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. 2018 Jul 24;23(8):1838. doi: 10.3390/molecules23081838

Table 2.

Control reactions for the iminoiodinane/I2 formation of N-sulfonyl imines.

graphic file with name molecules-23-01838-i002.jpg

Entry Variation from Standard Conditions Yield 2de (%) 1
1 NONE 72
2 0 equiv. I2 40
3 0.2 equiv. I2 66
4 4A Molecular sieves 8
5 Reaction in dark 2 74
6 1 equiv. TEMPO 19

1 Yields are based upon 1H-NMR integration with internal standard. 2 Reaction vessel was wrapped in aluminum foil and the experiment was performed in a laboratory with all lights turned off.