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(a) Variable-temperature 1H NMR spectra of [LMeFe(µ-H)]2 (3) between 26 °C and 85 °C in C6D6. (b) Variable temperature 1H NMR spectra of 3 between −90 °C and 20 °C in toluene-d8. The asterisks indicate the resonance that splits with a coalescence temperature of 0 °C.