Table 1.
Data collection and refinement statistics.
| PtAu1aLOV dark | PtAu1aLOV light | |
|---|---|---|
| Data collection | ||
| Space group | P212121 | P3221 |
| Cell dimensions | ||
| a, b, c (Å) | 64.4, 69.2, 74.6 | 108.6 108.6 104.7 |
| α, β, γ (°) | 90.0, 90.0, 90.0 | 90.0 90.0 120.0 |
| Resolution (Å) | 50–2.5 (2.5–2.6) * | 50–2.7 (2.7–3.2) |
| Rmeas | 13.2 (55.1) | 10.0 (63.7) |
| I / σI | 15.57 (4.50) | 13.01 (2.46) |
| Completeness (%) | 99.9 (100) | 98.9 (98.1) |
| Redundancy | 13.1 (13.5) | 5.0 (5.0) |
| Refinement | ||
| Resolution (Å) | 48.7-2.5 | 45.7-2.7 |
| No. reflections | 12,016 | 19,785 |
| Rwork / Rfree | 0.196/0.254 | 0.209/0.243 |
| No. atoms | 2237 | 2164 |
| Protein | 2108 | 2100 |
| Ligand/ion | 74 | 62 |
| Water | 55 | 2 |
| B factors | 33.3 | 74.7 |
| Protein | 33.4 | 74.9 |
| Ligand/ion | 32.6 | 69.1 |
| Water | 32.2 | 72.3 |
| r.m.s. deviations | ||
| Bond lengths (Å) | 0.007 | 0.009 |
| Bond angles (°) | 1.109 | 1.090 |
*Values in parentheses are for highest-resolution shell. One crystal was used for data measurements of PtAu1aLOV in its dark and light-adapted state, respectively.