| Crystal data |
| Chemical formula |
C26H28N5O2
+·Cl−·CH4O |
|
M
r
|
510.03 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
10.5572 (5), 11.0764 (4), 11.4408 (5) |
| α, β, γ (°) |
104.622 (1), 97.327 (2), 90.695 (1) |
|
V (Å3) |
1282.57 (10) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.19 |
| Crystal size (mm) |
0.50 × 0.46 × 0.38 |
| |
| Data collection |
| Diffractometer |
Rigaku R-AXIS RAPID/ZJUG |
| Absorption correction |
Multi-scan (ABSCOR; Higashi, 1995 ▸) |
|
T
min, T
max
|
0.91, 0.93 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
11090, 5000, 3865 |
|
R
int
|
0.044 |
| (sin θ/λ)max (Å−1) |
0.617 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.053, 0.154, 1.00 |
| No. of reflections |
5000 |
| No. of parameters |
328 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.31, −0.43 |
