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2D 31P-1H correlation spectra with 1H homonuclear decoupling, measured at 306 K under OMAS at 58.7°. (a) Pulse sequence for the homonuclear-decoupled HETCOR experiment. (b) 2D spectrum without 1H spin diffusion. (c) 2D spectrum with 0.5 ms 1H spin diffusion. (d) 1D 1H MAS spectrum. (e) 1D 1H OMAS spectrum at 58.7°. (f) 1H cross sections of DMPC with 0.5 ms (top) and 0 ms (bottom) spin diffusion, extracted from the 2D spectra in (b) and (c).
