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. Author manuscript; available in PMC: 2014 Nov 25.
Published in final edited form as: Organometallics. 2013 Nov 25;32(22):10.1021/om400651p. doi: 10.1021/om400651p

Scheme 2.

Scheme 2

a Catalytic borylation conditions: 5 mol% Tf2NH, PhMe, sealed tube, 160 °C, 14h, quenched with ca. 10 mol% n-Bu4NBH4. b Stoichiometric borylation conditions: 0.9 equiv Ph3C+ [B(C6F5)4]−, PhF, rt, 4h, quenched with ca. 1.1 equiv n-Bu4NBH4.