| Refinement on F2 | Hydrogen site location: mixed |
| Least-squares matrix: full | H atoms treated by a mixture of independent and constrained refinement |
| R[F2 > 2σ(F2)] = 0.075 | w = 1/[σ2(Fo2) + (0.1133P)2 + 4.1001P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.222 | (Δ/σ)max < 0.001 |
| S = 1.06 | Δρmax = 0.35 e Å−3 |
| 2334 reflections | Δρmin = −0.32 e Å−3 |
| 108 parameters | Absolute structure: Flack x determined using 458 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons et al., 2013) |
| 47 restraints | Absolute structure parameter: −0.018 (8) |
| Primary atom site location: iterative |