N-Cyclo­hexyl-N-(prop-2-en-1-yl)benzene­sulfonamide

Islam Ullah Khan; Zeeshan Haider; Muhammad Zia-ur-Rehman; Muhammad Nadeem Arshad; Muhammad Shafiq

doi:10.1107/S1600536809048077

. 2009 Nov 18;65(Pt 12):o3102. doi: 10.1107/S1600536809048077

N-Cyclohexyl-N-(prop-2-en-1-yl)benzenesulfonamide

Islam Ullah Khan ^a, Zeeshan Haider ^a, Muhammad Zia-ur-Rehman ^b,^*, Muhammad Nadeem Arshad ^a, Muhammad Shafiq ^a

PMCID: PMC2972124 PMID: 21578829

Abstract

The title compound, C₁₅H₂₁NO₂S, synthesized by N-alkylation of cyclohexylamine benzenesulfonamide with allyl iodide, is of interest as a precursor to biologically active sulfur-containing heterocyclic compounds. The cyclohexane ring is in a chair form and its mean plane makes a dihedral angle of 53.84 (12)° with the phenyl ring.

Related literature

For the synthesis of related molecules, see: Arshad et al. (2009 ▶); Zia-ur-Rehman et al. (2009 ▶). For biological applications of sulfonamides, see: Connor (1998 ▶); Berredjem et al. (2000 ▶); Lee & Lee (2002 ▶); Xiao & Timberlake (2000 ▶). For a related structure, see: Khan et al. (2009 ▶). For bond-length data, see: Allen et al. (1987 ▶). graphic file with name e-65-o3102-scheme1.jpg

Experimental

Crystal data

C₁₅H₂₁NO₂S
M _r = 279.39
Monoclinic,
a = 8.4911 (5) Å
b = 11.4176 (6) Å
c = 15.6274 (10) Å
β = 94.188 (3)°
V = 1511.00 (15) Å³
Z = 4
Mo Kα radiation
μ = 0.21 mm⁻¹
T = 296 K
0.38 × 0.18 × 0.12 mm

Data collection

Bruker APEXII CCD area-detector diffractometer
Absorption correction: multi-scan (SADABS; Sheldrick, 1996 ▶) T _min = 0.924, T _max = 0.975
16559 measured reflections
3746 independent reflections
2179 reflections with I > 2σ(I)
R _int = 0.047

Refinement

R[F ² > 2σ(F ²)] = 0.052
wR(F ²) = 0.144
S = 1.02
3746 reflections
172 parameters
H-atom parameters constrained
Δρ_max = 0.43 e Å⁻³
Δρ_min = −0.34 e Å⁻³

Data collection: APEX2 (Bruker, 2007 ▶); cell refinement: SAINT (Bruker, 2007 ▶); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008 ▶); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▶); molecular graphics: PLATON (Spek, 2009 ▶) and Mercury (Macrae et al., 2006 ▶); software used to prepare material for publication: WinGX (Farrugia, 1999 ▶) and PLATON.

Supplementary Material

Crystal structure: contains datablocks I, global. DOI: 10.1107/S1600536809048077/is2487sup1.cif

e-65-o3102-sup1.cif^{(18.6KB, cif)}

Structure factors: contains datablocks I. DOI: 10.1107/S1600536809048077/is2487Isup2.hkl

e-65-o3102-Isup2.hkl^{(183.7KB, hkl)}

Additional supplementary materials: crystallographic information; 3D view; checkCIF report

Acknowledgments

The authors are grateful to the Higher Education Commission of Pakistan for financial support to purchase the diffractometer.

supplementary crystallographic information

Comment

Sulfonamides are familiar in the literature for their anti-malarial, anti-convulsant and anti-hypertensive (Connor, 1998; Xiao & Timberlake, 2000; Berredjem et al., 2000; Lee & Lee, 2002) activities. As a part of our ongoing research program regarding the synthesis of sulfur containing heterocyclic compounds (Arshad et al., 2009; Zia-ur-Rehman et al., 2009; Khan et al., 2009), we herein report the crystal structure of the title compound (Fig. 1).

In the title molecule, bond lengths and bond angles are within the normal ranges (Allen et al., 1987). In the crystal structure, the phenyl ring is essentially planar while the cyclohexane ring is in a chair form. No significant hydrogen bond interactions are observed in the title molecule. The dihedral angle between the phenyl and cyclohexane rings is 53.84 (12)°.

Experimental

A mixture of N-cyclohexylbenzene sulfonamide (1.0 g, 0.43 mmol), sodium hydride (0.21 g, 0.88 mmol) and N, N-dimethylformamide (10.0 ml) was stirred at room temperature for half an hour followed by addition of allyl iodide (0.144 g, 0.86 mmol). Stirring was continued further for a period of three hours and the contents were poured over crushed ice. Precipitated product was isolated, washed and crystallized from methanol.

Figures

Fig. 1. — The molecular structure of the title compound, with displacement ellipsoids at the 50% probability level.

Crystal data

C₁₅H₂₁NO₂S	F(000) = 600
M_r = 279.39	D_x = 1.228 Mg m⁻³
Monoclinic, P2₁/n	Mo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2yn	Cell parameters from 3312 reflections
a = 8.4911 (5) Å	θ = 2.2–21.3°
b = 11.4176 (6) Å	µ = 0.21 mm⁻¹
c = 15.6274 (10) Å	T = 296 K
β = 94.188 (3)°	Needles, light yellow
V = 1511.00 (15) Å³	0.38 × 0.18 × 0.12 mm
Z = 4

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Data collection

Bruker APEXII CCD area-detector diffractometer	3746 independent reflections
Radiation source: fine-focus sealed tube	2179 reflections with I > 2σ(I)
graphite	R_int = 0.047
φ and ω scans	θ_max = 28.3°, θ_min = 2.2°
Absorption correction: multi-scan (SADABS; Sheldrick, 1996)	h = −11→11
T_min = 0.924, T_max = 0.975	k = −15→15
16559 measured reflections	l = −19→20

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Refinement

Refinement on F²	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F² > 2σ(F²)] = 0.052	Hydrogen site location: inferred from neighbouring sites
wR(F²) = 0.144	H-atom parameters constrained
S = 1.01	w = 1/[σ²(F_o²) + (0.0594P)² + 0.3938P] where P = (F_o² + 2F_c²)/3
3746 reflections	(Δ/σ)_max < 0.001
172 parameters	Δρ_max = 0.43 e Å⁻³
0 restraints	Δρ_min = −0.34 e Å⁻³

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Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

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Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²)

	x	y	z	U_iso*/U_eq
S1	0.27668 (7)	0.31209 (5)	0.25071 (4)	0.0519 (2)
O1	0.3713 (2)	0.21435 (17)	0.27943 (11)	0.0744 (6)
O2	0.3425 (2)	0.42730 (16)	0.25495 (14)	0.0776 (6)
N1	0.1228 (2)	0.31154 (15)	0.30554 (12)	0.0460 (5)
C1	0.2123 (2)	0.28696 (18)	0.14300 (14)	0.0438 (5)
C2	0.1843 (3)	0.3808 (2)	0.08789 (19)	0.0714 (8)
H2	0.2024	0.4570	0.1073	0.086*
C3	0.1297 (4)	0.3605 (3)	0.0047 (2)	0.0942 (11)
H3	0.1097	0.4233	−0.0324	0.113*
C4	0.1044 (4)	0.2497 (4)	−0.02421 (19)	0.0881 (10)
H4	0.0692	0.2370	−0.0812	0.106*
C5	0.1303 (3)	0.1558 (3)	0.03010 (18)	0.0744 (8)
H5	0.1110	0.0801	0.0101	0.089*
C6	0.1849 (3)	0.1740 (2)	0.11428 (16)	0.0534 (6)
H6	0.2032	0.1108	0.1513	0.064*
C7	0.0098 (2)	0.41024 (18)	0.29605 (14)	0.0416 (5)
H7	0.0635	0.4740	0.2679	0.050*
C8	−0.0307 (3)	0.45575 (19)	0.38291 (14)	0.0485 (6)
H8A	0.0654	0.4776	0.4164	0.058*
H8B	−0.0819	0.3943	0.4136	0.058*
C9	−0.1402 (3)	0.5618 (2)	0.37271 (16)	0.0584 (7)
H9A	−0.1702	0.5861	0.4287	0.070*
H9B	−0.0841	0.6263	0.3482	0.070*
C10	−0.2872 (3)	0.5350 (2)	0.31574 (16)	0.0573 (6)
H10A	−0.3497	0.4769	0.3433	0.069*
H10B	−0.3503	0.6055	0.3078	0.069*
C11	−0.2460 (3)	0.4895 (2)	0.22941 (16)	0.0621 (7)
H11A	−0.1928	0.5504	0.1993	0.074*
H11B	−0.3421	0.4689	0.1953	0.074*
C12	−0.1393 (3)	0.3822 (2)	0.23980 (15)	0.0539 (6)
H12A	−0.1959	0.3190	0.2655	0.065*
H12B	−0.1109	0.3563	0.1838	0.065*
C13	0.0737 (3)	0.20179 (19)	0.34549 (16)	0.0566 (6)
H13A	0.1046	0.1358	0.3114	0.068*
H13B	−0.0404	0.2007	0.3464	0.068*
C14	0.1475 (4)	0.1896 (2)	0.4359 (2)	0.0795 (9)
H14	0.2546	0.2069	0.4439	0.095*
C15	0.0842 (6)	0.1601 (3)	0.4985 (3)	0.1242 (14)
H15A	−0.0228	0.1417	0.4943	0.149*
H15B	0.1420	0.1557	0.5513	0.149*

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Atomic displacement parameters (Å²)

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
S1	0.0389 (3)	0.0632 (4)	0.0529 (4)	0.0041 (3)	−0.0012 (3)	−0.0167 (3)
O1	0.0604 (11)	0.1025 (14)	0.0580 (12)	0.0354 (10)	−0.0124 (9)	−0.0179 (10)
O2	0.0527 (10)	0.0808 (13)	0.1011 (15)	−0.0240 (9)	0.0184 (10)	−0.0401 (11)
N1	0.0466 (11)	0.0490 (10)	0.0423 (11)	0.0079 (8)	0.0035 (9)	−0.0034 (8)
C1	0.0376 (11)	0.0515 (12)	0.0429 (13)	0.0029 (9)	0.0074 (10)	−0.0026 (10)
C2	0.090 (2)	0.0625 (16)	0.0642 (19)	0.0097 (14)	0.0200 (16)	0.0112 (14)
C3	0.114 (3)	0.112 (3)	0.058 (2)	0.044 (2)	0.0161 (19)	0.026 (2)
C4	0.072 (2)	0.149 (3)	0.0426 (17)	0.027 (2)	−0.0041 (14)	−0.005 (2)
C5	0.0732 (19)	0.093 (2)	0.0562 (18)	−0.0054 (16)	0.0002 (15)	−0.0247 (16)
C6	0.0576 (15)	0.0552 (14)	0.0473 (14)	0.0014 (11)	0.0037 (12)	−0.0037 (11)
C7	0.0413 (12)	0.0455 (11)	0.0380 (12)	0.0012 (9)	0.0026 (10)	−0.0027 (9)
C8	0.0505 (13)	0.0538 (13)	0.0409 (13)	0.0021 (10)	0.0010 (11)	−0.0096 (10)
C9	0.0706 (17)	0.0520 (13)	0.0534 (15)	0.0092 (12)	0.0098 (13)	−0.0102 (11)
C10	0.0553 (15)	0.0609 (14)	0.0561 (16)	0.0170 (12)	0.0065 (12)	0.0024 (12)
C11	0.0565 (15)	0.0786 (17)	0.0496 (16)	0.0154 (13)	−0.0053 (12)	−0.0003 (13)
C12	0.0515 (14)	0.0666 (15)	0.0424 (14)	0.0077 (11)	−0.0056 (11)	−0.0133 (11)
C13	0.0663 (16)	0.0484 (13)	0.0549 (16)	0.0073 (11)	0.0034 (13)	−0.0028 (11)
C14	0.097 (2)	0.0728 (18)	0.070 (2)	0.0197 (16)	0.0169 (18)	0.0238 (16)
C15	0.164 (4)	0.111 (3)	0.097 (3)	0.014 (3)	0.009 (3)	0.025 (2)

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Geometric parameters (Å, °)

S1—O1	1.4283 (18)	C8—H8A	0.9700
S1—O2	1.4289 (17)	C8—H8B	0.9700
S1—N1	1.6136 (19)	C9—C10	1.511 (4)
S1—C1	1.755 (2)	C9—H9A	0.9700
N1—C13	1.474 (3)	C9—H9B	0.9700
N1—C7	1.481 (2)	C10—C11	1.510 (3)
C1—C6	1.380 (3)	C10—H10A	0.9700
C1—C2	1.385 (3)	C10—H10B	0.9700
C2—C3	1.368 (4)	C11—C12	1.525 (3)
C2—H2	0.9300	C11—H11A	0.9700
C3—C4	1.355 (5)	C11—H11B	0.9700
C3—H3	0.9300	C12—H12A	0.9700
C4—C5	1.375 (4)	C12—H12B	0.9700
C4—H4	0.9300	C13—C14	1.509 (4)
C5—C6	1.378 (4)	C13—H13A	0.9700
C5—H5	0.9300	C13—H13B	0.9700
C6—H6	0.9300	C14—C15	1.198 (4)
C7—C8	1.516 (3)	C14—H14	0.9300
C7—C12	1.522 (3)	C15—H15A	0.9300
C7—H7	0.9800	C15—H15B	0.9300
C8—C9	1.528 (3)

O1—S1—O2	119.70 (12)	H8A—C8—H8B	108.1
O1—S1—N1	106.79 (11)	C10—C9—C8	111.75 (18)
O2—S1—N1	107.95 (10)	C10—C9—H9A	109.3
O1—S1—C1	107.60 (10)	C8—C9—H9A	109.3
O2—S1—C1	106.76 (12)	C10—C9—H9B	109.3
N1—S1—C1	107.52 (10)	C8—C9—H9B	109.3
C13—N1—C7	119.21 (17)	H9A—C9—H9B	107.9
C13—N1—S1	119.58 (14)	C11—C10—C9	111.2 (2)
C7—N1—S1	119.19 (14)	C11—C10—H10A	109.4
C6—C1—C2	120.3 (2)	C9—C10—H10A	109.4
C6—C1—S1	119.87 (17)	C11—C10—H10B	109.4
C2—C1—S1	119.82 (19)	C9—C10—H10B	109.4
C3—C2—C1	119.4 (3)	H10A—C10—H10B	108.0
C3—C2—H2	120.3	C10—C11—C12	110.8 (2)
C1—C2—H2	120.3	C10—C11—H11A	109.5
C4—C3—C2	120.7 (3)	C12—C11—H11A	109.5
C4—C3—H3	119.7	C10—C11—H11B	109.5
C2—C3—H3	119.7	C12—C11—H11B	109.5
C3—C4—C5	120.5 (3)	H11A—C11—H11B	108.1
C3—C4—H4	119.8	C7—C12—C11	110.82 (19)
C5—C4—H4	119.8	C7—C12—H12A	109.5
C4—C5—C6	120.0 (3)	C11—C12—H12A	109.5
C4—C5—H5	120.0	C7—C12—H12B	109.5
C6—C5—H5	120.0	C11—C12—H12B	109.5
C5—C6—C1	119.2 (2)	H12A—C12—H12B	108.1
C5—C6—H6	120.4	N1—C13—C14	111.3 (2)
C1—C6—H6	120.4	N1—C13—H13A	109.4
N1—C7—C8	111.04 (17)	C14—C13—H13A	109.4
N1—C7—C12	113.81 (17)	N1—C13—H13B	109.4
C8—C7—C12	110.80 (18)	C14—C13—H13B	109.4
N1—C7—H7	106.9	H13A—C13—H13B	108.0
C8—C7—H7	106.9	C15—C14—C13	127.5 (4)
C12—C7—H7	106.9	C15—C14—H14	116.2
C7—C8—C9	110.76 (19)	C13—C14—H14	116.2
C7—C8—H8A	109.5	C14—C15—H15A	120.0
C9—C8—H8A	109.5	C14—C15—H15B	120.0
C7—C8—H8B	109.5	H15A—C15—H15B	120.0
C9—C8—H8B	109.5

O1—S1—N1—C13	−22.4 (2)	C2—C1—C6—C5	0.3 (4)
O2—S1—N1—C13	−152.36 (18)	S1—C1—C6—C5	178.25 (19)
C1—S1—N1—C13	92.80 (18)	C13—N1—C7—C8	64.3 (2)
O1—S1—N1—C7	173.87 (15)	S1—N1—C7—C8	−131.93 (17)
O2—S1—N1—C7	43.96 (19)	C13—N1—C7—C12	−61.5 (3)
C1—S1—N1—C7	−70.88 (17)	S1—N1—C7—C12	102.2 (2)
O1—S1—C1—C6	32.0 (2)	N1—C7—C8—C9	176.87 (18)
O2—S1—C1—C6	161.62 (18)	C12—C7—C8—C9	−55.6 (2)
N1—S1—C1—C6	−82.75 (19)	C7—C8—C9—C10	55.1 (3)
O1—S1—C1—C2	−150.1 (2)	C8—C9—C10—C11	−55.4 (3)
O2—S1—C1—C2	−20.4 (2)	C9—C10—C11—C12	56.1 (3)
N1—S1—C1—C2	95.2 (2)	N1—C7—C12—C11	−177.19 (19)
C6—C1—C2—C3	−0.2 (4)	C8—C7—C12—C11	56.8 (3)
S1—C1—C2—C3	−178.1 (2)	C10—C11—C12—C7	−56.9 (3)
C1—C2—C3—C4	−0.6 (5)	C7—N1—C13—C14	−104.9 (2)
C2—C3—C4—C5	1.3 (5)	S1—N1—C13—C14	91.5 (2)
C3—C4—C5—C6	−1.1 (5)	N1—C13—C14—C15	134.8 (4)
C4—C5—C6—C1	0.3 (4)

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Footnotes

Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: IS2487).

References

Allen, F. H., Kennard, O., Watson, D. G., Brammer, L., Orpen, A. G. & Taylor, R. (1987). J. Chem. Soc. Perkin Trans 2, pp. S1–19.
Arshad, M. N., Zia-ur-Rehman, M. & Khan, I. U. (2009). Acta Cryst. E65, o2596. [DOI] [PMC free article] [PubMed]
Berredjem, M., Régainia, Z., Djahoudi, A., Aouf, N. E., Dewinter, G. & Montero, J. L. (2000). Phosphorus Sulfur Silicon Relat. Elem 165, 249–264.
Bruker (2007). APEX2 and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA.
Connor, E. E. (1998). Prim. Care Update Ob. Gyn. 5, 32–35.
Farrugia, L. J. (1999). J. Appl. Cryst. 32, 837–838.
Khan, I. U., Haider, Z., Zia-ur-Rehman, M., Arshad, M. N. & Shafiq, M. (2009). Acta Cryst. E65, o2867. [DOI] [PMC free article] [PubMed]
Lee, J. S. & Lee, C. H. (2002). Bull. Korean Chem Soc. 23, 167–169.
Macrae, C. F., Edgington, P. R., McCabe, P., Pidcock, E., Shields, G. P., Taylor, R., Towler, M. & van de Streek, J. (2006). J. Appl. Cryst. 39, 453–457.
Sheldrick, G. M. (1996). SADABS. University of Göttingen, Germany.
Sheldrick, G. M. (2008). Acta Cryst. A64, 112–122. [DOI] [PubMed]
Spek, A. L. (2009). Acta Cryst. D65, 148–155. [DOI] [PMC free article] [PubMed]
Xiao, Z. & Timberlake, J. W. (2000). J. Heterocycl. Chem 37, 773–777.
Zia-ur-Rehman, M., Choudary, J. A., Elsegood, M. R. J., Siddiqui, H. L. & Khan, K. M. (2009). Eur. J. Med. Chem 44, 1311–1316. [DOI] [PubMed]

Associated Data

This section collects any data citations, data availability statements, or supplementary materials included in this article.

Supplementary Materials

Crystal structure: contains datablocks I, global. DOI: 10.1107/S1600536809048077/is2487sup1.cif

e-65-o3102-sup1.cif^{(18.6KB, cif)}

Structure factors: contains datablocks I. DOI: 10.1107/S1600536809048077/is2487Isup2.hkl

e-65-o3102-Isup2.hkl^{(183.7KB, hkl)}

Additional supplementary materials: crystallographic information; 3D view; checkCIF report

[bb1] Allen, F. H., Kennard, O., Watson, D. G., Brammer, L., Orpen, A. G. & Taylor, R. (1987). J. Chem. Soc. Perkin Trans 2, pp. S1–19.

[bb2] Arshad, M. N., Zia-ur-Rehman, M. & Khan, I. U. (2009). Acta Cryst. E65, o2596. [DOI] [PMC free article] [PubMed]

[bb3] Berredjem, M., Régainia, Z., Djahoudi, A., Aouf, N. E., Dewinter, G. & Montero, J. L. (2000). Phosphorus Sulfur Silicon Relat. Elem 165, 249–264.

[bb4] Bruker (2007). APEX2 and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA.

[bb5] Connor, E. E. (1998). Prim. Care Update Ob. Gyn. 5, 32–35.

[bb6] Farrugia, L. J. (1999). J. Appl. Cryst. 32, 837–838.

[bb7] Khan, I. U., Haider, Z., Zia-ur-Rehman, M., Arshad, M. N. & Shafiq, M. (2009). Acta Cryst. E65, o2867. [DOI] [PMC free article] [PubMed]

[bb8] Lee, J. S. & Lee, C. H. (2002). Bull. Korean Chem Soc. 23, 167–169.

[bb9] Macrae, C. F., Edgington, P. R., McCabe, P., Pidcock, E., Shields, G. P., Taylor, R., Towler, M. & van de Streek, J. (2006). J. Appl. Cryst. 39, 453–457.

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N-Cyclohexyl-N-(prop-2-en-1-yl)benzenesulfonamide

Islam Ullah Khan

Zeeshan Haider

Muhammad Zia-ur-Rehman

Muhammad Nadeem Arshad

Muhammad Shafiq

Abstract

Related literature

Experimental

Crystal data

Data collection

Refinement

Supplementary Material

Acknowledgments

supplementary crystallographic information

Comment

Experimental

Refinement

Figures

Fig. 1.

Crystal data

Data collection

Refinement

Special details

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²)

Atomic displacement parameters (Å²)

Geometric parameters (Å, °)

Footnotes

References

Associated Data

Supplementary Materials

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N-Cyclo­hexyl-N-(prop-2-en-1-yl)benzene­sulfonamide

Islam Ullah Khan

Zeeshan Haider

Muhammad Zia-ur-Rehman

Muhammad Nadeem Arshad

Muhammad Shafiq

Abstract

Related literature

Experimental

Crystal data

Data collection

Refinement

Supplementary Material

Acknowledgments

supplementary crystallographic information

Comment

Experimental

Refinement

Figures

Fig. 1.

Crystal data

Data collection

Refinement

Special details

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2)

Atomic displacement parameters (Å2)

Geometric parameters (Å, °)

Footnotes

References

Associated Data

Supplementary Materials

ACTIONS

PERMALINK

RESOURCES

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N-Cyclohexyl-N-(prop-2-en-1-yl)benzenesulfonamide

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²)

Atomic displacement parameters (Å²)