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1H NMR spectra of ACV starting material (upper spectrum, 400 MHz), and the oxidised product 7 (lower spectrum, 500 MHz). Assignments are for α‐, β‐, γ‐, δ‐ and methyl protons on the aminoadipoyl (A), cysteinyl (C) and valinyl (V) portions of the substrate. The asterisks indicate new peaks in the spectrum of 7 compared to ACV 1.
