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. 2023 Nov 1;28(21):7378. doi: 10.3390/molecules28217378

Table 9.

A comparison of the common extraction methods used for obtaining star anise extracts.

Extraction Methods Optimal Extraction Conditions Extraction Rates
(Retain Two Significant Digits)
Advantages Disadvantages References
Steam distillation (SD) fruit size: 425 μm
granulometry < 0.425 mm
8% mass
1 h
water volume of 200 mL
10% Simple equipment, convenient operation and low cost Time-consuming and low oil yield [99]
Ultrasonic-assisted extraction (UE) solid-to-liquid ratio of 1:15 (g/mL)
crushing particle size of 60 mesh
ultrasonic time of 30 min
28% Stable temperature, simple operation, short extraction time Difficult and costly equipment manufacture [100]
Supercritical fluid CO2 extraction (SCFE) 1 h
extraction temperature 40 °C
extraction pressure 250 bar
15% Low temperature extraction
No solvent residue
Strict requirements for equipment and materials [9]
Microwave-assisted Soxhlet extraction (MAEE) ratio of solvent to sample 17 mL/g
extraction time 16 min
microwave power 505 W
25% Safe and environmentally friendly
High extraction rate
Short time
High operational requirements [35,98,99]