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UV/Vis spectral changes observed in the four-electron reduction of O2 (0.22 mm) by Fc* (a) 3.0 mm at 298 K and b) 1.0 mm at 253 K) with TFA (10 mm) catalyzed by a) 1 (0.10 mm) and b) 2 (0.10 mm) in acetone. Inset shows the time profile of the absorbance at 780 nm due to Fc*+.