Table 2.
Entry | Conditions | Results |
---|---|---|
1 |
tert-BuOk tert-BuOH, rt, 20min |
Decomposition |
2 | NaOH, H2O Et2O, rt, 1h |
No rearrangement |
3 | Starting Material + unidentified product |
|
4 | NaH, THF 0 °C, 30 min |
Entry | Conditions | Results |
---|---|---|
1 |
tert-BuOk tert-BuOH, rt, 20min |
Decomposition |
2 | NaOH, H2O Et2O, rt, 1h |
No rearrangement |
3 | Starting Material + unidentified product |
|
4 | NaH, THF 0 °C, 30 min |