Figure 7.
Preparation of [11C]tozadenant from the N-Boc protected precursor 12. Conditions: (a) (Boc)2O, TEA, DMAP, THF, rt; (b) ammonium formate, Pd/C, DMF, 55 °C; (c) n.c.a. [11C]methyl iodide, NaOH, DMF, 60 °C; (d) conc. HCl, 100 °C.
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.