . . ? C00H C00D C011 126.4(13) . . ? C00H C00D C014 107.7(11) . . ? C011 C00D Ru01 126.6(9) . . ? C014 C00D Ru01 71.4(6) . . ? C014 C00D C011 125.6(13) . . ? C00A C00E H00E 120.2 . . ? C00A C00E C01A 119.5(11) . . ? C01A C00E H00E 120.2 . . ? C00B C00F C00G 120.8(11) . . ? C012 C00F C00B 117.1(11) . . ? C012 C00F C00G 122.1(12) . . ? C00J C00G C00F 176.8(13) . . ? C008 C00H Ru01 72.4(6) . . ? C008 C00H C019 126.3(11) . . ? C00D C00H Ru01 70.6(7) . . ? C00D C00H C008 108.3(10) . . ? C00D C00H C019 124.8(11) . . ? C019 C00H Ru01 129.6(8) . . ? C008 C00I Ru01 72.5(6) . . ? C008 C00I C014 107.8(10) . . ? C008 C00I C01O 127.6(13) . . ? C014 C00I Ru01 70.2(6) . . ? C014 C00I C01O 124.0(12) . . ? C01O C00I Ru01 129.2(8) . . ? C00G C00J Ru02 176.0(11) . . ? C020 C00K Ru01 176.6(11) . . ? C02H C00L P7 118.7(11) . . ? C02H C00L C01Q 120.0 . . ? C01Q C00L P7 121.3(11) . . ? C00L C02H H02H 120.0 . . ? C00L C02H C02P 120.0 . . ? C02P C02H H02H 120.0 . . ? C02H C02P H02P 120.0 . . ? C02N C02P C02H 120.0 . . ? C02N C02P H02P 120.0 . . ? C02P C02N H02N 120.0 . . ? C02F C02N C02P 120.0 . . ? C02F C02N H02N 120.0 . . ? C02N C02F H02F 120.0 . . ? C02N C02F C01Q 120.0 . . ? C01Q C02F H02F 120.0 . . ? C00L C01Q H01Q 120.0 . . ? C02F C01Q C00L 120.0 . . ? C02F C01Q H01Q 120.0 . . ? C009 C00N H00N 118.8 . . ? C01R C00N C009 122.4(13) . . ? C01R C00N H00N 118.8 . . ? C013 C00O Ru02 70.7(6) . . ? C013 C00O C01S 125.4(11) . . ? C015 C00O Ru02 71.5(6) . . ? C015 C00O C013 108.9(11) . . ? C015 C00O C01S 125.5(11) . . ? C01S C00O Ru02 127.7(9) . . ? C00R C00P P005 122.9(10) . . ? C00Y C00P P005 122.2(10) . . ? C00Y C00P C00R 114.8(13) . . ? C01P C00Q P003 123.5(12) . . ? C01P C00Q C01T 118.0(14) . . ? C01T C00Q P003 118.3(11) . . ? C00P C00R H00R 118.1 . . ? C01E C00R C00P 123.9(13) . . ? C01E C00R H00R 118.1 . . ? C00A C00S H00S 119.5 . . ? C00A C00S C01J 121.0(12) . . ? C01J C00S H00S 119.5 . . ? C00V C00T P003 120.6(10) . . ? C00X C00T P003 121.4(9) . . ? C00X C00T C00V 117.8(12) . . ? C00Z C00U Ru02 71.4(7) . . ? C00Z C00U C01Y 123.6(13) . . ? C015 C00U Ru02 72.0(7) . . ? C015 C00U C00Z 109.0(11) . . ? C015 C00U C01Y 126.7(13) . . ? C01Y C00U Ru02 130.1(9) . . ? C00T C00V H00V 119.3 . . ? C00T C00V C017 121.4(13) . . ? C017 C00V H00V 119.3 . . ? C01D C00W P005 119.7(11) . . ? C01D C00W C029 117.2(13) . . ? C029 C00W P005 122.0(10) . . ? C00T C00X H00X 119.3 . . ? C022 C00X C00T 121.5(13) . . ? C022 C00X H00X 119.3 . . ? C00P C00Y H00Y 118.4 . . ? C01Z C00Y C00P 123.2(14) . . ? C01Z C00Y H00Y 118.4 . . ? C00U C00Z Ru02 71.5(6) . . ? C00U C00Z C028 127.0(14) . . ? C013 C00Z Ru02 71.1(6) . . ? C013 C00Z C00U 106.6(11) . . ? C013 C00Z C028 126.3(13) . . ? C028 C00Z Ru02 125.4(9) . . ? C00C C010 H010 120.4 . . ? C016 C010 C00C 119.2(11) . . ? C016 C010 H010 120.4 . . ? C00D C011 H01A 109.5 . . ? C00D C011 H01B 109.5 . . ? C00D C011 H01C 109.5 . . ? H01A C011 H01B 109.5 . . ? H01A C011 H01C 109.5 . . ? H01B C011 H01C 109.5 . . ? C00F C012 H012 118.4 . . ? C016 C012 C00F 123.1(11) . . ? C016 C012 H012 118.4 . . ? C00O C013 Ru02 72.6(6) . . ? C00O C013 C00Z 108.2(10) . . ? C00O C013 C026 125.1(13) . . ? C00Z C013 Ru02 71.9(6) . . ? C00Z C013 C026 126.5(12) . . ? C026 C013 Ru02 125.2(10) . . ? C00D C014 Ru01 71.0(6) . . ? C00D C014 C024 124.0(14) . . ? C00I C014 Ru01 72.5(6) . . ? C00I C014 C00D 107.9(10) . . ? C00I C014 C024 128.0(13) . . ? C024 C014 Ru01 124.1(9) . . ? C00O C015 Ru02 72.1(7) . . ? C00O C015 C00U 107.2(10) . . ? C00O C015 C01I 125.4(12) . . ? C00U C015 Ru02 71.4(6) . . ? C00U C015 C01I 126.2(13) . . ? C01I C015 Ru02 131.5(8) . . ? C010 C016 H016 120.3 . . ? C012 C016 C010 119.4(11) . . ? C012 C016 H016 120.3 . . ? C00V C017 H017 120.6 . . ? C023 C017 C00V 118.8(14) . . ? C023 C017 H017 120.6 . . ? C01K C018 P006 120.4(11) . . ? C01K C018 C01U 118.1(14) . . ? C01U C018 P006 121.4(13) . . ? C00H C019 H01D 109.5 . . ? C00H C019 H01E 109.5 . . ? C00H C019 H01F 109.5 . . ? H01D C019 H01E 109.5 . . ? H01D C019 H01F 109.5 . . ? H01E C019 H01F 109.5 . . ? C00E C01A H01G 119.2 . . ? C01F C01A C00E 121.5(13) . . ? C01F C01A H01G 119.2 . . ? C008 C01B H01H 109.5 . . ? C008 C01B H01I 109.5 . . ? C008 C01B H01J 109.5 . . ? H01H C01B H01I 109.5 . . ? H01H C01B H01J 109.5 . . ? H01I C01B H01J 109.5 . . ? C009 C01C H01K 119.9 . . ? C01X C01C C009 120.2(14) . . ? C01X C01C H01K 119.9 . . ? C00W C01D H01L 118.4 . . ? C025 C01D C00W 123.1(15) . . ? C025 C01D H01L 118.4 . . ? C00R C01E H01M 120.3 . . ? C00R C01E C01W 119.4(15) . . ? C01W C01E H01M 120.3 . . ? C01A C01F H01N 120.0 . . ? C01A C01F C01J 120.1(13) . . ? C01J C01F H01N 120.0 . . ? P005 C01G H01O 110.4 . . ? P005 C01G H01P 110.4 . . ? H01O C01G H01P 108.6 . . ? C01H C01G P005 106.7(8) . . ? C01H C01G H01O 110.4 . . ? C01H C01G H01P 110.4 . . ? P006 C01H H01R 110.0 . . ? P006 C01H H01S 110.0 . . ? C01G C01H P006 108.5(9) . . ? C01G C01H H01R 110.0 . . ? C01G C01H H01S 110.0 . . ? H01R C01H H01S 108.4 . . ? C015 C01I H01T 109.5 . . ? C015 C01I H01U 109.5 . . ? C015 C01I H01V 109.5 . . ? H01T C01I H01U 109.5 . . ? H01T C01I H01V 109.5 . . ? H01U C01I H01V 109.5 . . ? C00S C01J H01W 120.7 . . ? C01F C01J C00S 118.5(12) . . ? C01F C01J H01W 120.7 . . ? C018 C01K H01X 119.4 . . ? C018 C01K C021 121.2(17) . . ? C021 C01K H01X 119.4 . . ? O007 C01L H01Y 109.5 . . ? O007 C01L H 109.5 . . ? O007 C01L HA 109.5 . . ? H01Y C01L H 109.5 . . ? H01Y C01L HA 109.5 . . ? H C01L HA 109.5 . . ? P003 C01M H01Z 109.7 . . ? P003 C01M HB 109.7 . . ? H01Z C01M HB 108.2 . . ? C01V C01M P003 110.0(9) . . ? C01V C01M H01Z 109.7 . . ? C01V C01M HB 109.7 . . ? C01P C01N H01 119.9 . . ? C02A C01N H01 119.9 . . ? C02A C01N C01P 120.1(19) . . ? C00I C01O H0AA 109.5 . . ? C00I C01O HC 109.5 . . ? C00I C01O HD 109.5 . . ? H0AA C01O HC 109.5 . . ? H0AA C01O HD 109.5 . . ? HC C01O HD 109.5 . . ? C00Q C01P C01N 119.8(18) . . ? C00Q C01P H1AA 120.1 . . ? C01N C01P H1AA 120.1 . . ? C00N C01R H2AA 120.1 . . ? C00N C01R C02E 119.9(15) . . ? C02E C01R H2AA 120.1 . . ? C00O C01S H3AA 109.5 . . ? C00O C01S HE 109.5 . . ? C00O C01S HF 109.5 . . ? H3AA C01S HE 109.5 . . ? H3AA C01S HF 109.5 . . ? HE C01S HF 109.5 . . ? C00Q C01T H4AA 119.3 . . ? C00Q C01T C02C 121.4(17) . . ? C02C C01T H4AA 119.3 . . ? C018 C01U H5AA 120.6 . . ? C018 C01U C02D 118.8(18) . . ? C02D C01U H5AA 120.6 . . ? P7 C01V H6AA 110.2 . . ? P7 C01V HG 110.2 . . ? C01M C01V P7 107.5(8) . . ? C01M C01V H6AA 110.2 . . ? C01M C01V HG 110.2 . . ? H6AA C01V HG 108.5 . . ? C01E C01W H7AA 120.3 . . ? C01E C01W C01Z 119.3(15) . . ? C01Z C01W H7AA 120.3 . . ? C01C C01X H8AA 118.6 . . ? C02E C01X C01C 122.8(15) . . ? C02E C01X H8AA 118.6 . . ? C00U C01Y H9AA 109.5 . . ? C00U C01Y HH 109.5 . . ? C00U C01Y HI 109.5 . . ? H9AA C01Y HH 109.5 . . ? H9AA C01Y HI 109.5 . . ? HH C01Y HI 109.5 . . ? C00Y C01Z C01W 119.2(14) . . ? C00Y C01Z H0BA 120.4 . . ? C01W C01Z H0BA 120.4 . . ? C00K C020 C00C 175.0(14) . . ? C01K C021 H021 119.1 . . ? C02B C021 C01K 122(2) . . ? C02B C021 H021 119.1 . . ? C00X C022 H022 119.8 . . ? C00X C022 C023 120.3(14) . . ? C023 C022 H022 119.8 . . ? C017 C023 H023 120.0 . . ? C022 C023 C017 120.1(13) . . ? C022 C023 H023 120.0 . . ? C014 C024 H02A 109.5 . . ? C014 C024 H02B 109.5 . . ? C014 C024 H02C 109.5 . . ? H02A C024 H02B 109.5 . . ? H02A C024 H02C 109.5 . . ? H02B C024 H02C 109.5 . . ? C01D C025 H025 120.3 . . ? C02J C025 C01D 119.4(16) . . ? C02J C025 H025 120.3 . . ? C013 C026 H02D 109.5 . . ? C013 C026 H02E 109.5 . . ? C013 C026 H02G 109.5 . . ? H02D C026 H02E 109.5 . . ? H02D C026 H02G 109.5 . . ? H02E C026 H02G 109.5 . . ? C00Z C028 H02I 109.5 . . ? C00Z C028 H02J 109.5 . . ? C00Z C028 H02K 109.5 . . ? H02I C028 H02J 109.5 . . ? H02I C028 H02K 109.5 . . ? H02J C028 H02K 109.5 . . ? C00W C029 H029 120.5 . . ? C00W C029 C02L 119.0(15) . . ? C02L C029 H029 120.5 . . ? C01N C02A H02L 119.2 . . ? C01N C02A C02C 121.5(18) . . ? C02C C02A H02L 119.2 . . ? C021 C02B H02M 120.0 . . ? C021 C02B C02D 120.1(18) . . ? C02D C02B H02M 120.0 . . ? C01T C02C H02O 120.4 . . ? C02A C02C C01T 119(2) . . ? C02A C02C H02O 120.4 . . ? C01U C02D H02Q 120.1 . . ? C02B C02D C01U 119.9(19) . . ? C02B C02D H02Q 120.1 . . ? C01R C02E H02R 120.8 . . ? C01X C02E C01R 118.5(15) . . ? C01X C02E H02R 120.8 . . ? C025 C02J H02S 120.4 . . ? C025 C02J C02L 119.2(17) . . ? C02L C02J H02S 120.4 . . ? C029 C02L H02T 119.1 . . ? C02J C02L C029 121.9(18) . . ? C02J C02L H02T 119.1 . . ? C02I C00M P7 124.9(15) . . ? C02I C00M C2AA 120.0 . . ? C2AA C00M P7 113.8(15) . . ? C00M C02I H02U 120.0 . . ? C02Q C02I C00M 120.0 . . ? C02Q C02I H02U 120.0 . . ? C02I C02Q H02V 120.0 . . ? C02I C02Q C02O 120.0 . . ? C02O C02Q H02V 120.0 . . ? C02Q C02O H02W 120.0 . . ? C02G C02O C02Q 120.0 . . ? C02G C02O H02W 120.0 . . ? C02O C02G H02X 120.0 . . ? C2AA C02G C02O 120.0 . . ? C2AA C02G H02X 120.0 . . ? C00M C2AA H2AB 120.0 . . ? C02G C2AA C00M 120.0 . . ? C02G C2AA H2AB 120.0 . . ? _smtbx_masks_special_details ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.064 0.024 0.066 13.7 0.0 ? 2 0.000 0.000 0.500 70.0 0.0 ? 3 0.064 -0.024 0.934 13.7 0.0 ? 4 0.000 0.500 1.000 70.0 0.0 ? 5 -0.064 0.476 0.566 13.7 0.0 ? 6 0.064 0.524 0.434 13.7 0.0 ? 7 0.500 0.000 0.500 291.6 81.5 O1C2H6 8 0.500 0.500 0.000 291.6 81.5 O1C2H6 9 0.479 0.090 0.785 18.4 0.1 ? 10 0.479 0.410 0.285 18.4 0.1 ? 11 0.521 0.590 0.715 18.4 0.2 ? 12 0.521 0.910 0.215 18.4 0.1 ? _shelx_res_file ; TITL pph349_a.res in P2(1)/c pph349.res created by SHELXL-2018/3 at 12:18:34 on 09-Aug-2019 REM Old TITL pph349 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.207, Rweak 0.029, Alpha 0.121, Orientation as input REM Formula found by SHELXT: C90 O5 Ru2 CELL 1.54184 18.8881 20.805 19.5529 90 103.523 90 ZERR 4 0.0003 0.0003 0.0003 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H O P Ru UNIT 332 336 4 16 8 RIGU C02P C02H C00L C01Q C02F C02N RIGU C00L C02H C02P C02N C02F C01Q C00M C02I C02Q C02O C02G C2AA RIGU C00W C01D C025 C02J C02L C029 RIGU C00Q C01T C02C C02A C01N C01P RIGU C02D C02B C021 C01K C018 C01U EADP C00L C02H C02P C02N C02F C01Q C00M C02I C02Q C02O C02G C2AA L.S. 4 PLAN 20 BOND $H list 4 fmap 2 53 acta ABIN REM REM REM WGHT 0.158100 89.312706 FVAR 0.13368 0.57807 RU01 5 0.216242 0.714465 0.318158 11.00000 0.03956 0.03530 = 0.06441 0.00246 0.01923 0.00239 RU02 5 0.796601 0.713259 0.426739 11.00000 0.04103 0.04152 = 0.04722 -0.00062 0.00927 -0.00380 P003 4 0.755566 0.796123 0.354180 11.00000 0.05454 0.03706 = 0.06454 -0.00388 0.02214 0.00129 P7 4 0.733494 0.652495 0.336790 11.00000 0.04392 0.03977 = 0.05544 -0.00499 0.00886 -0.00384 P005 4 0.268956 0.647045 0.253860 11.00000 0.04402 0.03851 = 0.08576 -0.00649 0.02911 0.00171 P006 4 0.257324 0.791654 0.255516 11.00000 0.05382 0.03512 = 0.06567 0.00192 0.01997 -0.00330 O007 3 0.505213 0.717096 0.378862 11.00000 0.05534 0.05576 = 0.05259 0.00736 0.01342 -0.00079 C008 1 0.093024 0.721229 0.301919 11.00000 0.03853 0.05052 = 0.06112 -0.00749 0.02401 0.00154 C009 1 0.188673 0.840980 0.196874 11.00000 0.05334 0.03723 = 0.05433 0.00388 0.00192 -0.00849 C00A 1 0.776437 0.619062 0.269117 11.00000 0.05015 0.04129 = 0.05575 -0.00317 0.01101 -0.00205 C00B 1 0.509512 0.708357 0.450033 11.00000 0.04606 0.04491 = 0.05902 0.00479 0.00590 0.00845 C00C 1 0.444050 0.703253 0.471069 11.00000 0.04330 0.03678 = 0.06360 0.00787 0.01949 0.00404 C00D 1 0.170654 0.731849 0.411792 11.00000 0.06378 0.07328 = 0.05087 0.00050 0.02671 -0.00389 C00E 1 0.843574 0.640862 0.264544 11.00000 0.06113 0.05310 = 0.05875 -0.00769 0.01432 -0.01101 AFIX 43 H00E 2 0.867542 0.671906 0.295733 11.00000 -1.20000 AFIX 0 C00F 1 0.577434 0.703771 0.496274 11.00000 0.05767 0.04063 = 0.05699 0.00473 0.02303 0.00320 C00G 1 0.643156 0.709908 0.471512 11.00000 0.03822 0.05309 = 0.09191 -0.00220 0.02089 -0.00034 C00H 1 0.127249 0.766455 0.355016 11.00000 0.05925 0.04832 = 0.06224 -0.00222 0.02036 0.00344 C00I 1 0.115525 0.658815 0.325824 11.00000 0.05269 0.04270 = 0.08740 0.00061 0.03651 -0.00525 C00J 1 0.699219 0.712264 0.452370 11.00000 0.05329 0.03615 = 0.05190 0.00062 0.00133 -0.00559 C00K 1 0.315430 0.712509 0.379144 11.00000 0.05690 0.04512 = 0.05831 0.00303 0.01652 0.00071 PART 1 AFIX 66 C00L 1 0.684981 0.582104 0.356365 21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 C02H 1 0.610027 0.586039 0.348393 21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02H 2 0.585481 0.623700 0.331671 21.00000 -1.20000 AFIX 65 C02P 1 0.571761 0.533685 0.365413 21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02P 2 0.521612 0.536318 0.360079 21.00000 -1.20000 AFIX 65 C02N 1 0.608447 0.477396 0.390406 21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02N 2 0.582843 0.442368 0.401794 21.00000 -1.20000 AFIX 65 C02F 1 0.683400 0.473460 0.398378 21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02F 2 0.707946 0.435798 0.415100 21.00000 -1.20000 AFIX 65 C01Q 1 0.721668 0.525813 0.381358 21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H01Q 2 0.771817 0.523180 0.386692 21.00000 -1.20000 AFIX 0 PART 0 C00N 1 0.173480 0.903879 0.213898 11.00000 0.06512 0.04056 = 0.07404 0.00167 0.00513 0.00417 AFIX 43 H00N 2 0.203381 0.923182 0.253082 11.00000 -1.20000 AFIX 0 C00O 1 0.890583 0.758097 0.506293 11.00000 0.05435 0.05871 = 0.05719 -0.00907 0.00846 -0.01627 C00P 1 0.219686 0.616316 0.168510 11.00000 0.06230 0.03786 = 0.08680 0.00440 0.03142 0.00301 C00Q 1 0.696747 0.857942 0.379317 11.00000 0.06697 0.03593 = 0.09723 -0.00510 0.02537 -0.01306 C00R 1 0.148759 0.635631 0.136089 11.00000 0.06019 0.04809 = 0.09740 0.01463 0.02865 0.00772 AFIX 43 H00R 2 0.125414 0.664127 0.160179 11.00000 -1.20000 AFIX 0 C00S 1 0.741820 0.572508 0.222282 11.00000 0.06847 0.05884 = 0.05649 -0.00934 0.00119 -0.01292 AFIX 43 H00S 2 0.696796 0.556770 0.226029 11.00000 -1.20000 AFIX 0 C00T 1 0.821606 0.849854 0.325576 11.00000 0.05321 0.04289 = 0.07395 0.00977 0.02019 0.01426 C00U 1 0.899691 0.656286 0.465641 11.00000 0.05468 0.07548 = 0.04635 0.00538 0.00219 0.01072 C00V 1 0.857998 0.829655 0.275347 11.00000 0.08198 0.05717 = 0.06922 0.00910 0.03245 0.01961 AFIX 43 H00V 2 0.847745 0.789333 0.254899 11.00000 -1.20000 AFIX 0 C00W 1 0.307191 0.572665 0.297846 11.00000 0.06723 0.04153 = 0.09170 -0.00616 0.01371 0.00978 C00X 1 0.840667 0.908732 0.357364 11.00000 0.07217 0.04385 = 0.08456 -0.00203 0.03789 -0.00676 AFIX 43 H00X 2 0.817826 0.922770 0.391940 11.00000 -1.20000 AFIX 0 C00Y 1 0.251795 0.574965 0.128596 11.00000 0.07223 0.04908 = 0.08705 -0.00371 0.03670 0.00373 AFIX 43 H00Y 2 0.299081 0.560938 0.147470 11.00000 -1.20000 AFIX 0 C00Z 1 0.856880 0.652686 0.517310 11.00000 0.05459 0.06361 = 0.05178 0.01374 0.00224 -0.00101 C010 1 0.447765 0.692304 0.544485 11.00000 0.08166 0.06048 = 0.08059 0.00765 0.04545 -0.01180 AFIX 43 H010 2 0.405379 0.687375 0.560405 11.00000 -1.20000 AFIX 0 C011 1 0.210740 0.759325 0.481669 11.00000 0.06802 0.11054 = 0.07618 -0.01322 0.02709 0.00998 AFIX 137 H01A 2 0.258063 0.739953 0.495546 11.00000 -1.50000 H01B 2 0.183741 0.750530 0.516558 11.00000 -1.50000 H01C 2 0.215883 0.804948 0.477299 11.00000 -1.50000 AFIX 0 C012 1 0.578666 0.693307 0.566662 11.00000 0.05216 0.06408 = 0.06984 0.00203 -0.00732 0.00678 AFIX 43 H012 2 0.623565 0.688891 0.598296 11.00000 -1.20000 AFIX 0 C013 1 0.851030 0.716749 0.541675 11.00000 0.05243 0.08244 = 0.03278 -0.00645 0.00265 -0.01436 C014 1 0.163476 0.664698 0.394366 11.00000 0.05853 0.06277 = 0.07990 0.01899 0.03937 0.00954 C015 1 0.919370 0.721359 0.458200 11.00000 0.04250 0.08519 = 0.03806 0.00948 0.00237 -0.01272 C016 1 0.516427 0.689146 0.591938 11.00000 0.06177 0.09086 = 0.05168 0.01863 0.01992 -0.00341 AFIX 43 H016 2 0.519795 0.684299 0.639876 11.00000 -1.20000 AFIX 0 C017 1 0.909400 0.868393 0.254987 11.00000 0.09329 0.06276 = 0.10226 0.03027 0.04176 0.02048 AFIX 43 H017 2 0.932009 0.854998 0.219991 11.00000 -1.20000 AFIX 0 C018 1 0.317257 0.855248 0.302541 11.00000 0.05326 0.04429 = 0.09725 0.00764 -0.00766 0.00161 C019 1 0.111545 0.837137 0.355868 11.00000 0.05268 0.05501 = 0.08799 -0.01302 0.02645 0.00391 AFIX 137 H01D 2 0.152014 0.858690 0.385986 11.00000 -1.50000 H01E 2 0.068552 0.843911 0.373139 11.00000 -1.50000 H01F 2 0.104026 0.854017 0.309024 11.00000 -1.50000 AFIX 0 C01A 1 0.875636 0.616284 0.212990 11.00000 0.06538 0.07705 = 0.08542 0.00105 0.03469 -0.00477 AFIX 43 H01G 2 0.921061 0.631490 0.209826 11.00000 -1.20000 AFIX 0 C01B 1 0.035080 0.738044 0.238022 11.00000 0.04696 0.07817 = 0.07940 -0.00375 0.01863 0.01049 AFIX 137 H01H 2 0.046439 0.778573 0.219682 11.00000 -1.50000 H01I 2 -0.011056 0.741024 0.250466 11.00000 -1.50000 H01J 2 0.032706 0.705316 0.202947 11.00000 -1.50000 AFIX 0 C01C 1 0.142454 0.814746 0.136197 11.00000 0.07889 0.06652 = 0.05244 -0.00054 0.00269 0.00012 AFIX 43 H01K 2 0.150663 0.773343 0.121866 11.00000 -1.20000 AFIX 0 C01D 1 0.264818 0.517912 0.291002 11.00000 0.07704 0.04958 = 0.08714 0.00161 0.02359 0.00151 AFIX 43 H01L 2 0.220853 0.517579 0.257469 11.00000 -1.20000 AFIX 0 C01E 1 0.112243 0.615330 0.071911 11.00000 0.07354 0.07088 = 0.08392 0.00268 0.01934 0.00004 AFIX 43 H01M 2 0.064867 0.629201 0.053179 11.00000 -1.20000 AFIX 0 C01F 1 0.842279 0.570719 0.167265 11.00000 0.09765 0.06542 = 0.08071 -0.00320 0.04298 0.00363 AFIX 43 H01N 2 0.865496 0.553974 0.134177 11.00000 -1.20000 AFIX 0 C01G 1 0.343725 0.692050 0.229282 11.00000 0.05431 0.05907 = 0.10835 -0.02004 0.04179 -0.00629 AFIX 23 H01O 2 0.382552 0.700300 0.270521 11.00000 -1.20000 H01P 2 0.363467 0.667659 0.195746 11.00000 -1.20000 AFIX 0 C01H 1 0.311198 0.755031 0.196676 11.00000 0.07452 0.05865 = 0.10465 -0.00355 0.05185 -0.01639 AFIX 23 H01R 2 0.279949 0.747120 0.150517 11.00000 -1.20000 H01S 2 0.349722 0.784091 0.191387 11.00000 -1.20000 AFIX 0 C01I 1 0.973592 0.745002 0.418680 11.00000 0.04288 0.13455 = 0.06743 0.00621 0.01477 -0.01270 AFIX 137 H01T 2 0.976433 0.714983 0.382129 11.00000 -1.50000 H01U 2 1.020556 0.748967 0.450434 11.00000 -1.50000 H01V 2 0.958428 0.786159 0.398228 11.00000 -1.50000 AFIX 0 C01J 1 0.773476 0.548965 0.169706 11.00000 0.09395 0.04913 = 0.06513 -0.00978 0.02827 -0.00654 AFIX 43 H01W 2 0.749025 0.519324 0.136976 11.00000 -1.20000 AFIX 0 C01K 1 0.320722 0.866870 0.371057 11.00000 0.07658 0.04909 = 0.09799 0.00140 -0.00757 0.00208 AFIX 43 H01X 2 0.294626 0.840903 0.395130 11.00000 -1.20000 AFIX 0 C01L 1 0.505622 0.782603 0.358226 11.00000 0.06731 0.06720 = 0.09157 0.02390 0.02572 0.00411 AFIX 137 H01Y 2 0.507691 0.784946 0.309697 11.00000 -1.50000 H 2 0.547372 0.803786 0.386759 11.00000 -1.50000 HA 2 0.462078 0.803305 0.364288 11.00000 -1.50000 AFIX 0 C01M 1 0.698819 0.766375 0.270507 11.00000 0.06448 0.05541 = 0.08191 0.01162 -0.00950 0.00975 AFIX 23 H01Z 2 0.661727 0.797923 0.251149 11.00000 -1.20000 HB 2 0.728767 0.759938 0.236985 11.00000 -1.20000 AFIX 0 C01N 1 0.611240 0.946703 0.357140 11.00000 0.06117 0.05112 = 0.20128 -0.00885 0.03933 -0.00301 AFIX 43 H01 2 0.581535 0.974056 0.325194 11.00000 -1.20000 AFIX 0 C01O 1 0.087936 0.596319 0.292683 11.00000 0.07544 0.05717 = 0.13706 -0.01419 0.05545 -0.01792 AFIX 137 H0AA 2 0.081085 0.599500 0.242579 11.00000 -1.50000 HC 2 0.042347 0.586192 0.303857 11.00000 -1.50000 HD 2 0.122619 0.563036 0.310280 11.00000 -1.50000 AFIX 0 C01P 1 0.655503 0.899646 0.332699 11.00000 0.07460 0.04144 = 0.13357 0.01425 0.03310 0.00059 AFIX 43 H1AA 2 0.655959 0.897705 0.285285 11.00000 -1.20000 AFIX 0 C01R 1 0.116455 0.937972 0.175188 11.00000 0.07998 0.05976 = 0.10062 0.01515 0.00532 0.00815 AFIX 43 H2AA 2 0.107420 0.979502 0.188559 11.00000 -1.20000 AFIX 0 C01S 1 0.904800 0.828467 0.521830 11.00000 0.07590 0.07105 = 0.08025 -0.01920 0.01327 -0.02206 AFIX 137 H3AA 2 0.931945 0.845849 0.490298 11.00000 -1.50000 HE 2 0.932234 0.833565 0.569467 11.00000 -1.50000 HF 2 0.859280 0.850829 0.515626 11.00000 -1.50000 AFIX 0 C01T 1 0.697126 0.864826 0.450658 11.00000 0.07972 0.06008 = 0.10560 -0.02212 0.03732 -0.01015 AFIX 43 H4AA 2 0.726473 0.837985 0.483496 11.00000 -1.20000 AFIX 0 C01U 1 0.357188 0.894265 0.268214 11.00000 0.05737 0.04891 = 0.13499 0.02308 0.00414 -0.00530 AFIX 43 H5AA 2 0.356189 0.887673 0.220954 11.00000 -1.20000 AFIX 0 C01V 1 0.663114 0.703664 0.282418 11.00000 0.04940 0.05537 = 0.07919 -0.02076 -0.01018 0.00994 AFIX 23 H6AA 2 0.642577 0.682866 0.237788 11.00000 -1.20000 HG 2 0.624248 0.711411 0.306205 11.00000 -1.20000 AFIX 0 C01W 1 0.145911 0.573719 0.034261 11.00000 0.10938 0.06303 = 0.07817 -0.00083 0.02254 -0.01081 AFIX 43 H7AA 2 0.121229 0.559057 -0.009804 11.00000 -1.20000 AFIX 0 C01X 1 0.085676 0.849899 0.098386 11.00000 0.10662 0.08975 = 0.06576 0.01702 -0.01917 -0.00987 AFIX 43 H8AA 2 0.055304 0.831216 0.059071 11.00000 -1.20000 AFIX 0 C01Y 1 0.928098 0.597668 0.434107 11.00000 0.08380 0.09062 = 0.08780 -0.00025 -0.00155 0.04083 AFIX 137 H9AA 2 0.912110 0.559369 0.453395 11.00000 -1.50000 HH 2 0.980350 0.598736 0.445023 11.00000 -1.50000 HI 2 0.909775 0.597875 0.383986 11.00000 -1.50000 AFIX 0 C01Z 1 0.217274 0.553971 0.063069 11.00000 0.09214 0.05117 = 0.10103 -0.00487 0.04368 0.00256 AFIX 43 H0BA 2 0.241057 0.526835 0.037951 11.00000 -1.20000 AFIX 0 C020 1 0.375470 0.710396 0.419946 11.00000 0.04835 0.06343 = 0.09319 0.00512 0.01261 -0.00242 C021 1 0.362277 0.916591 0.406173 11.00000 0.08068 0.06187 = 0.14152 -0.02902 -0.02312 0.01573 AFIX 43 H021 2 0.362485 0.924045 0.453117 11.00000 -1.20000 AFIX 0 C022 1 0.892287 0.946742 0.339131 11.00000 0.07193 0.04633 = 0.13424 0.00808 0.03745 -0.00338 AFIX 43 H022 2 0.904451 0.985977 0.361598 11.00000 -1.20000 AFIX 0 C023 1 0.926367 0.927288 0.287718 11.00000 0.07498 0.06637 = 0.12768 0.02943 0.04345 0.00016 AFIX 43 H023 2 0.960838 0.953709 0.274920 11.00000 -1.20000 AFIX 0 C024 1 0.199095 0.611167 0.443460 11.00000 0.08400 0.07587 = 0.12182 0.03712 0.03737 0.01125 AFIX 137 H02A 2 0.191143 0.570779 0.419125 11.00000 -1.50000 H02B 2 0.178179 0.609782 0.483707 11.00000 -1.50000 H02C 2 0.250449 0.619147 0.458540 11.00000 -1.50000 AFIX 0 C025 1 0.284567 0.463775 0.331469 11.00000 0.11329 0.04918 = 0.12185 0.01184 0.02835 0.01042 AFIX 43 H025 2 0.255880 0.426978 0.323150 11.00000 -1.20000 AFIX 0 C026 1 0.815307 0.736924 0.598764 11.00000 0.08271 0.13735 = 0.06571 -0.01503 0.03325 -0.01225 AFIX 137 H02D 2 0.793427 0.778454 0.587862 11.00000 -1.50000 H02E 2 0.851073 0.739046 0.642578 11.00000 -1.50000 H02G 2 0.778454 0.706243 0.602553 11.00000 -1.50000 AFIX 0 C028 1 0.827987 0.593215 0.544128 11.00000 0.11783 0.09467 = 0.07891 0.03221 0.00227 -0.03066 AFIX 137 H02I 2 0.797737 0.604918 0.575351 11.00000 -1.50000 H02J 2 0.867871 0.567372 0.568987 11.00000 -1.50000 H02K 2 0.799811 0.569188 0.505257 11.00000 -1.50000 AFIX 0 C029 1 0.372132 0.572034 0.348612 11.00000 0.07028 0.05797 = 0.14218 0.01825 -0.00196 0.00037 AFIX 43 H029 2 0.403260 0.607270 0.354312 11.00000 -1.20000 AFIX 0 C02A 1 0.612774 0.951178 0.426104 11.00000 0.07586 0.06790 = 0.20705 -0.04684 0.04646 -0.00609 AFIX 43 H02L 2 0.584695 0.982389 0.441300 11.00000 -1.20000 AFIX 0 C02B 1 0.400788 0.952954 0.375657 11.00000 0.08352 0.05908 = 0.20302 -0.02729 -0.01921 -0.00948 AFIX 43 H02M 2 0.429546 0.985200 0.401007 11.00000 -1.20000 AFIX 0 C02C 1 0.654041 0.911495 0.473674 11.00000 0.07936 0.07827 = 0.17349 -0.04556 0.05849 -0.01054 AFIX 43 H02O 2 0.654042 0.914911 0.521098 11.00000 -1.20000 AFIX 0 C02D 1 0.399429 0.944204 0.306151 11.00000 0.05956 0.04286 = 0.20733 0.01253 0.00906 -0.00539 AFIX 43 H02Q 2 0.426309 0.971126 0.283863 11.00000 -1.20000 AFIX 0 C02E 1 0.071722 0.910546 0.115577 11.00000 0.09353 0.08143 = 0.08252 0.01873 -0.00367 0.00941 AFIX 43 H02R 2 0.033088 0.933550 0.088237 11.00000 -1.20000 AFIX 0 C02J 1 0.345765 0.464576 0.383181 11.00000 0.11096 0.07160 = 0.16753 0.04891 0.01286 0.01904 AFIX 43 H02S 2 0.357902 0.429582 0.413233 11.00000 -1.20000 AFIX 0 C02L 1 0.390119 0.517821 0.391004 11.00000 0.08107 0.08465 = 0.19013 0.05074 0.00283 0.02113 AFIX 43 H02T 2 0.433335 0.517640 0.425560 11.00000 -1.20000 AFIX 66 PART 2 C00M 1 0.689516 0.579910 0.362472 -21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 C02I 1 0.624676 0.579586 0.384496 -21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02U 2 0.594900 0.615743 0.377791 -21.00000 -1.20000 AFIX 65 C02Q 1 0.604338 0.525220 0.416542 -21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02V 2 0.560955 0.525003 0.431277 -21.00000 -1.20000 AFIX 65 C02O 1 0.648841 0.471178 0.426563 -21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02W 2 0.635233 0.434803 0.448004 -21.00000 -1.20000 AFIX 65 C02G 1 0.713682 0.471501 0.404539 -21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H02X 2 0.743457 0.435343 0.411244 -21.00000 -1.20000 AFIX 65 C2AA 1 0.734020 0.525866 0.372493 -21.00000 0.07623 0.06431 = 0.08697 -0.00103 0.03156 -0.02067 AFIX 43 H2AB 2 0.777403 0.526082 0.357758 -21.00000 -1.20000 AFIX 0 HKLF 4 REM pph349_a.res in P2(1)/c REM wR2 = 0.3651, GooF = S = 1.110, Restrained GooF = 1.104 for all data REM R1 = 0.1129 for 11358 Fo > 4sig(Fo) and 0.1291 for all 15199 data REM 787 parameters refined using 180 restraints END WGHT 0.1581 89.1475 REM Highest difference peak 2.868, deepest hole -1.535, 1-sigma level 0.174 Q1 1 0.7967 0.7836 0.3799 11.00000 0.05 2.87 Q2 1 0.7925 0.7842 0.4748 11.00000 0.05 2.77 Q3 1 0.2101 0.7834 0.3609 11.00000 0.05 2.68 Q4 1 0.2175 0.7827 0.2723 11.00000 0.05 2.58 Q5 1 0.2169 0.7159 0.2204 11.00000 0.05 2.25 Q6 1 0.7912 0.7163 0.5228 11.00000 0.05 2.16 Q7 1 0.7955 0.7147 0.3274 11.00000 0.05 2.03 Q8 1 0.2147 0.7168 0.4132 11.00000 0.05 1.73 Q9 1 0.7932 0.7814 0.5184 11.00000 0.05 1.30 Q10 1 0.6341 0.7147 0.6103 11.00000 0.05 1.29 Q11 1 0.3705 0.7153 0.5767 11.00000 0.05 1.28 Q12 1 0.2125 0.7835 0.2213 11.00000 0.05 1.26 Q13 1 0.2192 0.7139 0.2773 11.00000 0.05 1.25 Q14 1 0.2201 0.7844 0.1812 11.00000 0.05 1.10 Q15 1 0.2565 0.7058 0.3918 11.00000 0.05 1.01 Q16 1 0.7332 0.8461 0.2886 11.00000 0.05 0.98 Q17 1 0.7586 0.7124 0.4189 11.00000 0.05 0.96 Q18 1 0.2102 0.7820 0.1257 11.00000 0.05 0.95 Q19 1 0.6349 0.7828 0.2009 11.00000 0.05 0.94 Q20 1 0.7975 0.7831 0.2785 11.00000 0.05 0.93 ; _shelx_res_checksum 26339 _shelx_hkl_file ; 0 0 -1 -0.02 0.17 0 0 -2 423.25 43.23 0 0 -2 574.56 43.41 0 0 -3 0.59 0.70 0 0 -3 0.52 1.55 0 0 4 651.36 48.31 0 0 -4 616.55 48.40 0 0 5 0.76 0.58 0 0 6 97.74 9.31 0 0 7 -0.41 0.56 0 0 7 -1.59 1.25 0 0 8 242.98 23.23 0 0 8 259.18 23.67 0 0 9 0.41 1.30 0 0 10 122.31 12.29 0 0 11 0.36 1.52 0 0 -12 83.42 9.62 0 0 -12 83.05 9.47 0 0 -12 85.84 9.57 0 0 -12 102.01 9.37 0 0 -12 104.26 10.00 0 0 12 111.47 9.98 0 0 -13 -0.20 1.74 0 0 -13 -1.03 1.62 0 0 -13 -0.35 1.71 0 0 -13 -0.14 1.22 0 0 -13 0.12 1.22 0 0 -13 -1.21 2.05 0 0 13 2.74 1.69 0 0 13 -1.54 2.09 0 0 -14 0.22 1.73 0 0 14 1.00 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109.98 11.22 0 11 -6 122.04 11.28 0 11 -6 127.17 11.62 0 -11 -6 117.06 10.83 0 -11 6 116.27 10.93 0 -11 -6 110.30 10.84 0 -11 7 37.16 5.62 0 11 7 54.92 7.56 0 11 7 42.10 6.65 0 11 7 56.46 6.32 0 -11 -7 59.03 5.58 0 -11 7 53.50 5.59 0 -11 -7 69.13 5.65 0 -11 -7 52.45 6.40 0 -11 -7 48.07 5.60 0 11 7 49.01 6.00 0 11 -7 56.93 6.11 0 11 -7 48.10 6.32 0 -11 -8 7.08 2.68 0 -11 -8 6.13 1.45 0 -11 8 2.34 1.68 0 11 8 4.26 2.84 0 11 8 7.62 3.76 0 11 8 7.27 2.63 0 -11 8 2.76 1.33 0 -11 -8 5.94 1.30 0 -11 -8 3.03 1.06 0 11 -8 7.34 2.91 0 11 -8 5.18 1.45 0 11 -8 7.36 2.20 0 11 -8 1.40 1.86 0 11 -8 4.65 2.26 0 11 8 5.71 2.11 0 -11 -9 27.54 5.04 0 -11 -9 40.54 4.12 0 11 9 41.93 6.64 0 11 9 20.96 5.06 0 -11 9 23.41 4.15 0 11 9 34.92 5.06 0 -11 9 37.20 3.95 0 -11 -9 38.98 3.71 0 -11 -9 33.17 3.83 0 11 -9 44.91 4.29 0 11 -9 39.59 5.50 0 11 -9 33.80 4.06 0 -11 -9 29.78 3.68 0 11 -9 23.99 4.41 0 11 9 38.72 4.71 0 11 -9 32.82 4.42 0 11 -9 38.14 4.68 0 -11 -10 39.47 4.25 0 11 10 35.42 6.42 0 -11 10 20.17 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144.57 13.66 0 12 9 2.61 2.55 0 -12 9 2.59 1.76 0 12 9 -1.76 3.87 0 -12 -9 6.48 1.22 0 -12 -9 5.88 1.48 0 -12 9 5.81 1.45 0 12 -9 6.73 3.18 0 12 -9 4.51 1.64 0 -12 -9 4.53 1.64 0 -12 -9 0.96 2.56 0 12 -9 2.19 2.31 0 12 -9 5.44 2.25 0 12 9 4.78 2.43 0 -12 -10 30.60 4.46 0 -12 -10 21.89 2.95 0 -12 10 12.28 2.87 0 12 10 22.73 5.77 0 12 10 21.87 4.19 0 -12 -10 21.88 2.66 0 -12 10 20.06 2.75 0 12 -10 23.35 4.43 0 12 -10 21.24 3.04 0 -12 -10 16.64 2.45 0 12 10 25.01 3.87 0 12 -10 24.73 3.56 0 -12 -11 73.75 7.85 0 12 11 93.46 11.17 0 12 11 85.61 9.51 0 -12 11 74.44 7.68 0 -12 -11 72.79 7.63 0 12 -11 86.01 9.46 0 12 -11 75.80 8.06 0 -12 -11 64.03 7.48 0 12 -11 75.41 7.91 0 12 11 91.42 8.90 0 12 -11 85.14 8.63 0 12 12 41.64 7.75 0 12 12 33.34 5.97 0 -12 -12 40.51 4.46 0 12 -12 43.32 4.81 0 12 -12 42.53 6.26 0 12 -12 33.94 4.47 0 -12 -12 29.44 3.99 0 12 -12 38.16 5.16 0 12 12 50.21 5.73 0 12 13 17.12 4.80 0 -12 -13 20.37 4.43 0 -12 -13 17.39 2.75 0 12 -13 14.01 4.27 0 12 -13 21.10 3.11 0 12 -13 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4.81 0 -15 3 23.03 3.56 0 -15 -3 28.54 3.74 0 -15 -3 29.43 4.25 0 -15 3 28.27 3.70 0 -15 3 33.15 3.75 0 15 -3 37.70 4.83 0 -15 -3 31.41 3.65 0 15 3 35.59 4.66 0 15 3 33.02 4.05 0 -15 -3 27.64 3.64 0 15 3 25.93 6.24 0 15 3 23.77 4.87 0 15 -3 36.97 4.08 0 15 -3 36.76 4.76 0 15 3 31.85 4.51 0 15 -3 28.15 4.85 0 -15 -4 41.02 4.27 0 -15 -4 30.23 4.67 0 15 4 36.14 5.45 0 15 -4 27.90 5.28 0 -15 4 35.71 4.04 0 -15 4 34.51 4.10 0 15 -4 33.83 4.93 0 15 4 30.38 4.19 0 15 4 41.44 4.96 0 -15 -4 38.89 4.17 0 -15 -4 34.28 4.00 0 -15 4 29.49 4.13 0 15 4 30.72 6.87 0 15 4 30.71 5.33 0 15 4 37.04 5.07 0 15 -4 28.24 4.88 0 15 -4 36.47 4.41 0 15 -4 35.26 5.02 0 -15 -5 19.51 2.65 0 -15 5 13.34 2.30 0 15 5 14.38 3.67 0 15 -5 12.10 3.95 0 -15 -5 16.13 3.33 0 15 5 18.04 2.79 0 -15 5 18.81 2.58 0 -15 -5 14.20 2.32 0 -15 5 15.46 2.43 0 15 5 13.03 3.29 0 -15 -5 14.95 2.41 0 15 -5 12.93 3.31 0 15 5 16.93 5.51 0 15 5 15.48 3.99 0 15 -5 16.05 3.54 0 15 -5 17.47 3.52 0 15 5 16.32 3.52 0 15 -5 16.47 2.80 0 15 6 75.44 10.39 0 15 6 80.10 7.87 0 -15 -6 62.31 6.84 0 -15 -6 76.24 6.96 0 -15 6 58.93 6.82 0 -15 6 57.81 6.84 0 15 6 71.89 7.21 0 -15 6 56.86 6.70 0 -15 -6 59.80 7.63 0 15 6 58.38 7.86 0 15 -6 74.96 7.40 0 15 6 71.06 7.91 0 15 -6 66.06 7.81 0 15 7 6.71 5.29 0 15 7 4.78 2.66 0 15 7 6.43 2.32 0 -15 -7 11.71 2.09 0 -15 -7 6.24 1.84 0 -15 7 6.51 1.84 0 -15 7 7.13 1.98 0 15 -7 9.40 3.89 0 -15 -7 9.42 3.13 0 15 7 11.84 3.65 0 15 -7 8.02 3.16 0 15 -7 9.50 2.61 0 15 7 12.51 3.39 0 15 8 9.47 5.24 0 15 8 4.83 2.16 0 -15 8 2.78 1.53 0 -15 -8 4.76 1.35 0 -15 8 4.85 1.52 0 15 8 2.29 2.41 0 -15 -8 3.62 1.45 0 15 8 6.62 3.43 0 -15 -8 3.95 2.73 0 -15 -8 3.86 1.80 0 15 -8 4.27 2.95 0 15 -8 3.77 2.08 0 15 8 4.27 2.86 0 15 -8 2.74 3.50 0 -15 -9 0.87 1.25 0 -15 9 -0.49 1.37 0 -15 9 -0.75 1.27 0 15 9 -0.23 1.98 0 -15 -9 1.71 2.62 0 15 9 4.28 3.23 0 -15 -9 2.49 1.72 0 15 -9 1.48 2.27 0 15 -9 1.11 2.51 0 15 9 1.92 3.06 0 15 10 157.46 16.74 0 -15 10 108.71 12.31 0 -15 -10 109.05 12.30 0 -15 10 126.51 12.49 0 -15 -10 121.92 12.60 0 15 10 160.63 14.04 0 -15 -10 142.28 13.75 0 15 -10 143.15 13.13 0 15 10 154.71 13.84 0 15 -10 123.92 12.58 0 15 11 8.16 5.54 0 -15 -11 7.09 3.34 0 -15 -11 5.66 1.96 0 15 -11 5.89 2.65 0 15 11 10.04 3.63 0 15 -11 5.33 1.94 0 15 -11 7.89 4.15 0 15 -12 -3.20 3.68 0 15 -12 0.93 1.73 0 15 12 -3.19 3.47 0 15 -12 1.80 2.36 0 -15 -12 1.72 1.63 0 -15 -12 4.93 2.97 0 15 -13 4.42 1.92 0 15 -13 8.23 3.78 0 15 -13 6.54 2.55 0 15 13 4.99 3.90 0 -15 -13 5.06 1.87 0 -15 -13 8.49 3.41 0 15 -14 0.35 1.71 0 15 -14 0.81 3.10 0 15 14 2.45 3.40 0 15 -14 0.24 2.29 0 -15 -14 -1.65 1.38 0 15 -15 2.13 1.65 0 15 -15 1.09 2.69 0 15 -15 5.15 2.44 0 -15 -15 1.31 1.29 0 15 -16 5.27 1.84 0 15 -16 0.61 2.58 0 15 -16 -1.01 2.13 0 15 16 -3.29 3.22 0 -15 -16 0.74 1.06 0 -15 -16 1.03 2.34 0 15 -17 -1.45 2.02 0 15 -17 1.12 1.30 0 15 -17 -0.35 1.60 0 -15 -17 2.78 2.09 0 15 -18 16.26 3.02 0 15 -18 25.41 2.91 0 -15 -18 28.36 3.45 0 15 -18 26.89 3.19 0 15 -19 1.96 1.11 0 -16 0 1217.67 109.82 0 16 0 1066.24 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5.06 0 16 -13 7.40 2.09 0 16 -13 2.09 3.19 0 16 13 8.63 4.33 0 16 -13 7.00 2.50 0 -16 -13 5.73 3.23 0 -16 -13 6.23 1.96 0 16 -14 2.26 2.88 0 16 -14 4.60 1.78 0 16 -14 5.73 2.31 0 16 14 9.71 3.86 0 -16 -14 6.98 1.66 0 -16 -14 7.64 3.03 0 16 -15 0.28 1.35 0 16 -15 1.65 2.49 0 16 -15 0.20 1.86 0 16 15 -1.29 3.30 0 -16 -15 0.59 1.23 0 16 -16 12.21 2.04 0 16 -16 10.74 2.92 0 16 -16 20.06 2.70 0 16 16 15.31 3.80 0 -16 -16 9.13 1.67 0 16 -17 4.24 1.99 0 16 -17 3.12 1.27 0 -16 -17 4.94 1.95 0 16 -17 1.74 1.53 0 16 -18 0.66 1.16 0 -17 0 -0.33 1.46 0 17 0 1.13 3.25 0 -17 0 0.16 1.48 0 17 0 4.88 2.12 0 17 0 4.77 2.49 0 -17 0 0.97 1.43 0 17 0 2.08 4.27 0 17 0 0.76 3.01 0 17 0 0.60 2.77 0 -17 -1 167.36 16.09 0 -17 1 160.64 16.04 0 17 1 153.81 17.05 0 17 -1 150.02 17.16 0 17 1 190.60 16.92 0 17 -1 183.38 16.91 0 -17 -1 154.62 16.01 0 17 -1 153.33 16.26 0 17 1 169.84 16.34 0 -17 1 161.15 16.03 0 17 1 143.62 18.50 0 17 1 160.56 17.25 0 17 -1 154.32 17.08 0 17 1 169.05 16.92 0 17 -1 163.72 16.88 0 -17 2 172.83 18.44 0 -17 -2 171.23 18.69 0 -17 -2 191.78 18.57 0 17 -2 154.87 19.40 0 17 2 193.92 19.75 0 -17 -2 196.01 18.49 0 17 2 216.59 19.36 0 17 -2 214.69 19.38 0 17 2 187.11 18.72 0 -17 2 206.70 18.55 0 17 2 170.23 21.03 0 17 2 194.19 19.79 0 17 -2 177.31 19.37 0 17 -2 193.48 19.33 0 -17 -3 12.76 2.41 0 17 3 12.41 3.85 0 -17 -3 12.75 2.83 0 -17 3 13.96 2.22 0 -17 3 12.86 2.25 0 17 3 10.20 2.55 0 -17 3 12.82 2.25 0 -17 -3 10.11 2.08 0 17 3 18.13 3.42 0 -17 -3 10.66 2.18 0 17 -3 12.00 3.22 0 17 3 14.63 5.61 0 17 3 12.43 4.29 0 17 -3 8.37 3.28 0 17 -3 12.56 3.59 0 -17 -4 0.89 1.53 0 17 4 2.67 3.65 0 -17 -4 0.26 2.13 0 -17 4 1.21 1.36 0 17 4 0.79 4.77 0 -17 4 -0.16 1.38 0 17 4 -1.10 1.99 0 17 -4 0.30 2.44 0 -17 -4 0.96 1.43 0 -17 4 1.37 1.55 0 -17 -4 0.32 1.35 0 17 4 2.99 2.52 0 17 4 4.09 3.78 0 17 -4 1.58 1.71 0 17 4 -0.31 2.88 0 17 -4 2.78 3.04 0 -17 -5 14.64 2.50 0 -17 5 11.11 2.15 0 -17 -5 14.55 3.14 0 17 5 10.03 4.16 0 17 5 9.84 5.83 0 17 5 16.47 3.36 0 -17 5 12.24 2.38 0 17 5 14.28 2.83 0 -17 -5 12.69 2.21 0 -17 -5 13.30 2.28 0 -17 5 10.06 2.15 0 17 -5 22.72 4.68 0 17 5 11.72 4.15 0 17 5 12.25 3.69 0 17 -5 14.60 3.72 0 17 -5 14.72 2.68 0 -17 6 13.97 2.33 0 -17 -6 16.41 2.73 0 17 6 21.98 4.67 0 -17 -6 16.00 3.42 0 17 6 11.84 5.80 0 -17 6 14.66 2.50 0 -17 -6 13.09 2.43 0 -17 -6 21.51 2.69 0 -17 6 16.41 2.62 0 17 -6 20.21 4.66 0 17 6 13.35 4.64 0 17 -6 20.50 3.18 0 17 -6 15.74 3.92 0 17 6 14.91 4.05 0 -17 -7 32.69 5.39 0 17 7 38.62 6.13 0 17 7 30.95 7.68 0 -17 7 36.61 4.57 0 -17 7 34.63 4.49 0 -17 -7 42.84 4.58 0 -17 -7 44.64 4.62 0 17 -7 30.31 6.06 0 17 7 35.97 6.48 0 17 -7 40.38 5.00 0 17 7 36.85 5.95 0 17 -7 43.25 5.89 0 17 8 -0.40 3.43 0 -17 -8 0.95 2.60 0 17 8 5.53 5.46 0 -17 8 0.17 1.33 0 -17 -8 1.39 1.30 0 -17 8 0.46 1.18 0 17 -8 1.90 3.24 0 17 8 0.92 3.91 0 17 -8 1.37 2.09 0 17 8 3.16 3.36 0 17 -8 0.29 2.72 0 -17 -9 19.71 4.11 0 17 9 24.82 4.91 0 -17 -9 22.82 3.16 0 17 9 12.18 6.31 0 17 -9 31.43 5.37 0 17 9 25.97 5.72 0 17 9 24.41 4.62 0 17 -9 22.68 3.61 0 -17 9 17.39 2.72 0 -17 -9 17.51 2.72 0 -17 9 19.37 2.87 0 -17 -10 53.76 8.31 0 17 10 71.33 9.14 0 -17 -10 68.65 7.67 0 17 -10 82.11 8.10 0 17 10 84.88 9.26 0 17 10 78.93 9.80 0 -17 -11 28.38 4.56 0 -17 -11 27.98 3.61 0 17 11 35.34 5.48 0 17 -11 23.11 3.95 0 -17 -12 -0.32 1.38 0 -17 -12 0.31 2.44 0 17 12 -0.36 3.55 0 17 -12 0.89 2.06 0 17 -12 1.69 3.09 0 -17 -13 1.59 1.35 0 -17 -13 4.03 2.71 0 17 13 3.94 4.31 0 17 13 0.35 3.59 0 17 -13 3.55 2.12 0 17 -13 2.31 2.99 0 -17 -14 1.77 1.32 0 -17 -14 0.52 2.34 0 17 14 0.48 4.43 0 17 -14 0.77 1.87 0 17 14 1.67 3.52 0 17 -14 2.07 2.99 0 -17 -15 2.76 2.31 0 -17 -15 1.24 1.04 0 17 15 -4.12 4.60 0 17 -15 0.34 1.64 0 17 15 -0.30 3.25 0 17 -15 2.65 2.34 0 -17 -16 -0.22 0.79 0 17 16 3.38 4.40 0 17 16 -3.42 2.94 0 17 -16 -0.57 1.42 0 17 -16 0.93 1.95 0 -17 -17 3.58 1.70 0 17 -17 3.99 1.55 0 17 17 4.10 3.71 0 17 -17 3.98 1.30 0 18 0 27.03 5.89 0 -18 0 39.54 4.60 0 18 0 48.32 5.64 0 -18 0 44.41 4.62 0 -18 0 40.72 4.59 0 18 0 27.04 6.61 0 18 0 29.38 5.88 0 18 0 33.48 5.69 0 18 -1 28.31 5.43 0 -18 -1 33.29 3.91 0 -18 1 29.23 3.76 0 18 1 27.00 5.33 0 18 -1 32.82 4.83 0 -18 -1 28.55 3.71 0 18 1 36.16 4.86 0 -18 1 29.23 3.76 0 18 1 23.48 6.47 0 18 1 17.20 4.94 0 18 -1 26.01 4.93 0 18 1 35.94 5.47 0 18 -1 30.30 5.26 0 -18 2 4.86 1.69 0 18 -2 -0.81 3.68 0 18 2 3.63 3.66 0 -18 -2 5.12 1.78 0 -18 2 5.70 1.77 0 18 2 -0.30 2.43 0 -18 -2 4.50 1.73 0 18 -2 1.22 2.46 0 18 2 -0.79 4.78 0 18 2 0.41 3.40 0 18 -2 2.09 2.98 0 18 -2 5.79 3.26 0 -18 -3 33.53 4.08 0 18 3 31.38 5.73 0 -18 -3 26.59 4.15 0 -18 3 33.50 3.84 0 18 3 21.85 7.02 0 -18 -3 32.59 3.92 0 -18 -3 31.61 3.88 0 -18 3 30.39 3.85 0 18 -3 32.78 4.96 0 -18 3 32.59 3.92 0 18 3 29.36 4.70 0 18 3 31.08 5.67 0 18 -3 34.67 5.19 0 18 -3 23.71 4.72 0 -18 -4 4.31 2.23 0 -18 4 0.91 1.36 0 -18 -4 3.27 1.76 0 18 4 4.09 3.88 0 18 4 5.02 5.27 0 -18 -4 3.38 1.62 0 18 4 3.62 2.47 0 -18 -4 3.33 1.68 0 -18 4 2.10 1.53 0 -18 4 0.50 1.35 0 18 -4 1.85 3.43 0 18 4 0.43 3.45 0 18 4 3.37 3.39 0 18 -4 1.28 3.01 0 -18 -5 9.45 2.75 0 -18 -5 11.36 2.38 0 18 5 7.44 4.05 0 -18 5 9.41 1.97 0 18 5 12.30 5.96 0 -18 5 8.56 2.12 0 -18 -5 10.84 2.08 0 -18 5 9.35 2.04 0 -18 -5 9.16 2.23 0 18 -5 14.53 4.16 0 18 5 7.91 4.19 0 18 5 9.26 3.65 0 18 -5 13.35 2.48 0 18 -5 13.33 3.53 0 -18 6 5.85 1.51 0 -18 -6 6.77 2.57 0 18 6 2.09 3.67 0 -18 -6 7.15 2.07 0 18 6 8.10 5.75 0 -18 6 5.03 1.74 0 -18 -6 4.52 1.56 0 -18 6 5.00 1.65 0 -18 -6 4.47 1.73 0 18 -6 7.07 3.79 0 18 6 8.54 4.37 0 18 -6 8.80 2.21 0 18 6 6.66 3.45 0 18 -6 7.76 3.31 0 -18 -7 49.05 6.35 0 18 7 49.87 7.55 0 18 7 43.15 9.24 0 18 -7 53.23 7.55 0 -18 7 42.69 5.55 0 -18 7 54.21 5.74 0 -18 -7 61.13 5.75 0 18 7 35.85 7.42 0 18 -7 50.14 6.73 0 18 -7 50.33 5.95 0 18 7 59.62 7.53 0 -18 -8 106.94 12.62 0 18 8 121.37 13.53 0 18 8 117.37 13.89 0 18 -8 127.28 12.35 0 18 8 141.70 13.64 0 18 -8 104.59 12.52 0 18 -8 131.91 13.85 0 18 9 80.16 9.70 0 -18 -9 66.41 7.99 0 -18 -9 73.82 8.77 0 18 9 80.24 10.04 0 18 -9 79.86 8.37 0 18 9 97.44 9.74 0 18 -9 75.62 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9.85 4 12 -6 106.58 10.97 4 12 -6 78.75 10.41 4 -12 -6 100.70 10.41 4 -12 -6 98.61 10.01 -4 12 6 94.16 10.39 -4 12 5 40.05 5.51 -4 -12 5 36.82 3.96 4 -12 -5 36.33 3.80 4 -12 -5 35.61 3.86 -4 -12 5 35.89 3.83 4 12 -5 35.95 4.70 4 12 -5 35.57 4.93 -4 12 5 29.73 5.33 4 -12 -5 37.91 4.47 4 12 -5 27.58 4.50 -4 12 5 26.66 4.50 4 -12 -5 34.33 4.02 4 -12 -5 30.78 3.94 -4 12 5 33.80 4.47 -4 12 4 366.00 34.55 4 -12 -4 365.63 33.29 -4 12 4 344.75 34.29 -4 -12 4 364.73 33.19 -4 -12 4 342.74 33.10 4 -12 -4 340.20 33.14 4 12 -4 367.49 33.67 4 12 -4 388.82 34.05 4 12 -4 320.97 33.64 -4 12 4 295.33 33.55 4 -12 -4 348.25 33.26 -4 12 4 352.78 33.58 4 12 -3 18.31 3.08 -4 12 3 12.01 3.00 -4 12 3 10.21 3.16 4 -12 -3 16.61 2.42 4 12 -3 18.20 3.12 -4 -12 3 18.07 2.35 4 -12 -3 18.67 2.31 -4 -12 3 15.98 2.26 -4 12 3 11.09 3.75 -4 12 3 11.34 3.38 -4 12 3 17.89 2.99 4 12 -2 58.36 6.49 -4 12 2 48.57 6.53 4 12 -2 65.42 6.45 4 12 -2 59.60 6.10 -4 -12 2 53.18 5.86 -4 -12 2 54.59 5.83 4 -12 -2 55.35 5.89 4 -12 -2 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1.36 1.04 4 -13 -20 13.51 1.59 -4 13 20 13.94 4.83 4 13 -20 12.31 2.14 4 13 -20 7.66 2.13 -4 13 19 0.92 4.59 4 -13 -19 -0.39 0.95 4 13 -19 3.92 1.87 4 13 -19 1.06 2.17 4 13 -19 -0.14 1.47 4 -13 -18 3.65 1.31 4 13 -18 4.21 2.20 4 13 -18 4.41 2.77 4 13 -18 6.31 2.04 4 13 -17 0.81 1.69 4 -13 -17 0.33 1.23 4 13 -17 0.23 1.99 4 13 -17 1.87 2.05 4 13 -17 1.19 2.93 4 -13 -16 0.37 1.38 4 13 -16 1.98 2.05 4 13 -16 0.96 2.14 4 13 -16 5.85 2.43 4 13 -16 1.75 3.38 4 -13 -15 1.23 1.29 4 -13 -15 2.04 3.07 4 13 -15 -1.40 3.34 4 13 -15 3.79 2.25 4 13 -15 -0.19 1.85 4 -13 -15 0.65 1.34 4 13 -15 2.24 2.24 4 -13 -14 69.62 7.77 4 -13 -14 89.71 9.31 4 13 -14 75.43 8.34 4 13 -14 88.70 10.05 -4 13 14 100.82 12.34 4 -13 -14 69.30 7.80 4 13 -14 77.23 8.18 4 13 -14 82.87 8.62 4 -13 -13 21.18 4.41 4 -13 -13 21.80 2.96 4 13 -13 22.46 3.31 4 -13 -13 16.66 2.66 4 13 -13 15.75 3.17 -4 13 13 16.13 3.92 4 13 -13 23.17 3.71 4 -13 -12 18.33 3.99 4 -13 -12 13.96 2.46 4 13 -12 15.88 2.97 -4 13 12 13.76 4.91 -4 13 12 18.61 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7.84 -4 13 7 68.26 9.53 -4 13 7 55.61 9.04 -4 -13 7 75.86 7.78 4 -13 -7 87.26 7.70 -4 -13 7 69.66 7.52 4 -13 -7 93.11 7.59 4 13 -7 83.91 9.17 4 13 -7 63.21 7.66 -4 13 7 75.41 8.29 4 13 -7 66.32 7.71 -4 13 6 116.84 11.88 4 13 -6 100.98 11.77 4 -13 -6 122.64 11.68 4 -13 -6 119.50 11.23 -4 13 6 131.05 13.19 -4 13 6 106.07 12.70 4 -13 -6 114.48 10.95 -4 -13 6 117.80 11.14 4 -13 -6 110.84 11.02 -4 -13 6 110.67 11.01 4 13 -6 111.46 12.13 4 13 -6 102.45 11.07 4 13 -6 94.26 11.37 -4 13 6 109.33 11.66 -4 13 5 24.35 4.61 4 13 -5 27.85 3.81 -4 -13 5 23.51 2.90 4 -13 -5 20.21 2.69 -4 -13 5 21.13 2.75 4 -13 -5 22.00 2.79 -4 13 5 15.53 4.71 4 13 -5 20.60 3.86 4 -13 -5 24.18 2.99 -4 13 5 22.31 3.75 4 -13 -5 17.22 3.19 4 -13 -5 20.01 2.93 4 13 -5 15.96 3.60 4 13 -5 24.94 3.43 -4 13 5 23.65 3.63 4 13 -4 46.74 6.03 -4 13 4 45.42 6.09 4 -13 -4 41.78 5.55 4 -13 -4 43.56 5.37 -4 13 4 38.63 6.46 4 -13 -4 61.15 5.57 -4 -13 4 52.33 5.37 -4 -13 4 51.39 5.26 4 13 -4 56.09 6.09 4 -13 -4 52.14 5.33 -4 13 4 47.77 7.05 4 13 -4 49.73 6.27 -4 13 4 50.95 6.56 4 13 -4 50.07 5.80 -4 13 4 46.96 5.88 -4 -13 3 1.87 1.92 -4 13 3 4.73 2.48 4 13 -3 1.98 2.20 -4 13 3 1.85 2.67 -4 13 3 0.42 3.36 4 -13 -3 4.57 1.58 4 -13 -3 4.77 1.51 4 13 -3 3.31 2.18 -4 13 3 4.52 2.55 -4 -13 3 3.71 1.35 -4 -13 3 4.67 1.38 4 13 -3 4.72 2.11 -4 13 3 3.83 2.89 4 13 -3 2.50 2.03 -4 13 3 4.18 2.29 -4 13 2 578.77 61.96 -4 -13 2 592.85 61.30 4 13 -2 677.36 62.10 -4 -13 2 571.24 61.98 4 13 -2 451.52 63.15 -4 13 2 525.99 62.25 4 -13 -2 685.23 61.57 -4 13 2 629.32 62.02 4 13 -2 725.29 62.01 -4 -13 2 775.52 61.57 4 13 -2 633.00 61.57 -4 -13 2 763.48 61.47 4 -13 -2 732.48 61.54 4 13 -2 645.63 62.06 -4 13 2 588.89 62.35 4 13 -2 672.91 61.77 -4 13 2 561.38 61.77 4 13 -1 18.13 3.38 -4 13 1 9.16 3.22 -4 -13 1 20.82 2.49 -4 -13 1 17.84 3.42 -4 -13 1 17.73 2.53 4 -13 -1 22.57 2.73 -4 -13 1 21.76 2.66 4 13 -1 22.77 2.82 4 13 -1 23.02 3.30 -4 13 1 14.34 3.62 4 -13 -1 19.18 2.73 -4 13 1 17.22 4.43 4 13 -1 30.33 6.28 -4 13 1 17.57 4.05 4 13 -1 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30.85 4.05 5 -13 -14 29.31 3.50 5 13 -14 27.23 4.10 5 -13 -13 3.08 2.89 5 -13 -13 3.59 1.51 5 13 -13 -1.07 1.94 -5 13 13 3.08 4.85 5 -13 -13 -0.14 1.45 5 13 -13 3.06 2.17 5 13 -13 2.12 2.22 5 -13 -12 8.70 3.11 5 -13 -12 8.33 1.90 5 13 -12 9.22 2.45 5 13 -12 4.21 3.39 -5 13 12 1.43 4.93 5 13 -12 7.03 2.28 5 13 -12 7.20 2.31 -5 13 12 6.87 2.93 5 -13 -11 11.84 3.38 5 -13 -11 10.48 2.10 -5 13 11 14.58 5.28 -5 13 11 10.64 4.58 -5 13 11 15.78 3.77 5 13 -11 14.90 4.02 5 13 -11 12.90 2.76 5 13 -11 15.57 2.72 5 13 -11 10.47 2.60 -5 13 11 9.25 3.16 5 -13 -10 207.32 19.24 5 -13 -10 177.37 18.33 -5 13 10 208.47 20.69 -5 13 10 184.15 20.60 -5 -13 10 189.99 18.27 5 13 -10 184.61 19.73 5 13 -10 175.80 18.49 5 13 -10 174.14 18.44 -5 13 10 206.93 19.12 5 13 -10 198.72 18.59 5 -13 -9 3.14 2.45 5 -13 -9 0.79 1.40 -5 13 9 0.56 3.63 -5 -13 9 0.43 1.27 5 -13 -9 -0.64 0.95 5 13 -9 2.03 3.00 -5 13 9 -1.08 3.64 5 13 -9 0.54 1.60 5 13 -9 2.66 1.70 5 13 -9 -0.71 1.73 -5 13 9 1.31 2.38 5 13 -8 15.07 3.47 5 -13 -8 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13 3 79.64 7.83 -5 -13 -4 58.96 6.48 -5 -13 -4 65.73 7.74 5 -13 4 51.37 6.61 5 13 4 68.10 9.72 -5 -13 -4 68.64 6.56 5 -13 4 54.06 6.47 5 13 4 68.12 7.00 -5 13 -4 59.13 7.28 -5 -13 -4 62.14 6.34 -5 13 -4 61.66 7.72 5 13 4 60.09 6.91 5 -13 5 3.27 1.70 -5 13 -5 1.44 2.56 -5 -13 -5 6.79 1.60 5 13 5 6.86 2.40 5 -13 5 2.60 1.84 5 13 5 5.92 5.21 -5 -13 -5 5.08 3.20 -5 -13 -5 3.86 1.52 -5 13 -5 2.85 3.09 -5 13 -5 3.72 2.59 5 13 5 6.50 2.51 -5 13 -5 3.67 2.94 -5 -13 -6 118.90 11.42 -5 -13 -6 102.21 9.94 5 -13 6 84.46 10.04 5 13 6 82.57 12.56 -5 13 -6 93.71 10.65 5 -13 6 93.43 9.89 -5 -13 -6 95.76 9.77 -5 -13 -6 91.41 9.77 -5 13 -6 106.19 11.09 -5 13 -6 128.03 10.93 -5 13 -6 85.05 10.57 5 13 7 18.43 4.42 5 -13 7 15.36 3.33 5 13 7 15.51 6.09 5 -13 7 24.20 3.37 -5 -13 -7 26.40 3.22 -5 13 -7 24.79 3.38 -5 -13 -7 18.24 3.12 -5 -13 -7 19.93 4.53 -5 13 -7 17.93 4.30 -5 -13 -7 30.55 3.17 -5 -13 -8 -0.35 1.52 5 -13 8 0.23 1.88 5 13 8 2.98 3.27 5 13 8 2.39 5.08 5 -13 8 1.39 1.45 -5 -13 -8 -0.83 1.30 -5 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14 -13 5.00 2.27 5 -14 -12 33.55 4.80 5 -14 -12 25.24 3.32 5 14 -12 21.27 3.68 5 14 -12 24.56 5.31 -5 14 12 22.21 6.46 -5 14 12 23.77 6.01 5 14 -12 23.22 3.59 5 14 -12 28.24 3.81 -5 14 12 28.51 4.76 5 -14 -11 11.83 3.30 5 -14 -11 7.79 2.03 5 14 -11 6.59 3.92 5 14 -11 11.07 2.47 -5 14 11 6.39 4.40 -5 14 11 12.20 5.11 5 14 -11 8.50 2.38 5 14 -11 7.96 2.30 -5 14 11 13.36 3.40 5 -14 -10 21.75 4.10 5 -14 -10 23.28 3.14 -5 14 10 26.00 6.39 -5 14 10 22.64 5.93 5 14 -10 21.92 4.65 5 14 -10 24.19 3.46 5 14 -10 21.65 3.24 5 14 -10 21.65 3.30 -5 14 10 24.35 4.37 5 -14 -9 16.82 2.57 5 -14 -9 8.08 3.13 -5 14 9 14.17 5.07 -5 14 9 11.47 5.10 -5 -14 9 17.34 2.36 5 14 -9 15.14 4.37 -5 14 9 14.44 4.67 5 14 -9 12.19 2.58 5 14 -9 5.97 2.24 -5 14 9 10.96 3.48 5 14 -8 116.93 16.15 5 -14 -8 158.92 16.31 5 -14 -8 159.85 15.76 -5 14 8 167.62 18.01 -5 14 8 171.29 17.93 -5 -14 8 173.02 15.71 5 -14 -8 159.36 15.49 -5 -14 8 154.03 15.48 5 14 -8 181.64 17.21 5 14 -8 147.94 15.69 -5 14 8 192.57 17.50 -5 14 8 176.83 16.52 5 -14 -7 48.90 5.70 5 -14 -7 56.60 5.38 5 14 -7 36.92 5.93 -5 14 7 42.29 7.08 -5 14 7 47.38 7.56 -5 -14 7 41.59 5.03 5 -14 -7 44.91 4.83 -5 -14 7 46.28 4.94 5 -14 -7 47.27 4.99 5 14 -7 52.69 6.66 5 14 -7 37.52 5.10 -5 14 7 53.06 6.09 5 14 -6 9.42 3.44 5 -14 -6 18.22 3.03 -5 14 6 17.74 3.58 5 -14 -6 18.33 2.62 -5 14 6 19.44 4.22 -5 14 6 14.79 4.75 5 -14 -6 17.39 2.32 -5 -14 6 14.36 2.33 5 -14 -6 13.66 2.12 -5 -14 6 13.65 2.17 5 14 -6 14.41 3.65 5 14 -6 14.38 2.46 -5 14 6 14.32 3.41 -5 14 5 2.27 3.16 5 -14 -5 1.19 1.46 -5 14 5 2.03 3.83 5 14 -5 2.20 2.46 -5 -14 5 1.48 1.40 5 -14 -5 2.10 1.24 -5 -14 5 2.04 1.25 5 -14 -5 4.29 1.36 5 14 -5 2.38 2.51 5 -14 -5 2.18 1.61 5 14 -5 0.88 2.35 -5 14 5 0.30 2.65 5 -14 -5 1.69 1.86 5 14 -5 3.52 2.17 -5 14 5 1.82 2.58 -5 14 4 2.12 2.92 -5 14 4 1.98 3.83 5 -14 -4 5.30 1.94 5 14 -4 5.88 2.93 -5 14 4 4.08 2.94 -5 -14 4 4.26 1.59 -5 -14 4 3.34 1.57 5 -14 -4 12.09 1.99 5 14 -4 1.26 2.36 -5 14 4 7.87 2.95 5 14 -4 4.12 2.79 -5 14 4 1.80 2.57 -5 14 3 24.39 4.54 5 14 -3 28.99 4.56 -5 -14 3 28.85 4.25 -5 14 3 23.39 4.69 5 -14 -3 29.02 3.68 5 14 -3 26.65 4.32 -5 -14 3 30.94 3.59 -5 14 3 32.47 4.73 -5 -14 3 34.18 3.54 5 -14 -3 27.87 3.48 5 14 -3 27.37 4.28 -5 14 3 18.69 4.70 -5 14 3 30.47 4.45 5 14 -3 29.33 4.07 5 14 -2 41.86 5.02 -5 14 2 20.59 4.63 -5 -14 2 34.19 3.73 -5 -14 2 23.01 4.63 -5 14 2 22.05 4.89 5 -14 -2 35.94 4.19 -5 14 2 28.98 5.84 -5 -14 2 47.71 4.16 -5 -14 2 31.91 3.77 5 14 -2 30.26 4.72 5 -14 -2 35.22 4.00 5 14 -2 21.01 4.28 -5 14 2 23.95 5.35 5 14 -2 34.80 4.41 -5 14 2 33.39 4.96 5 14 -1 43.24 5.46 -5 14 1 23.70 5.12 -5 -14 1 42.74 4.41 -5 -14 1 34.61 5.26 5 14 -1 39.52 5.13 -5 -14 1 42.81 4.59 -5 -14 1 38.01 4.40 5 -14 -1 40.27 4.54 5 -14 -1 39.17 4.63 5 14 -1 35.47 7.70 -5 14 1 38.09 6.30 -5 14 1 35.07 5.45 -5 14 1 40.95 6.18 5 14 -1 47.69 5.09 -5 14 1 35.04 5.18 -5 -14 0 184.87 16.88 -5 -14 0 158.98 17.60 -5 -14 0 180.49 16.86 5 14 0 184.99 17.44 -5 -14 0 189.31 17.00 5 -14 0 172.29 16.91 5 -14 0 178.71 17.03 5 14 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5.30 -5 -14 -5 0.82 1.56 -5 -14 -5 -1.11 2.72 -5 14 -5 -1.80 2.77 -5 14 -5 1.65 2.56 -5 14 -5 1.49 3.05 5 14 5 0.77 2.44 5 -14 5 0.68 1.42 -5 -14 -5 -0.90 1.30 5 14 5 -0.74 2.25 -5 14 -5 2.14 2.46 5 14 6 24.13 6.99 5 -14 6 15.68 3.45 -5 -14 -6 31.75 3.55 -5 -14 -6 26.39 4.86 -5 14 -6 36.98 5.25 -5 14 -6 25.00 4.57 -5 14 -6 37.70 4.57 5 -14 6 21.87 3.40 -5 -14 -6 26.30 3.27 -5 -14 -6 22.84 3.27 -5 14 -6 25.97 4.37 5 14 6 30.01 4.14 5 -14 7 0.21 1.75 5 14 7 -2.56 5.49 5 -14 7 -0.35 1.46 -5 -14 -7 -0.15 1.25 -5 -14 -7 0.16 1.41 5 14 7 1.34 2.42 -5 -14 -7 1.55 2.98 -5 -14 -7 1.58 1.64 -5 14 -7 0.35 3.03 -5 14 -7 -1.70 2.55 -5 -14 -8 207.87 19.21 -5 -14 -8 219.74 20.52 5 -14 8 155.47 19.08 5 14 8 199.98 22.68 -5 -14 -8 189.47 19.01 5 -14 8 183.15 19.04 -5 14 -8 207.50 19.11 -5 14 -8 220.85 20.16 -5 -14 -8 175.15 18.85 5 14 8 229.79 20.05 -5 14 -8 244.17 20.02 5 -14 9 0.86 1.86 5 14 9 4.43 5.25 5 -14 9 2.62 1.60 -5 -14 -9 2.05 1.20 -5 14 -9 1.31 3.01 -5 14 -9 1.76 1.59 -5 14 -9 3.52 2.79 5 14 9 7.30 3.41 5 -14 10 10.68 2.55 5 14 10 16.84 6.15 -5 14 -10 15.80 4.10 5 -14 10 13.97 2.43 -5 14 -10 16.21 2.61 -5 14 -10 16.14 3.57 5 14 10 25.09 4.38 -5 -14 -11 7.60 2.10 -5 -14 -11 7.76 3.50 -5 14 -11 8.32 2.18 -5 14 -11 7.68 2.76 5 14 11 12.89 3.83 -5 14 -11 2.72 2.87 -5 -14 -12 85.34 8.78 -5 -14 -12 74.37 9.54 -5 14 -12 89.51 9.39 -5 14 -12 74.94 9.54 -5 14 -12 77.12 8.71 -5 -14 -13 1.87 2.51 -5 -14 -13 1.63 1.59 5 14 13 0.34 3.23 -5 14 -13 -0.98 2.27 -5 14 -13 2.15 2.23 -5 14 -13 0.17 1.56 -5 -14 -14 8.43 2.76 -5 -14 -14 5.58 1.65 5 14 14 10.38 3.74 -5 14 -14 7.88 2.52 -5 14 -14 5.10 1.75 -5 14 -14 -0.25 1.92 -5 -14 -15 -0.45 1.99 -5 -14 -15 -0.25 1.24 -5 14 -15 1.54 1.91 5 14 15 2.10 3.00 -5 14 -15 -0.27 1.39 -5 -14 -16 1.90 1.82 -5 14 -16 0.48 1.57 5 14 16 3.69 3.03 -5 14 -16 0.81 1.25 -5 -14 -17 -0.33 1.11 -5 14 -17 -1.15 1.33 5 14 17 2.53 2.55 -5 14 -17 0.18 0.99 -5 14 -18 -0.80 0.96 -5 15 19 0.40 4.07 5 15 -19 -1.24 1.78 5 -15 -18 14.41 1.83 5 15 -18 12.78 2.26 5 15 -18 10.69 3.11 5 -15 -17 1.61 1.03 -5 15 17 0.50 4.52 5 15 -17 0.97 1.56 5 15 -17 3.09 3.02 5 -15 -16 23.25 3.88 5 15 -16 19.88 2.91 5 -15 -16 20.43 2.59 5 15 -16 21.82 3.21 5 15 -16 14.86 4.23 5 -15 -15 -1.17 2.51 -5 15 15 -0.54 4.74 5 -15 -15 0.67 1.18 5 15 -15 0.30 1.53 5 15 -15 0.40 1.78 5 15 -15 1.25 1.87 5 -15 -14 13.10 2.07 5 -15 -14 13.91 3.57 5 15 -14 14.27 2.51 -5 15 14 11.91 5.73 5 -15 -14 10.54 2.03 5 15 -14 13.61 2.73 5 15 -14 13.45 2.78 5 -15 -13 -0.63 2.79 5 -15 -13 1.72 1.41 5 15 -13 -0.94 3.32 5 15 -13 3.52 2.09 -5 15 13 8.04 5.07 5 -15 -13 0.25 1.33 5 15 -13 1.38 1.87 5 15 -13 2.98 2.02 -5 15 13 1.88 3.17 5 -15 -12 6.87 1.94 5 -15 -12 9.55 3.14 5 15 -12 7.17 3.90 5 15 -12 8.10 2.31 -5 15 12 13.80 5.74 -5 15 12 12.05 5.15 5 15 -12 8.32 2.14 5 15 -12 5.03 2.07 -5 15 12 10.61 3.65 5 -15 -11 7.17 2.92 5 -15 -11 6.30 1.85 5 15 -11 4.27 3.70 5 15 -11 5.08 2.18 -5 15 11 12.89 5.05 -5 15 11 4.75 4.53 -5 15 11 7.62 4.59 5 15 -11 3.02 1.87 5 15 -11 4.44 1.94 -5 15 11 5.16 3.36 5 -15 -10 228.03 22.34 5 -15 -10 215.51 21.64 -5 15 10 207.20 24.09 -5 15 10 192.79 23.82 5 15 -10 202.14 22.96 5 15 -10 212.98 21.63 -5 15 10 236.60 23.52 -5 15 10 259.51 22.72 5 15 -10 235.91 21.78 5 -15 -9 0.87 2.50 5 -15 -9 5.96 1.83 -5 15 9 10.77 5.03 -5 15 9 5.29 4.32 -5 -15 9 6.02 1.79 5 15 -9 2.68 3.11 -5 15 9 8.49 4.47 5 15 -9 4.10 1.83 -5 15 9 2.82 3.12 5 15 -8 -4.42 3.22 5 -15 -8 -1.77 1.62 5 -15 -8 -0.54 2.40 -5 15 8 2.55 4.43 -5 15 8 5.00 4.02 -5 -15 8 1.13 1.45 5 -15 -8 0.39 1.11 5 15 -8 1.28 2.86 5 15 -8 -1.16 1.53 -5 15 8 1.22 2.92 -5 15 7 24.28 5.46 -5 15 7 18.48 5.87 -5 -15 7 24.89 3.65 -5 -15 7 24.09 3.07 5 -15 -7 26.94 3.32 5 15 -7 26.32 5.10 5 15 -7 19.95 4.61 5 -15 -7 17.44 3.76 5 -15 -7 28.76 3.65 -5 15 7 37.65 5.03 -5 15 6 5.96 3.89 -5 15 6 8.31 4.36 -5 -15 6 8.55 1.88 5 -15 -6 8.59 1.55 -5 -15 6 5.80 1.52 5 -15 -6 5.88 1.57 5 15 -6 5.79 3.14 5 15 -6 4.31 2.87 -5 15 6 4.32 2.99 5 -15 -6 6.53 2.38 5 -15 -6 7.83 2.06 -5 15 6 7.30 3.27 -5 15 5 12.20 4.70 -5 15 5 23.46 5.79 -5 15 5 25.03 4.48 -5 -15 5 28.28 3.30 5 -15 -5 24.11 3.00 -5 -15 5 23.54 3.01 5 -15 -5 23.29 3.02 5 15 -5 24.25 4.31 5 15 -5 23.97 4.55 -5 15 5 25.30 4.45 5 -15 -5 26.36 3.36 5 -15 -5 20.71 3.43 5 -15 -5 20.42 3.23 -5 15 5 22.42 4.23 5 15 -5 22.04 3.81 5 15 -4 64.03 7.90 -5 15 4 46.85 7.72 5 -15 -4 71.89 7.06 -5 15 4 52.44 8.24 -5 15 4 60.70 9.24 -5 15 4 62.10 7.98 -5 -15 4 64.37 6.92 5 -15 -4 64.18 6.78 -5 -15 4 63.69 6.77 5 -15 -4 71.30 6.89 5 15 -4 59.89 7.66 5 15 -4 75.36 8.03 -5 15 4 57.79 8.35 5 15 -4 65.82 7.46 -5 15 4 74.17 7.89 5 15 -3 23.77 4.34 -5 15 3 22.16 4.38 -5 -15 3 20.46 3.79 -5 15 3 18.05 4.53 5 -15 -3 23.92 3.34 -5 -15 3 25.94 3.31 5 15 -3 25.94 4.08 -5 15 3 31.94 4.71 -5 -15 3 21.54 3.12 5 -15 -3 29.20 3.30 5 15 -3 25.54 4.12 -5 15 3 25.32 5.00 -5 15 3 27.43 4.29 5 15 -3 20.17 3.76 5 -15 -2 12.55 2.20 -5 15 2 2.71 3.02 5 15 -2 8.08 3.20 -5 -15 2 7.62 1.62 -5 -15 2 4.50 2.53 5 -15 -2 11.45 2.12 -5 15 2 5.22 4.09 -5 15 2 0.84 2.91 5 -15 -2 10.46 1.96 5 15 -2 5.37 2.59 -5 15 2 7.86 3.31 -5 -15 2 9.05 1.82 -5 -15 2 7.59 1.87 5 15 -2 1.19 2.33 -5 15 2 4.07 3.93 5 15 -2 13.01 2.80 -5 15 2 0.28 2.75 -5 -15 1 0.89 2.25 5 15 -1 -1.24 2.69 -5 -15 1 -0.14 1.20 5 -15 -1 0.78 1.36 5 15 -1 0.53 2.30 -5 -15 1 0.17 1.54 -5 -15 1 0.57 1.29 -5 15 1 1.02 3.60 5 -15 -1 0.34 1.50 -5 15 1 0.41 3.38 5 15 -1 -0.24 2.17 -5 15 1 1.42 2.66 -5 -15 0 75.23 7.08 -5 -15 0 63.47 7.89 -5 -15 0 66.37 7.02 5 15 0 60.75 7.61 5 -15 0 72.78 7.15 5 -15 0 74.74 7.26 5 15 0 50.84 10.04 -5 15 0 52.30 8.63 -5 15 0 48.42 8.26 5 15 0 67.05 7.64 -5 15 0 63.99 7.92 -5 15 -1 24.35 5.67 5 15 1 26.70 7.34 5 -15 1 30.72 4.04 -5 -15 -1 32.62 3.95 5 15 1 34.70 4.80 -5 -15 -1 35.74 5.13 -5 -15 -1 35.20 4.01 -5 15 -1 39.30 5.96 5 15 1 30.48 4.64 -5 15 -1 39.23 5.20 -5 -15 -2 146.84 15.67 -5 -15 -2 156.63 14.77 5 -15 2 134.59 14.78 -5 -15 -2 183.12 15.12 -5 -15 -2 146.15 14.71 5 15 2 156.68 15.40 -5 -15 -2 146.34 14.74 -5 15 -2 132.50 16.01 -5 15 -2 139.99 15.47 5 15 2 144.08 15.29 5 -15 3 10.68 2.38 5 -15 3 13.56 2.43 -5 -15 -3 15.04 2.53 -5 15 -3 14.97 3.57 -5 -15 -3 14.08 2.36 5 15 3 15.76 3.22 -5 -15 -3 11.57 2.18 -5 -15 -3 9.49 3.57 -5 -15 -3 15.11 2.40 -5 15 -3 10.29 4.02 5 15 3 13.94 3.26 5 -15 4 14.15 2.74 5 15 4 23.80 7.19 -5 -15 -4 21.10 4.13 -5 -15 -4 17.20 2.69 -5 15 -4 12.80 4.05 -5 15 -4 25.14 3.90 5 15 4 18.55 3.52 5 -15 4 16.73 2.75 -5 -15 -4 15.85 2.64 -5 15 -4 14.03 3.65 5 15 4 17.12 3.33 5 -15 5 16.86 3.01 5 15 5 26.23 7.14 -5 -15 -5 20.61 4.60 -5 -15 -5 23.58 3.08 -5 15 -5 17.36 4.41 -5 15 -5 19.76 4.17 -5 15 -5 30.68 4.23 5 15 5 20.48 4.02 5 -15 5 17.31 2.87 -5 15 -5 16.54 3.87 -5 -15 -5 21.51 2.89 5 15 5 19.37 3.62 5 -15 6 11.40 2.66 5 15 6 21.82 7.13 -5 -15 -6 21.11 4.40 -5 -15 -6 16.67 2.73 -5 15 -6 20.03 4.36 -5 15 -6 13.26 3.90 -5 15 -6 21.84 3.82 5 -15 6 11.64 2.51 -5 -15 -6 16.71 2.46 -5 15 -6 13.25 3.57 -5 -15 -6 15.68 2.54 5 15 6 21.22 3.68 5 -15 7 -0.79 1.65 5 15 7 -3.71 5.70 -5 -15 -7 -1.93 3.22 -5 -15 -7 -0.18 1.67 -5 15 -7 -1.13 2.61 -5 15 -7 2.43 3.19 5 -15 7 2.30 1.64 -5 -15 -7 0.30 1.28 -5 -15 -7 -0.83 1.39 5 15 7 0.57 2.49 5 -15 8 8.22 2.22 5 15 8 12.22 6.49 5 -15 8 10.68 2.15 -5 -15 -8 10.05 2.07 5 15 8 10.81 3.00 -5 -15 -8 8.52 1.87 -5 -15 -8 12.02 3.70 -5 -15 -8 13.88 2.51 -5 15 -8 14.72 3.30 -5 15 -8 10.52 3.26 5 15 8 15.39 4.00 -5 -15 -9 0.55 1.66 -5 -15 -9 -1.15 3.30 5 -15 9 -0.20 1.63 5 15 9 0.94 5.00 -5 15 -9 0.87 3.20 5 -15 9 0.86 1.38 5 15 9 2.70 2.42 -5 15 -9 1.49 1.44 -5 15 -9 3.06 2.77 5 15 9 1.66 3.28 -5 15 -9 1.39 2.43 -5 15 -10 119.21 12.94 5 15 10 157.72 13.78 -5 15 -10 123.45 13.70 -5 15 -10 112.83 12.28 -5 15 -11 2.27 2.31 5 15 11 9.64 3.75 -5 15 -11 4.92 2.88 -5 15 -11 2.48 1.64 -5 -15 -12 0.17 1.53 -5 -15 -12 0.97 2.87 5 15 12 3.76 3.47 -5 15 -12 -0.16 1.52 -5 15 -12 0.34 2.68 5 15 13 1.73 3.14 -5 -15 -13 2.01 2.63 -5 -15 -13 2.13 1.51 5 15 13 1.33 3.17 -5 15 -13 -0.29 2.29 -5 15 -13 0.74 1.53 -5 -15 -14 18.74 2.62 -5 -15 -14 17.52 3.36 -5 15 -14 19.70 3.11 -5 15 -14 14.41 2.52 -5 15 -14 19.30 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2.79 1.66 -5 16 11 2.69 3.18 5 -16 -10 25.32 4.37 5 -16 -10 22.11 3.43 -5 16 10 27.21 6.41 -5 16 10 22.65 6.25 5 16 -10 31.04 5.56 -5 16 10 33.93 6.59 -5 16 10 34.63 5.05 -5 16 9 17.78 5.58 -5 16 9 17.48 5.81 -5 -16 9 21.94 3.05 5 16 -9 20.82 5.08 5 -16 -9 27.81 4.00 5 -16 -9 19.29 3.13 -5 16 9 23.31 4.52 -5 16 8 100.83 13.93 -5 16 8 118.73 14.39 5 -16 -8 109.88 11.41 -5 -16 8 122.72 11.67 5 16 -8 119.14 13.18 5 16 -8 85.57 12.33 5 -16 -8 127.01 12.30 5 -16 -8 114.22 11.70 -5 16 8 142.94 12.89 -5 16 7 -1.89 3.83 -5 16 7 2.67 4.48 -5 16 7 8.01 3.45 -5 -16 7 0.41 1.27 5 -16 -7 3.26 1.37 -5 -16 7 1.68 1.51 5 16 -7 1.69 3.00 5 -16 -7 1.75 2.03 5 16 -7 4.30 3.28 5 -16 -7 2.02 1.82 -5 16 7 0.97 2.94 5 -16 -6 18.35 3.02 5 16 -6 17.45 4.24 -5 16 6 20.14 4.26 5 -16 -6 15.73 2.76 -5 16 6 9.53 4.14 -5 16 6 16.16 5.42 -5 -16 6 13.53 2.48 5 -16 -6 14.21 2.28 -5 16 6 14.63 4.00 -5 -16 6 17.70 2.44 5 -16 -6 18.26 2.49 5 16 -6 17.68 4.03 -5 16 6 18.00 5.04 -5 16 6 13.31 3.79 5 16 -6 15.69 3.28 5 -16 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18.35 2.57 -5 -16 2 12.21 2.20 5 -16 -2 17.81 2.63 5 16 -2 5.63 2.82 -5 16 2 10.03 4.36 -5 16 2 10.12 3.78 5 16 -2 12.72 3.26 5 16 -1 52.98 6.60 -5 -16 1 47.27 5.08 -5 -16 1 43.56 5.93 5 -16 -1 43.53 5.31 -5 16 1 51.90 6.43 -5 -16 1 55.48 5.45 -5 -16 1 42.22 5.11 5 16 -1 43.56 5.88 5 -16 -1 49.05 5.26 5 -16 -1 45.61 5.25 -5 16 1 37.82 6.99 -5 16 1 41.40 6.81 5 16 -1 45.94 5.92 -5 16 1 37.22 6.01 -5 -16 0 78.11 7.93 -5 -16 0 65.82 8.60 5 -16 0 82.15 8.07 -5 -16 0 76.41 7.94 5 16 0 87.28 8.83 5 -16 0 76.60 8.01 -5 16 0 65.61 9.43 5 16 0 71.74 8.59 -5 16 0 69.95 8.83 5 -16 1 0.87 1.46 5 16 1 0.92 5.80 5 16 1 -0.28 2.24 -5 -16 -1 -0.31 1.38 -5 -16 -1 -0.71 1.47 -5 -16 -1 0.32 2.46 -5 -16 -1 -0.77 1.39 -5 16 -1 -0.42 3.67 -5 16 -1 0.94 2.85 5 16 1 -0.80 2.43 5 -16 2 5.13 2.14 5 16 2 2.82 6.25 -5 -16 -2 13.24 2.45 -5 -16 -2 3.64 1.56 5 16 2 5.29 2.86 -5 -16 -2 4.90 1.70 -5 -16 -2 4.74 2.85 5 16 2 6.05 3.64 -5 -16 -2 9.00 1.91 -5 16 -2 2.22 3.34 -5 16 -2 3.73 3.81 5 16 2 5.49 3.05 -5 -16 -3 46.28 5.36 -5 -16 -3 52.65 6.57 5 -16 3 41.56 5.34 -5 -16 -3 47.26 5.48 -5 -16 -3 48.44 5.33 5 16 3 46.65 6.06 5 -16 3 51.60 5.41 -5 -16 -3 43.45 5.22 -5 16 -3 49.34 7.12 5 16 3 49.43 6.28 -5 16 -3 50.05 6.24 -5 -16 -4 54.29 5.78 -5 -16 -4 48.87 6.79 -5 -16 -4 55.72 5.76 5 16 4 51.29 6.43 -5 16 -4 55.64 6.74 5 -16 4 50.93 5.73 5 -16 4 37.91 5.58 -5 16 -4 53.70 7.21 -5 16 -4 61.19 6.68 5 16 4 52.79 6.67 -5 -16 -5 0.37 2.90 -5 -16 -5 1.75 1.62 5 -16 5 2.12 1.51 -5 -16 -5 1.15 1.42 -5 16 -5 0.98 2.65 5 16 5 1.42 2.51 5 -16 5 1.47 1.56 5 16 5 7.79 6.06 5 16 5 3.23 2.76 -5 16 -5 4.93 3.39 -5 16 -5 1.94 2.96 -5 16 -5 3.38 2.83 5 16 5 0.61 2.81 5 -16 6 2.03 1.56 5 16 6 2.92 5.55 -5 -16 -6 4.15 3.20 -5 -16 -6 4.29 1.94 -5 16 -6 5.77 3.18 -5 16 -6 3.53 3.08 -5 16 -6 3.95 2.71 -5 -16 -6 2.51 1.45 5 -16 6 3.18 1.62 -5 -16 -6 4.19 1.59 5 16 6 2.05 2.62 5 16 7 11.82 6.50 5 -16 7 4.23 1.77 5 -16 7 5.24 1.86 -5 -16 -7 9.80 1.75 -5 -16 -7 7.41 1.85 5 16 7 10.97 3.08 -5 -16 -7 14.31 3.90 -5 -16 -7 7.78 2.12 -5 16 -7 10.49 3.56 -5 16 -7 6.42 2.86 -5 -16 -8 88.75 8.75 -5 -16 -8 96.50 10.10 5 -16 8 56.57 8.46 5 16 8 98.90 13.23 -5 16 -8 90.55 10.43 -5 -16 -8 83.86 8.61 5 -16 8 79.73 8.59 -5 16 -8 108.32 9.87 -5 -16 -8 79.25 8.47 -5 16 -8 119.61 9.74 -5 -16 -9 46.97 5.32 -5 -16 -9 34.02 6.19 -5 16 -9 44.12 6.08 -5 16 -9 48.89 5.95 5 16 9 55.36 6.83 -5 16 -9 39.79 6.49 -5 -16 -10 4.17 3.07 -5 16 -10 6.92 2.61 -5 16 -10 5.66 2.54 -5 16 -10 0.40 2.96 5 16 11 17.65 4.55 -5 16 -11 6.70 2.41 5 16 11 15.12 4.05 -5 16 -11 10.36 2.81 -5 16 -11 9.34 1.95 -5 16 -11 3.97 3.03 5 16 12 47.06 6.02 -5 -16 -12 30.50 3.88 5 16 12 49.05 5.96 -5 16 -12 32.57 4.90 -5 16 -12 26.03 3.69 5 16 13 4.80 3.37 -5 -16 -13 3.87 1.59 -5 -16 -13 2.08 2.31 5 16 13 5.12 3.69 -5 16 -13 -1.60 2.16 -5 16 -13 1.82 1.42 -5 -16 -14 0.83 1.26 -5 -16 -14 0.22 1.98 5 16 14 3.25 3.17 -5 16 -14 1.56 1.15 -5 16 -14 2.62 1.81 -5 -16 -15 -1.20 1.66 -5 16 -15 -0.50 0.98 -5 -16 -16 5.71 1.56 5 16 16 8.53 2.81 -5 16 -16 8.06 1.64 -5 17 18 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17 1.54 4.59 6 -13 -17 2.63 1.39 6 13 -17 1.89 1.88 6 13 -17 0.21 2.04 6 13 -17 2.06 3.29 6 13 -17 4.66 2.13 6 -13 -16 6.32 3.15 -6 13 16 2.10 4.64 6 -13 -16 3.79 1.53 6 13 -16 5.13 2.09 6 13 -16 5.79 2.15 6 13 -16 1.82 3.46 6 13 -16 5.26 2.16 6 -13 -15 8.94 3.42 6 13 -15 5.73 2.36 6 -13 -15 4.99 1.67 6 13 -15 2.63 2.13 6 13 -15 5.07 2.36 6 -13 -14 165.73 14.73 6 13 -14 143.35 13.76 -6 13 14 155.63 17.16 6 -13 -14 119.92 13.22 6 13 -14 132.69 13.64 6 13 -14 128.54 13.73 6 -13 -13 6.16 1.55 6 -13 -13 8.40 3.26 6 13 -13 10.64 2.61 6 13 -13 11.19 4.18 -6 13 13 7.51 5.21 -6 13 13 4.41 4.22 6 13 -13 6.75 2.26 6 13 -13 3.84 2.31 6 -13 -12 8.53 3.12 6 -13 -12 8.54 1.86 6 13 -12 8.93 2.46 6 13 -12 5.24 3.83 -6 13 12 16.16 5.41 -6 13 12 7.43 4.42 6 13 -12 10.43 2.52 6 13 -12 7.96 2.29 6 -13 -11 15.15 3.76 6 -13 -11 16.89 2.68 6 13 -11 25.36 3.45 -6 13 11 18.90 5.62 6 13 -11 16.97 4.45 -6 13 11 22.78 5.93 6 13 -11 17.29 3.24 6 13 -11 21.96 3.19 -6 13 11 18.99 3.85 6 -13 -10 5.97 2.75 6 -13 -10 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3.60 8 6 -15 11.25 2.96 8 6 -15 12.50 2.08 8 6 -15 13.11 2.41 8 -6 -15 10.34 2.49 8 6 -14 4.70 1.74 8 -6 -14 3.93 2.00 8 -6 -14 2.23 1.93 8 6 -14 2.57 1.91 8 6 -14 3.05 2.21 -8 6 14 5.01 4.29 8 -6 -14 3.61 2.34 8 6 -14 1.85 1.97 -8 6 14 2.83 3.12 8 6 -14 0.88 3.30 8 6 -14 3.44 1.39 8 6 -14 3.83 2.37 8 6 -14 3.48 1.75 8 -6 -14 4.16 1.93 8 6 -13 81.47 11.45 8 6 -13 116.61 11.69 8 -6 -13 119.13 11.97 8 6 -13 122.94 11.49 8 -6 -13 134.12 11.88 8 -6 -13 99.80 11.57 8 6 -13 142.87 12.06 -8 6 13 114.50 12.70 8 6 -13 107.01 11.61 8 6 -13 118.95 11.87 8 6 -13 125.53 11.48 8 -6 -13 100.16 11.51 8 6 -12 0.44 1.27 8 -6 -12 0.70 1.60 8 -6 -12 4.54 2.63 8 6 -12 -0.19 1.56 8 -6 -12 1.35 2.03 8 6 -12 0.46 1.33 8 -6 -12 1.73 1.71 8 -6 -12 0.77 1.59 8 6 -12 0.42 1.66 -8 -6 12 0.58 1.65 8 6 -12 2.52 1.74 -8 6 12 2.16 2.75 8 6 -12 0.21 2.10 8 6 -12 0.39 1.61 8 6 -11 117.83 11.40 8 -6 -11 105.32 11.46 8 6 -11 125.96 11.55 8 -6 -11 112.22 11.70 8 -6 -11 103.68 11.50 8 6 -11 117.83 11.76 8 -6 -11 131.20 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5 -7 446.52 43.22 -10 -5 7 494.85 42.83 10 -5 -6 1.28 1.29 10 -5 -6 1.87 0.80 -10 -5 6 1.98 1.13 -10 -5 6 1.34 1.70 -10 5 6 2.12 1.72 10 5 -6 2.85 1.81 10 -5 -6 3.53 2.14 10 5 -6 2.15 2.05 10 -5 -6 0.32 1.48 -10 -5 5 3.09 1.81 -10 5 5 3.26 1.81 10 5 -5 3.43 1.80 -10 -5 5 3.84 1.22 10 -5 -5 3.60 2.33 10 -5 -5 2.94 1.72 10 5 -5 4.13 2.55 10 -5 -5 3.17 1.48 10 -5 -4 34.57 4.20 10 5 -4 30.54 4.83 10 5 -4 45.43 4.58 -10 5 4 36.67 4.70 -10 5 4 40.44 4.63 -10 -5 4 42.91 4.52 -10 -5 4 40.79 4.09 10 -5 -4 50.24 5.31 -10 -5 3 4.50 1.80 -10 5 3 6.85 1.98 -10 5 3 5.00 2.03 10 5 -3 4.55 1.88 -10 -5 3 3.67 1.35 10 -5 -3 8.74 3.02 10 5 -3 2.92 2.98 10 -5 -3 5.99 1.67 10 5 -3 4.04 2.50 10 -5 -2 45.82 4.97 -10 5 2 37.46 4.62 10 5 -2 52.00 5.85 10 5 -2 56.61 5.04 -10 5 2 46.92 5.14 -10 5 2 44.55 5.20 -10 -5 2 47.76 4.70 10 -5 -2 66.82 6.40 -10 5 1 1.59 1.89 -10 5 1 1.86 1.66 -10 -5 1 0.77 1.14 -10 5 1 0.83 1.44 10 5 -1 1.22 1.47 10 -5 -1 0.29 2.89 10 -5 -1 1.53 1.82 -10 5 1 0.54 0.86 10 -5 -1 0.43 1.99 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10.49 -10 6 13 85.79 12.12 10 6 -13 89.84 10.63 10 -6 -13 103.09 11.07 10 6 -13 74.71 11.55 -10 6 13 87.59 11.83 10 6 -13 95.83 10.97 10 -6 -13 92.89 10.59 10 6 -13 107.71 10.54 10 6 -12 1.43 1.68 10 -6 -12 -1.32 1.96 10 -6 -12 0.42 1.72 10 6 -12 -4.04 2.22 10 6 -12 0.20 1.70 -10 6 12 -1.91 3.42 10 6 -12 -0.43 1.82 10 -6 -12 -1.75 2.27 -10 -6 12 0.22 1.88 -10 6 12 2.07 2.88 10 6 -12 -0.42 2.97 10 6 -12 -0.47 2.20 10 6 -12 -2.30 1.68 10 -6 -12 -0.20 1.81 10 6 -11 180.39 15.65 10 -6 -11 170.69 15.86 10 -6 -11 157.09 15.60 10 6 -11 168.62 15.88 10 6 -11 152.97 15.47 -10 6 11 156.64 16.78 10 6 -11 158.68 15.61 10 -6 -11 158.28 15.82 10 6 -11 125.00 16.17 -10 6 11 160.68 16.67 -10 -6 11 160.25 15.75 10 6 -11 157.09 15.74 10 6 -11 148.78 15.34 10 -6 -11 133.70 15.40 10 6 -10 17.41 2.54 10 -6 -10 16.58 2.70 -10 6 10 26.40 4.30 10 6 -10 15.47 2.79 10 -6 -10 14.79 2.92 -10 -6 10 24.17 3.26 -10 6 10 26.13 4.27 10 6 -10 14.81 3.58 10 6 -10 17.42 3.12 10 6 -10 16.99 2.81 10 -6 -10 18.08 3.01 10 -6 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2.66 1.63 10 -6 -5 247.63 26.16 -10 6 5 270.09 26.53 10 6 -5 299.44 26.53 -10 6 5 268.65 26.72 -10 6 5 260.85 26.54 -10 -6 5 280.71 26.41 -10 -6 5 290.15 26.10 10 -6 -5 319.86 26.76 10 6 -5 252.57 26.51 10 -6 -5 255.40 26.24 -10 -6 4 10.43 2.21 -10 6 4 8.63 2.56 -10 6 4 7.99 2.35 10 6 -4 11.48 2.36 -10 -6 4 10.27 1.75 10 6 -4 3.36 2.72 10 -6 -4 9.85 2.90 10 -6 -4 11.49 2.10 -10 6 4 8.63 2.07 10 6 -4 11.84 2.54 -10 -6 3 16.01 2.47 -10 6 3 11.06 2.57 -10 6 3 12.67 2.69 10 6 -3 17.10 2.70 -10 -6 3 13.07 2.03 10 -6 -3 18.20 3.43 10 6 -3 6.10 3.06 10 -6 -3 14.74 2.32 -10 6 3 11.64 2.15 10 6 -3 14.88 3.21 -10 6 2 2.17 1.83 -10 6 2 4.47 2.03 -10 -6 2 3.25 1.36 10 6 -2 2.81 1.82 10 -6 -2 5.26 2.77 10 6 -2 4.73 3.20 10 -6 -2 3.64 1.81 -10 6 2 1.18 1.12 10 6 -2 4.03 2.43 10 -6 -1 322.77 21.67 10 -6 -1 268.94 21.73 10 6 -1 355.23 22.76 -10 6 1 291.13 21.53 10 6 -1 343.36 21.67 -10 6 1 280.95 21.69 -10 6 1 285.08 21.90 -10 -6 1 306.16 21.57 -10 -6 1 297.63 21.27 10 -6 -1 383.92 22.91 10 -6 0 63.40 6.53 -10 -6 0 45.21 4.79 10 -6 0 56.10 5.38 10 -6 0 42.13 5.23 10 6 0 48.16 6.19 -10 6 0 42.98 5.08 10 6 0 53.47 5.14 -10 6 0 35.78 5.00 -10 6 0 34.85 5.21 -10 -6 0 40.27 4.96 -10 6 0 38.58 5.50 -10 6 0 37.73 6.08 -10 -6 -1 136.57 13.91 10 -6 1 154.16 14.38 10 -6 1 136.22 14.40 10 6 1 167.07 15.31 -10 6 -1 146.82 14.16 10 6 1 167.53 14.21 -10 6 -1 129.35 14.12 -10 6 -1 120.79 14.35 -10 -6 -1 144.57 14.14 -10 6 -1 135.78 14.59 -10 6 -1 146.46 15.23 -10 -6 -1 135.00 14.89 -10 6 -2 54.14 7.78 -10 -6 -2 49.36 7.24 10 6 2 63.70 7.31 -10 -6 -2 69.70 6.40 -10 6 -2 48.80 6.37 10 -6 2 66.78 6.97 10 -6 2 53.68 6.79 10 6 2 60.98 7.83 -10 6 -2 58.74 6.54 10 6 2 67.47 6.58 10 -6 2 48.62 6.79 -10 -6 -2 64.16 6.50 -10 6 -2 61.02 7.10 -10 -6 -2 61.61 6.31 -10 -6 -3 449.55 38.12 10 -6 3 441.32 38.53 10 -6 3 379.51 38.42 10 6 3 471.45 39.52 -10 6 -3 316.78 37.93 -10 6 -3 424.49 38.14 -10 -6 -3 402.85 38.10 -10 6 -3 379.57 38.57 10 -6 3 372.73 38.39 -10 6 -3 438.40 39.24 -10 -6 -3 410.54 38.94 -10 -6 -4 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11 -15 40.79 5.01 -10 11 15 41.36 6.55 10 -11 -15 35.67 4.43 10 11 -15 39.74 6.38 10 -11 -14 70.71 7.76 10 11 -14 77.32 9.62 -10 11 14 85.45 9.79 10 11 -14 74.16 8.30 10 -11 -14 72.58 7.86 10 -11 -13 5.07 1.83 -10 11 13 11.32 4.46 -10 -11 13 7.38 2.37 -10 11 13 7.36 4.35 10 11 -13 9.18 3.82 -10 11 13 8.95 4.14 10 11 -13 9.77 2.77 10 -11 -13 6.60 2.07 10 -11 -12 -0.32 1.40 -10 11 12 1.16 3.49 10 -11 -12 1.04 1.68 -10 -11 12 1.03 1.88 10 11 -12 1.42 3.52 -10 11 12 -1.18 4.11 -10 11 12 0.88 3.48 10 11 -12 3.50 2.29 10 -11 -12 -0.70 1.82 10 -11 -11 16.68 2.64 -10 11 11 23.98 5.02 10 -11 -11 19.36 2.99 -10 -11 11 17.65 3.28 -10 11 11 21.03 5.16 10 11 -11 14.79 4.35 -10 11 11 8.52 4.43 10 11 -11 17.55 3.39 10 -11 -11 15.21 2.67 -10 11 10 69.24 8.86 -10 11 10 79.04 9.47 10 -11 -10 55.75 6.85 10 11 -10 71.00 8.54 -10 -11 10 78.07 7.72 10 11 -10 64.03 7.54 -10 11 10 78.25 8.82 10 -11 -10 64.94 7.03 -10 11 9 5.68 3.19 -10 -11 9 10.00 2.54 -10 11 9 4.04 3.66 10 11 -9 1.98 2.93 10 11 -9 2.85 2.23 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25.48 3.75 -10 12 13 3.28 3.96 10 12 -13 7.98 2.74 10 12 -13 10.10 4.04 -10 12 12 13.41 4.93 10 12 -12 9.79 2.84 -10 12 12 9.58 4.50 -10 -12 12 11.61 2.73 -10 12 12 8.20 4.65 10 12 -12 12.18 4.08 -10 12 11 18.13 5.00 10 12 -11 17.84 3.52 -10 12 11 12.16 4.56 -10 -12 11 26.17 3.77 -10 12 11 15.09 5.14 10 12 -11 24.63 4.79 -10 12 10 10.62 3.87 -10 12 10 16.37 4.75 10 12 -10 12.83 2.88 10 -12 -10 11.33 2.06 -10 -12 10 10.22 2.76 -10 12 10 16.22 4.89 10 12 -10 12.51 3.76 -10 12 9 73.84 9.84 -10 12 9 88.24 10.56 -10 -12 9 82.77 8.89 10 12 -9 95.49 10.05 10 12 -9 87.99 8.99 -10 12 9 73.86 10.03 10 -12 -9 75.11 8.32 -10 12 8 147.49 17.17 -10 12 8 186.47 18.14 -10 -12 8 169.11 16.04 -10 -12 8 181.73 16.65 10 12 -8 161.28 17.22 -10 12 8 160.33 17.53 10 12 -8 156.74 16.46 10 -12 -8 153.92 16.05 -10 12 7 8.53 3.02 -10 -12 7 11.02 1.97 -10 -12 7 8.79 2.43 10 12 -7 5.40 3.02 10 12 -7 7.64 2.76 -10 12 7 8.26 3.94 10 -12 -7 5.38 1.91 10 12 -6 42.86 5.24 -10 12 6 30.95 5.19 -10 -12 6 45.85 4.52 10 -12 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54.14 5.95 -10 -12 -3 44.30 5.16 -10 12 -3 55.61 6.73 -10 12 -3 42.38 5.01 10 12 3 45.87 5.51 -10 -12 -4 88.78 8.33 10 -12 4 64.90 8.39 -10 12 -4 78.19 8.77 10 12 4 95.67 9.07 10 -12 4 73.01 8.55 10 12 4 85.56 9.53 -10 12 -4 69.60 8.13 -10 12 -4 82.93 9.57 10 12 4 81.93 8.63 -10 -12 -4 76.31 8.16 -10 -12 -5 -6.11 3.57 10 -12 5 0.23 1.90 -10 -12 -5 1.08 1.72 -10 12 -5 2.05 2.17 -10 -12 -5 1.34 1.35 10 12 5 -1.39 2.49 10 12 5 1.24 3.04 10 -12 5 3.64 2.19 -10 12 -5 2.44 1.59 -10 12 -5 4.35 3.24 10 12 5 0.74 2.39 -10 12 -5 0.86 2.75 -10 -12 -6 7.70 3.43 10 -12 6 6.04 2.24 -10 -12 -6 3.13 1.94 10 12 6 8.37 2.72 10 12 6 6.16 3.53 10 -12 6 3.20 2.23 -10 12 -6 5.89 1.97 -10 -12 -6 2.83 1.52 -10 12 -6 9.83 3.50 -10 12 -6 4.51 2.91 10 -12 7 2.81 1.92 -10 -12 -7 4.93 3.49 -10 -12 -7 0.56 1.71 10 12 7 1.84 3.50 10 -12 7 0.49 1.86 10 12 7 -0.28 2.24 -10 12 -7 -0.91 1.72 -10 -12 -7 0.16 1.29 -10 12 -7 2.19 2.55 -10 12 -8 63.59 6.68 10 -12 8 58.01 6.88 10 -12 8 46.02 6.50 -10 -12 -8 59.87 6.68 -10 -12 -8 68.97 8.01 -10 12 -8 79.97 7.40 -10 -12 -8 59.68 6.44 10 -12 9 18.73 3.29 -10 -12 -9 22.72 3.46 -10 -12 -9 16.78 4.40 10 12 9 32.38 4.61 -10 12 -9 26.01 4.07 -10 12 -9 29.52 3.53 -10 12 -9 20.94 3.82 10 -12 10 0.17 1.50 -10 -12 -10 2.82 1.80 -10 -12 -10 1.92 2.81 10 12 10 2.58 2.96 -10 12 -10 -0.93 2.11 -10 12 -10 1.72 1.71 10 -12 11 3.19 1.46 -10 -12 -11 4.97 1.87 -10 -12 -11 5.52 2.53 -10 12 -11 2.42 1.74 -10 12 -11 8.66 2.32 -10 -12 -12 42.70 5.37 -10 12 -12 47.04 5.24 -10 12 -12 40.37 4.83 -10 -12 -13 4.40 1.82 10 12 13 2.72 2.76 -10 12 -13 1.26 1.63 -10 12 -13 1.04 1.37 -10 12 -14 0.63 1.30 10 12 14 2.20 2.39 -10 12 -14 -0.11 1.11 -10 12 -15 0.80 0.97 10 12 15 1.47 1.99 -10 12 -15 0.61 0.92 10 12 16 2.71 1.73 -10 12 -16 1.50 0.74 10 -13 -20 0.77 0.75 10 13 -20 3.57 1.87 10 -13 -19 3.19 1.13 10 13 -19 5.77 1.55 10 13 -19 2.49 2.61 -10 13 18 29.30 5.39 10 13 -18 27.33 3.75 10 -13 -18 31.31 3.45 -10 13 17 6.10 4.21 10 -13 -17 -0.11 1.23 10 13 -17 2.35 1.86 10 13 -17 3.09 3.34 10 -13 -16 13.09 2.15 10 13 -16 11.37 2.65 -10 13 16 20.87 4.84 10 13 -16 9.37 3.91 10 -13 -15 1.24 1.54 10 13 -15 3.73 2.02 10 13 -15 1.81 3.64 10 13 -14 59.67 7.04 -10 13 14 66.52 8.79 10 13 -14 57.53 8.28 -10 13 13 18.82 5.21 10 13 -13 19.71 3.36 10 13 -13 15.54 4.60 -10 13 12 -0.96 3.80 10 13 -12 -1.41 2.15 10 13 -12 5.66 3.68 -10 13 11 5.10 3.68 -10 13 11 -2.85 3.96 10 13 -11 2.37 2.24 10 -13 -11 2.51 1.31 -10 -13 11 2.85 2.21 -10 13 11 0.64 3.82 10 13 -11 1.37 3.22 -10 13 10 21.91 4.60 10 13 -10 10.93 2.87 -10 13 10 11.67 4.73 10 -13 -10 13.50 2.25 -10 -13 10 15.73 3.03 -10 13 10 17.20 5.10 10 13 -10 5.24 3.59 -10 13 9 6.66 3.59 -10 -13 9 8.68 2.64 -10 13 9 10.61 4.72 10 13 -9 5.44 3.27 10 13 -9 7.79 2.62 -10 13 9 9.62 4.34 10 -13 -9 8.21 1.91 -10 13 8 96.78 12.20 -10 13 8 98.45 11.47 -10 -13 8 100.71 10.62 10 13 -8 107.48 11.50 -10 -13 8 95.85 10.03 10 13 -8 95.64 10.49 -10 13 8 96.84 11.80 10 -13 -8 101.63 10.13 -10 -13 7 34.26 4.63 10 13 -7 34.99 5.40 -10 -13 7 37.59 4.22 -10 13 7 36.49 6.08 10 13 -7 34.33 4.70 10 -13 -7 36.12 4.54 10 13 -7 28.00 4.74 10 -13 -7 33.90 4.20 10 13 -6 163.26 18.40 10 -13 -6 173.99 18.21 10 -13 -6 168.29 18.01 -10 -13 6 201.91 18.05 -10 -13 6 197.84 18.43 10 13 -6 183.03 18.88 -10 13 6 170.26 19.33 10 13 -6 189.91 18.36 -10 13 6 197.98 18.59 10 13 -5 16.17 3.53 10 -13 -5 12.78 2.75 10 -13 -5 16.43 2.39 10 13 -5 16.50 3.76 -10 -13 5 17.14 2.58 -10 13 5 12.71 3.63 -10 13 5 16.47 4.43 10 13 -5 15.78 3.05 -10 13 5 12.78 4.43 -10 13 5 14.91 3.35 10 13 -4 1.41 2.37 10 -13 -4 -0.21 1.81 10 -13 -4 -0.73 1.35 10 13 -4 1.30 2.70 -10 13 4 -0.92 2.68 -10 -13 4 -0.14 1.19 -10 -13 4 0.50 1.36 -10 -13 4 1.13 1.77 -10 13 4 0.47 3.28 -10 13 4 1.26 3.49 10 13 -4 -0.69 2.11 -10 13 4 0.27 2.43 10 -13 -3 0.64 1.76 10 -13 -3 0.62 1.28 10 13 -3 3.15 2.61 -10 13 3 2.11 2.87 -10 -13 3 2.50 1.54 -10 -13 3 1.55 1.30 -10 -13 3 -0.22 1.72 -10 13 3 0.45 3.10 10 13 -3 2.07 2.20 -10 13 3 0.42 3.50 -10 13 3 3.01 2.76 -10 -13 2 52.64 8.03 10 -13 -2 66.45 7.22 -10 13 2 51.00 7.99 -10 13 2 53.68 7.55 -10 -13 2 68.58 6.99 -10 -13 2 66.38 6.79 10 13 -2 77.18 7.92 10 -13 -2 70.21 6.92 -10 -13 2 56.35 7.06 -10 13 2 63.87 8.47 -10 13 2 68.06 7.70 10 -13 -1 -1.51 1.95 10 13 -1 2.69 2.54 10 -13 -1 1.01 1.44 -10 -13 1 0.50 1.37 -10 13 1 3.24 2.71 -10 -13 1 0.60 1.31 -10 -13 1 3.15 1.86 -10 13 1 3.35 2.89 -10 -13 1 0.43 3.48 -10 13 1 -1.23 3.43 -10 13 1 2.26 2.88 10 13 -1 0.79 1.75 -10 13 0 27.12 5.74 10 -13 0 46.79 5.23 10 -13 0 38.15 4.79 -10 13 0 37.67 5.48 -10 -13 0 46.82 4.78 10 13 0 52.33 5.89 -10 -13 0 39.03 4.96 -10 -13 0 46.24 4.75 -10 -13 0 36.50 6.19 -10 -13 0 44.64 4.82 -10 13 0 31.26 6.07 -10 13 0 40.92 5.74 10 13 0 34.92 5.02 -10 13 -1 -1.18 2.56 10 -13 1 4.22 2.17 10 -13 1 1.80 1.59 -10 -13 -1 4.23 1.72 -10 13 -1 4.92 2.62 -10 -13 -1 3.04 1.52 10 13 1 3.74 2.59 -10 -13 -1 2.00 1.66 -10 -13 -1 2.35 1.63 -10 -13 -1 -0.44 3.41 -10 13 -1 3.99 3.40 -10 13 -1 2.61 2.90 10 13 1 3.87 2.13 -10 -13 -2 308.98 27.59 -10 -13 -2 308.95 29.17 10 -13 2 292.93 27.87 -10 13 -2 195.03 28.03 10 -13 2 259.01 27.57 -10 13 -2 287.02 28.18 10 13 2 350.41 28.51 -10 -13 -2 275.46 27.63 -10 13 -2 283.99 28.80 10 13 2 329.14 27.98 10 -13 3 1.14 1.87 10 -13 3 2.06 1.60 -10 -13 -3 3.07 1.51 -10 13 -3 3.09 2.43 10 13 3 2.02 2.57 -10 -13 -3 1.67 1.54 -10 -13 -3 4.41 1.74 -10 -13 -3 2.65 3.81 -10 13 -3 4.24 3.57 10 13 3 2.84 2.35 -10 -13 -4 31.40 3.94 -10 13 -4 30.14 4.48 10 13 4 34.85 4.74 10 -13 4 25.55 4.13 -10 13 -4 30.15 3.75 -10 13 -4 32.63 5.38 10 13 4 32.71 4.42 -10 -13 -4 27.41 3.80 10 -13 5 7.80 2.32 -10 -13 -5 7.19 2.04 -10 -13 -5 8.79 1.93 -10 13 -5 9.51 2.67 10 13 5 3.81 2.67 10 -13 5 7.97 2.37 -10 13 -5 8.28 1.94 -10 13 -5 8.39 3.75 10 13 5 8.82 2.94 -10 13 -5 13.31 3.20 -10 -13 -6 4.20 3.49 10 -13 6 0.63 1.76 -10 -13 -6 1.46 1.65 10 13 6 4.96 2.69 -10 13 -6 2.54 1.58 10 13 6 3.51 2.51 -10 13 -6 1.13 2.59 -10 -13 -6 1.83 1.42 10 -13 6 2.56 1.94 10 -13 7 -1.19 1.63 -10 -13 -7 -2.00 3.42 -10 -13 -7 1.65 1.77 -10 13 -7 -0.34 1.55 -10 -13 -7 -0.32 1.31 10 13 7 0.84 2.70 -10 13 -7 -1.09 2.57 10 -13 7 0.23 1.86 10 -13 8 0.92 1.56 -10 -13 -8 2.53 1.72 -10 -13 -8 1.50 2.93 -10 13 -8 4.56 1.75 10 13 8 4.27 3.05 -10 13 -8 3.35 2.45 10 -13 9 1.49 1.45 -10 -13 -9 5.44 1.92 -10 -13 -9 4.49 2.93 -10 13 -9 2.46 1.58 10 13 9 5.43 3.10 -10 13 -9 6.99 2.43 -10 13 -9 7.07 2.61 -10 -13 -10 83.95 9.22 -10 -13 -10 90.26 10.05 -10 13 -10 101.27 9.95 10 13 10 121.33 10.37 -10 13 -10 106.91 9.74 -10 13 -10 74.55 9.41 -10 13 -10 78.02 9.09 -10 -13 -11 2.01 1.46 -10 -13 -11 0.78 2.24 -10 13 -11 2.77 2.02 -10 13 -11 1.01 1.38 -10 -13 -12 -0.42 1.92 -10 13 -12 3.61 1.79 -10 13 -12 1.81 1.24 -10 -13 -13 -0.15 1.49 -10 13 -13 0.56 1.16 10 13 13 -3.03 2.47 -10 13 -13 0.14 1.44 -10 13 -14 -0.11 1.18 10 13 14 2.43 2.24 -10 13 -14 2.44 1.11 10 13 15 -1.13 1.80 -10 13 -15 -0.13 0.75 10 -14 -19 1.67 0.85 10 14 -19 0.90 1.06 10 -14 -18 3.17 1.14 10 14 -18 4.34 1.47 -10 14 18 1.60 3.39 10 -14 -17 5.49 1.37 -10 14 17 5.84 4.03 10 14 -17 4.81 1.83 10 14 -17 4.57 3.20 10 14 -16 38.19 5.10 -10 14 16 63.59 7.67 10 -14 -16 43.71 4.85 10 14 -16 55.81 6.79 -10 14 15 -3.70 3.99 10 -14 -15 -1.26 1.43 10 14 -15 -0.74 1.81 10 14 -15 3.38 3.24 -10 14 14 14.86 5.03 10 -14 -14 13.15 2.35 10 14 -14 17.39 2.96 10 14 -14 21.69 4.71 -10 14 13 1.95 4.12 10 14 -13 0.64 1.87 10 14 -13 0.45 3.26 -10 14 12 20.64 5.53 10 14 -12 19.78 3.38 10 14 -12 24.79 5.04 -10 14 11 12.73 5.01 10 14 -11 11.28 2.77 10 -14 -11 11.53 2.05 10 14 -11 18.01 4.33 -10 14 10 58.71 8.28 10 14 -10 57.98 6.74 -10 14 10 58.69 8.50 10 -14 -10 51.90 6.14 10 14 -10 64.89 7.96 -10 14 10 61.37 9.02 -10 -14 10 62.30 6.85 10 14 -9 2.52 2.18 -10 14 9 1.43 4.17 10 -14 -9 2.73 1.51 -10 -14 9 7.17 2.23 -10 14 9 5.05 4.16 10 14 -9 6.30 3.12 -10 14 8 217.38 22.05 -10 -14 8 201.27 20.12 10 14 -8 232.17 21.13 10 14 -8 200.83 20.03 -10 14 8 204.65 21.40 10 -14 -8 186.71 19.64 10 -14 -7 2.32 1.58 10 14 -7 2.02 2.59 -10 -14 7 4.73 2.18 10 14 -7 0.76 2.66 -10 -14 7 0.82 1.43 10 14 -7 1.37 2.12 -10 14 7 0.46 4.00 -10 14 7 0.82 2.60 10 14 -6 47.03 6.68 10 -14 -6 48.50 6.04 10 -14 -6 54.37 6.28 -10 14 6 58.11 7.08 -10 -14 6 62.78 6.11 10 14 -6 48.34 6.92 -10 14 6 52.75 8.03 -10 14 6 54.67 7.77 10 14 -6 56.63 6.40 -10 14 6 56.99 6.79 10 14 -5 2.40 2.61 10 -14 -5 0.22 1.76 10 14 -5 2.07 2.91 -10 -14 5 -0.68 1.54 -10 14 5 0.33 2.68 10 -14 -5 1.41 1.23 -10 14 5 3.18 3.82 10 14 -5 4.54 2.25 -10 14 5 0.90 3.86 -10 14 5 2.84 2.73 10 14 -4 29.79 4.50 -10 -14 4 15.39 4.30 10 -14 -4 19.10 3.24 10 14 -4 19.35 4.25 -10 -14 4 21.76 3.02 -10 14 4 20.05 4.13 -10 -14 4 19.07 2.79 10 -14 -4 22.83 2.88 -10 -14 4 20.00 3.44 -10 14 4 15.17 4.81 10 14 -4 23.39 3.53 -10 14 4 10.64 4.63 -10 14 4 19.76 3.99 10 14 -3 4.94 2.84 -10 -14 3 4.05 3.21 10 -14 -3 5.22 2.03 10 -14 -3 4.43 1.47 10 14 -3 6.71 3.21 -10 -14 3 5.36 1.67 -10 14 3 1.91 2.75 -10 -14 3 4.23 1.52 -10 -14 3 4.75 2.09 -10 14 3 4.41 3.44 10 14 -3 3.88 2.31 -10 14 3 5.22 3.96 -10 14 3 5.50 2.99 -10 -14 2 8.28 3.78 10 -14 -2 11.10 2.63 10 -14 -2 8.76 2.02 10 14 -2 10.70 3.38 -10 -14 2 16.91 2.43 -10 14 2 7.21 3.22 -10 -14 2 11.91 2.03 -10 -14 2 9.06 2.38 -10 14 2 9.97 3.96 10 14 -2 14.52 2.85 -10 14 2 12.05 4.16 -10 14 2 7.91 3.34 10 -14 -1 1.09 1.86 -10 14 1 -2.29 3.27 10 14 -1 3.52 2.79 10 -14 -1 1.37 1.42 -10 -14 1 1.56 1.44 -10 14 1 -1.86 2.67 -10 -14 1 0.31 1.33 -10 -14 1 1.29 1.61 -10 -14 1 0.84 3.26 -10 14 1 -0.59 2.87 -10 14 1 -1.70 3.59 10 14 -1 -0.42 1.88 -10 -14 0 107.37 9.64 -10 -14 0 87.26 10.94 -10 14 0 56.29 10.40 10 -14 0 113.99 10.10 -10 14 0 92.34 10.39 -10 -14 0 98.91 9.63 10 14 0 117.38 10.78 10 -14 0 92.17 9.66 -10 -14 0 80.89 9.72 -10 14 0 84.09 11.01 -10 14 0 92.92 10.44 10 14 0 90.31 9.95 -10 -14 0 94.92 9.69 -10 14 -1 3.77 2.93 10 -14 1 2.87 2.01 10 -14 1 5.45 1.75 -10 -14 -1 3.48 1.64 -10 14 -1 1.81 2.64 -10 -14 -1 1.15 1.40 10 14 1 3.68 2.65 -10 -14 -1 4.06 1.76 -10 -14 -1 3.46 1.49 -10 -14 -1 6.48 3.72 -10 14 -1 2.05 3.66 -10 14 -1 3.31 2.99 10 14 1 1.84 2.25 -10 -14 -2 86.95 8.89 -10 -14 -2 92.97 10.62 10 -14 2 83.80 9.16 10 -14 2 78.88 8.90 -10 14 -2 83.80 9.61 10 14 2 103.77 9.93 -10 -14 -2 78.34 8.96 -10 14 -2 100.18 10.51 10 14 2 86.40 9.32 10 -14 3 0.37 1.52 -10 -14 -3 -0.35 1.39 -10 14 -3 1.15 2.42 10 14 3 -1.54 2.63 10 -14 3 0.67 1.93 -10 -14 -3 -0.43 3.55 -10 -14 -3 -0.51 1.53 -10 14 -3 -2.34 3.54 10 14 3 1.50 2.34 10 -14 4 111.93 13.38 -10 14 -4 145.90 14.12 10 14 4 174.01 14.50 10 -14 4 128.11 13.67 -10 -14 -4 143.03 13.54 -10 -14 -4 153.98 15.09 10 14 4 150.63 14.10 -10 -14 -4 119.44 13.35 -10 -14 -5 -0.84 1.40 -10 -14 -5 -0.53 1.73 -10 14 -5 0.29 2.57 10 14 5 -1.34 2.57 10 -14 5 -0.22 1.81 -10 -14 -6 1.78 1.69 10 14 6 5.24 2.69 -10 14 -6 1.93 2.43 -10 14 -6 0.31 1.37 -10 -14 -7 0.77 3.18 -10 -14 -7 0.71 1.61 -10 14 -7 0.16 1.37 10 14 7 3.94 3.04 -10 14 -7 0.79 2.54 -10 -14 -8 26.00 3.84 -10 -14 -8 33.40 5.15 10 14 8 44.20 5.24 -10 14 -8 31.42 4.50 -10 14 -8 28.33 3.69 -10 -14 -9 5.94 1.86 -10 -14 -9 3.88 3.02 -10 14 -9 1.75 1.50 -10 14 -9 2.66 2.60 10 14 9 5.91 3.11 -10 14 -9 3.67 2.34 -10 14 -9 2.99 2.30 -10 -14 -10 -0.31 1.45 -10 -14 -10 1.99 2.51 -10 14 -10 0.54 1.31 -10 14 -10 2.36 2.39 10 14 10 -1.64 2.64 -10 14 -10 2.49 1.98 -10 14 -10 0.22 1.80 -10 -14 -11 12.16 2.84 -10 14 -11 7.68 1.81 -10 14 -11 15.58 2.53 -10 -14 -12 23.10 3.32 -10 14 -12 24.50 3.14 -10 14 -12 19.36 2.67 -10 -14 -13 -0.13 1.40 -10 14 -13 -1.14 1.29 10 14 13 0.86 2.40 -10 14 -13 0.80 0.98 -10 14 -14 1.13 1.02 10 14 14 1.08 2.01 -10 14 -14 0.99 0.81 10 -15 -19 -0.09 0.58 10 15 -18 26.29 4.24 10 15 -18 27.89 3.24 10 -15 -18 31.49 3.20 10 15 -17 -0.92 2.53 10 -15 -17 0.08 0.95 10 15 -17 -0.44 1.31 -10 15 17 -1.79 3.50 10 15 -16 10.22 3.43 10 -15 -16 7.68 1.52 -10 15 16 7.40 4.49 10 15 -16 6.50 1.87 10 15 -15 3.11 3.29 -10 15 15 2.23 4.65 10 -15 -15 2.71 1.32 10 15 -15 2.98 1.81 10 15 -14 41.09 6.41 10 -15 -14 40.01 4.56 -10 15 14 46.02 7.22 10 15 -14 40.55 4.88 10 15 -13 6.89 3.71 -10 15 13 13.55 5.00 10 15 -13 9.07 2.40 10 15 -12 0.87 3.15 -10 15 12 -1.47 4.28 10 15 -12 2.60 1.93 10 15 -11 2.60 3.27 10 -15 -11 3.62 1.33 -10 15 11 4.94 4.36 10 15 -11 4.78 2.26 10 15 -10 28.36 5.07 10 -15 -10 18.98 2.82 -10 15 10 29.11 6.02 10 15 -10 21.13 3.38 -10 -15 9 2.52 2.04 10 15 -9 -3.35 3.29 10 -15 -9 2.71 1.50 -10 15 9 -1.95 4.15 10 15 -9 0.43 2.06 10 15 -8 73.81 8.28 -10 15 8 54.70 9.14 -10 -15 8 70.20 7.33 10 15 -8 67.61 7.18 -10 15 8 66.80 8.89 -10 -15 8 47.70 7.23 10 -15 -8 62.03 6.77 10 15 -7 -0.30 2.48 -10 -15 7 -1.31 2.47 10 -15 -7 -0.18 1.58 -10 -15 7 -0.82 1.45 -10 15 7 1.07 2.93 -10 -15 7 0.50 1.98 10 15 -7 0.38 2.71 10 15 -7 -0.88 1.81 -10 15 7 1.91 4.03 -10 15 7 0.29 2.70 10 15 -6 194.19 21.56 10 -15 -6 196.51 21.13 -10 -15 6 178.80 21.58 10 -15 -6 206.03 21.05 -10 15 6 184.02 22.71 -10 15 6 252.66 22.15 -10 -15 6 227.11 21.00 10 15 -6 222.42 21.94 10 15 -6 224.99 21.27 -10 15 6 247.69 22.88 -10 15 6 253.01 21.84 10 -15 -5 0.38 1.76 10 15 -5 -0.95 2.73 -10 -15 5 1.09 2.55 10 -15 -5 -1.53 1.91 -10 -15 5 -0.52 1.46 -10 15 5 0.34 2.83 -10 -15 5 0.72 1.90 -10 15 5 -2.86 3.90 10 15 -5 2.42 2.02 -10 15 5 -1.85 4.00 -10 15 5 2.07 2.92 10 15 -4 3.53 2.89 -10 -15 4 0.38 2.81 10 -15 -4 2.17 1.83 10 15 -4 1.06 2.98 -10 -15 4 1.05 1.51 -10 15 4 4.38 2.88 -10 -15 4 1.44 1.27 10 -15 -4 0.30 1.34 -10 -15 4 -0.47 2.01 -10 15 4 2.73 3.83 10 15 -4 0.66 2.03 -10 15 4 -0.91 3.90 -10 15 4 -1.80 2.85 10 15 -3 11.77 3.48 -10 -15 3 13.22 3.85 -10 15 3 12.16 4.31 10 -15 -3 11.98 2.62 10 -15 -3 11.33 2.17 10 15 -3 14.12 3.74 -10 -15 3 13.43 2.39 -10 15 3 11.25 3.43 -10 -15 3 12.83 2.22 -10 -15 3 12.83 2.68 10 15 -3 13.52 2.82 -10 15 3 8.99 4.21 -10 15 3 16.88 3.72 10 15 -2 20.31 4.07 -10 -15 2 9.60 3.60 10 -15 -2 18.51 2.98 -10 15 2 13.10 4.26 10 -15 -2 12.96 2.35 10 15 -2 17.04 3.83 -10 -15 2 15.51 2.54 -10 15 2 12.06 3.47 -10 -15 2 15.87 2.35 -10 -15 2 13.64 2.69 10 15 -2 12.29 2.95 -10 15 2 8.41 4.21 -10 15 2 17.32 3.69 -10 -15 1 13.87 3.84 10 -15 -1 4.33 2.01 -10 15 1 7.26 3.66 10 -15 -1 6.69 1.76 10 15 -1 8.07 3.14 -10 -15 1 6.38 1.88 -10 15 1 8.01 3.01 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4.57 10 -15 4 29.44 4.39 -10 -15 -4 42.34 4.60 -10 -15 -4 48.31 6.31 10 15 4 50.01 5.42 -10 15 -4 54.09 5.76 -10 -15 -4 35.15 4.41 -10 -15 -5 3.99 3.47 -10 -15 -5 3.59 1.80 -10 15 -5 -0.28 2.56 10 15 5 1.91 2.67 -10 -15 -6 14.45 2.71 -10 15 -6 16.65 3.45 10 15 6 18.02 3.69 -10 -15 -7 -0.33 1.64 -10 15 -7 3.90 2.77 10 15 7 3.35 2.85 -10 15 -7 0.75 2.36 -10 -15 -8 8.68 2.01 -10 -15 -8 3.94 2.91 -10 15 -8 8.06 1.77 -10 15 -8 9.51 2.94 10 15 8 13.61 3.33 -10 15 -8 13.24 2.81 -10 15 -8 6.39 2.74 -10 -15 -9 4.56 1.60 -10 -15 -9 1.48 2.34 -10 15 -9 0.24 1.20 -10 15 -9 -0.24 2.21 10 15 9 4.08 2.79 -10 15 -9 1.68 1.98 -10 15 -9 -0.51 2.08 -10 -15 -10 43.82 4.59 -10 -15 -10 42.99 5.34 -10 15 -10 48.89 5.14 10 15 10 57.15 5.87 -10 15 -10 40.60 4.89 -10 15 -10 30.56 4.26 -10 15 -10 34.87 4.77 -10 -15 -11 2.33 1.93 -10 15 -11 1.30 1.71 -10 15 -11 0.59 1.06 -10 -15 -12 -0.32 1.51 -10 15 -12 1.49 1.51 -10 15 -12 -0.32 0.84 10 15 13 3.62 2.23 -10 -15 -13 3.80 1.25 -10 15 -13 5.99 1.41 -10 15 -13 2.34 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247.51 17.56 11 5 -2 52.65 15.67 11 -5 -2 208.55 16.23 11 -5 -2 223.73 15.92 -11 5 2 113.24 15.24 11 5 -2 200.15 16.82 -11 5 2 153.54 15.52 11 5 -2 208.52 15.81 11 -5 -2 143.81 15.86 -11 5 2 167.49 15.87 -11 5 2 163.71 16.03 -11 -5 2 155.92 17.03 -11 -5 2 187.46 15.54 11 -5 -1 36.36 4.84 11 5 -1 2.45 4.01 11 -5 -1 23.08 3.53 11 -5 -1 28.31 3.32 11 -5 -1 16.79 3.55 11 5 -1 28.31 4.41 -11 5 1 22.40 3.05 11 5 -1 27.25 3.18 -11 5 1 21.04 3.21 -11 5 1 19.63 3.47 -11 -5 1 21.83 3.21 -11 5 1 22.56 4.90 -11 -5 1 25.17 4.58 11 -5 -1 18.03 3.51 -11 5 1 19.46 3.48 -11 -5 1 21.68 2.81 -11 5 0 0.46 2.01 -11 -5 0 3.32 1.42 11 5 0 3.36 2.98 11 -5 0 3.00 1.87 11 -5 0 1.50 2.21 -11 5 0 1.71 1.40 11 5 0 2.32 1.45 -11 5 0 2.29 1.64 -11 5 0 2.98 1.95 -11 -5 0 4.27 1.63 11 -5 0 3.53 2.13 11 5 0 1.30 2.33 -11 5 0 3.14 3.48 -11 -5 0 2.17 3.14 11 -5 0 -0.34 3.24 -11 5 -1 2.10 6.99 -11 -5 -1 2.32 1.25 11 5 1 1.07 2.81 11 -5 1 -0.77 1.74 11 -5 1 0.26 1.97 -11 5 -1 1.95 1.39 11 5 1 -0.58 1.37 -11 5 -1 -0.50 1.42 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7.28 11 6 -14 59.69 6.66 11 -6 -14 69.01 7.07 11 -6 -14 64.31 7.07 11 6 -14 67.36 7.23 11 -6 -13 229.80 22.54 11 6 -13 220.15 22.30 -11 6 13 236.50 24.22 11 6 -13 201.46 22.50 11 -6 -13 233.39 22.86 11 6 -13 221.51 23.74 -11 6 13 262.67 24.14 11 6 -13 239.53 22.84 11 6 -13 230.53 22.42 11 -6 -13 257.34 22.77 11 -6 -13 239.26 22.69 11 6 -13 212.61 22.65 11 6 -12 48.86 5.64 11 -6 -12 47.65 5.84 -11 6 12 53.25 7.48 11 6 -12 45.79 5.92 11 -6 -12 50.63 6.18 -11 6 12 57.64 7.41 11 6 -12 44.04 6.99 -11 -6 12 57.77 6.20 11 6 -12 49.52 6.21 11 6 -12 60.38 5.92 11 -6 -12 55.28 6.10 11 -6 -12 51.51 6.05 11 6 -12 38.16 5.92 11 6 -11 69.89 7.73 11 -6 -11 59.89 7.78 -11 6 11 66.52 9.11 11 6 -11 78.79 8.10 11 -6 -11 61.92 8.06 11 6 -11 58.28 8.81 -11 6 11 75.22 9.20 -11 -6 11 82.87 8.25 11 6 -11 72.93 8.17 11 6 -11 85.43 8.04 11 -6 -11 81.73 8.25 11 -6 -11 85.17 8.13 11 6 -11 73.47 8.29 11 6 -10 0.98 1.31 -11 6 10 0.79 2.79 11 6 -10 -0.63 1.55 11 -6 -10 0.24 2.03 -11 -6 10 0.23 1.92 -11 6 10 2.27 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5.03 11 -6 -6 47.43 5.38 11 6 -6 39.83 5.16 11 -6 -6 44.88 4.97 -11 -6 5 345.68 30.59 11 -6 -5 325.88 30.71 -11 6 5 326.81 30.98 11 -6 -5 254.20 30.82 11 6 -5 260.71 30.79 11 6 -5 365.21 31.05 11 6 -5 286.79 31.07 -11 6 5 338.86 31.31 -11 6 5 328.47 31.18 -11 -6 5 378.38 31.05 -11 6 5 278.91 31.02 11 -6 -5 388.96 31.41 11 6 -5 325.09 31.16 11 -6 -5 321.68 30.80 11 6 -4 1.55 2.63 11 -6 -4 3.53 1.84 11 -6 -4 0.78 2.37 11 -6 -4 0.21 1.72 11 -6 -4 0.76 1.47 -11 6 4 1.25 1.39 11 6 -4 1.36 2.25 11 6 -4 0.37 1.84 -11 -6 4 1.70 1.33 -11 -6 4 1.48 1.82 -11 6 4 2.90 2.14 -11 6 4 0.24 1.96 -11 6 4 1.00 2.04 11 -6 -4 1.29 1.95 11 -6 -3 20.61 3.60 11 6 -3 3.50 3.12 11 -6 -3 13.67 2.67 11 -6 -3 16.21 2.46 -11 6 3 10.54 2.04 11 6 -3 13.18 3.28 11 6 -3 17.49 2.66 -11 -6 3 12.57 2.02 -11 -6 3 14.95 2.61 -11 6 3 14.07 2.84 -11 6 3 12.06 2.82 -11 6 3 9.01 2.84 11 -6 -3 9.72 2.56 -11 -6 3 10.01 3.74 -11 -6 2 53.81 8.01 11 -6 -2 85.21 8.17 11 -6 -2 75.92 7.24 11 -6 -2 86.23 7.09 11 6 -2 74.80 7.99 -11 6 2 67.05 6.84 11 -6 -2 55.71 6.98 11 6 -2 88.15 7.12 -11 6 2 66.82 7.09 -11 6 2 64.58 7.26 -11 6 2 50.86 7.11 -11 -6 2 81.34 6.69 -11 6 1 159.02 16.49 -11 -6 1 156.16 16.09 11 -6 -1 213.17 16.57 11 -6 -1 181.09 15.65 11 -6 -1 190.52 15.42 11 6 -1 182.48 16.23 -11 6 1 168.26 15.25 11 6 -1 158.31 15.62 11 6 -1 189.83 15.35 11 -6 -1 152.76 15.43 -11 6 1 155.31 15.38 -11 6 1 160.00 15.61 -11 -6 1 164.04 15.29 -11 6 1 151.58 15.60 -11 -6 1 167.14 15.02 -11 6 0 57.74 8.15 -11 -6 0 59.09 7.79 11 -6 0 83.57 8.37 -11 -6 0 76.04 6.80 11 -6 0 84.25 7.34 11 -6 0 65.30 7.25 11 6 0 90.38 8.41 -11 6 0 59.51 6.82 11 -6 0 59.53 7.18 11 6 0 73.29 7.56 11 6 0 70.80 7.00 -11 6 0 49.19 6.85 -11 6 0 57.16 7.24 -11 -6 0 66.91 6.97 -11 6 0 52.92 7.23 -11 -6 0 62.27 6.68 11 -6 1 7.83 3.49 -11 6 -1 0.69 6.41 -11 -6 -1 5.39 1.40 11 6 1 4.70 3.03 11 -6 1 3.98 2.00 11 -6 1 3.40 2.15 -11 -6 -1 3.65 1.49 -11 6 -1 2.24 1.64 11 6 1 3.11 1.69 -11 6 -1 0.93 1.60 -11 6 -1 4.58 2.42 -11 -6 -1 2.80 1.59 -11 -6 -1 5.57 2.99 11 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5 -7 144.72 15.59 -12 -5 7 178.07 15.24 -12 -5 6 9.47 1.69 12 -5 -6 6.89 1.80 12 -5 -6 3.90 2.31 12 5 -6 7.69 2.36 -12 -5 6 8.13 2.33 12 5 -6 5.02 2.46 -12 5 6 8.39 2.80 -12 5 6 7.37 2.36 12 5 -6 4.99 2.23 12 -5 -6 11.51 2.85 12 5 -6 11.19 2.95 12 -5 -6 9.59 2.35 -12 -5 5 1.42 1.14 12 -5 -5 0.15 1.37 -12 -5 5 1.67 1.90 12 5 -5 1.92 2.01 -12 5 5 -0.26 2.09 -12 5 5 1.95 1.98 12 -5 -5 1.95 1.97 12 5 -5 1.42 2.00 12 -5 -5 3.79 1.98 12 -5 -5 -0.28 2.49 12 5 -5 1.41 2.83 12 5 -4 5.58 3.40 12 -5 -4 18.84 3.72 12 -5 -4 15.07 2.90 12 -5 -4 16.61 2.48 -12 5 4 11.67 2.41 12 5 -4 14.13 3.32 12 5 -4 14.65 2.56 -12 5 4 19.90 3.19 -12 5 4 12.14 2.89 -12 -5 4 17.93 2.90 12 -5 -4 13.14 3.06 12 5 -4 15.01 3.02 -12 -5 4 16.16 2.26 12 -5 -3 132.28 11.63 12 5 -3 79.32 11.06 12 -5 -3 107.98 10.58 12 -5 -3 103.71 10.18 -12 5 3 91.21 10.03 12 5 -3 120.98 11.37 12 -5 -3 83.76 10.46 12 5 -3 99.33 10.70 12 5 -3 111.96 10.32 -12 5 3 103.04 10.59 -12 5 3 95.78 10.60 -12 -5 3 105.62 10.44 -12 -5 3 82.36 11.23 -12 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5.16 3.45 -12 -5 -5 1.93 2.94 -12 5 -5 1.23 2.98 -12 5 -5 -1.56 2.42 -12 5 -5 0.61 1.86 -12 -5 -6 40.24 5.28 12 -5 6 29.38 4.69 12 5 6 35.06 6.10 12 -5 6 36.91 4.86 -12 5 -6 2.59 6.29 -12 -5 -6 -4.77 6.55 -12 -5 -6 32.32 4.09 12 -5 6 34.63 4.98 -12 5 -6 34.88 5.29 -12 -5 -6 31.33 5.38 -12 5 -6 37.78 4.87 -12 5 -6 42.97 4.48 12 -5 7 20.77 3.63 12 -5 7 16.31 3.46 -12 -5 -7 19.88 3.70 -12 5 -7 -2.44 5.10 -12 -5 -7 -2.60 5.65 -12 5 -7 22.62 3.62 -12 5 -7 22.65 3.04 12 -5 7 14.00 3.77 -12 5 -7 21.05 4.05 -12 -5 -7 11.42 3.97 12 -5 8 0.91 2.88 -12 5 -8 1.88 2.89 -12 -5 -8 0.74 2.72 12 -5 8 1.84 2.25 12 -5 8 -0.28 2.42 -12 -5 -8 -0.28 2.15 -12 5 -8 4.53 4.75 -12 -5 -8 -6.76 5.05 -12 5 -8 0.21 1.78 -12 5 -8 2.43 2.42 12 -5 9 61.40 6.58 -12 -5 -9 33.69 5.96 -12 5 -9 32.24 5.94 -12 5 -9 85.16 6.14 -12 -5 -9 77.68 5.49 -12 -5 -9 8.84 6.55 -12 5 -9 2.59 5.90 12 -5 9 52.31 6.08 -12 -5 -10 37.72 3.91 -12 5 -10 48.92 4.61 -12 5 -10 15.12 4.25 -12 -5 -10 23.15 4.58 12 -5 10 35.55 4.92 -12 -5 -11 5.22 1.44 12 -5 11 2.99 2.56 -12 -5 -11 3.83 2.60 -12 5 -11 4.63 2.57 -12 5 -12 2.26 1.92 -12 -5 -12 -0.91 2.13 -12 5 -12 1.38 2.18 12 -5 12 -1.24 2.39 -12 -5 -12 -0.87 2.31 -12 -5 -13 17.14 2.63 -12 5 -13 8.90 2.11 -12 -5 -13 2.04 2.20 12 -5 13 16.38 2.84 -12 5 -13 0.24 2.24 -12 5 -14 0.42 1.37 -12 -5 -14 2.98 1.77 -12 5 -14 -0.44 1.47 12 -5 14 0.73 1.78 -12 5 -14 1.18 1.70 12 5 14 3.12 2.95 -12 -5 -14 0.43 1.88 -12 5 -15 2.52 1.23 -12 -5 -15 0.29 1.50 -12 5 -15 1.23 1.20 -12 -5 -15 -0.17 1.59 12 -5 15 2.14 1.57 -12 5 -15 -0.31 1.50 12 5 15 5.43 2.58 -12 -5 -16 0.77 1.16 -12 5 -16 0.26 0.99 -12 -5 -16 0.26 1.27 12 -5 16 0.58 1.10 12 5 16 2.19 1.99 -12 5 -16 0.11 1.03 12 -5 16 0.47 1.01 12 5 17 2.66 1.40 12 -6 -22 -0.64 1.09 12 -6 -22 0.11 1.21 12 -6 -22 0.93 0.81 12 -6 -21 3.43 1.44 12 -6 -21 2.72 1.73 12 6 -21 3.45 1.75 12 -6 -21 3.05 1.17 12 -6 -20 1.79 1.55 12 6 -20 -1.33 1.19 12 -6 -20 -1.39 1.93 12 6 -20 1.51 1.44 12 -6 -20 0.10 1.22 12 6 -20 1.06 1.92 12 -6 -19 12.09 2.34 12 6 -19 10.12 1.93 12 -6 -19 10.34 1.95 12 6 -19 12.55 2.72 12 -6 -19 9.36 2.59 12 6 -19 12.39 2.40 12 6 -18 2.90 1.51 12 -6 -18 6.34 2.18 12 -6 -18 2.70 1.57 12 6 -18 6.88 2.55 12 -6 -18 5.05 2.42 12 6 -18 6.71 2.31 12 6 -18 4.11 3.58 12 6 -17 153.59 14.73 12 -6 -17 152.38 15.02 12 6 -17 134.67 15.12 12 -6 -17 130.46 14.56 12 -6 -17 165.10 15.26 12 6 -17 169.80 15.19 12 6 -16 3.11 1.71 12 -6 -16 4.32 2.14 12 -6 -16 3.67 2.48 12 -6 -16 2.24 1.60 12 6 -16 4.67 2.72 12 -6 -16 2.17 2.41 12 6 -16 -0.24 2.40 12 6 -15 -0.36 1.66 12 -6 -15 1.55 2.00 -12 6 15 0.62 3.85 12 6 -15 0.72 2.08 12 -6 -15 1.43 2.28 -12 6 15 1.04 3.35 12 6 -15 2.52 3.61 -12 -6 15 0.35 2.59 12 -6 -15 2.58 1.58 12 6 -15 -1.59 2.25 12 6 -15 0.19 1.61 12 -6 -15 0.95 1.99 12 -6 -15 -1.46 2.38 12 6 -15 -0.50 2.44 12 6 -14 2.75 1.71 12 -6 -14 0.22 2.05 -12 6 14 5.24 3.86 12 6 -14 0.48 2.03 12 -6 -14 -3.14 2.38 -12 6 14 -1.53 3.64 12 6 -14 -0.99 3.87 -12 -6 14 0.36 2.46 12 -6 -14 1.66 1.55 12 6 -14 0.80 2.44 12 6 -14 -0.40 1.59 12 -6 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21.59 3.07 -12 11 -9 21.66 3.77 -12 11 -9 21.78 3.39 -12 11 -10 94.58 9.40 12 -11 10 71.36 9.26 -12 -11 -10 95.62 9.87 12 11 10 133.53 10.37 -12 11 -10 108.32 9.65 12 11 10 72.39 9.72 12 11 11 11.37 2.78 -12 -11 -11 7.97 2.23 12 -11 11 7.73 1.88 12 11 11 11.17 3.04 -12 11 -11 13.40 2.29 -12 11 -11 12.01 2.04 12 -11 12 0.11 1.05 -12 11 -12 0.12 1.25 12 11 12 2.56 2.29 -12 11 -12 0.13 1.30 -12 11 -13 -0.62 1.08 -12 11 -13 0.38 0.96 -12 11 -14 0.32 0.88 12 12 -20 17.78 2.26 12 12 -19 1.54 1.39 12 12 -18 4.28 1.82 12 12 -18 6.51 3.07 12 12 -17 2.78 1.86 12 12 -17 1.50 3.07 12 12 -16 2.16 2.06 -12 12 16 -0.34 3.35 12 -12 -16 0.85 1.06 12 12 -16 -0.41 3.33 12 -12 -15 3.23 1.37 -12 12 15 3.06 3.53 12 12 -15 1.93 2.12 12 -12 -15 7.45 1.70 12 12 -15 10.10 3.84 12 -12 -14 0.39 1.22 -12 12 14 1.22 3.69 12 12 -14 1.38 2.23 12 -12 -14 2.52 1.54 12 12 -14 0.45 3.35 12 12 -13 -0.91 3.29 12 -12 -13 0.14 1.20 -12 12 13 1.69 3.48 12 12 -13 0.24 2.35 -12 12 12 -0.43 3.66 12 12 -12 0.75 2.32 12 12 -12 3.66 3.49 -12 12 11 6.06 4.03 12 12 -11 7.12 2.65 -12 -12 11 5.35 2.30 -12 12 11 9.71 4.45 12 12 -11 8.55 3.80 12 12 -10 60.05 7.44 -12 12 10 65.95 8.72 -12 12 10 71.25 9.27 12 12 -10 72.30 8.61 -12 -12 10 61.60 7.43 -12 12 9 82.76 10.39 12 12 -9 81.98 9.75 -12 -12 9 90.98 8.96 12 -12 -9 70.75 8.06 12 12 -9 77.69 8.81 -12 12 9 88.73 10.03 12 12 -8 157.10 16.86 -12 -12 8 177.42 16.33 12 12 -8 144.04 16.19 -12 12 8 166.77 17.21 12 -12 -8 156.15 15.64 12 -12 -7 7.26 2.38 -12 -12 7 16.39 2.41 -12 -12 7 5.94 2.40 -12 12 7 9.07 4.01 12 12 -7 9.25 3.44 12 12 -7 11.34 3.17 -12 12 7 10.86 4.27 12 -12 -7 10.94 2.27 -12 -12 6 9.94 2.55 -12 12 6 9.56 4.04 -12 -12 6 8.50 1.91 -12 12 6 9.34 3.04 12 12 -6 5.42 2.82 -12 12 6 7.01 3.73 12 -12 -6 9.25 2.34 12 12 -5 7.00 2.62 12 -12 -5 7.24 2.27 12 12 -5 16.54 3.46 -12 -12 5 10.66 2.01 -12 12 5 7.97 2.84 -12 12 5 5.97 3.72 12 12 -5 7.24 2.81 -12 12 5 9.77 4.16 12 -12 -4 4.83 2.11 12 -12 -4 2.59 1.38 12 12 -4 5.12 3.04 -12 -12 4 4.40 1.66 -12 12 4 5.48 2.62 -12 -12 4 3.65 2.11 -12 12 4 7.84 3.46 12 12 -4 5.72 2.62 -12 12 4 2.41 3.62 -12 12 4 2.71 2.28 -12 -12 3 2.39 2.02 -12 12 3 5.02 3.09 12 -12 -3 6.20 1.62 12 12 -3 4.74 2.78 -12 -12 3 3.43 1.53 -12 12 3 3.68 2.55 -12 12 3 3.58 3.36 12 -12 -3 5.07 2.12 -12 -12 2 3.06 1.95 -12 12 2 2.01 2.72 12 12 -2 1.22 2.64 12 -12 -2 0.99 1.36 -12 -12 2 1.55 1.46 -12 12 2 0.83 2.35 -12 12 2 0.79 3.40 12 -12 -2 2.89 1.99 12 -12 -1 2.90 1.94 12 12 -1 2.41 2.66 12 -12 -1 2.76 1.56 -12 -12 1 4.36 1.65 -12 12 1 1.09 2.24 -12 -12 1 2.53 1.93 -12 12 1 3.46 2.61 -12 -12 1 0.93 3.64 -12 12 1 5.78 3.57 -12 -12 0 157.91 13.97 -12 -12 0 134.00 15.52 -12 12 0 95.91 14.44 -12 -12 0 137.51 14.22 12 -12 0 132.80 13.96 -12 12 0 134.67 14.41 12 12 0 186.16 15.08 -12 12 0 139.25 15.26 -12 -12 0 147.63 14.04 -12 -12 -1 1.08 1.65 -12 -12 -1 0.88 1.36 -12 12 -1 -0.78 2.17 12 12 1 -3.80 2.45 -12 -12 -1 0.49 1.39 -12 -12 -1 1.39 3.56 -12 12 -1 6.69 3.57 12 12 1 -1.19 1.80 -12 -12 -2 53.90 5.64 -12 -12 -2 39.87 5.60 -12 12 -2 60.10 5.72 -12 12 -2 56.21 6.95 12 12 2 51.54 5.90 -12 -12 -2 48.75 5.60 -12 12 -2 37.15 5.86 12 12 2 57.08 6.49 12 -12 3 5.14 2.25 -12 -12 -3 8.54 2.02 -12 -12 -3 3.16 3.52 -12 12 -3 6.07 1.89 -12 12 -3 6.02 3.26 12 12 3 6.20 2.27 -12 12 -3 3.13 2.06 12 12 3 3.69 2.47 -12 -12 -4 8.30 3.81 12 -12 4 6.69 2.36 -12 -12 -4 11.20 2.25 -12 12 -4 7.88 2.00 -12 12 -4 9.28 3.53 12 12 4 7.42 2.64 -12 -12 -4 6.84 1.85 12 12 4 9.82 2.84 -12 -12 -5 -0.83 3.41 12 -12 5 0.23 1.93 -12 -12 -5 -0.90 1.68 -12 12 -5 1.97 3.12 12 12 5 1.20 2.32 -12 12 -5 1.33 2.52 -12 -12 -5 -0.34 1.46 -12 12 -5 -0.52 1.59 -12 -12 -6 -1.97 3.04 -12 -12 -6 2.15 1.76 12 -12 6 -0.66 1.86 -12 12 -6 0.31 2.71 12 12 6 -2.23 2.46 -12 12 -6 -1.27 2.39 -12 12 -6 -1.88 1.60 -12 -12 -7 2.53 2.91 -12 -12 -7 7.76 2.04 12 -12 7 3.08 1.93 -12 12 -7 7.69 1.91 -12 12 -7 3.82 2.79 12 12 7 6.54 2.77 -12 12 -7 6.64 2.33 12 -12 8 99.62 12.60 -12 -12 -8 126.98 13.54 -12 12 -8 142.19 13.50 12 12 8 155.17 13.40 -12 12 -8 144.87 13.14 -12 12 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4.60 2.44 -12 13 11 4.42 3.80 12 13 -10 58.29 7.66 12 13 -10 53.59 6.65 -12 13 10 57.71 7.94 -12 -13 9 -0.53 1.95 -12 13 9 0.59 3.92 12 13 -9 0.81 2.83 12 -13 -9 -0.29 1.29 12 13 -9 -0.75 2.29 -12 13 9 2.65 3.97 12 13 -8 76.60 9.28 -12 -13 8 89.17 8.81 12 13 -8 77.61 8.68 -12 13 8 80.42 9.97 12 -13 -8 71.41 8.01 12 13 -7 47.10 6.18 -12 13 7 41.88 6.93 -12 -13 7 41.98 5.46 -12 13 7 52.37 6.21 -12 13 7 41.28 6.78 12 13 -7 40.00 5.57 12 -13 -7 44.72 5.33 12 -13 -7 39.45 4.90 12 -13 -6 61.38 6.78 -12 13 6 70.60 7.62 -12 13 6 54.23 8.18 12 13 -6 57.71 7.03 -12 13 6 57.91 8.03 -12 -13 6 55.15 6.39 12 13 -5 6.85 2.83 12 -13 -5 8.46 2.33 -12 13 5 12.16 3.75 -12 -13 5 6.26 1.78 -12 13 5 5.25 3.02 12 13 -5 8.16 2.69 -12 13 5 7.62 3.95 -12 13 5 10.01 2.95 12 13 -4 2.84 2.55 -12 -13 4 1.48 1.99 -12 13 4 0.47 3.20 12 13 -4 -0.67 2.79 -12 -13 4 2.07 1.57 -12 13 4 1.81 2.57 12 13 -4 0.77 2.44 -12 13 4 2.09 3.37 -12 13 4 2.32 2.46 -12 -13 3 7.74 2.40 -12 13 3 11.72 3.85 12 -13 -3 11.02 1.90 12 13 -3 8.86 3.08 -12 -13 3 7.85 1.92 -12 13 3 6.51 2.77 12 13 -3 9.32 2.94 -12 13 3 6.18 3.79 -12 13 2 40.29 5.37 12 13 -2 46.30 5.80 12 -13 -2 32.50 4.37 -12 -13 2 45.72 6.45 -12 -13 2 41.25 4.63 -12 13 2 44.24 6.26 -12 13 2 25.14 5.45 -12 -13 2 42.46 4.97 12 13 -1 -0.64 2.57 12 -13 -1 -0.17 1.30 -12 -13 1 1.77 1.41 -12 13 1 1.98 2.29 -12 -13 1 1.85 1.74 -12 13 1 0.41 2.68 -12 -13 1 1.82 3.34 -12 13 1 5.15 3.64 -12 13 0 14.79 3.95 -12 -13 0 17.51 3.31 12 -13 0 24.15 3.19 12 13 0 30.48 4.34 -12 13 0 20.99 3.78 -12 -13 0 27.79 5.36 -12 13 0 22.16 4.81 -12 -13 0 24.27 3.22 -12 -13 -1 1.50 1.61 12 13 1 8.16 2.72 12 -13 1 0.36 1.36 -12 -13 -1 0.89 1.36 -12 13 -1 2.41 2.26 -12 -13 -1 0.95 1.36 -12 -13 -1 0.45 3.63 -12 13 -1 -2.26 3.24 12 13 1 0.83 1.89 -12 -13 -2 93.02 8.50 -12 -13 -2 71.29 8.50 -12 13 -2 90.48 9.83 12 13 2 91.68 8.86 -12 -13 -2 78.53 8.45 12 -13 2 69.25 8.41 -12 13 -2 72.93 8.89 12 13 2 91.77 9.38 -12 -13 -3 0.17 1.55 -12 13 -3 2.12 3.07 12 13 3 3.64 2.21 12 -13 3 0.19 1.58 -12 -13 -4 25.76 5.15 -12 -13 -4 23.89 3.25 -12 13 -4 22.10 4.38 -12 13 -4 29.31 4.10 12 13 4 22.39 3.79 -12 -13 -4 20.41 3.10 -12 13 -4 20.30 3.02 -12 -13 -5 2.00 3.36 -12 -13 -5 0.17 1.49 -12 13 -5 5.15 2.90 12 13 5 -0.24 2.18 -12 13 -5 -1.04 2.36 -12 13 -5 0.16 1.47 -12 -13 -6 8.64 3.55 -12 -13 -6 7.17 1.94 -12 13 -6 13.95 3.39 12 13 6 4.69 2.63 -12 13 -6 7.13 2.68 -12 13 -6 6.06 1.89 -12 -13 -7 5.65 1.78 -12 -13 -7 6.52 3.23 -12 13 -7 5.73 1.76 -12 13 -7 7.28 2.91 12 13 7 6.20 2.67 -12 13 -7 3.66 2.29 -12 -13 -8 14.00 3.48 -12 13 -8 12.03 2.27 -12 13 -8 15.04 3.10 12 13 8 12.00 3.12 -12 13 -8 19.62 3.08 -12 13 -8 14.99 2.78 -12 -13 -9 1.57 2.27 -12 13 -9 2.00 1.34 -12 13 -9 4.10 2.24 12 13 9 3.32 2.53 -12 13 -9 4.85 2.08 -12 -13 -10 73.57 9.03 12 13 10 102.26 9.49 -12 13 -10 88.31 8.91 -12 13 -10 84.08 8.61 -12 -13 -11 5.60 1.78 -12 13 -11 3.66 1.25 12 13 11 6.40 2.49 -12 13 -11 2.81 1.57 -12 13 -12 -0.43 0.91 -12 13 -12 0.31 1.16 12 13 12 0.18 1.99 12 13 13 -0.30 1.78 -12 13 -13 0.39 0.72 12 -14 -19 0.44 0.62 12 14 -18 7.92 2.60 12 -14 -18 11.19 1.51 12 14 -18 9.93 1.72 12 14 -17 1.18 2.53 12 -14 -17 -0.25 1.01 12 14 -17 -0.49 1.38 12 14 -16 11.87 3.46 -12 14 16 7.48 3.63 12 -14 -16 11.25 1.83 12 14 -16 11.09 2.22 12 14 -15 8.87 3.47 12 -14 -15 10.34 1.80 -12 14 15 11.22 3.94 12 14 -15 9.33 2.28 12 14 -14 -0.40 3.05 -12 14 14 1.19 3.57 12 -14 -14 1.48 1.37 12 14 -14 0.38 1.76 12 14 -13 -0.41 3.25 -12 14 13 -1.25 3.82 12 14 -13 0.20 1.96 12 14 -12 1.66 3.13 -12 14 12 3.89 3.79 12 14 -12 1.73 1.97 12 14 -11 5.85 3.63 -12 14 11 -2.21 4.06 12 14 -11 0.45 2.09 12 14 -10 110.76 11.45 12 -14 -10 96.97 9.74 12 14 -10 94.05 10.34 -12 14 10 93.34 11.64 12 14 -9 1.60 3.04 12 -14 -9 1.13 1.36 -12 14 9 0.45 3.79 12 14 -9 -0.95 2.17 12 14 -8 160.09 16.80 12 -14 -8 152.33 15.59 12 14 -8 162.13 16.10 -12 14 8 170.75 17.35 -12 -14 7 6.15 2.21 -12 14 7 8.92 4.08 12 14 -7 3.22 2.77 12 14 -7 5.11 2.37 -12 14 7 4.41 4.02 12 -14 -7 4.71 1.79 12 -14 -6 12.29 2.29 12 14 -6 11.14 3.07 -12 14 6 18.95 4.76 -12 -14 6 9.10 2.08 -12 14 6 12.37 3.30 12 14 -6 8.35 2.84 -12 14 6 11.77 4.48 12 14 -5 2.85 2.53 -12 -14 5 2.05 2.98 -12 -14 5 1.75 1.97 -12 14 5 2.58 3.25 -12 -14 5 1.70 1.38 -12 14 5 -0.32 2.37 12 14 -5 0.99 2.19 -12 14 5 0.86 3.56 -12 14 5 0.52 2.44 12 14 -4 -1.18 2.56 -12 -14 4 3.36 3.32 -12 -14 4 0.74 1.81 -12 14 4 -1.99 3.27 12 14 -4 0.34 2.89 -12 -14 4 0.17 1.35 -12 14 4 0.93 2.53 12 14 -4 3.73 2.32 -12 14 4 2.12 3.74 -12 14 4 0.53 2.44 12 14 -3 9.47 3.09 -12 -14 3 6.43 3.60 -12 -14 3 9.15 2.38 -12 14 3 4.25 3.28 12 -14 -3 5.21 1.61 12 14 -3 2.05 2.80 -12 -14 3 6.48 1.77 -12 14 3 7.31 2.74 12 14 -3 7.03 2.47 -12 14 3 10.40 3.93 -12 -14 2 3.04 3.47 12 -14 -2 4.36 1.50 12 14 -2 7.08 3.05 -12 -14 2 2.65 1.52 -12 14 2 3.27 2.42 -12 -14 2 3.54 1.91 -12 14 2 3.16 3.02 12 14 -2 4.81 2.56 -12 14 2 2.45 3.49 -12 14 1 13.29 3.68 12 -14 -1 10.43 2.13 12 14 -1 10.31 3.34 -12 -14 1 13.11 2.28 -12 14 1 14.19 3.05 -12 -14 1 9.17 2.38 -12 -14 1 13.99 4.50 -12 14 1 7.60 3.79 -12 -14 0 62.13 7.77 12 -14 0 66.53 6.43 -12 14 0 53.01 6.58 12 -14 0 52.38 5.95 -12 -14 0 50.85 6.21 -12 14 0 52.25 7.33 -12 -14 0 48.81 5.89 12 -14 1 2.62 1.99 12 -14 1 7.77 1.85 -12 -14 -1 7.60 1.95 -12 -14 -1 7.44 2.05 -12 -14 -1 9.46 1.87 -12 -14 -1 11.73 3.99 -12 14 -1 10.91 3.80 12 14 1 9.10 2.40 -12 -14 -2 85.87 8.04 -12 -14 -2 74.07 9.41 -12 14 -2 84.80 9.31 12 14 2 71.50 8.30 12 -14 2 65.60 8.13 -12 14 -3 4.16 3.12 12 14 3 1.15 2.10 -12 -14 -3 -0.32 1.44 -12 14 -4 24.89 4.63 -12 14 -4 27.58 4.28 12 14 4 25.24 4.07 -12 -14 -4 26.93 3.48 -12 14 -5 0.93 2.77 -12 14 -5 2.01 2.42 12 14 5 1.68 2.29 -12 -14 -5 1.13 3.18 -12 -14 -5 -1.14 1.66 -12 -14 -6 1.05 2.92 -12 -14 -6 2.71 1.58 -12 14 -6 5.99 2.83 12 14 6 5.33 2.49 -12 14 -6 3.05 2.30 -12 14 -6 2.30 1.34 -12 -14 -7 -0.61 1.47 -12 -14 -7 1.27 2.46 -12 14 -7 -0.13 1.19 -12 14 -7 -0.78 2.39 12 14 7 1.68 2.50 -12 14 -7 -1.51 2.09 -12 -14 -8 69.84 7.87 -12 14 -8 83.95 7.83 12 14 8 84.81 7.88 -12 14 -8 72.90 7.43 -12 14 -8 55.17 7.15 -12 14 -8 58.19 6.81 -12 -14 -9 5.45 2.29 12 14 9 7.61 2.67 -12 14 -9 3.40 1.89 -12 14 -9 6.33 1.50 -12 -14 -10 2.10 1.90 12 14 10 3.75 2.33 -12 14 -10 4.11 1.67 -12 14 -10 2.04 1.15 -12 -14 -11 1.53 1.30 -12 14 -11 1.54 0.92 12 14 11 1.12 2.12 -12 14 -11 4.51 1.40 -12 14 -12 14.78 1.99 12 14 12 18.27 2.78 -12 14 -12 12.58 1.70 12 -15 -18 20.95 2.29 12 -15 -17 3.33 0.91 12 15 -17 1.37 1.14 12 15 -17 1.96 2.28 12 -15 -16 2.46 1.07 12 15 -16 3.54 1.41 -12 15 16 2.50 2.86 12 15 -16 3.49 2.64 12 -15 -15 -0.10 1.09 12 15 -15 0.56 1.49 -12 15 15 -2.35 3.39 12 15 -15 0.33 2.77 -12 15 14 1.12 3.46 12 -15 -14 2.52 1.34 12 15 -14 2.09 1.79 12 15 -14 -1.42 2.97 12 15 -13 3.20 1.87 -12 15 13 3.21 3.88 12 15 -13 5.23 3.26 -12 15 12 14.26 4.48 12 15 -12 11.70 2.59 12 15 -12 10.06 3.65 12 15 -11 -0.20 1.93 -12 15 11 2.59 3.91 12 15 -11 0.77 2.95 -12 15 10 41.34 7.00 12 15 -10 46.31 5.38 -12 -15 10 36.47 5.41 12 -15 -10 42.46 4.69 12 15 -10 53.92 6.49 -12 15 9 4.44 3.98 12 15 -9 2.19 2.07 -12 -15 9 2.05 2.46 12 -15 -9 2.03 1.35 12 15 -9 5.64 3.10 12 15 -8 59.43 6.66 -12 15 8 61.54 8.22 -12 -15 8 43.66 6.81 12 -15 -8 59.27 6.15 12 15 -8 61.52 7.47 -12 -15 7 3.78 2.85 12 -15 -7 5.54 1.87 -12 15 7 8.79 4.02 12 15 -7 2.97 2.37 12 15 -6 44.84 6.18 -12 -15 6 45.03 6.44 12 -15 -6 47.73 5.50 -12 15 6 53.84 7.33 12 15 -6 51.99 5.92 12 -15 -5 -0.36 1.78 12 15 -5 -0.87 2.60 -12 -15 5 -2.27 2.91 12 15 -5 1.64 2.04 -12 15 5 0.43 3.64 -12 15 5 -1.30 2.59 12 15 -4 10.24 3.21 -12 -15 4 10.17 3.64 12 15 -4 9.41 2.67 -12 15 4 8.06 4.09 12 -15 -4 8.64 2.19 12 15 -3 34.61 5.43 -12 -15 3 33.65 5.90 12 15 -3 43.18 5.12 -12 15 3 47.01 6.45 12 -15 -3 33.71 4.67 12 15 -2 62.33 7.10 -12 15 2 62.88 8.23 12 15 -2 64.17 7.62 -12 -15 2 52.47 7.78 12 -15 -2 60.40 6.83 -12 -15 1 12.30 3.84 -12 15 1 11.39 4.00 12 15 -1 14.42 3.11 -12 15 0 25.15 4.97 -12 -15 0 24.19 4.91 -12 15 -1 37.14 5.32 12 15 1 24.82 3.85 -12 -15 -1 25.20 4.95 -12 -15 -1 25.88 3.36 -12 -15 -2 41.49 6.55 -12 -15 -2 40.73 4.79 12 15 2 44.79 5.41 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3.03 1.69 13 -6 -14 5.01 2.30 13 -6 -14 3.12 2.40 13 6 -14 5.37 2.66 13 6 -13 173.27 18.32 13 -6 -13 180.51 18.58 -13 6 13 219.67 20.54 13 6 -13 183.37 18.67 13 -6 -13 170.36 18.81 13 6 -13 148.23 19.58 -13 6 13 229.84 20.46 -13 -6 13 231.47 19.73 13 6 -13 155.37 18.69 13 6 -13 172.91 18.42 13 -6 -13 194.08 18.77 13 -6 -13 205.44 18.83 13 6 -13 235.02 19.11 13 -6 -12 4.69 2.23 13 6 -12 3.41 1.73 -13 6 12 5.90 3.56 13 6 -12 1.96 1.89 13 -6 -12 2.55 2.45 -13 6 12 8.13 3.72 13 6 -12 2.78 3.39 -13 -6 12 3.22 2.31 13 6 -12 6.13 2.71 13 6 -12 3.66 1.88 13 -6 -12 6.39 2.32 13 -6 -12 4.94 2.43 13 6 -12 5.29 2.75 13 6 -11 96.68 10.82 13 -6 -11 98.17 11.00 -13 6 11 88.71 11.93 13 6 -11 95.66 11.09 13 -6 -11 93.93 11.38 13 6 -11 89.88 12.03 -13 6 11 102.52 12.26 -13 -6 11 127.90 11.52 13 6 -11 102.04 11.28 13 6 -11 114.29 11.22 13 -6 -11 111.62 11.38 13 -6 -11 104.06 11.18 -13 6 10 2.03 2.61 13 6 -10 1.45 1.98 13 -6 -10 0.82 2.26 13 6 -10 3.32 3.23 -13 6 10 1.69 3.02 -13 -6 10 2.95 2.34 13 6 -10 2.07 2.47 13 6 -10 5.84 2.92 13 6 -10 2.65 2.02 13 -6 -10 0.26 2.19 13 -6 -10 3.33 2.26 -13 6 9 4.73 2.96 13 -6 -9 -1.08 2.14 13 6 -9 1.93 2.09 13 6 -9 3.12 2.69 -13 6 9 1.57 2.88 -13 -6 9 2.35 2.20 13 6 -9 5.35 2.60 13 6 -9 5.32 2.92 13 -6 -9 1.80 2.06 13 6 -9 0.23 1.88 13 -6 -9 1.73 2.05 -13 6 8 0.97 2.17 13 -6 -8 -2.39 2.17 13 6 -8 2.43 2.04 -13 -6 8 2.55 2.12 13 6 -8 2.21 2.63 -13 6 8 0.30 2.08 13 6 -8 -2.25 2.36 13 -6 -8 2.64 2.34 13 6 -8 0.24 2.11 13 -6 -8 3.79 2.14 13 -6 -7 5.22 1.71 -13 6 7 4.28 2.10 13 6 -7 2.45 2.15 13 -6 -7 2.37 2.27 -13 -6 7 11.64 2.50 13 6 -7 -0.69 2.55 -13 6 7 8.55 3.09 -13 6 7 5.01 2.42 13 6 -7 5.68 2.36 13 -6 -7 8.45 2.50 13 -6 -7 4.06 2.52 13 6 -7 4.31 2.51 -13 -6 6 6.19 1.66 13 -6 -6 5.53 1.80 -13 6 6 4.23 1.90 13 -6 -6 2.87 2.23 13 6 -6 6.72 2.46 13 6 -6 6.12 2.74 -13 6 6 3.83 2.59 -13 6 6 5.89 2.58 -13 -6 6 8.45 2.36 13 6 -6 3.67 2.28 13 -6 -6 4.50 2.72 13 6 -6 3.25 2.56 13 -6 -5 291.64 27.21 -13 6 5 254.48 27.25 13 -6 -5 242.22 27.47 13 6 -5 251.94 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34.83 5.47 13 -11 -6 99.89 10.08 -13 11 6 92.27 11.24 -13 11 6 89.91 10.40 -13 -11 6 98.86 10.31 -13 11 6 88.40 10.97 13 11 -6 98.80 10.45 -13 -11 6 94.32 9.74 -13 11 5 -1.51 3.40 13 -11 -5 -0.65 1.83 -13 11 5 0.83 2.32 -13 -11 5 0.17 1.30 -13 11 5 0.43 2.84 13 11 -5 0.27 2.38 -13 11 5 -0.43 3.29 -13 11 4 10.85 3.65 13 -11 -4 6.09 2.24 13 11 -4 7.62 3.16 -13 -11 4 7.50 1.95 -13 11 4 10.51 2.72 -13 -11 4 8.85 2.45 -13 11 4 8.60 3.28 13 11 -4 15.00 3.19 -13 11 4 0.42 3.66 13 -11 -3 5.04 2.06 13 -11 -3 4.77 1.47 13 11 -3 2.08 2.60 -13 -11 3 4.50 1.66 -13 11 3 6.55 2.52 -13 -11 3 5.47 2.15 -13 11 3 4.25 2.95 -13 11 3 2.59 3.09 -13 11 3 2.80 3.28 13 -11 -2 33.84 4.24 13 -11 -2 28.72 3.65 13 11 -2 35.76 4.78 -13 11 2 32.76 4.39 -13 11 2 26.90 4.75 -13 -11 2 31.67 4.17 -13 11 2 33.68 5.33 -13 -11 2 32.95 3.75 13 -11 -1 -0.44 1.90 13 11 -1 0.87 2.41 -13 -11 1 0.35 1.42 -13 11 1 0.25 2.16 -13 11 1 -1.06 2.49 -13 -11 1 0.95 1.75 -13 11 1 -0.36 3.03 -13 11 1 0.36 3.12 -13 -11 0 -0.91 1.73 13 11 0 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8.02 14 12 -10 61.66 8.02 14 12 -9 42.59 5.52 14 12 -9 34.86 5.91 -14 12 9 43.38 6.15 14 12 -8 34.46 5.83 14 -12 -8 48.24 4.77 14 12 -8 44.84 5.79 -14 12 8 51.78 6.55 -14 12 7 4.55 3.64 14 -12 -7 4.09 1.66 14 12 -7 4.01 2.65 -14 12 7 2.62 3.16 -14 -12 7 2.70 2.07 -14 12 7 6.41 3.63 14 -12 -6 5.16 1.94 -14 -12 6 6.41 2.38 -14 12 6 7.04 3.41 14 12 -6 1.62 2.49 -14 12 6 4.46 3.30 14 -12 -5 1.08 1.84 -14 -12 5 0.67 1.26 -14 12 5 0.44 2.86 14 12 -5 1.36 2.44 -14 12 5 4.05 2.93 14 12 -4 42.08 5.13 -14 12 4 23.39 5.23 -14 -12 4 33.63 4.77 14 -12 -4 36.16 4.60 14 12 -4 40.56 5.16 -14 12 4 33.45 5.57 -14 -12 4 36.90 4.35 -14 12 3 7.29 3.14 -14 -12 3 6.03 2.24 14 -12 -3 3.47 2.00 14 12 -3 4.70 2.72 -14 12 3 4.30 3.26 -14 -12 3 5.96 1.78 14 -12 -2 15.61 2.60 -14 12 2 4.59 2.64 -14 -12 2 11.37 2.58 -14 -12 2 10.25 4.27 -14 12 2 14.08 3.92 -14 -12 2 11.51 2.20 14 -12 -1 31.44 4.14 14 -12 -1 28.19 3.63 -14 -12 1 28.83 4.06 -14 -12 1 31.42 5.63 -14 -12 1 29.24 3.76 -14 12 1 27.60 4.92 -14 -12 0 144.19 15.87 -14 12 0 157.98 16.60 -14 -12 0 148.88 15.69 14 -12 0 194.22 16.16 -14 12 -1 3.89 2.88 -14 12 -1 4.37 1.70 -14 -12 -2 10.67 4.11 -14 12 -2 12.23 3.55 14 12 2 12.64 2.48 -14 12 -2 16.35 2.46 -14 -12 -3 12.55 3.96 -14 12 -3 14.63 3.71 -14 12 -3 18.89 3.39 14 12 3 12.30 2.76 -14 12 -3 19.60 2.65 -14 -12 -4 15.93 4.06 -14 12 -4 16.17 3.55 14 12 4 14.30 2.82 -14 12 -4 14.21 3.08 -14 12 -4 15.29 2.51 -14 -12 -5 1.73 2.83 -14 12 -5 1.33 2.42 14 12 5 0.81 1.98 -14 12 -5 -0.86 1.95 -14 12 -5 0.15 1.44 -14 -12 -6 12.98 3.33 -14 12 -6 17.19 3.37 14 12 6 20.80 3.30 -14 12 -6 20.05 3.21 -14 12 -6 17.47 2.60 -14 -12 -7 2.93 2.45 -14 12 -7 1.21 1.36 -14 12 -7 4.68 2.36 14 12 7 4.95 2.29 -14 12 -7 3.50 1.95 -14 -12 -8 78.86 8.95 14 12 8 87.97 8.92 -14 12 -8 89.74 8.68 -14 12 -8 78.86 8.42 -14 -12 -9 0.50 1.54 14 12 9 -0.89 1.93 -14 12 -9 3.64 1.49 -14 12 -9 2.84 1.18 -14 -12 -10 2.51 1.19 -14 12 -10 2.72 1.14 -14 12 -10 2.44 1.13 -14 12 -11 6.21 1.22 14 12 11 7.68 1.93 14 -13 -18 8.95 1.26 14 13 -18 6.92 1.50 14 13 -17 6.83 1.68 14 13 -16 0.14 1.59 14 13 -16 1.48 2.58 14 13 -15 0.33 1.80 14 13 -15 0.66 2.62 14 13 -14 10.82 2.44 14 13 -14 8.15 3.45 14 13 -13 0.20 1.97 -14 13 13 1.22 2.84 14 13 -13 -2.23 2.98 14 13 -12 25.45 3.77 -14 13 12 24.92 4.57 14 13 -12 24.57 4.63 14 13 -11 2.29 2.20 -14 13 11 3.16 3.16 14 13 -11 8.72 3.37 14 13 -10 31.90 4.49 -14 13 10 30.59 5.43 14 13 -10 33.20 5.30 14 13 -9 0.49 2.22 -14 13 9 1.12 3.09 14 13 -9 0.72 2.59 14 -13 -8 35.41 4.23 -14 13 8 37.87 5.89 14 13 -8 42.63 5.26 14 -13 -7 8.56 1.93 -14 13 7 17.00 4.03 14 13 -7 12.00 2.91 14 -13 -6 8.21 1.92 -14 13 6 5.63 3.42 14 13 -6 9.31 2.92 -14 13 5 12.63 4.09 14 13 -5 14.64 3.14 14 13 -4 16.06 3.39 -14 13 4 13.56 4.21 14 13 -4 20.32 3.55 -14 -13 3 1.32 3.24 -14 13 3 1.80 3.28 14 13 -3 2.12 2.41 -14 -13 2 103.31 13.16 -14 13 2 108.92 12.70 14 13 -2 129.83 12.42 -14 13 1 3.75 3.13 -14 -13 1 7.00 3.81 -14 13 0 18.53 4.29 -14 -13 0 28.40 4.93 -14 13 -1 -0.96 2.76 -14 13 -2 -0.31 2.60 -14 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0.32 2.71 14 -15 -7 2.33 1.32 -14 15 7 1.42 3.23 14 15 -7 4.54 2.25 14 -15 -6 15.08 2.41 -14 -15 6 10.94 3.52 -14 15 6 19.24 4.27 14 15 -6 18.80 3.12 14 -15 -5 0.76 1.36 -14 -15 5 0.35 2.82 -14 15 5 -1.06 3.12 14 15 -5 -0.45 2.17 14 15 -4 30.90 4.35 -14 -15 4 26.25 4.81 14 -15 -4 26.02 3.55 -14 15 4 27.71 4.94 14 15 -4 31.30 4.27 14 15 -3 16.12 3.57 -14 -15 3 18.12 4.36 -14 15 3 24.72 4.44 14 15 -3 21.45 3.59 14 15 -2 110.03 11.76 -14 -15 2 111.66 12.32 -14 15 2 102.32 11.99 14 15 -2 113.11 11.52 14 15 -1 4.57 2.88 -14 -15 1 4.79 3.06 -14 15 1 3.18 2.81 14 15 -1 1.37 2.13 -14 -15 0 32.17 5.69 -14 15 0 36.84 5.52 14 15 0 48.89 5.31 -14 -15 -1 15.06 4.08 -14 15 -1 18.09 3.73 14 15 1 19.27 3.39 -14 15 -2 9.47 3.04 -14 15 -2 12.80 2.88 -14 15 -3 3.01 2.36 -14 15 -3 -0.42 1.91 -14 -15 -4 5.47 2.82 -14 15 -4 8.53 2.65 -14 15 -4 7.84 2.28 14 15 4 4.44 2.00 -14 -15 -5 5.71 2.51 -14 15 -5 5.41 2.31 -14 15 -5 6.56 2.05 14 15 5 5.99 1.94 -14 -15 -6 5.63 2.28 -14 15 -6 9.98 2.22 -14 15 -6 7.93 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16 -4 8.82 2.38 14 -16 -3 1.79 1.53 14 16 -3 2.00 2.32 -14 -16 3 1.94 2.80 -14 16 3 1.58 2.63 14 16 -3 -1.01 1.98 -14 -16 2 27.17 4.68 14 16 -2 25.33 4.23 -14 16 2 27.15 4.52 14 16 -2 29.55 3.98 14 16 -1 58.03 6.99 -14 -16 1 49.78 7.11 -14 16 1 54.49 7.11 14 16 -1 63.94 6.64 14 16 0 81.78 8.89 -14 -16 0 66.67 8.80 -14 16 0 69.47 8.72 14 16 0 87.80 8.42 -14 -16 -1 4.32 2.82 14 16 1 -0.28 2.61 -14 16 -1 -0.79 2.44 -14 16 -1 3.26 2.25 14 16 1 -0.19 1.95 14 16 2 31.64 4.79 -14 -16 -2 24.95 4.60 14 16 2 33.22 4.11 -14 16 -2 29.54 4.40 -14 16 -2 30.67 4.19 14 16 3 -1.90 1.88 -14 16 -3 -1.80 2.17 -14 16 -3 1.13 1.86 14 16 4 1.92 1.83 -14 16 -4 2.24 2.09 -14 16 -4 0.51 1.75 -14 -16 -5 0.22 2.02 14 16 5 0.57 1.45 14 16 5 1.39 1.45 -14 16 -5 1.27 1.86 -14 16 -5 0.46 1.52 -14 16 -5 2.26 1.59 -14 -16 -6 5.32 2.05 14 16 6 2.99 1.64 -14 16 -6 10.41 2.10 -14 16 -6 6.60 1.66 14 16 6 6.38 1.69 -14 -16 -7 4.79 1.61 -14 16 -7 2.77 1.32 14 16 7 4.20 1.27 -14 16 -8 19.30 2.19 -14 -16 -8 12.37 2.21 14 16 8 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4.92 4.23 15 -6 1 8.43 2.14 15 6 1 10.40 3.67 15 -6 1 7.30 2.90 -15 -6 -1 10.24 2.41 -15 6 -1 7.11 4.06 -15 -6 -1 2.50 3.53 15 6 1 10.61 3.68 15 -6 1 10.58 2.92 -15 6 -1 12.38 2.80 15 -6 2 33.53 5.49 15 6 2 4.58 5.06 -15 -6 -2 -7.16 7.22 -15 -6 -2 31.76 5.39 15 -6 2 29.73 3.77 15 6 2 32.25 5.47 -15 -6 -2 21.26 3.55 -15 6 -2 22.72 4.92 15 -6 2 34.62 4.56 15 6 2 28.65 4.92 -15 -6 -2 16.10 4.59 -15 6 -2 29.51 3.94 15 -6 3 146.69 12.20 -15 -6 -3 147.66 12.23 15 -6 3 161.57 10.90 15 -6 3 140.79 11.29 15 6 3 163.61 12.79 15 -6 3 152.20 11.49 15 6 3 158.81 12.04 -15 -6 -3 153.03 10.90 -15 6 -3 117.16 11.82 -15 -6 -3 104.68 11.40 -15 6 -3 168.88 11.25 -15 -6 -4 12.80 3.94 15 -6 4 23.84 3.28 15 6 4 24.80 4.97 15 -6 4 15.04 4.28 15 6 4 -1.59 4.57 -15 -6 -4 22.25 3.11 15 -6 4 19.87 3.72 15 6 4 24.24 4.69 -15 6 -4 16.72 4.24 -15 -6 -4 8.24 3.56 -15 6 -4 29.92 3.73 -15 -6 -5 15.28 3.71 15 -6 5 25.18 3.85 15 -6 5 17.39 3.55 15 6 5 24.11 4.41 -15 6 -5 9.91 3.68 -15 -6 -5 9.58 3.42 -15 6 -5 19.21 3.25 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86.62 9.57 15 -13 -7 0.64 1.21 -15 13 7 0.65 2.79 15 13 -7 0.49 2.28 15 -13 -6 81.99 8.54 15 13 -6 91.14 9.31 -15 13 6 77.96 9.60 -15 -13 5 7.42 3.55 -15 13 5 3.27 2.98 15 13 -5 5.31 2.75 -15 -13 4 0.42 3.30 -15 13 4 3.88 2.83 15 13 -4 0.51 2.34 15 13 -3 -0.49 2.10 -15 -13 3 0.42 3.53 -15 13 3 0.32 2.51 15 13 -3 -0.51 2.53 -15 -13 2 5.81 3.68 -15 13 2 5.89 3.04 15 13 -2 8.23 2.66 -15 -13 1 0.41 3.24 -15 13 1 0.30 2.61 15 13 -1 2.05 2.41 -15 13 0 17.60 3.63 -15 13 -1 1.66 2.54 -15 -13 -2 51.87 7.10 -15 13 -2 54.22 6.35 -15 13 -2 52.23 6.47 -15 -13 -3 2.00 2.86 -15 13 -3 1.72 2.21 -15 13 -3 4.75 2.12 -15 13 -4 36.83 4.09 -15 13 -4 39.62 4.96 15 13 4 31.98 4.31 -15 13 -4 42.02 4.78 -15 -13 -4 36.16 5.33 -15 -13 -5 1.88 2.31 -15 13 -5 -0.22 1.11 -15 13 -5 1.04 1.94 -15 13 -5 0.84 1.70 15 13 5 0.91 1.66 -15 13 -6 21.00 2.64 -15 13 -6 24.79 3.34 15 13 6 21.74 3.10 -15 13 -6 18.59 2.96 -15 -13 -6 23.09 3.63 -15 -13 -7 4.45 1.79 15 13 7 1.39 1.68 -15 13 -7 3.23 1.43 -15 13 -7 2.95 1.11 -15 -13 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19.56 4.20 15 14 -2 30.81 4.29 -15 -14 1 6.70 3.31 -15 14 1 10.02 3.05 15 14 -1 7.78 2.71 -15 -14 0 44.10 7.27 -15 14 0 53.85 7.01 -15 14 -1 1.04 2.38 -15 14 -2 9.29 2.80 -15 14 -2 7.08 2.64 -15 14 -3 0.23 2.19 -15 14 -3 3.45 2.06 -15 -14 -3 -1.81 2.78 -15 14 -4 25.26 3.69 -15 14 -4 25.88 3.43 -15 -14 -4 17.18 3.72 -15 14 -5 2.44 1.95 -15 14 -5 -0.46 1.59 15 14 5 0.39 1.41 -15 -14 -5 0.72 2.12 -15 14 -6 18.74 2.73 -15 14 -6 17.44 2.42 15 14 6 11.01 2.22 -15 -14 -6 14.67 2.82 -15 14 -7 0.22 1.22 15 14 7 0.23 1.30 -15 -14 -7 1.76 1.59 -15 14 -8 -0.25 0.91 -15 -14 -8 0.79 1.09 15 15 -15 4.91 1.29 15 15 -14 2.04 1.38 15 15 -13 0.40 1.47 15 15 -12 4.63 1.79 -15 -15 11 3.72 1.80 -15 15 11 4.64 2.56 15 15 -11 2.46 1.70 -15 -15 10 3.56 2.01 -15 15 10 2.93 2.68 15 15 -10 2.46 1.94 -15 -15 9 -0.25 2.22 -15 15 9 0.28 2.71 15 15 -9 0.93 1.77 -15 -15 8 32.36 5.07 15 15 -8 40.30 4.79 -15 15 8 40.13 5.53 -15 -15 7 -0.60 2.58 15 -15 -7 0.32 1.05 -15 15 7 0.89 2.63 15 15 -7 1.00 1.98 -15 -15 6 46.02 6.43 15 -15 -6 47.38 5.24 -15 15 6 49.61 6.49 15 15 -6 54.23 5.91 15 -15 -5 12.93 2.29 -15 -15 5 13.42 3.57 -15 15 5 17.62 3.64 15 15 -5 22.66 3.24 15 -15 -4 0.55 1.27 -15 -15 4 1.00 2.79 -15 15 4 2.65 2.97 15 15 -4 3.82 2.23 15 15 -3 -0.22 2.15 -15 -15 3 -1.01 2.61 -15 15 3 1.44 2.53 15 15 -3 1.06 2.06 15 15 -2 9.78 2.72 -15 -15 2 5.05 3.07 -15 15 2 4.74 2.72 15 15 -2 11.46 2.57 -15 -15 1 -0.99 2.90 15 15 -1 -0.25 2.34 -15 15 1 -0.54 2.51 15 15 -1 -0.21 2.04 -15 -15 0 -0.97 2.80 15 15 0 -0.25 2.39 -15 15 0 0.51 2.44 15 15 0 3.70 2.14 -15 -15 -1 1.53 2.58 -15 15 -1 -1.44 2.28 -15 15 -1 0.62 1.99 15 15 1 2.40 2.15 -15 15 -2 52.57 6.64 -15 15 -2 52.70 6.76 -15 -15 -3 5.56 2.54 -15 15 -3 -0.21 2.02 -15 15 -3 0.69 1.78 15 15 3 4.17 2.05 -15 -15 -4 6.85 2.46 -15 15 -4 3.89 1.93 15 15 4 9.24 2.18 -15 -15 -5 0.62 1.83 -15 15 -5 0.99 1.72 -15 15 -5 0.14 1.40 15 15 5 -1.36 1.66 -15 -15 -6 11.23 2.31 -15 15 -6 12.27 2.17 -15 15 -6 9.03 1.86 15 15 6 11.03 2.12 -15 -15 -7 0.13 1.25 -15 15 -7 1.67 1.11 15 15 7 0.11 1.23 15 16 -13 2.48 1.18 15 16 -12 1.29 1.33 -15 16 11 5.70 2.50 15 16 -11 7.02 1.73 -15 -16 10 0.49 1.51 -15 16 10 3.07 2.38 15 16 -10 0.29 1.51 -15 -16 9 3.56 1.85 -15 16 9 4.05 2.62 15 16 -9 5.47 1.89 -15 -16 8 3.60 2.15 -15 16 8 5.57 2.77 15 16 -8 8.09 2.03 -15 -16 7 1.23 2.04 15 -16 -7 3.06 1.07 -15 16 7 6.22 2.84 15 16 -7 3.44 1.93 15 -16 -6 28.00 3.36 -15 -16 6 29.61 4.38 -15 16 6 29.08 4.73 15 16 -6 34.42 4.02 -15 -16 5 6.66 2.71 15 -16 -5 5.15 1.45 -15 16 5 10.91 2.95 15 16 -5 8.31 2.09 -15 -16 4 37.13 5.79 15 -16 -4 44.23 4.86 -15 16 4 43.21 5.82 15 16 -4 51.51 5.41 -15 -16 3 -1.45 2.56 15 -16 -3 -0.51 1.24 15 16 -3 2.21 2.07 -15 16 3 2.62 2.39 15 16 -3 -0.37 1.93 -15 -16 2 3.48 3.07 15 -16 -2 7.00 1.63 15 16 -2 6.08 2.31 -15 16 2 5.31 2.64 15 16 -2 5.27 2.15 -15 -16 1 10.00 3.01 15 16 -1 9.05 2.64 -15 16 1 9.43 2.77 15 16 -1 7.86 2.30 15 16 0 37.12 5.27 -15 -16 0 38.18 5.44 -15 16 0 45.57 5.17 -15 16 0 37.99 5.21 15 16 0 43.85 4.97 15 16 1 16.40 3.45 -15 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143.83 13.41 16 -6 -13 149.77 13.32 16 6 -13 114.41 13.02 16 -6 -13 118.87 13.32 16 6 -12 0.37 1.67 16 -6 -12 0.66 2.01 16 6 -12 2.05 2.28 16 -6 -12 3.35 2.39 16 6 -12 4.33 2.15 16 -6 -12 0.55 2.50 16 6 -11 4.26 2.36 16 -6 -11 10.19 2.82 16 6 -11 6.83 2.78 16 6 -11 7.73 2.20 16 -6 -11 6.92 2.32 -16 -6 10 -0.34 2.42 -16 -6 10 0.28 2.05 16 6 -10 -1.29 2.17 16 -6 -10 -2.59 2.41 16 6 -10 0.27 2.47 16 6 -10 1.45 1.98 16 -6 -10 -0.83 2.24 -16 6 9 39.86 6.87 -16 -6 9 54.95 6.63 16 -6 -9 50.80 6.66 16 6 -9 54.15 6.56 16 6 -9 56.80 6.76 16 6 -9 59.33 6.58 16 -6 -9 58.09 6.70 -16 -6 8 1.85 3.46 -16 6 8 3.58 2.95 -16 -6 8 9.07 2.68 16 -6 -8 5.27 2.45 16 6 -8 7.96 2.60 16 6 -8 7.63 2.74 16 -6 -8 6.83 2.63 16 6 -8 5.79 2.38 -16 -6 7 6.47 3.73 -16 6 7 -0.38 2.57 -16 6 7 1.42 2.66 -16 -6 7 -1.69 2.04 16 -6 -7 1.47 2.50 16 6 -7 1.98 2.37 16 6 -7 4.10 2.57 16 -6 -7 2.12 2.43 16 6 -7 1.76 2.35 -16 -6 6 1.84 3.58 -16 6 6 2.48 2.33 -16 6 6 2.85 2.44 -16 -6 6 5.55 2.42 16 -6 -6 5.63 2.65 16 6 -6 2.90 2.66 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1.55 16 -7 -18 0.94 1.23 16 -7 -17 15.00 2.07 16 7 -17 13.96 2.76 16 -7 -17 18.80 2.55 16 7 -16 1.55 1.13 16 -7 -16 2.21 1.67 16 -7 -16 1.15 1.11 16 7 -16 1.37 2.03 16 -7 -16 5.04 1.94 16 -7 -16 0.82 1.92 16 -7 -15 5.75 2.02 16 7 -15 8.02 1.75 16 -7 -15 7.86 1.70 16 7 -15 9.70 2.62 16 -7 -15 12.79 2.53 16 -7 -15 8.53 2.41 16 7 -14 -0.42 1.30 16 -7 -14 0.38 1.72 16 -7 -14 -0.11 1.19 16 7 -14 2.09 2.35 16 -7 -14 4.27 2.21 16 7 -14 -0.19 1.63 16 -7 -14 0.96 2.02 16 7 -13 3.67 2.07 16 -7 -13 5.54 2.57 16 7 -13 2.63 1.72 16 -7 -13 2.98 2.01 16 -7 -13 6.12 1.61 16 7 -13 10.07 2.93 16 -7 -12 -1.04 2.25 16 7 -12 -0.65 1.81 16 7 -12 0.33 1.48 16 -7 -12 0.21 1.86 16 7 -12 -1.28 2.46 16 7 -11 178.17 17.68 16 -7 -11 173.02 17.85 16 7 -11 177.02 17.39 16 -7 -11 165.54 17.55 16 7 -11 193.92 18.03 16 7 -10 2.85 2.03 16 -7 -10 -1.36 2.10 16 7 -10 1.35 2.50 16 7 -10 0.36 1.58 -16 -7 10 -0.41 3.26 -16 -7 9 56.99 9.36 -16 7 9 58.21 9.26 -16 -7 9 63.01 8.76 16 7 -9 95.23 8.93 16 -7 -9 87.51 9.03 16 7 -9 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-4 -2 12.82 1.73 23 -5 -8 1.53 0.70 23 -5 -7 5.14 1.17 23 -5 -7 6.49 1.06 23 -5 -6 3.24 1.00 23 -5 -6 1.48 0.75 23 -5 -5 -0.40 0.80 23 -5 -5 0.06 0.66 23 -5 -4 7.63 1.26 0 0 0 0.00 0.00 TITL pph349 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 18.888080 20.805033 19.552940 90.0000 103.5232 90.0000 ZERR 4.00 0.000322 0.000285 0.000342 0.0000 0.0018 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H O Ru UNIT 400.00 400.00 4.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 10108 _shelx_fab_file ; -23 0 2 0.9251 0.2588 -23 0 4 0.5032 0.0876 -23 0 6 -2.8925 0.1078 -23 0 8 1.9893 0.2426 -23 0 10 -1.6231 -0.3996 -23 1 1 0.0905 -0.0202 -23 1 2 -0.6566 0.0771 -23 1 3 -1.0462 -0.0863 -23 1 4 1.4813 -0.0402 -23 1 5 1.8521 -0.0170 -23 1 6 -0.7550 -0.0357 -23 1 7 -0.4251 -0.2593 -23 1 8 -0.0439 0.2385 -23 1 9 1.0329 -0.1516 -23 1 10 0.9547 -0.2119 -23 2 1 0.6383 -0.0833 -23 2 2 -0.1678 -0.0841 -23 2 3 -0.6075 -0.0822 -23 2 4 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correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.634 _oxdiff_exptl_absorpt_empirical_full_min 0.417