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STM images of a) TBPB deposited on Pd(111) at 300 K; the inset shows a close‐up of a feature corresponding to a debrominated TBPB molecule. The dashed circle highlights hexagonally arranged split‐off Br adatoms. b) Porous sCOF formed upon deposition of TBPB on the Au–Pd(111) held at 475 K; the inset shows a close‐up of filled pores. The dashed perimeter indicates the boundary of a Br island within the sCOF on top of a Moiré pattern (−0.6 V, 300 pA).
