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. Author manuscript; available in PMC: 2017 Aug 16.
Published in final edited form as: Polyhedron. 2016 Aug 16;114:118–127. doi: 10.1016/j.poly.2015.11.014

Table 2.

Crystallographic data. L = PyMeEBC

[Ni(4)Cl]PF6
sja4_12		 [Cu(4)](PF6)2
sja26_12		 [Zn(4)Cl]PF6
sja3_12
Chemical Formula C17 H29 Cl F6 N5 Ni P C17 H29 Cu F12 N5 P2 C17 H29 Cl F6 N5 P Zn
a = …(esd) Å 11.6458(10) 11.4577(9) 11.584(2)
b = …(esd) Å 11.6930(12) 12.2495(14) 11.729(3)
c = …(esd) Å 15.6867(13) 17.1539(14) 15.730(3)
α = …(esd) degrees 90 90 90
β = …(esd) degrees 97.680(7) 95.837(6) 96.95(2)
γ = …(esd) degrees 90 90 90
V = … Å3 2117.0(3) 2395.1(4) 2121.6(9)
Z = 4 4 4
Formula Weight 542.58 656.93 549.24
Space Group P21/c P21/c P21/c
T = … K 150(2) 150(2) 150(2)
λ = … Å 0.71073 0.71073 0.71073
Dcalcd = … g cm−3 1.702 1.822 1.720
μ = … mm−1 1.186 1.157 1.427
R1(Fo2) = 0.1144 0.1125 0.0598
wR2 (Fo2) = 0.1980 0.1389 0.0660