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. Author manuscript; available in PMC: 2024 Dec 7.

Published in final edited form as: Structure. 2023 Aug 3;31(12):1499–1503.e2. doi: 10.1016/j.str.2023.07.005

Table 1.

Data collection and refinement statistics

Data Collection
Excitation voltage	300kV
Electron Source	Field Emission Gun
Wavelength (Å)	0.019687
Total dose per crystal	~1 e⁻/Å²
Frame rate	2 fps
Rotation rate	0.15 °/s
Data Processing
Number of crystals	3
Space group	P2₁2₁2₁
Unit cell dimensions
a, b, c (Å)	18.28 32.00 41.67
α=β=γ (°)	90.000 90.000 90.000
Resolution (Å)	1.10
Total reflections	95,258
Total Unique Reflections	10,374
R_merge (%)	0.258 (0.794)^a
CC_1/2	0.977 (0.810)^a
Multiplicity	9.2 (9.3)^a
Completeness (%)	98.9 (99.6)^a
Mean (I/σ(I))	5.3 (1.9)^a
Data Refinement
R_work/R_free (%)	20.98/22.57
RMSD Bonds (Å)	0.020
RMSD Angles (°)	1.759

^a

Values for highest resolution shell of 1.13 Å – 1.10 Å