Table 1.
Native PlcHR2 | Se-Met PlcHR2 | |
---|---|---|
Beam line | X10SA | X06SA |
Wavelength [Å] | 1.000 | 0.95370 |
Temperature [K] | 100 K | 100 K |
Oscillation range [°] | 1 | 1 |
No. of frames | 180 | 170 |
Unit cell dimensions [Å], [°] | 175.5, 196.4, 325.3 | 157.9, 75.4, 141.0 β = 93.2 |
Space group | C2221 | C2 |
max. resolution [Å] | 4.0 | 2.75 |
No. observed reflections | 150 089 | 150 083 |
No unique reflections | 45 739 | 43 080 |
Completeness (last shell) | 95.6 (92.2) | 99.7 (99.3) |
R sym* (last shell) | 0.103 (0.352) | 0.130 (0.308) |
I/σ (last shell) | 8.3 (2.7) | 9.3 (4.7) |
R = SUM (I-<I>)2/SUM(I2)