Table 9.
Yield of water mediated N-Boc-aniline deprotection at different temperatures [77].
| Entry | Temperature (°C) | Time (h) | Isolated yield (%) |
|---|---|---|---|
| 1 | 30 | 4 | 0 |
| 2 | 80 | 4 | 0 |
| 3 | 130 | 2 | 12 |
| 4 | 130 | 4 | 39 |
| 5 | 150 | 2 | 38 |
| 6 | 150 | 4 | 86 |
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