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SAXS patterns obtained from 1.0% w/w aqueous dispersions of PMAA56–PHBMAy diblock copolymer nano-objects at pH 5: (a) PMAA56–PHBMA50 spheres, (b) PMAA56–PHBMA150 “monkey nut” nanoparticles (prepared using purified HBMA monomer), (c) PMAA56–PHBMA150 “monkey nut” nanoparticles (prepared using as-received HBMA monomer), (d) PMAA56–PHBMA300 spheres, and (e) PMAA56–PHBMA1000 spheres.
