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Results of serial addition of Fc* to [1]0. The solution began with 5 equiv of Fc* and 20 equiv of [H(OEt2)2]BArF4. Asterisks mark the time that the headspace was analyzed and then evacuated. To the resulting solid was added another solution of 5 equiv of Fc*, and the headspace was reanalyzed after 30 min and then evacuated.
