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. 2011 Dec 16;16(12):10471–10478. doi: 10.3390/molecules161210471

Table 1.

1H-NMR data of 3 (600 MHz, CDCl3) a.

H   H  
1 1.01 m 14 1.36 dd (10.2, 2.5) α
1.97 m 1.76 m β
2 1.69 m 15 5.83 dd (17.3, 10.7)
1.78 m
3 3.23 dd (11.5, 4.7)b 16 4.94 dd (10.7, 0.8)
4.96 dd (17.3, 0.8)
6 5.56 d (6.3) 17 0.97 s
7 1.87 m 18 0.99 s
1.98 m
8 1.77 m 19 1.15 s
10 2.72 m 20 0.98 s
12 1.95 dd (12.6, 2.5) α    
2.73 d (12.6) β

a Chemical shift values are in δ (ppm); b Coupling constants are in Hz.