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. 2011 Sep 19;16(9):8041–8052. doi: 10.3390/molecules16098041

Table 2.

1H-NMR data of compounds 1–5.

Comp. Solvent δNH δHB 1J(C,HB) δHA 1J(C,HA) 2J(H,H)
1a CDCl3 6.35 4.89 159 4.51 157 11.5
DMSO 9.44 4.69 4.40 9.6
1b CDCl3 4.96 4.82 11.0
DMSO 5.17 4.87 11.3
1c CDCl3 6.49 4.81 159 4.66 157 11.6
DMSO 9.67 4.61 158 4.56 157 9.9
1d CDCl3 6.55 4.86 4.57 11.8
DMSO 9.62 4.67 4.53 9.7
1e CDCl3 7.37 5.19 160 4.74 158 14.6
DMSO 9.78 4.93 158 4.48 156 11.1
1f CDCl3 6.45 4.91 159 4.63 156.4 11.8
DMSO 9.58 4.67 160 4.57 158.7 9.6
1g CDCl3 6.56 4.86 4.62 11.3
DMSO 9.65 4.62 4.59 9.7
1h CDCl3 6.45 4.92 158 4.63 156 11.5
DMSO 9.62 4.68 159 4.59 157 9.7
1i CDCl3 4.91 4.84 11.0
DMSO 5.18 4.85 11.4
2a CDCl3 10.88 6.28 5.76 14.1
DMSO 10.10 5.99 5.49 15.0
2b CDCl3 6.82 152.1 6.59 146.3 15.6
DMSO 6.45 152.2 5.77 146.2 16.0
2c CDCl3 10.98 6.35 153.1 5.97 147.1 13.6
DMSO 10.48 5.97 151.1 5.66 149.1 15.1
2d CDCl3 10.80 6.16 6.11 14.1
DMSO 10.15 5.90 150.1 5.62 149.2 14.9
2e CDCl3 10.31 6.30 6.06 14.1
DMSO 10.20 5.97 5.64 15.6
2f CDCl3 10.92 6.38 150.6 5.92 146.5 13.6
DMSO 10.34 6.08 151.9 5.63 146.4 15.3
2g CDCl3 10.88 6.24 6.10 13.7
DMSO 10.31 5.94 5.46 14.9
2h CDCl3 6.84 6.62 15.8
DMSO 6.39 5.77 16.2
3a CDCl3 10.96 6.40 150.7 5.89 146.5 13.9
DMSO 10.21 6.08 151.1 5.56 145.4 15.1
3b CDCl3 10.95 6.40 151.4 5.89 146.3 13.9
DMSO 10.12 6.07 152.4 5.53 146.3 15.0
3c CDCl3 10.92 6.32 150.1 5.86 146.2 13.8
DMSO 10.28 6.08 152.1 5.56 146.4 15.1
3d CDCl3 10.96 6.40 148.3 5.89 146.2 13.9
DMSO 10.12 6.07 5.53 15.2
3e CDCl3 6.73 152.5 6.56 150.2 16.1
DMSO 6.48 152.5 5.78 147.5 16.5
4a CDCl3 8.30 4.52 and 4.47 16.7
DMSO 9.74 4.84 and 4.74 16.5
4f CDCl3 6.42 4.69 and 4.65 16.4
5a DMSO 9.91 4.72 and 4.65 16.0
5f DMSO 9.97 4.64 and 4.60 16.2