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Transmetalation experiments
| Entry | Complex | Cu(OAc)2⋅H2O | [7]tol | 2 a |
|---|---|---|---|---|
| 1 | [7]Cl | yes | – | – |
| 2 | [7]Cl | no | – | – |
| 3 | [7]OAc | yes | – | traces |
| 4 | [7]OAc | no | –[a] | 15 % |
| 5 | [7-OH2]SbF6 | yes | – | traces |
| 6 | [7-OH2]SbF6 | no | – | traces |
[a] A symmetrical complex of the type [Ru(p-cymene)]X2 was observed by 1H NMR spectroscopic analysis at the end of the reaction.[41]
