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. Author manuscript; available in PMC: 2013 Mar 5.
Published in final edited form as: Chemistry. 2012 Feb 3;18(10):2961–2971. doi: 10.1002/chem.201102899

Table 2.

Attempts at Payne Rearrangement

graphic file with name nihms-370017-t0022.jpg

Entry Conditions Results
1 tert-BuOk
tert-BuOH, rt, 20min
Decomposition
2 NaOH, H2O
Et2O, rt, 1h
No rearrangement
3 graphic file with name nihms-370017-t0023.jpg Starting Material
+ unidentified product
4 NaH, THF
0 °C, 30 min
graphic file with name nihms-370017-t0024.jpg