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. 2015 Feb 17;21(14):5380–5386. doi: 10.1002/chem.201405931

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© 2015 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution Non-Commercial NoDerivs License, which permits use and distribution in any medium, provided the original work is properly cited, the use is non-commercial and no modifications or adaptations are made.

© 2015 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution Non-Commercial NoDerivs License, which permits use and distribution in any medium, provided the original work is properly cited, the use is non-commercial and no modifications or adaptations are made.

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Scheme 6 — Preparation of ruthenacycles [7]Cl, [7]OAc, and [7-OH₂]SbF₆. Conditions: (i) [{RuCl₂(p-cymene)}₂] (0.5 equiv), MeOH, RT, 24 h, 78 %; ii) AgOAc (2.5 equiv), MTBE, RT, 24 h, 80 %; iii) AgSbF₆ (1.1 equiv), H₂O (6.9 equiv), [D₈]THF, RT. ORTEP representation of complex [7]Cl. Ellipsoids are drawn at the 50 % probability level with the MeOH solvate omitted for clarity. MTBE=methyl tert-butyl ether.