Table 1.
Recovering of soluble and insoluble material obtained by two crude heparin samples. Weightings before and after the separation and lyophilization procedure are shown.
| Sample | Crude (mg/mL) | Stirring | Supernatant (mg) | Precipitate (mg) | Weight loss % (%w) | Precipitate (%w) |
|---|---|---|---|---|---|---|
| G9709 | 40.4 | No | 35.3 | 1.2 | 9.7 | 3.3 |
| G9709 | 40.8 | No | 35.4 | 1.0 | 10.8 | 2.7 |
| G9709 | 38.9 | No | 33.7 | 1.2 | 10.3 | 3.4 |
| G9709 | 39.0 | Yes | 34.0 | 1.1 | 10.0 | 3.1 |
| G9709 | 79.7 | No | 60.4 | 10.0 | 11.7 | 14.2 |
| G9709 | 81.4 | Yes | 62.4 | 9.4 | 11.8 | 13.1 |
| G9710 | 39.0 | No | 33.8 | 2.7 | 6.4 | 7.4 |
| G9710 | 39.3 | Yes | 33.2 | 2.1 | 10.2 | 5.9 |
| G9710 | 79.5 | No | 56.8 | 13.8 | 11.2 | 19.5 |
| G9710 | 80.5 | Yes | 59.3 | 13.0 | 10.2 | 18.0 |