Table 1.
Position | δH (mult., J in Hz) | δC |
---|---|---|
1 | 168.2 | |
2 | 5.79 (1H, s) | 118.3 |
3 | 152.0 | |
4 | 8.00 (1H, d, 15.7) | 131.7 |
5 | 6.55 (1H, d, 15.7) | 135.7 |
1′ | 83.3 | |
2′ | 87.8 | |
3′ | 2.03 (1H, dd, 13.7, 7.0) 1.73 (1H, dd, 13.7, 10.4) | 46.0 |
4′ | 4.12 (1H, m) | 66.0 |
5′ | 1.86 (1H, dd, 13.5, 6.9) 1.68 (1H, dd, 13.5, 13.5) | 44.6 |
6′ | 49.2 | |
7′ | 1.16 (3H, s) | 19.6 |
8′ | 0.94 (3H, s) | 16.4 |
9′ | 3.82 (1H, d, 7.5) 3.72 (1H, d, 7.5) | 77.3 |
CH3-3 | 2.10 (3H, s,) | 21.2 |
OCH3 | 3.70 (3H, s) | 51.6 |