| Crystal data |
| Chemical formula |
[Cd2(C8H6NO4)2(NO3)2(C10H8N2)2]CH4O |
|
M
r
|
1053.50 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
295 |
|
a, b, c () |
8.4096(5), 10.9626(6), 11.5056(4) |
| , , () |
71.241(4), 86.537(4), 86.803(5) |
|
V (3) |
1001.79(9) |
|
Z
|
1 |
| Radiation type |
Mo K
|
| (mm1) |
1.14 |
| Crystal size (mm) |
0.36 0.14 0.10 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Gemini CCD S Ultra |
| Absorption correction |
Multi-scan (CrysAlis PRO; Oxford Diffraction, 2009 ▸) |
| No. of measured, independent and observed [I > 2(I)] reflections |
21744, 4819, 4155 |
|
R
int
|
0.057 |
| (sin /)max (1) |
0.684 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.036, 0.092, 1.01 |
| No. of reflections |
4819 |
| No. of parameters |
298 |
| No. of restraints |
4 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
1.07, 0.74 |
