| Bruker APEXII CCD area-detector diffractometer | 2772 independent reflections |
| Radiation source: fine-focus sealed tube | 2363 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.026 |
| ω and φ scans | θmax = 27.9°, θmin = 2.3° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −9→9 |
| Tmin = 0.972, Tmax = 0.992 | k = −11→11 |
| 11668 measured reflections | l = −10→12 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.